Title G3520C Internal Combustion Engine Operated at the Trail Ridge Energy, L.L. C., Trail Ridge Landfill, Duval County, Florida

Report May4, 2009

Test

Date(s) March 25 & 26 2009

I ILIlIt) lfllt)1IN 111011

Name Trail Ridge Energy, L.L.C., Trail Ridge Landfill

City, County j Jacksonville, Duval

Enchtv Permit ntuniuilion

DEP File No.: 0310358-011 -AC fenit No.: PSD-FL-374B

Testing Contractor

Company Derenzo and Associates, Inc.

Mailing 39395 Schoolcraft Road

Address Livonia, MI 48150

Phone (734) 464-3880

Project No. 0901014

39395 Schooleraft Road • Livonia, MI 48150 . (734) 464-3880 • FAX (734) 464-4368 4970 Northwind, Suite 213 • East Lansing, Ml 48823 • (517) 324-1880 • FAX (517) 324-5409
2.0 PLANT AND SAMPLING LOCATION DESCRiPTION 2

2.1 Generat Process Description 2

2.2 Rated Capacities, Type and Quantity of Raw Materials Used 2

2.3 Emission Control System Description 2

2.4 Sampling Locations (USEPA Method 1) 2

3.0 SUMMARY AND DISCUSSION OF TEST RESULTS 3

3.1 Purpose and Objectives of the Tests 3

3.2 VariatioHs from Normal Sampling Procedures or Operating Conditions 3

3.3 Operating Conditions during Compliance Tests 4

3.4 Air Pollutant Sampling Results 4

4.0 SAMPLING AND ANALYTICAL PROCEDURES 5

4.1 Exhaust Gas Velocity and Flowrate Determination (IJSEPA Method 2) 5

4.2 Exhaust Gas Molecular Weight Determination (USEPA Method 3A) 5

4.3 Exhaust Gas Moisture Content Detenninations (Method 4) 6

4.4 NO and CO Concentration Measurements (USEPA Method 7E and 10) 6

4.5 Particulate Matter Concentration Measurements (USEPA 5/USEPA 202) 6

4.6 Volatile Organic Compound Measurement (USEPA Methods 25A!l 8) 7

4.7 Hydrogen Chloride Measurements (USEPA Method 26A) 7

4.8 Visible Emissions Detenninations (USEPA Method 9) 7

5.0 INTERNAL QA/QC ACTIVITIES 7

5.1 NO Converter Efficiency Test 7

5.2 Sampling System Response Time Determination 7

5.3 Determination of Exhaust Gas Stratification 8

5.4 Instrumental Analyzer Interference Check 8

5.5 Instrument Calibration and System Bias Checks 8

5.6 Meter l3ox Calibrations and Percent Isokinetics 8
I

Trail

Particulate

Ridge

Matter

Energy,

less than 10 Microns (PM 10) Emission Rates from the Unit #4 Engine at the L.L.C. — Trail Ridge Landfill 11

2

Trail

Hydrogen

Ridge

Chloride

Landfill

Emission Rates from the Unit #4 Engine at the Trail Ridge Energy, L.L.C. -

12

3

the

Calculation

#4 Caterpillar

of HCI

Model

Emission

G3520C

Factor Based on Influent Landfill Gas Chlorinated Compounds to

Landfill Engine at the Trail Ridge Energy, LLC -Trail Ridge

13

4

Rates,

Nitrogen

and

Oxides,

Emission

Carbon Monoxide, and Volatile Organic Compound Concentrations, Emission

Ridge Energy,

Factors from the Unit #4 Caterpillar Model G3520C Engine at the Trail L.L.C. -Trail Ridge Landfill 14

5

#4

Six-Minute

at the Trail

USEPA

Ridge

Method 9 Opacity Averages for the Caterpillar Model G3520C Engine Unit Energy, LL.C -Trail Ridge Landfill 15

LIST OF PIGURE(S)

Figure 1. Trail Ridge Energy Facility Process Flow Diagram Figure 2. Trail Ridge Energy Source Diagram Figure 3. Trail Ridge Energy Exhaust Sampling Location

Figure

Figure 4.

5. Isokinetic

Instrumental

Sampling

Analyzer Sampling Train Diagram (USEPA Methods 3A, 7E, and 10)

Figure

Train Diagram (USEPA Methods 5 and 202) 6. Isokinetic Sampling Train Diagram (USEPA Methods 26A)

LIST OF APPENDICES

Appendix

Appendix A Computer Calculated and Field Sampling Data Sheets B Equipment Calibration Data and Opacity Certification Appendix C Laboratory Data Appendix D Sample Calculations

Appendix E Process Data

Appendix F Detailed Descriptions of Sampling Procedures
TRAIL RIDGE ENERGY, LL.C.

TRAIL RIDGE LANDFILL

DUVAL COUNTY, FLORIDA

1.0 SOURCE INFORMATION

County,

Trail Ridge

Florida.

Energy,

The

L.L.C. (Trail Ridge Energy) is located at the Trail Ridge Landfill in Duval

At Facility File No. is 0310358-011-AC and the Permit No. is PSD-FL-374B.

emission

its landfill

units

gas to energy (LFGTE) facility, Trail Ridge Energy is permitted to operate

Engines and

002 — 005 which consist of four (4) Caterpillar G3520C Lean Burn Reciprocating

generated at the

electricity

Trail Ridge

generator sets. These engines are fueled with methane-rich gas, which is Landfill, to power base load electricity generator operations.

of

The

specified

FDEP pennit requires perIbrinance testing of a representative engine for the cleternunation pollutant emissions while the unit is operated at near base load conditions.

particulate

Comnliance

with

testing

diameters

was performed to measure nitrogen oxides (NO), carbon monoxide (CU),

(VOC), hydrogen equal to or less than 10 microns (PM— 1 0), volatile organic COmpOUfld chloride (lid), and oxygen (02), concentrations from the exhaust of and emission rates and opacity the Unit #4 engine pursuant FDEP Air Construction to the testing requirements specified in the Permit.

environmental

The compliance

consulting

testing was performed on March 25, 2009 by Derenzo and Associates, Inc., an and testing company from Livonia, Michigan.

TheProtocol

exhaust

dated

gas

February

sampling and analysis was performed using procedures specified in the Test 13, 2009.

Questions regarding this emission test report should be directed to:

Mr. Michael Brack Mr. Michael Laframboise Field Services Manager Sr. Vice President Derenzo -Operations and Associates, Inc. Landfill Energy Systems. 39395 Schoolcraft Road 29261 WaIl Street Livonia, MI 48150 Wixorn, Mi 48393 (734) 464-3880 (248) 380-3920

3P)5

rmiuJ

Sclcr.fi

S1Itc

Ru: • L;v L\II 4I5O . (74 46--3Sfl • F\.\ (/ 1) 4(- 5 213 • I iic -
decomposition

Methane-rich landfill gas (LEG) is produced in the Trail Ridge Landfill from the anaerobic

capped landfill

ofcells

disposed waste materials. The methane-rich LFG is collected from both active and

system). The using a system of wells that are connected to a central header (gas collection

as fuel for the

collected

IC engine

LEG is directed to the Trail Ridge Energy facility where it is treated and used generators that produce electricity for transfer to the local utility.

combustion

The Trail Ridge Energy facility currently consists ofsix (6) CAT Model No.G3520C IC internal engines that are connected to individual electricity generators.

A process flow diagram for the LEG to electricity process is presented subsequent tables in this to the summary report.

2.2 Rated Capacities, Type and Quantity of Raw Materials Used

The

100%

representative

of

CAT (33520C IC engine generator set was operated at base load conditions (i.e.,

kilowatts

the

(kW).

design

Fuel

capachy of 2,233 brake horsepower) to produce a peak electricity output of 1,600

input rate

(treated landfill gas) consumption is regulated to maintain the required heat

The average

to support engine operations and is dependant on the tPel heat value (methane content).

recorded from

engine fuel consumption rate during the test periods was 541.4 scfm based on data the fuel flow meter installed and operated by Trail Ridge Energy.

Appendix

E provides engine generator process data collected during the compliance test.

2.3 Emission Control System Description

Thelow combustion

engines incorporate state of the art technology in order to fire lean fuel mixtures and produce

uncontrolled by-product emissions. Emissions from the combustion of LFG are released

noise control

into

system

the ambient air through a stack connected to the IC engine exhaust manifold and (noise muffler).

2.4 Sampling Locations (USEPA Method 1)

criteria

The exhaust

for a

stack sawpfrog port for the Model G3520C IC engine satistied the L’SEiA Method I

inches. The stack

representative sample location. The inner diameter of the engine exhaust stacks is 15.5

location

is equipped with two (2) sample ports, opposed 90°, that provide a sampling

from any

53

flow

inches

disturbance.

(34 duct diameters) downstream and 124 inches (8 duet diameters) upstream

I

Velocity

JS EPA Method

pressure traverse locations for the sampling points were tletermincd in accordance with

I fur thc lepresentative engine.
Thearea

relatively

of the

small stack diameter (15.5 inches) of the engine exhaust is obstructed by the surface

high side. The

isokinetic sampling probe, which tends to bias the exhaust velocity measurements on the test results are calculated from pre-test velocity averages.

3.0 SUMMARY AND DISCUSSION OF TEST RESULTS

3.1 Purpose and Objectives of the Tests

NOx,

Stack

PM-l0,

testing is

VOC,

required

HCI,

for the permitted emission units to demonstrate compliance with the CO,

to perform initial,

and opacity emission limits by permit conditions. The facility is required

satisfies

annual and permit renewal testing during a six-year period. This test event the 2009 initial pertbrxnance test required by the permit.

portions

The PM—i 0 emissions were determined by combining the total filterable with the total condensable of the USEPA Method 5 and USEPA Method 202 sampling trains.

The VOC emission rate from the tested engine was determined by subtracting the methane

concentration

concentration (in—field USEIA Method 18 field analysis) from the total hydrocarbon (THC) detennined by US EPA Method 25A field analysis.

The

during

exhausts

which

from the LFG-fueled IC engines were momtored for six (6) one-hour test periods the 02 and CO2exhaust gas concentrations were measured using instrumental

using

analyzers. The engine NON, and CO measurements consisted of triplicate 60-minute measurements

measurements

instrumental analyzers, and the PMI 0, and HCI consisted oftriplicate 60-minute using isokinetic sampling equipment.

of

Exhaust

the weight

gas moisture content from the representative engine was determined by gravimetric analysis

to each isokinetic

gain in the chilled impingers. Velocity and volumetric flow rates were measured prior sampling test period and during pre-test and post-test time periods.

areatest

Opacity

opacity

observations were made during one ofthe PM-b tests and were observed at the point of

continuous

in the portion of the plume where condensed water vapor is not present, with readings taken every 15 seconds for 60 minutes.

kW

The

peak

testing

electricity

was performed while the IC engine was operated at nonnal base load conditions (1600 output +1- 5%).

3.2 Variations from Normal Sampling Procedures or Operating Conditions

2000

The testing

and specified

for all pollutants

TISEPA

were performed in accordance with the Test Protocol dated February 13,

velocity measureincats.

test mcthods. Isokinetic s:unpl ag rates were determine(l using pm-test
g p

g

.

3.3 Operating Conditions during Compliance Tests

conditions

The representative

during

LFG-fueled IC engine was operated at base load (100% capacity +1- 5%)

engine data management

the compliance testing. The average kilowatt (kW) output value displayed by the

period. LFG flowrate computer (LCD screen) were manually recorded 3 times during each test

displayed by the fuel

information was obtained similarly (manually recorded readings) from data

during the testing was

flow rate meter installed at the facility. The average LFG consumption rate

rate during

541.4 standard cubic feet per minute (scfm). The average electrical output the test event was 1,601 kW.

3.4 Air Pollutant Sampling Results

performance

The following table presents the engine #4 three-test average emission rates from the initial evaluation:

Emission Parameter Unit #1 Emissions Pennit Limit NOx NO emissions (lb/he) 2.09 2.95 NO emissions (g/bhp-hr) 0.43 0.60

CO CO emissions (lb/hr) 13.13 13.54 CO emissions (g/bhp-hr) 2.70 2.75

VOC VOC emissions (lb/br) 0.0 1.37 VOC emissions (g/bhp-hr) 0.0 0.28

PM10 PM10emissions(lb/hr) 0.57 1.18 PM10 emissions (g/bhp-hr) 0.12 0.24

HC1 HC1 emissions (lb/hi) 0.02

- IICI emissions (Ib/IviMsef) 0.68 10.9

02 Oxygen concentration (%) 8.27

Opair/’ F-Lghesr 10 second average d6) 0.0 Notes 10

standard

(lb/he) pounds

cubic

per

foot

hour, (g/bhp-hr) grams per brake horsepower hour, (lb/MMscf pounds per million

Tables

representative

1 through

Ll’G-fueled

5 present measured gas conditions and io11utant emission rates for the IC engine.

Appendix A provides c miputel calculated and hold data sheets flr the [C engine tests.
4.0 SAMPLING AND ANALYTICAL PROCEDURES

by

A test

the

protocol

FDEP. Tins

for the compliance testing was prepared by Derenzo and Associates and reviewed

were used during

section provides a summary ofthe sampling and analytical procedures that the test and presented in the test plan.

Appendix

F presents diagrams for the USEPA Methods sampling trains.

4.1 Exhaust Gas Velocity and Flowrate Determination (USEPA Method 2)

engine

In order

exhaust

to determine

stack

air pollutant emission rates on a mass basis (e.g., pound per hour), IC

Method 2 prior to conducting

gas velocities, and volumetric flow rates were determined using USEPA

used to determine

tests. An S-type pitot tube connected to a red-oil manometer was velocity pressure. Gas temperature was measured using a K—type

tubing

thermocouple

were

mounted to the heated sample probe. The heated sample probe and connective leak-checked to verify tire integrity of the measurement system.

The

and oil

absence

manometer.

of cyclonic flow for each sampling location was verified using an S-type Pitot tube

planes of the

The Pitot tube was positioned at all of the velocity traverse points with the face openings of the Pitot tube perpendicular Pitot tube was then to the stack cross-sectional plane. The

perpendicular,

rotated to determine the null angle (rotational angle as measured from the or reference, position at which the differential pressure is equal to zero).

sampling

Exhaust gas

period

velocity pressure and temperature were measured during each one-hour isokinetic in accordance with USEPA Method 2.

4.2 Exhaust Gas Molecular Weight Determination (USEPA Method 3A)

each

CO2and

one-hour

02 content in the IC engine exhaust gas stream was measured continuously throughout

exhaust was monitored

test period in accordance with USEPA Method 3A. The CO2content of the

the exhaust was monitored using a non-dispersive infrared (NDIR) gas analyzer. The 02 content of using

a gas analyzer that utilizes a paramagnetic sensor.

was

During

extracted

each one-hour

from the

sanmpiirig period, a ontmnuous sample of the IC engine exhaust gas stream

line. The

stack using a stainless steel probe connected to a Teflon® heated sample

analyzer; therefore,

sampled gas

measurement

was conditioned by removing moisture prior to being introduced to the

conditions. The

of 02 and CO2concentrations correspond to standard dry gas

accuracy

instrument was calibrated using appropriate calibration gases to determine and system bias (described in Section 5.5 of this document).
Method

cordance with USEPA

4 using a chilled impinger sampling train as a component of the USEPA sampling procedures for PM (i.e., not as a separate measurement with train), which was performed concurrently the instrumental analyzer sampling methodologies. Moisture detenninations were measured similarly during each HC1 sampling period. During each sampling period, a gas sample was extracted at a predetermined rate from the source where moisture was removed from the sampled gas stream using imnplngers that were submersed in an ice bath, and then determined

was

gravimetrically. At the conclusion of each sampling period, the moisture gain in the impingers determined gravimetrically by weighing each impinger to determine net weight gain.

Appendix

F presents detailed gas sampling procedures for the US EPA sampling trains.

4.4 NO and CO Concentration Measurements (L SEPA Method 7E and 10)

NO and CO pollutant concentrations

chemiluininescence

in the exhaust of the IC engine were detennined using a NO analyzer and NDIR CC) analyzer.

Three (3) one-hour sampling periods were performed for the IC engine exhaust testing. Throughout each one-hour test period, a continuous sample of the engine exhaust gas was extracted from the stack

this document,

using the Teflon® heated sample line and gas conditioning system described in Section 4.2 of

was

and delivered to the instrumental analyzers. Instrument response for each analyzer

continuously

recorded on a data logging system that monitored the analog output of the instrumental analyzers and logged data as one-minute averages. Prior to, and at the conclusion of each test, the instruments were calibrated using appropriate upscale calibration and zero gas to determine analyzer calibration error and system bias. Sampling times were recorded on field data sheets.

4.5 Particulate Matter Concentration Measurements (USEPA 5/USEPA 202)

An integrated sample of the exhaust gas was withdrawn isokinetically from the IC engine exhaust

accordance

stack. The filterable

with

PM emissions were measured with the front-half of the sampling system in

with

US EPA Method 5. The condensible particulate concentrations were measured the back half of the sampling system in accordance with USEPA Method 202. The combined filterable and condensible emission rates constitute the PM-)O emission rates.

were

Upon completiun of the reLILLired posttest leak check of the isokmnetic sampling train, the impingers

nitrogen

transported to the mobile laboratory (trailer) where a nitrogen purge was conducted. The

20

purge consisted of bubbling reagent grade nitrogen through the impinger train at a rate of liter per minute for 60 minutes and was conducted on all PM-l0 sampling trains. Upon

methodologies;

completion of the nitrogen purge, the samples were recovered in accordance with the applicable the samples were clearly and uniquely labeled and readied for transport.

presented

(lravimetric analysis was conducted by Bureau

\7critas, Novi, Michigan. Laboratory data is in Appendix C.
The VOC emission rate from the engine was detenni ied by subtracting the methane concentration

ionization

from the total hydrocarbon (T1IC) concentration. TI-IC concentrations were measured using a flame

determined

analyzer in accordance with USEPA Method 25A. Methane concentrations were

The resultant

using

methane

a Direct Methane, Non-Methane Analyzer in accordance with USEPA Method 18.

values. The VOC

concentrations were subtracted from the THC concentrations giving VOC

Computer

values were used in calculating VOC emission rates from the engine exhaust. calculated and field data is presented in Appendix A.

4.7 Hydrogen Chloride Measurements (USEPA Method 26A)

An integrated sample of the exhaust gas was withdrawn isokinetically from the IC engine exhaust

analysis

stack. The Hydrogen chloride concentrations from the engine were deterrnmed by ion specific electrode of the ilnpinger contents in accordance with USEPA Method 26A.

presented

The 0.1 N H2S04samples were analyzed by Bureau Veritas, Novi, Michigan. Laboratory data is in Appendix C.

4.8 Visible Emissions Determinations (USEPA Method 9)

Opacity determinations were performed using USEPA Method 9 where 15-second readings recorded on an observation report for a total of 60 minutes.

5.0 INTERNAL QAIQC ACTiVITIES

5.1 NO Converter Efficiency Test

program.

The NO2—NO

A mixture

conversion efficiency of the Model 42c analyzer was verified prior to the testing

The bag was

of NO calibration gas and hydrocarbon free air gas was added to a Tedlar bag.

bag emptied.

attached

As

to the inlet of the analyzer and the instrument response was monitored as the

analyzer’s NO2

the conversion efficiency test progresses the NO reacts with 02 to form NO2.The

measurement.

— NO converter uses a catalyst at high temperatures to convert the NO2to NO for

concentration decreases

The conversion efficiency ofthe analyzer is deemed acceptable if the total NO no more than 2% of the highest observed concentration over a 30-minute time period.

The

concentration

NO2 — NO

decreased

conversion

by

efficiency test satisfied the USEPA Method 7E criteria (measured NO less than 2% over a 30-minute time period).

5.2 Sampling System Response Time Determination

izmtroclucmu

The response time of the sampline sstn was determined poor to the compliance test piogiam by upscale eas and zero mis. in series, into the sampling system using a Ice connection at the
5.3 Dctenriination of Exhaust Gas Stratification

measurement

Gaseous sample extraction was performed at sampling points corresponding to the predetermined

determined

points used for velocity measurements in accordance with USEPA Method I. It was that no stratification was present in the stack at the sampling location.

5.4 Instrumental Analyzer Interference Check

The instrumental analyzers used to measure NOx, CO, 02 and CO2have had an interference response test perfonned prior to their use in the field, pursuant to the interference response test

would

procedures specified in USEPA Method 7E. The appropriate interference test gases (i.e. gases that he encountered in the exhaust gas stream) were introduced into each analyzer, separately and

composite

as a mixture with the analyte that each analyzer is designed to measure. All of analyzers exhibited a deviation of less than 3.0% of the span for all measured interferent gases. No major analytical components of the analyzers have been replaced since performing the original interference tests.

5.5 Instrument Calibration and System Bias Checks

At the beginning of each day, initial three-point instrument calibrations were performed by injecting calibration gas directly into the inlet sample port for each instrument. System bias checks were preformed prior to and at the conclusion of each sampling period by introducing the appropriate upscale calibration gas and zero gas into the sampling system (at the base of the stainless steel sampling probe prior to the particulate filter and Teflon® heated sample line) and verifying the instrument response against the initial instrument calibration readings.

CO,

The instruments

THC

were calibrated with USEPA Protocol 1 certified concentrations of C0 2,02, NOx, and zeroed using pure nitrogen or hydrocarbon free air.

5.6 Meter Box Calibrations and Percent Isokinetics

The isokinetic sampling console, which was used for isokinetic testing, was calibrated prior to and

IJSFPA

after the

Method

testing program. This calibration uses the critical orifice calibration technique presented in S The metering consol calibration exhibited no data outside the acceptable ranges presented in US EPA Method 5.

All tests were within the required +-l0% isokinetic sampling rate required by USEPA Methods 5/202 and 26A.

Appendix 13 presents test equipment quality assurance data (i.e., NO2 — NO conversion efficiency test data, instrument cal ibratiori and system bias check records, calibration gas cer 0 ticatmumis, intem-tbrcnc’e test results, mimeter box calibration records. cvcluiiic flow determujtiius sheets, pilot
Equipment calibration and certifications are presented in Appendix B.

I hereby certify that the information given in this report is correct to the best of my knowledge. This test report has been reviewed and is approved for submittal to FDEP by the following representatives:

Report Prepared By:

Michael J. Brack

Field Services Manager

Derenzo and Associates, Inc.
I certify that all data required and provided to the person conducting the test are true and correct to my knowledge.

Report Certified By:

Scott Salisbury

President

Trail Ridge Energy, LL.C.
Test Test Times Engine Output Moisture 02 C02

ID (EST) (Kw) (bhp) (%) (%) (%)

Unit4-Test 1 8:05 -9:10 1,551 2,167 11.4 8.28 10.9 Unit 4-Test 2 9:48 - 10:53 1,581 2,208 11.6 8.29 10.9 Unit 4-Test 3 11:35 - 12:40 1,600 2,235 10.4 8.30 11.0

Average 1,577 2,203 1 1.1 8.29 10.9

Particulate Matter (USEPA Method 5 Filterable)

Test Flowrate Sample Volume Lab Weight Concentration PM Emission Rates

ID (dscfuii) (dscf) (mg) (mg/dscf) (lb/br) (g/bhp*hr)

Unit 4-Test 1 4,591 40.97 8.1 0.20 0.12 0.03 Unit4-Test2 4,573 40.44 8.2 0.20 0.12 0.03 Unit4-Tcst3 4,668 41.18 11.2 0.27 0.17 0.03

Average 4,61 1 40.87 9.2 0.22 0.14 0.03

Particulate Matter (USEPA Method 202 Condensible)

Test Flowrate Sample Volume Lab Weight Concentration PM Emission Rates

ID (dscfm) (dscf) (rng) (rng/dscf) (lb/br) (g/bhp*hr)

Unit 4-Test 1 4,591 40.97 27.3 0.67 0.41 0.08

Unit 4-Test 2 4,573 40.44 27.6 0.68 0.41 0.08 Unit4-Test3 4,668 41.18 31.9 0.77 0.48 0.10 Average 4,611 40.87 28.9 0.71 0.43 0.09

PM-b (Filterable and Condensible)

Test Flowrate Sample Volume Lab Weight Concentration PM Emission Rates

ID (dscfm) (dscf) (mg) (mgldscf) (lb/br) (g/bhp*hr)

Unit 4-Test 1 4,591 40.97 35.4 0.86 0.53 0.11 Unit4-Test2 4,573 40.44 35.8 0.89 0.54 0.11 Unit4-Test3 4,668 41.18 43.1 1.05 0.65 0.13

Average 4,611 40.87 38.1 0.93 0.57 0.12

Permit Limit: 1.18 0.24

Definitions:

(EST) = Eastern Standard Time

(Kw) = Killowatt

(bhp) brake horse power

(dscfn) = dry standard cubic feet per minute

(dscf) =dry standard cubic feet

(mg) = milligrams

(mg/dscf) = milligrams per dry standard cubic foot

(lb/br) = pounds per hour

(g/bhp*hr) grams per brake horse power hour

Equations:

(lb/br) = (mg*0.0l 543)/dscf*dscfiri*0.00858

(g/hhp*hr) = ih/hr*453.6 g/ib * 0.7457 Kw/bhp / (Kw / 0.96 efficiency)
Derenzo and Associates, Inc. Project No.: 0901014

Test Test Times Engine Output Moisture 0, CO, ID (EST) (Kw) (bhp) (%) (%) (%)

Unit 4-Test 1 14:09 - 15:14 1,601 2,236 11.7 8.27 10.91 Unit 4-Test 2 16:05 - 17:11 1,600 2,235 1 1.1 8.24 10.95 Unit 4-Test 3 17:57 -19:01 1,598 2,233 10.6 8.22 10.98

Average 1,600 2,235 11.1 8.25 10.94

Hydrogen Chloride

Test Flowrate Sample Volume Lab Weight Fuel Flow HCI Emission Rates ID (dscfm) (dscf) (mg) (IvlMscf/hr) (lb/br) (lb/Mlvtscf)

Unit 4-Test 1 4,555 38.37 0.5 0.03226 0.01 0.26 Unit 4-Test 2 4,582 72.17 3.4 0.03253 0.03 0.88 Unit 4-Test 3 4,648 72.43 3.5 0.03247 0.03 0.91 Average 4,595 60.99 2.5 0.03242 0.02 0.68

Permit Limit: 10.9

Definitions:

(EST) = Eastern Standard Time

(Kw) = Killowatt

(bhp) = brake horse power

(dscfm) = dry standard cubic feet per minute

(dscf) dry standard cubic feet

(mg) = milligrams

(mg!dscf) = milligrams per dry standard cubic foot

(lb/br) pounds per hour

(glbhp*hr) = grams per brake horse power hour

Equations:

(lb/br) = (mg*0.01543)/dscf*dscfm*0.00858

(g!bhp*hr) = lb/hr*453.6 glIb * 0.7457 Kw/bhp / (Kw / 0.96 efficiency)
Analytical Report No. FICI

LFG Influcnt Chlorine Coumpounds Concentration Molecular Chlorine Emission Faclor

(ppm) Formula Atoms (lb./MMcP)

Freon 12 (Dichiorodifluoromethane) 0.600 CC1,F 2 2 0.113

Freon 114 (Dichiorotetrafluroethane) <0.080 C2I,F 4 2 0.015

Chloromethane <0.320 CH3I 1 <0.030

Vinyl Chloride 0.097 C2HCI 1 0.009

Chloroethane <0.080 C,H 5I 1 <0.008

Freon 11 (Fluorotrichloromethane) <0.080 CFCI 3 3 0.023

Freon 113 (l,1,2-trichloro-1,2,2-trifluoroethane) <0.080 C21F3 2 <0.015

3-Chloropropene <0.320 C5HI 1 <0.030

Methylene Chloride (Dichloromethane) <0.080 CH2I 2 <0.015

I ,2-Dichloroethene (as cis- 1 ,2-Dichloroethene) 0.320 C2H1 7 2 <0.060

I .2-Dichloroetlsene(as trans-I ,2-Dichloroethene) <0.030 C,H 21 2 0.015

1.1-Dichloroethane <0.080 C2F141, 2 <0.015

1,1-Dichloroethene <0.080 C,H 21 2 <0.015

Chloroform <0.080 CHCI 3 3 <0.023

1.1,1-Trichloroethane <0.080 C2H31 3 <0.023

Carbon Tetrachloride <0.080 Cd 4 4 <0.030

1.2-Dichloroethane <0.080 C,H 4I, 2 <0.015

Trichloroethene 0.130 C2FICI 5 3 <0.037

1,2-dichloropropane <0.080 C3H6I, 2 0.015

Bromodichloromethane <0.080 CBrCI 2 2 <0.015

I ,3-Dichloropropene (as cis- 1 ,3-Dichloropropene) <0.080 C3H41 2 2 <0.015

1,3-Dichloropropene(as trans-1,3-Dichloropropene) <0.080 C3H41 2 2 <0.015

1,1,2-Trichloroethane <0.080 C,H 3l 3 <0.023

Tetrachioroethene (Perchloroethene) 0.250 C21 4 4 <0.094

Dibromochloromethane <0.080 CHBr 2I 1 0.008

Chlorobenzene <0.080 C6H5I 1 <0.008

1,1,2,2-Tetrachloroethane <0.080 C2H,C1 4 4 0.030

l,3-Dichlorobenzene <0.080 C6H41 2 2 <0.02

I ,4-Dichlorobenzene 0,270 C5H4I, 2 <0.05

aipha-Chlorotoluene <0.080 C7H1 1 0.008

I ,2-Dichlorobenzene <0.080 C6H4I 2 2 <0.02

I ,2,4-Trichlorobenzene <0.3 20 C6H31 3 <0.09

Hexachlorobutadiene <0.320 C41 6 6 <0.18

Total hydrogen chloride emission factor (lb/MMct) <1.07

Average fuel flow (scfm) 540.3

Calculated hydrogen chloride emission rate (lb/hr) <0.03 2

Sample Calculations:1. E’ample calculation for Freon 12 that assumes complete conversion of chloride to 1-ICI

(0.600 fit Freon l2iMMcf LFG) (2 mol FlCl/mol Freon 2) (3646 lb. HClfmol) I (387 ti’Jniol) 0.113 lb llCFhlMcflF(i

2 Example hydrogen chloride emission rate colculation as lb/hr

(I )7x 03 lb ll(l.ibl\lcl I Eli I l.000.Or)0 scl/hiNiset) 5$ 3 scf/min. meg. inlet (1os to engines dunii’ sanitilmnma) (nO nunihr 1)03 lb Ily hr
Engine Output Moisture 0, CO. (EST) (Kw) (bhp) (%) (%) (%)

Test 1 805-905 1,551 2,167 11.4 8.3 10.9 Test2 952-1052 1581 2,208 11.6 8.3 10.9 Test3 1135-1235 1598 2,233 10.4 8.3 11.0 Average 1,577 2,203 11.1 8.29 10.9

NOx

NOx Instrumental NOx Corrected NOx Emission NOx Emission Test Flowrate Concentration Concentration Rate Factor

ID (dscfln)’ (ppmv) (ppmv) (lb/br) (glbhp*hr)

Test 1 4,591 65.15 63.05 2.08 0.43 Test2 4,573 63.97 61.27 2.01 0.41 Test 3 4,668 68.07 65.21 2.18 044 Average 4,611 65.73 63.18 2.09 0.43

Permit Limits 2.95 0.60

Co

co

CO Ittstrunsental (‘otrected CO Emission CO Emission Test Flowrate Concentration Concentration Rate Factor

ID (dscfm)’ (ppmv) (ppmv) (lb/tsr) (g/bhpThr) —

Pest I 4,591 646 650 13.02 2.73 Test 2 4,573 649 653 13.04 2.68 lest 3 4.668 653 654 13.33 2.71 Average 4.611 649 652 13.13 2.70

Permit Limits 13.54 2.75

voc

THC VOC

Corrected Exhaust Methane Emission VOC Teat Flowrate Concentration Concentration 2 Rate Emission Factor

ID (scfin) t (ppmv) (ppmv) (lb/hr) 1 (glbhp*hr)S

Test I 5,180 562 628 0.0 0.0 Test 2 5,172 636 662 0.0 0.0 Test3 5,210 614 650 0.0 0.0 Average 5,188 604 647 0.0 0.0

Permit Limits 1.37 0.28

Notes:

= Flosvrute calculation based on Type S Pitot measurements (USEPA Methods 1 -4) pee-lest flosvrates 2 = Exhaust gas methane concentration (pptsv-svet), as propane

3 = Calculated emission rate derived from in-8etd, methane subtracted from THC as propane

Definitions:

(Kw) Kittowatt (EST) — Eastern Standard Time

(bhp) brake horseposver 0, = Oxygen

(g/bhp 5hr) grams per brake horsepower hour CO carbon dioxide

(dschu) dry standard cubic feet per ntisute NOx oxides of nitrogen

)scfm) standard cubic feet per inmate (wet) CO carbon monoxide

(lb/br) = pounds per hour THC total hydrocarbons

(ppmv) parts per mitlion by volume-as propane VOC sotatite organic compounds

NOx, CO. and VOC Emission Rate Calculation Formulas:

(63 pallistant!lOO 63 gas) • (lb.niok’385 63 potiutant) (lb pollutast/lh.nsol pollutant)

(exhaust flosvrate 1t3’min) (60 mis/br) = Ensssios Rate (tb/br)

(Emission Rite (lb/br)) 453.6 cR6) (blipi I/mission F,irtoi (g/bhphr)
g

, 

a

County, Florida

Test Date(s): March 25, 2009

Derenzo and Associates, Inc. Project No.: 0901014

Start Time: 11:30 End Time: 12:30 Page 1 of 1

Minute Second 6-mm

0 15 30 45 Average

1 0 0 0 0

2 0 0 0 03 0 0 0 0

4 0 0 0 05 0 0 0 0 -

6 0 0 0 0 0.0

7 0 0 0 0 0.08 0 0 0 0 0.0

9 0 0 0 0 0.0

10 0 0 0 0 0.0

11 0 0 0 0 0.0

12 0 0 0 0 0.013 0 0 0 0 0.0

14 0 0 0 0 0.015 0 0 0 0 0.0

16 0 0 0 0 0.0

17 0 0 0 0 0.018 0 0 0 0 0.019 0 0 0 0 0.0

20 0 0 0 0 0.021 0 0 0 0 0.0

22 0 0 0 0 0.0

23 0 0 0 0 0.0

24 0 0 0 0 0.0

25 0 0 0 0 0.0

26 0 0 0 0 0.0

27 0 0 0 0 0.0

28 0 0 0 0 0.029 0 0 0 0 0.0

30 0 0 0 0 0.0

6-minute average maximum 0.0
Trail RidgeEnergy LLC

Exhaust

Stack

Condensate

I

/

Figure 1.

Trail Ridge Energy LLC

LFG Electricity Generaticn Facility

Scale Sheet Derenzo and Associates

None I of I ProjectNo. 0901014

LFG Collection Header

Muffler

Air,’Gas

Cooler Treated LFG

to Engines

Treated with leachate

or returned to landfill

Gas Treatment

System

Engine Coolant

Radiator

Generator Sets —

Additional Five (5)

Identical Engine
0

-

— 0

0

oo

-t—. -t

—

-t

-t

-t

(t

N

ri-i

N CID

0

0

,,

0

0

0-

tij=

0

—

0Cu

0
Engine Exhausts

4.5 in. long

Sample Ports

Velocity sample lotions as

measured from sample port opening

Sample Port

4 15.41

5 17.74

6 19.46

Figure 3.

Trail Ridge Energy LLC

Exhaust Sample Locations

Derenzo and Associates

ProjectNo. 0901014

Exhaust Stack

Cross-Section

Muffler

Engine Facility Rooftop

Scale

None Sheet

1 of 1
4/2 8/0 9 USEPA Method 3A,7E,1O,18/25A

Sample Train

Sheet i Derenzo and Associates

I of 1 ProjectNo. 0901014

Stainless steel

sample probe

Spring-I oaded

check valve

7-Micron SS

Particulate Filter Heated

sample line

Heated Teflon

line

Calibration

Sample

Pump

Data Logger

Gas

Divider

Zero Gas

(HC Free Air!

— Nitrogen)

Excess sample

to atm

Figure 4.

Calibration gases Scale

None
Glass Filter

Housing

Glass Impingers

Stainless Steel

Heat Traced Glass-Lined Sample

Probe

J-Bar

Nutech Sampling and

Metering Console

Impinger # 1: 100 m L ofDI H20

Impinger #2: 100 m L ofDI H20

Impinger#3: lOOmLofDIH2O

Impinger # 4: Dried Silica Gel

Pitot Tube

Temperature Sensor

Stainless Steel Nozzle

/Type-S Pitot Tube

Ice!Water

Bath

fl Vacuum Gauge

= Temperature Measurement

(rf ct,,r1rri std or ‘mod’

Exhaust Orifice

Vacuum Line

Air-Tight

Pump

Figure 5.

USEPA Method 5/202

Scale

None

Sheet Derenzo and Associates

1 of 1 ProjectNo. 0901014
Heat Traced Glass-Lined Sample

Probe

Glass Filter

Housing

Glass Impingers J-Bar

Impinger Contents (indicate Standard ‘std’ or Modified “mod”)

Irnpinger# 1: 100 mLof0.1NHSO 4(std)

lrnpinger#2: 100 mLof0.INH 2SO4(std)

Impinger # 3: 100 mL of 0. 1 N NaOH (mod)*

Impinger#4: 100 mL of 0.1 NNaOH(mod)*

Impinger # 5: Dried S ilica Gel (mod)

* DiN NaOH impingers may be replaced with empty

knockout impinger as chloride e missions will not be

m easured.

Scale

None

Derenzo and Associates

Project No. 0901014

Pitot

Pitot Tube

Temperature Sensor

---( Glass Nozzle

Type-S Pitot Tube

Vacuum Gauge

Ice!Water

Bath

Temperature Measurement

Exhaust

Bypass

Valve

OrIfice

Main

Valve

Vacuum Line

Air-Tight

Pump

Figure 6.

Nutech Sampling and

Metering Console

USEPA Method 26A Sample Train

Sheet

I of I
APPENDIX A

COMPUTER CALCULATED AND FIELD DATA
tic 

Pressure

Stack Diameter

7.70 % N 80.86 (in.) 15.50 Md Traverse points 30.07 12 Ms Operator 28.70 TS/DW Moisture Content (%) 11.4

Traverse Traverse Point Stack Temp. Velocity Pres. Point Stack Temp. Velocity Pres. Number (°F) (“H20) Number (°F) Side A (“H20) Side B 1 881 3.30

2 1 879 3.20 881 3.60

3 2 880 3.20 882 3.60

4 3 880 3.30 884 3.505 4 881 3.50 880 3.50

6 5 882 3.40 878 3.40

Average 6 881 3.10 881 3.48 881 3.28

Average Velocity Pressure (“H,O) 3.3 83

Average Velocity Pressure Sqrt (“H20) 1.839

Stack Pressure (“Hg) 30.70

Stack Gas Specific Gravity (Gs) 0.99

Average Stack Temperature (°F) 881

Average Stack Velocity (fps) 162.9

Average Stack Velocity (fpm) 9775.0

Area of Stack (ft 2) 1.3 10

Flowrate (Actual-CFM) 12,809

Flowrate (Standard Wet-SCFM) 5,175

Flowrate (Standard Dry-DSCFM) 4,586

Derenzo and Associates, Inc.
Stack Static Pressure 0.00 7.50 % N Stack Diameter 80.77 (in.) 15.50 Md Traverse points 30.08 12 Ms Operator 28.68 TS/DW Moisture Content (%) 11.6

Traverse

Traverse

Number

Point Stack Temp. Velocity Pres. Point Stack Temp. Velocity Pres. (°F) (H2O) Number (°F) Side A (“H20) Side B 1 879 3.20

2 1 876 3.00 880 3.20

3 2 878 3.30 881 3.40

4 3 880 3.50 879 3.70

5 4 878 3.40 878 3.50

6 5 876 3.50 877 3.50

Average 6 877 3.30 879 3.42 878 3.33

Average Velocity Pressure (“H20) 3.3 75

Average Velocity Pressure Sqrt (“H20) 1.836

Stack Pressure (“Hg) 30.68

Stack Gas Specific Gravity (Gs) 0.99

Average Stack Temperature (°F) 878

Average Stack Velocity (fps) 162.6

Average Stack Velocity (fpm) 9757.8

Area of Stack (ft 2) 1.310

Flowrate (Actual-CFM) 12,786 Flowrate (Standard Wet-SCFM) 5,173 Flowrate (Standard Dry-DSCFM) 4,574

1)erenzo and Associates, Inc.
(in.) 15.50 Md 30.09

Traverse points 12 Ms 28.83Operator TS/DW Moisture Content (%) 10.4

Traverse Traverse

Point Stack Temp. Velocity Pres. Point Stack Temp. Velocity Pres.

Number (°F) (“H20) Number (°F) (UH2O) Side A Side B

1 881 3.20 1 878 3.10

2 879 3.50 2 880 3.30

3 880 3.70 3 883 3.50

4 882 3.40 4 879 3.60

5 880 3.40 5 878 3.50

6 879 3.50 6 877 3.30

Average 880 3.45 879 3.38

Average Velocity Pressure (‘H20) 3.4 17

Average Velocity Pressure Sqrt (“H20) 1.848

Stack Pressure (“Hg) 30.68

Stack Gas Specific Gravity (Gs) 1.00

Average Stack Temperature (°F) 880Average Stack Velocity (fs) 163.3

Average Stack Velocity (Thm) 9798.7

Area of Stack (ft 2) 1.310Flowrate (Actual-CFM) 12,840

Flowrate (Standard Wet-SCFM) 5,189Flowrate (Standard Dry-DSCFM) 4,650

Derenzo and Associates, Inc.
15.50 Md Traverse points 30.08 12 Ms Operator 28.66 TS/DW Moisture Content (%) 11.7

Traverse

Traverse Point Stack Temp. Velocity Pres.

Number Point Stack Temp. Velocity Pres. (°F) (“H20) Number (°F) Side A (“H20) Side B 1 877 3.10 1 875 2 876 3.00 3.20 2 880 3 880 3.20 3.30 3 881 4 879 3.60 3.40 4 876 5 880 3.50 3.50 5 878 6 878 3.40 3.40 6 876 Average 878 3.40 3.32 878 3.35

Average Velocity Pressure (“H20) 3.333 Average Velocity Pressure Sqrt (“H20) 1.825

Stack Pressure (“Hg) 30.70 Stack Gas Specific Gravity (Gs) 0.99 Average Stack Temperature (°F) 878 Average Stack Velocity (Ths) 161.6

Average Stack Velocity (fpm) 9697.8 Area of Stack (ft 2) 1.3 10 Flowrate (Actual-CFM) 12,708 Flowrate (Standard Wet-SCFM) 5,145 Flowrate (Standard Dry-DSCFM) 4,542

Derenzo and Associates, Inc.
Md Traverse points 30.08 12 Ms Operator 28.73 TS/DW Moisture Content (%) 11.1

Traverse Traverse

Number

Point Stack Temp. Velocity Pres. Point Stack Temp. Velocity Pres. (°F) (11H20) Number (°F) Side A (H2O) Side B 1 878 3.00

2 1 872 3.20 875 3.30

3 2 875 3.50 876 3.30

4 3 876 3.50 877 3.40

5 4 877 3.60 875 3.20

6 5 875 3.50 874 3.40

Average 6 874 3.30 876 3.27 875 3.43

Average Velocity Pressure (“H20) 3.350

Average Velocity Pressure Sqrt (“H20) 1.830

Stack Pressure (“Hg) 30.69

Stack Gas Specific Gravity (Gs) 0.99

Average Stack Temperature (°F) 875

Average Stack Velocity (Ths) 161.7

Average Stack Velocity (Thm) 9701.6

Area of Stack (ft 2) 1.310

Flowrate (Actual-CFM) 12,713 Flowrate (Standard Wet-SCFM) 5,156 Flowrate (Standard Dry-DSCFM) 4,581

Dercnzo and Associates, Inc.
StackDiameter (in.) 15.50 Md 30.09 Traverse points 12 Ms 28.81 Operator TS/DW Moisture Content (%) 10.6

Traverse Traverse

Point Stack Temp. Velocity Pres. Point Stack Temp. Velocity Pres. Number (°F) (“H20) Number (°F) (“H20) Side A Side B

1 877 3.00 1 873 3.30 2 878 3.30 2 879 3.60 3 877 3.30 3 876 3.70 4 880 3.60 4 875 3.60 5 879 3.30 5 873 3.50 6 878 3.40 6 874 3.40 Average 878 3.32 875 3.52

Average Velocity Pressure (“H20) 3.417

Average Velocity Pressure Sqrt (“H20) 1.848

Stack Pressure (“Hg) 30.68

Stack Gas Specific Gravity (Gs) 0.99

Average Stack Temperature (“F) 877

Average Stack Velocity (Ths) 163.2

Average Stack Velocity (fpm) 9790.2

Area of Stack (ft 2) 1.310

Flowrate (Actual-.CFM) 12,829

Flowrate (Standard Wet-SCFM) 5,197

Flowrate (Standard Dry-DSCFM) 4,647

Derenzo and Associates, Inc.
er (in.) 15.50 Md Traverse 30.09 points 12 Ms Operator 28.81 TS/DW Moisture Content (%) 10.6

Traverse Traverse Point Stack Temp. Velocity Pres. Point Stack Temp. Velocity Pres. Number (°F) (H2O) Number (°F) Side A (“H20) Side B 1 878 3.20 1 873 3.00 2 876 3.40 2 878 3.40 3 876 3.60 3 879 3.60 4 873 3.50 4 879 3.60 5 878 3.40 5 876 3.50 6 872 3.50

Average 6 873 3.00 876 3.43 876 3.35

Average Velocity Pressure (‘H20) 3.3 92

Average Velocity Pressure Sqrt (‘H20) 1.841

Stack Pressure (“Hg) 30.64

Stack Gas Specific Gravity (Gs) 0.99

Average Stack Temperature (°F) 876

Average Stack Velocity (fps) 162.6

Average Stack Velocity (Thm) 9756.8

Area of Stack (ft 2) 1.310Flowrate (Actual-CFM) 12,785

Flowrate (Standard Wet-SCFM) 5,175

Flowrate (Standard Dry-DSCFM) 4,628

Derenzo and Associates, Inc.
Derenzo and Associates, inc.

Company Trail Ridge Energy

Source Designation ICE #4 Exhaust

Test Date 3/25/2009 Assumed Moisture (Bws) 13

Test Number TREP-I Condensate Volume (Vie) 100.7

Operator TS’D\V Silica Gel Weight Gain (Vie) 11.0

Filter Number 124087 Nozzle Diameter (in.) 0.19

Barometric Pressure (Pb) 30.13 Leak Rate Initial 0.006

@ 15”

Stack Static Pressure (Ps) 7.70 Leak Rate Final 0.000 @5’

Stack Dimensions (in.) 5.5 Traverse points 12

Pitot Tube Number SF Pitot Corr. Factor (Cp) 0.84

Meter

fvleter Number Ni Meter Corr. Factor (Y) 1.002

I iso. Factor (Kiso) 823.534 Method 3A Results (%)

Delta H@ 2.026 CO, 10.86

0, 8.28

Traverse

Point

Sampling Time Sampling Stack Temp. Velocity Pres. Orifice Sample Volume Dry Gas Meter Temp. Probe Filter Box Last Impinger

(Minutes) Clock Time Train Vuc. (nF)

Number

(“H,O) Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature

o (24 hour) (Hg) Ts Delta

P (“H.O) Delta

H Vm (°F) Tm (°F) Tm (°F) (°F) (°F)

21

50 8:05:00

3 890 3.30 1.68 307.855 78 77 252 250 60

3 [0

8:10:00

3 895 3.60 1.83 311.27 79 78 253 253 61

4 15 8:20:00

8:15:00

3 892 3.60 1.84 3)4.79 81 78 253 252 62

5 20 8:25:00

3 894 3.50 1.79 318.38 83 79 253 251 63

6 25 830:00

3 892 3.50 1.80 321.87 85 79 253 250 65

off 30 835:00

3 894 3.40 1.74 325.36 86 79 254 251 64 - - - - 328.817 - - - - -

2I 30

35 8:45:00

8:40:00

3 880 3.20 1.65 328.817 82 80 253 250 62

3 40 8:50:00

33 882 3.20 1.66 332.18 86 80 253 252 62

4 45 8:55:00

885 3.30 1,71 335.55 88 80 252 251 57

5 50 9:00:00

3 883 3.50 1.82 339.02 89 81 254 251 56

6 55 0:05:00

3 886 3.40 1,77 342.52 91 81 254 251 56

off 60 9:10:00

3 885 3.10 1.6! 346,01 91 82 255 251 57 - - - - 340,388 - - - -

?verage 60

-

888.2 3.38 1.74 41.533 85 80 253 251 60
Derciazo and Associates, Inc.

Company Trail Ridge Energy

Source Designation ICE #4 Exhausl

Test Date 3/25)2009 Assumed Moisture (Bsvs) 13

Test Number TREP-2 Condensate Volume (Vie) 98.9

Operator TS/DW Silica Gel Weight Gain (Vie) 13.7

Filter Number 124088 Nozzle Diameter (in.) 0.19

Barometric Pressure (Pb) 30.13 Leak Rate Initial 0.000

@ 15”

Stack Static Pressure (Ps) 7.50 Leak Rate Final

Stack Dimensions

0.000 @7

(in.) 15.5 Traverse points 12

Pilot Tube Number 5F Pitot Corr. Factor (Cp)

Meter

0.84

Meter

Number N-i Meter Corr. Factor (Y) 1.0021

iso. Factor (lOso) 1823.534 Method 3A Results (%) Delta H@ 2.026 CO2 10.94 O 8.29

Traverse

Point (Minutes)

Sampling

Clock

Time

Time

Sampling Stack Temp. Velocity Pres. OrifIce Sample Volume Dry Gas Meter Temp. Probe Ftlter Box Last Impmger

Train Vac. (°F) (“H.O) Differential

Number

(cubic feet) Inlet Outlet Temperature Temperature Temperature

o (24 hour) (Hg) Ts Delta

P (“HO) Delta

H Vm (°F) Tm (°F) Tm (°F) (°F) (°F)

21

50

9:53:00

9:48:00

3 883 3.20 1.65 349.474 82 81 242 252 63

3 tO 9:58:00

3 886 3.20 1.06 352.81 87 82 248 251 61

4 15 10:03:00

3 888 3.40 1.77 356.08 91 83 251 253 63

5 20 10:08:00

4 889 3.70 1.93 359.55 94 83 252 251 62

6 25 10:13:00

3 897 3.50 tOt 363.21 96 84 252 252 63

off 30 10:18:00

3 893 3.50 1.82 366.7t 96 85 253 251 64 . - - - 370.939 - . . - -

2I

35

30

10:20:00

10:23:00

3 883 3.00 1.57 370.939 90 86 253 250 62

3 40 10:33:00

3 886 3.30 1.73 373.56 95 87 252 252 64

4 45 10:38:00

33

889 3.50 1.83 377.01 96 87 252 252 60

5 50 10:43:00

3

889 3.40 1.78 380.51 97 87 252 252 60

6 55 10.48:00

890 3.50 t.84 384.02 98 88 254 252 61

off 60 10:53:00

3.

892 3.30 1.73 387.52 99 88 253 251 61 - - - 391.003 - - -

Average 60

-

888.8 3.38 1.76 41.53 93 85 251 252 62
Derenzo and Associates, Inc.

Company Trail Ridge Energy

Source Designation ICE #4 Exhaust

Test Date 3/25/2009 Assumed Moisture (Bws)

Test Number 13

TREP-3 Condensate Volume (VIe)

Operator

80.3

TS/D\V Silica Gel Weight Gain (VIc)

Filter Number 21.2

124089 Nozzle Diameter (in.)

Barometric 0.19

Pressure (Pb) 30.13 Leak Rate Initial

Stack Static Pressure

0.000 IS

(Ps) 7.50 Leak Rate Final

Stack Dimensions

0.000

@ 5’

(in.) 5.5 Traverse points

Pitot Tube Number

12

SF Pitot Corr. Factor (Cp)

Meter Number

0.84

N-I Meter Corr. Factor (Y)

Meter

1.0021

iso. Factor (Kiso) 1823,534 Method 3A Results (%) Delta H@ 2.026 CO2 10.96

02 8.30

Traverse

Point

Sampling Time Sampling Stack Temp. Velocity Pres. Orifice Sample Volume Diy Gas Meter Temp. Probe Filter Box Last Impinger

(Minutes) Clock Time Train Vac. (nF) (‘ffO) Differential

Number

n (24 boar)

(cubic feet> Inlet Outlet Temperature Temperature Temperature

(‘l-Ig) Ts Delta

P CHO) Delta

H Vm (°F) Tm (°F) Tm (°F) (°F) (°F)

1

0 11:35:00

3 878 3.20 1.67 391.180 86 86 245 250 66

2

S 11:40:00

3 10 11:45:00

33 879 3.50 1.83 394.72 90 86 252 251 64

879 3,70 1.95 398,27 94 86 253 252 60

4 15 11:50:00

3 881 3.40 1.79 402,09 92 87 251 252 58

5 20

1 :55:00

3 880 3.40 1.79 405.50 98 87 252 252 57

a 25 12:00:00

3 878 3.50 1,86 408.95 100 88 254 252 57

off 30 12:05:00

-

-

-

- 412.577

-

-

-

-

-

I 30 12:10:00

3 883 3.10 1.63 412,577 92 88 252 250 62

2 35 12.15:00

3 878 3.30 1.75 415.900 98 89 255 252 59

3 40 12:20:00

3 872 3.50 1.87 419.40 100 90 253 251 59

4 45 12:25:00

3 875 3.60 1.92 423.02 102 90 254 251 59

5 50 12:30:00

3 886 3.50 1.85 426.64 102 91 253 251 59

Ii 55 12:35:00

3 879 3.30 1.76 430.20 103 91 254 250 60

off 60 240:00

-

-

-

- 433.701

-

-

.

-

0

Average 60 879.0 3.42

I 01 42.52 96 88 252 251 60

Dcrenzo and Associates, Inc.

Company Trail Ridge Energy

Source Designation ICE 8 4 Exhaust

Test Date 3/25/2009 Assumed Moisture (Bws) 13

Test Nunsber TREHCL-1 Condensate Volume (VIe) 94.9

Operator TS/DW Silica Gel Weight Gain (Vie) 13.2

Filter Number N/A Nozzle Diameter (in.) 0.185

Barometric Pressure (Pb) 30.13 Leak Rate Initial 0.000 @ 15”

Stack Static Pressure (Ps) 7.70 Leak Rate Final 0.000 @ 15”

Stack Dimensions (in.) 15.5 Traverse points 12

Pitot Tube Number SF Pitot Corr. Factor (Cp) 0.84

Meter Number N-I Meter Corr. Factor (Y) 1.0021

Meter iso. Factor (Kiso) 1823.534 Method 3A Results (°/)

Delta H@ 2.026 (Analyzer) CO2 10.91

(Analyzer) 02 8.27

Traverse

Point (Minutea)

Sampling

Clock

time

Time

Sampling Stack Temp. Velocity Pres. Orifice Sample Volume Ore Gas Meter Temp. Filler Box Probe Iautlmpinger

Train \‘ac. (°F)

Number 0

(‘H,O) Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature

(24 hour) (“Hg) Ta Delta P (‘l-LO) Delta H Vm (°F Tm (°F Tm (°F) (°

2

1

5

0

14:14:00

14:09:00 2 879 3.10 1.47 434.546 91 90 245 253 67

3 10 14:19:00

3 879 3.20 1.52 437.76 94 90 247 253 61

4 15 14:24:00

3 887 3.30 1.56 440.98 98 91 249 253 61

5 20 14:29:00 3

3 878 3.40 1.62 444.25 100 91 251 252 63

6 25 14:34:00 3

881 3.50 1.67 447.62 102 91 251 252 65

off 30 14:39:00 -

887 3.40 1.62 450.97 103 92 253 251 63

- - - 454.335 - - - - -

2

1

35

30 14:44:00

14:49:00 3

3 879 3.00 1.42 454.335 94 91 252 250 57

3 40 14:54:00 3

877 3.20 1.53 457.58 100 92 253 253 65

4 45 14:59:00 3

883 3.60 1.72 460.99 101 92 253 252 66

5 50 15:04:00 3

881 3.50 167 464.36 102 92 253 251 61

6 55 15:09:00

875 3.40 1.63 467.76 103 92 254 250 63

off 60 15:14:00

3

-

881 3.40 1.62 471.09 102 93 254 251 60

- - - 474.396 - - - -

Average 60

-

880.6 3.33 1.59 39.850 99 91 251 252 63
Dcrenzo and Associates, Inc.

Company Troll Ridge Energy

Source Designation ICE #4 Exhaust

Test Date 3/25i2009 Assumed Moisture (Bws) 13

Test Number TREHCL-2 Condensate Volume (VIe) 156.6

Operator TS)DW Silica Gel Weight Gain (VIe) 35.7

Filter Number N/A Nozzle Diameter (in.) 0.25

Barometric Pressure (Pb) 30.13 Leak Rate Initial 0.000 @ 15”

Stack Static Pressure (Ps) 7.60 Leak Rate Final 0.000 @ 5”

Stack Dimensions (in.) 15.5 Traverse points 12

Pilot Tube Number 5F Pilot Corr. Factor (Cp) 0.84

Meter Number N-I Meter Corr. Factor (Y) 1.0021

Meter iso. Factor (Kiso) 1823.534 Method 3A Results (%)

Delta l1@ 2.026 (Analyzer) CO2 10.95

(Analyzer) 02 8.24

Traverse Sampling Time Sampling Slack Temp. Velocity Pres. Orifice Sample Volume Dry Gas Meter Temp. Filter Box Probe Last linpinger

Point (Minutes) Clock Time Train Vac. (“F) (“H,O) Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature

Number 0 (24 hour) (Hg) Ts Delta P (“H,O) Della H Vm (“F) Tm (°F) Tm (“F) (“F) (°F)

I 0 16:05:00 6 875 3.00 4.77 475.742 91 89 248 251 63

2 5 16:10:00 7 883 3.30 5.25 481.56 97 90 251 252 63

3 10 16:15:00 7 877 3.30 5.30 487.61 103 90 251 253 62

4 15 16:20:00 7 888 3.40 5.44 493.61 106 92 252 252 64

5 20 16:25:00 8 888 3.20 5.13 499.91 107 92 253 252 62

6 25 16:30:00 7 892 3.40 5.44 505.13 107 93 254 251 61 off 30 16:35:00 - - - 512.439 - - - -

I 30 16:41:00 7 879 3.20 5.12 512.439 96 93 255 250 60

2 35 16:46:00 7 884 3.50 5.61 518.53 103 93 253 252 60

3 40 16:51:00 8 891 3.50 5.60 524.81 106 93 253 251 61 4 45 16:56:00 8 883 3.60 5.80 531.19 109 94 254 252 60

5 50 17:01:00 7 887 3.50 5.64 537.57 110 95 254 52 61 6 55 17:06:00 7 890 3.30 5.31 543.89 110 95 255 251 63

off 60 17:11:00 - - - - 550.382 - - - -

Average 60 884.8 3.35 5.37 74.640 104 92 253 235 62
Dercnzo and Associates, Inc.

Company Trail Ridge Energy

Source Designation ICE #4 Exhaust

Test Date 3/25/2009 Assumed Moisture (lSws) 13

Test Number TREI-{CL-3 Condensate Volume (VIe) 148.5

Opcrator TS/DW Silica Gel Weight Gain (VIe) 33.4

Filter Number N/A Nozzle Diameter (in.) 0.25

Barometric Pressure (Pb) 30.13 Leak Rate Initial 0.000 @ 15”

Stack Static Pressure (Ps) 7.50 Leak Rate Final 0.000 @ 10’

Stack Dimensions (in.) 15.5 Traverse points 12

Pilot Tube Number SF Pilot Corr. Factor (Cp) 0.84

Meter Number N-I Meter Corr. Factor (Y) 1.0021

Meter iso. Factor (Kiso) 1823.534 Method 3A Results (%)

Delta H@ 2.026 (Analyzer) CO1 10.98

(Analyzer) 02 8.22

Traverse Sampling Time Sampling Stack Temp. Velocity Pres. Orifice Sample Volume Dry Gas Meter Temp. Filter Box Probe Last Impinger

Point (Minutes) Clock Time Train Vac. (°F) (“HQ) Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature

Number 0 (24 hour) (“Hg) Ts Delta P (“H20) Delta H Vni (°F Tm (°F Tm (°F) (°F (°F)

I 0 17:57:00 7 881 3.00 4.76 550.665 92 90 252 250 59

2 5 18:02:00 7 888 3.30 5.24 556.48 100 90 254 252 56

3 10 18:07:00 7 884 3.30 5.29 562.49 106 91 254 252 58

4 15 18:12:00 7 887 3.60 5.78 568.76 108 92 254 252 61

5 20 18:17:00 7 885 3.30 5.31 574.98 108 93 254 251 62

5 25 18:22:00 7 896 3.40 5.43 581.22 109 94 255 252 63

off 30 18:27:00 - . . - 587.533 - . - - -

I 30 18:31:00 7 886 3.30 5.25 587.533 97 93 253 250 61

2 35 18:36:00 7 884 3.60 5.77 593.660 104 93 252 252 60

3 40 18:41:00 7 888 3.70 5.93 599.96 106 93 255 252 63

4 45 18:46:00 9 883 3.60 5.80 606.92 107 94 255 251 61

5 50 18:51:00 9 888 3.50 5.62 612.88 108 94 255 251 61

6 55 18:56:00 9 887 3.40 5.48 619.63 108 94 253 251 62

off 60 19:01:00 - . . - 625.615 . . - .

Average

-

60 886.4 3.42 5.47 74.95 104 93 254 251 61
ON —

— U. 0— U. U. DC

_so—, U.DCDC

0 .U UJ -

p

0flP ONONU

0 0 0 0 U. 

—4

‘0
Test 1 Test 2 Test 3 Average CO concentration = 646.1 648.9 653.1 ppmv

Average pre-test and post-test instrument zero = 0.24 0.28 1.26 ppmv

Average pre-test and post-test instrument calibration 601.2 600.6 603.6 ppmv

Midrange calibration gas concentration = 604.5 604.5 604.5 ppmv

Volumetric flow rate = 4,593 4,574 4,669 dscfm

Average generator kilowatt output = 1,551 1,581 1,598 kW

CO CONCENTRATION CORRECTED FOR CALIBRATION AND ZERO DRIFT

Cd(CO conc.-Avg. zero)x(Cal. gas conc.)/(Avg. cal-Avg. zero) = 649.7 653.1 654.2 ppmv

CO EMISSION RATE

(Cd) (Qdstd) (60 min!hr) (MW 0I (V) 13.03 13.04 13.33 lb/hr

where:

Cd = observed CO concentration, dry basis (ft 3 CO / 106 ft3 stack gas) Qstd stack gas flowrate (dscfm)

MW0 molecular weight CO (28.0 ib/Ib-mol)

VM = molar volume of ideal gas at std conditions (385 ft3Ilb-mol)

Engine Output (bHp) = (kWavg)/(O.96)/(O.7457 kWfbHp) = 2167 2208 2233 bHp

where:

kWavg = average recorded generator kilowatt output 0.96 = engine to generator efficiency

0.7457 = conversion factor, kilowatts to brake horsepower

(Ec 0)(453.6 g/ib) /(bHp) 2.73 2.68 2.71 g/bHp*hr

where:

E0 = CO emission rate (lb/hr)

453.6 = conversion factor, grams to pounds bHp = engine brake horsepower
Average Test 1 Test 2 Test 3 NOx concentration = 65.1 64.0 68.1 ppmv Average pre-test and post-test instrument zero = 0.66 1.00 0.77 ppmv Average pre-test and post-test instrument calibration = 99.1 99.9 100.1 ppmv

Midrange calibration gas concentration = 96.3 96.3 96.3 ppmv

Volumetric flow rate = 4,593 4,574 4,669 dscfm

Average generator kilowatt output 1,551 1,581 1,598 kW

NOx CONCENTRATION CORRECTED FOR CALIBRATION AND ZERO DRIFT

Cd = (NOx cone-Avg. zero)x(CaI. gas conc.)/(Avg. cal-Avg. zero) = 63.1 61.3 65.2 ppmv

NOx EMISSION RATE. AS NO.,

ENOX = (Cd) (Qdstd) (60 minfbr) (MWN 0,)/ (VM)

= 208 2.01 2.18 lb/hr as NO, where:

Cd = observed NOx concentration, dry basis (ft 3 NOx / 106 ft3 stack gas) Qdstd = stack gas flowrate (dscfm)

MWNOX = molecular weight NO, (46.0 ib/Ib-mol)

VM = molar volume of ideal gas at std conditions (385 fl3/lb-mol)

Engine Output (bHp) = (kWavg)/(O.96)/(0.7457 kW/bHp)

= 2167 2208 2233 bHp where:

kWavg = average recorded generator kilowatt output 0.96 = engine to generator efficiency 0.7457 = conversion factor, kilowatts to brake horsepower

(EN0X) (453.6 g/Ib) / (bHp)

0.43 0.41 0.44 g/bHp*hr

where:

ENOX = NOx emission rate (lb/hr)

453.6 = conversion factor, grams to pounds bHp = engine brake horsepower
Average pre-test and post-test instrument zero = 0.00 0.00 0.00 0.02 0.07 0.10 %

Average pre-test and post-test instrument calibration = 13.34 13.37 13.48 13.57 13.57 13.57 %

Midrange calibration gas concentration 13.52 13.52 13.52 13.52 13.52 13.52 %

CO, CONCENTATION CORRECTED FOR CATJBRATION AND ZERO DRIFT(CO 2cone-Avg. zero)x(Cal. gas conc.)/(Avg. cal-Avg. zero) 10.9 10.9 11.0 10.9 10.9 11.0 %
Average 02 concentration

Average pre-test and post-test instrument zero =

Average pre-test and post-test instrument calibration =

Midrange calibration gas concentration =

8.29 830 8.30 8.27 8.25 8.24 %

0.01 0.01 0.01 0.01 0.01 0.01 %

8.29 8.30 8.28 8.28 8.29 8.30 %

8.28 8.28 8.28 8.28 8.28 8.28 %

0, CONCENTATION CORRECTED FOR CALIBRATION AND ZERO DRIFT

8.28 8.29 8.30 8.27 8.24 8.22 % (02 conc.-Avg. zero)x(Cal. gas conc.)/(Avg. cal-Avg. zero) =
g

ured THC concentration, as propane

Average pre-test and post-test instrument zero

Average pre-test and post-test instniment calibration

Midrange calibration gas concentration

Methane Concentration (as methane)

THC Concentration Corrected for Calibration and Zero Drift

(THC conc.-Avg. zero)x(Cal. gas conc.)/(Avg. cal.-Avg. zero) as propane

VOC Concentration (THC with methane subtraction)

VOC EMISSION RATE, AS PROPANE

= (Cd) (Qdstd) (60 mm/br) (MWvc) / (VM)

where:

-0.84 -0.33 -0.47 lb/hi, as propane

Cd = observed VOC concentration, dry basis (ft 3 VOC / 106 ft3 stack gas) Qastd = stack gas flowrate (dscfm)

MWvx = molecular weight methane (16.0 Ib/Ib-mol)

VM = molar volume of ideal gas at std conditions (385 ft3/lb-mol)

Engine Output (bHp) (kWavg)/(0.96)/(0.7457 kWIbHp)

where:

kWvg = average recorded generator kilowatt output 0.96 = engine to generator efficiency 0.7457 = conversion factor, kilowatts to brake horsepower

(Evoc) (453.6 g/Ib) / (bHp)

where:

= 2167 2208 2233 bHp

= -0.18 -0.07 -0.10 g/bHp*hr

VOC emission rate (lb/br) 453.6 = conversion factor, grams to pounds bHp = engine brake horsepower

= 560.2

0.08

521.40

523.2

= 1,883

641.7

0.08

527.86

523.2

1,986

623.3

0.08

531.40

523.21,951

ppmv (wet)

ppmv

ppmv

ppmv

ppmv (wet)

= 562.17 636.13 613.71 ppmv (wet)

THC -Methane

Volumetric tow rate

Average generator kilowatt output

= -65

= 5,182

= 1,551

-26

5,174

1,581

-37

5,211

1,598

ppmv wet, as propane

scfm

kW
0.08 2.58 0.29 0.39 -0.07 0.79 0 12.56 3/24/2009 13:08 0.08 2.61 0.29 0.4 -0.07 0.44 0 12.47

3/24/2009

3/24/2009 13:09 0.08 2.61 0.3 0.4 -0.07 1.05 0 12.44

3/24/2009

13:10 0.08 2.46 0.31 0.41 -0.06 1.72 0.01 12.44

3/24/2009

13:11 0.08 2.63 0.3 0.4 -0.07 1.82 0.01 12.43

3/24/2009

13:12 0.08 2.66 0.31 0.4 -0.07 1.92 0.01 12.36

3/24/2009

13:13 0.09 2.61 0.3 0.4 -0.07 1.84 0.01 9.31

3/24/2009

13:14 0.08 2.62 0.3 0.4 -0.07 2.25 0.01 8.31

3/24/2009

13:15 0.08 2.7 0.32 0.4 -0.07 2.46 0.01 8.24

3/24/2009

13:16 0.09 2.69 0.31 0.41 -0.07 3.16 0.02 4.49

3/24/2009

13:17 0.09 2.68 0.31 0.4 -0.07 3.43 0.02 0.29

3/24/2009

13:18 0.09 2.7 0.32 0.41 -0.06 3.31 0.02 0.01

3/24/2009

13:19 0.08 2.67 0.31 0.41 -0.06 3.8 0.02 0.01 13:20 0.09 2.72 0.32 0.41 -0.06 4.66 0.02 13.03

3/24/2009

3/24/2009 13:21 0.09 2.62 0.3 0.4 -0.07 4.71 0.02 20.6

3/24/2009

13:22 0.09 2.57 0.3 0.4 -0.07 5.09 0.02 20.94 13:23 0.08 2.64 0.3 0.4 -0.06 5.1 0.02 21.02

3/24/2009

3/24/2009 13:24 0.09 2.68 0.31 0.4 -0.06 5.64 0.03 21.05

3/24/2009

13:25 0.08 2.63 0.31 0.41 -0.06 5.59 0.03 21.05

3/24/2009

13:26 0.08 2.64 0.32 0.41 -0.06 5.88 0.03 15.98

3/24/2009

13:27 0.09 2.62 0.32 0.41 -0.06 5.81 0.03 12.64

3/24/2009

13:28 0.09 2.6 0.31 0.41 -0.06 6.12 0.03 12.47

3/24/2009

13:29 0.08 2.65 0.31 0.41 -0.06 6.82 0.03 12.43

3/24/2009

13:30 0.08 2.62 0.31 0.41 -0.06 6.89 0.04 12.42

3/24/2009

13:31 0.08 2.6 0.31 0.41 -0.06 7.15 0.04 11.52

3/24/2009

13:32 0.08 2.6 0.3 0.41 -0.06 7.74 0.04 8.5 13:33 0.08 2.62 0.3 0.4 -0.06 7.18 0.04 8.26 3/24/2009 13:34 0.09 2.66 0.31 0.41 -0.06 7.67 0.04 8.23

3/24/2009

3/24/2009 13:35 0.09 2.66 0.31 0.41 -0.06 7.63 0.04 5.67

3/24/2009

13:36 0.08 2.61 0.31 0.41 -0.06 8.21 0.04 0.41

3/24/2009

13:37 0.08 2.46 0.31 0.41 -0.06 8.42 0.04 0.01

3/24/2009

13:38 0.08 2.57 0.31 0.41 -0.06 8.4 0.04 0.01

3/24/2009

13:39 0.09 2.66 0.31 0.41 -0.06 8.09 0.04 0.01

3/24/2009

13:40 0.08 2.65 0.31 0.41 -0.06 8.61 0.04 0.01

3/24/2009

13:41 0.09 2.67 0.31 0.4 -0.06 9.02 0.04 0.01

3/24/2009

13:42 0.09 2.66 0.32 0.4 0.05 9.43 0.05 0.01

3/24/2009

13:43 0.08 2.63 0.3 0.4 0.02 9.46 0.05 0.5 13:44 0.08 2.64 0.31 0.4 -0.06 9.44 0.05 17.55

3/24/2009

3/24/2009 13:45 0.08 2.65 0.31 0.41 -0.06 9.65 0.05 20.71 13:46 0.08 2.63 0.31 0.41 -0.06 9.93 0.05 20.94 3/24/2009

3/24/2009

13:47 0.08 2.63 0.31 0.41 -0.06 10.18 0.05 20.99 13:48 0.09 2.67 0.32 0.41 -0.06 10.26 0.05 21.01

3/24/2009

3/24/2009 13:49 0.09 2.66 0.31 0.41 -0.06 10.55 0.05 21.03

3/24/2009

13:50 0.08 2.67 0.31 0.41 -0.06 10.51 0.05 21.03

3/24/2009

13:51 0.09 2.68 0.31 0.41 -0.06 10.56 0.05 21.03

3/24/2009

13:52 0.08 2.72 0.32 0.41 -0.06 10.92 0.05 21.03

3/24/2009

13:53 0.09 2.69 0.31 0.41 -0.06 10.95 0.05 19.8 13:54 0.08 2.67 0.32 0.41 -0.06 11.05 0.05 13.17
0.31 0.41 -0.06 12.3 0.06 8.21 3/24/2009 14:04 0.08 2.41 0.31 0.41 -0.05 12.54 0.06 3.52 3/24/2009 14:05 0.08 2.41 0.32 0.41 -0.07 12.33 0.06 0.18 3/24/2009 14:06 0.09 2.05 0.33 0.42 -0.05 12.37 0.06 0.01 3/24/2009 14:07 0.08 2.52 0.29 0.4 -0.07 637.68 8.55 6.07 3/24/2009 14:08 0.08 1.71 0.36 0.43 -0.04 1023.28 15.29 12.32 3/24/2009 14:09 0.09 2.31 0.31 0.41 -0.06 1024.68 15.35 12.59 3/24/2009 14:10 0.08 2.1 0.32 0.42 -0.05 607.12 9.92 9.28 3/24/2009 14:11 0.08 2.08 0.33 0.42 -0.05 23.23 0.41 0.77 3/24/2009 14:12 0.09 1.53 0.38 0.44 -0.03 13.46 0.14 0.06 3/24/2009 14:13 0.08 1.83 0.37 0.44 -0.04 13.27 0.12 0.01 3/24/2009 14:14 0.07 1.77 0.37 0.43 -0.04 13.56 0.11 0.01 3/24/2009 14:15 0.09 2.31 0.33 0.42 -0.05 13.54 0.1 0.01 3/24/2009 14:16 0.09 1.7 0.29 0.38 -0.11 13.78 0.1 0.01 3/24/2009 14:17 0.09 2.03 0.36 0.43 -0.04 336.03 4.09 2.27 3/24/2009 14:18 0.08 2.56 0.32 0.41 -0.06 1019.48 15.15 11.93 3/24/2009 14:19 0.09 2.65 0.3 0.41 -0.06 1026.12 15.35 12.53 3/24/2009 14:20 0.08 2.66 0.3 0.41 -0.06 1025.42 15.37 12.63 3/24/2009 14:21 0.07 2.64 0.3 0.4 -0.06 372.6 6.42 6.58 3/24/2009 14:22 0.09 2.62 0.29 0.4 -0.06 17.3 0.23 0.41 3/24/2009 14:23 0.09 2.62 0.29 0.4 -0.06 15.24 0.16 0.02 3/24/2009 14:24 0.08 2.63 0.29 0.4 -0.07 15.08 0.14 0.01 3/24/2009 14:25 0.08 2 0.29 0.38 -0.09 49.99 0.4 0.04 3/24/2009 14:26 0.09 1.65 0.37 0.43 -0.04 923.33 13.1 9.45 3/24/2009 14:27 0.08 1.43 0.38 0.43 -0.04 1027.46 15.34 12.44 3/24/2009 14:28 0.08 1.82 0.36 0.42 -0.05 1028.09 15.37 12.61 3/24/2009 14:29 0.08 2.52 0.31 0.4 -0.06 1028.02 15.38 12.65 3/24/2009 14:30 0.09 1.96 0.35 0.42 -0.05 1027.81 15.39 12.66 3/24/2009 14:31 0.08 1.7 0.37 0.43 -0.04 1028.16 15.4 12.67 3/24/2009 14:32 0.08 2.52 0.31 0.41 -0.06 1028.66 15.41 12.67 3/24/2009 14:33 0.09 2.11 0.33 0.41 -0.06 1028.91 15.41 12.67 3/24/2009 14:34 0.09 2.53 0.3 0.4 -0.06 548 9.07 8.62 3/24/2009 14:35 0.08 2.41 0.31 0.4 -0.07 22.09 0.4 0.63 3/24/2009 14:36 0.08 2.29 0.32 0.41 -0.06 16.56 0.22 0.04 3/24/2009 14:37 0.09 2.25 0.32 0.41 -0.06 16.6 0.19 0.01 3/24/2009 14:38 0.08 2.54 0.3 0.4 -0.06 16.64 0.17 0.01 3/24/2009 14:39 0.08 1.54 0.38 0.43 -0.04 404.86 0.29 0.54 3/24/2009 14:40 0.08 2.34 0.31 0.41 -0.06 1048.34 0.16 0.11 3/24/2009 14:41 0.09 2.51 0.28 0.39 -0.08 1033.18 0.14 0.01 3/24/2009 14:42 0.08 1.63 0.34 0.41 -0.06 1015.25 0.13 0.01 3/24/2009 14:43 0.09 1.52 0.35 0.41 -0.05 1015.05 0.12 0.01 3/24/2009 14:44 0.09 2.38 0.28 0.39 -0.08 896.13 0.11 0.01 3/24/2009 14:45 0.08 2.46 0.28 0.39 -0.08 614.96 0.11 0.01 3/24/2009 14:46 0.07 2.12 0.31 0.4 -0.07 609.69 0.11 0.01 3/24/2009 14:47 0.09 1.48 0.36 0.42 -0.05 606.97 0.11 0.01 3/24/2009 14:48 0.08 1.47 0.4 0.45 -0.02 168.09 9.12 0.22 3/24/2009 14:49 0.08 2.15 0.35 0.43 -0.05 15.72 13.93 0.01 3/24/2009 14:50 0.09 231 0.33 0.42 -0.06 15.53 13.59 0.01

2
0.3 0.41 -0.06 16.83 0.17 20.74 3/24/2009 15:00 0.08 2.57 0.3 0.41 -0.06 16.96 0.16 20.91 3/24/2009 15:01 0.08 2.31 0.33 0.42 -0.05 16.89 0.14 20.96 3/24/2009 15:02 0.09 2.59 0.31 0.42 -0.05 17.18 0.14 20.97 3/24/2009 15:03 0.08 2.58 0.3 0.41 -0.06 17.11 0.13 20.97 3/24/2009 15:04 0.09 2.6 0.31 0.41 -0.06 0.75 0 21.01 3/24/2009 15:05 0.09 2.57 0.3 0.41 -0.05 0.05 0 21.01 3/24/2009 15:06 0.08 2.57 0.3 0.41 -0.06 0.1 0 19.43 3/24/2009 15:07 0.08 2.6 0.32 0.42 -0.05 0.08 0 11.48 3/24/2009 15:08 0.09 2.48 0.32 0.42 -0.06 -0.02 0 9.56 3/24/2009 15:09 0.09 1.72 0.37 0.44 -0.04 0.08 0 9.4 3/24/2009 15:10 0.08 2.54 0.3 0.41 -0.06 0.06 0 9.35 3/24/2009 15:11 0.09 2.53 0.3 0.41 -0.06 0.11 0 9.32 3/24/2009 15:12 0.09 2.41 0.31 0.41 -0.06 0.45 0 8.83 3/24/2009 15:13 0.09 2.55 0.29 0.41 -0.06 0.14 0 8.24 3/24/2009 15:14 0.09 2.39 0.31 0.41 -0.06 0.18 0 8.22 3/24/2009 15:15 0.09 1.41 0.55 0.44 0.43 0.16 0 8.22 3/24/2009 15:16 0.09 1.82 0.35 -0.21 0.86 0.39 0 8.55 3/24)2009 15:17 0.08 2.48 0.3 0.41 0.43 0.56 0 8.26 3/24/2009 15:18 0.09 1.65 3.22 1.76 2.12 0.46 0 7.9 3/24/2009 15:19 0.09 1.48 52.6 27.48 25.15 0.45 0 1.15 3/24/2009 15:20 0.09 1.63 199.1 184.21 15.63 0.5 0 0.06 3/24/2009 15:21 0.09 1.39 262.77 258.36 4.73 0.19 0 0.01 3/24/2009 15:22 0.09 1.41 248.21 248.73 -0.19 0.62 0 0.01 3/24/2009 15:23 0.09 1.48 236.53 239.19 -0.21 0.55 0 0.01 3/24/2009 15:24 0.08 2.27 106.55 108.52 0.54 0.99 0 0.01 3/24/2009 15:25 0.09 2.48 98.11 97.24 0.93 0.49 0 0.01 3/24/2009 15:26 0.09 2.27 97.86 97.07 0.92 0.83 0 0.01 3/24/2009 15:27 0.08 2.66 97.85 97.06 0.42 1.05 0 0.01 3/24/2009 15:28 156.5 419.17 50.9 58.62 -4.91 137.81 0.8 6.12 3/24/2009 15:29 13.53 1273.78 11.58 7 4.52 82.44 0.67 18.58 3/24/2009 15:30 14.13 491.79 1.53 0.41 0.91 2.33 0.02 20.69 3/24/2009 15:31 47.96 26.75 1.63 2.28 -0.66 97.55 0.19 20.15 3/24/2009 15:32 0.24 6.21 1.41 1.09 0.44 580.76 0.08 2.89 3/24/2009 15:33 0.09 4.03 0.79 0.41 0.43 593.12 0 0.37 3/24)2009 15:34 0.08 1.84 0.84 0.43 0.45 593.29 0 0.03 3/24/2009 15:35 0.09 2.23 0.82 0.42 0.44 593.7 0 0.01 3/24/2009 15:36 0.09 2.73 0.8 0.41 0.43 650.28 0 0.01 3/24/2009 15:37 0.08 2.69 0.54 0.41 0.43 986.28 0 0.01 3/24/2009 15:38 0.08 2.71 0.31 0.42 0.44 1015.47 0 0.01 3/24/2009 15:39 0.09 2.41 0.32 0.43 0.45 722.58 0 0.01 3/24)2009 15:40 0.09 2.76 0.3 0.41 0.43 606.84 0 0.01 3/24/2009 15:41 0.08 2.73 0.3 0.41 0.44 606.07 0 0.01 3/24/2009 15:42 0.09 2.68 0.31 0.41 0.43 414.49 2.86 0.01 3/24/2009 15:43 0,09 2.79 0.3 0.41 0.43 5.76 12.87 0.01 3/24/2009 15:44 0.09 2.83 0.3 0.41 0.43 2.2 13.14 0.01 3/24/2009 15:45 0.08 2.84 0.3 0.41 0.43 1.92 13.18 0.01 3/24/2009 15:46 0.09 2.82 0.31 0.41 0.43 1.77 13.33 0.01

3
009

3/24/2009 15:56

15:55 0.08 2.79 89 88.47 0.76 2.09 0.03 1.27

3/24/2009 15:57

0.08 2.41 97.57 99.44 -1.55 2.06 0.01 0.15

3/24/2009 15:58

0.08 1.42 97.93 99.62 -1.53 2.07 0.01 0.01

3/24/2009 15:59

0.09 2.32 97.89 99.6 -1.54 2.21 0 0.01

3/24/2009

0.08 2.79 63.83 69.07 -1.97 1.92 0 0.01

3/24/2009 16:01

16:00 0.09 2.73 1.23 1.05 0.23 2.02 0 0.01

3/24/2009 16:02

0.09 2.54 0.79 0.42 0.44 1.96 0 0.01

3/24/2009 16:03

322.28 2.68 0.3 0.41 0.41 40.01 0.32 0.06

3/24/2009 16:04

543.01 2.79 0.3 0.41 0.2 646.04 9.72 6.35

3/24/2009 16:05

565.37 1448.2 38.35 34 6.78 718.86 11.03 7.9

3/24/2009 16:06

561.04 2007.08 78.67 48.82 29.98 704.12 11.01 8.06

3/24/2009 16:07

560.85 2006.88 84.49 47.11 37.5 713.36 11.04 8.08

3/24/2009 16:08

558.62 2007.55 82.59 41.26 41.18 700.84 11.03 8.12

3/24/2009 16:09

541.07 2007.57 77.63 35.22 42.41 685.99 11.05 8.13

3/24/2009 16:10

554.46 2007.6 80.85 37.29 43.64 706.61 11.11 8.08

3/24/2009 16:11

563.25 2007.59 87.15 39.47 47.8 718.89 11.09 8.08

3/24/2009 16:12

578.77 2007.45 80.65 36.61 44.14 691.91 11.03 8.14

3/24/2009 16:13

578.82 1951.44 77.66 38.57 39.08 677.43 11.01 8.17

3/24/2009 16:14

582.08 1796.87 77.21 36.22 41.2 677.18 11 8.18

3/24/2009 16:15

576.89 1915.46 75.39 34.46 41.17 675.34 11 8.2

3/24/2009 16:16

586.81 2006.68 75.03 37.35 37.87 673.67 11 8.2

3/24/2009 16:17

587.51 2006.6 84.82 57.12 27.81 671.48 10.98 8.22

3/24/2009 16:18

543.84 2006.66 90.83 74.71 16 675.34 10.99 8.21

3/24/2009 16:19

554.2 2006.51 91.95 78.01 14.07 695.93 11.11 8.09

3/24/2009 16:20

582.64 2007.03 96.07 84.98 11.35 705.25 11.05 8.11

3/24/2009 16:21

570.38 2007.5 85.17 74.51 10.85 683.83 10.99 8.19

3/24/2009 16:22

571.69 2007.53 87.56 76.6 11.05 693.56 11.03 8.15

3/24/2009 16:23

582.93 1972.34 84.01 73.86 10.25 687.23 10.98 8.19

3/24/2009 16:24

578.47 1588.52 80.05 68.9 11.2 678.16 10.97 8.21

3/24/2009 16:25

591.24 1749.14 83.08 73 10.21 688.79 10.98 8.21

3/24/2009 16:26

600.02 2006.76 83.68 71.63 12.09 682.25 10.94 8.22

3/24/2009 16:27

587.53 1704.84 81.4 70.57 10.88 680.53 10.93 8.25

3/24/2009 16:28

574.65 1575.47 78.9 66.68 12.4 674.47 10.95 8.24

3/24/2009 16:29

583.26 1487.75 82.66 69.16 13.55 684.88 10.98 8.2

3/24/2009 16:30

573.78 1640.8 80.3 68.13 12.54 680.9 10.97 8.21

3/24/2009 16:31

603.41 2007.43 84.33 71.14 13.56 691.59 10.99 8.18

3/24/2009 16:32

600.09 1751.37 81.05 66.86 14.39 674.91 10.9 8.25

3/24/2009 16:33

595.7 1580.54 80.38 65.15 15.27 676.85 10.92 8.25

3/24/2009 16:34

606.55 1971.99 75.04 61.77 13.47 667.24 10.89 8.28

3/24/2009 16:35

614.78 1925.76 73.37 58.62 15 662.96 10.87 8.3

3/24/2009 16:36

590.5 1632.45 75.17 60.4 14.86 668.36 10.89 8.28

3/24/2009 16:37

609.08 1600.56 76.38 62.23 14.31 671.55 10.93 8.25

3/24/2009 16:38

595.94 1569.82 64.33 56.9 9.65 672.88 10.9 8.27

3/24/2009 16:39

606.31 1614.14 1.77 4.76 -1.69 671.08 10.9 8.27

3/24/2009 16:40

598.11 1617.99 0.42 0.4 0.41 666.82 10.88 8.29

3/24/2009 16:41

587.44 1574.27 8.64 6.46 2.46 661.39 10.92 8.27

3/24/2009 16:42

615.4 1574.58 19.68 19.43 0.42 675.35 10.93 8.25 593.65 1574.58 19.81 19.43 0.42 679.2 10.91 8.28

4
6

.16 42.88 43.01 -0.03 653.71 10.9 8,29 3/24/2009 16:52 596.9 2006.45 42.88 43.02 0.42 661.61 10.97 8.23 3/24/2009 16:53 610.08 1881.97 42.88 42.72 0.45 671.79 10.92 8.24 3/24/2009 16:54 606.11 1783.9 42.88 42.51 0.46 661.29 10.89 8.27 3/24/2009 16:55 607.8 1470.25 42.89 42.52 0.46 651.94 10.85 8.32 3/24/2009 16:56 608.99 1452.29 42.89 42.52 0.46 656.18 10.85 8.32 3/24/2009 16:57 585.04 1611.7 39.27 40.76 -1.27 650.04 10.85 8.32 3/24/2009 16:58 578.43 1795.9 41.61 43.13 -1.08 651.32 10.93 8.27 3/24/2009 16:59 605.71 2006.81 43.87 43.3 0.94 668.47 10.92 8.25 3/24/2009 17:00 606.22 2006.75 43.95 43.01 0.94 662.38 10.88 8.29 3/24/2009 17:01 597.03 1959.18 43.83 42.99 0.97 662.34 10.89 8.27 3/24/2009 17:02 606.82 1429.6 43.86 43 1.27 658.28 10.87 8.29 3/24/2009 17:03 601.54 1651.49 43.83 42.97 1.41 660.21 10.87 8.29 3/24/2009 17:04 613.71 2007.58 43.82 42.59 1.41 657.33 10.86 8.3 3/24/2009 17:05 582.71 1680.2 43.83 42.47 1.41 651.86 10,85 8.33 3/24/2009 17:06 582.77 1528.19 43.84 42.48 1.42 650.36 10.93 8.26 3/24/2009 17:07 614,01 2006.59 43.89 42.52 1.67 670.8 10.92 8.24 3/24/2009 17:08 546.43 1867.9 43.88 42.46 1.89 657.07 10.87 8.28 3/24/2009 17:09 5.13 1542.46 43.97 42.47 1.92 309.22 5.78 5.26 3/24/2009 17:10 1.89 595.47 44.32 42.25 1.92 5.04 0.2 0.37 3/24/2009 17:11 1.06 6.8 44.32 41.97 1.92 3.44 0.12 0.04 3/24/2009 17:12 0.76 3.49 44 42.02 1.96 3.28 0.09 0.01 3/24/2009 17:13 0.09 3.59 43.86 42 2.41 2.83 0.07 0.01 3/24/2009 17:14 0.08 2.88 43.82 41.73 2.41 2.62 0.05 0.01 3/24/2009 17:15 0.08 2.88 43.82 41.46 2.42 2.84 0.04 0.01 3/24/2009 17:16 0.08 2.87 43.82 41.46 2.41 2.79 0.03 0.01 3/24/2009 17:17 0.09 2.9 43.82 41.46 2.42 2.86 0.02 0.01 3/24/2009 17:18 0.08 2.86 43.82 41.24 2.72 2.79 0.01 0.01 3/24/2009 17:19 0.08 2.87 43.82 40.96 2.91 2.93 0.01 0.01 3/24/2009 17:20 0.08 2.85 43.82 40.96 2.91 2.82 0 0.01 3/24/2009 17:21 0.09 2.86 43.82 40.96 2.91 2.87 0 0.01 3/24/2009 17:22 0.08 2.84 43.82 40.96 2.91 2.97 0 0.01 3/24/2009 17:23 0.09 2.88 43.82 40.57 2.91 2.76 0 0.01 3/24/2009 17:24 0.09 2.87 43.82 40.46 3.15 2.57 0 0.01 3/24/2009 17:25 0.08 2.87 43.82 40.47 3.41 2.91 0 0.01 3/24/2009 17:26 0.08 2.88 43.82 40.47 3.41 2.61 0 0.01 3/24/2009 17:27 0.08 2.9 43.83 40.23 3.41 2.61 0 0.01 3/24/2009 17:28 0.08 2.88 43.82 39.96 3.41 2.73 0 0.01 3/24/2009 17:29 0.08 2.9 43.5 39.96 3.41 2.66 0 0.01 3/24/2009 17:30 0.09 2.88 43.32 39.96 3.48 2.75 0 0.01 3/24/2009 17:31 0.08 2.78 43.31 39.96 3.91 2.42 0 0.01 3/24/2009 17:32 0.08 2.41 37.07 37.06 0.26 2.61 0 0.01 3/24/2009 17:33 0.08 2.91 2 1.05 1.2 2.36 0 0.01 3/24/2009 17:34 0.3 2.88 0.3 0.4 0.42 2.31 0 0.01 3/24/2009 17:35 21.58 15.71 0.26 0.38 0.39 4.99 0.02 5.98 3/24/2009 17:36 20.38 88.63 18.73 16.41 2.28 16.18 0.24 19.61 3/24/2009 17:37 18.62 59.89 34.64 34.83 -0.22 14.05 0.19 20.3 3/24/2009 17:38 23.66 24.6 34.64 34.83 -0.22 9.06 0.12 20.5

S
.8

34.83 34.46 0.42 11.5 12.89 0.01 3/24/2009 17:48 0.08 2.84 34.82 34.46 0.42 2.35 13.35 0.01 3/24/2009 17:49 0.09 2.84 34.82 34.13 0.42 1.78 13.4 0.01 3/24/2009 17:50 0.08 2.85 34.83 33.96 0.42 1.89 13.43 0.01 3/24/2009 17:51 0.08 2.82 34.82 33.96 0.75 1.98 13.44 0.01 3/24/2009 17:52 0.08 1.85 34.87 33.99 0.93 1.83 13.46 0.01 3/24/2009 17:53 0.13 1.3 34.88 34.01 0.95 1.87 13.46 0.01 3/24/2009 17:54 0.09 1.33 34.89 34.01 0.96 1.71 7.7 3.05 3/24/2009 17:55 0.08 1.36 34.89 34.01 0.95 2.21 0.22 7.97 3/24/2009 17:56 0.08 1.32 34.89 34.01 0.96 2.39 0.1 8.21 3/24/2009 17:57 0.08 1.34 34.89 33.59 0.95 2.66 0.06 8.27 3/24/2009 17:58 0.09 1.28 34.87 33.49 0.94 2.22 0.04 8.29 3/24/2009 17:59 343.69 1.62 34.83 33.47 1.08 2.43 0.02 5.88 3/24/2009 18:00 756.03 2.57 34.59 33.47 1.42 5.65 0.06 19.38 3/24/2009 18:01 909.42 2.89 34.4 33.46 1.41 3.1 0.01 20.44 3/24/2009 18:02 533.14 2.86 34.32 33.46 1.41 2.67 0 20.58 3/24/2009 18:03 527.48 2.9 34.32 33.04 1.41 2.73 0 20.62 3/24/2009 18:04 527.66 2.89 34.32 32.96 1.41 2.82 0 20.64 3/24/2009 18:05 844.03 2.93 34.32 32.96 1.41 2.88 0 20.64 3/24/2009 18:06 773.03 2.88 34.32 32.95 1.41 2.74 0 20.64 3/24/2009 18:07 516.57 2.88 34.31 32.95 1.49 2.95 0 20.7 3/24/2009 18:08 425.68 2.9 34.32 32.96 1.92 2.37 0 20.77 3/24/2009 18:09 339.05 2.84 34.32 32.47 1.92 2.5 0 20.82 3/24/2009 18:10 568 2.89 34.32 32.46 1.91 2.78 0 20.83 3/24/2009 18:11 930.7 1523.25 34.33 32.46 1.91 2.48 0 20.78 3/24/2009 18:12 932.46 1905.64 34.32 32.46 1.91 2.31 0 20.77 3/24/2009 18:13 933.02 1923.34 34.32 32.45 1.91 2.39 0 20.77 3/24/2009 18:14 933.41 1916.68 34.33 32.46 1.91 2.27 0 20.77 3/24/2009 18:15 933.8 1907.3 34.33 32.29 1.91 2.25 0 20.78 3/24/2009 18:16 933.99 1918.82 34.32 31.96 1.91 2.14 0 20.77 3/24/2009 18:17 934.68 1923.34 34.32 31.96 2.33 2.27 0 20.78 3/24/2009 18:18 935.01 1904.59 34.32 31.96 2.41 2.18 0 20.78 3/24/2009 18:19 935.17 1885.24 34.32 31.96 2.41 2.04 0 20.79 3/24/2009 18:20 935.74 1875.25 34.15 31.96 2.41 2.18 0 20.79 3/24/2009 18:21 936.23 1875.39 36.62 34.15 2.43 2.18 0 20.79 3/24/2009 18:22 936.45 1877.1 38.47 34.94 3.49 2.09 0 20.79 3/24/2009 18:23 936.47 1876.31 33.34 31.59 1.81 2.24 0 20.79 3/24/2009 18:24 936.78 1876.66 27.4 25.75 1.52 2.07 0 20.8 3/24/2009 18:25 916.07 1890.77 36.06 32.08 4.03 2.11 0 20.79 3/24/2009 18:26 79.42 1512.2 37.15 0.45 37.18 8.01 0.06 20.78 3/24/2009 18:27 73.7 109.54 38.39 0.45 38.25 14.21 0.2 20.68 3/24/2009 18:28 62.85 119.58 38.38 0.45 38.04 14.14 0.18 20.71 3/24/2009 18:29 63.47 129.6 38.38 0.45 37.98 20.48 0.28 20.64 3/24/2009 18:30 85.17 103.93 38.27 0.45 37.98 27.08 0.37 20.54

6
59 3/25/2009 6:18 0.08

0 3.35

3/25/2009 6:19 0.09 3.7 0.11 0.28 -0.23 1013.16 0 0.28 2.43 0.11 0.28 -0.22 1014.31 0 0.01 3/25/2009 6:20 0.09 2.81 0.21 0.35 -0.14 1014,49 0 0.01 3/25/2009 6:21 0.41 3.64 0.22 0.35 -0.14 1010.95 0 0.01 3/25/2009

3/25/2009 6:23

6:22

0.09

0.16 18.37 0.18 0.33 -0.16 665.58 0 5.44

3/25/2009 6:24 0.14 12.23 0.09 0.27 -0.22 604.5 0 1.28 2.38 0.1 0.28 -0.23 571.84 0.18 0.01 3/25/2009 6:25 0.08 2.5 0.1 0.27 -0.24 33.32 11.63 0.04 3/25/2009 6:26 0.09 2.47 0.1 0.28 -0.23 0.67 13.22 0.01 3/25/2009 6:27 0.09 2.7 0.19 0.33 -0.16 0.42 13.42 0.01 3/25/2009 6:28 0.08 2.76 0.23 0.35 -0.13 0.49 13.52 0.01 3/25/2009 6:29 0.1 2.36 0.12 0.29 -0.21 0.5 13.14 0.01 3/25/2009 6:30 0.09 2.32 0.1 0.28 -0.22 0.19 8.29 0.01 3/25/2009 6:31 0.09 2.72 0.21 0.35 -0.15 0.26 8 0.01 3/25/2009 6:32 0.08 2.68 0.12 0.28 -0.23 0.49 4.36 6.89 3/25/2009 6:33 0.09 2.6 0.1 0.27 -0.24 1.01 0 20.25 3/25/2009 6:34 0,09 2.58 -0.55 0.27 -0.83 1 0 20.81 3/25/2009 6:35 0.08 2.48 0.09 0.27 0.25 0.84 0 20.95 3/25/2009 6:36 0.08 2.36 0.08 0.26 0.24 0.72 0 20.98 3/25/2009 6:37 0.09 2.25 0.07 0.26 0.25 0.91 0 20.07 3/25/2009 6:38 0.09 2.17 0.07 0.26 0.25 0.41 0 9.34 3/25/2009 6:39 0.08 2.15 0.07 0.27 0.26 0.72 0 8.4 3/25/2009 6:40 0.09 2.2 0.08 0.27 0.26 0.49 0 8.28 3/25/2009 6:41 0.08 2.71 0.19 0.34 0.25 0.79 0 6.19 3/25/2009 6:42 0.08 2.62 94.36 58.39 36.12 0.33 0 0.35 3/25/2009

3/25/2009 6:44

6:43

0.09

0.09 2.67 251.08 250.58 0.76 0.22 0 0.01

3/25/2009 6:45 0.09 2.56 245.57 251,69 -1.87 0.56 0 0.01 2.11 120 116.6 4.23 0.32 0 0.01 3/25/2009

3/25/2009 6:47

6:46

0.54

0.08 2.68 99.68 98.5 1.27 0.43 0 0.01 2.67 96.25 98.5 -0.95 0.72 0 0.01 3/25/2009 6:48 8.01 2.46 36.67 29.63 7.55 14.39 0.06 9.47 3/25/2009 6:49 0.08 2.57 21.05 28.48 -2.1 368.77 0.01 5.62 3/25/2009 6:50 0.09 2.54 1.11 0.27 0.75 601.74 0 0.35 3/25/2009 6:51 0.09 2.58 1.1 0.28 0.75 602.63 0 0.03 3/25/2009 6:52 0.08 2.53 0.68 0.27 0.74 602.89 0 0.01 3/25/2009 6:53 0.08 2.5 0.6 0.27 0.42 326.69 4.91 0.01 3/25/2009 6:54 0.09 2.5 0.6 0.27 0.25 2.53 13.15 0.01 3/25/2009 6:55 0.09 2.55 0.6 0.27 0.25 1 13.27 0.01 3/25/2009 6:56 0.08 2.16 0.57 0.26 0.25 0.29 13.31 0.01 3/25/2009 6:57 0.09 2.4 0,63 0.31 0.3 0.37 13.33 0.01 3/25/2009 6:58 0.09 2.48 0.65 0.31 0.31 0.34 13.34 0.01 3/25/2009 6:59 0.09 2.38 0.56 0.31 0.31 0.49 12.8 0.13 3/25/2009 7:00 0.07 2.67 0.29 0.34 0.35 0.62 1.38 6.8 3/25/2009 7:01 0.08 2,45 0.23 0.36 0.37 0.82 0.05 8.12 3/25/2009 7:02 0.08 2.74 0.24 0.36 0.38 1.06 0 8.23 3/25/2009 7:03 0.08 2.78 0.26 0.37 0.39 1.12 0 8.26 3/25/2009 7:04 0.08 2.46 0.27 0.38 0.4 1.05 0 8.27 3/25/2009 7:05 0.08 2.1 0.27 0.39 0.41 0,97 0 8.28 3)25/2009 7:06 0.08 2.78 7.91 13.2 -3.15 1.09 0 7.81 3/25/2009 7:07 0.08 2.76 92.43 91.69 0.93 0.79 0 0.99 3/25/2009 7:08 0.08 1.82 98.39 100.08 -1.49 0.78 0 0.14 3/25/2009 7:09 0.08 1.91 98.77 100.07 -1.59 1.18 0 0.01

I
3/25/2009 7:19 337.64 1.05 0.12 0.3 0.28 0.63 0 20.77 3/25/2009 7:20 697.2 1.13 0.11 0.29 0.26 0.43 0 20.78 3/25/2009 7:21 932.07 1483.48 0.31 0.4 0.4 0.21 0 20.69 3/25/2009 7:22 932.7 1904.8 0.31 0.4 0.4 0.29 0 20.69 3/25/2009 7:23 933.35 1940.19 0.23 0.35 0.34 0.19 0 20.69 3/25/2009 7:24 933.17 1930.6 0.22 0.35 0.34 0.25 0 20.69 3/25/2009 7:25 933.68 1914.23 0.21 0.34 0.33 0.28 0 20.7 3/25/2009 7:26 933.88 1932.18 0.17 0.3 0.31 0.16 0 20.71 3/25/2009 7:27 933.52 1940.95 0.15 0.29 0.3 0.27 0 20.7 3/25/2009 7:28 933.82 1889.65 0.17 0.3 0.31 0.23 0 20.71 3/25/2009 7:29 933.43 1882.93 0.16 0.3 0.31 0.24 0 20.7 3/25/2009 7:30 933.7 1880.73 0.16 0.3 0.31 0.29 0 20.7 3/25/2009 7:31 933.87 1882.28 0.18 0.31 0.32 0.2 0 20.69 3/25/2009 7:32 762.4 1835.77 0.32 0.41 0.41 0.25 0 20.69 3/25/2009 7:33 556.58 1483.26 0.34 0.42 0.34 0.29 0 20.73 3/25/2009 7:34 555.31 1341.24 0.34 0.42 0.43 0.24 0 20.76 3/25/2009 7:35 554.7 1142.54 0.34 0.42 0.25 0.28 0 20.78 3/25/2009 7:36 511.52 1142.62 0.34 0.42 0.28 0.21 0 20.77 3/25/2009 7:37 366.21 1135.98 0.35 0.43 0.09 0.24 0 20.78 3/25/2009 7:38 365.06 755.53 0.37 0.45 -0.03 0.31 0 20.81 3/25/2009 7:39 364.98 753.63 0.38 0.46 -0.01 0.19 0 20.82 3/25/2009 7:40 364.12 749.73 0.38 0.46 -0.02 0.25 0 20.81 3/25/2009 7:41 28.55 730.73 0.32 0.42 -0.05 0.26 0 20.83 3/25/2009 7:42 1.06 718.44 0.32 0.42 -0.05 0.23 0 20.89 3/25/2009 7:43 291.72 52.33 1.57 1.45 0.39 14.54 0.07 20.89 3/25/2009 7:44 576.64 344.82 46.6 43.96 2.69 570.45 8.66 12.04 3/25/2009 7:45 578.41 1462.22 58.26 45.7 12.44 641.91 10.56 8.63 3/25/2009 7:46 567.24 1505.12 61.39 39.73 21.74 643.22 10.61 8.43 3/25/2009 7:47 564.13 1542.54 64.58 37.1 27.62 650.61 10.67 8.34 3/25/2009 7:48 579.42 1504.11 66.73 35.68 31.03 650.41 10.67 8.33 3/25/2009 7:49 584.02 1489.18 68.65 34.22 34.47 652.27 10.68 8.31 3/25/2009 7:50 559.89 1448.11 66.79 31.84 34.89 646.5 10.66 8.35 3/25/2009 7:51 570.89 1699.89 67.91 31.24 36.73 646.9 10.7 8.32 3/25/2009 7:52 572.82 2007.55 76.18 46.27 29.9 650.66 10.69 8.31 3/25/2009 7:53 569.39 1598.58 67.45 26.42 41.09 648.91 10.7 8.32 3/25/2009 7:54 558.31 1489.58 65.68 21.72 44.09 648.52 10.7 8.32 3/25/2009 7:55 558.65 2007.65 65.74 19.8 45.95 649.28 10.71 8.31 3/25/2009 7:56 570.02 1989.57 66.04 18.66 47.17 650.34 10.72 8.31 3/25/2009 7:57 566.52 1959.21 64.35 16.43 47.87 645.12 10.71 8.3 3/25/2009 7:58 556.78 1815.83 62.7 14.72 47.91 642.35 10.69 8.33 3/25/2009 7:59 554.6 1744.44 64.63 15.01 49.69 651.15 10.74 8.28 3/25/2009 8:00 582.99 1576.06 64.26 15.41 48.85 648.77 10.72 8.28 3/25/2009 8:01 569.58 1583.7 61.79 14.56 47.22 641.99 10.69 8.32 3/25/2009 8:02 565.91 1620.52 62.52 15.28 47.32 643.86 10.71 8.31 3/25/2009 8:03 560.66 1519.9 63.39 16.85 46,53 645.84 10.7 8.31 3/25/2009 8:04 563.06 1448.02 64.35 18.14 46.21 647.07 10.72 8.29 3/25/2009 8:05 565.79 1501.16 66.15 19.41 46.79 650 10.73 8.28 3/25/2009 8:06 571.32 1537.96 66.15 19.41 46.69 647.52 10.7 8.3 3/25/2009 8:07 565.41 1670.57 67.32 19.98 47.42 647.59 10.7 8.3 3/25/2009 8:08 562.94 1833.37 66.04 19.07 47.05 644.4 10.69 8.33 3/25/2009 8:09 562.9 2007.37 66.41 19.41 47.2 645.08 10.71 8.3 3/25/2009 8:10 563.85 2007.38 67.66 19.67 47.92 650.06 10.72 8.28

2
3/25/2009

3.44 1976.17 66.3 17.16 48.97 650.04 10.71 8.28

3/25/2009

8:21 561.5 1957.25 65.63 16.74 48.89 647.65 10.7 8.29

3/25/2009

8:22 558.15 1885.94 64.1 16.13 47.89 641.97 10.68 8.32

3/25/2009

8:23 560.16 1931.45 64.52 16.33 48.1 645.8 10.69 8.3

3/25/2009

8:24 557.43 1957.25 63.89 15.87 48.14 644.35 10.69 8.31

3/25/2009

8:25 556.52 1938.07 64.51 15.96 48.59 646.27 10.69 8.3

3/25/2009

8:26 559.72 1906.25 63.85 16.29 47.68 645.85 10.69 8.31

3/25/2009

8:27 554.23 1889.23 63.47 15.88 47.56 645.85 10.7 8.29

3/25/2009

8:28 560.21 1861.03 63.31 15.75 47.55 645.74 10.69 8.3

3/25/2009

8:29 547.54 1881.87 63.81 15.67 48.14 647.29 10.7 8.3

3/25/2009

8:30 557.9 1846.86 63.73 15.54 48.02 645.6 10.71 8.28

3/25/2009

8:31 553.02 1826.24 63.72 15.71 47.97 647.12 10.7 8.29

3/25/2009

8:32 550.47 1833.79 64.89 15.88 48.97 651.64 10.72 8.28

3/25/2009

8:33 559.87 1834.6 63.94 15.92 47.93 646.79 10.71 8.29

3/25/2009

8:34 557.46 1902.21 62.81 15.91 47.01 642.17 10.72 8.29

3/25/2009

8:35 556.93 1877.66 63.4 16.5 47.02 645.98 10.71 8.28

3/25/2009

8:36 558.16 1883.99 63.81 15.95 47.9 646.44 10.71 8.28

3/25/2009

8:37 544.21 1866.28 63.06 15.75 47.44 644.93 10.71 8.28

3/25/2009

8:38 549.05 2007.37 63.32 17.25 46.07 652.24 10.75 8.25

3/25/2009

8:39 551.24 1958.18 64.28 25.05 39.14 649.1 10.71 8.28

3/25/2009

8:40 548.9 1913.17 68.84 30.77 38 647.1 10.71 8.27

3/25/2009

8:41 556.72 1875.97 64.88 21.37 43.59 644.24 10.71 8.28

3/25/2009

8:42 557.3 1857.69 64.77 19.03 45.82 644.79 10.71 8.28

3/25/2009

8:43 566.07 1973.18 63.99 17.91 46.09 641.55 10.7 8.3

3/25/2009

8:44 561.83 1875.71 63.99 17.16 46.83 642.92 10.71 8.29

3/25/2009

8:45 544.47 1855.04 63.49 16.38 47.17 641.61 10.71 8.29

3/25/2009

8:46 564 1938.63 65.65 17.03 48.57 648.4 10.75 8.25

3/25/2009

8:47 558.39 1859.18 64.08 16.28 47.76 643.59 10.71 8.29

3/25/2009

8:48 562.71 1874.22 64.57 15.49 49.15 643.39 10.72 8.28

3/25/2009

8:49 560.36 1834.94 63.54 14.42 49 643.49 10.73 8.28

3/25/2009

8:50 558.12 1846.67 65.2 14.5 50.69 646.78 10.74 8.26

3/25/2009

8:51 563.98 1922.58 64.25 12.27 51.84 645.82 10.74 8.26

3/25/2009

8:52 553.07 1864.54 63.96 11.64 52.34 649.79 10.75 8.27

3/25/2009

8:53 563.77 1877.41 64.33 11.2 53.14 647.14 10.74 8.26

3/25/2009

8:54 570.04 1882.73 63.29 11.12 52.36 644.59 10.73 8.28

3/25/2009

8:55 560.78 1854.3 62.23 10.47 51.6 642.21 10.72 8.29

3/25/2009

8:56 566.26 1874.19 65.15 13.42 51.68 646.08 10.76 8.25

3/25/2009

8:57 565.9 1858.31 64.41 13.7 50.74 643.37 10.73 8.28

3/25/2009

8:58 561.87 1823.94 62.85 12.89 49.99 641.13 10.73 8.29

3/25/2009

8:59 558.87 1883.77 64.48 12.96 51.39 648.45 10.76 8.26

3/25/2009

9:00 568.41 2007.45 67.22 17.37 49.97 650.75 10.75 8.26

3/25/2009

9:01 566.33 1994.25 72.52 25.76 46.99 652.29 10.75 8.25

3/25/2009

9:02 557.41 1996.67 69.38 22.28 47.15 647.67 10.76 8.26

3/25/2009

9:03 576.34 2006.62 71.48 22.16 49.37 655.87 10.78 8.23

3/25/2009

9:04 570.65 1940.9 67.16 18 49.12 646.14 10.73 8.28

3/25/2009

9:05 567.12 1920.96 64.99 15.39 49.56 642.85 10.75 8.27

3/25/2009

9:06 576.37 1969.86 62.96 10.3 52.7 644.35 10.74 8.28

3/25/2009

9:07 29.83 1278.83 49.32 12.95 36.22 371.6 6.86 6.13

3/25/2009

9:08 2.05 10.08 23.99 6.49 17.27 1.13 0.15 0.46

3/25/2009

9:09 1.06 7.36 20.02 5.25 14.82 0.23 0.04 0.07

3/25/2009

9:10 1.06 4.07 16.77 4.47 12.33 0.13 0.01 0.01 9:11 0.08 2.86 13.85 3.96 9.81 0.25 0 0.01

3
3/25/2009

3/25/2009

9:21 0.07 2.88 3.17 1.59 1.59 0.32 13.28 0.01

3/25/2009

9:22 0.08 2.86 2.68 1.34 1.43 0.27 13.3 0.01

3/25/2009

9:23 0.08 2.84 2.33 0.9 1.43 0.27 13.31 0.01

3/25/2009

9:24 0.08 2.88 2.09 0.9 1.11 0.29 13.32 0.01

3/25/2009

9:25 0.57 2.75 1.79 0.88 0.91 0.22 13.33 0.01

3/25/2009

9:26 1.26 2.77 1.86 0.86 0.89 0.54 9.8 1.68

3/25/2009

9:27 0.08 2.62 1.78 0.87 0.9 0.17 0.29 7.82

3/25/2009

9:28 0.07 2.79 1.79 0.87 0.9 0.19 0.07 8.19

3/25/2009

9:29 0.08 2.79 1.56 0.87 0.91 0.22 0.03 8.27

3/25/2009

9:30 0.08 2.89 1.32 0.9 0.92 0.13 0 8.29

3/25/2009

9:31 0.08 2.88 1.32 0.42 0.68 0.26 0 8.3

3/25/2009

9:32 0.07 2.77 1.33 0.41 0.44 0.15 0 8.3

3/25/2009

9:33 0.08 2.9 1.16 1.01 -0.16 0.2 0 8.3

3/25/2009

9:34 0.08 2.91 70.09 61.22 8.93 0.14 0 2.92

3/25/2009

9:35 0.08 1.67 99.34 100.32 -0.65 0.12 0 0.24

3/25/2009

9:36 0.19 1.68 99.43 100.62 -1.04 0.22 0 0.01

3/25/2009

9:37 433.85 2.16 58.64 62.54 -1.46 0.14 0 5.86

3/25/2009

9:38 481.82 2.62 1.93 1.14 0.96 0.26 0 19.88

3/25/2009

9:39 527 2.74 1.31 0.58 0.92 0.27 0 20.53

3/25/2009

9:40 527.98 2.79 1.32 0.42 0.84 0.2 0 20.67

3/25/2009

9:41 528.25 2.87 1.24 0.41 0.43 0.33 0 20.73

3/25/2009

9:42 532.28 2.82 0.83 0.41 0.43 0.2 0 20.73

3/25/2009

9:43 556.58 2.92 0.82 0.41 0.43 0.27 0 20.78

3/25/2009

9:44 557.03 1069.28 0.82 0.4 0.43 0.22 0 20.81

3/25)2009

9:45 557.06 1807.52 0.84 0.42 0.44 0.27 0 20.82

3/25/2009

9:46 557.73 1812.35 0.97 0.45 0.47 0.3 0 20.82

3/25/2009

9:47 558.35 1815.8 0.87 0.45 0.47 0.19 0 20.83

3/25/2009

9:48 559.97 1818.51 0.88 0.45 0.46 0.26 0 20.84

3/25/2009

9:49 656.56 1908.03 14.98 13.55 1.63 203.79 2.69 18.72

3/25/2009

9:50 668.26 1970.93 53.58 35.84 17.89 640.82 10.53 9.08

3/25/2009

9:51 683.12 1993.34 52.75 30.33 22.56 638.14 10.64 8.51

3/25/2009

9:52 649.61 1994.98 55.78 28.46 27.37 643.87 10.69 8.39

3/25/2009

9:53 639.15 1973.73 57.1 27.11 30.11 643.12 10.77 8.31

3/25/2009

9:54 662.5 1984.77 60.57 24.23 36.4 652.17 10.79 8.28

3/25/2009

9:55 651.91 1985.76 61.2 22.47 38.86 649.01 10.77 8.31

3/25/2009

9:56 654.98 1981.61 62.43 21.24 41.25 648.83 10.77 8.31

3/25/2009

9:57 644.79 1964.11 61.91 20.07 41.91 644.14 10.79 8.31

3/25/2009

9:58 645.52 1956.09 64.97 21.21 43.56 649.85 10.81 8.29

3/25/2009

9:59 650.09 1976.28 68.49 27.99 40.66 647.99 10.78 8.31

3/25/2009

10:00 653.41 1966.86 65.9 24.07 41.91 644.96 10.78 8.33

3/25/2009

10:01 646.23 1977.07 64.32 23.15 41.23 641.62 10.78 8.32

3)25/2009

10:02 626.89 1965.92 64.32 23.16 41.33 643.27 10.79 8.32

3/25/2009

10:03 631.33 2006.77 66.54 23.31 43.23 651.77 10.83 8.28

3/25/2009

10:04 645.52 2004.36 66.96 19.55 47.57 660 10.85 8.26

3/25/2009

10:05 652.45 2003.33 65.1 17.84 47.15 648.18 10.79 8.31

3/25/2009

10:06 657.43 2005.52 65.4 17.05 48.3 648.31 10.78 8.32

3/25/2009

10:07 624.89 2007.46 61.99 16 46.04 637.69 10.78 8.34

3/25/2009

10:08 631.66 2006.78 63.83 16.7 47.12 648.23 10.84 8.29

3/25/2009

10:09 638.8 2007.63 68.3 22 46.27 653.01 10.82 8.29

3/25/2009

10:10 616.06 2007.54 68.64 21.93 46.78 651.61 10.83 8.29

3/25/2009

10:11 630.68 2007.18 67.76 21.04 46.78 652.73 10.85 8.27 10:12 633.14 2007.23 69.92 22.27 47.81 657.43 10.84 8.27

4
3/25/2009 10:22 640.49 2007.58 62.19 10.52 51.8 651 10.83 8.28 3/25/2009 10:23 648.43 2007.32 62.61 12.4 50.28 657.5 10.83 8.28 3/25/2009 10:24 626.89 1936.79 61.99 13.09 48.98 653.22 10.83 8.28 3/25/2009 10:25 627.97 1927.14 64.69 13.9 50.83 661.67 10.89 8.23 3/25/2009 10:26 653.63 1957.03 63.38 13.64 49.82 650.56 10.83 8.29 3/25/2009 10:27 658.46 1979.08 62.85 13.74 49.12 645.92 10.8 8.33 3/25/2009 10:28 661.52 1988.12 63.94 13.6 50.4 648.59 10.83 8.29 3/25/2009 10:29 649.4 1970.4 62.05 12.63 49.44 641.37 10.8 8.34 3/25/2009 10:30 635.89 2006.58 61.41 12.92 48.47 642.86 10.84 8.3 3/25/2009 10:31 638.73 2006.64 62.64 13.09 49.56 648.44 10.85 8.29 3/25/2009 10:32 665.13 2006.87 64.7 14.03 50.75 652.74 10.84 8.29 3/25/2009 10:33 656.64 1980.63 63.46 13.76 49.85 645.86 10.81 8.32 3/25/2009 10:34 639.85 1989.4 63.32 13.54 49.94 649.63 10.83 8.3 3/25/2009 10:35 612.07 2006.71 62.49 13.21 49.36 644.94 10.84 8.31 3/25/2009 10:36 639.98 1998.45 63.01 15.9 47.09 656.23 10.88 8.26 3/25/2009 10:37 643.94 1985.14 66.06 18.8 47.42 658.52 10.85 8.28 3/25/2009 10:38 670.01 1999.75 63.75 15.53 48.46 645.43 10.8 8.33 3/25/2009 10:39 643.44 2006.6 62.2 13.61 48.39 641.31 10.79 8.36 3/25/2009 10:40 629.51 1913.68 62.15 13.63 48.53 643.82 10.83 8.32 3/25/2009 10:41 636.53 1970.19 61.93 13.43 48.35 645.77 10.85 8.3 3/25/2009 10:42 629.32 1967.59 65.05 13.97 51.04 654.7 10.85 8.29 3/25/2009 10:43 627.7 1966.57 64.95 13.91 51.18 651.37 10.84 8.3 3/25/2009 10:44 631.63 2006.64 64.09 14.03 50.31 649.24 10.85 8.3 3/25/2009 10:45 644.89 2007.03 63.24 13.73 49.52 646.53 10.84 8.31 3/25/2009 10:46 629.02 2007.03 62.63 14.61 48.07 650.42 10.84 8.32 3/25/2009 10:47 628.83 2007.5 61.92 15.99 45.96 646.41 10.86 8.3 3/25/2009 10:48 657.99 1892.05 65.69 16.13 49.63 655.81 10.87 8.28 3/25/2009 10:49 645.79 1915.83 65.21 15.6 49.7 652.13 10.85 8.3 3/25/2009 10:50 647.7 1899.07 64.74 15.28 49.42 649.6 10.84 8.31 3/25/2009 10:51 660.6 2003.51 61.84 16.03 45.93 643.99 10.81 8.33 3/25/2009 10:52 638.77 1973.39 63.91 17.19 46.76 646.89 10.84 8.32 3/25/2009 10:53 640.22 1979.53 62.95 15.26 47.73 642.01 10.85 8.31 3/25/2009 10:54 54.93 1987.34 56.92 19.11 37.93 397.25 7.32 6.46 3/25/2009 10:55 2.39 501.82 29.71 11.75 18.02 2.94 0.2 0.51 3/25/2009 10:56 1.32 6.51 23.28 8.17 15.18 1.23 0.07 0.09 3/25/2009 10:57 2.97 4.59 19.3 6.23 13.05 10.8 0.03 0.01 3/25/2009 10:58 1.06 4.61 15.58 4.92 10.69 520.66 0.01 0.1 3/25/2009 10:59 1.06 4.62 12.36 3.64 8.65 600.9 0 0.01 3/25/2009 11:00 0.59 3.34 9.66 2.69 7.06 601.68 0 0.01 3/25/2009 11:01 0.24 2.65 7.91 2.17 5.7 600.76 0 0.01 3/25/2009 11:02 0.08 4.55 6.23 1.76 4.57 135.18 9.19 0.01 3/25/2009 11:03 0.08 4.17 5.18 1.37 3.68 0.42 13.33 0.01 3/25/2009 11:04 0.09 2.69 4.33 1.24 3.09 0.42 13.4 0.01 3/25/2009 11:05 0.13 2.69 3.73 0.98 2.66 0.21 11.32 0.85 3/25/2009 11:06 0.08 2.72 3.25 0.91 2.38 0.37 0.48 7.57 3/25/2009 11:07 0.09 2.7 2.74 0.86 1.93 0.46 0.06 8.16 3/25/2009 11:08 0.08 2.71 2.3 0.86 1.76 0.26 0.01 8.25 3/25/2009 11:09 0.08 2.71 2.04 0.42 1.38 0.41 0 8.27 3/25/2009 11:10 0.09 2.29 1.77 0.39 1.39 0.19 0 8.27 3/25/2009 11:11 0.08 2.84 1.76 0.38 1.01 0.35 0 8.28 3/25/2009 11:12 0.08 2.82 1.32 0.38 0.89 0.27 0 8.27 3/25/2009 11:13 0.08 2.82 1.26 0.38 0.89 0.18 0 8.28

5
20.33 

11:23 540.59 1.54 1.37 0.48 0.48 0.82 0 20.58 3/25/2009 11:24 561.72 944.52 0.96 0.43 0.45 0.29 0 20.69 3/25/2009 11:25 562.48 1091.64 0.83 0.42 0.45 0.21 0 20.74 3/25/2009 11:26 563.18 1101.46 0.82 0.43 0.45 0.32 0 20.75 3/25)2009 11:27 564.45 1099.52 0.82 0.42 0.44 0.22 0 20.75 3/25/2009 11:28 566.46 1097.42 0.82 0.42 0.45 0.29 0 20.75 3/25/2009 11:29 610.44 1084.26 2.38 0.81 1.68 12.81 0.07 20.76 3/25/2009 11:30 650.13 1172.98 46.65 37.47 9.21 565.77 8.78 12.05 3/25/2009 11:31 662.8 2006.56 53.92 35.89 18.03 652.47 10.81 8.56 3)25/2009 11:32 660.9 1794.4 53.81 30.86 23.04 647.31 10.82 8.38 3/25/2009 11:33 658.93 1867.27 56.54 26.87 29.79 649.01 10.86 8.33 3/25/2009 11:34 658.17 1834.57 57.43 24.12 33.4 645.92 10.86 8.33 3/25/2009 11:35 670.2 2005.58 60.76 22.78 38.16 651.41 10.89 8.29 3/25/2009 11:36 654.59 1811.46 61.02 20.93 40.15 646.31 10.88 8.31 3)25/2009 11:37 623.07 1815.82 60.26 20.34 39.89 644.54 10.93 8.3 3/25/2009 11:38 650.59 2007.62 64.41 20.58 43.81 655.5 10.95 8.25 3/25/2009 11:39 655.55 1882.94 65.95 20.19 45.83 653.42 10.92 8.3 3/25/2009 11:40 653.33 1872.29 65.17 18.61 46.54 648.44 10.9 8.32 3/25/2009 11:41 620.98 1864.28 65.82 18.18 47.74 652.89 10.92 8.31 3/25/2009 11:42 635.11 1891.7 64.01 17.55 46.57 648.85 10.96 8.27 3/25/2009 11:43 649.83 2007.59 67.72 18 49.79 660.62 10.94 8.28 3/25/2009 11:44 657.67 1845.77 64.22 16.75 47.59 647.63 10.92 8.31 3/25/2009 11:45 649.71 1808.43 63.36 16.8 46.64 646.2 10.9 8.34 3/25/2009 11:46 666.68 1877.19 63.62 16.86 46.98 643.46 10.9 8.33 3/25/2009 11:47 657.7 1853.83 63.16 16.3 46.93 643.24 10.88 8.35 3/25/2009 11:48 631.24 1831.96 64.98 16.44 48.69 648.48 10.91 8.33 3/25/2009 11:49 613.46 1918.27 62.27 15.58 46.76 641.5 10.95 8.31 3/25/2009 11:50 647.4 2006.69 66.28 16.69 49.66 657.8 10.97 8.27 3/25/2009 11:51 662.54 1962.21 65.86 16.21 49.81 650.66 10.91 8.32 3/25/2009 11:52 643.37 1949.41 66.32 16.58 49.81 655.71 10.93 8.31 3/25/2009 11:53 662.11 2006.54 65.68 16.21 49.47 649.95 10.91 8.31 3/25/2009 11:54 639 1812.68 63.93 16.38 47.73 645.54 10.9 8.33 3/25/2009 11:55 612.65 1843.23 62.71 15.38 47.24 639.62 10.92 8.33 3/25/2009 11:56 628.39 1880.26 64.27 15.74 48.53 651.7 10.97 8.28 3/25/2009 11:57 646.02 1966.7 66.32 17.15 49.5 655.65 10.93 8.3 3/25/2009 11:58 644.98 2006.14 64.02 17 47.1 648.05 10.91 8.32 3/25)2009 11:59 623.94 2007.56 66.2 17.79 48.39 656.41 10.93 8.31 3/25/2009 12:00 646.71 2007.46 64.23 17.03 47.37 646.56 10.91 8.33 3/25/2009 12:01 642.69 2007.47 62.64 17.2 45.49 644.57 10.89 8.35 3)25/2009 12:02 612.86 2007.51 63.47 17.33 46.06 643.58 10.89 8.35 3/25/2009 12:03 608.94 2007.48 62.39 16.97 45.41 642.67 10.96 8.3 3/25/2009 12:04 634.89 1902 68.44 18.97 49.63 666.29 11 8.24 3/25/2009 12:05 642.15 1932.1 67.34 19.84 47.65 652.64 10.94 8.3 3/25/2009 12:06 622.54 1950.65 66.15 20.74 45.49 650.9 10.9 8.32 3/25/2009 12:07 626.47 2007,61 66.34 19.75 46.66 649.35 10.9 8.32 3)25)2009 12:08 622.81 2006.77 65.66 20.06 45.77 647.77 10.87 8.35 3/25/2009 12:09 595.26 2006.58 81 44.9 36.14 647.82 10.92 8.31 3)25)2009 12:10 610.68 2006.59 97.84 78.69 19.3 670.53 11 8.21 3/25/2009 12:11 628.06 1978.79 86.94 63.54 23.37 662.6! 10.94 8.25 3/25/2009 12:12 621.79 1937.13 81.75 54.35 27.79 657.99 10.91 8.28 3/25/2009 12:13 615 1997.61 80 51.78 28.36 659.27 10.91 8.29 3/25/2009 12:14 624.55 1923.51 78.56 49.27 29.32 659.1 10.92 8.29

6
3/25/2009 12:24 618.29 2006.55 68.69 3244 36.29 652.51 10.92 8.29 3/25/2009 12:25 602.47 2006.6 69.11 32.22 36.81 655.06 10.93 8.29 3/25/2009 12:26 606.24 1939.48 69.49 31.85 37.64 655.45 10.93 8,29 3/25/2009 12:27 590.58 1841.2 66.48 27.33 39.26 652.24 10.92 8.31 3/25/2009 12:28 560.96 1780.79 66.19 25.59 40.69 653.01 10.95 8.29 3/25/2009 12:29 564.1 2006.58 68.12 26.23 42.06 666.03 11.04 8.21 3/25/2009 12:30 598.8 2006.56 73.73 28.65 45.13 677.35 11.02 8.2 3/25/2009 12:31 595.79 2006.57 69.42 26.16 43.32 655.79 10.94 8.28 3/25/2009 12:32 594.12 2006.53 71.39 26.16 45.4 662.66 10.95 8.28 3/25/2009 12:33 601.22 1993.28 70.41 25.33 45.08 660.54 10.94 8.29 3/25/2009 12:34 578.84 1997.13 67.55 24.83 42.99 652.85 10.92 8.32 3/25/2009 12:35 572.83 1993.27 66.05 23.07 42.9 648.58 11 8.26 3/25/2009 12:36 598.12 2006.61 71.64 25.57 45.99 666.36 10.98 8.25 3/25/2009 12:37 582.81 2006,62 68.73 23.93 44.72 654.73 10.94 8.3 3/25/2009 12:38 576.48 1983 69.78 23.57 46.07 660.96 10.97 8.28 3/25/2009 12:39 578.67 1911.68 70.48 22.99 47.5 663.5 11.02 8.23 3/25/2009 12:40 605.39 1910.76 71.63 24.08 47.56 663.31 10.98 8.26 3/25/2009 12:41 250.69 1389 69.19 26.56 42.87 602.46 10.18 8.21 3/25/2009 12:42 2.64 219.84 29.7 11.59 18.18 34.04 0.83 1.67 3/25/2009 12:43 1.42 11.19 22.12 6.5 15.77 2.45 0.1 0.19 3/25/2009 12:44 1.07 4.66 16.87 3.49 13.52 2.17 0.06 0.01 3/25/2009 12:45 1.06 3.72 13.55 2.67 11.11 2.03 0.03 0.01 3/25/2009 12:46 0.18 2.71 11.3 2.33 8.87 1.98 0.01 0.01 3/25/2009 12:47 0.09 2.72 8.47 1.58 6.94 2.22 0 0.01 3/25/2009 12:48 0.08 2.65 6.54 0.99 5.51 2.28 0 0.01 3/25/2009 12:49 0.09 2.67 5.17 0.9 4.49 2.16 0 0.01 3/25/2009 12:50 0.08 2.47 4.23 0.64 3.66 2.15 0 0.01 3/25/2009 12:51 0.09 2.54 3.49 0.4 2.99 2.09 0 0.01 3/25/2009 12:52 0.09 2.77 2.94 0.41 2.5 2.12 0 0.01 3/25/2009 12:53 0.1 2.74 2.52 0.41 2.09 2.13 0 0.01 3/25/2009 12:54 0.31 2.73 2.28 0.41 1.92 2.25 0 0.01 3/25/2009 12:55 0.09 2.41 1.75 0.4 1.4 444.19 0 0.01 3/25/2009 12:56 0.09 1.34 1.77 0.42 1.4 604.6 0 0.01 3/25/2009 12:57 0.08 2.32 1.38 0.38 1.2 605.49 0 0.01 3/25/2009 12:58 0.16 2.55 1.21 0.37 0.87 381.38 3.88 0.01 3/25/2009 12:59 0.09 2.56 1.21 0.37 0.87 4.22 13.33 0.01 3/25/2009 13:00 0.08 1.44 1.16 0.41 0.9 2.24 13.49 0.01 3/25/2009 13:01 0.08 1.83 0.74 0.39 0.89 2.3 13.54 0.01 3/25/2009 13:02 0.09 1.78 0.74 0.39 0.55 2.17 13.56 0.01 3/25/2009 13:03 0.09 2 0.73 0.38 0.38 2.27 13.58 0.01 3/25/2009 13:04 0.08 1.97 0.73 0.39 038 2.1 11.86 0.63 3/25/2009 13:05 0.09 2.33 0.73 0.38 0.38 2.35 0.6 7.49 3/25/2009 13:06 0.09 2.39 0.72 0.38 0.38 2.69 0.09 8.15 3/25/2009 13:07 0.08 2.48 0.72 0.37 0.38 2.44 0.04 8.23 3/25/2009 13:08 0.09 2.56 0.71 0.37 0.37 2.46 0.02 8.26 3/25/2009 13:09 0.09 2.52 0.71 0.37 0.37 2.47 0 8.26 3/25/2009 13:10 0.08 2.48 0.71 0.37 0.37 2.44 0 8.27 3/25/2009 13:11 0.08 2.39 0.72 0.37 0.38 2.57 0 8.27 3/25/2009 13:12 0.09 2.51 11.19 16.06 -2.8 2.73 0 7.63 3/25/2009 13:13 0.08 2.45 95.96 95.15 0.92 2.72 0 0.82 3/25/2009 13:14 0.08 2.42 100.03 101.54 -1.47 2.53 0 0.12 3/25/2009 13:15 0.09 2.15 99.95 101.55 -1.61 2.78 0 0.01

7
13:25 609.8 1082.26 0.78 0.41 0.4 3.11 0 20.72 3/25)2009 13:26 609.94 1091.33 0.78 0.41 0.4 2.68 0 20.73 3/25/2009 13:27 609.77 1094.24 0.75 0.39 0.38 2.67 0 20.74 3/25/2009 13:28 609.68 1085.13 0.73 0.37 0.37 2.64 0 20.75 3/25/2009 13:29 643.57 1086.5 7.72 5.26 2.49 78.97 0.77 20.39 3/25/2009 13:30 643.19 1090.41 58.02 32.69 25.4 637.5 10.14 10.17 3/25/2009 13:31 628.31 1686.2 58.29 28.33 30.03 657.28 10.85 8.52 3/25/2009 13:32 86.96 1223.16 57.85 23.48 34.46 650.56 10.89 8.38 3/25/2009 13:33 -0.05 2.73 65.07 19.74 45.6 655.48 11 8.25 3/25/2009 13:34 0 1.34 74.4 22.55 52.02 675.43 10.99 8.23 3/25/2009 13:35 0.02 -0.22 23.06 7.88 15.31 665.71 10.95 8.27 3/25/2009 13:36 0.04 1.43 0.19 0.39 0.4 660.33 10.98 8.26 3/25/2009 13:37 0.05 -1.16 0.18 0.39 0.39 671.99 11.06 8.19 3/25/2009 13:38 0.04 0.57 6.51 1.68 5.34 673.07 11.01 8.22 3/25/2009 13:39 0.05 2.44 50.06 48.51 1.55 662.89 10.99 8.25 3/25/2009 13:40 0.05 0.31 49.08 50.37 -1.29 656.43 10.98 8.27 3/25/2009 13:41 0.07 -1.12 49.74 50.47 -0.73 665.09 10.98 8.26 3/25/2009 13:42 0.06 -1.85 49.99 50.58 -0.59 663.3 10.98 8.26 3/25/2009 13:43 0.06 -0.52 49.96 50.54 -0.58 657.43 10.95 8.31 3/25/2009 13:44 0.07 -1.25 50.27 50.48 -0.21 651.69 10.94 8.32 3/25/2009 13:45 0.06 2.37 50.4 50.48 -0.08 650.29 10.98 8.3 3/25/2009 13:46 0.06 2.79 49.96 50.04 -0.08 667.58 11.06 8.21 3/25/2009 13:47 0.07 3.68 50.05 50.01 0.04 677.38 11.02 8.23 3/25/2009 13:48 0.06 4.19 50.67 50.61 0.06 667.61 11 8.24 3/25/2009 13:49 0.06 6.86 50.86 50.69 0.41 669.16 10.99 8.24 3/25/2009 13:50 0.06 5.31 50.81 50.47 0.45 664.39 10.97 8.27 3/25/2009 13:51 0.06 3.76 50.7 50.28 0.91 656.15 10.94 8.3 3/25/2009 13:52 0.06 5.62 50.23 49.52 0.91 657.67 10.95 8.29 3/25/2009 13:53 0.07 0.4 50.25 49.48 0.92 658.81 10.95 8.29 3/25/2009 13:54 0.07 3.57 50.27 49.47 1.03 661.3 10.95 8.29 3/25/2009 13:55 0.05 3.4 50.33 49.48 1.42 652.14 10.98 8.27 3/25/2009 13:56 0.07 1.32 50.3 49.2 1.42 675.22 11.07 8.17 3/25/2009 13:57 0.06 3.19 50.25 48.98 1.42 670.17 10.99 8.22 3/25/2009 13:58 0.06 0.35 50.17 48.93 1.53 663.98 10.98 8.24 3/25/2009 13:59 0.07 3.57 50.13 48.7 1.79 671.22 11 8.22 3/25/2009 14:00 0.07 5.1 50.13 48.41 1.8 663.79 10.97 8.24 3/25/2009 14:01 0.07 1.61 50.1 48.38 1.78 659.11 10.94 8.29 3/25/2009 14:02 0.06 2.21 50.1 48.38 2.07 657.35 10.91 8.3 3/25/2009 14:03 0.07 1.9 50.1 47.92 2.28 661.02 10.94 8.28 3/25/2009 14:04 0.06 3 50.1 47.87 2.28 651.87 10.97 8.28 3/25/2009 14:05 0.07 -0.49 50.1 47.87 2.32 676.52 11.04 8.18 3/25/2009 14:06 0.07 1.86 50.1 47.41 2.77 662.58 10.97 8.24 3/25/2009 14:07 0.06 1.32 50.1 47.37 2.78 666.44 10.99 8.22 3/25/2009 14:08 0.07 0.54 50.1 47.37 2.77 670.72 11 8.21 3/25/2009 14:09 0.07 3.24 50.1 47.33 2.77 668.89 10.99 8.22 3/25/2009 14:10 0.06 1.97 50.1 46.87 3.23 656.99 10.94 8.28 3/25/2009 14:11 0.07 0 50.1 46.87 3.28 664.57 10.98 8.25 3/25/2009 14:12 0.07 2.57 50.1 46.87 3.27 664.31 10.98 8.24 3/25/2009 14:13 0.06 4.93 50.1 46.66 3.4 661.47 10.94 8.27 3/25/2009 14:14 0.07 1.21 50.1 46.38 3.78 651.92 10.89 8.32 3/25/2009 14:15 0.06 3.07 50.1 46.37 3.78 653.89 10.91 8.3 3/25/2009 14:16 0.07 3.52 50.1 46.33 3.78 650.2 10.91 8.29

8
3/25/2009

8.18

3/25/2009

14:26 0.08 4.17 49.62 44.89 4.79 673.58 10.96 8.24

3/25/2009

14:27 0.07 4.27 49.61 44.83 4.84 660.05 10.92 8.29

3/25/2009

14:28 0.06 -0.74 43.47 42.19 1.34 670.36 10.97 8.25

3/25/2009

14:29 0.06 0.87 2.64 1.8 1 662.98 10.95 8.27

3/25/2009

14:30 0.06 3.11 0.1 0.33 0.3 662.76 10.93 8.29

3/25/2009

14:31 0.06 -1.52 0.1 0.32 0.3 657.69 10.91 8.31

3/25/2009

14:32 0.08 3.63 0.08 0.31 0.29 663.36 10.93 8.28

3/25/2009

14:33 0.07 2.75 0.08 0.31 0.29 648.66 10.94 8.29

3/25/2009

14:34 0.05 0.24 0.08 0.3 0.29 662.45 11 8.24

3/25/2009

14:35 0.07 1.71 0.08 0.3 0.28 675.76 10.99 8.23

3/25/2009

14:36 0.07 1.05 0.08 0.31 0.29 667.6 10.95 8.26

3/25/2009

14:37 0.07 0.57 0.07 0.29 0.28 660.26 10.93 8.29

3/25/2009

14:38 0.05 4.92 0.07 0.3 0.28 677.88 10.98 8.24

3/25/2009

14:39 0.08 -2.38 0.07 0.3 0.28 667.08 10.94 8.27

3/25/2009

14:40 0.08 -0.55 0.07 0.3 0.28 660.15 10.92 8.29

3/25/2009 14:42

14:41 0.06 3.05 0.08 0.3 0.29 666.02 10.93 8.3

3/25/2009

0.05 5.04 0.07 0.3 0.28 660.68 10.93 8.3

3/25/2009

14:43 0.06 6.14 0.07 0.3 0.28 661.76 10.91 8.31

3/25/2009

14:44 0.06 5.17 0.07 0.29 0.28 649.15 10.9 8.33

3/25/2009

14:45 0.08 -1.23 0.07 0.29 0.28 655.28 11.01 8.24

3/25/2009

14:46

14:47

0.06 084 0.07 0.3 0.28 675.45 11.02 8.2

3/25/2009

0.07 0.64 0.07 0.3 0.28 671.14 10.98 8.24

3/25/2009

14:48 0.06 0.09 0.07 0.3 0.28 670.19 10.97 8.25

3/25/2009

14:49 0.06 0.6 0.07 0.3 0.28 664.06 10.95 8.27

3/25/2009

14:50 0.06 1.51 0.07 0.3 0.28 652.39 10.9 8.31

3/25/2009

14:51 0.05 4.94 0.07 0.3 0.28 656.29 10.91 8.31

3/25/2009

14:52 0.08 0.87 0.07 0.3 0.29 663.51 10.94 8.28

3/25/2009

14:53 0.07 -1.83 0.07 0.3 0.29 653.46 10.89 8.34

3/25/2009

14:54 0.07 0.67 0.09 0.31 0.29 648.23 10.97 8.28

3/25/2009

14:55 0.07 1.62 0.06 0.3 0.28 676.07 11 8.23

3/25/2009

14:56 0.07 -0.67 0.09 0.32 0.3 668.9 10.95 8.26

3/25/2009

14:57 0.07 1.28 0.08 0.31 0.29 659.99 10.98 8.26

3/25/2009

14:58 0.07 2.62 0.08 0.3 0.29 679.41 11.02 8.2

3/25/2009

14:59 0.06 4.57 0.08 0.3 0.28 660.43 10.92 8.27

3/25/2009

15:00 0.07 2.32 0.09 0.32 0.3 661.13 10.93 8.29

3/25/2009

15:01 0.06 0.67 0.08 0.31 0.29 657.56 10.9 8,31

3/25/2009

15:02 0.07 0.56 0.1 0.33 0.3 657.41 10.9 8.32

3/25/2009

15:03 0.07 -1.43 0.11 0.33 0.3 658.56 10.9 8.32

3/25/2009

15:04 0.07 2.89 0.1 0.33 0.3 656.01 10.88 8.34

3/25/2009

15:05 0.07 1.13 0.1 0.33 0.3 651.62 10.88 8.35

3/25/2009

15:06 0.07 4.43 0.08 0.31 0.29 648.4 10.97 8.28

3/25/2009

15:07 0.08 0.69 0.07 0.31 0.29 672.82 10.98 8.24

3/25/2009

15:08 0.07 3.38 0.07 0.31 0.29 672.9 10.98 8.23

3/25/2009

15:09 0.07 1.15 0.07 0.3 0.29 655.3 10.93 8.28

3/25/2009

15:10 0.07 0.96 0.08 0.31 0.29 656.84 10.92 8.3

3/25/2009

15:11 0.08 -0,03 0.08 0.31 0.29 659.95 10.91 8.32

3/25/2009

15:12 0.06 2.43 0.1 0.32 0.3 656.6 10.91 8.32

3/25/2009

15:13 0.07 0.14 0,08 0.31 0.29 654.55 10.89 8.34

3/25/2009

15:14 0.07 4.26 0.07 0.31 0.29 657.01 10.89 8.34

3/25/2009

15:15 0.07 4.06 0.07 0.3 0.29 511.31 11.18 7.71

3/25/2009

15:16 0.07 -1.62 0.07 0.3 0.29 6.99 13.48 0.73 15:17 0.06 5.48 0.07 0.3 0.29 2.69 13.56 0.12

9
3/25/2009 15:28

0.03 0.3 0.08 0.31 0.3 1.85 5.27 0.16

3/25/2009 15:29

0.04 -1.92 0.09 0.33 0.3 1.84 5.29 0.01

3/25/2009 15:30

0.05 0.37 0.58 0.33 0.3 1.4 5.3 0.01

3/25/2009 15:31

0.04 -1.47 1.09 6.01 -1.53 1.69 5.04 0.01

3/25/2009 15:32

0.05 3.16 88.98 91.66 -0.94 2.8 0.34 0.01

3/25/2009 15:33

0.05 -2.71 99.64 101.41 -1.28 3.48 0.03 0.01

3/25/2009 15:34

0.04 -1.11 99.64 101.5 -1.69 3.62 0.01 0.01

3/25/2009 15:35

0.05 -1.69 100.15 101.5 -1.69 3.84 0 0.01

3/25/2009 15:36

0.04 -0.27 100.08 101.68 -1.68 3.78 0 0.01

3/25/2009 15:37

0.06 2.08 100.06 102 -1.69 3.64 0 0.01

3/25/2009 15:38

0.05 0.6 100.05 101.65 -1.36 3.17 0 0.01

3/25/2009 15:39

0.04 0.91 56.27 62.74 -3.87 3.31 0 0.01

3/25/2009 15:40

0.04 3.03 50.02 50.88 -0.7 3.39 0 0.01

3/25/2009 15:41

0.04 1.8 49.6 50.88 -0.7 3.64 0 0.01

3/25/2009 15:42

0.04 5.51 49.59 50.88 -0.7 3.88 0 0.01

3/25/2009 15:43

0.07 0.18 49.6 50.91 -0.69 3.87 0 0.01

3/25/2009 15:44

0.06 0 49.6 50.47 -0.7 3.45 0 0.01

3/25/2009 15:45

0.05 3.2 49.6 50.38 -0.7 3.37 0 0.01

3/25/2009 15:46

0.04 6.31 49.6 50.72 -0.7 3.97 0 0.01

3/25/2009 15:47

0.04 -109 49.6 50.63 -0.71 3.46 0 0.01

3/25/2009 15:48

0.05 4.46 49.6 50.55 -0.7 3.83 0 0.01

3/25/2009 15:49

0.04 0.79 49.6 50.88 -0.71 3.88 0 0.01

3/25/2009 15:50

0.06 0.15 59.7 36.52 23.16 480.43 7.08 4.56

3/25/2009 15:51

0.04 0.21 64.95 20.96 43.95 667.91 10.88 8.05

3/25/2009 15:52

0.04 -0.78 71.78 21.58 50.33 669.98 10.93 8.2

3/25/2009 15:53

0.05 3.25 75.45 22.03 53.47 671.29 10.95 8.23

3/25/2009 15:54

0.04 -0.74 72.5 20.06 52.56 659.55 10.92 8.27

3/25/2009 15:55

0.06 2.57 68.4 17.1 51.19 647.11 10.87 8.35

3/25/2009 15:56

0.05 2.95 70.88 17.25 53.69 656.74 10.9 8.33

3/25/2009 15:57

0.05 1.53 68.7 16.24 52.34 647.76 10.95 8.31

3/25/2009 15:58

0.05 4.77 70.79 17.62 53.23 665.89 11.05 8.21

3/25/2009 15:59

0.06 5.6 79.76 20.83 58.91 679.49 11.04 8.2

3/25/2009 16:00

0.06 7.11 78.74 19.71 59.01 670.1 11.01 8.23

3/25/2009 16:01

0.05 4.89 77.47 19.13 58.15 663.28 11 8.24

3/25/2009 16:02

0.05 1.36 77.16 19.92 57.13 668.92 11.01 8.24

3/25/2009 16:03

0.04 -1.31 75.2 19.29 55.9 662.99 10.97 8.27

3/25/2009 16:04

0.05 -1.58 73.78 18.18 55.73 657.71 10.95 8.29

3/25/2009 16:05

0.06 -1.16 75.69 18.64 57.24 665.98 10.97 8.28

3/25/2009 16:06

0.05 2.88 71.83 17.2 54.56 654.89 10.93 8.32

3/25/2009 16:07

0.05 -0.44 69.79 16.6 53.26 652.94 11.03 8.25

3/25/2009 16:08

0.04 -2.17 77.13 18.92 58.17 676.35 11.07 8.19

3/25/2009 16:09

0.04 1.52 79.11 19.9 59.28 672.9 11.03 8.2

3/25/2009 16:10

0.05 0.91 76.3 18.93 57.43 665.83 11.02 8.22

3/25/2009 16:11

0.04 1.22 75.77 19.55 56.28 663.99 11 8.23

3/25/2009 16:12

0.04 5.53 75.74 19.15 56.62 662.08 10.96 8.28

3/25/2009 16:13

0.05 -0.56 73.02 18.9 54.32 656.6 10.94 8.3

3/25/2009 16:14

0.06 -2.16 73.51 18.92 54.56 660.39 10.95 8.3

3/25/2009 16:15

0.04 6.47 76.16 19.31 56.95 667.33 10.99 8.26

3/25/2009 16:16

0.05 2.8 76.78 20.13 56.79 673.56 10.99 8.26

3/25/2009 16:17

0.05 0.54 69.9 16.54 53.47 652.03 10.99 8.27

3/25/2009 16:18

0.05 2.38 75.92 17.61 58.27 672.62 11.07 8.18 0.05 1.58 78.33 19.72 58.64 677.02 11.03 8.21

10
3/25/2009 16:28 0.05 1.23 75.63 16.76 59 665.3 10.97 8.27 3/25/2009 16:29 0.05 0.6 73.06 16.2 56.83 665.57 11.05 8.21 3/25/2009 16:30 0.04 -0.37 82.12 18.34 63.83 681.42 11.03 8.2 3/25/2009 16:3 1 0.07 5.41 78.82 17.48 61.38 671.74 Ii 8.24 3/25/2009 16:32 0.05 -0.11 80.74 18.17 62.62 678.21 11.01 8.22 3/25/2009 16:33 0.04 1.15 79.03 16.65 62.34 666.34 10.98 8.26 3/25/2009 16:34 0.04 -2.67 76.54 16.26 60.3 662.92 10.95 8.29 3/25/2009 16:35 0.06 1.54 73.44 15.88 57.71 657.97 10.97 8.28 3/25/2009 16:36 0.06 4.91 74.3 16.06 58.47 669.27 11.05 8.2 3/25/2009 16:37 0.05 -0.54 78.46 16.85 61.64 672.15 11 8.23 3/25/2009 16:38 0.05 4.8 79.02 16.81 62.3 672.89 11 8.24 3/25/2009 16:39 0.04 -1.41 74.16 17.07 57.! 658.32 10.96 8.28 3/25/2009 16:40 0.05 1.53 75.65 18.68 56.94 668.04 10.97 8.26 3/25/2009 16:41 0.05 1.23 75.17 20.84 54.42 661.28 10.94 8.29 3/25/2009 16:42 0.05 1.07 76.9 20.15 56.73 664.01 10.94 8.3 3/25/2009 16:43 0.04 -2.61 72.21 19.03 53.31 656.46 10.94 8.3 3/25/2009 16:44 0.05 2.33 74.27 16.78 57.54 665.66 11.05 8.21 3/25/2009 16:45 0.06 0.72 79.85 19.22 60.64 678.98 11.02 8.21 3/25/2009 16:46 0.05 0.4 78.51 18.04 60.54 670.4 10.97 8.25 3/25/2009 16:47 0.05 2.01 80.26 19.68 60.66 670.84 10.97 8.26 3/25/2009 16:48 0.05 -0.51 75.88 18.44 57.48 658.54 10.94 8.29 3/25/2009 16:49 0.06 5.28 74.57 18.1! 56.54 660.79 10.94 8.3 3/25/2009 16:50 0.05 1.93 71.45 15.66 55.97 655.73 11.02 8.25 3/25/2009 16:51 0.05 0.54 79.19 16.59 62.65 680.77 11.05 8.2 3/25/2009 16:52 0.06 4.39 77.23 15.97 61.39 670.37 10.99 8.26 3/25/2009 16:53 0.05 0.57 77.55 15.86 61.74 672.66 11.01 8.25 3/25/2009 16:54 0.05 1.54 77.61 15.61 62.15 675.12 11.01 8.25 3/25/2009 16:55 0.05 -2.19 74.82 13.62 61.25 664.69 10.98 8.28 3/25/2009 16:56 0.05 1.73 72.1 13.79 58.44 661.1 10.96 8.31 3/25/2009 16:57 0.04 -4.47 70.3 12.75 57.54 658.58 11.01 8.28 3/25/2009 16:58 0.05 -3.07 74.55 13.03 61.53 673.8 11.08 8.19 3/25/2009 16:59 0.06 -0.48 76.72 14.15 62.77 679.9 11.04 8.22 3/25/2009 17:00 0.06 0.01 74.46 14.16 60.29 675.35 11.03 8.24 3/25/2009 17:01 0.05 0.52 79.85 14.72 65.13 677.98 11.04 8.23 3/25/2009 17:02 0.05 2.84 74.55 14.47 60.34 666.1 11 8.26 3/25/2009 17:03 0.05 -2.53 73.2 13.36 59.82 664.11 11.03 8.25 3/25/2009 17:04 0.05 2.45 74.63 13.92 60.79 673.4 11.07 8.21 3/25/2009 17:05 0.05 2.51 79.73 15.6 64.18 684.98 11.07 8.19 3/25/2009 17:06 0.05 -2.09 74.68 15.01 59.54 666.22 11.01 8.26 3/25/2009 17:07 0.05 0.01 78.68 17.26 61.46 676.5 11.04 8.23 3/25/2009 17:08 0.05 -4.24 76.66 16.13 60.5 669.5 11.01 8.26 3/25/2009 17:09 0.05 -1.87 73.43 14.89 58.54 662 10.98 8.29 3/25/2009 17:10 0.04 -5.21 73.94 14.56 59.34 664.33 10.98 8.28 3/25/2009 17:11 0.05 -0.63 76.99 15.86 61.13 676.11 11.01 8.26 3/25/2009 17:12 0.04 -5.65 69.02 13.69 55.38 654.84 11 8.29 3/25/2009 17:13 0.05 -2.45 70.86 13.9 57.05 668.37 11.07 8.22 3/25/2009 17:14 0.05 -2.33 76.23 11.89 64.42 682.61 11.05 8.22 3/25/2009 17:15 0.05 -3.36 75.31 12.22 63.35 675.13 11.05 8.23 3/25/2009 17:16 0.05 -4.36 74.61 12.18 62.6 673.35 11.04 8.22 3/25/2009 17:17 0.05 -7.85 75.15 11.97 63.2 672.48 11.01 8.26 3/25/2009 17:18 0.05 -3.9 69.87 9.81 59.93 658.86 11.03 8.25 3/25/2009 17:19 0.06 -1.65 73.81 10.39 63.46 675.18 11.08 8.21

11
3/25/2009 17:29 0.04 3.74 73.31 15.11 58.09 669.63 11 8.27 3/25/2009 17:30 0.05 2.35 73.04 14.29 58.77 667.13 11.03 8.26 3/25/2009 17:31 0.05 2.67 73.51 14.64 59 672.6 11.06 8.22 3/25/2009 17:32 0.04 1.9 76.05 15.57 60.48 673.51 11.02 8.24 3/25/2009 17:33 0.06 4.01 74.49 14.99 59.58 667.14 11.01 8.27 3/25/2009 17:34 0.05 0.41 74.76 14.75 60.05 668.08 11.01 8.27 3/25/2009 17:35 0.06 -2.51 71.63 14.41 57.32 660.22 10.98 8.29 3/25/2009 17:36 0.05 1.77 72.92 15.31 57.51 669.89 11.07 8.22 3/25/2009 17:37 0.05 -0.01 75.35 15.52 59.87 672.24 11.04 8.23 3/25/2009 17:38 0.05 2.51 75.79 16.27 59.51 674.04 11.04 8.23 3/25/2009 17:39 0.06 -1.68 75.78 14.71 61 670.68 11.02 8.25 3/25/2009 17:40 0.06 -2.12 72.81 14.66 58.27 665.83 11 8.27 3/25/2009 17:41 0.05 -3.92 75.31 15.09 60.26 670.73 11 8.27 3/25/2009 17:42 0.04 -1.44 73.02 15.29 57.93 667.27 ii 8.27 3/25/2009 17:43 0.04 -2.59 70.35 13.2] 57.19 657.98 11.04 8.26 3/25/2009 17:44 0.06 -1.52 75.32 16.16 59.35 683.37 11.07 8.2 3/25/2009 17:45 0.05 -0.31 74.76 15.85 58.9 651.54 10.9 8.21 3/25/2009 17:46 0.05 4.03 34.53 10 24.47 49.16 12.49 1.76 3/25/2009 17:47 0.05 1.46 18.19 4.18 13.95 5.14 13.56 0.17 3/25/2009 17:48 0.05 -5.78 13.24 3.21 10.22 4.88 13.55 0.01 3/25/2009 17:49 0.05 1.4 8.79 2.04 6.92 5.25 2.74 6.06 3/25/2009 17:50 0.05 2.11 6,12 1.34 4.72 5.74 0.16 8.16 3/25/2009 17:51 0.06 0.75 4.56 1.32 3.25 5.23 0.1 8.28 3/25/2009 17:52 0.05 3.65 3.63 1.31 2.33 5.33 0.07 8.21 3/25/2009 17:53 0.04 -2.86 6.4 1.85 5.13 38.75 0.35 1.25 3/25/2009 17:54 0.06 5.2 59.35 21.28 38.6 634.62 10.01 7.04 3/25/2009 17:55 0.05 2.17 59.02 14.96 44.14 662.39 10.92 8.18 3/25/2009 17:56 0.04 -2.99 62.04 15.74 46.43 662.59 10.98 8.23 3/25/2009 17:57 0.06 4.03 70.87 20.19 50.64 675.44 10.99 8.25 3/25/2009 17:58 0.05 3.07 72.68 23.15 49.5 673.85 11.03 8.22 3/25/2009 17:59 0.05 0.61 77.63 25.14 52.47 679.4 11.02 8.22 3/25/2009 18:00 0.05 -2.27 72.67 23.2 49.53 661 10.97 8.28 3/25/2009 18:01 0.04 -0.35 74.5 24.12 50.53 666.59 10.99 8.27 3/25/2009 18:02 0.05 2.15 72.99 23.75 49.21 663.25 11.05 8.22 3/25/2009 18:03 0.05 2.26 77.59 25.18 52.36 678.12 11.04 8.22 3/25/2009 18:04 0.05 0.99 78.46 22.85 55.75 676.74 11.04 8.23 3/25/2009 18:05 0.05 1.15 77.84 20.47 57.51 668.02 11.02 8.24 3/25/2009 18:06 0.05 -0.42 73.45 18.81 54.66 667.03 11.01 8.26 3/25/2009 18:07 0.05 0.78 75.54 18.74 56.77 666.78 11.01 8.26 3/25/2009 18:08 0.04 -0.48 74.25 17.47 56.98 672.52 11.04 8.23 3/25/2009 18:09 0.06 1.14 75.23 16.5 58.6 672.46 11.04 8.24 3/25/2009 18:10 0.05 1.82 75.88 16.33 59.59 670.19 11.01 8.26 3/25/2009 18:11 0.04 3.89 74.29 15.88 58.61 666.14 11.03 8.25 3/25/2009 18:12 0.06 1.43 74.02 15.27 58.8 669.06 11.07 8.22 3/25/2009 18:13 0.05 -0.8 77.25 14.9 62.31 676.78 11.06 8.21 3/25/2009 18:14 0.05 0.06 77.08 14.87 62.25 674.31 11.04 8.23 3/25/2009 18:15 0.05 0.65 76.12 14.58 61.5 672.54 11.03 8.24 3/25/2009 18:16 0.05 3.42 75.38 13.71 61.63 665.98 11.02 8.25 3/25/2009 18:17 0.06 4.3 75.73 15.28 60.4 669.84 11.02 8.26 3/25/2009 18:18 0.04 -2.63 75.24 16.61 58.58 666.22 11.02 8.25 3/25/2009 18:19 0.05 -0.96 75.75 16.94 59.01 665.91 11.01 8.27 3/25/2009 18:20 0.05 1.56 72.69 16.78 55.87 659.84 11.01 8.27

12
3/25/2009

0,05 

5.92 1.95 2.88 1.72 670,95 11.06 8.23

3/25/2009

18:31 0.04 -6.28 1.76 2.66 1.55 673.22 11.09 8.2

3/25/2009

18:32 0,06 8,31 0.49 1.86 1.78 673.45 11.04 8.24

3/25/2009

18:33 0.06 9.41 0.72 1.61 1.78 665.65 11.01 8.27

3/25/2009

18:34 0.05 5.33 -0.03 1.91 1.4 674 11.03 8.25

3/25/2009

18:35 0,04 -4.65 1.12 1.97 1.54 669.58 11.01 8.26

3/25/2009

18:36 0.06 -1.43 0.62 1.93 1.68 667.14 11 8.29

3/25/2009

18:37 0,04 2.7 0.8 1.85 1.52 666.25 11.03 8.26

3/25/2009

18:38 0.06 0.01 1.79 1.57 2.13 668.17 11.07 8.21

3/25/2009

18:39 0.04 2.93 1.54 1.74 1.61 674.32 11.03 8.24

3/25/2009

18:40 0.05 -3.55 0.51 2.34 1.28 675.19 11.04 8.23

3/25/2009

18:41 0.05 -3.15 -0.37 2.16 1.5 675.66 11.06 8.22

3/25/2009

18:42 0.06 -2.4 -0.01 1.72 1.58 675.85 11.09 8.19

3/25/2009

18:43 0.05 3.08 0.88 1.82 1.65 678.09 11.04 8.23

3/25/2009

18:44 0.05 2.54 0,47 1.98 1.48 672.38 11.02 8.25

3/25/2009

18:45 0,05 -2.62 -0.52 1,87 1.37 671.19 11.01 8.26

3/25/2009

18:46 0.05 -0.48 1.05 1.48 2.04 663.57 10.99 8.28

3/25/2009

18:47 0,04 7.4 1.43 1.68 1.55 663.59 11.05 8.25

3/25/2009

18:48 0.05 4.89 1.28 1.56 1.66 679.67 11.07 8.2

3/25/2009

18:49 0.05 2.35 0.87 l.59 1.68 672.27 11.03 8.24

3/25/2009

18:50 0.04 1.04 -0.59 2.1 1.23 672.29 11.04 8.24

3/25/2009

18:51 0.04 2.22 -0.84 2 1.15 670.33 11.02 8.25

3/25/2009

18:52 0.05 0.02 -0.84 1.96 1.21 664.67 11 8.27

3/25/2009

18:53 0.05 -1.58 -0.36 1.71 1.38 664.68 11.06 8.23

3/25/2009

18:54 0.05 3.43 1.88 1.33 1.97 681.06 11.07 8.2

3/25/2009

18:55 0.05 -0.26 0.82 1.62 1.54 675.88 11.04 8.23

3/25/2009

18:56 0.05 4.71 0.49 1.65 1.4 674.82 11.04 8.23

3/25/2009

18:57 0.06 1.82 1.03 1.47 1.66 671.35 11.03 8.24

3/25/2009

18:58 0.05 1.94 0.26 1.71 1.41 662.78 11.03 8.26

3/25/2009

18:59 0.05 2.98 0.41 1.73 1.49 675.18 11.05 8.23

3/25/2009

19:00 0.05 2.9 0.89 1.73 1.55 675.92 11.05 8.23

3/25/2009

19:01 0.05 2.69 0.42 1.78 1.46 678.11 11.09 8.2

3/25/2009

19:02 0.05 3.3 0.68 1.74 1.51 674.l6 11.05 8.22

3/25/2009

19:03 0.05 2.35 0.82 1.69 1.52 668.25 11.04 8.24

3/25/2009

19:04 0.06 1.23 0.64 1.65 1.45 472.92 10.31 6.66

3/25/2009

19:05 0.05 2.15 0.71 1.69 1.5 6.9 13.45 0.48

3/25/2009

19:06 0.05 -2.87 0.66 1.53 1.21 4.43 13.56 0.06

3/25/2009

19:07 0.05 -1.51 0.47 1.53 1.21 4.23 13.57 0.01

3/25/2009

19:08 0.04 -1 0.6 1.61 1.34 3.81 13.58 0.01

3/25/2009

19:09 0.04 2.03 0.81 1.56 1.45 13.76 6.93 3.79

3/25/2009

19:10 0.06 6.47 1.54 1.39 1.59 4.54 0.21 8.09

3/25/2009

19:11 0.05 -0.07 1.26 1.55 1.28 4.1 0.13 8.27

3/25/2009

19:12 0.06 -1.03 0 1.65 1.65 4.06 0.09 8.32 19:13 0.05 3.91 0.56 1.79 1.41 3.86 0.06 8.33

13
Static Pressure (in. H20)

CO2Content (%)

Wet Bulb Temp.

Inches from

Stack Wall

Traverse Poini

stacK

Temperature Velocity Head Number (°F) (in. H20) Null Angel (zero angle)

cj’ / ,7L2 Z yf ci..cL1 3

/2L.H 1-I 3Lf’ 7:7tL 5 5?9 .6

( 32.

: (çL)-zz

çc:; 3 5

7 ‘30

Stack / Duct Measurements

A=

Sample Ports

r= zi

.— L.j L

L\

‘,1;1)

.... ‘7 677

t 3,o z

3 c)

L4 c-S’f ZZ C) QIL2

-

x

Round Duct Dia. (D)

Square Duct (LxW)

Square DuctDia. (De):

De = 2LW / (L+W)

Straight Length:

(diameters)

(., -zi

AID

B/D

Traverse

Point

0.5 1 1.5 2 2.5 I I

24 or 25

p:ateil2

No. ofTraverse Points Per Dia.

6 8 10 12

4.4

14.6

29.6

70.4

85.4

9 5

2

3

4

5

6

7

8

9

10

II

12

3.2

10.5

19.4

32.2

67.7

80.6

89.5

96.8

B

a- Higher No. for rectanguar stacks

b- For stacks between 12 and 24 in.

2.6

8.2

14.6

22.6

34.2

65.8

77.4

85.4

91.8

I

2.1

6.7

11.8

17.7

25.0

35.6

64.4

75.0

82.3

88.2

93.3

97 9

97.
Traverse

Point

2

3

4

)

6

7

8

9

10

11

12

BID

No. ofTraverse Points Per Dia.

6 8 10 12

4.4 3.2 2.6

14.6 10.5 8 2

29.6 194 14.6

704 322 22.6

85.4 67.7 34 2

96.5 80.6 65.8

89.5 77.4

85.4

F-:; 974

2.1

6.7

11.8

17.7

25.0

35.6

64.4

75.0

82.3

81.2

93.3

97.9

Static Pressure (in. H,O)

,

CO2Content (%)

Wet Bulb Temp.

Inches from

Stack Wall

Traverse Point

Number

Stack

Temperature Velocity Head Null Angel (°F) (in. H20) (zero angle) Stack / Duct Measurements

I

2- .3 cgJ

.3 .(O Z

—

c-Z 3(1-) C)

6

9 WI’

O.

•3A 3

—

5

M

-

:::

— 2-

I .z 5

— 3 cD

—- 9.

S 35 5-

(1:,

Sample Ports

Round Duct Dia. (D)

Square Duct (LxW)

x

Square Duct Dia. (De):_____ De=2LW/(L+W)

Straight Length: A / D

(diameters)

A

1 1.5 2 0.5 2.5 I I I I I

24 or 25

If--

8 or 9 I I 2 I 3 4 5 6 7 8 9 10 B

a- Higher No. for rectanguar stacks b- I or stacks hetween 12 and 24 in.
Static Pressure (in. H20)

6 7 8

B

CO2Content (%)

Wet Bulb Temp.

Traverse

Point

2

3

4

5

6

7

8

9

10

11

12

BID

No. of Traverse Points Per Dia.

6 8 10 12

4.4 3.2 2.6

14.6 20 5 8.2

296 19.4 146

704 322 226

85.4 67.7 342

96.5 80.6 65.8

89.5 774

968 854

2.1

6.7

11.8

17.7

25.0

35.6

64.4

75.0

82.3

88.2

93.3

97.9

Inches from

Stack Wall

Traverse Poini

Number

Stack

Temperature

(°F)

Velocity Head

(in. H20)

Null Angel

(zero angle)

— z

. 3 I

L

.;

I z 2.O 2 <glç

— .

L

— 3,4/

::: 3,3

Stack I Duct Measurements

Sample Ports

Round Duct Dia. (D)

Square Duct (LxW) x

Square Duct Dia. (De):__________________ De2LW/(L+W)

Straight Length: A I D

(diameters)

0.5

A

1 1.5 2 I I I I I

24 or 25

8 or 9’ I I I 2 3 4 5

9

a- Higher No. for rectanguar stacks b- For stacks between 12 and 24 in.

2.5

10
Static Pressure (in. 1-170)

.3

L1

c

‘,.)

q

Velocity Head Null Angel

(in. H20) (zero angle)

13cDa’:

c’Z ? I

ZA 77Q

q5c-7

Y7

...-) -‘.

.,‘5

CO2Content (%)

Wet Bulb Temp.

Traverse

Point

2

3

4

5

6

78

9

10

II

12

BID

No. of Traverse Points Per Dia.

6 8 10 12

4:4 3.2 2.6

14.6 10.5 8.2

29.6 19.4 14.6

70.4 32.2 22.6

85.4 67.7 34.2

96.5 80.6 65.8

89.5 77.4

96.8 85.4

91.8

•71S

Inches from

Stack Wall

Traverse Point

Number

Stack

Temperature

(°F)

I ci 2 f7q

ji

z_

Stack / Duct Measurements

{A=

Sample Ports

.-

—-----.---—- —

-3 .3

Round Duct Dia. (D)

Square Duct (LxW) x

Square Duct Dia. (De):_____ De=2LW/(L+W)

Straight Length: A / D

(diameters)

0.5

A

1 1.5 2 2.5 I I. I

24or25

16

8 or 9’ I I I I 2 I 3 4 5 6 7 8 9 10 B

a- Higher No. for rectanguar stacks b-For stacks between 12 and 24 in.

2.1

6.7

11.8

17.7

25.0

35.6

64.4

75.0

82.3

88.2

93.3

97.9
0.5

1

Traverse

Point

2

3

4

5

6

7

8

9

10

11

12

BID

fTo. Of Traverse Points Per Dia.

6 8 10 12

4.4 3.2 26

146 10.5 82

296 194 146

70.4 32 2 22.6

85.4 67 7 34.2

965 806 65.8

89.5 77.4

96.8 854

918

974

2.1

6.7

11.8

17.7

25.0

35.6

64.4

75.082.3

88.2

93.3

97.9

Static Pressure (in. f120)

77

Inches from

Stack Wall

CO2Content (%)

Wet Bulb Temp.

Traverse Point

Number

Stack

Temperature Velocity Head Null Angel (°F) (in. H20) (zero angle) Stack / Duct Measurements

_____

I 7•7

3.1-

— 3

.

.

—-

.

I 75

—

Lt

— 5c’

[A=

Sample Ports

Round Duct Dia. (D)

x Square Duct (LxW)

Square Duct Dia. (De):_____ De = 2LW / (L+W)

Straight Length: A I D

(diameters)

A

I

1.5

24 or 25

16 Non-particulate 12

2.5

8or9 I I 2 3 4 I I I 5 6 7 8 9 10 B

a- Higher No. for rectanguar stacks

b- For stacks betv.’eeii 12 and 24 in.
Static Pressure (in. 1120) 7, 6,

Inches from Traverse Poini

Stack Wall Number

q

5 cj7

,

(

.7 7Lç

77

c479

U

c

L

A

1.5

3 4 5 6

a- Higher No. for rectanguar stacks

h For stacks hetwean 1 2 acd 24 in.

Stack! Duct Measurements

Traverse

Point

2

3

4

5

6

7

8

9

10

11

12

BID

No. of Traverse Points Per Dia.

6 8 10 12

4.4 3.2 2.6

14.6 10.5 8.2

29.6 19.4 14.6

70.4 32.2 22.6

85.4 67.7 34.2

96.5 80.6 65.8

89.5 77.4

i- 96.8 85.4

91.8

97.1

O2Content (%)

Wet Bulb Temp.

Stack

Temperature

(°F)

Velocity Head Null Angel

—

(in. 1120) (zero angle) c-7 —..o

—-

.

z 75 3J3

.33

3,4

.2,-7-

h.

iic 3rt1

7z 3*-

Sample Ports

.5

3,-

3’

3,5

r79 .3 3,

Round Duct Dia. (D)

Squate Duct (LxW) x

0.5

Square DuctDia. (De):________________ De=2LW/(L+W)

StraightLength; AID

(diameters)

2 2.5 I I I I I

24 or 25

Non-particulate 16 12

8 or 9’’

9 10

2

7

B

8

2.1

6.7

11.8

17.7

25.0

35.6

64.4

75.0

82.3

88.2

93.3

97.9
Static Pressure (in. H7O)

tent (%)

Wet Bulb Temp.

Stack

Inches from Traverse Point Temperature Velocity Head Stack Wall Number (°F) (in. H20)

Round Duct Dia. (D)

Square Duct (LxW) x

Square Duct Dia. (Be):_____

Be = 2LW I (L+W)

Straight Length: A / B

(diameters)

BID

2

3

4

)

6

7

8

9

1(1

11

12

4.4 32 26

14.6 105 82

296 194 146

704 322 226

854 677 342

965 806 658

89.5 77.4

96 8 85.4

91 8

97t

2.16.7

11.8

172

25.0

35.6

64.4

75.0

82.388.2

93.397.9

—7-)’; I —

Null Angel Stack I Duct Measurements

(zero angle)

A

1 ‘77

-_-*___ .

—

77 3

47I:7

z 79 3,4

. z

__ q 76

—- 173

Sample Ports

0.5

A

Traverse 1 1,5 2 2.5 Point I I I I

24 cr25’

20

16

Non-particulate 12

8 or9b I I 2 3 4 5 6 7 8 9 10

No. ofTraverse Points Per Dia.

6 8 10 ._2

a

a- Higher No. for rectanguar stacks

h- For stacks between 12 and 24 itt.
Static Pressure (in. 1-120)

CO2Content (%)

Wet Bulb Temp.

Round Duct Dia. (B)

Square Duct (LxW) x

Square Duct Dia. (Be):

Dc = 2LW / (L+W)

Straight Length: A I D

(diameters)

BID

4.4 3.2 26

146 .105 82

296 194 1’6

704 322 226

854 677 342

965 806 658

89.5 77.4

:>—; 96.8 854

918

2.16.7

11.8

17.7

25.0

35.6

64.4

75.0

82.3

88.2

93-3

97.9

7.o

Inches from Traverse Point

Stack Wall Number

Stack

Temperature Velocity Head Null Angel (°F) (in. H20) (zero angle) Stack I Duct Measurements —

I

2

:z .

Lk

Z__ S 7c3,q

—--

—_

z

—--

2.- D733-’t 7t q

.3

L -?‘l 73t .—_—z____ S 76 42t3. C 73 73

Sample Ports

EZZZ

A

Traverse No. of Traverse Points Per Dia.

Point 6 8 10 12

2

3

4

a

6

7

8

9

10

1112

B

a- Higher No for rectanguar stacks

For stacks etwesu 2 and 24 in.
G

‘J

+

z

p

Ii II

0’

L

z

H

C

r W

., ,

C

I I

E

B

q

B
% CO,

Moisture

Total Moisture Gain: Impingers Silica gel Total Description of silica gel

Description of irnpinger solution

Recovered Sample Filter container number

Description of particulate Sealed?

Back halfrinse container number Front halfrinse container number

Liquid level marked 

Liquid level marked Samples stored and locked

- Remarks

Blank filter container no.

Blanck PH rinse container no. Blank BH rinse container no. Blank reagent container no.

Date of laboratory custody —

Remarks

Blanks

4

Method Used:

Fyrite Orsat flO2 ECOH

Impinger 1st 2nd 3rd 4th

6th Silica gel Final 77 mUg 709 J(ã-:,

mUg Initial (g7, 7mug ?Oimug 7pL[3Jg mug mUg mug Net Gain , mu 1 (, mu mUg mUg mug
-ofl

I r

El

[I

I I I I I I I

—

—

+ +

z

+
Method Used:

Fyrite Orsat % CO2

Moisture

Total Moisture Gain: Impingcrs 1j Silica gel. 7 Total Description of silica gel

Description of iinpinger solution

Recovered Sample

Filter container number

Description of particulate Sealed?

Back halfrinse container number Front halfrinse container number

Samples stored and locked

Remarks

Blank filter container no.

Blanck FH rinse container no. Blank BH rinse container no.

Blank reagent container no.

Date of laboratory custody

Blanks

-Liquid level marked

Liquid level marked

Net Gain ‘7t( rLfg

Impinger 15t 2 3rd 4th 5th 6th Silica gel Fm 77 mUg 710 3 m 7j Initial 7oo mUg mUg mig 7 oO .mJJg mug mUg mUg 2J mug mUg mI_Jg mug

Remarks
5”

fl

‘-a

a a a a a a I

‘‘—

+

C-) 0
Method Used:

Fyrite Orsat

or r’ /o_, )

Moisture

Description of silica gel

Description of irupinger solution

Recovered Sample

Filter container number

Description of particulate Sealed?

Back halfrinse container number Front halfrinse container number Liquid level marked

-Liquid level marked

Samples stored and locked

Remarks

Blank filter container no.

Blanck FH rinse container no.

Blank BH rinse container no.

B lank reagent container no.

Date of laboratory custody

Blanks

Total Moisture Gain: irnpingers’ Silica ge1[\ L Total

Remarks
IsaIdneIje Field Sampling Data Sheet

Pon — Pbar+ (H@/t36) =

Phar + (Potol/l36)

Md —

Ms — (Md)(l-(n 5,lOO))+l S(Sws/lQO)

(VWC+VWO 6)/(VWC+V+V)

Vwc = O.04706(Vf_vj)

Vwsg OS4? lS(Wf-wj

Co isp airy

Test Dale

Tent Number

Operator

Fitter Numbers

Bar. Press (Pb)

Statie PSess (Pa)

Slack Di (hi,)

Lash flte Fired

(2

Mf 5(TovTs) * (dP)

MI— 846.72 ° (Da°4)

Mf

Note: All tensperatuaes arc *R (*F+460)

(H@) * (Cp’2) ((l-(BwsIloo))e2) Mf (Md/Lis) 846.72 (Ps/Pin)

(IC()5,0)*(_

Nozzle050ernsaoutjou.

H@ 4 / Kisa*(cp)02* 0.(BwsIlOO))e2*(Md/M)*(PSJ

(l°,ecoonrncnd maltiplyong calculate nozzle size by 5%) Do 5(55=

Yc— (lChVnt)*((oo5 19*(Tm))/pb)sg5

DERENZO AND ASSOCIATES, INC.
of r /OL

Moisture

Initial (1,qq Jg

Total Moisture Gain:

(q/.3ig(,;o3;) mUg

inipingers Jf\s

rnugq/,D

mU[ rv

IotaI

Description of silica gel

Description of Impinger solution

Recovered Sample

Filter container number

Description of particulate Sealed?

Back halfrinse container number Front halfrinse container number

Samples stored and locked

Remarks

Blank ifiter container no.

Blanck FH rinse container no.

Blank BH rinse container no.

Blank reagent container no.

Date of laboratory custody

Remarks

Blanks

-Liquid level marked

Liquid level marked

Method Used:

Fyrite Orsat %O2J FCO

npinger I le 20d 3rd 4th 5th 6th Silica gel

[Final 7gjg 7Q1qrniig /,/ mug mUg mug Zg

\\\mUg ,\ mU m

mUg mUg

Silica gel(
Inokinelic Field Sompling Dots Sheet

Mf= 846.72’ (Dn4) *

(H@) (C2) ((l-(Bws/loo)y 2)

* (Md’Ms) Mf= (Ps/Pin)

Mf846.72 (tlj‘(_2.2 LL1J_.J *LfL.j

3.%

Nozzle Dcleimjnoiion:

H@ 4

(Recommend

/ Kiso’(cpy2’(l.(8w 5/l

multiplying calculate

OO)Y’ 2’(Md/Mo)*(Ps/Pm)*ç1’pJr 5).

nozzle size by 5%) Do

shP(, 0

‘I .05

Pm. Pbnr+(Hl36)

Pn Pboe+(Pntnl/l3b)

Md —

O.44(%CQ2)fo32(%)+o2s(%N t’Co Ms (Md)(t-(flws/loo))÷l S(Bwu/l 00) Bws —

(VWC+Vwsg)/(vwc+vwsg+vm)

Vwc O.O 47Q6(vfvl)

Vwsg — O.O 47l5(Wf.\vi)

3 o1 &

Nate: All lemperatores ore R (‘F+460) Yc— (lOfVm)’((003 l9’(Tm))/pbyo5

DERENZO AND ASSOCIATES INC.
Method Used:

Fyrite Orsat

% CO2

Moisture

0//0 2 % CO

Inapinger 2’ 3rd 4th 5th 6th

Silica gel

Final 77t’frsJg 747/ mL!g

Initial

Ug mUg mUg mUg mJJg ( $r1ig (‘oq 1 mUg

NetGain mUg mIJg mUg

g mUg kUg mUg mUg mUg

Total Moisture Gaii: Impingers [ \

siiicagei Total

Description ofsilica gel

Description of impinger solution

Filter container number

Description ofparticulate

Back halfrinse container number

Front halfrinse container number

Recovered Sample

Sealed?

- Liquid level marked

-Liquid level marked

Samples stored and locked —

Remarks

Blank filter container no.

Blanck FH rinse container no.

Blank BH rinse container no.

B lank reagent container no.

Date of laboratory custody

Blanks

Remarks
Company

Field Sampling Data Sheet

Tot Date

Test Nunther

Operator

Filler Number 0

Oar. Freon (Pb)

Static Press (Ps)

Stoeb Din (to.)

I Tein 1t.

toter G Oatiel7 Probe Filter 13os Leo mop. Trim, 15 Temp

35 Trio 1,.

Mf a (Tmns) (P) Note: AU temperatemm ore 5R (‘F+460)

Yc— (l0Nm)s((OO319sm))b) Mf 046.72 5 * (0004) *

(M!@) * (Cp 02) ((l-(Bws/loo)y2) Mf= (MW14 5) (Ps/Pm) 846.72 *

,‘

s

( • (*

Pm — Pbor+ (H@/l3.6)

— Pbur + (Pstat/l 3.6)

Md —

Ms — (Md)(l-(fl 5,j00+j S(Bws/lOO)

Nozzto Detemsmtm,aal,on

Owl (Vwc+Vwsg)/(Vwc+v+v)

H@ / Ktso*(Cp)02.()(Bws/)OO02(Md/1 5)5(

5(,_n

Vwc 0 4706(Vfv((

(Recoom.niead mulliplytog calculate nozzle size by 5%) On t.05=

Vwog

DERENZO 0.0471 5(Wf-W 1)

AND ASSOCIATES, INC.
Method Used:

Fyrite

Orsat

r % O

% CO [ ]

Moisture

pinger l nd 3rd

6th

Silica gel

[Final 7f mg ?SA

al 7033mug t9Zrnvg c,oq/mug [Gain mUg mvg (‘mLIg \ mUg mUg mUg mUg

Total Moisture Gain: Impingers Silicagel Total

Description ofsilica gel

Description of impinge: saiu:ioe.

Recovered Sample

Filter container number

Description Sealed? of particulate

Back halfrinse container number

Front halfrinse container level marked number

level marked

Samples stored and locked

Remarks

Blanks

Blank filter container no.

Blanck FH rinse container no.

Blank BH rinse container no.

Blank reagent container no.

Date of laboratory custody —

Remarks
2

C? ‘7’

I - ‘2.0

‘(2,

c2’7 0

,

,‘:20

2

M205 Divider Certification

Inst 100% I I

(3( 60% — 12-

, 2 5 (5 40%-.f

8-o 

0% C9c,( 

ioO 2Lc (3 2 60% _i2 ..C.(3 

(3) 40% — C 

0% 

35Q 100% _2,’D 3 ‘- 

— 60% 

(2. — 40% 

-C) ( C) 

j_ 02 Inst mid _g 5 Must be within 10% of one of the above cuts 

zero 0

(Z mid _La3 I5 

zero / C)

LL7 

mid (5

Analyzer Calibration Error Ins

_lgc( C 

f5c5

zero

-( 2.. CO2Inst high (• ç ( 73:5 

mid(( .( 

zero 

O Inst high Ca’ zocp 

mid 

(5 - — zero

/52 NOx Inst

87 (7 

r1 — Response Times (see)

CO upscale: (3C)3 System Bias / Pre-Stratification

CO downsca1er5af2q./,q

‘_______

(5i’( I_yn _pscaleJc 4o. @9 JMust be closest to stack concentration 4 downscale CO2upscale: I5cf12t,- •5q3f — L ij P2 Dyn upscale CO2downsca1e;i 5qq ,‘- 52 .5( (2 

downscaie 02 Upscale5’($ 

Stratification probe lengths (m)

[xUsc:7

E upscaijf 

N[Ox Downsca e: (, 

downscale

Calibration Error iC-C)/CS x 100 (must be < 2%) Concentration direct instrament reading Cv = Concentration value

Initial System Bias (SB)=(C 5- C)/CS * 100 Cs = Concentration ofsystem (mustbe< 5%) CS = Calibration Span

SBf = System Bias fmal

SBi = System Bias initial

c3.c(

Calibration Drift =(SB - SBi) (must be <3%)
(7(C( CODyn mid

zero

(—7çz.. CODyn mid

zero

O2Dyn mid

zero

({7 I NOxDyn mid

L2- I zero

Cdir = Concentration direct instrument reading Cv = Concentration value

Cs

= Concentration of systeni

CS = Calibration Span

SBf = System Bias fmal

SBi

= System Bias initial

(t(

-qzyo

4

Post Stratification Calibration

IS

7 t’

(009. (i7

0-ac

/3.5/ 

From: - 0.0 K2z

I 

NOx Converter Test

NOx Converter Post-Calibration

I -H’ To:

J_ 4.

O

7 H9. 3 H Must be closest to bag NOx high value

I O-o9 I

- I (0f9

Calibration Error pre-test (Instrument)

/ ‘. 5-2

,.oo

0.o

•9g-

-?,5’

/o ( 7 Must be 100 -20% ofsuck concention

/, (0 - 2 Must be closest to stack concentration

0.0

(3.5

.

(i-C

?. 0.99

2.-

Analyzer 

COInst high 

mid 

zero 

_2. 3 COInst high 

mid 

zero

°2 Inst high 

çc 

zero (>.O

/ 

‘3 NOx Inst high 25 (.o3 G.

nid

zero

System Bias Calibration pre-test (dyn

(p’ 52- CO Dyn upscale t’02 S9 0cf.

-

downscale 0.. ‘(

5 CO Dyn upscale f?.3 (3, 52 -77 3 doscale 0.0 •

70 5 02 Dyn upscale 25 2 70 

downscale -2 - 0, 0.

? c’

9 NOx Dyn upscale 

7 2. downscale

PppieDyn high 

mid 

— low

-io9 7 I Methane Dyn high 

73, mid 

Z7(C) low 

zero imic calibration) 0% —7-7 —0-c S(f, 5 ,— zero o.o 9c-a5 0.(O 7G52? 3i( ?f77Q

0

Calibration Error (C, - C)/CS x 100 (must be< 2%)

Initial System Bias (SB) = (ç - Cd,)/CS * 100 (must be< 5%)

f2

(/c/Z (f2’.Z 7cf?.73 752-i

— Calibration Drift (SBf -SBi) (must be< 3%)
_l5 -

cc

(,c’ -

,c. 7’CO

3 — c7,

t’Oa-

•0.è

ii/r7— Rz7-.7

System Bias Calibration (dynamic calibration)

I.5-’(

(3.52

2c

a

3. o(O.(()

00

q-g -et

áq

hr

R.

C

System Bias Calibration (dynamic calibration) 4os( O’/5 12’? —3

2. ( c-’

g

— I —

2

C)c o.o

— -‘ ?o

c2

.7

c to

723-3

O.cS

/o?c2q ((9-

O.a

Cdir

= Concentration direct instrument reading Cv Concentration value

Cs Concentration ofsystem

CS Calibration Span

SBf

= System Bias final

SBi

= System Bias initial

System Bias Calibration (dynamic calibration) 

t D/.

ç

R:m: 523.23

Post Test 1

r-( CO Dyn upscale -5Q ‘.

5

‘ 2

— downscale O.r3 0.

Z CO2 Dyn upscale

— 13.

3

(- a Start Time: (1

— downscale -C) .0

QDyn upscale

— 3c) 

If

— downscale

0 ( - o I NOx Dyn upscale 1 t.

g (.

q c)4 33 downsca Stop Time:_______ (.( c3.(G ‘( F’ _Propane mid

— 

zero

_ç( Methane mid

zero

Test 2 Post Test 2 

CODyn upscale or,

j cf.

ç ftcc.( downscale -( Z

7;’, c( 22 Dyn upscale 

Start Time: 1 I ( I downscale

((( v..(

O2Dyn upscale _j

2 

_Jj{_ downscale of 

NOxDyn upscale 

/o -2 (? downscale

— ö.

3 

StopTime:’ ((z Propane mid

4 (9

— zero

-.0 ‘r 

((2C Methane mid /f’C) [.c./, f(97

2- zero

Test 3 Post Test 3

(257 CODyn upscale 

— downscale

/ 3 Dyn upscale 

St Time: 1 43 ( 0 doscale

.-3 (( 02 Dyn upscale

8

2 7

j3 c’3

— downscale 0. c’( ( f ,(7 NOx Dyn upscale 

(231

3 (0

— downscale 

Stop Time: __L3-( Propane mid j3

6 zero

(3

7 Methane mid 

zero

- 1a

-s —ge

Calibration Error =(C- CV)!CS x 100 (must be< 2%)

Initial System Bias (SB) (ç - Cdk)/CS * 100 (must be< 5%)

Calibration Drift =(SBf - SBI) (must be< 3%)
• Test

7fJf-(

Time:/f’ 7

Time:_/

Test 7

Time: 

Time: (7d;

Test’3 4

T1’ (-ct-3

nitial

alibration

System

Error

Bias

(Cj. -C)ICS x 100 (must be < 2%) Calibration Drift (SBf -SBi) (must be <3%) (SB)’(C -Cdjr)/CS * 100 (must be< 5%)
C) C) j’.) C) i—i C) P.) N) P.) P1 0 (0 (0 _i 0) o _i C) C) — 0 U) (0 - C) C) .P. C) N) - 0

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rFFFFFFFFFFFFFFFFFFFFFFFFFFF:
SOURCE NAME

-7A /

SOURCE ID NUMBER

ce_ PROC ESS EQUIPMENT OPERATING MODE

(1[ ill uL- L. •(

CONTROL EQUIPMENT OPERATING MODE

DESCRIBE EMISSION POINT

START STOP

HT ABOVE GRd&D LEVEL HT RELATIVE TO OBSERVER

STARTLSr STOP START STOP

D)STANCE FROM OBSERVER DIRECTION FROM OBSERVER

START’ STOP 3çr START At’ STOP tJ. DESCRIB EMISSIONS

START STOP

EMISSION COLOR PLUME TYPE: CONTINUOUSO

STARTUSTOP eLtI— FUGITIVED INTERMITTENTD

WATER DROPLETS PRESENT: IF WATER DROPLET PLUME:

NO - YES D ATTACHED D DETACHEDD

POINT IN THE PLUME AT WHICH OPACITY WAS DETERMINED

START STOP

DESCRIBE BACKGRO1JND

START’? )ôxL STOP 5.C

BACKGROUN SKY CONDITIONS

STARTS START? Ck’TOP

IIND SPEED WIND DIRECTION

TART71.i STOP 71 2— STARTJL STOP

\MBIENT TEMP WET BULB TEMP RH %

TART STOP 9 (L,

Source Layout Sketch Draw Nrrow

Emission Poiht X

Un

ind —

lume.

tack Sun Locat;Une*

SOURCE NAME

SOURCE ID NUMBER

PROCESS EQUIPMENT OPERATING MODE

CONTROL EQUIPMENT OPERATING MODE

DESCRIBE EMISSION POINT

START STOP

HT ABOVE GROUND LEVEL HT RELATIVE TO OBSERVER

START STOP START STOP

DISTANCE FROM OBSERVER DIRECTION FROM OBSERVER

START STOP START STOP

DESCRIBE EMISSIONS

START STOP

EMISSION COLOR PLUME TYPE: CONTINUOUSD

START STOP FUGITIVE Q INTERMITTENID

WATER DROPLETS PRESENT: IF WATER DROPLET PLUME:

NO D YES D ATTACHED D DETACHEDD

SOURCE NAME

SOURCE ID NUMBER

PROCESS EQUIPMENT OPERATING MODE

CONTROL EQUIPMENT OPERATING MODE

DESCRIBE EMISSION POINT

START STOP

HT ABOVE GROUND LEVEL HT RELATIVE TO OBSERVER

START STOP START STOP

DISTANCE FROM OBSERVER DIRECTION FROM OBSERVER

START STOP START STOP

DESCRIBE EMISSIONS

START STOP

EMISSION COLOR PLUME TYPE; CONTINUOUSD

START STOP FUGITIVED INTERMITIENTO

WATER DROPLETS PRESENT: IF WATER DROPLET PLUME.

POINT IN THE PLUME AT WHICH OPACITY WAS

NO D YES C ATTACHED C DETACHEDD

DETERMINED

START STOP

POINT IN THE PLUME AT WHICH OPACITY WAS DETERMINED

START

DESCRIBE BACKGROUND

STOP

START STOP

BACKGROUND COLOR SKY CONDITIONS

START STOP START STOP

WIND SPEED WIND DIRECTION

START STOP START STOP

AMBIENT TEMP WET BULB TEMP RH %

START STOP

Source Layout Sketch Draw North Arrow

Emission Point X 0

DESCRIBE BACKGROUND

START STOP

BACKGROUND COLOR SKY CONDITIONS

START STOP START. STOP

WIND SPEED WIND DIRECTION

START STOP START STOP

AMBIENTTEMP WET BULB TEMP RH %

START STOP

Source Layout Sketch Draw North Arrow

Emission Point X 0

Sun

Wind

Plume .

Stack Sun Locator Line

3SERVERS..NAME (PRINT)

///

ORGANIZATION

I .4;

DTE

y CERTIIEQY

-;/kf(1 1/I

Sun

Wind

Plume

Stack Sun Locator Line

ADDRESS

4-(CiAJ i4ep.5.• ,

C’3 t c’-O

Moj. , LA -7Iac7a
APPEND B

CALIBRATION DATA
Expected Analyzer Calibration

Concentration Anlyzer Outvut Error Gas Concentration (ppm) High .. (ppm) ‘‘ ..(%) /b 246.7 251.1 Mid 1.78

98.7 96.3 -0.99 Low

0.00 0.10 004

Instrument: Fuji ZRF -CO

Span: 1017 Response to Calibration Gas (ppm) Expected Analyzer Calibration Concentration Anlyzer Output Ertor Gas Concentration (jipm) (ppm) High (7.) 1017.0 1014.5 Mid -0.25

610.2 604.5 -0.56 Low

0.00 0,42 0.04

Instrument: Fuji ZRF -CO2

Span: 13.5 Response to Calibration Gas (ppm) Expected Analyzer Calibration Concentration Anlyzer Output Error Gas Concentration (ppm) (ppm (%) High

Mid

13.5 13.5 0.15

8.10 8,00 -0.74 Low 0.00 0,00 0,00

Instrument: Fuji ZRF -02

Span: 20.99 Response to Calibration Gas (ppm)

Expected Analyzer Calibration Concentration Anlyzer Output Error Gas Concentration (ppm) (ppm) (%) High

Mid

20.99 20.98 -0.05

8.40 8.28 -0.57 Low 0.00 0.01 0.05
Zero System Bias

Averatte Un-Scale Calibrations

NOx CO C02 02 Eng. 4 Test 1 99.1 601 13.34 829 Eng. 4 Test 2 99.9 601 13.37 8.30 Eng. 4 Test 3 100.1 604 13.48 8.28 Eng. 4 Test 4 13.57 8.28 Eng. 4 TestS I 3.57 8.29 Eng. 4 Test 6 13.57 8.30

Average Zeros

NOx CO C02 02 Eng. 4 Test! 0.66 0.24 0.00 0.01 Eng. 4 Test 2 1.00 0.28 0.00 0.01 Eng. 4 Test 3 0.77 1.26 0.00 0.01 F.ng. 4 Test 4 0.02 0.01 Eng. 4 TestS 0.07 0.01 Eng. 4 Test 6 0.10 0.01

Un-Scale Gas SYstem Bias Drift Drift Expected Cone. (ppm NO,) 96.3 ‘(%) ‘ (%) 0.10 (%) (%) Engine 4, Pre Test I 98.8 1.02 - 0.15 0.02 - Engine 4, Post Test 1/Pre Test 2 99.4 1.29 0.27 1,16 0.43 0.41 Engine 4, Post Test 2/Pre Test 3 100.4 1.69 0.40 0.83 0.30 0.13 Engine 4, Post Test 3 99.8 1.44 0.25 0.71 0.25 0.05

Instrument: Fuji ZRF -CO

Span: 1017 Response to Calibration Gas (ppm)

Up-Scale Gas System Bias Drift Zero System Bias Drift Expected Cone (ppm CO) 604 5 “ (/)

1I1fPS (%)$ “ 042 .. (°/) (%) Engine 4, Pre Test I 602.9 -0.16 - 0.34 -0.01 - Engine 4, Post Test 1/Pre Test 2 599.5 -0.50 0.34 0,13 .0.03 0.02 Engine 4, Post Test 2/Pre Test 3 601.7 -0,28 0.22 0.42 0.00 0.03 Engine4,PostTest3 605.5 0.tO 0.37 2.10 0.17 0.17

Instrument: Fuji ZRF -CO2

Span: 13,5 Response to Calibration Gas (ppm)

Up-Scale Gas System Bias Drift Zero System Bias Dnft Eqsected Cone. (ppm CO,) 13.52 (%) ‘ (%)< “‘v 000 (%) (%) Engine 4, Pre Test! t3.34 -1.33 - 0.00 0.00 - Eisgine 4, Post ‘rest l.Pre Test 2 13.33 -141 0.07 0.00 0.00 0.00 Engine 4, Post Test 2/Pre Test 3 13.40 -0.89 0.52 0.00 0.00 0.00 Enmine 4, Post Test 3/Pre Test 4 1 3.56 0.30 1 .19 0.00 0.00 0.00 Engine 4, Post Test 4/Pre ‘rests 13.57 0.37 0.07 0.04 0.30 0.30 Engine 4, Post Test 5/Pre Test 6 13.56 0.30 0.07 Entiine4, 0.10 0.74 0.44 Post Test 6 13.57 0.37 0.07 0.09 0.67 0.07

Instrument: Fuji iRE - 02

Span: 21.0 Response to Calibration Gas (ppm)

Up-Scale Gas System Bias Drift Expected Conc (ppm O) 828 Zero System Bias Drift f4W4dW(%) (‘) ‘W4s’ 44 001 (%) (‘7) Engine 4, Pie Test 1 8.28 0.00 - 0.01 0.00 - Engine 4, PostTest 1/PreTest2 8.30 0.10 0.10 0.01 0.00 0.00 Engine 4, Post Test 2/Pre Test 3 8.29 0.05 0.05 0.01 0.00 0.00 Engine 4, Post Test 3/Pre Test 4 8.27 -0.05 0.10 0.01 0,00 0.00 Engine4,PostTest4/PreTest5 8.29 0.05 0.10 0.01 0.00 0.00 Engine 4, Post Test 5/Pie Test 6 &28 0,00 0.05 0.01 0.00 0.00 Engine 4, Post Test 6 8.32 0.19 0.19 0.01 0.00 0.00
Run

No.

1

2

3

250

350

VOC Reference Method Analyzer Sampling System Bias Check arid Measured Value Correction

VOC RM Monitor Span 1000.00 PPM

800

900

Zero

Gas

Drift

0.00%

0.00%0.00%

Z-DriftPass if

<3%

Pass

PassPass

Average Up-Scale Calibrations THC

Eng.4Testl 521.40

Eng.4Test2 527.86Eng.4Test3 531.40

Average Zeros THC

Eng.4Testl 0.1

Eng.4Test2 0.1

Eng.4Test3 0.1

450

Calibration 550 Error Check

Linearity Check (Must be within 5%)

Cal. Gas

Serial #

Tag Value

Monitor

Expected

Monitor

Duff.

% Duff

Zero Low Mid High Gas Gas Gas Gas

Propane Propane Propane

:, 0.00 348.00I 522.00 870.00 0.08

. 871.99-

348.84

. 523.23*

•. 338.19 .: 514.55

0.08 -10.65 -8.68 1.99 0.0 1% -3.06% -1.66% 0.23% Pass Pass Pass Pass

(Cavg) (Co)i (Co)f Ave. Measured Initial Zero Gas Final Zero Gas

Raw (ppm)

L 560.21 0.08 0.08

641.74 0.08 0.08

. 623.29 0.08

.

. 0.08

(Crn)i

Initial

Run Upscale

No.

1

2

3

(Cm)f

Final

Upscale

514.55 528 25

528.25 527.46

527.46 535 34

Upscale

Gas

Drift

1.37%

-0.08%

0.79%

Up-Drift

Pass if

<3%

Pass

Pass

Pass
VOC Reference Method Analyzer Sampling System Bias Check and Measured Value Correction

Span Span Span 250 450 800

Calibration Error Check 350 550 900

Linearity Check (Must be within 5%)

Cal. Gas

Serial

#

Tag Value

Monitor

Expected

Monitor

Diff.

% Duff

Zero Low Mid High Gas Gas Gas Gas

Propane Propane Propane

0.00 752.80 1 1129.20 I 1882.00 0.76 1882.28

753.37 1129.7. I 749.73 1142.6II

-3.64 12.9

Pass

. -0.48%

Pass

1.15o6iaio 0

Pass Pass

VOC RM Monitor Span = 1000.00 PPM

(Cavg)

Ave. Measured

Raw (ppm)

(Co)i (Co)f Zero

Initial Zero Final Zero Gas Gas

Drift

Run

No.

I

2

3

Run

No.

I

2

3

1919.99drnI 0.76 2.80

J1.54

1.77

Z-Druft

Pass if

<3%

Pass

Pass

Pass

(Cm)i

Initial

Upscale

(Cm)f

Final

Upscale

0.20%

-0.13%

0.02%

Up-Drift

Pass if

<3%

Pass

Pass

Pass

k1142.62 1118.51

%1118.51: 1101.46

1094.24

Upscale

Gas

Drift

-2.4 1%

-1.71%

-0.72%
ent: Themo Environmental Instruments, Inc., Model 42c - NO, Span: 246.7 Response to Calibration Gas (ppm)

Expected Pre Stratification Analyzer Calibration Concentration Testing Error Gas .(ppm) (ppm) ‘..5(%) High 246.7 248.7 Mid 0.82 98.7 97.9 -0.33 Low 0.00 0.30 0.12

Instrument: Fuji ZRF -CO

Span: 1017 Response to Calibration Gas (ppm)

Expected Pre Stratification Analyzer Calibration Concentration Testin, Error Gas Concentratonsf (ppm) (ppm ( /) High

Mid

1017.0 1015.3 -0.17

610.2 609.7 -0.05 Low 0.00 005 0.00

Instrument: Fuji ZRF -CO2

Span: 13.5 Response to Calibration Gas (ppm)

Expected Pre Stratification Analyzer Calibration Concentration Testing Error Gas Concentration (ppm) (ppm) (%) High

Mid

13.5 13.5 0.07

8.10 8.11 0.07 Low 0.00 0.00 0.00

Instrument: Fuji ZRF - 0,

Span: 20.99 Response to Calibration Gas (ppm)

Expected Pre Stratification Analyzer Calibration Concentration Testing Error Gas Concentrahon (ppm) (ppm) (%) High

Mid

20.99 21.0 0.14

8.40 8.22 -0.86 Low 0.00 0.01 0.05
Environmental Instruments, Inc., Model 42c - NO, Span: 246.7 Response to Calibration Gas (ppm)

ExpectedConc.(ppmNOJ. Up-Scale 97.9 Gas System Bias Drift Zero System Bias Drift (%) Pre Stratification Test 030 (%) 97.9 0.03 - 0.30 0.00 - Post Stratification Test 49.6 0.11 0.08 0.09 -0.09 0.09 System Response Time (see) 114 - - 107 - -

Instrument: Fuji ZRF - COSpan: 1017 Response to Calibration Gas (ppm) Up-Scale Gas System Bias Drift Zero System Bias Drift [xpeeted Cone (ppm CO) 609 ( /o) 005 (%) ( /) Pre Stratification Test 606.1 -0.36 - 1.77 0.17 - Post Stratification Test 606.2 -0.34 0.01 1.78 0.17 0.00 System Response Time (see) 95 - - 106 - -

Instrument: Fuji ZRF -CO2

Span: 13.5 Response to Calibration Gas (ppm)

System Bias Drift Zero System Bias Drift

F xpcctcd Coiic (ppm CO,) 13 (%) (%) 000 (°‘) (%) Pre Stratification Test 13.52 0.07 - 0.03 0.22 - Post Stratification Test 13.46 -0.37 0.44 0.02 0.15 0.07 System Response Time (see) 110 - - 104 - -

Instrument: Fuji ZRF -O

Span: 21.0 Response to Calibration Gas (ppm)

Expected Cone (ppm O) Up-Scale 822 Gas System Bias Drift Zero System Bias Drift ,- s 5 (%) 001 (%) (%) Pre Stratification Test 8.27 0.24 - 0.01 0.00 - Post Stratification Test 8.29 0.33 0.10 System Response Time (see) 113 0.01 0.00 0.00

- - 133 - -
Derenzo and Associates, Inc.

Divider Expected Injection

Setting Concentration No. 1 No. 2 No. 3 Average %Error

100% 20.99 21.03 21.05 21.03 21.04 0.22%

60% 12.59 12.44 12.43 12.40 12.42 -1.36%

40% 8.40 8.24 8.26 8.23 8.24 -1.82%

0% 0.00 0.01 0.01 0.01 0.01 -

Introduce mid-level protocol gas (instrument). Repeat twice (total of 3 injections).

Mid-Range Expected Injection

Gas Concentration No. 1 No. 2 No. 3 Average %Error

°2 12.50 12.59 12.63 12.67 12.63 1.04%

1. Each injection shall differ no more than 2% from the triplicate average.

2. No average shall be greater than 2% ofthe predicted value.

Date:

Client:

dilution

module at

Gas used:

METHOD 205 -DILUTION MODULE VERIFICATION

3/24/2009

Trail Ridge Energy

20.99 %, oxygen calibration gas

Individual Response Errors

as Compared to Average

0.0% 0.1% 0.0%

0.1% 0.1% -0.2%

0.0% 0.2% -0.2%

Criteria:

Individual Response Errors

as Compared to Average

-0.3% 0.0% 0.3%
Derenzo and Associates, Inc.

METHOD 7E - NOx CONVERTER VERIFICATION

Date: 3/25/2009

Client: Trail Ridge Energy

Pre Test Analyzer Calibration Introduce high, mid, low calibration gases (must be within 2% of

calibration span).

Expected Observed Percent

Gas Time Concentration (ppmv) Concentration (ppmv) Error

High 6:43 247 251.1 1.65

Mid 6:47 97 96.25 -0.17

Low 6:25 0.00 0.10 0.04

Conveter Test Introduce approximate 1:1 mix of NOx calibration gas and zero air. NOx reading must remain

stable (cannot drop more than 2% of highest peak observed) for 30 minutes.

Beginning Beginning Ending Ending Elapsed

Pollutant Time Concentration (ppmv) Time Concentration (ppmv) Time %Change

NO 13:49 50.86 14:19 50.13 0:30 -1.44%

NO2

NO 13:49 50.69 14:19 45.9 0:30 -

13:49 0.41 14:19 4.29 0:30 -

Post Test Analyzer Calibration Introduce a calibration gas that most closely matches the concentration observed

during the test (must be within 1% of calibration span).

Expected Observed Percent

Gas Time Concentration (ppmv) Concentration (ppmv) Error

Mid 15:47 49.3 49.60 0.11

Zero 15:28 0.00 0.09 0.04
Derenzo and Associates, Inc.

Measure three points located at 16.7%, 50.0% and 83.3% of stack diameter for twice the system response time. Determine

the pecent difference of the response at each point compared the the three point average.

Engine No. 3 Recorded Recorded Concentrations (ppm)

Point Time CO CO2 02

1 16:39 658 10.96 8.28

2 16:48 659 10.94 8.29

3 16:57 659 11.01 8.28

Average - 658 10.97 8.28

Criteria:

1. If the response differs no more than 5% from the three point average, measure at one point.

2. If the response differs more than 5% but no more than 10% from the three point average, measure at three points.

3. If the response differs more than 10% from the three point average, measure at twelve points.

Date:

Client:

METHOD 7E - STACK STRATIFICATION DETERMINATION

3/24/2009

Trail Ridge Energy

Response as Compared to Average

CO CO2 02

0.0% -0.1% 0.0%

0.0% -0.3% 0.1%

0.0% 0.4% 0.0%
B

A:

B:

C:

Average:

/t)

/c’

F//a

Comments: S//
A:

B: B

C:

Average:

C

Comments:
B

A:

B:

C:

Average: /;__

Comments:
w z

31. z1.9cm Z

w7.62 cm

Or

32. Z 5.O8 cm

. Y7.62cm

Figure Bi Figure B2 or

No

B2.Yes No

Y

Figure C

No

Pitot Tube Correction Factor:
1 .05D A,B 1.5D

Longitudinal

Tube Axis

PB

No

No

No

z < 0.32 cm No

w < 0.08 cm

Transversal

Tube Axis

U.’ L

and a2 < 100

and 12 < 50

No

J31

12

Hz

No

Pitot Tube Correction Factor:
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

2>

1)

Record

Select three

barometric

critical orifices to calibrate the dry gas meter which bracket the expected operating range.

pressure before and after calibration procedure.

3) Run at maximum attainable vacuum (open coarse valve, close fine valve),

4) Record

tar period of 5 minutes minimum for large orifice up to 10 minutes for smatlest orifice.

readings in outlined bones below, other Columns are automatically calculated.

DERENZO & ASSOCIATES, INC

TEMPERATURES F

r INITIAL

0GM READINGS

FINAL

(FT’) AMBIENT 0GM INLET 0GM OUTLET 0GM TIME (MIN)

NET (V,> INITIAL FINAL INITIAL — FINAL - - AVG

1429 1 O.708 16.5 760.120 765,26 5.140

Crass 2 0.7968 16.5 765.26 770.4.4 5.180

3 0.7960 16.5 770.44 775.625 5.109

02$ I 0.6534 10 775.620 7e4.17 8.541

Crass 2 5.6534 16 7e4.17 792.76 8.590

3 O.e534 18 792.76 809.355 e.oao

520 1 0.5333 19.5 801.350 ao9.32 6.970

0rs 2 0.5333 19.5 eoe.32 015.28 6.960

3 0.5333 19.5 895.28 e22,2s6 6,976

LSIND THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:

films 1n2...’.;ng nqua2onx are usud to calculate the standard volumos of air passed through lire 0GM, 14, (old), and the arilical orifice, 14/,, (old), and the

DCV vu uratJnn taclur, Y. These equations are axIomatically nalculaled irs lIre spreadsheet abous.

(31 Y = ‘4, (old) = 0GM calibration factor

V01 (slid)

76 76 65 69

:L_

L2

Net volume of gas sample passed through DGI,I, corrected to standard condilians

K, 17.64 ‘K/in. Hg (English), S.3050’l(lmm Hg )Mvtric)

= Absolute 0GM avg. temperalure (‘K. English,’K- l.lelnc)

= Volume of gas sample passed through the critical orifice, corrected to slarudard condiIios

= Absolute ambient temperature (‘Fl -English, ‘K .Melds)

K’ = Average K’ laclur from Critical Orihce Calibralmon

67

67

67

67

67

67

67

67

67

77

77

76

77

76

77

70

71

71

71

79

72

IF Y VARIATION EXCEEDS 2.00%,

ORIFICE SHOULD BE RECALIBRATED

DATE: 3/6/09 METER SERIALS: NT

1.IETER PART 14: NI CRITICAL ORIFICE SET SERIALS: 1316

ORIFICE 0 RUN 0

K’

FACTOR

(AVG)

TESTED

VACUUM

(In HO)

INITIAL

BAROMETRIC PRESSURE (In Hg)L_2aj5

AVG (P5.,)

29.15

FINAL

29.15

ELAPSED

72,20

72.5

73

DGM&-I (1) (2) (3) Y

(in H5O) V,,,)STD( V, (STO( I VARIATION l’l

5.00 3.9

0.00 3.5

L 5.00 3.8

73.75 10.05 2.5

73.75 10.00 2.5

74 10.00 2.5

74 10.00 1.7

74 10.00 1.7

74 10.00 1.7

(1) V,,, (std)o

i2 V, 1 (std)

K1 V,,, P5•, + (AH!13.6(

1’,,

________________

5.0163 5,0603 1,0088

5,0529 5.0603 1,0015

5,0570 5.0663 1,6007

AVG = 1,0036 0.15

________________

8.2850 8.2993 1,0017

5,3325 8.2993 0.9960

8.3286 8.2993 0.9065

AVG 0,9589 -0.40

_________________

6,7443 6.7738 1,004.4

________________

6.7347 6.7730 1,0050

6.7501 6,7739 1.0035

AVG 1,0046 0.20

AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 1.0021

Y-S% 0,952 1,052

Delta H@ 2.026

K/so 1623.534

PYROMETER CALIBRATION

Meter 32 100 252 500 1500

Ome9a

1500

32 150 255 550 1009

‘I. DIfference 0.0

1500

0.5 0.0 0.0 0.5 5,0

I’tulech #1 Calibration
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

2)

1)

Record

Select three

barometric

critical orittces to calibrate the dry gas meter wtrich bracket the expected operating range.

pressure before arid after cahbration procedure.

3) Run at maximum attainable vacuum (open coarse valve, close fine valve>.

for period of 5 mInutes minimum for large orifice upto 10 minutes for smallest orifice.

4) Record readings ml outlined boxes below, other columns are automatically calculated.

DERENZO & ASSOCIATES, INC

731.649 738.57

738.57 745.52

745.52 752.478

5.160

5.220

5.219

8.601

8.650

8.611

6.521

6.550

6.958

TEMPERATURES’F

65 74 75 69 70

_

Net volume of gas sample passed through DGM, corrected to standard conditions

K 17.04 ‘Rim. Hg (English), 0.3058 ‘K/mm Hg )f.lelnc)

1’,. = Absolute 0GM avg. temperature R- Engimsh,’lc- Metric)

= Volume of gas sample passed through the critical orifice, corrected to standard Conditions

= Absolute ambient temperature )R - English. ‘K - f.letmic)

K’ Average K’ factor 1mm CritIcal Orifice Calibration

66

67

68

75

76

76

76

76

76

70

71

71

71

71

72

IF V VARIATION EXCEEDS 2.00%,

ORIFICE SHOULD BE RECALIBRATED

5.0448 5.0569 1.0024

5.6790 5.0569 0.9957

5.0756 5.0569 0.9563

AVG 0.9551 -0.09

8.3335 8.2858 0.9943

8.3732 8.2779 0.5806

8,3315 o.27sI 0,9926

AVG = 0.9918

6.6798 6.750 1.0105

6,7109 6.750 1.0058

6.7218 6.7564 1.0051

AVG 1.0072

DATE: 411105 METER SERIAL 6: Ni

1.IETER PART 6: Ni CRITICAL ORIFICE SET SERIAL 6: 1316

ORIFiCE II RUN S

K’

FACTOR

(AVG)

TESTED

VACUUM

(In tl)

INITIAL FINAL AVG (Pu.,)

8AROMETRIC PRESSURE (in Hg(: 20.08 I 29.07 29.075

INITIAL

0GM READINGS (PT’) AMBIENT 0GM INLET 0GM OUTLET 0GM TIME (fAIN)

FINAL NET (V,,) INITIAL FINAL INITIAL FINAL AVG 0

689,170 694.30

694.35 699.57

699.57 704.789

020 1 0.7968 16.5

Oruss 2 0.7968 16.5

16,5

024 1 0.6534 16

OrasS 2 0.6534 18

3 8.6534 18

1120 1 0.5333 19.5

Orass 2 0.5333 19,5

3 19,5

ELAPSED

L 704.789 713.39

713.39 722,04

722.84 730.651

DGM4H (I) (2) (3) V

(In H,D) V, )5TD( V,, )STD( V VARIATION (%l

SiNG THE CRITICAL OOIFICES AS CALIBRATION STANDARDS:

lila lois ...g nquaLuos are used tu calculale the otandard volumes of air passed thraugh the 0GM, V. (std), and the cribcal wince, V (std), and the

)Gl,l cu.bratioo boor, V. Thrse equations are automatically calculated in the spreadsheet abnoe.

72 5.00 3.8

72.5 5.00 3.8

72.75 5.00 3.8

73 10.50 2.5

73.5 10.00 2.5

73.75 10.00 2.5

74 10,00 1.7

73.75 10.00 1.7

73.0 10.00 1.7

>1) V,, (stct) = K5 V,, Pb., + (0H113.6)

T, 5

12) V,, )std) u K’

131 Y = 1,, (sOd)

V,, (sOd)

= 0GM Calibration factor

072

o.an

AVERAGE DRY GAS METER CALIBRATION FACTOR, y = 0,9990

Y-5% 0.949 1,049

Detta H@ 2.031

KIso 1534.575

PYROMETER CALIBRATION

Meter 32 99 I 252 500 1000

Omega

1501

32 100 250

1% Difference 0.0

500 1000 lOOT

.1.0 0.8 0.0 0.0 0.1

Nutocli 1111 Calibration
Customer Address:

& Associates Inc

39395 Schoolcraft Rd

Livonia

734-464-3880

Ml 48150

LAN-I 81

0902SC08

Al 6

Purchase Order:

Lot Number:

Size:

Content:

Serial #:

Analysis Date:

Shelf Life:

NIA

Work Order:

Product Name:

Pressure:

ET000205 0

9/18/2008

36 monThs

080466-03

2-Component Mixture, EPA Protocol

2300 pslg @ 89 Deg F

Expiration Date: 9/1812011 Component

Methane

Nominal Actual Accuracy Method

Air Balance 1850 ppm 1882 ppm +/-2% rel FID Balance

REFERENCE STANDARD Std Type Std# Concentration Exp Date GMIS 0327AB08 EB0001183 104.1000 3/27/2010

4:

INSTRUMENTATION Instrument I ID

CAl 300S-HFID

CH4 I

Note: *

OF

ANALYZED

GASEOUS

ACCORDING

CALIBRATION

TO

STANDARDSEPA TRACEABILITY PROTOCOL FOR ASSAY AND CERTIFICATION DO NOT USE SEPTEMBER 1997:01 STANDARD WHEN PRESSURE IS BELOW 150 PSIG

r H -4

Issued by: GJI, 9c’n.e&

pecialty Gases of America, Inc. QFO5I, Rev 0
Derenzo & Associates Inc

Customer Address: 39395 Schoo!craft Rd

e

-

.

Livonia Ml 48150 734-464-3880

Purchase Order: LAN-175

Lot Number: . Work Order; 076935-01 0304HF08 Product Name: 2-Component Mixture, EPA Protocol :4

-.

Size: 31A Pressure: Content: 2000 psig @ 70 Deg F NFA

V Serial#: SX28217

Analysis Date: 3/14/2008

Slielf Life: 36 months Expiration Date: 3J1 412011 _4 Component Nominal . Actual

,. Accuracy Method .21 0% 20.a% +J- 1% reL — Paramagneitc

._

Nitrogen Balance Balance

•1

REFERENCE STANDARD Std Type

GMIS Concentration Exp Date 1206BN05 EB0001234 V. 2156% 10/2/2009

I

V.

I INSTRUMENTATION InstrumentIlD Component Rosemount 755R

02

. •••

. ..

. •V•V

-

.•• •

- -t.4t

.•-.‘-V.

4.

.

Note: * ANALYZED ACCORDING TO EPA TRACEABILIT’? OFGASEOUS CALIBRATION STANDARDS PRO1 .LFDR ASSAVAND CERTFIAT1ON - SEPTEMBER 1997G1 * DO NOT USEVSTANDARD WHEN PRESSURE IS ELd’Vv: ió-P’sid

.

Issued by &nz

ciaIt Gases of Atnerlca 3Inc. QFO5I Rev 0
95 Schoolcraft Rd

Livonia MI 48150

Purchase Order: LAN-171 Work Order: 074669-00 Lot Number: 0410HA08 Product Name: 2-Component Mixture, EPA Protocol I.I4 Size: 31A Pressure: 2015 psig @ 70 Deg F Content: N/A

Serial #: EB0006707

Analysis Date: 4/14/2008

4 Shelf Life: 36 months Expiration Date: 4/14/2008

Component Nominal Actual Accuracy Method Carbon Dioxide

Nitrogen

13.5% 13.5% +1- 1% rel NDIR Balance Balance

REFERENCE STANDARD Std ii Type Std Concentration Exp Date GMIS 0306JD08 EB0000776 -I 7.5230 316/2010

INSTRUMENTATION Instrument I ID

Component on a

- 002

Note: *

OF

ANALYZED

GASEOUS

ACCORDING

CALIBRATION

TO EPA TRACEABILITY PROTOCOL FOR ASSAY AND CERTIFICATION

* DO STANDARDS - SEPTEMBER 1997:G1 NOT USE STANDARD WHEN PRESSURE IS BELOW 150 PSIG

Issued by:

y’ W

Specialty Gases of America, Inc. 0F051, Re’i 0
z u>cnocnr--

0 Ct 0 F 0 

—

?tIO 2. . • C •

rn “‘< —cD’

* * 3 CD CD 

C-n> C m CDQ 

OQZ

m 9:, z> z — 

p 0 -<

C”

:i 

z

C

ZJ

oioz

o ID C — 

m g C1’L

Z I

0

Icj —

mm C

0 > Q

CI)c) -

c rn 0 — 0) CD

m

—

-

-—J r- CD

C/,Q-nl

C) •

I

b — 0 a’ CD C) Cni 0 CD

ID _ 

— — 

C) 
Customer Name: Derenzo & Associates

Customer Address: 39395 Schoolcraft Fd -

-

Livonia MI •. :. 48150 j

Purchase Order: 0924 Work Order: 055955-02

Lot Number: I1O1SCO6 . Product Name: 4-Component Mixture, EPA Protocol

Size: 31A Iressure: 2250 psig @ 90 Deg F

Content: NA

4 Serial #: EB0004361 - -

Analysis Date: 11/18/2006

Shelf Life: 36 months Expiration Date: 11/18/2009

Component Nominal Actual Accuracy Method

15% .. -. 15.0%

. +/-Qi% GC-TCD -

l000ppm lOl6ppm +/-3ppm NDIR

12.5% 12.5% +1- 0.2% Paramagnetic

Balance Balance

Std Type Std# Concentration Exp Date

GMIS IO11BKO5 EB0000880 1000 ppm 1)20/2008

GMIS 1206BL05 EB0001508 15.16% 1/31/2008

GMIS 1O11SHO5 EB0000776 7.53% 2)3/2008

Instrument! ID Component

Horiba VA-3000 co

Rosemount 755R 02

GOWMAC-580 TCD C02

Note: *ANALYZEDACCORDGTOEPRACEALYOO ASSAY AND CERTIFICATION

DO NOT USE STANDARD WHEN PRESSURE IS BELOW 150 PSIG

Issued by: 9-n&

Carbon Dioxide

Carbon Monoxide

Oxygen

NitrogenREFERENCE STANDARD

INSTRUMENTATION

4

1

4
Customer Address: 39395 SchooIcraft Rd

Livonia Ml 48150

734-464-3880

b ‘1 Purchase Order: LAN-161 Work Order: 069795-00 Lot Number: 1128SA07 Product Name: 2-Component Mixture, EPA Protocol Size: 31A Pressure: 2200 psig @ 80 Deg F Content: NA

II4 Serial#: CC181509

‘4 Analysis Date: 12/11/2007

. Shelf Life: 36 months Expiration Date: 12/11)2010

Component Nominal Actual Accuracy Method Carbon Monoxide

Nitrogen

1000 ppm 1017 ppm +1- 1% rel NDIR BaIac Balane

--.--_.-.

--..

..

.IL4

REIERENCE STANDARD Std Type Concentration Exp Date 4 GMIS 1012BC05 EB0000962 2514 ppm 1/20)2008

INSTRUMENTATION Instrument/ID Component Horiba VA-3000 CO ‘1 P

Note: *

OF

ANALYZED

GASEOUS

ACCORDING TO EPA TRACEABILITY PROTOCOL FOR ASSAY AND CERTIFICATION

*

CALIBRATION STANDARDS - SEPTEMBER 1997:G1 DO NOT USE STANDARD WHEN PRESSURE IS BELOW 150 PSIG

Issued by: j2cJi, C4l,QA,

Specialty Gases of America, Inc. QFO51, Rev 0
AIR ENGINEERING SCOTT SPECIALTY GASES Project No.: 05-65079-003 DON ALLEN 1290 COMBERMERE STREET 500 W. WOOD STREET TROY, MI 48083 PALATINE IL 60067

ANALYTICAL INFORMATION

ThisProcedure

certification

G-1;

was performed according to EPA Traceability Protocol For Assay & Certification of Gaseous Calibration Standards; September, 1997.

Cylinder

Cylinder Number:

Pressure***:

ALM008541 Certification Date: 06May2008 Exp. Date: O6May2OlO 1983 PSIG

COMPONENT

NITRIC OXIDE

NITROGEN - OXYGEN FREE

TOTAL OXIDES OF NITROGEN 246.7 PPM Reference Value Only

Do not use when cylinder pressure is below 150 psig.

R=Reterence Gas T=Test Gas

Second Triad Analysis

= Correlation Coefficient)

Calibration Curve

NITRIC OXIDE

APPROVED BY:

CERTIFIED CONCENTRATION (Moles)

246.7 PPM

BALANCE

ANALYTICAL

ACCURACY* *

+1- 1%

TRACEABILITY

Direct NIST and NMi

“ Analytical accuracy is based on the requirements of EPA Protocol Procedure Ri, September 1997. REFERENCE STANDARD

TYPEISRM NO. EXPIRATION DATE CYLINDER NUMBER CONCENTRATION COMPONENT NIRM 1685 OiSop2OlO KAL003527 247.1 PPM NITRIC OXIDE

INSTRUMENTATION

INSTRUMENT!M ODEL/SERIA L# DATE LAST CALIBRATED ANALYTICAL PRINCIPLE FTIR//0928621 24Apr2008 FTIR

ANALYZER READINGS

first Triad AnalysIs

(Z=Zero Gas

Oate: 28Apr2006 Response Untt:PPM

11 -.0.31274 R1Z46.9272 T1—246.7670

R2= 246.9446 Z2-O.1389B T2. 246.7452

Z3 O.31568 T3 ..247.2013 H3247.874O

AS,g. concentration: 246.4 PPM

DOte: O6May200B Response Unit: PPM

Z1—-O.64681 R1245,4a17 Ti =244.9912

R2= 245.5777 22= .0.32221 T2= 245.0868

23 --0.24644 T3 =245.3372 R3 = 246.6467

Asg. Concentration: 246.9 PPM

Concentration=A+Bs + 0e2 + De3+6x4

r= 9.99999E.1Constants: A=0.00000E+06=9.825760-1 C4.60O00E-5

o=O.000000+0 E=0.000000+0

Rob McCrandall

fl... I .4 I
Certificate Number: 2011197-1 23008

All instruments

to the National

in the performance of the below calibration have direct traceability

has been performed

Institute of Standards and Technology (NIST). The calibration using the below listed procedure number.

Customer:

Customer Address:

Manufacturer: STEC

Description: Gas Divider

Condition Received: Passed Cal Procedure: BPP.-QM1001-012 Date Calibrated: 12/30/08

Part Number: SGD-SC-5L

Serial Number: 2011197

Condition Returned: Passed

Uncertainty: +1- 2% point Recalibration Due: 12/30/09

Standards Traceability

Service Technician: A4I ji___

QAManager:__________________________

ThisF1QM1001015

certificate/report may not be reproduced, except in full, without the written approval of Horiba

Issue Date: 3/27/01 Page 1

Derenzo & Associates, Inc 39395 Schoolcraft Rd

Livonia, MI 48150-5036

DHI/3E5

Mfr./Model Number Serial # Test Number Cal. Date Due Date 1015 59148 DHI/3E5 02/29/08 02/28/09 1016 59149 DHI/Molbox 02/29/08 02/28/09 IA 448 59147 02/29/08 02/28/09

Revision Date: N/A

Date: 12/30/08

Date: 12/30/08

Revision Level: A

ri -‘ 4’
042 4.0042 0.000 0.000 20 0.8031 3.2292 4.0323 19.917 0.416 40 1.6104 2.4273 4.0377 39.883 0.292 60 2.4176 1.6250 4.0426 59.803 0.330 80 3.2279 0.81 00 4.0379 79.940 0.075 100 4.0397 0.0000 4.0397 100.000 0.000

STD. DEV. 0.0142 LPM

MIXTURE GAS INLET PRESSURE TO DIVIDER:

DILUTION GAS INLET PRESSURE TO DIVIDER:

21.0 PSIG

(At 100% CUTPOINT)

17.0 PSIG

(AT 0.0% CUTPOINT)

OUTLET FLOW FROM GAS DIVIDER: 4.00 LPM
Whitlow Enterprises, LLC

www.smokeschooLnet

Certifies that

Daniel Wilson ofDerenzo & Associates, Inc Has passed the certification test required by 40 CFR 60Appendix A

and is qualified as a visible emissions evaluator

Certification Date: October 31 2008 Location: Toledo, OH

Qeorae ‘T4)fiit(ow

President

T0H103108-19
Test Gas Type Concentration Deviationfrom Expected

C0 2/N0 (ppm) Analyzer Response Response (ppm) 1.72%/26.4 26.20 CO2 0.20 4.29% -0.10

021N0 0.10 8.36%/26.4 26.27 02 0.13 20.9% 0.00 C0/N0 0.00 23.88/26.4 26.40 CO 0.00 59.70 -0.11 CH4/NOX 0.11 33.6/26.4 26.10 CH4 0.30 84.0 -0.11 S02/NOX 0.11 8.16/26.4 26.20 SO2 0.20 20.4 -0.10

C3H8INOX 0.10 33.32 / 26.4 26.34

C3H8 0.06 83.3 -0.11 0.11

Total Deviation 2 (ppm) 1.0

% of Calibration Span 3 2.38

1 -Measured concentrations were corrected for system bias.

2 -

tested

In summing

with and

the

without

total deviation use the larger of the absolute values obtained for the interferent the pollutant present.

3 -Total Interference must be less than 2.50% ofthe calibration span.
Deviation from Expected Test Gas Type Concentration (ppm) Analyzer Response ‘ C0 2 Response (ppm) /CO 1.72%! 179.3 179.1 0.20

02

CO2 1.72% 0.06 0.06 1C0 8.36%! 179.3 180.6 1.37

02 20.9% -0.09 0.09 NOX/CO 26.4/179.3 179.3 0.02 NO 44.0 -0.10 0.10 CH4/CO 33.6/ 179.3 180.6 1.28 CH4 84.0 -0.01 0.01 SO.,/CO 8.16/179.3 179.08 0.20 SO2 20.4

C3H8

1.29 1.29 /CO 33.32/179.3

C

179.42 0.14

3H8 83.3 0.02 0.02

Total Deviation (ppm) 2 4.38

% of Calibration Span 3 1.46

1 -Measured concentrations were corrected for system bias.

2 - In summing the total deviation use the larger of the absolute values obtained for the interferent tested with and without the pollutant present.

3 -Total Interference must be less than 2.50% ofthe calibration span.
- - - -

- Deviationfrom Expected I n Test Gas Type Concentration (ppm) Analyzer Response NOX/CO, .ftesponse tppm) 26.4 / 1.72% 1.72 NO 0.01 44.0 0.00

02 0.00 /C0 8.36% / 1.72% 1.73 0.02 20.9% 0.00 CO/CO 2 0.00 23.88 /2.57% 2.57 CO 0.00 59.70 0.00 CH4/CO 2 0.00 33.6 / 2.57% 2.57 CE4 0.00 84.0 0.00

C3H8/C0 2 0.00 33.32/2.57 2.57

C3H8 0.00 83.3 0.00 0.00

Total Deviation (ppm) 2 L03

/ of Cahbration Span 0.59

I -Measured concentrations were corrected for system bias.

2 -

tested

In summing

with

the total deviation use the larger of the absolute values obtained for the interferent and without the pollutant present.

3 -Total Interference must be less than 2.50% of the calibration span.
Test Gas Type Deviation from Expected

C0 2/0

Concentration (ppm) Analyzer Response’ Response (ppm) 1.72%! 12.54% 12.62 Co 2 0.08 4.29% 0.00 NO/0 2 0.00 26.4/8.36% 8.41 N0 0.05 44.0 0.00 C0/0 2 0.00 23.88/12.54 12.56 CO 0.02 59.70 0.00 S02/0 0.00 8.16 / 12.54 12.62 SO2 0.08 20.4 0.29

C3H8/02 0.29 33.32 / 12.54 12.58

C3H8 0.04 83.3 0.00 0.00

Total Deviation (ppm) 2 0.48

% of Calibration Span 3 2.30

1 -Measured concentrations were corrected for system bias.

2 -

tested

In summing

with

the total deviation use the larger of the absolute values obtained for the interferent and without the pollutant present.

3 -Total Interference must be less than 2.50% of the calibration span.
APPENDIX C

LABORATORY DATA
Daniel Wilson

DERENZO & ASSOCIATES, iNC.

39395 Schoolcraft Road

Livonia,MI 48150-

Bureau Veritas Work Order No. 09031333

Reference: 0901014

Dear Daniel Wilson:

Bureau Veritas North America, Inc. received 11 samples on 3/3 1/2009 for the analyses presented in the following report.

Enclosed is a copy of the Chain-of-Custody record, acknowledging receipt of these samples. Please note that any unused portion of the samples will be discarded 30 days after the (late of this report, unless you have requested othenvise.

This material is confidential and is intended solely for the person to whom it is addressed. If this is received in error, please contact the number provided below.

We appreciate the opportunity to assist you. If you have any questions concerning this report, please contact a Client Services Representative at (800) 806-5887.

Scott Caillouette

Client Services Representative

cc:

Bureau Veritas North America, Inc.

223i S Rucuhel Drive

Novi, MI 48375

\L4: 7 (248) 3q417()

Fax: (248) 3442F55
Work Order No 09031333

The results of this report relate only to the samples listed in the body of this report.

Unless otherwise noted below, the following statements apply: 1) all samples were received in acceptable condition, 2) all quality control results associated with this sample set were within acceptable limits and/or do not adversely affect the reported results, and 3) the industrial hygiene results have not been blank corrected.

Impinger volumes:

TREP- 1 Cont#2 81 mLTREP-2 Cont#2 41 mL

TREP-3 Cont#2 60 mL

Analytical Comments for Method EPA2O2: Volumes of impinger solutions follow below.

Lab ID Water (mL) Me2CI2 (mL)

09031333-2 390 110

09031333-4 400 140

09031333-6 400 150

0903 1333-7 495 88

Analytical Comments for Method EPA2O2, sample -007A: Please note an oily residue was observed for the methylene chloride blank. The blank sample was received in a plastic polypropylene sample jar. The value ofthe blank may not be representative for samples, since samples were received in glass jars. A white powdery residue was observed in the aqueos client blank.
Sample Type: Acetone Rinse Work Order No: 09031333

Method Reference Method EPA5 Date Received: 03/31/2009

RL (mg): 0.5 Analyst: MLG

Lab Air Particulate by Method EPAS Sample Volume No. Identification Date (liters) (mg) (mg/rn 3) (ppm) Analyzed OOIB TREP-1 CONT #2 03/25/09 0 6.4

--

-- 04/03/2009

0033 TREP-2 CONT #2 03/25/09 0 6.4

--

-- 04/03/2009

0053 TREP-3 CONT #2 03/25/09 0 9.4

--

-- 04/03/2009

General Notes:

<: Less than the indicated reporting limit (RL). Information not available or not applicable. Back sections (if applicable) were checked and showed rio significant breakthrough unless otherwise noted.
Sample Type: GF Filter, Tared Work Order No: 09031333

Method Reference Method EPAS Date Received: 03/31/2009

RL (mg): 0.5 Analyst: MLG

Lab Air Particulate by Method EPAS Sample Volume No. Identification Date (liters) (mg) (mgIm) (ppm) Analyzed OOIA TREP-l CONT#1 03/25/09 0 1.7

--

-- 04/03/2009

003A TREP-2 CONT#I 03/25/09 0 1.8

--

-- 04/03/2009

005A TREP-3 CONT#1 03/25/09 0 1.8

--

-- 04/03/2009

General Notes:

<: Less than the indicated reporting limit (RL). Information not available or not applicable. Back sections (if applicable) were checked and showed no significant breakthrough unless otherwise noted.
Lab ID: 09031333-002A Client Sample ID: TREP-1 CONT #4/CONT #5 Matrix: AIR

Tag Number:

Collection Date: 3/25/2009

Analyses Reporting Result Limit Qual Units DF Date Analyzed Analyst

EPA METHOD 202

Inorganic Condensible Particulate

Matter

Organic Condensible Particulate

Matter

Qualifiers: ND - Not Detected at the Reporting Limit (RL).

.1 - Analyte detected below the Reporting Limit

B - Analyte detected in the associated Method Blank

*

- Value exceeds Maximum Contaminant Level

mg

mg

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitation range

T - Tenta1iely dentied Compound (TI()

19 0.50

8.3 0.50

4/6/2009 MEN

4/6/2009 MEN
Lab ID: 09031333-004A Client Sample ID: TREP-2 CONT #4/CONT #5 Matrix: AIR

Tag Number:

Collection Date: 3/25/2009

Analyses Reporting Result Limit Qual Units DF Date Analyzed Analyst

EPA METHOD 202

Inorganic Condensible Particulate

Matter

Organic Condensible Particulate

Mattcr

Qualifiers: ND - Not Detected at the Reporting Limtt (RL).

-Analyte detected below the Reporting Limit

B - Analyte detected in the associated Method Blank

* Value exceeds Mairnum Contaminant Level

S - Spike Recovery outside accepted recovery limits

R - RPD outside accepted recovery limits

E - Value above quantitatlon range

- fe tat vely I den ti lect Co rnpound ( li( )

19 0.50 mg 1 4/6/2009 MEN

8.6 0.50 4/6/2009 MEN mg
Lab ID: 09031333-006A Client Sample ID: TREP-3 CONT #4/CONT #5

Matrix: AIR Tag Number:

Collection Date: 3/25/2009

Reporting Analyses Result Limit Qual Units DF Date Analyzed Analyst

EPA METHOD 202

Inorganic Condensible Particulate

Matter

Organic Condensible Particulate

Matter

Qualifiers: ND - Not Detected at the Reporting Limit (RL).

- Analyte detected below the Reporting Limit

B -Analyte detected in the associated Method Blank

*

- Value exceeds Maximum Contaminant evel

mg

mg

S - Spike Recovery outside accepted recovery limitsR -RPD outside accepted recovery limits

E - Value above quantitation range

I - Ten tatis ely den tiled (‘on pound (TIC)

27 0.50

4.9 0.50

4/6/2009 MEN

4/6/2009 MEN

_7, I.,
EPA METHOD 202

Inorganic Condensible Particulate

Matter

Organic Condensible ParticulateMatter

Qualifiers: Nt) -Not Detected at the Reporting Limit (RL).

-Analyte detected below the Reporting Limit

B -Analyte detected in the associated Method Blank

*

- Value exceeds Maximum Contaminant I evel

S -Spike Recovery outside accepted recovery limitsR -RPD outside accepted recovery limits

E - ValLie above quantitatlon range

1 — Tentati vcl y ldeiio tied C ornpound (I l(

Lab ID: 0903 1333-007A Client Sample ID: TREP-4 CONT #6-

H20/CONT #7-MECL2

BLANK

Matrix: AIR Tag Number:

Collection Date: 3/25/2009

Reporting

9.9 0.50 mg I 4/6/2009 MEN

3.8 0.50 mg 1 4/6/2009 MEN

C i-i
Lab ID: 09031333-008A Client Sample ID: TREHCL-1 CONT #3

Matrix: AIR Tag Number:

Collection Date: 3/25/2009

Reporting Analyses Result unit Qual Units DF Date Analyzed Analyst

EPA 26

Hydrochloric Acid 530 500 jig I 4/6/2009 MLG

Qualifiers: ND - Not Detected at the Reporting Limit (RL). S -Spike Recovery outside accepted recovery limits

-Analyte detected below the Reporting Limit R - RPD outside accepted recovery limits

13 - Analyte detected in the associated lethod Blank E -Value above quantitation ratige*

- Value exceeds Maximum Contaminant Level T - Tentatively Identified Compound (Tl()

0 1
Lab ID: 0903 1333-009A Client Sample ID: TREHCL-2 CONT #3

Matrix: AIR Tag Number:

Collection Date: 3/25/2009

Reporting Analyses Result Limit Qual Units DF Date Analyzed Analyst

Qualifiers: ND - Not Detected at the Reporting Limit (RL).

- Analyte detected below the Reporting Limit

B - Analyte detected in the associated Method Blank

*

- Value exceeds Maximum Contaminant level

S - Spike Recovery outside accepted recovery limitsR -RPD outside accepted recovery limits

E - Value above quantitation range

T - Fentatively denti tied Compound (IC)

EPA 26

Hydrochloric Acid 3,400 500 4/6/2009 MLG

I I I I
b 

D: 09031333

OIOA Client Sample ID: TREHCL-3 CONT #3

Matrix: AIR

Tag Number:

Collection Date: 3/25/2009

Reporting Analyses Result Limit Qual Units DF Date Analyzed Analyst

S - Spike Recovery outside accepted recovery limits

R -RPD outside accepted recovery limits

E - Value above quantitation range

T - Tentatively Identified Compound (TIC)

500 4/6/2009 MLG

EPA 26

Hydrochloric Acid 3,500

Qualifiers: ND -Not Detected at the Reporting Limit (RL).

- Analyte detected below the Reporttng Limit

B - Analyte detected In the associated Method Blank

C

- Value exceeds Maximum Contaminant Level

ti I 1)
Lab ID: 09031333-O1IA Client Sample ID: TREHCL-4 CONT #6 BLANKMatrix: AIR Tag Number:

Collection Date: 3/25/2009

Reporting Analyses Result Limit Qual Units DF Date Analyzed Analyst

S -Spike Recovery outside accepted recovery limitsR - RPD outside accepted recovery limits

E - Value above quantitation range

T - Tentatively ldeiiti tied Compound (1 IC)

420 4/6/2009 MLG

EPA 26

Hydrochloric Acid ND

Qualifiers: ND -Not Detected at the Reporting Limit (RL).

- Analyte detected below the Reporting Limit

B - Analte detected in the associated Method Blank*

- Value exceeds Maximum (‘ontaminant Level
Livonia Ml 48150

Project Name: Trail Ridge

Project #: 0901014

Workorder #: 0903722A

Dear Mr. David Derenzo

The following report includes the data for the above referenced project for sample(s) received on 3/27/2009 at Air Toxics Ltd.

The data and associated QC analyzed by Modified TO-is (5&20 ppbv) are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative.

Thank you for choosing Air Toxics Ltd. for you air analysis needs. Air Toxics Ltd. is committed to providing accurate data of the highest quality. Please feel free to contact the Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding the data in this report.

Regards,

Ausha Scott

Project Manager

180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630

(916) 985-1000 .FAX (916) 985-1020

Hours 8:00 A.M to 6:00 P.M. Pacific

Page lofl3
Work Order Summary

CLIENT: Mr. David Dereazo

Derenzo & Associates

39395 Schoolcraft Road

Livonia,Ml 48150

BILL TO: Ms. Donna Povich

Derenzo & Associates

39395 Schoolcraft Road

Livonia,Ivll 48150

PHONE:

FAX:

DATE RECEWED:

DATE COMPLETED:

734-464-3880

734-464-4368

03/27/2009

04/09/2009

P.O.# 1002

PROJECT # 0901014 Trail Ridge

CONTACT: Ausha Scott

CERTIFIED BY: _)

DATE: 04/09/09

Laboratory Director

Certfication numbers:

NY NELAP

CA NELAP -0211 OCA, LA NELAP/LELAP- Al 30763, NJ NELAP - CAOO4

Name of Accrediting

- 11291, UT NELAP -9166389892, AZ Licensure AZ0719

Accreditation

Agency:

number:

NELAP/Florida Department of Health, Scope ofApplication: Clean Air Act,

Air Toxics Ltd. certifies E87680, Effective date: 07/01/08, Expiration date: 06/30/09 that the test results contained in this report meet all requirements of the NELAC standards This report shall nut he reproduced, except in full, without the written approval of Air Toxics Ltd.

180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA -95630 (916) 985-1000 (800) 985-5955 FAX (916) 985-1020

RECEWT FINAL FRACTION # NAME TEST O1A TRE-1 VAC./PRES. PRESSURE Modified TO-IS (5&20 ppbv) 4.0 “Hg 5 psi 02A Lab Blank ModifiedTO-15(5&20ppbv) 03A CCV NA NA Modified TO-15 (5&20 ppbv) NA NA 04A LCS Modified TO-iS (5&20 ppbv) NA NA

Page 2of13
One 6 Liter Summa Canister sample was received on March 27, 2009. The laboratory performed analysis via modified EPA Method TO- 15 using GC/MS in the full scan mode. The method involves concentrating up to 50 rnLs of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.

This workorder was independently validated prior to submittal using ‘USEPA National Functional Guidelines’ as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control requirements and verification of all quantified amounts.

Method modifications taken to mn these samples are summarized in the table below. Specific project requirements may over-ride the ATL modifications.

Requirement TO-IS A TL ModUications Daily CCV ±- 30% Difference <1= 30% Difference with two allowed out up to </=40%.; flag and narrate outliers

Sample collection media Surmna canister ATL recommends use ofsumma canisters to insure data

defensibility, but will report results from Tedlar bags at client request

Method Detection Limit Follow 4OCFR PL136 The MDL met all relevant requirements in Method TO-15 App. B (statistical MDL less than the LOQ). The concentration of

the spiked replicate may have exceeded lOX the calculated

MDL in some cases

Receiving Notes

There were no receiving discrepancies.

Analytical Notes

The canisters in this work order were pressurized with Helium prior to sampling, per client request. Dilution factors have been adjusted accordingly.

Defmition of Data Qualifying Flags

Eight qualifiers may have been used on the data analysis sheets and indicates as follows: B - Compound present in laboratory blank greater than reporting limit (background subtraction no performed).

J - Estimated value.

E -Exceeds instrument calibration range.S - Saturated peak.

Q -Exceeds quality control limits.

Page 3of13
may have been used on the data analysis sheets and indicates as follows:

a-File was requantified

b-File was quantified by a second column and detector ri-File was requantified for the purpose ofreissue

Page 4 of 13
CumenePropylbenzene

4-Ethyltoluene

1 ,3,5-Trimethylbenzene

1 ,2,4-Trimethylbenzene

1 ,4-Dichlorobenzene

MODIFIED EPA METHOD TO-15 GC/MS

Rrt. Limit

(ppbv)

Client Sample ID: TRE-1

Lab ID#: 0903722A-O1A

Amount

(ppbv)

Rpt. Limit

(uglm3)

Amount

(uglm3) Compound Freon 12 80 600 390 3000 Vinyl Chloride 80 97 200 250 Ethanol 320 66000 600 120000 Acetone 320 15000 760 36000 2-Propanol 320 18000 780 45000 Hexane 80 250 280 870 2-Butanone (Methyl Ethyl Ketone) 80 17000 230 50000 cis-1,2-Dichloroethene 80 320 320 1300 Tetrahydrofuran 80 3200 230 9600 Cyclohexane 80 220 270 750 2,2,4-Trimethylpentane

Benzene

80 140 370 640

Heptane

80 950 250 300080 410 320 1700 Trichloroethene 80 130 430 710 4-Methyl-2-pentanone 80 910 320 3700 Toluene 80 12000 300 47000 Tetrachloroethene 80 250 540 1700 Ethyl Benzene 80 6400 340 28000 m,p-Xylene 80 13000 340 56000 o-Xylene 80 3800 340 16000 Styrene 80 600 340 2600

80 590 390 290080 480 390 2400

80 2000 390 9700

80

80

80

800

1700

270

390

390

480

4000

83001600

Page 5of 13
Freon 12

Freon 114

Chioromethane

Vinyl Chloride

1 ,3-Butadiene

Bromomethane

ChloroethaneFreon 11

Ethanol

Freon 113

1 ,1-Dichloroethene

Acetone

2-Pro parlol

Carbon Disulfide

3-C h lo rap rope n e

Methylene Chloride

Methyl tert-butyl ether

trans-i ,2-Dichloroethene

Hexane

1 ,1-Dichloroethane

2-Butanone (Methyl Ethyl Ketone)

cis-i ,2-Dichloroethene

Tetrahydrofuran

Chloroform

1,1 ,i-Trichloroethane

Cyclohexane

Carbon Tetrachioride

2,24-Trimethylpentane

1 ,4-Dioxane

Bromodichloromethane

cis-i ,3-Dichloropropene

4-Methyl-2-pentanone

Toluenetrans-i ,3-Dich)oropropene

80

80

320

80

80

8080

80

320

80

80

320320

80

320

80

80

80

80

80

80

80

80

80

80

80

80

80

80

80

320

80

80

80

80

80

600

Not Detected

Not Detected

97

Not Detected

Not Detected

Not Detected

Not Detected

66000

Not Detected

Not Detected

15000

18000

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

250

Not Detected

17000

320

3200

Not DetectedNot Detected

220

Not Detected

140

130

Not Detected

Not Detected

Not Detected

Not Detected

910

12000

Not Detected

390

560

660

200

180

310

210

450

600

610

320

760

780

250

1000

280

290

320

280

320

230

320

230

390

430

270

500

370

430

370

1100

530

360320

300

360

3000

Not Detected

Not Detected

250

Not Detected

Not Detected

Not Detected

Not Detected

120000

Not Detected

Not Detected

36000

45000

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

870

Not Detected

50000

1300

9600

Not Detected

Not Detected

750

Not Detected

640

710

Not Detected

Not Detected

Not Detected

Not Detected

3700

47000

Nat Detected

MODIFIED EPA METHOD TO-is CC/MS

File Name: b040217 Dii. Factor: Date of Collection: 3/25109 5:05:00 PM 15.9 Date of Analysis: 4/2/09 06:12 PM

Compound RDt. Limit Amount Rpt. Limit Amount (ppbv) (ppbv) (uglm3) (uglm3)

Benzene 80 950 250 3000

1 ,2-Dichloroethane

Heptane

80 Not Detected 320 Not Detected

Trichloroethene

80 410 320 1700

1 ,2-Dichloropropane

Page 6of 13
1 ,2-Dichloroethane-d4

Toluene-d84-Bromofi uo ro benze ne

1TIrn EPA METHOD TO-IS GC/MS

70-1 30

70-130

70-130

File Name:Dii. Factor:

b04021 7 Date of Collection: 3125109 5:05:00 PM

15.9 Date of Analysis: 412/09 06:12 PM

Rpt. Limit Amount Rpt. Limit Amount Compound (ppbv) (ppbv) (uglm3) (uglm3) 1,1 ,2-Trichloroethane 80 Not Detected 430 Not Detected Tetrachloroethene 80 250 540 1700 2-Hexanone 320 Not Detected 1300 Not Detected Dibromochloromethane 80 Not Detected 680 Not Detected 1 ,2-Dibromoethane (EDB) 80 Not Detected 610 Not Detected Chlorobenzene 80 Not Detected 360 Not Detected Ethyl Benzene 80 6400 340 28000 m,p-Xylene 80 13000 340 56000 o-Xylene 80 3800 340 16000 Styrene 80 600 340 2600 Bromoform 80 Not Detected 820 Not Detected Cumene 80 590 390 2900 1,1 ,2,2-Tetrachloroethane 80 Not Detected 540 Not Detected Propylbenzene 80 480 390 2400 4-Ethyltoluene 80 2000 390 9700 1 ,35-Trimethylbenzene 80 800 390 4000 1,2,4-Trimethylbenzene 80 1700 390 8300 1 ,3-Dichlorobenzene 80 Not Detected 480 Not Detected 1,4-Dichlorobenzene 80 270 480 1600 alpha-Chiorotoluene 80 Not Detected 410 Not Detected 1 ,2-Dichlorobenzene 80 Not Detected 480 Not Detected 1 ,2,4-Trichlorobenzene 320 Not Detected 2400 Not Detected Hexachlorobutadiene 320 Not Detected 3400 Not Detected

Container Type: 6 Liter Summa Canister

Method Surrogates %Recovery Limits

101

103

98

Page 70113
Freon 12

Freon 114

Chloromethane

Vinyl Chloride

1 ,3-Butadiene

Bromomethane

Chloroethane

Freon 11

Ethanol

Freon 113

1 ,1-Dichloroethene

Acetone

2-Propanol

Carbon Disulfide

3-Chioropropene

Methylene Chloride

Methyl tert-butyl ether

trans-i ,2-Dichloroethene

Hexane

1 ,1-Dichloroethane

2-Butanone (Methyl Ethyl Ketone)

cis-1 ,2-Dichloroethene

Tetrahydrofuran

Chloroform

1,1 ,1-Trichloroethane

Cyclohexane

Carbon Tetrachioride

2,2,4-Trimethylpentane

Benzene

1 ,2-Dichloroethane

Heptane

Trichloroethene

1 ,2-Dichloropropane

1 4-Dioxane

Bromodichloromethane

cis-i ,3-Dichloropropene

4-Methyl-2-pentanone

Toluene

trans-i 3-Dichioropropene

5.0

5.0

20

5.0

5.0

5.0

5.0

5.0

20

5.0

5.0

20

20

5.0

20

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

20

5.0

5.0

5.0

5.0

5.0

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

25

35

41

13

11

19

13

28

38

38

20

48

49

16

63

17

18

20

18

20

15

20

15

24

27

17

31

23

16

20

20

27

23

72

34

23

20

19

23

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

Not Detected

MODIFIED EPA METhOD TO-is GC/MS

File Name: b040206c Oil. Factor: Date of Collection: NA 1.00 Date of Analysis: 4/2/09 11:58 AM

Compound Rpt. Limit Amount Rpt. Limit Amount (ppbv) (ppbv) (uglm3) (ug/m3)

Page 8of 13
MODIFIED EPA METHOD TO-15 GC!MS

File Name: b040206c DII. Factor: Date of Collection: NA 1.00 Date of Analysis: 4/2/09 11:58 AM

Compound Rpt. Limit Amount Rpt. Limit Amount (ppbv) (ppbv) (uglm3) (ugIm3) 1,1,2-Trichloroethane

Tetrachloroethene

5.0 Not Detected 27 Not Detected

2-Hexanone

5.0 Not Detected 34 Not Detected

Dibromochloromethane

20 Not Detected 82 Not Detected

1 ,2-Dibromoethane

5.0 Not Detected 42 Not Detected (EDB)

Chlorobenzene

5.0 Not Detected 38 Not Detected

Ethyl Benzene

5.0 Not Detected 23 Not Detected

m,p-Xylene

5.0 Not Detected 22 Not Detected

o-Xylene

5.0 Not Detected 22 Not Detected

Styrene

5.0 Not Detected 22 Not Detected

Bromoform

5.0 Not Detected 21 Not Detected

Cumene

5.0 Not Detected 52 Not Detected

1,1 22-Tetrachloroethane

5.0 Not Detected 24 Not Detected

Propylbenzene

5.0 Not Detected 34 Not Detected

4-Ethyltoluene

5.0 Not Detected 24 Not Detected 5.0 Not Detected 24 Not Detected 1 ,3,5-Trimethylbenzene

1 ,2,4-Trimethylbenzene

5.0 Not Detected 24 Not Detected

I ,3-Dichlorobenzene

5.0 Not Detected 24 Not Detected

1 ,4-Dichlorobenzene

5.0 Not Detected 30 Not Detected

aipha-Chlorotoluene

5.0 Not Detected 30 Not Detected

I ,2-Dichlorobenzene

5.0 Not Detected 26 Not Detected

1 ,2,4-Trichlorobenzene

5.0 Not Detected 30 Not Detected

Hexachlorobutadiene

20 Not Detected 150 Not Detected 20 Not Detected 210 Not Detected

Container Type: NA - Not Applicable

Surrogates Method %Recovery Limits 1,2-Dichloroethane-d4 98 Toluene-d8 70-130

100 4-Bromofluorobenzene 70-130 94 70-130

Paqe 9of13
1 2-Dichloropropane

1 4-Dioxane

B rom od ich bramethane

cis-1 3-Dichboropropene

4-Methyl-2-pentanone

Toluene

trans-i ,3-Dichboropropene

MODIFIED EPA METHOD TO-15 GC!MS

Fe Name: b040202 - Date of Collection: NA

j Dii. Factor: 1.00 Date of Analysis: 412109 10:40 AM

Compound %Recovery Freon 12

97 Freon 114

92 Chboromethane

106 Vinyl Chloride

98 1,3-Butadiene

96 Bromomethane

105 Chloroethane

98 Freon 11

96 Ethanol

103 Freonli3

93

1 ,1-Dichboroethene 97 Acetone

92 2-Propanol

86 Carbon Disulfide

98 3-Chboropropene 94 Methylene Chloride

Methyl 99 tert-butyl ether 98 trans-I ,2-Dichboroethene 94 Hexane

96

1 ,1-Dichboroethane 97 2-Butanone (Methyl Ethyl Ketone) 96 cis-1 ,2-Dichboroethene

95 Tetrahydrofuran

Chloroform 101

95 1,1 ,1-Trichboroethane

92 Cyclohexane 96 Carbon Tetrachboride

87 22,4-Trimethylpentane 98 Benzene

99

1 ,2-Dichloroethane 96 Heptane

100 Trichboroethene

94

95

92

9393

9497

89

Page 10 of 13
MODIFIED EPA MET[IOD TO—15 (X/MS

File Name: b040202 DII. Factor: Date of Collection: NA 1.00 Date of Analysis: 412109 10:40 AM

1,1 ,2-Trichloroethane

Tetrachloroethene2-Hexanone

Di bromoch to romethane

1 ,2-Dibromoethane (EDB)

Oh to robe nzen e

Ethyl Benzene

m,p-Xylene

o-Xylene

S tyrene

Bromoform

Cumene

1 1 ,2,2-Tetrachtoroethane

Propylbenzene

4-Ethyltoluene

1 ,35-Trimethylbenzene

1 ,2,4-Trimethylbenzene

1 ,3-Dichlorobenzene

1 ,4-Dichtorobenzene

1 ,2-Dichtoroethane-d4

Toluene-d8

4-Bromofi uorobenzen e

%Recovery

96

95

92

92

95

95

95

96

96

96

88

95

96

94

97

94

91

91

88

83

90

107

103

97 70-130 102 70-130

98 70-130

Compound

alpha-Chiorotoluene1 ,2-Dichlorobenzene

1 ,2,4-Trichlorobenzene

Hexachiorobutadiene

Container Type: NA - Not Applicable

Method Surrogates %Recovery Limits

Page llofl3
B ro mod ch oromethane

cis-1 ,3-Dichloropropene

4-Methy?-2-pentanone

Toluene

trans-i ,3-Dichloropropene

90

102

89

100

99

MODIFIED EPA METHOD TO-15 CC/MS

File Name: b040203 Dii. Factor: Date of Collection: NA 1.00 Date of Analysis: 4/2/09 10:59AM

Compound

%Recovery Freon 12

98 Freon 114

Chloromethane 97

Vinyl Chloride 98

100 1,3-Butadiene

Bromomethane 94

Chloroethane 112

Freon 100 11

Ethanol 99

Freon 76 113

98

I ,1-Dichloroethene

Acetone 102

92 2-Propanol

Carbon 102 Disulfide

95 3-Chloropropene

Methylene 88 Chloride

Methyl 104 tert-butyl ether

104 trans-i ,2-Dichloroethene

Hexane 91

1,1-Dichloroethane 91

2-Butanone 101 (Methyl Ethyl Ketone)

cis-1 ,2-Dichloroethene 93

Tetrahydrofuran

Chloroform 93

1,1 ,1-Trichloroethane 99

Cyclohexane 97

Carbon 91 Tetrachloride

2,2,4-Trimethylpentane 85

Benzene 91

102 1,2-Dichloroethane

Heptane 99

Trichloroethene 92

100

1 ,2-Dichloropropane

99 14-Dioxane

88

Page 12of13
MODF[ED EPA METHOD TO-15 CC/MS

File Name: b040203 Date of Collection: NA Dii. Factor: 1.00 Date of Analysis: 412109 10:59 AM

1 ,1 ,2-Trichloroethane

Tetrachioroethene2-Hexanone

Dibromochloromethane1 ,2-Dibromoethane (EDB)

C h lorobenzen eEthyl Benzene

m,p-Xylene

o-XyleneStyrene

BromoformCumene

1,1 2,2-Tetrachloroethane

Pro pyl be nzene

4-Ethyltoluene

1 ,3,5-Trimethylbenzene

1 ,2,4-Trimethylbenzerie

1 3-Dichlorobenzene

1 ,4-Dichlorobenzene

aipha-Chlorotoluene1 ,2-Dichlorobenzene1 ,2,4-Trichlorobenzene

H exach lo rob utad len e

%Recovery

102

99

90

91

100

98

100

100100

106

92

101

101

89

92

96

9796

93

104

94

104

102

1 2-Dichloroethane-d4

Toluene-d84-Bromofluorobenzene

70-130

70-1 30

70-1 30

Compound

Container Type: NA - Not Applicable

Method Surrogates %Recovery Limits

98

102

98

Page l3of 13
P”• /1 All”

TOxics

— Rsli,qushiig signat.ire on th sdocumsril irdoatas thalsDmpk isbeing chpsd in eoniplianoc wfth 1813 BLUE RAVINE ROAD, SUITE B

L1 all applicable lcJ, $13.12. Fednl, national. and inteircicina aws, re;Jlations and crdinance2 Qf FOLSOM, CA 956304719 • any kfrid Air Tmics L matJ dbsUil irio dblet ‘iti iktspt’-t to kbe coiiacticn hans ing or shipping (916) 985-1000 FAX (91 S 985 1 020

CHAIN-OF—CUSTODY RECORD

at tttase samples. R3-wqLlismrç igrhirn Iso Iridlc te. ag.aemerTt to hold hd.rrni’s. tIs ‘zild. and ndewnify AlT Taxies Limited against any cThhn, r.ernsnd, aeuon. of any kud, related to the

colloion, amidTing, ur shipinc of aample€. D.O.T.

-

tUne (000) 467-392a 49 —01

Project Managa rnL-/ B/ti_/C -. 1t ojuntv: Turn Around LSLDIF

Ccted ar Siqiil xeie/ 6’ e./ Ti:_ Pessurizedbv:

Compa’y /)ena.r-co •_Emn&l 01 Cci

•... 1.1 Normal Date:

Address 3cj3cj5 tZ9o1Ci’61tfty Lw.witc State 2ip Cf 8(50 Projt1 - •_ J Rush Prassutizatlon Gas:

F’don€

Fax 4734 d1 (f 9’45 ProjactName ••

_____

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Field Sample ID. (Locatioii)

rAW-f

‘qciofy’

Date

Can# otccUection

lime

of Collection

Wzv/o’i foç47o5

Analyses Requested

Canister Pressure/Vacuum

Initial Final fleceipt Final

Q,TJ1

I —

vpuw’rnr /leL/fl Notes:

Homnquished by: (stg ature) Daie.’flimnci • elve by: (signaure) Dat /1mw

elinquishRd b:siyr1dure) Date/lime Received by:frignature)DatiilTimc

Lab Shipper Name )a’UilE Temp °C) Condition c’ ‘stod &‘rsk Intact 9 Work Order #

yes__NoPfl9O3722

Ftii i253 rsei1
APPENDIX D

SAMPLE CALCULATIONS
q

on 2a -Meter Volume at Standard Conditions: Vm(std) = VmY (Tstd)(Pbar + LJH/13.6) (Tm)(Pstd)

Equation 2b -Volume of Water Vapor Condensed: Vwc(std) Kl(Wf-Wi)

Equation 2c -Moisture Content:

Bws Vwc(std)/(Vwc(std) + Vm(std))

Equation 3a -Velocity at a Traverse Point:

Vd

Equation 3b -Volumetric Flow

=

Rate (Actual

KpCp(T5LIP/PsMWw)” 2

Basis): Q = Vd(avg)Ad 60

Equation 3c -Volumetric Flow Rate (Standard Basis): Qstd

= Q (Tstd)(Ps)

(Ts)(Pstd)

Equation 3d -Volumetric Flow Rate (Standard Dry Basis): Qstd(dry) Qstd(l-Bivs)

Equation 4a — Particulate Matter Concentration: (gr/dscf) PMC (gr/dscf) = (mg*0.01543)/Vm

Equation 4b — Particulate Matter Emission Rate: (lb/hr) PMER (lb/br) = PMC*0.00858*Qstd

Equation 4c — Particulate Matter Emission Rate: (g/bHp-hr) PMER (g/bHp-hr) PMER(lb/hr) * 453.6 * 0.7457 / (kW/0.96)

Equation 4d — PM-10 Emission Rate: (lb/br) PMI 0 (lb/br) = PMER(lb/hr) --Condensible ER(lb/hr)

Equation 4e — PM- 10 Emission Rate: (g/bHp-hr) PM1O ER (g/bHp-hr) = PMER(g/bHp-hr) + Condensible ER(g/bHp-hr)

Equation 5a — Nitrogen Oxides Concentration (ppmvd)

Avg. zero)

NOxC

= ((NOx pprnvd-avg. zero) x Cal. Gas conc.)) / Avg. cal. —
COC (ppmvd) (ppmCO

x (1-(%CO 2/l00)))-avg. zero)

x Cal. Gas conc.))/ Avg. cal.

— Avg. zero)

Equation 6b

—

— Carbon Monoxide Emission Rate: (lb/br) COER (lb/br)

= COC

x Qstd(dry)

x 28.20

x 0.07524/28950000

Equation 6c

— Carbon monoxide Emission Rate: (g/bHp-hr) COER (g/bHP-hr)

= (COER (lb/br) *( 453.6 g/ib) 0.7457 kW/bHp) / (kW /0.96)

Equation 7a

— Brake-horse Power (bHp) bHp (kW/0.96) * bHp/0.7457kW

Equation 8a

— Hydrogen Chloride Concentration: (gr/dscf) HCIC (gr/dscf)

= (mg*0.01543)/Vm

Equation 8b

— Hydrogen Chloride Emission Rate: (lb/br) HC1ER (lb/hi)

= HC1C*0.00858*Qstd

Equation 8c

— Hydrogen Chloride Emission Rate: (lb/MMsct) HCIER (lb/MMscf)

= HCIER(lb/hr) / MMscf/hr fuel consumption

SYMBOL IDENTIFICATION

Ad Area of duct (ft 2) bHp Brake-horse Power

Bws

= Water vapor in gas stream, proportional by volume COC Carbon monoxide concentration (ppmvd) COER

= Carbon monoxide emission rate (lb/br) Cp

= Pitot tube calibration factor (unitless) Ki Constant (0.047 15 fi3/g) Kp

= Constant (85.49) kW Kilowatt

lb/MMscf pounds per million standard cubic foot MWd

= Duct gas dry molecular weight (lb/lb-mole) MWw

= Duct gas wet molecular weight (lb/lb-mole) NOxC

= Nitrogen Oxides Concentration (ppmvd) NOxER

= Nitrogen Oxides Emission Rate (g/bHp-hr) Pbar

= Barometric pressure (“Hg) PMC

= Particulate matter concentration (gr/dscf) PMER

= Particulate matter emission rate (lb/hi) PMIOER PM-l0 emission rate (g/b}lp-hr)
Duct velocity at

a traverse point (flJs) Vm Dry test meter volume (cf)

Vwc(std)

Vm(std) Dry test meter volume at standard conditions (scf)

Wf

Volume ofwater vapor condensed at standard conditions (scf) Final weight ofimpinger/absorber Wi train (g)

= Initial weight ofimpinger/absorber

Y train (g)

= Dry test meter calibration factor (unitless) %C02

= Duct gas carbon dioxide content (%volume) %CO Duct gas carbon monoxide content (%volume) %N2

= Duct gas nitrogen content (%volume) %02

= Duct gas oxygen content (%volume) AH

= Pressure drop across orifice (“H20) tiP Pressure drop across pitot tube (“H20)
APPENDIX

E

PROCESS DATA
Kw Fuel Flow

8:00 1614 538

8:15 1592 536

8:30 1599 537

8:45 1614 539

9:00 1604 538

9:45 1596 536

10:00 1612 540

10:15 1607 537

10:30 1615 540

10:45 1593 537

11:30 1604 53911:45 1612 540

12:00 1598 537

12:15 1591 536

12:30 1595 540

47.4 % methane

38.03 % co2

1.8% oxygen

14:00 1606 553

14:15 1600 550

14:30 1590 548

14:45 1598 550

15:00 1610 554

16:00 1595 539

16:15 1612 545

16:30 1602 543

16:45 1597 543

17:00 1594 541

18:00 1606 545

18:15 1592 540

18:30 1598 541

18:45 1604 542

19:00 1592 538

48.4 % methane

38.9 % co2

1.4% oxygen
APPENDIX F

DETAILED DESCRIPTIONS OF

SAMPLFNG PROCEDURES
Sample probe -Stainless steel single opening probe located at predetermined sampling locations within the exhaust stack cross-section.

Three-way valve -A stainless steel three-way valve is installed between the sample probe and a stainless steel particulate filter to allow the introduction of calibration gases into the sampling system. The three-way valve is turned toward the desired gas flow direction during this sampling. During system bias checks, excess calibration gas exits the sampling probe tip to avoid the introduction of process gas or ambient air during calibration.

Heated sample line

—

A heated Teflon® line is used to transport the sample gas from the stack to

maintains

the instrument rack. The heated Teflon® line is equipped with a temperature controller which the temperature of the sample line at approximately 250°F to prevent moisture condensation.

Sample pump and flow control valve

—

A single head 100% oil-free vacuum pump fitted with a stainless steel flow control valve is used to transfer sampled gases from the heated sample line to the instrumental analyzer. The vacuum pump is leak-free and non-reactive to the gases being sampled. Subsequent sample transport lines and fittings are either stainless steel or Teflon®.

Gas Conditioner -A refrigerant-based condenser equipped with a peristaltic pump is used to remove moisture from the sampled gas stream that is directed to the instrumental analyzers, which require

a conditioned (or dry) gas samples. From the moisture removal system,

a sample gas manifold constructed of Teflon® transport lines and stainless steel Tee fittings is used to continuously deliver the sampled gas to the instrumental analyzers. Since the instrumental analyzers are equipped with internal sampling pumps, the end ofthe sample gas manifold is equipped with an atmospheric dump (or bypass discharge vent) to avoid over pressurization of the instrumental analyzers.

Data Logger

—

A data logging system is used to record I-minute average data from the analog output of the instrumental analyzers.

2.0 Instrumental Analyzer Quality Assurance / Calibration Procedures

Upon site arrival, the instrumental analyzers are set-up in accordance with the manufacturer’s written recommended procedures. Upon setting the appropriate range for the instrument, zero and appropriate span gases are introduced sequential order to verify instrument accuracy (three- point analyzer calibration error test).
ofthe sampling period, appropriate upscale and low-range (zero) gases are re introduced in series at the three-way valve in the sampling system to check against the method’s

of

performance

the

specifications for calibration drift and zero drift error. If the drift error is within 3% span over the period ofthe test run, the test run is considered acceptable

3.0 Isokinetic Sampling System and Procedures for PM-l0

PM-l0 concentrations are equal to the sum ofthe USEPA Method 5 sampling train (filterable) and the USEPA Method 202 sampling train (condensible) measured values. Therefore, combining the results ofthe 5 and 202 sampling train was performed for the determination of PM-l0 concentrations and emission rates from the engine exhaust.

A preliminary traverse ofthe duct was performed to determine duct velocity head and temperature distributions, as well as duct static pressure. Preliminary Method 3 and

4 runs were performed to determine duct moisture and fixed gas content. Based on this information, a sample nozzle of appropriate inside diameter was selected, and the impinger train charged as described below. Traverse points were marked on the probe. Sample time per traverse point was calculated based on the total anticipated sampling time.

A “goose-neck’ nozzle constructed of stainless steel was connected via stainless steel Swagelok® fitting to a borosilicate glass probe liner within a stainless steel probe. Attached to the sample probe was a Stausscheibe (Type S) pitot tube and type

K thermocouple which was used to measure duct velocity head pressure and temperature. The probe liner was attached to a glass filter holder containing a glass fiber filter. The back half of the filter holder was connected via connecting glassware, with temperature monitoring probe, to the impinger train.

The impinger train consisted of a set of impingers, connected in series and immersed in an ice bath. Crushed ice was placed around the impingers to keep the temperatures of the gases leaving the last impinger at 68 °F or less. The train was constructed and charged as follows:

Standard Greenberg-Smith (G-S) impinger containing 100 ml of DI

H20; Standard G-S impinger containing 100 ml of DI

H20; Modified G-S impinger containing 100 ml of DI

H20; Modified G-S impinger containing approximately 200 - 300 grams of pre-dried silica gel and glass fiber.

The sampling train was followed in series by an umbilical line, dry gas meter and calibrated orifice connected to an inclined manometer. Type-K thermocouples were used to measure the stack, impinger outlet, and dry gas meter inlet and outlet temperatures.

A carbon vane pump was used to provide the necessary vacuum for the sampling train.
etic Sampling System and Procedures for HC1

Hydrogen chloride concentrations and emission rates are determined by isokinetically drawing stack gas from the source through

a filter and a 0.1 Normality of Sulfuric acid (0.1

N

H2S04) absorbing solution. The filter collects particulate matter including halide salts but is not routinely recovered or analyzed. Acidic and alkaline absorbing solutions collect the gaseous hydrogen halides and halogens, respectively.

A preliminary traverse ofthe duct was performed to determine duct velocity head and temperature distributions, as well as duct static pressure. Preliminary Method 3 and

4 runs were performed to determine duct moisture and fixed gas content. Based on this information, a sample nozzle of appropriate inside diameter was selected, and the impinger train charged as described below. Traverse points were marked on the probe. Sample time per traverse point was calculated based on the total anticipated sampling time.

A ‘goose-neck nozzle constructed of borosilicate glass was connected via stainless steel Swagelok® fitting to a borosilicate glass probe liner within a stainless steel probe. Attached to the sample probe was a Stausscheibe (Type S) pitot tube and type

K thermocouple which was used to measure duct velocity head pressure and temperature. The probe liner was attached to a glass filter holder containing a quartz filter. The back half of the filter holder was connected via connecting glassware, with temperature monitoring probe, to the impinger train.

The impinger train consisted of

a set of impingers, connected in series and immersed in an ice bath. Crushed ice was placed around the impingers to keep the temperatures ofthe gases leaving the last impinger at 68 °F or less. The train was constructed and charged as follows:

Standard

Standard

G-S

Greenberg-Smith

impinger containing

(G-S) impinger containing 100 ml of 0.1

N

H2S04;

Modified G-S

100 ml of 0.1

N

H2S04; impinger empty; Modified G-S impinger containing approximately 200 - 300 grams of pre-dried silica gel and glass fiber.

The 0.1

N NaOH impingers required by USEPA Method 26A were replaced with an empty knockout impinger, as chloride concentrations are not required for this compliance emissions testing event.

The sampling train was followed in series by an umbilical line, dry gas meter and calibrated orifice connected to an inclined manometer. Type-K thermocouples were used to measure the stack, impinger outlet, and dry gas meter inlet and outlet temperatures.

A carbon vane pump was used to provide the necessary vacuum for the sampling train.
proper

used

operation ofthe metering console. The preliminary traverse velocity pressure values were

This

during the isokinetic testing rather than concurrent measurements ofthe velocity pressures.

concurrent

approach

measurements

was necessary to eliminate high biased flow rate measurements encountered when

are conducted. The high bias is caused by the high static pressure

muffler.

encountered at the sampling locations within the ductwork because ofthe close proximity to the

The dry gas meter temperatures were recorded on the data sheets. The isokinetic-sampling rate in terms of pressure drop across the calibrated orifice were calculated and recorded on the data sheets. The pump and timer was turned on, and the sample rate adjusted to correspond to the calculated isokinetic rate.

Once the sample rate is set, the following data was recorded:

- Dry gas meter inlet and outlet temperatures

- Sample vacuum

-Probe temperature

- lmpinger outlet temperature

-Filter holder outlet temperature

-Orifice differential pressure

-Sample volume (dry gas meter readings)

At the end ofthe sample time for the first point, the probe was moved to the next point; sampling

nozzle

and recording

was

of data was repeated. Upon completion ofsampling (each traverse), the probe, and removed from the port. The sampling train assembly was placed into the next traverse port and the previously described sampling procedures were repeated.

When the sample run was complete, the final, dry gas meter reading was recorded. The probe

check

and filter

was

assembly were removed from the sampling port and allowed to cool.

A post-test leak performed on the sampling train at a vacuum at least as great as that of the highest sample vacuum measured during each sample run. The final leak rate was recorded on the data sheets. The sample train was sealed from contamination and transported to the staging area for recovery.

graduated

Recovery consisted ofthe measurement ofthe liquid in the acid impingers to +1 ml by using a

quantitatively

cylinder or by weighing it to +0.5

g by using

a balance. The impinger contents were

connecting

transferred to a leak-free sample storage container.

A rinse of the impingers and

was

glassware including the back portion of the filter holder (and flexible tubing, if used) conducted with water and was added to the storage container. The container was sealed,