Mass Certification - MA-00071 Conn Certification - PH-0520 

## Mt.Tom Generating Co. LLC Analytical Laboratory 15 Agawam Avenue West Springfield, MA 01089 Phone (413) 214-6541 Fax (413) 214-6842 email-madhu.shah@gdfsuezna.com
April 16, 2010A. Douglass Analysis of # 6 Oil



### Enclosed are Report No(s):21446 ,21448 and 21450 Samples Analyzed

Customer Sample Description Laboratory Supervisor Madhu Shah madhu.shah@gdfsuezna.com eMail Report Date



# Thank you for your business

Madhu Shah, Laboratory Supervisor Date West Springfield Contact

ALL the information contained in this report has been reviewed for accuracy and checked against all quality control requirements outlined in each applicable method. This report may not be reproduced, except in full, without written approval from Mt.Tom Generating Co.LLC Analytical Laboratory.1 Pageof310-0499 Work Order 

### Sample Analysis

As-Arsenic Total ppm SW846-7060 0.60 1.00 04/14/10dfp Be-Beryllium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Cd-Cadmium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Co-Cobalt Total Less Than ppm SW846-6010B 1.11 1.00 04/12/10dfp Cr-Chromium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Hg-Mercury Total Less Than ppm SW846-7470 0.02 0.02 04/13/10dfp Mn-Manganese Total ppm SW846-6010B 2.50 1.00 04/12/10dfp 26.6 Ni-Nickel Total ppm SW846-6010B 1.00 04/12/10dfp Pb-Lead Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Se-Selenium Total ppm SW846-6010B 0.88 1.00 04/14/10dfp Chlorine ppm SW846-9076 124.00 1.00 04/12/10 sjr

0.10 Fluorine Less Than ppm SW846-9076 0.10 04/12/10 sjr Moisture % ASTM D-6304 0.20 0.01 04/08/10dfp Parameter Results Method MDL Analyzed/Time 21446 3/29/10 # 6 Oil Bottom West Springfield 4/1/10 Source Taken/TimeReceived SampleDescription Tech

As-Arsenic Total Less Than ppm SW846-7060 0.50 1.00 04/14/10dfp Be-Beryllium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Cd-Cadmium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Co-Cobalt Total ppm SW846-6010B 1.14 1.00 04/12/10dfp Cr-Chromium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Hg-Mercury Total Less Than ppm SW846-7470 0.02 0.02 04/13/10dfp Mn-Manganese Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp 27.5 Ni-Nickel Total ppm SW846-6010B 1.00 04/12/10dfp Pb-Lead Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Se-Selenium Total Less Than ppm SW846-6010B 0.50 1.00 04/14/10dfp Chlorine ppm SW846-9076 237.00 1.00 04/12/10 sjr 0.10 Fluorine Less Than ppm SW846-9076 0.10 04/12/10 sjr Moisture % ASTM D-6304 0.23 0.01 04/08/10dfp Parameter Results Method MDL Analyzed/Time 21448 3/30/10 # 6 Oil Middle West Springfield 4/1/10 Source Taken/TimeReceived SampleDescription Tech

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### Sample Analysis

As-Arsenic Total Less Than ppm SW846-7060 0.50 1.00 04/14/10dfp Be-Beryllium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Cd-Cadmium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Co-Cobalt Total ppm SW846-6010B 1.65 1.00 04/12/10dfp Cr-Chromium Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Hg-Mercury Total Less Than ppm SW846-7470 0.02 0.02 04/13/10dfp Mn-Manganese Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp 26.8 Ni-Nickel Total ppm SW846-6010B 1.00 04/12/10dfp Pb-Lead Total Less Than ppm SW846-6010B 1.00 1.00 04/12/10dfp Se-Selenium Total Less Than ppm SW846-9076 0.50 1.00 04/14/10dfp Chlorine ppm SW846-9076 153.00 1.00 04/12/10 sjr

0.10 Fluorine Less Than ppm SW846-9076 0.10 04/12/10 sjr Moisture % ASTM D-6304 0.26 0.01 04/08/10dfp Parameter Results Method MDL Analyzed/Time 21450 3/30/10 # 6 Oil Top West Springfield 4/1/10 Source Taken/TimeReceived SampleDescription Tech

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