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' 4.1 ... g ^ ' "1631.3;""" 1841 6 ' 2531,9r ""eoo'.'t!" " 1344.4; 6766. "4.51 

""377'.' " " 7.7 " ""1622.3! ' 1832.6; 2532.li 63676 " " i 350.3, ""' 0.00' 4.21 

"' 4.1' " ...8-17 "1631.67"' 183778*"" ' "" 118975i "60677; 135571 7'6.00; 4.58 

"4. T 7.9! i'651.8"' " 184BT& 1263.7! "630.0 "135572! "" 6.66: ""4.48 

'" 4.3 778!" 1663.8 "185576! 171075:' " 586.1' 1353.4: "" 0.00! " 4.47 

4.2 ' 8.1, "1669.0 ' 1861,8 " 2233.2: ~ 586.1;" 1345777 0.00/ "" 4.56 

4 2 8.3! "167573"- """ 186876':"" 1710.8: 586.1 1338.2] " " 6.66": """4770 

4.3; ... . 1681.37 " 1874.8: " 1636.0! "586.1:"" 126575! 0.66 47'80 

4.6! "8.7! " 1686.0: 1877.57 ' " 193477:""'' 586.1 " 1280.5] "6.667" 5.0-. 

" '4.3" "8.9!" " -1690.5!:

" "l882.0f"" "1563.8:

 r 586.i: " " "1241,3! "" " """o7o'b7" 5709 

4 3 " "976!" "'7693.5!"" "188475: "'1785.5! ""66677!" 1231.4 " " o.oo' 5.14 

VES018401 
Unit 3 Run 3 ACFM Deg F % Deg F Peg F Lb/Hr Lb/Hr 

•ytinjei-iStertip^W'i/y timeSiuiTyFlbtffam^ StackFlow SDA'OutTemp BH'PressDrop 02Pry|:PCDTerhr. iSCC.TempI LoWBTUwot S'pecFeed wgF HigHBWwgt C O Pn/ Corr 02We t 12/3/2009 3:46 PM ; 

12/3/2009 3-47 P M 

12/3/2009 3:48 PM!' 

12/3/2009 3:49 PM. 

i2/3/26'09 3:50 PM ' 

12/3/2069 3:51 PMf 

j 2/3/2669 3:52 PM l 

12/3/2009 3^53 PMi " 

T2/3/2069 3:54 PMi ' 

J2/S2609 3:55PMl" 

12/3C009 3:56 PMi 

12/37200^3:57' TM ; ' 

' 12/3726o¥3:58PM,'' 

1273/2669 3:59 PMl 

12/3/2009 4:06 P M 

"l'273rapTO4:6i"PM; 

T2/3/2669 4:02 PM';'" 

12/3/2009 4:03 PM ; 

'12/3/2009 4:04 PM : 

'12/3/2009 4:05 PMi 

]12/3/2009 4:06 PM!" 

'T273/26W4:07PM!" 

' 12/3/2669"4:68>M!] 

'"l273/2O69"4:j09J'M! 

12/3/2009 4:10 P M 

12/3/2069 4:11 P M 

12r^6094:12"PM l 

"12/3/26694:13'P"M;'" 

1276/2009 4:14 PMj 

i2/3/2bd94J57PMr 

"1273726694:16 PM ! 

" 12/372009 4:17 PM ] 

"'1273/2069 4: WpM r 

12/3/2009 4719 PM; ] 

"12/3/2009"4:20 P M 

12/3/2009 4-21 P M 

12/3/2309 4:22 P M 

'12/672009 4:23 P M 

7.9i 

' Y.9! " 

776 

7.9 

7.6:' 

7.9 

8.6; 

s.o 

7.9! 

7.6: 

7.9! 

7.9 

7-9| 

7.9i 

7.9' 

7.9; 

7.9! 

7.9! 

7.9! 

JK 

7.9; 

'7.9'" 

"7:6! 

7.9 

7.9r 

'778!" 

7.9 

'7,9: 

" 7.9: 

"7.9 

7.9! 

7.9 

.7-9: ' 

7.9; 

' 7.9" 

"7.9"' 

"77ft ' 

79!" 

69.2, 

692 ' 

]6972; 

69.2: 

692;" 

69.2 

69.2 

69.2' 

69.2;" 

69.2;' 

69.2 

"69.2-" 

69.2 

69.2 

69.2 

" 69.2 

69.2: 

69.2 

"69.2" 

" 6972' 

"6972:" 

"69.1!" 

69.1 

69.2:" 

' 69.2 

69.2 " 

76~9.2; 

69.2 

"69.2 

"6972!" 

69.2 

69.2 

69.2 

69.2 

6972 

69.2;"" 

"6972" 

"69.2 

15489.1! 

1507373! " 

15328.9 

15588.17 

-15577.3 

15141.1, 

15214.1: 

14749.9. 

" 1545176"' 

1560977,""' 

1537475"" 

" 15325 2 

15372.9 

154975.1' 

15488.9 

15369.3 

1549674: 

15509.5 

15039.5'" 

15325.6. 

i5205'.0." 

' 15457.2 

14952.7. 

15659.3.' 

' 153332 

" 1519279." 

15605.2 

15092.0 

1545274 

15105.2. 

1564174 

15230.8. 

1524571 

" 15183.9 

'14991.8:' 

15574.2 

14927.2 

15167.2 

Average! 

421.0. 

429.5 

424.8 

412.6. 

4057$'' 

410A 

4T8.3" 

421.3! 

409.3" 

408.0' 

417.0; 

424 0 

' 427.8 

"42i7"8r" 

4147s! 

410.5; 

414.5] 

423.0-

' 427.8' 

"425.br 

"417.3^ 

412.6! 

' 409.5 " 

' 413.5;"' 

"424.0.'" 

429 0' 

"42576!" 

418.5; 

"414.8 " 

]4l'6.3r 

' 41'9.'3:"' 

"42575: 

"427.5 ' 

424 3 

"417.0; 

4123' 

"412.5' 

416.8! 

" 420.1 

4.3I 

4.2; ' 

4.3, 

4.3 

'4 . 3 " 

4.2 

4.3 

4.0. 

4.3! ' 

4.4! "' 

"'4737'" 

'4.3: 

4.3 " 

4.3.:" 

4.4 

' 474 

4.4]]' 

'4.4 

' 472 

4.3: 

"4.4 

4.3 

4.2 

' 4.4" " 

" 4.3 

"4.3" 

4.4 

4 2. 

'"4.5! " 

"4.3 

"44:-

4.3'" 

4.3" 

473 

43 

4.5 

4.2 

" 4.2 """ 

1 

9.3 

'6.3! 

]974! 

9.9; 

I6.3! 

10.4: 

10.6{ 

1677! 

ibTTTif 

1672; 

16.43 

J6-3L 

10.3'"" 

10.2: 

10.2 

10.2! 

10.1!" 

10.6T" 

9.8: 

"9.7T" 

' 9.8' 

"9.7!" 

9.7'] 

9

-

7

f 

9.5; 

' 9.6: 

9.5] 

9

-

5

L 

672'" 

" 9.6"' 

- 9.4-

' 3.7; 

"977! 

"976'" 

9.8' 

"9.8 

" 9.5! 

1697.8! 

"'1766.0;' 

1700.8; 

1703.31" 

" 1699.5;" 

1692.5: 

"1684737" 

"167876: ' 

1674.8 ' 

1672.5!" 

166778. 

1659.8' 

"165\8 L 

J646.B! 

1645.0!" 

"1642.8!" 

J640.8| " 

' 164676!"" 

"164178]' 

1647.57 

"1653.81"" 

' 1660.5: 

1671.0 

16828' 

"1684.3-" 

"l678.o! 

167073: 

1665.3 

1666.0; " 

1657.67 

1650.8; 

1646.0 

"1641751' 

'1638.8] 

" 163575T] 

"'1633.3;' 

'1631.5. 

1632.8." 

166178. 

1888.3 

188875. 

1890.3 

18928; 

" 1889.8: 

1886.3; 

"18818; 

"187576! 

3"87475i 

1877.3 

187375! 

"1867.8: 

'".861.8!' 

'185775 

"185473: 

" 1857275! 

1850.3 

~ 1849.3"; 

1850.5 

1854.3 

"185873! 

J 862.8: 

1866.3 

1870.3 

"1875.0: 

1875.8 

1874.5. 

1873.0: 

18718 ! 

1871.37 

' 187673 

"i'869.5! 

"1868.8! 

"186375: 

1859.67 

1356.3' 

1856.3, 

"1857.6; 

' 186776 

1710.8 

1561.3; 

1785.57 

1710.8-

1561.8" 

178575 

1860.2 

1711 4 

" 816.5" 

1711.0 

2307.9!" 

208472: 

2669.5! 

1785751 

1934.7!' 

236779! 

1860.2 

1562.4!" 

7260674V 

2307.9 

2084.47 

215877: 

"230779' 

"208474! 

'2009.7! 

1785.5] 

2084.2 

2681.1 

1866727 

2084.2 

208472; 

2084.2. 

2158791' 

2382.4;' 

223372! 

1934.7: 

2307.9: 

"2069.5; 

1892.1! 

630.0; 1224.2 0.00! 5.24 

600.7 1204.4: " o.oo' ""5.41 

630.0 119771 ' ' 0.06 ' 5.53 

586.11 1196.9 0.00' 5.54 

586.1 1183.1 6.66 5".79 

586.1! ' 1181.3: "0.66: 6700 

630.0 ' 118676 0.00 "' 6.15 

717.9'"" 1179.8" o.oo] 6.28 

615.4'" "1179 1 "" 0.06 6.42 

674.0 1177.8 """" 67"o"6T

" "6.18 

586.1' ' 1194.7 " "o.oo!" "6.09 

586.1. 17201.8 " 0.06. " 6.11 

586.1. 1197.4 "6.60" ""6.09 

"615.4"!"' 1199.3" 0.00 &08 

70373. "1199.6; 6.60;' "" 6.01 

717.9- 1198.7 0.66" '"" 5.89 

732.6 ' 1200.6 "oToof "5.90 

586.1. '"" " 1205.5 6W 5.89 

381.0 1204.0 " "67oo!" " 5.91 

7293.0!" 1202.4' 0.06: ""5785 

"278.4' " " 1203.7 6.00. 5".75 

"1757B"""" 1205.3 6766":' "" 6776 

"676:"""" 1206.2 0.00: 5.70 

175.8 1205.9 67667 " 5.72 

571.4' ' 1206.2 0.06, 5775 

'674.6. 1200.7 ' 0.00 5.65 

600.7 ' 1204.6 "0.66T 5.63 

630.0: 1214.1! ' "67667 ' 5.55 

615.4. "1219. 1 6766;' "5.41 

674.6:" " 1224.6"'' o.oo-' 5.46 

"60677;" 1222.4' 6766;" ""'5.29 

644.7. 1214.9 6766: "5.50 

644.7; ' I20T.3" 0.60" 

" "o.bb*" 

"""5.46 

630.6 1195.8 

0.60" 

" "o.bb*" 5.62 

600.7." ' 1186.8. o.oo] 5.64 

669.3 " 1184.4 "" 'o.oo ' 5.56 

674.6 '"118575';"" " "" 0.667 """"5762 

586.1 1182.0 c.06: " 5765 

573.2! 1205.0 5.6 

VES018402 
Unit 3 Run 3 

TirrielStamp- • StackFlowHRA 

12/3/2009 10:49 AM 15006.2 

12/3/2009 10:50 AM 15007.8 

12/3/2009 10:51 AM; 15007.7 

12/3/2009 10:52 AM 14996.3 

12/3/2009 10:53 AM 14995.9 

12/3/2009 10:54 AM '14995.7 

12/3/2009 10:55 AM 1498971 

12/3/2009 10:56 AM 14991.0 

12/3/2009 10:57 AM; 14991.1 

12/3/2009 10:58 AM 14994.0 

12/3/2009 10:59 AM 14972.0 

12/3/2009 11:00 AM 14943.2 

12/3/2009 11:01 AM 1493879 

12/3/2009 11:02 AM 14"919.3 

12/3/2009 11:03 AM 14922.5 

12/3/2009 11:04 AM 14923.3 

12/3/2009 11:05 AM 14931.2 

12/3/2009 11:06 AM 14948.4 

12/3/2009 11:07 AM 14962.0 

12/3/2009 11:08 AM 14972.2 

12/3/2009 11:09 AM 14990.7 

12/3/2009 11:10AM 15007.8 

12/3/2009 11:11 AM ~15017. 9 

12/3/2009 11:12 AM 15033.2 

12/3/2009 11:13 AM 15051.7 

12/3/2009 11:14 AM 1505776 

12/3/2009 11:15AM 15067.3 

12/3/2009 11:16 AM 15079.6 

12/3/2009 11:17 AM T5082.7 

12/3/2009 11:18 AM 15091.8 

12/3/2009 11:19 AM 15111.1 

12/3/2009 11:20 AM 15107.7 

12/3/2009 11:21 AM 15118.7 

12/3/2009 11:22 AM "15124.8 

12/3/2009 11:23 AM 15130.7 

12/3/2009 11:24 AM 15139.2 

12/3/2009 11:25 AM 15148.3 

12/3/2009 11:26 AM '15153.4 

12/3/2009 11:27 AM 15163.1 

12/3/2009 11:28 AM '15183.7 

12/3/2009 11:29 AM 15204.0 

12/3/2009 11:30 AM 15214.7 

12/3/2009 11:31 AM 15236.3 

12/3/2009 11:32 AM '15248.4 

12/3/2009 11:33 AM 15269.8 

12/3/2009 11:34 AM 15284.9 

12/3/2009 11:35 AM 15296.9 
Unit 3 Run 3 

Time Stamp |-StackFlowHRA 

12/3/2009 11 36 AM: 15319.2 

12/3/2009 11 37 AMj 15340.6 

12/3/2009 11 38 AM: 15352.1 

12/3/2009 11 39 AM: 15363.0 

12/3/2009 11 40 AM;

. 15380.0 

12/3/2009 11 41 AM' 15386.3 

12/3/2009 11 42 AM! 15387.7 

12/3/200,9 11 43 AM; 15394.9 

12/3/2009 11 44 AMj 15392.7 

12/3/2009 11 45 AMj 15403.9 

12/3/2009 11 46 AM| 15404.8 

12/3/2009 11 47 AM! 15412.4 

12/3/2009 11 48 AM! 15409.8 

12/3/2009 11 49 AM! 15417.1 

12/3/2009 11 50 AM': 15411.7 

12/3/2009 11 51 AM: 15410.5 

Maximum! 15417.1 
Uni

t 3 Run 3 

TimeiStamp ; StackFlowHRA; 

_12/3/2009 1j19 PMj 

1273/20091:20 PM-

12/3/2009 1:21 PM! 

12/3/2009 1:22, PM; 

"12/3/2009 1:23 PMj 

12/3/2009 1:24 PM] 

12/3/2009 1:25 PMi 

12/3/2009 1:26 PM! 

12/3/2009 1:27 PM! 

12/3/2009 1:28 PM! 

12/3/2009 1:29 PM! 

12/3/2009 1:30 PMi" 

12/3/2009 1:31 PM: 

12/3/2009 1:32 PMj 

"12/3/2009 1:33 PM"! 

12/3/2009 1:34 PM"f 

12/3/2009 1:35 PM! 

12/3/2009 1:36 PM: r 

12/3/2009 1^37_PM: 

12/3/2009'l:38 PM 

12/3/2009 1:39 PM;" 

"12/3/2009 1:40 PM; 

12/3/2009 1:41 PMj 

"12/3/2009 1:42 PM. 

12/3/2009 1:43 PM] 

"12/3/2009 1:44 "PMj 

"12/3/2009 1:45 PMi 

12/3/20091:46 PM! 

12/3/2009 1:47 PM; 

12/3/2009 1:48 PMi 

12/3/2009 1:49 PM! 

12/3/2009 1:50 PMi 

12/3/20091:51 PM: 

12/3/20091:52 PM; 

12/3/2009 1:53 PM; 

12/3/2009 1:54 PM; 

12/3/20091:55 PMi 

12/3/20091:56 PM 

12/3/2009 1:57 PM: 

"12/3/2009 1:58 PMi 

12/3/2009 1:59 PMj 

12/3/2009 2:00 PMf 

12/3/2009 2:01 PMi 

12/3/2009 2:02 PM; 

12/3/2009 2:03 PM r 

"12/3/2009 2:04 PMi 

12/3/2009 2:05 PMi 

12/3/2009 2:06 PMi 

12/3/2009 2:07 PM! 

12/3/2009 2:08 PMi 

14984.3 

15014.5 

15040.9, 

15073.7 

1519 0 

T5207.4 

1522979 

15247.8 

15248.2 

15251.6 

15236.0 

15231.5 

^5212^! 

15192.5 

15175.2 

1516278, 

15147.9 

""1514179! 

'"1513478| 

"15"134.3 

1513976 

15143.3 

15145.5 

15158.0 

15147.0 

'15J55J 1 

15153.5, 

'1515273 

7514975 

15145,8 

1512576 

T5j27.9 

15120.4 

15120.9 

T5~fi'9.7 

1"5"118.3 

"l"5jl6!8 

T5l'2p| 

15139.2 

"'1514174 

15149.5 

1514978 

1514879 

15157.9 

15154.3 

15157.6* 

15164.3 

15172.1 

15174.5 

"I5l'8l74 

VES018405 
Uni

t 3 Run 3 

Time_Stamp StackFlowHRA 

12/3/2009 2:09 PM 15185.1 

12/3/2009 2:10 PM! 15185.3 

12/3/2009 2:11 PM; 1519073 

12/3/2009 2:12 PM 15198.9 

1 2/3/2009 2:13 PM 15199.5 

12/3/2009 2:14 PM; 15202.3 

"12/3/2009 2~15 PM 15214.6 

12/3/2009 2:16 PM! 15220.5 

12/3/2009 2:17 PMi ......

. ^224.1 

12/3/2009 2:18 PMl ' 152*3372 

12/3/2009 2:19 PM; 1522971 

12/3/2009 2:20 PMi 15227.5 

12/3/2009 2:21 PM; '15230.9 

12/3/2009 2:22 PM' 15235.6 

12/3/2009 2:23 PM; 15236.6 

12/3/2009 2:24 PM: '1524977 

12/3/2009 2:25 PM 15258.2 

12/3/2009 2:26 PM 15262.1 

12/3/2009 2:27 PM, 1526673 

12/3/2009 2:28 PM. 

"' '1527776 

12/3/2009 2:29 PM; 15285.5 

12/3/2009 2:30 PM; 15285.7 

12/3/2009 2:31 PM: 15300.5 

12/3/2009 2:32 PM! 15366.0 

12/3/2009 2:33 PM: 15311.7 

12/3/2009 2:34 PM; 15322.4 

12/3/2009 2:35 PM! 15327.6 

12/3/2009 2:36 PM; 15324.6 

12/3/2009 2:37 PM 15332.5 

12/3/2009 2:38 PMi 15332.3 

12/3/2009 2:39 PMj T5326.1' 

12/3/2009 2:40 PMi 15332.8 

12/3/2009 2:41 PM; 15329.6 

12/3/2009 2:42 PMi 153219 

12/3/2009 2:43 PM; 15326.5 

12/3/2009 2:44 PM; 15315.5 

12/3/2009 2:45 PM; 15307.3 

12/3/2009 2:46 PM; 15308.8 

12/3/2009 2:47 PMi 15308.5 

12/3/2009 2:48 PM! 1530773 

12/3/2009 2:49 PM; 15308.6 

12/3/2009 2:50 PM; 15287.0 

12/3/2009 2:51 PMi "1527476 

12/3/2009 2:52 PM 15263.7 

12/3/2009 2:53 PM; 15250.7 

12/3/2009 2:54 PM; 15244.6 

12/3/2009 2:55 PM; 15241.7 

12/3/2009 2:56 PMi 15233.7 

12/3/2009 2:57 PM 15234.0 

12/3/2009 2:58 PM; 15231.8 

VES018406 
Uni

t 3 Run 3 ' Time_Stamp StackFlowHRA 

15225.9 

15223.2 

1521872 

1518576 

15138.4 

15121.5 

1509379 

15061.2 

15045.1 

15027.1 

1501978 

£502679 

1501779 

15007.1 

1500272 

1500771 

15002.9 

150056 

1501279 

1500875 

1502376 

1502573 

15023.6 

15024.3 

1502974 

15023.'3 

15613.7 

1501772 

12/3/2009 3:27 PM,' 15025.1 

12/3/2009 3:28 PM; 15024.8 

12/3/2009 3:29 PM; 1502779 

12/3/2009 3:30 PMi 1503376 

12/3/2009 3:31 PM 15042.4 

12/3/2009 3:32 PMj 15044.8 

12/3/2009 3:33 PM! '15040.2 

12/3/2009 3:34 PMj ""15036. 9 

12/3/2009 3:35 PM, 

" "15030.2 

12/3/2009 3:36 PMi 1501873 

12/3/2009 3:37 PM; 15668.8 

12/3/2009 3:38 PMi 15008.4 

12/3/2009 3:39 PMi 15015.1 

12/3/2009 3:40 PMj 15012.7 

12/3/2009 3:41 PMi 15011.6 

12/3/2009 3:42 PMi 15019.4 

12/3/2009 3:43 PM; "1502674 

12/3/2009 3:44 PM' 1503576 

12/3/2009 3:45 PMj "I564473 

12/3/2009 3:46 PM; 15045.7 

12/3/2009 3:47 PM, 15039.3 

12/372009 3:48 PM! 15044.5 

12/3/2009 2:59 PMi 

"12/3/2009 3:00 PMj 

12/3/2009 3:01 PMj 

""12/3/2009 3:02 PMi " 

""12/3/2009 3:03 PMl 

"12/3/20093:04 PM '" 

"12/3/2009'3:05 PM; 

12/3/2009 3:06 PMi 

12/3/2009 3:07 PM7 " ' 12/3/2009 3:08 PM; 

12/3/2009 3:09 PMj 

"12/3/2009 3:10 PMj 

"12/3/2009 3:11 PMj 

12/3/2009"3:12 PM:: 

'12/3/2009 3:13 PM; 

12/3/2009 3:14 PMl 

""12/3/2009 3:15 PM; 

12/3/2009 3:16 PM7""" 

"12/3/20093:17 PMi " 

12/3/2009 3:18"PM|""" 

"12^^09JJ9£M:"" 

72/3/2009 3:20 PM; "" 

"12/3/2009 3:21 PMj 

12/3/2009 3:22" PMj 

12/3/2009 3:23 PMj 

"12/3/2009 3:24 PMP"'• 

12/3/2009 3:25 PM; 

"12/3/2009 3:26 PM; " " 

VES018407 
Unit 3 Run 3 

StackFloWHRA 

12/3/2009 3:49 PM! 15061.4 

12/3/2009 3:50 PM; 15084.9 

12/3/2009 3:51 PM: i'5098.3 

12/3/2009 3:52 PMi 15108.4 

12/3/2009 3:53 PM 15110.3 

12/3/2009 3:54 PM; 1512672 

12/3/2009 3:55 PM1 

' 15130.2 

12/3/2009 3:56 PM; 15137.T 

12/3/2009 3:57 PM; 15135.4 

"12/3/2009 3:58 PM] 15138.8 

12/3/2009 3:59 PM; 15143.5 

12/3/2009 4:00 PM; 15149.3 

12/3/2009 4:01 PMi 15156.8 

12/3/2009 4:02 PM1 15189.6 

12/3/2009 4:03 PM; 15242.5 

12/3/2009 4:04 PMi 15256.2 

12/3/2009 4:05 PMi 152815 

12/3/2009 4:06 PM: 15305.2 

12/3/2009 4:07 PMi 15325.7 

12/3/2009 4:08 PM; 15332.4 

12/3/2009 4:09 PM; 15340.6 

12/3/2009 4:10PMi 15338.0 

12/3/20094:11 PM| 15343.3 

12/3/2009 4:12 PM; "1535271 

12/3/2009 4:13 PMi '15353.9 

12/3/2009 4:14 PMi 15351.4 

12/3/2009 4:15 PMi 1534872 

12/3/2009 4:16 PM! 15352.2 

12/3/2009 4:17 PMi 15347.2 

12/3/2009 4:18 PM; 15347.3 

12/3/2009 4:19 PM; 15340.4 

12/3/2009 4:20 PMi 15333.9 

12/3/2009 4:21 PM; 15346.7 

12/3/2009 4:22 PMi 1533372 

12/3/2009 4:23 PM; 1532872 

Maximum! 1535379 

VES018408 
Uni

t 3 Run 3 

Timei Stamp LiquidWgtHRT •TotWgtHRT 

12/3/2009 10:491 

12/3/2009 10:49! 

"12/3/2009 10:49!" 

J2/3/2009 10:49; 

12/3/200910:50! 

12/3/2009 10:50; 

"12/3/2009 10:50; 

12/3/2009 10:50 

"12/3/2009 10:51; 

"12/3/2009 10:51-

12/3/200910:51! 

12/3/2009 10:51! 

12/3/2009 10:52r 

12/3/2009 10:52: 

3432.9) 

343376! 

3433!or 

"343375I" 

'3433.9, 

'3434.4;' 

''3434.8T 

34367:2! 

343777; 

3439.iT ' 3440!DT' 

"343871 [ 

'3435.5T 

~3433.fi 

12/3/2009 10:52; 

12/3/2009 10:52; 

12/3/2009 10:53 

12/3/2009 10:53! 

"12/3/2009 10:53;' 

12/3/2009 10:53! 

12/3/2009 10:54! 

12/3/2009 10:54! 

12/3/2009 10:54; 

12/3/2009 10:54! 

12/3/2009 10:55 

"12/3/2009 10:55 

12/3/2009 10:55! 

12/3/2009 10:55! 

12/3/2009 10:56: 

12/3/2009 10:56! 

"12/3/2009 10:56: 

12/3/2009 10:56 

12/3/2009 10:57; 

12/3/2009 10:57: 

12/3/2009 10:57; 

12/3/2009 10:57; 

12/3/2009 10:581 

12/3/200910:58! 

"12/3/2009 10:58|" 

12/3/2009 10:58! 

12/3/2009 10:59! 

12/3/2009 10:59! 

12/3/2009 10:59! 

12/3/200910:59! 

3431.1! 

3430.'4!' 

~342pT'" 

"3428.9;"" 

"34282: 

"3430JT 

3433.2 

343577;"' 

"343872;' 

3440.2 

344272; 

'3444.2. 

3446.2! 

'34477'2 

^3448^3!' 

3449.3: 

""345673!" 

3453.3" 

"3456.3;" 

"3459.3]' 

"346272!" 

|46i7'8r 

3461.6! 

"346676!" 

"3458.5!" 

"3453T4T 

344871; 

• " 343774! 

""342672!" 

4315.7 

4315.7 

4295.7 

429672 

"432373 

4323.7 

"432471 

'432575 

'430676 

"4368.0 

4336.7 

"433471 

"433176 

4329.1 

4305.1 

"'430473 

"43311 

12/3/2009 11:00! 

12/3/200911:00; 

12/3/2009 11:00: 

12/3/2009 11:00! 

12/3/2009 11:01; 

12/3/2009 11:01' 

3415.1) 

'340'472!' 

"339376]" 

'338578; 

'"'337872!' 

"337675; 

4330.3 

432976 

4332.1 

4313.5 

4316.6 

4345.2 

"434773 

"434973 

43513 

4333.6 

'43667J 

4361.8 

"436278 

436378 

'436678 

'4347.5 

"437776 

"4380.5 

4380.2 

4379.4 

""4378.4 

"437678 

""43517 

'4346.1 

4340.8 

"4335.4 

"4324'.'2 

43137 

"430272 

""42916 " 4263.5 

425578 

4248.2 

VES018409 
Unit 3 Run 3 

Time_Stamp LiquidWgtHRT ' To.tWgtHRT? J 

12/3/2009 11:011 3362.9; 4240.6 

12/3/2009 11:01 j ""3357.8 : 4261.7 

12/3/2009 11:02| 3353.0 425679 

12/3/2009 11:02! 334875; 4232.8 

12/3/2009 11:02! """'334471 ! '4228. 4 

12/3/2009 11:02; 3337.2; " "42217 6 

12/3/2009 11:03; 3330747 "'42 1 477 

12/3/2009 11:03; "332376 ; 4234.4 

12/3/2009 11:03! '331678 4227,6 

12/3/2009 11:03: 3313.5 4203.5 

12/3/2009 11:04! " 3310.2 """"426672 

12/3/2009 11:04| 3306.9 41 9679 

12/3/2009 11:04! 3303.7, 4193.7 

12/3/2009 11:04! 3366797 4218.6 

12/3/200911:05; 3298.1: 4215.9 

12/3/200911:05! 3295.6 4192.5 

12/3/2009 11:05! 329373!' ''41967 2 

12/3/2009 11:05- 3292.5: 4189.4 

12/3/2009 11:06! "3291.7 ; ' 4188.6 

12/3/2009 11:06! " 329176!' "4214*76 

12/3/2009 11:061 ""329017 4213.9 

12/3/2009 11:06; 3289.0! 4191.4 

12/3/200911:07; 3287.8 4190.1 

12/3/2009 11:07! "328675! 4188.9 

12/3/2009 11:07! 3285.3 

12/3/2009 11:07: 3282.1 " 421172 

12/3/2009 11:08! 3278.9 "

:

"4208. 6 

12/3/200911:08! 3275.6 "'4185.2 

12/3/2009 11:08! """3272. 1 418177 

12/3/2009 11:08! 3276.0; 4185.6 

12/3/2009 11:09! 3279.9! 4189.5 

12/3/2009 11:09! 3283.7" 4219.6 

. 12/3/2009 11:09; 3287.5 420271 

12/3/200911:09; 32857V "'"4 1 9977 

12/3/2009 11:10! 3282.7 419773 

12/3/2009 11:10! "3286.2, ""419478 

12/3/2009 11:10! 3277.7; 4 1 9273 

12/3/2009 11:10! 3276.9 '"""421972 

12/3/2009 11:11! "'3276. 1 4197.9 

12/3/2009 11:11! 3275.3 4197.1 

12/3/200911:11; 3274.6 " 4 1 9673 

12/3/2009 11:11! 3275.3! ' 4197.0 

12/3/2009 11:12; 3276.6: '42247 9 

12/3/2009 11:12! ""327677j"" 4225.7 

12/3/2009 11:12! 3277.'5| '420676 

12/3/2009 11:12; '3277.9 '4266.5 

12/3/2009 11:13; 3278.41 '4207.6 

12/3/2009 11:13; '"3278.9! " 4207.4 

12/3/2009 11:13; 3279.4. 

327873: 

4235.2 

12/3/2009 11:13! 

3279.4. 

327873: 4234.2 
Uni

t 3 Run 3 

iTirrie^ •LiquiaWgtHRT

. 1 TotWgtHRT1 

J2^/2009J114i 

12/3/2009 11:14; 

12/3/2009 11:14) 

•12/3/2009 11:14! 

12/3/2009 11:15; 

12/3/2009 11:15; 

12/3/2009 11:15; 

12/3/2009 11:15! 

12/3/2009 11:16! 

12/3/2009 11:16:' 

"12/3/2009 11:16;" 

12/3/2009 11:16! 

12/3/2009 11:17! 

12/3/2009 11:17; 

"12/3/2009 1"1:17! 

"12/3/2009 11:17 

12/3/2009 11:18; 

12/3/2009" 11:18!" 

12/3/2009 11:18! 

"12/3/2009 11:18: 

12/3/2009 11:19!' 

12/3/2009 11:19': 

12/3/2009 11:19; 

12/3/2009 11:19! 

12/3/2009 11:20; 

12/3/2009 11:20! 

12/3/2009 11:20;" 

12/3/200911:20! 

12/3/2009 11:21 f 

12/3/2009 11:21; 

12/3/2009 11:21! 

12/3/2009 11:21! 

12/3/2009 11:22 

12/3/2009 11:22: 

12/3/2009 11:22! 

12/3/2009 11:22' 

12/3/2009 11:23; 

"12/3/2009 11:23? 

12/3/2009 11:23; 

12/3/2009 11:23! 

"1273/2009 11:24;' 

12/3/2009 11:24. 

12/3/2009 11:24! 

12/3/2009 11:24: 

12/3/2009 11:251 

12/3/2009 11:25 

12/3/2009 11:25, 

12/3/2009 11:25; 

12/3/2009 11:26! 

12/3/2009 11:26! 

3277.3: 

3276.3! 

327573 

"327471 f 

327279] 

"327171" 

"327675!" 

Wiff " 

'7327277]"' 

"327378! 

3274.9: " 

"3273.1 

3271772! 

3269.3 

326774! 

3267.57 

3267.6!" 

"3267.6:" 

3267.7! 

"'326676;'" 

'326575]" 

"326473!" 

"32637721" 

3256.4! 

"7324975! 

'324277['' 

"323578

?

" 

'323572! 

"323476!" 

"323476!" 

3233.4; 

'323177;' 

"323671" 

'322874! 

"'322p r 

""3227.2!" 

"322775; 

"322779; 

"3228772!" 

322871 

322778! 

""322777!" 

3225778; 

'322379!" 

"322276! 

"7322076!" 

"321779;" 

'"3215777"]" 

"321376!" 

4212 3 

42113 

4210.3 

426971 

"423478 

"4233.5 

"420974 

4210.5 

"4211.6 

'421:277 

'4241.3 

4239.4 

"'4216.9 

4215.6 

4240.3 

424674 

"424675 

"424676 

"422672 

421971 

"421876 

42115.8 

"4194.7 

4187.9 

"418176 

4201.0 ' 4173.1 

-4172,4 

"41718 

4171.2 

4177.3 

417577 

417471 

"417274 

4170.8 

417773 

-41777 

"4178.0 

"4178.4 

415678 

4184.3 

"4184.2 

"418471 

"416174 

415975 

4186.0 

"418470 

"416679 

"4158.7 

"4156.6 

VES018411 
Unit 3 Run 3 

**!^Pffim^SStamp ' LiquidWgtHRT; TotWgtHRT 

12/3/2009 11 26 3211.4 4154.4 

12/3/2009 11 26 3209.5 417979 

12/3/2009 11 27 3207.6 4177.9 

12/3/200911 27 3205.6 417676 

12/3/200911 27 32037 "'417471 

12/3/2009 11 27 '"3207 . 6 4177.3 

12/3/2009 11 28 "3210. 2 4207.3 

1273/2009 11 28 3213.5 '""4210776 

12/3/2009 11 28 3216.8 421379 

12/3/2009 11 28 3222.3 4219.4 

12/3/200911 29 3227.8 4224.9 

12/3/200911 29 ""'32337 4 425879 

12/3/2009 11 29 ' 3238.9 4726474 

12/3/2009 11 29 3240.4 "42667 6 

12/3/200911 30 324270 426776 

12/3/2009 11 30 3243.6 4269.2 

12/3/200911 30 3245.2 429678 

12/3/2009 11 30 3250.6 4302.1 

12/3/2009 11 31 325579 4281.0 

12/3/200911 31 32613 "428673 

12/3/200911 31 3266.6 '42916 

12/3/2009 11 31 3268.4 4293.5 

12/3/2009 11 32 3276.3 " ":

 4324.0 

12/3/2009 11 32 3272.2 4325.8 

12/3/2009 11 32 3274.0 4300.9 

12/3/2009 11 32 3272.4 4299.3 

12/3/2009 11 33 3270.8 429777 

12/3/2009 11 33 3269.21 4322.8 

12/3/200911 33 3267.61 43212 

12/3/2009 11 33i 3265.5 4292.4 

12/3/2009 11 34 326374 429673 

12/3/2009 11 34 32613 "42887 2 

12/3/2009 11 34; 325972 131378 

12/3/2009 11 34 325879 431 374 

12/3/2009 11 35! ""325875 4313.6 

12/3/2009 11 35: 3258.1 4286.6 

12/3/200911 35 3257.8 ""42857 6 

12/3/2009 11 35; "'"325677 431376 

12/3/2009 11 36! 325576 4311.8 

12/3/2009 11 36; 3254.4 '"''431677 

12/3/200911 36; "325373 430976 

12/3/2009 11 36; 325674 ""'42797 1 

12/3/2009 11 37« "3247. 6 430376 

12/3/200911 37! 3244.7 4300.1 

12/3/2009 11 37i 32419 429773 

12/3/2009 11 37; 324676 '4295.4 

12/3/2009 11 38' 3238.2 4293.6 

12/3/2009 11 38! "3236.3 426874 

12/3/2009 11 38 '

:

32347 4 " '4266.5 

12/3/2009 11 38 '73231 3 ""4 2 9078 
Unit 3 Run 3 

'•'•i:y>- Time'iStarnp: •«¥!' *SS- LiquidWgtHRT •,?TbtWgtHRTi. 

12/3/2009 11 39 3228.2 4287.7 

12/3/2009 11 39 "3225. 0 """"428475 

12/3/2009 11 39 ' 3221.8 42813 

12/3/2009 11 39 32210 ''425376 

12/3/2009 11 40 32 2671 425277 

12/3/2009 11 40 3219.2 " 7 4278.7 

12/3/2009 11 40 3218.3 427778 

12/3/2009 11 40 3215.2 4274.7 

12/3/2009 11 41 3212.1 4271.6 

12/3/2009 11 41 3209.6 4241.3 

. 12/3/2009 11 41 320578 " 4238.2 

12/3/2009 11 41 3264.8 """"42637 7 

12/3/2009 11 42 3203.8 "'4262. 7 

12/3/2009 11 42| 3202.8 426177 

12/3/2009 11 42 3201.9 4233.8 

12/3/2009 11 42 32014 4233.3 

12/3/2009 11 43 3200.9 4232.8 

12/3/2009 11 43 37200.4' '4232.3 

12/3/2009 11 43 ""'" 3199.9 423179 

12/3/2009 11 43 326674 4260.1 

12/3/20.09 11 44 320176 4266.7 

12/3/2009 11 44 3201.5. 4261.2 

12/3/2009 11 44 3202.0 4261.7 

12/3/2009 11 44 "32017 5 """"4261. 2 

12/3/2009 11 45 '326*16 '4260.7 

12/3/2009 11 451 "326675 4234.6 

12/3/2009 11 45 3200.0 ""'4233. 5 

12/3/2009 11 45 3196.3 "' 4257.6 

12/3/2009 11 46 *"'31927 6 42 5379 

12/3/2009 11 46 3188.8 " 4250.2 

12/3/2009 11 46 3185.21 

" 424675 

12/3/2009 11 46 " 318576 4219.2 

12/3/2009 11 47 318671 4219.6 

12/3/2009 11 47 3186.6' 422671 

12/3/2009 11 47 3187.1 " 4220.6 

12/3/200911 47 3183.6 4217.1 

12/3/2009 11 48 "'318671 " "42418 

12/3/2009 11 48 ""317677 423873 

12/3/2009 11 48 3173.2 '""'4207775 

12/3/2009 11 48 31 "71.5 " 420578 

12/3/2009 11 49 ""*".'3169.9 ' " 4204.2 

12/3/2009 11 49 '''3168.2" """42'62". 5 

12/3/2009 11 49 " 316675 420678 

12/3/2009 11 49 3165.6 4199.9 

12/3/2009 11 50 3164.6, 4199.7 

12/3/200911 50 3163.7 419877 

12/3/2009 11 50: 3162.7 4197.7 

12/3/2009 11 50 3160.7 4195.8 
Unit3 Run 3 

^TirheiStamp, "; LiquidWgtHRT: TotWgtHRT." 

12/3/2009 13:191 

12/3/2009 13:19. 

12/3/2009 13:19: 

12/3/2009 13:19; 

12/3/2009 13:20; 

12/3/2009 13:20" 

T2/3/20Q9 13:20i 

"12/3/2009 13:20'.' 

12/3/2009 13:21; 

12/3/2009 13:21: 

12/3/2009 13:21; 

12/3/2009 13:21! 

12/3/2009 13:22! 

12/3/2009 13:22;' 

12/3/2009 13:22; 

12/3/2009 13:22; 

12/3/2009 13:23: 

12/3/2009 13:23: 

12/3/2009 13:23! 

12/3/2009 13:23; 

12/3/2009 13:24! 

12/3/2009 13:24; 

12/3/2009 13:24; 

12/3/2009 13:24 

12/3/2009 13:25! 

12/3/2009 13:25 

12/3/2009 13:25! 

12/3/2009 13:26! 

12/3/2009 13:26! 

12/3/2009 13:26! 

12/3/2009 13:26! 

12/3/2009 13:27! 

12/3/2009 13:27! 

12/3/2009 13:27! 

12/3/2009 13:27j 

12/3/2009 13:28! 

12/3/2009 13:28; 

12/3/2009 13:28! 

12/3/2009 13:28; 

12/3/2009" 13:29; 

12/3/2009 13:29! 

12/3/2009 13:29! 

12/3/2009 13:29! 

12/3/2009 13:30! 

12/3/2009 13:30! 

12/3/2009 13:30! 

12/3/2009 13:30; 

12/3/2009 13:31!' 

12/3/2009 13:31!" 

3224.4] 

32412! 

3258.6 

32721]' 

3286.2! 

"33'66."3T 

'333l'.6|" 

3347:6] 

'3364T1!'' 

'33807!" 

"3396T6T 

"mii'.IT' 

"34*26.71" 

"34421]' 

3457.4! 

l4~727f 

"3488.31 

35637!' 

"35p!6! 

3536.4! 

35527! 

"3569.61" 

3584.6: 

"3666.2! 

"3"6l57i' 

'36313]" 

"3646:4!" 

'3661.6!'' 

3704.4 

. 

3738.0 

3752.1 

3766:2 

"380478 

'"381879 

383575 

'3852.1 

"3868.6 

388572 

"3924.4 

'393977 

"3955.1 

3970.4 

39857 

'40011 

4040.4 

'465578 

407271 

"4688.4 

4104.8 

41211 

4160.9 

"4"l"767'5 

'"419276 

4207.6 

•4222.7 

4262.5 

3675.3 

3688.6 

"369978] 

"3711.1 r 

"372276] 

"3737279!" 

374374!" 

'375476'" 

'376475|' 

'3775.1 

377679!" 

377877;" 

'"378676! 

'3782.3! t 

3785.3; 

"3788 73|" 

'"379127! 

"37 9471:""' 

'379576]' 

"379776!" 

3795767 

4276.8 

'4289.5 

"436173 

"4312.6 

"4323.5 

"4357.3 

43678 

4378.4 

4389.6 

4399.5 

44014 

"4427.6 

4428".8 

4430.6 

"4433.6 

443676 

"4439.5 

'446675 

"44679 

"4469.4 

4467.9 
Unit 3 Run 3 

TimeAStamp': "LiquidWgtHRT I " TotWgtHRT 

12/3/200913:31 

12/3/2009 13:31; 

12/3/200913:32; 

12/3/200913:32! 

12/3/2009 13:32; 

12/3/2009 13:32]'' 

12/3/200913:33: 

12/3/2009 13:33: 

12/3/2009 13:33; 

12/3/2009 13:33! 

12/3/2009 13:34; 

12/3/2009"l3:34:" 

3794.0 

3795.9 

'379778. 

'379976' 

'38615! 

380179; 

3802.3 

'380276! 

380278| 

''38016! 

'3806.4! 

12/3/2009 13:34 

12/3/2009 13:34; 

12/3/2009 13:35! 

12/3/200913:35; 

12/3/2009 13:35! 

12/3/200913:35; 

"12/3/2009 13:36! 

12/3/2009 13:36! 

12/3/2009 13:36! 

12/3/2009 13:36! 

12/3/2009 13:37: 

12/3/2009 13:37; 

12/3/200913:37! 

12/3/2009 13:37! 

"12/3/2009 13:38' 

3799.3; 

'T798.lT" 

"Z795ST 

379577] 

''3794:5]'" 

_379373!" 

3795.3: 

"379773! 

3799.3T 

38014"; 

"380p7lT 

"3798.8] 

37976! 

'3796.47 

3795:2] 

3793.9] 

12/3/2009 13:38! 

12/3/2009 13:38! 

12/3/2009 13:38! 

12/3/2009 13:39 

12/3/2009 13:39; 

12/3/2009 13^39] 

"12/3/2009 13:39?" 

12/3/2009 13:40; 

12/3/2009 13:40! 

12/3/2009 13:40! 

12/3/2009 13:40; 

12/3/2009 13:41! 

12/3/2009 13:41! 

jn2iW^9^:41 ! 

12/3/2009 13:41. 

3792.7! 

'379147' 

379174!" 

37912! 

' 37911]' 

''379678" 

' 37913] 

3791:8}" 

"379274" 

' 3792.91" 

"379176] 

3790.4J 

378971] 

3787.9! 

1. 

12/3/2009 13:42; 

12/3/2009 13:42; 

12/3/2009'13:42! 

12/3/2009 13:42; 

12/3/2009 13:43; 

12/3/2009 13:43: 

12/3/2009 13:43. 

12/3/2009 13:43! 

"3788.7! 

3789.5; 

'379673!' 

3791.1] 

'3783.6''' 

'377671 

]376876i"" 

3761.6] 

375976' 

4466.3 

4468.2 

448971 

'44916 

449279 

"4493.3 

449377 

449476 

4518.8 

4496.1 

4494.9 

"449377 

449275 

~44jFT.3 

.4513.5 

451273 

'45111 

"4492.I 

4494.1 

4496.1 

4523.2 

452276 

"452677 

451974 

'451872 

4495.9 

'4518.5 

"45173 

45 1 670 

4515.9 

451578 

"4515.6 

4539.2 

451877 

"451972 

4519.7 

4520.2 

"451879 

"4540.5 

453972 

4538.0 

4514.3 

451 571 

"•451579 

"451677 

"4532.0 

4524.5 

"45170 

]4509.4 

448772 
Unit3 Run 3 | 

Time_Stamp LiquidWgtHRT | TotWgtHRT-. 

12/3/2009 13:441 

"12/3/2009 13:44i 

12/3/2009 13:44: 

12/3/2009 13:44. 

12/3/2009 13:451 

"l2/3/2009""l3:45 ' 

12/3/2009 13:45: 

12/3/2009 13:45: 

12/3/2009 13:46' 

12/3/2009 13:46; 

12/3/2009 13:46r 

"12/3/2009 13:46":" 

12/3/2009 13:47i 

12/3/2009 13:47; 

12/3/2009 13:47; 

"12/3/2009 13:47;' 

12/3/2009 13:48; 

12/3/2009 13:48: 

12/3/2009 13:48' 

"12/3/2009 13:48: 

12/3/2009 13:49; 

12/3/2009 13:49: 

12/3/2009 13:49; 

12/3/2009 13:49! 

12/3/2009 13:50; 

12/3/2009 13:50;' 

12/3/2009 13:50. 

12/3/2009 13:50; 

12/3/2009 13:51;"' 

12/3/2009 13:51: 

12/3/2009 13:511 

12/3/2009 13:51; 

12/3/2009 13:52j" 

"12/3/2009 13:52 

12/3/2009 13:52; 

12/3/2009 13:52: 

12/3/200913:53: 

12/3/2009 13:53; 

12/3/2009 13:53! 

12/3/2009 13:53; 

12/3/2009 13:54; 

12/3/2009 13:54; 

12/3/2009 13:54; 

12/3/2009 13:54; 

12/3/2009 13:55; 

'12/3/2009 13:551' 

"12/3/2009 13:551 

12/3/2009 13:55 

12/3/2009 13:56. 

"12/3/2009"13:56; 

3758.2; 

3756.7! 

375573; 

3752.1: 

374879; 

3745.7" 

"3742.5 

374275; 

"374275]" 

"374276;" 

3742777 

3738.7 

'3734777 

373677; 

3726.7 

3723.0 

3719.3' 

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3711.9;" 

"370779; 

370379. 

376676!" 

369676 

3691.1 

36 86721 

3681.3! 

367674' 

"3673.6:' 

"366974!' 

3665.81" 

3662721" 

"3661.3' 

3660.4; 

3659.5 

365874! 

3655.67 

"365278!" 

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3647.3! 

"3647r72r 

36471; 

"3647.1!" 

'3647.07 

364572; 

'36431.3 

3641.5: 

3639.7 

364177! 

364379! 

3646.1! 

4485.8 

"4508.1 

45 0676 

'456375 

4500.2 

4497.0 

4493.8 

451774j 

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''4496.4; 

4496751 

449275 

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448278 

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4456.0 

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445578 

4455.8 

4478.8 

447770 

4475.2 

4473.4 

4475.4 

447775 

4504.3 
Unit 3 Run 3 

- Tiroe^Stanip. LiquidWgtHRT ..TotWgtHRT, | 

12/3/200913:56, 

12/3/2009 13:56; 

12/3/200913:57: 

12/3/200913:57" 

12/3/2009 13:57 

12/3/200911757 

"12/3/2009 T3"58 

12/3/2009 13:5~8, 

13:58: 

13:58: 

12/3/2009 "13:59 

J2/3/2009 

12/3/2009" 

12/3/2009 13:59: 

"12/3/2009 13:59 

12/3/2009 

12/3/2009 

12/3/2009 14:01! 

12/3/2009 14:02! 

12/3/2009 14:02: 

12/3/2009 14:03': 

12/3/2009 14:04! 

12/3/2009 14:07! 

13:59: 

14:00! 

12/3/2009 li00 : 

"l2/3/2009~14:06: 

12/3/2009 14:00" 

"12/3/2009 14:01 

12/3/2009 14:01'" 

12/3/2009 14:01; 

12/3/2009 14:02; 

12/3/2009 14:02: 

12/3/2009 14:03-

12/3/200914:63! 

12/3/2009 14:03! 

12/3/2009 14:04! 

12/3/2009 14:04; 

12/3/200914:04! 

12/3/2009 14:05 

12/3/2009 14:05-' 

12/3/2009 14:05 

12/3/2009 14:05;" 

12/3/2009 14:06 

"12/3/2009 14:06:' 

"12/3/200914:06 

"12/3/2009 14:06" 

'12/3/2009 14:07;' 

12/3/2009 14:07! 

12/3/2009 14:07! 

12/3/2009 14:08! 

12/3/2009 14:08-

12/3/2009 14:08! 

"12/3/2009 14:08r 

3648.4; 

3656.9. 

""366575!" 

"3674.0:" 

3682.6: 

36907, 

3698.8 

376'6'!8: 

37.479 

3714! 8;' 

3714.7 

'3714.6] 

"'371 474!" 

3715.1 

4506.6 

"4515.1 

4523.7 

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4540.8 

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4574.5 

T57474 

4574.2 

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3715.6! 

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3716.'9 

"37161!" 

3715.2;" 

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3713.4!" 

371757 

37215] 

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3723.9 

371876!" 

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"3705.37 

3704.3; 

376372] 

370271! 

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3699.5: 

3698757' 

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! 369679:' 

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4609.8 

"461379 

460870 

460272 

457276 

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458876 

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4583.9 

4583.0 

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45813 

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"4581.7 

T582.2 

458277 

4583.2 

'458372 

458376 

"458376 

"458376 

'4583.7 
Uni

t 3 Run 3 

•Time^Starnp:: LiquidWgtHRT TotWgtHRT 

12/3/2009 14:09! 

12/3/2009 14:09; 

"12/3/2009 14:09; 

12/3/2009 14:09; 

12/3/2009 14:10; 

12/3/2009 14:10! 

12/3/2009 14:10 

"12/3/2009 14:10; 

12/3/2009 14:11 

12/3/2009 14:11: 

12/3/2009 14:11; 

12/3/2009 14:11; 

12/3/2009 14:12!" 

_12/3/2009 

12/3/2009 

14:12; 

14:12; 

12/3/2009 14:12! 

12/3/200914:13! 

12/3/2009 14:13r 

"12/3/200914:13!" 

"12/3/2009 14:13. 

12/3/2009 14:14; 

12/3/2009 14:14,' 

12/3/2009 14:14! 

12/3/2009 14:14-

"12/3/2009 14:15! 

12/3/2009" 14:15! 

12/3/2009 14:15! 

12/3/2009 14:15! 

"12/3/200914:16! 

12/3/2009 14:16; 

12/3/2009 14:16: 

12/3/2009 14:16 

12/3/2009 14:17; 

12/3/2009 14:17," 

12/3/2009 14:17 

12/3/2009 14:17! 

12/3/2009 14:18 

12/3/2009 14:18: 

12/3/2009 14:18; 

12/3/2009 14:18' 

12/3/2009 14:19, 

12/3/2009 14:19 

12/3/2009 14:19] 

"12/3/2009 14:19! 

12/3/2009" 14:20! 

12/3/2009 14:20,. 

12/3/2009 14:20: 

12/3/2009 14:20 

12/3/2009 14:21"! 

3700.5 

37012! 

3701.9"; 

3702.3 

"3762.8! 

376317" 

376378; 

370672": 

"370877; 

37T12T 

37i"3.6"" 

"3717276! 

"371T76

1

" 

3716.6, 

370975; 

3710.2! 

3716.9; 

"3711.7 

3712.4 

3712.3; 

3712.3! 

"371274!" 

371274; 

3715.6!" 

"37i'75;" 

37267i[" 

3722.7| 

372678!* 

"3719.9; 

371879;" 

^Oj f 

'37 2275 

3724.2 ' 

172676!" 

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3727.1. 

372776! 

1728721 

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"37 1 971! 

"3714.9!" 

4584.5 

4585.2 

"45'84".7 

'4585.2 

'458576 

"4586.1" 

12/3/2009 14:21 

37_10.5[ 

171274!" 

3714.2: 

1716.67 

"3717.9:" 

171727 

_37167'5!' 

371578! 

4586.6 

-458971 

'461776 

"459574 

45978 

"459678 

459578 

4594.8 

4617.2 

4593.2 

"459379 

"459476 

4595.3 

459573 

4622.9 

"462376' 

462176 

4625.6 

462871 

4655.4 

4657.9 

4657.0 

4656.1 

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4679.9 

46817 

4683.5 

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468578 

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468679 

4687.4 

465975 

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465076 

4671.1 

467376 

4674.8 

465271 

"4651.9 

4653.3 

4676.3 

"4575.6 

VES018418 
Uni

t 3 Run 3 

Time^Starop LiquidWgtHRT ^TptWgtHRTVl J 2/3/2009 

f2?3/200§' 

14j21i 

14:21; 

12/3/2009 14:22;. 

"12/3/2009 14:22" 

l2/3/2"609"l4:22; 

12/3/2009 14:22f 

12/3/2009 14:23; 

12/3/2009 14:23 

12/3/200914:23" 

12/3/2009 14:23; 

12/3/2009 14:24-

12/3/2009 14:24; 

"12/3/2009 14:24; 

12/3/2009 14:24; 

12/3/2009 14:25! 

12/3/2009"l4:25! 

12/3/2009 

""12/3/2009 

"12/3/2009 

"12/3/2009 

14:25; 

14:25r 

14:26! 

14j26j 

"12/3/200914:26! 

12/3/2009 14:26;' 

12/3/2009 14:27] 

12/3/2009 14:27; 

12/3/2009 14:27, 

12/3/2009 14:27; 

12/3/2009 14:28i 

12/3/2009 14:28 

12/3/2009 14:28! 

12/3/2009 14:28j 

12/3/2009 14

r

29! 

"12/3/2009 14:29. 

12/3/2009 14:29, 

12/3/2009 14:29. 

12/3/2009 14:30! 

12/3/2009 14:30! 

12/3/2009 14:30! 

12/3/2009 14:30: 

12/3/2009 14:31 

12/3/2009 

12/3/2009 

14:31: 

14:31! 

12/3/2009 14:32! 

12/3/2009 14:32; 

12/3/2009 14:32: 

12/3/2009 14:32! 

12/3/2009 14:33; 

'12/3/2009 14:33!' 

12/3/2009 14:33: 

12/3/2009" 14:33f 

3715.1: 

3712:7.' 

3710.3, 

"37679T 

"3705:5! 

12/3/2009 14:31; 

3705.0; 

''3704.6;' 

"3703.9; 

3703.4 

3704:2: 

'376576! 

3705.8' 

..„„,. , 

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3765.3 

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"3763:9; 

370576; 

3706.1! 

37671: 

3708.0! 

— 

"3769:5! 

"3712:6! 

371472"!" 

3715.0 

"3715:7!"" 

"371675! 

3717.3; 

" 3719"7i" 

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"3723".2T 

"372675]" 

"372671; ' 

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3^24jp 

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3728.3! 

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l73T._9"f 

3731.4; 

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373675!'" 

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"372975!" 

372973; 

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4675.0 

"4648.7 

"464673 

"464379 

4665.8 

466573 

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4662.4 

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4660.5 

4659.8 

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4636.8 

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4645.5 

4646.2 

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46716 

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Ji527"4 

"465477 

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4680.4 

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467975 

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4656.8 

4658.6 

4683.5 

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"4684.8 

"466p 

"4664.8 

466473" 

468774 

468'7.2 

"4687.1 

'466271 

"466572 

VES018419 
Unit3 Run 3 

Time_Stamp LiquidWgtHRT TotWgtHRT 

12/3/2009 14:34: 

12/3/2009 14:34;. 

'12/3/2009 14:34^ 

12/3/2009 14:34: 

"12/3/2009 14:35] 

12/3/2009 14:35; 

12/3/2009 14:35. 

12/3/2009 14:35; 

12/3/2009 14:36T 

12/3/2009 14:36; 

12/3/2009 14:36;" 

12/3/2009 14:36 ' 

12/3/2009 14:37? 

12/3/2009 14:37j 

12/3/2009 14:37!" 

"12/3/2009 14:37 

12/3/2009 14:38j 

12/3/2009 14:38;" 

12/3/2009 14:38: 

12/3/2009 14:38! 

12/3/2009 14:39!' 

12/3/2009 14:39, 

12/3/200914:39' 

12/3/200914:39 

12/372009 14:40 " 

"12/3/2009 14:40, 

"12/3/2009 14:40!" 

12/3/2009 14:40! 

12/3/2009 14:41! 

12/3/2009 14:41: 

12/3/2009 14:41. 

12/3/2009 14:41, 

12/3/2009 14:42: 

12/3/2009 14:421 

12/3/2009 14:42; 

12/3/2009 14:42! 

12/3/2009"T474l! 

12/3/2009 14:43! 

12/3/2009 14:43!" 

12/3/2009 14:43' 

12/3/2009 14:44[ 

12/3/2009 14:44! 

12/3/2009 14:44! 

12/3/2009 14:44! 

12/3/2009 14:457 

12/3/2009 14:45: 

12/3/2009 14:45: 

12/3/2009 14:45; 

12/3/2009 14:46 

12/3/2009 14:46! 

3735.3i 

3738.4; 

374T4!"' 

3742.6 

3742.5:' 

3743.0 

"3743.6 

3740.1 

3736.7 

3733.3 

'3729.9 

37317a 

'3734*0] 

"373671] 

J7381; 

' 3738.9! 

3_73'9.6: 

3746!5! 

374173* 

U 

3742.0] 

'3742.6.' 

3743.4! 

374472' 

3745.2: 

'3746.3; 

3747:3: 

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"374973!" 

3749.61" 

3750.1; 

'37567:' 

3751.2; 

IFs'll ] 

3752.8]" 

3J53.W 

3754.9 

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3764.6. 

'3768.6] 

"377276] 

1770.6! 

3769717 

'""37677;' 

"3766.2; 

3767.3 

37681! 

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4668 2 

4695.0 

469876 

4698.6 

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4676.3 

4676.8 

4696.8 

4693.4 

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4661 "6' 

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4665.7 

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4693.5 

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4671.2 

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467279 

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4675.6 

4676.7 

4700.3 

4701.3 

4761.6 

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4679.5 

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4763.7 

]4704.3 

470478 

"468376 

468476 

4768.4 

4709.5 

471375 

4726I 

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472277 

'4721".2 

"474371 

4741.7 

"471972 

4720.2 

"4744.8 
Unit

3 Run 3 

Time_Stamp LiquidWgtHRT TotWgtHRT, 

12/3/2009 14:46; 

12/3/2009 14:46-

12/3/2009 14:47; 

"12/3/2009 14:47?' 

"12/3/2009 14:47; 

12/3/2009 14:47' 

12/3/2009 14:48, 

12/3/2009 14:48, 

12/3/2009 14:48, 

12/3/2009 14:48; 

"12/3/2009 14:49; 

12/3/2009 T4?49; 

12/3/2009 14:49; 

12/3/2009 14:49; 

12/3/2009 14:50: 

12/3/2009 14:50; 

12/3/2009 14:50! 

12/3/2009 14:50' 

12/3/2009 14:51! 

12/3/2009 14:51j 

12/3/2009 14:51|" 

12/3/2009 14:51! 

12/3/2009 14:52! 

12/3/2009 14:52? 

12/3/2009 14:52" 

12/3/2009 14:52! 

12/3/2009 14:53! 

12/3/2009 14:53'* 

12/3/2009 14:53. 

12/3/2009 14:53! 

12/3/2009 14:54 

12/3/2009 14:54 

12/3/2009 14:54[ 

12/3/2009 14:54?' 

12/3/2009 14:55: 

12/3/2009 14:55! 

12/3/2009 14:55! 

"12/3/2009 14:551 

12/3/2009 14:56! 

12/3/2009 14:56! 

12/3/2009 14:56! 

12/3/2009 14:561 

12/3/2009 14:57! 

12/3/2009 14:57! 

12/3/2009 14:57! 

12/3/2009 14:57! 

12/3/2009 14:58j 

12/3/2009 14:58 

12/3/2009 14:58; 

12/3/2009 14:58: 

3770.4i 4745.9 

"3776.7 

'3771.0 4746.4 

3771.3; 4722.4 

3771.5! 4722.7 

3775.1: 4726.2 

3778.6! 4729.7 

3782.1; 4733772 

378"5?6; 4736.7 

3788.4" 473975 

3791.2 ""472676 

379476; 4722.8 

379678! 4725.6 

'379371! 4721.9 

3789.4! 4718.2 

3785.67 4714.5 

3781.9:. 4686.6 

3778.2! 4682.2 

"377474! 

" 4678775 

3770.7: 4674.7 

376679! 4670.9 

375974! 4663.5 

3751.9! 4631.6 

3744.3 .. . —

24 q 

3736.8! "'

" 461675 

3732.2! 4612.0 

'7372777? 4607.4 

'''3772372; " 

" "45797'6 

3718.6; 4575.1 

3715.1; 4571.6 

3711.6 """"456871" 

3708.1! "458771 

3704.5! 4583.6 

7376675| 4566.6 

""370874: '4562.5 

371074! 456475 

3712.3; 4566.4 

37iT.5r",~ 

:

'4589. 2 

3710.8. 4588.4 

"3710.61 456371 

370972! 456273 

3709.7; ""

" 4562778 

" 3710.1 

"' ""4563.2 

3710.5 4586.7 

"3711.6? 458772 

"'371277!" 456475 

3714.4; ""

" '4566.2 

3716.1; 4567.9 

3717.7; 456976 

""""3716? 9! 4592.1 

VES018421 
Uni

t 3 Run 3 

Time_Stamp LiquidWgtHR

T | TotWgtHRT 

12/3/2009 14:59^ 

"12/3/2009 14:59 

"12/3/2009 14:59; 

12/3/2009 14:59 

"12/3/2009 15~00: 

12/3/2009 15:00; 

"12/3/2009 15:00; 

12/3/2009 15:00 

12/3/2009 15:01 j 

12/3/2009 15:01r 

12/3/2009 15:01, 

12/3/200915:01; 

12/3/2009 15:02": 

12/3/2009 

12/3/2009 

15j02 

15:02! 

12/3/2009 15:02 

12/3/2009 15"03"i 

12/3/2009 15:03|" 

12/3/2009 15:03; 

12/3/2009 15:03; 

12/3/2009 15:04! 

12/3/2009 15:04!. 

12/3/200915:04; 

12/3/2009 15:04; 

12/3/2009 15:05: 

12/3/2009 15:05; 

12/3/200915:05; 

"12/3/2009 15:05 

12/3/200915.06; 

"12/3/2009 "15:06!" 

12/3/2009 15:061 

12/3/2009 15:06 

'12/3/2009 15:07; 

12/3/2009 15:07! 

12/3/2009 15:07, 

12/3/2009 15:07; 

"12/3/2009 15:08 

12/3/2009 15:08, 

12/3/2009 15:08? 

12/3/2009 

"12/3/2009 

15j08; 

15:09; 

12/3/2009 15:09 

12/3/2009 15:09." 

12/3/2009 15:09; 

12/3/2009 15:10; 

'12/3/2009 15:10]" 

12/3/2009 15:10 

12/3/2009 15:10; 

12/3/2009 15.11; 

12/3/2009 15:11? 

3716.2! 

3715747 

171 476! 

371676!' 

3717.5, 

3718.9 

372073; 

372575] 

373077] 

"373578: 

373976] 

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"372l'76i" 

"3711737 " 3701.6]' 

36971; 

3692776] 

368876; 

368375!" 

'""367T75!" 

3660.6!" 

"""3648.8'''' 

3637.7 

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"361475! 

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"359774! 

3587.6] 

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356611 

150479!' 

" 356378] 

3502.6! 

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356673!: 

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349379! 

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4591.3 

"456676 

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45*66.6 

456871 

4592.9 

4594.4 

457671 

458173 

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4571.6 

•453774 

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4523.2 

4518.7 

4536.5 

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448379 

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446177 

445377 ' 4*42271 

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4407.4 

4472676 

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4365.7 

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4348.9 

434675 

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4'287'76 

4363.'2 

4362.1 

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"429978 

4275.3 

"42 7471 

"427279 

"427178 

"4270.6 

"42677 

4239.4 

'42367'5 

VES018422 
Unit3 Run 3 

Time^_Stamp LiquiijWgtHRT TotWgtHRT •• 

12/3/2009 15:11j 3485.2 

12/3/2009 15:11! 

12/3/2009 15:12;' 

12/372009 15:12! 

"12/3/2009 15:12 

12/372009 15:12! 

'12/3/2009 15:13' 

12/3/2009" 15:13 

12/3/2009 15:13j 

12/3/2009 15:13;" 

12/3/200915:14,"" 

12/3/2009 15:14! 

12/3/2009 15:14! 

"2/3/2009 15:14"' 

"12/372009 15:15* 

12/3/200915:15 

12/3/2009 15:15! 

12/3/2009 15:15 

12/3/2009 15:16, 

"12/3/2009 15:16! 

12/3/2009 15; 16! 

12/3/2009 15:16; 

12/3/2009 15:17 

12/3/2009 15:17? 

"12/372009 15:17 

12/3/2009 15:17: 

12/3/2009 15:18; 

12/3/2009 15:18! 

12/3/2009 15:18; 

12/3/2009 15:18; 

12/3/2009 15:19; 

12/3/2009 15:19} 

'12/3/2009 15:19!" 

12/3/2009 15:19! 

12/3/2009*15:20!" 

12/3/2009 15:20; 

12/3/2009 15:207 

12/3/2009 15:20!" 

12/3/2009 15:21 

12/3/2009 15:21! 

12/3/2009 15:21! 

12/3/2009 15:21! 

12/3/2009 15:22! 

12/3/2009 15:22' 

3485.9; 

3486'2! 

3486.7! 

3486"!8; 

3486.8 

3486.9! 

"31873; 

'3487.6! 

3487!8 

34881'! 

348975! 

349T.6] 

3492."5t 

3494.6' 

3494.0'; 

3493.9: 

3493.9 

'3493.8 

348676! 

3479.4 

347272! 

'3465.6; 

'34687;' 

3472.5 

347672: 

3479.9!" 

"348367 

"3486.6[ 

3488.9; 

'34918"!" 

3496!7] 

348977!' 

34886!" 

"3487.6! 

'3489767' 

3490.5! 

'3492.6!' 

'349374! 

349676; 

349"9.8f 

3503.1 

12/3/2009 15:22! 

12/3/2009 15:22; 

12/3/2009 15:23; 

12/3/200915:23;" 

12/3/2009 15:23, 

12/3/2009 15:23; 

3506.2! 

'35jp7.5!' 

"350877;' 

'35lo!6T 

"35114! 

'35166;'" 

4233.6 

42340 

4234.3 

423476 

'423474 

"423475 

42346 

4234.7 

4234.8 

4257.9 

"42367 

42366 

423l7i 

"'4255.5 

42570 

"4233.8 

"423573 

425873 

425873 

4258.2 

"4258."2 

42276 

"4243.2 

"42361 

422879 

423276 

4259.1 

"42626 

4266.6 

42696 

"42664 

"42996 

4277.4 

4276.4 

"42751 

42972 

'4296.2 

"42976 

427573 

"429974 

"4300.8 

"430476 

743672 

'433476 

' 43T26 

"•'4314.1 

"4315.3 

"4316.6 

431876 

"4297.2 
Unit

3 Run 3 

fflTJmeiiStamp LiquidWgtHRT TotWgtHRTjfe: 

12/3/2009 15:24; 

12/3/2009 15:24; 

12/3/2009 15:24' 

12/3/2009 15:24; 

"12/3/2009 15:25' 

12/3/2009 15:25; 

12/3/2009 15:25; 

12/3/2009 15:25. 

12/3/2009 15:26; 

12/3/2009 15:26, 

12/3/2009 15:26: 

12/3/2009 15:26s 

12/3/2009 15:27; 

12/3/2009 15:30; 

12/3/2009 15:31! 

12/3/2009 15:27j 

"12/3/2009 15:27! 

12/3/2009 15:27:?" 

12/3/2009 15:28 

12/3/2009 15:28;" 

12/3/2009 15:28! 

'12/3/2009 15:26 

12/3/2009 15:29! 

12/3/2009 15:29'" 

12/3/2009 15:29. 

12/3/2009 15:29; 

12/3/200915:30' 

"12/3/2009 15:30:'" 

12/3/2009 15:30: 

12/3/2009 15:31; 

12/3/2009 15:31S 

12/3/2009 15:31; 

12/3/2009 15:32! 

12/3/2009 15:32; 

12/3/2009 15:32; 

12/3/2009 15:32; 

12/3/2009 15:331 

12/3/2009 15:33; 

„_ 

12/3/2009 15:33! 

12/3/2009 15:33; 

12/3/2009 15:34; 

12/3/2009 15:34! 

12/3/2009 15:34; 

12/3/2009 15:34; 

12/3/2009 15:35-

12/3/2009 15:35; 

"12/3/2009 15:35!' 

12/3/2009 15:35 

12/3/2009 15:36; 

12/3/2009 15:36! 

3509.8; 

'3569.6! 

35662!" ' 3503.4! 

34986; 

'3493.8r 

'3489.1 ' 34868! 

3484.5 

348272 

34769; 

'3480.9J 

"34816 

3483.7; 

"3486.7!" 

34896; 

3492.5 

34964: 

34944j 

3493.6 

"3492:3!" 

'3461:3!" 

3495.2 

3499.T 

35061; 

3507.0 

"35665|' 

"35669! 

3565:4!"' 

'35666; 

ISSETT 

3511.6" 

'3514.4; 

3517:6; 

3526 47 

6523.3]' 

'352672;' 

3529.3; 

"3536I'" " 35366;' 

"35317] 

"35326; 

"35377j ' 35426;' 

""3547.9 

I553.6;'" 

"355l':4?:' 

'3549:6' 

"3548:3; 

4296.4 

4295.6 

4318.2 

'4313.5 

46O8.7 

4280.3 

42968 

'4296.5 

4294.2 

'429l':9 

'4316:2 

4291.4 

"429Z3 

4293.3 

"43162 

4|19.2 

"432271 

4301.3 

4304.2 

"4334.5 

4333.4 

433274 

4331.4 

4335:2 

433972 

4343.1 

43470 

4346.5 

"4368.5 

"4345.6 

4344.6 

43477 

4356.8 

"43540 

"4380.6 

4359.6 

4662.5 

""436574 

4366.4 

4369.'2 

43761 

'4347.2 

"43486 

"4353.1 

"43562 

•43663 

4368.4 

"'434374 

'434i:8 

4340.2 

VES018424 
Unit3 Run 3 

Time'.Stamp LiquidWgtHRT^ TotWgtHRT: 

12/3/2009 15:36; 3546.7! 4338.6 

12/3/2009 15:36; 354278r"" '"43347 8 

12/3/2009 15:37: 3539.6' 433176 

12/3/2009 15:37, 3535.2! ' ''"4326.4 

12/3/2009 15:37' 3531.3 4322.5 

12/3/2009 15:37: 35297! 4326.9 

"12/3/2009 15:38": 3528.1: 4319.2 

12/3/2009 15:38, 3526.41 

" 4340.2 

12/3/2009 15:38 3524.8: 4338.6 

12/3/2009 15:38: 35272] 4318.3' 

12/3/2009 15:39: ""352975! 4320.7 

12/3/2009 15:39; 4323.0 

12/3/2009 15:39! 353471! "434872 

12/3/2009 15:39! 3533.8 "4347.8 

12/3/2009 15:40! 3533.47 ""43474 

12/3/2009 15:40; 3533.0! "432475 

12/3/2009 15:40! 3532.6; """'"'" "4346.9 

12/3/2009 15:40; 3530.6! 4344.9 

12/3/2009 15:41; """352874] 4342.7 

12/3/200915:41! 3526. l! 4340.5 

12/3/2009 15:41! 3523.9 4358.4 

12/3/2009 15:41: 3524.1! "' 4335.7 

12/3/2009 15:42: 3524.3; 4335.9 

12/3/2009 15:42: 3524:5; 4336.1 

12/3/2009 15:42; 3524.8; 4359.4 

12/3/200915:42;" 3523:6; "4357.6 

12/3/2009 15:43; 3521.2! 4355.8 

12/3/2009 15:43! 735i9. 3 " 4330.6 

12/3/200915:43; 351757 * 4328.8 

12/3/2009 15:43; 3513.9' 4348.7 

12/3/2009 15:44! 351*6.3 4345.1 

12/3/200915:44; 35067*7 ' "' 4319.2 

12/3/2009 15:44; '350371!"' 4315.6 

12/3/200915:44! 350576; "4340.8 

12/3/2009 15:45; """" 350679'""" 434278 

12/3/2009 15:45; 3508.8 4321.2 

12/3/200915:45! "351076; 4323.0 

12/3/2009 15:45! 3507.2! "'''""434277 

12/3/2009 15:46! "350377! 4339.3 

12/3/2009 15:46; 3566.3: 4312.3 

12/3/2009 15:46; 3496.8] ""4308.8 

12/3/2009 15:46; 3497.3; 436973 

12/3/200915:47! '""'3497.87"" 4332.3 

12/3/2009 15:47! 3*498.3] 4332.8 

12/3/2009 15:47; 3498.8: 4333.2 

12/3/2009 15:47! "349678 '* "433173 

12/3/2009 15:48; 349478! '" " 4352.2 

12/3/2009 15:48! 349278; 4350.2 

12/3/2009 15:48; 349678 "" 4348.2 

12/3/2009 15:48! ""348873! 4345.7 
Uni

t a Run 3 

TimeStamp 'LiquidWgtHRT TotWgtHRT 

12/3/2009 15:49 

12/3/2009 15:49' 

"12/3/200915:49!" 

12/3/2009 15:49] 

12/3/200915:50' 

12/3/2009 15:50; 

12/3/2009 15:50! 

12/3/2009 15:50; 

12/3/2009 15:51; 

12/3/2009 15"51i 

'12/3/2009 15:51"! 

12/3/2009 15:51 

"12/3/2009 15:52 

"12/3/2009 15:52; 

12/3/2009 15:52! 

12/3/2009 15:52i 

'12/3/2009 15:53-

12/3/2009 15:53; 

12/3/2009 15:53 

12/3/2009 15:53! 

12/3/2009 15:54; 

12/3/2009 15:54! 

12/3/2009 15:54 

12/3/2009 15:54; 

"12/3/2009 15:55? 

12/3/2009 15:55: 

12/3/2009 15:55; 

"12/3/2009 15":55! 

12/3/2009 15:56! 

12/3/2009 15:56; 

12/3/2009 15:56] 

12/3/2009 15:56 

12/3/2009 15:57: 

12/3/200915:57; 

12/3/200915:57; 

12/3/2009 15:57! 

12/3/2009 15:58, 

12/3/2009 15:58 

"12/3/2009 15:58] 

12/3/2009 15:58; 

"12/3/2009 15:59] 

12/3/2009 15:59; 

12/3/200915:59;' 

"12/3/2009 15:59]' 

12/3/2009 16:00? 

12/3/2009 16:00; 

12/3/200916:00; 

12/3/2009 16:00; 

12/3/200916:01! 

12/3/2009 16:01!" 

3485.8! 

3483.3. 

3480.7 

3488?!l! 

'3495:5!' 

"3562:9] 

35166? 

4366.1 

4363.5 

436176 

"436874 

'437 p 

"4463.1 

4410.5 

3515.3; 

3526.2 

'35251]' 

"35361] 

'3539:4] 

'65468! 

'3556:2f 

'6567.6| 

"356676'!" 

""3564.51 

3562.9; 

356i:3j" 

"3561.7;" 

3562.1: 

"356275[" 

"3562.9

T

" 

356375] 

3564:2] 

3565.6; 

36667 

35667] 

3565.6 

'35667?" 

3565.7! 

3565.4" 

"356627' 

"3564.9!" 

35646 

'3561.9]" 

"3559.2!" 

"355674T 

3553.7:"' 

3553797 

"355472!"' 

"3^474!" 

35 5477!" 

"355672! 

3557.7; 

"3559.2]' 

356677!" 

3557.4! 

"355472; 

355176! 

4415.5 

4420.4 

'4446I 

"445376 

"446274 

44716 

4461.2 

"4496.5 

4489.0 

'4487.4 

4509.4 

4507.8 

4'566.2 

"'45666 

"450974 

""4509.8 

"4616.4 

'4'5'llTl 

451178 

4536.3 

4512.7 

'451277 

"451277 

453876 

453874 

4538.1 

"451476 

''451476 

'453576 

"4533.1 

'453674 

452776 

4528.9 

"45291 

"4529.4 

4529.6 

~455574 

"4556.9 

'45366 45 3675 

"'465676 

"456674 

'46662 

VES018426 
Unit 3 Run 3 j 

:\ff Time Stamp, LiquidWgtHRT TotWgtHRT 

12/3/2009 16:01; 3549.1! 4548.4 

12/3/2009 16:011 3552.5 4551.8 

12/3/2009 16:02; 3556.3! 4566.5 

12/3/2009 16:02] 356a2! '4584.4 

12/3/2009 16:02; 3564.1 "4566 4 

12/3/2009 16:02 '3575.6 4599:8 

12/3/2009 16:03; 3587.1 ""4611 3 

12/3/2009 16:03! 3598.5 4624.4 

12/3/2009 16:03; 3610.6" 4636.6 

12/3/2009 16:03: 3621.0 4646.8 

12/3/2009 16:04! 3631.5 4657.3 

12/3/2009 16:04! "36417' 46676 

12/3/2009 16:04: 36517! 4677.5 

12/3/2009 16:04; 3660.1! 4710.5 

12/3/2009 16:05 ' 36666:' 4718.6 

12/3/2009 16:05; 3676.3! 4726.6 

12/3/2009 16:05! 3684.6 4734.4 

12/3/2009 16:05! 3691.5! 4719.3 

12/3/2009 16:06! 3698.9, 4750.6 

12/3/2009 16:065 3766.2! 4757.9 

12/3/2009 16:06! '"371'3.4 ; 4765.1 

12/3/2009 16:06; 3720.9; '4772:6 

12/3/2009 16:07! 37264 4780.1 

12/3/2009 16:07'; 3736.0! 4787.7 

12/3/2009 16:07; 3743.5! 4819.1 

12/3/2009 16:07! "37466 4824.1 

12/3/2009 16:08! '' 3753.7: 4829.3 

12/3/2009 16:08; 37569; 4834.6 

12/3/2009 16:08! 3764.2, 4816.5 

12/3/2009 16:08! ""37646! 4816.3 

12/3/2009 16:09; 37666:' 4816l 

12/3/2009 16:09: 37666 4839.2 

12/3/2009 16:09! "3766 6 4839.0 

12/3/2009 16:09! 3763.8; 4839.5 

12/3/2009 16:10; 6'764:6; ""4840:6 

12/3/2009 16:10! '6764.6 4840.5 

12/3/2009 16:10; "' "3765.3; 4840.9 

12/3/200916:10: 3765.6; 4846.7 

12/3/200916:11; "" 3764.8! 4864.6 

12/3/200916:11: 3764.6' 4864.2 

12/3/2009 16:11; 3764.6! 4864.6 

12/3/2009 16:11; 3768.3! 4868.0 

12/3/2009 16:12! 3772:3: ""4872. 6 

12/3/2009 16:12; "37763 ! 4876.6 

12/3/2009 16:12; 3780.4; 

12/3/2009 16:12! "

v

377"62f 4886.4 

12/3/2009 16:13! 3778.6 '4879.2 

12/3/2009 16:13! 3776.8, 4878.0 

12/3/200916:13! 37756! " 48766 

12/3/2009 16:13; 3776.2!' ""4854.6 
Unit3 Run 3 

.Timers tamp LiquidWgtHRT TotWgtHRT t? 

12/3/2009 16:14 

12/3/2009 16:14; 

12/3/2009 16:14 

"l2/3/2009"l6:14!" 

12/3/2009"l"6:15-" 

12/3/2009 16:15;" 

12/3/2009 16:151 

12/3/200916:15"; 

12/3/2009 16:16 

12/3/2009"l6Tl6; 

12/3/2009 16:16: 

12/3/2009 16:16 

12/3/2009 16:17, 

12/3/2009 16:17f 

"12/3/2009" 16:17; 

12/3/2009 16:17:'" 

12/3/2009 16:18! 

12/3/2009 16:18 

"12/3/2009 16:18] 

"12/372009 16:18; 

12/3/2009 16:19; 

12/3/2009 16:19; 

"12/3/2009 16:19] 

12/3/2009 16:19! 

"12/3/2009 16:20"! 

"12/3/2009 16:20: 

12/3/2009 16:20] 

12/3/2009 16:20; 

12/3/2009 16:21! 

12/3/2009 16:21! 

12/3/2009 16:21* 

12/3/2009 16:21; 

"12/3/2009 "16:22"; 

"i2/3/2009"l6:22] 

12/3/2009 16:22: 

12/3/2009' 16:22] 

3776.8 

" 377774] 

377870; 

37744! 

'377678] 

""376772! 

]376376; 

37 6379: 

'3764.3; 

'37647; 

3765.6] 

3771.5! 

3778.6: 

3784.5! 

379679; 

'378877! 

378674; 

"378472; 

3781.9 

3783.9' 

3785.8] 

"3787.8; 

3789.7 

378979] 

3790. ij 

Maximum 

3790.3; 

' 3796.5 ' 

379'6.9!' 

37913] 

37917]" 

"379272; 

3792.1; 

3792.0; 

3792.0; 

"737919! 

3790.6! 

'"3796.8"] 

4855.2 

485518 

488673 

"48 5378 

485071 

"484675 

"484279 

4820772 

'4826.6 

4843.3 

"484377 

485672 

"483372 

483977 

484671 

484379 

"481 879 

484672 

'4837.9 

4839.9 

4818.0 

4819.9 

482179 

482271 

"484676 

'4823.3 

'482374 

"4823.9 

48243 

480271 

4802.6 

4802.5 

4802.4 

" 4778.8 

"477877 

4777.4 

4886.4 

VES018428 
I. 

SPIK E PREPARATIO N LO G SHEETS 

VES018429 
No, SG/09-03-102 Date MAR 17, 2009 

PRODUCT 

FORM 

CQtQR 

' i * 

ODO R 

TES T CERTIFICAT E 

(CERTIFICAT E O F ANALYSIS ) 

: HEXACHLOROETHANE 

: WHITE, CRYSTALLINE POWDER 

(FREE-FLOWING MATERIAL) . 

; SNOW-WHITE 

: CAMPHOR-LIKE 

(lj PURITY (% BY GLC) 

$ MELTING POINT 

,I3)';MOISTURE(%WT. ) 

{4)ASH(%WT.) 

(5) ;^REE CHLORINE 

(6) .WATER SOLUBLE 

pHLQRlDE j(%NaCI) 

(7) GRADING 

99.9% 

186 °C 

0.011% . 

0.09% ; • 

NIL 

0.016% 

-18 +15,0 Mesh BSS 

VES018430 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 11 -SM "QCj 

Crew Personnel \oOL | Shift I . . 

' • Scale zeroed 

masm MHIH K IBiil l 1 BAG# " WBOBBM liiiiii i mmm 

1 6 .b 26 3 . 0 51 s.o 76 3 . 0 

2 3 . 0 27 3 - 0 52 3 . 0 77 3 . 0 

3 2>;o 28 • 3. 0 53 3 . 6 78 3 . 0 

• 4' 29 3 . 0 54 3 , 0 79 3 . 0 

5 3-0 30 3 . 0 55 3 . 0 80 3 . 0 

6 3-0 31 3 . 0 56 a o 81. 3 0 

7 3>B 32 3 . 0 57 . 3- 0 82 3.0. 

8 33 •3. 0 58 • 3 . 0 83 s . o 

9 3>Q • 34 3 - 0 59 3 . 0 84 

10 35 a . o 60 3 . 0 85 3 . 0 

11 3 ^ 36 3 . 0 61 3 , 0 86 3.0 

12 3 .0 37 3 . 0 62 3 . 6 87 3 . 0 

13 38 3 . 0 63 S .O 88 3.0 

14 3 .0 39 ' 3.0 64 3 . 0 89 3 . 0 

15 3 . o 40 3/3 65 3 . 0 90 3 0 

16 .41 3.0 66 3 0 91 .3.0 

' -17 42 3 , 0 67 3 . 0 92 3 - 0 

• 18 . 3 . 0 43 3 0 68 3 . 0 93 3 . 0 

19 3 . 0 44 3 ; o 69 3 . 0 94 3 . 0 

• 20 3 . 0 45 3 , 0 70 3 . 0 95 3 d 

21' ?>. 0 46 3 . 0 71 3 , 0 96 3 . 0 

. ' 22 3 . o 47 3 . 0 72 3 . 0 97 3-0 

23 3 . 0 48 3.<D. 73 • 3. 0 98 3-0 

24 ' 3 . o. 49 3 . 0 74' '3'.0 99 

25 3 . 0 50 3 0 75 3 . 0 100 3 . 0 

VES018431 
HEXACHLOROETHAN E SPIKE BAG S - Target Weight: 3.0 pounds Date )1 -Q 9 

Crew Personnel TOAtci c , ft,. PcoAV" , I) . SoMemmt r shift I 

• Scale zeroed TkS to<>. 

1! BBH H ran liHII I miBH i i==BAG.# = -null a „:.BA.G,# •> UNH H 

101 3.0 126 3.0 151 ' 3 0 . 176 3. a 

102 3,0 127 .3-0 152 3.0 . 177 3.o 

103 3.0 128 3.0 153 3.0 178 3<D 

104 3.0 129 3.0 154 a o 179 S.O 

105 ' 30 130 3.0 155 180 3 . C 

106 3.0. 131 30 156 3 0 181 3.0 

107 3.0 132 30 157 3.0 182 • 3-0 

108 3,0 133 3.0 158 3& 183 Z.O 

109 S . O 134 ' . 3.0 159 30) .184 '. a o 

110 3,0 135 3.0 160 3.0 185 30 

111 . 3-0 136 30 161 •*;0 186 30 

112 3.0 137 3.0 162 3.0 187 3-0 

113 3 . 0 138 30 163 3.0 188 30 

114 •3.0 139 •3,0 164 3.0 189 3.0 

115 3.0 140 3,0 165 3.b . 190 b.D 

. 116 3.0 141 30 166 3.0 191 3.0 

117 3.0 142 3.0 167 3.0- 192 3.0 

• 118 3.0 143 3;0 168' 3.0 •193 3-D 

119 3<0 144 3\0 169 3.0 194 3.0 

120 3 >0 . 145 3.0 170 .3.0 195 

121 ' 3.0 146 3 0 171 3.0 196 3.0 

122 • 3.0 147 3 0 172 3.0 197 3-0 

123 3D 148 3.0 173 3.0 198 3.0 

124 3.0" 149 " ' 3D 174 . 3.0 199 a o 

125 3-D 150. 30' • 175 ao 200 B . O 

VES018432 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date \l~3»MCrew Personnel TTGlidk . R.Pndrt/tXSoktomiec shift i 

S). ^ G A ^ Q V ^ _ . Scale zeroed AS " &^S -

Illililfl l§lli§l liiiiiii! lltlllfifi HiHlli 

201 3.0 226 3-D 251 3-C 276 3.0 

202 3-0 227 3.o ,252 3.o 277 3.0 

203 3.0 228 3-<o 253 3.0 278 3.o 

204 3.0 229 254 3.o 279 3.o 

205 ?>< 0 230 30 255 3 . o 280 3.o 

206 ,3.0 231 3.0 256 3.0 281 S . O 

207 c-30 232 3.0 257 ao 282 3.o 

. 208 3.0 233 3.0 258 6 . 0 283 3.o 

209 3.0 234 3.o 259 3.0 284 3.o 

210 3-D 235 S>o 260 3.o 285 3,o 

211 3o 236 3.o 261 286 3.o 

212 30 237 3.0 262 3.0 287 S.o 

213 3.0 238 3.0 263 288 3.o 

214 3 D 239 3.o 264 S.o 289 3.o 

215 3.0 240 3.o 265 3.0 . 290 3.o 

216 ao 241 S.o 266 3.0 291 3.^ 

217 3.0 242 3.0 267 3.0 292 3.o 

218 3.0 243 3.0 268 3.0 293 3tO 

219 3.0 244 30 269 3.0> 294 3.o 

220 3.0 245 270 3.<D 295 3.o 

221 3.o 246 3.0 271 3-0 296 3.o 

222 3.0 247 3. et 272 3.0 297 3.0 

223 2>.0 248 3.0 273 3.0 298 3 . o 

224 3(0 249 3. o 274 3.0 299 3.C 

225 3,0 250 3.0 275 3.o 300 3.o 

VES018433 
HEXACHLOROETHAN E SPIKE BAG S - Target Weight: 3.0 pounds Date U-^-Q ^ 

Crew Personnel " H QMC ; & Pc A D . SolvtpjyiW r Shift

 ] 

^V^Wtv n Scale zeroed 

[LBS B A G # BAG S WEIGHT (LBS) BAG # 

301 326 351 376 

302 327 A.o 352 3>o> 377 

303 328 353 378 

304 329 3-cs 354 3o> 379 do 

305 330 ao 355 380 

305 331 356 3-o 381 AO 

307 332 357 382 Ao 

308 333 3-0 358 383 

309 334 359 384 an 

310 335 eo 360 30 385 

311 cVO > 336 361 386 A - A 

312 337 362 387 S-O 

313 338 363 388 3-C> 

314 339 3 A 364 to 389 rSA 

315 30 340 365 3 r ) 390 A O 

316 8-0 341 366 Ad 391 A. A 

317 342 367 392 

318 ?>^> 343 368 393 

319 344 369 394 

320 345 3-0 370 395 

3-21 346 371 3-?) 396 

322 347 372 3o 397 

323 348 3-0 373 3-0 398 

324 349 374 399. 

325 P>C) 350 so 375 c>7) 400 

VES018434 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date WrBH-Q^ 

Crew Personnel \ . QioJc-, £. ftoAb ^'iA W shift i 

yv^ Scale zeroed 

Iiilii i iHiiiiii i 1 IlSlIf l •iiiiii i mmm 

l|BAG#i ' 

401 t , o 426 451 3.0 476 3.0 

402 3.o 427 3 - 0 452 3>-0 477 3<0 

403 3<o 428 453 3.0 478 3,0 

404 3 . 0 429 2 D 454 3-o 479 3.o 

405 3.0 430 3 - 0 455 3.o 480 B.o 

406 3.0 431 3 .O 456 481 3'.o 

407 432 3-0 457 3-D 482 3.o 

408 S^O 433 3.0 458 3.c> 483 

409 434 3.^ 459 3.o 484 

410 30 435 460 3-0 485 3-0 

411 3.o 436 3-0 461 3-0 486 3.0 

412 3.o 437 5.0 462 3.o 487 3.0 

413 3.(3 438 3o 463 - 3-0 488 3-o 

414 3.0 439 3.a 464 489 a.o 

415 3.o 440 3-o 465 S'.o 490 3 .O 

416 3 0 441 3.0 466 3 . o 491 3.0 

417 3.o 442 3-<0 467 3.0 492 3.o 

418 3-D 443 3-o 468 2>.D 493 a.o 

419 3>.£> 444 3.0 469 2>.D 494 3.0 

420 B.o 445 3 o 470 S.O 495 3.o 

421 3.£> 446 471 3.o 496 3.0 

422 3.o 447 3-^ 472 3.0 497 3.0 

423 3-0 448 3 . o 473 498 3.0 

424 B.O 449 3 . 0 474 3.0 499 3.0 

425 450 3 , D 475 3-D 500 3-0 

VES018435 
HEXAvCHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date //- £3-o9 

Crew Personnel l/iz/A/^SroM- / 'Sr>3d/k Shift Ztid 

Scale zeroed 

liiiiiii liiiiiii HUSH 1111IKI HHiiHI II HG * iiPllli 

501 3 ibs 526 3//>5 551 3/bS 576 3 /by 

502 3 U«S . 527 3fbs 552 3/hf 577 . 3 /b3 

503 3 \b5 528 3 /b5 553 3 ibs 578 3 /hi 

504 3 W 529 3/h<S 554 3/h$ 579 3/hS 

505 3 lb s 530 3(b5 555 3//is 580 3 Jhs 

506 3 \bs 531 3 /fe 556 3/b? 581 3 [hS 

507 3 \hS 532 557 3/b* 582 sib* 

508 3 \\>$ 533 Z/l5 558 3/hl 583 j./bs 

509 3 fb 5 534 3/65 559 3/hZ 584 

510 3 IW5 535 560 3/6S 585 3fb? 

511 536 3/b 5 561 3/As 586 2/bi 

512 3 ( bjs* 537 3/h$ 562 3/bi 587 3/bl 

513 3 \hs 538 3/h5 563 S/M 588 3 /bs 

514 5 )hs 539 3 //>? 564 3/Ai 589 3/bn 

515 5 !b 5 540 3//JS 565 3 /J><- 590 3 /bf 

516 3 \ k? 541 3/hs 566 3 591 

517 3 Ikj r 542 J/hs 567 3 /As 592 3/bf 

518 3 ^ 5 543 568 3 /Ss 593 3/h 

519 3 \hS 544 y/bs 569 J/As 594 3/6^ 

520 3 Ib 5 545 3/h5 570 3 /hs 595 *fbs 

521 3/b* 546 3/65 571 3 /b 596 3/6? 

522 3\hS 547 3/h5 572 3 /A 597 3 /bi 

523 3 /AS 548 3/hS 573 3 /b 598 J/h 

524 3 fbS 549 3/bf 574 J /b 599 

525 3 /_) 5 550 -3 to? 575 ? u 600 

VES018436 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date //-23'0<

j 

Crew Personnel //(//n?^ 5Tg/ o /BoB<zr£ shift ZAJOL 

Scale zeroed 

lilliiMIl! IIIIIII) 111 Sill!mmm ! 111! HI iiiiii i IllIlIII IliSffijjllsj 

601 3/h 626 3/h 651 3/b 676 3 //> 

602 3/6 627 3/h 652 3/b 677 3 lb 

603 3 ib 628 3/6 653 3/b 678 3/b 

604 3lh 629 3/6 654 3/b 679 3/6 

605 3/h 630 3/b 655 3/b 680 3/b 

606 3 lb 631 3/b 656 3/b 681 z/b 

607 3 lb 632 3/b 657 3/h 682 3/b 

608 3/b 633 3/b 658 31b 683 3/b 

609 yfb 634 3/b 659 3/h 684 lib 

610 3/h 635 3fb 660 3/b 685 3lb 

611 3/b 636 31b 661 3 lb 686 3/b 

612 3 )h 637 31b 662 3 lb 687 3/b 

613 3/b 638 31b 663 3/b 688 3/h 

614 3/b 639 3 lb 664 3(b 689 3/b 

615 •3/b 640 3/b 665 */k 690 3 fb 

616 SIS 641 dfh 666 3/h 691 Kb 

617 3/h 642 31b 667 J Ih 692 31$ 

618 3/A 643 3/h 668 ?)b 693 ?/b 

619 J / / 644 3 lb 669 3)b 694 3/b 

620 3 /b 645 3/b 670 3 16 695 3/b 

621 3)i 646 3 ih 671 Jib 696 *lh 

622 3 Ib 647 3(b 672 3/b 697 3 lb 

623 3 Ih 648 3/b 673 3/h 698 3/6 

624 3/b 649 ?/b 674 3//) 699 3 lb 

625 3/b 650 3/i 675 3/b 700 3/b 

VES018437 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date //-^3-<^'9 

Crew Personnel Lti/fti4im>A//J?O7?C >/t shift Zrj d 

Scale zeroed j/g"_5" 

iiiiiii! liiHII! imps 1SI1I1I1 WEIGHTli'liBS) Iiiiiii iiiiiii 

701 3 If) 726 3 lb 751 J/h 776 3(b 

702 3 lb 727 3)b 752 •3/b 111 3)j> 

703 3)h 728 3/b 753 3/b 778 3/6 

704 3)b 729 3ib 754 •jib 779 jr// 

705 3 Ih 730 3/b 755 lib 780 3/b 

706 3)b 731 3ib 756 3 lb 781 3/b 

707 3 lb 732 3 lb 757 ?ih 782 3/b 

708 3)b 733 3 ft? 758 3lb 783 3/b709 3 is 734 lib 759 3 lb 784 3/b 

710 735 3/b 760 3/b 785 3/b 

711 3 )b 736 761 3 fk 786 -3 1b 

712 ,?J h 737 31 h 762 3/b 787 3 lb 

713 3 \b 738 7 lb 763 3/h 788 3/h 

714 . 3\h 739 Jib 764 3 lb 789 31b 

715 3 )b 740 3 lb 765 31b 790 3(b 

716 7 i t 741 3 If) 766 31J? 791 3\b 

717 3 lb 742 ? Ih 767 3 lb 792 3)b 

718 3 )h 743 3fh 768 3ib 793 Vh 

719 3 Ih 744 3 lb 769 3/6 794 3\b 

720 3 lb 745 770 3/6 795 3\b 

721 3 \b 746 3 ib 771 3 lb 796 7 lb 

722 3 h 747 3\b 772 3 lb 797 3 IS 

723 3 lb 748 773 ?lb 798 3/b 

724 3 lb 749 J\b 774 3/b 799 3lb 

725 3 lb 750 -5 lb 775 Jib 800 3/b 

VES018438 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel shift J G T P 

Date 

Scale zeroed 

masm HMU M Iiiiiii HHU H BAG* WHO M Iiiiiii 

801 3 LBS 826 3

L

*5 851 876 3 

802 827 852 3 ^ 877 

803 3/# 828 853 878 3 AB- ? 

804 3l*S 829 3 L%5 854 3 > L ^ 879 3 i-B? 

805 , 830 3 or 855 3 t&s 880 3 U&3 

806 3-13$ 831 856 3 L&S 881 

807 832 % l&t 857 882 3 

808 3 IB S 833 858 , 3 883 3 PbS 

809 c 3135 834 , 3^>S 859 « 3 UE& 884 3 

810 835 , 860 . 3> i& f 885 3 LBS 

811 836 3 LP? 861 886 3 L&<^ 

812 837 , 862 3 i&s 887 . |3 

813 3 im 838 863 ^ ABS 888 , 3 ±43^* 

814 3L3? 839 3 u & 864 3 LBS 889 3 

815 840 865 890 "5'UBf 

816 3 u & 841 3 ^ 5 866 3L-B? 891 3/-B5 

817 3 842 ( 867 3 L&S 892 3 4 * 

818 843 3 ^ S 868 °> LB? 893 

819 J UBS 844 869 3 L $ ? 894 < 

820 845 870 895 

821 3

L

^ 1 846 , 871 896 

822 847 3 ^ 872 897 3 

823 848 „ 3 873 3 i-T>T 898 3 ^P5 " 

. 824 849 3 874 3 LB? 899 3 ^e_> 

825 3 850 3L?>$ 875 3 L%5 900 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel V.UhlANoHlr M , &£?0&?72( 

\A w/<vrzv / 

Date, 

Shift 

Scale zeroed 

III Iiiiii i II iillili i flSBlI I ii • H IIIIII I HiHiS i •iiii i flHHHH 

901 3 L&? 926 3 L&<y 951 3 976 ? LB? 

902 3 927 3 L&S 952 977 3 LB? 

903 < 3 Lg>? 928 3 u&? 953 3 L&S 978 3 >-*? 

904 < 3 L&f 929 3ab>5 954 979 3 LU? 

9Q5 . 3 930 SL&S 955 3 LBS 980 3 L&J 

906 3>i3S 931 3 L35 956 3 IBS 981 3 Lfi< 

907 3us^ 932 3 is* 957 3 LBS 982 3 LBS 

908 3>L&S 933 3 LhS 958 3 LbS 983 3 LBS 

909 3 LBS 934 3 i&s 959 3 L ^ 984 \8L%S 

910 , 3 935 3 LBS 960 3 L&5 985 3 Lp* 

911 936 3 LB S 961 3 L&S 986 3 LB* 

912 3 937 *> L&S 962 3 Ls>2 987 3 LBS 

913 3 LB S 938 3 LPS 963 3 LBf 988 , 3 13 f 

914 3 2-&.S 939 3 L&J 964 3L&* 989 3 LBS 

915 2>LBS 940 3 LBS 965 3i-BT 990 3 LBS 

916 3t-B5 941 . 3 966 3LB>* 991 3 LBS 

917 , 942 3L&5 967 3 LB< 992 

918 3 L&S 943 3 LB S 968 3 LBS 993 3 LBS 

919 3 944 969 994 3L&-

920 3i.B^ 945 3\j&s 970 995 3 LBS 

921 3 L-&5- 946 3 LBS 971 3LB? 996 3 LBS 

922 3 947 972 3 LB * 997 3 LBS 

923 3 ieo ? 948 973 3 Le>j> 998 3>L3S 

924 3 ;.b < 949 974 3^35 999 3 UBS 

925 3 /-H S 950 3 LBS- 975 3 LBS 1000 'hms 

VES018440 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date//-<SV7 Zsl 

Crew Personnel!). f4ALflyW/£H. S, bSZk£g* Shift /< T T> 

V / . W/IS£L\y ; Scale zeroed 

fill PHI ! iii iiiHSill i liiiiii i 1IIHI H i n i iiilii i 

1001 1026 . 3 LB< 1051 3 LB? 1076 3LB? 

1002 3 LUS 1027 < 1052 3 LB? 1077 3 UBS1003 - 3 LBS 1028 3j.B? 1053 3 LB? 1078 

s 

3 LB? 

1004 3>LBs 1029 3>U$>? 1054 3 LB? 1079 3 LB? 

1005 , 3 l&? 1030 3u&s 1055 . 3 is? 1080 3 LTZ? 

1006 . 3 A& S 1031 3LB< 1056 . 3 LB? 1081 3L&* 

1007 3 LBS 1032 3 L&S 1057 3 1082 3 LSS 

1008 3L$<? 1033 3L&S 1058 3 LBS 1083 3 LB* 

1009 3 L%S 1034 1059 3 m? 1084 3 Lf& 

1010 3 LR? 1035 3 LB 9 1060 3LB<5 1085 3 LB? 

1011 , 3L&S 1036 3 LBS 1061 3 A3 f 1086 ? LBS 

1012 3 L&S 1037 3 A£ < 1062 < 3 AEL * 1087 3 LbS 

1013 3u*>* 1038 3 LB? 1063 3 LB? 1088 3u&? 

1014 3 LB? 1039 3 LB? 1064 3 LB* 1089 • 3 UBS 

1015 3) LB? 1040 3 ABS 1065 3 LB? 1090 3 LB? 

1016 3LBS 1041 3 LB? 1066 ALBS 1091 3>L^S 

1017 , 3ks? 1042 3L&? 1067 3 IB? 1092 3 LB? 

1018 r 3 LBS 1043 3L&S 1068 3i~&s 1093 3 LB? 

1019 %L$f 1044 3 LB? 1069 3) LB? 1094 3 LBS1020 3 LB? 1045 ALBS 1070 3 LBS 1095 3 L&S 

1021 3LBS 1046 3LV? 1071 3<~B.S 1096 3 LB? 

1022 3L&? 1047 c?AB 5 1072 3 L-P<T 1097 3 LB? 

1023 SLB? 1048 3 UBS 1073 3 LBS 1098 3 LB? 

1024 3L%* 1049 3 1074 3 LP? 1099 3L&$ 

1025 3 LBS; 1050 3 LEi£ 1075 3

 L&s 1100 3 LBS 

VES018441 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 

Crew Personnel 3>t ; 5> ^>BCL<^P Shift Js>T P 

V - Scale zeroed Y^^ > 

IHllilli l iiiiii i IIIIII I I BsifPILBS ) WEIGHT <tBS) WEIGfjTl[LBs'j 

1101 3 LB* 1126 L LB* 1151 3 ABS 1176 3 LB-> 

1102 3 LQ>* 1127 t 3uzs 1152 3 L&S 1177 3 L&S 

1103 3 L&? 1128 3 LBS 1153 •3^B* 1178 3L-BS 

1104 3> LB 5 1129 3 LB S 1154 3LB* 1179 3 LB? 

1105 3 LBS 1130 3 Lte< 1155 3 LB* 1180 3 LB? 

1106 3i&s 1131 1156 3 LUS 1181 3LBS 

1107 3 LB* 1132 3 LB* 1157 3 L&S 1182 3LBS 

1108 3 LBS 1133 3 LBS 1158 A LBS 1183 2) LBS 

1109 3 J-B^ 1134 3L&* 1159 3in^ 1184 3 LB* 

1110 3 L&* 1135 3I~&* 1160 , ^LHS 1185 3LB* 

1111 3 LB* 1136 3 LB* 1161 , 3LBJS 1186 3L&? 

1112 

X 

- 3 LBS 1137 3LBS 1162 , ^Lp,* 1187 , 3 /-& s 

1113 3 LB* 1138 3 LB* 1163 , °>LB>* 1188 3LBS 

1114 3 LB? 1139 3 LBf 1164 3L&S 1189 3LBS 

1115 3 L&? 1140 3 LB* 1165 £>Lf?< 1190 ALK* 

1116 3 LP* 1141 3 LBS 1166 3 LBS 1191 3LB>* 

1117 3L&? 1142 3L.-P>* 1167 3 LBS 1192 3L$* 

1118 3 LB* 1143 3 LET 1168 3LBS 1193 3 LB? 

1119 <3J~B? 1144 3L&<? 1169 3>ue>s 1194 3i-B < 

1120 3>L35 1145 3 L&S 1170 3 VBK 1195 3LB?~ 

1121 3 L&S 1146 £L& * 1171 3 / 3 S 1196 3 L ^ 

1122 3) LB* 1147 3 LBS 1172 , ^LBS 1197 3 z -Z3 < 

1123 3L&* 1148 3 LBS 1173 3 LBS 1198 3LBS 

1124 3 LB* 1149 3LBS 1174 3LF& 1199 3LBS 

1125 3LBS 1150 3 LBS 1175 3z-B. s 1200 3*-BS 

VES018442 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date//'^.^ 7 "CJ^\ 

Crew Personnel .7), M/JtMA//£//j S. f Shift / W .P 

V> W/$&lX/ Scale zeroed VS^ 

BHfflWII mmm Iiiliii liiiiiii sun n ! iiiii lit liiiiiii 

1201 3 L&? 1226 , 4 LB* 1251 3 Lfr* 1276 3 LB* 

1202 , 1227 3 LB* 1252 3 Lp* 1277 3 LB*-

1203 3 LBS 1228 3 LB<? 1253 

/ 

i ^>LB7 1278 3 LBS1204 3 LBS 1229 3 L&* 1254 3 LBS 1279 3 LBS 

1205 , ^ LBS 1230 3 LB* 1255 3 LBS 1280 

V—* "" " 1 

3 LBS 

1206 , 3 1231 3LB? 1256 3 L&S 1281 3 LBS 

1207 3L&* 1232 3LR<- 1257 3 LBS 1282 3LB? 

1208 3 LBS 1233 3 LBJS 1258 3 LB* 1283 3 LBS 

1209 3L^5 1234 3LBT 1259 3 LBS 1284 3 LBS 

1210 SL&S 1235 3 LBr 1260 ALB* 1285 3 LBS 

1211 3 LBS 1236 3 LB* 1261 3 LBS 1286 3 LBS 

1212 3 LBS 1237 3L&? 1262 C3LBS 1287 3 LBS 

1213 3 LBS 1238 3L&* 1263 3LBS 1288 3 LBS 

1214 3 LBS 1239 3L$S 1264 3L&S 1289 3 LBS 

1215 3 LBS 1240 3 L£<r. 1265 -? LSS 1290 3>LB*r 

1216 3LP.* 1241 3 LB* 1266 3L&<? 1291 3 LB* 

1217 3 L ^ 1242 3LBS 1267 3 LB* 1292 3LP>S 

1218 3L13S 1243 &Lfo* , 1268 3 LB? 1293 3L&$ 

1219 3 LB* 1244, 3L&? 1269 3 LBS 1294 3L&$ 

1220 3 LBS 1245 < 3 LBS 1270 3LBS 1295 3LB<? 

1221 3l^K< 1246 3 LB* 1271 3 LB* 1296 3 Ln* 

1222 3*-8Z 1247 3L-&<T 1272 3 ISS 1297 3 LB* 

1223 3 LB? 1248 3LB* 1273 3 LBS 1298 3 L&* 

1224 3LRST 1249 3LRS 1274 3 LBs 1299 3 LB* 

1225 3LBS 1250 3 LBS 1275 3 LBS 1300 3 LB? 

VES018443 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel Shift / S T 13 

Scale zeroed 

mmmm iiiiii i IIHIB! Hilll l IIIIIII mmm mam iiiiii i 

1301 3 LB* 1326 , 3 LBS 1351 $ Lb* 1376 3 ABS 

1302 3 LB* 1327 3 LB f 1352 3 ms 1377 < 3 Lb? 

1303 3 L R « 5 1328 3 LBS 1353 3 LBS 1378 3 LB* 

1304 3 LBS 1329 3 LB* 1354 A LB* 1379 3 LBS 

1305 3z.B^ 1330 3 LB* 1355 3 L&S 1380 3 LBS 

1306 1331 3 LBS 1356 3 LBS 1381 3 LB* 

1307 1332 3 LBS 1357 3 LBS 1382 3 LBS 

1308 3 LBS 1333 3 LB* 1358 3 LBS 1383 3 LBS 

1309 3 LB? 1334 3 LBS 1359 3 LBS 1384 3LBS 

1310 3 1335 3 LBS 1360 3) LBS 1385 3LBS 

1311 ALBS 1336 3 LBS 1361 3 LBS 1386 3LBS 

1312 3 LBS 1337 3 Lb* 1362 3LB>* 1387 3 LB* 

1313 3 LBS 1338 ALBS 1363 1388 3L&S* 

1314 3 LB* 1339 3ms 1364 3LBS 1389 3J-&<

> 

1315 3 LBS 1340 3LB? 1365 3 LBS 1390 3 LBS 

1316 3 2-B? 1341 3 L&S 1366 3L9>S 1391 3L^S 

1317 3 LBS 1342 3>LBs 1367 3 LB* 1392 3LBS 

1318 3 LBS 1343 3 LBS 1368 3 LBS 1393 3L&S 

1319 3 LBS 1344 3 LB* 1369 3L$S 1394 3 LBS 

1320 <3LB< 1345 AlB? 1370 3L-R<S 1395 3 LBS 

1321 3 LBS 1346 3 L&* 1371 3)LPS 1396 3 LBS 

1322 3 LBS 1347 3 LB* 1372 3LB<; 1397 3LBS1323 3 LBS 1348 3 LBS 1373 3 LBS 1398 3LBS 

1324 3 LBS 1349 3 LB* 1374 3 LbS 1399 3 LBS 

1325 3 LBS 1350 3 LBS 1375 3 LBS 1400 3LB>^ 

VES018444 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 

Crew Personnel b< HPLAVdNfCL1 7 7 D#V^/> / Shift /gT T> 

V - WJS£~L y Scale zeroed V^^> 

lillMifl HiBSIl •mmm iilHlii Ittlllllll nisiii IIfflillfi!l iiilllli 

1401 1426 SAT?*- 1451 3 LBS 1476 3 LB*" 

1402 3 L&? 1427 3 LBS 1452 3 ivr 1477 3 LB? 

1403 3 LB* 1428 3 LB9 1453 3 L$SS> 1478 3) LBS 

1404 3 LR S 1429 3 LW> 1454 3 LB* 1479 3 LBS 

1405 3 LB? 1430 3 1455 • 3 Lt* 1480 .3 LBS 

1406 3 1431 3 L-frS 1456 3 LBS 1481 3 LBS 

1407 3 LB S 1432 3 L^>£ 1457 3 LBS 1482 3 LBS 

1408 3 LB S 1433 3 LBS 1458 3 LB* 1483 

1409 3 LB S 1434 3 LB? 1459 3 LB* 1484 r n LB? 

1410 3 L&S 1435 2> L&f 1460 3u>? 1485 3L-BV 

1411 3 IB? 1436 3 L3* 1461 3 L&s 1486 3LS? 

1412 1437 3 LV* 1462 33LBS 1487 3 Lbs 

1413 3 LB* 1438 3 LPS 1463 1488 QL&S 

1414 3 LB< 1439 J-PS 1464 3LBS 1489 3 LBJ 

1415 3 LB* 1440 3 LBS 1465 3 LB? 1490 3)LK* 

1416 3 LB* 1441 ^>LB< 1466 3LB* 1491 3 LB* 

1417 3>LB< 1442 3 LBS 1467 3 LB* 1492 3>LBG 

1418 3 L&S. 1443 3 LBS 1468 3 LB* 1493 3 VB< 

1419 ( 3 LBS 1444 3LB^ 1469 3 LB* 1494 3 LBS 

1420 < 3 LBS 1445 3L&? 1470 3 LB* 1495 3 LPS' 

1421 3 iss 1446 $LB5 1471 3 LBS 1496 3 LBS 

1422 3 LBS 1447 3 Lbr 1472 3 LBS 1497 3 LBS 

1423 3 LBS 1448 3 LPS 1473 3 LB* 1498 3 L&<f 

1424 3 L~$S 1449 3 LBS 1474 3 LBS 1499 3 L&r 

1425 3 L%<; 1450 3L&S 1475 3 LBS 1500 3 LBS 

VES018445 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 

Crew Personnel]), LfALA\/6f(/d/-/ ' J7 frO\/^jQ Shif f t J> 

V, \Nl<Z/L~LV/ . Scale zeroed V ^ r ^ 

i l l ii i III HHlH i IBIIi wiilfliii i iiiiiii i WEIGHT <LBS, ,\ BAG# , miiii m 

1501 1526 3 Lk* 1551 3 LJ!>* 1576 3 iLpS 

1502 3 IBS 1527 3 LB.S 1552 3 Ln* 1577 3 LBS 

1503 3 LBS 1528 3 LBS 1553 1578 3 LBS 

1504 « 3 LBS 1529 . 3LBS 1554 3 LBS 1579 3LB<S 

1505 3 L&S 1530 3>LB& 1555 c 3 LB* 1580 , 3 LBS 

1506 , 3 LBS 1531 3 LBS 1556 3 LBS 1581 3L&S 

1507 « 3 LPS 1532 3)Lp< 1557 3&s 1582 %L&? 

1508 3 LBS- 1533 , 3 LBS 1558 3L?S 1583 ^L&S 

1509 1534 < 3 L B ? 1559 3LH>? 1584 3L2>£ 

1510 3) LBS 1535 3L%S 1560 , 3 LBS 1585 , °>L^S 

1511 < 3 LBS 1536 3frs •fgsi- 3LB* 1586 3 IBS 

1512 1537 3>LB>S 1562 3*>LB* 1587 3 Lhr 

1513 3 LBS 1538 3) LBS '1563 3)v&< 1588 3 LBS1514 3 LBS 1539 3)LBS 1564 3jL&r 1589 3 LfeS 

1515 3 m 1540 3LBS 1565 3^<r 1590 3 Uses 

1516 3 LIBS 1541 3>L&$ 1566 3 LBS 1591 c3 LBS" 

1517 3 LBS 1542 3>L&S 1567 3>VBT 1592 

1518 3 LBS 1543 < 3 LB< 1568 3) LP,? 1593 , 3^s1519 3) L&< 1544 ' , 3 LMS 1569 3ws 1594 •3 LBS 

1520 3 IBS 1545 3 LB? 1570 3 LBS 1595 3)L&r 

1521 1 3 LBS 1546 3 LB>? 1571 SUBS 1596 , 3 ABT 

1522 3 IBS 1547 3 m 1572 3 LGrr 1597 Sh ' 

3LBS- 1523 3 LB>S 1548 « 3 IBS - 1573 3 m 1598 3LB9 

1524 3 LB* 1549 c 1574 3 LBS 1599 3 LBS 

1525 3 LVS 1550 3 m s 1575 3m<> 1600 . 3 LBS3 

VES018446 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date //'t^/p-P^ 

Crew Personnel D , (4ALA VfrN.fcL' f 77 .fe^t/^T^ / Shift fef 3> 

V. \AJ(S£L\/ Scale zeroed _V£^> 

lUHU l HIHI!! IIIIIII! IffflUllI illlll l HHilHI IIHIii 

1601 3 LBS 1626 3> LRS 1651 3 L&f 1676 3 / & r 

1602 c. 3>L®s 1627 , 3 LBS 1652 3 LB* 1677 3 LBS 

1603 3LRS 1628 £LB<T 1653 3 LBS 1678 3 LBS 

1604 3 LB* 1629 3 LBS- 1654 3 /-fer 1679 3 LBf 

1605 3 LBS 1630 3 Llss 1655 3 LB* 1680 , 3LBS160S 3L&<5 1631 3 LB<T 1656 3 LT2< 1681 3 Lns1607 3 LB? 1632 3 LZS 1657 , 3 LBS 1682 3>LB<T 

1608 '3 Use 1633 

e^"—•— — 

3 LBS 1658 3 LBS 1683 , 3A73<T 

1609 3 LB? 1634 3 LB< 1659 3 IBS 1684 3 LBS 

1610 3 LPS 1635 3L&<? 1660 3 LBS 1685 <^LB< 

1611 3LP>< 1636 3i$r 1661 3 LBS 1686 3LBS 

1612 3 LpS 1637 3 LIST 1662 3i&* 1687 3LB<Z 

1613 , 3 UBS 1638 3 LBS 1663 3L&<T 1688 3m< 

1614 3 LBS 1639 3 LBS 1664 3 LBS 1689 3 LBS 

1515 < 3 LB< 1640 3L&<T 1665 3LP,C 1690 3 W 

1516 3 LB* 1641 3L&* 1666 3LR< 1691 3L&S 

1617 3LP>* 1642 1667 3LP< 1692 3LB* 

1818 3 LBS 1643 3 LBS 1668 3 L&? 1693 

—-* s 3?L&sr 

1519 , 3 Libs 1644 

v '

 r r S— 

&L&S 1669 3 LBS 1694 ^Lfer 

1620 3 LBS 1645 1670 3 uzr 1695 SLTZS1821 3 LBS 1646 3L$S 1671 3L-BS 1696 3>L9f 

1S22 3 LBS 1647 3L^< 1672 3LRS 1697 3 LBS 

1S23 3 LBS 1648 3 LBS 1673 3LB>S 1698 3LTSS1S24 3 LQf 1649 3 L&r 1674 3&f 1699 3 lis 

1525 3 LBS 1650 3 LBS 1675 3L&? 1700 3^ 

VES018447 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew PersonnelVtUMAVM/tCtt, T, t&Y&R, 

y wissiy 

Date 

Shift /-sr- J7> 

Scale ^£2 zeroed 

iiiiiii liiiiiii lilHllII mills lllill.ll! WEIGHT (LBS) WEIGHT [iMs|j 

1701 3> LB* 1726 3 LB* 1751 3 LB* 1776 , 3>LU* 

1702 3 LU* 1727 3LB* 1752 3 LBS mi 3) LBS 

1703 3 U=i<r 1728 . 3 LBS 1753 3 LBS \118 3)LBsr 

1704 3 L&f 1729 3 LB* 1754 3 LBS 1779 3^is1705 3 LB,-? 1730 3 LB* 1755 3LB>? 1780 ( 3 LBT 

1706 3 1731 3 LBS 1756 3LB>S 

V 

1781 , 3tg< 

1707 2? 1732 3LDS 1757 3 LBS 1782 . 3L&*r 

1708 3 L&S 1733 3 LBS 1758 3 LBS 1783 3LBS 

1709 3 LPS 1734 3vBS 1759 . 3>L&S 1784 3 LBS 

1710 3 L & r * 1735 3>L&? • 1760 3)LL>< 1785 , 3 LBS 

1711 . 3 LB* 1736 . 3L&S 1761 , 

r—^> v* / 3 LBS 1786 , 3LB<r 

1712 3 LB* 1737 3LB>* 1762 c 3LBS 1787 3LZS 

1713 3 LBS 1738 3LB>5 1763 3 LBS 1788 , 3LM1714 3LV& 1739 3L&>S 1764 , 3i&s 1789 3LB*~ 

1715 3\®p 1740 3LBS 1765 3L&<T 1790 , 3LB>* 

1716 3 Ubc 1741 3L&* 1766 , 1791 3LBS 

1717 3 LBS 1742 3LBJ? 1767 3 LRs 1792 , 3 URS 

1718 3 LP* 1743 3L&<; 1768 %LBS 1793 3>L&< 

1719 3 LB* 1744 3 LBS 1769 , 3 LRS 1794 , 

1720 3 Lg*-1745 3 y&s 1770 3 LBS* 1795 3u^ 

1721 

3 LBS 

1746 3 LBS 1771 « 3 AS T 1796 i 3L&S* 

1722 3 LBf 1747 3 LBS 1772 3)L£S 1797 c ^LBS1723 3 L&* 1748 °)1J^S 1773 3 LBS 1798 ^3LB< 

1724 3 LB* 1749 3 LBS 1774 3 LBS 1799 3Lhr 

1725 3LB$ 1750 . 3LBS 1775 3i$? 1800 

VES018448 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

— - Personnel X>^AJ AV^N^J/, V XfrVtfg, 

Y wts&Ly 

Crew 

Date H'M'Cfl 

Shift l*srr T> 

Scale zeroed 

DRBHH IIIIIII lliiiill i mni i IIIIIII H U H ii! SiiSIiiiiii 

1801 3 LBS 1826- , *3LB* 1851 L 3> L&? 1876 3L%* 

1802 3 LBS 1827 / 3ips» 1852 < 3 LTzr 1877 3 LBS 

1803 3 AB < 1828 ( 3ip* 1853 1878 3 L&r 

1804 . 1829 3LB*- , 1854 C3LJ3<T 1879 3 LBS 

1805 3i.pr 1830 3Lsr 1855 , 3 LBS 1880 3 LB<r 

1806 3>JLBS 1831 3LB< 1856 3LB<T 1881 3>L&* 

1807 3 LB* 1832 3tt>? 1857 3 LBS 1882 3 L&S 

1808 3is<r 1833 3LBS 1858 3 L&S- 1883 3 LpS 

1809 3L&T 1834 3 LBS' 1859 , 3/-ps 1884 3 LBS 

1810 3>LU<T 1835 , 3)L&<r 1860 3 ms 1885 3 LBS 

1811 , 3L&* 1836 < 3 ms 1861 3 LBS 1886 3 u&r 

1812 r 3/-B- f 1837 \ 3 LBS 1862 .^LfrS 1887 P>Lp>sr 

1813 « 3LB* 1838 3LB^ 1863 3 LBS 1888 3L2*T 

1814 3L&?~ 1839 3L®S 1864 3 LBS 1889 3)L&* 

1815 3L&* 1840 3L3* 1865 3LPS 1890 3 LB* 

1816 < "3 Lte<r 1841 3 LBS 1866 ^L&S 1891 3LB<T 

1817 e - 3 LB* 1842 3LBS 1867 3tes 1892 3LBS* 

1818 3L&<T 1843 3 LB* 1868 3LB< 1893 A %LB< 

1819 3 LBr 1844 , %LB< 1869 3LBS 1894 3 LB,*-

1820 3 LBS 1845 i 3 LBS 1870 3^s 1895 . 3 LBS 

1821 1846 <3/£ < 1871 3LT5<r 1896 ,3LBS 

1822 3L£K 1847 3L&< 1872 3LB,T 1897 3 LB? 

1823 3 izs 1848 3I%< 1873 3 LBS 1898 3L&<T 

1824 1849 a ^ 

^ DLB* 1874 3LB<z, 1899 3LB<T 

1825 3\4& 1850 < 3 Lps 1875 3L&* 1900 3LB><: 

VES01844 9 
{V 

HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personneip ^A/./\ , T7 t^V^f 

Date //' g&~&? 

Shift 

Scale zeroed 

MM " BAG S 'BHtflL 

ii 

iii i iMiiiii 11111111 iiiiliBl iilllli 

1901 1 L%* 1926 1951 3 L&* 1976 3^,f 

1902 

1903 

1904 

1905 

1906 

1907 

1908 

1909 

1910 

1911 

1912 

1913 

1914 

1915 

1916 

1917 

1918 

1919 

1920 

1921 

1922 

1923 

1924 

1925 

3 Ly>S 1927 

LBS 

LBS_ 

3 ABS 

3 & * 

3 LBS 

3wr 

3 LBS 

,3L&>S 3 

\ 3 

L B S 

LBS_ 

LBS 

3L&S 

3d, 

3w 

3^s 

3*w 

°)<LBS 

LBS 

3 <LBS 

LBS 

3 LBS 

1928 

1929 

1930 

1931 

1932 

1933 

1934 

1935 

1936 

1937 

1938 

1939 

1940 

1941 

1942 

1943 

1944 

1945 

1946 

1947 

1948 

1949 

1950 

3 

2 

L--&* 

L&<? 

3>L&>«> 

3^ 

3? LBS 

3LV>S? 

•3LB$ 

3L&S 

3LZ>$ 

3 

3^s 

3LB>S 

3LBS 

3^BS 

3^BS 

3LR$ 

3

LBS 

3te<; 

L&s_ 

1952 

1953 

1954 

1955 

1956 

1957 

1958 

1959 

1960 

1961 

1962 

1963 

1964 

1965 

1966 

1967 

1968 

1969 

1970 

1971 

1972 

1973 

1974 

1975 

<3l&r 

3 ^ - 5 

3LB>S 

3 LBS 

3 LB* 

3>L9S 

3m< 

3 LP,* 

3)U&? 

QLBS3^ 

3L&S 

3 LBS 

13 LBS 

3LBS 

3 LBS 

3>LW 

3 LBS 

3 LBS 

\3L&S 

1977 

1978 

1979 

1980 

1981 

1982 

1983 

1984 

1985 

1986 

1987 

1988 

1989 

1990 

1991 

1992 

1993 

1994 

1995 

1996 

1997 

1998 

1999 

2000 

3 LBS 

3 LBS 

°>L&S 

3A&5 

3LB<; 

3L&S> 

3 LBS 

LUX 

3m<; 

3L& & 

3 L& S 

3?L&<? 

3L& -

3 LBS 

3LBS 

3 LBS 

3>L&? 

3LBS 

3L&r 

3LBS 

3LB^\ 

VES018450 
TEST DATE : l a A /c q 

TES T UNIT: {Jo, 3, 

TEST STAR T TIME: ^'.OO^M S (bNfc-tA^O 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver* Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

LltAfc-CiAT <, 

a • 

57 

a 

S i ' 

3t 

ao 

p. 

VES018451 
TEST DATE: \^/\/0°i 

TEST UNIT: 1*3 

TEST STAR T TIME: \\:% m fKl /C I K V 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

S7 JS-Tj&b 3 U 9 0 

3 13 

3 91 ?& 

ess <&> Il 

3 1 0 

3 % 81 -ffcST 

> I S 

> 

Ss 3 15 

3 I V J 

2 * 3 1 1 

3 13 

Ss 3 \c% 

• j> 

3 bo 11

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~> 

j> 6 1 K1& • 

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-> j» 5 0 

3 

3 ss 

-T7 3 HI 

> 

3 41 &i 

3 So 

3. % J> S 3 

3 IOO 3 3g 

3 3 3W S O •-

3 %1 "?> 41 -

VES018452 
TEST DATE: 1*2/1 /C ^ 

TEST UNIT: ^ 3 

TEST STAR T TIME: \ ^ 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3 3&40a b a 

3 3,1 an 

3 3>4 

3 H o ® ^ 

•7 

j> 35 f^4 

~> 

.> 3 3 ^4 

3 5Hr ^ 4 

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3 11 a w ^4-

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—? 

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3 at 1 14 

3 13 4 511 

.3 H Ir 4 

3 s 4 

3 i 5 ^ I 

4 a i 3 

3 

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K 4- ^i4 

1 1 3 4 

3 3QO 4 

a i l 

4 

4 ail o 

a -

4 

4 ^ 

4 

4 A 3 

i 

• 4 aq+ 

i. 4 

VES018453 
TEST DATE: P/ < /<fl 

TEST UNIT: ~% 3 

TEST STAR T TIME: M F 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver* Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

IW.30 

4 3 1 a <34& 

4 

W8,so 

4 4 

H M l 4 

4 

H H 

LL o s l 4 ass 

4 4 

4 cX 

3R3 r if 

4 

4 

if 

it 

4 ^ 4 

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4- as* 

4 

4 

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s & 4 */ 2(7 

4 V 

4 y 

4 

M 

q lit 

H 

H 

H V# Y 

^ 7 ^ 7 ^ 

VES018454 
TEST DATE: \^/ \ /O ^ 

TEST UNIT: # 3 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

lbs.) 

Hex 

Spike (3.0 

Ibs.) 

1 23/ . 

V 

H 23o H 

H 

</ m 

a l ^ 4 

Li- A l l $ 0 

s u b X7g 

317 

3W1 

31b 

Sl^ i 

3 0 \ <t 37a 

^ 0 1 3$3 

, Y H r 3 W 

H 

H O O 

( 

3<H > 

3 ? 5 

? V 

3 < H 
TEST DATE : iS^/Cf t 

TEST UNIT: # 3 

TEST STAR T TIME: SO UMfc-UT 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3S-3H4b a 

. a a 

> 

V 

Si 

SL 

S^ 

Ss 

:x 

!>• 

-> 

~\ 

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VES018456 
TES T DATE: 

TEST UNIT: * "3> 

TEST START TIME: iO' CiS» V\vA/tu 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

lbs.) 

Hex 

Spike (3.0 

Ibs.) 

< ^ J 3 1 5 3WV> 

% 

s 

3v>a ZSh 

.sx . 3 T f S I I 

3 ^ 3 

. 3U5> 3 W 0 

3 W \ 

3 S 7 3 S $ 

i s a 

3 5 ^ 3SW 

3 5 5 

3% 341 

f H & 3 ^ 3 

.Si H 3 3 ^ 

3 4 0 3 5 i 

3 4 ^ 

3 4 V 3 ^3 

3 4 ^ 

S x 3 3 1 

3 3 5 3 3 ^ 

p 3 3 ^ 

^ 3 0 33i X 

3 ^ 

f§; 3

:

* 5 

ft 3 a 3 

S? 3*2 i 

J> 3VH 3 n -

VES018457 
TEST DATE: p/^/C' l 

TEST UNIT: * J 

TEST START TIME: f ;x £>^j r 

Receiver # Charge* Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3 

ns,ao 

3 . I I I 

310 3 V 3 

-

314 3oi a 

3\3 CP* 

wo. a 

•2. 

_ H4 <"X • 

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F i b 3. 3S3^W 

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\ m IS* 4 IWbno 4 IU 

3 n4 MSIS3 n a \\P[-

mz-

\sn 

1*5 • 

15V 

HO Ji 4 111 

VES018458 
TEST DATE : \>l>tQ°l 

TEST UNIT: 3 

TEST STAR T TIME: 1^ -3,0 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

Spike (3.C 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

150 ' W p 

/ 

h\ 

V 

IA. / t o 

\*% 

\ 154 

m 

1 3 S 

in 

H 3 

13b 1 0 \ 

i S| lib 

K8- 114 

\si 163 

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| 

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/ !T3-

m U S 

in 

I4| . 105 

im 

134 • 115 

1 3 3 

13^ ' 

L 

( 3 \ ' 

s • 

VES018459 
TES T DATE: ^/'^M 

TES T UNIT: tt ~3 

TES T STAR T TIME: 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) • 

Hex 

Spike (3.0 

Ibs.) 

Receiver* Charge # Hex 

Spike (3.0 

ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3S^0<& 

.4 H. 11? 

icn 114 

i<# • - m 

1 713 

1b4 • , • 

115 

i<n 1 ^ 

11 V 

1^4 

H 4 its 

7 WO 

1W 7*50 

184' 9 s U S 

* 

1^0 15\ 

l^Bv 154 

1<S3 15^ 

1S5 -

1 5 7 

T l | an a 15% 

" T O 131 

11 ^ 7H5 

m 155 

710 

/ 

iu - - * 1 m 

7 ^ 

4 11C | * 1% 3 $ ? 

'A 

VES018460 
TES T DATE: I*/*/(ft 

TES T UNIT: #3 

TES T STAR T TIME: 

Receiver* Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver* Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

ibs.) 

| t -

1 lbs 

VES018461 
TEST DATE : l^l^lXfl 

TEST UNIT: £ 3 

TEST STAR T TIME: S'-ID Mtft a * 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

) Spike (3.C 

Ibs.) 

P Receiver* Charge # Hex 

Spike (3.C 

ibs.) 

H e i 

Spike (3.C 

Ibs.) 

• 

It 

->» yrV: 

ifft;. 

'£6 

ZX < ^ 

f t ^ > 

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f f 

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3> 

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VES018462 
tes t date : l>/*/cc

> 

tes t unit: * 3 

tes t star t time: Uu/[" a 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

) Spike (3.C 

Ibs.) 

) 

; Receiver* Charge # Hex 

Spike (3.C 

lbs.) 

Hex 

) Spike (3.C 

Ibs.) 

> 

-> 

,

, .r — 

\ 

I 

3S-5HHb 3 "15 3 1 4 3 

1 4 ^ 

1 4 1 1 3 b 

St' 1 C \ • 7 ^ 4 

1 \ W 'ii i 

1G4 -

1X1 1 1 5 

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1 S 4 7 3 6 

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13/ 3 

VES018463 
TEST DATE: lW5/( # 

TEST UNIT: * 3> 

TEST START TIME: ^ ^ 

Receiver* Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

) Spike (3.C 

Ibs.) 

) 

; Receiver* Charge # Hex 

Spike (3.C 

ibs.) 

Hex 

Spike (3.C 

Ibs.) 

3 a „ • 

m 

MO 1-93 

m 1* 

w 1% 

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LS3. bbO UO i 

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tm 

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bS\ * -PS 

hi W l 

bHS life 

Iff tol 

a • 

VES018464 
TEST DATE: 

TEST UNIT: 3> 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

) Spike (3.C 

Ibs.) 

) 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

Spike (3.C 

Ibs.) 

t ? n 

i7C 

t4\ 

W4 4aSJ 

Wo 4 9 6 

. w o 44+ 

IT* f\o ifs:* 441 

H4S' 

F^ 431 

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41$ 

km W'-i' 4 ^ 

413 

bafl. 43* 

b^5 i f 441 

b35 ?£•?!• 4*4 

4 3 3 

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b30 43b 

[QC^4 4*3 

4lV> 

^Ir" 4^4 

401 4,^ -

4(4 430 

TO Si' 4 3 3 

1 its; 4u 

VES018465 
TEST DATE: P/*/(jf i 

TEST UNIT: * 3 

TEST START TIME: 

Receiver* Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

Spike (3.C 

Ibs.) 

) 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

l i 3>40 ^ 4 

%\ !Kl>.. 410 

4SQ 

4 i i 

%<? 

L/C 4*1 

4 X ] 

% 3 Hc3 -

4 $ i f 

%b ' ' ' . 

HCI HI 

ft 

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4SU 4 ^ 3 

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41^ 

4$ 

4^ 

450 4^ 

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455 4lb 

til 4 ^ 

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4 1 5 8? y& 

453 

411 

VES018466 
Waste Feed Profiles 

VES018467 
Report: R7008 

DATE: 11/30/09 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

BUSINESS: 

DEPT 

ADDRESS 1: 

ADDRESS 2: 

•Y/ST. . : 

'ACT, . : 

ARCHER DANIELS MIDLAND, COVITAMIN E PLANT 

37 00 E. DIVISION STREET 

DECATUR IL 62526 

DAVID BROAD HACKER 

WASTE NAME: SOLVENT RECOVERY 

PROCESS3 GENERATING WASTE: SOLVENT RECOVERY 

SHIP. NAME: WASTE FLAMMABLE LIQUIDS, N.O.S 

ADDL. DESC: (ACETONE, METHANOL) 

Version 06. 04 

TWI-028691 

SELLING REGION LAB 

NUMBER : 142-8-789 

PHONE 217/151-4392 

EXPIRES . : 01/11/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: ILR000021550 

STATE EPA ID..: 1150155345 

EPA STATUS : CHK RESTRICT 

SALES OFFICE..: RFK 

CHEMICAL COMPOSITION ACETONE 

HEPTANE 

METHYL ALCOHOL 

WATER 

BENZENE 

NON-TRI CHEMICALS 

EMULSIFIED OIL 15 

UNIT DESCRIPTION 

25 35 % 

25 35 % 

25 35 % 

1 38 % 

1 38 PPM 

25 % 

METALS EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State...: Liquid 

Flash Point : > = 200 CL 

pH : 04.0 - 09.0 

Color VARIES 

Odor : NONE 

Layers : Single Layer 

Specific Gravity.: 0.950 - 1.150 

Free Liquids : 99 - 100 

Cyanides : < 5 PPM TOTAL 

Sulfides < 3 PPM TOTAL 

PCB'0 l PP1*, Regulated by 40 CFR 761: 

Phenolics : < 10 PPM 

% Taxable : DOT UN/NA NBR: UNIS93 

Treatment Codes..: T07 

CRQ RPT QTY Material Class: 

EPA Permit : EXP: 

Hazard Class : 3 

State Codes : 090001 

Benzene .: 38 NESHAP: Controlled Benzene NESHAP 

Packing Group . ...: II 

Process Codes....: CBC 

Cert of Dstrct Rq: 

Federal Codes: DOOl D018 F003 

NEO. GREY GLOVES 

TYPE C RESPIR CONST FLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NITRILE (INNER GLOVE) 

BENZENE NESHAP CONTROLS REQUIRED; NO CERT 

CANCER SUSPECT AGENT: BENZENE 

Inhalation: 2 

DOT PROPERTIES 

Oral: 2 Flammable: 0 Health: 0 

Waste Type 

Form Code 

B21S 

1 

CHARGE CODE: NS 

BENZENE NESHAP CONTROLS REQUIRED; NO CERT 

COMMENTS 

REVIEWED FOR MACT METALS 

VES018468 
Report: R7008 

DATE: 11/24/05 

BUSINESS: 

DEPT : 

ADDRESS 1: 

ADDRESS 2: 

'/ST.. : 

CT..: 

IMPERIAL CLEANERS 

2210 WISCONSIN AVE 

NEW HOLSTEIN 

KEN WALKER 

ONYX ENVIRONMENTAL SERVICES, 

WASTE PROFILE SUMMARY 

WI 53061 

WASTE NAME: TETRACHLOROETHYLENE CONTAMINAT ED SOIL 

PROCESS GENERATING WASTE: CLEANUP OF TETRACHLOROETHYLENE SOIL FROM DRY CLEAN 

SHIP. NAME: HAZARDOUS WASTE; SOLID, N.O.S 

ADDL. DESC: M3(TETRACHLOROETHYLENE) 

Version 06.04 

TWI-096110 

SELLING REGION LAB - MRL 

NUMBER : 144-0-059 

PHONE : 920/898-4800 

EXPIRES : 10/01/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: WID981540010 

STATE EPA ID..: 9550019999 

EPA STATUS CMC RESTRICT 

SALES OFFICE..: CSH 

CHEMICAL COMPOSITION 

TETRACHLOROETHYLENE 

SOIL 

NON-TRI CHEMICALS 

PAPER, PLASTIC, 

H - MAX UNIT DESCRIPTION 

0 10000 PPM 

95 100 % 

0 5 % 

METALS EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State. . . -• Solid 

Flash Point : > = 200 CL 

pH : 05.0 - 10.0 

Color : BROWN 

Odor : NONE 

Layers : Single Layer 

Specific Gravity.: 0.000 

Free Liquids : 0 

Cyanides : < 5 PPM TOTAL 

Sulfides : < 3 PPM TOTAL 

PCB's PP""> Regulated hy 40 CFR 761: 

Phenolics : 10 PPM 

% Taxable. ,.,.... : DOT UN/NA NBR: NA3077 

Treatment Codes..: T07 

CRQ RPT QTY. : 100 Material Class: 

EPA Permit : EXP: 

Hazard Class 9 

State Codes 090001 

Benzene : NESHAP: 

Packing Group.. ..: HI 

Process Codes,...: BSL 

Cert of Dstrct Rq: 

Federal Codes; 

NEO. GREY GLOVES 

TYPE C RESPIS CONST FLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NITRILE (INNER GLOVE) 

kapplers chem tape 2 

Inhalation: 2 

DOT PROPERTIES 

oral: 2 Flammable: 0 Health: 0 

SUMMARY 

Waste Type 

Form Code 

B301 

1 

CHARGE CODE: NS 

PE EVENT EXPIRES 12-31-09 

COMMENTS 

REVIEWED FOR MACT METALS 

VES018469 
Report: R7008 

DATE: 11/24/09 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

BASF CORP 

. .HANNIBAL PLANT 

3 ISO HWY JJ 

BUSINESS: 

DEPT : 

ADDRESS 1: 

ADDRESS 2 I 

"'/ST . . : 

.CT.. : 

WASTE NAME: IMI-2 HERBICIDE ORGANIC WASTE SPILL CLEANUP 

PROCESS GENERATING WASTE: ORGANIC WASTE SPILL CLEANUP 

SHIP. NAME: HAZARDOUS WASTE, SOLID, N.O.S 

ADDL. DESC: (TOLUENE, METHANOL) 

Version 06.04 

TWI-0S7802 

SELLING REGION LAB 

NUMBER 105-7-002 

PHONE ': 

EXPIRES : 10/27/11 

STATUS : APPR FOR SERV 

FEDERAL' EPA ID: MOD050226075 

STATE EPA ID..: 9290019999 

EPA STATUS . . . . .• CHK RESTRICT 

SALES OFFICE. . : RPK 

CHEMICAL COMPOSITION 

METHANOL 

TETRAHYDROFUTUW 

TOLUENE 

WATER 

NON-TRI CHEMICALS 

SOIL AND GRAVEL 

SPILL C1EAS-DP DEBRIS 

HERBICIDE BY-PRODUCTS 

UNIT DESCRIPTION 

0 

0 

.1 

0 

95 

0 

0 

.1 % 

.1 * 

2 % 

1 % 

99 % 

1 % 

.1 % 

METALS EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical'State...: Solid 

Flash Point N/A CL 

pH : 04.0 - 09.0 

Color ' BROWN 

Odor : NONE 

Layers .; Single Layer 

Specific Gravity.: 0.000 

Free Liquids : 0 

Cyanides : < S PPM 

Sulfides : < 3 PPM 

PCB's ppm. Regulated by 40 CFR 761i 

Phenolics : < 10 PPM 

% Taxable DOT UN/NA NBR: NA3077 

Treatment Codes..: T07 

CRQ RPT QTY : Material Class: 

EPA Permit EXP: 

Hazard Class : 9 

State Codes : 090001 

Benzene : NESHAP: 

Packing Group Il l 

Process Codes....: BSL 

Cert of Dstrct Rq: Y 

TOTAL 

TOTAL 

Federal Codes: DOOl F0O3 F005 

NEO. GREY SIiCVTiS 

TYPE C RESPH CONST FLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NlrRILE (INNER GLOVE) 

Inhalation: 2 

DOT PROPERTIES 

Dermal: 2 Oral: 2 Flammable: 0 

Waste Type 

Form Code 

B301 

1 

CHARGE CODE: NS 

PE 10-28-10 

COMMENTS 

REVIEWED FOR MACT METALS 

REPORT WEIGH37 

VES018470 
Report: R700B 

DATE: 11/30/03 

ONYX ENVIRONMENTAL SERVICES, 

WASTE PROFILE SUMMARY 

VEOLIA ES TECHNICAL SOLUTIONS 

7 MOBILE AVE 

BUSINESS : 

DEPT 

ADDRESS 1 

ADDRESS 2 

— v /ST. . 

C T . . 

WASTE NAME: ON-SITE RAINWATER & ASH WATER 

PROCESS GENERATING WASTE: COLLECTION OF ON-SITE STORMWATER & PRECIPITATION; 

SHIP. NAME: HAZARDOUS WASTE, LIQUID, N.O.S 

ADDL. DESC: 

Version vo.u* 

TWI-TW2519 

SELLING REGION LAB - MRL 

NUMBER : 110-9-722 

PHONE 

EXPIRES : 11/30/14 

STATUS : CONTRACT NOT IN PLACE 

FEDERAL EPA ID: ILD098642424 

STATE EPA ID..: 1631210009 

EPA STATUS : CHK RESTRICT 

SALES OFFICE..: RPK 

ATER 

CHEMICAL COMPOSITION 

WATER 

NON-TRI CHEMICALS 

ASHWATEB 

MISC SOLIDS, WASTE RESIDUES 

MIN - MAX UNIT DESCRIPTION 

S9 100 % 

50 % 

1 % 

METALS Arsenic as As 

Cadmium as Ct3 

Lead as Pb 

Mercury as Hg 

Selenium as Se 

Chromium Hex 

Nickel as Ni 

Thallium as Tl 

EP TOX/TCLP 

5.0 

1.0 

5.0 

.2 

1.0 

mg/l 

mg/l 

mg/l 

mg/l 

mg/l 

PHYSICAL CHARACTERISTICS 

Physical State...: Liquid 

Flash Point : > = 200 CL 

pH : 02.0 - 12.5 

Color : VARIES 

Odor : NONE 

Layers : Single Layer 

Specific Gravity. : 0.950 - 1.150 

Free Liquids : 99 - 100 

Cyanides : < 5 PPM TOTAL 

Sulfides : < 3 PPM TOTAL 

PCB's : PPm, Regulated by 40 CFR 761: 

Phenolics : < 10 PPM 

% Taxable : DOT UN/NA NBR: NA3082 

Treatment Codes..: T07 

CRQ RPT QTY...,..: Material Class: 

EPA Permit. : EXP: 

Hazard Class.....: 9 

State Codes : 090001 

Benzene : NESHAP: 

Packing Group-...: Il l 

Process Codes....: 

Cert of Dstrct Rq: 

Federal Codes: D003 D007 D008 D004 D005 D006 D009 DOlO D011 D012 D013 D014 D015 D016 D017 D018 + 

HANDLING 

SITE GENERATED WASTE 

DOT PROPERTIES 

Inhalation: 0 Dermal: 0 Oral: 0 Flammable: 0 Health: 0 

TWI Signed Addendum 

SITE GENERATED 

VES018471 
Report: R700B 

DATE: 11/30/09 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

BUSINESS i US ARMY FLW 

DEPT : ..DIRECTOR OF PUBLIC WORKS 

ADDRESS 1: IMHE-LNW-PWE,BLDG 2101, DPW 

ADDRESS 2: 1334 1ST ST 

'"/ST. . : FORT LEONARD WOOD MO 65473-8944 

1CT..: SHANNON CAIN 

WASTE NAME: DECON WATER-TREATED VX & OB TO DRINKING WATER STANDARDS 

PROCESS GENERATING WASTE: DECON OF CHEMICAL WEAPONS RECOGNITION TRAINING COM 

SHIP. NAME: NON-REGULATED MATERIAL 

ADDL, DESC: 

Version 06,04 

TWI-076886 

SELLING REGION LAB 

NUMBER : 143-S-3 93 

PHONE : 573 596 0682 

EXPIRES : 02/19/11 

STATUS APPR FOR SERV 

FEDERAL EPA ID: MO3213720979 

STATE EPA ID..: 9290019999 

EPA STATUS UNDETERMINABL 

SALES OFFICE..: TWI 

CHEMICAL COMPOSITION 

WATER 

SODIUM HYDROXIDE 

NON-TRI CHEMICALS 

SUPER TROPICAL BLEACH 

COMMENTS 

TRACES OF VX AND GB AGENT ARE NEUTRALIZED WITH BLEACH AND RINSED 

WITH THOUSANDS OF GALLONS OF WATER, THEN COLLECTED FOR 

INCINERATION. ALL WATER IS TESTED PRIOR TO SHIPMENT TO ENSURE 

COMPLIANCE WITH DRINKING WATER STANDRADS. VX AND GB 

CONCENTRATION ARE CERTIFIED TO BE BELOW 20 PPB AND ARE USUALLY 

<2 PPB. (3X LEVEL) 

N - MAX UNIT DESCRIPTION 

93 100 % 

1 2 % 

1 5 % 

EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State...: Liquid 

Flash Point : > = 200 CL 

pH : 05:0 - 09.0 

Color VARIES 

Odor : NONE 

Layers.. : Single Layer 

Specific Gravity.: 0.950 - 1.150 

Free Liquids 99 - 100 

Cyanides : < 5 PPM TOTAL 

Sulfides : < 3 PPM TOTAL 

PCB's : N/A ppm. Regulated by 40 CFR 761: 

Phenolics : <: 10 PPM 

% Taxable : DOT UN/NA NBR: 

Treatment Codes..: T07 

CRQ RPT QTY,,...,: Material Class: 

EPA Permit. : EXP: 

Hazard Class 

State Codes : 090002 

Benzene NESHAP: 

Packing Group....: 

Process Codes DI2 

Cert of Dstrct Rq: Y 

Federal Codea: NH00 

NEO. GREY GLOVES 

TYPE C RESPIR CONST FLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NITRILE (INNER GLOVE) 

DI-WATER WITH DECOMPOSITION PRODUCTS OF GB/VX. 

REACTIVE CATEGORY: A (FOR SCHEDULING ONLY) 

Inhalation: Dermal: 3 

DOT PROPERTIES 

Oral: 2 Flammable: 0 

SUMMARY 

Waste Type B219 

Form Code 1 

COMMENTS 

. -WARGE CODE: NS REVIEWED FOR MACT METALS 

'TIVE CATEGORY: A (FOR SCHEDULING ONLY) COD REQUIRED 

.. J-18-10 VEOLIA TRANSPORTATION ONLY. 

BILLING: TRIP TICK, WT TIC, COD AND COPY OF TAG WITH INVOICE. WHEN COD IS PRINTED, COPY TO CSR 

TO RETURN WITH MANIFEST TO GENERATOR ALSO. 

VES018472 
TWI Laboratory Analysis Report 

Receiver #: TK304 Visual Inspection: Glove Box / Hooded Feeder 

#of Druins: 1 

Date: 6/29/2001 

Profile*: 777777 

Generator TRAD E WAST E INCINERATION 

Descript: 

Process Code(s): 

Drum Storage Compatability 

Profiled DOT Hazard Class 9 

P = Pass F = Fail 

8A 8B 4/5 

Sample Number 

Drum Rep / Comp 

303022_j_iL00000001 

XI 

Free Liquid (%) IIIII III Profile Conform Date Initials 

Pumpable NO 303022 wwww v Yes No 11/06/09 MT 

Layers/Phases - % Ea . 

Color ^ \ 

Turbidity 

Viscosity L X 

Physical State 

Water Miscibility 

Add. Description 

Water Reactivity ^\\ \ 

Radiation Screen =BKG X 

Flam. Pot. Screen See Flashpoint X 

pH Screen 5 at 100 pert 2-12.5 X 

Oxidizer Screen ^\\\ 

Paint Filter Test wwww v 

Cyanide Screen wwww v 

Sulfide Screen \\\\\\\\\ ^ 

Incidental Odor 

Specific Gravity 1.01 11/04/09 MT 

BTU/Lb 1570 11/04/09 BD 

% Chloride 1.2 11/04/09 KD 

Flash Point-Deg F 01/01/00 

PCBs By G C - mg/kg <50ppm 11/06/09 

pH by Meter \\\\\\\\\ ^ 01/01/00 

Arsenic mg/kg 4.768 0 

Beryllium mg/kg 4.165 0 

Cadmium mg/kg 4.765 0 

Chromium mg/kg 4.805 0 

Lead mg/kg 4.7B4 0 

Mercury mg/kg 0.056 0 

Profile Review for Appendix WAP- C Consitituents by: 

Date: 

Add. Comments: The data in the sample information section(6/29/2001 )is date profile 77777.7. was created. 

VES018473 
File Inventory Print Approvals Chemist Receiving Laboratory Tank Farm Process Planning Window Billing Help 

ii^llll t jg| Waste-Tracking System 

VES018474 
I wi Laboratory Analysis Report 

Receiver #: TK310 Visual Inspection: Glove Box I Hooded Feeder 

# of Drums: 1 

Date: 6/29/2001 

Profile #: ZZZZZZ 

Generator: TRAD E WAST E INCINERATION 

Descript: 

Process Code(s): 

Drum Storage Compatibility 

Profiled DOT Hazard Class 9 

P = Pass F = Fail 

8A 8B 4/5 

Sample Mumber 

Drum Rep / Comp 

301556 ] iLOOOOOOOl 

1/ ~1 IIIIIII 

301556 

Free Liquid (%) IIIIIII 

301556 

Profile Conform Date Initials 

Pumpable NO 

IIIIIII 

301556 w w w Yes No 10/01/09 SL 

Layers/Phases - % Ea . www w 

Color 

Turbidity www w w w 

Viscosity L X 

Physical State www w 

Water Miscibility ' , www w W W 

Add. Description 

Water Reactivity www w W W 

Radiation Screen =BKG X 

Flam. Pot. Screen See Flashpoint X 

pH Screen 3 at 100 pent 2-12.5 X 

Oxidizer Screen 

Paint Filter Test WWW W ^ w 

Cyanide Screen ^\\\ 

Sulfide Screen w\ww w ^\\\ 

Incidental Odor www w 

Specific Gravity 0.83 10/01/09 SL 

BTU/Lb 9600 10/01/09 MT 

% Chloride <0.5 10/01/09 JF 

Flash Point - Deg F 01/01/00 

PCBs By G C - mg/kg <50ppm 10/01/09 

pH by Meter www w W W 01/01/00 

Arsenic mg/kg 0 0 

Beryllium mg/kg 0 0 

Cadmium mg/kg 0 0 

Chromium mg/kg 0 0 

Lead mg/kg 0 0 

Mercury mg/kg 0 0 

Profile Review for Appendix WAP- C Consitituents by: 

Date: 

Add. Comments: The data in the sample information section(6/29/2001)is date profile 777777 was created. 

VES018475 
Sa Waste 1 rucking System 

Fie Inventory Print Approvals Chemist Receiving Laboratory Tank Farm Process Plannhg Window Wing Help 

VES018476 
TWI Laboratory Analysis Report 

Receiver #: 352920 Sample Required 

# of Drums: 1 

Date: 10/22/2009 

Profile* 076886 

Generator: U S ARM Y FL W 

Descript: DECO N WATER-TREATE D VX & G B T O DRINKING WATE R STANDARD S 

Process Code(s): DI2 

Drum Storage Compatibility 

Profiled DOT Hazard Class 9 

P = Pass F = Fail 

8A 8B 4/5 

Sample M umber 

Drum Rep / Comp 

302522_j_005389778JJl 

BOLK/I 

302522 

Free Liquid (%) 100 

302522 

Profile Conform Date Initials 

Pumpable YES 302522 WWW W Yes No 10/22/09 SD 

Layers/Phases -% Ea. 100 WWW W \\\ \ 

Color colorless ^WWW W 

Turbidity transparent WWW W W W 

Viscosity low L X 

Physical State liquid WWW W 

Water Usability Misc w\\\ w W W 

Add. Description 

Water Reactivity No RXN 

Radiation Screen =3KG =BKG X 

Flam. Pot. Screen NEGATIVE See Flashpoint X 

pH Screen 7 at 100 pent 2-12.5 X 

Oxidizer Screen NEGATIVE wwww v 

w w 

Paint Filter Test N/A 

Cyanide Screen NEGATIVE www\ w 

Sulfide Screen NEGATIVE W W 

Incidental Odor No wwww v 

Specific Gravity 1.01 0.950-1.150 10/22/09 BD 

BTU/Lb <500 1 -5000 10/22/09 KD 

% Chloride <0.5 2 - 0 W W i 10/22/09 AJ 

Flash Point - Deg F >140 w w 01/01/00 

PCB s By G C - mg/kg <50ppm 10/22/09 

pH by Meter \\w\ w ^ \ w 

01/01/00 

Arsenic mg/kg 0 0 w w ^ 

Beryllium mg/kg 0 0 

Cadmium mg/kg 0 0 

Chromium mg/kg 0 0 W W 

Lead mg/kg 0 0 ^\\\ 

Mercury mg/kg 0 0 W W 

Additional Comments: MAY SHO W PO S O X SCREE N DU E T O BLEACH-OKA Y T O ACCEPT . 

Profile Review for Appendix WAP- C Consitituents by: KMEREDITH 

Date: 3/18/2009 

Add. Comments: DI-WATER W/DECOMPOSITION PRODUCT S OFGBA/ X 

VES018477 
CMS Performance Evaluation 

VES018478 
TAG 

LOOP 

DESCRIPON 

SERVICE 

LOCATION 

LP-SHT 

P&ID 

REMARKS 

INSTL-RMKS 

SPEC-RMKS 

S/N 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

QUARTERLY 

WT 

304 

WEIGHT TRANSMITTER 

SPECIALTY FEEDER (HOODED) 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

TOLEDO 

8140 EXP 

0-2,000 # 

0-2,000 # 

4-20 MADC 

0#=819 CC S 

200#=1147 Ct S 

1#=1.638 Ct S 

30012 

Check scale, digital Calibration per. Toledo instructions. 

Then with no weight on scale adjust analog zero. (NOTE: HMI 

will not display numbers less than zero). Next add weight 

= to 10% are more of scales range, then adjust analog span, 

to indicate weight on scale, as read on HMI screen. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

INPUT VALUE 

O 

120 

CALIBRATION REPORT 

INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments 

Performed by:. h> r r 

JB 

CALSHEET.WDB 

11-10-01 

. Dater4&-T7^cV^ Time: TL^t^ AM (PM^) 

Place:. 

VES018479 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

. LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #3 

QUARTERLY 

WT 

310 

WEIGHT TRANSMITTER 

SOLID CHARG CONV. 

FIELD 

3031 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

TOLEDO 

8140 

0-400 # 

0-400 # 

4-20 MADC 

0#=819 Ct S 

200#=2457 Ct S 

1#«8.19 Ct S 

30022 

Check scale, digital Calibration per. Toledo instructions. 

Then with no weight on scale adjust analog zero. (NOTE: HMI 

will not display numbers less than zero). Next add weight 

= to 10% are more of scales range, then adjust analog span, 

to indicate weight on scale, as read on HMI screen. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

INPUT VALUE 

D 

5 T 3 

CALIBRATION REPORT 

INSTRUMENT READING 

Before Calibration 

After Calibration 

O 

S2> 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by:. 

JB 

CALSHEET.WDB 

_ Vated®zjhQ%z_ Time: Z//Q AM (ST) 

Place 

VES018480 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

QUARTERLY 

PDT 

350 

PRESSURE DIFF. TRANSMITTE MANUFACT: YOKOGAWA 

BAGHOUSE INLET/OUTLET 

FIELD 

3035 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

0-15 xn wc 

4-20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH INCLINE MANOMETER AND 

LOOP CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT 

WITH LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

O

 Aft& r

 calibration tf> p? ^ 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: 

JB Place: 

CALSHEET.WDB (Field or Shop) 

VES018481 
TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

QUARTERLY 

TAG: PT 

LOOP: 300 

DESCRIPON: PRESSURE TRANSMITTER MANUFACT: Rosemount 

SERVICE: LOW CHAMBER PRESS. MODEL: 1151 DP 

LOCATION: FIELD SCALE: -7.5 to +2.5 in. wc, 

LP-SHT: CALIB-IN: 

P&ID: 3032 CALIB-OUT: 4-20 MADC 

REMARKS: PROCESS-SP: 

INSTL-RMKS: INST-SP: 

SPEC-RMKS: ACTION: 

S/N: I/O NUMBER: 

CALIBRATION NOTES 

Connect transmitter to be calibrated to pressure source 

and calibrated reference (Manometer), input appropriate 

pressure and verify with current meter. 

Complete and affix a properly filled-out calibration 

sticker. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

/r-M Before Calibration . 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: Q nl (3>Y. 

Performed by. /ff?e,Lo^ M'm, Date: °? Timai^L 

JB Place: 

CALSHEET.WDB (Field or Shop) 

PM 

VES018482 
TWI INSTRDMENT CALIBRATION RECORD 

UNIT #3 

QUARTERLY 

TAG: PT 

LOOP: 319 

DESCRIPON: PRESSURE TRANSMITTER MANUFACT 

SERVICE: UPPER CHAMBER PRESSURE MODEL 

LOCATION: FIELD SCALE 

LP-SHT: CALIB-IN 

P&ID: 3033 CALIB-OUT 

REMARKS: PROCESS-SP 

INSTL-RMKS: INST-SP 

SPEC-RMKS: ACTION 

S/N: I/O NUMBER 

-7.5 Co +2.5 in. 

4-20 MADC 

wc. 

CALIBRATION NOTES 

Connect transmitter to be calibrated to pressure source 

and calibrated reference (Manometer), input appropriate 

pressure and verify with current meter. 

Complete and affix a properly filled-out calibration 

sticker. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: /^^&/-.&jCi /gS'fri Date: ^ r ® ? Time: PM 

JB Place: 

CALSHEET.WDB (Field or Shop) 

VES018483 
TAG 

LOOP 

DESCRIPON 

SERVICE 

LOCATION 

LP-SHT 

P&ID 

REMARKS 

INSTL-RMKS 

SPEC-RMKS 

S/N 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

QUARTERLY 

Tribo 

Baghouse Leak Detection 

FLD 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

Auburn 

TRIBO.dgd 

0-1000pa 

0-l000pa 

4-20ma 

CALIBRATION NOTES 

Disconnect the input cable at the BNC connector on the input 

card, and check for zero. Use Auburn, Triboflow, filed test 

unit, model 2902, to input a Pico-Amp signal of 500pa and 

record these values. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

0 f A 

SOD p A 

INSTRUMENT READING Before Calibration 

5 P M fA 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments : lV)o Ca\<hT<xhloY\ nee-oled. 

Performed by: Date:. Time: 1 / • 3 &foMJVM 

JB Place: — 

CALSHEET.WDB ({Field)or Shop) 

VES018484 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #3 

QUARTERLY 

AT 

389 

OXYGEN 

STACK GAS ANALYZER 

FIELD 

3035 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

COSA 

0-25% 

0-25% 

4-20 MADC 

CALIBRATION NOTES 

Flow calibration gas at 2-3 psig and 3 scfh 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1.lb/hr 

CALIBRATION REPORT 

INSTRUMENT READING 

Before Calibration «^ ^ 

After Calibration 

INPUT VALUE 

? , 9 

2-1 • 

CALIBRATION SOURCE REFERENCE 

ZERO GAS CYL ft : PC i \X<J L 

SPAN GAS CYL #: !>&lfl\ \ 3 ^ 

Comments: . 

Performed by: Date: //"/A^ ^ Time: ^/JT^AjpPM 

JB Place: ... 

CALSHEET. WDB /(field J>r Shop) 

VES018485 
TWI INSTRUMENT CALIBRATION RECORD UNIT #3 

QUARTERLY 

TAG: 

LOOP : 

DESCRIPON: 

SERVICE: 

.LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

AT 

388B 

HC 

STACK GAS ANALYZER 

STACK 

556 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

Thermo Elect, 

51C 

0-100 PPM 

4-20 MADC 

C o . 

CALIBRATION NOTES 

1) Open sample gas bottle valves. 

2) Press MENU Button 

3) Press CALIBRATION 

4) Press ZERO ADJUST 

5) Press SPAN ADJUST after 4)finished 

6) Press RUN after 5)finished 

7) Close sample gas bottles. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

o 

Before Calibration INSTRUMENT READING 

c 

After Calibration 

GAS CYL #:. 

CALIBRATION SOURCE REFERENCE 

Comments: fat IV&E ^ 

Performed by:. 

JB 

CALSHEET.WDB 

Date: Time: f&l&fjp/ m 

Place:. 

(Field or Shop) 

VES018486 
TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

QUARTERLY 

TAG: AT 

LOOP: 388B 

DESCRIPON: OPACITY 

SERVICE: STACK GAS 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

STACK 

2.00 to 5.72ma 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

TELEDYNE INST. 

LightHawk 

0-100% 

4-20 MADC 

CALIBRATION NOTES 

Clean windows. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: Califataiynf |?-er YhQW^&chj ceS'k Q^uldAl^ey. 

Performed hy: J ^^T T ^1^90 Date: Ifi-jO '

J

0°\ Time: ll'OD'^)m 

JB Place: 

CALSHEET. WDB HFieldt or Shop) 

VES018487 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT:' 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TT 

300A 

PLC THERMOCOUPLE 

LOWER CHAMBER 

FIELD 

2032 

UNIT #3 

ANNUAL 

INPUT MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

MODICON 

883-200 

0-2500 deg. 

TYPE K 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a type K temperature signal of 500 deg F. and 2,000 

deg.F. at input of PLC, then verify this single on the 

control panel CRT. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

^00 ° f~ Befor e Calibration fT~QQD 

zooo ° F zooo° " 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments 

Performed by 

JB 

CALSHEET.WDB 

, £uJH-& , _ Date: Time: 

Place: 

{(Fielder Shop) 

VES018488 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #3 

ANNUAL 

TT 

300B 

PLC THERMOCOUPLE INPUT MANUFACT: 

LOWER CHAMBER MODEL: 

FIELD SCALE: 

CALIB-IN: 

3032 CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

MODICON 

883-200 

0-2500 deg. 

TYPE K 

Use cold junction compensated thermocouple calibrator to 

input a type K temperature signal of 500 deg F. and 2,000 

deg.F. at input of PLC, then verify this single on the 

control panel CRT. 

See Manufactures literature for detailed instructions 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

S0OD F 

Zooo0f 

Before Calibration 

INSTRUMENT READING 

— 

After Calibration 

SIX) 

Zooo° 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by 

JB 

CALSHEET.WDB 

ife /JT ? Date: )}HV-OC\ Time: 2 J^£^AM(S ) 

Place: 

(Field hr Shop) 

VES018489 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TT 

319A 

PLC THERMOCOUPLE 

UPPER CHAMBER 

FIELD 

3033 

UNIT #3 

ANNUAL 

INPUT MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

MODICON 

883-200 

0-2500 deg. 

TYPE K F. 

Use cold junction compensated thermocouple calibrator to 

input a type K temperature signal of 500 deg F. and 2,000 

deg.F. at input of PLC, then verify this single on the 

control panel CRT. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

INPUT VALUE 

ZOOQ°P 

CALIBRATION REPORT 

INSTRUMENT READING Before Calibration 

SOi0 

ZQoo ° 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments : KJ o ca fi bra. 4-> 6 A ne edeJPerformed by: — " I ~ — Date : W-IQ-Q^ Time:Z.' AMfjjjT) 

JB 

CALSHEET.WDB 

Place: 

Field/or Shop) 

VES018490 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

ANNUAL 

TT 

319B 

PLC THERMOCOUPLE INPUT MANUFACT 

UPPER CHAMBER MODEL 

FIELD SCALE 

CALIB-IN 

3033 CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

MODICON 

883-200 

0-2500 deg. 

TYPE K 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a type K temperature signal of 500 deg F. and 2,000 

deg.F. at input of PLC, then verify this single on the 

control panel CRT. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

5DODF 

Zooo°P 

INSTRUMENT READING 

Before Calibration SOO o 

2600 ' 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: Mo Cal 

Performed by: Date: \\~\Q~Cf\ Time: Z:^fS" AM (PM^) 

JB Place: ^=*~^ 

CALSHEET. WDB UFielcTSor Shop) 

VES018491 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #3 

ANNUAL 

TT 

323 

PLC THERMOCOUPLE 

SDA INLET 

FIELD 

3033 

INPUT MANUFACT 

MODEL 

SCALE 

CALIB-IN 

CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

CALIBRATION NOTES 

MODICON 

883-200 

0-2500 deg. 

TYPE K 

Use cold junction compensated thermocouple calibrator to 

input a type K temperature signal of 500 deg F. and 2,000 

deg.F. at input of PLC, then verify this single on the 

control panel CRT. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INSTRUMENT READING 

Before Calibration /•—» , 0 

Zooo° 

After Calibration 

INPUT VALUE 

soo°P 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: f . fi^y QflQ Date: Jl-lQ-Qf Time:2/,c /S~ AMtpjO 

JB Place: 

CALSHEET.WDB ((Field or Shop) 

VES018492 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #3 

ANNUAL 

TT 

370 

PLC THERMOCOUPLE INPUT MANUFACT 

SDA OUTLET TEMP. MODEL 

FIELD SCALE 

CALIB-IN 

3034 CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

MODICON 

883-200 

0-2500 deg. 

TYPE K F. 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a type K temperature signal of 500 deg F. and 2,000 

deg.F. at input of PLC, then verify this single on the 

control panel CRT. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

/—~ -. a .— Before Calibration __ . o 

SOO P SOI 

ZOOO °f 2002. ° 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments : M o Calibrating needed. 

Performed by: . Date: Time _AM 

JB 

CALSHEET.WDB 

Place:. 

(Field or Shop) 

VES018493 
TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

ANNUAL 

TAG: FT 

LOOP: 383 

DESCRIPON: STACK 

SERVICE: STACK 

LOCATION: FIELD 

LP-SHT: 

P&ID: 3035 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

FLOW TRANSMITTER MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

Rosemount 

0-20,000 ACFM 

0-.5»WC 

4-20 MADC 

Set Damp/pot to mid point 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH INCLINE MANOMETER AND 

LOOP CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT 

WITH LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

After Calibration * 

(U;> u?c / 9- ?ffrt fo 

CALIBRATION SOURCE REFERENCE 

Comments: fl/rs 

Performed by: >0te/x>^ JSi'm Date: ^fZ^/vfT±m&: //:o&<$$ 

JB Place: ; 

CALSHEET.WDB (Field or Shop) 

PM 

VES018494 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #3 

ANNUAL 

FT 

315 

FLOW TRANSMITTER 

HIGH BTU Liquid Feed 

FLD 

3031 

Flow Cal. *11464128834.26 

238615 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

MICRO MOTION 

DS-040S119SU 

0-3600 lb/hr 

4-20 MADC 

30001 

CALIBRATION NOTES 

Flush process piping, connect water hose to upstream side of 

flow meter, set control system to appropriate rate control, 

and read totalizer, flow water into a container and compare 

the toltalizer reading to the measured amount in container. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

. , /\ j Before Calibration !.>. i L 

10 IPS - vpQr. yn)y\ . \QS j m \r\ /(J , J J \ bS>-

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by- £k— ^ • fi^y. Date: )l-Z0-Q9\ Time: 2'3Q AM(PKT) 

JB 

CALSHEET.WDB 

Place:. (Fieldybr Shop) 

VES018495 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #3 

ANNUAL 

FT 

316 

FLOW TRANSMITTER 

LOW BTU 

FLD 

3031 

MANUFACT: MICRO MOTION 

MODEL: DS-040 

0-3600 lb/hr 

4-20 MADC 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 30002 

CALIBRATION NOTES 

Flush process piping, connect water hose to upstream side of 

flow meter, set control system to appropriate rate control, 

and read totalizer, flow water into a container and compare 

the toltalizer reading to the measured amount in container. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

i n ,< - r~i vBefore Calibration Ci QC^ * i IU lbs, pec, m,^. w c )r^'in. M o )oS>-

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments 

Performed by: Date: Time: .AM (PM^> 

JB Place: ^? 

CALSHEET.WDB ((Field) or Shop) 

VES018496 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #3 

ANNUAL 

FT 

3 88 

FLOW TRANSMITTER MANUFACT: E-H 

LIME SLURRY TO HEAD TANK 

FIELD 

3034 

MANUFACT 

MODEL 

SCALE 

CALIB-IN 

CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

0-20 GPM 

4-20 MADC 

CALIBRATION NOTES 

ESTABLISH UNIFORM FLOW INTO CONTAINER, READ TOTALIZER, FLOW 

FLUID INTO GRADUATED CONTAINER AND VERIFY WITH TOTALIZER. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Z

f (/ .. Before Calibration O <— if 

i s L 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments 

Performed by: jS>— 1 -^L^ Date: \h'2S'c>c\ Time: AM ^t) 

JB Place: -^—-^ 

CALSHEET.WDB fFieldJor Shop) 

VES018497 
ttyft<*m 

5404 Jadmed Ct. • St. Louis, MO 63123 

Business: (314) 845-7778 - Fax: (314) 845-7779 

Scal e Inspection Report 

Customer: ONYX ENVIRONMENTAL 

#7 MOBILE AVENUE 

SAUGET, IL 62201 

Location: Direct Injection 

M F G / Model: WI130 

Scale Type: VEHICLE 

Capacity: 60000LB 

escription: Class III L 

Serial No: 013121 

Scale No: 3 

Divisions: 5LB 

Scale was found in Tolerance: | [ yes 

Shift Test 

Sides/ Corners/ 

Sections 

Weights 

Applied 

Scale Reading 

(As found) 

Error (+/-) Tolerance 

Accept 

Scale Reading After 

Adjustment (As Left) 

Accept / 

Reject 

Section 1 21,000 lb 20,945 lb -55 lb +/- 20 lb 21,005 lb ACCEPT 

Section 2 21,000 lb 20,980 lb -20 lb +/- 20 lb 21,000 lb ACCEPT 

Section 3 21,000 lb 21,000 lb +0 lb +/- 20 lb 21,000 lb ACCEPT 

Section 4 21,000 lb 21,000 lb +0 lb +/- 20 lb 21,000 lb ACCEPT 

Section 5 21,000 lb 21,000 lb +0 lb +/- 20 lb 21,000 lb ACCEPT 

Section 6 21,000 ib 21,005 lb +5 ib +/- 20 lb 21,005 lb ACCEPT 

Buildup Weight Weights Applied Scale Reading 

(As found) 

Error (+/-) Tolerance 

Accept 

Scale Reading After 

Adjustment (As Left) 

Accept/ 

Reject 

Section 6 3,000 lb 3,005 lb +5 lb +/- 5 lb ACCEPT 

6,000 lb 6,005 lb +5 ib +/- 5 lb ACCEPT 

9,000 lb 9,005 lb +5 lb 10 lb ACCEPT 

12,000 lb 12,005 lb +5 lb +/- 10 lb ACCEPT 

15,000 lb 15,005 lb +5 lb +/- 15 lb ACCEPT 

18,000 lb 18,005 lb +5 lb +/- 20 lb ACCEPT 

Section 6 21,000 lb 21,005 lb +5 lb +/- 20 lb ACCEPT 

Test Procedure follows QSP009-001/002 NIST#: MO : 259883/253250 39598 OBS04-0268/03-0450 274998 

Rice Lake: 822/266926-02 822/272801-06 822/274081-06 

Comments/Environmental Conditions:Found broken foot insection 1, on closer inspection found the scale had 5 bad feet 

in scale. Installed 5 new cell and feet. ^/-^crt/rC —9 Ord-t Arr-~~ 

ty ~ ?;&LH 

Calibration Dates: JAN APR JU L OCT ' 

Cal Date: 11/12/2009 Next Cal due: 90 days 

Service Technician Registration #: 0152- IL' 

Calibrated By Service Technician: Alan Primo Job Queue*: LT217651 Report ID: 68961887 

Uncertainty of Measurement provided on request 

FOR CUSTOMER USE ONLY | 

Reviewed By; Date Reviewed. 

This document shall not be reproduced, except in ful,'without the appraval of Accurate Superior Scale Company.. 

PageloH ForniO3a,Rev15,08/1g/09 

VES018498 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Tas k IC4039) PAG E 1 OF 2 

OPERATIN G PARAMETER S P L C COIL BWCOI L PASS FAIL 

1 O C L T R V POSITION C a p Ope n 00791 00401 

2 O C L UPPE R CHAMBE R TEMP . <1794 for i MIN AV G 00867 00402 

3 O C L HI BT U #/HR MA X =>828#/HR 00964 00403 

4 O C L LOWE R CHAMBE R TEMP . <1590for1MINAV G 00869 00404 

5 O C L L O BT U #/HR MAX =.1822 #/HR 00966 00405 

6 O C L FLU E GA S HC L >100 PP M 1HR Rolling avg. 00871 00406 

7 O C L FLU E GA S C O >100PPM1H R Rolling avg. 00872 00407 

8 O C L FLU E GA S OPACITY =>30%for480Sea/Hr. 00873 00408 

9 O C L FLU E GA S OPACITY =>60% instantaneous 00874 00409 

10 O C L FLU E GA S FLO W RAT E >17,198 ACF M for >1 MIN. 00875 00410 

11 O C L HEA T INPU T =>16 MBTU/H R 00865 00411 

12 O C L CHLORIN E INPUT >217lbs/HR 00866 00412 

13 O C L SOLI D FEE D #/HR MA X =>1041 #/HR 00960 00413 

14 O C L UPPE R CHAMBE R TEMP . <1845 DEG F H R ROLLIN G AV G 00883 00414 

15 O C L SPECIALIT Y FEEDE D #/HR MA X =>508#/HR 00962 00415 

17 AWF C S D A OUTLE T TEMP . >500 deg . F 1MIN avg. 00887 00417 

18 AWF C B A G HOUS E DIFF.PR. DROP . =<2"WC O R =>10"WC 1MIN avg. 00889 00418 

19 AWF C FLU E GA S C O =>500 PP M 1MIN avg. 00890 00419 

2 0 AWF C FLU E GA S 0 2 =<3%1MINavg. 00892 00420 

21 AWF C FLU E GA S H C =>10PPM1MINavg . 00893 00421 

22 AWF C FLU E GA S HC L =>500 PP M 1MIN avg. 00894 00422 

2 3 AWF C FLU E GA S FLO W RAT E =>, 720 ACF M inst. 00895 00423 

AWF C FLU E GA S OPACITY =>10% 1MIN avg. 00897 00424 

i AWF C L O W CHAMBE R TEMP . <1617 deg . F 1H R rolling avg. 00882 00425 

26 AWF C LOWE R CHAMBE R PRES S =>-.1"wcfor 5 see s 00884 00426 

2 7 AWF C UPPE R CHAMBE R PRES S =>-.1" wefor 5 see s 00885 00427 

28 AWF C FAILE R O F PROCES S MONITOR LOS S O F SIGNA L 00864 00428 

2 9 AWF C ID FA N FAILUR E LOSS OF ID FAN M CONTACT OR VIB >5 MIN 00863 00429 

3 0 AWF C UC/L C TEMPS . TEMPERATUR E > 2400 DEG . F 01600 00430 

32 MWF C A L L WAST E FEE D OF F FRO M FIX W F SHUTDOWN MANUALLY FROM FIX 00680 00432 

3 5 MWF C FLU E GA S HC L =>50 PP M 1HR rolling avg. 00878 00435 

3 6 MWF C HEA T INPUT =>15.5 MBTU/H R anticipated 00880 00436 

3 7 MWF C CHLORIN E INPUT =>233 Ibs/HR 00881 00437 

38 MWF C E-STOP S orT/ C MODUL E E-STO P &T/ C MODUL E inactive 00899 00438 

3 9 MWF C FLU E GA S C O =>50 PP M 1H R rolling avg. 00891 00439 

4 0 MWF C ATOMIZE R HI-HI Vibration sw. >5 minutes 00862 00440 

41 SWF C SPEC . FEE D =>724#/HR EXCEEDE D 00963 00441 

"7* 

VES018499 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Task IC4039) PAG E 2 O F 2 

OPERATIN G PARAMETER S P L C COIL B W COIL PASS FAIL 

42 SWF C HIBTU =>2012#/HR EXCEEDE D 00965 00442 

43 SWF C LOBT U =>1993#/HR EXCEEDE D 00967 00443 

45 SWF C HIBTU (see note 1) LOS S O F SIGNA L 03019 00445 

46 SWF C LOBT U (see note 1) LOS S O F SIGNA L 03020 00446 

4 7 SWF C SPECIALITY FEE D LOS S O F SIGNA L 03021 00447 

48 MWF C NORTH & SOUT H IP S ALARM S FAILED COMMUNICATION' S TIME D out FO R BOT H 05703 00448 

50 MWF C NORT H S SOUT H IP S SERVER S FAILE D COMMUNICATION' S TIME D OU T FO R BOT H 05705 00450 

51 SWF C DIREC T INJEC T COMMO N ALAR M 03132 00451 

52 O P L Bag Leak Detection System (Tribo) 

65 O P L Pumpable 1 Hour Rolling Total OP L 08205 04113 

66 O P L Non-Pumpable 1 Hour Rolling Total OP L 08206 04114 

67 O P L Total waste 1 Hour Rolling Total OP L 08208 04115 

68 O P L C L 12 Hour Rolling Total OP L 08211 04116 

69 O P L Low Volatile 12 Hour Rolling Total OP L 08214 04117 

7 0 O P L Semi Volatile 12 Hour Rolling Total OP L 08216 04118 

71 O P L Mercuiy 12 Hour Rolling Total OP L 08218 04119 

72 O P L A s h 12 Hour Rolling Total OP L 08220 04120 

73 O P L P C C Temperature 1 Hour Rolling Average Lo w OP L 08222 04121 

74 O P L S C C Temperature 1 Hour Rolling Average Lo w OP L 08224 04122 

75 O P L S D A Outlet Temperature 1 Hour Rolling Average High OP L 08226 04123 

76 O P L Baghous e Differential Pressure 1 Minute Average Low OP L 08227 04124 

77 O P L Baghous e Differential Pressure 1 Minute Average High OP L 08228 04125 

O P L Stack HC L Corrected 1 Hour Rolling Average High OP L 08232 04126 

O P L Stack C O Corrected 1 Hour Rolling Average High OP L 08236 04127 

80 O P L Stack Flow 1 Hour Rolling Average High OP L 08244 04128 

81 O P L B T U 1 Hour Total OP L 08244 04129 

82 O P L Hit Cl/Hra Lime Flow 1 Minute Average High OP L 08251 04130 

83 AWF C Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 

84 WILL NO T ACCEP T SOLID CHARGE S >750 KBTU/L B 

85 (DO NORT H TAN K FARM , BIWEEKL Y CHECKS ) 

86 Hi/Dl Atomizing Air Low Pressure alarm (manual check) 

87 Lo/DI Atomizing Air Low Pressure alarm (manual check) 

88 Specialty Feede r Atomizing Air Low Pressure alarm (manual cheek) 

O C L CONDITIO N LIMIT 

AWF C =AUTOMATI C WAST E FEE D CUTOF F 

MWF C =MISC WAST E FEE D CUTOF F 

SWF C =SPECIFIC WAST E FEE D CUTOF F 

4

1 

~7~ 

~~7 

Comment s 

CHECKE D BY : f)Ul 0 J/ A . — DATE : 10 ~IH'-^ ^ TIME: /^S" " AM (PM]} 

P' 'ROVED : Jy^/2£-d-t3'^ J3'm PLACE : Control Room 

BIWEEKLY_ 3 

4/4/07 H K 

VES018500 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Tas k IC4039) PAG E 1 O F 2 

OPERATIN G PARAMETER S P L C COI L B W COIL PAS S 

1 O C L T R V POSITION C a p Open 00791 00401 

2 O C L UPPE R CHAMBE R TEMP . <1794 for 1MIN AV G 00867 00402 

3 O C L HI BT U #/HR MA X =>828#/HR 00964 00403 

4 O C L LOWE R CHAMBE R TEMP . <1590 for i MIN AV G 00869 00404 f 

5 O C L L O BT U #/HR MA X =.1822 #/HR 00966 00405 

6 O C L FLU E GA S HC L >100 PP M 1H R Roiling avg. 00871 00406 

7 O C L FLU E GA S C O >100PPM1H R Rolling avg. 00872 00407 

8 O C L FLU E GA S OPACIT Y =>30% for 480 Sea/Hr. 00873 00408 / 

9 O C L FLU E GA S OPACIT Y =>60% instantaneous 00874 00409 

.10 O C L FLU E GA S FLO W RAT E >17,198 ACF M for >1 MIN. 00875 00410 y 11. O C L HEA T INPUT =>16 MBTU/H R 00865 00411 S 

12 O C L CHLORIN E INPUT >217 Ibs/HR 00866 00412 

13 O C L SOU D FEE D #/HR MA X =>1041 #/HR 00960 00413 

14 O C L UPPE R CHAMBE R TEMP . <1845 DEG F H R ROLLIN G AV G 00883 00414 

15 O C L SPECIALITY FEEDE D #/HR MA X =>508#/HR 00962 00415 f 17 AWF C S D A OUTLE T TEMP . >500deg.F1MINavg . 00887 00417 s 18 AWF C B A G HOUS E DIFF.PR. DROP . =<2"WC O R =>10"WC 1MIN avg. 00889 00418 

19 AWF C FLU E GA S C O =>500PPM1MINavg . 00890 00419 

2 0 AWF C FLU E GA S 0 2 =<3% 1MIN avg. 00892 00420 

21 AWF C FLU E GA S H C =>10PPM1MINavg . 00893 00421 / 

22 AWF C FLU E GA S HC L =>500PP M 1 MIN avg. 00894 00422 

2 3 AWF C FLU E GA S FLO W RAT E =>, 720 ACF M inst. 00895 00423 

• M s AWF C FLU E GA S OPACIT Y =>10%1MINavg. 00897 00424 f 

AWF C L O W CHAMBE R TEMP . <1617 deg. F1H R rolling avg. 00882 00425 / 

Z6 AWF C LOWE R CHAMBE R PRES S =>-.1" wcfo r 5 sees 00884 00426 s 2 7 AWF C UPPE R CHAMBE R PRES S =>-.1"wcfor 5 sees 00885 00427 s 28 AWF C FAILER O F PROCES S MONITOR LOS S O F SIGNA L 00864 00428 

2 9 AWF C ID FA N FAILUR E LOS S O F ID FA N M CONTAC T O R VIB >5 MI N 00863 00429 •s 

30 AWF C UC/L C TEMPS . TEMPERATUR E > 2400 DEG . F 01600 00430 s 

32 MWF C A L L WAST E FEE D OF F FRO M FIX W F SHUTDOW N MANUALL Y FRO M FI X 00680 00432 s 35 MWF C FLU E GA S HC L =>50 PP M 1 H R rolling avg. 00878 00435 s 36 MWF C HEA T INPU T =>15.5 MBTU/H R anticipated 00880 00436 

37 MWF C CHLORIN E INPUT =>233 Ibs/HR 00881 00437 

38 MWF C E-STOP S or T/ C MODUL E E-STO P &T/ C MODUL E inactive 00899 00438 

3 9 MWF C FLU E GA S C O =>50 PP M 1 H R rolling avg. 00891 00439 s. 4 0 MWF C ATOMIZE R HI-HI Vibration sw. >5 minutes 00862 00440 

41 SWF C SPEC.FEE D =>724#/HR EXCEEDE D 00963 00441 / 

VES018501 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Tas k IC4039) PAG E 2 O F 2 

OPERATIN G PARAMETER S P L C COIL B W COIL 

42 SWF C HIBTU =>2012#/HR EXCEEDE D 00965 00442 

43 SWF C LOBT U =>1993#/HR EXCEEDE D 00967 00443 

45 SWF C HIBTU (see note 1) LOS S O F SIGNA L 03019 00445 

46 SWF C LOBT U (see note 1) LOS S O F SIGNA L 03020 00446 

47 SWF C SPECIALITY FEE D LOS S O F SIGNA L 03021 00447 

48 MWF C NORTH & SOUTH IPS ALARM S FAILE D COMMUNICATION' S TIME D our FO R BOT H 05703 00448 

50 MWF C NORT H S SOUT H IP S SERVER S FAILE D COMMUNICATION' S TIME D OU T FO R BOT H 05705 00450 

51 SWF C DIREC T INJEC T COMMO N ALAR M 03132 00451 

52 O P L B ag Leak Detection System (Tribo) 

65 O P L Pumpable 1 Hour Rolling Total OP L 08205 04113 

66 O P L Non-Pumpable 1 Hour Rolling Total OP L 08206 04114 

67 O P L Total waste 1 Hour Rolling Total OP L 08208 04115 

68 O P L C L 12 Hour Rolling Total OP L 08211 04116 

69 O P L Low Volatile 12 Hour Rolling Total OP L 08214 04117 

70 O P L Semi. Volatile 12 Hour Rolling Total OP L 08216 04118 

71 O P L Mercuiy 12 Hour Rolling Total OP L 08218 04119 

72 O P L A s h 12 Hour Rolling Total OP L 08220 04120 

73 O P L P C C Temperature 1 Hour Rolling Average Low OP L 08222 04121 

74 O P L S C C Temperature 1 Hour Rolling Average Low OP L 08224 04122 

75 O P L S D A Outlet Temperature 1 Hour Rolling Average High OP L 08226 04123 

76 O P L Baghouse Differential Pressure 1 Minute Average Low OP L 08227 04124 

77 O P L Baghouse Differential Pressure 1 Minute Average High OP L 08228 04125 

•7.6. O P L Stack HC L Corrected 1 Hour Roiling Average High OP L 08232 04126 

O P L Stack C O Corrected 1 Hour Rolling Average High OP L 08236 04127 

80 O P L Stack Flow 1 Hour Rolling Average High OP L 08244 04128 

81 O P L B T U 1 Hour Total OP L 08244 04129 

82 O P L Hit Cl/Hra Lime Flow 1 Minute Average High OP L 08251 04130 

83 AWF C Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 

84 WILL NO T ACCEP T SOLI D CHARGE S >750 KBTU/L B 

85 (DO NORT H TAN K FARM , BIWEEKL Y CHECKS ) 

86 Hi/DI Atomizing Air Low Pressure alarm (manual check) 

87 Lo/DI Atomizing Air Low Pressure alarm (manual check) 

88 Specialty Feeder Atomizing Air Low Pressure alarm (manual cheek) 

O C L CONDITIO N LIMIT 

AWF C =AUTOMATIC WAST E FEE D CUTOF F 

MWF C =MISC WAST E FEE D CUTOF F 

SWF C =SPECIFIC WAST E FEE D CUTOF F 

PAS S FAIL 

4-

y 

y 

y 

y y 

~y~ 

~7~ 

y 

y 

y 

y 

~7~ 

y 

7 

~7~ 

y 

~y~ 

~y 

X l 

Comments 

CHECKE D BY : 

A

-

"'QVED : 

DATE : tD-Zert><t TIME : 3)*t~? C^T > M 

PLACE : Control Roo m 

BIWEEKLY_ 3 

4/4/07 H K 

VES018502 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Tas k IC4039) PAG E 1 O F 2 

OPERATIN G PARAMETER S P L C COI L B W COIL PAS S FAIL 

1 O C L T R V POSITION C a p Ope n 00791 00401 

2 O C L UPPE R CHAMBE R TEMP . <1794 for i MIN AV G 00867 00402 

3 O C L HI BT U #/HR MA X =>828#/HR 00964 00403 

4 O C L LOWE R CHAMBE R TEMP . <1590for1MINAV G 00869 00404 

5 O C L L O BT U #/HR MA X = 1822 #/HR 00966 00405 

6 O C L FLU E GA S HC L >100 PP M 1H R Rolling avg. 00871 00406 

7 O C L FLU E GA S C O >100 PP M 1H R Rolling avg. 00872 00407 

8 O C L FLU E GA S OPACIT Y =>30%for480Sec7Hr. 00873 00408 

9 O C L FLU E GA S OPACIT Y =>60% instantaneous 00874 00409 

10 O C L FLU E GA S FLO W RAT E >17,198 ACF M for >1 MIN. 00875 00410 

11 O C L HEA T INPUT =>16 MBTU/H R 00865 00411 

12 O C L CHLORIN E INPUT >217 Ibs/HR 00866 00412 

13 O C L SOLID FEE D #/HR MA X =>1041 #/HR 00960 00413 

14 O C L UPPE R CHAMBE R TEMP . <1845 DEG F H R ROLLING AV G 00883 00414 

1 5 O C L SPECIALITY FEEDE D #/HR MA X =>508#/HR 00962 00415 

17 AWF C S D A OUTLE T TEMP . >500 deg. F1MI N avg. 00887 00417 

18 AWF C B A G HOUS E DIFF.PR. DROP . =<2"WC O R =>10"WC 1MIN avg. 00889 00418 

19 AWF C FLU E OA S C O =>500 PP M 1MIN avg. 00890 00419 

2 0 AWF C FLU E GA S 0 2 =<3% 1MIN avg. 00892 00420 

21 AWF C FLU E GA S H C =>10PPM1MINavg . 00893 00421 

22 AWF C FLU E GA S HC L =>500 PP M 1MIN avg. 00894 00422 

2 3 AWF C FLU E GA S FLO W RAT E =>, 720 ACF M inst. 00895 00423 

AWF C FLU E GA S OPACIT Y =>10%1MlNavg. 00897 00424 

AWF C L O W CHAMBE R TEMP . . <1617 deg . F1H R rolling avg. 00882 00425 

26 AWF C LOWE R CHAMBE R PRES S =>-.1"wcfor 5 sees 00884 00426 

27 AWF C UPPE R CHAMBE R PRES S =>-.1"wcfor 5 sees 00885 00427 

28 AWF C FAILE R O F PROCES S MONITOR LOS S O F SIGNA L 00864 00428 

2 9 AWF C ID FA N FAILUR E LOS S O F ID FA N M CONTAC T O R VIB >5 MIN 00863 00429 

30 AWF C UC/L C TEMPS . TEMPERATUR E > 2400 DEG . F 01600 00430 

32 MWF C A L L WAST E FEE D OF F FRO M FIX WF SHUTDOWN MANUALLY FROM FIX 00680 00432 

35 MWF C FLU E GA S HC L =>50 PP M 1H R rolling avg. 00878 00435 

36 MWF C HEA T INPUT =>15.5 MBTU/H R anticipated 00880 00436 

37 MWF C CHLORIN E INPUT =>233 Ibs/HR 00881 00437 

38 MWF C E-STOP S or T/ C MODUL E E-STO P & T/ C MODUL E inactive 00899 00438 

39 MWF C FLU E GA S C O =>50 PP M 1H R rolling avg. 00891 00439 

4 0 MWF C ATOMIZE R HI-HI Vibration sw. >5 minutes 00862 00440 

41 SWF C SPEC . FEE D =>724#/HR EXCEEDE D 00963 00441 

~Z1 

2 1 

~7 

1 

VES018503 
1 

BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

issssssBXBaBBMBnaBBBBiaassaeeaasssaspseess 

OPERATIN G PARAMETER S 

(CM S Tas k IC4039) PAG E 2 OF 2 

P L C COIL BWCOI L PAS S FAIL 

42 SWF C HIBTU =>2012#/HR EXCEEDE D 00965 00442 

43 SWF C LOBT U =>1993f7VHR EXCEEDE D 00967 00443 

45 SWF C HIBTU (see note 1) LOS S O F SIGNA L 03019 00445 

46 SWF C LOBT U (see note 1) LOS S O F SIGNA L 03020 00446 

47 SWF C SPECIALITY FEE D LOS S O F SIGNA L 03021 00447 

48 MWF C NORTH & SOUTH IPS ALARMS FAILED COMMUNICATION' S TIME D OU T FO R BOT H 05703 00448 

50 MWF C NORTH S SOUTH IPS SERVERS FAILED COMMUNICATION' S TIME D OU T FO R BOT H 05705 00450 

51 SWF C DIREC T INJEC T COMMO N ALAR M 03132 00451 

52 O P L B a g Leak Detection System (Tribo) 

65 O P L Pumpable 1 Hour Rolling Total OP L 08205 04113 

66 O P L Non-Pumpable 1 Hour Rolling Total OP L 08206 04114 

67 O P L Total waste 1 Hour Rolling Total OP L 08208 04115 

68 O P L C L 12 Hour Rolling Total OP L 08211 04116 

69 O P L Low Volatile 12 Hour Rolling Total OP L 08214 04117 

70 O P L Semi. Volatile 12 Hour Rolling Total OP L 08216 04118 

71 O P L Mercury 12 Hour Rolling Total OP L 08218 04119 

72 O P L A s h 12 Hour Rolling Total OP L 08220 04120 

73 O P L P C C Temperature 1 Hour Rolling Average Lo w OP L 08222 04121 

74 O P L S C C Temperature 1 Hour Rolling Average Lo w OP L 08224 04122 

75 O P L S D A Outlet Temperature 1 Hour Rolling Average High OP L 08226 04123 

76 O P L Baghous e Differential Pressure 1 Minute Averag e Lo w OP L 08227 04124 

77 O P L Baghous e Differential Pressure 1 Minute Averag e High OP L 08228 04125 

O P L Stack HC L Corrected 1 Hour Rolling Averag e High OP L 08232 04126 

1

 OP L Stack C O Corrected 1 Hour Rolling Average High OP L 08236 04127 

SO O P L Stack Flow 1 Hour Rolling Average High OP L 08244 04128 

81 O P L B T U 1 Hour Total OP L 08244 04129 

82 O P L Hrt Cl/Hra Lime Flow 1 Minute Average High OP L 08251 04130 

83 AWF C Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 

84 WILL NO T ACCEP T SOLID CHARGE S >750 KBTU/L B 

85 (DO NORT H TAN K FARM , BIWEEKL Y CHECKS ) 

86 Hi/DI Atomizing Air Low Pressure alarm (manual check) 

87 Lo/DI Atomizing Air Low Pressure alarm (manual check) 

88 Specialty Feeder Atomizing Air Low Pressure alarm (manual cheek) 

O C L =CONDITION LIMIT 

AWF C =AUTOMATI C WAST E FEE D CUTOF F 

MWF C =MISC WAST E FEE D CUTOF F 

SWF C =SPECIFIC WAST E FEE D CUTOF F 

Comments 

ZZ1 

x~~ 

X ^ 

X " 

X 

X ^ 

-7-

7^ 

ITS' 

X l 

CHECKE D B Y 

AMOVE D : /h i 

BiWEEKLY_ 3 

4/4/07 H K 

DATE : \\'ZS"0Ci TIME : <R)2^ QjypB M 

PLACE : Control Roo m 

VES018504 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Task IC4039) PAG E 1 O F 2 

OPERATIN G PARAMETER S P L C COIL BWCOI L PAS S FAIL 

1 O C L T R V POSITION C a p Ope n 00791 00401 

2 O C L UPPE R CHAMBE R TEMP . <1794 for i MIN AV G 00867 00402 

3 O C L HI BT U #/HR MA X =>828#/HR 00964 00403 

4 O C L LOWE R CHAMBE R TEMP . <1590 for i MIN AV G 00869 00404 

5 O C L L O BT U #/HR MA X = 1822 #/HR 00966 00405 

6 O C L FLU E GA S HC L >100PPM1H R Rolling avg. 00871 00406 

7 O C L FLU E GA S C O >100PPM1H R Rolling avg. 00872 00407 

8 O C L FLU E GA S OPACIT Y =>30%for480Sec/Hr. 00873 00408 

9 O C L FLU E GA S OPACIT Y =>60% instantaneous 00874 00409 

10 O C L FLU E GA S FLO W RAT E >17,198 ACF M for >1 MIN. 00875 00410 

11 O C L HEA T INPUT =>16 MBTU/H R 00865 00411 

12 O C L CHLORIN E INPUT >217 Ibs/HR 00866 00412 

13 O C L SOLI D FEE D #/HR MA X =>1041 #/HR 00960 00413 

14 O C L UPPE R CHAMBE R TEMP . <1845 DEG F H R ROLLIN G AV G 00883 00414 

15 O C L SPECIALIT Y FEEDE D #/HR MA X =>508 #/HR 00962 00415 

17 AWF C S D A OUTLE T TEMP . >500deg. F 1MIN avg. 00887 00417 

18 AWF C B A G HOUS E DIFF.PR. DROP . =<2"WC O R =>10"WC 1MIN avg. 00889 00418 

19 AWF C FLU E GA S C O =>500 PP M 1MIN avg. 00890 00419 

2 0 AWF C FLU E GA S 0 2 =<3% 1MIN avg. 00892 00420 

21 AWF C FLU E GA S H C =>10PPM1MINavg . 00893 00421 

22 AWF C FLU E GA S HC L =>500 PP M 1MIN avg. 00894 00422 

2 3 AWF C FLU E GA S FLO W RAT E =>, 720 ACF M inst. 00895 00423 

r M AWF C FLU E GA S OPACIT Y =>10%1MINavg. 00897 00424 

AWF C L O W CHAMBE R TEMP . <1617 deg . F1H R rolling avg. 00882 00425 

^6 AWF C LOWE R CHAMBE R PRES S =>-.1" wcfo r 5 see s 00884 00426 

2 7 AWF C UPPE R CHAMBE R PRES S =>-.1" wefo r 5 see s 00885 00427 

28 AWF C FAILE R O F PROCES S MONITO R LOS S O F SIGNA L 00864 00428 

29 AWF C ID FA N FAILUR E LOS S O F ID FA N M CONTAC T O R VIB >S MIN 00863 00429 

3 0 AWF C UC/L C TEMPS . TEMPERATUR E > 2400 DEG . F 01600 00430 

32 MWF C A L L WAST E FEE D OF F FRO M FIX WF SHUTDOWN MANUALLY FROM F K 00680 00432 

3 5 MWF C FLU E GA S HC L =>50 PP M 1H R rolling avg. 00878 00435 

36 MWF C HEA T INPUT =>15.5 MBTU/H R anticipated 00880 00436 

3 7 MWF C CHLORIN E INPUT =>233 Ibs/HR 00881 00437 

38 MWF C E-STOP S or T/ C MODUL E E-STO P & T/ C MODUL E inactive 00399 00438 

39 MWF C FLU E GA S C O =>50 PP M 1H R rolling avg. 00891 00439 

4 0 MWF C ATOMIZE R HI-HI Vibration sw. >5 minutes 00862 00440 

41 SWF C SPEC . FEE D =>724#/HR EXCEEDE D 00963 00441 

I 

t»y p 

-

\// _ 

%• 

^ 4 -

3k\ 

VES018505 
BIWEEKL Y UNIT #3 

COMPLIANC E CHEC K SHEE T 

(CM S Task IC4039) PAG E 2 O F 2 

OPERATIN G PARAMETER S P L C COIL BWCOI L PAS S FAIL 

42 SWF C HIBTU =>2012*fHR EXCEEDE D 00965 00442 

43 SWF C LOBT U =>1993#/HR EXCEEDE D 00967 00443 

45 SWF C HIBTU (see note 1) LOS S O F SIGNA L 03019 00445 t X 

4 6 SWF C LOBT U (see note 1) LOS S O F SIGNA L 03020 00446 c x 

47 SWF C SPECIALITY FEE D LOS S O F SIGNA L 03021 00447 u. 

48 MWF C NORTH & SOUT H IPS ALARMS FAILED COMMUNICATION' S TIME D OU T FO R BOT H 05703 00448 i / 

5 0 MWF C NORT H & SOUT H IP S SERVER S FAILE D COMMUNICATION' S TIME D OU T FO R BOT H 05705 00450 L X 

51 SWF C DIREC T INJEC T COMMO N ALAR M 03132 00451 X ' 

52 O P L B a g Leak Detection System (Tribo) \ ^ 

65 O P L Pumpable 1 Hour Rolling Total OP L 08205 04113 I X 

66 O P L Non-Pumpable 1 Hour Rolling Total OP L 08206 04114 

67 O P L Total waste 1 Hour Rolling Total OP L 08208 04115 i x 

68 O P L C L 12 Hour Rolling Total OP L 08211 04116 ( X 

69 O P L Low Volatile 12 Hour Rolling Total OP L 08214 04117 / X 

70 O P L Semi Volatile 12 Hour Rolling Total OP L 08216 04118 

71 O P L Mercury 12 Hour Rolling Total OP L 08218 04119 !v 

72 O P L A s h 12 Hour Rolling Total OP L 08220 04120 L X 

73 O P L P C C Temperature 1 Hour Rolling Average Low OP L 08222 04121 i ^ X 

74 O P L S C C Temperature 1 Hour Rolling Average Low OP L 08224 04122 X f 

75 O P L S D A Outlet Temperature 1 Hour Rolling Average High OP L 08226 04123 X 

76 O P L Baghous e Differential Pressure 1 Minute Average Low OP L 08227 04124 

. X 

7 7 O P L Baghous e Differential Pressure 1 Minute Average High OP L 08228 04125 l X . 

—*v O P L Stack HC L Corrected 1 Hour Rolling Average High OP L 08232 04126 X 

O P L Stack C O Corrected 1 Hour Rolling Average High OP L 08236 04127 x " 

80 O P L Stack Flow 1 Hour Rolling Average High OP L 08244 04128 

x S 

81 O P L B T U 1 Hour Total OP L 08244 04129 X 

82 O P L Hit Cl/Hra Lime Flow 1 Minute Average High OP L 08251 04130 X 

83 AWF C Lime Slurry Density 1 Hour Rolling Average Lo w 08156 04132 X 

84 WILL NO T ACCEP T SOLID CHARGE S >750 KBTU/L B K> 

85 (DO NORT H TAN K FARM , BIWEEKL Y CHECKS ) X 

86 Hi/DI Atomizing Air Low Pressure alarm (manual check) x > 

87 Lo/DI Atomizing Air Low Pressure alarm (manual check) X 

88 Spedalty Feeder Atomizing Air Low Pressure alarm (manual cheek) 

O C L 

AWF C 

MWF C 

SWF C 

CONDITIO N LIMIT 

=AUTOMATI C WAST E FEE D CUTOF F 

=MISC WAST E FEE D CUTOF F 

=SPEC1FIC WAST E FEE D CUTOF F 

Comments

 < 5fo U &f[fejZ 1 O/Xvi fi?Q (^- ^ 

CHECKE D B Y 

••OVED : //a+Lo*. /<>% 

DATE : //-7 '/" O 9 TIME : 5 ? 3 

PLACE : Control Roo m 

M 

BIWEEKLY_ 3 

4/4/07 H K 

VES018506 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit# Serial # COSA 

Parameter NIST Traceable Calibration Standards 

> 0 2 25 % G a s Concentration 

<~ CO-lo w range 200pp m Low (Zero) 0 ± 0.5 

r CO-high range 3000ppm Mid 8.93 ± 0.5 

r HCI 1000ppm High 15 ± 0.5 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0.2 -0.2 — — 

2-Mid 8.93 8.88 — 0.05 — 

3-High 15 15.1 — — -0.1 

4-Low 0 0.2 -0.2 — — 

5-Mid 8.93 8.83 — 0.1 — 

6-High 15 15.1 — — -0.1 

7-Low 0 0.2 -0.2 — — 

8-Mid 8.93 8.83 — 0.1 — 

9-High 15 15 — — 0 

Mean Difference = -0.20 0.08 -0.07 

Calibration Error = -0.80% 0.33% -0.27% 

Calibration Error = Mean Difference / Span Value * 100 

Bill Adams E/l Tech 

Name Title 

9/23/2009 

Signature 

2/4/2010 

Date 

VESO18507 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit # 3 Serial # 

Parameter NIST Traceable Calibration Standards 

r 0 2 25 % G a s Concentration 

CO-low range 200pp m Low (Zero) 0 ± 10 

r CO-high range 3000ppm Mid 68.9 + 10 

r HCI 1000pp m High 152 ± 10 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0.8 -0.8 — — 

2-Mid 68.9 73.3 — 4.4 — 

3-High 152 152.9 — — -0.9 

4-Low 0 1 -1 — — 

5-Mid . 68.9 72.1 — -3.2 — 

6-High 152 148.3 — — 3.7 

7-Low 0 -0,3 0.3 — — 

8-Mid 68.9 71.6 — -2.7 — 

9-High 152 148.1 — _ 3.9 

Mean Difference = -0.50 -3.43 2.23 

Calibration Error = -0.25% -1.72% 1,12% 

Calibration Error = Mean Difference / Span Value * 100 

Bill Adams 

Name 

Signature 

VES018508 

E/l Tech 

Title 

9/23/2009 

Date 

2/4/2010 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit#

 3 Serial # 

Parameter NIST Traceable Calibration Standards 

r 0 2 25 % G a s Concentration 

r CO-low range 200ppm Low (Zero) . 0 + 150 

e CO-high range 3000ppm Mid 1079.1 + 150 

r HCI 1000pp m High 2285 ± 150 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0.8 -0.8 — — 

2-Mid 1079.1 1127.1 — 4 8 — 

3-High 2285 2287.5 — — -2.5 

4-Low 0 0.9 -0.9 — — 

5-Mid . 1079.1 1081.6 — -2.5 — 

6-High 2285 2265.1 _ _ 19.9 

7-Low 0 -0.3 0.3 — — 

8-Mid 1079.1 1076.1 — 3 — 

9-High 2285 2252.4 — — 32.6 

Mean Difference = -0.47 -15.83 16.67 

Calibration Error = -0.02% -0.53% 0.56% 

Calibration Error = = Mean Difference / Span Value * 100 

Bill Adams E/ITEC H 

Name Title 

9/23/2009 

Signature 

2/4/2010 

Date 

VES018509 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit#

 3 Serial # 

Parameter NIST Traceable Calibration Standards 

r 0 2 25 % G a s Concentration 

f* CO-lo w range 200ppm Low (Zero) 0 ± 50 

r CO-high range 3000ppm Mid 318 + 50 

HCI 1000pp m High 730 + 50 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0.8 -0.8 — — 

2-Mid 318 326.8 — -8.8 — 

3-High 730 742.9 — — -12.9 . 

4-Low 0 0.9 -0.9 — _ 

5-Mid 318 345.2 — -27.2 — 

6-High 730 737.9 — — -7.9 

7-Low 0 -0.3 0.3 — — 

8-Mid 318 353.1 — -35.1 — 

9-High 730 737.1 — 

— -7.1 

Mean Difference = -0.47 -23.70 -9.30 

Calibration Error = -0.05% -2.37% -0.93% 

Calibration Error = Mean Difference / Span Value * 100 

Bill Adams 

Name 

Signature 

E/ITech 

Title 

9/23/2009 

Date 

2/4/2010 

VES018510 
Tabl e 1 

Summar y o f Relativ e Accurac y Tes t Audi t Result s 

Veoli a E S Technica l Solution s 

Sauget , Illinoi s 

Jun e 22,2 3 an d 24,200 9 

CEM S Paramete r Unit s Measure d R A Criteri a Pass/Fa U 

Unit 2 CO ppm @ 7% 02 0.004 ppma Unit 2 5a,b Pass 

Oz , dry %o2 0.09%a 1.0

 a

'

c Pass 

Unit 2 

02, wet 0.13%2 1.0a>c Pass 

Unit 3 CO ppm @ 7% 02 0.063 ppma Unit 3 5a,b Pass 

02, dry %o2 0.02%a 1.0a,c Pass 

Unit 3 

02, wet %o2 0.31%a 1.0

 a

'

c Pass 

Unit 4 CO ppm @ 7% 02 1.146 ppma Unit 4 5a,b Pass 

02,dry %o2 0.15%8 1.0

 a

'

c Pass 

Unit 4 

02, wet %o2 t 0.46%a 1.0a,c Pass 

a

 Percent of emission standard or absolute average difference (ppm or %). 

b

PS4B. 

C

PS3. 

INCINERATOR CEMS RATA 

"VEOLIA ES 

JULY 7, 2009 

CEC Project 090-861 

VES018511 
Incinerator 

Data Point 

Veolia 

Environmental Services 

Sauget Illinois 

Created 

Period Start 

Period E n 

1/1/2010 6:00 A M 

1/1/2010 6:00 A M 

1/1/2010 6:00 A M 

Page 3 of 7 

1 Mi n 1 Mi n 

A V G AV G 

Warn Shut 

IMi n 1 H r Roll 1 H r Roll I H r Roll I H r Roll 1 H r Roll 1 Hr Roll 12 H r 12 H r i2 H r 1 HrTo t lHrTo t 1 Hr Tot 

A V G Warn Shut OP L Tot Tot Shut Tot OP L Roll Tot Roll Tot RoUTo t Warn Shut OP L 

O P L Warn Warn Shut OP L 

Thermodynami c BT U 

HCLtoLim e 

Stack C O Corrected 

LimeSlurryDensity 

Stack HC L Corrected 

Stack HC L RCR A 

Stack 0 2 Corrected 

Stack 0 2 Ra w 

Stac k Opacity 

Stack Flo w 

S D A Outlet Tem p 

25.00000 28.00000 33.50000 

450.0000 500.0000 

67.50000 0.000000 

450.0000 500.0000 

450.0000 500.0000 

4.000000 

4.000000 3.000000 

8.000000 10.00000 

15000.00 

430.0000 500.0000 

Baghous e Diff Pres s Lo w 3.000000 2.000000 

Baghous e Diff Pres s High 9.000000 10.00000 

30.00000 75.00000 100.0000 

67.50000 67.30000 67.00000 

25.00000 32.00000 

20.00000 25.00000 100.0000 

14600.00 14950.00 15147.00 

417.0000 418.0000 420.0000 

15.00000 15.50000 16.00000 

VES018512 
Stac k TH C 

L o w BT U Weight 

Specia l Fee d Weight 

High BT U Weight 

Solids Weight 

P C C Tem p 

S C C Tem p 

Stack C O RCR A 

Liquid Weight 

Weight 

Chlorine 

Mercury 

A s h 

L o w Volatile 

Sem i Volatile 

8.000000 10.00000 

1750.000 1590.000 

1860.000 1794.000 

450.0000 500.0000 

Veolia 

Environmental Services 

Sauget Illinois 

1000.000 1020.000 1053.000 

1775.000 1742.000 1734.000 

1880.000 1854.000 1849.000 

50.00000 90.00000 100.0000 

2850.000 2950.000 3107.000 

3750.000 3850.000 4017.000 

200.0000 218.0000 

0.003000 0.003400 

625.0000 673.0000 

40.00000 46.00000 

Created 

Period Start 

Period En 

1/1/2010 6:00 A M 

1/1/2010 6:00 A M 

1/1/2010 6:00 A M 

Page 4 of 7 

. 1900.000 1933.000 1993.000 

. 600.0000 664.0000 724.0000 

. 1900.000 1952.000 2012.000 

. 1000.000 1020.000 1053.000 

. 2400.000 2500.000 2616.000 200,0000 217.0000 233.0000 

. 0.030000 0.034000 0.040800 . 

. 7500.000 8000.000 8076.000 

. 500.0000 530.0000 552.0000 

56.00000 63.00000 . 700.0000 730.0000 756.0000 

VES018513 
Facility Oxygen Data 

VES018514 
December, 2009 Average Oxygen Concentrations for Units 2, 3, and 4 

Unit 2 Method 5/26 Method 0023A 

Date Wet 02 Dry 02 Wet 02 Dry 02 

(%) (%) (%) (%) 

12/8/2009 5.6 10.3 4.8 9.1 

12/9/2009 5.8 10.4 5.1 9.3 

12/10/2009 , 5.1 9.3 4.3 8.2 

Unit 3 Method 5/26 Method 0023A 

Date Wet 02 Dry 02 Wet 02 Dry 02 

(%) (%) (%) (%) 

12/1/2009 5.7 9.5 4.0 7.3 

12/2/2009 4.5 7.8 4.1 7.3 

12/3/2009 6.2 10.4 5.6 9.5 

Unit 4 Method 5/26 Method 0023A 

Date Wet 02 Dry 02 Wet 02 Dry 02 

(%) (%) (%) (%) 

12/16/2009 8.6 12.7 7.7 12.6 

12/17/2009 7.9 12.5 8.0 12.4 

12/18/2009 7.3 12.6 6.9 12.3 
rjo 

I 

VES018516 
AECOM 

Appendix B 

Reference Method Field Data and Calculations 
Method 5/26A 

VES018518 
Results Summary 

Unit 3 

Veolia ES Technical Solutions 

Sauget, IL 

Run 1 Run 2 Run 3 Averaqe 

Parameter: Molecular (Total mg)'mg/dscm; (ppm@ (IWhr) (Total mg)'mg/dscm} (ppm® (Ib/hr) (Total mgj'mg/dscm; (ppm® (Ib/hr) (mg/dscm) (ppm® (Ib/hr) 

Weight 7%02) 7%02) 7%02) . 75402; 

HCI I 36,46 | I 14-1 I 13,1 10.5 0.25 I 14.8 I 13.7 9.6 0.25 I 27.4 I 24.4 21.3 0.51 17.1 13.8 0.34 

CL2 I 70.9 I I 0.49 I 0.46 0.17 0.009 I 0.48 I 0.4 0.2 0.01 I OSS I 0.49 0.18 0.010 0.46 0.18 0.01 

Total 10.7 9.8 21.5 14.0 

Where: 

Total fti8=T«W sajniae qolte|!te4mi)ligrarriB 

mgfdKni <= milBgraqia^jWiMfaMlSerdiy a(a«ai»iSutiii;mei9r= (rtgfdsd^X (33 3t4 CuWcfee»/eut)|e;roetBt> ; 

pfimH @ =4>affe 0*r million at rsioxyget^f^/ascnl ^ 04 BsrSWQlJteK>JWt>)'((?G,9-tS7(2lJ-.9.D?%)) ; 

VES018519 
Particulate Results Summary 

Unit 3 

Veolia ES Technical Solutions 

Sauget, IL 

Tes t Results : Run l Run 2 Run 3 Averaqe 

Particulate Emission Concentration: 

grains/dscf 0.00138 0.00145 0.00121 0.00135 

grains/dscf@ 7% 02 0.00169 0.00154 0.00160 0.00161 

Particulate Emission Concentration' 
Calculations Summary 

Unit 3 

Veolia ES Technical Solutions 

Sauget, IL 

Vw(std), scf = 

Vm(std), dscf = 

Bws= 

Md= 

Ms= 

Vs, ft/sec = 

Qs, acfm = 

Qs(std), dscfm = 

Isokinetic Sampling Rate, % 

Run 1 

29.085 

37.954 

0.434 

29.71 

24.63 

28.5 

14,187 

5,039 

102.8 

Run 2 

33.829 

38.247 

0.469 

29.91 

24.32 

29.8 

14,817 

4,874 

107.1 

Run 3 

28.859 

39.664 

0.421 

29.69 

24.77 

30.8 

15,340 

5,573 

97.2 

Averaqe 

30.591 

38,622 

0.441 

29.77 

24.57 

29.7 

14,781 

5,162 

102.4 

Vwr,std> s volume of water vapor in gas, standard conditions =; 0.Q47O7*Vlc 

Vra(std) =vol of gas sampled, standard conditions = 77:647 x Vrti xo,arnm& xfPb + (dH/l36)]/Tm<R) 

Bws water vapor jn^as stream, proportion hy Volume * Vw(sld)/{Vmtstd) + Vv^std}) 

Md = moteeUiar weight of stackers, dry basis =* (0 44x%CQ2) + (0.32 X%02) + [&28 x (%N2+ %CO)j 

Ms <= moiecuiar weight of staek gas, wet basis = [Me* x Cl-Bws)) + (15C x Bws) 

[Vs= stacks as vfctocity <= 65 49 X Cp x (aVg. Sq Rt. dP) x(Sq.Rt. (Ts(R»/[Ms X Ps)j 

Qs * stacK gas flow rate « Vs x As x 6Q 

|-Qs(5td) - stacH gas flow rate,-standard conditions = Qs x (1-Bws) x (528/tl%<R)>x (ps/2$.92) 

isokinetic sampling rate * {(Tsfft)) x[<0.boZ67x Vic) *• 0/m(sitfj/l7.647)] x 1<wnma xvs x ?&* An x60) 

VES018521 
Test Data Summary 

Unit 3 

Veolia ES Technical Solutions 

Sauget, IL 

Parameter 

Run Date 

Start Time 

Stop Time 

Duration of Run, Minutes 

Ave. Nozzle Diameter, inches 

Pitot Calibration Factor, C F 

Meter Gamma 

Meter Delta H, inches of H20 

Stack Diameter, inches 

Rectangular Width, inches 

Rectangular Length, inches 

Stack Area, sq.ft. 

Barometric Pressure, inches of Hg 

Static Pressure, inches of H20 

Drv Gas Meter Sample Volume. (VMW3 

Initial 

Final 

Difference 

Run 1 

12/01/09 

11:16 

12:21 

60 

0.431 

0.84 

0.991 

1.801 

39 

8.30 

29.75 

0.07 

597.095 

635.422 

38.327 

Run 2 

12/02/09 

10:05 

11:09 

60 

0.431 

0.84 

0.991 

1.801 

39 

8.30 

29.4 

-0.1 

746.362 

784.532 

38.17 

Run 3 

12/03/09 

10:48 

11:51 

60 

0.431 

0.84 

0.991 

1.801 

39 

8.30 

29.8 

-0.13 

897.579 

936.804 

39.225 

Ave. Stack Temperature, Ts(F) 

Ave. Meter Temperature, Tm(F) 

Ave. Run Delta H, inches of H20 

Ave. Square Root of Delta P 

376.9 

67.2 

1.37 

0.3714 

376.8 

54.8 

1.34 

0.3832 

377.7 

57.2 

1.44 

0.4028 

Moisture Data 

Volume of water collected, mis 

Silica Gel, grams 

Total Collected, mis 

610 

7.9 

617.9 

710 

8.7 

718.7 

605 

8.1 

613.1 

ORSAT Data 

%02 

%C02 

% C O 

9.5 

8.3 

7.8 

10.0 

10.4 

8.0 

VES018522 
Field Data Summary 

Unit 3 

Veolia ES Technical Solutions 

Sauget, IL 

Stack 

Temp(F) 

Delta 

P 

Delta 

H 

TmtF) SQRT 

Delta P 

Start 

TemplF) 

Delia P Delta 

H 

TmtF) soror| 

Delta P 

Stack 

TemplF) 

Delta 

P 

Delta 

H 

Tm(f) SORT 

Dalta P 

Stack 

Temp(F) 

Delta 

P 

Delta 

H In out 

SQRT 

Delta P 

Start 

TemplF) 

Delia P Delta 

H In out 

soror| 

Delta P 

Stack 

TemplF) 

Delta 

P 

Delta 

H in out 

SORT 

Dalta P 

374 0.16 1.54 60 63 0.400C 377 0.15 1.35 50 53 0.3873 !: 378 0.17 1.50 51 54 0.4123 378 0.17 1.63 60 63 0.4123 378 0.18 1.60 50 57 0.4243 :• 380 0.18 1.60 51 57 0.4243 

379 013 1.73 61 65 0.4243 378 0.14 1.30 50 58 0.3742 :• •:• 380 0.17 1.50 51 60 0.4123 

379 0.17 1.63 61 67 0.4123 330 0.14 1.30 50 59 0.3742 377 0.17 1.50 52 62 0.4123 

379 0.15 1.44 62 69 0.3873 376 0.11 1.00 51 '59 0.3317 ;: !:• 378 0.17 1.50 52 63 0.4123 

379 0.13 1.25 62 71 0.3606 374 0.13 1.20 51 59 0.3806 •:• 377 0.10 0.90 53 63 0.3162 

376 0.15 1.50 64 71 0.3B73 374 0.14 1.30 51 57 0.3742;: * 375 0.17 1.50 53 61 0.4123 

37B 0.16 1.60 65 74 0.4000 376 0.17 1.50 52 59 0.4123 ;• Si 377 0.17 1.50 53 62 0.4123 

378 0.13 1.30 66 76 0.3606 379 0.17 1.50 52 60 0.4123 ii 378 0.18 1.80 54 84 0.4243 

378 011 1.10 66 77 0.3317 378 0.17 1.50 52 60 0.4123 i|: 379 0.19 1.70 54 64 0.4359 

377 0.10 1.00 67 77 0.3162 378 0.14 1.30 52 61 0.3742 379 0.17 1.50 55 65 0.4123 

367 0.07 0.69 66 77 0.2S46 372 0.13 1.20 52 61 0.3606 :! 374 0.12 1.00 55 64 0.3464 

376.9 0.14 1.37 64 71 0.3714 376.8 0.15 1.34 51 59 0.3832 377.7 0.16 1.44 53 62 0.4028 

I Traverse 

I Point 

A1 

2 

3 

4 

5 

6 

B1 

2 

3 

4 

5 

6 

Average 

Laboratory Results 

FuelF-factor.dscf/MMBIu 

FiterlD 

Front Half Residues: 

Filer wt, g 

Acetone rinse volume, ml 

Acetone wt g 

F.H, Total, g 

Back Half Residues: 

EH.Total.g 

Run 1 

I T1817 

I 0.0007 

Run 3 

D r—i 

0.00121 

0.0027 I 

1 Z 3 c 60 

Total, g 

VES018523 
Dry Gas Meter Calibration Data Summary 

Unit 3 

Veolia ES Technical Solutions 

Sauget, IL 

Parameter 

Run ID 

Run Date 

Meter Box ID 

Duration of Run, Minutes 

Meter Gamma 

Delta H@ , inches of H2 0 

Barometric Pressure, inches of Hg 

Sample Volume, dcf (Vm) 

Ave. Meter Temperature, F (Tm) 

Dry Molecular Weight (Md) 

Ave. Delta H, inches of H20 

Ave. SQR T Delta H, inches of H2 0 

Yqa (calculated calibration factor) 

% Difference 

12/1/2009 

001 

60 

0.991 

1.801 

29.75 

38.327 

67.17 

29.71 

1.37 

1.16 

1.005 

1.4 

12/2/2009 

001 

60 

0.991 

1.801 

29.4 

38.170 

54.83 

29.91 

1.34 

1.15 

0.993 

0.2 

12/3/2009 

001 

60 

0.991 

1.801 

29.8 

39.225 

57.21 

29.69 

1.44 

1.20 

1.001 

1.0 

Averaqe 

0.9 

Yqa = (test duration/Vm) x (SQRT(0.0319*TmR)/(Delta H @ x (Pbar + Ave. Delta H/13.6)) x (SQRT(29/Md)) x Ave.(SQRT Delta 

% Difference = (Yqa - Meter Gamma)/Meter Gamma 

Three run Average % Difference must be <= 5% 

VES018524 
AECOM 

Sampling Train 

Run Number 

Client 

E P A ISOKINETI C SAMPLIN G FIEL D DAT A SHEE T 

Veolia ES Technical Solutions 

Facility Localioil 

Sci tt rce 

Date 

Operator 

Slack Dia. - in. 

Stan lime 

Stop Time 

Sauget, IL 

Barometric Pressure 

Sialic Pressure (+/-) /- g.-Q^ 

Pro lie/Pilot Number~^,Yl^~— */ Q 

I'itot Coefficient 

Filter Box No. 

Meter Box No. 

LEA K CHECK S lu "(lg 

INITIA L VAC . /£ } 

(.0. dx!,w -y r-rg/o^te!^ 

fr>l tlAj 

Orifice Coefficient (Y) 

Delia II @ 

Noz2le Size/No, 

XAI) Thermocouple ID: A4' 

Imp O 

FINAL VAC. k? 

yy 

C F M 

C F M 

C F M QfOOCLFINAL PITOT 

FILTE R DATA 

illclTCID: /0 7^— 

NUMBE R TAJtl* 

-r m \ 

IMl'INCEK VOL'S. 

SII.KACU. 

Ursat 

CU2 02 

Final Purge Rale 

E'inai P H 

SAMPI F 

I'OIN 1 

ci or K 

TIME 

,VMO C n\ 

HI All 

DcllaP, iii wc 

UIII1ItF 

MtriR\OI. 

DeUarl, in \>c 

as M I li it TEMPERATURE READINGS, °F | PUMP 

VACl UM 

in H R 

• COMMKINT S 

SAMPI F 

I'OIN 1 

ci or K 

TIME 

,VMO C n\ 

HI All 

DcllaP, iii wc 

UIII1ItF 

MtriR\OI. 

DeUarl, in \>c 

Mil 1 Ml 

fi" STACK !• iiniii OVEN 

t>l«.\M( 

MOIIIll I IMPINGLR 

• .\*>MIIIK 1 

IN | Ol 1 

PUMP 

VACl UM 

in H R 

• COMMKINT S 

o r / sf pro •2<yf y2-

/*).,/"? J-7o bo I -

/0 (C 0 - 6f &<r r 

tsr lo ZfS V (*'( sr 

( 

T 

J o s~ 

L £>lf. "26 37 f zs7 S" 

—ip— f 1 

Bi r?c if ^ / 7 / sr 

•2- o. l Co /4b' Ala. £1T 2 7 7 X 7f 

L'bO loisis — 3 7 o Me 7l *r 

f £).U /-/€> t?% ?7 i s» *r (9-tO Lo 37? i h 7 7 

L £T" Si . o 07 O.L f 77 

( 

VES018525 
AECOM E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

Sampling I rani 

Run INumljer 

CUtnl 

Barometric Pressure 

Static Pressure (+/-) 

2f ¥0 

•OdO 

Veolia ES Technical Solutions 

Facility Location 

Source 

Dale 

Operator 

Stack Dia.-

Start lime 

Stun Time 

Sauget, I L 

iocs' 

/D3S 

Probe/Pilot Number SfflZf- ¥£> 

Pilot Coefficient gt. fj> ^ 

Filter Box No. 01% j( 

Meter Hoi No. £)OHu 

Orifice Coefficient (Y) 

Delta II @ 

Nozzle Size/No. 

LEAK CHECKS in 'Hg 

INITIAL VAC. /,5 

MID VAC. 

FINAL VAC. 

C F M 

C F M 

CFM ^..fg.?! 

FINAL PITOT V v 

KILTLUDATA 

XAD tf>».7t TUernrorauule. ID: fft^jCJ^}-

Imp Outlet TC III: Z^ZT - 3 

M.MHKK IARI 

IMPINGE R VOI/S: 

jco 

-.SILIC A ;CE L 

Orsat 

i .C0 2 0 2 

TS 

Kate 

StMrl t 

POINT 

Cl OCK 

TIM E 

VFLOCIT V 

IIFAO 

DeltaP, in wr 

ORQ-IC F 

MLTL R VO L 

v.Dcltnllviiv wc .i^ 

CAS MFTE R TEMPERATUR E READINGS , ° F | .' PUMP 

VACUU M 

, ,in. HB. . 

COMMENT S 

StMrl t 

POINT 

Cl OCK 

TIM E 

VFLOCIT V 

IIFAO 

DeltaP, in wr 

ORQ-IC F 

MLTL R VO L 

v.Dcltnllviiv wc .i^ 

VOLUM E 

ff _ STAC K PROB E 'OVE N 

ORGANI C 

MODLLE . IMPINGE R 

C A S METE R 

.' PUMP 

VACUU M 

, ,in. HB. . 

COMMENT S 

StMrl t 

POINT 

Cl OCK 

TIM E 

VFLOCIT V 

IIFAO 

DeltaP, in wr 

ORQ-IC F 

MLTL R VO L 

v.Dcltnllviiv wc .i^ 

VOLUM E 

ff _ STAC K PROB E 'OVE N 

ORGANI C 

MODLLE . IMPINGE R I N o u r 

.' PUMP 

VACUU M 

, ,in. HB. . 

COMMENT S 

r4f e T /.3<r ^ 77 

3- T 7 v 9 . 5:3 2s7 257 37 ^7 

3 /\- , / f 13 37ft ?7 SO 5 8 

,W 2.-77 '

?

2 <;«? ST9 

r -*F m r i T7b <?7 3^ f i j 

4- IC JO ML "74.2, D3 2.65 9^ 

i~ '-v.'x i/f>j^~Hi 

»m 37 f 2s-a 37 <T7 Co ?—3—*— 

2- s r fo i-S 7&8.S 37 » 59 L 

I® ft A H i S ntbi ^7<? 2J&0 K i i 37 •7 

<f :

f. S3 « n IB 2.5.5 38 5 1 CD 

C $s zr r -K 7Tt5, <rJL, 37a 7 ST led 7g .'-«*<. 373L '26-2- 7 

7B^5*A 

VES018526 
AECOM 

Sampling Train 

E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

Sauget, IL 

Run Number *£ 

Client Veolia ES Technical Solution 

I'acility Loc:il 

Source 

Da It 

Operator 

Sl:ick Dia. - ii 

Sturt Time 

Stnp Time 

Barometric Pressure 

Static Pressure (+/-) 

JUL 

i or 

. r- ' 

I'robc/Pilol Number J?/?t "-^/£> 

I'ilut Coefficient {), jf if 

Filler Boi NO. ~~ 

Meter Box No. 

Orifice. CQeffieient {Y) 

Bella II® . 

Nozzle Size/No. 

XAD Tliormticuu|ile ID: 

Imp Outlet TC ID: 

LEAK CHECKS in "Hg 

INITIAL VAC. / S 

FINAL VAC. JL 

C F M o. 

C F M 

C F M o. co y 

d ff ( FINAL PITOT 

FIM'KK DATA 

NUMBER TARE 

tvisr 

IMPINCEU VOL'S. 

INIT. 

"30" 

ten 

FINAL 

Orsat 

C 0 2 

to 

rinitl Purge Rale 

SAMPLE 

POINT 

CLOC K 

TIME 

v n ocn v 

HEAD 

DeltsP, in yic 

ORIJ ICE 

METTR VOC 

.:..'HelaU;'in:.wc.v.. 

GV3 METER TEMPERATUR E READINGS , ° F _i 

PUMP 

VACLUM 

in. Hfi 

, COMMENTS 

SAMPLE 

POINT 

CLOC K 

TIME 

v n ocn v 

HEAD 

DeltsP, in yic 

ORIJ ICE 

METTR VOC 

.:..'HelaU;'in:.wc.v.. 

VOUUMF 

fe 

STACK. PRO III <I\IN 

ORI.VMC 

MODlIt f JMPINGEH 

GAS ME ILK 

_i 

PUMP 

VACLUM 

in. Hfi 

, COMMENTS 

SAMPLE 

POINT 

CLOC K 

TIME 

v n ocn v 

HEAD 

DeltsP, in yic 

ORIJ ICE 

METTR VOC 

.:..'HelaU;'in:.wc.v.. 

VOUUMF 

fe 

STACK. PRO III <I\IN 

ORI.VMC 

MODlIt f JMPINGEH DS OUT 

_i 

PUMP 

VACLUM 

in. Hfi 

, COMMENTS 

D ^ o.n / 6- Pi7- $77 37. 6 77J& m */ 5 Y 6 

•% <T fa /•O 2.6 S 3S~ S 7 5"7 <e 

3 iC StC IS" cY0<fr*~7 'Jsr to 7 4 If 2A 0 , i 7 l,B w 30$ Zip k 

i" to tr & > i 7 7S& >7 

"7 tr 70 f!> . fo c

it<-f- 4& 2-S"7' 2-5*1 3o<r car®: f// & 

917, •COX. i -r i_ _ 

sr o, n i 9 / 1 . OCX, vi <r "Z{r~1 1S7 7~7[ 5"-3 4f 7 rt-sit.ri'cL il 9-4 

L% :?C Vo Q< 17 no s i %17 >?/ 2 7 S3 -7 

i O r l g /X Slt> >9 4 Y Sett '7 

U 1,7 •^t 0 

< e t srr 0 / 7 i 5 L7 5-5 7 5 s r bS 

<zr~ bo i'X Hinyi- m tjsft 

1 I 

VES018527 
AECOM 

SAMPLE TRAIN MOISTURE RECOVERY DATA SHEET 

Referenc e Metho d / Samplin g Trai n : f \ l^A, / 5 

Recovered by : Jtjff CcfrVH^ Recovered by: Recovered by : 

Run No. 1 Date: (2-ol-$9 RunNy . Date: Vlt£-& i Run No. ^ Date: |^;03>-e^ 

X A D Module No. : X A D Module No. : X A D Module No.: 

Filter No. : T |?/7 Filter No.: T " ItHX Filter No. : T ~ U V 

Impinger No. and Volum e Im pinger No. and Volume Im pinger No. and Volum e 

1 Initial 

No. 1 (mL) 

Final 

(mL) 

Rinse 

(mL) No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) 

1 SO H2D 1 SO 1 So TO 

2 m 33f 2 ioo 2 345 

3 iOO 105 3 loo 3 hd HO 

4 0 0 4 0 0 4 0 0 

5 loo loo 5 ioo 5 joo Icq 

6 ioo 6 i c o ioo 6 I CO 

te 

7 Sb 7 % 7 & 7 Sb DIFF : 

7 % 

DIFF : 

7 & DIFF : 

Totals mo uo Totals no Totals 

Initial 

(g) 

Final 

(g) 

Initial 

(g) 

Final 

(g) 

Initial 

(g) 

Final 

(g) 

Initial 

(g) 

Final 

(g) DIFF : 

Initial 

(g) 

Final 

(g) DIFF : 

Initial 

(g) 

Final 

(g) DIFF : 

Silica 

Gel 3(<v3 7-9 Silica 

Gel i l Silica 

Gel w 

Final Net Moisture Gain : Final Net Moisture Gain: Final Net Moisture Gain: Hi-? 

C.\Documents and Setting s\mi!os\Desktop\[Moisiure Recovery.xls]A 

VES018528 
Metho d 0023 A 

VES018529 
Veolia ES Technical Solutions 

PCDD / PCDF Emission Results - TEQ Basis - Front Half 

Method 0023A Sampling Parameters 

Run No. 

Date 

Start Time 

1 

01-Dec-09 

13:41 

2 

02-Dec-09 

12:30 

3 

03-Dec-09 

13:18 

Run No. 

Date 

Start Time 

1 

01-Dec-09 

13:41 

2 

02-Dec-09 

12:30 

3 

03-Dec-09 

13:18 

Stop Time 16:49 15:35 16:53 

Sample Volume 

unit s 

dscf 106.679 112.729 120.283 

Sample Volume m

3 3.02 3.19 3.41 

Moisture Content % v/v 48.2 48.1 42.3 

0 2 Concentration % v/v (dry) 7.30 7.30 9.50 

C 0 2 Concentration % v/v (dry) 9.93 9.78 8.15 

Isokinetics % 109 107 98 

Stack Flowrate dscfm 4,462 4,810 5,573 

PCDD/PCDF 

Parameters TEF (a) 

P9 ng/m3 

TEQ 

pg ng/m3 

TEQ 

pg ng/m3 

TEQ 

2,3,7,8-TCDD 1.00 0.64 2.1 E-04 0.59 1.9E-04 0.74 2.2E-04 

1,2,3,7,8-PeCDD 0.50 0.92 1.5E-04 0.84 1.3E-04 1.14 1.7E-04 

1,2,3,4,7,8-HxCDD 0.10 0.84 2.8E-05 1.31 4.1 E-05 1.13 3.3E-05 

1,2,3,6,7,8-HxCDD 0.10 0.85 2.8E-05 1.31 4.1 E-05 1.14 3.3E-05 

1,2,3,7,8,9-HxCDD 0.10 0.78 2.6E-05 1.21 3.8E-05 1.05 I 3.1 E-05 

1,2,3,4,6,7,8-HpCDD 0.01 1.11 3.7E-06 1.24 3.9E-06 3.54 1.0E-05 

OCD D 0.001 3.46 . 1.1 E-06 3.31 1.0E-06 8.98 2.6E-06 

2,3,7,8-TCDF 0.10 0.60 2.0E-05 0.81 2.5E-05 0.85 2.5E-05 

1,2,3,7,8-PeCDF 0.05 0.67 11 E-05 0.86 1.3E-05 0.91 1.3E-05 

2,3,4,7,8-PeCDF 0.50 0.71 1.2E-04 0.91 1.4E-04 0.96 1.4E-04 

1,2,3,4,7,8-HxCDF 0.10 0.54 1.8E-05 0.75 2.4E-05 0.84 2.5E-05 

1,2,3,6,7,8-HxCDF o.i o 1 0.54 1.8E-05 0.76 2.4E-05 1.12 3.3E-05 

2,3,4,6,7,8-HxCDF 0.10 5.83 1.9E-04 0.81 2.5E-05 1.56 4.6E-05 

1,2,3,7,8,9-HxCDF 0.10 0.60 2.0E-05 0.83 2.6E-05 0.82 2.4E-05 

1,2,3,4,6,7,8-HpCDF 0.01 0.60 2.0E-06 0.76 2.4E-06 4.96 1.5E-05 

1,2,3,4,7,8,9-HpCDF 0.01 0.74 2.5E-06 0.84 2.6E-06 1.26 3.7E-06 

OCD F 

TOTAL TEQ s (ng/m0.001 

) 

0.89 2.9E-07 

8.5E-04 

1.14 3.6E-07 

7.3E-04 

2.56 7.5E-07 

8.2E-04 

TOTAL TEQ s (ng/m3 @ 7 % 0 2 ) 

TOTAL TEQ s (g/s) 

8.7E-0 4 

1.8E-12 

7.4E-0 4 

1.6E-12 

1.0E-03 

2.2E-12 

(a) U.S.EP A (1989) Toxic Equivalency Factor 

S \_JOB\2009\Veolia\Test DataUJnit 3\[unit3_M0023A.xlsx]TEQS-BH 

VES018530 
Veolia ES Technical Solutions 

PCDD / PCDF Emission Results - TEQ Basis - Back Half 

Method 0023A Sampling Parameters 

Run No. 1 2 3 

Date 01-Dec-09 02-Dec-09 03-Dec-09 

Start Time 13:41 12:30 13:18 

Stop Time 16:49 15:35 16:53 

Units 

Sample Volume dscf 106.679 112.729 120.283 

Sample Volume m

3 3.02 3.19 3.41 

Moisture Content % v/v 48.2 48.1 42.3 

0 2 Concentration % v/v (dry) 7.30 7.30 9.50 

C 0 2 Concentration % v/v (dry) 9.93 9.78 8.15 

Isokinetics % 109 107 98 

Stack Flowrate dscfm 4,462 4,810 5,573 

PCDD/PCDF pg ng/m3 

pg ng/m3 

pg ng/m3 

Parameters TEF (a) TEQ TEQ TEQ 

2,3,7,8-TCDD 1.00 4.67 1.5E-03 3.01 9.4E-04 3.86 1.1E-03 

1,2,3,7,8-PeCDD 0.50 24.2 4.0E-03 16.2 2.5E-03 20.3 3.0E-03 

1,2,3,4,7,8-HxCDD 0.10 26.4 8.7E-04 16.0 5.0E-04 17.0 5.0E-04 

1,2,3,6,7,8-HxCDD 0.10 58.7 1.9E-03 38.7 1.2E-03 40.3 1.2E-03 

1,2,3,7,8,9-HxCDD 0.10 36.9 1.2E-03 26.1 8.2E-04 25.6 7.5E-04 

1,2,3,4,6,7,8-HpCDD 0.01 405 1.3E-03 252 7.9E-04 268 7.9E-04 

OCD D 0.001 537 1.8E-04 327 1.0E-04 339 1.0E-04 

2,3,7.8-TCDF 0.10 33.3 1.1E-03 25.0 7.8E-04 30.0 8.8E-04 

1,2,3.7,8-PeCDF 0.05 45.5 7.5E-04 30.9 4.8E-04 38.3 5.6E-04 

2,3,4,7,8-PeCDF 0.50 97.6 1.6E-02 63.7 1.0E-02 88.0 1.3E-02 

1,2,3,4,7,8-HxCDF 0.10 71.5 2.4E-03 42.4 1.3E-03 50.7 1.5E-03 

1,2,3,6,7,8-HxCDF 0.10 60.8 2.0E-03 38.4 1.2E-03 48.7 1.4E-03 

2,3,4.6,7,8-FIxCDF 0.10 82.6 2.7E-03 53.0 1.7E-03 69.5 2.0E-03 

1,2,3.7,8,9-HxCDF 0.10 19.9 6.6E-04 12.4 3.9E-04 15.0 4.4E-04 

1,2,3,4,6,7,8-HpCDF 0.01 232 7.7E-04 122 3.8E-04 126 1 3.7E-04 

1,2,3.4,7,8,9-HpCDF 0.01 22.8 7.5E-05 14.8 4.6E-05 14.4 4.2E-05 

OCD F 0.001 84,3 2.8E-05 44.8 1.4E-05 37.6 1.1 E-05 

TOTAL TEQ s (ng/m3) 0.038 0.023 0.028 

TOTAL TEQ s (ng/m ' @ 7 % Oj) = 0.039 0.024 0.034 

TOTAL TEQ s (g/s) 7.95E-11 5.26E-11 7.26E-11 

(a) U.S.EP A (1989) Toxic Equivalency Factor 

S l_JOB\2009\Veolia\Test DaiaUJnil 3\[unit3_M0023A xlsx]TEQS-BH 

VES018531 
Veolia ES Technical Solutions 

Fixed Hearth Incinerator #3 

Method 0023A Sampling Parameters 

Run No. 1 

01-Dec-09 

13:41 

16:49 

2 

02-Dec-09 

12:30 

15:35 

3 

03-Dec-09 

13:18 

16:53 AVGS 

Date 

1 

01-Dec-09 

13:41 

16:49 

2 

02-Dec-09 

12:30 

15:35 

3 

03-Dec-09 

13:18 

16:53 AVGS 

Start Time Units 

1 

01-Dec-09 

13:41 

16:49 

2 

02-Dec-09 

12:30 

15:35 

3 

03-Dec-09 

13:18 

Stop Time 16:53 AVGS 

1 

01-Dec-09 

13:41 

16:49 

2 

02-Dec-09 

12:30 

15:35 

3 

03-Dec-09 

13:18 

16:53 AVGS 

Nozzle Diameter inches 0.431 

29.70 

180.0 

109.984 

0.431 

29.35 

180.0 

112.047 

0.431 

29.90 

180.0 

118.302 

0.431 

Barometric Pressure in. Hg 

0.431 

29.70 

180.0 

109.984 

0.431 

29.35 

180.0 

112.047 

0.431 

29.90 

180.0 

118.302 

29.65 

Net Sampling Time min. 

0.431 

29.70 

180.0 

109.984 

0.431 

29.35 

180.0 

112.047 

0.431 

29.90 

180.0 

118.302 

180.0 

Volume Metered dcf 

0.431 

29.70 

180.0 

109.984 

0.431 

29.35 

180.0 

112.047 

0.431 

29.90 

180.0 

118.302 113.444 

Avg. DGM Temp. °F 77.1 51.8 56,1 61.7 

Avg Delta H in H2 0 1.19 1.28 1.47 1.31 

Avg Delta H in. Hg 0.0872 0.0944 0.1081 0.0965 

DGM Calibration Factor — 0.9910 0.9910 0.9910 0.9910 

Gas Sample Volume dscf 106.679 112.729 120.283 113.231 

Total Water Collected mL 2103.2 2212.4 1869.2 2061.6 

Volume of Water Vapor scf 99.166 104.315 88.133 97.204 

Moisture (measured) % v/v 48.2 48.1 42.3 46.2 

Moisture (@ saturation) % v/v 100.8 102.6 100.1 100.9 

Dry Mole Fraction, 100-%M — 0.5182 I 0.5194 0.5771 0.5383 

C 0 2 at Stack %dry 9.93 

7.30 

9

_

. 78 

L 7.30 

8.15 

9.50 

9.29 

0 2 at Stack %dry 

9.93 

7.30 

9

_

. 78 

L 7.30 

8.15 

9.50 8.03 

CO + N2 % dry 82.77 82.92 82.35 82.68 

Dry Molecular Weight Ib/lb-mole 29.88 29.86 29,68 29.81 

Wet Molecular Weight Ib/lb-mole 24.16 24.16 24.74 24.35 

Excess Air at Stack % 50.2 50.0 77.6 59.3 

Stack Diameter inches 39.0 39.0 39.0 39.0 

Stack Area sq. in. 1194.6 1194.6 1194.6 1194.6 

Static Pressure in H2 0 -0.09 -0.12 -0.12 -0.11 

Stack Pressure in. Hg 29.69 29.34 29.89 29.64 

Avg. Stack Temp. °F 380.8 376.3 382.2 379.8 

Avg. Sqroot of Delta P — 0.3570 0.3852 0.4041 0.3821 

SDE Average — 10.351 11.141 11.728 11.073 

Pitot Coefficient — 0.84 0.84 0.84 0.84 

Stack Gas Velocity afpm 1,665 1,803 1,858 1,776 

Stack Flowrate wet acfm 13,816 14,958 15,417 14,730 

Stack Flowrate wet scfm 8,610 9,261 9,656 9,176 

Stack Flowrate dscfm 4,462 4,810 5,573 4,948 

Isokinetics % 109 107 98 105 

Meter Box No. — 2 

1.8010 

2 

1.8010 

2 

1,8010 

-

Delta H @ in. Hg 

2 

1.8010 

2 

1.8010 

2 

1,8010 -

Field QA Yqc -

0.992 0.995 1.006 0.998 

[Deviation] Pre-Y % 0.1% 0.4% 1.6% 0.7% 

S:\_JOB\2003Weolia\Test DataUJnit 3\[unit3_M0023A.xlSK]DATA 

VES018532 
Method 0023A Sampling Parameters 

PI 

R U N 1AVGS - - PCDDs / PCDF s R U N 2 AVG S - PCDDs/PCDF s R U N 3 AVG S - PCDDs/PCDF s 

PI DP SQRT 

DP 

DGM 

IN 

DGM 

OUT 

DH STACK 

TEMP 

DP SQRT 

DP 

DGM 

IN 

DGM 

OUT 

DH STACK 

TEMP 

DP SQRT 

DP 

DGM 

IN 

DGM 

OUT 

DH STACK 

TEMP 

al 0.15 0.3873 68 70 1.43 370 0.14 0.3742 53 55 1.20 377 0.18 0.4243 52 55 1.60 380 

1 0.14 0.3742 69 75 1.30 361 0.16 0,4000 52 58 1.40 377 0.18 0.4243 52 57 1.60 381 

a2 0.13 0.3606 70 77 1.20 384 0.15 0.3873 53 59 1.30 377 0.19 0.4359 53 61 1.70 385 

2 0.13 0.3606 70 78 1,20 386 0.15 0 3873 52 58 1.30 378 0.19 0.4359 53 60 1.70 385 

a3 0.15 0.3873 71 79 1.40 386 0.13 0,3606 52 58 1.10 378 0.19 0.4359 53 59 1.70 384 

3 0,14 0.3742 71 80 1.30 384 0.16 04000 52 58 1.40 379 0.19 0.4359 53 59 1.70 384 

al 0.14 0.3742 71 80 1.30 383 0.16 0.4000 52 58 1.40 379 0.20 0.4472 52 59 1.75 383 

4 0.13 0.3606 72 80 1.20 383 0.16 0.4000 52 58 1.40 380 0.20 0.4472 52 58 1.75 385 

a5 0.13 0.3606 72 80 1.20 383 0.13 0.3606 52 58 1.10 378 0.18 0.4243 52 58 1.60 384 

5 0.13 0.3606 73 81 1.20 381 0.14 0.3742 52 58 1,20 378 0.18 0.4243 52 58 1.60 382 

a6 0.13 0.3606 73 81 1.20 379 0.15 0.3873 51 57 1.30 370 0.09 0.3000 52 59 0.80 380 

6 0.12 0.3464 73 82 1.20 376 0.14 0.3742 51 57 1.20 369 0.09 0.3000 52 59 0.80 380 

b1 0.14 0.3742 74 77 1.30 375 0.16 0.4000 50 54 1.40 375 0.18 0.4243 53 59 1.60 379 

1 0.13 0.3606 74 82 1.20 381 0.16 0.4000 49 54 1.40 376 0.18 0.4243 53 60 1.60 382 

b2 0.14 0.3742 75 83 1.30 383 0.14 0.3742 48 53 1.20 378 0.17 0.4123 53 60 1.50 380 

2 0.14 0.3742 75 83 1,30 383 0.16 0.4000 47 52 1.40 376 0.17 0.4123 53 60 1.50 381 

b3 0.13 0.3606 75 84 1.20 382 0.16 0.4000 46 52 1.40 377 0.18 0.4243 53 60 1.60 383 

3 0.13 0.3606 76 84 1.20 381 0.16 0.4000 45 51 1.40 378 0.18 0.4243 54 60 1.60 384 

b4 0.12 0.3464 76 84 1.10 381 0.17 0.4123 45 51 1.45 377 0.18 0.4243 54 60 1.60 385 

4 0.12 0.3464 76 84 1.10 382 0.17 0.4123 46 50 1.45 378 0.18 0.4243 54 60 1.60 385 

b5 0.11 0.3317 76 84 1.00 381 0.14 0.3742 45 50 1.20 379 0.14 0.3742 54 60 1.20 384 

5 0.11 0.3317 76 84 1.00 380 0.14 0.3742 45 50 1.20 378 0.15 0.3873 55 60 1.30 383 

b6 0.09 0.3000 77 84 0.81 378 0.12 0.3464 44 50 1.00 370 0.10 0.3162 55 60 0.98 377 

6 0.09 0.3000 77 83 0.81 376 0.12 0.3464 44 50 1.00 370 0.10 0.3162 55 60 0.90 377 

A V G 0.13 0.3570 77.1 1.19 381 0.15 0.3852 51.8 1.28 376 0.17 0.4041 56.1 1.47 382 

VES018533 
AECOM 

Sampling Train 

EPA ISOKINETIC SAMPLING - FIELD DATA SHEET 

Run Number 

Client Vcolui ES Technical Solulions 

1'ncilily Location 

So iircc 

Date 

Operator 

Stuck Dia. - in. 

Start Time 

Stuji Time 

Sauftel, II. 

Barometric I'rcssim 

Sialic Pressure (+/-) 

I'robeJPUat Number 

I'itol Coefficient 

Filler Box No, 

Meter Lox Nu. 

Orifice Coefficieot (Y) 

Delta H@ 

Nozzle Size/No. 

O.gcf 

LEAK CHECKS in "Hg 

INITIAL VAC- {{& 

MID VAC. 

flNAL VAC. 

J2l 

IL 

CFM O, 

CFM 

0. otrc> 

CFM £}.OOJ 

INIT. PITOT 1 / • / FINAL PITOT 

FILTER DATA 

XAI> Thermocouple ID: X4D (,•: 

NI MBKH TARE 

IMPINUIKVO I 'S 

SAMPLF . 

POIN T 

< LOCK VHOC1IY ( 

HEA D V 

1) leal' 111 n 

ORIUCF 

'METE R VOI . 

^ DeltuII, in wc 

M I IIII l| TEMPERATURE READINGS, °F | 

1 

PUM P 

VACUU M 

in Mg 

COMVIl IVIS 

SAMPLF . 

POIN T 

< LOCK VHOC1IY ( 

HEA D V 

1) leal' 111 n 

ORIUCF 

'METE R VOI . 

^ DeltuII, in wc VOLUM E 1 

re | STAC K 

I'KOIII OVX N 

ORGANI C 

MODUL E 1MPINUER 

GASMF1FK 

1 

PUM P 

VACUU M 

in Mg 

COMVIl IVIS 

SAMPLF . 

POIN T 

< LOCK VHOC1IY ( 

HEA D V 

1) leal' 111 n 

ORIUCF 

'METE R VOI . 

^ DeltuII, in wc VOLUM E 1 

re | STAC K 

I'KOIII OVX N 

ORGANI C 

MODUL E 1MPINUER IN OLl 

1 

PUM P 

VACUU M 

in Mg 

COMVIl IVIS 

A-f 0 73 ('.45. 74<7 1<T7 TV 7 0 P.-/S.—' / S.<-j-^ 

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Xl? 37.S • n<i<r •2Jii ?h -7/ 77 fo 

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sis 0't<4 /.I 5^ 7^ BO f n 

5l.sr £0 0 i3 £.3 fto 

7 

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O- i3 lnt,~T(f> s s / so fit lO 

7£ m 0. fB ia rf'.-i . 1 B -2-t<r~ #6 75 sr / o 

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<n.r/0$~ Or 13 /•<3- m Md II 

fix* /.3 3*3 + H7 i ^O •75" S3 If 

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Orsat 

C 0 2 0 2 

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Final Purge Hate 

VES018534 
AECOM EPA ISOKINETIC SAMPLING - FIELD DATA SHEET 

Sampling Train 

Run Number 

Client 

1'actlily Loc: 

Source 

Dale 

Operator 

Stack Dia.-

Start Time 

Stop Time 

Veolia ES Technical Solution 

Sauget, IL 

(Mr 

,37 ' 

Barometric Pressure 

Static Pressure (+/-) 

Probe/Pilot Number 

i'itot Coefficient 

Filter Box No. 

Meter Box No. 

Orifice Coefficient (Y) 

Delta tf@ 

Nozzle Size/No. 

LEAK CHECKS in "Hg 

INITIAL VAC, (l-j 

MID VAC. 

FINAL VAC. 

OR it 

I E 

C F M 

C F M 

£> O O <j 

C F M o .pc y 

FINAL PITOT <y LA 

FILTER DATA 

XAD Thermocouple II): )</t-fe63 

}}KNDMBBIIB;E 1AKF 

IMPINGER VOI 'S 

SILICA GE L 

Orsat 

C 0 2 02 

U 7 J 

Final Purge Rale 

S A M PI I 

POINT 

( 1 III K 

IIMI 

VELOUFY 

III Ml 

DLMA P in WL 

OR1F ICI 

MLII K VOL 

Dtttull. in wi 

( \», Mh IU! 76f.. <

?^S ~ TEMPERATUR E READINGS , ° F 1! PUMP 

• COMMENTS 

S A M PI I 

POINT 

( 1 III K 

IIMI 

VELOUFY 

III Ml 

DLMA P in WL 

OR1F ICI 

MLII K VOL 

Dtttull. in wi 

Ul| 1 Ml 

II STA( K PDOIII OVIN (llt(.\M( 

, MODIII F IMPINGER 

GAS ME IFI! VAf II1IM • COMMENTS 

S A M PI I 

POINT 

( 1 III K 

IIMI 

VELOUFY 

III Ml 

DLMA P in WL 

OR1F ICI 

MLII K VOL 

Dtttull. in wi 

Ul| 1 Ml 

II STA( K PDOIII OVIN (llt(.\M( 

, MODIII F IMPINGER IN | III 1 

VAf II1IM • COMMENTS 

-A 1 O 7 V ' 0 -1 4 ! ^ A 5 7 37 7 *i "in r ( >_5C. 

—•/•-»-—i 7S~ /J5- 0 - « b ^7 3>7 2.57 i t > 5 « S ( 2 -

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AC 7f SIS " o „ is f,. 3 •a 70 i 6 7 %56 3^ 51 ~> "J 1 3 

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B97Jlf t 

VES018535 
AHCQA4 E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

Sampling Train 

Run (Number 

Client Vcoliii ES Technical Solutions 

facilit y Locatio n 

SHU rce 

Date 

Sau£Ct, IL 

Operato r //if. UAt^>^ 7~. i4&^j.<Sy_ 

Stack Dia. - III. S* ) 

Start Time 

Sfoji Tim e 

llurametri c Pressure 

Sialic Pressure (+/.) 

'Probe/Pilot Numbe r £, 0 jT-. 

Pilot Coefficien t ^7-ft5 * / 

I iltcr Bo i NO. 0(2 , j I 

Meter Bo x No. $ 0 3~ 

Orific e Coefficient (V) 

Dello II @ 

Nu*zle Size/No. 

XAII Thermocoupl e IIV. 

Imp Outle t T C ID: 

0

 C

l^f 

LEA K CHECK S i a 'Ti g 

INITIA L VAC . fS " 

MID VAC . 

FINA L VAC . 

C E M 

C U M 

C F M 

FINA L PITO T *S 

FILTER DATA 

•€01 

H A D 

M;MBK H TAR E 

IMPINGER VOL'S . 

mo 

# ^ 7 

I Orsat 

i co:.; 

u Tr 

l-'inal l'urye Kate 

SAMFLr 

rOINT 

ICLOCK : 

TIM F 

VEiocnv 

III A D 

- "i DeUaP,- in *ve 

ORIUCF 

METE R VOl 

DcH&II, in ytc 

<;.\s METE B !| TEMPERATURE READINGS, "F | . PUMP 

' VACUU M 

in.He 

COMMENTS 

SAMFLr 

rOINT 

ICLOCK : 

TIM F 

VEiocnv 

III A D 

- "i DeUaP,- in *ve 

ORIUCF 

METE R VOl 

DcH&II, in ytc 

VOLIIM F 

ff STACK PROBF 'oyi-N 

ORGANIC 

MODULE •IMPINGER 

CAS MblEIt 

. PUMP 

' VACUU M 

in.He 

COMMENTS 

SAMFLr 

rOINT 

ICLOCK : 

TIM F 

VEiocnv 

III A D 

- "i DeUaP,- in *ve 

ORIUCF 

METE R VOl 

DcH&II, in ytc 

VOLIIM F 

ff STACK PROBF 'oyi-N 

ORGANIC 

MODULE •IMPINGER IN Oil! 

. PUMP 

' VACUU M 

in.He 

COMMENTS 

£ I D i'r 3S"" IO 

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A-2- ' o JI /,'?- 7/i s HX- 34 S"3 L

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—r v— e J o 0 9 o /to5/ .47 377 2.W7 r ^ isO 7 

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VES018536 
AECOM 

SAMPLE TRAIN MOISTURE RECOVERY DATA SHEET 

Referenc e Metho d / Samplin g Trai n : ArET^t^h 0(V2.2> 

- r r \ 

Recovere d b y : J - tof'THfi. O 

Recovere d by : Recovere d by : 

R u n No . R J Date : O.-o\-0$ R u n No . Date : jl~Ol ~ 0 ^ R u n No . Date : l%~oy£i 

X A D Modul o No. : X A D Modul e No. : X A D Modul e No . : 

Filter No. : Filter No. : Filter No . : 

Im pinger No. and Volume Im pinger No. and Volum e Impinger No. and Volum e 

N o . 

Initial 

(mL) 

Fina l 

(mL ) 

Rins e 

(mL) N o . 

Initial 

(mL) 

Fina l 

(mL) 

Rins e 

(mL) N o . 

Initial 

(mL) 

Fina l 

(mL) 

Rinse 

(mL) 

1 0 1 

0 

1 0 M S 

2 200 [ U D 2 1150 2 

! 3 CI 0 

3 bo 3 ioo loo 3 

) 6 o 

4 O 0 4 4 

5 

S G r 

5 

s# 5 

6 6 6 

7 7 7 

DIFF : 

7 

DIFF : 

7 

DIFF : 

Totals Soo aot<r Totals ;3ct> a n f Totals 

Initial 

(9) 

Fina l 

(g) 

Initial 

(a) 

Fina l 

(g) 

Initial 

(g) 

Fina l 

(g) 

Initial 

(9) 

Fina l 

(g) DIFF : 

Initial 

(a) 

Fina l 

(g) DIFF : 

Initial 

(g) 

Fina l 

(g) DIFF : 

Silic a 

G e i 

Silic a 

G e l 37.V 

Silic a 

G e l 

Final Net Moisture Gain: Final Net Moisture Gain: Final Net Moisture Gain: 

C \Docurnents and Set!ings\milo3\Desktop\[Moisture Recovery, xts] A | ft^S , 

VES018537 
Method 25A 

VES018538 
AVERAGED CEM DATA Jo b Number: 60133216 Start Time : 13:41:00 

R u n ID: R1B Start Date: 12/01/09 

Date Tim e T H C 

12/1/2009 13:43:00 0.43 

12/1/2009 13:45:00 0.38 

12/1/2009 13:47:00 0.41 

12/1/2009 13:49:00 0.45 

12/1/2009 13:51:00 0.51 

12/1/2009 13:53:00 0.4 

12/1/2009 13:55:00 0.45 

12/1/2009 13:57:00 0.51 

12/1/2009 13:59:00 0.71 

12/1/2009 14:01:00 0.55 

12/1/2009 14:03:00 0.57 

12/1/2009 14:05:00 0.62 

12/1/2009 14:07:00 0.58 

12/1/2009 14:09:00 0.81 

12/1/2009 14:11:00 0.52 

12/1/2009 14:13:00 0.54 

12/1/2009 14:15:00 0.59 

12/1/2009 14:17:00 0.74 

12/1/2009 14:19:00 0.63 

12/1/2009 14:21:00 0.86 

12/1/2009 14:23:00 0.54 

12/1/2009 14:25:00 0.72 

12/1/2009 14:27:00 0.6 

12/1/2009 14:29:00 0.54 

12/1/2009 14:31:00 0.61 

12/1/2009 14:33:00 0.81 

12/1/2009 14:35:00 0.6 

12/1/2009 14:37:00 0.61 

12/1/2009 14:39:00 0.58 

12/1/2009 14:41:00 0.59 

Averag e Value : 0.58 

Correcte d Average : .47 

VES018539 
AVERAGED CEM DATA Jo b

 Number: 60133216 Start Time : 12:30:00 

R u n ID: R2B Start Date: 12/02/09 

Date Tim e T H C 

12/2/2009 12:32:00 0.42 

12/2/2009 12:34:00 0.34 

12/2/2009 12:36:00 0.38 

12/2/2009 12:38:00 0.41 

12/2/2009 12:40:00 0.45 

12/2/2009 12:42:00 0.42 

12/2/2009 12:44:00 0.52 

12/2/2009 12:46:00 0.38 

12/2/2009 12:48:00 0.46 

12/2/2009 12:50:00 0.49 

12/2/2009 12:52:00 0.48 

12/2/2009 12:54:00 0.45 

12/2/2009 12:56:00 0.44 

12/2/2009 12:58:00 0.52 

12/2/2009 13:00:00 0.35 

12/2/2009 13:02:00 0.28 

12/2/2009 13:04:00 0.31 

12/2/2009 13:06:00 0.37 

12/2/2009 13:08:00 0.35 

12/2/2009 13:10:00 0.34 

12/2/2009 13:12:00 0.36 

12/2/2009 13:14:00 0.36 

12/2/2009 13:16:00 0.33 

12/2/2009 13:18:00 0.29 

12/2/2009 13:20:00 0.38 

12/2/2009 13:22:00 0.34 

12/2/2009 13:24:00 0.52 

12/2/2009 13:26:00 0.49 

12/2/2009 13:28:00 0.48 

12/2/2009 13:30:00 0.44 

Averag e Value : 0.4 

Correcte d Average : .33 

VES018540 
AVERAGED CEM DATA

 Jo b

 Number: 60133216 Start Time : 13:18:00 

R u n ID: R3B Start Date : 12/03/09 

Date Tim e T H C 

12/3/2009 13:20:00 0.29 

12/3/2009 13:22:00 0.3 

12/3/2009 13:24:00 0.26 

12/3/2009 13:26:00 0.33 

12/3/2009 13:28:00 0.26 

12/3/2009 13:30:00 0.29 

12/3/2009 13:32:00 0.31 

12/3/2009 13:34:00 0.35 

12/3/2009 13:36:00 0.3 

12/3/2009 13:38:00 0.31 

12/3/2009 13:40:00 0.3 

12/3/2009 13:42:00 0.3 

12/3/2009 13:44:00 0.33 

12/3/2009 13:46:00 0.34 

12/3/2009 13:48:00 0.31 

12/3/2009 13:50:00 0.32 

12/3/2009 13:52:00 0.29 

12/3/2009 13:54:00 0.25 

12/3/2009 13:56:00 0.29 

12/3/2009 13:58:00 0.36 

12/3/2009 14:00:00 0.25 

12/3/2009 14:02:00 0.33 

12/3/2009 14:04:00 0.22 

12/3/2009 14:06:00 0.26 

12/3/2009 14:08:00 0.26 

12/3/2009 14:10:00 0.2 

12/3/2009 14:12:00 0.23 

12/3/2009 14:14:00 0.18 

12/3/2009 14:16:00 0.24 

12/3/2009 14:18:00 0.23 

Averag e Value : 0.28 

Correcte d Average : 

.2 

VES018541 
o 

VES018542