Dry Scrubber Blue Goose Combustion Data Septem ber 2010 Fyrite

Location : Dry

Scrubber Date 9/14/10 Time: 9:30

run O2 CO2

1 18 2 2 18 2 3 18 2
Avg 18 2

Molecular wt

1 29.04 2 29.04 3 29.04

AVG 29.04

diff 0

0 0

All diff must be less that 0.3
Analysts: O,Brien & Gere

Page 1Test ID: 9-14-10-POM-BG-Run# 2 

### Value 0

0 0

275.00 95.00 0.0021 0.0000 0.0000 200.00 200.00 0.0021

300.00 125.00 0.002 0.002

940.00 1000.00 0.0014 0.0001 0.00130



### Value 3.3000 2.1000 5.4000 Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)

Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #2** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/14/2010

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml)Test ID: 9-14-10-POM-BG-Run# 2



### Value 0.5869 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 2.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.04 28.53678307 0.045581244 532.8 636.9 29.84 70 1.92 1.004 29.84 128 1.19 80.24 81 29.82 0.252 0.00034636059



### Value 79.8551977 36.45753 67.7 3.18664 13.3 0.627095 0.045581 0.029517 104.4205 I = % Isokinetic variation 

### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moisture Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute average temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg) Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #2**  **9/14/2010**

**Method 5 Parameter**  p = Stack gas v elocity pressure (av g. sqrt  p - in. water) Cp = Pitot tube calibration coefficientTest ID: 9-14-10-POM-BG-Run# 2 LIMS ID#: 2010010513



### Value 3.3000 0.0033 2.1 0.0021 79.85519775 29.84 38.48 10.06 Green Carbon produced tons/hr 0.045581244 66377.54866 3982652.9194 84173.13852 Acfm 69547.61549 Scfm 0.0010 Emission Rate of Total MCEM gr/dscf 0.36 8.70 0.2307 5.54 **0.59**

**0.036 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon Baked**  **0.023 Emission Rate of Particulate MCEM lb/Ton of Green Carbon Baked**  **0.059 Emission Rate of Total MCEM lb/Ton of Green Carbon Baked** 

Start time: 9/14/2010 12:42 End time: 9/14/2010 15:03

Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #2**  **9/14/2010**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d

## Value 1.6

0.0016 79.85519775 29.84 38.48 10.06 Green Carbon produced tons/hr 0.045581244 66422.0675 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 3985324.048 0.0003 Particulate gr/dscf **0.18 Particulate lb/hr** 

**0.017 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Dry Scrubber Test #2**  **9/14/2010**

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions