### 1 0



# Sample Dat aSummar

y

VES01865 9

### 1 1

Lot-Sampl e # . Dat e Sampled . PARAMETE

R AECOM , In c Clien t Sampl e ID : HBTO-03-M26-R 1 Genera l Chemistr y H9L090423-00 1 Wor k Orde r #... : LQQM

7 12/01/0 9 Dat e Received.. : 12/04/0 9 Matrxx . WAST E

RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 83 5 20 0 mg/k g Dilutio nFactor : 1 10SO0 1BO

0 BTO/l b Dilutio nFactor ! 1 1920 0 187 0 tng/k g Dilutio nFactor : 9.3 5 _METHO D . AST M D482-00 a MD L : 5 1 AST M D240-0 2
MD L : 13 0 KNO XWC-001 S HD L : 56 0 PREPARATION - PRE P ANALYSI S DAT

E BATC H # 12/17-12/22/0 9 935149 7
12/14/0 9 934807 5
12/10-12/14/0 9 934406 0



### VES01866 0

### 1 2

AECOM , In c Clien t Sampl e ID : HBTU-TB-M26-R 2 Genera l Chemistry Lot-Sampl e # . .. : H9L090423-00 2 Wor k Orde c #... : LQQN H Matrix , r WAST E Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # AS hConten t 56 6 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : S I Gros s Calorifi c 1020 0 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MDL . i 13 0 Tota l Chlorin e 1470 0 120 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 6 MD L : 36 0



### VES01866 1

### 13

AECOM , In c . Clien t Sampl e ID : HBTU-U3-M26-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-00 3 Wor k Orde r #.... : LQQN J Matri x: WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNITS . METHO D ANALYSI S DAT E BATC H # As hConten t 52 7 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L ' : 5 1 Gros s Calorifi c 1030 0 180 0 BTO/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1670 0 167 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 8.3 5 MD L ; .500



### VES01866 2

### 1 4

AECOM , In c Clien t Sampl e ID : LBTU-TJ3-M26-R 1 Genera l Chemistr y Lot-Sampl e #... : H9L090423-00 4 Wor k Orde r #..'.: . LQQN L Matri x- : WAST E Dat e Sampled... : 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL

T K b. UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 123 0 20 0 mg/k g AST

M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTD/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 87 3 28 2 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1:4 1 MD L : 8 5



### VES01866 3

### 1 5

AECOM , In c Clien t Sampl e ID : LBTO-D3-M26-R 2 Genera l Chemistr y Lot-Sampl e #... : H9L090423-00 5 Wor k Orde r #.... . : LQQN N Matri x: WAST E Dat e Sampled. : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 117 0 20 0 mg/k g AST

M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor. : 1 MDL.. : : 5 1 Gros s Calorifi c N D ISD O BTU/l b. AST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L . : 13 0 Tota l Chlorin e 82 5 27 8 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1.3 9 MD L : 8 3



### VES01866 4

### 16

AECOM , In c Clien t Sampl e ID ; LBTU-U3-M26-R 3 Genera l Chemistr y Lot-Sampl e : H9L090423-00 S Wor k Orde r #... : LQQN

P Matri x, : WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 256 0 20 0 mg/k g AST

M D4B2-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 HD L : 5 1 Gros s Calorifi c N D 180 0 BTa/li > AST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 HD L : 13 0 Tota l Chlorin e 125 0 28 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1. 4 MD L : B

4



### VES01866 5

### 1 7

AECOM , In c Clien t Sampl e ID : SF-tr3-M26A-Rl Genera l Chemistr y Lot-Sampl e #... : H9L090423-00 7 Wor k Orde r : LQQN

T Matri x: WAST E Dat e Sampled... : 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D . ANALYSI S DAT E BATC H # As hConten t 760 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MDL.. . — : 5 1 GrOS S Calorifi c N D 180 0 BTU/l bASTMD240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 498 0 27 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1. 3 6 MDL.. . . : 8 2



### VES01866 6

### 18

AECOM , In c Clien t Sampl e ID : SF-TJ3-M26A-R 2 Genera l Chemistr y Lot-Sampl e #... : H9L090423-00 8 Wor k Orde r : LQQN

O Matri x: WAST E Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 562 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 502 0 28 4 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 2 MD L : B

5



### VES01866 7

### 1 9

ACCOM , In c Clien t Sampl e ID : SF-D3-M26A-R 3 Genera l Chemistr y Lot-Sampl e #.. . : H9L090423-00 9 Wor k Orde r #... : LQQN 2 Matrix,. ; : WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 602 0 20 0 mg/k g AST

M D4S2-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : S I Gros s Calorifi c N D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L 13 0 ' Tota l Chlorin e 509 0 28 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 1 MD L : 8 5



### VES01866 8

### 2 0

AECOM , In c Clien t Sampl e ID : CS-U3-M26A-R 1 Genera l Chemistr y Lot-Sampl e ft...: H9L090423-01 0 Wor k Orde r Dat e Sampled: 12/01/0 9 Dat e Received. .
PARAMETE

R As hConten t

Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T R

L UNIT S 69900 0 20 0 mg/k g Dilutio nFactor s 1 N D 1B0 D BTU/l b

Dilutio nFactor : 1 23 9 20 4 mg/k g Dilutio nFactor : 1.0 2 LQQN 4 12/04/0 9 Matrix . SOLID

_METHO

D AST M D482-00 a MD L 5 1 AST M DSB6S-0 0
MD L : 13 0 KNO XWC-001 6 MD L : 6 1 PREPARATION - PRE

P ANALYSI S DAT

E BATC

H S 12/11-12/15/0 9 934546 1
12/16/0 9 935003 2
12/10-12/14/0 9 934406 0



### VES01866 9

### 21

Lot-Sampl e # : Dat e Sample d:
PARAMETE

R AECOM , In c Clien t Sampl e ID : CS-03-M2GA-R 2 Genera l Chemistr y H9L090423-Q1 1 Wor k Orde r #.-. : LQQQ

R 12/02/0 9 Dat e Received.. : 12/04/0 9 Matrix . SOLID

As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T R L UNIT S 80100 0 20 0 mg/k g Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 10 5 B 20 4 mg/k g Dilutio nFactor. - 1.0 2 _METHO D AST M D482-00 a MD L : 5 1 AST M D58S5-0 0
HD L : 13 0 KNO XWC-001 6 MD L : S I PREPARATION - PRE P ANALYSI S DAT

E BATC H # 12/11-12/15/0 9 934546 1
12/15/0 9 935003 2
12/10-12/14/0 9 934406 0 NOTE(S) : R L Reportin

g Limi t B Estimate

dresult . Resul

t i s les s tha nRL .



### VES01867 0

### 2 2

AECOM , Xn

c Clien t Sampl e ID : CS-U3-M26A-R 3 Genera l Chemistr y Lot-Sample*... : H9L090423-0L 2 Wor k Orde r #... : LQQQ

W Matri x: SOLID Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL T ' R L • UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 79900 0 20 0 mg/kg AST M D482-0O

a 12/11-12/15/0 9 934546 1 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 160 0 BTU/l bAST M D5865-O O 12/ie/o s 935003 2 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 74. 9 B 20 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1 MD L : S O NOTE(S ) : \ . R L Reportin

g Limi t B Estimate

d result . Resul ti s les s tha n RL .



### VES01867 1

### 2 3

AECOM , In c Clien t Sampl e ID : HBTU-TJ3-M23A-R 1 Genera l Chemistr y Lot-Sampl e #... : H9L090423-01 3 Wor k Orde r # : LQQQ 7 Dat e Sampled. : 12/01/0 9 Dat e Received.. : 12/04/0 9 Matri x: WAST E

PARAMETE

R RESUL

T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 93 7 20 0 ,mg/k g Dilutio nFactor : 1 1040 0 180 0 BTO/lf a

Dilutio nFactor : 1 2060 0 167 0 mg/k g Dilutio nFactor : 8.3 4 _METHO D AST M D482-0O

a MD L -

. 5 1 AST M 1X240-0 2
MD L : 13 0 KNO XWC-001 6 MD L : 50 0 PREPARATION - PRE P ANALYSI S DAT

E BATC H # 12/17-12/22/0 9 935149 7
12/14/0 9 934807 5
12/11-12/16/0 9 934506 4



### VES018672

### 2 4

AECOM , In c Clien t Sampl e ID : HBTU-U3-M23A-R 2 Genera l Chemistr y Lot-Sampl e #... : H9L090423-01 4 Wor k Orde r : LQQE M Matri x: WAST E Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P . PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC

H # As hConten t 58 8 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c 1030 0 IBO O BTtr/l i AST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1470 0 172 0 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 8.6 2 MD L . : S2 0



### VES01867 3

### 2 5

AECOM , In c Clien t Sampl e ID : HBTU-U3-M23A-R 3 Genera l Chemistr y Lot-Sampl e #..- : H9L090423-01 5 Wor k Orde r it... : LQQR O Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 Matrxx . WAST E

PARAMETE

R RESUL

T R L UNIT S As hConten t

Gros s Calorifi c Valu e
Tota l Chlorin e 53 5 20 0 mg/k g Dilutio nFactor : 1 1030 0 180 0 BTTJ/Il ,

Dilutio nFactor : 1 1690 0 168 0 mg/k g Dilutio nFactor ; 8.3 3 _METHO D AST M D482-O0 a MD L : S I AST M D240-0 2
MD L : 13 0 KNO XWC-001 6 MDL... ' : 50 0 PREPARATION- PRE P ANALYSI S DAT

E BATC H # 12/17-12/22/0 9 935149 7
12/14/0 9 934807 5
12/11-12/16/0 9 934506 4



### VES01867 4

### 2 6

AECOM , In c Clien t Sampl e TD: LBTU-U3-M23A-R 1 Genera l Chemistr y Lot-Sampl e #.. . i H9L090423-01 6 Wor k Orde r .

- LQQR 6 Matri x: WAST E Dat e Sampleds 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL

T R L • UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 122 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MDI, . : 5 1 Gros s Calorifi c K D 180 0 BTU/l b. AST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 81 6 27 6 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 8 MD L : 8 3



### VES01867 5

### 2 7

AECOM , In c Cllen t Sampl e ID : LBT0-O3-M23A-R 2 Genera l Chemistr y Lot-Sampl e #... : H9L090423-01 7 Wor k Orde r #... : LQQR 7 Matri x: WAST E Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

R' RESOL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 126 0 20 0 mg/k g AST

M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L S I Gros s Calorifi c H D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L 13 0 Tota l Chlorin e 73 8 28 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 1 MDL... . : S S



### VES018676

### 2 8

AECOM , In c Clien t Sampl e ID: . LBTU-U3-M23A-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-01 8 Wor k Orde r #... : LQQR 8 Matri x... : WAST E Dat e Sampled... : 12/03/0 9 Dat e Received..: . 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 242 0 20 0 . mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MDL . •- 5 1 Gros s Calorifi c N D 180 0 BTD/l bAST M D240-0 2 12/14/0 9 934807 5

. Valu e Dilutio nFactor : 1 MD L 13 0 Tota l Chlorin e 123 0 28 2 mg/k g KNO

XWC-001 5 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 1 MD L : 8 5



### VES018677

### 2 9

AECOM , In c Clien t Sampl e ID : SF-03-M23A-R 1 Genera l Chemistr y Lot-Sampl e #-.. : H9L090423-01 9 Wor k Orde r #... : LQQT

A Matri x: WAST E Dat e Sampled... : 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 729 0 20 0 mg/k g AST

M D4B2-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 ' MD L : 5 1 Gros s Calorifi c N D leO

O BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 • MD L : 13 0 Tota l Chlorin e 503 0 27 4 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 7 MD L : B

2



### VES01867 8

### 3 0

Lot-Sampl e # . Dat e Sampled .
PARAMETE

R Ash- Conten t
Gros s calorifi c Valu e
Tota l Chlorin e AECOM , In c Clien t Sampl e ID : SF-U3-M23A-R 2 Genera l Chemistr y H9L090423-02 0 Wor k Orde r : LQQT

C Matri x: WAST E 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P RESULT R

L UNIT S METHO D • ANALYSI S DAT E BATC H # 695 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 N D 1S0 0 BTTJ/l bAST M D240-0 2 12/14/0 9 934807 5 Dilutio nFactor : 1 MD L : 13 0 501 0 27 4 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 7 MD L : 8 2



### VES01867 9

### 31

AECOM , In c

. Clien t Sampl e ID : SF-U3-M23A-H 3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-02 1 Wor k Orde r #... : LQQT

D Matri x. - WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 782 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 HDL.. . . : 5 1 Gros s Calorifi c N D IBO O s-cv/xt, AST M 0240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor s 1 MD L -. : 13 0 Tota l Chlorin e 502 0 27 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 6 MDL . : 8 2



### VES01868 0

### 3 2

AECOM , In c Clien t Sampl e ID ; CS-U3-M23A-R 1 Genera l Chemistr y Lot-Sampl e : H9L090423-02 2 Wor k Orde r #... : LQQT E Matri x: SOLID Dat e Sampled... : 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H & As hConten t 71100 0 20 0 mg/k g AST

M D482-Q0 a 12/11-12/15/0 9 934546 1 Dilutio nFactor s 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 12/16/0 9 935003 2 Valu e Dilutio nFactor s 1 MD L : 13 0 Tota l Chlorin e 22 0 20 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor s 1 MD L : S

O



### VES01868 1

### 3 3

AECOM , In c Clien t Sampl e TD: CS-U3-M23A-R 2 Genera l Chemistr y Lot-Sampl e #.-. : H9L090423-02 3 Wor k Orde r #...:'LQQT F Matri x: SOLID Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 70300 0 20 0 mg/k g AST

M D4B2-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor ; 1 MD L : 5 1 Gros s Calorifi c N D ISO OBTu/i bAST M DS86S-O O 12/16/0 9 935003 2 Valu e Dilutio nFactor : 1 MDL.. . : 13 0 Tota l Chlorin e 29 5 20 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1 MD L t 6 0



### VES01868 2

### 3 4

ABCOM , In c Clien t Sampl e ID : CS-D3-M23A-E3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-02 4 Wor k Orde r #..- : LQQT GMatri x: SOLID Dat e Sampled.12/03/0 9 Dat e Received.. : 12/04/0 9
PARAMETE

R As hConten t RESUL T ' R

L OMITS 70300 0 20 0 mg/k g Dilutio nFactor s 1 180 0 BTtr/l b Dilutio nFactor s 1 20 4 mg/k

g Dilutio nFactor s 1.0 2 _METHO D AST M D482-00 a MD D : 5 1 AST M D5865-0 0
MDL . : 13 0 KNO XWC-001 6 HD L 6 1 PREPARATION - PRE P ANALYSI S DAT

E BATC H # 12/11-12/15/0 9 934S46 1 12/16:/0 9 935003 2
12/10-12/14/0 9 934406 0 Gros s Calorifi c N D Valu e
Tota l Chlorin e 33 9



### VES01868 3

### 3 5

Clien t Lo t #... ; H9L09042 3
PARAMETE

R As hConten t

Tota l Chlorin e

Tota l Chlorin e
MOTE(S) ; RESUL T H D

N D

N D METHO D BLAN KREPOR T Genera l Chemistr y Matrix . WAST E REPORTIN

G LIMI T UNIT S METHO D PREPARATION - PRE P ANALYSI S DAT

E BATC H # Wor k Orde r # : LQ91G1A A M B Lot-Sampl e # : H9L170000-49 7 20 0 mg/k

g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor t 1 Wor k Orde r # : LQTX01A A M B Lot-Sampl e # : H9L100DOO-06 0 20 0 mg/k

g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor ! 1 Wor k orde r # : LQXER1A A M B Lot-Sampl e # : H9L110000-06 4 20 0 . mg/k

g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1

Calculation

s ar cpcrrormc

d beror e roundin ct o avoi d round-of

f error s i n calculate

d results .



### VES01868 4

### 3 6

METHO D BLAN KREPOR T Genera l COiemistr

y Clien t Lo t ft...: H9L09O42 3 Matri x: SOLID REPORTIN

GPREPARATION - PRE P PARAMETE

RRESUL

T LIMI T UNIT S METHO D ANALYSI S DATE BATC H # As hConten t Wor k Orde r # : LQ1E11A A M B Lot-Sampl e # : H9L110000-46 1 N D 20 0 mg/k g AST

M D482-O0a 12/11-12/15/0 9 934546 1 Dilutio nFactor : 1 NOTE(S ) : • Calculation

s ar cperforme

d befor e roundin g t o uvot d round-of

f error s i n calculate

d results .



### VES01868 5

### 3 7

LABORATOR

YCOHTRO

L SAMPL E EVALDATIO

H REPOR T Genera l Chemistr y Lot-Sajnpl e #... : H9L09042 3 Mat_cix: WAST E
PARAMETE

R As hConten t PERCEN T RECOVER Y 9 9 9 9 RECOVER

Y LIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PRE P BATC H # W0#:LQ91G1AC-LCS/LQ91G1AD-LCS D LC S Lot-Sample* : H9L170000-49 7 (9 0 - 110 ) AST M D482-O0 a 12/17-12/22/0 9 935149 7 (9 0 - 110 ) 0.4 8 (0-10 ) AST M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 Gros s calorifi c Valu e 10 0

9 9 W0#;-Q2K71AA-_CS/_Q2R7XAC-_CS D LC S _ofc-S_mple# : H9L140000-07 S

(9 8 - 102 ) (9 8 - 102 ) 0.0 8 {0-2 . Dilutio nFactor : 1 0 ) AST M D240-0 2 AST M D240-0 2 12/14/0 9

12/14/0 9 934807 5

934807 5
NOTE(S) : Calculation

s ar cperforme

d befor e roundin g t o avoi d round-of

f error s i ncalculate

d results .



### VES01868 6

### 3 8

LABORATOR

YCONTRO

L SAMPL E DAT A REPOR T Genera l Chemistr y Lot-Sampl e : H9L09042 3 Matrix..- . : WAST E SPIK E MEASURE

D PERCN

T PREPARATION- PRE P PARAMETE

RAMODN

T AMODN

T UNIT S RECVR

YRP D METHO

D ANALYSI S DAT E BATC H # As hConten t WO#:LQ91G1AC-LCS/LQ91G1AD-LCS D LCS Lot-Sample# : H9L170000-49 7 400 0 397 0 mg/k g 9 9 AST M D482-O0 a 12/17-12/22/0 9 935149 7 400 0 395 0 mg/k g 9 9 0.4 8 AST M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : l GrOS S Calorifi c WO # :LQ2R71AA-LCS/LQ2R71AC-LCS D LC S Lot-Sample# : H9L140000-07 5 valu e 2060 0 2050 0 BTU/l b10 0 AST M D240-0 2 12/14/0 9 934807 5 2060 0 2050 0 BTU/l b9 9 0.0 8 AST M D240-0 2 12/14/0 9 934807 5 Dilutio nFactor : 1 NOTE(S ) : ; Calculation

s ar e pcrrormc

d befor e roundinglo avoi

d round-of

T error s in calculate

d results .



### VES01868 7

### 39 .

LABORATOR

YCONTRO

L SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t #... : H9L09042 3 Matrix. - : WAST E PERCEN T RECOVER

YPREPARATION- PRE P PARAMETE

RRECOVER

YLIMIT S METHO D ANALYSIS'DAT E BATC

H # Tota l Chlorin e Wor k Orde r # : LQTX01A C LC S Lot-Sample# : H9L100000-OS O 10 0 (8 0 - 120 } KNO XWC-001 S 12/10-12/14/0 9 93440S 0 Dilutio nFactor : S Tota l Chlorin e Wor k Orde r # : LQXER1A C LC S Lot-Sample* : H9L110000-06 4 9 9 (8 0 - 120 ) KNOXWC-OOI S 12/H-1.2/1S/0 9 934506 4

Dilution . Factor : 5 NOTE(S ) : , Calculation

s ar cperforme

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



### VES01868 8

### 4 0

LABORATOR

YCONTRO

L SAMPL

E DAT A REPOR T Genera l Clteraistry Clien t Lo t H9LQ9042 3 Matri x: WAST E SPIK E MEASURE

D PERCN T PREPARATION - PRE P PARAMETE

RAMOUN

T AMOUN

T UNIT S RECVR YMETHO D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LQTX01A C LC S Lot-Sample# : H9L100000-OS O 1000 0 998 0 rng/k g 10 0 KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : S Tota l Chlorin e Wor k Orde r 4 : LQXER1A C LC S Lot-Samples. - H9L110000-06 4 1000 0 985 0 mg/k g 9 9 KNO

X WC-001 S X2/ll-12/16/0 9 934506 4 DilutionFactor : 5 NOT E (S ) ; Calculation

s ar cperforme

d befor e roundin g t o avoi d round-of

T error s i ncalculate

d results .



### VES01868 94 1

LABORATOR

YCONTRO

L SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L09042 3 Matri x: SOLI D
PARAMETE

R As hConten t PERCEN T RECOVER Y 10 0 10 0 RECOVER

Y LIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PRE P BATC H # W0#:LQ1E11AC-LCS/LQ1E11AD-LCS D LCS Lot-Sample# : H9L11OOO0-46 1 (9 0 - 110 } AST M D482-00 a 12/11-12/15/0 9 934546 1 (9 0 - 110 ) 0.4 2 (0-10 ) AST M D482-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor ; 1 Gros s Calorifi c Valu e 10 0

10 0 WO#:LQ5BPlAA-LCS/LQ58PlAC-LCSD LCS Lot-Sample# : H9L160000-03 2

(9 8 - 102 ) . AST M D5865-0 0 (9 8 - 102 ) 0.1 0 (0-2.0 ) AST M D5865-0 0 Dilutio nFactor : 1 12/16/0 9 12/16/0 9 935003 2

935003 2
NOTE(S ) : Calculation

s ar cperforme

d befor e roundin g t o avoi d round-of

f error s i ncalculate

d results .



### VES01869 0

### 4 2

LABORATOR

YCOHTRO

L SAMPL E DAT A REPOR T Genera l Chemistry Lot-Sampl e # : H9L09042 3 Matri x: SOLI D SPIK E MEASURE

D PERCN

T PREPARATION- PRE P PARAMETE

RAMOUN

T AMOUN

T UNIT S RECVR

YRP D METHO

D ANALYSI S DAT E BATC H # As hConten t W0#;LQ1E11AC-LCS/LQ1E11AD-LCS D LC S Lot-Sample* : H9L11O000-4S 1 400 0 401 0 mg/k g 10 0 AST M D482-00 a 12/11-12/15/0 9 934546 1 400 0 399 0 mg/k g 10 0 0.4 2 AST M D482-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor : 1 Gros s Calorifi c WO#:LQ58PlAA-LCS/LQ58PlAC-LCSD LC S Lot-Sample# : H9L160000-03 2 Valu e 1140 0 1130 0 BTU/l b10 0 AST M D5865-0 0 12/16/0 9 935003 2 '1140 0 1130 0 BTU/l b10 0 0.1 0 AST M D5865-0 0 12/16/0 9 935003 2 Dilutio nFactor : 1 NOTE(S ) : Calculation

s ar e performe

d befor e roundin

g t o avoi d round-of

f error s i ncalculate

d results .



### VES01869 1

### 4 3

MATRI XSPIK E SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t # . Dat e Sampled . , : H9L09042 3

. : 12/01/0 9 Dat e Received. . 12/04/0 9
PARAMETE

R Tota l Chlorin e

10 0 9 7 PERCEN T RECOVER

Y RECOVER

YLIMIT S RP

D RP D LIMIT S METHO

D Matrix . WAST E
PREPARATIO

N - ANALYSI S DAT

E PRE P BATC H # WO# : LQQNN1AG-MS/LQQNN1AH-MS D . M S Lot-Sampl e # : H9L090423-00 5 (8 0 - 120 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 (8 0 - 120 ) 3. 5 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 93440S 0 Dilutio nFactor : 7.0 7 Tota l Chlorin e W0# : LQQNT1AE-MS/LQQNT1AF-MS D M S Lot-Sampl e # : H9L090423-00 7 10 1 (8 0 - 120 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 10 1 (8 0 - 120 ) 3. 2 (0-10 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 7. 1 NOTE(S ) ; Calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i ncalculate

d results .



### VES01869 2

### 4 4

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l Chemi s try Clien t Lo t #... : H9L09042 3 Dat e Sanrpled... ; 12/01/0 9 Dat e Received._ : 12/04/0 9 Matrix . WAST E
SAMPL E SPIKE MEASR

D PARAMETE

RAMODN

T AM T Tota l Chlorin e

.825 1410 0 82 5 1400 0 AMOUNT . UNIT S PERCN T RECVR YRP D METHO

D PREPARATION - PRE P ANALYSI S DAT

E BATC H # WO# : LQQNNIAG-MS/LQQNNIAH-MS D M S Lot-Sampl e #.

- H9L090423-00 5 1500 0 mg/k

g 10 0 KNO XWC-001 6 12/10-12/14/0 9 934406 0 1450 0 mg/k

g 9 7 3. 5 KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 7.0 7 Tota l Chlorin e

49B 0 1420 0 498 0 1360 0 WO# : LQQNT1AE-MS/LQQNT1AF-MS D M S Lot-Sampl e # : H9L090423-00 7 1930 0 mg/k

g 10 1 KHO XWC-001 6 12/11-12/16/0 9 934506 4 1870 0 mg/k

g 10 1 3. 2 KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 7. 1 NOTE(S ) : Calculaiion

s ar cpcrrormc

d befor e roundin g i o avoi d round-of

f error s i ncalculate

d results .



### VES01869 3

### 4 5

MATRI XSPIK E SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t ft...; H9L09042 3 Dat e Sample d: 12/02/0 9 Dat e Received . 12/04/0 9 Matrix . SOLI D

PARAMETE

R Tota l Chlorin e

9 0 9 1 PERCEN T RECOVER

Y RECOVER YLIMIT S RP

D RP D LIMIT S METHO

D .PREPARATIONANALYSI S DAT

E PRE P BATC H # WO# : LQQQR1AG-MS/LQQQR1AH-MS D M S Lot-Sampl e # : H9LO90423-01 1 (8 0 - 120 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 (8 0 - 120 ) 0.7 7 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 4.7 3 NOTE(S ) : Calculaiion

s ar cperforme

d befor e roundin g t o avoi d round-of

T error s i ncalculaie

d results .



### VES01869 4

### 4 6

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l _enustr y Clien t Lo t #... : H9L09042 3 Dat e Sampled... : 12/02/0 9 Matrxx . SOLI D Dat e Received.. : 12/04/0 9 SAMPL E SPIK E . MEASR

D PARAMETE

RAMOUN

T AM T Tota l Chlorin e

10 5 947 0 10 5 945 0 AMODN T UNITS PERCN T RECVR YRP D METHO

D PREPARATION - PRE P ANALYSI S DAT

E BATC H # WO# : LQQQR1AG-MS/LQQQR1AH - MS D M S Lot-Sampl e # : H9L090423-01 1 864 0 mg/k

g 9 0 KNO XWC-001 6 12/10-12/14/0 9 934406 0 871 0 mg/k

g 9 1 0.7 7 KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 4.7

3 NOTE(S ) : Calculation

s ar e performe

d befor e roundin

g t o avoi d round-of

f error s i ncalculate

d results .



### VES01869 5

### 4 7

SAMPL E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Clien t Lo t #... : H9L09042 3 Wor k Orde r #... : LQQNN-SM P Matri x: WAST E LQQNN-DU

P Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 DUPLICATE RP D PREPARATION- PRE P PARA M RESULT RESUL

T UNIT S RP

D LIMI T METHO

D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L090423-00 5 Valu e N D N

D BTU/l b1 3 (0-10 ) AST M D240-0 2 12/14/0 9 9348D7 5 Dilutio nFactor : 1 As hConten t S D Lot-Sampl e # : H9L090423-00 5 117 0 121 0 mg/kg 3. 1 (0-10 ) AST M D4B2-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 Tota l Chlorin e S D Lot-Sampl e # : H9L090423-00 5 82 5 81 8 mg/k g 0.8 2 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1.3 3



### VES01869 6

### 4 8

Clien t Lo t S-. . Dat e Sampled.. . PARA M RESULT Tota l Chlorin e 498 0 H9L09042 3

12/01/0 9 DUPLICATE RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQQNT-SM P LQQNT-DU

P Dat e Received.. : 12/04/0 9
UNIT S RP

D RP D LIMI T METHO

D Matrxx . WAST E

PREPARATION

- PRE P ANALYSI S DAT

E BATC H 8 S D Lot-Sampl e # : H9L090423-00 7 S00 0 mg/k

g 0.4 2 (0-10 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor s 1.3 6



### VES01869 7

### 4 9

Clien t Lo t #-. . Dat e Sampled.. . PARA M RESUL T SAMPL E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y H9L09Q42 3 Wor k Orde r #...

t LQQQR-SM

P LQQQR-DU

P 12/02/0 9 Dat e Received.. : 12/04/0 9

Tota l Chlorin e 10 5 B DUPLICAT E RESUL T UNIT S 99. 6 B RP D RP D LIMI T METHO

D Matri x: SOLI D

PREPARATION- PRE

P ANALYSI S DAT

E BATC H # mg/k g 5. 3 Dilutio nFactor : 1.0 2 SD Lot-Sampl e # : H9L090423-01 1

(0-10 ) KNO

XWC-001 6 12/10-12/14/0 9 934406. 0
Gros s Calorifi c Valu e N D N

D BTD/l b0

Dilutio nFactor : 1 S D Lot-Sampl e # : H9L090423-01 1 (0-10 ) AST

M D5865-0 0 12/15/0 9 935003 2
As hConten t 80100 0 78400 0 mg/k g Dilutio nFactor : 1 S D Lot-Sampl e # : H9L090423-01 1 2. 2 (0-10 ) AST

M D482-O0a 12/11-12/15/0 9 934546 1
NOTE(S ) : Calculation

s ar cperforme

d befor e roundin g t o avoi d round-of

f error s i ncalculate

d results . B Estimate

d result , Resul ti s les s tha n RL ,



### VES01869 8

### 5 0

SAMPL E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Clien t Lo t H9L09042 3 Wor k Orde r #... : LQQRO-SM P Matri x.. : WAST E LQQRO-DU

P Dat e Sample d: 12/03/0 9 Dat e Received.. : 12/04/0 9 DUPLICATE RP D PREPARATION- PRE P PARA M RESULT RESUL

T UNIT S RP

D LIMI T METHO

D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L090423-01 5 Valu e 1030 0 1010 0 BTU/l b1. 4 (0-10 ) AST M D240-0 2 12/14/0 9 934807 5 Dilutio nFactor : 1



### VES01869 9

### 5 1

Clien t Lo t #... : H9L09042 3 Dat e Sampled: 12/02/0 9 SAMPL E DDPLICATE EVALUATIO N EEPOR T Genera l Chemistr y Wor k Orde r #... : LQQTC-SM P LQQTC-DU

P Dat e Received.. : 12/04/0 9
PARA M RESULT Tota l Chlorin e 501 0 DUPLICATE

RESUL T 510 0 Matrxx . WAST E

• UNIT S RP

D RP D LIMI T METHO

D PREPARATION - PRE P ANALYSI S DAT

E BATC H # S D Lot-Sampl e # : H9L090423-02 0 mg/k g 1. 9 (0-10 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 7



### VES01870 0

### 5 2

Clien t Lo t # . Dat e Sampled . PARA M RESUL T As hConten t 782 0 H9L09042 3

12/03/0 9 DUPLICAT

E RESUL T . SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQQTD-SM P LQQTD-DU

P Dat e Received.. t 12/04/0 9
UNIT S RP

D RP D LIMI T METHO

D Matrix . WAST E

591 0 rag/kg 1 2

Dilutio nFactor : 1 PREPARATION- PRE P ANALYSI S DATS BATC H # S D Lot-Sampl e # : H9L090423-02 1 (0-10 ) AST

M D482-00 a 12/17-12/22/0 9 935149 7



### VES01870 1

### 5 3



### 1



# Sample Receip t

Documentatio n

VES01870 2

### Sampl e Traceabilit yLis t 

## AECO M

Sit e o f Proqram : Veoli aE S Tec h Sampl e Date : &/

i- (ZtAfoR Projec tLocation : Sauqet , I L P.O.# : Typ e o f Program : CP T Dat e Shipped : 1^tJ.jnlhff Laboratory : TestAmerica , Inc . Knoxville , TN Project * 60133216 Proqram Office : Syracus e N Y Shipper/

Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica , Inc . Knoxville , TN Program Contact : Jef f Gorma n FedE xAi rBil l #

: Ite m Sampl e 1 0 Cod e Sampl

e Matri x Sampl e Descriptio

n Analitlca l Parameter

s Specia l Instruction

s 2 1 M HBTU-U3-M26-R 1 Liqui d Hig

h Btu , Uni t3, Ru n1 Physica l Parameter

s & C l 2 2 x HBTU-U3-WI26A-R 2 Liqui d Hig

h Btu, Uni

t3, Ru n2 Physica l Parameter

s & C l 2 3 > HBTU-U3-M26A-R 3 Liqui d Hig

h Btu , Uni t3 , Ru n3 Physica l Parameter

s & C l 24 2 5 iv < LBTU-U3-M26A-R 1 Liqui d Lo

wBtu , Uni t3 Ru n1 Physica l Parameter

s & C l

### \C > fHTfi)& 2 6 x L.BTU-U3-M26A-R 2 Liqui d Lo

wBtu , Uni t3 Ru n2 Physica l Parameter

s & Cr ^Ofijr ; 

### $ ]



### ^ 27 iLBTU-U3-M26A-R 3 Liqui d Lo

wBtu , Uni t3 Ru n3 Physica l Parameter

s & C l 

### f

? J5 5 2 8 * 5 2 9 U- tSF-U3-WI26A-R 1 Liqui d Specialit

y Feeder , Uni t3 , Ru n1 Physica

l Parameter

s & C l §/,

A 

### I * 5 3 0 % SF-U3-M26A-R 2 Liqui d Specllait

y Feeder , Uni t3, Ru n2 Physica

l Parameter

s & C l ftf p £ 3 1 ^ SF-U3-M26A-R 3 Liqui d Specialit

y Feeder , Uni t3, Ru n3 Physica

l Parameter

s & C l ft| f£\ £ 3 2 3 3 CS-U3-M26A-R 1 Soli d Containerize d Solids, Uni

t3, Ru n1 Physica

l Parameter

s & Clfi f n C\\ 0e 34 \

CS-U3-WI26A-R 2 Soli d Containerize d Solids, Uni

t3 , Ru n2 Physica

l Parameter

s & C l $}j)0[

[ft t -2.-1*3 1 3 5 V CS -U3-M26A-R 3 Soli d Containerize d Solids, Uni

t3, Ru n3 Physica

l Parameter

s & CIQ j„tPl

\ A t=; 3 6 . 8 ^ 

### t

. 37 3 8 39 4 0 Fiel d Notes

/ Comment

s 1. Physica l Parameter

s = Tota l chlorides, hea

tconten t5 ash content

. 2 . C l Pag e 2 o

f 2
_ Relinquishe

d By (print) : Date: . Signature : > Time : 

### Xto,j&r, riyuL!~7O0 Relinquishe d B y (print) : Date : Signature : Time : Relinquishe d By (print) : Date: Signature : Time : Receive d b y La b (print) : Date : \ n,\A\\

Received B

y (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Analytica l Laboralor

vDestination : TestAmericaInc

. 5815 Middlebroo

kPik e Knoxville , T N 3792

1 Attn : Mr , Kevi n Woodcoc

k865-291-300

0


### VES01870 3

### Sampl e Traceabilit yLis t 

## AECO M
Sit e o f Program : Veoli aE S Tec h Sample Date : t .±j /icf- AZ/JM^ Projec tLocation : Saupjet , I L P.O . * Typ e of Program : CP T Dat e Shipped : /Jl/j

} Jo 9 Laboratory : TestAmerica , Inc . Knoxville , TI M Project * 60133216 Shipper/ Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica , Inc . Knoxville , TI M Program Office : Syracuse N Y Shipper/

Steve n Mil o Recovery : Jef f Gorma n Laboratory : TestAmerica , Inc . Knoxville , TI M Program Contact : Jef f Gorma n • - ;: v--y.' ' • ' " ! '.:. : - ' • FedExAi rBill * Ite m Sampl e I D Cod e Sampl

e Matri x Sampl e Descriptio

n Analitica l Parameter

s Specia l Instruction

s 1 HBTU-U3-M23A-R 1 - Liqui d Hig

h Btu , Uni t3 , Ru n1 Physica l Parameter

s & C l 2 HBTU-U3-M23A-R 2 x Liqui d Hig

h Btu. Uni

t3 , Ru nZ Physica l Parameter

s & C l 3 HBTU-U3-M23A-R 3
_ Liqui d Hig

h Btu, Uni

t3, Ru n3 Physica l Parameter

s & C l 4 5 LBTU-U3-IW23A-R 1 Liqui d Lo

wBtu , Uni t3 Ru n1 Physica l Parameter

s & C l 6 L .BTU -U3-M23A-R 2 Liqui d Lo

wBtu , Uni t3 Ru n2 Physica l Parameter

s & Cl 7 LBTU-U3-M23A-R 3 - Liqui d Lo

wBlU, Uni

t3 Ru n3 Physica l Parameter

s & C l 8 9 SF-U3-M23A-R 1 Liqui d Specialit

y Feeder , Uni t3 , Ru n1 Physica

l Parameter

s & C l 10 SF-U3-M23A-R 2 Liqui d Specilait

y Feeder , Uni t3 , Ru n2 Physica

l Parameter

s & C l 11 SF-U3-WI23A-R 3 Liqui d Specialit

y Feeder , Uni t3, Ru n3 Physica

l Parameter

s & C l 1 2 1 3 CS-U3-M23A-R 1 Soli d Containerize d Solids , Uni

t3, Ru n1 Physica

l Parameter

s & C I 14 CS-U3-M23A-R 2 Soli d Containerize d Solids, Uni

t3, Ru n2 Physica

l Parameter

s & C l 1 5 CS-U3-M23A-R 3 Soli d Containerize d Solids, Uni

t3, Ru n3 Physica

l Parameter

s & Cl 1 6 1 7 18 1 9 2 0 Fiel d Notes

/ Comment

s 1 . Physica l Parameter

s = Tota l chlorides, hea

tconten t& as h content . 2. C l Page 1 of_ 2 Relinquishe

d B y (print) : Date : llRelinqulsbe d B y (print) : Date : Signature : Time : [Signature : Time : (700 

## 1 Relinquishe d B y (print) : Date : Signature : Time : ^ ~ Receive d b y La b (print) : Date : 

## ~%U tbVYMT- H rUij M femA fflffe Received B

y (print) : Date : IjReceive d B y (print) : Date : Signature : Time : Signature : Time : Receive d B y (print) : Date: Signature : Time : Analytica l Laborator

y Destination : Received B

y (print) : Date : IjReceive d B y (print) : Date : Signature : Time : Signature : Time : Receive d B y (print) : Date: Signature : Time : Tes tAmeric aInc . 581 5 Middlebroo

kPik e Knoxville , T N 3792

1 Attn : Mr . Kevi nWoodcoc

k865-291-300

0 O l 

### VES01870 4

### TESTAMERIC A KNOXVILL E SAMPL E RECEIPT/CONDITIO N UPO N RECEIP T ANOMAL Y CHECKLIS T Lo tNumber : VWUflMaT . Revie wItem

s f N A If No , wha

twas the problem ? Comments/Action s Take n 1 . D o sampl

e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

1- • l aD o no tmatc h CO C
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treceived
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e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

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n • leN o labe

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treceived
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e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

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treceived
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# J

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e infonnation 0 l cMarkin gsmeare

d O l d Label tor

n • leN o labe

l
• UCO C no

treceived
• l g Other : 1 . D o sampl

e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

1- • l aD o no tmatc h CO C
• l b Incomplet

e infonnation 0 l cMarkin gsmeare

d O l d Label tor

n • leN o labe

l
• UCO C no

treceived
• l g Other : 1 . D o sampl

e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

1- • l aD o no tmatc h CO C
• l b Incomplet

e infonnation 0 l cMarkin gsmeare

d O l d Label tor

n • leN o labe

l
• UCO C no

treceived
• l g Other : 1 . D o sampl

e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

1- • l aD o no tmatc h CO C
• l b Incomplet

e infonnation 0 l cMarkin gsmeare

d O l d Label tor

n • leN o labe

l
• UCO C no

treceived
• l g Other : 1 . D o sampl

e containe

rlabel s matc h COC ? (IDs , Dates , Times ) 

# J

1- • l aD o no tmatc h CO C
• l b Incomplet

e infonnation 0 l cMarkin gsmeare

d O l d Label tor

n • leN o labe

l
• UCO C no

treceived
• l g Other : 2. I s th e coolertemperatur

e withi n limits ? (

> freezin g temp , o f wate rt o 6°C;NC , 1668,1613B : 0-4°C ; VOST : 10°C;MA:2-6' , C ) 

# J • 2aTeni D Blank= 2. I s th e coolertemperatur

e withi n limits ? (

> freezin g temp , o f wate rt o 6°C;NC , 1668,1613B : 0-4°C ; VOST : 10°C;MA:2-6' , C ) 

# J 0 2 b Coole rTem p = 2. I s th e coolertemperatur

e withi n limits ? (

> freezin g temp , o f wate rt o 6°C;NC , 1668,1613B : 0-4°C ; VOST : 10°C;MA:2-6' , C ) 

# J J . Wer e sample

s received wit

h correc tchemica

l preservative (excluding Encore) ? 

# J • 3 aSample preservativ e = 

### J J . Wer e sample

s received wit

h correc tchemica

l preservative (excluding Encore) ? 

# J • 3 aSample preservativ e = 

### J 4 . Were custod

y seal s present/intac

to ncoole rand/or containers ? 

### y •ff l 4aNo tpresen

t • 4b Na tintac

t 0 4 cOther : 4 . Were custod

y seal s present/intac

to ncoole rand/or containers ? 

### y •ff l 4aNo tpresen

t • 4b Na tintac

t 0 4 cOther : 4 . Were custod

y seal s present/intac

to ncoole rand/or containers ? 

### y •ff l 4aNo tpresen

t • 4b Na tintac

t 0 4 cOther : 5 . Were all o f

th esample

s listed on th

e CO C received ? 

### J

I • 5aSample s received-no

ton CO C 0 5 b Sample

s no treceived-o

n CO C 5 . Were all o f

th esample

s listed on th

e CO C received ? 

### J

I • 5aSample s received-no

ton CO C 0 5 b Sample

s no treceived-o

n CO C 6 . Wer e al l o f

th e sample container

s received intact? 

# 1 1 • 6 aLeakin g • fib Broken 6 . Wer e al l o f

th e sample container

s received intact? 

# 1 1 • 6 aLeakin g • fib Broken 7. Wer e VO A sample s received withou

theadspace? 

### -L 4 0 7aHeadspac e (VO A only) 8 . Wer e sample

s received inappropriat e containers ? 

# J _.. / 0 8aImprope rcontaine

r 9 . Di d you chec

kfo rresidua

l chlorine , i f

necessary ? 

# / • 9 aCoul d no tb e determine

d du e t o matri xinterferenc

e 9 . Di d you chec

kfo rresidua

l chlorine , i f

necessary ? 

# / • 9 aCoul d no tb e determine

d du e t o matri xinterferenc

e 10. Wer e sample

s received within holding time ? • 10 aHoldin g tim

e expired 11 . Fo rra

d samples , wa

s sampl e activit y info , provided ? 

# J • Incomplet e information 12. Fo r16I3B wate

rsample s i s pH<9 ? If no , wa s p Hadjuste

d t o p H7 - 9 wit h sulfuri cacid ? 12. Fo r16I3B wate

rsample s i s pH<9 ? If no , wa s p Hadjuste

d t o p H7 - 9 wit h sulfuri cacid ? 13. Ar e th

e shipping container

s intact ? 

# J D 13 n Leakin g D 13b Other : 13. Ar e th

e shipping container

s intact ? 

# J D 13 n Leakin g D 13b Other : 14. Wa s CO C relinquished ? (Signed/Dated/Timed) 

# J • 14 aNo trelinquished 15. Ar e tests/parameter s listed fo reac

h sample ? • 15 aIncomplet

e information 16 . I s th e matri xofth e sample

s noted ? 

# i 0 15aIncomplet e information 17 . I s th e date/tim

e o f sample coliection noted? / 015 aIncomplet e information 18 . I s tlie clientan

d projec tname/ #identified ? 

### / • 15 aIncomplet

e infonnation 19. Wa s th

e sample ridentified o n th

e COC ? 7 Quote* : *— . P M Instructions : 

### 1 ;—MrV ^ e s a > — • Sampl e Receivin g Associate : 

### l ^jT^Y^H ^ Date:/X | f ^O^ QA026R21.doc , 09040 9



### VES01870 5

### 5 7



# We t Chemistr

y

VES01870 6

### 5 8



# Sampl e Summar

y

VES01870 7

### 5 9

Lot-Sampl e # . Dat e Sampled . PARAMETE

R AECOM , In c Clien t Sampl e ID : HBTO-U3-M2S-R 1 Genera l Chemistr y H9L090423-OQ1 Wor k Orde r #... : LQQM

7 12/01/0 9 Dat e Received.. : 12/04/0 9 Matri x: WAST E

RESUL T R L ONIT S As bConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 83 5 20 0 mg/k g Dilutio nFactor : 1 1050 0 180 0 BTTj/l b

Dilutio nFactor : X 19200 , 187 0 mg/k g Dilutio nFactor : 9.3 5 _METHO D AST M D482-00 a MD L : 5 1 AST M D240-0 2
HD L 13 0 KNO XWC-001 6 MD L t 56 0 PREPARATION- PRE P ANALYSI S DAT

E BATC H ft 12/17-12/22/0 9 935149 7
12/14/0 9 934807 5
12/10-12/14/0 9 934406 0



### VES01870 8

### 6 0

AECOM , m c Clien t Sampl e ID : HBT0-O3-M26-R 2 Genera l Chemistr y lK3t-Sampl e #... : H9L090423-00 2 Wor k Orde r #.. . : LQQN

H Matri x: WAST E Dat e Sampled.. . : 12/02/0 9 Dat e Received . - : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As nConten t 56 6 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : S I Gros s Calorifi c 1020 0 180 0 BT(J/Xt> JSSI M D2«O-O 2 12/14/0 9 S34807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Cnlorin e 1470 0 120 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : S MD L : 36 0



### VES01870 9

### 61

AECOM , Ul C Clien t Sampl e ID : HBTU-TJ3-M2S-E 3 Genera l Chemistr y Lot-Sampl e #--. : H9L090423-00 3 Wor k Orde r #... : LQQN J Dat e Sampled... : 12/03/0 9 Dat e Received. ,
PARAMETE

R RESUL

T R L UNIT S 12/04/0 9

METHO D Matri x: WAST E
PREPARATION- PRE

P ANALYSI S DAT

E BATC H # As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 52 7 20 0 mg/k g Dilutio nFactor : 1 1030 0 180 0 BT0/X b Dilutio nFactor : 1 1670 0 167 0 mg/k g Dilutio nFactor : 8.3 5 AST M D482-00 a MD L : 5 1 AST M D240-0 2
MD L : 13 0 KNO XWC-001 6 MD L : 5D0 12/17-12/22/0 9 935149 7 12/14/0 9 934807 5
12/10-12/14/0 9 934406 0



### VES01871 0

### 6 2

AECOM , In c Clien t Sampl e ID : LBTD-U3-M26-R 1 Genera l Chemistr y Lot-Sampl e #... : H9L090423-00 4 Wor k Orde r ft...: LQQN

L Matrxx . WAST E Dat e Sampled... : 12/01/0 9 Dat e Received .

PARAMETE R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 123 0 20 0 mg/k g Dilutio nFactor : 1
M D 180 0 BTU/l b

Dilutio nFactor : 1 87 3 28 2 mg/k g Dilutio nFactor : 1.4 1 12/04/0 9

_METHO D AST M D482-00 a MD L : 5 1 AST M D240-0 2
MD L : 13 0 KNO XWC-001 6 MD L : B

5 PREPARATION- PRE P ANALYSI S DAT

E BATC H ft 12/17-12/22/0 9 93S149 7 12/14/0 9 934807 5
12/10-12/14/0 9 934406 0



### VES01871 1

### 6 3

AECOM , In c Clien t Sampl e ID : LBTU-D3-M26-R 2 Genera l Chemistr y Lot-Sampl e # . .. : H9L090423-00 5 Wor k Orde r # . .. : LQQN N Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 Matri x: WAST E

PARAMETE

R RESUL

T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Ojlorin e 117 0 20 0 mg/k g Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 82 5 27 8 mg/k g Dilutio nFactor : 1.3 9 _METHO D AST M D482-00 a MD L : 5 1 AST M D240-0 2
MD L : 13 0 KNO XWC-001 6 HD L : 8 3 PREPARATION - PRE P ANALYSI S DAT

E BATC H # 12/17-12/22/0 9 935149 7 12/14/0 9 934807 5
12/10-12/14/0 9 934406 0



### VES01871 2

### 6 4

AECOM , In c Clien t Sampl e ID : I3TU-U3-M26-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L.090423-00 6 Wor k Orde r #... : LQQN P Matri x: WAST E Dat e Sampled.12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC

H # As hConten t 256 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 HD L : 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 125 0 28 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1. 4 MD L : 8 4



### VES01871 3

### 6 5

AECOM , In c Clien t Sampl e ID : SF-U3-M26A-R 1 Genera l Chemistr y Lot-Sampl e #.... - H9L090423-00 7 Wor k Orde r : LQQN T Matri x: WAST E Dat e Sample d: 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESDL T R

L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 760 0 20 0 mg/k g AST

M D4B2-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D 1B0 0 BTU/l bAST M D240-0 2 12/14/0 9 934B07 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 498 0 27 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 6 MD L : 3 2



### VES01871 4

### 6 6

AECOM , In c Clien t Sampl e ID : SF-U3-M26A-R 2 Genera l Chemistr y Lot-Sampl e #. . H9L090423-00 8 Wor k Orde r : LQQN O Matri x: WAST E Dat e Sample d: 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 562 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c N D IBO O BTo/i bAST M 0240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 502 0 28 4 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 2 MD L : B

5



### VES01871 5

### 6 7

AECOM , In c Clien t Sampl e ID : SF-TJ3-M26A-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-0O9 Wor k Orde r #... : LQQN 2 Matri xr WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D . ANALYSI S DAT E BATC H # As hConten t S02 0 20 0 mg/k g AST

M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor:' 1 MD L : 5 1 Gros s calorifi c H D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 509 0 28 2 mg/k g KNO

XWC-0016 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 1 MD L : B

S



### VES01871 6

### 6 8

AECOM , In c Clien t Sampl e ID : CS-U3-M26A-R 1 Genera l Chemistr y Lot-Sampl e : H9L090423-01 0 Wor k Orde r #..- : LQQN 4 Matri x: SOLID Dat e Sampled... : 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC

H # As hConten t 69900 0 20 0 mg/k g AST

M D482-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor ; 1 MD L : S I GrOS S Calorifi c N D 1B0

Q BTU/l bAST M DSBSS-O O12/16/0 9 935003 2 Valu e Dilutio nFactor. - 1 MD L : 13 0 Tota l Chlorin e 23 9 20 4 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1.0 2 MD L : 6 1



### VES01871 7

### 6 9

AECOM , In c Clien t Sampl e ID : CS-D3-M26A-R 2 Genera l Chemistr y Lot-Sampl e #.. . : H9L090423-01 1 Wor k Orde r #..- : LQQQ

RMatri x: SOLI D Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t B0100 0 20 O mg/k

g AST

M D4B2-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor : 1 MD L : S I Gros s Calorifi c N D xsoo BTO/I_ > AST M DSRES-O O12/16/0 9 935003 2 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 10 5 B 20 4 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1.0 2 MD L i 6 1 MOTE(S ) : R L Reportin

g Limi t B Estimate

dresult . Resul

t i s les s tha nRL .



### VES01871 8

### 7 0

AECOM , In c Clien t Sampl e IDs CS-03-M2SA-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-01 2 Wor k Orde r LQQQ

W Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 Matri x: SOLI D

PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T R L UNIT S 79900 0 20 0 mg/k g Dilutio nFactor : 1 ND 180 0 BTa/l b

Dilutio nFactor. - 1 74. 9 B 20 0 mg/k g Dilutio nFactor : 1 _METHO D AST M D482-00 a MD L : 5 1 AST M DSSSS-0 0
MD L : 13 0 KNO XWC-001 6 MDL . : 6 0 PREPARATION- PRE P ANALYSI S DAT

E BATC H # 12/11-12/15/0 9 934546 1
12/16/0 9 935003 2
12/10-12/14/0 9 934406 0 HOTE(S) : R L Reportin

g Limi t B Estimate

d result . Resul ti s les s tha n RL .



### VES01871 9

### 71

Lot-Sampl e if.. . Dat e Sampled.. .
PARAMETE

R As hConten t
Gros s Calorifi c valu e
Tota l Chlorin e AECOM , rn c Clien t Sampl e ID : HBTTT-D3-K23A-R 1 Genera l Chemistr y H9L090423-01 3 Wor k Orde r : LQQQ

7 12/01/0 9 Dat e Received.. : 12/04/0 9 Matri x: WAST E

RESUL T R L DNIT S 93 7 20 0 mg/k g Dilutio nFactor : 1 1040 0 X8O 0 BTTJ/X b

Dilutio nFactor : 1 2060 0 167 0 mg/k g Dilutio nFactor : 8.3 4 _METHO D AST M D482-00 a MD I 5 1 AST M D240-0 2
MD L : 13 0 KHO XWC-001 6 MD L : 50 0 PREPARATION - PRE P ANALYSI S DAT

E BATC H # 12/17-12/22/0 9 935149 7 12/14/0 9 934807 5
12/11-12/16/0 9 934506 4



### VES01872 0

### 7 2

AECOM , Iii c Clien t Sampl e ID : HBTO-D3-M23A-R 2 Genera l Chemistr y Lot-Sampl e #.-- : H9L090423-01 4 Wor k Orde r #... : LQQR

M Matrix . WAST E Dat e Sample d: 12/02/0 9 Dat e Received . 12/04/0 9
PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 58 8 20 0 mg/k g Dilutio nFactor : 1 1030 0 180 0 BTO/l b

Dilutio nFactor : 1 1470 0 172 0 mg/k g Dilutio nFactor : 8.6 2 _METHO D AST M D482-O0 a HD L : 5 1 AST M D240-0 2
MD L : 13 0 KNO XWC-001 6 MD L : 52 0 PREPARATION- PRE P ANALYSI S DAT

E BATC H # 12/17-12/22/0 9 935149 7
12/14/0 9 934807 5
12/11-12/16/0 9 934506 4



### VES01872 1

### 7 3

AECOM , In e Clien t Sampl e ID : HBT0-U3-M23A-R 3 Genera l Chemistr y Lot-Sampl e tt. . . : H9L090423-01 5 Wor k Orde r #... : LQQR

O Matri x: WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H j t As hConten t 53 5 20 0 mg/k g AST

M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calori-i c 1030 0 XSD O BTtr / l bAST M D240-0 2 12/14 /0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 1690 0 168 0 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 8. 3 9 MD L : 50 0



### VES01872 2

### 7 4

Lot-Sampl e #. . Dat e Sampled. .
PARAMETE

R Ash . Conten t
Gros s Calorifi c Valu e
Tota l Chlorin e AECOM , In c Clien t Sampl e ID : LETD-D3-M23A-R 1 Genera l Chemistr y H9L090423-01 6 Wor k Orde r # . - - : LQQR 6 Matri x: WAST E 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H f 122 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : S I N D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Dilutio nFactor : 1 MD L : 13 0 81 S 27 6 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 8 MD L : 8 3



### VES01872 3

### 7 5

AECOM , In c Clien t Sampl e ID : IflTTMB-M23A-R 2

Genera l Chemistr y Lot-Sampl e : H9L090423-01 7 Wor k Orde r #... : LQQR 7 Matri x: WAST E Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 126 0 20 0 mg/k g AST

M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s Calorifi c ND180 0 BTD/i bAST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 73 8 28 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 1 MD L : 8 5



### VES01872 4

### 7 6

AECOM , In c Clien t Sampl e ID : I_TD-D3-M23A-E3

Genera l Chemistr y Lot-Sampl e #... : H9L090423-01 8 Wor k Orde r #... : LQQR 8 Matri x: WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 242 0 20 0 rag/kg AST M D482-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : 5 1 Gros s calorifi c N D IBO O BTU/I

_AST M D240-0 2 12/14/0 9 934807 5 Valu e Dilutio nFactor : 1 MD L : 13 0 Tota l Chlorin e 123 0 28 2 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.4 1 MD L : B

5



### VES01872 5

### 7 7

Lot-Sampl e tt.. Dat e Sampled. .
PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l C_lorin e AECOM , In c Clien t Sampl e ID : SF-D3-M23A-R 1 Genera l Chemistr y H9L090423-01 9 Wor k Orde r LQQT

A Matri x: WAST E 12/01/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # 729 0 20 0 mg/k g AST

M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor ; 1 MD L : 5 1 N D 180 0 BTU/l bAST M D240-0 2 12/14/0 9 934807 5 Dilutio nFactor : 1 MD L : 13 0 503 0 27 4 mg/k g KHO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 7 MD L : 8 2



### VES01872 6

### 7 8

Lot-Sampl e #. . Dat e Sampled. ,
PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e AECOM , in c Clien t Sampl e UJ : SF-D3-M23A-R 2 Genera l Chemistr y H9L090423-02 0 Wor k Orde r : LQQT C Matri x: WAST E 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE

P RESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC

H # 695 0 20 0 mg/k g AST

M D4B2-O0 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 MD L : S I N D 180 0 BTU/r bAST M D240-0 2 12/14/0 9 934B07 5 Dilutio nFactor : 1 MD L : 13 0 501 0 27 4 mg/k g KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 7 MD L : 6 2



### VES01872 7

### 7 9

AECOM , In c Clien t Sampl e ID : SF-U3-M23A-R 3 Senera l Chemistr y Lot-Sample*... : H9L090423-02 1 Wor k Orde r #... : LQQT D Matri x: WAST E Dat e Sampled... : 12/03/0 9 Dat e Received.. : 12/04/0 9 PREPARATION- PRE P PARAMETE

RRESUL

T R L UNIT S METHO D ANALYSI S DAT E BATC H # AS hConten t 782 0 20 0 mg/k g AST

M D482-0O

a 12/17-12/22/0 9 935149 7 Dilutio nFactor s 1 MD L : 5 1 Gros s Calorifi c N D 180 0 BTU/I_ > AST M D_40-O

_12/14/0 9 934807 5 Valu e Dilutio nFactor ; 1 MD L : 13 0 Tota l Chlorin e 502 0 27 2 mg/k g KNO

XWC-001 6 12/11-12/1G/0 9 934506 4 Dilutio nFactor : 1.3 6 MD L : 8 2



### VES01872 8

### 8 0

AECOM , In c Clien t Sampl e ID : CS-U3-M23A-R 1 Genera l Chemistr y Lot-Sanrpl e #... : H9L090423-02 2 Wor k Orde r #.-- : LQQT

E Matrox . SOLI D Dat e Sampled... : 12/01/0 9 Dat e Received . 12/04/0 9
PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 71100 0 20 0 mg/k g Dilutio nFactor : 1 N D 180 0 BTO/l b

Dilutio nFactor : 1 22 0 20 0 mg/k g Dilutio nFactor : 1 METHO D AST M D482-00 a MD L : S I
AST M DS86S-0 0
MD L : 13 0 KNO XWC-001 6 MD L : €

0 PREPARATION- PRE P ANALYSI S DAT

E BATC H # 12/11-12/15/0 9 934545 1

12/16/0 9 935003 2
12/10-12/14/0 9 934406 0



### VES01872 9

### 81

AECOM , In c Clien t Sample " ID : CS-U3-M23A-R 2 Genera l Chemistr y Lot-Sampl e #... : H9L090423-02 3 Wor k Orde r #.-- : LQQT F Matri x: SOLID Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 PREPARATION - PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 70300 0 20 0 mg/k g AST

M D482-O0 a 12/11-12/15/0 9 93454S 1 Dilutio nFactor : 1 HD L r 5 1 Gros s Calorifi c N D 180 0 BTU/l bAST M DSS6S-0 0 12/lS/0 9 935003 2 Valu e Dilutio nFactor : 1 MD L : ' 13 0 Tota l Chlorin e 29 5 20 0 mg/k g KNO

XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1 MD L : 6 0



### VES01873 0

### 8 2

AECOM , In c Clien t Sampl e ID : CS-D3-M23A.-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L090423-02 4 Wor k Orde r #.. . : LQQT

G Matrix . SOLID Dat e Sampled... : 12/03/0 9 Dat e Received. . 12/04/0 9
PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 70300 0 20 0 mg/k g Dilutio nFactor : 1 N D 180 0 BTU/l b

Dilutio nFactor : 1 33 9 20 4 mg/k g Dilutio nFactor : 1.0 2 _METHO D AST M D482-00 a MD L : 5 1 AST M D5865-0 0
MD L : 13 0 KNO XWC-001 6 MD L : €

1 PREPARATION- PRE P ANALYSI S DAT

E BATC H # 12/11-12/15/0 9 934546 1
12/16/0 9 935003 2
12/10-12/14/0 9 934406 0



### VES01873 1

### 8 3

### 8 4

Clien t Lo t H9L09042 3
PARAMETE

R As hConten t

Tota l Chlorin e

Tota l Chlorin e RESUL T N O

N D

N D METHO D BLAN KREPOR T Genera l Chemistr y

REPORTIN

G LIMI T UNIT S METHO D Matrxx . WAST E PREPARATION- PRE

P ANALYSI S DAT

E BATC H # Wor k Orde r # : LQ91G1A A M B Lot-Sampl e # : H9L170000-49 7 20 0 mg/k

g Dilutio nFactor : 1 AST M D482-00 a 12/17-12/22/0 9 935149 7
Wor k Orde r # : LQTX01A A M B Lot-Sampl e # : H9L100000-OS O 20 0 mg/k

g Dilutio nFactor. - 1 KNO XWC-001 6 12/10-12/14/0 9 934406 0
Wor k Orde r # : LQXERIA A M B Lot-Sampl e # : H9L110000-06 4 20 0 mg/k

g Dilutio nFactor : 1 KNO XWC-001 6 12/11-12/16/0 9 934506 4 NOTB(S) : Calculation

s ar cperforme

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01873 3

### 8 5

METHO D BLAN KEEPOR T Genera l C-eraistr y Clien t Lo t #.. . H9L09042 3 Matrxx . SOLID
PARAMETE

R As hConten t RESUL T N D REPORTIN

G LIMI T UNIT S METHO D PREPARATION - PRE P ANALYSI S DAT

E BATC H # Wor k Orde r ft: LQ1E11A A M B Lot-Sampl e # : H9L110000-4G 1 20 0 mg/k

g AST

M D482-O0 a 12/11-12/15/0 9 934546 1 Dilutio nFactor. - 1 NOTE(S) : Calculation

s ar e performe

d befor e roundin

s ( 0 avoi d round-of

f error s i n calculate

d results .



### VES01873 48 6

LABORATOR

YCOHTROL SAMPL E EVALUATION REPORT Genera l Chemistr y Lot-Sampl e #... : H9L09042 3 Matrix .
PARAMETER As hConten t PERCENT

RECOVER

Y 9 9 99 RECOVER Y LIMIT S RPD RPD LIMIT S METHO

D PREPARATION ANALYSI S DAT E : WAST E

PRE ? BATCH # W0#:LQ91G1AC-LCS/LQ91G1AD-LCS D LC S Lot-Sample# : H9L17OO00-49 7 (9 0 - 110 ) AST M D482-00 a 12/17-12/22/0 9 935149 7 (9 0 - 110 ) 0.4 8 (0-10 ) AST M D482-0Da 12/17-12/22/ 0 9 935149 7 Dilutio nFactor : 1 Gros s Calorifi c Valu e 10 0

9 9 WO#:LQ2R71AA-_CS/LQ2R71AC-LCS D LC S Lot-Sample# : H9L140000-07 5

(9 8 - 102 ) (9 8 - 102 ) 0.0 8 (0-2.0 ) Dilutio nFactor : 1 AST M D240-0 2 AST M D240-0 2 12/14/0 9 12/14/0 9 934307 5

934807 5

NOTE(S ) : , Calculaiion s ar

e pcribrme d befor e roundin g l o avoi d round-of f errors in calculate d results .



### VES01873 58 7

LABORATOR

YCONTRO

L SAMPL E DAT

A REPOR T Genera l Chemistr y Lot-Sampl e #. .
PARAMETE

R As hConten t H9L09042 3

SPIK E MEASURE

D AMOUN T AMOUN

T UNIT S Matri x: HAST E

PERCN T RECVR YRPD METHO

D PREPARATION ANALYSI S DAT E 400 0 400 0 PREP BATCH ft WO#iLQ91GlAC-LCS/LQ91GlAD-LCS D LC S Lot-Satrtple# : H9L170000-49 7 3S7 0 mg/k

g 9 9 AST M D482-O0 a 12/17-12/22/0 9 935149 7 395 0 mg/k

g 9 9 0.4 8 AST M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 Gros s Calorifi c Valu e 2060 0

2060 0 WO#:LQ2R71AA-LCS/LQ2R71AC-LCS D LC S Lot-Sample# : H9L140000-07 5

2050 0 2050 0 BTU/l b10 0

BTU/l b9 9 Dilutio nFactor : 1 AST M D2 4 0-0 2 0.0 8 AST

M D240-0 2 12/14/0 9 12/14/0 9 934807 5

934807 5

NOTE(S) : Calculaiion s ar cperforme d before roundin g i o avoi d round-of f errors in calculated results .



### VES01873 6

### 8 8

LABORATOR

YCONTRO

L SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t H9L09042 3 Matri x: WAST E PERCEN T RECOVER

YPREPARATION - PRE

P PARAMETE

RRECOVER

YLIMIT S METHO D ANALYSI S DAT E BATC

H # Tota l Chlorin e Wor k Orde r # : LQTX01A C LC S Lot-Sample* : H9L100000-05 0 10 0 (8 0 - 120 ) KNO XWC-001 5 12/10-12/14/0 9 934406 0 Dilutio nFactor : 5 Tota l Chlorin e Wor k Orde r # : LQXER1A C LCS Lot-Sample* : H9L110000-06 4 9 9 (B

0 - 120 } KNO

XWC-001 5 12/11-12/16/0 9 934506 4 Dilutio nFactor : 5 MOT E tS ) ; ________________ _. . . . Calculation

s ar cpcrrormc

d befor e roundin

g t o avoi d round-of

f error s i n calculate

d results .



### VES01873 7

### 8 9

LABORATOR

YCONTRO

L SAMPL

E DAT A REPOR T Genera l Chemistr y Clien t Lo t H9L09D42 3 Matri x: WAST E SPIK E MEASURE

D PERCN T PREPARATION- PRE P PARAMETE

RAMODN

T AMOUN

T UNIT S RECVR YMETHO D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LQTX01A C LCS Lot-Sample# : H9L100000-06 0 1000 0 998 0 mg/k g 10 0 KNO

XWC-001 6 12/10-12/14/0 9 934405 0 Dilutio nFactor : S Tota l Chlorin e Wor k Orde r # : LQXER1A C LCS Lot-Sample# : H9L110000-06 4 1000 0 985 0 mg/k g 9 9 KNO

XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : S NOTE(S ) : _ Calculation

s ar e performe

d befor e roundin g t o avoi d round-of

f error s i n calculate

d results .



### VES01873 8

### 9 0

LABORATOR

YCONTRO

L SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Lot-Sampl e H9L09042 3 Matrxx .
PARAMETE

R As hConten t PERCEN T RECOVER Y 10 0 10 0 RECOVER

Y LIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E : SOLID PRE P BATC H # W0#:LQ1E11AC-LCS/LQ1E11AD-LCS D LCS Lot-Sample# : H9L110000-46 1 (9 0 - 110 ) AST M D4B2-00 a 12/11-12/15/0. 9 93454S 1 (9 0 - 110 } 0.4 2 (0-10 ) AST M D482-00 a 12/11-12/15/0 9 934545 1 Dilutio nFactor : 1 Gros s Calorifi c Valu e 10 0

10 0 W0#:LQ58P1AA-_CS/_Q58P1AC-_CS D LCS Lot-S_mple#. - H9L160000-03 2 (9 8 - 102 ) AST M D58S5-0 0 (•9 8 - 102 ) 0.1 0 (0-2.0 ) AST M D5865-0 0 Dilutio nFactor : 1 12/16/0 9 12/16/0 9 935003 2

935003 2
MOTE(S ) : Calculation

s ar cperforma

l befor e roundin g t o avoi d round-of

f error s i ncalculaie

d rcsulu.



### VES01873 99 1

LABOEATOR

r CONTRO

L SAMPL E DAT A REPOR T Genera l Oiernistr y Lot-Sampl e H9L09042 3 Matrix . SOLI D
PARAMETE

R As hConten t SPIK

E AMOUN T 400 0 400 0
Gros s Calorifi c Valu e 1140 0

1140 0 MEASURE

D AMOUN T UNITS PERCN

T RECVR YRP D METHO

D PREPARATIONANALYSI S DAT

E PRE P BATC H # WOft:LQlEllAC-LCS/LQlEllAD-LCS DLCS Lot-Sample# : H9L110000-46 1 401 0 mg/k

g 10 0 AST M D482-0O

a 12/11-12/15/0 9 934546 1 399 0 mg/k

g 10 0 0.4 2 AST M D482-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor : 1 W0#:LQ58P1AA-LCS/LQ5BP1AC-LCS D LC S Lot-Sample* : H9L160000-03 2 1130 0 BTU/l b10 0 1130 0 BTU/l b10 0

Dilutio nFactor : 1 AST M DS865-0 0 0.1 0 AST

M D586S-0 0 12/16/0 9

12/16/0 9 935003 2

935003 2
MOTE(S ) : Calculation

s at e performe

d befor e roundin

g t o avoi d round-of

f error s i ncalculate

d results .



### VES01874 0

### 9 2

MATRI XSPIK E SAMPL E EVALUATIO

N EEPOR T Genera l Chemistr y Clien t Lo t #...- . H9L09042 3 Dat e Sampled... : 12/01/0 9

PERCEN T RECOVER

Y PARAMETE

RRECOVER

YLIMIT S Tota l Chlorin e WO # 10 0 (8 0 9 7 (8 0 Dat e Received.. ; 12/04/0 9
RP D RP D LIMIT S METHO

D Matrox . WAST E
PREPARATIO

N - ANALYSI S DAT

E PRE P BATC H # LQQNNIAG-MS/LQQNN1AH-MS D M S Lot-Sampl e # : H9L090423-00 5 120 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 120 ) 3. 5 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 7.0 7 Tota l Chlorin e

10 1 (8 0 10 1 (8 0 WOt : LQQNT1AE-MS/LQQNTIAF-MS D M S Lot-Sampl e # : H9LD90423-00 7 120 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 120 ) 3. 2 (0-10 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 7. 1 HOTE(S ) •

• Calculation

s ar cpcrrormc

d befor e roundin g t o avoi d round-of

f error s i ncalculate

d results .



### VES01874 1

### 9 3

MATRI XSPIK E SAMPL E DAT A REPOR T Genera l C_temistx

y Clien t Lo t H9L09042 3 Dat e Sampled... ; 12/01/0 9 Matri x: WAST E Dat e Received.. : 12/04/0 9 SAMPL E SPIK E PARAMETE

RAMOUN

T AM T Tota l Chlorin e

82 5 82 5 MEASR D AMOUN T UNIT S PERCN T RECVR YRP D METHO

D PREPARATION - PRE P
1410 0 1400 0 ANALYSI S DAT E BATC H # WO# : LQQNN1AG-MS/LQQNN1AH-MS D M S Lot-Sampl e # : H9L090423-00 5 1500 0 mg/k

g 10 0 KNO XWC-001 6 12/10-12/14/0 9 934406 0 1450 0 mg/k

g 9 7 3. 5 KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 7.0 7 Tota l Chlorin e WO# : LQQNT1AE-MS/LQQNT1AF-MS D M S Lot-Sampl e #.

- H9L090423-00 7 498 0 1420 0 1930 0 mg/k g 10 1 KNO XWC-001 S 12/11-12/16/0 9 934506 4 498 0 1360 0 1870 0 mg/k g 10 1 3. 2 KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 7. 1 NOTE(S) : Calcubtian

s ar cperform

—befor e roundin g t o avoi d round-of

f error s i ncalculate

d results .



### VES018742

### 9 4

MATRI XSPIK E SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t #-.. : H9L09042 3 Matri x: SOLI D Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9

PERCEN T RECOVER

YRP

D PREPARATION- PRE P PARAMETE

RRECOVER

YLIMIT S RP

D LIMIT S METHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e WO# : LQQQR 1 A G- M S /LQQQR1A

H -MS D M S Lot-Sampl e # : H9L090423-01 1 9 0 (8 0 - 120 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 9 1 (8 0 - 120 ) 0.7 7 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 4.7 3 NOT E (S ) : Calculation

s ar e performe

d befor e roundin

g l o avoi d round-of

f error s i ncalculaie

d results .



### VES01874 3

### 9 5

MATRI XSPIK E SAMPL E DAT A EEPOR T Genera l Cfaemistr

y Clien t Lo t H9L09042 3 Dat e Sampled: 12/02/0 9

SAMPL E SPIK E MEASR

D Dat e Received.. : 12/04/0 9 Matrix . SOLI D

PARAMETE

RAMOUN

T AM T Tota l Chlorin e

10 5 947 0 10 5 945 0 AMOUN T UNIT S PERCN T RECVR YRP D METHO

D PREPARATION - PRE P ANALYSI S DAT

E BATC H # WO# : LQQQR1AG-MS/LQQQR1AK-MS D M S Lot-Sampl e # : H9L090423-01 1 8S4 0 mg/k

g 9 0 KNO XWC-001 6 12/10-12/14/0 9 934406 0 871 0 mg/k

g 9 1 0.7 7 KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 4.7 3 NOTE(S) : Calculation

s or e performe

d befor e roundin

g t o avoi d round-of

f error s i ncalculate

d results .



### VES01874 4

### 9 6

SAMPL E DUPLICATE ETOLDATIOI T EEPOR T Genera l Chemistry Clien t Lo t tt..-: H9L09042 3 Wor k Orde r #... : LQQNN-SM P Matri x: WAST E LQQNN-DU

P Dat e Sampled... : 12/02/0 9 Dat e Received.. : 12/04/0 9 DUPLICATE RP D PREPARATION - PRE P PARA M RESUL T RESUL

T UNIT S RP D LIMI T METHO

D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L090423-OO S Valu e N D N

D BTU/l b13 (0-10 ) AST M D240-0 2 12/14/0 9 934807 5 Dilutio nFactor : 1 As hConten t S D Lot-Sampl e # : H9L090423-00 5 117 0 121 0 mg/k g 3. 1 (0-10 ) AST M D482-00 a 12/17-12/22/0 9 935149 7 Dilutio nFactor : 1 Tota l Chlorin e S D Lot-Sampl e H9L090423-00 5 32 5 81 8 mg/k g 0.8 2 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1.3 9



### VES01874 5

### 9 7

Clien t Lo t #... : H9L09042 3 Dat e Sampled... : 12/01/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Cnemistr y Wor k Orde r LQQNT-SM P LQQNT-DU

P Dat e Received.. : 12/04/0 9
PARA M RESUL T Tota l Chlorin e 498 0 DUPLICATE

RESUL T 500 0 Matrix . WAST E

UNITS RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT

E BATC H ft S D Lot-Sampl e # : H9L090423-00 7 mg/k g 0.4 2 (0-10 ) KNO XWC-001 6 12/11-12/16/0 9 934506 4 Dilutio nFactor : 1.3 6



### VES01874 6

### 9 8

Clien t Lo t #. . Dat e Sampled. . PARA M RESUL T H9L09042 3 12/02/0 9 DUPLICATE RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQQQR-SM P Matrix . LQQQR-DU

P Dat e Received.. : 12/04/0 9 SOLID

Tota l Chlorin e 10 5 B
Gros s Calorifi c Valu e N D
As hConten t 80100 0 99. 6 B

N D

78400 0 RP D UNIT S RP

D LIMI T METHO

D PREPARATION - PRE P ANALYSI S DAT

E BATC H # S D Lot-Sampl e # : H9L090423-01 1 mg/k g 5. 3 (0-10 ) KNO XWC-001 6 12/10-12/14/0 9 934406 0 Dilutio nFactor : 1.0 2 S D Lot-Sampl e # : H9L090423-01 1 BTOyi b0 (0-10 ) AST M D5865-0 0 12/16/D 9 Dilutio nFactor : 1 935003 2
S D Lot-Sampl e # : H9L090423-01 1 mg/k g 2. 2 (0-10 ) AST M D4B2-00 a 12/11-12/15/0 9 934546 1 Dilutio nFactor : 1 NOTE(S ) : Calculation

s ar cperforme

d befor e roundin g t o avoi d round-of

T error s i ncalculate

d results . B Estimate

d result . Resul ti s les s tita n RL .



### VES01874 7

### 9 9

Clien t Lo t H9L09042 3 Dat e Sampled... : 12/03/0 9 SAMPL E DDPLICATE EVALDATIO H REPOR T Genera l Chemistr y Wor k Orde r #... : LQQRO-SM P LQQRO-DD

P Dat e Received.. : 12/04/0 9
PARA M RESDLT Gros s Calorifi c Valu e 1030 0 DDPLICAT E RESUL T UNITS RP D RP D LIMI T METHO

D Matri x: WAST E

PREPARATION

- PRE P ANALYSI S DAT

E BATC H ft S D Lot-Sampl e # : H9L090423-01 5 1010 0 BTU/l b1. 4 (0-10 ) AST M D240-0 2 12/14/0 9 Dilutio nFactor : 1 934807 5



### VES01874 8

### 101

Clien t Lo t # . Dat e Sampled PARA M RESUL T As hConten t 782 0 H9L09042 3

12/03/0 9 DUPLICATE RESUL T SAMPL

E DUPLICATE EVALTJATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LQQTD-SM P LQQTD-DU

P Dat e Received.. : 12/04/0 9
UNIT S RP

D RP D LIMI T METHO

D Matrix - WAST E

691 0 mg/k

g 1 2 Dilutio nFactor : 1 PREPARATION- PRE P ANALYSI S DAT

E BATC H # S D Lot-Sampl e # : H9L090423-02 1 (0-10 ) AST

M D482-O0 a 12/17-12/22/0 9 935149 7



### VES01874 9

### VES01875 0

# VES018751-019264.pd f