USDA Agricultural Marketing Service 

- U.S. DEPARTMENT OF AGRICULTURE 

Agricultural 

Marketing Pesticide Data Program Service 

Annual Summary, Calendar Year 2021 Science and 

Technology 

Program 

Visit the program website at: www.ams.usda.gov/pdp 

December 2022 
United States Department of Agriculture

December 2022

Dear Reader:

We are pleased to present the Pesticide Data Program’s (PDP’s) 31st Annual Summary for calendar 

year 2021. The 31 years of PDP residue data (available through our website) represent one of the 

largest sources of food pesticide residue data available. 

The U.S. Department of Agriculture (USDA), Agricultural Marketing Service (AMS) conducts the 

PDP each year to collect new/updated data on pesticide residues in food. This Annual Summary 

report shows that when pesticide residues are found on foods, they are nearly always at levels below 

the tolerance or maximum amount of a pesticide allowed to remain in or on a food, that is set by the 

U.S. Environmental Protection Agency (EPA).

The PDP provides high-quality, nationally representative pesticide residue data that contribute to the 

information available to help ensure consumer confidence in the foods they provide to their families. 

More than 99 percent of the products sampled through PDP had residues below the established EPA 

tolerances. Ultimately, if EPA determines a pesticide use is not safe for human consumption, EPA will 

mitigate exposure to the pesticide through actions such as amending the pesticide label instructions or 

changing or revoking a pesticide residue tolerance, or not registering a new use.

The PDP tests a wide variety of domestic and imported foods, with a strong focus on foods that are 

consumed by infants and children. EPA relies on PDP data to conduct dietary risk assessments and to 

review the maximum amount of a pesticide allowed to remain in or on a food. USDA uses the data 

to better understand the relationship of pesticide residues to agricultural practices and to implement 

USDA’s Integrated Pest Management objectives. USDA also works with U.S. growers to improve 

agricultural practices and to facilitate the adoption of integrated pest management techniques, 

including judicious use of pesticides, throughout the food supply chain.

The PDP is not designed for enforcement of EPA pesticide residue tolerances. Rather, the U.S. Food 

and Drug Administration (FDA) is responsible for enforcing EPA tolerances. The PDP provides FDA 

and EPA with monthly reports of pesticide residue testing and informs the FDA if residues detected 

exceed the EPA tolerance or have no EPA tolerance established.

To collect the data in this Annual Summary report, the PDP works with State agencies representing 

all census regions of the country and nearly half of the U.S. population. In 2021, analyzed samples 

were collected in California, Colorado, Florida, Maryland, Michigan, New York, Ohio, Texas, and 

Washington.

For more information about PDP, please visit our website at https://www.ams.usda.gov/datasets/pdp. 

For additional information about pesticides and food, please visit EPA’s website at http://www.epa.

gov/safepestcontrol and FDA’s website at http://www.fda.gov/Food/Chemicals-Metals-PesticidesFood/Pesticides.

Agricultural Marketing Service

1400 Independence Avenue, SW, Washington, DC 20250-0201

Voice (202) 720-8998 Fax (202) 720-7135

An Equal Opportunity Provider and Employer
Pesticide Data Program—Annual Summary, Calendar Year 2021

iii

Contents

Page No.

Acknowledgements........................................................................................................................ vii

Executive Summary...................................................................................................................... ix

Acronyms and Abbreviations........................................................................................................ xi

Section I--Introduction............................................................................................................... 1

Section II--Sampling Operations............................................................................................... 4

A. Conceptual Framework............................................................................................... 4

B. Sampling Procedures................................................................................................... 5

C. 2021 Sampling Operations.......................................................................................... 6

D. Fresh and Processed Commodities............................................................................. 7

E. Corn Grain................................................................................................................... 7

F. Butter........................................................................................................................... 13

G. Sampling Limitations.................................................................................................. 13

Section III--Laboratory Operations......................................................................................... 14

A. Overview..................................................................................................................... 14

B. Fresh and Processed Commodities............................................................................. 14

C. Corn Grain................................................................................................................... 16

D. Butter........................................................................................................................... 16

E. Quality Assurance Program......................................................................................... 16

Section IV--Database Management.......................................................................................... 18

A. Electronic Data Path................................................................................................... 18

B. Data Reporting............................................................................................................ 18

C. Online Database Search Tool...................................................................................... 20

Section V--Sample Results and Discussion.............................................................................. 20

A. Overview..................................................................................................................... 20

B. Import Versus Domestic Residue Comparisons.......................................................... 21

C. Postharvest Applications............................................................................................. 22

D. Discussion of Results ................................................................................................. 22

E. Special Projects............................................................................................................ 22

F. Environmental Contaminants....................................................................................... 23

G. Tolerance Violations..................................................................................................... 24

H. Look Ahead................................................................................................................... 25
Pesticide Data Program—Annual Summary, Calendar Year 2021

v

Figures Page No.

 1 Pesticide Data Program (PDP) Program Operations Support and Data Users................... 2

 2 Program Participants........................................................................................................... 3

 3 Commodity Origin.............................................................................................................. 10

 4 Origin of Selected Fresh Commodities: Blueberry, Eggplant and Winter Squash............. 12

 5 Location of Corn Grain Samples by Grower State............................................................. 13

 6 Pesticide Data Program (PDP) Data Pathway..................................................................... 19

Tables

 1 Pesticide Data Program (PDP) Commodity Collection Schedule for 2021........................ 6

 2 Distribution of Samples Collected by Each Participating State.......................................... 8

 3 Acceptable Products for Collected Commodities................................................................ 9

 4 Sample Preparation Steps for Analysis................................................................................ 15

 

Appendixes A-J

Appendix A Commodity History

Appendix B Distribution of Residues by Pesticide in Fruit and Vegetables

Appendix C Distribution of Residues by Pesticide in Corn Grain

Appendix D Distribution of Residues by Pesticide in Butter

Appendix E Distribution of Residues for Environmental Contaminants

Appendix F Sample Origin by State or Country

Appendix G Import Versus Domestic Pesticide Residue Comparisons

Appendix H Pesticide Residues by Commodity

Appendix I Number of Pesticides Detected per Sample

Appendix J Samples Reported to the U.S. Food and Drug Administration 

 as Exceeding the Tolerance or Without Established Tolerance
Pesticide Data Program—Annual Summary, Calendar Year 2021

vii

Acknowledgements

The States participating in the Pesticide Data 

Program (PDP) deserve special recognition for 

their contributions to the program. The dedication 

and flexibility of sample collectors allow the U.S. 

Department of Agriculture’s (USDA) Agricultural 

Marketing Service (AMS) to adjust sampling 

protocols when responding to changing trends 

in commodity distribution and availability. PDP 

acknowledges the contributions of the State 

laboratories in providing testing services to the 

program and the USDA, National Agricultural 

Statistics Service for providing statistical support. 

PDP also acknowledges the exceptional support 

of the Health Effects Division staff of the U.S. 

Environmental Protection Agency, Office of 

Pesticide Programs, and the U.S. Food and Drug 

Administration, Center for Food Safety and 

Applied Nutrition, Office of Food Safety, in 

helping to set the direction for PDP. 

 

Data presented in this report are the latest available 

and were collected and processed through the 

efforts of the following organizations:

USDA Program Administration

Agricultural Marketing Service

Science and Technology Program

1400 Independence Ave., SW

South Building, Mail Stop 0270

Washington, DC 20250

Ruihong Guo, Ph.D., Deputy Administrator

Science and Technology Program, AMS

(202) 720-8556

Brenda Foos, Director

Monitoring Programs Division, AMS

1400 Independence Ave, SW

South Building, Mail Stop 0276

Washington, DC 20250

(202) 572-8167

Electronic-mail Address:

amsmpo.data@usda.gov

Website:

http://www.ams.usda.gov/pdp

Participating State Agencies

California Department of Food and Agriculture

California Department of Pesticide Regulation

Colorado Department of Agriculture

Florida Department of Agriculture and

 Consumer Services

Maryland Department of Agriculture

Michigan Department of Agriculture and 

 Rural Development

New York Department of Agriculture and 

 Markets

Ohio Department of Agriculture

Texas Department of Agriculture

Washington State Department of Agriculture

Participating Laboratories

California Department of Food and Agriculture

Division of Inspection Services

Center for Analytical Chemistry

3292 Meadowview Rd.

Sacramento, CA 95832

 

Florida Department of Agriculture and

 Consumer Services

Chemical Residue Laboratory

3125 Conner Blvd., Bldg. 3

Tallahassee, FL 32399-1650

Michigan Department of Agriculture and 

 Rural Development

Laboratory Division

1615 South Harrison Rd.

East Lansing, MI 48823-5224

New York Department of Agriculture 

 and Markets

Food Laboratory

1220 Washington Ave, Bldg. 6

Albany, NY 12226
Pesticide Data Program—Annual Summary, Calendar Year 2021

viii

Ohio Department of Agriculture

Consumer Protection Laboratory

8995 East Main St.

Reynoldsburg, OH 43068

Texas Department of Agriculture

Pesticide Laboratory

1500 Research Parkway, Ste. B100

College Station, TX 77845

United States Department of Agriculture

Agricultural Marketing Service

National Science Laboratories

801 Summit Crossing Pl.

Gastonia, NC 28054

Washington State Department of Agriculture

Chemical and Hop Laboratory

21 N. 1st Ave., Ste. 106

Yakima, WA 98902
Pesticide Data Program—Annual Summary, Calendar Year 2021

ix

Executive Summary

In 1991, the U.S. Department of Agriculture 

(USDA), Agricultural Marketing Service (AMS) 

was charged with designing and implementing the 

Pesticide Data Program (PDP) to collect data on 

pesticide residues in food, and Congress mandated 

the program in the 1996 Food Quality Protection 

Act (FQPA). PDP provides high-quality data on 

pesticide residues in food, particularly foods most 

likely consumed by infants and children. This 31st 

Pesticide Data Program summary presents results 

for samples collected in 2021.

Before a company can sell or distribute any pesticide 

in the United States, the Environmental Protection 

Agency (EPA) reviews studies on the pesticide to 

ensure that it will not pose unreasonable risks to 

human health or the environment, while considering 

the economic, social, and environmental costs and 

benefits of the use of any pesticide. Once EPA has 

made that determination, it will license or register 

that pesticide for use in strict accordance with label 

directions. Before allowing a pesticide to be used 

on a food commodity, EPA sets limits on how much 

of a pesticide may be used on food during growing, 

processing, and storage, and how much can remain 

on the food that reaches the consumer. In setting 

the tolerance, or maximum residue limit in food, 

EPA makes a safety finding that the pesticide can 

be used with a reasonable certainty of no harm by 

considering the toxicity of the pesticide, how much 

of the pesticide is applied and how often, how much 

of the pesticide remains in or on food by the time 

it is marketed and prepared, and all possible routes 

of exposure including use on crops, exposure from 

drinking water, and residential exposure. EPA also 

sets standards to protect workers from exposure to 

pesticides on the job.

PDP data are provided to EPA for its consideration 

in setting and reviewing tolerances. FDA monitors 

food in interstate commerce to ensure that these 

limits are not exceeded. 

AMS’s Monitoring Programs Division (MPD) is 

responsible for the administration, planning, and 

coordination of day-to-day PDP operations. MPD 

regularly engages with EPA and other Government 

agencies to establish program priorities and 

direction. In 2021, sampling and/or testing program 

operations were carried out with the support of 9 

States: California, Colorado, Florida, Maryland, 

Michigan, New York, Ohio, Texas, and Washington. 

These States had a prominent role in program 

planning and policy setting, particularly policies 

relating to quality assurance.

PDP commodity sampling is based on a rigorous 

statistical design that ensures the data are reliable for 

use in exposure assessments and can be used to draw 

various conclusions about the Nation’s food supply. 

The pesticides and commodities to be included each 

year in the sampling are selected based on EPA data 

needs, and the types and amounts of food consumed 

by infants and children are considered. The number 

of samples collected by each State is apportioned 

according to that State’s population. Samples are 

randomly chosen close to the time and point of 

consumption (i.e., distribution centers rather than at 

the farm gate) and reflect what is typically available 

to the consumer throughout the year. Samples are 

selected without regard to country of origin, variety, 

growing season, or organic labeling.

Fresh and processed fruit and vegetables accounted 

for 94 percent of the total 10,127 samples collected 

in 2021. Fresh and processed fruit and vegetables 

tested during 2021 were: blueberries (fresh and 

frozen), broccoli, cantaloupe, carrots, cauliflower, 

celery, eggplant, grape juice, green beans, peaches 

(fresh and frozen), pears, plums, summer squash, 

sweet bell peppers, tangerines, watermelon, and 

winter squash. Corn grain and butter were also tested 

during 2021, accounting for 4.1 and 1.7 percent of the 

samples collected in 2021, respectively. Domestic 

samples accounted for 67.8 percent of the samples, 

while 30.8 percent were imports, 0.9 percent were 

of mixed national origin, and 0.5 percent were of 

unknown origin. 

COVID-19-related closures disrupted PDP 

sampling in the early months of 2021, which may 

have impacted the seasonal observations within the 

data this year. Specific COVID-19-related sampling 

information can be found in Section II. Sampling 

Operations. COVID-19-related delays also occurred 

in PDP laboratory operations in 2021, and more 

details on the affected samples can be found in 

Section III. Laboratory Operations.
Pesticide Data Program—Annual Summary, Calendar Year 2021

x

Because PDP data are used for risk assessments, 

PDP laboratory methods are geared to detect very 

low levels of pesticide residues, even when those 

levels are well below the tolerances established by 

EPA. Prior to testing, PDP analysts washed samples 

for 15 to 20 seconds with gently running cold water 

as a consumer may do; no chemicals, soaps, or any 

special washes were used. 

This summary report includes the distribution of 

residues by pesticide. The full results for more 

than 2.7 million analyses, representing each 

pesticide monitored on each commodity, are too 

numerous to be included in their entirety in this 

summary. The complete PDP database file for 2021 

along with annual summaries and database files for 

previous years are available on the PDP website 

at http://www.ams.usda.gov/pdp or by contacting 

MPD at amsmpo.data@usda.gov. PDP data are 

also available using the PDP database search tool 

that can be accessed at: https://apps.ams.usda.gov/

pdp.

In 2021, over 99 percent of the samples tested had 

residues below the tolerances established by the 

EPA with 24.0 percent having no detectable residue. 

Appendixes B, C, and D provide a distribution of 

residues by pesticide for the commodities tested. 

Residues exceeding the tolerance were detected 

in 0.53 percent (54 samples) of the total samples 

tested (10,127 samples). Of these 54 samples, 29 

were domestic (53.7 percent), 24 were imported 

(44.4 percent), and 1 was of unknown origin (1.9 

percent). Residues with no established tolerance 

were found in 3.7 percent (374 samples) of the 

total samples tested (10,127 samples). Of these 

374 samples, 220 were domestic (58.8 percent), 

150 were imported (40.1 percent), and 4 were of 

unknown origin (1.1 percent).

PDP is a voluntary program and is not designed for 

enforcement of tolerances. However, PDP informs 

the U.S. Food and Drug Administration and EPA 

of presumptive tolerance violations if detected 

residues exceed the EPA tolerance or if residues are 

detected that have no EPA tolerance established.

PDP laboratories also test foods for low levels of 

environmental contaminants that are no longer 

used as pesticides in the United States, but due to 

their persistence in the environment, particularly 

in soil, can be taken up by plants. Results for 

environmental contaminants in all commodities 

are listed in Appendix E. More information on 

results is provided in Section V. Sample Results 

and Discussion.

In accordance with Federal civil rights law and U.S. Department of Agriculture (USDA) civil rights regulations and 

policies, the USDA, its Agencies, offices, and employees, and institutions participating in or administering USDA 

programs are prohibited from discriminating based on race, color, national origin, religion, sex, gender identity (including 

gender expression), sexual orientation, disability, age, marital status, family/parental status, income derived from a 

public assistance program, political beliefs, or reprisal or retaliation for prior civil rights activity, in any program or 

activity conducted or funded by USDA (not all bases apply to all programs). Remedies and complaint filing deadlines 

vary by program or incident.

Persons with disabilities who require alternative means of communication for program information (e.g., Braille, large 

print, audiotape, American Sign Language, etc.) should contact the responsible Agency or USDA’s TARGET Center at 

(202) 720-2600 (voice and TTY) or contact USDA through the Federal Relay Service at (800) 877-8339. Additionally, 

program information may be made available in languages other than English.

To file a program discrimination complaint, complete the USDA Program Discrimination Complaint Form, AD-3027, 

found online at How to File a Program Discrimination Complaint and at any USDA office or write a letter addressed to 

USDA and provide in the letter all of the information requested in the form. To request a copy of the complaint form, call 

(866) 632-9992. Submit your completed form or letter to USDA by: (1) mail: U.S. Department of Agriculture, Office of 

the Assistant Secretary for Civil Rights, 1400 Independence Avenue, SW, Washington, D.C. 20250-9410; (2) fax: (202) 

690-7442; or (3) email: program.intake@usda.gov.

USDA is an equal opportunity provider, employer, and lender.

Mention of a trade name or brand name does not constitute endorsement or recommendation by USDA over 

similar products or vendors.
Pesticide Data Program—Annual Summary, Calendar Year 2021

xi

Acronyms and Abbreviations

% C.V. Percent Coefficient of Variation

A2LA American Association for Laboratory Accreditation

AL Action Level

AMPA Aminomethylphosphonic Acid

AMS Agricultural Marketing Service

BQL Below Quantifiable Level

CFR Code of Federal Regulations

CSV Comma-Separated Values

EPA U.S. Environmental Protection Agency

e-SIF Electronic Sample Information Form

FAO Food and Agriculture Organizations of the United Nations

FAPAS Food Analysis Performance Assessment Scheme

FDA U.S. Food and Drug Administration

FGIS Federal Grain Inspection Service

FQPA Food Quality Protection Act

GEMS Global Environmental Monitoring Systems – Food Contamination Monitoring and 

 Assessment Programme

GC Gas Chromatography

HCB Hexachlorobenzene

ISO International Organization for Standardization

LC Liquid Chromatography

LOD Limit of Detection

LOQ Limit of Quantitation

MPD Monitoring Programs Division

MRL Maximum Residue Limit

MRM Multiresidue Method

MS Mass Spectrometry
Pesticide Data Program—Annual Summary, Calendar Year 2021

xii

NASS National Agricultural Statistics Service

NGS National Grain Center

NSL National Science Laboratories

PDP Pesticide Data Program

POP Persistent Organic Pollutants

PPS Probability proportionate-to-size

PT Proficiency Testing

PTV Presumptive Tolerance Violation

QA Quality Assurance

QAU Quality Assurance Unit

QuEChERS Quick, Easy, Cheap, Effective, Rugged and Safe

QC Quality Control

RDE Remote Data Entry

SIF Sample Information Form

SOP Standard Operating Procedure

SQL Structured Query Language

USDA United States Department of Agriculture

WHO World Health Organization
Pesticide Data Program—Annual Summary, Calendar Year 2021

1

Pesticide Data Program (PDP)

Annual Summary, Calendar Year 2021

This summary consists of the following sections: (I.) Introduction, (II.) Sampling Operations, 

(III.) Laboratory Operations, (IV.) Database Management, and (V.) Sample Results and Discussion

I. Introduction

The U.S. Department of Agriculture’s (USDA) 

Agricultural Marketing Service (AMS) initiated the 

Pesticide Data Program (PDP) in 1991 to collect 

data on pesticide residues in food, and the program 

now has an important role in the implementation 

of the 1996 Food Quality Protection Act (FQPA). 

The law directs the Secretary of Agriculture to 

collect pesticide residue data on commodities most 

frequently consumed by infants and children. PDP 

data are used primarily by the U.S. Environmental 

Protection Agency (EPA) to assess dietary exposure 

during the review of the safety of existing pesticide 

tolerances (also referred to as maximum residue 

limits in other countries). EPA establishes the 

tolerances after developing a risk assessment that 

considers the following: the pesticide exposure 

through diet and drinking water and from uses in and 

around the home; the cumulative exposure to two or 

more pesticides that cause a common toxic effect; 

the possibility of increased susceptibility to infants 

and children or other sensitive populations from 

exposure to the pesticide; and the possibility that the 

pesticide produces an effect in people similar to an 

effect produced by a naturally occurring estrogen or 

produces other endocrine disruption. PDP data also 

are used by the U.S. Food and Drug Administration 

(FDA) to assist in planning commodity surveys for 

pesticide residues as a part of its enforcement and 

regulatory programs.

Because PDP collects data on food commodities 

primarily for consumer exposure assessment, 

program operations differ markedly from those 

followed by regulatory monitoring programs for 

tolerance enforcement. Commodities chosen for 

inclusion in the program are based on EPA data 

needs. PDP samples are collected closer to the 

point of consumption and are prepared emulating 

consumer practices (e.g., washing, peeling). PDP 

sampling does not impede commodity distribution. 

Laboratory operations are designed to achieve 

detection of low levels rather than quick sample 

turnaround. As PDP data are used in dietary risk 

assessment, the program prioritizes testing for 

pesticides with registered uses for the commodities 

in the program, as well as for pesticides that may 

not have U.S. tolerances but are used in other 

countries on commodities that are imported to the 

United States.

Primary contributors to PDP’s policy development 

and planning of operations include the participating 

States, other government agencies, and program 

stakeholders (Figure 1(a)), while primary data 

users include EPA, FDA, and a wide range of other 

agencies and groups (Figure 1(b)). Federal, State, 

and foreign government agencies and industries 

have used PDP data to promote the export of 

U.S. commodities to international markets. 

Additionally, PDP methodologies are consistent 

with international guidelines that have been adopted 

by the Codex Committee on Pesticide Residues 

for good laboratory practices (CAC/GL 40-1993), 

performance criteria for methods of analysis 

(CXG 90-2017), and use of mass spectrometry 

(CAC/GL 56-2005). PDP monitoring data are also 

incorporated into the World Health Organization’s 

(WHO) Global Environment Monitoring System - 

Food Contamination Monitoring and Assessment 

Programme (GEMS/Food), a data platform used 

by the Joint Food and Agriculture Organization 

of the United Nations (FAO)/WHO Meeting on 

Pesticide Residues to evaluate dietary exposure 

and recommend the establishment of pesticide 

maximum residue limits (MRLs) to the Codex 

Committee on Pesticide Residues.

In 2021, sampling services were provided by nine 

States (California, Colorado, Florida, Maryland, 

Michigan, New York, Ohio, Texas, and Washington; 

see Figure 2). Laboratory services were provided 

by the States of California, Florida, Michigan, New 

York, Ohio, Texas, and Washington, along with 

the USDA National Science Laboratories (NSL). 

Together, these States represent nearly 50 percent 

of the Nation’s population and all four census 

regions of the United States. They also represent 

major U.S. producers of fruit and vegetables.
Pesticide Data Program—Annual Summary, Calendar Year 2021

2

Figure 1. Pesticide Data Program (PDP) Program Operations Support and Data Users. This figure illustrates (a) 

agencies/groups that support PDP program policy and planning activities and (b) agencies/groups that use PDP data. 

Program Operations

Participating 

States

National

Agricultural Statistics 

Service

Industry and

Grower Groups

Environmental

Protection

Agency

(a) PDP Policy and Planning Contributors

Data

Food and Drug 

Administration Environmental 

Protection Agency

Academic 

Institutions

Agricultural 

Industry

Foreign 

Agricultural 

Service

Economic 

Research 

Service

Chemical 

Manufacturers, 

Environmental 

Interest Groups, Food 

Safety Organizations

Other 

Government 

Agencies

Participating 

States

(b) PDP Data Users

Food and Drug 

Administration
Pesticide Data Program—Annual Summary, Calendar Year 2021

3

The AMS Monitoring Programs Division (MPD) 

is responsible for overall management of PDP, 

including cooperative agreements with the States, 

sampling and laboratory testing approaches, 

and data management and analysis. Each year, 

MPD works closely with EPA and FDA to select 

commodities and pesticides for testing; both 

commodities and pesticides are prioritized by PDP 

based on EPA and/or FDA data needs. Typically, 

the selected commodities represent the highest 

U.S. consumption rates, with an emphasis on foods 

consumed by infants and children. Due to budget 

limitations, the high consumption commodities 

are cycled through the program approximately 

1 The U.S. National Residue Program (NRP) administered by the U.S. Department of Agriculture’s (USDA), Food Safety and 

Inspection Service (FSIS) monitors pesticide residues for meat, poultry, and egg products.

every 5 years rather than tested continuously. 

Specialized commodities (e.g., fresh herbs) are 

added to the rotation as data are needed. Fresh fruit 

and vegetable commodities remain in the program 

for 2 years to consider two full growing seasons, 

thereby capturing any changes due to seasonality or 

year-to-year variations. Processed products, as well 

as dairy, fish, and grains, are typically tested for 1 

full year. All commodity rotations are provided in 

the PDP Program Plans prior to the start of sampling 

and are shown in Table 1 for 2021. A total of 127 

commodities have been tested by PDP from the 

beginning of the program (in 1991) through 2022 

(Appendix A).1

Washington

California

Colorado

Texas

Ohio

New York

Florida

Maryland

Michigan

Participating State

Location of Participating State Laboratories

North Carolina

Figure 2. Program Participants. During 2021, USDA’s Agricultural Marketing Service established cooperative agreements 

with nine States to sample and/or test Pesticide Data Program commodities. Together, these States represent about 50 percent 

of the Nation’s population and all four census regions of the United States. These States are the major U.S. producers of fruit 

and vegetables. State laboratories were responsible for analyzing fresh and processed fruit and vegetable samples. The National 

Science Laboratory in Gastonia, NC, was responsible for anylyzing field corn grain.

Location of Participating Federal Laboratory
Pesticide Data Program—Annual Summary, Calendar Year 2021

4

Fruit and vegetable samples are collected at terminal 

markets2 and distribution centers from which 

food commodities are supplied to supermarkets 

and grocery stores. Sampling at these locations 

allows for residue measurements that include 

pesticides applied during crop production and those 

applied after harvest (such as fungicides, growth 

regulators, and sprouting inhibitors) and considers 

residue degradation while food commodities are 

in storage. Participation as a PDP sampling site 

is voluntary, which sets it apart from State and 

Federal enforcement programs. In 2021, 487 sites 

granted access and provided information, including 

site volume data, to sample collectors. Voluntary 

cooperation is important to PDP and makes it 

possible to adjust sampling protocols in response to 

fluctuations in food distribution and production.

Pesticides prioritized for screening by PDP include 

those with current registered uses for the commodity 

being tested and compounds for which toxicity 

data and preliminary estimates of dietary exposure 

indicate the need for more extensive/updated 

residue data. PDP may also monitor pesticides 

for which EPA has modified use directions (i.e., 

reduced application rates or frequency) as part of 

risk management activities. In addition, PDP tests 

for selected pesticides that may not have U.S. 

tolerances but are used in other countries that export 

commodities to the United States. Appendixes B, 

C, and D list the specific pesticides tested in the 

fruit and vegetable, corn grain, and butter samples, 

respectively. Environmental contaminants, or 

pesticides whose uses have been canceled in the 

United States, but their residues persist in the 

environment, are consolidated into Appendix E, 

which summarizes findings for these chemicals 

across all commodities.

II. Sampling Operations

A. Conceptual Framework

The goal of the PDP sampling program is to obtain 

a statistically valid representation of the U.S. food 

supply. PDP data reflect actual pesticide residue 

exposure from food. Using a rigorous statistical 

design, PDP has developed extensive procedures 

that ensure samples are randomly selected from the 

national food distribution system and reflect what is 

typically available to the consumer.

Nine States currently participate in PDP – 

California, Colorado, Florida, Maryland, Michigan, 

New York, Ohio, Texas, and Washington. The initial 

participating States in 1991 (California, Florida, 

Michigan, New York, Texas, and Washington) were 

selected based on agricultural production, analytical 

capabilities, population, and regional/geographic 

distribution – all four U.S. Census Regions (West, 

South, Midwest, and Northeast) were represented. 

Later, in 1993, Colorado joined to represent the 

Mountain Division of the Western Region and Ohio 

to further represent the densely populated East 

North Central Division of the Midwest Region. 

Maryland was added in 1997 to represent the South 

Atlantic Division of the Southern Region. Today, 

these States together represent about 50 percent of 

the Nation’s population and all four census regions 

of the United States.

Commodities chosen for inclusion in the program 

are based on EPA data needs. Foods selected for 

testing are high-consumption items with a strong 

focus on the foods that compose the diets of infants 

and children. Each fresh commodity is sampled and 

tested for 2 years in order to capture annual and 

seasonal variability. High-consumption items are 

rotated in and out of the program every 5 years; for 

example, apples, lettuce, and oranges are retested 

and the data refreshed every 5 years.

PDP collects a minimum of 600 samples per 

commodity per year in order to provide an accurate 

statistical representation for a given commodity. 

PDP collects additional samples to allow 

apportionment among the participating States over 

a 12-month period and to allow for a small sample 

overage for any missed, damaged, or unusable 

samples. Participating State population figures are 

used to apportion the number of samples scheduled 

for collection by each State (for more detail, see 

the 2021 Sampling Operations later in this section). 

PDP sampling operations may be adjusted according 

2 Terminal markets are facilities where wholesalers receive large quantities of fresh fruit and vegetables by rail, truck, and air 

from around the world for sale to grocers, restaurants, institutions, and other businesses. Terminal markets are often located in 

metropolitan areas at or near major transportation hubs.
Pesticide Data Program—Annual Summary, Calendar Year 2021

5

to product availability. For example, plums, 

tangerines, and peaches may be oversampled 

during the summer months to make up for low 

availability during winter months. In some cases, 

frozen product is allowed as an alternative to fresh 

(e.g., peaches).

PDP samples are collected at terminal markets 

and warehouse distribution centers, close to 

the point of consumption. Participating State 

agencies compile and maintain lists of these 

sampling sites. In 2021, 487 sites granted access 

to sample collectors. The States provide AMS 

and the USDA, National Agricultural Statistics 

Service (NASS) with annual volume information 

for commodities distributed at these sites. Based 

on this information, sites are assigned volume 

indicators compared to other sites in the same 

State. This volume indicator is used to ensure 

larger sites are selected more frequently than 

smaller sites. This information is used to weigh 

the site to determine the probability for sample 

selection. For example, a weight of 10 may be 

given to a site that distributes 100,000 pounds of 

produce annually and a weight of 1 is given to a site 

that distributes 10,000 pounds. This site selection 

method, termed probability-proportionate-to-size 

(PPS), then results in the larger site being 10 times 

more likely to be selected for sampling than the 

smaller site.

Each participating State works with NASS to 

develop statistical procedures for site weighting 

and selection. States are also given the option to 

have NASS perform their quarterly site selection. 

The number of sampling sites and the volume 

of produce distributed by the sites vary greatly 

among States. Sampling plans that include 

sampling dates, sites (primary and alternate), 

targeted commodities, and testing laboratories 

are prepared by each State on a quarterly basis. 

Collection of commodities is randomly assigned 

to weeks of the month, prior to selection of specific 

sampling dates within a week. Because sampling 

sites are selected for an entire quarter, States 

may assign the sites to particular months based 

on geographic location. Sample information is 

captured at the time of collection for inclusion in 

the PDP database. 

B. Sampling Procedures

While obtaining PDP samples, collectors randomly 

select the scheduled commodities. Collectors 

use established procedures to prevent crosscontamination and maintain chain-of-custody. PDP 

State sample collectors are trained to adhere to 

detailed program Standard Operating Procedures 

(SOPs) that provide criteria for site selection and 

specific instructions for sample selection, shipping 

and handling, and chain-of-custody. SOPs are 

updated as needed and serve as a technical 

reference in conducting program sampling reviews 

to ensure program goals and objectives are met. 

PDP sampling SOPs are available on the website: 

www.ams.usda.gov/datasets/pdp/pdp-standardoperating-procedures. On a quarterly basis, sample 

collectors are provided with Commodity Fact 

Sheets that list specific collection details for the 

individual commodities in the program.

Temperature-sensitive samples are packed in 

heavy-duty, temperature-controlled containers for 

shipment to the laboratory. Holding temperatures 

are preserved throughout transit time with the 

inclusion of ample frozen cold packs and insulating 

materials. Non-temperature-sensitive samples do 

not require temperature-controlled containers; 

however, they are shipped in heavy-duty, wellcushioned containers. To preserve sample integrity, 

most samples are shipped the same day by overnight 

delivery. Non-refrigerated processed commodities 

such as grape juice are often shipped by ground 

transportation to reduce shipping costs. Corn grain 

samples are collected in pesticide-free polyethylene 

bags and shipped in canvas pouches or boxes by 

ground transportation to the laboratory where the 

samples are refrigerated pending analysis.

Electronic Sample Information Forms (e-SIFs) 

are used for chain-of-custody and to capture 

information needed to characterize the sample. 

Sample collectors use tablets or laptop computers in 

the field to record sample identification information 

such as: (1) State of sample collection, (2) collection 

date, (3) sampling site code, (4) commodity code, 

and (5) testing laboratory code. Information from 

these five data elements is combined to form a 

unique PDP identification number for each sample.
Pesticide Data Program—Annual Summary, Calendar Year 2021

6

Other available information about each sample is 

also recorded, such as collector name; the country 

of origin; product variety; production claims such 

as organic; expiration date; and grower, packer, 

and/or distributor locations. The e-SIFs are sent 

electronically the same day as sample collection or, 

at the latest, by the next morning after collection to 

ensure that sample information is received at each 

laboratory by the time samples arrive for analysis. 

Refer to Section IV on Database Management for 

more information on the e-SIF system.

Because most PDP samples are collected at 

distribution centers, terminal markets, and other 

wholesalers, entire cases must be obtained while 

a significantly smaller portion is sent to the 

laboratory for testing. For example, if a 20-pound 

case of apples is collected and a 5-pound sample 

is sent for testing, the remaining 15 pounds are 

typically donated. In most cases, the excess 

samples are donated to organizations such as 

local food banks, shelters, senior assisted living 

centers, churches, and other charities. PDP often 

provides the only fresh commodity donations 

available to these organizations. In 2021, PDP 

State participants donated over 50,000 pounds of 

food to local charities. 

C. 2021 Sampling Operations

The number of fruit, vegetable, and dairy samples 

collected in each participating State is determined 

by State population. The monthly collection 

schedule for all 2021 commodities is shown in 

Table 1; however, not all samples scheduled were 

collected due to the Coronavirus COVID-19 

pandemic. California suspended sample collection 

in December 2020 and the State did not collect 

its 14 samples for any commodities for January 

and February 2021. California resumed partial 

sample collection on March 8 and collected all 

scheduled samples for 10 commodities that month. 

Commodity Jan-Mar Apr-Jun Jul-Sep Oct-Dec End Date

Blueberries Sep-22

Blueberries, Frozen Sep-22

Broccoli Dec-21

Butter Sep-22

Cantaloupe Jun-21

Carrots Mar-22

Cauliflower Sep-21

Celery Jun-23

Corn Grain Jun-22

Eggplant Dec-21

Grape Juice Dec-21

Green Beans Sep-22

Peaches Dec-22

Peaches, Frozen Dec-22

Pears Dec-22

Plums Jun-23

Summer Squash Sep-22

Sweet Bell Peppers Jun-21

Tangerines Sep-21

Watermelon Sep-23

Winter Squash Dec-21

Table 1. Pesticide Data Program (PDP) Commodity Collection Schedule for 2021. Samples are most often 

collected for a 2-year time period. Commodities are initiated or terminated in different quarters of the year so 

that new commodities are not brought into the program all at the same time. This table illustrates time ranges 

for the listed commodities. See Appendix A for the complete PDP commodity history (May 1991 through 

December 2022). 
Pesticide Data Program—Annual Summary, Calendar Year 2021

7

However, sample collection of peaches, pears, 

tangerines, and winter squash did not resume 

until April. California started collecting make-up 

samples in July. Make-up samples of cantaloupe 

and sweet bell peppers were not collected, as those 

commodities rotated out of the program before the 

make-up sampling began in July. While yearly 

minimum sample targets were met (minimum 600 

samples per commodity), results could potentially 

have been impacted by interruptions to the 2021 

sampling schedule. 

The total number of samples collected in each State 

for each commodity is listed in Table 2. Table 3 

lists the acceptable product types for each collected 

commodity as seen on Commodity Fact Sheets 

provided to sample collectors. For all commodities, 

domestic or imported and organically grown or 

conventionally grown products are acceptable. In 

2021, excluding corn grain, 6.6 percent of the tested 

samples were organic (643 of 9,709); summaries 

of findings by claim may be found by using the 

online PDP Database search tool at https://apps.

ams.usda.gov/pdp.

State population figures are used to assign the 

number of fruit, vegetable, and dairy samples 

scheduled for collection each month. During 

2021, the monthly number of samples assigned for 

each State included: California, 13; Colorado, 2; 

Florida, 7; Maryland, 4; Michigan, 6; New York, 

9; Ohio, 6; Texas, 8; and Washington, 4. This 

schedule resulted in a monthly target of 59 samples 

per commodity or 708 samples per commodity per 

year.

In 2021, fruit, vegetable, and dairy samples were 

randomly collected by trained State inspectors at 

terminal markets and large chain store distribution 

centers throughout the country. Surrogate or 

“proxy” sites (retail markets) are used to collect 

these samples when the commodity of interest is 

unavailable at a terminal market or distribution 

center. In these instances, the commodity is selected 

in the rear storage area of the retail facility to 

eliminate possible contamination by the consumer 

and to allow capture of sample information from 

product boxes. In 2021, 30.9 percent of fresh and 

processed samples were collected at proxy sites. 

The commodities most often collected at these 

facilities were frozen peaches, grape juice, and 

butter. 

Corn grain samples were collected at random from 

trucks, hopper cars, and barges by trained USDA 

Federal Grain Inspection Service (FGIS) inspectors.

The total number of samples per commodity and 

the percentage of each that were either domestic, 

imported, or of unknown origin are shown in Figure 

3. The origin of some fresh commodities can vary

greatly throughout the year. A graphic example

of this variation can be found in Figure 4, where

differences in origin (domestic versus import) are

depicted by month for blueberries, eggplant, and

winter squash samples.

Fresh and processed fruit, vegetable, and dairy 

samples originated from 42 States and 26 foreign 

countries (refer to Appendix F). Corn grain samples 

are excluded from Appendix F because this 

commodity relies on a different sampling frame.

D. Fresh and Processed Commodities

Of all samples collected and analyzed in 2021, 94 

percent (9,532 of 10,127) were fruit and vegetables, 

including fresh and processed products. The fresh 

commodities collected for PDP were blueberries, 

broccoli, cantaloupe, carrots, cauliflower, celery, 

eggplant, green beans, peaches, pears, plums, 

summer squash, sweet bell peppers, tangerines 

(mandarins), watermelon, and winter squash. The 

processed commodities included frozen blueberries, 

grape juice, and frozen peaches. 

Fresh and frozen fruit and vegetable samples 

weighed either 3 or 5 pounds, except for blueberries 

where the sample size was 1 pound. Three pounds 

were collected for smaller, low-weight commodities 

such as green beans and tangerines (mandarins), 

and 5 pounds were collected for larger, high-weight 

commodities such as broccoli and watermelon. For 

processed commodities, a sample size of 1 quart (32 

ounces) was collected for grape juice.

E. Corn Grain

In 2021, trained FGIS inspectors collected 418 corn 

grain samples for PDP. Samples were drawn from 
Pesticide Data Program—Annual Summary, Calendar Year 2021

8

State BB BR CE CF CN CR EP GB PC PE PP PU SS TA WM WS

Total 

Fresh

California 148 156 78 117 52 156 156 156 113 156 52 60 154 116 39 156 1,865

Colorado 22 24 12 18 12 24 23 24 15 24 12 10 24 18 6 24 292

Florida 83 84 42 63 42 84 84 83 66 84 42 36 83 64 21 84 1,045

Maryland 48 48 24 36 24 48 48 48 40 48 24 22 47 36 12 48 601

Michigan 70 72 36 54 36 72 72 66 43 72 36 26 66 54 18 72 865

New York 106 108 54 81 54 108 108 109 90 108 54 44 110 81 26 108 1,349

Ohio 72 72 36 54 36 72 72 72 55 72 36 26 72 54 18 71 890

Texas 95 96 48 72 48 96 93 96 71 95 48 35 96 72 24 95 1,180

Washington 48 48 24 36 24 48 47 46 25 48 24 18 46 36 11 48 577

TOTAL 692 708 354 531 328 708 703 700 518 707 328 277 698 531 175 706 8,664

State BZ GJ HZ

Total 

Processed

Total 

Fresh & 

Proccessed 

F&V

California 8 156 42 206 2,071

Colorado 24 8 32 324

Florida 1 83 18 102 1,147

Maryland 50 3 53 654

Michigan 2 66 29 97 962

New York 2 108 18 128 1,477

Ohio 72 17 89 979

Texas 1 96 7 104 1,284

Washington 45 12 57 634

TOTAL 14 700 54 868 9,532

Table 2. Distribution of Samples Collected by Each Participating State. This table includes those 

commodities collected at terminal markets, distribution centers, and retail markets. 

Commodity Legend

BB = Blueberries, Fresh GJ = Grape Juice

BR = Broccoli HZ = Peaches, Frozen

BU = Butter PC = Peaches, Fresh

BZ = Blueberries, Frozen PE = Pears

CE = Celery PP = Sweet Bell Peppers

CF = Cauliflower PU = Plums

CN = Cantaloupe SS = Summer Squash

CR = Carrots TA = Tangerines

EP = Eggplant WM = Watermelon

GB = Green Beans WS = Winter Squash

BU

39

6

21

12

18

27

18

24

12

177

Dairy
Pesticide Data Program—Annual Summary, Calendar Year 2021

9

Commodity Acceptable Products

Blueberries Any fresh, whole blueberry; cultivated (Highbush) or wild (Lowbush). Fresh are 

preferred, but frozen are acceptable.

Blueberries, Frozen Frozen blueberries; cultivated (Highbush) or wild (Lowbush). Individually 

quick frozen (IQF) or frozen in own juices. Fresh are preferred, but frozen are 

acceptable.

Broccoli Fresh broccoli. Broccoli crowns (bunch with top florets plus a little of the stem) 

are preferred. Broccoli with stems (bunch with top florets plus a lot of the stem) 

is acceptable if broccoli crowns are not available.

Butter Salted or unsalted sweet butter in cubes or sticks.

Cantaloupe Whole, fresh cantaloupe.

Carrots Fresh, whole carrots, with or without tops.

Cauliflower Any fresh whole cauliflower. White in color.

Celery Fresh, whole celery.

Corn Grain Corn grain from domestic lots representing trucks, hopper cars, and barges.

Eggplant Whole, fresh eggplant. Traditional types that are oval or pear in shape with a 

black, purplish-black, or purple skin color.

Grape Juice 100% Grape juice. Concord, red, or white grape juice. Domestic or import. 

Added nutritional ingredients such as citric acid and ascorbic acid. Organic or 

conventional. Ready-to-serve (RTS). Single strength (grape juice may have been 

reconstituted from concentrate). Shelf-stable or refrigerated. Individual singleserving boxes with the same lot number.

Green Beans Fresh green string beans. Whole or pre-cut.

Peaches Fresh whole peaches. Red or white. Clingstone, freestone, or semi-freestone. 

Attempt to select peaches that are not overly ripe or soft to the touch.

Peaches, Frozen Frozen peaches; whole, halved, sliced, or cut. Fresh are preferred, but frozen 

are acceptable when fresh are unavailable.

Pears Fresh whole pears.

Plums Fresh whole plums. Any color is acceptable. Hybrids of plums with apricots, 

such as plumcots, pluots, or dinosaur eggs (this includes interspecific plums with 

a PLU of 3278).

Summer Squash Fresh whole zucchini, yellow squash, or crookneck squash.

Sweet Bell Peppers Whole, fresh bell peppers. Colors may include, but are not limited to: green, 

orange, purple, red, or yellow.

Tangerines Any fresh, whole tangerine (mandarin or mandarin orange). Clementine, 

Minneola, Mediterranean mandarin, Satsuma mandarin, or tangelo.

Watermelon Fresh whole watermelon, including seeded and seedless varieties. Watermelon 

cut into halves or quarters or sliced watermelon with rind ONLY if whole is not 

available.

Winter Squash Whole winter squash varieties include but are not limited to: Acorn, banana, 

Boston marrow, buttercup, butternut, Hubbard, kabocha, and spaghetti.

Table 3. Acceptable Products for Collected Commodities. This table lists the acceptable products for 

each collected commodity as seen on the Commodity Fact Sheets provided to sample collectors. For all 

commodities, domestic or imported and organically grown or conventionally grown products are acceptable.
Pesticide Data Program—Annual Summary, Calendar Year 2021

10

A. Fresh Fruit and Vegetable Samples

Carrots (708 Samples)

Eggplant (703 Samples) Peaches (518 Samples)

Summer Squash (698 Samples)

Cauliflower (531 Samples) Celery (354 Samples)

Blueberries (692 Samples) Cantaloupe (328 Samples)

Domestic 55.9%

Domestic 95.5%

Import 29.9%

Import 43.1%

Import 62.3%

Import 4.2%

Unknown 0.3%

Domestic 69.3% Domestic 71.2%

Import 4.0%

Unknown 0.8%

Domestic 95.5%

Plums (277 Samples)

Import 74.7%

Domestic 100%

Pears (707 Samples)

Broccoli (708 Samples)

Domestic 80.5%

Domestic 25.3%

Unknown 1.0%

Import 28.6%

Unknown 0.2%

Import 19.2%

Domestic 82.1%

Import 17.8%

Domestic 75.4%

Unknown 0.1%

Import 24.5%

Green Beans (700 Samples)

Domestic 54.0%

Import 44.7%

Unknown 1.3%

Domestic 37.7%

Unknown 0.1%

Unknown 0.5%

Unknown 0.3%
Pesticide Data Program—Annual Summary, Calendar Year 2021

11

Sweet Bell Peppers (328 Samples)

Figure 3. Commodity Origin. This figure depicts the proportion of commodity origin (domestic, import, unknown, 

and mixed national origin) for each fresh and processed fruit and vegetable product tested in 2021.

Tangerines (531 Samples)

Domestic 61.0%

Import 39.0%

Domestic 36.9%

Import 63.1%

Grape Juice (700 Samples)

Domestic 78.9%

Blueberries, Frozen (14 Samples)

Import 6.1%

Peaches, Frozen (154 Samples)

Domestic 21.4%

Import 78.6%

Domestic 83.1%

Unknown 1.7%

B. Processed Fruit and Vegetable Commodities

Winter Squash (706 Samples)

Domestic 44.0%

Import 55.4%

Watermelon (175 Samples)

Domestic 40%

Import 60.0%

Import 16.9%

Mixed National 13.3%

Unknown 0.6%

trucks (0.7 percent of samples), hopper cars (98.3 

percent of samples), and barges (1.0 percent of 

samples). Corn grain slated for export was excluded 

from the sampling scheme. Sample information 

for corn included: Quality Assurance and Control 

System number, official agency collecting the 

sample, agency inspector, State of origin where 

the grain was grown, inspection point code, grain 

location city and State, variety, carrier type (truck, 

hopper car, or barge), carrier identification code, 

collection date, and shipment date. Field offices/

official agencies shipped corn grain samples to 

the National Grain Center (NGC) in Kansas City, 

MO, following FGIS chain of custody procedures. 

Truck, hopper car, and barge samples were held for 

up to 7, 10, and 30 days, respectively, prior to being 

released to PDP. Truck and hopper car samples 

were stored at room temperature prior to being 

shipped; barged samples were stored refrigerated. 

Samples selected for shipment to PDP were based 

on random selection. The sample size for corn 

grain was 500 grams. Pesticide residue analysis 
Pesticide Data Program—Annual Summary, Calendar Year 2021

12

Figure 4. Origin of Selected Fresh Commodity: Blueberry, Eggplant and Winter Squash Samples. 

Differences in origin (domestic vs. import) are illustrated by month. 

Domestic Imported Unknown

Origin of Blueberry Samples

JAN

FEB

MAR

APR

MAY

JUN

AUG

SEP

OCT

NOV

DEC

Number of Samples

Origin of Eggplant Samples

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

Number of Samples

JUL

Origin of Winter Squash Samples

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

Number of Samples
Pesticide Data Program—Annual Summary, Calendar Year 2021

13

was performed by the USDA National Science 

Laboratory (NSL) located in Gastonia, North 

Carolina. Corn samples were grown in 17 States. 

There were no imported corn samples; all were of 

domestic origin. The origin and number of samples 

grown in each State are displayed in Figure 5. 

F. Butter

In 2021, PDP collected and analyzed 177 butter 

samples. Samples were collected from routine PDP 

sampling sites, which included major distribution 

centers and terminal markets, as well as proxy sites. 

The sample size for butter was 1 pound. Analysis 

was performed by the New York laboratory. 

G. Sampling Limitations 

Nine States from all four census regions of the 

United States participate in PDP. The States that 

participate account for about 50 percent of the U.S. 

population and the major agricultural production 

areas of the country, making them generally 

representative of the United States as a whole.

PDP collects samples from 487 distribution centers, 

terminal markets, and wholesale/retail markets 

within the participating States. The total number 

of distribution centers, terminal markets, and 

wholesale/retail markets within the participating 

States is difficult to establish since existing sites 

may go out of business or merge and new sites 

may open during the year. However, there is no 

evidence to believe that sites within the States 

that participate differ significantly from those that 

do not participate. Since these sites are similar 

throughout the State, they are representative of all 

sites in the State.

Sometimes it is necessary to replace the site that 

was originally selected using PPS. In those cases, 

an alternate site of similar size is selected from 

Michigan

Idaho

North

Dakota

South

Dakota

Minnesota

Texas

Kansas

Nebraska Iowa

Missouri

Tennessee

Illinois

Kentucky

Ohio

Wisconsin

Indiana

Mississippi

2

2

14

61

71 28

53

1

28

1

16

21

57

16

30

1

16

Figure 5. Location of Corn Grain Samples by Grower State. A total of 418 corn grain sample were collected in 2021. The samples originated from 17 States. Residue testing for all samples was performed by the USDA laboratory located in Gastonia, NC.
Pesticide Data Program—Annual Summary, Calendar Year 2021

14

the quarterly site list by the State personnel to 

replace the original site. Whenever possible, a site 

of similar size in the same region as the original 

site is chosen as the replacement. Additionally, 

the availability of a specific commodity may 

necessitate a change in site selection. For example, 

cantaloupe may be collected from an alternate site 

if the primary site is out of stock.

III. Laboratory Operations

A. Overview

Seven State laboratories and one Federal laboratory 

performed analyses for PDP. These laboratories 

are equipped with instrumentation capable of 

detecting residues at very low levels. Laboratory 

staff members receive intensive training and 

must demonstrate analytical proficiency on an 

ongoing basis. Laboratory scientists continually 

test new technologies and develop new techniques 

to improve the levels of detection. Any major 

change in methodology and/or instrumentation 

is evaluated, and its soundness demonstrated 

and documented by means of method validation 

modules in accordance with PDP SOPs.

B. Fresh and Processed Commodities

A total of 9,532 fresh and processed fruit and 

vegetable samples were tested for 577 parent 

pesticides, metabolites, degradates, and/or isomers, 

plus 21 environmental contaminants using MultiResidue Methods (MRMs). Pesticides prioritized 

for screening by PDP include those with current 

registered uses for the commodity being tested and 

compounds for which toxicity data and preliminary 

estimates of dietary exposure indicate the need for 

more extensive residue data.

Upon arrival at the testing facility, samples of 

fresh commodities were visually examined for 

acceptability and discarded if determined to be 

inedible (decayed, extensively bruised, or spoiled). 

Laboratories are permitted to refrigerate incoming 

fresh fruit and vegetable samples of the same 

commodity up to 72 hours to allow for different 

sample arrival times from collection sites. Frozen 

and canned commodities may be held in storage 

(freezer or shelf) until the entire sample set is 

ready for analysis.

COVID-19 prevention measures and other factors 

resulted in laboratory delays during 2021 and 684 

fresh commodity samples were held frozen for 

more than 90 days before analysis, (93-222 days). 

Per PDP SOP, sample results are transmitted by 

the laboratories no more than 90 days from the 

date of receipt of samples. The data from the 684 

samples, consisting of 295 fresh and 143 frozen 

peaches, 196 celery, and 50 sweet bell peppers, 

have been annotated with a special extraction 

code in the downloadable/searchable PDP data 

set for 2021.

Each sample is prepared according to the 

procedures detailed in Table 4, which lists the 

steps for preparing each commodity for analysis as 

defined in the PDP Laboratory Sample Processing 

and Analysis SOP. For all commodities, the 

sample is chopped, mixed, or blended until a 

visually homogeneous mixture is attained.

Samples are separated into analytical portions 

(aliquots) for analysis. If testing cannot be 

performed immediately, the entire analytical set 

is frozen at -40°C or lower according to PDP’s 

Quality Assurance/Quality Control (QA/QC) 

requirements. Surplus aliquots not used for the 

initial testing are retained frozen if replication of 

analysis or verification testing is required.

For analysis of fruit and vegetable samples, testing 

laboratories use various Quick, Easy, Cheap, 

Effective, Rugged and Safe (QuEChERS)-based 

approaches.3 All MRMs are determined, prior to 

use and through appropriate method validation 

procedures, to produce equivalent data for PDP 

analytical purposes. PDP laboratories use gas 

chromatography (GC) and liquid chromatography 

(LC) instrumentation, coupled with tandem 

mass spectrometry (MS) detection systems for 

the simultaneous identification/confirmation 

and quantitation of pesticides. The GC-MS/MS 

and LC- MS/MS systems allow the program to 

capture data for a broad spectrum of pesticides, 

including emerging product chemistries.

3

 M. Anastassiades, S.J. Lehotay, D. Stajnbaher and F.J. Schenck, “Quick, Easy, Cheap, Effective, Rugged and Safe 

(QuEChERS) Method,” J AOAC Int 86 (2003) 412.
Pesticide Data Program—Annual Summary, Calendar Year 2021

15

Table 4. Sample Preparation Steps for Analysis. This table lists the steps for preparing each collected commodity for 

analysis as defined in the Laboratory Standard Operating Procedure. The wash and drain steps refer to a wash under cold 

running water for approximately 15-20 seconds to assure that all surfaces are rinsed, then a drain for at least 2 minutes. 

For all commodities, the sample is chopped, mixed, or blended until a visually homogeneous mixture is attained.

Commodity Sample Preparation Steps

Blueberries Wash blueberries by the handful or by using a colander and drain. 

Blueberries, Frozen The samples may be chopped while frozen, or to prevent damage to the chopper/homogenizer blades, 

the sample may be thawed in a refrigerator or in a room temperature water bath. Open the containers 

and pour the entire contents into the chopper/homogenizer. 

Broccoli Visually examine and discard any damaged portion or wilted florets. Do not discard leaves unless they 

are wilted. Trim away inedible portions of stems. If the stem is less than 3 inches, do not trim. If the 

stem is longer than 3 inches, thinly slice away the tough outer layer on the stalk. Wash and drain.

Butter If the sample is comprised of a single container, simply weigh appropriate analytical portion. If the 

sample is comprised of multiple containers, combine and mix enough containers to achieve the target 

sampling size (1 pound) and weigh appropriate analytical portion.

Cantaloupe Cut each cantaloupe in half and remove seeds and rind. Halves may be further divided at this point to 

facilitate removal of the rind.

Carrots If carrots have any visible dirt, hold each carrot under cold running tap water and gently scrub the entire 

surface with a clean vegetable brush to remove any loose soil and grit. Rinse and drain. With a clean, 

dry knife, remove stem cap portion from each carrot.

Cauliflower Visually examine the head and remove wrapper leaves and any damaged portions. Rinse, turn the 

head top side down to drain.

Celery Using a clean, dry knife, remove the inedible portion of the stalk (i.e., the woody part at the base of the 

stalk) to allow the stems to separate. Do not remove the leaves unless discolored or damaged. Wash 

and drain.

Corn Grain Pour entire grain sample into a container and mixed thoroughly to obtain a 500- gram sub-sample for 

homogenization. Grind the 500- gram subsample using an appropriate device. Tumble the resulting 

powder homogenate to obtain a homogeneous mixture.

Eggplant Wash and drain. Using a clean, dry knife, remove the end pieces.

Grape Juice For fresh and reconstituted juices, ensure that the sample is evenly mixed to obtain a homogeneous 

mixture. 

Green Beans Wash and drain. Do not peel. Using a clean, dry knife, remove any stems that are present.

Peaches Wash and drain. Do not peel. Remove stem and leaves if present. Using a clean, dry knife, cut the 

peach around the pit (i.e., without cutting through the pit). Remove the pit, being careful to remove as 

little of the meat as possible.

Peaches, Frozen The samples may be chopped while frozen, or to prevent damage to the chopper/homogenizer blades, 

the sample may be thawed in a refrigerator or in a room temperature water bath. Open the containers 

and pour the entire contents into the chopper/homogenizer.

Pears Wash and drain. Do not peel. Remove stem, if present. Using a clean, dry knife, cut each pear in half 

or quarters and remove the core portion.

Plums Wash and drain. Do not peel. Remove stem and leaves if present. Using a clean, dry knife, cut the 

plum around the pit (i.e., without cutting through the pit). Remove the pit, being careful to remove as 

little of the meat as possible.

Summer Squash Wash and drain. Using a clean, dry knife, remove end pieces.

Sweet Bell Peppers Wash and drain. Remove stem, core, and seeds.

Tangerines Peel each fruit and remove any excess white membrane.

Watermelon Wash and drain. Using a clean, dry knife, cut each watermelon into quarters, and remove the rind. 

For large watermelons, take alternate quarters of each fruit and mechanically chop just until a visually 

homogeneous mixture is attained. For small watermelons, take the entire sample and mechanically 

chop just until a visually homogeneous mixture is attained. If only pre-cut is available, do not rinse 

watermelon. Remove the rind.

Winter Squash Wash and drain. When possible, using a clean, dry knife, remove stem and/or end pieces.
Pesticide Data Program—Annual Summary, Calendar Year 2021

16

C. Corn Grain

USDA’s NSL tested 418 samples of field corn grain 

that originated from 17 States (Figure 5). A total 

of 115 parent pesticides, metabolites, degradates 

and/or isomers, including glyphosate and its 

aminomethylphosphonic acid (AMPA) metabolite, 

plus 8 environmental contaminants were screened 

in corn grain samples. Samples were prepared 

according to the procedures detailed in Table 4. 

Samples were extracted using a modification of 

the QuEChERS method and multiresidue analyses 

were performed using GC-MS/MS, GC-MS/MSNegative Chemical Ionization, and LC-MS/MS. 

Glyphosate and AMPA were screened by LC-MS/

MS using specialized methods. 

COVID-19 prevention measures and other factors 

led to the delays in analyzing and reporting 

analytical results for 251 corn grain samples 

within 90 days from the receipt of the samples, as 

stipulated in the PDP SOPs. The samples that were 

held (frozen) longer than 90 days (93-127 days) 

before analysis have been annotated with a special 

extraction code in the downloadable/searchable 

PDP data set for 2021.

D. Butter

The New York Department of Agriculture and 

Markets, Food Laboratory Division tested 177 

butter samples for a total of 196 parent pesticides, 

metabolites, degradates and/or isomers, plus 

14 environmental contaminants. Samples were 

prepared according to the procedures detailed 

in Table 4. Samples were extracted using a 

modification of the QuEChERS method and 

multiresidue analyses were performed using GCMS/MS, and LC-MS/MS. 

E. Quality Assurance Program

The primary objectives of the QA/QC program 

are to ensure the reliability of PDP data and the 

performance equivalency of the participating 

laboratories. Direction for the PDP QA program 

is provided through SOPs based on EPA Good 

Laboratory Practices, along with program-specific 

QA/QC requirements. The PDP SOPs provide 

uniform administrative and sampling procedures, 

as well as guidelines for laboratory operations 

and data analyses. The SOPs are revised annually 

to accommodate changes in the program and 

are aligned with International Organization 

for Standardization (ISO)4 requirements. PDP 

laboratories are accredited to ISO 17025 by 

the American Association for Laboratory 

Accreditation (A2LA), an internationally 

recognized accrediting body. 

A Technical Advisory Group, comprised of 

laboratory Technical Program Managers and 

Quality Assurance Officers, is responsible for 

annually reviewing program SOPs and addressing 

QA issues. For day-to-day QA oversight, PDP 

relies on the Quality Assurance Unit (QAU) at 

each participating facility. The QAU operates 

independently from the laboratory staff and is 

responsible for reviewing all data generated for 

PDP and for performing quarterly, internal program 

audits. Preliminary data review procedures are 

performed onsite by each laboratory’s QAU. 

MPD staff conduct a final review of data for 

conformance with SOPs.

Method Performance Requirements: Laboratories 

are required to determine and verify the limits 

of detection (LODs) and limits of quantitation 

(LOQs) for each pesticide/commodity pair. 

LODs depend on matrix, analyte, and methods 

used (extraction and instrumental). LODs for 

each pesticide/commodity pair are shown in 

the applicable crop results appendix. Additional 

method performance/validation requirements 

include modules for consistent instrument 

response (linearity), method range, and precision 

and accuracy.

Identification/Confirmation: Identification/confirmation is performed using MS technologies. 

Residue amounts greater than or equal to LOD 

and below LOQ are reported as below quantifiable 

level (BQL). BQLs are assigned values at onehalf the LOQ and are used along with values 

greater than or equal to LOQ and non-detects in 

dietary risk assessments when appropriate.

4 “ISO” is not an acronym because the initials would be different in various official languages. “ISO” is adopted from the 

Greek word “isos” meaning equal.
Pesticide Data Program—Annual Summary, Calendar Year 2021

17

Routine Quality Control Procedures: PDP 

procedures for QC are used to assess method and 

analyst performance during sample preparation, 

extraction, and cleanup. To maximize sample 

output and decrease the QC/sample ratio, samples 

are analyzed in analytical sets that include the test 

samples and the following components:

• Reagent Blank - For analysis of fruit and 

vegetables, an amount of distilled water, equivalent 

to the natural moisture content of the commodity, is 

run through the entire analytical process to confirm 

glassware cleanliness and system integrity.

• Matrix Blank - A previously analyzed sample 

of the same commodity, which contains either 

very low concentrations of known residues or no 

detectable residues, is divided into two portions. 

The first portion is used to determine background 

information on naturally occurring chemicals and 

the second to prepare a matrix spike.

• Matrix Spike(s) - Prior to extraction, a portion of 

the matrix blank is spiked with marker pesticides to 

determine the precision and accuracy of the analyst 

and instrument performance. Marker pesticides 

are compounds selected from different pesticide 

classes (e.g., organochlorines, organophosphates, 

carbamates, conazoles, imidazolinones, macrocyclic lactones, neonicotinyls, phenoxy acid 

herbicides, pyrethroids, strobilurins, sulfonyl urea 

herbicides, triazines, uracils), with physical and 

chemical characteristics representative of their 

corresponding pesticide class. Marker pesticides 

may be used to monitor recovery instead of spiking 

all pesticides. This use of marker pesticides 

optimizes the resources required to analyze the 

thousands of analyte/matrix combinations in the 

program while still allowing evaluation of daily 

recovery patterns.

In addition, each laboratory must perform matrix 

spikes at least quarterly for each analyte/crop 

combination it reports. Some laboratories choose to 

rotate spikes of all compounds on a set-by-set basis 

or spike all compounds analyzed with each set, so 

that the amount of spike recovery data obtained 

exceeds the minimal requirements previously 

stated. During 2021, PDP laboratories quantitated a 

total of 88,904 matrix spikes, with an overall mean 

recovery of 97.2 percent and an overall 20.1 percent 

coefficient of variation (% C.V.). The % C.V. is 

calculated as the standard deviation divided by the 

mean and then multiplied by 100.

• Process Control Spike - A compound with physical 

and chemical characteristics similar to those of 

the pesticides being tested is used to evaluate the 

analytical process on a sample-by-sample basis. 

Each of the analytical set components, except 

the reagent and matrix blanks, is spiked with 

process controls. During 2021, PDP laboratories 

quantitated a total of 22,135 process controls on 

10,127 samples, with an overall mean recovery 

of 101 percent and an overall 17.2 percent C.V. 

Of these process controls, 47 (0.21 percent) were 

reruns due to initial failure to meet PDP recovery 

criteria. The rerun values are not included in these 

statistics.

Proficiency Testing: All facilities are required 

to participate in PDP’s Proficiency Testing 

(PT) program. In order to properly benchmark 

performance, PDP laboratories participate in 

the international Food Analysis Performance 

Assessment Scheme (FAPAS), administered by 

the Food and Environment Research Agency, 

Sand Hutton, York, United Kingdom. In 2021, 

PDP laboratories that routinely analyze fruit and 

vegetable samples via MRMs participated in one 

FAPAS round for broccoli purée that contained 

14 fortified analytes. Laboratories were evaluated 

based on z-scores for reported compounds, as well 

as any reported false negatives or false positives. 

PDP laboratories typically obtained z-scores 

less than two, which is deemed satisfactory 

performance.

In addition, PDP laboratories participate in an 

internal PT program that is tailored to current PDP 

commodities and testing profiles. For this internal 

program, the California Department of Food and 

Agriculture QAU prepares and issues rounds 

designed in collaboration with MPD. Spiking 

compounds are selected with specificity and 

levels for each commodity. Fortification levels of 

selected analytes are generally 1 to 10 times the 

program LOQ for that commodity/compound pair. 

For each multiresidue round, one compound per 

set is typically repeated within the round to provide 

an indicator of repeatability. The resulting data are 

used to determine performance equivalency among 
Pesticide Data Program—Annual Summary, Calendar Year 2021

18

the testing laboratories and to evaluate individual 

laboratory performance.

During 2021, PDP laboratories received two 

multiresidue fruit and vegetable PT rounds (oranges 

and bell peppers), each consisting of three test 

samples. The orange samples were fortified with 

a total of 12 different compounds, with cyprodinil 

spiked on 2 different samples. The bell pepper 

samples were fortified with a total of 11 different 

compounds, with aldrin spiked on 2 different 

samples at the same level to evaluate within and 

between laboratory variability. Laboratories were 

evaluated based on percent recovery for reported 

compounds, as well as any reported false negatives 

or false positives. PDP laboratories typically 

obtained recoveries within the range of 50-150%, 

which is acceptable performance under the PDP 

QC SOP.

Onsite Reviews: In addition to the onsite assessments 

performed by A2LA that are required to maintain 

ISO 17025 accreditation, MPD staff chemists 

perform onsite reviews of laboratory operations 

to determine compliance with PDP SOPs and 

provide a report of findings identifying potential 

areas of improvement. Improvements in sampling, 

chain-of-custody, laboratory, recordkeeping, and 

electronic data transmission procedures are made 

as a result of onsite reviews. The 2021 onsite 

reviews were postponed due to COVID-19-related 

travel restrictions.

IV. Database Management

PDP maintains an electronic database that serves as a 

central data repository. The data captured and stored 

in the PDP database include sample collection and 

product information, residue findings, and process 

control recoveries for each sample analyzed, in 

addition to QA/QC fortified recoveries for each set 

of samples. Each calendar-year survey is stored in 

a separate database structure, which allows easier 

administration and data reporting. The PDP data 

pathway is illustrated in Figure 6.

A. Electronic Data Path

PDP utilizes the Remote Data Entry (RDE) 

application, which is a customized software 

tool that allows participating State and Federal 

laboratories to electronically enter and transmit 

data. The RDE application is distributed, with all 

user interface software and database files residing 

on laboratory computers. The laboratory users 

need only Microsoft® Office tools to interface 

with the RDE application. Access is controlled 

through separate user login/password accounts and 

user access rights for the various system functions 

based on position requirements. File encryption is 

used to secure all data stored in and transmitted 

from the RDE application.

A separate Windows®-based application allows 

sample collectors to capture the standardized 

Sample Information Form (SIF) electronically on 

laptop or tablet computers. The e-SIF application 

generates formatted text files containing sample 

information that are e-mailed to MPD staff for 

central processing and distribution to the analyzing 

laboratories for import into the RDE application.

The RDE data entry screens have extensive editing 

functions and cross-checks built into the software 

to ensure valid values are entered for all critical 

data elements. This task is made easier by the 

practice of capturing and storing standardized 

codes for all critical alphanumeric data elements 

rather than their complete names, meanings, or 

descriptions. This coding scheme allows for faster 

and more accurate data entry, saves disk storage 

space, and allows the user to perform ad-hoc 

queries (data searches) on the database easily. The 

data entry screens also perform checks on numeric 

fields, dates, and other character fields to ensure 

entries are within established boundaries.

MPD staff chemists review the data online and then 

mark the data as ready-for-upload to the central 

PDP database. A separate upload application 

converts and passes the data to the PDP database, 

which is maintained using Microsoft® SQL Server 

and Access database tools. Access to the central 

PDP database is limited to MPD personnel and is 

controlled through password protection and user 

access rights.

B. Data Reporting

The MPD staff frequently receives requests for 

data from government agencies and interested 

outside parties. Ad hoc queries and custom reports 
Pesticide Data Program—Annual Summary, Calendar Year 2021

19

- Collection in 9 States

- Samples taken close to consumer consumption

- Standardized sample information forms

- Data entry on tablet/laptop computers

- Chemists review data on-screen

- Upload data to central database

- 1 Federal and 7 State laboratories

- Fruit and vegetable samples prepared for

 consumption

- Detect residues at low levels

- Pesticide residue data generated

- Multi-tiered quality assurance data review

 process

- Customized data entry software

- Import data from other systems

- Access controlled by user login

- Extensive data cross-checks

- Data reconciliation

- Standard & ad hoc reporting

- Annual Summary

- Data available online

YEAR-END REVIEW

INTERNET

SAMPLE COLLECTION DATA REVIEW AT HQ

LABORATORY ANALYSIS

LABORATORY REMOTE DATA 

ENTRY (RDE) DATA REPORTING

INTERNET

Figure 6. Pesticide Data Program (PDP) Data Pathway: An illustration of PDP data path from sample collection 

through laboratory analysis and reporting.
Pesticide Data Program—Annual Summary, Calendar Year 2021

20

are generated to fill such requests. An electronic 

library of data queries is maintained to generate 

standardized data summaries, including the data 

tables, charts, and appendixes in this annual 

summary. PDP calendar-year database files are 

made available for download from the PDP website. 

The data files on the website are delimited text files 

that contain a portion of the sampling data, all 

reported residue findings, and reference lists that 

can be used to interpret the standardized codes seen 

in the PDP data. The data files can be imported into 

defined database structures and manipulated using 

common database management software packages.

C. Online Database Search Tool

An online PDP Database search tool is available 

for public use. The search tool allows anyone with 

internet access to search for PDP pesticide residue 

findings on commodities tested across all published 

years. Search criteria are selected from lists of all 

reported commodities, pesticides, and survey years. 

One of five output preferences is selected to show 

individual residue findings or summary data. The 

generated dataset can be exported to a commaseparated values (CSV) file. The search tool can be 

reached from any PDP website page or directly at 

https://apps.ams.usda.gov/pdp.

V. Sample Results and Discussion

A. Overview

In 2021, PDP conducted surveys on a variety of 

foods including fresh and processed fruit and 

vegetables, butter, and corn grain. Of the 10,127 

samples analyzed in 2021, 9,532 were fresh and 

processed fruit and vegetable samples, 177 were 

butter samples, and 418 were corn grain samples. 

PDP testing methods are designed to detect low 

levels of pesticide residues. In 2021, over 99 

percent of the samples tested had residues below 

the tolerances established by the EPA, with 24.0 

percent having no detectable pesticide residue. The 

data reported by PDP illustrate that residues found 

in agricultural products sampled are at levels that 

do not pose risk to consumers’ health and are safe 

according to EPA and FDA.

Appendix B tabulates the distribution of residue 

results for fruit and vegetables. Information 

included in this appendix are the number of 

samples analyzed for each compound, number 

and percent of samples with detections, range of 

concentrations detected, range of analytical LODs, 

and EPA tolerance levels. Appendixes C and D 

tabulate the distribution of residue results for corn 

and butter, respectively.

PDP laboratories tested foods for low levels 

of environmental contaminants. The selected 

contaminants were pesticides and are no longer 

used in the United States, but due to their 

persistence in the environment, particularly 

in soil, these contaminants can be still taken 

up by plants. Appendix E tabulates the results 

for environmental contaminants across all 

commodities. Environmental contaminants are 

consolidated into a single appendix because they 

have no registered uses and are not applied to 

crops in the United States. These compounds are 

subject to FDA Action Levels (ALs) rather than 

tolerances. Because environmental contaminants 

continue to persist in the environment, they may 

be present in food commodities at generally low 

levels.

For fresh and processed fruit and vegetables and 

butter, most of the collected and analyzed samples 

(66.5 percent) were produced in the United 

States, 32.1 percent were imports, 0.9 percent 

were of mixed national origin, and 0.5 percent 

were of unknown origin. Appendix F shows the 

distribution of sample origin by State or country. 

Of all samples collected and analyzed (excluding 

corn grain), approximately 33.1 percent (3,218 of 

9,709) were grown, packed, and/or distributed in or 

from California, which is the leading agricultural 

production and most populous State. Corn grain 

is excluded from Appendix F because the targeted 

corn samples rely on a different sampling frame 

and are not collected from routine PDP sample 

collection locations. The origins for the corn grain 

samples are shown on Figure 5. 

Food monitoring data, together with dietary 

consumption surveys, are used by EPA to estimate 

dietary exposure to pesticides to ensure the safety 

of existing pesticide uses. EPA uses all results 

reported by PDP, including sample results reported 

as below the LOD and those above the tolerance. 

PDP laboratories are required to establish LODs 
Pesticide Data Program—Annual Summary, Calendar Year 2021

21

and report any instrumental response below 

the LOD as a non-detect. LODs are established 

experimentally for each pesticide/commodity pair 

and are reported with each data set. The number 

of non-detects can be used in conjunction with 

percent-crop-treated data to determine what 

proportion of these values may be counted as zero 

towards the dietary exposure. All individual sample 

data can be downloaded from the PDP website 

at http://www.ams.usda.gov/pdp or obtained by 

contacting MPD.

B. Import Versus Domestic Residue Comparisons

Information about the origin of each PDP sample 

is recorded when the sample is collected. Figure 3 

illustrates the portion of the domestic and import 

component for each of the PDP fruit and vegetable 

commodities in 2021. The data generated by 

PDP reflect pesticide residues in foods, both 

domestic and imported products, available to the 

U.S. consumer. Many of the samples of fresh 

and processed commodities were almost entirely 

of domestic origin, such as plums (100 percent), 

cauliflower (95.5 percent), and celery (95.5 

percent), with only minor import (4.0 percent and 

4.2 percent, respectively) and unknown origins (0.5 

percent and 0.3 percent, respectively). Other fresh 

commodities, such as eggplant, summer squash 

and winter squash were available from domestic 

growers part of the year and imported during the 

remaining months, as illustrated in Figure 4.

Comparison of selected residues detected in 

imported versus domestic blueberries, green beans, 

peaches, and pears can be found in Appendix G. 

These commodity sets were selected to compare 

data where residues of the listed pesticides are 

present in greater than 5 percent of the total 

samples for the commodity. The comparison of 

individual pesticides between the countries of 

origin shows that the residue profiles for domestic 

and imported crops are significantly different, as 

would be expected due to different pest pressures.

The blueberry data in Appendix G show 

that acetamiprid, boscalid, fludioxonil and 

pyraclostrobin were detected more frequently 

in imported samples than in domestic samples. 

Boscalid was the most frequently detected in 

48.1 percent of the samples from Mexico, 65.6 

percent of the Peruvian samples, and 18.4 percent 

of the U.S. samples. Malathion and phosmet were 

detected more frequently in domestic samples. For 

example, malathion was detected in 18.4 percent 

of the U.S. samples, 3 percent of the Mexican 

samples, and was not detected in any of the 

samples from Peru. Imidacloprid and cyprodinil 

were detected with relatively equal frequency in 

the U.S., Mexican and Peruvian samples. 

The green bean data in Appendix G show that 

compounds like carbendazim and imidacloprid 

desnitro were detected more frequently in imported 

samples than in domestic samples. For example, 

carbendazim was detected in 51.4 percent of the 

samples from Mexico and 28 percent of the U.S. 

samples. Azoxystrobin and pyraclostrobin were 

detected more frequently in domestic samples than 

in imports. For example, azoxystrobin was detected 

in 32.6 percent of U.S. samples and 10.4 percent 

of Mexican samples. Bifenthrin and boscalid were 

detected with relatively equal frequency in both 

the U.S. and Mexican green beans.

The peach data in Appendix G show that 

compounds like acetamiprid, fludioxonil, and 

tebuconazole were detected more frequently 

in imported samples than in domestic samples. 

Azoxystrobin, fluopyram and pyraclostrobin were 

detected more frequently in domestic samples 

than in imports. For example, pyraclostrobin was 

detected in 27.1 percent of U.S. samples and was 

not detected in any of the samples from Chile. 

Chlorantraniliprole and methoxyfenozide were 

detected with relatively equal frequency in both 

the U.S. and Chilean peaches.

The pear data in Appendix G show that 

chlorantraniliprole, ethoxyquin and THPI were 

detected more frequently in imported samples than 

in domestic samples. THPI was the most detected 

in 63.1 percent of the Argentinian samples and 

0.2 percent of the U.S. samples. Spinetoram, 

thiophanate methyl and tolfenpyrad were detected 

more frequently in domestic samples than in 

imports. For example, tolfenpyrad was detected in 

31.1 percent of U.S. samples and was not detected 

in any of the samples from Argentina. Fludoxonil 

and thiabendazole were detected with relatively 

equal frequency in both the U.S. and Argentinian 

pears.
Pesticide Data Program—Annual Summary, Calendar Year 2021

22

All pesticides detected in this comparison of 

domestic and imported commodities had tolerances 

for the given commodity in the United States as 

shown in Appendix G; however, the profiles of 

residue findings were markedly different in U.S. 

samples versus imported samples. The differences 

in residue detections between countries were likely 

due to the pesticides used in response to pest 

pressures based on differing environmental and 

climatic conditions as well as crop production and 

protection practices.

C. Postharvest Applications

Pesticides can be applied before and after harvest 

depending on the crop and approved label use. 

PDP data capture both preharvest and postharvest 

uses because samples are collected at points when 

all pesticide applications have already occurred. 

Pesticides applied postharvest are used primarily 

as fungicides (e.g., azoxystrobin, imazalil, 

o-phenylphenol, and thiabendazole) and growth 

regulators/sprouting inhibitors (e.g., chlorpropham). 

Some detections reported in Appendix B most 

likely reflect postharvest applications to the raw 

agricultural commodity.

D. Discussion of Results

There are many pesticides registered for use on the 

same crop; however, not all registered pesticides 

are used at the same time or location. In 2021, 24.0 

percent of the samples tested had no detectable 

pesticide residue, and over 99 percent of the 

samples tested had residues below the tolerances 

established by the EPA. Pesticide use is primarily 

dictated by local pest pressures and environmental 

conditions conducive to growth of pest populations, 

as well as the planting of susceptible varieties.

These differences are captured by PDP data, which 

reflect actual residues present in food grown in 

various regions of the United States and foreign 

countries. Thus, in evaluating consumer exposure 

to pesticides through the diet, EPA uses all 

available information provided by registrants, PDP, 

and others to verify that tolerances meet the safety 

standards set by FQPA. The presence of residues 

at levels below the established tolerance serves to 

ensure and verify the safety of the Nation’s food 

supply.

Food commodities and the pesticides detected in 

at least 5 percent of samples tested are shown in 

Appendix H. The data shown include the range 

and mean of values detected and EPA tolerance 

references for each commodity/pesticide pair.

By virtue of the MRMs employed, PDP provides 

critical data that can be used by EPA to evaluate 

exposure to multiple residues from the same 

commodity. The data are crucial for assessments 

that consider cumulative exposure to pesticides 

determined to have common mechanisms of 

toxicity. The distribution of multiple pesticides 

occurring in samples tested during 2021 is 

presented in Appendix I. These data indicate that 

24.0 percent of all samples tested contained no 

detectable pesticides, 18.5 percent contained 

1 pesticide, and 57.5 percent contained more 

than 1 pesticide. Parent compounds and their 

metabolites are combined to report the number of 

“pesticides” rather than the number of “residues.” 

Environmental contaminants, listed in Appendix E, 

have been excluded from this count of pesticides.

One sample of peaches and 1 sample of winter 

squash contained residues of 19 pesticides. No 

residues found on the peach and winter squash 

samples exceeded the established tolerances. 

Multiple residue detections can result from the 

application of more than one pesticide on a crop 

during a growing season; in addition, several other 

factors can contribute to multiple detections. For 

example, unintentional spray drift in the field, 

planting of crops in fields previously treated 

with the pesticide, and/or transfer of residues of 

postharvest fungicides or growth regulators applied 

to other commodities stored in the same storage 

facilities could all contribute to residue detections.

In most cases, samples analyzed by PDP are 

composites of 3 to 5 pounds of commodity from the 

same lot. Therefore, the estimated concentrations 

for multiple residue detections in these composite 

sample results may or may not reflect the number 

or levels of pesticides in a single-serving item of a 

commodity.

E. Special Projects

Corn Grain: The USDA NSL conducted pesticide 

residue testing on 418 corn grain samples. Appendix 
Pesticide Data Program—Annual Summary, Calendar Year 2021

23

C shows that six different residues corresponding 

to five distinct pesticides were detected in corn 

grain samples. The most frequently detected 

residue was for glyphosate, which was detected 

in 146 samples (34.9 percent). Malathion was 

detected in seven samples (1.7 percent) and 

malathion oxygen analog was found in one sample 

(0.2 percent). Deltamethrin was found in five 

samples (1.2 percent), chlorpyrifos was detected 

in three samples (0.7 percent), and cypermethrin 

was detected in one sample (0.2 percent). All 

residue detections were lower than the established 

tolerances for those compounds with established 

tolerances.

Butter: The New York laboratory conducted testing 

for pesticide residues on 177 butter samples. Overall, 

15 different residues (including metabolites and 

isomers) representing 14 distinct pesticides were 

detected in butter samples (Appendix D). The most 

frequently detected residue was novaluron, which 

was detected in 75 butter samples (42.4 percent). 

Permethrin cis was detected in 71 samples (40.1 

percent) and permethrin trans was found in 69 

samples (39.0 percent). Bifenthrin was detected 

in 65 samples (36.7 percent), piperonyl butoxide 

was found in 42 samples (23.7 percent), and total 

cyhalothrin was detected in 41 samples (23.2 

percent). Flubendiamide and methoxyfenozide 

were each detected in three samples (1.7 percent). 

Buprofezin, difenoconazole, and pyraclostrobin 

were each found in two samples (1.1 percent). 

Residues of ametoctradin, diphenylamine, 

fenpyroximate, and thiabendazole were each 

detected in one sample (0.6 percent).

F. Environmental Contaminants

Persistent organic pollutants (POPs) are 

environmental contaminants that include pesticides 

with cancelled uses in the United States, but their 

residues persist in the environment, particularly in 

soil, where they may be taken up by plants. These 

data are also used to facilitate international trade. 

Residue results for environmental contaminants 

may be found in Appendix E.

DDT, DDD, and DDE: PDP screened samples for 

various metabolites of DDT including DDT o,p’; 

DDT p,p’; DDD o,p’; DDD p,p’; DDE o,p’; and 

DDE p,p’. Use of DDT has been prohibited in 

the United States since 1972; however, due to its 

persistence in the environment, low-level residues 

of DDT and its DDD and DDE metabolites were 

detected in some commodities tested. The DDE 

p,p’ metabolite was the most frequently detected. 

DDE p,p’ was detected in butter (45.2 percent of 

samples), summer squash (5.2 percent), broccoli 

(4.9 percent), winter squash (3.0 percent), carrots 

(2.4 percent), green beans (2.1 percent), celery (0.6 

percent), and tangerines (0.2 percent). DDT o,p’ 

was detected in summer squash (3.8 percent) and 

winter squash (1.0 percent). DDT p,p’ was detected 

in summer squash (1.9 percent), winter squash 

(1.0 percent), and carrots (0.1 percent). Residues 

of DDD o,p’ were detected in winter squash (0.4 

percent) and summer squash (0.3 percent), and 

DDD p,p’ was detected only in summer squash 

(0.3 percent). Residues of the metabolite DDE o,p’ 

were not detected in samples tested. All residues 

detected were lower than established FDA Action 

Levels.

PDP tested samples for additional POPs including: 

aldrin; dieldrin; endrin; BHC (alpha/beta/delta/

epsilon) and lindane (BCH gamma); chlordane (cis, 

trans) and its metabolite oxychlordane; heptachlor 

and its epoxide metabolite; hexachlorobenzene 

(HCB); and mirex. The POPs listed in this section 

have not been registered for sale and distribution 

in the United States since the 1970s and 1980s. 

Despite these cancellations and because they 

persist in the environment, trace-level residues 

of chlordane (cis and trans), dieldrin, endrin, 

heptachlor (epoxide), and oxychlordane were 

detected in some of the tested commodities.

Chlordane cis was detected in 1.4 percent of 

summer squash samples, 1.3 percent of winter 

squash samples, and in 0.1 percent of eggplant 

samples. Chlordane trans was detected in 1.1 

percent of winter squash samples and 0.3 percent 

of broccoli samples. Dieldrin was detected in 10.1 

percent of winter squash samples, 7.9 percent of 

summer squash samples, 0.4 percent of broccoli 

samples, and 0.3 percent of cantaloupe samples. 

Endrin was detected in 1.3 percent of winter 

squash samples and 1.0 percent of summer squash 

samples. Heptachlor epoxide was detected in 2.1 

percent of summer squash samples and 1.1 percent 

of winter squash samples. Oxychlordane was 

detected in 0.1 percent of winter squash samples. 
No residues of aldrin, BHC (alpha/beta/delta/

epsilon), HCB, heptachlor (parent), lindane (BHC 

gamma), or mirex were detected in any samples.

G. Tolerance Violations

A tolerance is defined under Section 408 of the 

Federal Food, Drug, and Cosmetic Act as the 

maximum quantity of a pesticide residue allowable 

on a raw agricultural commodity. Tolerances are 

also applicable to processed foods. The FQPA of 

1996 amended the Federal Insecticide, Fungicide 

and Rodenticide Act to require EPA to periodically 

review each pesticide registration using the most 

currently available data. Timely pesticide data 

provided by PDP enable the EPA to refine risk 

estimates used in the pesticide registration review 

process.

A tolerance violation occurs when a residue is 

found that exceeds the tolerance level or when 

a certain residue is found for which there is no 

established tolerance. Apart from meat, poultry, 

and egg products, for which USDA’s Food 

Safety and Inspection Service is responsible, 

FDA enforces tolerances for all imported foods 

and domestic foods that move through interstate 

commerce. Unlike enforcement programs, PDP 

emphasizes determination of residues at low 

levels of detection levels rather than quick turnaround times. When PDP identifies samples with 

residues exceeding the tolerance or with residues 

for which there is no established tolerance, these 

detections are reported to FDA’s headquarters 

office. This notification is made in accordance 

with a Memorandum of Understanding between 

USDA and FDA for the purpose of identifying 

areas where closer surveillance may be needed. 

FDA assesses PDP apparent violation data for 

appropriateness for follow up under its regulatory 

pesticide program. Due to the time required for 

completion of PDP analyses and data reporting, 

FDA follow up will usually be at a subsequent 

harvest or commodity availability period.

Residues exceeding the established tolerance 

or ALs are noted with an “X” in Appendix B. 

Similarly, residues for which a tolerance is not 

established are noted with a “V” in Appendixes 

B, D and E. The “X” and “V” annotations are 

followed by a number indicating the number of 

samples reported to FDA. The EPA tolerances cited 

in this summary and appendixes apply to 2021 and 

not to the current year. There may be instances 

where tolerances may have been recently changed 

that would influence whether a residue is violative.

An established tolerance may apply to more than 

one residue because pesticides may break down 

into more than one metabolite or contain more than 

one isomer. If a pesticide also has a metabolite 

of interest, PDP assigns the metabolite the same 

tolerance as the parent compound. However, if the 

metabolite has a higher tolerance in the Code of 

Federal Regulations (CFR), the higher of the two 

values is used for the metabolite. If a pesticide has 

multiple isomers, the tolerance is the sum of the 

parent and isomer(s) of interest. For example, the 

CFR tolerance for endosulfan combines residues of 

the isomers, endosulfan I and endosulfan II, and the 

metabolite endosulfan sulfate. Organophosphate 

tolerances may combine the parent compound and 

the sulfone and sulfoxide metabolites. Therefore, 

where applicable, the pesticide violations in 

Appendix J are combined residues of parent and 

any isomers and/or metabolites to count the total 

number of samples with tolerance violations.

A total of 423 samples with 466 pesticides were 

reported to FDA as Presumptive Tolerance 

Violations (PTV) either because they exceeded the 

established tolerance, or no tolerance is established. 

Pesticides exceeding the tolerance were detected 

in 0.53 percent (54 samples) of the total samples 

tested (10,127 samples). Of these 54 PTV exceeder 

samples, 29 were domestic (53.7 percent), 24 were 

imported (44.4 percent), and 1 was of unknown 

origin (1.9 percent). PTV exceeder samples 

represent 0.42 percent of the total domestic samples, 

0.75 percent of the total imported samples, and 

2.1 percent of the total unknown origin samples. 

The samples containing pesticides that exceeded 

established tolerances included: 4 samples of 

blueberries, 1 sample of broccoli, 2 samples of 

celery, 3 samples of eggplant, 31 samples of green 

beans, 5 samples of peaches, 1 sample of pears, 

and 7 samples of winter squash. Commodities that 

did not have any samples exceeding the established 

tolerances were the following: butter, cantaloupe, 

carrots, cauliflower, corn grain, grape juice, plums, 

summer squash, sweet bell peppers, tangerines, 

and watermelon.

Pesticide Data Program—Annual Summary, Calendar Year 2021

24
♦♦♦♦♦♦

Residues with no established tolerance were found 

in 3.7 percent (374 samples) of the total samples 

tested (10,127 samples). Of these 374 samples, 220 

were domestic (58.8 percent), 150 were imported 

(40.1 percent), and 4 samples were of unknown 

origin (1.1 percent). PTV samples with residue 

detections for which no tolerance was established 

represent 3.2 percent of the total domestic samples, 

4.7 percent of the total imported samples, and 

8.3 percent of the total unknown origin samples. 

These samples included 373 fresh fruit and 

vegetable samples and 1 butter sample. There were 

349 samples that contained 1 pesticide for which 

no tolerance was established; 23 samples with 2 

pesticides for which no tolerance was established; 

1 sample with 3 pesticides for which no tolerance 

was established; and 1 sample that contained 5 

pesticides for which no tolerance was established. 

Five of the 374 samples also contained 1 or more 

pesticides that exceeded an established tolerance. 

The pesticide residue levels and commodities are 

listed in Appendix J for samples with PTVs. In most 

cases, these pesticides with no established tolerance 

were detected at low levels. Some pesticide 

residues may have resulted from unintentional 

spray drift in the field; planting of crops in fields 

previously treated with the pesticide; transfer of 

pesticide residues, post-harvest fungicides, or other 

growth regulators applied to other commodities 

kept in the same storage facilities; or exposure 

to pesticides during transportation through the 

distribution chain. Commodities that did not have 

any samples with pesticides for which no tolerance 

was established were corn grain, grape juice, and 

watermelon.

H. Look Ahead

At the time this report was drafted, 2022 PDP 

sampling and testing was underway. Commodities 

included in the 2022 survey are: baby food green 

beans, baby food peaches, baby food pears, baby 

food sweet potatoes, blueberries, butter, carrots, 

celery, corn grain, grapes, green beans, mushrooms, 

peaches, peanut butter, pears, plums, potatoes, 

summer squash, tomatoes, and watermelon. It is 

anticipated that the 2022 PDP data will be published 

in an annual summary approximately 1 year after 

the date of this report.

Pesticide Data Program—Annual Summary, Calendar Year 2021

25
Appendix A 

Commodity History

Appendix A identifies commodities sampled by the Pesticide Data Program (PDP) through 

December 2022. Updates to this list are posted on the PDP Web site at

www.ams.usda.gov/pdp. 
Fresh Commodities

Commodity Start Date End Date

Apples 1 Sep-91 Dec-96

Apples (S-1) Jan-99 Dec-99

Apples (S-2) Jan-99 May-99

Apples Oct-00 Sep-02

Apples (T-1) Jan-03 Dec-03

Apples Jan-04 Dec-05

Apples Jan-09 Dec-10

Apples (B-1) Aug-12 Oct-12

Apples Oct-14 Sep-16

Asparagus Jan-02 Jun-03

Asparagus Jul-08 Jun-10

Asparagus Jul-17 Jun-19

Avocados Jul-12 Dec-12

Bananas Sep-91 Sep-95

Bananas Jan-01 Dec-02

Bananas (TSP) Jul-03 Dec-03

Bananas Jan-06 Dec-07

Bananas Apr-12 Mar-14

Bananas Jan-19 Dec-20

Basil Apr-19 Sep-19

Blueberries (cultivated) 2 Jan-07 Dec-08

Blueberries (cultivated) 2 Jan-14 Dec-14

Blueberries (cultivated) 2 Oct-20 Sep-22

Broccoli Oct-92 Dec-94

Broccoli Jan-01 Dec-02

Broccoli Oct-06 Sep-08

Broccoli Jan-13 Dec-14

Broccoli Jan-20 Dec-21

Cabbage Jan-10 Dec-11

Cabbage Jul-17 Jun-19

Cantaloupe Jul-98 Jun-00

Cantaloupe Oct-03 Sep-05

Cantaloupe Jan-10 Mar-10

Cantaloupe Oct-10 Jun-12

Cantaloupe Jul-19 Jun-21

Carrots 1 Oct-92 Sep-96

Carrots Oct-00 Sep-02

Carrots Jan-06 Dec-07

Carrots Jan-13 Dec-14

Carrots Apr-20 Mar-22

Cauliflower Oct-04 Sep-06

Cauliflower Oct-11 Sep-13

APPENDIX A. COMMODITY HISTORY

AS OF DECEMBER 2022

Appendix A. Page 1 of 11
Commodity Start Date End Date

Cauliflower Oct-19 Sep-21

Celery Feb-92 Mar-94

Celery Jan-01 Dec-02

Celery Jan-07 Dec-08

Celery Jan-13 Dec-14

Celery 

3 Jul-21 Ongoing

Cherries 

4 May-00 Aug-01

Cherries 

2 May-07 Sep-07

Cherries Apr-14 Mar-16

Cilantro Oct-09 Sep-10

Cilantro Oct-18 Mar-19

Collard Greens Oct-19 Sep-20

Cranberries Oct-06 Dec-06

Cranberries 

2 Oct-16 Mar-18

Cucumbers Jan-99 Dec-00

Cucumbers Oct-02 Sep-04

Cucumbers Jan-09 Dec-10

Cucumbers Jul-15 Jun-17

Eggplant Jan-05 Dec-06

Eggplant Jan-20 Dec-21

Grapefruit Aug-91 Dec-93

Grapefruit Jan-05 Dec-06

Grapefruit Oct-15 Sep-17

Grapes 

1 May-91 Dec-96

Grapes Jan-00 Dec-01

Grapes (TSP) Jul-03 Dec-03

Grapes Jan-04 Dec-05

Grapes Jan-09 Dec-10

Grapes Jan-15 Dec-16

Grapes Jan-22 Ongoing

Green Beans Feb-92 Dec-95

Green Beans Jan-00 Dec-01

Green Beans Apr-04 Mar-05

Green Beans Jan-07 Dec-08

Green Beans Jul-13 Sep-16

Green Beans Oct-20 Sep-22

Green Onions Oct-08 Sep-09

Green Onions Jan-18 Dec-18

Greens (collard & kale) Oct-06 Sep-08

Hot Peppers Oct-10 Sep-11

Hot Peppers Jan-19 Dec-19

Kale Jan-17 Dec-18

Kiwi Fruit Apr-18 Mar-20

Lettuce May-91 Dec-94

Lettuce Oct-99 Sep-01

Lettuce Jan-04 Dec-05

Lettuce Jan-10 Dec-11

Appendix A. Page 2 of 11
Commodity Start Date End Date

Lettuce Jul-15 Jun-17

Lettuce, Organic Jan-09 Dec-09

Mangoes Apr-10 Sep-10

Mangoes Oct-17 Sep-18

Mushrooms Oct-01 Sep-03

Mushrooms Oct-11 Sep-13

Mushrooms Jan-22 Ongoing

Mustard Greens Jan-19 Dec-19

Nectarines 

5 Jul-00 Sep-01

Nectarines Jan-07 Dec-08

Nectarines Jan-13 Dec-15

Onions Jan-02 Dec-03

Onions Oct-11 Sep-12

Onions Jan-17 Dec-17

Oranges 

1 Aug-91 Dec-96

Oranges Jan-00 Dec-01

Oranges Jan-04 Dec-05

Oranges Jan-09 Dec-10

Oranges Jan-15 Dec-16

Papaya Jul-11 Jun-12

Peaches Feb-92 Sep-96

Peaches (S-3) Jan-00 Sep-00

Peaches 

6 Jan-01 Sep-02

Peaches (T-1) May-03 Sep-03

Peaches Oct-06 Sep-08

Peaches (B-1) Aug-12 Oct-12

Peaches Jul-13 Jun-15

Peaches 

3 Jan-21 Dec-22

Pears Jan-97 Jun-99

Pears (S-1) Jul-98 Jun-99

Pears Oct-03 Sep-05

Pears Jan-09 Dec-10

Pears (B-1) Oct-12 Nov-12

Pears Jan-15 Dec-16

Pears Jan-21 Dec-22

Pineapples Jul-00 Jun-02

Plums 

7 Jan-05 Dec-06

Plums Oct-11 Sep-13

Plums Jul-21 Ongoing

Potatoes May-91 Dec-95

Potatoes (S-4) Dec-96 Dec-97

Potatoes Jul-00 Jun-02

Potatoes Jan-08 Dec-09

Potatoes Jan-15 Dec-16

Potatoes Apr-22 Ongoing

Radishes Jan-19 Dec-20

Raspberries 

2 Jan-13 Dec-13

Appendix A. Page 3 of 11
Commodity Start Date End Date

Snap Peas Jan-11 Dec-12

Snap Peas Jan-17 Dec-18

Spinach 1 Jan-95 Sep-97

Spinach Jul-02 Dec-03

Spinach 8 Jan-06 Sep-06

Spinach Jan-08 Dec-09

Spinach Jan-15 Dec-16

Strawberries 2 Jan-98 Sep-00

Strawberries Jan-04 Dec-05

Strawberries Jan-08 Dec-09

Strawberries Oct-14 Sep-16

Summer Squash Oct-06 Sep-08

Summer Squash Oct-12 Sep-14

Summer Squash Oct-20 Sep-22

Sweet Corn (on-the-cob) Oct-08 Sep-10

Sweet Corn (on-the-cob) Oct-14 Sep-15

Sweet Bell Peppers Jan-99 Dec-00

Sweet Bell Peppers Oct-02 Sep-04

Sweet Bell Peppers Jan-10 Mar-12

Sweet Bell Peppers 3 Jul-19 Jun-21

Sweet Potatoes 1 Jan-96 Jun-98

Sweet Potatoes Jan-03 Dec-04

Sweet Potatoes Oct-08 Sep-10

Sweet Potatoes Apr-16 Mar-18

Tangerines Jan-11 Dec-12

Tangerines Oct-19 Sep-21

Tomatoes 1 Jul-96 Jun-99

Tomatoes Jan-03 Dec-04

Tomatoes Jan-07 Dec-08

Tomatoes Oct-14 Sep-16

Tomatoes Jan-22 Ongoing

Tomatoes, Cherry/Grape Jan-11 Dec-12

Watermelon 9 Oct-05 Sep-06

Watermelon Apr-10 Sep-10

Watermelon Jul-14 Jun-15

Watermelon Oct-21 Ongoing

Winter Squash 2 Jan-97 Jun-99

Winter Squash Jul-04 Jun-06

Winter Squash Oct-11 Mar-13

Winter Squash Jan-20 Dec-21

NOTES

1

 Excludes sampling hiatus September - November 1996.

2

 Frozen collected when fresh unavailable.

3

 2021 samples that were delayed and held frozen for >90 days (due to COVID-19 pandemic

 related delays) are annotated in the downloadable/searchable PDP data set.

Appendix A. Page 4 of 11
Commodity Start Date End Date

4

 Sampling adjusted for market availability. Cherries were sampled for 2 years 

 (May-00 - Aug-01) for a total of 6 months.

5

 Sampling adjusted for market availability. Nectarines were sampled for 2 years 

 (Jul-00 - Sep-01) for a total of 6 months.

6

 Sampling adjusted for market availability. Peaches were sampled for 2 years

 (Jan-01 - Sep-02) for a total of 16 months.

7

 Dried plums (prunes) were collected when fresh plums were not available.

8

 Spinach ended earlier than planned due to the unavailability of product.

9

 Samples collected in California, Florida, and Texas only.

(B-1) Special project testing for bifenthrin in multi-residue screen.

(S-1) Special single serving project testing for organophosphates.

(S-2) Special single serving project testing for carbamates.

(S-3) Special single serving project testing for carbamate, organochlorine, 

 organophosphate, organonitrogen, and sulfur compounds.

(S-4) Special single serving project testing for aldicarb.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 5 of 11
Processed Commodities

Commodity Start Date End Date

Apple Juice 

1 Jul-96 Dec-98

Apple Juice Jan-02 Dec-02

Apple Juice Jul-07 Jun-08

Apple Juice Jul-12 Jun-13

Apple Juice Jan-20 Dec-20

Applesauce Jul-02 Dec-02

Applesauce Jan-06 Dec-06

Applesauce Oct-16 Sep-17

Asparagus, Canned Jul-03 Dec-03

Beans, Canned (4 varieties) 

2 Oct-08 Sep-10

Beets, Canned Jan-11 Dec-11

Blueberries (cultivated), Frozen 

3 Jan-07 Dec-08

Blueberries (cultivated/wild), Frozen 

3 Jan-14 Dec-14

Blueberries (cultivated/wild), Frozen 

3 Oct-20 Sep-22

Cherries, Frozen 

4 Apr-14 Mar-16

Corn Syrup 

4 Jan-98 Jun-99

Cranberries, Canned Apr-18 Sep-18

Cranberries, Frozen 

3 Oct-16 Mar-18

Garbanzo Beans, Canned Oct-17 Sep-18

Garbanzo Beans, Dried Jan-19 Dec-19

Grape Juice Jan-98 Dec-99

Grape Juice Jan-08 Dec-08

Grape Juice Oct-13 Sep-14

Grape Juice Jan-21 Dec-21

Green Beans, Canned/Frozen 

1 Jan-96 Jun-98

Green Beans, Canned Jan-03 Mar-04

Green Beans, Frozen Apr-05 Dec-05

Green Beans, Canned/Frozen Jan-14 Dec-14

Olives, Canned Oct-16 Sep-18

Orange Juice Jan-97 Dec-98

Orange Juice Oct-04 Sep-06

Orange Juice Oct-10 Sep-11

Orange Juice Jan-12 Jun-12

Orange Juice Oct-19 Sep-20

Peaches, Canned Dec-96 Dec-97

Peaches, Canned Jan-03 Dec-04

Peaches, Canned Jan-18 Dec-18

Peaches, Canned (T-1) Jan-03 Mar-03

Peaches, Canned (T-1) Oct-03 Dec-03

Peaches, Frozen 3, 5 Jan-21 Dec-22

Pear Juice, Concentrate/Puree Jul-02 Jun-03

Pears, Canned Jul-99 Jun-00

Peas, Canned/Frozen Apr-94 Jun-96

Peas, Canned/Frozen 

6 Oct-01 Sep-03

Peas, Canned/Frozen Oct-18 Sep-19

Peas, Frozen Jan-06 Dec-06

Appendix A. Page 6 of 11
Commodity Start Date End Date

Pineapple, Canned Jan-17 Dec-17

Plums, Dried (Prunes) 7 Jan-05 Dec-06

Plums, Dried (Prunes) Oct-17 Sep-18

Potatoes, Frozen Jan-06 Dec-07

Raisins Jul-06 Jun-07

Raisins Jan-18 Dec-18

Raspberries, Frozen 3 Jan-13 Dec-13

Spinach, Canned Oct-97 Dec-98

Spinach, Canned Jan-04 Jun-04

Spinach, Canned/Frozen Jul-10 Jun-11

Spinach, Canned/Frozen Oct-18 Sep-19

Spinach, Frozen Jan-99 Dec-99

Strawberries, Frozen 3 Jan-98 Sep-00

Strawberries, Frozen Oct-18 Sep-19

Sweet Corn, Canned/Frozen Apr-94 Mar-96

Sweet Corn, Canned/Frozen 6 Oct-01 Sep-03

Sweet Corn, Frozen 3 Oct-08 Sep-10

Sweet Corn, Frozen 3 Oct-14 Sep-15

Tomato Paste, Canned Jan-01 Jun-01

Tomato Paste, Canned Jan-09 Dec-09

Tomato Paste, Canned Oct-19 Sep-20

Tomatoes, Canned Jul-99 Jun-00

Tomatoes, Canned Oct-16 Sep-17

Winter Squash, Frozen 3 Jan-97 Jun-99

Baby Food / Formula Products

Commodity Start Date End Date

Baby Food, Applesauce Jul-12 Jun-13

Baby Food, Carrots Jan-12 Dec-12

Baby Food, Green Beans Oct-10 Sep-11

Baby Food, Green Beans Oct-22 Ongoing

Baby Food, Peaches Jan-12 Dec-12

Baby Food, Peaches Oct-22 Ongoing

Baby Food, Pears Oct-10 Sep-11

Baby Food, Pears Oct-22 Ongoing

Baby Food, Peas Jul-12 Jun-13

Baby Food, Sweet Potatoes Oct-10 Sep-11

Baby Food, Sweet Potatoes Oct-22 Ongoing

Infant Formula, Dairy-Based Oct-13 Sep-14

Infant Formula, Soy-Based Oct-13 Sep-14

NOTES

1 Excludes sampling hiatus September - November 1996.

2 Bean varieties included black, garbanzo, kidney, and pinto.

3 Frozen collected when fresh unavailable.

Appendix A. Page 7 of 11
4 Excludes sampling hiatus January 1999.

5

 2021 samples that were delayed and held frozen for >90 days (due to COVID-19 pandemic

 related delays) are annotated in the downloadable/searchable PDP data set.

6 Canned samples collected in first year and frozen samples in second year of testing.

7 Dried plums (prunes) were collected when fresh plums were not available.

(T-1) Triazole parent and metabolite compounds only.

Appendix A. Page 8 of 11
Grains

Commodity Start Date End Date

Barley Oct-01 Sep-03

Corn Oct-06 Sep-08

Corn 1 Jul-21 Ongoing

Oats Jul-99 Apr-00

Oats Jan-10 Jun-10

Oats Apr-14 Aug-14

Oats Jan-19 Dec-19

Rice Oct-00 Sep-02

Rice 2 Oct-08 Sep-09

Rice Apr-14 Aug-14

Rice Oct-18 Sep-19

Soybeans Sep-96 Feb-98

Soybeans Oct-03 Sep-05

Soybeans Sep-10 Apr-11

Soybeans (S-1) Oct-05 Dec-05

Wheat Feb-95 Jan-98

Wheat Sep-04 Jun-06

Wheat Jul-12 Sep-12

Wheat Flour Jan-03 Dec-04

Wheat Flour Jan-18 Dec-18

Wheat Flour (T-1) Jan-03 Dec-03

Nuts and Nut Products

Commodity Start Date End Date

Almonds Jul-07 Mar-08

Peanut Butter Jan-00 Dec-00

Peanut Butter (TSP) Jul-03 Dec-03

Peanut Butter Jan-06 Dec-06

Peanut Butter Apr-15 Aug-15

Peanut Butter Jan-22 Dec-22

Dairy Products

Commodity Start Date End Date

Butter Jan-03 Dec-03

Butter Jan-12 Dec-13

Butter Oct-21 Sep-22

Heavy Cream Jul-05 Dec-05

Heavy Cream Jan-07 Dec-07

Heavy Cream Jun-18 Aug-18

Milk 3 Jan-96 Oct-98

Milk (TSP) Jul-03 Dec-03

Milk Jan-04 Dec-05

Milk Jan-11 Dec-11

Milk Jan-16 Dec-17

Appendix A. Page 9 of 11
Fish Products

Commodity Type Start Date End Date

Fish 4 Catfish Apr-08 Jun-10

Fish Salmon Jul-13 Jun-14

Meat / Poultry / Pork Products

Commodity Type Start Date End Date

Poultry Young Chickens Apr-00 Mar-01

Poultry Young & Mature Chickens Jan-06 Dec-06

Beef Cows, Heifers, Steers Jun-01 Jul-02

Beef 5 Cows, Heifers, Steers Dec-08 May-09

Pork Gilt, Barrow Jan-05 Jun-05

Other Products

Commodity Start Date End Date

Eggs (TSP) Jul-03 Dec-03

Eggs Jul-10 Jun-11

Eggs Apr-16 Aug-16

Honey Oct-07 Sep-08

Honey Apr-17 Aug-17

Drinking Water

States Start Date End Date

Finished Water Only (27 sites)

California, Colorado, Kansas, New York, Texas Mar-01 Dec-03

Raw Intake and Finished Water (70 sites) Jan-04 Apr-13

Alabama, Arizona, California, Florida, Georgia, Illinois, Indiana, Iowa, Kansas,

Kentucky, Louisiana, Maryland, Michigan, Minnesota, Missouri, Montana, New Jersey, 

New York, North Carolina, North Dakota, Ohio, Oregon, Pennsylvania, South Carolina, 

Tennessee, Texas, Virginia, Washington State, and Washington, D.C.

Bottled Water 

10 Participating States Jan-05 Dec-06

10 Participating States Jan-17 Dec-17

Groundwater 

1,495 Private Wells in 45 States plus Washington, DC Jan-07 Feb-13

16 Municipal Water Facilities in 13 States Mar-10 Feb-13

Appendix A. Page 10 of 11
NOTES

1

 2021 samples that were delayed and held frozen for >90 days (due to COVID-19 pandemic

 related delays) are annotated in the downloadable/searchable PDP data set.

2

 Includes sampling hiatus May-July 2009.

3

 Excludes sampling hiatus September - November 1996.

4 Excludes sampling hiatus April-June 2009.

5

 Survey ended 7 months early due to budgetary constraints.

(S-1) Special survey for fungicides used to combat soybean rust.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 11 of 11
Appendix B

Distribution of Residues by Pesticide

in Fruit and Vegetables

Appendix B shows residue detections for all fruit and vegetable pesticide/commodity pairs 

tested, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerances for each pair. The EPA tolerances cited in 

this summary and appendixes apply to 2021 and not to the current year. There may be 

instances where tolerances have been recently set, modified, or revoked that would have an 

effect on whether a residue is violative or not.

In 2021, the Pesticide Data Program (PDP) analyzed 9,532 fruit and vegetable samples, of 

which 8,664 were fresh products and 868 were processed products. 

PDP reports tolerance violations to FDA as part of an interagency Memorandum of 

Understanding between the U.S. Department of Agriculture and FDA. Residues reported to 

FDA are shown in the “Tolerance Violation” column and are annotated as “X” (if the residue 

exceeded the established tolerance) or “V” (if the residue did not have a tolerance listed in the 

Code of Federal Regulations, Title 40, Part 180). In both cases, these annotations are followed 

by a number indicating the number of samples reported to FDA. 

Results for environmental contaminants across all commodities, including fruit and vegetables, 

have been consolidated in a separate appendix because they have no registered uses and are 

not applied to crops (see Appendix E). 
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

2,3,5-Trimethacarb (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

2,6-DIPN (plant growth regulator) 

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 1,771 0

Abamectin (insecticide)

Blueberries, Cultivated, Fresh 664 0 0.050 0.05

Blueberries, Frozen 14 0 0.050 0.05

Cantaloupe 328 0 0.050 0.01 FF

Grape Juice 700 0 0.004 0.02

Green Beans 700 0 0.020 0.08

Pears 707 1 0.1 0.007 0.004 0.02

Plums 277 0 0.050 0.09

Summer Squash 365 0 0.020 0.01 FF

Winter Squash 706 0 0.020 0.01 FF

TOTAL 4,461 1

Acephate (insecticide)

Blueberries, Cultivated, Fresh 692 0 0.003 0.02 FF

Blueberries, Frozen 14 0 0.003 0.02 FF

Cantaloupe 328 0 0.003 0.02 FF

Carrots 708 0 0.075 0.02 FF

Cauliflower 531 8 1.5 0.011 - 0.14 0.005 2.0

Celery 354 26 7.3 0.056 - 1.2 0.050 10

Eggplant 703 3 0.4 0.084 - 0.32 0.005 - 0.075 X-3 0.02 FF

Grape Juice 700 0 0.10 0.02 FF

Green Beans 700 44 6.3 0.006 - 10 0.005 X-28 0.02 FF

Peaches 518 0 0.050 0.02 FF

Peaches, Frozen 154 0 0.050 0.02 FF

Pears 707 0 0.10 0.02 FF

Plums 277 0 0.003 0.02 FF

Summer Squash 698 0 0.005 - 0.015 0.02 FF

Sweet Bell Peppers 319 2 0.6 0.18 - 0.20 0.050 4.0

Tangerines 531 0 0.060 0.02 FF

Watermelon 175 0 0.015 0.02 FF

Winter Squash 706 4 0.6 0.030 - 0.30 0.005 X-4 0.02 FF

TOTAL 8,815 87

Acequinocyl (acaricide) 

Carrots 708 0 0.20 NT

TOTAL 708 0

Acetamiprid (insecticide) 

Blueberries, Cultivated, Fresh 692 213 30.8 0.002 - 2.0 0.002 X-2 1.6

Blueberries, Frozen 14 6 42.9 0.005 - 0.044 0.002 1.6

Broccoli 708 3 0.4 0.002 - 0.005 0.001 - 0.003 1.2

Cantaloupe 328 74 22.6 0.002 - 0.025 0.002 0.50

Carrots 708 0 0.005 0.01

APPENDIX B. DISTRIBUTION OF RESIDUES BY PESTICIDE IN FRUIT AND VEGETABLES

Appendix B. Page 1 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cauliflower 531 0 0.003 1.2

Celery 354 8 2.3 0.011 - 0.048 0.010 3

Eggplant 703 102 14.5 0.002 - 0.14 0.001 - 0.005 0.20

Grape Juice 700 0 0.007 0.35

Green Beans 700 23 3.3 0.001 - 0.037 0.001 0.60

Peaches 518 97 18.7 0.010 - 0.20 0.010 1.5

Peaches, Frozen 154 1 0.6 0.083 0.010 1.5

Pears 707 178 25.2 0.012 - 0.70 0.007 1.0

Plums 277 8 2.9 0.002 - 0.012 0.002 1.5

Summer Squash 698 39 5.6 0.002 - 0.035 0.001 - 0.002 0.50

Sweet Bell Peppers 319 49 15.4 0.011 - 0.12 0.010 0.20

Tangerines 531 54 10.2 0.002 - 0.061 0.002 1.0

Watermelon 175 5 2.9 0.002 - 0.004 0.002 0.50

Winter Squash 706 79 11.2 0.001 - 0.010 0.001 0.50

TOTAL 9,523 939

Acetochlor (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 0 0.001 - 0.003 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.001 - 0.030 NT

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.030 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,771 0

Acibenzolar S methyl (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.020 0.15

Blueberries, Frozen 14 0 0.020 0.15

Broccoli 708 0 0.004 1.0

Cantaloupe 328 0 0.020 2.0

Carrots 708 0 0.040 NT

Cauliflower 531 0 0.004 - 0.012 1.0

Celery 354 0 0.010 0.25

Eggplant 703 0 0.004 - 0.040 1.0

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.015 0.05 IT

Plums 247 0 0.020 NT

Summer Squash 333 0 0.030 2.0

Sweet Bell Peppers 319 0 0.010 1.0

Tangerines 531 0 0.030 0.02

Watermelon 175 0 0.030 2.0

TOTAL 7,022 0

Aclonifen (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Appendix B. Page 2 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Afidopyropen (insecticide) 

Broccoli 708 2 0.3 0.002 0.001 0.50

Cauliflower 531 0 0.001 - 0.003 0.50

Eggplant 357 1 0.3 0.004 0.001 0.2

Pears 707 0 0.005 0.02

Summer Squash 333 0 0.010 0.70

Tangerines 531 0 0.010 0.15

Watermelon 175 0 0.010 0.70

TOTAL 3,342 3

Alachlor (herbicide) 

Broccoli 708 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 NT

Eggplant 703 0 0.002 - 0.010 NT

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.020 NT

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,460 0

Aldicarb (insecticide) 

Blueberries, Cultivated, Fresh 393 0 0.030 NT

Blueberries, Frozen 9 0 0.030 NT

Broccoli 708 0 0.001 - 0.003 NT

Cantaloupe 73 0 0.030 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.020 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 100 0 0.030 NT

Summer Squash 698 0 0.002 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.005 NT

TOTAL 7,380 0

Aldicarb sulfone (metabolite of Aldicarb)

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.025 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.003 - 0.025 NT

Green Beans 700 0 0.003 NT

Peaches 500 0 0.010 NT

Peaches, Frozen 152 0 0.010 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.003 - 0.010 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.020 NT

Appendix B. Page 3 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 7,388 0

Aldicarb sulfoxide (metabolite of Aldicarb)

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.055 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.002 - 0.055 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.005 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 5,838 0

Allethrin (insecticide) 

Carrots 708 0 0.080 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.080 NT

Peaches 518 0 0.010 - 0.025 NT

Peaches, Frozen 154 0 0.010 NT

Sweet Bell Peppers 319 0 0.010 - 0.025 NT

TOTAL 2,399 0

Allidochlor (herbicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Ametoctradin (fungicide) 

Broccoli 708 3 0.4 0.005 - 0.034 0.003 9.0

Carrots 708 0 0.010 NT

Cauliflower 531 8 1.5 0.002 0.001 9.0

Celery 354 0 0.010 40.0

Eggplant 703 1 0.1 0.008 0.003 - 0.010 1.5

Grape Juice 700 0 0.001 4.0

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 1 0.3 0.006 0.001 3.0

Sweet Bell Peppers 319 1 0.3 0.012 0.010 1.5

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 3.0

Winter Squash 706 25 3.5 0.001 - 0.072 0.001 3.0

TOTAL 7,172 39

Ametryn (herbicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 NT

Green Beans 700 1 0.1 0.004 0.001 V-1 NT

Appendix B. Page 4 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,209 1

Amicarbazone (herbicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Aminocarb (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Amisulbrom (fungicide) 

Grape Juice 700 0 0.005 0.40

TOTAL 700 0

Anilofos (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Aspon (insecticide) 

Celery 354 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

TOTAL 1,354 0

Asulam (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Atraton (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Atrazine (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 1 0.1 0.002 0.001 - 0.003 V-1 NT

Cantaloupe 299 0 0.002 NT

Carrots 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Appendix B. Page 5 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Celery 354 0 0.005 0.25 IN

Eggplant 703 0 0.001 NT

Green Beans 700 14 2 0.001 - 0.010 0.001 V-14 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.002 NT

Summer Squash 698 0 0.001 - 0.010 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,096 15

Azaconazole (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Azamethiphos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Azimsulfuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Azinphos (insecticide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Azinphos methyl (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.006 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.006 NT

Celery 354 0 0.020 NT

Eggplant 703 0 0.005 - 0.006 NT

Grape Juice 700 0 0.008 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.020 NT

Peaches, Frozen 154 0 0.020 NT

Pears 707 0 0.008 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.005 - 0.010 NT

Sweet Bell Peppers 328 0 0.020 NT

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.005 NT

TOTAL 9,532 0

Appendix B. Page 6 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Azinphos methyl oxygen analog (metabolite of Azinphos methyl)

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.010 NT

Grape Juice 700 0 0.005 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 6,888 0

Azoxystrobin (fungicide) 

Blueberries, Cultivated, Fresh 692 190 27.5 0.002 - 0.72 0.002 10.0

Blueberries, Frozen 14 3 21.4 0.006 - 0.083 0.002 10.0

Broccoli 708 76 10.7 0.002 - 0.48 0.001 3.0

Cantaloupe 328 8 2.4 0.002 - 0.003 0.002 0.3

Carrots 708 40 5.6 0.010 - 0.034 0.010 1.0

Cauliflower 531 2 0.4 0.002 0.001 3.0

Celery 354 70 19.8 0.002 - 0.14 0.002 30.0

Eggplant 703 32 4.6 0.002 - 0.028 0.001 - 0.010 3.0

Grape Juice 700 252 36 0.002 - 0.005 0.001 2.0

Green Beans 700 196 28 0.001 - 0.58 0.001 3.0

Peaches 518 75 14.5 0.002 - 0.091 0.002 2.0

Peaches, Frozen 154 2 1.3 0.002 0.002 2.0

Pears 707 0 0.001 NT

Plums 277 3 1.1 0.005 - 0.026 0.002 2.0

Summer Squash 698 40 5.7 0.001 - 0.026 0.001 0.3

Sweet Bell Peppers 319 54 16.9 0.002 - 0.10 0.002 3.0

Tangerines 531 161 30.3 0.002 - 0.24 0.002 15.0

Watermelon 175 1 0.6 0.001 0.001 0.3

Winter Squash 706 17 2.4 0.001 - 0.021 0.001 0.3

TOTAL 9,523 1,222

Beflubutamid (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Benalaxyl (fungicide) 

Grape Juice 700 0 0.003 3.0 FU

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,471 0

Bendiocarb (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.003 NT

Blueberries, Frozen 14 0 0.003 NT

Appendix B. Page 7 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.003 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.003 NT

Summer Squash 698 0 0.001 - 0.002 NT

Sweet Bell Peppers 319 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,816 0

Benfluralin (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Green Beans 700 0 0.003 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,082 0

Benoxacor (herbicide safener) 

Blueberries, Cultivated, Fresh 692 0 0.010 0.01

Blueberries, Frozen 14 0 0.010 0.01

Broccoli 708 0 0.001 0.01

Cantaloupe 328 0 0.010 0.01

Carrots 708 0 0.015 0.01

Cauliflower 531 0 0.001 0.01

Celery 354 0 0.005 0.01

Eggplant 703 0 0.001 - 0.015 0.01

Green Beans 700 0 0.003 0.01

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.003 - 0.020 0.01

Sweet Bell Peppers 328 0 0.005 0.01

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 0.01

Winter Squash 706 0 0.003 0.01

TOTAL 8,125 0

Bensulfuron methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Bensulide (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.004 NT

Blueberries, Frozen 14 0 0.004 NT

Appendix B. Page 8 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.004 0.15

Carrots 708 0 0.005 0.10 R

Celery 354 0 0.010 0.15

Eggplant 346 0 0.005 0.10

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.004 NT

Summer Squash 698 0 0.001 - 0.010 0.15

Sweet Bell Peppers 319 0 0.010 0.10

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.010 0.15

Winter Squash 706 1 0.1 0.002 0.001 0.15

TOTAL 6,520 1

Bensulide oxygen analog (metabolite of Bensulide)

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Cantaloupe 328 0 0.002 0.15

Carrots 708 0 0.010 0.10 R

Eggplant 346 0 0.010 0.10

Plums 277 0 0.002 NT

Summer Squash 333 0 0.002 0.15

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.002 0.15

TOTAL 3,404 0

Bentazon (herbicide) 

Carrots 708 0 0.030 NT

Eggplant 346 0 0.030 NT

Summer Squash 333 0 0.050 NT

Tangerines 531 0 0.10 NT

Watermelon 175 0 0.050 NT

TOTAL 2,093 0

Benthiavalicarb isopropyl (fungicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Grape Juice 700 0 0.002 0.25 FU

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,525 0

Benzobicyclon (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Benzovindiflupyr (fungicide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 1.5

Grape Juice 700 0 0.002 1.0

Green Beans 700 1 0.1 0.002 0.001 V-1 NT

Pears 707 0 0.002 0.20

Summer Squash 698 2 0.3 0.002 - 0.007 0.001 - 0.005 0.30

Appendix B. Page 9 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.30

Winter Squash 706 8 1.1 0.002 - 0.006 0.001 0.30

TOTAL 5,271 11

Bifenazate (acaricide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 4.0

Grape Juice 700 0 0.005 1.0

Green Beans 700 0 0.003 6.0

Peaches 518 21 4.1 0.010 - 0.16 0.010 2.5

Peaches, Frozen 154 0 0.010 2.5

Pears 707 37 5.2 0.008 - 0.046 0.005 0.7

Summer Squash 365 0 0.003 0.75

Sweet Bell Peppers 319 5 1.6 0.012 - 0.035 0.010 4.0

Winter Squash 706 0 0.003 0.75

TOTAL 5,577 63

Bifenox (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Bifenthrin (insecticide) 

Blueberries, Cultivated, Fresh 692 113 16.3 0.002 - 0.71 0.002 3

Blueberries, Frozen 14 6 42.9 0.037 - 0.47 0.002 3

Broccoli 708 22 3.1 0.002 - 0.038 0.001 0.6

Cantaloupe 328 11 3.4 0.002 - 0.004 0.002 0.4

Carrots 708 0 0.005 0.10

Cauliflower 531 0 0.001 0.6

Celery 354 23 6.5 0.005 - 0.16 0.005 3.0

Eggplant 703 44 6.3 0.002 - 0.041 0.001 - 0.005 0.5

Grape Juice 700 0 0.003 0.3

Green Beans 700 180 25.7 0.001 - 0.15 0.001 0.6

Peaches 518 2 0.4 0.005 - 0.020 0.005 0.7

Peaches, Frozen 154 0 0.005 0.7

Pears 707 4 0.6 0.005 - 0.16 0.003 0.9

Plums 277 0 0.002 0.05 FF

Summer Squash 698 36 5.2 0.002 - 0.033 0.001 - 0.005 0.4

Sweet Bell Peppers 328 39 11.9 0.005 - 0.12 0.005 0.5

Tangerines 531 0 0.005 0.05

Watermelon 175 5 2.9 0.007 - 0.027 0.005 0.4

Winter Squash 706 140 19.8 0.001 - 0.14 0.001 0.4

TOTAL 9,532 625

Biphenyl (fungicide) 

Carrots 708 0 0.075 NT

Eggplant 346 0 0.075 NT

TOTAL 1,054 0

Bitertanol (fungicide) 

Celery 354 0 0.010 NT

Green Beans 700 0 0.010 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Appendix B. Page 10 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 365 0 0.010 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 3,116 0

Boscalid (fungicide) 

Blueberries, Cultivated, Fresh 692 286 41.3 0.004 - 2.1 0.003 13.0

Blueberries, Frozen 14 8 57.1 0.009 - 0.51 0.003 13.0

Broccoli 708 51 7.2 0.002 - 0.86 0.001 6.0

Cantaloupe 328 0 0.003 3.0

Carrots 708 129 18.2 0.020 - 0.12 0.020 2.0

Cauliflower 531 4 0.8 0.002 0.001 6.0

Celery 354 25 7.1 0.010 - 0.24 0.010 45

Eggplant 703 11 1.6 0.002 - 0.020 0.001 - 0.010 3.0

Grape Juice 700 46 6.6 0.008 - 0.11 0.005 5.0

Green Beans 700 77 11 0.003 - 0.23 0.003 5.0

Peaches 518 60 11.6 0.014 - 0.43 0.010 3.5

Peaches, Frozen 154 0 0.010 3.5

Pears 707 21 3 0.008 - 0.16 0.005 3.0

Plums 277 9 3.2 0.003 - 0.011 0.003 3.5

Summer Squash 698 8 1.1 0.003 - 0.030 0.003 - 0.005 3.0

Sweet Bell Peppers 319 31 9.7 0.012 - 0.22 0.010 3.0

Tangerines 531 0 0.005 2.0

Watermelon 175 0 0.005 3.0

Winter Squash 706 26 3.7 0.003 - 0.018 0.003 3.0

TOTAL 9,523 792

Bromacil (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.003 NT

Blueberries, Frozen 14 0 0.003 NT

Cantaloupe 328 0 0.003 NT

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.003 NT

Plums 277 0 0.003 NT

Summer Squash 698 0 0.003 - 0.010 NT

Tangerines 531 0 0.010 0.1

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 5,175 0

Bromobutide (herbicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Bromophos ethyl (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Bromopropylate (acaricide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Appendix B. Page 11 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums 246 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,371 0

Bromuconazole (fungicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Bupirimate (fungicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Buprofezin (insecticide) 

Blueberries, Cultivated, Fresh 662 18 2.7 0.001 - 0.008 0.001 2.5

Blueberries, Frozen 14 0 0.001 2.5

Broccoli 708 0 0.001 12

Cantaloupe 298 0 0.001 0.50

Carrots 708 0 0.001 NT

Cauliflower 531 0 0.001 12

Celery 354 0 0.010 35

Eggplant 703 4 0.6 0.002 - 0.005 0.001 2.0

Grape Juice 700 0 0.001 2.5 IT

Green Beans 700 20 2.9 0.002 - 0.074 0.001 X-3 0.02

Peaches 518 1 0.2 0.028 0.010 9.0

Peaches, Frozen 154 0 0.010 9.0

Pears 707 125 17.7 0.002 - 0.83 0.001 6.0

Plums 277 8 2.9 0.001 - 0.004 0.001 2

Summer Squash 698 6 0.9 0.001 - 0.007 0.001 0.50

Sweet Bell Peppers 319 6 1.9 0.012 - 0.064 0.010 2.0

Tangerines 531 0 0.001 4

Watermelon 175 4 2.3 0.001 0.001 0.50

Winter Squash 706 7 1 0.002 - 0.008 0.001 0.50

TOTAL 9,463 199

Butachlor (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Butocarboxim (insecticide, acaricide)

Carrots 708 0 0.020 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.020 NT

Peaches 518 0 0.010 NT

Appendix B. Page 12 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.010 NT

Sweet Bell Peppers 319 0 0.010 NT

TOTAL 2,399 0

Butocarboxim sulfone (metabolite of Butocarboxim)

Carrots 708 0 0.015 NT

Eggplant 346 0 0.015 NT

TOTAL 1,054 0

Butocarboxim sulfoxide (metabolite of Butocarboxim)

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

TOTAL 1,054 0

Butralin (herbicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Butylate (herbicide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Cadusafos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Captan (fungicide) (parent of THPI)

Cantaloupe 241 0 0.025 0.05

Carrots 708 0 0.10 - 0.20 0.05

Celery 354 0 0.020 0.05

Eggplant 346 0 0.10 - 0.20 0.05

Peaches 518 36 6.9 0.023 - 1.1 0.020 15.0

Peaches, Frozen 154 0 0.020 15.0

Sweet Bell Peppers 328 0 0.020 0.05

TOTAL 2,649 36

Carbaryl (insecticide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.010 0.007 3.0

Blueberries, Frozen 14 0 0.007 3.0

Broccoli 708 1 0.1 0.17 0.003 10

Cantaloupe 328 0 0.003 3.0

Carrots 708 0 0.005 2.0

Cauliflower 531 1 0.2 0.002 0.001 10

Celery 354 22 6.2 0.012 - 0.44 0.010 3.0

Eggplant 703 21 3 0.002 - 0.65 0.001 - 0.005 5.0

Grape Juice 700 71 10.1 0.008 - 0.048 0.005 10

Green Beans 700 2 0.3 0.026 - 0.18 0.003 10

Peaches 518 2 0.4 0.049 - 0.94 0.010 10

Peaches, Frozen 154 0 0.010 10

Pears 707 0 0.005 12

Appendix B. Page 13 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums 277 0 0.003 10

Summer Squash 698 0 0.002 - 0.003 3.0

Sweet Bell Peppers 319 6 1.9 0.018 - 0.097 0.010 5.0

Tangerines 531 0 0.005 10

Watermelon 175 0 0.002 3.0

Winter Squash 706 0 0.003 3.0

TOTAL 9,523 127

Carbendazim - MBC (fungicide) (metabolite of Benomyl and Thiophanate Methyl)

Blueberries, Cultivated, Fresh 692 9 1.3 0.001 - 0.018 0.001 V-9 NT

Blueberries, Frozen 14 0 0.001 NT

Broccoli 708 3 0.4 0.004 - 0.014 0.003 V-3 NT

Cantaloupe 328 3 0.9 0.001 - 0.031 0.001 1.0 TP

Carrots 708 1 0.1 0.018 0.010 V-1 NT

Cauliflower 531 1 0.2 0.002 0.001 V-1 NT

Celery 354 0 0.010 NT

Eggplant 346 1 0.3 0.012 0.010 V-1 NT

Grape Juice 700 1 0.1 0.008 0.005 5.0 TP

Green Beans 700 234 33.4 0.001 - 0.26 0.001 2.0 TP

Peaches 518 2 0.4 0.013 - 0.13 0.010 3.0 TP

Peaches, Frozen 154 1 0.6 0.022 0.010 3.0 TP

Pears 707 217 30.7 0.008 - 0.20 0.005 3.0 TP

Plums 277 1 0.4 0.002 0.001 0.5 TP

Summer Squash 698 5 0.7 0.001 - 0.020 0.001 - 0.010 1.0 TP

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.050 NT

Watermelon 175 5 2.9 0.013 - 0.060 0.010 1.0 TP

Winter Squash 639 13 2 0.001 - 0.015 0.001 1.0 TP

TOTAL 9,099 497

Carbofuran (insecticide) (parent of 3-Hydroxycarbofuran)

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.005 NT

Plums 277 0 0.002 NT

Summer Squash 698 0 0.001 - 0.002 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 9,523 0

Carbophenothion (insecticide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Appendix B. Page 14 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carboxin (fungicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.003 0.2

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 668 0 0.003 - 0.025 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.025 NT

Watermelon 175 0 0.025 NT

Winter Squash 706 0 0.003 NT

TOTAL 5,188 0

Carfentrazone (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 0.10

Blueberries, Frozen 14 0 0.005 0.10

Broccoli 708 0 0.005 - 0.030 0.10

Cantaloupe 328 0 0.005 0.10

Carrots 708 0 0.020 0.10

Cauliflower 493 0 0.005 - 0.030 0.10

Celery 354 0 0.005 0.10

Eggplant 703 0 0.005 - 0.020 0.10

Grape Juice 700 0 0.006 0.10

Green Beans 700 0 0.003 0.10

Peaches 518 0 0.005 0.10

Peaches, Frozen 154 0 0.005 0.10

Pears 707 0 0.006 0.10

Plums 277 0 0.005 0.10

Summer Squash 698 0 0.003 - 0.005 0.10

Sweet Bell Peppers 328 0 0.005 0.10

Tangerines 531 0 0.005 0.10

Watermelon 175 0 0.005 0.10

Winter Squash 706 0 0.003 0.10

TOTAL 9,494 0

Carpropamid (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorantraniliprole (insecticide) 

Blueberries, Cultivated, Fresh 692 13 1.9 0.011 - 0.11 0.010 2.5

Blueberries, Frozen 14 0 0.010 2.5

Broccoli 708 16 2.3 0.006 - 0.19 0.005 4.0

Cantaloupe 328 0 0.010 0.5

Carrots 708 0 0.020 0.30

Cauliflower 531 1 0.2 0.005 0.002 4.0

Celery 354 24 6.8 0.021 - 0.16 0.020 13

Eggplant 703 17 2.4 0.003 - 0.010 0.002 - 0.020 1.4

Grape Juice 700 14 2 0.007 0.004 2.5

Green Beans 700 46 6.6 0.005 - 0.048 0.005 2.0

Peaches 518 53 10.2 0.020 - 0.081 0.020 4.0 IT

Peaches, Frozen 154 0 0.020 4.0 IT

Pears 707 256 36.2 0.007 - 0.13 0.004 1.2

Appendix B. Page 15 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums 277 6 2.2 0.011 - 0.034 0.010 4.0 IT

Summer Squash 698 8 1.1 0.005 - 0.049 0.005 0.5

Sweet Bell Peppers 319 1 0.3 0.024 0.020 1.4

Tangerines 531 0 0.005 1.4

Watermelon 175 3 1.7 0.006 - 0.007 0.005 0.5

Winter Squash 706 14 2 0.005 - 0.024 0.005 0.5

TOTAL 9,523 472

Chlorbromuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlordimeform (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorethoxyfos (insecticide) 

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,810 0

Chlorfenapyr (insecticide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.041 0.015 X-1 0.01 FF

Blueberries, Frozen 14 0 0.015 0.01 FF

Broccoli 708 0 0.002 0.01 FF

Cantaloupe 328 0 0.015 0.01 FF

Carrots 708 0 0.020 0.01 FF

Cauliflower 531 0 0.002 0.01 FF

Celery 354 0 0.005 0.01 FF

Eggplant 703 23 3.3 0.004 - 0.18 0.002 - 0.020 2

Grape Juice 700 0 0.018 0.01 FF

Green Beans 700 0 0.010 0.01 FF

Peaches 518 0 0.005 0.01 FF

Peaches, Frozen 154 0 0.005 0.01 FF

Pears 707 0 0.018 0.01 FF

Plums 277 0 0.015 0.01 FF

Summer Squash 698 0 0.010 - 0.025 0.01 FF

Sweet Bell Peppers 328 45 13.7 0.005 - 0.16 0.005 2

Tangerines 531 0 0.025 0.01 FF

Watermelon 175 0 0.025 0.01 FF

Winter Squash 706 6 0.8 0.010 - 0.084 0.010 X-3 0.01 FF

TOTAL 9,532 75

Chlorfenvinphos (insecticide) 

Broccoli 708 0 0.002 - 0.005 NT

Cauliflower 531 0 0.002 - 0.005 NT

Celery 354 0 0.005 NT

Eggplant 357 0 0.002 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Appendix B. Page 16 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,721 0

Chlorfluazuron (insect growth regulator) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorimuron ethyl (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,810 0

Chlorobenzilate (acaricide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chloroneb (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorothalonil (fungicide) 

Blueberries, Cultivated, Fresh 692 3 0.4 0.029 - 0.099 0.020 1.0

Blueberries, Frozen 14 1 7.1 0.035 0.020 1.0

Cantaloupe 328 0 0.020 5.0

Celery 354 93 26.3 0.005 - 0.86 0.005 15

Green Beans 700 106 15.1 0.005 - 0.73 0.005 - 0.040 5

Peaches 518 1 0.2 0.010 0.005 0.5

Peaches, Frozen 154 0 0.005 0.5

Plums 277 0 0.020 0.2

Summer Squash 365 27 7.4 0.005 - 0.16 0.005 5.0

Sweet Bell Peppers 328 27 8.2 0.006 - 0.10 0.005 6.0

Winter Squash 706 85 12 0.005 - 0.43 0.005 - 0.020 5.0

TOTAL 4,436 343

Chlorotoluron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chloroxuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Appendix B. Page 17 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Chlorpropham (herbicide, growth regulator)

Blueberries, Cultivated, Fresh 692 0 0.020 NT

Blueberries, Frozen 14 0 0.020 NT

Broccoli 708 23 3.2 0.002 - 0.031 0.001 - 0.003 V-23 NT

Cantaloupe 328 0 0.020 NT

Carrots 708 0 0.010 NT

Cauliflower 531 10 1.9 0.002 - 0.006 0.001 - 0.003 V-10 NT

Celery 354 0 0.005 NT

Eggplant 703 5 0.7 0.002 - 0.004 0.001 - 0.010 V-5 NT

Green Beans 700 15 2.1 0.001 - 0.036 0.001 V-15 NT

Peaches 518 5 1 0.005 - 0.024 0.005 V-5 NT

Peaches, Frozen 154 0 0.005 NT

Plums 246 0 0.020 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 4 1.2 0.005 - 0.023 0.005 V-4 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 41 5.8 0.001 - 0.018 0.001 V-41 NT

TOTAL 8,094 103

Chlorpyrifos (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.005 0.1 FF

Blueberries, Frozen 14 0 0.005 0.1 FF

Broccoli 708 8 1.1 0.002 - 0.14 0.001 1.0

Cantaloupe 328 0 0.005 0.1 FF

Carrots 708 0 0.010 0.1 FF

Cauliflower 531 1 0.2 0.11 0.001 1.0

Celery 354 0 0.005 0.1 FF

Eggplant 703 2 0.3 0.011 - 0.034 0.001 - 0.010 0.1 FF

Grape Juice 700 0 0.010 0.1 FF

Green Beans 700 9 1.3 0.003 - 0.10 0.003 0.1 FF

Peaches 518 2 0.4 0.005 - 0.012 0.005 0.1 FF

Peaches, Frozen 154 0 0.005 0.1 FF

Pears 707 0 0.010 0.1 FF

Plums 277 0 0.005 0.1 FF

Summer Squash 698 2 0.3 0.003 - 0.006 0.003 - 0.015 0.1 FF

Sweet Bell Peppers 328 19 5.8 0.006 - 0.22 0.005 1.0

Tangerines 531 0 0.015 1.0

Watermelon 175 1 0.6 0.025 0.015 0.1 FF

Winter Squash 706 7 1 0.003 - 0.031 0.003 0.1 FF

TOTAL 9,532 51

Chlorpyrifos oxygen analog (metabolite of Chlorpyrifos)

Blueberries, Cultivated, Fresh 692 0 0.004 0.1 FF

Blueberries, Frozen 14 0 0.004 0.1 FF

Broccoli 708 0 0.001 - 0.003 1.0

Cantaloupe 328 1 0.3 0.003 0.002 0.1 FF

Carrots 708 0 0.005 0.1 FF

Cauliflower 513 0 0.001 1.0

Celery 354 0 0.010 0.1 FF

Eggplant 703 0 0.001 - 0.005 0.1 FF

Grape Juice 700 0 0.002 0.1 FF

Green Beans 700 0 0.001 0.1 FF

Peaches 518 0 0.010 0.1 FF

Peaches, Frozen 154 0 0.010 0.1 FF

Pears 707 0 0.002 0.1 FF

Appendix B. Page 18 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums 277 0 0.002 0.1 FF

Summer Squash 698 0 0.001 - 0.005 0.1 FF

Sweet Bell Peppers 319 0 0.010 1.0

Tangerines 531 0 0.005 1.0

Watermelon 175 0 0.005 0.1 FF

Winter Squash 706 0 0.001 0.1 FF

TOTAL 9,505 1

Chlorpyrifos methyl (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorpyrifos methyl oxygen analog (insecticide metabolite)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorsulfuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Chlorthiophos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Clethodim (herbicide) 

Carrots 708 0 0.035 1.0

Cauliflower 531 0 0.002 3.0

Celery 354 0 0.010 0.60

Eggplant 703 0 0.002 - 0.035 1.0

Green Beans 700 0 0.010 3.5

Peaches 518 0 0.010 0.20

Peaches, Frozen 154 0 0.010 0.20

Pears 707 0 0.005 0.20

Summer Squash 698 0 0.005 - 0.010 0.50

Sweet Bell Peppers 319 0 0.010 1.0

Tangerines 531 0 0.20 NT

Watermelon 175 0 0.005 2.0

Winter Squash 706 0 0.010 0.50

TOTAL 6,804 0

Clethodim 5-OH sulfone (herbicide metabolite)

Carrots 708 0 0.10 1.0

Eggplant 346 0 0.10 1.0

TOTAL 1,054 0

Clethodim sulfone (herbicide metabolite)

Carrots 708 0 0.040 1.0

Eggplant 346 0 0.040 1.0

TOTAL 1,054 0

Appendix B. Page 19 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Clethodim sulfoxide (herbicide metabolite)

Carrots 708 0 0.040 1.0

Eggplant 346 0 0.040 1.0

TOTAL 1,054 0

Clodinafop propargyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Clofentezine (insecticide) 

Carrots 708 0 0.040 - 0.080 NT

Eggplant 346 0 0.040 NT

Grape Juice 700 0 0.003 1.0

Green Beans 700 0 0.005 NT

Pears 707 4 0.6 0.005 - 0.012 0.003 0.50

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 4,232 4

Clomazone (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 0 0.002 0.10

Cantaloupe 328 0 0.005 0.05

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.002 0.10

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.020 NT

Green Beans 700 0 0.001 0.05

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.001 - 0.005 0.1 IT

Sweet Bell Peppers 328 0 0.005 0.05

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.05

Winter Squash 706 1 0.1 0.001 0.001 0.1 IT

TOTAL 8,125 1

Cloquintocet-mexyl (herbicide safener) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Cloransulam methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Clothianidin (insecticide) (also a metabolite of Thiamethoxam)

Blueberries, Cultivated, Fresh 692 2 0.3 0.013 - 0.018 0.010 0.30 TP

Blueberries, Frozen 14 0 0.010 0.30 TP

Appendix B. Page 20 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 37 5.2 0.006 - 0.031 0.005 4.5 TP

Cantaloupe 328 19 5.8 0.011 - 0.057 0.010 0.2 TP

Carrots 708 0 0.035 0.8

Cauliflower 531 13 2.4 0.003 - 0.009 0.002 4.5 TP

Celery 354 3 0.8 0.011 - 0.023 0.010 4.0 TP

Eggplant 703 55 7.8 0.003 - 0.049 0.002 - 0.035 0.25 TP

Grape Juice 700 0 0.020 0.60

Green Beans 700 17 2.4 0.002 - 0.14 0.001 X-2 0.02 TP

Peaches 518 38 7.3 0.010 - 0.062 0.010 0.80

Peaches, Frozen 154 0 0.010 0.80

Pears 707 11 1.6 0.033 0.020 1.0

Plums 277 0 0.010 0.5 TP

Summer Squash 698 34 4.9 0.001 - 0.007 0.001 - 0.025 0.2 TP

Sweet Bell Peppers 319 79 24.8 0.010 - 0.15 0.010 0.80

Tangerines 531 1 0.2 0.034 0.025 0.40 TP

Watermelon 175 3 1.7 0.025 - 0.038 0.025 0.2 TP

Winter Squash 706 19 2.7 0.001 - 0.010 0.001 0.2 TP

TOTAL 9,523 331

Coumaphos (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.002 - 0.005 NT

Cantaloupe 328 0 0.010 NT

Cauliflower 531 0 0.002 - 0.005 NT

Celery 354 0 0.005 NT

Eggplant 357 0 0.002 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,032 0

Coumaphos oxygen analog (metabolite of Coumaphos)

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.010 NT

Cauliflower 531 0 0.003 NT

Eggplant 357 0 0.003 NT

Green Beans 700 0 0.001 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,678 0

Crotoxyphos (insecticide, acaricide)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Appendix B. Page 21 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Crufomate (insecticide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Cumyluron (herbicide) 

Celery 354 0 0.010 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Sweet Bell Peppers 319 0 0.010 NT

TOTAL 1,345 0

Cyanazine (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Cyantraniliprole (insecticide) 

Broccoli 708 14 2 0.008 - 0.39 0.008 3.0

Carrots 708 0 0.15 0.40

Cauliflower 531 0 0.002 3.0

Eggplant 703 9 1.3 0.004 - 0.023 0.002 - 0.15 2.0

Grape Juice 700 0 0.015 NT

Green Beans 700 16 2.3 0.003 - 0.18 0.003 2.0

Pears 707 19 2.7 0.025 - 0.084 0.015 1.5

Summer Squash 698 4 0.6 0.005 - 0.015 0.003 - 0.005 0.70

Tangerines 531 0 0.005 0.70

Watermelon 175 0 0.005 0.70

Winter Squash 706 0 0.003 0.70

TOTAL 6,867 62

Cyazofamid (fungicide) 

Broccoli 708 0 0.006 1.5

Carrots 708 4 0.6 0.020 - 0.025 0.020 0.09

Cauliflower 531 0 0.006 1.5

Eggplant 703 1 0.1 0.010 0.006 - 0.020 0.9

Grape Juice 700 0 0.003 1.5 R

Green Beans 700 2 0.3 0.013 - 0.014 0.010 0.5

Summer Squash 698 2 0.3 0.013 - 0.020 0.010 0.10

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 0.10

Winter Squash 706 1 0.1 0.014 0.010 0.10

TOTAL 6,160 10

Cyclaniliprole (insecticide) 

Carrots 708 0 0.010 - 0.070 EX1

Eggplant 346 0 0.010 - 0.050 0.20

Pears 707 0 0.010 0.30

Summer Squash 333 0 0.010 0.15

Tangerines 531 0 0.010 0.4

Watermelon 175 0 0.010 0.15

TOTAL 2,800 0

Appendix B. Page 22 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cyflufenamid (fungicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 0.20

Grape Juice 700 0 0.003 0.15

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.003 0.06

Summer Squash 698 42 6 0.001 - 0.038 0.001 - 0.005 0.10

Sweet Bell Peppers 319 0 0.010 0.20

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.10

Winter Squash 706 86 12.2 0.001 - 0.051 0.001 0.10

TOTAL 6,616 128

Cyflumetofen (acaricide) 

Carrots 708 0 0.015 NT

Eggplant 346 2 0.6 0.018 - 0.029 0.015 2

Grape Juice 700 0 0.005 0.60

Green Beans 589 0 0.005 NT

Pears 707 45 6.4 0.008 - 0.073 0.005 0.30

Summer Squash 559 0 0.005 - 0.020 NT

Tangerines 439 0 0.10 0.30

Winter Squash 588 0 0.005 NT

TOTAL 4,636 47

Cyfluthrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.004 0.05 FF

Blueberries, Frozen 14 0 0.004 0.05 FF

Broccoli 708 1 0.1 0.012 0.008 - 0.025 2.5

Cantaloupe 328 0 0.004 0.1

Carrots 708 0 0.025 0.20

Cauliflower 531 0 0.008 - 0.025 2.5

Celery 354 1 0.3 0.008 0.005 6.0

Eggplant 636 0 0.025 0.5

Grape Juice 700 0 0.015 1.0

Green Beans 700 17 2.4 0.003 - 0.029 0.003 0.05 FF

Peaches 518 63 12.2 0.006 - 0.13 0.005 0.3

Peaches, Frozen 154 0 0.005 0.3

Pears 707 1 0.1 0.025 0.015 0.5

Plums 277 0 0.004 0.3

Summer Squash 698 2 0.3 0.004 - 0.005 0.003 - 0.050 0.1

Sweet Bell Peppers 328 19 5.8 0.005 - 0.044 0.005 0.50

Tangerines 531 0 0.050 0.2

Watermelon 175 1 0.6 0.063 0.050 0.1

Winter Squash 706 8 1.1 0.003 - 0.015 0.003 0.1

TOTAL 9,465 113

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (insecticide)

Blueberries, Cultivated, Fresh 692 1 0.1 0.005 0.005 0.01 FF

Blueberries, Frozen 14 0 0.005 0.01 FF

Broccoli 708 39 5.5 0.005 - 0.059 0.003 0.4

Cantaloupe 328 0 0.005 0.05

Carrots 708 0 0.015 0.01 FF

Cauliflower 531 0 0.003 0.4

Celery 354 2 0.6 0.009 - 0.037 0.008 X-1 0.01 FF

Appendix B. Page 23 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 703 0 0.003 - 0.015 0.20

Grape Juice 700 0 0.015 0.01 FF

Green Beans 700 112 16 0.003 - 0.056 0.003 0.20

Peaches 518 90 17.4 0.008 - 0.076 0.008 0.50

Peaches, Frozen 154 0 0.008 0.50

Pears 707 6 0.8 0.025 - 0.060 0.015 0.30

Plums 277 0 0.005 0.50

Summer Squash 698 12 1.7 0.003 - 0.013 0.003 - 0.005 0.05

Sweet Bell Peppers 328 24 7.3 0.008 - 0.11 0.008 0.20

Tangerines 531 0 0.005 0.01 FF

Watermelon 175 0 0.005 0.05

Winter Squash 706 10 1.4 0.003 - 0.008 0.003 0.05

TOTAL 9,532 296

Cymoxanil (fungicide)

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Cantaloupe 328 0 0.005 0.05

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.010 NT

Celery 354 0 0.010 6.0

Eggplant 703 0 0.010 - 0.020 0.2

Grape Juice 700 0 0.025 0.10 R

Green Beans 700 0 0.010 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.010 - 0.050 0.05

Sweet Bell Peppers 319 0 0.010 0.2

Tangerines 531 0 0.10 NT

Watermelon 175 0 0.050 0.05

Winter Squash 706 0 0.010 0.05

TOTAL 8,108 0

Cypermethrin (insecticide) 

Blueberries, Cultivated, Fresh 692 159 23 0.010 - 0.60 0.010 0.8

Blueberries, Frozen 14 7 50 0.017 - 0.14 0.010 0.8

Broccoli 708 16 2.3 0.037 - 2.5 0.022 X-1 2.0

Cantaloupe 328 0 0.010 0.2

Carrots 708 0 0.035 0.1

Cauliflower 531 0 0.022 2.0

Celery 354 8 2.3 0.010 - 0.070 0.010 10

Eggplant 703 3 0.4 0.043 - 0.091 0.022 - 0.075 0.2

Grape Juice 700 0 0.070 2

Green Beans 700 109 15.6 0.005 - 0.19 0.005 0.7

Peaches 518 7 1.4 0.013 - 0.19 0.010 2

Peaches, Frozen 154 0 0.010 2

Pears 707 0 0.070 2

Plums 277 0 0.010 2

Summer Squash 698 2 0.3 0.005 - 0.029 0.005 - 0.050 0.2

Sweet Bell Peppers 328 69 21 0.010 - 0.14 0.010 0.2

Tangerines 531 0 0.050 0.35 IT

Watermelon 175 0 0.050 0.2

Winter Squash 706 23 3.3 0.005 - 0.028 0.005 0.2

TOTAL 9,532 403

Appendix B. Page 24 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cyphenothrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.015 NT

Blueberries, Frozen 14 0 0.015 NT

Cantaloupe 328 0 0.015 NT

Carrots 708 0 0.060 NT

Celery 354 0 0.008 NT

Eggplant 346 0 0.060 NT

Grape Juice 700 0 0.050 NT

Green Beans 700 0 0.015 NT

Peaches 518 0 0.008 NT

Peaches, Frozen 154 0 0.008 NT

Pears 707 0 0.050 NT

Plums 277 0 0.015 NT

Summer Squash 662 0 0.015 - 0.050 NT

Sweet Bell Peppers 328 0 0.008 NT

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.050 NT

Winter Squash 672 0 0.015 NT

TOTAL 7,866 0

Cyprazine (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Cyproconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 2 0.3 0.002 - 0.004 0.001 V-2 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,136 2

Cyprodinil (fungicide) 

Blueberries, Cultivated, Fresh 692 211 30.5 0.005 - 1.6 0.005 5.0

Blueberries, Frozen 14 5 35.7 0.027 - 0.10 0.005 5.0

Broccoli 708 16 2.3 0.002 - 0.16 0.001 1.0

Cantaloupe 328 7 2.1 0.006 - 0.015 0.005 0.70

Carrots 708 0 0.015 0.75

Cauliflower 531 0 0.001 1.0

Celery 354 1 0.3 0.010 0.005 30

Eggplant 294 13 4.4 0.016 - 0.060 0.015 1.5

Grape Juice 700 0 0.003 3.0

Green Beans 700 0 0.003 0.6

Peaches 518 91 17.6 0.005 - 0.63 0.005 2.0

Peaches, Frozen 154 31 20.1 0.005 - 0.054 0.005 2.0

Pears 707 2 0.3 0.005 - 0.41 0.003 1.7

Plums 277 14 5.1 0.009 - 0.16 0.005 2.0

Summer Squash 698 8 1.1 0.003 - 0.030 0.003 - 0.005 0.70

Sweet Bell Peppers 328 9 2.7 0.009 - 0.12 0.005 1.5

Tangerines 531 0 0.005 NT

Appendix B. Page 25 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 8 4.6 0.005 - 0.022 0.005 0.70

Winter Squash 706 12 1.7 0.003 - 0.016 0.003 0.70

TOTAL 9,123 428

Cyprosulfamide (herbicide safener) 

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.005 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,156 0

Cyromazine (insect growth regulator) 

Carrots 708 0 0.10 NT

Eggplant 346 0 0.10 3

Green Beans 700 18 2.6 0.006 - 0.13 0.005 2.0

Summer Squash 698 2 0.3 0.005 - 0.026 0.005 - 0.050 1.0

Watermelon 147 0 0.050 1.0

Winter Squash 706 4 0.6 0.009 - 0.015 0.005 1.0

TOTAL 3,305 24

Daimuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

DCPA (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 236 33.3 0.002 - 0.078 0.001 5.0

Cantaloupe 328 0 0.002 1.0

Carrots 708 0 0.020 NT

Cauliflower 531 25 4.7 0.002 - 0.006 0.001 5.0

Celery 354 2 0.6 0.007 - 0.024 0.005 V-2 NT

Eggplant 703 0 0.001 - 0.020 1.0 IN

Green Beans 700 9 1.3 0.001 - 0.003 0.001 2.0 IN

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.002 NT

Summer Squash 698 2 0.3 0.002 - 0.003 0.001 - 0.005 1.0 IN

Sweet Bell Peppers 328 0 0.005 2.0 IN

Tangerines 531 0 0.005 NT

Watermelon 175 1 0.6 0.010 0.005 1.0

Winter Squash 706 2 0.3 0.002 0.001 1.0 IN

TOTAL 8,125 277

DEF - Tribufos (herbicide, plant growth regulator)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Deltamethrin (includes parent Tralomethrin) (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.015 0.05 FF

Blueberries, Frozen 14 0 0.015 0.05 FF

Appendix B. Page 26 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.012 0.05 FF

Cantaloupe 328 0 0.015 0.2

Carrots 708 0 0.070 0.2

Cauliflower 531 0 0.012 0.05 FF

Celery 354 0 0.008 0.05 FF

Eggplant 703 0 0.012 - 0.14 0.3

Grape Juice 700 0 0.020 0.05 FF

Green Beans 700 8 1.1 0.003 - 0.015 0.001 0.05 FF

Peaches 518 0 0.008 0.05 FF

Peaches, Frozen 154 0 0.008 0.05 FF

Pears 707 0 0.020 0.2

Plums 277 0 0.015 0.05 FF

Summer Squash 698 0 0.001 - 0.050 0.2

Sweet Bell Peppers 328 7 2.1 0.008 - 0.026 0.008 0.3

Tangerines 531 0 0.050 0.05 FF

Watermelon 175 0 0.050 0.2

Winter Squash 706 0 0.001 0.2

TOTAL 9,532 15

Demeton-O (metabolite of the insecticide Demeton)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Demeton-S (metabolite of Demeton)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Demeton-S methyl (insecticide metabolite)

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Demeton-S sulfone (metabolite of Demeton-S)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Demeton-S sulfoxide (metabolite of Demeton-S)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Desethyl atrazine (herbicide metabolite)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Desmedipham (herbicide) 

Carrots 708 0 0.060 NT

Eggplant 346 0 0.060 NT

Appendix B. Page 27 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 333 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

TOTAL 2,093 0

Desmetryn (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Dialifos (insecticide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Diazinon (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.005 0.50

Blueberries, Frozen 14 0 0.005 0.50

Broccoli 708 0 0.001 0.70

Cantaloupe 328 0 0.005 0.75

Carrots 708 0 0.010 0.75

Cauliflower 531 0 0.001 0.70

Celery 354 0 0.002 0.70 R

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.001 0.75 IT

Green Beans 700 0 0.001 0.50

Peaches 518 0 0.002 0.20

Peaches, Frozen 154 0 0.002 0.20

Pears 707 2 0.3 0.002 - 0.003 0.001 0.50

Plums 277 0 0.005 0.20

Summer Squash 698 0 0.001 - 0.005 0.50 R

Sweet Bell Peppers 319 1 0.3 0.024 0.002 0.5 R

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.75

Winter Squash 706 0 0.001 0.75 R

TOTAL 9,523 3

Diazinon oxygen analog (metabolite of Diazinon)

Broccoli 708 0 0.001 0.70

Carrots 708 0 0.010 0.75

Cauliflower 531 0 0.001 0.70

Celery 354 0 0.001 0.70 R

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.002 0.75 IT

Green Beans 700 0 0.001 0.50

Peaches 518 0 0.001 0.20

Peaches, Frozen 154 0 0.001 0.20

Pears 707 0 0.002 0.50

Summer Squash 365 0 0.001 0.50 R

Sweet Bell Peppers 319 0 0.001 0.5 R

Tangerines 531 0 0.005 NT

Winter Squash 706 0 0.001 0.75 R

TOTAL 7,704 0

Appendix B. Page 28 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dichlobenil (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 0.15

Blueberries, Frozen 14 0 0.010 0.15

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.001 0.15

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 0.15

Peaches, Frozen 154 0 0.005 0.15

Pears 707 0 0.001 0.5

Plums 277 0 0.010 0.15

Summer Squash 698 0 0.001 - 0.002 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 9,532 0

Dichlofenthion (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Dichlormid (herbicide safener)

Carrots 708 0 0.040 0.05

Eggplant 346 0 0.040 0.05

Green Beans 700 0 0.020 0.05

Summer Squash 698 0 0.005 - 0.020 0.05

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.05

Winter Squash 706 0 0.020 0.05

TOTAL 3,864 0

Dichlorobenzophenone o,p' (insecticide) (also a breakdown product of Dicofol)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 690 0 0.001 NT

TOTAL 1,755 0

Dichlorobenzophenone p,p' (insecticide) (also a breakdown product of Dicofol)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 690 0 0.001 NT

TOTAL 1,755 0

Dichlorvos - DDVP (insecticide) (also a metabolite of Naled)

Blueberries, Cultivated, Fresh 692 0 0.020 0.5 TP

Blueberries, Frozen 14 0 0.020 0.5 TP

Broccoli 708 0 0.003 1 TP

Cantaloupe 328 0 0.020 0.5 TP

Carrots 708 0 0.010 0.5 TP

Cauliflower 531 0 0.010 1 TP

Appendix B. Page 29 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Celery 354 0 0.010 3 TP

Eggplant 703 0 0.003 - 0.010 0.5 TP

Grape Juice 700 0 0.075 0.5 TP

Green Beans 700 0 0.040 0.5 TP

Peaches 518 0 0.010 0.5 TP

Peaches, Frozen 154 0 0.010 0.5 TP

Pears 707 0 0.075 0.5 TP

Plums 277 0 0.020 0.5 TP

Summer Squash 698 0 0.005 - 0.040 0.5 TP

Sweet Bell Peppers 319 0 0.010 0.5 TP

Tangerines 531 0 0.005 3 TP

Watermelon 175 0 0.005 0.5 TP

Winter Squash 706 0 0.040 0.5 TP

TOTAL 9,523 0

Diclobutrazol (fungicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Diclofop methyl (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Cantaloupe 328 0 0.001 NT

Green Beans 700 0 0.001 NT

Plums 216 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,021 0

Dicloran (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.016 NT

Blueberries, Frozen 14 0 0.016 NT

Broccoli 708 0 0.002 NT

Cantaloupe 327 0 0.016 NT

Carrots 708 0 0.020 10 IT

Cauliflower 531 0 0.002 NT

Celery 354 24 6.8 0.006 - 0.44 0.005 15

Eggplant 703 0 0.002 - 0.020 NT

Grape Juice 700 0 0.015 10

Green Beans 700 63 9 0.001 - 2.2 0.001 20

Peaches 518 0 0.005 20

Peaches, Frozen 154 0 0.005 20

Plums 277 0 0.016 15

Summer Squash 698 0 0.001 - 0.010 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,824 87

Diclosulam (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Appendix B. Page 30 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dicofol (insecticide) 

Grape Juice 700 0 0.004 5.0 IT

Pears 707 0 0.004 10.0 IT

TOTAL 1,407 0

Dicofol o,p' (isomer of Dicofol) 

Carrots 708 0 0.015 NT

Eggplant 346 0 0.015 2.0 IT

TOTAL 1,054 0

Dicofol p,p' (isomer of Dicofol) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.001 NT

Cantaloupe 327 0 0.010 2.0 IT

Carrots 708 0 0.025 NT

Cauliflower 531 0 0.001 NT

Eggplant 703 0 0.001 - 0.025 2.0 IT

Plums 277 0 0.010 5.0 IT

Summer Squash 333 0 0.005 2.0 IT

Tangerines 531 0 0.005 6.0 IT

Watermelon 175 1 0.6 0.025 0.005 2.0 IT

TOTAL 4,999 1

Dicrotophos (insecticide) 

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Eggplant 357 0 0.001 NT

Green Beans 700 1 0.1 0.003 0.001 V-1 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,367 1

Diethofencarb (fungicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Difenoconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 39 5.6 0.010 - 0.77 0.010 5.0

Blueberries, Frozen 14 0 0.010 0.2

Broccoli 708 15 2.1 0.004 - 0.57 0.003 4.0

Cantaloupe 328 0 0.010 4.0

Carrots 708 12 1.7 0.005 - 0.014 0.005 2.0

Cauliflower 531 3 0.6 0.002 - 0.008 0.001 0.70

Celery 354 0 0.005 0.6

Eggplant 703 51 7.3 0.002 - 0.033 0.001 - 0.005 2.0

Green Beans 700 13 1.9 0.002 - 0.040 0.001 35

Peaches 518 60 11.6 0.005 - 0.10 0.005 0.60

Peaches, Frozen 154 0 0.005 V-3 NT

Pears 707 19 2.7 0.002 - 0.060 0.001 NT

Plums 277 0 0.010 0.60

Summer Squash 698 9 1.3 0.001 - 0.010 0.001 - 0.002 0.6

Sweet Bell Peppers 319 38 11.9 0.006 - 0.085 0.005 0.70

Tangerines 531 0 0.002 0.60

Appendix B. Page 31 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 0 0.002 0.60

Winter Squash 706 13 1.8 0.001 - 0.007 0.001 0.60

TOTAL 8,823 272

Diflubenzuron (insecticide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.003 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 688 0 0.003 NT

Cantaloupe 299 0 0.002 NT

Carrots 708 0 0.080 0.20

Cauliflower 531 0 0.001 - 0.003 NT

Eggplant 703 0 0.001 - 0.080 9.0

Green Beans 700 0 0.001 1.0

Pears 707 0 0.002 V-2 NT

Plums 277 8 2.9 0.002 - 0.005 0.002 NT

Summer Squash 698 0 0.001 - 0.020 3.0

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 3.0

Winter Squash 706 0 0.001 NT

TOTAL 7,429 9

Dimepiperate (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Dimethenamid (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.002 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 0.01 R

TOTAL 8,125 0

Dimethipin (plant growth regulator) 

Green Beans 700 0 0.020 NT

Summer Squash 365 0 0.020 NT

Winter Squash 706 0 0.020 NT

TOTAL 1,771 0

Dimethoate (insecticide) (parent of Omethoate)

Blueberries, Cultivated, Fresh 692 1 0.1 0.007 0.005 1.0 FU

Blueberries, Frozen 14 0 0.005 1.0 FU

Broccoli 708 1 0.1 0.005 0.003 2.0

Appendix B. Page 32 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.005 1.0

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 2.0

Celery 354 3 0.8 0.011 - 0.037 0.010 2.0

Eggplant 703 1 0.1 0.004 0.001 - 0.010 V-1 NT

Green Beans 700 32 4.6 0.001 - 0.27 0.001 2.0

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.005 2.0

Plums 277 0 0.005 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 1 0.3 0.010 0.010 2.0

Tangerines 531 0 0.005 2.0

Watermelon 175 0 0.005 1.0

Winter Squash 706 0 0.001 NT

TOTAL 8,823 39

Dimethomorph (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.003 NT

Blueberries, Frozen 14 0 0.003 NT

Broccoli 708 8 1.1 0.002 - 0.089 0.001 6.0

Cantaloupe 328 0 0.003 0.5

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 6.0

Celery 354 0 0.010 30.0

Eggplant 703 6 0.9 0.002 - 0.019 0.001 - 0.010 1.5

Grape Juice 700 0 0.010 3.0

Green Beans 700 2 0.3 0.006 - 0.012 0.003 V-2 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.003 NT

Summer Squash 698 1 0.1 0.038 0.003 - 0.020 0.5

Sweet Bell Peppers 319 3 0.9 0.012 - 0.025 0.010 1.5

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 0.5

Winter Squash 706 5 0.7 0.003 - 0.007 0.003 0.5

TOTAL 8,816 25

Dimethylvinphos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Dimetilan (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Dimoxystrobin (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Appendix B. Page 33 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Diniconazole (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Dinotefuran (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.003 0.2

Blueberries, Frozen 14 0 0.003 0.2

Broccoli 708 8 1.1 0.010 0.006 1.4

Cantaloupe 328 95 29 0.003 - 0.082 0.003 0.5

Carrots 708 0 0.015 0.01 FF

Cauliflower 531 0 0.006 1.4

Celery 354 4 1.1 0.015 - 0.027 0.010 5.0

Eggplant 703 77 11 0.010 - 0.16 0.006 - 0.015 0.7

Grape Juice 700 0 0.030 0.9

Green Beans 700 23 3.3 0.003 - 0.049 0.003 X-4 0.01 FF

Peaches 499 4 0.8 0.017 - 0.085 0.010 2.0 IT

Peaches, Frozen 154 0 0.010 2.0 IT

Pears 707 0 0.030 2.0 IT

Plums 277 0 0.003 2.0 IT

Summer Squash 698 31 4.4 0.003 - 0.19 0.003 - 0.040 0.5

Sweet Bell Peppers 319 42 13.2 0.010 - 0.62 0.010 0.7

Tangerines 531 0 0.040 0.01 FF

Watermelon 175 0 0.040 0.5

Winter Squash 706 30 4.2 0.003 - 0.051 0.003 0.5

TOTAL 9,504 314

Dioxacarb (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Dioxathion (insecticide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Diphenamid (herbicide) 

Broccoli 708 0 0.002 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 357 0 0.002 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,721 0

Diphenylamine - DPA (plant growth regulator) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 0 0.003 NT

Appendix B. Page 34 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 327 0 0.002 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.003 NT

Celery 334 0 0.005 NT

Eggplant 703 0 0.003 - 0.020 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 648 86 13.3 0.005 - 0.074 0.003 5.0 PH

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,436 86

Dipropetryn (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Disulfoton (insecticide) 

Carrots 708 0 0.050 - 0.10 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.050 NT

Green Beans 700 0 0.001 0.75 IT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Disulfoton oxygen analog (metabolite of Disulfoton)

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Broccoli 708 0 0.001 0.75 IT

Cantaloupe 328 0 0.001 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 0.75 IT

Eggplant 703 0 0.001 - 0.005 NT

Plums 277 0 0.001 NT

Summer Squash 333 0 0.001 NT

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 NT

TOTAL 5,000 0

Disulfoton sulfone (metabolite of Disulfoton)

Blueberries, Cultivated, Fresh 692 0 0.020 NT

Blueberries, Frozen 14 0 0.020 NT

Broccoli 708 0 0.001 0.75 IT

Cantaloupe 328 0 0.020 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 0.75 IT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 0.75 IT

Peaches 518 0 0.010 NT

Appendix B. Page 35 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.020 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,077 0

Disulfoton sulfone oxygen analog (metabolite of Disulfoton)

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

TOTAL 1,054 0

Disulfoton sulfoxide (metabolite of Disulfoton)

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 0 0.001 0.75 IT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 0.75 IT

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.001 0.75 IT

Plums 277 0 0.005 NT

Summer Squash 365 0 0.001 NT

Tangerines 531 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,263 0

Disulfoton sulfoxide oxygen analog (metabolite of Disulfoton)

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

TOTAL 1,054 0

Ditalimfos (fungicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Dithiopyr (herbicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 2,825 0

Diuron (herbicide) 

Blueberries, Cultivated, Fresh 692 2 0.3 0.005 - 0.019 0.002 0.1

Blueberries, Frozen 14 0 0.002 0.1

Broccoli 708 0 0.004 NT

Cantaloupe 328 1 0.3 0.004 0.002 V-1 NT

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.004 NT

Eggplant 703 0 0.004 - 0.015 NT

Grape Juice 700 0 0.006 0.05

Green Beans 700 0 0.010 NT

Pears 707 0 0.006 1

Appendix B. Page 36 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums 277 0 0.002 NT

Summer Squash 698 0 0.010 NT

Tangerines 531 0 0.010 0.05

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 8,178 3

DMST (4-dimethylaminosulphotosluidide) (metabolite of Tolyfluanid)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Dodine (fungicide) 

Green Beans 700 0 0.010 NT

Pears 707 2 0.3 0.008 0.005 5.0

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 2,478 2

Edifenphos (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Emamectin (insecticide) 

Green Beans 560 0 0.010 NT

Summer Squash 314 0 0.010 0.02

Winter Squash 588 0 0.010 0.02

TOTAL 1,462 0

Emamectin benzoate 1 (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 3 0.4 0.002 0.001 - 0.003 0.05

Cantaloupe 328 0 0.010 0.02

Carrots 614 0 0.005 - 0.20 NT

Cauliflower 531 1 0.2 0.008 0.001 - 0.003 0.05

Celery 354 0 0.010 0.1

Eggplant 616 1 0.2 0.005 0.001 - 0.005 0.02

Peaches 399 0 0.010 NT

Peaches, Frozen 147 0 0.010 NT

Pears 707 1 0.1 0.002 0.001 0.02

Plums 277 0 0.010 NT

Sweet Bell Peppers 319 0 0.010 0.02

TOTAL 5,706 6

Endosulfan I (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 0.3 IT

Blueberries, Frozen 14 0 0.010 0.3 IT

Broccoli 708 0 0.005 3.0 IT

Cantaloupe 328 0 0.010 1.0 IT

Carrots 708 0 0.030 0.2 IT

Cauliflower 531 0 0.005 2.0 IT

Celery 354 0 0.005 8.0 IT

Eggplant 703 0 0.005 - 0.030 1.0 IT

Green Beans 700 1 0.1 0.002 0.001 2.0 IT

Appendix B. Page 37 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches 518 0 0.005 2.0 IT

Peaches, Frozen 154 0 0.005 2.0 IT

Pears 707 0 0.006 2.0 IT

Plums 277 0 0.010 2.0 IT

Summer Squash 698 0 0.001 - 0.010 1.0 IT

Sweet Bell Peppers 328 0 0.005 2.0 IT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 1.0 IT

Winter Squash 706 0 0.001 1.0 IT

TOTAL 8,832 1

Endosulfan II (isomer of Endosulfan)

Blueberries, Cultivated, Fresh 692 0 0.015 0.3 IT

Blueberries, Frozen 14 0 0.015 0.3 IT

Broccoli 708 0 0.001 3.0 IT

Cantaloupe 328 0 0.015 1.0 IT

Carrots 708 0 0.030 0.2 IT

Cauliflower 531 0 0.001 2.0 IT

Celery 354 0 0.005 8.0 IT

Eggplant 703 0 0.001 - 0.030 1.0 IT

Green Beans 700 0 0.001 2.0 IT

Peaches 518 0 0.005 2.0 IT

Peaches, Frozen 154 0 0.005 2.0 IT

Pears 707 0 0.020 2.0 IT

Plums 277 0 0.015 2.0 IT

Summer Squash 698 0 0.001 - 0.005 1.0 IT

Sweet Bell Peppers 328 0 0.005 2.0 IT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 1.0 IT

Winter Squash 706 0 0.001 1.0 IT

TOTAL 8,832 0

Endosulfan sulfate (metabolite of Endosulfan)

Blueberries, Cultivated, Fresh 692 0 0.005 0.3 IT

Blueberries, Frozen 14 0 0.005 0.3 IT

Broccoli 708 0 0.018 3.0 IT

Cantaloupe 328 0 0.005 1.0 IT

Carrots 708 0 0.030 0.2 IT

Cauliflower 531 0 0.018 2.0 IT

Celery 354 0 0.005 8.0 IT

Eggplant 673 0 0.018 - 0.030 1.0 IT

Green Beans 700 1 0.1 0.010 0.001 2.0 IT

Peaches 518 1 0.2 0.053 0.005 2.0 IT

Peaches, Frozen 154 0 0.005 2.0 IT

Pears 707 0 0.004 2.0 IT

Plums 277 0 0.005 2.0 IT

Summer Squash 698 7 1 0.001 - 0.067 0.001 - 0.015 1.0 IT

Sweet Bell Peppers 328 0 0.005 2.0 IT

Tangerines 531 0 0.015 NT

Watermelon 175 0 0.015 1.0 IT

Winter Squash 706 1 0.1 0.024 0.001 1.0 IT

TOTAL 8,802 10

EPN (insecticide) 

Carrots 708 0 0.040 NT

Eggplant 346 0 0.040 NT

Green Beans 700 0 0.003 NT

Appendix B. Page 38 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Epoxiconazole (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

EPTC (herbicide) 

Broccoli 708 0 0.001 - 0.003 NT

Carrots 708 1 0.1 0.047 0.035 0.1

Cauliflower 531 0 0.001 - 0.003 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.035 NT

Green Beans 700 2 0.3 0.003 - 0.008 0.003 0.08

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 698 0 0.003 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 0.1

Watermelon 175 0 0.005 NT

Winter Squash 690 0 0.003 NT

TOTAL 6,789 3

Esfenvalerate+Fenvalerate Total (insecticide) 

Blueberries, Cultivated, Fresh 692 27 3.9 0.006 - 0.13 0.005 1.0

Blueberries, Frozen 14 1 7.1 0.017 0.005 1.0

Broccoli 708 4 0.6 0.004 - 0.023 0.002 1.0

Cantaloupe 269 0 0.005 0.5

Cauliflower 531 0 0.002 0.5

Celery 354 0 0.005 0.05 FF

Eggplant 305 0 0.008 0.5

Grape Juice 700 0 0.025 0.05 FF

Peaches 518 22 4.2 0.005 - 0.045 0.005 3.0

Peaches, Frozen 154 0 0.005 3.0

Pears 707 0 0.025 1.0

Plums 250 0 0.005 3.0

Summer Squash 333 0 0.050 0.5

Sweet Bell Peppers 328 11 3.4 0.006 - 0.020 0.005 0.5

Tangerines 531 0 0.050 0.05 FF

Watermelon 175 0 0.050 0.5

TOTAL 6,569 65

Esfenvalerate (isomer of Fenvalerate)

Carrots 708 0 0.020 0.5

Eggplant 346 0 0.020 0.5

Green Beans 700 10 1.4 0.005 - 0.025 0.005 1.0

Summer Squash 365 0 0.005 0.5

Winter Squash 706 0 0.005 0.5

TOTAL 2,825 10

Esprocarb (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Appendix B. Page 39 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Ethaboxam (fungicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 0.90

Grape Juice 700 0 0.001 6.0 FU

Green Beans 700 0 0.001 NT

Summer Squash 698 6 0.9 0.003 - 0.016 0.001 - 0.005 0.30

Watermelon 175 0 0.005 0.30

Winter Squash 706 8 1.1 0.001 - 0.055 0.001 0.30

TOTAL 4,033 14

Ethalfluralin (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 0 0.002 NT

Cantaloupe 328 0 0.005 0.05

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 NT

Eggplant 703 0 0.002 - 0.010 NT

Green Beans 700 0 0.003 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.001 - 0.003 0.05

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 0.05

Winter Squash 706 0 0.003 0.05

TOTAL 6,771 0

Ethametsulfuron methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Ethidimuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Ethiofencarb (insecticide) 

Broccoli 708 0 0.002 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.010 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,355 0

Ethiofencarb sulfone (metabolite of Ethiofencarb)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Appendix B. Page 40 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Ethiofencarb sulfoxide (metabolite of Ethiofencarb)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Ethion (insecticide) 

Broccoli 708 0 0.003 NT

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.015 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,766 0

Ethiprole (insecticide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Ethofumesate (herbicide) 

Carrots 708 0 0.005 7.0 R

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Ethoprop (insecticide) 

Broccoli 708 1 0.1 0.005 0.001 V-1 NT

Carrots 708 1 0.1 0.009 0.005 V-1 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.001 0.02

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,805 2

Ethoxyquin (plant growth regulator) 

Pears 707 150 21.2 0.020 - 1.7 0.012 3

Summer Squash 333 0 0.005 NT

Tangerines 514 0 0.005 NT

TOTAL 1,554 150

Appendix B. Page 41 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Ethylan - Perthane (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Etofenprox (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.025 5.0 FF

Blueberries, Frozen 14 0 0.025 5.0 FF

Broccoli 708 0 0.001 5.0 FF

Cantaloupe 328 0 0.025 5.0 FF

Carrots 708 0 0.020 5.0 FF

Cauliflower 531 0 0.001 5.0 FF

Eggplant 703 0 0.001 - 0.020 5.0 FF

Grape Juice 700 0 0.005 5.0 FF

Green Beans 700 1 0.1 0.003 0.001 5.0 FF

Pears 707 0 0.005 5.0 FF

Plums 277 0 0.025 5.0 FF

Summer Squash 698 0 0.001 - 0.010 5.0 FF

Tangerines 531 0 0.010 5.0 FF

Watermelon 175 0 0.010 5.0 FF

Winter Squash 706 0 0.001 5.0 FF

TOTAL 8,178 1

Etoxazole (acaricide) 

Broccoli 708 1 0.1 0.002 0.001 V-1 NT

Carrots 708 0 0.10 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.004 NT

Eggplant 703 15 2.1 0.002 - 0.013 0.001 - 0.10 0.20

Grape Juice 700 0 0.001 0.50

Green Beans 700 0 0.001 NT

Peaches 518 58 11.2 0.004 - 0.098 0.004 1.0

Peaches, Frozen 154 0 0.004 1.0

Pears 707 73 10.3 0.002 - 0.047 0.001 0.20

Summer Squash 665 1 0.2 0.002 0.001 0.02

Sweet Bell Peppers 319 0 0.004 0.20

Tangerines 531 1 0.2 0.001 0.001 0.10 FU

Watermelon 28 3 10.7 0.002 - 0.074 0.001 0.20

Winter Squash 706 4 0.6 0.002 - 0.005 0.001 0.02

TOTAL 8,032 156

Etridiazole (fungicide) 

Carrots 708 0 0.015 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.015 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 5,218 0

Appendix B. Page 42 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Etrimfos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Famoxadone (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.025 NT

Blueberries, Frozen 14 0 0.025 NT

Broccoli 708 2 0.3 0.004 0.002 - 0.008 V-2 NT

Cantaloupe 328 0 0.025 0.30

Carrots 708 0 0.050 NT

Cauliflower 531 0 0.002 - 0.008 NT

Eggplant 652 1 0.2 0.008 0.008 - 0.050 4.0

Grape Juice 700 0 0.050 2.5 R

Green Beans 700 0 0.010 NT

Plums 277 0 0.025 NT

Summer Squash 698 0 0.010 - 0.050 0.30

Tangerines 531 0 0.10 NT

Watermelon 175 0 0.050 0.30

Winter Squash 706 1 0.1 0.011 0.010 0.30

TOTAL 7,420 4

Famphur (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Fenamidone (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 8 1.1 0.004 - 0.026 0.002 5.0

Cantaloupe 328 0 0.005 0.15

Carrots 708 2 0.3 0.019 0.015 0.15

Cauliflower 531 1 0.2 0.004 0.002 5.0

Celery 354 1 0.3 0.012 0.010 60

Eggplant 703 0 0.002 - 0.015 1.0

Grape Juice 700 0 0.005 1.0 R

Green Beans 700 0 0.001 0.80

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.001 0.15

Sweet Bell Peppers 319 0 0.010 1.0

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 0.15

Winter Squash 706 0 0.001 0.15

TOTAL 8,816 12

Fenamiphos (insecticide) 

Broccoli 708 0 0.001 - 0.003 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 - 0.003 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.002 0.1 FU

Appendix B. Page 43 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,466 0

Fenamiphos sulfone (metabolite of Fenamiphos)

Broccoli 689 0 0.005 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.005 NT

Grape Juice 700 0 0.003 0.1 FU

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,447 0

Fenamiphos sulfoxide (metabolite of Fenamiphos)

Broccoli 708 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.010 NT

Grape Juice 700 0 0.004 0.1 FU

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 6,466 0

Fenarimol (fungicide) 

Broccoli 708 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.010 NT

Grape Juice 700 0 0.008 0.1 FU

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 707 0 0.008 0.1 FU

Summer Squash 365 0 0.001 0.20 FU

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Winter Squash 706 0 0.001 0.20 FU

TOTAL 7,713 0

Fenazaquin (insecticide, acaricide)

Blueberries, Cultivated, Fresh 692 1 0.1 0.053 0.005 2

Blueberries, Frozen 14 0 0.005 2

Appendix B. Page 44 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.005 0.3

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 0.3

Grape Juice 700 0 0.001 0.7

Green Beans 700 0 0.001 0.4

Pears 707 19 2.7 0.002 - 0.12 0.001 0.6

Plums 248 1 0.4 0.007 0.005 2

Summer Squash 698 0 0.001 - 0.005 0.3

Tangerines 531 0 0.005 0.5 IT

Watermelon 175 0 0.005 0.3

Winter Squash 706 0 0.001 0.3

TOTAL 6,553 21

Fenbuconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 15 2.2 0.005 - 0.11 0.005 0.3

Blueberries, Frozen 14 0 0.005 0.3

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.005 NT

Cauliflower 493 1 0.2 0.003 0.001 - 0.003 V-1 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.005 NT

Grape Juice 700 0 0.001 1.0 FU

Green Beans 700 0 0.001 NT

Peaches 518 58 11.2 0.005 - 0.12 0.005 1.0

Peaches, Frozen 154 0 0.005 1.0

Plums 277 1 0.4 0.009 0.005 1.0

Summer Squash 698 0 0.001 NT

Sweet Bell Peppers 319 0 0.005 1.0

Tangerines 531 0 0.001 1.0

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,778 75

Fenchlorphos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Fenhexamid (fungicide) 

Blueberries, Cultivated, Fresh 692 114 16.5 0.013 - 1.2 0.013 5

Blueberries, Frozen 14 2 14.3 0.067 - 0.077 0.013 5

Cantaloupe 328 0 0.013 NT

Carrots 708 0 0.015 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.015 2

Grape Juice 700 21 3 0.008 - 0.18 0.005 4

Green Beans 700 0 0.010 NT

Peaches 518 6 1.2 0.010 - 0.035 0.010 10

Peaches, Frozen 154 0 0.010 10

Pears 707 0 0.005 10

Plums 277 0 0.013 1.5

Summer Squash 698 0 0.010 NT

Sweet Bell Peppers 319 2 0.6 0.011 - 0.031 0.010 2

Tangerines 531 0 0.010 NT

Appendix B. Page 45 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 7,927 145

Fenitrothion (insecticide) 

Broccoli 708 0 0.002 NT

Cauliflower 531 0 0.002 NT

Eggplant 357 0 0.002 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,367 0

Fenobucarb - BPMC (insecticide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Fenoxaprop ethyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Fenoxycarb (insecticide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,825 0

Fenpropathrin (insecticide) 

Blueberries, Cultivated, Fresh 692 23 3.3 0.021 - 1.4 0.020 3.0

Blueberries, Frozen 14 0 0.020 3.0

Broccoli 708 0 0.002 3.0

Cantaloupe 328 0 0.020 0.5

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.002 3.0

Celery 354 1 0.3 0.008 0.005 V-1 NT

Eggplant 703 0 0.002 - 0.020 1.0

Grape Juice 700 0 0.010 5.0

Green Beans 700 4 0.6 0.002 - 0.035 0.001 V-4 NT

Peaches 518 54 10.4 0.005 - 0.90 0.005 1.4

Peaches, Frozen 154 1 0.6 0.008 0.005 1.4

Pears 707 1 0.1 0.017 0.010 5.0

Plums 277 0 0.020 1.4

Summer Squash 698 3 0.4 0.003 - 0.008 0.001 - 0.005 0.5

Sweet Bell Peppers 328 27 8.2 0.007 - 0.32 0.005 1.0

Tangerines 531 1 0.2 0.005 0.005 2.0

Watermelon 175 0 0.005 0.5

Winter Squash 706 18 2.5 0.002 - 0.032 0.001 0.5

TOTAL 9,532 133

Appendix B. Page 46 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fenpropidin (fungicide) 

Green Beans 700 0 0.040 NT

Summer Squash 365 0 0.040 NT

Winter Squash 706 0 0.040 NT

TOTAL 1,771 0

Fenpropimorph (fungicide) 

Blueberries, Cultivated, Fresh 692 2 0.3 0.003 - 0.004 0.001 V-2 NT

Blueberries, Frozen 14 0 0.001 NT

Cantaloupe 328 0 0.001 NT

Celery 354 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 1 0.4 0.042 0.001 V-1 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,427 3

Fenpyrazamine (fungicide) 

Grape Juice 700 0 0.002 4

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.001 - 0.003 NT

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,510 0

Fenpyroximate (acaricide) 

Blueberries, Cultivated, Fresh 692 10 1.4 0.007 - 0.097 0.005 3

Blueberries, Frozen 14 0 0.005 3

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.005 0.10

Carrots 708 0 0.005 NT

Cauliflower 531 1 0.2 0.002 0.001 V-1 NT

Celery 354 0 0.010 4

Eggplant 703 38 5.4 0.003 - 0.022 0.003 - 0.005 0.20

Grape Juice 700 0 0.001 1.0

Green Beans 700 0 0.001 0.40

Peaches 518 37 7.1 0.010 - 0.072 0.010 2.0

Peaches, Frozen 154 0 0.010 2.0

Pears 707 47 6.6 0.002 - 0.10 0.001 0.30

Plums 277 3 1.1 0.005 - 0.009 0.005 2.0

Summer Squash 365 0 0.001 0.4

Sweet Bell Peppers 319 7 2.2 0.011 - 0.058 0.010 0.20

Winter Squash 706 0 0.001 0.4

TOTAL 8,484 143

Fensulfothion (insecticide, fumigant)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Fenthion (insecticide) 

Broccoli 708 0 0.006 NT

Carrots 708 0 0.030 NT

Appendix B. Page 47 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cauliflower 531 0 0.002 - 0.006 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.030 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,775 0

Fenthion oxygen analog sulfone (metabolite of Fenthion)

Carrots 708 0 0.015 NT

Eggplant 346 0 0.015 NT

TOTAL 1,054 0

Fenthion oxygen analog sulfoxide (metabolite of Fenthion)

Carrots 708 0 0.015 NT

Eggplant 346 0 0.015 NT

TOTAL 1,054 0

Fenthion sulfone (metabolite of Fenthion)

Carrots 708 0 0.12 NT

Eggplant 346 0 0.12 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Fenthion sulfoxide (metabolite of Fenthion)

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 2,825 0

Fenuron (herbicide) 

Green Beans 700 0 0.020 NT

Summer Squash 365 0 0.020 NT

Winter Squash 706 0 0.020 NT

TOTAL 1,771 0

Fipronil (insecticide) 

Broccoli 708 0 0.001 NT

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.015 NT

Green Beans 700 1 0.1 0.009 0.001 V-1 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 1 0.3 0.013 0.005 V-1 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,775 2

Appendix B. Page 48 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fipronil sulfone - MB46136 (metabolite of Fipronil)

Blueberries, Cultivated, Fresh 692 0 0.050 NT

Blueberries, Frozen 14 0 0.050 NT

Cantaloupe 328 0 0.050 NT

Green Beans 700 1 0.1 0.002 0.001 V-1 NT

Plums 277 0 0.050 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,082 1

Flazasulfuron (herbicide) 

Grape Juice 700 0 0.006 0.01

Green Beans 700 0 0.005 NT

Summer Squash 698 0 0.005 NT

Tangerines 531 0 0.005 0.01

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 3,510 0

Flonicamid (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.006 1.5

Blueberries, Frozen 14 0 0.006 1.5

Broccoli 708 6 0.8 0.006 - 0.052 0.003 1.5

Cantaloupe 328 1 0.3 0.007 0.006 1.5

Carrots 708 0 0.005 0.60

Cauliflower 531 1 0.2 0.010 0.003 1.5

Celery 354 16 4.5 0.010 - 0.045 0.010 4.0

Eggplant 703 33 4.7 0.002 - 0.095 0.001 - 0.005 3.0

Green Beans 700 5 0.7 0.012 - 0.042 0.010 4.0

Peaches 518 0 0.010 0.60

Peaches, Frozen 154 0 0.010 0.60

Pears 707 0 0.003 0.20

Plums 277 0 0.006 0.60

Summer Squash 698 21 3 0.011 - 0.096 0.010 - 0.050 1.5

Sweet Bell Peppers 319 43 13.5 0.011 - 0.53 0.010 3.0

Tangerines 531 0 0.050 1.5

Watermelon 175 0 0.050 1.5

Winter Squash 706 1 0.1 0.032 0.010 1.5

TOTAL 8,823 127

Florpyrauxifen-Benzyl (herbicide) 

Green Beans 700 0 0.020 EX2

Summer Squash 365 0 0.020 EX2

Winter Squash 706 0 0.020 EX2

TOTAL 1,771 0

Fluazifop butyl (herbicide) 

Broccoli 708 1 0.1 0.002 0.001 V-1 NT

Carrots 328 0 0.005 2.0

Cauliflower 531 0 0.001 NT

Eggplant 532 0 0.001 - 0.005 NT

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 0.03

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,909 1

Appendix B. Page 49 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fluazifop-P-butyl (herbicide) 

Carrots 380 0 0.005 2.0

Eggplant 171 0 0.005 NT

Grape Juice 700 0 0.002 0.03

TOTAL 1,251 0

Fluazinam (fungicide) 

Carrots 708 0 0.025 0.70

Eggplant 346 0 0.025 0.09

TOTAL 1,054 0

Flubendiamide (insecticide) 

Blueberries, Cultivated, Fresh 606 0 0.004 1.5

Blueberries, Frozen 11 0 0.004 1.5

Broccoli 708 10 1.4 0.002 - 0.034 0.001 3.0

Cantaloupe 328 0 0.004 0.20

Carrots 708 0 0.010 NT

Cauliflower 531 1 0.2 0.019 0.003 3.0

Eggplant 703 1 0.1 0.059 0.003 - 0.010 0.60

Grape Juice 700 0 0.005 1.4

Green Beans 700 12 1.7 0.001 - 0.051 0.001 0.50

Pears 707 9 1.3 0.008 - 0.19 0.005 1.5

Plums 196 0 0.004 1.6

Summer Squash 698 4 0.6 0.001 - 0.004 0.001 - 0.020 0.20

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 0.20

Winter Squash 706 37 5.2 0.001 - 0.027 0.001 0.20

TOTAL 8,008 74

Flucythrinate (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Fludioxonil (fungicide) 

Blueberries, Cultivated, Fresh 692 167 24.1 0.025 - 3.1 0.025 X-1 3.0

Blueberries, Frozen 14 4 28.6 0.028 - 0.089 0.025 3.0

Broccoli 708 8 1.1 0.010 - 0.089 0.006 2

Cantaloupe 328 0 0.025 0.45

Carrots 708 0 0.065 7.0

Cauliflower 531 0 0.006 2

Celery 354 1 0.3 0.020 0.005 15

Eggplant 703 0 0.006 - 0.065 0.50

Grape Juice 700 5 0.7 0.017 - 0.037 0.010 2.0

Green Beans 700 0 0.010 0.4

Peaches 518 454 87.6 0.005 - 24 0.005 X-3 5.0

Peaches, Frozen 154 23 14.9 0.011 - 0.18 0.005 5.0

Pears 707 372 52.6 0.017 - 2.3 0.010 5.0

Plums 277 236 85.2 0.025 - 1.2 0.025 5.0

Summer Squash 698 1 0.1 0.014 0.005 - 0.010 0.45

Sweet Bell Peppers 328 6 1.8 0.005 - 0.088 0.005 0.50

Tangerines 531 196 36.9 0.005 - 0.26 0.005 10

Watermelon 175 0 0.005 0.45

Winter Squash 706 1 0.1 0.020 0.010 0.45

TOTAL 9,532 1,474

Appendix B. Page 50 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fluensulfone (nematicide) 

Carrots 708 0 0.010 4

Eggplant 346 0 0.010 0.7

Grape Juice 700 0 0.070 0.8

Pears 707 0 0.070 0.4

Summer Squash 333 0 0.005 0.7

Tangerines 531 0 0.005 0.3

Watermelon 175 0 0.005 0.7

TOTAL 3,500 0

Flufenacet (herbicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,218 0

Flufenoxuron (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Cantaloupe 328 0 0.001 NT

Grape Juice 700 0 0.002 0.70 FU

Green Beans 700 0 0.001 NT

Pears 707 0 0.002 0.50 FU

Plums 277 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,489 0

Flufenpyr ethyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Flumetsulam (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Flumiclorac pentyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Flumioxazin (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 0.07

Blueberries, Frozen 14 0 0.010 0.07

Appendix B. Page 51 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.010 0.02

Cantaloupe 298 0 0.010 0.03

Carrots 708 0 0.040 NT

Cauliflower 531 0 0.003 0.02

Celery 354 0 0.005 0.02

Eggplant 703 0 0.003 - 0.040 0.02

Grape Juice 700 0 0.030 0.02

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 0.02

Peaches, Frozen 154 0 0.005 0.02

Pears 707 0 0.030 0.02

Plums 247 0 0.010 0.02

Summer Squash 698 0 0.001 - 0.005 0.03

Sweet Bell Peppers 328 0 0.005 0.02

Tangerines 531 0 0.005 0.02

Watermelon 147 0 0.005 0.03

Winter Squash 706 0 0.001 0.03

TOTAL 9,444 0

Fluometuron (herbicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.004 NT

Tangerines 531 0 0.004 NT

Watermelon 175 0 0.004 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,864 0

Fluopicolide (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 32 4.5 0.002 - 0.011 0.001 5.0

Cantaloupe 328 6 1.8 0.005 - 0.008 0.005 0.50

Carrots 708 7 1 0.013 - 0.042 0.010 0.15

Cauliflower 531 9 1.7 0.002 - 0.006 0.001 5.0

Celery 354 0 0.010 25

Eggplant 703 16 2.3 0.002 - 0.018 0.001 - 0.010 1.6

Grape Juice 700 0 0.005 2.0

Green Beans 700 2 0.3 0.003 - 0.020 0.001 0.90

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.005 NT

Summer Squash 698 16 2.3 0.002 - 0.064 0.001 - 0.010 0.50

Sweet Bell Peppers 319 10 3.1 0.010 - 0.041 0.010 1.6

Tangerines 531 0 0.010 0.01

Watermelon 175 2 1.1 0.013 - 0.030 0.010 0.50

Winter Squash 706 17 2.4 0.001 - 0.014 0.001 0.50

TOTAL 8,816 117

Fluopyram (fungicide) 

Blueberries, Cultivated, Fresh 692 53 7.7 0.005 - 0.43 0.005 7.0

Blueberries, Frozen 14 4 28.6 0.006 - 0.056 0.005 7.0

Broccoli 708 59 8.3 0.002 - 0.024 0.001 4.0

Cantaloupe 328 44 13.4 0.005 - 0.036 0.005 1.0

Carrots 708 22 3.1 0.005 - 0.021 0.005 0.30

Cauliflower 531 21 4 0.002 - 0.005 0.001 4.0

Appendix B. Page 52 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Celery 354 0 0.010 20

Eggplant 703 180 25.6 0.002 - 0.27 0.001 - 0.005 4.0

Grape Juice 700 308 44 0.002 - 0.007 0.001 2.0

Green Beans 700 20 2.9 0.001 - 0.019 0.001 4.0

Peaches 518 89 17.2 0.010 - 0.25 0.010 1.0

Peaches, Frozen 154 10 6.5 0.010 - 0.026 0.010 1.0

Pears 707 35 5 0.002 - 0.068 0.001 0.80

Plums 277 41 14.8 0.006 - 0.060 0.005 0.50

Summer Squash 698 56 8 0.001 - 0.17 0.001 - 0.002 0.60

Sweet Bell Peppers 319 88 27.6 0.011 - 0.19 0.010 4.0

Tangerines 531 0 0.002 1.0

Watermelon 175 10 5.7 0.002 - 0.012 0.002 1.0

Winter Squash 706 23 3.3 0.001 - 0.052 0.001 0.60

TOTAL 9,523 1,063

Fluorodifen (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Fluoxastrobin (fungicide) 

Broccoli 708 0 0.001 - 0.003 NT

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.002 4.0

Eggplant 703 12 1.7 0.002 - 0.005 0.001 - 0.015 1.0

Green Beans 700 1 0.1 0.002 0.001 V-1 NT

Peaches 518 0 0.002 NT

Peaches, Frozen 154 0 0.002 NT

Summer Squash 698 0 0.001 0.50

Sweet Bell Peppers 319 1 0.3 0.022 0.002 1.0

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.001 1.5

Winter Squash 706 2 0.3 0.003 - 0.062 0.001 0.50

TOTAL 6,805 16

Flupyradifurone (insecticide) 

Broccoli 708 35 4.9 0.003 - 0.11 0.003 6

Carrots 708 0 0.10 0.90

Cauliflower 531 89 16.8 0.002 - 0.11 0.001 6

Eggplant 703 64 9.1 0.002 - 0.18 0.001 - 0.10 1.5

Grape Juice 700 0 0.015 3.0

Green Beans 700 23 3.3 0.001 - 0.091 0.001 3.0

Summer Squash 698 40 5.7 0.001 - 0.12 0.001 - 0.005 0.40

Tangerines 531 3 0.6 0.005 - 0.009 0.005 3.0

Watermelon 175 7 4 0.005 - 0.025 0.005 0.40

Winter Squash 706 41 5.8 0.001 - 0.085 0.001 0.40

TOTAL 6,160 302

Fluquinconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Celery 354 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Appendix B. Page 53 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums 247 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,397 0

Fluridone (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.001 0.1 IN

Blueberries, Frozen 14 0 0.001 0.1 IN

Broccoli 708 0 0.001 0.1 IN

Cantaloupe 328 0 0.001 0.1 IN

Carrots 708 0 0.005 0.1 IN

Cauliflower 531 0 0.001 0.1 IN

Celery 354 0 0.010 0.1 IN

Eggplant 703 0 0.001 - 0.005 0.1 IN

Grape Juice 700 0 0.001 0.1 IN

Green Beans 700 0 0.001 0.1 IN

Peaches 518 0 0.010 0.1 IN

Peaches, Frozen 154 0 0.010 0.1 IN

Pears 707 0 0.001 0.1 IN

Plums 277 0 0.001 0.1 IN

Summer Squash 698 0 0.001 - 0.002 0.1 IN

Sweet Bell Peppers 319 0 0.010 0.1 IN

Tangerines 531 0 0.002 0.1 IN

Watermelon 175 0 0.002 0.1 IN

Winter Squash 706 0 0.001 0.1 IN

TOTAL 9,523 0

Fluroxypyr-meptyl (herbicide) 

Pears 707 0 0.010 0.02

TOTAL 707 0

Flusilazole (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,490 0

Fluthiacet methyl (herbicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,864 0

Appendix B. Page 54 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Flutianil (fungicide) 

Grape Juice 700 0 0.002 0.7

Summer Squash 333 0 0.005 0.2

Watermelon 175 0 0.005 0.07

TOTAL 1,208 0

Flutolanil (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 1 0.1 0.019 0.001 V-1 NT

Plums 277 0 0.002 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,136 1

Flutriafol (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 6 0.8 0.002 - 0.004 0.001 1.5

Cantaloupe 328 3 0.9 0.021 - 0.026 0.010 0.30

Carrots 708 0 0.010 NT

Cauliflower 531 2 0.4 0.002 0.001 1.5

Eggplant 703 20 2.8 0.002 - 0.040 0.001 - 0.010 1.0

Grape Juice 700 83 11.9 0.003 - 0.028 0.002 1.5

Green Beans 700 14 2 0.002 - 0.027 0.001 V-14 NT

Pears 707 1 0.1 0.003 0.002 0.40

Plums 277 0 0.010 1.5

Summer Squash 698 63 9 0.001 - 0.045 0.001 - 0.002 0.30

Tangerines 531 1 0.2 0.002 0.002 V-1 NT

Watermelon 175 7 4 0.003 - 0.018 0.002 0.30

Winter Squash 706 37 5.2 0.001 - 0.032 0.001 0.30

TOTAL 8,178 237

Fluvalinate (insecticide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.051 0.050 V-1 NT

Blueberries, Frozen 14 0 0.050 NT

Cantaloupe 328 0 0.050 NT

Carrots 708 0 0.020 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.020 NT

Grape Juice 700 0 0.012 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 707 0 0.012 NT

Plums 252 0 0.050 NT

Summer Squash 698 0 0.001 - 0.050 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.050 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,911 1

Appendix B. Page 55 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fluxapyroxad (fungicide) 

Broccoli 708 13 1.8 0.002 - 0.010 0.001 4.0

Carrots 708 30 4.2 0.011 - 0.073 0.010 0.90

Cauliflower 531 0 0.003 4.0

Eggplant 703 17 2.4 0.002 - 0.020 0.001 - 0.010 0.7

Grape Juice 700 0 0.002 2.0

Green Beans 700 32 4.6 0.001 - 0.036 0.001 2.0

Pears 707 84 11.9 0.003 - 0.23 0.002 0.8

Summer Squash 698 11 1.6 0.001 - 0.007 0.001 - 0.005 0.50

Tangerines 531 0 0.005 1.0

Watermelon 175 0 0.005 0.50

Winter Squash 706 19 2.7 0.002 - 0.018 0.001 0.50

TOTAL 6,867 206

Folpet (fungicide) 

Cantaloupe 299 0 0.030 3.0 FU

Celery 354 0 0.015 NT

Grape Juice 700 0 0.10 50.0 FU

Peaches 518 0 0.015 NT

Peaches, Frozen 154 0 0.015 NT

Plums 250 0 0.030 NT

Sweet Bell Peppers 328 0 0.015 NT

TOTAL 2,603 0

Fomesafen (herbicide) 

Summer Squash 333 0 0.005 0.025

Tangerines 531 0 0.005 NT

Watermelon 147 0 0.005 0.025

TOTAL 1,011 0

Fonofos (insecticide) 

Broccoli 708 0 0.001 - 0.003 NT

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.015 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,775 0

Foramsulfuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Forchlorfenuron (plant growth regulator) 

Carrots 708 0 0.005 NT

Celery 354 0 0.002 NT

Eggplant 346 0 0.005 NT

Grape Juice 700 0 0.002 0.03

Green Beans 700 0 0.001 NT

Peaches 518 0 0.002 NT

Appendix B. Page 56 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.002 NT

Pears 707 0 0.002 0.01

Summer Squash 698 4 0.6 0.002 - 0.003 0.001 V-4 NT

Sweet Bell Peppers 319 0 0.002 NT

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,616 4

Formetanate hydrochloride (insecticide) 

Carrots 708 0 0.010 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 0.40 IT

Peaches, Frozen 154 0 0.010 0.40 IT

Pears 707 0 0.010 0.50 IT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 3 0.6 0.006 - 0.012 0.005 0.03

Winter Squash 706 0 0.001 NT

TOTAL 5,408 3

Fosthiazate (nematicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Furalaxyl (fungicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Furathiocarb (insecticide) 

Celery 354 0 0.010 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Sweet Bell Peppers 319 0 0.010 NT

TOTAL 1,345 0

Halosulfuron (herbicide) 

Carrots 679 0 0.050 NT

Eggplant 346 0 0.050 0.05

Tangerines 531 0 0.010 NT

TOTAL 1,556 0

Halosulfuron methyl 2 (herbicide) 

Celery 354 0 0.010 NT

Grape Juice 700 0 0.002 0.05 R

Green Beans 700 0 0.001 0.05

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.002 0.05

Summer Squash 698 0 0.001 - 0.010 0.5

Appendix B. Page 57 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Bell Peppers 319 0 0.010 0.05

Watermelon 175 0 0.010 0.1

Winter Squash 706 0 0.001 0.5

TOTAL 5,031 0

Heptenophos (insecticide, acaricide)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Hexaconazole (fungicide) 

Celery 354 0 0.010 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.005 NT

TOTAL 3,116 0

Hexazinone (herbicide) 

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,825 0

Hexythiazox (insecticide, acaricide)

Blueberries, Cultivated, Fresh 692 1 0.1 0.002 0.002 6

Blueberries, Frozen 14 0 0.002 6

Broccoli 708 0 0.006 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.015 NT

Cauliflower 531 3 0.6 0.003 0.002 V-3 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.006 - 0.015 1.5

Grape Juice 700 0 0.002 1

Green Beans 700 0 0.001 0.3 R

Peaches 518 14 2.7 0.010 - 0.23 0.010 1.0

Peaches, Frozen 154 0 0.010 1.0

Pears 707 5 0.7 0.003 0.002 0.4

Plums 247 27 10.9 0.002 - 0.013 0.002 1.0

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 1.5

Tangerines 469 0 0.010 0.6 R

Watermelon 175 0 0.005 NT

Winter Squash 706 1 0.1 0.001 0.001 V-1 NT

TOTAL 9,431 51

Hydroprene (insect growth regulator) 

Broccoli 708 0 0.005 0.2 FF

Carrots 708 0 0.015 0.2 FF

Cauliflower 531 0 0.002 - 0.005 0.2 FF

Eggplant 703 0 0.002 - 0.015 0.2 FF

Grape Juice 700 0 0.010 0.2 FF

Appendix B. Page 58 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 700 0 0.003 0.2 FF

Pears 707 0 0.010 0.2 FF

Summer Squash 698 0 0.003 - 0.005 0.2 FF

Tangerines 531 0 0.005 0.2 FF

Watermelon 175 0 0.005 0.2 FF

Winter Squash 706 0 0.003 0.2 FF

TOTAL 6,867 0

3-Hydroxycarbofuran (metabolite of Carbofuran)

Blueberries, Cultivated, Fresh 692 0 0.003 NT

Blueberries, Frozen 14 0 0.003 NT

Cantaloupe 328 0 0.003 NT

Carrots 708 0 0.005 NT

Cauliflower 513 0 0.004 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.004 - 0.005 NT

Grape Juice 700 0 0.008 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.008 NT

Plums 277 0 0.003 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,797 0

5-Hydroxythiabendazole (metabolite of Thiabendazole)

Carrots 708 0 0.005 10 TP

Green Beans 700 0 0.001 0.02 TP

Summer Squash 365 0 0.001 0.02 TP

Winter Squash 706 0 0.001 0.02 TP

TOTAL 2,479 0

Hydroxy Acequinocyl (metabolite of Acequinocyl)

Green Beans 700 1 0.1 0.003 0.001 0.25

Summer Squash 365 0 0.001 0.30

Winter Squash 690 0 0.001 0.30

TOTAL 1,755 1

Imazalil (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.005 NT

Cauliflower 531 1 0.2 0.002 0.001 V-1 NT

Celery 354 0 0.010 NT

Eggplant 703 1 0.1 0.002 0.001 - 0.005 V-1 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 1 0.1 0.017 0.010 V-1 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.003 - 0.005 NT

Appendix B. Page 59 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 504 94.9 0.006 - 1.1 0.005 10.0 PH

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 8,823 507

Imazethapyr (herbicide) 

Blueberries, Cultivated, Fresh 675 0 0.020 NT

Blueberries, Frozen 14 0 0.020 NT

Cantaloupe 328 0 0.020 NT

Plums 277 0 0.020 NT

TOTAL 1,294 0

Imazosulfuron (herbicide) 

Carrots 708 0 0.025 NT

Eggplant 346 0 0.025 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Imidacloprid (insecticide) 

Blueberries, Cultivated, Fresh 692 72 10.4 0.003 - 0.51 0.003 3.5

Blueberries, Frozen 14 5 35.7 0.004 - 0.038 0.003 3.5

Broccoli 708 118 16.7 0.003 - 0.053 0.003 3.5

Cantaloupe 328 63 19.2 0.003 - 0.060 0.003 0.5

Carrots 708 1 0.1 0.025 0.020 0.40

Cauliflower 531 96 18.1 0.003 - 1.1 0.003 3.5

Celery 354 5 1.4 0.010 - 0.020 0.010 6.0

Eggplant 703 149 21.2 0.002 - 0.13 0.001 - 0.020 1.0

Grape Juice 700 0 0.020 1.0

Green Beans 700 19 2.7 0.003 - 0.16 0.003 4.0

Peaches 518 28 5.4 0.011 - 0.32 0.010 3.0

Peaches, Frozen 154 0 0.010 3.0

Pears 707 63 8.9 0.033 - 0.29 0.020 0.6

Plums 277 6 2.2 0.005 - 0.009 0.003 3.0

Summer Squash 698 253 36.2 0.003 - 0.36 0.003 - 0.010 0.5

Sweet Bell Peppers 319 85 26.6 0.010 - 0.45 0.010 1.0

Tangerines 531 9 1.7 0.010 - 0.041 0.010 0.70

Watermelon 175 30 17.1 0.010 - 0.12 0.010 0.5

Winter Squash 706 253 35.8 0.003 - 0.21 0.003 0.5

TOTAL 9,523 1,255

Imidacloprid desnitro (metabolite of Imidacloprid)

Green Beans 679 56 8.2 0.001 - 0.023 0.001 4.0

Summer Squash 327 118 36.1 0.001 - 0.006 0.001 0.5

Winter Squash 706 299 42.4 0.001 - 0.018 0.001 0.5

TOTAL 1,712 473

Imidacloprid urea (metabolite of Imidacloprid)

Carrots 708 0 0.015 0.40

Eggplant 346 0 0.015 1.0

Grape Juice 700 0 0.025 1.0

Green Beans 700 11 1.6 0.001 - 0.008 0.001 4.0

Pears 707 2 0.3 0.042 0.025 0.6

Summer Squash 365 35 9.6 0.001 - 0.016 0.001 0.5

Winter Squash 706 26 3.7 0.001 - 0.006 0.001 0.5

TOTAL 4,232 74

Appendix B. Page 60 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Imiprothrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.045 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.045 NT

Green Beans 700 0 0.010 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.012 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.010 - 0.10 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.40 NT

Watermelon 175 0 0.10 NT

Winter Squash 706 0 0.010 NT

TOTAL 7,227 0

Indaziflam (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.001 0.01

Blueberries, Frozen 14 0 0.001 0.01

Cantaloupe 328 0 0.001 NT

Grape Juice 700 0 0.001 0.01

Green Beans 700 0 0.001 NT

Pears 707 0 0.001 0.01

Plums 277 0 0.001 0.01

Summer Squash 698 0 0.001 NT

Tangerines 531 0 0.001 0.01

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,528 0

Indoxacarb (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.020 1.5

Blueberries, Frozen 14 0 0.020 1.5

Cantaloupe 328 0 0.020 0.60

Carrots 708 0 0.025 NT

Celery 354 1 0.3 0.081 0.010 14

Eggplant 346 0 0.025 0.50

Grape Juice 700 0 0.003 2

Green Beans 700 0 0.005 0.9

Peaches 518 28 5.4 0.010 - 0.045 0.010 0.90

Peaches, Frozen 154 0 0.010 0.90

Pears 707 1 0.1 0.005 0.003 0.20

Plums 277 0 0.020 0.90

Summer Squash 698 0 0.005 - 0.050 0.60

Sweet Bell Peppers 319 2 0.6 0.011 - 0.013 0.010 0.50

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.050 0.60

Winter Squash 706 0 0.005 0.60

TOTAL 7,927 32

Ipconazole (fungicide) 

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Appendix B. Page 61 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 700 0 0.003 0.01

Summer Squash 698 0 0.003 - 0.010 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,864 0

Iprobenfos - IBP (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Iprodione (fungicide) 

Blueberries, Cultivated, Fresh 692 18 2.6 0.040 - 2.1 0.040 15.0

Blueberries, Frozen 14 1 7.1 0.37 0.040 15.0

Broccoli 708 1 0.1 0.28 0.009 25.0

Cantaloupe 328 0 0.040 NT

Carrots 708 66 9.3 0.015 - 3.3 0.015 5.0

Cauliflower 531 0 0.009 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.015 - 0.030 NT

Grape Juice 700 0 0.050 60.0

Green Beans 700 11 1.6 0.005 - 0.14 0.003 2.0

Peaches 518 27 5.2 0.005 - 0.044 0.005 20.0 PH

Peaches, Frozen 154 0 0.005 20.0 PH

Plums 277 0 0.040 20.0 PH

Summer Squash 698 0 0.003 - 0.075 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.075 NT

Watermelon 175 0 0.075 NT

Winter Squash 706 0 0.003 NT

TOTAL 8,825 124

Iprovalicarb (fungicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Grape Juice 700 0 0.002 2.0 FU

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,564 0

Isocarbophos (insecticide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Isofenphos (insecticide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.003 NT

Appendix B. Page 62 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,125 0

Isofenphos methyl (metabolite if Isofenphos)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Isofetamid (fungicide) 

Grape Juice 700 2 0.3 0.002 0.001 3.0

Pears 707 0 0.001 0.60

Summer Squash 333 0 0.001 NT

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.001 NT

TOTAL 2,446 2

Isoprocarb (insecticide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Isopropalin (herbicide) 

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 1,771 0

Isoprothiolane (fungicide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,125 0

Isoproturon (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Isopyrazam (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.30 FU

Winter Squash 706 0 0.001 NT

TOTAL 2,810 0

Isoxaben (herbicide) 

Grape Juice 700 0 0.001 0.01

Pears 707 0 0.001 NT

TOTAL 1,407 0

Appendix B. Page 63 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Isoxadifen ethyl (herbicide safener) 

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,864 0

Kinoprene (insecticide) 

Carrots 708 0 0.10 NT

Eggplant 346 0 0.10 NT

TOTAL 1,054 0

Kresoxim-methyl (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.002 NT

Cantaloupe 328 0 0.010 0.40

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.002 NT

Eggplant 703 0 0.002 - 0.015 NT

Grape Juice 700 0 0.015 1.0

Green Beans 700 0 0.005 NT

Pears 707 0 0.015 0.5

Plums 277 0 0.010 NT

Summer Squash 698 0 0.005 0.40

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.40

Winter Squash 706 0 0.005 0.40

TOTAL 8,178 0

Lactofen (herbicide) 

Green Beans 700 0 0.003 0.01

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Lenacil (herbicide) 

Celery 354 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

TOTAL 1,354 0

Leptophos oxygen analog (insecticide metabolite)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Linuron (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.008 NT

Blueberries, Frozen 14 0 0.008 NT

Broccoli 708 0 0.002 NT

Appendix B. Page 64 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.008 NT

Carrots 708 226 31.9 0.010 - 0.29 0.010 1.0

Cauliflower 531 0 0.002 NT

Celery 354 17 4.8 0.020 - 0.37 0.019 0.5 R

Eggplant 703 0 0.002 - 0.010 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.019 NT

Peaches, Frozen 154 0 0.019 NT

Plums 277 0 0.008 NT

Summer Squash 698 0 0.003 - 0.010 NT

Sweet Bell Peppers 328 0 0.019 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 8,125 243

Lufenuron (insecticide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

TOTAL 1,054 0

Malathion (insecticide) 

Blueberries, Cultivated, Fresh 692 65 9.4 0.002 - 0.15 0.002 8

Blueberries, Frozen 14 4 28.6 0.005 - 0.015 0.002 8

Broccoli 708 3 0.4 0.002 - 0.006 0.001 8

Cantaloupe 328 0 0.002 8

Carrots 708 0 0.005 8

Cauliflower 531 0 0.001 8

Celery 354 51 14.4 0.011 - 0.18 0.010 8

Eggplant 703 18 2.6 0.002 - 0.024 0.001 - 0.005 8

Grape Juice 700 0 0.004 8

Green Beans 700 0 0.003 8

Peaches 518 0 0.010 8

Peaches, Frozen 154 0 0.010 8

Pears 707 0 0.004 8

Plums 277 0 0.002 8

Summer Squash 698 0 0.003 - 0.010 8

Sweet Bell Peppers 319 3 0.9 0.013 - 0.064 0.010 8

Tangerines 531 0 0.010 8

Watermelon 175 0 0.010 8

Winter Squash 706 1 0.1 0.008 0.003 8

TOTAL 9,523 145

Malathion oxygen analog (metabolite of Malathion)

Blueberries, Cultivated, Fresh 381 4 1 0.003 - 0.004 0.002 8

Blueberries, Frozen 9 0 0.002 8

Broccoli 708 0 0.002 8

Cantaloupe 328 0 0.002 8

Carrots 708 0 0.005 8

Cauliflower 531 0 0.002 8

Celery 354 0 0.010 8

Eggplant 703 0 0.002 - 0.005 8

Grape Juice 700 0 0.007 8

Green Beans 700 0 0.001 8

Peaches 518 0 0.010 8

Peaches, Frozen 154 0 0.010 8

Appendix B. Page 65 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pears 707 0 0.007 8

Plums 219 0 0.002 8

Summer Squash 698 0 0.001 - 0.002 8

Sweet Bell Peppers 319 0 0.010 8

Tangerines 531 0 0.002 8

Watermelon 175 0 0.002 8

Winter Squash 706 0 0.001 8

TOTAL 9,149 4

Mandestrobin (fungicide) 

Grape Juice 700 0 0.004 5.0

TOTAL 700 0

Mandipropamid (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 8 1.1 0.005 - 0.32 0.003 - 0.010 3.0

Cantaloupe 328 0 0.002 0.6

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.003 3.0

Celery 354 2 0.6 0.008 - 0.020 0.005 20

Eggplant 703 1 0.1 0.023 0.003 - 0.020 1.0

Grape Juice 700 51 7.3 0.003 - 0.010 0.002 1.4

Green Beans 700 0 0.003 0.90

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.002 NT

Summer Squash 698 7 1 0.003 - 0.010 0.003 - 0.005 0.6

Sweet Bell Peppers 319 13 4.1 0.005 - 0.074 0.005 1.0

Tangerines 531 0 0.005 0.50

Watermelon 175 0 0.005 0.6

Winter Squash 706 7 1 0.004 - 0.045 0.003 0.6

TOTAL 8,816 89

Mecarbam (insecticide, acaricide)

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Mefenacet (herbicide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,125 0

Mefenpyr diethyl (herbicide safener) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Appendix B. Page 66 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mefentrifluconazole (fungicide) 

Grape Juice 700 0 0.015 1.5

Pears 707 0 0.015 1.5

Watermelon 175 0 0.005 0.5

TOTAL 1,582 0

Mepanipyrim (fungicide) 

Grape Juice 700 0 0.006 1.5

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,471 0

Mephosfolan (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Mepronil (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Mesotrione (herbicide) 

Grape Juice 700 0 0.12 NT

Pears 707 0 0.12 0.01

Summer Squash 333 0 0.050 NT

Tangerines 531 0 0.050 0.01

Watermelon 175 0 0.050 NT

TOTAL 2,446 0

Metaflumizone (insecticide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 1.5 FU

Grape Juice 700 0 0.050 5

Green Beans 610 0 0.010 NT

Summer Squash 698 0 0.005 - 0.010 NT

Tangerines 531 0 0.005 3

Watermelon 175 0 0.005 1 FU

Winter Squash 706 0 0.010 NT

TOTAL 4,474 0

Metalaxyl/Mefenoxam 3 (fungicide) 

Blueberries, Cultivated, Fresh 692 32 4.6 0.001 - 0.12 0.001 2.0

Blueberries, Frozen 14 1 7.1 0.002 0.001 2.0

Broccoli 708 3 0.4 0.002 - 0.006 0.001 2.0

Cantaloupe 328 70 21.3 0.001 - 0.019 0.001 1.0

Carrots 708 3 0.4 0.015 - 0.019 0.015 0.5

Cauliflower 531 12 2.3 0.002 - 0.070 0.001 1.0

Celery 354 1 0.3 0.032 0.005 5.0

Eggplant 703 0 0.001 - 0.015 1.0

Grape Juice 700 0 0.002 2.0

Green Beans 700 45 6.4 0.001 - 0.023 0.001 0.2

Peaches 518 0 0.005 1.0

Appendix B. Page 67 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 1.0

Plums 277 0 0.001 1.0

Summer Squash 698 43 6.2 0.001 - 0.33 0.001 - 0.010 1.0

Sweet Bell Peppers 328 41 12.5 0.006 - 0.21 0.005 1.0

Tangerines 531 0 0.010 1.0

Watermelon 175 4 2.3 0.011 - 0.041 0.010 1.0

Winter Squash 706 31 4.4 0.001 - 0.021 0.001 1.0

TOTAL 8,825 286

Metaldehyde (molluscicide) 

Carrots 708 0 0.055 NT

Eggplant 346 1 0.3 0.093 0.055 V-1 NT

Grape Juice 700 0 0.050 NT

TOTAL 1,754 1

Metamitron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Metconazole (fungicide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Methacrifos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 667 0 0.001 NT

TOTAL 1,732 0

Methamidophos (insecticide) (also a metabolite of Acephate)

Blueberries, Cultivated, Fresh 692 0 0.005 0.02 TP

Blueberries, Frozen 14 0 0.005 0.02 TP

Cantaloupe 328 0 0.005 0.02 TP

Carrots 708 0 0.035 0.02 TP

Cauliflower 531 9 1.7 0.005 - 0.030 0.004 2.0 TP

Celery 354 9 2.5 0.012 - 0.089 0.010 10 TP

Eggplant 703 0 0.001 - 0.035 0.02 TP

Grape Juice 700 0 0.025 0.02 TP

Green Beans 700 48 6.9 0.001 - 1.9 0.001 X-26 0.02 TP

Peaches 518 0 0.010 0.02 TP

Peaches, Frozen 154 0 0.010 0.02 TP

Pears 707 0 0.025 0.02 TP

Plums 277 0 0.005 0.02 TP

Summer Squash 698 0 0.001 - 0.020 0.02 TP

Sweet Bell Peppers 319 3 0.9 0.015 - 0.059 0.010 4.0 TP

Tangerines 531 0 0.10 0.02 TP

Watermelon 175 0 0.020 0.02 TP

Winter Squash 706 4 0.6 0.010 - 0.073 0.001 X-2 0.02 TP

TOTAL 8,815 73

Appendix B. Page 68 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Methfuroxam (fungicide) 

Summer Squash 365 0 0.001 NT

Winter Squash 639 0 0.001 NT

TOTAL 1,004 0

Methidathion (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.001 - 0.003 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.015 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 0.05 IT

Peaches, Frozen 154 0 0.010 0.05 IT

Pears 707 0 0.020 0.05 IT

Plums 277 0 0.010 0.05 IT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.002 6.0 IT

Winter Squash 706 0 0.003 NT

TOTAL 8,315 0

Methiocarb (insecticide)

Broccoli 708 0 0.001 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,766 0

Methiocarb sulfone (metabolite of Methiocarb)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,742 0

Methiocarb sulfoxide (metabolite of Methiocarb)

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Methomyl (insecticide) 

Blueberries, Cultivated, Fresh 692 10 1.4 0.032 - 1.0 0.030 6

Blueberries, Frozen 14 0 0.030 6

Broccoli 708 5 0.7 0.011 - 0.037 0.008 3

Cantaloupe 328 0 0.030 0.2

Carrots 708 0 0.015 0.2

Appendix B. Page 69 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cauliflower 531 4 0.8 0.009 - 0.26 0.008 6.0

Celery 354 18 5.1 0.010 - 0.082 0.010 3

Eggplant 703 13 1.8 0.011 - 0.24 0.002 - 0.015 0.2

Grape Juice 700 0 0.005 5 IT

Green Beans 700 21 3 0.013 - 1.5 0.010 2

Peaches 518 0 0.010 5

Peaches, Frozen 154 1 0.6 0.29 0.010 5

Pears 707 1 0.1 0.008 0.005 4 R

Plums 277 0 0.030 NT

Summer Squash 698 6 0.9 0.006 - 0.072 0.005 - 0.010 0.2

Sweet Bell Peppers 319 16 5 0.013 - 0.92 0.010 2

Tangerines 531 0 0.010 2

Watermelon 175 10 5.7 0.005 - 0.039 0.005 0.2

Winter Squash 706 1 0.1 0.027 0.010 0.2

TOTAL 9,523 106

Methomyl oxime (insecticide metabolite)

Carrots 708 0 0.10 0.2

Eggplant 346 0 0.10 0.2

Summer Squash 333 0 0.10 0.2

Tangerines 531 0 0.10 2

Watermelon 175 0 0.10 0.2

TOTAL 2,093 0

Methoprene (insect growth regulator) 

Broccoli 708 0 0.015 EX3

Carrots 708 0 0.060 EX3

Cauliflower 531 0 0.050 EX3

Eggplant 703 0 0.050 - 0.060 EX3

TOTAL 2,650 0

Methoprotryne (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Methoxychlor (insecticide) 

Broccoli 708 0 0.003 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.003 NT

Eggplant 703 0 0.003 - 0.020 NT

Green Beans 690 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 690 0 0.001 NT

TOTAL 4,395 0

Methoxychlor olefin (metabolite of Methoxychlor)

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Eggplant 357 0 0.001 NT

TOTAL 1,596 0

Methoxychlor p,p' (isomer of Methoxychlor)

Celery 354 0 0.005 NT

Peaches 518 0 0.005 NT

Appendix B. Page 70 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

TOTAL 1,354 0

Methoxyfenozide (insecticide) 

Blueberries, Cultivated, Fresh 692 31 4.5 0.004 - 0.28 0.003 3.0

Blueberries, Frozen 14 1 7.1 0.027 0.003 3.0

Broccoli 708 11 1.6 0.002 - 0.14 0.001 - 0.003 7.0

Cantaloupe 328 0 0.003 0.3

Carrots 708 0 0.010 - 0.020 0.90

Cauliflower 531 0 0.001 7.0

Celery 354 17 4.8 0.010 - 0.22 0.010 25

Eggplant 703 18 2.6 0.004 - 0.024 0.003 - 0.010 2.0

Grape Juice 700 479 68.4 0.002 - 0.031 0.001 1.0

Green Beans 700 25 3.6 0.003 - 0.27 0.003 1.5

Peaches 518 109 21 0.010 - 0.13 0.010 3.0

Peaches, Frozen 154 0 0.010 3.0

Pears 707 105 14.9 0.002 - 0.077 0.001 2.0

Plums 277 120 43.3 0.003 - 0.12 0.003 0.30

Summer Squash 698 6 0.9 0.003 - 0.012 0.002 - 0.003 0.3

Sweet Bell Peppers 319 16 5 0.010 - 0.076 0.010 2.0

Tangerines 531 0 0.010 3.0

Watermelon 175 0 0.002 0.3

Winter Squash 706 28 4 0.003 - 0.10 0.003 0.3

TOTAL 9,523 966

Metobromuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Metolachlor (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.001 0.40

Blueberries, Frozen 14 0 0.001 0.40

Broccoli 708 0 0.001 0.60

Cantaloupe 328 0 0.001 0.50

Carrots 708 0 0.010 0.40

Cauliflower 531 0 0.001 0.60

Celery 354 0 0.005 0.10

Eggplant 703 0 0.001 - 0.010 0.10

Green Beans 700 0 0.001 0.30

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.001 NT

Summer Squash 698 0 0.001 - 0.005 0.50

Sweet Bell Peppers 328 0 0.005 0.10

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.50

Winter Squash 706 0 0.001 0.50

TOTAL 8,125 0

Metolachlor oxanilic acid (OA) (herbicide metabolite)

Summer Squash 333 2 0.6 0.051 - 0.063 0.050 0.50

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.050 0.50

TOTAL 1,039 2

Appendix B. Page 71 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Metolcarb (insecticide, acaricide)

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 1,771 0

Metoxuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Metrafenone (fungicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 0.90

Grape Juice 700 0 0.005 4.5

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 0.70

Peaches, Frozen 154 0 0.010 0.70

Pears 707 0 0.005 1.5

Summer Squash 698 4 0.6 0.002 - 0.012 0.001 - 0.010 0.50

Sweet Bell Peppers 319 0 0.010 0.90

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 0.50

Winter Squash 706 7 1 0.002 - 0.016 0.001 0.50

TOTAL 6,616 11

Metribuzin (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 1 0.1 0.003 0.002 V-1 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.020 0.3

Cauliflower 531 0 0.002 NT

Eggplant 703 0 0.002 - 0.020 NT

Green Beans 700 0 0.005 NT

Plums 277 0 0.005 NT

Summer Squash 365 0 0.005 NT

Tangerines 531 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 6,263 1

Metsulfuron methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Mevinphos (insecticide) 

Broccoli 708 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.010 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Appendix B. Page 72 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.003 - 0.010 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 6,814 0

Mexacarbate (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

MGK-264 (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.10 5 FF

Blueberries, Frozen 14 0 0.10 5 FF

Broccoli 708 0 0.002 5 FF

Cantaloupe 328 0 0.10 5 FF

Carrots 708 0 0.015 5 FF

Cauliflower 531 0 0.002 5 FF

Celery 354 0 0.010 5 FF

Eggplant 703 0 0.005 - 0.015 5 FF

Grape Juice 700 0 0.006 5 FF

Green Beans 700 0 0.001 5 FF

Peaches 417 0 0.010 5 FF

Peaches, Frozen 149 0 0.010 5 FF

Plums 277 0 0.10 5 FF

Summer Squash 698 0 0.001 - 0.025 5 FF

Sweet Bell Peppers 319 0 0.010 5 FF

Tangerines 531 0 0.025 5 FF

Watermelon 175 0 0.025 5 FF

Winter Squash 706 0 0.001 5 FF

TOTAL 8,710 0

MGK-326 (insecticide) 

Carrots 708 0 0.015 NT

Eggplant 346 0 0.015 NT

TOTAL 1,054 0

Molinate (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Monocrotophos (insecticide) 

Carrots 708 0 0.020 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.003 NT

Peaches 500 0 0.010 NT

Peaches, Frozen 152 0 0.010 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,150 0

Appendix B. Page 73 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Monolinuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Monuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Myclobutanil (fungicide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.086 0.003 V-1 NT

Blueberries, Frozen 14 0 0.003 NT

Broccoli 708 0 0.003 0.03 IN

Cantaloupe 328 5 1.5 0.003 - 0.007 0.003 0.20

Carrots 708 51 7.2 0.001 - 0.006 0.001 0.03 IN

Cauliflower 531 0 0.001 0.03 IN

Celery 354 1 0.3 0.005 0.005 0.03 IN

Eggplant 703 6 0.9 0.002 - 0.010 0.001 4.0

Grape Juice 700 0 0.004 1.0

Green Beans 700 50 7.1 0.003 - 0.096 0.003 1.0

Peaches 518 31 6 0.005 - 0.17 0.005 2.0

Peaches, Frozen 154 2 1.3 0.006 - 0.009 0.005 2.0

Pears 707 2 0.3 0.007 0.004 V-2 NT

Plums 277 0 0.003 2.0

Summer Squash 698 22 3.2 0.003 - 0.044 0.003 - 0.010 0.20

Sweet Bell Peppers 328 23 7 0.006 - 0.062 0.005 4.0

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 0.20

Winter Squash 706 29 4.1 0.003 - 0.021 0.003 0.20

TOTAL 9,532 223

Naled (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.020 0.5 FF

Blueberries, Frozen 14 0 0.020 0.5 FF

Carrots 708 0 0.20 0.5 FF

Eggplant 346 0 0.20 0.5

Grape Juice 700 0 0.015 0.5 FF

Plums 277 0 0.020 0.5 FF

TOTAL 2,737 0

1-Naphthol (metabolite of Carbaryl)

Blueberries, Cultivated, Fresh 692 1 0.1 0.095 0.015 3.0 TP

Blueberries, Frozen 14 0 0.015 3.0 TP

Cantaloupe 162 0 0.015 3.0 TP

Carrots 708 0 0.20 2.0 TP

Eggplant 346 1 0.3 0.20 0.20 5.0 TP

Grape Juice 700 0 0.25 10 TP

Pears 707 0 0.25 12 TP

Plums 277 0 0.015 - 0.030 10 TP

TOTAL 3,606 2

Napropamide (herbicide) 

Broccoli 708 0 0.002 0.1

Carrots 708 0 0.010 NT

Appendix B. Page 74 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cauliflower 531 0 0.002 0.1

Celery 354 0 0.010 NT

Eggplant 703 0 0.002 - 0.010 0.1

Grape Juice 700 0 0.002 0.1

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 698 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 0.1

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,505 0

Neburon (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Nicosulfuron (herbicide) 

Summer Squash 218 0 0.005 NT

Tangerines 400 0 0.005 NT

Watermelon 175 0 0.005 NT

TOTAL 793 0

Nitenpyram (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Nitrapyrin (nitrification inhibitor) 

Summer Squash 698 0 0.003 - 0.005 NT

Tangerines 531 0 0.005 0.06

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,110 0

Nitrofen (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Norflurazon (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 0.2

Blueberries, Frozen 14 0 0.002 0.2

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.005 NT

Grape Juice 700 0 0.015 0.1

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 0.1

Appendix B. Page 75 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.010 0.1

Pears 707 0 0.015 0.1

Plums 277 0 0.002 0.1

Summer Squash 698 0 0.003 - 0.010 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.010 0.2

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 9,523 0

Norflurazon desmethyl (metabolite of Norflurazon)

Blueberries, Cultivated, Fresh 692 0 0.005 0.2

Blueberries, Frozen 14 0 0.005 0.2

Broccoli 708 2 0.3 0.002 0.001 - 0.003 V-2 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.010 NT

Cauliflower 531 1 0.2 0.002 0.001 V-1 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.010 0.1

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 0.1

Peaches, Frozen 154 0 0.010 0.1

Plums 277 0 0.005 0.1

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 0.2

Winter Squash 706 0 0.003 NT

TOTAL 8,308 3

Novaluron (insecticide) 

Blueberries, Cultivated, Fresh 692 5 0.7 0.018 - 0.38 0.009 7.0

Blueberries, Frozen 14 0 0.009 7.0

Broccoli 708 10 1.4 0.002 - 0.042 0.001 - 0.003 0.7

Cantaloupe 328 0 0.009 0.20

Carrots 708 0 0.010 0.05

Cauliflower 531 1 0.2 0.002 0.001 - 0.003 0.7

Celery 354 1 0.3 0.063 0.010 X-1 0.01 FF

Eggplant 682 10 1.5 0.002 - 0.031 0.001 - 0.010 2

Grape Juice 700 0 0.003 0.01 FF

Green Beans 700 47 6.7 0.003 - 0.11 0.003 0.70

Peaches 518 7 1.4 0.013 - 0.13 0.010 1.9

Peaches, Frozen 154 0 0.010 1.9

Pears 707 166 23.5 0.005 - 0.92 0.003 3.0

Plums 277 0 0.009 - 0.017 1.9

Summer Squash 698 4 0.6 0.009 - 0.028 0.003 - 0.005 0.20

Sweet Bell Peppers 319 17 5.3 0.011 - 0.046 0.010 2

Tangerines 531 0 0.025 0.01 FF

Winter Squash 706 16 2.3 0.003 - 0.032 0.003 0.20

TOTAL 9,327 284

Nuarimol (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Appendix B. Page 76 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Octhilinone (fungicide) 

Green Beans 431 0 0.005 NT

Summer Squash 160 0 0.005 NT

Winter Squash 376 0 0.005 NT

TOTAL 967 0

Omethoate (insecticide) (also a metabolite of Dimethoate)

Blueberries, Cultivated, Fresh 692 1 0.1 0.028 0.020 1.0 TP

Blueberries, Frozen 14 0 0.020 1.0 TP

Broccoli 708 1 0.1 0.004 0.002 2.0 TP

Cantaloupe 328 0 0.020 1.0 TP

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 2.0 TP

Celery 354 9 2.5 0.011 - 0.039 0.010 2.0 TP

Eggplant 703 2 0.3 0.016 - 0.019 0.002 - 0.010 V-2 NT

Green Beans 700 36 5.1 0.001 - 0.086 0.001 2.0 TP

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 0 0.005 2.0 TP

Plums 277 0 0.020 NT

Summer Squash 698 0 0.001 - 0.015 NT

Sweet Bell Peppers 319 0 0.010 2.0 TP

Tangerines 531 0 0.030 2.0 TP

Watermelon 175 0 0.015 1.0 TP

Winter Squash 706 1 0.1 0.006 0.001 V-1 NT

TOTAL 8,823 50

Oryzalin (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.020 0.05

Blueberries, Frozen 14 0 0.020 0.05

Cantaloupe 328 0 0.020 NT

Carrots 708 0 0.10 NT

Celery 354 0 0.020 NT

Eggplant 346 0 0.10 NT

Grape Juice 700 0 0.008 0.05

Peaches 518 0 0.020 0.05

Peaches, Frozen 154 0 0.020 0.05

Pears 707 0 0.008 0.05

Plums 247 0 0.020 0.05

Sweet Bell Peppers 319 0 0.10 NT

Tangerines 531 0 0.20 0.05

TOTAL 5,618 0

Oxadiazon (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,805 0

Oxadixyl (fungicide) 

Broccoli 708 0 0.003 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.010 NT

Eggplant 357 0 0.003 - 0.010 NT

Appendix B. Page 77 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,712 0

Oxamyl (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.003 NT

Blueberries, Frozen 14 0 0.003 NT

Cantaloupe 328 0 0.003 2.0

Carrots 708 0 0.005 0.1

Cauliflower 531 0 0.006 NT

Celery 354 10 2.8 0.010 - 0.047 0.010 10.0

Eggplant 346 9 2.6 0.005 - 0.088 0.005 2.0

Green Beans 700 1 0.1 0.005 0.005 V-1 NT

Peaches 500 0 0.010 NT

Peaches, Frozen 152 0 0.010 NT

Pears 707 0 0.015 2.0

Plums 246 0 0.003 NT

Summer Squash 698 22 3.2 0.005 - 1.5 0.005 2.0

Sweet Bell Peppers 319 22 6.9 0.012 - 0.18 0.010 2.0

Tangerines 531 0 0.005 3

Watermelon 175 1 0.6 0.017 0.005 2.0

Winter Squash 706 0 0.005 2.0

TOTAL 7,707 65

Oxamyl oxime (metabolite of Oxamyl)

Blueberries, Cultivated, Fresh 692 0 0.007 NT

Blueberries, Frozen 14 0 0.007 NT

Cantaloupe 328 24 7.3 0.008 - 0.15 0.007 2.0

Carrots 708 0 0.040 0.1

Celery 354 6 1.7 0.011 - 0.036 0.010 10.0

Eggplant 346 11 3.2 0.041 - 0.19 0.040 2.0

Green Beans 700 0 0.005 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.007 NT

Summer Squash 698 12 1.7 0.006 - 0.76 0.005 - 0.050 2.0

Sweet Bell Peppers 319 81 25.4 0.010 - 0.46 0.010 2.0

Tangerines 531 0 0.050 3

Watermelon 175 1 0.6 0.054 0.050 2.0

Winter Squash 706 1 0.1 0.063 0.005 2.0

TOTAL 6,520 136

Oxathiapiprolin (fungicide) 

Carrots 708 0 0.020 - 0.10 0.10 IN

Eggplant 346 0 0.020 0.50

Grape Juice 700 0 0.003 0.70 FU

Green Beans 700 0 0.001 0.10 IN

Summer Squash 698 0 0.001 - 0.010 0.20

Tangerines 531 0 0.010 0.06

Watermelon 175 0 0.010 0.20

Winter Squash 706 6 0.8 0.001 - 0.006 0.001 0.20

TOTAL 4,564 6

Appendix B. Page 78 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oxycarboxin (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Oxydemeton methyl (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Cantaloupe 328 0 0.002 0.2

Carrots 708 0 0.005 NT

Celery 353 0 0.010 NT

Eggplant 346 0 0.005 1.0

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.002 NT

Summer Squash 365 0 0.001 1.0

Sweet Bell Peppers 319 0 0.010 0.75

Winter Squash 706 0 0.001 0.3

TOTAL 5,480 0

Oxydemeton methyl sulfone (metabolite of Oxydemeton methyl)

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Cantaloupe 328 0 0.002 0.2

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 1.0

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.002 NT

Summer Squash 698 0 0.001 - 0.020 1.0

Sweet Bell Peppers 319 0 0.010 0.75

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 0.2

Winter Squash 706 0 0.001 0.3

TOTAL 6,520 0

Oxyfluorfen (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.050 NT

Blueberries, Frozen 14 0 0.050 NT

Broccoli 708 6 0.8 0.002 0.001 - 0.003 0.05

Cantaloupe 327 0 0.050 NT

Carrots 708 0 0.040 NT

Cauliflower 531 0 0.001 - 0.003 0.05

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.040 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 0.05

Peaches, Frozen 154 0 0.005 0.05

Plums 246 0 0.050 0.05

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,054 6

Appendix B. Page 79 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Paclobutrazol (plant growth regulator) 

Carrots 708 0 0.010 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Parathion (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.003 - 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,086 0

Parathion oxygen analog (metabolite of Parathion)

Broccoli 708 0 0.001 NT

Carrots 708 0 0.005 NT

Cauliflower 531 1 0.2 0.003 0.001 V-1 NT

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,421 1

Parathion methyl (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.002 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Appendix B. Page 80 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,125 0

Parathion methyl oxygen analog (metabolite of Parathion methyl)

Blueberries, Cultivated, Fresh 692 0 0.020 NT

Blueberries, Frozen 14 0 0.020 NT

Cantaloupe 328 0 0.020 NT

Carrots 708 0 0.025 NT

Eggplant 346 0 0.025 NT

Green Beans 700 0 0.010 NT

Plums 277 0 0.020 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 4,136 0

Pebulate (herbicide) 

Celery 354 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

TOTAL 1,354 0

Penconazole (fungicide) 

Carrots 708 0 0.010 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Pencycuron (fungicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,170 0

Pendimethalin (herbicide) 

Blueberries, Cultivated, Fresh 663 0 0.050 0.1

Blueberries, Frozen 13 0 0.050 0.1

Broccoli 708 26 3.7 0.002 - 0.014 0.001 0.1

Cantaloupe 328 0 0.050 0.10

Carrots 708 0 0.020 0.5

Cauliflower 531 0 0.001 0.1

Celery 354 3 0.8 0.007 - 0.009 0.005 0.2

Eggplant 703 0 0.001 - 0.020 0.1

Appendix B. Page 81 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grape Juice 700 0 0.007 0.1

Green Beans 700 14 2 0.001 - 0.007 0.001 0.10

Peaches 518 2 0.4 0.005 - 0.008 0.005 0.1

Peaches, Frozen 154 0 0.005 0.1

Pears 707 1 0.1 0.037 0.007 0.1

Plums 277 0 0.050 0.1

Summer Squash 698 5 0.7 0.001 - 0.002 0.001 - 0.005 V-5 NT

Sweet Bell Peppers 328 0 0.005 0.1

Tangerines 531 0 0.005 0.1

Watermelon 175 0 0.005 0.10

Winter Squash 706 4 0.6 0.002 - 0.007 0.001 V-4 NT

TOTAL 9,502 55

Penflufen (fungicide) 

Green Beans 700 0 0.001 0.01

Summer Squash 698 0 0.001 NT

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,810 0

Penoxsulam (herbicide) 

Celery 354 0 0.010 NT

Grape Juice 700 0 0.002 0.01

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 0.01

Peaches, Frozen 154 0 0.010 0.01

Pears 707 0 0.002 0.01

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,523 0

Pentachloroaniline - PCA (metabolite of Quintozene)

Blueberries, Cultivated, Fresh 692 0 0.004 NT

Blueberries, Frozen 14 0 0.004 NT

Broccoli 708 6 0.8 0.002 - 0.010 0.001 0.1

Cantaloupe 328 0 0.004 NT

Carrots 708 4 0.6 0.005 - 0.010 0.005 V-4 NT

Cauliflower 531 0 0.001 0.1

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.005 0.1

Green Beans 700 0 0.001 0.1

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.004 NT

Summer Squash 698 12 1.7 0.001 - 0.010 0.001 - 0.005 V-12 NT

Sweet Bell Peppers 328 2 0.6 0.005 - 0.014 0.005 0.1

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 7 1 0.001 - 0.006 0.001 V-7 NT

TOTAL 8,125 31

Pentachlorobenzene - PCB (metabolite of Quintozene)

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Broccoli 708 0 0.003 - 0.010 0.1

Appendix B. Page 82 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.002 NT

Cauliflower 531 0 0.003 - 0.010 0.1

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.010 0.1

Green Beans 700 0 0.001 0.1

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.005 NT

Summer Squash 698 2 0.3 0.007 - 0.008 0.001 - 0.002 V-2 NT

Sweet Bell Peppers 328 0 0.005 0.1

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,125 2

Pentachlorophenyl methyl sulfide - PCPMS (metabolite of Quintozene)

Broccoli 708 1 0.1 0.002 0.001 0.1

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.003 0.1

Celery 354 0 0.005 NT

Eggplant 294 0 0.010 0.1

Green Beans 700 0 0.003 0.1

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.003 - 0.015 NT

Sweet Bell Peppers 328 0 0.005 0.1

Tangerines 531 0 0.015 NT

Watermelon 175 0 0.015 NT

Winter Squash 706 0 0.003 NT

TOTAL 6,405 1

Penthiopyrad (fungicide) 

Broccoli 621 8 1.3 0.002 - 0.24 0.001 - 0.003 5

Carrots 708 36 5.1 0.001 - 0.067 0.001 3.0

Cauliflower 488 0 0.001 - 0.006 5

Celery 354 18 5.1 0.010 - 0.14 0.010 30

Eggplant 703 15 2.1 0.001 - 0.034 0.001 3.0

Green Beans 700 49 7 0.001 - 0.11 0.001 4.0

Peaches 518 21 4.1 0.010 - 0.20 0.010 4

Peaches, Frozen 154 0 0.010 4

Pears 707 0 0.001 0.50

Summer Squash 698 6 0.9 0.001 - 0.006 0.001 0.60

Sweet Bell Peppers 319 23 7.2 0.010 - 0.20 0.010 3.0

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 0.60

Winter Squash 706 5 0.7 0.002 - 0.004 0.001 0.60

TOTAL 7,382 181

Permethrin Total (insecticide)

Celery 354 171 48.3 0.005 - 0.27 0.005 5

Green Beans 700 8 1.1 0.004 - 0.076 0.003 V-8 NT

Peaches 518 15 2.9 0.029 - 0.42 0.005 2

Peaches, Frozen 154 0 0.005 2

Summer Squash 698 0 0.003 - 0.050 1.5

Sweet Bell Peppers 328 13 4 0.006 - 0.054 0.005 0.50

Tangerines 531 0 0.050 NT

Appendix B. Page 83 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 0 0.050 1.5

Winter Squash 706 15 2.1 0.003 - 0.015 0.003 1.5

TOTAL 4,164 222

Permethrin cis (isomer of Permethrin)

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 50 7.1 0.002 - 0.13 0.001 2.0

Cantaloupe 328 0 0.010 1.5

Carrots 708 0 0.010 NT

Cauliflower 531 4 0.8 0.002 - 0.012 0.001 0.5

Eggplant 703 35 5 0.002 - 0.12 0.001 - 0.010 0.50

Grape Juice 700 0 0.007 2 R

Pears 707 0 0.007 0.05

Plums 277 0 0.010 NT

TOTAL 5,368 89

Permethrin trans (isomer of Permethrin)

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 44 6.2 0.002 - 0.14 0.001 2.0

Cantaloupe 328 0 0.010 1.5

Carrots 708 0 0.010 NT

Cauliflower 531 4 0.8 0.002 0.001 0.5

Eggplant 703 33 4.7 0.002 - 0.12 0.001 - 0.010 0.50

Grape Juice 700 0 0.007 2 R

Pears 707 0 0.007 0.05

Plums 277 0 0.010 NT

TOTAL 5,368 81

Phenmedipham (herbicide) 

Summer Squash 333 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

TOTAL 1,039 0

Phenothrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.050 0.01 FF

Blueberries, Frozen 14 0 0.050 0.01 FF

Broccoli 708 0 0.002 0.01 FF

Cantaloupe 328 0 0.050 0.01 FF

Carrots 708 0 0.075 0.01 FF

Cauliflower 531 0 0.002 0.01 FF

Celery 354 0 0.005 0.01 FF

Eggplant 703 0 0.002 - 0.075 0.01 FF

Grape Juice 700 0 0.015 0.01 FF

Green Beans 700 0 0.010 0.01 FF

Peaches 518 0 0.005 0.01 FF

Peaches, Frozen 154 0 0.005 0.01 FF

Pears 707 0 0.015 0.01 FF

Plums 277 0 0.050 0.01 FF

Summer Squash 698 0 0.010 - 0.025 0.01 FF

Sweet Bell Peppers 328 0 0.005 0.01 FF

Tangerines 531 0 0.025 0.01 FF

Watermelon 175 0 0.025 0.01 FF

Winter Squash 706 0 0.010 0.01 FF

TOTAL 9,532 0

Appendix B. Page 84 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Phenthoate (insecticide) 

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Eggplant 357 0 0.001 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,367 0

o-Phenylphenol (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Cantaloupe 328 7 2.1 0.005 - 0.035 0.005 10 PH

Carrots 708 0 0.040 20 PH

Eggplant 346 0 0.040 NT

Pears 707 41 5.8 0.003 - 6.1 0.002 25.0 PH

Plums 277 0 0.005 20 PH

TOTAL 3,072 48

Phorate (insecticide) 

Broccoli 708 0 0.003 NT

Carrots 708 0 0.085 NT

Cauliflower 531 0 0.001 - 0.003 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.003 - 0.085 NT

Green Beans 700 0 0.003 0.05

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.003 - 0.030 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.030 NT

Watermelon 175 0 0.030 NT

Winter Squash 706 0 0.003 NT

TOTAL 6,814 0

Phorate oxygen analog (metabolite of Phorate)

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Eggplant 357 0 0.001 NT

Green Beans 700 0 0.005 0.05

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 3,367 0

Phorate oxygen analog sulfone (metabolite of Phorate)

Broccoli 708 0 0.001 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 0.05

Summer Squash 698 0 0.001 - 0.010 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,460 0

Appendix B. Page 85 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Phorate oxygen analog sulfoxide (metabolite of Phorate)

Broccoli 708 0 0.001 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 NT

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.001 0.05

Summer Squash 698 0 0.001 - 0.010 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,460 0

Phorate sulfone (metabolite of Phorate)

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.002 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.030 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.030 NT

Green Beans 700 0 0.003 0.05

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.003 - 0.025 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.025 NT

Winter Squash 706 0 0.003 NT

TOTAL 8,125 0

Phorate sulfoxide (metabolite of Phorate)

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 0.05

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.001 - 0.002 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,116 0

Phosalone (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Broccoli 708 0 0.005 NT

Cantaloupe 328 0 0.001 NT

Appendix B. Page 86 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carrots 708 0 0.015 NT

Cauliflower 531 0 0.002 - 0.005 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.015 NT

Grape Juice 700 0 0.015 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 707 0 0.015 NT

Plums 277 0 0.001 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 8,493 0

Phosmet (insecticide) 

Blueberries, Cultivated, Fresh 692 78 11.3 0.010 - 1.6 0.010 10

Blueberries, Frozen 14 4 28.6 0.019 - 0.10 0.010 10

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.025 NT

Celery 354 0 0.005 NT

Eggplant 616 0 0.005 - 0.025 NT

Grape Juice 700 6 0.9 0.012 0.007 10

Green Beans 700 0 0.001 NT

Peaches 518 9 1.7 0.009 - 0.16 0.005 10

Peaches, Frozen 154 0 0.005 10

Pears 707 0 0.007 10

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.020 5

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,873 97

Phosmet oxygen analog (metabolite of Phosmet)

Blueberries, Cultivated, Fresh 692 2 0.3 0.006 - 0.008 0.004 10

Blueberries, Frozen 14 1 7.1 0.015 0.004 10

Cantaloupe 328 0 0.004 NT

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Grape Juice 700 0 0.005 10

Green Beans 700 0 0.001 NT

Pears 707 0 0.005 10

Plums 277 0 0.004 NT

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 5

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,582 3

Phosphamidon (insecticide) 

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 357 0 0.001 NT

Green Beans 700 0 0.005 NT

Appendix B. Page 87 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.005 NT

TOTAL 4,712 0

Phoxim (insecticide) 

Carrots 708 0 0.025 NT

Eggplant 346 0 0.025 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,825 0

Picolinafen (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Picoxystrobin (fungicide) 

Broccoli 708 0 0.001 - 0.003 2.0

Carrots 708 0 0.001 0.50

Cauliflower 424 0 0.001 - 0.006 2.0

Eggplant 703 0 0.001 0.70

Green Beans 700 0 0.005 2.0

Summer Squash 698 0 0.005 0.30

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 0.30

Winter Squash 706 0 0.005 0.30

TOTAL 5,353 0

Pinoxaden (herbicide) 

Green Beans 528 0 0.020 NT

Summer Squash 284 0 0.020 NT

Winter Squash 588 0 0.020 NT

TOTAL 1,400 0

Piperonyl butoxide (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.005 10 FF

Blueberries, Frozen 14 0 0.005 10 FF

Broccoli 708 1 0.1 0.003 0.002 10 FF

Cantaloupe 328 0 0.005 10 FF

Carrots 708 0 0.015 10 FF

Cauliflower 531 0 0.002 10 FF

Celery 354 3 0.8 0.007 - 0.025 0.005 10 FF

Eggplant 703 0 0.002 - 0.015 10 FF

Grape Juice 700 1 0.1 0.007 0.004 10 FF

Green Beans 700 2 0.3 0.008 - 0.033 0.003 10 FF

Peaches 518 0 0.005 10 FF

Peaches, Frozen 154 0 0.005 10 FF

Pears 707 0 0.004 10 FF

Plums 277 0 0.005 10 FF

Summer Squash 698 0 0.003 - 0.025 10 FF

Sweet Bell Peppers 328 1 0.3 0.045 0.005 10 FF

Tangerines 531 0 0.025 10 FF

Appendix B. Page 88 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Watermelon 175 0 0.025 10 FF

Winter Squash 706 0 0.003 10 FF

TOTAL 9,532 8

Pirimicarb (insecticide) 

Broccoli 708 0 0.001 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,766 0

Pirimicarb desmethyl (metabolite of Pirimicarb)

Carrots 708 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.001 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,170 0

Pirimiphos ethyl (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Pirimiphos methyl (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.001 NT

Carrots 708 0 0.010 NT

Cauliflower 531 1 0.2 0.005 0.001 V-1 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.001 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,086 1

Prallethrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.008 1.0 FF

Blueberries, Frozen 14 0 0.008 1.0 FF

Appendix B. Page 89 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.008 1.0 FF

Carrots 708 0 0.045 1.0 FF

Celery 354 0 0.010 1.0 FF

Eggplant 346 0 0.045 1.0 FF

Grape Juice 700 0 0.005 1.0 FF

Green Beans 700 0 0.020 1.0 FF

Peaches 518 0 0.010 1.0 FF

Peaches, Frozen 154 0 0.010 1.0 FF

Pears 707 0 0.005 1.0 FF

Plums 277 0 0.008 1.0 FF

Summer Squash 365 0 0.020 1.0 FF

Sweet Bell Peppers 319 0 0.010 1.0 FF

Tangerines 531 0 0.030 1.0 FF

Winter Squash 706 0 0.020 1.0 FF

TOTAL 7,419 0

Pretilachlor (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Primisulfuron methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Prochloraz (fungicide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 3,125 0

Procymidone (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,490 0

Prodiamine (herbicide) 

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

TOTAL 1,054 0

Appendix B. Page 90 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Profenofos (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.075 NT

Blueberries, Frozen 14 0 0.075 NT

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.075 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 4 0.6 0.002 - 0.009 0.001 V-4 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.075 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,116 4

Profluralin (herbicide) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Promecarb (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Prometon (herbicide) 

Broccoli 708 1 0.1 0.002 0.001 V-1 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Eggplant 703 0 0.001 - 0.010 NT

TOTAL 2,650 1

Prometryn (herbicide) 

Broccoli 708 3 0.4 0.002 0.001 V-3 NT

Carrots 708 3 0.4 0.017 - 0.039 0.010 0.45

Cauliflower 531 1 0.2 0.002 0.001 V-1 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 0.05

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,421 7

Pronamide (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.002 0.05

Blueberries, Frozen 14 0 0.002 0.05

Broccoli 708 44 6.2 0.002 - 0.008 0.001 - 0.003 V-44 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 1 0.2 0.002 0.001 V-1 NT

Appendix B. Page 91 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Celery 354 1 0.3 0.005 0.005 V-1 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.010 0.1

Green Beans 700 1 0.1 0.002 0.001 V-1 NT

Peaches 518 0 0.005 0.1

Peaches, Frozen 154 0 0.005 0.1

Pears 707 0 0.010 0.1

Plums 277 0 0.002 0.1

Summer Squash 698 1 0.1 0.006 0.001 - 0.005 V-1 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 9,532 48

Propachlor (herbicide) 

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Eggplant 357 0 0.001 - 0.003 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,367 0

Propamocarb (fungicide) 

Celery 354 1 0.3 0.010 0.010 V-1 NT

Green Beans 700 11 1.6 0.001 - 0.12 0.001 V-11 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 19 5.2 0.001 - 0.41 0.001 1.5

Sweet Bell Peppers 319 22 6.9 0.010 - 0.64 0.010 4

Winter Squash 706 55 7.8 0.002 - 0.34 0.001 1.5

TOTAL 3,116 108

Propamocarb hydrochloride 4 (fungicide) 

Blueberries, Cultivated, Fresh 664 0 0.002 NT

Blueberries, Frozen 12 0 0.002 NT

Cantaloupe 328 69 21 0.002 - 0.018 0.002 1.5

Carrots 708 1 0.1 0.008 0.005 V-1 NT

Eggplant 346 6 1.7 0.005 - 0.053 0.005 4

Plums 277 0 0.002 NT

Summer Squash 333 25 7.5 0.001 - 0.16 0.001 1.5

Tangerines 531 0 0.001 NT

Watermelon 175 5 2.9 0.001 - 0.002 0.001 1.5

TOTAL 3,374 106

Propanil (herbicide) 

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Propaquizafop (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Appendix B. Page 92 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Propargite (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.050 NT

Blueberries, Frozen 14 0 0.050 NT

Broccoli 708 0 0.006 NT

Cantaloupe 328 0 0.050 NT

Carrots 708 0 0.040 NT

Cauliflower 531 0 0.006 - 0.020 NT

Celery 354 0 0.020 NT

Eggplant 703 0 0.006 - 0.040 NT

Grape Juice 700 0 0.008 10.0

Green Beans 700 1 0.1 0.002 0.001 V-1 NT

Peaches 518 0 0.020 NT

Peaches, Frozen 154 0 0.020 NT

Pears 707 0 0.008 NT

Plums 277 0 0.050 NT

Summer Squash 698 0 0.001 - 0.025 NT

Sweet Bell Peppers 328 0 0.020 NT

Tangerines 531 0 0.025 NT

Watermelon 175 0 0.025 NT

Winter Squash 706 0 0.001 NT

TOTAL 9,532 1

Propazine (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Propetamphos (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.001 - 0.003 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.001 - 0.020 NT

Grape Juice 700 0 0.005 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 8,308 0

Propham (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Propiconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 2 0.3 0.020 - 0.047 0.010 1.3

Blueberries, Frozen 14 0 0.010 1.3

Appendix B. Page 93 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 1 0.1 0.022 0.005 - 0.015 V-1 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.020 0.3

Cauliflower 531 0 0.005 NT

Celery 354 108 30.5 0.010 - 0.14 0.010 5

Eggplant 703 0 0.005 - 0.020 NT

Green Beans 700 5 0.7 0.001 - 0.051 0.001 0.70

Peaches 518 208 40.2 0.010 - 4.3 0.010 X-1 4.0

Peaches, Frozen 154 12 7.8 0.010 - 0.051 0.010 4.0

Plums 277 40 14.4 0.010 - 0.23 0.010 0.60

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 84 15.8 0.005 - 0.13 0.005 8.0

Watermelon 175 0 0.005 NT

Winter Squash 706 2 0.3 0.001 0.001 V-2 NT

TOTAL 8,116 462

Proquinazid (fungicide) 

Grape Juice 700 0 0.002 0.50 FU

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 2,471 0

Prosulfuron (herbicide) 

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.003 - 0.010 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,864 0

Prothioconazole (fungicide) 

Summer Squash 246 0 0.10 0.30

Tangerines 531 0 0.10 NT

Watermelon 175 0 0.10 0.30

TOTAL 952 0

Prothioconazole desthio (metabolite of Prothioconazole) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 0.30

Winter Squash 706 6 0.8 0.001 - 0.005 0.001 0.30

TOTAL 1,771 6

Prothiofos (insecticide) 

Carrots 708 0 0.040 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.040 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,150 0

Appendix B. Page 94 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pydiflumetofen (fungicide) 

Carrots 708 0 0.010 0.5

Eggplant 346 1 0.3 0.021 0.010 0.60

Grape Juice 700 0 0.015 1.5

Green Beans 700 3 0.4 0.002 - 0.007 0.001 1

Pears 707 0 0.015 0.2

Summer Squash 698 24 3.4 0.004 - 0.063 0.001 - 0.005 0.50

Tangerines 531 0 0.005 1

Watermelon 175 0 0.005 0.50

Winter Squash 706 42 5.9 0.001 - 0.18 0.001 0.50

TOTAL 5,271 70

Pymetrozine (insecticide) 

Broccoli 708 0 0.005 0.5

Carrots 708 0 0.085 NT

Cauliflower 531 0 0.005 0.5

Celery 354 0 0.010 0.6

Eggplant 703 0 0.005 - 0.085 0.2

Green Beans 700 1 0.1 0.003 0.001 V-1 NT

Peaches 500 0 0.010 NT

Peaches, Frozen 152 0 0.010 NT

Summer Squash 365 0 0.001 0.1

Sweet Bell Peppers 319 2 0.6 0.010 - 0.012 0.010 0.2

Winter Squash 706 0 0.001 0.1

TOTAL 5,746 3

Pyraclofos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Pyraclostrobin (fungicide) 

Blueberries, Cultivated, Fresh 692 130 18.8 0.003 - 0.56 0.003 4.0

Blueberries, Frozen 14 5 35.7 0.008 - 0.021 0.003 4.0

Broccoli 708 64 9 0.002 - 1.0 0.001 - 0.003 5.0

Cantaloupe 328 0 0.003 0.5

Carrots 708 72 10.2 0.005 - 0.046 0.005 0.4

Cauliflower 531 0 0.001 5.0

Celery 354 40 11.3 0.003 - 0.075 0.003 29

Eggplant 703 18 2.6 0.002 - 0.028 0.001 - 0.005 1.4

Grape Juice 700 0 0.002 2.0

Green Beans 700 143 20.4 0.001 - 0.20 0.001 0.5

Peaches 518 100 19.3 0.003 - 0.13 0.003 2.5

Peaches, Frozen 154 0 0.003 2.5

Pears 707 100 14.1 0.003 - 0.18 0.002 1.5

Plums 277 1 0.4 0.004 0.003 2.5

Summer Squash 698 67 9.6 0.001 - 0.033 0.001 0.5

Sweet Bell Peppers 319 65 20.4 0.003 - 0.12 0.003 1.4

Tangerines 531 5 0.9 0.002 - 0.012 0.001 2.0

Watermelon 175 0 0.001 0.5

Winter Squash 706 38 5.4 0.001 - 0.006 0.001 0.5

TOTAL 9,523 848

Pyraflufen ethyl (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Appendix B. Page 95 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.030 NT

Eggplant 346 0 0.030 NT

Grape Juice 700 0 0.003 0.01

Green Beans 700 0 0.001 NT

Pears 707 0 0.003 0.01

Plums 277 0 0.010 0.01

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,543 0

Pyrazon (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Pyrazophos (fungicide) 

Carrots 708 0 0.010 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,170 0

Pyrethrins (insecticide) 

Carrots 708 0 0.20 1.0 FF

Eggplant 346 0 0.20 1.0 FF

Green Beans 700 0 0.005 1.0 PH

Summer Squash 365 0 0.005 1.0 FF

Winter Squash 706 0 0.005 1.0 FF

TOTAL 2,825 0

Pyridaben (insecticide, acaricide)

Blueberries, Cultivated, Fresh 692 0 0.005 2.5

Blueberries, Frozen 14 0 0.005 2.5

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.001 NT

Grape Juice 700 0 0.001 2.0

Green Beans 700 0 0.001 NT

Peaches 518 3 0.6 0.008 - 0.011 0.005 3.0

Peaches, Frozen 154 0 0.005 3.0

Pears 707 6 0.8 0.002 - 0.016 0.001 0.75

Plums 277 0 0.005 3.0

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 0.9

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,936 9

Appendix B. Page 96 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pyridalyl (insecticide) 

Carrots 708 0 0.020 NT

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 143 0 0.005 NT

Winter Squash 706 2 0.3 0.003 - 0.009 0.001 V-2 NT

TOTAL 3,486 2

Pyridaphenthion (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Pyrifluquinazon (insecticide) 

Grape Juice 700 0 0.001 0.30

Green Beans 700 0 0.001 NT

Pears 707 0 0.001 0.07

Summer Squash 698 0 0.001 - 0.005 0.07

Tangerines 531 0 0.005 0.70

Watermelon 175 0 0.005 0.07

Winter Squash 706 0 0.001 0.07

TOTAL 4,217 0

Pyrimethanil (fungicide) 

Blueberries, Cultivated, Fresh 692 31 4.5 0.051 - 1.0 0.050 8.0

Blueberries, Frozen 14 0 0.050 8.0

Broccoli 708 1 0.1 0.006 0.001 V-1 NT

Cantaloupe 328 0 0.050 NT

Carrots 708 3 0.4 0.010 - 0.018 0.005 V-3 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.003 NT

Eggplant 703 0 0.001 - 0.005 NT

Grape Juice 700 11 1.6 0.003 - 0.022 0.002 5.0

Green Beans 700 2 0.3 0.27 - 0.51 0.005 V-2 NT

Peaches 518 83 16 0.003 - 18 0.003 X-2 10

Peaches, Frozen 154 1 0.6 0.39 0.003 10

Pears 707 450 63.6 0.003 - 17.9 0.002 X-1 15

Plums 277 0 0.050 10

Summer Squash 698 0 0.005 NT

Sweet Bell Peppers 319 1 0.3 0.003 0.003 V-1 NT

Tangerines 531 102 19.2 0.005 - 0.52 0.005 10

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 9,523 685

Pyriofenone (fungicide) 

Grape Juice 700 0 0.005 1.5

Green Beans 700 0 0.001 NT

Summer Squash 698 1 0.1 0.001 0.001 - 0.005 0.30

Watermelon 175 0 0.005 0.30

Winter Squash 706 1 0.1 0.006 0.001 0.30

TOTAL 2,979 2

Pyriproxyfen (insecticide, growth regulator)

Blueberries, Cultivated, Fresh 663 0 0.001 1.0

Blueberries, Frozen 13 0 0.001 1.0

Appendix B. Page 97 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.001 0.70

Cantaloupe 328 0 0.001 0.10

Carrots 708 0 0.005 0.15

Cauliflower 531 0 0.001 0.70

Celery 354 0 0.005 3.0

Eggplant 703 5 0.7 0.002 - 0.009 0.001 - 0.005 0.80

Grape Juice 700 0 0.006 2.5

Green Beans 700 11 1.6 0.001 - 0.031 0.001 0.20

Peaches 518 12 2.3 0.005 - 0.046 0.005 1.0

Peaches, Frozen 154 0 0.005 1.0

Pears 707 10 1.4 0.010 0.006 0.20

Plums 277 0 0.001 1.0

Summer Squash 698 2 0.3 0.002 0.001 0.10

Sweet Bell Peppers 328 27 8.2 0.005 - 0.051 0.005 0.80

Tangerines 531 2 0.4 0.001 0.001 0.50

Watermelon 175 0 0.001 0.10

Winter Squash 706 1 0.1 0.004 0.001 0.10

TOTAL 9,502 70

Pyroxasulfone (herbicide) 

Carrots 708 0 0.005 - 0.050 NT

Eggplant 346 0 0.005 - 0.050 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,825 0

Pyroxsulam (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Quinalphos (insecticide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Quinoxyfen (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.020 1.0

Blueberries, Frozen 14 0 0.020 1.0

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.020 0.08

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 1 0.1 0.010 0.001 - 0.005 1.7

Grape Juice 700 0 0.001 2.0

Green Beans 700 0 0.001 NT

Peaches 518 1 0.2 0.035 0.010 0.70

Appendix B. Page 98 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.010 0.70

Plums 277 0 0.020 0.70

Summer Squash 698 7 1 0.002 - 0.005 0.001 V-7 NT

Sweet Bell Peppers 319 1 0.3 0.018 0.010 1.7

Tangerines 531 0 0.001 NT

Watermelon 175 1 0.6 0.001 0.001 0.08

Winter Squash 706 21 3 0.001 - 0.012 0.001 0.20

TOTAL 8,816 32

Quintozene - PCNB (fungicide) (parent of HCB, PCA, PCB and PCPMS)

Broccoli 708 2 0.3 0.004 0.001 0.1

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 0.1

Celery 354 0 0.005 NT

Eggplant 703 0 0.003 - 0.010 0.1

Green Beans 700 1 0.1 0.003 0.001 0.1

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 2 0.3 0.005 - 0.009 0.001 - 0.005 V-2 NT

Sweet Bell Peppers 328 1 0.3 0.008 0.005 0.1

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 6,814 6

Quizalofop ethyl (herbicide) 

Green Beans 700 0 0.001 0.25

Summer Squash 698 0 0.001 - 0.025 NT

Tangerines 531 0 0.025 NT

Watermelon 175 0 0.025 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,810 0

Resmethrin (insecticide) 

Carrots 708 0 0.030 3.0 FF

Celery 354 0 0.020 3.0 FF

Eggplant 346 0 0.030 3.0 FF

Grape Juice 700 0 0.012 3.0 FF

Green Beans 700 0 0.003 3.0 FF

Peaches 518 0 0.020 3.0 FF

Peaches, Frozen 154 0 0.020 3.0 FF

Pears 707 0 0.012 3.0 FF

Summer Squash 365 0 0.003 3.0 FF

Sweet Bell Peppers 328 0 0.020 3.0 FF

Tangerines 531 0 0.050 3.0 FF

Winter Squash 706 0 0.003 3.0 FF

TOTAL 6,117 0

Resmethrin trans (isomer of Resmethrin)

Blueberries, Cultivated, Fresh 692 0 0.050 3.0 FF

Blueberries, Frozen 14 0 0.050 3.0 FF

Broccoli 685 0 0.002 - 0.008 3.0 FF

Cantaloupe 328 0 0.050 3.0 FF

Eggplant 357 0 0.002 3.0 FF

Plums 277 0 0.10 3.0 FF

TOTAL 2,353 0

Appendix B. Page 99 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Rimsulfuron (herbicide) 

Celery 354 0 0.010 NT

Grape Juice 700 0 0.005 0.01

Peaches 518 0 0.010 0.01

Peaches, Frozen 154 0 0.010 0.01

Pears 707 0 0.005 0.01

Summer Squash 333 0 0.005 NT

Sweet Bell Peppers 299 0 0.010 NT

Tangerines 531 0 0.010 0.01

Watermelon 175 0 0.005 NT

TOTAL 3,771 0

Rotenone (insecticide) 

Green Beans 700 0 0.003 EX4

Summer Squash 365 0 0.003 EX4

Winter Squash 706 0 0.003 EX4

TOTAL 1,771 0

Saflufenacil (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Celery 354 0 0.005 NT

Grape Juice 700 0 0.003 0.03

Green Beans 700 0 0.003 0.03

Peaches 518 0 0.005 0.03

Peaches, Frozen 154 0 0.005 0.03

Pears 707 0 0.003 0.03

Plums 277 0 0.010 0.03

Summer Squash 698 0 0.003 - 0.020 NT

Sweet Bell Peppers 299 0 0.005 NT

Tangerines 531 0 0.020 0.03

Watermelon 175 0 0.020 NT

Winter Squash 706 0 0.003 NT

TOTAL 6,853 0

S-Bioallethrin (insecticide) 

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 1,771 0

Sedaxane (fungicide) 

Carrots 708 0 0.050 NT

Eggplant 346 0 0.050 NT

Green Beans 700 0 0.005 0.01

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 2,825 0

Sethoxydim (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.003 4.0

Blueberries, Frozen 14 0 0.003 4.0

Cantaloupe 328 0 0.003 4.0

Carrots 708 0 0.010 4.0

Eggplant 346 0 0.010 4.0

Grape Juice 700 0 0.002 1.0

Appendix B. Page 100 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 700 0 0.003 15

Pears 707 0 0.002 0.2

Plums 277 0 0.003 NT

Summer Squash 698 0 0.003 - 0.005 4.0

Tangerines 531 0 0.005 0.5

Watermelon 175 0 0.005 4.0

Winter Squash 706 0 0.003 4.0

TOTAL 6,582 0

Siduron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Simazine (herbicide) 

Blueberries, Cultivated, Fresh 692 3 0.4 0.006 - 0.013 0.005 0.20

Blueberries, Frozen 14 0 0.005 0.20

Broccoli 708 0 0.001 - 0.003 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 - 0.003 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.002 0.20

Green Beans 700 0 0.001 NT

Pears 707 0 0.002 0.25

Plums 277 0 0.005 0.20

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,178 3

Simeconazole (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Simetryn (herbicide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,125 0

Spinetoram (insecticide) 

Blueberries, Cultivated, Fresh 692 37 5.3 0.003 - 0.036 0.003 0.90

Blueberries, Frozen 14 1 7.1 0.004 0.003 0.90

Broccoli 688 16 2.3 0.003 - 0.20 0.003 2

Cantaloupe 328 0 0.003 0.30

Carrots 708 0 0.010 0.10

Cauliflower 531 2 0.4 0.005 - 0.020 0.001 - 0.003 2

Celery 354 0 0.010 8

Appendix B. Page 101 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 703 4 0.6 0.002 - 0.003 0.001 - 0.010 0.40

Grape Juice 700 0 0.003 0.50

Green Beans 700 0 0.010 0.30

Peaches 518 43 8.3 0.010 - 0.037 0.010 0.30

Peaches, Frozen 154 0 0.010 0.30

Pears 707 186 26.3 0.005 - 0.059 0.003 0.20

Plums 277 0 0.003 0.30

Summer Squash 365 0 0.010 0.30

Sweet Bell Peppers 319 0 0.010 0.40

Tangerines 531 0 0.005 0.30

Winter Squash 706 0 0.010 0.30

TOTAL 8,995 289

Spinetoram J (metabolite of Spinetoram) 

Summer Squash 333 0 0.005 0.30

Watermelon 175 0 0.005 0.30

TOTAL 508 0

Spinetoram L (metabolite of Spinetoram) 

Summer Squash 333 0 0.005 0.30

Watermelon 175 0 0.005 0.30

TOTAL 508 0

Spinosad (insecticide) (total of spinosyns A and D)

Broccoli 708 6 0.8 0.004 - 0.022 0.003 2

Carrots 708 0 0.010 0.10

Cauliflower 531 1 0.2 0.012 0.003 2

Celery 354 0 0.004 8

Eggplant 703 1 0.1 0.006 0.003 - 0.010 0.40

Grape Juice 700 0 0.003 0.50

Green Beans 700 5 0.7 0.003 - 0.045 0.003 0.30

Peaches 508 83 16.3 0.004 - 0.21 0.004 X-1 0.20

Peaches, Frozen 127 0 0.004 0.20

Pears 707 14 2 0.005 - 0.038 0.003 0.20

Summer Squash 365 0 0.003 0.3

Sweet Bell Peppers 319 2 0.6 0.004 - 0.013 0.004 0.40

Winter Squash 706 0 0.003 0.3

TOTAL 7,136 112

Spinosad A (isomer of Spinosad) 

Blueberries, Cultivated, Fresh 692 42 6.1 0.003 - 0.17 0.003 0.90

Blueberries, Frozen 14 1 7.1 0.007 0.003 0.90

Cantaloupe 328 0 0.003 0.3

Plums 277 0 0.003 0.20

Summer Squash 333 0 0.002 0.3

Tangerines 531 0 0.002 0.30

Watermelon 175 0 0.002 0.3

TOTAL 2,350 43

Spinosad D (isomer of Spinosad) 

Summer Squash 333 0 0.002 0.3

Tangerines 531 0 0.002 0.30

Watermelon 175 0 0.002 0.3

TOTAL 1,039 0

Spirodiclofen (acaricide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Appendix B. Page 102 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 3 0.4 0.010 - 0.020 0.006 V-3 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Cauliflower 531 2 0.4 0.010 0.006 V-2 NT

Celery 354 0 0.010 NT

Eggplant 703 0 0.006 - 0.010 NT

Grape Juice 700 0 0.004 2.0

Green Beans 700 0 0.003 NT

Peaches 518 125 24.1 0.010 - 0.18 0.010 1.0

Peaches, Frozen 154 0 0.010 1.0

Pears 707 149 21.1 0.007 - 0.16 0.004 0.80

Plums 277 7 2.5 0.010 - 0.053 0.010 1.0

Summer Squash 698 0 0.003 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.005 0.50

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 9,523 286

Spiromesifen Total (parent + enol metabolite) (insecticide) 

Broccoli 708 0 0.002 2.0

Cauliflower 531 0 0.002 2.0

Eggplant 357 3 0.8 0.004 - 0.019 0.002 - 0.008 0.45

TOTAL 1,596 3

Spiromesifen (insecticide) 

Blueberries, Cultivated, Fresh 662 0 0.010 2.0

Blueberries, Frozen 13 0 0.010 2.0

Cantaloupe 328 0 0.010 0.10

Carrots 708 0 0.020 NT

Celery 354 0 0.002 6.0

Eggplant 346 3 0.9 0.022 - 0.035 0.020 0.45

Green Beans 700 0 0.003 0.80

Peaches 518 0 0.002 NT

Peaches, Frozen 154 0 0.002 NT

Plums 250 0 0.010 NT

Summer Squash 698 0 0.003 - 0.010 0.10

Sweet Bell Peppers 319 46 14.4 0.002 - 0.12 0.002 0.45

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 0.10

Winter Squash 706 4 0.6 0.003 - 0.010 0.003 0.10

TOTAL 6,462 53

Spiromesifen alcohol (metabolite of Spiromesifen)

Green Beans 700 0 0.001 0.80

Summer Squash 365 0 0.001 0.10

Winter Squash 706 1 0.1 0.001 0.001 0.10

TOTAL 1,771 1

Spiromesifen enol 5 (metabolite of Spiromesifen)

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 0.45

TOTAL 1,054 0

Spirotetramat (insecticide) 

Blueberries, Cultivated, Fresh 692 18 2.6 0.003 - 0.37 0.002 3.0

Blueberries, Frozen 14 0 0.002 3.0

Broccoli 708 7 1 0.003 - 0.010 0.002 2.5

Appendix B. Page 103 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.002 0.30

Carrots 708 0 0.005 0.15

Cauliflower 531 0 0.002 2.5

Celery 354 0 0.010 9.0

Eggplant 703 0 0.002 - 0.005 2.5

Grape Juice 700 0 0.002 1.3

Green Beans 700 0 0.001 2.5

Peaches 518 0 0.010 4.5

Peaches, Frozen 154 0 0.010 4.5

Pears 707 75 10.6 0.003 - 0.034 0.002 0.70

Plums 277 63 22.7 0.002 - 0.025 0.002 4.5

Summer Squash 698 0 0.001 - 0.002 0.30

Sweet Bell Peppers 319 2 0.6 0.012 - 0.023 0.010 2.5

Tangerines 531 0 0.002 0.60

Watermelon 175 0 0.002 0.30

Winter Squash 706 0 0.001 0.30

TOTAL 9,523 165

Spiroxamine (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 1.2 FU

Grape Juice 700 0 0.001 1.0 IM

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.001 - 0.002 NT

Sweet Bell Peppers 319 0 0.010 1.2 FU

Tangerines 499 0 0.002 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.001 NT

TOTAL 7,188 0

Sulfallate (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Sulfentrazone (herbicide) 

Carrots 708 0 0.035 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.035 0.15

Grape Juice 700 0 0.060 0.15

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.003 - 0.025 NT

Sweet Bell Peppers 328 0 0.005 0.15

Tangerines 531 0 0.050 0.15

Watermelon 175 0 0.025 0.15

Winter Squash 706 0 0.003 NT

TOTAL 5,918 0

Appendix B. Page 104 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sulfometuron methyl (herbicide) 

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 1,771 0

Sulfosulfuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Sulfoxaflor (insecticide) 

Carrots 708 0 0.10 0.05

Cauliflower 531 4 0.8 0.005 - 0.050 0.004 0.08

Eggplant 703 25 3.6 0.002 - 0.071 0.001 - 0.10 0.70

Grape Juice 700 0 0.010 2.0

Green Beans 700 11 1.6 0.003 - 0.079 0.003 4.0

Pears 707 8 1.1 0.017 0.010 0.50

Summer Squash 698 3 0.4 0.003 - 0.004 0.003 - 0.050 0.40

Tangerines 531 0 0.15 0.70

Watermelon 175 0 0.050 0.40

Winter Squash 706 0 0.003 0.40

TOTAL 6,159 51

Sulprofos (insecticide) 

Broccoli 708 0 0.002 NT

Cauliflower 531 0 0.002 NT

Eggplant 357 0 0.002 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,367 0

TCMTB (fungicide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.005 NT

Summer Squash 698 0 0.005 - 0.10 NT

Tangerines 531 0 0.10 NT

Watermelon 175 0 0.10 NT

Winter Squash 706 0 0.005 NT

TOTAL 3,864 0

Tebuconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.098 0.010 V-1 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 1 0.1 0.002 0.001 V-1 NT

Cantaloupe 328 0 0.010 0.4

Carrots 708 2 0.3 0.020 - 0.026 0.015 V-2 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 3 0.4 0.002 - 0.006 0.001 - 0.015 1.3

Grape Juice 700 155 22.1 0.003 0.002 6

Green Beans 700 35 5 0.001 - 0.092 0.001 0.1

Peaches 518 98 18.9 0.006 - 0.61 0.005 2

Appendix B. Page 105 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 11 7.1 0.005 - 0.043 0.005 2

Pears 707 4 0.6 0.003 - 0.016 0.002 1

Plums 277 1 0.4 0.012 0.010 1

Summer Squash 698 8 1.1 0.002 - 0.009 0.001 - 0.005 0.4

Sweet Bell Peppers 328 13 4 0.009 - 0.14 0.005 1.3

Tangerines 531 0 0.005 NT

Watermelon 175 1 0.6 0.014 0.005 0.4

Winter Squash 706 41 5.8 0.001 - 0.023 0.001 0.4

TOTAL 9,532 374

Tebufenozide (insecticide) 

Blueberries, Cultivated, Fresh 692 3 0.4 0.025 - 0.040 0.002 3.0

Blueberries, Frozen 14 1 7.1 0.014 0.002 3.0

Broccoli 667 0 0.002 - 0.005 5.0

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.005 NT

Cauliflower 384 0 0.002 5.0

Celery 354 0 0.005 2.0

Eggplant 703 0 0.002 - 0.005 1.0

Grape Juice 700 0 0.001 3.0

Green Beans 700 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 707 0 0.001 1.5 IT

Plums 277 0 0.002 NT

Summer Squash 698 0 0.005 NT

Sweet Bell Peppers 319 0 0.005 1.0

Tangerines 531 0 0.010 2.0

Winter Squash 706 0 0.005 NT

TOTAL 9,160 4

Tebufenpyrad (insecticide, acaricide)

Carrots 708 0 0.005 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Tebupirimfos (insecticide) 

Broccoli 685 0 0.001 NT

Cauliflower 531 0 0.001 NT

Eggplant 357 0 0.001 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,344 0

Tebutam (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Appendix B. Page 106 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tebuthiuron (herbicide) 

Broccoli 668 0 0.001 - 0.003 NT

Carrots 708 0 0.010 NT

Cauliflower 508 0 0.001 - 0.003 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,358 0

Tecnazene (plant growth regulator) 

Broccoli 708 0 0.001 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 357 0 0.001 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,721 0

Teflubenzuron (insecticide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.005 NT

Pears 707 0 0.025 NT

Summer Squash 365 0 0.005 NT

Tangerines 531 0 0.050 NT

Watermelon 175 0 0.050 0.30 FU

Winter Squash 706 0 0.005 NT

TOTAL 4,238 0

Tefluthrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.002 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Grape Juice 700 0 0.002 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 707 0 0.002 NT

Plums 277 0 0.002 NT

Summer Squash 698 0 0.003 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 9,532 0

Appendix B. Page 107 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Temephos (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Tepraloxydim (herbicide) 

Green Beans 700 0 0.010 NT

Summer Squash 365 0 0.010 NT

Tangerines 531 0 0.010 NT

Winter Squash 706 0 0.010 NT

TOTAL 2,302 0

Terbacil (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 0.2

Blueberries, Frozen 14 0 0.010 0.2

Broccoli 708 0 0.003 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.003 NT

Celery 354 0 0.008 NT

Eggplant 703 0 0.003 - 0.020 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.008 0.2

Peaches, Frozen 154 0 0.008 0.2

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.008 NT

Watermelon 175 0 0.005 1.0

Winter Squash 706 0 0.001 NT

TOTAL 7,261 0

Terbufos (insecticide) 

Carrots 708 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,864 0

Terbufos oxygen analog (metabolite of Terbufos)

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Summer Squash 333 0 0.001 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.001 NT

TOTAL 2,093 0

Terbufos oxygen analog sulfone (metabolite of Terbufos)

Carrots 708 0 0.005 NT

Eggplant 346 0 0.005 NT

Summer Squash 333 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

TOTAL 2,093 0

Appendix B. Page 108 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Terbufos oxygen analog sulfoxide (metabolite of Terbufos)

Summer Squash 333 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

TOTAL 1,039 0

Terbufos sulfone (metabolite of Terbufos)

Broccoli 708 0 0.001 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Tangerines 531 0 0.025 NT

Winter Squash 706 0 0.005 NT

TOTAL 4,952 0

Terbufos sulfoxide (metabolite of Terbufos)

Carrots 708 1 0.1 0.027 0.005 V-1 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.003 NT

Summer Squash 698 0 0.002 - 0.003 NT

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.002 NT

Winter Squash 706 0 0.003 NT

TOTAL 3,864 1

Terbuthylazine (herbicide) 

Carrots 708 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Terbutryn (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Tetrachlorvinphos (insecticide) 

Broccoli 708 0 0.005 NT

Cauliflower 531 0 0.002 - 0.005 NT

Eggplant 357 0 0.002 NT

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Tangerines 531 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,898 0

Appendix B. Page 109 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tetraconazole (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 0.25

Blueberries, Frozen 14 0 0.010 0.25

Broccoli 601 0 0.001 NT

Cantaloupe 328 0 0.010 0.15

Carrots 708 0 0.010 NT

Cauliflower 474 0 0.001 - 0.003 NT

Eggplant 657 0 0.003 - 0.010 0.30

Grape Juice 700 0 0.002 0.20

Green Beans 700 0 0.001 NT

Plums 277 0 0.010 NT

Summer Squash 698 17 2.4 0.002 - 0.040 0.001 0.15

Tangerines 531 0 0.001 NT

Watermelon 175 2 1.1 0.001 0.001 0.15

Winter Squash 706 2 0.3 0.002 - 0.027 0.001 0.15

TOTAL 7,261 21

Tetradifon (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.002 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.002 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.002 - 0.020 NT

Green Beans 700 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 7,086 0

Tetrahydrophthalimide - THPI (metabolite of Captafol and Captan)

Blueberries, Cultivated, Fresh 692 165 23.8 0.010 - 4.0 0.010 20.0 TP

Blueberries, Frozen 14 8 57.1 0.012 - 0.81 0.010 20.0 TP

Broccoli 708 0 0.004 0.05 TP

Cantaloupe 328 0 0.010 0.05 TP

Cauliflower 531 0 0.004 0.05 TP

Eggplant 357 0 0.012 0.05 TP

Grape Juice 700 46 6.6 0.017 - 0.29 0.010 25.0 TP

Green Beans 700 12 1.7 0.007 - 0.084 0.005 X-1 0.05 TP

Pears 707 67 9.5 0.038 - 0.86 0.010 25.0 TP

Plums 277 1 0.4 0.012 0.010 10.0 TP

Summer Squash 365 0 0.005 0.05 TP

Winter Squash 706 3 0.4 0.006 - 0.010 0.005 0.05 TP

TOTAL 6,085 302

Tetramethrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.005 NT

Blueberries, Frozen 14 0 0.005 NT

Cantaloupe 328 0 0.005 NT

Carrots 708 0 0.025 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.025 NT

Appendix B. Page 110 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 700 0 0.005 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Pears 707 0 0.005 NT

Plums 277 0 0.005 NT

Summer Squash 698 0 0.005 - 0.010 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.005 NT

TOTAL 7,236 0

Thiabendazole (fungicide) (parent of 5-hydroxythiabendazole)

Blueberries, Cultivated, Fresh 692 0 0.002 NT

Blueberries, Frozen 14 0 0.002 NT

Broccoli 708 0 0.003 0.02

Cantaloupe 328 48 14.6 0.002 - 0.11 0.002 15.0 FU

Carrots 708 3 0.4 0.005 - 0.39 0.005 10

Cauliflower 531 11 2.1 0.002 - 0.006 0.001 0.02

Celery 354 0 0.010 NT

Eggplant 703 1 0.1 0.005 0.003 - 0.005 V-1 NT

Green Beans 700 1 0.1 0.002 0.001 0.02

Peaches 518 4 0.8 0.013 - 0.031 0.010 V-4 NT

Peaches, Frozen 154 0 0.010 NT

Pears 707 322 45.5 0.002 - 2.8 0.001 10

Plums 277 4 1.4 0.002 - 0.003 0.002 V-4 NT

Summer Squash 698 0 0.001 - 0.005 0.02

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 401 75.5 0.010 - 2.5 0.010 10

Watermelon 175 1 0.6 0.014 0.005 0.02

Winter Squash 706 1 0.1 0.005 0.001 0.02

TOTAL 8,823 797

Thiacloprid (insecticide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.061 0.001 V-1 NT

Blueberries, Frozen 14 0 0.001 NT

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.001 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.010 NT

Eggplant 703 4 0.6 0.004 - 0.008 0.001 - 0.005 V-4 NT

Green Beans 700 1 0.1 0.002 0.001 V-1 NT

Peaches 518 19 3.7 0.010 - 0.042 0.010 0.5 FU

Peaches, Frozen 154 0 0.010 0.5 FU

Pears 707 9 1.3 0.042 - 0.14 0.025 0.30 FU

Plums 277 0 0.001 0.05 FU

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 319 20 6.3 0.010 - 0.080 0.010 1.0 FU

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,823 54

Thiamethoxam (insecticide) (also a parent of Clothianidin)

Blueberries, Cultivated, Fresh 692 8 1.2 0.003 - 0.022 0.003 0.30

Blueberries, Frozen 14 0 0.003 0.30

Appendix B. Page 111 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 165 23.3 0.003 - 0.045 0.002 - 0.005 4.5

Cantaloupe 328 10 3 0.003 - 0.008 0.003 0.2

Carrots 708 0 0.005 0.05

Cauliflower 531 125 23.5 0.003 - 0.080 0.002 - 0.005 4.5

Celery 354 9 2.5 0.010 - 0.031 0.010 4.0

Eggplant 703 168 23.9 0.003 - 0.19 0.002 - 0.005 0.25

Grape Juice 700 0 0.075 0.20

Green Beans 700 1 0.1 0.071 0.001 X-1 0.02

Peaches 518 0 0.010 0.5

Peaches, Frozen 154 0 0.010 0.5

Pears 707 0 0.075 0.2

Plums 277 0 0.003 0.5

Summer Squash 698 154 22.1 0.001 - 0.15 0.001 - 0.010 0.2

Sweet Bell Peppers 319 71 22.3 0.010 - 0.095 0.010 0.25

Tangerines 531 0 0.020 0.40

Watermelon 175 6 3.4 0.013 - 0.052 0.010 0.2

Winter Squash 706 103 14.6 0.001 - 0.030 0.001 0.2

TOTAL 9,523 820

Thiazopyr (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.008 NT

Blueberries, Frozen 14 0 0.008 NT

Cantaloupe 328 0 0.008 NT

Green Beans 700 0 0.003 NT

Plums 277 0 0.008 NT

Summer Squash 698 0 0.001 - 0.003 NT

Tangerines 531 0 0.001 NT

Watermelon 175 0 0.001 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,121 0

Thidiazuron (plant growth regulator) 

Green Beans 700 0 0.005 NT

Summer Squash 365 0 0.005 NT

Winter Squash 706 0 0.005 NT

TOTAL 1,771 0

Thiencarbazone methyl (herbicide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 2,825 0

Thifensulfuron methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Thiobencarb (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 1 0.1 0.007 0.003 V-1 NT

Cantaloupe 328 0 0.010 NT

Cauliflower 531 3 0.6 0.002 - 0.025 0.001 V-3 NT

Appendix B. Page 112 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 357 0 0.001 NT

Green Beans 700 0 0.003 NT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 4,678 4

Thiodicarb (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.003 NT

Blueberries, Frozen 14 0 0.003 NT

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 NT

Green Beans 677 0 0.010 NT

Plums 277 0 0.003 NT

Summer Squash 305 0 0.010 NT

Winter Squash 480 0 0.010 NT

TOTAL 3,499 0

Thionazin (insecticide, fumigant)

Green Beans 700 0 0.003 NT

Summer Squash 365 0 0.003 NT

Winter Squash 706 0 0.003 NT

TOTAL 1,771 0

Thiophanate methyl (fungicide) 

Carrots 552 0 0.10 NT

Eggplant 230 0 0.10 NT

Grape Juice 700 0 0.010 5.0

Pears 707 107 15.1 0.017 - 0.22 0.010 3.0

Summer Squash 333 1 0.3 0.25 0.020 1.0

Tangerines 531 0 0.020 NT

Watermelon 175 0 0.020 1.0

TOTAL 3,228 108

Tolclofos methyl (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Tolfenpyrad (insecticide) 

Carrots 708 0 0.025 NT

Eggplant 346 2 0.6 0.029 - 0.045 0.025 1.5

Grape Juice 700 0 0.003 2.0

Green Beans 700 6 0.9 0.011 - 0.044 0.003 V-6 NT

Pears 707 179 25.3 0.005 - 0.29 0.003 1.0

Summer Squash 698 0 0.003 - 0.005 0.70

Tangerines 531 0 0.005 1.5 IT

Watermelon 175 0 0.005 0.70

Winter Squash 706 0 0.003 0.70

TOTAL 5,271 187

Tolylfluanid (fungicide) 

Carrots 708 0 0.050 - 0.10 NT

Eggplant 346 0 0.050 - 0.10 NT

Grape Juice 700 0 0.006 11 FU

TOTAL 1,754 0

Appendix B. Page 113 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tri-Allate (herbicide) 

Celery 354 0 0.005 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,164 0

Triadimefon (fungicide) (also a parent of Triadimenol)

Broccoli 708 0 0.001 NT

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.003 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 5,775 0

Triadimenol (fungicide) (also a metabolite of Triadimefon)

Carrots 708 0 0.040 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.040 NT

Green Beans 700 0 0.040 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 365 0 0.040 NT

Sweet Bell Peppers 328 0 0.005 NT

Winter Squash 706 0 0.040 NT

TOTAL 4,179 0

Triasulfuron (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Triazophos (insecticide) 

Carrots 708 0 0.010 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,179 0

Appendix B. Page 114 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tribenuron methyl (herbicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Trichlorfon (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.050 - 0.10 NT

Eggplant 346 0 0.050 - 0.10 NT

Green Beans 700 0 0.003 NT

Plums 277 0 0.010 NT

Summer Squash 698 0 0.003 - 0.040 NT

Tangerines 531 0 0.040 NT

Watermelon 175 0 0.040 NT

Winter Squash 706 0 0.003 NT

TOTAL 5,175 0

Trichloronate (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Tricyclazole (fungicide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Trifloxystrobin (fungicide) 

Blueberries, Cultivated, Fresh 692 1 0.1 0.002 0.002 1.5

Blueberries, Frozen 14 0 0.002 1.5

Broccoli 708 4 0.6 0.010 - 0.016 0.003 2.0

Cantaloupe 328 0 0.002 0.50

Carrots 708 0 0.005 0.1

Cauliflower 531 0 0.001 2.0

Celery 354 8 2.3 0.006 - 0.033 0.005 9.0

Eggplant 703 2 0.3 0.002 - 0.011 0.001 - 0.005 0.5

Grape Juice 700 0 0.001 2.0

Green Beans 700 0 0.001 NT

Peaches 518 82 15.8 0.005 - 0.16 0.005 2

Peaches, Frozen 154 0 0.005 2

Pears 707 5 0.7 0.002 - 0.036 0.001 0.5

Plums 277 43 15.5 0.002 - 0.032 0.002 2

Summer Squash 698 4 0.6 0.001 - 0.017 0.001 0.50

Sweet Bell Peppers 319 7 2.2 0.005 - 0.061 0.005 0.5

Tangerines 531 0 0.001 0.6

Watermelon 175 0 0.001 0.50

Winter Squash 706 5 0.7 0.002 - 0.004 0.001 0.50

TOTAL 9,523 161

Trifloxysulfuron (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.020 NT

Blueberries, Frozen 14 0 0.020 NT

Appendix B. Page 115 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 328 0 0.020 NT

Green Beans 700 0 0.001 NT

Plums 277 0 0.020 NT

Summer Squash 698 0 0.001 - 0.010 NT

Tangerines 531 0 0.010 0.03

Watermelon 175 0 0.010 NT

Winter Squash 706 0 0.001 NT

TOTAL 4,121 0

Triflumezopyrim (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Triflumizole (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 2.0

Blueberries, Frozen 14 0 0.010 2.0

Broccoli 708 0 0.002 8.0

Cantaloupe 328 0 0.010 0.5

Carrots 708 0 0.005 NT

Cauliflower 531 0 0.002 - 0.005 8.0

Celery 354 0 0.003 NT

Eggplant 703 0 0.002 - 0.005 NT

Grape Juice 700 0 0.001 2.5

Green Beans 700 0 0.003 NT

Peaches 518 0 0.003 NT

Peaches, Frozen 154 0 0.003 NT

Pears 707 0 0.001 0.50

Plums 277 0 0.010 NT

Summer Squash 698 3 0.4 0.003 - 0.019 0.003 - 0.010 0.5

Sweet Bell Peppers 319 2 0.6 0.006 - 0.008 0.003 V-2 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.010 0.5

Winter Squash 706 1 0.1 0.004 0.003 0.5

TOTAL 9,523 6

Trifluralin (herbicide) 

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Broccoli 708 3 0.4 0.002 0.001 0.05

Cantaloupe 328 0 0.001 0.05

Carrots 708 6 0.8 0.012 - 0.049 0.010 1.0

Cauliflower 531 0 0.001 0.05

Celery 354 1 0.3 0.009 0.005 0.05

Eggplant 703 0 0.001 - 0.010 0.05

Grape Juice 700 0 0.003 0.05

Green Beans 700 0 0.001 0.05

Peaches 518 0 0.005 0.05

Peaches, Frozen 154 0 0.005 0.05

Plums 277 0 0.001 0.05

Summer Squash 698 4 0.6 0.001 - 0.004 0.001 - 0.005 0.05

Sweet Bell Peppers 328 0 0.005 0.05

Tangerines 531 0 0.005 0.05

Watermelon 175 0 0.005 0.05

Winter Squash 706 5 0.7 0.001 - 0.003 0.001 0.05

TOTAL 8,825 19

Appendix B. Page 116 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Triforine (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 1.0 FU

Blueberries, Frozen 14 0 0.010 1.0 FU

Cantaloupe 328 0 0.010 NT

Plums 277 0 0.010 NT

TOTAL 1,311 0

Triticonazole (fungicide) 

Carrots 708 0 0.010 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.010 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 698 0 0.003 - 0.005 NT

Sweet Bell Peppers 319 0 0.010 NT

Tangerines 531 0 0.010 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.003 NT

TOTAL 5,209 0

Uniconazole (fungicide) 

Carrots 708 0 0.020 NT

Eggplant 346 0 0.020 0.01

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 2,825 0

Valifenalate (fungicide) 

Grape Juice 700 0 0.003 5 FU

Green Beans 700 0 0.001 NT

Summer Squash 698 0 0.001 - 0.010 0.3

Watermelon 175 0 0.010 0.3

Winter Squash 706 0 0.001 0.3

TOTAL 2,979 0

Vamidothion (insecticide) 

Green Beans 700 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 1,771 0

Vernolate (herbicide) 

Celery 354 0 0.010 NT

Green Beans 700 0 0.040 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 365 0 0.040 NT

Sweet Bell Peppers 319 0 0.010 NT

Winter Squash 706 0 0.040 NT

TOTAL 3,116 0

Vinclozolin (fungicide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Appendix B. Page 117 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.001 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.010 NT

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.001 - 0.010 NT

Green Beans 700 0 0.001 2.0 IT

Peaches 518 0 0.005 25.0 IT

Peaches, Frozen 154 0 0.005 25.0 IT

Plums 277 0 0.010 NT

Summer Squash 365 0 0.001 NT

Sweet Bell Peppers 328 0 0.005 3.0 IT

Winter Squash 706 0 0.001 NT

TOTAL 7,086 0

Zoxamide (fungicide) 

Carrots 708 0 0.020 NT

Celery 354 0 0.010 NT

Eggplant 346 0 0.020 1.0

Grape Juice 700 0 0.004 5.0

Green Beans 700 0 0.001 NT

Peaches 518 0 0.010 NT

Peaches, Frozen 154 0 0.010 NT

Summer Squash 698 4 0.6 0.004 - 0.011 0.001 - 0.002 1.0

Sweet Bell Peppers 319 0 0.010 1.0

Tangerines 531 0 0.002 NT

Watermelon 175 0 0.002 1.0

Winter Squash 706 5 0.7 0.001 - 0.011 0.001 1.0

TOTAL 5,909 9

NOTES

^ = When a range is not listed, only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

1 Emamectin benzoate is the salt form of the active, Emamectin.

2 Halosulfuron methyl is the salt form of the active, Halosulfuron.

3 Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

4 Propamocarb analytically determined as the salt (hydrochloride).

5 Enol metabolite calculated as the parent, Spiromesifen.

Tolerance Violation Codes:

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

pages 1 through 3 in Appendix J to see the sample origin (domestic, imported, or unknown) for each occurrence.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 4 through 7 in Appendix J to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.

EPA Tolerance Codes:

EX1 = Exempt from the requirement of a tolerance in or on raw agricultural commodities that have no established tolerance when residues

are present as a result of subsequent uptake by crops rotated into fields where crops with tolerances were treated with cyclaniliprole.

EX2 = Exempt from the requirement of a tolerance in or on all food and feed commodities when applied as an herbicide in accordance

with good agricultural practices.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2021 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix B. Page 118 of 119
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

EX3 = Exempt from the requirement of a tolerance in or on all food commodities when used to control insect larvae.

EX4 = Exempt from the requirement of a tolerance when applied to growing crops in accordance with good agricultural practices.

FF = All food/feed commodities tolerance except those covered by a higher tolerance.

FU = Foreign use compound; There are no U.S. registrations.

IM = Import Tolerance.

IN = Inadvertent/negligible residue tolerance.

IT = Interim Tolerance/Temporary or time limited tolerance/Section 18.

NT = No tolerance level was set for that pesticide/commodity pair.

PH = Post-harvest application.

R = Regional tolerance.

TP = Tolerance is from parent compound.

Appendix B. Page 119 of 119
Appendix C

Distribution of Residues by Pesticide

in Corn Grain 

Appendix C shows residue detections for all compounds tested in corn grain, including range of 

values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this summary 

and appendixes apply to 2021 and not to the current year. There may be instances where 

tolerances have been recently set, modified, or revoked that would have an effect on whether a 

residue is violative or not. 

In 2021, the Pesticide Data Program (PDP) analyzed 418 corn grain samples. PDP detected 6 

different residues for 5 distinct pesticides in the corn grain samples. All residue detections were 

lower than the established tolerances for those compounds with established tolerances. 

Results for environmental contaminants across all commodities, including corn grain, have been 

consolidated in a separate appendix because they have no registered uses and are not applied 

to crops (see Appendix E). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

1-Naphthol IM 418 0.050 0.02 TP

3-Hydroxycarbofuran IM 418 0.025 NT

Acephate I 418 0.12 NT

Acetamiprid I 418 0.020 NT

Acetochlor H 418 0.10 0.05

Alachlor H 418 0.050 0.2

Ametryn H 418 0.50 0.05

Amicarbazone H 418 0.10 0.05

Aminomethylphosphonic acid (AMPA) HM 418 0.10 5.0

Atrazine H 418 0.050 0.20

Azinphos methyl I 418 0.020 NT

Azoxystrobin F 418 0.010 0.05

Bendiocarb I 418 0.025 NT

Benoxacor S 418 0.25 0.01

Bifenthrin I 418 0.010 0.05

Boscalid F 418 0.005 0.20 IN

Carbaryl I 418 0.025 0.02

Carbendazim (MBC) F 418 0.15 NT

Carbofuran I 418 0.010 NT

Carboxin F 418 0.050 0.2

Carfentrazone ethyl H 418 0.001 0.10

Chlorantraniliprole I 418 0.10 0.04

Chlorethoxyfos I 418 0.001 0.01

Chlorfenapyr I 418 0.001 NT

Chlorpyrifos I 418 3 0.7 0.001 - 0.003 0.001 0.05

Clothianidin I 418 0.010 0.02 TP

Cyantraniliprole I 418 0.25 0.01

Cyfluthrin I 418 0.005 0.05

Cyhalothrin, Lambda I 418 0.005 0.05

Cypermethrin I 418 1 0.2 0.016 0.005 0.05

DCPA H 418 0.001 0.05 IN

Deltamethrin 1 I 418 5 1.2 0.016 - 0.083 0.005 1.0

Dichlorvos (DDVP) I 418 0.050 0.5 TP

Dimethenamid H 418 0.005 0.01

Dimethoate I 418 0.005 0.1

Dinotefuran I 418 0.12 0.01 FF

Diuron H 418 0.020 0.1

Esfenvalerate+Fenvalerate Total I 418 0.001 0.02

Ethoprop I 418 0.020 0.02

Etofenprox I 418 0.020 5.0 FF

Etoxazole A 389 0.002 0.01

Etridiazole F 418 0.10 NT

APPENDIX C. DISTRIBUTION OF RESIDUES BY PESTICIDE IN CORN GRAIN

Appendix C. Page 1 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Fenamidone F 418 0.40 0.1 IN

Fenpyroximate A 418 0.005 0.02

Fipronil I 418 0.020 0.02

Flubendiamide I 418 0.10 0.03

Fludioxonil F 418 0.050 0.02

Flufenacet H 418 0.005 0.05

Fluometuron H 418 0.010 0.5 IN

Fluopyram F 418 0.003 0.02

Flupyradifurone I 418 0.005 0.05

Fluridone H 418 0.040 0.1 IN

Fluroxypyr HM 418 0.50 0.02

Flutriafol F 418 0.020 0.01

Fluvalinate I 418 0.010 NT

Fluxapyroxad F 418 0.005 0.01

Glyphosate H 418 146 34.9 0.050 - 0.14 0.035 5.0

Hexythiazox I 418 0.020 0.02

Imidacloprid I 418 0.015 0.05

Imiprothrin I 418 0.15 NT

Isoxaflutole H 418 0.050 0.02

Linuron H 418 0.050 0.1

Malathion I 418 7 1.7 0.025 - 2.7 0.025 8 PH

Malathion oxygen analog IM 418 1 0.2 0.021 0.015 8 PH

Mesotrione H 418 0.10 0.01

Metalaxyl/Mefenoxam 2 F 418 0.004 0.1

Metconazole F 418 0.10 0.02

Methamidophos I 418 0.050 NT

Methomyl I 418 0.005 0.1

Methoxyfenozide I 418 0.005 0.05

Metolachlor H 418 0.001 0.10

Metribuzin H 418 0.001 0.05

MGK-264 I 418 0.050 NT

Myclobutanil F 418 0.020 0.03 IN

Nitrapyrin N 418 0.010 0.1

Novaluron I 418 0.015 0.01 FF

Omethoate IM 418 0.025 0.1 TP

Oxyfluorfen H 418 0.020 0.05

Parathion methyl I 418 0.002 NT

Pendimethalin H 418 0.002 0.1

Penthiopyrad F 418 0.004 0.01

Permethrin Total I 418 0.010 0.05

Phenothrin I 418 0.35 0.01 FF

Phorate I 418 0.050 0.05

Phorate sulfone IM 418 0.25 0.05

Phorate sulfoxide IM 418 0.050 0.05

Appendix C. Page 2 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Phosmet I 418 0.005 NT

Phosmet oxygen analog IM 418 0.005 NT

Picoxystrobin F 418 0.003 0.04

Prallethrin I 418 0.001 1.0 FF

Propachlor H 418 0.15 0.2

Propetamphos I 418 0.10 NT

Propiconazole F 418 0.025 0.2

Pyraclostrobin F 418 0.012 0.1

Pyrethrins I 418 0.020 3.0 PH

Pyriproxyfen I 418 0.030 1.1

Saflufenacil H 418 0.010 0.03

Sethoxydim H 418 0.020 0.5

Simazine H 418 0.050 0.20

Spinetoram J IM 418 0.010 0.04

Spinosad I 418 0.10 1.5

Spiromesifen I 418 0.030 0.02

Sulfoxaflor I 418 0.015 0.015

Tebuconazole F 418 0.050 0.05

Tefluthrin I 418 0.001 0.06

Tetraconazole F 418 0.010 0.01

Tetrahydrophthalimide (THPI) FM 418 0.050 0.05 TP

Tetramethrin I 418 0.005 NT

Thiabendazole F 418 0.005 0.01

Thiamethoxam I 418 0.010 0.02

Thiodicarb I 418 0.010 NT

Triadimenol F 418 0.10 0.05

Trifloxystrobin F 418 0.005 0.05

Trifluralin H 418 0.001 0.05

Triticonazole F 418 0.10 0.01

NOTES

^ = When a range is not listed, only one distinct detected concentration or LOD value was reported for the 

 pesticide/commodity pair.

1 = Deltamethrin includes parent Tralomethrin.

2 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is advised to refer 

to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply to 2021 and not to the 

current year. There may be instances where a tolerance was recently set or revoked that would have an effect on whether a 

residue is violative or not. 

Appendix C. Page 3 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

N = Nitrification Inhibitor

S = Herbicide Safener

EPA Tolerance Codes:

FF = All food/feed commodities tolerance except those covered by a higher tolerance.

IN = Inadvertent/negligible residue tolerance.

NT = No tolerance established.

PH = Post-harvest application.

TP = Tolerance is from parent compound.

Appendix C. Page 4 of 4
Appendix D

Distribution of Residues by Pesticide

in Butter 

Appendix D shows residue detections for all compounds tested in butter, including range of 

values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this summary 

and appendixes apply to 2021 and not to the current year. There may be instances where 

tolerances have been recently set, modified, or revoked that would have an effect on whether a 

residue is violative or not. 

In 2021, the Pesticide Data Program (PDP) analyzed 177 butter samples. PDP detected 15 

different residues for 14 distinct pesticides in the butter samples. All residue detections were 

lower than the established tolerances for those compounds with established tolerances. 

PDP reports tolerance violations to FDA as part of an interagency Memorandum of 

Understanding between the U.S. Department of Agriculture and FDA. Residues reported to 

FDA are shown in the “Pesticide” column to the right of the pesticide name and are annotated 

as “X” (if the residue exceeded the established tolerance) or “V” (if the residue did not have a 

tolerance listed in the Code of Federal Regulations, Title 40, Part 180). In both cases, these 

annotations are followed by a number indicating the number of samples reported to FDA.

Results for environmental contaminants across all commodities, including butter, have been 

consolidated in a separate appendix because they have no registered uses and are not applied 

to crops (see Appendix E). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

3-Hydroxycarbofuran IM 177 0.001 NT

Acephate I 177 0.002 0.1

Acetamiprid I 177 0.001 0.30

Acetochlor H 177 0.001 - 0.004 0.02

Acibenzolar S methyl F 177 0.015 NT

Afidopyropen I 177 0.001 0.04

Alachlor H 177 0.002 0.02

Aldicarb I 177 0.001 NT

Aldicarb sulfone IM 177 0.004 NT

Aldicarb sulfoxide IM 177 0.002 NT

Ametoctradin (V-1) F 177 1 0.6 0.002 0.001 NT

Atrazine H 177 0.001 0.02

Azinphos methyl I 177 0.007 NT

Azoxystrobin F 177 0.001 0.006

Bendiocarb I 177 0.001 NT

Benoxacor S 177 0.001 0.01

Benzovindiflupyr F 177 0.002 - 0.007 0.02

Bifenthrin I 177 65 36.7 0.002 0.001 1.0

Boscalid F 177 0.001 0.10

Buprofezin I 177 2 1.1 0.002 0.001 0.01

Carbaryl I 177 0.001 1.0

Carbendazim (MBC) F 177 0.001 NT

Carbofuran I 177 0.001 NT

Carfentrazone ethyl H 177 0.005 - 0.018 0.05

Chlorantraniliprole I 177 0.006 0.1

Chlorfenapyr I 177 0.003 0.01 FF

Chlorfenvinphos total I 177 0.002 - 0.006 NT

Chlorpropham H 177 0.001 0.30

Chlorpyrifos I 177 0.001 0.25

Chlorpyrifos oxygen analog IM 177 0.001 - 0.004 0.25

Clethodim H 177 0.009 0.05

Clomazone H 177 0.003 NT

Clothianidin I 177 0.002 0.02 TP

Coumaphos I 177 0.002 - 0.006 0.5

Coumaphos oxygen analog IM 177 0.004 0.5

Cyantraniliprole I 177 0.003 0.20

Cyazofamid F 177 0.007 NT

Cyfluthrin I 177 0.030 5.0

Cyhalothrin, Total 1 I 177 41 23.2 0.006 0.004 10.0

Cypermethrin I 177 0.040 2.5

Cyprodinil F 177 0.001 NT

Cyromazine R 177 0.003 - 0.010 0.05

DCPA H 177 0.001 NT

Deltamethrin 2 I 177 0.048 0.1

APPENDIX D. DISTRIBUTION OF RESIDUES BY PESTICIDE IN BUTTER

Appendix D. Page 1 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Diazinon I 177 0.001 NT

Diazinon oxygen analog IM 177 0.001 NT

Dichlobenil H 177 0.001 NT

Dichlorvos (DDVP) I 177 0.004 0.5 FF

Dicloran F 177 0.003 NT

Dicofol p,p' I 177 0.001 22.0 IT

Dicrotophos I 177 0.001 NT

Difenoconazole F 177 2 1.1 0.002 0.001 - 0.004 0.02

Diflubenzuron I 99 0.004 0.05

Dimethenamid H 177 0.001 NT

Dimethoate I 177 0.001 - 0.004 0.002

Dimethomorph F 177 0.001 NT

Dinotefuran I 177 0.007 0.05

Diphenamid H 177 0.009 NT

Diphenylamine (DPA) F 177 1 0.6 0.006 0.004 0.01

Disulfoton oxygen analog IM 177 0.001 NT

Disulfoton sulfone IM 177 0.001 NT

Disulfoton sulfoxide IM 177 0.001 NT

Diuron H 177 0.005 NT

Emamectin benzoate I 177 0.001 - 0.004 0.003

Endosulfan I IM 177 0.005 2.0 IT

Endosulfan II IM 177 0.005 2.0 IT

Endosulfan sulfate IM 177 0.021 2.0 IT

EPTC H 177 0.004 NT

Esfenvalerate+Fenvalerate Total I 177 0.009 7.0

Ethalfluralin H 177 0.003 NT

Ethiofencarb I 177 0.003 - 0.009 NT

Ethion I 177 0.004 NT

Ethoprop I 177 0.001 NT

Etofenprox I 177 0.004 0.60

Etoxazole A 158 0.004 0.01

Famoxadone F 177 0.009 0.06

Fenamidone F 177 0.003 0.02

Fenamiphos I 177 0.001 - 0.004 NT

Fenamiphos sulfone IM 177 0.002 NT

Fenamiphos sulfoxide IM 177 0.002 NT

Fenarimol F 177 0.003 NT

Fenbuconazole F 177 0.001 - 0.004 NT

Fenitrothion I 177 0.003 NT

Fenpropathrin I 177 0.003 2.0

Fenpyroximate A 118 1 0.8 0.005 0.004 0.015

Fipronil I 177 0.001 1.50

Flonicamid I 177 0.001 0.05

Flubendiamide I 177 3 1.7 0.002 0.001 1.0

Fludioxonil F 177 0.007 0.01

Flumioxazin H 177 0.004 - 0.012 NT

Appendix D. Page 2 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Fluopicolide F 177 0.004 NT

Fluopyram F 177 0.001 0.15

Fluoxastrobin F 177 0.004 0.75

Flupyradifurone I 177 0.001 0.15

Fluridone H 177 0.001 0.05

Flutriafol F 177 0.001 0.02

Fluxapyroxad F 177 0.001 0.15

Fonofos I 177 0.004 NT

Hexythiazox I 118 0.007 0.05

Hydroprene R 177 0.004 - 0.012 0.2 FF

Imidacloprid I 177 0.001 0.10

Iprodione F 177 0.011 0.5

Kresoxim-methyl F 177 0.002 NT

Linuron H 177 0.002 0.05

Malathion I 177 0.001 0.5

Malathion oxygen analog IM 177 0.002 0.5

Mandipropamid F 177 0.004 NT

Mefentrifluconazole F 177 0.001 4

Metalaxyl/Mefenoxam 3 F 177 0.001 0.02

Methamidophos I 177 0.001 0.1 TP

Methidathion I 177 0.001 NT

Methiocarb I 177 0.001 NT

Methomyl I 177 0.003 NT

Methoprene R 177 0.009 - 0.030 EX

Methoxychlor olefin IM 177 0.001 NT

Methoxyfenozide I 177 3 1.7 0.002 0.001 0.10

Metolachlor H 177 0.001 0.02

Metrafenone F 177 0.004 NT

Metribuzin H 177 0.002 0.05

Mevinphos Total I 177 0.002 NT

MGK-264 I 177 0.002 5 FF

Myclobutanil F 157 0.001 - 0.004 0.2

Napropamide H 177 0.002 NT

Norflurazon H 177 0.001 0.1

Norflurazon desmethyl HM 157 0.001 - 0.004 0.1

Novaluron I 177 75 42.4 0.002 - 0.023 0.001 20

Omethoate IM 177 0.003 0.002 TP

Oxadixyl F 177 0.004 NT

Oxamyl I 177 0.002 NT

Oxyfluorfen H 177 0.004 0.01

Parathion ethyl I 177 0.004 NT

Parathion methyl I 177 0.003 NT

Parathion oxygen analog IM 177 0.001 NT

Pendimethalin H 177 0.004 0.04

Pentachloroaniline (PCA) FM 177 0.001 NT

Pentachlorophenyl methyl sulfide (PCPMS) FM 177 0.001 NT

Appendix D. Page 3 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Penthiopyrad F 177 0.001 - 0.004 0.02

Permethrin cis IM 177 71 40.1 0.002 - 0.007 0.001 3.0

Permethrin trans IM 177 69 39 0.002 - 0.008 0.001 3.0

Phenothrin I 177 0.003 0.01 FF

Phenthoate I 177 0.001 NT

Phorate I 58 0.004 NT

Phorate oxygen analog IM 177 0.001 NT

Phorate oxygen analog sulfone IM 177 0.001 NT

Phorate oxygen analog sulfoxide IM 177 0.001 NT

Phorate sulfone IM 177 0.002 NT

Phorate sulfoxide IM 177 0.001 NT

Phosalone I 177 0.006 NT

Phosmet I 177 0.006 0.1

Phosphamidon I 177 0.001 NT

Picoxystrobin F 177 0.001 - 0.004 0.01

Piperonyl butoxide I 177 42 23.7 0.003 - 0.009 0.002 - 0.006 0.25

Pirimicarb I 177 0.001 NT

Pirimiphos methyl I 177 0.001 NT

Profenofos I 177 0.004 0.01

Prometon H 177 0.001 NT

Prometryn H 177 0.001 - 0.004 NT

Pronamide (Propyzamide) H 177 0.001 0.02

Propachlor H 177 0.001 0.02

Propargite I 116 0.007 - 0.024 2.0

Propetamphos I 157 0.004 NT

Propiconazole F 177 0.005 0.05

Pydiflumetofen F 177 0.004 0.03

Pymetrozine I 177 0.002 NT

Pyraclostrobin F 177 2 1.1 0.002 0.001 - 0.004 0.1

Pyrimethanil F 177 0.001 0.05

Pyriproxyfen I 177 0.004 0.10 SU

Quinoxyfen F 177 0.001 NT

Quintozene (PCNB) F 177 0.004 NT

Resmethrin trans IM 177 0.003 3.0 FF

Simazine H 177 0.004 0.03

metabolite) I 177 0.003 0.25

Spirotetramat I 177 0.002 - 0.006 0.01

Sulfoxaflor I 177 0.001 0.3

Sulprofos I 177 0.002 NT

Tebuconazole F 177 0.001 - 0.004 0.1

Tebupirimfos I 177 0.001 NT

Tebuthiuron H 177 0.001 0.8

Tecnazene P 177 0.001 NT

Tefluthrin I 177 0.001 NT

Terbacil H 177 0.004 NT

Terbufos sulfone IM 177 0.001 - 0.004 NT

Appendix D. Page 4 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Tetrachlorvinphos I 177 0.002 - 0.006 0.05

Tetraconazole F 119 0.001 0.75

Tetradifon I 177 0.003 NT

Tetrahydrophthalimide (THPI) FM 177 0.015 0.10

Tetraniliprole I 177 0.001 - 0.004 0.05

Thiabendazole F 177 1 0.6 0.004 0.001 - 0.004 0.1

Thiacloprid I 177 0.001 0.030 FU

Thiamethoxam I 177 0.006 0.02

Thiobencarb H 177 0.004 0.05

Triadimefon F 177 0.001 NT

Trifloxystrobin F 177 0.004 0.02

Triflumizole F 177 0.002 NT

Trifluralin H 177 0.001 NT

Vinclozolin F 177 0.001 0.05 IT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. 

 Refer to pages 4 through 7 in Appendix J to see the number of occurrences broken down by sample origin

 (domestic, imported, or unknown) for a commodity/pesticide pair.

1 = Includes cyhalothrin lambda plus R157836 epimer.

2 = Deltamethrin includes parent Tralomethrin.

3 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

P = Plant Growth Regulator

R = Insect Growth Regulator

S = Herbicide Safener

EPA Tolerance Codes:

EX = Exempt from the requirement of a tolerance.

FF = All food/feed commodities tolerance except those covered by a higher tolerance.

FU = Foreign use compound; There are no U.S. registrations.

IT = Interim Tolerance/Temporary or time limited tolerance/Section 18.

NT = No tolerance established.

SU = Safe when used as a crack and crevice treatment in food establishments; no tolerance published.

TP = Tolerance is from parent compound.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is advised to refer 

to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply to 2021 and not to the 

current year. There may be instances where a tolerance was recently set or revoked that would have an effect on whether a 

residue is violative or not. 

Appendix D. Page 5 of 5
Appendix E

Distribution of Residues 

for Environmental Contaminants

Appendix E shows residue detections across all commodities for 21 compounds identified as 

environmental contaminants, including range of values detected, range of Limits of Detection 

(LODs), and U.S. Environmental Protection Agency (EPA) tolerances or U.S. Food and Drug 

Administration (FDA) Action Levels for each pair. Results for environmental contaminants have 

been consolidated in this appendix because they have no registered uses and are not applied to 

crops. 

The EPA tolerances cited in this summary and appendixes apply to 2021 and not to the current 

year. There may be instances where tolerances have been recently set, modified or revoked 

that would have an effect on whether a residue is violative or not.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by FDA. ALs are used for environmental contaminants when tolerances are not 

available. 

The Pesticide Data Program (PDP) reports tolerance violations to FDA as part of an interagency 

Memorandum of Understanding between the U.S. Department of Agriculture and FDA. 

Residues reported to FDA are shown in the “Pesticide/Commodity” column to the right of the 

commodity and are annotated as “X” (if the residue exceeded the established tolerance) or “V” 

(if the residue did not have a tolerance listed in the Code of Federal Regulations, Title 40, Part 

180). In both cases, these annotations are followed by a number indicating the number of 

samples reported to FDA. 
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Aldrin (insecticide) (parent of Dieldrin)

Blueberries, Cultivated, Fresh 692 0 0.003 0.05 AL

Blueberries, Frozen 14 0 0.003 0.05 AL

Broccoli 708 0 0.001 0.03 AL

Butter 177 0 0.001 - 0.004 0.3 AL

Cantaloupe 328 0 0.003 0.1 AL

Carrots 708 0 0.020 0.1 AL

Cauliflower 531 0 0.001 0.03 AL

Celery 354 0 0.005 0.03 AL

Corn Grain 418 0 0.010 0.02 AL

Eggplant 703 0 0.001 - 0.020 0.05 AL

Grape Juice 700 0 0.003 0.05 AL

Green Beans 700 0 0.001 0.05 AL

Peaches 518 0 0.005 0.02 AL

Peaches, Frozen 154 0 0.005 0.02 AL

Pears 707 0 0.003 0.03 AL

Plums 277 0 0.003 0.3 AL

Summer Squash 698 0 0.001 - 0.005 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.05 AL

Tangerines 531 0 0.005 0.02 AL

Watermelon 175 0 0.005 0.1 AL

Winter Squash 706 0 0.001 0.1 AL

TOTAL 10,127 0

BHC alpha (insecticide) (isomer of BHC)

Blueberries, Cultivated, Fresh 692 0 0.012 0.05 AL

Blueberries, Frozen 14 0 0.012 0.05 AL

Broccoli 708 0 0.001 0.05 AL

Butter 177 0 0.001 0.3 AL

Cantaloupe 328 0 0.012 0.05 AL

Carrots 708 0 0.005 0.3 AL

Cauliflower 531 0 0.001 0.05 AL

Celery 354 0 0.005 0.05 AL

Eggplant 703 0 0.001 - 0.005 0.05 AL

Grape Juice 700 0 0.002 0.05 AL

Green Beans 700 0 0.001 0.05 AL

Peaches 518 0 0.005 0.05 AL

Peaches, Frozen 154 0 0.005 0.05 AL

Pears 707 0 0.002 0.05 AL

Plums 277 0 0.012 0.05 AL

Summer Squash 698 0 0.001 - 0.010 0.05 AL

Sweet Bell Peppers 328 0 0.005 0.05 AL

Tangerines 531 0 0.010 0.05 AL

Watermelon 175 0 0.010 0.05 AL

Winter Squash 706 0 0.001 0.05 AL

TOTAL 9,709 0

BHC beta (isomer of BHC)

Blueberries, Cultivated, Fresh 692 0 0.014 0.05 AL

Blueberries, Frozen 14 0 0.014 0.05 AL

Cantaloupe 328 0 0.014 0.05 AL

Celery 354 0 0.005 0.05 AL

Grape Juice 700 0 0.003 0.05 AL

Green Beans 700 0 0.001 0.05 AL

Peaches 518 0 0.005 0.05 AL

APPENDIX E. DISTRIBUTION OF RESIDUES FOR ENVIRONMENTAL CONTAMINANTS

Appendix E. Page 1 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 0.05 AL

Pears 707 0 0.003 0.05 AL

Plums 277 0 0.014 0.05 AL

Summer Squash 698 0 0.001 - 0.005 0.05 AL

Sweet Bell Peppers 328 0 0.005 0.05 AL

Tangerines 531 0 0.005 0.05 AL

Watermelon 175 0 0.005 0.05 AL

Winter Squash 706 0 0.001 0.05 AL

TOTAL 6,882 0

BHC delta (isomer of BHC)

Carrots 708 0 0.005 0.3 AL

Eggplant 346 0 0.005 0.05 AL

Green Beans 700 0 0.001 0.05 AL

Summer Squash 365 0 0.001 0.05 AL

Winter Squash 706 0 0.001 0.05 AL

TOTAL 2,825 0

BHC epsilon (isomer of BHC)

Carrots 708 0 0.005 0.3 AL

Eggplant 346 0 0.005 0.05 AL

TOTAL 1,054 0

Chlordane cis (insecticide) (isomer of Chlordane)

Blueberries, Cultivated, Fresh 692 0 0.010 0.1 AL

Blueberries, Frozen 14 0 0.010 0.1 AL

Broccoli 708 0 0.001 0.1 AL

Butter 177 0 0.001 NT

Cantaloupe 328 0 0.010 0.1 AL

Carrots 708 0 0.010 0.1 AL

Cauliflower 531 0 0.001 0.1 AL

Celery 354 0 0.005 0.1 AL

Eggplant 703 1 0.1 0.005 0.001 - 0.010 0.1 AL

Grape Juice 700 0 0.002 0.1 AL

Green Beans 700 0 0.001 0.1 AL

Peaches 518 0 0.005 0.1 AL

Peaches, Frozen 154 0 0.005 0.1 AL

Pears 707 0 0.002 0.1 AL

Plums 277 0 0.010 0.1 AL

Summer Squash 365 5 1.4 0.001 - 0.004 0.001 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.1 AL

Tangerines 531 0 0.010 0.1 AL

Winter Squash 706 9 1.3 0.001 - 0.020 0.001 0.1 AL

TOTAL 9,201 15

Chlordane trans (isomer of Chlordane)

Blueberries, Cultivated, Fresh 692 0 0.010 0.1 AL

Blueberries, Frozen 14 0 0.010 0.1 AL

Broccoli 708 2 0.3 0.002 - 0.017 0.001 0.1 AL

Butter 177 0 0.001 NT

Cantaloupe 328 0 0.010 0.1 AL

Carrots 708 0 0.010 0.1 AL

Cauliflower 531 0 0.001 0.1 AL

Celery 354 0 0.005 0.1 AL

Eggplant 703 0 0.001 - 0.010 0.1 AL

Grape Juice 700 0 0.002 0.1 AL

Green Beans 700 0 0.001 0.1 AL

Peaches 518 0 0.005 0.1 AL

Appendix E. Page 2 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 0.1 AL

Pears 707 0 0.002 0.1 AL

Plums 277 0 0.010 0.1 AL

Summer Squash 365 0 0.001 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.1 AL

Tangerines 531 0 0.005 0.1 AL

Winter Squash 706 8 1.1 0.001 - 0.010 0.001 0.1 AL

TOTAL 9,201 10

DDD o,p' (metabolite of DDT)

Blueberries, Cultivated, Fresh 692 0 0.001 0.1 AL

Blueberries, Frozen 14 0 0.001 0.1 AL

Broccoli 708 0 0.001 0.5 AL

Butter 177 0 0.001 1.25 AL

Cantaloupe 328 0 0.001 0.1 AL

Cauliflower 531 0 0.001 0.5 AL

Corn Grain 418 0 0.020 0.5 AL

Eggplant 357 0 0.001 0.1 AL

Green Beans 700 0 0.001 0.2 AL

Plums 277 0 0.001 0.2 AL

Summer Squash 365 1 0.3 0.001 0.001 0.1 AL

Winter Squash 706 3 0.4 0.001 - 0.002 0.001 0.1 AL

TOTAL 5,273 4

DDD p,p' (metabolite of DDT)

Blueberries, Cultivated, Fresh 692 0 0.005 0.1 AL

Blueberries, Frozen 14 0 0.005 0.1 AL

Broccoli 708 0 0.001 0.5 AL

Butter 177 0 0.001 1.25 AL

Cantaloupe 328 0 0.005 0.1 AL

Carrots 708 0 0.005 3.0 AL

Cauliflower 531 0 0.001 0.5 AL

Celery 354 0 0.005 0.5 AL

Corn Grain 418 0 0.001 0.5 AL

Eggplant 703 0 0.001 - 0.005 0.1 AL

Peaches 518 0 0.005 0.2 AL

Peaches, Frozen 154 0 0.005 0.2 AL

Plums 277 0 0.005 0.2 AL

Summer Squash 333 1 0.3 0.005 0.005 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.1 AL

Tangerines 531 0 0.005 0.1 AL

Watermelon 175 0 0.005 0.1 AL

TOTAL 6,949 1

DDE o,p' (metabolite of DDT)

Blueberries, Cultivated, Fresh 692 0 0.001 0.1 AL

Blueberries, Frozen 14 0 0.001 0.1 AL

Cantaloupe 328 0 0.001 0.1 AL

Corn Grain 418 0 0.001 0.5 AL

Grape Juice 700 0 0.003 0.05 AL

Green Beans 700 0 0.001 0.2 AL

Pears 707 0 0.003 0.1 AL

Plums 277 0 0.001 0.2 AL

Summer Squash 365 0 0.001 0.1 AL

Winter Squash 706 0 0.001 0.1 AL

TOTAL 4,907 0

Appendix E. Page 3 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

DDE p,p' (metabolite of DDT)

Blueberries, Cultivated, Fresh 692 0 0.010 0.1 AL

Blueberries, Frozen 14 0 0.010 0.1 AL

Broccoli 708 35 4.9 0.002 - 0.005 0.001 0.5 AL

Butter 177 80 45.2 0.002 - 0.014 0.001 1.25 AL

Cantaloupe 328 0 0.010 0.1 AL

Carrots 708 17 2.4 0.010 - 0.030 0.010 3.0 AL

Cauliflower 531 0 0.001 0.5 AL

Celery 354 2 0.6 0.006 - 0.008 0.005 0.5 AL

Corn Grain 418 0 0.001 0.5 AL

Eggplant 703 0 0.001 - 0.010 0.1 AL

Grape Juice 700 0 0.002 0.05 AL

Green Beans 700 15 2.1 0.001 - 0.005 0.001 0.2 AL

Peaches 518 0 0.005 0.2 AL

Peaches, Frozen 154 0 0.005 0.2 AL

Pears 707 0 0.002 0.1 AL

Plums 277 0 0.010 0.2 AL

Summer Squash 365 19 5.2 0.001 - 0.008 0.001 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.1 AL

Tangerines 531 1 0.2 0.005 0.005 0.1 AL

Winter Squash 706 21 3 0.001 - 0.007 0.001 0.1 AL

TOTAL 9,619 190

DDT o,p' (insecticide) 

Broccoli 708 0 0.001 0.5 AL

Butter 177 0 0.001 1.25 AL

Cauliflower 531 0 0.001 0.5 AL

Eggplant 357 0 0.001 0.1 AL

Grape Juice 700 0 0.004 0.05 AL

Green Beans 700 0 0.001 0.2 AL

Pears 707 0 0.004 0.1 AL

Summer Squash 365 14 3.8 0.001 - 0.005 0.001 0.1 AL

Winter Squash 671 7 1 0.001 - 0.007 0.001 0.1 AL

TOTAL 4,916 21

DDT p,p' (insecticide) 

Blueberries, Cultivated, Fresh 638 0 0.001 0.1 AL

Blueberries, Frozen 12 0 0.001 0.1 AL

Broccoli 708 0 0.001 - 0.003 0.5 AL

Butter 177 0 0.001 - 0.007 1.25 AL

Cantaloupe 328 0 0.001 0.1 AL

Carrots 708 1 0.1 0.011 0.010 3.0 AL

Cauliflower 531 0 0.001 0.5 AL

Celery 354 0 0.005 0.5 AL

Corn Grain 418 0 0.005 0.5 AL

Eggplant 703 0 0.003 - 0.010 0.1 AL

Grape Juice 700 0 0.004 0.05 AL

Green Beans 700 0 0.001 0.2 AL

Peaches 518 0 0.005 0.2 AL

Peaches, Frozen 154 0 0.005 0.2 AL

Pears 707 0 0.004 0.1 AL

Plums 250 0 0.001 0.2 AL

Summer Squash 365 7 1.9 0.001 - 0.009 0.001 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.1 AL

Winter Squash 705 7 1 0.002 - 0.015 0.001 0.1 AL

TOTAL 9,004 15

Appendix E. Page 4 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Dieldrin (insecticide) (also a metabolite of Aldrin)

Blueberries, Cultivated, Fresh 692 0 0.010 0.05 AL

Blueberries, Frozen 14 0 0.010 0.05 AL

Broccoli 708 3 0.4 0.004 0.002 0.03 AL

Butter 177 0 0.003 0.3 AL

Cantaloupe 328 1 0.3 0.011 0.010 0.1 AL

Carrots 708 0 0.020 0.1 AL

Cauliflower 531 0 0.002 0.03 AL

Celery 354 0 0.005 0.03 AL

Corn Grain 418 0 0.010 0.02 AL

Eggplant 703 0 0.002 - 0.020 0.05 AL

Grape Juice 700 0 0.006 0.05 AL

Green Beans 700 0 0.003 0.05 AL

Peaches 518 0 0.005 0.02 AL

Peaches, Frozen 154 0 0.005 0.02 AL

Pears 707 0 0.006 0.03 AL

Plums 277 0 0.010 0.3 AL

Summer Squash 365 29 7.9 0.003 - 0.060 0.003 0.1 AL

Sweet Bell Peppers 328 0 0.005 0.05 AL

Tangerines 531 0 0.025 0.02 AL

Winter Squash 706 71 10.1 0.003 - 0.19 0.003 0.1 AL

TOTAL 9,619 104

Endrin (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.010 NT

Blueberries, Frozen 14 0 0.010 NT

Broccoli 708 0 0.005 NT

Butter 177 0 0.006 NT

Cantaloupe 328 0 0.010 NT

Carrots 708 0 0.020 NT

Cauliflower 531 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 703 0 0.005 - 0.020 NT

Green Beans 700 0 0.003 NT

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.010 NT

Summer Squash (V-7) 698 7 1 0.003 - 0.018 0.003 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash (V-9) 706 9 1.3 0.003 - 0.014 0.003 NT

TOTAL 8,302 16

Heptachlor (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.002 0.05 AL

Blueberries, Frozen 14 0 0.002 0.05 AL

Broccoli 708 0 0.001 0.05 AL

Butter 177 0 0.001 NT

Cantaloupe 328 0 0.002 0.05 AL

Carrots 708 0 0.025 NT

Cauliflower 531 0 0.001 0.05 AL

Celery 354 0 0.005 0.05 AL

Eggplant 703 0 0.001 - 0.025 0.03 AL

Grape Juice 700 0 0.002 0.05 AL

Green Beans 700 0 0.001 0.05 AL

Peaches 518 0 0.005 0.05 AL

Peaches, Frozen 154 0 0.005 0.05 AL

Pears 707 0 0.002 0.05 AL

Appendix E. Page 5 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Plums 277 0 0.002 0.05 AL

Summer Squash 698 0 0.001 0.05 AL

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.001 0.05 AL

Watermelon 175 0 0.001 0.05 AL

Winter Squash 706 0 0.001 0.05 AL

TOTAL 9,709 0

Heptachlor epoxide (metabolite of Heptachlor)

Blueberries, Cultivated, Fresh 692 0 0.005 0.05 AL

Blueberries, Frozen 14 0 0.005 0.05 AL

Broccoli 708 0 0.002 0.05 AL

Butter 177 0 0.003 NT

Cantaloupe 328 0 0.005 0.05 AL

Carrots 708 0 0.040 NT

Cauliflower 531 0 0.002 0.05 AL

Celery 354 0 0.005 0.05 AL

Eggplant 703 0 0.002 - 0.040 0.03 AL

Grape Juice 700 0 0.003 0.05 AL

Green Beans 700 0 0.001 0.05 AL

Peaches 518 0 0.005 0.05 AL

Peaches, Frozen 154 0 0.005 0.05 AL

Pears 707 0 0.003 0.05 AL

Plums 277 0 0.005 0.05 AL

Summer Squash 698 15 2.1 0.001 - 0.006 0.001 0.05 AL

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.001 0.05 AL

Watermelon 175 0 0.001 0.05 AL

Winter Squash 706 8 1.1 0.002 - 0.050 0.001 0.05 AL

TOTAL 9,709 23

Hexachlorobenzene - HCB (fungicide) (metabolite and impurity of Quintozene)

Carrots 708 0 0.005 NT

Celery 354 0 0.005 NT

Eggplant 346 0 0.005 0.1

Green Beans 700 0 0.001 0.1

Peaches 518 0 0.005 NT

Peaches, Frozen 154 0 0.005 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 0.1

Tangerines 531 0 0.005 NT

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 5,218 0

Lindane - BHC gamma (insecticide) (also an isomer of BHC)

Blueberries, Cultivated, Fresh 692 0 0.013 0.5 AL

Blueberries, Frozen 14 0 0.013 0.5 AL

Broccoli 708 0 0.001 NT

Butter 177 0 0.001 0.3 AL

Cantaloupe 328 0 0.013 NT

Carrots 708 0 0.005 0.5 AL

Cauliflower 531 0 0.001 NT

Celery 354 0 0.005 NT

Corn Grain 418 0 0.001 0.1 AL

Eggplant 703 0 0.001 - 0.005 NT

Green Beans 700 0 0.001 0.5 AL

Peaches 518 0 0.005 NT

Appendix E. Page 6 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Peaches, Frozen 154 0 0.005 NT

Plums 277 0 0.013 NT

Summer Squash 698 0 0.001 - 0.005 NT

Sweet Bell Peppers 328 0 0.005 NT

Tangerines 531 0 0.005 0.5 AL

Watermelon 175 0 0.005 NT

Winter Squash 706 0 0.001 NT

TOTAL 8,720 0

Mirex (insecticide) 

Blueberries, Cultivated, Fresh 692 0 0.001 NT

Blueberries, Frozen 14 0 0.001 NT

Cantaloupe 328 0 0.001 NT

Green Beans 700 0 0.001 NT

Plums 277 0 0.001 NT

Summer Squash 365 0 0.001 NT

Winter Squash 706 0 0.001 NT

TOTAL 3,082 0

Oxychlordane (metabolite of Chlordane)

Green Beans 679 0 0.005 0.1 AL

Summer Squash 327 0 0.005 0.1 AL

Winter Squash 706 1 0.1 0.011 0.005 0.1 AL

TOTAL 1,712 1

NOTES

^ = When a range is not listed, only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 4 through 7 in Appendix J to see the number of occurrences broken down by sample origin (domestic, imported, or unknown).

Appendix E. Page 7 of 7
Appendix F

Sample Origin by State or Country

(Determined by Grower, Packer, or Distributor)

Appendix F gives the number of samples per State or country of origin and the number of 

samples of unknown origin. Where available, the origin of fresh commodities is taken from the 

grower or packer information. For processed commodities, origin is determined primarily by 

packer or distributor. 

As shown in Appendix F, samples originated from 42 States and 26 foreign countries. 

There were 366 domestic samples from unknown States. There were an additional 48 

samples from unknown origins. Overall, 66.5 percent of samples were from U.S. sources, 

32.1 percent were imports from single countries, 0.9 percent were of mixed national origin, and 

0.5 percent were of unknown origin. 

Corn grain is excluded from Appendix F because the targeted corn samples rely on a different 

sampling frame and are not collected from routine Pesticide Data Program (PDP) sample 

collection locations. The origins for the corn grain samples are shown on Figure 5.
Part 1. Domestic Samples

Dairy # of % of

BB BR CE CF CN CR EP GB PC PE PP PU SS TA WM WS BZ GJ HZ BU Samples Total

Alabama 4 1 3 8 0.1

Arizona 9 7 17 32 1 2 1 4 2 2 1 78 0.8

Arkansas 2 2 2 3 3 5 25 5 9 56 0.6

California 119 469 266 447 46 376 111 113 235 102 27 242 79 262 19 119 1 105 57 23 3218 33.1

Colorado 2 6 1 1 6 1 9 3 7 3 10 1 8 3 61 0.6

Connecticut 2 3 1 1 1 8 0.1

Delaware 3 2 1 6 0.1

Florida 29 6 7 4 2 17 71 106 2 1 54 57 18 8 15 21 418 4.3

Georgia 8 5 1 64 19 17 10 46 22 192 2.0

Idaho 2 2 11 5 2 22 0.2

Illinois 4 10 2 1 20 13 1 6 6 1 26 14 104 1.1

Indiana 1 1 3 1 6 0.1

Iowa 1 1 < 0.1

Kansas 5 5 0.1

Kentucky 1 1 < 0.1

Louisiana 1 1 < 0.1

Maine 4 1 3 1 2 1 3 1 1 17 0.2

Maryland 1 3 3 1 2 9 17 8 6 2 20 2 5 5 6 1 91 0.9

Massachusetts 1 219 220 2.3

Michigan 23 1 18 1 15 16 27 4 1 25 2 39 1 36 12 13 234 2.4

Minnesota 3 2 1 1 5 3 31 46 0.5

Missouri 1 1 2 < 0.1

Montana 2 2 < 0.1

Nevada 5 1 6 0.1

New Hampshire 4 1 2 7 0.1

New Jersey 12 2 1 16 9 7 2 4 1 6 4 1 65 0.7

New Mexico 1 1 < 0.1

New York 1 16 1 5 2 13 4 1 12 1 5 13 1 12 6 10 103 1.1

North Carolina 17 6 13 5 3 3 10 7 1 1 1 67 0.7

Ohio 2 4 3 26 13 20 4 4 3 21 4 19 24 15 10 172 1.8

Oklahoma 1 1 < 0.1

Oregon 14 5 104 1 3 5 2 2 136 1.4

Pennsylvania 4 1 16 4 1 2 1 1 5 1 5 41 0.4

Rhode Island 5 1 1 7 0.1

South Carolina 1 3 33 1 1 39 0.4

Tennessee 1 1 4 3 9 0.1

Texas 2 10 7 11 5 16 12 44 6 13 5 2 29 4 10 2 19 14 7 218 2.2

Vermont 2 2 < 0.1

Virginia 2 3 1 1 7 0.1

Washington 14 8 10 6 1 8 4 4 313 1 1 8 9 2 9 398 4.1

West Virginia 2 2 < 0.1

Wisconsin 1 1 7 9 0.1

Unknown State 12 19 12 21 9 10 47 42 27 18 11 18 35 15 18 29 16 1 6 366 3.8

# of Domestic 261 581 338 507 83 534 393 485 369 569 121 277 377 324 70 311 3 552 128 170 6,453

% of Total 38 82 95 95 25 75 56 69 71 80 37 100 54 61 40 44 21 79 83 96 66.5

Fresh F&V

APPENDIX F. SAMPLE ORIGIN BY STATE OR COUNTRY 1

(Determined by Grower, Packer, or Distributor)

Processed F&V

Appendix F. Page 1 of 3
Part 2. Imported Samples

Dairy # of % of

BB BR CE CF CN CR EP GB PC PE PP PU SS TA WM WS BZ GJ HZ BU Samples Total

Argentina 9 103 35 147 1.5

Australia 1 9 10 0.1

Canada 41 7 7 5 112 8 20 6 14 5 2 227 2.3

Chile 84 148 28 55 5 3 6 329 3.4

China 1 1 < 0.1

Costa Rica 8 8 0.1

France 1 1 < 0.1

Germany 1 1 < 0.1

Greece 16 16 0.2

Guatemala 160 36 1 1 8 206 2.1

Honduras 64 1 5 24 94 1.0

Ireland 4 4 < 0.1

Israel 13 9 22 0.2

Japan 2 2 < 0.1

Mexico 135 119 8 16 13 48 289 173 2 181 305 1 97 353 1 1 1742 17.9

Morocco 22 22 0.2

Netherlands 5 5 0.1

New Zealand 1 1 < 0.1

Peru 160 1 75 236 2.4

Poland 1 1 < 0.1

South Africa 1 10 11 0.1

Turkey 2 2 < 0.1

Uruguay 2 26 28 0.3

# of Imports 431 126 15 21 245 173 303 209 148 136 207 0 312 207 105 391 11 43 26 7 3,116

% of Total 62 18 4 4 75 24 43 30 29 19 63 0 45 39 60 55 79 6 17 4 32.1

Part 3. Mixed National Origin Samples

Dairy # of % of

BB BR CE CF CN CR EP GB PC PE PP PU SS TA WM WS BZ GJ HZ BU Samples Total

Argentina / Brazil / Chile / Mexico / Spain / USA 1 1 < 0.1

Argentina / Brazil / Chile / USA 1 1 < 0.1

Argentina / Chile / Mexico / Spain / USA 1 1 < 0.1

Argentina / Chile / USA 3 3 < 0.1

Argentina / Spain 1 1 < 0.1

Argentina / Spain / USA 15 15 0.2

Argentina / USA 61 61 0.6

Austria / Mexico / USA 1 1 < 0.1

Brazil / USA 1 1 < 0.1

Chile / USA 6 6 0.1

South Africa / USA 1 1 < 0.1

# of Mixed National Origin Samples 92 92

% of Total 13 0.9

Fresh F&V Processed F&V

Fresh F&V Processed F&V

Appendix F. Page 2 of 3
Part 4. Unknown Origin Samples

Dairy # of % of

BB BR CE CF CN CR EP GB PC PE PP PU SS TA WM WS BZ GJ HZ BU Samples Total

Unknown Origin 1 1 3 1 7 6 1 2 9 4 13 48

% of Total < 1 < 1 1 < 1 1 1 < 1 < 1 1 1 2 0.5

Sample Totals: 692 708 354 531 328 708 703 700 518 707 328 277 698 531 175 706 14 700 154 177 9,709

NOTES

1 = Excludes corn grain samples. The origins for corn grain samples are shown on Figure 5.

Commodity Legend

BB = Blueberries, Cultivated, Fresh CR = Carrots PP = Sweet Bell Peppers

BR = Broccoli EP = Eggplant PU = Plums

BU = Butter GB = Green Beans SS = Summer Squash

BZ = Blueberries, Frozen GJ = Grape Juice TA = Tangerines

CE = Celery HZ = Peaches, Frozen WM = Watermelon

CF = Cauliflower PC = Peaches, Fresh WS = Winter Squash

CN = Cantaloupe PE = Pears

Fresh F&V Processed F&V

Appendix F. Page 3 of 3
Appendix G 

Import Versus Domestic Pesticide Residue Comparisons

 

The Pesticide Data Program is designed to provide a comprehensive statistical picture of 

pesticide residues in the U.S. food supply, representing all sources, including imports. Most 

commodities consumed are generally produced in the United States with import components 

that vary by commodity. However, several commodities tested over the past several years were 

cyclical; that is, part of the year the commodity was produced domestically and part of the year it 

was imported. 

Appendix G compares residue data reported for samples originating in the United States with 

those of the same commodity from major exporting countries in 2021. Residue data for 

domestic fresh blueberries are compared with data for samples originating in both Mexico and 

Peru. Residue data for domestic green beans are compared with data for samples originating in 

Mexico. Residue data for domestic peaches are compared with data for samples originating in 

Chile. Residue data for domestic pears are compared with data for samples originating in 

Argentina. These commodities were selected because they are fresh products collected all 12 

months of the year and they have more than 100 data points (samples) for each of the countries 

compared. Only residues detected in more than 5 percent of all samples are included in each 

comparison. All pesticides detected were registered in the United States. However, the profiles 

of residue findings were markedly different in the United States samples versus samples from 

these exporting countries. The differences in residue detections between countries were likely 

due to the pesticides used in response to pest pressures based on differing environmental and 

climatic conditions as well as crop production and protection practices. 
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Acetamiprid United States 261 43 16.5 0.002 - 0.45 1.6

Mexico 135 52 38.5 0.002 - 0.19 1.6

Peru 160 91 56.9 0.002 - 2.0 1.6

Azoxystrobin United States 261 91 34.9 0.002 - 0.72 10.0

Mexico 135 56 41.5 0.002 - 0.31 10.0

Peru 160 31 19.4 0.002 - 0.18 10.0

Bifenthrin United States 261 53 20.3 0.002 - 0.71 3

Mexico 135 32 23.7 0.002 - 0.44 3

Peru 160 0 3

Boscalid United States 261 48 18.4 0.004 - 1.7 13.0

Mexico 135 65 48.1 0.004 - 2.1 13.0

Peru 160 105 65.6 0.004 - 2.1 13.0

Cypermethrin United States 261 92 35.2 0.010 - 0.60 0.8

Mexico 135 54 40 0.010 - 0.54 0.8

Peru 160 0 0.8

Cyprodinil United States 261 76 29.1 0.005 - 0.66 5.0

Mexico 135 52 38.5 0.005 - 1.0 5.0

Peru 160 53 33.1 0.005 - 1.0 5.0

Difenoconazole United States 261 1 0.4 0.77 4.0

Mexico 135 9 6.7 0.029 - 0.10 4.0

Peru 160 28 17.5 0.010 - 0.77 4.0

Fenhexamid United States 261 17 6.5 0.016 - 1.1 5

Mexico 135 21 15.6 0.016 - 0.49 5

Peru 160 46 28.7 0.016 - 1.2 5

Fludioxonil United States 261 43 16.5 0.026 - 1.5 3.0

Mexico 135 46 34.1 0.025 - 1.4 3.0

Peru 160 50 31.2 0.026 - 1.7 3.0

Fluopyram United States 261 30 11.5 0.005 - 0.43 7.0

Mexico 135 0 7.0

Peru 160 4 2.5 0.005 - 0.08 7.0

Appendix G. Import Versus Domestic Pesticide Residue Comparisons

2021 Distribution of Residues for Fresh Blueberry Samples

Originating in Mexico and Peru Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix G. Page 1 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Imidacloprid United States 261 30 11.5 0.003 - 0.27 3.5

Mexico 135 17 12.6 0.003 - 0.51 3.5

Peru 160 16 10 0.003 - 0.025 3.5

Malathion United States 261 48 18.4 0.002 - 0.15 8

Mexico 135 4 3 0.002 - 0.012 8

Peru 160 0 8

Phosmet United States 261 40 15.3 0.010 - 1.6 10

Mexico 135 3 2.2 0.019 - 0.20 10

Peru 160 0 10

Pyraclostrobin United States 261 23 8.8 0.004 - 0.22 4.0

Mexico 135 38 28.1 0.004 - 0.56 4.0

Peru 160 44 27.5 0.003 - 0.49 4.0

Spinetoram United States 261 6 2.3 0.004 - 0.014 0.90

Mexico 135 15 11.1 0.003 - 0.035 0.90

Peru 160 5 3.1 0.004 - 0.036 0.90

Spinosad A United States 261 19 7.3 0.004 - 0.089 0.90

Mexico 135 12 8.9 0.004 - 0.17 0.90

Peru 160 3 1.9 0.004 - 0.012 0.90

Tetrahydrophthalimide (THPI) United States 261 87 33.3 0.010 - 4.0 20.0 TP

Mexico 135 20 14.8 0.010 - 0.22 20.0 TP

Peru 160 2 1.2 0.018 - 0.040 20.0 TP

NOTE: The Limits of Detection (LODs) for pesticide detections in blueberries are listed in Appendix B.

Appendix G. Page 2 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Acephate United States 485 22 4.5 0.006 - 10 0.02 FF

Mexico 173 20 11.6 0.006 - 0.73 0.02 FF

Azoxystrobin United States 485 158 32.6 0.001 - 0.58 3.0

Mexico 173 18 10.4 0.002 - 0.08 3.0

Bifenthrin United States 485 139 28.7 0.001 - 0.15 0.6

Mexico 173 37 21.4 0.002 - 0.077 0.6

Boscalid United States 485 41 8.5 0.004 - 0.23 5.0

Mexico 173 16 9.2 0.003 - 0.069 5.0

Carbendazim (MBC) United States 485 136 28 0.002 - 0.26 2.0 TP

Mexico 173 89 51.4 0.001 - 0.10 2.0 TP

Chlorantraniliprole United States 485 41 8.5 0.005 - 0.048 2.0

Mexico 173 4 2.3 0.005 - 0.035 2.0

Chlorothalonil United States 485 73 15.1 0.005 - 0.73 5

Mexico 173 19 11 0.006 - 0.19 5

Cyhalothrin, Total United States 485 62 12.8 0.003 - 0.056 0.20

Mexico 173 29 16.8 0.003 - 0.033 0.20

Cypermethrin United States 485 86 17.7 0.005 - 0.19 0.7

Mexico 173 16 9.2 0.006 - 0.070 0.7

Dicloran United States 485 42 8.7 0.001 - 2.2 20

Mexico 173 19 11 0.002 - 0.44 20

Imidacloprid desnitro United States 470 16 3.4 0.001 - 0.023 4.0

Mexico 168 32 19 0.001 - 0.023 4.0

Metalaxyl/Mefenoxam United States 485 32 6.6 0.001 - 0.022 0.2

Mexico 173 9 5.2 0.001 - 0.023 0.2

Methamidophos United States 485 23 4.7 0.001 - 1.9 0.02 TP

Mexico 173 23 13.3 0.002 - 0.33 0.02 TP

Myclobutanil United States 485 39 8 0.003 - 0.096 1.0

Mexico 173 10 5.8 0.004 - 0.089 1.0

2021 Distribution of Residues for Green Bean Samples

Originating in Mexico Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix G. Page 3 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Novaluron United States 485 43 8.9 0.003 - 0.11 0.70

Mexico 173 4 2.3 0.016 - 0.028 0.70

Omethoate United States 485 28 5.8 0.001 - 0.039 2.0 TP

Mexico 173 2 1.2 0.003 - 0.011 2.0 TP

Penthiopyrad United States 485 46 9.5 0.001 - 0.11 4.0

Mexico 173 3 1.7 0.001 - 0.020 4.0

Pyraclostrobin United States 485 111 22.9 0.001 - 0.20 0.5

Mexico 173 19 11 0.003 - 0.13 0.5

Tebuconazole United States 485 8 1.6 0.001 - 0.026 0.1

Mexico 173 15 8.7 0.001 - 0.092 0.1

NOTE: The Limits of Detection (LODs) for pesticide detections in green beans are listed in Appendix B.

Appendix G. Page 4 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Acetamiprid United States 369 28 7.6 0.010 - 0.20 1.5

Chile 148 69 46.6 0.011 - 0.11 1.5

Azoxystrobin United States 369 68 18.4 0.002 - 0.091 2.0

Chile 148 7 4.7 0.003 - 0.045 2.0

Boscalid United States 369 60 16.3 0.014 - 0.43 3.5

Chile 148 0 3.5

Captan United States 369 35 9.5 0.023 - 1.1 15.0

Chile 148 1 0.7 0.078 - 0.078 15.0

Chlorantraniliprole United States 369 37 10 0.020 - 0.053 4.0 IT

Chile 148 16 10.8 0.020 - 0.081 4.0 IT

Clothianidin United States 369 37 10 0.010 - 0.062 0.80

Chile 148 1 0.7 0.012 - 0.012 0.80

Cyfluthrin United States 369 63 17.1 0.006 - 0.13 0.3

Chile 148 0 0.3

Cyhalothrin, Total United States 369 46 12.5 0.008 - 0.076 0.50

Chile 148 44 29.7 0.008 - 0.052 0.50

Cyprodinil United States 369 82 22.2 0.005 - 0.63 2.0

Chile 148 9 6.1 0.005 - 0.017 2.0

Difenoconazole United States 369 56 15.2 0.005 - 0.10 2.5

Chile 148 4 2.7 0.009 - 0.035 2.5

Etoxazole United States 369 58 15.7 0.004 - 0.098 1.0

Chile 148 0 1.0

Fenbuconazole United States 369 58 15.7 0.005 - 0.12 1.0

Chile 148 0 1.0

Fenpropathrin United States 369 53 14.4 0.005 - 0.90 1.4

Chile 148 0 1.4

Fenpyroximate United States 369 37 10 0.010 - 0.072 2.0

Chile 148 0 2.0

2021 Distribution of Residues for Peach Samples

Originating in Chile Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix G. Page 5 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Fludioxonil United States 369 307 83.2 0.007 - 24 5.0

Chile 148 146 98.6 0.005 - 10 5.0

Fluopyram United States 369 85 23 0.010 - 0.25 1.0

Chile 148 4 2.7 0.011 - 0.048 1.0

Imidacloprid United States 369 23 6.2 0.011 - 0.32 3.0

Chile 148 5 3.4 0.016 - 0.036 3.0

Indoxacarb United States 369 16 4.3 0.010 - 0.045 0.90

Chile 148 12 8.1 0.010 - 0.045 0.90

Iprodione United States 369 2 0.5 0.006 - 0.015 20.0 PH

Chile 148 25 16.9 0.005 - 0.044 20.0 PH

Methoxyfenozide United States 369 83 22.5 0.011 - 0.13 3.0

Chile 148 26 17.6 0.010 - 0.042 3.0

Myclobutanil United States 369 19 5.1 0.005 - 0.17 2.0

Chile 148 12 8.1 0.006 - 0.031 2.0

Propiconazole United States 369 162 43.9 0.010 - 4.3 4.0

Chile 148 45 30.4 0.010 - 0.14 4.0

Pyraclostrobin United States 369 100 27.1 0.003 - 0.13 2.5

Chile 148 0 2.5

Pyrimethanil United States 369 25 6.8 0.003 - 0.53 10

Chile 148 58 39.2 0.003 - 18 10

Spinetoram United States 369 34 9.2 0.010 - 0.037 0.30

Chile 148 9 6.1 0.011 - 0.031 0.30

Spinosad United States 359 47 13.1 0.004 - 0.21 0.20

Chile 148 36 24.3 0.004 - 0.14 0.20

Spirodiclofen United States 369 61 16.5 0.010 - 0.18 1.0

Chile 148 63 42.6 0.010 - 0.077 1.0

Tebuconazole United States 369 17 4.6 0.007 - 0.13 2

Chile 148 81 54.7 0.006 - 0.61 2

Trifloxystrobin United States 369 82 22.2 0.005 - 0.16 2

Chile 148 0 2

NOTE: The Limits of Detection (LODs) for pesticide detections in peaches are listed in Appendix B.

Appendix G. Page 6 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Acetamiprid United States 569 118 20.7 0.012 - 0.70 1.0

Argentina 103 45 43.7 0.012 - 0.092 1.0

Bifenazate United States 569 36 6.3 0.008 - 0.046 0.7

Argentina 103 0 0.7

Buprofezin United States 569 113 19.9 0.002 - 0.83 6.0

Argentina 103 10 9.7 0.002 - 0.004 6.0

Carbendazim (MBC) United States 569 202 35.5 0.008 - 0.20 3.0 TP

Argentina 103 14 13.6 0.008 - 0.048 3.0 TP

Chlorantraniliprole United States 569 174 30.6 0.007 - 0.066 1.2

Argentina 103 62 60.2 0.007 - 0.13 1.2

Cyflumetofen United States 569 45 7.9 0.008 - 0.073 0.30

Argentina 103 0 0.30

Diphenylamine (DPA) United States 538 58 10.8 0.005 - 0.069 5.0 PH

Argentina 81 28 34.6 0.005 - 0.074 5.0 PH

Ethoxyquin United States 569 102 17.9 0.020 - 0.92 3

Argentina 103 46 44.7 0.020 - 1.7 3

Etoxazole United States 569 71 12.5 0.002 - 0.047 0.20

Argentina 103 0 0.20

Fenpyroximate United States 569 47 8.3 0.002 - 0.099 0.30

Argentina 103 0 0.30

Fludioxonil United States 569 286 50.3 0.017 - 2.2 5.0

Argentina 103 62 60.2 0.017 - 1.1 5.0

Fluxapyroxad United States 569 82 14.4 0.003 - 0.23 0.8

Argentina 103 0 0.8

Imidacloprid United States 569 62 10.9 0.033 - 0.29 0.6

Argentina 103 0 0.6

Methoxyfenozide United States 569 96 16.9 0.002 - 0.077 2.0

Argentina 103 0 2.0

2021 Distribution of Residues for Pear Samples

Originating in Argentina Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix G. Page 7 of 8
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, 

ppm ^

EPA 

Tolerance, 

ppm

Novaluron United States 569 154 27.1 0.005 - 0.92 3.0

Argentina 103 11 10.7 0.017 - 0.17 3.0

o-Phenylphenol United States 569 36 6.3 0.003 - 6.1 25.0 PH

Argentina 103 1 1 0.003 25.0 PH

Pyraclostrobin United States 569 97 17 0.003 - 0.18 1.5

Argentina 103 1 1 0.032 1.5

Pyrimethanil United States 569 382 67.1 0.003 - 17.9 15

Argentina 103 38 36.9 0.003 - 3.9 15

Spinetoram United States 569 181 31.8 0.005 - 0.059 0.20

Argentina 103 4 3.9 0.005 - 0.005 0.20

Spirodiclofen United States 569 144 25.3 0.007 - 0.16 0.80

Argentina 103 0 0.80

Spirotetramat United States 569 73 12.8 0.003 - 0.034 0.70

Argentina 103 0 0.70

Tetrahydrophthalimide (THPI) United States 569 1 0.2 0.039 25.0 TP

Argentina 103 65 63.1 0.056 - 0.86 25.0 TP

Thiabendazole United States 569 262 46 0.002 - 2.8 10

Argentina 103 49 47.6 0.002 - 1.3 10

Thiophanate methyl United States 569 104 18.3 0.017 - 0.22 3.0

Argentina 103 2 1.9 0.017 3.0

Tolfenpyrad United States 569 177 31.1 0.005 - 0.29 1.0

Argentina 103 0 1.0

NOTE: The Limits of Detection (LODs) for pesticide detections in pears are listed in Appendix B.

^ = Only one distinct detected concentration was reported for the commodity/pesticide/country combination.

EPA Tolerance Codes:

FF = All food/feed commodities tolerance except those covered by a higher tolerance.

FU = Foreign use compound; There are no U.S. registrations.

IT = Interim Tolerance/Temporary or time limited tolerance/Section 18.

PH = Post-harvest application.

TP = Tolerance is from parent compound.

Appendix G. Page 8 of 8
Appendix H 

Pesticide Residues by Commodity

(Pairs With Residue Detections in at Least 5 Percent of Samples)

Appendix H shows 272 commodity/pesticide pairs (including metabolites, isomers, and 

degradates) with detections in at least 5 percent of the samples tested. This appendix excludes 

environmental contaminants, which are listed in Appendix E. The data shown include the range 

and mean of values detected and U.S. Environmental Protection Agency (EPA) tolerance 

references for each pair. The EPA tolerances cited in this summary and appendixes apply to 

2021 and not to the current year. There may be instances where tolerances have been recently 

set, modified, or revoked that would have an effect on whether a residue is violative or not. 
APPENDIX H. PESTICIDE RESIDUES A

 BY COMMODITY

(Pairs With Residue Detections in at Least 5 Percent of Samples)

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

1 Blueberries, Cultivated, Fresh (17 pesticides)

Acetamiprid * I 30.8 692 213 0.002 - 2.0 0.076 1.6

Azoxystrobin F 27.5 692 190 0.002 - 0.72 0.084 10.0

Bifenthrin * I 16.3 692 113 0.002 - 0.71 0.093 3

Boscalid F 41.3 692 286 0.004 - 2.1 0.21 13.0

Cypermethrin * I 23 692 159 0.010 - 0.60 0.093 0.8

Cyprodinil F 30.5 692 211 0.005 - 1.6 0.11 5.0

Difenoconazole F 5.6 692 39 0.010 - 0.77 0.13 4.0

Fenhexamid F 16.5 692 114 0.013 - 1.2 0.18 5

Fludioxonil F 24.1 692 167 0.025 - 3.1 0.25 3.0

Fluopyram F 7.7 692 53 0.005 - 0.43 0.077 7.0

Imidacloprid I 10.4 692 72 0.003 - 0.51 0.028 3.5

Malathion I 9.4 692 65 0.002 - 0.15 0.030 8

Phosmet I 11.3 692 78 0.010 - 1.6 0.16 10

Pyraclostrobin F 18.8 692 130 0.003 - 0.56 0.049 4.0

Spinetoram I 5.3 692 37 0.003 - 0.036 0.010 0.90

Spinosad A * IM 6.1 692 42 0.003 - 0.17 0.023 0.90

Tetrahydrophthalimide (THPI) 1 FM 23.8 692 165 0.010 - 4.0 0.19 20.0 TP

2 Broccoli (10 pesticides)

Azoxystrobin F 10.7 708 76 0.002 - 0.48 0.057 3.0

Boscalid F 7.2 708 51 0.002 - 0.86 0.075 6.0

Cyhalothrin, Total 2 * I 5.5 708 39 0.005 - 0.059 0.017 0.4

DCPA H 33.3 708 236 0.002 - 0.078 0.006 5.0

Fluopyram F 8.3 708 59 0.002 - 0.024 0.004 4.0

Imidacloprid I 16.7 708 118 0.003 - 0.053 0.011 3.5

Permethrin (parent)

 Permethrin cis 3 IM 7.1 708 50 0.002 - 0.13 0.019 2.0

 Permethrin trans 3 IM 6.2 708 44 0.002 - 0.14 0.021 2.0

Pronamide (Propyzamide) H 6.2 708 44 0.002 - 0.008 0.003 NT

Pyraclostrobin F 9 708 64 0.002 - 1.0 0.040 5.0

Thiamethoxam (parent) * I 23.3 708 165 0.003 - 0.045 0.006 4.5

 Clothianidin 4 * I 5.2 708 37 0.006 - 0.031 0.012 4.5 TP

3 Butter (5 pesticides)

Bifenthrin * I 36.7 177 65 0.002 0.002 1.0

Cyhalothrin, Total 2 * I 23.2 177 41 0.006 0.006 10.0

Novaluron * I 42.4 177 75 0.002 - 0.023 0.010 20

Permethrin (parent)

 Permethrin cis 3 IM 40.1 177 71 0.002 - 0.007 0.002 3.0

 Permethrin trans 3 IM 39 177 69 0.002 - 0.008 0.003 3.0

Piperonyl butoxide I 23.7 177 42 0.003 - 0.009 0.003 0.25

Appendix H. Page 1 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

4 Cantaloupe (9 pesticides)

Acetamiprid * I 22.6 328 74 0.002 - 0.025 0.006 0.50

Clothianidin * I 5.8 328 19 0.011 - 0.057 0.024 0.2 TP

Dinotefuran * I 29 328 95 0.003 - 0.082 0.019 0.5

Fluopyram F 13.4 328 44 0.005 - 0.036 0.010 1.0

Imidacloprid I 19.2 328 63 0.003 - 0.060 0.008 0.5

Metalaxyl/Mefenoxam 5 F 21.3 328 70 0.001 - 0.019 0.005 1.0

Oxamyl oxime 6 IM 7.3 328 24 0.008 - 0.15 0.041 2.0

Propamocarb hydrochloride 7 F 21 328 69 0.002 - 0.018 0.005 1.5

Thiabendazole F 14.6 328 48 0.002 - 0.11 0.020 15.0 FU

5 Carrots (7 pesticides)

Azoxystrobin F 5.6 708 40 0.010 - 0.034 0.016 1.0

Boscalid F 18.2 708 129 0.020 - 0.12 0.043 2.0

Iprodione F 9.3 708 66 0.015 - 3.3 0.11 5.0

Linuron H 31.9 708 226 0.010 - 0.29 0.036 1.0

Myclobutanil F 7.2 708 51 0.001 - 0.006 0.003 0.03 IN

Penthiopyrad F 5.1 708 36 0.001 - 0.067 0.007 3.0

Pyraclostrobin F 10.2 708 72 0.005 - 0.046 0.008 0.4

6 Cauliflower (3 pesticides)

Flupyradifurone I 16.8 531 89 0.002 - 0.11 0.005 6

Imidacloprid I 18.1 531 96 0.003 - 1.1 0.019 3.5

Thiamethoxam * I 23.5 531 125 0.003 - 0.080 0.005 4.5

7 Celery (14 pesticides)

Acephate * I 7.3 354 26 0.056 - 1.2 0.23 10

Azoxystrobin F 19.8 354 70 0.002 - 0.14 0.025 30.0

Bifenthrin * I 6.5 354 23 0.005 - 0.16 0.033 3.0

Boscalid F 7.1 354 25 0.010 - 0.24 0.042 45

Carbaryl I 6.2 354 22 0.012 - 0.44 0.08 3.0

Chlorantraniliprole I 6.8 354 24 0.021 - 0.16 0.044 13

Chlorothalonil F 26.3 354 93 0.005 - 0.86 0.10 15

Dicloran F 6.8 354 24 0.006 - 0.44 0.095 15

Malathion I 14.4 354 51 0.011 - 0.18 0.052 8

Methomyl I 5.1 354 18 0.010 - 0.082 0.030 3

Penthiopyrad F 5.1 354 18 0.010 - 0.14 0.046 30

Permethrin Total I 48.3 354 171 0.005 - 0.27 0.045 5

Propiconazole F 30.5 354 108 0.010 - 0.14 0.023 5

Pyraclostrobin F 11.3 354 40 0.003 - 0.075 0.023 29

8 Corn Grain (1 pesticide)

Glyphosate H 34.9 418 146 0.050 - 0.14 0.052 5.0

9 Eggplant (10 pesticides)

Acetamiprid * I 14.5 703 102 0.002 - 0.14 0.019 0.20

Bifenthrin * I 6.3 703 44 0.002 - 0.041 0.010 0.5

Appendix H. Page 2 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

Difenoconazole F 7.3 703 51 0.002 - 0.033 0.009 0.60

Dinotefuran * I 11 703 77 0.010 - 0.16 0.033 0.7

Fenpyroximate A 5.4 703 38 0.003 - 0.022 0.007 0.20

Fluopyram F 25.6 703 180 0.002 - 0.27 0.019 4.0

Flupyradifurone I 9.1 703 64 0.002 - 0.18 0.031 1.5

Imidacloprid I 21.2 703 149 0.002 - 0.13 0.016 1.0

Permethrin cis 3 IM 5 703 35 0.002 - 0.12 0.020 0.50

Thiamethoxam (parent) * I 23.9 703 168 0.003 - 0.19 0.014 0.25

 Clothianidin 4

 * I 7.8 703 55 0.003 - 0.049 0.011 0.25 TP

10 Grape Juice (9 pesticides)

Azoxystrobin F 36 700 252 0.002 - 0.005 0.002 2.0

Boscalid F 6.6 700 46 0.008 - 0.11 0.015 5.0

Carbaryl I 10.1 700 71 0.008 - 0.048 0.017 10

Fluopyram F 44 700 308 0.002 - 0.007 0.002 2.0

Flutriafol F 11.9 700 83 0.003 - 0.028 0.006 1.5

Mandipropamid F 7.3 700 51 0.003 - 0.010 0.003 1.4

Methoxyfenozide I 68.4 700 479 0.002 - 0.031 0.008 1.0

Tebuconazole F 22.1 700 155 0.003 0.003 6

Tetrahydrophthalimide (THPI) 1 FM 6.6 700 46 0.017 - 0.29 0.049 25.0 TP

11 Green Beans (18 pesticides)

Acephate (parent) * I 6.3 700 44 0.006 - 10 0.86 0.02 FF

 Methamidophos 8 * I 6.9 700 48 0.001 - 1.9 0.19 0.02 TP

Azoxystrobin F 28 700 196 0.001 - 0.58 0.029 3.0

Bifenthrin * I 25.7 700 180 0.001 - 0.15 0.030 0.6

Boscalid F 11 700 77 0.003 - 0.23 0.043 5.0

Carbendazim (MBC) 9 F 33.4 700 234 0.001 - 0.26 0.033 2.0 TP

Chlorantraniliprole I 6.6 700 46 0.005 - 0.048 0.014 2.0

Chlorothalonil F 15.1 700 106 0.005 - 0.73 0.051 5

Cyhalothrin, Total 2 * I 16 700 112 0.003 - 0.056 0.012 0.20

Cypermethrin * I 15.6 700 109 0.005 - 0.19 0.04 0.7

Dicloran F 9 700 63 0.001 - 2.2 0.093 20

Imidacloprid desnitro 10 IM 8.2 679 56 0.001 - 0.023 0.005 4.0

Metalaxyl/Mefenoxam 5 F 6.4 700 45 0.001 - 0.023 0.006 0.2

Myclobutanil F 7.1 700 50 0.003 - 0.096 0.028 1.0

Novaluron * I 6.7 700 47 0.003 - 0.11 0.023 0.70

Omethoate 11 IM 5.1 700 36 0.001 - 0.086 0.017 2.0 TP

Penthiopyrad F 7 700 49 0.001 - 0.11 0.025 4.0

Pyraclostrobin F 20.4 700 143 0.001 - 0.20 0.017 0.5

Tebuconazole F 5 700 35 0.001 - 0.092 0.011 0.1

12 Peaches, Fresh (29 pesticides)

Acetamiprid * I 18.7 518 97 0.010 - 0.20 0.038 1.5

Azoxystrobin F 14.5 518 75 0.002 - 0.091 0.021 2.0

Boscalid F 11.6 518 60 0.014 - 0.43 0.073 3.5

Captan F 6.9 518 36 0.023 - 1.1 0.20 15.0

Appendix H. Page 3 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

Chlorantraniliprole I 10.2 518 53 0.020 - 0.081 0.030 4.0 IT

Clothianidin * I 7.3 518 38 0.010 - 0.062 0.027 0.80

Cyfluthrin * I 12.2 518 63 0.006 - 0.13 0.033 0.3

Cyhalothrin, Total 2

 * I 17.4 518 90 0.008 - 0.076 0.024 0.50

Cyprodinil F 17.6 518 91 0.005 - 0.63 0.088 2.0

Difenoconazole F 11.6 518 60 0.005 - 0.10 0.028 2.5

Etoxazole A 11.2 518 58 0.004 - 0.098 0.023 1.0

Fenbuconazole F 11.2 518 58 0.005 - 0.12 0.029 1.0

Fenpropathrin I 10.4 518 54 0.005 - 0.90 0.19 1.4

Fenpyroximate A 7.1 518 37 0.010 - 0.072 0.025 2.0

Fludioxonil F 87.6 518 454 0.005 - 24 1.2 5.0

Fluopyram F 17.2 518 89 0.010 - 0.25 0.059 1.0

Imidacloprid I 5.4 518 28 0.011 - 0.32 0.056 3.0

Indoxacarb I 5.4 518 28 0.010 - 0.045 0.019 0.90

Iprodione F 5.2 518 27 0.005 - 0.044 0.014 20.0 PH

Methoxyfenozide I 21 518 109 0.010 - 0.13 0.037 3.0

Myclobutanil F 6 518 31 0.005 - 0.17 0.022 2.0

Propiconazole F 40.2 518 208 0.010 - 4.3 0.23 4.0

Pyraclostrobin F 19.3 518 100 0.003 - 0.13 0.045 2.5

Pyrimethanil F 16 518 83 0.003 - 18 0.81 10

Spinetoram I 8.3 518 43 0.010 - 0.037 0.018 0.30

Spinosad * I 16.3 508 83 0.004 - 0.21 0.024 0.20

Spirodiclofen A 24.1 518 125 0.010 - 0.18 0.034 1.0

Tebuconazole F 18.9 518 98 0.006 - 0.61 0.071 2

Trifloxystrobin F 15.8 518 82 0.005 - 0.16 0.037 2

13 Peaches, Frozen (5 pesticides)

Cyprodinil F 20.1 154 31 0.005 - 0.054 0.024 2.0

Fludioxonil F 14.9 154 23 0.011 - 0.18 0.064 5.0

Fluopyram F 6.5 154 10 0.010 - 0.026 0.014 1.0

Propiconazole F 7.8 154 12 0.010 - 0.051 0.029 4.0

Tebuconazole F 7.1 154 11 0.005 - 0.043 0.013 2

14 Pears (25 pesticides)

Acetamiprid * I 25.2 707 178 0.012 - 0.70 0.082 1.0

Bifenazate A 5.2 707 37 0.008 - 0.046 0.015 0.7

Buprofezin I 17.7 707 125 0.002 - 0.83 0.077 6.0

Chlorantraniliprole I 36.2 707 256 0.007 - 0.13 0.018 1.2

Cyflumetofen A 6.4 707 45 0.008 - 0.073 0.014 0.30

Diphenylamine (DPA) F 13.3 648 86 0.005 - 0.074 0.012 5.0 PH

Ethoxyquin P 21.2 707 150 0.020 - 1.7 0.19 3

Etoxazole A 10.3 707 73 0.002 - 0.047 0.009 0.20

Fenpyroximate A 6.6 707 47 0.002 - 0.10 0.025 0.30

Fludioxonil F 52.6 707 372 0.017 - 2.3 0.54 5.0

Fluopyram F 5 707 35 0.002 - 0.068 0.004 0.80

Fluxapyroxad F 11.9 707 84 0.003 - 0.23 0.034 0.8

Appendix H. Page 4 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

Imidacloprid I 8.9 707 63 0.033 - 0.29 0.067 0.6

Methoxyfenozide I 14.9 707 105 0.002 - 0.077 0.006 2.0

Novaluron * I 23.5 707 166 0.005 - 0.92 0.044 3.0

o-Phenylphenol F 5.8 707 41 0.003 - 6.1 0.25 25.0 PH

Pyraclostrobin F 14.1 707 100 0.003 - 0.18 0.032 1.5

Pyrimethanil F 63.6 707 450 0.003 - 17.9 0.90 15

Spinetoram I 26.3 707 186 0.005 - 0.059 0.013 0.20

Spirodiclofen A 21.1 707 149 0.007 - 0.16 0.019 0.80

Spirotetramat I 10.6 707 75 0.003 - 0.034 0.005 0.70

Tetrahydrophthalimide (THPI) 1 FM 9.5 707 67 0.038 - 0.86 0.39 25.0 TP

Thiabendazole F 45.5 707 322 0.002 - 2.8 0.33 10

Thiophanate methyl (parent) F 15.1 707 107 0.017 - 0.22 0.031 3.0

 Carbendazim (MBC) 9 F 30.7 707 217 0.008 - 0.20 0.032 3.0 TP

Tolfenpyrad I 25.3 707 179 0.005 - 0.29 0.039 1.0

15 Plums (8 pesticides)

Cyprodinil F 5.1 277 14 0.009 - 0.16 0.072 2.0

Fludioxonil F 85.2 277 236 0.025 - 1.2 0.28 5.0

Fluopyram F 14.8 277 41 0.006 - 0.060 0.021 0.50

Hexythiazox I 10.9 247 27 0.002 - 0.013 0.005 1.0

Methoxyfenozide I 43.3 277 120 0.003 - 0.12 0.027 0.30

Propiconazole F 14.4 277 40 0.010 - 0.23 0.080 0.60

Spirotetramat I 22.7 277 63 0.002 - 0.025 0.005 4.5

Trifloxystrobin F 15.5 277 43 0.002 - 0.032 0.007 2

16 Summer Squash (13 pesticides)

Acetamiprid * I 5.6 698 39 0.002 - 0.035 0.008 0.50

Azoxystrobin F 5.7 698 40 0.001 - 0.026 0.004 0.3

Bifenthrin * I 5.2 698 36 0.002 - 0.033 0.008 0.4

Chlorothalonil F 7.4 365 27 0.005 - 0.16 0.039 5.0

Cyflufenamid F 6 698 42 0.001 - 0.038 0.011 0.10

Fluopyram F 8 698 56 0.001 - 0.17 0.014 0.60

Flupyradifurone I 5.7 698 40 0.001 - 0.12 0.017 0.40

Flutriafol F 9 698 63 0.001 - 0.045 0.007 0.30

Imidacloprid (parent) I 36.2 698 253 0.003 - 0.36 0.030 0.5

 Imidacloprid desnitro 10 IM 36.1 327 118 0.001 - 0.006 0.002 0.5

 Imidacloprid urea 10 IM 9.6 365 35 0.001 - 0.016 0.003 0.5

Metalaxyl/Mefenoxam 5 F 6.2 698 43 0.001 - 0.33 0.029 1.0

Propamocarb (parent) F 5.2 365 19 0.001 - 0.41 0.036 1.5

 Propamocarb hydrochloride 7 F 7.5 333 25 0.001 - 0.16 0.028 1.5

Pyraclostrobin F 9.6 698 67 0.001 - 0.033 0.008 0.5

Thiamethoxam * I 22.1 698 154 0.001 - 0.15 0.021 0.2

17 Sweet Bell Peppers (29 pesticides)

Acetamiprid * I 15.4 319 49 0.011 - 0.12 0.025 0.20

Azoxystrobin F 16.9 319 54 0.002 - 0.10 0.019 3.0

Appendix H. Page 5 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

Bifenthrin * I 11.9 328 39 0.005 - 0.12 0.026 0.5

Boscalid F 9.7 319 31 0.012 - 0.22 0.060 3.0

Chlorfenapyr * I 13.7 328 45 0.005 - 0.16 0.038 2

Chlorothalonil F 8.2 328 27 0.006 - 0.10 0.025 6.0

Chlorpyrifos * I 5.8 328 19 0.006 - 0.22 0.055 1.0

Cyfluthrin * I 5.8 328 19 0.005 - 0.044 0.015 0.50

Cyhalothrin, Total 2 * I 7.3 328 24 0.008 - 0.11 0.025 0.20

Cypermethrin * I 21 328 69 0.010 - 0.14 0.033 0.2

Difenoconazole F 11.9 319 38 0.006 - 0.085 0.028 0.60

Dinotefuran * I 13.2 319 42 0.010 - 0.62 0.073 0.7

Fenpropathrin I 8.2 328 27 0.007 - 0.32 0.064 1.0

Flonicamid I 13.5 319 43 0.011 - 0.53 0.065 3.0

Fluopyram F 27.6 319 88 0.011 - 0.19 0.036 4.0

Imidacloprid I 26.6 319 85 0.010 - 0.45 0.047 1.0

Metalaxyl/Mefenoxam 5 F 12.5 328 41 0.006 - 0.21 0.035 1.0

Methomyl I 5 319 16 0.013 - 0.92 0.13 2

Methoxyfenozide I 5 319 16 0.010 - 0.076 0.038 2.0

Myclobutanil F 7 328 23 0.006 - 0.062 0.022 4.0

Novaluron * I 5.3 319 17 0.011 - 0.046 0.025 2

Oxamyl (parent) I 6.9 319 22 0.012 - 0.18 0.050 2.0

 Oxamyl oxime 6 IM 25.4 319 81 0.010 - 0.46 0.086 2.0

Penthiopyrad F 7.2 319 23 0.010 - 0.20 0.034 3.0

Propamocarb F 6.9 319 22 0.010 - 0.64 0.099 4

Pyraclostrobin F 20.4 319 65 0.003 - 0.12 0.030 1.4

Pyriproxyfen * I 8.2 328 27 0.005 - 0.051 0.019 0.80

Spiromesifen I 14.4 319 46 0.002 - 0.12 0.021 0.45

Thiacloprid I 6.3 319 20 0.010 - 0.080 0.026 1.0 FU

Thiamethoxam (parent) * I 22.3 319 71 0.010 - 0.095 0.027 0.25

 Clothianidin 4 * I 24.8 319 79 0.010 - 0.15 0.033 0.80

18 Tangerines (7 pesticides)

Acetamiprid * I 10.2 531 54 0.002 - 0.061 0.010 1.0

Azoxystrobin F 30.3 531 161 0.002 - 0.24 0.026 15.0

Fludioxonil F 36.9 531 196 0.005 - 0.26 0.025 10

Imazalil F 94.9 531 504 0.006 - 1.1 0.19 10.0 PH

Propiconazole F 15.8 531 84 0.005 - 0.13 0.021 8.0

Pyrimethanil F 19.2 531 102 0.005 - 0.52 0.072 10

Thiabendazole F 75.5 531 401 0.010 - 2.5 0.21 10

19 Watermelon (4 pesticides)

Etoxazole A 10.7 28 3 0.002 - 0.074 0.028 0.20

Fluopyram F 5.7 175 10 0.002 - 0.012 0.004 1.0

Imidacloprid I 17.1 175 30 0.010 - 0.12 0.023 0.5

Methomyl I 5.7 175 10 0.005 - 0.039 0.014 0.2

Appendix H. Page 6 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ^ ppm ppm

20 Winter Squash (14 pesticides)

Acetamiprid * I 11.2 706 79 0.001 - 0.010 0.003 0.50

Bifenthrin * I 19.8 706 140 0.001 - 0.14 0.007 0.4

Chlorothalonil F 12 706 85 0.005 - 0.43 0.048 5.0

Chlorpropham H 5.8 706 41 0.001 - 0.018 0.004 NT

Cyflufenamid F 12.2 706 86 0.001 - 0.051 0.009 0.10

Flubendiamide I 5.2 706 37 0.001 - 0.027 0.006 0.20

Flupyradifurone I 5.8 706 41 0.001 - 0.085 0.010 0.40

Flutriafol F 5.2 706 37 0.001 - 0.032 0.007 0.30

Imidacloprid (parent) I 35.8 706 253 0.003 - 0.21 0.017 0.5

 Imidacloprid desnitro 10 IM 42.4 706 299 0.001 - 0.018 0.003 0.5

Propamocarb F 7.8 706 55 0.002 - 0.34 0.054 1.5

Pydiflumetofen F 5.9 706 42 0.001 - 0.18 0.028 0.50

Pyraclostrobin F 5.4 706 38 0.001 - 0.006 0.003 0.5

Tebuconazole F 5.8 706 41 0.001 - 0.023 0.004 0.4

Thiamethoxam * I 14.6 706 103 0.001 - 0.030 0.004 0.2

NOTES

A Excludes environmental contaminants, which are listed in Appendix E.

^ When a range is not listed, only one distinct detected concentration was reported for the pesticide/commodity pair.

* Residue may result from food handling establishment (FHE) application.

1 Metabolite of captafol and captan.

2 Includes cyhalothrin lambda plus R157836 epimer.

3 Isomer of parent, permethrin.

4 Metabolite of parent, thiamethoxam.

5 Metalaxyl/mefenoxam are spatial isomers which are analytically indistinguishable via multiresidue methods, but have

separate registrations.

6 Metabolite of parent, oxamyl. 

7 Propamocarb analytically determined as the salt (hydrochloride).

8 Metabolite of parent, acephate.

9 Metabolite of benomyl and thiophanate methyl.

10 Metabolite of parent, imidacloprid. 

11 Metabolite of parent, dimethoate. 

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

P = Plant Growth Regulator

EPA Tolerance Codes:

FF = All food/feed commodities tolerance except those covered by a higher tolerance.

FU = Foreign use compound. There are no U.S. registrations.

IN = Inadvertent/negligible residue tolerance.

NT = No tolerance established.

PH = Post-harvest application.

TP = Tolerance is from parent compound.

Appendix H. Page 7 of 7
Appendix I 

Number of Pesticides Detected per Sample

Appendix I shows the percentage of samples versus the number of pesticides detected per 

sample. This appendix excludes environmental contaminants, which are listed in Appendix E

The graph and data on page 1 show the overall number of samples and percentages (of total

number of samples analyzed) for each detection group across all commodities. The table on 

page 2 shows the number of pesticides detected by individual commodity. For the 10,127

samples analyzed, 24.0 percent of the samples had no detectable pesticides, 18.5 percent had 

1 pesticide, and 57.5 percent of the samples had more than 1 pesticide. 

This appendix reports the number of distinct pesticides rather than residues. A parent 

compound and its metabolites are reported as a single pesticide.
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19

# of

Samples 2,433 1,877 1,697 1,374 947 596 415 272 188 130 67 53 24 20 12 14 5 0 1 2

% of Total

Samples 24.0 18.5 16.8 13.6 9.4 5.9 4.1 2.7 1.9 1.3 0.7 0.5 0.2 0.2 0.1 0.1 0.05 - 0.01 0.02

TOTAL NUMBER OF SAMPLES = 10,127

NOTES

1

 Environmental contaminants, listed in Appendix E, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues."

APPENDIX I. NUMBER OF PESTICIDES 1

 DETECTED PER SAMPLE

30

Number of Pesticides Detected per Sample

Number of Pesticides Detected per Sample

20

10

Percent of Samples

18.5

5.9

9.4

13.6

Multiple pesticide detections may result from the application of more than one pesticide, 

spray drift, crop rotation, and/or cross-contamination.

24.0

16.8

4.1

2.7

1.9

1.3 0.7 0.5 0.2 0.2 0.1 0.1 0.05 0.01 0.02

Appendix I. Page 1 of 2
Commodity (# of samples) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19

Fresh Fruit and Vegetables: Percent

Blueberries, Cultivated (692) 16.0 13.6 12.0 12.3 12.7 9.0 8.8 6.5 3.9 3.0 1.0 0.4 0.3 0.1 0.1 0.1 -- -- -- --

Broccoli (708) 21.0 24.6 24.4 15.3 7.8 4.1 1.8 0.1 0.6 -- 0.1 -- 0.1 -- -- -- -- -- -- --

Cantaloupe (328) 19.5 28.7 25.3 17.1 5.8 2.1 1.5 -- -- -- -- -- -- -- -- -- -- -- -- --

Carrots (708) 46.0 28.0 11.7 8.1 4.5 1.3 0.3 0.1 -- -- -- -- -- -- -- -- -- -- -- --

Cauliflower (531) 41.2 36.9 16.4 3.8 1.1 0.4 -- 0.2 -- -- -- -- -- -- -- -- -- -- -- --

Celery (354) 16.4 16.4 21.2 22.3 13.0 4.8 4.2 0.6 0.8 0.3 -- -- -- -- -- -- -- -- -- --

Eggplant (703) 26.5 23.6 17.6 14.1 7.5 5.0 2.8 1.6 0.6 0.4 0.3 -- -- -- -- -- -- -- -- --

Green Beans (700) 15.7 15.1 16.7 16.1 12.4 7.9 5.1 4.7 2.4 1.6 0.9 0.7 0.1 0.3 -- -- 0.1 -- -- --

Peaches (518) 2.3 8.9 11.0 13.7 16.2 12.4 9.7 6.6 4.8 3.1 2.5 2.1 1.9 1.9 0.8 1.5 0.2 -- 0.2 0.2

Pears (707) 5.2 8.9 7.4 8.8 10.9 9.8 13.0 10.5 8.6 7.1 3.7 3.7 0.7 0.8 0.7 0.1 0.1 -- -- --

Plums (277) 11.6 24.2 23.5 17.7 8.7 11.2 2.5 -- 0.7 -- -- -- -- -- -- -- -- -- -- --

Summer Squash (698) 31.1 19.5 17.0 11.6 8.7 5.0 3.0 2.0 1.3 0.6 0.1 -- -- -- -- -- -- -- -- --

Sweet Bell Peppers (328) 10.4 14.0 12.2 12.2 12.2 8.2 9.5 7.6 4.0 3.4 2.1 1.8 0.9 -- 0.3 0.6 0.6 -- -- --

Tangerines (531) 2.6 5.8 33.0 31.3 16.9 8.3 1.5 0.6 -- -- -- -- -- -- -- -- -- -- -- --

Watermelon (175) 50.9 32.0 10.9 5.7 0.6 -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Winter Squash (706) 17.8 15.3 22.1 17.3 8.4 6.7 4.7 2.8 2.0 1.6 0.4 0.1 0.1 0.1 0.1 0.3 -- -- -- 0.1

Processed Fruit and Vegetables:

Blueberries, Frozen (14) 14.3 7.1 7.1 14.3 -- 7.1 7.1 -- 7.1 14.3 7.1 7.1 7.1 -- -- -- -- -- -- --

Grape Juice (700) 29.0 8.4 19.9 16.6 15.0 6.3 2.7 1.0 1.1 -- -- -- -- -- -- -- -- -- -- --

Peaches, Frozen (154) 68.8 14.3 5.8 8.4 1.9 0.6 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Percent of Total Samples 22.0 18.1 17.4 14.2 9.8 6.1 4.3 2.8 2.0 1.4 0.7 0.6 0.3 0.2 0.2 0.2 0.05 -- 0.01 0.02

Actual Number of Samples 2,095 1,721 1,657 1,349 930 579 414 271 188 130 67 53 24 20 12 14 5 -- 1 2

Grain Product: 

Corn Grain (418) 63.6 34.0 2.4 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 266 142 10 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Dairy Product: 

Butter (177) 40.7 7.9 16.9 14.1 9.6 9.6 0.6 0.6 -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 72 14 30 25 17 17 1 1 -- -- -- -- -- -- -- -- -- -- -- --

NOTES

1

 Environmental contaminants, listed in Appendix E, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues." 

Number of Pesticides 1

 Detected per Sample

APPENDIX I. NUMBER OF PESTICIDES DETECTED PER SAMPLE

TOTAL NUMBER OF FRUIT & VEGETABLE SAMPLES = 9,532

Appendix I. Page 2 of 2
Appendix J

Samples Reported to the

U.S. Food and Drug Administration as

Exceeding the Tolerance

or Without Established Tolerance

(per Code of Federal Regulations, Title 40, Part 180)

Appendix J shows pesticide residues reported to the U.S. Food and Drug Administration (FDA) 

as exceeding the tolerance or residues for which no established tolerance was listed under the 

Code of Federal Regulations, Title 40, Part 180. In 2021, a total of 423 samples with 466

pesticides were reported to the FDA as Presumptive Tolerance Violations.

Pesticides exceeding the tolerance were detected in 54 samples, including 4 samples of fresh 

blueberries, 1 sample of broccoli, 2 samples of celery, 3 samples of eggplant, 31 samples of 

green beans, 5 samples of peaches, 1 sample of pears, and 7 samples of winter squash. Of 

those 54 samples, 24 were reported as imported produce. One green bean sample contained 3 

pesticides that exceeded the established tolerances. Five green bean samples and 2 peach 

samples contained 2 pesticides each that exceeded the established tolerances. 

In addition, 374 samples were found to have pesticides for which no tolerance was established, 

including 373 fresh fruit and vegetable samples and 1 butter sample. 

o 349 samples contained 1 pesticide for which no tolerance was established.

o 23 samples contained 2 pesticides for which no tolerances were established.

o 1 sample contained 3 pesticides for which no tolerances were established.

o 1 sample contained 5 pesticides for which no tolerances were established.

 

Five of the 374 samples also contained one or more pesticides that exceeded an established 

tolerance. 

The columns under the Sample Origin heading provide the number of samples that were of 

domestic, imported, or unknown origin for each pesticide/commodity pair listed.

Appendix J also notes if metabolites (or isomers) were detected as part of the same sample. In 

instances where both parent and metabolite (or isomer) were detected, the Pesticide Data 

Program (PDP) accounted for both as part of the same tolerance expression.

The Environmental Protection Agency (EPA) tolerances cited in this summary and appendixes 

apply to 2021 and not to the current year. There may be instances where tolerances have been 

recently set, modified, or revoked that would have an effect on whether a residue is violative or 

not. 

A number of the findings shown in this appendix are less than 0.01 ppm. Levels below 0.01 

ppm are deemed by the U.S. FDA to be “not of regulatory significance”.
Residues Exceeding Established Tolerance

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm Country of Origin

1 Blueberries, Cultivated, Fresh / Acetamiprid 0.002 2 1.6 Peru

2 Blueberries, Cultivated, Fresh / Acetamiprid 0.002 1.9 1.6 Peru

3 Blueberries, Cultivated, Fresh / Chlorfenapyr 0.015 0.041 0.01 FF Mexico

4 Blueberries, Cultivated, Fresh / Fludioxonil 0.025 3.1 3.0 Chile

5 Broccoli / Cypermethrin 0.022 2.5 2.0 Mexico

6 Celery / Cyhalothrin, Total 1 0.008 0.037 0.01 FF U.S.

7 Celery / Novaluron 0.01 0.063 0.01 FF Canada

8 Eggplant / Acephate 2 0.075 0.32 0.02 FF U.S.

9 Eggplant / Acephate 2 0.075 0.18 0.02 FF U.S.

10 Eggplant / Acephate 2 0.075 0.084 0.02 FF U.S.

11 Green Beans / Acephate 2, 3 0.005 10 0.02 FF U.S.

12 Green Beans / Acephate 2, 4 0.005 7.5 0.02 FF U.S.

13 Green Beans / Acephate 2, 5 0.005 5.2 0.02 FF U.S.

14 Green Beans / Acephate 2, 6 0.005 4.7 0.02 FF U.S.

15 Green Beans / Acephate 2, 7 0.005 3.9 0.02 FF U.S.

16 Green Beans / Acephate 2, 8 0.005 1.2 0.02 FF U.S.

17 Green Beans / Acephate 2, 9 0.005 0.77 0.02 FF U.S.

18 Green Beans / Acephate 2, 10 0.005 0.73 0.02 FF Mexico

19 Green Beans / Acephate 2, 11 0.005 0.6 0.02 FF U.S.

20 Green Beans / Acephate 2, 12 0.005 0.44 0.02 FF U.S.

21 Green Beans / Acephate 2, 13 0.005 0.41 0.02 FF U.S.

22 Green Beans / Acephate 2, 14 0.005 0.34 0.02 FF Mexico

23 Green Beans / Acephate 2, 15 0.005 0.32 0.02 FF U.S.

24 Green Beans / Acephate 2, 16 0.005 0.19 0.02 FF Mexico

25 Green Beans / Acephate 2, 17 0.005 0.18 0.02 FF Mexico

26 Green Beans / Acephate 2, 18 0.005 0.14 0.02 FF Mexico

27 Green Beans / Acephate 2, 19 0.005 0.11 0.02 FF U.S.

28 Green Beans / Acephate 2, 20 0.005 0.098 0.02 FF Mexico

29 Green Beans / Acephate 2, 21 0.005 0.084 0.02 FF Mexico

30 Green Beans / Acephate 2, 22 0.005 0.082 0.02 FF U.S.

31 Green Beans / Acephate 2, 23 0.005 0.078 0.02 FF U.S.

APPENDIX J. SAMPLES REPORTED TO FDA AS EXCEEDING THE TOLERANCE

OR WITHOUT ESTABLISHED TOLERANCE

(per Code of Federal Regulations, Title 40, Part 180)

Appendix J. Page 1 of 7
Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm Country of Origin

32 Green Beans / Acephate 2, 24 0.005 0.075 0.02 FF Mexico

33 Green Beans / Acephate 2, 25 0.005 0.075 0.02 FF U.S.

34 Green Beans / Acephate 2, 26 0.005 0.067 0.02 FF U.S.

35 Green Beans / Acephate 2, 27 0.005 0.05 0.02 FF Mexico

36 Green Beans / Acephate 2, 28 0.005 0.045 0.02 FF Unknown

37 Green Beans / Acephate 2, 29 0.005 0.044 0.02 FF U.S.

38 Green Beans / Acephate 2 0.005 0.036 0.02 FF Mexico

39 Green Beans / Buprofezin 2, 4 0.001 0.074 0.02 U.S.

40 Green Beans / Buprofezin 2, 10 0.001 0.063 0.02 Mexico

41 Green Beans / Buprofezin 2, 3 0.001 0.055 0.02 U.S.

42 Green Beans / Clothianidin 30, 31 0.001 0.14 0.02 TP Mexico

43 Green Beans / Clothianidin 30 0.001 0.031 0.02 TP Mexico

44 Green Beans / Dinotefuran 2, 23 0.003 0.049 0.01 FF U.S.

45 Green Beans / Dinotefuran 2, 7 0.003 0.04 0.01 FF U.S.

46 Green Beans / Dinotefuran 2, 5 0.003 0.031 0.01 FF U.S.

47 Green Beans / Dinotefuran 2, 4 0.003 0.03 0.01 FF U.S.

48 Green Beans / Methamidophos 2, 3 0.001 1.9 0.02 TP U.S.

49 Green Beans / Methamidophos 2, 4 0.001 1.5 0.02 TP U.S.

50 Green Beans / Methamidophos 2, 6 0.001 1.1 0.02 TP U.S.

51 Green Beans / Methamidophos 2, 5 0.001 1 0.02 TP U.S.

52 Green Beans / Methamidophos 2, 7 0.001 0.9 0.02 TP U.S.

53 Green Beans / Methamidophos 2, 8 0.001 0.4 0.02 TP U.S.

54 Green Beans / Methamidophos 2, 11 0.001 0.35 0.02 TP U.S.

55 Green Beans / Methamidophos 2, 10 0.001 0.33 0.02 TP Mexico

56 Green Beans / Methamidophos 2, 9 0.001 0.23 0.02 TP U.S.

57 Green Beans / Methamidophos 2, 12 0.001 0.17 0.02 TP U.S.

58 Green Beans / Methamidophos 2, 13 0.001 0.17 0.02 TP U.S.

59 Green Beans / Methamidophos 2, 15 0.001 0.15 0.02 TP U.S.

60 Green Beans / Methamidophos 2, 14 0.001 0.14 0.02 TP Mexico

61 Green Beans / Methamidophos 2, 16 0.001 0.072 0.02 TP Mexico

62 Green Beans / Methamidophos 2, 19 0.001 0.072 0.02 TP U.S.

63 Green Beans / Methamidophos 2, 17 0.001 0.068 0.02 TP Mexico

64 Green Beans / Methamidophos 2, 18 0.001 0.064 0.02 TP Mexico

65 Green Beans / Methamidophos 2, 22 0.001 0.052 0.02 TP U.S.

66 Green Beans / Methamidophos 2, 24 0.001 0.051 0.02 TP Mexico

Appendix J. Page 2 of 7
Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm Country of Origin

67 Green Beans / Methamidophos 2, 20 0.001 0.048 0.02 TP Mexico

68 Green Beans / Methamidophos 2, 21 0.001 0.047 0.02 TP Mexico

69 Green Beans / Methamidophos 2, 26 0.001 0.045 0.02 TP U.S.

70 Green Beans / Methamidophos 2, 25 0.001 0.041 0.02 TP U.S.

71 Green Beans / Methamidophos 2, 27 0.001 0.033 0.02 TP Mexico

72 Green Beans / Methamidophos 2, 29 0.001 0.032 0.02 TP U.S.

73 Green Beans / Methamidophos 2, 28 0.001 0.03 0.02 TP Unknown

74 Green Beans / Tetrahydrophthalimide (THPI) 32 0.005 0.084 0.05 TP Mexico

75 Green Beans / Thiamethoxam 31 0.001 0.071 0.02 Mexico

76 Peaches / Fludioxonil 0.005 24 5.0 U.S.

77 Peaches / Fludioxonil 33 0.005 10 5.0 Chile

78 Peaches / Fludioxonil 34 0.005 9 5.0 Chile

79 Peaches / Propiconazole 0.01 4.3 4.0 U.S.

80 Peaches / Pyrimethanil 33 0.003 18 10 Chile

81 Peaches / Pyrimethanil 34 0.003 14 10 Chile

82 Peaches / Spinosad 0.004 0.21 0.20 U.S.

83 Pears / Pyrimethanil 0.002 17.9 15 U.S.

84 Winter Squash / Acephate 2, 35 0.005 0.3 0.02 FF U.S.

85 Winter Squash / Acephate 2, 36 0.005 0.16 0.02 FF U.S.

86 Winter Squash / Acephate 2 0.005 0.071 0.02 FF U.S.

87 Winter Squash / Acephate 2 0.005 0.03 0.02 FF U.S.

88 Winter Squash / Chlorfenapyr 0.01 0.084 0.01 FF Honduras

89 Winter Squash / Chlorfenapyr 0.01 0.064 0.01 FF Honduras

90 Winter Squash / Chlorfenapyr 0.01 0.034 0.01 FF Honduras

91 Winter Squash / Methamidophos 2, 35 0.001 0.073 0.02 TP U.S.

92 Winter Squash / Methamidophos 2, 36 0.001 0.04 0.02 TP U.S.

EPA Tolerance Codes:

FF = All food/feed commodities tolerance except those covered by a higher tolerance.

TP = Tolerance is from parent compound.

Appendix J. Page 3 of 7
Commodity / Pesticide U.S. Import Unk.

1 Blueberries, Cultivated, Fresh (7 pesticides)

Carbendazim (MBC) 37 692 9 1.3 0.001 - 0.018 0.001 1 8 0

Diflubenzuron 692 1 0.1 0.003 0.002 1 0 0

Fenpropimorph 692 2 0.3 0.003 - 0.004 0.001 0 2 0

Fluvalinate 692 1 0.1 0.051 0.050 1 0 0

Myclobutanil 692 1 0.1 0.086 0.003 0 1 0

Tebuconazole 692 1 0.1 0.098 0.010 0 1 0

Thiacloprid 692 1 0.1 0.061 0.001 0 1 0

2 Broccoli (17 pesticides)

Atrazine 708 1 0.1 0.002 0.001 - 0.003 0 1 0

Carbendazim (MBC) 37 708 3 0.4 0.004 - 0.014 0.003 2 1 0

Chlorpropham 708 23 3.2 0.002 - 0.031 0.001 - 0.003 18 5 0

Ethoprop 708 1 0.1 0.005 0.001 1 0 0

Etoxazole 708 1 0.1 0.002 0.001 1 0 0

Famoxadone 708 2 0.3 0.004 0.002 - 0.008 2 0 0

Fluazifop butyl 708 1 0.1 0.002 0.001 0 1 0

Metribuzin 708 1 0.1 0.003 0.002 1 0 0

Norflurazon desmethyl 708 2 0.3 0.002 0.001 - 0.003 2 0 0

Prometon 708 1 0.1 0.002 0.001 0 1 0

Prometryn 708 3 0.4 0.002 0.001 3 0 0

Pronamide (Propyzamide) 708 44 6.2 0.002 - 0.008 0.001 - 0.003 43 1 0

Propiconazole 708 1 0.1 0.022 0.005 - 0.015 1 0 0

Pyrimethanil 708 1 0.1 0.006 0.001 0 1 0

Spirodiclofen 708 3 0.4 0.010 - 0.020 0.006 3 0 0

Tebuconazole 708 1 0.1 0.002 0.001 0 1 0

Thiobencarb 708 1 0.1 0.007 0.003 1 0 0

3 Butter (1 pesticide)

Ametoctradin 177 1 0.6 0.002 0.001 1 0 0

4 Cantaloupe (1 pesticide)

Diuron 328 1 0.3 0.004 0.002 0 1 0

5 Carrots (7 pesticides)

Carbendazim (MBC) 37 708 1 0.1 0.018 0.010 0 1 0

Ethoprop 708 1 0.1 0.009 0.005 0 1 0

Pentachloroaniline (PCA) 708 4 0.6 0.005 - 0.010 0.005 3 1 0

Propamocarb hydrochloride 708 1 0.1 0.008 0.005 0 0 1

Pyrimethanil 708 3 0.4 0.010 - 0.018 0.005 3 0 0

Tebuconazole 708 2 0.3 0.020 - 0.026 0.015 0 2 0

Terbufos sulfoxide 708 1 0.1 0.027 0.005 0 1 0

Sample Origin

Distribution of Residues with No Tolerance Listed in 40 CFR, Part 180, 

Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

by Commodity/Pesticide

Appendix J. Page 4 of 7
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

6 Cauliflower (13 pesticides)

Carbendazim (MBC) 37 531 1 0.2 0.002 0.001 1 0 0

Chlorpropham 531 10 1.9 0.002 - 0.006 0.001 - 0.003 10 0 0

Fenbuconazole 493 1 0.2 0.003 0.001 - 0.003 1 0 0

Fenpyroximate 531 1 0.2 0.002 0.001 1 0 0

Hexythiazox 531 3 0.6 0.003 0.002 3 0 0

Imazalil 531 1 0.2 0.002 0.001 1 0 0

Norflurazon desmethyl 531 1 0.2 0.002 0.001 1 0 0

Parathion oxygen analog 531 1 0.2 0.003 0.001 1 0 0

Pirimiphos methyl 531 1 0.2 0.005 0.001 1 0 0

Prometryn 531 1 0.2 0.002 0.001 1 0 0

Pronamide (Propyzamide) 531 1 0.2 0.002 0.001 1 0 0

Spirodiclofen 531 2 0.4 0.010 0.006 2 0 0

Thiobencarb 531 3 0.6 0.002 - 0.025 0.001 3 0 0

7 Celery (4 pesticides)

DCPA 354 2 0.6 0.007 - 0.024 0.005 2 0 0

Fenpropathrin 354 1 0.3 0.008 0.005 0 1 0

Pronamide (Propyzamide) 354 1 0.3 0.005 0.005 1 0 0

Propamocarb 354 1 0.3 0.010 0.010 1 0 0

8 Eggplant (7 pesticides)

Carbendazim (MBC) 37 346 1 0.3 0.012 0.010 0 1 0

Chlorpropham 703 5 0.7 0.002 - 0.004 0.001 - 0.010 3 2 0

Dimethoate (parent) 38 703 1 0.1 0.004 0.001 - 0.010 0 1 0

 Omethoate 703 2 0.3 0.016 - 0.019 0.002 - 0.010 1 1 0

Imazalil 703 1 0.1 0.002 0.001 - 0.005 1 0 0

Metaldehyde 346 1 0.3 0.093 0.055 1 0 0

Thiabendazole 703 1 0.1 0.005 0.003 - 0.005 0 1 0

Thiacloprid 703 4 0.6 0.004 - 0.008 0.001 - 0.005 0 4 0

9 Green Beans (23 pesticides)

Ametryn 700 1 0.1 0.004 0.001 0 1 0

Atrazine 700 14 2 0.001 - 0.010 0.001 12 2 0

Benzovindiflupyr 700 1 0.1 0.002 0.001 1 0 0

Chlorpropham 700 15 2.1 0.001 - 0.036 0.001 10 5 0

Cyproconazole 700 2 0.3 0.002 - 0.004 0.001 1 1 0

Dicrotophos 700 1 0.1 0.003 0.001 1 0 0

Difenoconazole 700 13 1.9 0.002 - 0.040 0.001 6 7 0

Dimethomorph 700 2 0.3 0.006 - 0.012 0.003 1 1 0

Fenpropathrin 700 4 0.6 0.002 - 0.035 0.001 1 3 0

Fipronil (parent) 39 700 1 0.1 0.009 0.001 0 1 0

 Fipronil sulfone (MB46136) 700 1 0.1 0.002 0.001 0 1 0

Fluoxastrobin 700 1 0.1 0.002 0.001 0 1 0

Flutolanil 700 1 0.1 0.019 0.001 1 0 0

Flutriafol 700 14 2 0.002 - 0.027 0.001 11 2 1

Oxamyl 700 1 0.1 0.005 0.005 1 0 0

Appendix J. Page 5 of 7
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

Permethrin Total 700 8 1.1 0.004 - 0.076 0.003 3 5 0

Profenofos 700 4 0.6 0.002 - 0.009 0.001 1 3 0

Pronamide (Propyzamide) 700 1 0.1 0.002 0.001 1 0 0

Propamocarb 700 11 1.6 0.001 - 0.12 0.001 4 7 0

Propargite 700 1 0.1 0.002 0.001 1 0 0

Pymetrozine 700 1 0.1 0.003 0.001 0 1 0

Pyrimethanil 700 2 0.3 0.27 - 0.51 0.005 1 1 0

Thiacloprid 700 1 0.1 0.002 0.001 1 0 0

Tolfenpyrad 700 6 0.9 0.011 - 0.044 0.003 6 0 0

10 Peaches (2 pesticides)

Chlorpropham 518 5 1 0.005 - 0.024 0.005 4 1 0

Thiabendazole 518 4 0.8 0.013 - 0.031 0.010 1 3 0

11 Pears (2 pesticides)

Imazalil 707 1 0.1 0.017 0.010 0 1 0

Myclobutanil 707 2 0.3 0.007 0.004 0 2 0

12 Plums (2 pesticides)

Fenpropimorph 277 1 0.4 0.042 0.001 1 0 0

Thiabendazole 277 4 1.4 0.002 - 0.003 0.002 4 0 0

13 Summer Squash (6 pesticides)

Endrin 698 7 1 0.003 - 0.018 0.003 - 0.005 1 6 0

Forchlorfenuron 698 4 0.6 0.002 - 0.003 0.001 1 3 0

Pendimethalin 698 5 0.7 0.001 - 0.002 0.001 - 0.005 0 5 0

Pronamide (Propyzamide) 698 1 0.1 0.006 0.001 - 0.005 1 0 0

Quinoxyfen 698 7 1 0.002 - 0.005 0.001 5 2 0

Quintozene (PCNB) (parent) 40 698 2 0.3 0.005 - 0.009 0.001 - 0.005 2 0 0

 Pentachloroaniline (PCA) 698 12 1.7 0.001 - 0.010 0.001 - 0.005 8 3 1

 Pentachlorobenzene (PCB) 698 2 0.3 0.007 - 0.008 0.001 - 0.002 2 0 0

14 Sweet Bell Peppers (4 pesticides)

Chlorpropham 328 4 1.2 0.005 - 0.023 0.005 2 2 0

Fipronil 328 1 0.3 0.013 0.005 0 1 0

Pyrimethanil 319 1 0.3 0.003 0.003 0 1 0

Triflumizole 319 2 0.6 0.006 - 0.008 0.003 0 2 0

15 Tangerines (1 pesticide)

Flutriafol 531 1 0.2 0.002 0.002 0 1 0

16 Winter Squash (8 pesticides)

Chlorpropham 706 41 5.8 0.001 - 0.018 0.001 7 33 1

Endrin 706 9 1.3 0.003 - 0.014 0.003 0 9 0

Hexythiazox 706 1 0.1 0.001 0.001 1 0 0

Omethoate 706 1 0.1 0.006 0.001 1 0 0

Pendimethalin 706 4 0.6 0.002 - 0.007 0.001 4 0 0

Appendix J. Page 6 of 7
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

Pentachloroaniline (PCA) 706 7 1 0.001 - 0.006 0.001 5 2 0

Propiconazole 706 2 0.3 0.001 0.001 2 0 0

Pyridalyl 706 2 0.3 0.003 - 0.009 0.001 1 1 0

NOTES

1 Includes cyhalothrin lambda plus its R157836 epimer.

2 Food Handling Estabilishment (FHE) tolerance of 0.02 ppm was applied to both acephate and its metabolite/degradate methamidophos.

3 Green Bean sample had 3 tolerance exceeders: acephate and its methamidophos metabolite and buprofezin.

4 Green Bean sample had 4 tolerance exceeders: acephate and its methamidophos metabolite, buprofezin, and dinotefuron.

5 Green Bean sample had 3 tolerance exceeders: acephate and its methamidophos metabolite and dinotefuron.

6 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

7 Green Bean sample had 3 tolerance exceeders: acephate and its methamidophos metabolite and dinotefuron.

8 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

9 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

10 Green Bean sample had 3 tolerance exceeders: acephate and its methamidophos metabolite and buprofezin.

11 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

12 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

13 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

14 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

15 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

16 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

17 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

18 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

19 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

20 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

21 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

22 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

23 Green Bean sample had 2 tolerance exceeders: acephate and dinotefuron.

24 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

25 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

26 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

27 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

28 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

29 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

30 Clothianidin as also a metabolite of thiamethoxam.

31 Green Bean sample had 2 tolerance exceeders: thiamethoxam and its clothianidin metabolite.

32 Tetrahydrophthalimide (THPI) is a metabolite of captafol and captan.

33 Peach sample had 2 tolerance exceeders: fludioxonil and pyrimethanil.

34 Peach sample had 2 tolerance exceeders: fludioxonil and pyrimethanil.

35 Winter squash sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

36 Winter squash sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

37 Carbendazim (MBC) is a metabolite of benomyl and thiophanate methyl.

38 One eggplant sample contained both dimethoate and its omethoate metabolite.

39 One green bean sample contained both fipronil and its sulfone metabolite.

40 Two summer squash samples contained quintozene along with its PCA and PCB metabolites.

^ When a range is not listed, only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

Note:

For those pesticide/commodity pairs where the minimum detected value is less than the limit of quantitation (three times

the limit of detection), the reported values are estimates. In a few cases, this may apply to the maximum detected value.

Appendix J. Page 7 of 7
PESTICIDE DATA PROGRAM

 Annual Summary, Calendar Year 2021

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