10 

Sample Data Summary 

VES018659 
11 

Lot-Sample #. 

Date Sampled. 

PARAMETER 

AECOM, Inc 

Client Sample ID: HBTO-03-M26-R1 

General Chemistry 

H9L090423-001 Work Order #...: LQQM7 

12/01/09 Date Received..: 12/04/09 

Matrxx. WASTE 

RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

835 200 mg/kg 

Dilution Factor: 1 

10SO0 1BO0 BTO/lb 

Dilution Factor! 1 

19200 1870 tng/kg 

Dilution Factor: 9.35 

_ METHOD . 

ASTM D482-00a 

MDL : 51 

ASTM D240-02 

MDL : 130 

KNOX WC-001S 

HDL : 560 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/10-12/14/09 9344060 

VES018660 
12 

AECOM, Inc 

Client Sample ID: HBTU-TB-M26-R2 

General ChemistryLot-Sample #. ..: H9L090423-002 Work Ordec #...: LQQNH Matrix, r WASTE 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

ASh Content 566 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : SI 

Gross Calorific 10200 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL. i 130 

Total Chlorine 14700 1200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 6 MDL : 360 

VES018661 
13 

AECOM, Inc . 

Client Sample ID: HBTU-U3-M26-R3 

General Chemistry 

Lot-Sample #...: H9L090423-003 Work Order #....: LQQNJ Matrix : WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS. METHOD ANALYSIS DATE BATCH # 

Ash Content 527 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL ' : 51 

Gross Calorific 10300 1800 BTO/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 16700 1670 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 8.35 MDL ; .500 

VES018662 
14 

AECOM, Inc 

Client Sample ID: LBTU-TJ3-M26-R1 

General Chemistry 

Lot-Sample #...: H9L090423-004 Work Order #..'.:. LQQNL Matrix -: WASTE 

Date Sampled...: 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT Kb . UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 1230 200 mg/kg ASTM D482-O0a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross Calorific ND 1800 BTD/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 873 282 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1:41 MDL : 85 

VES018663 
15 

AECOM, Inc 

Client Sample ID: LBTO-D3-M26-R2 

General Chemistry 

Lot-Sample #...: H9L090423-005 Work Order #..... : LQQNN Matrix : WASTE 

Date Sampled.: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 1170 200 mg/kg ASTM D482-O0a 12/17-12/22/09 9351497 

Dilution Factor.: 1 MDL..: : 51 

Gross Calorific N D ISD O BTU/l b . AST M D240-0 2 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL .: 130 

Total Chlorine 825 278 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.39 MDL : 83 

VES018664 
16 

AECOM, Inc 

Client Sample ID; LBTU-U3-M26-R3 

General Chemistry 

Lot-Sample : H9L090423-00S Work Order #...: LQQNP Matrix ,: WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 2560 200 mg/kg ASTM D4B2-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 HDL : 51 

Gros s Calorifi c ND 1800 BTa/li> ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 HDL : 130 

Total Chlorine 1250 280 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.4 MDL : B4 

VES018665 
17 

AECOM, Inc 

Client Sample ID: SF-tr3-M26A-Rl 

General Chemistry 

Lot-Sample #...: H9L090423-007 Work Order : LQQNT Matrix : WASTE 

Date Sampled...: 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD . ANALYSIS DATE BATCH # 

Ash Content 7600 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL... — : 51 

GrOSS Calorific ND 1800 BTU/lb ASTMD240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 4980 272 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.3 6 MDL... .: 82 

VES018666 
18 

AECOM, Inc 

Client Sample ID: SF-TJ3-M26A-R2 

General Chemistry 

Lot-Sample #...: H9L090423-008 Work Order : LQQNO Matrix : WASTE 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 5620 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross Calorific ND 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 5020 284 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.42 MDL : B5 

VES018667 
19 

ACCOM, Inc 

Client Sample ID: SF-D3-M26A-R3 

General Chemistry 

Lot-Sample #... : H9L090423-009 Work Order #...: LQQN2 Matrix,.; : WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 6020 200 mg/kg ASTM D4S2-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : SI 

Gross Calorific ND 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL 130 ' 

Total Chlorine 5090 282 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.41 MDL : 85 

VES018668 
20 

AECOM, Inc 

Client Sample ID: CS-U3-M26A-R1 

General Chemistry 

Lot-Sample ft...: H9L090423-010 Work Order 

Date Sampled : 12/01/09 Date Received.. 

PARAMETER 

Ash Content 

Gros s Calorifi c 

Value 

Total Chlorine 

RESULT RL UNITS 

699000 200 mg/kg 

Dilution Factors 1 

ND 1B0D BTU/lb 

Dilution Factor: 1 

239 204 mg/kg 

Dilution Factor: 1.02 

LQQN4 

12/04/09 

Matrix. SOLID 

_ METHOD 

ASTM D482-00a 

MDL 51 

ASTM DSB6S-00 

MDL : 130 

KNOX WC-0016 

MDL : 61 

PREPARATION- PREP 

ANALYSIS DATE BATCH S 

12/11-12/15/09 9345461 

12/16/09 9350032 

12/10-12/14/09 9344060 

VES018669 
21 

Lot-Sample # : 

Date Sampled : 

PARAMETER 

AECOM, Inc 

Client Sample ID: CS-03-M2GA-R2 

General Chemistry 

H9L090423-Q11 Work Order #.-.: LQQQR 

12/02/09 Date Received..: 12/04/09 

Matrix. SOLID 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

RESULT RL UNITS 

801000 200 mg/kg 

Dilution Factor: 1 

ND 1800 BTU/lb 

Dilution Factor: 1 

105 B 204 mg/kg 

Dilution Factor.- 1.02 

_ METHOD 

ASTM D482-00a 

MDL : 51 

ASTM D58S5-00 

HDL : 130 

KNOX WC-0016 

MDL : SI 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/11-12/15/09 9345461 

12/15/09 9350032 

12/10-12/14/09 9344060 

NOTE(S): 

RL Reporting Limit 

B Estimated result. Result is less than RL. 

VES018670 
22 

AECOM, Xnc 

Client Sample ID: CS-U3-M26A-R3 

General Chemistry 

Lot-Sample*...: H9L090423-0L2 Work Order #...: LQQQW Matrix : SOLID 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT ' RL • UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 799000 200 mg/kg ASTM D482-0Oa 12/11-12/15/09 9345461 

Dilution Factor: 1 MDL : 51 

Gross Calorific ND 1600 BTU/lb ASTM D5865-OO 12/ie/os 9350032 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 74.9 B 200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1 MDL : SO 

NOTE(S) : \ . 

RL Reporting Limit 

B Estimated result. Result is less than RL. 

VES018671 
23 

AECOM, Inc 

Client Sample ID: HBTU-TJ3-M23A-R1 

General Chemistry 

Lot-Sample #...: H9L090423-013 Work Order # : LQQQ7 

Date Sampled.: 12/01/09 Date Received..: 12/04/09 

Matrix : WASTE 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

937 200 ,mg/kg 

Dilution Factor: 1 

10400 1800 BTO/lfa 

Dilution Factor: 1 

20600 1670 mg/kg 

Dilution Factor: 8.34 

_ METHOD 

ASTM D482-0Oa 

MDL -. 51 

ASTM 1X240-02 

MDL : 130 

KNOX WC-0016 

MDL : 500 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/11-12/16/09 9345064 

VES018672 
24 

AECOM, Inc 

Client Sample ID: HBTU-U3-M23A-R2 

General Chemistry 

Lot-Sample #...: H9L090423-014 Work Order : LQQEM Matrix : WASTE 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP . 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 588 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross Calorific 10300 IBOO BTtr/li ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 14700 1720 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 8.62 MDL .: S20 

VES018673 
25 

AECOM, Inc 

Client Sample ID: HBTU-U3-M23A-R3 

General Chemistry 

Lot-Sample #..-: H9L090423-015 Work Order it... : LQQRO 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

Matrxx. WASTE 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorifi c 

Value 

Total Chlorine 

535 200 mg/kg 

Dilution Factor: 1 

10300 1800 BTTJ/Il, 

Dilution Factor: 1 

16900 1680 mg/kg 

Dilution Factor; 8.33 

_ METHOD 

ASTM D482-O0a 

MDL : SI 

ASTM D240-02 

MDL : 130 

KNOX WC-0016 

MDL...' : 500 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/11-12/16/09 9345064 

VES018674 
26 

AECOM, Inc 

Client Sample TD: LBTU-U3-M23A-R1 

General Chemistry 

Lot-Sample #... i H9L090423-016 Work Order .- LQQR6 Matrix : WASTE 

Date Sampled s 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL • UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 1220 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDI,. : 51 

Gros s Calorifi c KD 1800 BTU/lb . ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 816 276 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.38 MDL : 83 

VES018675 
27 

AECOM, Inc 

Cllent Sample ID: LBT0-O3-M23A-R2 

General Chemistry 

Lot-Sample #...: H9L090423-017 Work Order #...: LQQR7 Matrix : WASTE 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER ' RESOLT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 1260 200 mg/kg ASTM D482-O0a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL SI 

Gros s Calorifi c HD 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL 130 

Total Chlorine 738 282 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.41 MDL.... : SS 

VES018676 
28 

AECOM, Inc 

Client Sample ID:. LBTU-U3-M23A-R3 

General Chemistry 

Lot-Sample #...: H9L090423-018 Work Order #...: LQQR8 Matrix ...: WASTE 

Date Sampled...: 12/03/09 Date Received..:. 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 2420 200 . mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL. •- 51 

Gross Calorific ND 1800 BTD/lb ASTM D240-02 12/14/09 9348075 

. Value 

Dilution Factor: 1 MDL 130 

Total Chlorine 1230 282 mg/kg KNOX WC-0015 12/11-12/16/09 9345064 

Dilution Factor: 1.41 MDL : 85 

VES018677 
29 

AECOM, Inc 

Client Sample ID: SF-03-M23A-R1 

General Chemistry 

Lot-Sample #-..: H9L090423-019 Work Order #...: LQQTA Matrix : WASTE 

Date Sampled...: 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 7290 200 mg/kg ASTM D4B2-O0a 12/17-12/22/09 9351497 

Dilution Factor: 1 ' MDL : 51 

Gross Calorific ND leOO BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 • MDL : 130 

Total Chlorine 5030 274 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.37 MDL : B2 

VES018678 
30 

Lot-Sample #. 

Date Sampled. 

PARAMETER 

Ash- Content 

Gross calorifi c 

Value 

Total Chlorine 

AECOM, Inc 

Client Sample ID: SF-U3-M23A-R2 

General Chemistry 

H9L090423-020 Work Order : LQQTC Matrix : WASTE 

12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

RESULT RL UNITS METHOD • ANALYSIS DATE BATCH # 

6950 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

ND 1S00 BTTJ/lb ASTM D240-02 12/14/09 9348075 

Dilution Factor: 1 MDL : 130 

5010 274 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.37 MDL : 82 

VES018679 
31 

AECOM, Inc 

. Client Sample ID: SF-U3-M23A-H3 

General Chemistry 

Lot-Sample #...: H9L090423-021 Work Order #...: LQQTD Matrix .- WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 7820 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 HDL... .: 51 

Gross Calorific ND IBOO s-cv/xt, ASTM 0240-02 12/14/09 9348075 

Value 

Dilution Factors 1 MDL -.: 130 

Total Chlorine 5020 272 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.36 MDL. : 82 

VES018680 
32 

AECOM, Inc 

Client Sample ID; CS-U3-M23A-R1 

General Chemistry 

Lot-Sample : H9L090423-022 Work Order #...: LQQTE Matrix : SOLID 

Date Sampled...: 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH & 

Ash Content 711000 200 mg/kg ASTM D482-Q0a 12/11-12/15/09 9345461 

Dilution Factors 1 MDL : 51 

Gross Calorific ND 1800 BTU/lb ASTM D5865-00 12/16/09 9350032 

Value 

Dilution Factors 1 MDL : 130 

Total Chlorine 220 200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factors 1 MDL : SO 

VES018681 
33 

AECOM, Inc 

Client Sample TD: CS-U3-M23A-R2 

General Chemistry 

Lot-Sample #.-.: H9L090423-023 Work Order #...:'LQQTF Matrix : SOLID 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 703000 200 mg/kg ASTM D4B2-00a 12/11-12/15/09 9345461 

Dilution Factor; 1 MDL : 51 

Gross Calorific ND ISOO BTu/ib ASTM DS86S-OO 12/16/09 9350032 

Value 

Dilution Factor: 1 MDL... : 130 

Total Chlorine 295 200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1 MDL t 60 

VES018682 
34 

ABCOM, Inc 

Client Sample ID: CS-D3-M23A-E3 

General Chemistry 

Lot-Sample #...: H9L090423-024 Work Order #..-: LQQTG Matrix : SOLID 

Date Sampled.12/03/09 Date Received..: 12/04/09 

PARAMETER 

Ash Content 

RESULT ' RL OMITS 

703000 200 mg/kg 

Dilution Factors 1 

1800 BTtr/lb 

Dilution Factors 1 

204 mg/kg 

Dilution Factors 1.02 

_ METHOD 

ASTM D482-00a 

MDD : 51 

ASTM D5865-00 

MDL. : 130 

KNOX WC-0016 

HDL 61 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/11-12/15/09 934S461 

12/16:/09 9350032 

12/10-12/14/09 9344060 

Gross Calorific ND 

Value 

Total Chlorine 339 

VES018683 
35 

Client Lot #...; H9L090423 

PARAMETER 

Ash Content 

Total Chlorine 

Total Chlorine 

MOTE(S); 

RESULT 

HD 

ND 

ND 

METHOD BLANK REPORT 

General Chemistry 

Matrix. WASTE 

REPORTING 

LIMIT UNITS METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

Work Order #: LQ91G1AA MB Lot-Sample #: H9L170000-497 

200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factort 1 

Work Order #: LQTX01AA MB Lot-Sample #: H9L100DOO-060 

200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor! 1 

Work order #: LQXER1AA MB Lot-Sample #: H9L110000-064 

200 . mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1 

Calculations arc pcrrormcd berore roundinc to avoid round-off errors in calculated results. 

VES018684 
36 

METHOD BLANK REPORT 

General COiemistry 

Client Lot ft...: H9L09O423 Matrix : SOLID 

REPORTING PREPARATION- PREP 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content Work Order #: LQ1E11AA MB Lot-Sample #: H9L110000-461 

ND 200 mg/kg ASTM D482-O0a 12/11-12/15/09 9345461 

Dilution Factor: 1 

NOTE(S) : • 

Calculations arc performed before rounding to uvotd round-off errors in calculated results. 

VES018685 
37 

LABORATORY COHTROL SAMPLE EVALDATIOH REPORT 

General Chemistry 

Lot-Sajnple #...: H9L090423 Mat_cix : WASTE 

PARAMETER 

Ash Content 

PERCENT 

RECOVERY 

99 

99 

RECOVERY 

LIMITS RPD 

RPD 

LIMITS METHOD 

PREPARATIONANALYSIS DATE 

PREP 

BATCH # 

W0#:LQ91G1AC-LCS/LQ91G1AD-LCSD LCS Lot-Sample*: H9L170000-497 

(90 - 110) ASTM D482-O0a 12/17-12/22/09 9351497 

(90 - 110) 0.48 (0-10) ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 

Gross calorifi c 

Value 

100 

99 

W0#;-Q2K71AA-_CS/_Q2R7XAC-_CSD LCS _ofc-S_mple#: H9L140000-07S 

(98 - 102) 

(98 - 102) 0.08 {0-2. 

Dilution Factor: 1 

0) 

ASTM D240-02 

ASTM D240-02 

12/14/09 

12/14/09 

9348075 

9348075 

NOTE(S): 

Calculations arc performed before rounding to avoid round-off errors in calculated results. 

VES018686 
38 

LABORATORY CONTROL SAMPLE DATA REPORT 

General Chemistry 

Lot-Sample : H9L090423 Matrix..-. : WASTE 

SPIKE MEASURED PERCNT PREPARATION- PREP 

PARAMETER AMODNT AMODNT UNITS RECVRY RPD METHOD ANALYSIS DATE BATCH # 

Ash Content WO#:LQ91G1AC-LCS/LQ91G1AD-LCSD LCS Lot-Sample#: H9L170000-497 

4000 3970 mg/kg 99 ASTM D482-O0a 12/17-12/22/09 9351497 

4000 3950 mg/kg 99 0.48 ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: l 

GrOSS Calorific WO# :LQ2R71AA-LCS/LQ2R71AC-LCSD LCS Lot-Sample#: H9L140000-075 

value 

20600 20500 BTU/lb 100 ASTM D240-02 12/14/09 9348075 

20600 20500 BTU/lb 99 0.08 ASTM D240-02 12/14/09 9348075 

Dilution Factor: 1 

NOTE(S) : ; 

Calculations are pcrrormcd before rounding lo avoid round-ofT errors in calculated results. 

VES018687 
39. 

LABORATORY CONTROL SAMPLE EVALUATION REPORT 

General Chemistry 

Client Lot #...: H9L090423 Matrix.- : WASTE 

PERCENT RECOVERY PREPARATION- PREP 

PARAMETER RECOVERY LIMITS METHOD ANALYSIS'DATE BATCH # 

Total Chlorine Work Order #: LQTX01AC LCS Lot-Sample#: H9L100000-OSO 

100 (80 - 120} KNOX WC-001S 12/10-12/14/09 93440S0 

Dilution Factor: S 

Total Chlorine Work Order #: LQXER1AC LCS Lot-Sample*: H9L110000-064 

99 (80 - 120) KNOX WC-OOIS 12/H-1.2/1S/09 9345064 

Dilution. Factor: 5 

NOTE(S) : , 

Calculations arc performed before rounding to avoid round-off errors in calculated results. 

VES018688 
40 

LABORATORY CONTROL SAMPLE DATA REPORT 

General Clteraistry 

Client Lot H9LQ90423 Matrix : WASTE 

SPIKE MEASURED PERCNT PREPARATION- PREP 

PARAMETER AMOUNT AMOUNT UNITS RECVRY METHOD ANALYSIS DATE BATCH # 

Total Chlorine Work Order #: LQTX01AC LCS Lot-Sample#: H9L100000-OSO 

10000 9980 rng/kg 100 KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: S 

Total Chlorine Work Order 4: LQXER1AC LCS Lot-Samples.- H9L110000-064 

10000 9850 mg/kg 99 KNOX WC-001S X2/ll-12/16/09 9345064 

Dilution Factor: 5 

NOTE (S) ; 

Calculations arc performed before rounding to avoid round-ofT errors in calculated results. 

VES018689 
41 

LABORATORY CONTROL SAMPLE EVALUATION REPORT 

General Chemistry 

Lot-Sample #...: H9L090423 Matrix : SOLID 

PARAMETER 

Ash Content 

PERCENT 

RECOVERY 

100 

100 

RECOVERY 

LIMITS RPD 

RPD 

LIMITS METHOD 

PREPARATIONANALYSIS DATE PREP 

BATCH # 

W0#:LQ1E11AC-LCS/LQ1E11AD-LCSD LCS Lot-Sample#: H9L11OOO0-461 

(90 - 110} ASTM D482-00a 12/11-12/15/09 9345461 

(90 - 110) 0.42 (0-10) ASTM D482-00a 12/11-12/15/09 9345461 

Dilution Factor; 1 

Gross Calorific 

Value 

100 

100 

WO#:LQ5BPlAA-LCS/LQ58PlAC-LCSD LCS Lot-Sample#: H9L160000-032 

(98 - 102) . ASTM D5865-00 

(98 - 102) 0.10 (0-2.0) ASTM D5865-00 

Dilution Factor: 1 

12/16/09 

12/16/09 

9350032 

9350032 

NOTE(S) : 

Calculations arc performed before rounding to avoid round-off errors in calculated results. 

VES018690 
42 

LABORATORY COHTROL SAMPLE DATA REPORT 

General Chemistry 

Lot-Sample # : H9L090423 Matrix : SOLID 

SPIKE MEASURED PERCNT PREPARATION- PREP 

PARAMETER AMOUNT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE BATCH # 

Ash Content W0#;LQ1E11AC-LCS/LQ1E11AD-LCSD LCS Lot-Sample*: H9L11O000-4S1 

4000 4010 mg/kg 100 ASTM D482-00a 12/11-12/15/09 9345461 

4000 3990 mg/kg 100 0.42 ASTM D482-00a 12/11-12/15/09 9345461 

Dilution Factor: 1 

Gross Calorific WO#:LQ58PlAA-LCS/LQ58PlAC-LCSD LCS Lot-Sample#: H9L160000-032 

Value 

11400 11300 BTU/lb 100 ASTM D5865-00 12/16/09 9350032 

'11400 11300 BTU/lb 100 0.10 ASTM D5865-00 12/16/09 9350032 

Dilution Factor: 1 

NOTE(S) : 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

VES018691 
43 

MATRIX SPIKE SAMPLE EVALUATION REPORT 

General Chemistry 

Client Lot #. 

Date Sampled. 

,: H9L090423 

.: 12/01/09 Date Received.. 12/04/09 

PARAMETER 

Total Chlorine 

100 

97 

PERCENT RECOVERY 

RECOVERY LIMITS RPD 

RPD 

LIMITS METHOD 

Matrix. WASTE 

PREPARATION -

ANALYSIS DATE 

PREP 

BATCH # 

WO#: LQQNN1AG-MS/LQQNN1AH-MSD . MS Lot-Sample #: H9L090423-005 

(80 - 120) KNOX WC-0016 12/10-12/14/09 9344060 

(80 - 120) 3.5 (0-10) KNOX WC-0016 12/10-12/14/09 93440S0 

Dilution Factor: 7.07 

Total Chlorine W0#: LQQNT1AE-MS/LQQNT1AF-MSD MS Lot-Sample #: H9L090423-007 

101 (80 - 120) KNOX WC-0016 12/11-12/16/09 9345064 

101 (80 - 120) 3.2 (0-10) KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 7.1 

NOTE(S) ; 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

VES018692 
44 

MATRIX SPIKE SAMPLE DATA REPORT 

General Chemis tryClient Lot #...: H9L090423 

Date Sanrpled...; 12/01/09 Date Received._: 12/04/09 

Matrix. WASTE 

SAMPLE SPIKE MEASRD 

PARAMETER AMODNT AMT 

Total Chlorine 

.825 14100 

825 14000 

AMOUNT. UNITS 

PERCNT 

RECVRY RPD METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

WO#: LQQNNIAG-MS/LQQNNIAH-MSD MS Lot-Sample #.- H9L090423-005 

15000 mg/kg 100 KNOX WC-0016 12/10-12/14/09 9344060 

14500 mg/kg 97 3.5 KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 7.07 

Total Chlorine 

49B0 14200 

4980 13600 

WO#: LQQNT1AE-MS/LQQNT1AF-MSD MS Lot-Sample #: H9L090423-007 

19300 mg/kg 101 KHOX WC-0016 12/11-12/16/09 9345064 

18700 mg/kg 101 3.2 KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 7.1 

NOTE(S) : 

Calculaiions arc pcrrormcd before rounding io avoid round-off errors in calculated results. 

VES018693 
45 

MATRIX SPIKE SAMPLE EVALUATION REPORT 

General Chemistry 

Client Lot ft...; H9L090423 

Date Sampled : 12/02/09 Date Received. 12/04/09 

Matrix. SOLID 

PARAMETER 

Total Chlorine 

90 

91 

PERCENT RECOVERY 

RECOVERY LIMITS RPD 

RPD 

LIMITS METHOD 

.PREPARATIONANALYSIS DATE PREP 

BATCH # 

WO#: LQQQR1AG-MS/LQQQR1AH-MSD MS Lot-Sample #: H9LO90423-011 

(80 - 120) KNOX WC-0016 12/10-12/14/09 9344060 

(80 - 120) 0.77 (0-10) KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 4.73 

NOTE(S) : 

Calculaiions arc performed before rounding to avoid round-ofT errors in calculaied results. 

VES018694 
46 

MATRIX SPIKE SAMPLE DATA REPORT 

General _enustry 

Client Lot #...: H9L090423 

Date Sampled...: 12/02/09 

Matrxx. SOLID 

Date Received..: 12/04/09 

SAMPLE SPIKE . MEASRD 

PARAMETER AMOUNT AMT 

Total Chlorine 

105 9470 

105 9450 

AMODNT UNITS 

PERCNT 

RECVRY RPD METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

WO#: LQQQR1AG-MS/LQQQR1AH- MSD MS Lot-Sample #: H9L090423-011 

8640 mg/kg 90 KNOX WC-0016 12/10-12/14/09 9344060 

8710 mg/kg 91 0.77 KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 4.73 

NOTE(S) : 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

VES018695 
47 

SAMPLE DUPLICATE EVALUATION REPORT 

General Chemistry 

Client Lot #...: H9L090423 Work Order #...: LQQNN-SMP Matrix : WASTE 

LQQNN-DUP 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

DUPLICATE RPD PREPARATION- PREP 

PARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH # 

Gross Calorific SD Lot-Sample #: H9L090423-005 

Value 

ND ND BTU/lb 13 (0-10) ASTM D240-02 12/14/09 9348D75 

Dilution Factor: 1 

Ash Content SD Lot-Sample #: H9L090423-005 

1170 1210 mg/kg 3.1 (0-10) ASTM D4B2-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 

Total Chlorine SD Lot-Sample #: H9L090423-005 

825 818 mg/kg 0.82 (0-10) KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.33 

VES018696 
48 

Client Lot S-.. 

Date Sampled... 

PARAM RESULT 

Total Chlorine 

4980 

H9L090423 

12/01/09 

DUPLICATE 

RESULT 

SAMPLE DUPLICATE EVALUATION REPORT 

General Chemistry 

Work Order #...: LQQNT-SMP 

LQQNT-DUP 

Date Received..: 12/04/09 

UNITS 

RPD 

RPD LIMIT METHOD 

Matrxx. WASTE 

PREPARATION- PREP 

ANALYSIS DATE BATCH 8 

SD Lot-Sample #: H9L090423-007 

S000 mg/kg 0.42 (0-10) KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factors 1.36 

VES018697 
49 

Client Lot #-.. 

Date Sampled... 

PARAM RESULT 

SAMPLE DUPLICATE EVALUATION REPORT 

General Chemistry 

H9L09Q423 Work Order #...t LQQQR-SMP 

LQQQR-DUP 

12/02/09 Date Received..: 12/04/09 

Total Chlorine 

105 B 

DUPLICATE 

RESULT UNITS 

99.6 B 

RPD 

RPD LIMIT METHOD 

Matrix : SOLID 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

mg/kg 5.3 

Dilution Factor: 1.02 

SD Lot-Sample #: H9L090423-011 

(0-10) KNOX WC-0016 12/10-12/14/09 934406.0 

Gross Calorific 

Value 

ND ND BTD/lb 0 

Dilution Factor: 1 

SD Lot-Sample #: H9L090423-011 

(0-10) ASTM D5865-00 12/15/09 9350032 

Ash Content 

801000 784000 mg/kg 

Dilution Factor: 1 

SD Lot-Sample #: H9L090423-011 

2.2 (0-10) ASTM D482-O0a 12/11-12/15/09 9345461 

NOTE(S) : 

Calculations arc performed before rounding to avoid round-off errors in calculated results. 

B Estimated result, Result is less than RL, 

VES018698 
50 

SAMPLE DUPLICATE EVALUATION REPORT 

General Chemistry 

Client Lot H9L090423 Work Order #...: LQQRO-SMP Matrix ..: WASTE 

LQQRO-DUP 

Date Sampled : 12/03/09 Date Received..: 12/04/09 

DUPLICATE RPD PREPARATION- PREP 

PARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH # 

Gross Calorific SD Lot-Sample #: H9L090423-015 

Value 

10300 10100 BTU/lb 1.4 (0-10) ASTM D240-02 12/14/09 9348075 

Dilution Factor: 1 

VES018699 
51 

Client Lot #...: H9L090423 

Date Sampled : 12/02/09 

SAMPLE DDPLICATE EVALUATION EEPORT 

General Chemistry 

Work Order #...: LQQTC-SMP 

LQQTC-DUP 

Date Received..: 12/04/09 

PARAM RESULT 

Total Chlorine 

5010 

DUPLICATE 

RESULT 

5100 

Matrxx. WASTE 

• UNITS 

RPD 

RPD LIMIT METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

SD Lot-Sample #: H9L090423-020 

mg/kg 1.9 (0-10) KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.37 

VES018700 
52 

Client Lot #. 

Date Sampled. 

PARAM RESULT 

Ash Content 

7820 

H9L090423 

12/03/09 

DUPLICATE 

RESULT . 

SAMPLE DUPLICATE EVALUATION REPORT 

General Chemistry 

Work Order #...: LQQTD-SMP 

LQQTD-DUP 

Date Received..t 12/04/09 

UNITS 

RPD 

RPD LIMIT METHOD 

Matrix. WASTE 

5910 rag/kg 12 

Dilution Factor: 1 

PREPARATION- PREP 

ANALYSIS DATS BATCH # 

SD Lot-Sample #: H9L090423-021 

(0-10) ASTM D482-00a 12/17-12/22/09 9351497 

VES018701 
53 

1 

Sample Receipt Documentation 

VES018702 
Sample Traceability List 

AECOM 

Site of Proqram: Veolia ES Tech Sample Date: &/ i - (ZtAfoR Project Location: Sauqet, IL P.O.#: 

Type of Program: CPT Date Shipped: 1^tJ.jnlhff Laboratory: Test America, Inc. 

Project* 60133216 Knoxville, TN 

Proqram Office: Syracuse NY 

Shipper/ Steven Milo 

Recovery: Jeff Gorman 

Laboratory: Test America, Inc. 

Knoxville, TN 

Program Contact: Jeff Gorman FedEx Air Bill #: 

Item Sample 10 Code Sample Matrix Sample Description Analitlcal Parameters Special Instructions 

21 M HBTU-U3-M26-R1 Liquid High Btu, Unit 3, Run 1 Physical Parameters & Cl 

22 x HBTU-U3-WI26A-R2 Liquid High Btu, Unit 3, Run 2 Physical Parameters & Cl 

23 > HBTU-U3-M26A-R3 Liquid High Btu, Unit 3, Run 3 Physical Parameters & Cl 

24 

25 iv< LBTU-U3-M26A-R1 Liquid Low Btu, Unit 3 Run 1 Physical Parameters & Cl \C> fHTfi)& 

26 x L.BTU-U3-M26A-R2 Liquid Low Btu, Unit 3 Run 2 Physical Parameters & Cr^Ofijr; $^ ] 

27 i LBTU-U3-M26A-R3 Liquid Low Btu, Unit 3 Run 3 Physical Parameters & Cl f? J55 

28 * 5 

29 U-t SF-U3-WI26A-R1 Liquid Speciality Feeder, Unit 3, Run 1 Physical Parameters & Cl §/,A I* 5 

30 % SF-U3-M26A-R2 Liquid Specllaity Feeder, Unit 3, Run 2 Physical Parameters & Cl ftf p £ 

31 ^ SF-U3-M26A-R3 Liquid Speciality Feeder, Unit 3, Run 3 Physical Parameters & Cl ft| f£\ £ 

32 

33 CS-U3-M26A-R1 Solid Containerized Solids, Unit 3, Run 1 Physical Parameters & Clfif nC\\0

 e 

34 \ CS-U3-WI26A-R2 Solid Containerized Solids, Unit 3, Run 2 Physical Parameters & Cl $}j)0[ [ft t -2.-1*31 

35 V CS-U3-M26A-R3 Solid Containerized Solids, Unit 3, Run 3 Physical Parameters & CIQ j„tPl \A

 t=; 

36 . 8 ^ t 

. 37 

38 

39 

40 

Field Notes/ Comments 1. Physical Parameters = Total chlorides, heat content 5 ash content. 

2. Cl 

Page 2 of 2 _ 

Relinquished By (print): Date:. 

Signature: > Time: 

Xto,j&r, riyuL !~7O0 

Relinquished By (print): Date: 

Signature: Time: 

Relinquished By (print): Date: 

Signature: Time: 

Received by Lab (print): Date: \ n,\A\\ 

Received By (print): Date: 

Signature: Time: 

Received By (print): Date: 

Signature: Time: 

Received By (print): Date: 

Signature: Time: 

Analytical Laboralorv Destination: 

TestAmerica Inc. 

5815 Middlebrook Pike 

Knoxville, TN 37921 

Attn: Mr, Kevin Woodcock 865-291-3000 

VES018703 
Sample Traceability List 

AECOM 

Site of Program: Veolia ES Tech Sample Date: t.±j/icf- AZ/JM^ Project Location: Saupjet, IL P.O. * 

Type of Program: CPT Date Shipped: /Jl/j} Jo 9 Laboratory: Test America, Inc. 

Project* 60133216 Shipper/ Steven Milo Knoxville, TIM 

Recovery: Jeff Gorman 

Laboratory: Test America, Inc. 

Knoxville, TIM 

Program Office: Syracuse NY 

Shipper/ Steven Milo 

Recovery: Jeff Gorman 

Laboratory: Test America, Inc. 

Knoxville, TIM 

Program Contact: Jeff Gorman • -

;:v--y.'' • ' " !'.:.:- ' • FedEx Air Bill* 

Item Sample ID Code Sample Matrix Sample Description Analitical Parameters Special Instructions 

1 HBTU-U3-M23A-R1 - Liquid High Btu, Unit 3, Run 1 Physical Parameters & Cl 

2 HBTU-U3-M23A-R2

 x Liquid High Btu. Unit 3, Run Z Physical Parameters & Cl 

3 HBTU-U3-M23A-R3 _ Liquid High Btu, Unit 3, Run 3 Physical Parameters & Cl 

4 

5 LBTU-U3-IW23A-R1 Liquid Low Btu, Unit 3 Run 1 Physical Parameters & Cl 

6 L.BTU-U3-M23A-R2 Liquid Low Btu, Unit 3 Run 2 Physical Parameters & Cl 

7 LBTU-U3-M23A-R3 - Liquid Low BlU, Unit 3 Run 3 Physical Parameters & Cl 

8 

9 SF-U3-M23A-R1 Liquid Speciality Feeder, Unit 3, Run 1 Physical Parameters & Cl 

10 SF-U3-M23A-R2 Liquid Specilaity Feeder, Unit 3, Run 2 Physical Parameters & Cl 

11 SF-U3-WI23A-R3 Liquid Speciality Feeder, Unit 3, Run 3 Physical Parameters & Cl 

12 

13 CS-U3-M23A-R1 Solid Containerized Solids, Unit 3, Run 1 Physical Parameters & CI 

14 CS-U3-M23A-R2 Solid Containerized Solids, Unit 3, Run 2 Physical Parameters & Cl 

15 CS-U3-M23A-R3 Solid Containerized Solids, Unit 3, Run 3 Physical Parameters & Cl 

16 

17 

18 

19 

20 

Field Notes/ Comments 1. Physical Parameters = Total chlorides, heat content & ash content. 

2. Cl 

Page 1 of_2 

Relinquished By (print): Date: llRelinqulsbed By (print): Date: 

Signature: Time: [Signature: Time: 

(700 1 

Relinquished By (print): Date: 

Signature: Time: ^ ~ 

Received by Lab (print): Date: 

~%U tbVYMT-H rUijM 

femA fflffe 

Received By (print): Date: IjReceived By (print): Date: 

Signature: Time: Signature: Time: 

Received By (print): Date: 

Signature: Time: 

Received By (print): Date: IjReceived By (print): Date: Analytical Laboratory Destination: 

Signature: Time: Signature: Time: 

Received By (print): Date: 

Signature: Time: 

Test America Inc. 

5815 Middlebrook Pike 

Knoxville, TN 37921 

Attn: Mr. Kevin Woodcock 865-291-3000 

Ol 

VES018704 
TESTAMERICA KNOXVILLE SAMPLE RECEIPT/CONDITION UPON RECEIPT ANOMALY CHECKLIST 

Lot Number: VWUflMaT . 

Review Items f NA If No, what was the problem? Comments/Actions Taken 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

1. Do sample container labels match COC? 

(IDs, Dates, Times) J 

1-

• la Do not match COC 

• lb Incomplete infonnation 

0 lc Marking smeared 

O l d Label torn 

• leNo label 

• UCO C not received 

• lg Other: 

2. Is the cooler temperature within limits? (> freezing 

temp, of water to 6°C;NC, 1668,1613B: 0-4°C; 

VOST: 10°C;MA:2-6',C) 

J 2. Is the cooler temperature within limits? (> freezing • 2aTeniD Blank = 

temp, of water to 6°C;NC, 1668,1613B: 0-4°C; 

VOST: 10°C;MA:2-6',C) 

J 0 2b Cooler Temp = 

2. Is the cooler temperature within limits? (> freezing 

temp, of water to 6°C;NC, 1668,1613B: 0-4°C; 

VOST: 10°C;MA:2-6',C) 

J 

J. Were samples received with correct chemical 

preservative (excluding Encore)? J • 3a Sample preservative = 

J 

J. Were samples received with correct chemical 

preservative (excluding Encore)? J • 3a Sample preservative = 

J 

4. Were custody seals present/intact on cooler and/or 

containers? y 

•ffl 4a Not present 

• 4b Nat intact 

0 4c Other: 

4. Were custody seals present/intact on cooler and/or 

containers? y 

•ffl 4a Not present 

• 4b Nat intact 

0 4c Other: 

4. Were custody seals present/intact on cooler and/or 

containers? y 

•ffl 4a Not present 

• 4b Nat intact 

0 4c Other: 

5. Were all of the samples listed on the COC received? J 

I 

• 5a Samples received-not on COC 

0 5b Samples not received-on COC 

5. Were all of the samples listed on the COC received? J 

I 

• 5a Samples received-not on COC 

0 5b Samples not received-on COC 

6. Were all of the sample containers received intact? 1 1 

• 6a Leaking 

• fib Broken 

6. Were all of the sample containers received intact? 1 1 

• 6a Leaking 

• fib Broken 

7. Were VOA samples received without headspace? -L 4 0 7a Headspace (VOA only) 

8. Were samples received in appropriate containers? J _../ 0 8a Improper container 

9. Did you check for residual chlorine, if necessary? / • 9a Could not be determined due 

to matrix interference 

9. Did you check for residual chlorine, if necessary? / • 9a Could not be determined due 

to matrix interference 

10. Were samples received within holding time? • 10a Holding time expired 

11. For rad samples, was sample activity info, provided? J • Incomplete information 

12. For 16I3B water samples is pH<9? If no, was pH adjusted to pH 7 - 9 

with sulfuric acid? 

12. For 16I3B water samples is pH<9? If no, was pH adjusted to pH 7 - 9 

with sulfuric acid? 

13. Are the shipping containers intact? J D 13n Leaking 

D 13b Other: 

13. Are the shipping containers intact? J D 13n Leaking 

D 13b Other: 

14. Was COC relinquished? (Signed/Dated/Timed) J • 14a Not relinquished 

15. Are tests/parameters listed for each sample? • 15a Incomplete information 

16. Is the matrix ofthe samples noted? i 0 15a Incomplete information 

17. Is the date/time of sample coliection noted? / 015a Incomplete information 

18. Is tlie client and project name/# identified? / • 15a Incomplete infonnation 

19. Was the sampler identified on the COC? 7 

Quote*: *—. PM Instructions: 

1 ;—MrV^ e s a > — • 

Sample Receiving Associate: l ^jT^Y^H ^ Date:/X| f ^O^ QA026R21.doc , 090409 

VES018705 
57 

Wet Chemistry 

VES018706 
58 

Sample Summary 

VES018707 
59 

Lot-Sample #. 

Date Sampled. 

PARAMETER 

AECOM, Inc 

Client Sample ID: HBTO-U3-M2S-R1 

General Chemistry 

H9L090423-OQ1 Work Order #...: LQQM7 

12/01/09 Date Received..: 12/04/09 

Matrix : WASTE 

RESULT RL ONITS 

Asb Content 

Gross Calorific 

Value 

Total Chlorine 

835 200 mg/kg 

Dilution Factor: 1 

10500 1800 BTTj/lb 

Dilution Factor: X 

19200, 1870 mg/kg 

Dilution Factor: 9.35 

_ METHOD 

ASTM D482-00a 

MDL : 51 

ASTM D240-02 

HDL 130 

KNOX WC-0016 

MDL t 560 

PREPARATION- PREP 

ANALYSIS DATE BATCH ft 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/10-12/14/09 9344060 

VES018708 
60 

AECOM, mc 

Client Sample ID: HBT0-O3-M26-R2 

General Chemistry 

lK3t-Sample #...: H9L090423-002 Work Order #... : LQQNH Matrix : WASTE 

Date Sampled... : 12/02/09 Date Received. -: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Asn Content 566 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : SI 

Gross Calorific 10200 1800 BT(J/Xt> JSSIM D2«O-O2 12/14/09 S348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Cnlorine 14700 1200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: S MDL : 360 

VES018709 
61 

AECOM, UlC 

Client Sample ID: HBTU-TJ3-M2S-E3 

General Chemistry 

Lot-Sample #--.: H9L090423-003 Work Order #...: LQQNJ 

Date Sampled...: 12/03/09 Date Received., 

PARAMETER RESULT RL UNITS 

12/04/09 

METHOD 

Matrix : WASTE 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

527 200 mg/kg 

Dilution Factor: 1 

10300 1800 BT0/Xb 

Dilution Factor: 1 

16700 1670 mg/kg 

Dilution Factor: 8.35 

ASTM D482-00a 

MDL : 51 

ASTM D240-02 

MDL : 130 

KNOX WC-0016 

MDL : 5D0 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/10-12/14/09 9344060 

VES018710 
62 

AECOM, Inc 

Client Sample ID: LBTD-U3-M26-R1 

General Chemistry 

Lot-Sample #...: H9L090423-004 Work Order ft...: LQQNL Matrxx. WASTE 

Date Sampled...: 12/01/09 Date Received. 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

1230 200 mg/kg 

Dilution Factor: 1 

MD 1800 BTU/lb 

Dilution Factor: 1 

873 282 mg/kg 

Dilution Factor: 1.41 

12/04/09 

_ METHOD 

ASTM D482-00a 

MDL : 51 

ASTM D240-02 

MDL : 130 

KNOX WC-0016 

MDL : B5 

PREPARATION- PREP 

ANALYSIS DATE BATCH ft 

12/17-12/22/09 93S1497 

12/14/09 9348075 

12/10-12/14/09 9344060 

VES018711 
63 

AECOM, Inc 

Client Sample ID: LBTU-D3-M26-R2 

General Chemistry 

Lot-Sample #. ..: H9L090423-005 Work Order #. ..: LQQNN 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

Matrix : WASTE 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Ojlorine 

1170 200 mg/kg 

Dilution Factor: 1 

ND 1800 BTU/lb 

Dilution Factor: 1 

825 278 mg/kg 

Dilution Factor: 1.39 

_ METHOD 

ASTM D482-00a 

MDL : 51 

ASTM D240-02 

MDL : 130 

KNOX WC-0016 

HDL : 83 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/10-12/14/09 9344060 

VES018712 
64 

AECOM, Inc 

Client Sample ID: I3TU-U3-M26-R3 

General Chemistry 

Lot-Sample #...: H9L.090423-006 Work Order #...: LQQNP Matrix : WASTE 

Date Sampled.12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 2560 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 HDL : 51 

Gross Calorific ND 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 1250 280 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.4 MDL : 84 

VES018713 
65 

AECOM, Inc 

Client Sample ID: SF-U3-M26A-R1 

General Chemistry 

Lot-Sample #....- H9L090423-007 Work Order : LQQNT Matrix : WASTE 

Date Sampled : 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESDLT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 7600 200 mg/kg ASTM D4B2-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross Calorific ND 1B00 BTU/lb ASTM D240-02 12/14/09 934B075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 4980 272 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.36 MDL : 32 

VES018714 
66 

AECOM, Inc 

Client Sample ID: SF-U3-M26A-R2 

General Chemistry 

Lot-Sample #.. H9L090423-008 Work Order : LQQNO Matrix : WASTE 

Date Sampled : 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 5620 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross Calorific ND IBOO BTo/ib ASTM 0240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 5020 284 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.42 MDL : B5 

VES018715 
67 

AECOM, Inc 

Client Sample ID: SF-TJ3-M26A-R3 

General Chemistry 

Lot-Sample #...: H9L090423-0O9 Work Order #...: LQQN2 Matrix r WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD . ANALYSIS DATE BATCH # 

Ash Content S020 200 mg/kg ASTM D482-O0a 12/17-12/22/09 9351497 

Dilution Factor:'1 MDL : 51 

Gross calorifi c HD 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 5090 282 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.41 MDL : BS 

VES018716 
68 

AECOM, Inc 

Client Sample ID: CS-U3-M26A-R1 

General Chemistry 

Lot-Sample : H9L090423-010 Work Order #..-: LQQN4 Matrix : SOLID 

Date Sampled...: 12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 699000 200 mg/kg ASTM D482-00a 12/11-12/15/09 9345461 

Dilution Factor; 1 MDL : SI 

GrOSS Calorific ND 1B0Q BTU/l b AST M DSBSS-O O 12/16/09 9350032 

Value 

Dilution Factor.- 1 MDL : 130 

Total Chlorine 239 204 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.02 MDL : 61 

VES018717 
69 

AECOM, Inc 

Client Sample ID: CS-D3-M26A-R2 

General Chemistry 

Lot-Sample #... : H9L090423-011 Work Order #..-: LQQQR Matrix : SOLID 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content B01000 20O mg/kg ASTM D4B2-00a 12/11-12/15/09 9345461 

Dilution Factor: 1 MDL : SI 

Gross Calorific ND xsoo BTO/I_> AST M DSRES-OO 12/16/09 9350032 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 105 B 204 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.02 MDL i 61 

MOTE(S) : 

RL Reporting Limit 

B Estimated result. Result is less than RL. 

VES018718 
70 

AECOM, Inc 

Client Sample IDs CS-03-M2SA-R3 

General Chemistry 

Lot-Sample #...: H9L090423-012 Work Order LQQQW 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

Matrix : SOLID 

PARAMETER 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

RESULT RL UNITS 

799000 200 mg/kg 

Dilution Factor: 1 

ND 1800 BTa/l b 

Dilution Factor.- 1 

74.9 B 200 mg/kg 

Dilution Factor: 1 

_ METHOD 

ASTM D482-00a 

MDL : 51 

ASTM DSSSS-00 

MDL : 130 

KNOX WC-0016 

MDL. : 60 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/11-12/15/09 9345461 

12/16/09 9350032 

12/10-12/14/09 9344060 

HOTE(S): 

RL Reporting Limit 

B Estimated result. Result is less than RL. 

VES018719 
71 

Lot-Sample if... 

Date Sampled... 

PARAMETER 

Ash Content 

Gross Calorific 

value 

Total Chlorine 

AECOM, rnc 

Client Sample ID: HBTTT-D3-K23A-R1 

General Chemistry 

H9L090423-013 Work Order : LQQQ7 

12/01/09 Date Received..: 12/04/09 

Matrix : WASTE 

RESULT RL DNITS 

937 200 mg/kg 

Dilution Factor: 1 

10400 X8O0 BTTJ/Xb 

Dilution Factor: 1 

20600 1670 mg/kg 

Dilution Factor: 8.34 

_ METHOD 

ASTM D482-00a 

MDI 51 

ASTM D240-02 

MDL : 130 

KHOX WC-0016 

MDL : 500 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/11-12/16/09 9345064 

VES018720 
72 

AECOM, Iiic 

Client Sample ID: HBTO-D3-M23A-R2 

General Chemistry 

Lot-Sample #.--: H9L090423-014 Work Order #...: LQQRM Matrix. WASTE 

Date Sampled : 12/02/09 Date Received. 12/04/09 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

588 200 mg/kg 

Dilution Factor: 1 

10300 1800 BTO/lb 

Dilution Factor: 1 

14700 1720 mg/kg 

Dilution Factor: 8.62 

_ METHOD 

ASTM D482-O0a 

HDL : 51 

ASTM D240-02 

MDL : 130 

KNOX WC-0016 

MDL : 520 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/17-12/22/09 9351497 

12/14/09 9348075 

12/11-12/16/09 9345064 

VES018721 
73 

AECOM, Ine 

Client Sample ID: HBT0-U3-M23A-R3 

General Chemistry 

Lot-Sample tt. .. : H9L090423-015 Work Order #...: LQQRO Matrix : WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH jt 

Ash Content 535 200 mg/kg ASTM D482-O0a 12/17-12/22/09 935149 7 

Dilution Factor: 1 MDL : 51 

Gross Calori-ic 10300 XSDO BTtr/ lb AST M D240-0 2 12/14/09 934807 5 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 1690 0 168 0 mg/kg KNOX WC-0016 12/11-12/16/09 934506 4 

Dilution Factor: 8.3 9 MDL : 500 

VES018722 
74 

Lot-Sample #.. 

Date Sampled.. 

PARAMETER 

Ash. Content 

Gross Calorific 

Value 

Total Chlorine 

AECOM, Inc 

Client Sample ID: LETD-D3-M23A-R1 

General Chemistry 

H9L090423-016 Work Order #. - -: LQQR6 Matrix : WASTE 

12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

RESULT RL UNITS METHOD ANALYSIS DATE BATCH f 

1220 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : SI 

ND 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Dilution Factor: 1 MDL : 130 

81S 276 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.38 MDL : 83 

VES018723 
75 

AECOM, Inc 

Client Sample ID: IflTTMB-M23A-R2 

General Chemistry 

Lot-Sample : H9L090423-017 Work Order #...: LQQR7 Matrix : WASTE 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 1260 200 mg/kg ASTM D482-O0a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross Calorific ND 1800 BTD/ib AST M D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 738 282 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.41 MDL : 85 

VES018724 
76 

AECOM, Inc 

Client Sample ID: I_TD-D3-M23A-E3 

General Chemistry 

Lot-Sample #...: H9L090423-018 Work Order #...: LQQR8 Matrix : WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 2420 200 rag/kg ASTM D482-O0a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : 51 

Gross calorifi c ND IBOO BTU/I _ ASTM D240-02 12/14/09 9348075 

Value 

Dilution Factor: 1 MDL : 130 

Total Chlorine 1230 282 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.41 MDL : B5 

VES018725 
77 

Lot-Sample tt.. 

Date Sampled.. 

PARAMETER 

Ash Content 

Gross Calorific 

Value 

Total C_lorine 

AECOM, Inc 

Client Sample ID: SF-D3-M23A-R1 

General Chemistry 

H9L090423-019 Work Order LQQTA Matrix : WASTE 

12/01/09 Date Received..: 12/04/09 

PREPARATION- PREP 

RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

7290 200 mg/kg ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor; 1 MDL : 51 

ND 1800 BTU/lb ASTM D240-02 12/14/09 9348075 

Dilution Factor: 1 MDL : 130 

5030 274 mg/kg KHOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.37 MDL : 82 

VES018726 
78 

Lot-Sample #.. 

Date Sampled., 

PARAMETER 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

AECOM, inc 

Client Sample UJ: SF-D3-M23A-R2 

General Chemistry 

H9L090423-020 Work Order : LQQTC Matrix : WASTE 

12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

6950 200 mg/kg ASTM D4B2-O0a 12/17-12/22/09 9351497 

Dilution Factor: 1 MDL : SI 

ND 1800 BTU/rb ASTM D240-02 12/14/09 934B075 

Dilution Factor: 1 MDL : 130 

5010 274 mg/kg KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.37 MDL : 62 

VES018727 
79 

AECOM, Inc 

Client Sample ID: SF-U3-M23A-R3 

Seneral Chemistry 

Lot-Sample*...: H9L090423-021 Work Order #...: LQQTD Matrix : WASTE 

Date Sampled...: 12/03/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

ASh Content 7820 200 mg/kg ASTM D482-0Oa 12/17-12/22/09 9351497 

Dilution Factors 1 MDL : 51 

Gross Calorific ND 1800 BTU/I_> AST M D_40-O_ 12/14/09 9348075 

Value 

Dilution Factor; 1 MDL : 130 

Total Chlorine 5020 272 mg/kg KNOX WC-0016 12/11-12/1G/09 9345064 

Dilution Factor: 1.36 MDL : 82 

VES018728 
80 

AECOM, Inc 

Client Sample ID: CS-U3-M23A-R1 

General Chemistry 

Lot-Sanrple #...: H9L090423-022 Work Order #.--: LQQTE Matrox. SOLID 

Date Sampled...: 12/01/09 Date Received. 12/04/09 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

711000 200 mg/kg 

Dilution Factor: 1 

ND 1800 BTO/lb 

Dilution Factor: 1 

220 200 mg/kg 

Dilution Factor: 1 

METHOD 

ASTM D482-00a 

MDL : SI 

AST M DS86S-0 0 

MDL : 130 

KNOX WC-0016 

MDL : €0 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/11-12/15/09 9345451 

12/16/09 9350032 

12/10-12/14/09 9344060 

VES018729 
81 

AECOM, Inc 

Client Sample" ID: CS-U3-M23A-R2 

General Chemistry 

Lot-Sample #...: H9L090423-023 Work Order #.--: LQQTF Matrix : SOLID 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PREPARATION- PREP 

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH # 

Ash Content 703000 200 mg/kg ASTM D482-O0a 12/11-12/15/09 93454S1 

Dilution Factor: 1 HDL r 51 

Gross Calorific ND 1800 BTU/lb ASTM DSS6S-00 12/lS/09 9350032 

Value 

Dilution Factor: 1 MDL :' 130 

Total Chlorine 295 200 mg/kg KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1 MDL : 60 

VES018730 
82 

AECOM, Inc 

Client Sample ID: CS-D3-M23A.-R3 

General Chemistry 

Lot-Sample #...: H9L090423-024 Work Order #... : LQQTG Matrix. SOLID 

Date Sampled...: 12/03/09 Date Received.. 12/04/09 

PARAMETER RESULT RL UNITS 

Ash Content 

Gross Calorific 

Value 

Total Chlorine 

703000 200 mg/kg 

Dilution Factor: 1 

ND 1800 BTU/lb 

Dilution Factor: 1 

339 204 mg/kg 

Dilution Factor: 1.02 

_ METHOD 

ASTM D482-00a 

MDL : 51 

ASTM D5865-00 

MDL : 130 

KNOX WC-0016 

MDL : €1 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

12/11-12/15/09 9345461 

12/16/09 9350032 

12/10-12/14/09 9344060 

VES018731 
83 
84 

Client Lot H9L090423 

PARAMETER 

Ash Content 

Total Chlorine 

Total Chlorine 

RESULT 

NO 

ND 

ND 

METHOD BLANK REPORT 

General Chemistry 

REPORTING 

LIMIT UNITS METHOD 

Matrxx. WASTE 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

Work Order #: LQ91G1AA MB Lot-Sample #: H9L170000-497 

200 mg/kg 

Dilution Factor: 1 

ASTM D482-00a 12/17-12/22/09 9351497 

Work Order #: LQTX01AA MB Lot-Sample #: H9L100000-OSO 

200 mg/kg 

Dilution Factor.- 1 

KNOX WC-0016 12/10-12/14/09 9344060 

Work Order #: LQXERIAA MB Lot-Sample #: H9L110000-064 

200 mg/kg 

Dilution Factor: 1 

KNOX WC-0016 12/11-12/16/09 9345064 

NOTB(S): 

Calculations arc performed before rounding to avoid round-off errors in calculated results. 

VES018733 
85 

METHOD BLANK EEPORT 

General C-eraistry 

Client Lot #... H9L090423 Matrxx. SOLID 

PARAMETER 

Ash Content 

RESULT 

ND 

REPORTING 

LIMIT UNITS METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

Work Order ft: LQ1E11AA MB Lot-Sample #: H9L110000-4G1 

200 mg/kg ASTM D482-O0a 12/11-12/15/09 9345461 

Dilution Factor.- 1 

NOTE(S): 

Calculations are performed before roundins (0 avoid round-off errors in calculated results. 

VES018734 
86 

LABORATORY COHTROL SAMPLE EVALUATION REPORT 

General Chemistry 

Lot-Sample #...: H9L090423 Matrix. 

PARAMETER 

Ash Content 

PERCENT 

RECOVERY 

99 

99 

RECOVERY 

LIMITS RPD 

RPD 

LIMITS METHOD 

PREPARATIONANALYSIS DATE 

: WASTE 

PRE? 

BATCH # 

W0#:LQ91G1AC-LCS/LQ91G1AD-LCSD LCS Lot-Sample#: H9L17OO00-497 

(90 - 110) ASTM D482-00a 12/17-12/22/09 9351497 

(90 - 110) 0.48 (0-10) ASTM D482-0Da 12/17-12/22/0 9 9351497 

Dilution Factor: 1 

Gross Calorifi c 

Value 

100 

99 

WO#:LQ2R71AA-_CS/LQ2R71AC-LCSD LCS Lot-Sample#: H9L140000-075 

(98 - 102) 

(98 - 102) 0.08 (0-2.0) 

Dilution Factor: 1 

ASTM D240-02 

ASTM D240-02 

12/14/09 

12/14/09 

9343075 

9348075 

NOTE(S) : , 

Calculaiions are pcribrmed before rounding lo avoid round-off errors in calculated results. 

VES018735 
87 

LABORATORY CONTROL SAMPLE DATA REPORT 

General Chemistry 

Lot-Sample #.. 

PARAMETER 

Ash Content 

H9L090423 

SPIKE MEASURED 

AMOUNT AMOUNT UNITS 

Matrix : HASTE 

PERCNT 

RECVRY RPD METHOD 

PREPARATIONANALYSIS DATE 

4000 

4000 

PREP 

BATCH ft 

WO#iLQ91GlAC-LCS/LQ91GlAD-LCSD LCS Lot-Satrtple#: H9L170000-497 

3S70 mg/kg 99 ASTM D482-O0a 12/17-12/22/09 9351497 

3950 mg/kg 99 0.48 ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 

Gross Calorifi c 

Value 

20600 

20600 

WO#:LQ2R71AA-LCS/LQ2R71AC-LCSD LCS Lot-Sample#: H9L140000-075 

20500 

20500 

BTU/lb 100 

BTU/lb 99 

Dilution Factor: 1 

ASTM D24 0-02 

0.08 ASTM D240-02 

12/14/09 

12/14/09 

9348075 

9348075 

NOTE(S): 

Calculaiions arc performed before rounding io avoid round-off errors in calculated results. 

VES018736 
88 

LABORATORY CONTROL SAMPLE EVALUATION REPORT 

General Chemistry 

Client Lot H9L090423 Matrix : WASTE 

PERCENT RECOVERY PREPARATION- PREP 

PARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE BATCH # 

Total Chlorine Work Order #: LQTX01AC LCS Lot-Sample*: H9L100000-050 

100 (80 - 120) KNOX WC-0015 12/10-12/14/09 9344060 

Dilution Factor: 5 

Total Chlorine Work Order #: LQXER1AC LCS Lot-Sample*: H9L110000-064 

99 (B0 - 120} KNOX WC-0015 12/11-12/16/09 9345064 

Dilution Factor: 5 

MOTE tS) ; ________________ _ .. .. 

Calculations arc pcrrormcd before rounding to avoid round-off errors in calculated results. 

VES018737 
89 

LABORATORY CONTROL SAMPLE DATA REPORT 

General Chemistry 

Client Lot H9L09D423 Matrix : WASTE 

SPIKE MEASURED PERCNT PREPARATION- PREP 

PARAMETER AMODNT AMOUNT UNITS RECVRY METHOD ANALYSIS DATE BATCH # 

Total Chlorine Work Order #: LQTX01AC LCS Lot-Sample#: H9L100000-060 

10000 9980 mg/kg 100 KNOX WC-0016 12/10-12/14/09 9344050 

Dilution Factor: S 

Total Chlorine Work Order #: LQXER1AC LCS Lot-Sample#: H9L110000-064 

10000 9850 mg/kg 99 KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: S 

NOTE(S) : _ 

Calculations are performed before rounding to avoid round-off errors in calculated results. 

VES018738 
90 

LABORATORY CONTROL SAMPLE EVALUATION REPORT 

General Chemistry 

Lot-Sample H9L090423 Matrxx. 

PARAMETER 

Ash Content 

PERCENT 

RECOVERY 

100 

100 

RECOVERY 

LIMITS RPD 

RPD 

LIMITS METHOD 

PREPARATIONANALYSIS DATE 

: SOLID 

PREP 

BATCH # 

W0#:LQ1E11AC-LCS/LQ1E11AD-LCSD LCS Lot-Sample#: H9L110000-461 

(90 - 110) ASTM D4B2-00a 12/11-12/15/0.9 93454S1 

(90 - 110} 0.42 (0-10) ASTM D482-00a 12/11-12/15/09 9345451 

Dilution Factor: 1 

Gross Calorific 

Value 

100 

100 

W0#:LQ58P1AA-_CS/_Q58P1AC-_CSD LCS Lot-S_mple#.- H9L160000-032 

(98 - 102) ASTM D58S5-00 

(•98 - 102) 0.10 (0-2.0) ASTM D5865-00 

Dilution Factor: 1 

12/16/09 

12/16/09 

9350032 

9350032 

MOTE(S) : 

Calculations arc performal before rounding to avoid round-off errors in calculaied rcsulu. 

VES018739 
91 

LABOEATORr CONTROL SAMPLE DATA REPORT 

General Oiernistry 

Lot-Sample H9L090423 Matrix. SOLID 

PARAMETER 

Ash Content 

SPIKE 

AMOUNT 

4000 

4000 

Gross Calorific 

Value 

11400 

11400 

MEASURED 

AMOUNT UNITS 

PERCNT 

RECVRY RPD METHOD 

PREPARATIONANALYSIS DATE 

PREP 

BATCH # 

WOft:LQlEllAC-LCS/LQlEllAD-LCSD LCS Lot-Sample#: H9L110000-461 

4010 mg/kg 100 ASTM D482-0Oa 12/11-12/15/09 9345461 

3990 mg/kg 100 0.42 ASTM D482-00a 12/11-12/15/09 9345461 

Dilution Factor: 1 

W0#:LQ58P1AA-LCS/LQ5BP1AC-LCSD LCS Lot-Sample*: H9L160000-032 

11300 BTU/lb 100 

11300 BTU/lb 100 

Dilution Factor: 1 

ASTM DS865-00 

0.10 ASTM D586S-00 

12/16/09 

12/16/09 

9350032 

9350032 

MOTE(S) : 

Calculations ate performed before rounding to avoid round-off errors in calculated results. 

VES018740 
92 

MATRIX SPIKE SAMPLE EVALUATION EEPORT 

General Chemistry 

Client Lot #...-. H9L090423 

Date Sampled...: 12/01/09 

PERCENT RECOVERY 

PARAMETER RECOVERY LIMITS 

Total Chlorine WO# 

100 (80 

97 (80 

Date Received..; 12/04/09 

RPD 

RPD 

LIMITS METHOD 

Matrox. WASTE 

PREPARATION -

ANALYSIS DATE 

PREP 

BATCH # 

LQQNNIAG-MS/LQQNN1AH-MSD MS Lot-Sample #: H9L090423-005 

120) KNOX WC-0016 12/10-12/14/09 9344060 

120) 3.5 (0-10) KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 7.07 

Tota l Chlorine 

101 (80 

101 (80 

WOt: LQQNT1AE-MS/LQQNTIAF-MSD MS Lot-Sample #: H9LD90423-007 

120) KNOX WC-0016 12/11-12/16/09 9345064 

120) 3.2 (0-10) KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 7.1 

HOTE(S) •• 

Calculations arc pcrrormcd before rounding to avoid round-off errors in calculated results. 

VES018741 
93 

MATRIX SPIKE SAMPLE DATA REPORT 

General C_temistxy 

Client Lot H9L090423 

Date Sampled...; 12/01/09 

Matrix : WASTE 

Date Received..: 12/04/09 

SAMPLE SPIKE 

PARAMETER AMOUNT AMT 

Total Chlorine 

825 

825 

MEASRD 

AMOUNT UNITS 

PERCNT 

RECVRY RPD METHOD 

PREPARATION- PREP 

14100 

14000 

ANALYSIS DATE BATCH # 

WO#: LQQNN1AG-MS/LQQNN1AH-MSD MS Lot-Sample #: H9L090423-005 

15000 mg/kg 100 KNOX WC-0016 12/10-12/14/09 9344060 

14500 mg/kg 97 3.5 KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 7.07 

Total Chlorine WO#: LQQNT1AE-MS/LQQNT1AF-MSD MS Lot-Sample #.- H9L090423-007 

4980 14200 19300 mg/kg 101 KNOX WC-001S 12/11-12/16/09 9345064 

4980 13600 18700 mg/kg 101 3.2 KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 7.1 

NOTE(S): 

Calcubtians arc perform— before rounding to avoid round-off errors in calculated results. 

VES018742 
94 

MATRIX SPIKE SAMPLE EVALUATION REPORT 

General Chemistry 

Client Lot #-..: H9L090423 Matrix : SOLID 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

PERCENT RECOVERY RPD PREPARATION- PREP 

PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE BATCH # 

Total Chlorine WO#: LQQQR1 AG - MS /LQQQR1AH -MSD MS Lot-Sample #: H9L090423-011 

90 (80 - 120) KNOX WC-0016 12/10-12/14/09 9344060 

91 (80 - 120) 0.77 (0-10) KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 4.73 

NOTE (S) : 

Calculations are performed before rounding lo avoid round-off errors in calculaied results. 

VES018743 
95 

MATRIX SPIKE SAMPLE DATA EEPORT 

General Cfaemistry 

Client Lot H9L090423 

Date Sampled : 12/02/09 

SAMPLE SPIKE MEASRD 

Date Received..: 12/04/09 

Matrix. SOLID 

PARAMETER AMOUNT AMT 

Total Chlorine 

105 9470 

105 9450 

AMOUNT UNITS 

PERCNT 

RECVRY RPD METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

WO#: LQQQR1AG-MS/LQQQR1AK-MSD MS Lot-Sample #: H9L090423-011 

8S40 mg/kg 90 KNOX WC-0016 12/10-12/14/09 9344060 

8710 mg/kg 91 0.77 KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 4.73 

NOTE(S): 

Calculations ore performed before rounding to avoid round-off errors in calculated results. 

VES018744 
96 

SAMPLE DUPLICATE ETOLDATIOIT EEPORT 

General Chemistry 

Client Lot tt..-: H9L090423 Work Order #...: LQQNN-SMP Matrix : WASTE 

LQQNN-DUP 

Date Sampled...: 12/02/09 Date Received..: 12/04/09 

DUPLICATE RPD PREPARATION- PREP 

PARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH # 

Gross Calorific SD Lot-Sample #: H9L090423-OOS 

Value 

ND ND BTU/lb 13 (0-10) ASTM D240-02 12/14/09 9348075 

Dilution Factor: 1 

Ash Content SD Lot-Sample #: H9L090423-005 

1170 1210 mg/kg 3.1 (0-10) ASTM D482-00a 12/17-12/22/09 9351497 

Dilution Factor: 1 

Total Chlorine SD Lot-Sample H9L090423-005 

325 818 mg/kg 0.82 (0-10) KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.39 

VES018745 
97 

Client Lot #...: H9L090423 

Date Sampled...: 12/01/09 

SAMPLE DUPLICATE EVALUATION REPORT 

General Cnemistry 

Work Order LQQNT-SMP 

LQQNT-DUP 

Date Received..: 12/04/09 

PARAM RESULT 

Total Chlorine 

4980 

DUPLICATE 

RESULT 

5000 

Matrix. WASTE 

UNITS 

RPD 

RPD LIMIT METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH ft 

SD Lot-Sample #: H9L090423-007 

mg/kg 0.42 (0-10) KNOX WC-0016 12/11-12/16/09 9345064 

Dilution Factor: 1.36 

VES018746 
98 

Client Lot #.. 

Date Sampled.. 

PARAM RESULT 

H9L090423 

12/02/09 

DUPLICATE 

RESULT 

SAMPLE DUPLICATE EVALUATION REPORT 

General Chemistry 

Work Order #...: LQQQR-SMP Matrix. 

LQQQR-DUP 

Date Received..: 12/04/09 

SOLID 

Total Chlorine 

105 B 

Gross Calorific 

Value 

ND 

Ash Content 

801000 

99.6 B 

ND 

784000 

RPD 

UNITS RPD LIMIT METHOD 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

SD Lot-Sample #: H9L090423-011 

mg/kg 5.3 (0-10) KNOX WC-0016 12/10-12/14/09 9344060 

Dilution Factor: 1.02 

SD Lot-Sample #: H9L090423-011 

BTOyib 0 (0-10) ASTM D5865-00 12/16/D9 

Dilution Factor: 1 

9350032 

SD Lot-Sample #: H9L090423-011 

mg/kg 2.2 (0-10) ASTM D4B2-00a 12/11-12/15/09 9345461 

Dilution Factor: 1 

NOTE(S) : 

Calculations arc performed before rounding to avoid round-ofT errors in calculated results. 

B Estimated result. Result is less titan RL. 

VES018747 
99 

Client Lot H9L090423 

Date Sampled...: 12/03/09 

SAMPLE DDPLICATE EVALDATIOH REPORT 

General Chemistry 

Work Order #...: LQQRO-SMP 

LQQRO-DDP 

Date Received..: 12/04/09 

PARAM RESDLT 

Gross Calorific 

Value 

10300 

DDPLICATE 

RESULT UNITS 

RPD 

RPD LIMIT METHOD 

Matrix : WASTE 

PREPARATION- PREP 

ANALYSIS DATE BATCH ft 

SD Lot-Sample #: H9L090423-015 

10100 BTU/lb 1.4 (0-10) ASTM D240-02 12/14/09 

Dilution Factor: 1 

9348075 

VES018748 
101 

Client Lot #. 

Date SampledPARAM RESULT 

Ash Content 

7820 

H9L090423 

12/03/09 

DUPLICATE 

RESULT 

SAMPLE DUPLICATE EVALTJATION REPORT 

General Chemistry 

Work Order #...: LQQTD-SMP 

LQQTD-DUP 

Date Received..: 12/04/09 

UNITS RPD 

RPD 

LIMIT METHOD 

Matrix- WASTE 

6910 mg/kg 12 

Dilution Factor: 1 

PREPARATION- PREP 

ANALYSIS DATE BATCH # 

SD Lot-Sample #: H9L090423-021 

(0-10) ASTM D482-O0a 12/17-12/22/09 9351497 

VES018749 
VES018750 
VES018751-019264.pdf