# Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility Pearl Harbor, Oahu, Hawaii Latitude: 21 o 

# 22’15” N Longitude: 157 o 

# 53’33” W
HDOH Facility ID No. 9-102271 HDOH Release ID No. 99051, 010011, 020028
February 2009

Prepared by:

TEC Inc. 1001 Bishop St. Suite 1400 American Savings Bank Tower Honolulu, Hawaii 96813

Prepared for:

Commander Navy Region Hawaii Environmental Department, Code N45 850 Ticonderoga Street, Suite 110 Pearl Harbor, Hawaii 96860-5101

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## i 

# Table of Contents

Table of Contents

............................................................................................................................. i Executive Summary ......................................................................................................................... 1 1.0 Introduction .......................................................................................................................... 5 1.1 Project Objective ............................................................................................................. . 5 1.2 Previous Reports .............................................................................................................. 5 1.3 Background .................................................................................................................... .. 6 1.3.1 Site Description ......................................................................................................... 6 1.3.2 Facility Information .................................................................................................. 6 1.3.3 UST Information ....................................................................................................... 6 1.4 Previous Environmental Investigations ............................................................................ 6 1.5 Regulatory Updates .......................................................................................................... 8 2.0 Sample Collection and Analyses ........................................................................................ 10 2.1 Monitoring Well Purging ............................................................................................... 10 2.2 Groundwater Sample Collection .................................................................................... 10 2.3 Groundwater Sample Analyses ...................................................................................... 10 3.0 Groundwater Sample Analytical Results ........................................................................... 11 3.1 October 2008 Sample Analytical Results ....................................................................... 11 3.2 Groundwater Contaminant Trend ................................................................................... 14 3.3 Results of Oil/Water Interface Measurements ............................................................... 14 3.4 Groundwater Status ........................................................................................................ 15 4.0 Summary and Conclusions ................................................................................................. 18 5.0 References .......................................................................................................................... 22

List of Tables Table 1 Analytical Results for Quarterly Gr oundwater Sampling Release Response Report ..13 Table 2 Oil/Water Inte rface Measurements ..............................................................................15 Table 3 Action Levels fo r Compounds of Concern ..................................................................15 Table 4 Responses to Groundwater Monitoring Results ..........................................................16 List of Figures Figure 1 TPH Trends in Groundw ater, Round 13 (October 22, 2008) ......................................20 Figure 2 PAH Trends in Groundw ater, Round 13 (October 22, 2008) ......................................21 List of Appendices Appendix A – Laboratory Analytical Reports

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 1 

# Executive Summary This Quarterly Groundwater Monitoring Report pr esents the results of groundwater sampling conducted on October 22, November 11, and December 16, 2008 at the United States (US) Navy Bulk Fuel Storage Facility at Red Hill, Oahu, Ha waii (the Facility). The sampling and reporting was conducted by TEC Inc. (TEC) for the Air Force Center for Engineering and the Environment (AFCEE) and the Fleet Industrial Su pply Center (FISC) at Pearl Harb or, Hawaii. This report is part of a series of quarterly groundwater m onitoring reports provided by the US Navy to the State of Hawaii Department of Health ( HDOH) in accordance with HDOH’s release response requirements. Currently, there are 18 active a nd 2 inactive, 12.5 million gallon, field-constructed underground storage tanks (USTs) located at the Facility. Background In 2002, the United States (US) Navy installed a groundwater monitoring well (currently named RHMW01) into the basal aquifer, directly down -gradient from the Facility, within the lower access tunnel. Groundwater samples from this well indicated that petrol eum from the Facility had migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the aquifer to prot ect their down-gradient drinking water resource associated with the US Navy Well 2254-01. The US Navy Well 2254 -01 is located appr oximately 3,000 feet downgradient from the Red Hill Fuel Storage F acility and provides appr oximately 24 % of the potable water to the Pearl Har bor Water System (PHWS). By September 2005, the US Navy had installe d two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facility lower access tunnel, a background groundwater monitoring well (RHMW04) up-grad ient from the Facility at ground surface adjacent to the US Navy Firing Range, and a groundwater monito ring well within th e US Navy Well 2254-01 infiltration gallery (RHMW2254-01). All five wells were sampled twice as part of a comprehensive environmental investigation and risk assessment (TEC, 2006). For this investig ation, groundwater samples were analyzed for petroleum constituents and compared agains t HDOH Drinking Water E nvironmental Action Levels (EALs) (HDOH, 2005a). In addition, a three-dimensional (3-D) groundwater model was developed to produce site-specific risk-based acti on levels (SSRBLs) for compounds of concern. The results of this modeling effort indicated that Jet Propulsion (JP)–5 fuel presented the biggest risk to the US Navy water supply, due to its mobili ty and toxicity. Fina lly, the model indicated that a non-aqueous plume (free product) of JP-5 must migrate to within 1,100 feet of the US Navy Well 2254-01 infiltration gallery for HDOH EALs to be exceeded within the gallery. Based on this, free-product must be observed at RHMW01 for EALs to be exceeded at the US Navy Well 2254-01. During the Summer and Fall of 2008, HDOH updated their EALs, wh ich resulted in significant changes to the action levels associated with met hylnaphthalenes. The dr inking water toxicity EAL for these compounds were each previously 240  g/L, assuming they were not carcinogens. Evidence that they are carcinogenic to humans has now been accepted by the United States

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 2 Environmental Protection Agency (USEPA), an d HDOH adopted more rigorous EALs of 4.7  g/L for 1-methylnaphthalene and 24  g/L for 2-methylnaphthalene (HDOH, 2008). The drinking water EAL for naphthalene was al so updated during this process. Previously, HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal (USEPA PRG) of 6.2  g/L, which is associated with a non-cancer Hazard Index of 1. HDOH has updated their naphthalen e drinking water EAL to 17  g/L, in deference to the California Department of Public Health’s Drinking Water Notification Levels (HDOH, 2008).
Finally, the drinking water EAL for TPH-DRO was increased from 100  g/L to 210  g/L, although the gross contamination EAL for TPH-DRO remains 100  g/L.
Groundwater Protection Plan In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater Protection Plan (TEC, 2008), or Plan, which specified SSRBLs for each well, and actions that would occur for the pertinent cases, based on categories for each groundwater monitoring well (Categories 1 through 4). The main object of the Plan is to protect groun dwater quality entering the US Navy Well 2254-01, which provides potable water to the PHWS. This is accomplished by comparing petroleum concentrations in the Facility wells (RHMW01, RHMW02, and RHMW03) to the SSRBLs and taking the corres ponding action. A secondary but important objective of the Plan is to identify leaking US Ts by evaluating increasing concentration trends, or the sudden and lasting presence of free product in one or more groundwater monitoring wells. In the current quarterly groundwat er monitoring report, the current water quality is compared to these categories and actions are recommended, based on those specified in the Plan.

Current Results In October 2008, four normal samples were collected from RHMW01, RHMW02, RHMW03 and the US Navy Well 2254-01, along with the re quired quality control samples (duplicate, matrix spike, spike duplicate, trip blank). Samples were analyzed for Total Petroleum Hydrocarbons (TPH) quantified as Diesel-Range Organics (DRO) and Gasoline Range Organics (GRO), Volatile Organic Compounds (VOCs), Po lynuclear Aromatic Hydrocarbons (PAHs), and lead. Naphthalene and 1-methylnaphthalene were detected at trace concentr ations in the sample from US Navy Well 2254-01; therefore, the well wa s re-sampled in December 2008 for VOCs. VOCs were not detected in the re-sample aliquot. TPH-DRO was detected at 459 micrograms per liter (μg/L) in RHMW01, at 5,420 μg/L (average of normal and duplicate sample) in RHMW02, and 244 μg/L in RHMW03. The HDOH Drinking Water EAL and Site-Specific Risk Ba sed Level for TPH-DRO are 210 μg/L and 4,500 μg/L, respectively. Two PAHs were detected by USEPA method 8270C SIM in the normal and duplicate samples associated with RHMW02 at average c oncentrations above the HDOH Drinking Water EALs: naphthalene at 89. 85 μg/L (HDOH EAL is 17 μg/L) and 1- methylnaphthalene at 67.25 μg/L (HDOH toxicity EAL is 4.7 μg/L). Naphthalene was also measured by USEPA method 8260B in RHMW02, at an average concentration of 242 μg/L.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 3 Trend Analysis At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water EAL since September 2005 but less than 25 percent of the SSRBL of 4,500  g/L. In October 2008, TPH-DRO increased in concentration follo wing a decreasing trend over three previous rounds, since January 2008.
At RHMW02, concentrations of TPH-DRO have been greater than the HDOH Drinking Water EAL since September 2005 and greater th an 50 percent of the SSRBL of 4,500  g/L over that same period. TPH-DRO has been increasing in concentration ove r the last four rounds, since January 2008, and the average c oncentration from the October 2008 sampling event was greater than the SSRBL (solubility limit). Three P AHs (naphthalene, 1-me thylnaphthalene, and 2- methylnaphthalene) also have exceeded the EALs since September 2005. In October 2008, these PAHs decreased in concentrations following increasing trends over three previous rounds (since January 2008). There are no SSRBLs set for these PAHs to date.
At RHMW03, concentrations of TPH-DRO have fluctuat ed around the HDOH EAL since September 2005 and are significantly lower th an at RHMW01 and RHMW02. TPH-DRO at RHMW03 has been increasing in concentration over the past three rounds, since April 2008.

Current Groundwater Status Based on the monitoring event that occurred in October 2008, no free product was observed at RHMW01, RHMW02, or RHMW03. Results fr om groundwater samples indicate that RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is greater than the HDOH EAL for drinking water (210  g/L), but less than ha lf the SSRBL of 4,500  g/L (solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires:

1. Quarterly reports to be sent to HDOH; and 2. Initiation of a leak determination progr am to identify if tanks are leaking. Results from groundwater samples indicate that RHMW02 is presently in Category 4 status, since TPH-DRO (4,540  g/L and 6,300  g/L [duplicate]) is greater than the HDOH EAL for drinking water (210  g/L), and greater than the SSRBL of 4,500  g/L (solubility limit of JP-5). Category 4 response at RHMW02 requires: A. Send quarterly reports to HDOH C. Notify HDOH verbally within 1 day and fo llow with written notification in 30 days D. Notify FISC Chain of Command within 1 day E. Send Type 1 Report to HDOH F. Send Type 2 Report to HDOH I. Remove sampling pumps, measure product in pertinent wells with interface probe, reinstall pumps if product is not detected. J. Immediately evaluate tanks for leaks K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 4 M. Prepare for alternative wa ter source at US Navy Well 2254-01 N. Re-measure for product every month with reports to HDOH

Conclusions and Recommendations There is no indication of an imminent threat to the US Navy Well 2254-01 wate r resources based on this report, since petroleum concentrations at RHMW01 remain less than half the SSRBLs. However, the groundwater status at RHMW02 is Category 4 since th e associated TPH-DRO result was greater than the SSRBL (4,500  g/L). The Groundwater Pr otection Plan requires specific responses to Category 4, which should be conducted. The US Navy plans to install an additional mon itoring well in the Facility lower access tunnel and dedicated oil/water interface probes in four lower access tunnel wells in the coming year to better monitor contaminant migration in the basal drinking water aquifer. It is also recommended that quarterly groundw ater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and lead be continued as previously scheduled until new data indicates a different schedule is required.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 5 

# 1.0 Introduction This report presents the results of the 13 th 

## groundwater sampling and analysis event, conducted in October 2008 (with follow-up sampling in Nove mber and December) at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafte r referred to as “the Facility ”). The Facility consists of 18 active and 2 inactive underground storage tanks (USTs) operated by the Fleet Industrial and Supply Center (FISC), Pearl Harbor. The groundwat er sampling and analysis event is part of a groundwater monitoring program fo r the UST site in response to past UST releases, previous environmental investigations, and recommendations from the State of Hawaii Department of Health (HDOH). 

# 1.1 Project Objective This groundwater sampling and analysis project was performed to evaluate the presence of chemicals of potential concern in groundwater underlying the Facility. The project was conducted to ensure the Navy remains in co mpliance with HDOH UST release response requirements as described in Hawaii Administra tive Rules (HAR) 11-281 Subchapter 7, Release Response Action. The groundwater sampling and an alysis procedures generally followed the procedures described in Red Hill Bulk Fuel Storage Fa cility Groundwater Protection Plan (TEC Inc [TEC], 2008) (Also refe rred to as “the Plan”). This groundwater sampling and analysis even t was conducted by TEC under Air Force Center for Engineering and the Environment (AFC EE) Contract Number F41624-03-D-8618, Task Order 021. 

# 1.2 Previous Reports The following groundwater monitoring reports we re previously submitted to the HDOH:

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 11. Groundwater Monitoring Results, April 2008 (submitted May 2008); and 12. Groundwater Monitoring Results, July 2008 (submitted October 2008).

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 6 

# 1.3 Background The following sections provide a description of th e site and information on the Facility and USTs.
1.3.1 Site Description The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacen t to the north of the Facility is occupied by Halawa Correctional Faci lity and private businesses. Land to the south and west of the Facility includes the Coast Guar d Reservation. Moanalua Valley is located east of the Facility (Dawson, 2006). The Navy Public Works Department operates a pot able water infiltratio n tunnel approximately 1,550 feet hydraulically down-gradient from the Facility (Dawson, 2006). The US Navy Well 2254-01 is located approximately 3,000 feet down-grad ient (west) of the Facility and provides approximately 24 % of the potable water to th e Pearl Harbor Water System, which serves approximately 52,200 military consumers (TEC, 2008).
1.3.2 Facility Information The Facility consists of 18 act ive and 2 inactive USTs operate d by Navy FISC Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006).
1.3.3 UST Information The USTs were constructed in th e early 1940s. The tanks were c onstructed of steel and currently contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel ). Previously, se veral tanks stored Navy Special Fuel Oil, Navy Distillate, aviati on gasoline, and motor gasoline. Each tank measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the tanks lie at depths varying between approxima tely 100 feet and 200 feet below the existing ground surface (TEC, 2006). 

# 1.4 Previous Environmental Investigations 1998 to 2001: From 1998 to 2001, the Navy conducted an i nvestigation at the Facility to assess potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy installed a one-inch diameter sentinel well RHMW01 (previously known as MW-V1D) to monitor for contamination of the basal aquifer underlying the Facility. The well was installed and completed at approximately 100 feet below grade within the underground access tunnel. At the time of well completion, depth to water in RHMW01 was measured at 86 feet below grade (Dawson, 2006). In February 2001, groundwater samples collected from sentinel well RHMW01 contained total petroleum hydrocarbons (TPH) concentrati ons ranging from 883 micrograms per liter (  g/L) to 1,050  g/L and total lead ranging from 10.4  g/L to 15  g/L. The maximum total lead concentration in the samples was equal to the primary drinking water standard of 15  g/L for lead and exceeded the HDOH Tier 1 groundwater action level of 5.6  g/L (Dawson, 2006).

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 7 2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing monitoring wells in 2005. Da wson Group, Inc. collected groundw ater samples from RHMW01 and the Red Hill Navy Pump Station (US Navy We ll 2254-01) in February, June, September, and December 2005. Samples collected in February and June 2005 were not filtered in the field prior to analysis for lead. Analytical results for samples collected from RHMW01 indicated concentrations of total lead were above the HDOH Tier 1 action level of 5.6  g/L. The results were not considered appropriate for risk assessment si nce the sample had not been filte red. In addition, lead was not a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility construction material (TEC, 2007). Samples were filtered in September and Decembe r 2005, and dissolved lead concentrations were below the HDOH Tier 1 action level. Concentra tions of all other cont aminants of potential concern were below HDOH Tier 1 action levels. 2005 – Site Investigation: As part of a site investigatio n, TEC installed three groundwater monitoring wells at the Facility between June and September 2005. Well RHMW02 was installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically upgradient of the USTs to provide geochemist ry for water moving through the basal aquifer beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of approximately 300 feet below ground surface outsi de the tunnel. Groundwater samples were collected from the three newly installed well s and two existing wells (RHMW01 and US Navy Well 2254-01) in September 2005. Naphthalene and trichloroethylene were dete cted in samples collected from RHMW02 at concentrations greater than the HDOH Tier 1 acti on levels. Lead was detected in the sample collected from RHMW01 at a con centration greater than the HDOH Tier 1 action level; however, the sample was not filtered in the field pr ior to analysis. Analytical results for filtered samples obtained by Dawson during the same period indicated concentrations of dissolved lead were below the HDOH Tier 1 action level. 2006 – Site Investigation: Dedicated sampling pumps were in stalled in five wells (RHMW01, RHMW02, RHMW03, RHMW04, a nd US Navy Well 2254-01). TEC collected groundwater samples from the wells in July 2006. The gr oundwater samples were analyzed for petroleum constituents. Naphthalene was detected in sa mples collected from RHMW02 at concentrations above the HDOH Tier 1 action level. In September 2005, with concurrence from the HDOH, the Navy decided to use the newer HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk Assessment project. The EALs are current and pr ovide action levels for more chemicals, and are much more useful for conducting screening ri sk assessments. Since the HDOH June 2005 Policy Letter stated that th e two sets of action levels should not be mixed, the Tier 1 screening levels

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 8 presented in HAR Section 11-281-78 would no longer be used to ev aluate environmental impact at the Facility. 2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. Analytical results indicated the following:

 No chemicals were detected in groundwat er from US Navy Well 2254-01 or RHMW03;

 TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH Drinking Water EALs in RHMW01; and

 TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthale ne were detected in groundwater above the HDOH Dri nking Water EALs in RHMW02. 2007 – Groundwater Sampling: Groundwater samples were co llected in March, June, and September 2007. Analytical resu lts indicated the following:

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 2254-01;

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three sampling events;

 TPH-GRO exceeded HDOH Drinking Wate r EALs at RHMW02 in March;

 TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during all three sampling events;

 1-methylnaphthalene and 2-methylnapht halene exceeded HDOH Drinking Water EAL for taste and odor at RHMW02 duri ng all three sampling events; and

 TPH-DRO exceeded HDOH Drinking Wate r EALs at RHMW03 in June. 2008 – Groundwater Sampling: Groundwater samples were coll ected in January, April, and July 2008. Analytical results indicated the following:

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 2254-01;

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01;

 TPH-GRO did not exceed HDOH Dr inking Water EALs at RHMW02;

 TPH-DRO, naphthalene, 1-me thylnaphthalene, and 2-met hylnaphthalene exceeded HDOH Drinking Water EALs at RHMW02; and

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03.


# 1.5 Regulatory Updates During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant changes to the action levels associated with me thylnaphthalenes. The drinking water toxicity EAL for these compounds was previously 240  g/L, assuming they were not carcinogens. Evidence that they are carcinogenic to humans has now been accepted by the United States Environmental Protection Agency (USEPA), an d HDOH adopted more rigorous EALs of 4.7  g/L for 1-methylnaphthalene and 24  g/L for 2-methylnaphthalene, corresponding to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008).

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 9 The drinking water EAL for naphthalene has also been updated during this process. Previously, HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal (USEPA PRG) of 6.2  g/L, which is associated with a non-cancer Hazard Index of 1. HDOH has updated their naphthalen e drinking water EAL to 17  g/L, in deference to the California Department of Public Health’s Drinking Wate r Notification Levels, a Hazard Index of 2.7 (HDOH, 2008). Finally, the drinking water EAL for TPH-DRO was increased from 100  g/L to 210  g/L, although the gross contamination EAL for TPH-DRO remains 100  g/L.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 10 

# 2.0 Sample Collection and Analyses The majority of field activities relating to gr oundwater sample collection were conducted on October 22, 2008. Groundwater samples were co llected from three monitoring wells located inside the Facility lower access tunnel and one monitoring well located at the Red Hill Navy Pump Station. Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan (TEC, 2008). A total of seven samples were collected; one normal sample from monitoring we lls US Navy Well 2254-01, RHMW01, RHMW02 and RHMW03, one duplicate sample from RHMW02 (Sampled as RHMWA01 and reported as RHMW02-WG11D), and one matrix spike and matrix spike duplicat e from US Navy Well 2254-01. The groundwater at RHMW01 was resampled for dissolved lead on November 3, 2008 because the original sample was not filtered in the field. Due to trace concentrations of naphthalene detect ed in the October 22, 2008 sample from the US Navy Well 2254-01, an additional sample was collect ed for Volatile Organic Compounds (VOCs) at US Navy Well 2254-01 on December 16, 2008 , including one duplicate for VOCs. 

# 2.1 Monitoring Well Purging The groundwater monitoring wells were purged a nd sampled using a dedicated pump system. Well purging was considered complete when no less than three successive water quality parameter measurements had stabilized within ap proximately 10 percent. Field parameters were measured at regular intervals during well pur ging and included pH, temperature, specific conductivity, dissolved oxyge n, and turbidity. Purge water was di sposed in the Facility oil/water separator system. 

# 2.2 Groundwater Sample Collection Each monitoring well was sampled immediatel y following purging. All wells were sampled directly from their dedicated bladder pump system. Samples were placed into sampling containers with appropriate pr eservatives (i.e., hydrochloric acid [HCl] for volatile organic analysis, nitric acid [HNO 3 

## ] for dissolved lead). Dissolved lead samples were filtered in the field and placed in preserved bottles. Sample cont ainers were labeled with the date, sample identification number, type of analysis, and sampler’s name. The containers were placed on ice in sample coolers and transporte d under chain-of-custody procedur es to the certified laboratory for analysis. 

# 2.3 Groundwater Sample Analyses Groundwater samples were analyzed by SGS Environm ental Service, Inc. in Anchorage, Alaska for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, polynuclear aromatic hydrocarbons (PAHs) by EP A Method 8270C SIM, and dissolved lead by EPA Method 6020.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 11 

# 3.0 Groundwater Sample Analytical Results This section provides a summary of analytical results for groundwater samples collected from three monitoring wells located in the lower access tunnel of the F acility and one monitoring well located at the Red Hill Navy Pump Station. Duplicate sample results from monitoring wells RHMW02 and RHMW2254-01 are reported in th is document as RHMW02D and RHMW2254- 01D, respectively. A summary of groundwater anal ytical results is incl uded in Table 1. Complete analytical laboratory repo rts are provided in Appendix A. 

# 3.1 October 2008 Sample Analytical Results All groundwater samples were analyzed for TP H-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. Naphthalene and 1-met hylnaphthalene were detected at US Navy Well 2254-01 at 0.05F μg/L and 0.03F μg/L, respectively. This is be low the HDOH Drinking Water EALs of 17 μg/L for naphthalene and 4.7 μg/L for 1-methylnaphthlen e. Data qualifier “F” indicates the result is between the method detection limit (MDL) and the reporting limit (RL) and considered an estimated value. However, naphthalene or 1- methynapthalene are generally not observed in groundwater from JP-5 releases when TPH is not detected. For th is reason, these lowconcentration PAH results may not be from th e groundwater, but the sour ce of the expected cross-contamination is not known. Following th e receipt of the preliminary results, FISC implemented an immediate re-sampling of the US Navy Well 2254-01 for VOCs, including naphthalene.

RHMW01 Four petroleum constituents were detected at RHMW01: TPH-DRO, fluorene, naphthalene, and lead. TPH-DRO was detected at RHMW01 at 459 μg/L, which is above the HDOH Drinking Water EAL of 210 μg/L. All other petroleum constituents were below HDOH Drinking Water EALs at RHMW01.

RHMW02 Eight petroleum constituents were detected at RHMW02: TPH-DRO, TPH-GRO, 1- methylnaphthalene, 2-methylnaphthalene, acenaphthene, fluorene, naphthalene, benzene, and ethylbenzene. TPH-DRO was detected at RH MW02 in the normal and duplicate samples, at 4,540 μg/L and 6,300 μg/L, respectively. Both results exceeded the HDOH EAL and sitespecific risk based level (SSRBL ) (the HDOH EAL is 210 μg/L and the SSRBL is 4,500 μg/L). Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. USEPA Method 8260B produced the highest naphthalene c oncentrations, which averaged 242 μg/L from the normal and duplicate sample (HDOH EAL is 17 μg/L). In addition, 1-methylnaphthalene and 2-methylnapthalene were detected by USEPA Method 8270C SIM in the normal and duplicate samples. The average result for 1-me thylnaphthalene was 67.25 μg /L, greater than the HDOH toxicity EAL of 4.7 μg/L. The average result for 2-me thylnaphthalene was 13.2 μg/L, less than the HDOH toxicity EAL of 24 μg/L but greater than the HDOH taste and odor EAL of 10  g/L. All other petroleum constituents were below HDOH Dri nking Water EALs at RHMW02.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 12 RHMW03 Four constituents were detected at RH MW03: TPH-DRO, 1-methylnaphthylene, 2- methylnaphthalene, and naphthale ne. TPH-DRO was detected at RHMW03 at 244 μg/L, slightly above the HDOH EAL of 210 μg/L. All other petroleum constituents were below HDOH Drinking Water EALs at RHMW03. US Navy Well 2254-01 as RHMW2254 RHMW2254 was sampled twice during this re porting period. On October 22, 2008, trace concentrations (less than the reporting limit but greater than the detectio n limit) of naphthalene (0.05 μg/L) and 1-methylnaphthalene (0.03 μg/L) were detected by USEPA Method 8270C SIM. On December 16, 2008, RHMW2254 was re-sam pled by USEPA Method 8260B. Although no petroleum constituents were observed in th e re-sample, the method detection limit for naphthalene was 0.62 μg/L and 1-met hylnaphthalene was not analyzed.Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (October 22, 2008 and December 16, 2008)Red Hill Fuel Storage Facility, Pearl Harbor, HawaiiResult Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RLTPH as DIESEL RANGE ORGANICS21010045982.50 412.00454080.00 400.00630098.20 491.00244F 88.40 442.00 ND U 84.20 421.00 NA NA NA NA NA NA NA NATPH as GASOLINE RANGE ORGANICS100100 ND U 10.00 100.00 52.80 F 10.00 100.00 52.90 F 10.00 100.00 ND U 10.00 100.00 ND U 10.00 100.00 NA NA NA NA NA NA NA NA1-METHYLNAPHTHALENE4.710ND U 0.015 0.0572.100.781 2.662.400.75 2.5 0.07 0.0155 0.0515 0.03 F 0.015 0.05 NA NA NA NA NA NA NA NA2-METHYLNAPHTHALENE2410ND U 0.015 0.0513.700.313 1.0412.700.3 1 0.09 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAACENAPHTHENE37020ND U 0.015 0.05 0.370.0156 0.0521 0.210.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAACENAPHTHYLENE2402000 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAANTHRACENE180022ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NABENZO(a)ANTHRACENE0.0925ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NABENZO(a)PYRENE0.21.9 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NABENZO(b)FLUORANTHENE0.0927ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NABENZO(g,h,i)PERYLENE15000.13 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NABENZO(k)FLUORANTHENE0.920.4 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAMethodHDOH ResidentialDrinking Water EALs1UG/LHDOH DrinkingWater CeilingEALs2UG/LChemicalRHMW01UG/LRHMW2254UG/LRHMW02UG/LRHMW02DUG/LRHMW03UG/L8015B (Petroleum)8270C SIM (PAHs)October 22, 2008October 22, 2008 October 22, 2008 October 22, 2008 October 22, 2008RHMW2254DUG/LDecember 16, 2008RHMW2254UG/LDecember 16, 2008CHRYSENE9.2 0.8 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NADIBENZ(a,h)ANTHRACENE0.0092 0.25 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAFLUORANTHENE1500 130 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAFLUORENE240 950 0.02 F 0.015 0.05 0.21 0.0156 0.0521 0.12 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAINDENO(1,2,3-c,d)PYRENE0.092 0.27 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NANAPHTHALENE17 21 0.10 0.031 0.197.401.61 5.2182.301.55 5 0.22 0.032 0.103 0.05 F 0.031 0.1 NA NA NA NA NA NA NA NAPHENANTHRENE240 410 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NAPYRENE180 68 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA1,1,1,2-TETRACHLOROETHANE0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,1-TRICHLOROETHANE200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1,2,2-TETRACHLOROETHANE0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,2-TRICHLOROETHANE5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1-DICHLOROETHANE2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2,4-TRICHLOROBENZENE3.8 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DIBROMO-3-CHLOROPROPANE (DBCP)0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 21,2-DICHLOROPROPANE5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,3-DICHLOROBENZENE180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,3-DICHLOROPROPANE0.4 50000 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.41,4-DICHLOROBENZENE75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5ACETONE22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10BENZENE5 170 ND U 0.12 0.4 0.14 F 0.12 0.4 0.15 F 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4BROMODICHLOROMETHANE0 1850000NDU0 150 5NDU0 150 5NDU0 150 5NDU0 150 5NDU0 150 5NDU0 150 5NDU0 150 5BROMODICHLOROMETHANE0.1850000NDU0.150.5NDU0.150.5NDU0.150.5NDU0.150.5NDU0.150.5NDU0.150.5NDU0.150.5BROMOFORM100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1BROMOMETHANE8.5 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3CARBON TETRACHLORIDE5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROBENZENE100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5CHLOROETHANE3.9 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROFORM100 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1CHLOROMETHANE160 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1cis-1,2-DICHLOROETHYLENE70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DIBROMOMETHANE0.0056 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1ETHYLBENZENE1.5 30 ND U 0.31 1 0.45 F 0.31 1 0.42 F 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1HEXACHLOROBUTADIENE0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1M,P-XYLENE (SUM OF ISOMERS)10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2METHYL ETHYL KETONE (2-BUTANONE)7000 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYL ISOBUTYL KETONE2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYLENE CHLORIDE4.3 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5NAPHTHALENE17 21 ND U 0.62 2239.0012.4 40245.0012.4 40 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2STYRENE100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TETRACHLOROETHYLENE(PCE)5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TOLUENE1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1trans-1,2-DICHLOROETHENE100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TRICHLOROETHYLENE(TCE)5310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 18260B (VOCs)( )VINYL CHLORIDE2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 16020LEAD15 50000 0.97 F 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 NA NA NA NA NA NA NA NAPAHs - Polynuclear aromatic hydrocarbonsMDL - Method detection limitVOCs - Volatile organic compoundsRL - Reporting limitUG/L - Micrograms per LiterTPH - Total petroleum hydrocarbonsQ - Data qualifierND - Indicates that the compound was not detected above the stated method detection limitU - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzedF - Indicates that the compound was identified but the concentration was above the MDL and below the RL-Result exceeds one or both HDOH EALs12Toxicity-based environmental action levels, Table D-1b,Screening For Environmental Concerns At Sites WithContaminated Soil and Groundwater,HDOH, 2008Taste, odor and solubility thresholds, Table G-1,Screening For Environmental Concerns At Sites With Contaminated Soiland Groundwater, HDOH, 2008200Page 1 of 1

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 14 

# 3.2 Groundwater Contaminant Trend Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 shows TPH trends in groundwater at the Facility. Fi gure 2 shows PAH trends in groundwater at the Facility. In these figures, open icons (without fill) repres ent the method detection limit for chemicals that were not detected.

RHMW01 TPH-GRO has only been detected in April 2008 at 13.6F μg/L, which is below the HDOH Drinking Water EAL of 100 μg/L . In October 2008, TPH-GRO wa s not detected. TPH-DRO was detected above the HDOH Dr inking Water EAL during all gr oundwater sampling events and showed a decreasing trend until the January 2 008 sampling event. Concentration of TPH-DRO observed during the October 2008 sampling event wa s greater than the concentrations observed in April and July 2008, but lower th an the January 2008 sampling event.

RHMW02 TPH-GRO was detected in nine of ten samplin g events since September 2005, and exceeded the HDOH Drinking Water EAL thr ee times during 2006 and 2007. The maximum concentration detected was 148 μg/L. The concentration of TPH-DRO was relatively stable at RHMW02 until January 2008, ranging from 2,250 to 3,180 μg/L. Ho wever, since January 2008 it has shown an increasing trend with concentr ations up to 5,420 μg/L, well above the HDOH EAL, and above the SSRBL of 4,500 μg/L. PAHs at RHMW02 remain above the HDOH Drinking Water EALs, and concentrations have decreased in Octobe r 2008 after showing an increasing trend since January 2008.

RHMW03 TPH-GRO has never been detected. TPH-DRO had shown a decreasing trend until the January 2008 sampling event. Concentrations of TPH- DRO observed during the October 2008 sampling event were higher than the previous rounds. In general, concentrations of petroleum-related compounds at RHMW03 have been the lowest of the three wells located within the Facility. 

# 3.3 Results of Oil/Water Interface Measurements The presence and thickness of light-non aque ous phased liquids (LNAPL), otherwise known as free product, released from the USTs were meas ured during this sampling event using a 300 ft Heron Oil/Water Interface Meter. The static water levels were measured to a precision of ± 0.01 ft and fuel thickness was measured to a pr ecision of ± 0.01 ft with this equipment. In January 2008, fuel was measured in mon itoring wells RHMW01 and RHMW02 at a thickness of < 0.01 ft, but has not been observed in othe r monitoring wells as of this document. Measurements to determine the presence and thickness of fuel were conducted at RHMW01, RHMW02, and RHMW03 during the current sampling round. No fuel pr oduct was observed in any of these wells during this event (see Table 2).

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 15 Table 2. Oil/Water In terface Measurements

Date RHMW01 RHMW02 RHMW03 SWL

(ft) LNAPL (ft) SWL (ft) LNAPL (ft) SWL (ft) LNAPL (ft) January 2008 17.74 < 0.01 18.78 < 0.01 NT NT July 2008 19.04 0.00 18.91 0.00 18.86 0.00 October 2008 18.61 0.00 18.56 0.00 18.82 0.00 November 2008 18.50 0.00 18.45 0.00 18.51 0.00

SWL Static water level, elevation above mean sea level LNAPL Light Non-Aqueous Phased Liquid, fuel product on groundwater ft Feet NT Not Taken 

# 3.4 Groundwater Status Compounds of concern are defined as those petroleum-related chem icals that have been observed in the groundwater samples above the HDOH EALs. In accordance with the Red Hill Bulk Fuel Storage Facility Final Groundwater Protection Plan (TEC, 2008), Table 3 defines the constituents of concern in gr oundwater at the Facility and the SSRBLs and updated EALs for each (HDOH 2008). Table 3. Action Levels for Constituents of Concern

Chemical EAL (μg/L) SSRBL (μg/L) Petroleum Mixtures TPH-DRO 210 4,500 TPH-GRO 100 4,500 Semi-Volatile Compounds 1-Methylnaphthalene 4.7 NA 2-Methylnaphthalene 24 NA Naphthalene 17 NA NA – Not applicable or not determined SSRBLs are applicable at RHMW01, RHMW02, and RHMW03 EALs are applicable at US Navy Well 2254-01 

## In addition, the Plan defines four results categor ies of groundwater status for the Facility, based on concentrations of constituents of c oncern in RHMW01, RHMW 02, RHMW03 and the US Navy Well 2254-01, and requires sp ecific responses when these categories are observed during quarterly groundwater sampling. Table 4 describe s each of the four results categories and identifies response actions to be taken in accordance with the Plan.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 16 Table 4. Results Categories and Response Actions to Changes in Groundwater Status

Results Category RHMW02 or RHMW03 RHMW01 US Navy Pumping Well 2254-01 Results Category 1: Result above detection limit but below drinking water EAL and trend for all compounds stable or decreasing A A A,D,M,E,P

Results Category 2: Trend for any compound increasing or drinking water EAL exceeded A, B A, B A,B,C,D,E,F,G,K, L,O Results Category 3: Result Between 1/10X SSRBL and SSRBL for benzene, or between 1/2X SSRBL and SSRBL for TPH A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J, K,L,O

Results Category 4: Result Exceeding any SSRBL or petroleum product observed A,C,D,E,F,I,J, K,M,N A,C,D,E,F,I, J,K,M,N,O A,C,D,E,F,G,I,J,K, L,O Specific Responses: A. Send quarterly reports to HDOH B. Begin program to determine the source of leak C. Notify HDOH verbally within 1 day and fo llow with written notification in 30 days D. Notify FISC Chain of Command within 1 day E. Send Type 1 Report (see box below) to HDOH F. Send Type 2 Report (see box below) to HDOH G. Increase monitoring frequency to once pe r month (if concentrations increasing) H. Notify HDOH verbally within 7 days and follow with written notification in 30 days I. Remove sampling pumps, measure product in pe rtinent wells with inte rface probe, re-install pumps if product is not detected. J. Immediately determine leaking tank K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01 L. Provide alternative water source at 2254-01 M. Prepare for alternative wa ter source at US Navy Well 2254-01 N. Re-measure for product every month with reports to HDOH O. Install additional monitoring well downgradient Report Types HDOH Type 1 Report

 Re-evaluate Tier 3 Risk Asse ssment/groundwater model results

 Proposal to HDOH on a course of action HDOH Type 2 Report

 Proposal for groundwater treatment

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 17 Based on the monitoring event that occurred in October and November 2008, no free product was observed at RHMW01, RHMW02, or RHMW03. Results from groundwater samples indicate that RHMW01 and RHMW 03 are presently in Category 2 status, since TPH-DRO is greater than the HDOH EAL for drinking water (210  g/L), but less than half the SSRBL of 4,500  g/L (solubility limit of JP-5). Cate gory 2 response at RHMW01 and RHMW03 requires: 1. Quarterly reports to be sent to HDOH; and 2. Initiation of a leak determination progr am to identify if tanks are leaking. Results from groundwater samples indicate that RHMW02 is presently in Category 4 status, since TPH-DRO (4,540  g/L and 6,300  g/L [duplicate]) is greater than the SSRBL of 4,500  g/L (solubility limit of JP-5). Category 4 response at RHMW02 requires: A. Send quarterly reports to HDOH C. Notify HDOH verbally within 1 day and fo llow with written notification in 30 days D. Notify FISC Chain of Command within 1 day E. Send Type 1 Report to HDOH F. Send Type 2 Report to HDOH I. Remove sampling pumps measure product in pe rtinent wells with interface probe, re-install pumps if product is not detected. J. Immediately evaluate tanks for leaks K. Collect samples from nearby Halawa D eep Monitoring Well (2253-03) and OWDF MW01. For permission to sample 2253-03, call DLNR Commission on Wate r Resource Management (808) 587-0214, DLNR.CWRM@Hawaii.gov M. Prepare for alternative wa ter source at US Navy Well 2254-01 N. Re-measure for product every month with reports to HDOH In response to the previous Category 3 conditions at RHMW02, oil/water interface measurements were collected in October 2008 and November 2008 at RHMW01, RHMW02 and RHMW03. To date, there is no evidence of fuel on groundwater at any of these wells based on oil/water interface measurements. Category 4 groundwater status at RHMW02 re quires additional efforts, including:

 Re-evaluate risk assessment and groundwater model (TEC, 2007) to ensure both are valid and protective of human health and the e nvironment under the existing conditions and provide a report describing the results of this re -evaluation to the HDOH;

 Evaluate potential requirement for groundwater treatment an d provide a report describing the results of this re-evaluation to the HDOH;

 Implement monthly oil/water interf ace measurements at RHMW01, RHMW02, RHMW03, and provide monthly lette r reports of the results;

 Evaluate tanks associated with the middle s ection of the Facility (Tanks 5, 6, 7, 8, 9, 10, 11, 12, 13, and 14);

 Collect samples from nearby Halawa D eep Monitoring Well (2253-03) and OWDF MW01;

 Prepare for alternative water source at US Navy Well 2254-01, as necessary.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 18 

# 4.0 Summary and Conclusions At RHMW02, the concentration of TPH-DR O in groundwater exceeded the SSRBL of 4,500  g/L, which indicates Category 4 groundwater status at RHMW02.

 The SSRBL of TPH-DRO is set at the solubi lity limit of JP-5 and exceeding the SSRBL implies that JP-5 is in direct contact w ith groundwater in the vicinity of RHMW02.

 Oil/water interface measurements were coll ected in October 2008 and November 2008 from RHMW01, RHMW02, and RHMW03 and no fuel thickness was measured.

 The concentration of TPH-DRO measured at RHMW01 in October 2008 was one tenth of the SSRBL. RHMW01 is down-gradie nt from RHMW02 and between RHMW02 and the US Navy Well 2254-01, an important drinki ng water source for the Pearl Harbor Water System.

 The US Navy Well 2254-01 is not imminently threatened at this time; however, conditions should be monitored closely to de termine if any USTs in the Facility are currently leaking fuel into the subsurface.

 Category 4 activities should be implemented, including:

 Re-evaluate risk assessment and groundw ater model (TEC, 2007) to ensure both are valid and protective of human health and the envi ronment under the existing conditions and provide a report describing th e results of this re-evaluation to the HDOH;

 Evaluate potential requirement for gr oundwater treatment and provide a report describing the results of this re-evaluation to the HDOH;

 Implement monthly oil/water interf ace measurements at RHMW01, RHMW02, RHMW03, and provide monthly lette r reports of the results;

 Evaluate tanks associated with the middle section of the Facility (Tanks 5, 6, 7, 8, 9, 10, 11, 12, 13, and 14);

 Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01;

 Prepare for alternative water source at US Navy Well 2254-01, as necessary. The US Navy plans to install an additional monitoring well (RHMW05) in the lower access tunnel of the Facility between RHMW01 and th e US Navy Well 2254-01 to better monitor the quality of the groundwater moving from the Facility to the US Navy Well 2254-01. Although the results from the groundwater sa mple collected from US Navy Well 2254-01 in October 2008 showed trace concen trations of naphthalene and 1-methylnaphthalene, no other petroleum constituents were detected in this sample. This well was re-sampled in December 2008. The sample was analyzed by USEPA Method 8620B and no petroleum constituents were detected.
It is recommended that RHMW01, RHMW02, RH MW03, and RHMW05 be evaluated monthly for the presence of fuel on groundwater, in accord ance with the Plan. The US Navy plans to install dedicated oil/water interface probes in each of these wells to facilitate these measurements.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 19 It is also recommended that quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and lead be continued as previously sche duled until new data indicates that a different schedule is required. The quarterly collection an d analysis of groundwater samples will continue to monitor the quality of the groundwater located beneath the Facility. Groundwater monitoring reports will be submitted to the HDOH upon receipt and evaluation of la boratory analytical results.10000TPHatRHMW02QuarterlyMonitoringResults10000TPHatRHMW03QuarterlyMonitoringResults1000
(μg/L)1000

μ g/L)100

Concentration100

Concentration ( μ1010Time(Date)GROEALTPH‐DROTPH‐GROTPH‐GROMDLSSRBLDROEALTime(Date)GROEALTPH‐DROTPH‐GROMDLTPH‐DROMDLSSRBLDROEAL10000TPHatRHMW01QuarterlyMonitoringResults1000

ation (μg/L)100

Concentr10Time(Date)GROEALTPH‐DROTPH‐GROMDLTPH‐GROSSRBLDROEALFigure1TPHTrendsinGroundwaterRound13(October22,2008)RedHillFuelStorageFacilityThe HDOH toxicity EALs were updated in Fall, 2008.•TPH-DRO Residential Tap Water EAL is 210 ug/L; and•TPH-GRO Residential Tap Water EAL is 100 ug/L;(HDOH 2008)g yOahu,Hawaii(HDOH,2008).1000PAHsatRHMW02QuarterlyMonitoringResults100100010

t ration (μg/L)1

Concen t0.1Time(Date)Naphthalene1‐Methylnaphthalene2‐MethylnaphthaleneNaphEAL*1‐MethEAL*2‐MethEAL*Figure2PAHTrendsinGroundwaterRound13(October22,2008)RedHillFuelStorageFacilityThe HDOH toxicity EALs were updated in Fall, 2008.• Naphthalene Residential Tap Water EAL is 17 ug/L;• 1-methylnaphthalene Residential Tap Water EAL is 4.7 ug/L; and• 2- methylnaphthalene Residential Tap Water EAL is 24 ug/L(HDOH 2008)g yOahu,Hawaii(HDOH,2008).

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility February 2009

____________________________________________________________________________________________



## 22 

# 5.0 References AMEC. 2002. Red Hill Bulk Fuel Storage Facility Investigation Report , Prepared for NAVFAC Pacific, August 2002. Dawson Group, Inc. 2006. Fourth Quarter 2005 Groundwater Sam pling Report, Red Hill Fuel Storage Facility, Hawaii. February 2006.
Hawaii Administrative Rules, Titl e 11, Chapter 281, Subchapter 7. State of Hawaii Department of Health (HDOH). 2005. Screening for Envir onmental Concerns at Sites with Contaminated Soil and Groundwater, Volume 1: Summary Tier 1 Lookup Tables. Interim Final. May 2005. State of Hawaii Department of Health. 2005a. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underg round Storage Tank Sites . Memo. 15 July.

HDOH. 2008. Evaluation of Environmental Hazards at Sites With Contaminated Soil and Groundwater . Summer 2008 (updated October 2008). The Environmental Company, Inc. and AMEC. 2005. Red Hill Bulk Fuel Storage Facility Work Plan, Pearl Harbor, Hawaii. June.

TEC Inc. 2006. Red Hill Bulk Fuel Storage Facility , Final – Addendum Planning Documents, Pearl Harbor, Hawaii. May.

TEC Inc. 2007. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, Hawaii . August.

TEC Inc. 2008. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl Harbor, Hawaii. January.

# Appendix A Laboratory Analytical Reports

## SGS Work Order:

Contents:
Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS Environmental Services Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 9121-003 Red Hill BFSF The Environmental Company, Inc. (TEC) 1085813

# Case Narrative THEENVC The Environmenta l Company, Inc. (TEC) 1085813 9121-003 Red Hill BFSF Customer: Project: NPDL WO: 

# SGS Environmental Services Inc.

Refer to the sample receipt form for information on sample condition. 

### 1085813001 PS RHMW2254-WG13 8015C DRO - LCS recovery is outside of acceptance criteria (biased low). The sample wa s re-extracted outside of the 14 day holding time and reanalyzed. The results did confirm with passing QC. Results for all associated samples are considered estimated. 

### 1085813004 PS RHMW03-WG13 8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy. 

### 1085813005 PS RHMW02-WG13 8015C DRO - The pattern is consistent with a weathered middle distillate. 8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy. 

### 1085813006 PS RHMWA01-WG13 8015C DRO - The pattern is consistent with a weathered middle distillate. 8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy. 

### 1085813007 PS RHMW01-WG13 8015C DRO - Unknown hydrocarbon with several peaks is present. 8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy. 

### 1085813002 BMS RHMW2254-WG13 MS 8015C DRO - LCS recovery is outside of acceptance criteria (biased low). The sample wa s re-extracted outside of the 14 day holding time and reanalyzed. The results did confirm with passing QC. Results for all associated samples are considered estimated. 

### 868545 MS 1085813001MS 8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy. 

### 1085813003 BMSD RHMW2254-WG13 MSD 8015C DRO - LCS recovery is outside of acceptance criteria (biased low). The sample wa s re-extracted outside of the 14 day holding time and reanalyzed. The results did confirm with passing QC. Results for all associated samples are considered estimated. 

### 868546 MSD 1085813001MSD 8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy. 

### 869198 LCS XXX/20313 ] 8015C DRO - LCS recovery is outside of acceptance criter ia (biased low). Results for all associated samples are considered estimated.

# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1085813

Certification:
I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1001 Bishop Street Ste 1400 ASB Tower Honolulu, HI 96813
Attn: Jeff Hart T: (808)528-1445 F:(808)528-0768 jshart@tecinc.com

Tamara Rentz tamara.rentz@sgs.com Project Manager 

### 9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roupEnclosed are the analytical results associated with this workorder.
As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).
Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.
If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 907-562-2343.
The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit PQL Practical Quantitation Limit (reporting limit). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indicates value that is greater than or equal to the MDL. J The quantitation is an estimation. ND Indicates the analyte is not detected B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits. D The analyte concentration is the result of dilution. GT Greater Than LT Less Than Q QC parameter out of acceptance range. M A matrix effect was present. E The analyte result is above the calibrated range. R Rejected DF Analytical Dilution Factor JL The analyte was positively identified, but the quantitation is a low estimation. <Surr> Surrogate QC spiked standard <Surr/IS> Surrogate / Internal Standard QC spiked standard QC Quality Control QA Quality Assurance MB Method Blank LCS (D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) BMS(D) Site Specific Matrix Spike RPD Relative Percent Difference ICV Initial Calibration Verification CCV Continuous Calibration Verification MSA Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified Print Date: 11/20/2008

Notes: All DRO/RRO analysese are integrated per SOP.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of SG S G roup

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 9121-003 Red Hill BFSF Workorder No.: 1085813 

## Analytical Methods

Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS AFCEE 3.1 8260 (W) SW8260B Dissolved Metals by ICP-MS SW6020 DRO by 8015B (W) SW8015C GRO (W) SW8015C Print Date: 11/20/2008



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1085813001 RHMW2254-WG13 1085813002 RHMW2254-WG13 MS 1085813003 RHMW2254-WG13 MSD 1085813004 RHMW03-WG13 1085813005 RHMW02-WG13 1085813006 RHMWA01-WG13 1085813007 RHMW01-WG13 1085813008 TB01-WG13

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of SG S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW2254-WG13 SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5719 MXX21031 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5719 Analytical Method: SW6020 Analysis Date/Time: 11/14/08 20:12 Prep Batch: MXX21031 Prep Method: SW3010A Prep Date/Time: 11/04/08 18:15 Container ID:1085813001-G Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW2254-WG13 SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 ug/L VFC9248 VXX18967 10.0 1 4-Bromofluorobenzene <surr> 99.1 50-150 % VFC9248 VXX18967 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9248 Analytical Method: SW8015C Analysis Date/Time: 10/30/08 10:09 Prep Batch: VXX18967 Prep Method: SW5030B Prep Date/Time: 10/30/08 08:00 Container ID:1085813001-A Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW2254-WG13 SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.421 mg/L XFC8338 XXX20313 0.0842 1 5a Androstane <surr> 93.1 50-150 % XFC8338 XXX20313 1

Batch Information Initial Prep Wt./Vol.: 950 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8338 Analytical Method: SW8015C Analysis Date/Time: 11/05/08 09:36 Prep Batch: XXX20313 Prep Method: SW3520C Prep Date/Time: 11/03/08 17:15 Container ID:1085813001-I Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW2254-WG13 SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10242 VXX18954 0.120 1 Toluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Styrene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromomethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Acetone ND 10.0 ug/L VMS10242 VXX18954 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10242 VXX18954 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10242 VXX18954 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 Chloroform ND 1.00 ug/L VMS10242 VXX18954 0.300 1 Bromobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromomethane ND 3.00 ug/L VMS10242 VXX18954 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW2254-WG13 SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 Methylene chloride ND 5.00 ug/L VMS10242 VXX18954 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Naphthalene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 o-Xylene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromoform ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Trichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloroethane-D4 <surr> 105 73-120 % VMS10242 VXX18954 1 Toluene-d8 <surr> 104 80-120 % VMS10242 VXX18954 1 4-Bromofluorobenzene <surr> 111 76-120 % VMS10242 VXX18954 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10242 Analytical Method: SW8260B Analysis Date/Time: 10/27/08 17:17 Prep Batch: VXX18954 Prep Method: SW5030B Prep Date/Time: 10/27/08 11:41 Container ID:1085813001-D Dilution Factor: 1 Analyst: JDB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW2254-WG13 SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Acenaphthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Fluorene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Phenanthrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo(a)Anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Chrysene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[b]Fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[k]fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[a]pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Dibenzo[a,h]anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[g,h,i]perylene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Naphthalene 0.0466 J 0.100 ug/L XMS4761 XXX20276 0.0310 1 1-Methylnaphthalene 0.0276 J 0.0500 ug/L XMS4761 XXX20276 0.0150 1 2-Methylnaphthalene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Terphenyl-d14 <surr> 92.2 50-135 % XMS4761 XXX20276 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4761 Analytical Method: 8270D SIMS Analysis Date/Time: 10/30/08 14:48 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813001-J Dilution Factor: 1 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW03-WG13 SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5719 MXX21031 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5719 Analytical Method: SW6020 Analysis Date/Time: 11/14/08 22:05 Prep Batch: MXX21031 Prep Method: SW3010A Prep Date/Time: 11/04/08 18:15 Container ID:1085813004-G Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW03-WG13 SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 ug/L VFC9248 VXX18967 10.0 1 4-Bromofluorobenzene <surr> 94.8 50-150 % VFC9248 VXX18967 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9248 Analytical Method: SW8015C Analysis Date/Time: 10/30/08 11:18 Prep Batch: VXX18967 Prep Method: SW5030B Prep Date/Time: 10/30/08 08:00 Container ID:1085813004-A Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW03-WG13 SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.244 J 0.442 mg/L XFC8323 XXX20290 0.0884 1 5a Androstane <surr> 101 50-150 % XFC8323 XXX20290 1

Batch Information Initial Prep Wt./Vol.: 905 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8323 Analytical Method: SW8015C Analysis Date/Time: 10/31/08 12:33 Prep Batch: XXX20290 Prep Method: SW3520C Prep Date/Time: 10/29/08 18:00 Container ID:1085813004-H Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW03-WG13 SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10242 VXX18954 0.120 1 Toluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Styrene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromomethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Acetone ND 10.0 ug/L VMS10242 VXX18954 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10242 VXX18954 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10242 VXX18954 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 Chloroform ND 1.00 ug/L VMS10242 VXX18954 0.300 1 Bromobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromomethane ND 3.00 ug/L VMS10242 VXX18954 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW03-WG13 SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 Methylene chloride ND 5.00 ug/L VMS10242 VXX18954 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Naphthalene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 o-Xylene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromoform ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Trichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloroethane-D4 <surr> 104 73-120 % VMS10242 VXX18954 1 Toluene-d8 <surr> 103 80-120 % VMS10242 VXX18954 1 4-Bromofluorobenzene <surr> 113 76-120 % VMS10242 VXX18954 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10242 Analytical Method: SW8260B Analysis Date/Time: 10/27/08 17:50 Prep Batch: VXX18954 Prep Method: SW5030B Prep Date/Time: 10/27/08 11:41 Container ID:1085813004-D Dilution Factor: 1 Analyst: JDB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW03-WG13 SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Acenaphthene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Fluorene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Phenanthrene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Anthracene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Fluoranthene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Pyrene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Benzo(a)Anthracene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Chrysene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Benzo[b]Fluoranthene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Benzo[k]fluoranthene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Benzo[a]pyrene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Indeno[1,2,3-c,d] pyrene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Dibenzo[a,h]anthracene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Benzo[g,h,i]perylene ND 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Naphthalene 0.219 0.103 ug/L XMS4761 XXX20276 0.0320 1 1-Methylnaphthalene 0.0658 0.0515 ug/L XMS4761 XXX20276 0.0155 1 2-Methylnaphthalene 0.0937 0.0515 ug/L XMS4761 XXX20276 0.0155 1 Terphenyl-d14 <surr> 89.4 50-135 % XMS4761 XXX20276 1

Batch Information Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4761 Analytical Method: 8270D SIMS Analysis Date/Time: 10/30/08 16:29 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813004-J Dilution Factor: 1 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5719 MXX21031 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5719 Analytical Method: SW6020 Analysis Date/Time: 11/14/08 22:12 Prep Batch: MXX21031 Prep Method: SW3010A Prep Date/Time: 11/04/08 18:15 Container ID:1085813005-G Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics 52.8 J 100 ug/L VFC9248 VXX18967 10.0 1 4-Bromofluorobenzene <surr> 129 50-150 % VFC9248 VXX18967 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9248 Analytical Method: SW8015C Analysis Date/Time: 10/30/08 11:36 Prep Batch: VXX18967 Prep Method: SW5030B Prep Date/Time: 10/30/08 08:00 Container ID:1085813005-A Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 4.54 0.400 mg/L XFC8323 XXX20290 0.0800 1 5a Androstane <surr> 97.8 50-150 % XFC8323 XXX20290 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8323 Analytical Method: SW8015C Analysis Date/Time: 10/31/08 12:42 Prep Batch: XXX20290 Prep Method: SW3520C Prep Date/Time: 10/29/08 18:00 Container ID:1085813005-H Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.140 J 0.400 ug/L VMS10242 VXX18954 0.120 1 Toluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Ethylbenzene 0.450 J 1.00 ug/L VMS10242 VXX18954 0.310 1 n-Butylbenzene 9.65 1.00 ug/L VMS10242 VXX18954 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 n-Propylbenzene 12.4 1.00 ug/L VMS10242 VXX18954 0.310 1 Styrene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromomethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Acetone ND 10.0 ug/L VMS10242 VXX18954 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10242 VXX18954 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10242 VXX18954 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 Chloroform ND 1.00 ug/L VMS10242 VXX18954 0.300 1 Bromobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromomethane ND 3.00 ug/L VMS10242 VXX18954 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 sec-Butylbenzene 8.48 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 Methylene chloride ND 5.00 ug/L VMS10242 VXX18954 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Naphthalene 239 40.0 ug/L VMS10254 VXX18976 12.4 20 o-Xylene 0.450 J 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromoform ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 tert-Butylbenzene 1.29 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Trichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Isopropylbenzene (Cumene) 6.64 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloroethane-D4 <surr> 104 73-120 % VMS10242 VXX18954 1 Toluene-d8 <surr> 104 80-120 % VMS10242 VXX18954 1 4-Bromofluorobenzene <surr> 104 76-120 % VMS10242 VXX18954 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10242 Analytical Method: SW8260B Analysis Date/Time: 10/27/08 18:24 Prep Batch: VXX18954 Prep Method: SW5030B Prep Date/Time: 10/27/08 11:41 Container ID:1085813005-E Dilution Factor: 1 Analyst: JDB Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10254 Analytical Method: SW8260B Analysis Date/Time: 10/31/08 08:38 Prep Batch: VXX18976 Prep Method: SW5030B Prep Date/Time: 10/31/08 01:28 Container ID:1085813005-C Dilution Factor: 20 Analyst: DSH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW02-WG13 SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Acenaphthene 0.365 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Fluorene 0.214 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Phenanthrene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Anthracene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Fluoranthene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Pyrene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Benzo(a)Anthracene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Chrysene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Benzo[b]Fluoranthene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Benzo[k]fluoranthene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Benzo[a]pyrene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Indeno[1,2,3-c,d] pyrene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Dibenzo[a,h]anthracene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Benzo[g,h,i]perylene ND 0.0521 ug/L XMS4761 XXX20276 0.0156 1 Naphthalene 97.4 5.21 ug/L XMS4763 XXX20276 1.61 50 1-Methylnaphthalene 72.1 2.60 ug/L XMS4763 XXX20276 0.781 50 2-Methylnaphthalene 13.7 1.04 ug/L XMS4763 XXX20276 0.313 20 Terphenyl-d14 <surr> 89.6 50-135 % XMS4761 XXX20276 1

Batch Information Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4761 Analytical Method: 8270D SIMS Analysis Date/Time: 10/30/08 17:02 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813005-J Dilution Factor: 1 Analyst: JDH Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4763 Analytical Method: 8270D SIMS Analysis Date/Time: 10/31/08 11:49 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813005-J Dilution Factor: 20 Analyst: JDH Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4763 Analytical Method: 8270D SIMS Analysis Date/Time: 10/31/08 15:57 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813005-J Dilution Factor: 50 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5719 MXX21031 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5719 Analytical Method: SW6020 Analysis Date/Time: 11/14/08 22:19 Prep Batch: MXX21031 Prep Method: SW3010A Prep Date/Time: 11/04/08 18:15 Container ID:1085813006-G Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics 52.9 J 100 ug/L VFC9248 VXX18967 10.0 1 4-Bromofluorobenzene <surr> 130 50-150 % VFC9248 VXX18967 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9248 Analytical Method: SW8015C Analysis Date/Time: 10/30/08 11:54 Prep Batch: VXX18967 Prep Method: SW5030B Prep Date/Time: 10/30/08 08:00 Container ID:1085813006-A Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 6.30 0.491 mg/L XFC8323 XXX20290 0.0982 1 5a Androstane <surr> 104 50-150 % XFC8323 XXX20290 1

Batch Information Initial Prep Wt./Vol.: 815 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8323 Analytical Method: SW8015C Analysis Date/Time: 10/31/08 12:52 Prep Batch: XXX20290 Prep Method: SW3520C Prep Date/Time: 10/29/08 18:00 Container ID:1085813006-H Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.150 J 0.400 ug/L VMS10242 VXX18954 0.120 1 Toluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Ethylbenzene 0.420 J 1.00 ug/L VMS10242 VXX18954 0.310 1 n-Butylbenzene 9.47 1.00 ug/L VMS10242 VXX18954 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 n-Propylbenzene 12.5 1.00 ug/L VMS10242 VXX18954 0.310 1 Styrene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromomethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Acetone ND 10.0 ug/L VMS10242 VXX18954 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10242 VXX18954 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10242 VXX18954 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 Chloroform ND 1.00 ug/L VMS10242 VXX18954 0.300 1 Bromobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromomethane ND 3.00 ug/L VMS10242 VXX18954 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 sec-Butylbenzene 8.57 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 Methylene chloride ND 5.00 ug/L VMS10242 VXX18954 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Naphthalene 245 40.0 ug/L VMS10254 VXX18976 12.4 20 o-Xylene 0.490 J 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromoform ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 tert-Butylbenzene 1.31 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Trichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Isopropylbenzene (Cumene) 6.48 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS10242 VXX18954 1 Toluene-d8 <surr> 103 80-120 % VMS10242 VXX18954 1 4-Bromofluorobenzene <surr> 105 76-120 % VMS10242 VXX18954 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10242 Analytical Method: SW8260B Analysis Date/Time: 10/27/08 18:58 Prep Batch: VXX18954 Prep Method: SW5030B Prep Date/Time: 10/27/08 11:41 Container ID:1085813006-D Dilution Factor: 1 Analyst: JDB Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10254 Analytical Method: SW8260B Analysis Date/Time: 10/31/08 09:09 Prep Batch: VXX18976 Prep Method: SW5030B Prep Date/Time: 10/31/08 01:28 Container ID:1085813006-C Dilution Factor: 20 Analyst: DSH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMWA01-WG13 SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Acenaphthene 0.208 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Fluorene 0.122 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Phenanthrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo(a)Anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Chrysene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[b]Fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[k]fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[a]pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Dibenzo[a,h]anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[g,h,i]perylene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Naphthalene 82.3 5.00 ug/L XMS4763 XXX20276 1.55 50 1-Methylnaphthalene 62.4 2.50 ug/L XMS4763 XXX20276 0.750 50 2-Methylnaphthalene 12.7 1.00 ug/L XMS4763 XXX20276 0.300 20 Terphenyl-d14 <surr> 87.7 50-135 % XMS4761 XXX20276 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4761 Analytical Method: 8270D SIMS Analysis Date/Time: 10/30/08 17:36 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813006-J Dilution Factor: 1 Analyst: JDH Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4763 Analytical Method: 8270D SIMS Analysis Date/Time: 10/31/08 12:22 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813006-J Dilution Factor: 20 Analyst: JDH Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4763 Analytical Method: 8270D SIMS Analysis Date/Time: 10/31/08 16:31 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813006-J Dilution Factor: 50 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 ug/L VFC9248 VXX18967 10.0 1 4-Bromofluorobenzene <surr> 92.5 50-150 % VFC9248 VXX18967 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9248 Analytical Method: SW8015C Analysis Date/Time: 10/30/08 12:12 Prep Batch: VXX18967 Prep Method: SW5030B Prep Date/Time: 10/30/08 08:00 Container ID:1085813007-A Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.459 0.412 mg/L XFC8323 XXX20290 0.0825 1 5a Androstane <surr> 103 50-150 % XFC8323 XXX20290 1

Batch Information Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8323 Analytical Method: SW8015C Analysis Date/Time: 10/31/08 13:01 Prep Batch: XXX20290 Prep Method: SW3520C Prep Date/Time: 10/29/08 18:00 Container ID:1085813007-H Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10242 VXX18954 0.120 1 Toluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Styrene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromomethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Acetone ND 10.0 ug/L VMS10242 VXX18954 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10242 VXX18954 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10242 VXX18954 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 Chloroform ND 1.00 ug/L VMS10242 VXX18954 0.300 1 Bromobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromomethane ND 3.00 ug/L VMS10242 VXX18954 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 Methylene chloride ND 5.00 ug/L VMS10242 VXX18954 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Naphthalene ND 2.00 ug/L VMS10254 VXX18976 0.620 1 o-Xylene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromoform ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Trichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS10242 VXX18954 1 Toluene-d8 <surr> 104 80-120 % VMS10242 VXX18954 1 4-Bromofluorobenzene <surr> 109 76-120 % VMS10242 VXX18954 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10242 Analytical Method: SW8260B Analysis Date/Time: 10/27/08 19:31 Prep Batch: VXX18954 Prep Method: SW5030B Prep Date/Time: 10/27/08 11:41 Container ID:1085813007-D Dilution Factor: 1 Analyst: JDB Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10254 Analytical Method: SW8260B Analysis Date/Time: 10/31/08 07:36 Prep Batch: VXX18976 Prep Method: SW5030B Prep Date/Time: 10/31/08 01:28 Container ID:1085813007-F Dilution Factor: 1 Analyst: DSH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Acenaphthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Fluorene 0.0207 J 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Phenanthrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo(a)Anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Chrysene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[b]Fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[k]fluoranthene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[a]pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Dibenzo[a,h]anthracene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Benzo[g,h,i]perylene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Naphthalene 0.103 0.100 ug/L XMS4761 XXX20276 0.0310 1 1-Methylnaphthalene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 2-Methylnaphthalene ND 0.0500 ug/L XMS4761 XXX20276 0.0150 1 Terphenyl-d14 <surr> 91.1 50-135 % XMS4761 XXX20276 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4761 Analytical Method: 8270D SIMS Analysis Date/Time: 10/30/08 18:09 Prep Batch: XXX20276 Prep Method: SW3520C Prep Date/Time: 10/28/08 10:10 Container ID:1085813007-J Dilution Factor: 1 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### TB01-WG13 SGS Ref. #: 1085813008 Collection Date/Time: 10/22/08 08:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10242 VXX18954 0.120 1 Toluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10242 VXX18954 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Styrene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromomethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Acetone ND 10.0 ug/L VMS10242 VXX18954 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10242 VXX18954 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10242 VXX18954 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 Chloroform ND 1.00 ug/L VMS10242 VXX18954 0.300 1 Bromobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Chloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromomethane ND 3.00 ug/L VMS10242 VXX18954 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)

### The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: 

### TB01-WG13 SGS Ref. #: 1085813008 Collection Date/Time: 10/22/08 08:05 Receipt Date/Time: 10/24/08 10:50 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10242 VXX18954 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10242 VXX18954 3.10 1 Methylene chloride ND 5.00 ug/L VMS10242 VXX18954 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 Naphthalene ND 2.00 ug/L VMS10242 VXX18954 0.620 1 o-Xylene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Bromoform ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Trichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10242 VXX18954 0.310 1 1,2-Dichloroethane-D4 <surr> 105 73-120 % VMS10242 VXX18954 1 Toluene-d8 <surr> 106 80-120 % VMS10242 VXX18954 1 4-Bromofluorobenzene <surr> 112 76-120 % VMS10242 VXX18954 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10242 Analytical Method: SW8260B Analysis Date/Time: 10/27/08 16:09 Prep Batch: VXX18954 Prep Method: SW5030B Prep Date/Time: 10/27/08 11:41 Container ID:1085813008-A Dilution Factor: 1 Analyst: JDB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 867629 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18954 SW5030B 10/27/2008 QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006, 1085813007, 1085813008

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene ND 0.400 ug/L 10/27/08 

### 0.120 Toluene ND 1.00 ug/L 10/27/08 

### 0.310 Ethylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 n-Butylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 1,4-Dichlorobenzene ND 0.500 ug/L 10/27/08 

### 0.150 1,2-Dichloroethane ND 0.500 ug/L 10/27/08 

### 0.150 1,3,5-Trimethylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 4-Chlorotoluene ND 1.00 ug/L 10/27/08 

### 0.310 Chlorobenzene ND 0.500 ug/L 10/27/08 

### 0.150 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 10/27/08 

### 3.10 cis-1,2-Dichloroethene ND 1.00 ug/L 10/27/08 

### 0.310 4-Isopropyltoluene ND 1.00 ug/L 10/27/08 

### 0.310 cis-1,3-Dichloropropene ND 0.500 ug/L 10/27/08 

### 0.150 n-Propylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 Styrene ND 1.00 ug/L 10/27/08 

### 0.310 Dibromomethane ND 1.00 ug/L 10/27/08 

### 0.310 trans-1,3-Dichloropropene ND 1.00 ug/L 10/27/08 

### 0.310 1,2,4-Trichlorobenzene ND 1.00 ug/L 10/27/08 

### 0.310 Acetone ND 10.0 ug/L 10/27/08 

### 3.10 1,1,2,2-Tetrachloroethane ND 0.500 ug/L 10/27/08 

### 0.150 1,2-Dibromo-3-chloropropane ND 2.00 ug/L 10/27/08 

### 0.620 Methyl-t-butyl ether ND 5.00 ug/L 10/27/08 

### 1.50 Tetrachloroethene ND 1.00 ug/L 10/27/08 

### 0.310 Dibromochloromethane ND 0.500 ug/L 10/27/08 

### 0.150 1,3-Dichloropropane ND 0.400 ug/L 10/27/08 

### 0.120 1,2-Dibromoethane ND 1.00 ug/L 10/27/08 

### 0.310 Carbon tetrachloride ND 1.00 ug/L 10/27/08 

### 0.310 1,1,1,2-Tetrachloroethane ND 0.500 ug/L 10/27/08 

### 0.150 Chloroform ND 1.00 ug/L 10/27/08 

### 0.300 Bromobenzene ND 1.00 ug/L 10/27/08 

### 0.310 Chloromethane ND 1.00 ug/L 10/27/08 

### 0.310 1,2,3-Trichloropropane ND 1.00 ug/L 10/27/08 

### 0.310 Bromomethane ND 3.00 ug/L 10/27/08 

### 0.940 Bromochloromethane ND 1.00 ug/L 10/27/08 

### 0.310 Vinyl chloride ND 1.00 ug/L 10/27/08 

### 0.310 Dichlorodifluoromethane ND 1.00 ug/L 10/27/08 

### 0.310Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 867629 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18954 SW5030B 10/27/2008

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Chloroethane ND 1.00 ug/L 10/27/08 

### 0.310 sec-Butylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 Bromodichloromethane ND 0.500 ug/L 10/27/08 

### 0.150 1,1-Dichloroethene ND 1.00 ug/L 10/27/08 

### 0.310 2-Butanone (MEK) ND 10.0 ug/L 10/27/08 

### 3.10 Methylene chloride ND 5.00 ug/L 10/27/08 

### 1.00 Trichlorofluoromethane ND 1.00 ug/L 10/27/08 

### 0.310 P & M -Xylene ND 2.00 ug/L 10/27/08 

### 0.620 Naphthalene ND 2.00 ug/L 10/27/08 

### 0.620 o-Xylene ND 1.00 ug/L 10/27/08 

### 0.310 Bromoform ND 1.00 ug/L 10/27/08 

### 0.310 1-Chlorohexane ND 1.00 ug/L 10/27/08 

### 0.310 1,2,4-Trimethylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 tert-Butylbenzene ND 1.00 ug/L 10/27/08 

### 0.310 1,1,1-Trichloroethane ND 1.00 ug/L 10/27/08 

### 0.310 1,1-Dichloroethane ND 1.00 ug/L 10/27/08 

### 0.310 2-Chlorotoluene ND 1.00 ug/L 10/27/08 

### 0.310 Trichloroethene ND 1.00 ug/L 10/27/08 

### 0.310 trans-1,2-Dichloroethene ND 1.00 ug/L 10/27/08 

### 0.310 1,2-Dichlorobenzene ND 1.00 ug/L 10/27/08 

### 0.310 2,2-Dichloropropane ND 1.00 ug/L 10/27/08 

### 0.310 Hexachlorobutadiene ND 1.00 ug/L 10/27/08 

### 0.310 Isopropylbenzene (Cumene) ND 1.00 ug/L 10/27/08 

### 0.310 1,2-Dichloropropane ND 1.00 ug/L 10/27/08 

### 0.310 1,1-Dichloropropene ND 1.00 ug/L 10/27/08 

### 0.310 1,1,2-Trichloroethane ND 1.00 ug/L 10/27/08 

### 0.310 1,3-Dichlorobenzene ND 1.00 ug/L 10/27/08 

### 0.310 1,2,3-Trichlorobenzene ND 1.00 ug/L 10/27/08 

### 0.310
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 102 73-120 % 10/27/08 

### Toluene-d8 <surr> 105 80-120 % 10/27/08 

### 4-Bromofluorobenzene <surr> 109 76-120 % 10/27/08

Instrument Method Batch VMS10242

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 867655 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20276 SW3520C 10/28/2008 QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Polynuclear Aromatics GC/MS


### Acenaphthylene ND 0.0500 ug/L 10/30/08 

### 0.0150 Acenaphthene ND 0.0500 ug/L 10/30/08 

### 0.0150 Fluorene ND 0.0500 ug/L 10/30/08 

### 0.0150 Phenanthrene ND 0.0500 ug/L 10/30/08 

### 0.0150 Anthracene ND 0.0500 ug/L 10/30/08 

### 0.0150 Fluoranthene ND 0.0500 ug/L 10/30/08 

### 0.0150 Pyrene ND 0.0500 ug/L 10/30/08 

### 0.0150 Benzo(a)Anthracene ND 0.0500 ug/L 10/30/08 

### 0.0150 Chrysene ND 0.0500 ug/L 10/30/08 

### 0.0150 Benzo[b]Fluoranthene ND 0.0500 ug/L 10/30/08 

### 0.0150 Benzo[k]fluoranthene ND 0.0500 ug/L 10/30/08 

### 0.0150 Benzo[a]pyrene ND 0.0500 ug/L 10/30/08 

### 0.0150 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L 10/30/08 

### 0.0150 Dibenzo[a,h]anthracene ND 0.0500 ug/L 10/30/08 

### 0.0150 Benzo[g,h,i]perylene ND 0.0500 ug/L 10/30/08 

### 0.0150 Naphthalene ND 0.100 ug/L 10/30/08 

### 0.0310 1-Methylnaphthalene ND 0.0500 ug/L 10/30/08 

### 0.0150 2-Methylnaphthalene ND 0.0500 ug/L 10/30/08 

### 0.0150
Surrogates 

### Terphenyl-d14 <surr> 88.5 50-135 % 10/30/08

Instrument Method Batch XMS4761

8270D SIMS HP 5890 Series II MS2 SVOAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 868151 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20290 SW3520C 10/29/2008 QC results affect the following production samples: 

### 1085813004, 1085813005, 1085813006, 1085813007

Parameter Results Reporting/Control Limit Units Analysis Date MDL



### Semivolatile Organic Fuels Department


### Diesel Range Organics ND 0.400 mg/L 10/31/08 

### 0.0800
Surrogates


### 5a Androstane <surr> 104 60-120 % 10/31/08

Instrument Method Batch XFC8323

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 868324 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18967 SW5030B 10/30/2008 QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter Results Reporting/Control Limit Units Analysis Date MDL



### Volatile Fuels Department


### Gasoline Range Organics ND 100 ug/L 10/30/08 

### 10.0
Surrogates


### 4-Bromofluorobenzene <surr> 94.9 50-150 % 10/30/08

Instrument Method Batch VFC9248

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 868746 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18976 SW5030B 10/31/2008 QC results affect the following production samples: 

### 1085813005, 1085813006, 1085813007

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy


### Naphthalene ND 2.00 ug/L 10/31/08 

### 0.620
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 102 73-120 % 10/31/08 

### Toluene-d8 <surr> 100 80-120 % 10/31/08 

### 4-Bromofluorobenzene <surr> 101 76-120 % 10/31/08

Instrument Method Batch VMS10254

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 869197 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20313 SW3520C 11/03/2008 QC results affect the following production samples: 

### 1085813001

Parameter Results Reporting/Control Limit Units Analysis Date MDL



### Semivolatile Organic Fuels Department


### Diesel Range Organics ND 0.400 mg/L 11/05/08 

### 0.0800
Surrogates


### 5a Androstane <surr> 97.3 60-120 % 11/05/08

Instrument Method Batch XFC8338

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Prep 

### 869581 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX21031 SW3010A 11/04/2008 QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Metals by ICP/MS



### Lead ND 1.00 ug/L 11/14/08 

### 0.310

Instrument Method Batch MMS5719

SW6020 Perkin Elmer Sciex ICP-MS P4Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867630 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18954 SW5030B 10/27/2008

QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006, 1085813007, 1085813008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene LCS 27.9 93 ( 80-120 ) 30 ug/L 10/27/2008

Toluene LCS 29.5 98 ( 77-120 ) 30 ug/L 10/27/2008
Ethylbenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 10/27/2008
n-Butylbenzene LCS 30.2 101 ( 80-124 ) 30 ug/L 10/27/2008

1,4-Dichlorobenzene LCS 29.5 98 ( 80-120 ) 30 ug/L 10/27/2008

1,2-Dichloroethane LCS 28.4 95 ( 80-129 ) 30 ug/L 10/27/2008
1,3,5-Trimethylbenzene LCS 32.7 109 ( 80-128 ) 30 ug/L 10/27/2008

4-Chlorotoluene LCS 31.3 104 ( 79-128 ) 30 ug/L 10/27/2008

Chlorobenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 10/27/2008
4-Methyl-2-pentanone (MIBK) LCS 83.7 93 ( 69-134 ) 90 ug/L 10/27/2008

cis-1,2-Dichloroethene LCS 29.3 98 ( 80-125 ) 30 ug/L 10/27/2008
4-Isopropyltoluene LCS 31.8 106 ( 80-125 ) 30 ug/L 10/27/2008
cis-1,3-Dichloropropene LCS 30.2 101 ( 80-120 ) 30 ug/L 10/27/2008
n-Propylbenzene LCS 31.6 105 ( 80-129 ) 30 ug/L 10/27/2008
Styrene LCS 31.7 106 ( 80-120 ) 30 ug/L 10/27/2008

Dibromomethane LCS 29.4 98 ( 80-120 ) 30 ug/L 10/27/2008
trans-1,3-Dichloropropene LCS 32.1 107 ( 80-124 ) 30 ug/L 10/27/2008

1,2,4-Trichlorobenzene LCS 29.0 97 ( 80-120 ) 30 ug/L 10/27/2008

Acetone LCS 81.6 91 ( 50-135 ) 90 ug/L 10/27/2008

1,1,2,2-Tetrachloroethane LCS 30.3 101 ( 76-123 ) 30 ug/L 10/27/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867630 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18954 SW5030B 10/27/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dibromo-3-chloropropane LCS 34.1 114 ( 73-130 ) 30 ug/L 10/27/2008
Methyl-t-butyl ether LCS 45.0 100 ( 80-120 ) 45 ug/L 10/27/2008

Tetrachloroethene LCS 29.6 99 ( 79-122 ) 30 ug/L 10/27/2008

Dibromochloromethane LCS 31.8 106 ( 80-120 ) 30 ug/L 10/27/2008
1,3-Dichloropropane LCS 30.7 102 ( 80-121 ) 30 ug/L 10/27/2008

1,2-Dibromoethane LCS 31.3 104 ( 80-120 ) 30 ug/L 10/27/2008

Carbon tetrachloride LCS 30.7 102 ( 80-126 ) 30 ug/L 10/27/2008

1,1,1,2-Tetrachloroethane LCS 31.9 106 ( 80-120 ) 30 ug/L 10/27/2008

Chloroform LCS 29.8 99 ( 80-124 ) 30 ug/L 10/27/2008

Bromobenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 10/27/2008

Chloromethane LCS 28.6 95 ( 67-125 ) 30 ug/L 10/27/2008
1,2,3-Trichloropropane LCS 30.2 101 ( 80-120 ) 30 ug/L 10/27/2008

Bromomethane LCS 31.6 105 ( 30-140 ) 30 ug/L 10/27/2008

Bromochloromethane LCS 30.5 102 ( 77-129 ) 30 ug/L 10/27/2008
Vinyl chloride LCS 28.8 96 ( 72-145 ) 30 ug/L 10/27/2008

Dichlorodifluoromethane LCS 27.5 92 ( 62-153 ) 30 ug/L 10/27/2008

Chloroethane LCS 28.4 95 ( 67-133 ) 30 ug/L 10/27/2008
sec-Butylbenzene LCS 32.3 108 ( 80-120 ) 30 ug/L 10/27/2008

Bromodichloromethane LCS 31.8 106 ( 80-120 ) 30 ug/L 10/27/2008

1,1-Dichloroethene LCS 29.5 98 ( 76-130 ) 30 ug/L 10/27/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867630 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18954 SW5030B 10/27/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) LCS 84.4 94 ( 66-136 ) 90 ug/L 10/27/2008
Methylene chloride LCS 30.2 101 ( 63-131 ) 30 ug/L 10/27/2008

Trichlorofluoromethane LCS 30.0 100 ( 68-145 ) 30 ug/L 10/27/2008
P & M -Xylene LCS 62.4 104 ( 80-120 ) 60 ug/L 10/27/2008
Naphthalene LCS 28.5 95 ( 75-120 ) 30 ug/L 10/27/2008
o-Xylene LCS 31.5 105 ( 80-120 ) 30 ug/L 10/27/2008

Bromoform LCS 31.8 106 ( 80-120 ) 30 ug/L 10/27/2008

1-Chlorohexane LCS 44.5 99 ( 70-125 ) 45 ug/L 10/27/2008
1,2,4-Trimethylbenzene LCS 31.8 106 ( 80-125 ) 30 ug/L 10/27/2008
tert-Butylbenzene LCS 32.4 108 ( 80-122 ) 30 ug/L 10/27/2008

1,1,1-Trichloroethane LCS 32.0 107 ( 80-122 ) 30 ug/L 10/27/2008

1,1-Dichloroethane LCS 30.6 102 ( 80-120 ) 30 ug/L 10/27/2008

2-Chlorotoluene LCS 31.0 103 ( 80-125 ) 30 ug/L 10/27/2008

Trichloroethene LCS 28.4 95 ( 80-125 ) 30 ug/L 10/27/2008

trans-1,2-Dichloroethene LCS 30.2 101 ( 79-132 ) 30 ug/L 10/27/2008

1,2-Dichlorobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 10/27/2008
2,2-Dichloropropane LCS 31.2 104 ( 80-132 ) 30 ug/L 10/27/2008

Hexachlorobutadiene LCS 26.4 88 ( 77-125 ) 30 ug/L 10/27/2008
Isopropylbenzene (Cumene) LCS 31.7 106 ( 80-121 ) 30 ug/L 10/27/2008
1,2-Dichloropropane LCS 29.1 97 ( 80-121 ) 30 ug/L 10/27/2008
1,1-Dichloropropene LCS 29.3 98 ( 80-122 ) 30 ug/L 10/27/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867630 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18954 SW5030B 10/27/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,1,2-Trichloroethane LCS 30.1 100 ( 77-120 ) 30 ug/L 10/27/2008

1,3-Dichlorobenzene LCS 29.1 97 ( 80-120 ) 30 ug/L 10/27/2008

1,2,3-Trichlorobenzene LCS 26.3 88 ( 77-120 ) 30 ug/L 10/27/2008

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 10/27/2008

Toluene-d8 <surr> LCS 104 ( 80-120 ) 10/27/2008

4-Bromofluorobenzene <surr> LCS 103 ( 76-120 ) 10/27/2008

Batch Method Instrument 

### VMS10242

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867656 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20276 SW3520C 10/28/2008

QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MSMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867656 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20276 SW3520C 10/28/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Acenaphthylene LCS 0.333 67 ( 50-105 ) 0.5 ug/L 10/30/2008
Acenaphthene LCS 0.314 63 ( 45-110 ) 0.5 ug/L 10/30/2008

Fluorene LCS 0.342 68 ( 50-110 ) 0.5 ug/L 10/30/2008

Phenanthrene LCS 0.369 74 ( 50-115 ) 0.5 ug/L 10/30/2008

Anthracene LCS 0.382 76 ( 55-110 ) 0.5 ug/L 10/30/2008

Fluoranthene LCS 0.342 68 ( 55-125 ) 0.5 ug/L 10/30/2008
Pyrene LCS 0.323 65 ( 50-130 ) 0.5 ug/L 10/30/2008
Benzo(a)Anthracene LCS 0.376 75 ( 55-120 ) 0.5 ug/L 10/30/2008
Chrysene LCS 0.339 68 ( 55-120 ) 0.5 ug/L 10/30/2008
Benzo[b]Fluoranthene LCS 0.376 75 ( 46-130 ) 0.5 ug/L 10/30/2008
Benzo[k]fluoranthene LCS 0.378 76 ( 60-125 ) 0.5 ug/L 10/30/2008
Benzo[a]pyrene LCS 0.416 83 ( 55-120 ) 0.5 ug/L 10/30/2008
Indeno[1,2,3-c,d] pyrene LCS 0.379 76 ( 45-125 ) 0.5 ug/L 10/30/2008
Dibenzo[a,h]anthracene LCS 0.389 78 ( 41-140 ) 0.5 ug/L 10/30/2008
Benzo[g,h,i]perylene LCS 0.376 75 ( 46-125 ) 0.5 ug/L 10/30/2008
Naphthalene LCS 0.266 53 ( 42-100 ) 0.5 ug/L 10/30/2008
1-Methylnaphthalene LCS 0.277 55 ( 46-115 ) 0.5 ug/L 10/30/2008
2-Methylnaphthalene LCS 0.290 58 ( 45-105 ) 0.5 ug/L 10/30/2008

Surrogates 

### Terphenyl-d14 <surr> LCS 93 ( 50-135 ) 10/30/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 867656 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20276 SW3520C 10/28/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS4761

8270D SIMS HP 5890 Series II MS2 SVOAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 868152 Lab Control Sample 868153 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20290 SW3520C 10/29/2008

QC results affect the following production samples: 

### 1085813004, 1085813005, 1085813006, 1085813007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.42 89 ( 75-125 ) 5 mg/L 10/31/2008 LCSD 5.32 106 18 (< 20 ) 5 mg/L 10/31/2008

Surrogates 

### 5a Androstane <surr> LCS 100 ( 60-120 ) 10/31/2008 LCSD 110 10 10/31/2008

Batch Method Instrument 

### XFC8323

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 868325 Lab Control Sample 868326 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18967 SW5030B 10/30/2008

QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Volatile Fuels Department 

### Gasoline Range Organics LCS 192 96 ( 79-108 ) 200 ug/L 10/30/2008 LCSD 189 95 2 (< 20 ) 200 ug/L 10/30/2008

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 96 ( 50-150 ) 10/30/2008 LCSD 95 0 10/30/2008

Batch Method Instrument 

### VFC9248

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 868747 Lab Control Sample 868748 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18976 SW5030B 10/31/2008

QC results affect the following production samples: 

### 1085813005, 1085813006, 1085813007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Naphthalene LCS 29.2 97 ( 75-120 ) 30 ug/L 10/31/2008 LCSD 28.9 96 1 (< 20 ) 30 ug/L 10/31/2008

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 102 ( 73-120 ) 10/31/2008 LCSD 99 3 10/31/2008

Toluene-d8 <surr> LCS 99 ( 80-120 ) 10/31/2008 LCSD 99 0 10/31/2008

4-Bromofluorobenzene <surr> LCS 99 ( 76-120 ) 10/31/2008 LCSD 97 2 10/31/2008

Batch Method Instrument 

### VMS10254

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 869198 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX20313 SW3520C 11/03/2008

QC results affect the following production samples: 

### 1085813001

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 2.81 56 ( 75-125 ) * 5 mg/L 11/05/2008

Surrogates 

### 5a Androstane <surr> LCS 84 ( 60-120 ) 11/05/2008

Batch Method Instrument 

### XFC8338

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 11/20/2008 8:09
Batch Method Date Prep 

### 869582 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX21031 SW3010A 11/04/2008

QC results affect the following production samples: 

### 1085813001, 1085813004, 1085813005, 1085813006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS



### Lead LCS 1070 107 ( 80-120 ) 1000 ug/L 11/14/2008

Batch Method Instrument 

### MMS5719

SW6020 Perkin Elmer Sciex ICP-MS P4Matrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 868545 Matrix Spike 868546 Matrix Spike Duplicate

871926 Water (Surface, Eff., Ground) XXX20290 Cnt. Liq/Liq Ext. for AK102/3 10/29/2008

QC results affect the following production samples: 

### 1085813004, 1085813005, 1085813006, 1085813007

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers



### Semivolatile Organic Fuels Department 

### Diesel Range Organics MS ND ND 0* ( 75-125 ) 5.26 mg/L 10/31/2008 MSD 0.00 0 * 0 (< 30 ) 5.26 mg/L 10/31/2008 Surrogates 

### 5a Androstane <surr> MS .107 102 ( 50-150 ) 10/31/2008 MSD 0.102 97 5 10/31/2008
Batch Method Instrument 

### XFC8323

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) MXX21031 3010 H20 Digest for Metals ICP-MS 11/04/2008

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS ND 1020 102 ( 80-120 ) 1000 ug/L 11/14/2008 BMSD 1000 100 1 (< 15 ) 1000 ug/L 11/14/2008
Batch Method Instrument 

### MMS5719

SW6020 Perkin Elmer Sciex ICP-MS P4

Volatile Fuels Department 

### Gasoline Range Organics BMS ND 448 100 ( 79-108 ) 450 ug/L 10/30/2008 BMSD 401 89 11 (< 20 ) 450 ug/L 10/30/2008 Surrogates 

### 4-Bromofluorobenzene <surr> BMS 50.9 102 ( 50-150 ) 10/30/2008 BMSD 48.6 97 5 10/30/2008
Batch Method Instrument 

### VFC9248

SW8015C HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS ND 4.89 94 ( 75-125 ) 5.21 mg/L 11/05/2008 BMSD 4.72 94 4 (< 30 ) 5.00 mg/L 11/05/2008 Surrogates 

### 5a Androstane <surr> BMS .103 99 ( 50-150 ) 11/05/2008 BMSD 0.102 102 1 11/05/2008
Batch Method Instrument 

### XFC8338

SW8015C HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) VXX18954 Volatiles Extraction AFCEE 3.1 8260 (W) 10/27/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene BMS ND 27.9 93 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 28.4 95 2 (< 20 ) 30.0 ug/L 10/27/2008 Toluene BMS ND 29.6 99 ( 77-120 ) 30.0 ug/L 10/27/2008 BMSD 29.6 99 0 (< 20 ) 30.0 ug/L 10/27/2008 Ethylbenzene BMS ND 30.6 102 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 31.3 104 2 (< 20 ) 30.0 ug/L 10/27/2008 n-Butylbenzene BMS ND 34.4 115 ( 80-124 ) 30.0 ug/L 10/27/2008 BMSD 35.5 118 3 (< 20 ) 30.0 ug/L 10/27/2008 1,4-Dichlorobenzene BMS ND 29.3 98 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.9 103 5 (< 20 ) 30.0 ug/L 10/27/2008 1,2-Dichloroethane BMS ND 28.3 94 ( 80-129 ) 30.0 ug/L 10/27/2008 BMSD 29.2 97 3 (< 20 ) 30.0 ug/L 10/27/2008 1,3,5-Trimethylbenzene BMS ND 33 110 ( 80-128 ) 30.0 ug/L 10/27/2008 BMSD 34.0 113 3 (< 20 ) 30.0 ug/L 10/27/2008 4-Chlorotoluene BMS ND 31.8 106 ( 79-128 ) 30.0 ug/L 10/27/2008 BMSD 33.0 110 4 (< 20 ) 30.0 ug/L 10/27/2008 Chlorobenzene BMS ND 30 100 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 29.9 100 0 (< 20 ) 30.0 ug/L 10/27/2008 4-Methyl-2-pentanone (MIBK) BMS ND 82.4 92 ( 69-134 ) 90.0 ug/L 10/27/2008 BMSD 87.9 98 7 (< 20 ) 90.0 ug/L 10/27/2008 cis-1,2-Dichloroethene BMS ND 29.4 98 ( 80-125 ) 30.0 ug/L 10/27/2008 BMSD 29.8 99 1 (< 20 ) 30.0 ug/L 10/27/2008 4-Isopropyltoluene BMS ND 33.7 112 ( 80-125 ) 30.0 ug/L 10/27/2008 BMSD 34.4 115 2 (< 20 ) 30.0 ug/L 10/27/2008 cis-1,3-Dichloropropene BMS ND 29.5 98 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.8 103 5 (< 20 ) 30.0 ug/L 10/27/2008 n-Propylbenzene BMS ND 32.5 108 ( 80-129 ) 30.0 ug/L 10/27/2008 BMSD 33.7 112 4 (< 20 ) 30.0 ug/L 10/27/2008 Styrene BMS ND 32 107 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 32.3 108 1 (< 20 ) 30.0 ug/L 10/27/2008 Dibromomethane BMS ND 28.4 95 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 29.7 99 5 (< 20 ) 30.0 ug/L 10/27/2008 trans-1,3-Dichloropropene BMS ND 30.1 100 ( 80-124 ) 30.0 ug/L 10/27/2008 BMSD 31.5 105 5 (< 20 ) 30.0 ug/L 10/27/2008 1,2,4-Trichlorobenzene BMS ND 30.9 103 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 32.2 107 4 (< 20 ) 30.0 ug/L 10/27/2008 Acetone BMS ND 83.2 93 ( 50-135 ) 90.0 ug/L 10/27/2008 BMSD 86.9 97 4 (< 20 ) 90.0 ug/L 10/27/2008 1,1,2,2-Tetrachloroethane BMS ND 29.3 98 ( 76-123 ) 30.0 ug/L 10/27/2008 BMSD 30.7 102 4 (< 20 ) 30.0 ug/L 10/27/2008Matrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) VXX18954 Volatiles Extraction AFCEE 3.1 8260 (W) 10/27/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,2-Dibromo-3-chloropropane BMS ND 32.6 109 ( 73-130 ) 30.0 ug/L 10/27/2008 BMSD 34.4 115 5 (< 20 ) 30.0 ug/L 10/27/2008 Methyl-t-butyl ether BMS ND 45.4 101 ( 80-120 ) 45.0 ug/L 10/27/2008 BMSD 47.2 105 4 (< 20 ) 45.0 ug/L 10/27/2008 Tetrachloroethene BMS ND 30.6 102 ( 79-122 ) 30.0 ug/L 10/27/2008 BMSD 30.5 102 0 (< 20 ) 30.0 ug/L 10/27/2008 Dibromochloromethane BMS ND 29.9 100 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 10/27/2008 1,3-Dichloropropane BMS ND 30.2 101 ( 80-121 ) 30.0 ug/L 10/27/2008 BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/27/2008 1,2-Dibromoethane BMS ND 29.8 99 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.4 101 2 (< 20 ) 30.0 ug/L 10/27/2008 Carbon tetrachloride BMS ND 29.4 98 ( 80-126 ) 30.0 ug/L 10/27/2008 BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 10/27/2008 1,1,1,2-Tetrachloroethane BMS ND 30.2 101 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/27/2008 Chloroform BMS ND 29.2 97 ( 80-124 ) 30.0 ug/L 10/27/2008 BMSD 29.7 99 2 (< 20 ) 30.0 ug/L 10/27/2008 Bromobenzene BMS ND 29.9 100 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 31.2 104 4 (< 20 ) 30.0 ug/L 10/27/2008 Chloromethane BMS ND 28.2 94 ( 67-125 ) 30.0 ug/L 10/27/2008 BMSD 28.9 96 2 (< 20 ) 30.0 ug/L 10/27/2008 1,2,3-Trichloropropane BMS ND 30.4 101 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 10/27/2008 Bromomethane BMS ND 32.8 109 ( 30-140 ) 30.0 ug/L 10/27/2008 BMSD 35.7 119 9 (< 20 ) 30.0 ug/L 10/27/2008 Bromochloromethane BMS ND 28.4 95 ( 77-129 ) 30.0 ug/L 10/27/2008 BMSD 29.0 97 2 (< 20 ) 30.0 ug/L 10/27/2008 Vinyl chloride BMS ND 29.6 99 ( 72-145 ) 30.0 ug/L 10/27/2008 BMSD 30.3 101 2 (< 20 ) 30.0 ug/L 10/27/2008 Dichlorodifluoromethane BMS ND 28.7 96 ( 62-153 ) 30.0 ug/L 10/27/2008 BMSD 29.1 97 2 (< 20 ) 30.0 ug/L 10/27/2008 Chloroethane BMS ND 30 100 ( 67-133 ) 30.0 ug/L 10/27/2008 BMSD 34.5 115 14 (< 20 ) 30.0 ug/L 10/27/2008 sec-Butylbenzene BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 34.7 116 4 (< 20 ) 30.0 ug/L 10/27/2008 Bromodichloromethane BMS ND 30.5 102 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 31.8 106 4 (< 20 ) 30.0 ug/L 10/27/2008 1,1-Dichloroethene BMS ND 31.6 105 ( 76-130 ) 30.0 ug/L 10/27/2008 BMSD 32.5 108 3 (< 20 ) 30.0 ug/L 10/27/2008Matrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) VXX18954 Volatiles Extraction AFCEE 3.1 8260 (W) 10/27/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) BMS ND 85.1 95 ( 66-136 ) 90.0 ug/L 10/27/2008 BMSD 87.2 97 2 (< 20 ) 90.0 ug/L 10/27/2008 Methylene chloride BMS ND 31.3 104 ( 63-131 ) 30.0 ug/L 10/27/2008 BMSD 32.9 110 5 (< 20 ) 30.0 ug/L 10/27/2008 Trichlorofluoromethane BMS ND 30.7 102 ( 68-145 ) 30.0 ug/L 10/27/2008 BMSD 31.0 103 1 (< 20 ) 30.0 ug/L 10/27/2008 P & M -Xylene BMS ND 64.7 108 ( 80-120 ) 60.0 ug/L 10/27/2008 BMSD 65.1 109 1 (< 20 ) 60.0 ug/L 10/27/2008 Naphthalene BMS ND 28.8 96 ( 75-120 ) 30.0 ug/L 10/27/2008 BMSD 30.2 101 5 (< 20 ) 30.0 ug/L 10/27/2008 o-Xylene BMS ND 31.8 106 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 31.8 106 0 (< 20 ) 30.0 ug/L 10/27/2008 Bromoform BMS ND 29.9 100 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.9 103 3 (< 20 ) 30.0 ug/L 10/27/2008 1-Chlorohexane BMS ND 50.2 111 ( 70-125 ) 45.0 ug/L 10/27/2008 BMSD 50.2 112 0 (< 20 ) 45.0 ug/L 10/27/2008 1,2,4-Trimethylbenzene BMS ND 32.4 108 ( 80-125 ) 30.0 ug/L 10/27/2008 BMSD 33.6 112 4 (< 20 ) 30.0 ug/L 10/27/2008 tert-Butylbenzene BMS ND 32.1 107 ( 80-122 ) 30.0 ug/L 10/27/2008 BMSD 33.6 112 5 (< 20 ) 30.0 ug/L 10/27/2008 1,1,1-Trichloroethane BMS ND 31.3 104 ( 80-122 ) 30.0 ug/L 10/27/2008 BMSD 32.1 107 3 (< 20 ) 30.0 ug/L 10/27/2008 1,1-Dichloroethane BMS ND 31.6 105 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 32.4 108 3 (< 20 ) 30.0 ug/L 10/27/2008 2-Chlorotoluene BMS ND 30.9 103 ( 80-125 ) 30.0 ug/L 10/27/2008 BMSD 32.2 107 4 (< 20 ) 30.0 ug/L 10/27/2008 Trichloroethene BMS ND 29 97 ( 80-125 ) 30.0 ug/L 10/27/2008 BMSD 29.3 98 1 (< 20 ) 30.0 ug/L 10/27/2008 trans-1,2-Dichloroethene BMS ND 32.6 109 ( 79-132 ) 30.0 ug/L 10/27/2008 BMSD 33.0 110 1 (< 20 ) 30.0 ug/L 10/27/2008 1,2-Dichlorobenzene BMS ND 30.2 101 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 31.4 105 4 (< 20 ) 30.0 ug/L 10/27/2008 2,2-Dichloropropane BMS ND 31.9 106 ( 80-132 ) 30.0 ug/L 10/27/2008 BMSD 32.9 110 3 (< 20 ) 30.0 ug/L 10/27/2008 Hexachlorobutadiene BMS ND 29.6 99 ( 77-125 ) 30.0 ug/L 10/27/2008 BMSD 30.0 100 1 (< 20 ) 30.0 ug/L 10/27/2008 Isopropylbenzene (Cumene) BMS ND 32.4 108 ( 80-121 ) 30.0 ug/L 10/27/2008 BMSD 32.7 109 1 (< 20 ) 30.0 ug/L 10/27/2008 1,2-Dichloropropane BMS ND 28.9 96 ( 80-121 ) 30.0 ug/L 10/27/2008 BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 10/27/2008Matrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) VXX18954 Volatiles Extraction AFCEE 3.1 8260 (W) 10/27/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1-Dichloropropene BMS ND 30.3 101 ( 80-122 ) 30.0 ug/L 10/27/2008 BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 10/27/2008 1,1,2-Trichloroethane BMS ND 29.7 99 ( 77-120 ) 30.0 ug/L 10/27/2008 BMSD 30.1 100 2 (< 20 ) 30.0 ug/L 10/27/2008 1,3-Dichlorobenzene BMS ND 29.5 99 ( 80-120 ) 30.0 ug/L 10/27/2008 BMSD 30.5 102 3 (< 20 ) 30.0 ug/L 10/27/2008 1,2,3-Trichlorobenzene BMS ND 27.7 92 ( 77-120 ) 30.0 ug/L 10/27/2008 BMSD 29.3 98 5 (< 20 ) 30.0 ug/L 10/27/2008 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 30.9 103 ( 73-120 ) 10/27/2008 BMSD 31.0 103 0 10/27/2008 Toluene-d8 <surr> BMS 30.9 103 ( 80-120 ) 10/27/2008 BMSD 30.8 103 0 10/27/2008 4-Bromofluorobenzene <surr> BMS 30.3 101 ( 76-120 ) 10/27/2008 BMSD 31.0 103 2 10/27/2008
Batch Method Instrument 

### VMS10242

SW8260B HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) XXX20276 3520 Liquid/Liquid Ext for 8270 SIM 10/28/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### Acenaphthylene BMS ND .362 68 ( 50-105 ) 0.532 ug/L 10/30/2008 BMSD 0.350 64 3 (< 30 ) 0.549 ug/L 10/30/2008 Acenaphthene BMS ND .345 65 ( 45-110 ) 0.532 ug/L 10/30/2008 BMSD 0.342 62 1 (< 30 ) 0.549 ug/L 10/30/2008 Fluorene BMS ND .36 68 ( 50-110 ) 0.532 ug/L 10/30/2008 BMSD 0.349 64 3 (< 30 ) 0.549 ug/L 10/30/2008 Phenanthrene BMS ND .348 65 ( 50-115 ) 0.532 ug/L 10/30/2008 BMSD 0.343 63 1 (< 30 ) 0.549 ug/L 10/30/2008 Anthracene BMS ND .372 70 ( 55-110 ) 0.532 ug/L 10/30/2008 BMSD 0.363 66 2 (< 30 ) 0.549 ug/L 10/30/2008 Fluoranthene BMS ND .38 71 ( 55-125 ) 0.532 ug/L 10/30/2008 BMSD 0.378 69 1 (< 30 ) 0.549 ug/L 10/30/2008 Pyrene BMS ND .366 69 ( 50-130 ) 0.532 ug/L 10/30/2008 BMSD 0.364 66 1 (< 30 ) 0.549 ug/L 10/30/2008 Benzo(a)Anthracene BMS ND .398 75 ( 55-120 ) 0.532 ug/L 10/30/2008 BMSD 0.380 69 5 (< 30 ) 0.549 ug/L 10/30/2008 Chrysene BMS ND .386 73 ( 55-120 ) 0.532 ug/L 10/30/2008 BMSD 0.387 70 0 (< 30 ) 0.549 ug/L 10/30/2008 Benzo[b]Fluoranthene BMS ND .406 76 ( 46-130 ) 0.532 ug/L 10/30/2008 BMSD 0.408 74 1 (< 30 ) 0.549 ug/L 10/30/2008 Benzo[k]fluoranthene BMS ND .413 78 ( 60-125 ) 0.532 ug/L 10/30/2008 BMSD 0.392 71 5 (< 30 ) 0.549 ug/L 10/30/2008 Benzo[a]pyrene BMS ND .43 81 ( 55-120 ) 0.532 ug/L 10/30/2008 BMSD 0.418 76 3 (< 30 ) 0.549 ug/L 10/30/2008 Indeno[1,2,3-c,d] pyrene BMS ND .416 78 ( 45-125 ) 0.532 ug/L 10/30/2008 BMSD 0.414 75 1 (< 30 ) 0.549 ug/L 10/30/2008 Dibenzo[a,h]anthracene BMS ND .424 80 ( 41-140 ) 0.532 ug/L 10/30/2008 BMSD 0.425 77 0 (< 30 ) 0.549 ug/L 10/30/2008 Benzo[g,h,i]perylene BMS ND .421 79 ( 46-125 ) 0.532 ug/L 10/30/2008 BMSD 0.416 76 1 (< 30 ) 0.549 ug/L 10/30/2008 Naphthalene BMS 0.0466 J .333 54 ( 42-100 ) 0.532 ug/L 10/30/2008 BMSD 0.325 51 3 (< 30 ) 0.549 ug/L 10/30/2008 1-Methylnaphthalene BMS 0.0276 J .341 59 ( 46-115 ) 0.532 ug/L 10/30/2008 BMSD 0.336 56 2 (< 30 ) 0.549 ug/L 10/30/2008 2-Methylnaphthalene BMS ND .336 63 ( 45-105 ) 0.532 ug/L 10/30/2008 BMSD 0.327 60 3 (< 30 ) 0.549 ug/L 10/30/2008 Surrogates 

### Terphenyl-d14 <surr> BMS .457 86 ( 50-135 ) 10/30/2008 BMSD 0.454 83 1 10/30/2008Matrix SGS Ref.# Printed Date/Time 

### 11/20/2008 8:09 Batch Method Date Original Prep 

### 1085813002 Billable Matrix Spike 1085813003 Billable Matrix Spike Dup.

1085813001 Water (Surface, Eff., Ground) XXX20276 3520 Liquid/Liquid Ext for 8270 SIM 10/28/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS4761

8270D SIMS HP 5890 Series II MS2 SVOA

## Hager, Barbara (Anchorage)

From: Adkisson, Richard K. [RKAdkisson@tecinc.com] Sent: Wednesday, October 29, 2008 8:58 AM To: Hager, Barbara (Anchorage) Cc: Hart, Jeff; Whitman, William M.C.; Adkisson, Richard K. Subject: Analysis of Sample RHMW01-WG13 Importance: High Attachments: image001.jpg 

## Pa g e 1 of 1

10/29/2008 Barbara,

Please cancel the analysis of sample RHMW01

‐ WG13 for total lead

. TEC will collect another sample, filter it in the field, and sent it for dissolved lead analysis. Please press on with the other requested analysis for RHMW01

‐ WG13 and all other samples. Thank you.

Rick Adkisson TEC, Inc. 1001 Bishop Street, Suite 1400 Honolulu, HI 96813 Phone: 808

‐ 528

‐ 1445 Fax: 808

‐ 528

‐ 0768

## SGS Work Order:

Contents:
Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS Environmental Services Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 9121-003 Red Hill BFSF The Environmental Company, Inc. (TEC) 1086126

## CASE NARRATIVE Print Date: 12/11/2008

Workorder No.: 1086126 Project Name: 9121-003 Red Hill BFSF Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID 

## Sample Comments

Sample Type Client Sample ID Refer to the sample receipt form for information on sample condition.

There were no analytical anomalies associated with the data reported herein.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of SG S G roup (S ociété G énérale de S urveillance)

# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1086126

Certification:
I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1001 Bishop Street Ste 1400 ASB Tower Honolulu, HI 96813
Attn: Jeff Hart T: (808)528-1445 F:(808)528-0768 jshart@tecinc.com

Tamara Rentz tamara.rentz@sgs.com Project Manager 

### 9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roupEnclosed are the analytical results associated with this workorder.
As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).
Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.
If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 907-562-2343.
The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit PQL Practical Quantitation Limit (reporting limit). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indicates value that is greater than or equal to the MDL. J The quantitation is an estimation. ND Indicates the analyte is not detected B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits. D The analyte concentration is the result of dilution. GT Greater Than LT Less Than Q QC parameter out of acceptance range. M A matrix effect was present. E The analyte result is above the calibrated range. R Rejected DF Analytical Dilution Factor JL The analyte was positively identified, but the quantitation is a low estimation. <Surr> Surrogate QC spiked standard <Surr/IS> Surrogate / Internal Standard QC spiked standard QC Quality Control QA Quality Assurance MB Method Blank LCS (D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) BMS(D) Site Specific Matrix Spike RPD Relative Percent Difference ICV Initial Calibration Verification CCV Continuous Calibration Verification MSA Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified Print Date: 12/11/2008

Notes: All DRO/RRO analysese are integrated per SOP.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of SG S G roup

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 9121-003 Red Hill BFSF Workorder No.: 1086126 

## Analytical Methods

Method Description Analytical Method Dissolved Metals by ICP-MS SW6020 Print Date: 12/11/2008 1:06 pm



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1086126001 RHMW01-WG13

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of SG S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/11/2008 1:06 pm

Client Sample ID: 

### RHMW01-WG13 SGS Ref. #: 1086126001 Collection Date/Time: 11/03/08 13:35 Receipt Date/Time: 11/05/08 09:45 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead 0.966 J 1.00 ug/L MMS5721 MXX21078 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5721 Analytical Method: SW6020 Analysis Date/Time: 11/15/08 17:30 Prep Batch: MXX21078 Prep Method: SW3010A Prep Date/Time: 11/13/08 20:00 Container ID:1086126001-A Dilution Factor: 5 Analyst: BME

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 www. us. sgs.com Member of SGS Group (Société Générale de Surveillance)Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 12/11/2008 13:06 Batch Method Date Prep 

### 871318 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX21078 SW3010A 11/13/2008 QC results affect the following production samples: 

### 1086126001

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Metals by ICP/MS



### Lead ND 1.00 ug/L 11/20/08 

### 0.310

Instrument Method Batch MMS5732

SW6020 Perkin Elmer Sciex ICP-MS P4Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/11/2008 13:06
Batch Method Date Prep 

### 871319 Lab Control Sample
The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX21078 SW3010A 11/13/2008

QC results affect the following production samples: 

### 1086126001

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS



### Lead LCS 1000 100 ( 80-120 ) 1000 ug/L 11/20/2008

Batch Method Instrument 

### MMS5732

SW6020 Perkin Elmer Sciex ICP-MS P4

## SGS Work Order:

Contents:
Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS Environmental Services Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 9121-003 Red Hill BFSF The Environmental Company, Inc. (TEC) 1086721

## CASE NARRATIVE Print Date: 12/22/2008

Workorder No.: 1086721 Project Name: 9121-003 Red Hill BFSF Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID 

## Sample Comments

Sample Type Client Sample ID Refer to the sample receipt form for information on sample condition.

876591 8260B - MS recovery for several analytes does not meet QC goals (biased high). See LCS for accuracy.

MS 1086597003A(876590MS)

876592 8260B - MSD recovery for several analytes does not meet QC goals (biased high). See LCS for accuracy.

MSD 1086597003A(876590MSD)

876594 8260B - ICV recovery for dichlorodifluoromethane and 1,1-dichloroethene does not meet QC goals (biased high). These

analytes were not detected above the PQL in the associated samples. CCV CCV for HBN 210083 [VMS/10317]

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 ww w. us. sgs.com M em ber of SG S G roup (S ociété G énérale de S urveillance)

# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1086721

Certification:
I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1001 Bishop Street Ste 1400 ASB Tower Honolulu, HI 96813
Attn: Jeff Hart T: (808)528-1445 F:(808)528-0768 jshart@tecinc.com

Tamara Rentz tamara.rentz@sgs.com Project Manager 

### 9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roupEnclosed are the analytical results associated with this workorder.
As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).
Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.
If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 907-562-2343.
The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit PQL Practical Quantitation Limit (reporting limit). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indicates value that is greater than or equal to the MDL. J The quantitation is an estimation. ND Indicates the analyte is not detected B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits. D The analyte concentration is the result of dilution. GT Greater Than LT Less Than Q QC parameter out of acceptance range. M A matrix effect was present. E The analyte result is above the calibrated range. R Rejected DF Analytical Dilution Factor JL The analyte was positively identified, but the quantitation is a low estimation. <Surr> Surrogate QC spiked standard <Surr/IS> Surrogate / Internal Standard QC spiked standard QC Quality Control QA Quality Assurance MB Method Blank LCS (D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) BMS(D) Site Specific Matrix Spike RPD Relative Percent Difference ICV Initial Calibration Verification CCV Continuous Calibration Verification MSA Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified Print Date: 12/22/2008

Notes: All DRO/RRO analysese are integrated per SOP.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 ww w. us. sgs.com M em ber of SG S G roup

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 9121-003 Red Hill BFSF Workorder No.: 1086721 

## Analytical Methods

Method Description Analytical Method AFCEE 3.1 8260 (W) SW8260B Print Date: 12/22/2008 11:45 am



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1086721001 RHMW2254-WG13B
1086721002 RHMWA01-WG13B 1086721003 TB01-WG13B

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 ww w. us. sgs.com M em ber of SG S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: 

### RHMW2254-WG13B SGS Ref. #: 1086721001 Collection Date/Time: 12/16/08 10:05 Receipt Date/Time: 12/17/08 11:55 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10317 VXX19107 0.120 1 Toluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10317 VXX19107 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Styrene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dibromomethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Acetone ND 10.0 ug/L VMS10317 VXX19107 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10317 VXX19107 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10317 VXX19107 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10317 VXX19107 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 Chloroform ND 1.00 ug/L VMS10317 VXX19107 0.300 1 Bromobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Chloromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromomethane ND 3.00 ug/L VMS10317 VXX19107 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: 

### RHMW2254-WG13B SGS Ref. #: 1086721001 Collection Date/Time: 12/16/08 10:05 Receipt Date/Time: 12/17/08 11:55 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10317 VXX19107 3.10 1 Methylene chloride ND 5.00 ug/L VMS10317 VXX19107 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10317 VXX19107 0.620 1 Naphthalene ND 2.00 ug/L VMS10317 VXX19107 0.620 1 o-Xylene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromoform ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Trichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichloroethane-D4 <surr> 99.2 73-120 % VMS10317 VXX19107 1 Toluene-d8 <surr> 99.6 80-120 % VMS10317 VXX19107 1 4-Bromofluorobenzene <surr> 100 76-120 % VMS10317 VXX19107 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10317 Analytical Method: SW8260B Analysis Date/Time: 12/19/08 02:19 Prep Batch: VXX19107 Prep Method: SW5030B Prep Date/Time: 12/18/08 14:04 Container ID:1086721001-A Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: 

### RHMWA01-WG13B SGS Ref. #: 1086721002 Collection Date/Time: 12/16/08 12:05 Receipt Date/Time: 12/17/08 11:55 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10317 VXX19107 0.120 1 Toluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10317 VXX19107 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Styrene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dibromomethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Acetone ND 10.0 ug/L VMS10317 VXX19107 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10317 VXX19107 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10317 VXX19107 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10317 VXX19107 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 Chloroform ND 1.00 ug/L VMS10317 VXX19107 0.300 1 Bromobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Chloromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromomethane ND 3.00 ug/L VMS10317 VXX19107 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: 

### RHMWA01-WG13B SGS Ref. #: 1086721002 Collection Date/Time: 12/16/08 12:05 Receipt Date/Time: 12/17/08 11:55 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10317 VXX19107 3.10 1 Methylene chloride ND 5.00 ug/L VMS10317 VXX19107 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10317 VXX19107 0.620 1 Naphthalene ND 2.00 ug/L VMS10317 VXX19107 0.620 1 o-Xylene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromoform ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Trichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichloroethane-D4 <surr> 95.9 73-120 % VMS10317 VXX19107 1 Toluene-d8 <surr> 102 80-120 % VMS10317 VXX19107 1 4-Bromofluorobenzene <surr> 99.6 76-120 % VMS10317 VXX19107 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10317 Analytical Method: SW8260B Analysis Date/Time: 12/19/08 02:52 Prep Batch: VXX19107 Prep Method: SW5030B Prep Date/Time: 12/18/08 14:04 Container ID:1086721002-A Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: 

### TB01-WG13B SGS Ref. #: 1086721003 Collection Date/Time: 12/16/08 08:05 Receipt Date/Time: 12/17/08 11:55 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10317 VXX19107 0.120 1 Toluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10317 VXX19107 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10317 VXX19107 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Styrene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dibromomethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Acetone ND 10.0 ug/L VMS10317 VXX19107 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10317 VXX19107 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10317 VXX19107 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10317 VXX19107 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 Chloroform ND 1.00 ug/L VMS10317 VXX19107 0.300 1 Bromobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Chloromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromomethane ND 3.00 ug/L VMS10317 VXX19107 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: 

### TB01-WG13B SGS Ref. #: 1086721003 Collection Date/Time: 12/16/08 08:05 Receipt Date/Time: 12/17/08 11:55 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10317 VXX19107 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10317 VXX19107 3.10 1 Methylene chloride ND 5.00 ug/L VMS10317 VXX19107 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10317 VXX19107 0.620 1 Naphthalene ND 2.00 ug/L VMS10317 VXX19107 0.620 1 o-Xylene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Bromoform ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Trichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10317 VXX19107 0.310 1 1,2-Dichloroethane-D4 <surr> 114 73-120 % VMS10317 VXX19107 1 Toluene-d8 <surr> 99.2 80-120 % VMS10317 VXX19107 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS10317 VXX19107 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10317 Analytical Method: SW8260B Analysis Date/Time: 12/18/08 20:43 Prep Batch: VXX19107 Prep Method: SW5030B Prep Date/Time: 12/18/08 14:04 Container ID:1086721003-A Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45 Batch Method Date Prep 

### 876587 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008 QC results affect the following production samples: 

### 1086721001, 1086721002, 1086721003

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene ND 0.400 ug/L 12/18/08 

### 0.120 Toluene ND 1.00 ug/L 12/18/08 

### 0.310 Ethylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 n-Butylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 1,4-Dichlorobenzene ND 0.500 ug/L 12/18/08 

### 0.150 1,2-Dichloroethane ND 0.500 ug/L 12/18/08 

### 0.150 1,3,5-Trimethylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 4-Chlorotoluene ND 1.00 ug/L 12/18/08 

### 0.310 Chlorobenzene ND 0.500 ug/L 12/18/08 

### 0.150 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 12/18/08 

### 3.10 cis-1,2-Dichloroethene ND 1.00 ug/L 12/18/08 

### 0.310 4-Isopropyltoluene ND 1.00 ug/L 12/18/08 

### 0.310 cis-1,3-Dichloropropene ND 0.500 ug/L 12/18/08 

### 0.150 n-Propylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 Styrene ND 1.00 ug/L 12/18/08 

### 0.310 Dibromomethane ND 1.00 ug/L 12/18/08 

### 0.310 trans-1,3-Dichloropropene ND 1.00 ug/L 12/18/08 

### 0.310 1,2,4-Trichlorobenzene ND 1.00 ug/L 12/18/08 

### 0.310 Acetone ND 10.0 ug/L 12/18/08 

### 3.10 1,1,2,2-Tetrachloroethane ND 0.500 ug/L 12/18/08 

### 0.150 1,2-Dibromo-3-chloropropane ND 2.00 ug/L 12/18/08 

### 0.620 Methyl-t-butyl ether ND 5.00 ug/L 12/18/08 

### 1.50 Tetrachloroethene ND 1.00 ug/L 12/18/08 

### 0.310 Dibromochloromethane ND 0.500 ug/L 12/18/08 

### 0.150 1,3-Dichloropropane ND 0.400 ug/L 12/18/08 

### 0.120 1,2-Dibromoethane ND 1.00 ug/L 12/18/08 

### 0.310 Carbon tetrachloride ND 1.00 ug/L 12/18/08 

### 0.310 1,1,1,2-Tetrachloroethane ND 0.500 ug/L 12/18/08 

### 0.150 Chloroform ND 1.00 ug/L 12/18/08 

### 0.300 Bromobenzene ND 1.00 ug/L 12/18/08 

### 0.310 Chloromethane ND 1.00 ug/L 12/18/08 

### 0.310 1,2,3-Trichloropropane ND 1.00 ug/L 12/18/08 

### 0.310 Bromomethane ND 3.00 ug/L 12/18/08 

### 0.940 Bromochloromethane ND 1.00 ug/L 12/18/08 

### 0.310 Vinyl chloride ND 1.00 ug/L 12/18/08 

### 0.310 Dichlorodifluoromethane ND 1.00 ug/L 12/18/08 

### 0.310Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45 Batch Method Date Prep 

### 876587 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Chloroethane ND 1.00 ug/L 12/18/08 

### 0.310 sec-Butylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 Bromodichloromethane ND 0.500 ug/L 12/18/08 

### 0.150 1,1-Dichloroethene ND 1.00 ug/L 12/18/08 

### 0.310 2-Butanone (MEK) ND 10.0 ug/L 12/18/08 

### 3.10 Methylene chloride ND 5.00 ug/L 12/18/08 

### 1.00 Trichlorofluoromethane ND 1.00 ug/L 12/18/08 

### 0.310 P & M -Xylene ND 2.00 ug/L 12/18/08 

### 0.620 Naphthalene ND 2.00 ug/L 12/18/08 

### 0.620 o-Xylene ND 1.00 ug/L 12/18/08 

### 0.310 Bromoform ND 1.00 ug/L 12/18/08 

### 0.310 1-Chlorohexane ND 1.00 ug/L 12/18/08 

### 0.310 1,2,4-Trimethylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 tert-Butylbenzene ND 1.00 ug/L 12/18/08 

### 0.310 1,1,1-Trichloroethane ND 1.00 ug/L 12/18/08 

### 0.310 1,1-Dichloroethane ND 1.00 ug/L 12/18/08 

### 0.310 2-Chlorotoluene ND 1.00 ug/L 12/18/08 

### 0.310 Trichloroethene ND 1.00 ug/L 12/18/08 

### 0.310 trans-1,2-Dichloroethene ND 1.00 ug/L 12/18/08 

### 0.310 1,2-Dichlorobenzene ND 1.00 ug/L 12/18/08 

### 0.310 2,2-Dichloropropane ND 1.00 ug/L 12/18/08 

### 0.310 Hexachlorobutadiene ND 1.00 ug/L 12/18/08 

### 0.310 Isopropylbenzene (Cumene) ND 1.00 ug/L 12/18/08 

### 0.310 1,2-Dichloropropane ND 1.00 ug/L 12/18/08 

### 0.310 1,1-Dichloropropene ND 1.00 ug/L 12/18/08 

### 0.310 1,1,2-Trichloroethane ND 1.00 ug/L 12/18/08 

### 0.310 1,3-Dichlorobenzene ND 1.00 ug/L 12/18/08 

### 0.310 1,2,3-Trichlorobenzene ND 1.00 ug/L 12/18/08 

### 0.310
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 114 73-120 % 12/18/08 

### Toluene-d8 <surr> 99.4 80-120 % 12/18/08 

### 4-Bromofluorobenzene <surr> 103 76-120 % 12/18/08

Instrument Method Batch VMS10317

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45
Batch Method Date Prep 

### 876588 Lab Control Sample 876589 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

QC results affect the following production samples: 

### 1086721001, 1086721002, 1086721003

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene LCS 32.9 110 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 33.1 110 1 (< 20 ) 30 ug/L 12/18/2008

Toluene LCS 32.5 108 ( 77-120 ) 30 ug/L 12/18/2008 LCSD 32.2 107 1 (< 20 ) 30 ug/L 12/18/2008
Ethylbenzene LCS 32.7 109 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.7 109 0 (< 20 ) 30 ug/L 12/18/2008
n-Butylbenzene LCS 33.4 111 ( 80-124 ) 30 ug/L 12/18/2008 LCSD 33.1 110 1 (< 20 ) 30 ug/L 12/18/2008

1,4-Dichlorobenzene LCS 32.6 109 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.2 107 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dichloroethane LCS 32.6 109 ( 80-129 ) 30 ug/L 12/18/2008 LCSD 32.4 108 1 (< 20 ) 30 ug/L 12/18/2008
1,3,5-Trimethylbenzene LCS 33.3 111 ( 80-128 ) 30 ug/L 12/18/2008 LCSD 32.8 109 2 (< 20 ) 30 ug/L 12/18/2008

4-Chlorotoluene LCS 33.2 111 ( 79-128 ) 30 ug/L 12/18/2008 LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

Chlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 30.5 102 0 (< 20 ) 30 ug/L 12/18/2008
4-Methyl-2-pentanone (MIBK) LCS 93.0 103 ( 69-134 ) 90 ug/L 12/18/2008 LCSD 98.2 109 5 (< 20 ) 90 ug/L 12/18/2008

cis-1,2-Dichloroethene LCS 34.4 115 ( 80-125 ) 30 ug/L 12/18/2008 LCSD 34.1 114 1 (< 20 ) 30 ug/L 12/18/2008
4-Isopropyltoluene LCS 33.3 111 ( 80-125 ) 30 ug/L 12/18/2008 LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008
cis-1,3-Dichloropropene LCS 29.5 98 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 30.1 100 2 (< 20 ) 30 ug/L 12/18/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45
Batch Method Date Prep 

### 876588 Lab Control Sample 876589 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### n-Propylbenzene LCS 33.1 110 ( 80-129 ) 30 ug/L 12/18/2008 LCSD 32.6 109 2 (< 20 ) 30 ug/L 12/18/2008
Styrene LCS 30.5 102 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 30.8 103 1 (< 20 ) 30 ug/L 12/18/2008

Dibromomethane LCS 31.4 105 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.5 108 3 (< 20 ) 30 ug/L 12/18/2008
trans-1,3-Dichloropropene LCS 32.5 108 ( 80-124 ) 30 ug/L 12/18/2008 LCSD 33.1 110 2 (< 20 ) 30 ug/L 12/18/2008

1,2,4-Trichlorobenzene LCS 30.7 102 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 30.3 101 1 (< 20 ) 30 ug/L 12/18/2008

Acetone LCS 94.2 105 ( 50-135 ) 90 ug/L 12/18/2008 LCSD 101 112 7 (< 20 ) 90 ug/L 12/18/2008

1,1,2,2-Tetrachloroethane LCS 32.1 107 ( 76-123 ) 30 ug/L 12/18/2008 LCSD 33.0 110 3 (< 20 ) 30 ug/L 12/18/2008
1,2-Dibromo-3-chloropropane LCS 34.8 116 ( 73-130 ) 30 ug/L 12/18/2008 LCSD 33.9 113 3 (< 20 ) 30 ug/L 12/18/2008
Methyl-t-butyl ether LCS 49.6 110 ( 80-120 ) 45 ug/L 12/18/2008 LCSD 49.9 111 1 (< 20 ) 45 ug/L 12/18/2008

Tetrachloroethene LCS 31.2 104 ( 79-122 ) 30 ug/L 12/18/2008 LCSD 31.2 104 0 (< 20 ) 30 ug/L 12/18/2008

Dibromochloromethane LCS 33.0 110 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 33.5 112 2 (< 20 ) 30 ug/L 12/18/2008
1,3-Dichloropropane LCS 33.1 110 ( 80-121 ) 30 ug/L 12/18/2008 LCSD 33.4 111 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dibromoethane LCS 32.5 108 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

Carbon tetrachloride LCS 32.9 110 ( 80-126 ) 30 ug/L 12/18/2008 LCSD 32.9 110 0 (< 20 ) 30 ug/L 12/18/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45
Batch Method Date Prep 

### 876588 Lab Control Sample 876589 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,1,1,2-Tetrachloroethane LCS 32.4 108 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.6 109 1 (< 20 ) 30 ug/L 12/18/2008

Chloroform LCS 32.2 107 ( 80-124 ) 30 ug/L 12/18/2008 LCSD 33.0 110 3 (< 20 ) 30 ug/L 12/18/2008

Bromobenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 31.4 105 0 (< 20 ) 30 ug/L 12/18/2008

Chloromethane LCS 32.7 109 ( 67-125 ) 30 ug/L 12/18/2008 LCSD 31.8 106 3 (< 20 ) 30 ug/L 12/18/2008
1,2,3-Trichloropropane LCS 31.9 106 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.9 110 3 (< 20 ) 30 ug/L 12/18/2008

Bromomethane LCS 32.2 107 ( 30-140 ) 30 ug/L 12/18/2008 LCSD 31.6 105 2 (< 20 ) 30 ug/L 12/18/2008

Bromochloromethane LCS 32.2 107 ( 77-129 ) 30 ug/L 12/18/2008 LCSD 32.4 108 1 (< 20 ) 30 ug/L 12/18/2008
Vinyl chloride LCS 32.9 110 ( 72-145 ) 30 ug/L 12/18/2008 LCSD 32.0 107 3 (< 20 ) 30 ug/L 12/18/2008

Dichlorodifluoromethane LCS 32.6 109 ( 62-153 ) 30 ug/L 12/18/2008 LCSD 31.8 106 3 (< 20 ) 30 ug/L 12/18/2008

Chloroethane LCS 34.1 114 ( 67-133 ) 30 ug/L 12/18/2008 LCSD 33.5 112 2 (< 20 ) 30 ug/L 12/18/2008
sec-Butylbenzene LCS 33.6 112 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 33.2 111 1 (< 20 ) 30 ug/L 12/18/2008

Bromodichloromethane LCS 31.1 104 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 31.4 105 1 (< 20 ) 30 ug/L 12/18/2008

1,1-Dichloroethene LCS 34.2 114 ( 76-130 ) 30 ug/L 12/18/2008 LCSD 34.4 115 1 (< 20 ) 30 ug/L 12/18/2008
2-Butanone (MEK) LCS 93.1 103 ( 66-136 ) 90 ug/L 12/18/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45
Batch Method Date Prep 

### 876588 Lab Control Sample 876589 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 102 114 9 (< 20 ) 90 ug/L 12/18/2008
Methylene chloride LCS 33.1 110 ( 63-131 ) 30 ug/L 12/18/2008 LCSD 31.4 105 5 (< 20 ) 30 ug/L 12/18/2008

Trichlorofluoromethane LCS 35.4 118 ( 68-145 ) 30 ug/L 12/18/2008 LCSD 34.2 114 3 (< 20 ) 30 ug/L 12/18/2008
P & M -Xylene LCS 65.5 109 ( 80-120 ) 60 ug/L 12/18/2008 LCSD 66.5 111 2 (< 20 ) 60 ug/L 12/18/2008
Naphthalene LCS 30.8 103 ( 75-120 ) 30 ug/L 12/18/2008 LCSD 29.8 99 3 (< 20 ) 30 ug/L 12/18/2008
o-Xylene LCS 32.9 110 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.7 109 1 (< 20 ) 30 ug/L 12/18/2008

Bromoform LCS 34.0 113 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 34.4 115 1 (< 20 ) 30 ug/L 12/18/2008

1-Chlorohexane LCS 50.8 113 ( 70-125 ) 45 ug/L 12/18/2008 LCSD 50.4 112 1 (< 20 ) 45 ug/L 12/18/2008
1,2,4-Trimethylbenzene LCS 32.8 109 ( 80-125 ) 30 ug/L 12/18/2008 LCSD 32.4 108 1 (< 20 ) 30 ug/L 12/18/2008
tert-Butylbenzene LCS 34.5 115 ( 80-122 ) 30 ug/L 12/18/2008 LCSD 34.1 114 1 (< 20 ) 30 ug/L 12/18/2008

1,1,1-Trichloroethane LCS 31.0 103 ( 80-122 ) 30 ug/L 12/18/2008 LCSD 31.3 104 1 (< 20 ) 30 ug/L 12/18/2008

1,1-Dichloroethane LCS 33.3 111 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

2-Chlorotoluene LCS 32.5 108 ( 80-125 ) 30 ug/L 12/18/2008 LCSD 32.3 108 1 (< 20 ) 30 ug/L 12/18/2008

Trichloroethene LCS 32.4 108 ( 80-125 ) 30 ug/L 12/18/2008 LCSD 32.9 110 2 (< 20 ) 30 ug/L 12/18/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45
Batch Method Date Prep 

### 876588 Lab Control Sample 876589 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### trans-1,2-Dichloroethene LCS 32.4 108 ( 79-132 ) 30 ug/L 12/18/2008 LCSD 32.2 107 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dichlorobenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 31.6 105 0 (< 20 ) 30 ug/L 12/18/2008
2,2-Dichloropropane LCS 34.5 115 ( 80-132 ) 30 ug/L 12/18/2008 LCSD 33.8 113 2 (< 20 ) 30 ug/L 12/18/2008

Hexachlorobutadiene LCS 32.2 107 ( 77-125 ) 30 ug/L 12/18/2008 LCSD 31.7 106 1 (< 20 ) 30 ug/L 12/18/2008
Isopropylbenzene (Cumene) LCS 34.3 114 ( 80-121 ) 30 ug/L 12/18/2008 LCSD 34.1 114 1 (< 20 ) 30 ug/L 12/18/2008
1,2-Dichloropropane LCS 32.0 107 ( 80-121 ) 30 ug/L 12/18/2008 LCSD 32.7 109 2 (< 20 ) 30 ug/L 12/18/2008
1,1-Dichloropropene LCS 32.4 108 ( 80-122 ) 30 ug/L 12/18/2008 LCSD 32.3 108 0 (< 20 ) 30 ug/L 12/18/2008

1,1,2-Trichloroethane LCS 32.3 108 ( 77-120 ) 30 ug/L 12/18/2008 LCSD 32.5 108 0 (< 20 ) 30 ug/L 12/18/2008

1,3-Dichlorobenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 12/18/2008 LCSD 32.0 107 0 (< 20 ) 30 ug/L 12/18/2008

1,2,3-Trichlorobenzene LCS 31.0 103 ( 77-120 ) 30 ug/L 12/18/2008 LCSD 30.6 102 1 (< 20 ) 30 ug/L 12/18/2008

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 99 ( 73-120 ) 12/18/2008 LCSD 100 2 12/18/2008

Toluene-d8 <surr> LCS 99 ( 80-120 ) 12/18/2008 LCSD 100 1 12/18/2008

4-Bromofluorobenzene <surr> LCS 98 ( 76-120 ) 12/18/2008 LCSD 98 0 12/18/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 12/22/2008 11:45
Batch Method Date Prep 

### 876588 Lab Control Sample 876589 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX19107 SW5030B 12/18/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS10317

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Printed Date/Time 

### 12/22/2008 11:45 Batch Method Date Original Prep 

### 876591 Matrix Spike 876592 Matrix Spike Duplicate

876590 Water (Surface, Eff., Ground) VXX19107 Volatiles Extraction AFCEE 3.1 8260 (W) 12/18/2008

QC results affect the following production samples: 

### 1086721001, 1086721002, 1086721003

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene MS ND 33 110 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.2 114 4 (< 20 ) 30.0 ug/L 12/18/2008 Toluene MS ND 32.2 107 ( 77-120 ) 30.0 ug/L 12/18/2008 MSD 33.4 111 4 (< 20 ) 30.0 ug/L 12/18/2008 Ethylbenzene MS ND 33.1 110 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.1 114 3 (< 20 ) 30.0 ug/L 12/18/2008 n-Butylbenzene MS ND 35.1 117 ( 80-124 ) 30.0 ug/L 12/18/2008 MSD 37.7 126 * 7 (< 20 ) 30.0 ug/L 12/18/2008 1,4-Dichlorobenzene MS ND 33 110 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 35.3 118 7 (< 20 ) 30.0 ug/L 12/18/2008 1,2-Dichloroethane MS ND 38 127 ( 80-129 ) 30.0 ug/L 12/18/2008 MSD 34.5 115 10 (< 20 ) 30.0 ug/L 12/18/2008 1,3,5-Trimethylbenzene MS ND 33.8 113 ( 80-128 ) 30.0 ug/L 12/18/2008 MSD 35.4 118 5 (< 20 ) 30.0 ug/L 12/18/2008 4-Chlorotoluene MS ND 33.7 112 ( 79-128 ) 30.0 ug/L 12/18/2008 MSD 35.3 118 5 (< 20 ) 30.0 ug/L 12/18/2008 Chlorobenzene MS ND 30.5 102 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 31.5 105 3 (< 20 ) 30.0 ug/L 12/18/2008 4-Methyl-2-pentanone (MIBK) MS ND 102 113 ( 69-134 ) 90.0 ug/L 12/18/2008 MSD 103 115 1 (< 20 ) 90.0 ug/L 12/18/2008 cis-1,2-Dichloroethene MS ND 38.6 129* ( 80-125 ) 30.0 ug/L 12/18/2008 MSD 36.3 121 6 (< 20 ) 30.0 ug/L 12/18/2008 4-Isopropyltoluene MS ND 34.1 114 ( 80-125 ) 30.0 ug/L 12/18/2008 MSD 36.4 121 7 (< 20 ) 30.0 ug/L 12/18/2008 cis-1,3-Dichloropropene MS ND 31.7 106 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 31.9 106 1 (< 20 ) 30.0 ug/L 12/18/2008 n-Propylbenzene MS ND 33.8 113 ( 80-129 ) 30.0 ug/L 12/18/2008 MSD 35.4 118 5 (< 20 ) 30.0 ug/L 12/18/2008 Styrene MS ND 31.2 104 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 31.5 105 1 (< 20 ) 30.0 ug/L 12/18/2008 Dibromomethane MS ND 37.2 124* ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.1 114 9 (< 20 ) 30.0 ug/L 12/18/2008 trans-1,3-Dichloropropene MS ND 33.6 112 ( 80-124 ) 30.0 ug/L 12/18/2008 MSD 33.5 112 0 (< 20 ) 30.0 ug/L 12/18/2008 1,2,4-Trichlorobenzene MS ND 31.7 106 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.1 114 7 (< 20 ) 30.0 ug/L 12/18/2008 Acetone MS ND 104 116 ( 50-135 ) 90.0 ug/L 12/18/2008Matrix SGS Ref.# Printed Date/Time 

### 12/22/2008 11:45 Batch Method Date Original Prep 

### 876591 Matrix Spike 876592 Matrix Spike Duplicate

876590 Water (Surface, Eff., Ground) VXX19107 Volatiles Extraction AFCEE 3.1 8260 (W) 12/18/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### MSD 102 114 2 (< 20 ) 90.0 ug/L 12/18/2008 1,1,2,2-Tetrachloroethane MS ND 34.1 114 ( 76-123 ) 30.0 ug/L 12/18/2008 MSD 34.8 116 2 (< 20 ) 30.0 ug/L 12/18/2008 1,2-Dibromo-3-chloropropane MS ND 35.2 117 ( 73-130 ) 30.0 ug/L 12/18/2008 MSD 36.1 120 2 (< 20 ) 30.0 ug/L 12/18/2008 Methyl-t-butyl ether MS ND 55 122* ( 80-120 ) 45.0 ug/L 12/18/2008 MSD 53.2 118 3 (< 20 ) 45.0 ug/L 12/18/2008 Tetrachloroethene MS ND 32.4 108 ( 79-122 ) 30.0 ug/L 12/18/2008 MSD 32.9 110 2 (< 20 ) 30.0 ug/L 12/18/2008 Dibromochloromethane MS ND 34.5 115 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 33.4 111 3 (< 20 ) 30.0 ug/L 12/18/2008 1,3-Dichloropropane MS ND 35.1 117 ( 80-121 ) 30.0 ug/L 12/18/2008 MSD 34.4 115 2 (< 20 ) 30.0 ug/L 12/18/2008 1,2-Dibromoethane MS ND 34.5 115 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 33.8 113 2 (< 20 ) 30.0 ug/L 12/18/2008 Carbon tetrachloride MS ND 36.5 122 ( 80-126 ) 30.0 ug/L 12/18/2008 MSD 35.1 117 4 (< 20 ) 30.0 ug/L 12/18/2008 1,1,1,2-Tetrachloroethane MS ND 33.1 110 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 32.6 109 2 (< 20 ) 30.0 ug/L 12/18/2008 Chloroform MS ND 38.5 128* ( 80-124 ) 30.0 ug/L 12/18/2008 MSD 35.1 117 9 (< 20 ) 30.0 ug/L 12/18/2008 Bromobenzene MS ND 32.4 108 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 33.6 112 4 (< 20 ) 30.0 ug/L 12/18/2008 Chloromethane MS ND 28.8 96 ( 67-125 ) 30.0 ug/L 12/18/2008 MSD 31.3 104 8 (< 20 ) 30.0 ug/L 12/18/2008 1,2,3-Trichloropropane MS ND 32.7 109 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.8 116 6 (< 20 ) 30.0 ug/L 12/18/2008 Bromomethane MS ND 32 107 ( 30-140 ) 30.0 ug/L 12/18/2008 MSD 33.8 113 6 (< 20 ) 30.0 ug/L 12/18/2008 Bromochloromethane MS ND 34 113 ( 77-129 ) 30.0 ug/L 12/18/2008 MSD 33.8 113 1 (< 20 ) 30.0 ug/L 12/18/2008 Vinyl chloride MS ND 31 103 ( 72-145 ) 30.0 ug/L 12/18/2008 MSD 32.0 107 3 (< 20 ) 30.0 ug/L 12/18/2008 Dichlorodifluoromethane MS ND 33.3 111 ( 62-153 ) 30.0 ug/L 12/18/2008 MSD 33.8 113 2 (< 20 ) 30.0 ug/L 12/18/2008 Chloroethane MS ND 49.8 166* ( 67-133 ) 30.0 ug/L 12/18/2008 MSD 51.3 171 * 3 (< 20 ) 30.0 ug/L 12/18/2008 sec-Butylbenzene MS ND 34.1 114 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 35.9 120 5 (< 20 ) 30.0 ug/L 12/18/2008 Bromodichloromethane MS ND 34.5 115 ( 80-120 ) 30.0 ug/L 12/18/2008Matrix SGS Ref.# Printed Date/Time 

### 12/22/2008 11:45 Batch Method Date Original Prep 

### 876591 Matrix Spike 876592 Matrix Spike Duplicate

876590 Water (Surface, Eff., Ground) VXX19107 Volatiles Extraction AFCEE 3.1 8260 (W) 12/18/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### MSD 32.6 109 5 (< 20 ) 30.0 ug/L 12/18/2008 1,1-Dichloroethene MS ND 37.4 125 ( 76-130 ) 30.0 ug/L 12/18/2008 MSD 35.8 119 5 (< 20 ) 30.0 ug/L 12/18/2008 2-Butanone (MEK) MS ND 105 117 ( 66-136 ) 90.0 ug/L 12/18/2008 MSD 105 116 0 (< 20 ) 90.0 ug/L 12/18/2008 Methylene chloride MS ND 31.4 105 ( 63-131 ) 30.0 ug/L 12/18/2008 MSD 32.3 108 3 (< 20 ) 30.0 ug/L 12/18/2008 Trichlorofluoromethane MS ND 38 127 ( 68-145 ) 30.0 ug/L 12/18/2008 MSD 37.4 125 2 (< 20 ) 30.0 ug/L 12/18/2008 P & M -Xylene MS ND 66.4 111 ( 80-120 ) 60.0 ug/L 12/18/2008 MSD 68.6 114 3 (< 20 ) 60.0 ug/L 12/18/2008 Naphthalene MS ND 31.3 104 ( 75-120 ) 30.0 ug/L 12/18/2008 MSD 34.1 114 8 (< 20 ) 30.0 ug/L 12/18/2008 o-Xylene MS ND 32.9 110 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 33.9 113 3 (< 20 ) 30.0 ug/L 12/18/2008 Bromoform MS ND 34.6 115 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.2 114 1 (< 20 ) 30.0 ug/L 12/18/2008 1-Chlorohexane MS ND 53.6 119 ( 70-125 ) 45.0 ug/L 12/18/2008 MSD 55.6 123 4 (< 20 ) 45.0 ug/L 12/18/2008 1,2,4-Trimethylbenzene MS ND 33.2 111 ( 80-125 ) 30.0 ug/L 12/18/2008 MSD 34.8 116 5 (< 20 ) 30.0 ug/L 12/18/2008 tert-Butylbenzene MS ND 34.8 116 ( 80-122 ) 30.0 ug/L 12/18/2008 MSD 36.8 123 * 6 (< 20 ) 30.0 ug/L 12/18/2008 1,1,1-Trichloroethane MS ND 34.5 115 ( 80-122 ) 30.0 ug/L 12/18/2008 MSD 33.0 110 5 (< 20 ) 30.0 ug/L 12/18/2008 1,1-Dichloroethane MS ND 37 123* ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.8 116 6 (< 20 ) 30.0 ug/L 12/18/2008 2-Chlorotoluene MS ND 32.8 109 ( 80-125 ) 30.0 ug/L 12/18/2008 MSD 34.8 116 6 (< 20 ) 30.0 ug/L 12/18/2008 Trichloroethene MS ND 33 110 ( 80-125 ) 30.0 ug/L 12/18/2008 MSD 34.4 115 4 (< 20 ) 30.0 ug/L 12/18/2008 trans-1,2-Dichloroethene MS ND 38.4 128 ( 79-132 ) 30.0 ug/L 12/18/2008 MSD 34.2 114 12 (< 20 ) 30.0 ug/L 12/18/2008 1,2-Dichlorobenzene MS ND 32.4 108 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 33.9 113 4 (< 20 ) 30.0 ug/L 12/18/2008 2,2-Dichloropropane MS ND 39.7 132 ( 80-132 ) 30.0 ug/L 12/18/2008 MSD 38.6 129 3 (< 20 ) 30.0 ug/L 12/18/2008 Hexachlorobutadiene MS ND 33.8 113 ( 77-125 ) 30.0 ug/L 12/18/2008 MSD 35.9 120 6 (< 20 ) 30.0 ug/L 12/18/2008 Isopropylbenzene (Cumene) MS ND 34.8 116 ( 80-121 ) 30.0 ug/L 12/18/2008Matrix SGS Ref.# Printed Date/Time 

### 12/22/2008 11:45 Batch Method Date Original Prep 

### 876591 Matrix Spike 876592 Matrix Spike Duplicate

876590 Water (Surface, Eff., Ground) VXX19107 Volatiles Extraction AFCEE 3.1 8260 (W) 12/18/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### MSD 35.5 118 2 (< 20 ) 30.0 ug/L 12/18/2008 1,2-Dichloropropane MS ND 33.3 111 ( 80-121 ) 30.0 ug/L 12/18/2008 MSD 34.3 114 3 (< 20 ) 30.0 ug/L 12/18/2008 1,1-Dichloropropene MS ND 34.4 115 ( 80-122 ) 30.0 ug/L 12/18/2008 MSD 34.8 116 1 (< 20 ) 30.0 ug/L 12/18/2008 1,1,2-Trichloroethane MS ND 33.7 112 ( 77-120 ) 30.0 ug/L 12/18/2008 MSD 33.4 111 1 (< 20 ) 30.0 ug/L 12/18/2008 1,3-Dichlorobenzene MS ND 32.7 109 ( 80-120 ) 30.0 ug/L 12/18/2008 MSD 34.6 115 6 (< 20 ) 30.0 ug/L 12/18/2008 1,2,3-Trichlorobenzene MS ND 31.2 104 ( 77-120 ) 30.0 ug/L 12/18/2008 MSD 33.6 112 7 (< 20 ) 30.0 ug/L 12/18/2008 Surrogates 

### 1,2-Dichloroethane-D4 <surr> MS 34.2 114 ( 73-120 ) 12/18/2008 MSD 29.9 100 13 12/18/2008 Toluene-d8 <surr> MS 29.7 99 ( 80-120 ) 12/18/2008 MSD 29.3 98 2 12/18/2008 4-Bromofluorobenzene <surr> MS 29.3 98 ( 76-120 ) 12/18/2008 MSD 29.6 99 1 12/18/2008
Batch Method Instrument 

### VMS10317

SW8260B HP 5890 Series II MS3 VNA