United States Department of Agriculture

February 2018

Dear Reader:

We are pleased to present the Pesticide Data Program’s (PDP) 26th Annual Summary for 

calendar year 2016. The U.S. Department of Agriculture (USDA), Agricultural Marketing 

Service (AMS), conducts this program each year to collect data on pesticide residues in food. 

This report shows that when pesticide residues are found on foods, they are nearly always at 

levels below the tolerances set by the U.S. Environmental Protection Agency (EPA).

The PDP provides reliable data to help assure consumers that the food they feed themselves 

and their families is safe. Over 99 percent of the products sampled through PDP had residues 

below the EPA tolerances. Ultimately, if EPA determines a pesticide is not safe for human 

consumption, it is removed from the market. 

The PDP tests a wide variety of domestic and imported foods, with a strong focus on foods 

that are consumed by infants and children. EPA relies on PDP data to conduct dietary risk 

assessments and to ensure that any pesticide residues in foods remain at safe levels. USDA 

uses the data to better understand the relationship of pesticide residues to agricultural practices 

and to enhance USDA’s Integrated Pest Management objectives. USDA also works with U.S. 

growers to improve agricultural practices.

The PDP is not designed for enforcement of EPA pesticide residue tolerances. Rather, the 

U.S. Food and Drug Administration (FDA) is responsible for enforcing EPA tolerances. PDP 

provides FDA and EPA with monthly reports of pesticide residue testing and informs the FDA if 

residues detected exceed the EPA tolerance or have no EPA tolerance established.

The PDP works with State agencies representing all census regions of the country and 

approximately half of the U.S. population. In 2016, samples were collected and analyzed in 

California, Colorado, Florida, Maryland, Michigan, New York, North Carolina, Ohio, Texas, 

and Washington.

For more information about PDP, please visit our website at https://www.ams.usda.gov/

datasets/pdp. For more information about pesticides and food, please visit EPA’s website 

at http://www.epa.gov/safepestcontrol and FDA’s website at http://www.fda.gov/Food/

FoodborneIllnessContaminants/Pesticides.

Agricultural Marketing Service

1400 Independence Avenue, SW, Washington, DC 20250-0201

Voice (202) 720-8998 Fax (202) 720-7135

An Equal Opportunity Provider and Employer
Pesticide Data Program—Annual Summary, Calendar Year 2016

iii

Contents

Page No.

Acknowledgements........................................................................................................................ vii

Executive Summary...................................................................................................................... ix

Acronyms and Abbreviations........................................................................................................ xi

Section I--Introduction............................................................................................................... 1

Section II--Sampling Operations............................................................................................... 4

Conceptual Framework.................................................................................................... 4

Sampling Procedures....................................................................................................... 5

2016 Sampling Operations.............................................................................................. 6

Fresh and Processed Commodities.................................................................................. 8

Eggs................................................................................................................................. 12

Milk................................................................................................................................. 12

Sampling Limitations...................................................................................................... 12

Section III--Laboratory Operations......................................................................................... 12

Overview.......................................................................................................................... 12

Fresh and Processed Commodities.................................................................................. 12

Eggs................................................................................................................................. 14

Milk.................................................................................................................................. 14

Quality Assurance Program............................................................................................. 14

Section IV--Database Management.......................................................................................... 16

Electronic Data Path........................................................................................................ 16

Data Reporting................................................................................................................ 18

Online Database Search Tool.......................................................................................... 18

Section V--Sample Results and Discussion.............................................................................. 18

Overview......................................................................................................................... 18

Import Versus Domestic Residue Comparisons.............................................................. 19

Postharvest Applications................................................................................................. 19

Discussion of Results ..................................................................................................... 19

Special Projects............................................................................................................... 20

Environmental Contaminants.......................................................................................... 20

Tolerance Violations........................................................................................................ 21
Pesticide Data Program—Annual Summary, Calendar Year 2016

v

Figures Page No.

 1 Pesticide Data Program (PDP) Program Operations Support and Data Users................... 2

 2 Program Participants........................................................................................................... 3

 3 Commodity Origin.............................................................................................................. 9

 4 Origin of Selected Fresh Commodities: Cucumber and Grape Samples............................ 11

 5 Pesticide Data Program (PDP) Data Pathway..................................................................... 17

Tables

 1 Pesticide Data Program (PDP) Commodity Collection Schedule for 2016........................ 6

 2 Distribution of Samples Collected by Each Participating State.......................................... 7

 3 Acceptable Products for Collected Commodities................................................................ 8

 4 Sample Preparation Steps for Analysis................................................................................ 13

 

Appendixes A-J

Appendix A Commodity History

Appendix B Distribution of Residues by Pesticide in Fruit and Vegetables

Appendix C Distribution of Residues by Pesticide in Eggs

Appendix D Distribution of Residues by Pesticide in Milk

Appendix E Distribution of Residues for Environmental Contaminants

Appendix F Sample Origin by State or Country

Appendix G Import Versus Domestic Pesticide Residue Comparisons

Appendix H Pesticide Residues by Commodity

Appendix I Number of Pesticides Detected per Sample

Appendix J Samples Reported to the U.S. Food and Drug Administration 

 as Exceeding the Tolerance or Without Established Tolerance
Pesticide Data Program—Annual Summary, Calendar Year 2016

vii

Acknowledgements

The States participating in the Pesticide Data 

Program (PDP) deserve special recognition for 

their contributions to the program. The dedication 

and flexibility of sample collectors allow the U.S. 

Department of Agriculture’s (USDA) Agricultural 

Marketing Service (AMS) to adjust sampling 

protocols when responding to changing trends 

in commodity distribution and availability. PDP 

acknowledges the contributions of the State 

laboratories in providing testing services to the 

program and the USDA National Agricultural 

Statistics Service for providing statistical support. 

PDP also acknowledges the exceptional support 

of the Health Effects Division staff of the U.S. 

Environmental Protection Agency, Office of 

Pesticide Programs, and the U.S. Food and 

Drug Administration, Center of Food Safety and 

Nutrition, Office of Food Safety, in helping to set 

the direction for PDP. 

 

Data presented in this report are the latest available 

and were collected and processed through the 

efforts of the following organizations:

USDA Program Administration

Agricultural Marketing Service

Science and Technology Program

1400 Independence Ave., SW

South Building, Mail Stop 0270

Washington, DC 20250

Ruihong Guo, Ph.D., Deputy Administrator

Science and Technology Program

(202) 720-8556, Facsimile (202) 720-6496

Diana Haynes, Director

Monitoring Programs Division, AMS

1400 Independence Ave, SW

Room 0611-S, Stop 0276

Washington, DC 20250: 

(202) 572-8167, Facsimile (202) 619-1724

Electronic-mail Address:

amsmpo.data@ams.usda.gov

Website:

http://www.ams.usda.gov/pdp

Participating State Agencies

California Department of Food and Agriculture

California Department of Pesticide Regulation

Colorado Department of Agriculture

Florida Department of Agriculture and

 Consumer Services

Maryland Department of Agriculture

Michigan Department of Agriculture and 

 Rural Development

New York Department of Agriculture and 

 Markets

North Carolina Department of Agriculture &

 Consumer Services

Ohio Department of Agriculture

Texas Department of Agriculture

Washington State Department of Agriculture

Participating Laboratories

California Department of Food and Agriculture

Division of Inspection Services

Center for Analytical Chemistry

3292 Meadowview Rd.

Sacramento, CA 95832

 

Florida Department of Agriculture and

 Consumer Services

Chemical Residue Laboratory

3125 Conner Blvd., Bldg. 3

Tallahassee, FL 32399-1650

Michigan Department of Agriculture and 

 Rural Development

Laboratory Division

1615 South Harrison Rd.

East Lansing, MI 48823-5224

New York Department of Agriculture 

 and Markets

Food Laboratory

6 Harriman Campus Road

Albany, NY 12235
Pesticide Data Program—Annual Summary, Calendar Year 2016

viii

Ohio Department of Agriculture

Consumer Analytical Laboratory

8995 East Main St.

Reynoldsburg, OH 43068

Texas Department of Agriculture

Pesticide Laboratory

1500 Research Parkway, Ste. B100

College Station, TX 77845

United States Department of Agriculture

Agricultural Marketing Service

National Science Laboratories

801 Summit Crossing Pl.

Gastonia, NC 28054

Washington State Department of Agriculture

Chemical and Hop Laboratory

21 N. 1st Ave., Ste. 106

Yakima, WA 98902
Pesticide Data Program—Annual Summary, Calendar Year 2016

ix

Executive Summary

In 1991, the U.S. Department of Agriculture 

(USDA), Agricultural Marketing Service (AMS), 

was charged with designing and implementing 

the Pesticide Data Program (PDP) to collect data 

on pesticide residues in food. PDP provides highquality data on residues in food, particularly foods 

most likely consumed by infants and children. 

This 26th Pesticide Data Program summary 

presents results for samples collected in 2016.

This information is provided to the U.S. 

Environmental Protection Agency (EPA). Before 

a company can sell or distribute any pesticide in the 

United States, EPA reviews studies on the pesticide 

to ensure that it will not pose unreasonable risks 

to human health or the environment. Once EPA 

has made that determination, it will license or 

register that pesticide for use in strict accordance 

with label directions. 

Before allowing a pesticide to be used on a food 

commodity, EPA sets limits on how much of a 

pesticide may be used on food during growing, 

processing, and storage, and how much can 

remain on the food that reaches the consumer. 

Government inspectors monitor food in interstate 

commerce to ensure that these limits are not 

exceeded. EPA also sets standards to protect 

workers from exposure to pesticides on the job. 

AMS’s Monitoring Programs Division (MPD) 

is responsible for the administration, planning, 

and coordination of day-to-day PDP operations. 

MPD meets regularly with EPA and other 

Government agencies to establish program 

priorities and direction. In 2016, sampling and/or 

testing program operations were carried out with 

the support of 10 States: California, Colorado, 

Florida, Maryland, Michigan, New York, North 

Carolina, Ohio, Texas, and Washington. These 

States had a prominent role in program planning 

and policy setting, particularly policies relating to 

quality assurance.

PDP commodity sampling is based on a rigorous 

statistical design that ensures the data are reliable 

for use in exposure assessments and can be used 

to draw various conclusions about the Nation’s 

food supply. The pesticides and commodities to 

be included each year in the sampling are selected 

based on EPA data needs and take into account the 

types and amounts of food consumed by infants 

and children. The number of samples collected by 

the States is apportioned according to that State’s 

population. Samples are randomly chosen close to 

the time and point of consumption (i.e., distribution 

centers rather than at the farm gate) and reflect what 

is typically available to the consumer throughout 

the year. Samples are selected without regard 

to country of origin, variety, growing season, or 

organic labeling.

Fresh and processed fruit and vegetables accounted 

for 90.3 percent of the total 10,365 samples 

collected in 2016. Other samples collected 

included eggs (2.8 percent) and milk (6.8 percent). 

Fresh and processed fruit and vegetables tested 

during 2016 were: apples, applesauce, cherries 

(fresh and frozen), cranberries (fresh and frozen), 

cucumbers, grapefruit, grapes, green beans, lettuce, 

olives (canned), oranges, pears, potatoes, spinach, 

strawberries, sweet potatoes, and tomatoes (fresh 

and canned). Domestic samples accounted for 81.2 

percent of the samples while 18.3 percent were 

imports, and 0.5 percent were of unknown origin.

Because PDP data are mainly used for risk 

assessments, PDP laboratory methods are geared 

to detect the lowest possible levels of pesticide 

residues, even when those levels are well below 

the tolerances established by EPA. Prior to testing, 

PDP analysts washed samples for 15-20 seconds 

with gently running cold water as a consumer 

would do; no chemicals, soap, or any special wash 

was used. Results for more than 2 million analyses 

were reported by the laboratories in 2016 and are 

too numerous to be included in their entirety in 

this summary. The PDP database file for 2016, 

along with annual summaries and database files for 

previous years, are available on the PDP website 

at http://www.ams.usda.gov/pdp or by contacting 

MPD.

In 2016, over 99 percent of the samples tested 

had residues well below the tolerances established 

by the EPA with 23 percent having no detectable 
Pesticide Data Program—Annual Summary, Calendar Year 2016

x

pesticide residue. Appendixes B through E 

provide a distribution of residues by pesticide 

for the commodities tested. Residues exceeding 

the tolerance were detected in 0.46 percent (48 

samples) of the total samples tested (10,365 

samples). Of these 48 samples, 26 were domestic 

(54.2 percent), 20 were imported (41.7 percent), 

and 2 were of unknown origin (4.1 percent). 

Residues with no established tolerance were found 

in 2.6 percent (273 samples) of the total samples 

tested (10,365 samples). Of these 273 samples, 179 

were domestic (65.6 percent), 90 were imported 

(32.9 percent), and 4 were of unknown origin (1.5 

percent).

PDP is a voluntary program and is not designed for 

enforcement of tolerances. However, PDP informs 

the U.S. Food and Drug Administration and EPA if 

residues detected exceed the EPA tolerance or have 

no EPA tolerance established.

PDP laboratories also test foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in 

the environment, particularly in soil, can be taken up 

by plants. Results for environmental contaminants 

in all commodities are listed in Appendix E. More 

information on results is provided in the Sample 

Results and Discussion section of this summary.

PDP continually strives to improve methods for 

collecting, testing, and reporting data. These data 

are freely available to EPA and other Federal and 

State agencies charged with regulating and setting 

policies on the use of pesticides and to the public 

by hard copy, internet, or custom reports generated 

by MPD. Additional copies of the PDP Annual 

Summary may be obtained by mailing the form 

provided at the end of the Summary.

Non-Discrimination Statement

In accordance with Federal civil rights law and U.S. Department of Agriculture (USDA) civil rights regulations 

and policies, the USDA, its Agencies, offices, and employees, and institutions participating in or administering 

USDA programs are prohibited from discriminating based on race, color, national origin, religion, sex, gender 

identity (including gender expression), sexual orientation, disability, age, marital status, family/parental status, 

income derived from a public assistance program, political beliefs, or reprisal or retaliation for prior civil 

rights activity, in any program or activity conducted or funded by USDA (not all bases apply to all programs). 

Remedies and complaint filing deadlines vary by program or incident.

Persons with disabilities who require alternative means of communication for program information (e.g., 

Braille, large print, audiotape, American Sign Language, etc.) should contact the responsible Agency or 

USDA’s TARGET Center at (202) 720-2600 (voice and TTY) or contact USDA through the Federal Relay 

Service at (800) 877-8339. Additionally, program information may be made available in languages other than 

English.

To file a program discrimination complaint, complete the USDA Program Discrimination Complaint Form, 

AD-3027, found online at How to File a Program Discrimination Complaint and at any USDA office or write 

a letter addressed to USDA and provide in the letter all of the information requested in the form. To request 

a copy of the complaint form, call (866) 632-9992. Submit your completed form or letter to USDA by: (1) 

mail: U.S. Department of Agriculture, Office of the Assistant Secretary for Civil Rights, 1400 Independence 

Avenue, SW, Washington, D.C. 20250-9410; (2) fax: (202) 690-7442; or (3) email: program.intake@usda.

gov.

USDA is an equal opportunity provider, employer, and lender.

Disclaimer: Mention of a trade name or brand name does not constitute endorsement or recommendation by 

USDA over similar products or vendors.
Pesticide Data Program—Annual Summary, Calendar Year 2016

xi

Acronyms and Abbreviations

% C.V. Percent Coefficient of Variation

A2LA American Association for Laboratory Accreditation

AL Action Level

AMS Agricultural Marketing Service

BQL Below Quantifiable Level

CSV Comma-Separated Values

EPA U.S. Environmental Protection Agency

e-SIF Electronic Sample Information Form

FAPAS Food Analysis Performance Assessment Scheme

FDA U.S. Food and Drug Administration

FQPA Food Quality Protection Act

GC Gas Chromatography

HCB Hexachlorobenzene

ISO International Organization for Standardization

LC Liquid Chromatography

LOD Limit of Detection

LOQ Limit of Quantitation

MPD Monitoring Programs Division

MRM Multiresidue Method

MS Mass Spectrometry

NASS National Agricultural Statistics Service

NSL National Science Laboratories

PDP Pesticide Data Program

PPS Probability proportionate-to-size

PT Proficiency Testing

QA Quality Assurance

QAU Quality Assurance Unit
Pesticide Data Program—Annual Summary, Calendar Year 2016

xii

QuEChERS Quick, Easy, Cheap, Effective, Rugged and Safe

QC Quality Control

RDE Remote Data Entry

SIF Sample Information Form

SOP Standard Operating Procedure

SQL Structured Query Language

USDA United States Department of Agriculture
Pesticide Data Program—Annual Summary, Calendar Year 2016

1

Pesticide Data Program (PDP)

Annual Summary, Calendar Year 2016

This summary consists of the following sections: (I.) Introduction, (II.) Sampling Operations, 

(III.) Laboratory Operations, (IV.) Database Management, and (V.) Sample Results and Discussion

I. Introduction

The U.S. Department of Agriculture’s (USDA) 

Agricultural Marketing Service (AMS) initiated the 

Pesticide Data Program (PDP) in 1991 to collect 

data on pesticide residues in food, and the program 

now has an important role in the implementation 

of the 1996 Food Quality Protection Act (FQPA). 

The law directs the Secretary of Agriculture to 

collect pesticide residue data on commodities 

most frequently consumed by infants and 

children. PDP data are used primarily by the 

U.S. Environmental Protection Agency (EPA) to 

assess dietary exposure during the review of the 

safety of existing pesticide tolerances (Maximum 

Residue Limits). EPA establishes the tolerances 

after developing a risk assessment that considers 

the following: the pesticide exposure through diet 

and drinking water and from uses in and around 

the home; the cumulative exposure to two or more 

pesticides that cause a common toxic effect; the 

possibility of increased susceptibility to infants and 

children or other sensitive subpopulations from 

exposure to the pesticide; and the possibility that 

the pesticide produces an effect in people similar 

to an effect produced by a naturally occurring 

estrogen or produces other endocrine disruptions. 

PDP data also are used by the U.S. Food and 

Drug Administration (FDA) to assist in planning 

commodity surveys for pesticide residues for its 

enforcement and regulatory programs.

Because PDP collects data on food commodities 

primarily for exposure assessment, program 

operations differ markedly from those followed 

by regulatory monitoring programs for tolerance 

enforcement. Commodities chosen for inclusion 

in the program are based on EPA data needs. 

PDP samples are collected closer to the point of 

consumption and are prepared emulating consumer 

practices. PDP sampling does not impede 

commodity distribution. Laboratory operations 

are designed to achieve the lowest detectable 

levels rather than quick sample turnaround. As 

a dietary risk assessment support program, PDP 

tests for registered uses for the commodities in the 

program, as well as for pesticides that may not have 

U.S. tolerances but are used in other countries on 

commodities exported to the United States.

Figure 1(a) illustrates contributors to PDP 

policy development and planning operations. 

Primary contributors to these activities include 

the participating States, EPA, USDA’s National 

Agricultural Statistics Service (NASS), and 

additional stakeholders including industry and 

grower groups. Figure 1(b) depicts PDP primary 

data users including EPA, FDA, USDA’s Economic 

Research Service and Foreign Agricultural Service, 

participating States, academic institutions, chemical 

manufacturers, environmental interest groups, food 

safety organizations, and groups within the private 

sector representing food producers. Other Federal, 

State, and foreign government agencies and industries 

have used PDP data to promote the export of U.S. 

commodities to international markets. Additionally, 

the Codex Alimentarius Committee on Pesticides 

Residues recognizes PDP methodologies as official 

and validated methods for the determination of 

pesticide residues in foods.

In 2016, sampling services were provided by 10 

States (California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, Texas, 

and Washington). Laboratory services were provided 

by the States of California, Florida, Michigan, New 

York, Ohio, Texas, and Washington, along with the 

AMS National Science Laboratories (NSL). The 

AMS Monitoring Programs Division (MPD) is 

responsible for overall management of PDP.

Figure 2 shows the States that participate in 

program sampling and/or testing. Together, these 

States represent about 50 percent of the Nation’s 

population and all four census regions of the United 

States. They also represent major U.S. producers 

of fruit and vegetables. MPD works closely with 

EPA and FDA to select commodities and pesticides 

for testing. The selected commodities represent the 

highest U.S. consumption, with an emphasis on 
Pesticide Data Program—Annual Summary, Calendar Year 2016

2

Figure 1. Pesticide Data Program (PDP) Program Operations Support and Data Users. This figure 

illustrates (a) agencies/groups that support PDP program policy and planning activities and (b) agencies/groups 

that use PDP data. 

Program Operations

Participating 

States

National

Agricultural Statistics 

Service

Industry and

Grower Groups

Environmental

Protection

Agency

(a) PDP Policy and Planning Contributions

Data

Food and Drug 

Administration Environmental 

Protection 

Agency

Academic 

Institutions

Agricultural 

Industry

Foreign 

Agricultural 

Service

Economic 

Research 

Service

Chemical 

Manufacturers, 

Environmental 

Interest Groups, Food 

Safety Organizations

Other 

Government 

Agencies

Participating 

States

(b) PDP Data Users
Pesticide Data Program—Annual Summary, Calendar Year 2016

3

foods consumed by infants and children. Commodities 

are cycled through the program approximately every 

5 years. High-consumption fresh fruit and vegetable 

commodities remain in the program for 2 years to 

capture two full growing seasons, thereby capturing any 

changes due to seasonality or year-to-year variations. 

Processed products, as well as dairy, meat, fish, and 

grains, are tested for 1 full year. Appendix A provides 

a list of commodities tested by PDP from the beginning 

of the program in 1991 through 2017.

Fruit and vegetable samples are collected at terminal 

markets1 and large chain store distribution centers from 

which food commodities are supplied to supermarkets 

and grocery stores. Sampling at these locations 

allows for residue measurements that include 

pesticides applied during crop production and those 

applied after harvest (such as fungicides, growth 

regulators, and sprouting inhibitors) and takes into 

account residue degradation while food commodities 

are in storage. Participation as a PDP sampling site is 

voluntary, which sets it apart from State and Federal 

enforcement programs. In 2016, over 600 sites 

granted access and provided information, including 

site volume data, to sample collectors. Voluntary 

cooperation is important to PDP and makes it 

possible to adjust sampling protocols in response to 

fluctuations in food distribution and production.

Washington

California

Colorado

Texas

Ohio

New York

Florida

Maryland

Michigan

Participating State

Location of Participating State Laboratories

North Carolina

Location of Participating Federal Laboratory

Figure 2. Program Participants. During 2016, USDA’s Agricultural Marketing Service established cooperative agreements 

with 10 States to sample and/or test Pesticide Data Program commodities. Together, these States represent about 50 percent 

of the Nation’s population and all four census regions of the United States. These States are the major U.S. producers of fruit 

and vegetables. State laboratories were responsible for analyzing fresh and processed fruit and vegetable samples. The USDA 

National Science Laboratory analyzed the egg samples.

1 Terminal markets are facilities where wholesalers receive large quantities of fresh fruit and vegetables by rail, truck, and air 

from around the world for sale to grocers, restaurants, institutions, and other businesses. Terminal markets are often located 

in metropolitan areas at or near major transportation hubs.
Pesticide Data Program—Annual Summary, Calendar Year 2016

4

Pesticides screened by PDP include those with 

current registered uses for the commodity being 

tested and compounds for which toxicity data and 

preliminary estimates of dietary exposure indicate 

the need for more extensive residue data. PDP also 

monitors pesticides for which EPA has modified 

use directions (i.e., reduced application rates or 

frequency) as part of risk management activities. 

In addition, PDP tests for selected pesticides 

that may not have U.S. tolerances but are used in 

other countries that export commodities to the 

United States. The following appendixes list the 

specific pesticides tested in the program: fruit and 

vegetables (Appendix B), eggs (Appendix C), and 

milk (Appendix D). Environmental contaminants, 

or pesticides whose uses have been canceled in 

the United States but their residues persist in the 

environment, are consolidated into Appendix E, 

which summarizes findings for these chemicals 

across all commodities. 

II. Sampling Operations

♦ Conceptual Framework

The goal of the PDP sampling program is to obtain 

a statistically valid representation of the U.S. food 

supply. PDP data reflect actual pesticide residue 

exposure from food. Using a rigorous statistical 

design, PDP has developed extensive procedures 

that ensure samples are randomly selected from the 

national food distribution system and reflect what is 

typically available to the consumer.

Ten States currently participate in PDP–California, 

Colorado, Florida, Maryland, Michigan, New York, 

North Carolina, Ohio, Texas, and Washington. The 

initial participating States in 1991 (California, Florida, 

Michigan, New York, Texas, and Washington) were 

selected based on agricultural production, analytical 

capabilities, population, and regional/geographic 

distribution – all four U.S. Census Regions (West, 

South, Midwest, Northeast) were represented. Later 

in 1993, Colorado joined to represent the Mountain 

Division of the Western Region and Ohio to further 

represent the densely populated East North Central 

Division of the Midwest Region. In 1993, North 

Carolina was included to better represent the South 

Atlantic Division of the Southern Region. Maryland 

was added in 1997 to represent the South Atlantic 

Division of the Southern Region. Today, these 

States together represent about 50 percent of the 

Nation’s population and all four census regions of 

the United States.

Commodities chosen for inclusion in the program 

are based on EPA data needs. Foods selected for 

testing are high-consumption items with a strong 

focus on foods that are highly consumed by infants 

and children. Each fresh commodity is sampled 

and tested for 2 years in order to capture annual 

and seasonal variability. High-consumption items 

are rotated in and out of the program every 5 years 

– for example, apples, lettuce, and oranges are 

retested and the data refreshed every 5 years.

PDP collects a minimum of 600 samples per 

commodity per year in order to provide an 

accurate statistical representation for a given 

commodity. PDP collects additional samples 

to allow apportionment among the participating 

States over a 12-month period and to allow for a 

small sample overage for any missed, damaged, or 

unusable samples. Participating State population 

figures are used to apportion the number of 

samples scheduled for collection each month. PDP 

sampling operations may be adjusted according 

to product availability. For example, cherries, 

nectarines, and peaches may be oversampled 

during the summer months to make up for low 

availability during winter months. In some cases, 

frozen product is allowed as an alternative to fresh 

(e.g., cranberries).

PDP samples are collected at terminal markets and 

warehouse distribution centers, close to the point of 

consumption. Participating State agencies compile 

and maintain lists of these sampling sites. In 2016, 

over 600 sites granted access to sample collectors. 

The States provide AMS and NASS with annual 

volume information for commodities distributed 

at these sites. Based on this information, sites are 

assigned volume indicators compared to other sites 

in the same State. This volume indicator is used 

to ensure larger sites are selected more frequently 

than smaller sites. This information is used to 

weight the site to determine the probability for 

sample selection. For example, a weight of 10 may 

be given to a site that distributes 100,000 pounds 

of produce annually and a weight of 1 is given 
Pesticide Data Program—Annual Summary, Calendar Year 2016

5

to a site that distributes 10,000 pounds. This site 

selection method, termed probability-proportionateto-size (PPS), then results in the larger site being 10 

times more likely to be selected for sampling than 

the smaller site. 

Each participating State works with NASS to 

develop statistical procedures for site weighting 

and selection. States are also given the option to 

have NASS perform their quarterly site selection. 

The number of sampling sites and the volume of 

produce distributed by the sites vary greatly among 

States. Sampling plans that include sampling dates, 

sites (primary and alternate), targeted commodities, 

and testing laboratories are prepared by each State 

on a quarterly basis. Collection of commodities is 

randomly assigned to weeks of the month, prior to 

selection of specific sampling dates within a week. 

Because sampling sites are selected for an entire 

quarter, States may assign the sites to particular 

months based on geographic location.

Sample information is captured at the time of 

collection for inclusion in the PDP database. PDP 

sample origin data identify the State or country 

where the commodity was produced. A comparison 

of PDP sample origin data to State production and 

import data by USDA’s NASS shows PDP sampling 

is representative of the U.S. food supply. 

♦ Sampling Procedures

While obtaining PDP samples, collectors randomly 

select the scheduled commodities. Collectors 

use established procedures to prevent crosscontamination and maintain chain-of-custody. PDP 

State sample collectors are trained to adhere to 

detailed program Standard Operating Procedures 

(SOPs) that provide criteria for site selection and 

specific instructions for sample selection, shipping 

and handling, and chain-of-custody. SOPs are 

updated as needed and serve as a technical reference 

in conducting program sampling reviews to ensure 

program goals and objectives are met. PDP 

sampling SOPs are available on the website: www.

ams.usda.gov/pdp. On a quarterly basis, sample 

collectors are provided with Commodity Fact Sheets 

that list specific collection details for the individual 

commodities in the program.

Temperature-sensitive samples are packed in 

heavy-duty, temperature-controlled containers. 

Holding temperatures are preserved throughout 

transit time with the inclusion of ample frozen cold 

packs and insulating materials. Non-temperaturesensitive samples do not require temperaturecontrolled containers; however, they are shipped 

in heavy-duty, well-cushioned containers. To 

preserve sample integrity, most samples are 

shipped the same day by overnight delivery. 

Non-refrigerated processed commodities such 

as peanut butter are often shipped by ground 

transportation to reduce shipping costs. 

Electronic Sample Information Forms (e-SIFs) 

are used for chain-of-custody and to capture 

information needed to characterize the sample. 

Sample collectors use tablets or laptop computers 

in the field to record sample identification 

information such as: (1) State of sample 

collection, (2) collection date, (3) sampling 

site code, (4) commodity code, and (5) testing 

laboratory code. Information from these five 

data elements is combined to form a unique PDP 

identification number for each sample. Other 

available information about each sample is also 

recorded, such as collector name; the State or 

country of origin; product variety; production 

claims such as organic; expiration date; and 

grower, packer, and/or distributor locations. 

The e-SIFs are sent electronically the same day 

as sample collection or, at the latest, by the next 

morning after collection to ensure that sample 

information is received at each laboratory by 

the time samples arrive for analysis. Refer to 

Section IV on Database Management for more 

information on the e-SIF system. 

Because most PDP samples are collected at 

distribution centers, terminal markets, and other 

wholesalers, entire cases must be obtained while 

a significantly smaller portion is sent to the 

laboratory for testing. For example, if a 20-pound 

case of apples is collected and a 5-pound sample 

is sent for testing, the remaining 15 pounds is 

donated. In most cases, the excess samples are 

donated to organizations such as local food banks, 

shelters, senior assisted living centers, churches, 

and other charities. PDP often provides the only 

fresh commodity donations available to these 
Pesticide Data Program—Annual Summary, Calendar Year 2016

6

organizations. As a specific example, the State of 

Michigan donated over 2,000 pounds of produce 

each month to the Greater Lansing Food Bank 

during 2016.

♦ 2016 Sampling Operations

The number of fruit, vegetable, eggs, and milk 

samples collected in each participating State is 

determined by State population. The quarterly 

collection schedule for all 2016 commodities is 

shown in Table 1. The total number of samples 

collected in each State for each commodity is listed 

in Table 2. Figure 2 illustrates the participating 

collection States and the laboratories to which 

samples were shipped. Table 3 lists the acceptable 

product types for each collected commodity as seen 

on Commodity Fact Sheets provided to sample 

collectors. For all commodities, domestic or 

imported and organically grown or conventionally 

grown products are acceptable. In 2016, 4.8 percent 

of the tested samples were organic (502 of 10,365).

State population figures are used to assign the number 

of fruit, vegetable, and other specialty samples 

scheduled for collection each month. During 2016, 

the monthly number of samples assigned for each 

State included: California, 13; Colorado, 2; Florida, 

7; Maryland, 4; Michigan, 6; New York, 9; Ohio, 6; 

Texas, 8; and Washington, 4. This schedule resulted 

in a monthly target of 59 samples per commodity, or 

708 samples per commodity per year. Additionally, 

North Carolina collected 4 samples per month for 

selected commodities–applesauce, cranberries, 

cucumbers, green beans, lettuce, canned olives, and 

canned tomatoes, which resulted in a total of 756 

samples per commodity per year for these products. 

In 2016, fruit, vegetables, egg, and milk samples 

were randomly collected by trained State inspectors 

at terminal markets and large chain store distribution 

Commodity Jan-Mar Apr-Jun Jul-Sep Oct-Dec End Date

Apples Sep-16

Applesauce Sep-17

Cherries, Fresh/Frozen Mar-16

Cranberries, Fresh/Frozen Sep-18

Cucumbers Jun-17

Eggs Aug-16

Grapefruit Sep-17

Grapes Dec-16

Green Beans Sep-16

Lettuce Jun-17

Milk Dec-17

Olives, Canned Sep-18

Oranges Dec-16

Pears Dec-16

Potatoes Dec-16

Spinach Dec-16

Strawberries Sep-16

Sweet Potatoes Mar-18

Tomatoes Sep-16

Tomatoes, Canned Sep-17

Table 1. Pesticide Data Program (PDP) Commodity Collection Schedule for 2016. Samples are 

most often collected for a 2-year time period. Commodities are initiated or terminated in different 

quarters of the year so that new commodities are not brought into the program all at the same time. 

This table illustrates time ranges for the listed commodities. See Appendix A for the complete PDP 

commodity history (May 1991 through December 2017).
Pesticide Data Program—Annual Summary, Calendar Year 2016

7

State AP CA CH CU GB GF GR LT OG PE PO SP ST SW TO

Total 

Fresh

California 117 29 4 156 117 155 156 156 156 156 156 154 117 117 117 1,863

Colorado 18 6 24 18 25 24 24 24 23 24 25 18 18 18 289

Florida 63 13 1 84 63 82 84 84 84 84 84 84 62 63 63 998

Maryland 36 12 4 48 36 48 48 48 48 48 48 48 36 36 34 575

Michigan 54 18 2 72 54 72 72 72 72 72 72 72 54 54 54 866

New York 81 27 7 108 81 108 108 108 108 108 108 108 81 81 81 1,303

N. Carolina 6 46 36 48 136

Ohio 54 17 1 72 54 70 72 72 72 72 72 72 54 54 53 861

Texas 72 18 10 96 72 95 96 96 96 96 96 96 72 72 72 1,155

Washington 36 10 1 48 36 49 48 48 48 48 48 48 36 37 36 577

TOTAL 531 156 30 754 567 704 708 756 708 707 708 707 530 532 582 8,626

State AC AZ CZ OL TC

Total 

Processed

Total 

Fresh & 

Proccessed 

F&V

California 39 7 34 39 39 158 2,021

Colorado 6 4 6 6 22 311

Florida 21 7 20 21 21 90 1,088

Maryland 13 8 12 12 45 623

Michigan 18 16 18 18 70 936

New York 27 20 27 27 101 1,404

N. Carolina 12 5 12 12 41 177

Ohio 18 1 17 18 18 72 933

Texas 24 3 14 24 24 89 1,244

Washington 12 2 11 12 12 49 626

TOTAL 190 25 144 189 189 737 9,872

Commodity Legend

AC = Applesauce GB = Green Beans PE = Pears

AP = Apples GF = Grapefruit PO = Potatoes

AZ = Cranberries, Frozen GR = Grapes SP = Spinach

CA = Cranberries, Fresh LT = Lettuce ST = Strawberries

CH = Cherries, Fresh MK = Milk SW = Sweet Potatoes

CU = Cucumbers OG = Oranges TC = Tomatoes, Canned

CZ = Cherries, Frozen OL = Olives, Canned TO = Tomatoes, Fresh

EG = Eggs

Table 2. Distribution of Samples Collected by Each Participating State. This table includes those 

commodities collected at terminal markets, distribution centers, and retail markets. 

Eggs

EG

65

10

35

20

30

45

30

39

20

294

Dairy

Milk

MK

156

24

84

48

72

108

71

96

49

708
Pesticide Data Program—Annual Summary, Calendar Year 2016

8

centers throughout the country. Surrogate or 

“proxy” sites (retail markets) are used to collect 

these samples when the commodity of interest is 

unavailable at a terminal market or distribution 

center. In these instances, the commodity is 

selected in the rear storage area of the retail 

facility so possible contamination by the consumer 

is eliminated and to allow capture of sample 

information from product boxes. In 2016, 23 

percent of fruit, vegetable, egg, and milk samples 

were collected at proxy sites. The commodities 

most often collected at these facilities were frozen 

cherries, frozen cranberries, canned olives, canned 

tomatoes, applesauce, milk, and eggs. 

The total number of samples per commodity and 

the percentage of each that were either domestic, 

imported, or of unknown origin are shown in Figure 

3. The origin of some fresh commodities can vary 

greatly throughout the year. Graphic examples 

of this variation can be found in Figure 4, where 

differences in origin (domestic versus import) 

are depicted by month for grapes and cucumbers. 

Fresh and processed fruit and vegetable egg, and 

milk samples originated from 42 States and 20 

foreign countries (refer to Appendix F). 

♦ Fresh and Processed Commodities 

Of all samples collected and analyzed in 2016, 90.3 

percent (9,363 of 10,365) were fruit and vegetables, 

including fresh and processed products. The fresh 

commodities collected for PDP were apples, 

cherries, cranberries, cucumbers, grapefruit, 

Commodity Acceptable Products

Apples All fresh, whole apples.

Applesauce Processed applesauce; regular or chunky; sweetened/unsweetened/lite varieties. Containers 

may be plastic, glass, or cans; however, plastic or cans are preferred because of potential 

breakage with glass.

Cherries Any fresh, whole sweet cherry. Fresh are preferred, but frozen are acceptable.

Cherries, Frozen Frozen sweet cherries. Individually quick frozen or frozen in own juices.

Cranberries Fresh whole cranberries, pre-bagged or loose. Fresh are preferred, but frozen are acceptable.

Cranberries, Frozen Frozen cranberries. Individually quick frozen or frozen in own juices.

Cucumbers Fresh cucumbers. Common, English, burpless, garden, hothouse, seedless, Japanese, or Kirby.

Eggs Whole, fresh raw eggs in the shell. White or brown.

Grapefruit Any fresh whole grapefruit. Pink, red, or white fleshed.

Grapes Fresh table grapes: white/green, red, purple/blue, or black.

Green Beans Fresh green string beans. Whole or pre-cut.

Lettuce Leaf and head (wrapped or unwrapped) lettuce.

Milk Whole milk; pasteurized; Vitamin A and/or D fortified. Container may be glass if plastic or carton 

is not available.

Olives, Canned Canned, pitted black olives. Whole, sliced, chopped, crushed, diced.

Oranges Any fresh, whole oranges.

Pears Any fresh, whole pears.

Potatoes Fresh whole potatoes (Russet, White, Yellow, and Red). No individual size requirements (U.S. 

No.1 or U.S. No.1 size A are the most preferred sizes because they are the most widely 

consumed).

Spinach Any fresh spinach, consisting mainly of four types: Savoy, Flat or Smooth-Leafed, Semi-Savoy, 

and Baby (or Teen). May be in pre-sealed bags, bunched (tied together), or loose (bulk).

Strawberries Fresh, whole strawberries.

Sweet Potatoes Fresh whole sweet potatoes. No individual size requirements.

Tomatoes Fresh tomatoes. Regular round varieties or Plum/Roma.

Tomatoes, Canned Canned tomatoes. Whole, peeled, diced, stewed, puree, crushed.

Table 3. Acceptable Products for Collected Commodities. This table lists the acceptable products for 

each collected commodity as seen on the Commodity Fact Sheets provided to sample collectors. For all 

commodities, domestic or imported and organically grown or conventionally grown products are acceptable.
Pesticide Data Program—Annual Summary, Calendar Year 2016

9

Cucumbers (754 Samples)

A. Fresh Fruit and Vegetable Samples

Pears (707 Samples) Potatoes (708 Samples)

Green Beans (567 Samples) Lettuce (756 Samples) Oranges (708 Samples)

Grapefruit (704 Samples) Grapes (708 Samples)

Cherries (30 Samples) Cranberries (156 Samples)

Spinach (707 Samples)

Domestic 66.8%

Domestic 50.2% Domestic 34.9%

Domestic 78.2%

Import 2.4%

Import 30.9%

Import 63.8%

Import 100%

Import 49.4%

Import 21.8%

Unknown 0.4%

Domestic 85.4% Domestic 95.3% Domestic 96.5%

Domestic 96.6% Domestic 89.0%

Import 3.2% Import 4.1%

Import 14.6%

Import 10.6%

Unknown 1.0%

Unknown 0.4%

Import 6.0%

Apples (531 Samples)

Domestic 94.0%

Import 3.8%

Unknown 0.3%

Unknown 1.3%

Unknown 2.3%

Domestic 95.8%

Unknown 0.4%

Unknown 0.6%
Pesticide Data Program—Annual Summary, Calendar Year 2016

10

B. Processed Fruit and Vegetable Commodities

Figure 3. Commodity Origin. This figure depicts the proportion of commodity origin (domestic, import, unknown, 

and mixed national origin) for each fresh and processed fruit and vegetable product tested in 2016.

Cherries, Frozen (144 Samples)

Domestic 96.3%

Import 20.0%

Domestic 47.2%

Applesauce (190 Samples)

Unknown 0.4%

Sweet Potatoes (532 Samples)

Domestic 99.6%

Unknown 0.5%

Import 52.8%

Import 60.0%

Tomatoes (528 Samples)

Domestic 39.8%

Import 10.6%

Strawberries (530 Samples)

Domestic 89.4% Unknown 0.2%

Cranberries, Frozen (25 Samples)

Tomatoes, Canned (189 Samples)

Domestic 91.1%

Import 8.4%

Domestic 80.0%

Import 3.7%

Domestic 76.7%

Olives, Canned (189 Samples)

Import 23.3%
Pesticide Data Program—Annual Summary, Calendar Year 2016

11

grapes, green beans, lettuce, oranges, pears, potatoes, 

spinach, strawberries, sweet potatoes, and tomatoes. 

The processed commodities included applesauce, 

frozen cherries, frozen cranberries, canned olives, 

and canned tomatoes. Fresh and frozen fruit and 

vegetable samples weighed either 3 or 5 pounds 

with the exception of cranberries, where the sample 

size was 1 pound. Three pounds were collected for 

smaller, low-weight commodities such as spinach 

and frozen samples, and 5 pounds were collected for 

larger, high-weight commodities such as apples and 

sweet potatoes. 

♦ Eggs 

PDP collected and analyzed 294 chicken egg 

samples in 2016. Samples, comprised of one dozen 

eggs, were collected from routine PDP sampling 

sites that included major chain-store distribution 

centers, terminal markets, and proxy sites. About 

64 percent of the samples were collected from proxy 

sites. All of the egg samples were domestic. Only 

fresh, in their shell, egg samples were collected, 

regardless of size or color. Analysis was performed 

by the USDA’s NSL located in Gastonia, NC. 

Figure 4. Origin of Selected Fresh Commodities: Cucumber and Grape Samples. Differences in origin (domestic 

vs. import) are illustrated by month. 

Origin of Cucumber Samples

Domestic Imported Unknown

JANFEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

Origin of Grape Samples

Number of Samples Number of Samples
Pesticide Data Program—Annual Summary, Calendar Year 2016

12

♦ Milk 

PDP collected and analyzed 708 milk samples in 

2016. One quart samples were collected from routine 

PDP sampling sites that included major chain-store 

distribution centers, terminal markets, and proxy 

sites. Sixty-four and a half percent of the samples 

were collected from proxy sites. All of the milk 

samples were domestic. Only whole pasteurized 

milk samples were collected. Reduced fat milk (1% 

or 2%), flavored milk (chocolate, strawberry), ultrahigh temperature pasteurized milk (not requiring 

refrigeration), and any milk other than cow’s milk 

were excluded. Analysis was performed by the 

California Department of Food and Agriculture 

laboratory located in Sacramento, CA.

♦ Sampling Limitations

Ten States from all four census regions of the United 

States participate in PDP. The States that participate 

account for about 50 percent of the U.S. population 

and the major agricultural production areas of the 

country, making them representative of the United 

States as a whole. 

PDP collects samples from over 600 distribution 

centers and terminal markets within the participating 

States. The total number of distribution centers and 

terminal markets within the participating States is 

difficult to establish since existing sites may go out 

of business or merge and new sites may open during 

the course of the year. However, sites within the 

States that participate do not differ significantly from 

those that do not participate. Since these sites are 

similar throughout the State, they are representative 

of all sites in the State. 

Sometimes it is necessary to replace the site that 

was originally selected using PPS. In those cases, 

an alternate site is selected by the State personnel 

to replace the original site. Whenever possible, a 

site of similar size in the same region as the original 

site is chosen as the replacement. Additionally, the 

availability of a specific commodity may necessitate 

a change in site selection. For example, lettuce may 

be collected from an alternate site if the primary site 

is out of stock.

III. Laboratory Operations

♦ Overview

Seven State laboratories and one USDA laboratory 

performed analyses for PDP. These laboratories 

are equipped with instrumentation capable of 

detecting residues at very low levels. Laboratory 

staff members receive intensive training and must 

demonstrate analytical proficiency on an ongoing 

basis. Laboratory scientists continually test new 

technologies and develop new techniques to 

improve the levels of detection. Any major change 

in methodology and/or instrumentation is evaluated 

and its soundness demonstrated and documented by 

means of method validation modules in accordance 

with PDP SOPs.

♦ Fresh and Processed Commodities

Fruit and vegetable samples were tested for 480 

parent pesticides, metabolites, degradates, and/

or isomers, plus 22 environmental contaminants 

using Multi-Residue Methods (MRMs). Pesticides 

screened by PDP include those with current 

registered uses for the commodity being tested and 

compounds for which toxicity data and preliminary 

estimates of dietary exposure indicate the need for 

more extensive residue data. 

Upon arrival at the testing facility, samples of 

fresh commodities were visually examined for 

acceptability and discarded if determined to be 

inedible (decayed, extensively bruised, or spoiled). 

Laboratories are permitted to refrigerate incoming 

fresh fruit and vegetable samples of the same 

commodity up to 72 hours to allow for different 

sample arrival times from collection sites. Frozen 

and canned commodities may be held in storage 

(freezer or shelf) until the entire sample set is ready 

for analysis.

Each sample is prepared according to the procedures 

detailed in Table 4, which lists the steps for 

preparing each commodity for analysis as defined 

in the Laboratory Sample Processing and Analysis 

Standard Operating Procedure. For all commodities, 

the sample is chopped, mixed, or blended until a 

visually homogeneous mixture is attained. 
Pesticide Data Program—Annual Summary, Calendar Year 2016

13

Commodity Sample Preparation Steps

Apples Wash and drain. Do not peel. Remove the stem. Remove the core using a commercially

available apple corer, or cut each apple in half or quarters and remove the core portion.

Applesauce If the sample is comprised of a single container, simply weigh appropriate analytical portion. If 

the sample is comprised of multiple containers, combine and mix enough containers to achieve 

the specified sampling size (48 ounces) and weigh appropriate analytical portion.

Canned Product: Olives, 

Tomatoes

If the lid of the can has visible dirt or dust, rinse the lid under cold running tap water for 5 to 10 

seconds. Dry the lid with a paper towel. Open each can and pour the entire contents of each 

can including the liquid into a blender/homogenizer. 

Cherries Remove the stem from each cherry. Wash and drain. Remove the pit, being careful to

remove as little of the meat as possible.

Cranberries Wash by the handful or by using a colander and drain.

Cucumbers Wash and drain. Cucumbers may be halved or quartered at this point to facilitate

homogenization.

Eggs Crack open eggs that make up the sample unit (minimum 10 eggs) into a clean blender/

homogenizer. Discard the egg shells.

Frozen Product: Cherries, 

Cranberries

The samples may be chopped while frozen, or to prevent damage to the chopper/homogenizer

blades, the sample may be thawed in a refrigerator or in a room temperature water bath. Open

the containers and pour the entire contents into the chopper/homogenizer.

Grapefruit Peel each fruit and remove any excess white membrane.

Grapes Wash and drain. Remove all stems and extraneous matter.

Green Beans Wash and drain. Do not peel. Using a clean, dry knife, remove any stems that are present.

Lettuce - Head Visually examine the head and remove wrapper and damaged or wilted leaves. Rinse and turn

the head top side down to drain.

Lettuce - Leaf Visually examine the sample and remove only the damaged or wilted leaves and any woody

stems. Wash and drain.

Milk If the sample is comprised of a single container, simply weigh appropriate analytical portion. If 

the sample is comprised of multiple containers, combine and mix enough containers to achieve 

the specified sampling size (1 quart) and weigh appropriate analytical portion.

Oranges Peel each fruit and remove any excess white membrane.

Pears Do not peel. Remove stem, if present. Using a clean, dry knife, cut each pear in half or

quarters and remove the core portion.

Potatoes Hold each potato under cold running tap water and gently scrub the entire surface with a clean

vegetable brush to remove any loose soil and grit. Wash and drain.

Spinach Visually examine the sample and remove only the damaged or wilted leaves and any woody

stems. Wash and drain. Note: Bagged pre-washed spinach does not require washing by the

laboratory.

Strawberries Wash by the handful or by using a colander and drain. Remove stems and leaves if present.

Sweet Potatoes Hold each sweet potato under cold running tap water and gently scrub the entire surface with a 

clean vegetable brush to remove any loose soil and grit (remove any woody stems if present). 

Wash and drain.

Tomatoes Wash and drain. Do not peel. Using a clean, dry knife, cut the tomato around the stem area.

Remove any stem, being careful to remove as little of the meat as possible. The tomatoes

may be quartered prior to homogenization.

Table 4. Sample Preparation Steps for Analysis. This table lists the steps for preparing each collected commodity 

for analysis as defined in the Laboratory Standard Operating Procedure. The wash and drain steps refer to a wash 

under cold running water for approximately 15-20 seconds to assure that all surfaces are rinsed, then a drain for 

at least 2 minutes. For all commodities, the sample is chopped, mixed, or blended until a visually homogeneous 

mixture is attained.
Pesticide Data Program—Annual Summary, Calendar Year 2016

14

Samples are separated into analytical portions 

(aliquots) for analysis. If testing cannot be performed 

immediately, the entire analytical set is frozen 

at -40°C or lower, according to PDP’s Quality 

Assurance/Quality Control (QA/QC) requirements. 

Surplus aliquots not used for the initial testing are 

retained frozen in the event that replication of 

analysis or verification testing is required.

For analysis of fruit and vegetables, testing 

laboratories use various Quick, Easy, Cheap, 

Effective, Rugged and Safe (QuEChERS)-based 

approaches.2 All MRMs are determined, prior to 

use and through appropriate method validation 

procedures, to produce equivalent data for PDP 

analytical purposes.

PDP laboratories use gas chromatography (GC) 

and liquid chromatography (LC) instrumentation, 

coupled with tandem mass spectrometry (MS) 

detection systems for the simultaneous identification/

confirmation and quantitation of pesticides. The use 

of these GC-MS/MS and LC-MS/MS systems allows 

the program to capture data for a broad spectrum of 

pesticides, including emerging product chemistries.

♦ Eggs

USDA’s NSL tested 294 samples of raw, whole 

shell eggs from chickens. A total of 107 parent 

pesticides, metabolites, degradates and/or isomers, 

plus 16 environmental contaminants were screened 

in egg samples. Samples were prepared according 

to the procedures detailed in Table 4. Samples were 

extracted using modifications of the QuEChERS 

method, and analyses were performed using GC/MS, 

GC-MS/MS, and LC-MS/MS.

♦ Milk

The California Department of Food and Agriculture 

laboratory tested 708 samples of pasteurized whole 

milk from cows. A total of 425 parent pesticides, 

metabolites, degradates and/or isomers, plus 19 

environmental contaminants were screened in 

milk samples. Samples were prepared according to 

the procedures detailed in Table 4. Samples were 

extracted using modifications of the QuEChERS 

method, and analyses were performed using GC-MS, 

GC-MS/MS, and LC-MS/MS.

♦ Quality Assurance Program

The primary objectives of the QA/QC program 

are to ensure the reliability of PDP data and the 

performance equivalency of the participating 

laboratories. Direction for the PDP QA program 

is provided through SOPs based on EPA Good 

Laboratory Practices, along with program-specific 

QA/QC requirements. The PDP SOPs provide 

uniform administrative and sampling procedures, 

as well as guidelines for laboratory operations and 

data analyses. The SOPs are revised annually to 

accommodate changes in the program and are aligned 

with International Organization for Standardization 

(ISO)3 requirements. PDP laboratories are accredited 

to ISO 17025 by the American Association for 

Laboratory Accreditation (A2LA), an internationally 

recognized accrediting body.

A Technical Advisory Group, comprised of 

laboratory Technical Program Managers and Quality 

Assurance Officers, is responsible for annually 

reviewing program SOPs and addressing QA issues. 

For day-to-day QA oversight, PDP relies on the 

Quality Assurance Unit (QAU) at each participating 

facility. The QAU operates independently from the 

laboratory staff and is responsible for reviewing all 

data generated for PDP and for performing quarterly, 

internal program audits. Preliminary data review 

procedures are performed onsite by each laboratory’s 

QAU. MPD staff conduct a final review of data for 

conformance with SOPs.

Method Performance Requirements: Laboratories 

are required to determine and verify the limits of 

detection (LODs) and limits of quantitation (LOQs) 

for each pesticide/commodity pair. LODs depend 

on matrix, analyte, and methods used (extraction 

and instrumental). LODs for each pesticide/

 3 “ISO” is not an acronym because the initials would be different in various official languages. “ISO” is adopted from the 

Greek word “isos” meaning equal.

2

 M. Anastassiades, S.J. Lehotay, D. Stajnbaher and F.J. Schenck, “Quick, Easy, Cheap, Effective, Rugged and Safe 

(QuEChERS) Method,” J AOAC Int 86 (2003) 412.
Pesticide Data Program—Annual Summary, Calendar Year 2016

15

commodity pair are shown in the applicable crop 

results appendix. Additional method performance/

validation requirements include modules for 

consistent instrument response (linearity), method 

range, and precision and accuracy.

Identification/Confirmation: Identification/confirmation is performed using MS technologies. Residue 

amounts greater than or equal to LOD and below 

LOQ are reported as below quantifiable level (BQL). 

BQLs are assigned values at one-half the LOQ and 

are used along with values greater than or equal to 

LOQ and non-detects in dietary risk assessments 

when appropriate.

Routine Quality Control Procedures: PDP 

procedures for QC are used to assess method and 

analyst performance during sample preparation, 

extraction, and cleanup. To maximize sample 

output and decrease the QC/sample ratio, samples 

are analyzed in analytical sets that include the test 

samples and the following components:

• Reagent Blank - For analysis of fruit and 

vegetables, eggs, and milk, an amount of distilled 

water, equivalent to the natural moisture content of 

the commodity, is run through the entire analytical 

process to confirm glassware cleanliness and system 

integrity.

• Matrix Blank - A previously analyzed sample of 

the same commodity, which contains either very low 

concentrations of known residues or no detectable 

residues, is divided into two portions. The first 

portion is used to determine background information 

on naturally occurring chemicals and the second to 

prepare a matrix spike.

• Matrix Spike(s) - Prior to extraction, a portion of 

the matrix blank is spiked with marker pesticides to 

determine the precision and accuracy of the analyst 

and instrument performance. Marker pesticides 

are compounds selected from different pesticide 

classes (e.g., organochlorines, organophosphates, 

carbamates, conazoles, imidazolinones, macrocyclic 

lactones, neonicotinyls, phenoxy acid herbicides, 

pyrethroids, strobilurins, sulfonyl urea herbicides, 

triazines, uracils), with physical and chemical 

characteristics representative of their corresponding 

pesticide class. Marker pesticides may be used to 

monitor recovery instead of spiking all pesticides. 

This use of marker pesticides optimizes the 

resources required to analyze the thousands of 

analyte/matrix combinations in the program while 

still allowing evaluation of daily recovery patterns. 

In addition, each laboratory must perform matrix 

spikes at least quarterly for each analyte/crop 

combination it reports. Some laboratories choose 

to rotate spikes of all compounds on a set-to-set 

basis or spike all compounds analyzed with each 

set, so that the amount of spike recovery data 

obtained actually exceeds the minimal requirements 

previously stated. During 2016, PDP laboratories 

quantitated a total of 78,276 matrix spikes, with an 

overall mean recovery of 96 percent and an overall 

22 percent coefficient of variation (% C.V.). The % 

C.V. is calculated as the standard deviation divided 

by the mean.

• Process Control Spike - A compound with physical 

and chemical characteristics similar to those of 

the pesticides being tested is used to evaluate the 

analytical process on a sample-by-sample basis. 

Each of the analytical set components, except the 

reagent and matrix blanks, is spiked with process 

controls. During 2016, PDP laboratories quantitated 

a total of 26,560 process controls on 10,365 samples, 

with an overall mean recovery of 100 percent and 

an overall 17% C.V. Of these process controls, 91 

(0.34 percent) were reruns due to initial failure to 

meet PDP recovery criteria. The rerun values are 

not included in these statistics.

Proficiency Testing: All facilities are required 

to participate in PDP’s Proficiency Testing 

(PT) program. In order to properly benchmark 

performance, PDP laboratories participate in 

the international Food Analysis Performance 

Assessment Scheme (FAPAS), administered by 

the Food and Environment Research Agency, 

Sand Hutton, York, United Kingdom. In 2016, 

PDP laboratories that routinely analyze fruit and 

vegetables via MRMs participated in one FAPAS 

round for carrot purée that contained 10 fortified 

analytes. Laboratories were evaluated based on 

z-scores for reported compounds, as well as any 

reported false negatives or false positives. All PDP 

laboratories obtained z-scores less than two, which 

is deemed satisfactory performance.
Pesticide Data Program—Annual Summary, Calendar Year 2016

16

In addition, PDP laboratories participate in an 

internal PT program that is tailored to current 

PDP commodities and testing profiles. For this 

internal program, the California Department of 

Food and Agriculture QAU prepares and issues 

rounds designed by MPD. Spiking compounds 

are selected with specificity and levels for each 

commodity. Fortification levels of selected 

analytes are generally 1 to 10 times the program 

LOQ for that commodity/compound pair. For 

each multiresidue round, one compound per set is 

typically repeated within the round to provide an 

indicator of repeatability. The resulting data are 

used to determine performance equivalency among 

the testing laboratories and to evaluate individual 

laboratory performance. 

During 2016, PDP laboratories received two 

multi-residue fruit and vegetable PT rounds 

(strawberries and zucchini), each consisting of 

three test samples. The strawberry samples were 

fortified with a total of 12 different compounds 

with pyriproxyfen spiked on 2 different samples. 

The zucchini samples were fortified with a total of 

13 different compounds with trifluralin spiked on 

2 different samples at the same level to evaluate 

within and between laboratory variability. All 

PDP laboratories demonstrated satisfactory 

performance in the PT rounds during 2016. 

Onsite Reviews: In addition to the onsite 

assessments performed by A2LA that are required 

to maintain ISO 17025 accreditation, MPD staff 

chemists perform onsite reviews of laboratory 

operations to determine compliance with PDP 

SOPs and provide a report of findings identifying 

potential areas of improvement. Improvements 

in sampling, chain-of-custody, laboratory, 

recordkeeping, and electronic data transmission 

procedures are made as a result of onsite reviews.

IV. Database Management

PDP maintains an electronic database that serves 

as a central data repository. The data captured 

and stored in the PDP database include sample 

collection and product information, residue 

findings, and process control recoveries for each 

sample analyzed, in addition to QA/QC fortified 

recoveries for each set of samples. Each calendaryear survey is stored in a separate database structure, 

which allows easier administration and data reporting. 

The PDP data pathway is illustrated in Figure 5.

♦ Electronic Data Path

 

PDP utilizes the Remote Data Entry (RDE) system, 

which is a customized software application that 

allows participating State and Federal laboratories 

to enter and transmit data electronically. The RDE 

system is centralized with all user interface software 

and database files residing on USDA servers. 

The laboratory users need only a Web browser to 

interface with the RDE system. Access is controlled 

through separate user login/password accounts and 

user access rights for the various system functions 

based on position requirements. The RDE system 

utilizes Secure Sockets Layer technology to encrypt 

all data passed between users’ computers and the 

central Web server. 

A separate Windows®-based system allows sample 

collectors to capture the standardized Sample 

Information Form (SIF) electronically on laptop 

or tablet computers. The e-SIF system generates 

formatted text files containing sample information 

that are e-mailed to MPD staff for import into the 

Web-based RDE system.

The RDE data entry screens have extensive editing 

functions and cross-checks built into the software to 

ensure valid values are entered for all critical data 

elements. This task is made easier by the practice 

of capturing and storing standardized codes for all 

critical alphanumeric data elements rather than their 

complete names, meanings, or descriptions. This 

coding scheme allows for faster and more accurate 

data entry, saves disk storage space, and allows the 

user to perform ad-hoc queries (data searches) on the 

database easily. The data entry screens also perform 

automatic edits on numeric fields, dates, and other 

character fields to ensure entries are within prescribed 

boundaries. 

MPD staff chemists review the data online and 

then to mark the data as ready-for-upload to the 

central PDP database. A separate upload application 

converts and passes the data to the PDP database, 

which is maintained using Microsoft® Access and 

SQL Server database tools. Access to the central 
Pesticide Data Program—Annual Summary, Calendar Year 2016

17

- Collection in 10 States

- Samples taken close to consumer consumption

- Standardized sample information forms

- Data entry on tablet/laptop computers

- Chemists review data on-screen

- Upload data to central database

- 7 State laboratories, 1 Federal laboratory

- Fruit and vegetable samples prepared for

 consumption

- Detect residues at low levels

- Pesticide residue data generated

- Multi-tiered quality assurance data review

 process

- Web-based data entry software

- Import data from other systems

- Access controlled by user login

- Extensive data cross-checks

- Data reconciliation

- Standard & ad hoc reporting

- Annual Summary

- Custom data sets

YEAR-END REVIEW

INTERNET

SAMPLE COLLECTION DATA REVIEW AT HQ

LABORATORY ANALYSIS

LABORATORY REMOTE DATA 

ENTRY (RDE)

DATA REPORTING

Figure 5. Pesticide Data Program (PDP) Data Pathway. An illustration of PDP data path from sample 

collection through laboratory analysis and reporting.

INTERNET
Pesticide Data Program—Annual Summary, Calendar Year 2016

18

PDP database is limited to MPD personnel and is 

controlled through password protection and user 

access rights.

♦ Data Reporting 

The MPD staff frequently receives requests for 

data from government agencies and interested 

outside parties. Ad-hoc queries and custom reports 

are generated to fill such requests. An electronic 

library of data queries is maintained to generate 

standardized data summaries, including the data 

tables, charts, and appendixes in this annual 

summary. Subsets of the PDP calendar-year 

databases are made available for download from 

the PDP website. The data files on the website 

are delimited text files that contain a portion of 

the sampling data, all reported residue findings, 

and reference lists that can be used to interpret 

the standardized codes used in the PDP data. The 

data files can be imported into defined database 

structures and manipulated using common database 

management software packages.

♦ Online Database Search Tool 

In January 2017, a new online PDP Database search 

tool was made available for public use. The search 

tool allows anyone with internet access to search 

for PDP pesticide residue findings on commodities 

tested across all published years. Search criteria 

are selected from lists of all reported commodities, 

pesticides, and survey years. One of five output 

preferences is selected to show individual residue 

findings or summary data. The generated dataset 

can be exported to a comma-separated values 

(CSV) file. The search tool can be reached from 

any PDP website page or directly at https://apps.

ams.usda.gov/pdp.

V. Sample Results and Discussion

♦ Overview

In 2016, PDP conducted surveys on a variety of 

foods including fresh and processed fruit and 

vegetables, eggs, and milk. Of the 10,365 samples 

analyzed, 9,363 were fresh and processed fruit and 

vegetable samples, 294 were eggs, and 708 were 

milk samples. PDP testing methods are designed 

to detect the lowest possible levels of pesticide 

residues. In 2016, over 99 percent of the samples 

tested had residues well below the tolerances 

established by the EPA with 23 percent having no 

detectable pesticide residue. The data reported by 

PDP corroborate that residues found in agricultural 

products sampled are at levels that do not pose risk 

to consumers’ health and are safe according to EPA.

Appendix B tabulates the distribution of residue 

results for fruit and vegetables. Information included 

in this appendix are: number of samples analyzed 

for each compound, number and percent of samples 

with detections, range of concentrations detected, 

range of analytical LODs, and EPA tolerance levels. 

Appendix C provides the distribution of residues 

for eggs. Appendix D provides the distribution of 

residues for milk. 

PDP laboratories tested foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in the 

environment, particularly in soil, these contaminants 

can be taken up by plants. Appendix E tabulates 

the results for environmental contaminants across 

all commodities. Environmental contaminants are 

consolidated into a single appendix because they 

have no registered uses and are not applied to crops 

in the United States. These compounds are subject 

to FDA Action Levels (ALs), rather than tolerances. 

Because environmental contaminants continue to 

persist in the environment, they may be present in 

food commodities at generally low levels. 

Most of the collected and analyzed samples (81.2 

percent) were produced in the United States, 18.3 

percent were imports, and 0.5 percent were of 

unknown origin. Appendix F shows the distribution 

of sample origin by State or country. Of all samples 

collected and analyzed, approximately 35.2 percent 

(3,644 of 10,365) were grown, packed, and/or 

distributed in or from California. Appendix G 

includes a comparison of residues for selected 

commodities with a significant import component.

Food monitoring data, together with dietary 

consumption surveys, are used by EPA to estimate 

dietary exposure to pesticides to ensure the safety of 

existing pesticide uses. EPA uses all results reported 

by PDP, including sample results reported as below 
Pesticide Data Program—Annual Summary, Calendar Year 2016

19

the LOD and those above the tolerance. PDP 

laboratories are required to establish LODs and 

report any instrumental response below the LOD as 

a non-detect. LODs are established experimentally 

for each pesticide/commodity pair and are reported 

with each data set. The number of non-detects 

can be used in conjunction with percent-croptreated data to determine what proportion of these 

values may be counted as zero towards the dietary 

exposure. All individual sample data can be 

downloaded from the PDP Website at http://www.

ams.usda.gov/pdp or obtained by contacting MPD.

♦ Import Versus Domestic Residue Comparisons 

Information about the origin of each PDP sample 

is recorded when the sample is collected. Figure 3 

illustrates the portion of the domestic and import 

component for each of the PDP fruit and vegetable 

commodities in 2016. The data generated by PDP 

reflect pesticide residues in foods, both domestic 

and imported products, available to the U.S. 

consumer. Many fresh and processed commodities 

are almost entirely of domestic origin, such as 

grapefruits (95.8 percent); lettuce (96.6 percent); 

sweet potatoes (99.6 percent); and spinach (96.5 

percent) with only minor import (3.8 percent, 2.4 

percent, 0 percent, and 3.2 percent, respectively) 

and unknown origins (0.4 percent, 1.0 percent, 0.4 

percent, and 0.3 percent, respectively). Other fresh 

commodities, such as grapes and cucumbers, are 

available from domestic growers part of the year 

and imported during the remaining months, as 

illustrated in Figure 4.

Comparisons of selected residues detected in 

imported versus domestic grapes, green beans, 

and tomatoes can be found in Appendix G. These 

sample sets were selected to compare data where 

residues are present in greater than 10 percent of the 

commodity samples and allow for the comparison 

of individual residues. These data also show that 

the residue profiles for domestic and imported 

crops are significantly different. 

The data in Appendix G illustrate that some 

residues were detected more frequently in imported 

samples, some were detected more frequently in 

domestic samples, and some were detected with 

relative equal frequency in domestic and imported 

samples. For example, the fungicide fenhexamid 

was detected in 67.0 percent of the grape samples 

from Chile and 18.3 percent of the U.S. samples. 

In contrast, the fungicide azoxystrobin was detected 

in 33.8 percent of the green bean samples from 

the United States and 3.4 percent of the samples 

from Mexico. The fungicide difenoconazole was 

detected in 22.9 percent of the tomato samples from 

the United States and 21.4 percent of the samples 

from Mexico, showing nearly equal detection rates 

between domestic and imported samples.

All pesticides detected were registered in the United 

States; however, the profiles of residue findings 

were markedly different in the U.S. samples versus 

imported samples. The differences in residue 

detections between countries were likely due to the 

pesticides used in response to pest pressures based 

on differing environmental and climatic conditions 

as well as crop production and protection practices.

♦ Postharvest Applications

Pesticides can be applied before and after harvest 

depending on the crop and approved label use. 

PDP data capture both preharvest and postharvest 

uses because samples are collected at points when 

all pesticide applications have already occurred. 

Pesticides applied postharvest are used primarily 

as fungicides (e.g., azoxystrobin, imazalil, 

o-phenylphenol, and thiabendazole) and growth 

regulators/sprouting inhibitors (e.g., chlorpropham). 

Some detections reported in Appendix B most 

likely reflect postharvest applications to the raw 

agricultural commodity.

♦ Discussion of Results

There are many pesticides registered for use on the 

same crop; however, not all registered pesticides 

are used at the same time or location. Twenty-three 

percent of the samples tested had no detectable 

pesticide residue, and over 99 percent of the samples 

tested had residues below the tolerances established 

by the EPA. Pesticide use is primarily dictated by 

local pest pressures and environmental conditions 

conducive to growth of pest populations, as well 

as the planting of susceptible varieties. These 

differences are captured by PDP data, which reflect 

actual residues present in food grown in various 
Pesticide Data Program—Annual Summary, Calendar Year 2016

20

regions of the United States and overseas. Thus, 

in evaluating consumer exposure to pesticides 

through the diet, EPA uses all available information 

provided by registrants, PDP, and others to verify 

that tolerances meet the safety standards set by 

FQPA. The reporting of residues present at levels 

below the established tolerance serves to ensure 

and verify the safety of the Nation’s food supply.

Food commodities with pesticides detected in 

at least 5 percent of samples tested are shown in 

Appendix H. The data shown include the range 

and mean of values detected and EPA tolerance 

references for each pair. 

By virtue of the MRMs employed, PDP provides 

critical data that can be used by EPA to evaluate 

exposure to multiple residues from the same 

commodity. The data are crucial for assessments 

that consider cumulative exposure to pesticides 

determined to have common mechanisms of 

toxicity. The distribution of multiple pesticides 

occurring in samples tested during 2016 is 

presented in Appendix I. These data indicate 

that 22.7 percent of all samples tested contained 

no detectable pesticides, 15.7 percent contained 

1 pesticide, and 61.6 percent contained more 

than 1 pesticide. Parent compounds and their 

metabolites are combined to report the number of 

“pesticides” rather than the number of “residues.” 

Environmental contaminants, listed in Appendix E, 

have been excluded from this count of pesticides. 

One sample of strawberries imported from Mexico 

contained residues of 22 pesticides. None of the 

residues found on the strawberry sample exceeded 

the established tolerance. Multiple residue 

detections can result from the application of more 

than one pesticide on a crop during a growing 

season; in addition, a number of other factors can 

contribute to multiple detections. For example, 

unintentional spray drift in the field, planting 

of crops in fields previously treated with the 

pesticide, and/or transfer of residues of postharvest 

fungicides or growth regulators applied to other 

commodities stored in the same storage facilities 

could all contribute to residue detections.

In most cases, samples analyzed by PDP are 

composites of 3 to 5 pounds of commodity from the 

same lot. Therefore, the estimated concentrations 

for multiple residue detections in these composite 

sample results may or may not reflect the number 

or levels of pesticides in a single serving item of a 

commodity.

♦ Special Projects

Eggs: The NSL conducted testing on 294 egg 

samples. Appendix C shows that just one residue 

representing one pesticide was detected in eggs. 

Cyromazine was detected in two samples (0.7 

percent). The residue detections were much lower 

than the established tolerance. 

Milk: The California laboratory conducted testing 

for pesticide residues on 708 milk samples. One 

residue representing one pesticide was detected in 

milk (Appendix D). Flubendiamide was detected 

in 18 samples (2.5 percent) of milk. The residue 

detections were much lower than the established 

tolerance. 

♦ Environmental Contaminants

Environmental contaminants include pesticides 

whose uses have been canceled in the United 

States, but their residues persist in the environment, 

particularly in soil, where they may be taken up 

by plants. These data are also used to facilitate 

international trade. Residue results for environmental 

contaminants may be found in Appendix E.

DDT, DDD, and DDE: PDP screened samples for 

various metabolites of DDT including: DDT o,p’; 

DDT p,p’; DDD o,p’; DDD p,p’; DDE o,p’; and 

DDE p,p’. Use of DDT has been prohibited in 

the United States since 1972; however, due to its 

persistence in the environment, low-level residues 

of DDT and its DDD and DDE metabolites were 

detected in some commodities tested. DDE p,p’ was 

detected in spinach (39.2 percent), potatoes (16.7 

percent), sweet potatoes (0.2 percent), tomatoes 

(0.2 percent), and grapes (0.1 percent). DDT p,p’ 

was detected in spinach (15.1 percent), potatoes 

(4.5 percent), and lettuce (0.8 percent). DDT o,p’ 

was detected in spinach (6.7 percent) and potatoes 

(1.4 percent). DDD o,p’ was detected in spinach 

(0.6 percent). DDD p,p’ was detected in spinach 

(0.3 percent), sweet potatoes (0.2 percent), and 
Pesticide Data Program—Annual Summary, Calendar Year 2016

21

potatoes (0.1 percent). No residues of DDE o,p’ 

were detected in any samples. All residues detected 

were lower than established FDA ALs.

Other Extraneous Pesticides: PDP screened 

samples for other environmental contaminants 

including: aldrin, which readily metabolizes 

to dieldrin; BHC (alpha/beta/delta); chlordane 

(total, cis, trans) and its metabolite oxychlordane; 

dieldrin; endrin; heptachlor and its epoxide 

metabolite (total, cis); hexachlorobenzene (HCB); 

lindane (BHC gamma); and mirex. HCB was 

used as a seed protectant until 1965 and, due to 

its persistence, remains in soil and grasses. In 

1974, all aldrin and dieldrin uses were canceled in 

the United States and, in 1978, all heptachlor and 

mirex uses were canceled. In 1986, chlordane uses, 

except termiticide uses, were canceled. Despite 

these cancellations and because they persist in the 

environment, trace residues of chlordane (cis and 

trans) and dieldrin were detected in some of the 

tested commodities.

For example, dieldrin was detected in 4.8 percent of 

cucumber samples, 2.1 percent of spinach samples, 

and 1.6 percent of potato samples. Chlordane (cis) 

was detected in 0.6 percent of spinach samples, 

0.4 percent of potato samples, and 0.3 percent of 

cucumber samples. Chlordane (trans) was detected 

in 0.4 percent of spinach samples. No residues of 

aldrin, BHC (alpha/beta/delta), chlordane (total), 

endrin, heptachlor (parent), heptachlor epoxide 

(total, cis), HCB, lindane (BHC gamma), mirex, or 

oxychlordane were detected in any samples.

♦ Tolerance Violations

A tolerance is defined under Section 408 of the 

Federal Food, Drug, and Cosmetic Act as the 

maximum quantity of a pesticide residue allowable 

on a raw agricultural commodity. Tolerances are 

also applicable to processed foods. The FQPA of 

1996 amended the Federal Insecticide, Fungicide 

and Rodenticide Act to require EPA to periodically 

review each pesticide registration using the most 

currently available data. Timely pesticide data 

provided by PDP enable the EPA to refine risk 

estimates used in the pesticide reregistration 

process. 

A tolerance violation occurs when a residue is 

found that exceeds the tolerance level or when 

a certain residue is found for which there is no 

established tolerance. With the exception of meat, 

poultry, and egg products, for which USDA’s 

Food Safety and Inspection Service is responsible, 

FDA enforces tolerances for all imported foods 

and domestic foods that move through interstate 

commerce. Unlike enforcement programs, PDP 

emphasizes determination of residues at the 

lowest detectable levels rather than quick turnaround times. When PDP identifies samples with 

residues exceeding the tolerance or with residues 

for which there is no established tolerance, these 

detections are reported to FDA’s headquarters 

office. This notification is made in accordance 

with a Memorandum of Understanding between 

USDA and FDA for the purpose of identifying 

areas where closer surveillance may be needed. 

FDA assesses PDP apparent violation data for 

appropriateness for follow up under its regulatory 

pesticide program. Due to the time period required 

for completion of PDP analyses and data reporting, 

FDA follow up will usually be at a subsequent 

harvest or commodity availability period. 

Residues exceeding the established tolerance or 

Action Level are noted with an “X” in Appendix 

B. Similarly, residues for which a tolerance is not 

established are noted with a “V” in Appendix B. 

The “X” and “V” annotations are followed by a 

number indicating the number of samples reported 

to FDA. The EPA tolerances cited in this summary 

and appendices apply to 2016 and not to the current 

year. There may be instances where tolerances 

may have been recently changed that would have 

an effect on whether a residue is violative.

An established tolerance may apply to more than 

one residue because pesticides may break down into 

more than one metabolite or contain more than one 

isomer. For example, the tolerance for endosulfan 

combines residues of endosulfan I, endosulfan 

II, and endosulfan sulfate; and organophosphate 

tolerances may combine the parent compound and 

the sulfone and sulfoxide metabolites. Therefore, 

where applicable, the pesticide violations in 

Appendix J are combined residues of parent and 

any isomers and/or metabolites to count the total 

number of samples with tolerance violations.
♦♦♦♦♦♦

Pesticide Data Program—Annual Summary, Calendar Year 2016

22

A total of 318 samples with 358 pesticides was 

reported to FDA as Presumptive Tolerance 

Violations. Pesticides exceeding the tolerance 

were detected in 0.46 percent (48 samples) of the 

total samples tested (10,365 samples). Of these 

48 samples, 26 were domestic (54.2 percent), 

20 were imported (41.7 percent), and 2 were 

of unknown origin (4.1 percent). The samples 

containing pesticides that exceeded established 

tolerances included: 1 sample of fresh cherries, 

11 samples of cucumbers, 6 grape samples, 3 

fresh green bean samples, 16 samples of spinach, 

3 samples of strawberries, 5 samples of sweet 

potatoes, and 3 samples of tomatoes. 

Residues with no established tolerance were 

found in 2.6 percent (273 samples) of the total 

samples tested (10,365 samples). Of these 273 

samples, 179 were domestic (65.6 percent), 90 

were imported (32.9 percent), and 4 were of 

unknown origin (1.5 percent). These samples 

included 256 fresh fruit and vegetable samples 

and 17 processed fruit/vegetable samples. The 

17 processed fruit/vegetable samples were frozen 

cherries and canned olives. There were 244 

samples that contained 1 pesticide for which 

no tolerance was established, 21 samples with 2 

pesticides for which no tolerance was established, 

and 8 samples that contained 3 pesticides for 

which no tolerance was established. Three of the 

273 samples also contained 1 pesticide each that 

exceeded an established tolerance. In most cases, 

these pesticides with no established tolerance 

were detected at very low levels. Some pesticide 

residues may have resulted from unintentional 

spray drift in the field, planting of crops in fields 

previously treated with the pesticide, or transfer 

of pesticide residues of postharvest fungicides or 

growth regulators applied to other commodities 

stored in the same storage facilities. The pesticide 

residue levels and commodities are listed in 

Appendix J.
Appendix A

Commodity History

Appendix A identifies commodities sampled by the Pesticide Data Program (PDP) through 

December 2017. Updates to this list are posted on the PDP Web site at www.ams.usda.gov/

pdp. 
Appendix A. Page 1 of 8

Fresh Commodities

Commodity Start Date End Date

Apples 1 Sep-91 Dec-96

Apples (S-1) Jan-99 Dec-99

Apples (S-2) Jan-99 May-99

Apples Oct-00 Sep-02

Apples (T-1) Jan-03 Dec-03

Apples Jan-04 Dec-05

Apples Jan-09 Dec-10

Apples (B-1) Aug-12 Oct-12

Apples Oct-14 Sep-16

Asparagus Jan-02 Jun-03

Asparagus Jul-08 Jun-10

Asparagus Jul-17 Ongoing

Avocados Jul-12 Dec-12

Bananas Sep-91 Sep-95

Bananas Jan-01 Dec-02

Bananas (TSP) Jul-03 Dec-03

Bananas Jan-06 Dec-07

Bananas Apr-12 Mar-14

Blueberries (cultivated) 2 Jan-07 Dec-08

Blueberries (cultivated) 2 Jan-14 Dec-14

Broccoli Oct-92 Dec-94

Broccoli Jan-01 Dec-02

Broccoli Oct-06 Sep-08

Broccoli Jan-13 Dec-14

Cabbage Jan-10 Dec-11

Cabbage Jul-17 Ongoing

Cantaloupe Jul-98 Jun-00

Cantaloupe Oct-03 Sep-05

Cantaloupe Jan-10 Mar-10

Cantaloupe Oct-10 Jun-12

Carrots 1 Oct-92 Sep-96

Carrots Oct-00 Sep-02

Carrots Jan-06 Dec-07

Carrots Jan-13 Dec-14

Cauliflower Oct-04 Sep-06

Cauliflower Oct-11 Sep-13

Celery Feb-92 Mar-94

Celery Jan-01 Dec-02

Celery Jan-07 Dec-08

Celery Jan-13 Dec-14

Cherries 3 May-00 Aug-01

Cherries 2 May-07 Sep-07

Cherries Apr-14 Mar-16

APPENDIX A. COMMODITY HISTORY

AS OF DECEMBER 2017
Appendix A. Page 2 of 8

Commodity Start Date End Date

Cilantro Oct-09 Sep-10

Cranberries Oct-06 Dec-06

Cranberries 2 Oct-16 Ongoing

Cucumbers Jan-99 Dec-00

Cucumbers Oct-02 Sep-04

Cucumbers Jan-09 Dec-10

Cucumbers Jul-15 Jun-17

Eggplant Jan-05 Dec-06

Grapefruit Aug-91 Dec-93

Grapefruit Jan-05 Dec-06

Grapefruit Oct-15 Sep-17

Grapes 1 May-91 Dec-96

Grapes Jan-00 Dec-01

Grapes (TSP) Jul-03 Dec-03

Grapes Jan-04 Dec-05

Grapes Jan-09 Dec-10

Grapes Jan-15 Dec-16

Green Beans Feb-92 Dec-95

Green Beans Jan-00 Dec-01

Green Beans Apr-04 Mar-05

Green Beans Jan-07 Dec-08

Green Beans Jul-13 Sep-16

Green Onions (scallions) Oct-08 Sep-09

Greens (collard & kale) Oct-06 Sep-08

Hot Peppers Oct-10 Sep-11

Kale Jan-17 Ongoing

Lettuce May-91 Dec-94

Lettuce Oct-99 Sep-01

Lettuce Jan-04 Dec-05

Lettuce Jan-10 Dec-11

Lettuce Jul-15 Jun-17

Lettuce, Organic Jan-09 Dec-09

Mangoes Apr-10 Sep-10

Mangoes Oct-17 Ongoing

Mushrooms Oct-01 Sep-03

Mushrooms Oct-11 Sep-13

Nectarines 4 Jul-00 Sep-01

Nectarines Jan-07 Dec-08

Nectarines Jan-13 Dec-15

Onions Jan-02 Dec-03

Onions Oct-11 Sep-12

Onions Jan-17 Dec-17

Oranges 1 Aug-91 Dec-96

Oranges Jan-00 Dec-01

Oranges Jan-04 Dec-05

Oranges Jan-09 Dec-10

Oranges Jan-15 Dec-16

Papaya Jul-11 Jun-12
Appendix A. Page 3 of 8

Commodity Start Date End Date

Peaches Feb-92 Sep-96

Peaches (S-3) Jan-00 Sep-00

Peaches 5 Jan-01 Sep-02

Peaches (T-1) May-03 Sep-03

Peaches Oct-06 Sep-08

Peaches (B-1) Aug-12 Oct-12

Peaches Jul-13 Jun-15

Pears Jan-97 Jun-99

Pears (S-1) Jul-98 Jun-99

Pears Oct-03 Sep-05

Pears Jan-09 Dec-10

Pears Jan-15 Dec-16

Pears (B-1) Oct-12 Nov-12

Pineapples Jul-00 Jun-02

Plums 6 Jan-05 Dec-06

Plums Oct-11 Sep-13

Potatoes May-91 Dec-95

Potatoes (S-4) Dec-96 Dec-97

Potatoes Jul-00 Jun-02

Potatoes Jan-08 Dec-09

Potatoes Jan-15 Dec-16

Raspberries 2 Jan-13 Dec-13

Snap Peas Jan-11 Dec-12

Snap Peas Jan-17 Ongoing

Spinach 1 Jan-95 Sep-97

Spinach Jul-02 Dec-03

Spinach 7 Jan-06 Sep-06

Spinach Jan-08 Dec-09

Spinach Jan-15 Dec-16

Strawberries 2 Jan-98 Sep-00

Strawberries Jan-04 Dec-05

Strawberries Jan-08 Dec-09

Strawberries Oct-14 Sep-16

Summer Squash Oct-06 Sep-08

Summer Squash Oct-12 Sep-14

Sweet Corn (on-the-cob) Oct-08 Sep-10

Sweet Corn (on-the-cob) Oct-14 Sep-15

Sweet Bell Peppers Jan-99 Dec-00

Sweet Bell Peppers Oct-02 Sep-04

Sweet Bell Peppers Jan-10 Mar-12

Sweet Potatoes 1 Jan-96 Jun-98

Sweet Potatoes Jan-03 Dec-04

Sweet Potatoes Oct-08 Sep-10

Sweet Potatoes Apr-16 Ongoing

Tangerines Jan-11 Dec-12

Tomatoes 1 Jul-96 Jun-99

Tomatoes Jan-03 Dec-04

Tomatoes Jan-07 Dec-08
Appendix A. Page 4 of 8

Commodity Start Date End Date

Tomatoes Oct-14 Sep-16

Tomatoes, Cherry/Grape Jan-11 Dec-12

Watermelon 8 Oct-05 Sep-06

Watermelon Apr-10 Sep-10

Watermelon Jul-14 Jun-15

Winter Squash 2 Jan-97 Jun-99

Winter Squash Jul-04 Jun-06

Winter Squash Oct-11 Mar-13

NOTES

1

 Excludes sampling hiatus September - November 1996.

2

 Frozen collected when fresh unavailable.

3

 Sampling adjusted for market availability. Cherries were sampled for 2 years 

 (May-00 - Aug-01) for a total of 6 months.

4

 Sampling adjusted for market availability. Nectarines were sampled for 2 years 

 (Jul-00 - Sep-01) for a total of 6 months.

5

 Sampling adjusted for market availability. Peaches were sampled for 2 years

 (Jan-01 - Sep-02) for a total of 16 months.

6

 Dried plums (prunes) were collected when fresh plums were not available.

7

 Spinach ended earlier than planned due to the unavailability of product.

8

 Samples collected in California, Florida, and Texas only.

(B-1) Special project testing for bifenthrin in multi-residue screen.

(S-1) Special single serving project testing for organophosphates.

(S-2) Special single serving project testing for carbamates.

(S-3) Special single serving project testing for carbamate, organochlorine, 

 organophosphate, organonitrogen, and sulfur compounds.

(S-4) Special single serving project testing for aldicarb.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.
Appendix A. Page 5 of 8

Processed Commodities

Commodity Start Date End Date

Apple Juice 1 Jul-96 Dec-98

Apple Juice Jan-02 Dec-02

Apple Juice Jul-07 Jun-08

Apple Juice Jul-12 Jun-13

Applesauce Jul-02 Dec-02

Applesauce Jan-06 Dec-06

Applesauce Oct-16 Sep-17

Asparagus, Canned Jul-03 Dec-03

Beans, Canned (4 varieties) 2 Oct-08 Sep-10

Beets, Canned Jan-11 Dec-11

Blueberries (cultivated), Frozen 3 Jan-07 Dec-08

Blueberries (cultivated/wild), Frozen 3 Jan-14 Dec-14

Cherries, Frozen 4 Apr-14 Mar-16

Corn Syrup 4 Jan-98 Jun-99

Cranberries, Frozen 3 Oct-16 Ongoing

Garbanzo Beans, Canned Oct-17 Ongoing

Grape Juice Jan-98 Dec-99

Grape Juice Jan-08 Dec-08

Grape Juice Oct-13 Sep-14

Green Beans, Canned/Frozen 1 Jan-96 Jun-98

Green Beans, Canned Jan-03 Mar-04

Green Beans, Frozen Apr-05 Dec-05

Green Beans, Canned/Frozen Jan-14 Dec-14

Olives, Canned Oct-16 Ongoing

Orange Juice Jan-97 Dec-98

Orange Juice Oct-04 Sep-06

Orange Juice Oct-10 Sep-11

Orange Juice Jan-12 Jun-12

Peaches, Canned Dec-96 Dec-97

Peaches, Canned Jan-03 Dec-04

Peaches, Canned (T-1) Jan-03 Mar-03

Peaches, Canned (T-1) Oct-03 Dec-03

Pear Juice, Concentrate/Puree Jul-02 Jun-03

Pears, Canned Jul-99 Jun-00

Peas, Canned/Frozen Apr-94 Jun-96

Peas, Canned/Frozen 5 Oct-01 Sep-03

Peas, Frozen Jan-06 Dec-06

Pineapple, Canned Jan-17 Dec-17

Plums, Dried (Prunes) 6 Jan-05 Dec-06

Plums, Dried (Prunes) Oct-17 Ongoing

Potatoes, Frozen Jan-06 Dec-07

Raisins Jul-06 Jun-07

Raspberries, Frozen 3 Jan-13 Dec-13

Spinach, Canned Oct-97 Dec-98
Appendix A. Page 6 of 8

Commodity Start Date End Date

Spinach, Canned Jan-04 Jun-04

Spinach, Canned/Frozen Jul-10 Jun-11

Spinach, Frozen Jan-99 Dec-99

Strawberries, Frozen 3 Jan-98 Sep-00

Sweet Corn, Canned/Frozen Apr-94 Mar-96

Sweet Corn, Canned/Frozen 5 Oct-01 Sep-03

Sweet Corn, Frozen 3 Oct-08 Sep-10

Sweet Corn, Frozen 3 Oct-14 Sep-15

Tomato Paste, Canned Jan-01 Jun-01

Tomato Paste, Canned Jan-09 Dec-09

Tomatoes, Canned Jul-99 Jun-00

Tomatoes, Canned Oct-16 Sep-17

Winter Squash, Frozen 3 Jan-97 Jun-99

Baby Food / Formula Products

Commodity Start Date End Date

Baby Food, Applesauce Jul-12 Jun-13

Baby Food, Carrots Jan-12 Dec-12

Baby Food, Green Beans Oct-10 Sep-11

Baby Food, Peaches Jan-12 Dec-12

Baby Food, Pears Oct-10 Sep-11

Baby Food, Peas Jul-12 Jun-13

Baby Food, Sweet Potatoes Oct-10 Sep-11

Infant Formula, Dairy-Based Oct-13 Sep-14

Infant Formula, Soy-Based Oct-13 Sep-14

NOTES

1 Excludes sampling hiatus September - November 1996.

2 Bean varieties included black, garbanzo, kidney, and pinto.

3 Frozen collected when fresh unavailable.

4 Excludes sampling hiatus January 1999.

5 Canned samples collected in first year and frozen samples in second year of testing.

6 Dried plums (prunes) were collected when fresh plums were not available.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.
Appendix A. Page 7 of 8

Grains

Commodity Start Date End Date

Barley Oct-01 Sep-03

Corn Oct-06 Sep-08

Oats Jul-99 Apr-00

Oats Jan-10 Jun-10

Oats Apr-14 Aug-14

Rice Oct-00 Sep-02

Rice1 Oct-08 Sep-09

Rice Apr-14 Aug-14

Soybeans Sep-96 Feb-98

Soybeans Oct-03 Sep-05

Soybeans Sep-10 Apr-11

Soybeans (S-1) Oct-05 Dec-05

Wheat Feb-95 Jan-98

Wheat Sep-04 Jun-06

Wheat Jul-12 Sep-12

Wheat Flour Jan-03 Dec-04

Wheat Flour (T-1) Jan-03 Dec-03

Nuts and Nut Products

Commodity Start Date End Date

Almonds Jul-07 Mar-08

Peanut Butter Jan-00 Dec-00

Peanut Butter (TSP) Jul-03 Dec-03

Peanut Butter Jan-06 Dec-06

Peanut Butter Apr-15 Aug-15

Dairy Products

Commodity Start Date End Date

Butter Jan-03 Dec-03

Butter Jan-12 Dec-13

Heavy Cream Jul-05 Dec-05

Heavy Cream Jan-07 Dec-07

Milk 2 Jan-96 Oct-98

Milk (TSP) Jul-03 Dec-03

Milk Jan-04 Dec-05

Milk Jan-11 Dec-11

Milk Jan-16 Dec-17

Fish Products

Commodity Type Start Date End Date

Fish 3 Catfish Apr-08 Jun-10

Fish Salmon Jul-13 Jun-14
Appendix A. Page 8 of 8

Meat / Poultry / Pork Products

Commodity Type Start Date End Date

Poultry Young Chickens Apr-00 Mar-01

Poultry Young & Mature Chickens Jan-06 Dec-06

Beef Cows, Heifers, Steers Jun-01 Jul-02

Beef 4 Cows, Heifers, Steers Dec-08 May-09

Pork Gilt, Barrow Jan-05 Jun-05

Other Products

Commodity Start Date End Date

Eggs (TSP) Jul-03 Dec-03

Eggs Jul-10 Jun-11

Eggs Apr-16 Aug-16

Honey Oct-07 Sep-08

Honey Apr-17 Aug-17

Drinking Water

States Start Date End Date

Finished Water Only (27 sites)

California, Colorado, Kansas, New York, Texas Mar-01 Dec-03

Raw Intake and Finished Water (70 sites) Jan-04 Apr-13

Alabama, Arizona, California, Florida, Georgia, Illinois, Indiana, Iowa, Kansas,

Kentucky, Louisiana, Maryland, Michigan, Minnesota, Missouri, Montana, New Jersey, 

New York, North Carolina, North Dakota, Ohio, Oregon, Pennsylvania, South Carolina, 

Tennessee, Texas, Virginia, Washington State, and Washington, D.C.

Bottled Water 

10 Participating States Jan-05 Dec-06

10 Participating States Jan-17 Dec-17

Groundwater 

1,495 Private Wells in 45 States plus Washington, DC Jan-07 Feb-13

16 Municipal Water Facilities in 13 States Mar-10 Feb-13

NOTES

1

 Includes sampling hiatus May-July 2009.

2

 Excludes sampling hiatus September - November 1996.

3 Excludes sampling hiatus April-June 2009.

4

 Survey ended 7 months early due to budgetary constraints.

(S-1) Special survey for fungicides used to combat soybean rust.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.
Appendix B

Distribution of Residues by Pesticide

in Fruit and Vegetables

Appendix B shows residue detections for all fruit and vegetable pesticide/commodity pairs 

tested, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerances for each pair. The EPA tolerances 

cited in this summary and appendixes apply to 2016 and not to the current year. There 

may be instances where tolerances have been recently set, modified, or revoked that 

would have an effect on whether a residue is violative or not.

In 2016, 9,363 fruit and vegetable samples were analyzed, of which 8,626 were fresh 

products and 737 were processed products.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by the U.S. Food and Drug Administration (FDA). Under the Food Quality 

Protection Act, responsibility for establishing tolerances in lieu of ALs has been transferred 

to EPA. In the interim, ALs are used.

The Pesticide Data Program reports tolerance violations to FDA as part of an interagency 

Memorandum of Understanding between the U.S. Department of Agriculture and FDA. 

Residues reported to FDA are shown in the “Tolerance Violation” column and are annotated 

as “X” (if the residue exceeded the established tolerance) or “V” (if the residue did not 

have a tolerance listed in the Code of Federal Regulations, Title 40, Part 180). In both 

cases, these annotations are followed by a number indicating the number of samples 

reported to FDA. 

Results for environmental contaminants across all commodities, including fruit and 

vegetables, have been consolidated in a separate appendix because they have no 

registered uses and are not applied to crops (see Appendix E). 
Appendix B. Page 1 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

2,4,5-T (herbicide) 

Grapefruit 268 0 0.10 ^ NT

Strawberries 530 0 0.10 ^ NT

TOTAL 798 0

2,4-D (herbicide) 

Grapefruit 268 0 0.050 ^ 3.0

Strawberries 530 0 0.050 ^ 0.05

TOTAL 798 0

2,4-DB (herbicide) 

Grapefruit 268 0 0.10 ^ NT

Strawberries 530 0 0.10 ^ NT

TOTAL 798 0

2,4-dimethylphenyl formamide (2,4-DMPF) (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

2,6-DIPN (plant growth regulator) 

Grapefruit 90 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

TOTAL 279 0

Abamectin (insecticide)

Applesauce 190 0 0.050 ^ 0.02

Grapefruit 358 0 0.020 ^ 0.02

Grapes 708 0 0.050 ^ 0.02

Olives, Canned 189 0 0.020 ^ 0.01

Pears 707 0 0.050 ^ 0.02

Strawberries 530 1 0.2 0.029 ^ 0.020 ^ 0.05

TOTAL 2,682 1

Acephate (insecticide)

Apples 531 0 0.003 ^ 0.02

Applesauce 190 0 0.003 ^ 0.02

Cherries 30 0 0.15 ^ 0.02

Cherries, Frozen 144 0 0.15 ^ 0.02

Cranberries 156 0 0.015 ^ 0.5

Cranberries, Frozen 25 0 0.015 ^ 0.5

Cucumbers 731 0 0.050 ^ 0.02

Grapefruit 704 0 0.005 - 0.030 0.02

Grapes 708 0 0.050 ^ 0.02

Green Beans 567 51 9 0.031 - 1.7 0.030 ^ 3.0

Lettuce 756 39 5.2 0.003 - 0.14 0.003 ^ 10

Olives, Canned 189 0 0.005 ^ 0.02

Oranges 708 0 0.050 ^ 0.02

Pears 707 0 0.050 ^ 0.02

Potatoes 708 0 0.002 - 0.005 0.02

Spinach 707 0 0.005 - 0.15 0.02

Strawberries 530 0 0.005 ^ 0.02

Sweet Potatoes 532 0 0.15 ^ 0.02

APPENDIX B. DISTRIBUTION OF RESIDUES BY PESTICIDE IN FRUIT AND VEGETABLES
Appendix B. Page 2 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 528 1 0.2 0.023 ^ 0.002 - 0.010 0.02

Tomatoes, Canned 189 0 0.002 ^ 0.02

TOTAL 9,340 91

Acetamiprid (insecticide) 

Apples 531 173 32.6 0.002 - 0.18 0.002 ^ 1.0

Applesauce 190 150 78.9 0.002 - 0.079 0.002 ^ 1.0

Cherries 30 18 60 0.003 - 0.13 0.002 ^ 1.20

Cherries, Frozen 144 92 63.9 0.002 - 0.10 0.002 ^ 1.20

Cranberries 156 0 0.002 ^ 1.6

Cranberries, Frozen 25 0 0.002 ^ 1.6

Cucumbers 754 24 3.2 0.010 - 0.070 0.010 ^ 0.50

Grapefruit 704 5 0.7 0.001 - 0.012 0.001 - 0.002 1.0

Grapes 708 63 8.9 0.017 - 2.1 0.010 ^ X - 4 0.35

Green Beans 567 8 1.4 0.002 - 0.17 0.002 ^ 0.60

Lettuce 756 29 3.8 0.002 - 0.23 0.002 ^ 3.00

Olives, Canned 189 0 0.001 ^ 0.01

Oranges 708 5 0.7 0.011 - 0.014 0.010 ^ 1.0

Pears 706 102 14.4 0.017 - 0.35 0.010 ^ 1.0

Potatoes 708 0 0.001 ^ 0.01

Spinach 707 64 9.1 0.002 - 1.3 0.001 - 0.005 3.00

Strawberries 530 158 29.8 0.001 - 0.89 0.001 ^ X - 1 0.60

Sweet Potatoes 532 0 0.005 ^ 0.01

Tomatoes 528 47 8.9 0.002 - 0.076 0.001 ^ 0.20

Tomatoes, Canned 189 2 1.1 0.002 ^ 0.001 ^ 0.20

TOTAL 9,362 940

Acetochlor (herbicide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cranberries 156 0 0.030 ^ NT

Cranberries, Frozen 25 0 0.030 ^ NT

Grapefruit 704 0 0.005 ^ NT

Green Beans 567 0 0.005 ^ NT

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.050 ^ NT

TOTAL 4,180 0

Acibenzolar S methyl (plant activator) 

Apples 531 0 0.020 ^ 0.03

Applesauce 190 0 0.020 ^ 0.03

Cranberries 156 0 0.030 ^ 0.15

Cranberries, Frozen 25 0 0.030 ^ 0.15

Grapefruit 346 0 0.005 ^ 0.02

Green Beans 567 0 0.020 ^ NT

Lettuce 756 0 0.020 ^ 0.25

Pears 707 0 0.015 ^ 0.03

Potatoes 708 0 0.004 - 0.012 NT

Spinach 707 0 0.004 - 0.040 1.0

Sweet Potatoes 266 0 0.040 ^ NT

Tomatoes 528 0 0.004 - 0.012 1.0

Tomatoes, Canned 189 0 0.004 - 0.012 1.0

TOTAL 5,676 0
Appendix B. Page 3 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Acifluorfen (herbicide) 

Grapefruit 358 0 0.050 ^ NT

Olives, Canned 189 0 0.050 ^ NT

Strawberries 530 0 0.050 ^ 0.05

TOTAL 1,077 0

Alachlor (herbicide) 

Cranberries 156 0 0.020 ^ NT

Cranberries, Frozen 25 0 0.020 ^ NT

Grapefruit 704 0 0.010 - 0.020 NT

Green Beans 567 0 0.020 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 3,954 0

Aldicarb (insecticide) 

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.005 0.3

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ 0.3

Potatoes 708 0 0.001 ^ 1

Spinach 707 0 0.003 - 0.020 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.020 ^ 0.1

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 5,904 0

Aldicarb sulfone (metabolite of Aldicarb)

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.025 ^ NT

Cherries, Frozen 144 0 0.025 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.003 - 0.020 0.3

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 0.3

Potatoes 708 0 0.003 ^ 1

Spinach 707 0 0.003 - 0.025 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.025 ^ 0.1

Tomatoes 528 0 0.003 - 0.010 NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 7,381 0
Appendix B. Page 4 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Aldicarb sulfoxide (metabolite of Aldicarb)

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.051 ^ NT

Cherries, Frozen 144 0 0.051 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ 0.3

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 0.3

Potatoes 708 0 0.002 - 0.006 1

Spinach 707 0 0.002 - 0.055 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.055 ^ 0.1

Tomatoes 528 0 0.002 - 0.006 NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,854 0

Allethrin (insecticide) 

Cherries 30 0 0.080 ^ NT

Cherries, Frozen 144 0 0.080 ^ NT

Cucumbers 754 0 0.020 - 0.040 NT

Grapefruit 704 0 0.010 - 0.050 NT

Grapes 708 0 0.030 ^ NT

Green Beans 567 0 0.050 ^ EX

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.020 - 0.040 NT

Spinach 349 0 0.085 ^ NT

Strawberries 530 0 0.010 ^ EX

Sweet Potatoes 532 0 0.080 ^ NT

TOTAL 5,215 0

Ametoctradin (fungicide) 

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Grapefruit 704 1 0.1 0.017 ^ 0.001 ^ V - 1 NT

Green Beans 567 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.05

Spinach 358 214 59.8 0.002 - 13 0.001 ^ 50.0

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 14 2.7 0.002 - 0.011 0.001 ^ 1.5

Tomatoes, Canned 189 0 0.001 ^ 1.5

TOTAL 3,954 230

Ametryn (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.005 NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 3,066 0
Appendix B. Page 5 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Amicarbazone (herbicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Asulam (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Atrazine (herbicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.005 NT

Lettuce 756 1 0.1 0.004 ^ 0.002 ^ 0.25

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 6 0.8 0.002 ^ 0.001 ^ 0.25

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.001 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,207 7

Azinphos (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Azinphos methyl (insecticide) 

Apples 531 0 0.010 ^ 1.5

Applesauce 190 0 0.010 ^ 1.5

Cherries 30 0 0.004 - 0.008 2.0

Cherries, Frozen 144 0 0.004 - 0.008 2.0

Cranberries 156 0 0.010 ^ 0.5

Cranberries, Frozen 25 0 0.010 ^ 0.5

Cucumbers 754 0 0.020 ^ NT

Grapefruit 704 0 0.005 - 0.020 NT

Grapes 708 0 0.015 ^ NT

Green Beans 567 0 0.020 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.020 ^ NT

Pears 707 2 0.3 0.025 ^ 0.015 ^ 1.5

Potatoes 708 0 0.012 ^ NT

Spinach 707 0 0.005 - 0.012 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT
Appendix B. Page 6 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 528 0 0.012 ^ NT

Tomatoes, Canned 189 0 0.012 ^ NT

TOTAL 9,363 2

Azinphos methyl oxygen analog (metabolite of Azinphos methyl)

Apples 531 0 0.010 ^ 1.5

Applesauce 190 0 0.010 ^ 1.5

Cherries 30 0 0.003 ^ 2.0

Cherries, Frozen 144 0 0.003 ^ 2.0

Cranberries 156 0 0.015 ^ 0.5

Cranberries, Frozen 25 0 0.015 ^ 0.5

Grapefruit 704 0 0.003 - 0.015 NT

Grapes 708 0 0.003 ^ NT

Green Beans 567 0 0.003 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Pears 707 1 0.1 0.005 ^ 0.003 ^ 1.5

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 6,118 1

Azoxystrobin (fungicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.005 ^ 2.0

Cherries, Frozen 144 3 2.1 0.012 - 0.14 0.005 ^ 1.5

Cranberries 156 35 22.4 0.001 - 0.008 0.001 ^ 5.0

Cranberries, Frozen 25 1 4 0.001 ^ 0.001 ^ 5.0

Cucumbers 754 110 14.6 0.002 - 0.039 0.002 ^ 0.3

Grapefruit 704 1 0.1 0.013 ^ 0.001 - 0.010 15.0

Grapes 708 32 4.5 0.005 - 0.048 0.003 ^ 2.0

Green Beans 567 150 26.5 0.001 - 0.47 0.001 ^ 3.0

Lettuce 756 8 1.1 0.002 - 0.16 0.002 ^ 30.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 2 0.3 0.004 - 0.022 0.002 ^ 15.0

Potatoes 708 197 27.8 0.002 - 1.2 0.001 ^ 8.0

Spinach 707 37 5.2 0.002 - 4.4 0.001 - 0.010 30.0

Strawberries 530 88 16.6 0.001 - 0.64 0.001 ^ 10.0

Sweet Potatoes 532 0 0.010 ^ 8.0

Tomatoes 528 124 23.5 0.002 - 0.045 0.001 ^ 0.2

Tomatoes, Canned 189 30 15.9 0.002 - 0.012 0.001 ^ 0.2

TOTAL 8,656 818

Benalaxyl (fungicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Benazolin (herbicide) 

Grapefruit 358 0 0.050 ^ NT

Olives, Canned 189 0 0.050 ^ NT

Strawberries 530 0 0.050 ^ NT

TOTAL 1,077 0
Appendix B. Page 7 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Bendiocarb (insecticide) 

Apples 531 0 0.003 ^ SU

Applesauce 190 0 0.003 ^ SU

Cherries 30 0 0.010 ^ SU

Cherries, Frozen 144 0 0.010 ^ SU

Cranberries 156 0 0.002 ^ SU

Cranberries, Frozen 25 0 0.002 ^ SU

Cucumbers 754 0 0.005 ^ SU

Grapefruit 704 0 0.001 - 0.015 SU

Grapes 708 0 0.003 ^ SU

Green Beans 567 0 0.015 ^ SU

Lettuce 756 0 0.003 ^ SU

Olives, Canned 189 0 0.001 ^ SU

Oranges 708 0 0.005 ^ SU

Pears 707 0 0.003 ^ SU

Potatoes 708 0 0.001 ^ SU

Spinach 707 0 0.001 - 0.010 SU

Strawberries 530 0 0.001 ^ SU

Sweet Potatoes 532 0 0.010 ^ SU

Tomatoes 528 0 0.001 ^ SU

Tomatoes, Canned 189 0 0.001 ^ SU

TOTAL 9,363 0

Benfluralin (herbicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Lettuce 756 0 0.010 ^ 0.05

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 2,554 0

Benoxacor (herbicide safener) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.012 ^ NT

Cherries, Frozen 144 0 0.012 ^ NT

Cranberries 156 0 0.020 ^ 0.01

Cranberries, Frozen 25 0 0.020 ^ 0.01

Grapefruit 704 0 0.003 - 0.020 NT

Green Beans 567 0 0.020 ^ 0.01

Lettuce 756 0 0.010 ^ 0.01

Olives, Canned 189 0 0.003 ^ NT

Potatoes 708 0 0.001 ^ 0.01

Spinach 707 0 0.001 - 0.015 0.01

Strawberries 530 0 0.003 ^ 0.01

Sweet Potatoes 532 0 0.015 ^ 0.01

Tomatoes 528 0 0.001 ^ 0.01

Tomatoes, Canned 189 0 0.001 ^ 0.01

TOTAL 6,486 0

Bensulide (herbicide) 

Apples 531 0 0.004 ^ NT

Applesauce 190 0 0.004 ^ NT
Appendix B. Page 8 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.005 - 0.015 NT

Green Beans 567 0 0.015 ^ NT

Lettuce 756 2 0.3 0.005 ^ 0.004 ^ 0.15

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 3,467 2

Bensulide oxygen analog (metabolite of Bensulide)

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Grapefruit 346 0 0.002 ^ NT

Green Beans 567 0 0.002 ^ NT

Lettuce 756 15 2 0.002 - 0.009 0.002 ^ 0.15

TOTAL 2,571 15

Bentazon (herbicide) 

Cherries 30 0 0.030 ^ NT

Cherries, Frozen 144 0 0.030 ^ NT

Cranberries 156 0 0.050 ^ NT

Cranberries, Frozen 25 0 0.050 ^ NT

Grapefruit 704 0 0.003 - 0.10 NT

Green Beans 567 0 0.10 ^ 0.5

Olives, Canned 189 0 0.003 ^ NT

Spinach 349 0 0.030 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.030 ^ NT

TOTAL 3,226 0

Benthiavalicarb isopropyl (fungicide) 

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Spinach 349 0 0.010 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 1,055 0

Bifenazate (acaricide) 

Cherries 30 0 0.005 ^ 2.5

Cherries, Frozen 144 0 0.005 ^ 2.5

Grapefruit 358 0 0.003 ^ NT

Grapes 708 3 0.4 0.017 ^ 0.010 ^ 0.75

Olives, Canned 189 0 0.003 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 109 20.6 0.003 - 0.93 0.003 ^ 1.5

Sweet Potatoes 532 0 0.005 ^ 0.10

TOTAL 2,840 112

Bifenox (herbicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0
Appendix B. Page 9 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Bifenthrin (insecticide) 

Apples 531 3 0.6 0.039 - 0.060 0.002 ^ 0.5

Applesauce 190 2 1.1 0.002 ^ 0.002 ^ 0.5

Cherries 30 0 0.008 ^ 0.05

Cherries, Frozen 144 0 0.008 ^ 0.05

Cranberries 156 0 0.005 ^ 1.8

Cranberries, Frozen 25 0 0.005 ^ 1.8

Cucumbers 754 74 9.8 0.005 - 0.085 0.005 ^ 0.4

Grapefruit 704 0 0.003 - 0.040 0.05

Grapes 708 28 4 0.002 - 0.099 0.001 ^ 0.2

Green Beans 567 45 7.9 0.040 - 0.19 0.040 ^ 0.6

Lettuce 756 11 1.5 0.002 - 0.17 0.002 ^ 3.0

Olives, Canned 189 0 0.003 ^ 0.05

Oranges 708 0 0.005 ^ 0.05

Pears 707 2 0.3 0.002 - 0.005 0.001 ^ 0.5

Potatoes 708 27 3.8 0.002 - 0.008 0.001 ^ 0.05

Spinach 707 51 7.2 0.002 - 1.3 0.001 - 0.010 X - 3 0.2

Strawberries 530 135 25.5 0.003 - 0.29 0.003 ^ 3.0

Sweet Potatoes 532 4 0.8 0.019 - 0.088 0.010 ^ X - 2 0.05

Tomatoes 528 84 15.9 0.002 - 0.069 0.001 ^ 0.15

Tomatoes, Canned 189 32 16.9 0.002 - 0.015 0.001 ^ 0.15

TOTAL 9,363 498

Biphenyl (fungicide) 

Spinach 349 0 0.075 ^ NT

Sweet Potatoes 532 0 0.075 ^ NT

TOTAL 881 0

Bitertanol (fungicide) 

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 0 0.002 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 3,246 0

Boscalid (fungicide) 

Apples 531 121 22.8 0.003 - 0.21 0.003 ^ 3.0

Applesauce 190 17 8.9 0.004 - 0.026 0.003 ^ 3.0

Cherries 30 1 3.3 0.025 ^ 0.013 ^ 3.5

Cherries, Frozen 144 53 36.8 0.013 - 0.35 0.013 ^ 3.5

Cranberries 156 0 0.005 ^ 13.0

Cranberries, Frozen 25 0 0.005 ^ 13.0

Cucumbers 754 46 6.1 0.011 - 0.098 0.010 ^ 0.5

Grapefruit 704 0 0.003 - 0.005 2.0

Grapes 708 421 59.5 0.008 - 1.2 0.005 ^ 5.0

Green Beans 567 63 11.1 0.005 - 0.54 0.005 ^ 1.6

Lettuce 756 52 6.9 0.003 - 0.063 0.003 ^ 11.0

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 2.0

Pears 707 159 22.5 0.008 - 0.24 0.005 ^ 3.0

Potatoes 708 138 19.5 0.003 - 0.034 0.002 ^ 0.05

Spinach 707 136 19.2 0.003 - 0.14 0.002 - 0.015 60

Strawberries 530 288 54.3 0.003 - 1.2 0.003 ^ 4.5
Appendix B. Page 10 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 532 0 0.015 ^ 0.05

Tomatoes 528 147 27.8 0.003 - 0.089 0.002 ^ 3.0

Tomatoes, Canned 189 0 0.002 ^ 3.0

TOTAL 9,363 1,642

Bromacil (herbicide) 

Apples 531 0 0.003 ^ NT

Applesauce 190 0 0.003 ^ NT

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.005 - 0.010 0.1

Lettuce 756 0 0.003 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Spinach 349 0 0.020 ^ NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.020 ^ NT

TOTAL 4,136 0

Bromopropylate (acaricide) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 2,539 0

Bromoxynil (herbicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Bromuconazole (fungicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Bupirimate (fungicide) 

Cherries 30 0 0.002 ^ NT

Cherries, Frozen 144 0 0.002 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,594 0

Buprofezin (insecticide) 

Apples 531 4 0.8 0.005 - 0.52 0.001 ^ 3.0

Applesauce 190 2 1.1 0.001 - 0.002 0.001 ^ 3.0
Appendix B. Page 11 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries 30 4 13.3 0.002 - 0.042 0.001 ^ 1.9

Cherries, Frozen 144 21 14.6 0.001 - 0.022 0.001 ^ 1.9

Cranberries 156 0 0.001 ^ 2.5

Cranberries, Frozen 25 0 0.001 ^ 2.5

Cucumbers 754 7 0.9 0.010 - 0.014 0.010 ^ 0.50

Grapefruit 704 2 0.3 0.002 - 0.004 0.001 ^ 2.5

Grapes 707 74 10.5 0.005 - 0.30 0.003 ^ 2.5

Green Beans 567 7 1.2 0.001 - 0.018 0.001 ^ 0.02

Lettuce 756 2 0.3 0.002 - 0.005 0.001 ^ 35

Olives, Canned 189 27 14.3 0.001 - 0.073 0.001 ^ 3.5

Oranges 708 0 0.010 ^ 2.5

Pears 707 30 4.2 0.005 - 0.29 0.003 ^ 6.0

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 ^ 35

Strawberries 530 7 1.3 0.002 - 0.38 0.001 ^ 2.5

Sweet Potatoes 532 0 0.001 ^ NT

Tomatoes 528 33 6.2 0.002 - 0.13 0.001 ^ 2.0

Tomatoes, Canned 189 0 0.001 ^ 2.0

TOTAL 9,362 220

Butocarboxim (insecticide, acaricide)

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cucumbers 754 0 0.010 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.010 - 0.020 NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 2,517 0

Butocarboxim sulfone (metabolite of Butocarboxim)

Cherries 30 0 0.011 ^ NT

Cherries, Frozen 144 0 0.011 ^ NT

Spinach 349 0 0.015 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

TOTAL 1,055 0

Butocarboxim sulfoxide (metabolite of Butocarboxim)

Cherries 30 0 0.006 ^ NT

Cherries, Frozen 144 0 0.006 ^ NT

Spinach 349 0 0.010 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 1,055 0

Butylate (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Cadusafos (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0
Appendix B. Page 12 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Captan (fungicide) (parent of THPI)

Cucumbers 610 0 0.020 ^ 0.05

Grapes 708 3 0.4 0.083 - 1.5 0.050 ^ 25.0

Oranges 708 0 0.020 ^ NT

Pears 707 28 4 0.083 - 0.93 0.050 ^ 25.0

TOTAL 2,733 31

Carbaryl (insecticide) 

Apples 531 5 0.9 0.004 - 0.58 0.003 ^ 12

Applesauce 190 3 1.6 0.008 - 0.053 0.003 ^ 12

Cherries 30 0 0.003 ^ 10

Cherries, Frozen 144 17 11.8 0.004 - 0.69 0.003 ^ 10

Cranberries 156 0 0.002 ^ 3.0

Cranberries, Frozen 25 0 0.002 ^ 3.0

Cucumbers 754 1 0.1 0.023 ^ 0.010 ^ 3.0

Grapefruit 704 4 0.6 0.003 - 0.004 0.002 - 0.003 10

Grapes 708 0 0.004 ^ 10

Green Beans 567 5 0.9 0.006 - 0.21 0.002 ^ 10

Lettuce 756 1 0.1 0.052 ^ 0.003 ^ 10

Olives, Canned 189 0 0.003 ^ 10

Oranges 708 12 1.7 0.012 - 0.043 0.010 ^ 10

Pears 707 0 0.004 ^ 12

Potatoes 708 0 0.001 ^ 2.0

Spinach 707 0 0.001 - 0.005 22

Strawberries 530 1 0.2 0.014 ^ 0.003 ^ 4.0

Sweet Potatoes 532 0 0.005 ^ 0.2

Tomatoes 528 0 0.001 - 0.003 5.0

Tomatoes, Canned 189 0 0.003 ^ 5.0

TOTAL 9,363 49

Carbendazim - MBC (fungicide) (metabolite of Benomyl and Thiophanate Methyl)

Apples 531 75 14.1 0.001 - 0.11 0.001 ^ 2.0

Applesauce 190 133 70 0.001 - 0.076 0.001 ^ 2.0

Cherries 30 1 3.3 0.022 ^ 0.005 ^ 20.0

Cherries, Frozen 144 30 20.8 0.005 - 0.58 0.005 ^ 20.0

Cucumbers 754 57 7.6 0.010 - 0.082 0.010 ^ 1.0

Grapefruit 358 0 0.001 ^ NT

Grapes 708 1 0.1 0.017 ^ 0.010 ^ 5.0

Lettuce 756 0 0.001 ^ NT

Olives, Canned 189 4 2.1 0.002 ^ 0.001 ^ V - 4 NT

Oranges 708 0 0.010 ^ NT

Pears 707 182 25.7 0.017 - 0.15 0.010 ^ 3.0

Spinach 707 1 0.1 0.004 ^ 0.001 - 0.010 V - 1 NT

Strawberries 530 68 12.8 0.002 - 0.26 0.001 ^ 7.0

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 509 5 1 0.002 - 0.028 0.001 ^ V - 5 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,542 557

Carbofuran (insecticide) (parent of 3-Hydroxycarbofuran)

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.006 - 0.012 NT

Cherries, Frozen 144 0 0.006 - 0.012 NT

Cranberries 156 0 0.002 ^ NT
Appendix B. Page 13 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 ^ NT

Grapes 708 0 0.001 ^ NT

Green Beans 567 3 0.5 0.002 - 0.012 0.001 ^ V - 3 NT

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 0 0.001 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 9,363 3

Carbophenothion (insecticide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 2,860 0

Carboxin (fungicide) 

Cranberries 156 0 0.025 ^ NT

Cranberries, Frozen 25 0 0.025 ^ NT

Grapefruit 704 0 0.003 - 0.050 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 503 0 0.003 ^ NT

TOTAL 1,577 0

Carfentrazone (herbicide) 

Apples 531 0 0.005 ^ 0.10

Applesauce 190 0 0.005 ^ 0.10

Cherries 30 0 0.016 ^ 0.10

Cherries, Frozen 144 0 0.016 ^ 0.10

Cranberries 156 0 0.005 ^ 0.10

Cranberries, Frozen 25 0 0.005 ^ 0.10

Cucumbers 754 0 0.005 ^ 0.10

Grapefruit 704 0 0.003 - 0.005 0.10

Grapes 708 0 0.002 ^ 0.10

Green Beans 567 0 0.005 ^ 0.10

Lettuce 756 0 0.005 ^ 0.10

Olives, Canned 189 0 0.003 ^ 0.10

Oranges 708 0 0.005 ^ 0.10

Pears 707 0 0.002 ^ 0.10

Potatoes 708 0 0.005 - 0.015 0.10

Spinach 707 0 0.005 - 0.020 0.10

Strawberries 530 0 0.003 ^ 0.10

Sweet Potatoes 532 0 0.020 ^ 0.10
Appendix B. Page 14 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 508 0 0.005 - 0.015 0.10

Tomatoes, Canned 189 0 0.005 ^ 0.10

TOTAL 9,343 0

Chlorantraniliprole (insecticide) 

Apples 531 134 25.2 0.010 - 0.076 0.010 ^ 1.2

Applesauce 190 2 1.1 0.011 - 0.015 0.010 ^ 1.2

Cranberries 156 11 7.1 0.005 - 0.014 0.005 ^ 2.5

Cranberries, Frozen 25 0 0.005 ^ 2.5

Cucumbers 754 2 0.3 0.025 - 0.033 0.020 ^ 0.5

Grapefruit 704 0 0.001 - 0.005 1.4

Grapes 708 65 9.2 0.025 - 0.069 0.015 ^ 2.5

Green Beans 567 65 11.5 0.001 - 0.051 0.001 ^ 2.0

Lettuce 756 20 2.6 0.010 - 0.35 0.010 ^ 13

Olives, Canned 189 0 0.005 ^ 4.0

Oranges 708 0 0.020 ^ 1.4

Pears 706 91 12.9 0.025 - 0.083 0.015 ^ 1.2

Potatoes 708 2 0.3 0.003 ^ 0.002 - 0.005 0.30

Spinach 707 232 32.8 0.003 - 9.3 0.002 - 0.010 13

Strawberries 530 53 10 0.005 - 0.16 0.005 ^ 1.0

Sweet Potatoes 532 0 0.010 ^ 0.30

Tomatoes 528 114 21.6 0.003 - 0.056 0.002 ^ 1.4

Tomatoes, Canned 189 2 1.1 0.003 ^ 0.002 - 0.005 1.4

TOTAL 9,188 793

Chlorethoxyfos (insecticide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.020 NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,604 0

Chlorfenapyr (insecticide) 

Apples 531 0 0.015 ^ 0.01

Applesauce 190 0 0.015 ^ 0.01

Cherries 30 0 0.040 ^ 0.01

Cherries, Frozen 144 0 0.040 ^ 0.01

Cranberries 156 0 0.025 ^ 0.01

Cranberries, Frozen 25 0 0.025 ^ 0.01

Cucumbers 754 26 3.4 0.005 - 0.051 0.005 ^ X - 11 0.01

Grapefruit 704 0 0.025 - 0.25 0.01

Grapes 708 0 0.050 ^ 0.01

Green Beans 567 1 0.2 0.060 ^ 0.025 ^ X - 1 0.01

Lettuce 756 0 0.015 ^ 0.01

Olives, Canned 189 0 0.25 ^ 0.01

Oranges 708 0 0.005 ^ 0.01

Pears 707 0 0.050 ^ 0.01

Potatoes 708 0 0.002 ^ 0.01

Spinach 707 0 0.002 - 0.040 0.01

Strawberries 530 0 0.25 ^ 0.01

Sweet Potatoes 532 0 0.040 ^ 0.01

Tomatoes 528 21 4 0.004 - 0.098 0.002 ^ 1.0

Tomatoes, Canned 189 0 0.002 ^ 1.0

TOTAL 9,363 48
Appendix B. Page 15 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Chlorfenvinphos (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.004 ^ NT

Spinach 358 0 0.004 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.004 ^ NT

Tomatoes, Canned 189 0 0.004 ^ NT

TOTAL 2,860 0

Chlorimuron ethyl (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,258 0

Chlorobenzilate (acaricide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Chloroneb (fungicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Chlorothalonil (fungicide) 

Cucumbers 754 105 13.9 0.005 - 0.30 0.005 ^ 5.0

Grapefruit 269 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Strawberries 472 1 0.2 0.053 ^ 0.005 ^ V - 1 NT

TOTAL 2,203 106

Chlorpropham (herbicide, growth regulator)

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 1 0.6 0.007 ^ 0.005 ^ V - 1 NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 7 0.9 0.005 - 0.014 0.005 ^ V - 7 NT

Grapefruit 704 0 0.003 - 0.005 NT

Green Beans 567 0 0.020 ^ NT

Lettuce 756 0 0.020 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 705 99.6 0.002 - 10 0.001 - 0.003 30

Spinach 707 1 0.1 0.003 ^ 0.001 - 0.020 V - 1 NT

Strawberries 530 2 0.4 0.003 - 0.009 0.003 ^ V - 2 NT

Sweet Potatoes 532 4 0.8 0.020 - 0.038 0.020 ^ V - 4 NT
Appendix B. Page 16 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 528 43 8.1 0.002 - 0.015 0.001 ^ V - 43 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,948 763

Chlorpyrifos (insecticide) 

Apples 531 0 0.005 ^ 0.1

Applesauce 190 0 0.005 ^ 0.1

Cherries 30 0 0.010 ^ 1.0

Cherries, Frozen 144 1 0.7 0.038 ^ 0.010 ^ 1.0

Cranberries 156 2 1.3 0.019 - 0.034 0.015 ^ 1.0

Cranberries, Frozen 25 0 0.015 ^ 1.0

Cucumbers 754 5 0.7 0.006 - 0.061 0.005 ^ 0.1

Grapefruit 704 0 0.003 - 0.035 1.0

Grapes 708 2 0.3 0.017 ^ 0.010 ^ 0.1

Green Beans 567 0 0.035 ^ 0.1

Lettuce 756 1 0.1 0.006 ^ 0.005 ^ 0.1

Olives, Canned 189 1 0.5 0.003 ^ 0.003 ^ 0.1

Oranges 708 0 0.005 ^ 1.0

Pears 707 3 0.4 0.017 - 0.057 0.010 ^ 0.1

Potatoes 708 0 0.001 ^ 0.1

Spinach 707 6 0.8 0.002 - 0.023 0.001 - 0.010 0.1

Strawberries 530 0 0.003 ^ 0.2

Sweet Potatoes 532 3 0.6 0.012 - 0.015 0.010 ^ 0.1

Tomatoes 528 4 0.8 0.002 ^ 0.001 ^ 0.1

Tomatoes, Canned 189 5 2.6 0.002 - 0.004 0.001 ^ 0.1

TOTAL 9,363 33

Chlorpyrifos oxygen analog (metabolite of Chlorpyrifos)

Apples 531 0 0.002 ^ 0.1

Applesauce 190 0 0.002 ^ 0.1

Cherries 30 0 0.004 ^ 1.0

Cherries, Frozen 144 0 0.004 ^ 1.0

Cranberries 156 0 0.005 ^ 1.0

Cranberries, Frozen 25 0 0.005 ^ 1.0

Cucumbers 754 0 0.010 ^ 0.1

Grapefruit 704 0 0.001 ^ 1.0

Grapes 708 0 0.005 ^ 0.1

Green Beans 567 0 0.001 ^ 0.1

Lettuce 756 0 0.002 ^ 0.1

Olives, Canned 189 0 0.001 ^ 0.1

Oranges 708 0 0.010 ^ 1.0

Pears 707 0 0.005 ^ 0.1

Potatoes 708 0 0.001 ^ 0.1

Spinach 707 0 0.001 - 0.005 0.1

Strawberries 530 0 0.001 ^ 0.2

Sweet Potatoes 532 0 0.005 ^ 0.1

Tomatoes 528 0 0.001 ^ 0.1

Tomatoes, Canned 189 0 0.001 ^ 0.1

TOTAL 9,363 0

Chlorsulfuron (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0
Appendix B. Page 17 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Clethodim (herbicide) 

Cranberries 107 0 0.20 ^ 0.50

Cranberries, Frozen 13 0 0.20 ^ 0.50

Grapefruit 704 0 0.010 - 0.40 NT

Green Beans 567 0 0.40 ^ 3.5

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ 1.0

Spinach 358 0 0.002 ^ 2.0

Strawberries 530 0 0.010 ^ 3.0

Tomatoes 528 0 0.002 ^ 1.0

Tomatoes, Canned 189 0 0.002 ^ 1.0

TOTAL 3,893 0

Clofentezine (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Grapes 708 4 0.6 0.008 - 0.037 0.005 ^ 1.0

Olives, Canned 189 0 0.005 ^ NT

Pears 707 3 0.4 0.008 ^ 0.005 ^ 0.50

Strawberries 530 1 0.2 0.056 ^ 0.005 ^ V - 1 NT

TOTAL 2,492 8

Clomazone (herbicide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.070 ^ NT

Cherries, Frozen 144 0 0.070 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ 0.1

Grapefruit 704 0 0.003 - 0.005 NT

Green Beans 567 0 0.005 ^ 0.05

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.075 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.070 ^ 0.05

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 7,948 0

Clopyralid (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ 4.0

TOTAL 1,077 0

Cloransulam methyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0
Appendix B. Page 18 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Clothianidin (insecticide) (also a metabolite of Thiamethoxam)

Apples 531 1 0.2 0.030 ^ 0.010 ^ 1.0

Applesauce 190 0 0.010 ^ 1.0

Cherries 30 0 0.035 ^ 0.02

Cherries, Frozen 144 0 0.035 ^ 0.02

Cranberries 156 0 0.025 ^ 0.01

Cranberries, Frozen 25 0 0.025 ^ 0.01

Cucumbers 754 1 0.1 0.019 ^ 0.010 ^ 0.06

Grapefruit 704 17 2.4 0.001 - 0.026 0.001 - 0.005 0.07

Grapes 707 32 4.5 0.017 - 0.33 0.010 ^ 0.60

Green Beans 567 5 0.9 0.006 - 0.034 0.005 ^ X - 1 0.02

Lettuce 756 2 0.3 0.012 - 0.026 0.010 ^ 3.0

Olives, Canned 189 0 0.001 ^ 0.02

Oranges 708 0 0.010 ^ 0.07

Pears 707 28 4 0.017 - 0.081 0.010 ^ 1.0

Potatoes 708 94 13.3 0.003 - 0.032 0.002 ^ 0.3

Spinach 707 268 37.9 0.003 - 0.64 0.002 - 0.035 3.0

Strawberries 530 9 1.7 0.001 - 0.004 0.001 ^ 0.30

Sweet Potatoes 532 0 0.035 ^ 0.3

Tomatoes 528 77 14.6 0.003 - 0.064 0.002 - 0.005 0.20

Tomatoes, Canned 189 3 1.6 0.003 ^ 0.002 - 0.005 0.20

TOTAL 9,362 537

Coumaphos (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.002 - 0.005 NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 5,799 0

Coumaphos oxygen analog (metabolite of Coumaphos)

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.008 ^ NT

Spinach 358 0 0.008 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.008 ^ NT

Tomatoes, Canned 189 0 0.008 ^ NT

TOTAL 4,337 0

Crotoxyphos (insecticide, acaricide)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0
Appendix B. Page 19 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Crufomate (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Cyantraniliprole (insecticide) 

Cranberries 156 0 0.005 ^ 4.0

Cranberries, Frozen 25 0 0.005 ^ 4.0

Grapefruit 704 0 0.003 - 0.005 0.70

Olives, Canned 189 0 0.003 ^ NT

Potatoes 708 0 0.004 ^ 0.15

Spinach 707 5 0.7 0.006 - 0.88 0.004 - 0.30 20

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.15 ^ 0.15

Tomatoes 528 5 0.9 0.006 - 0.019 0.004 ^ 2.0

Tomatoes, Canned 189 0 0.004 ^ 2.0

TOTAL 4,268 10

Cyazofamid (fungicide) 

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.010 ^ NT

Grapes 708 0 0.017 ^ 1.5

Green Beans 567 1 0.2 0.017 ^ 0.010 ^ 0.5

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.012 ^ 0.02

Spinach 707 65 9.2 0.020 - 2.0 0.012 - 0.020 10

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 1 0.2 0.054 ^ 0.020 ^ X - 1 0.02

Tomatoes 528 3 0.6 0.020 ^ 0.012 ^ 0.9

Tomatoes, Canned 189 0 0.012 ^ 0.9

TOTAL 5,717 70

Cyclanilide (plant growth regulator) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Cyflufenamid (fungicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 - 0.002 NT

Strawberries 530 47 8.9 0.001 - 0.044 0.001 ^ 0.20

TOTAL 1,077 47

Cyflumetofen (acaricide) 

Cranberries 156 0 0.020 ^ NT

Cranberries, Frozen 25 0 0.020 ^ NT

Grapefruit 704 0 0.003 - 0.20 0.30

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 122 23 0.003 - 0.55 0.003 ^ 0.60

TOTAL 1,604 122
Appendix B. Page 20 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cyfluthrin (insecticide) 

Apples 531 8 1.5 0.004 - 0.029 0.004 ^ 0.5

Applesauce 190 0 0.004 ^ 0.5

Cherries 30 0 0.042 ^ 0.3

Cherries, Frozen 144 0 0.042 ^ 0.3

Cranberries 156 0 0.050 ^ 0.05

Cranberries, Frozen 25 0 0.050 ^ 0.05

Cucumbers 754 2 0.3 0.007 - 0.013 0.005 ^ 0.1

Grapefruit 704 0 0.010 ^ 0.2

Grapes 708 2 0.3 0.033 ^ 0.020 ^ 1.0

Green Beans 535 6 1.1 0.012 - 0.029 0.010 ^ 0.05

Lettuce 756 4 0.5 0.005 - 0.17 0.004 ^ 3.0

Olives, Canned 189 0 0.010 ^ 0.05

Oranges 708 0 0.005 ^ 0.2

Pears 707 0 0.020 ^ 0.5

Potatoes 689 0 0.008 - 0.025 0.01

Spinach 707 31 4.4 0.012 - 0.97 0.008 - 0.045 6.0

Strawberries 530 0 0.010 ^ 0.05

Sweet Potatoes 532 0 0.045 ^ 0.01

Tomatoes 528 3 0.6 0.012 ^ 0.008 ^ 0.20

Tomatoes, Canned 189 0 0.008 - 0.025 0.20

TOTAL 9,312 56

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (insecticide)

Apples 531 27 5.1 0.005 - 0.037 0.005 ^ 0.30

Applesauce 190 0 0.005 ^ 0.30

Cherries 30 4 13.3 0.014 - 0.020 0.012 ^ 0.50

Cherries, Frozen 144 40 27.8 0.012 - 0.088 0.012 ^ 0.50

Cranberries 156 0 0.005 ^ 0.01

Cranberries, Frozen 25 0 0.005 ^ 0.01

Cucumbers 754 11 1.5 0.008 - 0.027 0.008 ^ 0.05

Grapefruit 704 0 0.010 - 0.025 0.01

Green Beans 535 34 6.4 0.008 - 0.15 0.008 ^ 0.20

Lettuce 756 77 10.2 0.005 - 0.59 0.005 ^ 2.0

Olives, Canned 189 0 0.010 ^ 0.01

Oranges 708 0 0.008 ^ 0.01

Potatoes 708 0 0.003 - 0.010 0.02

Spinach 707 23 3.3 0.005 - 0.48 0.003 - 0.015 X - 9 0.01

Strawberries 530 0 0.010 ^ 0.01

Sweet Potatoes 532 0 0.015 ^ 0.02

Tomatoes 528 17 3.2 0.005 - 0.027 0.003 ^ 0.1

Tomatoes, Canned 189 1 0.5 0.005 ^ 0.003 ^ 0.1

TOTAL 7,916 234

Cyhalothrin, Lambda (includes gamma isomer)

Grapes 708 2 0.3 0.003 ^ 0.002 ^ 0.01

Pears 707 33 4.7 0.003 - 0.017 0.002 ^ 0.30

TOTAL 1,415 35

Cymoxanil (fungicide)

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.050 ^ NT
Appendix B. Page 21 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 25 0 0.050 ^ NT

Grapefruit 704 0 0.010 ^ NT

Grapes 708 0 0.025 ^ 0.10

Green Beans 567 0 0.010 ^ NT

Lettuce 756 8 1.1 0.006 - 0.54 0.002 ^ 19

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.003 ^ 0.05

Spinach 707 5 0.7 0.005 - 0.22 0.003 - 0.020 19

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 0 0.003 ^ 0.2

Tomatoes, Canned 189 0 0.003 ^ 0.2

TOTAL 7,194 13

Cypermethrin (insecticide) 

Apples 531 0 0.010 ^ 2

Applesauce 190 0 0.010 ^ 2

Cherries 30 0 0.068 ^ 1

Cherries, Frozen 144 10 6.9 0.073 - 0.16 0.068 ^ 1

Cranberries 156 0 0.050 ^ 0.8

Cranberries, Frozen 25 0 0.050 ^ 0.8

Cucumbers 754 9 1.2 0.010 - 0.041 0.010 ^ 0.2

Grapefruit 704 0 0.020 - 0.025 0.35

Grapes 708 7 1 0.033 - 0.18 0.020 ^ 2

Green Beans 567 23 4.1 0.030 - 0.23 0.030 ^ 0.5

Lettuce 756 19 2.5 0.010 - 0.72 0.010 ^ 10.00

Olives, Canned 189 0 0.020 ^ 0.05

Oranges 708 0 0.010 ^ 0.35

Pears 707 0 0.020 ^ 2

Potatoes 689 0 0.022 - 0.15 0.1

Spinach 707 143 20.2 0.037 - 4.0 0.022 - 0.070 10.00

Strawberries 530 0 0.020 ^ 0.8

Sweet Potatoes 532 0 0.070 ^ 0.1

Tomatoes 528 6 1.1 0.037 ^ 0.022 ^ 0.2

Tomatoes, Canned 189 0 0.022 ^ 0.2

TOTAL 9,344 217

Cyphenothrin (insecticide) 

Apples 531 0 0.015 ^ NT

Applesauce 190 0 0.015 ^ NT

Cherries 30 0 0.058 ^ NT

Cherries, Frozen 144 0 0.058 ^ NT

Cranberries 126 0 0.050 ^ NT

Cranberries, Frozen 23 0 0.050 ^ NT

Grapefruit 704 0 0.010 - 0.050 NT

Grapes 708 0 0.012 ^ NT

Green Beans 567 0 0.050 ^ NT

Lettuce 756 0 0.015 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Pears 707 0 0.012 ^ NT

Spinach 349 0 0.060 ^ NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.060 ^ NT

TOTAL 6,086 0
Appendix B. Page 22 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cyproconazole (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.005 - 0.010 NT

Cherries, Frozen 144 0 0.005 - 0.010 NT

Grapefruit 358 0 0.005 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,609 0

Cyprodinil (fungicide) 

Apples 531 21 4 0.005 - 0.11 0.005 ^ 1.7

Applesauce 190 20 10.5 0.005 - 0.012 0.005 ^ 1.7

Cherries 30 0 0.012 ^ 2.0

Cherries, Frozen 144 0 0.012 ^ 2.0

Cranberries 156 0 0.005 ^ 3.0

Cranberries, Frozen 25 0 0.005 ^ 3.0

Cucumbers 754 45 6 0.005 - 0.055 0.005 ^ 0.70

Grapefruit 704 0 0.005 - 0.055 NT

Grapes 708 295 41.7 0.010 - 1.3 0.006 ^ 3.0

Green Beans 567 2 0.4 0.11 - 0.16 0.055 ^ 0.6

Lettuce 756 2 0.3 0.006 - 0.037 0.005 ^ 50

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.006 ^ 1.7

Spinach 349 0 0.015 ^ 50

Strawberries 530 266 50.2 0.005 - 1.7 0.005 ^ 5.0

Sweet Potatoes 532 0 0.015 ^ NT

TOTAL 7,580 651

Cyprosulfamide (herbicide safener) 

Cranberries 156 0 0.004 ^ NT

Cranberries, Frozen 25 0 0.004 ^ NT

Grapefruit 704 0 0.002 - 0.003 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,604 0

Cyromazine (insect growth regulator) 

Cranberries 156 0 0.050 ^ NT

Cranberries, Frozen 25 0 0.050 ^ NT

Grapefruit 358 0 0.005 ^ NT

Green Beans 567 0 0.10 ^ 2.0

Olives, Canned 189 0 0.005 ^ NT

Potatoes 669 0 0.008 - 0.016 0.8

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.008 ^ 0.5

Tomatoes, Canned 189 0 0.008 ^ 0.5

TOTAL 3,211 0

DCPA (herbicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT
Appendix B. Page 23 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ 1.0

Grapefruit 704 0 0.003 - 0.010 NT

Grapes 708 0 0.001 ^ NT

Green Beans 567 0 0.010 ^ 2.0

Lettuce 756 58 7.7 0.002 - 0.050 0.002 ^ 2.0

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ 2.0

Spinach 707 36 5.1 0.002 - 0.008 0.001 - 0.020 V - 36 NT

Strawberries 530 0 0.003 ^ 2.0

Sweet Potatoes 532 0 0.020 ^ 2.0

Tomatoes 528 0 0.001 ^ 1.0

Tomatoes, Canned 189 0 0.001 ^ 1.0

TOTAL 8,656 94

DEF - Tribufos (herbicide, plant growth regulator)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Deltamethrin (includes parent Tralomethrin) (insecticide) 

Apples 531 0 0.015 ^ 0.2

Applesauce 190 0 0.015 ^ 0.2

Cherries 30 1 3.3 0.15 ^ 0.12 ^ X - 1 0.05

Cherries, Frozen 144 0 0.12 ^ 0.05

Cranberries 156 0 0.050 ^ 0.05

Cranberries, Frozen 25 0 0.050 ^ 0.05

Cucumbers 754 1 0.1 0.011 ^ 0.008 ^ 0.2

Grapefruit 704 0 0.005 - 0.50 0.05

Grapes 708 0 0.015 ^ 0.05

Green Beans 567 0 0.050 ^ 0.05

Lettuce 756 0 0.015 - 0.030 0.05

Olives, Canned 189 0 0.005 ^ 0.05

Oranges 708 0 0.008 ^ 0.05

Pears 707 1 0.1 0.025 ^ 0.015 ^ 0.2

Potatoes 689 0 0.012 - 0.040 0.04

Spinach 707 4 0.6 0.12 - 0.19 0.012 - 0.12 X - 4 0.05

Strawberries 530 0 0.005 ^ 0.05

Sweet Potatoes 532 1 0.2 0.13 ^ 0.12 ^ X - 1 0.04

Tomatoes 528 1 0.2 0.020 ^ 0.012 ^ 0.2

Tomatoes, Canned 189 0 0.012 ^ 0.2

TOTAL 9,344 9

Demeton-O (metabolite of the insecticide Demeton)

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0
Appendix B. Page 24 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Demeton-S (metabolite of Demeton)

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Demeton-S sulfone (metabolite of Demeton-S)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Desmedipham (herbicide) 

Spinach 349 0 0.030 - 0.060 6.0

Sweet Potatoes 532 0 0.030 ^ NT

TOTAL 881 0

Dialifos (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Diazinon (insecticide) 

Apples 531 16 3 0.005 - 0.064 0.005 ^ 0.50

Applesauce 190 0 0.005 ^ 0.50

Cherries 30 0 0.010 ^ 0.20

Cherries, Frozen 144 0 0.010 ^ 0.20

Cranberries 156 8 5.1 0.006 - 0.028 0.005 ^ 0.50

Cranberries, Frozen 25 0 0.005 ^ 0.50

Cucumbers 754 5 0.7 0.002 - 0.022 0.002 ^ 0.75

Grapefruit 704 0 0.001 - 0.005 NT

Grapes 708 0 0.001 ^ 0.75

Green Beans 567 0 0.001 ^ 0.50

Lettuce 756 0 0.005 ^ 0.70

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.002 ^ NT

Pears 707 2 0.3 0.002 ^ 0.001 ^ 0.50

Potatoes 708 0 0.001 ^ 0.10

Spinach 707 0 0.001 - 0.010 0.70

Strawberries 530 1 0.2 0.002 ^ 0.001 ^ 0.50

Sweet Potatoes 532 0 0.010 ^ 0.10

Tomatoes 528 0 0.001 ^ 0.75

Tomatoes, Canned 189 0 0.001 ^ 0.75

TOTAL 9,363 32

Diazinon oxygen analog (metabolite of Diazinon)

Cherries 30 0 0.008 ^ 0.20

Cherries, Frozen 144 0 0.008 ^ 0.20

Cranberries 108 0 0.005 ^ 0.50

Cranberries, Frozen 12 0 0.005 ^ 0.50

Cucumbers 754 0 0.001 ^ 0.75

Grapefruit 704 0 0.001 - 0.005 NT

Grapes 708 0 0.001 ^ 0.75

Green Beans 567 0 0.001 ^ 0.50
Appendix B. Page 25 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.001 ^ NT

Pears 707 0 0.001 ^ 0.50

Potatoes 708 0 0.001 ^ 0.10

Spinach 707 0 0.001 - 0.010 0.70

Strawberries 530 0 0.001 ^ 0.50

Sweet Potatoes 532 0 0.010 ^ 0.10

Tomatoes 528 0 0.001 ^ 0.75

Tomatoes, Canned 189 0 0.001 ^ 0.75

TOTAL 7,825 0

Dicamba (herbicide) 

Grapefruit 268 0 0.25 ^ NT

Strawberries 530 0 0.25 ^ NT

TOTAL 798 0

Dichlobenil (herbicide) 

Apples 531 0 0.010 ^ 0.5

Applesauce 190 0 0.010 ^ 0.5

Cherries 30 0 0.007 ^ 0.15

Cherries, Frozen 144 0 0.007 ^ 0.15

Cranberries 156 0 0.002 ^ 0.15

Cranberries, Frozen 25 0 0.002 ^ 0.15

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 0 0.001 ^ 0.15

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.001 ^ 0.5

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 8,450 0

Dichlofluanid (fungicide, acaricide)

Cherries 30 0 0.17 ^ NT

Cherries, Frozen 144 0 0.17 ^ NT

TOTAL 174 0

Dichlormid (herbicide safener)

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.020 NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,604 0

Dichlorprop (herbicide) 

Grapefruit 358 0 0.050 ^ NT

Olives, Canned 189 0 0.050 ^ NT

Strawberries 530 0 0.050 ^ NT

TOTAL 1,077 0
Appendix B. Page 26 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dichlorvos - DDVP (insecticide) (also a metabolite of Naled)

Apples 531 0 0.020 ^ 0.5

Applesauce 190 0 0.020 ^ 0.5

Cherries 30 0 0.005 ^ 0.5

Cherries, Frozen 144 0 0.005 ^ 0.5

Cranberries 156 0 0.005 ^ 0.5

Cranberries, Frozen 25 0 0.005 ^ 0.5

Cucumbers 754 1 0.1 0.033 ^ 0.010 ^ 0.5

Grapefruit 704 0 0.005 - 0.020 3

Grapes 708 0 0.050 ^ 0.5

Green Beans 567 0 0.060 ^ 0.5

Lettuce 756 0 0.020 ^ 0.5

Olives, Canned 189 0 0.020 ^ 0.5

Oranges 708 0 0.010 ^ 3

Pears 707 0 0.050 ^ 0.5

Potatoes 708 0 0.003 ^ 0.5

Spinach 707 0 0.003 - 0.005 3

Strawberries 530 5 0.9 0.030 - 0.85 0.020 ^ 1

Sweet Potatoes 532 0 0.005 ^ 0.5

TOTAL 8,646 6

Diclofop methyl (herbicide) 

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Lettuce 756 0 0.001 ^ NT

TOTAL 1,477 0

Dicloran (fungicide) 

Apples 531 0 0.016 ^ NT

Applesauce 190 0 0.016 ^ NT

Cherries 30 0 0.020 ^ 20

Cherries, Frozen 144 0 0.020 ^ 20

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 7 0.9 0.008 - 0.033 0.005 ^ 5

Grapefruit 704 0 0.020 - 0.10 NT

Grapes 708 0 0.015 ^ 10

Green Beans 567 38 6.7 0.011 - 15 0.010 ^ 20

Lettuce 756 1 0.1 0.034 ^ 0.016 ^ 10

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ 0.25

Spinach 707 3 0.4 0.004 ^ 0.002 - 0.020 V - 3 NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 148 27.8 0.026 - 3.5 0.020 ^ 10

Tomatoes 528 8 1.5 0.004 - 0.072 0.002 ^ 5

Tomatoes, Canned 189 0 0.002 ^ 5

TOTAL 8,656 205

Diclosulam (herbicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0
Appendix B. Page 27 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dicofol Total (insecticide) 

Grapes 708 0 0.002 ^ 5.0

Green Beans 567 0 0.015 ^ 3.0

Pears 707 0 0.002 ^ 10.0

TOTAL 1,982 0

Dicofol o,p' (isomer of Dicofol) 

Cherries 30 0 0.015 ^ 5.0

Cherries, Frozen 144 0 0.015 ^ 5.0

Grapefruit 358 0 0.005 ^ 6.0

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.015 NT

Strawberries 530 1 0.2 0.005 ^ 0.005 ^ 10.0

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.002 ^ 2.0

Tomatoes, Canned 189 0 0.002 ^ 2.0

TOTAL 3,915 1

Dicofol p,p' (isomer of Dicofol) 

Apples 531 0 0.010 ^ 10.0

Applesauce 190 0 0.010 ^ 10.0

Cherries 30 0 0.024 ^ 5.0

Cherries, Frozen 144 0 0.024 ^ 5.0

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 ^ 6.0

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.025 NT

Strawberries 530 1 0.2 0.037 ^ 0.005 ^ 10.0

Sweet Potatoes 532 0 0.025 ^ NT

Tomatoes 528 0 0.001 ^ 2.0

Tomatoes, Canned 189 0 0.001 ^ 2.0

TOTAL 5,919 1

Dicrotophos (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 2,860 0

Diethofencarb (fungicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Difenoconazole (fungicide) 

Apples 531 2 0.4 0.014 - 0.015 0.010 ^ 5.0

Applesauce 190 0 0.010 ^ 5.0
Appendix B. Page 28 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries 30 0 0.005 ^ 2.5

Cherries, Frozen 144 0 0.005 ^ 2.5

Cranberries 156 0 0.002 ^ 4.0

Cranberries, Frozen 25 0 0.002 ^ 4.0

Cucumbers 754 0 0.005 ^ 0.70

Grapefruit 704 0 0.003 - 0.005 0.60

Grapes 708 100 14.1 0.002 - 0.13 0.001 ^ 4.0

Green Beans 567 3 0.5 0.006 - 0.010 0.005 ^ V - 3 NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ 0.60

Pears 707 11 1.6 0.002 - 0.009 0.001 ^ 5.0

Potatoes 708 81 11.4 0.002 - 1.8 0.001 - 0.003 4.0

Spinach 707 0 0.003 - 0.005 NT

Strawberries 530 5 0.9 0.032 - 0.46 0.003 ^ 2.5

Sweet Potatoes 532 0 0.005 ^ 4.0

Tomatoes 528 108 20.5 0.003 - 0.11 0.001 - 0.003 0.60

Tomatoes, Canned 189 12 6.3 0.004 - 0.017 0.003 ^ 0.60

TOTAL 9,363 322

Diflubenzuron (insecticide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.076 ^ NT

Cherries, Frozen 144 0 0.076 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 1 0.1 0.001 ^ 0.001 - 0.020 3.0

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Pears 707 4 0.6 0.005 - 0.034 0.003 ^ 0.50

Potatoes 708 0 0.002 ^ NT

Spinach 707 2 0.3 0.003 ^ 0.002 - 0.080 V - 2 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.080 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,626 7

Diflufenzopyr (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 346 0 0.001 ^ NT

TOTAL 527 0

Dimethenamid (herbicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.007 ^ NT

Cherries, Frozen 144 0 0.007 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.005 NT

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT
Appendix B. Page 29 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Potatoes 708 0 0.001 ^ 0.01

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ 0.01

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 5,919 0

Dimethoate (insecticide) (parent of Omethoate)

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.005 ^ 2.0

Cherries, Frozen 144 11 7.6 0.005 - 0.052 0.005 ^ 2.0

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 ^ 2.0

Grapes 708 0 0.005 ^ NT

Green Beans 567 54 9.5 0.001 - 0.97 0.001 ^ 2.0

Lettuce 756 1 0.1 0.063 ^ 0.005 ^ 2.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 2.0

Pears 707 0 0.005 ^ 2.0

Potatoes 708 1 0.1 0.004 ^ 0.002 ^ 0.2

Spinach 707 1 0.1 0.010 ^ 0.002 - 0.010 V - 1 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ 2.0

Tomatoes, Canned 189 0 0.002 ^ 2.0

TOTAL 9,363 68

Dimethomorph (fungicide) 

Apples 531 0 0.003 ^ NT

Applesauce 190 0 0.003 ^ NT

Cranberries 156 0 0.020 ^ NT

Cranberries, Frozen 25 0 0.020 ^ NT

Cucumbers 754 10 1.3 0.010 - 0.21 0.010 ^ 0.5

Grapefruit 704 0 0.003 - 0.25 NT

Grapes 708 0 0.007 ^ 3.0

Green Beans 567 1 0.2 0.004 ^ 0.001 ^ V - 1 NT

Lettuce 756 123 16.3 0.003 - 2.9 0.003 ^ 30.0

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 2 0.3 0.002 ^ 0.001 ^ 0.05

Spinach 707 242 34.2 0.002 - 4.4 0.001 - 0.010 30.0

Strawberries 530 0 0.003 ^ 0.90

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 20 3.8 0.002 - 0.021 0.001 ^ 1.5

Tomatoes, Canned 189 4 2.1 0.002 - 0.005 0.001 ^ 1.5

TOTAL 8,482 402

Diniconazole (fungicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0
Appendix B. Page 30 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dinotefuran (insecticide) 

Apples 531 0 0.003 ^ 2.0

Applesauce 190 0 0.003 ^ 2.0

Cherries 30 0 0.015 - 0.030 2.0

Cherries, Frozen 144 0 0.015 - 0.030 2.0

Cranberries 156 0 0.040 ^ 0.2

Cranberries, Frozen 25 0 0.040 ^ 0.2

Cucumbers 754 54 7.2 0.010 - 0.27 0.010 ^ 0.5

Grapefruit 704 0 0.003 - 0.040 0.01

Grapes 708 0 0.050 ^ 0.9

Green Beans 567 1 0.2 0.054 ^ 0.040 ^ X - 1 0.01

Lettuce 756 2 0.3 0.003 - 0.004 0.003 ^ 5.0

Olives, Canned 189 0 0.003 ^ 0.01

Oranges 708 0 0.010 ^ 0.01

Pears 707 0 0.050 ^ 2.0

Potatoes 708 0 0.006 ^ 0.05

Spinach 707 12 1.7 0.010 - 0.25 0.006 - 0.015 5.0

Strawberries 530 1 0.2 0.004 ^ 0.003 ^ 0.01

Sweet Potatoes 532 0 0.015 ^ 0.05

Tomatoes 528 63 11.9 0.010 - 0.14 0.006 ^ 0.7

Tomatoes, Canned 189 0 0.006 ^ 0.7

TOTAL 9,363 133

Dioxacarb (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Dioxathion (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Diphenamid (herbicide) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 - 0.008 NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 4,322 0

Diphenylamine - DPA (plant growth regulator) 

Apples 531 426 80.2 0.002 - 3.8 0.002 ^ 10.0

Applesauce 190 68 35.8 0.002 - 0.050 0.002 ^ 10.0

Cherries 30 0 0.061 ^ NT

Cherries, Frozen 144 0 0.061 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Grapes 708 0 0.004 ^ NT
Appendix B. Page 31 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 76 10.7 0.007 - 1.4 0.004 ^ 5.0

Potatoes 708 0 0.003 ^ NT

Spinach 707 0 0.003 - 0.065 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.065 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 8,269 570

Disulfoton (insecticide) 

Cherries 30 0 0.050 ^ NT

Cherries, Frozen 144 0 0.050 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 - 0.007 NT

Spinach 647 0 0.002 - 0.050 NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.050 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 5,317 0

Disulfoton oxygen analog (metabolite of Disulfoton)

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Cherries 30 0 0.002 ^ NT

Cherries, Frozen 144 0 0.002 ^ NT

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Grapefruit 346 0 0.001 ^ NT

Green Beans 567 0 0.001 ^ 0.75

Lettuce 724 0 0.001 ^ 2

Potatoes 708 0 0.002 ^ NT

Spinach 647 0 0.002 - 0.005 NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 5,317 0

Disulfoton sulfone (metabolite of Disulfoton)

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.020 ^ 2

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ NT
Appendix B. Page 32 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,854 0

Disulfoton sulfone oxygen analog (metabolite of Disulfoton)

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Green Beans 567 0 0.005 ^ 0.75

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.010 NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 3,405 0

Disulfoton sulfoxide (metabolite of Disulfoton)

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Grapefruit 704 0 0.001 ^ NT

Green Beans 567 0 0.001 ^ 0.75

Lettuce 756 0 0.005 ^ 2

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,486 0

Disulfoton sulfoxide oxygen analog (metabolite of Disulfoton)

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Green Beans 567 0 0.001 ^ 0.75

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.010 NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 3,405 0

Diuron (herbicide) 

Apples 531 0 0.002 ^ 0.1

Applesauce 190 0 0.002 ^ 0.1

Cherries 30 0 0.015 ^ NT

Cherries, Frozen 144 0 0.015 ^ NT

Cranberries 156 0 0.010 ^ 0.1

Cranberries, Frozen 25 0 0.010 ^ 0.1
Appendix B. Page 33 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.010 ^ 0.05

Grapes 708 0 0.006 ^ 0.1

Green Beans 567 0 0.010 ^ NT

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.010 ^ 1

Pears 707 0 0.006 ^ 1

Potatoes 708 0 0.008 ^ NT

Spinach 707 0 0.008 - 0.015 NT

Strawberries 530 0 0.010 ^ 0.1

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.008 ^ NT

Tomatoes, Canned 189 0 0.008 ^ NT

TOTAL 7,901 0

DMST (4-dimethylaminosulphotosluidide) (metabolite of Tolyfluanid)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Dodine (fungicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Pears 707 2 0.3 0.033 ^ 0.020 ^ 5.0

Strawberries 530 0 0.010 ^ 5.0

TOTAL 1,784 2

Emamectin (insecticide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Emamectin benzoate 1 (insecticide) 

Apples 531 0 0.010 ^ 0.025

Applesauce 190 0 0.010 ^ 0.025

Lettuce 756 0 0.010 ^ 0.100

Pears 706 0 0.002 ^ 0.025

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ V - 1 NT

Spinach 358 0 0.001 ^ 0.100

Tomatoes 528 0 0.001 ^ 0.020

Tomatoes, Canned 189 0 0.001 ^ 0.020

TOTAL 3,966 1

Endosulfan I (insecticide) 

Apples 502 1 0.2 0.016 ^ 0.010 ^ 1.0

Applesauce 190 0 0.010 ^ 1.0

Cherries 30 0 0.030 ^ 2.0

Cherries, Frozen 144 0 0.030 ^ 2.0

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 0 0.005 ^ 1.0

Grapefruit 704 0 0.010 - 0.020 NT

Grapes 708 0 0.005 ^ NT

Green Beans 567 0 0.012 ^ 2.0
Appendix B. Page 34 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Lettuce 756 0 0.010 ^ 11.0

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.005 ^ 2.0

Potatoes 708 0 0.005 ^ 0.2

Spinach 707 0 0.005 - 0.030 NT

Strawberries 530 0 0.020 ^ 2.0

Sweet Potatoes 532 0 0.030 ^ 0.15

Tomatoes 528 0 0.005 ^ 1.0

Tomatoes, Canned 189 2 1.1 0.008 ^ 0.005 ^ 1.0

TOTAL 9,334 3

Endosulfan II (isomer of Endosulfan)

Apples 531 0 0.015 ^ 1.0

Applesauce 190 0 0.015 ^ 1.0

Cherries 30 0 0.085 ^ 2.0

Cherries, Frozen 144 0 0.085 ^ 2.0

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ 1.0

Grapefruit 704 0 0.005 - 0.010 NT

Grapes 708 0 0.010 ^ NT

Green Beans 567 0 0.003 ^ 2.0

Lettuce 756 0 0.015 ^ 11.0

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.010 ^ 2.0

Potatoes 708 1 0.1 0.002 ^ 0.001 - 0.004 0.2

Spinach 707 0 0.001 - 0.090 NT

Strawberries 530 0 0.010 ^ 2.0

Sweet Potatoes 532 0 0.085 ^ 0.15

Tomatoes 528 1 0.2 0.010 ^ 0.001 ^ 1.0

Tomatoes, Canned 189 4 2.1 0.002 - 0.010 0.001 ^ 1.0

TOTAL 9,363 6

Endosulfan sulfate (metabolite of Endosulfan)

Apples 531 0 0.005 ^ 1.0

Applesauce 190 0 0.005 ^ 1.0

Cherries 30 0 0.040 ^ 2.0

Cherries, Frozen 144 0 0.040 ^ 2.0

Cranberries 156 0 0.015 ^ NT

Cranberries, Frozen 25 0 0.015 ^ NT

Cucumbers 754 17 2.3 0.006 - 0.021 0.005 ^ 1.0

Grapefruit 704 0 0.010 - 0.025 NT

Grapes 708 0 0.003 ^ NT

Green Beans 567 1 0.2 0.031 ^ 0.025 ^ 2.0

Lettuce 756 0 0.005 ^ 11.0

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.003 ^ 2.0

Potatoes 631 1 0.2 0.035 ^ 0.005 - 0.035 0.2

Spinach 707 0 0.018 - 0.045 NT

Strawberries 530 1 0.2 0.020 ^ 0.010 ^ 2.0

Sweet Potatoes 532 0 0.040 ^ 0.15
Appendix B. Page 35 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 528 0 0.005 - 0.018 1.0

Tomatoes, Canned 168 0 0.005 - 0.018 1.0

TOTAL 9,265 20

EPN (insecticide) 

Grapefruit 358 0 0.020 ^ NT

Grapes 708 0 0.005 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Pears 707 0 0.005 ^ NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.040 ^ NT

TOTAL 3,024 0

Epoxiconazole (fungicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

EPTC (herbicide) 

Cherries 30 0 0.035 - 0.070 NT

Cherries, Frozen 144 0 0.035 - 0.070 NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 346 0 0.005 ^ 0.1

Green Beans 535 1 0.2 0.001 ^ 0.001 ^ 0.08

Oranges 708 0 0.010 ^ 0.1

Spinach 349 0 0.040 ^ NT

Sweet Potatoes 532 0 0.035 ^ 0.1

TOTAL 3,579 1

Esfenvalerate+Fenvalerate Total (insecticide) 

Apples 531 1 0.2 0.028 ^ 0.005 ^ 1.0

Applesauce 190 0 0.005 ^ 1.0

Cranberries 156 0 0.050 ^ 0.05

Cranberries, Frozen 25 0 0.050 ^ 0.05

Cucumbers 754 0 0.005 ^ 0.5

Grapefruit 346 0 0.025 ^ 0.05

Green Beans 567 19 3.4 0.023 - 0.12 0.008 ^ 1.0

Lettuce 756 0 0.005 ^ 5.0

Oranges 708 0 0.005 ^ 0.05

Potatoes 669 0 0.002 - 0.008 0.05

Spinach 358 1 0.3 0.016 ^ 0.002 - 0.008 0.05

Tomatoes 528 16 3 0.004 - 0.024 0.002 ^ 0.5

Tomatoes, Canned 189 3 1.6 0.004 ^ 0.002 ^ 0.5

TOTAL 5,777 40

Esfenvalerate (isomer of Fenvalerate)

Cherries 30 0 0.035 ^ 3.0

Cherries, Frozen 144 1 0.7 0.058 ^ 0.035 ^ 3.0

Grapefruit 358 0 0.005 ^ 0.05

Grapes 708 0 0.015 ^ 0.05

Olives, Canned 189 0 0.005 ^ 0.05

Pears 707 1 0.1 0.067 ^ 0.015 ^ 1.0
Appendix B. Page 36 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinach 349 0 0.035 ^ 0.05

Strawberries 530 0 0.005 ^ 0.05

Sweet Potatoes 532 0 0.035 ^ 0.05

TOTAL 3,547 2

Ethalfluralin (herbicide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Grapefruit 704 0 0.010 ^ NT

Green Beans 567 0 0.010 ^ NT

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ 0.05

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,486 0

Ethiofencarb (insecticide) 

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 648 0 0.002 - 0.008 NT

Spinach 358 0 0.002 - 0.008 NT

Strawberries 530 0 0.003 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 - 0.008 NT

TOTAL 4,262 0

Ethiofencarb sulfone (metabolite of Ethiofencarb)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Ethiofencarb sulfoxide (metabolite of Ethiofencarb)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Ethion (insecticide) 

Cherries 30 0 0.014 ^ NT

Cherries, Frozen 144 0 0.014 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT
Appendix B. Page 37 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Potatoes 708 0 0.001 - 0.003 NT

Spinach 707 0 0.001 - 0.015 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.001 - 0.003 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 5,377 0

Ethion mono oxon (metabolite of Ethion)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 2,860 0

Ethiprole (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Ethofumesate (herbicide) 

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 2,132 0

Ethoprop (insecticide) 

Cherries 30 0 0.002 - 0.004 NT

Cherries, Frozen 144 0 0.002 - 0.004 NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ 0.02

Grapefruit 704 0 0.001 ^ NT

Green Beans 567 0 0.001 ^ 0.02

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 1 0.1 0.006 ^ 0.001 ^ 0.02

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ 0.02

Tomatoes 528 0 0.001 - 0.003 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 6,471 1

Ethoxyquin (plant growth regulator) 

Grapes 708 0 0.006 ^ NT

Pears 707 186 26.3 0.010 - 1.5 0.006 ^ 3

TOTAL 1,415 186
Appendix B. Page 38 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Ethylan (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Etofenprox (insecticide) 

Apples 531 0 0.025 ^ 5.0

Applesauce 190 0 0.025 ^ 5.0

Cranberries 156 0 0.010 ^ 5.0

Cranberries, Frozen 25 0 0.010 ^ 5.0

Grapefruit 704 0 0.001 - 0.020 5.0

Grapes 708 1 0.1 0.002 ^ 0.001 ^ 5.0

Lettuce 756 0 0.025 ^ 5.0

Olives, Canned 189 0 0.020 ^ 5.0

Pears 707 0 0.001 ^ 5.0

Potatoes 708 1 0.1 0.017 ^ 0.002 - 0.005 5.0

Spinach 358 2 0.6 0.003 ^ 0.002 ^ 5.0

Strawberries 530 0 0.001 ^ 5.0

Sweet Potatoes 532 0 0.035 ^ 5.0

Tomatoes 528 0 0.002 ^ 5.0

Tomatoes, Canned 189 0 0.002 ^ 5.0

TOTAL 6,811 4

Etoxazole (acaricide) 

Cranberries 156 0 0.001 ^ 0.50

Cranberries, Frozen 25 0 0.001 ^ 0.50

Cucumbers 754 0 0.004 ^ 0.02

Grapefruit 704 0 0.001 ^ NT

Grapes 708 45 6.4 0.002 - 0.074 0.001 ^ 0.50

Green Beans 567 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.004 ^ 0.10

Pears 707 148 20.9 0.002 - 0.050 0.001 ^ 0.20

Potatoes 708 0 0.001 ^ NT

Spinach 358 1 0.3 0.002 ^ 0.001 ^ V - 1 NT

Strawberries 530 26 4.9 0.001 - 0.10 0.001 ^ 0.50

Tomatoes 528 3 0.6 0.002 - 0.003 0.001 ^ 0.20

Tomatoes, Canned 189 0 0.001 ^ 0.20

TOTAL 6,831 223

Etridiazole (fungicide) 

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.040 NT

Green Beans 347 0 0.030 ^ 0.1

Olives, Canned 189 0 0.040 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.010 - 0.020 NT

Strawberries 530 0 0.040 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 4,468 0
Appendix B. Page 39 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Famoxadone (fungicide) 

Apples 531 0 0.025 ^ NT

Applesauce 190 0 0.025 ^ NT

Cranberries 156 0 0.050 ^ NT

Cranberries, Frozen 25 0 0.050 ^ NT

Grapefruit 704 0 0.010 - 0.050 NT

Grapes 708 0 0.015 ^ 2.5

Lettuce 756 6 0.8 0.030 - 0.92 0.025 ^ 25

Olives, Canned 189 0 0.010 ^ NT

Potatoes 669 0 0.008 - 0.015 0.02

Spinach 707 53 7.5 0.004 - 4.8 0.002 - 0.050 50

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.050 ^ NT

Tomatoes 528 43 8.1 0.004 - 0.025 0.002 - 0.008 1.0

Tomatoes, Canned 189 4 2.1 0.004 - 0.013 0.002 - 0.008 1.0

TOTAL 6,414 106

Fenamidone (fungicide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.060 ^ NT

Cherries, Frozen 144 0 0.060 ^ NT

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Cucumbers 754 1 0.1 0.011 ^ 0.010 ^ 0.15

Grapefruit 704 0 0.001 ^ NT

Grapes 708 0 0.002 ^ 1.0

Green Beans 567 0 0.001 ^ 0.80

Lettuce 756 99 13.1 0.005 - 2.5 0.005 ^ 60

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ 0.02

Spinach 707 197 27.9 0.004 - 6.6 0.002 - 0.060 60

Strawberries 530 0 0.001 ^ 0.02

Sweet Potatoes 532 0 0.060 ^ 0.02

Tomatoes 528 11 2.1 0.004 - 0.028 0.002 ^ 1.0

Tomatoes, Canned 189 0 0.002 ^ 1.0

TOTAL 8,656 308

Fenamiphos (insecticide) 

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 0 0.002 ^ 0.1

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.050 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 6,085 0
Appendix B. Page 40 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fenamiphos sulfone (metabolite of Fenamiphos)

Cherries 30 0 0.002 ^ NT

Cherries, Frozen 144 0 0.002 ^ NT

Cucumbers 754 8 1.1 0.005 - 0.026 0.005 ^ V - 8 NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 0 0.005 ^ 0.1

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.004 ^ NT

Spinach 707 0 0.004 - 0.005 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.004 ^ NT

Tomatoes, Canned 189 0 0.004 ^ NT

TOTAL 6,085 8

Fenamiphos sulfoxide (metabolite of Fenamiphos)

Cherries 30 0 0.008 ^ NT

Cherries, Frozen 144 0 0.008 ^ NT

Cucumbers 754 10 1.3 0.010 - 0.081 0.005 ^ V - 10 NT

Grapefruit 358 0 0.003 ^ NT

Grapes 708 1 0.1 0.005 ^ 0.003 ^ 0.1

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.004 ^ NT

Spinach 707 0 0.004 - 0.010 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.004 ^ NT

Tomatoes, Canned 189 0 0.004 ^ NT

TOTAL 6,085 11

Fenarimol (fungicide) 

Cherries 30 0 0.013 ^ 1.0

Cherries, Frozen 144 0 0.013 ^ 1.0

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ 0.20

Grapefruit 704 0 0.003 - 0.005 NT

Grapes 708 4 0.6 0.005 - 0.014 0.003 ^ 0.1

Green Beans 567 0 0.005 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.003 ^ 0.1

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.015 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 7,886 4

Fenazaquin (insecticide, acaricide)

Apples 531 0 0.005 ^ 0.2

Applesauce 190 0 0.005 ^ 0.2
Appendix B. Page 41 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.010 NT

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Pears 707 0 0.001 ^ 0.2

Strawberries 530 1 0.2 0.11 ^ 0.001 ^ V - 1 NT

TOTAL 3,788 1

Fenbuconazole (fungicide) 

Apples 531 7 1.3 0.005 - 0.045 0.005 ^ 0.4

Applesauce 190 1 0.5 0.007 ^ 0.005 ^ 0.4

Cherries 30 5 16.7 0.005 - 0.13 0.005 ^ 1.0

Cherries, Frozen 144 47 32.6 0.005 - 0.78 0.005 ^ 1.0

Cranberries 156 38 24.4 0.001 - 0.009 0.001 ^ 0.5

Cranberries, Frozen 25 0 0.001 ^ 0.5

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.003 1.0

Grapes 708 1 0.1 0.002 ^ 0.001 ^ 1.0

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ 1.0

Potatoes 708 0 0.001 - 0.003 NT

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 8,089 99

Fenbutatin oxide (insecticide, acaricide)

Grapes 708 0 0.010 ^ 5.0

Pears 707 76 10.7 0.017 - 0.39 0.010 ^ 15.0

TOTAL 1,415 76

Fenchlorphos (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Fenhexamid (fungicide) 

Apples 531 0 0.013 ^ NT

Applesauce 190 0 0.013 ^ NT

Cherries 30 9 30 0.011 - 0.10 0.011 ^ 10.0

Cherries, Frozen 144 9 6.2 0.014 - 0.078 0.011 ^ 10.0

Cranberries 156 0 0.010 ^ 5.0

Cranberries, Frozen 25 0 0.010 ^ 5.0

Cucumbers 754 0 0.010 ^ 2.0

Grapefruit 704 0 0.002 - 0.010 NT

Grapes 706 250 35.4 0.008 - 0.69 0.005 ^ 4.0

Green Beans 567 0 0.002 ^ NT

Lettuce 756 0 0.013 ^ 30.0

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.010 ^ NT
Appendix B. Page 42 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pears 707 0 0.005 ^ 10

Potatoes 413 0 0.030 ^ NT

Spinach 692 0 0.009 - 0.015 NT

Strawberries 530 120 22.6 0.010 - 0.97 0.010 ^ 3.0

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.030 ^ 2.0

Tomatoes, Canned 189 0 0.030 ^ 2.0

TOTAL 9,051 388

Fenitrothion (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 2,860 0

Fenobucarb - BPMC (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Fenoxaprop ethyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Fenoxycarb (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Fenpropathrin (insecticide) 

Apples 531 12 2.3 0.022 - 0.14 0.020 ^ 5.0

Applesauce 190 0 0.020 ^ 5.0

Cherries 30 0 0.020 ^ 5.0

Cherries, Frozen 144 40 27.8 0.021 - 1.0 0.020 ^ 5.0

Cranberries 156 0 0.005 ^ 3.0

Cranberries, Frozen 25 0 0.005 ^ 3.0

Cucumbers 754 6 0.8 0.007 - 0.056 0.005 ^ 0.5

Grapefruit 704 0 0.005 - 0.010 2.0

Grapes 708 70 9.9 0.005 - 0.34 0.003 ^ 5.0

Green Beans 567 0 0.050 ^ NT

Lettuce 756 0 0.020 ^ NT

Olives, Canned 189 16 8.5 0.005 - 0.051 0.005 ^ 5.0

Oranges 708 0 0.005 ^ 2.0

Pears 707 9 1.3 0.005 - 0.076 0.003 ^ 5.0

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.020 NT

Strawberries 530 35 6.6 0.005 - 0.62 0.005 ^ 2.0
Appendix B. Page 43 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 14 2.7 0.004 - 0.072 0.002 ^ 1.0

Tomatoes, Canned 189 1 0.5 0.004 ^ 0.002 ^ 1.0

TOTAL 9,363 203

Fenpropidin (fungicide) 

Grapefruit 358 0 0.040 ^ NT

Olives, Canned 189 0 0.040 ^ NT

Strawberries 530 0 0.040 ^ NT

TOTAL 1,077 0

Fenpropimorph (fungicide) 

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 4,016 0

Fenpyrazamine (fungicide) 

Cranberries 156 0 0.001 ^ 5

Cranberries, Frozen 25 0 0.001 ^ 5

Grapefruit 358 0 0.020 ^ NT

Grapes 708 3 0.4 0.005 - 0.025 0.003 ^ 3

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ 3

TOTAL 1,966 3

Fenpyroximate (acaricide) 

Apples 531 1 0.2 0.008 ^ 0.005 ^ 0.30

Applesauce 190 0 0.005 ^ 0.30

Cucumbers 754 1 0.1 0.012 ^ 0.010 ^ 0.40

Grapefruit 358 0 0.001 ^ 0.50

Grapes 708 23 3.2 0.005 - 0.086 0.001 ^ 1.0

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 0.50

Pears 707 137 19.4 0.002 - 0.19 0.001 ^ 0.30

Potatoes 708 0 0.001 - 0.003 0.10

Spinach 358 0 0.003 ^ NT

Strawberries 530 33 6.2 0.002 - 0.15 0.001 ^ 1.0

Tomatoes 528 22 4.2 0.004 - 0.025 0.001 - 0.003 0.20

Tomatoes, Canned 189 0 0.003 ^ 0.20

TOTAL 7,214 217

Fensulfothion (insecticide, fumigant)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0
Appendix B. Page 44 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fenthion (insecticide) 

Cherries 30 0 0.015 ^ NT

Cherries, Frozen 144 0 0.015 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Grapes 708 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.030 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.002 - 0.008 NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,085 0

Fenthion oxygen analog sulfone (metabolite of Fenthion)

Cherries 30 0 0.014 ^ NT

Cherries, Frozen 144 0 0.014 ^ NT

Grapes 708 0 0.015 ^ NT

Spinach 349 0 0.015 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

TOTAL 1,763 0

Fenthion oxygen analog sulfoxide (metabolite of Fenthion)

Cherries 30 0 0.014 ^ NT

Cherries, Frozen 144 0 0.014 ^ NT

Spinach 349 0 0.015 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

TOTAL 1,055 0

Fenthion sulfone (metabolite of Fenthion)

Cherries 30 0 0.12 ^ NT

Cherries, Frozen 144 0 0.12 ^ NT

Grapefruit 358 0 0.020 ^ NT

Grapes 708 0 0.012 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Spinach 349 0 0.12 ^ NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.12 ^ NT

TOTAL 2,840 0

Fenthion sulfoxide (metabolite of Fenthion)

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Grapefruit 358 0 0.020 ^ NT

Grapes 708 0 0.012 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Spinach 349 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.020 ^ NT

TOTAL 2,840 0
Appendix B. Page 45 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fenuron (herbicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Fipronil (insecticide) 

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 14 2 0.003 - 0.010 0.002 ^ 0.03

Spinach 707 0 0.002 - 0.020 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 5,377 14

Fipronil sulfone - MB46136 (metabolite of Fipronil)

Apples 531 0 0.050 ^ NT

Applesauce 190 0 0.050 ^ NT

Grapefruit 358 0 0.003 ^ NT

Lettuce 756 0 0.050 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 2,554 0

Flazasulfuron (herbicide) 

Cranberries 126 0 0.005 ^ NT

Cranberries, Frozen 23 0 0.005 ^ NT

Grapefruit 704 0 0.005 ^ 0.01

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,572 0

Flonicamid (insecticide) 

Apples 531 1 0.2 0.010 ^ 0.006 ^ 0.20

Applesauce 190 0 0.006 ^ 0.20

Cherries 30 0 0.005 ^ 0.60

Cherries, Frozen 144 0 0.005 ^ 0.60

Cranberries 156 0 0.050 ^ 1.5

Cranberries, Frozen 25 0 0.050 ^ 1.5

Cucumbers 754 60 8 0.012 - 0.30 0.010 ^ 1.5

Grapefruit 704 0 0.010 - 0.10 NT

Green Beans 567 0 0.10 ^ NT

Lettuce 756 52 6.9 0.006 - 1.5 0.006 ^ 4.0

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 0 0.020 ^ 0.20

Potatoes 708 3 0.4 0.002 - 0.005 0.001 ^ 0.20

Spinach 707 209 29.6 0.002 - 4.1 0.001 - 0.005 9.0

Strawberries 530 156 29.4 0.010 - 0.61 0.010 ^ 1.5
Appendix B. Page 46 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 532 0 0.005 ^ 0.20

Tomatoes 528 129 24.4 0.002 - 0.23 0.001 ^ 0.40

Tomatoes, Canned 189 0 0.001 ^ 0.40

TOTAL 8,655 610

Fluazifop (herbicide) 

Grapefruit 358 0 0.050 ^ NT

Olives, Canned 189 0 0.050 ^ NT

Strawberries 530 0 0.050 ^ NT

TOTAL 1,077 0

Fluazifop butyl (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.005 0.03

Grapes 708 0 0.001 ^ 0.01

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.001 ^ 1.0

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes C2629 528 1 0.2 0.002 ^ 0.001 ^ V - 1 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 4,095 1

Fluazinam (fungicide) 

Grapefruit 358 0 0.003 ^ NT

Grapes 708 0 0.020 ^ 3.0

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,785 0

Flubendiamide (insecticide) 

Apples 531 27 5.1 0.005 - 0.13 0.004 ^ 1.5

Applesauce 190 50 26.3 0.004 - 0.017 0.004 ^ 1.5

Cranberries 156 0 0.020 ^ NT

Cranberries, Frozen 25 0 0.020 ^ NT

Grapefruit 704 0 0.003 ^ NT

Grapes 708 7 1 0.017 - 0.081 0.010 ^ 1.4

Green Beans 567 10 1.8 0.005 - 0.050 0.003 ^ 0.50

Lettuce 756 13 1.7 0.004 - 0.77 0.004 ^ 11

Olives, Canned 189 0 0.003 ^ NT

Pears 706 5 0.7 0.017 - 0.095 0.010 ^ 1.5

Strawberries 530 9 1.7 0.003 - 0.055 0.003 ^ 1.5

TOTAL 5,062 121

Flucythrinate (insecticide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Fludioxonil (fungicide) 

Apples 531 186 35 0.028 - 2.8 0.025 ^ 5.0

Applesauce 190 19 10 0.025 - 0.12 0.025 ^ 5.0

Cherries 30 18 60 0.050 - 1.2 0.031 - 0.062 5.0
Appendix B. Page 47 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries, Frozen 144 8 5.6 0.037 - 0.71 0.031 - 0.062 5.0

Cranberries 156 0 0.005 ^ 2.0

Cranberries, Frozen 25 0 0.005 ^ 2.0

Cucumbers 754 5 0.7 0.007 - 0.028 0.005 ^ 0.45

Grapefruit 704 3 0.4 0.011 - 0.028 0.010 - 0.020 10

Grapes 708 139 19.6 0.033 - 0.44 0.020 ^ 2.0

Green Beans 567 0 0.050 ^ 0.4

Lettuce 756 1 0.1 0.052 ^ 0.025 ^ 30

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 9 1.3 0.006 - 0.028 0.005 ^ 10

Pears 707 296 41.9 0.033 - 3.9 0.020 ^ 5.0

Potatoes 708 66 9.3 0.020 - 0.93 0.012 - 0.040 6.0

Spinach 707 1 0.1 0.038 ^ 0.012 - 0.040 30

Strawberries 530 192 36.2 0.010 - 0.62 0.010 ^ 3.0

Sweet Potatoes 532 127 23.9 0.067 - 0.70 0.065 ^ 6.0

Tomatoes 528 7 1.3 0.020 - 0.065 0.012 ^ 5.0

Tomatoes, Canned 189 0 0.012 ^ 5.0

TOTAL 9,363 1,077

Flufenacet (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.010 NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,604 0

Flufenoxuron (insecticide) 

Apples 531 0 0.001 ^ 0.50

Applesauce 190 0 0.001 ^ 0.50

Grapefruit 358 0 0.001 ^ NT

Grapes 708 0 0.005 ^ 0.70

Lettuce 567 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Pears 707 0 0.005 ^ 0.50

Strawberries 530 0 0.001 ^ NT

TOTAL 3,780 0

Flufenpyr ethyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Flumetsulam (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Flumiclorac pentyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0
Appendix B. Page 48 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Flumioxazin (herbicide) 

Apples 531 0 0.010 ^ 0.02

Applesauce 190 0 0.010 ^ 0.02

Cherries 30 0 0.010 ^ 0.02

Cherries, Frozen 144 0 0.010 - 0.020 0.02

Grapefruit 704 0 0.020 ^ NT

Grapes 708 0 0.035 ^ 0.02

Green Beans 567 0 0.080 ^ NT

Lettuce 724 0 0.001 - 0.010 NT

Olives, Canned 189 0 0.020 ^ 0.02

Pears 707 0 0.035 ^ 0.02

Potatoes 708 0 0.002 - 0.005 0.02

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.020 ^ 0.07

Sweet Potatoes 502 0 0.050 ^ 0.02

Tomatoes 528 0 0.002 - 0.005 0.02

Tomatoes, Canned 189 0 0.002 ^ 0.02

TOTAL 7,658 0

Fluometuron (herbicide) 

Cranberries 156 0 0.004 ^ NT

Cranberries, Frozen 25 0 0.004 ^ NT

Grapefruit 704 0 0.002 - 0.003 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,604 0

Fluopicolide (fungicide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.013 ^ NT

Cherries, Frozen 144 0 0.013 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 60 8 0.010 - 0.11 0.010 ^ 0.50

Grapefruit 704 0 0.001 - 0.002 NT

Grapes 708 0 0.010 ^ 2.0

Green Beans 567 0 0.002 ^ NT

Lettuce 756 26 3.4 0.005 - 2.6 0.005 ^ 25

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ 0.3

Spinach 707 276 39 0.003 - 6.6 0.002 - 0.015 25

Strawberries 530 7 1.3 0.001 - 0.010 0.001 ^ V - 7 NT

Sweet Potatoes 532 0 0.015 ^ 0.3

Tomatoes 528 26 4.9 0.003 - 0.046 0.002 ^ 1.60

Tomatoes, Canned 189 2 1.1 0.003 - 0.009 0.002 ^ 1.60

TOTAL 8,656 397

Fluopyram (fungicide) 

Apples 531 9 1.7 0.006 - 0.052 0.005 - 0.025 0.80

Applesauce 190 1 0.5 0.006 ^ 0.005 ^ 0.80

Cranberries 156 0 0.002 ^ 7.0

Cranberries, Frozen 25 0 0.002 ^ 7.0

Cucumbers 754 21 2.8 0.012 - 0.061 0.010 ^ 0.60
Appendix B. Page 49 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.001 - 0.002 1.0

Lettuce 756 3 0.4 0.006 - 0.25 0.005 - 0.025 40

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 1.0

Strawberries 530 48 9.1 0.002 - 0.41 0.001 ^ 2.0

Sweet Potatoes 532 0 0.005 ^ 0.10

TOTAL 5,075 82

Fluoxastrobin (fungicide) 

Cherries 30 0 0.013 ^ NT

Cherries, Frozen 144 0 0.013 ^ NT

Cranberries 156 0 0.001 ^ 1.9

Cranberries, Frozen 25 0 0.001 ^ 1.9

Cucumbers 754 15 2 0.003 - 0.043 0.002 ^ 0.50

Grapefruit 704 0 0.001 ^ NT

Green Beans 567 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.002 ^ NT

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.010

Spinach 707 0 0.001 - 0.015 NT

Strawberries 530 1 0.2 0.002 ^ 0.001 ^ 1.9

Sweet Potatoes 532 0 0.015 ^ 0.010

Tomatoes 528 17 3.2 0.002 - 0.019 0.001 ^ 1.0

Tomatoes, Canned 189 0 0.001 ^ 1.0

TOTAL 6,471 34

Flupyradifurone (insecticide) 

Cranberries 156 0 0.005 ^ 4.0

Cranberries, Frozen 25 0 0.005 ^ 4.0

Grapefruit 704 15 2.1 0.001 - 0.003 0.001 - 0.020 3.0

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 84 15.8 0.001 - 0.23 0.001 ^ 1.5

TOTAL 1,604 99

Fluquinconazole (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 2,554 0

Fluridone (herbicide) 

Apples 531 0 0.001 ^ 0.1

Applesauce 190 0 0.001 ^ 0.1

Cherries 30 0 0.002 ^ 0.1

Cherries, Frozen 144 0 0.002 ^ 0.1

Cranberries 156 0 0.002 ^ 0.1

Cranberries, Frozen 25 0 0.002 ^ 0.1

Cucumbers 754 0 0.010 ^ 0.1

Grapefruit 704 0 0.001 ^ 0.1

Grapes 708 0 0.001 ^ 0.1

Green Beans 567 0 0.001 ^ 0.1

Lettuce 756 0 0.001 ^ 0.1
Appendix B. Page 50 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 3 1.6 0.002 ^ 0.001 ^ V - 3 NT

Oranges 708 0 0.010 ^ 0.1

Pears 707 0 0.001 ^ 0.1

Spinach 349 0 0.005 ^ 0.1

Strawberries 530 0 0.001 ^ 0.1

Sweet Potatoes 532 0 0.005 ^ 0.1

TOTAL 7,580 3

Fluroxypyr (herbicide metabolite)

Grapefruit 358 0 0.050 ^ NT

Olives, Canned 189 0 0.050 ^ NT

Strawberries 530 0 0.050 ^ NT

TOTAL 1,077 0

Flusilazole (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.008 ^ NT

Cherries, Frozen 144 0 0.008 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 0 0.001 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 5,779 0

Fluthiacet methyl (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.003 - 0.005 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,604 0

Flutolanil (fungicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 2,554 0

Flutriafol (fungicide) 

Apples 531 3 0.6 0.015 - 0.026 0.010 ^ 0.40

Applesauce 190 0 0.010 ^ 0.40

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Grapefruit 704 0 0.001 - 0.025 NT

Grapes 708 20 2.8 0.003 - 0.29 0.002 ^ 1.5

Lettuce 756 0 0.010 ^ 10
Appendix B. Page 51 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.001 ^ NT

Pears 707 0 0.002 ^ 0.40

Strawberries 530 17 3.2 0.006 - 0.24 0.001 ^ 1.5

TOTAL 4,496 40

Fluvalinate (insecticide) 

Apples 531 0 0.050 ^ NT

Applesauce 190 0 0.050 ^ NT

Cherries 30 0 0.035 ^ NT

Cherries, Frozen 144 0 0.035 ^ NT

Cranberries 156 0 0.050 ^ NT

Cranberries, Frozen 25 0 0.050 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 703 0 0.005 - 0.010 NT

Grapes 708 0 0.005 ^ NT

Green Beans 567 0 0.015 ^ NT

Lettuce 756 0 0.050 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.005 ^ NT

Spinach 349 0 0.035 ^ NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.035 ^ NT

TOTAL 7,579 0

Fluxapyroxad (fungicide) 

Cranberries 156 0 0.005 ^ 7.0

Cranberries, Frozen 25 0 0.005 ^ 7.0

Grapefruit 704 0 0.001 - 0.005 NT

Grapes 708 0 0.005 ^ 2.0

Green Beans 567 16 2.8 0.005 - 0.23 0.005 ^ 2.0

Olives, Canned 189 0 0.001 ^ NT

Pears 707 0 0.005 ^ 0.8

Potatoes 708 9 1.3 0.002 - 0.010 0.001 ^ 0.02

Spinach 358 11 3.1 0.002 - 2.0 0.001 ^ 30

Strawberries 530 170 32.1 0.001 - 0.58 0.001 ^ 4.0

Sweet Potatoes 532 0 0.010 ^ 0.02

Tomatoes 528 41 7.8 0.002 - 0.044 0.001 ^ 0.7

Tomatoes, Canned 189 25 13.2 0.002 - 0.009 0.001 ^ 0.7

TOTAL 5,901 272

Folpet (fungicide) 

Apples 472 0 0.030 ^ 5.0

Applesauce 158 0 0.030 - 0.15 5.0

Cranberries 126 0 0.005 ^ 15.0

Cranberries, Frozen 23 0 0.005 ^ 15.0

Cucumbers 610 1 0.2 0.047 ^ 0.015 ^ 2.0

Grapes 708 1 0.1 0.042 ^ 0.025 ^ 50.0

Oranges 708 0 0.015 ^ NT

TOTAL 2,805 2

Fomesafen (herbicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0
Appendix B. Page 52 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fonofos (insecticide) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.030 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 4,854 0

Forchlorfenuron (plant growth regulator) 

Cranberries 156 0 0.001 ^ 0.01

Cranberries, Frozen 25 0 0.001 ^ 0.01

Cucumbers 754 0 0.002 ^ NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 3 0.4 0.003 ^ 0.002 ^ 0.03

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.002 ^ NT

Pears 707 0 0.002 ^ 0.01

Strawberries 530 0 0.001 ^ NT

TOTAL 4,135 3

Formetanate hydrochloride (insecticide) 

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ 1.5

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 1.5

Pears 707 0 0.030 ^ 0.50

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 4,301 0

Fosthiazate (nematicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Furalaxyl (fungicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Furathiocarb (insecticide) 

Cucumbers 754 0 0.010 ^ NT

Oranges 708 0 0.010 ^ NT

TOTAL 1,462 0
Appendix B. Page 53 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Halosulfuron (herbicide) 

Cherries 30 0 0.050 ^ NT

Cherries, Frozen 144 0 0.050 ^ NT

Cranberries 156 0 0.010 ^ 0.05

Cranberries, Frozen 25 0 0.010 ^ 0.05

Grapefruit 346 0 0.005 ^ NT

Green Beans 567 0 0.005 ^ NT

Spinach 349 0 0.050 ^ NT

Sweet Potatoes 532 0 0.055 ^ 0.05

TOTAL 2,149 0

Halosulfuron methyl 2

 (herbicide) 

Cucumbers 754 0 0.010 ^ 0.5

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.010 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 2,539 0

Haloxyfop (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Heptenophos (insecticide, acaricide)

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Hexaconazole (fungicide) 

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 2,539 0

Hexazinone (herbicide) 

Cherries 30 0 0.002 ^ NT

Cherries, Frozen 144 0 0.002 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 2,132 0

Hexythiazox (insecticide, acaricide)

Apples 531 36 6.8 0.003 - 0.036 0.002 ^ 0.4

Applesauce 190 0 0.002 ^ 0.4

Cherries 30 0 0.012 ^ 1.0

Cherries, Frozen 144 1 0.7 0.014 ^ 0.012 ^ 1.0

Cucumbers 754 0 0.010 ^ NT
Appendix B. Page 54 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.001 - 0.30 0.6

Grapes 708 6 0.8 0.008 - 0.022 0.005 ^ 1

Green Beans 536 0 0.30 ^ 0.3

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 0.6

Pears 707 19 2.7 0.008 - 0.069 0.005 ^ 0.4

Spinach 349 0 0.015 ^ NT

Strawberries 530 69 13 0.001 - 0.35 0.001 ^ 6

Sweet Potatoes 532 0 0.015 ^ NT

TOTAL 7,368 131

Hydroprene (insect growth regulator) 

Cranberries 156 0 0.005 ^ 0.2

Cranberries, Frozen 25 0 0.005 ^ 0.2

Grapefruit 704 0 0.010 - 0.020 0.2

Grapes 708 0 0.007 ^ 0.2

Green Beans 567 0 0.008 ^ 0.2

Olives, Canned 189 0 0.020 ^ 0.2

Pears 707 0 0.007 ^ 0.2

Potatoes 708 0 0.002 ^ 0.2

Spinach 707 0 0.002 - 0.015 0.2

Strawberries 530 0 0.020 ^ 0.2

Sweet Potatoes 532 0 0.015 ^ 0.2

Tomatoes 528 0 0.002 ^ 0.2

Tomatoes, Canned 189 0 0.002 ^ 0.2

TOTAL 6,250 0

3-Hydroxycarbofuran (metabolite of Carbofuran)

Apples 531 0 0.003 ^ NT

Applesauce 190 0 0.003 ^ NT

Cherries 30 0 0.002 - 0.004 NT

Cherries, Frozen 144 0 0.002 - 0.004 NT

Cranberries 156 0 0.004 ^ NT

Cranberries, Frozen 25 0 0.004 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.004 NT

Grapes 708 0 0.050 ^ NT

Green Beans 567 1 0.2 0.002 ^ 0.002 ^ V - 1 NT

Lettuce 756 0 0.003 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 0 0.050 ^ NT

Potatoes 708 0 0.001 - 0.004 NT

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 - 0.004 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 9,363 1

5-Hydroxythiabendazole (metabolite of Thiabendazole)

Grapefruit 358 6 1.7 0.001 - 0.003 0.001 ^ 10.0

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ 5.0

TOTAL 1,077 6
Appendix B. Page 55 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Imazalil (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 1 0.7 0.028 ^ 0.005 ^ V - 1 NT

Cranberries 126 0 0.005 ^ NT

Cranberries, Frozen 23 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 562 79.8 0.001 - 0.11 0.001 - 0.003 10.0

Grapes 708 0 0.003 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 591 83.5 0.010 - 0.47 0.010 ^ 10.0

Pears 707 1 0.1 3.0 ^ 0.003 ^ V - 1 NT

Potatoes 708 1 0.1 0.004 ^ 0.001 - 0.003 V - 1 NT

Spinach 678 0 0.001 - 0.005 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 8,735 1,156

Imazapic (herbicide) 

Grapefruit 30 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 749 0

Imazapyr (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Imazaquin (herbicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Imazethapyr (herbicide) 

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,798 0

Imazosulfuron (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.025 ^ 0.02

TOTAL 1,609 0
Appendix B. Page 56 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Imidacloprid (insecticide) 

Apples 531 40 7.5 0.003 - 0.021 0.003 ^ 0.5

Applesauce 190 18 9.5 0.004 - 0.013 0.003 ^ 0.5

Cherries 30 0 0.019 ^ 3.0

Cherries, Frozen 144 31 21.5 0.019 - 0.23 0.019 ^ 3.0

Cranberries 156 0 0.005 ^ 0.05

Cranberries, Frozen 25 0 0.005 ^ 0.05

Cucumbers 754 21 2.8 0.010 - 0.060 0.010 ^ 0.5

Grapefruit 704 95 13.5 0.003 - 0.039 0.003 - 0.005 0.70

Grapes 707 61 8.6 0.042 - 2.2 0.025 - 0.083 X - 1 1.0

Green Beans 567 18 3.2 0.005 - 0.071 0.005 ^ 4.0

Lettuce 756 285 37.7 0.003 - 0.16 0.003 ^ 3.5

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 11 1.6 0.011 - 0.045 0.010 ^ 0.70

Pears 706 71 10.1 0.042 - 0.36 0.025 ^ 0.6

Potatoes 708 301 42.5 0.002 - 0.11 0.001 ^ 0.40

Spinach 707 291 41.2 0.002 - 0.57 0.001 - 0.020 3.5

Strawberries 530 75 14.2 0.003 - 0.063 0.003 ^ 0.50

Sweet Potatoes 532 0 0.020 ^ 0.40

Tomatoes 528 123 23.3 0.002 - 0.11 0.001 - 0.003 1.0

Tomatoes, Canned 189 52 27.5 0.002 - 0.016 0.001 ^ 1.0

TOTAL 9,361 1,493

Imidacloprid urea (metabolite of Imidacloprid)

Cherries 30 0 0.011 ^ 3.0

Cherries, Frozen 144 0 0.011 ^ 3.0

Spinach 349 0 0.015 ^ 3.5

Sweet Potatoes 532 0 0.015 ^ 0.40

TOTAL 1,055 0

Imiprothrin (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.091 ^ NT

Cherries, Frozen 144 0 0.091 ^ NT

Cranberries 156 0 0.050 ^ NT

Cranberries, Frozen 25 0 0.050 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.010 - 0.040 NT

Grapes 708 0 0.010 ^ NT

Green Beans 567 0 0.030 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Oranges 689 0 0.010 ^ NT

Pears 707 0 0.010 ^ NT

Spinach 349 0 0.095 ^ NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.095 ^ NT

TOTAL 7,561 0

Indaziflam (herbicide) 

Apples 531 0 0.001 ^ 0.01

Applesauce 190 0 0.001 ^ 0.01

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT
Appendix B. Page 57 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.001 ^ 0.01

Grapes 708 0 0.006 ^ 0.01

Lettuce 756 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ 0.01

Pears 707 0 0.006 ^ 0.01

Strawberries 530 0 0.001 ^ NT

TOTAL 4,496 0

Indoxacarb (insecticide) 

Apples 531 2 0.4 0.030 - 0.055 0.020 ^ 1.0

Applesauce 190 0 0.020 ^ 1.0

Cherries 30 0 0.021 - 0.042 0.90

Cherries, Frozen 144 0 0.021 - 0.042 0.90

Cranberries 156 0 0.050 ^ 1.5

Cranberries, Frozen 25 0 0.050 ^ 1.5

Cucumbers 754 0 0.010 ^ 0.60

Grapefruit 675 0 0.005 - 0.010 NT

Grapes 708 13 1.8 0.013 - 0.062 0.008 ^ 2

Green Beans 567 0 0.050 ^ 0.9

Lettuce 756 0 0.020 ^ 14

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 2 0.3 0.013 ^ 0.008 ^ 0.20

Spinach 349 1 0.3 0.037 ^ 0.025 ^ 14

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.025 ^ 0.01

TOTAL 7,551 18

Ipconazole (fungicide) 

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 675 0 0.003 - 0.020 NT

Green Beans 567 0 0.002 ^ 0.01

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 2,142 0

Iprodione (fungicide) 

Apples 531 0 0.040 ^ NT

Applesauce 190 0 0.040 ^ NT

Cherries 30 28 93.3 0.032 - 2.6 0.022 ^ 20.0

Cherries, Frozen 144 30 20.8 0.034 - 1.7 0.022 ^ 20.0

Cranberries 156 0 0.075 ^ NT

Cranberries, Frozen 25 0 0.075 ^ NT

Cucumbers 754 1 0.1 0.022 ^ 0.005 ^ V - 1 NT

Grapefruit 704 0 0.010 - 0.15 NT

Grapes 708 77 10.9 0.017 - 1.2 0.010 ^ 60.0

Green Beans 567 0 0.15 ^ 2.0

Lettuce 756 2 0.3 0.40 ^ 0.040 ^ 25.0

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 668 0 0.009 - 0.030 0.5

Spinach 707 2 0.3 0.015 - 0.042 0.009 - 0.030 V - 2 NT

Strawberries 530 13 2.5 0.012 - 0.59 0.010 ^ 15.0

Sweet Potatoes 532 0 0.025 ^ NT
Appendix B. Page 58 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 528 0 0.009 ^ NT

Tomatoes, Canned 189 0 0.009 - 0.030 NT

TOTAL 8,616 153

Iprovalicarb (fungicide) 

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ NT

Grapes 708 0 0.001 ^ 2.0

Olives, Canned 189 0 0.003 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 2,840 0

Isocarbophos (insecticide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Isofenphos (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Isofenphos methyl (metabolite if Isofenphos)

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Isofetamid (fungicide) 

Cranberries 156 0 0.001 ^ 5.0

Cranberries, Frozen 25 0 0.001 ^ 5.0

TOTAL 181 0

Isoprocarb (insecticide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Isoproturon (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Isoxadifen ethyl (herbicide safener) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 ^ NT
Appendix B. Page 59 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,604 0

Kresoxim-methyl (fungicide) 

Apples 531 0 0.010 ^ 0.5

Applesauce 190 0 0.010 ^ 0.5

Cherries 30 0 0.015 ^ NT

Cherries, Frozen 144 0 0.015 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 ^ NT

Grapes 708 19 2.7 0.013 - 0.047 0.008 ^ 1.0

Green Beans 567 0 0.020 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Pears 707 1 0.1 0.013 ^ 0.008 ^ 0.5

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.015 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 7,901 20

Lactofen (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Lenacil (herbicide) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 2,539 0

Leptophos oxygen analog (insecticide metabolite)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Linuron (herbicide) 

Cherries 30 0 0.007 ^ NT

Cherries, Frozen 144 1 0.7 0.026 ^ 0.007 ^ V - 1 NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 0 0.019 ^ NT

Grapefruit 704 0 0.003 - 0.016 NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.019 ^ NT

Potatoes 708 0 0.003 ^ 0.2

Spinach 707 12 1.7 0.005 - 0.023 0.003 - 0.010 V - 12 NT
Appendix B. Page 60 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 5,904 13

Lufenuron (insecticide) 

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 2,132 0

Malathion (insecticide) 

Apples 531 1 0.2 0.004 ^ 0.002 ^ 8

Applesauce 190 0 0.002 ^ 8

Cherries 30 0 0.005 ^ 8

Cherries, Frozen 144 5 3.5 0.005 - 0.036 0.005 ^ 8

Cranberries 156 0 0.010 ^ 8

Cranberries, Frozen 25 0 0.010 ^ 8

Cucumbers 754 0 0.010 ^ 8

Grapefruit 704 0 0.003 - 0.005 8

Grapes 708 0 0.002 ^ 8

Green Beans 567 1 0.2 0.006 ^ 0.002 ^ 8

Lettuce 756 0 0.002 ^ 8

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 8

Pears 707 0 0.002 ^ 8

Potatoes 708 0 0.001 ^ 8

Spinach 707 0 0.001 - 0.005 8

Strawberries 530 33 6.2 0.003 - 0.068 0.003 ^ 8

Sweet Potatoes 532 1 0.2 0.005 ^ 0.005 ^ 1

Tomatoes 528 1 0.2 0.006 ^ 0.001 - 0.003 8

Tomatoes, Canned 189 0 0.001 ^ 8

TOTAL 9,363 42

Malathion oxygen analog (metabolite of Malathion)

Apples 502 0 0.002 ^ 8

Applesauce 190 0 0.002 ^ 8

Cherries 30 0 0.004 ^ 8

Cherries, Frozen 144 0 0.004 ^ 8

Cranberries 156 0 0.002 ^ 8

Cranberries, Frozen 25 0 0.002 ^ 8

Cucumbers 754 0 0.010 ^ 8

Grapefruit 704 0 0.001 ^ 8

Grapes 708 0 0.005 ^ 8

Green Beans 567 0 0.001 ^ 8

Lettuce 756 0 0.002 ^ 8

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 8

Pears 707 0 0.005 ^ 8

Potatoes 708 0 0.003 ^ 8
Appendix B. Page 61 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinach 707 0 0.003 - 0.005 8

Strawberries 530 11 2.1 0.001 - 0.004 0.001 ^ 8

Sweet Potatoes 532 0 0.005 ^ 1

Tomatoes 528 0 0.003 ^ 8

Tomatoes, Canned 189 0 0.003 ^ 8

TOTAL 9,334 11

Mandipropamid (fungicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 6 0.8 0.005 - 0.013 0.005 ^ 0.6

Grapefruit 704 0 0.001 - 0.003 NT

Grapes 708 0 0.003 ^ 1.4

Green Beans 567 0 0.001 ^ 0.90

Lettuce 756 111 14.7 0.002 - 2.3 0.002 ^ 20

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.005 ^ 0.09

Spinach 707 481 68 0.008 - 7.1 0.005 - 0.020 20

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.020 ^ 0.09

Tomatoes 528 11 2.1 0.008 ^ 0.005 ^ 1.0

Tomatoes, Canned 189 1 0.5 0.008 ^ 0.005 ^ 1.0

TOTAL 8,656 610

MCPA (herbicide) 

Grapefruit 268 0 0.25 ^ NT

Strawberries 530 0 0.25 ^ NT

TOTAL 798 0

MCPB (herbicide) 

Grapefruit 268 0 0.25 ^ NT

Strawberries 530 0 0.25 ^ NT

TOTAL 798 0

Mecarbam (insecticide, acaricide)

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Mecoprop - MCPP (herbicide) 

Grapefruit 358 0 0.25 ^ NT

Olives, Canned 189 0 0.25 ^ NT

Strawberries 530 0 0.25 ^ NT

TOTAL 1,077 0

Mefenpyr diethyl (herbicide safener) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0
Appendix B. Page 62 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mepanipyrim (fungicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 - 0.003 NT

Strawberries 530 0 0.001 ^ 1.5

TOTAL 1,077 0

Mesotrione (herbicide) 

Cranberries 156 0 0.050 ^ 0.02

Cranberries, Frozen 25 0 0.050 ^ 0.02

Grapefruit 346 0 0.010 ^ 0.01

Strawberries 530 0 0.020 ^ 0.01

TOTAL 1,057 0

Metaflumizone (insecticide) 

Cherries 30 0 0.005 ^ 0.04

Cherries, Frozen 144 0 0.005 ^ 0.04

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Grapefruit 704 0 0.001 - 0.010 0.04

Olives, Canned 189 0 0.010 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 2,659 0

Metalaxyl/Mefenoxam 3 (fungicide) 

Apples 531 0 0.001 ^ 0.2

Applesauce 190 0 0.001 ^ 0.2

Cherries 30 0 0.030 ^ 1.0

Cherries, Frozen 144 0 0.030 ^ 1.0

Cranberries 156 0 0.010 ^ 4.0

Cranberries, Frozen 25 0 0.010 ^ 4.0

Cucumbers 754 225 29.8 0.005 - 0.32 0.005 ^ 1.0

Grapefruit 704 0 0.001 - 0.005 1.0

Grapes 708 3 0.4 0.005 - 0.034 0.003 ^ 2.0

Green Beans 567 28 4.9 0.001 - 0.066 0.001 ^ 0.2

Lettuce 756 46 6.1 0.001 - 0.017 0.001 ^ 5.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ 1.0

Potatoes 708 54 7.6 0.002 - 0.017 0.001 ^ 0.5

Spinach 707 16 2.3 0.002 - 0.19 0.001 - 0.030 10.0

Strawberries 530 84 15.8 0.001 - 0.15 0.001 ^ 10.0

Sweet Potatoes 532 0 0.030 ^ 0.5

Tomatoes 528 6 1.1 0.002 - 0.066 0.001 ^ 1.0

Tomatoes, Canned 189 2 1.1 0.002 ^ 0.001 ^ 1.0

TOTAL 8,656 464

Metaldehyde (molluscicide) 

Cherries 30 0 0.11 ^ NT

Cherries, Frozen 144 0 0.11 ^ NT

Grapefruit 358 0 0.10 ^ 0.26

Olives, Canned 189 0 0.10 ^ NT

Spinach 349 0 0.11 ^ NT

Strawberries 530 1 0.2 0.12 ^ 0.10 ^ 6.25

Sweet Potatoes 532 0 0.11 ^ NT

TOTAL 2,132 1
Appendix B. Page 63 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Metconazole (fungicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ 0.04

TOTAL 1,609 0

Methamidophos (insecticide) (also a metabolite of Acephate)

Apples 531 0 0.005 ^ 0.02

Applesauce 190 0 0.005 ^ 0.02

Cherries 30 0 0.033 ^ 0.02

Cherries, Frozen 144 0 0.033 ^ 0.02

Cranberries 156 0 0.020 ^ 0.1

Cranberries, Frozen 25 0 0.020 ^ 0.1

Cucumbers 754 1 0.1 0.016 ^ 0.010 ^ 0.02

Grapefruit 704 0 0.001 - 0.020 0.02

Grapes 708 0 0.050 ^ 0.02

Green Beans 567 54 9.5 0.020 - 0.58 0.020 ^ 1 4

Lettuce 756 5 0.7 0.006 - 0.019 0.005 ^ 1 4

Olives, Canned 189 0 0.001 ^ 0.02

Oranges 708 0 0.010 ^ 0.02

Potatoes 708 0 0.001 - 0.004 0.1

Spinach 707 0 0.004 - 0.035 0.02

Strawberries 530 0 0.001 ^ 0.02

Sweet Potatoes 532 0 0.035 ^ 0.02

Tomatoes 528 2 0.4 0.002 - 0.008 0.001 ^ 2.0

Tomatoes, Canned 189 0 0.001 ^ 2.0

TOTAL 8,656 62

Methidathion (insecticide) 

Apples 472 0 0.010 ^ 0.05

Applesauce 190 0 0.010 ^ 0.05

Cherries 30 0 0.012 ^ 0.05

Cherries, Frozen 144 0 0.012 ^ 0.05

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.003 4.0

Grapes 708 0 0.003 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ 0.05

Oranges 708 0 0.010 ^ 4.0

Pears 707 3 0.4 0.005 - 0.040 0.003 ^ 0.05

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.015 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 8,737 3

Methiocarb (insecticide)

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT
Appendix B. Page 64 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.001 - 0.003 NT

Spinach 358 0 0.001 - 0.003 NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 508 0 0.001 - 0.003 NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 4,302 0

Methiocarb sulfone (metabolite of Methiocarb)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Methiocarb sulfoxide (metabolite of Methiocarb)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Methomyl (insecticide) 

Apples 531 0 0.030 ^ 1

Applesauce 190 0 0.030 ^ 1

Cherries 30 0 0.013 ^ NT

Cherries, Frozen 144 0 0.013 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 4 0.5 0.016 - 0.068 0.010 ^ 0.2

Grapefruit 704 0 0.001 - 0.010 2

Grapes 708 3 0.4 0.017 - 0.49 0.005 ^ 5

Green Beans 567 51 9 0.001 - 0.62 0.001 ^ 2

Lettuce 756 18 2.4 0.030 - 0.83 0.030 ^ 5

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.010 ^ 2

Pears 707 0 0.005 ^ 4

Potatoes 708 0 0.002 ^ 0.2

Spinach 707 30 4.2 0.004 - 1.0 0.002 - 0.015 6

Strawberries 530 2 0.4 0.016 - 0.11 0.010 ^ V - 2 NT

Sweet Potatoes 532 0 0.015 ^ 0.2

Tomatoes 528 0 0.002 ^ 1

Tomatoes, Canned 189 0 0.002 ^ 1

TOTAL 9,363 108

Methomyl oxime (metabolite of Methomyl)

Grapefruit 346 0 0.050 ^ 2

TOTAL 346 0

Methoprene (insect growth regulator) 

Grapefruit 346 0 0.050 ^ EX2

Green Beans 567 0 0.040 ^ EX2

Potatoes 708 0 0.015 ^ EX2

Sweet Potatoes 532 0 0.030 ^ EX2

Tomatoes 528 0 0.015 ^ EX2

Tomatoes, Canned 189 0 0.015 ^ EX2

TOTAL 2,870 0
Appendix B. Page 65 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Methoxychlor Total (insecticide) 

Cherries 30 0 0.039 ^ NT

Cherries, Frozen 144 0 0.039 ^ NT

Potatoes 689 0 0.001 - 0.003 NT

Spinach 678 0 0.001 - 0.20 NT

Sweet Potatoes 532 0 0.040 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 - 0.003 NT

TOTAL 2,790 0

Methoxychlor olefin (metabolite of Methoxychlor)

Potatoes 708 0 0.001 - 0.003 NT

Spinach 358 0 0.001 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 1,783 0

Methoxychlor p,p' (isomer of Methoxychlor)

Cucumbers 690 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 2,475 0

Methoxyfenozide (insecticide) 

Apples 531 25 4.7 0.004 - 0.045 0.003 ^ 2.0

Applesauce 190 2 1.1 0.004 - 0.010 0.003 ^ 2.0

Cherries 30 0 0.006 ^ 3.0

Cherries, Frozen 144 1 0.7 0.006 ^ 0.006 ^ 3.0

Cranberries 156 3 1.9 0.002 - 0.003 0.002 ^ 3.0

Cranberries, Frozen 25 6 24 0.002 - 0.008 0.002 ^ 3.0

Cucumbers 754 0 0.010 ^ 0.3

Grapefruit 704 2 0.3 0.003 - 0.004 0.002 - 0.003 3.0

Grapes 708 81 11.4 0.008 - 0.15 0.005 ^ 1.0

Green Beans 567 8 1.4 0.002 - 0.062 0.002 ^ 1.5

Lettuce 756 11 1.5 0.003 - 0.29 0.003 ^ 30

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 3.0

Pears 707 15 2.1 0.008 - 0.073 0.005 ^ 2.0

Potatoes 708 0 0.001 ^ 0.02

Spinach 707 40 5.7 0.002 - 5.0 0.001 - 0.010 30

Strawberries 530 24 4.5 0.003 - 0.15 0.003 ^ 2.0

Sweet Potatoes 532 0 0.010 ^ 0.02

Tomatoes 528 52 9.8 0.002 - 0.028 0.001 ^ 2.0

Tomatoes, Canned 189 6 3.2 0.002 - 0.006 0.001 ^ 2.0

TOTAL 9,363 276

Metolachlor (herbicide) 

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Cherries 30 0 0.007 ^ NT

Cherries, Frozen 144 0 0.007 ^ NT

Cranberries 156 0 0.005 ^ 0.15

Cranberries, Frozen 25 0 0.005 ^ 0.15
Appendix B. Page 66 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cucumbers 754 1 0.1 0.007 ^ 0.005 ^ 0.50

Grapefruit 704 0 0.003 - 0.010 NT

Green Beans 567 0 0.005 ^ 0.30

Lettuce 756 0 0.001 ^ 1.5

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ 0.20

Spinach 707 0 0.001 - 0.010 0.50

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ 0.20

Tomatoes 528 0 0.001 ^ 0.10

Tomatoes, Canned 189 0 0.001 ^ 0.10

TOTAL 7,948 1

Metolcarb (insecticide, acaricide)

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Metrafenone (fungicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Metribuzin (herbicide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.016 ^ NT

Cherries, Frozen 144 0 0.016 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 ^ NT

Green Beans 567 0 0.002 ^ NT

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 6 0.8 0.003 - 0.008 0.002 ^ 0.6

Spinach 707 1 0.1 0.037 ^ 0.002 - 0.020 V - 1 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 0 0.002 ^ 0.1

Tomatoes, Canned 189 0 0.002 ^ 0.1

TOTAL 6,486 7

Metsulfuron methyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Mevinphos (insecticide) 

Cherries 30 0 0.006 ^ NT

Cherries, Frozen 144 0 0.006 ^ NT

Cranberries 156 0 0.010 ^ NT
Appendix B. Page 67 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.002 - 0.003 NT

Green Beans 567 0 0.002 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 - 0.005 NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 5,763 0

MGK-264 (insecticide) 

Apples 531 0 0.10 ^ 5

Applesauce 190 0 0.10 ^ 5

Cherries 30 0 0.030 ^ 5

Cherries, Frozen 144 0 0.030 ^ 5

Cranberries 156 0 0.025 ^ 5

Cranberries, Frozen 25 0 0.025 ^ 5

Grapefruit 704 0 0.005 ^ 5

Grapes 708 0 0.001 ^ 5

Green Beans 567 0 0.020 ^ 5

Lettuce 756 0 0.10 ^ 5

Olives, Canned 189 0 0.005 ^ 5

Pears 707 0 0.001 ^ 5

Potatoes 708 0 0.002 ^ 5

Spinach 707 0 0.002 - 0.030 5

Strawberries 530 0 0.005 ^ 5

Sweet Potatoes 532 0 0.030 ^ 5

Tomatoes 528 0 0.002 ^ 5

Tomatoes, Canned 189 0 0.002 ^ 5

TOTAL 7,901 0

Monocrotophos (insecticide) 

Cherries 30 0 0.017 ^ NT

Cherries, Frozen 144 1 0.7 0.037 ^ 0.017 ^ V - 1 NT

Cucumbers 754 1 0.1 0.081 ^ 0.010 ^ V - 1 NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.020 ^ NT

Strawberries 530 2 0.4 0.003 - 0.18 0.003 ^ V - 2 NT

Sweet Potatoes 532 0 0.020 ^ NT

TOTAL 3,594 4

Monolinuron (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Myclobutanil (fungicide) 

Apples 531 10 1.9 0.004 - 0.017 0.003 ^ 0.5

Applesauce 190 1 0.5 0.004 ^ 0.003 ^ 0.5
Appendix B. Page 68 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries 30 0 0.001 - 0.002 5.0

Cherries, Frozen 144 18 12.5 0.001 - 0.061 0.001 - 0.002 5.0

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 31 4.1 0.005 - 0.067 0.005 ^ 0.20

Grapefruit 704 0 0.003 - 0.010 NT

Grapes 708 165 23.3 0.017 - 1.8 0.010 ^ X - 1 1.0

Green Beans 567 19 3.4 0.006 - 0.11 0.005 ^ 1.0

Lettuce 756 17 2.2 0.003 - 0.43 0.003 ^ 9.0

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.010 ^ NT

Potatoes 708 0 0.001 - 0.003 0.03

Spinach 707 0 0.001 - 0.003 0.03

Strawberries 530 139 26.2 0.003 - 0.55 0.003 ^ X - 2 0.50

Sweet Potatoes 532 0 0.001 ^ 0.03

Tomatoes 528 22 4.2 0.002 - 0.013 0.001 - 0.003 0.30

Tomatoes, Canned 189 1 0.5 0.002 ^ 0.001 ^ 0.30

TOTAL 9,363 423

Naled (insecticide) 

Apples 531 0 0.020 ^ 0.5

Applesauce 190 0 0.020 ^ 0.5

Grapes 708 0 0.025 ^ 0.5

Lettuce 756 0 0.020 ^ 0.5

Pears 707 0 0.025 ^ 0.5

TOTAL 2,892 0

1-Naphthol (metabolite of Carbaryl)

Apples 442 3 0.7 0.031 - 0.54 0.015 ^ 12

Applesauce 190 1 0.5 0.034 ^ 0.015 ^ 12

Cranberries 156 7 4.5 0.010 - 0.021 0.010 ^ 3.0

Cranberries, Frozen 25 0 0.010 ^ 3.0

Grapefruit 346 0 0.010 ^ 10

Grapes 708 0 0.050 ^ 10

Green Beans 408 5 1.2 0.013 - 4.4 0.006 ^ 10

Lettuce 126 0 0.015 ^ 10

Pears 707 0 0.050 ^ 12

TOTAL 3,108 16

Napropamide (herbicide) 

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cranberries 156 0 0.001 ^ 0.1

Cranberries, Frozen 25 0 0.001 ^ 0.1

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Grapes 708 0 0.002 ^ 0.1

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 0 0.002 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.020 NT

Strawberries 530 0 0.005 ^ 0.1

Sweet Potatoes 532 0 0.020 ^ 0.1
Appendix B. Page 69 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 508 0 0.002 ^ 0.1

Tomatoes, Canned 189 0 0.002 ^ 0.1

TOTAL 6,953 0

Nicosulfuron (herbicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.005 NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,604 0

Nitrapyrin (nitrification inhibitor) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.020 NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,604 0

Nitrofen (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Norflurazon (herbicide) 

Apples 531 0 0.002 ^ 0.1

Applesauce 190 0 0.002 ^ 0.1

Cherries 30 0 0.005 ^ 0.1

Cherries, Frozen 144 0 0.005 ^ 0.1

Cranberries 156 0 0.010 ^ 0.1

Cranberries, Frozen 25 0 0.010 ^ 0.1

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.003 - 0.005 0.2

Grapes 708 0 0.010 ^ 0.1

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 0.2

Pears 707 1 0.1 0.017 ^ 0.010 ^ 0.1

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 8,796 1

Norflurazon desmethyl (metabolite of Norflurazon)

Apples 531 0 0.005 ^ 0.1

Applesauce 190 0 0.005 ^ 0.1

Cherries 30 0 0.010 ^ 0.1

Cherries, Frozen 144 0 0.010 ^ 0.1

Cranberries 156 0 0.005 ^ 0.1

Cranberries, Frozen 25 0 0.005 ^ 0.1

Cucumbers 754 0 0.010 ^ NT
Appendix B. Page 70 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.001 - 0.003 0.2

Grapes 708 0 0.020 ^ 0.1

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 1 0.1 0.015 ^ 0.010 ^ 0.2

Potatoes 708 2 0.3 0.002 ^ 0.001 ^ V - 2 NT

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 1 0.2 0.003 ^ 0.003 ^ V - 1 NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 8,089 4

Novaluron (insecticide) 

Cherries 30 0 0.010 ^ 8.0

Cherries, Frozen 144 0 0.010 ^ 8.0

Cranberries 156 0 0.005 ^ 7.0

Cranberries, Frozen 25 0 0.005 ^ 7.0

Cucumbers 754 0 0.010 ^ 0.20

Grapefruit 704 0 0.020 - 0.050 0.01

Grapes 708 0 0.007 ^ 0.01

Green Beans 567 4 0.7 0.064 - 0.12 0.050 ^ 0.70

Olives, Canned 189 0 0.020 ^ 0.01

Oranges 708 0 0.010 ^ 0.01

Pears 707 41 5.8 0.012 - 0.13 0.007 ^ 3.0

Potatoes 708 0 0.001 - 0.003 0.05

Spinach 707 3 0.4 0.002 ^ 0.001 - 0.010 0.01

Strawberries 530 147 27.7 0.020 - 0.28 0.020 ^ 0.45

Sweet Potatoes 532 0 0.010 ^ 0.05

Tomatoes 528 5 0.9 0.005 - 0.022 0.003 ^ 1.0

Tomatoes, Canned 189 0 0.003 ^ 1.0

TOTAL 7,886 200

Omethoate (insecticide) (also a metabolite of Dimethoate)

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Cherries 30 0 0.010 ^ 2.0

Cherries, Frozen 144 8 5.6 0.010 - 0.053 0.010 ^ 2.0

Cranberries 156 0 0.015 ^ NT

Cranberries, Frozen 25 0 0.015 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.006 2.0

Grapes 708 0 0.025 ^ NT

Green Beans 567 25 4.4 0.006 - 0.19 0.006 ^ 2.0

Lettuce 756 1 0.1 0.037 ^ 0.020 ^ 2.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 2.0

Pears 707 0 0.025 ^ 2.0

Potatoes 708 0 0.002 ^ 0.2

Spinach 707 12 1.7 0.004 - 0.021 0.002 - 0.010 V - 12 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 4 0.8 0.004 ^ 0.002 ^ 2.0

Tomatoes, Canned 189 0 0.002 ^ 2.0

TOTAL 9,363 50
Appendix B. Page 71 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oryzalin (herbicide) 

Apples 531 0 0.020 ^ 0.05

Applesauce 190 0 0.020 ^ 0.05

Cherries 30 0 0.099 ^ 0.05

Cherries, Frozen 144 0 0.099 ^ 0.05

Cranberries 156 0 0.20 ^ 0.05

Cranberries, Frozen 25 0 0.20 ^ 0.05

Cucumbers 754 0 0.020 ^ NT

Grapefruit 704 0 0.020 - 0.10 0.05

Grapes 708 0 0.025 ^ 0.05

Lettuce 756 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ 0.05

Oranges 708 0 0.020 ^ 0.05

Pears 707 0 0.025 ^ 0.05

Spinach 349 0 0.10 ^ NT

Strawberries 530 0 0.020 ^ 0.05

Sweet Potatoes 532 0 0.10 ^ NT

TOTAL 7,013 0

Oxadiazon (herbicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ NT

Lettuce 725 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 2,523 0

Oxadixyl (fungicide) 

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.003 ^ NT

Spinach 358 0 0.003 ^ NT

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 4,322 0

Oxamyl (insecticide) 

Apples 531 0 0.003 ^ 2

Applesauce 190 0 0.003 ^ 2

Cherries 30 0 0.004 ^ NT

Cherries, Frozen 144 0 0.004 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 3 0.4 0.013 - 0.028 0.010 ^ 2.0

Grapefruit 704 0 0.002 - 0.005 3

Green Beans 567 1 0.2 0.005 ^ 0.002 ^ V - 1 NT

Lettuce 756 1 0.1 0.017 ^ 0.003 ^ V - 1 NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ 3

Pears 707 0 0.016 ^ 2.0

Potatoes 708 0 0.002 - 0.006 0.1
Appendix B. Page 72 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinach 707 0 0.005 - 0.006 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.005 ^ 0.1

Tomatoes 528 1 0.2 0.014 ^ 0.002 ^ 2

Tomatoes, Canned 189 0 0.002 ^ 2

TOTAL 8,655 6

Oxamyl oxime (metabolite of Oxamyl)

Apples 531 0 0.006 ^ 2

Applesauce 190 0 0.006 ^ 2

Cherries 30 0 0.040 ^ NT

Cherries, Frozen 144 0 0.040 ^ NT

Cranberries 156 0 0.050 ^ NT

Cranberries, Frozen 25 0 0.050 ^ NT

Cucumbers 754 23 3.1 0.010 - 0.12 0.010 ^ 2.0

Grapefruit 704 0 0.005 - 0.050 3

Green Beans 567 0 0.050 ^ NT

Lettuce 756 1 0.1 0.006 ^ 0.006 ^ V - 1 NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ 3

Spinach 349 0 0.040 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.040 ^ 0.1

TOTAL 6,165 24

Oxydemeton methyl (insecticide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Cranberries 58 0 0.025 ^ NT

Cranberries, Frozen 14 0 0.025 ^ NT

Cucumbers 754 0 0.010 ^ 1.0

Grapefruit 704 0 0.001 - 0.050 1.0

Green Beans 567 0 0.002 ^ NT

Lettuce 756 6 0.8 0.003 - 0.012 0.002 ^ 2.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 1.0

Spinach 349 0 0.005 ^ NT

Strawberries 530 1 0.2 0.004 ^ 0.001 ^ 2.0

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 6,056 7

Oxydemeton methyl sulfone (metabolite of Oxydemeton methyl)

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 0 0.010 ^ 1.0

Grapefruit 704 0 0.001 - 0.002 1.0

Green Beans 567 0 0.001 ^ NT

Lettuce 756 0 0.002 ^ 2.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 1.0

Strawberries 530 0 0.001 ^ 2.0

TOTAL 5,110 0
Appendix B. Page 73 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oxyfluorfen (herbicide) 

Apples 531 0 0.050 ^ 0.05

Applesauce 190 0 0.050 ^ 0.05

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.020 ^ NT

Grapes 708 0 0.006 ^ 0.05

Lettuce 756 0 0.050 ^ NT

Olives, Canned 189 0 0.020 ^ 0.05

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.006 ^ 0.05

Potatoes 708 0 0.001 - 0.003 NT

Spinach 358 14 3.9 0.002 - 0.004 0.001 ^ V - 14 NT

Strawberries 530 0 0.020 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,214 14

Paclobutrazol (plant growth regulator) 

Cherries 30 0 0.007 ^ NT

Cherries, Frozen 144 0 0.007 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 3,594 0

Parathion (insecticide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.059 ^ NT

Cherries, Frozen 144 0 0.059 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.003 ^ NT

Spinach 707 0 0.003 - 0.060 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.060 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 6,854 0

Parathion methyl (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.016 ^ NT

Cherries, Frozen 144 0 0.016 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT
Appendix B. Page 74 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.005 - 0.020 NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.015 ^ NT

Potatoes 708 0 0.002 ^ 0.1

Spinach 707 0 0.002 - 0.020 NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.020 ^ 0.1

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 8,088 0

Parathion methyl oxygen analog (metabolite of Parathion methyl)

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Grapefruit 704 0 0.005 - 0.010 NT

Lettuce 756 0 0.020 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ 0.1

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 4,683 0

Parathion oxygen analog (metabolite of Parathion)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Potatoes 708 0 0.003 ^ NT

Spinach 358 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 2,860 0

Pebulate (herbicide) 

Cucumbers 754 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

TOTAL 1,462 0

Penconazole (fungicide) 

Cherries 30 0 0.006 ^ NT

Cherries, Frozen 144 0 0.006 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Grapes 708 4 0.6 0.007 - 0.037 0.004 ^ V - 4 NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 4,302 4
Appendix B. Page 75 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pencycuron (fungicide) 

Cherries 30 0 0.003 ^ NT

Cherries, Frozen 144 0 0.003 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,594 0

Pendimethalin (herbicide) 

Apples 531 0 0.050 ^ 0.1

Applesauce 190 0 0.050 ^ 0.1

Cherries 30 0 0.032 ^ 0.1

Cherries, Frozen 144 0 0.032 ^ 0.1

Cranberries 156 0 0.005 ^ 0.1

Cranberries, Frozen 25 0 0.005 ^ 0.1

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.010 - 0.045 0.1

Grapes 708 0 0.005 ^ 0.1

Green Beans 567 0 0.040 ^ 0.10

Lettuce 756 0 0.050 ^ 4.0

Olives, Canned 189 0 0.010 ^ 0.1

Oranges 708 0 0.005 ^ 0.1

Pears 707 0 0.005 ^ 0.1

Potatoes 708 10 1.4 0.002 - 0.007 0.001 ^ 0.1

Spinach 707 18 2.5 0.002 - 0.011 0.001 - 0.035 V - 18 NT

Strawberries 530 0 0.010 ^ 0.1

Sweet Potatoes 532 0 0.035 ^ NT

Tomatoes 528 0 0.001 ^ 0.1

Tomatoes, Canned 189 2 1.1 0.002 ^ 0.001 ^ 0.1

TOTAL 9,363 30

Penflufen (fungicide) 

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Grapefruit 704 0 0.001 ^ NT

Green Beans 567 0 0.001 ^ 0.01

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 2,171 0

Penoxsulam (herbicide) 

Cucumbers 754 0 0.010 ^ NT

Grapefruit 90 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ 0.01

Oranges 708 0 0.010 ^ NT

TOTAL 1,741 0

Pentachloroaniline - PCA (metabolite of Quintozene)

Apples 531 0 0.004 ^ NT

Applesauce 190 0 0.004 ^ NT

Cranberries 156 0 0.005 ^ NT
Appendix B. Page 76 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.003 - 0.060 NT

Green Beans 567 0 0.060 ^ 0.1

Lettuce 756 0 0.004 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 31 4.4 0.002 - 0.009 0.001 ^ 0.1

Spinach 707 4 0.6 0.002 - 0.005 0.001 - 0.005 V - 4 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 - 0.010 NT

Tomatoes 528 0 0.001 ^ 0.1

Tomatoes, Canned 189 0 0.001 ^ 0.1

TOTAL 7,774 35

Pentachlorobenzene - PCB (metabolite of Quintozene)

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.015 NT

Green Beans 474 0 0.015 ^ 0.1

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 689 0 0.010 ^ 0.1

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.001 ^ NT

Tomatoes 509 0 0.003 - 0.010 0.1

Tomatoes, Canned 189 0 0.003 - 0.010 0.1

TOTAL 7,643 0

Pentachlorophenyl methyl sulfide (metabolite of Quintozene)

Cranberries 156 0 0.015 ^ NT

Cranberries, Frozen 25 0 0.015 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.020 - 0.025 NT

Green Beans 567 0 0.025 ^ 0.1

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 692 0 0.001 - 0.005 NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 4,857 0

Penthiopyrad (fungicide) 

Cranberries 156 0 0.001 ^ 3.0

Cranberries, Frozen 25 0 0.001 ^ 3.0

Cucumbers 754 0 0.010 ^ 0.60

Grapefruit 704 0 0.001 ^ NT

Green Beans 567 38 6.7 0.001 - 0.25 0.001 ^ 4.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT
Appendix B. Page 77 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pears 707 1 0.1 0.003 ^ 0.002 ^ 0.50

Potatoes 708 8 1.1 0.003 - 0.009 0.002 ^ 0.06

Spinach 358 14 3.9 0.003 - 3.3 0.002 ^ 30

Strawberries 530 147 27.7 0.001 - 0.74 0.001 ^ 3.0

Tomatoes 528 39 7.4 0.003 - 0.24 0.002 ^ 3.0

Tomatoes, Canned 189 7 3.7 0.003 - 0.009 0.002 ^ 3.0

TOTAL 6,123 254

Permethrin Total (insecticide)

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 4 0.5 0.008 - 0.013 0.005 ^ 1.5

Grapefruit 346 0 0.010 ^ NT

Grapes 708 1 0.1 0.010 ^ 0.006 ^ V - 1 NT

Green Beans 567 1 0.2 0.097 ^ 0.040 ^ V - 1 NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.006 ^ 0.05

TOTAL 3,971 6

Permethrin cis (isomer of Permethrin)

Apples 531 0 0.010 ^ 0.05

Applesauce 190 0 0.010 ^ 0.05

Cherries 30 0 0.020 ^ 4.0

Cherries, Frozen 144 8 5.6 0.020 - 0.059 0.020 ^ 4.0

Grapefruit 358 0 0.010 ^ NT

Lettuce 756 61 8.1 0.010 - 0.74 0.010 ^ 20

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.05

Spinach 707 493 69.7 0.002 - 4.3 0.001 - 0.020 20

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 4 0.8 0.020 - 0.19 0.020 ^ V - 4 NT

Tomatoes 528 8 1.5 0.002 - 0.030 0.001 ^ 2.0

Tomatoes, Canned 189 2 1.1 0.002 - 0.005 0.001 ^ 2.0

TOTAL 5,392 577

Permethrin trans (isomer of Permethrin)

Apples 531 0 0.010 ^ 0.05

Applesauce 190 0 0.010 ^ 0.05

Cherries 30 0 0.010 ^ 4.0

Cherries, Frozen 144 10 6.9 0.013 - 0.086 0.010 ^ 4.0

Grapefruit 358 0 0.010 ^ NT

Lettuce 756 62 8.2 0.010 - 0.92 0.010 ^ 20

Olives, Canned 189 0 0.010 ^ NT

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.05

Spinach 707 502 71 0.002 - 5.9 0.001 - 0.010 20

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 7 1.3 0.013 - 0.28 0.010 ^ V - 7 NT

Tomatoes 528 9 1.7 0.002 - 0.041 0.001 ^ 2.0

Tomatoes, Canned 189 2 1.1 0.002 - 0.005 0.001 ^ 2.0

TOTAL 5,392 593

Phenothrin (insecticide) 

Apples 531 0 0.050 ^ 0.01

Applesauce 190 0 0.050 ^ 0.01

Cherries 30 0 0.15 ^ 0.01
Appendix B. Page 78 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries, Frozen 144 0 0.15 ^ 0.01

Cranberries 156 0 0.025 ^ 0.01

Cranberries, Frozen 25 0 0.025 ^ 0.01

Cucumbers 754 0 0.005 ^ 0.01

Grapefruit 704 0 0.005 ^ 0.01

Grapes 708 0 0.005 ^ 0.01

Green Beans 567 0 0.030 ^ 0.01

Lettuce 756 0 0.050 ^ 0.01

Olives, Canned 189 0 0.005 ^ 0.01

Oranges 708 0 0.005 ^ 0.01

Pears 707 0 0.005 ^ 0.01

Potatoes 708 0 0.002 ^ 0.01

Spinach 707 0 0.002 - 0.15 0.01

Strawberries 530 0 0.005 ^ 0.01

Sweet Potatoes 532 0 0.15 ^ 0.01

Tomatoes 528 0 0.002 ^ 0.01

Tomatoes, Canned 189 0 0.002 ^ 0.01

TOTAL 9,363 0

Phenthoate (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 2,860 0

o-Phenylphenol (fungicide) 

Apples 531 2 0.4 0.013 - 0.024 0.005 ^ 25

Applesauce 190 0 0.005 ^ 25

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 2 0.3 0.006 - 0.012 0.005 - 0.010 10

Lettuce 756 0 0.005 ^ NT

Pears 707 142 20.1 0.003 - 20 0.002 ^ 25.0

Tomatoes 528 4 0.8 0.002 - 0.007 0.001 ^ 10

Tomatoes, Canned 189 0 0.001 ^ 10

TOTAL 3,786 150

Phorate (insecticide) 

Cherries 30 0 0.17 ^ NT

Cherries, Frozen 144 0 0.17 ^ NT

Cranberries 156 0 0.030 ^ NT

Cranberries, Frozen 25 0 0.030 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 675 0 0.020 - 0.060 NT

Green Beans 567 0 0.060 ^ 0.05

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 - 0.006 0.2

Spinach 707 0 0.002 - 0.17 NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 532 0 0.17 ^ NT
Appendix B. Page 79 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,442 0

Phorate oxygen analog (metabolite of Phorate)

Grapefruit 704 0 0.002 - 0.005 NT

Green Beans 567 0 0.001 ^ 0.05

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ 0.2

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 3,773 0

Phorate oxygen analog sulfone (metabolite of Phorate)

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.004 NT

Green Beans 567 0 0.002 ^ 0.05

Olives, Canned 189 0 0.001 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 3,226 0

Phorate oxygen analog sulfoxide (metabolite of Phorate)

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.004 NT

Green Beans 567 0 0.002 ^ 0.05

Olives, Canned 189 0 0.001 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,226 0

Phorate sulfone (metabolite of Phorate)

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.030 ^ NT

Cherries, Frozen 144 0 0.030 ^ NT

Cranberries 156 0 0.025 ^ NT

Cranberries, Frozen 25 0 0.025 ^ NT

Cucumbers 734 0 0.020 - 0.050 NT

Grapefruit 704 0 0.003 - 0.005 NT

Green Beans 567 0 0.005 ^ 0.05

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 689 0 0.020 ^ NT

Potatoes 708 4 0.6 0.005 - 0.095 0.003 ^ 0.2
Appendix B. Page 80 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinach 707 0 0.003 - 0.030 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.030 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 7,909 4

Phorate sulfoxide (metabolite of Phorate)

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.001 ^ NT

Green Beans 567 1 0.2 0.008 ^ 0.001 ^ 0.05

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 4 0.6 0.003 - 0.12 0.002 - 0.005 0.2

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 7,948 5

Phosalone (insecticide) 

Apples 531 0 0.001 ^ 10.0

Applesauce 190 0 0.001 ^ 10.0

Cherries 30 0 0.013 ^ 15.0

Cherries, Frozen 144 0 0.013 ^ 15.0

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Grapes 708 0 0.003 ^ 10.0

Lettuce 756 0 0.001 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.003 ^ 10.0

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.015 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 8,269 0

Phosmet (insecticide) 

Apples 531 17 3.2 0.016 - 0.49 0.010 ^ 10

Applesauce 190 1 0.5 0.014 ^ 0.010 ^ 10

Cherries 30 0 0.025 ^ 10

Cherries, Frozen 144 0 0.025 ^ 10

Cranberries 156 0 0.010 ^ 10

Cranberries, Frozen 25 0 0.010 ^ 10
Appendix B. Page 81 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.010 5

Grapes 708 0 0.015 ^ 10

Green Beans 567 0 0.010 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ 5

Pears 707 12 1.7 0.025 - 0.33 0.015 ^ 10

Spinach 349 0 0.025 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 8 1.5 0.025 - 0.41 0.025 ^ 12

TOTAL 7,580 38

Phosmet oxygen analog (metabolite of Phosmet)

Apples 531 0 0.004 ^ 10

Applesauce 190 0 0.004 ^ 10

Cherries 30 0 0.006 ^ 10

Cherries, Frozen 144 0 0.006 ^ 10

Cranberries 156 0 0.005 ^ 10

Cranberries, Frozen 25 0 0.005 ^ 10

Grapefruit 704 0 0.001 ^ 5

Grapes 708 0 0.002 ^ 10

Green Beans 567 0 0.001 ^ NT

Lettuce 756 0 0.004 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Pears 707 5 0.7 0.003 - 0.079 0.002 ^ 10

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ 12

TOTAL 6,118 5

Phosphamidon (insecticide) 

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.003 ^ NT

Spinach 358 0 0.003 ^ NT

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 4,322 0

Phoxim (insecticide) 

Cherries 30 0 0.024 ^ NT

Cherries, Frozen 144 0 0.024 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Spinach 349 0 0.025 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.025 ^ NT

TOTAL 2,132 0

Picoxystrobin (fungicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT
Appendix B. Page 82 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,604 0

Pinoxaden (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Piperonyl butoxide (insecticide) 

Apples 531 1 0.2 0.052 ^ 0.005 ^ 10

Applesauce 190 0 0.005 ^ 10

Cherries 30 0 0.013 ^ 10

Cherries, Frozen 144 0 0.013 ^ 10

Cranberries 156 0 0.025 ^ 10

Cranberries, Frozen 25 0 0.025 ^ 10

Cucumbers 754 0 0.005 ^ 10

Grapefruit 704 0 0.010 - 0.025 10

Grapes 708 0 0.005 ^ 10

Green Beans 567 0 0.030 ^ 10

Lettuce 756 0 0.005 ^ 10

Olives, Canned 189 0 0.010 ^ 10

Oranges 708 0 0.005 ^ 10

Pears 707 0 0.005 ^ 10

Potatoes 708 0 0.003 ^ 10

Spinach 707 0 0.005 - 0.015 10

Strawberries 530 10 1.9 0.018 - 1.1 0.010 ^ 10

Sweet Potatoes 532 53 10 0.015 - 18 0.015 ^ X - 1 10

Tomatoes 528 5 0.9 0.016 - 0.32 0.003 ^ 10

Tomatoes, Canned 189 0 0.003 ^ 10

TOTAL 9,363 69

Pirimicarb (insecticide) 

Cherries 30 0 0.002 ^ NT

Cherries, Frozen 144 1 0.7 0.011 ^ 0.002 ^ V - 1 NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 5,377 1

Pirimicarb desmethyl (metabolite of Pirimicarb)

Cherries 30 0 0.001 ^ NT

Cherries, Frozen 144 0 0.001 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT
Appendix B. Page 83 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.001 ^ NT

TOTAL 3,594 0

Pirimiphos ethyl (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Pirimiphos methyl (insecticide) 

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 6,331 0

Prallethrin (insecticide) 

Apples 472 0 0.010 ^ 1.0

Applesauce 190 0 0.010 ^ 1.0

Cherries 30 0 0.10 ^ 1.0

Cherries, Frozen 144 0 0.10 ^ 1.0

Cranberries 156 0 0.030 ^ 1.0

Cranberries, Frozen 25 0 0.030 ^ 1.0

Grapefruit 704 0 0.020 - 0.10 1.0

Grapes 708 0 0.030 ^ 1.0

Green Beans 567 0 0.20 ^ 1.0

Lettuce 126 0 0.010 ^ 1.0

Olives, Canned 189 0 0.020 ^ 1.0

Pears 707 0 0.030 ^ 1.0

Spinach 349 0 0.10 ^ 1.0

Strawberries 530 0 0.020 ^ 1.0

Sweet Potatoes 532 0 0.10 ^ 1.0

TOTAL 5,429 0

Primisulfuron methyl (herbicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Prochloraz (fungicide) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT
Appendix B. Page 84 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oranges 708 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 2,539 0

Procymidone (fungicide) 

Apples 472 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Grapes 708 0 0.020 ^ 5.0

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 5,720 0

Profenofos (insecticide) 

Apples 531 0 0.075 ^ NT

Applesauce 190 0 0.075 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.005 ^ NT

Grapes 708 0 0.005 ^ NT

Lettuce 756 0 0.075 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.005 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 7,915 0

Profluralin (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Profoxydim (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Promecarb (insecticide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0
Appendix B. Page 85 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Prometryn (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 14 3.9 0.002 - 0.007 0.001 ^ V - 14 NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 2,860 14

Pronamide (herbicide) 

Apples 531 0 0.002 ^ 0.1

Applesauce 190 0 0.002 ^ 0.1

Cherries 30 0 0.012 ^ 0.1

Cherries, Frozen 144 0 0.012 ^ 0.1

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.003 - 0.050 NT

Grapes 708 0 0.003 ^ 0.1

Green Beans 567 0 0.005 ^ NT

Lettuce 756 13 1.7 0.002 - 0.009 0.002 ^ 1.0

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.003 ^ 0.1

Potatoes 708 0 0.001 ^ NT

Spinach 707 2 0.3 0.002 ^ 0.001 - 0.015 V - 2 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 9,363 15

Propachlor (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 2,860 0

Propamocarb (fungicide) 

Cucumbers 189 83 43.9 0.010 - 0.58 0.010 ^ 1.5

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 216 0 0.010 ^ NT

Strawberries 530 2 0.4 0.002 - 0.006 0.001 ^ V - 2 NT

TOTAL 1,482 85

Propamocarb hydrochloride 5 (fungicide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cranberries 156 0 0.001 ^ NT
Appendix B. Page 86 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 25 0 0.001 ^ NT

Cucumbers 565 277 49 0.011 - 0.78 0.010 ^ 1.5

Grapefruit 346 0 0.001 ^ NT

Green Beans 567 13 2.3 0.001 - 0.14 0.001 ^ V - 13 NT

Lettuce 756 143 18.9 0.002 - 30 0.002 ^ 90

Oranges 492 0 0.010 ^ NT

Spinach 349 2 0.6 0.009 - 0.042 0.001 - 0.005 V - 2 NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 4,509 435

Propanil (herbicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Propaquizafop (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Propargite (insecticide) 

Apples 531 0 0.050 ^ NT

Applesauce 190 0 0.050 ^ NT

Cherries 30 0 0.036 ^ NT

Cherries, Frozen 144 0 0.036 ^ NT

Cranberries 156 0 0.025 ^ NT

Cranberries, Frozen 25 0 0.025 ^ NT

Cucumbers 754 0 0.020 ^ NT

Grapefruit 704 0 0.001 - 0.010 5.0

Grapes 708 0 0.005 ^ 10.0

Lettuce 756 0 0.050 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.020 ^ 10.0

Potatoes 708 0 0.006 ^ 0.1

Spinach 707 0 0.006 - 0.040 NT

Strawberries 530 2 0.4 0.076 - 0.089 0.001 ^ V - 2 NT

Sweet Potatoes 532 0 0.040 ^ NT

Tomatoes 528 0 0.006 ^ NT

Tomatoes, Canned 189 0 0.006 ^ NT

TOTAL 8,089 2

Propetamphos (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.005 ^ NT

Grapes 708 0 0.010 ^ NT

Green Beans 567 0 0.10 ^ 0.1

Lettuce 756 0 0.010 ^ NT
Appendix B. Page 87 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 0 0.010 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.010 NT

Strawberries 530 0 0.005 ^ 0.1

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 9,363 0

Propham (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Propiconazole (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.018 ^ 4.0

Cherries, Frozen 144 11 7.6 0.019 - 0.083 0.018 ^ 4.0

Cranberries 156 0 0.005 ^ 1.0

Cranberries, Frozen 25 1 4 0.013 ^ 0.005 ^ 1.0

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 6 0.9 0.005 - 0.014 0.005 ^ 8.0

Green Beans 567 2 0.4 0.006 - 0.012 0.005 ^ 0.70

Lettuce 756 1 0.1 0.021 ^ 0.010 ^ V - 1 NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 9 1.3 0.010 - 0.018 0.010 ^ 8.0

Potatoes 708 0 0.008 ^ NT

Spinach 707 0 0.008 - 0.020 NT

Strawberries 530 36 6.8 0.005 - 0.16 0.005 ^ 1.3

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 0 0.008 ^ 3.0

Tomatoes, Canned 189 0 0.008 ^ 3.0

TOTAL 7,948 66

Proquinazid (fungicide) 

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,077 0

Prosulfuron (herbicide) 

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.003 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,604 0

Prothioconazole (fungicide) 

Cranberries 156 0 0.10 ^ 2.0

Cranberries, Frozen 25 0 0.10 ^ 2.0
Appendix B. Page 88 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 358 0 0.020 ^ NT

Green Beans 567 0 0.50 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,636 0

Prothiofos (insecticide) 

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.020 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.020 - 0.040 NT

TOTAL 3,405 0

Pymetrozine (insecticide) 

Cherries 30 0 0.081 ^ NT

Cherries, Frozen 144 0 0.081 ^ NT

Cucumbers 754 2 0.3 0.010 - 0.033 0.010 ^ 0.1

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.005 ^ 0.02

Spinach 707 6 0.8 0.008 - 0.17 0.005 - 0.085 0.6

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.085 ^ 0.02

Tomatoes 528 6 1.1 0.008 - 0.042 0.005 ^ 0.2

Tomatoes, Canned 189 0 0.005 ^ 0.2

TOTAL 5,377 14

Pyraclostrobin (fungicide) 

Apples 531 109 20.5 0.003 - 0.12 0.003 ^ 1.5

Applesauce 190 0 0.003 ^ 1.5

Cherries 30 2 6.7 0.004 - 0.005 0.002 ^ 2.5

Cherries, Frozen 144 62 43.1 0.002 - 0.18 0.002 ^ 2.5

Cranberries 156 0 0.001 ^ 4.0

Cranberries, Frozen 25 0 0.001 ^ 4.0

Cucumbers 754 29 3.8 0.003 - 0.028 0.003 ^ 0.5

Grapefruit 704 0 0.001 ^ 2.0

Grapes 708 269 38 0.005 - 0.23 0.003 ^ 2.0

Green Beans 567 99 17.5 0.001 - 0.54 0.001 ^ 0.5

Lettuce 756 23 3 0.003 - 2.5 0.003 ^ 29.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.003 ^ 2.0

Pears 707 152 21.5 0.005 - 0.18 0.003 ^ 1.5

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.04

Spinach 707 71 10 0.002 - 1.7 0.001 - 0.005 29.0

Strawberries 530 259 48.9 0.001 - 0.83 0.001 ^ 1.2

Sweet Potatoes 532 0 0.005 ^ 0.04

Tomatoes 528 129 24.4 0.002 - 0.068 0.001 ^ 1.4

Tomatoes, Canned 189 0 0.001 ^ 1.4

TOTAL 9,363 1,205
Appendix B. Page 89 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pyraflufen (precursor to Pyraflufen ethyl)

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Pyraflufen ethyl (herbicide) 

Apples 531 0 0.010 ^ 0.01

Applesauce 190 0 0.010 ^ 0.01

Grapefruit 358 0 0.001 ^ NT

Grapes 708 0 0.005 ^ 0.01

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ 0.01

Pears 707 0 0.005 ^ 0.01

Strawberries 530 0 0.001 ^ NT

TOTAL 3,969 0

Pyrasulfotole (herbicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Pyrazon (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Pyrazophos (fungicide) 

Cherries 30 0 0.006 ^ NT

Cherries, Frozen 144 0 0.006 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.015 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 3,594 0

Pyrethrins (insecticide) 

Cherries 30 0 0.20 ^ 1.0

Cherries, Frozen 144 0 0.20 ^ 1.0

Spinach 349 0 0.20 ^ 1.0

Sweet Potatoes 532 1 0.2 0.29 ^ 0.20 ^ 1.0

TOTAL 1,055 1

Pyridaben (insecticide, acaricide)

Apples 531 4 0.8 0.005 - 0.071 0.005 ^ 0.75

Applesauce 190 0 0.005 ^ 0.75

Cherries 30 0 0.001 ^ 3.0

Cherries, Frozen 144 0 0.001 ^ 3.0

Cranberries 156 0 0.005 ^ 0.5

Cranberries, Frozen 25 0 0.005 ^ 0.5
Appendix B. Page 90 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cucumbers 754 0 0.005 ^ 0.50

Grapefruit 704 0 0.001 - 0.005 0.9

Grapes 708 0 0.002 ^ 2.0

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ 0.9

Pears 707 43 6.1 0.003 - 0.10 0.002 ^ 0.75

Spinach 349 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ 2.5

Sweet Potatoes 532 0 0.001 ^ NT

TOTAL 7,013 47

Pyridalyl (insecticide) 

Grapefruit 358 0 0.001 - 0.040 NT

Olives, Canned 189 0 0.040 ^ NT

Spinach 349 0 0.005 ^ 20

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 1,958 0

Pyrimethanil (fungicide) 

Apples 531 180 33.9 0.053 - 6.2 0.050 ^ 15

Applesauce 190 35 18.4 0.061 - 1.3 0.050 ^ 15

Cherries 30 3 10 0.008 - 0.62 0.002 - 0.004 10

Cherries, Frozen 144 0 0.002 - 0.004 10

Cranberries 156 0 0.005 ^ 8.0

Cranberries, Frozen 25 0 0.005 ^ 8.0

Cucumbers 754 17 2.3 0.003 - 0.019 0.003 ^ 1.5

Grapefruit 704 28 4 0.005 - 0.017 0.005 ^ 10

Grapes 708 89 12.6 0.008 - 1.6 0.005 ^ 5.0

Green Beans 567 2 0.4 0.004 - 0.32 0.001 ^ V - 2 NT

Lettuce 756 0 0.050 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 41 5.8 0.003 - 0.065 0.003 ^ 10

Pears 707 371 52.5 0.008 - 7.1 0.005 ^ 15

Potatoes 708 2 0.3 0.002 ^ 0.001 ^ 0.05

Spinach 707 1 0.1 0.002 ^ 0.001 - 0.005 V - 1 NT

Strawberries 530 127 24 0.005 - 2.3 0.005 ^ 3.0

Sweet Potatoes 532 0 0.005 ^ 0.05

Tomatoes 528 74 14 0.002 - 0.13 0.001 ^ 0.50

Tomatoes, Canned 189 0 0.001 ^ 0.50

TOTAL 9,363 970

Pyriproxyfen (insecticide, growth regulator)

Apples 531 8 1.5 0.001 - 0.012 0.001 ^ 0.20

Applesauce 190 0 0.001 ^ 0.20

Cherries 30 0 0.002 ^ 1.0

Cherries, Frozen 144 0 0.002 ^ 1.0

Cranberries 156 0 0.001 ^ 1.0

Cranberries, Frozen 25 0 0.001 ^ 1.0

Cucumbers 754 0 0.005 ^ 0.10

Grapefruit 704 0 0.001 - 0.005 0.50

Grapes 708 0 0.001 ^ 2.5

Green Beans 567 4 0.7 0.001 - 0.010 0.001 ^ 0.20

Lettuce 756 0 0.001 ^ 3.0
Appendix B. Page 91 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.001 ^ 1.0

Oranges 708 0 0.005 ^ 0.50

Pears 707 21 3 0.002 - 0.011 0.001 ^ 0.20

Potatoes 708 0 0.002 ^ 0.15

Spinach 707 0 0.002 - 0.005 3.0

Strawberries 530 3 0.6 0.004 - 0.029 0.001 ^ 0.30

Sweet Potatoes 532 0 0.005 ^ 0.15

Tomatoes 528 44 8.3 0.004 - 0.024 0.002 ^ 0.80

Tomatoes, Canned 189 0 0.002 ^ 0.80

TOTAL 9,363 80

Pyroxasulfone (herbicide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Quinalphos (insecticide) 

Cherries 30 0 0.003 - 0.006 NT

Cherries, Frozen 144 0 0.003 - 0.006 NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,594 0

Quinoxyfen (fungicide) 

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Cranberries 156 0 0.001 ^ 1.0

Cranberries, Frozen 25 0 0.001 ^ 1.0

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 198 28 0.003 - 0.14 0.002 ^ 2.0

Lettuce 756 6 0.8 0.023 - 0.39 0.020 ^ 19

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 2 0.6 0.002 ^ 0.001 ^ V - 2 NT

Strawberries 530 112 21.1 0.001 - 0.19 0.001 ^ 1.0

Tomatoes 528 13 2.5 0.002 - 0.017 0.001 ^ 1.7

Tomatoes, Canned 189 0 0.001 ^ 1.7

TOTAL 6,688 331

Quintozene - PCNB (fungicide) (parent of HCB, PCA, PCB and PCPMS)

Cherries 30 0 0.021 ^ NT

Cherries, Frozen 144 0 0.021 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 1 0.1 0.005 ^ 0.005 ^ V - 1 NT

Grapefruit 704 0 0.005 - 0.025 NT

Green Beans 567 0 0.025 ^ 0.1
Appendix B. Page 92 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 9 1.3 0.002 - 0.021 0.001 - 0.003 0.1

Spinach 707 1 0.1 0.002 ^ 0.001 - 0.025 V - 1 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.025 ^ NT

Tomatoes 528 0 0.001 ^ 0.1

Tomatoes, Canned 189 0 0.001 ^ 0.1

TOTAL 6,471 11

Quizalofop (metabolite of Quizalofop ethyl)

Grapefruit 358 0 0.050 ^ NT

Olives, Canned 189 0 0.050 ^ NT

Strawberries 530 0 0.050 ^ NT

TOTAL 1,077 0

Quizalofop ethyl (herbicide) 

Cranberries 156 0 0.025 ^ NT

Cranberries, Frozen 25 0 0.025 ^ NT

Grapefruit 704 0 0.001 - 0.005 NT

Green Beans 567 0 0.35 ^ 0.25

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 2,171 0

Resmethrin (insecticide) 

Cherries 30 0 0.028 ^ 3.0

Cherries, Frozen 144 0 0.028 ^ 3.0

Cucumbers 689 0 0.020 ^ 3.0

Grapefruit 675 0 0.003 - 0.005 3.0

Grapes 708 0 0.002 ^ 3.0

Green Beans 567 0 0.20 ^ 3.0

Olives, Canned 189 0 0.003 ^ 3.0

Oranges 708 0 0.020 ^ 3.0

Pears 707 0 0.002 ^ 3.0

Spinach 260 0 0.060 ^ 3.0

Strawberries 530 0 0.003 ^ 3.0

Sweet Potatoes 532 0 0.030 ^ 3.0

TOTAL 5,739 0

Resmethrin cis (isomer of Resmethrin)

Apples 531 0 0.050 ^ 3.0

Applesauce 190 0 0.050 ^ 3.0

Lettuce 756 0 0.050 ^ 3.0

Potatoes 708 0 0.002 ^ 3.0

Spinach 328 0 0.008 ^ 3.0

Tomatoes 528 0 0.002 ^ 3.0

Tomatoes, Canned 189 0 0.002 ^ 3.0

TOTAL 3,230 0

Resmethrin trans (isomer of Resmethrin)

Apples 531 0 0.050 ^ 3.0

Applesauce 190 0 0.050 ^ 3.0

Lettuce 756 0 0.050 ^ 3.0

Potatoes 708 0 0.002 ^ 3.0
Appendix B. Page 93 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinach 343 0 0.002 - 0.008 3.0

Tomatoes 528 0 0.002 ^ 3.0

Tomatoes, Canned 189 0 0.002 ^ 3.0

TOTAL 3,245 0

Rimsulfuron (herbicide) 

Cranberries 156 0 0.005 ^ 0.01

Cranberries, Frozen 25 0 0.005 ^ 0.01

Cucumbers 754 0 0.010 ^ NT

Grapefruit 646 0 0.003 - 0.005 0.01

Grapes 708 0 0.010 ^ 0.01

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 0.01

Pears 707 0 0.010 ^ 0.01

Strawberries 530 0 0.003 ^ NT

TOTAL 4,423 0

Rotenone (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Saflufenacil (herbicide) 

Apples 531 0 0.010 ^ 0.03

Applesauce 190 0 0.010 ^ 0.03

Cranberries 156 0 0.020 ^ NT

Cranberries, Frozen 25 0 0.020 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.003 - 0.010 0.03

Grapes 708 0 0.010 ^ 0.03

Green Beans 567 0 0.010 ^ 0.03

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ 0.03

Oranges 708 0 0.005 ^ 0.03

Pears 707 0 0.010 ^ 0.03

Strawberries 530 0 0.003 ^ NT

TOTAL 6,525 0

Sedaxane (fungicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Sethoxydim (herbicide) 

Apples 531 0 0.003 ^ 0.2

Applesauce 190 0 0.003 ^ 0.2

Cherries 30 0 0.007 ^ 0.2

Cherries, Frozen 144 0 0.007 ^ 0.2

Cranberries 156 0 0.005 ^ 4.0

Cranberries, Frozen 25 0 0.005 ^ 4.0

Grapefruit 704 0 0.003 - 0.005 0.5

Grapes 708 0 0.001 ^ 1.0

Green Beans 567 0 0.005 ^ 15
Appendix B. Page 94 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Lettuce 724 0 0.003 ^ 4.0

Olives, Canned 189 0 0.003 ^ NT

Pears 707 0 0.001 ^ 0.2

Spinach 29 0 0.015 ^ 4.0

Strawberries 530 0 0.003 ^ 10

Sweet Potatoes 532 0 0.010 ^ 4.0

TOTAL 5,766 0

Simazine (herbicide) 

Apples 531 0 0.005 ^ 0.20

Applesauce 190 0 0.005 ^ 0.20

Cherries 30 0 0.005 ^ 0.25

Cherries, Frozen 144 0 0.005 ^ 0.25

Cranberries 156 0 0.005 ^ 0.25

Cranberries, Frozen 25 0 0.005 ^ 0.25

Grapefruit 704 0 0.001 - 0.010 0.25

Grapes 708 0 0.004 ^ 0.20

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.001 ^ 0.20

Pears 707 0 0.004 ^ 0.25

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 0 0.001 ^ 0.25

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,334 0

Spinetoram (insecticide) 

Apples 531 13 2.4 0.003 - 0.017 0.003 ^ 0.20

Applesauce 190 0 0.003 ^ 0.20

Cherries 30 0 0.005 ^ 0.30

Cherries, Frozen 144 7 4.9 0.005 - 0.011 0.005 ^ 0.30

Cranberries 156 5 3.2 0.001 - 0.002 0.001 ^ 0.50

Cranberries, Frozen 25 0 0.001 ^ 0.50

Cucumbers 754 0 0.010 ^ 0.30

Grapefruit 704 0 0.001 - 0.010 0.30

Grapes 708 0 0.020 ^ 0.50

Green Beans 567 12 2.1 0.001 - 0.010 0.001 ^ 0.30

Lettuce 756 61 8.1 0.003 - 0.20 0.003 ^ 8.0

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.010 ^ 0.30

Pears 707 35 5 0.033 - 0.080 0.020 ^ 0.20

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.10

Spinach 707 341 48.2 0.002 - 0.52 0.001 - 0.010 8.0

Strawberries 530 46 8.7 0.010 - 0.12 0.010 ^ 0.90

Sweet Potatoes 532 0 0.010 ^ 0.10

Tomatoes 528 0 0.001 ^ 0.40

Tomatoes, Canned 189 0 0.001 ^ 0.40

TOTAL 9,363 521

Spinosad (insecticide) (total of spinosyns A and D)

Cranberries 156 0 0.002 ^ 0.40

Cranberries, Frozen 25 0 0.002 ^ 0.40

Cucumbers 754 6 0.8 0.005 - 0.046 0.004 ^ 0.3
Appendix B. Page 95 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.002 - 0.003 0.30

Grapes 708 29 4.1 0.010 - 0.067 0.006 ^ 0.50

Green Beans 567 2 0.4 0.004 - 0.024 0.002 ^ 0.30

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.004 ^ 0.30

Pears 707 5 0.7 0.010 - 0.063 0.006 ^ 0.20

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 0.10

Spinach 358 65 18.2 0.002 - 0.82 0.001 ^ 8.0

Strawberries 530 21 4 0.003 - 0.063 0.003 ^ 0.90

Tomatoes 528 7 1.3 0.002 - 0.020 0.001 ^ 0.40

Tomatoes, Canned 189 0 0.001 ^ 0.40

TOTAL 6,831 136

Spinosad A (isomer of Spinosad) 

Apples 531 3 0.6 0.004 - 0.008 0.003 ^ 0.20

Applesauce 190 0 0.003 ^ 0.20

Cherries 30 2 6.7 0.005 - 0.029 0.003 ^ 0.20

Cherries, Frozen 144 33 22.9 0.003 - 0.037 0.003 ^ 0.20

Lettuce 756 7 0.9 0.004 - 0.23 0.003 ^ 8.0

Spinach 349 39 11.2 0.006 - 1.6 0.005 ^ 8.0

Sweet Potatoes 532 0 0.005 ^ 0.10

TOTAL 2,532 84

Spinosad D (isomer of Spinosad) 

Cherries 30 1 3.3 0.004 ^ 0.003 ^ 0.20

Cherries, Frozen 144 11 7.6 0.004 - 0.007 0.003 ^ 0.20

Spinach 349 26 7.4 0.005 - 0.44 0.005 ^ 8.0

Sweet Potatoes 532 0 0.005 ^ 0.10

TOTAL 1,055 38

Spirodiclofen (acaricide) 

Apples 531 76 14.3 0.010 - 0.085 0.010 ^ 0.80

Applesauce 190 0 0.010 ^ 0.80

Cherries 30 0 0.006 ^ 1.0

Cherries, Frozen 144 0 0.006 ^ 1.0

Cranberries 126 0 0.005 ^ NT

Cranberries, Frozen 23 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 675 0 0.003 - 0.005 0.50

Grapes 708 18 2.5 0.008 - 0.16 0.005 ^ 2.0

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.010 ^ 0.50

Pears 707 81 11.5 0.008 - 0.13 0.005 ^ 0.80

Spinach 349 0 0.010 - 0.050 NT

Strawberries 530 2 0.4 0.098 - 0.28 0.003 ^ V - 2 NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 6,952 177

Spiromesifen Total (parent + enol metabolite) (insecticide) 

Potatoes 708 0 0.008 ^ 0.02

Spinach 358 0 0.002 ^ 12

Tomatoes 527 20 3.8 0.004 - 0.10 0.002 - 0.008 0.45

Tomatoes, Canned 126 0 0.002 ^ 0.45

TOTAL 1,719 20
Appendix B. Page 96 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spiromesifen (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 158 0 0.010 ^ NT

Cranberries 156 0 0.010 ^ 2.0

Cranberries, Frozen 25 0 0.010 ^ 2.0

Cucumbers 754 8 1.1 0.002 - 0.015 0.002 ^ 0.10

Grapefruit 704 0 0.003 - 0.020 NT

Green Beans 567 0 0.020 ^ 0.80

Lettuce 724 0 0.010 ^ 12

Olives, Canned 189 0 0.003 ^ NT

Oranges 669 0 0.002 ^ NT

Strawberries 530 34 6.4 0.003 - 0.27 0.003 ^ 2.0

TOTAL 5,007 42

Spiromesifen alcohol (metabolite of Spiromesifen)

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 69 13 0.001 - 0.16 0.001 ^ 2.0

TOTAL 1,077 69

Spirotetramat (insecticide) 

Apples 531 0 0.002 ^ 0.70

Applesauce 190 0 0.002 ^ 0.70

Cranberries 156 0 0.002 ^ 3.0

Cranberries, Frozen 25 0 0.002 ^ 3.0

Grapefruit 704 0 0.001 ^ 0.60

Grapes 708 161 22.7 0.003 - 0.068 0.002 ^ 1.3

Green Beans 567 0 0.001 ^ 2.5

Lettuce 756 35 4.6 0.002 - 0.40 0.002 ^ 9.0

Olives, Canned 189 0 0.001 ^ NT

Pears 707 143 20.2 0.003 - 0.031 0.002 ^ 0.70

Potatoes 708 0 0.002 - 0.005 0.60

Spinach 358 11 3.1 0.003 - 0.087 0.002 - 0.005 9.0

Strawberries 530 4 0.8 0.015 - 0.11 0.001 ^ 0.40

Sweet Potatoes 532 0 0.005 ^ 0.60

TOTAL 6,661 354

Spiroxamine (fungicide) 

Apples 472 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.003 ^ NT

Cherries, Frozen 144 0 0.003 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Grapes 708 18 2.5 0.002 - 0.010 0.001 ^ 1.0

Lettuce 724 0 0.010 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.005 - 0.010 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 5,688 18
Appendix B. Page 97 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sulfallate (herbicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Sulfentrazone (herbicide) 

Cherries 30 0 0.035 - 0.070 NT

Cherries, Frozen 144 0 0.035 - 0.070 NT

Cranberries 156 0 0.015 ^ 0.15

Cranberries, Frozen 25 0 0.015 ^ 0.15

Grapefruit 704 0 0.010 - 0.015 0.15

Grapes 708 0 0.020 ^ 0.15

Green Beans 567 0 0.015 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Spinach 349 0 0.035 ^ NT

Strawberries 530 0 0.010 ^ 0.15

Sweet Potatoes 532 0 0.035 ^ 0.15

TOTAL 3,934 0

Sulfosulfuron (herbicide) 

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 719 0

Sulfoxaflor (insecticide) 

Cranberries 156 0 0.050 ^ 0.70

Cranberries, Frozen 25 0 0.050 ^ 0.70

Grapefruit 704 19 2.7 0.003 - 0.009 0.003 - 0.10 0.70

Olives, Canned 189 0 0.003 ^ NT

Potatoes 708 0 0.001 ^ 0.05

Spinach 358 7 2 0.002 - 0.14 0.001 ^ 6.0

Strawberries 530 1 0.2 0.023 ^ 0.003 ^ 0.70

Tomatoes 528 72 13.6 0.002 - 0.091 0.001 ^ 0.70

Tomatoes, Canned 189 0 0.001 ^ 0.70

TOTAL 3,387 99

Sulprofos (insecticide) 

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.003 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 2,860 0

TCMTB (fungicide) 

Cranberries 156 0 0.10 ^ NT

Cranberries, Frozen 25 0 0.10 ^ NT

Grapefruit 675 0 0.005 - 0.010 NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,575 0
Appendix B. Page 98 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tebuconazole (fungicide) 

Apples 531 0 0.010 ^ 0.05

Applesauce 190 0 0.010 ^ 0.05

Cherries 30 28 93.3 0.060 - 1.9 0.012 ^ 5.0

Cherries, Frozen 144 50 34.7 0.013 - 1.3 0.012 ^ 5.0

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 9 1.2 0.006 - 0.049 0.005 ^ 0.4

Grapefruit 704 0 0.005 ^ NT

Grapes 708 305 43.1 0.003 - 0.73 0.002 ^ 5.0

Green Beans 567 40 7.1 0.001 - 0.080 0.001 ^ 0.1

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 6 3.2 0.006 - 0.034 0.005 ^ V - 6 NT

Oranges 708 0 0.005 ^ 1.0

Pears 707 1 0.1 0.007 ^ 0.002 ^ 0.05

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.006 - 0.015 NT

Strawberries 530 1 0.2 0.028 ^ 0.005 ^ V - 1 NT

Sweet Potatoes 532 0 0.015 ^ NT

Tomatoes 528 7 1.3 0.003 - 0.058 0.002 ^ 1.3

Tomatoes, Canned 189 0 0.002 ^ 1.3

TOTAL 9,363 447

Tebufenozide (insecticide) 

Apples 531 1 0.2 0.024 ^ 0.002 ^ 1.0

Applesauce 190 0 0.002 ^ 1.0

Cherries 30 0 0.003 - 0.005 NT

Cherries, Frozen 144 0 0.003 - 0.005 NT

Cranberries 156 0 0.002 ^ 1.0

Cranberries, Frozen 25 0 0.002 ^ 1.0

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.020 0.80

Grapes 708 4 0.6 0.003 - 0.051 0.002 ^ 3.0

Lettuce 756 0 0.002 ^ 10.0

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ 0.80

Pears 707 0 0.002 ^ 1.5

Potatoes 708 0 0.003 ^ NT

Spinach 707 1 0.1 0.005 ^ 0.003 - 0.005 10.0

Strawberries 530 0 0.005 ^ 3.0

Sweet Potatoes 532 0 0.005 ^ 0.015

Tomatoes 528 2 0.4 0.019 ^ 0.003 ^ 1.0

Tomatoes, Canned 189 0 0.003 ^ 1.0

TOTAL 8,796 8

Tebufenpyrad (insecticide, acaricide)

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 1 0.7 0.007 ^ 0.005 ^ V - 1 NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,594 1
Appendix B. Page 99 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tebuthiuron (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 2,860 0

Tecnazene (plant growth regulator) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 4,322 0

Teflubenzuron (insecticide) 

Cherries 30 0 0.010 ^ NT

Cherries, Frozen 144 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Spinach 349 0 0.010 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 2,132 0

Tefluthrin (insecticide) 

Apples 531 0 0.002 ^ NT

Applesauce 190 0 0.002 ^ NT

Cherries 30 0 0.009 ^ NT

Cherries, Frozen 144 0 0.009 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.010 NT

Grapes 708 0 0.007 ^ NT

Green Beans 567 0 0.050 ^ NT

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.007 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 9,363 0
Appendix B. Page 100 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tepraloxydim (herbicide) 

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.005 - 0.010 NT

Green Beans 567 0 0.005 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Strawberries 530 0 0.010 ^ NT

TOTAL 2,171 0

Terbacil (herbicide) 

Apples 531 0 0.010 ^ 0.3

Applesauce 190 0 0.010 ^ 0.3

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cucumbers 754 0 0.008 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.008 ^ NT

Potatoes 708 0 0.003 - 0.010 NT

Spinach 707 0 0.003 - 0.020 NT

Strawberries 530 0 0.005 ^ 0.1

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 6,496 0

Terbufos (insecticide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.003 - 0.005 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,604 0

Terbufos oxygen analog (metabolite of Terbufos)

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Grapefruit 346 0 0.001 ^ NT

TOTAL 527 0

Terbufos oxygen analog sulfone (metabolite of Terbufos)

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.010 NT

Strawberries 530 0 0.010 ^ NT

TOTAL 1,415 0

Terbufos oxygen analog sulfoxide (metabolite of Terbufos)

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 346 0 0.005 ^ NT

TOTAL 527 0

Terbufos sulfone (metabolite of Terbufos)

Cranberries 156 0 0.025 ^ NT

Cranberries, Frozen 25 0 0.025 ^ NT
Appendix B. Page 101 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 358 0 0.002 ^ NT

Strawberries 530 0 0.005 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 3,387 0

Terbufos sulfoxide (metabolite of Terbufos)

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Grapefruit 704 0 0.002 - 0.003 NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,604 0

Terbuthylazine (herbicide) 

Cherries 30 0 0.002 ^ NT

Cherries, Frozen 144 0 0.002 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.005 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 3,594 0

Tetrachlorvinphos (insecticide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 704 0 0.001 - 0.005 NT

Green Beans 567 0 0.005 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Potatoes 708 0 0.003 ^ NT

Spinach 358 0 0.003 ^ NT

Strawberries 530 0 0.001 ^ NT

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 3,954 0

Tetraconazole (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.005 ^ NT

Grapes 708 58 8.2 0.003 - 0.10 0.002 ^ 0.20

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 6 1.7 0.002 - 0.006 0.001 ^ V - 6 NT

Strawberries 530 41 7.7 0.005 - 0.12 0.005 ^ 0.25

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 5,045 105
Appendix B. Page 102 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tetradifon (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.020 ^ NT

Cherries, Frozen 144 0 0.020 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.010 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.002 ^ NT

Spinach 707 0 0.002 - 0.020 NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.020 ^ NT

Tomatoes 528 0 0.002 ^ NT

Tomatoes, Canned 189 0 0.002 ^ NT

TOTAL 6,854 0

Tetrahydrophthalimide - THPI (metabolite of Captafol and Captan)

Apples 531 65 12.2 0.011 - 0.61 0.010 ^ 25.0

Applesauce 190 142 74.7 0.012 - 0.51 0.010 ^ 25.0

Grapefruit 358 0 0.020 ^ NT

Lettuce 756 0 0.010 ^ 0.05

Olives, Canned 189 0 0.020 ^ NT

Potatoes 648 0 0.004 - 0.012 0.05

Spinach 343 1 0.3 0.006 ^ 0.004 ^ 0.05

Strawberries 530 272 51.3 0.022 - 3.1 0.020 ^ 20.0

Tomatoes 470 37 7.9 0.006 - 0.089 0.004 ^ X - 3 0.05

Tomatoes, Canned 189 1 0.5 0.006 ^ 0.004 ^ 0.05

TOTAL 4,204 518

Tetramethrin (insecticide) 

Apples 531 0 0.005 ^ NT

Applesauce 190 0 0.005 ^ NT

Cherries 30 0 0.10 ^ NT

Cherries, Frozen 144 0 0.10 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 589 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.010 NT

Grapes 708 0 0.002 ^ NT

Green Beans 567 0 0.050 ^ NT

Lettuce 756 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Pears 707 0 0.002 ^ NT

Spinach 349 0 0.10 ^ NT

Strawberries 530 0 0.005 ^ NT

Sweet Potatoes 532 0 0.10 ^ NT

TOTAL 7,415 0

Thiabendazole (fungicide) (parent of 5-hydroxythiabendazole)

Apples 531 334 62.9 0.002 - 3.3 0.002 ^ 5.0

Applesauce 190 54 28.4 0.002 - 0.89 0.002 ^ 5.0

Cherries 30 0 0.005 ^ NT
Appendix B. Page 103 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cherries, Frozen 144 0 0.005 ^ NT

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ 0.02

Grapefruit 704 490 69.6 0.002 - 0.15 0.001 - 0.016 10.0

Grapes 708 0 0.003 ^ NT

Lettuce 756 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 524 74 0.010 - 0.42 0.010 ^ 10.0

Pears 696 228 32.8 0.005 - 3.5 0.003 ^ 5.0

Potatoes 708 47 6.6 0.002 - 3.1 0.001 ^ 10.0

Spinach 707 0 0.001 - 0.005 0.02

Strawberries 530 6 1.1 0.011 - 1.1 0.001 ^ 5.0

Sweet Potatoes 532 108 20.3 0.005 - 3.0 0.005 ^ 10

Tomatoes 528 1 0.2 0.002 ^ 0.001 ^ V - 1 NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 8,785 1,792

Thiacloprid (insecticide) 

Apples 531 24 4.5 0.001 - 0.031 0.001 ^ 0.30

Applesauce 190 3 1.6 0.001 - 0.002 0.001 ^ 0.30

Cherries 30 2 6.7 0.013 - 0.016 0.005 ^ 0.5

Cherries, Frozen 144 41 28.5 0.006 - 0.095 0.005 ^ 0.5

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Lettuce 756 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Pears 707 31 4.4 0.008 - 0.11 0.005 ^ 0.30

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,561 101

Thiamethoxam (insecticide) (also a parent of Clothianidin)

Apples 531 9 1.7 0.003 - 0.015 0.003 ^ 0.2

Applesauce 190 0 0.003 ^ 0.2

Cherries 30 0 0.005 - 0.010 0.5

Cherries, Frozen 144 39 27.1 0.006 - 0.34 0.005 - 0.010 0.5

Cranberries 156 0 0.010 ^ 0.02

Cranberries, Frozen 25 0 0.010 ^ 0.02

Cucumbers 754 74 9.8 0.010 - 0.25 0.010 ^ 0.2

Grapefruit 704 13 1.8 0.001 - 0.023 0.001 - 0.005 0.40

Grapes 708 0 0.025 ^ 0.20

Green Beans 567 0 0.005 ^ 0.02

Lettuce 756 137 18.1 0.003 - 0.22 0.003 ^ 4.0

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ 0.40

Pears 707 0 0.025 ^ 0.2

Potatoes 708 29 4.1 0.008 - 0.022 0.005 ^ 0.25

Spinach 707 56 7.9 0.005 - 0.55 0.005 ^ 4.0

Strawberries 530 87 16.4 0.001 - 0.12 0.001 ^ 0.30
Appendix B. Page 104 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 532 0 0.005 ^ 0.02

Tomatoes 528 29 5.5 0.008 - 0.028 0.005 ^ 0.25

Tomatoes, Canned 189 0 0.005 ^ 0.25

TOTAL 9,363 473

Thiazopyr (herbicide) 

Apples 531 0 0.008 ^ NT

Applesauce 190 0 0.008 ^ NT

Cranberries 156 0 0.001 ^ NT

Cranberries, Frozen 25 0 0.001 ^ NT

Grapefruit 704 0 0.001 - 0.003 0.05

Lettuce 756 0 0.008 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 3,081 0

Thidiazuron (plant growth regulator) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Thiencarbazone methyl (herbicide) 

Grapefruit 358 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ NT

Strawberries 530 0 0.020 ^ NT

TOTAL 1,077 0

Thifensulfuron methyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Thiobencarb (herbicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.003 ^ NT

Lettuce 756 0 0.010 ^ 0.2

Olives, Canned 189 0 0.003 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.003 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 4,337 0

Thiodicarb (insecticide) 

Apples 531 0 0.003 ^ NT

Applesauce 190 0 0.003 ^ NT

Grapefruit 358 0 0.010 ^ NT

Lettuce 756 0 0.003 ^ 35

Olives, Canned 189 0 0.010 ^ NT

Spinach 349 0 0.010 ^ 35
Appendix B. Page 105 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 3,435 0

Thionazin (insecticide, fumigant)

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 1,077 0

Thiophanate methyl (fungicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Grapefruit 346 0 0.005 ^ NT

Green Beans 535 23 4.3 0.005 - 0.025 0.005 ^ 2.0

TOTAL 1,062 23

Tolclofos methyl (fungicide) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Tolfenpyrad (insecticide) 

Grapefruit 358 0 0.005 ^ 1.5

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Tolylfluanid (fungicide) 

Cherries 30 0 0.048 ^ NT

Cherries, Frozen 144 0 0.048 ^ NT

Grapes 708 0 0.030 ^ 11

Sweet Potatoes 532 0 0.050 ^ NT

TOTAL 1,414 0

Topramezone (herbicide) 

Grapefruit 346 0 0.25 ^ NT

TOTAL 346 0

Tri-Allate (herbicide) 

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.005 ^ NT

Green Beans 567 0 0.008 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 3,106 0

Triadimefon (fungicide) (also a parent of Triadimenol)

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 358 0 0.003 ^ NT

Olives, Canned 189 0 0.003 ^ NT
Appendix B. Page 106 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.005 NT

Strawberries 530 0 0.003 ^ NT

Sweet Potatoes 532 0 0.005 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 5,377 0

Triadimenol (fungicide) (also a metabolite of Triadimefon)

Cherries 30 0 0.017 - 0.034 NT

Cherries, Frozen 144 0 0.017 - 0.034 NT

Cranberries 156 0 0.025 ^ NT

Cranberries, Frozen 25 0 0.025 ^ NT

Cucumbers 754 0 0.005 ^ NT

Grapefruit 704 0 0.005 - 0.020 NT

Grapes 708 4 0.6 0.017 - 0.42 0.010 ^ V - 4 NT

Olives, Canned 189 0 0.020 ^ NT

Oranges 708 0 0.005 ^ NT

Spinach 349 0 0.020 - 0.10 NT

Strawberries 530 0 0.020 ^ NT

Sweet Potatoes 472 0 0.020 - 0.040 NT

TOTAL 4,769 4

Triasulfuron (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Triazophos (insecticide) 

Cherries 30 0 0.005 ^ NT

Cherries, Frozen 144 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.010 ^ NT

Strawberries 530 0 0.001 ^ NT

Sweet Potatoes 532 0 0.010 ^ NT

TOTAL 3,245 0

Tribenuron methyl (herbicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Trichlorfon (insecticide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cranberries 156 0 0.040 ^ NT

Cranberries, Frozen 25 0 0.040 ^ NT

Grapefruit 704 0 0.003 - 0.020 NT

Lettuce 756 0 0.010 ^ NT
Appendix B. Page 107 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.003 ^ NT

Strawberries 530 3 0.6 0.004 - 0.009 0.003 ^ V - 3 NT

TOTAL 3,081 3

Triclopyr (herbicide) 

Grapefruit 358 0 0.25 ^ NT

Olives, Canned 189 0 0.25 ^ NT

Strawberries 530 0 0.25 ^ NT

TOTAL 1,077 0

Tricyclazole (fungicide) 

Grapefruit 358 0 0.001 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 1,077 0

Trifloxystrobin (fungicide) 

Apples 531 49 9.2 0.002 - 0.016 0.002 ^ 0.5

Applesauce 190 0 0.002 ^ 0.5

Cherries 30 0 0.005 ^ 2

Cherries, Frozen 144 44 30.6 0.006 - 0.083 0.005 ^ 2

Cranberries 156 0 0.001 ^ 1.5

Cranberries, Frozen 25 0 0.001 ^ 1.5

Cucumbers 754 0 0.005 ^ 0.50

Grapefruit 704 1 0.1 0.001 ^ 0.001 ^ 0.6

Grapes 708 175 24.7 0.005 - 0.18 0.003 ^ 2.0

Green Beans 567 1 0.2 0.013 ^ 0.001 ^ V - 1 NT

Lettuce 756 1 0.1 0.27 ^ 0.002 ^ 30

Olives, Canned 189 0 0.001 ^ NT

Oranges 708 0 0.005 ^ 0.6

Pears 707 1 0.1 0.005 ^ 0.003 ^ 0.5

Potatoes 708 0 0.001 ^ 0.04

Spinach 707 1 0.1 0.048 ^ 0.001 - 0.005 30

Strawberries 530 63 11.9 0.002 - 0.14 0.001 ^ 1.5

Sweet Potatoes 532 0 0.005 ^ 0.04

Tomatoes 528 11 2.1 0.002 - 0.014 0.001 ^ 0.5

Tomatoes, Canned 189 0 0.001 ^ 0.5

TOTAL 9,363 347

Trifloxysulfuron (herbicide) 

Apples 531 0 0.020 ^ NT

Applesauce 190 0 0.020 ^ NT

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Grapefruit 704 0 0.001 - 0.005 0.03

Lettuce 724 0 0.020 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 3,049 0

Triflumizole (fungicide) 

Apples 531 0 0.010 ^ 0.50

Applesauce 190 0 0.010 ^ 0.50

Cherries 30 0 0.002 ^ 1.5

Cherries, Frozen 144 25 17.4 0.003 - 0.24 0.002 ^ 1.5
Appendix B. Page 108 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 15 2 0.003 - 0.047 0.003 ^ 0.5

Grapefruit 704 0 0.003 - 0.005 NT

Grapes 708 36 5.1 0.002 - 0.015 0.001 ^ 2.5

Green Beans 567 0 0.001 ^ NT

Lettuce 756 0 0.010 ^ 35

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.003 ^ NT

Pears 707 0 0.001 ^ 0.50

Spinach 349 0 0.005 ^ NT

Strawberries 530 40 7.5 0.003 - 0.18 0.003 ^ 2.0

Sweet Potatoes 532 0 0.005 ^ NT

TOTAL 7,580 116

Trifluralin (herbicide) 

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Cherries 30 0 0.009 ^ 0.05

Cherries, Frozen 144 0 0.009 ^ 0.05

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ 0.05

Grapefruit 704 0 0.005 - 0.010 0.05

Grapes 708 0 0.002 ^ 0.05

Green Beans 567 0 0.005 ^ 0.05

Lettuce 756 2 0.3 0.001 - 0.002 0.001 ^ V - 2 NT

Olives, Canned 189 0 0.010 ^ NT

Oranges 708 0 0.005 ^ 0.05

Potatoes 708 2 0.3 0.002 ^ 0.001 ^ 0.05

Spinach 707 3 0.4 0.002 - 0.025 0.001 - 0.010 V - 3 NT

Strawberries 530 0 0.010 ^ NT

Sweet Potatoes 532 0 0.010 ^ 0.05

Tomatoes 528 1 0.2 0.002 ^ 0.001 ^ 0.05

Tomatoes, Canned 189 2 1.1 0.002 ^ 0.001 ^ 0.05

TOTAL 8,656 10

Triforine (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Grapefruit 358 0 0.10 ^ NT

Lettuce 756 0 0.010 ^ NT

Olives, Canned 189 0 0.10 ^ NT

Strawberries 530 0 0.10 ^ NT

TOTAL 2,554 0

Triticonazole (fungicide) 

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.010 ^ NT

Grapefruit 704 0 0.005 - 0.025 NT

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.010 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 3,066 0
Appendix B. Page 109 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Uniconazole (insect growth regulator) 

Grapefruit 358 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ NT

Strawberries 530 0 0.005 ^ NT

TOTAL 1,077 0

Vernolate (herbicide) 

Cucumbers 754 0 0.010 ^ NT

Oranges 708 0 0.010 ^ NT

TOTAL 1,462 0

Vinclozolin (fungicide) 

Apples 531 0 0.010 ^ NT

Applesauce 190 0 0.010 ^ NT

Cherries 30 0 0.010 ^ 25.0

Cherries, Frozen 144 0 0.010 ^ 25.0

Cucumbers 754 0 0.005 ^ 1.0

Grapefruit 358 0 0.005 ^ NT

Grapes 708 0 0.002 ^ 6.0

Lettuce 756 0 0.010 ^ 10.0

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ NT

Potatoes 708 0 0.001 ^ NT

Spinach 707 0 0.001 - 0.010 NT

Strawberries 530 0 0.005 ^ 10.0

Sweet Potatoes 532 0 0.010 ^ NT

Tomatoes 528 0 0.001 ^ NT

Tomatoes, Canned 189 0 0.001 ^ NT

TOTAL 7,562 0

Zoxamide (fungicide) 

Cranberries 156 0 0.002 ^ NT

Cranberries, Frozen 25 0 0.002 ^ NT

Grapefruit 704 0 0.001 - 0.002 NT

Green Beans 567 0 0.002 ^ NT

Olives, Canned 189 0 0.001 ^ NT

Strawberries 530 0 0.001 ^ NT

TOTAL 2,171 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

EX2 = Exempt from the requirement of a tolerance in or on all food commodities when used to control insect larvae.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 Emamectin benzoate is the salt form of the active, Emamectin.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2016 and not to the current year. There may be instances where a tolerance was recently set or revoked 

that would have an effect on whether a residue is violative or not. 
Appendix B. Page 110 of 110

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

2 Halosulfuron methyl is the salt form of the active, Halosulfuron.

3 Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

4 Specific tolerance established for methamidophos in green beans and lettuce as a possible result of an acephate application.

5 Propamocarb analytically determined as the salt (hydrochloride).

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

pages 1 and 2 in Appendix J to see the sample origin (domestic, imported, or unknown) for each occurrence.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 3 through 5 in Appendix J to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.
Appendix C

Distribution of Residues by Pesticide

in Eggs 

Appendix C shows residue detections for all compounds tested in eggs, including range of values 

detected, range of Limits of Detection (LODs), and U.S. Environmental Protection Agency (EPA) 

tolerance references for each pair. The EPA tolerances cited in this summary and appendixes 

apply to 2016 and not to the current year. There may be instances where tolerances have been 

recently set, modified, or revoked that would have an effect on whether a residue is violative or 

not. 

In 2016, the Pesticide Data Program (PDP) analyzed 294 egg samples. PDP detected just one 

pesticide in the egg samples, the insect growth regulator Cyromazine, which was detected in two 

samples at a concentration of 0.050 ppm where the established tolerance was 0.25 ppm.

Results for environmental contaminants across all commodities, including eggs, have been 

consolidated in a separate appendix because they have no registered uses and are not applied 

to crops (see Appendix E). 
Appendix C. Page 1 of 3

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Abamectin I 294 0.040 ^ 0.01

Acephate I 294 0.040 ^ 0.1

Acetamiprid I 294 0.040 ^ 0.010

Alachlor H 294 0.040 ^ 0.02

Azinphos methyl I 294 0.040 ^ NT

Azinphos methyl oxygen analog IM 294 0.040 ^ NT

Bendiocarb I 294 0.040 ^ SU

Benoxacor S 294 0.040 ^ 0.01

Bentazon H 294 0.040 ^ 0.05

Bifenthrin I 294 0.040 ^ 0.05

Boscalid F 294 0.040 ^ 0.02

Carbaryl I 294 0.040 ^ 0.5

Carbendazim (MBC) F 294 0.040 ^ NT

Carbofuran I 294 0.040 ^ NT

Carboxin F 294 0.040 ^ 0.05

Chlorantraniliprole I 294 0.040 ^ 1.0

Chlorfenapyr I 294 0.040 ^ 0.01

Chlorpyrifos I 294 0.040 ^ 0.1

Chlorpyrifos methyl I 294 0.040 ^ 0.1

Chlorpyrifos oxygen analog IM 294 0.040 ^ 0.1

Clothianidin I 294 0.040 ^ 0.02

Cyfluthrin I 294 0.040 ^ 0.01

Cyhalothrin, Lambda I 294 0.040 ^ 0.01

Cypermethrin I 294 0.040 ^ 0.05

Cyphenothrin I 294 0.040 ^ NT

Cyromazine R 294 2 0.7 0.050 ^ 0.040 ^ 0.25

Deltamethrin 1 I 294 0.040 ^ 0.02

Dichlorvos (DDVP) I 294 0.040 ^ 0.5

Dicofol o,p' I 294 0.040 ^ 0.05

Dicofol p,p' I 294 0.040 ^ 0.05

Difenoconazole F 294 0.040 ^ 0.02

Diflubenzuron I 294 0.040 ^ 0.07

Dimethoate I 294 0.040 ^ 0.02

Dinotefuran I 294 0.040 ^ 0.01

EPN I 294 0.040 ^ NT

Esfenvalerate+Fenvalerate Total I 294 0.080 ^ 0.03

Etofenprox I 294 0.040 ^ 0.40

Fenpropathrin I 294 0.040 ^ 0.05

Fipronil I 294 0.040 ^ 0.03

Flonicamid I 294 0.040 ^ 0.04

Fluazifop butyl H 294 0.040 ^ 0.05

Flubendiamide I 294 0.040 ^ 0.40

APPENDIX C. DISTRIBUTION OF RESIDUES BY PESTICIDE IN EGGS
Appendix C. Page 2 of 3

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fluometuron H 294 0.040 ^ 0.1

Fluopyram F 294 0.040 ^ 0.08

Flupyradifurone I 294 0.040 ^ 0.01

Fluridone H 117 0.040 ^ 0.05

Flutolanil F 294 0.040 ^ 0.05

Flutriafol F 294 0.040 ^ 0.01

Fluvalinate I 294 0.040 ^ NT

Fluxapyroxad F 294 0.040 ^ 0.01

Hexythiazox I 294 0.040 ^ 0.05

3-Hydroxycarbofuran IM 294 0.040 ^ NT

Imidacloprid I 294 0.040 ^ 0.02

Imiprothrin I 294 0.040 ^ NT

Indoxacarb I 294 0.040 ^ 0.20

Iprodione F 294 0.040 ^ 1.5

Malathion I 294 0.040 ^ 0.1

Malathion oxygen analog IM 294 0.040 ^ 0.1

Metalaxyl/Mefenoxam 2 F 294 0.040 ^ 0.05

Metconazole F 294 0.040 ^ 0.04

Methamidophos I 294 0.040 ^ 0.02

Methoxyfenozide I 294 0.040 ^ 0.02

Metolachlor H 294 0.040 ^ 0.02

Metribuzin H 294 0.040 ^ 0.01

Myclobutanil F 294 0.040 ^ 0.02

1-Naphthol IM 294 0.040 ^ 0.5

Novaluron I 294 0.040 ^ 1.5

Omethoate IM 294 0.040 ^ 0.02

Oxydemeton methyl I 294 0.040 ^ 0.01

Oxydemeton methyl sulfone IM 294 0.040 ^ 0.01

Oxyfluorfen H 294 0.040 ^ 0.03

Pentachlorobenzene (PCB) FM 294 0.040 ^ NT

Permethrin Total I 294 0.040 ^ 0.10

Phenothrin I 294 0.040 ^ 0.01

Phosmet I 294 0.040 ^ NT

Phosmet oxygen analog IM 294 0.040 ^ NT

Picoxystrobin F 294 0.040 ^ 0.01

Pinoxaden H 294 0.040 ^ 0.06

Piperonyl butoxide I 294 0.040 ^ 10

Prallethrin I 294 0.040 ^ 1.0

Primisulfuron methyl H 294 0.040 ^ 0.10

Pronamide H 294 0.040 ^ 0.02

Propanil H 294 0.040 ^ 0.30

Propargite I 294 0.040 ^ 0.1

Propetamphos I 294 0.040 ^ NT

Pyraclostrobin F 294 0.040 ^ NT
Appendix C. Page 3 of 3

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Pyrethrins I 294 0.040 ^ 1.0

Pyriproxyfen I 294 0.040 ^ 0.10

Quintozene (PCNB) F 294 0.040 ^ NT

Sethoxydim H 294 0.040 ^ 2.0

Simazine H 294 0.040 ^ 0.03

Spinetoram I 176 0.040 ^ 0.04

Spinetoram J IM 118 0.040 ^ 0.04

Spinetoram L IM 118 0.040 ^ 0.04

Spinosad I 176 0.040 ^ 0.30

Spinosad A IM 118 0.040 ^ 0.30

Spinosad D IM 118 0.040 ^ 0.30

Spirotetramat I 294 0.040 ^ 0.02

Sulfoxaflor I 294 0.040 ^ NT

Tefluthrin I 294 0.040 ^ NT

Tetrachlorvinphos I 294 0.040 ^ 0.2

Tetraconazole F 294 0.040 ^ 0.02

Tetramethrin I 294 0.040 ^ NT

Thiamethoxam I 294 0.040 ^ 0.02

Thiobencarb H 294 0.040 ^ 0.2

Trifloxystrobin F 294 0.040 ^ 0.04

Triflumizole F 294 0.040 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

NT = No tolerance level was set for that pesticide/commodity pair.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 = Deltamethrin includes parent Tralomethrin.

2 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

R = Insect Growth Regulator

S = Herbicide Safener

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply 

to 2016 and not to the current year. There may be instances where a tolerance was recently set or revoked that 

would have an effect on whether a residue is violative or not. 
Appendix D

Distribution of Residues by Pesticide

in Milk 

Appendix D shows residue detections for all compounds tested in milk, including range of 

values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this 

summary and appendixes apply to 2016 and not to the current year. There may be 

instances where tolerances have been recently set, modified, or revoked that would have 

an effect on whether a residue is violative or not. 

In 2016, the Pesticide Data Program (PDP) analyzed 708 milk samples. PDP detected 

just one pesticide in the milk samples, the insecticide Flubendiamide, which was detected 

in 18 samples at concentrations ranging from 0.003 to 0.006 ppm where the established 

tolerance was 0.15 ppm.

Results for environmental contaminants across all commodities, including milk, have 

been consolidated in a separate appendix because they have no registered uses and are 

not applied to crops (see Appendix E). 
Appendix D. Page 1 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

2,4,5-T H 531 0.10 ^ NT

2,4-D H 531 0.050 ^ 0.05

2,4-DB H 531 0.10 ^ NT

2,4-dimethylphenyl formamide (2,4-DMPF) I 708 0.005 ^ NT

2,6-DIPN P 708 0.010 ^ 0.02

Abamectin I 708 0.020 ^ 0.015

Acephate I 708 0.005 ^ 0.1

Acetamiprid I 708 0.0012 ^ 0.30

Acetochlor H 708 0.005 ^ NT

Acifluorfen H 708 0.050 ^ NT

Alachlor H 708 0.010 ^ 0.02

Aldicarb I 708 0.005 ^ NT

Aldicarb sulfone IM 708 0.0026 ^ NT

Aldicarb sulfoxide IM 708 0.0026 ^ NT

Allethrin I 708 0.010 ^ NT

Ametoctradin F 708 0.0012 ^ NT

Ametryn H 708 0.0012 ^ NT

Amicarbazone H 708 0.005 ^ 0.01

Asulam H 708 0.0012 ^ 0.05

Atrazine H 708 0.0012 ^ 0.02

Azinphos ethyl I 708 0.005 ^ NT

Azinphos methyl I 708 0.005 ^ NT

Azinphos methyl oxygen analog IM 708 0.0026 ^ NT

Azoxystrobin F 708 0.0012 ^ 0.006

Benalaxyl F 708 0.010 ^ NT

Benazolin H 708 0.050 ^ NT

Bendiocarb I 708 0.0012 ^ SU

Benfluralin H 708 0.005 ^ NT

Benoxacor S 708 0.0026 ^ 0.01

Bensulide H 708 0.005 ^ NT

Bentazon H 708 0.0026 ^ 0.02

Bifenazate A 708 0.0026 ^ 0.02

Bifenox H 708 0.010 - 0.020 NT

Bifenthrin I 708 0.0026 ^ 0.1

Bitertanol F 708 0.010 ^ NT

Boscalid F 708 0.0026 ^ 0.10

Bromacil H 708 0.010 ^ NT

Bromopropylate A 708 0.0026 ^ NT

Bromoxynil H 708 0.010 ^ 0.4

Bromuconazole F 708 0.005 ^ NT

Bupirimate F 708 0.0012 ^ NT

Buprofezin I 708 0.0012 ^ 0.01

Butylate H 708 0.020 ^ NT

Cadusafos I 708 0.0012 ^ NT

Carbaryl I 708 0.0026 ^ 1.0

APPENDIX D. DISTRIBUTION OF RESIDUES BY PESTICIDE IN MILK
Appendix D. Page 2 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carbendazim (MBC) F 708 0.0012 ^ NT

Carbofuran I 708 0.0012 ^ NT

Carbophenothion I 708 0.010 ^ NT

Carboxin F 708 0.0026 ^ 0.05

Carfentrazone ethyl H 708 0.0026 ^ 0.05

Chlorantraniliprole I 708 0.005 ^ 0.1

Chlorethoxyfos I 708 0.020 ^ NT

Chlorfenapyr I 708 0.25 ^ 0.01

Chlorfenvinphos total I 708 0.0012 ^ NT

Chlorimuron ethyl H 708 0.0026 ^ NT

Chlorobenzilate A 708 0.0026 ^ NT

Chloroneb F 708 0.005 ^ 0.05

Chlorothalonil F 562 0.005 ^ 0.1

Chlorpropham H 708 0.0026 ^ 0.30

Chlorpyrifos I 708 0.0026 ^ 0.25

Chlorpyrifos oxygen analog IM 708 0.0012 ^ 0.25

Chlorsulfuron H 708 0.0012 ^ 0.1

Clethodim H 708 0.010 ^ 0.05

Clofentezine I 708 0.005 ^ 0.01

Clomazone H 708 0.0026 ^ NT

Cloransulam Methyl H 708 0.0012 ^ NT

Clothianidin I 708 0.0012 ^ 0.01

Coumaphos I 708 0.0012 ^ 0.5

Coumaphos oxygen analog IM 708 0.0012 ^ 0.5

Crotoxyphos I 708 0.0026 ^ NT

Crufomate I 708 0.0026 ^ NT

Cyantraniliprole I 708 0.0026 ^ 0.01

Cyazofamid F 708 0.010 ^ NT

Cyclanilide P 708 0.020 ^ 0.04

Cyflufenamid F 708 0.0012 ^ NT

Cyflumetofen A 708 0.0026 ^ NT

Cyfluthrin I 708 0.010 ^ 0.2

Cyhalothrin, Total 1 I 708 0.010 ^ 0.4

Cymoxanil F 708 0.010 ^ NT

Cypermethrin I 708 0.020 ^ 2.5

Cyphenothrin I 708 0.010 ^ NT

Cyproconazole F 708 0.005 ^ 0.02

Cyprodinil F 708 0.005 ^ NT

Cyprosulfamide S 708 0.0026 ^ NT

Cyromazine R 708 0.005 ^ 0.05

DCPA H 708 0.0026 ^ NT

DEF (Tribufos) H 708 0.0012 ^ 0.01

Deltamethrin 2 I 708 0.005 ^ 0.1

Demeton-O IM 708 0.010 ^ NT

Demeton-S IM 708 0.010 ^ NT

Demeton-S sulfone IM 708 0.0012 ^ NT

Dialifos I 708 0.005 ^ NT
Appendix D. Page 3 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Diazinon I 708 0.0012 ^ NT

Diazinon oxygen analog IM 708 0.0012 ^ NT

Dicamba H 531 0.25 ^ 0.2

Dichlobenil H 708 0.0012 ^ NT

Dichlormid H 708 0.020 ^ NT

Dichlorprop H 708 0.050 ^ NT

Dichlorvos (DDVP) I 708 0.020 ^ 0.5

Dicloran F 708 0.020 ^ NT

Diclosulam H 708 0.010 ^ NT

Dicofol o,p' I 708 0.005 ^ 22.0

Dicofol p,p' I 708 0.005 ^ 22.0

Dicrotophos I 708 0.0012 ^ NT

Diethofencarb F 708 0.0026 ^ NT

Difenoconazole F 708 0.0026 ^ 0.02

Diflubenzuron I 708 0.0012 ^ 0.05

Dimethenamid H 708 0.0012 ^ NT

Dimethoate I 708 0.0012 ^ 0.002

Dimethomorph F 708 0.0026 ^ NT

Diniconazole F 708 0.005 ^ NT

Dinotefuran I 708 0.0026 ^ 0.05

Dioxacarb I 708 0.0012 ^ NT

Dioxathion I 708 0.005 ^ NT

Diphenamid H 708 0.005 ^ NT

Diphenylamine (DPA) F 708 0.0026 ^ 0.01

Disulfoton I 708 0.020 ^ NT

Disulfoton sulfone IM 708 0.0012 ^ NT

Disulfoton sulfoxide IM 708 0.0012 ^ NT

Diuron H 708 0.010 ^ NT

DMST (4-dimethylaminosulphotosluidide) FM 708 0.0026 ^ NT

Dodine F 708 0.010 ^ NT

Emamectin I 708 0.010 ^ 0.003

Endosulfan I IM 708 0.020 ^ 2.0

Endosulfan II IM 708 0.010 ^ 2.0

Endosulfan sulfate IM 708 0.010 ^ 2.0

EPN I 678 0.020 ^ NT

Epoxiconazole F 708 0.0026 ^ NT

Esfenvalerate I 619 0.005 ^ 0.3

Ethalfluralin H 708 0.010 ^ NT

Ethiofencarb I 708 0.0026 ^ NT

Ethiofencarb sulfone IM 708 0.0026 ^ NT

Ethiofencarb sulfoxide IM 708 0.0012 ^ NT

Ethion I 708 0.0012 ^ NT

Ethion mono oxon IM 708 0.0012 ^ NT

Ethiprole I 708 0.005 ^ NT

Ethofumesate H 708 0.0026 ^ NT

Ethoprop I 708 0.0012 ^ NT

Ethylan I 708 0.0026 ^ NT
Appendix D. Page 4 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Etofenprox I 592 0.0012 - 0.020 0.60

Etoxazole A 708 0.0012 ^ 0.01

Etridiazole F 708 0.040 ^ NT

Famoxadone F 708 0.010 ^ 0.06

Fenamidone F 708 0.0012 ^ 0.02

Fenamiphos I 708 0.0012 ^ NT

Fenamiphos sulfone IM 708 0.0012 ^ NT

Fenamiphos sulfoxide IM 708 0.0026 ^ NT

Fenarimol F 708 0.0026 ^ NT

Fenazaquin I 708 0.0012 ^ NT

Fenbuconazole F 708 0.0026 ^ NT

Fenchlorphos I 708 0.0026 ^ NT

Fenhexamid F 708 0.010 ^ NT

Fenitrothion I 708 0.005 ^ NT

Fenobucarb (BPMC) I 708 0.0026 ^ NT

Fenoxaprop ethyl H 708 0.0012 ^ 0.02

Fenoxycarb I 708 0.0012 ^ NT

Fenpropathrin I 708 0.005 ^ 0.08

Fenpropidin F 708 0.040 ^ NT

Fenpropimorph F 708 0.0012 ^ NT

Fenpyrazamine F 708 0.020 ^ NT

Fenpyroximate A 708 0.0012 ^ 0.015

Fensulfothion I 708 0.0012 ^ NT

Fenthion I 708 0.0026 ^ NT

Fenthion sulfone IM 708 0.020 ^ NT

Fenthion sulfoxide IM 708 0.020 ^ NT

Fenuron H 708 0.005 ^ NT

Fipronil I 708 0.0026 ^ 0.05

Fipronil sulfone (MB46136) IM 708 0.0026 ^ 0.05

Flazasulfuron H 708 0.005 ^ NT

Flonicamid I 708 0.010 ^ 0.05

Fluazifop H 708 0.050 ^ NT

Fluazifop butyl H 708 0.0012 ^ 0.05

Fluazinam F 708 0.0026 ^ NT

Flubendiamide I 708 18 2.5 0.003 - 0.006 0.0026 ^ 0.15

Flucythrinate I 708 0.010 ^ NT

Fludioxonil F 708 0.010 ^ 0.01

Flufenacet H 708 0.010 ^ NT

Flufenoxuron I 708 0.0012 ^ 0.20

Flufenpyr ethyl H 708 0.0012 ^ NT

Flumetsulam H 708 0.0026 ^ NT

Flumiclorac pentyl H 708 0.0012 ^ NT

Flumioxazin H 708 0.020 ^ NT

Fluometuron H 708 0.0026 ^ 0.02

Fluopicolide F 708 0.0012 ^ NT

Fluopyram F 708 0.0012 ^ 0.40

Fluoxastrobin F 708 0.0012 ^ 0.03
Appendix D. Page 5 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Flupyradifurone I 708 0.0012 ^ 0.15

Fluquinconazole F 708 0.0026 ^ NT

Fluridone H 708 0.0012 ^ 0.05

Fluroxypyr HM 708 0.050 ^ 0.3

Flusilazole F 708 0.0012 ^ NT

Fluthiacet methyl H 708 0.0026 ^ NT

Flutolanil F 708 0.0012 ^ 0.05

Flutriafol F 708 0.0012 ^ 0.02

Fluvalinate I 678 0.010 ^ NT

Fluxapyroxad F 708 0.0012 ^ 0.02

Fomesafen H 708 0.005 ^ NT

Fonofos I 708 0.0026 ^ NT

Forchlorfenuron P 708 0.0012 ^ NT

Formetanate hydrochloride I 708 0.0012 ^ NT

Fosthiazate T 708 0.0012 ^ NT

Furalaxyl F 708 0.010 ^ NT

Halosulfuron methyl H 708 0.020 ^ 0.05

Haloxyfop H 708 0.020 ^ NT

Heptenophos I 708 0.010 ^ NT

Hexaconazole F 708 0.005 ^ NT

Hexazinone H 708 0.005 ^ 11

Hexythiazox I 708 0.0012 ^ 0.05

Hydroprene R 708 0.020 ^ 0.2

3-Hydroxycarbofuran IM 708 0.0012 ^ NT

5-Hydroxythiabendazole FM 708 0.0012 ^ 0.1

Imazalil F 708 0.0026 ^ 0.02

Imazapic H 708 0.005 ^ 0.1

Imazaquin H 708 0.010 ^ NT

Imazethapyr H 708 0.020 ^ NT

Imazosulfuron H 708 0.0026 ^ NT

Imidacloprid I 708 0.0026 ^ 0.10

Imiprothrin I 708 0.010 ^ NT

Indaziflam H 708 0.0012 ^ NT

Indoxacarb I 708 0.005 ^ 0.15

Ipconazole F 708 0.0026 ^ NT

Iprodione F 708 0.010 ^ 0.5

Iprovalicarb F 708 0.0026 ^ NT

Isocarbophos I 708 0.010 ^ NT

Isofenphos I 708 0.0026 ^ NT

Isofenphos methyl IM 708 0.005 ^ NT

Isoprocarb I 708 0.005 ^ NT

Isoproturon H 708 0.0026 ^ NT

Isoxadifen ethyl S 708 0.005 ^ NT

Kresoxim-methyl F 708 0.005 ^ NT

Lactofen H 708 0.0026 ^ NT

Lenacil H 708 0.0026 ^ NT

Leptophos oxygen analog IM 708 0.0026 ^ NT
Appendix D. Page 6 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Linuron H 708 0.0026 ^ 0.05

Lufenuron I 708 0.005 ^ NT

Malathion I 708 0.0026 ^ 0.5

Malathion oxygen analog IM 708 0.0012 ^ 0.5

Mandipropamid F 708 0.0026 ^ NT

MCPA H 531 0.25 ^ 0.1

MCPB H 531 0.25 ^ NT

Mecarbam I 708 0.020 ^ NT

Mecoprop (MCPP) H 708 0.25 ^ NT

Mefenpyr diethyl S 708 0.0026 ^ NT

Mepanipyrim F 708 0.0012 ^ NT

Metaflumizone I 708 0.010 ^ NT

Metalaxyl/Mefenoxam 3 F 708 0.0012 ^ 0.02

Metaldehyde O 708 0.10 ^ NT

Metconazole F 708 0.0026 ^ NT

Methamidophos I 708 0.0012 ^ 0.1

Methidathion I 708 0.0026 ^ NT

Methiocarb I 708 0.0012 ^ NT

Methiocarb sulfone IM 708 0.0026 ^ NT

Methiocarb sulfoxide IM 708 0.0012 ^ NT

Methomyl I 708 0.010 ^ NT

Methoxychlor p,p' IM 708 0.005 ^ NT

Methoxyfenozide I 708 0.0026 ^ 0.10

Metolachlor H 708 0.0026 ^ 0.02

Metolcarb I 708 0.010 ^ NT

Metrafenone F 708 0.0012 ^ NT

Metribuzin H 708 0.005 ^ 0.05

Metsulfuron methyl H 708 0.0012 ^ 0.05

Mevinphos Total I 708 0.0026 ^ NT

MGK-264 I 708 0.005 ^ 5

Monocrotophos I 708 0.0026 ^ NT

Monolinuron H 708 0.0012 ^ NT

Myclobutanil F 708 0.0026 ^ 0.2

Napropamide H 708 0.005 ^ NT

Nicosulfuron H 708 0.0012 ^ 0.01

Nitrapyrin N 708 0.020 ^ NT

Nitrofen H 708 0.020 ^ NT

Norflurazon H 708 0.0026 ^ 0.1

Norflurazon desmethyl HM 708 0.0026 ^ 0.1

Novaluron I 708 0.020 ^ 1.0

Omethoate IM 708 0.0012 ^ 0.002

Oryzalin H 708 0.020 ^ NT

Oxadiazon H 708 0.0026 ^ NT

Oxadixyl F 708 0.005 ^ NT

Oxamyl I 708 0.005 ^ NT

Oxamyl oxime IM 708 0.005 ^ NT

Oxydemeton methyl I 708 0.0012 ^ 0.01
Appendix D. Page 7 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Oxydemeton methyl sulfone IM 708 0.0012 ^ 0.01

Oxyfluorfen H 708 0.020 ^ 0.01

Paclobutrazol P 708 0.005 ^ NT

Parathion ethyl I 708 0.005 ^ NT

Parathion methyl I 708 0.020 ^ NT

Parathion methyl oxygen analog IM 708 0.010 ^ NT

Parathion oxygen analog IM 708 0.0026 ^ NT

Penconazole F 708 0.0026 ^ NT

Pencycuron F 708 0.0026 ^ NT

Pendimethalin H 708 0.010 ^ 0.04

Penflufen F 708 0.0012 ^ NT

Penoxsulam H 177 0.0012 ^ NT

Pentachloroaniline (PCA) FM 708 0.0026 ^ NT

Pentachlorobenzene (PCB) FM 708 0.005 ^ NT

Pentachlorophenyl methyl sulfide FM 708 0.020 ^ NT

Penthiopyrad F 708 0.0012 ^ 0.02

Permethrin cis IM 708 0.010 ^ 3.0

Permethrin trans IM 708 0.010 ^ 3.0

Phenothrin I 708 0.005 ^ 0.01

Phenthoate I 708 0.0012 ^ NT

Phorate I 708 0.020 ^ NT

Phorate oxygen analog IM 708 0.005 ^ NT

Phorate oxygen analog sulfone IM 708 0.0012 ^ NT

Phorate oxygen analog sulfoxide IM 708 0.0012 ^ NT

Phorate sulfone IM 708 0.0026 ^ NT

Phorate sulfoxide IM 708 0.0012 ^ NT

Phosalone I 708 0.0026 ^ NT

Phosmet I 708 0.0012 ^ 0.1

Phosmet oxygen analog IM 708 0.0012 ^ 0.1

Phosphamidon I 708 0.005 ^ NT

Phoxim I 708 0.0012 ^ NT

Picoxystrobin F 708 0.005 ^ 0.01

Pinoxaden H 708 0.020 ^ 0.02

Piperonyl butoxide I 708 0.010 ^ 10

Pirimicarb I 708 0.0012 ^ NT

Pirimicarb desmethyl IM 708 0.0012 ^ NT

Pirimiphos methyl I 708 0.0012 ^ NT

Pirimiphos-ethyl I 708 0.0012 ^ NT

Prallethrin I 708 0.020 ^ 1.0

Primisulfuron methyl H 708 0.005 ^ 0.02

Prochloraz F 708 0.005 ^ NT

Procymidone F 708 0.005 ^ NT

Profenofos I 708 0.005 ^ 0.01

Profluralin H 708 0.020 ^ NT

Profoxydim H 708 0.0026 ^ NT

Promecarb I 708 0.0012 ^ NT

Prometryn H 708 0.0012 ^ NT
Appendix D. Page 8 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Pronamide H 708 0.0026 ^ 0.02

Propachlor H 708 0.0012 ^ 0.02

Propamocarb F 708 0.0012 ^ NT

Propanil H 708 0.010 ^ 0.05

Propaquizafop H 708 0.0012 ^ NT

Propargite I 708 0.0012 ^ 2.0

Propetamphos I 708 0.005 ^ NT

Propham H 708 0.0026 ^ NT

Propiconazole F 708 0.005 ^ 0.05

Proquinazid F 708 0.010 ^ NT

Prosulfuron H 708 0.0026 ^ NT

Prothiofos I 708 0.005 ^ NT

Pymetrozine I 708 0.0012 ^ NT

Pyraclostrobin F 708 0.0012 ^ 0.1

Pyraflufen HM 708 0.020 ^ NT

Pyraflufen ethyl H 708 0.0012 ^ 0.03

Pyrasulfotole H 708 0.005 ^ 0.03

Pyrazon H 708 0.0012 ^ 0.02

Pyrazophos F 708 0.0012 ^ NT

Pyridaben I 708 0.0012 ^ 0.01

Pyridalyl I 679 0.0012 - 0.040 NT

Pyrimethanil F 708 0.005 ^ 0.05

Pyriproxyfen I 708 0.0012 ^ 0.10

Pyroxasulfone H 708 0.0026 ^ 0.003

Quinalphos I 708 0.0012 ^ NT

Quinoxyfen F 708 0.0012 ^ NT

Quintozene (PCNB) F 708 0.005 ^ NT

Quizalofop HM 708 0.050 ^ NT

Quizalofop ethyl H 708 0.0012 ^ 0.01

Resmethrin I 708 0.0026 ^ 3.0

Rimsulfuron H 708 0.0026 ^ NT

Rotenone I 708 0.0026 ^ NT

Saflufenacil H 708 0.0026 ^ 0.01

Sedaxane F 708 0.005 ^ NT

Sethoxydim H 708 0.0026 ^ 0.5

Simazine H 708 0.0012 ^ 0.03

Spinetoram I 708 0.010 ^ 0.30

Spinosad I 708 0.0026 ^ 7.0

Spirodiclofen A 708 0.0026 ^ 0.01

Spiromesifen I 708 0.0026 ^ 0.01

Spiromesifen alcohol IM 708 0.0012 ^ 0.01

Spirotetramat I 708 0.0012 ^ 0.01

Spiroxamine F 708 0.0012 ^ NT

Sulfallate H 708 0.005 ^ NT

Sulfentrazone H 708 0.010 ^ NT

Sulfosulfuron H 708 0.005 ^ 0.02

Sulfoxaflor I 708 0.0026 ^ 0.15
Appendix D. Page 9 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sulprofos I 708 0.0026 ^ NT

TCMTB F 708 0.005 ^ NT

Tebuconazole F 708 0.005 ^ 0.1

Tebufenozide I 708 0.005 ^ 0.04

Tebufenpyrad I 708 0.0012 ^ NT

Tebuthiuron H 708 0.0012 ^ 0.8

Tecnazene P 708 0.010 ^ NT

Teflubenzuron I 708 0.005 ^ NT

Tefluthrin I 708 0.005 ^ NT

Tepraloxydim H 708 0.010 ^ 0.10

Terbacil H 708 0.005 ^ NT

Terbufos I 708 0.0026 ^ NT

Terbufos oxygen analog sulfone IM 649 0.010 - 0.020 NT

Terbufos sulfone IM 708 0.005 ^ NT

Terbufos sulfoxide IM 708 0.0026 ^ NT

Terbuthylazine H 708 0.0012 ^ NT

Tetrachlorvinphos I 708 0.0012 ^ 0.05

Tetraconazole F 708 0.005 ^ 0.03

Tetradifon I 708 0.010 ^ 0.4

Tetrahydrophthalimide (THPI) FM 708 0.020 ^ 0.10

Tetramethrin I 708 0.005 ^ NT

Thiabendazole F 708 0.0012 ^ 0.1

Thiacloprid I 708 0.0012 ^ 0.030

Thiamethoxam I 708 0.0012 ^ 0.02

Thiazopyr H 708 0.0026 ^ NT

Thidiazuron P 708 0.005 ^ 0.05

Thiencarbazone methyl H 708 0.020 ^ 0.02

Thifensulfuron methyl H 708 0.0012 ^ NT

Thiobencarb H 708 0.0026 ^ 0.05

Thiodicarb I 708 0.010 ^ NT

Thionazin I 708 0.0026 ^ NT

Tolclofos methyl F 708 0.005 ^ NT

Tolfenpyrad I 708 0.005 ^ 0.03

Tri Allate H 708 0.005 ^ NT

Triadimefon F 708 0.0026 ^ NT

Triadimenol F 708 0.020 ^ NT

Triasulfuron H 708 0.0012 ^ 0.02

Triazophos I 708 0.0012 ^ NT

Tribenuron methyl H 708 0.0012 ^ NT

Trichlorfon I 708 0.0026 ^ NT

Triclopyr H 708 0.25 ^ 0.60

Tricyclazole F 708 0.0012 ^ NT

Trifloxystrobin F 708 0.0012 ^ 0.02

Trifloxysulfuron H 708 0.0012 ^ NT

Triflumizole F 708 0.0026 ^ NT

Trifluralin H 708 0.010 ^ NT

Triforine F 708 0.10 ^ NT
Appendix D. Page 10 of 10

Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Triticonazole F 708 0.005 ^ NT

Uniconazole R 708 0.005 ^ NT

Vinclozolin F 708 0.005 ^ 0.05

Zoxamide F 708 0.0012 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

NT = No tolerance level was set for that pesticide/commodity pair.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 = Includes cyhalothrin lambda plus R157836 epimer.

2 = Includes parent Tralomethrin.

3 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

N = Nitrification Inhibitor

O = Molluscicide

P = Plant Growth Regulator

R = Insect Growth Regulator

S = Herbicide Safener

T = Nematicide

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply 

to 2016 and not to the current year. There may be instances where a tolerance was recently set or revoked that 

would have an effect on whether a residue is violative or not. 
Appendix E

Distribution of Residues 

for Environmental Contaminants

Appendix E shows residue detections across all commodities for 22 compounds identified 

as environmental contaminants, including range of values detected, range of Limits of 

Detection (LODs), and U.S. Environmental Protection Agency (EPA) tolerances or Action 

Levels for each pair. Results for environmental contaminants have been consolidated in 

this appendix because they have no registered uses and are not applied to crops.

The EPA tolerances cited in this summary and appendixes apply to 2016 and not to the 

current year. There may be instances where tolerances have been recently set, modified 

or revoked that would have an effect on whether a residue is violative or not.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by the U.S. Food and Drug Administration (FDA). Under the Food Quality 

Protection Act, responsibility for establishing tolerances in lieu of ALs has been transferred 

to EPA. In the interim, ALs are used.
Appendix E. Page 1 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Aldrin (insecticide) (parent of Dieldrin)

Apples 531 0 0.003 ^ 0.03 AL

Applesauce 190 0 0.003 ^ 0.03 AL

Cherries 30 0 0.041 ^ 0.3 AL

Cherries, Frozen 144 0 0.041 ^ 0.3 AL

Cranberries 156 0 0.005 ^ 0.05 AL

Cranberries, Frozen 25 0 0.005 ^ 0.05 AL

Cucumbers 754 0 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.03 AL

Grapefruit 704 0 0.010 ^ 0.02 AL

Grapes 708 0 0.003 ^ 0.05 AL

Green Beans 567 0 0.010 ^ 0.05 AL

Lettuce 756 0 0.003 ^ 0.03 AL

Milk 708 0 0.010 ^ 0.3 AL

Olives, Canned 189 0 0.010 ^ 0.05 AL

Oranges 708 0 0.005 ^ 0.02 AL

Pears 707 0 0.003 ^ 0.03 AL

Potatoes 708 0 0.001 - 0.003 0.1 AL

Spinach 707 0 0.001 - 0.040 0.05 AL

Strawberries 530 0 0.010 ^ 0.05 AL

Sweet Potatoes 468 0 0.045 ^ 0.1 AL

Tomatoes 528 0 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 10,301 0

BHC alpha (insecticide) (isomer of BHC)

Apples 531 0 0.012 ^ 0.05 AL

Applesauce 190 0 0.012 ^ 0.05 AL

Cherries 30 0 0.007 ^ 0.05 AL

Cherries, Frozen 144 0 0.007 ^ 0.05 AL

Cranberries 156 0 0.010 ^ 0.05 AL

Cranberries, Frozen 25 0 0.010 ^ 0.05 AL

Cucumbers 754 0 0.005 ^ 0.05 AL

Eggs 294 0 0.040 ^ 0.05 AL

Grapefruit 704 0 0.003 - 0.005 0.05 AL

Grapes 708 0 0.001 ^ 0.05 AL

Green Beans 567 0 0.020 ^ 0.05 AL

Lettuce 756 0 0.012 ^ 0.05 AL

Milk 708 0 0.0026 ^ 0.3 AL

Olives, Canned 189 0 0.003 ^ 0.05 AL

Oranges 708 0 0.005 ^ 0.05 AL

Pears 707 0 0.001 ^ 0.05 AL

Potatoes 708 0 0.001 ^ 0.05 AL

Spinach 707 0 0.001 - 0.010 0.05 AL

Strawberries 530 0 0.003 ^ 0.05 AL

Sweet Potatoes 532 0 0.010 ^ 0.05 AL

Tomatoes 528 0 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 10,365 0

BHC beta (isomer of BHC)

Apples 531 0 0.014 ^ 0.05 AL

Applesauce 190 0 0.014 ^ 0.05 AL

Cranberries 156 0 0.005 ^ 0.05 AL

Cranberries, Frozen 25 0 0.005 ^ 0.05 AL

Cucumbers 754 0 0.005 ^ 0.05 AL

APPENDIX E. DISTRIBUTION OF RESIDUES FOR ENVIRONMENTAL CONTAMINANTS
Appendix E. Page 2 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Grapefruit 704 0 0.003 - 0.010 0.05 AL

Grapes 708 0 0.001 ^ 0.05 AL

Green Beans 567 0 0.020 ^ 0.05 AL

Lettuce 756 0 0.014 ^ 0.05 AL

Milk 708 0 0.0026 ^ 0.3 AL

Olives, Canned 189 0 0.003 ^ 0.05 AL

Oranges 708 0 0.005 ^ 0.05 AL

Pears 707 0 0.001 ^ 0.05 AL

Strawberries 530 0 0.003 ^ 0.05 AL

TOTAL 7,233 0

BHC delta (isomer of BHC)

Grapefruit 358 0 0.005 ^ 0.05 AL

Milk 708 0 0.005 ^ 0.3 AL

Olives, Canned 189 0 0.005 ^ 0.05 AL

Strawberries 530 0 0.005 ^ 0.05 AL

TOTAL 1,785 0

Chlordane Total (insecticide) 

Grapes 708 0 0.012 ^ 0.1 AL

Pears 707 0 0.012 ^ 0.1 AL

TOTAL 1,415 0

Chlordane cis (isomer of Chlordane)

Apples 472 0 0.010 ^ 0.1 AL

Applesauce 190 0 0.010 ^ 0.1 AL

Cherries 30 0 0.005 ^ 0.1 AL

Cherries, Frozen 144 0 0.005 ^ 0.1 AL

Cranberries 156 0 0.010 ^ NT

Cranberries, Frozen 25 0 0.010 ^ NT

Cucumbers 754 2 0.3 0.008 - 0.009 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ NT

Grapefruit 704 0 0.005 - 0.025 0.1 AL

Green Beans 567 0 0.025 ^ 0.1 AL

Lettuce 756 0 0.010 ^ 0.1 AL

Milk 708 0 0.005 ^ NT

Olives, Canned 189 0 0.005 ^ 0.1 AL

Oranges 708 0 0.005 ^ 0.1 AL

Potatoes 708 3 0.4 0.002 ^ 0.001 ^ 0.1 AL

Spinach 707 4 0.6 0.002 ^ 0.001 - 0.010 0.1 AL

Strawberries 530 0 0.005 ^ 0.1 AL

Sweet Potatoes 532 0 0.010 ^ 0.1 AL

Tomatoes 528 0 0.001 ^ 0.1 AL

Tomatoes, Canned 189 0 0.001 ^ 0.1 AL

TOTAL 8,891 9

Chlordane trans (isomer of Chlordane)

Apples 472 0 0.010 ^ 0.1 AL

Applesauce 190 0 0.010 ^ 0.1 AL

Cherries 30 0 0.005 ^ 0.1 AL

Cherries, Frozen 144 0 0.005 ^ 0.1 AL

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ NT

Grapefruit 704 0 0.005 - 0.010 0.1 AL

Green Beans 567 0 0.010 ^ 0.1 AL

Lettuce 756 0 0.010 ^ 0.1 AL

Milk 708 0 0.005 ^ NT
Appendix E. Page 3 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Olives, Canned 189 0 0.005 ^ 0.1 AL

Oranges 708 0 0.005 ^ 0.1 AL

Potatoes 708 0 0.001 ^ 0.1 AL

Spinach 707 3 0.4 0.002 ^ 0.001 - 0.010 0.1 AL

Strawberries 530 0 0.005 ^ 0.1 AL

Sweet Potatoes 532 0 0.010 ^ 0.1 AL

Tomatoes 528 0 0.001 ^ 0.1 AL

Tomatoes, Canned 189 0 0.001 ^ 0.1 AL

TOTAL 8,891 3

DDD o,p' (metabolite of DDT)

Apples 531 0 0.001 ^ 0.1 AL

Applesauce 190 0 0.001 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.5 AL

Grapefruit 358 0 0.001 ^ 0.1 AL

Lettuce 756 0 0.001 ^ 0.5 AL

Milk 708 0 0.0012 ^ 1.25 AL

Olives, Canned 189 0 0.001 ^ 0.1 AL

Potatoes 708 0 0.001 ^ 1 AL

Spinach 358 2 0.6 0.002 - 0.003 0.001 ^ 0.5 AL

Strawberries 530 0 0.001 ^ 0.1 AL

Tomatoes 528 0 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 5,339 2

DDD p,p' (metabolite of DDT)

Apples 502 0 0.005 ^ 0.1 AL

Applesauce 190 0 0.005 ^ 0.1 AL

Cherries 30 0 0.005 ^ 0.2 AL

Cherries, Frozen 144 0 0.005 ^ 0.2 AL

Cranberries 156 0 0.005 ^ 0.1 AL

Cranberries, Frozen 25 0 0.005 ^ 0.1 AL

Cucumbers 754 0 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.5 AL

Grapefruit 645 0 0.003 - 0.025 0.1 AL

Green Beans 567 0 0.025 ^ 0.2 AL

Lettuce 724 0 0.005 ^ 0.5 AL

Milk 500 0 0.0026 ^ 1.25 AL

Oranges 708 0 0.005 ^ 0.1 AL

Potatoes 708 1 0.1 0.002 ^ 0.001 ^ 1 AL

Spinach 707 2 0.3 0.002 ^ 0.001 - 0.005 0.5 AL

Strawberries 530 0 0.003 ^ 0.1 AL

Sweet Potatoes 532 1 0.2 0.021 ^ 0.005 ^ 1 AL

Tomatoes 528 0 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 8,433 4

DDE o,p' (metabolite of DDT)

Apples 502 0 0.001 ^ 0.1 AL

Applesauce 190 0 0.001 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.5 AL

Grapefruit 358 0 0.005 ^ 0.1 AL

Grapes 708 0 0.002 ^ 0.05 AL

Lettuce 756 0 0.001 ^ 0.5 AL

Milk 708 0 0.005 ^ 1.25 AL

Olives, Canned 189 0 0.005 ^ 0.1 AL

Pears 707 0 0.002 ^ 0.1 AL

Strawberries 530 0 0.005 ^ 0.1 AL

TOTAL 4,942 0
Appendix E. Page 4 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

DDE p,p' (metabolite of DDT)

Apples 531 0 0.010 ^ 0.1 AL

Applesauce 190 0 0.010 ^ 0.1 AL

Cherries 30 0 0.005 ^ 0.2 AL

Cherries, Frozen 144 0 0.005 ^ 0.2 AL

Cranberries 156 0 0.005 ^ 0.1 AL

Cranberries, Frozen 25 0 0.005 ^ 0.1 AL

Cucumbers 754 0 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.5 AL

Grapefruit 704 0 0.001 - 0.010 0.1 AL

Grapes 708 1 0.1 0.003 ^ 0.002 ^ 0.05 AL

Green Beans 567 0 0.005 ^ 0.2 AL

Lettuce 756 0 0.010 ^ 0.5 AL

Milk 708 0 0.0012 ^ 1.25 AL

Olives, Canned 189 0 0.001 ^ 0.1 AL

Oranges 708 0 0.005 ^ 0.1 AL

Pears 707 0 0.002 ^ 0.1 AL

Potatoes 708 118 16.7 0.002 - 0.012 0.001 - 0.003 1 AL

Spinach 707 277 39.2 0.002 - 0.057 0.001 - 0.005 0.5 AL

Strawberries 530 0 0.001 ^ 0.1 AL

Sweet Potatoes 532 1 0.2 0.009 ^ 0.005 ^ 1 AL

Tomatoes 528 1 0.2 0.002 ^ 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 10,365 398

DDT o,p' (insecticide) 

Eggs 294 0 0.040 ^ 0.5 AL

Grapefruit 329 0 0.005 ^ 0.1 AL

Grapes 708 0 0.002 ^ 0.05 AL

Milk 589 0 0.005 ^ 1.25 AL

Olives, Canned 64 0 0.005 ^ 0.1 AL

Pears 707 0 0.002 ^ 0.1 AL

Potatoes 708 10 1.4 0.002 ^ 0.001 ^ 1 AL

Spinach 358 24 6.7 0.002 - 0.005 0.001 ^ 0.5 AL

Strawberries 530 0 0.005 ^ 0.1 AL

Tomatoes 528 0 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 5,004 34

DDT p,p' (insecticide) 

Apples 531 0 0.001 ^ 0.1 AL

Applesauce 190 0 0.001 ^ 0.1 AL

Cherries 30 0 0.075 ^ 0.2 AL

Cherries, Frozen 144 0 0.075 ^ 0.2 AL

Cucumbers 710 0 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.5 AL

Grapefruit 358 0 0.005 ^ 0.1 AL

Grapes 708 0 0.002 ^ 0.05 AL

Lettuce 756 6 0.8 0.001 - 0.002 0.001 ^ 0.5 AL

Milk 708 0 0.005 ^ 1.25 AL

Olives, Canned 189 0 0.005 ^ 0.1 AL

Oranges 708 0 0.005 ^ 0.1 AL

Pears 707 0 0.002 ^ 0.1 AL

Potatoes 689 31 4.5 0.002 - 0.014 0.001 ^ 1 AL

Spinach 358 54 15.1 0.002 - 0.010 0.001 - 0.003 0.5 AL

Strawberries 530 0 0.005 ^ 0.1 AL

Sweet Potatoes 532 0 0.075 ^ 1 AL
Appendix E. Page 5 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 528 0 0.001 ^ 0.05 AL

Tomatoes, Canned 189 0 0.001 ^ 0.05 AL

TOTAL 8,859 91

Dieldrin (insecticide) (also a metabolite of Aldrin)

Apples 531 0 0.010 ^ 0.03 AL

Applesauce 190 0 0.010 ^ 0.03 AL

Cherries 30 0 0.040 ^ 0.3 AL

Cherries, Frozen 144 0 0.040 ^ 0.3 AL

Cranberries 156 0 0.025 ^ 0.05 AL

Cranberries, Frozen 25 0 0.025 ^ 0.05 AL

Cucumbers 754 36 4.8 0.006 - 0.054 0.005 ^ 0.1 AL

Eggs 294 0 0.040 ^ 0.03 AL

Grapefruit 704 0 0.020 - 0.025 0.02 AL

Grapes 708 0 0.005 ^ 0.05 AL

Green Beans 567 0 0.025 ^ 0.05 AL

Lettuce 756 0 0.010 ^ 0.03 AL

Milk 708 0 0.020 ^ 0.3 AL

Olives, Canned 189 0 0.020 ^ 0.05 AL

Oranges 708 0 0.005 ^ 0.02 AL

Pears 707 0 0.005 ^ 0.03 AL

Potatoes 708 11 1.6 0.004 ^ 0.002 ^ 0.1 AL

Spinach 707 15 2.1 0.004 ^ 0.002 - 0.040 0.05 AL

Strawberries 530 0 0.020 ^ 0.05 AL

Sweet Potatoes 532 0 0.045 ^ 0.1 AL

Tomatoes 528 0 0.002 ^ 0.05 AL

Tomatoes, Canned 189 0 0.002 ^ 0.05 AL

TOTAL 10,365 62

Endrin (insecticide) 

Apples 531 0 0.010 ^ 0.03 AL

Applesauce 190 0 0.010 ^ 0.03 AL

Cherries 30 0 0.031 ^ 0.03 AL

Cherries, Frozen 144 0 0.031 ^ 0.03 AL

Cranberries 156 0 0.005 ^ 0.05 AL

Cranberries, Frozen 25 0 0.005 ^ 0.05 AL

Cucumbers 754 0 0.005 ^ 0.05 AL

Eggs 294 0 0.040 ^ 0.03 AL

Grapefruit 704 0 0.010 - 0.030 0.02 AL

Green Beans 567 0 0.003 ^ 0.05 AL

Lettuce 756 0 0.010 ^ 0.05 AL

Milk 708 0 0.010 ^ 0.3 AL

Olives, Canned 189 0 0.010 ^ 0.05 AL

Oranges 708 0 0.005 ^ 0.02 AL

Pears 707 0 0.003 ^ 0.03 AL

Potatoes 708 0 0.005 ^ 0.05 AL

Spinach 707 0 0.005 - 0.035 0.05 AL

Strawberries 530 0 0.010 ^ 0.05 AL

Sweet Potatoes 532 0 0.035 ^ 0.05 AL

Tomatoes 528 0 0.005 ^ 0.05 AL

Tomatoes, Canned 189 0 0.005 ^ 0.05 AL

TOTAL 9,657 0

Heptachlor (insecticide) 

Apples 531 0 0.002 ^ 0.01 AL

Applesauce 190 0 0.002 ^ 0.01 AL

Cherries 30 0 0.10 ^ 0.05 AL

Cherries, Frozen 144 0 0.10 ^ 0.05 AL
Appendix E. Page 6 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cranberries 156 0 0.001 ^ 0.05 AL

Cranberries, Frozen 25 0 0.001 ^ 0.05 AL

Cucumbers 754 0 0.005 ^ 0.05 AL

Eggs 294 0 0.040 ^ 0.05 AL

Grapefruit 704 0 0.005 ^ 0.05 AL

Grapes 708 0 0.001 ^ 0.05 AL

Green Beans 567 0 0.005 ^ 0.05 AL

Lettuce 756 0 0.002 ^ 0.05 AL

Milk 708 0 0.005 ^ 0.1 AL

Olives, Canned 189 0 0.005 ^ 0.01 AL

Oranges 708 0 0.005 ^ 0.05 AL

Pears 707 0 0.001 ^ 0.05 AL

Potatoes 708 0 0.001 - 0.003 0.01 AL

Spinach 707 0 0.001 - 0.10 0.05 AL

Strawberries 530 0 0.005 ^ 0.05 AL

Sweet Potatoes 532 0 0.10 ^ 0.01 AL

Tomatoes 528 0 0.001 ^ 0.01 AL

Tomatoes, Canned 189 0 0.001 - 0.003 0.01 AL

TOTAL 10,365 0

Heptachlor epoxide (metabolite of Heptachlor)

Apples 531 0 0.005 ^ 0.01 AL

Applesauce 190 0 0.005 ^ 0.01 AL

Cherries 30 0 0.040 ^ 0.05 AL

Cherries, Frozen 144 0 0.040 ^ 0.05 AL

Cranberries 156 0 0.001 ^ 0.05 AL

Cranberries, Frozen 25 0 0.001 ^ 0.05 AL

Cucumbers 754 0 0.005 ^ 0.05 AL

Eggs 294 0 0.040 ^ 0.05 AL

Grapefruit 704 0 0.010 ^ 0.05 AL

Green Beans 567 0 0.010 ^ 0.05 AL

Lettuce 756 0 0.005 ^ 0.05 AL

Milk 708 0 0.010 ^ 0.1 AL

Olives, Canned 189 0 0.010 ^ 0.01 AL

Oranges 708 0 0.005 ^ 0.05 AL

Potatoes 708 0 0.002 ^ 0.01 AL

Spinach 707 0 0.002 - 0.040 0.05 AL

Strawberries 530 0 0.010 ^ 0.05 AL

Sweet Potatoes 532 0 0.040 ^ 0.01 AL

Tomatoes 528 0 0.002 ^ 0.01 AL

Tomatoes, Canned 189 0 0.002 ^ 0.01 AL

TOTAL 8,950 0

Heptachlor epoxide cis (metabolite of Heptachlor)

Grapes 708 0 0.004 ^ 0.05 AL

Pears 707 0 0.004 ^ 0.05 AL

TOTAL 1,415 0

Hexachlorobenzene - HCB (metabolite and impurity of Quintozene)

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Eggs 294 0 0.040 ^ NT

Grapefruit 704 0 0.003 - 0.050 NT

Green Beans 379 0 0.050 ^ 0.1

Milk 708 0 0.0026 ^ NT

Olives, Canned 189 0 0.003 ^ NT

Oranges 708 0 0.005 ^ NT
Appendix E. Page 7 of 7

 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Spinach 358 0 0.001 ^ NT

Strawberries 530 0 0.003 ^ NT

TOTAL 4,805 0

Lindane - BHC gamma (insecticide) (also an isomer of BHC)

Apples 531 0 0.013 ^ NT

Applesauce 190 0 0.013 ^ NT

Cherries 30 0 0.045 ^ 0.5

Cherries, Frozen 144 0 0.045 ^ 0.5

Cranberries 156 0 0.005 ^ NT

Cranberries, Frozen 25 0 0.005 ^ NT

Cucumbers 754 0 0.005 ^ NT

Eggs 294 0 0.040 ^ 0.5

Grapefruit 704 0 0.005 ^ 0.5

Green Beans 567 0 0.008 ^ 0.5

Lettuce 756 0 0.013 ^ NT

Milk 708 0 0.005 ^ 0.3

Olives, Canned 189 0 0.005 ^ NT

Oranges 708 0 0.005 ^ 0.5

Potatoes 708 0 0.001 ^ 0.5

Spinach 707 0 0.001 - 0.045 NT

Strawberries 530 0 0.005 ^ 0.5

Sweet Potatoes 532 0 0.045 ^ 0.5

Tomatoes 528 0 0.003 ^ NT

Tomatoes, Canned 189 0 0.003 ^ NT

TOTAL 8,950 0

Mirex (insecticide) 

Apples 531 0 0.001 ^ NT

Applesauce 190 0 0.001 ^ NT

Lettuce 756 0 0.001 ^ NT

TOTAL 1,477 0

Oxychlordane (metabolite of Chlordane)

Grapefruit 358 0 0.020 ^ 0.1 AL

Milk 708 0 0.020 ^ NT

Olives, Canned 189 0 0.020 ^ 0.1 AL

Strawberries 530 0 0.020 ^ 0.1 AL

TOTAL 1,785 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.
Appendix F

Sample Origin by State or Country

(Determined by Grower, Packer, or Distributor)

Appendix F gives the number of samples per State or country of origin and the number of 

samples of unknown origin. Where available, the origin of fresh commodities is taken from 

the grower or packer information. For processed commodities, origin is determined primarily 

by packer or distributor.

As shown in Appendix F, samples originated from 42 States and 20 foreign countries. There 

were 339 domestic samples from unknown States and one imported sample from an unknown 

country. There were an additional 50 samples from unknown origins. Overall, 81.2 percent 

of samples were from U.S. sources, 18.3 percent were imports, and 0.5 percent were of 

unknown origin.
Appendix F. Page 1 of 2

Part 1. Domestic Samples

Egg Milk # of % of

AP CA CH CU GB GF GR LT OG PE PO SP ST SW TO AC AZ CZ OL TC EG MK Samples Total

Alabama 6 6 0.1

Arizona 11 1 3 3 2 5 2 2 3 3 2 5 42 0.4

Arkansas 1 12 7 4 4 7 7 9 8 59 0.6

California 15 15 20 92 292 324 650 538 87 83 495 409 175 61 20 4 26 75 39 56 168 3644 35.2

Colorado 1 5 3 1 28 9 2 1 3 21 74 0.7

Connecticut 2 3 2 2 2 1 1 1 3 17 0.2

Delaware 1 1 2 < 0.1

Florida 1 40 103 145 1 4 29 1 20 6 43 1 76 2 1 4 7 42 526 5.1

Georgia 44 25 1 2 2 5 8 87 0.8

Idaho 1 1 214 7 2 1 2 228 2.2

Illinois 7 3 5 1 1 5 6 14 7 1 15 10 11 10 13 109 1.1

Indiana 1 1 2 11 8 23 0.2

Kansas 1 2 3 < 0.1

Kentucky 1 1 2 < 0.1

Louisiana 30 1 31 0.3

Maine 6 1 1 1 2 11 0.1

Maryland 3 7 8 1 1 3 2 3 12 2 2 2 1 2 3 2 4 12 70 0.7

Massachusetts 69 3 3 7 7 89 0.9

Michigan 20 5 25 8 2 3 2 12 7 1 7 11 10 6 9 18 48 194 1.9

Minnesota 1 2 5 4 1 6 4 5 6 3 6 15 58 0.6

Mississippi 1 60 10 71 0.7

Missouri 3 1 3 1 6 14 0.1

Nebraska 27 27 0.3

Nevada 2 2 < 0.1

New Hampshire 5 5 < 0.1

New Jersey 2 7 12 2 1 5 4 1 1 1 9 6 30 81 0.8

New Mexico 4 1 5 < 0.1

New York 29 12 5 2 22 8 2 7 6 5 2 8 9 13 63 193 1.9

North Carolina 10 7 2 20 2 136 5 10 2 4 10 7 21 236 2.3

North Dakota 5 5 < 0.1

Ohio 2 7 12 2 5 10 4 1 2 8 13 6 17 29 81 199 1.9

Oregon 3 1 1 140 17 1 1 4 3 6 177 1.7

Pennsylvania 5 2 4 1 6 12 2 19 1 2 39 22 115 1.1

Rhode Island 1 1 < 0.1

South Carolina 7 2 9 0.1

Tennessee 1 1 3 2 7 0.1

Texas 10 23 22 202 10 20 27 14 63 41 8 7 48 1 5 6 6 26 91 630 6.1

Utah 3 3 < 0.1

Vermont 1 1 2 < 0.1

Virginia 2 2 6 2 2 1 4 19 0.2

Washington 394 4 4 4 5 1 8 339 135 5 3 2 13 5 6 24 952 9.2

Wisconsin 21 1 1 3 18 2 4 50 0.5

Unknown State 7 3 38 57 20 9 23 18 10 8 25 11 77 14 2 2 1 5 9 339 3.3

No. of Domestic 499 122 0 263 379 674 355 730 630 604 675 682 474 530 210 173 20 68 145 182 294 708 8,417

% of Total 94 78 0 35 67 96 50 97 89 85 95 96 89 100 40 91 80 47 77 96 100 100 81.2

Processed F&V

APPENDIX F. SAMPLE ORIGIN BY STATE OR COUNTRY

(Determined by Grower, Packer, or Distributor)

Fresh F&V
Appendix F. Page 2 of 2

Part 2. Imported Samples

Egg Milk # of % of

AP CA CH CU GB GF GR LT OG PE PO SP ST SW TO AC AZ CZ OL TC EG MK Samples Total

Argentina 1 72 73 0.7

Australia 5 5 < 0.1

Brazil 1 1 < 0.1

Canada 1 34 53 6 9 29 9 41 15 5 202 1.9

Chile 17 29 231 38 27 33 375 3.6

China 1 1 1 3 < 0.1

Dominican Repub. 8 8 0.1

Egypt 1 1 < 0.1

France 1 1 < 0.1

Greece 26 26 0.3

Guatemala 23 23 0.2

Honduras 23 1 24 0.2

Italy 7 7 0.1

Mexico 393 145 4 61 9 9 14 56 276 967 9.3

Morocco 1 1 < 0.1

New Zealand 12 3 15 0.1

Peru 3 56 59 0.6

South Africa 20 23 43 0.4

Spain 4 40 44 0.4

Turkey 17 2 19 0.2

Unknown Country 1 1 < 0.1

No. of Imports 32 34 30 481 175 27 350 18 75 103 29 23 56 0 317 16 5 76 44 7 0 0 1,898

% of Total 6 22 100 64 31 4 49 2 11 15 4 3 11 0 60 8 20 53 23 4 0 0 18.3

Part 3. Unknown Origin Samples

Egg Milk # of % of

AP CA CH CU GB GF GR LT OG PE PO SP ST SW TO AC AZ CZ OL TC EG MK Samples Total

Unknown Origin 10 13 3 3 8 3 4 2 2 1 1 50 0.5

% of Total 1 2 < 1 < 1 1 < 1 1 < 1 < 1 < 1 1 0.5

Sample Totals: 531 156 30 754 567 704 708 756 708 707 708 707 530 532 528 190 25 144 189 189 294 708 10,365

Commodity Legend

 AC = Applesauce GB = Green Beans PE = Pears

 AP = Apples GF = Grapefruit PO = Potatoes

 AZ = Cranberries, Frozen GR = Grapes SP = Spinach

 CA = Cranberries, Fresh LT = Lettuce ST = Strawberries

 CH = Cherries, Fresh MK = Milk SW = Sweet Potatoes

 CU = Cucumbers OG = Oranges TC = Tomatoes, Canned

 CZ = Cherries, Frozen OL = Olives, Canned TO = Tomatoes, Fresh

 EG = Eggs

Fresh F&V Processed F&V

Fresh F&V Processed F&V
Appendix G

Import Versus Domestic Pesticide Residue Comparisons

The Pesticide Data Program is designed to provide a comprehensive statistical picture of 

pesticide residues in the U.S. food supply, representing all sources, including imports. Most 

commodities consumed are generally produced in the United States with import components 

that vary by commodity. However, several commodities tested over the past several years 

were cyclical; that is, part of the year the commodity was produced domestically and part of the 

year it was imported. 

Appendix G compares residue data reported for samples originating in the United States 

with those of the same commodity from major exporting countries in 2016. Residue data 

for domestic grapes are compared with data for samples originating in Chile. Residue data 

for domestic green beans and tomatoes are compared with data for samples originating in 

Mexico. Only residues detected in more than 10 percent of all samples are included in each 

comparison. All pesticides detected were registered in the United States. However, the profiles 

of residue findings were markedly different in the United States samples versus samples from 

these exporting countries. The differences in residue detections between countries were likely 

due to the pesticides used in response to pest pressures based on differing environmental and 

climatic conditions as well as crop production and protection practices. 
Appendix G. Page 1 of 3

Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Boscalid United States 355 211 59.4

Chile 231 169 73.2

Buprofezin United States 354 68 19.2

Chile 231 0 0

Cyprodinil United States 355 150 42.3

Chile 231 134 58.0

Difenoconazole United States 355 16 4.5

Chile 231 72 31.2

Fenhexamid United States 355 65 18.3

Chile 230 154 67.0

Fludioxonil United States 355 54 15.2

Chile 231 77 33.3

Iprodione United States 355 4 1.1

Chile 231 52 22.5

Methoxyfenozide United States 355 64 18.0

Chile 231 16 6.9

Myclobutanil United States 355 87 24.5

Chile 231 52 22.5

Pyraclostrobin United States 355 181 51.0

Chile 231 62 26.8

Pyrimethanil United States 355 26 7.3

Chile 231 59 25.5

Quinoxyfen United States 355 111 31.3

Chile 231 71 30.7

Spirotetramat United States 355 115 32.4

Chile 231 30 13.0

Tebuconazole United States 355 92 25.9

Chile 231 147 63.6

Trifloxystrobin United States 355 76 21.4

Chile 231 59 25.5

NOTE: The Limits of Detection (LODs) for pesticide detections in grapes are listed in Appendix B.

Appendix G. Import Versus Domestic Pesticide Residue Comparisons

2016 Distribution of Residues for Grape Samples

Originating in Chile Versus United States

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)
Appendix G. Page 2 of 3

Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Azoxystrobin United States 379 128 33.8

Mexico 145 5 3.4

Boscalid United States 379 31 8.2

Mexico 145 18 12.4

Chlorantraniliprole United States 379 55 14.5

Mexico 145 6 4.1

Pyraclostrobin United States 379 69 18.2

Mexico 145 21 14.5

NOTE: The Limits of Detection (LODs) for pesticide detections in green beans are listed in Appendix B.

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

2016 Distribution of Residues for Green Bean Samples

Originating in Mexico Versus United States
Appendix G. Page 3 of 3

Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Azoxystrobin United States 210 28 13.3

Mexico 276 94 34.1

Bifenthrin United States 210 64 30.5

Mexico 276 18 6.5

Boscalid United States 210 20 9.5

Mexico 276 120 43.5

Chlorantraniliprole United States 210 70 33.3

Mexico 276 29 10.5

Clothianidin United States 210 24 11.4

Mexico 276 51 18.5

Difenoconazole United States 210 48 22.9

Mexico 276 59 21.4

Dinotefuran United States 210 36 17.1

Mexico 276 25 9.1

Flonicamid United States 210 6 2.9

Mexico 276 108 39.1

Imidacloprid United States 210 77 36.7

Mexico 276 44 15.9

Pyraclostrobin United States 210 41 19.5

Mexico 276 82 29.7

Pyrimethanil United States 210 20 9.5

Mexico 276 45 16.3

Sulfoxaflor United States 210 6 2.9

Mexico 276 66 23.9

NOTE: The Limits of Detection (LODs) for pesticide detections in tomatoes are listed in Appendix B.

2016 Distribution of Residues for Tomato Samples

Originating in Mexico Versus United States

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)
Appendix H

Pesticide Residues by Commodity

(Pairs With Residue Detections in at Least 5 Percent of Samples)

Appendix H shows 265 commodity/pesticide pairs (including metabolites, isomers, and 

degradates) with detections in at least 5 percent of the samples tested. The data shown 

include the range and mean of values detected and U.S. Environmental Protection Agency 

(EPA) tolerance references for each pair. The EPA tolerances cited in this summary and 

Appendixes apply to 2016 and not to the current year. There may be instances where 

tolerances have been recently set, modified, or revoked that would have an effect on 

whether a residue is violative or not. 
Appendix H. Page 1 of 7

APPENDIX H. PESTICIDE RESIDUES A BY COMMODITY

(Pairs With Residue Detections in at Least 5 Percent of Samples)

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

1 Apples (16 pesticides)

Acetamiprid * I 32.6 531 173 0.002 - 0.18 0.026 1.0

Boscalid F 22.8 531 121 0.003 - 0.21 0.057 3.0

Carbendazim (MBC) 1 F 14.1 531 75 0.001 - 0.11 0.028 2.0

Chlorantraniliprole I 25.2 531 134 0.010 - 0.076 0.023 1.2

Cyhalothrin, Total 2 * I 5.1 531 27 0.005 - 0.037 0.013 0.30

Diphenylamine (DPA) F 80.2 531 426 0.002 - 3.8 0.283 10.0

Flubendiamide I 5.1 531 27 0.005 - 0.13 0.034 1.5

Fludioxonil F 35 531 186 0.028 - 2.8 0.417 5.0

Hexythiazox I 6.8 531 36 0.003 - 0.036 0.013 0.4

Imidacloprid I 7.5 531 40 0.003 - 0.021 0.007 0.5

Pyraclostrobin F 20.5 531 109 0.003 - 0.12 0.033 1.5

Pyrimethanil F 33.9 531 180 0.053 - 6.2 1.668 15

Spirodiclofen A 14.3 531 76 0.010 - 0.085 0.027 0.80

Tetrahydrophthalimide (THPI) 3 FM 12.2 531 65 0.011 - 0.61 0.133 25.0

Thiabendazole F 62.9 531 334 0.002 - 3.3 0.391 5.0 

Trifloxystrobin F 9.2 531 49 0.002 - 0.016 0.005 0.5

2 Applesauce (11 pesticides)

Acetamiprid * I 78.9 190 150 0.002 - 0.079 0.011 1.0

Boscalid F 8.9 190 17 0.004 - 0.026 0.009 3.0

Carbendazim (MBC) 1 F 70 190 133 0.001 - 0.076 0.015 2.0

Cyprodinil F 10.5 190 20 0.005 - 0.012 0.008 1.7

Diphenylamine (DPA) F 35.8 190 68 0.002 - 0.050 0.013 10.0

Flubendiamide I 26.3 190 50 0.004 - 0.017 0.007 1.5

Fludioxonil F 10 190 19 0.025 - 0.12 0.045 5.0

Imidacloprid I 9.5 190 18 0.004 - 0.013 0.006 0.5

Pyrimethanil F 18.4 190 35 0.061 - 1.3 0.401 15

Tetrahydrophthalimide (THPI) 3 FM 74.7 190 142 0.012 - 0.51 0.065 25.0

Thiabendazole F 28.4 190 54 0.002 - 0.89 0.141 5.0 

3 Cherries, Fresh (12 pesticides)

Acetamiprid * I 60 30 18 0.003 - 0.13 0.045 1.20

Buprofezin I 13.3 30 4 0.002 - 0.042 0.019 1.9

Cyhalothrin, Total 2 * I 13.3 30 4 0.014 - 0.020 0.016 0.50

Fenbuconazole F 16.7 30 5 0.005 - 0.13 0.034 1.0

Fenhexamid F 30 30 9 0.011 - 0.10 0.053 10.0

Fludioxonil F 60 30 18 0.050 - 1.2 0.417 5.0

Iprodione F 93.3 30 28 0.032 - 2.6 0.968 20.0 

Pyraclostrobin F 6.7 30 2 0.004 - 0.005 0.005 2.5

Pyrimethanil F 10 30 3 0.008 - 0.62 0.213 10

Spinosad A 4 IM 6.7 30 2 0.005 - 0.029 0.017 0.20

Tebuconazole F 93.3 30 28 0.060 - 1.9 0.71 5.0 

Thiacloprid I 6.7 30 2 0.013 - 0.016 0.014 0.5
Appendix H. Page 2 of 7

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

4 Cherries, Frozen (24 pesticides)

Acetamiprid * I 63.9 144 92 0.002 - 0.10 0.021 1.20

Boscalid F 36.8 144 53 0.013 - 0.35 0.071 3.5

Buprofezin I 14.6 144 21 0.001 - 0.022 0.008 1.9

Carbaryl I 11.8 144 17 0.004 - 0.69 0.172 10

Carbendazim (MBC) 1 F 20.8 144 30 0.005 - 0.58 0.052 20.0

Cyhalothrin, Total 2 * I 27.8 144 40 0.012 - 0.088 0.038 0.50

Cypermethrin I 6.9 144 10 0.073 - 0.16 0.112 1

Dimethoate (parent) I 7.6 144 11 0.005 - 0.052 0.021 2.0 

 Omethoate 5 IM 5.6 144 8 0.010 - 0.053 0.018 2.0 

Fenbuconazole F 32.6 144 47 0.005 - 0.78 0.164 1.0

Fenhexamid F 6.2 144 9 0.014 - 0.078 0.039 10.0

Fenpropathrin I 27.8 144 40 0.021 - 1.0 0.3 5.0

Fludioxonil F 5.6 144 8 0.037 - 0.71 0.298 5.0

Imidacloprid I 21.5 144 31 0.019 - 0.23 0.066 3.0

Iprodione F 20.8 144 30 0.034 - 1.7 0.383 20.0 

Myclobutanil F 12.5 144 18 0.001 - 0.061 0.01 5.0

Permethrin

 Permethrin cis 6 IM 5.6 144 8 0.020 - 0.059 0.04 4.0

 Permethrin trans 6 IM 6.9 144 10 0.013 - 0.086 0.051 4.0

Propiconazole F 7.6 144 11 0.019 - 0.083 0.039 4.0

Pyraclostrobin F 43.1 144 62 0.002 - 0.18 0.043 2.5

Spinosad

 Spinosad A 4 IM 22.9 144 33 0.003 - 0.037 0.014 0.20

 Spinosad D 4 IM 7.6 144 11 0.004 - 0.007 0.005 0.20

Tebuconazole F 34.7 144 50 0.013 - 1.3 0.184 5.0 

Thiacloprid I 28.5 144 41 0.006 - 0.095 0.025 0.5

Thiamethoxam * I 27.1 144 39 0.006 - 0.34 0.053 0.5

Trifloxystrobin F 30.6 144 44 0.006 - 0.083 0.029 2

Triflumizole F 17.4 144 25 0.003 - 0.24 0.033 1.5

5 Cranberries (4 pesticides)

Azoxystrobin F 22.4 156 35 0.001 - 0.008 0.003 5.0

Chlorantraniliprole I 7.1 156 11 0.005 - 0.014 0.008 2.5

Diazinon I 5.1 156 8 0.006 - 0.028 0.013 0.50

Fenbuconazole F 24.4 156 38 0.001 - 0.009 0.004 0.5

6 Cranberries, Frozen (1 pesticide)

Methoxyfenozide I 24 25 6 0.002 - 0.008 0.004 3.0

7 Cucumbers (12 pesticides)

Azoxystrobin F 14.6 754 110 0.002 - 0.039 0.007 0.3

Bifenthrin * I 9.8 754 74 0.005 - 0.085 0.015 0.4

Boscalid F 6.1 754 46 0.011 - 0.098 0.021 0.5

Carbendazim (MBC) 1 F 7.6 754 57 0.010 - 0.082 0.021 1.0

Chlorothalonil F 13.9 754 105 0.005 - 0.30 0.021 5.0

Cyprodinil F 6 754 45 0.005 - 0.055 0.017 0.70

Dinotefuran * I 7.2 754 54 0.010 - 0.27 0.033 0.5

Flonicamid I 8 754 60 0.012 - 0.30 0.065 1.5
Appendix H. Page 3 of 7

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Fluopicolide F 8 754 60 0.010 - 0.11 0.021 0.50

Metalaxyl/Mefenoxam 7 F 29.8 754 225 0.005 - 0.32 0.04 1.0

Propamocarb F 43.9 189 83 0.010 - 0.58 0.121 1.5

 Propamocarb hydrochloride 8 F 49 565 277 0.011 - 0.78 0.13 1.5

Thiamethoxam * I 9.8 754 74 0.010 - 0.25 0.031 0.2

8 Grapefruit (3 pesticides)

Imazalil F 79.8 704 562 0.001 - 0.11 0.021 10.0 

Imidacloprid I 13.5 704 95 0.003 - 0.039 0.007 0.70

Thiabendazole F 69.6 704 490 0.002 - 0.15 0.032 10.0 

9 Grapes (22 pesticides)

Acetamiprid * I 8.9 708 63 0.017 - 2.1 0.161 0.35

Boscalid F 59.5 708 421 0.008 - 1.2 0.112 5.0

Buprofezin I 10.5 707 74 0.005 - 0.30 0.022 2.5

Chlorantraniliprole I 9.2 708 65 0.025 - 0.069 0.027 2.5

Cyprodinil F 41.7 708 295 0.010 - 1.3 0.19 3.0

Difenoconazole F 14.1 708 100 0.002 - 0.13 0.012 4.0

Etoxazole A 6.4 708 45 0.002 - 0.074 0.007 0.50

Fenhexamid F 35.4 706 250 0.008 - 0.69 0.134 4.0

Fenpropathrin I 9.9 708 70 0.005 - 0.34 0.079 5.0

Fludioxonil F 19.6 708 139 0.033 - 0.44 0.071 2.0

Imidacloprid I 8.6 707 61 0.042 - 2.2 0.263 1.0

Iprodione F 10.9 708 77 0.017 - 1.2 0.167 60.0

Methoxyfenozide I 11.4 708 81 0.008 - 0.15 0.038 1.0

Myclobutanil F 23.3 708 165 0.017 - 1.8 0.053 1.0

Pyraclostrobin F 38 708 269 0.005 - 0.23 0.04 2.0

Pyrimethanil F 12.6 708 89 0.008 - 1.6 0.387 5.0

Quinoxyfen F 28 708 198 0.003 - 0.14 0.013 2.0

Spirotetramat I 22.7 708 161 0.003 - 0.068 0.01 1.3

Tebuconazole F 43.1 708 305 0.003 - 0.73 0.043 5.0

Tetraconazole F 8.2 708 58 0.003 - 0.10 0.019 0.20

Trifloxystrobin F 24.7 708 175 0.005 - 0.18 0.017 2.0

Triflumizole F 5.1 708 36 0.002 - 0.015 0.004 2.5

10 Green Beans, Fresh (12 pesticides)

Acephate (parent) * I 9 567 51 0.031 - 1.7 0.291 3.0

 Methamidophos 9 * I 9.5 567 54 0.020 - 0.58 0.139 1 

Azoxystrobin F 26.5 567 150 0.001 - 0.47 0.028 3.0

Bifenthrin * I 7.9 567 45 0.040 - 0.19 0.072 0.6

Boscalid F 11.1 567 63 0.005 - 0.54 0.055 1.6

Chlorantraniliprole I 11.5 567 65 0.001 - 0.051 0.009 2.0

Cyhalothrin, Total 2 * I 6.4 535 34 0.008 - 0.15 0.033 0.20

Dicloran F 6.7 567 38 0.011 - 15 1.849 20

Dimethoate I 9.5 567 54 0.001 - 0.97 0.114 2.0

Methomyl I 9 567 51 0.001 - 0.62 0.057 2

Penthiopyrad F 6.7 567 38 0.001 - 0.25 0.024 4.0

Pyraclostrobin F 17.5 567 99 0.001 - 0.54 0.027 0.5

Tebuconazole F 7.1 567 40 0.001 - 0.080 0.02 0.1
Appendix H. Page 4 of 7

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

11 Lettuce (14 pesticides)

Acephate I 5.2 756 39 0.003 - 0.14 0.014 10

Boscalid F 6.9 756 52 0.003 - 0.063 0.009 11.0

Cyhalothrin, Total 2 * I 10.2 756 77 0.005 - 0.59 0.071 2.0

DCPA H 7.7 756 58 0.002 - 0.050 0.005 2.0 

Dimethomorph F 16.3 756 123 0.003 - 2.9 0.178 30.0

Fenamidone F 13.1 756 99 0.005 - 2.5 0.181 60

Flonicamid I 6.9 756 52 0.006 - 1.5 0.117 4.0

Imidacloprid I 37.7 756 285 0.003 - 0.16 0.013 3.5

Mandipropamid F 14.7 756 111 0.002 - 2.3 0.203 20

Metalaxyl/Mefenoxam 7 F 6.1 756 46 0.001 - 0.017 0.005 5.0

Permethrin

 Permethrin cis 6 IM 8.1 756 61 0.010 - 0.74 0.167 20

 Permethrin trans 6 IM 8.2 756 62 0.010 - 0.92 0.181 20

Propamocarb hydrochloride 8 F 18.9 756 143 0.002 - 30 0.741 90

Spinetoram I 8.1 756 61 0.003 - 0.20 0.024 8.0

Thiamethoxam * I 18.1 756 137 0.003 - 0.22 0.011 4.0

12 Olives, Canned (2 pesticides)

Buprofezin I 14.3 189 27 0.001 - 0.073 0.021 3.5

Fenpropathrin I 8.5 189 16 0.005 - 0.051 0.011 5.0

13 Oranges (3 pesticides)

Imazalil F 83.5 708 591 0.010 - 0.47 0.059 10.0 

Pyrimethanil F 5.8 708 41 0.003 - 0.065 0.019 10

Thiabendazole F 74 708 524 0.010 - 0.42 0.053 10.0 

14 Pears (20 pesticides)

Acetamiprid * I 14.4 706 102 0.017 - 0.35 0.06 1.0

Boscalid F 22.5 707 159 0.008 - 0.24 0.073 3.0

Carbendazim (MBC) 1 F 25.7 707 182 0.017 - 0.15 0.043 3.0

Chlorantraniliprole I 12.9 706 91 0.025 - 0.083 0.03 1.2

Diphenylamine (DPA) F 10.7 707 76 0.007 - 1.4 0.041 5.0

Ethoxyquin P 26.3 707 186 0.010 - 1.5 0.212 3

Etoxazole A 20.9 707 148 0.002 - 0.050 0.008 0.20

Fenbutatin oxide I 10.7 707 76 0.017 - 0.39 0.121 15.0

Fenpyroximate A 19.4 707 137 0.002 - 0.19 0.026 0.30

Fludioxonil F 41.9 707 296 0.033 - 3.9 0.597 5.0

Imidacloprid I 10.1 706 71 0.042 - 0.36 0.095 0.6

Novaluron I 5.8 707 41 0.012 - 0.13 0.029 3.0

o-Phenylphenol F 20.1 707 142 0.003 - 20 0.94 25.0 

Pyraclostrobin F 21.5 707 152 0.005 - 0.18 0.038 1.5

Pyridaben I 6.1 707 43 0.003 - 0.10 0.015 0.75

Pyrimethanil F 52.5 707 371 0.008 - 7.1 1.101 15

Spinetoram I 5 707 35 0.033 - 0.080 0.035 0.20

Spirodiclofen A 11.5 707 81 0.008 - 0.13 0.03 0.80

Spirotetramat I 20.2 707 143 0.003 - 0.031 0.007 0.70

Thiabendazole F 32.8 696 228 0.005 - 3.5 0.421 5.0 
Appendix H. Page 5 of 7

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

15 Potatoes (9 pesticides)

Azoxystrobin F 27.8 708 197 0.002 - 1.2 0.082 8.0

Boscalid F 19.5 708 138 0.003 - 0.034 0.004 0.05

Chlorpropham H 99.6 708 705 0.002 - 10 1.89 30

Clothianidin * I 13.3 708 94 0.003 - 0.032 0.005 0.3

Difenoconazole F 11.4 708 81 0.002 - 1.8 0.414 4.0

Fludioxonil F 9.3 708 66 0.020 - 0.93 0.295 6.0

Imidacloprid I 42.5 708 301 0.002 - 0.11 0.01 0.40

Metalaxyl/Mefenoxam 7 F 7.6 708 54 0.002 - 0.017 0.004 0.5

Thiabendazole F 6.6 708 47 0.002 - 3.1 0.269 10.0 

16 Spinach (23 pesticides)

Acetamiprid * I 9.1 707 64 0.002 - 1.3 0.146 3.00

Ametoctradin F 59.8 358 214 0.002 - 13 1.668 50.0

Azoxystrobin F 5.2 707 37 0.002 - 4.4 0.446 30.0

Bifenthrin * I 7.2 707 51 0.002 - 1.3 0.071 0.2

Boscalid F 19.2 707 136 0.003 - 0.14 0.012 60

Chlorantraniliprole I 32.8 707 232 0.003 - 9.3 0.397 13

Clothianidin * I 37.9 707 268 0.003 - 0.64 0.075 3.0

Cyazofamid F 9.2 707 65 0.020 - 2.0 0.494 10

Cypermethrin I 20.2 707 143 0.037 - 4.0 0.406 10.00

DCPA H 5.1 707 36 0.002 - 0.008 0.003 NT

Dimethomorph F 34.2 707 242 0.002 - 4.4 0.278 30.0

Famoxadone F 7.5 707 53 0.004 - 4.8 0.88 50

Fenamidone F 27.9 707 197 0.004 - 6.6 0.529 60

Flonicamid I 29.6 707 209 0.002 - 4.1 0.554 9.0

Fluopicolide F 39 707 276 0.003 - 6.6 0.654 25

Imidacloprid I 41.2 707 291 0.002 - 0.57 0.034 3.5

Mandipropamid F 68 707 481 0.008 - 7.1 0.928 20

Methoxyfenozide I 5.7 707 40 0.002 - 5.0 0.46 30

Permethrin

 Permethrin cis 6 IM 69.7 707 493 0.002 - 4.3 0.797 20

 Permethrin trans 6 IM 71 707 502 0.002 - 5.9 0.848 20

Pyraclostrobin F 10 707 71 0.002 - 1.7 0.22 29.0

Spinetoram I 48.2 707 341 0.002 - 0.52 0.037 8.0

Spinosad (parent) I 18.2 358 65 0.002 - 0.82 0.057 8.0

 Spinosad A 4 IM 11.2 349 39 0.006 - 1.6 0.137 8.0

 Spinosad D 4 IM 7.4 349 26 0.005 - 0.44 0.046 8.0

Thiamethoxam * I 7.9 707 56 0.005 - 0.55 0.04 4.0

17 Strawberries (36 pesticides)

Acetamiprid * I 29.8 530 158 0.001 - 0.89 0.045 0.60

Azoxystrobin F 16.6 530 88 0.001 - 0.64 0.061 10.0

Bifenazate A 20.6 530 109 0.003 - 0.93 0.115 1.5

Bifenthrin * I 25.5 530 135 0.003 - 0.29 0.043 3.0

Boscalid F 54.3 530 288 0.003 - 1.2 0.072 4.5

Carbendazim (MBC) 1 F 12.8 530 68 0.002 - 0.26 0.039 7.0

Chlorantraniliprole I 10 530 53 0.005 - 0.16 0.032 1.0

Cyflufenamid F 8.9 530 47 0.001 - 0.044 0.007 0.20
Appendix H. Page 6 of 7

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Cyflumetofen A 23 530 122 0.003 - 0.55 0.053 0.60

Cyprodinil F 50.2 530 266 0.005 - 1.7 0.159 5.0

Fenhexamid F 22.6 530 120 0.010 - 0.97 0.163 3.0

Fenpropathrin I 6.6 530 35 0.005 - 0.62 0.098 2.0

Fenpyroximate A 6.2 530 33 0.002 - 0.15 0.015 1.0

Flonicamid I 29.4 530 156 0.010 - 0.61 0.093 1.5

Fludioxonil F 36.2 530 192 0.010 - 0.62 0.076 3.0

Fluopyram F 9.1 530 48 0.002 - 0.41 0.097 2.0

Flupyradifurone I 15.8 530 84 0.001 - 0.23 0.04 1.5

Fluxapyroxad F 32.1 530 170 0.001 - 0.58 0.046 4.0

Hexythiazox I 13 530 69 0.001 - 0.35 0.028 6

Imidacloprid I 14.2 530 75 0.003 - 0.063 0.011 0.50

Malathion I 6.2 530 33 0.003 - 0.068 0.018 8

Metalaxyl/Mefenoxam 7 F 15.8 530 84 0.001 - 0.15 0.014 10.0

Myclobutanil F 26.2 530 139 0.003 - 0.55 0.053 0.50

Novaluron I 27.7 530 147 0.020 - 0.28 0.053 0.45

Penthiopyrad F 27.7 530 147 0.001 - 0.74 0.116 3.0

Propiconazole F 6.8 530 36 0.005 - 0.16 0.038 1.3

Pyraclostrobin F 48.9 530 259 0.001 - 0.83 0.061 1.2

Pyrimethanil F 24 530 127 0.005 - 2.3 0.286 3.0

Quinoxyfen F 21.1 530 112 0.001 - 0.19 0.028 1.0

Spinetoram I 8.7 530 46 0.010 - 0.12 0.027 0.90

Spiromesifen (parent) I 6.4 530 34 0.003 - 0.27 0.086 2.0

 Spiromesifen alcohol 10 IM 13 530 69 0.001 - 0.16 0.032 2.0

Tetraconazole F 7.7 530 41 0.005 - 0.12 0.03 0.25

Tetrahydrophthalimide (THPI) 3 FM 51.3 530 272 0.022 - 3.1 0.507 20.0

Thiamethoxam * I 16.4 530 87 0.001 - 0.12 0.015 0.30

Trifloxystrobin F 11.9 530 63 0.002 - 0.14 0.036 1.5

Triflumizole F 7.5 530 40 0.003 - 0.18 0.028 2.0

18 Sweet Potatoes (4 pesticides)

Dicloran F 27.8 532 148 0.026 - 3.5 0.521 10

Fludioxonil F 23.9 532 127 0.067 - 0.70 0.225 6.0

Piperonyl butoxide I 10 532 53 0.015 - 18 0.443 10

Thiabendazole F 20.3 532 108 0.005 - 3.0 0.549 10 

19 Tomatoes (22 pesticides)

Acetamiprid * I 8.9 528 47 0.002 - 0.076 0.007 0.20

Azoxystrobin F 23.5 528 124 0.002 - 0.045 0.008 0.2

Bifenthrin * I 15.9 528 84 0.002 - 0.069 0.011 0.15

Boscalid F 27.8 528 147 0.003 - 0.089 0.014 3.0

Buprofezin I 6.2 528 33 0.002 - 0.13 0.015 2.0

Chlorantraniliprole I 21.6 528 114 0.003 - 0.056 0.009 1.4

Chlorpropham H 8.1 528 43 0.002 - 0.015 0.003 NT

Clothianidin * I 14.6 528 77 0.003 - 0.064 0.005 0.20

Difenoconazole F 20.5 528 108 0.003 - 0.11 0.016 0.60

Dinotefuran * I 11.9 528 63 0.010 - 0.14 0.025 0.7

Famoxadone F 8.1 528 43 0.004 - 0.025 0.01 1.0

Flonicamid I 24.4 528 129 0.002 - 0.23 0.031 0.40
Appendix H. Page 7 of 7

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Fluxapyroxad F 7.8 528 41 0.002 - 0.044 0.007 0.7

Imidacloprid I 23.3 528 123 0.002 - 0.11 0.011 1.0

Methoxyfenozide I 9.8 528 52 0.002 - 0.028 0.006 2.0

Penthiopyrad F 7.4 528 39 0.003 - 0.24 0.023 3.0

Pyraclostrobin F 24.4 528 129 0.002 - 0.068 0.009 1.4

Pyrimethanil F 14 528 74 0.002 - 0.13 0.016 0.50

Pyriproxyfen I 8.3 528 44 0.004 - 0.024 0.008 0.80

Sulfoxaflor I 13.6 528 72 0.002 - 0.091 0.015 0.70

Tetrahydrophthalimide (THPI) 3 FM 7.9 470 37 0.006 - 0.089 0.023 0.05

Thiamethoxam * I 5.5 528 29 0.008 - 0.028 0.011 0.25

20 Tomatoes, Canned (5 pesticides)

Azoxystrobin F 15.9 189 30 0.002 - 0.012 0.003 0.2

Bifenthrin * I 16.9 189 32 0.002 - 0.015 0.003 0.15

Difenoconazole F 6.3 189 12 0.004 - 0.017 0.007 0.60

Fluxapyroxad F 13.2 189 25 0.002 - 0.009 0.004 0.7

Imidacloprid I 27.5 189 52 0.002 - 0.016 0.004 1.0

NOTES

A Excludes environmental contaminants, which are listed in Appendix E.

NT No tolerance established.

* Residue may result from food handling establishment (FHE) application.

1 From parent, benomyl.

2 Includes cyhalothrin lambda plus R157836 epimer.

3 Metabolite of captafol and captan.

4 Isomer of parent, spinosad.

5 Metabolite of parent, dimethoate.

6 Isomer of parent, permethrin.

7 Metalaxyl/mefenoxam are spatial isomers which are analytically indistinguishable via multiresidue methods, but have

separate registrations.

8 Analytically determined as the salt (hydrochloride).

9 Specific tolerance established for methamidophos in green beans as a possible result of an acephate application.

10 Metabolite of parent, spiromesifen.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

P = Plant Growth Regulator
Appendix I

Number of Pesticides Detected per Sample

Appendix I shows the percentage of samples versus the number of pesticides detected 

per sample. The graph and data on page 1 show the overall number of samples and 

percentages (of total number of samples analyzed) for each detection group across all 

commodities. The table on page 2 shows the number of pesticides detected by individual 

commodity. For the 10,365 samples analyzed, 22.7 percent of the samples had no 

detectable pesticides, 15.7 percent had 1 pesticide, and 61.6 percent of the samples had 

more than 1 pesticide. 

This appendix reports the number of distinct pesticides rather than residues. A parent 

compound and its metabolites are reported as a single pesticide.
Appendix I. Page 1 of 2

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 22

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 22

# of

Samples 2,352 1,627 1,940 1,139 790 646 529 411 280 218 170 111 74 39 17 15 3 2 1 1

% of Total

Samples 22.7 15.7 18.7 11.0 7.6 6.2 5.1 4.0 2.7 2.1 1.6 1.1 0.7 0.4 0.2 0.1 0.03 0.02 0.01 0.01

TOTAL NUMBER OF SAMPLES = 10,365

NOTES

1

 Environmental contaminants, listed in Appendix E, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues."

APPENDIX I. NUMBER OF PESTICIDES 1 DETECTED PER SAMPLE

Number of Pesticides Detected per Sample

Number of Pesticides Detected per Sample

15

10

5

20

25

Percent of Samples

15.7

6.2

7.6

11.0

2.1

2.7

4.0

5.1

Multiple pesticide detections may result from the application of more than one pesticide, spray 

drift, crop rotation, and/or cross-contamination.

1.1 1.6

0.4 0.2 0.1 0.01

0.7

0.03 0.02 0.01

22.7

18.7
Appendix I. Page 2 of 2

Commodity (# of samples) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 22

Fresh Fruit and Vegetables: Percent

Apples (531) 3.6 4.9 10.7 21.5 16.9 15.8 11.1 7.9 2.6 3.0 1.1 0.4 0.4 -- -- -- -- -- -- --

Cherries (30) 3.3 -- -- 40.0 20.0 13.3 13.3 6.7 3.3 -- -- -- -- -- -- -- -- -- -- --

Cranberries (156) 49.4 33.3 14.7 2.6 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Cucumbers (754) 17.1 21.0 21.8 19.0 13.4 4.6 2.3 0.8 0.1 -- -- -- -- -- -- -- -- -- -- --

Grapefruit (704) 6.7 27.7 49.6 13.1 2.1 0.9 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Grapes (708) 5.9 6.4 7.1 12.7 13.1 13.3 13.0 11.3 6.1 5.2 3.1 1.7 0.8 -- 0.1 0.1 -- -- -- --

Green Beans (567) 28.4 24.5 20.1 13.8 6.3 2.5 2.5 1.1 0.4 0.2 -- -- 0.4 -- -- -- -- -- -- --

Lettuce (756) 19.6 31.0 18.8 10.6 5.3 4.5 3.6 2.9 1.7 0.9 0.8 0.3 -- 0.1 -- -- -- -- -- --

Oranges (708) 8.1 21.6 62.9 7.1 0.4 -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Pears (707) 12.2 9.3 6.9 13.0 10.0 13.2 12.0 9.1 7.2 3.8 2.0 1.1 0.1 -- -- -- -- -- -- --

Potatoes (708) 0.3 19.4 36.0 22.7 12.3 6.8 2.4 0.1 -- -- -- -- -- -- -- -- -- -- -- --

Spinach (707) 5.2 5.7 5.5 7.4 10.3 10.9 11.6 9.1 8.8 6.6 6.4 5.1 3.0 2.1 0.7 1.3 0.1 0.1 0.1 --

Strawberries (530) 5.1 1.3 1.1 2.5 4.3 7.9 8.1 12.6 10.6 11.7 12.3 8.3 6.8 3.8 1.9 0.9 0.4 0.2 -- 0.2

Sweet Potatoes (532) 41.7 32.5 22.6 3.0 -- 0.2 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Tomatoes (528) 9.7 12.9 13.6 15.7 12.9 11.0 9.3 4.5 5.3 2.5 0.9 0.4 0.6 0.6 0.2 -- -- -- -- --

Processed Fruit and Vegetables:

Applesauce (190) 5.8 3.2 9.5 20.0 28.4 18.4 10.0 4.7 -- -- -- -- -- -- -- -- -- -- -- --

Cherries, Frozen (144) -- 8.3 9.0 8.3 13.2 11.1 11.8 16.0 6.3 5.6 4.9 3.5 2.1 -- -- -- -- -- -- --

Cranberries, Frozen (25) 68.0 32.0 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Olives, Canned (189) 74.1 22.2 3.2 0.5 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Tomatoes, Canned (189) 50.8 24.3 9.5 4.2 5.8 2.6 2.1 0.5 -- -- -- -- -- -- -- -- -- -- -- --

Percent of Total Samples 14.6 17.2 20.7 12.2 8.4 6.9 5.6 4.4 3.0 2.3 1.8 1.2 0.8 0.4 0.2 0.2 0.03 0.02 0.01 0.01

Actual Number of Samples 1,370 1,607 1,940 1,139 790 646 529 411 280 218 170 111 74 39 17 15 3 2 1 1

Egg Product: 

Eggs (294) 99.3 0.7 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 292 2 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Dairy Product: 

Milk (708) 97.5 2.5 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 690 18 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

NOTES

1 Environmental contaminants, listed in Appendix E, have been excluded from the count of pesticides detected in this appendix. Parent

compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues." 

APPENDIX I. NUMBER OF PESTICIDES DETECTED PER SAMPLE

Number of Pesticides 1 Detected per Sample

TOTAL NUMBER OF FRUIT & VEGETABLE SAMPLES = 9,363
Appendix J

Samples Reported to the

U.S. Food and Drug Administration as

Exceeding the Tolerance

or Without Established Tolerance

(per Code of Federal Regulations, Title 40, Part 180)

Appendix J shows pesticide residues reported to the U.S. Food and Drug Administration (FDA) 

as exceeding the tolerance or residues for which no established tolerance was listed under 

the Code of Federal Regulations, Title 40, Part 180. In 2016, a total of 318 samples with 358 

pesticides were reported to the FDA as Presumptive Tolerance Violations.

Pesticides exceeding the tolerance were detected in 48 samples including 1 sample of fresh 

cherries, 11 samples of cucumbers, 6 grape samples, 3 samples of green beans, 16 samples 

of spinach, 3 strawberry samples, 5 samples of sweet potatoes, and 3 tomato samples. Of 

those 48 samples, 20 were reported as imported produce.

In addition, 273 samples were found to have pesticides for which no tolerance was established, 

including 256 fresh fruit and vegetable samples and 17 processed fruit/vegetable samples.

o 244 samples contained 1 pesticide for which no tolerance was established.

o 21 samples contained 2 pesticides for which no tolerance was established.

o 8 samples contained 3 pesticides for which no tolerance was established.

Three of the 273 samples also contained 1 pesticide each that exceeded an established 

tolerance.

The columns under the Sample Origin heading provide the number of samples that were of 

domestic, imported, or unknown origin for each pesticide/commodity pair listed.

Appendix J also notes if metabolites (or isomers) were detected as part of the same sample. 

In instances where both parent and metabolite (or isomer) were detected, the Pesticide Data 

Program accounted for both as part of the same tolerance expression.

A number of the findings shown in this appendix are less than 0.01 ppm. Levels below 0.01 

ppm are deemed by the U.S. FDA to be “not of regulatory significance”.
Appendix J. Page 1 of 5

Residues Exceeding Established Tolerance

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm

Country of 

Origin

1 Cherries / Deltamethrin 1 0.12 0.15 0.05 Chile

2 Cucumbers / Chlorfenapyr 0.005 0.051 0.01 Mexico

3 Cucumbers / Chlorfenapyr 0.005 0.043 0.01 Mexico

4 Cucumbers / Chlorfenapyr 0.005 0.042 0.01 Honduras

5 Cucumbers / Chlorfenapyr 0.005 0.038 0.01 Unknown

6 Cucumbers / Chlorfenapyr 0.005 0.037 0.01 Mexico

7 Cucumbers / Chlorfenapyr 0.005 0.036 0.01 Honduras

8 Cucumbers / Chlorfenapyr 0.005 0.031 0.01 U.S.

9 Cucumbers / Chlorfenapyr 0.005 0.027 0.01 Honduras

10 Cucumbers / Chlorfenapyr 0.005 0.027 0.01 Unknown

11 Cucumbers / Chlorfenapyr 0.005 0.026 0.01 Honduras

12 Cucumbers / Chlorfenapyr 0.005 0.021 0.01 Mexico

13 Grapes / Acetamiprid 0.01 2.1 0.35 Chile

14 Grapes / Acetamiprid 0.01 1.4 0.35 Chile

15 Grapes / Acetamiprid 0.01 0.43 0.35 Chile

16 Grapes / Acetamiprid 0.01 0.36 0.35 Chile

17 Grapes / Imidacloprid 0.025 2.2 1.0 Chile

18 Grapes / Myclobutanil 0.01 1.8 1.0 Peru

19 Green Beans / Chlorfenapyr 0.025 0.06 0.01 Mexico

20 Green Beans / Clothianidin 0.005 0.034 0.02 Guatemala

21 Green Beans / Dinotefuran 0.04 0.054 0.01 U.S.

22 Spinach / Bifenthrin 0.001 1.3 0.2 U.S.

23 Spinach / Bifenthrin 0.001 1.3 0.2 U.S.

24 Spinach / Bifenthrin 0.01 0.41 0.2 U.S.

25 Spinach / Cyhalothrin, Total 2 0.015 0.48 0.01 U.S.

26 Spinach / Cyhalothrin, Total 2 0.003 0.098 0.01 U.S.

27 Spinach / Cyhalothrin, Total 2 0.015 0.082 0.01 U.S.

28 Spinach / Cyhalothrin, Total 2 0.015 0.068 0.01 U.S.

29 Spinach / Cyhalothrin, Total 2 0.003 0.052 0.01 U.S.

30 Spinach / Cyhalothrin, Total 2 0.015 0.039 0.01 U.S.

31 Spinach / Cyhalothrin, Total 2 0.015 0.033 0.01 U.S.

32 Spinach / Cyhalothrin, Total 2 0.015 0.028 0.01 U.S.

33 Spinach / Cyhalothrin, Total 2 0.015 0.022 0.01 U.S.

34 Spinach / Deltamethrin 1 0.12 0.19 0.05 U.S.

35 Spinach / Deltamethrin 1 0.12 0.18 0.05 U.S.

36 Spinach / Deltamethrin 1 0.12 0.15 0.05 U.S.

37 Spinach / Deltamethrin 1 0.12 0.12 0.05 U.S.

38 Strawberries / Acetamiprid 0.001 0.89 0.60 U.S.

39 Strawberries / Myclobutanil 0.003 0.55 0.50 U.S.

APPENDIX J. SAMPLES REPORTED TO FDA AS EXCEEDING THE TOLERANCE

OR WITHOUT ESTABLISHED TOLERANCE

(per Code of Federal Regulations, Title 40, Part 180)
Appendix J. Page 2 of 5

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm

Country of 

Origin

40 Strawberries / Myclobutanil 0.003 0.52 0.50 U.S.

41 Sweet Potatoes / Bifenthrin 0.01 0.088 0.05 U.S.

42 Sweet Potatoes / Bifenthrin 0.01 0.084 0.05 U.S.

43 Sweet Potatoes / Cyazofamid 0.02 0.054 0.02 U.S.

44 Sweet Potatoes / Deltamethrin 1 0.12 0.13 0.04 U.S.

45 Sweet Potatoes / Piperonyl butoxide 0.015 18 10 U.S.

46 Tomatoes / Tetrahydrophthalimide (THPI) 3 0.004 0.089 0.05 Mexico

47 Tomatoes / Tetrahydrophthalimide (THPI) 3 0.004 0.087 0.05 Mexico

48 Tomatoes / Tetrahydrophthalimide (THPI) 3 0.004 0.081 0.05 Mexico
Appendix J. Page 3 of 5

Commodity / Pesticide U.S. Import Unk.

1 Cherries, Frozen (5 pesticides)

Imazalil 144 1 0.7 0.028 ^ 0.005 ^ 0 1 0

Linuron 144 1 0.7 0.026 ^ 0.007 ^ 0 1 0

Monocrotophos 144 1 0.7 0.037 ^ 0.017 ^ 0 1 0

Pirimicarb 144 1 0.7 0.011 ^ 0.002 ^ 0 1 0

Tebufenpyrad 144 1 0.7 0.007 ^ 0.005 ^ 0 1 0

2 Cranberries (1 pesticide)

Chlorpropham 156 1 0.6 0.007 ^ 0.005 ^ 1 0 0

3 Cucumbers (5 pesticides)

Chlorpropham 754 7 0.9 0.005 - 0.014 0.005 ^ 3 3 1

Fenamiphos (parent) 4

 Fenamiphos sulfone 754 8 1.1 0.005 - 0.026 0.005 ^ 3 4 1

 Fenamiphos sulfoxide 754 10 1.3 0.010 - 0.081 0.005 ^ 4 5 1

Iprodione 754 1 0.1 0.022 ^ 0.005 ^ 0 1 0

Monocrotophos 754 1 0.1 0.081 ^ 0.010 ^ 0 1 0

Quintozene (PCNB) 754 1 0.1 0.005 ^ 0.005 ^ 0 1 0

4 Grapefruit (1 pesticide)

Ametoctradin 704 1 0.1 0.017 ^ 0.001 ^ 1 0 0

5 Grapes (3 pesticides)

Penconazole 708 4 0.6 0.007 - 0.037 0.004 ^ 1 3 0

Permethrin Total 708 1 0.1 0.010 ^ 0.006 ^ 1 0 0

Triadimenol 708 4 0.6 0.017 - 0.42 0.010 ^ 0 4 0

6 Green Beans (8 pesticides)

Carbofuran (parent) 567 3 0.5 0.002 - 0.012 0.001 ^ 0 3 0

 3-Hydroxycarbofuran 5 567 1 0.2 0.002 ^ 0.002 ^ 0 1 0

Difenoconazole 567 3 0.5 0.006 - 0.010 0.005 ^ 1 2 0

Dimethomorph 567 1 0.2 0.004 ^ 0.001 ^ 0 1 0

Oxamyl 567 1 0.2 0.005 ^ 0.002 ^ 0 1 0

Permethrin Total 567 1 0.2 0.097 ^ 0.040 ^ 0 1 0

Propamocarb hydrochloride 567 13 2.3 0.001 - 0.14 0.001 ^ 2 10 1

Pyrimethanil 567 2 0.4 0.004 - 0.32 0.001 ^ 0 2 0

Trifloxystrobin 567 1 0.2 0.013 ^ 0.001 ^ 0 1 0

7 Lettuce (3 pesticides)

Oxamyl (parent) 6 756 1 0.1 0.017 ^ 0.003 ^ 0 0 1

 Oxamyl oxime 756 1 0.1 0.006 ^ 0.006 ^ 0 0 1

Propiconazole 756 1 0.1 0.021 ^ 0.010 ^ 1 0 0

Trifluralin 756 2 0.3 0.001 - 0.002 0.001 ^ 2 0 0

Sample Origin

Distribution of Residues with No Tolerance Listed in 40 CFR, Part 180, 

Range of 

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

by Commodity/Pesticide
Appendix J. Page 4 of 5

Commodity / Pesticide U.S. Import Unk.

Range of Sample Origin

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

8 Olives, Canned (3 pesticides)

Carbendazim (MBC) 7 189 4 2.1 0.002 ^ 0.001 ^ 4 0 0

Fluridone 189 3 1.6 0.002 ^ 0.001 ^ 3 0 0

Tebuconazole 189 6 3.2 0.006 - 0.034 0.005 ^ 5 1 0

9 Pears (1 pesticide)

Imazalil 707 1 0.1 3.0 ^ 0.003 ^ 0 1 0

10 Potatoes (3 pesticides)

Emamectin benzoate 708 1 0.1 0.002 ^ 0.001 ^ 1 0 0

Imazalil 708 1 0.1 0.004 ^ 0.001 - 0.003 1 0 0

Norflurazon desmethyl 708 2 0.3 0.002 ^ 0.001 ^ 2 0 0

11 Spinach (20 pesticides)

Carbendazim (MBC) 7 707 1 0.1 0.004 ^ 0.001 - 0.010 1 0 0

Chlorpropham 707 1 0.1 0.003 ^ 0.001 - 0.020 1 0 0

DCPA 707 36 5.1 0.002 - 0.008 0.001 - 0.020 36 0 0

Dicloran 707 3 0.4 0.004 ^ 0.002 - 0.020 3 0 0

Diflubenzuron 707 2 0.3 0.003 ^ 0.002 - 0.080 2 0 0

Dimethoate (parent) 8 707 1 0.1 0.010 ^ 0.002 - 0.010 1 0 0

 Omethoate 707 12 1.7 0.004 - 0.021 0.002 - 0.010 12 0 0

Etoxazole 358 1 0.3 0.002 ^ 0.001 ^ 1 0 0

Iprodione 707 2 0.3 0.015 - 0.042 0.009 - 0.030 2 0 0

Linuron 707 12 1.7 0.005 - 0.023 0.003 - 0.010 10 2 0

Metribuzin 707 1 0.1 0.037 ^ 0.002 - 0.020 1 0 0

Oxyfluorfen 358 14 3.9 0.002 - 0.004 0.001 ^ 14 0 0

Pendimethalin 707 18 2.5 0.002 - 0.011 0.001 - 0.035 15 3 0

Prometryn 358 14 3.9 0.002 - 0.007 0.001 ^ 14 0 0

Pronamide 707 2 0.3 0.002 ^ 0.001 - 0.015 2 0 0

Propamocarb hydrochloride 349 2 0.6 0.009 - 0.042 0.001 - 0.005 2 0 0

Pyrimethanil 707 1 0.1 0.002 ^ 0.001 - 0.005 1 0 0

Quinoxyfen 358 2 0.6 0.002 ^ 0.001 ^ 2 0 0

Quintozene - PCNB (parent) 9 707 1 0.1 0.002 ^ 0.001 - 0.025 1 0 0

 Pentachloroaniline (PCA) 707 4 0.6 0.002 - 0.005 0.001 - 0.005 4 0 0

Tetraconazole 358 6 1.7 0.002 - 0.006 0.001 ^ 6 0 0

Trifluralin 707 3 0.4 0.002 - 0.025 0.001 - 0.010 3 0 0

12 Strawberries (13 pesticides)

Chlorothalonil 472 1 0.2 0.053 ^ 0.005 ^ 0 1 0

Chlorpropham 530 2 0.4 0.003 - 0.009 0.003 ^ 2 0 0

Clofentezine 530 1 0.2 0.056 ^ 0.005 ^ 0 1 0

Fenazaquin 530 1 0.2 0.11 ^ 0.001 ^ 0 1 0

Fluopicolide 530 7 1.3 0.001 - 0.010 0.001 ^ 7 0 0

Methomyl 530 2 0.4 0.016 - 0.11 0.010 ^ 2 0 0

Monocrotophos 530 2 0.4 0.003 - 0.18 0.003 ^ 0 2 0

Norflurazon desmethyl 530 1 0.2 0.003 ^ 0.003 ^ 1 0 0

Propamocarb 530 2 0.4 0.002 - 0.006 0.001 ^ 2 0 0

Propargite 530 2 0.4 0.076 - 0.089 0.001 ^ 0 2 0

Spirodiclofen 530 2 0.4 0.098 - 0.28 0.003 ^ 0 2 0
Appendix J. Page 5 of 5

Commodity / Pesticide U.S. Import Unk.

Range of Sample Origin

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

Tebuconazole 530 1 0.2 0.028 ^ 0.005 ^ 1 0 0

Trichlorfon 530 3 0.6 0.004 - 0.009 0.003 ^ 2 1 0

13 Sweet Potatoes (2 pesticides)

Chlorpropham 532 4 0.8 0.020 - 0.038 0.020 ^ 4 0 0

Permethrin (parent) 10

 Permethrin cis 532 4 0.8 0.020 - 0.19 0.020 ^ 4 0 0

 Permethrin trans 532 7 1.3 0.013 - 0.28 0.010 ^ 7 0 0

14 Tomatoes (4 pesticides)

Carbendazim (MBC) 7 509 5 1 0.002 - 0.028 0.001 ^ 1 4 0

Chlorpropham 528 43 8.1 0.002 - 0.015 0.001 ^ 8 35 0

Fluazifop butyl 528 1 0.2 0.002 ^ 0.001 ^ 1 0 0

Thiabendazole 528 1 0.2 0.002 ^ 0.001 ^ 1 0 0

NOTES

1 Deltamethrin includes parent Tralomethrin.

2 Includes cyhalothrin lambda plus R157836 epimer.

3 Tetrahydrophthalimide (THPI) is a metabolite of Captafol and Captan.

4 Eight cucumber samples contained both the sulfone and sulfoxide metabolites of Fenamiphos.

5 One green bean sample contained both Carbofuran and its 3-Hydroxycarbofuran metabolite.

6 One lettuce sample contained both Oxamyl and its oxime metabolite.

7 Carbendazim (MBC) is a metabolite of Benomyl and Thiophanate methyl.

8 Omethoate is a metabolite of the parent, Dimethoate. No samples contained both the parent and its metabolite.

9 Pentachloroaniline (PCA) is a metabolite of the parent, Quintozene. No samples contained both the parent and its metabolite.

10 Four sweet potato samples contained both the cis and trans permethrin isomers.

Note:

For those pesticide/commodity pairs where the minimum detected value is less than the limit of quantitation (three times

the limit of detection), the reported values are estimates. In a few cases, this may apply to the maximum detected value.
PESTICIDE DATA PROGRAM

 Annual Summary, Calendar Year 2016

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