# Instructions for filling the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon Monoxide, Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi HAPs, Sulfer Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total Dissolved Solids (TDS), and Total Suspended Solids (TSS). You must complete 3 separate sampling events for each of the requested constituents. spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in yellow are required. All cells that are shaded in light green are populated using drop

-down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please Do Not modify the structure of this spreadsheet by adding or subtracting
rows, columns, cells. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family requred for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constiuent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg+2

# , or if the Ontario

- Hydro Method was used, you would need to enter Hg0

# , Hg P

# , and Hg Specieated Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop provided in the Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure (deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field. 2. Please provide the values of all requested parameters for each of the 3 sample testing periods in the Sample 1, Sample 2, and Sample 3 fields

. 3. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

-downs in the Fuel Type Selection field. You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

# If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O2 (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field.

# This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon Monoxide, Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi

-Volatile Organic HAPs, Sulfer Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total Dissolved Solids (TDS), and Total Suspended Solids (TSS). You must complete 3 separate sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using Fields shaded in yellow are required. All cells that are shaded in light green are down lists. You do not need to populate cells shaded in gray, as they are automatically populated

Please Do Not modify the structure of this spreadsheet by adding or subtracting Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

1. Please enter the the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family requred for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constiuent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 

# and , and Hg+2 

# . However, both the Volatile Organic HAP worksheets allow you to use a drop

-down provided in the Constituent field to define as many records as needed to record each HAP that you have results for.

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure (deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field. 2. Please provide the values of all requested parameters for each of the 3 sample testing periods in the Sample 1, Sample

3. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

# If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O2 (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). Please provide any other information that you feel may be important in the Other Supporting Information field.

# EIA

Facility Code Facility Name Boiler ID

# Control Device Configuraton

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Sample 3 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate

Sample 3

Emission Test Results CO Emission Rate Sample 1 (lb/MMBtu) CO Emission Rate Sample 1 (ppmvd @ 7% O2) CO Emission Rate Sample 2 (lb/MMBtu)

# Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Unit of Measure Fuel Flow Measurement Method Other Supporting

Information

CO Emission Rate Sample 2 (ppmvd @ 7% O2) CO Emission Rate Sample 3 (lb/MMBtu) CO Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used (ex. U.S. EPA Method 10A) Other Supporting Information

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Sample 3 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate

Sample 3

Emission Test Results Formaldehyde Emission Rate Sample 1 (lb/MMBtu) Formaldehyde

Emission Rate Sample 1 (ppmvd @ 7% O2) Formaldehyde Emission Rate Sample 2 (lb/MMBtu)

# Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Unit of Measure Fuel Flow Measurement Method Other Supporting

Information

Formaldehyde Emission Rate Sample 2 (ppmvd @ 7% O2) Formaldehyde Emission Rate Sample 3 (lb/MMBtu) Formaldehyde

Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used (ex. U.S. EPA Method 320)

# Other Supporting

Information

# EIA

Facility Code Facility Name Boiler ID CPS Energy JK Spruce Unit 1

Parameter Sample 1 Sample 2 Date of Testing 5/10/2010 5/11/2010 SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2

Emission Test Results Methane Emission Rate Sample 1 (lb/MMBtu) Methane Emission Rate Sample 1 (ppmvd @ 7% O2)

# Sample 3 Unit of Measure Other Supporting Information 5/11/2010 1000 lb/hr

MMBtu/hr N/A %

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting Information

Methane Emission Rate Sample 2 (lb/MMBtu) Methane Emission Rate Sample 2 (ppmvd @ 7% O2) Methane Emission Rate Sample 3 (lb/MMBtu) Methane Emission Rate Sample 3 (ppmvd @ 7% O2)

# Test Method Used

(ex. U.S. EPA Method 18) Other Supporting Information

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Sample 3 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3

Emission Test Results SO2 Emission Rate Sample 1 (lb/MMBtu) SO2 Emission Rate Sample 1 (ppmvd @ 7% O2) SO2 Emission Rate Sample 2 (lb/MMBtu)

# Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Unit of Measure Fuel Flow Measurement Method Other Supporting Information

SO2 Emission Rate Sample 2 (ppmvd @ 7% O2) SO2 Emission Rate Sample 3 (lb/MMBtu) SO2 Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used (ex. U.S. EPA Method 6)

# Other Supporting

Information

# EIA

Facility Code Facility Name Boiler ID CPS Energy JK Spruce Unit 1

Parameter Sample 1 Sample 2 Date of Testing 5/6/2010 5/6/2010 SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2

Emission Test Results Total Vapor Phase Me rcury Emission Rate Sample 1 (lb/MMBtu) Total Vapor Phase

Me rcury Emission Rate Sample 2 (lb/MMBtu) 3.12E-06 2.92E-06

# Sample 3 Unit of Measure Other Supporting Information 5/7/2010 1000 lb/hr

MMBtu/hr N/A %

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information

Total Vapor Phase Me rcury Emission Rate Sample 3 (lb/MMBtu) Test Method Used (ex. U.S. EPA Method 30B) Other Supporting

Information 3.48E-06 U.S. EPA Method 30B

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2

Emission Test Results Me rcury Species Me rcury Emission Rate Sample 1 (lb/MMBtu) Hg 0 

# Hg +2 

# Hg P

# Sample 3 Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information

Me rcury Emission Rate Sample 2 (lb/MMBtu) Me rcury Emission Rate Sample 3 (lb/MMBtu) Test Method Used

(ex. ASTM Method D6784) Other Supporting InformationEIA Facility Code Facility Name Boiler ID

CPS Energy JK Spruce Unit 1

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 5/11/2010 5/11/2010 5/11/2010 Steam Output (1000 lb/hr) 1000 lb/hr Total Heat Input (MMBtu/hr) MMBtu/hr Basis (Wet/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture % Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information bituminous 1020554 1046503 1014947 lb/hour

Compound (use drop down to define for as many

rows as needed) Volatile Organic HAP Emission Rate Sample

1 (lb/MMBtu) Volatile Organic HAP

Emission Rate Sample

1 (ug/dscm @ 7% O2) Volatile Organic HAP Emission Rate Sample 2 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 2 (ug/dscm @ 7% O2) Volatile Organic

HAP Emission Rate Sample 3 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 3 (ug/dscm @ 7% O2) Test Method

Used Other

Supporting Information Dichlorodifluoromethane [<2.85E-06] [<3.11] [<4.39E-06] [<4.78] [<2.91E-06] [<3.18] U.S. EPA Method 0031 with SW-846 Method 8260B Chloromethane [5.46E-06] [5.96] [8.53E-06] [9.29] [5.00E-06] [5.45] U.S. EPA Method 0031 with SW-846 Method 8260B Vinyl chloride [<1.20E-06] [<1.31] [<1.90E-06] [<2.07] [<1.23E-06] [<1.34] U.S. EPA Method 0031 with SW-846 Method 8260B Bromomethane [<7.13E-06] [<7.77] [<1.20E-05] [<13.04] [<7.28E-06] [<7.94] U.S. EPA Method 0031 with SW-846 Method 8260B Chloroethane [<2.44E-06] [<2.66] [<3.97E-06] [<4.33] [<2.50E-06] [<2.72] U.S. EPA Method 0031 with SW-846 Method 8260B Trichlorofluoromethane [<4.52E-06] [<4.93] [<7.96E-06] [<8.68] [<4.62E-06] [<5.04] U.S. EPA Method 0031 with SW-846 Method 8260B Acetone [<2.30E-05] [<25.09] [<3.83E-05] [<41.78] [<2.36E-05] [<25.74] U.S. EPA Method 0031 with SW-846 Method 8260B

Iodomethane [<2.02E-06] [<2.20] [<3.01E-06] [<3.28] [<2.06E-06] [<2.25] U.S. EPA Method 0031 with SW-846 Method 8260B Carbon disulfide [<2.17E-06] [<2.36] [<3.03E-06] [<3.30] [<2.21E-06] [<2.41] U.S. EPA Method 0031 with SW-846 Method 8260B Methylene chloride [3.36E-06] [3.66] [<5.12E-06] [<5.59] [3.57E-06] [3.89] U.S. EPA Method 0031 with SW-846 Method 8260B 1,1-Dichloroethane [<1.20E-06] [<1.31] [<1.90E-06] [<2.07] [<1.23E-06] [<1.34] U.S. EPA Method 0031 with SW-846 Method 8260B

Chloroform [<1.20E-06] [<1.31] [<1.90E-06] [<2.07] [<1.23E-06] [<1.34] U.S. EPA Method 0031 with SW-846 Method 8260B 1,2-Dichloroethane [<1.31E-06] [<1.43] [<2.14E-06] [<2.34] [<1.34E-06] [<1.46] U.S. EPA Method 0031 with SW-846 Method 8260B 2-Butanone (MEK) [<2.26E-05] [<24.59] [<3.78E-05] [<41.16] [<2.31E-05] [<25.13] U.S. EPA Method 0031 with SW-846 Method 8260B

Carbon tetrachloride [<1.80E-06] [<1.96] [<2.64E-06] [<2.88] [<1.84E-06] [<2.00] U.S. EPA Method 0031 with SW-846 Method 8260B Benzene [<1.40E-06] [<1.52] [<2.22E-06] [<2.42] [<1.42E-06] [<1.55] U.S. EPA Method 0031 with SW-846 Method 8260B 1,1,2-Trichloroethane [<1.80E-06] [<1.96] [<2.64E-06] [<2.88] [<1.84E-06] [<2.00] U.S. EPA Method 0031 with SW-846 Method 8260B 1,2-Dichloropropane [<1.42E-06] [<1.55] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B

Dibromomethane [<1.42E-06] [<1.55] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B Bromodichloromethane [<1.20E-06] [<1.31] [<1.99E-06] [<2.17] [<1.23E-06] [<1.34] U.S. EPA Method 0031 with SW-846 Method 8260B cis-1,3-Dichloropropene [<1.20E-06] [<1.31] [<1.90E-06] [<2.07] [<1.23E-06] [<1.34] U.S. EPA Method 0031 with SW-846 Method 8260B trans-1,3-Dichloropropene [<1.54E-06] [<1.68] [<2.51E-06] [<2.73] [<1.57E-06] [<1.71] U.S. EPA Method 0031 with SW-846 Method 8260B

2-Hexanone U.S. EPA Method 0031 with SW-846 Method 8260B Toluene [<1.52E-06] [<1.66] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B

Chlorobenzene [<1.42E-06] [<1.55] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B 1,1,1,2-Tetrachloroethane [<1.42E-06] [<1.55] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B Ethylbenzene [<1.42E-06] [<1.55] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B

Styrene [<1.42E-06] [<1.55] [<2.26E-06] [<2.46] [<1.46E-06] [<1.59] U.S. EPA Method 0031 with SW-846 Method 8260B o-Xylene [<1.80E-06] [<1.96] [<2.64E-06] [<2.88] [<1.84E-06] [<2.00] U.S. EPA Method 0031 with SW-846 Method 8260B Bromoform [<1.20E-06] [<1.31] [<2.27E-06] [<2.47] [<1.23E-06] [<1.34] U.S. EPA Method 0031 with SW-846 Method 8260B 1,1,2,2-Tetrachloroethane [<4.52E-06] [<4.93] [<7.96E-06] [<8.68] [<4.62E-06] [<5.04] U.S. EPA Method 0031 with SW-846 Method 8260B 1,2,3-Trichloropropane [<2.02E-06] [<2.20] [<3.01E-06] [<3.28] [<2.06E-06] [<2.25] U.S. EPA Method 0031 with SW-846 Method 8260B 1,3-Dichlorobenzene [<1.80E-06] [<1.96] [<2.64E-06] [<2.88] [<1.84E-06] [<2.00] U.S. EPA Method 0031 with SW-846 Method 8260B 1,4-Dichlorobenzene [<1.80E-06] [<1.96] [<2.64E-06] [<2.88] [<1.84E-06] [<2.00] U.S. EPA Method 0031 with SW-846 Method 8260B 1,2-Dichlorobenzene [<1.80E-06] [<1.96] [<2.64E-06] [<2.88] [<1.84E-06] [<2.00] U.S. EPA Method 0031 with SW-846 Method 8260B Speciated Volatile Organic HAP Emission DataEIA Facility Code Facility Name Boiler ID CPS Energy JK Spruce Unit 1

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure Other Supporting Information Date of Testing 5/10/2010 5/11/2010 5/11/2010 Steam Output (1000 lb/hr) 1000 lb/hr Total Heat Input (MMBtu/hr) MMBtu/hr Basis (W et/Dry) Dry Dry Dry N/A Exhaust Steam % Moisture % Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting Information bituminous

Compound (use drop down to define for as many rows as needed) Semi-Volatile Organic HAP Emission Rate Sample 1 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 1 (ug/dscm @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 2 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 2 (ug/dscm @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 3 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 3 (ug/dscm @ 7% O2) Test Method Used Other

Supporting Information 1,2,4-Trichlorobenzene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 1,2-Dichlorobenzene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 1,3-Dichlorobenzene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 1,4-Dichlorobenzene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 1-Chloronaphthalene U.S. EPA Method 0010 with SW-846 Method 8270D

2,4,5-Trichlorophenol [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 2,4,6-Trichlorophenol [<6.94E-06] [<7.57E+00] [<6.80E-06] [<7.42E+00] [<6.83E-06] [<7.45E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 2,4-Dichlorophenol [<5.56E-06] [<6.06E+00] [<5.44E-06] [<5.93E+00] [<5.47E-06] [<5.96E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 2,4-Dimethylphenol [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 2,4-Dinitrophenol [<1.39E-05] [<1.51E+01] [<1.36E-05] [<1.48E+01] [<1.37E-05] [<1.49E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 2,4-Dinitrotoluene [<2.78E-06] [<3.03E+00] [<2.72E-06] [<2.97E+00] [<2.73E-06] [<2.98E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 2,6-Dinitrotoluene [<4.17E-06] [<4.54E+00] [<2.86E-06] [<3.12E+00] [<4.10E-06] [<4.47E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 2-Chloronaphthalene [<4.17E-07] [<4.54E+01] [<4.08E-07] [<4.45E+01] [<4.10E-07] [<4.47E-01] U.S. EPA Method 0010 with SW-846 Method 8270D 2-Chlorophenol [<1.11E-05] [<1.21E+01] [<1.09E-05] [<1.19E+01] [<1.09E-05] [<1.19E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 2-Methylnaphthalene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D 2-Methylphenol [<1.25E-05] [<1.36E+01] [<1.22E-05] [<1.34E+01] [<1.23E-05] [<1.34E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 2-Nitroaniline [<2.78E-05] [<3.03E+01] [<2.72E-05] [<2.97E+01] [<2.73E-05] [<2.98E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 2-Nitrophenol [<6.94E-06] [<7.57E+00] [<6.80E-06] [<7.42E+00] [<6.83E-06] [<7.45E+00] U.S. EPA Method 0010 with SW-846 Method 8270D

3,3'-Dichlorobenzidine [<1.11E-05] [<1.21E+01] [<1.09E-05] [<1.19E+01] [<1.09E-05] [<1.19E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 3-Nitroaniline [<2.78E-05] [<3.03E+01] [<2.72E-05] [<1.36E-05] [<2.73E-05] [<2.98E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 4,6-Dinitro-2-methylphenol [<1.39E-05] [<1.51E+01] [<1.36E-05] [<1.48E+01] [<1.37E-05] [<1.49E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 4-Bromophenyl phenyl ether [<2.78E-06] [<3.03E+00] [<2.72E-06] [<2.97E+00] [<2.73E-06] [<2.98E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 4-Chloro-3-methylphenol [<6.94E-06] [<7.57E+00] [<6.80E-06] [<7.42E+00] [<6.83E-06] [<7.45E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 4-Chloroaniline [<2.78E-05] [<3.03E+01] [<2.72E-05] [<2.97E+01] [<2.73E-05] [<2.98E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 4-Chlorophenyl phenyl ether [<4.17E-06] [<4.54E+00] [<4.08E-06] [<4.45E+00] [<4.10E-06] [<4.47E+00] U.S. EPA Method 0010 with SW-846 Method 8270D 4-Nitroaniline [<2.78E-05] [<3.03E+01] [<2.72E-05] [<2.97E+01] [<2.73E-05] [<2.98E+01] U.S. EPA Method 0010 with SW-846 Method 8270D 4-Nitrophenol [<1.39E-05] [<1.51E+01] [<1.36E-05] [<1.48E+01] [<1.37E-05] [<1.49E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Acenaphthene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Acenaphthylene [<2.08E-07] [<2.27E-01] [<2.63E-07] [<2.87E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Aniline [<2.78E-05] [<3.03E+01] [<2.72E-05] [<2.97E+01] [<2.73E-05] [<2.98E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Anthracene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzidine [<8.33E-05] [<9.08E+01] [<8.16E-05] [<8.90E+01] [<8.20E-05] [<8.94E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Benz(a)anthracene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzo(a)pyrene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzo(b)fluoranthene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzo(g,h,i)perylene [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzo(k)fluoranthene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzoic acid [<1.44E-05] [<1.56E+01] [<2.40E-05] [<2.62E+01] [<2.00E-05] [<2.18E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Benzyl alcohol [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Butyl benzyl phthalate [<2.78E-06] [<3.03E+00] [<2.72E-06] [<2.97E+00] [<2.73E-06] [<2.98E+00] U.S. EPA Method 0010 with SW-846 Method 8270D

Bis(2-chloroethoxy)methane [<5.56E-06] [<6.06E+00] [<5.44E-06] [<5.93E+00] [<5.47E-06] [<5.96E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Bis(2-chloroethyl) ether [<6.94E-06] [<7.57E+00] [<6.80E-06] [<7.42E+00] [<6.83E-06] [<7.45E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Bis(2-chloroisopropyl) ether [<6.94E-06] [7.57E+00] [<6.80E-06] [7.42E+00] [<6.83E-06] [7.45E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Bis(2-ethylhexyl) phthalate [<2.04E-05] [<2.22E+01] [<2.49E-05] [<2.72E+01] [<2.60E-05] [<2.83E+01] U.S. EPA Method 0010 with SW-846 Method 8270D

Chrysene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Dibenz(a,h)anthracene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Dibenzofuran [<2.78E-05] [<3.03E+01] [<2.72E-05] [<2.97E+01] [<2.73E-05] [<2.98E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Diethyl phthalate [<6.94E-06] [<7.57E+00] [<4.54E-06] [<4.94E+00] [<4.10E-06] [<4.47E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Dimethyl phthalate [<4.17E-06] [<4.54E+00] [<4.08E-06] [<4.45E+00] [<4.10E-06] [<4.47E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Di-n-butyl phthalate [<5.09E-06] [<5.55E+00] [<4.08E-06] [<4.45E+00] [<4.10E-06] [<4.47E+00] U.S. EPA Method 0010 with SW-846 Method 8270D

Fluoranthene [<2.18E-07] [<2.37E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Fluorene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Hexachlorobenzene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Hexachlorobutadiene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Hexachlorocyclopentadiene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Hexachloroethane [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Indeno(1,2,3-cd)pyrene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Isophorone [<1.39E-05] [<1.51E+01] [<1.36E-05] [<1.48E+01] [<1.37E-05] [<1.49E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Naphthalene [<4.17E-07] [<4.54E+01] [<4.08E-07] [<4.45E-01] [<4.10E-07] [<4.47E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Nitrobenzene [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D N-Nitrosodimethylamine [<4.17E-05] [<4.54E+01] [<4.08E-05] [<4.45E+01] [<4.10E-05] [<4.47E+01] U.S. EPA Method 0010 with SW-846 Method 8270D N-Nitrosodi-n-propylamine [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D N-Nitrosodiphenylamine [<8.33E-06] [<9.08E+00] [<8.16E-06] [<8.90E+00] [<8.20E-06] [<8.94E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Pentachlorophenol [<1.25E-05] [<1.36E+01] [<1.22E-05] [<1.34E+01] [<1.23E-05] [<1.34E+01] U.S. EPA Method 0010 with SW-846 Method 8270D Phenanthrene [<3.38E-07] [<3.68E-01] [<2.45E-07] [<2.67E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Phenol [<6.94E-06] [<7.57E+00] [<6.80E-06] [<7.42E+00] [<6.83E-06] [<7.45E+00] U.S. EPA Method 0010 with SW-846 Method 8270D Pyrene [<2.08E-07] [<2.27E-01] [<2.04E-07] [<2.23E-01] [<2.05E-07] [<2.23E-01] U.S. EPA Method 0010 with SW-846 Method 8270D Speciated Semi Volatile Organic HAP Emission Data

# EIA

Facility Code Facility Name Boiler ID CPS Energy JK Spruce Unit 1

Parameter Sample 1 Sample 2 Sample 3 Date of Testing 5/6/2010 5/6/2010 5/6/2010 SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 Fuel Input Rate Sample 3

Emission Test Results Hydrogen Cyanide Emission Rate Sample 1 (lb/MMBtu) Hydrogen Cyanide

Emission Rate Sample 2 (lb/MMBtu) Hydrogen Cyanide

Emission Rate Sample 3 (lb/MMBtu) 3.20E-04 3.13E-04 3.17E-04

# Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Unit of Measure Fuel Flow Measurement Method

Test Method Used (ex. U.S. EPA

Conditional Test Method 033) Other Supporting Information U.S. EPA Conditional Test Method 033 (CTM-033)

# Other Supporting Information

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2

Emission Test Results Constituent Consitutent Emission Rate Sample 1 (%)
O 2 

# CO 2

# Sample 3 Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting Information

Consitutent Emission Rate

Sample 2 (%) Consitutent Emission Rate Sample 3 (%) Test Method Used

(ex. U.S. EPA

Method 3B) Other Supporting Information

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2

Emission Test Results Constituent Nitrogen Oxides Emission Rate Sample 1 (lb/MMBtu) NO NO 2

# Sample 3 Unit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method

Nitrogen Oxides Emission Rate

Sample 1 (ppmvd @ 7% O2) Nitrogen Oxides Emission Rate Sample 2 (lb/MMBtu) Nitrogen Oxides Emission Rate Sample 2 (ppmvd @ 7% O2)

# Other Supporting Information

Nitrogen Oxides Emission Rate

Sample 3 (lb/MMBtu) Nitrogen Oxides Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used (ex. U.S. EPA

Method 7)

# Other Supporting

Information

# EIA

Facility Code Facility Name Boiler ID 0 0 0

Parameter Sample 1 Sample 2 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (W et/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2

Emission Test Results Constituent Constituent Emission Rate Sample 1 (mg solids/liter) Total Dissolved Solids (TDS) Total Suspended Solids (TSS)

# Sample 3 Unit of Measure

1000 lb/hr MMBtu/hr N/A %

Fuel Input Rate Sample 3 Unit of Measure

Constituent Emission Rate

Sample 2 (mg solids/liter) Constituent Emission Rate Sample 3 (mg solids/liter)

# Other Supporting Information

Fuel Flow Measurement Method

Test Method Used (ex. Standard Test Method for Filterable and Nonfilterable Matter in Water ASTM D5907)

# Other Supporting

Information

Other Supporting Information