United States Department of Agriculture

December 2015

Dear Reader:

We are pleased to present the Pesticide Data Program’s (PDP) 24th Annual Summary for 

calendar year 2014. The U.S. Department of Agriculture (USDA), Agricultural Marketing 

Service (AMS), conducts this program each year to collect data on pesticide residues in 

food. This report shows that overall pesticide residues found in foods are at levels below the 

tolerances set by the U.S. Environmental Protection Agency (EPA).

The PDP provides reliable data that help assure consumers that the food they feed their families 

is safe. Over 99 percent of the products sampled through PDP had residues below the EPA 

tolerances. Ultimately, if EPA determines a pesticide is not safe for our families, it is removed 

from the market. This system of checks and balances provides Americans with the safest food 

supply in the world.

The PDP tests a wide variety of domestic and imported foods using a sound statistical program 

and the most current laboratory methods. The EPA uses the PDP data when looking at dietary 

pesticide exposure, a critical step to verify that all sources of exposure to pesticides meet U.S. 

safety standards. 

The PDP is not designed for enforcement of EPA pesticide residue tolerances. Rather, the 

U.S. Food and Drug Administration (FDA) is responsible for enforcing EPA tolerances. PDP 

provides FDA and EPA with monthly reports of pesticide residue testing and informs the FDA if 

residues detected exceed the EPA tolerance or have no EPA tolerance established. In instances 

where a PDP finding is extraordinary and may pose a safety risk, FDA and EPA are notified 

immediately. In such cases, USDA may also work with U.S. growers in an outreach effort to 

communicate possible pesticide regulatory decisions or improved agricultural practices.

The PDP works with State agencies representing all regions of the country and more than half 

of the U.S. population. In 2014, samples were collected and analyzed in California, Colorado, 

Florida, Maryland, Michigan, New York, North Carolina, Ohio, Texas, and Washington. The 

data reported by PDP corroborate that residues found in agricultural products sampled are at 

levels that do not pose risk to consumers’ health (i.e., are safe according to EPA). 

For more information about PDP, please visit our website at www.ams.usda.gov. For more 

information about pesticides and food, please visit EPA’s website at 

http://www.epa.gov/pesticides.

Agricultural Marketing Service

1400 Independence Avenue, SW, Washington, DC 20250-0201

Voice (202) 720-8998 Fax (202) 720-7135

An Equal Opportunity Provider and Employer
Pesticide Data Program—Annual Summary, Calendar Year 2014

iii

Contents

Page No.

Acknowledgements........................................................................................................................ vii

Executive Summary...................................................................................................................... ix

Acronyms and Abbreviations........................................................................................................ xi

Section I--Introduction............................................................................................................... 1

Section II--Sampling Operations............................................................................................... 4

Conceptual Framework.................................................................................................... 4

Sampling Procedures....................................................................................................... 5

2014 Sampling Operations.............................................................................................. 5

Fresh and Processed Commodities.................................................................................. 6

Infant Formula................................................................................................................. 10

Salmon............................................................................................................................. 11

Sampling Limitations...................................................................................................... 12

Section III--Laboratory Operations......................................................................................... 12

Overview.......................................................................................................................... 12

Fresh and Processed Commodities.................................................................................. 12

Oats and Rice................................................................................................................... 13

Infant Formula................................................................................................................. 13

Salmon............................................................................................................................. 13

Quality Assurance Program............................................................................................. 13

Section IV--Database Management.......................................................................................... 16

Electronic Data Path........................................................................................................ 16

Data Reporting............................................................................................................... 18

Section V--Sample Results and Discussion.............................................................................. 18

Overview......................................................................................................................... 18

Import Versus Domestic Residue Comparisons.............................................................. 19

Postharvest Applications................................................................................................. 20

Discussion of Results ..................................................................................................... 20

Special Projects............................................................................................................... 21

Environmental Contaminants.......................................................................................... 21

Tolerance Violations........................................................................................................ 22
Pesticide Data Program—Annual Summary, Calendar Year 2014

v

Figures Page No.

 1 Pesticide Data Program (PDP) Program Operations Support and Data Users................... 2

 2 Program Participants........................................................................................................... 3

 3 Commodity Origin.............................................................................................................. 9

 4 Origin of Selected Fresh Commodities: Blueberry and Green Bean Samples................... 11

 5 Pesticide Data Program (PDP) Data Pathway..................................................................... 17

Tables

 1 Pesticide Data Program (PDP) Commodity Collection Schedule for 2014........................ 6

 2 Distribution of Samples Collected by Each Participating State.......................................... 7

 3 Acceptable Products for Collected Commodities................................................................ 8

 4 Sample Preparation Steps for Analysis................................................................................ 14

 

Appendixes A-L

Appendix A Commodity History

Appendix B Distribution of Residues by Pesticide in Fruit and Vegetables

Appendix C Distribution of Residues by Pesticide in Oats

Appendix D Distribution of Residues by Pesticide in Rice

Appendix E Distribution of Residues by Pesticide in Infant Formula

Appendix F Distribution of Residues by Pesticide in Salmon

Appendix G Distribution of Residues for Environmental Contaminants

Appendix H Sample Origin by State or Country

Appendix I Import Versus Domestic Pesticide Residue Comparisons

Appendix J Pesticide Residues by Commodity

Appendix K Number of Pesticides Detected per Sample

Appendix L Fruit and Vegetable Samples Reported to the U.S. Food and Drug 

 Administration as Exceeding the Tolerance or Without Established 

 Tolerance
Pesticide Data Program—Annual Summary, Calendar Year 2014

vii

Acknowledgements

The States participating in the Pesticide Data 

Program (PDP) deserve special recognition for 

their contributions to the program. The dedication 

and flexibility of sample collectors allow the U.S. 

Department of Agriculture’s (USDA) Agricultural 

Marketing Service (AMS) to adjust sampling 

protocols when responding to changing trends 

in commodity distribution and availability. PDP 

acknowledges the contributions of the State 

laboratories in providing testing services to the 

program and the USDA National Agricultural 

Statistics Service for providing statistical support. 

PDP also acknowledges the exceptional support 

of the Health Effects Division staff of the U.S. 

Environmental Protection Agency, Office of 

Pesticide Programs, and the U.S. Food and 

Drug Administration, Center of Food Safety and 

Nutrition, Office of Food Safety, in helping to set 

the direction for PDP. 

 

Data presented in this report are the latest 

available and were collected and processed 

through the efforts of the following organizations:

USDA Program Administration

Agricultural Marketing Service

Science and Technology Program

1400 Independence Ave., SW

South Building, Mail Stop 0270

Washington, DC 20250

Ruihong Guo, Ph.D., Deputy Administrator, 

Science and Technology Program

(202) 720-8556, Facsimile (202) 720-6496

Diana Haynes, Director

Monitoring Programs Division, AMS

1400 Independence Ave, SW

Room 0611-S, Stop 0276

Washington, DC 20250: 

(202) 572-8167, Facsimile (202) 619-1724

Electronic-mail Address:

amsmpo.data@ams.usda.gov

Website:

http://www.ams.usda.gov/pdp

Participating State Agencies

California Department of Food and Agriculture

California Department of Pesticide Regulation

Colorado Department of Agriculture

Florida Department of Agriculture and

 Consumer Services

Maryland Department of Agriculture

Michigan Department of Agriculture and 

 Rural Development

New York Department of Agriculture and 

 Markets

North Carolina Department of Agriculture &

 Consumer Services

Ohio Department of Agriculture

Texas Department of Agriculture

Washington State Department of Agriculture

Participating Laboratories

California Department of Food and Agriculture

Division of Inspection Services

Center for Analytical Chemistry

3292 Meadowview Rd.

Sacramento, CA 95832

 

Florida Department of Agriculture and

 Consumer Services

Chemical Residue Laboratory

3125 Conner Blvd., Bldg. 3

Tallahassee, FL 32399-1650

Michigan Department of Agriculture and 

 Rural Development

Laboratory Division

1615 South Harrison Rd.

East Lansing, MI 48823-5224

New York Department of Agriculture 

 and Markets

Food Laboratory

6 Harriman Campus Road

Albany, NY 12235
Pesticide Data Program—Annual Summary, Calendar Year 2014

viii

Ohio Department of Agriculture

Consumer Analytical Laboratory

8995 East Main St.

Reynoldsburg, OH 43068

Texas Department of Agriculture

Pesticide Laboratory

1500 Research Parkway, Ste. B100

College Station, TX 77845

United States Department of Agriculture

Agricultural Marketing Service

National Science Laboratories

801 Summit Crossing Pl.

Gastonia, NC 28054

Washington State Department of Agriculture

Chemical and Hop Laboratory

21 N. 1st Ave., Ste. 106

Yakima, WA 98902
Pesticide Data Program—Annual Summary, Calendar Year 2014

ix

Executive Summary

In 1991, the U.S. Department of Agriculture 

(USDA), Agricultural Marketing Service (AMS), 

was charged with designing and implementing the 

Pesticide Data Program (PDP) to collect data on 

pesticide residues in food. PDP provides highquality data on residues in food, particularly foods 

most likely consumed by infants and children. This 

24th Pesticide Data Program summary presents 

results for samples collected in 2014.

This information is provided to the U.S. 

Environmental Protection Agency (EPA). Before 

a company can sell or distribute any pesticide in 

the United States of America, EPA must review 

studies on the pesticide to determine that it will 

not pose unreasonable risks to human health 

or the environment. Once EPA has made that 

determination, it will license or register that 

pesticide for use in strict accordance with label 

directions. 

Before allowing a pesticide to be used on a food 

commodity, EPA sets limits on how much of a 

pesticide may be used on food during growing, 

processing, and storage, and how much can remain 

on the food that reaches the consumer. Government 

inspectors monitor food in interstate commerce to 

ensure that these limits are not exceeded. EPA also 

sets standards to protect workers from exposure to 

pesticides on the job. 

AMS’s Monitoring Programs Division (MPD) is 

responsible for the administration, planning, and 

coordination of day-to-day PDP operations. MPD 

meets regularly with EPA and other Government 

agencies to establish program priorities and 

direction. Sampling and/or testing program 

operations were carried out with the support of 10 

States: California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, Texas, 

and Washington. These States had a prominent role 

in program planning and policy setting, particularly 

policies relating to quality assurance.

PDP commodity sampling is based on a rigorous 

statistical design that ensures the data are reliable 

for use in exposure assessments and can be used 

to draw various conclusions about the Nation’s 

food supply. The pesticides and commodities to 

be included each year in the sampling are selected 

based on EPA data needs and take into account the 

types and amounts of food consumed by infants 

and children. The number of samples collected by 

the States is apportioned according to that State’s 

population. Samples are randomly chosen close to 

the time and point of consumption (i.e., distribution 

centers rather than at the farm gate) and reflect what 

is typically available to the consumer throughout 

the year. Samples are selected without regard to 

country of origin, variety, or organic labeling.

Fresh and processed fruit and vegetables accounted 

for 80.8 percent of the total 10,619 samples 

collected in 2014. Other samples collected 

included infant formula, 9.9 percent; salmon, 3.3 

percent; and oats and rice, 3.0 percent each. Fresh 

and processed fruit and vegetables tested during 

2014 were: apples, bananas, blueberries (fresh and 

frozen), broccoli, carrots, celery, cherries (fresh and 

frozen), grape juice, green beans (fresh, frozen, and 

canned), nectarines, peaches, strawberries, summer 

squash, sweet corn (fresh and frozen), tomatoes, 

and watermelon. Domestic samples accounted for 

75.5 percent of the samples while 22.9 percent 

were imports, 0.7 percent were of mixed origin, 

and 0.9 percent were of unknown origin.

Because PDP data are mainly used for risk 

assessments, PDP laboratory methods are geared 

to detect the lowest possible levels of pesticide 

residues, even when those levels are well below 

the tolerances established by EPA. Prior to testing, 

PDP analysts washed samples for 15-20 seconds 

with gently running cold water as a consumer 

would do; no chemicals, soap, or any special wash 

was used. Results for more than 2 million analyses 

were reported by the laboratories in 2014 and are 

too numerous to be included in their entirety in 

this summary. The PDP database file for 2014 and 

annual summaries/database files for previous years 

are available on the PDP website at http://www.

ams.usda.gov/pdp or by contacting MPD.

In 2014, over 41 percent of the samples tested 

had no detectable pesticide residue, and over 99 

percent of the samples tested had residues below 
Pesticide Data Program—Annual Summary, Calendar Year 2014

x

the tolerances established by the EPA. Appendixes 

B through G provide a distribution of residues by 

pesticide for the commodities tested. Residues 

exceeding the tolerance were detected in 0.36 

percent (38 samples) of the total samples tested 

(10,619 samples). Of these 38 samples, 19 were 

imported (50 percent) and 19 were domestic (50 

percent). Residues with no established tolerance 

were found in 2.6 percent (281 samples) of the 

total samples tested (10,619 samples). Of these 

281 samples, 138 were domestic (49.1 percent), 

140 were imported (49.8 percent), and 3 were of 

unknown origin (1.1 percent). PDP is a voluntary 

program and is not designed for enforcement of 

tolerances. However, PDP informs the U.S. Food 

and Drug Administration and EPA if residues 

detected exceed the EPA tolerance or have no EPA 

tolerance established. 

PDP laboratories also test foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in 

the environment, particularly in soil, can be taken up 

by plants. Results for environmental contaminants 

in all commodities are listed in Appendix G. More 

information on results is provided in the Sample 

Results and Discussion section of this summary.

PDP continually strives to improve methods for 

collecting, testing, and reporting data. These data 

are freely available to EPA and other Federal and 

State agencies charged with regulating and setting 

policies on the use of pesticides and to the public 

by hard copy, Internet, or custom reports generated 

by MPD. Additional copies of the PDP Annual 

Summary may be obtained by mailing the form 

provided at the end of the Summary.

The U.S. Department of Agriculture (USDA) prohibits discrimination in all its programs and activities on the basis of race, color, national origin, age, disability, 

and where applicable, sex, marital status, familial status, parental status, religion, sexual orientation, genetic information, political beliefs, reprisal, or because 

all or part of an individual’s income is derived from any public assistance program (not all prohibited bases apply to all programs). Persons with disabilities 

who require alternative means for communication of program information (Braille, large print, audiotape, etc.) should contact USDA’s TARGET Center at 

(202) 720-2600 (voice and TDD). To file a complaint of discrimination, write to USDA, Director, Office of Civil Rights, 1400 Independence Avenue, S.W., 

Washington, D.C. 20250-9410, or call (800) 795-3272 (voice) or (202) 720-6382 (TDD). USDA is an equal opportunity provider and employer.

Disclaimer: Mention of a trade name or brand name does not constitute endorsement or recommendation by USDA over 

similar products or vendors.
Pesticide Data Program—Annual Summary, Calendar Year 2014

xi

Acronyms and Abbreviations

% C.V. Percent Coefficient of Variation

A2LA American Association for Laboratory Accreditation

AL Action Level

AMS Agricultural Marketing Service

BQL Below Quantifiable Level

EPA U.S. Environmental Protection Agency

e-SIF Electronic Sample Information Form

FAPAS Food Analysis Performance Assessment Scheme

FDA U.S. Food and Drug Administration

FQPA Food Quality Protection Act

GC Gas Chromatography

HCB Hexachlorobenzene

ISO International Organization for Standardization

LC Liquid Chromatography

LOD Limit of Detection

LOQ Limit of Quantitation

MPD Monitoring Programs Division

MRM Multiresidue Method

MS Mass Spectrometry

NASS National Agricultural Statistics Service

NSL National Science Laboratories

PDP Pesticide Data Program

PPS Probability proportionate-to-size

PT Proficiency Testing

QA Quality Assurance

QAU Quality Assurance Unit

QuEChERS Quick, Easy, Cheap, Effective, Rugged and Safe
Pesticide Data Program—Annual Summary, Calendar Year 2014

xii

QC Quality Control

RDE Remote Data Entry

SIF Sample Information Form

SOP Standard Operating Procedure

THPI Tetrahydrophthalimide

USDA United States Department of Agriculture
Pesticide Data Program—Annual Summary, Calendar Year 2014

1

Pesticide Data Program (PDP)

Annual Summary, Calendar Year 2014

This summary consists of the following sections: (I.) Introduction, (II.) Sampling Operations, 

(III.) Laboratory Operations, (IV.) Database Management, and (V.) Sample Results and Discussion

I. Introduction

The U.S. Department of Agriculture’s (USDA) 

Agricultural Marketing Service (AMS) initiated 

the Pesticide Data Program (PDP) in 1991 to 

collect data on pesticide residues in food and 

now has an important role in the implementation 

of the 1996 Food Quality Protection Act (FQPA). 

The law directs the Secretary of Agriculture to 

collect pesticide residue data on commodities most 

frequently consumed by infants and children. PDP 

data are used primarily by the U.S. Environmental 

Protection Agency (EPA) to assess dietary 

exposure during the review of the safety of existing 

pesticide tolerances (Maximum Residue Limits). 

PDP data also are used by the U.S. Food and 

Drug Administration (FDA) to assist in planning 

commodity surveys for pesticide residues from an 

enforcement/regulatory perspective.

Because PDP collects data on food commodities 

primarily for exposure assessment, program 

operations differ markedly from those followed 

by regulatory monitoring programs for tolerance 

enforcement. Commodities chosen for inclusion 

in the program are based on EPA data needs. 

PDP samples are collected closer to the point of 

consumption and are prepared emulating consumer 

practices. PDP sampling does not impede 

commodity distribution. Laboratory operations 

are designed to achieve the lowest detectable 

levels rather than quick sample turnaround. As 

a dietary risk assessment support program, PDP 

tests for registered uses for the commodities in the 

program, as well as for pesticides that may not have 

U.S. tolerances but are used in other countries on 

commodities exported to the United States.

Figure 1(a) illustrates contributors to PDP 

policy development and planning operations. 

Primary contributors to these activities include 

the participating States, EPA, USDA’s National 

Agricultural Statistics Service (NASS), and 

additional stakeholders including industry and 

grower groups. Figure 1(b) depicts PDP primary 

data users including EPA, FDA, USDA’s Economic 

Research Service and Foreign Agricultural Service, 

participating States, academic institutions, chemical 

manufacturers, environmental interest groups, 

food safety organizations, and groups within the 

private sector representing food producers. Other 

Federal, State, and foreign government agencies 

and industries have used PDP data to promote 

the export of U.S. commodities to international 

markets. Additionally, the Codex Alimentarius 

Committee on Pesticides Residues recognizes PDP 

methodologies as official and validated methods 

for the determination of pesticide residues in foods.

In 2014, sampling services were provided by 10 

States (California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, 

Texas, and Washington). Laboratory services 

were provided by the States of California, Florida, 

Michigan, New York, Ohio, Texas, and Washington, 

along with the Agricultural Marketing Service 

(AMS), National Science Laboratories (NSL). The 

AMS Monitoring Programs Division (MPD) is 

responsible for overall management of PDP.

Figure 2 shows the States that participate in 

program sampling and/or testing. Together, these 

States represent about 50 percent of the Nation’s 

population and all four census regions of the United 

States. They also represent major U.S. producers 

of fruit and vegetables. MPD works closely with 

EPA and FDA to select commodities and pesticides 

for testing. The selected commodities represent 

the highest U.S. consumption, with an emphasis 

on foods consumed by infants and children. 

Commodities are cycled through the program 

approximately every 5 years. High-consumption 

fresh fruit and vegetable commodities remain in 

the program for 2 years to capture two full growing 

seasons, thereby capturing any changes due to 

seasonality or year-to-year variations. Processed 

products, as well as dairy, meat, fish, and grains, are 

tested for 1 full year. Appendix A provides a list of 

commodities tested by PDP from the beginning of 

the program in 1991 through 2015.
Pesticide Data Program—Annual Summary, Calendar Year 2014

2

Figure 1. Pesticide Data Program (PDP) Program Operations Support and Data Users. This figure 

illustrates (a) agencies/groups that support PDP program policy and planning activities and (b) agencies/groups 

that use PDP data. 

Program Operations

Participating 

States

National

Agricultural Statistics 

Service

Industry and

Grower Groups

Environmental

Protection

Agency

(a) PDP Policy and Planning Contributions

Data

Food and Drug 

Administration Environmental 

Protection 

Agency

Academic 

Institutions

Agricultural 

Industry

Foreign 

Agricultural 

Service

Economic 

Research 

Service

Chemical 

Manufacturers, 

Environmental 

Interest Groups, Food 

Safety Organizations

Other 

Government 

Agencies

Participating 

States

(b) PDP Data Users
Washington

California

Colorado

Texas

Ohio

New York

Florida

Maryland

Michigan

Participating State

Location of Participating State Laboratories

North Carolina

Location of Participating Federal Laboratory

Pesticide Data Program—Annual Summary, Calendar Year 2014

3

Fruit and vegetable samples are collected at terminal 

markets1 and large chain store distribution centers 

from which food commodities are supplied to 

supermarkets and grocery stores. Sampling at these 

locations allows for residue measurements that 

include pesticides applied during crop production 

and those applied after harvest (such as fungicides, 

growth regulators, and sprouting inhibitors) and 

takes into account residue degradation while food 

commodities are in storage. Participation as a 

PDP sampling site is voluntary, which sets it apart 

from State and Federal enforcement programs. In 

2014, over 600 sites granted access and provided 

information, including site volume data, to sample 

collectors. Voluntary cooperation is important to PDP 

and makes it possible to adjust sampling protocols 

in response to fluctuations in food distribution and 

production.

Pesticides screened by PDP include those with 

current registered uses for the commodity being 

tested and compounds for which toxicity data and 

preliminary estimates of dietary exposure indicate 

the need for more extensive residue data. PDP also 

monitors pesticides for which EPA has modified 

use directions (i.e., reduced application rates or 

frequency) as part of risk management activities. 

In addition, PDP tests for selected pesticides that 

may not have U.S. tolerances but are used in other 

countries that export commodities to the United 

1

 Terminal markets are facilities where wholesalers receive large quantities of fresh fruit and vegetables by rail, truck 

and air from around the world for sale to grocers, restaurants, institutions, and other businesses. Terminal markets are 

often located in metropolitan areas at or near major transportation hubs.

Figure 2. Program Participants. During 2014, USDA’s Agricultural Marketing Service established cooperative agreements 

with 10 States to sample and/or test Pesticide Data Program commodities. Together, these States represent about 50 percent 

of the Nation’s population and all four census regions of the United States. They also represent major U.S. producers of fruit 

and vegetables. State laboratories were responsible for analyzing fresh and processed fruit and vegetables, infant formula, and 

salmon. The USDA National Science Laboratory analyzed the rice and oat samples.
Pesticide Data Program—Annual Summary, Calendar Year 2014

4

States. The following appendices list the specific 

pesticides tested in the program: fruit and vegetables 

(Appendix B), oats (Appendix C), rice (Appendix D), 

infant formula (Appendix E), and salmon (Appendix 

F). Environmental contaminants, or pesticides 

whose uses have been canceled in the United States 

but their residues persist in the environment, are 

consolidated into Appendix G, which summarizes 

findings for these chemicals across all commodities. 

II. Sampling Operations

♦ Conceptual Framework

The goal of the PDP sampling program is to obtain 

a statistically valid representation of the U.S. food 

supply. PDP data reflect actual pesticide residue 

exposure from food. Using a rigorous statistical 

design, PDP has developed extensive procedures 

that ensure samples are randomly selected from the 

national food distribution system and reflect what is 

typically available to the consumer.

Ten States currently participate in PDP–California, 

Colorado, Florida, Maryland, Michigan, New York, 

North Carolina, Ohio, Texas, and Washington. 

Participating States were selected based on 

agricultural production, analytical capabilities, 

population, and geographic distribution. Together, 

these States represent about 50 percent of the 

Nation’s population and all four census regions of 

the United States.

Commodities chosen for inclusion in the program 

are based on EPA data needs. Foods selected for 

testing are high-consumption items with a strong 

focus on foods that are highly consumed by infants 

and children. Each fresh commodity is sampled 

and tested for 2 years in order to capture annual and 

seasonal variability. High-consumption items are 

rotated in and out of the program every 5 years – for 

example, apples, lettuce, oranges are retested and 

the data refreshed every 5 years.

A minimum of 600 samples per commodity per year 

is required in order to provide an accurate statistical 

representation for a given commodity. PDP collects 

additional samples to allow apportionment among 

the participating States over a 12-month period and 

to allow for a small sample overage for any missed, 

damaged, or unusable samples. Participating 

State population figures are used to apportion 

the number of samples scheduled for collection 

each month. PDP sampling operations may be 

adjusted according to product availability. For 

example, cherries, peaches, and nectarines may be 

oversampled during the summer months to make 

up for low availability during winter months.

PDP samples are collected at terminal markets and 

warehouse distribution centers, close to the point of 

consumption. Participating State agencies compile 

and maintain lists of these sampling sites. In 2014, 

over 600 sites granted access to sample collectors. 

The States provide AMS and NASS with annual 

volume information for commodities distributed 

at these sites. Based on this information, sites are 

assigned volume indicators compared to other sites 

in the same State. This volume indicator is used to 

ensure larger sites are selected more frequently than 

smaller sites. This information is used to weight 

the site to determine the probability for sample 

selection. For example, a weight of 10 may be 

given to a site that distributes 100,000 pounds of 

produce annually and a weight of 1 is given to a site 

that distributes 10,000 pounds. This site selection 

method, termed probability-proportionate-to-size 

(PPS), then results in the larger site being 10 times 

more likely to be selected for sampling than the 

smaller site. 

Each participating State works with NASS to 

develop statistical procedures for site weighting 

and selection. States are also given the option to 

have NASS perform their quarterly site selection. 

The number of sampling sites and the volume of 

produce distributed by the sites vary greatly among 

States. Sampling plans that include sampling dates, 

sites (primary and alternate), targeted commodities, 

and testing laboratories are prepared by each State 

on a quarterly basis. Collection of commodities is 

randomly assigned to weeks of the month, prior to 

selection of specific sampling dates within a week. 

Because sampling sites are selected for an entire 

quarter, States may assign the sites to particular 

months based on geographic location.

Sample information is captured at the time of 

collection for inclusion in the PDP database. PDP 

sample origin data identify the State or country 
Pesticide Data Program—Annual Summary, Calendar Year 2014

5

where the commodity was produced. A comparison 

of PDP sample origin data to State production and 

import data by USDA’s NASS shows PDP sampling 

is representative of the U.S. food supply. 

♦ Sampling Procedures

PDP State sample collectors are trained to adhere 

to detailed program Standard Operating Procedures 

(SOPs) that provide criteria for site selection and 

specific instructions for sample selection, shipping 

and handling, and chain-of-custody. SOPs are 

updated as needed and serve as a technical reference 

in conducting program sampling reviews to ensure 

program goals and objectives are met. SOPs for 

PDP sampling are available on the Internet at 

www.ams.usda.gov/pdp. On a quarterly basis, 

sample collectors are provided with Commodity 

Fact Sheets that list specific collection details for 

individual commodities that have been added to the 

program.

Temperature-sensitive samples are packed in heavyduty, temperature-controlled containers. Holding 

temperatures are preserved throughout transit time 

with the inclusion of ample frozen cold packs and 

insulating materials. Non-temperature-sensitive 

samples do not require temperature-controlled 

containers; however, they are shipped in heavy-duty, 

well-cushioned containers. To preserve sample 

integrity, most samples are shipped the same day as 

collection by overnight delivery. Non-refrigerated 

processed commodities such as grape juice, oats, 

rice, and infant formula are often shipped by ground 

transportation to reduce shipping costs. 

Electronic Sample Information Forms (e-SIFs) 

are used for chain-of-custody and to capture 

information needed to characterize the sample. 

Sample collectors use tablets or laptop computers in 

the field to record sample identification information 

such as: (1) State of sample collection, (2) collection 

date, (3) sampling site code, (4) commodity code, 

and (5) testing laboratory code. Information from 

these five data elements is combined to form a 

unique PDP identification number for each sample. 

Other available information about each sample is 

also recorded, such as collector name; the State or 

country of origin; product variety; production claims 

such as organic; postharvest chemical applications; 

and grower, packer, and/or distributor locations. 

The e-SIFs are electronically mailed the same 

day as sample collection or, at the latest, by 

the next morning after collection to ensure that 

sample information is received at each laboratory 

by the time samples arrive for analysis. Refer to 

Section IV on Database Management for more 

information on the e-SIF system. 

♦ 2014 Sampling Operations

The number of fruit, vegetable, oat, rice, infant 

formula, and salmon samples collected in 

each participating State is determined by State 

population. The quarterly collection schedule for 

all 2014 commodities is shown in Table 1. The 

total number of samples collected in each State 

for each commodity is listed in Table 2. Figure 2 

illustrates the participating collection States and 

the laboratories to which samples were shipped. 

Table 3 lists the acceptable product types for 

each collected commodity as seen on Commodity 

Fact Sheets provided to sample collectors. For 

all commodities, domestic or imported and 

organically grown or conventionally grown 

products are acceptable.

State population figures are used to assign the 

number of fruit, vegetable, and other specialty 

samples scheduled for collection each month. 

At the beginning of 2014, these population- and 

distribution-network-based numbers resulted in 

the following monthly collection assignments for 

each State: California, 13; Colorado, 2; Florida, 

7; Maryland, 4; Michigan, 6; New York, 9; Ohio, 

6; Texas, 8; and Washington, 4. This schedule 

resulted in a monthly target of 59 samples per 

commodity, or 708 samples per commodity per 

year. Additionally, North Carolina collected four 

samples per month for selected commodities–

green beans (fresh, frozen, and canned), peaches, 

oats, rice, and watermelon. 

In 2014, fruit, vegetables, oats, rice, infant 

formula, and salmon were randomly collected by 

trained State inspectors at terminal markets and 

large chain store distribution centers throughout 

the country. Surrogate or “proxy” sites (retail 

markets) are used to collect these samples when the 

commodity of interest is unavailable at a terminal 
Pesticide Data Program—Annual Summary, Calendar Year 2014

6

market or distribution center. In these instances, 

the commodity is selected in the rear storage area 

of the retail facility so possible contamination by 

the consumer is eliminated and to allow capture of 

sample information from product boxes. In 2014, 

36.8 percent of fruit, vegetable, oats, rice, infant 

formula, and salmon samples were collected at 

proxy sites. The commodities most often collected 

at these facilities were frozen cherries, infant 

formula, oats, grape juice, frozen blueberries, rice, 

salmon, and canned green beans. 

The total number of samples per commodity and 

the percentage of each that were either domestic, 

imported, or of unknown origin are shown in Figure 

3. The origin of some fresh commodities can vary 

greatly throughout the year. Graphic examples 

of this variation can be found in Figure 4, where 

differences in origin (domestic versus import) are 

depicted by month for blueberries and green beans. 

Fresh and processed fruit and vegetable, oats, rice, 

infant formula, and salmon samples originated 

from 39 States, 1 U.S. Territory, and 31 foreign 

countries (refer to Appendix H). 

♦ Fresh and Processed Commodities 

Of all samples collected and analyzed in 2014, 

80.8 percent (8,582 of 10,619) were fruit and 

vegetables, including fresh and processed products. 

The fresh commodities collected for PDP were 

apples, bananas, blueberries, broccoli, carrots, 

celery, cherries, green beans, nectarines, peaches, 

strawberries, summer squash, sweet corn, tomatoes, 

and watermelon. The processed commodities 

included frozen blueberries, frozen cherries, grape 

juice (ready-to-serve and concentrate), canned and 

frozen green beans, frozen sweet corn, oats, rice, 

Commodity Jan-Mar Apr-Jun Jul-Sep Oct-Dec End Date

Apples Sep-16

Bananas Mar-14

Blueberries, Fresh/Frozen Dec-14

Broccoli Dec-14

Carrots Dec-14

Celery Dec-14

Cherries, Fresh/Frozen Mar-16

Dairy-based Formula Sep-14

Fish, Salmon Jun-14

Grape Juice Sep-14

Green Beans Sep-16

Green Beans, Canned Sep-14

Green Beans, Frozen Dec-14

Nectarines Dec-15

Oats Aug-14

Peaches Jun-15

Rice Aug-14

Soy-based Formula Sep-14

Strawberries Sep-16

Summer Squash Sep-14

Sweet Corn, Fresh/Frozen Sep-15

Tomatoes Sep-16

Watermelon Jun-15

Table 1. Pesticide Data Program (PDP) Commodity Collection Schedule for 2014. Samples are 

most often collected for a 2-year time period. Commodities are initiated or terminated in different 

quarters of the year so that new commodities are not brought into the program all at the same time. 

This table illustrates time ranges for the listed commodities. See Appendix A for the complete PDP 

commodity history (May 1991 through December 2015).
Pesticide Data Program—Annual Summary, Calendar Year 2014

7

State AP BB BN BR CB CE CH CR GB NE PC SS ST TO WM

Total 

Fresh

California 39 154 39 160 35 156 58 156 156 147 138 117 39 39 78 1,511

Colorado 6 24 6 24 1 24 8 24 24 24 22 18 6 6 12 229

Florida 21 78 21 84 20 84 21 84 85 103 100 63 20 21 55 860

Maryland 12 48 12 48 10 48 21 48 48 39 39 36 12 12 24 457

Michigan 18 72 18 72 13 72 18 72 72 87 90 54 18 18 39 730

New York 27 105 27 108 21 108 27 108 108 108 108 81 27 27 54 1,044

N. Carolina 48 28 99

Ohio 18 67 18 72 7 72 19 72 72 54 58 54 18 18 36 655

Texas 24 95 26 96 22 96 44 96 96 75 84 72 24 24 48 922

Washington 12 45 12 48 5 48 12 48 48 44 40 36 12 12 24 446

TOTAL 177 688 179 712 134 708 228 708 757 681 707 531 176 177 390 6,953

State BZ CS CZ GC GJ GZ

Total 

Processed

Total 

Fresh & 

Proccessed 

F&V

California 1 4 44 78 117 78 322 1,833

Colorado 3 9 12 18 12 54 283

Florida 6 1 42 43 63 42 197 1,057

Maryland 2 15 24 36 24 101 558

Michigan 5 36 36 54 36 167 897

New York 3 6 54 54 81 54 252 1,296

N. Carolina 24 24 48 147

Ohio 5 11 35 36 54 36 177 832

Texas 1 2 26 48 72 48 197 1,119

Washington 3 7 21 23 36 24 114 560

TOTAL 19 41 282 378 531 378 1,629 8,582

Grains

OA RI

64 65

10 10

35 35

20 19

30 30

45 45

20 20

30 30

40 40

20 20

314 314

Commodity Legend

AP = Apples CS = Sweet Corn, Frozen OA = Oats

BB = Blueberries, Cultivated, Fresh CZ = Cherries, Frozen PC = Peaches

BN = Bananas DF = Dairy-based Infant Formula RI = Rice

BR = Broccoli FS = Fish, Salmon SS = Summer Squash

BZ = Blueberries, Frozen GB = Green Beans, Fresh ST = Strawberries

CB = Sweet Corn, Fresh (on-the-cob) GC = Green Beans, Canned TO = Tomatoes

CE = Celery GJ = Grape Juice WM = Watermelon

CH = Cherries GZ = Green Beans, Frozen YF = Soy-based Infant Formula

CR = Carrots NE = Nectarines

Table 2. Distribution of Samples Collected by Each Participating State. This table includes those 

commodities collected at terminal markets, distribution centers, and retail markets. 

Fish

FS

78

12

42

24

36

54

36

48

24

354

Infant Formula

DF YF

114 114

18 18

63 63

36 36

54 54

81 81

54 54

72 71

36 36

528 527
Pesticide Data Program—Annual Summary, Calendar Year 2014

8

Commodity Acceptable Products

Apples All fresh, whole apples.

Bananas Whole, fresh bananas.

Blueberries, 

Cultivated Fresh

Any fresh, whole blueberry. Cultivated (Highbush) or wild (Lowbush). Fresh are preferred, but 

frozen are acceptable.

Blueberries, Frozen Frozen blueberries. Cultivated (Highbush) or wild (Lowbush). Individually quick frozen (IQF) or 

frozen in own juice.

Broccoli Fresh broccoli. Broccoli crowns (bunch with top florets plus a little of the stem) are preferred. 

Broccoli with stems (bunch with top florets plus a lot of the stem) is acceptable if broccoli crowns 

are not available.

Carrots Fresh, whole carrots, with or without tops.

Celery Fresh, whole celery.

Cherries Any fresh, whole sweet cherry. Fresh are preferred, but frozen are acceptable.

Cherries, Frozen Frozen sweet cherries. Individually quick frozen or frozen in own juices.

Grape Juice 100% Grape Juice. Concord, red or white grape juice. Added nutritional ingredients such as 

citric acid and ascorbic acid. Ready-to-serve or frozen concentrate are rotated according to 

a fixed schedule. Ready-to-serve: single strength (grape juice may have been reconstitutued 

from concentrate). Shelf-stable or refrigerated. Individual single-serving boxes with the same lot 

number. Frozen concentrate includes cans of concentrated grape juice that are frozen. Nonconcentrated grape juice may not be substituted for frozen grape juice concentrate.

Green Beans Fresh green string beans. Whole or pre-cut.

Green Beans, 

Canned

Canned green beans only. Whole style, kitchen sliced, cut or French cut. May contain salt, citric 

acid, calcium chloride, or sugar as ingredients.

Green Beans, Frozen Frozen green beans. Any style cut (string beans, cut, French cut, etc.).

Infant Formula, DairyBasedAny dairy-based infant formula. Powdered, concentrated liquid, or ready-to-eat. Samples may 

contain ARA, DHA, Choline, vitamins, minerals (e.g., iron, zinc, etc.), probiotics, and prebiotics. 

Formula with pre-digested proteins (i.e., hydrolyzed proteins).

Infant Formula, SoyBasedAny soy-based infant formula. Powdered, concentrated liquid, or ready-to-eat. Samples may 

contain ARA, DHA, Choline, vitamins, minerals (e.g., iron, zinc, etc.), probiotics, and prebiotics. 

Formula with pre-digested proteins (i.e., hydrolyzed proteins).

Nectarines Any fresh, whole nectarines.

Oats Whole grain oats (oat groats), rolled oats (old-fashioned oats), steel-cut oats (Irish oats, Scotch 

oats, pinhead oats, coarse-cut oats), oat bran.

Peaches Fresh, whole peaches. Red or white. Clingstone, freestone or semi-freestone. Attempt to select 

peaches that are not overly ripe or soft to the touch.

Rice Regular milled white rice (short, medium, and long grain), brown rice, basmati rice, jasmine rice, 

texmati rice. Polished rices. Arroz (Portuguese and Spanish word for long-grained rice).

Salmon Fresh or frozen raw (uncooked) salmon. Filets, nuggets, strips, or steaks; bones-in or no bones; 

Atlantic or Pacific; farm-raised or wild caught.

Strawberries Fresh, whole strawberries.

Summer Squash Fresh whole zucchini, yellow squash, or crookneck squash.

Sweet Corn Fresh corn-on-the-cob, with or without husks (samplers should not remove husks). When fresh 

on-the-cob corn is not available, bagged frozen niblet-style corn is acceptable.

Sweet Corn, Frozen Bagged frozen niblet-style corn in white kernels, yellow kernels, or a mixture (bread & butter).

Tomatoes Fresh tomatoes. Regular round varieties or Plum/Roma.

Watermelon Fresh whole watermelon, including seeded and seedless varieties. Watermelon cut into halves 

or quarters ONLY if whole is not available.

Table 3. Acceptable Products for Collected Commodities. This table lists the acceptable products for each 

collected commodity as seen on Commodity Fact Sheets provided to sample collectors. For all commodities, 

domestic or imported and organically grown or conventionally grown products are acceptable.
Pesticide Data Program—Annual Summary, Calendar Year 2014

9

Broccoli (712 Samples)

A. Fresh Fruit and Vegetable Samples

Peaches (707 Samples) Strawberries (176 Samples)

Cherries (228 Samples) Green Beans (757 Samples) Nectarines (681 Samples)

Carrots (708 Samples) Celery (708 Samples)

Bananas (179 Samples) Blueberries, Cultivated (688 Samples)

Summer Squash (531 Samples)

Domestic 77.6%

Domestic 88.2% Domestic 78.5% Domestic 95.5%

Domestic 44.2%

Import 21.9% Import 22.5%

Import 10.8%

Import 20.4% Import 3.8%

Import 55.8%

Unknown 0.7%

Unknown 1.1%

Domestic 72.8% Domestic 83.5% Domestic 60.1%

Domestic 75.8% Domestic 70.8%

Import 37.7% Import 26.5% Import 16.5%

Import 28.9%

Unknown 1.7% Unknown 0.3%

Unknown 0.7%

Import 0.6%

Apples (177 Samples)

Domestic 99.4%

Import 100%

Unknown 2.2%

Unknown 1.0%

Unknown 0.5%
Pesticide Data Program—Annual Summary, Calendar Year 2014

10

and infant formula. All fresh and frozen fruit and 

vegetable samples weighed either 3 or 5 pounds 

with the exception of blueberries which weighed 

1 pound. Three pounds were collected for 

smaller, low-weight commodities such as green 

beans, and 5 pounds were collected for larger, 

high-weight commodities such as bananas and 

watermelon. Juice and infant formula samples 

were 1 quart or 32 ounces. Canned samples were 

28 ounces. Grain samples were 1 pound for oats 

and 3 pounds for rice.

♦ Infant Formula 

In 2014, PDP tested two types of infant formula – 

dairy-based and soy-based. Acceptable samples 

included concentrated liquid, powdered, and 

ready-to-eat; domestic or imported; organic or 

conventional products. The minimum weight 

was enough to reconstitute to 32 ounces. PDP 

collected and tested 528 dairy-based samples and 

527 soy-based samples. For the 527 soy-based 

infant formula samples, 34 were concentrated 

B. Processed Fruit and Vegetable Commodities

Figure 3. Commodity Origin. This figure depicts the proportion of commodity origin (domestic, import, 

unknown, and mixed national origin) for each fresh and processed fruit and vegetable product tested in 2014.

Cherries, Frozen (282 Samples)

Domestic 37.9%

Import 61.0%

Green Beans, Canned (378 Samples)

Domestic 47.4%

Blueberries, Frozen

 (19 Samples)

Domestic 95.1%

Grape Juice (531 Samples)

Domestic 87.2%

Import 54.3%

Tomatoes (177 Samples)

Domestic 44.6%

Unknown 1.1%

Import 4.9%

Sweet Corn, Frozen (41 Samples)

Mixed National 1.1%

Import 52.6%

Domestic 99.2%

Unknown 0.3%

Import 25.9%

Watermelon (390 Samples)

Domestic 72.3%

Import 11.2%

Sweet Corn, Fresh (134 Samples)

Domestic 87.3%

Unknown 1.5%

Unknown 1.1% Unknown 1.8%

Green Beans, Frozen (378 Samples)

Domestic 89.4%

Mixed National 0.8%

Unknown 0.3%

Import 2.8%

Mixed National 8.9%

Import 9.5%

Import 0.5%
Pesticide Data Program—Annual Summary, Calendar Year 2014

11

liquid, 395 were powdered, and 98 were ready-toeat. For the 528 dairy-based infant formula samples, 

29 were concentrated liquid, 390 were powdered, 

and 109 were ready-to-eat. Samples were collected 

from routine PDP sampling sites, which included 

major distribution centers and terminal markets 

as well as proxy sites. Dairy-based samples were 

tested at the New York laboratory, and soy-based 

samples were tested at the California laboratory.

♦ Salmon

In 2013, EPA requested collection of salmon data 

to examine levels of pesticides present in salmon, 

whether from environmental contaminants or 

from pesticides used in aquaculture. Current, 

comprehensive data on pesticide residues on fish 

available for purchase by the U.S. consumer is 

largely unavailable. Sampling was designed to 

capture domestic and imported products, including 

farm-raised and wild-caught salmon. PDP sampled 

salmon available at designated sampling locations 

regardless of country of origin, in order to capture 

results for salmon consumed by the American public. 

PDP collected and analyzed 354 salmon samples in 

2014. Each sample consisted of 2 pounds of fresh 

or frozen raw salmon. Proxy/retail sites provided 

72.0 percent of salmon samples. Whole salmon 

samples were not collected; rather, only fillets, 

Figure 4. Origin of Selected Fresh Commodities: Blueberry and Green Bean Samples. Differences in origin 

(domestic vs. import) are illustrated by month. 

Origin of Blueberry Samples

Domestic Imported Unknown

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

Origin of Green Bean Samples

Number of Samples Number of Samples
Pesticide Data Program—Annual Summary, Calendar Year 2014

12

nuggets, strips, or steaks were obtained for testing. 

Both bones-in and no bones were acceptable sample 

types. To ensure salmon samples arrived at the 

laboratory in acceptable condition, samples were 

first frozen overnight and then shipped the following 

day by overnight air with ample frozen cold packs 

and insulating materials surrounding all sample 

units. Analysis was performed by the Washington 

State laboratory. 

Farm-raised or wild-caught and domestic or 

imported salmon were collected on a random, asavailable basis. The majority of samples were wildcaught and imported. Approximately 64 percent 

were wild-caught and 23 percent of the samples were 

farm-raised. The remainder of the samples had no 

available source information. Approximately 71.5 

percent were imported, while 28.5 percent of the 

samples originated in the United States. Distribution 

of residues in salmon may be found in Appendix F.

♦ Sampling Limitations

A limited number of States across the United States 

participate in PDP. The States that do participate 

account for about 50 percent of the U.S. population, 

all four census regions of the U.S., and the major 

agricultural production areas of the country, so are 

representative of the U.S. as a whole.

PDP collects samples from 600 distribution centers 

and terminal markets within the participating States. 

The total number of distribution centers and terminal 

markets within the participating States is difficult to 

establish since existing sites may go out of business 

or merge and new sites may open during the course 

of the year. However, sites within the States that 

participate do not differ significantly from those that 

do not participate; therefore, the selected sites are 

representative of all sites in the State. 

Sometimes it is necessary to replace the site that 

was originally selected using PPS. In those cases, 

an alternate site is selected by the State personnel to 

replace the original site. Whenever possible, a site 

of similar size in the same region as the original site 

is chosen as the replacement. Because participation 

in the PDP survey is voluntary and multiple visits 

can be detrimental to the goodwill of facility 

management, it is sometimes necessary to limit the 

number of times facilities are visited during a given 

month or quarter. Additionally, the availability of 

a specific commodity may necessitate a change in 

site selection. For example, if a site is selected for 

frozen green beans and that site only carries fresh 

produce, a replacement site is required.

III. Laboratory Operations 

♦ Overview

Seven State laboratories and one USDA laboratory 

performed analyses for PDP. These laboratories are 

equipped with instrumentation capable of detecting 

residues at very low levels. Laboratory staff members 

receive intensive training and must demonstrate 

analytical proficiency on an ongoing basis. Program 

scientists continually test new technologies and 

develop new techniques to improve the levels of 

detection. Major changes in methodology and/or 

instrumentation are evaluated and their soundness 

demonstrated and documented by means of method 

validation modules in accordance with PDP SOPs.

♦ Fresh and Processed Commodities

Fruit and vegetable samples were tested for 457 

parent pesticides, metabolites, degradates, and/or 

isomers, plus 22 environmental contaminants using 

Multiresidue Methods (MRMs). Pesticides screened 

by PDP include those with current registered uses 

for the commodity being tested and compounds for 

which toxicity data and preliminary estimates of 

dietary exposure indicate the need for more extensive 

residue data. 

Upon arrival at the testing facility, samples of 

fresh commodities were visually examined for 

acceptability and discarded if determined to be 

inedible (decayed, extensively bruised, or spoiled). 

Laboratories are permitted to refrigerate incoming 

fresh fruit and vegetable samples of the same 

commodity up to 72 hours to allow for different 

sample arrival times from collection sites. Frozen 

and canned commodities may be held in storage 

(freezer or shelf) until the entire sample set is ready 

for analysis.

Each sample is prepared according to the procedures 

detailed in Table 4, which lists the steps for 
Pesticide Data Program—Annual Summary, Calendar Year 2014

13

preparing each commodity for analysis as defined 

in the Laboratory Sample Processing and Analysis 

Standard Operating Procedure. For all commodities, 

the sample is chopped, mixed, or blended until a 

visually homogeneous mixture is attained. 

Samples are homogenized using choppers and/

or blenders and separated into analytical portions 

(aliquots) for analysis. If testing cannot be 

performed immediately, the entire analytical set is 

frozen at -40°C or lower, according to PDP’s Quality 

Assurance/Quality Control (QA/QC) requirements. 

Surplus aliquots not used for the initial testing 

are retained frozen in the event that replication of 

analysis or verification testing is required.

For analysis of fruit and vegetables, testing 

laboratories use various Quick, Easy, Cheap, 

Effective, Rugged and Safe (QuEChERS)-based 

approaches2. All MRMs are determined, prior to 

use and through appropriate method validation 

procedures, to produce equivalent data for PDP 

analytical purposes.

PDP laboratories use gas chromatography (GC) 

and liquid chromatography (LC) instrumentation, 

coupled with tandem mass spectrometry (MS) 

detection systems for the simultaneous identification/

confirmation and quantitation of pesticides. The use 

of these GC-MS/MS and LC-MS/MS systems allows 

the program to capture data for a broad spectrum of 

pesticides, including emerging product chemistries.

♦ Oats and Rice

The NSL analyzed 314 samples of oat grain and 

314 samples of rice. The number of pesticides, 

metabolites, degradates, and/or isomers tested were 

89 and 94 for oats and rice, respectively. In addition, 

13 environmental contaminants were screened in 

each commodity. Samples were prepared according 

to the procedures detailed in Table 4. Samples were 

extracted using a modification of the QuEChERS 

method, and analyses were performed utilizing GCMS/MS and LC-MS/MS as well as GC/MS in the 

negative chemical ionization mode.

♦ Infant Formula

In 2014, the California laboratory tested 527 

soy-based infant formula samples, and the New 

York laboratory tested 528 dairy-based infant 

formula samples. A total of 314 parent pesticides, 

metabolites, degradates, and/or isomers, plus 18 

environmental contaminants, were screened in the 

infant formula samples. Samples were prepared 

according to the procedures detailed in Table 4. 

Samples were extracted using modifications of the 

QuEChERS method, and analyses were performed 

utilizing GC-MS/MS and LC-MS/MS.

♦ Salmon

The Washington State laboratory analyzed 354 

samples of salmon for 166 parent pesticides, 

metabolites, degradates, and/or isomers, plus 

15 environmental contaminants. Samples were 

prepared according to the procedures detailed in 

Table 4. Samples were extracted using a modification 

of the QuEChERS method followed by analysis via 

GC-MS/MS and LC-MS/MS.

♦ Quality Assurance Program

The primary objectives of the QA/QC program 

are to ensure the reliability of PDP data and the 

performance equivalency of the participating 

laboratories. Direction for the PDP QA program 

is provided through SOPs initially based on EPA 

Good Laboratory Practices, along with programspecific QA/QC requirements. The PDP SOPs 

provide uniform administrative and sampling 

procedures, as well as laboratory operations and data 

analyses guidelines. The program SOPs are revised 

annually to accommodate changes in the program 

and are aligned with International Organization 

for Standardization (ISO)3 requirements. PDP 

laboratories are accredited to ISO 17025 by the 

2

 M. Anastassiades, S.J. Lehotay, D. Stajnbaher and F.J. Schenck, “Quick, Easy, Cheap, Effective, Rugged and Safe 

(QuEChERS) Method,” J AOAC Int 86 (2003) 412.

 3 “ISO” is not an acronym because the initials would be different in various official languages. “ISO” is adopted from the 

Greek word “isos” meaning equal.
Pesticide Data Program—Annual Summary, Calendar Year 2014

14

Commodity Sample Preparation Steps

Apples Wash and drain. Do not peel. Remove the stem. Remove the core using a commercially 

available apple corer, or cut each apple in half or quarters and remove the core portion. 

Bananas If necessary, banana samples may be stored in a secure location at room temperature for up to 

72 hours for ripening purposes. Peel each fruit. 

Blueberries, Cultivated Wash by the handful or by using a colander and drain.

Broccoli Visually examine and discard any damaged portion or wilted florets. Trim away inedible portions 

of stems. Wash and drain.

Carrots If carrots have any visible dirt, hold each carrot under cold running tap water and gently scrub 

the entire surface with a clean vegetable brush to remove any loose soil and grit. Wash and 

drain. Remove stem cap portion from each carrot.

Celery Using a clean, dry knife, remove the inedible portion of the stalk to allow stems to separate. 

Wash and drain.

Cherries Remove the stem from each cherry. Wash and drain. Remove the pit, being careful to remove as 

little of the meat as possible. 

Frozen Product: 

Blueberries, Cherries, 

Green Beans, Sweet Corn

The samples may be chopped while frozen, or to prevent damage to the chopper/homogenizer 

blades, the sample may be thawed in a refrigerator or in a room temperature water bath. Open 

the containers and pour the entire contents into the chopper/homogenizer. 

Grain Product: Oats, Rice Grind the entire grain sample using an appropriate device to obtain a homogeneous mixture. If 

a significantly large sample is received, a subsample can be homogenized at the target weight.

Grape Juice For fresh and reconstituted juices, ensure that sample is evenly mixed in order to obtain a 

homogeneous mixture. For concentrates, dilute juice in a dry, clean container with cold running 

tap water, according to label directions. 

Green Beans Wash and drain. Do not peel. Using a clean, dry knife, remove any stems that are present. 

Green Beans, Canned If the lid of the can has visible dirt or dust, rinse the lid under cold running tap water for 5 to 10 

seconds. Dry the lid with a paper towel. Open each can and pour the entire contents of each can 

including the liquid into a blender/homogenizer. 

Infant Formula: DairyBased, Soy-basedFor ready-to-eat samples, ensure that sample is evenly mixed in order to obtain a

homogeneous mixture. For concentrated liquid samples, dilute in a dry, clean container with 

reagent water, according to label directions and mix well to ensure a homogeneous mixture. For 

powdered samples, reconstitute in a dry, clean container with reagent water

according to label directions and mix well to ensure a homogeneous mixture.

Nectarines & Peaches Wash and drain. Do not peel. Remove stem and leaves if present. Using a clean, dry knife, cut 

the nectarine/peach around the pit (i.e., without cutting through the pit). Remove the pit, being 

careful to remove as little of the meat as possible. 

Salmon Mechanically homogenize each tissue until a visually homogeneous mixture is attained. Dry ice 

may be used during the homogenization procedure.

Strawberries Wash by the handful or by using a colander and drain. Remove stems and leaves if present. 

Summer Squash Wash and drain. Using a clean, dry knife, remove end pieces. 

Sweet Corn Remove husk and silk from each ear. Wash and drain. Using a clean dry knife or other 

appropriate utensil, remove the kernels from cob. 

Tomatoes Wash and drain. Do not peel. Using a clean, dry knife, cut the tomato around the stem area. 

Remove any stem, being careful to remove as little of the meat as possible. The tomatoes may 

be quartered prior to homogenization. 

Watermelon Wash and drain. Using a clean, dry knife, cut each watermelon into quarters, and remove the 

rind. For large watermelons take alternate quarters of each fruit for homogenization For small 

watermelons, homogenize the entire sample.

Table 4. Sample Preparation Steps for Analysis. This table lists the steps for preparing each collected commodity 

for analysis as defined in the Laboratory Standard Operating Procedure. The wash and drain steps refer to a wash 

under cold running water for approximately 15-20 seconds to ensure that all surfaces are rinsed, then drained for 

at least 2 minutes. For all commodities, the sample is chopped, mixed, or blended until a visually homogeneous 

mixture is attained.
Pesticide Data Program—Annual Summary, Calendar Year 2014

15

American Association for Laboratory Accreditation 

(A2LA), an internationally recognized accrediting 

body.

Laboratory Technical Advisory Group and Quality 

Assurance Officers: A Technical Advisory Group, 

comprised of laboratory Technical Program 

Managers and Quality Assurance Officers, is 

responsible for annually reviewing program SOPs 

and addressing QA issues. For day-to-day QA 

oversight, PDP relies on the Quality Assurance Unit 

(QAU) at each participating facility. The QAU 

operates independently from the laboratory staff 

and is responsible for reviewing all data generated 

for PDP and for performing quarterly, internal 

program audits. Preliminary data review procedures 

are performed onsite by each laboratory’s QAU. 

Final review procedures are performed by MPD 

staff assigned to each laboratory that is responsible 

for collating and reviewing data for conformance 

with SOPs.

Method Performance Requirements: Laboratories 

are required to determine and verify the limits of 

detection (LODs) and limits of quantitation (LOQs) 

for each pesticide/commodity pair. LODs depend 

on matrix, analyte, and methods used (extraction 

and instrumental). LODs for each pesticide/

commodity pair are shown in the applicable crop 

results appendix. Additional method performance/

validation requirements include modules for 

consistent instrument response (linearity), method 

range, and precision and accuracy.

Identification/Confirmation: Identification/confirmation is performed by MS technologies. Residue 

amounts greater than or equal to LOD and below 

LOQ are reported as below quantifiable level 

(BQL). BQLs are assigned values at one-half the 

LOQ and are used along with values greater than 

or equal to LOQ and non-detects in dietary risk 

assessments when appropriate.

Routine Quality Control Procedures: PDP 

procedures for QC are intended to assess method 

and analyst performance during sample preparation, 

extraction, and cleanup. To maximize sample 

output and decrease the QC/sample ratio, samples 

are analyzed in analytical sets that include the test 

samples and the following components:

• Reagent Blank - For analysis of fruit and 

vegetables, oats, rice, infant formula, and salmon, 

an amount of distilled water, equivalent to the 

natural moisture content of the commodity, is run 

through the entire analytical process to confirm 

glassware cleanliness and system integrity.

• Matrix Blank - A previously analyzed sample 

of the same commodity, which contains either 

very low concentrations of known residues or no 

detectable residues, is divided into two portions. 

The first portion is used to determine background 

information on naturally occurring chemicals and 

the second to prepare a matrix spike.

• Matrix Spike(s) - Prior to extraction, a portion of 

the matrix blank is spiked with marker pesticides to 

determine the precision and accuracy of the analyst 

and instrument performance. Marker pesticides 

are compounds selected from different pesticide 

classes (e.g., organochlorines, organophosphates, 

carbamates, conazoles, imidazolinones, macrocyclic lactones, neonicotinyls, phenoxy acid 

herbicides, pyrethroids, strobilurins, sulfonyl urea 

herbicides, triazines, uracils), with physical and 

chemical characteristics representative of their 

corresponding pesticide class. Marker pesticides 

may be used to monitor recovery instead of spiking 

all pesticides. This use of marker pesticides 

optimizes the resources required to analyze the 

thousands of analyte/matrix combinations in the 

program while still allowing evaluation of daily 

recovery patterns. In addition, each laboratory 

must perform matrix spikes at least quarterly 

for each analyte/crop combination it reports. 

Some laboratories choose to rotate spikes of 

all compounds on a set-to-set basis or spike all 

compounds analyzed with each set, so that the 

amount of spike recovery data obtained actually 

exceeds the minimal requirements previously 

stated. During 2014, PDP laboratories quantitated 

a total of 70,089 matrix spikes, with an overall 

mean recovery of 98 percent and an overall 22 

percent coefficient of variation (% C.V.). The % 

C.V. is calculated as the standard deviation divided 

by the mean.

• Process Control Spike - A compound with 

physical and chemical characteristics similar 

to those of the pesticides being tested is used 
Pesticide Data Program—Annual Summary, Calendar Year 2014

16

to evaluate the analytical process on a sampleby-sample basis. Each of the analytical set 

components, except the reagent and matrix blanks, 

is spiked with process controls. During 2014, PDP 

laboratories quantitated a total of 26,557 process 

controls on 10,619 samples, with an overall mean 

recovery of 99 percent and an overall 16 % C.V. 

Of these process controls, 8 (0.03 percent) were 

reruns due to initial failure to meet PDP recovery 

criteria. The rerun values are not included in these 

statistics.

Proficiency Testing: All facilities are required 

to participate in PDP’s Proficiency Testing 

(PT) program. In order to properly benchmark 

performance, PDP laboratories participate in 

an international PT program, the Food Analysis 

Performance Assessment Scheme (FAPAS) 

PT program, administered by the Food and 

Environment Research Agency, Sand Hutton, 

York, United Kingdom. In 2014, PDP laboratories 

that routinely analyze fruit and vegetables via 

MRMs participated in one FAPAS round for 

pears that contained eight fortified analytes. 

Laboratories were evaluated based on z-scores for 

reported compounds, as well as any reported false 

negatives or false positives. PDP laboratories 

typically obtained z-scores less than two, which is 

deemed satisfactory performance.

In addition, PDP laboratories participate in an 

internal PT program that is tailored to current 

PDP commodities and testing profiles. For this 

internal program, the California Department of 

Food and Agriculture QAU prepares and issues 

rounds designed by MPD. Spiking compounds 

are selected with specificity and levels for each 

commodity. Fortification levels of selected 

analytes are generally 1 to 10 times the program 

LOQ for that commodity/compound pair. For 

each multiresidue round, one compound per set 

is typically repeated within the round to provide 

an indicator of repeatability. The resulting data 

are used to determine performance equivalency 

among the testing laboratories and to evaluate 

individual laboratory performance. 

During 2014, PDP laboratories received two 

multiresidue fruit and vegetable PT rounds (grapes 

and green beans), each consisting of three test 

samples. The grape samples were fortified with a 

total of 10 different pesticides with buprofezin spiked 

on 2 different samples. The green bean samples were 

fortified with a total of 10 different compounds with 

trifloxystrobin spiked on 2 different samples at the 

same level to evaluate within and between laboratory 

variability.

Onsite Reviews: In addition to the onsite assessments 

performed by A2LA that are required to maintain 

ISO 17025 accreditation, MPD staff chemists 

perform onsite reviews of laboratory operations 

to determine compliance specifically with PDP 

SOPs. Improvements in sampling, chain-ofcustody, laboratory, recordkeeping, and electronic 

data transmission procedures are made as a result of 

onsite reviews.

IV. Database Management

 

PDP maintains an electronic database at the MPD 

in Washington, D.C., that serves as a central data 

repository. The data captured and stored in the PDP 

database include sample collection and product 

information, residue findings, and process control 

recoveries for each sample analyzed, in addition to 

QA/QC fortified recoveries for each set of samples. 

Each calendar-year survey is stored in a separate 

database structure, which allows easier administration 

and data reporting. The PDP data path is illustrated 

in Figure 5.

♦ Electronic Data Path

 

PDP utilizes the Remote Data Entry (RDE) system, 

which is a customized software application that 

allows participating State and Federal laboratories 

to enter and transmit data electronically. The RDE 

system is centralized with all user interface software 

and database files residing in Washington, D.C. 

The laboratory users need only a Web browser to 

interface with the RDE system. Access is controlled 

through separate user login/password accounts and 

user access rights for the various system functions 

based on position requirements. The RDE system 

utilizes Secure Sockets Layer technology to encrypt 

all data passed between users’ computers and the 

central Web server. 

A separate Windows®-based system allows sample 

collectors to capture the standardized Sample 
Pesticide Data Program—Annual Summary, Calendar Year 2014

17

- Collection in 10 States

- Samples taken close to consumer consumption

- Standardized sample information forms

- Data entry on tablet/laptop computers

- Chemists review data on-screen

- Upload data to central database

- 7 State laboratories, 1 Federal laboratory

- Fruit and vegetable samples prepared for

 consumption

- Detect residues at low levels

- Pesticide residue data generated

- Multi-tiered quality assurance data review

 process

- Web-based data entry software

- Import data from other systems

- Access controlled by user login

- Extensive data cross-checks

- Data reconciliation

- Standard & ad hoc reporting

- Annual Summary

- Custom data sets

YEAR-END REVIEW

INTERNET

SAMPLE COLLECTION DATA REVIEW AT HQ

LABORATORY ANALYSIS

LABORATORY REMOTE DATA 

ENTRY (RDE)

DATA REPORTING

Figure 5. Pesticide Data Program (PDP) Data Pathway. An illustration of PDP data path from sample 

collection through laboratory analysis and reporting.

INTERNET
Pesticide Data Program—Annual Summary, Calendar Year 2014

18

Information Form (SIF) electronically on laptop 

or tablet computers. The e-SIF system generates 

formatted text files containing sample information 

that are e-mailed to PDP headquarters and then 

imported into the Web-based RDE system.

The RDE data entry screens have extensive editing 

functions and cross-checks built into the software 

to ensure valid values are entered for all critical 

data elements. This task is made easier by the 

practice of capturing and storing standardized 

codes for all critical alphanumeric data elements 

rather than their complete names, meanings, or 

descriptions. This coding scheme allows for faster 

and more accurate data entry, saves disk storage 

space, and allows the user to perform ad-hoc 

queries (data searches) on the database easily. The 

data entry screens also perform automatic edits on 

numeric fields, dates, and other character fields to 

ensure entries are within prescribed boundaries. 

At PDP headquarters, the RDE system allows staff 

chemists to review the data online and then to mark 

the data as ready-for-upload to the central PDP 

database. A separate upload application converts 

and passes the data to the PDP database, which 

is maintained using Microsoft® Access and SQL 

Server database tools. Access to the central PDP 

database is limited to MPD personnel only and is 

controlled through password protection and user 

access rights.

♦ Data Reporting 

The MPD staff frequently receives requests for 

data from Government agencies and interested 

outside parties. Ad-hoc queries and custom reports 

are generated to fill such requests. An electronic 

library of data queries is maintained to generate 

standardized data summaries, including the data 

tables, charts, and appendices in this annual 

summary. Subsets of the PDP calendar year 

databases are made available for download from 

the PDP website. The data files on the website 

are delimited text files that contain a portion of 

the sampling data, all reported residue findings, 

and reference lists that can be used to interpret 

the standardized codes used in the PDP data. The 

data files can be imported into defined database 

structures and manipulated using common 

database management software packages.

V. Sample Results and Discussion

♦ Overview

In 2014, PDP conducted surveys on a variety of foods 

including fresh and processed fruit and vegetables, 

oats, rice, infant formula, and salmon. Of the total 

10,619 samples collected and analyzed; 8,582 were 

fresh and processed fruit and vegetable commodities, 

314 were oat samples, 314 were rice samples, 1,055 

were infant formula samples, and 354 were salmon 

samples. Over 41 percent of the samples tested 

had no detectable pesticide residue, and over 99 

percent of the samples tested had residues below the 

tolerances established by the EPA. 

Appendix B tabulates the distribution of residues in 

fruit and vegetables for the complete 2014 data set. 

Information included in this appendix are: number 

of samples analyzed for a particular compound, 

number and percent of samples with detections, 

range of concentrations detected, range of analytical 

LODs, and EPA tolerance levels. Appendices C, D, 

E, and F provide the distribution of residues for oats, 

rice, infant formula, and salmon, respectively. 

PDP laboratories tested foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in 

the environment, particularly in soil, can be taken 

up by plants. Appendix G tabulates the results for 

environmental contaminants across all commodities. 

Environmental contaminants are consolidated into 

a single appendix because they have no registered 

uses and are not applied to crops in the U.S. These 

compounds are subject to FDA Action Levels (ALs), 

rather than tolerances. Because environmental 

contaminants continue to persist in the environment, 

they are practically unavoidable and may be present 

in food commodities at generally low levels. All 

individual sample data can be downloaded from the 

PDP Website at http://www.ams.usda.gov/pdp or 

obtained by contacting MPD.

For fresh and processed fruit and vegetables, oats, 

rice, infant formula, and salmon, 75.5 percent of all 

samples were produced in the United States, 22.9 

percent were imports, 0.7 percent were of mixed 

origin, and 0.9 percent were of unknown origin. 

Appendix H shows the distribution of sample origin 
Pesticide Data Program—Annual Summary, Calendar Year 2014

19

by State or country. Of all fresh and processed fruit 

and vegetables, oats, rice, infant formula, and salmon 

samples collected and analyzed, approximately 

31.5 percent (3,340 of 10,619) were grown, packed, 

and/or distributed in or from California. Appendix 

I includes a comparison of residues for selected 

commodities with a significant import component.

Food monitoring data, together with dietary 

consumption surveys, are used by EPA to estimate 

dietary exposure to pesticides to ensure the safety 

of existing pesticide uses. EPA uses all results 

reported by PDP, including sample results reported 

as below the LOD and those above the tolerance. 

PDP laboratories are required to establish LODs and 

report any instrumental response below the LOD as 

a non-detect. LODs are established experimentally 

for each pesticide/commodity pair and are reported 

with each data set. The number of non-detects can be 

used in conjunction with percent-crop-treated data 

to determine what proportion of these values may 

be counted as zero towards the dietary exposure.

♦ Import Versus Domestic Residue Comparisons 

Information about the origin of each PDP sample 

is recorded when the sample is collected. Figure 

3 illustrates the portion of the domestic and import 

component for each of the PDP fruit and vegetable 

commodities in 2014. The data generated by PDP 

reflect pesticide residues in foods, both domestic and 

imported products, available to the U.S. consumer. 

Many fresh and processed commodities are almost 

entirely of domestic origin, such as apples (99.4 

percent); canned green beans (99.2 percent); 

celery (95.5 percent); and frozen sweet corn (95.1 

percent) with only minor import (0.6 percent, 0.5 

percent, 3.8 percent, and 4.9 percent, respectively) 

and unknown origins (0 percent, 0.3 percent, 0.7 

percent and 0 percent, respectively). Some fresh 

fruit and vegetables are entirely imported such as 

bananas (100 percent). Other fresh commodities, 

such as blueberries and fresh green beans, are 

available from domestic growers part of the year 

and imported during the remaining months, as 

illustrated in Figure 4.

Comparisons of selected residues detected in 

imported versus domestic blueberries, nectarines, 

and peaches can be found in Appendix I. These 

sample sets were selected to compare data where 

residues are present in greater than 10 percent of 

the commodity and allow for the comparison of 

individual residues. These data also show that the 

residue profiles for domestic and imported crops are 

significantly different. 

The blueberry data in Appendix I illustrate that, 

in 2014, azoxystrobin, fenhexamid, and phosmet 

and its oxygen analog metabolite were detected 

more frequently in imported samples than in 

domestic samples. Azoxystrobin was detected in 

37.3 percent of the samples from Mexico, 25.7 

percent of the U.S. samples, and 1.1 percent of the 

Chilean samples. Fenhexamid was detected in 21.9 

percent of the Chilean samples, 10.7 percent of 

the Mexican samples, and 7.9 percent of the U.S. 

samples. Phosmet and its oxygen analog metabolite 

were detected in 50.8 percent and 34.8 percent of 

Chilean samples, respectively, and 23.7 percent 

and 13.2 percent of U.S. samples, respectively. 

No phosmet or its oxygen analog metabolite were 

detected in samples from Mexico. Acetamiprid, 

boscalid, fludioxonil, and pyraclostrobin also 

were detected more frequently in imported 

samples than in domestic samples. Malathion and 

tetrahydrophthalimide (THPI), a metabolite of the 

fungicide captan, were detected more frequently in 

domestic samples than in imports. Malathion was 

detected in 22.0 percent of U.S. samples and 10.7 

percent of samples from Mexico. No malathion was 

detected in Chilean samples. THPI was detected 

in 35.3 percent of U.S. samples, 20.4 percent of 

Chilean samples, and 12.5 percent of samples 

from Mexico. Cypermethrin and cyprodinil were 

detected with relatively equal frequency in U.S. 

and Mexican samples. Cyprodinil was detected less 

frequently in Chilean samples, and no cypermethrin 

was detected in samples from Chile.

The data for nectarines in Appendix I illustrate 

that, in 2014, acetamiprid, cyhalothrin (lambda), 

iprodione, pyrimethanil, spinosad, and tebuconazole 

were detected more frequently in imported samples 

than in domestic samples. For example, iprodione 

was detected in 97.5 percent of Chilean samples 

and 1.7 percent of U.S. samples, and tebuconazole 

was detected in 80.7 percent of samples from Chile 

and 2.5 percent of samples from the U.S. Boscalid, 

fludioxonil, propiconazole, and spinetoram were 
Pesticide Data Program—Annual Summary, Calendar Year 2014

20

detected more frequently in domestic samples than 

in imports. For example, fludioxonil was detected 

in 83.6 percent of the U.S. samples and in 17.3 

percent of Chilean samples while propiconazole 

was detected in 41.1 percent of samples from the 

U.S. and 18.3 percent of the samples from Chile. 

Indoxacarb and methoxyfenozide were detected 

with relatively equal frequency in both the U.S. and 

Chilean nectarines.

The peach data in Appendix I illustrate that in 

2014 acetamiprid, iprodione, pyrimethanil, and 

tebuconazole were detected more frequently in 

imported samples than in domestic samples. For 

example, iprodione was detected in 99.5 percent 

of the samples from Chile and 1.2 percent of the 

samples grown in the U.S., and tebuconazole was 

detected in 76.2 percent of Chilean samples and 

4.9 percent of U.S. samples. Boscalid, cyfluthrin, 

fenbuconazole, fludioxonil, propiconazole, and 

pyraclostrobin were detected more frequently in 

domestic samples than in imports. For example, 

fludioxonil was detected in 79.2 percent of U.S. 

samples and 24.0 percent of the samples from Chile. 

Chlorantraniliprole, cyhalothrin, methoxyfenozide, 

phosmet, and spirodiclofen were detected with 

relatively equal frequency in both the U.S. and 

Chilean peaches.

All pesticides detected were registered in the United 

States; however, the profiles of residue findings 

were markedly different in the U.S. samples versus 

samples from these exporting countries. The 

differences in residue detections between countries 

were likely due to the pesticides used in response 

to pest pressures based on differing environmental 

and climatic conditions as well as crop production 

and protection practices.

♦ Postharvest Applications

Pesticides can be applied before and after harvest 

depending on the crop and approved label use. 

PDP data capture both preharvest and postharvest 

uses because samples are collected at points when 

all pesticide applications have already occurred. 

Pesticides applied postharvest are used primarily 

as fungicides (e.g., azoxystrobin, imazalil, 

o-phenylphenol, and thiabendazole) and growth 

regulators/sprouting inhibitors (e.g., chlorpropham). 

Some detections reported in Appendix B most 

likely reflect postharvest applications to the raw 

agricultural commodity.

♦ Discussion of Results

There are many pesticides registered for use on the 

same crop; however, not all crops are sprayed and 

not all available pesticides are used at the same time 

or location. Over 41 percent of the samples tested 

had no detectable pesticide residue, and over 99 

percent of the samples tested had residues below 

the tolerances established by the EPA. Pesticide 

use is primarily dictated by local pest pressures 

and environmental conditions conducive to growth 

of pest populations, as well as the planting of 

susceptible varieties. These differences are captured 

by PDP data, which reflect actual residues present 

in food grown in various regions of the U.S. and 

overseas. Thus, in evaluating consumer exposure to 

pesticides through the diet, EPA uses all available 

information provided by registrants, PDP, and others 

to verify that tolerances meet the safety standards set 

by FQPA. The reporting of residues present at levels 

below the established tolerance serves to ensure and 

verify the safety of the Nation’s food supply.

Food commodities with pesticides detected in at 

least five percent of samples tested are shown in 

Appendix J. The data shown include the range and 

mean of values detected and U.S. EPA tolerance 

references for each pair. 

By virtue of the MRMs employed, PDP provides 

novel data that can be used by EPA to evaluate 

exposure to multiple residues from the same 

commodity. The data are crucial for assessments 

that consider cumulative exposure to pesticides 

determined to have common mechanisms of toxicity. 

The distribution of multiple pesticides occurring in 

samples tested during 2014 is presented in Appendix 

K. These data indicate that 41.5 percent of all 

samples tested contained no detectable pesticides, 

14.8 percent contained 1 pesticide, and 43.7 percent 

contained more than 1 pesticide. Parent compounds 

and their metabolites are combined to report the 

number of “pesticides” rather than the number of 

“residues.” Environmental contaminants, listed in 

Appendix G, have been excluded from this count of 

pesticides. 
Pesticide Data Program—Annual Summary, Calendar Year 2014

21

One sample of strawberries contained residues 

of 17 pesticides. None of the residues found on 

the strawberry sample exceeded the established 

tolerance. Multiple residue detections can result 

from the application of more than one pesticide on a 

crop during a growing season; in addition, a number 

of other factors can contribute to multiple detections. 

For example, unintentional spray drift in the field, 

planting of crops in fields previously treated with the 

pesticide, and/or transfer of residues of postharvest 

fungicides or growth regulators applied to other 

commodities stored in the same storage facilities 

could all contribute to residue detections.

In most cases, samples analyzed by PDP are 

composites of 3 to 5 pounds of commodity from the 

same lot. Therefore, the estimated concentrations 

for multiple residue detections in these composite 

sample results may or may not reflect the number 

or levels of pesticides in a single serving item of a 

commodity.

♦ Special Projects

Oats: The NSL conducted testing on 314 oat samples. 

Appendix C shows that one residue representing 

one pesticide was detected in oats. Piperonyl 

butoxide was detected in one sample (0.3 percent). 

The residue detection was much lower than the 

established tolerance. 

Rice: The NSL conducted testing on 314 rice samples. 

Appendix D shows that five different residues, 

representing five pesticides, were detected in the 

rice samples. The most frequently detected residue 

was piperonyl butoxide, which was detected in 35 

samples (11.1 percent). Tricyclazole was detected 

in five samples (1.6 percent) and dinotefuran was 

detected in three samples (1.0 percent). MGK264 and tebuconazole were each detected in one 

sample (0.3 percent). All residue detections were 

much lower than the established tolerances for those 

compounds with established tolerances.

Infant Formula: The New York and California 

laboratories tested dairy-based and soy-based 

infant formula samples, respectively. Results for 

infant formula are contained in Appendix E. There 

were no residue detections in the 528 dairy-based 

formula samples. MGK-264, a pesticide formulation 

ingredient used to enhance the active ingredient, 

was detected in 7 (1.3 percent) of the 527 soybased samples. All detections of MGK-264 were 

much lower than the established tolerance. 

Salmon: The Washington State laboratory 

conducted testing for pesticide residues on 354 

salmon samples. Three residues representing three 

pesticides were detected in the salmon samples 

(Appendix F and Appendix G). Lufenuron was 

detected in one (0.3 percent) sample of salmon 

(Appendix F). The environmental contaminants 

DDT p,p’ and mirex were detected in the salmon 

samples. DDT p,p’ was detected in seven of the 

salmon samples (2.0 percent) and mirex was 

detected in one (0.3 percent) of the salmon samples 

(Appendix G). Both residue detections were lower 

than FDA’s established AL. 

♦ Environmental Contaminants

Environmental contaminants include pesticides 

whose uses have been canceled in the United 

States, but their residues persist in the 

environment, particularly in soil, where they may 

be taken up by plants. These data are also used 

to facilitate international trade. Residue results 

for environmental contaminants may be found in 

Appendix G.

DDT, DDD, and DDE: PDP screened samples for 

various metabolites of DDT including: DDT o,p’; 

DDT p,p’; DDD o,p’; DDD p,p’; DDE o,p’; and 

DDE p,p’. Use of DDT has been prohibited in 

the United States since 1972; however, due to its 

persistence in the environment, low-level residues 

of DDT and its DDD and DDE metabolites were 

detected in some commodities tested. DDE p,p’ 

was detected in carrots (24.7 percent), celery (10.6 

percent), summer squash (3.0 percent), frozen 

green beans (1.1 percent), and fresh green beans 

(0.1 percent). DDT p,p’ was detected in carrots 

(9.5 percent), summer squash (4.8 percent), salmon 

(2.0 percent), and celery (0.3 percent). DDT o,p’ 

was detected in carrots (4.2 percent) and summer 

squash (2.1 percent). DDD o,p’ and DDD p,p’ were 

detected in summer squash (0.4 and 0.2 percent, 

respectively) and DDE o,p’ was detected in carrots 

(0.1 percent). All residues detected were lower 

than established FDA ALs.
Pesticide Data Program—Annual Summary, Calendar Year 2014

22

Other Extraneous Pesticides: PDP screened samples 

for other environmental contaminants including: 

aldrin, which readily metabolizes to dieldrin; BHC 

(alpha/beta/delta/epsilon); chlordane (total, cis, 

trans) and its metabolite oxychlordane; dieldrin; 

endrin; heptachlor and its epoxide metabolite 

(total, cis); hexachlorobenzene (HCB); and mirex. 

HCB was used as a seed protectant until 1965 and, 

due to its persistence, remains in soil and grasses. 

In 1974, all aldrin and dieldrin uses were canceled 

in the United States and, in 1978, all heptachlor 

and mirex uses were canceled. In 1986, chlordane 

uses, except termiticide uses, were canceled. 

Despite these cancellations and because they 

persist in the environment, trace residues of BHC 

beta, chlordane, dieldrin, heptachlor epoxide, 

and mirex were detected in some of the tested 

commodities.

For example, dieldrin was detected in 3.1 percent 

of carrot samples and 3.0 percent of summer 

squash, while chlordane (cis) and chlordane (trans) 

were detected in 1.5 percent and 0.8 percent, 

respectively, in summer squash. Chlordane (total) 

was detected in 0.7 percent of carrot samples, 

while BHC (beta) was detected in 0.6 percent of 

carrots. Heptachlor epoxide (total) was detected 

in 1.3 percent of summer squash. Heptachlor 

epoxide (cis) was detected in 0.1 percent of carrot 

samples. Mirex was detected in 0.3 percent of 

salmon samples. No residues of aldrin, BHC 

alpha, BHC delta, BHC epsilon, endrin, heptachlor 

(parent), HCB, or oxychlordane were detected in 

any samples.

♦ Tolerance Violations

A tolerance is defined under Section 408 of the 

Federal Food, Drug, and Cosmetic Act as the 

maximum quantity of a pesticide residue allowable 

on a raw agricultural commodity. Tolerances are 

also applicable to processed foods. The FQPA of 

1996 amended the Federal Insecticide, Fungicide 

and Rodenticide Act to require EPA to periodically 

review each pesticide registration using the most 

currently available data. Timely pesticide data 

provided by PDP enable the EPA to refine risk 

estimates used in the pesticide reregistration 

process. 

A tolerance violation occurs when a residue is found 

that exceeds the tolerance level or when a certain 

residue is found for which there is no established 

tolerance. With the exception of meat, poultry, and 

egg products, for which USDA’s Food Safety and 

Inspection Service is responsible, FDA enforces 

tolerances for all imported foods and domestic 

foods that move through interstate commerce. 

Unlike enforcement programs, PDP emphasizes 

determination of residues at the lowest detectable 

levels rather than quick turn-around times. When 

PDP identifies samples with residues exceeding 

the tolerance or with residues for which there is no 

established tolerance, these detections are reported to 

FDA’s headquarters office. This notification is made 

in accordance with a Memorandum of Understanding 

between USDA and FDA for the purpose of 

identifying areas where closer surveillance may be 

needed. FDA assesses PDP apparent violation data 

for appropriateness for follow up under its regulatory 

pesticide program. Due to the time period required 

for completion of PDP analyses and data reporting, 

FDA follow up will usually be at a subsequent harvest 

or commodity availability period. In instances where 

a PDP finding is extraordinary and may pose a safety 

risk, FDA and EPA are immediately notified.

Residues exceeding the established tolerance or 

Action Level are noted with an “X” in Appendix 

B and Appendix G. Similarly, residues for which 

a tolerance is not established are noted with a “V” 

in Appendix B and Appendix D. The “X” and “V” 

annotations are followed by a number indicating 

the number of samples reported to FDA. The EPA 

tolerances cited in this summary and appendices 

apply to 2014 and not to the current year. There may 

be instances where tolerances may have been recently 

set or revoked that would have an effect on whether a 

residue is violative.

An established tolerance may apply to more than 

one residue because pesticides may break down into 

more than one metabolite or contain more than one 

isomer. For example, the tolerance for endosulfan 

combines residues of endosulfan I, endosulfan II, and 

endosulfan sulfate; and organophosphate tolerances 

may combine the parent compound and the sulfone 

and sulfoxide metabolites. Therefore, where 

applicable, the pesticide violations in Appendix L are 

combined residues of parent and any isomers and/or 
Pesticide Data Program—Annual Summary, Calendar Year 2014

23

metabolites to count the total number of samples 

with tolerance violations.

A total of 316 samples with 352 pesticides was 

reported to FDA as Presumptive Tolerance 

Violations. Pesticides exceeding the tolerance 

were detected in 0.36 percent (38 samples) of 

the total samples tested (10,619 samples). Of 

these 38 samples, 19 were imported (50 percent) 

and 19 were domestic (50 percent). The samples 

containing pesticides that exceeded established 

tolerances included: 1 sample of bananas, 2 samples 

of broccoli, 12 fresh green bean samples, 1 sample 

of nectarines, 11 samples of peaches, 5 samples 

of strawberries, 2 samples of summer squash, 3 

samples of tomatoes, and 1 sample of watermelon. 

Residues with no established tolerance were found 

in 2.6 percent (281samples) of the total samples 

tested (10,619 samples). Of these 281 samples, 138 

were domestic (49.1 percent), 140 were imported 

(49.8 percent), and 3 were of unknown origin (1.1 

percent). These samples included 258 fresh fruit and 

vegetable samples, 22 processed fruit/vegetable 

samples, and 1 rice sample. The 22 processed fruit/

vegetable samples were canned and frozen green 

beans, grape juice, and frozen cherries. There 

were 250 samples that contained 1 pesticide for 

which no tolerance was established and 29 samples 

with 2 pesticides for which no tolerance was 

established. One sample of celery and one sample 

of fresh green beans contained three pesticides for 

which no tolerance was established. Three of the 

281 samples also contained 1 pesticide each that 

exceeded an established tolerance. In most cases, 

these pesticides with no established tolerance 

were detected at very low levels. Some pesticide 

residues may have resulted from unintentional 

spray drift in the field, planting of crops in fields 

previously treated with the pesticide, or transfer 

of pesticide residues of postharvest fungicides or 

growth regulators applied to other commodities 

stored in the same storage facilities. The pesticide 

residue levels and commodities are listed in 

Appendix L.

♦♦♦♦♦♦
Appendix A

Commodity History

Appendix A identifi es commodities sampled by the Pesticide Data Program (PDP) through 

December 2015. Updates to this list are posted on the PDP Web site at www.ams.usda.gov/

pdp. 
Fresh Commodities

Commodity Start Date End Date

Apples 1 Sep-91 Dec-96

Apples (S-1) Jan-99 Dec-99

Apples (S-2) Jan-99 May-99

Apples Oct-00 Sep-02

Apples (T-1) Jan-03 Dec-03

Apples Jan-04 Dec-05

Apples Jan-09 Dec-10

Apples (B-1) Aug-12 Oct-12

Apples Oct-14 Ongoing

Asparagus Jan-02 Jun-03

Asparagus Jul-08 Jun-10

Avocados Jul-12 Dec-12

Bananas Sep-91 Sep-95

Bananas Jan-01 Dec-02

Bananas (TSP) Jul-03 Dec-03

Bananas Jan-06 Dec-07

Bananas Apr-12 Mar-14

Blueberries (cultivated) 2 Jan-07 Dec-08

Blueberries (cultivated) 2 Jan-14 Dec-14

Broccoli Oct-92 Dec-94

Broccoli Jan-01 Dec-02

Broccoli Oct-06 Sep-08

Broccoli Jan-13 Dec-14

Cabbage Jan-10 Dec-11

Cantaloupe Jul-98 Jun-00

Cantaloupe Oct-03 Sep-05

Cantaloupe Jan-10 Mar-10

Cantaloupe Oct-10 Jun-12

Carrots 1 Oct-92 Sep-96

Carrots Oct-00 Sep-02

Carrots Jan-06 Dec-07

Carrots Jan-13 Dec-14

Cauliflower Oct-04 Sep-06

Cauliflower Oct-11 Sep-13

Celery Feb-92 Mar-94

Celery Jan-01 Dec-02

Celery Jan-07 Dec-08

Celery Jan-13 Dec-14

Cherries 3 May-00 Aug-01

Cherries 2 May-07 Sep-07

Cherries Apr-14 Ongoing

Cilantro Oct-09 Sep-10

Cranberries Oct-06 Dec-06

Cucumbers Jan-99 Dec-00

Cucumbers Oct-02 Sep-04

Cucumbers Jan-09 Dec-10

Cucumbers Jul-15 Ongoing

Eggplant Jan-05 Dec-06

Grapefruit Aug-91 Dec-93

Grapefruit Jan-05 Dec-06

Grapefruit Oct-15 Ongoing

APPENDIX A. COMMODITY HISTORY

AS OF DECEMBER 2015

Appendix A. Page 1 of 7
Commodity Start Date End Date

Grapes 1 May-91 Dec-96

Grapes Jan-00 Dec-01

Grapes (TSP) Jul-03 Dec-03

Grapes Jan-04 Dec-05

Grapes Jan-09 Dec-10

Grapes Jan-15 Ongoing

Green Beans Feb-92 Dec-95

Green Beans Jan-00 Dec-01

Green Beans Apr-04 Mar-05

Green Beans Jan-07 Dec-08

Green Beans Jul-13 Ongoing

Green Onions (scallions) Oct-08 Sep-09

Greens (collard & kale) Oct-06 Sep-08

Hot Peppers Oct-10 Sep-11

Lettuce May-91 Dec-94

Lettuce Oct-99 Sep-01

Lettuce Jan-04 Dec-05

Lettuce Jan-10 Dec-11

Lettuce Jul-15 Ongoing

Lettuce, Organic Jan-09 Dec-09

Mangoes Apr-10 Sep-10

Mushrooms Oct-01 Sep-03

Mushrooms Oct-11 Sep-13

Nectarines 4 Jul-00 Sep-01

Nectarines Jan-07 Dec-08

Nectarines Jan-13 Ongoing

Onions Jan-02 Dec-03

Onions Oct-11 Sep-12

Oranges 1 Aug-91 Dec-96

Oranges Jan-00 Dec-01

Oranges Jan-04 Dec-05

Oranges Jan-09 Dec-10

Oranges Jan-15 Ongoing

Papaya Jul-11 Jun-12

Peaches Feb-92 Sep-96

Peaches (S-3) Jan-00 Sep-00

Peaches 5 Jan-01 Sep-02

Peaches (T-1) May-03 Sep-03

Peaches Oct-06 Sep-08

Peaches (B-1) Aug-12 Oct-12

Peaches Jul-13 Jun-15

Pears Jan-97 Jun-99

Pears (S-1) Jul-98 Jun-99

Pears Oct-03 Sep-05

Pears Jan-09 Dec-10

Pears Jan-15 Ongoing

Pears (B-1) Oct-12 Nov-12

Pineapples Jul-00 Jun-02

Plums 6 Jan-05 Dec-06

Plums Oct-11 Sep-13

Potatoes May-91 Dec-95

Potatoes (S-4) Dec-96 Dec-97

Potatoes Jul-00 Jun-02

Potatoes Jan-08 Dec-09

Potatoes Jan-15 Ongoing

Appendix A. Page 2 of 7
Commodity Start Date End Date

Raspberries 2 Jan-13 Dec-13

Snap Peas Jan-11 Dec-12

Spinach 1 Jan-95 Sep-97

Spinach Jul-02 Dec-03

Spinach 7 Jan-06 Sep-06

Spinach Jan-08 Dec-09

Spinach Jan-15 Ongoing

Strawberries 2 Jan-98 Sep-00

Strawberries Jan-04 Dec-05

Strawberries Jan-08 Dec-09

Strawberries Oct-14 Ongoing

Summer Squash Oct-06 Sep-08

Summer Squash Oct-12 Sep-14

Sweet Corn (on-the-cob) Oct-08 Sep-10

Sweet Corn (on-the-cob) Oct-14 Sep-15

Sweet Bell Peppers Jan-99 Dec-00

Sweet Bell Peppers Oct-02 Sep-04

Sweet Bell Peppers Jan-10 Mar-12

Sweet Potatoes 1 Jan-96 Jun-98

Sweet Potatoes Jan-03 Dec-04

Sweet Potatoes Oct-08 Sep-10

Tangerines Jan-11 Dec-12

Tomatoes 1 Jul-96 Jun-99

Tomatoes Jan-03 Dec-04

Tomatoes Jan-07 Dec-08

Tomatoes Oct-14 Ongoing

Tomatoes, Cherry/Grape Jan-11 Dec-12

Watermelon 8 Oct-05 Sep-06

Watermelon Apr-10 Sep-10

Watermelon Jul-14 Jun-15

Winter Squash 2 Jan-97 Jun-99

Winter Squash Jul-04 Jun-06

Winter Squash Oct-11 Mar-13

1

 Excludes sampling hiatus September - November 1996.

2

 Frozen collected when fresh unavailable.

3

 Sampling adjusted for market availability. Cherries were sampled for 2 years 

 (May-00 - Aug-01) for a total of 6 months.

4

 Sampling adjusted for market availability. Nectarines were sampled for 2 years 

 (Jul-00 - Sep-01) for a total of 6 months.

5

 Sampling adjusted for market availability. Peaches were sampled for 2 years

 (Jan-01 - Sep-02) for a total of 16 months.

6

 Dried plums (prunes) were collected when fresh plums were not available.

7

 Spinach ended earlier than planned due to the unavailability of product.

8

 Samples collected in California, Florida, and Texas only.

(B-1) Special project testing for bifenthrin in multi-residue screen.

(S-1) Special single serving project testing for organophosphates.

(S-2) Special single serving project testing for carbamates.

(S-3) Special single serving project testing for carbamate, organochlorine, 

 organophosphate, organonitrogen, and sulfur compounds.

(S-4) Special single serving project testing for aldicarb.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 3 of 7
Processed Commodities

Commodity Start Date End Date

Apple Juice 1 Jul-96 Dec-98

Apple Juice Jan-02 Dec-02

Apple Juice Jul-07 Jun-08

Apple Juice Jul-12 Jun-13

Applesauce Jul-02 Dec-02

Applesauce Jan-06 Dec-06

Asparagus, Canned Jul-03 Dec-03

Beans, Canned (4 varieties) Oct-08 Sep-10

Beets, Canned Jan-11 Dec-11

Blueberries (cultivated), Frozen 2 Jan-07 Dec-08

Blueberries (cultivated/wild), Frozen 2 Jan-14 Dec-14

Cherries, Frozen 2 Apr-14 Ongoing

Corn Syrup 3 Jan-98 Jun-99

Grape Juice Jan-98 Dec-99

Grape Juice Jan-08 Dec-08

Grape Juice Oct-13 Sep-14

Green Beans, Canned/Frozen 1 Jan-96 Jun-98

Green Beans, Canned Jan-03 Mar-04

Green Beans, Frozen Apr-05 Dec-05

Green Beans, Canned/Frozen Jan-14 Dec-14

Orange Juice Jan-97 Dec-98

Orange Juice Oct-04 Sep-06

Orange Juice Oct-10 Sep-11

Orange Juice Jan-12 Jun-12

Peaches, Canned Dec-96 Dec-97

Peaches, Canned Jan-03 Dec-04

Peaches, Canned (T-1) Jan-03 Mar-03

Peaches, Canned (T-1) Oct-03 Dec-03

Pear Juice, Concentrate/Puree Jul-02 Jun-03

Pears, Canned Jul-99 Jun-00

Peas, Canned/Frozen Apr-94 Jun-96

Peas, Canned/Frozen 4 Oct-01 Sep-03

Peas, Frozen Jan-06 Dec-06

Plums, Dried (Prunes) 5 Jan-05 Dec-06

Potatoes, Frozen Jan-06 Dec-07

Raisins Jul-06 Jun-07

Raspberries, Frozen 2 Jan-13 Dec-13

Spinach, Canned Oct-97 Dec-98

Spinach, Frozen Jan-99 Dec-99

Spinach, Canned Jan-04 Jun-04

Spinach, Canned/Frozen Jul-10 Jun-11

Strawberries, Frozen 2 Jan-98 Sep-00

Sweet Corn, Canned/Frozen Apr-94 Mar-96

Sweet Corn, Canned/Frozen 4 Oct-01 Sep-03

Sweet Corn, Frozen 2 Oct-08 Sep-10

Appendix A. Page 4 of 7
Commodity Start Date End Date

Sweet Corn, Frozen 2 Oct-14 Ongoing

Tomato Paste, Canned Jan-01 Jun-01

Tomato Paste, Canned Jan-09 Dec-09

Tomatoes, Canned Jul-99 Jun-00

Winter Squash, Frozen 2 Jan-97 Jun-99

Baby Food / Formula Products

Commodity Start Date End Date

Baby Food, Applesauce Jul-12 Jun-13

Baby Food, Carrots Jan-12 Dec-12

Baby Food, Green Beans Oct-10 Sep-11

Baby Food, Peaches Jan-12 Dec-12

Baby Food, Pears Oct-10 Sep-11

Baby Food, Peas Jul-12 Jun-13

Baby Food, Sweet Potatoes Oct-10 Sep-11

Infant Formula, Dairy-Based Oct-13 Sep-14

Infant Formula, Soy-Based Oct-13 Sep-14

1 Excludes sampling hiatus September - November 1996.

2 Frozen collected when fresh unavailable.

3 Excludes sampling hiatus January 1999.

4 Canned samples collected in first year and frozen samples in second year of testing.

5 Dried plums (prunes) were collected when fresh plums were not available.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 5 of 7
Grains

Commodity Start Date End Date

Barley Oct-01 Sep-03

Corn Oct-06 Sep-08

Oats Jul-99 Apr-00

Oats Jan-10 Jun-10

Oats Apr-14 Aug-14

Rice Oct-00 Sep-02

Rice1 Oct-08 Sep-09

Rice Apr-14 Aug-14

Soybeans Sep-96 Feb-98

Soybeans Oct-03 Sep-05

Soybeans Sep-10 Apr-11

Soybeans (S-1) Oct-05 Dec-05

Wheat Feb-95 Jan-98

Wheat Sep-04 Jun-06

Wheat Jul-12 Sep-12

Wheat Flour Jan-03 Dec-04

Wheat Flour (T-1) Jan-03 Dec-03

Nuts and Nut Products

Commodity Start Date End Date

Almonds Jul-07 Mar-08

Peanut Butter Jan-00 Dec-00

Peanut Butter (TSP) Jul-03 Dec-03

Peanut Butter Jan-06 Dec-06

Peanut Butter Apr-15 Aug-15

Dairy Products

Commodity Start Date End Date

Butter Jan-03 Dec-03

Butter Jan-12 Dec-13

Heavy Cream Jul-05 Dec-05

Heavy Cream Jan-07 Dec-07

Milk 2 Jan-96 Oct-98

Milk (TSP) Jul-03 Dec-03

Milk Jan-04 Dec-05

Milk Jan-11 Dec-11

Meat / Poultry / Pork Products

Commodity Type Start Date End Date

Poultry Young Chickens Apr-00 Mar-01

Poultry Young & Mature Chickens Jan-06 Dec-06

Beef Cows, Heifers, Steers Jun-01 Jul-02

Beef 3 Cows, Heifers, Steers Dec-08 May-09

Pork Gilt, Barrow Jan-05 Jun-05

Appendix A. Page 6 of 7
Fish Products

Commodity Type Start Date End Date

Fish 4 Catfish Apr-08 Jun-10

Fish Salmon Jul-13 Jun-14

Other Products

Commodity Start Date End Date

Eggs (TSP) Jul-03 Dec-03

Eggs Jul-10 Jun-11

Honey Oct-07 Sep-08

Drinking Water

States Start Date End Date

Finished Water Only (27 sites)

California, Colorado, Kansas, New York, Texas Mar-01 Dec-03

Raw Intake and Finished Water (70 sites) Jan-04 Apr-13

Alabama, Arizona, California, Florida, Georgia, Illinois, Indiana, Iowa, Kansas,

Kentucky, Louisiana, Maryland, Michigan, Minnesota, Missouri, Montana, New Jersey, 

New York, North Carolina, North Dakota, Ohio, Oregon, Pennsylvania, South Carolina, 

Tennessee, Texas, Virginia, Washington State, and Washington, D.C.

Bottled Water 

10 Participating States Jan-05 Dec-06

Groundwater 

1,495 Private Wells in 45 States plus Washington, DC Jan-07 Feb-13

16 Municipal Water Facilities in 13 States Mar-10 Feb-13

1

 Includes sampling hiatus May-July 2009.

2

 Excludes sampling hiatus September - November 1996.

3

 Survey ended 7 months early due to budgetary constraints. 4 Excludes sampling hiatus April-June 2009.

(S-1) Special survey for fungicides used to combat soybean rust.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 7 of 7
Appendix B

Distribution of Residues by Pesticide

in Fruit and Vegetables

Appendix B shows residue detections for all fruit and vegetable pesticide/commodity pairs 

tested, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerances for each pair. The EPA tolerances 

cited in this summary and appendices apply to 2014 and not to the current year. There 

may be instances where tolerances have been recently set, modifi ed, or revoked that 

would have an effect on whether a residue is violative or not.

In 2014, 8,582 fruit and vegetable samples were analyzed, of which 6,953 were fresh 

products and 1,629 were processed products.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by the U.S. Food and Drug Administration (FDA). Under the Food Quality 

Protection Act, responsibility for establishing tolerances in lieu of ALs has been transferred 

to EPA. In the interim, ALs are used.

The Pesticide Data Program reports tolerance violations to FDA as part of an interagency 

Memorandum of Understanding between the U.S. Department of Agriculture and FDA. 

Residues reported to FDA are shown in the “Pesticide/Commodity” column to the right 

of the commodity and are annotated as “X” (if the residue exceeded the established 

tolerance) or “V” (if the residue did not have a tolerance listed in the Code of Federal 

Regulations, Title 40, Part 180). In both cases, these annotations are followed by a 

number indicating the number of samples reported to FDA. 

Results for environmental contaminants across all commodities, including fruit and 

vegetables, have been consolidated in a separate appendix because they have no 

registered uses and are not applied to crops (see Appendix G). 
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

2,4,5-T (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.10 ^ NT

Blueberries, Frozen 5 0 0.10 ^ NT

Celery 348 0 0.10 ^ NT

Strawberries 176 0 0.10 ^ NT

Summer Squash 270 0 0.10 ^ NT

Sweet Corn, Fresh 78 0 0.10 ^ NT

Sweet Corn, Frozen 12 0 0.10 ^ NT

TOTAL 1,243 0

2,4-D (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.050 ^ 0.2

Blueberries, Frozen 5 0 0.050 ^ 0.2

Celery 348 0 0.050 ^ 0.4

Strawberries 176 0 0.050 ^ 0.05

Summer Squash 270 0 0.050 ^ 0.05

Sweet Corn, Fresh 78 0 0.050 ^ 0.05

Sweet Corn, Frozen 12 0 0.050 ^ 0.05

TOTAL 1,243 0

2,4-DB (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.10 ^ NT

Blueberries, Frozen 5 0 0.10 ^ NT

Celery 348 0 0.10 ^ NT

Strawberries 176 0 0.10 ^ NT

Summer Squash 270 0 0.10 ^ NT

Sweet Corn, Fresh 78 0 0.10 ^ NT

Sweet Corn, Frozen 12 0 0.10 ^ NT

TOTAL 1,243 0

Abamectin (insecticide, acaricide)

Blueberries, Cultivated, Fresh 354 0 0.020 ^ 0.01

Blueberries, Frozen 5 0 0.020 ^ 0.01

Celery 348 0 0.020 ^ 0.10

Strawberries 176 1 0.6 0.042 ^ 0.020 ^ 0.05

Summer Squash 270 0 0.020 ^ 0.005

Sweet Corn, Fresh 78 0 0.020 ^ 0.01

Sweet Corn, Frozen 12 0 0.020 ^ 0.01

TOTAL 1,243 1

Acephate (insecticide)

Apples 177 0 0.030 ^ 0.02

Bananas 179 0 0.075 ^ 0.02

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.15 0.02

Blueberries, Frozen 19 0 0.010 - 0.15 0.02

Broccoli 652 0 0.050 ^ 0.02

Carrots 708 0 0.050 ^ 0.02

Celery 708 194 27.4 0.005 - 0.64 0.002 - 0.010 10

Cherries, Fresh 228 0 0.15 ^ 0.02

Cherries, Frozen 282 0 0.15 ^ 0.02

Grape Juice 531 0 0.030 ^ 0.02

APPENDIX B. DISTRIBUTION OF RESIDUES BY PESTICIDE IN FRUIT AND VEGETABLES

Appendix B. Page 1 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Canned 378 40 10.6 0.003 - 0.028 0.002 ^ 3.0

Green Beans, Fresh (X-1) 757 135 17.8 0.031 - 3.4 0.030 ^ 3.0

Green Beans, Frozen 378 82 21.7 0.003 - 0.30 0.002 ^ 3.0

Nectarines 681 0 0.040 ^ 0.02

Peaches 707 0 0.010 ^ 0.02

Strawberries 176 0 0.005 ^ 0.02

Summer Squash (X-1) 531 1 0.2 0.19 ^ 0.010 - 0.030 0.02

Sweet Corn, Fresh 134 0 0.005 - 0.030 0.02

Sweet Corn, Frozen 41 0 0.005 - 0.030 0.02

Tomatoes 177 0 0.002 ^ 0.02

Watermelon (X-1) 390 1 0.3 0.084 ^ 0.030 ^ 0.02

TOTAL 8,522 453

Acequinocyl (acaricide) 

Green Beans, Fresh 473 0 0.20 ^ 0.25

Strawberries (X-5) 1176 20 11.4 0.014 - 1.6 0.005 ^ 0.50

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 739 20

Acetamiprid (insecticide) 

Apples 177 58 32.8 0.002 - 0.13 0.002 ^ 1.0

Bananas 179 0 0.002 ^ 0.01

Blueberries, Cultivated, Fresh 688 74 10.8 0.002 - 0.19 0.002 - 0.003 1.6

Blueberries, Frozen 19 3 15.8 0.002 - 0.072 0.002 - 0.003 1.6

Broccoli 712 1 0.1 0.094 ^ 0.010 ^ 1.20

Carrots 708 0 0.005 ^ 0.01

Celery 708 80 11.3 0.002 - 0.022 0.001 - 0.003 3.00

Cherries, Fresh 228 55 24.1 0.002 - 0.23 0.002 ^ 1.20

Cherries, Frozen 282 203 72 0.002 - 0.11 0.002 ^ 1.20

Grape Juice 501 0 0.003 ^ 0.35

Green Beans, Canned 378 0 0.001 ^ 0.60

Green Beans, Fresh 757 10 1.3 0.002 - 0.070 0.002 ^ 0.60

Green Beans, Frozen 378 0 0.001 ^ 0.60

Nectarines 681 97 14.2 0.017 - 0.096 0.010 ^ 1.20

Peaches 707 77 10.9 0.010 - 0.11 0.010 ^ 1.20

Strawberries 176 52 29.5 0.003 - 0.31 0.003 ^ 0.60

Summer Squash 531 8 1.5 0.003 - 0.032 0.003 - 0.020 0.50

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.01

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.01

Tomatoes 177 15 8.5 0.002 - 0.044 0.001 ^ 0.20

Watermelon 390 3 0.8 0.002 ^ 0.002 ^ 0.50

TOTAL 8,552 736

Acetochlor (herbicide) 

Apples 177 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Fresh 757 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Appendix B. Page 2 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 134 0 0.005 ^ 0.05

Sweet Corn, Frozen 41 0 0.005 ^ 0.05

Watermelon 390 0 0.005 ^ NT

TOTAL 3,183 0

Acibenzolar S methyl (plant activator) 

Apples 177 0 0.020 ^ 0.05

Celery 360 0 0.004 - 0.012 0.25

Green Beans, Canned 378 0 0.004 - 0.012 NT

Green Beans, Fresh 757 0 0.020 ^ NT

Green Beans, Frozen 357 0 0.004 - 0.012 NT

Summer Squash 261 0 0.10 ^ 2.0

Sweet Corn, Fresh 56 0 0.005 ^ NT

Sweet Corn, Frozen 29 0 0.005 ^ NT

Tomatoes 177 0 0.004 ^ 1.0

Watermelon 390 0 0.020 ^ 2.0

TOTAL 2,942 0

Acifluorfen (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.050 ^ NT

Blueberries, Frozen 5 0 0.050 ^ NT

Celery 348 0 0.050 ^ NT

Strawberries 176 0 0.050 ^ 0.05

Summer Squash 270 0 0.050 ^ NT

Sweet Corn, Fresh 78 0 0.050 ^ NT

Sweet Corn, Frozen 12 0 0.050 ^ NT

TOTAL 1,243 0

Acrinathrin (insecticide, acaricide)

Apples 177 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 1,098 0

Alachlor (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.020 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.020 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.020 0.05

Tomatoes 177 0 0.002 ^ NT

TOTAL 3,378 0

Aldicarb (insecticide) 

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Broccoli 712 0 0.010 ^ NT

Appendix B. Page 3 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 708 0 0.003 - 0.010 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Nectarines 681 0 0.003 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.001 - 0.003 NT

TOTAL 5,673 0

Aldicarb sulfone (metabolite of Aldicarb)

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.025 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.025 NT

Blueberries, Frozen 19 0 0.010 - 0.025 NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.003 - 0.010 NT

Cherries, Fresh 228 0 0.025 ^ NT

Cherries, Frozen 282 0 0.025 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.010 ^ NT

Green Beans, Frozen 378 0 0.010 ^ NT

Nectarines 681 0 0.050 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 6,771 0

Aldicarb sulfoxide (metabolite of Aldicarb)

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.050 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.051 NT

Blueberries, Frozen 19 0 0.010 - 0.051 NT

Broccoli 674 0 0.010 ^ NT

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 228 0 0.051 ^ NT

Cherries, Frozen 282 0 0.051 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.006 ^ NT

Green Beans, Frozen 378 0 0.006 ^ NT

Nectarines 681 0 0.050 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Appendix B. Page 4 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 6,733 0

Allethrin (insecticide) 

Bananas 179 0 0.080 ^ EX

Blueberries, Cultivated, Fresh 688 0 0.020 - 0.080 EX

Blueberries, Frozen 19 0 0.020 - 0.080 EX

Broccoli 712 0 0.020 ^ EX

Carrots 708 0 0.016 ^ EX

Celery 348 0 0.020 ^ EX

Cherries, Fresh 228 0 0.080 ^ EX

Cherries, Frozen 282 0 0.080 ^ EX

Green Beans, Fresh 757 0 0.050 ^ EX

Nectarines 681 0 0.016 ^ EX

Peaches 707 0 0.020 ^ EX

Strawberries 176 0 0.010 ^ EX

Summer Squash 531 0 0.020 - 0.10 EX

Sweet Corn, Fresh 134 0 0.010 - 0.050 EX

Sweet Corn, Frozen 41 0 0.010 - 0.050 EX

TOTAL 6,191 0

Ametoctradin (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 1 0.3 0.003 ^ 0.003 ^ 40.0

Green Beans, Fresh 757 0 0.001 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 7 1.3 0.004 - 0.052 0.003 - 0.005 3.0

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

Tomatoes 177 0 0.001 ^ 1.5

TOTAL 2,523 8

Ametryn (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ 0.25

Sweet Corn, Frozen 41 0 0.005 ^ 0.25

TOTAL 2,035 0

Atrazine (herbicide) 

Apples 177 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 708 3 0.4 0.002 ^ 0.001 - 0.005 0.25

Grape Juice 442 0 0.002 ^ NT

Appendix B. Page 5 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.20

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.20

Tomatoes 177 0 0.001 ^ NT

Watermelon 296 0 0.002 ^ NT

TOTAL 4,955 3

Avermectin (insecticide, acaricide)

Carrots 708 0 0.030 ^ 0.01

Nectarines 681 0 0.050 ^ 0.09

TOTAL 1,389 0

Azinphos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Azinphos methyl (insecticide) 

Apples 177 0 0.010 ^ 1.5

Bananas 179 0 0.004 ^ NT

Blueberries, Cultivated, Fresh 688 11 1.6 0.006 - 0.26 0.004 - 0.005 5.0

Blueberries, Frozen 19 0 0.004 - 0.005 5.0

Carrots 708 0 0.015 ^ NT

Celery 708 0 0.005 - 0.012 NT

Cherries, Fresh 228 0 0.004 ^ 2.0

Cherries, Frozen 282 3 1.1 0.006 - 0.012 0.004 ^ 2.0

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.012 ^ NT

Green Beans, Fresh 757 0 0.020 ^ NT

Green Beans, Frozen 378 0 0.012 ^ NT

Nectarines 681 5 0.7 0.008 - 0.020 0.005 ^ 2.0

Peaches 707 4 0.6 0.026 - 0.037 0.020 ^ 2.0

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.090 NT

Sweet Corn, Fresh 134 0 0.005 - 0.020 NT

Sweet Corn, Frozen 41 0 0.005 - 0.020 NT

Tomatoes 177 0 0.012 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 7,870 23

Azinphos methyl oxygen analog (metabolite of Azinphos methyl)

Apples 177 0 0.010 ^ 1.5

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 3 0.4 0.003 - 0.004 0.003 - 0.010 5.0

Appendix B. Page 6 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 19 0 0.003 - 0.010 5.0

Carrots 708 0 0.008 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.003 ^ 2.0

Cherries, Frozen 282 1 0.4 0.003 ^ 0.003 ^ 2.0

Grape Juice 501 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.003 ^ NT

Nectarines 681 0 0.001 - 0.003 2.0

Strawberries 176 0 0.010 ^ NT

Summer Squash 531 0 0.010 - 0.015 NT

Sweet Corn, Fresh 134 0 0.003 - 0.010 NT

Sweet Corn, Frozen 41 0 0.003 - 0.010 NT

Watermelon 390 0 0.010 ^ NT

TOTAL 5,840 4

Azoxystrobin (fungicide) 

Apples 177 0 0.002 ^ NT

Bananas 179 27 15.1 0.005 - 0.028 0.005 ^ 2.0

Blueberries, Cultivated, Fresh 688 123 17.9 0.003 - 1.0 0.003 - 0.005 5.0

Blueberries, Frozen 19 2 10.5 0.013 - 0.055 0.003 - 0.005 5.0

Broccoli 712 52 7.3 0.002 - 0.65 0.002 ^ 3.0

Carrots 707 98 13.9 0.003 - 0.044 0.002 ^ 0.5

Celery 708 68 9.6 0.002 - 0.57 0.001 - 0.003 30.0

Cherries, Fresh 228 4 1.8 0.038 - 0.10 0.005 ^ 1.5

Cherries, Frozen 282 20 7.1 0.006 - 0.31 0.005 ^ 1.5

Grape Juice 530 0 0.003 ^ 2.0

Green Beans, Canned 378 4 1.1 0.002 - 0.007 0.001 ^ 3.0

Green Beans, Fresh 757 217 28.7 0.001 - 0.28 0.001 ^ 3.0

Green Beans, Frozen 378 44 11.6 0.002 - 0.016 0.001 ^ 3.0

Nectarines 681 27 4 0.002 - 0.025 0.001 ^ 1.5

Peaches 707 20 2.8 0.002 - 0.28 0.002 ^ 1.5

Strawberries 176 34 19.3 0.003 - 0.37 0.003 ^ 10.0

Summer Squash 531 2 0.4 0.004 - 0.012 0.003 - 0.005 0.3

Sweet Corn, Fresh 134 0 0.003 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.003 - 0.010 0.05

Tomatoes 177 36 20.3 0.002 - 0.023 0.001 - 0.003 0.2

Watermelon 390 0 0.002 ^ 0.3

TOTAL 8,580 778

Benalaxyl (fungicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Benazolin (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.050 ^ NT

Blueberries, Frozen 5 0 0.050 ^ NT

Celery 348 0 0.050 ^ NT

Strawberries 176 0 0.050 ^ NT

Summer Squash 270 0 0.050 ^ NT

Appendix B. Page 7 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.050 ^ NT

Sweet Corn, Frozen 12 0 0.050 ^ NT

TOTAL 1,243 0

Bendiocarb (insecticide) 

Apples 177 0 0.003 ^ SU

Bananas 179 0 0.009 ^ SU

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 SU

Blueberries, Frozen 19 0 0.005 - 0.010 SU

Broccoli 712 0 0.005 ^ SU

Carrots 708 0 0.002 ^ SU

Celery 708 0 0.001 - 0.015 SU

Cherries, Fresh 228 0 0.010 ^ SU

Cherries, Frozen 282 0 0.010 ^ SU

Grape Juice 531 0 0.003 ^ SU

Green Beans, Canned 378 0 0.001 ^ SU

Green Beans, Fresh 757 0 0.015 ^ SU

Green Beans, Frozen 378 0 0.001 ^ SU

Nectarines 681 0 0.001 ^ SU

Peaches 707 0 0.005 ^ SU

Strawberries 176 0 0.003 ^ SU

Summer Squash 531 0 0.005 - 0.015 SU

Sweet Corn, Fresh 134 0 0.003 - 0.015 SU

Sweet Corn, Frozen 41 0 0.003 - 0.015 SU

Tomatoes 177 0 0.001 ^ SU

Watermelon 390 0 0.003 ^ SU

TOTAL 8,582 0

Benfluralin (herbicide) 

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Grape Juice 531 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 2,341 0

Benoxacor (herbicide safener) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.012 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.012 0.01

Blueberries, Frozen 19 0 0.010 - 0.012 0.01

Carrots 708 0 0.015 ^ 0.01

Celery 708 0 0.001 - 0.010 0.01

Cherries, Fresh 228 0 0.012 ^ NT

Cherries, Frozen 282 0 0.012 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.01

Green Beans, Fresh 757 0 0.020 ^ 0.01

Appendix B. Page 8 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Frozen 378 0 0.001 ^ 0.01

Nectarines 681 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.010 - 0.020 0.01

Sweet Corn, Frozen 41 0 0.010 - 0.020 0.01

Tomatoes 177 0 0.001 ^ 0.01

Watermelon 390 0 0.010 ^ 0.01

TOTAL 6,902 0

Bensulide (herbicide) 

Apples 177 0 0.004 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 - 0.010 NT

Blueberries, Frozen 5 0 0.005 - 0.010 NT

Carrots 708 0 0.003 ^ 0.10

Celery 348 1 0.3 0.008 ^ 0.005 ^ 0.15

Grape Juice 531 0 0.004 ^ NT

Green Beans, Fresh 757 0 0.015 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 ^ 0.15

Sweet Corn, Fresh 134 0 0.005 - 0.015 NT

Sweet Corn, Frozen 41 0 0.005 - 0.015 NT

Watermelon 390 0 0.004 ^ 0.15

TOTAL 4,152 1

Bensulide oxygen analog (metabolite of Bensulide)

Apples 177 0 0.002 ^ NT

Carrots 708 0 0.002 ^ 0.10

Grape Juice 531 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Summer Squash 261 0 0.005 ^ 0.15

Sweet Corn, Fresh 56 0 0.002 ^ NT

Sweet Corn, Frozen 29 0 0.002 ^ NT

Watermelon 390 0 0.002 ^ 0.15

TOTAL 2,909 0

Bentazon (herbicide) 

Bananas 179 0 0.015 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.030 NT

Blueberries, Frozen 19 0 0.003 - 0.030 NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.030 ^ NT

Cherries, Frozen 282 0 0.030 ^ NT

Green Beans, Fresh 757 0 0.10 ^ 0.5

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.10 0.05

Sweet Corn, Frozen 41 0 0.003 - 0.10 0.05

TOTAL 3,122 0

Benthiavalicarb isopropyl (fungicide) 

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.005 ^ NT

Appendix B. Page 9 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 14 0 0.005 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

TOTAL 1,037 0

Bifenazate (acaricide) 

Blueberries, Cultivated, Fresh 334 0 0.005 ^ 1.5

Blueberries, Frozen 14 0 0.005 ^ 1.5

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.005 ^ 2.5

Cherries, Frozen 282 0 0.005 ^ 2.5

Strawberries 176 34 19.3 0.003 - 1.5 0.003 ^ 1.5

Summer Squash 270 0 0.005 ^ 0.75

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,742 34

Bifenox (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Bifenthrin (insecticide) 

Apples 177 3 1.7 0.010 - 0.20 0.002 ^ 0.5

Bananas 179 0 0.008 ^ 0.1

Blueberries, Cultivated, Fresh 688 53 7.7 0.013 - 0.77 0.008 - 0.010 1.8

Blueberries, Frozen 19 2 10.5 0.014 - 0.034 0.008 - 0.010 1.8

Broccoli 712 5 0.7 0.011 - 0.066 0.005 ^ 0.6

Carrots 708 3 0.4 0.002 - 0.003 0.001 ^ 0.10

Celery 708 34 4.8 0.003 - 0.080 0.002 - 0.010 3.0

Cherries, Fresh 228 0 0.008 ^ 0.05

Cherries, Frozen 282 0 0.008 ^ 0.05

Grape Juice 531 0 0.005 ^ 0.2

Green Beans, Canned 378 197 52.1 0.003 - 0.056 0.002 ^ 0.6

Green Beans, Fresh 757 52 6.9 0.040 - 0.36 0.040 ^ 0.6

Green Beans, Frozen 378 166 43.9 0.003 - 0.064 0.002 ^ 0.6

Nectarines 681 10 1.5 0.002 - 0.13 0.001 ^ 0.5

Peaches 707 1 0.1 0.11 ^ 0.005 ^ 0.5

Strawberries 176 73 41.5 0.010 - 0.21 0.010 ^ 3.0

Summer Squash 531 5 0.9 0.013 - 0.046 0.010 - 0.020 0.4

Sweet Corn, Fresh 134 0 0.010 - 0.040 0.05

Sweet Corn, Frozen 41 0 0.010 - 0.040 0.05

Tomatoes 177 30 16.9 0.002 - 0.024 0.001 ^ 0.15

Watermelon 390 31 7.9 0.002 - 0.009 0.002 - 0.005 0.4

TOTAL 8,582 665

Appendix B. Page 10 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bitertanol (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.040 ^ NT

Blueberries, Frozen 5 0 0.040 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.040 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.040 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 2,662 0

Boscalid (fungicide) 

Apples 177 35 19.8 0.003 - 0.14 0.003 ^ 3.0

Bananas 179 0 0.013 ^ 0.40

Blueberries, Cultivated, Fresh 688 264 38.4 0.005 - 1.7 0.005 - 0.013 13.0

Blueberries, Frozen 19 15 78.9 0.006 - 1.0 0.005 - 0.013 13.0

Broccoli 712 13 1.8 0.010 - 0.088 0.010 ^ 3.0

Carrots 708 149 21 0.025 - 0.15 0.015 ^ 1.0

Celery 708 96 13.6 0.005 - 0.17 0.005 - 0.006 45

Cherries, Fresh 228 131 57.5 0.013 - 0.17 0.013 ^ 3.5

Cherries, Frozen 282 69 24.5 0.013 - 0.18 0.013 ^ 3.5

Grape Juice 531 11 2.1 0.003 - 0.084 0.003 ^ 5.0

Green Beans, Canned 378 10 2.6 0.010 ^ 0.006 - 0.020 1.6

Green Beans, Fresh 757 29 3.8 0.005 - 0.19 0.005 ^ 1.6

Green Beans, Frozen 378 28 7.4 0.010 - 0.13 0.006 - 0.040 1.6

Nectarines 679 91 13.4 0.002 - 0.21 0.001 - 0.003 3.5

Peaches 707 112 15.8 0.011 - 0.46 0.010 ^ 3.5

Strawberries 176 107 60.8 0.006 - 0.68 0.005 ^ 4.5

Summer Squash 531 5 0.9 0.005 - 0.025 0.005 - 0.015 1.6

Sweet Corn, Fresh 134 0 0.005 ^ 0.20

Sweet Corn, Frozen 41 0 0.005 ^ 0.20

Tomatoes 177 13 7.3 0.021 - 0.079 0.020 ^ 3.0

Watermelon 390 5 1.3 0.004 - 0.010 0.003 ^ 1.6

TOTAL 8,580 1,183

Bromacil (herbicide) 

Apples 177 0 0.003 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.003 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 48 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Watermelon 390 0 0.003 ^ NT

TOTAL 3,348 0

Appendix B. Page 11 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bromopropylate (acaricide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.010 ^ NT

Nectarines 681 0 0.001 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 3,343 0

Bromuconazole (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Bupirimate (fungicide) 

Apples 177 0 0.001 ^ NT

Bananas 179 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.040 NT

Blueberries, Frozen 19 0 0.002 - 0.040 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.040 ^ NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

Grape Juice 531 0 0.001 ^ NT

Nectarines 681 0 0.003 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.040 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 5,478 0

Buprofezin (insecticide) 

Apples 177 2 1.1 0.004 ^ 0.001 - 0.002 3.0

Bananas 179 39 21.8 0.001 - 0.055 0.001 ^ 0.20

Blueberries, Cultivated, Fresh 688 1 0.1 0.001 ^ 0.001 - 0.005 2.5

Blueberries, Frozen 19 0 0.001 - 0.005 2.5

Broccoli 712 5 0.7 0.010 - 0.057 0.010 ^ 12.0

Celery 708 26 3.7 0.002 - 0.040 0.001 - 0.005 35

Cherries, Fresh 228 33 14.5 0.001 - 0.077 0.001 ^ 1.9

Cherries, Frozen 282 57 20.2 0.001 - 0.035 0.001 ^ 1.9

Grape Juice 531 0 0.001 ^ 2.5

Green Beans, Canned 378 0 0.001 ^ 0.02

Appendix B. Page 12 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Fresh 757 6 0.8 0.001 - 0.009 0.001 ^ 0.02

Green Beans, Frozen 378 0 0.001 ^ 0.02

Nectarines 681 41 6 0.002 - 0.015 0.001 ^ 9.0

Peaches 707 9 1.3 0.013 - 0.090 0.010 ^ 9.0

Strawberries 176 3 1.7 0.007 - 1.1 0.003 ^ 2.5

Summer Squash 531 6 1.1 0.006 - 0.025 0.005 ^ 0.50

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

Tomatoes 177 21 11.9 0.002 - 0.030 0.001 ^ 2.0

Watermelon 390 0 0.001 ^ 0.50

TOTAL 7,874 249

Butocarboxim (insecticide, acaricide)

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.010 ^ NT

Blueberries, Frozen 14 0 0.010 ^ NT

Broccoli 712 0 0.010 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Nectarines 681 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

TOTAL 3,137 0

Butocarboxim sulfone (metabolite of Butocarboxim)

Bananas 179 0 0.021 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.011 ^ NT

Blueberries, Frozen 14 0 0.011 ^ NT

Cherries, Fresh 228 0 0.011 ^ NT

Cherries, Frozen 282 0 0.011 ^ NT

TOTAL 1,037 0

Butocarboxim sulfoxide (metabolite of Butocarboxim)

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.006 ^ NT

Blueberries, Frozen 14 0 0.006 ^ NT

Cherries, Fresh 228 0 0.006 ^ NT

Cherries, Frozen 282 0 0.006 ^ NT

Nectarines 681 0 0.030 ^ NT

TOTAL 1,718 0

Butylate (herbicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ 0.1

Sweet Corn, Frozen 12 0 0.005 ^ 0.1

TOTAL 266 0

Cadusafos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Appendix B. Page 13 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Captan (fungicide) (parent of THPI)

Bananas 179 0 0.19 ^ NT

Carrots 708 0 0.050 ^ 0.05

Nectarines 681 9 1.3 0.083 - 1.0 0.050 ^ 25.0

Peaches 707 49 6.9 0.021 - 3.7 0.020 ^ 15.0

TOTAL 2,275 58

Carbaryl (insecticide) 

Apples 177 1 0.6 0.16 ^ 0.003 ^ 12

Bananas 179 0 0.005 ^ 5.0

Blueberries, Cultivated, Fresh 688 7 1 0.005 - 1.3 0.003 - 0.005 3.0

Blueberries, Frozen 19 0 0.003 - 0.005 3.0

Broccoli 712 0 0.010 ^ 10

Carrots 708 0 0.002 ^ 2.0

Celery 708 1 0.1 0.25 ^ 0.001 - 0.005 3.0

Cherries, Fresh 228 12 5.3 0.003 - 0.24 0.003 ^ 10

Cherries, Frozen 282 33 11.7 0.003 - 0.73 0.003 ^ 10

Grape Juice 502 101 20.1 0.003 - 0.012 0.003 ^ 10

Green Beans, Canned 378 0 0.001 ^ 10

Green Beans, Fresh 757 9 1.2 0.007 - 0.40 0.002 ^ 10

Green Beans, Frozen 378 0 0.001 ^ 10

Nectarines 681 3 0.4 0.071 - 0.61 0.004 ^ 10

Peaches 707 8 1.1 0.034 - 1.4 0.010 ^ 10

Strawberries 176 1 0.6 1.7 ^ 0.003 ^ 4.0

Summer Squash 531 1 0.2 0.038 ^ 0.005 - 0.020 3.0

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.1

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.1

Tomatoes 177 0 0.001 ^ 5.0

Watermelon 359 0 0.003 ^ 3.0

TOTAL 8,522 177

Carbendazim - MBC (fungicide) (metabolite of Benomyl and Thiophanate Methyl)

Apples 177 26 14.7 0.001 - 0.20 0.001 ^ 2.0

Bananas 179 0 0.005 ^ 2.0

Blueberries, Cultiv., Fresh (V-2) 688 2 0.3 0.021 - 0.073 0.005 ^ NT

Blueberries, Frozen 19 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Carrots (V-1) 708 1 0.1 0.005 ^ 0.003 ^ NT

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 8 3.5 0.006 - 0.14 0.005 ^ 20.0

Cherries, Frozen 282 90 31.9 0.006 - 0.33 0.005 ^ 20.0

Grape Juice 531 3 0.6 0.001 ^ 0.001 ^ 5.0

Green Beans, Canned 378 181 47.9 0.002 - 0.057 0.001 ^ 2.0

Green Beans, Frozen 378 182 48.1 0.002 - 0.095 0.001 ^ 2.0

Nectarines 681 16 2.3 0.005 - 0.12 0.003 ^ 3.0

Peaches 707 24 3.4 0.012 - 0.15 0.010 ^ 3.0

Strawberries 176 54 30.7 0.003 - 0.27 0.003 ^ 7.0

Summer Squash 270 3 1.1 0.008 - 0.010 0.005 ^ 1.0

Sweet Corn, Fresh 78 0 0.003 ^ NT

Appendix B. Page 14 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes (V-17) 177 17 9.6 0.002 - 0.037 0.001 ^ NT

Watermelon 390 24 6.2 0.001 - 0.013 0.001 ^ 1.0

TOTAL 7,479 631

Carbofuran (insecticide) (parent of 3-Hydroxycarbofuran)

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.006 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.006 NT

Blueberries, Frozen 19 0 0.005 - 0.006 NT

Broccoli 712 0 0.010 ^ NT

Carrots 708 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.006 ^ NT

Cherries, Frozen 282 0 0.006 ^ NT

Grape Juice 531 0 0.003 ^ 0.4

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh 757 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ 0.5

Summer Squash 531 0 0.005 ^ 0.8

Sweet Corn, Fresh 134 0 0.001 - 0.003 1.0

Sweet Corn, Frozen 41 0 0.001 - 0.003 1.0

Tomatoes 177 0 0.001 ^ NT

Watermelon 359 0 0.002 ^ 0.4

TOTAL 8,551 0

Carbophenothion (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.002 - 0.010 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 357 0 0.002 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,515 0

Carbophenothion methyl (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Appendix B. Page 15 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carboxin (fungicide) 

Blueberries, Cultivated, Fresh 325 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.050 0.2

Sweet Corn, Frozen 41 0 0.005 - 0.050 0.2

TOTAL 1,299 0

Carfentrazone (herbicide) 

Apples 177 0 0.005 ^ 0.10

Bananas 179 0 0.016 ^ 0.20

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.016 0.10

Blueberries, Frozen 19 0 0.003 - 0.016 0.10

Broccoli 712 0 0.005 ^ 0.10

Carrots 708 0 0.002 ^ 0.10

Celery 708 0 0.003 - 0.015 0.10

Cherries, Fresh 228 0 0.016 ^ 0.10

Cherries, Frozen 282 0 0.016 ^ 0.10

Grape Juice 531 0 0.005 ^ 0.10

Green Beans, Canned 378 0 0.005 ^ 0.10

Green Beans, Fresh 757 0 0.005 ^ 0.10

Green Beans, Frozen 378 0 0.005 - 0.015 0.10

Nectarines 681 0 0.002 ^ 0.10

Peaches 707 0 0.005 ^ 0.10

Strawberries 176 0 0.003 ^ 0.10

Summer Squash 502 0 0.003 - 0.005 0.10

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.10

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.10

Tomatoes 177 0 0.005 ^ 0.10

Watermelon 390 0 0.005 ^ 0.10

TOTAL 8,553 0

Chlorantraniliprole (insecticide) 

Apples 177 42 23.7 0.010 - 0.044 0.010 ^ 1.2

Blueberries, Cultivated, Fresh 354 10 2.8 0.011 - 0.32 0.010 ^ 2.5

Blueberries, Frozen 5 0 0.010 ^ 2.5

Broccoli 712 7 1 0.020 - 0.092 0.020 ^ 4.0

Carrots 708 0 0.005 ^ 0.30

Celery 708 221 31.2 0.003 - 0.24 0.002 - 0.010 13

Grape Juice 531 0 0.010 ^ 2.5

Green Beans, Canned 378 0 0.002 ^ 2.0

Green Beans, Fresh 757 58 7.7 0.001 - 0.042 0.001 ^ 2.0

Green Beans, Frozen 378 3 0.8 0.003 ^ 0.002 ^ 2.0

Nectarines 681 6 0.9 0.083 ^ 0.050 ^ 4.0

Peaches 707 111 15.7 0.020 - 0.12 0.020 ^ 4.0

Strawberries 176 39 22.2 0.010 - 0.12 0.010 ^ 1.0

Summer Squash 531 2 0.4 0.006 ^ 0.005 - 0.010 0.5

Sweet Corn, Fresh 134 0 0.001 - 0.010 0.02

Sweet Corn, Frozen 41 0 0.001 - 0.010 0.02

Appendix B. Page 16 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 42 23.7 0.003 - 0.027 0.002 ^ 1.4

Watermelon 390 1 0.3 0.012 ^ 0.010 ^ 0.5

TOTAL 7,545 542

Chlorethoxyfos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.01

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.01

TOTAL 1,328 0

Chlorfenapyr (insecticide) 

Apples 177 0 0.015 ^ 0.01

Bananas 179 0 0.040 ^ 0.01

Blueberries, Cultivated, Fresh 688 0 0.040 - 0.25 0.01

Blueberries, Frozen 19 0 0.040 - 0.25 0.01

Broccoli 712 0 0.005 ^ 0.01

Carrots 708 0 0.050 ^ 0.01

Celery 708 0 0.002 - 0.25 0.01

Cherries, Fresh 228 0 0.040 ^ 0.01

Cherries, Frozen 282 0 0.040 ^ 0.01

Grape Juice 531 0 0.015 ^ 0.01

Green Beans, Canned 378 0 0.002 ^ 0.01

Green Beans, Fresh (X-1) 757 1 0.1 0.071 ^ 0.025 ^ 0.01

Green Beans, Frozen 378 0 0.002 ^ 0.01

Nectarines 681 0 0.025 ^ 0.01

Peaches 707 0 0.005 ^ 0.01

Strawberries 176 0 0.25 ^ 0.01

Summer Squash 531 0 0.050 - 0.25 0.01

Sweet Corn, Fresh 134 0 0.025 - 0.25 0.01

Sweet Corn, Frozen 41 0 0.025 - 0.25 0.01

Tomatoes 177 21 11.9 0.004 - 0.36 0.002 ^ 1.0

Watermelon 390 0 0.015 ^ 0.01

TOTAL 8,582 22

Chlorfenvinphos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.004 - 0.010 NT

Green Beans, Canned 378 0 0.004 ^ NT

Green Beans, Frozen 378 0 0.004 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.004 ^ NT

TOTAL 2,536 0

Appendix B. Page 17 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Chlorimuron ethyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ 0.02

Blueberries, Frozen 5 0 0.020 ^ 0.02

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Chlorobenzilate (acaricide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Chloroneb (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Chlorothalonil (fungicide) 

Apples 177 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 354 6 1.7 0.021 - 0.11 0.010 ^ 1.0

Blueberries, Frozen 5 0 0.010 ^ 1.0

Celery 348 107 30.7 0.010 - 0.60 0.010 ^ 15

Peaches 677 7 1 0.006 - 0.029 0.005 ^ 0.5

Strawberries (V-2) 176 2 1.1 0.036 - 0.14 0.010 ^ NT

Summer Squash 270 20 7.4 0.011 - 0.22 0.010 ^ 5.0

Watermelon 390 0 0.020 ^ 5.0

TOTAL 2,397 142

Chlorpropham (herbicide, growth regulator)

Apples 177 0 0.020 ^ NT

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.020 NT

Blueberries, Frozen 19 0 0.005 - 0.020 NT

Broccoli (V-2) 712 2 0.3 0.006 - 0.010 0.005 ^ NT

Celery (V-1) 708 1 0.1 0.002 ^ 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.020 ^ NT

Green Beans, Canned 378 0 0.001 - 0.003 NT

Green Beans, Fresh 757 0 0.020 ^ NT

Appendix B. Page 18 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Frozen (V-1) 378 1 0.3 0.035 ^ 0.001 ^ NT

Nectarines 681 0 0.060 ^ NT

Peaches (V-2) 677 2 0.3 0.008 - 0.043 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.20 NT

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes (V-8) 177 8 4.5 0.002 - 0.058 0.001 ^ NT

Watermelon 390 0 0.020 ^ NT

TOTAL 7,844 14

Chlorpyrifos (insecticide) 

Apples 177 0 0.005 ^ 0.01

Bananas 179 0 0.005 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.010 ^ 0.1

Blueberries, Frozen 19 0 0.010 ^ 0.1

Broccoli 712 3 0.4 0.007 - 0.014 0.005 ^ 1.0

Carrots 708 0 0.006 ^ 0.1

Celery 708 3 0.4 0.002 - 0.022 0.001 - 0.010 0.1

Cherries, Fresh 228 0 0.010 ^ 1.0

Cherries, Frozen 282 1 0.4 0.018 ^ 0.010 ^ 1.0

Grape Juice 531 0 0.005 ^ 0.01

Green Beans, Canned 378 0 0.001 ^ 0.05

Green Beans, Fresh 757 0 0.035 ^ 0.05

Green Beans, Frozen 378 1 0.3 0.017 ^ 0.001 ^ 0.05

Nectarines 681 33 4.8 0.005 - 0.040 0.003 ^ 0.05

Peaches (X-1) 707 32 4.5 0.005 - 0.065 0.005 ^ 0.05

Strawberries 176 1 0.6 0.005 ^ 0.005 ^ 0.2

Summer Squash 531 1 0.2 0.011 ^ 0.010 - 0.075 0.1

Sweet Corn, Fresh 134 0 0.005 - 0.035 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.035 0.05

Tomatoes 177 0 0.001 ^ 0.1

Watermelon 390 0 0.005 ^ 0.1

TOTAL 8,582 75

Chlorpyrifos oxygen analog (metabolite of Chlorpyrifos)

Apples 177 0 0.002 ^ 0.01

Bananas 179 0 0.009 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.004 - 0.010 0.1

Blueberries, Frozen 19 0 0.004 - 0.010 0.1

Carrots 708 0 0.002 ^ 0.1

Celery 708 0 0.001 - 0.010 0.1

Cherries, Fresh 228 0 0.004 ^ 1.0

Cherries, Frozen 282 0 0.004 ^ 1.0

Grape Juice 531 0 0.002 ^ 0.01

Green Beans, Canned 378 0 0.001 ^ 0.05

Green Beans, Fresh 757 0 0.001 ^ 0.05

Green Beans, Frozen 378 0 0.001 ^ 0.05

Nectarines 681 0 0.001 ^ 0.05

Strawberries 176 0 0.010 ^ 0.2

Summer Squash 531 0 0.005 - 0.010 0.1

Sweet Corn, Fresh 134 0 0.001 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.001 - 0.010 0.05

Appendix B. Page 19 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 0 0.001 ^ 0.1

Watermelon 390 0 0.002 ^ 0.1

TOTAL 7,163 0

Clethodim (herbicide) 

Carrots 688 0 0.001 ^ 1.0

Celery 360 0 0.002 - 0.008 0.60

Green Beans, Canned 378 0 0.008 ^ 3.5

Green Beans, Fresh 757 0 0.40 ^ 3.5

Green Beans, Frozen 378 0 0.008 ^ 3.5

Nectarines 681 0 0.001 ^ 0.20

Strawberries 176 0 0.040 ^ 3.0

Summer Squash 232 0 0.20 ^ 0.50

Sweet Corn, Fresh 134 0 0.040 - 0.40 NT

Sweet Corn, Frozen 41 0 0.040 - 0.40 NT

Tomatoes 177 0 0.002 ^ 1.0

TOTAL 4,002 0

Clofentezine (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Nectarines 668 5 0.7 0.004 - 0.055 0.001 - 0.003 1.0

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,911 5

Clomazone (herbicide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.070 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.070 NT

Blueberries, Frozen 19 0 0.003 - 0.070 NT

Broccoli 712 0 0.005 ^ 0.10

Celery 708 0 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.070 ^ NT

Cherries, Frozen 282 0 0.070 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.002 ^ 0.05

Green Beans, Fresh 757 0 0.005 ^ 0.05

Green Beans, Frozen 378 0 0.002 ^ 0.05

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.050 0.1

Sweet Corn, Fresh 134 0 0.003 - 0.005 NT

Sweet Corn, Frozen 41 0 0.003 - 0.005 NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.005 ^ 0.05

TOTAL 7,193 0

Appendix B. Page 20 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Clopyralid (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ 0.50

Blueberries, Frozen 5 0 0.020 ^ 0.50

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ 4.0

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ 1.0

Sweet Corn, Frozen 12 0 0.020 ^ 1.0

TOTAL 1,243 0

Cloransulam methyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Clothianidin (insecticide) (also a metabolite of Thiamethoxam)

Apples 177 0 0.010 ^ 1.0

Bananas 179 0 0.035 ^ 0.02

Blueberries, Cultivated, Fresh 688 3 0.4 0.005 - 0.006 0.005 - 0.035 0.01

Blueberries, Frozen 19 0 0.005 - 0.035 0.01

Broccoli 712 5 0.7 0.010 - 0.013 0.010 ^ 1.9

Carrots 708 0 0.005 ^ 0.8

Celery 708 0 0.002 - 0.005 3.0

Cherries, Fresh 228 0 0.035 ^ 0.5

Cherries, Frozen 282 0 0.035 ^ 0.5

Grape Juice 531 0 0.010 ^ 0.60

Green Beans, Canned 378 0 0.002 ^ 0.02

Green Beans, Fresh 757 3 0.4 0.009 - 0.019 0.005 ^ 0.02

Green Beans, Frozen 378 0 0.002 ^ 0.02

Nectarines 680 7 1 0.008 - 0.058 0.005 ^ 0.80

Peaches 707 44 6.2 0.010 - 0.17 0.010 ^ 0.80

Strawberries 176 0 0.003 ^ 0.02

Summer Squash 531 8 1.5 0.005 - 0.011 0.005 - 0.050 0.06

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.01

Sweet Corn, Frozen 41 1 2.4 0.003 ^ 0.003 - 0.005 0.01

Tomatoes 177 17 9.6 0.003 - 0.038 0.002 ^ 0.20

Watermelon 390 0 0.010 ^ 0.06

TOTAL 8,581 88

Coumaphos (insecticide) 

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Appendix B. Page 21 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 4,522 0

Coumaphos oxygen analog (metabolite of Coumaphos)

Apples 177 0 0.010 ^ NT

Celery 360 0 0.008 ^ NT

Green Beans, Canned 378 0 0.008 ^ NT

Green Beans, Frozen 378 0 0.008 ^ NT

Tomatoes 177 0 0.008 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 1,860 0

Crotoxyphos (insecticide, acaricide)

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Crufomate (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Cyantraniliprole (insecticide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.004 ^ 2.0

TOTAL 443 0

Cyazofamid (fungicide) 

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Carrots 707 58 8.2 0.007 - 0.029 0.004 ^ 0.09

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Green Beans, Fresh 757 8 1.1 0.013 - 0.077 0.010 ^ 0.5

Appendix B. Page 22 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.010 ^ NT

Summer Squash 531 1 0.2 0.011 ^ 0.010 - 0.050 0.10

Sweet Corn, Fresh 134 0 0.010 ^ NT

Sweet Corn, Frozen 41 0 0.010 ^ NT

Tomatoes 177 0 0.012 ^ 0.9

TOTAL 4,267 67

Cyflufenamid (fungicide) 

Strawberries 176 5 2.8 0.003 - 0.027 0.003 ^ 0.20

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Strawberries 176 2 1.1 0.013 - 0.054 0.005 ^ 0.60

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 532 7

Cyfluthrin (insecticide) 

Apples 177 1 0.6 0.007 ^ 0.004 ^ 0.5

Bananas 179 0 0.042 ^ 0.05

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.042 0.05

Blueberries, Frozen 19 0 0.005 - 0.042 0.05

Broccoli 712 5 0.7 0.008 - 0.025 0.005 ^ 2.5

Carrots 708 0 0.015 ^ 0.20

Celery 708 8 1.1 0.005 - 0.032 0.005 - 0.050 6.0

Cherries, Fresh 228 0 0.042 ^ 0.3

Cherries, Frozen 282 5 1.8 0.050 - 0.13 0.042 ^ 0.3

Grape Juice 531 0 0.004 ^ 1.0

Green Beans, Canned 378 0 0.008 - 0.025 0.05

Green Beans, Fresh 726 2 0.3 0.010 - 0.011 0.010 - 0.10 0.05

Green Beans, Frozen 378 0 0.008 ^ 0.05

Nectarines 681 8 1.2 0.025 ^ 0.015 ^ 0.3

Peaches 707 75 10.6 0.005 - 0.11 0.005 ^ 0.3

Strawberries 176 0 0.005 ^ 0.05

Summer Squash 531 0 0.005 - 0.10 0.1

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.05

Tomatoes 177 0 0.025 ^ 0.20

Watermelon 390 0 0.004 ^ 0.1

TOTAL 8,551 104

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (insecticide)

Apples 177 9 5.1 0.005 - 0.020 0.005 ^ 0.30

Bananas 179 0 0.012 ^ 0.01

Blueberries, Cultivated, Fresh 688 1 0.1 0.012 ^ 0.010 - 0.012 0.01

Blueberries, Frozen 19 0 0.010 - 0.012 0.01

Broccoli 712 13 1.8 0.013 - 0.051 0.008 ^ 0.4

Celery 708 1 0.1 0.005 ^ 0.003 - 0.010 0.01

Cherries, Fresh 228 96 42.1 0.012 - 0.11 0.012 - 0.024 0.50

Cherries, Frozen 282 13 4.6 0.012 - 0.21 0.012 - 0.024 0.50

Grape Juice 531 0 0.005 ^ 0.01

Green Beans, Canned 378 4 1.1 0.005 - 0.017 0.003 ^ 0.20

Green Beans, Fresh 757 13 1.7 0.008 - 0.076 0.008 - 0.075 0.20

Green Beans, Frozen 378 12 3.2 0.005 - 0.027 0.003 ^ 0.20

Appendix B. Page 23 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 707 116 16.4 0.008 - 0.086 0.008 ^ 0.50

Strawberries 176 0 0.010 ^ 0.01

Summer Squash 531 0 0.010 - 0.075 0.05

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.05

Tomatoes 177 5 2.8 0.005 ^ 0.003 ^ 0.1

Watermelon 390 0 0.005 ^ 0.05

TOTAL 7,193 283

Cyhalothrin, Lambda (includes gamma isomer)

Carrots 708 1 0.1 0.003 ^ 0.002 ^ 0.01

Nectarines 681 172 25.3 0.003 - 0.053 0.002 ^ 0.50

TOTAL 1,389 173

Cymoxanil (fungicide)

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Celery 708 0 0.003 - 0.010 6.0

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Fresh 757 0 0.010 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 531 0 0.010 - 0.050 0.05

Sweet Corn, Fresh 134 0 0.010 ^ NT

Sweet Corn, Frozen 41 0 0.010 ^ NT

Tomatoes 177 0 0.003 ^ 0.2

Watermelon 263 0 0.002 ^ 0.05

TOTAL 5,116 0

Cypermethrin (insecticide) 

Apples 177 1 0.6 0.046 ^ 0.010 ^ 2

Bananas 179 0 0.069 ^ 0.05

Blueberries, Cultivated, Fresh 688 137 19.9 0.011 - 0.66 0.010 - 0.068 0.8

Blueberries, Frozen 19 8 42.1 0.015 - 0.15 0.010 - 0.068 0.8

Broccoli (X-1) 712 8 1.1 0.013 - 2.6 0.010 ^ 2.0

Carrots 708 0 0.020 ^ 0.1

Celery 708 24 3.4 0.010 - 0.11 0.010 - 0.075 10.00

Cherries, Fresh 228 0 0.068 ^ 1

Cherries, Frozen 282 28 9.9 0.070 - 0.34 0.068 ^ 1

Grape Juice 531 0 0.010 ^ 2

Green Beans, Canned 378 6 1.6 0.037 - 0.11 0.022 ^ 0.5

Green Beans, Fresh 757 12 1.6 0.031 - 0.061 0.030 - 0.30 0.5

Green Beans, Frozen 378 9 2.4 0.037 ^ 0.022 ^ 0.5

Nectarines 681 0 0.020 ^ 1

Peaches 707 21 3 0.010 - 0.18 0.010 ^ 1

Strawberries 176 0 0.010 ^ 0.8

Summer Squash 531 5 0.9 0.011 - 0.035 0.010 - 0.20 0.2

Sweet Corn, Fresh 134 0 0.010 - 0.025 0.05

Sweet Corn, Frozen 41 0 0.010 - 0.025 0.05

Appendix B. Page 24 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 3 1.7 0.037 ^ 0.022 ^ 0.2

Watermelon 390 0 0.010 ^ 0.2

TOTAL 8,582 262

Cyphenothrin (insecticide) 

Apples 177 0 0.015 ^ NT

Bananas 179 0 0.029 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.058 NT

Blueberries, Frozen 19 0 0.010 - 0.058 NT

Carrots 708 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.058 ^ NT

Cherries, Frozen 282 0 0.058 ^ NT

Grape Juice 531 0 0.015 ^ NT

Green Beans, Fresh 757 0 0.050 ^ NT

Nectarines 681 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 531 0 0.010 - 0.050 NT

Sweet Corn, Fresh 134 0 0.010 - 0.050 NT

Sweet Corn, Frozen 41 0 0.010 - 0.050 NT

Watermelon 390 0 0.015 ^ NT

TOTAL 5,870 0

Cyproconazole (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultiv., Fresh (V-1) 688 1 0.1 0.007 ^ 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 30 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 3,318 1

Cyprodinil (fungicide) 

Apples 177 13 7.3 0.005 - 0.045 0.005 ^ 1.7

Bananas 179 0 0.012 ^ NT

Blueberries, Cultivated, Fresh 688 189 27.5 0.003 - 1.0 0.003 - 0.012 3.0

Blueberries, Frozen 19 10 52.6 0.009 - 0.28 0.003 - 0.012 3.0

Broccoli (X-1) 712 2 0.3 0.022 - 1.4 0.005 ^ 1.0

Carrots 708 1 0.1 0.026 ^ 0.001 ^ 0.75

Celery 348 1 0.3 0.003 ^ 0.003 ^ 30

Cherries, Fresh 228 2 0.9 0.021 - 0.045 0.012 ^ 2.0

Cherries, Frozen 282 0 0.012 ^ 2.0

Grape Juice 501 0 0.005 ^ 3.0

Green Beans, Fresh 757 2 0.3 0.055 - 0.069 0.055 ^ 0.6

Nectarines 681 13 1.9 0.003 - 0.27 0.002 ^ 2.0

Peaches 707 40 5.7 0.006 - 0.77 0.005 ^ 2.0

Strawberries 176 112 63.6 0.003 - 1.3 0.003 ^ 5.0

Appendix B. Page 25 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 531 2 0.4 0.003 - 0.006 0.003 - 0.055 0.70

Sweet Corn, Fresh 134 0 0.003 - 0.055 NT

Sweet Corn, Frozen 41 0 0.003 - 0.055 NT

Watermelon 390 23 5.9 0.005 - 0.026 0.005 ^ 0.70

TOTAL 7,259 410

Cyprosulfamide (herbicide safener) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.01

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.01

TOTAL 351 0

Cyromazine (insect growth regulator) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 86 24.7 0.005 - 0.066 0.005 ^ 7.0

Green Beans, Fresh 757 0 0.10 ^ 2.0

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 3 0.6 0.005 - 0.015 0.005 - 0.16 1.0

Sweet Corn, Fresh 134 0 0.005 - 0.10 0.5

Sweet Corn, Frozen 41 0 0.005 - 0.10 0.5

Tomatoes 177 0 0.008 ^ 0.5

TOTAL 2,523 89

DCPA (herbicide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.020 NT

Blueberries, Frozen 19 0 0.003 - 0.020 NT

Broccoli 712 55 7.7 0.005 - 0.056 0.005 ^ 5.0

Celery (V-9) 708 9 1.3 0.002 - 0.007 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.002 ^ NT

Green Beans, Canned 378 0 0.001 ^ 2.0

Green Beans, Fresh 757 0 0.010 ^ 2.0

Green Beans, Frozen 378 2 0.5 0.002 ^ 0.001 ^ 2.0

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ 2.0

Summer Squash 531 0 0.003 - 0.025 1.0

Sweet Corn, Fresh 134 0 0.003 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.003 - 0.010 0.05

Tomatoes 177 0 0.001 ^ 1.0

Watermelon 390 0 0.002 ^ 1.0

TOTAL 7,193 66

DEF - Tribufos (herbicide, plant growth regulator)

Apples 177 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.002 ^ NT

Strawberries 176 0 0.003 ^ NT

Appendix B. Page 26 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 2,341 0

Deltamethrin (includes parent Tralomethrin) (insecticide) 

Apples 177 0 0.015 ^ 0.2

Bananas 179 0 0.12 ^ 0.05

Blueberries, Cultivated, Fresh 688 1 0.1 0.007 ^ 0.005 - 0.12 0.05

Blueberries, Frozen 19 0 0.005 - 0.12 0.05

Broccoli 712 0 0.008 ^ 0.05

Carrots 708 0 0.020 ^ 0.2

Celery 708 0 0.005 - 0.040 0.05

Cherries, Fresh 228 0 0.12 ^ 0.05

Cherries, Frozen 282 0 0.12 ^ 0.05

Grape Juice 531 0 0.015 ^ 0.05

Green Beans, Canned 378 0 0.012 ^ 0.05

Green Beans, Fresh 757 0 0.050 ^ 0.05

Green Beans, Frozen 378 0 0.012 - 0.040 0.05

Nectarines 681 0 0.020 ^ 0.05

Peaches 707 0 0.008 ^ 0.05

Strawberries 176 0 0.005 ^ 0.05

Summer Squash 531 0 0.005 - 0.10 0.2

Sweet Corn, Fresh 134 0 0.005 - 0.025 0.03

Sweet Corn, Frozen 41 0 0.005 - 0.025 0.03

Tomatoes 177 1 0.6 0.048 ^ 0.040 ^ 0.2

Watermelon 390 0 0.015 ^ 0.2

TOTAL 8,582 2

Demeton-O (metabolite of the insecticide Demeton)

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Demeton-S (metabolite of Demeton)

Blueberries, Cultivated, Fresh 354 0 0.030 ^ NT

Blueberries, Frozen 5 0 0.030 ^ NT

Celery 348 0 0.030 ^ NT

Strawberries 176 0 0.030 ^ NT

Summer Squash 270 0 0.030 ^ NT

Sweet Corn, Fresh 78 0 0.030 ^ NT

Sweet Corn, Frozen 12 0 0.030 ^ NT

TOTAL 1,243 0

Demeton-S sulfone (metabolite of Demeton-S)

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Appendix B. Page 27 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Dialifos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Diazinon (insecticide) 

Apples 177 11 6.2 0.005 - 0.071 0.005 ^ 0.50

Bananas 179 0 0.010 ^ 0.20

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.010 0.50

Blueberries, Frozen 19 0 0.003 - 0.010 0.50

Broccoli 712 0 0.002 ^ 0.70

Carrots 708 30 4.2 0.002 - 0.045 0.001 ^ 0.75

Celery 348 2 0.6 0.004 - 0.022 0.003 ^ 0.70

Cherries, Fresh 228 0 0.010 ^ 0.20

Cherries, Frozen 282 0 0.010 ^ 0.20

Grape Juice 531 0 0.005 ^ 0.75

Green Beans, Fresh 757 1 0.1 0.002 ^ 0.001 ^ 0.50

Nectarines 681 3 0.4 0.002 - 0.004 0.001 ^ 0.20

Peaches 707 1 0.1 0.003 ^ 0.002 ^ 0.20

Strawberries 176 0 0.003 ^ 0.50

Summer Squash 531 0 0.003 - 0.20 0.50

Sweet Corn, Fresh 134 0 0.003 - 0.005 NT

Sweet Corn, Frozen 41 0 0.003 - 0.005 NT

Watermelon 390 0 0.005 ^ 0.75

TOTAL 7,289 48

Diazinon oxygen analog (metabolite of Diazinon)

Bananas 179 0 0.008 ^ 0.20

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.008 0.50

Blueberries, Frozen 19 0 0.005 - 0.008 0.50

Broccoli 712 0 0.001 ^ 0.70

Carrots 708 0 0.001 ^ 0.75

Celery 708 0 0.001 - 0.005 0.70

Cherries, Fresh 228 0 0.008 ^ 0.20

Cherries, Frozen 282 0 0.008 ^ 0.20

Green Beans, Canned 378 0 0.001 ^ 0.50

Green Beans, Fresh 757 0 0.001 ^ 0.50

Green Beans, Frozen 378 0 0.001 ^ 0.50

Nectarines 681 0 0.001 ^ 0.20

Peaches 707 0 0.001 ^ 0.20

Strawberries 176 0 0.005 ^ 0.50

Appendix B. Page 28 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 531 0 0.005 - 0.060 0.50

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ 0.75

TOTAL 7,484 0

Dicamba (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.25 ^ NT

Blueberries, Frozen 5 0 0.25 ^ NT

Celery 348 0 0.25 ^ NT

Strawberries 176 0 0.25 ^ NT

Summer Squash 270 0 0.25 ^ NT

Sweet Corn, Fresh 78 0 0.25 ^ 0.04

Sweet Corn, Frozen 12 0 0.25 ^ 0.04

TOTAL 1,243 0

Dichlobenil (herbicide) 

Apples 177 0 0.010 ^ 0.5

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.007 NT

Blueberries, Frozen 19 0 0.003 - 0.007 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.007 ^ 0.15

Cherries, Frozen 282 0 0.007 ^ 0.15

Grape Juice 531 0 0.010 ^ 0.15

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ 0.15

Strawberries 176 0 0.003 ^ NT

Summer Squash (V-1) 270 1 0.4 0.004 ^ 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,090 1

Dichlofluanid (fungicide, acaricide)

Bananas 179 0 0.035 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.017 ^ NT

Blueberries, Frozen 14 0 0.017 ^ NT

Cherries, Fresh 228 0 0.017 ^ NT

Cherries, Frozen 282 0 0.017 ^ NT

TOTAL 1,037 0

Dichlormid (herbicide safener)

Strawberries 176 0 0.050 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.050 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.050 0.05

TOTAL 351 0

Appendix B. Page 29 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Dichlorprop (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.050 ^ NT

Blueberries, Frozen 5 0 0.050 ^ NT

Celery 348 0 0.050 ^ NT

Strawberries 176 0 0.050 ^ NT

Summer Squash 270 0 0.050 ^ NT

Sweet Corn, Fresh 78 0 0.050 ^ NT

Sweet Corn, Frozen 12 0 0.050 ^ NT

TOTAL 1,243 0

Dichlorvos - DDVP (insecticide) (also a metabolite of Naled)

Apples 177 0 0.020 ^ 0.5

Bananas 179 0 0.005 ^ 0.5

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.020 0.5

Blueberries, Frozen 19 0 0.005 - 0.020 0.5

Carrots 708 0 0.012 ^ 0.5

Celery 708 0 0.003 - 0.020 0.5

Cherries, Fresh 228 0 0.005 ^ 0.5

Cherries, Frozen 282 0 0.005 ^ 0.5

Grape Juice 472 0 0.020 ^ 0.5

Green Beans, Canned 378 0 0.003 ^ 0.5

Green Beans, Fresh 757 0 0.060 ^ 0.5

Green Beans, Frozen 378 0 0.003 ^ 0.5

Nectarines 681 0 0.010 ^ 0.5

Strawberries 176 4 2.3 0.074 - 0.40 0.020 ^ 0.5

Summer Squash 531 0 0.020 - 0.060 0.5

Sweet Corn, Fresh 134 0 0.005 - 0.020 0.5

Sweet Corn, Frozen 41 0 0.005 - 0.020 0.5

Watermelon 327 0 0.020 ^ 0.5

TOTAL 6,864 4

Diclofop methyl (herbicide) 

Apples 177 0 0.001 ^ NT

Grape Juice 531 0 0.001 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 1,098 0

Dicloran (fungicide) 

Apples 177 0 0.016 ^ NT

Bananas 179 0 0.020 - 0.040 NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.020 ^ 10

Celery 708 294 41.5 0.004 - 1.5 0.002 - 0.010 15

Cherries, Fresh 228 0 0.020 ^ 20

Cherries, Frozen 282 0 0.020 ^ 20

Grape Juice 531 0 0.016 ^ 10

Green Beans, Canned 357 0 0.002 - 0.008 20

Green Beans, Fresh 757 54 7.1 0.010 - 3.4 0.010 - 0.10 20

Green Beans, Frozen 378 0 0.002 ^ 20

Nectarines 681 0 0.020 ^ 20

Peaches 707 0 0.005 ^ 20

Appendix B. Page 30 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.010 - 0.10 NT

Sweet Corn, Frozen 41 0 0.010 - 0.10 NT

Tomatoes 177 7 4 0.011 - 0.11 0.002 ^ 5

Watermelon 390 0 0.016 ^ NT

TOTAL 8,300 355

Diclosulam (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 1,243 0

Dicofol Total (insecticide) 

Green Beans, Fresh 757 0 0.015 - 0.15 3.0

Nectarines 681 1 0.1 0.005 ^ 0.003 ^ 5.0

Summer Squash 261 0 0.15 ^ 2.0

TOTAL 1,699 1

Dicofol o,p' (isomer of Dicofol) 

Bananas 179 0 0.015 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.015 NT

Blueberries, Frozen 19 0 0.010 - 0.015 NT

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 228 0 0.015 ^ 5.0

Cherries, Frozen 282 0 0.015 ^ 5.0

Green Beans, Canned 378 0 0.002 ^ 3.0

Green Beans, Frozen 378 0 0.002 ^ 3.0

Strawberries 176 0 0.010 ^ 10.0

Summer Squash 270 0 0.010 ^ 2.0

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.002 ^ 2.0

TOTAL 3,573 0

Dicofol p,p' (isomer of Dicofol) 

Apples 177 0 0.010 ^ 10.0

Bananas 179 0 0.024 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.024 NT

Blueberries, Frozen 19 0 0.005 - 0.024 NT

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.024 ^ 5.0

Cherries, Frozen 282 0 0.024 ^ 5.0

Grape Juice 531 0 0.010 ^ 5.0

Green Beans, Canned 378 0 0.001 ^ 3.0

Green Beans, Frozen 378 0 0.001 ^ 3.0

Peaches 453 0 0.005 ^ 5.0

Strawberries 176 0 0.005 ^ 10.0

Appendix B. Page 31 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.005 ^ 2.0

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ 2.0

Watermelon 390 0 0.010 ^ 2.0

TOTAL 5,209 0

Dicrotophos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 708 0 0.002 - 0.003 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,536 0

Diethofencarb (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Difenoconazole (fungicide) 

Apples 177 2 1.1 0.011 - 0.014 0.010 ^ 1.0

Bananas 179 0 0.005 ^ 0.2

Blueberries, Cultivated, Fresh 688 4 0.6 0.007 - 0.020 0.005 ^ 2.5

Blueberries, Frozen 19 0 0.005 ^ 2.5

Broccoli 712 3 0.4 0.009 - 0.097 0.005 ^ 1.9

Carrots 708 16 2.3 0.002 - 0.009 0.001 ^ 0.50

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 2 0.9 0.022 - 0.030 0.005 ^ 2.5

Cherries, Frozen 282 0 0.005 ^ 2.5

Grape Juice 531 0 0.010 ^ 4.0

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh (V-1) 757 1 0.1 0.005 ^ 0.005 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.001 ^ 2.5

Peaches 707 23 3.3 0.007 - 0.18 0.005 ^ 2.5

Strawberries 176 2 1.1 0.031 - 0.087 0.005 ^ 2.5

Summer Squash 531 1 0.2 0.013 ^ 0.005 ^ 0.70

Sweet Corn, Fresh 134 0 0.005 ^ 0.01

Sweet Corn, Frozen 41 0 0.005 ^ 0.01

Tomatoes 177 37 20.9 0.002 - 0.041 0.001 ^ 0.60

Watermelon 390 0 0.010 ^ 0.70

TOTAL 8,582 91

Appendix B. Page 32 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Diflubenzuron (insecticide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.15 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.020 - 0.076 NT

Blueberries, Frozen 19 0 0.020 - 0.076 NT

Carrots 708 0 0.002 ^ NT

Celery 708 0 0.002 - 0.020 NT

Cherries, Fresh 228 0 0.076 ^ NT

Cherries, Frozen 282 0 0.076 ^ NT

Grape Juice 531 0 0.003 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Nectarines 681 3 0.4 0.005 - 0.017 0.003 ^ 0.07

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 6,060 3

Diflufenzopyr (herbicide) 

Sweet Corn, Fresh 56 0 0.001 ^ 0.05

Sweet Corn, Frozen 29 0 0.001 ^ 0.05

TOTAL 85 0

Dimethenamid (herbicide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.007 NT

Blueberries, Frozen 19 0 0.003 - 0.007 NT

Celery 693 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.007 ^ NT

Cherries, Frozen 282 0 0.007 ^ NT

Grape Juice 531 0 0.003 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.01

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.01

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 4,741 0

Dimethoate (insecticide) (parent of Omethoate)

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 2 0.3 0.005 - 0.020 0.003 - 0.005 1.0

Blueberries, Frozen 19 1 5.3 0.006 ^ 0.003 - 0.005 1.0

Broccoli 712 0 0.010 ^ 2.0

Celery 708 26 3.7 0.003 - 0.092 0.002 - 0.003 2.0

Appendix B. Page 33 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cherries, Fresh 228 1 0.4 0.067 ^ 0.005 ^ 2.0

Cherries, Frozen 282 34 12.1 0.005 - 0.25 0.005 ^ 2.0

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.002 - 0.008 2.0

Green Beans, Fresh (X-3) 757 54 7.1 0.001 - 2.6 0.001 ^ 2.0

Green Beans, Frozen 378 0 0.002 ^ 2.0

Nectarines 681 0 0.003 ^ NT

Peaches (V-2) 707 2 0.3 0.015 - 0.028 0.010 ^ NT

Strawberries (V-1) 176 1 0.6 0.005 ^ 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.010 NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

Tomatoes 177 1 0.6 0.011 ^ 0.002 ^ 2.0

Watermelon 390 1 0.3 0.007 ^ 0.005 ^ 1.0

TOTAL 7,874 123

Dimethomorph (fungicide) 

Apples 177 0 0.003 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 2 0.3 0.26 - 0.29 0.010 ^ 6.0

Celery 708 3 0.4 0.002 ^ 0.001 - 0.005 30.0

Grape Juice 531 0 0.003 ^ 3.0

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh (V-1) 757 1 0.1 0.005 ^ 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.010 0.5

Sweet Corn, Fresh 134 0 0.005 - 0.025 NT

Sweet Corn, Frozen 41 0 0.005 - 0.025 NT

Tomatoes 177 8 4.5 0.002 - 0.020 0.001 ^ 1.5

Watermelon 390 0 0.003 ^ 0.5

TOTAL 6,156 14

Diniconazole (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Dinotefuran (insecticide) 

Apples 177 0 0.003 ^ 2.0

Bananas 179 0 0.015 ^ 0.01

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.015 0.2

Blueberries, Frozen 19 0 0.010 - 0.015 0.2

Celery 708 32 4.5 0.011 - 0.094 0.006 - 0.020 5.0

Cherries, Fresh 228 0 0.015 ^ 2.0

Cherries, Frozen 282 0 0.015 ^ 2.0

Appendix B. Page 34 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Grape Juice 531 0 0.003 ^ 0.9

Green Beans, Canned 378 0 0.006 ^ 0.01

Green Beans, Fresh (X-7) 757 7 0.9 0.069 - 0.16 0.040 ^ 0.01

Green Beans, Frozen 378 0 0.006 ^ 0.01

Nectarines 681 0 0.060 ^ 1.0

Strawberries 176 0 0.005 ^ 0.01

Summer Squash 531 10 1.9 0.013 - 0.49 0.010 - 0.10 0.5

Sweet Corn, Fresh 134 0 0.005 - 0.040 0.01

Sweet Corn, Frozen 41 0 0.005 - 0.040 0.01

Tomatoes 177 34 19.2 0.010 - 0.13 0.006 ^ 0.7

Watermelon 390 7 1.8 0.004 - 0.012 0.003 ^ 0.5

TOTAL 6,455 90

Dioxacarb (insecticide) 

Nectarines 681 0 0.004 - 0.013 NT

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 947 0

Dioxathion (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Diphenamid (herbicide) 

Broccoli 712 0 0.005 ^ NT

Celery 360 0 0.002 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,712 0

Diphenylamine - DPA (plant growth regulator) 

Apples 177 109 61.6 0.002 - 4.2 0.002 ^ 10.0

Bananas 179 0 0.060 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.061 NT

Blueberries, Frozen 19 0 0.003 - 0.061 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.003 - 0.010 NT

Cherries, Fresh 228 0 0.061 ^ NT

Cherries, Frozen 282 0 0.061 ^ NT

Grape Juice (V-1) 531 1 0.2 0.002 ^ 0.002 ^ NT

Green Beans, Canned 378 0 0.003 - 0.010 NT

Green Beans, Frozen 378 0 0.003 ^ NT

Peaches 673 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Appendix B. Page 35 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 6,056 110

Disulfoton (insecticide) 

Bananas 179 0 0.050 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.050 NT

Blueberries, Frozen 19 0 0.010 - 0.050 NT

Broccoli 712 0 0.005 ^ 0.75

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 218 0 0.050 ^ NT

Cherries, Frozen 267 0 0.050 ^ NT

Green Beans, Canned 378 0 0.002 ^ 0.75

Green Beans, Frozen 378 0 0.002 ^ 0.75

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 4,967 0

Disulfoton oxygen analog (metabolite of Disulfoton)

Apples 177 0 0.001 ^ NT

Bananas 179 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.002 ^ NT

Blueberries, Frozen 14 0 0.002 ^ NT

Celery 360 0 0.002 ^ NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

Grape Juice 531 0 0.001 ^ NT

Green Beans, Canned 378 0 0.002 ^ 0.75

Green Beans, Fresh 757 0 0.001 ^ 0.75

Green Beans, Frozen 378 0 0.002 ^ 0.75

Sweet Corn, Fresh 56 0 0.001 ^ NT

Sweet Corn, Frozen 29 0 0.001 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 4,270 0

Disulfoton sulfone (metabolite of Disulfoton)

Apples 177 0 0.020 ^ NT

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.010 NT

Blueberries, Frozen 19 0 0.003 - 0.010 NT

Broccoli 692 0 0.050 ^ 0.75

Celery (V-1) 708 1 0.1 0.004 ^ 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.010 - 0.020 NT

Cherries, Frozen 282 0 0.010 - 0.020 NT

Grape Juice 531 0 0.020 ^ NT

Appendix B. Page 36 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Canned 378 0 0.002 ^ 0.75

Green Beans, Frozen 378 0 0.002 ^ 0.75

Peaches 707 0 0.050 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.020 ^ NT

TOTAL 6,070 1

Disulfoton sulfone oxygen analog (metabolite of Disulfoton)

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.010 ^ NT

Blueberries, Frozen 14 0 0.010 ^ NT

Celery 360 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.75

Green Beans, Fresh 757 0 0.005 ^ 0.75

Green Beans, Frozen 378 0 0.001 ^ 0.75

Sweet Corn, Fresh 56 0 0.005 ^ NT

Sweet Corn, Frozen 29 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 3,172 0

Disulfoton sulfoxide (metabolite of Disulfoton)

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Celery 708 0 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.002 ^ 0.75

Green Beans, Fresh 757 0 0.001 ^ 0.75

Green Beans, Frozen 378 0 0.002 ^ 0.75

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 5,513 0

Disulfoton sulfoxide oxygen analog (metabolite of Disulfoton)

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.010 ^ NT

Blueberries, Frozen 14 0 0.010 ^ NT

Celery 360 0 0.001 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Appendix B. Page 37 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Canned 378 0 0.001 ^ 0.75

Green Beans, Fresh 757 2 0.3 0.003 - 0.005 0.001 ^ 0.75

Green Beans, Frozen 378 0 0.001 ^ 0.75

Sweet Corn, Fresh 56 0 0.001 ^ NT

Sweet Corn, Frozen 29 0 0.001 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 3,172 2

Diuron (herbicide) 

Apples 177 0 0.002 ^ 0.1

Bananas 179 0 0.030 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.015 - 0.020 0.1

Blueberries, Frozen 19 0 0.015 - 0.020 0.1

Celery 708 0 0.008 - 0.020 NT

Cherries, Fresh 228 0 0.015 ^ NT

Cherries, Frozen 282 0 0.015 ^ NT

Grape Juice 531 0 0.003 ^ 0.05

Green Beans, Canned 378 0 0.008 ^ NT

Green Beans, Fresh 757 0 0.010 ^ NT

Green Beans, Frozen 378 0 0.008 ^ NT

Nectarines 681 0 0.020 ^ 0.1

Strawberries 176 0 0.010 ^ 0.1

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 134 0 0.010 ^ NT

Sweet Corn, Frozen 41 0 0.010 ^ NT

Tomatoes 177 0 0.008 ^ NT

Watermelon 358 0 0.002 ^ NT

TOTAL 6,162 0

DMST (4-dimethylaminosulphotosluidide) (metabolite of Tolyfluanid)

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Dodine (fungicide) 

Apples 177 1 0.6 0.017 ^ 0.010 ^ 5.0

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Grape Juice 531 0 0.010 ^ NT

Nectarines 681 1 0.1 0.025 ^ 0.015 ^ 5.0

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

Watermelon 358 0 0.010 ^ NT

TOTAL 2,990 2

Appendix B. Page 38 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Emamectin (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ 0.100

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ 0.02

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 1,243 0

Emamectin benzoate 2 (insecticide) 

Apples 177 0 0.010 ^ 0.025

Celery 360 0 0.001 ^ 0.100

Grape Juice 531 0 0.010 ^ 0.03

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Tomatoes 177 0 0.001 ^ 0.020

Watermelon 390 0 0.010 ^ 0.02

TOTAL 2,391 0

Endosulfan I (insecticide) 

Apples 177 1 0.6 0.040 ^ 0.010 ^ 1.0

Bananas 179 0 0.030 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.030 0.3

Blueberries, Frozen 19 0 0.010 - 0.030 0.3

Broccoli 712 1 0.1 0.008 ^ 0.005 ^ 3.0

Carrots 708 0 0.004 ^ 0.2

Celery 708 2 0.3 0.010 - 0.032 0.006 - 0.010 8.0

Cherries, Fresh 228 0 0.030 ^ 2.0

Cherries, Frozen 282 0 0.030 ^ 2.0

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.006 ^ 2.0

Green Beans, Fresh 757 0 0.012 - 0.12 2.0

Green Beans, Frozen 378 0 0.006 ^ 2.0

Nectarines 681 0 0.004 ^ 2.0

Peaches 707 0 0.005 ^ 2.0

Strawberries 176 0 0.010 ^ 2.0

Summer Squash 531 3 0.6 0.012 - 0.033 0.010 - 0.25 1.0

Sweet Corn, Fresh 134 0 0.010 ^ 0.2

Sweet Corn, Frozen 41 0 0.010 ^ 0.2

Tomatoes 177 3 1.7 0.008 ^ 0.005 ^ 1.0

Watermelon 390 0 0.010 ^ 1.0

TOTAL 8,582 10

Endosulfan II (isomer of Endosulfan)

Apples 177 1 0.6 0.078 ^ 0.015 ^ 1.0

Bananas 179 0 0.042 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.085 0.3

Blueberries, Frozen 19 0 0.010 - 0.085 0.3

Broccoli 712 0 0.005 ^ 3.0

Carrots 708 0 0.010 ^ 0.2

Celery 708 3 0.4 0.002 - 0.017 0.001 - 0.010 8.0

Cherries, Fresh 228 0 0.085 ^ 2.0

Appendix B. Page 39 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cherries, Frozen 282 0 0.085 ^ 2.0

Grape Juice 531 0 0.015 ^ NT

Green Beans, Canned 378 0 0.001 ^ 2.0

Green Beans, Fresh 757 1 0.1 0.004 ^ 0.003 - 0.025 2.0

Green Beans, Frozen 378 1 0.3 0.002 ^ 0.001 ^ 2.0

Nectarines 681 0 0.010 ^ 2.0

Peaches 707 0 0.005 ^ 2.0

Strawberries 176 0 0.010 ^ 2.0

Summer Squash 531 0 0.010 - 0.050 1.0

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.2

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.2

Tomatoes 177 13 7.3 0.002 - 0.027 0.001 ^ 1.0

Watermelon 390 0 0.015 ^ 1.0

TOTAL 8,582 19

Endosulfan sulfate (metabolite of Endosulfan)

Apples 177 1 0.6 0.015 ^ 0.005 ^ 1.0

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.040 0.3

Blueberries, Frozen 19 0 0.005 - 0.040 0.3

Broccoli 712 1 0.1 0.012 ^ 0.005 ^ 3.0

Carrots 708 12 1.7 0.003 - 0.008 0.002 ^ 0.2

Celery 693 2 0.3 0.009 - 0.075 0.005 - 0.024 8.0

Cherries, Fresh 228 0 0.040 ^ 2.0

Cherries, Frozen 282 0 0.040 ^ 2.0

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.012 ^ 2.0

Green Beans, Fresh 757 8 1.1 0.026 - 0.17 0.025 ^ 2.0

Green Beans, Frozen 378 1 0.3 0.018 ^ 0.012 ^ 2.0

Nectarines 681 0 0.002 ^ 2.0

Peaches 707 0 0.005 ^ 2.0

Strawberries 176 0 0.005 ^ 2.0

Summer Squash 531 56 10.5 0.005 - 0.15 0.005 - 0.050 1.0

Sweet Corn, Fresh 134 0 0.005 - 0.025 0.2

Sweet Corn, Frozen 41 0 0.005 - 0.025 0.2

Tomatoes 177 1 0.6 0.054 ^ 0.018 ^ 1.0

Watermelon 390 0 0.005 ^ 1.0

TOTAL 8,567 82

EPN (insecticide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Epoxiconazole (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Appendix B. Page 40 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

EPTC (herbicide) 

Bananas 179 0 0.035 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.035 ^ NT

Blueberries, Frozen 14 0 0.035 ^ NT

Carrots 708 2 0.3 0.15 - 0.16 0.004 ^ 0.1

Celery 360 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.035 ^ NT

Cherries, Frozen 282 0 0.035 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.08

Green Beans, Fresh 757 4 0.5 0.002 - 0.015 0.001 ^ 0.08

Green Beans, Frozen 378 0 0.001 - 0.003 0.08

Sweet Corn, Fresh 56 0 0.005 ^ 0.08

Sweet Corn, Frozen 29 0 0.005 ^ 0.08

TOTAL 3,703 6

Esfenvalerate+Fenvalerate Total (insecticide) 

Apples 177 2 1.1 0.006 - 0.009 0.005 ^ 1.0

Blueberries, Cultivated, Fresh 354 12 3.4 0.006 - 0.060 0.005 ^ 1.0

Blueberries, Frozen 5 0 0.005 ^ 1.0

Broccoli 712 3 0.4 0.008 - 0.038 0.005 - 0.010 1.0

Celery 708 0 0.002 - 0.008 0.05

Grape Juice 471 0 0.005 ^ 0.05

Green Beans, Canned 378 10 2.6 0.004 - 0.025 0.002 ^ 1.0

Green Beans, Fresh 726 27 3.7 0.008 - 0.12 0.008 - 0.075 1.0

Green Beans, Frozen 378 8 2.1 0.004 - 0.028 0.002 ^ 1.0

Peaches 707 46 6.5 0.007 - 0.10 0.005 ^ 3.0

Summer Squash 531 0 0.005 - 0.075 0.5

Sweet Corn, Fresh 56 0 0.005 ^ 0.1

Sweet Corn, Frozen 29 0 0.005 ^ 0.1

Tomatoes 177 4 2.3 0.009 - 0.032 0.008 ^ 0.5

Watermelon 390 0 0.005 ^ 0.5

TOTAL 5,799 112

Esfenvalerate (isomer of Fenvalerate)

Bananas 179 0 0.035 ^ 0.05

Blueberries, Cultivated, Fresh 334 9 2.7 0.036 - 0.10 0.035 ^ 1.0

Blueberries, Frozen 14 0 0.035 ^ 1.0

Carrots 708 0 0.015 ^ 0.5

Cherries, Fresh 228 0 0.035 ^ 3.0

Cherries, Frozen 282 8 2.8 0.037 - 0.12 0.035 ^ 3.0

Nectarines 681 10 1.5 0.025 ^ 0.015 ^ 3.0

Strawberries 176 0 0.005 ^ 0.05

Sweet Corn, Fresh 78 0 0.005 ^ 0.1

Sweet Corn, Frozen 12 0 0.005 ^ 0.1

TOTAL 2,692 27

Ethalfluralin (herbicide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.010 ^ NT

Appendix B. Page 41 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.010 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.020 0.05

Sweet Corn, Fresh 134 0 0.005 - 0.010 NT

Sweet Corn, Frozen 41 0 0.005 - 0.010 NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.005 ^ 0.05

TOTAL 5,774 0

Ethiofencarb (insecticide) 

Broccoli 712 0 0.010 ^ NT

Celery 359 0 0.002 - 0.008 NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,221 0

Ethiofencarb sulfone (metabolite of Ethiofencarb)

Strawberries 176 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 266 0

Ethiofencarb sulfoxide (metabolite of Ethiofencarb)

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 266 0

Ethion (insecticide) 

Apples 177 0 0.001 ^ NT

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.014 NT

Blueberries, Frozen 19 0 0.003 - 0.014 NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.014 ^ NT

Cherries, Frozen 282 0 0.014 ^ NT

Grape Juice 531 0 0.001 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Appendix B. Page 42 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 6,090 0

Ethion mono oxon (metabolite of Ethion)

Apples 177 0 0.001 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 708 0 0.002 - 0.003 NT

Grape Juice 531 0 0.001 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 3,634 0

Ethiprole (insecticide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Ethofumesate (herbicide) 

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Carrots 708 0 0.015 ^ 7.0

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 2,988 0

Ethoprop (insecticide) 

Apples 177 0 0.002 ^ NT

Bananas 179 1 0.6 0.003 ^ 0.002 ^ 0.02

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.003 NT

Blueberries, Frozen 19 0 0.002 - 0.003 NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.02

Appendix B. Page 43 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Fresh 757 0 0.001 ^ 0.02

Green Beans, Frozen 378 0 0.001 ^ 0.02

Nectarines 681 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.02

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.02

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 7,082 1

Ethylan (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Etofenprox (insecticide) 

Apples 177 0 0.025 ^ 5.0

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 5.0

Blueberries, Frozen 5 0 0.003 ^ 5.0

Celery 348 0 0.003 ^ 5.0

Grape Juice 531 0 0.025 ^ 5.0

Strawberries 176 0 0.003 ^ 5.0

Summer Squash 270 0 0.003 ^ 5.0

Sweet Corn, Fresh 134 0 0.003 - 0.010 5.0

Sweet Corn, Frozen 41 0 0.003 - 0.010 5.0

Tomatoes 177 0 0.002 ^ 5.0

Watermelon 390 0 0.025 ^ 5.0

TOTAL 2,603 0

Etoxazole (acaricide) 

Apples 177 0 0.005 ^ 0.20

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 0.50

Blueberries, Frozen 5 0 0.003 ^ 0.50

Broccoli 712 0 0.004 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 501 0 0.005 ^ 0.50

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh 757 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 4 0.6 0.015 - 0.031 0.001 ^ 1.0

Peaches 707 7 1 0.006 - 0.038 0.004 ^ 1.0

Strawberries 176 10 5.7 0.004 - 0.067 0.003 ^ 0.50

Summer Squash 531 0 0.003 - 0.005 0.02

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

Appendix B. Page 44 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 1 0.6 0.023 ^ 0.001 ^ 0.20

Watermelon 390 5 1.3 0.007 - 0.014 0.005 ^ 0.20

TOTAL 6,807 27

Etridiazole (fungicide) 

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.020 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.030 - 0.30 0.1

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.020 NT

Sweet Corn, Frozen 41 0 0.005 - 0.020 NT

TOTAL 4,541 0

Famoxadone (fungicide) 

Apples 177 0 0.025 ^ NT

Bananas 179 0 0.033 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 678 0 0.003 - 0.010 25

Grape Juice 531 0 0.025 ^ 2.5

Green Beans, Canned 378 0 0.003 - 0.012 NT

Green Beans, Frozen 378 0 0.003 - 0.006 NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 531 1 0.2 0.040 ^ 0.010 - 0.050 0.30

Sweet Corn, Fresh 134 0 0.010 - 0.050 NT

Sweet Corn, Frozen 41 0 0.010 - 0.050 NT

Tomatoes 177 10 5.6 0.010 - 0.032 0.008 - 0.015 1.0

Watermelon 390 0 0.025 ^ 0.30

TOTAL 4,129 11

Fenamidone (fungicide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.060 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.060 NT

Blueberries, Frozen 19 0 0.010 - 0.060 NT

Carrots 708 28 4 0.008 - 0.033 0.005 ^ 0.15

Celery 708 3 0.4 0.004 - 0.017 0.002 - 0.010 60

Cherries, Fresh 228 0 0.060 ^ NT

Cherries, Frozen 282 0 0.060 ^ NT

Grape Juice 531 0 0.005 ^ 1.0

Green Beans, Canned 378 0 0.002 ^ 0.80

Green Beans, Fresh 757 0 0.001 ^ 0.80

Green Beans, Frozen 378 0 0.002 ^ 0.80

Strawberries 176 0 0.005 ^ 0.02

Summer Squash 531 0 0.010 - 0.050 0.15

Sweet Corn, Fresh 134 0 0.001 - 0.005 NT

Appendix B. Page 45 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 41 0 0.001 - 0.005 NT

Tomatoes 177 1 0.6 0.004 ^ 0.002 ^ 1.0

Watermelon 390 0 0.005 ^ 0.15

TOTAL 6,482 32

Fenamiphos (insecticide) 

Bananas 179 0 0.020 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.010 NT

Blueberries, Frozen 19 0 0.003 - 0.010 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Grape Juice 531 0 0.050 ^ 0.1

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 221 0 0.050 ^ NT

TOTAL 5,744 0

Fenamiphos sulfone (metabolite of Fenamiphos)

Bananas 179 0 0.004 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.005 NT

Blueberries, Frozen 19 0 0.002 - 0.005 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.004 - 0.005 NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

Green Beans, Canned 378 0 0.004 ^ NT

Green Beans, Frozen 378 0 0.004 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.004 ^ NT

TOTAL 4,992 0

Fenamiphos sulfoxide (metabolite of Fenamiphos)

Bananas 179 0 0.004 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.008 - 0.020 NT

Blueberries, Frozen 19 0 0.008 - 0.020 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.004 - 0.020 NT

Cherries, Fresh 228 0 0.008 ^ NT

Cherries, Frozen 282 0 0.008 ^ NT

Grape Juice 531 0 0.050 ^ 0.1

Green Beans, Canned 378 0 0.004 ^ NT

Appendix B. Page 46 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Frozen 378 0 0.004 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

Tomatoes 177 0 0.004 ^ NT

Watermelon 221 0 0.050 ^ NT

TOTAL 5,744 0

Fenarimol (fungicide) 

Bananas 179 0 0.013 ^ 0.25

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.013 NT

Blueberries, Frozen 19 0 0.003 - 0.013 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.013 ^ 1.0

Cherries, Frozen 282 0 0.013 ^ 1.0

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.005 ^ NT

Green Beans, Frozen 378 0 0.002 - 0.008 NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.025 0.20

Sweet Corn, Fresh 134 0 0.003 - 0.005 NT

Sweet Corn, Frozen 41 0 0.003 - 0.005 NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 6,095 0

Fenazaquin (insecticide, acaricide)

Apples 177 0 0.005 ^ 0.2

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.005 ^ NT

Strawberries (V-2) 176 2 1.1 0.003 - 0.29 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 23 0 0.003 ^ NT

Sweet Corn, Frozen 7 0 0.003 ^ NT

Watermelon 358 0 0.005 ^ NT

TOTAL 2,249 2

Fenbuconazole (fungicide) 

Apples 177 4 2.3 0.008 - 0.015 0.005 ^ 0.4

Bananas 179 0 0.005 ^ 0.3

Blueberries, Cultivated, Fresh 688 20 2.9 0.005 - 0.38 0.005 - 0.010 0.3

Blueberries, Frozen 19 1 5.3 0.007 ^ 0.005 - 0.010 0.3

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.001 - 0.010 NT

Cherries, Fresh 228 6 2.6 0.007 - 0.44 0.005 ^ 1.0

Cherries, Frozen 282 136 48.2 0.005 - 0.48 0.005 ^ 1.0

Grape Juice 531 0 0.005 ^ 1.0

Green Beans, Canned 378 0 0.001 ^ NT

Appendix B. Page 47 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 676 30 4.4 0.003 - 0.047 0.002 ^ 1.0

Peaches 707 90 12.7 0.005 - 0.15 0.005 ^ 1.0

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes (V-5) 177 5 2.8 0.002 - 0.028 0.001 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 6,766 292

Fenbutatin oxide (insecticide, acaricide)

Nectarines 681 2 0.3 0.098 - 0.22 0.012 ^ 10.0

TOTAL 681 2

Fenchlorphos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Fenhexamid (fungicide) 

Apples 177 0 0.013 ^ NT

Bananas 179 0 0.011 ^ NT

Blueberries, Cultivated, Fresh 688 85 12.4 0.011 - 0.91 0.011 - 0.040 5.0

Blueberries, Frozen 19 3 15.8 0.011 - 0.14 0.011 - 0.040 5.0

Celery 708 0 0.009 - 0.040 NT

Cherries, Fresh 228 20 8.8 0.013 - 0.37 0.011 ^ 10.0

Cherries, Frozen 282 9 3.2 0.012 - 0.060 0.011 ^ 10.0

Grape Juice 531 4 0.8 0.040 - 0.047 0.013 ^ 4.0

Green Beans, Canned 378 0 0.009 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Green Beans, Frozen (V-1) 378 1 0.3 0.015 ^ 0.009 ^ NT

Nectarines 681 56 8.2 0.008 - 1.2 0.005 ^ 10.0

Strawberries 176 35 19.9 0.021 - 1.0 0.020 ^ 3.0

Summer Squash 531 0 0.010 - 0.040 NT

Sweet Corn, Fresh 134 0 0.005 - 0.020 NT

Sweet Corn, Frozen 41 0 0.005 - 0.020 NT

Tomatoes 177 5 2.8 0.015 - 0.096 0.009 ^ 2.0

Watermelon 390 0 0.013 ^ NT

TOTAL 6,455 218

Fenitrothion (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 708 0 0.003 - 0.005 NT

Green Beans, Canned 378 0 0.003 - 0.010 NT

Green Beans, Frozen 378 0 0.003 ^ NT

Strawberries 176 0 0.005 ^ NT

Appendix B. Page 48 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,536 0

Fenobucarb - BPMC (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Fenoxaprop ethyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Fenoxycarb (insecticide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 266 0

Fenpropathrin (insecticide) 

Apples 177 4 2.3 0.050 - 0.36 0.020 ^ 5.0

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 31 4.5 0.023 - 1.0 0.005 - 0.020 3.0

Blueberries, Frozen 19 0 0.005 - 0.020 3.0

Broccoli 712 0 0.005 ^ 3.0

Carrots 708 0 0.003 ^ NT

Celery 708 0 0.003 - 0.005 NT

Cherries, Fresh 228 47 20.6 0.027 - 1.0 0.020 ^ 5.0

Cherries, Frozen 282 35 12.4 0.020 - 1.1 0.020 ^ 5.0

Grape Juice 531 0 0.020 ^ 5.0

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Fresh (V-3) 757 3 0.4 0.064 - 0.092 0.050 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Nectarines 681 54 7.9 0.005 - 0.38 0.003 ^ 1.4

Peaches 707 45 6.4 0.006 - 0.80 0.005 ^ 1.4

Strawberries 176 45 25.6 0.005 - 0.51 0.005 ^ 2.0

Summer Squash 531 1 0.2 0.033 ^ 0.005 - 0.10 0.5

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Appendix B. Page 49 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 12 6.8 0.004 - 0.080 0.002 ^ 1.0

Watermelon 390 0 0.020 ^ 0.5

TOTAL 8,582 277

Fenpropidin (fungicide) 

Strawberries 176 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 266 0

Fenpropimorph (fungicide) 

Apples 177 0 0.001 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 3,760 0

Fenpyrazamine (fungicide) 

Strawberries 176 0 0.010 ^ 3

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 266 0

Fenpyroximate (acaricide) 

Apples 177 6 3.4 0.005 - 0.013 0.005 ^ 0.30

Broccoli 712 0 0.010 ^ NT

Celery 360 0 0.001 - 0.003 NT

Grape Juice 531 0 0.005 ^ 1.0

Green Beans, Canned 378 0 0.001 - 0.003 0.40

Green Beans, Frozen 378 0 0.001 ^ 0.40

Nectarines 681 38 5.6 0.002 - 0.053 0.001 ^ 2.0

Peaches 707 44 6.2 0.010 - 0.071 0.010 ^ 2.0

Strawberries 176 8 4.5 0.003 - 0.11 0.003 ^ 1.0

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 5 2.8 0.002 - 0.010 0.001 ^ 0.20

Watermelon 358 0 0.005 ^ 0.10

TOTAL 4,725 101

Fensulfothion (insecticide, fumigant)

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Appendix B. Page 50 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Fenthion (insecticide) 

Bananas 179 0 0.015 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.015 NT

Blueberries, Frozen 19 0 0.003 - 0.015 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.015 ^ NT

Cherries, Frozen 282 0 0.015 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.008 ^ NT

Watermelon 221 0 0.010 ^ NT

TOTAL 5,744 0

Fenthion oxygen analog sulfone (metabolite of Fenthion)

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.014 ^ NT

Blueberries, Frozen 14 0 0.014 ^ NT

Cherries, Fresh 228 0 0.014 ^ NT

Cherries, Frozen 282 0 0.014 ^ NT

Grape Juice 531 0 0.15 ^ NT

Watermelon 221 0 0.15 ^ NT

TOTAL 1,789 0

Fenthion oxygen analog sulfoxide (metabolite of Fenthion)

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.014 ^ NT

Blueberries, Frozen 14 0 0.014 ^ NT

Cherries, Fresh 228 0 0.014 ^ NT

Cherries, Frozen 282 0 0.014 ^ NT

Grape Juice 531 0 0.050 ^ NT

Watermelon 221 0 0.050 ^ NT

TOTAL 1,789 0

Fenthion sulfone (metabolite of Fenthion)

Bananas 179 0 0.030 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.12 ^ NT

Blueberries, Frozen 14 0 0.12 ^ NT

Cherries, Fresh 228 0 0.12 ^ NT

Cherries, Frozen 282 0 0.12 ^ NT

Grape Juice 531 0 0.075 ^ NT

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Appendix B. Page 51 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 221 0 0.075 ^ NT

TOTAL 2,055 0

Fenthion sulfoxide (metabolite of Fenthion)

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.020 ^ NT

Blueberries, Frozen 14 0 0.020 ^ NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.020 ^ NT

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 221 0 0.020 ^ NT

TOTAL 2,055 0

Fenuron (herbicide) 

Carrots 708 0 0.005 ^ NT

Nectarines 681 0 0.025 ^ NT

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,655 0

Fipronil (insecticide) 

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.020 NT

Blueberries, Frozen 19 0 0.003 - 0.020 NT

Broccoli 692 0 0.005 ^ NT

Celery 708 0 0.002 - 0.006 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Green Beans, Canned 378 0 0.002 - 0.012 NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 4,972 0

Fipronil sulfone - MB46136 (metabolite of Fipronil)

Apples 177 0 0.050 ^ NT

Grape Juice 531 0 0.050 ^ NT

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.050 ^ NT

TOTAL 1,364 0

Appendix B. Page 52 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Flonicamid (insecticide) 

Apples 177 3 1.7 0.012 - 0.039 0.006 ^ 0.20

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.030 1.5

Blueberries, Frozen 19 0 0.005 - 0.030 1.5

Broccoli 712 1 0.1 0.019 ^ 0.010 ^ 1.5

Carrots 708 0 0.004 ^ 0.60

Celery 708 64 9 0.002 - 0.074 0.001 - 0.030 4.0

Cherries, Fresh 228 0 0.005 ^ 0.60

Cherries, Frozen 282 0 0.005 ^ 0.60

Grape Juice 531 0 0.006 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Fresh (V-1) 757 1 0.1 0.10 ^ 0.10 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Nectarines 681 0 0.010 ^ 0.60

Peaches 707 0 0.010 ^ 0.60

Strawberries 176 41 23.3 0.033 - 0.48 0.030 ^ 1.5

Summer Squash 531 9 1.7 0.031 - 0.062 0.030 - 0.10 1.5

Sweet Corn, Fresh 134 0 0.030 - 0.10 NT

Sweet Corn, Frozen 41 0 0.030 - 0.10 NT

Tomatoes 177 41 23.2 0.002 - 0.34 0.001 ^ 0.40

Watermelon 390 2 0.5 0.030 - 0.10 0.006 ^ 1.5

TOTAL 8,582 162

Fluazifop (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.050 ^ NT

Blueberries, Frozen 5 0 0.050 ^ NT

Celery 348 0 0.050 ^ NT

Strawberries 176 0 0.050 ^ NT

Summer Squash 270 0 0.050 ^ NT

Sweet Corn, Fresh 78 0 0.050 ^ NT

Sweet Corn, Frozen 12 0 0.050 ^ NT

TOTAL 1,243 0

Fluazifop butyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Carrots 708 0 0.001 ^ 2.0

Celery 708 0 0.001 - 0.003 NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.001 ^ 0.05

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 3,925 0

Fluazinam (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 7.0

Blueberries, Frozen 5 0 0.003 ^ 7.0

Carrots 708 1 0.1 0.017 ^ 0.010 ^ 0.70

Appendix B. Page 53 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,951 1

Flubendiamide (insecticide) 

Apples 177 0 0.035 ^ 1.5

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 1.5

Blueberries, Frozen 5 0 0.003 ^ 1.5

Celery 348 17 4.9 0.003 - 0.023 0.003 ^ 11

Grape Juice 531 0 0.035 ^ 1.4

Green Beans, Fresh 757 22 2.9 0.003 - 0.034 0.003 ^ 0.50

Nectarines 681 17 2.5 0.005 - 0.086 0.003 ^ 1.6

Strawberries 176 4 2.3 0.005 - 0.079 0.003 ^ 1.5

Summer Squash 531 2 0.4 0.003 - 0.011 0.003 - 0.005 0.20

Sweet Corn, Fresh 134 1 0.7 0.003 ^ 0.003 ^ 0.01

Sweet Corn, Frozen 41 0 0.003 ^ 0.01

Watermelon 390 0 0.035 ^ 0.20

TOTAL 4,125 63

Fludioxonil (fungicide) 

Apples 177 30 16.9 0.025 - 1.0 0.025 ^ 5.0

Bananas 179 0 0.015 ^ NT

Blueberries, Cultivated, Fresh 688 113 16.4 0.010 - 0.63 0.010 - 0.062 2.0

Blueberries, Frozen 19 5 26.3 0.016 - 0.13 0.010 - 0.062 2.0

Broccoli 693 1 0.1 1.2 ^ 0.005 ^ 2.0

Carrots 708 0 0.027 ^ 0.75

Celery 708 0 0.010 - 0.012 15

Cherries, Fresh 228 59 25.9 0.031 - 2.0 0.031 ^ 5.0

Cherries, Frozen 282 6 2.1 0.054 - 0.40 0.031 ^ 5.0

Grape Juice 531 0 0.025 ^ 2.0

Green Beans, Canned 378 0 0.012 ^ 0.4

Green Beans, Fresh 757 0 0.050 ^ 0.4

Green Beans, Frozen 378 1 0.3 0.020 ^ 0.012 ^ 0.4

Nectarines 681 439 64.5 0.033 - 3.2 0.020 ^ 5.0

Peaches (X-1) 697 453 65 0.005 - 6.7 0.005 ^ 5.0

Strawberries 176 89 50.6 0.010 - 0.56 0.010 ^ 3.0

Summer Squash 531 0 0.010 - 0.060 0.45

Sweet Corn, Fresh 134 0 0.010 - 0.020 0.02

Sweet Corn, Frozen 41 0 0.010 - 0.020 0.02

Tomatoes 177 11 6.2 0.020 - 0.090 0.012 ^ 5.0

Watermelon 390 0 0.025 ^ 0.03

TOTAL 8,553 1,207

Flufenacet (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Appendix B. Page 54 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.05

TOTAL 1,328 0

Flufenoxuron (insecticide) 

Apples 177 0 0.001 ^ 0.50

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Grape Juice 531 0 0.002 ^ 0.70

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 2,341 0

Flufenpyr ethyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Flumetsulam (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Flumiclorac pentyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Flumioxazin (herbicide) 

Apples 177 0 0.010 ^ 0.02

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 0.02

Blueberries, Frozen 19 0 0.010 - 0.020 0.02

Celery 708 0 0.002 - 0.020 0.02

Appendix B. Page 55 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cherries, Fresh 228 0 0.010 ^ 0.02

Cherries, Frozen 282 0 0.010 ^ 0.02

Grape Juice 531 0 0.010 ^ 0.02

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.080 ^ NT

Green Beans, Frozen 378 0 0.002 - 0.005 NT

Nectarines 681 0 0.023 ^ 0.02

Strawberries 176 0 0.020 ^ 0.07

Summer Squash 531 0 0.020 - 0.18 0.03

Sweet Corn, Fresh 134 0 0.010 - 0.020 NT

Sweet Corn, Frozen 41 0 0.010 - 0.020 NT

Tomatoes 177 0 0.002 ^ 0.02

Watermelon 390 0 0.010 ^ 0.03

TOTAL 6,455 0

Fluometuron (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.010 NT

Sweet Corn, Frozen 41 0 0.003 - 0.010 NT

TOTAL 1,328 0

Fluopicolide (fungicide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.013 NT

Blueberries, Frozen 19 0 0.003 - 0.013 NT

Carrots 708 38 5.4 0.010 - 0.051 0.006 ^ 0.15

Celery 708 16 2.3 0.003 - 0.012 0.002 - 0.003 25

Cherries, Fresh 228 0 0.013 ^ NT

Cherries, Frozen 282 0 0.013 ^ NT

Grape Juice 531 0 0.015 ^ 2.0

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh (V-1) 757 1 0.1 0.052 ^ 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 19 3.6 0.004 - 0.090 0.003 - 0.010 0.50

Sweet Corn, Fresh 134 0 0.002 - 0.003 NT

Sweet Corn, Frozen 41 0 0.002 - 0.003 NT

Tomatoes 177 4 2.3 0.003 - 0.010 0.002 ^ 1.60

Watermelon 390 13 3.3 0.005 - 0.031 0.005 - 0.015 0.50

TOTAL 6,482 91

Fluopyram (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ 1.5

Summer Squash 270 0 0.003 ^ NT

Appendix B. Page 56 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 134 0 0.002 - 0.003 1.5

Sweet Corn, Frozen 41 0 0.002 - 0.003 1.5

TOTAL 1,328 0

Fluoxastrobin (fungicide) 

Bananas 179 0 0.025 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.013 1.9

Blueberries, Frozen 19 0 0.003 - 0.013 1.9

Broccoli (V-3) 712 3 0.4 0.016 - 0.081 0.002 ^ NT

Celery 708 0 0.001 - 0.004 4.0

Cherries, Fresh 228 0 0.013 ^ NT

Cherries, Frozen 282 0 0.013 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh 757 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.002 ^ NT

Strawberries 176 0 0.003 ^ 1.9

Summer Squash 531 0 0.003 - 0.005 0.50

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.01

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.01

Tomatoes 177 0 0.001 ^ 1.0

TOTAL 6,095 3

Fluquinconazole (fungicide) 

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 2,341 0

Fluridone (herbicide) 

Apples 177 0 0.001 ^ 0.1

Bananas 179 0 0.001 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.003 0.1

Blueberries, Frozen 19 0 0.002 - 0.003 0.1

Broccoli 712 0 0.010 ^ 0.1

Carrots 708 0 0.001 ^ 0.1

Celery 348 0 0.003 ^ 0.1

Cherries, Fresh 228 0 0.002 ^ 0.1

Cherries, Frozen 282 0 0.002 ^ 0.1

Grape Juice 531 0 0.001 ^ 0.1

Green Beans, Fresh 757 0 0.001 ^ 0.1

Nectarines 681 0 0.001 ^ 0.1

Peaches 707 0 0.010 ^ 0.1

Strawberries 176 0 0.003 ^ 0.1

Summer Squash 531 0 0.003 - 0.005 0.1

Sweet Corn, Fresh 134 0 0.003 - 0.025 0.1

Appendix B. Page 57 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 41 0 0.003 - 0.025 0.1

Watermelon 390 0 0.001 ^ 0.1

TOTAL 7,289 0

Fluroxypyr (herbicide metabolite)

Blueberries, Cultivated, Fresh 354 0 0.050 ^ NT

Blueberries, Frozen 5 0 0.050 ^ NT

Celery 348 0 0.050 ^ NT

Strawberries 176 0 0.050 ^ NT

Summer Squash 270 0 0.050 ^ NT

Sweet Corn, Fresh 78 0 0.050 ^ 0.02

Sweet Corn, Frozen 12 0 0.050 ^ 0.02

TOTAL 1,243 0

Flusilazole (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.008 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.008 NT

Blueberries, Frozen 19 0 0.003 - 0.008 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.008 ^ NT

Cherries, Frozen 282 0 0.008 ^ NT

Grape Juice 531 0 0.010 ^ NT

Nectarines 681 0 0.003 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 5,478 0

Fluthiacet methyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.010

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.010

TOTAL 1,328 0

Flutolanil (fungicide) 

Apples 177 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Appendix B. Page 58 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 2,341 0

Flutriafol (fungicide) 

Apples 177 0 0.010 ^ 0.40

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ 1.5

Strawberries 176 0 0.005 ^ 1.5

Summer Squash 270 0 0.010 ^ 0.30

Sweet Corn, Fresh 134 0 0.005 ^ 0.01

Sweet Corn, Frozen 41 0 0.005 ^ 0.01

Watermelon 390 0 0.010 ^ 0.30

TOTAL 2,426 0

Fluvalinate (insecticide) 

Apples 177 0 0.050 ^ NT

Bananas 179 0 0.036 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.035 NT

Blueberries, Frozen 19 0 0.010 - 0.035 NT

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.007 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.035 ^ NT

Cherries, Frozen 282 0 0.035 ^ NT

Grape Juice 531 0 0.050 ^ NT

Green Beans, Fresh 726 0 0.015 - 0.15 NT

Nectarines 681 0 0.007 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 531 0 0.010 - 0.30 NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 NT

Sweet Corn, Frozen 41 0 0.005 - 0.010 NT

Watermelon 390 0 0.050 ^ NT

TOTAL 7,258 0

Fluxapyroxad (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 7.0

Blueberries, Frozen 5 0 0.003 ^ 7.0

Celery 348 0 0.003 ^ 30

Green Beans, Fresh 757 6 0.8 0.005 - 0.011 0.005 ^ 2.0

Nectarines 681 9 1.3 0.007 - 0.12 0.002 ^ 2.0

Strawberries 176 11 6.2 0.006 - 0.73 0.003 ^ 4.0

Summer Squash 270 0 0.003 ^ 0.50

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.15

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.15

Tomatoes 177 10 5.6 0.002 - 0.024 0.001 ^ 0.7

TOTAL 2,943 36

Appendix B. Page 59 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Folpet (fungicide) 

Apples 177 0 0.030 ^ 5.0

Nectarines 681 0 0.064 ^ NT

Peaches 707 0 0.015 ^ NT

Watermelon 390 0 0.030 ^ 3.0

TOTAL 1,955 0

Fomesafen (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ 0.025

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Fonofos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.003 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 3,955 0

Forchlorfenuron (plant growth regulator) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 0.01

Blueberries, Frozen 5 0 0.003 ^ 0.01

Celery 348 0 0.003 ^ NT

Nectarines 681 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 2,631 0

Formetanate hydrochloride (insecticide) 

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 ^ NT

Blueberries, Frozen 19 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Nectarines 681 9 1.3 0.050 ^ 0.030 ^ 0.40

Peaches 681 0 0.010 ^ 0.40

Appendix B. Page 60 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 3,642 9

Fosthiazate (nematicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Furalaxyl (fungicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Halosulfuron (herbicide) 

Bananas 179 0 0.099 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.050 ^ 0.05

Blueberries, Frozen 14 0 0.050 ^ 0.05

Cherries, Fresh 228 0 0.050 ^ NT

Cherries, Frozen 282 0 0.050 ^ NT

Green Beans, Fresh 757 0 0.005 ^ NT

Summer Squash 261 0 0.050 ^ 0.5

Sweet Corn, Fresh 56 0 0.005 ^ 0.05

Sweet Corn, Frozen 29 0 0.005 ^ 0.05

TOTAL 2,140 0

Halosulfuron methyl 3 (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ 0.05

Blueberries, Frozen 5 0 0.020 ^ 0.05

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.020 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ 0.5

Sweet Corn, Fresh 78 0 0.020 ^ 0.05

Sweet Corn, Frozen 12 0 0.020 ^ 0.05

TOTAL 2,662 0

Haloxyfop (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Appendix B. Page 61 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Heptenophos (insecticide, acaricide)

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Hexaconazole (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.020 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 2,662 0

Hexazinone (herbicide) 

Bananas 179 0 0.004 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.002 ^ 0.6

Blueberries, Frozen 14 0 0.002 ^ 0.6

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

TOTAL 1,037 0

Hexythiazox (insecticide, acaricide)

Apples 177 0 0.002 ^ 0.4

Bananas 179 0 0.012 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.012 6

Blueberries, Frozen 19 0 0.005 - 0.012 6

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.012 ^ 1.0

Cherries, Frozen 282 0 0.012 ^ 1.0

Grape Juice 531 0 0.002 ^ 1

Green Beans, Fresh 726 0 0.30 ^ 0.3

Nectarines 681 13 1.9 0.058 ^ 0.035 ^ 1.0

Peaches 707 40 5.7 0.011 - 0.12 0.010 ^ 1.0

Strawberries 176 23 13.1 0.003 - 0.31 0.003 ^ 6

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.30 0.1

Sweet Corn, Frozen 41 0 0.003 - 0.30 0.1

Watermelon 390 0 0.002 ^ NT

TOTAL 6,289 76

Hydroprene (insect growth regulator) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ 0.2

Blueberries, Frozen 5 0 0.010 ^ 0.2

Appendix B. Page 62 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carrots 707 0 0.001 ^ 0.2

Celery 708 0 0.002 - 0.010 0.2

Grape Juice 30 0 0.10 ^ 0.2

Green Beans, Canned 378 0 0.002 ^ 0.2

Green Beans, Fresh 757 0 0.008 - 0.080 0.2

Green Beans, Frozen 378 0 0.002 ^ 0.2

Nectarines 681 0 0.001 ^ 0.2

Strawberries 176 0 0.010 ^ 0.2

Summer Squash 531 0 0.010 - 0.080 0.2

Sweet Corn, Fresh 134 0 0.010 ^ 0.2

Sweet Corn, Frozen 41 0 0.010 ^ 0.2

Tomatoes 177 0 0.002 ^ 0.2

TOTAL 5,057 0

3-Hydroxycarbofuran (metabolite of Carbofuran)

Apples 177 0 0.003 ^ NT

Bananas 179 0 0.002 ^ 0.1

Blueberries, Cultiv., Fresh (V-2) 688 2 0.3 0.002 - 0.003 0.002 - 0.010 NT

Blueberries, Frozen 19 0 0.002 - 0.010 NT

Broccoli 712 0 0.010 ^ NT

Carrots 708 0 0.050 ^ NT

Celery 708 0 0.001 - 0.010 NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

Grape Juice 531 0 0.003 ^ 0.4

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.050 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 1 0.6 0.003 ^ 0.003 ^ 0.5

Summer Squash 531 0 0.010 ^ 0.8

Sweet Corn, Fresh 134 0 0.002 - 0.003 1.0

Sweet Corn, Frozen 41 0 0.002 - 0.003 1.0

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.003 ^ 0.4

TOTAL 8,582 3

5-Hydroxythiabendazole (metabolite of Thiabendazole)

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ 5.0

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ 0.01

Sweet Corn, Frozen 12 0 0.003 ^ 0.01

TOTAL 1,243 0

Imazalil (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 41 22.9 0.005 - 0.068 0.005 ^ 3.0

Blueberries, Cultivated, Fresh 688 0 0.005 ^ NT

Blueberries, Frozen 19 0 0.005 ^ NT

Appendix B. Page 63 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines (V-33) 681 33 4.8 0.007 - 0.11 0.004 ^ NT

Peaches (V-10) 707 10 1.4 0.011 - 0.072 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,771 84

Imazapyr (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Imazaquin (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 1,243 0

Imazethapyr (herbicide) 

Apples 177 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Grape Juice 89 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

Watermelon 359 0 0.020 ^ NT

TOTAL 1,868 0

Appendix B. Page 64 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Imazosulfuron (herbicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Imidacloprid (insecticide) 

Apples 177 41 23.2 0.003 - 0.032 0.003 ^ 0.5

Bananas 179 0 0.009 ^ 0.50

Blueberries, Cultivated, Fresh 688 44 6.4 0.010 - 0.44 0.010 - 0.019 3.5

Blueberries, Frozen 19 0 0.010 - 0.019 3.5

Broccoli 712 30 4.2 0.010 - 0.45 0.010 ^ 3.5

Carrots 695 10 1.4 0.005 - 0.025 0.003 - 0.009 0.40

Celery 708 27 3.8 0.002 - 0.071 0.001 - 0.010 6.0

Cherries, Fresh 228 81 35.5 0.019 - 0.24 0.019 ^ 3.0

Cherries, Frozen 282 65 23 0.025 - 0.40 0.019 ^ 3.0

Grape Juice 531 14 2.6 0.003 - 0.035 0.003 ^ 1.5

Green Beans, Canned 378 0 0.003 ^ 4.0

Green Beans, Fresh 757 29 3.8 0.005 - 0.45 0.005 ^ 4.0

Green Beans, Frozen 378 0 0.003 ^ 4.0

Nectarines 681 22 3.2 0.017 - 0.23 0.010 ^ 3.0

Peaches 707 44 6.2 0.010 - 0.13 0.010 ^ 3.0

Strawberries 176 19 10.8 0.005 - 0.075 0.005 ^ 0.50

Summer Squash 531 84 15.8 0.010 - 0.35 0.010 - 0.030 0.5

Sweet Corn, Fresh 134 0 0.005 ^ 0.05

Sweet Corn, Frozen 41 0 0.005 ^ 0.05

Tomatoes 177 38 21.5 0.003 - 0.080 0.003 ^ 1.0

Watermelon 390 46 11.8 0.003 - 0.093 0.003 ^ 0.5

TOTAL 8,569 594

Imidacloprid urea (metabolite of Imidacloprid)

Bananas 179 0 0.022 ^ 0.50

Blueberries, Cultivated, Fresh 334 1 0.3 0.023 ^ 0.011 ^ 3.5

Blueberries, Frozen 14 0 0.011 ^ 3.5

Cherries, Fresh 228 0 0.011 ^ 3.0

Cherries, Frozen 282 0 0.011 ^ 3.0

TOTAL 1,037 1

Imiprothrin (insecticide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.090 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.091 NT

Blueberries, Frozen 19 0 0.010 - 0.091 NT

Carrots 708 0 0.009 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.091 ^ NT

Cherries, Frozen 282 0 0.091 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.030 ^ NT

Nectarines 681 0 0.009 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.010 - 0.040 NT

Appendix B. Page 65 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 41 0 0.010 - 0.040 NT

Watermelon 390 0 0.010 ^ NT

TOTAL 5,609 0

Indaziflam (herbicide) 

Apples 177 0 0.001 ^ 0.01

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.001 ^ 0.01

Nectarines 681 0 0.002 ^ 0.01

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 3,022 0

Indoxacarb (insecticide) 

Apples 177 0 0.020 ^ 1.0

Bananas 179 0 0.021 ^ NT

Blueberries, Cultivated, Fresh 688 9 1.3 0.010 - 0.046 0.010 - 0.021 1.5

Blueberries, Frozen 19 0 0.010 - 0.021 1.5

Broccoli 712 23 3.2 0.011 - 0.24 0.010 ^ 12

Celery 348 3 0.9 0.012 - 0.033 0.010 ^ 14

Cherries, Fresh 228 0 0.021 ^ 0.90

Cherries, Frozen 282 1 0.4 0.023 ^ 0.021 ^ 0.90

Grape Juice 531 0 0.020 ^ 2

Green Beans, Fresh 757 0 0.050 ^ 0.9

Nectarines 675 85 12.6 0.003 - 0.069 0.002 - 0.007 0.90

Peaches 707 47 6.6 0.010 - 0.066 0.010 ^ 0.90

Strawberries 176 0 0.010 ^ NT

Summer Squash 444 0 0.005 - 0.010 0.60

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.02

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.02

Watermelon 390 0 0.020 ^ 0.60

TOTAL 6,488 168

Ipconazole (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.010 ^ 0.01

Sweet Corn, Frozen 41 0 0.010 ^ 0.01

TOTAL 2,085 0

Iprodione (fungicide) 

Apples 177 0 0.040 ^ NT

Bananas 179 0 0.022 ^ NT

Blueberries, Cultivated, Fresh 688 55 8 0.005 - 2.7 0.005 - 0.022 15.0

Blueberries, Frozen 19 0 0.005 - 0.022 15.0

Appendix B. Page 66 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 712 1 0.1 0.063 ^ 0.005 ^ 25.0

Carrots 708 25 3.5 0.033 - 0.70 0.020 ^ 5.0

Celery 708 0 0.005 - 0.030 NT

Cherries, Fresh 228 49 21.5 0.022 - 2.6 0.022 ^ 20.0

Cherries, Frozen 282 76 27 0.022 - 0.63 0.022 ^ 20.0

Grape Juice 531 0 0.040 ^ 60.0

Green Beans, Canned 378 7 1.9 0.015 ^ 0.009 - 0.030 2.0

Green Beans, Fresh 757 0 0.15 ^ 2.0

Green Beans, Frozen 378 44 11.6 0.015 - 0.44 0.009 ^ 2.0

Nectarines 681 200 29.4 0.008 - 6.2 0.005 ^ 20.0

Peaches 707 190 26.9 0.006 - 7.2 0.005 ^ 20.0

Strawberries 176 3 1.7 0.020 - 2.6 0.005 ^ 15.0

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.15 NT

Sweet Corn, Frozen 41 0 0.005 - 0.15 NT

Tomatoes (V-1) 177 1 0.6 0.030 ^ 0.009 ^ NT

Watermelon 390 0 0.040 ^ NT

TOTAL 8,321 651

Iprovalicarb (fungicide) 

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 2,280 0

Isocarbophos (insecticide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Isofenphos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Isofenphos methyl (metabolite if Isofenphos)

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Appendix B. Page 67 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Isoprocarb (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 1,243 0

Isoproturon (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Isoxadifen ethyl (herbicide safener) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ 0.04

Sweet Corn, Frozen 41 0 0.005 ^ 0.04

TOTAL 351 0

Kresoxim-methyl (fungicide) 

Apples 177 0 0.010 ^ 0.5

Bananas 179 0 0.008 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.015 NT

Blueberries, Frozen 19 0 0.010 - 0.015 NT

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 228 0 0.015 ^ NT

Cherries, Frozen 282 0 0.015 ^ NT

Grape Juice 531 0 0.010 ^ 1.0

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.020 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.010 - 0.025 0.40

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ 0.40

TOTAL 5,774 0

Lactofen (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Appendix B. Page 68 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Lenacil (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 2,662 0

Leptophos oxygen analog (insecticide metabolite)

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Lindane - BHC gamma (insecticide) 

Apples 177 0 0.013 ^ NT

Bananas 179 0 0.044 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.045 0.5 AL

Blueberries, Frozen 19 0 0.003 - 0.045 0.5 AL

Carrots 708 0 0.001 ^ 0.5 AL

Celery 708 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.045 ^ NT

Cherries, Frozen 282 0 0.045 ^ NT

Grape Juice 531 0 0.013 ^ 0.5 AL

Green Beans, Canned 378 0 0.001 ^ 0.5 AL

Green Beans, Fresh 726 0 0.008 - 0.075 0.5 AL

Green Beans, Frozen 378 0 0.001 ^ 0.5 AL

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ 0.5

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.5

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.5

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.013 ^ NT

TOTAL 6,897 0

Linuron (herbicide) 

Apples 177 0 0.003 ^ NT

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.007 - 0.010 NT

Blueberries, Frozen 19 0 0.007 - 0.010 NT

Appendix B. Page 69 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 712 0 0.019 ^ NT

Carrots 708 174 24.6 0.017 - 0.65 0.010 ^ 1.0

Celery 708 93 13.1 0.005 - 0.043 0.003 - 0.010 0.5

Cherries, Fresh 228 0 0.007 ^ NT

Cherries, Frozen 282 0 0.007 ^ NT

Grape Juice 531 0 0.003 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Peaches 707 0 0.019 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.008 0.25

Sweet Corn, Frozen 41 0 0.005 - 0.008 0.25

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.003 ^ NT

TOTAL 6,883 267

Lufenuron (insecticide) 

Apples 147 0 0.020 ^ NT

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.020 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 390 0 0.020 ^ NT

TOTAL 3,348 0

Malathion (insecticide) 

Apples 177 0 0.002 ^ 8

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 94 13.7 0.005 - 0.67 0.005 ^ 8

Blueberries, Frozen 19 10 52.6 0.005 - 0.060 0.005 ^ 8

Broccoli 712 0 0.010 ^ 8

Carrots 708 0 0.001 ^ 8

Celery 708 87 12.3 0.002 - 0.11 0.001 - 0.005 8

Cherries, Fresh 228 6 2.6 0.006 - 0.015 0.005 ^ 8

Cherries, Frozen 282 6 2.1 0.007 - 0.012 0.005 ^ 8

Grape Juice 501 0 0.002 ^ 8

Green Beans, Canned 378 0 0.001 ^ 8

Green Beans, Fresh 757 0 0.002 ^ 8

Green Beans, Frozen 378 0 0.001 - 0.003 8

Nectarines 681 0 0.002 ^ 8

Peaches 707 1 0.1 0.012 ^ 0.010 ^ 8

Strawberries 176 19 10.8 0.005 - 0.15 0.005 ^ 8

Summer Squash 531 0 0.005 - 0.010 8

Sweet Corn, Fresh 134 0 0.005 ^ 2

Sweet Corn, Frozen 41 0 0.005 ^ 2

Appendix B. Page 70 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 1 0.6 0.007 ^ 0.003 ^ 8

Watermelon 390 0 0.002 ^ 8

TOTAL 8,552 224

Malathion oxygen analog (metabolite of Malathion)

Apples 177 0 0.002 ^ 8

Bananas 179 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 688 29 4.2 0.003 - 0.034 0.003 - 0.004 8

Blueberries, Frozen 19 2 10.5 0.005 ^ 0.003 - 0.004 8

Broccoli 712 0 0.010 ^ 8

Carrots 708 0 0.002 ^ 8

Celery 708 0 0.003 - 0.010 8

Cherries, Fresh 228 0 0.004 ^ 8

Cherries, Frozen 282 0 0.004 ^ 8

Grape Juice 501 0 0.002 ^ 8

Green Beans, Canned 378 0 0.010 ^ 8

Green Beans, Fresh 757 0 0.001 ^ 8

Green Beans, Frozen 378 0 0.010 ^ 8

Nectarines 681 0 0.002 ^ 8

Peaches 707 0 0.010 ^ 8

Strawberries 176 1 0.6 0.003 ^ 0.003 ^ 8

Summer Squash 531 0 0.003 - 0.005 8

Sweet Corn, Fresh 134 0 0.003 ^ 2

Sweet Corn, Frozen 41 0 0.003 ^ 2

Tomatoes 177 0 0.003 ^ 8

Watermelon 390 0 0.002 ^ 8

TOTAL 8,552 32

Mandipropamid (fungicide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.020 NT

Blueberries, Frozen 19 0 0.005 - 0.020 NT

Broccoli 712 8 1.1 0.006 - 0.11 0.005 ^ 3

Celery 708 1 0.1 0.010 ^ 0.005 - 0.015 20

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 19 3.6 0.002 - 0.004 0.002 ^ 1.4

Green Beans, Canned 378 0 0.015 ^ 0.90

Green Beans, Fresh 757 3 0.4 0.004 - 0.008 0.001 ^ 0.90

Green Beans, Frozen 378 0 0.015 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 3 0.6 0.007 - 0.030 0.005 ^ 0.6

Sweet Corn, Fresh 134 0 0.001 - 0.005 NT

Sweet Corn, Frozen 41 0 0.001 - 0.005 NT

Tomatoes 177 7 4 0.008 - 0.064 0.005 ^ 1.0

Watermelon 390 0 0.002 ^ 0.6

TOTAL 7,193 41

MCPA (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.25 ^ NT

Blueberries, Frozen 5 0 0.25 ^ NT

Appendix B. Page 71 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 348 0 0.25 ^ NT

Strawberries 176 0 0.25 ^ NT

Summer Squash 270 0 0.25 ^ NT

Sweet Corn, Fresh 78 0 0.25 ^ NT

Sweet Corn, Frozen 12 0 0.25 ^ NT

TOTAL 1,243 0

MCPB (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.25 ^ NT

Blueberries, Frozen 5 0 0.25 ^ NT

Celery 348 0 0.25 ^ NT

Strawberries 176 0 0.25 ^ NT

Summer Squash 270 0 0.25 ^ NT

Sweet Corn, Fresh 78 0 0.25 ^ NT

Sweet Corn, Frozen 12 0 0.25 ^ NT

TOTAL 1,243 0

Mecarbam (insecticide, acaricide)

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Mecoprop - MCPP (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.25 ^ NT

Blueberries, Frozen 5 0 0.25 ^ NT

Celery 348 0 0.25 ^ NT

Strawberries 176 0 0.25 ^ NT

Summer Squash 270 0 0.25 ^ NT

Sweet Corn, Fresh 78 0 0.25 ^ NT

Sweet Corn, Frozen 12 0 0.25 ^ NT

TOTAL 1,243 0

Mefenpyr diethyl (herbicide safener) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Mepanipyrim (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ 1.5

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Appendix B. Page 72 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Mesotrione (herbicide) 

Strawberries 176 0 0.040 ^ 0.01

Sweet Corn, Fresh 56 0 0.010 ^ 0.01

Sweet Corn, Frozen 29 0 0.010 ^ 0.01

TOTAL 261 0

Metaflumizone (insecticide) 

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.025 NT

Blueberries, Frozen 19 0 0.005 - 0.025 NT

Celery 348 0 0.020 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 2,280 0

Metalaxyl/Mefenoxam 4 (fungicide) 

Apples 177 0 0.001 ^ 0.2

Bananas 179 0 0.030 ^ NT

Blueberries, Cultivated, Fresh 688 3 0.4 0.003 - 0.027 0.003 - 0.030 2.0

Blueberries, Frozen 19 0 0.003 - 0.030 2.0

Broccoli 712 2 0.3 0.025 - 0.038 0.005 ^ 2.0

Carrots 708 38 5.4 0.008 - 0.034 0.005 ^ 0.5

Celery 708 0 0.001 - 0.003 5.0

Cherries, Fresh 228 0 0.030 ^ 1.0

Cherries, Frozen 282 0 0.030 ^ 1.0

Grape Juice 531 1 0.2 0.001 ^ 0.001 ^ 2.0

Green Beans, Canned 378 0 0.001 ^ 0.2

Green Beans, Fresh 757 29 3.8 0.001 - 0.041 0.001 ^ 0.2

Green Beans, Frozen 378 0 0.001 ^ 0.2

Nectarines 681 0 0.001 ^ 1.0

Peaches 707 0 0.005 ^ 1.0

Strawberries 176 25 14.2 0.003 - 0.25 0.003 ^ 10.0

Summer Squash 531 28 5.3 0.003 - 0.18 0.003 - 0.050 1.0

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.1

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.1

Tomatoes 177 8 4.5 0.002 - 0.006 0.001 ^ 1.0

Watermelon 390 37 9.5 0.001 - 0.049 0.001 ^ 1.0

TOTAL 8,582 171

Metaldehyde (molluscicide) 

Bananas 179 0 0.22 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.11 ^ 0.15

Blueberries, Frozen 14 0 0.11 ^ 0.15

Cherries, Fresh 228 0 0.11 ^ NT

Cherries, Frozen 282 0 0.11 ^ NT

Strawberries 176 0 0.10 ^ 6.25

Sweet Corn, Fresh 78 0 0.10 ^ 0.05

Sweet Corn, Frozen 12 0 0.10 ^ 0.05

TOTAL 1,303 0

Appendix B. Page 73 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Metconazole (fungicide) 

Blueberries, Cultivated, Fresh 354 7 2 0.011 - 0.14 0.010 ^ 0.40

Blueberries, Frozen 5 0 0.010 ^ 0.40

Celery 348 0 0.010 ^ NT

Nectarines 681 0 0.002 ^ 0.20

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.01

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.01

TOTAL 2,009 7

Methamidophos (insecticide) (also a metabolite of Acephate)

Apples 177 0 0.005 ^ 0.02

Bananas 179 0 0.008 ^ 0.02

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.033 0.02

Blueberries, Frozen 19 0 0.005 - 0.033 0.02

Broccoli 712 1 0.1 0.096 ^ 0.050 ^ 1.0

Carrots 708 0 0.024 ^ 0.02

Celery 708 69 9.7 0.004 - 0.049 0.001 - 0.005 1 5

Cherries, Fresh 228 0 0.033 ^ 0.02

Cherries, Frozen 282 0 0.033 ^ 0.02

Grape Juice 531 0 0.005 ^ 0.02

Green Beans, Canned 378 47 12.4 0.002 - 0.060 0.001 ^ 1 6

Green Beans, Fresh 757 124 16.4 0.020 - 0.63 0.020 ^ 1 6

Green Beans, Frozen 378 79 20.9 0.002 - 0.079 0.001 ^ 1 6

Nectarines 681 0 0.025 ^ 0.02

Peaches 707 0 0.050 ^ 0.02

Strawberries 176 0 0.005 ^ 0.02

Summer Squash 531 0 0.005 - 0.10 0.02

Sweet Corn, Fresh 134 0 0.005 - 0.020 0.02

Sweet Corn, Frozen 41 0 0.005 - 0.020 0.02

Tomatoes 177 0 0.001 ^ 2.0

Watermelon 390 2 0.5 0.009 - 0.018 0.005 ^ 0.02

TOTAL 8,582 322

Methidathion (insecticide) 

Apples 177 0 0.010 ^ 0.05

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.012 NT

Blueberries, Frozen 19 0 0.003 - 0.012 NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.002 - 0.003 NT

Cherries, Fresh 228 0 0.012 ^ 0.05

Cherries, Frozen 282 0 0.012 ^ 0.05

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Nectarines 681 0 0.001 - 0.003 0.05

Peaches 707 0 0.010 ^ 0.05

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Appendix B. Page 74 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,771 0

Methiocarb (insecticide)

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.001 - 0.010 NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 2,536 0

Methiocarb sulfone (metabolite of Methiocarb)

Apples 177 0 0.001 ^ NT

Grape Juice 531 0 0.001 ^ NT

Strawberries 176 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 1,364 0

Methiocarb sulfoxide (metabolite of Methiocarb)

Apples 177 0 0.001 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Grape Juice 531 0 0.001 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 2,341 0

Methomyl (insecticide) 

Apples 177 1 0.6 0.070 ^ 0.030 ^ 1

Bananas 179 0 0.013 ^ NT

Blueberries, Cultivated, Fresh 688 35 5.1 0.013 - 2.5 0.013 - 0.020 6

Blueberries, Frozen 19 0 0.013 - 0.020 6

Broccoli 712 2 0.3 0.012 - 0.15 0.010 ^ 3

Carrots 708 0 0.015 ^ 0.2

Celery 708 13 1.8 0.010 - 0.13 0.002 - 0.020 3

Cherries, Fresh 228 0 0.013 ^ NT

Cherries, Frozen 282 0 0.013 ^ NT

Grape Juice 473 0 0.030 ^ 5

Green Beans, Canned 378 0 0.002 ^ 2

Green Beans, Fresh 757 51 6.7 0.001 - 1.1 0.001 ^ 2

Appendix B. Page 75 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Frozen 378 0 0.002 ^ 2

Nectarines 681 0 0.003 - 0.010 5

Peaches 707 12 1.7 0.013 - 0.98 0.010 ^ 5

Strawberries (V-3) 176 3 1.7 0.011 - 0.055 0.010 ^ NT

Summer Squash 531 4 0.8 0.005 - 0.045 0.005 - 0.020 0.2

Sweet Corn, Fresh 134 1 0.7 0.001 ^ 0.001 - 0.010 0.1

Sweet Corn, Frozen 41 0 0.001 - 0.010 0.1

Tomatoes 177 0 0.002 ^ 1

Watermelon 358 1 0.3 0.066 ^ 0.030 ^ 0.2

TOTAL 8,492 123

Methoprene (insect growth regulator) 

Celery 360 0 0.015 ^ EX2

Green Beans, Canned 378 0 0.015 ^ EX2

Green Beans, Fresh 757 0 0.040 - 0.40 EX2

Green Beans, Frozen 378 0 0.015 ^ EX2

Sweet Corn, Fresh 56 0 0.025 ^ EX2

Sweet Corn, Frozen 29 0 0.025 ^ EX2

Tomatoes 177 0 0.015 ^ EX2

TOTAL 2,135 0

Methoxychlor Total (insecticide) 

Bananas 179 0 0.008 - 0.016 NT

Blueberries, Cultivated, Fresh 334 0 0.039 ^ NT

Blueberries, Frozen 14 0 0.039 ^ NT

Celery 360 0 0.001 ^ NT

Cherries, Fresh 228 0 0.039 ^ NT

Cherries, Frozen 282 0 0.039 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 2,330 0

Methoxychlor olefin (metabolite of Methoxychlor)

Celery 360 0 0.001 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 1,293 0

Methoxychlor p,p' (isomer of Methoxychlor)

Blueberries, Cultiv., Fresh (V-3) 354 3 0.8 0.005 - 0.007 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 - 0.020 NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 2,662 3

Appendix B. Page 76 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Methoxyfenozide (insecticide) 

Apples 177 7 4 0.004 - 0.024 0.003 ^ 2.0

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 65 9.4 0.009 - 0.58 0.005 - 0.006 3.0

Blueberries, Frozen 19 1 5.3 0.012 ^ 0.005 - 0.006 3.0

Broccoli 712 2 0.3 0.012 - 0.017 0.010 ^ 7.0

Carrots 708 1 0.1 0.007 ^ 0.004 ^ 0.90

Celery 708 165 23.3 0.002 - 0.077 0.001 - 0.005 25

Cherries, Fresh 228 18 7.9 0.006 - 0.067 0.006 ^ 3.0

Cherries, Frozen 282 1 0.4 0.007 ^ 0.006 ^ 3.0

Grape Juice 531 63 11.9 0.003 - 0.030 0.003 ^ 1.0

Green Beans, Canned 378 0 0.001 ^ 1.5

Green Beans, Fresh 757 24 3.2 0.002 - 0.081 0.002 ^ 1.5

Green Beans, Frozen 378 0 0.001 ^ 1.5

Nectarines 681 93 13.7 0.003 - 0.099 0.002 ^ 3.0

Peaches 707 106 15 0.010 - 0.20 0.010 ^ 3.0

Strawberries 176 41 23.3 0.003 - 0.21 0.003 ^ 2.0

Summer Squash 531 0 0.005 - 0.010 0.3

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.05

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.05

Tomatoes 177 15 8.5 0.002 - 0.015 0.001 ^ 2.0

Watermelon 390 0 0.003 ^ 0.3

TOTAL 8,582 602

Metolachlor (herbicide) 

Apples 177 0 0.001 ^ NT

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.007 0.15

Blueberries, Frozen 19 0 0.003 - 0.007 0.15

Broccoli 712 0 0.005 ^ 0.60

Carrots 708 5 0.7 0.002 - 0.059 0.001 ^ 0.40

Celery 708 12 1.7 0.002 - 0.008 0.001 - 0.003 0.10

Cherries, Fresh 228 0 0.007 ^ NT

Cherries, Frozen 282 0 0.007 ^ NT

Grape Juice 531 0 0.001 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.30

Green Beans, Fresh 757 1 0.1 0.006 ^ 0.005 ^ 0.30

Green Beans, Frozen 378 0 0.001 ^ 0.30

Peaches 692 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.10

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.10

Tomatoes 177 0 0.001 ^ 0.10

Watermelon 390 0 0.001 ^ 0.10

TOTAL 7,625 18

Metolcarb (insecticide, acaricide)

Strawberries 176 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 266 0

Appendix B. Page 77 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Metribuzin (herbicide) 

Apples 147 0 0.005 ^ NT

Bananas 179 0 0.004 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.016 NT

Blueberries, Frozen 19 0 0.005 - 0.016 NT

Carrots 708 1 0.1 0.003 ^ 0.002 ^ 0.3

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.016 ^ NT

Cherries, Frozen 282 0 0.016 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Green Beans, Frozen (V-1) 378 1 0.3 0.003 ^ 0.002 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ 0.05

Sweet Corn, Frozen 41 0 0.005 ^ 0.05

Tomatoes 177 0 0.002 ^ 0.1

Watermelon 390 0 0.005 ^ NT

TOTAL 6,191 2

Mevinphos (insecticide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.006 NT

Blueberries, Frozen 19 0 0.003 - 0.006 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.006 ^ NT

Cherries, Frozen 282 0 0.006 ^ NT

Grape Juice 531 0 0.002 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 NT

Sweet Corn, Frozen 41 0 0.003 - 0.005 NT

Tomatoes 177 0 0.005 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 6,932 0

MGK-264 (insecticide) 

Apples 177 0 0.10 ^ 5

Bananas 179 0 0.030 ^ 5

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.030 5

Blueberries, Frozen 19 0 0.003 - 0.030 5

Carrots 708 0 0.001 ^ 5

Celery 348 0 0.003 ^ 5

Cherries, Fresh 228 0 0.030 ^ 5

Cherries, Frozen 282 0 0.030 ^ 5

Grape Juice 531 0 0.10 ^ 5

Appendix B. Page 78 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Fresh 757 0 0.020 ^ 5

Nectarines 681 0 0.001 ^ 5

Strawberries 176 0 0.003 ^ 5

Summer Squash 531 0 0.003 - 0.040 5

Sweet Corn, Fresh 134 0 0.003 - 0.005 5

Sweet Corn, Frozen 41 0 0.003 - 0.005 5

Tomatoes 177 0 0.002 ^ 5

Watermelon 390 0 0.10 ^ 5

TOTAL 6,047 0

Monocrotophos (insecticide) 

Bananas 179 0 0.004 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.017 NT

Blueberries, Frozen 19 0 0.005 - 0.017 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.017 ^ NT

Cherries, Frozen (V-3) 282 3 1.1 0.023 - 0.057 0.017 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash (V-1) 270 1 0.4 0.46 ^ 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 3,699 4

Monolinuron (herbicide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 266 0

Myclobutanil (fungicide) 

Apples 177 4 2.3 0.003 - 0.005 0.003 ^ 0.5

Bananas 179 31 17.3 0.003 - 0.10 0.001 ^ 4.0

Blueberries, Cultivated, Fresh 688 0 0.001 - 0.010 NT

Blueberries, Frozen 19 0 0.001 - 0.010 NT

Broccoli 712 0 0.005 ^ 0.03

Carrots 708 2 0.3 0.003 ^ 0.002 ^ 0.03

Celery 708 12 1.7 0.002 - 0.012 0.001 - 0.010 0.03

Cherries, Fresh 228 67 29.4 0.001 - 0.16 0.001 ^ 5.0

Cherries, Frozen 282 26 9.2 0.001 - 0.086 0.001 ^ 5.0

Grape Juice 531 0 0.003 ^ 1.0

Green Beans, Canned 378 2 0.5 0.002 - 0.005 0.001 ^ 1.0

Green Beans, Fresh 757 22 2.9 0.006 - 0.11 0.005 ^ 1.0

Green Beans, Frozen 378 4 1.1 0.002 - 0.041 0.001 - 0.003 1.0

Nectarines 680 45 6.6 0.003 - 0.095 0.002 ^ 2.0

Peaches 707 38 5.4 0.005 - 0.14 0.005 ^ 2.0

Strawberries 176 31 17.6 0.012 - 0.23 0.010 ^ 0.50

Summer Squash 531 13 2.4 0.010 - 0.031 0.010 - 0.020 0.20

Sweet Corn, Fresh 134 0 0.010 ^ 0.03

Sweet Corn, Frozen 41 0 0.010 ^ 0.03

Appendix B. Page 79 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 14 7.9 0.003 - 0.051 0.003 ^ 0.30

Watermelon 390 1 0.3 0.003 ^ 0.003 ^ 0.20

TOTAL 8,581 312

Naled (insecticide) 

Apples 177 0 0.020 ^ 0.5

Carrots 708 0 0.025 ^ 0.5

Grape Juice 322 0 0.020 ^ 0.5

Nectarines 681 0 0.015 ^ 0.5

Watermelon 359 0 0.020 ^ 0.5

TOTAL 2,247 0

1-Naphthol (metabolite of Carbaryl)

Apples 177 1 0.6 0.48 ^ 0.015 ^ 12

Carrots 708 0 0.050 ^ 2.0

Green Beans, Fresh 726 9 1.2 0.018 - 0.29 0.006 - 0.060 10

Nectarines 681 1 0.1 0.13 ^ 0.015 ^ 10

Summer Squash 261 1 0.4 0.030 ^ 0.020 ^ 3.0

Sweet Corn, Fresh 56 0 0.010 ^ 0.1

Sweet Corn, Frozen 29 0 0.010 ^ 0.1

Watermelon 390 0 0.015 ^ 3.0

TOTAL 3,028 12

Napropamide (herbicide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.020 0.1

Blueberries, Frozen 19 0 0.005 - 0.020 0.1

Broccoli 712 0 0.010 ^ 0.1

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.005 ^ 0.1

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ 0.1

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ 0.1

Watermelon 390 0 0.005 ^ NT

TOTAL 6,090 0

Nicosulfuron (herbicide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.1

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.1

TOTAL 351 0

Appendix B. Page 80 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nitrapyrin (nitrification inhibitor) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ 0.1

Sweet Corn, Frozen 41 0 0.005 ^ 0.1

TOTAL 351 0

Nitrofen (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Norflurazon (herbicide) 

Apples 177 0 0.002 ^ 0.1

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 0.2

Blueberries, Frozen 19 0 0.005 - 0.010 0.2

Broccoli 712 0 0.010 ^ NT

Celery (V-2) 708 2 0.3 0.002 - 0.005 0.001 - 0.010 NT

Cherries, Fresh 228 0 0.005 ^ 0.1

Cherries, Frozen 282 0 0.005 ^ 0.1

Grape Juice 531 0 0.002 ^ 0.1

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.001 ^ 0.1

Peaches 707 0 0.010 ^ 0.1

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 6,771 2

Norflurazon desmethyl (metabolite of Norflurazon)

Apples 177 0 0.005 ^ 0.1

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 ^ 0.2

Blueberries, Frozen 19 0 0.010 ^ 0.2

Broccoli 712 0 0.010 ^ NT

Celery (V-4) 708 4 0.6 0.002 - 0.020 0.001 - 0.010 NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Grape Juice 531 0 0.005 ^ 0.1

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 680 0 0.005 ^ 0.1

Peaches 707 0 0.010 ^ 0.1

Strawberries 176 0 0.005 ^ NT

Appendix B. Page 81 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 6,770 4

Novaluron (insecticide) 

Bananas 179 0 0.010 ^ 0.01

Blueberries, Cultivated, Fresh 688 2 0.3 0.015 - 0.024 0.010 - 0.020 7.0

Blueberries, Frozen 19 0 0.010 - 0.020 7.0

Broccoli 712 0 0.010 ^ 0.50

Carrots 708 0 0.005 ^ 0.01

Celery 708 0 0.001 - 0.020 0.01

Cherries, Fresh 228 0 0.010 ^ 8.0

Cherries, Frozen 282 4 1.4 0.034 - 0.091 0.010 ^ 8.0

Green Beans, Canned 378 0 0.001 - 0.003 0.60

Green Beans, Fresh 757 0 0.050 ^ 0.60

Green Beans, Frozen 378 0 0.001 - 0.003 0.60

Nectarines 680 0 0.001 ^ 1.9

Peaches 707 3 0.4 0.012 - 0.051 0.010 ^ 1.9

Strawberries 176 27 15.3 0.020 - 0.10 0.020 ^ 0.45

Summer Squash 531 0 0.020 - 0.050 0.15

Sweet Corn, Fresh 134 0 0.020 - 0.050 0.05

Sweet Corn, Frozen 41 0 0.020 - 0.050 0.05

Tomatoes 177 2 1.1 0.002 - 0.006 0.001 ^ 1.0

TOTAL 7,483 38

Omethoate (insecticide) (also a metabolite of Dimethoate)

Apples 177 0 0.020 ^ NT

Bananas 179 0 0.019 ^ NT

Blueberries, Cultivated, Fresh 688 2 0.3 0.040 - 0.062 0.005 - 0.010 1.0

Blueberries, Frozen 19 0 0.005 - 0.010 1.0

Broccoli 712 0 0.010 ^ 2.0

Celery 708 44 6.2 0.005 - 0.043 0.002 - 0.008 2.0

Cherries, Fresh 228 1 0.4 0.15 ^ 0.010 ^ 2.0

Cherries, Frozen 282 26 9.2 0.012 - 0.19 0.010 ^ 2.0

Grape Juice 531 0 0.020 ^ NT

Green Beans, Canned 378 0 0.002 ^ 2.0

Green Beans, Fresh 757 41 5.4 0.006 - 0.34 0.006 ^ 2.0

Green Beans, Frozen 378 0 0.002 ^ 2.0

Nectarines 681 0 0.060 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries (V-1) 176 1 0.6 0.003 ^ 0.003 ^ NT

Summer Squash 531 0 0.005 - 0.015 NT

Sweet Corn, Fresh 134 0 0.003 - 0.006 NT

Sweet Corn, Frozen 41 0 0.003 - 0.006 NT

Tomatoes 177 4 2.3 0.004 - 0.009 0.002 ^ 2.0

Watermelon 390 0 0.020 ^ 1.0

TOTAL 7,874 119

Appendix B. Page 82 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Oryzalin (herbicide) 

Apples 177 0 0.020 ^ 0.05

Bananas 179 0 0.050 ^ NT

Blueberries, Cultivated, Fresh 688 1 0.1 0.021 ^ 0.020 - 0.099 0.05

Blueberries, Frozen 19 0 0.020 - 0.099 0.05

Broccoli 712 0 0.10 ^ NT

Celery 348 0 0.020 ^ NT

Cherries, Fresh 228 0 0.099 ^ 0.05

Cherries, Frozen 282 0 0.099 ^ 0.05

Grape Juice 531 0 0.020 ^ 0.05

Nectarines 679 2 0.3 0.017 ^ 0.010 - 0.033 0.05

Peaches 707 0 0.020 ^ 0.05

Strawberries 176 0 0.020 ^ 0.05

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

Watermelon 390 0 0.020 ^ NT

TOTAL 5,476 3

Oxadiazon (herbicide) 

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 2,341 0

Oxadixyl (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.003 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.003 ^ NT

TOTAL 3,955 0

Oxamyl (insecticide) 

Apples 177 0 0.003 ^ 2

Bananas 179 0 0.008 ^ 0.3

Blueberries, Cultivated, Fresh 688 0 0.004 - 0.010 NT

Blueberries, Frozen 19 0 0.004 - 0.010 NT

Broccoli 712 0 0.010 ^ NT

Appendix B. Page 83 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carrots 708 0 0.008 ^ 0.1

Celery 708 69 9.7 0.003 - 0.089 0.002 - 0.010 10.0

Cherries, Fresh 228 0 0.004 ^ NT

Cherries, Frozen 282 0 0.004 ^ NT

Grape Juice 531 0 0.003 ^ NT

Green Beans, Canned 378 0 0.006 ^ NT

Green Beans, Fresh (V-3) 757 3 0.4 0.011 - 0.14 0.002 ^ NT

Green Beans, Frozen 378 0 0.006 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries (V-1) 176 1 0.6 0.033 ^ 0.005 ^ NT

Summer Squash 531 17 3.2 0.011 - 1.3 0.010 ^ 2.0

Sweet Corn, Fresh 134 0 0.002 - 0.005 NT

Sweet Corn, Frozen 41 0 0.002 - 0.005 NT

Tomatoes 177 7 4 0.003 - 0.045 0.002 ^ 2

Watermelon 390 11 2.8 0.004 - 0.033 0.003 ^ 2.0

TOTAL 7,901 108

Oxamyl oxime (metabolite of Oxamyl)

Apples 177 2 1.1 0.009 - 0.015 0.006 ^ 2

Bananas 179 4 2.2 0.025 - 0.17 0.020 - 0.040 0.3

Blueberries, Cultivated, Fresh 688 0 0.020 - 0.040 NT

Blueberries, Frozen 19 0 0.020 - 0.040 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 2 0.6 0.026 - 0.027 0.020 ^ 10.0

Cherries, Fresh 228 0 0.040 ^ NT

Cherries, Frozen 282 0 0.040 ^ NT

Grape Juice 412 0 0.003 - 0.006 NT

Green Beans, Fresh (V-1) 757 1 0.1 0.060 ^ 0.050 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries (V-1) 176 1 0.6 0.020 ^ 0.010 ^ NT

Summer Squash 531 6 1.1 0.059 - 0.098 0.020 - 0.060 2.0

Sweet Corn, Fresh 134 0 0.010 - 0.050 NT

Sweet Corn, Frozen 41 0 0.010 - 0.050 NT

Watermelon 390 13 3.3 0.007 - 0.13 0.006 ^ 2.0

TOTAL 5,781 29

Oxydemeton methyl (insecticide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Broccoli 712 1 0.1 0.044 ^ 0.010 ^ 1.0

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.002 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ 2.0

Summer Squash 531 0 0.003 - 0.010 1.0

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.5

Appendix B. Page 84 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.5

Watermelon 390 0 0.002 ^ 0.2

TOTAL 5,900 1

Oxydemeton methyl sulfone (metabolite of Oxydemeton methyl)

Apples 177 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ 1.0

Celery 708 0 0.005 - 0.012 NT

Grape Juice 531 0 0.002 ^ NT

Green Beans, Canned 378 0 0.012 ^ NT

Green Beans, Fresh 757 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.012 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ 2.0

Summer Squash 531 0 0.005 - 0.010 1.0

Sweet Corn, Fresh 134 0 0.001 - 0.005 0.5

Sweet Corn, Frozen 41 0 0.001 - 0.005 0.5

Tomatoes 177 0 0.012 ^ NT

Watermelon 390 0 0.002 ^ 0.2

TOTAL 6,156 0

Oxyfluorfen (herbicide) 

Apples 177 0 0.050 ^ 0.05

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Broccoli 712 0 0.005 ^ 0.05

Celery (V-1) 708 1 0.1 0.002 ^ 0.001 - 0.010 NT

Grape Juice 531 0 0.050 ^ 0.05

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.006 ^ 0.05

Peaches 707 0 0.005 ^ 0.05

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.050 ^ NT

TOTAL 5,734 1

Paclobutrazol (plant growth regulator) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.007 - 0.010 NT

Blueberries, Frozen 19 0 0.007 - 0.010 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.007 ^ NT

Cherries, Frozen 282 0 0.007 ^ NT

Grape Juice 531 0 0.010 ^ NT

Nectarines 681 0 0.025 ^ NT

Appendix B. Page 85 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 5,478 0

Parathion (insecticide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.060 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.059 NT

Blueberries, Frozen 19 0 0.005 - 0.059 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.003 - 0.005 NT

Cherries, Fresh 228 0 0.059 ^ NT

Cherries, Frozen 282 0 0.059 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.003 - 0.010 NT

Green Beans, Frozen 378 0 0.003 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 - 0.020 NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 6,090 0

Parathion methyl (insecticide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.016 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.016 NT

Blueberries, Frozen 19 0 0.005 - 0.016 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.016 ^ NT

Cherries, Frozen 282 0 0.016 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.002 - 0.008 NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 - 0.020 NT

Sweet Corn, Fresh 134 0 0.005 ^ 1.0

Sweet Corn, Frozen 41 0 0.005 ^ 1.0

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,175 0

Parathion methyl oxygen analog (metabolite of Parathion methyl)

Apples 147 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Appendix B. Page 86 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.005 - 0.010 NT

Grape Juice 531 0 0.020 ^ NT

Green Beans, Canned 378 0 0.005 ^ NT

Green Beans, Frozen 378 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 1.0

Sweet Corn, Frozen 41 0 0.005 - 0.010 1.0

Tomatoes 177 0 0.005 ^ NT

Watermelon 390 0 0.020 ^ NT

TOTAL 3,689 0

Parathion oxygen analog (metabolite of Parathion)

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.003 - 0.010 NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 - 0.010 NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.003 ^ NT

TOTAL 2,536 0

Pebulate (herbicide) 

Broccoli 712 0 0.005 ^ NT

Peaches 707 0 0.005 ^ NT

TOTAL 1,419 0

Penconazole (fungicide) 

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.006 - 0.010 NT

Blueberries, Frozen 19 0 0.006 - 0.010 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.006 ^ NT

Cherries, Frozen 282 0 0.006 ^ NT

Nectarines 681 0 0.003 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 4,380 0

Pencycuron (fungicide) 

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Appendix B. Page 87 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cherries, Fresh 228 0 0.003 ^ NT

Cherries, Frozen 282 0 0.003 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 3,699 0

Pendimethalin (herbicide) 

Apples 177 0 0.050 ^ 0.10

Bananas 179 0 0.032 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.032 NT

Blueberries, Frozen 19 0 0.005 - 0.032 NT

Broccoli 712 2 0.3 0.007 - 0.009 0.005 - 0.010 0.1

Carrots 708 7 1 0.010 ^ 0.006 ^ 0.5

Celery (V-5) 708 5 0.7 0.002 - 0.009 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.032 ^ 0.10

Cherries, Frozen 282 0 0.032 ^ 0.10

Grape Juice 531 0 0.10 ^ 0.1

Green Beans, Canned 378 2 0.5 0.002 ^ 0.001 ^ 0.10

Green Beans, Fresh 757 0 0.040 ^ 0.10

Green Beans, Frozen 378 9 2.4 0.002 - 0.012 0.001 ^ 0.10

Nectarines 681 8 1.2 0.010 ^ 0.006 ^ 0.10

Peaches 707 1 0.1 0.005 ^ 0.005 ^ 0.10

Strawberries 176 0 0.005 ^ 0.10

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.040 0.1

Sweet Corn, Frozen 41 0 0.005 - 0.040 0.1

Tomatoes 177 0 0.001 ^ 0.10

Watermelon 390 0 0.050 ^ 0.10

TOTAL 8,321 34

Penflufen (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Green Beans, Fresh 757 0 0.001 ^ 0.01

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

TOTAL 2,085 0

Pentachloroaniline - PCA (metabolite of Quintozene)

Apples 177 0 0.004 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Broccoli 712 0 0.005 ^ 0.1

Carrots (V-20) 708 20 2.8 0.003 - 0.020 0.002 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 531 0 0.004 ^ NT

Green Beans, Canned 378 1 0.3 0.002 ^ 0.001 ^ 0.1

Appendix B. Page 88 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Fresh 726 0 0.060 ^ 0.1

Green Beans, Frozen 378 0 0.001 ^ 0.1

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash (V-6) 531 6 1.1 0.003 - 0.007 0.003 - 0.12 NT

Sweet Corn, Fresh 134 0 0.003 - 0.060 NT

Sweet Corn, Frozen 41 0 0.003 - 0.060 NT

Tomatoes 177 0 0.001 ^ 0.1

Watermelon (V-1) 390 1 0.3 0.006 ^ 0.004 ^ NT

TOTAL 6,833 28

Pentachlorobenzene - PCB (metabolite of Quintozene)

Apples 177 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ 0.1

Carrots (V-1) 708 1 0.1 0.020 ^ 0.001 ^ NT

Celery 708 0 0.005 - 0.008 NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Canned 378 0 0.008 - 0.015 0.1

Green Beans, Fresh 506 0 0.015 ^ 0.1

Green Beans, Frozen 378 0 0.008 ^ 0.1

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash (V-1) 531 1 0.2 0.008 ^ 0.005 - 0.010 NT

Sweet Corn, Fresh 134 0 0.005 - 0.015 NT

Sweet Corn, Frozen 41 0 0.005 - 0.015 NT

Tomatoes 177 0 0.010 ^ 0.1

Watermelon 390 0 0.005 ^ NT

TOTAL 6,613 2

Pentachlorophenyl methyl sulfide (metabolite of Quintozene)

Apples 177 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ 0.1

Carrots (V-1) 708 1 0.1 0.007 ^ 0.002 ^ NT

Celery 360 0 0.003 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Fresh 631 0 0.025 ^ 0.1

Peaches 707 0 0.005 ^ NT

Summer Squash 261 0 0.050 ^ NT

Sweet Corn, Fresh 56 0 0.025 ^ NT

Sweet Corn, Frozen 29 0 0.025 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 4,562 1

Penthiopyrad (fungicide) 

Blueberries, Cultivated, Fresh 295 0 0.003 ^ 3.0

Blueberries, Frozen 5 0 0.003 ^ 3.0

Carrots 708 31 4.4 0.003 - 0.034 0.002 ^ 3.0

Celery 319 11 3.4 0.006 - 0.076 0.003 ^ 30

Green Beans, Fresh 757 78 10.3 0.001 - 0.24 0.001 ^ 4.0

Nectarines 681 11 1.6 0.002 - 0.090 0.001 ^ 4.0

Strawberries 176 16 9.1 0.007 - 1.5 0.003 ^ 3.0

Appendix B. Page 89 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 531 2 0.4 0.007 - 0.20 0.003 - 0.005 0.60

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.01

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.01

Tomatoes 177 14 7.9 0.003 - 0.044 0.002 ^ 3.0

TOTAL 3,824 163

Permethrin Total (insecticide)

Broccoli 712 10 1.4 0.010 - 0.16 0.010 ^ 2.0

Carrots 708 0 0.004 ^ NT

Green Beans, Fresh (V-3) 757 3 0.4 0.073 - 0.11 0.040 ^ NT

Nectarines 681 17 2.5 0.007 - 0.72 0.004 ^ 1.0

Peaches 707 17 2.4 0.012 - 0.46 0.010 ^ 1.0

Summer Squash 261 0 0.040 ^ 1.5

Sweet Corn, Fresh 56 0 0.005 ^ 0.10

Sweet Corn, Frozen 29 0 0.005 ^ 0.10

TOTAL 3,911 47

Permethrin cis (isomer of Permethrin)

Apples 177 0 0.010 ^ 0.05

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.020 NT

Blueberries, Frozen 19 0 0.005 - 0.020 NT

Celery 708 257 36.3 0.002 - 0.23 0.001 - 0.005 5.0

Cherries, Fresh 228 1 0.4 0.14 ^ 0.020 ^ 4.0

Cherries, Frozen 282 27 9.6 0.020 - 0.39 0.020 ^ 4.0

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned (V-1) 378 1 0.3 0.004 ^ 0.001 ^ NT

Green Beans, Frozen (V-1) 378 1 0.3 0.002 ^ 0.001 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 1 0.4 0.020 ^ 0.005 ^ 1.5

Sweet Corn, Fresh 78 0 0.005 ^ 0.10

Sweet Corn, Frozen 12 0 0.005 ^ 0.10

Tomatoes 177 8 4.5 0.002 - 0.017 0.001 ^ 2.0

Watermelon 390 0 0.010 ^ 1.5

TOTAL 4,671 296

Permethrin trans (isomer of Permethrin)

Apples 177 0 0.010 ^ 0.05

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Celery 708 230 32.5 0.002 - 0.26 0.001 - 0.005 5.0

Cherries, Fresh 228 1 0.4 0.21 ^ 0.010 ^ 4.0

Cherries, Frozen 282 29 10.3 0.014 - 0.56 0.010 ^ 4.0

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned (V-1) 378 1 0.3 0.005 ^ 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 1 0.4 0.015 ^ 0.005 ^ 1.5

Sweet Corn, Fresh 78 0 0.005 ^ 0.10

Sweet Corn, Frozen 12 0 0.005 ^ 0.10

Appendix B. Page 90 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 9 5.1 0.002 - 0.020 0.001 ^ 2.0

Watermelon 390 0 0.010 ^ 1.5

TOTAL 4,671 271

Phenothrin (insecticide) 

Apples 177 0 0.050 ^ 0.01

Bananas 179 0 0.018 ^ 0.01

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.15 0.01

Blueberries, Frozen 19 0 0.005 - 0.15 0.01

Broccoli 712 0 0.005 ^ 0.01

Carrots 708 0 0.003 ^ 0.01

Celery 708 0 0.002 - 0.005 0.01

Cherries, Fresh 228 0 0.15 ^ 0.01

Cherries, Frozen 282 0 0.15 ^ 0.01

Grape Juice 531 0 0.050 ^ 0.01

Green Beans, Canned 378 0 0.002 ^ 0.01

Green Beans, Fresh 757 0 0.030 ^ 0.01

Green Beans, Frozen 378 0 0.002 ^ 0.01

Nectarines 681 0 0.003 ^ 0.01

Peaches 707 0 0.005 ^ 0.01

Strawberries 176 0 0.005 ^ 0.01

Summer Squash 531 0 0.005 - 0.030 0.01

Sweet Corn, Fresh 134 0 0.005 ^ 0.01

Sweet Corn, Frozen 41 0 0.005 ^ 0.01

Tomatoes 177 0 0.002 ^ 0.01

Watermelon 390 0 0.050 ^ 0.01

TOTAL 8,582 0

Phenthoate (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 708 0 0.001 - 0.003 NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 2,536 0

o-Phenylphenol (fungicide) 

Apples 177 2 1.1 0.005 - 0.007 0.005 ^ 25

Carrots 708 0 0.004 ^ 20

Grape Juice 531 0 0.005 ^ NT

Nectarines 681 2 0.3 0.007 ^ 0.004 ^ 5

Tomatoes 177 0 0.001 ^ 10

Watermelon 390 0 0.005 ^ NT

TOTAL 2,664 4

Phorate (insecticide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.042 ^ NT

Appendix B. Page 91 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.17 NT

Blueberries, Frozen 19 0 0.010 - 0.17 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 228 0 0.17 ^ NT

Cherries, Frozen 282 0 0.17 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.002 ^ 0.05

Green Beans, Fresh 757 0 0.060 ^ 0.05

Green Beans, Frozen 378 0 0.002 ^ 0.05

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.010 - 0.060 0.05

Sweet Corn, Frozen 41 0 0.010 - 0.060 0.05

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,932 0

Phorate oxygen analog (metabolite of Phorate)

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.05

Green Beans, Fresh 757 0 0.001 ^ 0.05

Green Beans, Frozen 378 0 0.001 ^ 0.05

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.005 0.05

Sweet Corn, Frozen 41 0 0.001 - 0.005 0.05

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 4,476 0

Phorate oxygen analog sulfone (metabolite of Phorate)

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.010 NT

Blueberries, Frozen 19 0 0.003 - 0.010 NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.002 ^ 0.05

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.05

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.05

TOTAL 3,122 0

Phorate oxygen analog sulfoxide (metabolite of Phorate)

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Appendix B. Page 92 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Green Beans, Fresh 757 0 0.002 ^ 0.05

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.05

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.05

TOTAL 3,122 0

Phorate sulfone (metabolite of Phorate)

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.030 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.030 NT

Blueberries, Frozen 19 0 0.005 - 0.030 NT

Celery 708 0 0.003 - 0.005 NT

Cherries, Fresh 228 0 0.030 ^ NT

Cherries, Frozen 282 0 0.030 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.003 ^ 0.05

Green Beans, Fresh 757 0 0.005 ^ 0.05

Green Beans, Frozen 378 0 0.003 - 0.010 0.05

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.05

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.05

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 5,513 0

Phorate sulfoxide (metabolite of Phorate)

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 ^ NT

Blueberries, Frozen 19 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.002 ^ 0.05

Green Beans, Fresh 757 0 0.001 ^ 0.05

Green Beans, Frozen 378 0 0.002 - 0.005 0.05

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.05

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.05

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,932 0

Appendix B. Page 93 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Phosalone (insecticide) 

Apples 177 0 0.001 ^ 10.0

Bananas 179 0 0.026 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.013 NT

Blueberries, Frozen 19 0 0.005 - 0.013 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Cherries, Fresh 228 0 0.013 ^ 15.0

Cherries, Frozen 282 0 0.013 ^ 15.0

Grape Juice 531 0 0.001 ^ 10.0

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ 15.0

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 6,090 0

Phosmet (insecticide) 

Apples 177 14 7.9 0.011 - 0.28 0.010 ^ 10

Bananas 179 0 0.049 ^ NT

Blueberries, Cultivated, Fresh 688 167 24.3 0.006 - 1.7 0.005 - 0.025 10

Blueberries, Frozen 19 4 21.1 0.018 - 0.29 0.005 - 0.025 10

Broccoli 712 0 0.005 ^ NT

Carrots (V-3) 708 3 0.4 0.017 ^ 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.025 ^ 10

Cherries, Frozen 282 6 2.1 0.025 - 0.26 0.025 ^ 10

Grape Juice 531 5 0.9 0.011 - 0.015 0.010 ^ 10

Green Beans, Fresh 757 0 0.010 ^ NT

Nectarines 681 31 4.6 0.083 - 0.27 0.050 ^ 5

Peaches 707 101 14.3 0.005 - 1.8 0.005 ^ 10

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.12 NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 NT

Sweet Corn, Frozen 41 0 0.005 - 0.010 NT

Watermelon 390 0 0.010 ^ NT

TOTAL 7,289 331

Phosmet oxygen analog (metabolite of Phosmet)

Apples 30 1 3.3 0.005 ^ 0.004 ^ 10

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 105 15.3 0.003 - 0.065 0.003 - 0.006 10

Blueberries, Frozen 19 3 15.8 0.003 - 0.037 0.003 - 0.006 10

Carrots 708 0 0.002 ^ NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.006 ^ 10

Cherries, Frozen 282 1 0.4 0.008 ^ 0.006 ^ 10

Green Beans, Fresh 757 0 0.001 ^ NT

Nectarines 677 9 1.3 0.002 - 0.004 0.001 ^ 5

Appendix B. Page 94 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.010 NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 NT

Sweet Corn, Frozen 41 0 0.001 - 0.003 NT

Watermelon 252 0 0.004 ^ NT

TOTAL 5,050 119

Phosphamidon (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.003 - 0.005 NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.003 ^ NT

TOTAL 3,955 0

Phoxim (insecticide) 

Bananas 179 0 0.049 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.024 NT

Blueberries, Frozen 19 0 0.003 - 0.024 NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.024 ^ NT

Cherries, Frozen 282 0 0.024 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 2,280 0

Picoxystrobin (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ 0.04

Sweet Corn, Frozen 41 0 0.005 ^ 0.04

TOTAL 1,328 0

Piperonyl butoxide (insecticide) 

Apples 177 0 0.005 ^ 8

Bananas 179 0 0.013 ^ EX3

Blueberries, Cultivated, Fresh 688 1 0.1 0.037 ^ 0.005 - 0.013 8

Blueberries, Frozen 19 0 0.005 - 0.013 8

Broccoli 712 0 0.005 ^ EX3

Carrots 708 0 0.003 ^ EX3

Celery 708 1 0.1 0.011 ^ 0.005 ^ EX3

Appendix B. Page 95 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cherries, Fresh 228 0 0.013 ^ 8

Cherries, Frozen 282 0 0.013 ^ 8

Grape Juice 531 0 0.005 ^ 8

Green Beans, Canned 378 0 0.005 ^ 8

Green Beans, Fresh 757 0 0.030 ^ 8

Green Beans, Frozen 378 0 0.005 ^ 8

Nectarines 681 0 0.003 ^ 8

Peaches 707 1 0.1 0.020 ^ 0.005 ^ 8

Strawberries 176 12 6.8 0.005 - 0.96 0.005 ^ EX3

Summer Squash 531 0 0.005 - 0.030 EX3

Sweet Corn, Fresh 134 0 0.005 - 0.025 EX3

Sweet Corn, Frozen 41 0 0.005 - 0.025 EX3

Tomatoes 177 13 7.3 0.005 - 0.29 0.003 ^ 8

Watermelon 390 0 0.005 ^ EX3

TOTAL 8,582 28

Pirimicarb (insecticide) 

Bananas 179 0 0.003 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.010 NT

Blueberries, Frozen 19 0 0.002 - 0.010 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.001 - 0.010 NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen (V-2) 282 2 0.7 0.002 - 0.003 0.002 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen (V-1) 378 1 0.3 0.002 ^ 0.001 ^ NT

Nectarines 681 0 0.005 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 5,673 3

Pirimicarb desmethyl (metabolite of Pirimicarb)

Bananas 179 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.001 - 0.003 NT

Blueberries, Frozen 19 0 0.001 - 0.003 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.001 ^ NT

Cherries, Frozen 282 0 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 3,699 0

Pirimiphos methyl (insecticide) 

Apples 177 0 0.001 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Appendix B. Page 96 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 531 0 0.001 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 5,053 0

Prallethrin (insecticide) 

Apples 177 0 0.010 ^ 1.0

Bananas 179 0 0.10 ^ 1.0

Blueberries, Cultivated, Fresh 629 0 0.020 - 0.10 1.0

Blueberries, Frozen 19 0 0.020 - 0.10 1.0

Carrots 708 0 0.015 ^ 1.0

Celery 319 0 0.020 ^ 1.0

Cherries, Fresh 228 0 0.10 ^ 1.0

Cherries, Frozen 282 0 0.10 ^ 1.0

Green Beans, Fresh 757 0 0.20 ^ 1.0

Nectarines 681 0 0.015 ^ 1.0

Strawberries 176 0 0.020 ^ 1.0

Summer Squash 531 0 0.020 - 0.10 1.0

Sweet Corn, Fresh 134 0 0.010 - 0.020 1.0

Sweet Corn, Frozen 41 0 0.010 - 0.020 1.0

Watermelon 390 0 0.010 ^ 1.0

TOTAL 5,251 0

Prochloraz (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.010 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 2,662 0

Procymidone (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 ^ NT

Blueberries, Frozen 19 0 0.010 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Appendix B. Page 97 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cherries, Frozen 282 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ 5.0

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 4,797 0

Profenofos (insecticide) 

Apples 177 0 0.075 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 531 0 0.075 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.075 ^ NT

TOTAL 5,138 0

Profluralin (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Profoxydim (herbicide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 266 0

Promecarb (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,243 0

Appendix B. Page 98 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Prometryn (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Carrots 708 2 0.3 0.005 - 0.011 0.003 ^ 0.45

Celery 708 15 2.1 0.002 - 0.015 0.001 - 0.003 0.50

Green Beans, Canned 378 0 0.001 ^ 0.05

Green Beans, Frozen 378 0 0.001 ^ 0.05

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 3,244 17

Pronamide (herbicide) 

Apples 177 0 0.002 ^ 0.1

Bananas 179 0 0.012 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.012 0.05

Blueberries, Frozen 19 0 0.003 - 0.012 0.05

Broccoli (V-1) 712 1 0.1 0.006 ^ 0.005 ^ NT

Celery (V-5) 708 5 0.7 0.002 - 0.005 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.012 ^ 0.1

Cherries, Frozen 282 0 0.012 ^ 0.1

Grape Juice 531 0 0.002 ^ 0.1

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh 757 0 0.005 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.001 ^ 0.1

Peaches 707 0 0.005 ^ 0.1

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 NT

Sweet Corn, Frozen 41 0 0.003 - 0.005 NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 7,613 6

Propachlor (herbicide) 

Celery 360 0 0.001 - 0.003 NT

Green Beans, Canned (V-1) 378 1 0.3 0.002 ^ 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 1,293 1

Propamocarb (fungicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Appendix B. Page 99 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Propamocarb hydrochloride 7 (fungicide) 

Apples 177 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Broccoli (V-2) 712 2 0.3 0.010 - 0.024 0.010 ^ NT

Celery (V-3) 348 3 0.9 0.014 - 0.025 0.010 ^ NT

Grape Juice 473 0 0.003 ^ NT

Green Beans, Fresh (V-17) 757 17 2.2 0.001 - 0.11 0.001 ^ NT

Peaches 707 0 0.010 ^ NT

Summer Squash 531 42 7.9 0.006 - 0.57 0.005 - 0.010 1.5

Sweet Corn, Fresh 31 0 0.001 ^ NT

Sweet Corn, Frozen 25 0 0.001 ^ NT

Watermelon 390 13 3.3 0.002 - 0.007 0.002 ^ 1.5

TOTAL 4,510 77

Propanil (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 1,243 0

Propaquizafop (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Propargite (insecticide) 

Apples 177 0 0.050 ^ NT

Bananas 179 0 0.018 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.036 NT

Blueberries, Frozen 19 0 0.005 - 0.036 NT

Broccoli 712 0 0.020 ^ NT

Celery 708 0 0.005 - 0.006 NT

Cherries, Fresh 228 0 0.036 ^ NT

Cherries, Frozen (V-3) 282 3 1.1 0.049 - 0.25 0.036 ^ NT

Grape Juice 531 0 0.050 ^ 10.0

Green Beans, Canned 378 0 0.006 ^ NT

Green Beans, Frozen 378 0 0.006 ^ NT

Nectarines 681 3 0.4 0.10 - 0.37 0.030 ^ 4.0

Peaches (V-1) 707 1 0.1 0.029 ^ 0.020 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.1

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.1

Appendix B. Page 100 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 0 0.006 ^ NT

Watermelon 390 0 0.050 ^ NT

TOTAL 6,856 7

Propetamphos (insecticide) 

Apples 147 0 0.010 ^ 0.1

Bananas 179 0 0.010 ^ 0.1

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 0.1

Blueberries, Frozen 19 0 0.005 - 0.010 0.1

Broccoli 712 0 0.010 ^ 0.1

Carrots 708 0 0.010 ^ 0.1

Celery 708 0 0.002 - 0.005 0.1

Cherries, Fresh 228 0 0.010 ^ 0.1

Cherries, Frozen 282 0 0.010 ^ 0.1

Grape Juice 531 0 0.010 ^ 0.1

Green Beans, Canned 378 0 0.002 ^ 0.1

Green Beans, Fresh 757 0 0.10 ^ 0.1

Green Beans, Frozen 378 0 0.002 - 0.005 0.1

Nectarines 681 0 0.001 - 0.003 0.1

Peaches 707 0 0.010 ^ 0.1

Strawberries 176 0 0.005 ^ 0.1

Summer Squash 531 0 0.005 - 0.050 0.1

Sweet Corn, Fresh 134 0 0.005 ^ 0.1

Sweet Corn, Frozen 41 0 0.005 ^ 0.1

Tomatoes 177 0 0.002 ^ 0.1

Watermelon 390 0 0.010 ^ 0.1

TOTAL 8,552 0

Propham (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Propiconazole (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.018 ^ 0.2

Blueberries, Cultivated, Fresh 688 1 0.1 0.068 ^ 0.010 - 0.018 1.0

Blueberries, Frozen 19 0 0.010 - 0.018 1.0

Broccoli 712 0 0.010 ^ NT

Carrots 708 0 0.020 ^ 0.25

Celery 708 182 25.7 0.010 - 0.13 0.008 - 0.010 5.0

Cherries, Fresh 228 14 6.1 0.018 - 0.15 0.018 ^ 4.0

Cherries, Frozen 282 13 4.6 0.030 - 0.17 0.018 ^ 4.0

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.008 ^ 0.70

Green Beans, Fresh 757 1 0.1 0.019 ^ 0.005 ^ 0.70

Green Beans, Frozen 378 0 0.008 ^ 0.70

Nectarines 681 235 34.5 0.007 - 0.57 0.004 ^ 4.0

Appendix B. Page 101 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 707 258 36.5 0.010 - 1.2 0.010 ^ 4.0

Strawberries 176 7 4 0.018 - 0.30 0.010 ^ 1.3

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.1

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.1

Tomatoes 177 0 0.008 ^ 3.0

Watermelon 390 0 0.010 ^ NT

TOTAL 8,321 711

Proquinazid (fungicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Prosulfuron (herbicide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.01

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.01

TOTAL 351 0

Prothioconazole (fungicide) 

Green Beans, Fresh 757 0 0.50 ^ NT

Strawberries 176 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ 0.04

Sweet Corn, Frozen 12 0 0.020 ^ 0.04

TOTAL 1,023 0

Prothiofos (insecticide) 

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.20 NT

Blueberries, Frozen 19 0 0.010 - 0.20 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.020 - 0.10 NT

Cherries, Frozen 282 0 0.020 - 0.10 NT

Nectarines 681 0 0.025 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 23 0 0.010 ^ NT

Sweet Corn, Frozen 7 0 0.010 ^ NT

TOTAL 4,141 0

Pymetrozine (insecticide) 

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.081 NT

Blueberries, Frozen 19 0 0.003 - 0.081 NT

Celery 708 1 0.1 0.005 ^ 0.003 - 0.005 0.6

Cherries, Fresh 228 0 0.081 ^ NT

Cherries, Frozen 282 0 0.081 ^ NT

Green Beans, Canned 378 0 0.005 ^ NT

Green Beans, Frozen 378 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Appendix B. Page 102 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 1 0.4 0.003 ^ 0.003 ^ 0.1

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 8 4.5 0.008 - 0.055 0.005 ^ 0.2

TOTAL 3,573 10

Pyraclostrobin (fungicide) 

Apples 177 23 13 0.004 - 0.057 0.003 ^ 1.5

Bananas 179 0 0.001 ^ 0.04

Blueberries, Cultivated, Fresh 688 180 26.2 0.002 - 0.26 0.002 - 0.003 4.0

Blueberries, Frozen 19 14 73.7 0.003 - 0.030 0.002 - 0.003 4.0

Broccoli 712 22 3.1 0.003 - 0.34 0.003 ^ 5.0

Carrots 707 112 15.8 0.005 - 0.054 0.003 ^ 0.4

Celery 708 143 20.2 0.003 - 0.15 0.001 - 0.004 29.0

Cherries, Fresh 228 143 62.7 0.002 - 0.20 0.002 ^ 2.5

Cherries, Frozen 282 74 26.2 0.002 - 0.17 0.002 ^ 2.5

Grape Juice 531 0 0.003 ^ 2.0

Green Beans, Canned 378 0 0.001 ^ 0.5

Green Beans, Fresh 757 100 13.2 0.001 - 0.10 0.001 ^ 0.5

Green Beans, Frozen 378 7 1.9 0.002 - 0.043 0.001 ^ 0.5

Nectarines 679 67 9.9 0.002 - 0.12 0.001 ^ 2.5

Peaches 707 150 21.2 0.003 - 0.23 0.003 ^ 2.5

Strawberries 176 82 46.6 0.003 - 0.66 0.003 ^ 1.2

Summer Squash 531 28 5.3 0.003 - 0.035 0.003 - 0.005 0.5

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.04

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.04

Tomatoes 177 48 27.1 0.002 - 0.056 0.001 ^ 1.4

Watermelon 390 0 0.003 ^ 0.5

TOTAL 8,579 1,193

Pyraflufen (precursor to Pyraflufen ethyl)

Blueberries, Cultivated, Fresh 354 0 0.020 ^ NT

Blueberries, Frozen 5 0 0.020 ^ NT

Celery 348 0 0.020 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.020 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Pyraflufen ethyl (herbicide) 

Apples 177 0 0.010 ^ 0.01

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Grape Juice 531 0 0.010 ^ 0.01

Nectarines 681 0 0.001 ^ 0.01

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 3,022 0

Appendix B. Page 103 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Pyrazophos (fungicide) 

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.006 NT

Blueberries, Frozen 19 0 0.005 - 0.006 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.006 ^ NT

Cherries, Frozen 282 0 0.006 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 3,699 0

Pyrethrins (insecticide) 

Bananas 179 0 0.20 ^ 1.0

Blueberries, Cultivated, Fresh 334 0 0.20 ^ 1.0

Blueberries, Frozen 14 0 0.20 ^ 1.0

Cherries, Fresh 228 0 0.20 ^ 1.0

Cherries, Frozen 282 0 0.20 ^ 1.0

TOTAL 1,037 0

Pyridaben (insecticide, acaricide)

Apples 30 0 0.005 ^ 0.5

Bananas 179 0 0.001 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.001 - 0.003 NT

Blueberries, Frozen 19 0 0.001 - 0.003 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.001 ^ 2.5

Cherries, Frozen 282 0 0.001 ^ 2.5

Grape Juice 531 0 0.005 ^ 1.5

Nectarines 681 3 0.4 0.007 - 0.032 0.001 ^ 2.5

Peaches 707 7 1 0.011 - 0.033 0.005 ^ 2.5

Strawberries 176 0 0.003 ^ 2.5

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 315 0 0.005 ^ NT

TOTAL 5,256 10

Pyridalyl (insecticide) 

Blueberries, Cultivated, Fresh 238 0 0.005 ^ NT

Blueberries, Frozen 2 0 0.005 ^ NT

Celery 348 0 0.005 ^ 20

Strawberries 176 0 0.005 ^ NT

Summer Squash 240 0 0.005 ^ NT

TOTAL 1,004 0

Appendix B. Page 104 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Pyrimethanil (fungicide) 

Apples 177 13 7.3 0.050 - 4.0 0.050 ^ 14

Bananas (X-1) 179 22 12.3 0.002 - 0.11 0.002 ^ 0.10

Blueberries, Cultivated, Fresh 688 4 0.6 0.003 - 0.006 0.002 - 0.005 3.0

Blueberries, Frozen 19 0 0.002 - 0.005 3.0

Broccoli 712 0 0.003 ^ NT

Celery (V-3) 708 3 0.4 0.002 - 0.006 0.001 - 0.005 NT

Cherries, Fresh 228 2 0.9 0.003 - 0.005 0.002 ^ 10

Cherries, Frozen 282 2 0.7 0.003 - 0.004 0.002 ^ 10

Grape Juice 501 0 0.10 ^ 5.0

Green Beans, Canned (V-2) 378 2 0.5 0.002 ^ 0.001 ^ NT

Green Beans, Fresh (V-2) 757 2 0.3 0.001 - 0.031 0.001 ^ NT

Green Beans, Frozen (V-2) 378 2 0.5 0.002 ^ 0.001 ^ NT

Nectarines 680 120 17.6 0.002 - 1.6 0.001 ^ 10

Peaches 707 140 19.8 0.003 - 1.6 0.003 ^ 10

Strawberries 176 47 26.7 0.005 - 1.5 0.005 ^ 3.0

Summer Squash 531 0 0.005 - 0.10 NT

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 33 18.6 0.002 - 0.14 0.001 ^ 0.50

Watermelon 390 0 0.050 ^ NT

TOTAL 7,843 392

Pyriproxyfen (insecticide, growth regulator)

Apples 177 3 1.7 0.003 - 0.005 0.001 ^ 0.20

Bananas 179 0 0.002 ^ 0.20

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.003 1.0

Blueberries, Frozen 19 0 0.002 - 0.003 1.0

Broccoli 712 2 0.3 0.006 - 0.029 0.005 ^ 0.70

Carrots 708 0 0.001 ^ 0.15

Celery 708 0 0.003 ^ 3.0

Cherries, Fresh 228 2 0.9 0.004 - 0.010 0.002 ^ 1.0

Cherries, Frozen 282 5 1.8 0.003 - 0.008 0.002 ^ 1.0

Grape Juice 531 0 0.001 ^ 2.5

Green Beans, Canned 378 0 0.003 ^ 0.20

Green Beans, Fresh 757 10 1.3 0.001 - 0.026 0.001 ^ 0.20

Green Beans, Frozen 378 0 0.003 ^ 0.20

Nectarines 681 19 2.8 0.002 - 0.026 0.001 ^ 1.0

Peaches 707 9 1.3 0.006 - 0.060 0.005 ^ 1.0

Strawberries 176 1 0.6 0.005 ^ 0.003 ^ 0.30

Summer Squash 531 0 0.003 - 0.010 0.10

Sweet Corn, Fresh 134 0 0.003 - 0.005 1.1

Sweet Corn, Frozen 41 0 0.003 - 0.005 1.1

Tomatoes 177 16 9 0.004 - 0.046 0.002 ^ 0.80

Watermelon 390 0 0.001 ^ 0.10

TOTAL 8,582 67

Pyroxasulfone (herbicide) 

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.015

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.015

TOTAL 351 0

Appendix B. Page 105 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Quinalphos (insecticide) 

Bananas 179 0 0.003 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.003 ^ NT

Cherries, Frozen 282 0 0.003 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 3,699 0

Quinoxyfen (fungicide) 

Apples 177 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 1.0

Blueberries, Frozen 5 0 0.003 ^ 1.0

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 531 0 0.020 ^ 2.0

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 7 1 0.002 - 0.017 0.001 ^ 0.70

Peaches 707 1 0.1 0.019 ^ 0.010 ^ 0.70

Strawberries 176 43 24.4 0.003 - 0.12 0.003 ^ 1.0

Summer Squash (V-1) 270 1 0.4 0.008 ^ 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ 1.7

Watermelon 390 0 0.020 ^ 0.08

TOTAL 5,734 52

Quintozene - PCNB (fungicide) (parent of HCB, PCA, PCB and PCPMS)

Apples 177 0 0.004 ^ NT

Bananas 179 0 0.021 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.021 NT

Blueberries, Frozen 19 0 0.005 - 0.021 NT

Broccoli 712 0 0.005 ^ 0.1

Carrots 708 0 0.006 ^ NT

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.021 ^ NT

Cherries, Frozen 282 0 0.021 ^ NT

Grape Juice 531 0 0.004 ^ NT

Green Beans, Canned 378 0 0.001 ^ 0.1

Green Beans, Fresh 757 0 0.025 ^ 0.1

Green Beans, Frozen 378 0 0.001 ^ 0.1

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.050 NT

Sweet Corn, Fresh 134 0 0.005 - 0.025 NT

Sweet Corn, Frozen 41 0 0.005 - 0.025 NT

Appendix B. Page 106 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 0 0.001 ^ 0.1

Watermelon 390 0 0.004 ^ NT

TOTAL 7,901 0

Quizalofop (metabolite of Quizalofop ethyl)

Blueberries, Cultivated, Fresh 354 0 0.050 ^ NT

Blueberries, Frozen 5 0 0.050 ^ NT

Celery 348 0 0.050 ^ NT

Strawberries 176 0 0.050 ^ NT

Summer Squash 270 0 0.050 ^ NT

Sweet Corn, Fresh 78 0 0.050 ^ NT

Sweet Corn, Frozen 12 0 0.050 ^ NT

TOTAL 1,243 0

Quizalofop ethyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.35 ^ 0.25

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

TOTAL 2,085 0

Resmethrin (insecticide) 

Bananas 179 0 0.028 ^ 3.0

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.028 3.0

Blueberries, Frozen 19 0 0.010 - 0.028 3.0

Broccoli 712 0 0.020 ^ 3.0

Celery 348 0 0.010 ^ 3.0

Cherries, Fresh 228 0 0.028 ^ 3.0

Cherries, Frozen 282 0 0.028 ^ 3.0

Green Beans, Fresh 504 0 0.20 ^ 3.0

Peaches 707 0 0.020 ^ 3.0

Strawberries 176 0 0.010 ^ 3.0

Summer Squash 531 0 0.010 - 0.25 3.0

Sweet Corn, Fresh 134 0 0.005 - 0.010 3.0

Sweet Corn, Frozen 41 0 0.005 - 0.010 3.0

TOTAL 4,549 0

Resmethrin cis (isomer of Resmethrin)

Apples 177 0 0.050 ^ 3.0

Carrots 708 0 0.002 ^ 3.0

Celery 360 0 0.002 ^ 3.0

Grape Juice 531 0 0.050 ^ 3.0

Green Beans, Canned 378 0 0.002 ^ 3.0

Green Beans, Frozen 378 0 0.002 ^ 3.0

Nectarines 681 0 0.002 ^ 3.0

Tomatoes 177 0 0.002 ^ 3.0

Watermelon 390 0 0.050 ^ 3.0

TOTAL 3,780 0

Appendix B. Page 107 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Resmethrin trans (isomer of Resmethrin)

Apples 177 0 0.050 ^ 3.0

Carrots 708 0 0.002 ^ 3.0

Celery 360 0 0.002 ^ 3.0

Grape Juice 531 0 0.050 ^ 3.0

Green Beans, Canned 378 0 0.002 ^ 3.0

Green Beans, Frozen 378 0 0.002 ^ 3.0

Nectarines 681 0 0.002 ^ 3.0

Tomatoes 177 0 0.002 ^ 3.0

Watermelon 390 0 0.050 ^ 3.0

TOTAL 3,780 0

Rimsulfuron (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ 0.01

Blueberries, Frozen 5 0 0.010 ^ 0.01

Celery 348 0 0.010 ^ NT

Nectarines 681 0 0.003 ^ 0.01

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,924 0

Rotenone (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.040 ^ NT

Blueberries, Frozen 5 0 0.040 ^ NT

Celery 348 0 0.040 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.040 ^ NT

Sweet Corn, Fresh 78 0 0.020 ^ NT

Sweet Corn, Frozen 12 0 0.020 ^ NT

TOTAL 1,243 0

Saflufenacil (herbicide) 

Apples 177 0 0.010 ^ 0.03

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Grape Juice 119 0 0.010 ^ 0.03

Green Beans, Fresh 757 0 0.010 ^ 0.03

Nectarines 681 0 0.005 ^ 0.03

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.010 ^ 0.03

Sweet Corn, Frozen 41 0 0.010 ^ 0.03

Watermelon 390 0 0.010 ^ NT

TOTAL 3,452 0

Sedaxane (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Appendix B. Page 108 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ 0.01

Sweet Corn, Frozen 12 0 0.005 ^ 0.01

TOTAL 1,243 0

Sethoxydim (herbicide) 

Apples 177 0 0.003 ^ 0.2

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.007 4.0

Blueberries, Frozen 19 0 0.005 - 0.007 4.0

Carrots 708 0 0.001 ^ 4.0

Celery 348 0 0.005 ^ 4.0

Cherries, Fresh 228 0 0.007 ^ 0.2

Cherries, Frozen 282 0 0.007 ^ 0.2

Grape Juice 501 0 0.003 ^ 1.0

Green Beans, Fresh 757 0 0.005 ^ 15

Nectarines 681 0 0.001 ^ 0.2

Strawberries 176 0 0.005 ^ 10

Summer Squash 531 0 0.005 - 0.020 4.0

Sweet Corn, Fresh 134 0 0.005 ^ 0.4

Sweet Corn, Frozen 41 0 0.005 ^ 0.4

Watermelon 390 0 0.003 ^ 4.0

TOTAL 5,840 0

Simazine (herbicide) 

Apples 177 0 0.005 ^ 0.20

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 3 0.4 0.009 - 0.012 0.005 ^ 0.20

Blueberries, Frozen 19 0 0.005 ^ 0.20

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.005 ^ 0.20

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.004 ^ 0.20

Strawberries 176 0 0.003 ^ 0.25

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.25

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.25

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 5,437 3

Spinetoram (insecticide) 

Apples 177 6 3.4 0.004 - 0.006 0.003 ^ 0.20

Bananas 179 0 0.005 ^ 0.25

Blueberries, Cultivated, Fresh 688 15 2.2 0.006 - 0.090 0.005 - 0.010 0.25

Blueberries, Frozen 19 0 0.005 - 0.010 0.25

Carrots 708 0 0.015 ^ 0.10

Celery 708 1 0.1 0.011 ^ 0.001 - 0.010 8.0

Cherries, Fresh 228 33 14.5 0.005 - 0.029 0.005 ^ 0.20

Cherries, Frozen 282 4 1.4 0.007 - 0.008 0.005 ^ 0.20

Appendix B. Page 109 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Grape Juice 502 0 0.005 ^ 0.50

Green Beans, Canned 378 0 0.001 ^ 0.30

Green Beans, Fresh 757 14 1.8 0.001 - 0.006 0.001 ^ 0.30

Green Beans, Frozen 378 0 0.001 ^ 0.30

Nectarines 681 139 20.4 0.013 - 0.099 0.008 ^ 0.20

Strawberries 176 4 2.3 0.010 - 0.019 0.010 ^ 1.0

Summer Squash 270 0 0.010 ^ 0.30

Sweet Corn, Fresh 134 0 0.001 - 0.010 0.04

Sweet Corn, Frozen 41 0 0.001 - 0.010 0.04

Tomatoes 177 0 0.001 ^ 0.40

Watermelon 390 0 0.003 ^ 0.30

TOTAL 6,873 216

Spinosad (insecticide) (total of spinosyns A and D)

Blueberries, Cultivated, Fresh 354 8 2.3 0.003 - 0.028 0.003 ^ 0.250

Blueberries, Frozen 5 0 0.003 ^ 0.250

Carrots 708 0 0.005 ^ 0.10

Celery 708 6 0.8 0.002 - 0.006 0.001 - 0.003 8.0

Green Beans, Canned 378 0 0.001 ^ 0.30

Green Beans, Fresh 757 1 0.1 0.007 ^ 0.002 ^ 0.30

Green Beans, Frozen 378 0 0.001 ^ 0.30

Nectarines 680 167 24.6 0.010 - 0.10 0.006 ^ 0.20

Strawberries 176 6 3.4 0.003 - 0.034 0.003 ^ 1.0

Summer Squash 531 0 0.003 - 0.005 0.3

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.02

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.02

Tomatoes 177 4 2.3 0.002 - 0.018 0.001 ^ 0.4

TOTAL 5,027 192

Spinosad A (isomer of Spinosad) 

Apples 177 1 0.6 0.003 ^ 0.003 ^ 0.20

Bananas 179 0 0.005 ^ 0.25

Blueberries, Cultivated, Fresh 334 3 0.9 0.004 - 0.047 0.003 ^ 0.250

Blueberries, Frozen 14 2 14.3 0.008 - 0.013 0.003 ^ 0.250

Broccoli 712 2 0.3 0.005 - 0.011 0.002 ^ 2.0

Cherries, Fresh 228 81 35.5 0.003 - 0.064 0.003 ^ 0.20

Cherries, Frozen 282 20 7.1 0.003 - 0.047 0.003 ^ 0.20

Grape Juice 502 0 0.005 ^ 0.50

Watermelon 390 0 0.003 ^ 0.3

TOTAL 2,818 109

Spinosad D (isomer of Spinosad) 

Bananas 179 0 0.005 ^ 0.25

Blueberries, Cultivated, Fresh 334 1 0.3 0.009 ^ 0.003 ^ 0.250

Blueberries, Frozen 14 1 7.1 0.003 ^ 0.003 ^ 0.250

Broccoli 712 1 0.1 0.003 ^ 0.002 ^ 2.0

Cherries, Fresh 228 18 7.9 0.003 - 0.018 0.003 ^ 0.20

Cherries, Frozen 282 4 1.4 0.003 - 0.007 0.003 ^ 0.20

Grape Juice 30 0 0.007 ^ 0.50

TOTAL 1,779 25

Appendix B. Page 110 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Spirodiclofen (acaricide) 

Apples 177 23 13 0.015 - 0.068 0.010 ^ 0.80

Bananas 179 0 0.006 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.006 NT

Blueberries, Frozen 19 0 0.005 - 0.006 NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.006 ^ 1.0

Cherries, Frozen 282 0 0.006 ^ 1.0

Grape Juice 531 0 0.010 ^ 2.0

Nectarines 681 13 1.9 0.11 ^ 0.065 ^ 1.0

Peaches 688 99 14.4 0.010 - 0.23 0.010 ^ 1.0

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 5,459 135

Spiromesifen Total (parent + enol metabolite) (insecticide) 

Celery 300 1 0.3 0.085 ^ 0.002 - 0.016 6.0

Green Beans, Canned 378 0 0.002 ^ 0.80

Green Beans, Frozen 378 0 0.002 ^ 0.80

TOTAL 1,056 1

Spiromesifen (insecticide) 

Apples 89 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.005 ^ 2.0

Blueberries, Frozen 5 0 0.005 ^ 2.0

Broccoli 712 0 0.002 ^ 2.0

Celery 348 0 0.005 ^ 6.0

Grape Juice 531 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.020 ^ 0.80

Peaches 707 0 0.002 ^ NT

Strawberries 176 20 11.4 0.003 - 0.26 0.003 ^ 2.0

Summer Squash 531 0 0.005 - 0.040 0.10

Sweet Corn, Fresh 134 0 0.003 - 0.020 0.02

Sweet Corn, Frozen 41 0 0.003 - 0.020 0.02

Watermelon 378 0 0.010 ^ 0.10

TOTAL 4,763 20

Spiromesifen alcohol (metabolite of Spiromesifen)

Blueberries, Cultivated, Fresh 295 0 0.003 ^ 2.0

Blueberries, Frozen 5 0 0.003 ^ 2.0

Celery 319 0 0.003 ^ 6.0

Strawberries 176 50 28.4 0.002 - 0.23 0.001 ^ 2.0

Summer Squash 270 0 0.003 ^ 0.10

Sweet Corn, Fresh 78 0 0.001 ^ 0.02

Sweet Corn, Frozen 12 0 0.001 ^ 0.02

TOTAL 1,155 50

Appendix B. Page 111 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Spirotetramat (insecticide) 

Apples 177 0 0.002 ^ 0.70

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 3.0

Blueberries, Frozen 5 0 0.003 ^ 3.0

Celery 348 11 3.2 0.003 - 0.080 0.003 ^ 9.0

Grape Juice 531 0 0.002 ^ 1.3

Green Beans, Fresh 757 0 0.001 ^ 2.5

Nectarines 681 2 0.3 0.002 - 0.007 0.001 ^ 4.5

Strawberries 176 0 0.003 ^ 0.40

Summer Squash 531 0 0.003 - 0.010 0.30

Sweet Corn, Fresh 134 0 0.001 - 0.003 1.5

Sweet Corn, Frozen 41 0 0.001 - 0.003 1.5

Watermelon 390 0 0.002 ^ 0.30

TOTAL 4,125 13

Spiroxamine (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.002 ^ 3.0

Blueberries, Cultivated, Fresh 688 0 0.003 ^ NT

Blueberries, Frozen 19 0 0.003 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.003 ^ NT

Cherries, Frozen 282 0 0.003 ^ NT

Grape Juice 531 0 0.010 ^ 1.0

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 4,797 0

Sulfallate (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Sulfentrazone (herbicide) 

Bananas 179 0 0.035 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.035 0.15

Blueberries, Frozen 19 0 0.010 - 0.035 0.15

Celery 348 0 0.010 ^ NT

Cherries, Fresh 228 0 0.035 ^ NT

Cherries, Frozen 282 0 0.035 ^ NT

Green Beans, Fresh 757 0 0.015 ^ NT

Strawberries 176 0 0.010 ^ 0.15

Summer Squash 270 0 0.010 ^ NT

Appendix B. Page 112 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 134 0 0.010 - 0.015 NT

Sweet Corn, Frozen 41 0 0.010 - 0.015 NT

TOTAL 3,122 0

Sulfoxaflor (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 0.70

Blueberries, Frozen 5 0 0.003 ^ 0.70

Celery 348 0 0.003 ^ 2.0

Strawberries 176 0 0.003 ^ 0.70

Summer Squash 270 2 0.7 0.017 - 0.078 0.003 ^ 0.40

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 4 2.3 0.003 - 0.013 0.002 ^ 0.70

TOTAL 1,420 6

Sulprofos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,536 0

TCMTB (fungicide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 56 0 0.005 ^ NT

Sweet Corn, Frozen 29 0 0.005 ^ NT

TOTAL 261 0

Tebuconazole (fungicide) 

Apples 177 0 0.010 ^ 0.05

Bananas 179 0 0.006 ^ 0.05

Blueberries, Cultiv., Fresh (V-4) 688 4 0.6 0.022 - 0.070 0.010 - 0.012 NT

Blueberries, Frozen 19 0 0.010 - 0.012 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 228 65 28.5 0.012 - 3.0 0.012 ^ 5.0

Cherries, Frozen 282 146 51.8 0.012 - 0.81 0.012 ^ 5.0

Grape Juice 531 0 0.010 ^ 5.0

Green Beans, Canned 378 0 0.006 ^ 0.1

Green Beans, Fresh 757 42 5.5 0.001 - 0.048 0.001 ^ 0.1

Green Beans, Frozen 378 0 0.006 ^ 0.1

Nectarines (X-1) 681 172 25.3 0.002 - 1.5 0.001 ^ 1.0

Peaches (X-9) 707 167 23.6 0.005 - 6.6 0.005 ^ 1.0

Strawberries (V-1) 176 1 0.6 0.018 ^ 0.003 ^ NT

Summer Squash 531 0 0.005 - 0.010 0.4

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.5

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.5

Appendix B. Page 113 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 5 2.8 0.003 - 0.042 0.002 ^ 1.3

Watermelon 390 0 0.010 ^ 0.4

TOTAL 7,874 602

Tebufenozide (insecticide) 

Apples 177 0 0.002 ^ 1.0

Bananas 179 0 0.003 ^ NT

Blueberries, Cultivated, Fresh 688 7 1 0.005 - 1.3 0.003 - 0.005 3.0

Blueberries, Frozen 19 0 0.003 - 0.005 3.0

Broccoli 712 0 0.025 ^ 5.0

Celery 708 0 0.003 - 0.010 2.0

Cherries, Fresh 228 0 0.003 ^ NT

Cherries, Frozen 282 0 0.003 ^ NT

Grape Juice 531 0 0.002 ^ 3.0

Green Beans, Canned 378 0 0.003 - 0.010 NT

Green Beans, Frozen 378 0 0.003 - 0.010 NT

Peaches 707 0 0.050 ^ NT

Strawberries 176 0 0.005 ^ 3.0

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 1 0.6 0.005 ^ 0.003 - 0.020 1.0

Watermelon 390 0 0.002 ^ NT

TOTAL 6,090 8

Tebufenpyrad (insecticide, acaricide)

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 ^ NT

Blueberries, Frozen 19 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.010 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 4,797 0

Tebuthiuron (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 708 0 0.001 - 0.003 NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Appendix B. Page 114 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 0 0.001 ^ NT

TOTAL 2,536 0

Tecnazene (plant growth regulator) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.003 - 0.010 NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 3,955 0

Teflubenzuron (insecticide) 

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 2,280 0

Tefluthrin (insecticide) 

Apples 177 0 0.002 ^ NT

Bananas 179 0 0.009 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.009 NT

Blueberries, Frozen 19 0 0.003 - 0.009 NT

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.002 ^ NT

Celery 708 0 0.001 - 0.003 NT

Cherries, Fresh 228 0 0.009 ^ NT

Cherries, Frozen 282 0 0.009 ^ NT

Grape Juice 531 0 0.002 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh 757 0 0.050 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines 681 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.050 NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.05

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.05

Appendix B. Page 115 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 8,582 0

Tepraloxydim (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Green Beans, Fresh 757 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 NT

Sweet Corn, Frozen 41 0 0.005 - 0.010 NT

TOTAL 2,085 0

Terbacil (herbicide) 

Apples 177 0 0.010 ^ 0.3

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.020 0.2

Blueberries, Frozen 19 0 0.005 - 0.020 0.2

Broccoli 649 0 0.008 ^ NT

Celery 708 0 0.003 - 0.005 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Nectarines 681 0 0.020 ^ 0.2

Peaches 707 0 0.008 ^ 0.2

Strawberries 176 0 0.005 ^ 0.1

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.003 ^ NT

Watermelon 390 0 0.010 ^ 1.0

TOTAL 6,708 0

Terbufos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.05

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.05

TOTAL 1,328 0

Terbufos oxygen analog (metabolite of Terbufos)

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.05

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.05

TOTAL 351 0

Appendix B. Page 116 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Terbufos oxygen analog sulfone (metabolite of Terbufos)

Strawberries 176 0 0.010 - 0.020 NT

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.05

TOTAL 351 0

Terbufos oxygen analog sulfoxide (metabolite of Terbufos)

Sweet Corn, Fresh 56 0 0.005 ^ 0.05

Sweet Corn, Frozen 29 0 0.005 ^ 0.05

TOTAL 85 0

Terbufos sulfone (metabolite of Terbufos)

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.002 - 0.010 NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ 0.05

Sweet Corn, Frozen 41 0 0.005 ^ 0.05

Tomatoes 177 0 0.002 ^ NT

TOTAL 2,621 0

Terbufos sulfoxide (metabolite of Terbufos)

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.002 - 0.003 0.05

Sweet Corn, Frozen 41 0 0.002 - 0.003 0.05

TOTAL 1,328 0

Terbuthylazine (herbicide) 

Bananas 179 0 0.002 ^ NT

Blueberries, Cultiv., Fresh (V-2) 688 2 0.3 0.003 - 0.004 0.002 - 0.003 NT

Blueberries, Frozen 19 0 0.002 - 0.003 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.003 ^ NT

Cherries, Fresh 228 0 0.002 ^ NT

Cherries, Frozen 282 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 3,699 2

Terbutryn (herbicide) 

Grape Juice 325 0 0.025 ^ NT

TOTAL 325 0

Appendix B. Page 117 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tetrachlorvinphos (insecticide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 708 0 0.003 - 0.005 NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Fresh 757 0 0.005 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 0 0.003 ^ NT

TOTAL 3,378 0

Tetraconazole (fungicide) 

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ 0.25

Blueberries, Frozen 5 0 0.010 ^ 0.25

Celery (V-1) 708 1 0.1 0.002 ^ 0.001 - 0.010 NT

Grape Juice 531 0 0.010 ^ 0.20

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 13 7.4 0.003 - 0.079 0.003 ^ 0.25

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 3,634 14

Tetradifon (insecticide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.020 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.020 NT

Blueberries, Frozen 19 0 0.010 - 0.020 NT

Broccoli 712 0 0.005 ^ NT

Celery 708 0 0.002 - 0.010 NT

Cherries, Fresh 228 0 0.020 ^ NT

Cherries, Frozen 282 0 0.020 ^ NT

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.002 ^ NT

Green Beans, Frozen 378 0 0.002 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.002 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,090 0

Appendix B. Page 118 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tetrahydrophthalimide - THPI (metabolite of Captafol and Captan)

Apples 177 37 20.9 0.010 - 0.75 0.010 ^ 25.0

Blueberries, Cultivated, Fresh 354 94 26.6 0.010 - 2.7 0.010 ^ 20.0

Blueberries, Frozen 5 2 40 0.038 - 0.060 0.010 ^ 20.0

Celery 708 0 0.004 - 0.010 0.05

Grape Juice 531 35 6.6 0.010 - 0.28 0.010 ^ 25.0

Green Beans, Canned 378 0 0.004 ^ 0.05

Green Beans, Frozen 378 0 0.004 ^ 0.05

Strawberries 176 128 72.7 0.012 - 2.5 0.010 ^ 20.0

Summer Squash 270 0 0.010 - 0.040 0.05

Sweet Corn, Fresh 78 0 0.010 ^ 0.05

Sweet Corn, Frozen 12 0 0.010 ^ 0.05

Tomatoes (X-3) 157 14 8.9 0.006 - 0.15 0.004 ^ 0.05

Watermelon 390 0 0.010 ^ 0.05

TOTAL 3,614 310

Tetramethrin (insecticide) 

Apples 177 0 0.005 ^ NT

Bananas 179 0 0.099 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.10 NT

Blueberries, Frozen 19 0 0.005 - 0.10 NT

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.001 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.10 ^ NT

Cherries, Frozen 282 0 0.10 ^ NT

Grape Juice 531 0 0.005 ^ NT

Green Beans, Fresh 757 0 0.050 ^ NT

Nectarines (V-1) 681 1 0.1 0.002 ^ 0.001 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Watermelon 390 0 0.005 ^ NT

TOTAL 6,943 1

Thiabendazole (fungicide) (parent of 5-hydroxythiabendazole)

Apples 177 86 48.6 0.002 - 2.0 0.002 ^ 5.0

Bananas 179 104 58.1 0.008 - 0.22 0.006 ^ 3.0

Blueberries, Cultivated, Fresh 688 0 0.005 ^ NT

Blueberries, Frozen 19 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Carrots 708 0 0.002 ^ 10.0

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh (V-2) 228 2 0.9 0.012 - 0.014 0.005 ^ NT

Cherries, Frozen (V-2) 282 2 0.7 0.008 - 0.009 0.005 ^ NT

Grape Juice 531 0 0.003 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Nectarines (V-62) 681 62 9.1 0.003 - 0.042 0.002 ^ NT

Peaches (V-10) 707 10 1.4 0.011 - 0.12 0.010 ^ NT

Strawberries 176 5 2.8 0.003 - 0.53 0.003 ^ 5.0

Appendix B. Page 119 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.008 0.01

Sweet Corn, Frozen 41 0 0.003 - 0.008 0.01

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.002 ^ NT

TOTAL 7,564 271

Thiacloprid (insecticide) 

Apples 177 26 14.7 0.001 - 0.021 0.001 ^ 0.30

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Broccoli 712 0 0.010 ^ NT

Celery 708 0 0.001 - 0.003 NT

Cherries, Fresh 228 1 0.4 0.014 ^ 0.005 ^ 0.5

Cherries, Frozen 282 99 35.1 0.005 - 0.11 0.005 ^ 0.5

Grape Juice 531 0 0.001 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Nectarines 681 9 1.3 0.008 - 0.024 0.005 ^ 0.5

Peaches 707 1 0.1 0.026 ^ 0.010 ^ 0.5

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Tomatoes (V-1) 177 1 0.6 0.002 ^ 0.001 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 6,771 137

Thiamethoxam (insecticide) (also a parent of Clothianidin)

Apples 177 6 3.4 0.003 - 0.009 0.003 ^ 0.2

Bananas 179 0 0.010 ^ 0.02

Blueberries, Cultivated, Fresh 688 9 1.3 0.003 - 0.007 0.003 - 0.005 0.30

Blueberries, Frozen 19 0 0.003 - 0.005 0.30

Broccoli 712 20 2.8 0.010 - 0.062 0.010 ^ 4.5

Carrots 708 0 0.008 ^ 0.05

Celery 708 86 12.1 0.003 - 0.034 0.003 - 0.015 4.0

Cherries, Fresh 228 7 3.1 0.007 - 0.059 0.005 ^ 0.5

Cherries, Frozen 282 58 20.6 0.005 - 0.074 0.005 ^ 0.5

Grape Juice 531 0 0.003 ^ 0.20

Green Beans, Canned 378 0 0.015 ^ 0.02

Green Beans, Fresh 757 0 0.005 ^ 0.02

Green Beans, Frozen 378 0 0.015 ^ 0.02

Nectarines 681 0 0.025 ^ 0.5

Peaches 707 1 0.1 0.029 ^ 0.010 ^ 0.5

Strawberries 176 35 19.9 0.003 - 0.11 0.003 ^ 0.30

Summer Squash 531 78 14.7 0.003 - 0.14 0.003 - 0.060 0.2

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.02

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.02

Tomatoes 177 12 6.8 0.008 - 0.020 0.005 ^ 0.25

Watermelon 390 30 7.7 0.003 - 0.033 0.003 ^ 0.2

TOTAL 8,582 342

Appendix B. Page 120 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Thiazopyr (herbicide) 

Apples 177 0 0.008 ^ NT

Grape Juice 531 0 0.008 ^ NT

Watermelon 390 0 0.008 ^ NT

TOTAL 1,098 0

Thifensulfuron methyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.001 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.001 ^ NT

Sweet Corn, Frozen 12 0 0.001 ^ NT

TOTAL 1,243 0

Thiobencarb (herbicide) 

Apples 177 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 708 0 0.001 - 0.010 0.2

Grape Juice 531 0 0.010 ^ NT

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 3,634 0

Thiodicarb (insecticide) 

Apples 177 0 0.003 ^ NT

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ 35

Grape Juice 531 0 0.003 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Watermelon 390 0 0.003 ^ NT

TOTAL 2,251 0

Thionazin (insecticide, fumigant)

Blueberries, Cultivated, Fresh 354 0 0.005 ^ NT

Blueberries, Frozen 5 0 0.005 ^ NT

Celery 348 0 0.005 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Appendix B. Page 121 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Thiophanate methyl (fungicide) 

Green Beans, Fresh 757 18 2.4 0.005 - 0.030 0.005 ^ 2.0

Summer Squash 232 0 0.040 ^ 1.0

Sweet Corn, Fresh 56 0 0.005 ^ NT

Sweet Corn, Frozen 29 0 0.005 ^ NT

TOTAL 1,074 18

Tolclofos methyl (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.010 ^ NT

Blueberries, Frozen 5 0 0.010 ^ NT

Celery 348 0 0.010 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

TOTAL 1,243 0

Tolfenpyrad (insecticide) 

Strawberries 176 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 266 0

Tolylfluanid (fungicide) 

Bananas 179 0 0.047 ^ NT

Blueberries, Cultivated, Fresh 334 0 0.048 ^ NT

Blueberries, Frozen 14 0 0.048 ^ NT

Cherries, Fresh 228 0 0.048 ^ NT

Cherries, Frozen 282 0 0.048 ^ NT

TOTAL 1,037 0

Topramezone (herbicide) 

Sweet Corn, Fresh 56 0 0.25 ^ 0.01

Sweet Corn, Frozen 29 0 0.25 ^ 0.01

TOTAL 85 0

Tri-Allate (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.003 ^ NT

Green Beans, Fresh 757 0 0.008 - 0.075 NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.075 NT

Sweet Corn, Frozen 41 0 0.003 - 0.075 NT

TOTAL 3,504 0

Triadimefon (fungicide) (also a parent of Triadimenol)

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Broccoli 712 0 0.005 ^ NT

Appendix B. Page 122 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 708 0 0.001 - 0.010 NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Green Beans, Canned 378 0 0.003 ^ NT

Green Beans, Frozen 378 0 0.003 ^ NT

Nectarines 681 0 0.015 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.010 ^ NT

Summer Squash 270 0 0.010 ^ NT

Sweet Corn, Fresh 78 0 0.010 ^ NT

Sweet Corn, Frozen 12 0 0.010 ^ NT

Tomatoes 177 0 0.001 ^ NT

TOTAL 5,673 0

Triadimenol (fungicide) (also a metabolite of Triadimefon)

Bananas 179 0 0.017 ^ 0.2

Blueberries, Cultivated, Fresh 688 0 0.017 - 0.030 NT

Blueberries, Frozen 19 0 0.017 - 0.030 NT

Broccoli 712 0 0.005 ^ NT

Celery 348 0 0.030 ^ NT

Cherries, Fresh 228 0 0.017 ^ NT

Cherries, Frozen 282 0 0.017 ^ NT

Nectarines 681 0 0.050 ^ NT

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.020 ^ NT

Summer Squash 270 0 0.030 ^ NT

Sweet Corn, Fresh 134 0 0.005 - 0.020 0.05

Sweet Corn, Frozen 41 0 0.005 - 0.020 0.05

TOTAL 4,465 0

Triazophos (insecticide) 

Apples 177 0 0.001 ^ NT

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 ^ NT

Blueberries, Frozen 19 0 0.005 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 0 0.005 ^ NT

Cherries, Frozen 282 0 0.005 ^ NT

Grape Juice 531 0 0.001 ^ NT

Nectarines 681 0 0.003 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.005 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 5,478 0

Tribenuron methyl (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Appendix B. Page 123 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.003 ^ NT

Summer Squash 240 0 0.003 ^ NT

Sweet Corn, Fresh 78 0 0.003 ^ NT

Sweet Corn, Frozen 12 0 0.003 ^ NT

TOTAL 1,213 0

Trichlorfon (insecticide) 

Apples 177 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.020 NT

Sweet Corn, Frozen 41 0 0.003 - 0.020 NT

Watermelon 390 0 0.010 ^ NT

TOTAL 1,449 0

Triclopyr (herbicide) 

Blueberries, Cultivated, Fresh 354 0 0.25 ^ NT

Blueberries, Frozen 5 0 0.25 ^ NT

Celery 348 0 0.25 ^ NT

Strawberries 176 0 0.25 ^ NT

Summer Squash 270 0 0.25 ^ NT

Sweet Corn, Fresh 78 0 0.25 ^ NT

Sweet Corn, Frozen 12 0 0.25 ^ NT

TOTAL 1,243 0

Tricyclazole (fungicide) 

Strawberries 176 0 0.001 ^ NT

Sweet Corn, Fresh 78 0 0.001 ^ NT

Sweet Corn, Frozen 12 0 0.001 ^ NT

TOTAL 266 0

Trifloxystrobin (fungicide) 

Apples 177 12 6.8 0.002 - 0.016 0.002 ^ 0.5

Bananas 179 0 0.005 ^ 0.10

Blueberries, Cultiv., Fresh (V-1) 688 1 0.1 0.013 ^ 0.003 - 0.005 NT

Blueberries, Frozen 19 0 0.003 - 0.005 NT

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.001 ^ 0.1

Celery 708 23 3.2 0.002 - 0.020 0.001 - 0.003 3.5

Cherries, Fresh 228 37 16.2 0.005 - 0.090 0.005 ^ 2

Cherries, Frozen 282 61 21.6 0.005 - 0.14 0.005 ^ 2

Grape Juice 531 0 0.003 ^ 2.0

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Fresh (V-2) 757 2 0.3 0.001 - 0.004 0.001 ^ NT

Green Beans, Frozen (V-2) 378 2 0.5 0.002 - 0.011 0.001 ^ NT

Nectarines 681 29 4.3 0.005 - 0.12 0.003 ^ 2

Peaches 707 13 1.8 0.006 - 0.070 0.005 ^ 2

Strawberries 176 6 3.4 0.005 - 0.055 0.003 ^ 1.1

Summer Squash 531 1 0.2 0.003 ^ 0.003 - 0.005 0.50

Sweet Corn, Fresh 134 0 0.001 - 0.003 0.04

Sweet Corn, Frozen 41 0 0.001 - 0.003 0.04

Appendix B. Page 124 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tomatoes 177 1 0.6 0.012 ^ 0.001 ^ 0.5

Watermelon 390 0 0.002 ^ 0.50

TOTAL 8,582 188

Trifloxysulfuron (herbicide) 

Apples 177 0 0.020 ^ NT

Grape Juice 119 0 0.020 ^ NT

Watermelon 390 0 0.020 ^ NT

TOTAL 686 0

Triflumizole (fungicide) 

Apples 177 0 0.010 ^ 0.50

Bananas 179 0 0.002 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.002 - 0.005 2.0

Blueberries, Frozen 19 0 0.002 - 0.005 2.0

Broccoli 712 0 0.003 ^ 8.0

Celery 348 0 0.005 ^ NT

Cherries, Fresh 228 92 40.4 0.002 - 0.30 0.002 ^ 1.5

Cherries, Frozen 282 16 5.7 0.003 - 0.16 0.002 ^ 1.5

Grape Juice 501 0 0.010 ^ 2.5

Green Beans, Fresh 757 0 0.001 ^ NT

Peaches 707 0 0.003 ^ NT

Strawberries 176 12 6.8 0.006 - 0.38 0.005 ^ 2.0

Summer Squash 531 6 1.1 0.005 - 0.046 0.005 - 0.062 0.5

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Watermelon 358 0 0.010 ^ 0.5

TOTAL 5,838 126

Trifluralin (herbicide) 

Apples 177 0 0.001 ^ NT

Bananas 179 0 0.009 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.009 NT

Blueberries, Frozen 19 0 0.005 - 0.009 NT

Broccoli 712 0 0.005 ^ 0.05

Carrots 708 148 20.9 0.003 - 0.24 0.002 ^ 1.0

Celery 708 2 0.3 0.002 ^ 0.001 - 0.005 0.05

Cherries, Fresh 228 0 0.009 ^ 0.05

Cherries, Frozen 282 0 0.009 ^ 0.05

Grape Juice 531 0 0.001 ^ 0.05

Green Beans, Canned 378 0 0.001 ^ 0.05

Green Beans, Fresh 757 0 0.005 ^ 0.05

Green Beans, Frozen 378 0 0.001 ^ 0.05

Nectarines 681 0 0.002 ^ 0.05

Peaches 707 0 0.005 ^ 0.05

Strawberries 176 0 0.005 ^ NT

Summer Squash 531 0 0.005 - 0.010 0.05

Sweet Corn, Fresh 134 0 0.005 ^ NT

Sweet Corn, Frozen 41 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ 0.05

Watermelon 390 0 0.001 ^ 0.05

TOTAL 8,582 150

Appendix B. Page 125 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Triforine (fungicide) 

Apples 177 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ NT

Nectarines 681 0 0.025 ^ NT

Strawberries 176 0 0.10 ^ NT

Sweet Corn, Fresh 78 0 0.10 ^ NT

Sweet Corn, Frozen 12 0 0.10 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 2,045 0

Triticonazole (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.040 ^ NT

Blueberries, Frozen 5 0 0.040 ^ NT

Broccoli 712 0 0.010 ^ NT

Celery 348 0 0.040 ^ NT

Peaches 707 0 0.010 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 270 0 0.040 ^ NT

Sweet Corn, Fresh 134 0 0.003 - 0.025 NT

Sweet Corn, Frozen 41 0 0.003 - 0.025 NT

TOTAL 2,747 0

Uniconazole (insect growth regulator) 

Blueberries, Cultivated, Fresh 354 0 0.040 ^ NT

Blueberries, Frozen 5 0 0.040 ^ NT

Celery 348 0 0.040 ^ NT

Strawberries 176 0 0.005 ^ NT

Summer Squash 270 0 0.040 ^ NT

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

TOTAL 1,243 0

Vernolate (herbicide) 

Broccoli 712 0 0.010 ^ NT

Peaches 707 0 0.010 ^ NT

TOTAL 1,419 0

Vinclozolin (fungicide) 

Apples 177 0 0.010 ^ NT

Bananas 179 0 0.010 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.010 NT

Blueberries, Frozen 19 0 0.005 - 0.010 NT

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.002 ^ NT

Celery 708 0 0.001 - 0.005 NT

Cherries, Fresh 228 0 0.010 ^ NT

Cherries, Frozen 282 0 0.010 ^ NT

Grape Juice 531 0 0.010 ^ 6.0

Green Beans, Canned 378 0 0.001 ^ NT

Green Beans, Frozen 378 0 0.001 ^ NT

Peaches 707 0 0.005 ^ 25.0

Strawberries 176 0 0.005 ^ 10.0

Summer Squash 270 0 0.005 ^ NT

Appendix B. Page 126 of 127
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 78 0 0.005 ^ NT

Sweet Corn, Frozen 12 0 0.005 ^ NT

Tomatoes 177 0 0.001 ^ NT

Watermelon 390 0 0.010 ^ NT

TOTAL 6,798 0

Zoxamide (fungicide) 

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Celery 348 0 0.003 ^ NT

Green Beans, Fresh 757 0 0.002 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.010 1.0

Sweet Corn, Fresh 134 0 0.002 - 0.003 NT

Sweet Corn, Frozen 41 0 0.002 - 0.003 NT

TOTAL 2,346 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

EX2 = Exempt from the requirement of a tolerance in or on all food commodities when used to control insect larvae.

EX3 = Exempt from the requirement of a tolerance when applied to growing crops, in accordance with good agricultural practice.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 Acequinocyl in strawberries analyzed as the hydroxy metabolite.

2 Emamectin benzoate is the salt form of the active, Emamectin.

3 Halosulfuron methyl is the salt form of the active, Halosulfuron.

Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

4 isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

5 Specific tolerance established for methamidophos in celery as a possible result of an acephate application.

6 Specific tolerance established for methamidophos in green beans as a possible result of an acephate application.

7 Propamocarb analytically determined as the salt (hydrochloride).

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

page 1 in Appendix L to see the sample origin (domestic, imported, or unknown) for each occurrence.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 2 through 4 in Appendix L to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2014 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix B. Page 127 of 127
Appendix C

Distribution of Residues by Pesticide

in Oats 

Appendix C shows residue detections for all compounds tested in oats, including range of values 

detected, range of Limits of Detection (LODs), and U.S. Environmental Protection Agency (EPA) 

tolerance references for each pair. The EPA tolerances cited in this summary and appendices 

apply to 2014 and not to the current year. There may be instances where tolerances have been 

recently set, modifi ed, or revoked that would have an effect on whether a residue is violative or 

not. 

In 2014, the Pesticide Data Program (PDP) analyzed 314 oat samples. PDP detected just one 

pesticide in the oat samples, the insecticide Piperonyl butoxide, at a concentration of 0.007 ppm 

where the established tolerance was 8 ppm.

Results for environmental contaminants across all commodities, including oats, have been 

consolidated in a separate appendix because they have no registered uses and are not applied 

to crops (see Appendix G). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Acephate I 286 0.050 ^ 0.02

Acetamiprid I 314 0.025 ^ 0.01

Acetochlor H 314 0.20 ^ 0.05

Alachlor H 314 0.20 ^ 0.05

Azinphos methyl I 314 0.30 ^ NT

Azinphos methyl oxygen analog IM 314 0.050 ^ NT

Azoxystrobin F 314 0.25 ^ 1.5

Bendiocarb I 314 0.025 ^ SU

Benoxacor S 314 0.10 ^ 0.01

Bifenthrin I 314 0.025 ^ 0.05

Boscalid F 314 0.010 ^ 0.20

Captan F 314 0.20 ^ 0.05

Carbaryl I 267 0.025 ^ NT

Carbendazim (MBC) F 314 0.025 ^ NT

Carbofuran I 314 0.010 ^ 0.2

Carboxin F 314 0.20 ^ 0.2

Carfentrazone ethyl H 314 0.025 ^ 0.10

Chlorantraniliprole I 314 0.050 ^ 6.0

Chlorfenapyr I 314 0.010 ^ 0.01

Chlorpyrifos I 314 0.025 ^ 0.1

Clothianidin I 314 0.025 ^ 0.01

Cyfluthrin I 314 0.10 ^ 0.15

Cyhalothrin, Lambda I 314 0.020 ^ 0.05

Cypermethrin I 314 0.10 ^ 3.0

Cyproconazole F 314 0.050 ^ NT

Dichlorvos (DDVP) I 314 0.25 ^ 0.5

Difenoconazole F 314 0.25 ^ 0.01

Diflubenzuron I 284 0.20 ^ 0.06

Dinotefuran I 314 0.025 ^ 0.01

Diuron H 314 0.10 ^ 0.1

Esfenvalerate+Fenvalerate Total I 314 0.050 ^ 0.05

Fenamidone F 198 0.40 ^ 0.1

Fenbuconazole F 314 0.050 ^ NT

Fenpropathrin I 314 0.050 ^ NT

Fenpyroximate A 314 0.005 ^ NT

Florasulam H 314 0.075 ^ 0.01

Flufenacet H 314 0.20 ^ 0.1

Fluometuron H 314 0.050 ^ 0.5

Fluoxastrobin F 314 0.005 ^ NT

Fluridone H 314 0.40 ^ 0.1

Fluvalinate I 314 0.025 ^ NT

Hexythiazox I 314 0.050 ^ NT

APPENDIX C. DISTRIBUTION OF RESIDUES BY PESTICIDE IN OATS

Appendix C. Page 1 of 3
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

3-Hydroxycarbofuran IM 314 0.025 ^ 0.2

Imidacloprid I 314 0.025 ^ 0.05

Lindane (BHC gamma) I 314 0.10 ^ 0.1

Malathion I 284 0.10 ^ 8

Malathion oxygen analog IM 314 0.50 ^ 8

Metalaxyl/Mefenoxam * F 314 0.025 ^ 0.2

Metconazole F 314 0.20 ^ 1.0

Methamidophos I 314 0.050 ^ 0.02

Methomyl I 314 0.050 ^ 1

Methoxyfenozide I 314 0.025 ^ NT

Metolachlor H 314 0.10 ^ 0.10

MGK-264 I 314 0.20 ^ 5

Myclobutanil F 314 0.025 ^ 0.03

1-Naphthol IM 314 0.25 ^ NT

Parathion methyl I 314 0.050 ^ 1.0

Permethrin Total I 314 0.40 ^ NT

Phenothrin I 314 0.40 ^ 0.01

Phorate oxygen analog IM 314 0.025 ^ NT

Phosmet I 314 0.050 ^ NT

Piperonyl butoxide I 314 1 0.3 0.007 ^ 0.005 ^ 8

Pirimiphos methyl I 314 0.10 ^ NT

Prallethrin I 314 0.050 ^ 1.0

Propargite I 314 0.075 ^ NT

Propetamphos I 314 0.10 ^ 0.1

Propiconazole F 314 0.25 ^ 3.0

Prosulfuron H 314 0.050 ^ 0.01

Prothioconazole F 204 0.50 ^ 0.35

Pyraclostrobin F 314 0.005 ^ 1.2

Pyrasulfotole H 314 0.050 ^ 0.08

Pyrethrins I 314 0.40 ^ 1.0

Pyriproxyfen I 314 0.005 ^ 1.1

Resmethrin I 314 0.40 ^ 3.0

Rimsulfuron H 284 0.050 ^ NT

Saflufenacil H 314 0.12 ^ 0.03

Spinetoram I 314 0.050 ^ 0.04

Spinosad I 314 0.40 ^ 1.5

Spiromesifen I 314 0.005 ^ 0.03

Spirotetramat I 314 0.010 ^ NT

TCMTB F 314 0.050 ^ 0.1

Tebuconazole F 314 0.025 ^ 0.15

Tefluthrin I 314 0.005 ^ NT

Tetraconazole F 314 0.10 ^ NT

Tetrahydrophthalimide (THPI) FM 314 0.25 ^ 0.05

Thiamethoxam I 314 0.025 ^ 0.02

Appendix C. Page 2 of 3
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Trifloxystrobin F 314 0.050 ^ 0.05

Trifluralin H 314 0.005 ^ NT

Triticonazole F 286 0.20 ^ 0.01

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

NT = No tolerance level was set for that pesticide/commodity pair.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

S = Herbicide Safener

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply 

to 2014 and not to the current year. There may be instances where a tolerance was recently set or revoked that 

Appendix C. Page 3 of 3
Appendix D

Distribution of Residues by Pesticide

in Rice 

Appendix D shows residue detections for all compounds tested in rice, including range of 

values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this 

summary and appendices apply to 2014 and not to the current year. There may be 

instances where tolerances have been recently set, modifi ed, or revoked that would have 

an effect on whether a residue is violative or not. 

In 2014, the Pesticide Data Program (PDP) analyzed 314 rice samples. PDP detected 

fi ve different residues (including metabolites), representing fi ve pesticides, in the rice 

samples. All residue detections were lower than the established tolerances for those 

compounds with established tolerances.

The Pesticide Data Program reports tolerance violations to the U.S. Food and Drug 

Administration (FDA) as part of an interagency Memorandum of Understanding between 

the U.S. Department of Agriculture and FDA. Residues reported to FDA are shown in 

the “Pesticide/Commodity” column to the right of the commodity and are annotated as 

“X” (if the residue exceeded the established tolerance) or “V” (if the residue did not have 

a tolerance listed in the Code of Federal Regulations, Title 40, Part 180). In both cases, 

these annotations are followed by a number indicating the number of samples reported 

to FDA. 

Results for environmental contaminants across all commodities, including rice, have been 

consolidated in a separate appendix because they have no registered uses and are not 

applied to crops (see Appendix G). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Acephate I 314 0.050 ^ 0.02

Acetamiprid I 314 0.025 ^ 0.01

Acetochlor H 314 0.20 ^ 0.05

Azinphos methyl I 314 0.30 ^ NT

Azinphos methyl oxygen analog IM 314 0.050 ^ NT

Azoxystrobin F 314 0.25 ^ 5.0

Bendiocarb I 314 0.025 ^ SU

Benoxacor S 314 0.10 ^ 0.01

Bifenthrin I 314 0.025 ^ 0.05

Boscalid F 314 0.010 ^ 0.20

Buprofezin I 314 0.10 ^ NT

Captan F 314 0.20 ^ 0.05

Carbaryl I 300 0.025 ^ 15

Carbendazim (MBC) F 314 0.025 ^ NT

Carbofuran I 314 0.010 ^ 0.2

Carboxin F 314 0.20 ^ 0.2

Carfentrazone ethyl H 314 0.025 ^ 0.10

Chlorantraniliprole I 314 0.050 ^ 0.15

Chlorfenapyr I 279 0.010 ^ 0.01

Chlorpyrifos I 314 0.025 ^ 0.1

Chlorpyrifos methyl I 314 0.025 ^ 6.0

Clothianidin I 314 0.025 ^ 0.01

Cyfluthrin I 314 0.10 ^ 0.05

Cyhalothrin, Lambda I 314 0.020 ^ 1.0

Cypermethrin I 314 0.10 ^ 1.50

Cyproconazole F 314 0.050 ^ NT

Diazinon I 314 0.050 ^ NT

Diazinon oxygen analog IM 314 0.050 ^ NT

Dichlorvos (DDVP) I 314 0.25 ^ 0.5

Difenoconazole F 314 0.25 ^ NT

Diflubenzuron I 300 0.20 ^ 0.02

Dinotefuran I 314 3 1 0.037 - 0.0485 0.025 ^ 9.0

Diuron H 314 0.10 ^ NT

Esfenvalerate+Fenvalerate Total I 314 0.050 ^ 0.05

Etofenprox I 314 0.050 ^ 0.01

Fenbuconazole F 314 0.050 ^ NT

Fenoxaprop ethyl H 314 0.005 ^ 0.05

Fenpropathrin I 314 0.050 ^ NT

Fenpyroximate A 314 0.005 ^ NT

Fipronil I 314 0.20 ^ 0.04

Fluometuron H 314 0.050 ^ 0.5

Fluoxastrobin F 314 0.005 ^ 4.0

APPENDIX D. DISTRIBUTION OF RESIDUES BY PESTICIDE IN RICE

Appendix D. Page 1 of 3
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fluridone H 314 0.40 ^ 0.1

Flutolanil F 314 0.10 ^ 7.0

Fluvalinate I 314 0.025 ^ NT

Hexythiazox I 314 0.050 ^ NT

3-Hydroxycarbofuran IM 314 0.025 ^ 0.2

Imidacloprid I 314 0.025 ^ 0.05

Lindane (BHC gamma) I 314 0.10 ^ 0.1

Malathion I 314 0.10 ^ 8

Malathion oxygen analog IM 314 0.50 ^ 8

Metalaxyl/Mefenoxam * F 314 0.025 ^ 0.1

Metconazole F 314 0.20 ^ NT

Methamidophos I 314 0.050 ^ 0.02

Methomyl I 314 0.050 ^ NT

Methoxyfenozide I 314 0.025 ^ NT

Metolachlor H 314 0.10 ^ 0.10

MGK-264 I 314 1 0.3 0.48 ^ 0.20 ^ 5

Molinate H 314 0.050 ^ NT

Myclobutanil F 285 0.025 ^ 0.03

1-Naphthol IM 314 0.25 ^ 15

Parathion methyl I 314 0.050 ^ 1.0

Pendimethalin H 314 0.10 ^ 0.1

Permethrin Total I 314 0.40 ^ NT

Phenothrin I 314 0.40 ^ 0.01

Phosmet I 314 0.050 ^ NT

Phosmet oxygen analog IM 314 0.025 ^ NT

Piperonyl butoxide I 314 35 11.1 0.005 - 0.30 0.005 ^ 20

Pirimiphos methyl I 314 0.10 ^ NT

Prallethrin I 314 0.050 ^ 1.0

Propanil H 314 0.20 ^ 10

Propargite I 314 0.075 ^ NT

Propetamphos I 313 0.10 ^ 0.1

Propiconazole F 300 0.25 ^ 7.0

Prothioconazole F 300 0.50 ^ 0.35

Pyraclostrobin F 314 0.005 ^ NT

Pyrasulfotole H 314 0.050 ^ NT

Pyrethrins I 314 0.40 ^ 3.0

Pyriproxyfen I 314 0.005 ^ 1.1

Resmethrin I 314 0.40 ^ 3.0

Rimsulfuron H 314 0.050 ^ NT

Saflufenacil H 314 0.12 ^ 0.03

Spinosad I 314 0.40 ^ 1.5

Spirotetramat I 300 0.010 ^ NT

TCMTB F 314 0.050 ^ 0.1

Tebuconazole (V-1) F 314 1 0.3 0.0378 ^ 0.025 ^ NT

Appendix D. Page 2 of 3
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tefluthrin I 314 0.005 ^ NT

Tetraconazole F 300 0.10 ^ NT

Tetrahydrophthalimide (THPI) FM 314 0.25 ^ 0.05

Thiamethoxam I 314 0.025 ^ 0.02

Thiobencarb H 314 0.050 ^ 0.2

Tricyclazole F 314 5 1.6 0.0708 - 0.12 0.050 ^ 3.0

Trifloxystrobin F 314 0.050 ^ 3.5

Trifluralin H 314 0.005 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

NT = No tolerance level was set for that pesticide/commodity pair.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. 

 Refer to pages 2 through 4 in Appendix L to see the number of occurrences broken down by sample origin

 (domestic, imported, or unknown) for a commodity/pesticide pair.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

S = Herbicide Safener

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply 

to 2014 and not to the current year. There may be instances where a tolerance was recently set or revoked that 

Appendix D. Page 3 of 3
Appendix E

Distribution of Residues by Pesticide

in Infant Formula

Appendix E shows residue detections for all compounds tested in dairy-based and soybased infant formula, including range of values detected, range of Limits of Detection 

(LODs), and U.S. Environmental Protection Agency (EPA) tolerance references for each 

pair. The EPA tolerances cited in this summary and appendices apply to 2014 and not 

to the current year. There may be instances where tolerances have been recently set, 

modifi ed, or revoked that would have an effect on whether a residue is violative or not. 

In 2014, the Pesticide Data Program (PDP) analyzed 528 dairy-based formula samples 

and 527 soy-based formula samples. PDP detected just one pesticide in seven infant 

formula samples; the insecticide synergist MGK-264, at a concentration of 0.003 ppm 

where the established tolerance was 5 ppm.

Results for environmental contaminants across all commodities, including infant formula, 

have been consolidated in a separate appendix because they have no registered uses 

and are not applied to crops (see Appendix G). 
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Abamectin (I)

 Infant Formula, Soy-based 527 0.020 ^ 0.01

Acephate (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.1

 Infant Formula, Soy-based 527 0.010 ^ 1.0

Acetamiprid (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.30

 Infant Formula, Soy-based 527 0.003 ^ 0.03

Acetochlor (H)

 Infant Formula, Soy-based 527 0.005 ^ 1.0

Acibenzolar S methyl (L)

 Infant Formula, Dairy-based 488 0.004 - 0.012 NT

Alachlor (H)

 Infant Formula, Dairy-based 528 0.002 ^ 0.02

 Infant Formula, Soy-based 527 0.005 ^ NT

Aldicarb (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ 0.02

Aldicarb sulfone (IM)

 Infant Formula, Dairy-based 528 0.003 - 0.010 NT

 Infant Formula, Soy-based 527 0.010 ^ 0.02

Aldicarb sulfoxide (IM)

 Infant Formula, Dairy-based 528 0.002 - 0.012 NT

 Infant Formula, Soy-based 527 0.010 ^ 0.02

Allethrin (I)

 Infant Formula, Soy-based 527 0.020 ^ EX

Ametoctradin (F)

 Infant Formula, Soy-based 527 0.003 ^ NT

Ametryn (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Atrazine (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

 Infant Formula, Soy-based 527 0.005 ^ NT

Azinphos ethyl (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Azinphos methyl (I)

 Infant Formula, Dairy-based 528 0.012 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Azinphos methyl oxygen analog (IM)

 Infant Formula, Soy-based 527 0.010 ^ NT

Azoxystrobin (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.006

 Infant Formula, Soy-based 527 0.003 ^ 0.5

Bendiocarb (I)

 Infant Formula, Dairy-based 528 0.001 ^ SU

 Infant Formula, Soy-based 527 0.005 ^ SU

Benfluralin (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Benoxacor (S)

 Infant Formula, Dairy-based 528 0.001 ^ 0.01

 Infant Formula, Soy-based 527 0.010 ^ 0.01

Bensulide (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

APPENDIX E. DISTRIBUTION OF RESIDUES BY PESTICIDE IN INFANT FORMULA

Appendix E. Page 1 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bifenox (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Bifenthrin (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.1

 Infant Formula, Soy-based 527 0.010 ^ 0.2

Bitertanol (F)

 Infant Formula, Soy-based 527 0.040 ^ NT

Boscalid (F)

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Bromacil (H)

 Infant Formula, Soy-based 527 0.010 ^ NT

Bromopropylate (A)

 Infant Formula, Soy-based 527 0.010 ^ NT

Bromuconazole (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Bupirimate (F)

 Infant Formula, Soy-based 527 0.040 ^ NT

Buprofezin (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.01

 Infant Formula, Soy-based 527 0.005 ^ NT

Cadusafos (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Carbaryl (I)

 Infant Formula, Dairy-based 528 0.001 ^ 1.0

 Infant Formula, Soy-based 527 0.005 ^ 0.5

Carbendazim (MBC) (F)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.2

Carbofuran (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.1

 Infant Formula, Soy-based 527 0.005 ^ 1.0

Carbophenothion (I)

 Infant Formula, Dairy-based 488 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Carbophenothion methyl (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Carboxin (F)

 Infant Formula, Soy-based 527 0.005 ^ 0.2

Carfentrazone ethyl (H)

 Infant Formula, Dairy-based 528 0.005 - 0.015 0.05

 Infant Formula, Soy-based 527 0.003 ^ 0.10

Chlorantraniliprole (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.1

 Infant Formula, Soy-based 527 0.010 ^ 2.0

Chlorethoxyfos (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Chlorfenapyr (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.01

Chlorfenvinphos (I)

 Infant Formula, Dairy-based 528 0.004 - 0.012 NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Chlorobenzilate (A)

 Infant Formula, Soy-based 527 0.003 ^ NT

Chloroneb (F)

 Infant Formula, Soy-based 527 0.005 ^ 0.2

Appendix E. Page 2 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Chlorothalonil (F)

 Infant Formula, Soy-based 498 0.010 ^ 0.2

Chlorpropham (H)

 Infant Formula, Dairy-based 528 0.001 - 0.003 0.30

 Infant Formula, Soy-based 527 0.005 ^ NT

Chlorpyrifos (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.01

 Infant Formula, Soy-based 527 0.010 ^ 0.3

Chlorpyrifos oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.001 ^ 0.01

 Infant Formula, Soy-based 527 0.010 ^ 0.3

Clethodim (H)

 Infant Formula, Dairy-based 528 0.002 ^ 0.05

Clofentezine (I)

 Infant Formula, Soy-based 527 0.020 ^ NT

Clomazone (H)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ 0.05

Clothianidin (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.01

 Infant Formula, Soy-based 527 0.005 ^ 0.02

Coumaphos (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Coumaphos oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.008 ^ NT

Crotoxyphos (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Crufomate (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Cyazofamid (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Cyfluthrin (I)

 Infant Formula, Dairy-based 528 0.008 ^ 0.2

 Infant Formula, Soy-based 527 0.005 ^ 0.03

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (I)

 Infant Formula, Dairy-based 528 0.003 ^ 0.4

 Infant Formula, Soy-based 527 0.010 ^ 0.01

Cymoxanil (F)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Cypermethrin (I)

 Infant Formula, Dairy-based 528 0.022 ^ 0.10

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Cyphenothrin (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Cyproconazole (F)

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Cyprodinil (F)

 Infant Formula, Soy-based 527 0.003 ^ 0.6

DCPA (H)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ 2.0

DEF (Tribufos) (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Appendix E. Page 3 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Deltamethrin (includes parent Tralomethrin) (I)

 Infant Formula, Dairy-based 528 0.012 - 0.040 0.02

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Demeton-O (IM)

 Infant Formula, Soy-based 527 0.020 ^ NT

Demeton-S (IM)

 Infant Formula, Soy-based 527 0.030 ^ NT

Demeton-S sulfone (IM)

 Infant Formula, Soy-based 527 0.003 ^ NT

Dialifos (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Diazinon (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Diazinon oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Dichlobenil (H)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Dichlorvos (DDVP) (I)

 Infant Formula, Dairy-based 528 0.003 ^ 0.02

 Infant Formula, Soy-based 527 0.020 ^ 0.5

Dicloran (F)

 Infant Formula, Dairy-based 508 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Dicofol o,p' (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.75

 Infant Formula, Soy-based 527 0.010 ^ 0.5

Dicofol p,p' (I)

 Infant Formula, Dairy-based 528 0.001 - 0.003 0.75

 Infant Formula, Soy-based 527 0.005 ^ 0.5

Dicrotophos (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Diethofencarb (F)

 Infant Formula, Soy-based 527 0.003 ^ NT

Difenoconazole (F)

 Infant Formula, Dairy-based 528 0.003 ^ 0.01

 Infant Formula, Soy-based 527 0.005 ^ 0.15

Diflubenzuron (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.05

 Infant Formula, Soy-based 527 0.020 ^ 0.05

Dimethenamid (H)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Dimethoate (I)

 Infant Formula, Dairy-based 508 0.002 - 0.008 0.002

 Infant Formula, Soy-based 527 0.003 ^ 0.05

Dimethomorph (F)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Diniconazole (F)

 Infant Formula, Soy-based 527 0.020 ^ NT

Dinotefuran (I)

 Infant Formula, Dairy-based 528 0.006 ^ 0.05

 Infant Formula, Soy-based 527 0.010 ^ 0.01

Appendix E. Page 4 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Dioxathion (I)

 Infant Formula, Soy-based 527 0.020 ^ NT

Diphenamid (H)

 Infant Formula, Dairy-based 528 0.002 ^ NT

Diphenylamine (DPA) (F)

 Infant Formula, Dairy-based 528 0.003 - 0.010 0.01

 Infant Formula, Soy-based 527 0.003 ^ NT

Disulfoton (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Disulfoton oxon (IM)

 Infant Formula, Dairy-based 528 0.002 ^ NT

Disulfoton sulfone (IM)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Disulfoton sulfone oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.003 ^ NT

Disulfoton sulfoxide (IM)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Disulfoton sulfoxide oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.001 ^ NT

Diuron (H)

 Infant Formula, Dairy-based 528 0.008 ^ NT

 Infant Formula, Soy-based 527 0.020 ^ NT

DMST (4-dimethylaminosulphotosluidide) (FM)

 Infant Formula, Soy-based 527 0.003 ^ NT

Dodine (F)

 Infant Formula, Soy-based 527 0.020 ^ NT

Emamectin (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Emamectin benzoate (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.003

Endosulfan I (IM)

 Infant Formula, Dairy-based 528 0.006 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ 2.0

Endosulfan II (IM)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ 2.0

Endosulfan sulfate (IM)

 Infant Formula, Dairy-based 528 0.012 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 2.0

Epoxiconazole (F)

 Infant Formula, Soy-based 527 0.005 ^ NT

EPTC (H)

 Infant Formula, Dairy-based 528 0.001 ^ NT

Esfenvalerate+Fenvalerate Total (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.3

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Ethalfluralin (H)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Ethion (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Appendix E. Page 5 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Ethion mono oxon (IM)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Ethofumesate (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Ethoprop (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Ethylan (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Etofenprox (I)

 Infant Formula, Soy-based 497 0.003 ^ 5.0

Etoxazole (A)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Etridiazole (F)

 Infant Formula, Soy-based 527 0.020 ^ 0.1

Famoxadone (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Fenamidone (F)

 Infant Formula, Dairy-based 508 0.002 ^ 0.02

 Infant Formula, Soy-based 527 0.010 ^ 0.02

Fenamiphos (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Fenamiphos sulfone (IM)

 Infant Formula, Dairy-based 528 0.004 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Fenamiphos sulfoxide (IM)

 Infant Formula, Dairy-based 528 0.004 ^ NT

 Infant Formula, Soy-based 527 0.020 ^ NT

Fenarimol (F)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Fenazaquin (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Fenbuconazole (F)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Fenchlorphos (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Fenhexamid (F)

 Infant Formula, Dairy-based 59 0.030 ^ NT

 Infant Formula, Soy-based 527 0.040 ^ NT

Fenitrothion (I)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Fenobucarb (BPMC) (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Fenpropathrin (I)

 Infant Formula, Dairy-based 528 0.003 ^ 0.08

 Infant Formula, Soy-based 527 0.005 ^ NT

Fenpropimorph (F)

 Infant Formula, Soy-based 527 0.003 ^ NT

Fenpyroximate (A)

 Infant Formula, Dairy-based 528 0.001 - 0.003 0.015

Appendix E. Page 6 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fensulfothion (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Fenthion (I)

 Infant Formula, Dairy-based 528 0.002 - 0.016 NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Fipronil (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.05

Flonicamid (I)

 Infant Formula, Dairy-based 528 0.001 - 0.003 0.05

 Infant Formula, Soy-based 527 0.030 ^ NT

Fluazifop butyl (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.05

 Infant Formula, Soy-based 527 0.003 ^ 2.5

Fludioxonil (F)

 Infant Formula, Dairy-based 528 0.012 - 0.040 0.01

 Infant Formula, Soy-based 527 0.010 ^ 0.4

Flufenacet (H)

 Infant Formula, Soy-based 527 0.010 ^ 0.1

Flufenoxuron (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Flumioxazin (H)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.020 ^ 0.02

Fluopicolide (F)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Fluoxastrobin (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.03

 Infant Formula, Soy-based 527 0.003 ^ 0.05

Fluquinconazole (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Fluridone (H)

 Infant Formula, Soy-based 527 0.003 ^ 0.1

Flusilazole (F)

 Infant Formula, Soy-based 527 0.003 ^ 0.04

Flutolanil (F)

 Infant Formula, Soy-based 527 0.003 ^ 0.20

Flutriafol (F)

 Infant Formula, Soy-based 527 0.010 ^ 0.35

Fluvalinate (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Fonofos (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Forchlorfenuron (P)

 Infant Formula, Soy-based 527 0.003 ^ NT

Formetanate hydrochloride (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Fosthiazate (T)

 Infant Formula, Soy-based 527 0.003 ^ NT

Hexaconazole (F)

 Infant Formula, Soy-based 527 0.020 ^ NT

Hexythiazox (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Appendix E. Page 7 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Hydroprene (R)

 Infant Formula, Dairy-based 59 0.002 ^ 0.2

 Infant Formula, Soy-based 527 0.010 ^ 0.2

3-Hydroxycarbofuran (IM)

 Infant Formula, Dairy-based 528 0.001 - 0.004 0.1

 Infant Formula, Soy-based 527 0.010 ^ 1.0

5-Hydroxythiabendazole (FM)

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Imazalil (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

 Infant Formula, Soy-based 527 0.005 ^ NT

Imidacloprid (I)

 Infant Formula, Dairy-based 528 0.003 ^ 0.10

 Infant Formula, Soy-based 527 0.010 ^ 0.3

Imiprothrin (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Indaziflam (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Indoxacarb (I)

 Infant Formula, Soy-based 527 0.010 ^ 0.80

Iprodione (F)

 Infant Formula, Dairy-based 59 0.009 ^ 0.5

 Infant Formula, Soy-based 527 0.005 ^ 2.0

Iprovalicarb (F)

 Infant Formula, Soy-based 527 0.005 ^ NT

Isofenphos (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Isoprocarb (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Isoproturon (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Kresoxim-methyl (F)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Lactofen (H)

 Infant Formula, Soy-based 527 0.005 ^ 0.01

Lenacil (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Leptophos oxygen analog (IM)

 Infant Formula, Soy-based 527 0.020 ^ NT

Lindane (BHC gamma) (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.3

 Infant Formula, Soy-based 527 0.003 ^ 0.5 AL

Linuron (H)

 Infant Formula, Dairy-based 528 0.003 ^ 0.05

 Infant Formula, Soy-based 527 0.010 ^ 1.0

Malathion (I)

 Infant Formula, Dairy-based 528 0.001 - 0.003 0.5

 Infant Formula, Soy-based 527 0.005 ^ 8

Malathion oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.010 ^ 0.5

 Infant Formula, Soy-based 527 0.003 ^ 8

Mandipropamid (F)

 Infant Formula, Dairy-based 528 0.015 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Appendix E. Page 8 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Melamine (RM)

 Infant Formula, Dairy-based 469 0.015 ^ 0.05

Mepanipyrim (F)

 Infant Formula, Soy-based 527 0.005 ^ NT

Metalaxyl/Mefenoxam (F) *

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

 Infant Formula, Soy-based 527 0.003 ^ 1.0

Metconazole (F)

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Methamidophos (I)

 Infant Formula, Dairy-based 528 0.004 ^ 0.1

 Infant Formula, Soy-based 527 0.005 ^ 1.0

Methidathion (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Methiocarb (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Methiocarb sulfoxide (IM)

 Infant Formula, Soy-based 527 0.005 ^ NT

Methomyl (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.020 ^ 2

Methoprene (R)

 Infant Formula, Dairy-based 528 0.050 ^ EX2

Methoxychlor Total (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

Methoxychlor olefin (IM)

 Infant Formula, Dairy-based 528 0.001 ^ NT

Methoxychlor p,p' (IM)

 Infant Formula, Soy-based 527 0.005 ^ NT

Methoxyfenozide (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.10

 Infant Formula, Soy-based 527 0.005 ^ 1.0

Metolachlor (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

 Infant Formula, Soy-based 527 0.003 ^ 0.20

Metribuzin (H)

 Infant Formula, Dairy-based 528 0.002 ^ 0.05

 Infant Formula, Soy-based 527 0.005 ^ 0.3

Mevinphos (I)

 Infant Formula, Dairy-based 528 0.005 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

MGK-264 (I)

 Infant Formula, Soy-based 527 7 1.3 0.003 ^ 0.003 ^ 5

Monocrotophos (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Myclobutanil (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.2

 Infant Formula, Soy-based 527 0.010 ^ 0.25

Napropamide (H)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Nitrofen (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Appendix E. Page 9 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Norflurazon (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.1

 Infant Formula, Soy-based 527 0.010 ^ 0.1

Norflurazon desmethyl (HM)

 Infant Formula, Dairy-based 528 0.001 ^ 0.1

 Infant Formula, Soy-based 527 0.010 ^ 0.1

Novaluron (I)

 Infant Formula, Dairy-based 489 0.001 - 0.006 1.0

 Infant Formula, Soy-based 527 0.080 ^ 0.07

Omethoate (IM)

 Infant Formula, Dairy-based 528 0.002 ^ 0.002

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Oxadiazon (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Oxadixyl (F)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Oxamyl (I)

 Infant Formula, Dairy-based 528 0.002 - 0.012 NT

 Infant Formula, Soy-based 527 0.010 ^ 0.1

Oxamyl oxime (IM)

 Infant Formula, Soy-based 527 0.020 ^ 0.1

Oxydemeton methyl (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Oxydemeton methyl sulfone (IM)

 Infant Formula, Dairy-based 528 0.012 ^ 0.01

 Infant Formula, Soy-based 527 0.005 ^ NT

Oxyfluorfen (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.01

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Paclobutrazol (P)

 Infant Formula, Soy-based 527 0.010 ^ NT

Parathion (I)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Parathion methyl (I)

 Infant Formula, Dairy-based 528 0.002 - 0.008 NT

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Parathion methyl oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.005 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ 0.1

Parathion oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.003 - 0.010 NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Penconazole (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Pencycuron (F)

 Infant Formula, Soy-based 527 0.005 ^ NT

Pendimethalin (H)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.10

Pentachloroaniline (PCA) (FM)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ 0.1

Appendix E. Page 10 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Pentachlorobenzene (PCB) (FM)

 Infant Formula, Dairy-based 528 0.008 - 0.015 NT

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Pentachlorophenyl methyl sulfide (FM)

 Infant Formula, Dairy-based 59 0.003 ^ NT

Penthiopyrad (F)

 Infant Formula, Soy-based 527 0.003 ^ 0.40

Permethrin cis (IM)

 Infant Formula, Dairy-based 528 0.001 ^ 0.88

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Permethrin trans (IM)

 Infant Formula, Dairy-based 528 0.001 ^ 0.88

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Phenothrin (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.01

 Infant Formula, Soy-based 527 0.005 ^ 0.01

Phenthoate (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Phorate (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Phorate oxygen analog (IM)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Phorate sulfone (IM)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Phorate sulfoxide (IM)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Phosalone (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Phosmet (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Phosphamidon (I)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Phoxim (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Piperonyl butoxide (I)

 Infant Formula, Dairy-based 528 0.005 ^ 0.25

Pirimicarb (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Pirimicarb desmethyl (IM)

 Infant Formula, Soy-based 527 0.003 ^ NT

Pirimiphos methyl (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Prallethrin (I)

 Infant Formula, Soy-based 527 0.020 ^ 1.0

Prochloraz (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Appendix E. Page 11 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Procymidone (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Profenofos (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.01

 Infant Formula, Soy-based 527 0.005 ^ NT

Profluralin (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Promecarb (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Prometryn (H)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Pronamide (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

 Infant Formula, Soy-based 527 0.003 ^ NT

Propachlor (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

Propamocarb hydrochloride (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Propanil (H)

 Infant Formula, Soy-based 527 0.010 ^ NT

Propaquizafop (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Propargite (I)

 Infant Formula, Dairy-based 528 0.006 ^ 0.08

 Infant Formula, Soy-based 527 0.005 ^ 0.2

Propetamphos (I)

 Infant Formula, Dairy-based 528 0.002 ^ 0.1

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Propham (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Propiconazole (F)

 Infant Formula, Dairy-based 528 0.008 ^ 0.05

 Infant Formula, Soy-based 527 0.010 ^ 2.0

Prothiofos (I)

 Infant Formula, Soy-based 527 0.010 ^ NT

Pymetrozine (I)

 Infant Formula, Dairy-based 528 0.005 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Pyraclostrobin (F)

 Infant Formula, Dairy-based 528 0.004 ^ 0.1

 Infant Formula, Soy-based 527 0.003 ^ 0.04

Pyraflufen ethyl (H)

 Infant Formula, Soy-based 527 0.003 ^ 0.01

Pyrazophos (F)

 Infant Formula, Soy-based 527 0.005 ^ NT

Pyridaben (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Pyrimethanil (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.05

 Infant Formula, Soy-based 527 0.005 ^ NT

Pyriproxyfen (I)

 Infant Formula, Dairy-based 528 0.003 ^ 0.10

 Infant Formula, Soy-based 527 0.003 ^ 0.20

Quinalphos (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Appendix E. Page 12 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Quinoxyfen (F)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Quintozene (PCNB) (F)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Quizalofop ethyl (H)

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Resmethrin (I)

 Infant Formula, Soy-based 527 0.010 ^ 3.0

Resmethrin cis (IM)

 Infant Formula, Dairy-based 528 0.002 ^ 3.0

Resmethrin trans (IM)

 Infant Formula, Dairy-based 528 0.002 ^ 3.0

Rotenone (I)

 Infant Formula, Soy-based 527 0.040 ^ NT

Sethoxydim (H)

 Infant Formula, Soy-based 527 0.005 ^ 16

Simazine (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.03

 Infant Formula, Soy-based 527 0.005 ^ NT

Spinetoram (I)

 Infant Formula, Dairy-based 528 0.001 ^ 0.30

 Infant Formula, Soy-based 527 0.010 ^ 0.04

Spinosad (I)

 Infant Formula, Dairy-based 528 0.001 ^ 7.0

 Infant Formula, Soy-based 527 0.003 ^ 0.02

Spirodiclofen (A)

 Infant Formula, Soy-based 527 0.005 ^ NT

Spiromesifen Total (parent + enol metabolite) (I)

 Infant Formula, Dairy-based 59 0.002 ^ 0.01

Spiromesifen (I)

 Infant Formula, Soy-based 527 0.005 ^ 0.02

Spirotetramat (I)

 Infant Formula, Soy-based 527 0.003 ^ 5.0

Spiroxamine (F)

 Infant Formula, Soy-based 527 0.003 ^ NT

Sulfallate (H)

 Infant Formula, Soy-based 527 0.005 ^ NT

Sulfentrazone (H)

 Infant Formula, Soy-based 527 0.010 ^ 0.15

Sulprofos (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Tebuconazole (F)

 Infant Formula, Dairy-based 528 0.002 ^ 0.1

 Infant Formula, Soy-based 527 0.010 ^ 0.08

Tebufenozide (I)

 Infant Formula, Dairy-based 528 0.010 ^ 0.04

 Infant Formula, Soy-based 527 0.005 ^ NT

Tebufenpyrad (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Tebuthiuron (H)

 Infant Formula, Dairy-based 528 0.001 ^ 0.8

 Infant Formula, Soy-based 527 0.003 ^ NT

Appendix E. Page 13 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tecnazene (P)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Tefluthrin (I)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.003 ^ NT

Terbacil (H)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Terbufos (I)

 Infant Formula, Soy-based 527 0.003 ^ NT

Terbufos sulfone (IM)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Terbuthylazine (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Tetrachlorvinphos (I)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Tetraconazole (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.03

 Infant Formula, Soy-based 527 0.010 ^ 0.15

Tetradifon (I)

 Infant Formula, Dairy-based 528 0.002 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Tetrahydrophthalimide (THPI) (FM)

 Infant Formula, Dairy-based 528 0.004 ^ 0.10

 Infant Formula, Soy-based 527 0.010 ^ 0.05

Tetramethrin (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Thiabendazole (F)

 Infant Formula, Dairy-based 508 0.001 ^ 0.1

 Infant Formula, Soy-based 527 0.005 ^ 0.1

Thiacloprid (I)

 Infant Formula, Dairy-based 528 0.003 ^ 0.030

 Infant Formula, Soy-based 527 0.003 ^ NT

Thiamethoxam (I)

 Infant Formula, Dairy-based 528 0.005 - 0.015 0.02

 Infant Formula, Soy-based 527 0.003 ^ 0.02

Thiobencarb (H)

 Infant Formula, Dairy-based 528 0.003 ^ 0.05

 Infant Formula, Soy-based 527 0.010 ^ NT

Thiodicarb (I)

 Infant Formula, Soy-based 527 0.010 ^ 0.2

Thionazin (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Tolclofos methyl (F)

 Infant Formula, Soy-based 527 0.010 ^ NT

Tri Allate (H)

 Infant Formula, Soy-based 527 0.003 ^ NT

Triadimefon (F)

 Infant Formula, Dairy-based 528 0.003 ^ NT

 Infant Formula, Soy-based 527 0.010 ^ NT

Triadimenol (F)

 Infant Formula, Soy-based 527 0.030 ^ NT

Appendix E. Page 14 of 15
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Triazophos (I)

 Infant Formula, Soy-based 527 0.005 ^ NT

Trifloxystrobin (F)

 Infant Formula, Dairy-based 528 0.001 ^ 0.02

 Infant Formula, Soy-based 527 0.003 ^ 0.08

Triflumizole (F)

 Infant Formula, Soy-based 527 0.005 ^ NT

Trifluralin (H)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ 0.05

Triticonazole (F)

 Infant Formula, Soy-based 527 0.040 ^ NT

Uniconazole (R)

 Infant Formula, Soy-based 527 0.040 ^ NT

Vinclozolin (F)

 Infant Formula, Dairy-based 528 0.001 ^ NT

 Infant Formula, Soy-based 527 0.005 ^ NT

Zoxamide (F)

 Infant Formula, Soy-based 527 0.003 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

EX2 = Exempt from the requirement of a tolerance in or on all food commodities when used to control insect larvae.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

AL = Number shown is an Action Level established by U.S. Food and Drug Administration. Under the Food Quality 

 Protection Act, responsibility for establishing tolerances in lieu of action levels has been transferred to EPA. 

 In the interim, action levels are used.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

L = Plant Activator

P = Plant Growth Regulator

R = Insect Growth Regulator, RM = Insect Growth Regulator Metabolite

S = Herbicide Safener

T = Nematicide

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2014 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix E. Page 15 of 15
Appendix F

Distribution of Residues by Pesticide

in Salmon

Appendix F shows residue detections for all compounds tested in salmon, including range 

of values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this summary 

and appendices apply to 2014 and not to the current year. There may be instances where 

tolerances have been recently set, modifi ed or revoked that would have an effect on whether 

a residue is violative or not. 

In 2014, the Pesticide Data Program (PDP) analyzed 354 salmon samples. PDP detected 

just one pesticide in one salmon sample, the insecticide Lufenuron, at a concentration of 

0.028 part per million. 

Results for environmental contaminants across all commodities, including salmon, have 

been consolidated in a separate appendix because they have no registered uses and are not 

applied to crops (see Appendix G). PDP detected two environmental contaminants, DDT p,p’ 

and Mirex, in the salmon samples.
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Acetamiprid I 354 0.002 ^ 0.01

Acetochlor H 354 0.005 ^ NA

Acrinathrin I 354 0.010 ^ NA

Atrazine H 295 0.002 ^ NA

Azinphos methyl I 354 0.010 ^ NA

Azinphos methyl oxygen analog IM 354 0.010 ^ NA

Azoxystrobin F 354 0.002 ^ NA

Bendiocarb I 354 0.003 ^ SU

Benfluralin H 354 0.010 ^ NA

Benoxacor S 354 0.010 ^ NA

Bensulide H 354 0.004 ^ NA

Bensulide oxygen analog HM 354 0.002 ^ NA

Bifenthrin I 354 0.005 ^ 0.05

Boscalid F 354 0.003 ^ NA

Bromacil H 354 0.003 ^ NA

Carbaryl I 237 0.003 ^ NA

Carbendazim (MBC) F 325 0.001 ^ NA

Carbofuran I 354 0.002 ^ NA

Carfentrazone ethyl H 354 0.005 ^ 0.30

Chlorantraniliprole I 354 0.010 ^ NA

Chlorfenapyr I 354 0.015 ^ 0.01

Chlorpropham H 354 0.020 ^ NA

Chlorpyrifos I 354 0.005 ^ 0.1

Chlorpyrifos oxygen analog IM 354 0.002 ^ 0.1

Clomazone H 354 0.005 ^ NA

Clothianidin I 354 0.010 ^ 0.02

Coumaphos I 354 0.010 ^ NA

Coumaphos oxygen analog IM 354 0.010 ^ NA

Cyfluthrin I 354 0.004 ^ 0.05

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) I 354 0.005 ^ 0.01

Cymoxanil F 295 0.005 ^ NA

Cypermethrin I 354 0.010 ^ 0.05

Cyphenothrin I 354 0.015 ^ NA

DCPA H 354 0.002 ^ NA

DEF (Tribufos) H 354 0.002 ^ NA

Deltamethrin (includes parent Tralomethrin) I 354 0.015 ^ 0.05

Diazinon I 354 0.005 ^ NA

Dichlobenil H 354 0.010 ^ NA

Dichlorvos (DDVP) I 295 0.020 ^ 0.5

Diclofop methyl H 354 0.001 ^ NA

APPENDIX F. DISTRIBUTION OF RESIDUES BY PESTICIDE IN SALMON

Appendix F. Page 1 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Dicloran F 354 0.016 ^ NA

Dicofol p,p' I 354 0.010 ^ NA

Diflubenzuron I 354 0.002 ^ NA

Dimethenamid H 354 0.002 ^ NA

Diphenylamine (DPA) F 354 0.002 ^ NA

Disulfoton oxygen analog IM 354 0.001 ^ NA

Disulfoton sulfone IM 354 0.020 ^ NA

Disulfoton sulfoxide IM 354 0.005 ^ NA

Diuron H 266 0.002 ^ 2.0 1

Endosulfan I IM 354 0.010 ^ NA

Endosulfan II IM 354 0.015 ^ NA

Endosulfan sulfate IM 354 0.005 ^ NA

Esfenvalerate+Fenvalerate Total I 324 0.005 ^ 0.05

Ethalfluralin H 354 0.005 ^ NA

Ethion I 354 0.001 ^ NA

Ethion mono oxon IM 354 0.001 ^ NA

Ethoprop I 30 0.002 ^ NA

Famoxadone F 354 0.025 ^ NA

Fenamidone F 325 0.005 ^ NA

Fenbuconazole F 354 0.005 ^ NA

Fenhexamid F 354 0.013 ^ NA

Fenpropathrin I 354 0.020 ^ NA

Fenpyroximate A 354 0.005 ^ NA

Fipronil sulfone (MB46136) IM 354 0.050 ^ NA

Flonicamid I 324 0.006 ^ NA

Flubendiamide I 354 0.035 ^ NA

Fludioxonil F 354 0.025 ^ NA

Flufenoxuron I 354 0.001 ^ NA

Flumioxazin H 354 0.010 ^ 1.5 2

Fluopicolide F 354 0.015 ^ NA

Fluquinconazole F 354 0.010 ^ NA

Fluridone H 295 0.001 ^ 0.5

Flusilazole F 325 0.010 ^ NA

Flutolanil F 354 0.002 ^ NA

Flutriafol F 265 0.010 ^ NA

Fluvalinate I 354 0.050 ^ NA

Hexythiazox I 354 0.002 ^ NA

3-Hydroxycarbofuran IM 354 0.003 ^ NA

Imidacloprid I 354 0.003 ^ 0.05

Imiprothrin I 354 0.010 ^ NA

Indaziflam H 265 0.001 ^ NA

Appendix F. Page 2 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Indoxacarb I 354 0.020 ^ NA

Iprodione F 354 0.040 ^ NA

Kresoxim-methyl F 354 0.010 ^ NA

Lindane (BHC gamma) I 354 0.013 ^ NA

Linuron H 354 0.003 ^ NA

Lufenuron I 354 1 0.3 0.028 ^ 0.020 ^ NA

Malathion I 354 0.002 ^ NA

Malathion oxygen analog IM 354 0.002 ^ NA

Mandipropamid F 354 0.002 ^ NA

Metalaxyl/Mefenoxam * F 354 0.001 ^ NA

Methidathion I 354 0.010 ^ NA

Methiocarb sulfone IM 354 0.001 ^ NA

Methiocarb sulfoxide IM 354 0.001 ^ NA

Methomyl I 177 0.030 ^ NA

Methoxyfenozide I 354 0.003 ^ NA

Metolachlor H 354 0.001 ^ NA

Metribuzin H 354 0.005 ^ NA

Mevinphos Total I 354 0.002 ^ NA

MGK-264 I 354 0.10 ^ 5

Myclobutanil F 354 0.003 ^ NA

Napropamide H 295 0.005 ^ NA

Norflurazon H 354 0.002 ^ NA

Norflurazon desmethyl HM 354 0.005 ^ NA

Oryzalin H 354 0.020 ^ NA

Oxadiazon H 354 0.010 ^ NA

Oxydemeton methyl sulfone IM 354 0.002 ^ NA

Oxyfluorfen H 354 0.050 ^ NA

Paclobutrazol P 354 0.010 ^ NA

Parathion ethyl I 354 0.005 ^ NA

Parathion methyl I 354 0.010 ^ NA

Parathion methyl oxygen analog IM 354 0.020 ^ NA

Pendimethalin H 354 0.050 ^ NA

Pentachloroaniline (PCA) FM 354 0.004 ^ NA

Pentachlorobenzene (PCB) FM 354 0.005 ^ NA

Pentachlorophenyl methyl sulfide FM 354 0.005 ^ NA

Permethrin cis IM 354 0.010 ^ NA

Permethrin trans IM 354 0.010 ^ NA

Phenothrin I 354 0.050 ^ 0.01

o-Phenylphenol F 354 0.005 ^ NA

Phorate I 354 0.010 ^ NA

Phorate oxygen analog IM 354 0.010 ^ NA

Appendix F. Page 3 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Phorate sulfone IM 354 0.010 ^ NA

Phorate sulfoxide IM 354 0.010 ^ NA

Phosalone I 354 0.001 ^ NA

Phosmet I 354 0.010 ^ NA

Piperonyl butoxide I 354 0.005 ^ NA

Pirimiphos methyl I 325 0.001 ^ NA

Pronamide H 354 0.002 ^ NA

Propargite I 354 0.050 ^ NA

Propetamphos I 354 0.010 ^ 0.1

Propiconazole F 325 0.010 ^ NA

Pyraclostrobin F 354 0.003 ^ NA

Pyraflufen ethyl H 354 0.010 ^ NA

Pyridaben I 354 0.005 ^ NA

Pyrimethanil F 354 0.050 ^ NA

Pyriproxyfen I 354 0.001 ^ 0.10

Quinoxyfen F 354 0.020 ^ NA

Quintozene (PCNB) F 354 0.004 ^ NA

Resmethrin cis IM 354 0.050 ^ 3.0

Resmethrin trans IM 354 0.050 ^ 3.0

Saflufenacil H 354 0.010 ^ NA

Sethoxydim H 325 0.003 ^ NA

Simazine H 354 0.005 ^ NA

Spirodiclofen A 354 0.010 ^ NA

Spiromesifen I 325 0.010 ^ NA

Tebufenozide I 354 0.002 ^ NA

Tebufenpyrad I 354 0.010 ^ NA

Tefluthrin I 354 0.002 ^ NA

Terbacil H 354 0.010 ^ NA

Terbutryn H 354 0.025 ^ NA

Tetraconazole F 354 0.010 ^ NA

Tetradifon I 354 0.010 ^ NA

Tetrahydrophthalimide (THPI) FM 354 0.010 ^ NA

Tetramethrin I 354 0.005 ^ NA

Thiacloprid I 354 0.001 ^ NA

Thiamethoxam I 354 0.003 ^ 0.02

Thiazopyr H 354 0.008 ^ NA

Thiobencarb H 354 0.010 ^ NA

Triazophos I 354 0.001 ^ NA

Trichlorfon I 354 0.010 ^ NA

Trifloxystrobin F 354 0.002 ^ NA

Trifloxysulfuron H 354 0.020 ^ NA

Appendix F. Page 4 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Trifluralin H 354 0.001 ^ NA

Triforine F 354 0.010 ^ NA

Vinclozolin F 354 0.010 ^ NA

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

NA = Findings in salmon are covered by tolerances established for fish, by tolerances set for pesticide uses in food 

 handling establishments, and by action levels set for persistent chemicals commonly found in the environment.

 In addition, there are other findings that may arise from a number of attributable sources including runoff from

 agricultural uses to water sources or ponds. For the latter group, where no specific tolerance has been

 established, “NA” has been entered as the tolerance value.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 = Specific tolerance for Diuron in freshwater, farm-raised finfish.

2 = Specific tolerance for Flumioxazin in freshwater fish.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

P = Plant Growth Regulator

S = Herbicide Safener

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is advised 

to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply to 2014 

and not to the current year. There may be instances where a tolerance was recently set or revoked that would 

have an effect on whether a residue is violative or not. 

Appendix F. Page 5 of 5
Appendix G

Distribution of Residues 

for Environmental Contaminants

Appendix G shows residue detections across all commodities for 22 compounds identifi ed as 

environmental contaminants, including range of values detected, range of Limits of Detection 

(LODs), and U.S. Environmental Protection Agency (EPA) tolerances or Action Levels for each 

pair. Results for environmental contaminants have been consolidated in this appendix because 

they have no registered uses and are not applied to crops.

The EPA tolerances cited in this summary and appendices apply to 2014 and not to the current 

year. There may be instances where tolerances have been recently set, modifi ed or revoked 

that would have an effect on whether a residue is violative or not.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by the U.S. Food and Drug Administration (FDA). Under the Food Quality Protection 

Act, responsibility for establishing tolerances in lieu of ALs has been transferred to EPA. In the 

interim, ALs are used.

The Pesticide Data Program reports tolerance violations to the U.S. Food and Drug Administration 

(FDA) as part of an interagency Memorandum of Understanding between the U.S. Department 

of Agriculture and FDA. Residues reported to FDA are shown in the “Pesticide/Commodity” 

column to the right of the commodity and are annotated as “X” (if the residue exceeded the 

established tolerance) or “V” (if the residue did not have a tolerance listed in the Code of 

Federal Regulations, Title 40, Part 180). In both cases, these annotations are followed by a 

number indicating the number of samples reported to FDA.
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Aldrin (insecticide) (parent of Dieldrin)

Apples 177 0 0.003 ^ 0.03 AL

Bananas 179 0 0.040 ^ 0.02 AL

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.041 0.05 AL

Blueberries, Frozen 19 0 0.005 - 0.041 0.05 AL

Broccoli 712 0 0.005 ^ 0.03 AL

Carrots 708 0 0.002 ^ 0.1 AL

Celery 708 0 0.001 - 0.005 0.03 AL

Cherries, Fresh 228 0 0.041 ^ 0.3 AL

Cherries, Frozen 282 0 0.041 ^ 0.3 AL

Fish, Salmon 354 0 0.003 ^ 0.3 AL

Grape Juice 531 0 0.003 ^ 0.05 AL

Green Beans, Fresh 757 0 0.010 ^ 0.05 AL

Green Beans, Canned 378 0 0.001 ^ 0.05 AL

Green Beans, Frozen 378 0 0.001 ^ 0.05 AL

Infant Formula, Dairy-based 59 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.005 ^ 0.05 AL

Nectarines 681 0 0.002 ^ 0.02 AL

Oats 314 0 0.15 ^ 0.02 AL

Peaches 707 0 0.005 ^ 0.02 AL

Rice 314 0 0.15 ^ 0.02 AL

Strawberries 176 0 0.005 ^ 0.05 AL

Summer Squash 531 0 0.005 - 0.020 0.1 AL

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.02 AL

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.02 AL

Tomatoes 177 0 0.001 ^ 0.05 AL

Watermelon 390 0 0.003 ^ 0.1 AL

TOTAL 10,150 0

BHC alpha (insecticide) (isomer of BHC)

Apples 177 0 0.012 ^ 0.05 AL

Bananas 179 0 0.007 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.007 0.05 AL

Blueberries, Frozen 19 0 0.003 - 0.007 0.05 AL

Broccoli 712 0 0.005 ^ NT

Carrots 708 0 0.001 ^ 0.3 AL

Celery 708 0 0.001 - 0.003 0.05 AL

Cherries, Fresh 228 0 0.007 ^ 0.05 AL

Cherries, Frozen 282 0 0.007 ^ 0.05 AL

Fish, Salmon 354 0 0.012 ^ NA

Grape Juice 531 0 0.012 ^ 0.05 AL

Green Beans, Fresh 757 0 0.020 - 0.20 0.05 AL

Green Beans, Canned 378 0 0.001 ^ 0.05 AL

Green Beans, Frozen 378 0 0.001 ^ 0.05 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.05 AL

Nectarines 681 0 0.001 ^ 0.05 AL

Oats 314 0 0.15 ^ 0.05 AL

Peaches 707 0 0.005 ^ 0.05 AL

Rice 314 0 0.15 ^ 0.05 AL

Strawberries 176 0 0.003 ^ 0.05 AL

Summer Squash 531 0 0.003 - 0.20 0.05 AL

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.05 AL

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.05 AL

Tomatoes 177 0 0.001 ^ 0.05 AL

Watermelon 390 0 0.012 ^ 0.05 AL

TOTAL 10,619 0

APPENDIX G. DISTRIBUTION OF RESIDUES FOR ENVIRONMENTAL CONTAMINANTS

Appendix G. Page 1 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

BHC beta (isomer of BHC)

Apples 177 0 0.014 ^ 0.05 AL

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 0.05 AL

Blueberries, Frozen 5 0 0.003 ^ 0.05 AL

Carrots 708 4 0.6 0.002 ^ 0.001 ^ 0.3 AL

Celery 348 0 0.003 ^ 0.05 AL

Fish, Salmon 354 0 0.014 ^ NA

Grape Juice 531 0 0.014 ^ 0.05 AL

Green Beans, Fresh 757 0 0.020 - 0.20 0.05 AL

Infant Formula, Soy-based 527 0 0.003 ^ 0.05 AL

Nectarines 681 0 0.001 ^ 0.05 AL

Oats 314 0 0.30 ^ 0.05 AL

Peaches 707 0 0.005 ^ 0.05 AL

Rice 314 0 0.30 ^ 0.05 AL

Strawberries 176 0 0.003 ^ 0.05 AL

Summer Squash 531 0 0.003 - 0.20 0.05 AL

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.05 AL

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.05 AL

Watermelon 390 0 0.014 ^ 0.05 AL

TOTAL 7,049 4

BHC delta (isomer of BHC)

Blueberries, Cultivated, Fresh 354 0 0.005 ^ 0.05 AL

Blueberries, Frozen 5 0 0.005 ^ 0.05 AL

Celery 348 0 0.005 ^ 0.05 AL

Infant Formula, Soy-based 527 0 0.005 ^ 0.05 AL

Strawberries 176 0 0.005 ^ 0.05 AL

Summer Squash 270 0 0.005 ^ 0.05 AL

Sweet Corn, Fresh 78 0 0.005 ^ 0.05 AL

Sweet Corn, Frozen 12 0 0.005 ^ 0.05 AL

TOTAL 1,770 0

BHC epsilon (isomer of BHC)

Blueberries, Cultivated, Fresh 354 0 0.005 ^ 0.05 AL

Blueberries, Frozen 5 0 0.005 ^ 0.05 AL

Celery 348 0 0.005 ^ 0.05 AL

Infant Formula, Soy-based 527 0 0.005 ^ 0.05 AL

Strawberries 176 0 0.005 ^ 0.05 AL

Summer Squash 270 0 0.005 ^ 0.05 AL

Sweet Corn, Fresh 78 0 0.005 ^ 0.05 AL

Sweet Corn, Frozen 12 0 0.005 ^ 0.05 AL

TOTAL 1,770 0

Chlordane Total (insecticide) 

Carrots 708 5 0.7 0.017 ^ 0.010 ^ 0.1 AL

Nectarines 681 0 0.010 ^ 0.1 AL

TOTAL 1,389 5

Chlordane cis (isomer of Chlordane)

Apples 177 0 0.010 ^ 0.1 AL

Bananas 179 0 0.005 ^ 0.1 AL

Blueberries, Cultivated, Fresh 688 0 0.005 ^ 0.1 AL

Blueberries, Frozen 19 0 0.005 ^ 0.1 AL

Broccoli 712 0 0.005 ^ 0.1 AL

Celery 708 0 0.001 - 0.005 0.1 AL

Cherries, Fresh 228 0 0.005 ^ 0.1 AL

Cherries, Frozen 282 0 0.005 ^ 0.1 AL

Fish, Salmon 354 0 0.010 ^ 0.3 AL

Grape Juice 531 0 0.010 ^ 0.1 AL

Green Beans, Fresh 757 0 0.025 ^ 0.1 AL

Green Beans, Canned 378 0 0.001 ^ 0.1 AL

Green Beans, Frozen 378 0 0.001 ^ 0.1 AL

Appendix G. Page 2 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.005 ^ 0.1 AL

Peaches 707 0 0.005 ^ 0.1 AL

Strawberries 176 0 0.005 ^ 0.1 AL

Summer Squash 531 8 1.5 0.006 - 0.019 0.005 - 0.050 0.1 AL

Sweet Corn, Fresh 134 0 0.005 - 0.025 0.1 AL

Sweet Corn, Frozen 41 0 0.005 - 0.025 0.1 AL

Tomatoes 177 0 0.001 ^ 0.1 AL

Watermelon 390 0 0.010 ^ 0.1 AL

TOTAL 8,602 8

Chlordane trans (isomer of Chlordane)

Apples 177 0 0.010 ^ 0.1 AL

Bananas 179 0 0.005 ^ 0.1 AL

Blueberries, Cultivated, Fresh 688 0 0.005 ^ 0.1 AL

Blueberries, Frozen 19 0 0.005 ^ 0.1 AL

Broccoli 712 0 0.005 ^ 0.1 AL

Celery 708 0 0.001 - 0.005 0.1 AL

Cherries, Fresh 228 0 0.005 ^ 0.1 AL

Cherries, Frozen 282 0 0.005 ^ 0.1 AL

Fish, Salmon 354 0 0.010 ^ 0.3 AL

Grape Juice 531 0 0.010 ^ 0.1 AL

Green Beans, Fresh 757 0 0.010 ^ 0.1 AL

Green Beans, Canned 378 0 0.001 ^ 0.1 AL

Green Beans, Frozen 378 0 0.001 ^ 0.1 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.005 ^ 0.1 AL

Peaches 707 0 0.005 ^ 0.1 AL

Strawberries 176 0 0.005 ^ 0.1 AL

Summer Squash 531 4 0.8 0.006 - 0.029 0.005 - 0.025 0.1 AL

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.1 AL

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.1 AL

Tomatoes 177 0 0.001 ^ 0.1 AL

Watermelon 390 0 0.010 ^ 0.1 AL

TOTAL 8,602 4

DDD o,p' (metabolite of DDT)

Apples 177 0 0.001 ^ 0.1 AL

Blueberries, Cultivated, Fresh 354 0 0.003 ^ 0.1 AL

Blueberries, Frozen 5 0 0.003 ^ 0.1 AL

Celery 708 0 0.001 - 0.003 0.5 AL

Fish, Salmon 354 0 0.001 ^ 5 AL

Grape Juice 531 0 0.001 ^ 0.05 AL

Green Beans, Canned 378 0 0.001 ^ 0.2 AL

Green Beans, Frozen 378 0 0.001 ^ 0.2 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.2 AL

Oats 314 0 0.050 ^ 0.5 AL

Rice 314 0 0.050 ^ 0.5 AL

Strawberries 176 0 0.003 ^ 0.1 AL

Summer Squash 270 1 0.4 0.003 ^ 0.003 ^ 0.1 AL

Sweet Corn, Fresh 78 0 0.003 ^ 0.1 AL

Sweet Corn, Frozen 12 0 0.003 ^ 0.1 AL

Tomatoes 177 0 0.001 ^ 0.05 AL

Watermelon 390 0 0.001 ^ 0.1 AL

TOTAL 5,671 1

DDD p,p' (metabolite of DDT)

Apples 177 0 0.005 ^ 0.1 AL

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 0.1 AL

Blueberries, Frozen 19 0 0.003 - 0.005 0.1 AL

Appendix G. Page 3 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 712 0 0.005 ^ 0.5 AL

Celery 708 0 0.001 - 0.003 0.5 AL

Cherries, Fresh 228 0 0.005 ^ 0.2 AL

Cherries, Frozen 282 0 0.005 ^ 0.2 AL

Fish, Salmon 354 0 0.005 ^ 5 AL

Grape Juice 531 0 0.005 ^ 0.05 AL

Green Beans, Fresh 757 0 0.025 ^ 0.2 AL

Green Beans, Canned 378 0 0.001 ^ 0.2 AL

Green Beans, Frozen 378 0 0.001 ^ 0.2 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.2 AL

Oats 314 0 0.075 ^ 0.5 AL

Peaches 707 0 0.005 ^ 0.2 AL

Rice 314 0 0.075 ^ 0.5 AL

Strawberries 176 0 0.003 ^ 0.1 AL

Summer Squash 531 1 0.2 0.003 ^ 0.003 - 0.050 0.1 AL

Sweet Corn, Fresh 134 0 0.003 - 0.025 0.1 AL

Sweet Corn, Frozen 41 0 0.003 - 0.025 0.1 AL

Tomatoes 177 0 0.001 ^ 0.05 AL

Watermelon 390 0 0.005 ^ 0.1 AL

TOTAL 9,230 1

DDE o,p' (metabolite of DDT)

Apples 177 0 0.001 ^ 0.1 AL

Blueberries, Cultivated, Fresh 354 0 0.005 ^ 0.1 AL

Blueberries, Frozen 5 0 0.005 ^ 0.1 AL

Carrots 708 1 0.1 0.003 ^ 0.002 ^ 3 AL

Celery 348 0 0.005 ^ 0.5 AL

Fish, Salmon 354 0 0.001 ^ 5 AL

Grape Juice 531 0 0.001 ^ 0.05 AL

Infant Formula, Soy-based 527 0 0.005 ^ 0.2 AL

Nectarines 681 0 0.002 ^ 0.2 AL

Oats 314 0 0.020 ^ 0.5 AL

Rice 314 0 0.020 ^ 0.5 AL

Strawberries 176 0 0.005 ^ 0.1 AL

Summer Squash 270 0 0.005 ^ 0.1 AL

Sweet Corn, Fresh 78 0 0.005 ^ 0.1 AL

Sweet Corn, Frozen 12 0 0.005 ^ 0.1 AL

Watermelon 390 0 0.001 ^ 0.1 AL

TOTAL 5,239 1

DDE p,p' (metabolite of DDT)

Apples 177 0 0.010 ^ 0.1 AL

Bananas 179 0 0.005 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.005 0.1 AL

Blueberries, Frozen 19 0 0.003 - 0.005 0.1 AL

Broccoli 712 0 0.005 ^ 0.5 AL

Carrots 708 175 24.7 0.003 - 0.066 0.002 ^ 3 AL

Celery 708 75 10.6 0.002 - 0.006 0.001 - 0.003 0.5 AL

Cherries, Fresh 228 0 0.005 ^ 0.2 AL

Cherries, Frozen 282 0 0.005 ^ 0.2 AL

Fish, Salmon 354 0 0.010 ^ 5 AL

Grape Juice 531 0 0.010 ^ 0.05 AL

Green Beans, Fresh 757 1 0.1 0.009 ^ 0.005 ^ 0.2 AL

Green Beans, Canned 378 0 0.001 ^ 0.2 AL

Green Beans, Frozen 378 4 1.1 0.002 ^ 0.001 ^ 0.2 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.2 AL

Nectarines 681 0 0.002 ^ 0.2 AL

Oats 314 0 0.025 ^ 0.5 AL

Peaches 707 0 0.005 ^ 0.2 AL

Rice 314 0 0.025 ^ 0.5 AL

Appendix G. Page 4 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Strawberries 176 0 0.003 ^ 0.1 AL

Summer Squash 531 16 3 0.003 - 0.011 0.003 - 0.005 0.1 AL

Sweet Corn, Fresh 134 0 0.003 - 0.010 0.1 AL

Sweet Corn, Frozen 41 0 0.003 - 0.010 0.1 AL

Tomatoes 157 0 0.001 ^ 0.05 AL

Watermelon 390 0 0.010 ^ 0.1 AL

TOTAL 10,599 271

DDT o,p' (insecticide) 

Blueberries, Cultivated, Fresh 325 0 0.003 ^ 0.1 AL

Blueberries, Frozen 4 0 0.003 ^ 0.1 AL

Carrots 708 30 4.2 0.002 - 0.004 0.001 ^ 3 AL

Celery 650 0 0.001 - 0.003 0.5 AL

Green Beans, Canned 378 0 0.001 ^ 0.2 AL

Green Beans, Frozen 378 0 0.001 ^ 0.2 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.2 AL

Nectarines 681 0 0.001 ^ 0.2 AL

Oats 314 0 0.075 ^ 0.5 AL

Rice 314 0 0.050 ^ 0.5 AL

Strawberries 176 0 0.003 ^ 0.1 AL

Summer Squash 240 5 2.1 0.003 - 0.012 0.003 - 0.010 0.1 AL

Sweet Corn, Fresh 78 0 0.003 ^ 0.1 AL

Sweet Corn, Frozen 12 0 0.003 ^ 0.1 AL

Tomatoes 177 0 0.001 ^ 0.05 AL

TOTAL 5,490 35

DDT p,p' (insecticide) 

Apples 177 0 0.001 ^ 0.1 AL

Bananas 179 0 0.076 ^ NT

Blueberries, Cultivated, Fresh 659 0 0.003 - 0.075 0.1 AL

Blueberries, Frozen 18 0 0.003 - 0.075 0.1 AL

Broccoli 712 0 0.005 ^ 0.5 AL

Carrots 708 67 9.5 0.002 - 0.007 0.001 ^ 3 AL

Celery 679 2 0.3 0.002 ^ 0.001 - 0.003 0.5 AL

Cherries, Fresh 228 0 0.075 ^ 0.2 AL

Cherries, Frozen 282 0 0.075 ^ 0.2 AL

Fish, Salmon 354 7 2 0.001 - 0.003 0.001 ^ 5 AL

Grape Juice 531 0 0.001 ^ 0.05 AL

Green Beans, Canned 378 0 0.001 ^ 0.2 AL

Green Beans, Frozen 378 0 0.001 ^ 0.2 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.2 AL

Nectarines 681 0 0.001 ^ 0.2 AL

Oats 314 0 0.050 ^ 0.5 AL

Peaches 707 0 0.005 ^ 0.2 AL

Rice 314 0 0.075 ^ 0.5 AL

Strawberries 176 0 0.003 ^ 0.1 AL

Summer Squash 270 13 4.8 0.003 - 0.011 0.003 - 0.010 0.1 AL

Sweet Corn, Fresh 78 0 0.003 ^ 0.1 AL

Sweet Corn, Frozen 12 0 0.003 ^ 0.1 AL

Tomatoes 177 0 0.001 ^ 0.05 AL

Watermelon 390 0 0.001 ^ 0.1 AL

TOTAL 9,457 89

Dieldrin (insecticide) (also a metabolite of Aldrin)

Apples 177 0 0.010 ^ 0.03 AL

Bananas 179 0 0.020 ^ 0.02 AL

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.040 0.05 AL

Blueberries, Frozen 19 0 0.010 - 0.040 0.05 AL

Broccoli 712 0 0.005 ^ 0.03 AL

Carrots 708 22 3.1 0.007 - 0.017 0.004 ^ 0.1 AL

Appendix G. Page 5 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 708 0 0.002 - 0.010 0.03 AL

Cherries, Fresh 228 0 0.040 ^ 0.3 AL

Cherries, Frozen 282 0 0.040 ^ 0.3 AL

Fish, Salmon 354 0 0.010 ^ 0.3 AL

Grape Juice 531 0 0.010 ^ 0.05 AL

Green Beans, Fresh 725 0 0.025 ^ 0.05 AL

Green Beans, Canned 378 0 0.002 ^ 0.05 AL

Green Beans, Frozen 378 0 0.002 ^ 0.05 AL

Infant Formula, Dairy-based 528 0 0.002 ^ NT

Infant Formula, Soy-based 527 0 0.010 ^ 0.05 AL

Nectarines 681 0 0.004 ^ 0.02 AL

Oats 314 0 0.10 ^ 0.02 AL

Peaches 707 0 0.005 ^ 0.02 AL

Rice 314 0 0.10 ^ 0.02 AL

Strawberries 176 0 0.010 ^ 0.05 AL

Summer Squash 531 16 3 0.010 - 0.076 0.010 - 0.050 0.1 AL

Sweet Corn, Fresh 134 0 0.010 - 0.025 0.02 AL

Sweet Corn, Frozen 41 0 0.010 - 0.025 0.02 AL

Tomatoes 177 0 0.002 ^ 0.05 AL

Watermelon 390 0 0.010 ^ 0.1 AL

TOTAL 10,587 38

Endrin (insecticide) 

Apples 177 0 0.010 ^ 0.03 AL

Bananas 179 0 0.031 ^ 0.02 AL

Blueberries, Cultivated, Fresh 688 0 0.010 - 0.031 0.05 AL

Blueberries, Frozen 19 0 0.010 - 0.031 0.05 AL

Broccoli 712 0 0.005 ^ 0.03 AL

Celery 708 0 0.008 - 0.010 0.03 AL

Cherries, Fresh 228 0 0.031 ^ 0.03 AL

Cherries, Frozen 282 0 0.031 ^ 0.03 AL

Fish, Salmon 354 0 0.010 ^ 0.3 AL

Grape Juice 531 0 0.010 ^ 0.05 AL

Green Beans, Fresh 757 0 0.003 - 0.030 0.05 AL

Green Beans, Canned 378 0 0.008 ^ 0.05 AL

Green Beans, Frozen 378 0 0.008 ^ 0.05 AL

Infant Formula, Dairy-based 528 0 0.008 ^ NT

Infant Formula, Soy-based 527 0 0.010 ^ 0.05 AL

Oats 314 0 0.15 ^ 0.02 AL

Peaches 707 0 0.005 ^ 0.02 AL

Rice 314 0 0.15 ^ 0.02 AL

Strawberries 176 0 0.010 ^ 0.05 AL

Summer Squash 531 0 0.010 - 0.062 0.1 AL

Sweet Corn, Fresh 134 0 0.010 - 0.030 0.02 AL

Sweet Corn, Frozen 41 0 0.010 - 0.030 0.02 AL

Tomatoes 177 0 0.005 ^ 0.05 AL

Watermelon 390 0 0.010 ^ 0.1 AL

TOTAL 9,230 0

Heptachlor (insecticide) 

Apples 177 0 0.002 ^ 0.01 AL

Bananas 179 0 0.049 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.003 - 0.10 0.05 AL

Blueberries, Frozen 19 0 0.003 - 0.10 0.05 AL

Broccoli 712 0 0.005 ^ 0.01 AL

Carrots 708 0 0.001 ^ 0.01 AL

Celery 708 0 0.001 - 0.003 0.05 AL

Cherries, Fresh 228 0 0.10 ^ 0.05 AL

Cherries, Frozen 282 0 0.10 ^ 0.05 AL

Fish, Salmon 354 0 0.002 ^ 0.3 AL

Grape Juice 531 0 0.002 ^ 0.05 AL

Green Beans, Fresh 757 0 0.005 ^ 0.01 AL

Appendix G. Page 6 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans, Canned 378 0 0.001 ^ 0.01 AL

Green Beans, Frozen 378 0 0.001 ^ 0.01 AL

Infant Formula, Dairy-based 528 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.05 AL

Nectarines 681 0 0.001 ^ 0.05 AL

Oats 314 0 0.10 ^ 0.01 AL

Peaches 707 0 0.005 ^ 0.05 AL

Rice 314 0 0.10 ^ 0.03 AL

Strawberries 176 0 0.003 ^ 0.05 AL

Summer Squash 531 0 0.003 - 0.015 0.05 AL

Sweet Corn, Fresh 134 0 0.003 - 0.005 0.01 AL

Sweet Corn, Frozen 41 0 0.003 - 0.005 0.01 AL

Tomatoes 177 0 0.001 ^ 0.01 AL

Watermelon 390 0 0.002 ^ 0.05 AL

TOTAL 10,619 0

Heptachlor epoxide (metabolite of Heptachlor)

Apples 177 0 0.005 ^ 0.01 AL

Bananas 179 0 0.041 ^ NT

Blueberries, Cultivated, Fresh 688 0 0.005 - 0.040 0.05 AL

Blueberries, Frozen 19 0 0.005 - 0.040 0.05 AL

Broccoli 712 0 0.005 ^ 0.01 AL

Celery 708 0 0.004 - 0.005 0.05 AL

Cherries, Fresh 228 0 0.040 ^ 0.05 AL

Cherries, Frozen 282 0 0.040 ^ 0.05 AL

Fish, Salmon 354 0 0.005 ^ 0.3 AL

Grape Juice 531 0 0.005 ^ 0.05 AL

Green Beans, Fresh 757 0 0.010 ^ 0.01 AL

Green Beans, Canned 378 0 0.004 ^ 0.01 AL

Green Beans, Frozen 378 0 0.004 ^ 0.01 AL

Infant Formula, Dairy-based 528 0 0.004 ^ NT

Infant Formula, Soy-based 527 0 0.005 ^ 0.05 AL

Oats 314 0 0.25 ^ 0.01 AL

Peaches 707 0 0.005 ^ 0.05 AL

Rice 314 0 0.25 ^ 0.03 AL

Strawberries 176 0 0.005 ^ 0.05 AL

Summer Squash (X-1) 531 7 1.3 0.007 - 0.079 0.005 - 0.010 0.05 AL

Sweet Corn, Fresh 134 0 0.005 - 0.010 0.01 AL

Sweet Corn, Frozen 41 0 0.005 - 0.010 0.01 AL

Tomatoes 177 0 0.002 ^ 0.01 AL

Watermelon 390 0 0.005 ^ 0.05 AL

TOTAL 9,230 7

Heptachlor epoxide cis (metabolite of Heptachlor)

Carrots 708 1 0.1 0.007 ^ 0.004 ^ 0.01 AL

Nectarines 681 0 0.004 ^ 0.05 AL

TOTAL 1,389 1

Hexachlorobenzene - HCB (metabolite and impurity of Quintozene)

Blueberries, Cultivated, Fresh 354 0 0.003 ^ NT

Blueberries, Frozen 5 0 0.003 ^ NT

Broccoli 712 0 0.005 ^ 0.1

Carrots 708 0 0.002 ^ NT

Celery 708 0 0.001 - 0.003 NT

Green Beans, Fresh 286 0 0.050 ^ 0.1

Infant Formula, Dairy-based 59 0 0.001 ^ NT

Infant Formula, Soy-based 527 0 0.003 ^ 0.1

Peaches 707 0 0.005 ^ NT

Strawberries 176 0 0.003 ^ NT

Summer Squash 531 0 0.003 - 0.10 NT

Appendix G. Page 7 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Corn, Fresh 134 0 0.003 - 0.050 NT

Sweet Corn, Frozen 41 0 0.003 - 0.050 NT

TOTAL 4,948 0

Mirex (insecticide) 

Apples 177 0 0.001 ^ NT

Fish, Salmon 354 1 0.3 0.002 ^ 0.001 ^ 0.1 AL

Grape Juice 531 0 0.001 ^ NT

Watermelon 390 0 0.001 ^ NT

TOTAL 1,452 1

Oxychlordane (metabolite of Chlordane)

Strawberries 176 0 0.005 ^ 0.1 AL

Sweet Corn, Fresh 78 0 0.005 ^ 0.1 AL

Sweet Corn, Frozen 12 0 0.005 ^ 0.1 AL

TOTAL 266 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NA = Findings in salmon are covered by tolerances established for fish, by tolerances set for pesticide uses in food handling

establishments, and by action levels set for persistent chemicals commonly found in the environment. In addition, there are

other findings that may arise from a number of attributable sources including runoff from agricultural uses to water sources or 

ponds. For the latter group, where no specific tolerance has been established, “NA” has been entered as the tolerance value.

NT = No tolerance level was set for that pesticide/commodity pair.

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

page 1 in Appendix L to see the sample origin (domestic, imported, or unknown) for each occurrence.

Appendix G. Page 8 of 8
Appendix H

Sample Origin by State or Country

(Determined by Grower, Packer, or Distributor)

Appendix H gives the number of fruit and vegetable, oats, rice, infant formula, and salmon 

samples per State or country of origin and the number of samples of unknown origin. 

Where available, the origin of fresh commodities is taken from the grower or packer 

information. For processed commodities, origin is determined primarily by packer or 

distributor.

As shown in Appendix H, fruit and vegetable, oats, rice, infant formula, and salmon 

samples originated from 39 States, 1 U.S. territory, and 31 foreign countries. There were 

74 samples from mixed national origins (multiple countries). There were 302 domestic 

samples from unknown States. There were an additional 95 samples from unknown 

origins. Overall, 75.5 percent of samples were from U.S. sources, 22.9 percent were 

imports, 0.7 percent were of mixed national origin, and 0.9 percent were of unknown 

origin.
Part 1. Domestic Samples

Fish # of % of

AP BB BN BR CB CE CH CR GB NE PC SS ST TO WM BZ CS CZ GC GJ GZ OA RI DF YF FS Samples Total

Alabama 1 1 <0.1

Alaska 7 7 0.1

Arizona 2 1 1 1 35 10 1 6 1 2 5 65 0.6

Arkansas 9 1 3 2 1 24 18 13 17 20 16 15 2 141 1.3

California 4 143 510 28 547 51 406 145 428 357 75 126 17 88 1 1 54 134 47 64 19 43 9 16 27 3340 31.5

Colorado 1 6 6 4 2 1 2 22 0.2

Connecticut 1 1 <0.1

Delaware 4 4 <0.1

Florida 36 31 32 67 155 14 51 20 35 20 1 2 6 9 17 10 9 2 2 9 528 5.0

Georgia 4 1 14 17 32 14 31 2 15 1 1 132 1.2

Idaho 1 2 1 2 1 1 4 2 9 1 24 0.2

Illinois 4 16 2 1 4 12 2 2 1 5 22 15 14 120 5 7 10 8 250 2.4

Indiana 2 1 1 3 1 1 191 182 2 384 3.6

Iowa 1 1 <0.1

Kansas 3 4 3 10 0.1

Kentucky 3 11 5 <0.1

Maine 8 1 1 10 0.1

Maryland 1 10 2 6 1 4 10 2 3 11 1 12 3 6 6 2 1 5 86 0.8

Massachusetts 1 243 244 2.3

Michigan 13 41 1 1 17 1 36 6 1 6 13 1 6 1 4 13 16 44 16 11 8 15 11 282 2.7

Minnesota 1 3 1 3 1 32 14 16 20 10 4 6 3 114 1.1

Missouri 1 1 3 3 4 4 16 0.2

Nevada 5 5 <0.1

New Hampshire 1 11 3 <0.1

New Jersey 24 2 9 5 17 10 1 1 8 7 6 44 1 19 45 78 277 2.6

New York 18 1 12 2 6 3 9 4 3 4 41 13 26 8 3 17 10 1 181 1.7

North Carolina 12 17 8 1 5 13 1 16 7 11 3 1 95 0.9

Ohio 3 1 1 2 2 18 24 19 1 7 1 4 19 17 18 22 14 12 194 163 3 545 5.1

Oregon 1 30 5 2 2 1 2 1 8 1 2 32 3 90 0.8

Pennsylvania 7 1 4 5 3 4 1 4 19 19 2 5 2 76 0.7

Puerto Rico 1 1 <0.1

Rhode Island 1 1 <0.1

South Carolina 39 5 44 0.4

Tennessee 3 2 3 20 28 0.3

Texas 1 6 16 12 21 1 13 33 2 5 26 1 5 29 1 2 2 15 11 21 8 69 3 3 3 309 2.9

Vermont 4 10 14 0.1

Virginia 1 1 10 3 3 18 0.2

Washington 119 4 5 6 113 3 4 29 23 10 1 3 1 2 3 1 26 353 3.3

West Virginia 2 2 <0.1

Wisconsin 2 12 2 7 0.1

Unknown State 2 1 9 18 8 3 8 84 7 21 38 5 60 2 2 4 3 3 3 9 10 2 302 2.8

No. of Domestic 176 304 0 628 117 676 177 556 574 482 515 319 147 79 282 9 39 107 375 463 338 284 231 520 519 101 8,018

% of Total 99 44 0 88 87 95 78 79 76 71 73 60 84 45 72 47 95 38 99 87 89 90 74 98 98 29 75.5

Fresh F&V Processed F&V Formula

APPENDIX H. SAMPLE ORIGIN BY STATE OR COUNTRY

(Determined by Grower, Packer, or Distributor)

Grain

Appendix H. Page 1 of 3
Part 2. Imported Samples

Fish # of % of

AP BB BN BR CB CE CH CR GB NE PC SS ST TO WM BZ CS CZ GC GJ GZ OA RI DF YF FS Samples Total

Argentina 66 1 14 81 0.8

Belgium 3 3 <0.1

Canada 42 3 2 5 10 81 1 2 13 8 2 1 25 13 10 218 2.1

Chile 187 39 197 185 2 71 72 753 7.1

China 1 128 129 1.2

Colombia 15 15 0.1

Costa Rica 40 1 41 0.4

Denmark 4 4 <0.1

Dominican Republic 2 2 <0.1

Ecuador 45 1 46 0.4

Egypt 3 3 <0.1

France 4 4 <0.1

Greece 65 65 0.6

Guatemala 45 14 9 68 0.6

Honduras 26 26 0.2

India 14 14 0.1

Ireland 8 8 0.1

Israel 16 16 0.2

Mexico 75 3 74 13 22 46 155 2 195 29 83 92 1 790 7.4

New Zealand 1 2 3 <0.1

Nicaragua 2 2 <0.1

Norway 12 12 0.1

Pakistan 9 9 0.1

Peru 9 9 0.1

Russia 2 2 <0.1

Thailand 56 56 0.5

Turkey 36 36 0.3

United Kingdom 1 4 5 <0.1

Uruguay 5 5 <0.1

Vietnam 2 2 <0.1

Unknown Country 3 1 1 5 <0.1

No. of Imports 1 384 179 77 15 27 50 144 170 197 187 200 29 96 101 10 2 172 2 15 36 23 81 0 0 234 2,432

% of Total 1 56 100 11 11 4 22 20 22 29 26 38 16 54 26 53 5 61 1 3 10 7 26 0 0 66 22.9

Fish # of % of

AP BB BN BR CB CE CH CR GB NE PC SS ST TO WM BZ CS CZ GC GJ GZ OA RI DF YF FS Samples Total

Argentina / Brazil 1 1 <0.1

Argentina / Chile / USA 1 1 <0.1

Argentina / China / Thailand / Uruguay / Vietnam / USA 1 1 <0.1

Argentina / Mexico / USA 4 4 <0.1

Argentina / USA 40 40 0.4

Canada / USA 3 1 4 <0.1

Chile / Turkey / USA 1 1 <0.1

China / Russia 3 3 <0.1

China / USA 16 16 0.2

Greece / USA 1 1 <0.1

Mexico / USA 1 1 <0.1

Turkey / USA 1 1 <0.1

No. of Mixed National Origin Samples 3 47 3 1 1 19 74

% of Total 1 9 1 < 1 <1 5 0.7

Processed F&V Formula

Processed F&V Formula

Part 3. Mixed National Origin Samples

Fresh F&V

Fresh F&V Grain

Grain

Appendix H. Page 2 of 3
Part 4. Unknown Origin Samples

Fish # of % of

AP BB BN BR CB CE CH CR GB NE PC SS ST TO WM BZ CS CZ GC GJ GZ OA RI DF YF FS Samples Total

Unknown Origin 7 2 5 1 8 13 2 5 12 2 7 1 6 1 6 1 8 8 95

% of Total 1 1 1 <1 1 2 <1 1 2 1 2 <1 1 <1 2 <1 2 2 0.9

Sample Totals: 177 688 179 712 134 708 228 708 757 681 707 531 176 177 390 19 41 282 378 531 378 314 314 528 527 354 10,619

Commodity Legend

 AP = Apples CS = Sweet Corn, Frozen OA = Oats

 BB = Blueberries, Cultivated, Fresh CZ = Cherries, Frozen PC = Peaches

 BN = Bananas DF = Infant Formula, Dairy-Based RI = Rice

 BR = Broccoli FS = Fish, Salmon SS = Summer Squash

 BZ = Blueberries, Frozen GB = Green Beans, Fresh ST = Strawberries

 CB = Sweet Corn, Fresh, On-the-Cob GC = Green Beans, Canned TO = Tomatoes

 CE = Celery GJ = Grape Juice WM = Watermelon

 CH = Cherries, Fresh GZ = Green Beans, Frozen YF = Infant Formula, Soy-based

 CR = Carrots NE = Nectarines

Fresh F&V Grain Processed F&V Formula

Appendix H. Page 3 of 3
Appendix I

Import Versus Domestic Pesticide Residue Comparisons

The Pesticide Data Program is designed to provide a comprehensive statistical picture 

of pesticide residues in the U.S. food supply, representing all sources, including imports. 

Most commodities consumed are generally produced in the United States with import 

components that vary by commodity. However, several commodities tested over the 

past several years were cyclical; that is, part of the year the commodity was produced 

domestically and part of the year it was imported. 

Appendix I compares residue data reported for samples originating in the United States 

with those of the same commodity from major exporting countries in 2014. Residue data 

for domestic blueberries are compared with data for samples originating in Chile and 

Mexico. Residue data for domestic nectarines and peaches are compared with data 

for samples originating in Chile. Only residues detected in more than 10 percent of all 

samples are included in each comparison. All pesticides detected were registered in the 

United States. However, the profi les of residue fi ndings were markedly different in the 

United States samples versus samples from these exporting countries. The differences in 

residue detections between countries were likely due to the pesticides used in response 

to pest pressures based on differing environmental and climatic conditions as well as crop 

production and protection practices. 
Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Acetamiprid United States 304 50 16.4

Chile 187 1 0.5

Mexico 75 18 24

Azoxystrobin United States 304 78 25.7

Chile 187 2 1.1

Mexico 75 28 37.3

Boscalid United States 304 99 32.6

Chile 187 57 30.5

Mexico 75 31 41.3

Cypermethrin United States 304 108 35.5

Chile 187 0 0

Mexico 75 25 33.3

Cyprodinil United States 304 97 31.9

Chile 187 16 8.6

Mexico 75 22 29.3

Fenhexamid United States 304 24 7.9

Chile 187 41 21.9

Mexico 75 8 10.7

Fludioxonil United States 304 63 20.7

Chile 187 6 3.2

Mexico 75 21 28

Malathion United States 304 67 22

Chile 187 0 0

Mexico 75 8 10.7

Phosmet United States 304 72 23.7

Chile 187 95 50.8

Mexico 75 0 0

Phosmet oxygen analog United States 304 40 13.2

Chile 187 65 34.8

Mexico 75 0 0

Pyraclostrobin United States 304 80 26.3

Chile 187 28 15

Mexico 75 25 33.3

Tetrahydrophthalimide (THPI) United States 156 55 35.3

Chile 93 19 20.4

Mexico 48 6 12.5

NOTE: The Limits of Detection (LODs) for pesticide detections in blueberries are listed in Appendix B.

Appendix I. Import Versus Domestic Pesticide Residue Comparisons

2014 Distribution of Residues for Blueberry Samples

Originating in Chile and Mexico Versus United States

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

Appendix I. Page 1 of 3
Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Acetamiprid United States 482 14 2.9

Chile 197 83 42.1

Boscalid United States 480 87 18.1

Chile 197 4 2.0

Cyhalothrin, Lambda United States 482 80 16.6

Chile 197 92 46.7

Fludioxonil United States 482 403 83.6

Chile 197 34 17.3

Indoxacarb United States 476 64 13.4

Chile 197 20 10.2

Iprodione United States 482 8 1.7

Chile 197 192 97.5

Methoxyfenozide United States 482 52 10.8

Chile 197 40 20.3

Propiconazole United States 482 198 41.1

Chile 197 36 18.3

Pyrimethanil United States 482 34 7.1

Chile 196 85 43.4

Spinetoram United States 482 138 28.6

Chile 197 0 0

Spinosad United States 482 53 11

Chile 196 113 57.7

Tebuconazole United States 482 12 2.5

Chile 197 159 80.7

NOTE: The Limits of Detection (LODs) for pesticide detections in nectarines are listed in Appendix B.

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

2014 Distribution of Residues for Nectarine Samples

Originating in Chile Versus United States

Appendix I. Page 2 of 3
Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Acetamiprid United States 515 21 4.1

Chile 185 56 30.3

Boscalid United States 515 112 21.7

Chile 185 0 0

Chlorantraniliprole United States 515 94 18.3

Chile 185 16 8.6

Cyfluthrin United States 515 74 14.4

Chile 185 0 0

Cyhalothrin, Total United States 515 75 14.6

 (Cyhalothrin-Lambda + R157836 epimer) Chile 185 41 22.2

Fenbuconazole United States 515 89 17.3

Chile 185 1 0.5

Fludioxonil United States 515 408 79.2

Chile 175 42 24

Iprodione United States 515 6 1.2

Chile 185 184 99.5

Methoxyfenozide United States 515 82 15.9

Chile 185 23 12.4

Phosmet United States 515 68 13.2

Chile 185 31 16.8

Propiconazole United States 515 222 43.1

Chile 185 33 17.8

Pyraclostrobin United States 515 148 28.7

Chile 185 1 0.5

Pyrimethanil United States 515 74 14.4

Chile 185 66 35.7

Spirodiclofen United States 515 88 17.1

Chile 166 11 6.6

Tebuconazole United States 515 25 4.9

Chile 185 141 76.2

NOTE: The Limits of Detection (LODs) for pesticide detections in peaches are listed in Appendix B.

2014 Distribution of Residues for Peach Samples

Originating in Chile Versus United States

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

Appendix I. Page 3 of 3
Appendix J

Pesticide Residues by Commodity

(Pairs With Residue Detections in at Least 5 Percent of Samples)

Appendix J shows 259 commodity/pesticide pairs (including metabolites, isomers, and 

degradates) with detections in at least 5 percent of the samples tested. The data shown 

include the range and mean of values detected and U.S. Environmental Protection Agency 

(EPA) tolerance references for each pair. The EPA tolerances cited in this summary and 

appendices apply to 2014 and not to the current year. There may be instances where 

tolerances have been recently set, modifi ed, or revoked that would have an effect on 

whether a residue is violative or not. 
APPENDIX J. PESTICIDE RESIDUES A

 BY COMMODITY

(Pairs With Residue Detections in at Least 5 Percent of Samples)

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

1 Apples (18 pesticides)

Acetamiprid * I 32.8 177 58 0.002 - 0.13 0.029 1.0

Boscalid F 19.8 177 35 0.003 - 0.14 0.023 3.0

Carbendazim (MBC) 1 F 14.7 177 26 0.001 - 0.20 0.039 2.0

Chlorantraniliprole I 23.7 177 42 0.010 - 0.044 0.017 1.2

Cyhalothrin, Total 2 * I 5.1 177 9 0.005 - 0.020 0.011 0.30

Cyprodinil F 7.3 177 13 0.005 - 0.045 0.016 1.7

Diazinon I 6.2 177 11 0.005 - 0.071 0.017 0.50

Diphenylamine (DPA) F 61.6 177 109 0.002 - 4.2 0.335 10.0

Fludioxonil F 16.9 177 30 0.025 - 1.0 0.259 5.0

Imidacloprid I 23.2 177 41 0.003 - 0.032 0.007 0.5

Phosmet I 7.9 177 14 0.011 - 0.28 0.102 10

Pyraclostrobin F 13.0 177 23 0.004 - 0.057 0.014 1.5

Pyrimethanil F 7.3 177 13 0.050 - 4.0 1.23 14

Spirodiclofen A 13 177 23 0.015 - 0.068 0.033 0.80

Tetrahydrophthalimide (THPI) 3 FM 20.9 177 37 0.010 - 0.75 0.236 25.0

Thiabendazole F 48.6 177 86 0.002 - 2.0 0.283 5.0

Thiacloprid I 14.7 177 26 0.001 - 0.021 0.007 0.30

Trifloxystrobin F 6.8 177 12 0.002 - 0.016 0.006 0.5

2 Bananas (6 pesticides)

Azoxystrobin F 15.1 179 27 0.005 - 0.028 0.011 2.0

Buprofezin I 21.8 179 39 0.001 - 0.055 0.011 0.20

Imazalil F 22.9 179 41 0.005 - 0.068 0.014 3.0

Myclobutanil F 17.3 179 31 0.003 - 0.10 0.03 4.0

Pyrimethanil F 12.3 179 22 0.002 - 0.11 0.009 0.10

Thiabendazole F 58.1 179 104 0.008 - 0.22 0.054 3.0

3 Blueberries, Cultivated (16 pesticides)

Acetamiprid * I 10.8 688 74 0.002 - 0.19 0.038 1.6

Azoxystrobin F 17.9 688 123 0.003 - 1.0 0.091 5.0

Bifenthrin * I 7.7 688 53 0.013 - 0.77 0.14 1.8

Boscalid F 38.4 688 264 0.005 - 1.7 0.186 13.0

Cypermethrin I 19.9 688 137 0.011 - 0.66 0.134 0.8

Cyprodinil F 27.5 688 189 0.003 - 1.0 0.11 3.0

Fenhexamid F 12.4 688 85 0.011 - 0.91 0.147 5.0

Fludioxonil F 16.4 688 113 0.010 - 0.63 0.108 2.0

Imidacloprid I 6.4 688 44 0.010 - 0.44 0.04 3.5

Iprodione F 8.0 688 55 0.005 - 2.7 0.176 15.0

Malathion I 13.7 688 94 0.005 - 0.67 0.072 8

Methomyl I 5.1 688 35 0.013 - 2.5 0.334 6

Methoxyfenozide I 9.4 688 65 0.009 - 0.58 0.087 3.0

Appendix J. Page 1 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Phosmet (parent) I 24.3 688 167 0.006 - 1.7 0.164 10

 Phosmet oxygen analog IM 15.3 688 105 0.003 - 0.065 0.013 10

Pyraclostrobin F 26.2 688 180 0.002 - 0.26 0.031 4.0

Tetrahydrophthalimide (THPI) 3 FM 26.6 354 94 0.010 - 2.7 0.225 20.0

4 Broccoli (2 pesticides)

Azoxystrobin F 7.3 712 52 0.002 - 0.65 0.103 3.0

DCPA H 7.7 712 55 0.005 - 0.056 0.018 5.0

5 Carrots (8 pesticides)

Azoxystrobin F 13.9 707 98 0.003 - 0.044 0.007 0.5

Boscalid F 21 708 149 0.025 - 0.15 0.035 1.0

Cyazofamid F 8.2 707 58 0.007 - 0.029 0.008 0.09

Fluopicolide F 5.4 708 38 0.010 - 0.051 0.019 0.15

Linuron H 24.6 708 174 0.017 - 0.65 0.046 1.0

Metalaxyl/Mefenoxam 4 F 5.4 708 38 0.008 - 0.034 0.012 0.5

Pyraclostrobin F 15.8 707 112 0.005 - 0.054 0.01 0.4

Trifluralin H 20.9 708 148 0.003 - 0.24 0.033 1.0

6 Celery (18 pesticides)

Acephate (parent) * I 27.4 708 194 0.005 - 0.64 0.097 10

 Methamidophos 5

 * IM 9.7 708 69 0.004 - 0.049 0.013 1

Acetamiprid * I 11.3 708 80 0.002 - 0.022 0.005 3.00

Azoxystrobin F 9.6 708 68 0.002 - 0.57 0.026 30.0

Boscalid F 13.6 708 96 0.005 - 0.17 0.021 45

Chlorantraniliprole I 31.2 708 221 0.003 - 0.24 0.015 13

Chlorothalonil F 30.7 348 107 0.010 - 0.60 0.108 15

Cyromazine R 24.7 348 86 0.005 - 0.066 0.019 7.0

Dicloran F 41.5 708 294 0.004 - 1.5 0.09 15

Flonicamid I 9.0 708 64 0.002 - 0.074 0.016 4.0

Linuron H 13.1 708 93 0.005 - 0.043 0.011 0.5

Malathion I 12.3 708 87 0.002 - 0.11 0.024 8

Methoxyfenozide I 23.3 708 165 0.002 - 0.077 0.012 25

Omethoate IM 6.2 708 44 0.005 - 0.043 0.015 2.0

Oxamyl I 9.7 708 69 0.003 - 0.089 0.013 10.0

Permethrin

 Permethrin cis 6 IM 36.3 708 257 0.002 - 0.23 0.019 5.0

 Permethrin trans 6 IM 32.5 708 230 0.002 - 0.26 0.019 5.0

Propiconazole F 25.7 708 182 0.010 - 0.13 0.022 5.0

Pyraclostrobin F 20.2 708 143 0.003 - 0.15 0.029 29.0

Thiamethoxam I 12.1 708 86 0.003 - 0.034 0.009 4.0

7 Cherries, Fresh (19 pesticides)

Acetamiprid I 24.1 228 55 0.002 - 0.23 0.057 1.20

Boscalid F 57.5 228 131 0.013 - 0.17 0.056 3.5

Buprofezin I 14.5 228 33 0.001 - 0.077 0.02 1.9

Appendix J. Page 2 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Carbaryl I 5.3 228 12 0.003 - 0.24 0.046 10

Cyhalothrin, Total 2 * I 42.1 228 96 0.012 - 0.11 0.038 0.50

Fenhexamid F 8.8 228 20 0.013 - 0.37 0.085 10.0

Fenpropathrin I 20.6 228 47 0.027 - 1.0 0.293 5.0

Fludioxonil F 25.9 228 59 0.031 - 2.0 0.264 5.0

Imidacloprid I 35.5 228 81 0.019 - 0.24 0.069 3.0

Iprodione F 21.5 228 49 0.022 - 2.6 0.619 20.0

Methoxyfenozide I 7.9 228 18 0.006 - 0.067 0.016 3.0

Myclobutanil F 29.4 228 67 0.001 - 0.16 0.033 5.0

Propiconazole F 6.1 228 14 0.018 - 0.15 0.059 4.0

Pyraclostrobin F 62.7 228 143 0.002 - 0.20 0.047 2.5

Spinetoram I 14.5 228 33 0.005 - 0.029 0.011 0.20

Spinosad

 Spinosad A IM 35.5 228 81 0.003 - 0.064 0.01 0.20

 Spinosad D IM 7.9 228 18 0.003 - 0.018 0.005 0.20

Tebuconazole F 28.5 228 65 0.012 - 3.0 0.391 5.0

Trifloxystrobin F 16.2 228 37 0.005 - 0.090 0.029 2

Triflumizole F 40.4 228 92 0.002 - 0.30 0.045 1.5

8 Cherries, Frozen (21 pesticides)

Acetamiprid * I 72 282 203 0.002 - 0.11 0.022 1.20

Azoxystrobin F 7.1 282 20 0.006 - 0.31 0.064 1.5

Boscalid F 24.5 282 69 0.013 - 0.18 0.045 3.5

Buprofezin I 20.2 282 57 0.001 - 0.035 0.006 1.9

Carbaryl I 11.7 282 33 0.003 - 0.73 0.088 10

Carbendazim (MBC) 1 F 31.9 282 90 0.006 - 0.33 0.036 20.0

Cypermethrin I 9.9 282 28 0.070 - 0.34 0.135 1

Dimethoate (parent) I 12.1 282 34 0.005 - 0.25 0.036 2.0

 Omethoate 7 IM 9.2 282 26 0.012 - 0.19 0.064 2.0

Fenbuconazole F 48.2 282 136 0.005 - 0.48 0.128 1.0

Fenpropathrin I 12.4 282 35 0.020 - 1.1 0.244 5.0

Imidacloprid I 23 282 65 0.025 - 0.40 0.108 3.0

Iprodione F 27 282 76 0.022 - 0.63 0.194 20.0

Myclobutanil F 9.2 282 26 0.001 - 0.086 0.013 5

Permethrin

 Permethrin cis 6 IM 9.6 282 27 0.020 - 0.39 0.072 4.0

 Permethrin trans 6 IM 10.3 282 29 0.014 - 0.56 0.1 4.0

Pyraclostrobin F 26.2 282 74 0.002 - 0.17 0.025 2.5

Spinosad A IM 7.1 282 20 0.003 - 0.047 0.01 0.20

Tebuconazole F 51.8 282 146 0.012 - 0.81 0.127 5.0

Thiacloprid I 35.1 282 99 0.005 - 0.11 0.03 0.5

Thiamethoxam I 20.6 282 58 0.005 - 0.074 0.021 0.5

Trifloxystrobin F 21.6 282 61 0.005 - 0.14 0.024 2

Triflumizole F 5.7 282 16 0.003 - 0.16 0.032 1.5

Appendix J. Page 3 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

9 Grape Juice (3 pesticides)

Carbaryl I 20.1 502 101 0.003 - 0.012 0.005 10

Methoxyfenozide I 11.9 531 63 0.003 - 0.030 0.007 1.0

Tetrahydrophthalimide (THPI) 3 FM 6.6 531 35 0.010 - 0.28 0.069 25.0

10 Green Beans, Fresh (10 pesticides)

Acephate (parent) * I 17.8 757 135 0.031 - 3.4 0.415 3.0

 Methamidophos 5

 * IM 16.4 757 124 0.020 - 0.63 0.139 1

Azoxystrobin F 28.7 757 217 0.001 - 0.28 0.018 3.0

Bifenthrin * I 6.9 757 52 0.040 - 0.36 0.077 0.6

Chlorantraniliprole I 7.7 757 58 0.001 - 0.042 0.006 2.0

Dicloran F 7.1 757 54 0.010 - 3.4 0.25 20

Dimethoate (parent) I 7.1 757 54 0.001 - 2.6 0.293 2.0

 Omethoate 7 IM 5.4 757 41 0.006 - 0.34 0.062 2.0

Methomyl I 6.7 757 51 0.001 - 1.1 0.07 2

Penthiopyrad F 10.3 757 78 0.001 - 0.24 0.07 4.0

Pyraclostrobin F 13.2 757 100 0.001 - 0.10 0.015 0.5

Tebuconazole F 5.5 757 42 0.001 - 0.048 0.009 0.1

11 Green Beans, Canned (3 pesticides)

Acephate (parent) * I 10.6 378 40 0.003 - 0.028 0.008 3.0

 Methamidophos 5 * IM 12.4 378 47 0.002 - 0.060 0.012 1

Bifenthrin * I 52.1 378 197 0.003 - 0.056 0.01 0.6

Carbendazim (MBC) 1 F 47.9 378 181 0.002 - 0.057 0.008 2.0

12 Green Beans, Frozen (6 pesticides)

Acephate (parent) * I 21.7 378 82 0.003 - 0.30 0.039 3.0

 Methamidophos 5

 * IM 20.9 378 79 0.002 - 0.079 0.016 1

Azoxystrobin F 11.6 378 44 0.002 - 0.016 0.004 3.0

Bifenthrin * I 43.9 378 166 0.003 - 0.064 0.021 0.6

Boscalid F 7.4 378 28 0.010 - 0.13 0.041 1.6

Carbendazim (MBC) 1 F 48.1 378 182 0.002 - 0.095 0.012 2.0

Iprodione F 11.6 378 44 0.015 - 0.44 0.065 2.0

13 Nectarines (19 pesticides)

Acetamiprid * I 14.2 681 97 0.017 - 0.096 0.035 1.20

Boscalid F 13.4 679 91 0.002 - 0.21 0.043 3.5

Buprofezin I 6.0 681 41 0.002 - 0.015 0.003 9.0

Cyhalothrin, Lambda * I 25.3 681 172 0.003 - 0.053 0.01 0.50

Fenhexamid F 8.2 681 56 0.008 - 1.2 0.169 10.0

Fenpropathrin I 7.9 681 54 0.005 - 0.38 0.132 1.4

Fenpyroximate A 5.6 681 38 0.002 - 0.053 0.026 2.0

Fludioxonil F 64.5 681 439 0.033 - 3.2 0.595 5.0

Indoxacarb I 12.6 675 85 0.003 - 0.069 0.017 0.90

Iprodione F 29.4 681 200 0.008 - 6.2 1.296 20.0

Methoxyfenozide I 13.7 681 93 0.003 - 0.099 0.024 3.0

Appendix J. Page 4 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Myclobutanil F 6.6 680 45 0.003 - 0.095 0.016 2.0

Propiconazole F 34.5 681 235 0.007 - 0.57 0.117 4.0

Pyraclostrobin F 9.9 679 67 0.002 - 0.12 0.035 2.5

Pyrimethanil F 17.6 680 120 0.002 - 1.6 0.142 10

Spinetoram I 20.4 681 139 0.013 - 0.099 0.024 0.20

Spinosad I 24.6 680 167 0.010 - 0.10 0.02 0.20

Tebuconazole F 25.3 681 172 0.002 - 1.5 0.179 1.0

Thiabendazole F 9.1 681 62 0.003 - 0.042 0.007 NT

14 Peaches (25 pesticides)

Acetamiprid * I 10.9 707 77 0.010 - 0.11 0.033 1.20

Boscalid F 15.8 707 112 0.011 - 0.46 0.094 3.5

Captan F 6.9 707 49 0.021 - 3.7 0.288 15.0

Chlorantraniliprole I 15.7 707 111 0.020 - 0.12 0.039 4.0

Clothianidin * I 6.2 707 44 0.010 - 0.17 0.029 0.80

Cyfluthrin * I 10.6 707 75 0.005 - 0.11 0.023 0.3

Cyhalothrin, Total 2 * I 16.4 707 116 0.008 - 0.086 0.02 0.50

Cyprodinil F 5.7 707 40 0.006 - 0.77 0.188 2.0

Esfenvalerate+Fenvalerate Total * I 6.5 707 46 0.007 - 0.10 0.03 3.0

Fenbuconazole F 12.7 707 90 0.005 - 0.15 0.024 1.0

Fenpropathrin I 6.4 707 45 0.006 - 0.80 0.207 1.4

Fenpyroximate A 6.2 707 44 0.010 - 0.071 0.026 2.0

Fludioxonil F 65 697 453 0.005 - 6.7 0.786 5.0

Hexythiazox I 5.7 707 40 0.011 - 0.12 0.033 1.0

Imidacloprid I 6.2 707 44 0.010 - 0.13 0.028 3.0

Indoxacarb I 6.6 707 47 0.010 - 0.066 0.025 0.90

Iprodione F 26.9 707 190 0.006 - 7.2 1.419 20.0

Methoxyfenozide I 15 707 106 0.010 - 0.20 0.04 3.0

Myclobutanil F 5.4 707 38 0.005 - 0.14 0.035 2.0

Phosmet I 14.3 707 101 0.005 - 1.8 0.11 10

Propiconazole F 36.5 707 258 0.010 - 1.2 0.162 4.0

Pyraclostrobin F 21.2 707 150 0.003 - 0.23 0.058 2.5

Pyrimethanil F 19.8 707 140 0.003 - 1.6 0.217 10

Spirodiclofen A 14.4 688 99 0.010 - 0.23 0.049 1.0

Tebuconazole F 23.6 707 167 0.005 - 6.6 0.288 1.0

15 Rice (1 pesticide)

Piperonyl butoxide I 11.1 314 35 0.005 - 0.30 0.067 20

16 Strawberries (32 pesticides)

Acequinocyl A 11.4 176 20 0.014 - 1.6 0.335 0.50

Acetamiprid * I 29.5 176 52 0.003 - 0.31 0.059 0.60

Azoxystrobin F 19.3 176 34 0.003 - 0.37 0.056 10.0

Bifenazate A 19.3 176 34 0.003 - 1.5 0.103 1.5

Bifenthrin * I 41.5 176 73 0.010 - 0.21 0.054 3.0

Boscalid F 60.8 176 107 0.006 - 0.68 0.099 4.5

Appendix J. Page 5 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Carbendazim (MBC) 1 F 30.7 176 54 0.003 - 0.27 0.069 7.0

Chlorantraniliprole I 22.2 176 39 0.010 - 0.12 0.027 1.0

Cyprodinil F 63.6 176 112 0.003 - 1.3 0.168 5.0

Etoxazole A 5.7 176 10 0.004 - 0.067 0.026 0.50

Fenhexamid F 19.9 176 35 0.021 - 1.0 0.218 3.0

Fenpropathrin I 25.6 176 45 0.005 - 0.51 0.069 2.0

Flonicamid I 23.3 176 41 0.033 - 0.48 0.113 1.5

Fludioxonil F 50.6 176 89 0.010 - 0.56 0.113 3.0

Fluxapyroxad F 6.2 176 11 0.006 - 0.73 0.115 4.0

Hexythiazox I 13.1 176 23 0.003 - 0.31 0.041 6

Imidacloprid I 10.8 176 19 0.005 - 0.075 0.017 0.50

Malathion I 10.8 176 19 0.005 - 0.15 0.026 8

Metalaxyl/Mefenoxam 4 F 14.2 176 25 0.003 - 0.25 0.059 10.0

Methoxyfenozide I 23.3 176 41 0.003 - 0.21 0.032 2.0

Myclobutanil F 17.6 176 31 0.012 - 0.23 0.071 0.50

Novaluron I 15.3 176 27 0.020 - 0.10 0.037 0.45

Penthiopyrad F 9.1 176 16 0.007 - 1.5 0.212 3.0

Piperonyl butoxide I 6.8 176 12 0.005 - 0.96 0.172 EX

Pyraclostrobin F 46.6 176 82 0.003 - 0.66 0.075 1.2

Pyrimethanil F 26.7 176 47 0.005 - 1.5 0.366 3.0

Quinoxyfen F 24.4 176 43 0.003 - 0.12 0.025 1.0

Spiromesifen (parent) I 11.4 176 20 0.003 - 0.26 0.056 2.0

 Spiromesifen alcohol IM 28.4 176 50 0.002 - 0.23 0.026 2.0

Tetraconazole F 7.4 176 13 0.003 - 0.079 0.023 0.25

Tetrahydrophthalimide (THPI) 3 FM 72.7 176 128 0.012 - 2.5 0.566 20.0

Thiamethoxam I 19.9 176 35 0.003 - 0.11 0.016 0.30

Triflumizole F 6.8 176 12 0.006 - 0.38 0.056 2.0

17 Summer Squash (7 pesticides)

Chlorothalonil F 7.4 270 20 0.011 - 0.22 0.062 5.0

Endosulfan sulfate 8 IM 10.5 531 56 0.005 - 0.15 0.046 1.0

Imidacloprid I 15.8 531 84 0.010 - 0.35 0.045 0.5

Metalaxyl/Mefenoxam 4 F 5.3 531 28 0.003 - 0.18 0.04 1.0

Propamocarb hydrochloride 9 F 7.9 531 42 0.006 - 0.57 0.102 1.5

Pyraclostrobin F 5.3 531 28 0.003 - 0.035 0.012 0.5

Thiamethoxam * I 14.7 531 78 0.003 - 0.14 0.023 0.2

18 Tomatoes (28 pesticides)

Acetamiprid * I 8.5 177 15 0.002 - 0.044 0.011 0.20

Azoxystrobin F 20.3 177 36 0.002 - 0.023 0.007 0.2

Bifenthrin * I 16.9 177 30 0.002 - 0.024 0.008 0.15

Boscalid F 7.3 177 13 0.021 - 0.079 0.035 3.0

Buprofezin I 11.9 177 21 0.002 - 0.030 0.006 2.0

Carbendazim (MBC) 1 F 9.6 177 17 0.002 - 0.037 0.01 NT

Chlorantraniliprole I 23.7 177 42 0.003 - 0.027 0.007 1.4

Chlorfenapyr I 11.9 177 21 0.004 - 0.36 0.044 1.0

Appendix J. Page 6 of 7
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Clothianidin I 9.6 177 17 0.003 - 0.038 0.006 0.20

Difenoconazole F 20.9 177 37 0.002 - 0.041 0.009 0.60

Dinotefuran I 19.2 177 34 0.010 - 0.13 0.029 0.7

Endosulfan II 8 IM 7.3 177 13 0.002 - 0.027 0.008 1.0

Famoxadone F 5.6 177 10 0.010 - 0.032 0.018 1.0

Fenpropathrin I 6.8 177 12 0.004 - 0.080 0.019 1.0

Flonicamid I 23.2 177 41 0.002 - 0.34 0.033 0.40

Fludioxonil F 6.2 177 11 0.020 - 0.090 0.033 5.0

Fluxapyroxad F 5.6 177 10 0.002 - 0.024 0.007 0.7

Imidacloprid I 21.5 177 38 0.003 - 0.080 0.01 1.0

Methoxyfenozide I 8.5 177 15 0.002 - 0.015 0.006 2.0

Myclobutanil F 7.9 177 14 0.003 - 0.051 0.012 0.30

Penthiopyrad F 7.9 177 14 0.003 - 0.044 0.014 3.0

Permethrin trans IM 5.1 177 9 0.002 - 0.020 0.008 2.0

Piperonyl butoxide I 7.3 177 13 0.005 - 0.29 0.077 8

Pyraclostrobin F 27.1 177 48 0.002 - 0.056 0.009 1.4

Pyrimethanil F 18.6 177 33 0.002 - 0.14 0.018 0.50

Pyriproxyfen I 9.0 177 16 0.004 - 0.046 0.013 0.80

Tetrahydrophthalimide (THPI) 3 FM 8.9 157 14 0.006 - 0.15 0.032 0.05

Thiamethoxam * I 6.8 177 12 0.008 - 0.020 0.009 0.25

19 Watermelon (6 pesticides)

Bifenthrin * I 7.9 390 31 0.002 - 0.009 0.004 0.4

Carbendazim (MBC) 1 F 6.2 390 24 0.001 - 0.013 0.003 1.0

Cyprodinil F 5.9 390 23 0.005 - 0.026 0.011 0.70

Imidacloprid I 11.8 390 46 0.003 - 0.093 0.014 0.5

Metalaxyl/Mefenoxam 4 F 9.5 390 37 0.001 - 0.049 0.009 1.0

Thiamethoxam * I 7.7 390 30 0.003 - 0.033 0.009 0.2

NOTES

A Excludes environmental contaminants, which are listed in Appendix G.

NT No tolerance established.

* Residue may result from food handling establishment (FHE) application.

1 From parent, benomyl.

2 Includes cyhalothrin lambda plus R157836 epimer.

3 Metabolite of captafol and captan.

4 Metalaxyl/mefenoxam are spatial isomers which are analytically indistinguishable via multiresidue methods, but have

separate registrations.

5 Specific tolerance established for methamidophos in celery and green beans as a possible result of an acephate application.

6 Isomer of parent, permethrin.

7 Metabolite of parent, dimethoate.

8 From parent, endosulfan.

9 Analytically determined as the salt (hydrochloride).

Pesticide Types:

A = Acaricide I = Insecticide, IM = Insecticide Metabolite

F = Fungicide, FM = Fungicide Metabolite R = Insect Growth Regulator

H = Herbicide

Appendix J. Page 7 of 7
Appendix K

Number of Pesticides Detected per Sample

Appendix K shows the percentage of samples versus the number of pesticides detected 

per sample. The graph and data on page 1 show the overall number of samples and 

percentages (of total number of samples analyzed) for each detection group across all 

commodities. The table on page 2 shows the number of pesticides detected by individual 

commodity. For the 10,619 samples analyzed, 41.5 percent of the samples had no 

detectable pesticides, 14.8 percent had 1 pesticide, and 43.7 percent of the samples had 

more than 1 pesticide. 

This appendix reports the number of distinct pesticides rather than residues. A parent 

compound and its metabolites are reported as a single pesticide.
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17

Number of

Samples 4,409 1,569 1,347 927 743 572 369 226 185 105 84 33 21 12 8 5 3 1

Percent of

Total Samples 41.5 14.8 12.7 8.7 7.0 5.4 3.5 2.1 1.7 1.0 0.8 0.3 0.2 0.1 0.08 0.05 0.03 0.01

TOTAL NUMBER OF SAMPLES = 10,619 

NOTES

1

 Environmental contaminants, listed in Appendix G, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues."

APPENDIX K. NUMBER OF PESTICIDES 1 DETECTED PER SAMPLE

Number of Pesticides Detected per Sample

Number of Pesticides Detected per Sample

50

40

30

20

10

Percent of Samples

41.5

12.7

14.8

5.4

7.0

8.7

1.0 1.7 2.1

3.5

Multiple pesticide detections may result from the application of more than one pesticide, spray drift, crop 

rotation, and/or cross-contamination.

0.8 0.3 0.2 0.1 0.08 0.05 0.03 0.01

Appendix K. Page 1 of 2
Commodity (# of samples) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17

Fresh Fruit and Vegetables:

Apples (177) 4.5 8.5 13.0 20.9 23.7 13.0 6.8 4.5 2.3 1.1 0.6 -- -- 0.6 -- 0.6 -- --

Bananas (179) 17.3 36.3 28.5 14.5 3.4 -- -- -- -- -- -- -- -- -- -- -- -- --

Blueberries, Cultivated (688) 22.7 14.1 15.3 14.2 9.4 7.3 6.5 3.3 3.2 2.2 1.3 0.4 -- -- -- -- -- --

Broccoli (712) 70.8 18.0 7.3 3.2 0.7 -- -- -- -- -- -- -- -- -- -- -- -- --

Carrots (708) 38.3 23.4 15.5 11.4 5.5 3.5 1.3 0.4 0.6 -- -- -- -- -- -- -- -- --

Celery (708) 6.8 8.6 14.1 16.1 17.7 17.5 8.6 4.7 3.2 1.3 0.8 -- 0.4 0.1 -- -- -- --

Cherries (228) 2.2 3.5 7.9 9.2 17.5 19.7 15.4 7.0 7.0 5.3 3.1 1.3 0.9 -- -- -- -- --

Green Beans (757) 29.7 24.0 23.5 12.5 5.2 2.2 1.7 0.7 0.3 -- 0.1 -- -- -- -- -- -- --

Nectarines (681) 1.3 8.4 16.9 14.7 18.8 14.5 10.7 7.5 3.8 1.2 1.0 0.7 0.4 -- -- -- -- --

Peaches (707) 2.5 10.6 17.0 17.7 15.3 11.5 7.6 3.3 5.8 4.5 4.0 0.3 -- -- -- -- -- --

Strawberries (176) 1.7 2.3 2.3 3.4 6.8 9.7 9.7 10.2 6.3 7.4 9.7 9.1 6.8 5.7 4.5 2.3 1.7 0.6

Summer Squash (531) 50.7 25.6 12.4 6.0 3.6 0.9 0.2 0.6 -- -- -- -- -- -- -- -- -- --

Sweet Corn, On-the-Cob (134) 98.5 1.5 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Tomatoes (177) 1.7 11.9 17.5 15.8 15.3 14.7 6.8 6.8 5.6 2.3 1.7 -- -- -- -- -- -- --

Watermelon (390) 54.1 32.1 8.7 3.8 1.0 0.3 -- -- -- -- -- -- -- -- -- -- -- --

Processed Fruit and Vegetables:

Blueberries, Frozen (19) 5.3 5.3 -- 26.3 21.1 10.5 5.3 26.3 -- -- -- -- -- -- -- -- -- --

Cherries, Frozen (282) 0.4 1.8 4.3 12.1 23.8 19.5 12.8 9.2 9.2 3.5 1.8 1.4 0.4 -- -- -- -- --

Grape Juice (531) 68 18.5 10.5 2.6 -- 0.2 -- -- -- -- -- -- -- -- -- -- -- --

Green Beans, Canned (378) 21.4 39.9 31.7 5.3 1.6 -- -- -- -- -- -- -- -- -- -- -- -- --

Green Beans, Frozen (378) 12.2 32.0 39.7 14.0 1.9 0.3 -- -- -- -- -- -- -- -- -- -- -- --

Sweet Corn, Frozen (41) 97.6 2.4 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Percent of Total Samples 28.2 17.7 15.7 10.8 8.7 6.7 4.3 2.6 2.2 1.2 1.0 0.4 0.2 0.1 0.1 0.1 0.03 0.01

Actual Number of Samples 2,424 1,519 1,345 927 743 571 370 226 185 105 84 33 21 12 8 5 3 1

Grain Products: 

Oats (314) 99.7 0.3 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Rice (314) 86.3 13.1 0.6 -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 584 42 2 -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Infant Formula Products: 

Infant Formula, Dairy-based (528) 100 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Infant Formula, Soy-based (527) 98.7 1.3 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 1048 7 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Fish Product: 

Salmon (354) 99.7 0.3 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 353 1 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

NOTES

1 Environmental contaminants, listed in Appendix G, have been excluded from the count of pesticides detected in this appendix. Parent

compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues." 

Percent

APPENDIX K. NUMBER OF PESTICIDES DETECTED PER SAMPLE

Number of Pesticides 1 Detected per Sample

TOTAL NUMBER OF FRUIT & VEGETABLE SAMPLES = 8,582

Appendix K. Page 2 of 2
Appendix L

Fruit and Vegetable Samples Reported to the

U.S. Food and Drug Administration as

Exceeding the Tolerance

or Without Established Tolerance

(per Code of Federal Regulations, Title 40, Part 180)

Appendix L shows pesticide residues reported to the U.S. Food and Drug Administration 

(FDA) as exceeding the tolerance or residues for which no established tolerance was 

listed under the Code of Federal Regulations, Title 40, Part 180. In 2014, a total of 

316 samples with 352 pesticides were reported to the FDA as Presumptive Tolerance 

Violations.

Pesticides exceeding the tolerance were detected in 38 samples including 1 sample of 

bananas, 2 samples of broccoli, 12 fresh green bean samples, 1 sample of nectarines, 

11 peach samples, 5 samples of strawberries, 2 samples of summer squash, 3 samples 

of tomatoes, and 1 sample of watermelon. Of those 38 samples, 19 were reported as 

imported produce.

In addition, 281 samples were found to have pesticides for which no tolerance was 

established, including 258 fresh fruit and vegetable samples, 22 processed fruit/vegetable 

samples, and 1 rice sample.

o 250 samples contained 1 pesticide for which no tolerance was established.

o 29 samples contained 2 pesticides for which no tolerance was established.

o 1 sample of celery and 1 sample of fresh green beans contained 3 pesticides for 

which no tolerance was established.

Three of the 281 samples also contained 1 pesticide each that exceeded an established 

tolerance.

The columns under the Sample Origin heading provide the number of samples that were 

of domestic, imported, or unknown origin for each pesticide/commodity pair listed.

Appendix L also notes if metabolites (or isomers) were detected as part of the same 

sample. In instances where both parent and metabolite (or isomer) were detected, the 

Pesticide Data Program accounted for both as part of the same tolerance expression.

A number of the fi ndings shown in this appendix are less than 0.01 ppm. Levels below 

0.01 ppm are deemed by the U.S. FDA to be “not of regulatory signifi cance”.
Residues Exceeding Established Tolerance

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm

Country of 

Origin

1 Bananas / Pyrimethanil 0.002 0.11 0.10 Costa Rica

2 Broccoli / Cypermethrin 0.01 2.6 2.0 Mexico

3 Broccoli / Cyprodinil 0.005 1.4 1.0 U.S.

4 Green Beans / Acephate 0.03 3.4 3.0 U.S.

5 Green Beans / Chlorfenapyr 0.025 0.071 0.01 Mexico

6 Green Beans / Dimethoate 0.001 2.6 2.0 U.S.

7 Green Beans / Dimethoate 0.001 2.3 2.0 U.S.

8 Green Beans / Dimethoate 0.001 2.1 2.0 U.S.

9 Green Beans / Dinotefuran 0.04 0.16 0.01 U.S.

10 Green Beans / Dinotefuran 0.04 0.16 0.01 U.S.

11 Green Beans / Dinotefuran 0.04 0.14 0.01 U.S.

12 Green Beans / Dinotefuran 0.04 0.11 0.01 U.S.

13 Green Beans / Dinotefuran 0.04 0.09 0.01 U.S.

14 Green Beans / Dinotefuran 0.04 0.074 0.01 U.S.

15 Green Beans / Dinotefuran 0.04 0.069 0.01 U.S.

16 Nectarines / Tebuconazole 0.001 1.5 1.0 Chile

17 Peaches / Chlorpyrifos 0.005 0.065 0.05 U.S.

18 Peaches / Fludioxonil 0.005 6.7 5.0 U.S.

19 Peaches / Tebuconazole 0.005 6.6 1.0 Chile

20 Peaches / Tebuconazole 0.005 2.3 1.0 Chile

21 Peaches / Tebuconazole 0.005 2.2 1.0 Chile

22 Peaches / Tebuconazole 0.005 1.6 1.0 Chile

23 Peaches / Tebuconazole 0.005 1.5 1.0 Chile

24 Peaches / Tebuconazole 0.005 1.2 1.0 Chile

25 Peaches / Tebuconazole 0.005 1.2 1.0 Chile

26 Peaches / Tebuconazole 0.005 1.2 1.0 Chile

27 Peaches / Tebuconazole 0.005 1.2 1.0 Chile

28 Strawberries / Acequinocyl 1

0.005 1.6 0.50 U.S.

29 Strawberries / Acequinocyl 1

0.005 1.2 0.50 U.S.

30 Strawberries / Acequinocyl 1

0.005 0.99 0.50 Mexico

31 Strawberries / Acequinocyl 1

0.005 0.7 0.50 Mexico

32 Strawberries / Acequinocyl 1

0.005 0.52 0.50 Mexico

33 Summer Squash / Acephate 0.03 0.19 0.02 U.S.

34 Summer Squash / Heptachlor epoxide 0.01 0.079 0.05 AL U.S.

35 Tomatoes / Tetrahydrophthalimide (THPI) 2

0.004 0.15 0.05 Mexico

36 Tomatoes / Tetrahydrophthalimide (THPI) 2

0.004 0.066 0.05 Mexico

37 Tomatoes / Tetrahydrophthalimide (THPI) 2

0.004 0.064 0.05 Mexico

38 Watermelon / Acephate 0.03 0.084 0.02 U.S.

APPENDIX L. SAMPLES REPORTED TO FDA AS EXCEEDING THE TOLERANCE

OR WITHOUT ESTABLISHED TOLERANCE

(per Code of Federal Regulations, Title 40, Part 180)

Appendix L. Page 1 of 4
Commodity / Pesticide U.S. Import Unk.

1 Blueberries, Cultivated, Fresh (7 pesticides)

Carbendazim (MBC) 3688 2 0.3 0.021 - 0.073 0.005 ^ 1 1 0

Cyproconazole 688 1 0.1 0.007 ^ 0.005 - 0.010 0 1 0

3-Hydroxycarbofuran 688 2 0.3 0.002 - 0.003 0.002 - 0.010 0 2 0

Methoxychlor p,p' 354 3 0.8 0.005 - 0.007 0.005 ^ 2 1 0

Tebuconazole 688 4 0.6 0.022 - 0.070 0.010 - 0.012 0 4 0

Terbuthylazine 688 2 0.3 0.003 - 0.004 0.002 - 0.003 0 2 0

Trifloxystrobin 688 1 0.1 0.013 ^ 0.003 - 0.005 0 1 0

2 Broccoli (4 pesticides)

Chlorpropham 712 2 0.3 0.006 - 0.010 0.005 ^ 2 0 0

Fluoxastrobin 712 3 0.4 0.016 - 0.081 0.002 ^ 3 0 0

Pronamide 712 1 0.1 0.006 ^ 0.005 ^ 1 0 0

Propamocarb hydrochloride 4 712 2 0.3 0.010 - 0.024 0.010 ^ 2 0 0

3 Carrots (3 pesticides)

Carbendazim (MBC) 3708 1 0.1 0.005 ^ 0.003 ^ 1 0 0

Quintozene - PCNB (parent) 5

 Pentachloroaniline (PCA) 708 20 2.8 0.003 - 0.020 0.002 ^ 14 6 0

 Pentachlorobenzene (PCB) 708 1 0.1 0.020 ^ 0.001 ^ 1 0 0

 Pentachlorophenyl methyl sulfide 708 1 0.1 0.007 ^ 0.002 ^ 1 0 0

Phosmet 708 3 0.4 0.017 ^ 0.010 ^ 0 3 0

4 Celery (10 pesticides)

Chlorpropham 708 1 0.1 0.002 ^ 0.001 - 0.005 1 0 0

DCPA 708 9 1.3 0.002 - 0.007 0.001 - 0.003 9 0 0

Disulfoton sulfone 708 1 0.1 0.004 ^ 0.002 - 0.003 1 0 0

Norflurazon (parent) 6708 2 0.3 0.002 - 0.005 0.001 - 0.010 2 0 0

 Norflurazon desmethyl 708 4 0.6 0.002 - 0.020 0.001 - 0.010 4 0 0

Oxyfluorfen 708 1 0.1 0.002 ^ 0.001 - 0.010 1 0 0

Pendimethalin 708 5 0.7 0.002 - 0.009 0.001 - 0.005 2 3 0

Pronamide 708 5 0.7 0.002 - 0.005 0.001 - 0.003 4 0 1

Propamocarb hydrochloride 4 348 3 0.9 0.014 - 0.025 0.010 ^ 3 0 0

Pyrimethanil 708 3 0.4 0.002 - 0.006 0.001 - 0.005 3 0 0

Tetraconazole 708 1 0.1 0.002 ^ 0.001 - 0.010 1 0 0

5 Cherries, Fresh (1 pesticide)

Thiabendazole 228 2 0.9 0.012 - 0.014 0.005 ^ 2 0 0

6 Cherries, Frozen (4 pesticides)

Monocrotophos 282 3 1.1 0.023 - 0.057 0.017 ^ 0 3 0

Pirimicarb 282 2 0.7 0.002 - 0.003 0.002 ^ 0 2 0

Propargite 282 3 1.1 0.049 - 0.25 0.036 ^ 0 3 0

Thiabendazole 282 2 0.7 0.008 - 0.009 0.005 ^ 0 2 0

7 Grape Juice (1 pesticide)

Diphenylamine (DPA) 531 1 0.2 0.002 ^ 0.002 ^ 1 0 0

Sample Origin

Distribution of Residues with No Tolerance Listed in 40 CFR, Part 180, 

Range of 

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

by Commodity/Pesticide

Appendix L. Page 2 of 4
Commodity / Pesticide U.S. Import Unk.

Range of Sample Origin

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

8 Green Beans, Fresh (10 pesticides)

Difenoconazole 757 1 0.1 0.005 ^ 0.005 ^ 0 1 0

Dimethomorph 757 1 0.1 0.005 ^ 0.001 ^ 0 1 0

Fenpropathrin 757 3 0.4 0.064 - 0.092 0.050 ^ 0 3 0

Flonicamid 757 1 0.1 0.10 ^ 0.10 ^ 1 0 0

Fluopicolide 757 1 0.1 0.052 ^ 0.002 ^ 1 0 0

Oxamyl (parent) 757 3 0.4 0.011 - 0.14 0.002 ^ 2 1 0

 Oxamyl oxime 7 757 1 0.1 0.060 ^ 0.050 ^ 1 0 0

Permethrin Total 8757 3 0.4 0.073 - 0.11 0.040 ^ 0 3 0

Propamocarb hydrochloride 4 757 17 2.2 0.001 - 0.11 0.001 ^ 6 10 1

Pyrimethanil 757 2 0.3 0.001 - 0.031 0.001 ^ 1 1 0

Trifloxystrobin 757 2 0.3 0.001 - 0.004 0.001 ^ 1 1 0

9 Green Beans, Canned (3 pesticides)

Permethrin (parent) 9

 Permethrin cis 378 1 0.3 0.004 ^ 0.001 ^ 1 0 0

 Permethrin trans 378 1 0.3 0.005 ^ 0.001 ^ 1 0 0

Propachlor 378 1 0.3 0.002 ^ 0.001 ^ 1 0 0

Pyrimethanil 378 2 0.5 0.002 ^ 0.001 ^ 2 0 0

10 Green Beans, Frozen (7 pesticides)

Chlorpropham 378 1 0.3 0.035 ^ 0.001 ^ 0 1 0

Fenhexamid 378 1 0.3 0.015 ^ 0.009 ^ 1 0 0

Metribuzin 378 1 0.3 0.003 ^ 0.002 ^ 1 0 0

Permethrin cis 378 1 0.3 0.002 ^ 0.001 ^ 1 0 0

Pirimicarb 378 1 0.3 0.002 ^ 0.001 ^ 0 1 0

Pyrimethanil 378 2 0.5 0.002 ^ 0.001 ^ 1 1 0

Trifloxystrobin 378 2 0.5 0.002 - 0.011 0.001 ^ 2 0 0

11 Nectarines (3 pesticides)

Imazalil 681 33 4.8 0.007 - 0.11 0.004 ^ 15 18 0

Tetramethrin 681 1 0.1 0.002 ^ 0.001 ^ 0 1 0

Thiabendazole 681 62 9.1 0.003 - 0.042 0.002 ^ 27 35 0

12 Peaches (5 pesticides)

Chlorpropham 677 2 0.3 0.008 - 0.043 0.005 ^ 2 0 0

Dimethoate 707 2 0.3 0.015 - 0.028 0.010 ^ 2 0 0

Imazalil 707 10 1.4 0.011 - 0.072 0.010 ^ 6 4 0

Propargite 707 1 0.1 0.029 ^ 0.020 ^ 1 0 0

Thiabendazole 707 10 1.4 0.011 - 0.12 0.010 ^ 8 2 0

13 Rice (1 pesticide)

Tebuconazole 314 1 0.3 0.038 ^ 0.025 ^ 0 1 0

14 Strawberries (6 pesticides)

Chlorothalonil 176 2 1.1 0.036 - 0.14 0.010 ^ 0 2 0

Dimethoate (parent) 10 176 1 0.6 0.005 ^ 0.003 ^ 1 0 0

 Omethoate 176 1 0.6 0.003 ^ 0.003 ^ 1 0 0

Fenazaquin 176 2 1.1 0.003 - 0.29 0.003 ^ 0 2 0

Methomyl 176 3 1.7 0.011 - 0.055 0.010 ^ 2 1 0

Appendix L. Page 3 of 4
Commodity / Pesticide U.S. Import Unk.

Range of Sample Origin

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

Oxamyl (parent) 7176 1 0.6 0.033 ^ 0.005 ^ 1 0 0

 Oxamyl oxime 176 1 0.6 0.020 ^ 0.010 ^ 1 0 0

Tebuconazole 176 1 0.6 0.018 ^ 0.003 ^ 0 1 0

15 Summer Squash (4 pesticides)

Dichlobenil 270 1 0.4 0.004 ^ 0.003 ^ 0 1 0

Monocrotophos 270 1 0.4 0.46 ^ 0.005 ^ 0 1 0

Quintozene - PCNB (parent) 11

 Pentachloroaniline (PCA) 531 6 1.1 0.003 - 0.007 0.003 - 0.12 5 1 0

 Pentachlorobenzene (PCB) 531 1 0.2 0.008 ^ 0.005 - 0.010 1 0 0

Quinoxyfen 270 1 0.4 0.008 ^ 0.003 ^ 1 0 0

16 Tomatoes (5 pesticides)

Carbendazim (MBC) 3177 17 9.6 0.002 - 0.037 0.001 ^ 4 13 0

Chlorpropham 177 8 4.5 0.002 - 0.058 0.001 ^ 4 4 0

Fenbuconazole 177 5 2.8 0.002 - 0.028 0.001 ^ 1 4 0

Iprodione 177 1 0.6 0.030 ^ 0.009 ^ 0 0 1

Thiacloprid 177 1 0.6 0.002 ^ 0.001 ^ 0 1 0

17 Watermelon (1 pesticide)

Pentachloroaniline (PCA) 390 1 0.3 0.006 ^ 0.004 ^ 0 1 0

NOTES

AL Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to the U.S. Environmental Protection Agency. In the interim, action levels

are used.

1 Acequinocyl in strawberries analyzed as the hydroxy metabolite.

2 Tetrahydrophthalimide (THPI) is a metabolite of Captafol and Captan.

3 Carbendazim (MBC) is a metabolite of Benomyl and Thiophanate methyl.

4 Propamocarb analytically determined as the salt (hydrochloride).

5 One carrot sample contained all three of the PCNB metabilites.

6 Two celery samples contained both Norflurazon and its desmethyl metabolite.

7 One fresh green bean sample and one strawberry sample contained both Oxamyl and its oxime metabolite.

8 Permethrin Total includes the cis permethrin isomer plus the trans permethrin isomer.

9 One canned green bean sample contained both the cis and trans permethrin isomers.

10 Omethoate is a metabolite of the parent, Dimethoate. One strawberry sample contained both Dimethoate and Omethoate.

11 One summer squash sample contained both the PCA and PCB metabolites.

Note:

For those pesticide/commodity pairs where the minimum detected value is less than the limit of quantitation (three times

the limit of detection), the reported values are estimates. In a few cases, this may apply to the maximum detected value.

Appendix L. Page 4 of 4
PESTICIDE DATA PROGRAM

Annual Summary, Calendar Yea

Your satisfaction is very important to us, and we welcome your comments and

suggestions. Thank you for taking time to fill out and return this car

How would you rate this document on: Good Fair Poor

	 	 	 Visual Presentation?	 	 

	 	 	 Ease of Readability?	 	 

	 	 Information Provided

Comments/ Suggestions: (Attach additional pages if needed)

	 	 	 	 	 	 	 	 	 	 	 	 	

How did you obtain this copy?	 	 	 	 	 	 	 	 	

Would you like additional copies? (limit 10 per person, 25 per organization)	

# Requested 	 	

Mailing Address	 	 	 	 	 	 	 	 	

	 	 	 	 	 	 	 	 	 	 	

Mail or Fax to:	 USDA-AMS-S&T-Monitoring Programs Division

	 	 	 1400 Independence Ave, SW

	 	 	 Room 0611-S, Stop 0276

	 	 	 Facsimile: 202-572-81

	 	 	 Electronic Mail: amsmpo.data@ams.usda.g