### Name: Thomas Reed

Title: Environmental Engineer Company: Manitowoc Public Utilities Sign Date: 8/11/2010 Name: Chet Gutwein Title: Engineer Company: Airtech Environmental Services Inc. Sign Date: 8/10/2010 Permitted Facility Representative / Date Testing Company Representative / Date 

## 3225 Manitowoc Public Utilities Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Sunday, January 30, 2011 Page 1 of 43

### 3225 Manitowoc Public Utilities

8/11/2010 Facility Information:

MPU Power Plant

1303 S 8TH ST

Manitowoc WI 54220
Contact: Thomas Reed

Phone: (920) 686-4384

Fax: (920) 686-4315

Email: tomreed@mpu.org Testing Company:

Airtech Environmental Services Inc. 601A Country Club Drive

Bensenville IL 60106
Contact: Brandon Check

Phone: (630) 860-4740

Fax: (630) 860-4745

Email: bcheck@airtechenv.com

Air Permit Number:
4125 Permitted Source ID/Name:
Boiler 9 B09

Permitted Maximum Process Rate:
N/A Max. Normal Operation Process Rate:
N/A Target Process Test Rate
N/A

Description of the source (including control equipment). Please see the attachments for source or process flow diagram:
Manitowoc Public Utilities Unit #9 is an atmospheric pressure circulating fluidized bed (CFB) boiler that fires coal, petroleum coke, paper pellets or a combination of any of the three fuels, along with natural gas as a start-up fuel. The boiler produces steam, which is used to turn a steam turbine/electric generator set and to provide steam for off-site utilization (cogeneration). The Manitowoc Public Utilities Power Plant is located at 701 Columbus Street in the City of Manitowoc, in Manitowoc County, Wisconsin. The Manitowoc Public Utilities business office is located on the same site with an address of 1303 South 8th Street. Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: 5507100008 FRS #: 110000421384

SCC / Description 10100202 External Combustion Boilers - Electric Generation - Bituminous/Subbituminous Coal - Pulverized Coal: Dry Bottom (Bituminous Coal)

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width
Stack Exit 108 2.8 2.8 2 108 24 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location

Carbon Monoxide Method 10 3 120 0 Stack Exit 2,3,7,8-TCDD Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDD Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDD Method 23 3 480 0 Stack Exit



### Sunday, January 30, 2011 Page 2 of 43

### 3225 Manitowoc Public Utilities

8/11/2010
1,2,3,7,8,9-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,4,6,7,8-HpCDD Method 23 3 480 0 Stack Exit OCDD Method 23 3 480 0 Stack Exit 2,3,7,8-TCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDF Method 23 3 480 0 Stack Exit 2,3,4,7,8-PeCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 2,3,4,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8,9-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,4,6,7,8-HpCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8,9-HpCDF Method 23 3 480 0 Stack Exit OCDF Method 23 3 480 0 Stack Exit Other TCDD Method 23 0 Stack Exit Other PeCDD Method 23 0 Stack Exit Other HxCDD Method 23 0 Stack Exit Other HpCDD Method 23 0 Stack Exit Other TCDF Method 23 0 Stack Exit Other PeCDF Method 23 0 Stack Exit Other HxCDF Method 23 0 Stack Exit Other HpCDF Method 23 0 Stack Exit Total Dioxins Method 23 3 480 0 Stack Exit Total Furans Method 23 3 480 0 Stack Exit 3,3',4,4'-TCB (PCB77) Method 23 3 480 0 Stack Exit 3,4,4',5-TCB (PCB81) Method 23 3 480 0 Stack Exit 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 0 Stack Exit 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 0 Stack Exit 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 0 Stack Exit 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 0 Stack Exit 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 0 Stack Exit 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 0 Stack Exit

2,3',4,4',5,5'-HxCB (PCB167) Method 23 3 480 0 Stack Exit 3,3',4,4',5,5'-HxCB (PCB169) Method 23 3 480 0 Stack Exit 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 0 Stack Exit

Total PCBs Method 23 3 480 0 Stack Exit Total TEQ Method 23 3 480 0 Stack Exit Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Stack Exit

Hydrogen Fluoride Method 26A 3 180 0 Measured using NaOH impingers Stack Exit

Hydrogen Chloride Method 26A 3 180 0 Measured using NaOH impingers Stack Exit

Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 240 0 Stack Exit

Filterable Particulate OTM - 27/28 3 240 0 Stack Exit Filterable PM2.5 OTM - 27/28 3 240 0 Stack Exit Organic Condensible

Particulate OTM - 27/28 3 240 0 Stack Exit

Total PM2.5 OTM - 27/28 3 240 0 Stack Exit Total Particulate OTM - 27/28 3 240 0 Stack Exit Nickel Method 29 3 240 0 Stack Exit



### Sunday, January 30, 2011 Page 3 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.
The following is a list of the test methods that are to be used for this test program and their respective promulgation dates:

Methods 1 through 29 – August 1997 Method 30B – January 2008 Method 316 - March 1997 Other Test Methods 27 and 28 – April 2009 SW-846 0010 – September 1986 SW-846 0030 – December 1996

Antimony Method 29 3 240 0 Stack Exit Arsenic Method 29 3 240 0 Stack Exit Beryllium Method 29 3 240 0 Stack Exit Cadmium Method 29 3 240 0 Stack Exit Chromium Method 29 3 240 0 Stack Exit Filterable Particulate Method 29 3 240 0 Stack Exit Manganese Method 29 3 240 0 Stack Exit Selenium Method 29 3 240 0 Stack Exit Cobalt Method 29 3 240 0 Stack Exit Lead Method 29 3 240 0 Stack Exit O2 Method 3A O2 3 480 0 Stack Exit Co2 Method 3A CO2 3 480 0 Stack Exit Sulfur Dioxide Method 6C 3 180 0 Stack Exit Nitrogen oxides (NOx) Method 7E 3 180 0 Stack Exit



### Sunday, January 30, 2011 Page 4 of 43

### 3225 Manitowoc Public Utilities

8/11/2010 Sampling / Stack Data Results Summary



### Location Stack Exit - Method 10 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 10 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 5 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 23 Average
Run Number 1 2 3

Test Date 5/18/2010 5/19/2010 5/20/2010

Run Start Time 9:00:00 AM 8:00:00 AM 7:51:00 AM

Run Finish Time 5:20:00 PM 4:11:00 PM 4:05:00 PM
Net Run Time, minutes 480 480 480 Dry Gas Meter Volume Sampled, dscf 325.588 334.028 327.676 329.097
Moisture Content of Stack Gas, % 6.13 6.60 6.64 6.457 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000
Carbon Dioxide, % 14.9 14.3 15.4 14.867 Oxygen, % 4.57 4.5 4.23 4.433 Average Stack Gas Temperature, °F 357.67 362.88 361.33 360.627 Dry Volumetric Flow Rate, dry scfm 126,527.3 128,796.8 128,174.0 127,832.700
Actual Wet Volumetric Flue Gas Flow Rate, acfm 211,997.3 218,638.9 217,264.8 215,967.000 Percent Isokinetic of Sampling Rate, % 100.0 100.8 99.4 100.067
F-Factor, dscfm/MMBtu @ %O2 9847 9794 9828 9,823.000

Fw 0 0 0 0.000

Fc 0 0 0 0.000



### Location Stack Exit - Method 25A Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 6 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 25A 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 26A Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Sunday, January 30, 2011 Page 7 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 29 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Stack Exit - Method 3A CO2 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 8 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A CO2 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 3A CO2 3 6 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 9 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A O2 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 3A O2 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 10 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A O2 3 6 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 6C Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 11 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 6C 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 7E Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Sunday, January 30, 2011 Page 12 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 7E 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - OTM - 27/28 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Sunday, January 30, 2011 Page 13 of 43

### 3225 Manitowoc Public Utilities

8/11/2010 Emissions Summary



### Location: Stack Exit - Method 10 Compound: Carbon Monoxide Average
Run 5-20B 5-20C 5-21A lb/mmBtuO2 4.23E-03 5.07E-03 5.15E-03 0.005
ppm 4.72E+00 5.66E+00 5.50E+00 5.293 ppm@7%O2 3.94E+00 4.72E+00 4.80E+00 4.487



### Location: Stack Exit - Method 10 3 Compound: Carbon Monoxide Average
Run 5-21B lb/mmBtuO2 5.37E-03 0.005
ppm 6.03E+00 6.030 ppm@7%O2 5.00E+00 5.000



### Location: Stack Exit - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber 1 2 3 Mass_mg 0.000000007 0.0000000056 0.0000000066 0.000 lb/mmBtuO2 5.97E-13 4.61E-13 5.47E-13 0.000 ng/dscm 7.59E-04 5.92E-04 7.11E-04 0.001 ng/dscm@7%O2 6.46E-04 5.02E-04 5.93E-04 0.001


### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber 1 2 3 Mass_mg 0.000000017 0.000000012 0.0000000087 0.000 lb/mmBtuO2 1.45E-12 9.89E-13 7.21E-13 0.000 ng/dscm 1.84E-03 1.27E-03 9.38E-04 0.001 ng/dscm@7%O2 1.57E-03 1.08E-03 7.82E-04 0.001


### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000037 0.0000000043 0.000000003 0.000 lb/mmBtuO2 3.16E-13 3.54E-13 2.49E-13 0.000 ng/dscm 4.01E-04 4.55E-04 3.23E-04 0.000 ng/dscm@7%O2 3.41E-04 3.86E-04 2.69E-04 0.000


### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000028 0.0000000021 0.0000000025 0.000 lb/mmBtuO2 2.39E-13 1.73E-13 2.07E-13 0.000 ng/dscm 3.04E-04 2.22E-04 2.69E-04 0.000 ng/dscm@7%O2 2.59E-04 1.88E-04 2.24E-04 0.000



### Sunday, January 30, 2011 Page 14 of 43

### 3225 Manitowoc Public Utilities

8/11/2010
Compound: 1,2,3,4,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.000000015 0.000000012 0.000000011 0.000 lb/mmBtuO2 1.28E-12 9.89E-13 9.12E-13 0.000 ng/dscm 1.63E-03 1.27E-03 1.19E-03 0.001 ng/dscm@7%O2 1.39E-03 1.08E-03 9.92E-04 0.001


### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000027 0.000000002 0.0000000025 0.000 lb/mmBtuO2 2.30E-13 1.65E-13 2.07E-13 0.000 ng/dscm 2.93E-04 2.11E-04 2.69E-04 0.000 ng/dscm@7%O2 2.49E-04 1.79E-04 2.24E-04 0.000


### Compound: 1,2,3,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000081 0.0000000063 0.0000000049 0.000 lb/mmBtuO2 6.91E-13 5.19E-13 4.06E-13 0.000 ng/dscm 8.79E-04 6.66E-04 5.28E-04 0.001 ng/dscm@7%O2 7.48E-04 5.64E-04 4.40E-04 0.001


### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000028 0.0000000021 0.0000000025 0.000 lb/mmBtuO2 2.39E-13 1.73E-13 2.07E-13 0.000 ng/dscm 3.04E-04 2.22E-04 2.69E-04 0.000 ng/dscm@7%O2 2.59E-04 1.88E-04 2.24E-04 0.000


### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000023 0.0000000017 0.000000002 0.000 lb/mmBtuO2 1.96E-13 1.40E-13 1.66E-13 0.000 ng/dscm 2.50E-04 1.80E-04 2.16E-04 0.000 ng/dscm@7%O2 2.13E-04 1.53E-04 1.80E-04 0.000


### Compound: 1,2,3,7,8-PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000031 0.0000000027 0.0000000031 0.000 lb/mmBtuO2 2.65E-13 2.22E-13 2.57E-13 0.000 ng/dscm 3.36E-04 2.85E-04 3.34E-04 0.000 ng/dscm@7%O2 2.86E-04 2.42E-04 2.79E-04 0.000


### Compound: 1,2,3,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.000000013 0.0000000042 0.0000000076 0.000 lb/mmBtuO2 1.11E-12 3.46E-13 6.30E-13 0.000



### Sunday, January 30, 2011 Page 15 of 43

### 3225 Manitowoc Public Utilities

8/11/2010 ng/dscm 1.41E-03 4.44E-04 8.19E-04 0.001 ng/dscm@7%O2 1.20E-03 3.76E-04 6.83E-04 0.001


### Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber 1 2 3 Mass_mg 0.0000000071 0.000000007 0.0000000066 0.000 lb/mmBtuO2 6.06E-13 5.77E-13 5.47E-13 0.000 ng/dscm 7.70E-04 7.40E-04 7.11E-04 0.001 ng/dscm@7%O2 6.55E-04 6.27E-04 5.93E-04 0.001


### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber 1 2 3 Mass_mg 0.000000072 0.0000000136 0.0000000116 0.000 lb/mmBtuO2 6.14E-12 1.12E-12 9.62E-13 0.000 ng/dscm 7.81E-03 1.44E-03 1.25E-03 0.004 ng/dscm@7%O2 6.65E-03 1.22E-03 1.04E-03 0.003


### Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber 1 2 3 Mass_mg 0.000000157 0.000000203 0.000000208 0.000 lb/mmBtuO2 1.34E-11 1.67E-11 1.72E-11 0.000 ng/dscm 1.70E-02 2.15E-02 2.24E-02 0.020 ng/dscm@7%O2 1.45E-02 1.82E-02 1.87E-02 0.017


### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber 1 2 3 Mass_mg 0.0000000167 0.0000000146 0.000000009 0.000 lb/mmBtuO2 1.43E-12 1.20E-12 7.46E-13 0.000 ng/dscm 1.81E-03 1.54E-03 9.70E-04 0.001 ng/dscm@7%O2 1.54E-03 1.31E-03 8.09E-04 0.001


### Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber 1 2 3 Mass_mg 0.0000000086 0.0000000089 0.0000000087 0.000 lb/mmBtuO2 7.34E-13 7.33E-13 7.21E-13 0.000 ng/dscm 9.33E-04 9.41E-04 9.38E-04 0.001 ng/dscm@7%O2 7.94E-04 7.98E-04 7.82E-04 0.001


### Compound: 2,3',4,4',5-PeCB (PCB118) Average RunNumber 1 2 3 Mass_mg 0.00000046 0.0000005 0.00000061 0.000 lb/mmBtuO2 3.93E-11 4.12E-11 5.06E-11 0.000 ng/dscm 4.99E-02 5.29E-02 6.58E-02 0.056 ng/dscm@7%O2 4.25E-02 4.48E-02 5.49E-02 0.047


### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber 1 2 3



### Sunday, January 30, 2011 Page 16 of 43

### 3225 Manitowoc Public Utilities

8/11/2010
Mass_mg 0.0000000122 0.000000108 0.0000000097 0.000 lb/mmBtuO2 1.04E-12 8.90E-12 8.04E-13 0.000 ng/dscm 1.32E-03 1.14E-02 1.05E-03 0.005 ng/dscm@7%O2 1.12E-03 9.66E-03 8.76E-04 0.004


### Compound: 2,3,4,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.000000004 0.0000000015 0.0000000028 0.000 lb/mmBtuO2 3.41E-13 1.24E-13 2.32E-13 0.000 ng/dscm 4.34E-04 1.59E-04 3.02E-04 0.000 ng/dscm@7%O2 3.69E-04 1.35E-04 2.52E-04 0.000


### Compound: 2,3,4,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.000000008 0.0000000064 0.0000000051 0.000 lb/mmBtuO2 6.83E-13 5.27E-13 4.23E-13 0.000 ng/dscm 8.68E-04 6.77E-04 5.50E-04 0.001 ng/dscm@7%O2 7.39E-04 5.74E-04 4.59E-04 0.001


### Compound: 2,3,7,8-TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000058 0.0000000052 0.0000000061 0.000 lb/mmBtuO2 4.95E-13 4.28E-13 5.06E-13 0.000 ng/dscm 6.29E-04 5.50E-04 6.58E-04 0.001 ng/dscm@7%O2 5.35E-04 4.66E-04 5.49E-04 0.001


### Compound: 2,3,7,8-TCDF Average RunNumber 1 2 3 Mass_mg 0.000000016 0.00000001 0.0000000096 0.000 lb/mmBtuO2 1.37E-12 8.24E-13 7.96E-13 0.000 ng/dscm 1.74E-03 1.06E-03 1.03E-03 0.001 ng/dscm@7%O2 1.48E-03 8.98E-04 8.59E-04 0.001


### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber 1 2 3 Mass_mg 0.0000000102 0.0000000108 0.0000000093 0.000 lb/mmBtuO2 8.70E-13 8.90E-13 7.71E-13 0.000 ng/dscm 1.11E-03 1.14E-03 1.00E-03 0.001 ng/dscm@7%O2 9.45E-04 9.66E-04 8.34E-04 0.001


### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber 1 2 3 Mass_mg 0.0000000097 0.0000000106 0.0000000097 0.000 lb/mmBtuO2 8.28E-13 8.73E-13 8.04E-13 0.000 ng/dscm 1.05E-03 1.12E-03 1.05E-03 0.001 ng/dscm@7%O2 8.94E-04 9.49E-04 8.76E-04 0.001



### Sunday, January 30, 2011 Page 17 of 43

### 3225 Manitowoc Public Utilities

8/11/2010
Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber 1 2 3 Mass_mg 0.0000000314 0.00000005 0.000000047 0.000 lb/mmBtuO2 2.68E-12 4.12E-12 3.90E-12 0.000 ng/dscm 3.41E-03 5.29E-03 5.07E-03 0.005 ng/dscm@7%O2 2.90E-03 4.48E-03 4.23E-03 0.004


### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber 1 2 3 Mass_mg 0.0000000143 0.0000000146 0.0000000132 0.000 lb/mmBtuO2 1.22E-12 1.20E-12 1.09E-12 0.000 ng/dscm 1.55E-03 1.54E-03 1.42E-03 0.002 ng/dscm@7%O2 1.32E-03 1.31E-03 1.18E-03 0.001


### Compound: OCDD Average RunNumber 1 2 3 Mass_mg 0.000000021 0.00000002 0.000000019 0.000 lb/mmBtuO2 1.79E-12 1.65E-12 1.58E-12 0.000 ng/dscm 2.28E-03 2.11E-03 2.05E-03 0.002 ng/dscm@7%O2 1.94E-03 1.79E-03 1.71E-03 0.002


### Compound: OCDF Average RunNumber 1 2 3 Mass_mg 0.0000000047 0.0000000086 0.0000000081 0.000 lb/mmBtuO2 4.01E-13 7.08E-13 6.72E-13 0.000 ng/dscm 5.10E-04 9.09E-04 8.73E-04 0.001 ng/dscm@7%O2 4.34E-04 7.70E-04 7.28E-04 0.001


### Compound: Other HpCDD Average RunNumber 1 2 3 Mass_mg 0.000000012 0.0000000044 0.0000000064 0.000 lb/mmBtuO2 1.02E-12 3.62E-13 5.31E-13 0.000 ng/dscm 1.30E-03 4.65E-04 6.90E-04 0.001 ng/dscm@7%O2 1.11E-03 3.94E-04 5.75E-04 0.001


### Compound: Other HpCDF Average RunNumber 1 2 3 Mass_mg 0 0.0000000037 0 0.000 lb/mmBtuO2 0.00E+00 3.05E-13 0.00E+00 0.000 ng/dscm 0.00E+00 3.91E-04 0.00E+00 0.000 ng/dscm@7%O2 0.00E+00 3.31E-04 0.00E+00 0.000


### Compound: Other HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000417 0.0000000218 0.0000000225 0.000 lb/mmBtuO2 3.56E-12 1.80E-12 1.87E-12 0.000



### Sunday, January 30, 2011 Page 18 of 43

### 3225 Manitowoc Public Utilities

8/11/2010 ng/dscm 4.52E-03 2.31E-03 2.43E-03 0.003 ng/dscm@7%O2 3.85E-03 1.96E-03 2.03E-03 0.003


### Compound: Other HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000356 0.0000000275 0.0000000223 0.000 lb/mmBtuO2 3.04E-12 2.27E-12 1.85E-12 0.000 ng/dscm 3.86E-03 2.91E-03 2.40E-03 0.003 ng/dscm@7%O2 3.29E-03 2.47E-03 2.00E-03 0.003


### Compound: Other PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000479 0.0000000233 0.0000000289 0.000 lb/mmBtuO2 4.09E-12 1.92E-12 2.40E-12 0.000 ng/dscm 5.20E-03 2.46E-03 3.12E-03 0.004 ng/dscm@7%O2 4.43E-03 2.09E-03 2.60E-03 0.003


### Compound: Other PeCDF Average RunNumber 1 2 3 Mass_mg 0.000000099 0.0000000544 0.0000000493 0.000 lb/mmBtuO2 8.45E-12 4.48E-12 4.09E-12 0.000 ng/dscm 1.07E-02 5.75E-03 5.31E-03 0.007 ng/dscm@7%O2 9.11E-03 4.87E-03 4.43E-03 0.006


### Compound: Other TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000472 0.0000000288 0.0000000209 0.000 lb/mmBtuO2 4.03E-12 2.37E-12 1.73E-12 0.000 ng/dscm 5.12E-03 3.05E-03 2.25E-03 0.003 ng/dscm@7%O2 4.36E-03 2.59E-03 1.88E-03 0.003


### Compound: Other TCDF Average RunNumber 1 2 3 Mass_mg 0.000000124 0.00000011 0.0000000614 0.000 lb/mmBtuO2 1.06E-11 9.06E-12 5.09E-12 0.000 ng/dscm 1.35E-02 1.16E-02 6.62E-03 0.011 ng/dscm@7%O2 1.15E-02 9.83E-03 5.52E-03 0.009


### Compound: Total Dioxins Average RunNumber 1 2 3 Mass_mg 0.000000173 0.000000098 0.000000102 0.000 lb/mmBtuO2 1.48E-11 8.07E-12 8.46E-12 0.000 ng/dscm 1.88E-02 1.04E-02 1.10E-02 0.013 ng/dscm@7%O2 1.60E-02 8.81E-03 9.17E-03 0.011


### Compound: Total Furans Average RunNumber 1 2 3



### Sunday, January 30, 2011 Page 19 of 43

### 3225 Manitowoc Public Utilities

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Mass_mg 0.000000342 0.000000254 0.000000185 0.000 lb/mmBtuO2 2.92E-11 2.09E-11 1.53E-11 0.000 ng/dscm 3.71E-02 2.69E-02 1.99E-02 0.028 ng/dscm@7%O2 3.16E-02 2.28E-02 1.66E-02 0.024


### Compound: Total PCBs Average RunNumber 1 2 3 Mass_mg 0.000000733 0.000000632 0.000000973 0.000 lb/mmBtuO2 6.26E-11 5.21E-11 8.07E-11 0.000 ng/dscm 7.95E-02 6.68E-02 1.05E-01 0.084 ng/dscm@7%O2 6.77E-02 5.66E-02 8.76E-02 0.071


### Compound: Total TEQ Average RunNumber 1 2 3 Mass_mg 0.00000000922 0.00000000649 0.00000000594 0.000 lb/mmBtuO2 7.87E-13 5.35E-13 4.92E-13 0.000 ng/dscm 1.00E-03 6.86E-04 6.40E-04 0.001 ng/dscm@7%O2 8.51E-04 5.81E-04 5.34E-04 0.001



### Location: Stack Exit - Method 25A Compound: Total organic compounds (TOC) as Average
Run 5-20B 5-20C 5-21A lb/mmBtuO2 1.04E-04 1.50E-04 4.50E-04 0.000
ppm 7.23E-02 1.07E-01 3.05E-01 0.161 ppm@7%O2 6.13E-02 8.92E-02 2.66E-01 0.139



### Location: Stack Exit - Method 25A 3 Compound: Total organic compounds (TOC) as Average
Run 5-21B lb/mmBtuO2 2.90E-04 0.000
ppm 2.07E-01 0.207 ppm@7%O2 1.72E-01 0.172



### Location: Stack Exit - Method 26A Compound: Hydrogen Chloride Average RunNumber 1 2 3 Mass_mg 5.87 16.3 23 15.057 Elb/hr 9.42E-01 2.56E+00 3.66E+00 2.387 lb/mmBtuO2 1.63E-03 4.47E-03 6.18E-03 0.004 mg/dscm 2.11E+00 5.83E+00 8.16E+00 5.367 mg/dscm@7%O2 1.78E+00 4.85E+00 6.70E+00 4.443


### Compound: Hydrogen Fluoride Average RunNumber 1 2 3 Mass_mg 0.464 0.637 0.594 0.565 Elb/hr 7.45E-02 1.00E-01 9.45E-02 0.090



### Sunday, January 30, 2011 Page 20 of 43

### 3225 Manitowoc Public Utilities

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lb/mmBtuO2 1.29E-04 1.75E-04 1.60E-04 0.000 mg/dscm 1.67E-01 2.28E-01 2.11E-01 0.202 mg/dscm@7%O2 1.41E-01 1.90E-01 1.73E-01 0.168



### Location: Stack Exit - Method 29 

### Compound: Antimony Average RunNumber 1 2 3 Mass_mg 0.000786 0.001206 0.002496 0.001 Elb/hr 9.72E-05 1.46E-04 3.07E-04 0.000 lb/mmBtuO2 1.68E-07 2.55E-07 5.26E-07 0.000 mg/dscm 2.12E-04 3.25E-04 6.82E-04 0.000 mg/dscm@7%O2 1.82E-04 2.77E-04 5.70E-04 0.000


### Compound: Arsenic Average RunNumber 1 2 3 Mass_mg 0.015825 0.014825 0.015526 0.015 Elb/hr 1.96E-03 1.80E-03 1.91E-03 0.002 lb/mmBtuO2 3.38E-06 3.14E-06 3.27E-06 0.000 mg/dscm 4.27E-03 4.00E-03 4.24E-03 0.004 mg/dscm@7%O2 3.66E-03 3.42E-03 3.55E-03 0.004


### Compound: Beryllium Average RunNumber 1 2 3 Mass_mg 0.000261 0.000212 0.000259 0.000 Elb/hr 3.23E-05 2.57E-05 3.19E-05 0.000 lb/mmBtuO2 5.57E-08 4.49E-08 5.46E-08 0.000 mg/dscm 7.04E-05 5.72E-05 7.08E-05 0.000 mg/dscm@7%O2 6.03E-05 4.88E-05 5.92E-05 0.000


### Compound: Cadmium Average RunNumber 1 2 3 Mass_mg 0.000681 0.000647 0.00083 0.001 Elb/hr 8.42E-05 7.84E-05 1.02E-04 0.000 lb/mmBtuO2 1.45E-07 1.37E-07 1.75E-07 0.000 mg/dscm 1.84E-04 1.74E-04 2.27E-04 0.000 mg/dscm@7%O2 1.58E-04 1.49E-04 1.90E-04 0.000


### Compound: Chromium Average RunNumber 1 2 3 Mass_mg 0.00337 0.00366 0.00292 0.003 Elb/hr 4.17E-04 4.44E-04 3.60E-04 0.000 lb/mmBtuO2 7.20E-07 7.75E-07 6.16E-07 0.000 mg/dscm 9.09E-04 9.87E-04 7.98E-04 0.001 mg/dscm@7%O2 7.79E-04 8.43E-04 6.67E-04 0.001


### Compound: Cobalt Average RunNumber 1 2 3



### Sunday, January 30, 2011 Page 21 of 43

### 3225 Manitowoc Public Utilities

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Mass_mg 0.001253 0.001523 0.002083 0.002 Elb/hr 1.55E-04 1.85E-04 2.57E-04 0.000 lb/mmBtuO2 2.68E-07 3.22E-07 4.39E-07 0.000 mg/dscm 3.38E-04 4.11E-04 5.69E-04 0.000 mg/dscm@7%O2 2.90E-04 3.51E-04 4.76E-04 0.000


### Compound: Filterable Particulate Average RunNumber 1 2 3 Mass_mg 0.76 0.375 1.01 0.715 Elb/hr 9.40E-02 4.55E-02 1.24E-01 0.088 lb/mmBtuO2 1.62E-04 7.94E-05 2.13E-04 0.000 mg/dscm 2.05E-01 1.01E-01 2.76E-01 0.194 mg/dscm@7%O2 1.76E-01 8.62E-02 2.31E-01 0.164


### Compound: Lead Average RunNumber 1 2 3 Mass_mg 0.00297 0.00289 0.00347 0.003 Elb/hr 3.67E-04 3.50E-04 4.27E-04 0.000 lb/mmBtuO2 6.34E-07 6.12E-07 7.32E-07 0.000 mg/dscm 8.01E-04 7.79E-04 9.48E-04 0.001 mg/dscm@7%O2 6.86E-04 6.65E-04 7.93E-04 0.001


### Compound: Manganese Average RunNumber 1 2 3 Mass_mg 0.00988 0.00928 0.00542 0.008 Elb/hr 1.22E-03 1.12E-03 6.67E-04 0.001 lb/mmBtuO2 2.11E-06 1.96E-06 1.14E-06 0.000 mg/dscm 2.66E-03 2.50E-03 1.48E-03 0.002 mg/dscm@7%O2 2.28E-03 2.13E-03 1.24E-03 0.002


### Compound: Nickel Average RunNumber 1 2 3 Mass_mg 0.01524 0.01234 0.01394 0.014 Elb/hr 1.88E-03 1.50E-03 1.72E-03 0.002 lb/mmBtuO2 3.25E-06 2.61E-06 2.94E-06 0.000 mg/dscm 4.11E-03 3.33E-03 3.81E-03 0.004 mg/dscm@7%O2 3.52E-03 2.84E-03 3.19E-03 0.003


### Compound: Selenium Average RunNumber 1 2 3 Mass_mg 0.103803 0.118803 0.114803 0.112 Elb/hr 1.28E-02 1.44E-02 1.41E-02 0.014 lb/mmBtuO2 2.22E-05 2.51E-05 2.42E-05 0.000 mg/dscm 2.80E-02 3.20E-02 3.14E-02 0.030 mg/dscm@7%O2 2.40E-02 2.73E-02 2.63E-02 0.026



### Location: Stack Exit - Method 6C



### Sunday, January 30, 2011 Page 22 of 43

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Compound: Sulfur Dioxide Average
Run 5-19B 5-20A 5-20B Elb/hr 1.79E+02 1.72E+02 1.68E+02 173.000 lb/mmBtuO2 2.88E-01 2.76E-01 2.69E-01 0.278 mg/dscm 3.70E+02 3.59E+02 3.50E+02 359.667 mg/dscm@7%O2 3.14E+02 2.99E+02 2.92E+02 301.667
ppm 1.39E+02 1.35E+02 1.32E+02 135.333 ppm@7%O2 1.18E+02 1.13E+02 1.10E+02 113.667



### Location: Stack Exit - Method 6C 3 Compound: Sulfur Dioxide Average
Run 5-20C 5-21A 5-21B Elb/hr 1.69E+02 1.51E+02 1.71E+02 163.667 lb/mmBtuO2 2.70E-01 2.57E-01 2.74E-01 0.267 mg/dscm 3.51E+02 3.19E+02 3.59E+02 343.000 mg/dscm@7%O2 2.93E+02 2.79E+02 2.98E+02 290.000
ppm 1.32E+02 1.20E+02 1.35E+02 129.000 ppm@7%O2 1.10E+02 1.05E+02 1.12E+02 109.000



### Location: Stack Exit - Method 7E 

### Compound: Nitrogen oxides (NOx) Average
Run 5-19B 5-20A 5-20B Elb/hr 6.26E+01 3.75E+01 3.85E+01 46.200 lb/mmBtuO2 1.01E-01 6.02E-02 6.17E-02 0.074 mg/dscm 1.30E+02 7.82E+01 8.02E+01 96.133 mg/dscm@7%O2 1.10E+02 6.52E+01 6.69E+01 80.700
ppm 6.79E+01 4.09E+01 4.19E+01 50.233 ppm@7%O2 5.75E+01 3.41E+01 3.49E+01 42.167



### Location: Stack Exit - Method 7E 3 Compound: Nitrogen oxides (NOx) Average
Run 5-20C 5-21A 5-21B Elb/hr 3.54E+01 3.03E+01 3.36E+01 33.100 lb/mmBtuO2 5.67E-02 5.16E-02 5.40E-02 0.054 mg/dscm 7.37E+01 6.41E+01 7.06E+01 69.467 mg/dscm@7%O2 6.15E+01 5.60E+01 5.86E+01 58.700
ppm 3.85E+01 3.35E+01 3.69E+01 36.300 ppm@7%O2 3.21E+01 2.92E+01 3.06E+01 30.633



### Location: Stack Exit - OTM - 27/28 Compound: Filterable Particulate Average RunNumber 1 2 3 Mass_mg 0.3 0 0.1 0.133 lb/mmBtuO2 6.90E-05 0.00E+00 2.20E-05 0.000



### Sunday, January 30, 2011 Page 23 of 43

### 3225 Manitowoc Public Utilities

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Process Run Data Compound: Filterable PM2.5 Average RunNumber 1 2 3 Mass_mg 0.1 0 0 0.033 lb/mmBtuO2 2.30E-05 0.00E+00 0.00E+00 0.000


### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber 1 2 3 Mass_mg 6 23.8 10.1 13.300 lb/mmBtuO2 1.38E-03 5.29E-03 2.23E-03 0.003


### Compound: Organic Condensible Particulate Average RunNumber 1 2 3 Mass_mg 2.4 2.9 2.1 2.467 lb/mmBtuO2 5.52E-04 6.45E-04 4.63E-04 0.001


### Compound: Total Particulate Average RunNumber 1 2 3 Mass_mg 8.7 26.7 12.4 15.933 lb/mmBtuO2 2.00E-03 5.93E-03 2.73E-03 0.004


### Compound: Total PM2.5 Average RunNumber 1 2 3 Mass_mg 8.5 26.7 12.3 15.833 lb/mmBtuO2 1.96E-03 5.93E-03 2.71E-03 0.004



### Sunday, January 30, 2011 Page 24 of 43

### 3225 Manitowoc Public Utilities

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Process Run Data

APCD Run Data

Process Lab Run Data 

### Run Name Value UOM Comments Target Value
1 Coal Firing Rate 0 1000 tons/hr 0.0202



### 2 Coal Firing Rate 0 1000 tons/hr 0.0202

3 Coal Firing Rate 0 1000 tons/hr 0.0202

1 Average Heat Input 0 MMBtu/hr 0



### 2 Average Heat Input 0 MMBtu/hr 0

3 Average Heat Input 0 MMBtu/hr 0

1 Steam Output 0 1000 lb steam/hr 400



### 2 Steam Output 0 1000 lb steam/hr 400

3 Steam Output 0 1000 lb steam/hr 400

1 Flue Gas Flow Rate 0 dscfm 0



### 1 Pressure Drop Across FGD (if applicable) 0 in H20 0

1 FGD Scrubber Liquor pH 0 pH 0

1 FGD Scrubber Liquor Flow Rate 0 gal/min 0



### 1 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 11

1 Flue Gas Oxygen Content 0 % 3.5



### 1 Flue Gas Carbon Dioxide Content 0 % 0

1 Flue Gas Moisture Content 0 % 0

1 Flue Gas Sampling Point Temperature 0 Deg F 300



### 1 Unit Gross Electrical Output 0 MW 50

1 Unit Net Electric Generation 0 MWh 45



### Sunday, January 30, 2011 Page 25 of 43

### 3225 Manitowoc Public Utilities

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Sampling / Stack Data Results Detail



### Location Stack Exit - Method 10 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 26 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 10 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 27 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 23 Average Run Number 1 2 3
Test Date 5/18/2010 5/19/2010 5/20/2010 Run Start Time 9:00:00 AM 8:00:00 AM 7:51:00 AM Run Finish Time 5:20:00 PM 4:11:00 PM 4:05:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 480 480 480 Nozzle Diameter, inches 0.25 0.25 0.25 0.250 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.9928 0.9928 0.9928 0.993 Barometric Pressure, inches of Mercury 29.45 29.4 29.4 29.417 Average Orifice Meter Differential, inches H2O 1.70 1.77 1.76 1.743 Dry Gas Meter Volume Sampled, cubic feet 344.920 350.480 346.490 347.297 Average Dry Gas Meter Temperature, °F 88.92 82.85 87.06 86.277 Dry Gas Meter Volume Sampled, dscf 325.588 334.028 327.676 329.097 Total Moisture Liquid collected, g 451.8 501.9 495.5 483.067 Volume of Water Vapor, standard cubic feet 21.27 23.62 23.32 22.737 Moisture Content of Stack Gas, % 6.13 6.60 6.64 6.457 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9387 0.934 0.9336 0.935 Carbon Dioxide, % 14.9 14.3 15.4 14.867 Oxygen, % 4.57 4.5 4.23 4.433 Carbon Monoxide & Nitrogen, % 80.53 81.2 80.37 80.700 Fuel Factor 1.10 1.15 1.08 Dry Molecular Weight, lb/lb-Mole 30.57 30.47 30.63 30.557 Wet Molecular weight, lb/lb-Mole 29.80 29.65 29.79 29.747 Flue Gas Static Pressure, inches of H2O 0.2 0.2 0.2 0.200 Absolute Flue Gas Pressure, inches of Mercury 29.46 29.41 29.41 29.427 Average Stack Gas Temperature, °F 357.67 362.88 361.33 360.627 Average Velocity Head, inches of H2O 0.6421974765 9002 0.674205109

797874 0.670154945

801014 0.662

Average Stack Gas Velocity, feet/second 55.54 57.28 56.92 56.580 Stack Cross-Sectional Area, square feet 63.617 63.617 63.617 63.617 Dry Volumetric Flow Rate, dry scfm 126,527.3 128,796.8 128,174.0 127,832.700 Actual Wet Volumetric Flue Gas Flow Rate, acfm 211,997.3 218,638.9 217,264.8 215,967.000 Percent Isokinetic of Sampling Rate, % 100.0 100.8 99.4 100.067 Percent Excess Air, % 27.4 26.6 24.9 26.300 F-Factor, dscfm/MMBtu @ %O2 9847 9794 9828 9,823.000 Round Duct Diameter, inches 108 108 108 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0
Fw 0 0 0 0.000
Fc 0 0 0 0.000



### Sunday, January 30, 2011 Page 28 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 25A Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 29 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 25A 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 30 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 26A Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Sunday, January 30, 2011 Page 31 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 29 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Sunday, January 30, 2011 Page 32 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A CO2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 33 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A CO2 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 34 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A CO2 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 35 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A O2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 36 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A O2 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 37 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 3A O2 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 38 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 6C Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 39 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 6C 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 40 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 7E Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 41 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - Method 7E 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Sunday, January 30, 2011 Page 42 of 43

### 3225 Manitowoc Public Utilities

8/11/2010

Location Stack Exit - OTM - 27/28 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Sunday, January 30, 2011 Page 43 of 43