# Bioassays of 

# MacDill Air Force Base Defense Fuel Support Point Industrial WWTF Hillsborough County NPDES #FL0035149 Sampled August 30, 2004

January 2005

Biology Section Bureau of Laboratories Division of Resource Asses sment and Management Quality Manual No. 870346G NELAC Certification No. E31780

### MacDill Air F o rce Base De fense F uel Suppo rt Point Indu strial Wastewater T r eat ment Facility, 5313 N. Bounda ry Ro ad Bldg. 112 2, MacDill Air Force Base, Tampa, Hill sb orou gh Count y, Florida, NP DES #FL00 351 49. Effluent samples for thi s facility were collecte d on Augu st 30, 200 4


## Introduction The MacDill Air Force Base (AFB) Defe nse Fuel Support Point is a region al wholesal e fuel supply center whi c h sto r e s and ship s pet roleu m pro d u c ts to all bran che s of the m ilitary. This facility does n o t have a desi gn flow. The mea n monthly flow from Jan u a r y 1 through Au g u st 31, 200 4, (exclu ding n o - flow du rin g March and May) was 0.61 million gallons per day (M GD). The permittee is authorized to discharge storm w ater from Outfall D-001 to Tampa Bay, a Clas s III marine surface water, from within the diked areas, whi c h contai n rack r unoff, hydrost a tic test water, pump house wastewater and fire suppression test water. Effluen t sample s are colle cted at the point of di scharge from the oil/wa ter sep a rato r str u ctur e. The facility was issued an Administrative Order (AO) No. AO-068-SW, on the issuance date of the permit, that requi re s addition al effluent and flo w monitorin g re quire ment s for interim di scharg e point from Outfall D-0 03, the ou tfall from which the facility has be en di schargi ng. The AO also r equi res the con s truction of an oil-wate r separator p r io r to the point of disch arg e , Outfall D-0 0 1

. All constru c t i on, per the A O , was to be com p leted by Octobe r 2 9 , 2004. The facility is pen ding submi tta l of the compl e ted co nstruction repo rt. The facility wi ll comme nce discha rgin g from D-001 p e nding p e rmit rene wal The disch a rg e monitori ng report s (DMRs) sho w the fa cility has h a d and still ha s violations in regards to not monitori n g or re portin g flow, pH, and other in form ation, and ha s exce ede d its oil and g r ea se water quality standard limit, whi c h has not been reported (facility informati on pr ovided by Nahir Cornwell and Ilia Balcom of F D EP Southwest Distri ct office).


## Methods Sample s we re colle cted from the NPDE S samplin g p o in t D-0 01 (fi nal disch a rg e point) by Na hir Co rn well and Lo ri Pillsbury (F DEP Southwe s t Di stri ct Offi ce) f o llowin g DEP
- SOP-0 01/01 FS 2400 Wastewater Sampling. All DEP SOP’s a r e availabl e o n the web at: http://www.flo r idad ep.o r g/la bs/qa/ sop s .ht m The 48 -ho u r acute scree n i ng toxicity tests and alg a l g r owth p o tenti a l test we re p e rform ed follo wing internal DEP SOP’s TA07_ 01,TA07_ 02, and TA08 _01 through TA0 8_07. All internal DEP SOP’s are available on t he we b at: http://www.flo r id adep.o r g/lab s /cgi-bi n /so p /b ioso p.asp Prior to test i n itiation, bioa ssay sampl e s were a e rated for two hou rs at approxima t ely 100 bubb les pe r minute, red u cing the dissol ved oxygen conc entratio n from 10.9 mg/ L to 7.9 mg/L.


## Toxicit y Test Results Test s we re p e rform ed Aug u st 31 – Sept embe r 2, 200 4. Ceri oda phni a

dubia 48 -h r acute scree n i ng bioa ssay – LC 50 

### > 100%, 0%* mortality in 100% sample at 48 hours Cyprinella leedsi 48 -h r acute scree n ing b i oassay – L C 50 

### > 100%, 0%* mortality in 100% sa mp le at 48 hours See Appen di x 1 for bioassay bench sh e e ts. *NOTE: In a 48-h r a c ute scre enin g test of 100% effluent, mortality of <20% provides rea s on a b le assuran c e th at the effluent meets the a c ute toxicity cri t erion of Flori da’s Su rface Wate r Quality Standard s (Rul e 62 -302. 500 (1 )(a)4, F.A.C.). Mo rtality between 2 0 -50% mo rtal ity indicates l o w to mode ra te levels of toxicity, and furthe r actio n may be req u ired. Mortality of >50% provides rea s o n a b le assu ran c e that the



## 2

### effluent fails to meet the minimum re qui rement to disc harg e to wate rs of the state (Rule 6 2 -4.2 44(3 ) (a), F.A.C.) 

## Algal Gro w t h Potent ial The effluent AGP was 0.3 mg dry wt/L (betwe en t he l aboratory min i mum dete c tion limit and p r acti cal quantitation li mit) of the unicellul a r g r een alga, Pseud o k irchn e ri ella subcapitata , formerly known as Selena strum cap r icornutu m . Rasch ke a nd Shultz (19 87) foun d tha t Algal Growt h Potential (AGP) value s above 5.0 mg dry weight/L rep r e s ent a “probl em” th re shol d for fre s h receiving waters, implyin g nutrient enri c hm ent. A saltwate r AGP test wa s not perfo rme d ; howeve r , the freshwater AGP result s sug g e s t that nutrient en ri chment is likel y not an issu e. The analytica l chemi s try su gge sts that the effluent is n i trogen -limite d . The pre d ict ed AGP base d on nitroge n and pho sph o ru s concentratio n s was 4.2 9 (±2 0 %) mg dry wt/L (Table 1; Miller et al. 1978). Differen c e s b e twee n actu a l and pre d icte d AGP values greate r than an ord e r of m agnitud e are con s id ere d sufficie n t evidence to warra n t follow up testing with the algal growt h inhibition bi oassay. Tru e algal growth inhibition can only be determined by pe rformin g an a c tual algal g r o w th inhibition test. Should a l gal gro w th be su sp ecte d , the district should r equ est that the algal growth in hibi tion test be p e rform ed a s a follow-up to the inspe c t i on. See Table 1 f o r AGP re sult s. 

## Chemistr y Results Total re sidu al chlori ne an d total ammoni a were not de te cted in the bioa ssay sam p le in the lab o rato ry. The total ammoni a con c e n trati on in the sam p le coll ecte d and preserve d for ch emica l analysi s wa s 0.025m g/L. Based o n field measureme n ts of the pH, salinity and tempe r ature o f the effluent whe n coll ecte d, the cal c ulate d uni onized amm o nia co ncentra tion wa s < 0. 001 mg/L. Aluminum an d lead were d e tected in the effluent at le vels that com p ly with Cla s s III Marine wa ter quality crite r ia. Co pp er, nickel, an d zin c we re d e tected b e tween the lab o ratory minimu m detection li mits (M DL) and practi cal quantitation li mits (PQL ). Effluent iron (4 53 μg/L) an d dissolved oxy gen (2.9 m g /L) concentrations did not meet their respective Class III Marine water quality criteri a of ≤ 300 μg/ L (62
- 302.53 0(3 9 ), F.A.C.) and ≥ 4.0 mg/L (62
- 302.5 3 0 ( 31 ), F.A.C.). See Table 2 f o r re sult s of analytes dete c ted in the effluent, and correspon ding li mits. See Appen di x 2 for a com p lete list of ch emical a nalyses pe rform e d

. 

## Conclusion The effluent sample s coll ected from D-00 1 for this fa cili ty on August 30, 2004, did not sho w a c u t e toxicity to either test spe c ie s du rin g the 48-h o u r acute bi o a ssays. The efflu ent AGP resu lt did not exceed the "probl em” thresh old for fre s h re ceivin g waters, sugg esting n u trien t enrich m ent i s likely not an issu e. Effluent iron and di ssolved oxygen concentrations fail ed to meet Cl ass III Marine water quality standards. 

## Literature Cited Miller, W. E., T. E. Maloney, and J. C. Green e. 1978. The Selena strum cap r ico r nutum Printz algal assay bottle test. EPA-600/9-78-018. U. S. EPA, Cinci nnati, Ohio. 126 p. Ra schke, R. L. and D. A. Schultz. 198 7. The use of the algal gro w th potential test for data asse ssm ent. J. Wat. Poll. Cont. Fed. 5 9 (4 ): 222-2 2 7

.



## 3

### L o cat io n AG P ( m easu red) Pred ict e d A G P ( T SIN) ± 20% Inor ga nic N:P ratio Ef

f l uent Sam p les 0.300 AJ U 4 .29 ± 0.858 6.28 A

- V a lue reported is the mean of two or more determinations J - Estimated value U - Material analyzed for but not d e

tected; value reported is the minimum detection limit T

able 1. M eas ur ed and pr ed ic ted algal gr owth potential ( A G P ) for total s o luble nitr ogen ( T SIN) limitation of Ps eudok ir c hner iella s ubc apitata for s a mples from M

a c D ill Air F

o r

c e Bas e Defens e F uel Suppor t Indus tr ial W W T F

on Augus t 30, 2004.



## 4

### Ta ble 2. Effl uen t limits, Cla s s III Cr iter ia a n d wa te r q u a l i t

y da ta f

o r

sa m p l

e s col l e cte d fr om M acDill A i r Fo r c e Base De f e nse Fue l S upp or t I ndustr i a l W W T F Cl ass II I Mar i ne S t a nda r d s Ef f l ue nt Lim i ts Ef f l ue nt Sa m p le s

No ne Detected
- - - B enz en e ≤ 7 1 .28 a R ep or t 0 .5 U A l um in um ≤ 150 0
- 1 0 3 Ar s e nic ≤ 50
- 1 7 U Ca dm i u m ≤ 9.3
- 0

. 0 25 U C a lc iu m ( m g/ L)
- - 46 .6 A Ch r o m i um - III
- - 2 U Co ppe r ≤ 3.7 R ep or t 0 .9 6 I Ir on ≤ 3 0 0 R ep or t 453 A L ead ≤ 8.5 R ep or t 3 .5 A Ma gne sium ( m g / L )
- - 4.5 A Ni ck e l ≤ 8.3
- 2.2 I Se le niu m ≤ 71
- 1 U S ilv er - - 0.02 U Zi n c ≤ 86 Rep o r t 4.2 I TS S
- R e p o r t 4 I Or tho-pho spha te
- - 0

. 0 1 8 T o t a l Ph os ph o r u s - - 0. 06 6 A m m o nia
- - 0 .0 25 Un ioniz e d Am m o nia
- - < 0.001 c N i tr at e+N i tr ite
- - 0

. 0 8 8 T o ta l K j el dah l Nitr o gen - - 0.79 Or ga nic Nitr oge n - - 0 .7 65 c T o t a l N i t r og en - - 0. 87 8 c T u r b idit y t
- 4 .4 A Dissol v e d O x y gen (m g/L) ≥ 4 s R ep or t 2 .9 p H (S.U.) 6.5 - 8.5 6 .5 - 8.5 7 .4 C o nduc t ivity ( u m h os /c m )
- - 423 T e m p e r ature ( C )
- - 2 9

. 8 BO D ( m g/ L)
- - 1

. 4 K O il a n d G r ea s e ( m g/ L) ≤ 5 ≤ 50

. 8 4 I H a r d ne s s ( m g / L )
- - 13 4. 9 c T o ta l Re sidua l Chlorine ( m g/L) ( l a b ) ≤ 0.01
- ≤ 0. 03 U AG P ( m g D r y W t / L )
- - 0

. 3 AJ U V

a lue exceeds the C l ass III Mar i ne W a te r Q u ality Cr i t

er

ia (62-302, F.A

. C

. ) a - A n n ual a v

erag e c - ca lculate d va lue t - S h a ll no t exce ed

29 NT Us a b o

ve

ba ckgr o

u n

d A

- V a l u e re po rt

ed is the me an

of

tw o o r mo re

de termin at

io

ns I - Th e rep o

rted v

a l u e i s b

e

tw

ee n t he la bo ra tory meth od

de tec t io

n l i m i t and th

e l a borat ory prac t i c

a l qu ant it ati o n l i mi t. J - E s ti mated val u e K - A c tua l va l ue is k

now n to be le s s th an v a l u e gi v e n U - Ma teri al a n a l y

z e

d fo r bu t no t d

e

te

c t ed ; v a lu e rep o

rte

d i s

th

e mi ni mum de tec t i o

n l i m i t s - Sin g le

sam p

le Gener a l Ph y si ca l a n d C h em ic al Par a m e t e rs Or g a n ic C ons ti tue n ts ( μ g /L )

Me t a l s ( μ g / L un l e s s other w is e noted )

Nut r ient s ( m g /L ) M

a c D ill Air F

o r

c e Ba s e D e fe ns e F u e l Sup p o r t In du s t r i a l

W W T F

on Au gu s t 30 , 20 0 4

.



## 5

## Appendix 1. Bench Sheets

6

## 7

## 8

## 9

## 10

### Appendix 2. Chemical analyses perfo rmed on the effluent fro m MacDill Air Force Base Defense Fuel Support Industrial WWT F, sampled on August 3 0 , 2004.

Date Samp led F i eld ID Anal ys is Group Comp one nt Result Units Remark MDL PQL 8/30/20 04 1 0 :0 0 F Y 13 BioAGP/LimNut Alga l Gro w t h Potentia l 0.3 mg Dry W t/L A J U 0

. 3 0

. 9 8/30/20 04 1 0 :0 0 F Y 13 Bio-BOD Bioch e mica l Oxyg en Dema nd-5 D a y,N-Inhib 1

. 4 m g / L K 8/30/20 04 1 0 :0 0 F Y 13 Bio-Ch l-a Chlor o p h y ll-A, Monoc hromati c , W a ter 0

. 8 5 u g / L U 0

. 8 5 2

. 6 8/30/20 04 1 0 :0 0 F Y 13 Bio-Ch l-a Phae op h y t i n-A , Monoc hromati c , W a ter 0

. 8 5 u g / L U 0

. 8 5 2

. 6 8/30/20 04 1 0 :0 0 F Y 13 Bio-T o xic o lo g y Bioass a y-Acut e-Scree n F W -C.dubia, L C 50 1 0 0 L C 5 0 L 8/30/20 04 1 0 :0 0 F Y 13 Bio-T o xic o lo g y Bioass a y-Acut e-Scree n F W -F ish, LC50 1 0 0 L C 5 0 L 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 1,2,4- T r ichloro benz en e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 1,2- Dic hlor obe nzen e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 1,3- Dic hlor obe nzen e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 1,4- Dic hlor obe nzen e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2,4,6- T r ichloro phe n o l 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2,4- Dic hlor oph eno l 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2, 4-Dimet h y lp h eno l 4 8 u g / L U 4 8 1 9 0 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2, 4-Di nitrop he n o l 1 4 u g / L U 1 4 5 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2,4- Di nitrotol ue n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2,6- Di nitrotol ue n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2-Ch l o ro nap ht hal e n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2- Chl o ro phe no l 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2-Meth y l -4,6- d initrophenol 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 2- Nitrop h e n o l 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 3,3' -Dichl oro b e n zidi n e 3 8 u g / L U 3 8 1 5 0 8/30/20 04 1 0 :0 0 FY13 BNA-Water 4 , 4 '
- D D D 1

. 4 ug/ L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 4,4'
- D D E 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 4,4' -DDT 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 4-Bromop hen y l p hen y l ethe r 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 4-Chl o ro - 3 -met h ylp hen o l 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 4-Chlorop hen y l p hen y l ethe r 1

. 9 u g / L U 1

. 9 7

. 6 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter 4-Nitrop h e nol 14 ug/L U 14 57 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Ac ena phth ene 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Ac ena phth y l e n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter A l d r i n 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Anthrace n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Benzi d in e 95 ug/L U 95 380 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Benz o( a)ant hracen e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Benz o( a)p y re n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Benzo( b)fluor a n then e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Benzo( g,h,i)p e r y l en e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Benzo( k)fl uora n then e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Bis(2-chloroetho xy)methan e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Bis(2-ch l o ro eth y l) e t h e r 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Bis(2-chloroisoprop y l )ethe r 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Bis(2-eth y lhe x y l ) phthalate 1 4 u g / L U 1 4 5 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter But y l benz yl ph thalate 4

. 8 u g / L U 4

. 8 1 9 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Chr y se n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8


## 118/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Di-n- b u t y l phth a late 4.8 ug/L U 4.8 19 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Di-n-oc t y l p h th alate 0.95 ug/L U 0.95 3.8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Dibe n zo ( a ,h)a nthrace n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Diel d ri n 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Dieth yl phth a la te 18 ug/L UJ 18 72 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Dim eth y l phtha late 48 ug/L U 48 190 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Endos ulfa n I 3.8 ug/L U 3.8 15 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Endos ulfa n II 3.8 ug/L U 3.8 15 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Endos ulfa n sul f ate 1.4 ug/L U 1.4 5.7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Endri n 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Endr i n ald e h y d e 3.8 ug/L U 3.8 15 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter F l uora n the n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter F l uore n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter H eptac h l o r 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Heptac hlor e p o x i de 1.4 ug/L U 1.4 5.7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter He xa c h lor o b e n z e n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter He xa c h lor o b u tadi e n e 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Hexachloroc y clo pentadiene 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter He xac h lor oeth a n e 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Inden o( 1,2,3-c d )p yre n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Isophor on e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter N-Nitrosodi-n -pro p y lamine 1

. 9 u g / L U 1

. 9 7

. 6 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter N-Nitro so dimet h ylami n e 1

. 9 u g / L U 1

. 9 7

. 6 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter N-Nit roso di phe n y lami n e 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Na p h thal en e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Nit rob enze n e 1

. 9 u g / L U 1

. 9 7

. 6 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter P entach l or oph eno l 2

. 9 u g / L U 2

. 9 1 1 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter P hen anthr ene 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter Phen o l 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a te r P y re n e 0

. 9 5 u g / L U 0

. 9 5 3

. 8 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter T R PH 0.5 mg/L U 0.5 2 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter alp ha-BH C 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter beta-BH C 1

. 4 ug/ L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter delta-B H C 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :0 0 F Y 13 BNA-W a ter gamma-BH C 1

. 4 u g / L U 1

. 4 5

. 7 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a ter 1,2,4-T r ichloro benz en e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r 1 , 2
- D i c hlor obe nzen e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r 1 , 3
- D i c hlor obe nzen e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r 1 , 4
- D i c hlor obe nzen e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water 2,4,6-T r ichloro phe nol 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r 2 , 4
- D i c hlor oph eno l 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a t e r 2 , 4
- D i m e t h y lp h eno l 4 8 u g / L U 4 8 1 9 0 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r 2 , 4
- D i nitrop he n o l 1 4 u g / L U 1 4 5 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r 2 , 4
- D i nitrotol ue n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r 2 , 6
- D i nitrotol ue n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a te r 2
- C h l o ro nap ht hal e n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r 2
- C h l o ro phe no l 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water 2-Meth y l -4,6- d initrophenol 2

. 9 u g / L U 2

. 9 1 2 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r 2
- N i t r o p h e n o l 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a te r 3 , 3 ' -Dichl oro b e n zidi n e 3 8 u g / L U 3 8 1 5 0 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA- W a t e r 4 , 4 '
- D D D 1. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r 4 , 4 '
- D D E 1. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r 4 , 4 ' -DDT 1

. 4 u g / L U 1

. 4 5

. 8 

## 128/30/2004 10:40 EQUIPMENT BLANK BNA-Water 4-Bromop hen y l p hen y l ethe r 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLAN K B N A
- W a t e r 4-Chl o ro- 3 -met h ylp hen o l 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water 4-Chlorop hen y l p hen y l ethe r 1

. 9 u g / L U 1

. 9 7

. 7 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r 4
- N i t r o p h e n o l 1 4 u g / L U 1 4 5 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r A c e n a phth ene 0. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r A c e n a phth y l e n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r A l d r i n 1

. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r A n t h r a c e n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BN A-W a t e r B e n z i d in e 9 6 u g / L U 9 6 3 8 0 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r B e n z o ( a)ant hracen e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r B e n z o ( a)p y re n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Benzo( b)fluor a n then e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Benzo( g,h,i)p e r y l en e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Benzo(k)fl uora n then e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Bis(2-chloroetho xy)methan e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Bi s(2-chl o ro eth y l) ether 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Bis(2-chloroisoprop y l )ethe r 2

. 9 u g / L U 2

. 9 1 2 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Bis(2-eth y lhe x y l ) phthalate 1 4 u g / L U 1 4 5 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a ter But y l benz yl ph thalat e 4

. 8 u g / L U 4

. 8 1 9 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r C h r y se n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r D i
- n - b u t y l phth a l a t e 4

. 8 u g / L U 4

. 8 1 9 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Di-n-oct y l p h th alate 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Dibe n zo( a ,h)a nthrace n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r D i e l d ri n 1

. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r D i e t h yl phth a la t e 1 8 u g / L U 1 8 7 1 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a t e r D i m e t h y l phtha l a t e 4 8 u g / L U 4 8 1 9 0 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA- W a t e r E n d o s ulfa n I 3

. 8 u g / L U 3

. 8 1 5 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA- W a t e r E n d o s ulfa n I I 3

. 8 u g / L U 3

. 8 1 5 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a te r E n d o s ulfa n sul f a t e 1

. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r E n d r i n 1

. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r E n d r i n ald e h y d e 3

. 8 u g / L U 3

. 8 1 5 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r F l uora n the n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r F l uore n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r H e p t a c h l o r 1. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Heptac hlor e p o x i de 1

. 4 u g / L U 1

. 4 5

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a te r H e xac h lor o b e n z e n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a te r H e xac h lor o b u tadi e n e 2

. 9 u g / L U 2

. 9 1 2 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water Hexachloroc y clo pentadiene 2

. 9 u g / L U 2

. 9 1 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a t e r H e xac h lor oeth a n e 2

. 9 u g / L U 2

. 9 1 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA-W a ter Inden o(1,2,3-c d )p yre n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK BNA- W a t e r I s o p h o r on e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water N-Nitrosodi-n -pro p y lamine 1

. 9 u g / L U 1

. 9 7

. 7 8/30/2004 10:40 EQUIPMENT BLANK BNA-Water N-Nitroso dimet h ylami n e 1

. 9 u g / L U 1

. 9 7

. 7 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wate r N
- N i t r o s o di phe n y lami n e 2

. 9 u g / L U 2

. 9 1 2 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r N a p h thal en e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r N i t r o b enze n e 1

. 9 u g / L U 1

. 9 7

. 7 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r P e n t a c h l or oph eno l 2

. 9 u g / L U 2

. 9 1 2 8/30/2004 10:40 EQUIPMENT BLANK BNA-Wa t e r P h e n anthr ene 0. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r P h e n o l 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BN A-W a t e r P y re n e 0

. 9 6 u g / L U 0

. 9 6 3

. 8 8/30/2004 10:40 EQUIPMENT BLANK BN A-W a t e r T R P H 0

. 5 m g / L U 0

. 5 2 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r a l p ha-BH C 1

. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r b e t a - B H C 1

. 4 u g / L U 1

. 4 5

. 8 

## 138/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r d e l t a - B H C 1

. 4 u g / L U 1

. 4 5

. 8 8/30/2004 10:40 EQUIPMENT BLANK BNA- W a t e r g a m m a - B H C 1

. 4 u g / L U 1

. 4 5

. 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Alach l o r 0

. 5 8 u g / L U 0

. 5 8 2

. 3 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Ametr y n 0

. 0 4 8 ug/ L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater A t r a z i n e 0

. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Azin p hos Meth yl 0.048 ug/L U 0.048 0.19 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater B r o m a c i l 0

. 1 9 ug/ L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater But y l a t e 0

. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Chlor p yrifos Et h y l 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Chlor p yrifos M e th yl 0. 0 9 6 u g / L U 0

. 0 9 6 0

. 3 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Diazi no n 0

. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater E t h i o n 0

. 0 4 8 ug/ L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Ethopro p 0

. 0 9 6 ug/ L U 0

. 0 9 6 0

. 3 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater F enami p h o s 0

. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater F o n o f o s 0

. 0 9 6 ug/ L U 0

. 0 9 6 0

. 3 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater He xazi no n e 0

. 0 9 6 u g / L U 0

. 0 9 6 0

. 3 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Malath i o n 0

. 1 4 u g / L U 0

. 1 4 0

. 5 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Metala xyl 0

. 2 4 u g / L U 0

. 2 4 0

. 9 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Me tolac h l o r 0

. 4 8 u g / L U 0

. 4 8 1

. 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Me tribuzi n 0

. 0 9 6 u g / L U 0

. 0 9 6 0

. 3 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Mevin p h o s 0

. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Nale d 0

. 7 7 u g / L U J 0

. 7 7 3

. 1 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater No rfluraz o n 0

. 0 9 6 u g / L U 0

. 0 9 6 0

. 3 8 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Para thi on Eth y l 0.14 u g / L U J 0

. 1 4 0

. 5 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Para thi on Meth yl 0.096 ug/L U 0.096 0.38 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater P h o r a t e 0

. 0 4 8 ug/ L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Prometr y n 0

. 1 4 u g / L U 0

. 1 4 0

. 5 6 8/30/20 04 1 0 :0 0 F Y 13 GC-W ater Simazin e 0

. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r A l a c h l o r 0. 5 7 u g / L U 0

. 5 7 2

. 3 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r A m e t r y n 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r A t r a z i n e 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W ater A z i n p h o s Meth y l 0

. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r B r o m a c i l 0. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r B u t y l a t e 0. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W ater Chlor p yrifos Et h y l 0

. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W ater Chlor p yrifos M e th yl 0

. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r D i a z i no n 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC -W a t e r E t h i o n 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r E t h o p r o p 0. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r F enami p h o s 0. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r F o n o f o s 0. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r H e xazi no n e 0. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r M a l a t h i o n 0. 1 4 u g / L U 0

. 1 4 0

. 5 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r M e t a l a xyl 0. 2 4 u g / L U 0

. 2 4 0

. 9 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W at e r M e t o l a c h l o r 0

. 4 8 u g / L U 0

. 4 8 1

. 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W at e r M e t r i b u z i n 0. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r M e v i n p h o s 0. 1 9 u g / L U 0

. 1 9 0

. 7 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC -W a t e r N a l e d 0

. 7 6 u g / L U J 0

. 7 6 3 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W at e r N o r f l u r a z o n 0. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W ater P a r a t h i o n Eth y l 0

. 1 4 u g / L U J 0

. 1 4 0

. 5 6 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W ater P a r a t h i o n Meth y l 0

. 0 9 5 u g / L U 0

. 0 9 5 0

. 3 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r P h o r a t e 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r P r o m e t r y n 0. 1 4 u g / L U 0

. 1 4 0

. 5 6 

## 148/30/20 04 1 0 :4 0 EQUIPMENT BLANK GC-W a t e r S i m a z i n e 0. 0 4 8 u g / L U 0

. 0 4 8 0

. 1 9 8/30/20 04 1 0 :0 0 F Y 13 Metals-W at e r A l u m i n u m 1 0 3 u g / L 5 2 0 8/30/20 04 1 0 :0 0 F Y 13 Metals-W a t e r A r s e n i c 1 7 u g / L U 1 7 6 8 8/30/20 04 1 0 :0 0 F Y 13 Metals-W ater C a d m i u m 0

. 0 2 5 u g / L U 0

. 0 2 5 0

. 1 8/30/20 04 1 0 :0 0 F Y 13 Metals-W ater C a l c i u m 4 6

. 6 m g / L A 0

. 0 5 0

. 2 8/30/20 04 1 0 :0 0 F Y 13 Metals-W ater Chromi um 2 ug/L U 2 8 8/30/20 04 1 0 :0 0 F Y 13 Metals-W at e r C o p p e r 0

. 9 6 u g / L I 0

. 7 5 3 8/30/20 04 1 0 :0 0 F Y 13 Metals-W ater Iron 453 ug/L A 10 40 8/30/20 04 1 0 :0 0 F Y 13 Metals-W at e r L e a d 3

. 5 u g / L A 0

. 1 3 0

. 5 2 8/30/20 04 1 0 :0 0 F Y 13 Metals-W ater Magn e s i u m 4

. 5 m g / L A 0

. 0 2 0

. 0 8 8/30/20 04 1 0 :0 0 F Y 13 Metals-W a t e r N i c k e l 2

. 2 u g / L I 2 8 8/30/20 04 1 0 :0 0 F Y 13 Metals-W at e r S e l e n i u m 1 u g / L U 1 4 8/30/20 04 1 0 :0 0 F Y 13 Metals-W ater S i l v e r 0

. 0 2 u g / L U 0

. 0 2 0

. 0 8 8/30/20 04 1 0 :0 0 F Y 13 Metals-W a t e r Z i n c 4

. 2 u g / L I 3 1 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Meta ls-W a t e r A l u m i n u m 5 u g / L U 5 2 0 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Me tals-W a t e r A r s e n i c 6 u g / L U 6 2 4 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Metals -W a t e r C a d m i u m 0. 0 2 5 u g / L U 0

. 0 2 5 0

. 1 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Metals -W a t e r C a l c i u m 0

. 0 5 m g / L U 0

. 0 5 0

. 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Meta ls-W a t e r C h r o m i u m 2 u g / L U 2 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Meta ls-W a t e r C o p p e r 0

. 7 5 u g / L U 0

. 7 5 3 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Metals-W a t e r I r o n 1 0 u g / L U 1 0 4 0 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Meta ls-W a t e r L e a d 0. 0 5 u g / L U 0

. 0 5 0

. 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Metals-W a t e r M a g n e s i u m 0

. 0 2 m g / L U 0

. 0 2 0

. 0 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Me tals-W a t e r N i c k e l 2 u g / L U 2 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Meta ls-W a t e r S e l e n i u m 1 u g / L U 1 4 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Metals -W a t e r S i l v e r 0. 0 2 u g / L U 0

. 0 2 0

. 0 8 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Me tals-W a t e r Z i n c 3 u g / L U 3 1 2 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d A m m o n i a - N 0

. 0 2 5 mg N / L 0

. 0 1 0

. 0 2 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d Kj el dah l Nitrog en 0.79 mg N/L 0.06 0.2 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d N O 2 N O 3
- N 0

. 0 8 8 mg N / L 0

. 0 0 4 0

. 0 1 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d O-Phosph ate- P 0

. 0 1 8 mg P/L 0.004 0.01 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d T SS 4 mg/L I 4 16 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d T o t a l
- P 0

. 0 6 6 mg P / L 0

. 0 2 0

. 0 6 8/30/20 04 1 0 :0 0 F Y 13 Nutrie nts-Liq u i d T u rbidit y 4

. 4 NT U A 0

. 0 5 0

. 0 5 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Nutrie nts- Liq u i d A m m o n i a - N 0. 0 1 m g N / L U 0

. 0 1 0

. 0 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Nutrie nts-Liq u i d Kjel dah l Nitrog en 0.06 mg N/L U 0.06 0.2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Nutrie nts- Liq u i d N O 2 N O 3
- N 0

. 0 0 4 mg N / L U 0

. 0 0 4 0

. 0 1 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Nutrie nts-Li q u i d O
- P h o s p h ate- P 0. 0 0 4 m g P / L U 0

. 0 0 4 0

. 0 1 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Nutrie nts- Liq u i d T o t a l
- P 0

. 0 2 mg P / L U 0

. 0 2 0

. 0 6 8/30/20 04 1 0 :0 0 F Y 13 Overflo w Oil and Greas e 0.84 mg/L I 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK Over flo w Oil and Greas e 0.69 mg/L U 8/30/20 04 1 0 :0 0 F Y 13 VOC-W a te r B e n z e n e 0

. 5 u g / L U 0

. 5 1 8/30/20 04 1 0 :0 0 F Y 13 VOC-W a ter Eth y l b e n ze n e 0

. 5 u g / L U 0

. 5 2 8/30/20 04 1 0 :0 0 F Y 13 VOC-W a te r T o l u e n e 0

. 5 u g / L U 0

. 5 2 8/30/20 04 1 0 :0 0 F Y 13 VOC-W a ter m,p-Xyl e n e 0

. 5 u g / L U 0

. 5 2 8/30/20 04 1 0 :0 0 F Y 13 VOC-W a te r o - X y l e n e 0

. 5 u g / L U 0

. 5 2 8/30/2004 10:40 EQUIPMENT BLANK VO C-W a t e r B e n z e n e 0

. 5 u g / L U 0

. 5 1 8/30/20 04 1 0 :4 0 EQUIPMENT B L A N K V O C
- W a t e r Eth y l b e n ze n e 0

. 5 u g / L U 0

. 5 2 8/30/20 04 1 0 :4 0 EQUIPMENT BLANK VO C-W a t e r T o l u e n e 0

. 5 u g / L U 0

. 5 2 8/30/20 04 1 0 :4 0 EQUIPMENT B L A N K V O C
- W a t e r m,p-Xyl e n e 0

. 5 u g / L U 0

. 5 2 8/30/2004 10:40 EQUIPMENT BLANK VO C-W a t e r o - X y l e n e 0

. 5 u g / L U 0

. 5 2



## 15T ransact i o n Code NP DE S NU M B E R Y R /M O/DA I n sp T y p e I n spector F ac T y pe 1 N 2 5 3 F L 00351 4 9 1 1 1 204 0830 1 8 B 19 S 20 2

66

T ransact i o n Code NP DE S NU M B E R Y R /M O/DA I n sp T y p e I n spector F ac T y pe

1 N 2 5 3 F L 00351 4 9 1 1 1 204 0830 1 8 X 19 S 20 2

66 Fill O u t This Se c t io n For All Su rface W a t e r D i sc h a r g e r I n spe c t i o n s (C EI , C S I , C B I, PAI, X S I-R I O p t i o n a l )

Rem a rk s 

# The Bi oa ss ay of M a cDi l l A i r Forc e Ba s e De fe nse Fuel Suppor t I ndus tr i a l WWTF ef fl ue nt sa mpl e d on A ugust 30 , 2 0 0 4 , NP DE S #FL0035149. Fill O u t This Se c t io n For All Su rface W a t e r D i sc h a r g e r I n spe c t i o n s (C EI , C S I , C B I, PAI, X S I-R I O p t i o n a l )

Rem a rk s



# T h e Pr io rit y P o llu t a n ts A n aly s is f o r B i o a s s a y o f M acD ill A i r F o r c e Bas e De fe nse Fuel S uppor t I ndus tr i a l WWTF ef fl uent s a m pl e d on A ugus t 30 , 2 0 0 4 , NP DE S # FL0 03 51 49 .

16