### Jul y30 , 200 8

Charli e i AI R fcNFORCEMENTBRANCH iU.S . EPA . REGIO N 5 

## JU L3 0 200

8

Attache d i s th e June , 200 6 Tes tRepor tfo rUni t3
. Thi s repor tcontain s informatio n o n th e arseni cissu e fro m May , 200 6 an d th e subsequen ttestin g result s fro m June , 200 6 tha t demonstrat e complianc e wit h th e LV M standards
. I n addition , informatio n tha t wa s sen tt o Sara h Marshal l regardin g th e arseni cissu e i s als o included
. Pleas e cal l i fyo u hav e an yquestions
.TECHNICA LSOLUTION S NORT H AMERIC A 

### ENVIRONMENTA L SERVICE S 

## JU L8 0 200 8

Octobe r30 , 200 6 Ms
. Sara h Marshal l Ai ran d Radiatio n Divisio n Unite d State s Environmenta l Protectio n Agenc y Regio n 5 7 7 Wes tJackso n Blv d Chicago , I I 60604-359 0 R E : Veoli a E S Technica l Solutions , L.L.C
. Notic e o fViolatio n an d Findin g o fViolatio n EPA-5-06-28-I L Dea rMs
. Marshall : Pursuan tt o you rreques tdurin g ou rmeetin g o n Octobe r23 , 2006 , Veoli a E S Technica l Solutions , L.L.C
. i s submittin g th e following :

•Tes trepor t fo rth e "Evaluatio n o fMetals , Particulat e Matte ran d PCDD/PCD F Emission s fo rFixe d Heart h Incinerato rUni t3 , Jun e 2006. " •Historica l Arseni cEmission s fo rIncinerator s 2 , 3 an d 4 fro m 200 1 throug h 2006
. •Arseni cconcentration s fro m por t an d stac k samples , May , 200 6 an d June , 2006
. Veoli a i s finalizin g th e emission s calculation s fro m Materia l Processin g Area s 1 an d 2 an d wil l b e submittin g tha t informatio n t o yo u b yNovembe r13 , a s requested
. Pleas e cal l m e o rDenni s Warchol , a t(618 ) 271-2804 , i fyo u hav e an yquestion s o rnee d an yadditiona l information
.

Dou g Harri s Genera l Manage r

Veoli a E S Technica l Services , Inc
. #7 Mobil e Ave , Sauget , I L6220 1 tel : 61 8 271280 4 - fax : 6i 3 2712128 www.VeoliaES.co m

### Att
.

cc : Grei g Siedo r Jo e Kellmeyer , Thompson-Cobum , LL P USEP AFil e

## Historical Arseni cEmissions fo rVeoli aE S - Sauge t

Tes tDat e Uni t Ru n 1 Ru n 2 Ru n 3 Averag e (ug/dscm ) (ug/dscm ) (ug/dscm ) (ug/dscm ) Apr-0 1 4 14.1 6 14.1 6 24.1 6 17.4 9 Apr-0 1 2 2.8 1 4.2 1 3.0 4 3.3 5 May-0 2 4 1.8 9 3.4 5 2.6 7 May-0 2 4 3.6 7 3.6 5 3.6 6 May-0 2 3 1.1 3 0.3 8 0.7 6 Aug-0 2 4 48.1 5 37.6 8 52.1 3 45.9 9 Aug-0 2 3 3.2 2 1.72 2.4 7 Aug-0 2 3 1.62 1.8 3 1.72 Nov-0 2 3 1.32 2.5 4 1.9 3 Nov-0 2 2 16.0 2 6.7 1 11.3 7 Nov-0 2 4 1.7 1 1.3 3 1.2 9 1.44 Sep-0 3 4 12. 4 11. 1 63. 9 29. 1 Sep-0 3 2 1. 4 1. 5 0.6 3 1. 2 May-0 6 3 6.1 4 12 6 55 7 23 0 Jun-0 6 3 3. 4 1. 9 2.9 8 2. 8 

## The above table show s th e historical arsenic emissio nresults fo r Veoli aincinerators during.testing conducte

di n2001 , 2002 , 2003 , an d2006
. The tota

l LV M emission s fo r al lofth e above test

s wer e belo w 9 7 ug/dscmwiththe exceptiono f th e Ma y 200 6 test performe do nUni t

3
. N o scrutin

y wa s givent o an y o f th e results fo r

arsenic i nth

e pre200 6 tests sinc e th

e tota l LV M emission s wer

e belo w th

e InterimMAC TStandar d emissio nlimi t

o f 97 ug/dscm
. Althoug hth e magnitud

e i s not a s great , th e result s fo r

Uni t 4 testing i nAugus t

2002 an dfo r on e runi nSeptembe

r 200 3 ma y hav e bee nfalsel y elevateddu

e t o simila r contaminationfro mrust/scale fro mth e sampling ports a

s was determinedfo r

th e Uni t 3 May 200 6 testing
.

## Laborator y Analyses fo rRust/Scale Sample s from Uni t3 Stac

k

Durin g the investigatio nto determin e the caus e ofth e elevate darseni c result s observe ddurin g the emission s testin g i nMa y 200 6 o nUni t 3 , analyse s wer e performe do nrust/scal e sample s obtaine dfro mth e Uni t 3 stack
. Fou r

sample s were take no nMa y 3 0 an dtw o more sample s were take no nJun e 8
. Belo w ar e th e analytica l result s obtained : Ma y 30

—27 9 pp m(sampl e take ninsid e stack aroun dsampl e port) Ma y 3 0 —437 5 pp m(sampl e take ninsid e stack aroun dsampl e port) Ma y 3 0 —183 0 pp m(sampl e take ninsid e stack aroun dsampl e port) Ma y 3 0 —46 3 pp m(sampl e take ninsid e stack aroun dsampl e port) Jun e 8 —267 6 pp m(sampl e take nfro minsid e flang e i nstack) Jun e 8 —8 2 pp m(sampl e scrape dof f o f removabl e blank

flange ) Kevi nMattiso nan dMichae l Ree do f the Illinoi s Environmenta l Protectio n Agenc y wer e on-site durin g the Jun e 8 sampling
.

# Evaluatio n ofMetals , Particulat e Matte r an d PCDD/PCD F Emission s fo rFixe d Heart h Incinerato rUni t3 Jun e 200 6

ENS R Corporatio n Septembe r200 6 Documen tNo. : 10002-01 7 

# ENS R AECO M

### Prepare d for :

Veoli a E S Technica l Solution s Sauget , Illinoi s



# Evaluatio n o fMetals , Particulat e Matte r an d PCDD/PCD F Emission s fo rFixe d Heart h Incinerato rUni t3 Jun e 200 6

Prepare d By : Jeffre yT
. Gorman , Projec tManage r

Reviewe d By : Crai g R
. Doolittle , rE , Manager , Ai rMeasurement s

ENS R Corporatio n Septembe r200 6 Documen t No. : 10002-01 7 

# ENS R AECO M

# ENS R

Content s ) 

### 1. 0 Introductio n 1- 1

1. 1 Progra m Summary1- 1 2. 0 Incinerato rProces s Descriptio n 2- 1 2. 1 Proces s Overview.
. 2- 1 2. 2 Wast e Fee d System s [4 0 CF R §63.1207(f)(1)(iii)(D)(E ) an d (f)(1)(ii)(C) ] 2- 1 2. 3 Manufacturer , Mak e an d Mode l ofth e Incinerato r[40 CF R §63.1207(f)(1)(iii)(A) ] 2- 1 2. 4 Ai rPollutio n Contro l Equipmen t[4 0 CF R §63.1207(f)(1)(iii)(G) ] 2- 2 2.4. 1 Lim e Syste m 2- 2 2.4. 2 Spra yDr

yAbsorbe r2- 3 2.4. 3 Fabri cFilte r2- 3 2.4. 4 Induce d Draft Fa n an d Stac k 2- 3 3 . 0 Summar

yo fResult s 3- 1 3. 1 Introductio n 3- 1 3. 2 Stac k

Emissio n Result s fo rPCDDs/PCDF s 3- 1 3. 3 Stac k

Emissio n Result s fo rTarge tMetal s an d Particulat e Matte r3- 1 \ 3. 4 Metal s Sampi e Contaminatio n 3- 2 4. 0 Samplin g an d Analytica l Procedure s 4- 1 4. 1 Samplin g Procedure s 4- 1 4.1. 1 Velocity , Moistur e an d Fixe d Ga s Determination s 4- 1 4.1. 2 PCDD/PCD F Samplin g 4- 1 4.1. 3 Metal s an d Particulat e Samplin g 4- 1 4. 2 Analytica l Procedure s 4- 1 4.2. 1 PCDD/PCD F Analyse s 4- 1 4.2. 2 Metal s Analyse s 4- 2 4. 3 Proces s Operatin g Condition s 4- 2 5. 0 Qualit

yAssuranc e 5- 1 5. 1 Introductio n 5- 1 5.1. 1 Pre-Samplin g Activitie s 5- 1 5.1. 2 Equipmen tCalibratio n 5- 1 5.1. 3 Glasswar e Preparatio n 5- 2

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# ENS R

List ofAppendice s Appendi xAFacilit yOperatin g Dat a Appendi xB Referenc e Metho d Fiel d Dat a an d Calculation s Appendi xC Referenc e Metho d Calibrations , Verifications , an d Certification s Appendi xD Stac k

Configuration , Samplin g Por tan d Travers e Poin tLocation s Appendi xE Laborator

yDat a 

# List o fTable s Tabl e 3- 1 PCD D /

PCD F Emissio n Result s - TE Q Basi s 3- 3 Tabl e 3- 2 Emissio n Result s fo rLV M Metal s - Ma y2006.
. Tabl e 3- 3 Emissio n Result s fo rLV M Metal s - Jun e 200 6 Tabl e 3- 4 Emissio n Result s fo rSV M Metal s an d Mercur y Tabl e 3- 5 Summaryo

fTarge t Metal s 3- 4 3- 5 3- 6 3- 7 Tabl e 3- 6 Emissio n Result s fo rParticulat e Matte r- Ma y2006.
. Tabl e 3- 7 Emissio n Result s fo rParticulat e Matte r- Jun e 200 6 3- 9 3- 8

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### i i Septembe r200 6

# ENS R

1. 0 Introductio n
1. 1 Progra m Summar y ENS R wa s retaine d byVeoli a E S Technica l Solution s (Veolia) , formerl yOny xEnvironmenta l Service s t o conduc tstac k ga s emissio n samplin g durin g th e week s o fMa y8 , 200 6 an d Jun e 19 , 2006
. Th e samplin g wa s performe d o n th e Fixe d Heart h Hazardou s Wast e Incinerato rUni t3 atthei r facilityi n Sauget , Illinois
. Th e purpos e o fthi s Performanc e Tes twa s t o evaluat e th e performanc e o f th e incinerato rrelativ e t o th e emission s standard s fo rexistin g incinerators foun d i n 4 0 CF R Par t63 , SubpartEE E (th e HW C MAC Tregulations)
. T o thi s end , th e specifi cobjective s ofthi s Performanc e Tes twer e t o demonstrat e emission s o fth e followin g pollutants :

•Mercury •Lo wVolatil e Metal s (arsenic , beryllium , an d chromium )
•Semi-volatil e Metal s (lea d an d cadmium )
•Dioxin s an d Furan s •Particulat e Matte r Th e Performanc e Tes tinclude d feedin g certai n type s ofwaste s an d material s int o th e incinerator , samplin g an d analyzin g thes e feedstreams , monitorin g certai n proces s parameter s whil e concurrentl yconductin g emission s testing
. Th e result s fro m thi s testin g indicat e that emission s fo rth e abov e pollutant s metth e emissio n standard s fo rth e HW C MAC Tregulations
. Asummaryofth e tes tresult s ca n b e foun d i n Sectio n 3 o fthi s report
.

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### 1- 1 Septembe r200 6

# ENS R

2. 0 Incinerato rProces s Descriptio n
2. 1 Proces s Overvie w Veoli a operate s 2 Fixe d Heart h Dua l Chambere d Incinerators (Unit s 2 an d 3 ) an d on e rotar ykil n (Uni t 4 ) at th e Sauget , I L facility
. Th e tw o fixe d heart h unit s ar e rate d at 1 6 millio n Btu/h reach
. Incineratio n Uni t No
. 3 i s a mirro rimag e o fUni t No
. 2
. Bot h ofthes e unit s have thei row n wast e handlin g system s a s describe d i n th e section s that follow
. Th e onl ydifferenc e bein g Uni t No
. 2 i s equippe d wit h fou r(4) baghous e modules , whil e Uni tNo
. 3 i s equippe d wit h thre e (3) baghous e modules
. Uni t 4 i s rate d at5 0 millio n Btu/h ran d i s equippe d wit h it s ow n tan k far m system , dru m storage , bul k

solid s storag e an d fee d systems
. 2. 2 Wast e Fee d System s [4 0 CF R §63.1207(f)( 1 )(iii)(D)(E ) an d (f)( 1 )(ii)(C) ] Fixe d heart h incinerato rno . 3 i s designe d t o receiv e containers , aqueou s liqui d wastes ; organi c liqui d waste s fe d throug h air-atomizin g nozzles , specialt yliqui d feed s an d directinject liquid s fed throug h th e aqueou s o rorgani cliqui d fee d systems
. Thi s uni t ca n receiv e an ycombinatio n of waste s ~ liquid , semi-solid , o rsoli d - - wit h a hea t valu e ofu p t o 1 6 millio n Btu/hr
. Eac h o fth e fixe d heart h incinerators ar e supporte d bystorage/blen d tank s locate d i n Tan k Far m #1
. Rate s o ffee d ar e controlle d at eac h incinerator
. Segregate d liqui d waste s ar e store d unti l utilize d i n th e wast e blendin g facilities
. At that time , liquid s ar e delivere d t o th e blendin g tanks wher e th e dail y liqui d fee d t o th e incinerato ri s formulated , tested , an d release d t o th e incinerator
. Blendin g o f store d liqui d waste s t o achiev e optimu m heatin g valu e an d viscosit yfo rincineratio n take s plac e i n Tank s 2 , 4 , 6 & 8
. Si xadditiona l tank s (10,20,30,40 , 5 0 & 60 ) ar e use d t o segregat e differen t wast e strea m type s fo rblendin g o fliqui d fee d t o th e incinerator
. Severa l criteri a ar e importan t i n designin g a blen d fro m availabl e waste s that hav e bee n segregate d principall yb yphysica l an d chemica l properties
. Thes e includ e compatibility , prope rrang e ofheatin g value , an d permi t restriction s regardin g elementa l compositio n (base d o n emissio n limitations)
. I n complianc e wit h th e Benzen e NESHAP , al l tank s are vente d t o individua l carbo n adsorptio n canister s fo rremova l oforganic s befor e vapo ri s discharge d t o th e atmosphere
. Eac h carbo n adsorbe rcaniste ri s essentiall yequivalen tt o a 5 5 gallo n containe ro rgreater , i fnecessary . Al l tank s ar e equippe d wit h conservatio n vents , i n additio n t o th e carbo n caniste radsorber
. Al l tank s ar e grounded , an d flam e arrestor s ar e installe d betwee n th e carbo n adsorber s an d th e tanks
. 2. 3 Manufacturer , Make an d Mode l o fth e Incinerato r[40 CF R §63.1207(f)( 1 )(iii)(A) ] Incinerato runi t no . 3 feature s a two-stag e combustio n process . Ignitio n o fwast e materia l take s plac e i n th e primar

y(lower) combustio n chamber
. Asecondary(upper) combustio n chamberserve s a s a n "after-burner " fo rproces s gases . Ignitio n ofth e wast e take s plac e at temperature s i n exces s o f1,60 0 degree s F
. Th e secondarycombustio n chambe rmaintain s a minimu m temperatur e o f 1,80 0 degree s F
. Thes e temperature s ar e presente d i n curren toperatin g conditions
. Th e Serie s 2 incinerato rha s a tota l o ftwo burners , on e burner , a Nort h America n burner , rate d at 12. 0 millio n Btu/hr. , i s use d i n th e lowe rchambert o maintai n temperatures
. It wil l bur n onl ynatura l ga s o rNo
. 2 fue l oil
. Asecon d burne ri s mounte d i n th e uppe rchamber ; itto o wil l b e use d t o suppl y additiona l hea t an d wil l b e fuele d wit h natura l ga s o r# 2 fue l oil
. Thi s burne ri s a Nort h America n

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### 2- 1 Septembe r200 6

# ENS R

Burner , rate d at 6. 0 millio n Btu/hr
. Liqui d o rgaseou s waste s ar e injecte d throug h separat e fee d nozzle s a s describe d i n sectio n 2.2 , above
. Th e primar

yan d secondarychamber s hav e a n externa l diamete rof9 feet , an d ar e 17. 5 fee t long
. Th e interio rwall s ofbot h chamber s ar e line d wit h approximatel y1 0 inche s ofbric k refractor yan d insulatio n backing , makin g th e interna l operatin g diamete rapproximatel y7'2"
. Th e cross-sectiona l are a ofth e chamber s i s thu s 40. 3 squar e feet
. Combustio n ai ri s controlle d separatel yi n th e uppe r an d lowe rchambers
. Followin g ignitio n ofth e wast e materia l unde rcontrolle d o rstarved-ai rcondition s i n th e lowe r chamber , off-gase s trave l throug h a refractory-line d flu e ga s passag e int o th e uppe rchamber , whic h act s a s a n afterburner
. Turbulenc e i s achieve d b yth e tangentia l introductio n o fai ran d additiona l fue l i n th e uppe rchamber
. Ga s temperature s ar e normall ymaintaine d a t1,800-2,20 0 degree s F i n th e uppe rchambe ran d 1500-190 0 degree s F i n th e lowe rchamber , pursuan t t o curren t Illinoi s EP A permi t operatin g conditions
. Leavin g th e uppe rchamber , th e ho t ga s strea m travel s throug h 2 8 fee t ofrefractory-line d stac k section s befor e reachin g th e star t ofth e ga s scrubbin g system
. Th e combine d volum e ofth e uppe r an d lowe rchambers , th e flu e ga s passag e an d th e hot crossove rsectio n i s approximatel y1,56 7 cubi cfeet
. Th e tota l retentio n tim e o fcombustio n gase s withi n th e syste m i s approximatel y5 seconds
. Th e incinerato ri s rate d at1 6 millio n Btu/hr. , wit h a desig n uni t hea t releas e o f approximatel y10,00 0 Bt u pe rcubi cfoot
. Maximu m ga s volum e whe n firin g a heatreleas e o f1 6 millio n Btu/hr
. i s abou t 15,00 0 acf m at 40 0 degree s F
. 2. 4 Ai rPollutio n Contro l Equipmen t [4 0 CF R §63.1207(f)( 1 )(iii)(G)] Th e ai rpollutio n contro l syste m consist s ofa spra ydrye rabsorbe ran d fabri cfilte rbaghouse
. Th e ai rpollutio n contro l syste m neutralize s acidi ccompound s an d remove s particulat e fro m th e exhaus t gas . Tw o subsystems , th e spra ydrye rabsorbe ran d th e fabri cfilter , carryou tth e chemica l neutralizatio n an d particulat e remova l functions , respectively
. Athird subsystem , th e lim e system , i s use d t o prepar e an d provid e lim e slurr yt o th e spra ydrye rabsorbe rfo rus e i n th e chemica l neutralizatio n process . Th e induce d draft fa n an d stac k provid e th e mechanica l energ yrequire d t o transpor t th e flu e ga s throug h th e interconnectin g ductwork , t o it s eventua l discharg e poin t t o atmosphere
. 2.4. 1 Lim e Syste m Th e lim e syste m prepare s lim e slurr yfo rus e i n th e chemica l neutralizatio n proces s i n sufficien t suppl yan d concentratio n to maintai n continuou s flu e ga s treatmen t i n th e spra ydrye rabsorber
. Th e syste m ha s bee n designe d fo rbatc h mixin g t o provid e thi s service
. Hydrate d lim e i s store d i n a storag e bi n abov e th e lim e preparatio n area . Th e storag e bi n i s size d t o hol d enoug h hydrate d lim e t o maintai n severa l day s o fsyste m operatio n at th e maximu m combustio n rat e o

fth e incinerator
. Lim e i s discharge d throug h th e conica l storag e bi n bottom
. Th e flo wofth e materia l fro m th e bi n i s aide d b ya vibratin g "liv e bottom, " o rbi n activator
. Avariabl e spee d rotar

yfeede ri s use d t o mete rth e hydrate d lim e i n th e proportion s require d fo rbatc h mixin g lim e siurry
. Th e lim e i s mixe d wit h wate ri n a tan k beneat h th e lim e storag e bin
. Th e rotar yfeede r spee d an d th e rat e that wate ri s adde d t o th e lim e slurr ytan k ar e variabl e s o that th e desire d 20 % lim e solid s concentratio n ca n b e achieve d i n th e tank
. Th e variabl e fee d adjustment s allo wwate r an d lim e t o b e adde d to th e lim e slurr ytan k ata rat e that wil l allo wa batc h mod e o fmixing
. A n agitato ri s provide d i n th e slurr ytan k t o mi xth e wate ran d lim e an d t o maintai n th e suspensio n of

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# ENS R

lim e solids
. Th e mixe d lim e slurryi s pumpe d a t a continuou s rat e offlo wthroug h a recirculatio n loo p t o th e atomizer
. 2.4.2 Spra yDr yAbsorbe r Slurryflo wt o th e spra ydrye rabsorbe ri s metere d b ya flo wcontro l valv e t o obtai n th e prope rfee d concentratio n t o th e spra ydrye rabsorbe ratomizer
. Automati c(o rmanual ) adjustmen tt o th e flo wi s mad e a s a functio n o

fth e outpu t fro m a hydrochlori caci d (HCI ) analyze ri n th e ga s duct downstrea m ofth e Fabri cfilter
. Th e amoun t ofslurrymetere d i s proportiona l t o th e amoun tofHC I monitored
. Th e slurrypasse s throug h a stationaryswirl-typ e liqui d distributo rint o th e atomize rwhee l wher e induce d centrifuga l forc e fro m th e rapidl yspinnin g whee l discharge s th e slurrythroug h th e whee l nozzle s at hig h velocity
. Th e desig n ofth e atomize rwheel , its rat e o fspin , an d th e discharg e velocit yo

fth e slurry , creat e a clou d offinel ydivide d droplet s aroun d th e peripheryo fth e atomize r wheel
. Afeedbac k

signa l fro m th e atomize rpowe rtransmitte rprovide s verificatio n that wate rflo wt o th e atomize rincrease s o rdecrease s i n proportio n t o th e spra ydrye rabsorbe routle t temperature
. Flu e ga s enter s fro m th e botto m ofth e spra ydrye rabsorbe rthroug h a vertical , centrall ylocate d disperser
. Th e disperse rdirect s th e flu e ga s throug h th e zon e fille d b yth e atomize d slurryclou d wher e th e flu e ga s an d slurr ymix , an d mos t o

fth e absorptio n occurs . Th e spra ydrye rabsorbe rfeature s a two-poin t product discharge
. Aportio n o fth e drie d spen t chemical s an d as h settl e t o th e botto m o fth e chamber
. Thi s materia l i s discharge d at th e bas e of th e powde rdischarg e cone . Itthe n passe s throug h a lum p breake rwhic h reduce s larg e agglomeration s o

fmateria l t o a manageabl e size
. Finally , i t i s discharge d throug h a rotar yvalv e t o th e conveyin g system
. Th e remainde ro fth e spen t chemical s i s carrie d fro m th e modul e entraine d i n th e flu e gas . 2.4. 3 Fabri c Filte r Ga s exhauste d fro m th e spra ydrye rabsorbe ri s distribute d bymanifol d duct s t o thre e fabri cfilte r module s a

t Uni t 3
. Withi n eac h filte rmodule , th e ga s i s passe d throug h Teflon-coate d fiberglas s clot h bags
. Th e ga s passe s fro m th e outsid e t o th e insid e ofth e filte rbags
. Particulate , entraine d i n th e ga s stream , i s mechanicall ydeposite d o n th e outsid e o fth e filte rbag s a s th e ga s passe s throug h th e cloth
. Th e fabri cfilte rcleanin g mechanis m utilize s jet s ofai rt o clea n th e filte rbags
. Periodically , th e cleanin g sequenc e wil l b e initiated
. Th e sequenc e i s eithe rstarte d atth e en d ofa time d cycle , o r whe n th e differentia l pressur e acros s th e filte rreache s a predetermine d setpoin tofapproximatel y 7.0 " w.c . Th e controlle rthe n sequence s t o eac h rowoffilte rbag s i n eac h module , releasin g a burs t ofai ropposit e t o th e directio n ofga s flow
. Th e quickl yrelease d burs to fai rdislodge s dus tcak e o n th e exterio rofeac h ba g a s i t travel s fro m th e to p t o th e botto m o fth e bags
. Release d fro m th e bag , th e dus t cak e fall s b ygravityinto th e hoppe rat th e botto m ofth e module
. Th e dus t cleane d fro m th e filte rbag s i s remove d atth e bas e o fth e hoppe rthroug h a rotar yvalv e fo r discharg e t o th e conveyin g system
. Treate d byth e spra ydrye rabsorbe ran d filtere d b yth e fabri c filter , th e cleane d flu e ga s exit s th e fabri cfilte rmodule s t o a n outle t manifol d fo rexhaust
. 2 .4. 4 Induce d Draf t Fa n an d Stac k Th e induce d draft fa n an d stac k ar e locate d downstrea m o fth e fabri cfilter
. Combustio n gase s ar e draw n throug h th e syste m bya 7 5 h p induce d draft (ID ) fan , rate d at 15,00 0 acf m at 400 ° F saturated , an d 22 ' wate rcolum n pressure . Th e induce d draft fa n provide s th e mechanis m fo r

C:\Documerrts an d Seffing5\jwoodward\Loca l SeMngsYTemporar

yInternet Rles\0lK7C\0ny x200 6 Tes t ReporLdo c 

### 2- 3 Septembe r200 6

# ENS R

transportin g th e incinerato rflu e ga s throug h th e spra ydrye rabsorber , Fabri cfilter , an d al l interconnectin g ducts
. Th e velocityofth e ga s withi n th e ductin g an d treatmen t device s i s regulate d b yth e dampe rassociate d wit h th e fan
. Treate d gasse s exhauste d fro m th e induce d draft fa n t o th e atmospher e throug h a 90-ft
. hig h stack
. Th e stac k diamete rfo rUni t3 i s 3 9 inche s I.D
. Th e stac k i s equippe d wit h instrumen tsamplin g port s an d a samplin g platfor m fo remission s testing
. Appendi xD provide s detail s o n th e desig n an d sampl e por t location s an d configuration s fo rUni t3
.

C:\Document s an d SetBngs\jwoodward\Loca l SettingsYTemporar

yInternet Rles\OLK7C\Onyx200 6 Test Reportdo c 

### 2- 4 Septembe r200 6

# 3. 0 Summar yo fResult s 

# ENS R

3. 1 Introductio n Thi s sectio n summarize s th e tes tprogra m results
. Appendi xB present s copie s ofENSR' s fiel d dat a an d calculations
. Emissio n dat a i s summarize d i n thi s sectio n an d fee d an d proces s operatin g dat a ar e include d i n Appendi xA
. 3. 2 Stac k

Emissio n Result s fo rPCDDs/PCDF s Metho d 0023 Arequire d separat e analysi s ofth e front-hal fan d back-hal fsampl e trai n fractions
. Progra m sample s wer e submitte d t o Alt a Analytica l Laboratorie s i n E l Dorad o Hills , C Afo ral l analysi s ofal l targe t parameters
. Asummaryofth e PCDD/PCD F emissio n result s o n a TE Q basi s fo rUni t3 ar e include d i n Tabl e 3-1
.
•Th e PCDD/PCD F emission s fo rUni t3 (averag e emission s fo rrun s 1 , 2 an d 3 wer e 0.02 4 ng/m 3

### @ 7 % 0 2 

### ) ar e belo wth e HW C MAC Temissio n standar d o f0. 2 ng/m 3

### @ 7 % 0 2 

### . 3. 3 Stac k

Emissio n Result s fo rTarge t Metal s an d Particulat e Matte r Asummaryo

fth e metal s an d particulat e matte remission s fo rUni t3 i s include d i n Table s 3- 2 throug h 3-7
. Table s 3- 2 an d 3- 3 provid e a detaile d summaryofth e Lo wVolatil e Metal s (LVM ) emission s fro m th e Ma y200 6 an d Jun e 200 6 testing
. Adetaile d summaryo fmetal s emission s categorize d b ySemi-volatil e Metal s (SVM ) an d mercur yi s provide d i n Tabl e 3-4
. Tabl e 3- 5 provide s a summaryo

fal l si xtarge t metals
. Table s 3- 6 an d 3- 7 summariz e th e particulat e matte remission s fro m th e Ma y200 6 an d Jun e 200 6 testing
.

. Th e LV M metal s emission s fo rUni t3 fro m th e Ma y200 6 testin g (averag e emission s fo rrun s 1, 2 an d 3 wer e 24 9 ug/m 3

### @ 7 % 0 2 

### fo rLVMs ) wer e highe rtha n th e HW C MAC Temissio n standard s of9 7 ug/m 3 

### ;

. Th e LV M metal s emission s fo rUni t3 fro m th e Jun e 200 6 testin g (averag e emission s fo rrun s 1 , 2 an d 3 wer e 7.6 1 ug/m 3

### @ 7 % 0 2 

### fo rLVMs ) wer e lowe rtha n th e HW C MAC Temissio n standard s o

f9 7 ug/m 3 

### ;

. Th e SV M an d mercur yemission s fo rUni t3 (averag e fo rrun s 1 , 2 an d 3 wer e 16. 6 ug/m 3

### @ 7 % O 2 

### fo rSVM s an d 61. 5 ug/m 3

### @ 7 % 0 2 

### fo rmercury ) wer e belo wth e HW C MAC Temissio n standard s o

fan d 24 0 pg/m 3

### (correcte d t o 7 % 0 2 

### ) an d 13 0 pg/m 3

### @ 7 % 0 2

### fo rSVM s an d mercur yrespectively ;

. Th e particulat e matte remission s fo rUni t3 fro m th e Ma y200 6 testin g (averag e emission s fo r run s 1 , 2 an d 3 were 6.3 9 mg/m 3

### @ 7 % 0 2 

### ) i s belo wth e HW C MAC Temissio n standar d o f3 4 mg/m 3

### @ 7 % 0 2 

### ;

•Th e particulat e matte remission s fo rUni t3 fro m th e Jun e 200 6 testin g (averag e emission s fo r run s 1 , 2 an d 3 were 2.6 6 mg/m 3

### @ 7 % 0 2 

### ) i s belo wth e HW C MAC Temissio n standar d o f3 4 mg/m 3

### @ 7 % 0 2 

### .

C:\Document s an d Setb'ngs\jwoodward\Loca l SettingsYTemporar

yInterne t Files\0LK7C\0ny x200 6 Tes t Reportdo c 

### 3- 1 Septembe r200 6

# ENS R

3. 4 Metal s Sampl e Contaminatio n Durin g th e Ma y200 6 testing , hig h arseni clevels , whic h wer e inconsisten t amon g th e thre e runs , wer e detecte d i n sampl e result s fro m th e Metho d 2 9 train
. Adetaile d revie wwa s conducte d b ybot h ENS R an d Veoli a personne l t o asses s possibl e cause s and/o rsource s o fcros s contamination
. Thi s revie wincluded :

•Sampl e trai n clean-u p an d preparatio n procedure s •Sampl e por

t acces s an d preparatio n fo rsamplin g •Samplin g anomalie s (i.e. , observation s offilter , sampl e trai n an d procedures ) •La b contaminatio n o rincorrect result s (duplicat e sample s wer e analyze d at a separat e laboratory ) •Operatin g o requipmen t issue s that coul d hav e cause d non-representativ e particulat e matte r containin g hig h arseni ct o b e collecte d i n th e sampl e trai n I t wa s conclude d that there wa s cross-contaminatio n ofth e sampl e trai n durin g samplin g that wa s mos t likel ycause d b ydislodgemen t an d re-entrainmen t i n th e flu e ga s o fscal e that ha d buil t u p o n th e insid e ofth e stac k

sampl e por

t ove rtime , causin g a non-representativ e result
. Also , durin g thi s revie wi t wa s determine d that th e numbe ro ftravers e point s fo rth e port s use d fo rth e dioxi n an d fura n samplin g wa s incorrect base d o n Metho d 1 criteria , althoug h result s wer e wel l withi n th e MAC Temissio n standards
. A s a result , Uni t 3 wa s re-teste d i n Jun e t o furthe revaluat e lo wvolatil e meta l an d dioxi n an d fura n emission s performance
. Port s wer e cleane d prio rt o testin g an d th e correctnumbe ro ftravers e point s wa s use d fo rth e selecte d samplin g locations
. Dioxi n an d fura n result s wer e agai n wel l withi n th e emissio n standard
. Lo wvolatil e meta l result s wer e als o wel l withi n th e emissio n standard
.

C:\Document s an d Seffings\jwoodward\l_oca l Sett'ngsXTemporar

yInterne t Rles\0LK7C\0ny x200 6 Tes t Report.do c 

### 3- 2 Septembe r200 6

# ENS R

Tabl e 3- 1 PCD D /

PCD F Emissio n Results - TE Q Basi s Ru n No
. 

### Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 Star tTim e 

### 14:4 0 09:3 0 09:3 0 Sto p Tim e 

### 17:5 9 13:0 5 11:4 3 Units Sampl e Volum e dscf 128.36 3 129.71 0 126.37 9 Sampl e Volum e m 3 

### 3.6 3 3.6 7 3.5 8 Moistur e Conten t % v/ v 44. 4 47. 7 45. 6 0 2

### Concentratio n % v/ v(dry ) 

### 10.0 0 8.2 0 9.6 0 C 0 2

### Concentratio n % v/ v(dry ) 

### 7.4 0 7.6 0 7.4 0 Isokinetic s % 9 9 10 4 10 0 Stac k Flowrat e dscf m 5,44 1 5,21 2 5,28 0 PCDD/PCD F p g ng/m 3 

### p g ng/m 3 

### p g ng/m 3 

### Parameter s TEF a 

### TE Q TE Q TE Q 2,3,7,8-TCD D 1.0 0 0.0 0 0.0E+0 0 3.4 4 9.4E-0 4 0.0 0 0.0E+0 0 1,2,3,7,8-PeCD D 0.5 0 17. 0 2.3E-0 3 17. 6 2.4E-0 3 16. 7 2.3E-0 3 1,2,3,4,7,8-HxCD D 0.1 0 19. 1 5.3E-0 4 16. 8 4.6E-0 4 14. 6 4. 1 E-0 4 1,2,3,6,7,8-HxCD D 0.1 0 46. 1 1.3E-0 3 34. 7 9.4E-0 4 35. 7 1.0E-0 3 1,2,3,7,8,9-HxCD D 0.1 0 37. 0 1.0E-0 3 27. 1 7.4E-0 4 26. 3 7.3E-0 4 1,2,3,4,6,7,8-HpCD D 0.0 1 19 0 5.2E-0 4 17 5 4.8E-0 4 156. 0 4.4E-0 4 OCD D 0.00 1 24 7 6.8E-0 5 17 5 4.8E-0 5 15 1 4.2E-0 5 2,3,7,8-TCD F 0.1 0 3 0 8. 1 E-0 4 32. 8 8.9E-0 4 31.8 8.9E-0 4 1,2,3,7,8-PeCD F 0.0 5 3 6 4.9E-0 4 4 1 5.6E-0 4 4 1 5.7E-0 4 2,3,4,7,8-PeCD F 0.5 0 6 5 9.0E-0 3 7 0 9.6E-0 3 7 6 1. 1 E-0 2 1,2,3,4,7,8-HxCD F 0.1 0 3 6 9.9E-0 4 3 3 9.0E-0 4 3 8 1. 1 E-0 3 1,2,3,6,7,8-HxCD F 0.1 0 3 2 8.8E-0 4 3 2 8.6E-0 4 3 4 9.4E-0 4 2,3,4,6,7,8-HxCD F 0.1 0 4 4 1.2E-0 3 4 2 1. 1 E-0 3 4 5 1.3E-0 3 1,2,3,7,8,9-HxCD F 0.1 0 1 0 2.8E-0 4 1 2 3.2E-0 4 1 1 3. 1 E-0 4 1,2,3,4,6,7,8-HpCD F 0.0 1 7 8 2. 1 E-0 4 6 7 1.8E-0 4 7 1 2.0E-0 4 1,2,3,4,7,8,9-HpCD F 0.0 1 8 2.2E-0 5 5 1.4E-0 5 7 2.0E-0 5 OCD F 0.00 1 2 0 5.6E-0 6 1 5 4.0E-0 6 1 3 3.7E-0 6 Tota l TEQ s (ng/m 3



### ) = 0.02 0 0.020 0.02 1 Tota l TEQ s (ng/m 3

### @ 7 % 0 2 

### ) = 0.02 5 0.02

2 0.02

6 % o fStandard " = 12 % 11 % 13 %

a

### U.S.EP A(1989 ) Toxi cEquivalenc yFacto r " PCDD/PCD F Standar

d = 0.2 0 ng/dsc m @ 7% 0 2

C:\Oocuments an d Settings\jwoodward\Loca l SettmgsYTemporar

yInterne t Files\0LK7C\0nyx200 6 Tes t Reportdo c 

### 3- 3 Septembe r200 6

# ENS R

Tabl e 3- 2 Emissio n Result s fo rLV M Metal s - Ma y200 6
Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-06 10-May-0 6 11-May-0 6 

### Star t Tim e Unit s 10:0 8 15:0 0 11:2 5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S Samplin gParameters - 

### Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Volum e Metere d def 81.24 8 83.54 6 76.76 1 80.51 8 Sampl e Volum e dsc f 79.59 8 84.05 6 76.26 9 79.97 4 Moistur e % v/ v 43. 0 43. 6 44. 6 43. 7 0 2

### a t Stac k %dr y 12.4 0 9.4 0 10.0 0 10.6 0 Avg
. Stac k

Temp
. ° F 38 1 37 1 37 1 37 5 Stac k Flowrat e dscf m 5,57 6 5,69 1 5,08 8 5,45 1 Isokinetic s % 10 9 10 1 10 2 10 4 Arseni c(As) ~ 

### LV M Quantit yCollecte d M 9 8.5 0 24 8 94 5 40 1 Stac k Cone
. @ 7 % 0 2 

### ug/m 3 

### 6.1 4 12 6 55 7 23 0 Stac k Emissio n Rat e Ib/h r 7.88E-0 5 2.22E-0 3 8.34E-0 3 3.55E-0 3

g/se c 9.92E-0 6 2.80E-0 4 1.05E-0 3 4.47E-0 4 Berylliu m(Be

) — 

### LV M Quantit yCollecte d u g 0.1 0 0.1 0 0.1 0 0.1 0 Stac k Cone
. @ 7 % 0 2 

### ug/m 3 

### 0.0 7 0.0 5 0.0 6 0.0 6 Stac k Emissio n Rat e Ib/h r 9.27E-0 7 8.96E-0 7 8.82E-0 7 9.02E-0 7

g/se c 1.17E-0 7 1.13E-0 7 1.11E-0 7 0.0 0 Tota l Chromiu m(Cr ) - - 

### LV M Quantit yCollecte d u g 16. 7 28. 0 54. 8 33. 2 Stac k Cone
. @ 7 % 0 2 

### Mg/m 3 

### 12. 1 14. 2 32. 3 19. 5 Stac k Emissio n Rat e Ib/h r 1.55E-0 4 2.5 1 E-0 4 4.83E-0 4 2.96E-0 4

g/se c 1.95E-0 5 3.16E-0 5 6.09E-0 5 0.0 0

C:\Documents an d Settings\jwoodward\Loca l SettingsYTemporar

yInterne t Rles\0LK7C\0ny x200 6 Tes t Reportdo c 

### 3- 4 Septembe r200 6

# ENS R

Tabl e 3- 3 Emissio n Result s fo rLV M Metal s - Jun e 200 6 Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 

### StartTim e Unit s 15:1 2 10:0 6 10:0 6 Sto p Tim e 17:2 9 12:2 9 12:4 4 AVG S Samplin gParameter

s - Barometri cPressur e in
. H g 29.5 5 29.5 5 29.5 0 29.5 3 Volum e Metere d de f 78.24 4 82.90 2 81.74 5 80.96 4 Sampl e Volum e dscf 72.24 7 76.48 2 75.57 3 74.76 8 Moistur e % V/ V 

### 46. 7 47.8 45. 5 46. 7 0 2

### a t Stac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 Avg
. Stac k

Temp
. ° F 38 6 38 8 38 6 38 7 Stac k Flowrat e dscf m 4,73 0 4,91 5 5,11 4 4,92 0 Isokinetic s % 10 4 10 6 i

_

### 10 1 10 4 Arseni c(As ) — LV M Quantit yCollecte d p g 5.5 3 3.6 9 5.2 0 4.8 1 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 3.4 4 1.8 6 2.9 8 2.7 6 Stac k Emissio n Rat e Ib/h r 4.79E-0 5 3.14E-0 5 4.65E-0 5 4.19E-0 5

g/se c 6.03E-0 6 3.95E-0 6 0.0 0 0.0 0 Berylliu m(Be ) — LV M Quantit yCollecte d p g 0.0 0 0.087 0 0.0 0 0.029 0 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 0.0 0 0.043 9 0.0 0 0.014 6 Stac k Emissio n Rat e Ib/h r 0.00E+0 0 7.39E-0 7 0.00E+0 0 2.46E-0 7

g/se c 0.00E+0 0 9.32E-0 8 0.00E+0 0 3.11E-0 8 Tota l Chromiu

m(Cr ) - - LV M Quantit yCollecte d p g 9.9 1 3.8 5 11. 2 8.3 0 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 6.1 7 1.9 4 6.4 0 4.8 4 Stac k Emissio n Rat e Ib/h r 8.58E-0 5 3.27E-0 5 9.98E-0 5 7.28E-0 5

g/se c 1.08E-0 5 4.12E-0 6 1.26E-0 5 9.17E-0 6

C:\Documents an d SetSngs\jwoodward\Loca l SettingsYTemporar

yInterne t Files\OLK7C\Onyx200 6 Tes t Report.do c 

### 3- 5 Septembe r200 6

# ENS R

Tabl e 3- 4 Emissio n Result s fo rSV M Metal s an d Mercur y Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-0 6 10-May-06 11-May-0 6 

### Start Tim e Unit s 10:0 8 15:0 0 11:2 5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S Samplin gParameter

s — Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Volum e Metere d de f 81.24 8 83.54 6 76.76 1 80.51 8 Sampl e Volum e dsc f 79.59 8 84.05 6 76.26 9 79.97 4 Moistur e % v/ v 43. 0 43. 6 44. 6 43. 7 0 2

### a tStac k %dr y 12.4 0 9.4 0 10.0 0 10.6 0 Avg
. Stac k

Temp
. ° F 38 1 37 1 37 1 37 5 Stac k Flowrat e dscf m 5,57 6 5,69 1 5,08 8 5,45 1 Isokinetic s % 10 9 10 1 10 2 10 4 Cadmiu m (Cd ) - SV M Quantit yCollecte d p g 0.3 4 1.04 2.4 2 1.2 7 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 0.2 5 0.5 3 1.4 3 0.7 3 Stac k Emissio n Rat e Ib/h r 3.15E-0 6 9.3 1 E-0 6 2.14E-0 5 1.13E-0 5

g/se c 3.97E-0 7 1.17E-0 6 2.69E-0 6 0.0 0 Lea d (Pb ) - SV M Quantit yCollecte d M g 21. 2 19. 6 37. 9 26. 2 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 15. 3 9. 9 22. 3 15. 9 Stac k Emissio n Rat e Ib/h r 1.96E-0 4 1.76E-0 4 3.34E-0 4 2.35E-0 4

g/se c 2.47E-0 5 2.2 1 E-0 5 4.2 1 E-0 5 2.97E-0 5 Mercur y (He ) ~ V M Quantit yCollecte d p g 97. 3 12 1 89. 4
. 10 3 Stac k Cone
. @ 7 % 0 2 

### pg/m 3 

### 70. 3 61. 5 52. 7 61. 5 Stac k Emissio n Rat e Ib/h r 9.0 1 E-0 4 1.09E-0 3 7.88E-0 4 9.25E-0 4

jj/se c 1.14E-0 4 1.37E-0 4 9.93E-0 5 1.17E-0 4

C:\Documents an d Settings\jwoodward\Loca l SettingsYTemporar

yInterne t Files\OLK7C\Onyx200 6 Test Reportdo c 

### 3- 6 Septembe r200 6

### Tabl e 3- 5 Summar yo fTarge t Metal s Lo wVolatil e Metal s Emission s - micrograms/m 3 

### Ma y200 6 Tes t Metal s Ru n 1 Ru n 2 Ru n 3 Averag e A s 6.1 4 12 6 55 7 23 0 B e 0.0 7 0.0 5 0.0 6 0.0 6 C r 12.0 5 14. 2 32. 3 19. 5 Tota l LV M 18. 3 14 0 58 9 24 9 Jun e 200

6 Tes t Metal s Ru n 1 Ru n 2 Ru n 3 Averag e A s 3. 4 1. 9 2.9 8 2. 8 B e 0.0 0 0.0 4 0.0 0 0.0 1 C r 6.1 7 1.9 4 6.4 0 4.8 4 Tota l LV M 9.6 1 3.8 5 9.3 8 7 .6 1

LV M RegulatoryStandar d = 9 7 micrograms/ m 3 Semi-Volatil e I

V eta l Emission s - micrograms/m 3 

### Metal s Ru n 1 Ru n 2 Ru n 3 Averag e P b 15. 3 9. 9 22. 3 15. 9 C d 0.2 5 0.5 3 1.4 3 0.7 3 Tota l SV M 15. 6 10. 5 23. 8 16.6

SV M RegulatoryStandar d = 24 0 micrograms/m 3 

### Mercur yEmission s - micrograms/m 3 

### Metal s Ru n 1 Ru n 2 Ru n 3 Averag e H g 70. 3 61. 5 52. 7 61.5 MercuryRegulatoryStandar d = 13 0 micrograms/m 3

C:\Document s an d SetBngs\jwoodward\Loca l SettingsYTemporar

yInterne t Files\OLK7C\Onyx200 6 Tes t ReporLdo c 

### 3- 7

# ENS R

Tabl e 3- 6 Emissio n Result s fo rParticulate Matte r- Ma y200 6 Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-06 10-May-06 11-May-06 

### Start Tim e Unit s 10:0 8 15:0 0 11:2 5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S Samplin q Parameters - - Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Volum e Metere d dcf 81.99 1 84.12 8 81.69 9 82.60 6 Volum e o

fGa s Collecte d dsc f 79.52 6 83.46 2 80.40 2 81.13 0 Moistur e % v/v 44. 4 44. 8 44. 1 44. 4 0 2

### at Stac k %dr y 12.5 0 9.4 0 10.0 0 10.6 3 C 0 2

### at Stac k %dr y 6.4 0 6.8 0 7.0 0 6.7 3 Avg
. Stac k

Temp
. ° F 37 6 36 6 36 4 36 9 Stac k Flowrat e dscf m 5,46 8 5,48 3 5,28 7 5,41 3 Isokinetic s % 10 9 10 0 10 0 10 3 Particulate Emissio n Result s - Fron t Hal fRins e g 0.003 1 0.006 6 0.005 8 0.005 2 Particulat e Filte r g 0.003 0 0.008 1 0.007 1 0.006 1 Tota l Particulat e m g 6.1 0 14. 7 12. 9 11. 2 P M Loadin g @ 7 % 0 2 

### mg/dsc m 4.4 6 7.5 1 7.2 1 6.3 9 Grai n Loadin g gr/dsc f 0.001 2 0.002 7 0.002 5 0.002 1 Grai n Loadin g @ 7 % 0 2 

### gr/dsc f 0.001 9 0.003 3 0.003 1 0.002 8 Particulate Matte rStandar d = 34 mg/dsc m @ 7% 0 2

C:\Document s an d SetBngs\jwoodward\Loca l SetdngsVTemporar

yInterne t Files\OLK7C\Onyx200 6 Tes t Reportdo c 

### 3- 8 Septembe r200 6

# ENS R

Tabl e 3- 7 Emissio n Result s fo rParticulate Matter- Jun e 200 6 Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 20-Jun-0 6 21-Jun-0 6 

### Start Tim e Unit s 15:1 2 10:0 6 10:0 6 Sto p Tim e 17:2 9 12:2 9 12:4 4 AVG S Samplin gParameter

s - - Barometri cPressur e in
. H g 29.5 5 29.5 5 29.5 0 29.5 3 Volum e Metere d dcf 78.24 4 82.90 2 81.74 5 80.96 4 Volum e ofGa s Collecte d dscf 72.24 7 76.48 2 75.57 3 74.76 8 Moistur e % v/ v 46. 7 47. 8 45. 5 46. 7 0 2

### at Stac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C 0 2

### at Stac k %dr y 7.4 0 7.6 0 7.4 0 7.4 7 Avg
. Stac k

Temp
. ° F 38 6 38 8 38 6 38 7 Stac k Flowrat e dscf m 4,73 0 4,91 5 5,11 4 4,92 0 Isokinetic s % 10 4 10 6 10 1 10 4 Particulat

e Emissio

nResult s — Fron t Hal fRins e g 0.004 0 0.002 8 0.001 7 0. 0 Particulat e Filte r g 0.002 2 0.001 7 0.001 6 0. 0 Tota l Particulat e m g 6.2 0 4.4 6 3.2 5 4.6 4 P M Loadin g @ 7 % 0 2 

### mg/dsc m 3.8 6 2.2

5 1 .8

7 2.66 Grai n Loadin g gr/dscf 0.001 3 0.0009 0 0.0006 6 0.001 0 Grai n Loadin g @ 7 % 0 2 

### gr/dscf 0.001 7 0.001 0 0.000 8 0.001 2

a

### Particulate Matte rStandar d = 34 mg/dscm @ 7% 0 2

C:\Document s an d Settings\jwoodward\Loca l SettingsYTemporar

yInterne t Rles\0LK7C\0ny x200 6 Tes t Reportdo c 

### 3- 9 Septembe r200 6

# 4.0 Samplin g an d Analytica l Procedure s 

# ENS R

4. 1 Samplin g Procedure s Severa l differen t samplin g an d monitorin g technique s wer e use d t o provid e th e require d dat a t o mee t th e goal s o

fthi s tes tprogram . Thre e (3) run s eac h wer e conducte d o n Uni t 3 fo rEP AMetho d 0023A , EP AMetho d 29 , an d EP AMetho d 5
. Th e samplin g activitie s describe d belo wwer e conducte d durin g al l runs . Al l fiel d activitie s wer e documente d i n accordanc e wit h EP Aaccepte d procedure s an d copie s o fal l fiel d note s an d dat a sheet s ar e include d i n Appendi xB o fthi s report
. 4.1. 1 Velocity , Moistur e an d Fixe d Ga s Determination s Ga s strea m velocit yan d temperatur e wer e determine d i n conjunctio n wit h eac h manua l samplin g method
. Atyp e "S " pitot tub e connecte d t o a n incline d wate rmanomete rwa s use d t o determin e velocit yhea d ofth e flu e ga s at eac h duct travers e poin t a s specifie d i n EP AReferenc e Metho d 2
. Th e temperatur e profil e o fth e flu e ga s ateac h duc ttravers e poin t wa s obtaine d bytakin g readings wit h a thermocoupl e an d pyromete rconcurren t wit h th e velocityhea d measurements
. Moistur e conten t wa s determine d a s specifie d i n EP AMetho d 4
. Velocit yan d temperatur e measuremen t profile s wer e establishe d prio rt o testin g t o ai d i n sampl e trai n set-up
. Sample s fo rth e determinatio n o fth e fixe d ga s compositio n wer e collected usin g th e integrate d ba g techniqu e detaile d i n EP A Referenc e Metho d 3
. 4.1 . 2 PCDD/PCD F Samplin g Samplin g fo rdioxin s an d furan s wa s complete d i n accordanc e wit h EP AMetho d 23 A(4 0 CF R 60 , Appendi xA)
. Eac h samplin g ru n wa s 19 2 minute s i n duratio n coverin g 1 6 samplin g point s at1 2 minute s pe rpoint
. 4.1. 3 Metal s an d Particulate Samplin g Th e EP AMultipl e Metal s Trai n (EP AMetho d 29,4 0 CF R 6 0 Appendi xA ) wa s utilize d durin g th e testin g progra m fo rth e collectio n o fth e followin g metals : arsenic , beryllium , cadmium , chromium , lead , an d mercury . Prio rt o metal s analyse s th e tare d filte ran d fron t hal faceton e rins e wer e analyze d gravimetricall yfo rparticulat e matte ri n accordanc e wit h EP AR M 5
. Eac h ru n wa s 12 0 minute s i n duratio n coverin g 1 6 samplin g point s at 7. 5 minute s pe rpoint
. 4. 2 Analytica l Procedure s 4 .2
. 1 PCDD/PCD F Analyse s PCDD/PCD F analyse s wer e performe d b yAlt a Analytica l Laboratory , Inc
. i n E l Dorad o Hills , CA
. Sampl e fraction s wer e extracted , concentrate d an d analyze d b yEP AMetho d 829 0 (Hig h Resolutio n Ga s Chromatograp h / Hig h Resolutio n Mas s Spectrophotomete r(HRGC/HRMS))
. Th e trai n fraction s recovere d fo ranalysi s o fPCDDs/PCDF s includ e th e fron t hal frinse , th e particulat e filter , th e bac k

hal frins e an d th e XA D resi n trap
. Th e analytica l result s fo rth e fron t hal fan d bac k hal ffraction s wer e analyze d an d reporte d separately
.

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# ENS R

4.2. 2 Metal s Analyse s Metal s analyse s fo rth e wast e fee d sample s wer e complete d usin g two separat e procedures
. First , sample s wer e prepare d an d analyze d fo rarsenic , beryllium , cadmium , chromium , an d lea d a s specifie d i n EP AMetho d 602 0 (ICP-MS) , SW846,3 r d

### Edition
. Mercurywa s analyze d vi a metho d 747 1 A
. Metal s analyse s wer e performe d byMaxxa m Analytica l Inc
. o fBurlington , Ontari o (Canada)
. 4. 3 Proces s Operatin g Condition s Throughou tth e fiel d program , detaile d proces s informatio n wa s collecte d continuousl ybyth e facility' s proces s contro l computer s an d dat a acquisitio n syste m (DAS)
. Proces s dat a includin g minimum , maximu m an d averag e value s fo rke yproces s variable s recorde d durin g eac h tes t condition
. I n general , target-operatin g condition s specifie d wer e achieved
.

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# ENS R

5.0 Qualit

yAssuranc e
5. 1 Introductio n Thi s sectio n present s th e result s ofal l QA/Q C measure s implemente d durin g th e fiel d samplin g progra m an d al l phase s ofsubsequen tanalysis
. Dat a generate d fo rth e progra m ar e judge d t o b e vali d a s overal l accurac yan d precisio n result s ar e consisten twit h genera l objectives
. Analytica l QA/Q C dat a ar e presente d t o supportal l sampl e result s use d fo rdeterminin g complianc e wit h performanc e criteri a o remissio n standards
. Throughou tth e overal l program , al l samplin g wa s performe d usin g samplin g protocol s describe d herei n an d approve d b yUSEP Aan d th e Illinoi s Environmenta l Protectio n Agency
. 5.1. 1 Pre-Samplin g Activitie s Pre-samplin g activitie s include d equipmen tcalibration , sampl e medi a preparation , cleanin g of sampl e trai n glassware , preparatio n o fcomputer-generate d sampl e label s an d othe rmiscellaneou s tasks
. Eac h o

fthes e activitie s ar e describe d o rreference d i n th e followin g subsections
. Othe rpre samplin g activitie s include d suc h detail s a s tea m meetings , equipmen tpackin g an d shipment , equipmen tsetup , an d finalizatio n ofal l detail s leadin g u p t o th e coordinate d initiatio n o fth e samplin g program . 5.1.2 Equipmen t Calibratio n Amos timportan t aspec tofpre-samplin g preparation s wa s th e inspectio n an d calibratio n ofal l equipmen tuse d fo rth e fiel d effort
. Equipmen twa s inspecte d fo rprope roperatio n an d durability prio rt o calibration
. Calibratio n o fequipmen twa s conducte d i n accordanc e wit h th e procedure s outline d i n th e EP Adocumen tentitle d "QualityAssuranc e Handboo k fo rAi rPollutio n Measuremen t Systems ; Volum e III—Stationar ySourc e Specifi cMethods " (EPA-600/4-77-027b)
. Equipmen t calibratio n wa s performe d i n accordanc e wit h EP Aguideline s and/o rmanufacturer' s recommendations
. Copie s o fthese s calibration s ar e presente d i n Appendi xC
. Example s o ffiel d equipmen tuse d an d typica l calibratio n requirement s follows :

•PROB E NOZZLE S 

### (Q AHandboo k Sectio n 3.4.2 , pg . 19 ) - measurement s o fth e nozzl e I D (to th e neares t0.001-in. ) alon g thre e differen t diameters wit h a micrometer
. Differenc e betwee n th e hig h an d lo wvalue s shoul d notexcee d 0.00 4 in
. Post-tes tcheck s - inspectfo rdamage
. •PITO TTUBE S 

### (Q AHandboo k Sectio n 3.1.2 , pp . 1 -13 ) - measure d fo rappropriat e spacin g an d dimension s o rcalibrat e i n a win d tunnel
. Rejectio n criteri a give n o n th e calibratio n sheet
. Post-tes tcheck s - inspectfo rdamage
. •THERMOCOUPLE S 

### (Q AHandboo k Sectio n 3.4.2 , pp . 15-18 ) - verifyagains ta mercury-in-glas s thermomete rattw o o rmore point s includin g th e anticipate d measuremen trange . Acceptanc e limit s - impinge r±2°F ; DG M ±5.4°F ; stac k ±1. 5 percen to

fstac k temperature
. •DR YGA S METER S 

### (Q AHandboo k Sectio n 3.4.2 , pp . 1 -12 ) - calibrat e agains ta we ttes t meter
. Acceptanc e criteri a - pretes tY i = Y+ 0.2 ; posttes t Y= ±0.0 5 Yi
. •FIEL D BAROMETER S 

### (Q AHandboo k Sectio n 3.4.2 , pp . 18-19 ) - compar e agains ta mercury in-glas s baromete ro rus e AirportStatio n B P an d correctfo relevation
. Acceptanc e criteri a - ±0.0 2 in
. Hg ; post-tes tcheck s - same .

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### 5- 1 Septembe r200 6

# ENS R

5.1. 3 Glassware Preparatio n Sampl e trai n glasswar e an d sampl e container s require d specialize d pre-cleanin g t o avoi d contaminatio n o

fth e sampl e fro m th e collectio n containe ro rdevices
. Cleaning/storag e procedure s fo rsampl e trai n glasswar e ar e summarize d below
. Not e that al l bottl e cap s ar e fitte d wit h Teflo n liners , whic h wer e cleane d i n th e sam e manne ra s th e bottle s themselves
. Sampl e container s use d fo rwast e fee d stream s ar e purchase d pre-cleane d an d seale d t o specifie d EP Aprotocols
.

•EP AMETHO D 001 0 / 0023 A GLASSWAR E AN D CONTAINER S (PCDDS/PCDFS ) 

### - washe d wit h soa p an d water , rinse d thre e time s wit h deionize d (DI ) water , bake d at400° C fo r2-hours , rinse d thre e time s wit h pesticid e grad e methylen e chloride , rinse d thre e time s wit h pesticid e grad e toluen e an d ai rdry
.

•EP AMETHO D 5 / 29 / 006 0 GLASSWAR E AN D CONTAINER S (METAL S AN D PARTICULAT E MATTER )



### - washe d wit h soa p an d water , rinse d wit h hotta p wate ran d rinse d thre e time s wit h reagen t water
. Th e glasswar e wa s soake d i n a 10 % nitri caci d solutio n fo ra minimu m o f4-hours , rinse d thre e time s wit h reagen twater , rinse d a fina l tim e wit h aceton e an d air-dried
. Al l glasswar e opening s wher e contaminatio n ca n occurar e covere d wit h Parafil m unti l th e samplin g trai n wa s assemble d prio rt o sampling
. 5.1.3. 1 

### Sampl e Medi a Preparatio n Al l reagent s wer e checke d i n accordanc e wit h ENSR' s existin g Q C Progra m t o minimiz e th e probabilityofusin g contaminate d solvents
. Thi s include d th e us e ofth e prope rgrad e reagents/solvent s a s specifie d i n th e tes tmethod , selectio n ofreagent s fro m th e sam e lotan d collectio n an d analysi s o fth e appropriat e blanks
. Samplin g medi a wa s procure d an d prepare d i n accordanc e wit h th e appropriat e tes tmethod s a s describe d below :

•XA D resi n use d i n th e Metho d 0023 Atrai n wa s purchase d ne wan d packe d i n speciall y designe d sorben ttraps
. Al l glas s cleanin g an d sorben tpackin g procedure s followe d th e protocol s specifie d i n EP AMetho d 0023A
.
•Quart z filters use d i n th e Metho d 5 / 2 9 / 006 0 samplin g trai n wer e supplie d b yMaxxa m Analytics , Inc
. wh o pre-scree n filters fo rmetal s content
.

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yInterne t Files\OLK7C\Onyx200 6 Tes t Report.do c 

### 5- 2 Septembe r200 6

# ENS R

Appendi xA FacilityOperatin g Dat a

S:\_JOB\2006\Onyx\Performanc e Test\Report\Ony x200 6 Tes tReport.do c Septembe r200 6

### Uni t #

3 ) Ru n #

1 Date : 05/10/0

6 Tes t Time : 09:4

7 to 13:5 1 Ru n Length : 19

9 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c PC C Hig h Bt u 682 0 0. 5 0. 3 0.1 3 2. 5 1 5 PC C Lo wBt u 50 0 0. 5 0.3 3 0.0 5 2. 5 ! 5 (Chlorin e Spike ) 50 0 85. 5 0. 1 0.1 3 2. 5 1 

### 5 PC C S p Fd r 50 0 0. 5 0. 1 0.0 5 2. 5 i 5 (Chromiu m Spike ) 50 0 0. 5 23. 4 0.1 3 2. 5 1 

### 1. 3 PC C Soli d Charge s 50 0 0. 5 81. 8 0.2 1 20. 1 1 8. 6 (Lea d Spike ) 50 0 0. 5 66. 4 0.1 3 63000 0 20 8 6 (Chlorin e Spike ) 50 0 63. 5 96. 3 0.1 3 2. 5 1 5 (MercurySpike ) 50 0 0. 5 0. 1 60 0 2. 5 1 5 Total s

### ) Averag e Therma l Chlorin e As h Mercury Lea d PP M Fee d rat e Loadin g Loadin g Loadin g Loadin g Loadin g liu m Chromiu m (Ib/hr ) (MMBtu/hr ; (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 2. 5 98 2 6.7 0 4.9 1 2.9 5 0.00012 8 0.0 0 0. 1 2. 5 171 5 0.8 6 8.5 8 5.6 6 0.00008 6 0.0 0 0. 1 2. 5 11 7 0.0 6 100.0 4 0.1 2 0.00001 5 0.0 0 0. 1 2. 5 45 8 0.2 3 2.2 9 0.4 6 0.00002 3 0.0 0 0. 1 18000 0 25 1 0.1 3 1.2 6 58.7 3 Q.00003 3 0.0 0 0.2 9 26. 1 61 9 0.3 1 3.1 0 506.3 4 0.00013 0 0.0 1 0. 1 2. 5 9 2 0.0 5 0.4 6 61.0 9 0.00001 2 57.9 6 0. 1 2. 5 13 8 0.0 7 87.6 3 132.8 9 0.00001 8 0.0 0 0. 1 2. 5 1.35 0.0 0 0.0 1 0.0 0 0.00081 0 0.0 0
437 3 8.3 9 208.2 6 768.2 4 0.0012 5 57.9 8

### Cadmiu m Arseni c

Loadin g Loadin g (Ib/hr ) (Ib/hr

) 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 Berylliu m Chromiu m

Loadin g Loadin g (Ib/hr ) (Ib/hr

) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 45.1 8 0.0 0 0.0 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 2 0.0 2 0.0 0 45.2 0

### Uni t #

3 1 Ru n #

2 Date : 05/10/0

6 Tes t Time : 14:5 1 to 18:1 7 Ru n Length : 20

6 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 672 0 0.5 6 0.2 8 0.1 3 2. 5 1 5 PC C Lo wBt u 50 0 0. 5 0.3 2 0.0 5 2. 5 1 5 (Chlorin e Spike ) 50 0 85. 5 0. 1 0.1 3 2. 5 1 

### 5 PC C S p Fd r 50 0 0. 5 0. 1 0.0 5 2. 5 1 5 (Chromiu m Spike ) 50 0 0. 5 23. 4 0.1 3 2. 5 1 

### 2. 6 PC C Soli d Charge s 50 0 0. 5 8 2 0.1 9 19. 6 1 9. 5 (Lea d Spike ) 50 0 0. 5 66. 4 0.1 3 63000 0 22 1 1. 6 (Chlorin e Spike ) 50 0 63. 5 96. 3 0.1 3 2. 5 1 5 (MercurySpike ) 50 0 0. 5 0. 1 60 0 2. 5 1 5 Total s

### Averag e Therma l Chlorin e As h Mercury Lea d PP M Fee d rat e Loadin g Loadin g Loadin g Loadin g Loadin g Hu m Chromiu m (Ib/hr ) (MMBtu/hr) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 2. 5 99 2 6.6 7 5.5 6 2.7 8 0.00012 9 0.0 0 0. 1 2. 5 168 1 0.8 4 8.4 1 5.3 8 0.00008 4 0.0 0 0. 1 2. 5 10 0 0.0 5 85.5 0 0.1 0 0.00001 3 0.0 0 0. 1 2. 5 46 1 0.2 3 2.3 1 0.4 6 0.00002 3 0.0 0 0. 1 18000 0 25 5 0.1 3 1.2 8 59.6 7 0.00003 3 0.0 0 0.4 3 28. 1 71 9 0.3 6 3.6 0 589.5 8 0.00013 7 .0.0 1 0. 1 2. 5 10 8 0.0 5 0.5 4 71.7 1 0.00001 4 68.0 4 0. 1 2. 5 16 1 0.0 8 102.2 4 155.0 4 0.00002 1 0.0 0 0. 1 2. 5 1.5 8 0.0 0 0.0 1 0.0 0 0.00094 8 0.0 0
447 9 8.4 1 209.4 2 884.7 2 0.0014 0 68.0 6

### Cadmiu m Arseni cBerylliu m Chromiu m

Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 2 0.0 0 0.0 0 0.0 0

0.0 1 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0

0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0

0.0 0 0.0 0 0.0 0 45.9 0 0.0 2 0.0 0 0.0 0 0.0 0
0.0 3 0.0 2 0.0 0 45.9 3

### Uni t #

3 ! Ru n # 3 Date : 05/11/0

6 Tes t Time : 11:25 t o 14:4 8 Ru n Length : 20

3 minutes PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 763 0 0.6 6 0.2 8 0.1 3 2. 5 1 5 PC C Lo wBt u 50 0 0. 5 0.3 1 0.0 5 2. 5 1 5 (Chlorin e Spike ) 50 0 85. 5 0. 1 0.1 3 2. 5 1 

### 5 PC C S p Fd r 50 0 0. 5 0. 1 0.0 5 2. 5 1 5 (Chromiu m Spike ) 50 0 0. 5 23. 4 0.1 3 2. 5 1 

### 2 PC C Soli d Charge s 50 0 0. 5 82. 6 0.3 5 36. 8 1 11. 2 (Lea d Spike ) 50 0 0. 5 66. 4 0.1 3 63000 0 28 3 9. 1 (Chlorin e Spike ) 50 0 63: 5 96. 3 0.1 3 15 0 1 5 (MercurySpike ) 50 0 0. 5 0. 1 60 0 2. 5 1 5 Total s

### Averag e Therma l Chlorin e As h Mercur yLea d

PP M PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr) (Ib/hr

) (Ib/hr

) (Ib/hr

) (ib/hr

) 0. 1 2. 5 100 0 7.6 3 6.6 0 2.8 0 0.00013 0 0.0 0 0. 1 2. 5 193 1 0.9 7 9.6 6 5.9 9 0.00009 7 0.0 0 0. 1 2. 5 9 2 0.0 5 78.6 6 0.0 9 0.00001 2 0.0 0 0. 1 2. 5 44 8 0.2 2 2.2 4 0.4 5 0.00002 2 0.0 0 0.1
. 18000 0 24 5 0.1 2 1.2 3 57.3 3 0.00003 2 0.0 0 0. 9 26. 3 72 3 0.3 6 3.6 2 597.2 0 0.00025 3 0.0 3 0. 1 1. 3 10 6 0.0 5 0.5 3 70.3 8 0.00001 4 66.7 8 0. 1 2. 5 15 8 0.0 8 100.3 3 152.1 5 0.00002 1 0.0 2 0. 1 2. 5 1.5 5 0.0 0 0.0 1 0.0 0 0.00093 0 0.0 0 470 5 9.4 8 202.8 6 886.3 9 0.0015 1 66.8 4

### Cadmiu m Arseni cBerylliu m Chromiu m

Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 44.1 0 0.0 0 0.0 1 0.0 0 0.0 2 0.0 3 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 3 0.0 3 0.0 0 44.1 3

### Uni t #3

Ru n # 1 Date : 06/19/0

6 Tes t Time : 14:4

0 to 18:0

5 Ru n Length : 20

5 minutes PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c PC C Hig h Bt u 993 0 3. 2 1. 5 0.41 3 18. 8 1.9 8 2. 5 PC C Lo wBt u 50 0 0. 5 0. 2 0.020 2 1.2 7 0.037 2 0.27 2 (Chlorin e Spike ) 317 0 85. 5 0. 1 0.01 1 0. 1 0.0 2 0. 2 PC C S p Fd r 50 0 0. 5 0. 1 0.0003 5 1.3 8 0.005 2 12. 1 (Chromiu m Spike ) 50 0 0. 5 25. 9 0.00 2 80 0 97 0 88 0 PC C Soli d Charge s 88 0 0. 6 70. 6 0.02 5 12.9 3 0.3 0 6.7 3 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000 0 2 7 2 5 (Chlorin e Spike ) 50 0 63. 5 97. 4 0.0 2 17 0 5 2 5 (MercurySpike ) 50 0 0. 5 0. 1 64 6 0. 1 0.0 2 0. 2 Total s

### ) Averag e Therma l Chlorin e As h Mercury Lea d PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g liu m Chromiu m (Ib/hr ) (MMBtu/hr ) (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 13. 3 111 0 11.0 2 35.5 2 16.6 5 0.00045 8 0.0 2 1.00 1 0.46 2 189 6 0.9 5 9.4 8 3.7 9 0.00003 8 0.0 0 0.0 5 0.0 4 9 5 0.3 0 81.2 3 0.1 0 0.00000 1 0.0 0 0.0 1 0.012 1 56 9 0.2 8 2.8 5 0.5 7 0.00000 0 0.0 0 96 0 18000 0 25 1 0.1 3 1.2 6 65.0 1 0.00000 1 0.2 0 0.3 7 157.8 1 79 8 0.7 0 4.7 1 563.7 4 0.00002 0 0.0 1 4. 8 2 11 9 0.0 6 0.6 0 78.0 6 0.00000 2 74.9 7 2. 5 2 17 9 0.0 9 113.6 7 174.3 5 0.00000 4 0.0 3 0.0 5 0.0 4 1.75 0.0 0 0.0 1 0.0 0 0.00113 1 0.0 0 501 9 13.5 3 249.3 0 902.2 7 0.0016 6 75.2 4

### Cadmiu m

Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.2 4 0.0 0 0.0 0 0.0 0 0.0 0 Arseni c Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 1 0.2 2 0.0 1 0.0 0 0.0 0 0.0 0 Berylliu m Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.2 4 0.0 0 0.0 0 0.0 0 0.0 0 Chromiu m Loadin g (Ib/hr ) 0.0 1 0.0 0 0.0 0 0.0 0 45.1 8 0.1 3 0.0 0 0.0 0 0.0 0
0.2 5 0.2 4 0.2 4 45.3 2

### Uni t #

3 ) Ru n #

2 Date : 06/20/0

6 Tes t Time : 09:30 to 13:0 5 Ru n Length : 21 5 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c PC C Hig h Bt u 900 0 2. 3 4. 9 0.41 3 4 0.3 5 2. 5 PC C Lo wBt u 50 0 0. 5 0. 2 0.0019 2 0.0 4 0.003 4 0.25 3 (Chlorin e Spike ) 317 0 85. 5 0. 1 0.01 4 0. 1 0.0 2 0. 2 PC C S p Fd r 50 0 0. 5 0. 1 0.000 2 0.091 4 0.00 2 0.18 6 (Chromiu m Spike ) 50 0 0. 5 25. 9 0.00 2 10 0 2 0 20 0 PC C Soli d Charge s 82 4 0. 6 69. 9 0.03 8 16.4 5 0.3 7 6.2 5 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000 0 3 2 2 5 (Chlorin e Spike ) 50 0 63. 5 97. 4 0.0 2 4 2 5 2 5 (MercurySpike ) 50 0 0. 5 0. 1 64 6 0. 1 0.0 2 0. 2 Total s

### Averag e Therma l Chlorin e As h Mercury Lea d

PP M PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr ) (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 1 3 112 6 10.1 3 25.9 0 55.1 7 0.00046 5 0.0 0 0.00 1 0.057 9 195 9 0.9 8 9.8 0 3.9 2 0.00000 4 0.0 0 0.0 5 0.04 6 10 2 0.3 2 87.2 1 0.1 0 0.00000 1 0.0 0 0.00 1 0.011 6 54 3 0.2 7 2.7 2 0.5 4 0.00000 0 0.0 0 5 0 18000 0 25 0 0.1 3 1.2 5 64.7 5 0.00000 1 0.0 3 0.3 1 11.8 8 80 5 0.6 6 4.9 6 563.0 1 0.00003 0 0.0 1 7. 8 2 11 7 0.0 6 0.5 9 76.7 5 0.00000 2 73.7 1 2. 5 2 17 6 " 0.0 9 111.7 6 171.4 2 0.00000 4 0.0 1 0.0 5 0.0 4 1.7 2 0.0 0 0.0 1 0.0 0 0.00111 1 0.0 0 508 0 12.6 4 244.1 8 935.6 7 0.0016 2 73.7 6

### Cadmiu m

Loadin g (lb/hr) 0.0 0 0.0 0 0.0 0 0.0 0 0.01
. 0.0 0 0.0 0 0.0 0 0.0 0 Arseni c Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 5 0.0 1 0.0 0 0.0 0 0.0 0 Berylliu m Loadin g (Ib/hr ) 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 Chromiu m Loadin g (Ib/hr ) 0.0 1 0.0 0 0.0 0 0.0 0 45.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 1 0.0 7 0.0 1 45.0 2

### Uni t #

3 ) Ru n # 3 Date : 06/21/06 Test Time : 09:30 t o 13:1 9 Ru n Length : 229 minute s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c PC C Hig h Bt u 1022 0 3. 1 0. 4 0.67 9 3.8 5 0.8 3 6.7 7 PC C Lo wBt u 50 0 0. 5 0. 2 0.0018 4 0.0 4 0.005 4 0.25 7 (Chlorin e Spike ) 317 0 85. 5 0. 1 0.004 5 0. 1 0.0 2 0. 2 PC C S p Fd r 50 0 0. 5 0. 1 0.000 2 0.043 2 0.00 2 0.070 9 (Chromiu m Spike ) 50 0 0. 5 25. 9 0.00 2 10 0 2 0 20 0 PC C Soli d Charge s 79 3 0. 5 70. 8 0.15 7 18.4 6 0.4 4 5.7 6 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000 0 4 2 2 5 (Chlorin e Spike ) 50 0 63. 5 97. 4 0.0 2 1 8 5 2 5 (MercurySpike ) 50 0 0. 5 0. 1 64 6 0. 1 0.0 2 0. 2 Total s

### Averag e Therma l Chlorin e As h Mercury Lea d

PP M PP M Fee d rat e Loadin g Loadin g Loadin g Loadin g Loadin g Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr ) (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 5.7 4 107 9 11.0 3 33.4 5 4.3 2 0.00073 3 0.0 0 0.00 1 0.058 6 203 9 1.0 2 10.2 0 4.0 8 0.00000 4 0.0 0 0.0 5 0.0 4 9 6 0.3 0 82.0 8 0.1 0 0.00000 0 0.0 0 0.00 1 0.040 8 54 7 0.2 7 2.7 3 0.5 5 0.00000 0 0.0 0 5 0 18000 0 24 9 0.1 2 1.2 5 64.4 9 0.00000 0 0.0 2 0.3 5 12.4 7 81 5 0.6 5 4.3 1 577.2 9 0.00012 8 0.0 2 8. 1 2 11 9 0.0 6 0.6 0 78.0 6 0.00000 2 74.9 7 2. 5 2 17 8 0.0 9 113.0 3 173.3 7 0.00000 4 0.0 0 0.0 5 0.0 4 1.74 0.0 0 0.0 1 0.0 0 0.00112 4 0.0 0 512 4 13.5 5 247.6 5 902.2 5 0.0020 0 75.0 2

### Cadmiu m Arseni c

Loadin g Loadin g (Ib/hr ) (Ib/hr

) 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 5 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 Berylliu m Chromiu m

Loadin g Loadin g (Ib/hr ) (Ib/hr

) 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 44.8 2 0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 1 0.0 7 0.0 1 44.8 4

### ) Uni t 3 Operating.Parameter s June , 200 6

Baghous e Inle

t Temp . (Deg F

) (Ave
. o ftes t ru n ave.'s ) PC C Temp . (Deg F

) (Ave
. oftes t ru n ave.'s ) SC C Temp . (Deg F

) (Ave
. o ftes t ru n ave.'s ) Stackflow(ACFM ) (Ave
. o fmax . HRA' s o

feac h tes t run ) Pumpabl e Waste Fee d (Lb/hr ) (Ave
. o fmax . HRA' s o

feac h tes t run ) (Includes average spiked liquids flows) Tota l Waste Fee d (Lb/hr ) (Ave
. o fmax . HRA' s o

feac h tes t run ) (Includes average spiked liquids flows) Mercur yFeed (Lb/hr) (Ave
. o ftes t ru n ave.'s ) As h Fee d (Lb/hr) (Ave
. oftes t ru n ave.'s ) LV M Fee d (Lb/hr) (Ave
. o ftes t ru n ave.'s ) SV M Fee d (Lb/hr) (Ave
. o ftes t ru n ave.'s ) Chlorin e Fee d (Lb/hr

) (Ave
. o ftes t ru n ave.'s ) Ru n 1 Ru n 2 Ru n 3 Averag e 42 0 42 1 42 1 42 0 173 5 172 5 174 1 173 4 184 5 185 0 185 1 184 9 1488 8 1534 9 1526 7 1516 8 414 7 416 1 417 2 416 0 346 352

345



### n a 527 3 536 7 539 1 534 4 346 352

345



### n a 0.001 7 0.001 6 0.002 0 0.001 8 90 2 93 6 90 2 91 3
4 6 4 5 4 5 4 5
7 5 ' 7 4 7 5 7 5
24 9 24 4 24 8 24 7

### Uni t 3 Operatin g Parameter s

May , 200 6

Ru n 1 

### 42 0
171 3 184 5 1487 3 371 8 368 AIM 368 

### 0.001 3 76 8
4 5
5 8 20 8 Ru n 2

42 0
171 5 184 5 1542 8 368 3 355 

### 486 2 355 

### 0.001 4 88 5 4 6 68 20 9 Ru n 3

42 0
171 2 184 6 1446 8 380 0 337 

### 479 3 337 

### 0.001 5 88 6
4 4 6 7 20 3 Averag e

42 0
171 3 184 5 1492 3 373 4
na 479 1 na 0.001 4 84 6
4 5 6 4 20 7

# ENS R

Appendi xB Referenc e Metho d Fiel d Data an d Calculation s

S:\_JOB\2006\Onyx\Performanc e Test\Report\Ony x200 6 Tes tReport.do c Septembe r200 6

# May2006 Tes t)



# Particulate Matte rData

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 5 Samplin g Parameter s Ru n No
. Ru n 1 Ru n 2 Ru n 3 AVG S Dat e 10-May-0 6 io-May-06 11-May-0 6 AVG S Star tTim e Units 10:0 8 15:0 0 11:2 5 AVG S Sto p Tim e 12:5 1 17:1 6 13:3 9 Nozzl e Diamete r inche s 0.41 2 0.44 0 0.44 0 0.43 1 Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.0 6 Ne tSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dc f 81.99 1 84.12 8 81.69 9 82.60 6 Avg
. DG M Temp
. ° F 85. 9 72. 5 77. 1 78. 5 Av g Delt a H i n H 2 0 1.5 7 1.73 1.5 6 1 .62 Av g Delt a H in
. H g 0.115 8 0.127 4 0.114 6 0.119 3 DG M Calibratio n Facto r 

## - 1.027 0 1.027 0 1.027 0 1.027 0 Ga s Sampl

e Volum e dscf 79.52 6 83.46

2 80.40

2 81.13

0 Tota l Wate rCollecte d m L 1344. 7 1438. 7 1343. 8 1375. 7 Volum e ofWate rVapo r scf 63.40 3 67.83 5 63.36 0 64.86 6 Moistur e (measured ) % v/ v 44. 4 44. 8 44. 1 44. 4 Moistur e ( @ saturation ) % v/ v I 102. 8 103. 0 103. 0 102. 9 Dr yMol e Fraction , 100-% M 

## - 0.556 4 0.551 6 0.559 3 0.555 8 C O zat Stac k %dr y 6.4 0 6.8 0 7.0 0 6.7 3 0 2a t Stac k %dr y 12.5 0 9.4 0 10.0 0 10.6 3 C O + N 2 %dr y 81.1 0 83.8 0 83.0 0 82.6 3 Dr yMolecula rWeigh t Ib/lb-mol e 29.5 2 29.4 6 29.5 2 1 29.5 0 We tMolecula rWeigh t Ib/lb-mol e 24.4 1 24.3 2 24.4 4 24.3 9 Exces s Ai ra

tStac k % 140. 3 73. 9 83. 9 99. 4 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 0 0.2 2 0.2 2 0.0 7 0.1 7 Stac k Pressur e inH g 29.1 2 29.0 4 29.0 6 29.0 7 Avg
. Stac k

Temp
. ° F 376. 4 366. 2 364. 3 369. 0 Avg
. Sqroo to

fDelt a P — 0.412 5 0.414 5 0.394 6 0.407 2 SD E Averag e — 11.93 1 11.91 5 11.33 0 11.72 5 Pito tCoefficien t — 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,92 8 1,932 1,832 1,89 7 Stac k Flowrat e wetacf m 15,99 8 16,02 7 15,19 8 15,74 1 Stac k Flowrat e we tscf m 9,82 7 9,94 0 9,45 3 9,74 0 Stac k Flowrat e dscf m 5,46 8 5,48

3 5,28

7 5,41 3 Isokinetics % 10 9 10

0 10

0 10

3 Mete rBo xNo
. — 8061 0 8061 0 8061 0 — Delt a H @ i n H a O 1.80 3 1.80 3 1.80 3 - - Fiel d Q AYq c — 1.046 5 1.059 1 1.037 5 1.047 7 [Deviation ] Pre- Y % 1.90 % 3.13 % 1.02 % 2.02 % S:\_JOB\2006\OnyiAPetformance TesRTes t0ata\Otiy xMa y2006\(M S P M #

3 Ma y2006 da

y2.xls]DAT

A

### Metho d 5 Samplin g Parameter s

P T Run l Ru n

### 2 Ru n 

### 3 P T Delt a P SQR T

Delt a P DG M

I N DG M

OU T Delt a H STAC K TEM P Delt a P SQR T Delt a P DG M

I N DG M

OU T Delt a H STAC K

TEM P Delt a P SQR T Delt a P DG M

I N DG M

OU T Delt a H STAC K

TEM P a 1 

### 0.1 5 0.387 3 7 0 7 0 1.38 34 6 0.1 8 0.424 3 76 7 5 1.90 37 0 0.1 3 0.360 6 7 0 6 9 1.30 35 0 a 2 

### 0.2 0 0.447 2 7 7 72 1.8 1 37 8 0.2 0 0.447 2 7 5 74 1.99 37 0 0.1 6 0.400 0 7 4 6 9 1.58 36 4 a 3 

### 0.2 0 0.447 2 8 2 7 4 1.8 1 37 8 0.2 1 0.458 3 7 6 7 3 2.0 9 36 8 0.1 7 0.412 3 7 7 7 0 1.68 36 9 a 4 

### 0.2 1 0.458 3 8 5 7 5 1.89 38 8 0.2 0 0.447 2 7 7 7 2 1.99 36 6 0.1 9 0.435 9 8 0 7 1 1.88 36 9 a 5 

### 0.2 0 0.447 2 8 6 8 0 1.82 39 0 0.1 9 0.435 9 7 5 7 1 1.9 0 36 3 0.1 7 0.412 3 8 1 7 2 1.70 36 8 a 6 

### 0.1 8 0.424 3 9 0 8 2 1.66 37 4 0.1 9 0.435 9 7 1 6 9 1.90 36 4 0.1 6 0.400 0 8 2 7 3 1.60 36 2 a 7 

### 0.1 5 0.387 3 9 2 8 2 1.3 8 37 5 0.1 5 0.387 3 7 6 6 9 1.50 36 2 0.1 6 0.400 0 8 3 7 4 1.60 36 4 a 8 

### 0.1 1 0.331 7 9 3 8 3 1.0 2 37 4 0.1 1 0.331 7 7 6 6 9 1.1 0 36 3 0.1 4 0.374 2 8 3 7 5 1.40 36 5 b 1 

### 0.1 6 0.400 0 8 6 8 4 1.4 8 37 4 0.1 2 0.346 4 6 9 6 8 1.2 0 36 5 0.1 5 0.387 3 7 5 7 4 1.50 36 3 b2 

### 0.1 8 0.424 3 9 3 8 5 1.67 37 7 0.1 6 0.400 0 7 4 6 8 1.60 36 5 0.1 7 0.412 3 8 0 7 5 1.70 36 6 b 3 

### 0.1 8 0.424 3 9 4 8 6 1.67 37 8 0.1 8 0.424 3 7 5 6 8 1.80 36 5 0.1 7 0.412 3 8 3 7 5 1.70 36 6 b 4 

### 0.1 6 0.400 0 9 6 8 8 1.48 37 9 0.1 8 0.424 3 7 6 6 9 1.80 36 6 0.1 7 0.412 3 8 4 7 6 1.70 36 5 b 5 

### 0.1 8 0.424 3 9 6 8 8 1.66 37 9 0.1 8 0.424 3 7 5 6 8 1.80 36 4 0.1 6 0.400 0 8 4 7 6 1.60 36 5 b 6 

### 0.1 9 0.435 9 9 6 8 8 1.75 37 8 0.2 0 0.447 2 7 6 6 8 1.98 37 2 0.1 5 0.387 3 8 5 7 7 1.50 36 8 b 7 

### 0.1 5 0.387 3 9 7 9 0 1.39 37 8 0.1 8 0.424 3 7 7 6 8 1.78 37 2 0.1 3 0.360 6 8 2 7 7 1.30 36 4 b 8 

### 0.1 4 0.374 2 9 8 9 1 1.3 2 37 7 0.1 4 0.374 2 7 8 6 8 1.40 36 4 0.1 2 0.346 4 8 4 7 7 1.2 0 ' 36 1

AV G 

### 0.1 7 0.412 5 85. 9 1.57 37 6 0.1 7 0.414 5 72. 5 1.73 36 6 0.1 6 0.394 6 77. 1 1.56 36 4

# ENS . 

# MtCO M EP AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T LEA KCHECKS: SAMPLIN G TRAIN : M5 / Particulate BAROMETRI C PRESSURE : INITIAL VAC . In . CF M
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### J



# Metal s Data

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 006

0 (Metals

) Samplin g Parameter

s Ru n No . Ru n 

### 1 Ru n 2 

### Ru n 3
AVG S Dat e 10-May-06 10-May-0 6 11-May-06 AVG S StartTim e Unit s 10:0 8 15:0 0 11:2 5 AVG S Sto p Tim e 12:5 1 17:1 6 13:3 9 Nozzl e Diamete r inche s 0.40 8 0.43 1 0.43 1 0.42 3 Barometri cPressur e in
. H g 29.1 0 29.0 2 29.0 5 29.06 Ne tSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dc f 81.24 8 83.54 6 76.76 1 80.51 8 Avg
. DG M Temp
. ° F 86. 8 71. 2 78. 0 78. 7 Av g Delt a H i n H 2 0 1.5 7 1.7 6 1.42 1.5 8 Av g Delt a H in
. H g 0.115 6 0.129 2 0.104 1 0.116 3 DG M Calibratio n Facto r 

# - 1.039 0 1.039 0 1.039 0 1.039 0 Ga s Sample Volum e dsc f 79.598 84.05 6 76.26

9 79.97

4 Tota l Wate rCollecte d m L 1271. 1 1380. 4 1300. 2 1317. 2 Volum e ofWate rVapo r sc f 59.93 2 65.08 6 61.30 4 62.10 8 Moistur e (measured ) % v/ v 43. 0 43. 6 44. 6 43. 7 Moistur e ( @ saturation ) % v/ v 102. 8 103. 0 103. 0 102. 9 DryMol e Fraction , 100-% M — 0.570 5 0.563 6 0.554 4 0.562 8 C 0 2at Stac k %dr y 6.4 0 6.8 0 7.0 0 6.7 3 0 2a t Stac k %dr y 12.4 0 9.4 0 10.0 0 10.6 0 C O + N 2 %dr y 81.2 0 83.8 0 83.0 0 82.6 7 DryMolecula rWeigh t Ib/lb-mol e 29.5 2 29.4 6 29.5 2 29.5 0 We tMolecula rWeigh t Ib/lb-mol e 24.5 7 24.46 24.3 9 24.4 7 Exces s Ai rat Stac k % 137. 2 73. 9 83. 9 98. 3 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 0 0.2 2 0.2 1 0.0 7 0.1 7 Stac k Pressur e in
. H g 29.1 2 29.0 4 29.0 6 29.0 7 Avg
. Stac k

Temp
. ° F 381. 2 371. 1 371. 4 374.6 Avg
. Sqroo

t ofDelt a P — 0.412 8 0.423 5 0.384 3 0.406 9 SD E Averag e — 11.97 2 12.20 9 11.08 2 11.75 4 Pito tCoefficien t — 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,92 9 1,97 4 1,79 4 1,89 9 Stac k Flowrat e we tacf m 16,00 1 16,37 7 14,88 3 15,75 3 Stac k Flowrat e we tscf m 9,77 4 10,09 7 9,17 8 9,68 3 Stac k Flowrate dscf m 5,57 6 5,691 5,08 8 5,451 Isokinetic s % 10 9 10

1 10

2 10

4 Mete rBo xNo
. — 8018 4 8018 4 8018 4 - - Delt a H @ i n H 2 0 1.881 0 1.881 0 1.881 0 

## - Fiel d Q AYq c — 1.034 0 1.050 0 1.031 3 1.03 8 [Deviation ] Pre- Y % 0.48 % 1.06 % 0.74 % 0.8 %

### Method 006 0 (Metals

) Samplin g Parameter

s P T a 1

b 1

AV G 

### Run l AVGSMETAL S Delt a P SQR T

Delt a P 0.1 5 0.387 3 0.2 0 0.447 2 0.2 0 0.2 1 0.447 2 0.458 3 0.2 1 0.458 3 0.1 8 0.424 3 0.1 5 0.387 3 0.1 1 0.1 4 0.1 7 0.2 0 0.1 8 0.1 8 0.2 0 0.1 5 0.1 2 0.1 7 0.331 7 0.374 2 0.412 3 0.447 2 0.424 3 0.424 3 0.447 2 0.387 3 0.346 4 0.412 8 DG M

I N 7 3 7 8 8 1 8 4 8 8 8 9 9 0 9 1 8 8 9 3 9 4 95 95 9 6 9 6 9 7 86. 8 DG M

OU T 7 2 7 4 75 7 7 8 3 8 4 8 5 8 5 8 6 8 7 8 8 8 9 9 0 9 1 9 1 9 2 Delt a H

1.3 8 1.8 0 1.8 0 1.9 2 1.9 2 1.6 5 1.4 0 1.0 0 1.3 0 1.5 6 1.8 0 1.6 5 1.6 5 1.8 0 1.4 0 1.1 2 1.5 7 STAC K TEM P 36 6 37 9 38 1 38 5 38 2 38 3 38 2 38 1 36 7 38 5 38 6 38 6 38 6 38 5 38 3 38 2 38 1 

### Run2 AVGS--METAL S Ru n3 AVG S —MET A

L S Delt a P SQR T

Delt a P DG M

I N DG M OU T Delt a H | STAC K

TEM P Delt a P SQR T

Delt a P DG M

I N DG M OU T Delt a H STAC K

TEM P 0.1 2 0.346 4 7 9 7 7 1.2 0 35 9 0.1 6 0.400 0 7 1 7 1 1.5 0 36 7 0.2 1 0.458 3 7 6 7 5 2.0 0 37 5 0.1 7 0.412 3 7 5 7 1 1.6 0 37 2 0.2 0 0.447 2 7 4 7 4 1.9 0 37 6 0.1 8 0.424 3 7 7 7 2 1.7 0 37 3 0.2 1 0.458 3 7 2 7 3 2.0 0 37 6 0.1 7 0.412 3 7 9 7 2 1.6 0 37 3 0.2 1 0.458 3 7 2 7 1 2.0 0 37 3 0.1 6 0.400 0 8 0 7 4 1.5 0 37 4 0.2 0 0.447 2 7 0 6 8 1.9 0 37 1 0.1 5 0.387 3 8 1 7 5 1.4 5 37 3 0.1 7 0.412 3 7 1 6 8 1.6 0 36 8 0.1 2 0.346 4 8 1 7 6 1.1 5 37 2 0.1 2 0.346 4 7 2 6 8 1.2 0 36 7 0.1 0 0.316 2 8 1 7 6 0.9 5 35 7 0.1 5 0.387 3 6 9 6 8 1.4 5 35 8 0.1 2 0.346 4 7 8 7 7 1.1 5 36 9 0.1 7 0.412 3 7 2 6 8 1.6 0 37 1 0.1 6 0.400 0 8 1 7 7 1.5 5 36 6 0.2 0 0.447 2 7 3 6 9 1.9 0 37 5 0.1 8 0.424 3 8 3 7 8 1.7 0 37 4 0.1 7 0.412 3 7 2 6 8 1.6 0 37 6 0.1 7 0.412 3 8 3 7 8 1.6 0 37 5 0.2 0 0.447 2 7 1 6 7 1.9 0 37 6 0.1 5 0.387 3 8 3 7 9 1.4 5 37 5 0.2 0 0.447 2 7 2 6 8 1.9 0 37 6 0.1 5 0.387 3 8 3 7 9 1.4 5 37 5 0.1 9 0.435 9 7 3 6 8 1.8 0 37 6 0.1 2 0.346 4 8 2 7 9 1.1 5 37 4 0.1 7 0.412 3 7 3 6 8 1.6 0 36 4 0.1 2 0.346 4 8 4 8 0 1.1 5 37 4 0.1 8 0.423 5 71. 2 1.7 6 37 1 0.1 5 0.384 3 78. 0 1.4 2 37 1

# ENS R Multi-Metals Blan kCorrection
FRON T HAL F BAC KHAL F TOTA L
Elemen t Sampl

e f g R dBl

k u g Defaul

t Valu e(a ) 5 % o f Sampl e Correcte

d Fron tHal f l» g Sampl

e " g HdBl k

u g Defaul

t Valu e " g 5%

o f Sampl e M g Correcte d Bac kHal f Corrected

F H+ B H f« g Silve r(Ag ) 0.0

0 0.0

0 13.7

8 0.0 0 0.0

0 0.0

0 1.0

0

_

_ 0.0

0 0.0

0 Aluminu m (Al) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Arseni c(As ) 9.2

6 0.7

6 * 13.7

8 0.4

6 8.5

0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 8.5

0 Bariu m(Ba ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Berylliu m (Be ) 0.1

0 (0.10

) 13.7

8 0.0

1 0.1

0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.1

0 Cadmiu m (Cd ) 0.6

8 0.3

4 * 13.7

8 0.0

3 0.3

4 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.3

4 Cobal t(Co ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Chromiu m (Cr ) 17.7

0 1.0

1 * 13.7

8 0.8

9 16.6

9 0.0

0 0.0

0 1.0

0 

### - 0.0 0 16.6

9 Coppe r(Cu ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 - 0.0 0 0.0

0 Manganes

e (Mn ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Lea d (Pb ) 23.9

0 2.7

0 * 13.7

8 1.2

0 21.2

0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 21.2

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Seleniu m (Se ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Thalliu m(Tl) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Vanadiu m (V) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Zinc(Zn ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 - - 0.0 0 0.0

0
I f FH B i s betwee n 0 t o 13.7 8 u gus e blan kvalu e t o correc t I f FHB > 13.7

8 u gthe nus e th e greate ro f 13.7 8 n g o rth e lesse rvalu e betwee n FH B o r5 % o f FH S .
* - valu e use d fo rblan kcorrectio

n MERCURY : (a ) - base d o na3.5 4 - in . filte

rsiz e I f BH B i s > 0 bu t<= 1 n g the nus e th e BHB valu

e t o correc t I f BH B i s > 1 u gus e th e greate ro f eithe r1 u go r5 % o f B H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t

Mercur y Fractio n Sampl

e e g Fid Bl

k I ' g Defaul

t Valu e 

### n 5

% o f Sampl e

" g Correcte d Amoun tH g H g FRON T HAL F (0.03 ) (0.03

) 6.0

0 (0.00

) (0.03

) BAC KHAL F 97.3 3 0.0

4 * 6.0

0 4.8

7 97.2

9 

# 1 TOTA L H g 97.2 9 CLIEN T : Ony xEnvironmenta

l Service, Inc. PROGRA M : Fixe d Heart h Kil n# 3 1 RU NNO . Run1

I f F B i s > 0 bu t<= 6 u gthe nus e th e FB valu

e t o correc t If F B i s > 6 u gus e th e greate ro f eithe r6 n g o r5 % o f F H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t * Indicate

s valu e use d fo rblan kcorrectio

n

# ENS R AECO M Multi-Metals Blan kCorrection

FRON T HAL F BAC KHAL F TOTA L
Elemen t Sampl

e u g Fid Bl

k u g Defaul

t Valu e(a ) u g 5

% o f Sampl e u g Correcte d Fron tHal f u g Sampl

e u g Fid Bl

k u g Defaul

t Valu e u g 5%

o f Sampl e u g Correcte d Bac kHal f u g Corrected

F H+ B H u g Silve r(Ag ) 0.0

0 0.0

0 13.7

8 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Aluminu m (Al) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Arseni c(As ) 249.0

0 0.7

6 * 13.7

8 12.4

5 248.2

4 0.0

0 0.0

0 1.0

0 

### - 0.0 0 248.2

4 Bariu m(Ba ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Berylliu m (Be ) 0.1

0 (0.10

) 13.7

8 0.0

1 0.1

0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.1

0 Cadmiu m (Cd ) 1.3

8 0.3

4 * 13.7

8 0.0

7 1.0

4 0.0

0 0.0

0 1.0

0 

### - 0.0 0 1.0

4 Cobal t(Co ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Chromiu m (Cr ) 29.0

0 1.0

1 * 13.7

8 1.4

5 27.9

9 0.0

0 0.0

0 1.0

0 0.0 0 27.9

9 Coppe r(Cu ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Manganes

e (Mn ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Lea d (Pb ) 22.3

0 2.7

0 * 13.7

8 1.1

2 19.6

0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 19.6

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Seleniu m (Se ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 - - 0.0 0 0.0

0 Thalliu m(Tl ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Vanadiu m (V) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Zin c(Zn ) 0.0

0 0.0

0 13.7

8 - - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0
I f FH B i s betwee n 0 t o 13.7 8 u gus e blan kvalu e t o correc t I f FH B > 13.7 8 p gthe nus e th e greate ro f 13.7 8 u go rth e lesse rvalu e betwee n FH B o r5 % o f FH S .
* - valu e use d fo rblan kcorrectio

n MERCURY : (a ) - base d o na3.5 4 - in . filtersiz

e I f BHB i s > 0 bu t<= 1 u gthe nus e th e BHB valu

e t o correc t I f BH B i s > 1 u gus e th e greate ro f eithe r1 n g o r5% o f B H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t

Mercur y Fractio n Sampl

e u g Fid Blk

u g Defaul

t Valu e u g 5

% o f Sampl e u g Correcte

d Amoun tH g u g FRON T HAL F 0.1 0 (0.03

) 6.0

0 0.0

1 0.1

0 BAC KHAL F 121.2 3 0.0

4 * 6.0

0 6.0

6 121.1

9 

# I TOTA L H g 121.2 9 CLIEN T : Ony xEnvironmenta

l Service, Inc

. PROGRA M : Fixed Heart h Kil n# 3 RU NNO . Run2

I f F B i s > 0 bu t<= 6 n g the nus e th e F B valu e t o correc t I f F B i s > 6 u gus e th e greate ro f eithe r6 n g o r5 % o f F H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t * Indicate

s valu e use d fo rblan kcorrectio

n

# ENS R Multi-Metals Blan kCorrection
FRON T HAL F BAC KHAL F TOTA L Corrected F H+ B H
" g Elemen t Sampl

e H g Fid Blk

H g Defaul

t Valu e(a ) u g 5

% o f Sampl e u g Correcte d Fron tHal f H g Sampl

e H g FidBlk

H g Defaul

t Valu e H g 5

% o f Sampl e M g Correcte

d Bac kHal f H g TOTA L

Corrected F H+ B H
" g Silve r(Ag ) 0.0

0 0.0

0 13.7

8 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Aluminu m (Ai ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 . 0.0 0 0.0

0 Arseni c(As ) 946.0

0 0.7

6 * 13.7

8 47.3

0 945.2

4 0.0

0 0.0

0 1.0

0 

### - 0.0 0 945.2

4 Bariu m(Ba ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Berylliu m (Be ) 0.1

0 (0.10

) 13.7

8 0.0

1 0.1

0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.1

0 Cadmiu m (Cd ) 2.7

6 0.3

4 * 13.7

8 0.1

4 2.4

2 0.0

0 0.0

0 1.0

0 

## - 0.0 0 2.4

2 Cobal t(Co ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Chromiu m (Cr ) 55.8

0 1.0

1 * 13.7

8 2.7

9 54.7

9 0.0

0 0.0

0 1.0

0 

## - 0.0 0 54.7

9 Coppe r(Cu ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Manganes

e (Mn ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Lea d (Pb ) 40.6

0 2.7

0 * 13.7

8 2.0

3 37.9

0 0.0

0 0.0

0 ' 1.0

0 

### - 0.0 0 37.9

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 .0.0

0 1.0

0 

### - 0.0 0 0.0

0 Seleniu m (Se ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Thalliu m(Tl) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Vanadiu m (V ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Zin c(Zn ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0


### - 0.0 0 0.0

0
I f FH B i s betwee n 0 t o 13.7 8 p gus e blan kvalu e t o correc t I f FH B > 13.7 8 p gthe nus e th e greate ro f 13.7 8 p go rth e lesse rvalu e betwee n FH B o r5 % o f FH S .
* - valu e use d fo rblan kcorrectio

n MERCURY : (a ) - base d o na3.5 4 - in . filtersiz

e I f BHB i s > 0 bu t<= 1 u gthe nus e th e BHB valu

e t o correc t I f BHB i s > 1 p gus e th e greate ro f eithe r1 u go r5 % o f B H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t

Mercur y Fractio n Sampl

e H g Fi

d Blk H g Defaul

t Valu e H g 5%

o f Sampl e H g Correcte

d Amoun tH g H g FRON T HAL F 0.2 7 (0.03

) 6.0

0 0.0

1 0.2

7 BAC KHAL F 89.1 2 0.0

4 * 6.0

0 4.4

6 89.0

8 

# 1 TOTA L H g 89.3 5 CLIENT :

PROGRAM : RU N NO . Ony xEnvironmenta

l Service , Inc. Fixe d Heart h Kil n# 3 Run3

I f F B i s > 0 bu t<= 6 p gthe nus e th e F B valu e t o correc t If F B i s > 6 p gus e th e greate ro f eithe r6 p go r5 % o f FH ( ) No tDetecte d / Reportabl

e Detectio

nLimi t * Indicate

s valu e use d fo rblan kcorrectio

n

# ENS , ACCO M EP AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T
SAMPLIN G TRAIN : M29/Metal s PLANT : ONY XEnvironmenta l DATE : TES TLOCATION : Uni t # 3 Fixe d Heart h RU N NUMBER : / Stac k Diamete r- Inches : 39 " OPERATOR : STAR TTIME : STO P TIME : BAROMETRI C PRESSURE : STATI C PRESSUR E (+/-) : Probe/Pitot Number : Pito t Coefficient : Filte rBoxNo. : Mete rBoxNumber : Orific e Coefficien t (Y) : Delta H@ : Nozzl e Size : XA D Thermocoupl e ID : Impinge rOutle

t ID : 

### tor-*-? INITIAL VAC . MI D VAC . FINA L VAC . LEA KCHECKS : in . CF M CF M CF M in . in . 0.8 4 /•(Pi? 

# 7 W 6-4 08 INIT . PITOT
" FINA L PITOT ORSA TInitial : O^SA TFinal FILTE R DAT A IMPINGE R VOL' S Rins e ORSA

TDAT A SdNiTliilSi&E I Volumes 0 

### n\ 10 0 10 0 0 ( S 10 0 10 0 10 0 I2K.I . 

### ^.siypA
. FO R MOISTURI E CALC : Fina l Vol . 15 1 NE TGAIN : < / ml . SAMPL E POIM T CLOC K

TIM E VELOCITY ;

HEA O DedaRKw

c . ORIFIC E METE R VOL . ,.D<*aH.lnv(

C ; OA S METE R '

VOLUM E ff TEMPERATUR E READINGS . ° F PUM P VACUU M

. . In.Ha. . . COMMENT S SAMPL E POIM T CLOC K

TIM E VELOCITY ;

HEA O DedaRKw

c . ORIFIC E METE R VOL . ,.D<*aH.lnv(

C ; OA S METE R '

VOLUM E ff STAC K PRO& E FILTE R BO X ,, t IMPIKIOE

A ; I XA D Tra

p

. , . . . . GA S METE R •1 PUM P VACUU M

. . In.Ha. . . COMMENT S SAMPL E POIM T CLOC K

TIM E VELOCITY ;

HEA O DedaRKw

c . ORIFIC E METE R VOL . ,.D<*aH.lnv(

C ; OA S METE R '

VOLUM E ff STAC K PRO& E FILTE R BO X ,, t IMPIKIOE

A ; I XA D Tra

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### Ru n 1 

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### AVG S Dat e 19-Jun-0 6 15:1 2 20-Jun-0 6

10:0 6 21-Jun-0 6

10:06 

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10:0 6 21-Jun-0 6

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### AVG S Sto p Tim e 17:2 9 12:2 9 12:4 4 Nozzl e Diamete r inche s 0.43 1 0.43 1 0.43 1 0.43 1 Barometri cPressur e 

## in:.H.a 29.5 5 29.5 5 29.5 0 29.5 3 Ne tSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dcf 78.24 4 82.90 2 81.74 5 80.96 4 Avg
. DG M Temp
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. 0.096 4 0.104 9 0.103 4 0.101 6 DG M Calibratio n Facto r 1.007 0 1.007 0 1.007 0 1.007 0 Ga s Sampl e Volum e dsc f 72.247 76.482 75.57 3 74.76 8 Tota l Wate rCollecte d m L 1341. 0 1487. 9 1340. 1 1389. 7 Volum e o fWate rVapo r sc f 63.22 8 70.15 4 63.18 6 65.52 3 Moistur e (measured ) I % W v 46. 7 47. 8 I 45. 5 46. 7 I Moistur e ( @ saturation ) % v/ v 101. 3 101. 3 101. 5 101. 3 DryMol e Fraction , 100-% M 

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Temp
. ° F 386. 2 387. 9 385. 9 386. 6 Avg
. Sqroo to fDelt a P 

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## - 10.76 5 11.42 0 11.42 9 11.20 5 Pito t Coefficien t 

## - 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,73 6 1,84 7 1,84 0 1,80 8 Stac k Flowrat e we tacf m 14,39 9 15,32 6 15,26 2 14,99 6 Stac k Flowrat e we tscf m 8,87 0 9,42 2 9,39 0 9,22 8 Stac k Flowrat e dscf m 4,730 4 ,91 5 5,11 4 4,92 0 Isokinetic s % 10 4 10

6 10

1 10

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t DataUun e 2006\2n d Retest\[PM.x!s]DAT

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### Metho d 5 Samplin g Parameter s
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T Delt a P DGM

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T Delt a P DGM

IN DGM OU T Delt a H STACK TEM P Delt

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I N DG M OU T Delt a H STACK TEM P
a 1 0.0 7 0.264 6 10 4 10 2 0.6 6 38 2 0.1 0 0.316 2 10 2 9 9 0.9 2 38 2 0.1 7 0.412 3 8 9 8 7 1.5 3 37 9 a 2 0.1 2 0.346 4 10 4 10 2 1.1 3 38 7 0.1 0 0.316 2 10 6 10 2 0.9 2 38 3 0.1 5 0.387 3 9 2 8 9 1.3 5 38 0 a 3 0.1 9 0.435 9 10 9 10 4 1.7 9 38 6 0.1 6 0.400 0 10 8 10 3 1.4 7 38 6 0.1 4 0.374 2 9 5 9 0 1.2 6 37 9 a 4 0.1 9 0.435 9 11 1 10 4 1.7 9 38 7 0.1 8 0.424 3 11 1 10 4 1.6 6 38 9 0.1 4 0.374 2 10 8 10 6 1.2 6 38 4 a 5 0.1 5 0.387 3 11 4 10 6 1.4 1 38 8 0.1 4 0.374 2 11 2 10 5 1.2 9 38 7 0.1 8 0.424 3 11 2 10 6 1.6 2 38 8 a 6 0.1 6 0,400 0 11 5 10 7 1.5 0 38 8 0.1 5 0.387 3 11 2 10 6 1.3 8 38 5 0.1 8 0.424 3 11 4 10 7 1.6 2 38 8
a 7 0.1 2 0.346 4 11 5 10 6 1.1 3 38 3 0.1 8 0.424 3 11 5 10 7 1.6 6 38 5 0.1 2 0.346 4 11 6 10 8 1.0 8 38 7
a 8 0.1 5 0.387 3 11 6 10 4 1.4 1 38 2 0.1 5 0.387 3 11 6 10 9 1.3 8 38 8 0.1 0 0.316 2 11 7 10 9 0.9 0 38 1 b 1 0.0 7 0.264 6 11 3 11 1 0.6 6 38 2 0.1 8 0.424 3 11 0 11 0 1.6 6 38 6 0.2 2 0.469 0 11 2 11 1 1.9 8 38 4 b 2 0.1 4 0.374 2 11 3 11 1 1.3 2 38 3 0.1 8 0.424 3 11 4 11 1 1.6 6 38 8 0.1 7 0.412 3 11 2 11 1 1.5 3 38 8 b 3 0.1 1 0.331 7 11 5 11 1 1.0 3 38 9 0.1 8 0.424 3 11 6 11 2 1.6 6 39 0 0.1 8 0.424 3 11 6 11 2 1.6 2 38 9 b 4 0.1 3 0.360 6 11 6 11 1 1.2 2 39 1 0.1 6 0.400 0 11 8 11 2 1.4 7 39 1 0.1 9 0.435 9 11 8 11 3 1.7 1 39 0 b 5 0.1 4 0.374 2 11 6 11 2 1.3 2 39 0 0.1 8 0.424 3 11 9 11 3 1.6 6 39 2 0.1 8 0.424 3 12 0 11 4 1.6 2 39 0 b 6 0.1 5 0.387 3 11 6 11 2 1.4 1 38 7 0.1 6 0.400 0 12 1 11 4 1.4 7 39 5 0.1 6 0.400 0 12 0 11 5 1.4 4 39 2 b 7 0.1 7 0.412 3 11 7 11 2 1.6 0 38 8 0.1 4 0.374 2 12 1 11 4 1.2 9 39 2 0.1 2 0.346 4 12 0 11 5 1.0 8 39 1 b 8 0.1 7 0.412 3 11 7 11 2 1.6 0 38 6 0.1 4 0.374 2 12 2 11 5 1.2 9 38 7 0.1 0 0.316 2 12 0 11 5 0.9 0 38 4

A V G 0.1 4 0.370 1 110. 6 1.3 1 38 6 0.1 6 0.392 2 111. 2 1.4 3 38 8 0.1 6 0.393 0 109. 0 1.4 1 38 6

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## EPA ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T :::iMp:iKGfift.voL j s;::- : Orsat Samplin g Trai n /AJ T/ /" \ 5 Barometri c Pressur e fc 5^ LEA KCHECK S I n "Hg ::INITI:-:: - 

### ym wo:-:-:-:-:

•RINS E :co 2 •::o2-: - Hu n Numbe rjV i Stati c Pressur e (+/- ) - . IL INITIA L VAC . | L in . CF M •e>cg i 6 

# '7 - M Clien t f W v Probe/Pito t Numbe rA S MI D VAC . In . CF M ^ 0 3&8 

# '7 - M Facilit yLocatio n ^ftU^C fi I L Pilo t Coefficien

t FINA L VAC . i , in . CF M 

# 1- 1 Sourc e FilterBo xNo . r

- J 

### +

/• / VI" 0 1 

# 1- 1 Dat e MeierBo xNo . INIT . PITO TV V FINA L P1T01 

# 1. 1 Operatu r T .(.ft'Mflt J Orific e Coefficien

t (Y ) 1 .DOI FILTE R DAT A 

# 1. 1 Stac k Ula.-lu . Delt a H @ 1/93? . •XNOMBER: - X-MAREX- : Star t Tim e 

### iru, Nozzl e Size/No . ! Ti T Sto p Tim e XA D Thermocoupl e ID : — /3./3L vX-X-SmCABE&XvX . Fina l Purg e Rat e Im p Outle t T C ID : L X -1 2 Fina l ri l SAMPL E CLOC K VELOCIT Y ORIFIC E «A S Mi-TE R TEMPERATUR E READINGS . ° F fOIN T JtM b IWAD Mff l LR.VQ L VOLUM E ORGANf C VACUU M COMMENTS Belt*! 1 , lo w

c Pe|tmi,|n* r r e STAC K PK.OB E MOGUL S iM,pi(sfc5Br t iil|iii3(|i)Fi!i! ; M O 

# n I.S ^ — 1 a 1.S " -IC " 1-3 5 

### _ Ho 

# \ 3 K .I V no. a 31 T 

# - - \ M 

### ib5. I a w 1< ? 10 6 1 s If t U D 3 S S — l i |i | P IcO^ , 1

n . c . w U 3 115. 1 JR S 211 — 

# c < / c i 1 7 • I X L O S no 

### s 3 8 7 

### 1H0
— 

# 5 7 U 6 

# loi ? / % S3. ? 

### 'iO 3 8 1 — 

# i n 1* ? )

— 6 I C O 

### >21 Lif t M . U — h ( 1 

# •I

T I . S i 

### l4$, C — tu 2 

### 3 7S ' I.C 2 

### ZHO
— 1. 6 (12 

### a

s a c .1 ? M l .'•51 0 

# J »v t 33f l — 11 3 

# a S A O - i p U i 3 ? 0 

### 2H)

— - K M 3 4 

# <n c •i t m a * m a m S t \t< 2 

# 7 » o r 

# .1 2 222
. < ? 39 1 — 

# S 3 US 

# $ M2. 5 •1 0 .9 0 

### ICO — S 3 12 0 

### US 

# 1 \70 —

— '

— •



## i 11



# Metal s Data

)

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato rUni t 3 Metho d 006

0 (Metals

) Samplin g Parameter s Ru n No
. 

### Ru n 1 Ru n 2 

### Ru n 3
AVG S Dat e 19-Jun-06 20-Jun-06 21-Jun-06 AVG S StartTim e Units 15:1 2 10:0 6 10:0 6 AVG S Sto p Tim e 17:2 9 12:2 9 12:4 4 Nozzl e Diamete r inche s 0.43 1 0.43 1 0.43 1 0.43 1 Barometri cPressur e in
. H g 29.5 5 29.5 5 29.5 0 29.5 3 Ne tSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dcf 78.24 4 82.90 2 81.74 5 80.96 4 Avg
. DG M Temp
. ° F 110. 6 111. 2 109. 0 110. 3 Av g Delt a H i n H 2 0 1.3 1 1.4 3 1.4 1 1.3 8 Av g Delt a H in
. H g 0.096 4 0.104 9 0.103 4 0.101 6 DG M Calibratio n Facto r — 1.007 0 1.007 0 1.007 0 1.007 0 Ga s Sampl e Volum e dscf 72.24 7 76.48

2 75.57

3 74.768 Tota l Wate rCollecte d m L 1341. 0 1487. 9 1340. 1 1389. 7 Volum e ofWate rVapo r sc f 63.22 8 70.15 4 63.18 6 65.52 3 Moistur e (measured ) % V/ V 46. 7 47. 8 45. 5 46. 7 Moistur e ( @ saturation ) % v/ v 101. 3 101. 3 101. 5 101. 3 Dr yMol e Fraction , 100-% M — 0.533 3 0.521 6 0.544 6 0.533 2 C O aa t Stac k %dr y 7.4 0 7.6 0 7.4 0 7.4 7 0 2a t Stac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C O + N 2 %dr y 82.6 0 84.2 0 83.0 0 83.2 7 DryMolecula rWeigh t Ib/lb-mole 29.5 8 29.5 4 29.5 7 29.5 7 We tMolecula rWeigh t Ib/lb-mole 24.1 8 24.0 2 24.3 0 24.1 7 Exces s Ai ra t Stac k % 84. 7 58. 5 78. 0 73. 7 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 0 -0.1 5 -0.1 5 -0.1 3 -0.1 4 Stac k Pressur e in
. H g 29.5 4 29.5 4 29.4 9 29.5 2 Avg
. Stac k

Temp
. ° F 386. 2 387. 9 385. 9 386. 6 Avg
. Sqroo tofDelt a P — 0.370 1 0.392 2 0.393 0 0.385 1 SD E Averag e — 10.76 5 11.42 0 11.42 9 11.20 5 Pito tCoefficien t — 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,73 6 1,84 7 1,84 0 1,80 8 Stac k Flowrat e wetacf m 14,39 9 15,32 6 15,26 2 14,99 6 Stac k Flowrat e wetscf m 8,87 0 9,42 2 9,39 0 9,22 8 Stac k Flowrate dscf m 4,730 4,91 5 5 ,11 4 4,920 Isokinetic s % 10 4 10 6 10

1 10 4 Mete rBo xNo
. ~ 8075 4 8075 4 8075 4 — Delt a H @ i n H 2 0 1.832 0 1.832 0 1.832 0


## - Fiel d Q AYq c — 1.006 6 0.991 8 0.997 4 0.99 9 [Deviation ] Pre- Y % 0.04 % 1.51 % 0.95 % 0.8 %

### Method 006 0 (Metals

) Samplin g Parameter

s P T 

### Run l AVGS--METAL S Ru n2 AVGS--METAL S Ru n3 AVGS--METAL S P T Delt a P SQR T

Delt a P DG M

I N DG M OU T Delt a H STAC K

TEM P Delt a P SQR T

Delt a P DG M

I N DG M OU T Delt a H |STAC K

TEM P Delt a P SQR T

Delt a P DG M



### I N DG M OU T Delt a H STAC K

TEM P a 1 0.0 7 0.264 6 ^ 10 4 10 2 0.6 6 38 2 0.1 0 0.316 2 10 2 9 9 0.9 2 38 2 0.1 7 0.412 3 8 9 8 7 1.5 3 37 9 2 0.1 2 0.346 4 10 4 10 2 1.1 3 38 7 0.1 0 0.316 2 10 6 10 2 0.9 2 38 3 0.1 5 0.387 3 9 2 8 9 1.3 5 38 0 3 0.1 9 0.435 9 10 9 10 4 1.7 9 38 6 0.1 6 0.400 0 10 8 10 3 1.4 7 38 6 0.1 4 0.374 2 95 9 0 1.2 6 37 9 4 0.1 9 0.435 9 11 1 10 4 1.7 9 38 7 0.1 8 0.424 3 11 1 10 4 1.6 6 38 9 0.1 4 0.374 2 10 8 10 6 1.2 6 38 4 5 0.1 5 0.387 3 11 4 10 6 1.4 1 38 8 0.1 4 0.374 2 11 2 10 5 1.2 9 38 7 0.1 8 0.424 3 11 2 10 6 1.6 2 38 8 6 0.1 6 0.400 0 11 5 10 7 1.5 0 38 8 0.1 5 0.387 3 11 2 10 6 1.3 8 38 5 0.1 8 0.424 3 11 4 10 7 1.62 38 8 7 0.1 2 0.346 4 11 5 10 6 1.1 3 38 3 0.1 8 0.424 3 11 5 10 7 1.6 6 38 5 0.1 2 0.346 4 11 6 10 8 1.0 8 38 7 8 0.1 5 0.387 3 11 6 10 4 1.4 1 38 2 0.1 5 0.387 3 11 6 10 9 1.3 8 38 8 0.1 0 0.316 2 11 7 10 9 0.9 0 38 1 b 1 0.0 7 0.264 6 11 3 11 1 0.6 6 38 2 0.1 8 0.424 3 11 0 11 0 1.6 6 38 6 0.2 2 0.469 0 11 2 11 1 1.9 8 38 4 2 0.1 4 0.374 2 11 3 11 1 1.32 38 3 0.1 8 0.424 3 11 4 11 1 1.6 6 38 8 0.1 7 0.412 3 11 2 11 1 1.5 3 38 8 3 0.1 1 0.3317 11 5 11 1 1.0 3 38 9 0.1 8 0.424 3 11 6 11 2 1.6 6 39 0 0.1 8 0.424 3 11 6 11 2 1.6 2 38 9 4 0.1 3 0.360 6 11 6 11 1 1.2 2 39 1 0.1 6 0.400 0 11 8 11 2 1.4 7 39 1 0.1 9 0.435 9 11 8 11 3 1.7 1 39 0 5 0.1 4 0.374 2 11 6 11 2 1.32 39 0 0.1 8 0.424 3 11 9 11 3 1.6 6 39 2 0.1 8 0.424 3 12 0 11 4 1.6 2 39 0 6 0.1 5 0.387 3 11 6 11 2 1.4 1 38 7 0.1 6 0.400 0 12 1 11 4 1.4 7 39 5 0.1 6 0.400 0 12 0 11 5 1.44 39 2 7 0.1 7 0.412 3 11 7 11 2 1.6 0 38 8 0.1 4 0.374 2 12 1 11 4 1.2 9 39 2 0.1 2 0.346 4 12 0 11 5 1.0 8 39 1 8 0.1 7 0.412 3 11 7 11 2 1.6 0 38 6 0.1 4 0.374 2 12 2 11 5 1.2 9 38 7 0.1 0 0.316 2 12 0 11 5 0.9 0 38 4 

### AV G 0.1 4 0.370 1 110. 6 | 1.3 1 38 6 0.1 6 0.392 2 111. 2 1.4 3 38 8 0.1 6 0.393 0 109. 0 1.4 1 38 6

# ENS R Multi-Metals Blan kCorrection
FRON T HAL F BAC KHAL F TOTA L
Elemen t Sampl

e H g Fid Blk

H g Defaul

t Valu e(a ) H g 5

% o f Sampl e H g Correcte d Fron tHal f H g Sampl

e H g Fid Bl

k H g Defaul

t Valu e H g 5%

o f Sampl e H g Correcte d Bac kHal f H g Corrected

F H+ B H M g Silve r(Ag ) 0.0

0 0.0

0 13.7

8 0.0 0 0.0

0 0.0

0 1.0

0 _ 0.0 0 0.0

0 Aluminu m (AI ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Arseni c(As ) 5.8

1 0.6

1 * 13.7

8 0.2

9 5.2

0 0.3

3 0.0

0 1.0

0 0.0

2 0.3

3 5.5

3 Bariu m(Ba ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Berylliu m (Be ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Cadmiu m (Cd ) 0.0

0 0.0

0 13.7

8 

## - . 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Cobal t(Co ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Chromiu m (Cr ) 9.6

4 0.7

9 * 13.7

8 0.4

8 8.8

5 1.0

6 0.0

0 1.0

0 0.0

5 1.0

6 9.91 Coppe r(Cu ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Manganes

e (Mn ) 0.0

0 0.0

0 13.7

8 - - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Lea d (Pb ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Seleniu m (Se ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Thalliu m(TJ ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Vanadiu m (V) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

## - 0.0 0 0.0

0 Zin c(Zn ) 0.0

0 0.0

0 13.7

8 - - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0
I f FH B i s betwee n 0 t o 13.7 8 n g us e blan kvalu e t o correc t I f FH B > 13.7 8 n gthe nus e th e greate ro f 13.7 8 u go rth e lesse rvalu e betwee n FH B o r5 % o f FH S .
* - valu e use d fo rblan kcorrectio

n MERCURY : (a ) - base d o na3.5 4 - in . filte

rsiz e I f BH B i s > 0 bu t<= 1 n gthe nus e th e BH B valu e t o correc t I f BH B i s > 1 [i gus e th e greate ro f eithe r1 (t g o r5 % o f B H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t

Mercur y Fractio n FRON T HAL F BAC KHAL F Sampl e H g 0.0 0 0.0 0 Fi

d Bl k H g 0.0 0 0.0 0 Defaul

t Valu e H g 6.0 0 6.0 0 5

% o f Sampl e H g 0.0 0 0.0 0 Correcte

d Amoun tH g H g 0.0 0 0.0 0 CLIEN T : VeoliaE S Technica l Solution

s PROGRA M : Fixe d Heart h Incinerato

rUni t3 RU N NO . Run1

TOTA L H g0.0 0 I f F B i s > 0 bu t<= 6 u g the nus e th e F B valu e t o correc t I f F B i s > 6 n gus e th e greate ro f eithe r6 n go r5% o f F H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t * Indicate

s valu e use d fo rblan kcorrectio

n

# ENS R Multi-Metals Blan kCorrection
FRON T HAL F BAC KHAL F TOTA L
Elemen t Sampl

e H g Fid Blk

M g Defaul

t Valu e(a ) H g 5

% o f Sampl e M g Correcte

d Fron tHal f H g Sampl

e H g Fid Blk

H S Defaul

t Valu e H g 5

% o f Sampl e H g Correcte d Bac kHal f H g Corrected

F H+ B H M g Silve r(Ag ) 0.0

0 0.0

0 13.7

8 0.0 0 0.0

0 0.0

0 1.0

0 

### „ 0.0 0 0.0

0 Aluminu m (Al) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Arseni c(As ) 4.3

0 0.6

1 * 13.7

8 0.2

2 3.6

9 0.0

0 0.0

0 LO

O 

### - 0.0 0 3.6

9 Bariu m(Ba ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Berylliu m (Be ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

9 0.0

0 1.0

0 0.0

0 0.0

9 0.0

9 Cadmiu m (Cd ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Cobal t(Co ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 LO

O 0.0 0 0.0

0 Chromiu m (Cr ) 3.9

8 0.7

9 * 13.7

8 0.2

0 3.19 0.6 6 0.0

0 LO

O 0.0

3 0.6

6 3.8

5 Coppe r(Cu ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Manganes

e (Mn ) O.O

O 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 LO

O 

### - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Lea d (Pb ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Seleniu m (Se ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Thalliu m(Tl) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Vanadiu m (V ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Zin c(Zn ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0
I f FH B i s betwee n 0 t o 13.7 8 u gus e blan kvalu e t o correc t I f FH B > 13.7 8 n gthe nus e th e greate ro f 13.7 8 n go rth e lesse rvalu e betwee n FH B o r5% o f FH S . * - valu e use d fo rblan kcorrectio

n MERCURY : (a ) - base d o na3.5 4 - in . filtersiz

e I f BHB i s > 0 bu t<= 1 n gthe nus e th e BHB valu

e t o correc t I f BHB i s > 1 n gus e th e greate ro f eithe r1 n go r5 % o f B H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t

Mercur y Fractio n Sampl

e H g Fid Bl

k H g Defaul

t Valu e H g 5%

o f Sampl e H g Correcte

d Amoun tH g H g FRON T HAL F 0.0 0 0.0

0 6.0

0 0.0

0 0.0

0 BAC KHAL F 0.0 0 0.0

0 6.0

0 0.0

0 0.0

0 

# I I TOTA L H g 0.0 0 CLIEN T : VeoliaE S Technica l Solution

s PROGRA M : Fixe d Heart h Incinerato

rUni t3 RU N NO . Run2

I f F B i s > 0 bu t<= 6 n g the nus e Ih e F B valu e t o correc t I f F B i s > 6 ng us e th e greate ro f eithe r6 n g o r5% o f F H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t * Indicate

s valu e use d fo rblan kcorrectio

n

# ENS R Multi-Metals Blan kCorrection
FRON T HAL F BAC KHAL F TOTA L
Elemen t Sampl

e H g Fi

d Blk H g Defaul

t Valu e(a ) H g 5%

o f Sampl e H g Correcte d Fron tHal f H g Sampl

e H g Fid Bl

k H g Defaul

t Valu e H g 5%

o f Sampl e H S Conrecte d Bac kHal f H g Corrected

F H+ B H H g Silve r(Ag ) 0.0

0 0.0

0 13.7

8 0.0 0 0.0

0 0.0

0 1.0

0 „ 0.0 0 0.0

0 Aluminu m (Al) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Arseni c(As ) 5.6

0 0.6

1 * 13.7

8 0.2

8 4.9

9 0.2

1 0.0

0 LO

O 0.0

1 0.2

1 5.2

0 Bariu m(Ba ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 LO

O 

### - 0.0 0 0.0

0 Berylliu m (Be ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Cadmiu m (Cd ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Cobal t(Co ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 - 0.0 0 0.0

0 Chromiu m (Cr ) 11.1

0 0.7

9 * 13.7

8 0.5

6 10.3

1 0.8

4 0.0

0 1.0

0 0.0

4 0.8

4 11.1

5 Coppe r(Cu ) 0.0

0 0.0

0 13.7

8 - - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Manganes

e (Mn ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 LO

O 

### - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Lea d (Pb ) 0.0

0 0.0

0 13.7

8 

## - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Seleniu m (Se ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Thalliu m (Tl ) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0 Vanadiu m (V) 0.0

0 0.0

0 13.7

8 

### - 0.0 0 0.0

0 0.0

0 LO

O 

### - 0.0 0 0.0

0 Zinc(Zn ) 0.0

0 0.0

0 13.7

8 - - 0.0 0 0.0

0 0.0

0 1.0

0 

### - 0.0 0 0.0

0
I f FH B i s betwee n 0 t o 13.7 8 n gus e blan kvalu e t o correc t I f FH B > 13.7 8 u-gthe nus e th e greate ro f 13.7 8 n g o rth e lesse rvalu e betwee n FH B o r5 % o f FH S . * - valu e use d fo rblan kcorrectio

n MERCURY : (a ) - base d o na3.5 4 - in . filte

rsiz e I f BH B i s > 0 bu t<= 1 n gthe nus e th e BHB valu

e t o correc t I f BH B i s > 1 n gus e th e greate ro f eithe r1 n go r5 % o f B H ( ) No tDetecte d / Reportabl

e Detectio

nLimi t

Mercur y Fractio n Sampl

e H g Fid Blk

H g Defaul

t Valu e H g 5

% o f Sampl e H g Correcte

d Amoun tH g H g FRON T HAL F 0.0 0 0.0

0 6.0

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# PCDD/PCD F Data

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r# 3 Metho d 0023 A Samplin g Parameter s Ru n No
. Run l Ru n 2 Ru n 3 AVG S Dat e 19-Jun-0 6 20-Jun-0

6 21-Jun-0

6 AVG S StartTim e Unit s 14:4 0 9:3 0 9:3 0 AVG S Sto p Tim e 17:5 9 13:0 5 11:4 3 Nozzl e Diamete r inche s 0.43 5 0.43 5 0.43 5 0.43 5 Barometri cPressur e in
. H g 29.5 5 29.5 0 29.5 0 29.5 2 Ne tSamplin g Tim e min
. 192. 0 192. 0 192. 0 192. 0 Volum e Metere d dcf 135.21 5 136.33 1 133.04 6 134.86 4 Avg
. DG M Temp
. ° F 109. 3 107. 1 107. 9 108. 1 Av g Delt a H i n H 2 

### 0 1.7 1 1.74 1.6 7 1.7 1 Av g Delt a H in
. H g 0.125 7 0.128 2 0.122 5 0.125 5 DG M Calibratio n Facto r - - 

### 1.032 0 1.032 0 1.032 0 1.032 0 Ga s Sampl e Volum e dsc f 128.36 3 129.71 0 126.37 9 128.15 1 Tota l Wate rCollecte d m L 2171. 7 2509. 0 2250. 4 2310. 4 Volum e o

fWate rVapo r sc f 102.39 6 118.29 9 106.10 6 108.93 4 Moistur e (measured ) , % v/ v 44. 4 47. 7 45. 6 45. 9 Moistur e ( @ saturation ) % v/ v 101. 3 101. 5 101. 5 101. 4 Dr yMol e Fraction , 100-% M - - 

### 0.556 3 0.523 0 0.543 6 0.541 0 C 0 2

### a t Stac k %dr y 7.4 0 7.6 0 7.4 0 7.4 7 0 2

### at Stac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 C O + N 2 

### %dr y 82.6 0 84.2 0 83.0 0 83.2 7 DryMolecula rWeigh t Ib/lb-mole 29.5 8 29.5 4 I 29.5 7 29.5 7 We tMolecula rWeigh t Ib/lb-mole 24.4 4 24.0 4 24.2 9 24.2 6 Exces s Ai rat Stac k % 84. 7 58. 5 78. 0 73. 7 Stac k Diamete r inche s 39. 6 39. 0 39. 0 39. 0 Stac k Are a sq . in
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### O -0.1 3 -0.1 5 -0.1 7 -0.1 5 Stac k Pressur e in
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. Stac k

Temp
. ° F 390. 4 393. 1 385. 0 389. 5 Avg
. Sqroo tofDelt a P ~ 

### 0.411 3 0.416 6 0.406 2 0.411 4 SD E Averag e — 

### 11.99 4 12.16 8 11.80 8 11.99 0 Pito tCoefficien t


# - 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,92 3 1,96 9 1,90 1 1,93 1 Stac k Flowrat e we tacf m 15,95 6 16,33 8 15,77 3 16,02 2 Stac k Flowrat e we tscf m 9,78 1 9,96 6 9,71 3 9,82 0 Stac k Flowrate dscf m 5,44 1 5,21 2 5,28 0 5,31 1 Isokinetic s % 

### 9 9 10

4 10

0 10

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### 8064 5 8064 5 8064 5 — 

### Delt a H @ in
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# - Fiel d Q AYq c ~ 

### 1.04 8 1.05 0 1.05 2 1.05 0 [Deviation ] Pre- Y % 1.6 % 1.7 % 1.9 % 1.7 % S:\_JOB\2006\Onyx\Performanc e TesftTes

t DataVlun

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A Separat

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### Method 0023 A Samplin g Parameter s

P T R U N 1 AVG S - •PCDDs/PCDF s R U N 2 AVG S - - PCDDs/PCDF s R U N 3 AVG S • - PCDDs/PCDF s P T D P SQR T D P D G M

I N D G M

O U T D H STAC K TEM P D P SQR T D P D G M

I N D G M

O U T D H STAC K TEM P D P SQR T D P D G M

I N D G M

O U T D H STAC K TEM P A 1 0,2 2 0.469 0 10 3 10 0 2.2 0 38 9 0.1 4 0.374 2 9 4 9 3 1.4 0 38 7 0.1 4 0.374 2 9 6 9 5 1.4 0 37 0 1 0.2 5 0.500 0 10 5 10 1 2.5 0 38 9 0.1 4 0.374 2 9 5 9 3 1.4 0 38 6 0.1 1 0.331 7 9 7 9 5 1.1 0 38 0 2 0.2 5 0.500 0 11 4 10 3 2.5 0 38 9 0.2 0 0.447 2 9 6 9 4 2.0 0 38 9 0.1 5 0.387 3 9 8 9 6 1.5 0 38 2 2 0.2 1 0.458 3 11 5 10 5 2.1 0 38 9 0.2 0 0.447 2 9 9 9 5 2.0 0 38 8 0.1 6 0.400 0 10 1 9 7 1.6 0 38 5 3 0.2 2 0.469 0 11 6 10 6 2.2 0 39 0 0.2 0 0.447 2 10 1 9 6 2.0 0 39 0 0.1 5 0.387 3 10 2 9 7 1.5 0 38 5 3 0.2 1 0.458 3 11 7 10 8 2.1 0 38 9 0.2 0 0.447 2 10 5 9 7 2.0 0 39 0 0.1 5 0.387 3 10 5 9 9 1.5 0 38 6 4 0.1 2 0.346 4 11 7 10 9 1.2 0 39 0 0.2 0 0.447 2 10 4 9 9 2.0 0 39 1 0.1 7 0.412 3 10 7 10 0 1.7 0 38 8 4 0.1 6 0.400 0 11 5 10 8 1.6 0 38 9 0.1 5 0.387 3 10 6 10 0 1.5 0 39 2 0.1 7 0.412 3 10 7 10 1 1.7 0 38 8 5 0.2 0 0.447 2 11 6 10 9 2.0 0 39 0 0,1 8 0.424 3 10 8 10 1 1.8 0 39 2 0.1 4 0.374 2 10 6 10 4 1.4 0 39 0 5 0.1 6 0.400 0 11 6 10 8 1.6 0 38 9 0.2 0 0.447 2 10 8 10 2 2.0 0 39 3 0.1 7 0.412 3 10 7 10 4 1.7 0 39 0 6 0.1 6 0.400 0 11 5 10 9 1.6 0 39 1 0.2 0 0.447 2 10 9 10 3 2.0 0 39 1 0.2 0 0.447 2 10 9 10 5 2.0 0 39 1 6 0.1 4 0.374 2 11 5 10 8 1.4 0 39 1 0.2 0 0.447 2 10 9 10 3 2.0 0 38 7 0.1 5 0.387 3 11 0 10 5 1.5 0 39 0 7 0.1 3 0.360 6 11 4 10 9 1.3 0 38 3 0.1 5 0.387 3 10 9 10 4
. 1.5 0 38 4 0.2 0 0.447 2 11 3 10 7 2.0 0 39 1 7 0.1 5 0.387 3 11 4 10 8 1.5 0 38 3 0.1 7 0.412 3 10 8 10 4 1.7 0 38 5 0.2 0 0.447 2 11 3 10 7 2.0 0 39 1 8 0.1 3 0.360 6 11 3 10 8 1.3 0 38 7 0.1 5 0.387 3 10 8 10 4 1.5 0 38 4 0.2 0 0.447 2 11 4 10 7 2.0 0 39 0 8 0.1 4 0.374 2 11 2 10 5 1.4 0 38 8 0.1 5 0.387 3 11 0 10 4 1.5 0 39 0 0.2 0 0.447 2 11 5 10 8 2.0 0 39 1 B 1 0.1 7 0.412 3 10 5 10 6 1.7 0 39 2 0.1 5 0.387 3 10 7 10 7 1.5 0 38 4 0,1 2 0.346 4 10 9 10 8 1.2 0 32 7 1 0.1 7 0.412 3 10 7 10 6 1.7 0 39 2 0.1 4 0.374 2 10 9 10 7 1.4 0 39 2 0.1 2 0.346 4 10 9 10 7 1.2 0 31 3 2 0.19 0.435 9 10 8 10 6 1.9 0 39 4 0.1 2 0.346 4 11 2 10 8 1.2 0 39 6 0.2 0 0.447 2 11 0 10 7 2.0 0 37 1 2 0.1 7 0.412 3 10 9 10 5 1.7 0 39 4 0.1 8 0,424 3 11 3 10 8 1.8 0 39 8 0.2 0 0.447 2 11 3 10 9 2.0 0 39 3 3 0.1 5 0.387 3 11 0 10 6 1.5 0 39 4 0.1 8 0.424 3 11 5 10 9 1.8 0 39 9 0.2 0 0.447 2 11 4 10 9 2.0 0 39 3 3 0.1 5 0.387 3 11 1 10 6 1.5 0 39 5 0.1 8 0.424 3 11 5 11 0 1.8 0 39 9 0.2 0 0.447 2 11 5 10 9 2.0 0 39 4 4 0.1 3 0.360 6 11 1 10 7 1.3 0 38 8 0.19 0.435 9 11 5 11 0 1.9 0 40 0 0.1 8 0.424 3 11 4 10 9 1.8 0 39 3 4 0.1 0 0.316 2 11 2 10 7 1.0 0 38 3 0.19 0.435 9 11 5 11 0 1.9 0 40 0 0.1 8 0.424 3 11 5 11 0 1.8 0 39 5 S 0.1 5 0.387 3 11 2 10 7 1.5 0 38 8 0.1 7 0.412 3 11 5 11 2 1.7 0 40 1 0.1 2 0.346 4 11 5 11 0 1.2 0 39 4 5 0.1 6 0.400 0 11 2 10 7 1.6 0 39 0 0.1 5 0.387 3 11 6 11 1 1.5 0 40 0 0.1 4 0.374 2 11 5 11 1 1.4 0 38 8 6 0.1 8 0.424 3 11 2 10 7 1.8 0 39 4 0.1 7 0.412 3 11 6 11 1 1.7 0 39 9 0.1 4 0.374 2 11 5 11 2 1.4 0 39 5 6 0.2 0 0.447 2 11 2 10 7 2.0 0 39 3 0.1 7 0.412 3 11 6 11 2 1.7 0 39 8 0.1 3 0.360 6 11 6 11 1 1.3 0 39 5 7 0.1 7 0.412 3 11 2 10 7 1.7 0 39 5 0.1 8 0.424 3 11 7 11 3 1.8 0 39 9 0.1 3 0.360 6 11 5 11 1 1.3 0 39 5 7 0.1 7 0.412 3 11 2 10 7 1,7 0 39 5 0.2 0 0.447 2 11 6 11 3 2.0 0 39 8 0.1 7 0.412 3 11 6 11 2 1.7 0 39 5 8 0.1 8 0.424 3 11 2 10 7 1.8 0 39 5 0.1 8 0.424 3 11 6 11 3 1.8 0 39 8 0.2 2 0.469 0 11 6 11 2 2.2 0 39 5 8 0.1 8 0.424 3 11 2 10 7 1.8 0 39 5 0.2 0 0.447 2 11 5 11 3 2.0 0 39 9 0.2 2 0.469 0 11 6 11 1 2.2 0 39 6

A V G 0.1 7 0.411 3 109. 3 1.7 1 39 0 0.1 7 0.416 6 107. 1 1.7 4 39 3 0.1 7 0.406 2 107. 9 1.6 7 38 5

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# Appendi xC Referenc e Metho d Calibrations , Verifications , an d Certification s

S:\_JOB\2006\Onyx\Performanc e Test\Report\Ony x200 6 Tes tReport.do c Septembe r200 6

# ENS R AECO M DR YGA S METER CALIBRATION Mete rBo xNo. : 8075 4 Chec k one : Annua l Calibratio n XRecalibratio n iDate : 3/14/200 6 Pretes t Lea k Check s | Operato rJames Ruckdesche l Allowabl e Actua

l | (Barometri c Pressure : 28.5 5 (i n Hg)l Positiv e 0 0.0 0 | [Theoretica l Critica l Vacuum : 13.4 7 (i n Hg)

j (a

t 5-7ln . H 2

0 ) in . H 2 0 pe

rmin . Manufacturer

: Anderso n NUTEC H Negativ e 0 0.00 0 Manufacturer

: Anderso n NUTEC H (a t 3in.Hg ) cf

m cf

m Dat e Received/Place

d i n service: Pr e 199 0 Seria l No. : 8075 4 DR YGA S METE R DAT A CRITICA L ORIFIC E DAT A
A H (i n H 2 0 ) Tim

e (min ) Volum e Ter n 3 Critica

l Orific e Serial * K

' Orific e Calibratio n Coefficien t Actua

l Vacuu m . (i n Hg ) Ambien

t Temperatur

e | A H (i n H 2 0 ) Tim

e (min ) Initia

l (ft 3 ) Fina

l (ft 3 ) Tota

l (ft 3 ) Initia

l Fina

l Critica

l Orific e Serial * K

' Orific e Calibratio n Coefficien t Actua

l Vacuu m . (i n Hg ) Initia

l Fina

l Averag

e | A H (i n H 2 0 ) Tim

e (min ) Initia

l (ft 3 ) Fina

l (ft 3 ) Tota

l (ft 3 ) ° F ° F Critica l Orific e Serial * K

' Orific e Calibratio n Coefficien t Actua

l Vacuu m . (i n Hg ) ° F ° F ° F I 0.24 20 677.30 0 683.17

0 5.87

0 6

9 70 4 8 0.225 1 5 6 8 68 6

8 

### I 0.91 1 5 691.80 0 700.156 8.356 74 74 52 0.427 1 5 6 9 73 7

1 

### J 1.5 0 1 5 711.600 722.61 3 11.01 3 7 6 79 63 0.56 2 1 5 7

3 74 7

4 

### j 3.8 0 1 0 733.800 744.59 0 10.790 8

1 83 7 6 0.83 1 1 5 7 2 7

3 7

3 

### I S

CORRECTE D VOLUM E I Dr yGa s Critica

l | DR YGA S METE R DRYGA S METE R j | Mete

r Orific

e I CALIBRATIO N CALIBRATION I 

### I V m (st d it

3 ) Ve r(st d ft

3 ) I FACTO R Y FACTO R AH ® \ J 5.58

7 5.591 I 1.00 1 -0.006 | | 1.72 7 -0.104 | [ 7.89

9 7.93

6 

### I 1.00 5 0.0

0 1.82 9 -0.003 | I 10.359 10.420 [ 1.00 6 0.0

0 1.74 8 -0.083 I I 10.124 10.281 

### I 1.01 6 0.01 2.022 0.1 9 

### I i | Avg . 1.00 7 

### ] I Avg . AH ® 1.83 2 | Notes : 1 ) Fo

rvali d tes t results , th e Actua l Vacuu m shoul d b e 1 t o 2 in . H g greate rtha n th e Theoretica

l Critica l Vacuu m show n above . 2 ) Th e Critica l Orific e Coefficient

, rC , mus t b e entere d i n Englis h units , (fty^'tde g R)*0.S/((in.Hg)*(mln))

. 3 ) Th e minimu m numbe ro fsampl e volum e require d pe rorific e i s 5 cubi c feet . 4 ) Fo rCalibratio

n Facto rY , th e rati o o fth e readin g o fth e calibratio

n mete rt o th e dr yga s meter , acceptabl

e toleranc e o findividua l value s fro m th e averag e i s ±0. C 5 ) Fo rOrific e Calibratio

n Facto rA H @ , th e orific e differentia

l pressur e in inche s o fH 2 0tha t equate s t o 0.7 5 cf m o faira t 6 8 F an d 29.9 2 inche s o fHg, acceptabl e toleranc e o findividua l value s fro m th e averag e i s ±0.2 .
Dr yGa s MaterThermocoupl e Calibratio n Ref . T C ID #Fluk e RT D 213103 ! Inle t ID# : 80754-I N Outle

t ID# : 80754-OU T Ref . Sourc e Ref

, ° F ° F A ° F A Amb . Ai r 6

5 6

6 -

1 6

6 1 Ho t Wate r 10

6 10

6 0 10

4 -

2 Potentiomete rCalibratio n |

Lo w 5 0 ° F 5

0 Mi d 45 0 ° F 450 Hig h 95 0 ° F 952_ J
Notes : 1 ) Ho

t Wate rt o b e i n th e rang e o f104-12 2 °F . 2 ) Toleranc e allowe d fo ral l thermocoupl

e individua

l reading s : ±5. 4 ° F 3 } Toleranc

e allowe d fo ral l potentiomete

rindividua l readings : ±2 ° F
P. + V.^ ) = ".6 4 (y„ > A H

1 3 . 6 t. +46 0 cr(std ) n{std )

# ENS R •AECO M DR YGA S METER CALIBRATION Mete rBo xNo. : 80645 Chec k one: Annua l Calibratio n XRecalibratio n Date : 12/27/200 5 I Pretes t Lea k Check s lOperator : Rya n Burns I Allowabl e Actua

l barometri c Pressure : 29.5 0 (inHg ) 1 Positiv e 0 0.0 0 |Theoretica l Critica l Vacuum : 13.9 2 (i n Hg) j (a t 5 - 7 in . H 2

0 ) in . H 20 pe

rmin . I Negativ

e 0 0.00 0 Manufacturer

: Anderso n NUTEC H j (a t 3 in . Hg ) cf

m cf

m Dat e Received/Place

d i n service: Pr

e 199 0 Seria l No. : DRYGA S METE R DAT A CRITICA L ORIFIC E DAT A
A H (i n H 2 0 ) Tim

e (min ) Volum

e Ter n P Critica

l Orific e Seria l # K ' Orific e Calibratio n Coefficien t Actua

l Vacuu m (inHg ) Ambien

t Temperatur

e A H (i n H 2 0 ) Tim

e (min ) Initia

l (ft 3 ) Fina

l (ft 3 ) Tota

l (ft 3 ) Initia

l Fina

l Critica

l Orific e Seria l # K ' Orific e Calibratio n Coefficien t Actua

l Vacuu m (inHg ) Initia

l Fina

l Averag

e A H (i n H 2 0 ) Tim

e (min ) Initia

l (ft 3 ) Fina

l (ft 3 ) Tota

l (ft 3 ) °p V Critica l Orific e Seria l # K ' Orific e Calibratio n Coefficien t Actua

l Vacuu m (inHg ) ° F ° F ° F 0.26 2 0 826.50 0 832.32

7 5.827 8

1 8

1 4

0 0.22

5 1 5 68 68 6 8 0.99 1 5 811.80 0 819.95

0 8.150 8

3 83 5 2 0.427 1 5 6 8 6 8 6

8 1.8 0 1 5 777.40 0 788.20

5 10.80

5 8

0 8

0 6

3 0.56

2 1 5 68 6 8 68 4.0 0 1 0 857.40 0 868.228 10.828 8 0 8

0 7

6 0.831 1 5 68 68 6 8

CORRECTE D VOLUM E Dr yGa s Mete r V m (st d ft

3 ) Critica

l Orific e Ve r(st d ft

3 ) 

### I 5.60 9 5.78

2 7.830 8.223 10.459 10.825 10.539 10.667 DR YGA S METE R CALIBRATIO N FACTO R Y I 1.03 1 -0.00 1 j 

### I 1.05 0 0.0 2 

### I 1.03 5 .0.0 0 I 

### j 1.01 2 -0.02 

### j I I DRYGA S METE R CALIBRATION FACTO R AH

® 1.75 0 -0.13 1 j 1.85 3 -0.028 1.94 4 0.06

3 1.97 7 0.1 0 

### I 

## I Avg . Y1.03

2 

## j j Avg . A H @ 1.881 \ Notes : 1 ) Fo

rvali d tes t results , th e Actua l Vacuu m shoul d b e 1 t o 2 in . H g greate rtha n th e Theoretica

l Critica l Vacuu m show n above . 2 ) Th e Critica l Orific e Coefficient

, K \ mus t b e entere d in Englis

h units , (fty^'fde g Ryvj.5/((in.Hg)*(min))

. 3 ) Th e minimu m numbe ro fsampl e volum e require d pe rorific e i s 5 cubi c feet . 4 ) Fo rCalibratio n Facto rY , th e rati o o fth e readin g o fth e calibratio

n mete rt o th e dr yga s meter , acceptabl

e toleranc e o findividua l value s fro m th e averag e 5 ) Fo rOrific e Calibratio

n Facto rA H ® , th e orific e differentia

l pressur e i n inche s o fH 2 0 tha t equate s t o 0.7 5 dm o faira t 6 8 F an d 29.9 2 inche s o fHg, acceptabl e toleranc e o fIndividua l value s fro m th e averag e I s ±0.2 .

Ref.TCIO * 2131035 Inle t ID# : 80645-I N Outle

t ID# : 80645-OUT l Lo w 5 0 ° F 5 0 Ref . Sourc e Ref

, ° F ° F A ° F A Mi d 45

0 ° F 449 Amb . Air 6

8 68 0 68 0

# I Hig h 95 0 ° F 948 | Ho t Wate r 11 2 11 2 0 11 1 - 1 | Notes : 1 ) Ho

t Wate rt o b e i n th e rang e o f10 4 -12 2 °F . 2 ) Toleranc e allowe d fo ral l thermocoupl

e individua

l reading s : ±5. 4 ° F 3 ) Toleranc e allowe d fo ral l potentiomete

rindividua l reading s : ±2 ° F

: 1 7 .6 4 

### (y

m 

### ] p . + AH /„ + 46 0 '(«d ) m (std

# ENS R AECO M DR YGA S METER CALIBRATION Mete rBo xNo. : 8018 4 Check one : Annua l Calibratio n Recalibratio n

Dat e Received/Place d i n service : Seria l No. : Date : 12/27/200 5 1 Pretest Lea k Checks [ Operator : Rya n Burn s | Allowabl e Actua l j Barometri c Pressure : 29.5 0 (i n Hg)

j Positiv e 0 0.00 Theoretica l Critica l Vacuum : 13.9 2 (i n Hg) | (a t5-7in
. H 2 0 ) in
. H 2 0 pe rmin
. Negativ e 0 0.00 0 Manufacturer: Anderson NUTEC H (a t3 in
. Hg) cfm cfm

DRYGA S METE R DAT A CRITICA L ORIFIC E DAT AI Volume Tem p Critica l K ' Orific e Actua l Ambien tTemperatur

e I A H Time Initial Final Total Initial Fina l Orific e Calibratio n Vacuu m Initia l Fina l Averag e j (i n H 2 0 ) (min

) (ft 3 ) (ft 3 ) (ft 3 ) ° F ° F Seria l # Coefficient (inHg ) ° F ° F ° F 0.26 20 103.30 0 109.11 5 5.81 5 78 79 40 0.225 1 5 6 8 68 6 8 0.99 1 5 83.30 0 91.38

5 8.08

5 7

5 7

6 52 0.427 1 5 6 8 68 6 8 1.8 0 1 5 161.70 0 172.46

8 10.76

8 8

2 83 6 3 0.56 2 1 5 6 8 68 6 8 4.00 1 0 134.00 0 144.63 1 10.631 83 8 4 76 0.83 1 1 5 6 8 6 8 6 8

CORRECTE D VOLUM E Dr yGas Mete r V m (st d ft 3) Critica l Orific e Ve r(st d ft3 ) 5.623 5.78

2 7.87 6 8.223 10.37 5 10.825 10.28 0 10.66

7 DR

YGA S METE R CALIBRATIO N FACTO R Y 1.02 8 -0.01 0 1.04 4 0.01 1.04 3 0.0

0 1.03 8 0.0

0 DRYGA S METE R CALIBRATIO N FACTO R AH ® I 1.75 0 -0.13 1 I 1.85 3 -0.028 1.94 4 0.06

3 1.97 7 0.1 0 

## j Avg . Y1.03

8 | Avg . A H @ 1.881 | Notes : 1 ) Fo rvali d tes t results , th e Actua l Vacuu m shoul d b e 1 t o 2 in
. H g greate rthan th e Theoretica l Critica l Vacuu m show n above
. 2 ) Th e Critica l Orific

e Coefficient , K' , mus

tb e entere d i n Englis h units , (ft^S'lde g R)"0.5/((in.Hg) -(min))
. 3 ) Th e minimu m numbero

fsample volume require

d pe rorific e i s 5 cubi cfeet
. 4 ) Fo rCalibratio n Facto rY , the ratio o fthe readin g o

fthe calibratio n mete rt

o the dr yga s meter , acceptabl e toleranc

e o findividua l values from the averag e i s 5 ) Fo rOrific e Calibratio n Facto rAH® , the orific e differentia l pressur

e i n inches o

fH 2 0 tha t equate s t o 0.7 5 cf m o fai ra t 68 F an d 29.9

2 inches o fHg , acceptabl e toleranc

e o findividual value

s from the average i s ±0.2
.
Dr yGa s Mete rThermocoupl e Calibratio n | Ref
. TCID # 2131035 Inle t ID* : 80184-I N Outle

t ID# : 80184-OU T Ref
. Sourc

e Ref , ° F ° F A ° F A Amb
. Ai r 68 6 8 0 6

8 0 Ho tWate r 11 1 11 1 0 11 1 o | Potentiomete rCalibratio n Lo w 50 ° F 5

0 Mi d 450 ° F 45

0 Hig h 950 ° F 951
Notes : 1 ) Ho

tWate rt o b e i n the range o

f10 4 -12 2 °F
. 2 ) Toleranc e allowe d fo ral l thermocouple individual readings : ±5. 4 ° F 3 ) Toleranc e allowe d fo ral l potentiomete rindividual readings : ±2 ° F



### •r

# ENS R AECO M SAMPL E PROB E CALIBRATIO N DAT A FOR M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E



### Thermocoupl e Calibratio n PROB E ID: M5-4-A Reformc * TrrarmomatwI D # : ENS R RT D #213103 5 Omeg a cnooo , *0602220

0 Omeg a CI1000 , #0602220 0 PROB E ID: M5-4-A Reformc * TrrarmomatwI D # : k»BaH ) Boiling Wtter TUDoFumaco[300 * SOO * 0 PROB E ID: M5-4-A « . —_- • - T C Hr * Tar « y«w a — r

l « Jva * jl « 3/6/200

6 M5-4-A 32.5 9 273.46 3 4 27

4 1 212. 2 373. 3 21 4 37 4 0. 3 450. 0 505. 3 45 1 506 0. 1 

### ra M5-4-A 32.5 9 273.48 3 4 27

4 1 212. 1 373. 2 21 4 374 0. 3 450. 0 505. 3 45 1 506 0. 1 

### ra M5-4-A 32.6 0 273.48 34 27 4 1 212. 0 373. 1 21 4 37 4 0. 3 450. 0 505. 3 45 1 506 0. 1 32.5 9 273.48 3

4 27

4 1 212. 1 373. 2 21 4 374 0. 3 450. 0 505. 3 45 1 506 0. 1 

### Type "S " Phot Tub e Calibration : Leve l an d Perpendicula r Obstructio n Damage d a , (-10°- : a , £+ 10°

) ct j (-10 ° £o^ s +10° ) B , (-5 ° 2 6,5+5* ) S 2(-5° s B 2s +5° ) T e z = ATany(±- - 0.125" ) W= ATan9(± s 0.03125" ) D , (3/1 6 s D,-

5 3/8 -) A/2D , (1.0

5 £P W1-5

) N o

N o 0. 8

0. 5

0.925 1.2 3 D*ar* « indkwtln

s Uv* l po»*ttor

. fo r d«t«m(n.naTth« n calculat

e Z
. 

### Pito

t Tub e t o Nozzl e Calibration :

1 ) Plto t t o nozzl a separatio n 2) TriefiTVXOLtpt

e t o pilo t separ . 3 ) Plto t an d l o probe unio n dia l >3/4 " (H/.500 nozzle ) >3/4 ' >3.0 ' 

### Prob e Informatio n
(Manufacturer : Dat e Receive d an d place d I n Service : Conditio n o l Prob e whe n place d I n service : .QA/Q C Chec k Completenes s X_ , Legibility RECONDITIONE D (circl e one )

Accurac yX
_ certifytha t th e Typ e S plto t tube/prob e ID#
_ _M5-4'-A
_ _meet s orexceed s af l Specffications , icftteri a and/o rapplicabl e desig n feature s an d Is hereb yassigne d a pltot tub e calibratio n (acto rC p o f0.8 4

Cartille d by : Fre d Sanguodoic e / 03-13-200 6 Personne l (Signature/Date ) Tea m Leade r(Signature/Date ) Al l constructio n criteri a fo ra n Isolate d *3 " typ e plto t ar e withi n give n tolerance s prescribe d I n Qualit yAssuranc e Handboo k to rAi rPollutio n Measuremen t Systems : Volum e III , StationarySource-Specifi c Methods . EPA/600/R-94/038c , Septembe r199 4

~> v06/P S

WOTES :

# ENS R AECO M SAMPL E PROB E CALIBRATIO N DAT AFOR M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E



### Thermocoupl e Calibratio n Rajforenc

a TrMnTOTietwrl D #

. M5-4- B
M5-4- B ENS R RT O #213103 5

273.52 273.52 3

4 3 4 3 5 274 Omeg a cuooo , #0602220

0

212. 2 212. 2 373. 3

373. 3 21 0 37

2 Omeg a C M 000 , #0602220 0 Tub a Furnac e (300 * - SOO * F ) 450. 0 450. 0 505. 3 447

447 503

50 4 -0. 3 50 4 -0. 3 32.67 273.52 3

4 212. 2 373. 3 21 0 •0. 3 450. 0 505. 3 44 7 503 

### Type "S " Pito

t Tub e Calibration : W- *

> ~*= F Leve l an d Perpendicula r Obstructio n Damage d a , (-10 ° £a , £+ 10°

) a- , (-10 ° £a, , £+10° ) B , (-5° £B , £+5° ) B-
. {-5° £fl 2 £+5° )
1 0 z = ATany(± £0.125" ) W= ATan0(-t £0.03125" ) D , (3/1 6 £D, £3/8" ) A A/2D , (1.05 £P,/D, £1-S )
O-agrw * indicatin g Uv« l positio n fo r dat«mintneYth« n calcutct * Z. Ye s N o N o

0. 1

0. 9
0.01 4 0.375



### Pito t Tub e t o Nozzl e Calibration :

atria l V».7.«aTtfair.. ) = l i 

### Bal l

1 ) Pilo t t o nozzl e S« f 2 ) Thtymocoopl e to pilo t s«par . 3 ) Plto t an d to probe unio n dts t >3/4 ' (w/.500nozzte) >3/4 " >3.0 " 0.376 0.975 

### Prob e Informatio n
(Manufacture r Dat e Receive d an d place d I n Service : I Conditio n ot Prob e whe n place d I n service : pre-199 5

QA/Q C Chec k Completenes s X Legibilit y_X_
_ RECONDITIONE D (circiaone )

Accurac y. Specification s X
_ [Reasonablenes s X
1 1 certif ythat th e Typ e S pitot tube/prob e 1D#
_ _meet s o rexceed s al l Specifications , criteri a and/o rapplicabl e desig n feature s an d I s hereb yassigne d a pilo t tub e calibratio n (acto rC^ot 0.8 4

Certifie d by : Fre d Sanguedolc e / 03-13-200 6 Personne l (Signature/Date ) Tea m Leade r{Signature/Date ) A U constructio n criteri a fo ra n Isolate d "S " typ e pltot ar e withi n give n tolerance s prescribe d i n (QualityAssuranc e Handboo k fo rAi rPollutio n Measuremen t Systems : Volum e 111, Stationar ySource-Specifi c Ntetnods . EPA/600/R-94/038C . Septembe r199 4

! ^>V06/P S

# ENS R AECO M SAMPL E PROB E CALIBRATIO N DAT AFOR M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E



### Thermocoupl e Calibratio n

M S 5- F MS-5- F 32.1 8 32.1 8 273.25 273.25 33 Omeg a C M 00 0 #06 0

211. 8 211. 8 373. 0

373. 0 209 37 1

37 1 -0. 4 -0. 4 -0. 4 Omeg a CI100 0 #060 2

450. 0 505. 3 450. 0 505. 3 44

3 44 3 50

2 -0. 7 50 1 273.2 5 211. 8 373. 0 209 •0.4 450. 0 505. 3 44 3 

### Typ e "S " Pito

t Tube Calibration :

Leve l an d Perpendicula r Obstructio n Damage d a , (-10 ° £a , £+ 10°

) (-10° £a- £+10° ) B , (-5° £I3,£+5° ) 13- , <-5°£G 2 £+5° ) T 0 z = ATany(± £0.125" ) W= ATan0(± s 0.03125" ) 0 , (3/1 6 £D, £3/8" ) A A/2D , (1.05 £PVD| £1-5 )
D«gr* « indicatin g Wv« i poaJtlon fo r detan-itnlnsftha n ctslculat * Z . Ye s
0. 3 0. 9

-0. 4

1.1 2


### Pito t Tube to Nozzl e Calibration :

Yin7,aawn<3ln. ) j

1 ) Plto t t o nozzl e separatio n X 2 ) TtiefTTrOCoapl

a t o plto t separ . Z 3 ) Plto t en d t o prob e unio n dist Y >a/4 ' (w/,50 0 nozzle ) >3/4 * >3.0 ' 1.027 1.&4 5 

### Probe Informatio n Manufacturer

. Dat e Receive d an d place d t n Service : iCondttto n o (Prob e wha n place d I n service : |QA/Q C Chec k Completenes s Legibility_X
_ RECONDITIONE D (circl e one )

Accurac yX
_ Specification s __X_
_ Reasonablenes s I certif ytha t th e Typ e S pilo t tube/prob e ID#
_ _M5-5'-F
_ _meet s o rexceed s al l Specifications . icittert a and/o rapplicabl e desig n feature s an d Is hereb yassigne d a pitot tub e calibratio n facto rC D o10.8 4

Certifie d by : Fre d Sarquedolc a / 03-13-200 6 Personne l (Signature/Date ) Tea m Leade r(Signatura/Date ) Al l cor^ructto n criteri a to ra n isolate d "S " typ e pilo t ar e withi n give n tolerance s prescribe d i n Qualit yAssuranc e Handboo k fo rAi rPollutio n Measuremen t Systems : Volum e III . Stationar ySource-Specifi c Methods . |6PA/600/R-94/038c , Septembe r199 4 06/P S

NOTES :

# ENS R Calibrator : Rya n Burn s Referenc e Thremomete rID : DV M CCL05015241 7 Date : 3/6/200 6 Las t Impinge rThermocoupl e Calibratio n 200 6 Thermocoupl e Referenc e Differenc e (+/ - 2° ) Thermocoupl e Referenc e Differenc e (+/ - 2° ) 1 1 o Ho

t 21 2 21 2 0 1 1-9 1 Ho t 21 1 21 1 0 Ll- Z Col d 3 3 3 2 1 Col d 3 3 32 1 Manufacture rAnderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pre 1990 Dat e received/place d i n service : Pr e 199 0

1 1 A Ho

t 21 1 21 1 0 Ho t 21 3 21 2 1 LI-4 Col d 3 3 3 3 0 Col d 3 5 3 3 2 Manufacture rAnderso n NUTEC H Manufacturer : Seria l No. : Seria l No. : Dat e received/place d i n service : Pre 1990 Date received/place d i n service : Pre 199 0 1 I-/ 5 Ho t 0 1 1-9' ? Ho t 21 1 21 2 - 1 LI-O Col d 0 Col d 35 3 3 2 Manufacturer : Anderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Date received/place d i n service : Pr e 199 0 LI-7 Ho

t 21 2 21 2 0 LI-24 Ho t 0 LI-7 Col d 3 3 3 2 1 LI-24 Col d 0 Manufacturer . Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 1990 Dat e received/place d i n service : Pre 1990 

### mm P M U- 8 Ho

t 21 2 21 2 0 LI-25 Ho t 21 2 21 2 0 U- 8 Col d 3 4 3 3 1 LI-25 Col d 3 3 32 1 Manufacture rAnderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pre 1990 Dat e received/place d i n service : Pre 199 0 LI-9 Ho

t 21 1 21 2 -1 Ll-2 6 Ho t 21 4 21 2 2 LI-9 Col d 3 3 3 3 0 Ll-2 6 Col d 35 3 4 1 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 1990 Dat e received/place d i n service : Pre 199 0 LI-1 0 Ho

t 21 2 21 2 0 LI-27 Ho t 21 0 21 2 - 2 LI-1 0 Col d 3 2 3 2 0 LI-27 Col d 3 4 3 3 1 Manufacturer : Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n service : Pr e 1990 Dat e received/place d i n service : Pre 199 0 Ll-1 1 Ho

t 0 1 I-9 A Ho t 21 2 21 2 0 Ll-1 1 Col d 0 Col d 3 3 3 3 0 Manufacturer . Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n service : Pr e 1990 Dat e received/place d i n service : Pr e 1990 LI-1 2 Ho

t 21 1 21 2 - 1 1 I-9

Q Ho t 21 2 21 2 0 LI-1 2 Col d 3 2 3 2 0 Col d 3 3 3 3 0 Manufacturer : Anderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n service : Pre 1990 Date received/place d i n service : Pre 1990 Ll-1 3 Ho

t 21 3 21 2 1 Ho t 21 3 21 2 1 Ll-1 3 Col d 3 3 3 3 0 1.1* 0 Col d 34 33 1 Manufacturer : Anderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n service : Pre 1990 Dat e received/place d i n service : Pre 199 0 LI-2 0 Ho

t 21 1 21 1 0 1 1 1 A Ho t 21 1 21 1 0 LI-2 0 Col d 3 4 3 3 1 Ll - 1 1 Col d 32 3 3 - 1 Manufacturer : Anderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n ser . Pre 1990 Dat e received/place d i n service : Pre 1990 ; chectt vaiir

e use e fo rlmpnaj - trfa t 1 1

### ENS R AECO M

Calibrator : Fre d Sanguedofc e Referenc e Thermometer : Fluk e RT D 213103 5 Fitte rBo xCalibratio n Ho t Bo x#

1 Ho tBo x#1 1 Manufacturer : Anderso n NUTEC H I v anirfacturer : Anderso n NUTEC H Seria l No. : Dat a received/place d I

n service : N/

A Pr e 199 5 S D erialNo. : at e received/place d I n service : N/

A Pr e 199 5 Calibratio n Date : 16-Feb-0 6 C .alibratio n Date : 16-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 9 24 7 P eterenc e Temperature s 7 2 24 6 Actua l Temperature s 6 9 24 9 A dua l Temperature s 7 1 24 9 Tem p Differenc e (tol . - +-2 ) 0 - 2 1 em p Differenc e (tol . * +-2 ) 1 - 1 Ho tB e >X# 2 Ho tBo x#1 2 Manufacturer : Anderso n NUTEC H t \ rlanufacture n Anderso n NUTEC H Seria l No. : N/ A •aria

l No. : N/A Date received/place d I n service : Pr e 199 5 r .at e received/place d I n service : Pr e 199 5 Calibratio n Date : 15-Feb-0 6 C Alibratio n Date : 16-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 6 24 9 f Referenc e Temperature s 7 0 24 6 Actua l Temperature s 7 0 24 7 Actua l Temperature s 7 1 24 7 Tem p Differenc e (tol . = +-2) -2 2 em p Differenc e (tol . = +-2 ) - 1 - 1 Ho t Bo x#

3 Ho t Bo x#1 3 Manufacturer : Anderso n NUTEC H vlanufacturer : Anderso n NUTEC H Seria l No. : N/ A Seria l No. : N/ A Date racervad/place d I n service : Pr e 199 5 Dal e received/place d i n service : Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 1$-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 9 24 4 Referenc e Temperature s 6 7 24 6 Actua l Temperature s 6 9 24 4 Actua l Temperature s 6 7 24 6 Tem p Differenc e (tol . = +-2 ) 0 0 Tem p Differenc e (tol . = +-2 ) 0 0 Ho tBo x#

4 HotBo x#1 4 Manufacture r Anderso n NUTEC H Manufacturer
. Anderso n NUTEC H Seria l No. : •at e received/place d I n service : N/ A Pr e 199 5 Seria l No. : Dat e received/place d i n service : N / A Prft199 5 Calibratio n Date : 1&-Feb-06 Calibratio n Date : ie-Feb-0 6 Ambien t Hot Ambien t Ho t Referenc e Temperature s 7 1 24 4 Referenc e Temperature s 6 8 24 7 Actua l Temperature s 7 1 24 3 Actua l Temperature s 7 0 24 7 Tem p Differenc e (tol . = +-2 ) 0 1 Tem p Differenc e (tol . = +-2) - 2 0 Ho tBo x# 5 Ho tBo x#1 5 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Date received/place d I n servic e N/ A Pr e 199 5 Seria l No. : Dat e received/place d I n service : N/A Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 15-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 6 6 25 1 Referenc e Temperature s 6 8 24 7 Actua l Temperature s 6 6 25 2 Actua l Temperature s 6 6 24 7 Tem p Differenc e (tol . = +-2

) 0 - 1 Tem p Differenc e (tol . = +-2 ) 2 0 Ho U 3ox# 6 Ho tBo x#1 6 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Date received/place d I n servic e N/ A Pr e 1995 Seria l No. : Dat e received/place d i n servic e N/A Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 17-Feb-0 6 Ambien t Hot Ambien t Hot Referenc e Temperature s 6 9 24 5 Referenc e Temperature s 7 1 24 1 Actua l Temperature s 7 0 24 5 Actua l Temperature s 6 9 24 1 Tem p Differenc e (tol . = +-2 ) -

1 0 Tem p Differenc e (tol . = +-2) 2 0 Ho t BO X# 7 Ho tBo x#1 7 Manufacturer : Seria l No. : Date received/place d I n servic e Anderso n NUTEC H

U/ A Pr e 199 5 Manufacturer : Seria l No. : Dat e received/place d i n servic e Anderso n NUTEC H N/A Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 16-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s Actua l Temperature s 7 1 24 8 Referenc e Temperature s 6 9 24 5 Referenc e Temperature s Actua l Temperature s 7 1 25 0 Actua l Temperature s 7 0 24 7 Tem p Differenc e (tol . = +-2 ) 0 - 2 Tem p Differenc e (tol . = +-2 ) - 1 - 2 HotBo x# 6 Ho t Bo x#1 8 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date received/place d I n servfca : Pr e 199 5 Manufacturer : Anderso n NUTEC H Seria l No. : N/A Dat e received/place d i n service : Pr e 199 5 Calibratio n Date : 16-Feb-0 6 Calibratio n Date : 15-Feb-0 6 Ambien t Ho t Ambien t Ho t Referenc e Temperature s 7 0 24 4 Referenc e Temperature s 7 2 24 7 Actua l Temperature s 7 1 24 6 Actua l Temperature s 7 0 24 8 Tem p Differenc e (tol , = +-21 - 1 •2 Tem p Differenc e (tol . = +-2 } 2 - 1 Hot Bo x#

9 Ho tBo x#1 9 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date recetved/place d i n service : Pr e 199 5 Seria l No. : N/ A Dat e received/place d i n service : Pr e 199 5 Calibratio n Date : 1&-Feb-06 Calibratio n Date : 16-Feb-0 6 Ambien t Hot Ambien t Ho t Referenc e Temperature s 6 9 24 9 Referenc e Temperature s 7 0 24 4 Actua l Temperature s Tem p Differenc e (tol . = +-2

) 7 0 25 1 Actua l Temperature s 7 1 24 4 Actua l Temperature s Tem p Differenc e (tol . = +-2

) -

1 - 2 Tem p Differenc e (tol . = +-2 ) - 1 0 Ho tBo x#1 0 Ho tBo x#2 1 Manufacturer : Anderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Date received/place d t n service : Pre 199 5 Seria l No. : N/A Dat e received/place d I n service : Pr e 199 5 Calibratio n Date : 16-Fetv0 6 Calibratio n Date : 17-Feb-0 6 Ambien t Ho t Ambien t Hot Referenc e Temperature s 7 3 24 7 Relerenc e Temperature s 6 6 24 1 Actua l Temperature s 7 2 24 6 Actua l Temperature s 6 9 24 3 Tem p Differenc e (tol . = +-2 ) 1 1 Tem p Differenc e (tol . = -4-2 ) -

1 -2

# ENS R AECO M

XA D Thermocoupl e Calibration s - 200 6 date 3/13/200 6 BP : 29. 1 Referenc e Thermomete rID#: Manufacture : Dat e place d i n Service : Calibrator : Jame s Ruckdesche l Ambien t Tem p (F) : 6 3 Fluk e Digita l RT D 213103 5 Fluk e Pr e 198 0
Ic e Bat h 

# I Ambien t Thermocoupl e 1D # Referenc e

Tem p XA D

Tem p Tem p

Differenc e To l = +- 2 F Referenc e

Tem p XA D



### Tem p Tem p

Differenc e To l = + - 2 F XAD - 1 3 3 3 2 - 1 6 2 6 2 0 XAD- 2 3 3 3 3 0 6 2 6 3 1 XAD - 3 3 3 3 1 - 2 6 2 6 2 0 XAD- 4 3 1 3 1 0 6 3 6 3 0 XAD- 5 3 1 3 3 2 6 3 6 3 0 XAD - 6 3 2 3 2 0 6 3 6 3 0 XAD- 7 3 2 3 2 0 6 4 6 4 0 XAD- 8 3 2 3 2 0 6 5 6 3 - 2 XAD - 9 0 0 XAD-1 0 3 2 3 2 0 6 6 6 4 - 2 XAD -1 1 0 0 XAD -1 2 0 0

# ENS R

Appendi xD Stac k Configuration , Samplin g Por t an d Travers e Poin t Location s

S:\JOB\2006\OnyjAPerforrnanc e Test\Report\Ony x200 6 TestReport.do c Septembe r200 6T 3



### ENS R ENS R CORPORATIO N 660 1 Klrfcvllle Roa

d Eas t Syracuse , Ne

wYork 1305 7 

### AECO M FIXE D HEART H INCINERATO R UNI T3

VEOLI AE S TECHNICA LSOLUTION S

Sauget , Illinoi s 

### i



# 1

PHONE : (315 ) +32-050 6 FAX : (315) 437-050 9 WEB : HTTP://WWW.ENSR.AEC0M.CO M DRAW N BY : CHECKE

D BY : DATE

: PROJEC

TNUMBER

; DRAWIN

G NUMBER

: PHONE : (315 ) +32-050 6 FAX : (315) 437-050 9 WEB : HTTP://WWW.ENSR.AEC0M.CO M LL M W W 9/11/0 6 10002-01 7 1 O F 1 <

### )

I 

### TRAVERS E POIN TLOCATIONS (Particulat e Travers e - Circula rStack )

FACILTY : Ony xEnvironmenta l Service s STAC KIDENTIFICATION : Uni t 3 STAC KDIAMETER : 3 9 inche s SAMPLIN G LOCATIONS : 14.9 5 diameter s downstrea m 9.8 5 diameter s upstrea m MINIMU M NUMBE R O F TRAVERS E POINT S A S SPECIFIE D B YEP AMETHO D 1 : 1 6
NUMBE R O F TRAVERS E POINT S SAMPLED : 1 6

Travers e Poin tPercen tofStac k Diamete r Numbe rFro m Insid e Wal l Distanc e i n Inche s Fro m Insid e Wall * 1 3. 2 1. 2 2 10. 5 4. 1 3 19. 4 7. 6 4 32. 3 12. 6 5 67. 7 26. 4 6 80. 6 31. 4 7 89. 5 34. 9 8 96. 8 37. 8

* Fo rstack s wit h a n insid e diamete r(ID ) of2 4 inche s o rless , n o travers e poin t ma yb e locate d withi n 0. 5 inche s ofth e insid e wall
. Fo rstack s wit h a n I D greate rtha n 2 4 inches , n o travers e poin t ma yb e locate d withi n 1. 0 inche s ofth e insid e wall
. An ypoin t notmeetin g th e criteri a shal l b e adjusted
.

# ENS R

Appendi xE Laborator

yDat a

S:\_JOB\2006\Onyx\Performanc e Test\Report\Ony x200 6 Tes tReport.do c Septembe r200 6

# ENS R AECO M

ENS RAi rToxic

s TSPLaborator

y Analytica l Repor t
Client : Jef

f Gorma nClientID : 10002-01 7 ENSR 660 1 KirkvilleRoa

d E . Syracuse

, N Y 1305

7 Laborator

y ID : 06-06

7 Dat e Received : 5/12/0

6

A l l wor k containe d i n thi s repor

t ha s bee n don e i n accordanc e wit h laboratorystandard operatin g procedures
. ENSR' s Ai r 3 Toxic s TS P Laborator yfollow s methodologie s base d upo n standard EPA/NIOSH/OSH AMethods
. Dat a containe d herei n shoul d b e considere d accurat e an d complet e t o th e bes to fou rknowledge
. Thi s repor t canno tb e dupUcate d i n par t withou t th e writte n pennissio n o fENSR
.

Arthu rCarpenit o / Dat e LaboratoryAnalys t ENS R Ai rToxic s TS P Laboratory

NYSDO H / NELA C # 1163 1

pag e 1 o f6ENS R I ArX.P M

Metho d 5 Expose

d FilterDat

a Shee t Projec t Manager : Project Name : Project Nunrtber: Analysi s Mathod : Jef fGorman Projec t Manager : Project Name : Project Nunrtber: Analysi s Mathod : Ony x Star t Frida

y 05/12/0

6 16:3

4 4

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6 15:3

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6 7

2 A C Projec t Manager : Project Name : Project Nunrtber: Analysi s Mathod : tttJlrtlf'lWIrnalinrt . * or Oven Drie d Wt. 2 Tuesda y 05/16/0

6 9:2

8 3

7 7

2 A C Wt. 3 Wt. 4 OASIflSt Initial Wolah l filter * Sampl o ftunDat* •k

'. yim^i ^'.'.b; . i . i
, *8 »mnKil D Filter J^po/Stlg ^ 1» l w u

•Sffi'mi 1 . * jlnd Wt

. A1UW t Grairij | J •4th w j • " OftTM* " Tsiuvn . AF^HH WI OASIflSt .1 , OM». . filter * Sampl o ftunDat* •k

'. yim^i ^'.'.b; . i . i
, *8 »mnKil D Filter J^po/Stlg ^ 1» l w u

•Sffi'mi 1 . * jlnd Wt

. A1UW t Grairij | J •4th w j • " OftTM* " Tsiuvn . 20 4 01/09/0

6 0,409

3 G383

2 N/

A LA B FILTE R BLAN K 9 0 m m 0.409

2 0.409

4 0.000

2 okbyWt . 0.409 3 0.000

3 20 4 01/09/0

6 0.406

7 G382

5 05/09/0

6 PRETEST-M5-FILTE R 9 0 m m 0.410

1 0.410

2 0.000

1 o k b yWt . 0.410 2 0.003

5 20 4 01/09/0

6 0.405

7 G382

7 05710/0

6 U3-M5-F-R 1 9 0 m m 0.408

6 0.408

8 0.000

2 okbyWt . 0.408 7 0.003

0 20 4 01/00/0

6 0.405

4 G382

4 05/10/0

6 U3-M5-F-R2 9 0 m m 0.413

6 0.413

4 0.000

2 o k b yWt . 0.413 5 0.008

1 20 4 01/09/0

6 0.405

4 G382

8 05/11/0

6 U3-M5-F-R3 9 0 m m 0.412

6 0.412

4 0.000

2 o k b vWt . 0.412 5 0.007

1 • o 0J o a C D w o

Fille

rTyp a Tolio n Quail *

1 . Deli a Weigh l loloranc a t/ -O.OOOS

g o ftota l woigh l les s tar e weigh ! betwee n tw o consecutiv

e weighting

s o raverag e weight . 2 . Filter s mus t b e weighe d wil h Ih e prope rcondition s (R H = 2 5 - 6 0 % an d R T= 50-7 8 de g f ) 3 . Filler s mus t b e propotl yconditione

d (2 4 hou rdesiccation: Furthe

rConditionin

g > 6 hours)

. 4 . Conditionin

g fo rove n method ; Ove n drio d a t 10 5 de g c f o 2- 3 hours ; Furthe rconditionin

g > 6 hours

. 5 . Tota l grant s belo wo requa l t o .000 5 (I.DL ) i s presente d a s .0003 .ENS R ! .v. .

Metho d S Fron t Hal fAceton e Prob e Rins e Dat a Shee t Balanc e Used : Matller3 Projec t Manager : Projec t Name : Project Number . Analvs/ s Method : JelfGorma

n 

# mm H i 72 Projec t Manager : Projec t Name : Project Number . Analvs/ s Method : Ony

x Star t Tuesda

y 05/16/0

6 15:4

0 4

4 72 A C Projec t Manager : Projec t Name : Project Number . Analvs/ s Method : 10002-01 7 Wt . 1 Wednesda y 05/17/0

6 17:0

6 4

1 7

1 A C Projec t Manager : Projec t Name : Project Number . Analvs/ s Method : Namra l Kuanoraiin n o r !Hfia);Ai&fiMliif i Wt. 2 Thursda y 05/18/0

6 8:4 7 4

7 6

9 A C " Wt. 3 Thursda y 05/18/0

6 14:4

8 4

0 7

3 A C Wt. 4 BASIwo l ... . l L Bi>akfijl L Simpl e m
, .^Simpj o I

D 1 Hol d Lab * 

# ' * » lill l 'SSSL 43 4 05/11/0 6 115.166 6 3 2 N/

A LA B ACETON E BLAN K 5 0 115.168

6 115.167

8 0.000

8 115.167

6 0.000

0 ok b yWL 115.167 8 0.001 0 43 4 05/11/0 6 86 .2956 3 9 05/09/0 6 PRETEST-M5-ACETON E 5 2 5 0 86.299

2 86.296

8 0.000

4 o k byWt . 86.299 0 0.003

4 43 4 05

/11 /0 6 103 .534

7 6 4 05/10/0 6 U3-M5-AR-R 1 6 3 5 0 103.538

3 103.537

7 0.000

6 103.537

8 0.0001 o

k b yWt . 103.537

8 0.003 1 43 4 05/11/0 6 101.047 5 12 0 05

/10 /0 6 U3-M6-AR-R 2 11 1 5 0 101.054

2 101.054

0 . 0.000

2 o k b yWt . 101.0541 0.006 6 43 4 05/11/0 6 105.363 2 154 05/11/0 6 U3-M5-AR-R 3 9 5 5 0 105.3691 105.368 9 0.000

2 o k byWt . 105.369 0 0,005

8

Acetone Manufacturer/to t No.:_F(sher/052584 : Aceton o Rins e - 2 5 mi s twic o •(S Q nil s totnl ) . . . 1 . Deli a Weigh t toleranc e +/-0.0Q05

g o ftota l weightles s tar e weigh t betwee n tw o consecutiv

e weighting

s o raverag e weight . 2. Beaker s mus t b o weighe d wit h th o prope rcondition s (R K = 2 5 * 5 0 % an d R T« 59-7 8 de g f ) 3 . Beaker s mus t b o propert yconditione

d (2 4 hou rdesiccation; Furthe

rConditionin

g > 6 hours)

. 4 . Natural Evaporatio

n Metho d = Evaporat

e t o drynossa

t roo m temperatur

e unde ra hood/watc

h glas s cove r 5 . Moa t Applicatio

n = Unde ra hoo d an d watc h glas s ove rsample , appl yhea t belo wth e boilin g poin t o fsampl e unti l evaporate

d t o 2 5 mis ; the n follo wste p 4 (above

) fo rremainin g portion . 6 . Tota l gram s belo wo requa l t o .000 5 (LDL ) i s presente d a s .0003 .

### PROJECT NARRATIV E Maxza m Analytic

s (Burlingto

nON ) Maxxam ; Jo

b # : A64446 9 Client : ENS RInternationa l Clien tProject: 10002-017-01

7 ONY X L SAMPL E RECEIPT/ANALYSI S

a ) Sampl e Listin g 

### Maxxa m Clien

t Dat

e Dat

e Dat

e Dat

e I D Samplel

D Sample

d Receive

d Proppe

d Ru n Mercury IB via EPA Method 29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 8 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 8 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 8 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 7 06705/1 8 

### Mercury 2B via EPA Method 29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 6 

### Mercury 3A via EPA Method 29 L9982 8 TJ3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06705/1 5 06/05/1 6 

### Mercury 3B via EPA Method 29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 5 06/05/1 6 

### Mercury 3C

via EPA Method

29 L9982 8 U3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 6 06/05/1 8 

### Metals in Air(Combined) via EPA Method 29 (ICP/MS) L9982 8 TJ3-M29-R B 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 L9982 9 U3-M29-R 1 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 L9983 0 U3-M29-R 2 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 L9983 1 U3-M29-R 3 06/05/1 0 06/05/1 2 06/05/1 7 06/05/1 9 R u n Dat e i s define d a s th e dat e o finjectio n ofth e las t calibratio n standar d (1 2 hour s o rless ) prio rt o th e sample s analyze d withi n tha t ru n sequence . Therefor e th e tim e o fcalibratio n injectio n tha t define s th e ru n dat e i s alway s withi n 1 2 hour s o fth e tim e o fsampl e injection . b ) Shippin g Problems : non e encountere d
c ) Documentatio n Problems : non e encountere d 

### J H Pag e 1 o f 2

### I L SAMPL E PREP : N o problem s encountere

d U L SAMPL E ANALYSIS : Se e als o comment

s withi nth e appropriat

eCertificat

eo f Analysi s a ) Hol d Times : al l withi nrecommende

d hol d time s b ) Instrumen

tCalibration

: a U withi ncontro l limit s c ) Qualit y Control : Al l applicabl

e Q C meet s contro l criteria , excep twher e otherwis e noted . I certif y tha tthi s dat apackag e i s i ncomplianc

e wit h th e term s an d condition

s o f th e contract , bot h technicall

y an d fo rothe rtha nth e condition

s detaile d above . I naddition , I certify , tha tt o th e bes to f m y knowledg

e an d belief , th e dat aa s reporte d ar e tru e an d accurate . Releas e o f th e dat acontaine d i nthi s dat apackag e ha s bee nauthorize

d b y th e cognizan

tlaborator y officia l o rhis/he rdesignee , a s verifie d b y thi s signature

.

Mary-Ann <

J H Pag e 2 o f2

# 2 . DAT A SUMMAR Y

- Certificat

eo f Analysi s -
Sampl e analyt e resul t Metho d blan k

resul t LC S Result s wit h % Recoverie s Matri xSpik e data wit h % Recoverie s Matri xSpik e Duplicat e data wit h % Recoverie s Surrogat e recoverie s2 | ^^^^^ | Driven by service and Science You rProject* : 10002-017-01 7 Site : ONY X
Attention : Jef fGorma n ENS R Internationa l 6601KirkvilleR d EastSyracuse , N Y US A1305 7 Repor tDate : 200(5/05/2 0 

### CERTIFICAT E O F ANALYSI S MAXXA M JO B # : A64446 9 Received : 2006/05/12,12:0 0 Sampl e Matrix : Filte r # Samples Received : 4 Dat e Dat

e Metho d Analyse s Quantit y Extracte

d Analyze

d Laborator

y Metho d Referenc

e Mercur y lB-AirCFilta+Acctone)b y CVAA © 4 2006/05/1 7 2006/05/18 SOPING11 1 . EP A CF RPT M 2 9 Metal s inAi r(Combined

) b y ICP/MS © 4 2006/05/1 7 2006/05/19 SOPTN G 108/10 9 EP A SW846-602 0 Sampl e Matrix : Impinge rSolutio n # Samples Received : 4 Analyse s Quantit y Dat

e Extracte d Dat

e Analyze d Laborator

y Metho d Metho

d Referenc e Mercur y 3 C i nAi r(HC

IImpinger

) byCVA A © Mercur y 3 A inAi r(HN0

3 Rinse ) b yCVA A Q Mercur y 2 B inAir(HN03/H20 2 Imp ) b y CVA A © Mercur y 3 B i nAi r(KMnO4/H2S04) by CVA A © 4 2006/05/16 2006/05/18 SOPIN G 111 4 2006705/1

5 2006/05/16 SOPIN G 11 1 4 2006/05/16 2006/05/16 SO PIN G 11 1 4 2006/05/1

5 2006/05/16 SOPING 11 1 EP A CF RPT M 2 9 EP A CF RPT M 2

9 EP A CF RPT M 2

9 EP A CF RPT M 2

9 {1 ) Thi s tes

t was performe d b yMaxxa m Analytic s Burlingto n

.7 2 Pag e 1 o f1 1 674 0 Campobell o Road
. Misstssauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Td l free:800-563-626 6 Fax : 905-817-577 7Attention : Jef fGorma n ENS R Internationa l 6601KirkvilleR d EastSyracuse , N Y US A1305 7 Driven t>y service and Science www.wiaxxamanalytlcs.co m You rProjects
. 10002-017-01 7 "Site : ONY X

Repor tDate : 2006/05/2 0
CERTIFICAT E O F ANALYSI S

-2 -



### J Validate d by :

Tota l cove rpages : 2 Page2o f1 1
674 0 Campobell o Road , Mississauga
. Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free.800-563-626 6 Fax : 905-817-577 7£ AoBlytlc s in c

Maxxa m Jo b #:A64446 9 Repor tDate : 2006/05/2 0 Driven by service and Science ENS R Internationa l Clien tProjec

t#. 10002-017-01 7 Projec tname : ONY X Sample rInitials : 

### MERCUR YB YCOL D VAPOU R A A(FILTER ) Maxxa m I D L9982 8 L9982 9 L9982 9 L9983 0 L9983 1 Samplin g Date 2006705/1 0 2006/05/1 0 2006/05/1 0 2006/05/1 0 2006/05/1 0

Units U3-M29-R B U3-M29-R 1 U3-M29-R 1 Lab-Du p U3-M29-R 2 U3-M29-R 3 RD L Q C Batc h MD L
Tota l Mercury-1 B u g . N D N D N D 0.1 0 0.27 0.0 3 972395 0.03 N D = No t detected RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit

yContro l Batc h

Pag e 3 o f1 1 674 0 Campobell o Road
. Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:S00-563-626 6 Fax:905-817-577 7

## IVi a y&st

m f w ,s^ Analytic s ir* c Maxxa m Jo b # : A64446 9 Repor tDate : 2005/05/2 0 Driven by service aitd Science www.imixxainanalytics.co m ENS R Internationa l Clien tProjec

t# : 10002-017-01 7 Projec tname : ONY X Sample rInitials : 

### ELEMENT

S BYICP/M S (FILTER

) Maxxa m I D L9982 8 L9982 9 L9982 9 L99830 L9983 1 Samplin q Dat

e 2006/05/1 0 2006/05/1 0 2006/05/1 0 2006/05/1 0 2006705/1 0

Units U3-M29-R B U3-M29-R 1 U3-M29-R 1 Lab-Du p U3-M29-R 2 U3-M29-R 3 R D L 3 C Batc h M D L
Tota l Arseni c (As) u g 0.76 9.29 9.62 24 9 946 0.40 . 97201 2 0.4 0 Tota l Berylliu m (Be

) u g N D N D N D N D N D 0.1 0 97201 2 0.1 0 Tota l Cadmiu m (Cd ) u g 

### 034 0.68 0.7 1 1.3 8 2.76 0.1 0 97201 2 0.1 0 Tota l Chromiu m (Cr

) u g 1.01 17. 7 19. 8 29. 0 55. 8 0.30 97201 2 0.3 0 Total'Lea d (Pb) u g . 2.70 23. 9 . . 24. 1 22. 3 40. 6 0.20 97201 2 0.2 0 N D = No t detected RD L = Reportabl e Detectio n Limit Q C Batc h = Qualit

yContro l Batc h

Pag e 4 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-817-570 0 Tol l frae.800-563-626 6 Fax:905-817-577 7Driven by service and Science \Tww.maxxamaual}*tic5.co m ENS R Internationa l Clien tProject* : 10002-017-01 7 Projec tname : ONY X Sample rInitials : 

### MERCUR YBYCOL D VAPOU R A A(IMPINGER SOLUTION) Maxxam I D L9982 8 L9982 9 L9982 9 Samplin g Date 2006705/1 0 2006/05/1 0 2006/05/1 0

Unit s U3-M29-R B RD L U3-W29-R 1 U3-M29-R 1 Lab-Du p RD L Batc h MD L
Tota l Mercury-2 B u g N D 0. 3 74. 7 75. 4 1. 6 97009 1 0.0 1 Tota l Mercury-3A u g N D 0.01 3.38 3.40 0.1 3 97004 5 0.05 Tota l Mercury-3 B u g 0.0 4 0.0

2 10. 7 10. 7 0. 5 970066 0.0 5 Tota l Mercury~3C u g N D 0.0 5 8.55 8.58 0.25 97132 2 0.0 5 N D = No

t detected RD L = Reportabl e Detectio n Limit Q C Batc h = Qualit

yContro l Batc h 

## T4 

# •I-' - IM f Analytic * in c Maxxam , Jo b #:A64446 9 Repor tDate : 2006705/2 0

Maxxa m ID L9983 0 L9983 1 Samplin g Date 2006/05/1 0 2006705/1 0

Units U3-M29-R 2 3D L U3-M29-R 3 . i 3iw»'!»i:Raiimt M Tota l Mercury-2 B u g 10 4 1.

7 78. 6 1. 5 97009 1 0.0 1 Tota l Mercury-3 A u g 1.29 0.0 2 1.2

6 0.0

2 970045 0.0

5 Tota l Mercury-3 B u g 7.9 9 0.25 1.5 6 0.0

5 970066 0.0

5 Tota l Mercury-3 C u g 7.95 0.25 7.7 0 0.25 97132 2 0.0 5 RD L = Reportabl e Detectio n Limit Q C Batc h = Qualit

yContro l Batc h

Pag e 5 o f1 1 674 0 Campobell o Road
. Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-317-570 0 Tol l free:800-563-626 6 Fax : 905-31.7-577 7Driven by service and Science >vww.niaxxa.manalyt f cs.co m ENS R Internationa l Clien tProject* ; 10002-017-01 7 Projec tname : ONY X Sample rInitials : 

### Tes tSummary
Maxxa m 1 0 Sampl e I D Matri x L99828 U3-M29-R B Filte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinger ) b vCVA A CVA A 97132 2 2006/05/1 6 2006/05/1 8 FF S Mercur y3 Ai n Ai r(HN0 3 Rinse) bvCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 FF S Mercur y2 B i n Air(HNO3/H20 2 Imp ) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 FF S Mercur y3 B i n Ai r( KMn04/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 . FF S Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 FF S Metal s i n Ai r(Combined ) b vICP/M S 1CP1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R Maxxa m I D Sampl e I D Matri x L99829 U3-M29-R 1 Filte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinger ) b vCVA A CVA A 971.32 2 2006/05/1 6 2006/05/1 8 FF S Mercur y3 AI n Ai r(HN0 3 Rinse) b vCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 FF S . Mercur y2 B In AWHNO3/H20 2 Imp ) b yCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 •FF S Mercur y3 B i n Ai r(KMnO4/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 FF S Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 v. . FF S Metal s " m Ai r(Combined ) b

vICP/M S ICP1/M S 97201 2 2006/05/1 7 •2006/05/1 9 • N R Maxxa m I D Sampl e I D Matri x L99829Du p U3-M29-R 1 Filte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C In Ai r(HC I Implnqer ) b vCVA A CVA A 97132 2 2006/05/1 6 2006/05/1 8 FF S Mercur y3 AI n Ai r(HN0 3 Rinse) b

vCVA A CVA A 970045 2006/05/1 5 2006/05/1 6 •FF S Mercur y2 B i n AiKHN03/H20 2 Imp ) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 FF S •' Mercur y3 B i n Ai r(KMn04/H2S04 ) bvCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 " FF S Mercur y1 B -Ai r(Filter+Acetone ) b yCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 FF S Metal s i n Ai r(Combined ) b vICP/M S ICP1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R Maxxa m I D Sampl e I D Matri x L99830 U3-M29-R 2 Fitte r Collecte d Shippe d Receive d 2006/05/1 0

2006/05/1 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I impinqer ) b vCVA A CVA A 97132 2 2006/05/1 6 2006/05/1 8 FF S Mercur y3 Ai n Ai r(HN0 3 Rinse) b vCVA A CVA A 970045 2006/05/1 5 2006/05/1 6 FF S Mercur y2 B i n AWHN03/H20 2 Imp ) b vCV A CVA A 97009 1 2006/05/1 6 2006/05/1 6 FF S Mercur y3 B i n Ai r(KMnO4/H2S04 ) b vCV A CVA A 97006 6 2006/05/1 5 2006/05/1 6 FF S Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 97239 5 2006/05/1 7 2006/05/1 8 FF S Metal s i n Ai r(Combined ) b vICP/M S ICP1/M S 97201 2 2006/05/1 7 2006/05/1 9 N R

Pag e 6 o

f1 1 674 0 Camppfaeli o Road , Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-817-570 0 Tol l free;800-563-626 6 Fax:905-817-577 7 

# IV S a rT 1

' Analytic s I r Maxxa m Jo b # : A64446 9 Repor tDate : 2006/05/2 0. . • Driven by service and Science xvww.maxxamanalytics.co m ENS R Internationa l Clien tProjec

t# : 10002-017-01 7 Projec tname : ONY X Sample rInitials : Tes t Summar

y
Maxxa m I D L9983 1 Collecte d 2006/05/1 0 Sampl e I D U3-M29-R 3 Shippe d Matri x Filte r Receive d 2006/05/1 2 Tes t Descriptio n Instrumentatio n Batc h ' Prepare d Analyze d Analys t Mercur y3 C i n Ai r(HC I Impinger ) b yCVA A CVA A 971322 ' 2006/05/1 6 2006/05/1 8 FF S Mercur y3 Ai n Ai r(HN0 3 Rinse ) b yCVA A CVA A 97004 5 2006/05/1 5 2006/05/1 6 FF S Mercur y2 B I n AMHN03/H20 2 Imp ) b vCV A CVA A 97009 1 ' 2006/05/1 6 2006/05/1 6 FF S Mercur y3 B i n Ai r(KMn04/H2SD4 ) b yCV A CVA A 970066 . 2006/05/1 5 2006/05/1 6 FF S Mercur y1 B -Ai r(Filter+Acetone ) b vCVA A CVA A 972395 ' 2006/05/1 7 2006/05/1 8 FF S Metal s In Ai r(Combined ) bv.lCP/M S ICP1/M S 972012 . 2006/05/1 7 2006/05/1 9 N R

Page7o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7 

### tV I a t j^y^si m Maxxa m Jo b #:A64446 9 Repor tDate : 2006705/2 0

# IV! Si £>rivert h}- service and

Science Maxxa m Jo b #:A64446 9 Repor tDate : 2006/05/2 0 wwTv.m axx a manalytlcs.co

m ENS R Internationa l Clien tProjec

tft 10002-017-01 7 Projec tname : ONY X Sample rInitials :

GENERA L COMMENT S ICPMS : Post digestio n duplicat e an d spik

e o n sampl e L9982 9 Result s relat e onl yto th e item s tested .

Pag e 8 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax
. 905-817-577 7

## IN

/I . 

# a 

# x5^ a m

ff. tr

### y*

Anaty:i< « m c www.masxamanalytic3.co m Driven by service mid Science ENS R Internationa l Attention : JeffGorma n Clien tProject* : 10002-017-01 7 P.O.# : Projec tname : ONY X Qualit yAssuranc e Repor t Maxxa m Jo b Number : GA64446 9 QA/Q C • Batc h Nu m Ini t QCTyp e Paramete r Date Analyze d WW/mm/d d Valu e "/oRecoveiY Units Q C Limit s MATRI XSPIK E (L99829 ) Tota l Mercury-3 A 2006/05/1 6 0.00 , RDL=0.1 3 10 2 u g 85 - 11 5 MATRI XSPIK E DU P (L99829

) Tota l Mercury-3 A 2006/05/1 6 0.00 , RDL=0.1 3 105 u g 85 - 11 5 Spike d Blan k

- Tota l Mercury-3 A 2006/05/1 6 0.11 , RDL=0.0 1 10 6 u g 90 - 11 0 Spike d Blan k

DU P Tota l Mercuty-3 A 2006/05/1 6 0.11,RDL=0.0 1 10 7 u g 90 - n a Method Blan k Tota l Mercury-3 A 2006/05/1 6 ND , RDL=0.0 1 u g RP D Tota l Mercury-3 A 2006/05/1 6 0. 6 % 2 0 MATRI XSPIK E (L99829 ) Tota l Mercury-3 B 2006/05/1 6 0.5 , RDL=0. 5 105 u g 85 - 11 5 MATRI XSPIK E DU P (L99829

) Tota l Meicury-3 B 2006/05/1 6 0.5 , RDL=0. 5 10 7 u g 85 - 11 5 Spike d Blan k Tota l Mercury-3 B 2006/05/1 6 0.55 , RDL=0.05 11 0 u g 90 - 11 0 Spike d Blan k

DU P Tota l Mercury-3 B 2006/05/1 6 0.54 , RDL=0.05 108 u g 90 - 11 0 Method Blan k Tota l Mercury-3 B 2006/05/1 6 ND , RDL=O.0 5 u g RP D Tota l Mercury-3 B 2006/05/1 6 0.0 5 % 2 0 MATRI XSPIK E (L99829 ) Tota l Mercury-2 B 2006/05/1 6 0.0,RDL=1. 6 10 0 u g 85 - 11 5 MATRI XSPIK E DU P (L99829

) Tota l Mercury-2 B 2006/05/1 6 0.0,RDL=1. 6 9 5 u g 85 - 11 5 Spike d Blan k Tota l Mercury-2 B 2006/05/1 6 0.11 , RDL=0.0 1 10 7 u g 90 - 11 0 Spike d Blan k

DU P Tota l Mercury-2 B 2006/05/1 6 0.11,RDL=0.0 1 10 9 u g 90 - 11 0 Method Blan k Tota l Mercury-2 B 2006/05/1 6 ND , RDL=0.0 1 u g RP D Tota l Mercury-2 B 2006/05/1 6 0. 9 % 2 0 MATRI XSPIK E (L99829 ) Tota l Mercury-3 C 2006/05/1 8 0.54 , RDL=0.2 5 10 8 u g 85 - 11 5 MATRI XSPIK E DU P (L99829

) Tota l Mercury-3 C 2006/05/1 8 0.54 , RDL=0.2 5 10 8 u g 85 - •115 ; Spike d Blan k Tota l Mercury-3 C 2006/05/1 8 0.51 , RDL=0.05 102 ug - 90 - •11 0 Spike d Blan k

DU P Tota l Mercury-3 C 2006/05/1 8 0.52 , RDL=0.05 10 3 ug - 90 - •11 0 Method Blan k Tota l Meroury-3 C 2006/05/1 8 ND , RDL=0.05 " 9 RP D Tota l Mercury-3 C 2006/05/1 8 0.4 % 20 MATRI XSPIK E (L99829 ) Tota l Arseni c (As) 2006/05/1 9 49.5 , RDL=0.4 0 9 9 u g 70 - •13 0 MATRI XSPIK E DU P (L99829

) Tota l Arseni c (As) 2006/05/1 9 49.5 , RDL=0.40 9 9 u g 70 -•13 0 MATRI XSPIK E (L99829 ) Tota l Berylliu m (Be ) 2006/05/1 9 44.5 . RDL=0.1 0 8 9 u g 70 - -13 0 MATRI XSPIK E DU P (L99829

) Tota l Berylliu m (Be) 2006/05/1 9 45.5 , RDL=0.1 0 9 1 u g 70 -13 0 MATRI XSPIK E (L99829 ) Tota l Cadmiu m (Cd ) 2006705/1 9 26.0 , RDL=0.1 0 10 4 u g 70 - -13 0 MATRI XSPIK E DU P (L99829

) Tota l Cadmiu m (Cd ) 2006/05/1 9 26.3 , RDL=0.1 0 10 5 u g 70 --13 © MATRI XSPIK E (L99829 ) Tota l Chromiu m (Cr ) 2006/05/1 9 52.5 , RDL=0.3 0 10 5 u g 70 -13 0 MATRI XSPIK E DU P (L99829

) Tota l Chromiu m (Cr ) 2006/05/1 9 51.5 , RDL=0.3 0 103 u g 70 -13 0 MATRI XSPIK E (L99829) Tota l Lea d (Pb ) 2006/05/1 9 50.5 , RDL=0.2 0 101 u g 7 0 -13 0 MATRI XSPIK E DU P (L99829

) Tota l Lea d (Pb) 2006/05/1 9 50.5 , RDL=0.2 0 101 u g 7 0 -13 0 Spike d Blan k Tota l Arseni c (As ) 2006/05/1 9 51.5 , RDL=0.40 10 3 u g 85 -11 5 Spike d Blan k

DU P Tota l Arseni c (As ) 2006705/1 9 51.5 , RDL=0.40 10 3 u g 8 5 -11 5 Spike d Blan k Tota l Berylliu m (Be ) 2006705/1 9 47.0 . RDL=0.1 0 9 4 u g 85 -11 5 Spike d Blan k

DU P Tota l Berylliu m (Be ) 2006/05/1 9 47.0 , RDL=0.1 0 94 u g 85 -11 5 970045 FF S

97006 6 FF S

97009 1 FF S

97132 2 FF S

97201 2 N R

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# M a
'^^ ^ Anoly t 

# m www.maxx a manalytics-co

m 'Driven by service and Science fcNSR internationa l Attention : Jef fGorma n Clien tProjec

t# : 10002-017-01 7 P.O
. # : Projec tname : ONY X Qualit yAssuranc e Repor t (Continued ) Maxxa m Jo b Numbe rGA64446 9 QA/Q C Batc h Nu m Ini t QCTvp e Paramete r Date Analyze d ww /mm/d d Valu e % Recover y Units Q C Limits 97201 2 N_ R Spike d Blan k Tota l Cadmiu m (Cd ) 2006/05/1 9 25.8 , RDL=0.1 0 103 u g 85 - 11 5 Spike d Blan k

DU P Tota l Cadmiu m (Cd ) 2006/05/1 9 25.8 , RDL=0.1 0 103 u g 85 - 11 5 Spike d Blan k

Tota l Chromiu m (Cr ) 2006/05/1 9 53.0 , RDL=0.3 0 106 u g 85 - 11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/05/1 9 53.5 , RDL=0.3 0 10 7 u g 85 - 11 5 Spike d Blan k

Tota l Lea d (Pb) •2006/05/1 9 51.0 , RDL=0.2 0 10 2 u g 85 - 11 5 Spike d Blan k

DU P Tota l Lea d (Pb) 2006/05/1 9 52.0 , RDL=0.2 0 10 4 u g 85 - 11 5 * Metho d Blan k Tota l Arseni c (As) 2006/05/1 9 ND , RDL=0.40 u g Metho d Blan k

DU P Tota l Arseni c (As) 2006/05/1 9 ND , RDL=0.40 u g Metho d Blan k

Tota l Berylliu m (Be ) 2006/05/1 9 ND . RDL=0.1 0 . u g Metho d Blan k

DU P Tota l Berylliu m (Be ) ' 2006/05/1 9 ND . RDL=0.1 0 u g Metho d Blan k

Tota l Cadmiu m (Cd ) 2006705/1 9 ND , RDL=0.1 0 u g Metho d Blan k

DU P Tota l Cadmiu m (Cd ) 2006/05/1 9 ND , RDL=0.1 0 u g Method Blan k

Tota l Chromiu m (Cr ) 2006705/1 9 ND , RDL=0.3 0 u g Metho d Blan k

DU P Tota l Chromiu m (Cr ) 2006/05/1 9 ND , RDL=0.3 0
. u g Metho d Blan k

Tota l Lea d (Pb ) 2006/05/1 9 ND , RDL=0.2 0 u g Method Blan k

DU P Tota l Lea d (Pb) 2006/05/1 9 ND , RDL=0.2 0 u g RP D Tota l Arseni c (As) 2006/05/1 9 3. 5 % 2 0

Tota l Berylliu m (Be

) 2006/05/1 9 N C % 2 0 Tota l Cadmiu m (Cd ) 2006/05/1 9 3. 9 % 2 0 Tota l Chromiu m (Cr

) 2006/05/1 9 11. 2 % 2 0 Tota l Lea d (Pb) 2006/05/1 9 0. 7 % 2 0 972395 FF S • MATRI XSPIK E

(L99829 ) Tota l Mercury-1 B 2006/05/1 8 0.30 . RDL=0.03 9 9 u g . 85 - 11 5 MATRI XSPIK E DU P (L99329

) Tota l Mercury- 1 B 2006/05/1 8 0.30 , RDL=0.03 10 0 u g 85 - 11 5 Spike d Blan k

: Tota l Mercury- 1 B 2006/05/1 8 0.31,RDL=0.0 3 10 3 u g 90 - 11 0 Spike d Blan k

DU P Tota l Mercury- 1 B 2006/05/1 8 0.31,RDL=0.0 3 10 3 u g 90 - 11 0 Method Blan k

Tota l Mercury- 1 B 2006/05/1 8 ND , RDL=0.03 u g RP D Tota l Mercurv-1 B 2006/05/1 8 N C % 2 0 N D = No t detecte d N C = Non-calculabl e RP D = Relativ

e Percen t Difference SPIK E = Fortified sampi e

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. Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7

### S I 

## yCyC

S i m Driven by service ana Science Anoiytic i in c www.maxxamanaIytlcs.coi n 

### Validatio n Signature Paq e Maxxa m Jo b # : A64446 9

Th eanalytica

l dat aan d al l Q C containe

d i nthi s repor twer e reviewed an

d validate d b y th efollowin

gindividuals) .

FRAN KMO , B.Sc , Inorgani cLab. Manage

r

Maxxa m ha s procedure

s i nplac e to guar d agains timprope

rus eo f th eelectroni

csignatur

e an d hav e th erequire d "signatories" , a

s pe rsectio n5.10. 2 o f ISO/IE C 1702S:2005(E) , signin gth ereports . SC C an

d CAEA L hav

e approve

d thi s reportingproces

s an d electroni

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t

Pag e 1 1 o f 1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-S70 0 Tol l free:800-563-626 6 Fax:905-817-577 7

### Sectio nI : Sampl

eInventor

y Repor t Dat e Received : Projec tNo. : Projec tName: 6/22/200 6 2780 3 10002-01

7

Lab . Sampl eID Clien tSampleI D ComponentID 001 00 2 00 3 00 4 00 5 00 6 00 7 U3-M23A-XAD-R 1 U3-M23A-PF-R 1 U3-M23A-XAD-R 2 U3-M23A-PF-R 2 U3-M23A-XAD-R 3 U3-M23A-PF-R3 U3-M23A-XAD-F B B HACE/MeC12/TO L XA D F HACE/MeC12/TO L FILTE R B HACE/MeC12/TO L XA D F HACE/MeC12/TO L FILTE R B HACE/MeC12/TO L XA D F HACE/MeC12/TO L FILTE R BH/F HACE/MeC12/TO L FILTE R XA D

Projec t2780 3 SmpinvgnmmS.rpt

Projec t2 o f 46 6

## SECTIO N n

Projec t2780 3 Projec t3 cMetho d

### Blan k Metho d 0023 A Matrix : MM 5 Q C Batc h No. : 812

0 La

b Sample : 0-MB00 1 Sampl e Size : Sampl

e Dat e Extracted : 22-Jun-0 6 Dat

e Analyzed DB-5 : 26-Jun-0 6 Dat

e Analyze d DB-225 : N A AnalyteCone . (pg/Sample) D L aEMP C Qualifier s Labele d Standard % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 0.87 9 IS 13C-2,3,7,8-TCD D 93.8 40-13 5 1,2,3,7,8-PeCDD N D 0.80 2 13C-l,2,3,7,8-PeCD D 88. 8 40-13 5 1,2,3,4,7,8-HxCDD N D 1.6 9 13C-l,2,3,6,7,8-HxCD D 85. 3 40-13 5 1,2,3,6,7,8-HxCDD N D 1.4 3 13C-l,2,3,4,6,7,8-HpCD D 77. 3 40-13 5 1,2,3,7,8,9-HxCDD N D 1.5 5 13C-OCD D 59. 8 40-13 5 1,2,3,4,6,7,8-HpCDD N D 1.8 2 13C-2,3,7,8-TCD F 82.1 40-13 5 OCD D N D 6.9 5 13C-l,2,3,7,8-PeCD F 77.9 40-13 5 2,3,7,8-TCD F N D 1.0 8 13C-l,2,3,6,7,8-HxCD F 95. 9 40-13 5 1,2,3,7,8-PeCDF N D 1.4 5 13C-l,2,3,4,6,7,8-HpCD F 79. 6 40-13 5 2,3,4,7,8-PeCDF N D 1.3 3 13C-OCD F 23. 2 40 - 13

5 H 1,2,3,4,7,8-HxCDF N D 0.58 7 PS 37Cl-2,3,7,8-TCD D 10 1 7

0 - 13 0 1,2,3,6,7,8-HxCDF N D 0.46 9 13C-2,3,4,7,8-PeCDF 99. 6 7

0 - 13 0 2,3,4,6,7,8-HxCD F N D 0.55 2 13C-l,2,3,4,7,8-HxCD D 95. 2 70-13 0 1,2,3,7,8,9-HxCDF N D 0.70 7 13C-l,2,3,4,7,8-HxCD F 88. 0 7

0 - 13 0 l^Aej^HpCD F 0.38 6 13C-l,2,3,4,7,8,9-HpCD F 73.1 70-13 0 i,2,3,4,7,8,9-HpCD F N D 0.84 6 A S 13C-l,2,3,7,8,9-HxCD F 83. 3 40-13 5 OCD F N D 7.4 6 Total s Toxi cEquivalentQuotient(TEQ ) Data e Tota l TCD D N D 0.87 9 TE Q (Min-Max) : 0.00386-2.87 Tota l PeCD D N D 0.66 9 Tota l HxCD D N D 1.5 5 a . Sampl especificestimate

d detectio

nlimit. Tota l HpCD D N D 1.8 2 b. Estimate d maximu

m possibl

e concentration. ; Tota l TCD F N D 1.0 8 c . Method detectio

nlimit. Tota l PeCD F N D 1.3 9 d . Lowercontro l limit - uppe

rcontro l limit. ; r Tota l HxCD F N D 0.56 6 e . TE Q base

d o n(1989 ) Internationa

l Toxi cEquivalen

tFactor s (1TEF) . Tota l HpCD F 0.38 6 Analyst : RA S Approved By : William J . Luksembur g 27-Jun-200

6 15:1 1 Projec t2780 3 Projec t4 o f 46 6OP RResult s 

### Method 0023 A
Matrix : MM 5 Q C Batch No. : 812 0 Lab Sample : 0-OPR00 1 SampleSize : Sampl e Dat e Extracted : 22-Jun-0 6 Dat

e Analyzed DB-5 : 26-Jun-0 6 Dat

e Analyzed DB-225 : N A Analyte Spike Cone . Cone . (ng/mL ) OP RLimits Labele d Standard % R LCL-UC L 2,3,7,8-TCD D 2.5 0 2.4

8 1.75-3.25 I S 13C-2,3,7,8-TCD D 84. 5 40-13 5 1,2,3,7,8-PeCDD 12. 5 12.

6 8.7

5 -16.25 13C-l,2,3,7,8-PeCD D 82. 3 40-13 5 1,2,3,4,7,8-HxCDD 12. 8 8.7

5 - 16.2 5 13C-l,2,3,6,7,8-HxCD D 79. 1 4 0 -13 5 1,2,3,6,7,8-HxCDD 12. 5 14.

0 8.75-16.25 13C-1,2,3,4,6,7,8-HpCDD 77. 4 40-13 5 1,2,3,7,8,9-HxCDD 14. 0 8.75-16.25 13C-OCD D 62. 9 40-13 5 1,2,3,4,6,7,8-HpCDD 12. 5 12.

0 8.7

5 - 16.2 5 13C-2,3,7,8-TCD F 78. 1 40-13 5 OCD D 25. 0 17.5-32. 5 13C-l,2,3,7,8-PeCD F 75. 4 40-13 5 2,3,7,8-TCD F 2.5 0 2.4

0 1.75-3.25 13C-l,2,3,6,7,8-HxCD F 83. 5 40-13 5 1,2,3,7,8-PeCDF 12. 5 12.

5 8.75-16.25 13C-l,2,3,4,6,7,8-HpCD F 78. 7 40-13 5 2,3,4,7,8-PeCDF 12. 5 11.

8 8.75-16.25 13C-OCD F 27. 2 40-13 5 1,2,3,4,7,8-HxCDF ; .-s;. . - 12.5r/; 12. 3 8.75-16.25 A S 13C-l,2,3,7,8,9-HxCD F 90. 7 40 - 13

5 1,2,3,6,7,8-HxCDF 12. 5 13.

9 8.75-16.25 2,3,4,6,7,8-HxCD F 12. 5 13.

6 8.7

5 - 16.2 5 1,2,3,7,8,9-HxCDF 12. 5 12.

9 8.75-16.25 1,2,3,4,6,7,8-HpCDF i2;§'.: : , ;: . 8.7 5 - 16.2 5 1,2,3,4,7,8,9-HpCDF 12. 5 8.9

2 8.75 - 16.2 5 OCD F 25. 0 24.

7 17.5-32. 5
Analyst : RA S ApprovedBy : William J . Luksembur g 27-Jun-200

6 15:1 1

Projec t2780 3 Projec t5 of 46 6SamplelD : 

## TJ3-M23A-XAD--R 1 Metho d 0023 A Clien tData Sampl e Data Laborator y Data Name : ENS R Project : 10002 -01 7 Dat e Collected : 19-Jun-0 6 TimeCollected : Matrix : Sample Size : MM 5

Sampl e La b Sample : 27803-001

Q C Batc h No. : 812 0 Dat eAnalyzed DB-5 : 26-Jun-0 6 Dat

e Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Date s Analyzed DB-225 : 27-Jun-0 6 Analyte Cone . (pg/Sample) D L a EMPC b Qualifier s Labele d Standard % R LCL-UCL dQualifier s 2 ,3,7,8-TCD D N D ••• 3 6 4 I S 13C-2,3,7,8-TCD D 91. 6 40-13 5 1,2,3,7,8-PeCDD 17
. 0 J 13C-l,2,3,7,8-PeCD D 88. 7 40 - 13

5 1,2,3,4,7,8-HxCDD 19.1 J 13C-l,2,3,6,7,8-HxCD D 89. 2 40-13 5 1,2,3,6,7,8-HxCDD 46. 1 J 13C-l,2,3,4,6,7,8-HpCD D 96. 7 40-13 5 1 ,2,3,7,8,9-HxCDD 37.0 J 13C-OCD D 10 5 40-13 5 1,2 ,3,4,6,7,8-HpCDD 19 0 13C-2,3,7,8-TCD F 88. 3 40-13 5 OCD D 23 6 13C-l,2,3,7,8-PeCD F 80. 4 40-13 5 2 ,3,7,8-TCD F 29. 5 13C-l,2,3,6,7,8-HxCD F 97.0 40-13 5 1,2,3,7,8-PcCDF 35. 5 J 13C-l,2,3,4,6,7,8-HpCD F 92. 7 40-13 5 2 ,3,4,7,8-PeCD F 65. 4 13C-OCD F 83. 4 40-13 5 1 ,2,3,4,7,8-HxCD F 36.0 J £ S 37Cl-2,3,7,8-TCD D 86.1 70-13 0 1 ,2 ,3,6,7,8-HxCD F 31. 9 J,D 13C-2,3,4,7,8-PeCDF 91. 4 70 - 13

0 2,3,4,6,7,8-HxCD F 43.8 13C-l,2,3,4,7,8-HxCD D 85. 7 7 0 -13 0 1 ,2 ,3,7,8,9-HxCD F 10. 3 J 13C-l,2,3,4,7,8-HxCD F 85. 9 7 0 - 13 0 1,2,3,4,6,7,8-HpCDF 78. 1 B 13C-l,2,3,4,7,8,9-HpCD F 7 7 9 7 0 - 13 0 1 ,2 ,3,4,7,8,9-IIpCDF 8.10 J M 13 C-I ,2,3,7,8,9- H X CD F 95. 2 40 - 13

5 OCD F 20. 4 J Total s Toxi cEquivalentQuotient(TEQ ) Dat a e Tota l TCD D 118 0 TE Q (Min-Max) : 71. 4 - 75.0 Tota l PeCD D 86 9 Tota l HxCD D 147 0 a . Sampl e specificestimate

d detectio

nlimit. Tota l HpCD D Mi2 ::;:-; :; ''; ; 2;f' b . Estimate d maximu

m possibl

e concentration : Tota l TCD F 108 0 c. Method detectio nlimit. Tota l PeCD F 80 0 D d . Lowe rcontro l limi t- uppe rcontro l limit. Tota l HxCD F 39 1 39 5 D e . TE Q base

d o n(1989 ) tnternationa

l Toxi cEquivalen

tFactor s (ITEF) . Tota l HpCD F 11 2 : B Analyst : RA S Approve d By : William J . Luksembur g27-Jun-200

6 15:11 Projec t2780 3 Projec t6 o f 46 6SamplelD : 

## U3-M23A-PF-R1 Metho d 0023 A Clien tData Sampl e Dat a Laborator y Dat a Name : ENS R Project : 10002-01 7 Dat e Collected : 19-Jun-0 6 Tim eCollected : Matrix : Sample Size : MM 5

Sampl e Lab Sample : 27803-00 2 Q C Batc h No. : 812 0 Dat eAnalyzed DB-5 : 26-Jun-0 6 Dat

e Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Dat e Analyzed DB-225 : N A Analyte Cone . (pg/Sample) D L a EMPC b Qualifier s Labele d Standard % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 1 1 8 I S 13C-2,3,7,8-TCD D 91. 5 4 0 - 13 5 1,2,3,7,8-PeCDD N D 1.3 8 13C-l,2,3,7,8-PeCD D 92. 8 40-13 5 1,2,3,4,7,8-HxCDD N D 2.7 6 13C-l,2,3,6,7,8-HxCD D 89. 4 4 0 - 13 5 1,2,3,6,7,8-HxCDD N D 2.3 3 13C-1,2,3,4,6,7,8-HpCDD 83.1 40-13 5 1,2,3,7,8,9-HxCDD N D 2.5 3 I3C-OCD D 86. 7 40-13 5 1,2,3,4,6,7,8-HpCDD N D 2.5 2 13C-2,3,7,8-TCD F 85. 3 40-13 5 OCD D 10. 8 J 13C-l,2,3,7,8-PeCD F 82. 3 40-13 5 2,3,7,8-TCD F N D 1.2 7 13C-l,2,3,6,7,8-HxCD F 97. 8 40-13 5 1,2,3,7,8-PcCDF N D 1.5 1 13C-l,2,3,4,6,7,8-HpCD F 80. 9 40-13 5 2,3,4,7,8-PeCDF N D 1.3 8 13C-OCD F 69.1 40-13 5 1,2,3,4,7,8- 1 IxCD F N D 0 92 3 £ S 37Cl-2,3,7,8-TCD D 94. 4 70 - 13

0 1,2,3,6,7,8-HxCDF N D 0.73 7 13C-2,3,4,7,8-PeCDF 93. 9 70-13 0 2,3,4,6,7,8-HxCD F N D 0.86 8 13C-l,2,3,4,7,8-HxCD D 90. 7 70-13 0 1,2,3,7,8,9-HxCDF N D 1.11 13C-l,2,3,4,7,8-HxCD F 87. 4 70-13 0 1,2,3,4,6,7,8-HpCDF N D 1.2 9 13C-l,2,3,4,7,8,9-HpCD F 79.0 70-13 0 1,2,3,4,7,8,9-HpCDF N D 1.11 A S 13C-l,2,3,7,8,9-HxCD F 93. 7 40-13 5 OCD F N D 5.0 2 Total s Toxi cEquivalentQuotient(TEQ ) Dat a e Tota l TCD D N D 1.1 8 TE Q (Min-Max) : 0.0108-3.9 5 Tota l PeCD D N D 1.3 8 Tota l HxCD D N D 3.3 4 a . Sampl e specificestimate

d detectio

nlimit. Tota l HpCD D • i-77 '.r - b. Estimate d maximu

m possibl

e concentration. Tota l TCD F N D 1.2 7 c . Metho d detectio

nlimit. Tota l PeCD F N D 1.4 4 d. Lowercontro l limit -. s uppe rcontro l limit. ; Tota l HxCD F N D 0.89 0 e . TE Q base

d o n(1989 ) Internationa

l Toxi cEquivalen

tFactor s (ITEF) . Tota l HpCD F N D 1.4 9 Analyst : RA S Approve dBy : William J . Luksembur g 27-Jun-200

6 15:11 Projec t2780 3 Projec t7 of 46 6Sampl e ID : 

### TJ3-M23A-XAD--R2 Metho d 0023 A Clien tDat a Sampl e Dat a Laborator yDat a Name : ENS R Project : 10002-01 7 Dat e Collected : 20-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : MM 5

Sampl e La b Sample : 27803-00 3 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 27-Jun-0 6 Date Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Date s Analyze d DB-225 : 27-Jun-0 6 Analyte Cone . (pg/Sample) D L a EMPC b Qualifier s Labele d Standard 

### % R LCL-UCL dQualifier s 2,3,7,8-TCD D 3.4 4 

### J I S 13C-2,3,7,8-TCD D 90. 7 40-13 5 1,2,3,7,8-PeCDD 17. 6 J 13C-l,2,3,7,8-PeCD D 96. 2 4 0 - 13 5 1,2,3,4,7,8-HxCDD 16. 8 J 13C-l,2,3,6,7,8-HxCD D 90. 0 40 - 13

5 1,2,3,6,7,8-IIxCDD 34. 7 J 13C-l,2,3,4,6,7,8-HpCD D 89.1 40-13 5 1,2,3,7,8,9-HxCDD 27. 1 J 13C-OCD D 88. 8 40-13 5 1,2,3,4,6,7,8-HpCDD 17 5 13C-2,3,7,8-TCD F 84. 8 40-13 5 OCD D 17 5 13C-l,2,3,7,8-PeCD F 91. 8 40-13 5 2,3,7,8-TCD F 32. 8 13C-l,2,3,6,7,8-HxCD F 96. 2 40-13 5 1,2,3,7,8-PcCDF 41. 2 J 13C-l,2,3,4,6,7,8-HpCD F 83. 0 4 0 -13 5 2,3,4,7,8-PeCDF 70. 2 13C-OCD F 59. 8 40 - 13

5 1,2,3,4,7,8-HxCDF 33.0 J P S 37Cl-2,3,7,8-TCD D 99. 4 70-13 0 1,2,3,6,7,8-HxCDF 31. 7 J,D 13C-2,3,4,7,8-PeCDF 89. 2 70-13 0 2,3,4,6,7,8-HxCD F 41.8 13C-l,2,3,4,7,8-HxCD D 92. 3 70-13 0 1,2,3,7,8,9-HxCDF 11. 6 J 13C-1,2,3,4,7,8-HxCDF 92. 3 7 0 - 13 0 1,2,3,4,6,7,8-HpCDF 66. 8 13C-l,2,3,4,7,8,9-HpCD F 83. 2 70-13 0 1,2,3,4,7,8,9-HpCDF 5.2 1 

### J A S 13C-1,2,3,7,8,9-HxCDF 99. 2 40-13 5 OCD F 14. 8 J Total s Toxi cEquivalentQuotient(TEQ ) Data e Tota l TCD D 121 0 TE Q (Min-Max) : 75. 0 - 75. 0 Tota l PeCD D 84 8 Tota l HxCD D 133 0 a . Sampl e specifi c estimate d detectio n limit . Tota l HpCD D 38

1 b. Estimated maximu m possibl e concentration . Tota l TCD F 135 0 c . Method detectio n limit . Tota l PeCD F 86

2 D d . Lowe rcontro l limi t - uppercontro l limit : : Tota l HxCD F 39 0 D c . TE Q base d o n (1989

) Internationa l Toxi c Equivalent Factor s (ITEF) . Tota l HpCD F ' 98.0 B Analyst : RA S Approve d By : WilliamJ . Luksembur g 27-Jun-200

6 15:1 1 Projec t2780 3 Projec t8 o f 46 6Sampl e ID : 

## U3^M23A-PF-R 2 Metho d 0023 A Clien t Dat a Sampl e Dat a Laborator yDat a Name : ENS R Project : 10002-01 7 Date Collected : 20-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : MM 5

Sampl e La b Sample : 27803-00 4 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 27-Jun-0 6 Dat

e Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Dat e Analyze d DB-225 : N A Analyte Cone . (pg/Sample) D L a EMPC b Qualifier s Labele d Standard % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 1.2 1 I S 13C-2,3,7,8-TCD D 95. 2 4 0 -13 5 1,2,3,7,8-PeCDD N D 3.2 6 13C-1,2,3,7,8-PeCDD 10 1 40-13 5 1,2,3,4,7,8-HxCDD ND 2 6 3 13C-l,2,3,6,7,8-HxCD D 94. 3 40-13 5 1,2,3,6,7,8-HxCDD N D 2.2 3 13C-1,2,3,4,6,7,8-HpCDD 83. 0 40-13 5 1,2,3,7,8,9-HxCDD N D 2.41 13C-OCD D 88. 2 40-13 5 1,2,3,4,6,7,8-HpCDD N D 4.12 13C-2,3,7,8-TCD F 92. 6 40-13 5 OCD D N D 6.3 3 13C-l,2,3,7,8-PeCD F 88. 9 4 0 - 13 5 2,3,7,8-TCD F N D 0.951 13C-l,2,3,6,7,8-HxCD F 10 1 40 - 13

5 1,2,3,7,8-PeCDF N D 3.4 4 13C-l,2,3,4,6,7,8-HpCD F 79. 5 40-13 5 2,3,4,7,8-PeCDF N D 3.14 13C-OCD F 61. 5 40-13 5 1,2,3,4,7,8-HxCDF N D 0.68 4 ? S 37Cl-2,3,7,8-TCD D 97. 5 7 0 - 13 0 1,2,3,6,7,8-HxCDF N D 0.54 6 13C-2,3,4,7,8-PeCDF 99. 4 70-13 0 2,3,4,6,7,8-HxCD F N D 0.64 3 13C-l,2,3,4,7,8-HxCD D 95.0 70-13 0 1,2,3,7,8,9-HxCDF N D 0.82 3 13C-1,2,3,4,7,8-HxCDF 88. 7 70 - 13

0 1,2,3,4,6,7,8-HpCDF N D 0.70 5 13C-l,2,3,4,7,8,9-HpCD F 7 9 4 70 - 13

0 1,2,3,4,7,8,9-HpCDF N D 0.971 A S 13C-1,2,3,7,8,9-HxCDF 92. 8 40-13 5 OCD F N D 6.3 8 Total s Toxi cEquivalentQuotient(TEQ ) Dat a e Tota l TCD D N D 1.2 1 TE Q (Min-Max) : 0-5.7 4 Tota l PeCD D N D 3.2 6 Tota l HxCD D N D 2.4 1 a . Sample specifi c estimate d detectio n limit . Tota l HpCD D N D 4 1 2 b. Estimate d maximu m possibl e concentration : : : Tota l TCD F N D 0.951 c . Method detectio n limit . Tota l PeCD F N D 3.2 8 d . Lowe rcontro l limi t - uppe rcontro l limit . •»•• : Tota l HxCD F N D 0.66 0 e . TE Q base d o n (1989

) Internationa l Toxi c Equivalen t Factor s (ITEF) . Tota l HpCD F N D 0.817 Analyst : RA S Approve d By : WilliamJ . Luksembur g 27-Jun-200

6 15:1 1 Projec t2780 3 Projec t9 o f 46 6Sampl e ID : 

### U3-M23A-XAD—R 3 Method 0023 A Clien t Dat a Sampl e Dat a Laborator yDat a Name : ENS R Project : 10002-01 7 Dat e Collected : 21-Jun-0 6 Tim e Collected : Matrix : Sampl e Size : MM 5

Sampl e La b Sample : 27803-00 5 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 27-Jun-0 6 Dat

e Received : 22-Jun-0 6 Date Extracted : 22-Jun-0 6 Date s Analyze d DB-22 5 : 27-Jun-0 6 Analyte Cone . (pg/SampIe ) D L a EMPC b Qualifier s Labele d Standard 

### % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 3.9 2 J

S 13C-2,3,7,8-TCD D 88. 3 40-13 5 1,2,3,7,8-PeCDD 16. 7 J 13C-1,2,3,7,8-PeCDD 94. 0 40-13 5 1,2,3,4,7,8-HxCDD 14. 6 J 13C-l,2,3,6,7,8-HxCD D 89. 7 4 0 - 13 5 1,2,3,6,7,8-HxCDD 35. 7 J 13C-l,2,3,4,6,7,8-HpCD D 95. 2 40-13 5 1,2,3,7,8,9-HxCDD 26. 3 J 13C-OCD D 95.9 40-13 5 1,2,3,4,6,7,8-HpCDD 15 6 13C-2,3,7,8-TCD F 86. 6 40-13 5 OCD D 14 1 13C-l,2,3,7,8-PeCD F 84. 3 40-13 5 2,3,7,8-TCD F 31. 8 13C-i;2,3,6,7,8-HxCD F 95. 9 40-13 5 1,2,3,7,8-PeCDF 41. 1 J 13C-l,2,3,4,6,7,8-HpCD F 9 0 8 40-13 5 2,3,4,7,8-PeCDF 76. 2 13C-OCD F 81. 0 40-13 5 1,2,3,4,7,8-HxCDF 

### ^37.8:'7:' V J P S 37Cl-2,3,7,8-TCD D 9 8 2 70-13 0 1,2,3,6,7,8-HxCDF 33.6 J, D 13C-2,3,4,7,8-PeCDF 97. 8 7 0 - 13 0 2,3,4,6,7,8-HxCD F 44.9 13C-l,2,3,4,7,8-HxCD D 92.9 70-13 0 1,2,3,7,8,9-HxCDF 11. 1 j 13C-1,2,3,4,7,8-HxCDF 90. 7 70 - 13

0 1,2,3,4,6,7,8-HpCDF 70. 7 B 13C-l,2,3,4,7,8,9-HpCD F 92. 5 70-13 0 1,2,3,4,7,8,9-HpCDF 7.1 5 J A S 13C-l,2,3,7,8,9-HxCD F 91. 1 40-13 5 OCD F 13. 2 . J ' Total s Toxi cEquivalen tQuotient(TEQ ) Dat a e Tota l TCD D 87 9 89 9 TE Q (Min-Max) : 74.6 - 78 . 5 Tota l PcCD D 68 6 Tota l HxCD D 111 0 a . Sample specifi c estimate d detectio n limit . Tota l HpCD D 33 5 b . Estimate d maximu m possibl e concentration . Tota l TCD F 131 0 c . Metho d detectio n limit . Tota l PeCD F 94

8 D d . Lowe rcontro l limit - uppercontro l limit: : Tota l HxCD F 410 D e . TE Q base

d on (1989

) Internationa l Toxi c Equivalen t Factor s (ITEF) . Tota l HpCD F 10 2 B Analyst : RA S Approve d By : WilliamJ . Luksembur g 27-Jun-200

6 15:11 Projec t2780 3 Projec t1 Q o f 46 6SamplelD : 

### U3-M23A-PF-R3 Metho d 0023 A Clien tDat a Sampl eDat a Laborator y Dat a Name : ENS R Project : 10002-01 7 Dat e Collected : 21-Jun-0 6 Tim eCollected : Matrix : Sampl eSize : MM 5

Sampl e La b Sample : 27803-00 6 Q C Batc h No. : 812 0 Dat eAnalyzed DB-5 : 27-Jun-0 6 Dat

e Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Dat e Analyze d DB-225 : N A Analyte Cone , (pg/Saraple ) D L a EMPC b Qualifier s Labele d Standard % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 1.4 0 I S 13C-2,3,7,8-TCD D 88. 4 40-13 5 1,2,3,7,8-PeCDD N D 3.8 3 13C-1,2,3,7,8-PeCDD 93. 9 40-13 5 1,2,3,4,7,8-HxCDD N D 2.1 3 I3C-l,2,3,6,7,8-HxCD D , 92. 5 40-13 5 1,2,3,6,7,8-HxCDD N D 1.8 1 13C-1,2,3,4,6,7,8-HpCDD 95. 6 40-13 5 1,2,3,7,8,9-HxCDD N D 1.9 6 13C-OCD D 94. 0 40-13 5 1,2,3,4,6,7,8-HpCDD N D 2.5 3 13C-2,3,7,8-TCD F 89. 7 40-13 5 OCD D 10.1 J 13C-l,2,3,7,8-PeCD F 84. 1 40-13 5 2,3,7,8-TCD F N D 1.1 5 13C-l,2,3,6,7,8-HxCD F 99. 3 40-13 5 1,2,3,7,8-PeCDF N D 3.0 0 13C-1,2,3,4,6,7,8-HpCDF 97. 3 4 0 -13 5 2,3,4,7,8-PeCDF N D 2.7 4 13C-OCD F 85. 9 40-13 5 1,2,3,4,7,8-HxCDF N D 0.641 P S 37Cl-2,3,7,8-TCD D 10 0 70-13 0 1,2,3,6,7,8-HxCDF N D 0.51 2 13C-2,3,4,7,8-PeCDF 10 4 70-13 0 2,3,4,6,7,8-HxCD F 0 60 3 13C-l,2,3,4,7,8-HxCD D 94. 3 70-13 0 1,2,3,7,8,9-HxCDF N D 0.771 13C-l,2,3,4,7,8-HxCD F 90. 4 70-13 0 1,2,3,4,6,7,8-HpCDF N D 0.819 13C-l,2,3,4,7,8,9-HpCD F 91. 8 70-13 0 1,2,3,4,7,8,9-HpCDF N D 0.60 2 A S 13C-l,2,3,7,8,9-HxCD F 99. 0 40-13 5 OCD F N D 3.8 4 Total s Toxi cEquivalentQuotient(TEQ ) Dat a e Tota l TCD D N D 1.4 0 TE Q (Min-Max) : 0.0101 - 5.8 5 Tota l PeCD D N D 3 8 3 Tota l HxCD D 3.3 5 a . Sampl especificestimate

d detectio

nlimit. Tota l HpCD D N D 2.5 3 b . Estimate d maximu

m possible concenlration. Tota l TCD F N D 1.1 5 c. Method detectio nlimit. Tota l PeCD F N D 2.8 6 d . Lowercontro l limi t- uppe rcontro l limit. Tota l HxCD F N D 0.618 e . TE Q base

d o n(1989 ) Internationa

l Toxi cEquivalen

tFactor s (ITEF) . Tota l HpCD F N D 0.95 0 Analyst : RA S Approve d By : WilliamJ . Luksembur g27-Jun-200

6 15:11 Projec t2780 3 Projec t11 o f 46 6

### SamplelD : U3-M23A-XAD—F B 

### Metho d 0023 A Clien tData Sampl e Dat a Laborator y Data Name : ENS R Project : 10002-01 7 Dat e Collected : 20-Jun-0 6 Tim eCollected : Matrix : Sample Size : MM 5 .

Sampl e La b Sample : 27803-00 7 Q C Batch No. : 812 0 Dat eAnalyzed DB-5 : 26-Jun-0 6 Dat

e Received : 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Dat e Analyze d DB-225 : N A Analyte Cone . (pg/SampIe ) D L a EMPC b Qualifier s Labele d Standard 

### % R LCL-UCL dQualifier s 2,3,7,8-TCD D N D 0.84 5 J S 13C-2,3,7,8-TCD D 88. 4 40-13 5 1,2,3,7,8-PeCDD N D 0.84 4 13C-l,2,3,7,8-PeCD D 89. 2 40-13 5 1,2,3,4,7,8-HxCDD N D 1.3 8 13C-l,2,3,6,7,8-HxCD D 93. 7 4 0 - 13 5 1,2,3,6,7,8-HxCDD N D 1.1 6 13C-1,2,3,4,6,7,8-HpCDD 80. 2 40 - 13

5 1,2,3,7,8,9-HxCDD N D 1.2 6 13C-OCD D 84. 5 40-13 5 1,2,3,4,6,7,8-HpCDD N D 1.4 2 13C-2,3,7,8-TCD F 85. 9 40-13 5 OCD D N D 4.2 9 13C-l,2,3,7,8-PeCD F 81. 7 40-13 5 2,3,7,8-TCD F N D 0.73 2 I 3 C-I ,2,3,6,7,8- HXCD F 96. 2 40-13 5 1,2,3,7,8-PcCDF N D ; 13C-1,2,3,4,6,7,8-HpCDF 81. 1 40-13 5 2,3,4,7,8-PeCDF N D 1.0 5 13C-OCD F 59. 9 40-13 5 1,2,3,4,7,8-HxCDF N D 0.401 E S 37Cl-2,3,7,8-TCD D 95. 3 7 0 - 13 0 1,2,3,6,7,8-HxCDF N D 0.32 0 13C-2,3,4,7,8-PeCDF 96. 5 70 - 13

0 2,3,4,6,7,8-HxCD F N D 0.37 7 13C-l,2,3,4,7,8-HxCD D 88.0 7 0 - 13 0 1,2,3,7,8,9-HxCDF N D 0.48 3 13C-l,2,3,4,7,8-HxCD F 90. 4 7 0 -13 0 1,2,3,4,6,7,8-HpCDF N D 0.66 6 13C-l,2,3,4,7,8,9-FIpCDF 76. 2 70-13 0 1,2,3,4,7,8,9-HpCDF N D 0.918 A S 13C-l,2,3,7,8,9-HxCD F 90. 6 40-13 5 OCD F N D 3.7 0 Total s Toxi cEquivalentQuotient(TEQ ) Dat a e Tota l TCD D N D 0.84 5 TE Q (Min-Max) : 0-2.5 0 Tota l PeCD D N D 0.84 4 Tota l HxCD D N D 1.2 6 a. Sampl e specifi cestimate

d detectio

nlimit. Tota l HpCD D N D 1 4 2 b. Estimate d maximu

m possible concentration. Tota l TCD F N D 0.73 2 c. Method detectio nlimit. Tota l PeCD F N D 1.1 0 d . Lowercontro l limi t- uppe rcontro l limit. Tota l HxCD F N D 0.38 7 e . TE Q base

d o n(1989 ) Internationa

l Toxi cEquivalen

tFactor s (ITEF) . Tota l HpCD F N D 0.77 2 Analyst : Approved By : William J . Luksembur g 27-Jun-200

6 15:1 1 Projec t2780 3 Projec t1 2 of 46 6PROJEC T NARRATIV E

Maxxam Analytics (BurlingtonON ) Maxxam Job #

: A662175 Client : ENS RInternationa l ClientProject : 10002-017-820 ONY X I . SAMPL E RECEIPT/ANALYSI S
a ) Sampl e Listing Maxxam 

### TD Clien t

Sample ID Dat e Sample d Dat

e Received Dat

e Prepped Dat

e Ru n Metals i nAi r(BackHalf ) vi aEP A Metho d 2

9 M7314 6 M29-RBB H2006/06/21 2006/06/2 2 M7314 7 M29-U3-R1B H2006/06/19 2006/06/2 2 M73147Dup M29-U3-R1B H2006/06/19 2006/06/2 2 M7314 8 M29-U3-R2B H2006/06/2 0 2006/06/2

2 M7314 9 M29-U3-R3B H2006/06/21 2006/06/2 2 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 2006/06/2

9 Metals i nAi r(Fron tHalf ) vi aEP A Metho d 2

9 M7314 2 M29-RBF H2006/0672 1 2006/06/2

2 2006/06/2

8 2006/06/2

9 M7314 3 M29-U3-R1F H2006/06/19 2006/06/2 2 2006/06/2

8 2006/06/2

9 M7314 3 Du p M29-U3-R 1 F H2006/06/19 2006/06/2 2 2006/06/2

8 2006/06/2

9 M7314 4 M29-U3-R2F H2006/06/2 0 2006/06/2

2 2006/06/2

8 2006/06/2

9 M7314 5 M29-U3-R3F H2006/06/2 1 2006/06/2 2 2006/06/2

8 2006/06/2

9 Particulates i nAi r(Aceton e Rinse) vi aEP A Metho d 5 M7314 2 M29-RBF H2006/06/21 2006/06/2 2 M7314 3 M29-U3-R1F H2006/06/19 2006/06/2 2 M7314 4 M29-U3-R2F H2006/06/2 0 2006/06/2

2 M7314 5 M29-U3-R3F H2006/06/21 2006/06/2 2 2006/06/2

7 2006/06/2

8 2006/06/2

7 2006/06/2

8 2006/06/2

7 2006/06/2

8 2006/06/2

7 2006/06/2

8 Particulates i nAi r(Filter) vi aEP A Metho d 5 ( M7314 2 M29-RBF H2006/06/21 2006/06/2 2 M7314 3 M29-U3-R1F H2006/06/19 2006/06/2 2 M7314 4 M29-U3-R2F H2006/06/2 0 2006/06/2

2 M7314 5 M29-U3-R3F H2006/06/21 2006/06/2 2 2006/06/2

6 2006/06/2

6 2006/06/2

6 2006/06/2

6 2006/06/2

6 2006/06/2

6 2006/06/2

6 2006/06/2

6 Ru nDat e is define

d a s ti e dat e o f injectio nof th e las tcalibratio

nstandar

d (1 2 hour s o rless ) priort o th e sample s analyze

d withi ntha tru nsequence

. Therefor

eth e tim e o f calibratio

ninjectio

ntha tdefine s th e ru ndat e is alway

s withi n1 2 hour s o f th e time o f sampl e injection. b) Shippin

gProblems : non

e encountere

d
c ) Documentatio

nProblems : non

e encountere

d H . SAMPL E PREP : N o problem

s encountere

dffl. SAMPL E ANALYSIS :

Se e als o comment

s withinth

eappropriat

eCertificat

eo f Analysis
a ) Hol d Times : all withinrecommende d hol d times b ) Instrumen

tCalibration : all withi

ncontro l limit s
c ) Qualit y Control : Al l applicabl eQ C meet

s contro l criteria , excep twher e otherwis

e noted. I certif y tha tthi s dat apackag e is i ncomplianc

ewit h th eterm s an d condition

s ofth e contract

, bot h technicall y an d fo rothe

rtha nth econdition

s detaile d above . I naddition

, I certify , tha

tt o th ebes to f my knowledg

e an d belief , th e dat aa s reporte d ar etru ean d accurate . Releas e ofth e dat

acontaine

d i nthi s dat apackag e ha s bee nauthorize

d b y th e cognizan

t laborator y officia l orhis/he

rdesignee

, a s verified by thi

s signature

. 

# JU

L 0 S 200

6 Mary-Ann

eJohnson

, Projec tManage

r Dat e

r

# 2 . DAT ASUMMAR Y Certificat e o fAnalysi s -
Sampl e analyt e resul t Metho d blan kresul t LC S Reisult

s wit h % Recoverie

s Matri xSpik e dat awit h % Recoverie

s Matri xSpik e Duplicat

e dat awit h % Recoverie

s Surrogat e recoverie

sClien t

La b numbe rIssue d
Supplie rP/ N Lot #

FilterDimension

s

Dat e o f Dessicatio

n(yyyymmd

d hh:mm

) 

### fe

Filterpr eweigh taverag e
Weigh tof filte rbefor e (g ) # 1

Initia l Dat e weighe d (yyyymrnd

d hh:mm

) 

# I I Weigh to f filterbefor

e (g ) # 2 

### 1 i Fina l Daleweighe

d (yyyymmd

d hh:mm

)

O O O 

## s - s - fr % Acceptabilit y
PgP Weigh ! o f filterdifferenc

e

Initia l Temperatur

e(14. 4 t o 25.6 C )

Initia l Humidit

y (% )0.0000 Initia l Balanc eZer o0.3000 Initia l 0.300 0 gram s

( O o Fina l Tem p (14. 4 t o 25. 6 < 3 de gchange )

Fina l Humidit

y (% ) (< 5 % change

)

k > Chang

ei nTemperatur

e(C )

o Chang

ei nHumidit

y (% )0.0000 Fina l Balanc eZer o0.3000 Fina l 0.300 0 grams .

# IS/

I 

# a xx a 

# m ly riven by service and Science www.m

a xx a inanaly tics.c

o m YourProjec

t# : 10002-017-82

0 Site : ONY X
Attention : Jef

f Gorman ENS RInternationa

l 6601 KirkvilleRd Eas tSyracuse

, N Y US A 1305

7 Repor tDate : 2006/09/1 1 

### CERTIFICAT E O F ANALYSIS MAXXA M JO B #

: A66217 5 Received : 2006/06/22,13:5 0 Sampl eMatrix : Filter #Sample

s Received : 4 Dat e Dat

e Method Analyse s Quantit y Extracte

d Analyzed Laborator y Metho d Referenc

e Metal s inAi r(Fron

tHalf ) b y ICP/M S <S 4 2006/06/2 8 2006/06/2

9 SOPIN G 108/10

9 EP A SW846-602 0 Particulate

s inAi r(Aceton

e Rinse ) (M5) ( P 4 2006/06/2 7 2006/06/2

8 SO PIN G 50

5 EP A CF RPT M 5 Particulate

s inAi r(Filter

) < 5 4 2006/06/2 6 2006/06/2

6 SOPIN G 50

5 EP A CF RPT M 5 Final Volumeo f

Aceton eProb eRins e$ 4 2006/09/1 1 2006/09/1 1 Sampl eMatrix : Impinge

rSolutio n #Sample

s Received : 4 Dat e Dat

e Method Analyse s Quantit y Extracte

d Analyzed Laborator y Metho d Referenc

e Metal s inAi r(BackHalf

) b y ICP/M S ® 4 2006/06/2 9 2006/06/2

9 SO PIN G 108/10

9 EP A SW846-3010A.60 (1 ) This tes

twa s perfonne

d byMaxxa

m Analytic

s Burlingto

n

MAXXA M ANALYTIC S INC .
MARY-ANN E JOHNSON , BA , B.Sc . Projec tManage

r MAJ/ma j encl . 

## Jl Page l of

1 1
674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-6266 Fax : 905-817-577 7Driven by service and Science www.maxxiamaiialytlcs.co m YourProjec

t# : 10002-017-82

0 Site : ONY X
Attention : Jef

f Gorman ENS RInternationa

l 6601 Kirkvill eRd Eas tSyracuse

, N Y . US A 1305

7 Repor tDate : 2006/09/1 1
CERTIFICAT E O F ANALYSI S

-2 -

Validated by :

Tota l cove rpages : 2 Pag e 2 o

f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7 Anolyt iDriven by service and Science wwwjnaxxamaoalytics.com ENS R Internationa l Clien tProject* : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### RESULT S O F ANALYSE S O F FILTE R Maxxa m I D M7314 2 M7314 3 M7314 4 M7314 5 Samplin g Dat e 2006/06/2 1 2006/06/1 9 2006/06/2 0 2006/06/2 1 Unit s M29-R B F H M29-U3-R 1 F H M29-U3-R 2

F H M29-U3-R 3

F H RD L 3 C Batc h MD L
Particulat e Weigh t i n Aceton e Rins e m g N D 4. 0 2. 8 1.7 0. 5 1001275 0. 5 Volum e m l 9 8 5 7 8 7 5 6 1 104987 0 1 Particulate Weigh t o n Filte r m g 0.6 5 2.2 0 1.6 5 1.55 0.3 0 100126 5 0.3 0 N D = Not detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = QualityContro l Batc h

Pag e 3 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax : 905-817-577 7

f Analytic s I r Maxxa m Jo b # : A66217 5 ReportDate : 2006/09/1 1* .fl*. n o ly t l c s In c Maxxa m Jo b # : A66217 5 Repor tDate : 2006/09/1 1 Driven by service and Science www.maxxaoianalytlcs.co m ENS R Internationa l Clien tProject# : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### ELEMENT S BYICP/M S (FILTER) Maxxa m I D M7314 2 M7314 3 M7314 3 M7314 4 M7314 5 Samplin g Date 2006/06/2 1 2006/06/1 9 2006/06/1 9 2006/06/2 0 2006/06/2 1 Unit s M29-R B F H M29-U3-R 1 F H M29-U3-R 1

F H Lab-Du p M29-U3-R 2

F H M29-U3-R 3

F H RD L Q C Batc h MD L [Tota l Arseni c (As) u g 0.6 1 5.8 1 6.0 1 4.2 7 5.6 2 0.4 0 100100 8 0.4 0 [Tota l Berylliu m (Be ) N D N D N D N D N D 0.1 0 100100 8 0.1 0 Tota l Chromiu m (Cr) u g 0.7 9 9.6 4 11.9(1 ) 3.9 8 11. 1 0.3 0 100100 8 0.3 0 N D = Not detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = QualityContro l Batc h ( 1 ) Pleas e refe rto Genera l Comment s pag e fo rspecifi c clarification .

Pag e 4 o

f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Toi l free:800-563-6266 Fax:905-817-577 7

### fSA £ l f Analytic s In c Driven by service and Science Maxxa m Jo b # : A66217 5 Repor tDate : 2006/09/1 1 www.maxxamahalylics.co m ENS R Internationa l Clien tProject# : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### ELEMENT S BYICP/M S (IMPINGE R SOLUTION ) Maxxa m I D M7314 6 M7314 7 M7314 7 M7314 8 M7314 9 Samplin q Dat e 2006/06/2 1 2006/06/1 9 2006/06/1 9 2006/06/2 0 2006/06/2 1 Jnit s M29-R B B H M29-U3-R 1 B H M29-U3-R 1

B H Lab-Du o M29-U3-R 2

B H M29-U3-R 3

B H RD L 3 C Batc h MD L
Tota l Arseni c (As) u g N D 0.3 3 0.3 3 N D 0.2 1 0.2 0 100175 8 0.2 0 Tota l Berylliu m (Be

) u g N D N D N D 0.08 7 N D 0.05 0 100175 8 0.05 0 Tota l Chromiu m (Cr

) u g N D 1.0 6 1.0

2 0.6 6 0.8 4 0.1 5 100175 8 0.1 5 N D = Not detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = QualityContro l Batc h

Pag e 5 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tei : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7

# IV

S 

# a

' Analytic s In c Driven by seri*ice and Science Maxxa m Jo b #:A66217 5 Repor tDate : 2006/09/1 1 www.maxxamaxialytlcs.co m ENS R Internationa l Clien tProject* : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### Test Summar

y
Maxxa m I D Sampl e I D Matri x M7314 2

M29-R B F H Filte r Collecte d Shippe d Receive d 2006/06/2 1

2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) b vICP/M S ICP1/MS 100100 8 2006/06/2 8 2006/06/2 9 N R Particulates i n Ai r(Aceton e Rinse ) (M5) BA L 100127 5 2006/06/2 7 2006/06/2 8 IM R Particulates i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o

fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O

Maxxa m I D Sampl e I D Matri x M7314 3

M29-U3-R 1 F H Filte r Collecte d Shippe d Receive d 2006/06/1 9

2006/06/2 2 Tes t Descriptio n instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) b vICP/M S ICP1/MS 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse) (M5 ) BA L 1001275 2006/06/2 7 2006/06/2 8 . IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o

fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O

Maxxa m I D Sampl e I D Matri x M73143Du p

M29-U3-R 1 F H Filte r Collecte d Shippe d Receive d 2006/06/1 9

2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) b yICP/M S ICP1/MS 100100 8 2006/06/2 8 2006/06/2 9 N_ R 

### I

Maxxa m I D Sampl e I D Matri x M7314 4

M29-U3-R 2 F H Filte r Collecte d Shippe d Receive d 2006/06/2 0

2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) b vICP/M S ICP1/MS 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse) (M5) BA L 100127 5 2006/06/2 7 2006/06/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o

fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O

Maxxa m I D M73145 Collecte d 2006/06/2 1 Sampl e I D M29-U3-R 3 F H Shippe d Matri x Filte r Receive d 2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) byICP/M S ICP1/M S 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse) (M5) BA L 1001275 2006/06/2 7 2006/06/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006/06/2 6 VP 2 Fina l Volum e o

fAceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O

Pag e 6 o

f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7

# IVI 

# a m f Analytic s In c Maxxa m Jo b #:A66217 5 ReportDate : 2006/09/1 1 Driven by service and Science www.maxxamaiudytics.coi n ENS R Internationa l Clien tProject# : 10002-017-82 0 Projectname : ONY X Sample rInitials : 

### Tes tSummar y
Maxxa m I D M7314 6 Samplel D M29-R B B H Matri xImpinge rSolutio n Collecte d 2006/06/2 1 Shippe d Receive d 2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t IMetal s i n Ai r(Bac k

Half) b yICP/M S 1CP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N_ R
Maxxa m I D M7314 7 Sampl e I D M29-U3-R 1 B H Matri xImpinge rSolutio n Collecte d 2006/06/1 9 Shippe d Receive d 2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d IMetal s i n Ai r(Bac k

Half ) b yICP/M S ICP1/M S 100175 8 2006/06/2 9 Analyze d Analys t 2006/06/2 9 N_ R
Maxxa m I D M73147Du p Sampl e I D M29-U3-R 1 B H Matri xImpinge rSolutio n Collecte d 2006/06/1 9 Shippe d Receive d 2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t IMetal s i n Ai r(Bac k

Half ) byICP/M S ICP1/MS 100175 8 2006/06/2 9 2006/06/2 9 N_ R

Maxxa m I D M7314 8 Samplel D M29-U3-R2B H Matri xImpinge rSolutio n Collecte d 2006/06/2 0 Shippe d Receive d 2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t IMetal s i n Ai r(Bac k

Half ) byICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N R

Maxxa m I D M7314 9 Samplel D M29-U3-R3B H Matri xImpinge rSolutio n Collecte d 2006/06/2 1 Shippe d Receive d 2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t IMetal s i n Ai r(Bac k

Half ) b yICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 N R

Pag e 7 o

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# IV

I 

# a ^ a m Analytic s In c Maxxa m Jo b #:A66217 5 Repor tDate : 2006/09/1 1 Driven by service and Science www.max3tamaitaIytIcs.coin . ENS R Internationa l Clien tProject* : 10002-017-82 0 Projectname : ONY X Sample rInitials :

GENERA L COMMENT S
Result s relat e onl yt o th e item s tested .

Pag e 8 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 71^ Analytic s In c imw.maxxamanaivtks.co m Driven by service and Science ENS H Internationa l Attention : JeffGorma n Clien tProject# : 10002-017-82 0 P.O
. # : Projectname : ONY X 

### QualityAssuranc e Repor t Maxxa m Jo b Numbe rGA66217 5 QA/Q C Batc h Nu m Init Q C Typ e Paramete r Date Analyze d yyyy/mm/d d Valu e %Recover y Unit s Q C Limits : 100100 8 N_ R MATRI XSPIK E

(M73143 ) Tota l Arseni c (As ) 2006/06/2 9 49 .5 , RDL=0.4 0 9 9 u g 70 - 130 : MATRI XSPIK E DUP(M73143 ) Tota l Arseni c (As ) 2006/06/2 9 49.5 , RDL=0.4 0 9 9 u g 70 - 130 MATRI XSPIK E (M73143 ) Tota l Berylliu m (Be) 2006/06/2 9 48.0 , RDL=0.1 0 9 6 u g 70 - 13 0 MATRI XSPIK E DUP(M73143 ) Tota l Berylliu m (Be) 2006/06/2 9 47.0 , RDL=0.1 0 9 4 u g 70 - 130 i MATRI XSPIK E (M73143 ) Tota l Chromiu m (Cr ) 2006/06/2 9 48.5 , RDL=0.3 0 9 7 u g 70 - 13 0 MATRI XSPIK E DUP(M73143 ) Tota l Chromiu m (Cr ) 2006/06/2 9 47 .5 , RDL=0.3 0 9 5 u g 70 - 13 0 Spike d Blan k Tota l Arseni c (As ) 2006/06/2 9 48.5 , RDL=0.4 0 9 7 u g 85 - 11 5 Spike d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 49.0 , RDL=0.4 0 9 8 u g 85 - 11 5 • Spike d Blan k Tota l Berylliu m (Be) 2006/06/2 9 59.5 , RDL=0.1 0 119(1 ) u g 85 - 11 5 Spike d Blan k

DU P Tota l Berylliu m (Be) 2006/06/2 9 58.5 , RDL=0.1 0 117(1 ) u g 85 - 11 5 Spike d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 53.0 , RDL=0.3 0 106 u g 85 - 11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/06/2 9 53.0 , RDL=0.3 0 10 6 u g 85 - 115 3 Metho d Blan k Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=0.4 0 u g Metho d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=0.4 0 u g Metho d Blan k Tota l Berylliu m (Be) 2006/06/2 9 ND , RDL=0.1 0 u g Metho d Blan k

DU P Tota l Berylliu m (Be) 2006/06/2 9 ND , RDL=0.1 0 u g Tota l Chromiu m (Cr

) 2006/06/2 9 ND , RDL=0.3 0 u g Metho d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.3 0 u g RP D Tota l Arseni c (As ) 2006/06/2 9 3. 4 % 2 0

Tota l Berylliu m (Be) 2006/06/2 9 N C / o 2 0 Tota l Chromiu m (Cr

) 2006/06/2 9 21.2(1 ) % 2 0 100127 5 IM R Metho d Blan k Particulate Weigh t i n Aceton e Rins e 2006/06/2 8 ND , RDL=0. 5 m g 100175 8 N_ R MATRI XSPIK E

(M73147) Tota l Arseni c (As ) 2006/06/2 9 48.5 , RDL=0.2 0 9 7 u g 7 0 13 0 MATRI XSPIK E DUP(M73147 ) Tota l Arseni c (As ) 2006/06/2 9 50.0 , RDL=0.2 0 10 0 u g 7 0 •130 ' MATRI XSPIK E (M73147) Tota l Berylliu m (Be) 2006/06/2 9 57.5 , RDL=0.05 0 11 5 u g 7 0 -130 : MATRI XSPIK E DU P (M73147) Tota l Berylliu m (Be) 2006/06/2 9 58.5 , RDL=0.05 0 11 7 u g 7 0 •13 0 MATRI XSPIK E (M73147) Tota l Chromiu m (Cr ) 2006/06/2 9 50.0 , RDL=0.1 5 10 0 u g 7 0 -13 0 MATRI XSPIK E DUP(M73147 ) Tota l Chromiu m (Cr ) 2006/06/2 9 51.0 , RDL=0.1 5 10 2 u g 7 0 -13 0 Spike d Blan k Tota l Arseni c (As ) 2006/06/2 9 50.5 , RDL=0.2 0 10 1 u g 8 5 -115 ^ Spike d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 50.0 , RDL=0.2 0 10 0 u g 8 5 -11 5 Spike d Blan k Tota l Berylliu m (Be) 2006/06/2 9 58.5 , RDL=0.05 0 11 7 u g 8 5 -115 ; Spike d Blan k

DU P Tota l Berylliu m (Be) 2006/06/2 9 58.0 , RDL=0.05 0 11 6 u g 8 5 -115 : Spike d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 52.0 , RDL=0.1 5 104 u g 8 5 - 11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/06/2 9 52.0 , RDL=0.1 5 10 4 u g 8 5 -11 5 Metho d Blan k Tota l Arseni c (As ) 2006/06/2 9 ND , RDL=O.2 0 u g Metho d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 ND , RDL ==0.2 0 u g Metho d Blan k Tota l Berylliu m (Be) 2006/06/2 9 ND , RDL=0.05 0 u g Metho d Blan k

DU P Tota l Berylliu m (Be) 2006/06/2 9 ND , RDL=0.05 0 u g Metho d Blan k Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.1 5 u g Metho d Blan k

DU P Tota l Chromiu m (Cr ) 2006/06/2 9 ND , RDL=0.1 5 u g RP D Tota l Arseni c (As ) 2006/06/2 9 N C % 2 0

Tota l Berylliu m (Be

) 2006/06/2 9 N C % 2 0 Tota l Chromiu m (Cr

) 2006/06/2 9 4. 2 % 2 0 N D = Not detecte d 

# i

Pag e 9 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-626 6 Fax:905-817-577 7Driven fry service and

Science bNS H International—~~ ~ Attention : JeffGorma n Clien tProject# : 10002-017-82 0 P.O.f : Projectname : ONY X Qualit yAssuranc e Repor t(Continued ) Maxxa m Jo b Numbe rGA66217 5 N C = Non-calculabl e RP D = Relative Percen t Differenc e SPIK E = Fortifie d sampl e 1 ) Pleas e refe rt o Genera l Comment s pag e fo rspecifi c clarification . 

# X x a 

# m

•^/Analytic s tn e

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### )^)^<E 1 

## "in Driven by service anti Science f Analytic s inc wvrw.maxxaman.alytics.co m 

### Validatio n Signatur e Pag e Maxxam Jo b #

: A66217 5

Th e analytica l dat a an d al l Q C containe d i n thi s report were reviewe d an d validate d b yth e followin g individual(s)
.

FRAN KMO , B.Sc , Inorgani cLab
. Manager

Maxxa m ha s procedure

s inplac e t o guar d agains timprope

rus e o f th e electroni

csignatur

e an d hav e th e require d "signatories" , a

s pe rsectio n5.10. 2 o f ISO/IE C 17025:2005(E) , signin gth e reports . SC C an

d CAEA L hav

e approve

d thi s reportin

gproces s an d electroni

crepor tformat .

Pag e 1 1 o f 1 1 

### 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-817-570 0 Tol l free:80G-563-626 6 Fax:905-817-577 7