United States Department of Agriculture

December 2018

Dear Reader:

We are pleased to present the Pesticide Data Program’s (PDP) 27th Annual Summary for 

calendar year 2017. The U.S. Department of Agriculture (USDA), Agricultural Marketing 

Service (AMS), conducts this program each year to collect data on pesticide residues in food. 

This report shows that when pesticide residues are found on foods, they are nearly always at 

levels below the tolerances set by the U.S. Environmental Protection Agency (EPA).

Over 99 percent of the products sampled through PDP had residues below the EPA tolerances. 

Ultimately, if EPA determines a pesticide is not safe for human consumption, it is removed from 

the market. 

The PDP tests a wide variety of domestic and imported foods, with a strong focus on foods 

that are consumed by infants and children. EPA relies on PDP data to conduct dietary risk 

assessments and to ensure that any pesticide residues in foods remain at safe levels. USDA 

uses the data to better understand the relationship of pesticide residues to agricultural practices 

and to enhance USDA’s Integrated Pest Management objectives. USDA also works with U.S. 

growers to improve agricultural practices.

The PDP is not designed for enforcement of EPA pesticide residue tolerances. Rather, the 

U.S. Food and Drug Administration (FDA) is responsible for enforcing EPA tolerances. PDP 

provides FDA and EPA with monthly reports of pesticide residue testing and informs the FDA if 

residues detected exceed the EPA tolerance or have no EPA tolerance established.

The PDP works with State agencies representing all census regions of the country and 

approximately half of the U.S. population. In 2017, samples were collected and analyzed in 

California, Colorado, Florida, Maryland, Michigan, New York, North Carolina, Ohio, Texas, 

and Washington.

For more information about PDP, please visit our website at https://www.ams.usda.gov/

datasets/pdp. For more information about pesticides and food, please visit EPA’s website 

at http://www.epa.gov/safepestcontrol and FDA’s website at http://www.fda.gov/Food/

FoodborneIllnessContaminants/Pesticides.

Agricultural Marketing Service

1400 Independence Avenue, SW, Washington, DC 20250-0201

Voice (202) 720-8998 Fax (202) 720-7135

An Equal Opportunity Provider and Employer
Pesticide Data Program—Annual Summary, Calendar Year 2017

iii

Contents

Page No.

Acknowledgements........................................................................................................................ vii

Executive Summary...................................................................................................................... ix

Acronyms and Abbreviations........................................................................................................ xi

Section I--Introduction............................................................................................................... 1

Section II--Sampling Operations............................................................................................... 4

Conceptual Framework.................................................................................................... 4

Sampling Procedures....................................................................................................... 5

2017 Sampling Operations.............................................................................................. 6

Fresh and Processed Commodities.................................................................................. 8

Honey............................................................................................................................... 10

Milk................................................................................................................................. 11

Bottled Water................................................................................................................... 11

Sampling Limitations...................................................................................................... 11

Section III--Laboratory Operations......................................................................................... 12

Overview.......................................................................................................................... 12

Fresh and Processed Commodities.................................................................................. 14

Honey............................................................................................................................... 14

Milk.................................................................................................................................. 14

Bottled Water.................................................................................................................... 14

Quality Assurance Program............................................................................................. 15

Section IV--Database Management.......................................................................................... 16

Electronic Data Path........................................................................................................ 17

Data Reporting................................................................................................................ 17

Online Database Search Tool.......................................................................................... 17

Section V--Sample Results and Discussion.............................................................................. 17

Overview......................................................................................................................... 17

Import Versus Domestic Residue Comparisons.............................................................. 19

Postharvest Applications................................................................................................. 20

Discussion of Results ..................................................................................................... 20

Special Projects............................................................................................................... 21

Environmental Contaminants.......................................................................................... 21

Tolerance Violations........................................................................................................ 22
Pesticide Data Program—Annual Summary, Calendar Year 2017

v

Figures Page No.

 1 Pesticide Data Program (PDP) Program Operations Support and Data Users................... 2

 2 Program Participants........................................................................................................... 3

 3 Commodity Origin.............................................................................................................. 9

 4 Origin of Selected Fresh Commodity: Snap Peas............................................................. 11

 5 Pesticide Data Program (PDP) Data Pathway..................................................................... 18

Tables

 1 Pesticide Data Program (PDP) Commodity Collection Schedule for 2017........................ 6

 2 Distribution of Samples Collected by Each Participating State.......................................... 7

 3 Acceptable Products for Collected Commodities................................................................ 8

 4 Quantile Estimates for Lettuce/Imidacloprid....................................................................... 12

 5 Sample Preparation Steps for Analysis................................................................................ 13

 

Appendixes A-K

Appendix A Commodity History

Appendix B Distribution of Residues by Pesticide in Fruit and Vegetables

Appendix C Distribution of Residues by Pesticide in Honey

Appendix D Distribution of Residues by Pesticide in Milk

Appendix E Distribution of Residues by Pesticide in Bottled Water

Appendix F Distribution of Residues for Environmental Contaminants

Appendix G Sample Origin by State or Country

Appendix H Import Versus Domestic Pesticide Residue Comparisons

Appendix I Pesticide Residues by Commodity

Appendix J Number of Pesticides Detected per Sample

Appendix K Samples Reported to the U.S. Food and Drug Administration 

 as Exceeding the Tolerance or Without Established Tolerance
Pesticide Data Program—Annual Summary, Calendar Year 2017

vii

Acknowledgements

The States participating in the Pesticide Data 

Program (PDP) deserve special recognition for 

their contributions to the program. The dedication 

and flexibility of sample collectors allow the U.S. 

Department of Agriculture’s (USDA) Agricultural 

Marketing Service (AMS) to adjust sampling 

protocols when responding to changing trends 

in commodity distribution and availability. PDP 

acknowledges the contributions of the State 

laboratories in providing testing services to the 

program and the USDA National Agricultural 

Statistics Service for providing statistical support. 

PDP also acknowledges the exceptional support 

of the Health Effects Division staff of the U.S. 

Environmental Protection Agency, Office of 

Pesticide Programs, and the U.S. Food and 

Drug Administration, Center of Food Safety and 

Nutrition, Office of Food Safety, in helping to set 

the direction for PDP. 

 

Data presented in this report are the latest available 

and were collected and processed through the 

efforts of the following organizations:

USDA Program Administration

Agricultural Marketing Service

Science and Technology Program

1400 Independence Ave., SW

South Building, Mail Stop 0270

Washington, DC 20250

Ruihong Guo, Ph.D., Deputy Administrator

Science and Technology Program

(202) 720-8556, Facsimile (202) 720-6496

Monitoring Programs Division, AMS

1400 Independence Ave, SW

Room 0611-S, Stop 0276

Washington, DC 20250: 

(202) 572-8167, Facsimile (202) 619-1724

Electronic-mail Address:

amsmpo.data@usda.gov

Website:

http://www.ams.usda.gov/pdp

Participating State Agencies

California Department of Food and Agriculture

California Department of Pesticide Regulation

Colorado Department of Agriculture

Florida Department of Agriculture and

 Consumer Services

Maryland Department of Agriculture

Michigan Department of Agriculture and 

 Rural Development

New York Department of Agriculture and 

 Markets

North Carolina Department of Agriculture &

 Consumer Services

Ohio Department of Agriculture

Texas Department of Agriculture

Washington State Department of Agriculture

Participating Laboratories

California Department of Food and Agriculture

Division of Inspection Services

Center for Analytical Chemistry

3292 Meadowview Rd.

Sacramento, CA 95832

 

Florida Department of Agriculture and

 Consumer Services

Chemical Residue Laboratory

3125 Conner Blvd., Bldg. 3

Tallahassee, FL 32399-1650

Michigan Department of Agriculture and 

 Rural Development

Laboratory Division

1615 South Harrison Rd.

East Lansing, MI 48823-5224

New York Department of Agriculture 

 and Markets

Food Laboratory

6 Harriman Campus Road

Albany, NY 12235
Pesticide Data Program—Annual Summary, Calendar Year 2017

viii

Ohio Department of Agriculture

Consumer Analytical Laboratory

8995 East Main St.

Reynoldsburg, OH 43068

Texas Department of Agriculture

Pesticide Laboratory

1500 Research Parkway, Ste. B100

College Station, TX 77845

United States Department of Agriculture

Agricultural Marketing Service

National Science Laboratories

801 Summit Crossing Pl.

Gastonia, NC 28054

Washington State Department of Agriculture

Chemical and Hop Laboratory

21 N. 1st Ave., Ste. 106

Yakima, WA 98902

In memory of Diana Haynes

In August 2018, the Pesticide Data Program lost a wonderful leader, 

colleague and friend. Diana had been a part of the Pesticide Data Program 

from its inception in 1991, first working as a chemist at the Washington 

State Department of Agriculture to eventually becoming the Director of 

the program in 2014. Her knowledge of the Pesticide Data Program was 

unsurpassed. Diana will be greatly missed by all who have known and 

worked with her.
Pesticide Data Program—Annual Summary, Calendar Year 2017

ix

Executive Summary

In 1991, the U.S. Department of Agriculture 

(USDA), Agricultural Marketing Service (AMS), 

was charged with designing and implementing 

the Pesticide Data Program (PDP) to collect data 

on pesticide residues in food. PDP provides highquality data on residues in food, particularly foods 

most likely consumed by infants and children. 

This 27th Pesticide Data Program summary 

presents results for samples collected in 2017.

This information is provided to the U.S. 

Environmental Protection Agency (EPA). Before 

a company can sell or distribute any pesticide in the 

United States, EPA reviews studies on the pesticide 

to ensure that it will not pose unreasonable risks 

to human health or the environment. Once EPA 

has made that determination, it will license or 

register that pesticide for use in strict accordance 

with label directions. 

Before allowing a pesticide to be used on a food 

commodity, EPA sets limits on how much of a 

pesticide may be used on food during growing, 

processing, and storage, and how much can 

remain on the food that reaches the consumer. In 

setting the tolerance, EPA makes a safety finding 

that the pesticide can be used with a reasonable 

certainty of no harm by considering the toxicity 

of the pesticide, how much of the pesticide is 

applied and how often, how much of the pesticide 

remains in or on food by the time it is marketed 

and prepared, and all possible routes of exposure 

including use on crops, exposure from drinking 

water, and residential exposure. Government 

inspectors monitor food in interstate commerce to 

ensure that these limits are not exceeded. EPA also 

sets standards to protect workers from exposure 

to pesticides on the job. 

AMS’s Monitoring Programs Division (MPD) 

is responsible for the administration, planning, 

and coordination of day-to-day PDP operations. 

MPD meets regularly with EPA and other 

Government agencies to establish program 

priorities and direction. In 2017, sampling and/or 

testing program operations were carried out with 

the support of 10 States: California, Colorado, 

Florida, Maryland, Michigan, New York, North 

Carolina, Ohio, Texas, and Washington. These 

States had a prominent role in program planning 

and policy setting, particularly policies relating to 

quality assurance.

PDP commodity sampling is based on a rigorous 

statistical design that ensures the data are reliable 

for use in exposure assessments and can be used 

to draw various conclusions about the Nation’s 

food supply. The pesticides and commodities to 

be included each year in the sampling are selected 

based on EPA data needs and take into account the 

types and amounts of food consumed by infants 

and children. The number of samples collected by 

the States is apportioned according to that State’s 

population. Samples are randomly chosen close to 

the time and point of consumption (i.e., distribution 

centers rather than at the farm gate) and reflect what 

is typically available to the consumer throughout 

the year. Samples are selected without regard 

to country of origin, variety, growing season, or 

organic labeling.

Fresh and processed fruit and vegetables accounted 

for 83.1 percent of the total 10,541 samples 

collected in 2017. Other samples collected included 

honey (3.0 percent), milk (6.7 percent), and bottled 

water (7.2 percent). Fresh and processed fruit and 

vegetables tested during 2017 were: applesauce, 

asparagus, cabbage, cranberries (fresh and frozen), 

cucumbers, garbanzo beans (canned), grapefruit, 

kale, lettuce, mangoes, olives (canned), onions, 

pineapple (canned), plums (dried/prunes), snap 

peas, sweet potatoes, and tomatoes (canned). 

Domestic samples accounted for 72.4 percent of 

the samples, while 26.0 percent were imports, 1.1 

percent were of mixed national origin, and 0.5 

percent were of unknown origin.

Because PDP data are mainly used for risk 

assessments, PDP laboratory methods are geared 

to detect the lowest possible levels of pesticide 

residues, even when those levels are well below 

the tolerances established by EPA. Prior to testing, 

PDP analysts washed samples for 15 to 20 seconds 

with gently running cold water as a consumer 

would do; no chemicals, soap, or any special wash 

was used. Results for more than 2 million analyses 
Pesticide Data Program—Annual Summary, Calendar Year 2017

x

were reported by the laboratories in 2017 and are 

too numerous to be included in their entirety in 

this summary. The PDP database file for 2017, 

along with annual summaries and database files for 

previous years, are available on the PDP website 

at http://www.ams.usda.gov/pdp or by contacting 

MPD.

In 2017, over 99 percent of the samples tested 

had residues well below the tolerances established 

by the EPA with 53 percent having no detectable 

pesticide residue. Appendixes B through F provide 

a distribution of residues by pesticide for the 

commodities tested. Excluding bottled water, 

residues exceeding the tolerance were detected 

in 0.59 percent (58 samples) of the total samples 

tested (9,785 samples). Of these 58 samples, 24 

were domestic (41.4 percent), 32 were imported 

(55.2 percent), and 2 were of unknown origin (3.4 

percent). Residues with no established tolerance 

were found in 3.3 percent (320 samples) of the 

total samples tested (9,785 samples). Of these 320 

samples, 150 were domestic (46.9 percent) and 170 

were imported (53.1 percent).

PDP is a voluntary program and is not designed for 

enforcement of tolerances. However, PDP informs 

the U.S. Food and Drug Administration and EPA if 

detected residues exceed the EPA tolerance or have 

no EPA tolerance established.

PDP laboratories also test foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in 

the environment, particularly in soil, can be taken up 

by plants. Results for environmental contaminants 

in all commodities are listed in Appendix F. More 

information on results is provided in the Sample 

Results and Discussion section of this summary.

PDP continually strives to improve methods for 

collecting, testing, and reporting data. These data 

are freely available to EPA and other Federal and 

State agencies charged with regulating and setting 

policies on the use of pesticides and to the public 

by hard copy, internet, or custom reports generated 

by MPD. Additional copies of the PDP Annual 

Summary may be obtained by mailing the form 

provided at the end of the Summary.

In accordance with Federal civil rights law and U.S. Department of Agriculture (USDA) civil rights regulations 

and policies, the USDA, its Agencies, offices, and employees, and institutions participating in or administering 

USDA programs are prohibited from discriminating based on race, color, national origin, religion, sex, gender 

identity (including gender expression), sexual orientation, disability, age, marital status, family/parental status, 

income derived from a public assistance program, political beliefs, or reprisal or retaliation for prior civil rights 

activity, in any program or activity conducted or funded by USDA (not all bases apply to all programs). Remedies 

and complaint filing deadlines vary by program or incident.

Persons with disabilities who require alternative means of communication for program information (e.g., Braille, 

large print, audiotape, American Sign Language, etc.) should contact the responsible Agency or USDA’s TARGET 

Center at (202) 720-2600 (voice and TTY) or contact USDA through the Federal Relay Service at (800) 877-8339. 

Additionally, program information may be made available in languages other than English.

To file a program discrimination complaint, complete the USDA Program Discrimination Complaint Form, AD3027, found online at How to File a Program Discrimination Complaint and at any USDA office or write a letter 

addressed to USDA and provide in the letter all of the information requested in the form. To request a copy of the 

complaint form, call (866) 632-9992. Submit your completed form or letter to USDA by: (1) mail: U.S. Department 

of Agriculture, Office of the Assistant Secretary for Civil Rights, 1400 Independence Avenue, SW, Washington, 

D.C. 20250-9410; (2) fax: (202) 690-7442; or (3) email: program.intake@usda.gov.

USDA is an equal opportunity provider, employer, and lender.

Mention of a trade name or brand name does not constitute endorsement or recommendation by USDA over 

similar products or vendors.
Pesticide Data Program—Annual Summary, Calendar Year 2017

xi

Acronyms and Abbreviations

% C.V. Percent Coefficient of Variation

A2LA American Association for Laboratory Accreditation

AL Action Level

AMS Agricultural Marketing Service

BQL Below Quantifiable Level

CSV Comma-Separated Values

EPA U.S. Environmental Protection Agency

e-SIF Electronic Sample Information Form

FAPAS Food Analysis Performance Assessment Scheme

FDA U.S. Food and Drug Administration

FQPA Food Quality Protection Act

GAO General Accountability Office

GC Gas Chromatography

HCB Hexachlorobenzene

ISO International Organization for Standardization

LC Liquid Chromatography

LOD Limit of Detection

LOQ Limit of Quantitation

MPD Monitoring Programs Division

MRM Multiresidue Method

MS Mass Spectrometry

NASS National Agricultural Statistics Service

NSL National Science Laboratories

PDP Pesticide Data Program

PPS Probability proportionate-to-size

PT Proficiency Testing

QA Quality Assurance
Pesticide Data Program—Annual Summary, Calendar Year 2017

xii

QAU Quality Assurance Unit

QuEChERS Quick, Easy, Cheap, Effective, Rugged and Safe

QC Quality Control

RDE Remote Data Entry

SIF Sample Information Form

SOP Standard Operating Procedure

SQL Structured Query Language

USDA United States Department of Agriculture
Pesticide Data Program—Annual Summary, Calendar Year 2017

1

Pesticide Data Program (PDP)

Annual Summary, Calendar Year 2017

This summary consists of the following sections: (I.) Introduction, (II.) Sampling Operations, 

(III.) Laboratory Operations, (IV.) Database Management, and (V.) Sample Results and Discussion

I. Introduction

The U.S. Department of Agriculture’s (USDA) 

Agricultural Marketing Service (AMS) initiated the 

Pesticide Data Program (PDP) in 1991 to collect 

data on pesticide residues in food, and the program 

now has an important role in the implementation 

of the 1996 Food Quality Protection Act (FQPA). 

The law directs the Secretary of Agriculture to 

collect pesticide residue data on commodities 

most frequently consumed by infants and 

children. PDP data are used primarily by the 

U.S. Environmental Protection Agency (EPA) to 

assess dietary exposure during the review of the 

safety of existing pesticide tolerances (Maximum 

Residue Limits). EPA establishes the tolerances 

after developing a risk assessment that considers 

the following: the pesticide exposure through diet 

and drinking water and from uses in and around 

the home; the cumulative exposure to two or more 

pesticides that cause a common toxic effect; the 

possibility of increased susceptibility to infants and 

children or other sensitive subpopulations from 

exposure to the pesticide; and the possibility that 

the pesticide produces an effect in people similar 

to an effect produced by a naturally occurring 

estrogen or produces other endocrine disruptions. 

PDP data also are used by the U.S. Food and 

Drug Administration (FDA) to assist in planning 

commodity surveys for pesticide residues for its 

enforcement and regulatory programs.

Because PDP collects data on food commodities 

primarily for consumer exposure assessment, 

program operations differ markedly from those 

followed by regulatory monitoring programs for 

tolerance enforcement. Commodities chosen for 

inclusion in the program are based on EPA data 

needs. PDP samples are collected closer to the 

point of consumption and are prepared emulating 

consumer practices. PDP sampling does not impede 

commodity distribution. Laboratory operations 

are designed to achieve the lowest detectable 

levels rather than quick sample turnaround. As 

a dietary risk assessment support program, PDP 

tests for registered uses for the commodities in the 

program, as well as for pesticides that may not have 

U.S. tolerances but are used in other countries on 

commodities exported to the United States.

Figure 1(a) illustrates contributors to PDP 

policy development and planning operations. 

Primary contributors to these activities include 

the participating States, EPA, USDA’s National 

Agricultural Statistics Service (NASS), and 

additional stakeholders including industry and 

grower groups. Figure 1(b) depicts PDP primary 

data users including EPA, FDA, USDA’s Economic 

Research Service and Foreign Agricultural Service, 

participating States, academic institutions, chemical 

manufacturers, environmental interest groups, 

food safety organizations, and groups within the 

private sector representing food producers. Other 

Federal, State, and foreign government agencies 

and industries have used PDP data to promote the 

export of U.S. commodities to international markets. 

Additionally, the Codex Alimentarius Committee on 

Pesticide Residues recognizes PDP methodologies as 

official and validated methods for the determination 

of pesticide residues in foods.

In 2017, sampling services were provided by 10 

States (California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, Texas, 

and Washington). Laboratory services were provided 

by the States of California, Florida, Michigan, New 

York, Ohio, Texas, and Washington, along with the 

AMS National Science Laboratories (NSL). The 

AMS Monitoring Programs Division (MPD) is 

responsible for overall management of PDP.

Figure 2 shows the States that participate in 

program sampling and/or testing. Together, these 

States represent about 50 percent of the Nation’s 

population and all four census regions of the United 

States. They also represent major U.S. producers 

of fruit and vegetables. MPD works closely with 

EPA and FDA to select commodities and pesticides 

for testing. The selected commodities represent the 

highest U.S. consumption, with an emphasis on foods 

consumed by infants and children. Commodities are 

cycled through the program approximately every 5 
Pesticide Data Program—Annual Summary, Calendar Year 2017

2

Figure 1. Pesticide Data Program (PDP) Program Operations Support and Data Users. This figure 

illustrates (a) agencies/groups that support PDP program policy and planning activities and (b) agencies/groups 

that use PDP data. 

Program Operations

Participating 

States

National

Agricultural Statistics 

Service

Industry and

Grower Groups

Environmental

Protection

Agency

(a) PDP Policy and Planning Contributions

Data

Food and Drug 

Administration Environmental 

Protection 

Agency

Academic 

Institutions

Agricultural 

Industry

Foreign 

Agricultural 

Service

Economic 

Research 

Service

Chemical 

Manufacturers, 

Environmental 

Interest Groups, Food 

Safety Organizations

Other 

Government 

Agencies

Participating 

States

(b) PDP Data Users
Pesticide Data Program—Annual Summary, Calendar Year 2017

3

years. High-consumption fresh fruit and vegetable 

commodities remain in the program for 2 years to 

capture two full growing seasons, thereby capturing any 

changes due to seasonality or year-to-year variations. 

Processed products, as well as dairy, meat, fish, and 

grains, are tested for 1 full year. Appendix A provides 

a list of commodities tested by PDP from the beginning 

of the program in 1991 through 2018.

Fruit and vegetable samples are collected at terminal 

markets1 and large chain store distribution centers from 

which food commodities are supplied to supermarkets 

and grocery stores. Sampling at these locations allows 

Washington

California

Colorado

Texas

Ohio

New York

Florida

Maryland

Michigan

Participating State

Location of Participating State Laboratories

North Carolina

Location of Participating Federal Laboratory

Figure 2. Program Participants. During 2017, USDA’s Agricultural Marketing Service established cooperative agreements 

with 10 States to sample and/or test Pesticide Data Program commodities. Together, these States represent about 50 percent 

of the Nation’s population and all four census regions of the United States. These States are the major U.S. producers of fruit 

and vegetables. State laboratories were responsible for analyzing fresh and processed fruit and vegetable samples. The USDA 

National Science Laboratory analyzed the honey samples.

1 Terminal markets are facilities where wholesalers receive large quantities of fresh fruit and vegetables by rail, truck, and air 

from around the world for sale to grocers, restaurants, institutions, and other businesses. Terminal markets are often located 

in metropolitan areas at or near major transportation hubs.

for residue measurements that include pesticides 

applied during crop production and those applied 

after harvest (such as fungicides, growth regulators, 

and sprouting inhibitors) and takes into account 

residue degradation while food commodities are 

in storage. Participation as a PDP sampling site is 

voluntary, which sets it apart from State and Federal 

enforcement programs. In 2017, over 600 sites 

granted access and provided information, including 

site volume data, to sample collectors. Voluntary 

cooperation is important to PDP and makes it 

possible to adjust sampling protocols in response to 

fluctuations in food distribution and production.
Pesticide Data Program—Annual Summary, Calendar Year 2017

4

Pesticides screened by PDP include those with 

current registered uses for the commodity being 

tested and compounds for which toxicity data and 

preliminary estimates of dietary exposure indicate 

the need for more extensive residue data. PDP also 

monitors pesticides for which EPA has modified 

use directions (i.e., reduced application rates or 

frequency) as part of risk management activities. 

In addition, PDP tests for selected pesticides 

that may not have U.S. tolerances but are used 

in other countries that export commodities to the 

United States. The following appendixes list the 

specific pesticides tested in the program: fruit and 

vegetables (Appendix B), honey (Appendix C), 

milk (Appendix D), and bottled water (Appendix 

E). Environmental contaminants, or pesticides 

whose uses have been canceled in the United States 

but their residues persist in the environment, are 

consolidated into Appendix F, which summarizes 

findings for these chemicals across all commodities.

II. Sampling Operations

♦ Conceptual Framework

The goal of the PDP sampling program is to obtain 

a statistically valid representation of the U.S. food 

supply. PDP data reflect actual pesticide residue 

exposure from food. Using a rigorous statistical 

design, PDP has developed extensive procedures 

that ensure samples are randomly selected from the 

national food distribution system and reflect what is 

typically available to the consumer.

Ten States currently participate in PDP – California, 

Colorado, Florida, Maryland, Michigan, New York, 

North Carolina, Ohio, Texas, and Washington. The 

initial participating States in 1991 (California, 

Florida, Michigan, New York, Texas, and 

Washington) were selected based on agricultural 

production, analytical capabilities, population, 

and regional/geographic distribution – all four 

U.S. Census Regions (West, South, Midwest, 

and Northeast) were represented. Later in 1993, 

Colorado joined to represent the Mountain Division 

of the Western Region and Ohio to further represent 

the densely populated East North Central Division 

of the Midwest Region. In 1993, North Carolina 

was included to better represent the South Atlantic 

Division of the Southern Region. Maryland was 

added in 1997 to represent the South Atlantic 

Division of the Southern Region. Today, these 

States together represent about 50 percent of the 

Nation’s population and all four census regions of 

the United States.

Commodities chosen for inclusion in the program 

are based on EPA data needs. Foods selected for 

testing are high-consumption items with a strong 

focus on foods that are highly consumed by infants 

and children. Each fresh commodity is sampled and 

tested for 2 years in order to capture annual and 

seasonal variability. High-consumption items are 

rotated in and out of the program every 5 years – for 

example, apples, lettuce, and oranges are retested 

and the data refreshed every 5 years.

PDP collects a minimum of 600 samples per 

commodity per year in order to provide an accurate 

statistical representation for a given commodity. 

PDP collects additional samples to allow 

apportionment among the participating States over 

a 12-month period and to allow for a small sample 

overage for any missed, damaged, or unusable 

samples. Participating State population figures are 

used to apportion the number of samples scheduled 

for collection each month. PDP sampling operations 

may be adjusted according to product availability. 

For example, cherries, nectarines, and peaches 

may be oversampled during the summer months to 

make up for low availability during winter months. 

In some cases, frozen product is allowed as an 

alternative to fresh (e.g., cranberries).

PDP samples are collected at terminal markets and 

warehouse distribution centers, close to the point of 

consumption. Participating State agencies compile 

and maintain lists of these sampling sites. In 2017, 

over 600 sites granted access to sample collectors. 

The States provide AMS and NASS with annual 

volume information for commodities distributed 

at these sites. Based on this information, sites are 

assigned volume indicators compared to other sites 

in the same State. This volume indicator is used to 

ensure larger sites are selected more frequently than 

smaller sites. This information is used to weight 

the site to determine the probability for sample 

selection. For example, a weight of 10 may be 

given to a site that distributes 100,000 pounds of 

produce annually and a weight of 1 is given to a site 
Pesticide Data Program—Annual Summary, Calendar Year 2017

5

that distributes 10,000 pounds. This site selection 

method, termed probability-proportionate-to-size 

(PPS), then results in the larger site being 10 times 

more likely to be selected for sampling than the 

smaller site. 

Each participating State works with NASS to 

develop statistical procedures for site weighting 

and selection. States are also given the option to 

have NASS perform their quarterly site selection. 

The number of sampling sites and the volume of 

produce distributed by the sites vary greatly among 

States. Sampling plans that include sampling dates, 

sites (primary and alternate), targeted commodities, 

and testing laboratories are prepared by each State 

on a quarterly basis. Collection of commodities is 

randomly assigned to weeks of the month, prior to 

selection of specific sampling dates within a week. 

Because sampling sites are selected for an entire 

quarter, States may assign the sites to particular 

months based on geographic location.

Sample information is captured at the time of 

collection for inclusion in the PDP database. PDP 

sample origin data identify the State or country 

where the commodity was produced. A comparison 

of PDP sample origin data to State production and 

import data by USDA’s NASS shows PDP sampling 

is representative of the U.S. food supply. 

♦ Sampling Procedures

While obtaining PDP samples, collectors randomly 

select the scheduled commodities. Collectors 

use established procedures to prevent crosscontamination and maintain chain-of-custody. PDP 

State sample collectors are trained to adhere to 

detailed program Standard Operating Procedures 

(SOPs) that provide criteria for site selection 

and specific instructions for sample selection, 

shipping and handling, and chain-of-custody. SOPs 

are updated as needed and serve as a technical 

reference in conducting program sampling reviews 

to ensure program goals and objectives are met. 

PDP sampling SOPs are available on the website: 

www.ams.usda.gov/pdp. On a quarterly basis, 

sample collectors are provided with Commodity 

Fact Sheets that list specific collection details for 

the individual commodities in the program.

Temperature-sensitive samples are packed in heavyduty, temperature-controlled containers. Holding 

temperatures are preserved throughout transit time 

with the inclusion of ample frozen cold packs and 

insulating materials. Non-temperature-sensitive 

samples do not require temperature-controlled 

containers; however, they are shipped in heavy-duty, 

well-cushioned containers. To preserve sample 

integrity, most samples are shipped the same day 

by overnight delivery. Non-refrigerated processed 

commodities such as canned olives are often shipped 

by ground transportation to reduce shipping costs. 

Electronic Sample Information Forms (e-SIFs) 

are used for chain-of-custody and to capture 

information needed to characterize the sample. 

Sample collectors use tablets or laptop computers in 

the field to record sample identification information 

such as: (1) State of sample collection, (2) collection 

date, (3) sampling site code, (4) commodity code, 

and (5) testing laboratory code. Information from 

these five data elements is combined to form a 

unique PDP identification number for each sample. 

Other available information about each sample is 

also recorded, such as collector name; the State or 

country of origin; product variety; production claims 

such as organic; expiration date; and grower, packer, 

and/or distributor locations. The e-SIFs are sent 

electronically the same day as sample collection or, 

at the latest, by the next morning after collection to 

ensure that sample information is received at each 

laboratory by the time samples arrive for analysis. 

Refer to Section IV on Database Management for 

more information on the e-SIF system. 

Because most PDP samples are collected at 

distribution centers, terminal markets, and other 

wholesalers, entire cases must be obtained while a 

significantly smaller portion is sent to the laboratory 

for testing. For example, if a 20-pound case of apples 

is collected and a 5-pound sample is sent for testing, 

the remaining 15 pounds are donated. In most cases, 

the excess samples are donated to organizations 

such as local food banks, shelters, senior assisted 

living centers, churches, and other charities. PDP 

often provides the only fresh commodity donations 

available to these organizations. As a specific 

example, the State of Michigan donated over 18,000 

pounds of produce to the Greater Lansing Food 

Bank during 2017.
Pesticide Data Program—Annual Summary, Calendar Year 2017

6

♦ 2017 Sampling Operations

The number of fruit, vegetable, honey, milk and 

bottled water samples collected in each participating 

State is determined by State population. The quarterly 

collection schedule for all 2017 commodities is shown 

in Table 1. The total number of samples collected 

in each State for each commodity is listed in Table 

2. Figure 2 illustrates the participating collection 

States and the laboratories to which samples were 

shipped. Table 3 lists the acceptable product types 

for each collected commodity as seen on Commodity 

Fact Sheets provided to sample collectors. For all 

commodities, domestic or imported and organically 

grown or conventionally grown products are 

acceptable. In 2017, excluding bottled water, 6.2 

percent of the tested samples were organic (609 of 

9,785).

State population figures are used to assign the number 

of fruit, vegetable, and other specialty samples 

scheduled for collection each month. During 2017, 

the monthly number of samples assigned for each 

State included: California, 13; Colorado, 2; Florida, 

7; Maryland, 4; Michigan, 6; New York, 9; Ohio, 6; 

Texas, 8; and Washington, 4. This schedule resulted 

in a monthly target of 59 samples per commodity, or 

708 samples per commodity per year. Additionally, 

North Carolina collected 4 samples per month for 

selected commodities - applesauce, fresh and frozen 

cranberries, cucumbers, honey, lettuce, canned 

olives, canned pineapple, dried plums (prunes), 

canned tomatoes, canned garbanzo beans and 

bottled water, which resulted in a total of 63 samples 

per commodity per month for these products. 

In 2017, fruit, vegetable, honey, milk and bottled 

water samples were randomly collected by trained 

State inspectors at terminal markets and large chain 

store distribution centers throughout the country. 

Surrogate or “proxy” sites (retail markets) are 

used to collect these samples when the commodity 

of interest is unavailable at a terminal market 

or distribution center. In these instances, the 

Commodity Jan-Mar Apr-Jun Jul-Sep Oct-Dec End Date

Applesauce Sep-17

Asparagus Jun-19

Cabbage Jun-19

Cranberries, Fresh/Frozen Sep-18

Cucumbers Jun-17

Garbanzo Beans, Canned Sep-18

Grapefruit Sep-17

Honey Aug-17

Kale Dec-18

Lettuce Jun-17

Mangoes Sep-18

Milk Dec-17

Olives, Canned Sep-18

Onion Dec-17

Pineapple, Canned Dec-17

Plums, Dried (Prunes) Sep-18

Snap Peas Dec-18

Sweet Potatoes Mar-18

Tomatoes, Canned Sep-17

Water, Bottled Dec-17

Table 1. Pesticide Data Program (PDP) Commodity Collection Schedule for 2017. Samples are 

most often collected for a 2-year time period. Commodities are initiated or terminated in different 

quarters of the year so that new commodities are not brought into the program all at the same time. 

This table illustrates time ranges for the listed commodities. See Appendix A for the complete PDP 

commodity history (May 1991 through December 2018).
Pesticide Data Program—Annual Summary, Calendar Year 2017

7

State AS CA CG CU GF GK LT MA ON SN SW

Total 

Fresh

California 78 50 78 78 118 156 78 39 156 156 149 1,136

Colorado 12 13 12 12 18 24 12 6 24 24 24 181

Florida 42 40 42 42 57 85 42 22 84 86 84 626

Maryland 24 17 24 24 36 48 24 12 48 48 48 353

Michigan 36 18 36 36 54 72 36 18 72 72 72 522

New York 54 31 54 54 81 108 54 27 108 108 108 787

N. Carolina 13 24 24 61

Ohio 36 43 36 36 54 72 36 17 72 72 72 546

Texas 46 61 48 48 72 95 48 24 96 96 96 732

Washington 24 25 24 24 36 48 24 12 48 48 48 361

TOTAL 354 311 354 378 526 708 378 177 708 710 701 5,305

State AC AZ NC OL PD TC ZB

Total 

Processed

Total 

Fresh & 

Proccessed 

F&V

California 117 104 156 156 39 117 39 728 1,864

Colorado 18 9 23 24 6 18 6 104 285

Florida 63 45 85 85 22 63 21 384 1,010

Maryland 36 31 47 48 12 35 12 221 574

Michigan 54 55 72 72 18 54 18 343 865

New York 81 77 108 108 27 81 27 509 1,296

N. Carolina 36 19 48 48 13 36 12 212 273

Ohio 57 29 74 69 18 54 18 319 865

Texas 72 35 95 96 24 72 24 418 1,150

Washington 36 24 48 48 12 36 12 216 577

TOTAL 570 428 756 754 191 566 189 3,454 8,759

Commodity Legend

AC = Applesauce GK = Kale ON = Onions

AS = Asparagus HY = Honey PD = Plums, Dried (Prunes)

AZ = Cranberries, Frozen LT = Lettuce SN = Snap Peas

CA = Cranberries, Fresh MA = Mangoes SW = Sweet Potatoes

CG = Cabbage MK = Milk TC = Tomatoes, Canned

CU = Cucumbers NC = Pineapple, Canned WB= Water, Bottled

GF = Grapefruit OL = Olives, Canned ZB = Garbanzo Beans, Canned

Table 2. Distribution of Samples Collected by Each Participating State. This table includes those 

commodities collected at terminal markets, distribution centers, and retail markets. 

Honey

HY

65

10

35

20

30

45

20

30

40

20

315

Dairy

Milk

MK

156

24

85

48

72

108

74

96

48

711

Water

WB

156

24

84

48

72

108

48

72

96

48

756
Pesticide Data Program—Annual Summary, Calendar Year 2017

8

commodity is selected in the rear storage area of 

the retail facility so possible contamination by the 

consumer is eliminated and to allow capture of 

sample information from product boxes. In 2017, 

41.0 percent of fruit, vegetable, honey, milk, and 

bottled water samples were collected at proxy 

sites. The commodities most often collected at 

these facilities were applesauce, fresh and frozen 

cranberries, canned garbanzo beans, honey, milk, 

canned olives, canned pineapple, dried plums 

(prunes), canned tomatoes, and bottled water. 

The total number of samples per commodity and 

the percentage of each that were either domestic, 

Commodity Acceptable Products

Applesauce Processed applesauce; regular or chunky; sweetened/unsweetened/lite varieties. Containers

may be plastic, glass, or cans; however, plastic or cans are preferred because of potential

breakage with glass.

Asparagus Fresh green, purple, or white asparagus spears.

Cabbage Fresh, whole head cabbage (green, red, or curly/Savory); Napa cabbage (celery cabbage, tightheaded 

Chinese cabbage).

Cranberries Fresh whole cranberries, pre-bagged or loose. Fresh are preferred, but frozen are acceptable.

Cranberries, Frozen Frozen cranberries. Individually quick frozen (IQF) or frozen in own juices.

Cucumbers Fresh cucumbers. Common, English, burpless, garden, hothouse, seedless, Japanese, or Kirby.

Garbanzo Beans, 

Canned

Canned whole garbanzo beans (chickpeas).

Grapefruit Any fresh, whole grapefruit. Pink, red, or white fleshed.

Honey 100% Pure Honey; blossom flavored honey; creamed honey; honey with honeycomb in the jar.

Kale Fresh kale. Curly, Lacinato, Dinosaur, Tuscan, Red Russian, or Siberian kale. Whole leaf,

sliced, cut or chopped. Pre-bagged or loose.

Lettuce Leaf and head (wrapped or unwrapped) lettuce.

Mangoes Fresh, whole mangoes.

Milk Whole milk; pasteurized; Vitamin A and/or D fortified. Container may be glass if plastic or

carton is not available.

Olives, Canned Canned, pitted black olives. Whole, sliced, chopped, crushed, or diced.

Onions Any fresh, whole bulb onion. Yellow, white, or red.

Pineapple, Canned Canned pineapple. Slices, half-slices, broken slices, spears, tidbits, chunks, cubes, or crushed.

Canning liquid may be syrup (heavy, light, extra light), pineapple juice, or water.

Plums, Dried (Prunes) Dried, pitted plums/prunes. Potassium sorbate, sunflower oil, and medium chain triglycerides

are acceptable products.

Snap Peas Any fresh, whole edible podded pea. Snap pea, sugar pea, sugar snap pea, snow pea (Chinese

pea), or stringless sugar pea.

Sweet Potatoes Fresh, whole sweet potatoes. No individual size requirements.

Tomatoes, Canned Canned tomatoes. Whole, peeled, diced, stewed, puree, or crushed.

Water, Bottled Spring water, artesian water, well water, fluoridated water, oxygenated water, filtered water,

drinking water, purified water, distilled water, pure water, and ground water. Baby bottled water

(bottled water used for infant formula) also acceptable.

Table 3. Acceptable Products for Collected Commodities. This table lists the acceptable products for 

each collected commodity as seen on the Commodity Fact Sheets provided to sample collectors. For all 

commodities, domestic or imported and organically grown or conventionally grown products are acceptable.

imported, or of unknown origin are shown in Figure 

3. The origin of some fresh commodities can vary 

greatly throughout the year. A graphic example 

of this variation can be found in Figure 4, where 

differences in origin (domestic versus import) are 

depicted by month for snap pea samples. Fresh 

and processed fruit, vegetable, honey, milk, and 

bottled water samples originated from 45 States 

and 36 foreign countries (refer to Appendix G). 

♦ Fresh and Processed Commodities 

Of all samples collected and analyzed in 2017, 83.1 

percent (8,759 of 10,541) were fruit and vegetables, 
Pesticide Data Program—Annual Summary, Calendar Year 2017

9

Cucumbers (378 Samples)

A. Fresh Fruit and Vegetable Samples

Snap Peas (710 Samples) Sweet Potatoes (701 Samples)

Lettuce (378 Samples) Mangoes (177 Samples) Onions (708 Samples)

Grapefruit (526 Samples) Kale (708 Samples)

Cabbage (354 Samples) Cranberries (311 Samples)

Domestic 97.9%

Domestic 92.0%

Domestic 21.7%

Domestic 78.8%

Import 93.2%

Import 1.3%

Import 77.5%

Import 8.5%

Import 7.6%

Import 21.2%

Unknown 0.8%

Domestic 99.9%

Domestic 31.1%

Domestic 89.7%

Domestic 6.8%

Import 0.1%

Import 68.7%

Import 10.0%

Unknown 0.3%

Import 96.6%

Asparagus (354 Samples)

Domestic 3.4%

Import 4.0%

Unknown 0.8%

Unknown 0.8%

Domestic 95.2%

Unknown 0.4%

Domestic 91.5%

Unknown 0.2%
Pesticide Data Program—Annual Summary, Calendar Year 2017

10

including fresh and processed products. The fresh 

commodities collected for PDP were asparagus, 

cranberries, cabbage, cucumbers, grapefruit, kale, 

lettuce, mangoes, onions, snap peas, and sweet 

potatoes. The processed commodities included 

applesauce, frozen cranberries, canned pineapple, 

canned olives, dried plums (prunes), canned 

tomatoes, and canned garbanzo beans. Fresh and 

frozen fruit and vegetable samples weighed either 

3 or 5 pounds except for cranberries and snap peas 

where the sample sizes were 1 pound. Three pounds 

were collected for smaller, low-weight commodities 

such as asparagus and onions, and 5 pounds were 

collected for larger, high-weight commodities such 

as grapefruit and sweet potatoes. 

B. Processed Fruit and Vegetable Commodities

Figure 3. Commodity Origin. This figure depicts the proportion of commodity origin (domestic, import, unknown, 

and mixed national origin) for each fresh and processed fruit and vegetable product tested in 2017.

Cranberries, Frozen (428 Samples)

Domestic 95.0%

Import 1.6%

Domestic 84.1%

Applesauce (570 Samples)

Pineapples, Canned (756 Samples)

Domestic 3.0%

Unknown 0.9%

Import 15.9%

Import 17.8%

Plums, Dried (Prunes) (191 Samples)

Domestic 62.3%

Import 18.3%

Olives, Canned (754 Samples)

Domestic 81.2%

Unknown 0.5%

Garbanzo Beans, Canned (189 Samples)

Tomatoes, Canned (566 Samples)

Domestic 93.0%

Import 6.1% Domestic 93.6%

Import 3.9%

Unknown 4.8%

Unknown 0.5%

Import 97.0% Mixed National 19.4%

Unknown 1.1%

♦ Honey

PDP collected and analyzed 315 honey samples 

in 2017. Samples, comprised of 12- to 32-ounce 

containers of 100 percent pure honey, were collected 

from routine PDP sampling sites that included major 

chain-store distribution centers, terminal markets, 

and proxy sites. About 67 percent of the samples 

were collected from proxy sites. Clover honey, other 

blossom-flavored honey (such as alfalfa, orange 

blossom, tupelo, lavender, rosemary, etc.), creamed 

honey, and honey with honey combs in the jar were 

collected. Imitation honey (made from rice or corn 

syrup), solid comb honey, and honey with added 

flavors were excluded. Distribution of residues 
Pesticide Data Program—Annual Summary, Calendar Year 2017

11

Figure 4. Origin of Selected Fresh Commodity: Snap Pea Samples. Differences in origin (domestic vs. import) 

are illustrated by month. 

Origin of Snap Pea Samples

Domestic Imported Unknown

JANFEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

Number of Samples

in honey may be found in Appendix C. Pesticide 

residue analysis was performed by the USDA’s NSL 

located in Gastonia, NC. 

♦ Milk 

PDP collected and analyzed 711 milk samples 

in 2017. One-quart samples were collected from 

routine PDP sampling sites that included major 

chain-store distribution centers, terminal markets, 

and proxy sites. About 67 percent of the samples 

were collected from proxy sites. All the milk 

samples were domestic. Only whole pasteurized 

milk samples were collected. Reduced fat milk (1% 

or 2%), flavored milk (chocolate, strawberry), ultrahigh temperature pasteurized milk (not requiring 

refrigeration), and any milk other than cow’s milk 

were excluded. Distribution of residues in milk may 

be found in Appendix D. Pesticide residue analysis 

was performed by the California Department of Food 

and Agriculture laboratory located in Sacramento, 

CA.

♦ Bottled Water

PDP collected and analyzed 756 bottled water 

samples in 2017. Two-liter samples were collected 

from routine PDP sampling sites that included major 

chain-stores distribution centers, terminal markets, 

and proxy sites. About 67 percent of the samples 

were collected from proxy sites. Seltzer, flavored, 

mineral, carbonated, sparkling and sweetened water 

were excluded. Distribution of residues in bottled 

water may be found in Appendix E. Pesticide residue 

analysis was performed by the New York Department 

of Agriculture and Markets laboratory located in 

Albany, NY.

♦ Sampling Limitations

Ten States from all four census regions of the United 

States participate in PDP. The States that participate 

account for about 50 percent of the U.S. population 

and the major agricultural production areas of the 

country, making them representative of the United 

States as a whole. 

PDP collects samples from over 600 distribution 

centers and terminal markets within the participating 

States. The total number of distribution centers and 

terminal markets within the participating States is 

difficult to establish since existing sites may go out of 

business or merge and new sites may open during the 

course of the year. However, sites within the States 

that participate do not differ significantly from those 

that do not participate. Since these sites are similar 

throughout the State, they are representative of all 

sites in the State. 
Pesticide Data Program—Annual Summary, Calendar Year 2017

12

Sometimes it is necessary to replace the site that 

was originally selected using PPS. In those cases, 

an alternate site is selected by the State personnel 

to replace the original site. Whenever possible, a 

site of similar size in the same region as the original 

site is chosen as the replacement. Additionally, the 

availability of a specific commodity may necessitate 

a change in site selection. For example, lettuce may 

be collected from an alternate site if the primary site 

is out of stock.

In 2012, the General Accountability Office (GAO) 

recommended that PDP determine measures of 

sampling error for reported estimates of pesticide 

residue levels and communicate that data to the 

public. NASS performed this analysis and the results 

for a selected commodity/pesticide pair, lettuce/

imidacloprid, are presented in Table 4. Lettuce was 

sampled and tested by PDP from 2015-2017 and 

the analyses depicted in this table are for pesticide 

residue results from 2015-2016.

The percentile estimates in Table 4 are obtained from 

a design-based approach using historical patterns 

of site selection to estimate sampling weights. The 

percentile estimates for the commodity/pesticide pair 

presented are at the national level, over the span of 

the most recent sampling cycle for the commodity 

in question. Confidence intervals for the percentile 

estimates are based on estimates of the standard error 

using the Woodruff Method where applicable. The 

delete-one jackknife procedure is used to estimate 

the standard error when the Woodruff Method is not 

applicable. As would be expected, standard error 

estimates are generally larger for higher quantiles. 

The Woodruff method and the delete-one jackknife 

produce comparable standard errors for all quantiles 

estimated.

III. Laboratory Operations

♦ Overview

Seven State laboratories and one USDA laboratory 

performed analyses for PDP. These laboratories 

are equipped with instrumentation capable of 

detecting residues at very low levels. Laboratory 

staff members receive intensive training and must 

demonstrate analytical proficiency on an ongoing 

basis. Laboratory scientists continually test new 

technologies and develop new techniques to 

improve the levels of detection. Any major change 

in methodology and/or instrumentation is evaluated 

and its soundness demonstrated and documented by 

means of method validation modules in accordance 

with PDP SOPs.

Percentile Results for Lettuce/Imidacloprid

(Woodruff Method)

Quantile

Estimate 

(ppm)

Standard 

Error

Lower 95% 

Confidence 

Limit

Upper 95% 

Confidence 

Limit

50% 0.00150 0.00072 0.00008 0.00292

90% 0.01514 0.00179 0.01162 0.01867

95% 0.01970 0.00112 0.01751 0.02189

99% 0.03089 0.00284 0.02531 0.03647

Number of Sample Points = 846

Percentile Results for Lettuce/Imidacloprid

(Jackknife Method)

Quantile

Estimate 

(PPM)

Standard 

Error

Lower 95% 

Confidence 

Limit

Upper 95% 

Confidence 

Limit

50% 0.00150 0.00187 -0.00217 0.00517

90% 0.01514 0.00139 0.01241 0.01788

95% 0.01970 0.00091 0.01790 0.02149

99% 0.03089 0.00612 0.01888 0.04290

Number of Sample Points = 846

Table 4. Quantile Estimates for Lettuce/Imidacloprid. Presented here are the quantile estimates and standard 

errors for imidacloprid in lettuce as determined based on pesticide residue results from samples collected during 

2015-2016. The Woodruff method and delete-one Jackknife method produce comparable standard errors for all 

quantiles estimated.
Pesticide Data Program—Annual Summary, Calendar Year 2017

13

♦ Fresh and Processed Commodities

A total of 8,759 fresh and processed fruit and 

vegetable samples were tested for 512 parent 

pesticides, metabolites, degradates, and/or isomers, 

plus 21 environmental contaminants using MultiResidue Methods (MRMs). Pesticides screened by 

PDP include those with current registered uses for 

the commodity being tested and compounds for 

which toxicity data and preliminary estimates of 

dietary exposure indicate the need for more extensive 

residue data. 

Upon arrival at the testing facility, samples of 

fresh commodities were visually examined for 

acceptability and discarded if determined to be 

inedible (decayed, extensively bruised, or spoiled). 

Laboratories are permitted to refrigerate incoming 

fresh fruit and vegetable samples of the same 

commodity up to 72 hours to allow for different 

sample arrival times from collection sites. Frozen 

and canned commodities may be held in storage 

(freezer or shelf) until the entire sample set is ready 

for analysis.

Each sample is prepared according to the procedures 

detailed in Table 5, which lists the steps for preparing 

each commodity for analysis as defi ned in the 

Laboratory Sample Processing and Analysis SOP. 

For all commodities, the sample is chopped, mixed, 

or blended until a visually homogeneous mixture is 

attained. 

Samples are separated into analytical portions 

(aliquots) for analysis. If testing cannot be 

performed immediately, the entire analytical set is 

frozen at -40°C or lower, according to PDP’s Quality 

Assurance/Quality Control (QA/QC) requirements. 

Surplus aliquots not used for the initial testing 

are retained frozen in the event that replication of 

analysis or verifi cation testing is required.

For analysis of fruit and vegetable samples, testing 

laboratories use various Quick, Easy, Cheap, 

Effective, Rugged and Safe (QuEChERS)-based 

approaches.2

 All MRMs are determined, prior to 

use and through appropriate method validation 

procedures, to produce equivalent data for PDP 

analytical purposes.

PDP laboratories use gas chromatography (GC) 

and liquid chromatography (LC) instrumentation, 

coupled with tandem mass spectrometry 

(MS) detection systems for the simultaneous 

identifi cation/confi rmation and quantitation of 

pesticides. The use of these GC-MS/MS and LCMS/MS systems allows the program to capture 

data for a broad spectrum of pesticides, including 

emerging product chemistries.

♦ Honey

USDA’s NSL tested 315 samples of honey. A total 

of 198 parent pesticides, metabolites, degradates 

and/or isomers, plus 1 environmental contaminant 

were screened in honey samples. Samples were 

prepared according to the procedures detailed 

in Table 5. Samples were extracted using 

modifi cations of the QuEChERS method, and 

analyses were performed using GC-MS/MS and 

LC-MS/MS.

♦ Milk

The California Department of Food and 

Agriculture laboratory tested 711 samples of 

pasteurized whole milk from cows. A total of 420 

parent pesticides, metabolites, degradates and/or 

isomers, plus 18 environmental contaminants were 

screened in milk samples. Samples were prepared 

according to the procedures detailed in Table 

5. Samples were extracted using modifi cations 

of the QuEChERS method, and analyses were 

performed using GC-MS/MS, and LC-MS/MS.

♦ Bottled Water

The New York Department of Agriculture 

and Markets laboratory tested 756 samples of 

bottled water. A total of 166 parent pesticides, 

metabolites, degradates and/or isomers, plus 13 

environmental contaminants were screened in 

bottled water samples. Upon arrival at the testing 

facility, bottled water samples were visually 

examined for acceptability and discarded if 

determined to be damaged. Samples were held 

at room temperature until the entire sample set 

was ready for analysis. Samples were prepared 

according to the procedures detailed in Table 5. 

Samples were extracted using a modifi ed solid 

2

 M. Anastassiades, S.J. Lehotay, D. Stajnbaher and F.J. Schenck, “Quick, Easy, Cheap, Effective, Rugged and Safe 

(QuEChERS) Method,” J AOAC Int 86 (2003) 412.
Pesticide Data Program—Annual Summary, Calendar Year 2017

14

Commodity Sample Preparation Steps

Applesauce If the sample is comprised of a single container, simply weigh appropriate analytical portion. If

the sample is comprised of multiple containers, combine and mix enough containers to achieve

the specified sampling size (48 ounces) and weigh appropriate analytical portion.

Asparagus Remove an inch or two of the woody stem, if inedible. Wash and drain.

Cabbage Visually examine the head, and remove wrapper, damaged, or wilted leaves, and the core.

Rinse, turn the head top side down to drain.

Canned Products:

Garbanzo Beans, Olives, 

Pineapples, Tomatoes

If the lid of the can has visible dirt or dust, rinse the lid under cold running tap water for 5 to 10

seconds. Dry the lid with a paper towel. Open each can and pour the entire contents of each

can including the liquid into a blender/homogenizer.

Cranberries Wash by the handful or by using a colander and drain.

Cucumbers Wash and drain. Cucumbers may be halved or quartered to facilitate homogenization.

Frozen Product:

Cranberries

The samples may be chopped while frozen, or to prevent damage to the chopper/homogenizer

blades, the sample may be thawed in a refrigerator or in a room temperature water bath. Open

the containers and pour the entire contents into the chopper/homogenizer.

Grapefruit Peel each fruit and remove any excess white membrane.

Honey If the sample is comprised of a single container, simply weigh appropriate analytical portion. If

the sample is comprised of multiple containers, combine and mix enough containers to achieve

the specified sampling size (12 to 32 ounces) and weigh the approproate analytical portion.

Kale Visually examine the sample and remove only the damaged or wilted leaves and any woody

stems. Wash and drain. Note: Bagged pre-washed kale do not require washing.

Lettuce - Head Visually examine the head and remove wrapper and damaged or wilted leaves. Rinse and turn

the head top side down to drain.

Lettuce - Leaf Visually examine the sample and remove only the damaged or wilted leaves and any woody

stems. Wash and drain.

Mangoes Wash and drain. Do not remove peel. Remove stem if present. Cut the mango around the pit to 

remove it, being careful to remove as little of the meat as possible.

Milk If the sample is comprised of a single container, simply weigh appropriate analytical portion. If

the sample is comprised of multiple containers, combine and mix enough containers to achieve

the specified sampling size (1 quart) and weigh appropriate analytical portion.

Onions Remove top outer layer, the first white layer and membrane, and any other inedible portions.

Remove root portion last to minimize fumes. Wash and drain.

Plums, Dried (Prunes) Open all of the dried fruit package(s) into a container and mix or shake to obtain a

representative analtyical portion. Add enough water to cover the analytical portion and soak

with water until re-hydrated. Prepare for extraction.

Snap Peas Wash and drain. Remove inedible portion(s). Note: Bagged pre-washed, ready-to-eat, and

steam in a bag snap peas do not require washing.

Sweet Potatoes Hold each sweet potato under cold running tap water and gently scrub the entire surface with a

clean vegetable brush to remove any loose soil and grit (remove any woody stems if present).

Wash and drain.

Water, Bottled Visually examine bottles for leakage.

Table 5. Sample Preparation Steps for Analysis. This table lists the steps for preparing each collected commodity 

for analysis as defined in the Laboratory Standard Operating Procedure. The wash and drain steps refer to a wash 

under cold running water for approximately 15-20 seconds to assure that all surfaces are rinsed, then a drain for 

at least 2 minutes. For all commodities, the sample is chopped, mixed, or blended until a visually homogeneous 

mixture is attained.
Pesticide Data Program—Annual Summary, Calendar Year 2017

15

 3 “ISO” is not an acronym because the initials would be different in various official languages. “ISO” is adopted from the 

Greek word “isos” meaning equal.

phase extraction method developed by the Montana 

Department of Agriculture and analyses were 

performed using GC-MS/MS and LC-MS/MS.

♦ Quality Assurance Program

The primary objectives of the QA/QC program 

are to ensure the reliability of PDP data and the 

performance equivalency of the participating 

laboratories. Direction for the PDP QA program 

is provided through SOPs based on EPA Good 

Laboratory Practices, along with program-specific 

QA/QC requirements. The PDP SOPs provide 

uniform administrative and sampling procedures, 

as well as guidelines for laboratory operations 

and data analyses. The SOPs are revised annually 

to accommodate changes in the program and 

are aligned with International Organization for 

Standardization (ISO)3 requirements. PDP 

laboratories are accredited to ISO 17025 by the 

American Association for Laboratory Accreditation 

(A2LA), an internationally recognized accrediting 

body.

A Technical Advisory Group, comprised of 

laboratory Technical Program Managers and 

Quality Assurance Officers, is responsible for 

annually reviewing program SOPs and addressing 

QA issues. For day-to-day QA oversight, PDP 

relies on the Quality Assurance Unit (QAU) at 

each participating facility. The QAU operates 

independently from the laboratory staff and is 

responsible for reviewing all data generated for 

PDP and for performing quarterly, internal program 

audits. Preliminary data review procedures are 

performed onsite by each laboratory’s QAU. MPD 

staff conduct a final review of data for conformance 

with SOPs.

Method Performance Requirements: Laboratories 

are required to determine and verify the limits of 

detection (LODs) and limits of quantitation (LOQs) 

for each pesticide/commodity pair. LODs depend 

on matrix, analyte, and methods used (extraction 

and instrumental). LODs for each pesticide/

commodity pair are shown in the applicable crop 

results appendix. Additional method performance/

validation requirements include modules for 

consistent instrument response (linearity), method 

range, and precision and accuracy.

Identification/Confirmation: Identification/confirmation is performed using MS technologies. 

Residue amounts greater than or equal to LOD 

and below LOQ are reported as below quantifiable 

level (BQL). BQLs are assigned values at one-half 

the LOQ and are used along with values greater 

than or equal to LOQ and non-detects in dietary 

risk assessments when appropriate.

Routine Quality Control Procedures: PDP 

procedures for QC are used to assess method and 

analyst performance during sample preparation, 

extraction, and cleanup. To maximize sample 

output and decrease the QC/sample ratio, samples 

are analyzed in analytical sets that include the test 

samples and the following components:

• Reagent Blank - For analysis of fruit and 

vegetables, honey, and milk, an amount of distilled 

water, equivalent to the natural moisture content of 

the commodity, is run through the entire analytical 

process to confirm glassware cleanliness and 

system integrity. For bottled water reagent blanks, 

the amount of distilled water was equal to sample 

volume. 

• Matrix Blank - A previously analyzed sample 

of the same commodity, which contains either 

very low concentrations of known residues or no 

detectable residues, is divided into two portions. 

The first portion is used to determine background 

information on naturally occurring chemicals and 

the second to prepare a matrix spike.

• Matrix Spike(s) - Prior to extraction, a portion of 

the matrix blank is spiked with marker pesticides to 

determine the precision and accuracy of the analyst 

and instrument performance. Marker pesticides 

are compounds selected from different pesticide 

classes (e.g., organochlorines, organophosphates, 

carbamates, conazoles, imidazolinones, macrocyclic lactones, neonicotinyls, phenoxy acid 

herbicides, pyrethroids, strobilurins, sulfonyl urea 

herbicides, triazines, uracils), with physical and 

chemical characteristics representative of their 
Pesticide Data Program—Annual Summary, Calendar Year 2017

16

corresponding pesticide class. Marker pesticides 

may be used to monitor recovery instead of spiking 

all pesticides. This use of marker pesticides 

optimizes the resources required to analyze the 

thousands of analyte/matrix combinations in the 

program while still allowing evaluation of daily 

recovery patterns. 

In addition, each laboratory must perform matrix 

spikes at least quarterly for each analyte/crop 

combination it reports. Some laboratories choose 

to rotate spikes of all compounds on a set-toset basis or spike all compounds analyzed with 

each set, so that the amount of spike recovery 

data obtained actually exceeds the minimal 

requirements previously stated. During 2017, PDP 

laboratories quantitated a total of 78,179 matrix 

spikes, with an overall mean recovery of 96.4 

percent and an overall 23 percent coefficient of 

variation (% C.V.). The % C.V. is calculated as the 

standard deviation divided by the mean.

• Process Control Spike - A compound with 

physical and chemical characteristics similar 

to those of the pesticides being tested is used 

to evaluate the analytical process on a sampleby-sample basis. Each of the analytical set 

components, except the reagent and matrix blanks, 

is spiked with process controls. During 2017, PDP 

laboratories quantitated a total of 25,880 process 

controls on 10,541 samples, with an overall 

mean recovery of 100 percent and an overall 19 

percent C.V. Of these process controls, 83 (0.32 

percent) were reruns due to initial failure to meet 

PDP recovery criteria. The rerun values are not 

included in these statistics.

Proficiency Testing: All facilities are required 

to participate in PDP’s Proficiency Testing 

(PT) program. In order to properly benchmark 

performance, PDP laboratories participate in 

the international Food Analysis Performance 

Assessment Scheme (FAPAS), administered by 

the Food and Environment Research Agency, 

Sand Hutton, York, United Kingdom. In 2017, 

PDP laboratories that routinely analyze fruit and 

vegetable samples via MRMs participated in one 

FAPAS round for apple purée that contained 10 

fortified analytes. Laboratories were evaluated 

based on z-scores for reported compounds, as well 

as any reported false negatives or false positives. 

PDP laboratories typically obtained z-scores 

less than two, which is deemed satisfactory 

performance.

In addition, PDP laboratories participate in an 

internal PT program that is tailored to current 

PDP commodities and testing profiles. For this 

internal program, the California Department of 

Food and Agriculture QAU prepares and issues 

rounds designed by MPD. Spiking compounds 

are selected with specificity and levels for each 

commodity. Fortification levels of selected 

analytes are generally 1 to 10 times the program 

LOQ for that commodity/compound pair. For 

each multiresidue round, one compound per set 

is typically repeated within the round to provide 

an indicator of repeatability. The resulting data 

are used to determine performance equivalency 

among the testing laboratories and to evaluate 

individual laboratory performance. 

During 2017, PDP laboratories received two 

multi-residue fruit and vegetable PT rounds 

(nectarines and cabbage), each consisting of 

three test samples. The nectarine samples were 

fortified with a total of 10 different compounds 

with trifluralin spiked on 2 different samples. The 

cabbage samples were fortified with a total of 12 

different compounds with carbofuran spiked on 

2 different samples at the same level to evaluate 

within and between laboratory variability. 

Onsite Reviews: In addition to the onsite 

assessments performed by A2LA that are required 

to maintain ISO 17025 accreditation, MPD staff 

chemists perform onsite reviews of laboratory 

operations to determine compliance with PDP 

SOPs and provide a report of findings identifying 

potential areas of improvement. Improvements 

in sampling, chain-of-custody, laboratory, 

recordkeeping, and electronic data transmission 

procedures are made as a result of onsite reviews.

IV. Database Management

PDP maintains an electronic database that serves 

as a central data repository. The data captured 

and stored in the PDP database include sample 

collection and product information, residue 

findings, and process control recoveries for each 
Pesticide Data Program—Annual Summary, Calendar Year 2017

17

sample analyzed, in addition to QA/QC fortified 

recoveries for each set of samples. Each calendaryear survey is stored in a separate database 

structure, which allows easier administration and 

data reporting. The PDP data pathway is illustrated 

in Figure 5.

♦ Electronic Data Path

 

PDP utilizes the Remote Data Entry (RDE) system, 

which is a customized software application that 

allows participating State and Federal laboratories 

to enter and transmit data electronically. The 

RDE system is centralized with all user interface 

software and database files residing on USDA 

servers. The laboratory users need only a Web 

browser to interface with the RDE system. Access 

is controlled through separate user login/password 

accounts and user access rights for the various 

system functions based on position requirements. 

The RDE system utilizes Secure Sockets Layer 

technology to encrypt all data passed between 

users’ computers and the central Web server. 

A separate Windows®-based system allows sample 

collectors to capture the standardized Sample 

Information Form (SIF) electronically on laptop 

or tablet computers. The e-SIF system generates 

formatted text files containing sample information 

that are e-mailed to MPD staff for import into the 

Web-based RDE system.

The RDE data entry screens have extensive editing 

functions and cross-checks built into the software 

to ensure valid values are entered for all critical 

data elements. This task is made easier by the 

practice of capturing and storing standardized 

codes for all critical alphanumeric data elements 

rather than their complete names, meanings, or 

descriptions. This coding scheme allows for faster 

and more accurate data entry, saves disk storage 

space, and allows the user to perform ad-hoc 

queries (data searches) on the database easily. The 

data entry screens also perform automatic edits on 

numeric fields, dates, and other character fields to 

ensure entries are within prescribed boundaries. 

MPD staff chemists review the data online and then 

mark the data as ready-for-upload to the central 

PDP database. A separate upload application 

converts and passes the data to the PDP database, 

which is maintained using Microsoft® Access and 

SQL Server database tools. Access to the central 

PDP database is limited to MPD personnel and is 

controlled through password protection and user 

access rights.

♦ Data Reporting 

The MPD staff frequently receives requests for 

data from government agencies and interested 

outside parties. Ad-hoc queries and custom reports 

are generated to fill such requests. An electronic 

library of data queries is maintained to generate 

standardized data summaries, including the data 

tables, charts, and appendixes in this annual 

summary. Subsets of the PDP calendar-year 

databases are made available for download from 

the PDP website. The data files on the website 

are delimited text files that contain a portion of 

the sampling data, all reported residue findings, 

and reference lists that can be used to interpret 

the standardized codes used in the PDP data. The 

data files can be imported into defined database 

structures and manipulated using common 

database management software packages.

♦ Online Database Search Tool 

An online PDP Database search tool is available 

for public use. The search tool allows anyone 

with internet access to search for PDP pesticide 

residue findings on commodities tested across 

all published years. Search criteria are selected 

from lists of all reported commodities, pesticides, 

and survey years. One of five output preferences 

is selected to show individual residue findings 

or summary data. The generated dataset can be 

exported to a comma-separated values (CSV) file. 

The search tool can be reached from any PDP 

website page or directly at https://apps.ams.usda.

gov/pdp.

V. Sample Results and Discussion

♦ Overview

In 2017, PDP conducted surveys on a variety 

of foods including fresh and processed fruit and 

vegetables, honey, milk, and bottled water. Of 

the 10,541 samples analyzed, 8,759 were fresh 

and processed fruit and vegetable samples, 315 
Pesticide Data Program—Annual Summary, Calendar Year 2017

18

- Collection in 10 States

- Samples taken close to consumer consumption

- Standardized sample information forms

- Data entry on tablet/laptop computers

- Chemists review data on-screen

- Upload data to central database

- 7 State laboratories, 1 Federal laboratory

- Fruit and vegetable samples prepared for

 consumption

- Detect residues at low levels

- Pesticide residue data generated

- Multi-tiered quality assurance data review

 process

- Web-based data entry software

- Import data from other systems

- Access controlled by user login

- Extensive data cross-checks

- Data reconciliation

- Standard & ad hoc reporting

- Annual Summary

- Data available online

YEAR-END REVIEW

INTERNET

SAMPLE COLLECTION DATA REVIEW AT HQ

LABORATORY ANALYSIS

LABORATORY REMOTE DATA 

ENTRY (RDE)

DATA REPORTING

Figure 5. Pesticide Data Program (PDP) Data Pathway. An illustration of PDP data path from sample 

collection through laboratory analysis and reporting.

INTERNET
Pesticide Data Program—Annual Summary, Calendar Year 2017

19

were honey, 711 were milk samples and 756 were 

bottled water, respectively. PDP testing methods 

are designed to detect the lowest possible levels 

of pesticide residues. In 2017, over 99 percent 

of the samples tested had residues well below the 

tolerances established by the EPA with 53.0 percent 

having no detectable pesticide residue. The data 

reported by PDP corroborate that residues found 

in agricultural products sampled are at levels that 

do not pose risk to consumers’ health and are safe 

according to EPA and FDA.

Appendix B tabulates the distribution of residue 

results for fruit and vegetables. Information 

included in this appendix are: number of samples 

analyzed for each compound, number and percent 

of samples with detections, range of concentrations 

detected, range of analytical LODs, and EPA 

tolerance levels. Appendixes C, D and E provides 

the distribution of residues for honey, milk, and 

bottled water, respectively. 

PDP laboratories tested foods for low levels 

of environmental contaminants that are no 

longer used in the United States, but due to their 

persistence in the environment, particularly in 

soil, these contaminants can be taken up by plants. 

Appendix F tabulates the results for environmental 

contaminants across all commodities. 

Environmental contaminants are consolidated 

into a single appendix because they have no 

registered uses and are not applied to crops in the 

United States. These compounds are subject to 

FDA Action Levels (ALs), rather than tolerances. 

Because environmental contaminants continue to 

persist in the environment, they may be present in 

food commodities at generally low levels. 

Most of the collected and analyzed samples (72.4 

percent) were produced in the United States, 26.0 

percent were imports, 1.1 percent were of mixed 

national origin, and 0.5 percent were of unknown 

origin. Appendix G shows the distribution of 

sample origin by State or country. Of all samples 

collected and analyzed, approximately 23.6 

percent (2,490 of 10,541) were grown, packed, 

and/or distributed in or from California. Appendix 

H includes a comparison of residues for a select 

commodity with a significant import component.

Food monitoring data, together with dietary 

consumption surveys, are used by EPA to estimate 

dietary exposure to pesticides to ensure the safety 

of existing pesticide uses. EPA uses all results 

reported by PDP, including sample results reported 

as below the LOD and those above the tolerance. 

PDP laboratories are required to establish LODs 

and report any instrumental response below 

the LOD as a non-detect. LODs are established 

experimentally for each pesticide/commodity pair 

and are reported with each data set. The number of 

non-detects can be used in conjunction with percentcrop-treated data to determine what proportion of 

these values may be counted as zero towards the 

dietary exposure. All individual sample data can 

be downloaded from the PDP website at http://

www.ams.usda.gov/pdp or obtained by contacting 

MPD.

♦ Import Versus Domestic Residue Comparisons 

Information about the origin of each PDP sample 

is recorded when the sample is collected. Figure 

3 illustrates the portion of the domestic and import 

component for each of the PDP fruit and vegetable 

commodities in 2017. The data generated by 

PDP reflect pesticide residues in foods, both 

domestic and imported products, available to 

the U.S. consumer. Many fresh and processed 

commodities are almost entirely of domestic 

origin, such as grapefruit (95.2 percent); lettuce 

(97.9 percent); sweet potatoes (99.9 percent); and 

canned tomatoes (95.0 percent) with only minor 

import (4.0 percent, 1.3 percent, 0.1 percent, and 

3.9 percent, respectively) and unknown origins 

(0.8 percent, 0.8 percent, 0 percent, and 1.1 

percent, respectively). Other fresh commodities, 

such as snap peas, are available from domestic 

growers part of the year and imported during the 

remaining months, as illustrated in Figure 4.

Comparison of selected residues detected in 

imported versus domestic snap peas can be found 

in Appendix H. These sample sets were selected to 

compare data where residues are present in greater 

than 5 percent of the commodity samples and 

allow for the comparison of individual residues. 

These data also show that the residue profiles for 

domestic and imported crops are significantly 

different. 
Pesticide Data Program—Annual Summary, Calendar Year 2017

20

percent of the samples tested had residues below 

the tolerances established by the EPA, while 53 

percent of the samples tested had no detectable 

pesticide residue. This is critical information for 

consumers wanting to understand the relationship 

of on-farm pesticide use to human health concerns, 

and whether food sold at the market place is safe 

to consume. Pesticide use is primarily dictated by 

local pest pressures and environmental conditions 

conducive to growth of pest populations, as well 

as the planting of susceptible varieties. These 

differences are captured by PDP data, which reflect 

actual residues present in food grown in various 

regions of the United States and overseas. Thus, 

in evaluating consumer exposure to pesticides 

through the diet, EPA uses all available information 

provided by registrants, PDP, and others to verify 

that tolerances meet the safety standards set by 

FQPA. The reporting of residues present at levels 

below the established tolerance serves to ensure 

and verify the safety of the Nation’s food supply.

Food commodities with pesticides detected in 

at least 5 percent of samples tested are shown in 

Appendix I. The data shown include the range 

and mean of values detected and EPA tolerance 

references for each pair. 

By virtue of the MRMs employed, PDP provides 

critical data that can be used by EPA to evaluate 

exposure to multiple residues from the same 

commodity. The data are crucial for assessments 

that consider cumulative exposure to pesticides 

determined to have common mechanisms of 

toxicity. The distribution of multiple pesticides 

occurring in samples tested during 2017 is 

presented in Appendix J. These data indicate 

that 53.0 percent of all samples tested contained 

no detectable pesticides, 19.5 percent contained 

one pesticide, and 27.5 percent contained more 

than one pesticide. Parent compounds and their 

metabolites are combined to report the number of 

“pesticides” rather than the number of “residues.” 

Environmental contaminants, listed in Appendix F, 

have been excluded from this count of pesticides. 

Three samples of kale (2 from California and 1 

imported from Mexico) contained residues of 17 

pesticides. None of the residues found on the 

kale samples exceeded the established tolerances. 

The data in Appendix H illustrate that some 

residues were detected more frequently in imported 

samples, some were detected more frequently in 

domestic samples, and some were detected with 

relative equal frequency in domestic and imported 

samples. For example, the insecticide cyhalothrin 

(lambda) was detected in 39.0 percent of the snap 

pea samples from Guatemala, 2.0 percent from 

Mexico, and 12.2 percent of the U.S. samples. In 

contrast, the herbicide DCPA was detected in 22.6 

percent of the snap pea samples from the United 

States and 2.0 percent of the samples from Mexico. 

No DCPA was detected in Guatemalan samples. 

The insecticide cypermethrin was detected in 14.0 

percent of the snap pea samples from the United 

States, 17.9 percent of the samples from Mexico, 

and 10.2 percent of the Guatemalan samples 

showing nearly equal detection rates between 

domestic and imported samples.

All pesticides detected were registered in the 

United States; however, the profiles of residue 

findings were markedly different in the U.S. 

samples versus imported samples. The differences 

in residue detections between countries were 

likely due to the pesticides used in response to pest 

pressures based on differing environmental and 

climatic conditions as well as crop production and 

protection practices.

♦ Postharvest Applications

Pesticides can be applied before and after harvest 

depending on the crop and approved label use. 

PDP data capture both preharvest and postharvest 

uses because samples are collected at points 

when all pesticide applications have already 

occurred. Pesticides applied postharvest are 

used primarily as fungicides (e.g., azoxystrobin, 

imazalil, o-phenylphenol, and thiabendazole) 

and growth regulators/sprouting inhibitors 

(e.g., chlorpropham). Some detections reported 

in Appendix B most likely reflect postharvest 

applications to the raw agricultural commodity.

♦ Discussion of Results

There are many pesticides registered for use on the 

same crop; however, not all registered pesticides 

are used at the same time or location. Over 99 
Multiple residue detections can result from the 

application of more than one pesticide on a crop 

during a growing season; in addition, a number of 

other factors can contribute to multiple detections. 

For example, unintentional spray drift in the field, 

planting of crops in fields previously treated with the 

pesticide, and/or transfer of residues of postharvest 

fungicides or growth regulators applied to other 

commodities stored in the same storage facilities 

could all contribute to residue detections.

In most cases, samples analyzed by PDP are 

composites of 3 to 5 pounds of commodity from the 

same lot. Therefore, the estimated concentrations 

for multiple residue detections in these composite 

sample results may or may not reflect the number 

or levels of pesticides in a single-serving item of a 

commodity.

♦ Special Projects

Honey: USDA’s NSL laboratory conducted testing 

for pesticide residues on 315 honey samples. Six 

residues (including metabolites and isomers), 

representing six pesticides, were detected in honey 

(Appendix C). The most frequently detected residue 

was 2,4-dimethylphenyl formamide (2,4-DMPF), 

a metabolite of the pesticide amitraz, which was 

detected in 238 samples (75.6 percent). Thymol 

was detected in 43 samples (13.7 percent), alachlor 

in 3 samples (1 percent), carbendazim (MBC) in 

3 samples (1 percent), 2,6-dichlorobenzamide, 

a metabolite of the pesticide dichlobenil, in 2 

samples (0.6 percent), and coumaphos in 1 sample 

(0.3 percent). All residue detections were lower 

than the tolerances for the two pesticides that have 

established tolerances - 2,4-DMPF and coumaphos. 

Thymol is exempt from the requirement of a 

tolerance and the other three pesticides have no 

tolerance established.

Milk: The California laboratory conducted testing 

for pesticide residues on 711 milk samples. One 

residue representing one pesticide was detected in 

milk (Appendix D). Flubendiamide was detected 

in 12 samples (1.7 percent) of milk. The residue 

detections were much lower than the established 

tolerance. 

Bottled Water: The New York laboratory conducted 

testing on 756 bottled water samples. Appendix 

Pesticide Data Program—Annual Summary, Calendar Year 2017

21

E shows 10 residues representing 7 pesticides 

detected in bottled water. Alachlor ethanesulfonic 

acid (ESA) was detected in 49 samples (6.5 

percent); metolachlor ethanesulfonic acid 

(ESA) was detected in 29 samples (3.8 percent); 

desethyl atrazine was detected in 22 samples (2.9 

percent); and atrazine was detected in 5 samples 

(0.7 percent). Each of the following compounds 

were detected on 1 of the 756 samples, each 

representing 0.1 percent of the samples 

tested: acetochlor ethanesulfonic acid (ESA), 

desisopropyl atrazine, imidacloprid, metolachlor, 

simazine, and tebuthiuron. 

♦ Environmental Contaminants

Environmental contaminants include pesticides 

whose uses have been canceled in the United 

States, but their residues persist in the 

environment, particularly in soil, where they may 

be taken up by plants. These data are also used 

to facilitate international trade. Residue results 

for environmental contaminants may be found in 

Appendix F.

DDT, DDD, and DDE: PDP screened samples for 

various metabolites of DDT including: DDT o,p’; 

DDT p,p’; DDD o,p’; DDD p,p’; DDE o,p’; and 

DDE p,p’. Use of DDT has been prohibited in 

the United States since 1972; however, due to its 

persistence in the environment, low-level residues 

of DDT and its DDD and DDE metabolites were 

detected in some commodities tested. DDE p,p’ 

was detected in kale (39 percent), snap peas (1.5 

percent), milk (0.1 percent), and sweet potatoes 

(0.1 percent). DDT p,p’ was detected in kale 

(6.8 percent) and lettuce (0.3 percent). DDT 

o,p’ was detected in kale (9 percent). DDE o,p’ 

was detected in kale (0.1 percent). No residues 

of DDD o,p’ or DDD p,p’ were detected in any 

samples. All residues detected were lower than 

established FDA ALs.

Other Extraneous Pesticides: PDP screened 

samples for other environmental contaminants 

including: aldrin, which readily metabolizes 

to dieldrin; BHC (alpha/beta/delta); chlordane 

(total, cis, trans) and its metabolite oxychlordane; 

dieldrin; endrin; heptachlor and its epoxide 

metabolite (total, cis); hexachlorobenzene 

(HCB); lindane (BHC gamma); and mirex. HCB 
was used as a seed protectant until 1965 and, due 

to its persistence, remains in soil and grasses. In 

1974, all aldrin and dieldrin uses were canceled in 

the United States and, in 1978, all heptachlor and 

mirex uses were canceled. In 1986, chlordane uses, 

except termiticide uses, were canceled. Despite 

these cancellations and because they persist in the 

environment, trace residues of chlordane (cis and 

trans), dieldrin, and endrin were detected in some 

of the tested commodities.

Dieldrin was detected in 11 percent of kale and 

0.3 percent of cucumber samples. Chlordane (cis) 

was detected in 1.1 percent of kale samples, while 

chlordane (trans) was detected in 0.4 percent of kale 

samples and 0.2 percent of canned tomato samples. 

Endrin was detected in 0.3 percent of kale samples. 

All residues detected were lower than established 

FDA ALs. No residues of aldrin, BHC (alpha/beta/

delta), heptachlor (parent), heptachlor epoxide 

(total, cis), HCB, lindane (BHC gamma), mirex, or 

oxychlordane were detected in any samples.

♦ Tolerance Violations

A tolerance is defined under Section 408 of the 

Federal Food, Drug, and Cosmetic Act as the 

maximum quantity of a pesticide residue allowable 

on a raw agricultural commodity. Tolerances are 

also applicable to processed foods. The FQPA of 

1996 amended the Federal Insecticide, Fungicide 

and Rodenticide Act to require EPA to periodically 

review each pesticide registration using the most 

currently available data. Timely pesticide data 

provided by PDP enable the EPA to refine risk 

estimates used in the pesticide reregistration 

process. 

A tolerance violation occurs when a residue is 

found that exceeds the tolerance level or when 

a certain residue is found for which there is no 

established tolerance. With the exception of meat, 

poultry, and egg products, for which USDA’s 

Food Safety and Inspection Service is responsible, 

FDA enforces tolerances for all imported foods 

and domestic foods that move through interstate 

commerce. Unlike enforcement programs, PDP 

emphasizes determination of residues at the 

lowest detectable levels rather than quick turnaround times. When PDP identifies samples with 

residues exceeding the tolerance or with residues 

for which there is no established tolerance, these 

detections are reported to FDA’s headquarters 

office. This notification is made in accordance with 

a Memorandum of Understanding between USDA 

and FDA for the purpose of identifying areas where 

closer surveillance may be needed. FDA assesses 

PDP apparent violation data for appropriateness for 

follow up under its regulatory pesticide program. 

Due to the time period required for completion 

of PDP analyses and data reporting, FDA follow 

up will usually be at a subsequent harvest or 

commodity availability period. 

Residues exceeding the established tolerance or 

Action Level are noted with an “X” in Appendixes 

B and C. Similarly, residues for which a tolerance 

is not established are noted with a “V” in Appendix 

B. The “X” and “V” annotations are followed by a 

number indicating the number of samples reported 

to FDA. The EPA tolerances cited in this summary 

and appendixes apply to 2017 and not to the current 

year. There may be instances where tolerances 

may have been recently changed that would have 

an effect on whether a residue is violative.

An established tolerance may apply to more than 

one residue because pesticides may break down into 

more than one metabolite or contain more than one 

isomer. For example, the tolerance for endosulfan 

combines residues of endosulfan I, endosulfan 

II, and endosulfan sulfate; and organophosphate 

tolerances may combine the parent compound and 

the sulfone and sulfoxide metabolites. Therefore, 

where applicable, the pesticide violations in 

Appendix K are combined residues of parent and 

any isomers and/or metabolites to count the total 

number of samples with tolerance violations.

A total of 368 samples with 431 pesticides were 

reported to FDA as Presumptive Tolerance 

Violations. Pesticides exceeding the tolerance were 

detected in 0.59 percent (58 samples) of the total 

samples tested (9,785 samples), excluding bottled 

water. Of these 58 samples, 24 were domestic 

(41.4 percent), 32 were imported (55.2 percent), 

and 2 were of unknown origin (3.4 percent). 

The samples containing pesticides that exceeded 

established tolerances included: 5 samples of 

asparagus, 1 sample of fresh cranberries, 9 samples 

Pesticide Data Program—Annual Summary, Calendar Year 2017

22
of cucumbers, 24 samples of kale, 2 samples of 

onions, 16 snap pea samples, and 1 sample of sweet 

potatoes.

Residues with no established tolerance were found 

in 3.3 percent (320 samples) of the total samples 

tested (9,785 samples), excluding bottled water. 

Of these 320 samples, 150 were domestic (46.9 

percent) and 170 were imported (53.1 percent). 

These samples included 239 fresh fruit and 

vegetable samples, 73 processed fruit/vegetable 

samples, and 8 honey samples. The 73 processed 

fruit/vegetable samples were canned garbanzo 

beans, canned olives, canned pineapples, and 

dried plums/prunes. There were 270 samples that 

contained 1 pesticide for which no tolerance was 

established, 48 samples with 2 pesticides for which 

no tolerance was established, and 2 samples that 

contained 3 pesticides for which no tolerance was 

established. Ten of the 320 samples also contained 

1 pesticide each that exceeded an established 

tolerance. In most cases, these pesticides with 

no established tolerance were detected at very 

low levels. Some pesticide residues may have 

resulted from unintentional spray drift in the field, 

planting of crops in fields previously treated with 

the pesticide, or transfer of pesticide residues 

of postharvest fungicides or growth regulators 

applied to other commodities stored in the same 

storage facilities. The pesticide residue levels and 

commodities are listed in Appendix K.

Pesticide Data Program—Annual Summary, Calendar Year 2017

23

♦♦♦♦♦♦
Appendix A

Commodity History

Appendix A identifies commodities sampled by the Pesticide Data Program (PDP) through 

December 2018. Updates to this list are posted on the PDP Web site at www.ams.usda.gov/

pdp. 
Fresh Commodities

Commodity Start Date End Date

Apples 1 Sep-91 Dec-96

Apples (S-1) Jan-99 Dec-99

Apples (S-2) Jan-99 May-99

Apples Oct-00 Sep-02

Apples (T-1) Jan-03 Dec-03

Apples Jan-04 Dec-05

Apples Jan-09 Dec-10

Apples (B-1) Aug-12 Oct-12

Apples Oct-14 Sep-16

Asparagus Jan-02 Jun-03

Asparagus Jul-08 Jun-10

Asparagus Jul-17 Ongoing

Avocados Jul-12 Dec-12

Bananas Sep-91 Sep-95

Bananas Jan-01 Dec-02

Bananas (TSP) Jul-03 Dec-03

Bananas Jan-06 Dec-07

Bananas Apr-12 Mar-14

Basil Oct-18 Ongoing

Blueberries (cultivated) 2 Jan-07 Dec-08

Blueberries (cultivated) 2 Jan-14 Dec-14

Broccoli Oct-92 Dec-94

Broccoli Jan-01 Dec-02

Broccoli Oct-06 Sep-08

Broccoli Jan-13 Dec-14

Cabbage Jan-10 Dec-11

Cabbage Jul-17 Ongoing

Cantaloupe Jul-98 Jun-00

Cantaloupe Oct-03 Sep-05

Cantaloupe Jan-10 Mar-10

Cantaloupe Oct-10 Jun-12

Carrots 1 Oct-92 Sep-96

Carrots Oct-00 Sep-02

Carrots Jan-06 Dec-07

Carrots Jan-13 Dec-14

Cauliflower Oct-04 Sep-06

Cauliflower Oct-11 Sep-13

Celery Feb-92 Mar-94

Celery Jan-01 Dec-02

Celery Jan-07 Dec-08

Celery Jan-13 Dec-14

Cherries 3 May-00 Aug-01

APPENDIX A. COMMODITY HISTORY

AS OF DECEMBER 2018

Appendix A. Page 1 of 9
Commodity Start Date End Date

Cherries 2 May-07 Sep-07

Cherries Apr-14 Mar-16

Cilantro Oct-09 Sep-10

Cranberries Oct-06 Dec-06

Cranberries 2 Oct-16 Mar-18

Cucumbers Jan-99 Dec-00

Cucumbers Oct-02 Sep-04

Cucumbers Jan-09 Dec-10

Cucumbers Jul-15 Jun-17

Eggplant Jan-05 Dec-06

Grapefruit Aug-91 Dec-93

Grapefruit Jan-05 Dec-06

Grapefruit Oct-15 Sep-17

Grapes 1 May-91 Dec-96

Grapes Jan-00 Dec-01

Grapes (TSP) Jul-03 Dec-03

Grapes Jan-04 Dec-05

Grapes Jan-09 Dec-10

Grapes Jan-15 Dec-16

Green Beans Feb-92 Dec-95

Green Beans Jan-00 Dec-01

Green Beans Apr-04 Mar-05

Green Beans Jan-07 Dec-08

Green Beans Jul-13 Sep-16

Green Onions Oct-08 Sep-09

Green Onions Jan-18 Dec-18

Greens (collard & kale) Oct-06 Sep-08

Hot Peppers Oct-10 Sep-11

Kale Jan-17 Dec-18

Kiwi Apr-18 Ongoing

Lettuce May-91 Dec-94

Lettuce Oct-99 Sep-01

Lettuce Jan-04 Dec-05

Lettuce Jan-10 Dec-11

Lettuce Jul-15 Jun-17

Lettuce, Organic Jan-09 Dec-09

Mangoes Apr-10 Sep-10

Mangoes Oct-17 Sep-18

Mushrooms Oct-01 Sep-03

Mushrooms Oct-11 Sep-13

Nectarines 4 Jul-00 Sep-01

Nectarines Jan-07 Dec-08

Nectarines Jan-13 Dec-15

Onions Jan-02 Dec-03

Onions Oct-11 Sep-12

Onions Jan-17 Dec-17

Oranges 1 Aug-91 Dec-96

Appendix A. Page 2 of 9
Commodity Start Date End Date

Oranges Jan-00 Dec-01

Oranges Jan-04 Dec-05

Oranges Jan-09 Dec-10

Oranges Jan-15 Dec-16

Papaya Jul-11 Jun-12

Peaches Feb-92 Sep-96

Peaches (S-3) Jan-00 Sep-00

Peaches 5 Jan-01 Sep-02

Peaches (T-1) May-03 Sep-03

Peaches Oct-06 Sep-08

Peaches (B-1) Aug-12 Oct-12

Peaches Jul-13 Jun-15

Pears Jan-97 Jun-99

Pears (S-1) Jul-98 Jun-99

Pears Oct-03 Sep-05

Pears Jan-09 Dec-10

Pears Jan-15 Dec-16

Pears (B-1) Oct-12 Nov-12

Pineapples Jul-00 Jun-02

Plums 6 Jan-05 Dec-06

Plums Oct-11 Sep-13

Potatoes May-91 Dec-95

Potatoes (S-4) Dec-96 Dec-97

Potatoes Jul-00 Jun-02

Potatoes Jan-08 Dec-09

Potatoes Jan-15 Dec-16

Raspberries 2 Jan-13 Dec-13

Snap Peas Jan-11 Dec-12

Snap Peas Jan-17 Dec-18

Spinach 1 Jan-95 Sep-97

Spinach Jul-02 Dec-03

Spinach 7 Jan-06 Sep-06

Spinach Jan-08 Dec-09

Spinach Jan-15 Dec-16

Strawberries 2 Jan-98 Sep-00

Strawberries Jan-04 Dec-05

Strawberries Jan-08 Dec-09

Strawberries Oct-14 Sep-16

Summer Squash Oct-06 Sep-08

Summer Squash Oct-12 Sep-14

Sweet Corn (on-the-cob) Oct-08 Sep-10

Sweet Corn (on-the-cob) Oct-14 Sep-15

Sweet Bell Peppers Jan-99 Dec-00

Sweet Bell Peppers Oct-02 Sep-04

Sweet Bell Peppers Jan-10 Mar-12

Sweet Potatoes 1 Jan-96 Jun-98

Sweet Potatoes Jan-03 Dec-04

Appendix A. Page 3 of 9
Commodity Start Date End Date

Sweet Potatoes Oct-08 Sep-10

Sweet Potatoes Apr-16 Mar-18

Tangerines Jan-11 Dec-12

Tomatoes 1 Jul-96 Jun-99

Tomatoes Jan-03 Dec-04

Tomatoes Jan-07 Dec-08

Tomatoes Oct-14 Sep-16

Tomatoes, Cherry/Grape Jan-11 Dec-12

Watermelon 8 Oct-05 Sep-06

Watermelon Apr-10 Sep-10

Watermelon Jul-14 Jun-15

Winter Squash 2 Jan-97 Jun-99

Winter Squash Jul-04 Jun-06

Winter Squash Oct-11 Mar-13

NOTES

1

 Excludes sampling hiatus September - November 1996.

2

 Frozen collected when fresh unavailable.

3

 Sampling adjusted for market availability. Cherries were sampled for 2 years 

 (May-00 - Aug-01) for a total of 6 months.

4

 Sampling adjusted for market availability. Nectarines were sampled for 2 years 

 (Jul-00 - Sep-01) for a total of 6 months.

5

 Sampling adjusted for market availability. Peaches were sampled for 2 years

 (Jan-01 - Sep-02) for a total of 16 months.

6

 Dried plums (prunes) were collected when fresh plums were not available.

7

 Spinach ended earlier than planned due to the unavailability of product.

8

 Samples collected in California, Florida, and Texas only.

(B-1) Special project testing for bifenthrin in multi-residue screen.

(S-1) Special single serving project testing for organophosphates.

(S-2) Special single serving project testing for carbamates.

(S-3) Special single serving project testing for carbamate, organochlorine, 

 organophosphate, organonitrogen, and sulfur compounds.

(S-4) Special single serving project testing for aldicarb.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 4 of 9
Processed Commodities

Commodity Start Date End Date

Apple Juice 1 Jul-96 Dec-98

Apple Juice Jan-02 Dec-02

Apple Juice Jul-07 Jun-08

Apple Juice Jul-12 Jun-13

Applesauce Jul-02 Dec-02

Applesauce Jan-06 Dec-06

Applesauce Oct-16 Sep-17

Asparagus, Canned Jul-03 Dec-03

Beans, Canned (4 varieties) 2 Oct-08 Sep-10

Beets, Canned Jan-11 Dec-11

Blueberries (cultivated), Frozen 3 Jan-07 Dec-08

Blueberries (cultivated/wild), Frozen 3 Jan-14 Dec-14

Cherries, Frozen 4 Apr-14 Mar-16

Corn Syrup 4 Jan-98 Jun-99

Cranberries, Canned Apr-18 Sep-18

Cranberries, Frozen 3 Oct-16 Mar-18

Garbanzo Beans, Canned Oct-17 Sep-18

Grape Juice Jan-98 Dec-99

Grape Juice Jan-08 Dec-08

Grape Juice Oct-13 Sep-14

Green Beans, Canned/Frozen 1 Jan-96 Jun-98

Green Beans, Canned Jan-03 Mar-04

Green Beans, Frozen Apr-05 Dec-05

Green Beans, Canned/Frozen Jan-14 Dec-14

Olives, Canned Oct-16 Sep-18

Orange Juice Jan-97 Dec-98

Orange Juice Oct-04 Sep-06

Orange Juice Oct-10 Sep-11

Orange Juice Jan-12 Jun-12

Peaches, Canned Dec-96 Dec-97

Peaches, Canned Jan-03 Dec-04

Peaches, Canned Jan-18 Dec-18

Peaches, Canned (T-1) Jan-03 Mar-03

Peaches, Canned (T-1) Oct-03 Dec-03

Pear Juice, Concentrate/Puree Jul-02 Jun-03

Pears, Canned Jul-99 Jun-00

Peas, Canned/Frozen Apr-94 Jun-96

Peas, Canned/Frozen 5 Oct-01 Sep-03

Peas, Canned/Frozen Oct-18 Ongoing

Peas, Frozen Jan-06 Dec-06

Pineapple, Canned Jan-17 Dec-17

Plums, Dried (Prunes) 6 Jan-05 Dec-06

Plums, Dried (Prunes) Oct-17 Sep-18

Potatoes, Frozen Jan-06 Dec-07

Appendix A. Page 5 of 9
Commodity Start Date End Date

Raisins Jul-06 Jun-07

Raisins Jan-18 Dec-18

Raspberries, Frozen 3 Jan-13 Dec-13

Spinach, Canned Oct-97 Dec-98

Spinach, Canned Jan-04 Jun-04

Spinach, Canned/Frozen Jul-10 Jun-11

Spinach, Canned/Frozen Oct-18 Ongoing

Spinach, Frozen Jan-99 Dec-99

Strawberries, Frozen 3 Jan-98 Sep-00

Strawberries, Frozen Oct-18 Ongoing

Sweet Corn, Canned/Frozen Apr-94 Mar-96

Sweet Corn, Canned/Frozen 5 Oct-01 Sep-03

Sweet Corn, Frozen 3 Oct-08 Sep-10

Sweet Corn, Frozen 3 Oct-14 Sep-15

Tomato Paste, Canned Jan-01 Jun-01

Tomato Paste, Canned Jan-09 Dec-09

Tomatoes, Canned Jul-99 Jun-00

Tomatoes, Canned Oct-16 Sep-17

Winter Squash, Frozen 3 Jan-97 Jun-99

Baby Food / Formula Products

Commodity Start Date End Date

Baby Food, Applesauce Jul-12 Jun-13

Baby Food, Carrots Jan-12 Dec-12

Baby Food, Green Beans Oct-10 Sep-11

Baby Food, Peaches Jan-12 Dec-12

Baby Food, Pears Oct-10 Sep-11

Baby Food, Peas Jul-12 Jun-13

Baby Food, Sweet Potatoes Oct-10 Sep-11

Infant Formula, Dairy-Based Oct-13 Sep-14

Infant Formula, Soy-Based Oct-13 Sep-14

NOTES

1 Excludes sampling hiatus September - November 1996.

2 Bean varieties included black, garbanzo, kidney, and pinto.

3 Frozen collected when fresh unavailable.

4 Excludes sampling hiatus January 1999.

5 Canned samples collected in first year and frozen samples in second year of testing.

6 Dried plums (prunes) were collected when fresh plums were not available.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 6 of 9
Grains

Commodity Start Date End Date

Barley Oct-01 Sep-03

Corn Oct-06 Sep-08

Oats Jul-99 Apr-00

Oats Jan-10 Jun-10

Oats Apr-14 Aug-14

Rice Oct-00 Sep-02

Rice1 Oct-08 Sep-09

Rice Apr-14 Aug-14

Rice Oct-18 Ongoing

Soybeans Sep-96 Feb-98

Soybeans Oct-03 Sep-05

Soybeans Sep-10 Apr-11

Soybeans (S-1) Oct-05 Dec-05

Wheat Feb-95 Jan-98

Wheat Sep-04 Jun-06

Wheat Jul-12 Sep-12

Wheat Flour Jan-03 Dec-04

Wheat Flour Jan-18 Dec-18

Wheat Flour (T-1) Jan-03 Dec-03

Nuts and Nut Products

Commodity Start Date End Date

Almonds Jul-07 Mar-08

Peanut Butter Jan-00 Dec-00

Peanut Butter (TSP) Jul-03 Dec-03

Peanut Butter Jan-06 Dec-06

Peanut Butter Apr-15 Aug-15

Dairy Products

Commodity Start Date End Date

Butter Jan-03 Dec-03

Butter Jan-12 Dec-13

Heavy Cream Jul-05 Dec-05

Heavy Cream Jan-07 Dec-07

Heavy Cream Jun-18 Aug-18

Milk 2 Jan-96 Oct-98

Milk (TSP) Jul-03 Dec-03

Milk Jan-04 Dec-05

Milk Jan-11 Dec-11

Milk Jan-16 Dec-17

Appendix A. Page 7 of 9
Fish Products

Commodity Type Start Date End Date

Fish 3 Catfish Apr-08 Jun-10

Fish Salmon Jul-13 Jun-14

Meat / Poultry / Pork Products

Commodity Type Start Date End Date

Poultry Young Chickens Apr-00 Mar-01

Poultry Young & Mature Chickens Jan-06 Dec-06

Beef Cows, Heifers, Steers Jun-01 Jul-02

Beef 4 Cows, Heifers, Steers Dec-08 May-09

Pork Gilt, Barrow Jan-05 Jun-05

Other Products

Commodity Start Date End Date

Eggs (TSP) Jul-03 Dec-03

Eggs Jul-10 Jun-11

Eggs Apr-16 Aug-16

Honey Oct-07 Sep-08

Honey Apr-17 Aug-17

Drinking Water

States Start Date End Date

Finished Water Only (27 sites)

California, Colorado, Kansas, New York, Texas Mar-01 Dec-03

Raw Intake and Finished Water (70 sites) Jan-04 Apr-13

Alabama, Arizona, California, Florida, Georgia, Illinois, Indiana, Iowa, Kansas,

Kentucky, Louisiana, Maryland, Michigan, Minnesota, Missouri, Montana, New Jersey, 

New York, North Carolina, North Dakota, Ohio, Oregon, Pennsylvania, South Carolina, 

Tennessee, Texas, Virginia, Washington State, and Washington, D.C.

Bottled Water 

10 Participating States Jan-05 Dec-06

10 Participating States Jan-17 Dec-17

Groundwater 

1,495 Private Wells in 45 States plus Washington, DC Jan-07 Feb-13

16 Municipal Water Facilities in 13 States Mar-10 Feb-13

Appendix A. Page 8 of 9
NOTES

1

 Includes sampling hiatus May-July 2009.

2

 Excludes sampling hiatus September - November 1996.

3 Excludes sampling hiatus April-June 2009.

4

 Survey ended 7 months early due to budgetary constraints.

(S-1) Special survey for fungicides used to combat soybean rust.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 9 of 9
Appendix B

Distribution of Residues by Pesticide

in Fruit and Vegetables

Appendix B shows residue detections for all fruit and vegetable pesticide/commodity pairs 

tested, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerances for each pair. The EPA tolerances 

cited in this summary and appendixes apply to 2017 and not to the current year. There 

may be instances where tolerances have been recently set, modified, or revoked that 

would have an effect on whether a residue is violative or not.

In 2017, the Pesticide Data Program (PDP) analyzed 8,759 fruit and vegetable samples, 

of which 5,305 were fresh products and 3,454 were processed products.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by the U.S. Food and Drug Administration (FDA). Under the Food Quality 

Protection Act, responsibility for establishing tolerances in lieu of ALs has been transferred 

to EPA. In the interim, ALs are used.

PDP reports tolerance violations to FDA as part of an interagency Memorandum of 

Understanding between the U.S. Department of Agriculture and FDA. Residues reported 

to FDA are shown in the “Pesticide/Commodity” column to the right of the commodity 

and are annotated as “X” (if the residue exceeded the established tolerance) or “V” (if the 

residue did not have a tolerance listed in the Code of Federal Regulations, Title 40, Part 

180). In both cases, these annotations are followed by a number indicating the number 

of samples reported to FDA. 

Results for environmental contaminants across all commodities, including fruit and 

vegetables, have been consolidated in a separate appendix because they have no 

registered uses and are not applied to crops (see Appendix F).
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

2,4-dimethylphenyl formamide (2,4-DMPF) (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.003 - 0.005 NT

Olives, Canned 693 0 0.005 ^ NT

TOTAL 1,054 0

2,6-DIPN (plant growth regulator) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 60 0 0.010 ^ NT

Olives, Canned 754 0 0.003 - 0.010 NT

TOTAL 1,085 0

Abamectin (insecticide)

Applesauce 570 0 0.050 ^ 0.02

Asparagus 354 0 0.050 ^ 0.01

Grapefruit 271 0 0.020 ^ 0.02

Kale 708 0 0.025 ^ 0.01

Mangoes 90 0 0.020 ^ 0.01

Olives, Canned 754 0 0.020 ^ 0.01

Plums, Dried / Prunes 191 0 0.050 ^ 0.025

Snap Peas 710 0 0.025 ^ 0.01

TOTAL 3,648 0

Acephate (insecticide)

Applesauce 570 0 0.003 ^ 0.02

Asparagus 354 0 0.003 ^ 0.02

Cabbage 354 0 0.050 ^ 0.02

Cranberries 311 0 0.015 ^ 0.5

Cranberries, Frozen 427 0 0.015 ^ 0.5

Cucumbers 355 0 0.050 ^ 0.02

Garbanzo Beans, Canned 189 0 0.015 ^ 0.02

Grapefruit 526 0 0.005 - 0.030 0.02

Kale 708 0 0.050 ^ 0.02

Lettuce 378 15 4 0.003 - 0.026 0.003 ^ 10/0.02 &

Mangoes 177 0 0.005 - 0.015 0.02

Olives, Canned 754 0 0.005 ^ 0.02

Onions 708 5 0.7 0.007 - 0.053 0.005 - 0.050 X-2 0.02

Pineapple, Canned 756 0 0.050 - 0.15 0.02

Plums, Dried / Prunes 159 0 0.003 ^ 0.02

Snap Peas 710 0 0.050 ^ 0.02

Sweet Potatoes 701 0 0.15 ^ 0.02

Tomatoes, Canned 566 0 0.005 ^ 0.02

TOTAL 8,703 20

Acetamiprid (insecticide) 

Applesauce 570 440 77.2 0.002 - 0.058 0.002 ^ 1.0

Asparagus 354 0 0.001 - 0.002 0.80

Cabbage 354 4 1.1 0.013 - 0.018 0.010 ^ 1.20

Cranberries 311 0 0.002 ^ 1.6

Cranberries, Frozen 428 0 0.002 ^ 1.6

Cucumbers 378 10 2.6 0.010 - 0.035 0.010 ^ 0.50

Garbanzo Beans, Canned 189 0 0.001 ^ 0.40

APPENDIX B. DISTRIBUTION OF RESIDUES BY PESTICIDE IN FRUIT AND VEGETABLES

Appendix B. Page 1 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 526 11 2.1 0.001 - 0.009 0.001 - 0.002 1.0

Kale 708 39 5.5 0.017 - 3.6 0.010 ^ 15

Lettuce 378 8 2.1 0.002 - 0.019 0.002 ^ 3.00

Mangoes 177 0 0.001 - 0.002 0.01

Olives, Canned 754 0 0.001 ^ 0.01

Onions 708 0 0.001 - 0.010 0.02

Pineapple, Canned 756 0 0.005 - 0.010 0.01

Plums, Dried / Prunes 191 0 0.002 ^ 0.40

Snap Peas 710 9 1.3 0.017 - 0.15 0.010 ^ 0.60

Sweet Potatoes 701 0 0.005 ^ 0.01

Tomatoes, Canned 566 1 0.2 0.002 ^ 0.001 ^ 0.20

TOTAL 8,759 522

Acetochlor (herbicide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cranberries 311 0 0.030 ^ NT

Cranberries, Frozen 428 0 0.030 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 ^ NT

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.030 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 360 0 0.003 ^ NT

Pineapple, Canned 359 0 0.050 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.050 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 5,864 0

Acibenzolar S methyl (plant activator) 

Applesauce 570 0 0.020 ^ 0.05

Asparagus 354 0 0.020 ^ NT

Cabbage 354 0 0.010 ^ 1.0

Cranberries 311 0 0.030 ^ 0.15

Cranberries, Frozen 428 0 0.030 ^ 0.15

Garbanzo Beans, Canned 189 0 0.012 ^ NT

Grapefruit 255 0 0.005 ^ 0.02

Kale 708 0 0.025 ^ 1.0

Lettuce 378 0 0.020 ^ 0.25

Mangoes 87 0 0.030 ^ NT

Onions 693 0 0.004 - 0.012 0.1

Pineapple, Canned 756 0 0.010 - 0.040 NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

Sweet Potatoes 701 0 0.040 ^ NT

Tomatoes, Canned 545 0 0.004 - 0.012 1.0

TOTAL 6,520 0

Acifluorfen (herbicide) 

Grapefruit 271 0 0.050 ^ NT

Olives, Canned 630 0 0.050 ^ NT

TOTAL 901 0

Aclonifen (herbicide) 

Appendix B. Page 2 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Alachlor (herbicide) 

Cranberries 311 0 0.020 ^ NT

Cranberries, Frozen 428 0 0.020 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.010 - 0.020 NT

Mangoes 177 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 360 0 0.002 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 3,311 0

Aldicarb (insecticide) 

Asparagus 205 0 0.030 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 497 0 0.001 - 0.005 0.3

Mangoes 177 0 0.002 - 0.005 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.010 - 0.020 NT

Plums, Dried / Prunes 127 0 0.030 ^ NT

Sweet Potatoes 701 0 0.020 ^ 0.1

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,151 0

Aldicarb sulfone (metabolite of Aldicarb)

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.010 ^ NT

Grapefruit 526 0 0.003 - 0.020 0.3

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.003 - 0.010 NT

Pineapple, Canned 756 0 0.010 - 0.025 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.025 ^ 0.1

Tomatoes, Canned 566 0 0.003 ^ NT

TOTAL 7,341 0

Aldicarb sulfoxide (metabolite of Aldicarb)

Applesauce 570 0 0.005 ^ NT

Appendix B. Page 3 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Asparagus 32 0 0.005 ^ NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.006 ^ NT

Grapefruit 271 0 0.003 ^ 0.3

Lettuce 378 0 0.005 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.002 - 0.010 NT

Pineapple, Canned 756 0 0.010 - 0.055 NT

Sweet Potatoes 701 0 0.055 ^ 0.1

Tomatoes, Canned 566 0 0.006 ^ NT

TOTAL 5,747 0

Allethrin (insecticide) 

Cabbage 354 0 0.020 ^ NT

Cucumbers 378 0 0.040 ^ NT

Grapefruit 526 0 0.010 - 0.050 NT

Mangoes 60 0 0.010 ^ NT

Olives, Canned 693 0 0.010 ^ NT

Onions 348 0 0.040 ^ NT

Pineapple, Canned 756 0 0.040 - 0.080 NT

Sweet Potatoes 701 0 0.080 ^ NT

TOTAL 3,816 0

Ametoctradin (fungicide) 

Cranberries 311 1 0.3 0.003 ^ 0.001 ^ V-1 NT

Cranberries, Frozen 428 0 0.001 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Kale 708 45 6.4 0.003 - 37 0.002 ^ 50

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ 1.5

Tomatoes, Canned 566 0 0.001 ^ 1.5

TOTAL 4,019 46

Ametryn (herbicide) 

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.001 - 0.010 0.05

TOTAL 4,032 0

Amicarbazone (herbicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Appendix B. Page 4 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Anilofos (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Aspon (insecticide) 

Cabbage 354 0 0.005 ^ NT

TOTAL 354 0

Asulam (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Atraton (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Atrazine (herbicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 1 0.3 0.53 ^ 0.002 ^ V-1 NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Lettuce 378 3 0.8 0.002 - 0.020 0.002 ^ 0.25

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.001 - 0.005 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 4

Azinphos (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Azinphos methyl (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.020 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.020 ^ NT

Garbanzo Beans, Canned 189 0 0.006 ^ NT

Grapefruit 526 0 0.005 - 0.020 NT

Kale 708 0 0.020 ^ NT

Appendix B. Page 5 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.006 - 0.020 NT

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Snap Peas 710 0 0.020 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.006 ^ NT

TOTAL 8,759 0

Azinphos methyl oxygen analog (metabolite of Azinphos methyl)

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cranberries 311 0 0.015 ^ NT

Cranberries, Frozen 428 0 0.015 ^ NT

Grapefruit 526 0 0.003 - 0.015 NT

Kale 708 0 0.020 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.003 - 0.015 NT

Olives, Canned 754 0 0.003 ^ NT

Pineapple, Canned 359 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Snap Peas 710 0 0.020 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 6,167 0

Azoxystrobin (fungicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.001 - 0.002 0.04

Cabbage 328 13 4 0.003 - 0.21 0.002 ^ 3.0

Cranberries 311 30 9.6 0.001 - 0.005 0.001 ^ 5.0

Cranberries, Frozen 428 6 1.4 0.001 - 0.004 0.001 ^ 5.0

Cucumbers 378 66 17.5 0.002 - 0.038 0.002 ^ 0.3

Garbanzo Beans, Canned 189 0 0.001 ^ 0.50

Grapefruit 526 21 4 0.001 - 0.057 0.001 - 0.010 15.0

Kale 708 243 34.3 0.003 - 11.5 0.002 ^ 25

Lettuce 378 8 2.1 0.002 - 0.66 0.002 ^ 30.0

Mangoes 177 38 21.5 0.001 - 0.51 0.001 ^ 2.0

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.002 1.0

Pineapple, Canned 756 0 0.002 - 0.010 NT

Plums, Dried / Prunes 191 25 13.1 0.002 - 0.025 0.002 ^ 2.0

Snap Peas 710 94 13.2 0.003 - 0.33 0.002 ^ 3.0

Sweet Potatoes 701 0 0.010 ^ 8.0

Tomatoes, Canned 566 107 18.9 0.002 - 0.015 0.001 ^ 0.2

TOTAL 8,733 651

Beflubutamid (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 - 0.005 NT

TOTAL 91 0

Benalaxyl (fungicide) 

Appendix B. Page 6 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.005 - 0.010 NT

TOTAL 1,115 0

Benazolin (herbicide) 

Grapefruit 271 0 0.050 ^ NT

Olives, Canned 630 0 0.050 ^ NT

TOTAL 901 0

Bendiocarb (insecticide) 

Applesauce 570 0 0.003 ^ SU

Asparagus 354 0 0.003 ^ SU

Cabbage 354 0 0.005 ^ SU

Cranberries 311 0 0.002 ^ SU

Cranberries, Frozen 428 0 0.002 ^ SU

Cucumbers 378 0 0.005 ^ SU

Garbanzo Beans, Canned 189 0 0.001 ^ SU

Grapefruit 526 0 0.001 - 0.015 SU

Kale 708 0 0.010 ^ SU

Lettuce 378 0 0.003 ^ SU

Mangoes 177 0 0.001 - 0.002 SU

Olives, Canned 754 0 0.001 ^ SU

Onions 679 0 0.001 - 0.005 SU

Pineapple, Canned 756 0 0.005 - 0.010 SU

Plums, Dried / Prunes 191 0 0.003 ^ SU

Snap Peas 710 0 0.010 ^ SU

Sweet Potatoes 701 0 0.010 ^ SU

Tomatoes, Canned 566 0 0.001 ^ SU

TOTAL 8,730 0

Benfluralin (herbicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Grapefruit 271 0 0.005 ^ NT

Lettuce 378 0 0.010 ^ 0.05

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

TOTAL 2,608 0

Benomyl (fungicide) 

Kale 176 0 0.10 ^ NT

Snap Peas 118 0 0.10 ^ NT

TOTAL 294 0

Benoxacor (herbicide safener) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ 0.1

Cabbage 354 0 0.005 ^ 0.01

Cranberries 311 0 0.020 ^ 0.01

Cranberries, Frozen 428 0 0.020 ^ 0.01

Garbanzo Beans, Canned 189 0 0.001 ^ 0.01

Appendix B. Page 7 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 526 0 0.003 - 0.020 NT

Lettuce 378 0 0.010 ^ 0.01

Mangoes 177 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 360 0 0.001 ^ 0.01

Pineapple, Canned 359 0 0.015 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ 0.01

Snap Peas 710 0 0.040 ^ 0.01

Sweet Potatoes 701 0 0.015 ^ 0.01

Tomatoes, Canned 566 0 0.001 ^ 0.01

TOTAL 6,928 0

Bensulide (herbicide) 

Applesauce 570 0 0.004 ^ NT

Asparagus 354 0 0.004 ^ NT

Grapefruit 526 0 0.005 - 0.015 NT

Kale 708 3 0.4 0.017 - 0.081 0.010 ^ 0.15

Lettuce 378 0 0.004 ^ 0.15

Mangoes 90 0 0.001 ^ NT

Olives, Canned 691 0 0.001 - 0.005 NT

Plums, Dried / Prunes 191 0 0.004 ^ NT

TOTAL 3,508 3

Bensulide oxygen analog (metabolite of Bensulide)

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Grapefruit 255 0 0.002 ^ NT

Lettuce 378 0 0.002 ^ 0.15

Mangoes 87 0 0.002 ^ NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

TOTAL 2,574 0

Bentazon (herbicide) 

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Grapefruit 526 0 0.003 - 0.10 NT

Mangoes 87 0 0.050 ^ NT

Olives, Canned 630 0 0.003 ^ NT

Pineapple, Canned 359 0 0.030 ^ NT

Sweet Potatoes 701 0 0.030 ^ NT

TOTAL 3,042 0

Benthiavalicarb isopropyl (fungicide) 

Pineapple, Canned 359 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 1,060 0

Bifenazate (acaricide) 

Cabbage 354 0 0.010 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ 7.0

Appendix B. Page 8 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 754 0 0.003 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Snap Peas 710 2 0.3 0.052 - 0.081 0.015 ^ 6.0

Sweet Potatoes 701 0 0.005 ^ 0.3

TOTAL 3,984 2

Bifenox (herbicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

TOTAL 1,115 0

Bifenthrin (insecticide) 

Applesauce 570 9 1.6 0.002 - 0.006 0.002 ^ 0.5

Asparagus 354 0 0.002 ^ 0.05

Cabbage 354 6 1.7 0.010 - 0.16 0.005 ^ 4.0

Cranberries 311 2 0.6 0.005 - 0.006 0.005 ^ 1.8

Cranberries, Frozen 428 4 0.9 0.009 - 0.016 0.005 ^ 1.8

Cucumbers 378 34 9 0.005 - 0.029 0.005 ^ 0.4

Garbanzo Beans, Canned 189 0 0.001 ^ 0.05

Grapefruit 526 0 0.003 - 0.040 0.05

Kale 708 210 29.7 0.002 - 2.5 0.001 ^ 3.5

Lettuce 378 0 0.002 ^ 3.0

Mangoes 177 1 0.6 0.003 ^ 0.001 - 0.005 0.05

Olives, Canned 754 0 0.001 - 0.003 0.05

Onions 708 0 0.001 - 0.005 0.05

Pineapple, Canned 756 0 0.005 - 0.010 0.05

Plums, Dried / Prunes 191 0 0.002 ^ 0.05

Snap Peas 710 64 9 0.002 - 0.11 0.001 ^ 0.6

Sweet Potatoes 701 1 0.1 0.012 ^ 0.010 ^ 0.05

Tomatoes, Canned 566 103 18.2 0.002 - 0.018 0.001 ^ 0.15

TOTAL 8,759 434

Bioallethrin (insecticide) 

Mangoes 30 0 0.010 ^ NT

Olives, Canned 61 0 0.010 ^ NT

TOTAL 91 0

Biphenyl (fungicide) 

Pineapple, Canned 359 0 0.075 ^ NT

Sweet Potatoes 701 0 0.075 ^ NT

TOTAL 1,060 0

Bitertanol (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,592 0

Appendix B. Page 9 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Boscalid (fungicide) 

Applesauce 570 38 6.7 0.003 - 0.018 0.003 ^ 3.0

Asparagus 354 0 0.003 ^ NT

Cabbage 354 2 0.6 0.040 - 0.19 0.010 ^ 3.0

Cranberries 309 0 0.005 ^ 13.0

Cranberries, Frozen 409 0 0.005 ^ 13.0

Cucumbers 378 31 8.2 0.010 - 0.26 0.010 ^ 0.5

Garbanzo Beans, Canned 189 0 0.001 ^ 0.6

Grapefruit 526 0 0.003 - 0.005 2.0

Kale 708 84 11.9 0.017 - 15.7 0.010 ^ 18.0

Lettuce 378 26 6.9 0.003 - 1.1 0.003 ^ 6.5/11.0 &

Mangoes 177 4 2.3 0.004 - 0.029 0.003 - 0.005 1.5

Olives, Canned 754 0 0.003 ^ NT

Onions 708 91 12.9 0.002 - 0.022 0.001 - 0.010 5.0

Pineapple, Canned 756 0 0.010 - 0.015 NT

Plums, Dried / Prunes 191 6 3.1 0.005 - 0.029 0.003 ^ 3.5

Snap Peas 710 29 4.1 0.017 - 0.46 0.010 ^ 5.0

Sweet Potatoes 701 0 0.015 ^ 0.05

Tomatoes, Canned 566 7 1.2 0.002 - 0.005 0.001 ^ 3.0

TOTAL 8,738 318

Bromacil (herbicide) 

Applesauce 570 0 0.003 ^ NT

Asparagus 354 0 0.003 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Grapefruit 526 0 0.005 - 0.010 0.1

Lettuce 378 0 0.003 ^ NT

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Pineapple, Canned 359 0 0.020 ^ 0.1

Plums, Dried / Prunes 191 0 0.003 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

TOTAL 4,749 0

Bromophos ethyl (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Bromopropylate (acaricide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 2,592 0

Bromoxynil (herbicide) 

Grapefruit 271 0 0.010 ^ NT

Olives, Canned 630 0 0.010 ^ NT

TOTAL 901 0

Appendix B. Page 10 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Bromuconazole (fungicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

TOTAL 1,115 0

Bupirimate (fungicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,652 0

Buprofezin (insecticide) 

Applesauce 570 1 0.2 0.001 ^ 0.001 ^ 3.0

Asparagus 354 0 0.001 ^ NT

Cabbage 354 1 0.3 0.011 ^ 0.010 ^ 12.0

Cranberries 311 0 0.001 ^ 2.5

Cranberries, Frozen 428 0 0.001 ^ 2.5

Cucumbers 378 2 0.5 0.014 - 0.056 0.010 ^ 0.50

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ 2.5

Kale 708 30 4.2 0.002 - 5.0 0.001 ^ 60

Lettuce 378 0 0.001 ^ 6.0/35 &

Mangoes 177 0 0.001 ^ 0.90

Olives, Canned 754 109 14.5 0.001 - 0.057 0.001 ^ 3.5

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.001 - 0.010 NT

Plums, Dried / Prunes 191 1 0.5 0.001 ^ 0.001 ^ 1.9

Snap Peas 710 3 0.4 0.002 - 0.004 0.001 ^ V-3 NT

Sweet Potatoes 701 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ 2.0

TOTAL 8,759 147

Butachlor (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Butocarboxim (insecticide, acaricide)

Cabbage 294 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Onions 320 0 0.010 ^ NT

Pineapple, Canned 722 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 2,415 0

Butocarboxim sulfone (metabolite of Butocarboxim)

Pineapple, Canned 359 0 0.015 ^ NT

Appendix B. Page 11 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 701 0 0.015 ^ NT

TOTAL 1,060 0

Butocarboxim sulfoxide (metabolite of Butocarboxim)

Pineapple, Canned 359 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 1,060 0

Butylate (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

TOTAL 1,115 0

Cadusafos (insecticide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Captan (fungicide) (parent of THPI)

Cucumbers 292 0 0.020 ^ 0.05

Kale 708 0 0.050 ^ 0.05

Onions 348 0 0.020 ^ 0.05

Pineapple, Canned 397 0 0.020 ^ NT

Snap Peas 710 0 0.050 ^ 0.05

TOTAL 2,455 0

Carbaryl (insecticide) 

Applesauce 570 11 1.9 0.004 - 0.11 0.003 ^ 12

Asparagus 354 0 0.003 ^ 15

Cabbage 354 0 0.010 ^ 21

Cranberries 311 0 0.002 ^ 3.0

Cranberries, Frozen 428 0 0.002 ^ 3.0

Cucumbers 378 0 0.010 ^ 3.0

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.002 - 0.003 10

Kale 708 3 0.4 0.033 - 0.14 0.020 ^ 10

Lettuce 378 0 0.003 ^ 10

Mangoes 177 0 0.002 - 0.003 NT

Olives, Canned 754 0 0.003 ^ 10

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 2.0

Plums, Dried / Prunes 191 1 0.5 0.11 ^ 0.003 ^ 10

Snap Peas 710 0 0.020 ^ 10

Sweet Potatoes 701 0 0.005 ^ 0.2

Tomatoes, Canned 566 0 0.001 ^ 5.0

TOTAL 8,759 15

Carbendazim - MBC (fungicide) (metabolite of Benomyl and Thiophanate Methyl)

Applesauce 570 382 67 0.001 - 0.060 0.001 ^ 2.0

Asparagus 294 1 0.3 0.002 ^ 0.001 ^ V-1 NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 37 9.8 0.010 - 0.051 0.010 ^ 1.0

Appendix B. Page 12 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 271 0 0.001 ^ NT

Kale 708 0 0.015 ^ NT

Lettuce 378 1 0.3 0.003 ^ 0.001 ^ V-1 NT

Mangoes 177 28 15.8 0.001 - 0.015 0.001 - 0.010 V-28 NT

Olives, Canned 754 25 3.3 0.001 - 0.004 0.001 ^ V-25 NT

Onions 708 0 0.001 - 0.010 0.5

Pineapple, Canned 756 1 0.1 0.012 ^ 0.010 ^ V-1 NT

Plums, Dried / Prunes 191 23 12 0.001 - 0.007 0.001 ^ 0.5

Snap Peas 710 46 6.5 0.025 - 2.3 0.015 ^ V-46 NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,705 544

Carbofuran (insecticide) (parent of 3-Hydroxycarbofuran)

Applesauce 570 0 0.002 ^ NT

Asparagus 354 4 1.1 0.005 - 0.13 0.001 - 0.002 V-4 NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Kale 708 0 0.005 ^ NT

Lettuce 378 0 0.002 ^ NT

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Snap Peas 710 0 0.005 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 8,759 4

Carbophenothion (insecticide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.005 - 0.010 NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Carboxin (fungicide) 

Cabbage 354 0 0.005 ^ NT

Cranberries 266 0 0.025 ^ NT

Cranberries, Frozen 402 0 0.025 ^ NT

Grapefruit 526 0 0.003 - 0.050 NT

Mangoes 177 0 0.003 - 0.025 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,479 0

Appendix B. Page 13 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carfentrazone (herbicide) 

Applesauce 570 0 0.005 ^ 0.10

Asparagus 327 0 0.005 ^ 0.10

Cabbage 354 0 0.005 ^ 0.10

Cranberries 311 0 0.005 ^ 0.10

Cranberries, Frozen 428 0 0.005 ^ 0.10

Cucumbers 378 0 0.005 ^ 0.10

Garbanzo Beans, Canned 189 0 0.005 ^ 0.10

Grapefruit 526 0 0.003 - 0.005 0.10

Kale 708 0 0.002 ^ 0.10

Lettuce 378 0 0.005 ^ 0.10

Mangoes 177 0 0.003 - 0.005 0.10

Olives, Canned 754 0 0.003 ^ 0.10

Onions 708 0 0.005 ^ 0.10

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.005 ^ 0.10

Snap Peas 710 0 0.002 ^ 0.10

Sweet Potatoes 701 0 0.020 ^ 0.10

Tomatoes, Canned 566 0 0.005 - 0.015 0.10

TOTAL 8,732 0

Chlorantraniliprole (insecticide) 

Applesauce 570 1 0.2 0.011 ^ 0.010 ^ 1.2

Asparagus 354 1 0.3 0.030 ^ 0.010 ^ 13

Cabbage 354 6 1.7 0.021 - 0.056 0.020 ^ 4.0

Cranberries 311 38 12.2 0.005 - 0.018 0.005 ^ 2.5

Cranberries, Frozen 428 38 8.9 0.005 - 0.016 0.005 ^ 2.5

Cucumbers 378 0 0.020 ^ 0.5

Garbanzo Beans, Canned 189 0 0.002 ^ 2.0

Grapefruit 526 0 0.001 - 0.005 1.4

Kale 708 172 24.3 0.017 - 7.5 0.010 ^ 11

Lettuce 378 9 2.4 0.011 - 0.078 0.010 ^ 13

Mangoes 177 0 0.005 ^ 4.0

Olives, Canned 754 0 0.005 ^ 4.0

Onions 708 0 0.002 - 0.020 0.30

Pineapple, Canned 726 0 0.010 - 0.020 3.0

Plums, Dried / Prunes 191 0 0.010 ^ 2.5

Snap Peas 710 66 9.3 0.017 - 0.19 0.010 ^ 2.0

Sweet Potatoes 701 0 0.010 ^ 0.30

Tomatoes, Canned 566 0 0.002 ^ 1.4

TOTAL 8,729 331

Chlordimeform (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Chlorethoxyfos (insecticide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.020 NT

Mangoes 177 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 - 0.020 NT

Appendix B. Page 14 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

TOTAL 2,196 0

Chlorfenapyr (insecticide) 

Applesauce 570 0 0.015 ^ 0.01

Asparagus 354 0 0.015 ^ 0.01

Cabbage 354 0 0.005 ^ 0.01

Cranberries 311 0 0.025 ^ 0.01

Cranberries, Frozen 428 0 0.025 ^ 0.01

Cucumbers 378 11 2.9 0.011 - 0.031 0.005 ^ X-7 0.01

Garbanzo Beans, Canned 189 0 0.002 ^ 0.01

Grapefruit 526 0 0.025 - 0.25 0.01

Kale 708 0 0.020 - 0.067 0.01

Lettuce 378 0 0.015 ^ 0.01

Mangoes 117 0 0.005 - 0.025 0.01

Olives, Canned 691 0 0.005 - 0.25 0.01

Onions 708 0 0.002 - 0.005 0.01

Pineapple, Canned 756 0 0.005 - 0.040 0.01

Plums, Dried / Prunes 191 0 0.015 ^ 0.01

Snap Peas 710 0 0.020 ^ 0.01

Sweet Potatoes 701 0 0.040 ^ 0.01

Tomatoes, Canned 566 0 0.002 ^ 1.0

TOTAL 8,636 11

Chlorfenvinphos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.002 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 2,584 0

Chlorimuron ethyl (herbicide) 

Cranberries 311 0 0.005 ^ 0.02

Cranberries, Frozen 428 0 0.005 ^ 0.02

Grapefruit 271 0 0.003 ^ NT

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,941 0

Chlorobenzilate (acaricide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

TOTAL 1,115 0

Chloroneb (fungicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

TOTAL 1,115 0

Chlorothalonil (fungicide) 

Appendix B. Page 15 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Asparagus 354 0 0.020 ^ 0.1

Cucumbers 378 31 8.2 0.005 - 0.64 0.005 ^ 5.0

Grapefruit 271 0 0.005 ^ NT

Mangoes 177 0 0.005 ^ 1.0

Olives, Canned 61 0 0.005 ^ NT

Onions 290 0 0.005 ^ 0.5

Pineapple, Canned 397 0 0.005 ^ NT

Plums, Dried / Prunes 159 0 0.020 ^ 0.2

TOTAL 2,087 31

Chlorpropham (herbicide, growth regulator)

Applesauce 570 0 0.020 ^ NT

Asparagus 354 0 0.020 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 1 0.3 0.023 ^ 0.005 ^ V-1 NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 5 1.3 0.006 - 0.047 0.005 ^ V-5 NT

Garbanzo Beans, Canned 189 0 0.001 - 0.003 NT

Grapefruit 526 0 0.003 - 0.005 NT

Lettuce 378 0 0.020 ^ NT

Mangoes 177 6 3.4 0.002 - 0.044 0.001 - 0.005 V-6 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

Sweet Potatoes 701 3 0.4 0.024 - 0.029 0.020 ^ V-3 NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 15

Chlorpyrifos (insecticide) 

Applesauce 570 1 0.2 0.006 ^ 0.005 ^ 0.1

Asparagus 354 31 8.8 0.005 - 0.16 0.005 ^ 5.0

Cabbage 354 0 0.005 ^ 1.0

Cranberries 311 1 0.3 0.039 ^ 0.015 ^ 1.0

Cranberries, Frozen 428 0 0.015 ^ 1.0

Cucumbers 378 4 1.1 0.007 - 0.060 0.005 ^ 0.1

Garbanzo Beans, Canned 189 0 0.001 ^ 0.1

Grapefruit 526 0 0.003 - 0.035 1.0

Kale 708 9 1.3 0.017 - 0.27 0.010 ^ 1.0

Lettuce 378 1 0.3 0.006 ^ 0.005 ^ 0.1

Mangoes 177 0 0.003 - 0.015 0.1

Olives, Canned 754 14 1.9 0.003 - 0.020 0.003 ^ 0.1

Onions 708 0 0.001 - 0.005 0.5

Pineapple, Canned 756 0 0.005 - 0.010 0.1

Plums, Dried / Prunes 191 0 0.005 ^ 0.1

Snap Peas 710 7 1 0.017 - 0.11 0.010 ^ 0.1

Sweet Potatoes 701 2 0.3 0.010 - 0.013 0.010 ^ 0.1

Tomatoes, Canned 566 7 1.2 0.002 - 0.009 0.001 ^ 0.1

TOTAL 8,759 77

Chlorpyrifos methyl (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Appendix B. Page 16 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Chlorpyrifos oxygen analog (metabolite of Chlorpyrifos)

Applesauce 570 0 0.002 ^ 0.1

Asparagus 354 0 0.004 ^ 5.0

Cabbage 354 0 0.010 ^ 1.0

Cranberries 311 0 0.005 ^ 1.0

Cranberries, Frozen 428 0 0.005 ^ 1.0

Cucumbers 378 0 0.010 ^ 0.1

Garbanzo Beans, Canned 189 0 0.001 ^ 0.1

Grapefruit 526 0 0.001 ^ 1.0

Kale 708 0 0.003 ^ 1.0

Lettuce 378 1 0.3 0.002 ^ 0.002 ^ 0.1

Mangoes 177 0 0.001 - 0.005 0.1

Olives, Canned 754 0 0.001 ^ 0.1

Onions 708 0 0.001 - 0.010 0.5

Pineapple, Canned 756 0 0.005 - 0.010 0.1

Plums, Dried / Prunes 159 0 0.002 - 0.004 0.1

Snap Peas 710 0 0.003 ^ 0.1

Sweet Potatoes 701 0 0.005 ^ 0.1

Tomatoes, Canned 566 0 0.001 ^ 0.1

TOTAL 8,727 1

Chlorsulfuron (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Chlorthiophos (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Clethodim (herbicide) 

Cabbage 354 0 0.010 ^ 3.0

Cranberries 279 0 0.20 ^ 0.50

Cranberries, Frozen 403 0 0.20 ^ 0.50

Garbanzo Beans, Canned 189 0 0.002 ^ 3.5

Grapefruit 526 0 0.010 - 0.40 NT

Kale 708 0 0.010 ^ 3.0

Mangoes 177 0 0.010 - 0.20 NT

Olives, Canned 754 0 0.010 ^ NT

Onions 708 0 0.002 - 0.010 0.50

Pineapple, Canned 397 0 0.010 ^ NT

Snap Peas 710 0 0.010 ^ 3.5

Tomatoes, Canned 566 0 0.002 ^ 1.0

TOTAL 5,771 0

Clofentezine (insecticide) 

Grapefruit 241 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,085 0

Appendix B. Page 17 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Clomazone (herbicide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ 0.05

Cabbage 354 0 0.005 ^ 0.1

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 0.1

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.003 - 0.005 NT

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.070 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Snap Peas 710 0 0.003 ^ 0.05

Sweet Potatoes 701 0 0.070 ^ 0.05

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 7,691 0

Clopyralid (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Olives, Canned 630 0 0.020 ^ NT

TOTAL 901 0

Cloransulam methyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Clothianidin (insecticide) (also a metabolite of Thiamethoxam)

Applesauce 570 0 0.010 ^ 1.0

Asparagus 354 1 0.3 0.028 ^ 0.010 ^ 0.02

Cabbage 354 2 0.6 0.012 - 0.018 0.010 ^ 1.9

Cranberries 311 0 0.025 ^ 0.01

Cranberries, Frozen 428 0 0.025 ^ 0.01

Cucumbers 378 1 0.3 0.016 ^ 0.010 ^ 0.06

Garbanzo Beans, Canned 189 0 0.005 ^ 0.02

Grapefruit 526 5 1 0.002 - 0.012 0.001 - 0.005 0.07

Kale 708 9 1.3 0.083 - 0.17 0.050 ^ 1.9

Lettuce 378 2 0.5 0.010 - 0.017 0.010 ^ 3.0

Mangoes 177 6 3.4 0.001 - 0.006 0.001 - 0.025 0.40

Olives, Canned 754 0 0.001 ^ 0.02

Onions 708 0 0.002 - 0.010 0.45

Pineapple, Canned 756 0 0.010 - 0.035 0.02

Plums, Dried / Prunes 191 0 0.010 ^ 0.5

Snap Peas 710 0 0.050 ^ 0.02

Sweet Potatoes 701 0 0.035 ^ 0.3

Tomatoes, Canned 566 3 0.5 0.006 - 0.009 0.005 ^ 0.20

TOTAL 8,759 29

Coumaphos (insecticide) 

Applesauce 570 0 0.010 ^ NT

Appendix B. Page 18 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 397 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 5,200 0

Coumaphos oxygen analog (metabolite of Coumaphos)

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.003 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.003 ^ NT

TOTAL 3,723 0

Crotoxyphos (insecticide, acaricide)

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Crufomate (insecticide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Cumyluron (herbicide) 

Cabbage 354 0 0.010 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 1,099 0

Cyantraniliprole (insecticide) 

Cranberries 311 0 0.005 ^ 4.0

Cranberries, Frozen 428 1 0.2 0.006 ^ 0.005 ^ 4.0

Garbanzo Beans, Canned 189 0 0.002 ^ 0.20

Grapefruit 526 0 0.003 - 0.005 0.70

Kale 708 51 7.2 0.017 - 8.4 0.010 ^ 30

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ 1.5

Appendix B. Page 19 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 360 0 0.008 ^ 0.04

Pineapple, Canned 329 0 0.15 ^ NT

Sweet Potatoes 701 0 0.15 ^ 0.15

Tomatoes, Canned 566 0 0.002 ^ 2.0

TOTAL 5,049 52

Cyazofamid (fungicide) 

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.006 ^ NT

Grapefruit 526 0 0.010 ^ NT

Kale 708 31 4.4 0.008 - 2.8 0.005 ^ 12.0

Mangoes 177 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

Onions 360 0 0.006 ^ 2.0

Pineapple, Canned 359 0 0.020 ^ NT

Sweet Potatoes 701 0 0.020 ^ 0.02

Tomatoes, Canned 566 0 0.006 ^ 0.9

TOTAL 5,079 31

Cyclanilide (plant growth regulator) 

Grapefruit 271 0 0.020 ^ NT

Olives, Canned 630 0 0.020 ^ NT

TOTAL 901 0

Cyflufenamid (fungicide) 

Cabbage 354 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,214 0

Cyflumetofen (acaricide) 

Cranberries 311 0 0.020 ^ NT

Cranberries, Frozen 409 0 0.020 ^ NT

Grapefruit 526 0 0.003 - 0.20 0.30

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,090 0

Cyfluthrin (insecticide) 

Applesauce 570 0 0.004 ^ 0.5

Asparagus 354 0 0.004 ^ 0.05

Cabbage 354 4 1.1 0.006 - 0.020 0.005 ^ 2.5

Cranberries 311 0 0.050 ^ 0.05

Cranberries, Frozen 428 0 0.050 ^ 0.05

Cucumbers 378 3 0.8 0.006 - 0.019 0.005 ^ 0.1

Garbanzo Beans, Canned 189 0 0.025 ^ 0.05

Grapefruit 526 0 0.010 ^ 0.2

Kale 708 79 11.2 0.013 - 2.6 0.008 ^ 7.0

Lettuce 378 3 0.8 0.036 - 0.29 0.004 ^ 2.0/3.0 &

Mangoes 177 0 0.003 - 0.050 0.05

Appendix B. Page 20 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 754 0 0.003 - 0.010 0.05

Onions 708 0 0.005 - 0.008 0.05

Pineapple, Canned 756 0 0.005 - 0.045 0.05

Plums, Dried / Prunes 191 0 0.004 ^ 0.3

Snap Peas 710 0 0.008 ^ 0.25

Sweet Potatoes 701 0 0.045 ^ 0.01

Tomatoes, Canned 566 0 0.008 - 0.025 0.20

TOTAL 8,759 89

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (insecticide)

Applesauce 570 0 0.005 ^ 0.30

Asparagus 354 0 0.005 ^ 0.01

Cabbage 354 6 1.7 0.015 - 0.048 0.008 ^ 0.40

Cranberries 311 0 0.005 ^ 0.01

Cranberries, Frozen 428 0 0.005 ^ 0.01

Cucumbers 378 6 1.6 0.009 - 0.022 0.008 ^ 0.05

Garbanzo Beans, Canned 189 0 0.003 ^ 0.01

Grapefruit 526 0 0.010 - 0.025 0.01

Lettuce 378 26 6.9 0.009 - 0.64 0.005 ^ 2.0

Mangoes 177 1 0.6 0.005 ^ 0.003 - 0.010 0.01

Olives, Canned 754 0 0.003 - 0.010 0.01

Onions 708 0 0.003 - 0.008 0.1

Pineapple, Canned 756 0 0.008 - 0.015 0.01

Plums, Dried / Prunes 191 0 0.005 ^ 0.50

Sweet Potatoes 701 0 0.015 ^ 0.02

Tomatoes, Canned 566 17 3 0.005 - 0.029 0.003 ^ 0.1

TOTAL 7,341 56

Cyhalothrin, Lambda (includes gamma isomer)

Kale 708 55 7.8 0.003 - 0.33 0.002 ^ X-16 0.01

Snap Peas 710 146 20.6 0.003 - 0.091 0.002 ^ 0.20

TOTAL 1,418 201

Cymoxanil (fungicide)

Applesauce 570 0 0.002 ^ NT

Asparagus 237 0 0.005 ^ NT

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 526 0 0.010 ^ NT

Lettuce 378 4 1.1 0.006 - 0.098 0.002 ^ 19

Mangoes 177 0 0.010 - 0.050 NT

Olives, Canned 754 0 0.010 ^ NT

Onions 330 0 0.003 - 0.010 0.05

Pineapple, Canned 359 0 0.020 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.003 ^ 0.2

TOTAL 5,717 4

Cypermethrin (insecticide) 

Applesauce 570 0 0.010 ^ 2

Asparagus 354 2 0.6 0.020 - 0.14 0.010 ^ X-1 0.05

Cabbage 354 9 2.5 0.013 - 0.065 0.010 ^ 2.0

Appendix B. Page 21 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.050 ^ 0.8

Cranberries, Frozen 428 0 0.050 ^ 0.8

Cucumbers 378 12 3.2 0.011 - 0.094 0.010 ^ 0.2

Garbanzo Beans, Canned 189 0 0.075 ^ 0.1

Grapefruit 526 0 0.020 - 0.025 0.35

Kale 708 203 28.7 0.020 - 4.2 0.012 ^ 14.0

Lettuce 378 10 2.6 0.022 - 0.25 0.010 ^ 4.0/10.00 &

Mangoes 177 1 0.6 0.011 ^ 0.010 - 0.050 0.70

Olives, Canned 754 0 0.010 - 0.020 0.05

Onions 708 0 0.010 - 0.022 0.1

Pineapple, Canned 756 0 0.010 - 0.070 0.05

Plums, Dried / Prunes 191 4 2.1 0.012 - 0.073 0.010 ^ 1

Snap Peas 710 88 12.4 0.020 - 0.61 0.012 ^ X-1 0.5

Sweet Potatoes 701 0 0.070 ^ 0.1

Tomatoes, Canned 566 0 0.022 ^ 0.2

TOTAL 8,759 329

Cyphenothrin (insecticide) 

Applesauce 570 0 0.015 ^ NT

Asparagus 354 0 0.015 ^ NT

Cabbage 354 0 0.008 ^ NT

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Grapefruit 526 0 0.010 - 0.050 NT

Kale 708 0 0.030 ^ NT

Lettuce 378 0 0.015 ^ NT

Mangoes 177 0 0.010 - 0.050 NT

Olives, Canned 754 0 0.010 ^ NT

Pineapple, Canned 359 0 0.060 ^ NT

Plums, Dried / Prunes 191 0 0.015 ^ NT

Snap Peas 710 0 0.030 ^ NT

Sweet Potatoes 701 0 0.060 ^ NT

TOTAL 6,521 0

Cyproconazole (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Grapefruit 271 0 0.005 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 - 0.005 NT

Pineapple, Canned 359 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,668 0

Cyprodinil (fungicide) 

Applesauce 570 59 10.4 0.005 - 0.015 0.005 ^ 1.7

Asparagus 354 0 0.005 ^ NT

Cabbage 354 1 0.3 0.006 ^ 0.005 ^ 1.0

Cranberries 311 0 0.005 ^ 3.0

Cranberries, Frozen 428 0 0.005 ^ 3.0

Cucumbers 378 30 7.9 0.007 - 0.11 0.005 ^ 0.70

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Appendix B. Page 22 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 526 0 0.005 - 0.055 NT

Kale 708 13 1.8 0.005 - 0.30 0.003 ^ 10.0

Lettuce 378 0 0.005 ^ 50

Mangoes 177 0 0.003 - 0.005 1.2

Olives, Canned 754 0 0.003 - 0.005 NT

Onions 348 0 0.005 ^ 0.6

Pineapple, Canned 756 0 0.005 - 0.015 NT

Plums, Dried / Prunes 191 1 0.5 0.006 ^ 0.005 ^ 2.0

Sweet Potatoes 701 0 0.015 ^ 0.01

TOTAL 7,123 104

Cyprosulfamide (herbicide safener) 

Cranberries 311 0 0.004 ^ NT

Cranberries, Frozen 428 0 0.004 ^ NT

Grapefruit 526 0 0.002 - 0.003 NT

Mangoes 177 0 0.003 - 0.004 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,196 0

Cyromazine (insect growth regulator) 

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Garbanzo Beans, Canned 189 0 0.008 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ 0.3

Olives, Canned 754 0 0.005 ^ NT

TOTAL 2,043 0

DCPA (herbicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cabbage 354 0 0.005 ^ 5

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 1.0

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.003 - 0.010 NT

Kale 708 389 54.9 0.002 - 0.74 0.001 ^ 5.0

Lettuce 378 17 4.5 0.002 - 0.008 0.002 ^ 2.0

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 679 0 0.001 - 0.005 1.0

Pineapple, Canned 693 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Snap Peas 710 53 7.5 0.002 - 0.014 0.001 ^ V-53 NT

Sweet Potatoes 701 0 0.020 ^ 2.0

Tomatoes, Canned 566 0 0.001 ^ 1.0

TOTAL 8,667 459

DEF - Tribufos (herbicide, plant growth regulator)

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Appendix B. Page 23 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Deltamethrin (includes parent Tralomethrin) (insecticide) 

Applesauce 570 0 0.015 ^ 0.2

Asparagus 354 0 0.015 ^ 0.05

Cabbage 354 0 0.008 ^ 0.05

Cranberries 311 0 0.050 ^ 0.05

Cranberries, Frozen 428 0 0.050 ^ 0.05

Cucumbers 378 0 0.008 ^ 0.2

Garbanzo Beans, Canned 189 0 0.040 ^ 0.05

Grapefruit 526 0 0.005 - 0.50 0.05

Kale 708 5 0.7 0.007 - 1.9 0.004 ^ X-3 0.05

Lettuce 378 0 0.015 ^ 0.05

Mangoes 177 0 0.001 - 0.050 0.05

Olives, Canned 754 0 0.001 - 0.005 0.05

Onions 708 0 0.008 - 0.012 0.1

Pineapple, Canned 756 0 0.008 - 0.12 0.05

Plums, Dried / Prunes 191 0 0.015 ^ 0.05

Snap Peas 710 34 4.8 0.007 - 0.16 0.004 ^ X-1 0.05

Sweet Potatoes 701 1 0.1 0.12 ^ 0.12 ^ X-1 0.05

Tomatoes, Canned 566 0 0.012 ^ 0.2

TOTAL 8,759 40

Demeton-O (metabolite of the insecticide Demeton)

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

TOTAL 1,115 0

Demeton-S (metabolite of Demeton)

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

TOTAL 1,115 0

Demeton-S sulfone (metabolite of Demeton-S)

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Desethyl atrazine (herbicide metabolite)

Mangoes 30 0 0.003 ^ NT

Olives, Canned 61 0 0.003 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 1,017 0

Desisopropyl atrazine (herbicide metabolite)

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 566 0

Desmedipham (herbicide) 

Pineapple, Canned 359 0 0.030 ^ NT

Sweet Potatoes 672 0 0.030 ^ NT

Appendix B. Page 24 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

TOTAL 1,031 0

Desmetryn (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Dialifos (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Diazinon (insecticide) 

Applesauce 570 0 0.005 ^ 0.50

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.002 ^ 0.70

Cranberries 311 3 1 0.005 - 0.007 0.005 ^ 0.50

Cranberries, Frozen 428 0 0.005 ^ 0.50

Cucumbers 378 2 0.5 0.010 - 0.034 0.002 ^ 0.75

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Kale 708 3 0.4 0.002 - 0.22 0.001 ^ 0.70

Lettuce 378 0 0.005 ^ 0.70

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.002 0.75

Pineapple, Canned 756 0 0.002 - 0.010 0.50

Plums, Dried / Prunes 191 0 0.005 ^ 0.20

Snap Peas 710 2 0.3 0.002 - 0.005 0.001 ^ 0.50

Sweet Potatoes 701 0 0.010 ^ 0.10

Tomatoes, Canned 566 0 0.001 ^ 0.75

TOTAL 8,759 10

Diazinon oxygen analog (metabolite of Diazinon)

Cabbage 354 0 0.001 ^ 0.70

Cranberries 246 0 0.005 ^ 0.50

Cranberries, Frozen 317 0 0.005 ^ 0.50

Cucumbers 378 0 0.001 ^ 0.75

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Kale 708 0 0.001 ^ 0.70

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 ^ 0.75

Pineapple, Canned 756 0 0.001 - 0.010 0.50

Snap Peas 710 0 0.001 ^ 0.50

Sweet Potatoes 701 0 0.010 ^ 0.10

Tomatoes, Canned 566 0 0.001 ^ 0.75

TOTAL 7,090 0

Dichlobenil (herbicide) 

Applesauce 570 0 0.010 ^ 0.5

Asparagus 354 0 0.010 ^ NT

Appendix B. Page 25 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.002 ^ 0.15

Cranberries, Frozen 428 0 0.002 ^ 0.15

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.010 ^ 0.15

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,086 0

Dichlofenthion (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Dichlormid (herbicide safener)

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.020 NT

Mangoes 177 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.020 ^ NT

TOTAL 2,196 0

Dichlorprop (herbicide) 

Grapefruit 271 0 0.050 ^ NT

Olives, Canned 630 0 0.050 ^ NT

TOTAL 901 0

Dichlorvos - DDVP (insecticide) (also a metabolite of Naled)

Applesauce 570 0 0.020 ^ 0.5

Asparagus 354 0 0.020 ^ 0.5

Cabbage 354 0 0.010 ^ 1.0

Cranberries 311 0 0.005 ^ 0.5

Cranberries, Frozen 428 0 0.005 ^ 0.5

Cucumbers 378 3 0.8 0.011 - 0.051 0.010 ^ 0.5

Garbanzo Beans, Canned 189 0 0.002 ^ 0.5

Grapefruit 526 0 0.005 - 0.020 3

Lettuce 378 0 0.020 ^ 0.5

Mangoes 177 0 0.005 - 0.020 0.5

Olives, Canned 754 0 0.020 ^ 0.5

Onions 708 0 0.005 - 0.010 0.5

Pineapple, Canned 756 0 0.005 - 0.010 0.5

Plums, Dried / Prunes 191 0 0.020 ^ 0.5

Snap Peas 710 0 0.050 ^ 0.5

Sweet Potatoes 701 0 0.005 ^ 0.5

TOTAL 7,485 3

Appendix B. Page 26 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Diclofop methyl (herbicide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

TOTAL 1,493 0

Dicloran (fungicide) 

Applesauce 570 0 0.016 ^ NT

Asparagus 354 0 0.016 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 7 1.9 0.006 - 0.12 0.005 ^ 5

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.020 - 0.10 NT

Lettuce 378 0 0.016 ^ 10

Mangoes 177 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.001 - 0.020 NT

Onions 708 8 1.1 0.004 - 0.029 0.002 - 0.005 10

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.016 ^ 15

Snap Peas 710 0 0.030 ^ NT

Sweet Potatoes 701 179 25.5 0.022 - 4.7 0.020 ^ 10

Tomatoes, Canned 566 0 0.002 ^ 5

TOTAL 8,051 194

Diclosulam (herbicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 30 0 0.003 ^ NT

Olives, Canned 691 0 0.003 - 0.010 NT

TOTAL 992 0

Dicofol Total (insecticide) 

Mangoes 30 0 0.003 ^ NT

Olives, Canned 61 0 0.003 ^ NT

TOTAL 91 0

Dicofol o,p' (isomer of Dicofol) 

Grapefruit 271 0 0.005 ^ 6.0

Mangoes 60 0 0.005 ^ NT

Olives, Canned 693 0 0.005 ^ NT

Pineapple, Canned 329 0 0.015 ^ NT

Sweet Potatoes 701 0 0.015 ^ NT

TOTAL 2,054 0

Dicofol p,p' (isomer of Dicofol) 

Applesauce 570 0 0.010 ^ 10.0

Asparagus 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 ^ 6.0

Appendix B. Page 27 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Lettuce 378 0 0.010 ^ NT

Mangoes 147 0 0.005 ^ NT

Olives, Canned 693 0 0.005 ^ NT

Onions 360 0 0.001 ^ NT

Pineapple, Canned 329 0 0.025 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ 5.0

Sweet Potatoes 701 0 0.025 ^ NT

Tomatoes, Canned 566 0 0.001 ^ 2.0

TOTAL 5,743 0

Dicrotophos (insecticide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Diethofencarb (fungicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Difenoconazole (fungicide) 

Applesauce 570 0 0.010 ^ 5.0

Asparagus 354 0 0.010 ^ NT

Cabbage 354 2 0.6 0.011 - 0.022 0.005 ^ 1.9

Cranberries 311 0 0.002 ^ 4.0

Cranberries, Frozen 428 0 0.002 ^ 4.0

Cucumbers 378 1 0.3 0.023 ^ 0.005 ^ 0.70

Garbanzo Beans, Canned 189 0 0.010 ^ NT

Grapefruit 526 0 0.003 - 0.005 0.60

Kale 708 39 5.5 0.002 - 1.6 0.001 ^ 35

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.001 - 0.003 0.07

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 0.20

Pineapple, Canned 756 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ 2.5

Sweet Potatoes 701 2 0.3 0.006 - 0.013 0.005 ^ 4.0

Tomatoes, Canned 566 37 6.5 0.003 - 0.021 0.003 ^ 0.60

TOTAL 8,049 81

Diflubenzuron (insecticide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.001 - 0.002 NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.020 3.0

Kale 708 3 0.4 0.035 - 1.4 0.005 ^ 9.0

Lettuce 378 1 0.3 0.002 ^ 0.002 ^ V-1 NT

Appendix B. Page 28 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.003 ^ NT

Pineapple, Canned 359 0 0.080 ^ NT

Plums, Dried / Prunes 191 0 0.002 ^ 0.50

Sweet Potatoes 701 0 0.080 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,572 4

Diflufenzopyr (herbicide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 255 0 0.001 ^ NT

TOTAL 994 0

Dimepiperate (herbicide) 

Mangoes 30 0 0.003 ^ NT

Olives, Canned 61 0 0.003 ^ NT

TOTAL 91 0

Dimethenamid (herbicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.001 - 0.002 NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Lettuce 378 0 0.002 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 - 0.003 0.01

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 0 0.010 ^ 0.01

Tomatoes, Canned 566 0 0.001 - 0.003 NT

TOTAL 6,218 0

Dimethoate (insecticide) (parent of Omethoate)

Applesauce 570 0 0.005 ^ NT

Asparagus 354 2 0.6 0.079 - 1.8 0.005 ^ X-1 0.15

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.001 ^ 2.0

Kale 708 4 0.6 0.025 - 0.14 0.015 ^ 2.0

Lettuce 378 0 0.005 ^ 2.0

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.010 NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Appendix B. Page 29 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Snap Peas 710 105 14.8 0.025 - 2.0 0.015 ^ 2.0

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 ^ 2.0

TOTAL 8,759 111

Dimethomorph (fungicide) 

Applesauce 570 0 0.003 ^ NT

Asparagus 354 0 0.003 ^ NT

Cabbage 354 2 0.6 0.014 - 0.033 0.010 ^ 6.0

Cranberries 311 0 0.020 ^ NT

Cranberries, Frozen 428 0 0.020 ^ NT

Cucumbers 378 7 1.9 0.011 - 0.026 0.010 ^ 0.5

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.003 - 0.25 NT

Kale 708 41 5.8 0.050 - 13.7 0.030 ^ 30.0

Lettuce 378 74 19.6 0.003 - 1.5 0.003 ^ 30.0

Mangoes 177 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.001 - 0.010 0.6

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.003 ^ NT

Snap Peas 710 0 0.030 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 10 1.8 0.002 - 0.009 0.001 ^ 1.5

TOTAL 8,759 134

Diniconazole (fungicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

TOTAL 1,115 0

Dinotefuran (insecticide) 

Applesauce 570 4 0.7 0.003 - 0.005 0.003 ^ 2.0

Asparagus 354 0 0.003 ^ 0.01

Cabbage 354 3 0.8 0.012 - 0.040 0.010 ^ 1.4

Cranberries 311 0 0.040 ^ 0.2

Cranberries, Frozen 428 0 0.040 ^ 0.2

Cucumbers 378 19 5 0.010 - 0.16 0.010 ^ 0.5

Garbanzo Beans, Canned 189 0 0.006 ^ 0.01

Grapefruit 526 0 0.003 - 0.040 0.01

Kale 708 12 1.7 0.083 - 0.64 0.050 ^ 15.0

Lettuce 378 1 0.3 0.003 ^ 0.003 ^ 5.0

Mangoes 177 0 0.003 - 0.040 0.01

Olives, Canned 754 0 0.003 ^ 0.01

Onions 348 2 0.6 0.012 - 0.015 0.010 ^ 0.15

Pineapple, Canned 756 0 0.010 - 0.015 0.01

Plums, Dried / Prunes 191 0 0.003 ^ 2.0

Snap Peas 710 0 0.050 ^ 0.01

Sweet Potatoes 701 0 0.015 ^ 0.05

Tomatoes, Canned 566 0 0.020 ^ 0.7

TOTAL 8,399 41

Dioxacarb (insecticide) 

Appendix B. Page 30 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Dioxathion (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Diphenamid (herbicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 397 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 3,707 0

Diphenylamine - DPA (plant growth regulator) 

Applesauce 570 279 48.9 0.002 - 0.12 0.002 ^ 10.0

Asparagus 354 2 0.6 0.004 - 0.007 0.002 ^ V-2 NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 1 0.5 0.021 ^ 0.003 ^ V-1 NT

Grapefruit 271 0 0.003 ^ NT

Lettuce 378 1 0.3 0.004 ^ 0.002 ^ V-1 NT

Mangoes 90 1 1.1 0.001 ^ 0.001 - 0.003 V-1 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.003 - 0.005 NT

Pineapple, Canned 726 0 0.005 - 0.065 NT

Plums, Dried / Prunes 191 18 9.4 0.002 - 0.010 0.002 ^ V-18 NT

Sweet Potatoes 701 0 0.065 ^ NT

Tomatoes, Canned 566 0 0.003 ^ NT

TOTAL 6,230 302

Dipropetryn (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Disulfoton (insecticide) 

Cabbage 354 0 0.005 ^ 0.75

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 - 0.020 NT

Onions 708 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.10 NT

Appendix B. Page 31 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Snap Peas 710 0 0.050 ^ NT

Sweet Potatoes 701 0 0.050 ^ NT

Tomatoes, Canned 566 0 0.002 - 0.005 NT

TOTAL 5,477 0

Disulfoton oxygen analog (metabolite of Disulfoton)

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ 0.1

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 255 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ 0.75/2 &

Mangoes 87 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Pineapple, Canned 359 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

Snap Peas 710 0 0.030 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 5,459 0

Disulfoton sulfone (metabolite of Disulfoton)

Applesauce 570 0 0.020 ^ NT

Asparagus 354 0 0.020 ^ 0.1

Cabbage 354 0 0.010 ^ 0.75

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.020 ^ 0.75/2 &

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

Snap Peas 710 0 0.040 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,970 0

Disulfoton sulfone oxygen analog (metabolite of Disulfoton)

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Onions 360 0 0.003 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Snap Peas 710 0 0.10 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,885 0

Disulfoton sulfoxide (metabolite of Disulfoton)

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ 0.1

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Appendix B. Page 32 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Lettuce 378 0 0.005 ^ 0.75/2 &

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Pineapple, Canned 359 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Snap Peas 710 0 0.020 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,574 0

Disulfoton sulfoxide oxygen analog (metabolite of Disulfoton)

Onions 360 0 0.001 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Snap Peas 710 0 0.040 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,696 0

Ditalimfos (fungicide) 

Mangoes 30 0 0.005 ^ NT

Olives, Canned 61 0 0.005 ^ NT

TOTAL 91 0

Diuron (herbicide) 

Applesauce 570 0 0.002 ^ 0.1

Asparagus 354 2 0.6 0.002 ^ 0.001 - 0.002 7

Cranberries 311 0 0.010 ^ 0.1

Cranberries, Frozen 428 0 0.010 ^ 0.1

Garbanzo Beans, Canned 189 0 0.004 ^ NT

Grapefruit 526 0 0.010 ^ 0.05

Lettuce 378 2 0.5 0.002 - 0.004 0.002 ^ V-2 NT

Mangoes 177 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ 1

Onions 360 0 0.004 - 0.012 NT

Pineapple, Canned 359 0 0.015 ^ 0.1

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.004 ^ NT

TOTAL 5,864 4

DMST (4-dimethylaminosulphotosluidide) (metabolite of Tolyfluanid)

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Dodine (fungicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

TOTAL 1,115 0

Appendix B. Page 33 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Emamectin (insecticide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

TOTAL 1,115 0

Emamectin benzoate 1

 (insecticide) 

Applesauce 570 0 0.010 ^ 0.025

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ 0.050

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Kale 708 12 1.7 0.003 - 0.042 0.002 ^ 0.050

Lettuce 378 0 0.010 ^ 0.100

Onions 320 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ 0.020

TOTAL 4,027 12

Endosulfan I (insecticide) 

Applesauce 570 0 0.010 ^ 1.0

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ 4.0

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.005 ^ 1.0

Garbanzo Beans, Canned 189 0 0.005 ^ 2.0

Grapefruit 526 0 0.010 - 0.020 NT

Kale 708 1 0.1 0.29 ^ 0.004 ^ 2.0

Lettuce 378 0 0.010 ^ 11.0/6.0 &

Mangoes 177 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 - 0.020 NT

Onions 708 0 0.005 ^ NT

Pineapple, Canned 726 0 0.005 - 0.030 1.0

Plums, Dried / Prunes 191 0 0.010 ^ 2.0

Sweet Potatoes 701 0 0.030 ^ 0.15

Tomatoes, Canned 566 2 0.4 0.008 ^ 0.005 ^ 1.0

TOTAL 8,019 3

Endosulfan II (isomer of Endosulfan)

Applesauce 570 0 0.015 ^ 1.0

Asparagus 354 0 0.015 ^ NT

Cabbage 354 0 0.005 ^ 4.0

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 1.0

Garbanzo Beans, Canned 189 0 0.001 ^ 2.0

Grapefruit 526 0 0.005 - 0.010 NT

Kale 708 1 0.1 0.37 ^ 0.012 ^ 2.0

Lettuce 378 0 0.015 ^ 11.0/6.0 &

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 726 0 0.005 - 0.085 1.0

Appendix B. Page 34 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums, Dried / Prunes 191 0 0.015 ^ 2.0

Sweet Potatoes 701 0 0.085 ^ 0.15

Tomatoes, Canned 566 4 0.7 0.002 - 0.007 0.001 ^ 1.0

TOTAL 8,019 5

Endosulfan sulfate (metabolite of Endosulfan)

Applesauce 570 0 0.005 ^ 1.0

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.005 ^ 4.0

Cranberries 310 0 0.015 ^ NT

Cranberries, Frozen 428 0 0.015 ^ NT

Cucumbers 378 2 0.5 0.007 - 0.009 0.005 ^ 1.0

Garbanzo Beans, Canned 189 0 0.005 - 0.018 2.0

Grapefruit 526 0 0.010 - 0.025 NT

Kale 708 7 1 0.003 - 0.39 0.002 ^ 2.0

Lettuce 378 0 0.005 ^ 11.0/6.0 &

Mangoes 177 0 0.003 - 0.015 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 708 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.040 1.0

Plums, Dried / Prunes 191 0 0.005 ^ 2.0

Sweet Potatoes 701 0 0.040 ^ 0.15

Tomatoes, Canned 566 0 0.018 ^ 1.0

TOTAL 8,048 9

EPN (insecticide) 

Grapefruit 271 0 0.020 ^ NT

Kale 708 0 0.005 ^ NT

Mangoes 90 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

Pineapple, Canned 359 0 0.040 ^ NT

Snap Peas 710 0 0.005 ^ NT

Sweet Potatoes 701 0 0.040 ^ NT

TOTAL 3,593 0

Epoxiconazole (fungicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

TOTAL 1,115 0

EPTC (herbicide) 

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 255 0 0.005 ^ 0.1

Mangoes 87 0 0.005 ^ NT

Onions 708 0 0.001 - 0.010 0.1

Pineapple, Canned 756 0 0.010 - 0.035 NT

Sweet Potatoes 701 0 0.035 ^ 0.1

TOTAL 4,167 0

Appendix B. Page 35 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Esfenvalerate+Fenvalerate Total (insecticide) 

Applesauce 570 0 0.005 ^ 1.0

Asparagus 354 0 0.005 ^ 0.05

Cabbage 354 0 0.005 ^ 3.0

Cranberries 311 0 0.050 ^ 0.05

Cranberries, Frozen 428 0 0.050 ^ 0.05

Cucumbers 378 0 0.005 ^ 0.5

Garbanzo Beans, Canned 189 0 0.008 ^ 0.05

Grapefruit 255 0 0.025 ^ 0.05

Lettuce 378 0 0.005 ^ 5.0

Mangoes 87 0 0.050 ^ 0.05

Onions 708 0 0.002 - 0.005 0.05

Pineapple, Canned 397 0 0.005 ^ 0.05

Plums, Dried / Prunes 191 1 0.5 0.007 ^ 0.005 ^ 3.0

Tomatoes, Canned 566 6 1.1 0.004 ^ 0.002 ^ 0.5

TOTAL 5,166 7

Esfenvalerate (isomer of Fenvalerate)

Grapefruit 271 0 0.005 ^ 0.05

Kale 708 5 0.7 0.005 - 0.017 0.003 ^ 0.05

Mangoes 90 0 0.005 ^ 0.05

Olives, Canned 754 0 0.005 ^ 0.05

Pineapple, Canned 359 0 0.035 ^ 0.05

Snap Peas 710 10 1.4 0.005 - 0.030 0.003 ^ 0.5

Sweet Potatoes 701 0 0.035 ^ 0.05

TOTAL 3,593 15

Ethalfluralin (herbicide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.010 ^ NT

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 360 0 0.002 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 5,864 0

Ethiofencarb (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 168 0 0.002 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.002 - 0.010 NT

Appendix B. Page 36 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pineapple, Canned 397 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 - 0.008 NT

TOTAL 3,686 0

Ethiofencarb sulfone (metabolite of Ethiofencarb)

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Ethiofencarb sulfoxide (metabolite of Ethiofencarb)

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Ethion (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.003 - 0.010 NT

Pineapple, Canned 756 0 0.010 - 0.015 NT

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 4,767 0

Ethion mono oxon (metabolite of Ethion)

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Ethiprole (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Ethofumesate (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Pineapple, Canned 359 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 2,175 0

Ethoprop (insecticide) 

Cabbage 354 0 0.010 ^ 0.02

Appendix B. Page 37 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ 0.02

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 0.02

Snap Peas 710 0 0.001 ^ NT

Sweet Potatoes 701 0 0.005 ^ 0.02

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,558 0

Ethoxyquin (plant growth regulator) 

Kale 708 0 0.007 ^ NT

Mangoes 87 0 0.005 ^ NT

Snap Peas 710 0 0.007 ^ NT

TOTAL 1,505 0

Ethylan (insecticide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

TOTAL 1,115 0

Etofenprox (insecticide) 

Applesauce 570 0 0.025 ^ 5.0

Asparagus 354 0 0.025 ^ 5.0

Cranberries 281 0 0.010 ^ 5.0

Cranberries, Frozen 423 0 0.010 ^ 5.0

Garbanzo Beans, Canned 189 0 0.002 ^ 5.0

Grapefruit 526 0 0.010 - 0.020 5.0

Kale 708 2 0.3 0.002 ^ 0.001 ^ 5.0

Lettuce 378 0 0.025 ^ 5.0

Mangoes 177 0 0.001 - 0.020 5.0

Olives, Canned 754 0 0.001 - 0.020 5.0

Onions 360 0 0.002 ^ 5.0

Pineapple, Canned 359 0 0.035 ^ 5.0

Plums, Dried / Prunes 191 0 0.025 ^ 5.0

Snap Peas 710 0 0.001 ^ 5.0

Sweet Potatoes 701 0 0.035 ^ 5.0

Tomatoes, Canned 566 0 0.002 ^ 5.0

TOTAL 7,247 2

Etoxazole (acaricide) 

Cabbage 354 0 0.004 ^ NT

Cranberries 311 0 0.001 ^ 0.50

Cranberries, Frozen 428 0 0.001 ^ 0.50

Cucumbers 378 0 0.004 ^ 0.02

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Mangoes 177 0 0.001 ^ 0.20

Appendix B. Page 38 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.004 ^ NT

Pineapple, Canned 397 0 0.004 ^ NT

Tomatoes, Canned 566 0 0.001 ^ 0.20

TOTAL 4,428 0

Etridiazole (fungicide) 

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.040 NT

Mangoes 177 0 0.005 - 0.040 NT

Olives, Canned 754 0 0.005 - 0.040 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 4,733 0

Etrimfos (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Famoxadone (fungicide) 

Applesauce 570 0 0.025 ^ NT

Asparagus 354 0 0.025 ^ NT

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Garbanzo Beans, Canned 147 0 0.008 ^ NT

Grapefruit 526 0 0.010 - 0.050 NT

Lettuce 378 11 2.9 0.031 - 1.2 0.025 ^ 25

Mangoes 177 0 0.010 - 0.050 NT

Olives, Canned 754 0 0.010 ^ NT

Onions 360 0 0.002 ^ 0.45

Pineapple, Canned 359 0 0.050 ^ NT

Plums, Dried / Prunes 191 0 0.025 ^ NT

Sweet Potatoes 701 0 0.050 ^ NT

Tomatoes, Canned 566 11 1.9 0.004 - 0.014 0.002 - 0.008 1.0

TOTAL 5,822 22

Famphur (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Fenamidone (fungicide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 325 0 0.005 ^ NT

Cabbage 354 1 0.3 0.052 ^ 0.010 ^ 5.0

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Cucumbers 378 0 0.010 ^ 0.15

Appendix B. Page 39 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 1 0.2 0.001 ^ 0.001 ^ V-1 NT

Kale 708 41 5.8 0.008 - 8.7 0.005 ^ 60

Lettuce 378 69 18.3 0.005 - 3.2 0.005 ^ 60

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.010 0.20

Pineapple, Canned 756 0 0.010 - 0.060 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.060 ^ 0.02

Tomatoes, Canned 566 0 0.002 ^ 1.0

TOTAL 8,020 112

Fenamiphos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.010 0.3

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 4,767 0

Fenamiphos sulfone (metabolite of Fenamiphos)

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 756 0 0.005 ^ 0.3

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 4,767 0

Fenamiphos sulfoxide (metabolite of Fenamiphos)

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.010 0.3

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 4,767 0

Fenarimol (fungicide) 

Cabbage 354 0 0.005 ^ NT

Appendix B. Page 40 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 0.20

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.003 - 0.005 NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 726 0 0.005 - 0.015 NT

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 5,818 0

Fenazaquin (insecticide, acaricide)

Applesauce 570 0 0.005 ^ 0.2

Asparagus 89 0 0.005 ^ NT

Cranberries 258 0 0.005 ^ NT

Cranberries, Frozen 417 0 0.005 ^ NT

Grapefruit 526 0 0.001 - 0.010 NT

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

TOTAL 3,360 0

Fenbuconazole (fungicide) 

Applesauce 570 0 0.005 ^ 0.4

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 32 10.3 0.001 - 0.012 0.001 ^ 0.5

Cranberries, Frozen 428 58 13.6 0.001 - 0.036 0.001 ^ 0.5

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.003 1.0

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ 1.0

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 90

Fenchlorphos (insecticide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

TOTAL 1,115 0

Fenhexamid (fungicide) 

Applesauce 570 0 0.013 ^ NT

Asparagus 354 0 0.013 ^ 0.02

Cabbage 354 0 0.010 ^ NT

Appendix B. Page 41 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.010 ^ 5.0

Cranberries, Frozen 428 0 0.010 ^ 5.0

Cucumbers 378 0 0.010 ^ 2.0

Grapefruit 526 0 0.002 - 0.010 NT

Lettuce 378 0 0.013 ^ 30.0

Mangoes 177 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 - 0.015 NT

Plums, Dried / Prunes 191 1 0.5 0.064 ^ 0.013 ^ 2.5

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 62 0 0.030 ^ 2.0

TOTAL 6,288 1

Fenitrothion (insecticide) 

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 360 0 0.002 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 2,230 0

Fenobucarb - BPMC (insecticide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Fenoxaprop ethyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Fenoxycarb (insecticide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Fenpropathrin (insecticide) 

Applesauce 570 0 0.020 ^ 5.0

Asparagus 354 0 0.020 ^ NT

Cabbage 354 0 0.005 ^ 3.0

Cranberries 311 0 0.005 ^ 3.0

Cranberries, Frozen 428 0 0.005 ^ 3.0

Cucumbers 378 3 0.8 0.005 - 0.11 0.005 ^ 0.5

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.005 - 0.010 2.0

Kale 708 1 0.1 0.003 ^ 0.002 ^ V-1 NT

Lettuce 378 0 0.020 ^ NT

Mangoes 177 0 0.001 - 0.005 1.0

Olives, Canned 754 137 18.2 0.001 - 0.16 0.001 - 0.005 5.0

Appendix B. Page 42 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.020 ^ 1.4

Snap Peas 710 0 0.002 ^ 0.02

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 6 1.1 0.004 ^ 0.002 ^ 1.0

TOTAL 8,759 147

Fenpropidin (fungicide) 

Grapefruit 271 0 0.040 ^ NT

Mangoes 90 0 0.040 ^ NT

Olives, Canned 722 0 0.040 ^ NT

TOTAL 1,083 0

Fenpropimorph (fungicide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

TOTAL 4,085 0

Fenpyrazamine (fungicide) 

Cranberries 311 0 0.001 ^ 5

Cranberries, Frozen 428 0 0.001 ^ 5

Grapefruit 271 0 0.020 ^ NT

Mangoes 177 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

TOTAL 1,941 0

Fenpyroximate (acaricide) 

Applesauce 570 0 0.005 ^ 0.30

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 1 0.3 0.016 ^ 0.010 ^ 0.40

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 271 0 0.001 ^ 0.50

Lettuce 378 0 0.005 ^ NT

Mangoes 148 0 0.001 - 0.010 0.15

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

Plums, Dried / Prunes 191 1 0.5 0.006 ^ 0.005 ^ 2.0

Snap Peas 710 1 0.1 0.087 ^ 0.001 ^ V-1 NT

Tomatoes, Canned 566 0 0.003 ^ 0.20

TOTAL 5,608 3

Fensulfothion (insecticide, fumigant)

Appendix B. Page 43 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Fenthion (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.015 NT

Sweet Potatoes 701 0 0.015 ^ NT

TOTAL 3,841 0

Fenthion oxygen analog sulfone (metabolite of Fenthion)

Pineapple, Canned 359 0 0.015 ^ NT

Sweet Potatoes 701 0 0.015 ^ NT

TOTAL 1,060 0

Fenthion oxygen analog sulfoxide (metabolite of Fenthion)

Pineapple, Canned 359 0 0.015 ^ NT

Sweet Potatoes 701 0 0.015 ^ NT

TOTAL 1,060 0

Fenthion sulfone (metabolite of Fenthion)

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

Pineapple, Canned 359 0 0.12 ^ NT

Sweet Potatoes 701 0 0.12 ^ NT

TOTAL 2,175 0

Fenthion sulfoxide (metabolite of Fenthion)

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.010 - 0.020 NT

Olives, Canned 754 0 0.010 - 0.020 NT

Pineapple, Canned 359 0 0.020 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

TOTAL 2,175 0

Fenuron (herbicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Fipronil (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 30 0 0.001 ^ NT

Appendix B. Page 44 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 691 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.020 NT

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 4,644 0

Fipronil sulfone - MB46136 (metabolite of Fipronil)

Applesauce 570 0 0.050 ^ NT

Asparagus 354 0 0.050 ^ NT

Grapefruit 271 0 0.003 ^ NT

Lettuce 378 0 0.050 ^ NT

Mangoes 30 0 0.001 ^ NT

Olives, Canned 691 0 0.001 - 0.003 NT

Plums, Dried / Prunes 191 0 0.050 ^ NT

TOTAL 2,485 0

Flazasulfuron (herbicide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 ^ 0.01

Mangoes 177 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ 0.01

TOTAL 2,196 0

Flonicamid (insecticide) 

Applesauce 570 0 0.006 ^ 0.20

Asparagus 354 0 0.006 ^ NT

Cabbage 354 4 1.1 0.010 - 0.046 0.010 ^ 1.5

Cranberries 311 0 0.050 ^ 1.5

Cranberries, Frozen 428 0 0.050 ^ 1.5

Cucumbers 378 30 7.9 0.011 - 0.32 0.010 ^ 1.5

Garbanzo Beans, Canned 189 0 0.003 ^ 7.0

Grapefruit 526 0 0.010 - 0.10 1.5

Kale 708 37 5.2 0.083 - 4.8 0.050 ^ 16

Lettuce 378 22 5.8 0.006 - 1.0 0.006 ^ 4.0

Mangoes 177 0 0.010 - 0.050 NT

Olives, Canned 754 0 0.010 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.006 ^ 0.60

Sweet Potatoes 701 0 0.005 ^ 0.20

Tomatoes, Canned 566 0 0.001 ^ 0.4

TOTAL 8,049 93

Fluazifop (herbicide) 

Grapefruit 271 0 0.050 ^ 0.03

Olives, Canned 630 0 0.050 ^ NT

TOTAL 901 0

Fluazifop butyl (herbicide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Appendix B. Page 45 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 526 0 0.001 - 0.005 0.03

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 - 0.003 0.5

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 3,311 0

Fluazinam (fungicide) 

Grapefruit 271 0 0.003 ^ NT

Kale 708 0 0.010 ^ 0.01

Olives, Canned 630 0 0.003 ^ NT

Snap Peas 710 0 0.010 ^ 0.10

TOTAL 2,319 0

Flubendiamide (insecticide) 

Applesauce 570 121 21.2 0.004 - 0.015 0.004 ^ 1.5

Cranberries 311 0 0.020 ^ NT

Cranberries, Frozen 428 0 0.020 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ 0.05

Grapefruit 526 0 0.003 ^ NT

Kale 708 21 3 0.005 - 4.2 0.003 ^ 25

Lettuce 282 0 0.004 ^ 11

Mangoes 177 0 0.001 - 0.020 NT

Olives, Canned 691 0 0.001 - 0.003 NT

Plums, Dried / Prunes 191 0 0.004 ^ 1.6

Snap Peas 710 20 2.8 0.005 - 0.25 0.003 ^ 0.50

TOTAL 4,783 162

Flucythrinate (insecticide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

TOTAL 1,115 0

Fludioxonil (fungicide) 

Applesauce 570 80 14 0.026 - 0.37 0.025 ^ 5.0

Asparagus 354 0 0.025 ^ NT

Cabbage 354 0 0.005 ^ 2.0

Cranberries 311 0 0.005 ^ 2.0

Cranberries, Frozen 428 0 0.005 ^ 2.0

Cucumbers 378 2 0.5 0.023 - 0.028 0.005 ^ 0.45

Garbanzo Beans, Canned 189 0 0.006 - 0.020 0.01

Grapefruit 526 15 2.9 0.010 - 0.078 0.010 - 0.020 10

Kale 708 12 1.7 0.020 - 7.3 0.005 - 0.017 10

Lettuce 378 0 0.025 ^ 30

Mangoes 177 0 0.005 - 0.010 5.0

Olives, Canned 754 0 0.010 ^ NT

Onions 708 0 0.005 - 0.006 0.50

Pineapple, Canned 756 0 0.005 - 0.070 20

Plums, Dried / Prunes 191 0 0.025 ^ 5.0

Snap Peas 710 1 0.1 0.008 ^ 0.005 ^ 0.01

Sweet Potatoes 701 161 23 0.066 - 3.0 0.065 - 0.13 6.0

Tomatoes, Canned 566 0 0.006 - 0.020 5.0

TOTAL 8,759 271

Appendix B. Page 46 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fluensulfone (nematicide) 

Kale 708 0 0.040 ^ 9.0

TOTAL 708 0

Flufenacet (herbicide) 

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

TOTAL 2,550 0

Flufenoxuron (insecticide) 

Applesauce 570 0 0.001 ^ 0.50

Asparagus 354 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

TOTAL 2,608 0

Flufenpyr ethyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Flumetsulam (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Flumiclorac pentyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Flumioxazin (herbicide) 

Applesauce 570 0 0.010 ^ 0.02

Asparagus 354 0 0.001 - 0.010 0.02

Cabbage 354 0 0.005 ^ 0.02

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.020 ^ 0.02

Lettuce 378 0 0.001 ^ NT

Mangoes 90 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.001 - 0.020 0.02

Onions 315 0 0.005 - 0.010 0.02

Pineapple, Canned 359 0 0.020 ^ NT

Plums, Dried / Prunes 191 0 0.001 - 0.010 0.02

Appendix B. Page 47 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 701 0 0.050 ^ 0.02

Tomatoes, Canned 566 0 0.002 - 0.005 0.02

TOTAL 5,347 0

Fluometuron (herbicide) 

Cranberries 311 0 0.004 ^ NT

Cranberries, Frozen 428 0 0.004 ^ NT

Grapefruit 526 0 0.002 - 0.003 NT

Mangoes 177 0 0.003 - 0.004 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,196 0

Fluopicolide (fungicide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cabbage 354 4 1.1 0.012 - 0.86 0.010 ^ 5.0

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 43 11.4 0.010 - 0.12 0.010 ^ 0.50

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.002 NT

Kale 708 206 29.1 0.003 - 1.8 0.002 ^ 18

Lettuce 378 10 2.6 0.006 - 0.67 0.005 ^ 25

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.003 - 0.010 7.0

Pineapple, Canned 756 0 0.010 - 0.015 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.015 ^ 0.09

Tomatoes, Canned 566 7 1.2 0.002 - 0.012 0.001 ^ 1.60

TOTAL 8,049 270

Fluopyram (fungicide) 

Applesauce 570 9 1.6 0.005 - 0.011 0.005 ^ 0.80

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.010 ^ 4.0

Cranberries 311 0 0.002 ^ 7.0

Cranberries, Frozen 428 0 0.002 ^ 7.0

Cucumbers 378 14 3.7 0.011 - 0.099 0.010 ^ 0.60

Garbanzo Beans, Canned 189 0 0.001 ^ 0.20

Grapefruit 526 0 0.001 - 0.002 1.0

Kale 708 58 8.2 0.003 - 2.5 0.002 ^ 50

Lettuce 378 2 0.5 0.008 - 0.009 0.005 ^ 40

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ 0.40

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 1 0.5 0.046 ^ 0.005 ^ 0.50

Snap Peas 710 2 0.3 0.003 - 0.036 0.002 ^ 4.0

Sweet Potatoes 701 1 0.1 0.007 ^ 0.005 ^ 0.10

TOTAL 7,833 87

Fluorodifen (herbicide) 

Appendix B. Page 48 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Fluoxastrobin (fungicide) 

Cabbage 354 0 0.002 ^ NT

Cranberries 311 0 0.001 ^ 1.9

Cranberries, Frozen 428 0 0.001 ^ 1.9

Cucumbers 378 6 1.6 0.003 - 0.008 0.002 ^ 0.50

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.003 NT

Pineapple, Canned 756 0 0.002 - 0.015 NT

Sweet Potatoes 701 0 0.015 ^ 0.010

Tomatoes, Canned 566 0 0.001 ^ 1.0

TOTAL 5,848 6

Flupyradifurone (insecticide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 1 0.2 0.003 ^ 0.001 - 0.020 3.0

Kale 708 49 6.9 0.050 - 3.8 0.030 ^ 40

Mangoes 177 0 0.001 - 0.005 0.60

Olives, Canned 754 0 0.001 ^ 0.60

Snap Peas 710 0 0.030 ^ 3.0

TOTAL 3,803 50

Fluquinconazole (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Grapefruit 271 0 0.003 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

TOTAL 3,707 0

Fluridone (herbicide) 

Applesauce 570 0 0.001 ^ 0.1

Asparagus 354 0 0.001 ^ NT

Cabbage 354 0 0.010 ^ 0.1

Cranberries 311 0 0.002 ^ 0.1

Cranberries, Frozen 428 0 0.002 ^ 0.1

Cucumbers 378 0 0.010 ^ 0.1

Garbanzo Beans, Canned 189 0 0.001 ^ 0.1

Grapefruit 526 0 0.001 ^ 0.1

Kale 708 0 0.002 ^ 0.1

Lettuce 378 0 0.001 ^ 0.1

Appendix B. Page 49 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 26 3.4 0.001 - 0.002 0.001 ^ V-26 NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.001 ^ 0.1

Snap Peas 710 0 0.002 ^ 0.1

Sweet Potatoes 701 0 0.005 ^ 0.1

Tomatoes, Canned 566 0 0.001 ^ 0.1

TOTAL 8,759 26

Fluroxypyr (herbicide metabolite)

Grapefruit 271 0 0.050 ^ NT

Olives, Canned 630 0 0.050 ^ NT

TOTAL 901 0

Flusilazole (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 5,145 0

Fluthiacet methyl (herbicide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.003 - 0.005 NT

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,196 0

Flutolanil (fungicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.001 - 0.002 NT

Grapefruit 271 0 0.001 ^ NT

Kale 708 0 0.004 ^ 0.1

Lettuce 378 0 0.002 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

TOTAL 3,316 0

Flutriafol (fungicide) 

Applesauce 570 0 0.010 ^ 0.40

Asparagus 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Appendix B. Page 50 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 428 0 0.002 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.025 NT

Kale 708 2 0.3 0.52 - 0.93 0.006 ^ 7.0

Lettuce 378 0 0.010 ^ 1.5/10 &

Mangoes 177 8 4.5 0.002 - 0.011 0.001 - 0.002 V-8 NT

Olives, Canned 754 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ 1.5

TOTAL 4,586 10

Fluvalinate (insecticide) 

Applesauce 570 0 0.050 ^ NT

Asparagus 354 0 0.050 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 467 0 0.005 - 0.010 NT

Kale 708 0 0.002 ^ NT

Lettuce 378 0 0.050 ^ NT

Mangoes 147 0 0.010 - 0.050 NT

Olives, Canned 754 0 0.001 - 0.010 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.035 NT

Plums, Dried / Prunes 191 0 0.050 ^ NT

Snap Peas 710 0 0.002 ^ NT

Sweet Potatoes 701 0 0.035 ^ NT

TOTAL 7,555 0

Fluxapyroxad (fungicide) 

Cranberries 311 0 0.005 ^ 7.0

Cranberries, Frozen 428 0 0.005 ^ 7.0

Garbanzo Beans, Canned 189 0 0.001 ^ 0.5

Grapefruit 526 0 0.001 - 0.005 1.0

Kale 708 30 4.2 0.005 - 1.9 0.003 ^ 4.0

Mangoes 177 0 0.001 - 0.005 0.7

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ 1.5

Pineapple, Canned 359 0 0.010 ^ NT

Snap Peas 710 0 0.003 ^ 2.0

Sweet Potatoes 701 0 0.010 ^ 0.02

Tomatoes, Canned 566 67 11.8 0.002 - 0.030 0.001 ^ 0.7

TOTAL 5,789 97

Folpet (fungicide) 

Applesauce 536 0 0.030 - 0.060 5.0

Asparagus 235 0 0.030 ^ NT

Cranberries 311 0 0.005 ^ 15.0

Cranberries, Frozen 428 0 0.005 ^ 15.0

Cucumbers 292 0 0.015 ^ 2.0

Mangoes 87 0 0.005 ^ NT

Onions 348 0 0.015 ^ 2.0

Pineapple, Canned 397 0 0.015 ^ NT

TOTAL 2,634 0

Appendix B. Page 51 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fomesafen (herbicide) 

Grapefruit 271 0 0.005 ^ NT

Olives, Canned 630 0 0.005 ^ NT

Snap Peas 710 0 0.030 ^ 0.025

TOTAL 1,611 0

Fonofos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.030 NT

Sweet Potatoes 701 0 0.030 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 4,767 0

Forchlorfenuron (plant growth regulator) 

Cabbage 354 0 0.002 ^ NT

Cranberries 311 0 0.001 ^ 0.01

Cranberries, Frozen 428 0 0.001 ^ 0.01

Cucumbers 378 0 0.002 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.002 ^ NT

Pineapple, Canned 397 0 0.002 ^ NT

TOTAL 3,418 0

Formetanate hydrochloride (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ 1.5

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,652 0

Fosthiazate (nematicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Furalaxyl (fungicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.005 - 0.010 NT

TOTAL 1,115 0

Appendix B. Page 52 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Furathiocarb (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 1,477 0

Halosulfuron (herbicide) 

Cranberries 311 0 0.010 ^ 0.05

Cranberries, Frozen 428 0 0.010 ^ 0.05

Grapefruit 255 0 0.005 ^ NT

Mangoes 87 0 0.010 ^ NT

Pineapple, Canned 359 0 0.050 ^ NT

Sweet Potatoes 701 0 0.055 ^ 0.05

TOTAL 2,141 0

Halosulfuron methyl 2

 (herbicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ 0.5

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 691 0 0.001 - 0.020 NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,529 0

Haloxyfop (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Olives, Canned 630 0 0.020 ^ NT

TOTAL 901 0

Heptenophos (insecticide, acaricide)

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

TOTAL 1,115 0

Hexaconazole (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,592 0

Hexazinone (herbicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Pineapple, Canned 359 0 0.005 ^ 0.6

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 2,175 0

Appendix B. Page 53 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Hexythiazox (insecticide, acaricide)

Applesauce 570 0 0.002 ^ 0.4

Asparagus 354 0 0.002 ^ NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ 0.3

Grapefruit 526 0 0.001 - 0.30 0.6

Lettuce 378 0 0.002 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 - 0.015 NT

Plums, Dried / Prunes 191 9 4.7 0.002 - 0.035 0.002 ^ 1.3

Sweet Potatoes 701 0 0.015 ^ NT

TOTAL 5,589 9

Hydroprene (insect growth regulator) 

Cranberries 311 0 0.005 ^ 0.2

Cranberries, Frozen 428 0 0.005 ^ 0.2

Garbanzo Beans, Canned 189 0 0.002 ^ 0.2

Grapefruit 526 0 0.010 - 0.020 0.2

Kale 708 0 0.015 ^ 0.2

Mangoes 177 0 0.003 - 0.020 0.2

Olives, Canned 754 0 0.003 - 0.020 0.2

Onions 360 0 0.002 ^ 0.2

Pineapple, Canned 359 0 0.015 ^ 0.2

Snap Peas 710 0 0.015 ^ 0.2

Sweet Potatoes 701 0 0.015 ^ 0.2

Tomatoes, Canned 566 0 0.002 ^ 0.2

TOTAL 5,789 0

3-Hydroxycarbofuran (metabolite of Carbofuran)

Applesauce 570 0 0.003 ^ NT

Asparagus 354 2 0.6 0.003 - 0.035 0.003 ^ V-2 NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.004 ^ NT

Cranberries, Frozen 428 0 0.004 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.004 NT

Kale 708 0 0.050 ^ NT

Lettuce 378 0 0.003 ^ NT

Mangoes 177 0 0.001 - 0.004 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.004 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.003 ^ NT

Snap Peas 710 0 0.050 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 - 0.004 NT

TOTAL 8,759 2

5-Hydroxythiabendazole (metabolite of Thiabendazole)

Appendix B. Page 54 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 271 2 0.7 0.002 - 0.005 0.001 ^ 10.0

Mangoes 90 15 16.7 0.001 - 0.003 0.001 ^ 10.0

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 17

Imazalil (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 309 0 0.005 ^ NT

Cranberries, Frozen 409 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 450 85.6 0.001 - 0.21 0.001 - 0.003 10.0

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.003 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,320 450

Imazapic (herbicide) 

Grapefruit 121 0 0.005 ^ NT

Olives, Canned 630 0 0.005 ^ NT

TOTAL 751 0

Imazapyr (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Olives, Canned 630 0 0.020 ^ NT

TOTAL 901 0

Imazaquin (herbicide) 

Grapefruit 271 0 0.010 ^ NT

Olives, Canned 630 0 0.010 ^ NT

TOTAL 901 0

Imazethapyr (herbicide) 

Applesauce 570 0 0.020 ^ NT

Asparagus 354 0 0.020 - 20 NT

Grapefruit 271 0 0.020 ^ NT

Olives, Canned 630 0 0.020 ^ NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

Snap Peas 710 0 0.050 ^ 0.1

TOTAL 2,726 0

Imazosulfuron (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Sweet Potatoes 701 0 0.025 ^ 0.02

TOTAL 1,816 0

Appendix B. Page 55 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Imidacloprid (insecticide) 

Applesauce 570 47 8.2 0.003 - 0.025 0.003 ^ 0.5

Asparagus 354 8 2.3 0.004 - 0.092 0.003 ^ V-8 NT

Cabbage 354 28 7.9 0.010 - 0.063 0.010 ^ 3.5

Cranberries 311 0 0.005 ^ 0.05

Cranberries, Frozen 428 0 0.005 ^ 0.05

Cucumbers 378 6 1.6 0.011 - 0.067 0.010 ^ 0.5

Garbanzo Beans, Canned 189 0 0.001 ^ 4.0

Grapefruit 526 87 16.5 0.003 - 0.020 0.003 - 0.005 0.70

Lettuce 378 153 40.5 0.003 - 0.087 0.003 ^ 3.5

Mangoes 177 25 14.1 0.003 - 0.032 0.003 - 0.005 1.0

Olives, Canned 754 0 0.003 ^ NT

Onions 708 48 6.8 0.002 - 0.016 0.001 - 0.010 0.15

Pineapple, Canned 756 0 0.010 - 0.020 NT

Plums, Dried / Prunes 191 5 2.6 0.003 - 0.018 0.003 ^ 3.0

Snap Peas 710 3 0.4 0.067 - 0.17 0.040 ^ 4.0

Sweet Potatoes 701 0 0.020 ^ 0.40

Tomatoes, Canned 566 169 29.9 0.002 - 0.018 0.001 ^ 1.0

TOTAL 8,051 579

Imidacloprid urea (metabolite of Imidacloprid)

Pineapple, Canned 359 0 0.015 ^ NT

Sweet Potatoes 701 0 0.015 ^ 0.40

TOTAL 1,060 0

Imiprothrin (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 526 0 0.010 - 0.040 NT

Kale 708 0 0.007 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.010 - 0.050 NT

Olives, Canned 754 0 0.010 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 - 0.095 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Snap Peas 710 0 0.007 ^ NT

Sweet Potatoes 701 0 0.095 ^ NT

TOTAL 7,644 0

Indaziflam (herbicide) 

Applesauce 570 0 0.001 ^ 0.01

Asparagus 354 0 0.001 ^ NT

Cranberries 311 0 0.001 ^ 0.01

Cranberries, Frozen 428 0 0.001 ^ 0.01

Grapefruit 526 0 0.001 ^ 0.01

Lettuce 378 0 0.001 ^ NT

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ 0.01

Appendix B. Page 56 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Plums, Dried / Prunes 191 0 0.001 ^ 0.01

TOTAL 3,689 0

Indoxacarb (insecticide) 

Applesauce 570 0 0.020 ^ 1.0

Asparagus 354 0 0.020 ^ NT

Cabbage 354 5 1.4 0.010 - 0.28 0.010 ^ 12

Cranberries 311 0 0.050 ^ 1.5

Cranberries, Frozen 428 0 0.050 ^ 1.5

Cucumbers 378 0 0.010 ^ 0.60

Grapefruit 496 0 0.005 - 0.010 NT

Kale 708 70 9.9 0.005 - 2.5 0.003 ^ 12

Lettuce 378 0 0.020 ^ 14

Mangoes 177 0 0.005 - 0.050 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 - 0.025 NT

Plums, Dried / Prunes 191 0 0.020 ^ 0.90

Sweet Potatoes 701 0 0.025 ^ 0.01

TOTAL 6,904 75

Ipconazole (fungicide) 

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Grapefruit 408 0 0.003 - 0.020 NT

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

Snap Peas 710 0 0.005 ^ 0.01

TOTAL 2,788 0

Iprobenfos - IBP (fungicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Iprodione (fungicide) 

Applesauce 570 0 0.040 ^ NT

Asparagus 354 0 0.040 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.075 ^ NT

Cranberries, Frozen 428 0 0.075 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.009 ^ NT

Grapefruit 526 0 0.010 - 0.15 NT

Lettuce 378 0 0.040 ^ 25.0

Mangoes 177 0 0.005 - 0.075 NT

Olives, Canned 754 0 0.005 - 0.010 NT

Onions 708 1 0.1 0.010 ^ 0.005 - 0.009 0.5

Pineapple, Canned 756 0 0.005 - 0.025 NT

Plums, Dried / Prunes 191 0 0.040 ^ 20.0

Sweet Potatoes 701 0 0.025 ^ NT

Tomatoes, Canned 545 0 0.009 ^ NT

TOTAL 7,320 1

Appendix B. Page 57 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Iprovalicarb (fungicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 2,175 0

Isocarbophos (insecticide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

TOTAL 1,115 0

Isofenphos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,469 0

Isofenphos methyl (metabolite if Isofenphos)

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

TOTAL 1,115 0

Isofetamid (fungicide) 

Cranberries 311 0 0.001 ^ 5.0

Cranberries, Frozen 428 0 0.001 ^ 5.0

Mangoes 87 0 0.001 ^ NT

TOTAL 826 0

Isoprocarb (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Isoprothiolane (fungicide) 

Cabbage 354 0 0.005 ^ NT

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 445 0

Isoproturon (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Isoxadifen ethyl (herbicide safener) 

Cranberries 311 0 0.005 ^ NT

Appendix B. Page 58 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

TOTAL 2,196 0

Kresoxim-methyl (fungicide) 

Applesauce 570 0 0.010 ^ 0.5

Asparagus 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.005 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 360 0 0.002 ^ NT

Pineapple, Canned 359 0 0.015 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 5,864 0

Lactofen (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Snap Peas 710 0 0.004 ^ NT

TOTAL 1,825 0

Lenacil (herbicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 60 0 0.003 ^ NT

Olives, Canned 661 0 0.003 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 2,469 0

Leptophos oxygen analog (insecticide metabolite)

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Linuron (herbicide) 

Asparagus 354 6 1.7 0.008 - 0.066 0.008 ^ 7

Cabbage 354 0 0.019 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.019 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.003 - 0.016 NT

Appendix B. Page 59 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.002 - 0.019 NT

Pineapple, Canned 756 0 0.010 - 0.019 NT

Plums, Dried / Prunes 191 0 0.008 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 6,393 6

Lufenuron (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Olives, Canned 630 0 0.005 ^ NT

Pineapple, Canned 359 0 0.005 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 1,961 0

Malathion (insecticide) 

Applesauce 570 0 0.002 ^ 8

Asparagus 354 0 0.002 ^ 8

Cabbage 354 0 0.010 ^ 8

Cranberries 311 0 0.010 ^ 8

Cranberries, Frozen 428 0 0.010 ^ 8

Cucumbers 378 0 0.010 ^ 8

Garbanzo Beans, Canned 189 0 0.001 ^ 8

Grapefruit 526 0 0.003 - 0.005 8

Kale 708 8 1.1 0.008 - 1.0 0.005 ^ 8

Lettuce 378 1 0.3 0.035 ^ 0.002 ^ 8

Mangoes 177 7 4 0.003 - 0.013 0.003 - 0.010 8

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.003 - 0.010 8

Pineapple, Canned 756 0 0.005 - 0.010 8

Plums, Dried / Prunes 191 0 0.002 ^ 8

Sweet Potatoes 701 0 0.005 ^ 1

Tomatoes, Canned 566 0 0.001 ^ 8

TOTAL 8,049 16

Malathion oxygen analog (metabolite of Malathion)

Applesauce 570 0 0.002 ^ 8

Asparagus 354 0 0.002 ^ 8

Cabbage 354 0 0.010 ^ 8

Cranberries 311 0 0.002 ^ 8

Cranberries, Frozen 428 0 0.002 ^ 8

Cucumbers 378 0 0.010 ^ 8

Garbanzo Beans, Canned 189 0 0.002 ^ 8

Grapefruit 526 0 0.001 ^ 8

Kale 708 0 0.015 ^ 8

Lettuce 378 0 0.002 ^ 8

Mangoes 177 0 0.001 - 0.002 8

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.010 8

Pineapple, Canned 756 0 0.005 - 0.010 8

Plums, Dried / Prunes 191 0 0.002 ^ 8

Sweet Potatoes 701 0 0.005 ^ 1

Appendix B. Page 60 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomatoes, Canned 566 0 0.002 ^ 8

TOTAL 8,049 0

Mandipropamid (fungicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cabbage 354 2 0.6 0.006 - 0.015 0.005 ^ 3

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 2 0.5 0.005 - 0.009 0.005 ^ 0.6

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 526 0 0.001 - 0.003 NT

Kale 708 130 18.4 0.008 - 11.5 0.005 ^ 25

Lettuce 378 49 13 0.002 - 3.1 0.002 ^ 20

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.003 - 0.010 0.05

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 0 0.020 ^ 0.09

Tomatoes, Canned 566 3 0.5 0.005 ^ 0.003 ^ 1.0

TOTAL 8,049 186

Mecarbam (insecticide, acaricide)

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

TOTAL 1,115 0

Mecoprop - MCPP (herbicide) 

Grapefruit 271 0 0.25 ^ NT

Olives, Canned 630 0 0.25 ^ NT

TOTAL 901 0

Mefenacet (herbicide) 

Cabbage 354 0 0.005 ^ NT

TOTAL 354 0

Mefenpyr diethyl (herbicide safener) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Mepanipyrim (fungicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 - 0.003 NT

TOTAL 1,115 0

Mephosfolan (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

Appendix B. Page 61 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

TOTAL 91 0

Mesotrione (herbicide) 

Cranberries 311 0 0.050 ^ 0.02

Cranberries, Frozen 428 0 0.050 ^ 0.02

Grapefruit 255 0 0.010 ^ 0.01

TOTAL 994 0

Metaflumizone (insecticide) 

Cranberries 278 0 0.002 ^ NT

Cranberries, Frozen 373 0 0.002 ^ NT

Grapefruit 526 0 0.001 - 0.010 0.04

Mangoes 119 0 0.002 - 0.010 NT

Olives, Canned 754 0 0.010 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Sweet Potatoes 701 0 0.005 - 0.010 NT

TOTAL 3,110 0

Metalaxyl/Mefenoxam 3

 (fungicide) 

Applesauce 570 0 0.001 ^ 0.2

Asparagus 354 0 0.001 ^ 7

Cabbage 354 0 0.005 ^ 1

Cranberries 311 0 0.010 ^ 4.0

Cranberries, Frozen 428 0 0.010 ^ 4.0

Cucumbers 378 98 25.9 0.005 - 0.32 0.005 ^ 1.0

Garbanzo Beans, Canned 189 0 0.001 ^ 0.2

Grapefruit 526 0 0.001 - 0.005 1.0

Kale 708 47 6.6 0.007 - 2.6 0.004 ^ X-4 0.1

Lettuce 378 28 7.4 0.001 - 0.009 0.001 ^ 5.0

Mangoes 177 0 0.001 - 0.010 0.40

Olives, Canned 754 0 0.001 ^ NT

Onions 708 17 2.4 0.002 - 0.031 0.001 - 0.005 3.0

Pineapple, Canned 756 0 0.005 - 0.030 0.1

Plums, Dried / Prunes 191 0 0.001 ^ 4.0

Snap Peas 710 4 0.6 0.007 - 0.029 0.004 ^ 0.2

Sweet Potatoes 701 0 0.030 ^ 0.5

Tomatoes, Canned 566 4 0.7 0.002 - 0.006 0.001 ^ 1.0

TOTAL 8,759 198

Metaldehyde (molluscicide) 

Grapefruit 271 0 0.10 ^ 0.26

Kale 708 0 0.040 ^ 2.5

Mangoes 60 0 0.10 ^ NT

Olives, Canned 661 0 0.10 ^ NT

Pineapple, Canned 359 0 0.11 ^ NT

Snap Peas 710 0 0.040 ^ 0.80

Sweet Potatoes 701 0 0.11 ^ NT

TOTAL 3,470 0

Metconazole (fungicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Appendix B. Page 62 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pineapple, Canned 359 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ 0.04

TOTAL 2,175 0

Methacrifos (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Methamidophos (insecticide) (also a metabolite of Acephate)

Applesauce 570 0 0.005 ^ 0.02

Asparagus 354 7 2 0.022 - 0.83 0.005 ^ X-4 0.02

Cabbage 354 1 0.3 0.017 ^ 0.010 ^ 0.02

Cranberries 311 0 0.020 ^ 0.5

Cranberries, Frozen 428 0 0.020 ^ 0.5

Cucumbers 378 1 0.3 0.11 ^ 0.010 ^ X-1 0.02

Garbanzo Beans, Canned 189 0 0.004 ^ 0.02

Grapefruit 526 0 0.001 - 0.020 0.02

Kale 708 0 0.050 ^ 0.02

Lettuce 378 2 0.5 0.005 - 0.006 0.005 ^ 10/0.02 &

Mangoes 177 0 0.001 - 0.020 0.02

Olives, Canned 754 0 0.001 ^ 0.02

Onions 708 0 0.001 - 0.010 0.02

Pineapple, Canned 756 0 0.010 - 0.035 0.02

Plums, Dried / Prunes 191 0 0.005 ^ 0.02

Snap Peas 710 0 0.050 ^ 0.02

Sweet Potatoes 701 0 0.035 ^ 0.02

Tomatoes, Canned 566 0 0.004 ^ 0.02

TOTAL 8,759 11

Methidathion (insecticide) 

Applesauce 570 0 0.010 ^ 0.05

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.003 4.0

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.002 - 0.003 0.05

Olives, Canned 754 0 0.003 ^ 0.05

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.010 - 0.015 NT

Plums, Dried / Prunes 191 0 0.010 ^ 0.05

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.001 - 0.003 NT

TOTAL 7,341 0

Methiocarb (insecticide)

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Appendix B. Page 63 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 603 0 0.001 - 0.010 NT

Pineapple, Canned 397 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 - 0.003 NT

TOTAL 3,602 0

Methiocarb sulfone (metabolite of Methiocarb)

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Methiocarb sulfoxide (metabolite of Methiocarb)

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Methomyl (insecticide) 

Applesauce 570 0 0.030 ^ 1

Asparagus 323 2 0.6 0.035 - 0.43 0.030 ^ 2

Cabbage 354 4 1.1 0.010 - 0.029 0.010 ^ 5

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 2 0.5 0.14 - 0.68 0.010 ^ X-1 0.2

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.001 - 0.010 2

Kale 708 5 0.7 0.042 - 1.6 0.025 ^ 6

Lettuce 378 5 1.3 0.036 - 0.13 0.030 ^ 5

Mangoes 177 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.010 ^ NT

Onions 708 2 0.3 0.004 - 0.014 0.002 - 0.010 V-2 NT

Pineapple, Canned 756 0 0.010 - 0.015 NT

Plums, Dried / Prunes 191 0 0.030 ^ NT

Sweet Potatoes 701 0 0.015 ^ 0.2

Tomatoes, Canned 566 0 0.002 ^ 1

TOTAL 8,018 20

Methomyl oxime (metabolite of Methomyl)

Grapefruit 255 0 0.050 ^ 2

TOTAL 255 0

Methoprene (insect growth regulator) 

Garbanzo Beans, Canned 189 0 0.015 ^ EX

Grapefruit 255 0 0.050 ^ EX

Onions 360 0 0.015 ^ EX

Pineapple, Canned 359 0 0.030 ^ EX

Sweet Potatoes 701 0 0.030 ^ EX

Tomatoes, Canned 566 0 0.015 ^ EX

TOTAL 2,430 0

Methoxychlor Total (insecticide) 

Appendix B. Page 64 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 330 0 0.001 - 0.006 NT

Pineapple, Canned 329 0 0.040 ^ NT

Sweet Potatoes 701 0 0.040 ^ NT

Tomatoes, Canned 545 0 0.001 - 0.003 NT

TOTAL 1,905 0

Methoxychlor olefin (metabolite of Methoxychlor)

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 1,115 0

Methoxychlor p,p' (isomer of Methoxychlor)

Cabbage 354 0 0.005 ^ NT

Cucumbers 312 0 0.005 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 2,526 0

Methoxyfenozide (insecticide) 

Applesauce 570 16 2.8 0.004 - 0.010 0.003 ^ 2.0

Asparagus 354 0 0.003 ^ NT

Cabbage 354 0 0.010 ^ 7.0

Cranberries 311 9 2.9 0.002 - 0.006 0.002 ^ 3.0

Cranberries, Frozen 428 88 20.6 0.002 - 0.016 0.002 ^ 3.0

Cucumbers 378 2 0.5 0.016 - 0.038 0.010 ^ 0.3

Garbanzo Beans, Canned 189 0 0.001 ^ 0.2

Grapefruit 526 0 0.002 - 0.003 3.0

Kale 708 80 11.3 0.017 - 12.9 0.010 ^ 30

Lettuce 378 6 1.6 0.003 - 0.36 0.003 ^ 30

Mangoes 177 0 0.002 - 0.003 0.6

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.001 - 0.010 0.10

Pineapple, Canned 756 0 0.010 ^ 0.70

Plums, Dried / Prunes 191 27 14.1 0.003 - 0.088 0.003 ^ 0.30

Snap Peas 710 5 0.7 0.017 - 0.10 0.010 ^ 1.5

Sweet Potatoes 701 0 0.010 ^ 0.02

Tomatoes, Canned 566 18 3.2 0.002 - 0.008 0.001 ^ 2.0

TOTAL 8,759 251

Metolachlor (herbicide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ 0.1

Cabbage 354 0 0.005 ^ 0.6

Cranberries 311 0 0.005 ^ 0.15

Cranberries, Frozen 428 0 0.005 ^ 0.15

Cucumbers 378 0 0.005 ^ 0.50

Garbanzo Beans, Canned 189 0 0.001 ^ 0.30

Grapefruit 526 0 0.003 - 0.010 NT

Kale 708 0 0.002 ^ 1.8

Lettuce 378 0 0.001 ^ 1.5

Appendix B. Page 65 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 0.10

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

Snap Peas 710 0 0.002 ^ 0.30

Sweet Potatoes 701 0 0.010 ^ 0.20

Tomatoes, Canned 566 3 0.5 0.002 ^ 0.001 ^ 0.10

TOTAL 8,759 3

Metolcarb (insecticide, acaricide)

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

TOTAL 1,115 0

Metrafenone (fungicide) 

Cabbage 354 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,214 0

Metribuzin (herbicide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 14 4 0.005 - 0.10 0.005 ^ 0.1

Cranberries 278 0 0.005 ^ NT

Cranberries, Frozen 426 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.005 ^ NT

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 360 0 0.002 ^ NT

Pineapple, Canned 359 0 0.020 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 4 0.7 0.003 ^ 0.002 ^ 0.1

TOTAL 5,829 18

Metsulfuron methyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Mevinphos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.002 - 0.003 NT

Appendix B. Page 66 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 5,848 0

MGK-264 (insecticide) 

Applesauce 570 0 0.10 ^ 5

Asparagus 354 0 0.10 ^ 5

Cranberries 311 0 0.025 ^ 5

Cranberries, Frozen 428 0 0.025 ^ 5

Garbanzo Beans, Canned 189 3 1.6 0.003 ^ 0.002 ^ 5

Grapefruit 526 0 0.005 ^ 5

Kale 708 0 0.001 ^ 5

Lettuce 378 0 0.10 ^ 5

Mangoes 177 0 0.001 - 0.025 5

Olives, Canned 754 0 0.001 - 0.005 5

Onions 360 0 0.002 ^ 5

Pineapple, Canned 359 0 0.030 ^ 5

Plums, Dried / Prunes 191 0 0.10 ^ 5

Snap Peas 710 0 0.001 ^ 5

Sweet Potatoes 701 0 0.030 ^ 5

Tomatoes, Canned 566 0 0.002 ^ 5

TOTAL 7,282 3

Molinate (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Monocrotophos (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 - 0.020 NT

Sweet Potatoes 701 0 0.020 ^ NT

TOTAL 3,652 0

Monolinuron (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Myclobutanil (fungicide) 

Applesauce 570 2 0.4 0.003 - 0.005 0.003 ^ 0.5

Asparagus 354 0 0.003 ^ 0.02

Cabbage 354 0 0.005 ^ 0.03

Appendix B. Page 67 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 15 4 0.006 - 0.077 0.005 ^ 0.20

Garbanzo Beans, Canned 189 0 0.001 ^ 0.03

Grapefruit 526 0 0.003 - 0.010 NT

Lettuce 378 0 0.003 ^ 9.0

Mangoes 177 0 0.003 - 0.010 3.0

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.001 - 0.005 NT

Plums, Dried / Prunes 191 0 0.003 ^ 8.0

Snap Peas 710 1 0.1 0.008 ^ 0.005 ^ 0.03

Sweet Potatoes 701 0 0.001 ^ 0.03

Tomatoes, Canned 566 3 0.5 0.005 - 0.008 0.003 ^ 0.30

TOTAL 8,051 21

Naled (insecticide) 

Applesauce 570 0 0.020 ^ 0.5

Kale 708 0 0.025 ^ 3

Lettuce 378 0 0.020 ^ 0.5

Plums, Dried / Prunes 191 0 0.020 ^ 0.5

Snap Peas 710 0 0.025 ^ 0.5

TOTAL 2,557 0

1-Naphthol (metabolite of Carbaryl)

Applesauce 570 4 0.7 0.016 - 0.074 0.015 ^ 12

Asparagus 298 0 0.015 ^ 15

Cranberries 311 9 2.9 0.010 - 0.10 0.010 ^ 3.0

Cranberries, Frozen 426 2 0.5 0.033 - 0.11 0.010 ^ 3.0

Grapefruit 255 0 0.010 ^ 10

Kale 708 3 0.4 0.042 - 0.15 0.025 ^ 10

Lettuce 378 0 0.015 ^ 10

Mangoes 87 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.015 ^ 10

Snap Peas 710 0 0.025 ^ 10

TOTAL 3,934 18

Napropamide (herbicide) 

Cabbage 354 0 0.010 ^ 0.1

Cranberries 311 0 0.001 ^ 0.1

Cranberries, Frozen 428 0 0.001 ^ 0.1

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.005 ^ NT

Kale 708 0 0.003 ^ 0.1

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 722 0 0.003 - 0.005 NT

Onions 708 0 0.002 - 0.010 NT

Pineapple, Canned 756 0 0.010 - 0.020 NT

Sweet Potatoes 701 0 0.020 ^ 0.1

Tomatoes, Canned 566 0 0.002 ^ 0.1

TOTAL 6,269 0

Nicosulfuron (herbicide) 

Appendix B. Page 68 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 2,109 0

Nitrapyrin (nitrification inhibitor) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.020 NT

Mangoes 177 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.001 - 0.020 NT

TOTAL 2,196 0

Nitrofen (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.001 - 0.020 NT

TOTAL 1,115 0

Norflurazon (herbicide) 

Applesauce 570 0 0.002 ^ 0.1

Asparagus 354 0 0.001 - 0.002 0.05

Cabbage 354 0 0.010 ^ NT

Cranberries 208 0 0.010 ^ 0.1

Cranberries, Frozen 418 0 0.010 ^ 0.1

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.003 - 0.005 0.2

Lettuce 378 0 0.002 ^ NT

Mangoes 148 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.002 ^ 0.1

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,199 0

Norflurazon desmethyl (metabolite of Norflurazon)

Applesauce 570 0 0.005 ^ 0.1

Asparagus 354 0 0.005 ^ 0.05

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ 0.1

Cranberries, Frozen 428 1 0.2 0.007 ^ 0.005 ^ 0.1

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.003 0.2

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.001 - 0.010 NT

Appendix B. Page 69 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ 0.1

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 1

Novaluron (insecticide) 

Asparagus 354 0 0.008 - 0.009 0.01

Cabbage 354 0 0.010 ^ 0.50

Cranberries 311 0 0.005 ^ 7.0

Cranberries, Frozen 428 9 2.1 0.012 - 0.032 0.005 ^ 7.0

Cucumbers 378 0 0.010 ^ 0.20

Garbanzo Beans, Canned 189 0 0.001 - 0.003 0.01

Grapefruit 526 0 0.020 - 0.050 0.01

Kale 708 1 0.1 0.48 ^ 0.010 ^ 25

Mangoes 177 0 0.001 - 0.005 0.01

Olives, Canned 691 0 0.001 - 0.020 0.01

Onions 708 0 0.001 - 0.010 0.01

Pineapple, Canned 756 0 0.010 ^ 0.01

Plums, Dried / Prunes 191 0 0.009 ^ 3.0

Snap Peas 710 0 0.010 ^ 0.01

Sweet Potatoes 701 0 0.010 ^ 0.05

Tomatoes, Canned 566 0 0.001 - 0.003 1.0

TOTAL 7,748 10

Omethoate (insecticide) (also a metabolite of Dimethoate)

Applesauce 570 0 0.020 ^ NT

Asparagus 354 2 0.6 0.025 - 0.28 0.020 ^ X-1 0.15

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.015 ^ NT

Cranberries, Frozen 428 0 0.015 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.001 - 0.006 2.0

Kale 708 3 0.4 0.083 - 0.48 0.050 ^ 2.0

Lettuce 378 0 0.020 ^ 2.0

Mangoes 177 0 0.001 - 0.015 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.010 NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

Snap Peas 710 21 3 0.083 - 0.19 0.050 ^ 2.0

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.008 ^ 2.0

TOTAL 8,759 26

Oryzalin (herbicide) 

Applesauce 570 0 0.020 ^ 0.05

Asparagus 354 0 0.020 ^ NT

Cabbage 335 0 0.020 - 0.050 NT

Cranberries 311 0 0.20 ^ 0.05

Cranberries, Frozen 428 0 0.20 ^ 0.05

Cucumbers 378 0 0.020 - 0.050 NT

Grapefruit 526 0 0.020 - 0.10 0.05

Appendix B. Page 70 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Lettuce 378 1 0.3 0.021 ^ 0.020 ^ V-1 NT

Mangoes 87 0 0.20 ^ NT

Olives, Canned 630 0 0.020 ^ 0.05

Onions 348 0 0.020 ^ NT

Pineapple, Canned 756 0 0.020 - 0.20 NT

Plums, Dried / Prunes 191 0 0.020 ^ 0.05

Sweet Potatoes 701 0 0.10 ^ NT

TOTAL 5,993 1

Oxadiazon (herbicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Grapefruit 271 0 0.003 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 722 0 0.001 - 0.003 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

TOTAL 2,576 0

Oxadixyl (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 - 0.005 NT

Onions 708 0 0.003 - 0.010 NT

Pineapple, Canned 397 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.003 ^ NT

TOTAL 3,707 0

Oxamyl (insecticide) 

Applesauce 570 0 0.003 ^ 2

Asparagus 354 0 0.003 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 2 0.5 0.011 - 0.077 0.010 ^ 2.0

Garbanzo Beans, Canned 189 0 0.006 ^ NT

Grapefruit 526 0 0.002 - 0.005 3

Lettuce 378 0 0.003 ^ NT

Mangoes 177 0 0.002 - 0.005 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.002 - 0.010 0.2

Pineapple, Canned 756 0 0.005 - 0.010 1

Plums, Dried / Prunes 191 0 0.003 ^ NT

Sweet Potatoes 701 0 0.005 ^ 0.1

Tomatoes, Canned 566 0 0.002 ^ 2

TOTAL 7,341 2

Oxamyl oxime (metabolite of Oxamyl)

Applesauce 570 0 0.006 ^ 2

Asparagus 354 0 0.006 ^ NT

Cabbage 354 0 0.010 ^ NT

Appendix B. Page 71 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.050 ^ NT

Cranberries, Frozen 428 0 0.050 ^ NT

Cucumbers 378 12 3.2 0.013 - 0.15 0.010 ^ 2.0

Grapefruit 526 0 0.005 - 0.050 3

Lettuce 378 0 0.006 ^ NT

Mangoes 177 0 0.005 - 0.050 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 348 0 0.010 ^ 0.2

Pineapple, Canned 756 0 0.010 - 0.040 1

Plums, Dried / Prunes 191 0 0.006 - 0.007 NT

Sweet Potatoes 701 0 0.040 ^ 0.1

TOTAL 6,226 12

Oxydemeton methyl (insecticide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cabbage 354 1 0.3 0.019 ^ 0.010 ^ 2

Cucumbers 378 0 0.010 ^ 1.0

Grapefruit 526 0 0.001 - 0.050 1.0

Lettuce 378 0 0.002 ^ 2.0

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ 0.05

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 5,400 1

Oxydemeton methyl sulfone (metabolite of Oxydemeton methyl)

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cabbage 354 1 0.3 0.031 ^ 0.010 ^ 2

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ 1.0

Grapefruit 526 0 0.001 - 0.002 1.0

Lettuce 378 0 0.002 ^ 2.0

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ 0.05

Pineapple, Canned 397 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

TOTAL 5,166 1

Oxyfluorfen (herbicide) 

Applesauce 570 0 0.050 ^ 0.05

Asparagus 354 0 0.050 ^ NT

Cabbage 354 0 0.005 ^ 0.05

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.020 ^ NT

Lettuce 378 0 0.050 ^ NT

Mangoes 90 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.001 - 0.020 0.05

Appendix B. Page 72 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 708 0 0.001 - 0.005 0.05

Pineapple, Canned 397 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.050 ^ 0.05

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 5,200 0

Paclobutrazol (plant growth regulator) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.020 NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,652 0

Parathion (insecticide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Grapefruit 271 0 0.005 ^ NT

Lettuce 378 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.003 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.060 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.060 ^ NT

Tomatoes, Canned 566 0 0.003 ^ NT

TOTAL 6,260 0

Parathion methyl (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.005 - 0.020 NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.001 - 0.020 NT

Olives, Canned 754 0 0.001 - 0.020 NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 7,341 0

Parathion methyl oxygen analog (metabolite of Parathion methyl)

Appendix B. Page 73 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Applesauce 570 0 0.020 ^ NT

Asparagus 354 0 0.020 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Lettuce 378 0 0.020 ^ NT

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

Onions 360 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 3,978 0

Parathion oxygen analog (metabolite of Parathion)

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Pebulate (herbicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 1,477 0

Penconazole (fungicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,652 0

Pencycuron (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,652 0

Pendimethalin (herbicide) 

Applesauce 570 0 0.050 ^ 0.1

Asparagus 354 0 0.050 ^ 0.15

Cabbage 354 0 0.005 ^ 0.1

Appendix B. Page 74 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.005 ^ 0.1

Cranberries, Frozen 428 0 0.005 ^ 0.1

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.010 - 0.045 0.1

Kale 708 62 8.8 0.005 - 0.059 0.003 ^ 0.20

Lettuce 378 0 0.050 ^ 4.0

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 0.1

Onions 708 0 0.001 - 0.005 0.1

Pineapple, Canned 756 0 0.005 - 0.035 NT

Plums, Dried / Prunes 191 0 0.050 ^ 0.10

Sweet Potatoes 701 0 0.035 ^ NT

Tomatoes, Canned 566 7 1.2 0.002 ^ 0.001 ^ 0.10

TOTAL 8,049 69

Penflufen (fungicide) 

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Snap Peas 710 0 0.002 ^ 0.01

TOTAL 2,906 0

Penoxsulam (herbicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ 0.01

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,592 0

Pentachloroaniline - PCA (metabolite of Quintozene)

Applesauce 570 0 0.004 ^ NT

Asparagus 354 0 0.004 ^ NT

Cabbage 354 0 0.005 ^ 0.1

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.003 - 0.060 NT

Kale 708 5 0.7 0.003 ^ 0.002 ^ 0.2

Lettuce 378 0 0.004 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.004 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ 0.1

Appendix B. Page 75 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

TOTAL 8,049 5

Pentachlorobenzene - PCB (metabolite of Quintozene)

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.005 ^ 0.1

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.010 ^ NT

Grapefruit 526 0 0.005 - 0.015 NT

Kale 708 0 0.001 ^ 0.2

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.003 - 0.010 NT

Pineapple, Canned 756 0 0.001 - 0.005 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Sweet Potatoes 701 0 0.001 ^ NT

Tomatoes, Canned 545 0 0.010 ^ 0.1

TOTAL 8,028 0

Pentachlorophenyl methyl sulfide (metabolite of Quintozene)

Cabbage 354 0 0.005 ^ 0.1

Cranberries 311 0 0.015 ^ NT

Cranberries, Frozen 428 0 0.015 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.020 - 0.025 NT

Kale 708 0 0.002 ^ 0.2

Mangoes 177 0 0.003 - 0.020 NT

Olives, Canned 754 0 0.003 - 0.020 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 726 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 5,600 0

Penthiopyrad (fungicide) 

Cabbage 354 1 0.3 0.052 ^ 0.010 ^ 5.0

Cranberries 311 0 0.001 ^ 3.0

Cranberries, Frozen 428 0 0.001 ^ 3.0

Cucumbers 378 2 0.5 0.015 - 0.017 0.010 ^ 0.60

Garbanzo Beans, Canned 189 0 0.001 ^ 0.40

Grapefruit 526 0 0.001 ^ NT

Kale 708 55 7.8 0.003 - 12 0.002 ^ 50

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 11 1.6 0.002 ^ 0.001 - 0.010 3.0

Pineapple, Canned 397 0 0.010 ^ NT

Snap Peas 710 22 3.1 0.003 - 0.36 0.002 ^ 4.0

Tomatoes, Canned 566 16 2.8 0.002 - 0.018 0.001 ^ 3.0

TOTAL 6,206 107

Appendix B. Page 76 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Permethrin Total (insecticide)

Cabbage 354 2 0.6 0.019 - 0.076 0.005 ^ 6

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 1 0.3 0.010 ^ 0.005 ^ 1.5

Grapefruit 255 0 0.010 ^ NT

Kale 708 54 7.6 0.005 - 4.9 0.003 ^ 5.0

Mangoes 87 0 0.005 ^ NT

Onions 348 0 0.005 ^ 0.10

Pineapple, Canned 397 0 0.005 ^ NT

Snap Peas 704 10 1.4 0.005 - 0.33 0.003 ^ V-10 NT

TOTAL 3,970 67

Permethrin cis (isomer of Permethrin)

Applesauce 570 0 0.010 ^ 0.05

Asparagus 354 1 0.3 0.11 ^ 0.010 ^ 2

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.010 ^ NT

Lettuce 378 24 6.3 0.011 - 1.2 0.010 ^ 20

Mangoes 90 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 360 0 0.001 ^ 0.10

Pineapple, Canned 359 0 0.020 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 2 0.3 0.040 - 0.095 0.020 ^ V-2 NT

Tomatoes, Canned 566 8 1.4 0.002 - 0.008 0.001 ^ 2.0

TOTAL 4,783 35

Permethrin trans (isomer of Permethrin)

Applesauce 570 0 0.010 ^ 0.05

Asparagus 354 1 0.3 0.069 ^ 0.010 ^ 2

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.010 ^ NT

Lettuce 378 21 5.6 0.010 - 1.5 0.010 ^ 20

Mangoes 90 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 360 0 0.001 ^ 0.10

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 2 0.3 0.027 - 0.12 0.010 ^ V-2 NT

Tomatoes, Canned 566 7 1.2 0.002 - 0.009 0.001 ^ 2.0

TOTAL 4,783 31

Phenothrin (insecticide) 

Applesauce 570 0 0.050 ^ 0.01

Asparagus 354 0 0.050 ^ 0.01

Cabbage 335 0 0.005 ^ 0.01

Cranberries 311 1 0.3 0.029 ^ 0.025 ^ X-1 0.01

Cranberries, Frozen 428 0 0.025 ^ 0.01

Cucumbers 378 0 0.005 ^ 0.01

Garbanzo Beans, Canned 189 0 0.002 ^ 0.01

Grapefruit 526 0 0.005 ^ 0.01

Kale 708 0 0.004 ^ 0.01

Lettuce 378 0 0.050 ^ 0.01

Mangoes 177 0 0.005 - 0.025 0.01

Appendix B. Page 77 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 754 0 0.005 ^ 0.01

Onions 708 0 0.002 - 0.005 0.01

Pineapple, Canned 756 0 0.005 - 0.15 0.01

Plums, Dried / Prunes 191 0 0.050 ^ 0.01

Snap Peas 710 0 0.004 ^ 0.01

Sweet Potatoes 701 0 0.15 ^ 0.01

Tomatoes, Canned 566 0 0.002 ^ 0.01

TOTAL 8,740 1

Phenthoate (insecticide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

o-Phenylphenol (fungicide) 

Applesauce 570 0 0.005 ^ 25

Asparagus 354 0 0.005 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Grapefruit 526 2 0.4 0.006 ^ 0.005 - 0.010 10

Lettuce 378 0 0.005 ^ NT

Mangoes 87 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ 20

Tomatoes, Canned 566 0 0.001 ^ 10

TOTAL 3,411 2

Phorate (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.030 ^ NT

Cranberries, Frozen 428 0 0.030 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.020 - 0.060 NT

Mangoes 177 0 0.005 - 0.030 NT

Olives, Canned 754 0 0.005 - 0.020 NT

Onions 708 0 0.003 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.17 NT

Sweet Potatoes 701 0 0.17 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 5,848 0

Phorate oxygen analog (metabolite of Phorate)

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.002 - 0.005 NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,485 0

Appendix B. Page 78 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Phorate oxygen analog sulfone (metabolite of Phorate)

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.004 NT

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,445 0

Phorate oxygen analog sulfoxide (metabolite of Phorate)

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.004 NT

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 ^ NT

Pineapple, Canned 359 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,445 0

Phorate sulfone (metabolite of Phorate)

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.025 ^ NT

Cranberries, Frozen 428 0 0.025 ^ NT

Cucumbers 292 0 0.020 - 0.050 NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.003 - 0.005 NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.003 - 0.025 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 679 0 0.002 - 0.050 NT

Pineapple, Canned 756 0 0.020 - 0.050 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.030 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 7,226 0

Phorate sulfoxide (metabolite of Phorate)

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.003 - 0.010 NT

Appendix B. Page 79 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 0

Phosalone (insecticide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.003 ^ NT

Lettuce 378 0 0.001 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.015 NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.002 - 0.005 NT

TOTAL 6,260 0

Phosmet (insecticide) 

Applesauce 570 0 0.010 ^ 10

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.010 ^ 10

Cranberries, Frozen 428 0 0.010 ^ 10

Cucumbers 378 0 0.005 ^ NT

Grapefruit 526 0 0.001 - 0.010 5

Kale 708 0 0.010 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.025 NT

Plums, Dried / Prunes 191 0 0.010 ^ 5

Snap Peas 710 0 0.010 ^ 1

Sweet Potatoes 701 3 0.4 0.061 - 0.15 0.025 ^ 12

TOTAL 7,644 3

Phosmet oxygen analog (metabolite of Phosmet)

Applesauce 570 0 0.004 ^ 10

Asparagus 354 0 0.004 ^ NT

Cranberries 311 0 0.005 ^ 10

Cranberries, Frozen 428 0 0.005 ^ 10

Grapefruit 526 0 0.001 ^ 5

Kale 708 0 0.003 - 0.010 NT

Lettuce 378 0 0.004 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.004 ^ 5

Appendix B. Page 80 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Snap Peas 710 0 0.003 ^ 1

Sweet Potatoes 701 0 0.010 ^ 12

TOTAL 6,167 0

Phosphamidon (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 397 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 3,707 0

Phoxim (insecticide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Pineapple, Canned 359 0 0.025 ^ NT

Sweet Potatoes 701 0 0.025 ^ NT

TOTAL 2,175 0

Picoxystrobin (fungicide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 ^ NT

Mangoes 177 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 2,196 0

Pinoxaden (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.020 ^ NT

Olives, Canned 687 0 0.020 ^ NT

TOTAL 1,048 0

Piperonyl butoxide (insecticide) 

Applesauce 570 0 0.005 ^ 10

Asparagus 354 0 0.005 ^ 10

Cabbage 354 0 0.005 ^ 10

Cranberries 278 0 0.025 ^ 10

Cranberries, Frozen 426 0 0.025 ^ 10

Cucumbers 378 0 0.005 ^ 10

Garbanzo Beans, Canned 189 2 1.1 0.003 ^ 0.002 ^ 10

Grapefruit 526 0 0.010 - 0.025 10

Kale 703 0 0.004 ^ 10

Lettuce 378 0 0.005 ^ 10

Mangoes 177 0 0.003 - 0.025 10

Olives, Canned 754 0 0.003 - 0.010 10

Onions 708 0 0.002 - 0.005 10

Pineapple, Canned 756 0 0.005 - 0.015 10

Plums, Dried / Prunes 191 13 6.8 0.010 - 0.19 0.005 ^ 10

Appendix B. Page 81 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Snap Peas 710 13 1.8 0.007 - 0.035 0.004 ^ 10

Sweet Potatoes 701 55 7.8 0.015 - 0.80 0.015 ^ 10

Tomatoes, Canned 566 2 0.4 0.003 ^ 0.002 ^ 10

TOTAL 8,719 85

Pirimicarb (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 4,767 0

Pirimicarb desmethyl (metabolite of Pirimicarb)

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.001 - 0.010 NT

Sweet Potatoes 701 0 0.001 ^ NT

TOTAL 3,652 0

Pirimiphos ethyl (insecticide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Pirimiphos methyl (insecticide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,260 0

Prallethrin (insecticide) 

Applesauce 570 0 0.010 ^ 1.0

Appendix B. Page 82 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Asparagus 354 0 0.008 ^ 1.0

Cranberries 311 0 0.030 ^ 1.0

Cranberries, Frozen 428 0 0.030 ^ 1.0

Grapefruit 526 0 0.020 - 0.10 1.0

Kale 708 0 0.005 ^ 1.0

Lettuce 378 0 0.010 ^ 1.0

Mangoes 177 0 0.020 - 0.030 1.0

Olives, Canned 754 0 0.020 ^ 1.0

Pineapple, Canned 359 0 0.10 ^ 1.0

Plums, Dried / Prunes 191 0 0.008 ^ 1.0

Snap Peas 710 0 0.005 ^ 1.0

Sweet Potatoes 701 0 0.10 ^ 1.0

TOTAL 6,167 0

Pretilachlor (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Primisulfuron methyl (herbicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 30 0 0.001 ^ NT

Olives, Canned 691 0 0.001 - 0.005 NT

TOTAL 992 0

Prochloraz (fungicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 2,592 0

Procymidone (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.005 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 5,145 0

Profenofos (insecticide) 

Applesauce 570 0 0.075 ^ NT

Asparagus 354 0 0.075 ^ NT

Appendix B. Page 83 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 ^ NT

Lettuce 378 0 0.075 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.075 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 0

Profluralin (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Mangoes 90 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

TOTAL 1,115 0

Profoxydim (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Promecarb (insecticide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Prometon (herbicide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 1,115 0

Prometryn (herbicide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Pronamide (herbicide) 

Applesauce 570 0 0.002 ^ 0.1

Asparagus 354 0 0.002 ^ NT

Cabbage 354 0 0.005 ^ NT

Appendix B. Page 84 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries 311 0 0.005 ^ 0.05

Cranberries, Frozen 428 0 0.005 ^ 0.05

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.003 - 0.050 NT

Lettuce 378 10 2.6 0.002 - 0.016 0.002 ^ 1.0

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.015 NT

Plums, Dried / Prunes 191 0 0.002 ^ 0.1

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,341 10

Propachlor (herbicide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Propamocarb (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 255 67.5 0.010 - 0.88 0.010 ^ 1.5

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 2,592 255

Propamocarb hydrochloride 5

 (fungicide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Grapefruit 255 0 0.001 ^ NT

Lettuce 378 63 16.7 0.002 - 3.0 0.002 ^ 50/90 &

Pineapple, Canned 359 0 0.005 ^ NT

Plums, Dried / Prunes 159 0 0.002 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,515 63

Propanil (herbicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

TOTAL 1,115 0

Propaquizafop (herbicide) 

Appendix B. Page 85 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Propargite (insecticide) 

Applesauce 570 0 0.050 ^ NT

Asparagus 354 0 0.050 ^ NT

Cabbage 354 0 0.020 ^ NT

Cranberries 311 0 0.025 ^ NT

Cranberries, Frozen 428 0 0.025 ^ NT

Cucumbers 378 0 0.020 ^ NT

Garbanzo Beans, Canned 189 0 0.006 ^ NT

Grapefruit 526 0 0.001 - 0.010 5.0

Lettuce 378 0 0.050 ^ NT

Mangoes 177 0 0.001 - 0.025 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.020 ^ NT

Pineapple, Canned 756 0 0.020 - 0.040 NT

Plums, Dried / Prunes 191 0 0.050 ^ NT

Sweet Potatoes 701 0 0.040 ^ NT

Tomatoes, Canned 566 0 0.006 ^ NT

TOTAL 7,341 0

Propazine (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Propetamphos (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 325 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 ^ NT

Kale 708 0 0.010 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.003 - 0.010 NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Snap Peas 710 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 8,730 0

Propham (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Appendix B. Page 86 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

TOTAL 1,115 0

Propiconazole (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 272 0 0.005 ^ 1.0

Cranberries, Frozen 423 0 0.005 ^ 1.0

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.005 ^ NT

Grapefruit 526 1 0.2 0.007 ^ 0.005 ^ 8.0

Kale 708 8 1.1 0.008 - 1.3 0.005 ^ 20

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.005 - 0.010 0.2

Pineapple, Canned 756 0 0.010 - 0.020 4.5

Plums, Dried / Prunes 191 1 0.5 0.010 ^ 0.010 ^ 0.60

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.015 ^ 3.0

TOTAL 8,005 10

Proquinazid (fungicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.005 - 0.010 NT

TOTAL 1,115 0

Prosulfuron (herbicide) 

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Grapefruit 526 0 0.001 - 0.003 NT

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,196 0

Prothioconazole (fungicide) 

Cranberries 311 0 0.10 ^ 2.0

Cranberries, Frozen 428 0 0.10 ^ 2.0

Grapefruit 271 0 0.020 ^ NT

Mangoes 58 0 0.10 ^ NT

TOTAL 1,068 0

Prothiofos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

Sweet Potatoes 701 0 0.020 - 0.040 NT

TOTAL 2,539 0

Pymetrozine (insecticide) 

Appendix B. Page 87 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cabbage 354 0 0.010 ^ 0.5

Cucumbers 378 3 0.8 0.018 - 0.12 0.010 ^ 0.1

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.001 ^ NT

Kale 708 1 0.1 0.083 ^ 0.050 ^ 0.25

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 - 0.085 NT

Sweet Potatoes 701 0 0.085 ^ 0.02

Tomatoes, Canned 566 0 0.002 ^ 0.2

TOTAL 5,115 4

Pyraclofos (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Pyraclostrobin (fungicide) 

Applesauce 570 0 0.003 ^ 1.5

Asparagus 354 0 0.003 ^ NT

Cabbage 354 9 2.5 0.003 - 0.11 0.003 ^ 5.0

Cranberries 311 0 0.001 ^ 4.0

Cranberries, Frozen 428 0 0.001 ^ 4.0

Cucumbers 378 27 7.1 0.003 - 0.082 0.003 ^ 0.5

Garbanzo Beans, Canned 189 0 0.001 ^ 0.5

Grapefruit 526 5 1 0.001 - 0.002 0.001 ^ 2.0

Kale 708 114 16.1 0.003 - 8.8 0.002 ^ 16.0

Lettuce 378 7 1.9 0.004 - 0.24 0.003 ^ 29.0

Mangoes 177 15 8.5 0.001 - 0.007 0.001 ^ 0.6

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.003 ^ 0.9

Pineapple, Canned 756 0 0.003 - 0.005 NT

Plums, Dried / Prunes 191 3 1.6 0.004 - 0.028 0.003 ^ 2.5

Snap Peas 710 47 6.6 0.003 - 0.19 0.002 ^ 0.5

Sweet Potatoes 701 0 0.005 ^ 0.04

Tomatoes, Canned 566 1 0.2 0.002 ^ 0.001 ^ 1.4

TOTAL 8,759 228

Pyraflufen (precursor to Pyraflufen ethyl)

Grapefruit 271 0 0.020 ^ NT

Olives, Canned 630 0 0.020 ^ 0.01

TOTAL 901 0

Pyraflufen ethyl (herbicide) 

Applesauce 570 0 0.010 ^ 0.01

Asparagus 270 0 0.020 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ 0.01

Plums, Dried / Prunes 191 0 0.010 - 0.020 0.01

TOTAL 2,524 0

Appendix B. Page 88 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pyrasulfotole (herbicide) 

Grapefruit 211 0 0.005 ^ NT

Olives, Canned 534 0 0.005 ^ NT

TOTAL 745 0

Pyrazon (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Pyrazophos (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,652 0

Pyrethrins (insecticide) 

Pineapple, Canned 359 0 0.20 ^ 1.0

Sweet Potatoes 701 0 0.20 ^ 1.0

TOTAL 1,060 0

Pyridaben (insecticide, acaricide)

Applesauce 570 2 0.4 0.021 - 0.022 0.005 ^ 0.75

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ 0.5

Cranberries, Frozen 428 0 0.005 ^ 0.5

Cucumbers 378 0 0.005 ^ NT

Grapefruit 526 0 0.001 - 0.005 0.9

Lettuce 378 0 0.005 ^ NT

Mangoes 177 1 0.6 0.002 ^ 0.001 - 0.005 0.10

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.001 - 0.005 NT

Plums, Dried / Prunes 191 0 0.005 ^ 3.0

Sweet Potatoes 701 0 0.001 - 0.002 NT

TOTAL 6,226 3

Pyridalyl (insecticide) 

Grapefruit 271 0 0.040 ^ NT

Mangoes 90 0 0.003 - 0.040 NT

Olives, Canned 754 0 0.003 - 0.040 NT

Pineapple, Canned 329 0 0.010 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 2,145 0

Pyridaphenthion (insecticide) 

Mangoes 30 0 0.001 ^ NT

Appendix B. Page 89 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Pyrimethanil (fungicide) 

Applesauce 570 139 24.4 0.056 - 2.7 0.050 ^ 15

Asparagus 354 0 0.050 ^ NT

Cabbage 354 0 0.003 ^ NT

Cranberries 311 0 0.005 ^ 8.0

Cranberries, Frozen 428 0 0.005 ^ 8.0

Cucumbers 378 10 2.6 0.003 - 0.11 0.003 ^ 1.5

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 2 0.4 0.005 - 0.006 0.005 ^ 10

Lettuce 378 0 0.050 ^ NT

Mangoes 177 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.001 - 0.003 0.2

Pineapple, Canned 756 0 0.003 - 0.005 NT

Plums, Dried / Prunes 191 0 0.050 ^ 10

Sweet Potatoes 701 0 0.005 ^ 0.05

Tomatoes, Canned 566 0 0.001 ^ 0.50

TOTAL 7,341 151

Pyriproxyfen (insecticide, growth regulator)

Applesauce 570 0 0.001 ^ 0.20

Asparagus 354 0 0.001 ^ 2

Cabbage 354 0 0.005 ^ 0.70

Cranberries 311 0 0.001 ^ 1.0

Cranberries, Frozen 428 0 0.001 ^ 1.0

Cucumbers 378 0 0.005 ^ 0.10

Garbanzo Beans, Canned 189 0 0.002 ^ 0.20

Grapefruit 526 0 0.001 - 0.005 0.50

Kale 708 2 0.3 0.002 - 0.042 0.001 ^ 2.0

Lettuce 378 0 0.001 ^ 3.0

Mangoes 177 0 0.001 ^ 1.0

Olives, Canned 754 5 0.7 0.001 - 0.002 0.001 ^ 1.0

Onions 708 0 0.002 - 0.005 0.70

Pineapple, Canned 756 0 0.005 ^ 0.30

Plums, Dried / Prunes 191 4 2.1 0.002 - 0.005 0.001 ^ 1.0

Snap Peas 710 2 0.3 0.019 - 0.036 0.001 ^ 0.20

Sweet Potatoes 701 0 0.005 ^ 0.15

Tomatoes, Canned 566 0 0.002 ^ 0.80

TOTAL 8,759 13

Pyroxasulfone (herbicide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.001 - 0.003 NT

TOTAL 1,115 0

Quinalphos (insecticide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Appendix B. Page 90 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,652 0

Quinoxyfen (fungicide) 

Applesauce 570 0 0.020 ^ NT

Asparagus 354 0 0.020 ^ NT

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.001 ^ 1.0

Cranberries, Frozen 428 0 0.001 ^ 1.0

Cucumbers 378 1 0.3 0.016 ^ 0.010 ^ V-1 NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.020 ^ 7.0/19 &

Mangoes 177 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 397 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.020 ^ 0.70

Tomatoes, Canned 566 0 0.001 ^ 1.7

TOTAL 6,026 1

Quintozene - PCNB (fungicide) (parent of HCB, PCA, PCB and PCPMS)

Cabbage 354 0 0.005 ^ 0.1

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 - 0.025 NT

Kale 708 3 0.4 0.003 ^ 0.002 ^ 0.2

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 726 0 0.005 - 0.025 NT

Sweet Potatoes 701 0 0.025 ^ NT

Tomatoes, Canned 566 0 0.003 ^ 0.1

TOTAL 6,526 3

Quizalofop (metabolite of Quizalofop ethyl)

Grapefruit 271 0 0.050 ^ NT

Olives, Canned 630 0 0.050 ^ NT

TOTAL 901 0

Quizalofop ethyl (herbicide) 

Cranberries 311 0 0.025 ^ NT

Cranberries, Frozen 428 0 0.025 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Mangoes 177 0 0.001 - 0.025 NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 2,196 0

Resmethrin (insecticide) 

Appendix B. Page 91 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cabbage 354 0 0.020 ^ 3.0

Cucumbers 298 0 0.020 ^ 3.0

Grapefruit 526 0 0.003 - 0.005 3.0

Kale 708 0 0.005 ^ 3.0

Mangoes 148 0 0.003 - 0.050 3.0

Olives, Canned 754 0 0.003 ^ 3.0

Onions 348 0 0.020 ^ 3.0

Pineapple, Canned 756 0 0.020 - 0.030 3.0

Snap Peas 710 0 0.005 ^ 3.0

Sweet Potatoes 701 1 0.1 0.090 ^ 0.030 ^ 3.0

TOTAL 5,303 1

Resmethrin cis (isomer of Resmethrin)

Applesauce 570 0 0.050 ^ 3.0

Asparagus 337 0 0.050 ^ 3.0

Garbanzo Beans, Canned 189 0 0.002 ^ 3.0

Lettuce 378 0 0.050 ^ 3.0

Onions 360 0 0.002 ^ 3.0

Plums, Dried / Prunes 191 0 0.050 ^ 3.0

Tomatoes, Canned 566 0 0.002 ^ 3.0

TOTAL 2,591 0

Resmethrin trans (isomer of Resmethrin)

Applesauce 570 0 0.050 ^ 3.0

Asparagus 298 0 0.050 ^ 3.0

Garbanzo Beans, Canned 189 0 0.002 ^ 3.0

Lettuce 378 0 0.050 ^ 3.0

Onions 360 0 0.002 ^ 3.0

Plums, Dried / Prunes 191 0 0.050 ^ 3.0

Tomatoes, Canned 566 0 0.002 ^ 3.0

TOTAL 2,552 0

Rimsulfuron (herbicide) 

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ 0.01

Cranberries, Frozen 428 0 0.005 ^ 0.01

Cucumbers 378 0 0.010 ^ NT

Grapefruit 526 0 0.003 - 0.005 0.01

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 3,673 0

Rotenone (insecticide) 

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Saflufenacil (herbicide) 

Applesauce 570 0 0.010 ^ 0.03

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.020 ^ NT

Appendix B. Page 92 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cranberries, Frozen 428 0 0.020 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 526 0 0.003 - 0.010 0.03

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.003 - 0.020 0.03

Olives, Canned 754 0 0.003 ^ 0.03

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ 0.03

Snap Peas 710 0 0.004 ^ 0.03

TOTAL 5,876 0

Sedaxane (fungicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Sethoxydim (herbicide) 

Applesauce 570 0 0.003 ^ 0.2

Asparagus 354 0 0.003 ^ 4

Cranberries 311 0 0.005 ^ 4.0

Cranberries, Frozen 428 0 0.005 ^ 4.0

Grapefruit 526 0 0.003 - 0.005 0.5

Kale 708 0 0.002 ^ 5.0

Lettuce 378 0 0.003 ^ 4.0

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.003 ^ NT

Sweet Potatoes 701 0 0.010 ^ 4.0

TOTAL 5,457 0

Simazine (herbicide) 

Applesauce 570 0 0.005 ^ 0.20

Asparagus 354 0 0.005 ^ NT

Cranberries 309 0 0.005 ^ 0.25

Cranberries, Frozen 409 0 0.005 ^ 0.25

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.010 0.25

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ 0.20

Onions 360 0 0.001 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.005 ^ 0.20

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 5,843 0

Simetryn (herbicide) 

Cabbage 354 0 0.005 ^ NT

TOTAL 354 0

Appendix B. Page 93 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Spinetoram (insecticide) 

Applesauce 570 0 0.003 ^ 0.20

Asparagus 354 0 0.003 ^ 0.04

Cabbage 354 0 0.010 ^ 2.0

Cranberries 311 2 0.6 0.001 - 0.002 0.001 ^ 0.50

Cranberries, Frozen 428 22 5.1 0.001 - 0.005 0.001 ^ 0.50

Cucumbers 378 0 0.010 ^ 0.30

Garbanzo Beans, Canned 189 0 0.001 ^ 0.04

Grapefruit 526 0 0.001 - 0.010 0.30

Kale 708 85 12 0.017 - 0.41 0.010 ^ 10

Lettuce 378 12 3.2 0.003 - 0.12 0.003 ^ 8.0

Mangoes 177 0 0.001 - 0.010 0.30

Olives, Canned 754 0 0.010 ^ NT

Onions 320 0 0.010 ^ 0.10

Pineapple, Canned 756 0 0.010 ^ 0.04

Plums, Dried / Prunes 191 0 0.003 ^ 0.30

Snap Peas 710 15 2.1 0.017 ^ 0.010 ^ 0.30

Sweet Potatoes 701 0 0.010 ^ 0.10

Tomatoes, Canned 566 0 0.001 ^ 0.40

TOTAL 8,371 136

Spinosad (insecticide) (total of spinosyns A and D)

Cabbage 354 0 0.004 ^ 2.0

Cranberries 311 7 2.3 0.002 - 0.004 0.002 ^ 0.40

Cranberries, Frozen 428 13 3 0.002 - 0.013 0.002 ^ 0.40

Cucumbers 378 0 0.004 ^ 0.3

Garbanzo Beans, Canned 189 0 0.001 ^ 0.02

Grapefruit 526 0 0.002 - 0.003 0.30

Kale 708 36 5.1 0.003 - 1.2 0.002 ^ 10.0

Mangoes 177 0 0.002 - 0.003 0.3

Olives, Canned 754 0 0.003 ^ 0.02

Onions 320 0 0.004 ^ 0.10

Pineapple, Canned 397 0 0.004 ^ 0.02

Snap Peas 710 22 3.1 0.003 - 0.070 0.002 ^ 0.30

Tomatoes, Canned 566 1 0.2 0.002 ^ 0.001 ^ 0.40

TOTAL 5,818 79

Spinosad A (isomer of Spinosad) 

Applesauce 570 0 0.003 ^ 0.20

Asparagus 354 0 0.003 ^ 0.2

Lettuce 378 2 0.5 0.008 - 0.11 0.003 ^ 8.0

Pineapple, Canned 359 0 0.005 ^ 0.02

Plums, Dried / Prunes 191 0 0.003 ^ 0.20

Sweet Potatoes 701 0 0.005 ^ 0.10

TOTAL 2,553 2

Spinosad D (isomer of Spinosad) 

Pineapple, Canned 359 0 0.005 ^ 0.02

Sweet Potatoes 701 0 0.005 ^ 0.10

TOTAL 1,060 0

Spirodiclofen (acaricide) 

Applesauce 570 0 0.010 ^ 0.80

Asparagus 354 0 0.010 ^ NT

Appendix B. Page 94 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cabbage 354 0 0.010 ^ NT

Cranberries 307 0 0.005 ^ NT

Cranberries, Frozen 380 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.005 ^ NT

Grapefruit 467 0 0.003 - 0.005 0.50

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.003 - 0.005 1.0

Olives, Canned 754 0 0.003 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ 1.0

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 6,304 0

Spiromesifen Total (parent + enol metabolite) (insecticide) 

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Onions 360 0 0.002 ^ 0.09

Tomatoes, Canned 566 0 0.008 ^ 0.45

TOTAL 1,115 0

Spiromesifen (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 325 0 0.010 ^ NT

Cranberries 311 0 0.010 ^ 2.0

Cranberries, Frozen 428 0 0.010 ^ 2.0

Cucumbers 378 13 3.4 0.002 - 0.010 0.002 ^ 0.10

Grapefruit 526 0 0.003 - 0.020 NT

Kale 708 5 0.7 0.002 - 0.13 0.001 ^ 12

Lettuce 378 0 0.010 ^ 12

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

TOTAL 4,746 18

Spiromesifen alcohol (metabolite of Spiromesifen)

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Spirotetramat (insecticide) 

Applesauce 570 0 0.002 ^ 0.70

Asparagus 354 0 0.002 ^ NT

Cabbage 354 0 0.010 ^ 2.5

Cranberries 311 0 0.002 ^ 3.0

Cranberries, Frozen 428 3 0.7 0.003 - 0.005 0.002 ^ 3.0

Garbanzo Beans, Canned 189 0 0.002 ^ 2.5

Grapefruit 526 0 0.001 ^ 0.60

Kale 708 84 11.9 0.008 - 0.89 0.005 ^ 8.0

Lettuce 378 13 3.4 0.002 - 0.082 0.002 ^ 9.0

Mangoes 177 0 0.001 - 0.002 0.60

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.002 - 0.010 0.80

Appendix B. Page 95 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pineapple, Canned 756 0 0.005 - 0.010 0.30

Plums, Dried / Prunes 191 0 0.002 ^ 4.5

Snap Peas 710 2 0.3 0.008 ^ 0.005 ^ 2.5

Sweet Potatoes 701 0 0.005 ^ 0.60

TOTAL 7,815 102

Spiroxamine (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ 0.05

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 320 0 0.010 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 5,117 0

Sulfallate (herbicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

TOTAL 1,115 0

Sulfentrazone (herbicide) 

Cabbage 354 0 0.005 ^ 0.20

Cranberries 311 0 0.015 ^ 0.15

Cranberries, Frozen 428 0 0.015 ^ 0.15

Grapefruit 526 0 0.010 - 0.015 0.15

Kale 708 0 0.020 - 0.067 0.4

Mangoes 177 0 0.003 - 0.015 NT

Olives, Canned 691 0 0.003 - 0.010 NT

Pineapple, Canned 359 0 0.035 ^ NT

Snap Peas 710 0 0.020 ^ 0.15

Sweet Potatoes 701 0 0.035 ^ 0.15

TOTAL 4,965 0

Sulfometuron methyl (herbicide) 

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

TOTAL 1,115 0

Sulfosulfuron (herbicide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 691 0 0.001 - 0.005 NT

TOTAL 721 0

Sulfoxaflor (insecticide) 

Cranberries 311 0 0.050 ^ 0.70

Cranberries, Frozen 428 0 0.050 ^ 0.70

Appendix B. Page 96 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.003 - 0.10 3.0

Kale 708 8 1.1 0.033 - 0.13 0.020 - 0.067 2.0

Mangoes 177 0 0.003 - 0.050 NT

Olives, Canned 754 0 0.003 ^ NT

Onions 360 0 0.001 - 0.004 0.01

Tomatoes, Canned 566 0 0.001 ^ 0.70

TOTAL 4,019 8

Sulprofos (insecticide) 

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 360 0 0.002 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 2,230 0

TCMTB (fungicide) 

Cranberries 311 0 0.10 ^ NT

Cranberries, Frozen 428 0 0.10 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Mangoes 177 0 0.005 - 0.10 NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 2,196 0

Tebuconazole (fungicide) 

Applesauce 570 0 0.010 ^ 0.05

Asparagus 354 0 0.010 ^ 0.05

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 5 1.3 0.007 - 0.027 0.005 ^ 0.4

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 ^ NT

Kale 708 34 4.8 0.008 - 5.9 0.005 ^ X-1 2.5

Lettuce 378 0 0.010 ^ NT

Mangoes 177 3 1.7 0.005 - 0.011 0.003 - 0.005 0.15

Olives, Canned 754 13 1.7 0.008 - 0.038 0.003 - 0.005 V-13 NT

Onions 708 0 0.001 - 0.005 0.2

Pineapple, Canned 756 0 0.005 - 0.015 NT

Plums, Dried / Prunes 191 2 1 0.011 - 0.033 0.010 ^ 1.0

Snap Peas 710 82 11.5 0.008 - 0.39 0.005 ^ V-82 NT

Sweet Potatoes 701 0 0.015 ^ NT

Tomatoes, Canned 566 0 0.003 ^ 1.3

TOTAL 8,759 139

Tebufenozide (insecticide) 

Applesauce 570 0 0.002 ^ 1.0

Asparagus 354 0 0.002 ^ NT

Cabbage 354 0 0.005 ^ 5.0

Cranberries 311 9 2.9 0.004 - 0.010 0.002 ^ 1.0

Cranberries, Frozen 428 0 0.002 ^ 1.0

Cucumbers 378 0 0.005 ^ NT

Appendix B. Page 97 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.005 - 0.020 2.0

Lettuce 378 0 0.002 ^ 10.0

Mangoes 177 0 0.002 - 0.005 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 708 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 0 0.005 ^ 0.015

Tomatoes, Canned 566 0 0.002 ^ 1.0

TOTAL 7,341 9

Tebufenpyrad (insecticide, acaricide)

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,652 0

Tebupirimfos (insecticide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

TOTAL 549 0

Tebuthiuron (herbicide) 

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 2,230 0

Tecnazene (plant growth regulator) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 - 0.010 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 397 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 3,707 0

Teflubenzuron (insecticide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 117 0 0.005 - 0.010 1.5

Olives, Canned 691 0 0.005 ^ NT

Pineapple, Canned 359 0 0.020 ^ 0.80

Appendix B. Page 98 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 2,139 0

Tefluthrin (insecticide) 

Applesauce 570 0 0.002 ^ NT

Asparagus 354 0 0.002 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Kale 708 0 0.001 ^ NT

Lettuce 378 0 0.002 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Snap Peas 710 0 0.001 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 8,759 0

Tepraloxydim (herbicide) 

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Mangoes 177 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

TOTAL 2,196 0

Terbacil (herbicide) 

Applesauce 570 0 0.010 ^ 0.3

Asparagus 354 0 0.010 ^ 0.4

Cabbage 354 0 0.008 ^ NT

Cucumbers 378 0 0.008 ^ NT

Garbanzo Beans, Canned 189 0 0.003 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 626 0 0.001 - 0.005 NT

Onions 708 0 0.003 - 0.008 NT

Pineapple, Canned 756 0 0.008 - 0.020 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.003 ^ NT

TOTAL 5,861 0

Terbufos (insecticide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.003 - 0.005 NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.003 NT

Appendix B. Page 99 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

TOTAL 2,196 0

Terbufos oxygen analog (metabolite of Terbufos)

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Grapefruit 255 0 0.001 ^ NT

Mangoes 87 0 0.001 ^ NT

TOTAL 1,081 0

Terbufos oxygen analog sulfone (metabolite of Terbufos)

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Mangoes 177 0 0.005 - 0.010 NT

TOTAL 1,442 0

Terbufos oxygen analog sulfoxide (metabolite of Terbufos)

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 255 0 0.005 ^ NT

Mangoes 87 0 0.005 ^ NT

TOTAL 1,081 0

Terbufos sulfone (metabolite of Terbufos)

Cranberries 311 0 0.025 ^ NT

Cranberries, Frozen 428 0 0.025 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.005 ^ NT

Mangoes 177 0 0.005 - 0.025 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 360 0 0.001 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 3,311 0

Terbufos sulfoxide (metabolite of Terbufos)

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Grapefruit 526 0 0.002 - 0.003 NT

Mangoes 177 0 0.002 - 0.003 NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 2,196 0

Terbuthylazine (herbicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 3,652 0

Terbutryn (herbicide) 

Appendix B. Page 100 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 30 0 0.001 ^ NT

Olives, Canned 31 0 0.001 ^ NT

TOTAL 61 0

Tetrachlorvinphos (insecticide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 526 0 0.001 - 0.005 NT

Mangoes 177 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 360 0 0.002 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 3,311 0

Tetraconazole (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.005 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 360 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ 0.30

TOTAL 3,723 0

Tetradifon (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.002 ^ NT

Grapefruit 271 0 0.010 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 90 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Onions 708 0 0.002 - 0.005 NT

Pineapple, Canned 726 0 0.005 - 0.020 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.020 ^ NT

Tomatoes, Canned 566 0 0.002 ^ NT

TOTAL 6,230 0

Tetrahydrophthalimide - THPI (metabolite of Captafol and Captan)

Applesauce 570 394 69.1 0.010 - 0.45 0.010 ^ 25.0

Asparagus 354 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.004 ^ 0.05

Grapefruit 271 0 0.020 ^ NT

Kale 708 2 0.3 0.012 - 0.027 0.007 ^ 0.05

Lettuce 378 0 0.010 ^ 0.05

Mangoes 90 0 0.005 - 0.020 NT

Olives, Canned 754 0 0.005 - 0.020 NT

Appendix B. Page 101 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 360 0 0.004 ^ 0.05

Plums, Dried / Prunes 191 0 0.010 ^ 10.0

Snap Peas 710 57 8 0.012 - 0.25 0.007 ^ X-11 0.05

Tomatoes, Canned 566 0 0.004 - 0.012 0.05

TOTAL 5,141 453

Tetramethrin (insecticide) 

Applesauce 570 0 0.005 ^ NT

Asparagus 354 0 0.005 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 272 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.010 NT

Kale 708 0 0.003 ^ NT

Lettuce 378 0 0.005 ^ NT

Mangoes 177 0 0.005 - 0.010 NT

Olives, Canned 754 0 0.005 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.10 NT

Plums, Dried / Prunes 191 0 0.005 ^ NT

Snap Peas 710 0 0.003 ^ NT

Sweet Potatoes 701 0 0.10 ^ NT

TOTAL 7,538 0

Thiabendazole (fungicide) (parent of 5-hydroxythiabendazole)

Applesauce 570 184 32.3 0.002 - 0.67 0.002 ^ 5.0

Asparagus 294 0 0.002 ^ NT

Cabbage 354 0 0.010 ^ 0.02

Cranberries 280 0 0.005 ^ NT

Cranberries, Frozen 425 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ 0.02

Garbanzo Beans, Canned 189 0 0.001 ^ 0.02

Grapefruit 526 377 71.7 0.001 - 0.20 0.001 - 0.016 10.0

Lettuce 378 1 0.3 0.005 ^ 0.002 ^ V-1 NT

Mangoes 177 85 48 0.001 - 2.0 0.001 - 0.005 10.0

Olives, Canned 754 0 0.001 ^ NT

Onions 708 0 0.001 - 0.010 0.02

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.002 ^ NT

Sweet Potatoes 701 97 13.8 0.006 - 4.1 0.005 ^ 10

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 7,247 744

Thiacloprid (insecticide) 

Applesauce 570 9 1.6 0.001 - 0.002 0.001 ^ 0.30

Asparagus 354 0 0.001 ^ NT

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Appendix B. Page 102 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 708 0 0.001 - 0.010 NT

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.001 ^ 0.05

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,260 9

Thiamethoxam (insecticide) (also a parent of Clothianidin)

Applesauce 570 5 0.9 0.004 - 0.005 0.003 ^ 0.2

Asparagus 354 1 0.3 0.008 ^ 0.003 ^ 0.02

Cabbage 354 13 3.7 0.010 - 0.081 0.010 ^ 4.5

Cranberries 311 0 0.010 ^ 0.20

Cranberries, Frozen 428 0 0.010 ^ 0.20

Cucumbers 378 41 10.8 0.010 - 0.065 0.010 ^ 0.2

Garbanzo Beans, Canned 189 0 0.002 ^ 0.02

Grapefruit 526 8 1.5 0.001 - 0.030 0.001 - 0.005 0.40

Kale 708 24 3.4 0.050 - 0.40 0.030 ^ 3.0

Lettuce 378 52 13.8 0.003 - 0.049 0.003 ^ 4.0

Mangoes 177 0 0.001 - 0.010 0.40

Olives, Canned 754 0 0.001 ^ 0.02

Onions 708 2 0.3 0.003 ^ 0.002 - 0.010 0.03

Pineapple, Canned 756 0 0.005 - 0.010 0.02

Plums, Dried / Prunes 191 0 0.003 ^ 0.5

Snap Peas 710 3 0.4 0.050 - 0.17 0.030 ^ X-3 0.02

Sweet Potatoes 701 0 0.005 ^ 0.02

Tomatoes, Canned 566 0 0.002 ^ 0.25

TOTAL 8,759 149

Thiazopyr (herbicide) 

Applesauce 570 0 0.008 ^ NT

Asparagus 354 0 0.008 ^ NT

Cranberries 311 0 0.001 ^ NT

Cranberries, Frozen 428 0 0.001 ^ NT

Grapefruit 526 0 0.001 - 0.003 NT

Lettuce 378 0 0.008 ^ NT

Mangoes 177 0 0.001 - 0.003 NT

Olives, Canned 754 0 0.003 ^ NT

Plums, Dried / Prunes 191 0 0.008 ^ NT

TOTAL 3,689 0

Thidiazuron (plant growth regulator) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.005 ^ NT

Olives, Canned 754 0 0.005 ^ NT

TOTAL 1,115 0

Thiencarbazone methyl (herbicide) 

Grapefruit 271 0 0.020 ^ NT

Mangoes 30 0 0.003 ^ NT

Olives, Canned 691 0 0.003 - 0.020 NT

TOTAL 992 0

Thifensulfuron methyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Appendix B. Page 103 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Thiobencarb (herbicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.003 ^ NT

Lettuce 378 0 0.010 ^ 0.2

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 360 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 3,723 0

Thiodicarb (insecticide) 

Applesauce 570 0 0.003 ^ NT

Asparagus 354 0 0.003 ^ NT

Grapefruit 271 0 0.010 ^ NT

Lettuce 378 0 0.003 ^ 35

Mangoes 90 0 0.010 ^ NT

Olives, Canned 754 0 0.010 ^ NT

Pineapple, Canned 359 0 0.010 ^ NT

Plums, Dried / Prunes 191 0 0.003 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,668 0

Thionazin (insecticide, fumigant)

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

TOTAL 1,115 0

Thiophanate methyl (fungicide) 

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Grapefruit 255 0 0.005 ^ NT

Mangoes 87 0 0.005 ^ NT

TOTAL 1,081 0

Tolclofos methyl (fungicide) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 - 0.005 NT

TOTAL 1,115 0

Tolfenpyrad (insecticide) 

Grapefruit 271 0 0.005 ^ 1.5

Mangoes 90 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 - 0.005 NT

TOTAL 1,115 0

Appendix B. Page 104 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tolylfluanid (fungicide) 

Pineapple, Canned 329 0 0.050 - 0.10 NT

Sweet Potatoes 701 0 0.050 ^ NT

TOTAL 1,030 0

Topramezone (herbicide) 

Cranberries 299 0 0.10 ^ NT

Cranberries, Frozen 418 0 0.10 ^ NT

Grapefruit 255 0 0.25 ^ NT

TOTAL 972 0

Tri-Allate (herbicide) 

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 754 0 0.001 - 0.005 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 2,592 0

Triadimefon (fungicide) (also a parent of Triadimenol)

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.003 ^ NT

Mangoes 90 0 0.003 ^ NT

Olives, Canned 754 0 0.003 ^ NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 ^ 2.0

Sweet Potatoes 701 0 0.005 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 4,767 0

Triadimenol (fungicide) (also a metabolite of Triadimefon)

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.025 ^ NT

Cranberries, Frozen 428 0 0.025 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 526 0 0.005 - 0.020 NT

Mangoes 177 0 0.020 - 0.025 NT

Olives, Canned 754 0 0.020 ^ NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 756 0 0.005 - 0.020 2.0

Sweet Potatoes 701 0 0.020 ^ NT

TOTAL 4,733 0

Triasulfuron (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Appendix B. Page 105 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Triazophos (insecticide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 756 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

TOTAL 3,652 0

Tribenuron methyl (herbicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Trichlorfon (insecticide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cranberries 311 0 0.040 ^ NT

Cranberries, Frozen 428 0 0.040 ^ NT

Grapefruit 526 0 0.003 - 0.020 NT

Lettuce 378 0 0.010 ^ NT

Mangoes 177 0 0.003 - 0.040 NT

Olives, Canned 754 0 0.003 - 0.005 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

TOTAL 3,689 0

Trichloronate (insecticide) 

Mangoes 30 0 0.001 ^ NT

Olives, Canned 61 0 0.001 ^ NT

TOTAL 91 0

Triclopyr (herbicide) 

Grapefruit 271 0 0.25 ^ NT

Olives, Canned 630 0 0.25 ^ NT

TOTAL 901 0

Tricyclazole (fungicide) 

Grapefruit 271 0 0.001 ^ NT

Mangoes 90 0 0.001 ^ NT

Olives, Canned 754 0 0.001 ^ NT

TOTAL 1,115 0

Trifloxystrobin (fungicide) 

Applesauce 570 0 0.002 ^ 0.5

Asparagus 354 0 0.001 - 0.002 0.07

Cabbage 354 0 0.005 ^ 2.0

Cranberries 311 0 0.001 ^ 1.5

Cranberries, Frozen 428 0 0.001 ^ 1.5

Cucumbers 378 0 0.005 ^ 0.50

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 526 0 0.001 ^ 0.6

Appendix B. Page 106 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Kale 708 14 2 0.003 - 0.88 0.002 ^ 30

Lettuce 378 0 0.002 ^ 30

Mangoes 177 22 12.4 0.001 - 0.061 0.001 ^ 0.7

Olives, Canned 754 1 0.1 0.006 ^ 0.001 ^ V-1 NT

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 756 0 0.005 ^ NT

Plums, Dried / Prunes 191 2 1 0.003 - 0.010 0.002 ^ 2

Sweet Potatoes 701 0 0.005 ^ 0.04

Tomatoes, Canned 566 1 0.2 0.002 ^ 0.001 ^ 0.5

TOTAL 8,049 40

Trifloxysulfuron (herbicide) 

Applesauce 570 0 0.020 ^ NT

Asparagus 354 0 0.020 ^ NT

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Grapefruit 526 0 0.001 - 0.005 0.03

Lettuce 378 0 0.020 ^ NT

Mangoes 177 0 0.001 - 0.010 NT

Olives, Canned 754 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.020 ^ NT

TOTAL 3,689 0

Triflumizole (fungicide) 

Applesauce 570 0 0.010 ^ 0.50

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.003 ^ 8.0

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 3 0.8 0.038 - 0.058 0.003 ^ 0.5

Grapefruit 526 0 0.003 - 0.005 NT

Kale 708 24 3.4 0.003 - 0.84 0.002 ^ 40

Lettuce 378 0 0.010 ^ 35

Mangoes 177 0 0.003 - 0.010 2.5

Olives, Canned 754 0 0.003 ^ NT

Onions 348 0 0.003 ^ NT

Pineapple, Canned 756 0 0.003 - 0.005 4.0

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.005 ^ NT

TOTAL 6,934 27

Trifluralin (herbicide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 2 0.6 0.001 ^ 0.001 ^ 0.05

Cabbage 354 0 0.005 ^ 0.05

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 0.05

Garbanzo Beans, Canned 189 0 0.001 ^ 0.05

Grapefruit 526 0 0.005 - 0.010 0.05

Kale 708 63 8.9 0.002 - 0.016 0.001 ^ 0.05

Lettuce 378 1 0.3 0.001 ^ 0.001 ^ V-1 NT

Mangoes 177 0 0.003 - 0.010 NT

Olives, Canned 754 0 0.003 - 0.010 NT

Appendix B. Page 107 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Onions 708 0 0.001 - 0.005 0.05

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.001 ^ 0.05

Snap Peas 710 0 0.001 ^ 0.05

Sweet Potatoes 701 0 0.010 ^ 0.05

Tomatoes, Canned 566 5 0.9 0.002 - 0.007 0.001 ^ 0.05

TOTAL 8,759 71

Triforine (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Grapefruit 271 0 0.10 ^ NT

Lettuce 378 0 0.010 ^ NT

Mangoes 60 0 0.10 ^ NT

Olives, Canned 661 0 0.10 ^ NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

TOTAL 2,485 0

Triticonazole (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.010 ^ NT

Grapefruit 526 0 0.005 - 0.025 NT

Mangoes 177 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 - 0.005 NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 3,673 0

Uniconazole (insect growth regulator) 

Grapefruit 271 0 0.005 ^ NT

Mangoes 90 0 0.001 - 0.005 NT

Olives, Canned 722 0 0.001 - 0.005 NT

TOTAL 1,083 0

Vernolate (herbicide) 

Cabbage 354 0 0.010 ^ NT

Cucumbers 378 0 0.010 ^ NT

Onions 348 0 0.010 ^ NT

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 1,477 0

Vinclozolin (fungicide) 

Applesauce 570 0 0.010 ^ NT

Asparagus 354 0 0.010 ^ NT

Cabbage 354 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 1.0

Garbanzo Beans, Canned 189 0 0.001 ^ NT

Grapefruit 271 0 0.005 ^ NT

Lettuce 378 0 0.010 ^ 10.0

Mangoes 90 0 0.003 - 0.005 NT

Olives, Canned 754 0 0.003 - 0.005 NT

Onions 708 0 0.001 - 0.005 NT

Appendix B. Page 108 of 109
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pineapple, Canned 756 0 0.005 - 0.010 NT

Plums, Dried / Prunes 191 0 0.010 ^ NT

Sweet Potatoes 701 0 0.010 ^ NT

Tomatoes, Canned 566 0 0.001 ^ NT

TOTAL 6,260 0

Zoxamide (fungicide) 

Cabbage 354 0 0.010 ^ NT

Cranberries 311 0 0.002 ^ NT

Cranberries, Frozen 428 0 0.002 ^ NT

Grapefruit 526 0 0.001 - 0.002 NT

Mangoes 177 0 0.001 - 0.002 NT

Olives, Canned 754 0 0.001 ^ NT

Onions 348 0 0.010 ^ 0.7

Pineapple, Canned 397 0 0.010 ^ NT

TOTAL 3,295 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

& Tolerance is different for head and leaf lettuce. First value shown is for head lettuce and the second is for leaf lettuce.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities when used to control insect larvae.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 Emamectin benzoate is the salt form of the active, Emamectin.

2 Halosulfuron methyl is the salt form of the active, Halosulfuron.

3 Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

4 Specific tolerance established for methamidophos in lettuce as a possible result of an acephate application.

5 Propamocarb analytically determined as the salt (hydrochloride).

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

pages 1 and 2 in Appendix K to see the sample origin (domestic, imported, or unknown) for each occurrence.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 3 and 4 in Appendix K to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2017 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix B. Page 109 of 109
Appendix C

Distribution of Residues by Pesticide

in Honey 

Appendix C shows residue detections for all compounds tested in honey, including range of values 

detected, range of Limits of Detection (LODs), and U.S. Environmental Protection Agency (EPA) 

tolerance references for each pair. The EPA tolerances cited in this summary and appendixes 

apply to 2017 and not to the current year. There may be instances where tolerances have been 

recently set, modified, or revoked that would have an effect on whether a residue is violative or 

not. 

In 2017, the Pesticide Data Program (PDP) analyzed 315 honey samples. PDP detected six 

different residues (including metabolites), representing six pesticides, in the honey samples. 

All residue detections were lower than the established tolerances for those compounds with 

established tolerances.

Results for environmental contaminants across all commodities, including honey, have been 

consolidated in a separate appendix because they have no registered uses and are not applied 

to crops (see Appendix F). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

1-Naphthol IM 315 0.20 ^ NT

2,4-dimethylphenyl formamide (2,4-DMPF) I 315 238 75.6 0.003 - 0.082 0.003 ^ 0.2

2,6-dichlorobenzamide (V-2) HM 315 2 0.6 0.020 - 0.074 0.008 ^ NT

3-Hydroxycarbofuran IM 315 0.005 ^ NT

4-Hydroxychlorothalonil FM 315 0.005 ^ NT

Acephate I 315 0.050 ^ 0.02

Acetamiprid I 315 0.005 ^ 0.01

Acetochlor H 315 0.20 ^ NT

Acrinathrin I 315 0.20 ^ NT

Alachlor (V-3) H 315 3 1 0.46 - 1.1 0.40 ^ NT

Aldicarb I 315 0.015 ^ NT

Aldicarb sulfone IM 315 0.003 ^ NT

Aldicarb sulfoxide IM 315 0.008 ^ NT

Ametoctradin F 315 0.003 ^ NT

Atrazine H 315 0.008 ^ NT

Avermectin I 315 0.10 ^ NT

Azinphos methyl I 315 0.50 ^ NT

Azoxystrobin F 315 0.003 ^ NT

Bensulide H 315 0.008 ^ NT

Bentazon H 315 0.060 ^ NT

Bifenazate A 252 0.007 ^ NT

Bifenthrin I 315 0.020 ^ 0.05

Boscalid F 315 0.010 ^ NT

Bromacil H 315 0.020 ^ NT

Bromopropylate A 315 0.050 ^ NT

Bromuconazole F 315 0.020 ^ NT

Buprofezin I 315 0.004 ^ NT

Captan F 315 0.50 ^ NT

Carbaryl I 315 0.010 ^ NT

Carbendazim (MBC) (V-3) F 315 3 1 0.005 ^ 0.005 ^ NT

Carbofuran I 315 0.003 ^ NT

Carfentrazone ethyl H 315 0.010 ^ NT

Chlorantraniliprole I 315 0.030 ^ NT

Chlorfenapyr I 315 0.50 ^ 0.01

Chlorfenvinphos total I 315 0.10 ^ NT

Chlorothalonil F 252 0.50 ^ NT

Chlorpropham H 315 0.030 ^ NT

Chlorpyrifos I 315 0.010 ^ 0.1

Chlorpyrifos methyl I 315 0.020 ^ NT

Clofentezine I 315 0.050 ^ NT

Clothianidin I 315 0.015 ^ 0.02

Coumaphos I 315 1 0.3 0.013 ^ 0.008 ^ 0.15

Coumaphos oxygen analog IM 315 0.001 ^ 0.15

Cyantraniliprole I 315 0.030 ^ NT

APPENDIX C. DISTRIBUTION OF RESIDUES BY PESTICIDE IN HONEY

Appendix C. Page 1 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Cyazofamid F 315 0.004 ^ NT

Cyflufenamid F 315 0.003 ^ NT

Cyflumetofen A 315 0.025 ^ NT

Cyfluthrin I 315 0.050 ^ 0.05

Cyhalothrin, Lambda I 315 0.20 ^ 0.01

Cymiazole A 315 0.008 ^ NT

Cymoxanil F 315 0.008 ^ NT

Cypermethrin I 315 0.050 ^ 0.05

Cyphenothrin I 315 2.0 ^ NT

Cyprodinil F 315 0.004 ^ NT

Cyromazine R 315 0.010 ^ NT

DCPA H 315 0.005 ^ NT

DEET (N,N-diethyl-m-toluamide) X 315 0.006 ^ NT

DEF (Tribufos) H 315 0.20 ^ NT

Deltamethrin 1 I 315 0.20 ^ 0.05

Diazinon I 315 0.050 ^ NT

Diazinon oxygen analog IM 256 0.008 ^ NT

Dichlorvos (DDVP) I 315 0.006 ^ 0.5

Dicloran F 315 0.050 ^ NT

Dicofol p,p' I 315 0.50 ^ NT

Difenoconazole F 315 0.008 ^ NT

Diflubenzuron I 315 0.005 ^ NT

Dimethenamid H 315 0.010 ^ NT

Dimethoate I 315 0.005 ^ NT

Dimethomorph F 315 0.050 ^ NT

Dinotefuran I 315 0.010 ^ 0.01

Diphenamid H 315 0.010 ^ NT

Diphenylamine (DPA) F 315 0.005 ^ NT

Diuron H 315 0.002 ^ NT

Emamectin benzoate I 315 0.004 ^ NT

Endosulfan I IM 315 0.020 ^ NT

Endosulfan II IM 315 0.020 ^ NT

Endosulfan sulfate IM 315 0.020 ^ NT

Epoxiconazole F 315 0.004 ^ NT

Esfenvalerate+Fenvalerate Total I 315 0.050 ^ 0.05

Ethion I 315 0.050 ^ NT

Ethofumesate H 315 0.030 ^ NT

Etofenprox I 315 0.050 ^ 5.0

Etoxazole A 315 0.001 ^ NT

Famoxadone F 315 0.010 ^ NT

Fenamidone F 315 0.003 ^ NT

Fenarimol F 315 0.025 ^ NT

Fenazaquin I 315 0.005 ^ NT

Fenbuconazole F 315 0.006 ^ NT

Fenhexamid F 315 0.009 ^ NT

Fenoxaprop ethyl H 315 0.004 ^ NT

Appendix C. Page 2 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fenpropathrin I 315 0.050 ^ NT

Fenpyroximate A 315 0.006 ^ 0.10

Fipronil I 315 0.050 ^ NT

Fipronil sulfide (MB45950) IM 315 0.010 ^ NT

Fipronil sulfone (MB46136) IM 315 0.050 ^ NT

Flonicamid I 315 0.015 ^ NT

Fludioxonil F 315 0.020 ^ NT

Fluometuron H 315 0.003 ^ NT

Fluopicolide F 315 0.006 ^ NT

Fluopyram F 315 0.002 ^ NT

Fluoxastrobin F 315 0.005 ^ NT

Flupyradifurone I 315 0.015 ^ NT

Fluridone H 315 0.002 ^ NT

Flutriafol F 315 0.020 ^ NT

Fluvalinate I 315 0.050 ^ 0.02

Fluxapyroxad F 315 0.004 ^ NT

Hexazinone H 315 0.002 ^ NT

Hexythiazox I 315 0.005 ^ NT

Imazalil F 315 0.025 ^ NT

Imidacloprid I 315 0.010 ^ NT

Indoxacarb I 315 0.015 ^ NT

Iprodione F 315 0.20 ^ NT

Kresoxim-methyl F 315 0.005 ^ NT

Linuron H 315 0.030 ^ NT

Malathion I 315 0.050 ^ NT

Mandipropamid F 315 0.004 ^ NT

Metalaxyl/Mefenoxam 2 F 315 0.003 ^ NT

Metconazole F 315 0.010 ^ NT

Methamidophos I 315 0.15 ^ 0.02

Methidathion I 315 0.004 ^ NT

Methomyl I 315 0.007 ^ NT

Methoprene R 315 0.010 ^ NT

Methoxyfenozide I 315 0.002 ^ NT

Metolachlor H 315 0.050 ^ NT

Metribuzin H 315 0.050 ^ NT

MGK-264 I 315 0.015 ^ 5

Momfluorothrin I 315 0.050 ^ NT

Myclobutanil F 315 0.015 ^ NT

Norflurazon H 315 0.015 ^ NT

Norflurazon desmethyl HM 315 0.010 ^ NT

Novaluron I 315 0.010 ^ 0.01

Omethoate IM 252 0.025 ^ NT

Oxamyl I 315 0.020 ^ NT

Oxyfluorfen H 315 0.20 ^ NT

Parathion ethyl I 315 0.10 ^ NT

Parathion methyl I 315 0.050 ^ NT

Appendix C. Page 3 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Penconazole F 315 0.004 ^ NT

Pendimethalin H 315 0.040 ^ NT

Penthiopyrad F 315 0.002 ^ NT

Permethrin Total I 315 0.20 ^ NT

Phenothrin I 315 0.20 ^ 0.01

Phorate I 315 0.020 ^ NT

Phosalone I 315 0.010 ^ NT

Phosmet I 315 0.20 ^ NT

Phosmet oxygen analog IM 315 0.002 ^ NT

Picoxystrobin F 315 0.006 ^ NT

Piperonyl butoxide I 315 0.025 ^ 10

Prallethrin I 315 0.50 ^ 1.0

Prodiamine H 315 0.020 ^ NT

Profenofos I 315 0.005 ^ NT

Prometon H 315 0.002 ^ NT

Prometryn H 315 0.008 ^ NT

Pronamide H 315 0.050 ^ NT

Propachlor H 315 0.005 ^ NT

Propamocarb hydrochloride F 315 0.005 ^ NT

Propanil H 315 0.010 ^ NT

Propargite I 315 0.005 ^ NT

Propazine H 315 0.005 ^ NT

Propetamphos I 315 0.005 ^ NT

Propiconazole F 315 0.005 ^ NT

Pymetrozine I 315 0.050 ^ NT

Pyraclostrobin F 315 0.005 ^ NT

Pyridaben I 315 0.005 ^ NT

Pyrimethanil F 315 0.010 ^ NT

Pyriproxyfen I 315 0.003 ^ 0.10

Quinoxyfen F 315 0.004 ^ NT

Quintozene (PCNB) F 315 0.010 ^ NT

Resmethrin cis IM 315 0.50 ^ 3.0

Resmethrin trans IM 315 0.50 ^ 3.0

Sethoxydim H 315 0.005 ^ NT

Simazine H 315 0.040 ^ NT

Spinetoram I 315 0.030 ^ NT

Spinosad I 315 0.015 ^ NT

Spirodiclofen A 315 0.008 ^ NT

Spiromesifen I 315 0.050 ^ NT

Spirotetramat I 315 0.005 ^ NT

Sulfoxaflor I 315 0.020 ^ NT

Tebuconazole F 315 0.010 ^ NT

Tebufenozide I 315 0.001 ^ NT

Tebuthiuron H 315 0.005 ^ NT

Tefluthrin I 315 0.005 ^ NT

Tetraconazole F 315 0.005 ^ NT

Appendix C. Page 4 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tetradifon I 315 0.020 ^ NT

Tetrahydrophthalimide (THPI) FM 315 0.25 ^ NT

Tetramethrin I 315 0.20 ^ NT

Thiabendazole F 315 0.010 ^ NT

Thiacloprid I 315 0.005 ^ NT

Thiamethoxam I 315 0.005 ^ 0.02

Thymol F 315 43 13.7 0.007 - 0.21 0.005 ^ EX

Tolfenpyrad I 315 0.008 ^ NT

Triadimefon F 315 0.015 ^ NT

Triadimenol F 315 0.025 ^ NT

Triazophos I 315 0.003 ^ NT

Trifloxystrobin F 315 0.002 ^ NT

Triflumizole F 315 0.002 ^ NT

Trifluralin H 315 0.020 ^ NT

Triticonazole F 315 0.010 ^ NT

Vinclozolin F 315 0.050 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. 

 Refer to pages 3 and 4 in Appendix K to see the number of occurrences broken down by sample origin

 (domestic, imported, or unknown) for a commodity/pesticide pair.

1 = Deltamethrin includes parent Tralomethrin.

2 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

R = Insect Growth Regulator

X = Other (Insect Repellent)

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply 

to 2017 and not to the current year. There may be instances where a tolerance was recently set or revoked that 

would have an effect on whether a residue is violative or not. 

Appendix C. Page 5 of 5
Appendix D

Distribution of Residues by Pesticide

in Milk 

Appendix D shows residue detections for all compounds tested in milk, including range of 

values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this 

summary and appendixes apply to 2017 and not to the current year. There may be 

instances where tolerances have been recently set, modified, or revoked that would have 

an effect on whether a residue is violative or not. 

In 2017, the Pesticide Data Program (PDP) analyzed 711 milk samples. PDP detected 

just 1 pesticide in the milk samples, the insecticide Flubendiamide, which was detected 

in 12 samples at concentrations ranging from 0.003 to 0.005 ppm where the established 

tolerance was 0.15 ppm.

Results for environmental contaminants across all commodities, including milk, have 

been consolidated in a separate appendix because they have no registered uses and are 

not applied to crops (see Appendix F). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

2,4-dimethylphenyl formamide (2,4-DMPF) I 711 0.005 ^ 0.03

2,6-DIPN P 711 0.010 ^ 0.02 *

3-Hydroxycarbofuran IM 711 0.0012 ^ NT

5-Hydroxythiabendazole FM 681 0.0012 ^ 0.1

Abamectin I 711 0.020 ^ 0.015

Acephate I 711 0.005 ^ 0.1

Acetamiprid I 711 0.0012 ^ 0.30

Acetochlor H 711 0.005 ^ 0.02

Acifluorfen H 622 0.050 ^ NT

Alachlor H 711 0.010 ^ 0.02

Aldicarb I 711 0.005 ^ NT

Aldicarb sulfone IM 711 0.0026 ^ NT

Aldicarb sulfoxide IM 711 0.0026 ^ NT

Allethrin I 711 0.010 ^ NT

Ametoctradin F 711 0.0012 ^ NT

Ametryn H 711 0.0012 ^ NT

Amicarbazone H 711 0.005 ^ 0.01

Asulam H 711 0.0012 ^ 0.05

Atrazine H 711 0.0012 ^ 0.02

Azinphos ethyl I 711 0.005 ^ NT

Azinphos methyl I 711 0.005 ^ NT

Azinphos methyl oxygen analog IM 711 0.0026 ^ NT

Azoxystrobin F 711 0.0012 ^ 0.006

Benalaxyl F 711 0.010 ^ NT

Benazolin H 622 0.050 ^ NT

Bendiocarb I 711 0.0012 ^ SU

Benfluralin H 711 0.005 ^ NT

Benoxacor S 711 0.0026 ^ 0.01

Bensulide H 711 0.005 ^ NT

Bentazon H 622 0.0026 ^ 0.02

Bifenazate A 711 0.0026 ^ 0.02

Bifenox H 711 0.010 ^ NT

Bifenthrin I 711 0.0026 ^ 0.1

Bitertanol F 711 0.010 ^ NT

Boscalid F 711 0.0026 ^ 0.10

Bromacil H 711 0.010 ^ NT

Bromopropylate A 711 0.0026 ^ NT

Bromoxynil H 622 0.010 ^ 0.4

Bromuconazole F 711 0.005 ^ NT

Bupirimate F 711 0.0012 ^ NT

Buprofezin I 711 0.0012 ^ 0.01

Butylate H 711 0.020 ^ NT

Cadusafos I 711 0.0012 ^ NT

Carbaryl I 711 0.0026 ^ 1.0

APPENDIX D. DISTRIBUTION OF RESIDUES BY PESTICIDE IN MILK

Appendix D. Page 1 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carbendazim (MBC) F 711 0.0012 ^ NT

Carbofuran I 711 0.0012 ^ NT

Carbophenothion I 711 0.010 ^ NT

Carboxin F 711 0.0026 ^ 0.05

Carfentrazone ethyl H 711 0.0026 ^ 0.05

Chlorantraniliprole I 711 0.005 ^ 0.1

Chlorethoxyfos I 711 0.020 ^ NT

Chlorfenapyr I 622 0.25 ^ 0.01

Chlorfenvinphos total I 711 0.0012 ^ NT

Chlorimuron ethyl H 711 0.0026 ^ NT

Chlorobenzilate A 711 0.0026 ^ NT

Chloroneb F 711 0.005 ^ NT

Chlorothalonil F 711 0.005 ^ 0.1

Chlorpropham H 711 0.0026 ^ 0.30

Chlorpyrifos I 711 0.0026 ^ 0.01

Chlorpyrifos oxygen analog IM 711 0.0012 ^ 0.01

Chlorsulfuron H 711 0.0012 ^ 0.1

Clethodim H 711 0.010 ^ 0.05

Clofentezine I 711 0.005 ^ 0.01

Clomazone H 679 0.0026 ^ NT

Cloransulam Methyl H 711 0.0012 ^ NT

Clothianidin I 711 0.0012 ^ 0.01

Coumaphos I 711 0.0012 ^ 0.5 *

Coumaphos oxygen analog IM 711 0.0012 ^ 0.5 *

Crotoxyphos I 711 0.0026 ^ NT

Crufomate I 711 0.0026 ^ NT

Cyantraniliprole I 711 0.0026 ^ 0.20

Cyazofamid F 711 0.010 ^ NT

Cyclanilide P 622 0.020 ^ 0.04

Cyflufenamid F 711 0.0012 ^ NT

Cyflumetofen A 711 0.0026 ^ NT

Cyfluthrin I 711 0.010 ^ 0.2

Cyhalothrin, Total 1 I 679 0.010 ^ 0.4

Cymoxanil F 711 0.010 ^ NT

Cypermethrin I 711 0.020 ^ 0.10

Cyphenothrin I 711 0.010 ^ NT

Cyproconazole F 711 0.005 ^ 0.02

Cyprodinil F 711 0.005 ^ NT

Cyprosulfamide S 711 0.0026 ^ NT

Cyromazine R 711 0.005 ^ 0.05

DCPA H 711 0.0026 ^ NT

DEF (Tribufos) H 711 0.0012 ^ 0.01

Deltamethrin 2 I 711 0.005 ^ 0.02

Demeton-O IM 711 0.010 ^ NT

Demeton-S IM 711 0.010 ^ NT

Demeton-S sulfone IM 711 0.0012 ^ NT

Appendix D. Page 2 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Dialifos I 711 0.005 ^ NT

Diazinon I 711 0.0012 ^ NT

Diazinon oxygen analog IM 711 0.0012 ^ NT

Dichlobenil H 711 0.0012 ^ NT

Dichlormid H 711 0.020 ^ NT

Dichlorprop H 622 0.050 ^ NT

Dichlorvos (DDVP) I 711 0.020 ^ 0.02

Dicloran F 711 0.020 ^ NT

Diclosulam H 622 0.010 ^ NT

Dicofol o,p' I 711 0.005 ^ 0.75

Dicofol p,p' I 711 0.005 ^ 0.75

Dicrotophos I 711 0.0012 ^ NT

Diethofencarb F 711 0.0026 ^ NT

Difenoconazole F 711 0.0026 ^ 0.02

Diflubenzuron I 711 0.0012 ^ 0.05

Dimethenamid H 711 0.0012 ^ NT

Dimethoate I 711 0.0012 ^ 0.002

Dimethomorph F 711 0.0026 ^ NT

Diniconazole F 711 0.005 ^ NT

Dinotefuran I 711 0.0026 ^ 0.05

Dioxacarb I 711 0.0012 ^ NT

Dioxathion I 711 0.005 ^ NT

Diphenamid H 711 0.005 ^ NT

Diphenylamine (DPA) F 711 0.0026 ^ 0.01

Disulfoton I 711 0.020 ^ NT

Disulfoton sulfone IM 711 0.0012 ^ NT

Disulfoton sulfoxide IM 711 0.0012 ^ NT

Diuron H 711 0.010 ^ NT

DMST (4-dimethylaminosulphotosluidide) FM 711 0.0026 ^ NT

Dodine F 711 0.010 ^ NT

Emamectin I 711 0.010 ^ 0.003

Endosulfan I IM 711 0.020 ^ 2.0 *

Endosulfan II IM 711 0.010 ^ 2.0 *

Endosulfan sulfate IM 711 0.010 ^ 2.0 *

EPN I 711 0.020 ^ NT

Epoxiconazole F 711 0.0026 ^ NT

Esfenvalerate I 679 0.005 ^ 0.3

Ethalfluralin H 711 0.010 ^ NT

Ethiofencarb I 711 0.0026 ^ NT

Ethiofencarb sulfone IM 711 0.0026 ^ NT

Ethiofencarb sulfoxide IM 711 0.0012 ^ NT

Ethion I 711 0.0012 ^ NT

Ethion mono oxon IM 711 0.0012 ^ NT

Ethiprole I 711 0.005 ^ NT

Ethofumesate H 711 0.0026 ^ NT

Ethoprop I 711 0.0012 ^ NT

Appendix D. Page 3 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Ethylan I 711 0.0026 ^ NT

Etofenprox I 711 0.020 ^ 0.60

Etoxazole A 711 0.0012 ^ 0.01 *

Etridiazole F 711 0.040 ^ NT

Famoxadone F 711 0.010 ^ 0.06 *

Fenamidone F 711 0.0012 ^ 0.02

Fenamiphos I 711 0.0012 ^ NT

Fenamiphos sulfone IM 711 0.0012 ^ NT

Fenamiphos sulfoxide IM 711 0.0026 ^ NT

Fenarimol F 711 0.0026 ^ NT

Fenazaquin I 711 0.0012 ^ NT

Fenbuconazole F 711 0.0026 ^ NT

Fenchlorphos (Ronnel) I 711 0.0026 ^ NT

Fenhexamid F 711 0.010 ^ NT

Fenitrothion I 711 0.005 ^ NT

Fenobucarb (BPMC) I 711 0.0026 ^ NT

Fenoxaprop ethyl H 711 0.0012 ^ 0.02

Fenoxycarb I 711 0.0012 ^ NT

Fenpropathrin I 711 0.005 ^ 0.08

Fenpropidin F 711 0.040 ^ NT

Fenpropimorph F 681 0.0012 ^ NT

Fenpyrazamine F 711 0.020 ^ NT

Fenpyroximate A 711 0.0012 ^ 0.015

Fensulfothion I 711 0.0012 ^ NT

Fenthion I 711 0.0026 ^ NT

Fenthion sulfone IM 711 0.020 ^ NT

Fenthion sulfoxide IM 711 0.020 ^ NT

Fenuron H 711 0.005 ^ NT

Fipronil I 622 0.0026 ^ 0.05

Fipronil sulfone (MB46136) IM 622 0.0026 ^ 0.05

Flazasulfuron H 711 0.005 ^ NT

Flonicamid I 711 0.010 ^ 0.05

Fluazifop H 622 0.050 ^ 0.05

Fluazifop butyl H 711 0.0012 ^ 0.05

Fluazinam F 622 0.0026 ^ NT

Flubendiamide I 711 12 1.7

 

0.0046 0.0026 ^ 0.15

Flucythrinate I 679 0.010 ^ NT

Fludioxonil F 711 0.010 ^ 0.01

Flufenacet H 711 0.010 ^ NT

Flufenoxuron I 711 0.0012 ^ 0.20

Flufenpyr ethyl H 711 0.0012 ^ NT

Flumetsulam H 711 0.0026 ^ NT

Flumiclorac pentyl H 711 0.0012 ^ NT

Flumioxazin H 711 0.020 ^ NT

Fluometuron H 711 0.0026 ^ 0.02

Fluopicolide F 711 0.0012 ^ NT

Appendix D. Page 4 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fluopyram F 711 0.0012 ^ 0.40

Fluoxastrobin F 711 0.0012 ^ 0.03

Flupyradifurone I 711 0.0012 ^ 0.15

Fluquinconazole F 711 0.0026 ^ NT

Fluridone H 711 0.0012 ^ 0.05

Fluroxypyr HM 622 0.050 ^ 0.3

Flusilazole F 711 0.0012 ^ NT

Fluthiacet methyl H 711 0.0026 ^ NT

Flutolanil F 711 0.0012 ^ 0.05

Flutriafol F 711 0.0012 ^ 0.02

Fluvalinate I 679 0.010 ^ NT

Fluxapyroxad F 711 0.0012 ^ 0.01

Fomesafen H 622 0.005 ^ NT

Fonofos I 711 0.0026 ^ NT

Forchlorfenuron P 711 0.0012 ^ NT

Formetanate hydrochloride I 711 0.0012 ^ NT

Fosthiazate T 711 0.0012 ^ NT

Furalaxyl F 711 0.010 ^ NT

Halosulfuron methyl H 711 0.020 ^ 0.05

Haloxyfop H 622 0.020 ^ NT

Heptenophos I 711 0.010 ^ NT

Hexaconazole F 711 0.005 ^ NT

Hexazinone H 711 0.005 ^ 11

Hexythiazox I 711 0.0012 ^ 0.05

Hydroprene R 711 0.020 ^ 0.2

Imazalil F 711 0.0026 ^ 0.02

Imazapic H 622 0.005 ^ 0.1

Imazaquin H 622 0.010 ^ NT

Imazethapyr H 622 0.020 ^ NT

Imazosulfuron H 711 0.0026 ^ NT

Imidacloprid I 711 0.0026 ^ 0.10

Imiprothrin I 711 0.010 ^ NT

Indaziflam H 711 0.0012 ^ NT

Indoxacarb I 711 0.005 ^ 0.15

Ipconazole F 711 0.0026 ^ NT

Iprodione F 711 0.010 ^ 0.5

Iprovalicarb F 711 0.0026 ^ NT

Isocarbophos I 711 0.010 ^ NT

Isofenphos I 711 0.0026 ^ NT

Isofenphos methyl IM 711 0.005 ^ NT

Isoprocarb I 711 0.005 ^ NT

Isoproturon H 711 0.0026 ^ NT

Isoxadifen ethyl S 711 0.005 ^ NT

Kresoxim-methyl F 711 0.005 ^ NT

Lactofen H 711 0.0026 ^ NT

Lenacil H 592 0.0026 ^ NT

Appendix D. Page 5 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Leptophos oxygen analog IM 711 0.0026 ^ NT

Linuron H 711 0.0026 ^ 0.05

Lufenuron I 622 0.005 ^ NT

Malathion I 711 0.0026 ^ 0.5 *

Malathion oxygen analog IM 711 0.0012 ^ 0.5 *

Mandipropamid F 711 0.0026 ^ NT

Mecarbam I 711 0.020 ^ NT

Mecoprop (MCPP) H 622 0.25 ^ NT

Mefenpyr diethyl S 711 0.0026 ^ NT

Mepanipyrim F 681 0.0012 ^ NT

Metaflumizone I 711 0.010 ^ NT

Metalaxyl/Mefenoxam 3 F 711 0.0012 ^ 0.02

Metaldehyde O 592 0.10 ^ NT

Metconazole F 711 0.0026 ^ NT

Methamidophos I 711 0.0012 ^ 0.1

Methidathion I 711 0.0026 ^ NT

Methiocarb I 711 0.0012 ^ NT

Methiocarb sulfone IM 711 0.0026 ^ NT

Methiocarb sulfoxide IM 711 0.0012 ^ NT

Methomyl I 711 0.010 ^ NT

Methoxychlor p,p' IM 711 0.005 ^ NT

Methoxyfenozide I 711 0.0026 ^ 0.10

Metolachlor H 711 0.0026 ^ 0.02

Metolcarb I 711 0.010 ^ NT

Metrafenone F 711 0.0012 ^ NT

Metribuzin H 711 0.005 ^ 0.05

Metsulfuron methyl H 711 0.0012 ^ 0.05

Mevinphos Total I 711 0.0026 ^ NT

MGK-264 I 711 0.005 ^ 5

Monocrotophos I 711 0.0026 ^ NT

Monolinuron H 711 0.0012 ^ NT

Myclobutanil F 711 0.0026 ^ 0.2

Napropamide H 711 0.005 ^ NT

Nicosulfuron H 711 0.0012 ^ 0.01

Nitrapyrin N 711 0.020 ^ NT

Nitrofen H 711 0.020 ^ NT

Norflurazon H 711 0.0026 ^ 0.1

Norflurazon desmethyl HM 711 0.0026 ^ 0.1

Novaluron I 711 0.020 ^ 1.0

Omethoate IM 711 0.0012 ^ 0.002

Oryzalin H 622 0.020 ^ NT

Oxadiazon H 711 0.0026 ^ NT

Oxadixyl F 711 0.005 ^ NT

Oxamyl I 711 0.005 ^ NT

Oxamyl oxime IM 711 0.005 ^ NT

Oxydemeton methyl I 711 0.0012 ^ 0.01

Appendix D. Page 6 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Oxydemeton methyl sulfone IM 711 0.0012 ^ 0.01

Oxyfluorfen H 711 0.020 ^ 0.01

Paclobutrazol P 711 0.005 ^ NT

Parathion ethyl I 711 0.005 ^ NT

Parathion methyl I 711 0.020 ^ NT

Parathion methyl oxygen analog IM 711 0.010 ^ NT

Parathion oxygen analog IM 711 0.0026 ^ NT

Penconazole F 711 0.0026 ^ NT

Pencycuron F 711 0.0026 ^ NT

Pendimethalin H 711 0.010 ^ 0.04

Penflufen F 711 0.0012 ^ NT

Penoxsulam H 711 0.0012 ^ NT

Pentachloroaniline (PCA) FM 711 0.0026 ^ NT

Pentachlorobenzene (PCB) FM 711 0.005 ^ NT

Pentachlorophenyl methyl sulfide FM 683 0.020 ^ NT

Penthiopyrad F 711 0.0012 ^ 0.02

Permethrin cis IM 711 0.010 ^ 3.0 *

Permethrin trans IM 711 0.010 ^ 3.0 *

Phenothrin I 683 0.005 ^ 0.01

Phenthoate I 711 0.0012 ^ NT

Phorate I 711 0.020 ^ NT

Phorate oxygen analog IM 711 0.005 ^ NT

Phorate oxygen analog sulfone IM 711 0.0012 ^ NT

Phorate oxygen analog sulfoxide IM 711 0.0012 ^ NT

Phorate sulfone IM 711 0.0026 ^ NT

Phorate sulfoxide IM 711 0.0012 ^ NT

Phosalone I 711 0.0026 ^ NT

Phosmet I 711 0.0012 ^ 0.1

Phosmet oxygen analog IM 711 0.0012 ^ 0.1

Phosphamidon I 711 0.005 ^ NT

Phoxim I 711 0.0012 ^ NT

Picoxystrobin F 711 0.005 ^ 0.01

Pinoxaden H 653 0.020 ^ 0.02

Piperonyl butoxide I 711 0.010 ^ 10

Pirimicarb I 711 0.0012 ^ NT

Pirimicarb desmethyl IM 711 0.0012 ^ NT

Pirimiphos methyl I 711 0.0012 ^ NT

Pirimiphos-ethyl I 711 0.0012 ^ NT

Prallethrin I 711 0.020 ^ 1.0

Primisulfuron methyl H 622 0.005 ^ 0.02

Prochloraz F 711 0.005 ^ NT

Procymidone F 711 0.005 ^ NT

Profenofos I 711 0.005 ^ 0.01

Profluralin H 711 0.020 ^ NT

Profoxydim H 711 0.0026 ^ NT

Promecarb I 711 0.0012 ^ NT

Appendix D. Page 7 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Prometryn H 711 0.0012 ^ NT

Pronamide H 711 0.0026 ^ 0.02

Propachlor H 711 0.0012 ^ 0.02

Propamocarb F 711 0.0012 ^ NT

Propanil H 711 0.010 ^ 0.05

Propaquizafop H 711 0.0012 ^ NT

Propargite I 711 0.0012 ^ 0.08

Propetamphos I 711 0.005 ^ NT

Propham H 711 0.0026 ^ NT

Propiconazole F 711 0.005 ^ 0.05

Proquinazid F 711 0.010 ^ NT

Prosulfuron H 711 0.0026 ^ NT

Prothiofos I 711 0.005 ^ NT

Pymetrozine I 711 0.0012 ^ NT

Pyraclostrobin F 711 0.0012 ^ 0.1

Pyraflufen HM 622 0.020 ^ 0.03

Pyraflufen ethyl H 711 0.0012 ^ 0.03

Pyrasulfotole H 474 0.005 ^ 0.03

Pyrazon H 711 0.0012 ^ 0.02

Pyrazophos F 711 0.0012 ^ NT

Pyridaben I 711 0.0012 ^ 0.01

Pyridalyl I 621 0.040 ^ NT

Pyrimethanil F 711 0.005 ^ 0.05

Pyriproxyfen I 711 0.0012 ^ 0.10

Pyroxasulfone H 711 0.0026 ^ 0.003

Quinalphos I 711 0.0012 ^ NT

Quinoxyfen F 711 0.0012 ^ NT

Quintozene (PCNB) F 711 0.005 ^ NT

Quizalofop HM 622 0.050 ^ 0.01

Quizalofop ethyl H 711 0.0012 ^ 0.01

Resmethrin I 711 0.0026 ^ 3.0

Rimsulfuron H 711 0.0026 ^ NT

Rotenone I 711 0.0026 ^ NT

Saflufenacil H 711 0.0026 ^ 0.01

Sedaxane F 711 0.005 ^ NT

Sethoxydim H 711 0.0026 ^ 0.5

Simazine H 711 0.0012 ^ 0.03

Spinetoram I 711 0.010 ^ 0.30

Spinosad I 711 0.0026 ^ 7.0

Spirodiclofen A 711 0.0026 ^ 0.01

Spiromesifen I 711 0.0026 ^ 0.01

Spiromesifen alcohol IM 711 0.0012 ^ 0.01

Spirotetramat I 711 0.0012 ^ 0.01

Spiroxamine F 711 0.0012 ^ NT

Sulfallate H 711 0.005 ^ NT

Sulfentrazone H 711 0.010 ^ NT

Appendix D. Page 8 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sulfometuron methyl H 711 0.010 ^ NT

Sulfosulfuron H 711 0.005 ^ 0.02

Sulfoxaflor I 711 0.0026 ^ 0.15

Sulprofos I 711 0.0026 ^ NT

TCMTB F 711 0.005 ^ NT

Tebuconazole F 711 0.005 ^ 0.1

Tebufenozide I 711 0.005 ^ 0.04

Tebufenpyrad I 711 0.0012 ^ NT

Tebuthiuron H 711 0.0012 ^ 0.8

Tecnazene P 711 0.010 ^ NT

Teflubenzuron I 622 0.005 ^ NT

Tefluthrin I 711 0.005 ^ NT

Tepraloxydim H 711 0.010 ^ 0.10

Terbacil H 711 0.005 ^ NT

Terbufos I 711 0.0026 ^ NT

Terbufos oxygen analog sulfone IM 711 0.010 ^ NT

Terbufos sulfone IM 711 0.005 ^ NT

Terbufos sulfoxide IM 711 0.0026 ^ NT

Terbuthylazine H 711 0.0012 ^ NT

Tetrachlorvinphos I 711 0.0012 ^ 0.05 *

Tetraconazole F 711 0.005 ^ 0.03

Tetradifon I 711 0.010 ^ NT

Tetrahydrophthalimide (THPI) FM 711 0.020 ^ 0.10

Tetramethrin I 711 0.005 ^ NT

Thiabendazole F 681 0.0012 ^ 0.1

Thiacloprid I 711 0.0012 ^ 0.030

Thiamethoxam I 711 0.0012 ^ 0.02

Thiazopyr H 711 0.0026 ^ NT

Thidiazuron P 711 0.005 ^ 0.05

Thiencarbazone methyl H 711 0.020 ^ 0.02

Thifensulfuron methyl H 711 0.0012 ^ NT

Thiobencarb H 711 0.0026 ^ 0.05

Thiodicarb I 711 0.010 ^ NT

Thionazin I 711 0.0026 ^ NT

Tolclofos methyl F 711 0.005 ^ NT

Tolfenpyrad I 711 0.005 ^ 0.03

Tri Allate H 711 0.005 ^ NT

Triadimefon F 711 0.0026 ^ NT

Triadimenol F 711 0.020 ^ NT

Triasulfuron H 711 0.0012 ^ 0.02

Triazophos I 711 0.0012 ^ NT

Tribenuron methyl H 711 0.0012 ^ NT

Trichlorfon I 711 0.0026 ^ NT

Triclopyr H 622 0.25 ^ 0.60

Tricyclazole F 711 0.0012 ^ NT

Trifloxystrobin F 711 0.0012 ^ 0.02

Appendix D. Page 9 of 10
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Trifloxysulfuron H 711 0.0012 ^ NT

Triflumizole F 711 0.0026 ^ NT

Trifluralin H 711 0.010 ^ NT

Triforine F 592 0.10 ^ NT

Triticonazole F 711 0.005 ^ NT

Uniconazole R 711 0.005 ^ NT

Vinclozolin F 711 0.005 ^ 0.05

Zoxamide F 711 0.0012 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

* = Measured on a fat basis for milk.

NT = No tolerance level was set for that pesticide/commodity pair.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 = Includes cyhalothrin lambda plus R157836 epimer.

2 = Includes parent Tralomethrin.

3 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

N = Nitrification Inhibitor

O = Molluscicide

P = Plant Growth Regulator

R = Insect Growth Regulator

S = Herbicide Safener

T = Nematicide

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2017 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix D. Page 10 of 10
Appendix E

Distribution of Residues by Pesticide

in Bottled Water

Appendix E shows residue detections for all compounds tested in bottled water, including 

range of values detected and range of Limits of Detection (LODs) for each pair. The U.S. 

Food and Drug Administration (FDA) Standards of Quality (SOQ) values for bottled water 

are also shown. 

In 2017, PDP analyzed 756 bottled water samples. PDP detected 10 different residues 

(including metabolites), representing 7 pesticides, in the bottled water samples. All 

detections were well below established FDA SOQs.

Bottled water is regulated by the FDA and State regulatory agencies for the same list of 

pesticides currently regulated in public drinking water by EPA. The Safe Drinking Water 

Act amendments of 1996 require that FDA consider applicability of all EPA MCLs and 

monitoring for bottled water. FDA has adopted EPA’s MCLs for municipal water systems 

as its SOQs for bottled water. The SOQ values can be referenced in the Code of Federal 

Regulations (CFR), Title 21, Part 165.110. 

FDA SOQ values are expressed in parts per million (ppm) in the CFR. Because bottled 

water residues are expressed in parts per trillion (ppt) in the PDP data, the FDA SOQ 

values have been multiplied by a factor of 1,000,000 as a basis for comparison using a 

single scale. There is no intention to imply any more exactness in the value than that 

originally expressed by FDA.

Results for environmental contaminants across all commodities, including bottled water, 

have been consolidated in a separate appendix because they have no registered uses 

and are not applied to crops (see Appendix F). 
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

FDA SOQ, 

ppt 1

2,4-D H 735 6.8 - 45 70,000

3-Hydroxycarbofuran IM 735 9.0 ^

Acetamiprid I 756 6.8 ^

Acetochlor H 756 6.8 ^

Acetochlor ethanesulfonic acid (ESA) HM 756 1 0.1 10.5 ^ 6.3 ^

Acibenzolar S methyl L 735 93.8 ^

Alachlor H 756 11.2 ^ 2,000

Alachlor ethanesulfonic acid (ESA) HM 756 49 6.5 11.3 - 128 6.8 ^

Ametoctradin F 756 6.8 ^

Atrazine H 756 5 0.7 11.3 - 36 6.8 ^ 3,000

Azinphos methyl I 756 45 ^

Azoxystrobin F 756 6.8 ^

Bendiocarb I 756 6.8 ^

Benoxacor S 756 6.8 ^

Bifenthrin I 756 22.5 ^

Boscalid F 756 6.8 ^

Buprofezin I 756 6.8 ^

Carbaryl I 756 6.8 ^

Carbendazim (MBC) F 756 6.8 ^

Carbofuran I 756 6.8 ^ 40,000

Carbophenothion I 756 6.8 ^

Carfentrazone ethyl H 756 112.5 ^

Chlorantraniliprole I 756 11.2 ^

Chlorfenapyr I 756 16.9 ^

Chlorfenvinphos total I 756 11.2 ^

Chlorpropham H 756 6.8 - 22.5

Chlorpyrifos I 756 6.8 ^

Chlorpyrifos oxygen analog IM 756 6.8 ^

Clomazone H 756 16.9 ^

Clothianidin I 756 37.5 ^

Coumaphos I 756 11.2 ^

Coumaphos oxygen analog IM 756 22.5 ^

Cyantraniliprole I 756 16.9 ^

Cyazofamid F 756 45 ^

Cyfluthrin I 756 187.5 ^

Cyhalothrin Total 2 I 756 22.5 ^

Cymoxanil F 756 22.5 ^

Cypermethrin I 756 168.8 ^

DCPA H 756 6.8 ^

Deltamethrin 3 I 756 90 ^

Desethyl atrazine HM 756 22 2.9 11.3 - 36 6.8 ^

Desethyl-desisopropyl atrazine HM 756 22.5 ^

Desisopropyl atrazine HM 756 1 0.1 11.3 ^ 6.8 ^

Diazinon I 714 6.8 ^

APPENDIX E. DISTRIBUTION OF RESIDUES BY PESTICIDE IN BOTTLED WATER

Appendix E. Page 1 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

FDA SOQ, 

ppt 1

Dichlobenil H 756 6.8 ^

Dichlorvos (DDVP) I 756 11.2 ^

Dicofol p,p' I 756 6.8 ^

Dicrotophos I 756 6.8 ^

Difenoconazole F 756 22.5 ^

Dimethenamid H 756 22.5 ^

Dimethoate I 714 18 ^

Dimethomorph F 756 6.8 ^

Dinotefuran I 756 45 ^

Diphenamid H 756 56.3 ^

Disulfoton sulfone IM 756 6.8 ^

Disulfoton sulfone oxygen analog IM 756 6.8 ^

Disulfoton sulfoxide IM 756 6.8 ^

Disulfoton sulfoxide oxygen analog IM 756 6.8 ^

Diuron H 756 93.8 ^

Emamectin benzoate I 756 6.8 ^

Endosulfan I IM 756 33.8 ^

Endosulfan II IM 756 9.0 ^

Endosulfan sulfate IM 756 39.4 ^

EPTC H 756 6.8 ^

Esfenvalerate+Fenvalerate Total I 756 56.3 ^

Ethalfluralin H 756 16.9 ^

Ethion mono oxon IM 756 6.8 ^

Ethoprop I 756 6.8 ^

Etofenprox I 756 37.5 ^

Fenamiphos I 735 6.8 ^

Fenamiphos sulfone IM 756 11.2 ^

Fenamiphos sulfoxide IM 756 11.2 ^

Fenarimol F 756 56.3 ^

Fenbuconazole F 756 6.8 ^

Fenitrothion I 756 16.9 ^

Fenpropathrin I 756 16.9 ^

Fipronil I 756 6.8 ^

Flonicamid I 756 6.8 ^

Fluazifop butyl H 756 6.8 ^

Fludioxonil F 756 45 ^

Flumioxazin H 756 37.5 ^

Fluopicolide F 756 6.8 ^

Fluoxastrobin F 756 6.8 ^

Fluridone H 756 6.8 ^

Fluxapyroxad F 756 6.8 ^

Fonofos I 756 6.8 ^

Imazalil F 756 6.8 ^

Imidacloprid I 756 1 0.1 34 ^ 6.8 ^

Kresoxim-methyl F 756 11.2 ^

Linuron H 756 11.2 ^

Appendix E. Page 2 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

FDA SOQ, 

ppt 1

Malathion I 756 6.8 ^

Malathion oxygen analog IM 756 11.2 ^

Mandipropamid F 756 22.5 ^

Metalaxyl/Mefenoxam 4 F 756 30 ^

Methidathion I 756 6.8 - 22.5

Methomyl I 756 18 ^

Methoprene R 756 112.5 ^

Methoxychlor olefin IM 756 6.8 ^

Methoxychlor Total I 756 6.8 - 45 40,000

Methoxyfenozide I 756 6.8 ^

Metolachlor H 756 1 0.1 47 ^ 6.8 ^

Metolachlor ethanesulfonic acid (ESA) HM 756 29 3.8 11.3 - 153 6.8 ^

Mevinphos Total I 756 11.2 ^

MGK-264 I 756 11.2 ^

Myclobutanil F 756 6.8 ^

Napropamide H 756 37.5 ^

Norflurazon H 756 6.8 ^

Norflurazon desmethyl HM 756 6.8 ^

Oxadixyl F 756 22.5 ^

Oxamyl I 756 45 ^

Oxyfluorfen H 756 6.8 ^

Parathion ethyl I 756 22.5 ^

Parathion methyl I 756 18 ^

Parathion methyl oxygen analog IM 756 6.8 ^

Parathion oxygen analog IM 756 6.8 ^

Pendimethalin H 756 6.8 ^

Penthiopyrad F 756 6.8 ^

Permethrin cis IM 756 6.8 ^

Permethrin trans IM 756 9.0 ^

Phenothrin I 756 16.9 ^

Phenthoate I 756 9.0 ^

Phorate sulfone IM 756 11.2 ^

Phorate sulfoxide IM 756 22.5 ^

Phosalone I 756 11.2 ^

Phosphamidon I 756 6.8 ^

Piperonyl butoxide I 756 37.5 ^

Pirimicarb I 756 6.8 ^

Pirimiphos methyl I 756 6.8 ^

Profenofos I 756 6.8 ^

Prometon H 756 6.8 ^

Prometryn H 756 6.8 ^

Propachlor H 756 22.5 ^

Propetamphos I 756 6.8 ^

Propiconazole F 756 33.8 ^

Pyraclostrobin F 756 6.8 ^

Pyrimethanil F 756 6.8 ^

Appendix E. Page 3 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

FDA SOQ, 

ppt 1

Pyriproxyfen I 756 16.9 ^

Quinoxyfen F 756 9.0 ^

Quintozene (PCNB) F 756 6.8 ^

Resmethrin cis IM 756 56.3 ^

Resmethrin trans IM 756 56.3 ^

Simazine H 756 1 0.1 11.3 ^ 6.8 ^ 4,000

Spinetoram I 756 6.8 ^

Spinosad I 756 6.8 ^

Spiromesifen Total 5 I 756 16.9 ^

Spirotetramat I 756 11.2 ^

Sulfoxaflor I 756 30 ^

Tebuconazole F 756 6.8 ^

Tebufenozide I 756 11.2 ^

Tebupirimfos I 756 6.8 ^

Tebuthiuron H 756 1 0.1 11.3 ^ 6.8 ^

Tecnazene P 756 6.8 ^

Tefluthrin I 756 22.5 ^

Terbacil H 756 22.5 ^

Terbufos sulfone IM 756 6.8 ^

Tetrachlorvinphos I 756 11.2 ^

Tetraconazole F 756 6.8 ^

Tetradifon I 756 16.9 ^

Thiabendazole F 756 6.8 ^

Thiacloprid I 756 6.8 ^

Thiamethoxam I 756 11.2 - 37.5

Thiobencarb H 756 22.5 ^

Triadimefon F 756 6.8 ^

Trifloxystrobin F 756 6.8 ^

Trifluralin H 756 6.8 ^

Vinclozolin F 756 6.8 ^

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

1 = FDA Standards of Quality (SOQ) values have been multiplied by a factor of 1,000,000 as a basis for comparison using 

 a single scale. There is no intention to imply any more exactness in the value than that originally expressed by FDA. 

2 = Includes cyhalothrin lambda plus R157836 epimer.

3 = Includes parent Tralomethrin.

4 = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

5 = Includes parent Spiromesifen plus enol metabolite.

Pesticide Types:

F = Fungicide O = Molluscicide

H = Herbicide, HM = Herbicide Metabolite P = Plant Growth Regulator

I = Insecticide, IM = Insecticide Metabolite R = Insect Growth Regulator

L = Plant Activator S = Herbicide Safener

Appendix E. Page 4 of 4
Appendix F

Distribution of Residues 

for Environmental Contaminants

Appendix F shows residue detections across all commodities for 21 compounds identified as 

environmental contaminants, including range of values detected, range of Limits of Detection 

(LODs), and U.S. Environmental Protection Agency (EPA) tolerances or Action Levels for 

each pair. Results for environmental contaminants have been consolidated in this appendix 

because they have no registered uses and are not applied to crops.

The EPA tolerances cited in this summary and appendixes apply to 2017 and not to the 

current year. There may be instances where tolerances have been recently set, modified or 

revoked that would have an effect on whether a residue is violative or not.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by the U.S. Food and Drug Administration (FDA). Under the Food Quality 

Protection Act, responsibility for establishing tolerances in lieu of ALs has been transferred to 

EPA. In the interim, ALs are used.
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Aldrin (insecticide) (parent of Dieldrin)

Applesauce 570 0 0.003 ^ 0.03 AL

Asparagus 354 0 0.003 ^ 0.03 AL

Cabbage 354 0 0.005 ^ 0.03 AL

Cranberries 311 0 0.005 ^ 0.05 AL

Cranberries, Frozen 428 0 0.005 ^ 0.05 AL

Cucumbers 378 0 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.05 AL

Grapefruit 526 0 0.010 ^ 0.02 AL

Kale 708 0 0.002 ^ 0.05 AL

Lettuce 378 0 0.003 ^ 0.03 AL

Mangoes 177 0 0.001 - 0.010 0.03 AL

Milk 711 0 0.010 ^ 0.3 AL *

Olives, Canned 754 0 0.001 - 0.010 0.05 AL

Onions 708 0 0.001 - 0.005 0.1 AL

Pineapple, Canned 726 0 0.005 - 0.040 0.03 AL

Plums, Dried / Prunes 191 0 0.003 ^ 0.03 AL

Snap Peas 710 0 0.002 ^ 0.03 AL

Sweet Potatoes 701 0 0.045 ^ 0.1 AL

Tomatoes, Canned 566 0 0.001 ^ 0.05 AL

TOTAL 9,440 0

BHC alpha (insecticide) (isomer of BHC)

Applesauce 570 0 0.012 ^ 0.05 AL

Asparagus 354 0 0.012 ^ 0.05 AL

Cabbage 354 0 0.005 ^ 0.05 AL

Cranberries 311 0 0.010 ^ 0.05 AL

Cranberries, Frozen 428 0 0.010 ^ 0.05 AL

Cucumbers 378 0 0.005 ^ 0.05 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.05 AL

Grapefruit 526 0 0.003 - 0.005 0.05 AL

Kale 708 0 0.001 ^ 0.05 AL

Lettuce 378 0 0.012 ^ 0.05 AL

Mangoes 177 0 0.001 - 0.010 0.05 AL

Milk 711 0 0.0026 ^ 0.3 AL *

Olives, Canned 754 0 0.001 - 0.003 0.05 AL

Onions 708 0 0.001 - 0.005 0.05 AL

Pineapple, Canned 726 0 0.005 - 0.010 0.05 AL

Plums, Dried / Prunes 191 0 0.012 ^ 0.05 AL

Sweet Potatoes 701 0 0.010 ^ 0.05 AL

Tomatoes, Canned 566 0 0.001 ^ 0.05 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 9,486 0

BHC beta (isomer of BHC)

Applesauce 570 0 0.014 ^ 0.05 AL

Asparagus 354 0 0.014 ^ 0.05 AL

Cabbage 354 0 0.005 ^ 0.05 AL

Cranberries 311 0 0.005 ^ 0.05 AL

Cranberries, Frozen 428 0 0.005 ^ 0.05 AL

Cucumbers 378 0 0.005 ^ 0.05 AL

Grapefruit 526 0 0.003 - 0.010 0.05 AL

Kale 708 0 0.004 ^ 0.05 AL

Lettuce 378 0 0.014 ^ 0.05 AL

Mangoes 177 0 0.001 - 0.005 0.05 AL

APPENDIX F. DISTRIBUTION OF RESIDUES FOR ENVIRONMENTAL CONTAMINANTS

Appendix F. Page 1 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Milk 711 0 0.0026 ^ 0.3 AL *

Olives, Canned 754 0 0.001 - 0.003 0.05 AL

Onions 348 0 0.005 ^ 0.05 AL

Pineapple, Canned 397 0 0.005 ^ 0.05 AL

Plums, Dried / Prunes 191 0 0.014 ^ 0.05 AL

TOTAL 6,585 0

BHC delta (isomer of BHC)

Grapefruit 271 0 0.005 ^ 0.05 AL

Mangoes 90 0 0.001 - 0.005 0.05 AL

Milk 711 0 0.005 ^ 0.3 AL *

Olives, Canned 754 0 0.001 - 0.005 0.05 AL

TOTAL 1,826 0

Chlordane cis (isomer of Chlordane)

Applesauce 570 0 0.010 ^ 0.1 AL

Asparagus 354 0 0.010 ^ 0.1 AL

Cabbage 354 0 0.005 ^ 0.1 AL

Cranberries 311 0 0.010 ^ NT

Cranberries, Frozen 428 0 0.010 ^ NT

Cucumbers 378 0 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.1 AL

Grapefruit 526 0 0.005 - 0.025 0.1 AL

Kale 708 8 1.1 0.002 ^ 0.001 ^ 0.1 AL

Lettuce 378 0 0.010 ^ 0.1 AL

Mangoes 177 0 0.001 - 0.010 NT

Milk 711 0 0.005 ^ NT

Olives, Canned 754 0 0.001 - 0.005 0.1 AL

Onions 708 0 0.001 - 0.005 0.1 AL

Pineapple, Canned 726 0 0.005 - 0.010 0.1 AL

Plums, Dried / Prunes 191 0 0.010 ^ 0.1 AL

Sweet Potatoes 701 0 0.010 ^ 0.1 AL

Tomatoes, Canned 566 0 0.001 ^ 0.1 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 9,486 8

Chlordane trans (isomer of Chlordane)

Applesauce 570 0 0.010 ^ 0.1 AL

Asparagus 354 0 0.010 ^ 0.1 AL

Cabbage 354 0 0.005 ^ 0.1 AL

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.1 AL

Grapefruit 526 0 0.005 - 0.010 0.1 AL

Kale 708 3 0.4 0.002 ^ 0.001 ^ 0.1 AL

Lettuce 378 0 0.010 ^ 0.1 AL

Mangoes 177 0 0.001 - 0.005 NT

Milk 711 0 0.005 ^ NT

Olives, Canned 754 0 0.001 - 0.005 0.1 AL

Onions 708 0 0.001 - 0.005 0.1 AL

Pineapple, Canned 726 0 0.005 - 0.010 0.1 AL

Plums, Dried / Prunes 191 0 0.010 ^ 0.1 AL

Sweet Potatoes 701 0 0.010 ^ 0.1 AL

Tomatoes, Canned 566 1 0.2 0.004 ^ 0.001 ^ 0.1 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 9,486 4

Appendix F. Page 2 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

DDD o,p' (metabolite of DDT)

Applesauce 570 0 0.001 ^ 0.1 AL

Asparagus 354 0 0.001 ^ 0.5 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.2 AL

Grapefruit 271 0 0.001 ^ 0.1 AL

Lettuce 378 0 0.001 ^ 0.5 AL

Mangoes 90 0 0.001 ^ 0.2 AL

Milk 711 0 0.0012 ^ 1.25 AL *

Olives, Canned 722 0 0.001 ^ 0.1 AL

Onions 360 0 0.001 ^ 0.2 AL

Plums, Dried / Prunes 191 0 0.001 ^ 0.2 AL

Tomatoes, Canned 566 0 0.001 ^ 0.05 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 5,158 0

DDD p,p' (metabolite of DDT)

Applesauce 570 0 0.005 ^ 0.1 AL

Asparagus 354 0 0.005 ^ 0.5 AL

Cabbage 354 0 0.005 ^ 0.5 AL

Cranberries 311 0 0.005 ^ 0.1 AL

Cranberries, Frozen 428 0 0.005 ^ 0.1 AL

Cucumbers 378 0 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.2 AL

Grapefruit 255 0 0.025 ^ 0.1 AL

Lettuce 378 0 0.005 ^ 0.5 AL

Mangoes 87 0 0.005 ^ 0.2 AL

Onions 708 0 0.001 - 0.005 0.2 AL

Pineapple, Canned 726 0 0.005 ^ 0.2 AL

Plums, Dried / Prunes 191 0 0.005 ^ 0.2 AL

Sweet Potatoes 701 0 0.005 ^ 1 AL

Tomatoes, Canned 545 0 0.001 ^ 0.05 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 6,931 0

DDE o,p' (metabolite of DDT)

Applesauce 570 0 0.001 ^ 0.1 AL

Asparagus 354 0 0.001 ^ 0.5 AL

Grapefruit 271 0 0.005 ^ 0.1 AL

Kale 708 1 0.1 0.009 ^ 0.002 ^ 0.5 AL

Lettuce 378 0 0.001 ^ 0.5 AL

Mangoes 90 0 0.001 - 0.005 0.2 AL

Milk 711 0 0.005 ^ 1.25 AL *

Olives, Canned 754 0 0.001 - 0.005 0.1 AL

Plums, Dried / Prunes 191 0 0.001 ^ 0.2 AL

Snap Peas 710 0 0.002 ^ 0.2 AL

TOTAL 4,737 1

DDE p,p' (metabolite of DDT)

Applesauce 475 0 0.010 ^ 0.1 AL

Asparagus 354 0 0.010 ^ 0.5 AL

Cabbage 354 0 0.005 ^ 0.5 AL

Cranberries 311 0 0.005 ^ 0.1 AL

Cranberries, Frozen 428 0 0.005 ^ 0.1 AL

Cucumbers 378 0 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.2 AL

Grapefruit 526 0 0.001 - 0.010 0.1 AL

Honey 315 0 0.005 ^ NT

Appendix F. Page 3 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Kale 708 276 39 0.002 - 0.050 0.001 ^ 0.5 AL

Lettuce 347 0 0.010 ^ 0.5 AL

Mangoes 177 0 0.001 - 0.005 0.2 AL

Milk 711 1 0.1 0.0015 ^ 0.0012 ^ 1.25 AL *

Olives, Canned 691 0 0.001 ^ 0.1 AL

Onions 708 0 0.001 - 0.005 0.2 AL

Pineapple, Canned 726 0 0.005 ^ 0.2 AL

Plums, Dried / Prunes 191 0 0.010 ^ 0.2 AL

Snap Peas 710 11 1.5 0.002 ^ 0.001 ^ 0.2 AL

Sweet Potatoes 701 1 0.1 0.006 ^ 0.005 ^ 1 AL

Tomatoes, Canned 566 0 0.001 ^ 0.05 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 10,322 289

DDT o,p' (insecticide) 

Garbanzo Beans, Canned 189 0 0.001 - 0.003 0.2 AL

Grapefruit 271 0 0.005 ^ 0.1 AL

Kale 708 64 9 0.002 - 0.006 0.001 ^ 0.5 AL

Mangoes 90 0 0.001 - 0.005 0.2 AL

Milk 711 0 0.005 ^ 1.25 AL *

Olives, Canned 754 0 0.001 - 0.005 0.1 AL

Onions 360 0 0.001 ^ 0.2 AL

Snap Peas 710 0 0.001 ^ 0.2 AL

Tomatoes, Canned 566 0 0.001 ^ 0.05 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 5,115 64

DDT p,p' (insecticide) 

Applesauce 570 0 0.001 ^ 0.1 AL

Asparagus 264 0 0.001 ^ 0.5 AL

Cabbage 354 0 0.005 ^ 0.5 AL

Cucumbers 335 0 0.005 ^ 0.1 AL

Grapefruit 271 0 0.005 ^ 0.1 AL

Kale 708 48 6.8 0.003 - 0.007 0.002 ^ 0.5 AL

Lettuce 378 1 0.3 0.002 ^ 0.001 ^ 0.5 AL

Mangoes 90 0 0.001 - 0.005 0.2 AL

Milk 711 0 0.005 ^ 1.25 AL *

Olives, Canned 754 0 0.001 - 0.005 0.1 AL

Onions 708 0 0.001 - 0.030 0.2 AL

Pineapple, Canned 726 0 0.005 - 0.075 0.2 AL

Plums, Dried / Prunes 191 0 0.001 ^ 0.2 AL

Snap Peas 710 0 0.002 ^ 0.2 AL

Sweet Potatoes 701 0 0.075 ^ 1 AL

Tomatoes, Canned 566 0 0.001 - 0.003 0.05 AL

Water, Bottled 756 0 6.8 - 22.5 (ppt)

TOTAL 8,793 49

Dieldrin (insecticide) (also a metabolite of Aldrin)

Applesauce 570 0 0.010 ^ 0.03 AL

Asparagus 354 0 0.010 ^ 0.03 AL

Cabbage 354 0 0.005 ^ 0.03 AL

Cranberries 311 0 0.025 ^ 0.05 AL

Cranberries, Frozen 428 0 0.025 ^ 0.05 AL

Cucumbers 378 1 0.3 0.007 ^ 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.002 ^ 0.05 AL

Grapefruit 526 0 0.020 - 0.025 0.02 AL

Kale 708 78 11 0.003 - 0.019 0.002 ^ 0.05 AL

Appendix F. Page 4 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Lettuce 378 0 0.010 ^ 0.03 AL

Mangoes 177 0 0.003 - 0.025 0.03 AL

Milk 711 0 0.020 ^ 0.3 AL *

Olives, Canned 723 0 0.003 - 0.020 0.05 AL

Onions 708 0 0.002 - 0.005 0.1 AL

Pineapple, Canned 726 0 0.005 - 0.040 0.03 AL

Plums, Dried / Prunes 191 0 0.010 ^ 0.03 AL

Snap Peas 710 0 0.002 ^ 0.03 AL

Sweet Potatoes 701 0 0.045 ^ 0.1 AL

Tomatoes, Canned 566 0 0.002 ^ 0.05 AL

Water, Bottled 756 0 16.9 ^ (ppt)

TOTAL 10,165 79

Endrin (insecticide) 

Applesauce 570 0 0.010 ^ 0.03 AL

Asparagus 354 0 0.010 ^ 0.03 AL

Cabbage 354 0 0.005 ^ 0.03 AL

Cranberries 311 0 0.005 ^ 0.05 AL

Cranberries, Frozen 428 0 0.005 ^ 0.05 AL

Cucumbers 378 0 0.005 ^ 0.1 AL

Garbanzo Beans, Canned 189 0 0.005 ^ 0.05 AL

Grapefruit 526 0 0.010 - 0.030 0.02 AL

Kale 708 2 0.3 0.003 ^ 0.002 ^ 0.05 AL

Lettuce 378 0 0.010 ^ 0.03 AL

Mangoes 177 0 0.003 - 0.010 0.03 AL

Milk 711 0 0.010 ^ 0.3 AL *

Olives, Canned 754 0 0.003 - 0.010 0.05 AL

Onions 708 0 0.005 ^ 0.1 AL

Pineapple, Canned 726 0 0.005 - 0.035 0.03 AL

Plums, Dried / Prunes 191 0 0.010 ^ 0.03 AL

Snap Peas 710 0 0.002 ^ 0.03 AL

Sweet Potatoes 701 0 0.035 ^ 0.1 AL

Tomatoes, Canned 566 0 0.005 ^ 0.05 AL

Water, Bottled 756 0 39.4 ^ (ppt)

TOTAL 10,196 2

Heptachlor (insecticide) 

Applesauce 570 0 0.002 ^ 0.01 AL

Asparagus 354 0 0.002 ^ 0.05 AL

Cabbage 354 0 0.005 ^ 0.05 AL

Cranberries 311 0 0.001 ^ 0.05 AL

Cranberries, Frozen 428 0 0.001 ^ 0.05 AL

Cucumbers 378 0 0.005 ^ 0.05 AL

Garbanzo Beans, Canned 189 0 0.001 ^ 0.05 AL

Grapefruit 526 0 0.005 ^ 0.05 AL

Kale 708 0 0.001 ^ 0.05 AL

Lettuce 378 0 0.002 ^ 0.05 AL

Mangoes 177 0 0.001 - 0.005 NT

Milk 711 0 0.005 ^ 0.1 AL *

Olives, Canned 754 0 0.001 - 0.005 0.01 AL

Onions 708 0 0.001 - 0.005 0.01 AL

Pineapple, Canned 726 0 0.005 - 0.10 0.02 AL

Plums, Dried / Prunes 191 0 0.002 ^ 0.05 AL

Sweet Potatoes 701 0 0.10 ^ 0.01 AL

Tomatoes, Canned 566 0 0.001 ^ 0.01 AL

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 9,486 0

Appendix F. Page 5 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Heptachlor epoxide (metabolite of Heptachlor)

Applesauce 570 0 0.005 ^ 0.01 AL

Asparagus 354 0 0.005 ^ 0.05 AL

Cabbage 354 0 0.005 ^ 0.05 AL

Cranberries 311 0 0.001 ^ 0.05 AL

Cranberries, Frozen 428 0 0.001 ^ 0.05 AL

Cucumbers 378 0 0.005 ^ 0.05 AL

Garbanzo Beans, Canned 189 0 0.002 ^ 0.05 AL

Grapefruit 526 0 0.010 ^ 0.05 AL

Lettuce 378 0 0.005 ^ 0.05 AL

Mangoes 177 0 0.001 - 0.010 NT

Milk 711 0 0.010 ^ 0.1 AL *

Olives, Canned 754 0 0.003 - 0.010 0.01 AL

Onions 708 0 0.002 - 0.005 0.01 AL

Pineapple, Canned 726 0 0.005 - 0.040 0.02 AL

Plums, Dried / Prunes 191 0 0.005 ^ 0.05 AL

Sweet Potatoes 701 0 0.040 ^ 0.01 AL

Tomatoes, Canned 566 0 0.002 ^ 0.01 AL

Water, Bottled 756 0 16.9 ^ (ppt)

TOTAL 8,778 0

Heptachlor epoxide cis (metabolite of Heptachlor)

Kale 708 0 0.003 ^ 0.05 AL

TOTAL 708 0

Hexachlorobenzene - HCB (metabolite and impurity of Quintozene)

Cabbage 354 0 0.005 ^ 0.1

Cranberries 311 0 0.005 ^ NT

Cranberries, Frozen 428 0 0.005 ^ NT

Cucumbers 378 0 0.005 ^ NT

Grapefruit 526 0 0.003 - 0.050 NT

Kale 708 0 0.001 ^ 0.2

Mangoes 177 0 0.001 - 0.005 NT

Milk 711 0 0.0026 ^ NT

Olives, Canned 754 0 0.001 - 0.003 NT

Onions 348 0 0.005 ^ NT

Pineapple, Canned 397 0 0.005 ^ NT

TOTAL 5,092 0

Lindane - BHC gamma (insecticide) (also an isomer of BHC)

Applesauce 570 0 0.013 ^ NT

Asparagus 354 0 0.013 ^ NT

Cabbage 354 0 0.005 ^ NT

Cranberries 311 0 0.005 ^ 0.5 AL

Cranberries, Frozen 428 0 0.005 ^ 0.5 AL

Cucumbers 378 0 0.005 ^ NT

Garbanzo Beans, Canned 189 0 0.001 ^ 0.5 AL

Grapefruit 526 0 0.005 ^ 0.5 AL

Lettuce 378 0 0.013 ^ NT

Mangoes 177 0 0.001 - 0.005 NT

Milk 711 0 0.005 ^ 0.3 AL *

Olives, Canned 754 0 0.001 - 0.005 0.5 AL

Onions 708 0 0.001 - 0.005 NT

Pineapple, Canned 726 0 0.005 - 0.045 NT

Plums, Dried / Prunes 191 0 0.013 ^ NT

Appendix F. Page 6 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Sweet Potatoes 701 0 0.045 ^ 0.5 AL

Tomatoes, Canned 566 0 0.001 ^ NT

Water, Bottled 756 0 6.8 ^ (ppt)

TOTAL 8,778 0

Mirex (insecticide) 

Applesauce 570 0 0.001 ^ NT

Asparagus 354 0 0.001 ^ NT

Lettuce 378 0 0.001 ^ NT

Plums, Dried / Prunes 191 0 0.001 ^ NT

TOTAL 1,493 0

Oxychlordane (metabolite of Chlordane)

Grapefruit 271 0 0.020 ^ 0.1 AL

Mangoes 90 0 0.005 - 0.020 NT

Milk 711 0 0.020 ^ NT

Olives, Canned 754 0 0.005 - 0.020 0.1 AL

TOTAL 1,826 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pair.

* Measured on a fat basis for milk.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.

(ppt) = Findings in bottled water are expressed in parts-per-trillion (ppt). All other findings are expressed in parts-per-million (ppm).

Appendix F. Page 7 of 7
Appendix G

Sample Origin by State or Country

(Determined by Grower, Packer, or Distributor)

Appendix G gives the number of samples per State or country of origin and the number of 

samples of unknown origin. Where available, the origin of fresh commodities is taken from the 

grower or packer information. For processed commodities, origin is determined primarily by 

packer or distributor.

As shown in Appendix G, samples originated from 45 States and 36 foreign countries. There 

were 360 domestic samples from unknown States and 4 mixed national origin samples from 

unknown countries. There were an additional 51 samples from unknown origins. Overall, 72.4 

percent of samples were from U.S. sources, 26.0 percent were imports from single countries, 

1.1 percent were of mixed national origin, and 0.5 percent were of unknown origin.
Part 1. Domestic Samples

# of % of

AS CA CG CU GF GK LT MA ON SN SW AC AZ NC OL PD TC ZB HY MK WB Samples Total

Alabama 1 1 < 0.1

Alaska 1 1 0.0

Arizona 3 1 6 6 5 2 7 18 2 16 4 1 3 74 0.7

Arkansas 7 11 21 1 31 2 24 6 8 6 8 125 1.2

California 6 38 95 4 261 274 318 9 120 173 231 66 58 11 319 81 88 23 42 155 118 2490 23.6

Colorado 20 12 1 17 7 3 7 33 1 101 1.0

Connecticut 1 1 3 2 119 126 1.2

Delaware 2 2 0.0

Florida 4 34 75 12 13 4 6 5 5 1 13 3 5 3 11 41 19 254 2.4

Georgia 5 9 74 39 7 2 1 5 25 167 1.6

Hawaii 4 4 < 0.1

Idaho 52 3 6 5 1 3 1 5 76 0.7

Illinois 4 4 1 6 14 2 45 2 3 32 1 38 13 14 9 18 206 2.0

Indiana 1 1 1 1 1 3 35 5 48 0.5

Iowa 20 20 0.2

Kansas 1 4 4 3 7 2 21 0.2

Kentucky 1 1 2 < 0.1

Louisiana 24 1 25 0.2

Maine 3 33 5 1 9 4 55 0.5

Maryland 1 1 12 30 3 4 3 1 8 4 6 3 3 15 94 0.9

Massachusetts 149 1 1 2 115 2 4 1 275 2.6

Michigan 7 20 14 21 1 28 32 20 1 19 5 10 68 43 289 2.7

Minnesota 2 15 1 2 16 27 27 2 18 17 16 2 145 1.4

Mississippi 106 106 1.0

Missouri 1 4 3 1 11 2 1 7 2 32 0.3

Nebraska 74 74 0.7

Nevada 29 29 0.3

New Hampshire 1 2 1 4 < 0.1

New Jersey 3 6 4 9 7 2 12 22 23 7 24 3 122 1.2

New Mexico 1 18 2 21 0.2

New York 27 12 1 32 12 22 15 1 22 7 4 73 79 307 2.9

North Carolina 11 2 11 181 24 27 30 4 3 19 16 328 3.1

Ohio 13 3 23 12 10 1 18 2 28 4 43 9 7 72 26 271 2.6

Oklahoma 1 1 < 0.1

Oregon 2 2 70 1 5 72 4 5 3 2 7 5 178 1.7

Pennsylvania 3 1 1 4 2 2 55 2 12 15 8 17 31 153 1.5

Rhode Island 1 2 3 < 0.1

South Carolina 30 1 2 33 0.3

Tennessee 25 8 6 39 0.4

Texas 1 21 9 138 49 8 50 10 23 135 12 1 33 9 30 10 22 72 20 653 6.2

Utah 5 5 < 0.1

Vermont 2 1 3 < 0.1

Virginia 1 1 1 16 4 11 8 42 0.4

Washington 2 19 2 6 99 2 39 1 7 2 21 9 209 2.0

Wisconsin 33 5 7 3 2 3 53 0.5

Unknown State 4 6 52 14 19 56 21 3 36 9 68 8 5 1 5 1 7 2 5 38 360 3.4

No. of Domestic 12 245 324 82 501 651 370 12 635 221 700 530 360 23 612 119 538 177 199 707 609 7,627

% of Total 3 79 92 22 95 92 98 7 90 31 100 93 84 3 81 62 95 94 63 99 81 72.4

APPENDIX G. SAMPLE ORIGIN BY STATE OR COUNTRY

(Determined by Grower, Packer, or Distributor)

Fresh F&V Processed F&V Others

Appendix G. Page 1 of 3
Part 2. Imported Samples

# of % of

AS CA CG CU GF GK LT MA ON SN SW AC AZ NC OL PD TC ZB HY MK WB Samples Total

Argentina 18 1 19 0.2

Australia 1 1 < 0.1

Bahamas 1 1 < 0.1

Brazil 67 25 92 0.9

Canada 66 26 30 7 1 10 32 68 1 3 3 10 257 2.4

Chile 1 15 16 0.2

China 32 5 < 0.1

Croatia 2 2 < 0.1

Dominican Republic 4 4 < 0.1

Ecuador 71 71 0.7

Egypt 6 6 0.1

Fiji 35 35 0.3

France 1 64 65 0.6

Guatemala 295 295 2.8

Honduras 19 19 0.2

Iceland 9 9 0.1

India 2 2 < 0.1

Indonesia 117 1 118 1.1

Italy 19 6 25 0.2

Kenya 9 9 0.1

Mexico 160 4 238 10 47 4 27 29 151 1 671 6.4

Morocco 3 3 < 0.1

New Zealand 11 11 0.1

Norway 2 2 < 0.1

Peru 181 32 42 255 2.4

Philippines 202 1 203 1.9

Romania 1 1 < 0.1

South Africa 11 11 0.1

Spain 1 128 1 130 1.2

Sri Lanka 5 5 < 0.1

Thailand 385 385 3.7

Turkey 1 1 < 0.1

Ukraine 2 2 < 0.1

United Kingdom 1 1 < 0.1

Vietnam 13 13 0.1

No. of Imports 342 66 30 293 21 54 5 165 71 488 1 35 68 733 138 34 22 3 35 0 141 2,745

% of Total 97 21 8 78 4 8 1 93 10 69 < 1 6 16 97 18 18 4 2 11 0 19 26.0

Fresh F&V Processed F&V Others

Appendix G. Page 2 of 3
Part 3. Mixed National Origin Samples

# of % of

AS CA CG CU GF GK LT MA ON SN SW AC AZ NC OL PD TC ZB HY MK WB Samples Total

Argentina / Australia / Chile / USA 8 8 0.1

Argentina / Brazil 1 1 < 0.1

Argentina / Canada / India / Ukraine / Uruguay / USA 1 1 < 0.1

Argentina / Canada / India / Ukraine / USA 10 10 0.1

Argentina / Canada / India / Uruguay / USA 6 6 0.1

Argentina / Canada / India / USA 1 1 < 0.1

Argentina / Canada / Mexico 1 1 < 0.1

Argentina / Canada / Mexico / USA 4 4 < 0.1

Argentina / Canada / Ukraine 2 2 < 0.1

Argentina / Canada / Ukraine / USA 3 3 < 0.1

Argentina / Canada / USA 18 18 0.2

Argentina / Chile / France / USA 14 14 0.1

Argentina / Chile / USA 14 14 0.1

Argentina / India / Mexico / Uruguay / USA 1 1 < 0.1

Argentina / USA 6 6 0.1

Argentina / Vietnam / USA 1 1 < 0.1

Brazil / Canada 3 3 < 0.1

Brazil / Mexico 4 4 < 0.1

Brazil / Mexico / Uruguay 4 4 < 0.1

Brazil / Mexico / USA 1 1 < 0.1

Canada / India / Ukraine / USA 1 1 < 0.1

India / Mexico / Ukraine 2 2 < 0.1

India / Ukraine 3 3 < 0.1

India / Ukraine / Vietnam 4 4 < 0.1

India / Vietnam 1 1 < 0.1

Multi-Country Origin - Countries Unknown 13 4 < 0.1

No. of Mixed National Origin Samples 37 81 118

% of Total 19 26 1.1

Part 4. Unknown Origin Samples

# of % of

AS CA CG CU GF GK LT MA ON SN SW AC AZ NC OL PD TC ZB HY MK WB Samples Total

Unknown Origin 3 4 3 3 2 1 5 4 1 6 9 4 6 51 0.5

% of Total 1 1 < 1 1 < 1 < 1 1 1 1 1 5 1 1 0.5

Sample Totals: 354 311 354 378 526 708 378 177 708 710 701 570 428 756 754 191 566 189 315 711 756 10,541

Commodity Legend

 AC = Applesauce GK = Kale ON = Onions

 AS = Asparagus HY = Honey PD = Plums, Dried (Prunes)

 AZ = Cranberries, Frozen LT = Lettuce SN = Snap Peas

 CA = Cranberries, Fresh MA = Mangoes SW = Sweet Potatoes

 CG = Cabbage MK = Milk TC = Tomatoes, Canned

 CU = Cucumbers NC = Pineapple, Canned WB = Water, Bottled

 GF = Grapefruit OL = Olives, Canned ZB = Garbanzo Beans, Canned

Others

Fresh F&V Processed F&V Others

Fresh F&V Processed F&V

Appendix G. Page 3 of 3
Appendix H

Import Versus Domestic Pesticide Residue Comparisons

The Pesticide Data Program is designed to provide a comprehensive statistical picture 

of pesticide residues in the U.S. food supply, representing all sources, including imports. 

Most commodities consumed are generally produced in the United States with import 

components that vary by commodity. However, several commodities tested over the 

past several years were cyclical; that is, part of the year the commodity was produced 

domestically and part of the year it was imported. 

Appendix H compares residue data reported for samples originating in the United States 

with those of the same commodity from major exporting countries in 2017. Residue data 

for domestic snap peas are compared with data for samples originating in both Guatemala 

and Mexico. Only residues detected in more than 5 percent of all samples are included in 

each comparison. All pesticides detected were registered in the United States. However, 

the profiles of residue findings were markedly different in the United States samples 

versus samples from these exporting countries. The differences in residue detections 

between countries were likely due to the pesticides used in response to pest pressures 

based on differing environmental and climatic conditions as well as crop production and 

protection practices. 
Appendix H. Page 1 of 1

Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, ppm

EPA 

Tolerance, 

ppm

Azoxystrobin United States 221 11 5.0 0.003 - 0.33 3.0

Guatemala 295 37 12.5 0.003 - 0.32 3.0

Mexico 151 44 29.1 0.003 - 0.25 3.0

Bifenthrin United States 221 30 13.6 0.002 - 0.11 0.6

Guatemala 295 2 0.7 0.009 - 0.024 0.6

Mexico 151 32 21.2 0.002 - 0.10 0.6

Carbendazim (MBC) United States 221 4 1.8 0.025 - 0.23 NT

Guatemala 295 42 14.2 0.025 - 2.3 NT

Mexico 151 0 0 NT

Chlorantraniliprole United States 221 45 20.4 0.02 - 0.19 2.0

Guatemala 295 1 0.3 0.02 2.0

Mexico 151 20 13.2 0.02 - 0.10 2.0

Cyhalothrin, Lambda United States 221 27 12.2 0.003 - 0.042 0.20

Guatemala 295 115 39.0 0.003 - 0.091 0.20

Mexico 151 3 2.0 0.003 - 0.031 0.20

Cypermethrin United States 221 31 14.0 0.02 - 0.17 0.5

Guatemala 295 30 10.2 0.02 - 0.30 0.5

Mexico 151 27 17.9 0.02 - 0.61 0.5

DCPA United States 221 50 22.6 0.002 - 0.014 NT

Guatemala 295 0 0 NT

Mexico 151 3 2.0 0.002 - 0.014 NT

Dimethoate United States 221 15 6.8 0.025 - 0.16 2.0

Guatemala 295 87 29.5 0.025 - 2.0 2.0

Mexico 151 2 1.3 0.025 - 0.74 2.0

Pyraclostrobin United States 221 10 4.5 0.003 - 0.046 0.5

Guatemala 295 26 8.8 0.003 - 0.14 0.5

Mexico 151 10 6.6 0.003 - 0.19 0.5

Tebuconazole United States 221 7 3.2 0.008 - 0.096 NT

Guatemala 295 69 23.4 0.008 - 0.39 NT

Mexico 151 1 0.7 0.008 NT

Tetrahydrophthalimide (THPI) United States 221 4 1.8 0.025 - 0.036 0.05

Guatemala 295 51 17.3 0.012 - 0.25 0.05

Mexico 151 1 0.7 0.059 0.05

NOTE: The Limits of Detection (LODs) for pesticide detections in snap peas are listed in Appendix B.

Appendix H. Import Versus Domestic Pesticide Residue Comparisons

2017 Distribution of Residues for Snap Pea Samples

Originating in Guatemala and Mexico Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)
Appendix I

Pesticide Residues by Commodity

(Pairs With Residue Detections in at Least 5 Percent of Samples)

Appendix I shows 116 commodity/pesticide pairs (including metabolites, isomers, and 

degradates) with detections in at least 5 percent of the samples tested. The data shown 

include the range and mean of values detected and U.S. Environmental Protection Agency 

(EPA) tolerance references for each pair. The EPA tolerances cited in this summary and 

Appendixes apply to 2017 and not to the current year. There may be instances where 

tolerances have been recently set, modified, or revoked that would have an effect on 

whether a residue is violative or not. 
APPENDIX I. PESTICIDE RESIDUES A

 BY COMMODITY

(Pairs With Residue Detections in at Least 5 Percent of Samples)

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

1 Applesauce (11 pesticides)

Acetamiprid * I 77.2 570 440 0.002 - 0.058 0.013 1.0

Boscalid F 6.7 570 38 0.003 - 0.018 0.007 3.0

Carbendazim (MBC) 1 F 67 570 382 0.001 - 0.060 0.013 2.0

Cyprodinil F 10.4 570 59 0.005 - 0.015 0.007 1.7

Diphenylamine (DPA) F 48.9 570 279 0.002 - 0.12 0.016 10.0

Flubendiamide I 21.2 570 121 0.004 - 0.015 0.006 1.5

Fludioxonil F 14 570 80 0.026 - 0.37 0.081 5.0

Imidacloprid I 8.2 570 47 0.003 - 0.025 0.007 0.5

Pyrimethanil F 24.4 570 139 0.056 - 2.7 0.308 15

Tetrahydrophthalimide (THPI) 2 FM 69.1 570 394 0.010 - 0.45 0.068 25.0

Thiabendazole F 32.3 570 184 0.002 - 0.67 0.077 5.0

2 Asparagus (1 pesticide)

Chlorpyrifos * I 8.8 354 31 0.005 - 0.16 0.04 5.0

3 Cabbage (1 pesticide)

Imidacloprid I 7.9 354 28 0.010 - 0.063 0.022 3.5

4 Cranberries (3 pesticides)

Azoxystrobin F 9.6 311 30 0.001 - 0.005 0.002 5.0

Chlorantraniliprole I 12.2 311 38 0.005 - 0.018 0.008 2.5

Fenbuconazole F 10.3 311 32 0.001 - 0.012 0.002 0.5

5 Cranberries, Frozen (4 pesticides)

Chlorantraniliprole I 8.9 428 38 0.005 - 0.016 0.007 2.5

Fenbuconazole F 13.6 428 58 0.001 - 0.036 0.007 0.5

Methoxyfenozide I 20.6 428 88 0.002 - 0.016 0.005 3.0

Spinetoram I 5.1 428 22 0.001 - 0.005 0.003 0.90

6 Cucumbers (13 pesticides)

Azoxystrobin F 17.5 378 66 0.002 - 0.038 0.008 0.3

Bifenthrin * I 9 378 34 0.005 - 0.029 0.013 0.4

Boscalid F 8.2 378 31 0.010 - 0.26 0.033 0.5

Carbendazim (MBC) 1 F 9.8 378 37 0.010 - 0.051 0.022 1.0

Chlorothalonil F 8.2 378 31 0.005 - 0.64 0.045 5.0

Cyprodinil F 7.9 378 30 0.007 - 0.11 0.022 0.70

Dinotefuran * I 5 378 19 0.010 - 0.16 0.049 0.5

Flonicamid I 7.9 378 30 0.011 - 0.32 0.073 1.5

Fluopicolide F 11.4 378 43 0.010 - 0.12 0.023 0.50

Metalaxyl/Mefenoxam 3 F 25.9 378 98 0.005 - 0.32 0.053 1.0

Propamocarb F 67.5 378 255 0.010 - 0.88 0.13 1.5

Pyraclostrobin F 7.1 378 27 0.003 - 0.082 0.009 0.5

Thiamethoxam * I 10.8 378 41 0.010 - 0.065 0.03 0.2

Appendix I. Page 1 of 4
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

7 Grapefruit (3 pesticides)

Imazalil F 85.6 526 450 0.001 - 0.21 0.032 10.0

Imidacloprid I 16.5 526 87 0.003 - 0.020 0.006 0.70

Thiabendazole F 71.7 526 377 0.001 - 0.20 0.044 10.0

8 Honey (2 pesticides)

2,4-dimethylphenyl formamide I 75.6 315 238 0.003 - 0.082 0.015 0.2

Thymol F 13.7 315 43 0.007 - 0.21 0.059 EX

9 Kale (30 pesticides)

Acetamiprid * I 5.5 708 39 0.017 - 3.6 0.403 15

Ametoctradin F 6.4 708 45 0.003 - 37 2.802 50

Azoxystrobin F 34.3 708 243 0.003 - 11.5 0.989 25

Bifenthrin * I 29.7 708 210 0.002 - 2.5 0.106 3.5

Boscalid F 11.9 708 84 0.017 - 15.7 0.753 18.0

Chlorantraniliprole I 24.3 708 172 0.017 - 7.5 0.533 11

Cyantraniliprole I 7.2 708 51 0.017 - 8.4 0.678 30

Cyfluthrin * I 11.2 708 79 0.013 - 2.6 0.282 7.0

Cyhalothrin, Lambda * I 7.8 708 55 0.003 - 0.33 0.041 0.01

Cypermethrin * I 28.7 708 203 0.020 - 4.2 0.502 14.0

DCPA H 54.9 708 389 0.002 - 0.74 0.037 5.0

Difenoconazole F 5.5 708 39 0.002 - 1.6 0.222 35

Dimethomorph F 5.8 708 41 0.050 - 13.7 1.09 30.0

Fenamidone F 5.8 708 41 0.008 - 8.7 0.521 60

Flonicamid I 5.2 708 37 0.083 - 4.8 0.509 16

Fluopicolide F 29.1 708 206 0.003 - 1.8 0.082 18

Fluopyram F 8.2 708 58 0.003 - 2.5 0.121 50

Flupyradifurone I 6.9 708 49 0.050 - 3.8 0.408 40

Indoxacarb I 9.9 708 70 0.005 - 2.5 0.49 12

Mandipropamid F 18.4 708 130 0.008 - 11.5 0.834 25

Metalaxyl/Mefenoxam 3 F 6.6 708 47 0.007 - 2.6 0.119 0.1

Methoxyfenozide I 11.3 708 80 0.017 - 12.9 1.553 30

Pendimethalin H 8.8 708 62 0.005 - 0.059 0.014 0.20

Penthiopyrad F 7.8 708 55 0.003 - 12 0.717 50

Permethrin Total I 7.6 708 54 0.005 - 4.9 0.367 5.0

Pyraclostrobin F 16.1 708 114 0.003 - 8.8 0.563 16.0

Spinetoram I 12 708 85 0.017 - 0.41 0.066 10

Spinosad I 5.1 708 36 0.003 - 1.2 0.089 10.0

Spirotetramat I 11.9 708 84 0.008 - 0.89 0.086 8.0

Trifluralin H 8.9 708 63 0.002 - 0.016 0.002 0.05

10 Lettuce (11 pesticides)

Boscalid F 6.9 378 26 0.003 - 1.1 0.061 6.5/11.0 &

Cyhalothrin, Total 4 * I 6.9 378 26 0.009 - 0.64 0.093 2.0

Dimethomorph F 19.6 378 74 0.003 - 1.5 0.106 30.0

Fenamidone F 18.3 378 69 0.005 - 3.2 0.161 60

Flonicamid I 5.8 378 22 0.006 - 1.0 0.102 4.0

Imidacloprid I 40.5 378 153 0.003 - 0.087 0.017 3.5

Mandipropamid F 13 378 49 0.002 - 3.1 0.217 20

Metalaxyl/Mefenoxam 3 F 7.4 378 28 0.001 - 0.009 0.003 5.0

Appendix I. Page 2 of 4
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Permethrin

 Permethrin cis 5 IM 6.3 378 24 0.011 - 1.2 0.155 20

 Permethrin trans 5 IM 5.6 378 21 0.010 - 1.5 0.171 20

Propamocarb hydrochloride 6 F 16.7 378 63 0.002 - 3.0 0.182 50/90 &

Thiamethoxam * I 13.8 378 52 0.003 - 0.049 0.01 4.0

11 Mangoes (6 pesticides)

Azoxystrobin F 21.5 177 38 0.001 - 0.51 0.087 2.0

Carbendazim (MBC) F 15.8 177 28 0.001 - 0.015 0.003 NT

Imidacloprid I 14.1 177 25 0.003 - 0.032 0.012 1.0

Pyraclostrobin F 8.5 177 15 0.001 - 0.007 0.002 0.6

Thiabendazole (parent) F 48 177 85 0.001 - 2.0 0.343 10.0

 5-Hydroxythiabendazole 7 FM 16.7 90 15 0.001 - 0.003 0.002 10.0

Trifloxystrobin F 12.4 177 22 0.001 - 0.061 0.02 0.7

12 Olives, Canned (2 pesticides)

Buprofezin I 14.5 754 109 0.001 - 0.057 0.011 3.5

Fenpropathrin I 18.2 754 137 0.001 - 0.16 0.016 5.0

13 Onions (2 pesticides)

Boscalid F 12.9 708 91 0.002 - 0.022 0.004 5.0

Imidacloprid I 6.8 708 48 0.002 - 0.016 0.005 0.15

14 Plums, Dried / Prunes (5 pesticides)

Azoxystrobin F 13.1 191 25 0.002 - 0.025 0.008 2.0

Carbendazim (MBC) 1 F 12 191 23 0.001 - 0.007 0.003 0.5

Diphenylamine (DPA) F 9.4 191 18 0.002 - 0.010 0.004 NT

Methoxyfenozide I 14.1 191 27 0.003 - 0.088 0.015 0.30

Piperonyl butoxide * I 6.8 191 13 0.010 - 0.19 0.053 10

15 Snap Peas (11 pesticides)

Azoxystrobin F 13.2 710 94 0.003 - 0.33 0.052 3.0

Bifenthrin * I 9 710 64 0.002 - 0.11 0.026 0.6

Carbendazim (MBC) 1 F 6.5 710 46 0.025 - 2.3 0.311 NT

Chlorantraniliprole I 9.3 710 66 0.017 - 0.19 0.06 2.0

Cyhalothrin, Lambda * I 20.6 710 146 0.003 - 0.091 0.014 0.20

Cypermethrin * I 12.4 710 88 0.020 - 0.61 0.071 0.5

DCPA H 7.5 710 53 0.002 - 0.014 0.003 NT

Dimethoate I 14.8 710 105 0.025 - 2.0 0.127 2.0

Pyraclostrobin F 6.6 710 47 0.003 - 0.19 0.027 0.5

Tebuconazole F 11.5 710 82 0.008 - 0.39 0.046 NT

Tetrahydrophthalimide (THPI) 2 FM 8 710 57 0.012 - 0.25 0.042 0.05

16 Sweet Potatoes (4 pesticides)

Dicloran F 25.5 701 179 0.022 - 4.7 0.683 10

Fludioxonil F 23 701 161 0.066 - 3.0 0.326 6.0

Piperonyl butoxide I 7.8 701 55 0.015 - 0.80 0.099 10

Thiabendazole F 13.8 701 97 0.006 - 4.1 0.492 10

Appendix I. Page 3 of 4
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

17 Tomatoes, Canned (5 pesticides)

Azoxystrobin F 18.9 566 107 0.002 - 0.015 0.003 0.2

Bifenthrin * I 18.2 566 103 0.002 - 0.018 0.004 0.15

Difenoconazole F 6.5 566 37 0.003 - 0.021 0.008 0.60

Fluxapyroxad F 11.8 566 67 0.002 - 0.030 0.004 0.7

Imidacloprid I 29.9 566 169 0.002 - 0.018 0.003 1.0

NOTES

A Excludes environmental contaminants, which are listed in Appendix F.

NT No tolerance established.

EX Exempt from the requirement of a tolerance.

* Residue may result from food handling establishment (FHE) application.

& Tolerance is different for head and leaf lettuce. First value shown is for head lettuce and the second is for leaf lettuce.

1 From parent, benomyl.

2 Metabolite of captafol and captan.

3 Metalaxyl/mefenoxam are spatial isomers which are analytically indistinguishable via multiresidue methods, but have

separate registrations.

4 Includes cyhalothrin lambda plus R157836 epimer.

5 Isomer of parent, permethrin.

6 Analytically determined as the salt (hydrochloride).

7 Metabolite of parent, thiabendazole.

Pesticide Types:

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

Appendix I. Page 4 of 4
Appendix J

Number of Pesticides Detected per Sample

Appendix J shows the percentage of samples versus the number of pesticides detected per 

sample. The graph and data on page 1 show the overall number of samples and percentages 

(of total number of samples analyzed) for each detection group across all commodities. The 

table on page 2 shows the number of pesticides detected by individual commodity. For the 

10,541 samples analyzed, 53.0 percent of the samples had no detectable pesticides, 19.5 

percent had 1 pesticide, and 27.5 percent of the samples had more than 1 pesticide. 

This appendix reports the number of distinct pesticides rather than residues. A parent compound 

and its metabolites are reported as a single pesticide.
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17

# of

Samples 5,590 2,052 1,207 640 370 256 181 99 57 40 16 14 4 3 3 1 5 3

% of Total

Samples 53.0 19.5 11.5 6.1 3.5 2.4 1.7 0.9 0.5 0.4 0.2 0.1 0.04 0.03 0.03 0.01 0.05 0.03

TOTAL NUMBER OF SAMPLES = 10,541

NOTES

1

 Environmental contaminants, listed in Appendix F, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues."

APPENDIX J. NUMBER OF PESTICIDES 1

 DETECTED PER SAMPLE

40

50

Number of Pesticides Detected per Sample

Number of Pesticides Detected per Sample

30

20

10

60

Percent of Samples

19.5

2.4

3.5

6.1

0. 0.4 0.9 1.7

Multiple pesticide detections may result from the application of more than one pesticide, spray drift, crop 

rotation, and/or cross-contamination.

0.2 0.1 0.04 0.03 0.03 0.01 0.05 0.03

53.0

11.5

Appendix J. Page 1 of 2
Commodity (# of samples) 0123 4 5 6 7 8 9 10 11 12 13 14 15 16 17

Fresh Fruit and Vegetables: Percent

Asparagus (354) 81.1 15.0 2.3 1.7 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Cabbage (354) 74.9 16.7 5.4 2.3 0.6 -- 0.3 -- -- -- -- -- -- -- -- -- -- --

Cranberries (311) 61.1 31.5 7.1 0.3 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Cucumbers (378) 9.3 20.9 26.5 19.8 13.8 5.8 1.6 2.1 0.3 -- -- -- -- -- -- -- -- --

Grapefruit (526) 5.7 24.9 49.8 16.2 3.4 -- -- -- -- -- -- -- -- -- -- -- -- --

Kale (708) 5.4 11.9 11.4 12.1 13.1 11.7 9.5 7.3 5.8 5.4 1.7 2.0 0.6 0.4 0.4 0.1 0.7 0.4

Lettuce (378) 22.2 28.8 19.0 11.9 6.6 4.2 4.0 1.1 1.1 0.5 0.5 -- -- -- -- -- -- --

Mangoes (177) 23.2 33.3 26.0 14.7 1.1 1.7 -- -- -- -- -- -- -- -- -- -- -- --

Onions (178) 76.8 20.3 2.4 0.4 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Snap Peas (710) 27.0 27.6 25.5 13.1 3.8 1.3 1.3 0.1 -- -- 0.3 -- -- -- -- -- -- --

Sweet Potatoes (701) 45.1 38.9 14.4 1.6 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Processed Fruit and Vegetables:

Applesauce (570) 7.4 2.5 8.1 23.0 20.5 18.1 13.7 5.1 1.8 -- -- -- -- -- -- -- -- --

Cranberries, Frozen (428) 62.4 19.2 17.3 1.2 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Garbanzo Beans, Canned (189) 96.8 3.2 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Olives, Canned (754) 64.9 27.9 6.1 1.1 0.1 -- -- -- -- -- -- -- -- -- -- -- -- --

Pineapple, Canned (756) 99.9 0.1 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Plums, Dried/Prunes (191) 48.2 31.4 15.7 4.2 -- 0.5 -- -- -- -- -- -- -- -- -- -- -- --

Tomatoes, Canned (566) 52.1 20.7 9.0 7.2 5.7 3.4 0.9 0.9 0.2 -- -- -- -- -- -- -- -- --

Percent of Total Samples 47.3 20.3 13.2 7.2 4.2 2.9 2.1 1.1 0.7 0.5 0.2 0.2 0.05 0.03 0.03 0.01 0.06 0.03

Actual Number of Samples 4,145 1,775 1,156 632 369 256 181 99 57 40 16 14 4 33153

Honey Product: 

Honey (315) 23.2 61.6 15.2 -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 73 194 48 -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Dairy Product: 

Milk (711) 98.3 1.7 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 699 12 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Water Product: 

Water, Bottled (756) 89.0 9.4 0.4 1.1 0.1 -- -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 673 71 3 8 1 -- -- -- -- -- -- -- -- -- -- -- -- --

NOTES

1 Environmental contaminants, listed in Appendix F, have been excluded from the count of pesticides detected in this appendix. Parent

compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues." 

Number of Pesticides 1 Detected per Sample

TOTAL NUMBER OF FRUIT & VEGETABLE SAMPLES = 8,759

APPENDIX J. NUMBER OF PESTICIDES DETECTED PER SAMPLE

Appendix J. Page 2 of 2
Appendix K

Samples Reported to the

U.S. Food and Drug Administration as

Exceeding the Tolerance

or Without Established Tolerance

(per Code of Federal Regulations, Title 40, Part 180)

Appendix K shows pesticide residues reported to the U.S. Food and Drug Administration (FDA) 

as exceeding the tolerance or residues for which no established tolerance was listed under 

the Code of Federal Regulations, Title 40, Part 180. In 2017, a total of 368 samples with 431 

pesticides were reported to the FDA as Presumptive Tolerance Violations.

Pesticides exceeding the tolerance were detected in 58 samples including 5 samples of 

asparagus, 1 sample of fresh cranberries, 9 samples of cucumbers, 24 samples of kale, 2 

samples of onions, 16 samples of snap peas, and 1 sample of sweet potatoes. Of those 58 

samples, 32 were reported as imported produce.

In addition, 320 samples were found to have pesticides for which no tolerance was established, 

including 239 fresh fruit and vegetable samples, 73 processed fruit/vegetable samples, and 8 

honey samples.

o 270 samples contained 1 pesticide for which no tolerance was established.

o 48 samples contained 2 pesticides for which no tolerance was established.

o 2 samples contained 3 pesticides for which no tolerance was established.

Ten of the 320 samples also contained 1 pesticide each that exceeded an established tolerance.

The columns under the Sample Origin heading provide the number of samples that were of 

domestic, imported, or unknown origin for each pesticide/commodity pair listed.

Appendix K also notes if metabolites (or isomers) were detected as part of the same sample. 

In instances where both parent and metabolite (or isomer) were detected, the Pesticide Data 

Program accounted for both as part of the same tolerance expression.

A number of the findings shown in this appendix are less than 0.01 ppm. Levels below 0.01 

ppm are deemed by the U.S. FDA to be “not of regulatory significance.”
Residues Exceeding Established Tolerance

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm

Country of 

Origin

1 Asparagus / Cypermethrin 0.01 0.14 0.05 Peru

2 Asparagus / Dimethoate 1 0.005 1.8 0.15 Peru

3 Asparagus / Methamidophos 0.005 0.83 0.02 Peru

4 Asparagus / Methamidophos 0.005 0.17 0.02 Peru

5 Asparagus / Methamidophos 0.005 0.041 0.02 Peru

6 Asparagus / Methamidophos 0.005 0.038 0.02 Peru

7 Asparagus / Omethoate 1 0.02 0.28 0.15 Peru

8 Cranberries / Phenothrin 0.025 0.029 0.01 U.S.

9 Cucumbers / Chlorfenapyr 0.005 0.031 0.01 Mexico

10 Cucumbers / Chlorfenapyr 0.005 0.029 0.01 U.S.

11 Cucumbers / Chlorfenapyr 0.005 0.026 0.01 Mexico

12 Cucumbers / Chlorfenapyr 0.005 0.026 0.01 Honduras

13 Cucumbers / Chlorfenapyr 0.005 0.022 0.01 Mexico

14 Cucumbers / Chlorfenapyr 0.005 0.021 0.01 Mexico

15 Cucumbers / Chlorfenapyr 0.005 0.02 0.01 Mexico

16 Cucumbers / Methamidophos 0.01 0.11 0.02 Mexico

17 Cucumbers / Methomyl 0.01 0.68 0.2 U.S.

18 Kale / Cyhalothrin, Lambda 0.002 0.33 0.01 U.S.

19 Kale / Cyhalothrin, Lambda 0.002 0.26 0.01 U.S.

20 Kale / Cyhalothrin, Lambda 0.002 0.23 0.01 U.S.

21 Kale / Cyhalothrin, Lambda 0.002 0.22 0.01 U.S.

22 Kale / Cyhalothrin, Lambda 0.002 0.19 0.01 Canada

23 Kale / Cyhalothrin, Lambda 0.002 0.16 0.01 U.S.

24 Kale / Cyhalothrin, Lambda 0.002 0.12 0.01 Canada

25 Kale / Cyhalothrin, Lambda 0.002 0.11 0.01 U.S.

26 Kale / Cyhalothrin, Lambda 0.002 0.067 0.01 Unknown

27 Kale / Cyhalothrin, Lambda 0.002 0.066 0.01 U.S.

28 Kale / Cyhalothrin, Lambda 0.002 0.061 0.01 Unknown

29 Kale / Cyhalothrin, Lambda 0.002 0.051 0.01 U.S.

30 Kale / Cyhalothrin, Lambda 0.002 0.05 0.01 U.S.

31 Kale / Cyhalothrin, Lambda 0.002 0.04 0.01 U.S.

32 Kale / Cyhalothrin, Lambda 0.002 0.038 0.01 U.S.

33 Kale / Cyhalothrin, Lambda 0.002 0.024 0.01 U.S.

34 Kale / Deltamethrin 2 0.004 1.9 0.05 U.S.

35 Kale / Deltamethrin 2 0.004 0.29 0.05 U.S.

36 Kale / Deltamethrin 2 0.004 0.09 0.05 U.S.

APPENDIX K. SAMPLES REPORTED TO FDA AS EXCEEDING THE TOLERANCE

OR WITHOUT ESTABLISHED TOLERANCE

(per Code of Federal Regulations, Title 40, Part 180)

Appendix K. Page 1 of 4
Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm

Country of 

Origin

37 Kale / Metalaxyl/Mefenoxam 3 0.004 2.6 0.1 Mexico

38 Kale / Metalaxyl/Mefenoxam 3 0.004 1.4 0.1 Mexico

39 Kale / Metalaxyl/Mefenoxam 3 0.004 0.27 0.1 Mexico

40 Kale / Metalaxyl/Mefenoxam 3 0.004 0.2 0.1 U.S.

41 Kale / Tebuconazole 0.005 5.9 2.5 U.S.

42 Onions / Acephate 0.005 0.053 0.02 U.S.

43 Onions / Acephate 0.005 0.036 0.02 U.S.

44 Snap Peas / Cypermethrin 0.012 0.61 0.5 Mexico

45 Snap Peas / Deltamethrin 2 0.004 0.16 0.05 Peru

46 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.25 0.05 Guatemala

47 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.2 0.05 Guatemala

48 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.16 0.05 Guatemala

49 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.14 0.05 Guatemala

50 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.14 0.05 Guatemala

51 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.1 0.05 Guatemala

52 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.073 0.05 Guatemala

53 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.069 0.05 Guatemala

54 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.068 0.05 Guatemala

55 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.064 0.05 Guatemala

56 Snap Peas / Tetrahydrophthalimide (THPI) 4 0.007 0.064 0.05 Guatemala

57 Snap Peas / Thiamethoxam 0.03 0.17 0.02 Mexico

58 Snap Peas / Thiamethoxam 0.03 0.05 0.02 Guatemala

59 Snap Peas / Thiamethoxam 0.03 0.05 0.02 U.S.

60 Sweet Potatoes / Deltamethrin 2 0.12 0.12 0.05 U.S.

Appendix K. Page 2 of 4
Commodity / Pesticide U.S. Import Unk.

1 Asparagus (5 pesticides)

Atrazine 354 1 0.3 0.53 ^ 0.002 ^ 0 1 0

Carbendazim (MBC) 5 294 1 0.3 0.002 ^ 0.001 ^ 0 1 0

Carbofuran (parent) 354 4 1.1 0.005 - 0.13 0.001 - 0.002 0 4 0

 3-Hydroxycarbofuran 6 354 2 0.6 0.003 - 0.035 0.003 ^ 0 2 0

Diphenylamine (DPA) 354 2 0.6 0.004 - 0.007 0.002 ^ 0 2 0

Imidacloprid 354 8 2.3 0.004 - 0.092 0.003 ^ 0 8 0

2 Cranberries (2 pesticides)

Ametoctradin 311 1 0.3 0.003 ^ 0.001 ^ 1 0 0

Chlorpropham 311 1 0.3 0.023 ^ 0.005 ^ 1 0 0

3 Cucumbers (2 pesticides)

Chlorpropham 378 5 1.3 0.006 - 0.047 0.005 ^ 1 4 0

Quinoxyfen 378 1 0.3 0.016 ^ 0.010 ^ 1 0 0

4 Garbanzo Beans, Canned (1 pesticide)

Diphenylamine (DPA) 189 1 0.5 0.021 ^ 0.003 ^ 1 0 0

5 Grapefruit (1 pesticide)

Fenamidone 526 1 0.2 0.001 ^ 0.001 ^ 1 0 0

6 Honey (3 pesticides)

2,6-dichlorobenzamide 315 2 0.6 0.020 - 0.074 0.008 ^ 2 0 0

Alachlor 315 3 1 0.46 - 1.1 0.40 ^ 1 2 0

Carbendazim (MBC) 5 315 3 1 0.005 ^ 0.005 ^ 3 0 0

7 Kale (1 pesticide)

Fenpropathrin 708 1 0.1 0.003 ^ 0.002 ^ 1 0 0

8 Lettuce (7 pesticides)

Carbendazim (MBC) 5 378 1 0.3 0.003 ^ 0.001 ^ 0 1 0

Diflubenzuron 378 1 0.3 0.002 ^ 0.002 ^ 1 0 0

Diphenylamine (DPA) 378 1 0.3 0.004 ^ 0.002 ^ 1 0 0

Diuron 378 2 0.5 0.002 - 0.004 0.002 ^ 2 0 0

Oryzalin 378 1 0.3 0.021 ^ 0.020 ^ 1 0 0

Thiabendazole 378 1 0.3 0.005 ^ 0.002 ^ 1 0 0

Trifluralin 378 1 0.3 0.001 ^ 0.001 ^ 1 0 0

9 Mangoes (4 pesticides)

Carbendazim (MBC) 5 177 28 15.8 0.001 - 0.015 0.001 - 0.010 1 27 0

Chlorpropham 177 6 3.4 0.002 - 0.044 0.001 - 0.005 1 5 0

Diphenylamine (DPA) 90 1 1.1 0.001 ^ 0.001 - 0.003 1 0 0

Flutriafol 177 8 4.5 0.002 - 0.011 0.001 - 0.002 0 8 0

Sample Origin

Distribution of Residues with No Tolerance Listed in 40 CFR, Part 180, 

Range of 

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

by Commodity/Pesticide

Appendix K. Page 3 of 4
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

10 Olives, Canned (4 pesticides)

Carbendazim (MBC) 5 754 25 3.3 0.001 - 0.004 0.001 ^ 25 0 0

Fluridone 754 26 3.4 0.001 - 0.002 0.001 ^ 26 0 0

Tebuconazole 754 13 1.7 0.008 - 0.038 0.003 - 0.005 13 0 0

Trifloxystrobin 754 1 0.1 0.006 ^ 0.001 ^ 0 1 0

11 Onions (1 pesticide)

Methomyl 708 2 0.3 0.004 - 0.014 0.002 - 0.010 2 0 0

12 Pineapple, Canned (1 pesticide)

Carbendazim (MBC) 5 756 1 0.1 0.012 ^ 0.010 ^ 0 1 0

13 Plums, Dried / Prunes (1 pesticide)

Diphenylamine (DPA) 191 18 9.4 0.002 - 0.010 0.002 ^ 9 9 0

14 Snap Peas (6 pesticides)

Buprofezin 710 3 0.4 0.002 - 0.004 0.001 ^ 0 3 0

Carbendazim (MBC) 5 710 46 6.5 0.025 - 2.3 0.015 ^ 4 42 0

DCPA 710 53 7.5 0.002 - 0.014 0.001 ^ 50 3 0

Fenpyroximate 710 1 0.1 0.087 ^ 0.001 ^ 0 1 0

Permethrin Total 704 10 1.4 0.005 - 0.33 0.003 ^ 4 6 0

Tebuconazole 710 82 11.5 0.008 - 0.39 0.005 ^ 7 75 0

15 Sweet Potatoes (2 pesticides)

Chlorpropham 701 3 0.4 0.024 - 0.029 0.020 ^ 3 0 0

Permethrin (parent) 7

 Permethrin cis 701 2 0.3 0.040 - 0.095 0.020 ^ 2 0 0

 Permethrin trans 701 2 0.3 0.027 - 0.12 0.010 ^ 2 0 0

NOTES

1 Omethoate is a metabolite of the parent, Dimethoate. One asparagus sample contained both Dimethoate and Omethoate.

2 Deltamethrin includes parent Tralomethrin.

3 Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

4 Tetrahydrophthalimide (THPI) is a metabolite of Captafol and Captan.

5 Carbendazim (MBC) is a metabolite of Benomyl and Thiophanate methyl.

6 Two asparagus samples contained both Carbofuran and its 3-Hydroxycarbofuran metabolite.

7 Two sweet potato samples contained both the cis and trans permethrin isomers.

Note:

For those pesticide/commodity pairs where the minimum detected value is less than the limit of quantitation (three times

the limit of detection), the reported values are estimates. In a few cases, this may apply to the maximum detected value.

Appendix K. Page 4 of 4
PESTICIDE DATA PROGRAM

 Annual Summary, Calendar Year 2017

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