### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1 IN_W abash River Station Wa bash River Station Unit 4 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte 

### IN_Wabash River Station

Wabash River Station

Unit 4 As Received Higher Heating Value 

### IN_Wabash River Station

Wabash River Station

Unit 4 As Received % Moisture 

### IN_Wabash River Station

Wabash River Station

Unit 4 As Received % Ash 

### IN_Wabash River Station

Wabash River Station

Unit 4 As Received % Sulfur 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Higher Heating Value 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis % Ash 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis % Sulfur 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Antim ony 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Arsenic 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Bery llium 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Cadmium 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Chlorine 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Chromium 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Cobalt 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Fluorine 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Lead 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Manganese 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Mercury 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis Nickel 

### IN_Wabash River Station

Wabash River Station

Unit 4 Dry

basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 ASTM D5865 ASTM D3174 ASTM D4239 SW6010B SW6010B SW6010B SW6010B ASTM E776/9253 SW6010B SW6010B ASTM D3761 SW6010B SW6010B ASTM D6722 SW6010B SW6010BEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### IN_Wabash River Station

Wbash River Station Unit 4 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units WR S-AC-COAL-COMP-R1



### 6/4/2010 6/4/2010 10970.00 Btu/lb WR S-AC-COAL-COMP-R2



### 6/4/2010 6/4/2010 11030.00 Btu/lb WR S-AC-COAL-COMP-R3



### 6/4/2010 6/4/2010 10970.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 16.6 8.59 2 13150 Btu/lb 10.3 2.4 16 8 2.28 13130 Btu/lb 9.52 2.71 16.5 7.93 2.14 13140 Btu/lb 9.5 2.56Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 0.05 % 0.07 % 0.05 %Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 51 ppm 16.6 50 ppm 16 46 ppm 16.5 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 41 10.3 48.8 72.8 4.56 1.88 2.4 39.8 9.52 50.7 72.6 5.23 1.46 2.71 40.5 9.5 49.9 73.5 4.98 1.44 2.56 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 8.09 8.4 7.83EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### IN_Wabash River Station

Wbash River Station Unit 4 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units WR S-ORG-COAL-COMP-R1



### 6/5/2010 6/5/2010 10920.00 Btu/lb WR S-ORG-COAL-COMP-R2



### 6/5/2010 6/5/2010 10890.00 Btu/lb WR S-ORG-COAL-COMP-R3



### 6/5/2010 6/5/2010 10650.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 16.7 8.14 2.14 13110 Btu/lb 9.77 2.57 16.8 8.33 2.21 13090 Btu/lb 10 2.66 18.8 7.54 2.02 13120 Btu/lb 9.29 2.49Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 16.7 39.4 9.77 50.8 73.6 4.83 1.79 2.57 16.8 42.2 10 47.8 72.6 4.83 1.78 2.66 18.8 39.9 9.29 50.9 73.3 5.12 1.59 2.49 Proximate A naly

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 7.48 8.19 8.35EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### IN_Wabash River Station

Wbash River Station Unit 4 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units WR S-MET-COAL-COMP-R1



### 6/9/2010 6/9/2010 11200.00 Btu/lb WR S-MET-COAL-COMP-R2



### 6/9/2010 6/9/2010 11160.00 Btu/lb WR S-MET-COAL-COMP-R3



### 6/10/2010 6/10/2010 11060.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 15.4 7.93 1.96 13240 Btu/lb 9.37 2.32 15.3 8.17 2.13 13180 Btu/lb 9.65 2.51 15.9 8.15 1.93 13150 Btu/lb 9.69 2.29Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 0.092 mg/Kg [< 3.00] BDL mg/Kg 15.9 mg/Kg 2.31 0.088 mg/Kg [< 3.00] BDL mg/Kg 15.2 mg/Kg 2.19 0.087 mg/Kg [< 3.00] BDL mg/Kg 13.4 mg/Kg 2.18Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg 1.51 mg/Kg 16.4 mg/Kg 20.5 mg/Kg 136 mg/Kg mg/Kg 1.48 mg/Kg 15.9 mg/Kg 18.7 mg/Kg 17.3 mg/Kg mg/Kg 1.39 mg/Kg 14.8 mg/Kg 16.1 mg/Kg 13.2 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 22.4 mg/Kg [< 2.00] BDL mg/Kg 5.36 mg/Kg 15.4 20.7 mg/Kg [< 2.00] BDL mg/Kg 5.4 mg/Kg 15.3 20.5 mg/Kg [< 2.00] BDL mg/Kg 5.15 mg/Kg 15.9 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 40.4 9.37 50.1 72 4.98 1.84 2.32 9.48 40.1 9.65 50.3 72.5 4.55 1.7 2.51 9.11 41.7 9.69 48.6 72.5 4.67 1.69 2.29 9.2 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### IN_Wabash River Station

Wbash River Station Unit 4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orange hightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm