Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

February 2009 

Prepared by: 

TEC Inc. 

1001 Bishop St. Suite 1400 

American Savings Bank Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
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Red Hill Fuel Storage Facility February 2009 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 5

1.1 Project Objective .............................................................................................................. 5

1.2 Previous Reports .............................................................................................................. 5

1.3 Background ...................................................................................................................... 6

1.3.1 Site Description ......................................................................................................... 6

1.3.2 Facility Information .................................................................................................. 6

1.3.3 UST Information ....................................................................................................... 6

1.4 Previous Environmental Investigations ............................................................................ 6

1.5 Regulatory Updates .......................................................................................................... 8

2.0 Sample Collection and Analyses ........................................................................................ 10

2.1 Monitoring Well Purging ............................................................................................... 10

2.2 Groundwater Sample Collection .................................................................................... 10

2.3 Groundwater Sample Analyses ...................................................................................... 10

3.0 Groundwater Sample Analytical Results ........................................................................... 11

3.1 October 2008 Sample Analytical Results ....................................................................... 11

3.2 Groundwater Contaminant Trend ................................................................................... 14

3.3 Results of Oil/Water Interface Measurements ............................................................... 14

3.4 Groundwater Status ........................................................................................................ 15

4.0 Summary and Conclusions ................................................................................................. 18

5.0 References .......................................................................................................................... 22

List of Tables 

Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ..13 

Table 2 Oil/Water Interface Measurements ..............................................................................15 

Table 3 Action Levels for Compounds of Concern ..................................................................15 

Table 4 Responses to Groundwater Monitoring Results ..........................................................16 

List of Figures 

Figure 1 TPH Trends in Groundwater, Round 13 (October 22, 2008) ......................................20 

Figure 2 PAH Trends in Groundwater, Round 13 (October 22, 2008) ......................................21 

List of Appendices 

Appendix A – Laboratory Analytical Reports 
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Red Hill Fuel Storage Facility February 2009 

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Executive Summary 

This Quarterly Groundwater Monitoring Report presents the results of groundwater sampling 

conducted on October 22, November 11, and December 16, 2008 at the United States (US) Navy 

Bulk Fuel Storage Facility at Red Hill, Oahu, Hawaii (the Facility). The sampling and reporting 

was conducted by TEC Inc. (TEC) for the Air Force Center for Engineering and the Environment 

(AFCEE) and the Fleet Industrial Supply Center (FISC) at Pearl Harbor, Hawaii. This report is 

part of a series of quarterly groundwater monitoring reports provided by the US Navy to the 

State of Hawaii Department of Health (HDOH) in accordance with HDOH’s release response 

requirements. Currently, there are 18 active and 2 inactive, 12.5 million gallon, field-constructed 

underground storage tanks (USTs) located at the Facility. 

Background 

In 2002, the United States (US) Navy installed a groundwater monitoring well (currently named 

RHMW01) into the basal aquifer, directly down-gradient from the Facility, within the lower 

access tunnel. Groundwater samples from this well indicated that petroleum from the Facility 

had migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly 

monitoring of the aquifer to protect their down-gradient drinking water resource associated with 

the US Navy Well 2254-01. The US Navy Well 2254-01 is located approximately 3,000 feet 

downgradient from the Red Hill Fuel Storage Facility and provides approximately 24 % of the 

potable water to the Pearl Harbor Water System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility lower access tunnel, a background groundwater 

monitoring well (RHMW04) up-gradient from the Facility at ground surface adjacent to the US 

Navy Firing Range, and a groundwater monitoring well within the US Navy Well 2254-01 

infiltration gallery (RHMW2254-01). 

All five wells were sampled twice as part of a comprehensive environmental investigation and 

risk assessment (TEC, 2006). For this investigation, groundwater samples were analyzed for 

petroleum constituents and compared against HDOH Drinking Water Environmental Action 

Levels (EALs) (HDOH, 2005a). In addition, a three-dimensional (3-D) groundwater model was 

developed to produce site-specific risk-based action levels (SSRBLs) for compounds of concern. 

The results of this modeling effort indicated that Jet Propulsion (JP)–5 fuel presented the biggest 

risk to the US Navy water supply, due to its mobility and toxicity. Finally, the model indicated 

that a non-aqueous plume (free product) of JP-5 must migrate to within 1,100 feet of the US 

Navy Well 2254-01 infiltration gallery for HDOH EALs to be exceeded within the gallery. 

Based on this, free-product must be observed at RHMW01 for EALs to be exceeded at the US 

Navy Well 2254-01. 

During the Summer and Fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds were each previously 240 g/L, assuming they were not carcinogens. 

Evidence that they are carcinogenic to humans has now been accepted by the United States 
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Environmental Protection Agency (USEPA), and HDOH adopted more rigorous EALs of 4.7 

g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene (HDOH, 2008). 

The drinking water EAL for naphthalene was also updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels (HDOH, 2008). 

Finally, the drinking water EAL for TPH-DRO was increased from 100 g/L to 210 g/L, 

although the gross contamination EAL for TPH-DRO remains 100 g/L. 

Groundwater Protection Plan 

In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater 

Protection Plan (TEC, 2008), or Plan, which specified SSRBLs for each well, and actions that 

would occur for the pertinent cases, based on categories for each groundwater monitoring well 

(Categories 1 through 4). The main object of the Plan is to protect groundwater quality entering 

the US Navy Well 2254-01, which provides potable water to the PHWS. This is accomplished 

by comparing petroleum concentrations in the Facility wells (RHMW01, RHMW02, and 

RHMW03) to the SSRBLs and taking the corresponding action. A secondary but important 

objective of the Plan is to identify leaking USTs by evaluating increasing concentration trends, 

or the sudden and lasting presence of free product in one or more groundwater monitoring wells. 

In the current quarterly groundwater monitoring report, the current water quality is compared to 

these categories and actions are recommended, based on those specified in the Plan. 

Current Results 

In October 2008, four normal samples were collected from RHMW01, RHMW02, RHMW03 

and the US Navy Well 2254-01, along with the required quality control samples (duplicate, 

matrix spike, spike duplicate, trip blank). Samples were analyzed for Total Petroleum 

Hydrocarbons (TPH) quantified as Diesel-Range Organics (DRO) and Gasoline Range Organics 

(GRO), Volatile Organic Compounds (VOCs), Polynuclear Aromatic Hydrocarbons (PAHs), and 

lead. Naphthalene and 1-methylnaphthalene were detected at trace concentrations in the sample 

from US Navy Well 2254-01; therefore, the well was re-sampled in December 2008 for VOCs. 

VOCs were not detected in the re-sample aliquot. 

TPH-DRO was detected at 459 micrograms per liter (μg/L) in RHMW01, at 5,420 μg/L (average 

of normal and duplicate sample) in RHMW02, and 244 μg/L in RHMW03. The HDOH 

Drinking Water EAL and Site-Specific Risk Based Level for TPH-DRO are 210 μg/L and 4,500 

μg/L, respectively. Two PAHs were detected by USEPA method 8270C SIM in the normal and 

duplicate samples associated with RHMW02 at average concentrations above the HDOH 

Drinking Water EALs: naphthalene at 89.85 μg/L (HDOH EAL is 17 μg/L) and 1-

methylnaphthalene at 67.25 μg/L (HDOH toxicity EAL is 4.7 μg/L). Naphthalene was also 

measured by USEPA method 8260B in RHMW02, at an average concentration of 242 μg/L. 
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Trend Analysis 

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005 but less than 25 percent of the SSRBL of 4,500 g/L. In October 

2008, TPH-DRO increased in concentration following a decreasing trend over three previous 

rounds, since January 2008. 

At RHMW02, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005 and greater than 50 percent of the SSRBL of 4,500 g/L over that 

same period. TPH-DRO has been increasing in concentration over the last four rounds, since 

January 2008, and the average concentration from the October 2008 sampling event was greater 

than the SSRBL (solubility limit). Three PAHs (naphthalene, 1-methylnaphthalene, and 2-

methylnaphthalene) also have exceeded the EALs since September 2005. In October 2008, these 

PAHs decreased in concentrations following increasing trends over three previous rounds (since 

January 2008). There are no SSRBLs set for these PAHs to date. 

At RHMW03, concentrations of TPH-DRO have fluctuated around the HDOH EAL since 

September 2005 and are significantly lower than at RHMW01 and RHMW02. TPH-DRO at 

RHMW03 has been increasing in concentration over the past three rounds, since April 2008. 

Current Groundwater Status 

Based on the monitoring event that occurred in October 2008, no free product was observed at 

RHMW01, RHMW02, or RHMW03. Results from groundwater samples indicate that 

RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is greater than the 

HDOH EAL for drinking water (210 g/L), but less than half the SSRBL of 4,500 g/L 

(solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Results from groundwater samples indicate that RHMW02 is presently in Category 4 status, 

since TPH-DRO (4,540 g/L and 6,300 g/L [duplicate]) is greater than the HDOH EAL for 

drinking water (210 g/L), and greater than the SSRBL of 4,500 g/L (solubility limit of JP-5). 

Category 4 response at RHMW02 requires: 

A. Send quarterly reports to HDOH 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report to HDOH 

F. Send Type 2 Report to HDOH 

I. Remove sampling pumps, measure product in pertinent wells with interface probe, reinstall pumps if product is not detected. 

J. Immediately evaluate tanks for leaks 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF 

MW01 
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M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

Conclusions and Recommendations 

There is no indication of an imminent threat to the US Navy Well 2254-01 water resources based 

on this report, since petroleum concentrations at RHMW01 remain less than half the SSRBLs. 

However, the groundwater status at RHMW02 is Category 4 since the associated TPH-DRO 

result was greater than the SSRBL (4,500 g/L). The Groundwater Protection Plan requires 

specific responses to Category 4, which should be conducted. 

The US Navy plans to install an additional monitoring well in the Facility lower access tunnel 

and dedicated oil/water interface probes in four lower access tunnel wells in the coming year to 

better monitor contaminant migration in the basal drinking water aquifer. 

It is also recommended that quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, 

PAHs, and lead be continued as previously scheduled until new data indicates a different 

schedule is required.
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1.0 Introduction

This report presents the results of the 13th groundwater sampling and analysis event, conducted 

in October 2008 (with follow-up sampling in November and December) at the Red Hill Fuel 

Storage Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). The Facility consists of 

18 active and 2 inactive underground storage tanks (USTs) operated by the Fleet Industrial and 

Supply Center (FISC), Pearl Harbor. The groundwater sampling and analysis event is part of a 

groundwater monitoring program for the UST site in response to past UST releases, previous 

environmental investigations, and recommendations from the State of Hawaii Department of 

Health (HDOH). 

1.1 Project Objective 

This groundwater sampling and analysis project was performed to evaluate the presence of 

chemicals of potential concern in groundwater underlying the Facility. The project was 

conducted to ensure the Navy remains in compliance with HDOH UST release response 

requirements as described in Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release 

Response Action. The groundwater sampling and analysis procedures generally followed the 

procedures described in Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan (TEC 

Inc [TEC], 2008) (Also referred to as “the Plan”). 

This groundwater sampling and analysis event was conducted by TEC under Air Force Center 

for Engineering and the Environment (AFCEE) Contract Number F41624-03-D-8618, Task 

Order 021. 

1.2 Previous Reports 

The following groundwater monitoring reports were previously submitted to the HDOH: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); and 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008). 
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1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the 

Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south 

and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east 

of the Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet hydraulically down-gradient from the Facility (Dawson, 2006). The US Navy Well 

2254-01 is located approximately 3,000 feet down-gradient (west) of the Facility and provides 

approximately 24 % of the potable water to the Pearl Harbor Water System, which serves 

approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel). Previously, several tanks stored 

Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Previous Environmental Investigations 

1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess 

potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy 

installed a one-inch diameter sentinel well RHMW01 (previously known as MW-V1D) to 

monitor for contamination of the basal aquifer underlying the Facility. The well was installed 

and completed at approximately 100 feet below grade within the underground access tunnel. At 

the time of well completion, depth to water in RHMW01 was measured at 86 feet below grade 

(Dawson, 2006). 

In February 2001, groundwater samples collected from sentinel well RHMW01 contained total 

petroleum hydrocarbons (TPH) concentrations ranging from 883 micrograms per liter (g/L) to 

1,050 g/L and total lead ranging from 10.4 g/L to 15 g/L. The maximum total lead 

concentration in the samples was equal to the primary drinking water standard of 15 g/L for 

lead and exceeded the HDOH Tier 1 groundwater action level of 5.6 g/L (Dawson, 2006). 
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2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing 

monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 

and the Red Hill Navy Pump Station (US Navy Well 2254-01) in February, June, September, and 

December 2005. 

Samples collected in February and June 2005 were not filtered in the field prior to analysis for 

lead. Analytical results for samples collected from RHMW01 indicated concentrations of total 

lead were above the HDOH Tier 1 action level of 5.6 g/L. The results were not considered 

appropriate for risk assessment since the sample had not been filtered. In addition, lead was not 

a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility 

construction material (TEC, 2007). 

Samples were filtered in September and December 2005, and dissolved lead concentrations were 

below the HDOH Tier 1 action level. Concentrations of all other contaminants of potential 

concern were below HDOH Tier 1 action levels. 

2005 – Site Investigation: As part of a site investigation, TEC installed three groundwater 

monitoring wells at the Facility between June and September 2005. Well RHMW02 was 

installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the 

lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically 

upgradient of the USTs to provide geochemistry for water moving through the basal aquifer 

beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of 

approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of 

approximately 300 feet below ground surface outside the tunnel. Groundwater samples were 

collected from the three newly installed wells and two existing wells (RHMW01 and US Navy 

Well 2254-01) in September 2005. 

Naphthalene and trichloroethylene were detected in samples collected from RHMW02 at 

concentrations greater than the HDOH Tier 1 action levels. Lead was detected in the sample 

collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; 

however, the sample was not filtered in the field prior to analysis. Analytical results for filtered 

samples obtained by Dawson during the same period indicated concentrations of dissolved lead 

were below the HDOH Tier 1 action level. 

2006 – Site Investigation: Dedicated sampling pumps were installed in five wells (RHMW01, 

RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater 

samples from the wells in July 2006. The groundwater samples were analyzed for petroleum 

constituents. Naphthalene was detected in samples collected from RHMW02 at concentrations 

above the HDOH Tier 1 action level. 

In September 2005, with concurrence from the HDOH, the Navy decided to use the newer 

HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk 

Assessment project. The EALs are current and provide action levels for more chemicals, and are 

much more useful for conducting screening risk assessments. Since the HDOH June 2005 Policy 

Letter stated that the two sets of action levels should not be mixed, the Tier 1 screening levels 
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presented in HAR Section 11-281-78 would no longer be used to evaluate environmental impact 

at the Facility. 

2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. 

Analytical results indicated the following: 

 No chemicals were detected in groundwater from US Navy Well 2254-01 or RHMW03; 

 TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH 

Drinking Water EALs in RHMW01; and 

 TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected 

in groundwater above the HDOH Drinking Water EALs in RHMW02. 

2007 – Groundwater Sampling: Groundwater samples were collected in March, June, and 

September 2007. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three 

sampling events; 

 TPH-GRO exceeded HDOH Drinking Water EALs at RHMW02 in March; 

 TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during 

all three sampling events; 

 1-methylnaphthalene and 2-methylnaphthalene exceeded HDOH Drinking Water EAL 

for taste and odor at RHMW02 during all three sampling events; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in June. 

2008 – Groundwater Sampling: Groundwater samples were collected in January, April, and 

July 2008. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01; 

 TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 

 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03. 

1.5 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was previously 240 g/L, assuming they were not carcinogens. 

Evidence that they are carcinogenic to humans has now been accepted by the United States 

Environmental Protection Agency (USEPA), and HDOH adopted more rigorous EALs of 4.7 

g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding to a 

residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 
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The drinking water EAL for naphthalene has also been updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels, a Hazard Index of 2.7 

(HDOH, 2008). 

Finally, the drinking water EAL for TPH-DRO was increased from 100 g/L to 210 g/L, 

although the gross contamination EAL for TPH-DRO remains 100 g/L. 
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2.0 Sample Collection and Analyses 

The majority of field activities relating to groundwater sample collection were conducted on 

October 22, 2008. Groundwater samples were collected from three monitoring wells located 

inside the Facility lower access tunnel and one monitoring well located at the Red Hill Navy 

Pump Station. Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage 

Facility Groundwater Protection Plan (TEC, 2008). A total of seven samples were collected; 

one normal sample from monitoring wells US Navy Well 2254-01, RHMW01, RHMW02 and 

RHMW03, one duplicate sample from RHMW02 (Sampled as RHMWA01 and reported as 

RHMW02-WG11D), and one matrix spike and matrix spike duplicate from US Navy Well 

2254-01. 

The groundwater at RHMW01 was resampled for dissolved lead on November 3, 2008 because 

the original sample was not filtered in the field. 

Due to trace concentrations of naphthalene detected in the October 22, 2008 sample from the US 

Navy Well 2254-01, an additional sample was collected for Volatile Organic Compounds (VOCs) 

at US Navy Well 2254-01 on December 16, 2008, including one duplicate for VOCs. 

2.1 Monitoring Well Purging 

The groundwater monitoring wells were purged and sampled using a dedicated pump system. 

Well purging was considered complete when no less than three successive water quality 

parameter measurements had stabilized within approximately 10 percent. Field parameters were 

measured at regular intervals during well purging and included pH, temperature, specific 

conductivity, dissolved oxygen, and turbidity. Purge water was disposed in the Facility oil/water 

separator system. 

2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. All wells were sampled 

directly from their dedicated bladder pump system. Samples were placed into sampling 

containers with appropriate preservatives (i.e., hydrochloric acid [HCl] for volatile organic 

analysis, nitric acid [HNO3] for dissolved lead). Dissolved lead samples were filtered in the field 

and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, 

polynuclear aromatic hydrocarbons (PAHs) by EPA Method 8270C SIM, and dissolved lead by 

EPA Method 6020. 
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3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

three monitoring wells located in the lower access tunnel of the Facility and one monitoring well 

located at the Red Hill Navy Pump Station. Duplicate sample results from monitoring wells 

RHMW02 and RHMW2254-01 are reported in this document as RHMW02D and RHMW2254-

01D, respectively. A summary of groundwater analytical results is included in Table 1. 

Complete analytical laboratory reports are provided in Appendix A. 

3.1 October 2008 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. Naphthalene and 1-methylnaphthalene were detected at US Navy Well 2254-01 at 0.05F 

μg/L and 0.03F μg/L, respectively. This is below the HDOH Drinking Water EALs of 17 μg/L 

for naphthalene and 4.7 μg/L for 1-methylnaphthlene. Data qualifier “F” indicates the result is 

between the method detection limit (MDL) and the reporting limit (RL) and considered an 

estimated value. However, naphthalene or 1-methynapthalene are generally not observed in 

groundwater from JP-5 releases when TPH is not detected. For this reason, these lowconcentration PAH results may not be from the groundwater, but the source of the expected 

cross-contamination is not known. Following the receipt of the preliminary results, FISC 

implemented an immediate re-sampling of the US Navy Well 2254-01 for VOCs, including 

naphthalene. 

RHMW01

Four petroleum constituents were detected at RHMW01: TPH-DRO, fluorene, naphthalene, and 

lead. TPH-DRO was detected at RHMW01 at 459 μg/L, which is above the HDOH Drinking 

Water EAL of 210 μg/L. All other petroleum constituents were below HDOH Drinking Water 

EALs at RHMW01. 

RHMW02

Eight petroleum constituents were detected at RHMW02: TPH-DRO, TPH-GRO, 1-

methylnaphthalene, 2-methylnaphthalene, acenaphthene, fluorene, naphthalene, benzene, and 

ethylbenzene. TPH-DRO was detected at RHMW02 in the normal and duplicate samples, at 

4,540 μg/L and 6,300 μg/L, respectively. Both results exceeded the HDOH EAL and sitespecific risk based level (SSRBL) (the HDOH EAL is 210 μg/L and the SSRBL is 4,500 μg/L). 

Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. USEPA 

Method 8260B produced the highest naphthalene concentrations, which averaged 242 μg/L from 

the normal and duplicate sample (HDOH EAL is 17 μg/L). In addition, 1-methylnaphthalene 

and 2-methylnapthalene were detected by USEPA Method 8270C SIM in the normal and 

duplicate samples. The average result for 1-methylnaphthalene was 67.25 μg/L, greater than the 

HDOH toxicity EAL of 4.7 μg/L. The average result for 2-methylnaphthalene was 13.2 μg/L, 

less than the HDOH toxicity EAL of 24 μg/L but greater than the HDOH taste and odor EAL of 

10 g/L. All other petroleum constituents were below HDOH Drinking Water EALs at 

RHMW02. 
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RHMW03

Four constituents were detected at RHMW03: TPH-DRO, 1-methylnaphthylene, 2-

methylnaphthalene, and naphthalene. TPH-DRO was detected at RHMW03 at 244 μg/L, slightly 

above the HDOH EAL of 210 μg/L. All other petroleum constituents were below HDOH 

Drinking Water EALs at RHMW03. 

US Navy Well 2254-01 as RHMW2254

RHMW2254 was sampled twice during this reporting period. On October 22, 2008, trace 

concentrations (less than the reporting limit but greater than the detection limit) of naphthalene 

(0.05 μg/L) and 1-methylnaphthalene (0.03 μg/L) were detected by USEPA Method 8270C SIM. 

On December 16, 2008, RHMW2254 was re-sampled by USEPA Method 8260B. Although no 

petroleum constituents were observed in the re-sample, the method detection limit for 

naphthalene was 0.62 μg/L and 1-methylnaphthalene was not analyzed. 
Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (October 22, 2008 and December 16, 2008)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL

TPH as DIESEL RANGE ORGANICS 210 100 459 82.50 412.00 4540 80.00 400.00 6300 98.20 491.00 244 F 88.40 442.00 ND U 84.20 421.00 NA NA NA NA NA NA NA NA TPH as GASOLINE RANGE ORGANICS 100 100 ND U 10.00 100.00 52.80 F 10.00 100.00 52.90 F 10.00 100.00 ND U 10.00 100.00 ND U 10.00 100.00 NA NA NA NA NA NA NA NA 1-METHYLNAPHTHALENE 4.7 10 ND U 0.015 0.05 72.10 0.781 2.6 62.40 0.75 2.5 0.07 0.0155 0.0515 0.03 F 0.015 0.05 NA NA NA NA NA NA NA NA 2-METHYLNAPHTHALENE 24 10 ND U 0.015 0.05 13.70 0.313 1.04 12.70 0.3 1 0.09 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA 

ACENAPHTHENE 370 20 ND U 0.015 0.05 0.37 0.0156 0.0521 0.21 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA 

ACENAPHTHYLENE 240 2000 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA ANTHRACENE 1800 22 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA BENZO(a)ANTHRACENE 0.092 5 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA BENZO(a)PYRENE 0.2 1.9 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA 

BENZO(b)FLUORANTHENE 0.092 7 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA 

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA 

Method HDOH Residential 

Drinking Water EALs1

UG/L

Water Ceiling 

HDOH Drinking 

EALs2

UG/L

Chemical

RHMW01

UG/L

RHMW2254

UG/L

RHMW02

UG/L

RHMW02D

UG/L

RHMW03

UG/L

8015B (Petroleum)

8270C SIM (PAHs)

October 22, 2008 October 22, 2008 October 22, 2008 October 22, 2008 October 22, 2008

RHMW2254D

UG/L

December 16, 2008

RHMW2254

UG/L

December 16, 2008

CHRYSENE 9.2 0.8 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA DIBENZ(a,h)ANTHRACENE 0.0092 0.25 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA FLUORANTHENE 1500 130 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA FLUORENE 240 950 0.02 F 0.015 0.05 0.21 0.0156 0.0521 0.12 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA INDENO(1,2,3-c,d)PYRENE 0.092 0.27 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA NAPHTHALENE 17 21 0.10 0.031 0.1 97.40 1.61 5.21 82.30 1.55 5 0.22 0.032 0.103 0.05 F 0.031 0.1 NA NA NA NA NA NA NA NA 

PHENANTHRENE 240 410 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA PYRENE 180 68 ND U 0.015 0.05 ND U 0.0156 0.0521 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.015 0.05 NA NA NA NA NA NA NA NA 1,1,1,2-TETRACHLOROETHANE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.51,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2,4-TRICHLOROBENZENE 3.8 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 21,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 11,3-DICHLOROPROPANE 0.4 50000 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.41,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10BENZENE 5 170 ND U 0.12 0.4 0.14 F 0.12 0.4 0.15 F 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4

BROMODICHLOROMETHANE 0 18 50000 ND U 0 15 0 5 ND U 0 15 0 5 ND U 0 15 0 5 ND U 0 15 0 5 ND U 0 15 0 5 ND U 0 15 0 5 ND U 0 15 0 5 BROMODICHLOROMETHANE 0.18 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1BROMOMETHANE 8.5 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5CHLOROETHANE 3.9 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROFORM 100 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1CHLOROMETHANE 160 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DIBROMOMETHANE 0.0056 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1ETHYLBENZENE 1.5 30 ND U 0.31 1 0.45 F 0.31 1 0.42 F 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2METHYL ETHYL KETONE (2-BUTANONE) 7000 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYL ISOBUTYL KETONE 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYLENE CHLORIDE 4.3 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5NAPHTHALENE 17 21 ND U 0.62 2 239.00 12.4 40 245.00 12.4 40 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

8260B (VOCs)

( )

VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

6020 LEAD 15 50000 0.97 F 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 NA NA NA NA NA NA NA NA 

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method detection limit

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

U - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzed

- Result exceeds one or both HDOH EALs

21 Toxicity-based environmental action levels, Table D-1b, Screening For Environmental Concerns At Sites With 

Contaminated Soil and Groundwater, HDOH, 2008Taste, odor and solubility thresholds, Table G-1, Screening For Environmental Concerns At Sites With Contaminated Soil and Groundwater , HDOH, 2008

200

Page 1 of 1
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

14 

3.2 Groundwater Contaminant Trend 

Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 

shows TPH trends in groundwater at the Facility. Figure 2 shows PAH trends in groundwater at 

the Facility. In these figures, open icons (without fill) represent the method detection limit for 

chemicals that were not detected. 

RHMW01

TPH-GRO has only been detected in April 2008 at 13.6F μg/L, which is below the HDOH 

Drinking Water EAL of 100 μg/L. In October 2008, TPH-GRO was not detected. TPH-DRO 

was detected above the HDOH Drinking Water EAL during all groundwater sampling events and 

showed a decreasing trend until the January 2008 sampling event. Concentration of TPH-DRO 

observed during the October 2008 sampling event was greater than the concentrations observed 

in April and July 2008, but lower than the January 2008 sampling event. 

RHMW02

TPH-GRO was detected in nine of ten sampling events since September 2005, and exceeded the 

HDOH Drinking Water EAL three times during 2006 and 2007. The maximum concentration 

detected was 148 μg/L. The concentration of TPH-DRO was relatively stable at RHMW02 until 

January 2008, ranging from 2,250 to 3,180 μg/L. However, since January 2008 it has shown an 

increasing trend with concentrations up to 5,420 μg/L, well above the HDOH EAL, and above 

the SSRBL of 4,500 μg/L. PAHs at RHMW02 remain above the HDOH Drinking Water EALs, 

and concentrations have decreased in October 2008 after showing an increasing trend since 

January 2008. 

RHMW03

TPH-GRO has never been detected. TPH-DRO had shown a decreasing trend until the January 

2008 sampling event. Concentrations of TPH-DRO observed during the October 2008 sampling 

event were higher than the previous rounds. In general, concentrations of petroleum-related 

compounds at RHMW03 have been the lowest of the three wells located within the Facility. 

3.3 Results of Oil/Water Interface Measurements 

The presence and thickness of light-non aqueous phased liquids (LNAPL), otherwise known as 

free product, released from the USTs were measured during this sampling event using a 300 ft 

Heron Oil/Water Interface Meter. The static water levels were measured to a precision of ± 0.01 

ft and fuel thickness was measured to a precision of ± 0.01 ft with this equipment. 

In January 2008, fuel was measured in monitoring wells RHMW01 and RHMW02 at a thickness 

of < 0.01 ft, but has not been observed in other monitoring wells as of this document. 

Measurements to determine the presence and thickness of fuel were conducted at RHMW01, 

RHMW02, and RHMW03 during the current sampling round. No fuel product was observed in 

any of these wells during this event (see Table 2). 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

15 

Table 2. Oil/Water Interface Measurements 

Date 

RHMW01 RHMW02 RHMW03 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

 January 2008 17.74 < 0.01 18.78 < 0.01 NT NT 

 July 2008 19.04 0.00 18.91 0.00 18.86 0.00 

October 2008 18.61 0.00 18.56 0.00 18.82 0.00 

November 2008 18.50 0.00 18.45 0.00 18.51 0.00 

SWL Static water level, elevation above mean sea level 

LNAPL Light Non-Aqueous Phased Liquid, fuel product on groundwater 

ft Feet 

NT Not Taken 

3.4 Groundwater Status 

Compounds of concern are defined as those petroleum-related chemicals that have been observed 

in the groundwater samples above the HDOH EALs. In accordance with the Red Hill Bulk Fuel 

Storage Facility Final Groundwater Protection Plan (TEC, 2008), Table 3 defines the 

constituents of concern in groundwater at the Facility and the SSRBLs and updated EALs for 

each (HDOH 2008). 

Table 3. Action Levels for Constituents of Concern 

Chemical EAL (μg/L) SSRBL (μg/L) 

Petroleum Mixtures 

TPH-DRO 210 4,500 

TPH-GRO 100 4,500 

Semi-Volatile Compounds 

1-Methylnaphthalene 4.7 NA 

2-Methylnaphthalene 24 NA 

Naphthalene 17 NA 

NA – Not applicable or not determined 

SSRBLs are applicable at RHMW01, RHMW02, and RHMW03 

EALs are applicable at US Navy Well 2254-01 

In addition, the Plan defines four results categories of groundwater status for the Facility, based 

on concentrations of constituents of concern in RHMW01, RHMW02, RHMW03 and the US 

Navy Well 2254-01, and requires specific responses when these categories are observed during 

quarterly groundwater sampling. Table 4 describes each of the four results categories and 

identifies response actions to be taken in accordance with the Plan. 

 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

16 

Table 4. Results Categories and Response Actions to Changes in Groundwater Status 

Results Category RHMW02 or 

RHMW03 

RHMW01 US Navy Pumping 

Well 2254-01 

Results Category 1: Result above 

detection limit but below drinking 

water EAL and trend for all 

compounds stable or decreasing 

A A A,D,M,E,P 

Results Category 2: Trend for any 

compound increasing or drinking 

water EAL exceeded 

A, B A, B A,B,C,D,E,F,G,K, 

L,O 

Results Category 3: Result 

Between 1/10X SSRBL and 

SSRBL for benzene, or between 

1/2X SSRBL and SSRBL for TPH 

A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J,

K,L,O 

Results Category 4: Result 

Exceeding any SSRBL or 

petroleum product observed 

A,C,D,E,F,I,J, 

K,M,N 

A,C,D,E,F,I, 

J,K,M,N,O 

A,C,D,E,F,G,I,J,K,

L,O 

Specific Responses: 

A. Send quarterly reports to HDOH 

B. Begin program to determine the source of leak 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report (see box below) to HDOH 

F. Send Type 2 Report (see box below) to HDOH 

G. Increase monitoring frequency to once per month (if concentrations increasing) 

H. Notify HDOH verbally within 7 days and follow with written notification in 30 days 

I. Remove sampling pumps, measure product in pertinent wells with interface probe, re-install 

pumps if product is not detected. 

J. Immediately determine leaking tank 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01 

L. Provide alternative water source at 2254-01 

M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

O. Install additional monitoring well downgradient 

Report Types 

HDOH Type 1 Report 

 Re-evaluate Tier 3 Risk Assessment/groundwater model results 

 Proposal to HDOH on a course of action 

HDOH Type 2 Report 

 Proposal for groundwater treatment 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

17 

Based on the monitoring event that occurred in October and November 2008, no free product 

was observed at RHMW01, RHMW02, or RHMW03. Results from groundwater samples 

indicate that RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is 

greater than the HDOH EAL for drinking water (210 g/L), but less than half the SSRBL of 

4,500 g/L (solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Results from groundwater samples indicate that RHMW02 is presently in Category 4 status, 

since TPH-DRO (4,540 g/L and 6,300 g/L [duplicate]) is greater than the SSRBL of 4,500 

g/L (solubility limit of JP-5). Category 4 response at RHMW02 requires: 

A. Send quarterly reports to HDOH 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report to HDOH 

F. Send Type 2 Report to HDOH 

I. Remove sampling pumps measure product in pertinent wells with interface probe, re-install 

pumps if product is not detected. 

J. Immediately evaluate tanks for leaks 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01. 

 For permission to sample 2253-03, call DLNR Commission on Water Resource Management 

 (808) 587-0214, DLNR.CWRM@Hawaii.gov

M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

In response to the previous Category 3 conditions at RHMW02, oil/water interface 

measurements were collected in October 2008 and November 2008 at RHMW01, RHMW02 and 

RHMW03. To date, there is no evidence of fuel on groundwater at any of these wells based on 

oil/water interface measurements. 

Category 4 groundwater status at RHMW02 requires additional efforts, including: 

 Re-evaluate risk assessment and groundwater model (TEC, 2007) to ensure both are valid 

and protective of human health and the environment under the existing conditions and 

provide a report describing the results of this re-evaluation to the HDOH; 

 Evaluate potential requirement for groundwater treatment and provide a report describing 

the results of this re-evaluation to the HDOH; 

 Implement monthly oil/water interface measurements at RHMW01, RHMW02, 

RHMW03, and provide monthly letter reports of the results; 

 Evaluate tanks associated with the middle section of the Facility (Tanks 5, 6, 7, 8, 9, 10, 

11, 12, 13, and 14); 

 Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF 

MW01; 

 Prepare for alternative water source at US Navy Well 2254-01, as necessary. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

18 

4.0 Summary and Conclusions 

At RHMW02, the concentration of TPH-DRO in groundwater exceeded the SSRBL of 4,500 

g/L, which indicates Category 4 groundwater status at RHMW02. 

 The SSRBL of TPH-DRO is set at the solubility limit of JP-5 and exceeding the SSRBL 

implies that JP-5 is in direct contact with groundwater in the vicinity of RHMW02. 

 Oil/water interface measurements were collected in October 2008 and November 2008 

from RHMW01, RHMW02, and RHMW03 and no fuel thickness was measured. 

 The concentration of TPH-DRO measured at RHMW01 in October 2008 was one tenth 

of the SSRBL. RHMW01 is down-gradient from RHMW02 and between RHMW02 and 

the US Navy Well 2254-01, an important drinking water source for the Pearl Harbor 

Water System. 

 The US Navy Well 2254-01 is not imminently threatened at this time; however, 

conditions should be monitored closely to determine if any USTs in the Facility are 

currently leaking fuel into the subsurface. 

 Category 4 activities should be implemented, including: 

 Re-evaluate risk assessment and groundwater model (TEC, 2007) to ensure both 

are valid and protective of human health and the environment under the existing 

conditions and provide a report describing the results of this re-evaluation to the 

HDOH; 

 Evaluate potential requirement for groundwater treatment and provide a report 

describing the results of this re-evaluation to the HDOH; 

 Implement monthly oil/water interface measurements at RHMW01, RHMW02, 

RHMW03, and provide monthly letter reports of the results; 

 Evaluate tanks associated with the middle section of the Facility (Tanks 5, 6, 7, 8, 

9, 10, 11, 12, 13, and 14); 

 Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and 

OWDF MW01; 

 Prepare for alternative water source at US Navy Well 2254-01, as necessary. 

The US Navy plans to install an additional monitoring well (RHMW05) in the lower access 

tunnel of the Facility between RHMW01 and the US Navy Well 2254-01 to better monitor the 

quality of the groundwater moving from the Facility to the US Navy Well 2254-01. 

Although the results from the groundwater sample collected from US Navy Well 2254-01 in 

October 2008 showed trace concentrations of naphthalene and 1-methylnaphthalene, no other 

petroleum constituents were detected in this sample. This well was re-sampled in December 

2008. The sample was analyzed by USEPA Method 8620B and no petroleum constituents were 

detected. 

It is recommended that RHMW01, RHMW02, RHMW03, and RHMW05 be evaluated monthly 

for the presence of fuel on groundwater, in accordance with the Plan. The US Navy plans to 

install dedicated oil/water interface probes in each of these wells to facilitate these measurements. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

19 

 It is also recommended that quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, 

PAHs, and lead be continued as previously scheduled until new data indicates that a different 

schedule is required. The quarterly collection and analysis of groundwater samples will continue 

to monitor the quality of the groundwater located beneath the Facility. Groundwater monitoring 

reports will be submitted to the HDOH upon receipt and evaluation of laboratory analytical 

results. 
10000

TPH at RHMW02

QuarterlyMonitoring Results

10000

TPHat RHMW03

QuarterlyMonitoring Results

1000

(μg/L)1000 μg/L)

100

Concentration

100 Concentration

(μ

10 10

Time (Date)

GROEAL TPH‐DRO TPH‐GRO TPH‐GRO MDL SSRBL DRO EAL

Time (Date)

GROEAL TPH‐DRO TPH‐GRO MDL TPH‐DRO MDL SSRBL DRO EAL

10000

TPH at RHMW01

QuarterlyMonitoring Results

1000

ation (μg/L)

100

Concentr

10

Time (Date)

GRO EAL TPH‐DRO TPH‐GRO MDL TPH‐GRO SSRBL DROEAL

Figure 1

TPH Trends in Groundwater

Round 13 (October 22, 2008)

Red Hill Fuel Storage Facility (HDOH 2008) •TPH-GRO Residential Tap Water EAL is 100 ug/L;

•TPH-DRO Residential Tap Water EAL is 210 ug/L; andThe HDOH toxicity EALs were updated in Fall, 2008. 

g y

Oahu, Hawaii

(HDOH, 2008).
1000

PAHs at RHMW02

QuarterlyMonitoring Results

100

1000

10

tration (μg/L)

1

Concent

0.1

Time (Date)

Naphthalene 1‐Methylnaphthalene 2‐Methylnaphthalene Naph EAL* 1‐Meth EAL* 2‐Meth EAL*

Figure 2

PAH Trends in Groundwater

Round 13 (October 22, 2008)

Red Hill Fuel Storage Facility

• 1-methylnaphthalene Re• Naphthalene Residential Tap Water EAL is 17 ug/L;The HDOH toxicity EALs were updated in Fall, 2008. 

sidential Tap Water EAL is 4.7 ug/L; and

(HDOH 2008)• 2- methylnaphthalene Residential Tap Water EAL is 24 ug/L g y

Oahu, Hawaii

(HDOH, 2008).
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility February 2009 

 ____________________________________________________________________________________________ 

22 

5.0 References 

AMEC. 2002. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. 2006. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

State of Hawaii Department of Health (HDOH). 2005. Screening for Environmental Concerns 

at Sites with Contaminated Soil and Groundwater, Volume 1: Summary Tier 1 Lookup Tables. 

Interim Final. May 2005. 

State of Hawaii Department of Health. 2005a. Use of May 2005 Environmental Action Levels 

(“EALs”) at Leaking Underground Storage Tank Sites. Memo. 15 July. 

HDOH. 2008. Evaluation of Environmental Hazards at Sites With Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

The Environmental Company, Inc. and AMEC. 2005. Red Hill Bulk Fuel Storage Facility Work 

Plan, Pearl Harbor, Hawaii. June. 

TEC Inc. 2006. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, 

Pearl Harbor, Hawaii. May. 

TEC Inc. 2007. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, 

Hawaii. August. 

TEC Inc. 2008. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS Environmental Services

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

9121-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1085813
Case Narrative

THEENVC The Environmental Company, Inc. (TEC)

1085813 9121-003 Red Hill BFSF

Customer:

Project:

NPDL WO:

SGS Environmental Services Inc.

Refer to the sample receipt form for information on sample condition.

1085813001 PS RHMW2254-WG13

8015C DRO - LCS recovery is outside of acceptance criteria (biased low). The sample was re-extracted outside of 

the 14 day holding time and reanalyzed. The results did confirm with passing QC. Results for all associated 

samples are considered estimated.

1085813004 PS RHMW03-WG13

8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy.

1085813005 PS RHMW02-WG13

8015C DRO - The pattern is consistent with a weathered middle distillate.

8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy.

1085813006 PS RHMWA01-WG13

8015C DRO - The pattern is consistent with a weathered middle distillate.

8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy.

1085813007 PS RHMW01-WG13

8015C DRO - Unknown hydrocarbon with several peaks is present.

8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy.

1085813002 BMS RHMW2254-WG13 MS

8015C DRO - LCS recovery is outside of acceptance criteria (biased low). The sample was re-extracted outside of 

the 14 day holding time and reanalyzed. The results did confirm with passing QC. Results for all associated 

samples are considered estimated.

868545 MS 1085813001MS

8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy.

1085813003 BMSD RHMW2254-WG13 MSD

8015C DRO - LCS recovery is outside of acceptance criteria (biased low). The sample was re-extracted outside of 

the 14 day holding time and reanalyzed. The results did confirm with passing QC. Results for all associated 

samples are considered estimated.

868546 MSD 1085813001MSD

8015C DRO - MS/MSD were not spiked due to lab error. See LCS/LCSD for precision and accuracy.

869198 LCS XXX/20313]

8015C DRO - LCS recovery is outside of acceptance criteria (biased low). Results for all associated samples are 

considered estimated.
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1085813

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street Ste 1400

ASB Tower

Honolulu, HI 96813

Attn: Jeff Hart

T: (808)528-1445 F:(808)528-0768

jshart@tecinc.com

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343.

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 11/20/2008

Notes: All DRO/RRO analysese are integrated per SOP.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of SG S G roup
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 9121-003 Red Hill BFSF

Workorder No.: 1085813

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015B (W) SW8015C

GRO (W) SW8015C

Print Date: 11/20/2008

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1085813001 RHMW2254-WG13

1085813002 RHMW2254-WG13 MS

1085813003 RHMW2254-WG13 MSD

1085813004 RHMW03-WG13

1085813005 RHMW02-WG13

1085813006 RHMWA01-WG13

1085813007 RHMW01-WG13

1085813008 TB01-WG13

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW2254-WG13

SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5719 MXX21031

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5719

Analytical Method: SW6020

Analysis Date/Time: 11/14/08 20:12

Prep Batch: MXX21031

Prep Method: SW3010A

Prep Date/Time: 11/04/08 18:15 Container ID:1085813001-G

Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW2254-WG13

SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 10.0 ug/L 1 VFC9248 VXX18967

4-Bromofluorobenzene <surr> 99.1 50-150 % 1 VFC9248 VXX18967

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9248

Analytical Method: SW8015C

Analysis Date/Time: 10/30/08 10:09

Prep Batch: VXX18967

Prep Method: SW5030B

Prep Date/Time: 10/30/08 08:00 Container ID:1085813001-A

Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW2254-WG13

SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.421 0.0842 mg/L 1 XFC8338 XXX20313

5a Androstane <surr> 93.1 50-150 % 1 XFC8338 XXX20313

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8338

Analytical Method: SW8015C

Analysis Date/Time: 11/05/08 09:36

Prep Batch: XXX20313

Prep Method: SW3520C

Prep Date/Time: 11/03/08 17:15 Container ID:1085813001-I

Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW2254-WG13

SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

Toluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Styrene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Acetone ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10242 VXX18954

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

Chloroform ND 1.00 0.300 ug/L 1 VMS10242 VXX18954

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromomethane ND 3.00 0.940 ug/L 1 VMS10242 VXX18954

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW2254-WG13

SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10242 VXX18954

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Naphthalene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

o-Xylene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromoform ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane-D4 <surr> 105 73-120 % 1 VMS10242 VXX18954

Toluene-d8 <surr> 104 80-120 % 1 VMS10242 VXX18954

4-Bromofluorobenzene <surr> 111 76-120 % 1 VMS10242 VXX18954

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10242

Analytical Method: SW8260B

Analysis Date/Time: 10/27/08 17:17

Prep Batch: VXX18954

Prep Method: SW5030B

Prep Date/Time: 10/27/08 11:41 Container ID:1085813001-D

Dilution Factor: 1 Analyst: JDB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW2254-WG13

SGS Ref. #: 1085813001 Collection Date/Time: 10/22/08 09:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Acenaphthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Fluorene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Phenanthrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Chrysene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Naphthalene 0.0466 J 0.100 0.0310 ug/L 1 XMS4761 XXX20276

1-Methylnaphthalene 0.0276 J 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Terphenyl-d14 <surr> 92.2 50-135 % 1 XMS4761 XXX20276

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4761

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/30/08 14:48

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813001-J

Dilution Factor: 1 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW03-WG13

SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5719 MXX21031

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5719

Analytical Method: SW6020

Analysis Date/Time: 11/14/08 22:05

Prep Batch: MXX21031

Prep Method: SW3010A

Prep Date/Time: 11/04/08 18:15 Container ID:1085813004-G

Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW03-WG13

SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 10.0 ug/L 1 VFC9248 VXX18967

4-Bromofluorobenzene <surr> 94.8 50-150 % 1 VFC9248 VXX18967

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9248

Analytical Method: SW8015C

Analysis Date/Time: 10/30/08 11:18

Prep Batch: VXX18967

Prep Method: SW5030B

Prep Date/Time: 10/30/08 08:00 Container ID:1085813004-A

Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW03-WG13

SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.244 J 0.442 0.0884 mg/L 1 XFC8323 XXX20290

5a Androstane <surr> 101 50-150 % 1 XFC8323 XXX20290

Batch Information

Initial Prep Wt./Vol.: 905 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8323

Analytical Method: SW8015C

Analysis Date/Time: 10/31/08 12:33

Prep Batch: XXX20290

Prep Method: SW3520C

Prep Date/Time: 10/29/08 18:00 Container ID:1085813004-H

Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW03-WG13

SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

Toluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Styrene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Acetone ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10242 VXX18954

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

Chloroform ND 1.00 0.300 ug/L 1 VMS10242 VXX18954

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromomethane ND 3.00 0.940 ug/L 1 VMS10242 VXX18954

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW03-WG13

SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10242 VXX18954

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Naphthalene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

o-Xylene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromoform ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane-D4 <surr> 104 73-120 % 1 VMS10242 VXX18954

Toluene-d8 <surr> 103 80-120 % 1 VMS10242 VXX18954

4-Bromofluorobenzene <surr> 113 76-120 % 1 VMS10242 VXX18954

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10242

Analytical Method: SW8260B

Analysis Date/Time: 10/27/08 17:50

Prep Batch: VXX18954

Prep Method: SW5030B

Prep Date/Time: 10/27/08 11:41 Container ID:1085813004-D

Dilution Factor: 1 Analyst: JDB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW03-WG13

SGS Ref. #: 1085813004 Collection Date/Time: 10/22/08 11:15

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Acenaphthene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Fluorene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Phenanthrene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Anthracene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Pyrene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Benzo(a)Anthracene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Chrysene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Benzo[b]Fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Benzo[k]fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Benzo[a]pyrene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Indeno[1,2,3-c,d] pyrene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Dibenzo[a,h]anthracene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Benzo[g,h,i]perylene ND 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Naphthalene 0.219 0.103 0.0320 ug/L 1 XMS4761 XXX20276

1-Methylnaphthalene 0.0658 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

2-Methylnaphthalene 0.0937 0.0515 0.0155 ug/L 1 XMS4761 XXX20276

Terphenyl-d14 <surr> 89.4 50-135 % 1 XMS4761 XXX20276

Batch Information

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4761

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/30/08 16:29

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813004-J

Dilution Factor: 1 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5719 MXX21031

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5719

Analytical Method: SW6020

Analysis Date/Time: 11/14/08 22:12

Prep Batch: MXX21031

Prep Method: SW3010A

Prep Date/Time: 11/04/08 18:15 Container ID:1085813005-G

Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 52.8 J 100 10.0 ug/L 1 VFC9248 VXX18967

4-Bromofluorobenzene <surr> 129 50-150 % 1 VFC9248 VXX18967

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9248

Analytical Method: SW8015C

Analysis Date/Time: 10/30/08 11:36

Prep Batch: VXX18967

Prep Method: SW5030B

Prep Date/Time: 10/30/08 08:00 Container ID:1085813005-A

Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 4.54 0.400 0.0800 mg/L 1 XFC8323 XXX20290

5a Androstane <surr> 97.8 50-150 % 1 XFC8323 XXX20290

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8323

Analytical Method: SW8015C

Analysis Date/Time: 10/31/08 12:42

Prep Batch: XXX20290

Prep Method: SW3520C

Prep Date/Time: 10/29/08 18:00 Container ID:1085813005-H

Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.140 J 0.400 0.120 ug/L 1 VMS10242 VXX18954

Toluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Ethylbenzene 0.450 J 1.00 0.310 ug/L 1 VMS10242 VXX18954

n-Butylbenzene 9.65 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

n-Propylbenzene 12.4 1.00 0.310 ug/L 1 VMS10242 VXX18954

Styrene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Acetone ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10242 VXX18954

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

Chloroform ND 1.00 0.300 ug/L 1 VMS10242 VXX18954

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromomethane ND 3.00 0.940 ug/L 1 VMS10242 VXX18954

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

sec-Butylbenzene 8.48 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10242 VXX18954

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Naphthalene 239 40.0 12.4 ug/L 20 VMS10254 VXX18976

o-Xylene 0.450 J 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromoform ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

tert-Butylbenzene 1.29 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Isopropylbenzene (Cumene) 6.64 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane-D4 <surr> 104 73-120 % 1 VMS10242 VXX18954

Toluene-d8 <surr> 104 80-120 % 1 VMS10242 VXX18954

4-Bromofluorobenzene <surr> 104 76-120 % 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10242

Analytical Method: SW8260B

Analysis Date/Time: 10/27/08 18:24

Prep Batch: VXX18954

Prep Method: SW5030B

Prep Date/Time: 10/27/08 11:41 Container ID:1085813005-E

Dilution Factor: 1 Analyst: JDB

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10254

Analytical Method: SW8260B

Analysis Date/Time: 10/31/08 08:38

Prep Batch: VXX18976

Prep Method: SW5030B

Prep Date/Time: 10/31/08 01:28 Container ID:1085813005-C

Dilution Factor: 20 Analyst: DSH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW02-WG13

SGS Ref. #: 1085813005 Collection Date/Time: 10/22/08 12:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Acenaphthene 0.365 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Fluorene 0.214 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Phenanthrene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Anthracene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Pyrene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Benzo(a)Anthracene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Chrysene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Benzo[b]Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Benzo[k]fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Benzo[a]pyrene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Indeno[1,2,3-c,d] pyrene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Dibenzo[a,h]anthracene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Benzo[g,h,i]perylene ND 0.0521 0.0156 ug/L 1 XMS4761 XXX20276

Naphthalene 97.4 5.21 1.61 ug/L 50 XMS4763 XXX20276

1-Methylnaphthalene 72.1 2.60 0.781 ug/L 50 XMS4763 XXX20276

2-Methylnaphthalene 13.7 1.04 0.313 ug/L 20 XMS4763 XXX20276

Terphenyl-d14 <surr> 89.6 50-135 % 1 XMS4761 XXX20276

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4761

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/30/08 17:02

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813005-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4763

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/31/08 11:49

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813005-J

Dilution Factor: 20 Analyst: JDH

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4763

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/31/08 15:57

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813005-J

Dilution Factor: 50 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5719 MXX21031

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5719

Analytical Method: SW6020

Analysis Date/Time: 11/14/08 22:19

Prep Batch: MXX21031

Prep Method: SW3010A

Prep Date/Time: 11/04/08 18:15 Container ID:1085813006-G

Dilution Factor: 5 Analyst: NRB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 52.9 J 100 10.0 ug/L 1 VFC9248 VXX18967

4-Bromofluorobenzene <surr> 130 50-150 % 1 VFC9248 VXX18967

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9248

Analytical Method: SW8015C

Analysis Date/Time: 10/30/08 11:54

Prep Batch: VXX18967

Prep Method: SW5030B

Prep Date/Time: 10/30/08 08:00 Container ID:1085813006-A

Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 6.30 0.491 0.0982 mg/L 1 XFC8323 XXX20290

5a Androstane <surr> 104 50-150 % 1 XFC8323 XXX20290

Batch Information

Initial Prep Wt./Vol.: 815 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8323

Analytical Method: SW8015C

Analysis Date/Time: 10/31/08 12:52

Prep Batch: XXX20290

Prep Method: SW3520C

Prep Date/Time: 10/29/08 18:00 Container ID:1085813006-H

Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.150 J 0.400 0.120 ug/L 1 VMS10242 VXX18954

Toluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Ethylbenzene 0.420 J 1.00 0.310 ug/L 1 VMS10242 VXX18954

n-Butylbenzene 9.47 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

n-Propylbenzene 12.5 1.00 0.310 ug/L 1 VMS10242 VXX18954

Styrene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Acetone ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10242 VXX18954

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

Chloroform ND 1.00 0.300 ug/L 1 VMS10242 VXX18954

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromomethane ND 3.00 0.940 ug/L 1 VMS10242 VXX18954

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

sec-Butylbenzene 8.57 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10242 VXX18954

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Naphthalene 245 40.0 12.4 ug/L 20 VMS10254 VXX18976

o-Xylene 0.490 J 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromoform ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

tert-Butylbenzene 1.31 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Isopropylbenzene (Cumene) 6.48 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS10242 VXX18954

Toluene-d8 <surr> 103 80-120 % 1 VMS10242 VXX18954

4-Bromofluorobenzene <surr> 105 76-120 % 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10242

Analytical Method: SW8260B

Analysis Date/Time: 10/27/08 18:58

Prep Batch: VXX18954

Prep Method: SW5030B

Prep Date/Time: 10/27/08 11:41 Container ID:1085813006-D

Dilution Factor: 1 Analyst: JDB

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10254

Analytical Method: SW8260B

Analysis Date/Time: 10/31/08 09:09

Prep Batch: VXX18976

Prep Method: SW5030B

Prep Date/Time: 10/31/08 01:28 Container ID:1085813006-C

Dilution Factor: 20 Analyst: DSH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMWA01-WG13

SGS Ref. #: 1085813006 Collection Date/Time: 10/22/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Acenaphthene 0.208 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Fluorene 0.122 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Phenanthrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Chrysene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Naphthalene 82.3 5.00 1.55 ug/L 50 XMS4763 XXX20276

1-Methylnaphthalene 62.4 2.50 0.750 ug/L 50 XMS4763 XXX20276

2-Methylnaphthalene 12.7 1.00 0.300 ug/L 20 XMS4763 XXX20276

Terphenyl-d14 <surr> 87.7 50-135 % 1 XMS4761 XXX20276

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4761

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/30/08 17:36

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813006-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4763

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/31/08 12:22

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813006-J

Dilution Factor: 20 Analyst: JDH

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4763

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/31/08 16:31

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813006-J

Dilution Factor: 50 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 10.0 ug/L 1 VFC9248 VXX18967

4-Bromofluorobenzene <surr> 92.5 50-150 % 1 VFC9248 VXX18967

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9248

Analytical Method: SW8015C

Analysis Date/Time: 10/30/08 12:12

Prep Batch: VXX18967

Prep Method: SW5030B

Prep Date/Time: 10/30/08 08:00 Container ID:1085813007-A

Dilution Factor: 1 Analyst: HM

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.459 0.412 0.0825 mg/L 1 XFC8323 XXX20290

5a Androstane <surr> 103 50-150 % 1 XFC8323 XXX20290

Batch Information

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8323

Analytical Method: SW8015C

Analysis Date/Time: 10/31/08 13:01

Prep Batch: XXX20290

Prep Method: SW3520C

Prep Date/Time: 10/29/08 18:00 Container ID:1085813007-H

Dilution Factor: 1 Analyst: GL

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

Toluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Styrene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Acetone ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10242 VXX18954

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

Chloroform ND 1.00 0.300 ug/L 1 VMS10242 VXX18954

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromomethane ND 3.00 0.940 ug/L 1 VMS10242 VXX18954

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10242 VXX18954

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Naphthalene ND 2.00 0.620 ug/L 1 VMS10254 VXX18976

o-Xylene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromoform ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS10242 VXX18954

Toluene-d8 <surr> 104 80-120 % 1 VMS10242 VXX18954

4-Bromofluorobenzene <surr> 109 76-120 % 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10242

Analytical Method: SW8260B

Analysis Date/Time: 10/27/08 19:31

Prep Batch: VXX18954

Prep Method: SW5030B

Prep Date/Time: 10/27/08 11:41 Container ID:1085813007-D

Dilution Factor: 1 Analyst: JDB

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10254

Analytical Method: SW8260B

Analysis Date/Time: 10/31/08 07:36

Prep Batch: VXX18976

Prep Method: SW5030B

Prep Date/Time: 10/31/08 01:28 Container ID:1085813007-F

Dilution Factor: 1 Analyst: DSH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1085813007 Collection Date/Time: 10/22/08 15:00

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Acenaphthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Fluorene 0.0207 J 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Phenanthrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Chrysene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Naphthalene 0.103 0.100 0.0310 ug/L 1 XMS4761 XXX20276

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4761 XXX20276

Terphenyl-d14 <surr> 91.1 50-135 % 1 XMS4761 XXX20276

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4761

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/30/08 18:09

Prep Batch: XXX20276

Prep Method: SW3520C

Prep Date/Time: 10/28/08 10:10 Container ID:1085813007-J

Dilution Factor: 1 Analyst: JDH

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: TB01-WG13

SGS Ref. #: 1085813008 Collection Date/Time: 10/22/08 08:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

Toluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Styrene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Acetone ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10242 VXX18954

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10242 VXX18954

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

Chloroform ND 1.00 0.300 ug/L 1 VMS10242 VXX18954

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Chloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromomethane ND 3.00 0.940 ug/L 1 VMS10242 VXX18954

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
The Environmental Company, Inc. (TEC) Print Date: 11/20/2008

Client Sample ID: TB01-WG13

SGS Ref. #: 1085813008 Collection Date/Time: 10/22/08 08:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 10/24/08 10:50

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10242 VXX18954

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10242 VXX18954

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

Naphthalene ND 2.00 0.620 ug/L 1 VMS10242 VXX18954

o-Xylene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Bromoform ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10242 VXX18954

1,2-Dichloroethane-D4 <surr> 105 73-120 % 1 VMS10242 VXX18954

Toluene-d8 <surr> 106 80-120 % 1 VMS10242 VXX18954

4-Bromofluorobenzene <surr> 112 76-120 % 1 VMS10242 VXX18954

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10242

Analytical Method: SW8260B

Analysis Date/Time: 10/27/08 16:09

Prep Batch: VXX18954

Prep Method: SW5030B

Prep Date/Time: 10/27/08 11:41 Container ID:1085813008-A

Dilution Factor: 1 Analyst: JDB

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867629 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18954

SW5030B

10/27/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006, 1085813007, 1085813008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 10/27/08

Toluene ND 1.00 0.310 ug/L 10/27/08

Ethylbenzene ND 1.00 0.310 ug/L 10/27/08

n-Butylbenzene ND 1.00 0.310 ug/L 10/27/08

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 10/27/08

1,2-Dichloroethane ND 0.500 0.150 ug/L 10/27/08

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 10/27/08

4-Chlorotoluene ND 1.00 0.310 ug/L 10/27/08

Chlorobenzene ND 0.500 0.150 ug/L 10/27/08

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 10/27/08

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 10/27/08

4-Isopropyltoluene ND 1.00 0.310 ug/L 10/27/08

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 10/27/08

n-Propylbenzene ND 1.00 0.310 ug/L 10/27/08

Styrene ND 1.00 0.310 ug/L 10/27/08

Dibromomethane ND 1.00 0.310 ug/L 10/27/08

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 10/27/08

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 10/27/08

Acetone ND 10.0 3.10 ug/L 10/27/08

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 10/27/08

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 10/27/08

Methyl-t-butyl ether ND 5.00 1.50 ug/L 10/27/08

Tetrachloroethene ND 1.00 0.310 ug/L 10/27/08

Dibromochloromethane ND 0.500 0.150 ug/L 10/27/08

1,3-Dichloropropane ND 0.400 0.120 ug/L 10/27/08

1,2-Dibromoethane ND 1.00 0.310 ug/L 10/27/08

Carbon tetrachloride ND 1.00 0.310 ug/L 10/27/08

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 10/27/08

Chloroform ND 1.00 0.300 ug/L 10/27/08

Bromobenzene ND 1.00 0.310 ug/L 10/27/08

Chloromethane ND 1.00 0.310 ug/L 10/27/08

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 10/27/08

Bromomethane ND 3.00 0.940 ug/L 10/27/08

Bromochloromethane ND 1.00 0.310 ug/L 10/27/08

Vinyl chloride ND 1.00 0.310 ug/L 10/27/08

Dichlorodifluoromethane ND 1.00 0.310 ug/L 10/27/08
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867629 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18954

SW5030B

10/27/2008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Chloroethane ND 1.00 0.310 ug/L 10/27/08

sec-Butylbenzene ND 1.00 0.310 ug/L 10/27/08

Bromodichloromethane ND 0.500 0.150 ug/L 10/27/08

1,1-Dichloroethene ND 1.00 0.310 ug/L 10/27/08

2-Butanone (MEK) ND 10.0 3.10 ug/L 10/27/08

Methylene chloride ND 5.00 1.00 ug/L 10/27/08

Trichlorofluoromethane ND 1.00 0.310 ug/L 10/27/08

P & M -Xylene ND 2.00 0.620 ug/L 10/27/08

Naphthalene ND 2.00 0.620 ug/L 10/27/08

o-Xylene ND 1.00 0.310 ug/L 10/27/08

Bromoform ND 1.00 0.310 ug/L 10/27/08

1-Chlorohexane ND 1.00 0.310 ug/L 10/27/08

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 10/27/08

tert-Butylbenzene ND 1.00 0.310 ug/L 10/27/08

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 10/27/08

1,1-Dichloroethane ND 1.00 0.310 ug/L 10/27/08

2-Chlorotoluene ND 1.00 0.310 ug/L 10/27/08

Trichloroethene ND 1.00 0.310 ug/L 10/27/08

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 10/27/08

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 10/27/08

2,2-Dichloropropane ND 1.00 0.310 ug/L 10/27/08

Hexachlorobutadiene ND 1.00 0.310 ug/L 10/27/08

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 10/27/08

1,2-Dichloropropane ND 1.00 0.310 ug/L 10/27/08

1,1-Dichloropropene ND 1.00 0.310 ug/L 10/27/08

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 10/27/08

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 10/27/08

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 10/27/08

Surrogates 

1,2-Dichloroethane-D4 <surr> 102 73-120 % 10/27/08

Toluene-d8 <surr> 105 80-120 % 10/27/08

4-Bromofluorobenzene <surr> 109 76-120 % 10/27/08

Instrument

Method

Batch VMS10242

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867655 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20276

SW3520C

10/28/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 10/30/08

Acenaphthene ND 0.0500 0.0150 ug/L 10/30/08

Fluorene ND 0.0500 0.0150 ug/L 10/30/08

Phenanthrene ND 0.0500 0.0150 ug/L 10/30/08

Anthracene ND 0.0500 0.0150 ug/L 10/30/08

Fluoranthene ND 0.0500 0.0150 ug/L 10/30/08

Pyrene ND 0.0500 0.0150 ug/L 10/30/08

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 10/30/08

Chrysene ND 0.0500 0.0150 ug/L 10/30/08

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 10/30/08

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 10/30/08

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 10/30/08

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 10/30/08

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 10/30/08

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 10/30/08

Naphthalene ND 0.100 0.0310 ug/L 10/30/08

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 10/30/08

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 10/30/08

Surrogates 

Terphenyl-d14 <surr> 88.5 50-135 % 10/30/08

Instrument

Method

Batch XMS4761

8270D SIMS

HP 5890 Series II MS2 SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

868151 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20290

SW3520C

10/29/2008

QC results affect the following production samples:

1085813004, 1085813005, 1085813006, 1085813007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics ND 0.400 0.0800 mg/L 10/31/08

Surrogates 

5a Androstane <surr> 104 60-120 % 10/31/08

Instrument

Method

Batch XFC8323

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

868324 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18967

SW5030B

10/30/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics ND 100 10.0 ug/L 10/30/08

Surrogates 

4-Bromofluorobenzene <surr> 94.9 50-150 % 10/30/08

Instrument

Method

Batch VFC9248

SW8015C

HP 5890 Series II PID+FID VCA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

868746 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18976

SW5030B

10/31/2008

QC results affect the following production samples:

1085813005, 1085813006, 1085813007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Naphthalene ND 2.00 0.620 ug/L 10/31/08

Surrogates 

1,2-Dichloroethane-D4 <surr> 102 73-120 % 10/31/08

Toluene-d8 <surr> 100 80-120 % 10/31/08

4-Bromofluorobenzene <surr> 101 76-120 % 10/31/08

Instrument

Method

Batch VMS10254

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

869197 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20313

SW3520C

11/03/2008

QC results affect the following production samples:

1085813001

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics ND 0.400 0.0800 mg/L 11/05/08

Surrogates 

5a Androstane <surr> 97.3 60-120 % 11/05/08

Instrument

Method

Batch XFC8338

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

869581 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX21031

SW3010A

11/04/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 11/14/08

Instrument

Method

Batch MMS5719

SW6020

Perkin Elmer Sciex ICP-MS P4
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867630 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18954

SW5030B

10/27/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006, 1085813007, 1085813008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 27.9 93 ( 80-120 ) 30 ug/L 10/27/2008

Toluene LCS 29.5 98 ( 77-120 ) 30 ug/L 10/27/2008

Ethylbenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 10/27/2008

n-Butylbenzene LCS 30.2 101 ( 80-124 ) 30 ug/L 10/27/2008

1,4-Dichlorobenzene LCS 29.5 98 ( 80-120 ) 30 ug/L 10/27/2008

1,2-Dichloroethane LCS 28.4 95 ( 80-129 ) 30 ug/L 10/27/2008

1,3,5-Trimethylbenzene LCS 32.7 109 ( 80-128 ) 30 ug/L 10/27/2008

4-Chlorotoluene LCS 31.3 104 ( 79-128 ) 30 ug/L 10/27/2008

Chlorobenzene LCS 30.1 100 ( 80-120 ) 30 ug/L 10/27/2008

4-Methyl-2-pentanone (MIBK) LCS 83.7 93 ( 69-134 ) 90 ug/L 10/27/2008

cis-1,2-Dichloroethene LCS 29.3 98 ( 80-125 ) 30 ug/L 10/27/2008

4-Isopropyltoluene LCS 31.8 106 ( 80-125 ) 30 ug/L 10/27/2008

cis-1,3-Dichloropropene LCS 30.2 101 ( 80-120 ) 30 ug/L 10/27/2008

n-Propylbenzene LCS 31.6 105 ( 80-129 ) 30 ug/L 10/27/2008

Styrene LCS 31.7 106 ( 80-120 ) 30 ug/L 10/27/2008

Dibromomethane LCS 29.4 98 ( 80-120 ) 30 ug/L 10/27/2008

trans-1,3-Dichloropropene LCS 32.1 107 ( 80-124 ) 30 ug/L 10/27/2008

1,2,4-Trichlorobenzene LCS 29.0 97 ( 80-120 ) 30 ug/L 10/27/2008

Acetone LCS 81.6 91 ( 50-135 ) 90 ug/L 10/27/2008

1,1,2,2-Tetrachloroethane LCS 30.3 101 ( 76-123 ) 30 ug/L 10/27/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867630 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18954

SW5030B

10/27/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane LCS 34.1 114 ( 73-130 ) 30 ug/L 10/27/2008

Methyl-t-butyl ether LCS 45.0 100 ( 80-120 ) 45 ug/L 10/27/2008

Tetrachloroethene LCS 29.6 99 ( 79-122 ) 30 ug/L 10/27/2008

Dibromochloromethane LCS 31.8 106 ( 80-120 ) 30 ug/L 10/27/2008

1,3-Dichloropropane LCS 30.7 102 ( 80-121 ) 30 ug/L 10/27/2008

1,2-Dibromoethane LCS 31.3 104 ( 80-120 ) 30 ug/L 10/27/2008

Carbon tetrachloride LCS 30.7 102 ( 80-126 ) 30 ug/L 10/27/2008

1,1,1,2-Tetrachloroethane LCS 31.9 106 ( 80-120 ) 30 ug/L 10/27/2008

Chloroform LCS 29.8 99 ( 80-124 ) 30 ug/L 10/27/2008

Bromobenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 10/27/2008

Chloromethane LCS 28.6 95 ( 67-125 ) 30 ug/L 10/27/2008

1,2,3-Trichloropropane LCS 30.2 101 ( 80-120 ) 30 ug/L 10/27/2008

Bromomethane LCS 31.6 105 ( 30-140 ) 30 ug/L 10/27/2008

Bromochloromethane LCS 30.5 102 ( 77-129 ) 30 ug/L 10/27/2008

Vinyl chloride LCS 28.8 96 ( 72-145 ) 30 ug/L 10/27/2008

Dichlorodifluoromethane LCS 27.5 92 ( 62-153 ) 30 ug/L 10/27/2008

Chloroethane LCS 28.4 95 ( 67-133 ) 30 ug/L 10/27/2008

sec-Butylbenzene LCS 32.3 108 ( 80-120 ) 30 ug/L 10/27/2008

Bromodichloromethane LCS 31.8 106 ( 80-120 ) 30 ug/L 10/27/2008

1,1-Dichloroethene LCS 29.5 98 ( 76-130 ) 30 ug/L 10/27/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867630 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18954

SW5030B

10/27/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) LCS 84.4 94 ( 66-136 ) 90 ug/L 10/27/2008

Methylene chloride LCS 30.2 101 ( 63-131 ) 30 ug/L 10/27/2008

Trichlorofluoromethane LCS 30.0 100 ( 68-145 ) 30 ug/L 10/27/2008

P & M -Xylene LCS 62.4 104 ( 80-120 ) 60 ug/L 10/27/2008

Naphthalene LCS 28.5 95 ( 75-120 ) 30 ug/L 10/27/2008

o-Xylene LCS 31.5 105 ( 80-120 ) 30 ug/L 10/27/2008

Bromoform LCS 31.8 106 ( 80-120 ) 30 ug/L 10/27/2008

1-Chlorohexane LCS 44.5 99 ( 70-125 ) 45 ug/L 10/27/2008

1,2,4-Trimethylbenzene LCS 31.8 106 ( 80-125 ) 30 ug/L 10/27/2008

tert-Butylbenzene LCS 32.4 108 ( 80-122 ) 30 ug/L 10/27/2008

1,1,1-Trichloroethane LCS 32.0 107 ( 80-122 ) 30 ug/L 10/27/2008

1,1-Dichloroethane LCS 30.6 102 ( 80-120 ) 30 ug/L 10/27/2008

2-Chlorotoluene LCS 31.0 103 ( 80-125 ) 30 ug/L 10/27/2008

Trichloroethene LCS 28.4 95 ( 80-125 ) 30 ug/L 10/27/2008

trans-1,2-Dichloroethene LCS 30.2 101 ( 79-132 ) 30 ug/L 10/27/2008

1,2-Dichlorobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 10/27/2008

2,2-Dichloropropane LCS 31.2 104 ( 80-132 ) 30 ug/L 10/27/2008

Hexachlorobutadiene LCS 26.4 88 ( 77-125 ) 30 ug/L 10/27/2008

Isopropylbenzene (Cumene) LCS 31.7 106 ( 80-121 ) 30 ug/L 10/27/2008

1,2-Dichloropropane LCS 29.1 97 ( 80-121 ) 30 ug/L 10/27/2008

1,1-Dichloropropene LCS 29.3 98 ( 80-122 ) 30 ug/L 10/27/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867630 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18954

SW5030B

10/27/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,2-Trichloroethane LCS 30.1 100 ( 77-120 ) 30 ug/L 10/27/2008

1,3-Dichlorobenzene LCS 29.1 97 ( 80-120 ) 30 ug/L 10/27/2008

1,2,3-Trichlorobenzene LCS 26.3 88 ( 77-120 ) 30 ug/L 10/27/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 10/27/2008

Toluene-d8 <surr> LCS 104 ( 80-120 ) 10/27/2008

4-Bromofluorobenzene <surr> LCS 103 ( 76-120 ) 10/27/2008

Batch

Method

Instrument

VMS10242

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867656 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20276

SW3520C

10/28/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867656 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20276

SW3520C

10/28/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.333 67 ( 50-105 ) 0.5 ug/L 10/30/2008

Acenaphthene LCS 0.314 63 ( 45-110 ) 0.5 ug/L 10/30/2008

Fluorene LCS 0.342 68 ( 50-110 ) 0.5 ug/L 10/30/2008

Phenanthrene LCS 0.369 74 ( 50-115 ) 0.5 ug/L 10/30/2008

Anthracene LCS 0.382 76 ( 55-110 ) 0.5 ug/L 10/30/2008

Fluoranthene LCS 0.342 68 ( 55-125 ) 0.5 ug/L 10/30/2008

Pyrene LCS 0.323 65 ( 50-130 ) 0.5 ug/L 10/30/2008

Benzo(a)Anthracene LCS 0.376 75 ( 55-120 ) 0.5 ug/L 10/30/2008

Chrysene LCS 0.339 68 ( 55-120 ) 0.5 ug/L 10/30/2008

Benzo[b]Fluoranthene LCS 0.376 75 ( 46-130 ) 0.5 ug/L 10/30/2008

Benzo[k]fluoranthene LCS 0.378 76 ( 60-125 ) 0.5 ug/L 10/30/2008

Benzo[a]pyrene LCS 0.416 83 ( 55-120 ) 0.5 ug/L 10/30/2008

Indeno[1,2,3-c,d] pyrene LCS 0.379 76 ( 45-125 ) 0.5 ug/L 10/30/2008

Dibenzo[a,h]anthracene LCS 0.389 78 ( 41-140 ) 0.5 ug/L 10/30/2008

Benzo[g,h,i]perylene LCS 0.376 75 ( 46-125 ) 0.5 ug/L 10/30/2008

Naphthalene LCS 0.266 53 ( 42-100 ) 0.5 ug/L 10/30/2008

1-Methylnaphthalene LCS 0.277 55 ( 46-115 ) 0.5 ug/L 10/30/2008

2-Methylnaphthalene LCS 0.290 58 ( 45-105 ) 0.5 ug/L 10/30/2008

Surrogates 

Terphenyl-d14 <surr> LCS 93 ( 50-135 ) 10/30/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

867656 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20276

SW3520C

10/28/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4761

8270D SIMS

HP 5890 Series II MS2 SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

868152 Lab Control Sample

868153 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20290

SW3520C

10/29/2008

QC results affect the following production samples:

1085813004, 1085813005, 1085813006, 1085813007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.42 89 ( 75-125 ) 5 mg/L 10/31/2008

LCSD 5.32 106 18 (< 20 ) 5 mg/L 10/31/2008

Surrogates 

5a Androstane <surr> LCS 100 ( 60-120 ) 10/31/2008

LCSD 110 10 10/31/2008

Batch

Method

Instrument

XFC8323

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

868325 Lab Control Sample

868326 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18967

SW5030B

10/30/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006, 1085813007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 192 96 ( 79-108 ) 200 ug/L 10/30/2008

LCSD 189 95 2 (< 20 ) 200 ug/L 10/30/2008

Surrogates 

4-Bromofluorobenzene <surr> LCS 96 ( 50-150 ) 10/30/2008

LCSD 95 0 10/30/2008

Batch

Method

Instrument

VFC9248

SW8015C

HP 5890 Series II PID+FID VCA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

868747 Lab Control Sample

868748 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18976

SW5030B

10/31/2008

QC results affect the following production samples:

1085813005, 1085813006, 1085813007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Naphthalene LCS 29.2 97 ( 75-120 ) 30 ug/L 10/31/2008

LCSD 28.9 96 1 (< 20 ) 30 ug/L 10/31/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 102 ( 73-120 ) 10/31/2008

LCSD 99 3 10/31/2008

Toluene-d8 <surr> LCS 99 ( 80-120 ) 10/31/2008

LCSD 99 0 10/31/2008

4-Bromofluorobenzene <surr> LCS 99 ( 76-120 ) 10/31/2008

LCSD 97 2 10/31/2008

Batch

Method

Instrument

VMS10254

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

869198 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX20313

SW3520C

11/03/2008

QC results affect the following production samples:

1085813001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 2.81 56 ( 75-125 ) * 5 mg/L 11/05/2008

Surrogates 

5a Androstane <surr> LCS 84 ( 60-120 ) 11/05/2008

Batch

Method

Instrument

XFC8338

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Prep

869582 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX21031

SW3010A

11/04/2008

QC results affect the following production samples:

1085813001, 1085813004, 1085813005, 1085813006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1070 107 ( 80-120 ) 1000 ug/L 11/14/2008

Batch

Method

Instrument

MMS5719

SW6020

Perkin Elmer Sciex ICP-MS P4
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

868545 Matrix Spike

868546 Matrix Spike Duplicate

871926

Water (Surface, Eff., Ground)

XXX20290

Cnt. Liq/Liq Ext. for AK102/3

10/29/2008

QC results affect the following production samples:

1085813004, 1085813005, 1085813006, 1085813007

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Semivolatile Organic Fuels Department

Diesel Range Organics MS ND ND 0* ( 75-125 ) 5.26 mg/L 10/31/2008

MSD 0.00 0* 0 (< 30 ) 5.26 mg/L 10/31/2008

Surrogates 

5a Androstane <surr> MS .107 102 ( 50-150 ) 10/31/2008

MSD 0.102 97 5 10/31/2008

Batch

Method

Instrument

XFC8323

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

MXX21031

3010 H20 Digest for Metals ICP-MS

11/04/2008

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS ND 1020 102 ( 80-120 ) 1000 ug/L 11/14/2008

BMSD 1000 100 1 (< 15 ) 1000 ug/L 11/14/2008

Batch

Method

Instrument

MMS5719

SW6020

Perkin Elmer Sciex ICP-MS P4

Volatile Fuels Department

Gasoline Range Organics BMS ND 448 100 ( 79-108 ) 450 ug/L 10/30/2008

BMSD 401 89 11 (< 20 ) 450 ug/L 10/30/2008

Surrogates 

4-Bromofluorobenzene <surr> BMS 50.9 102 ( 50-150 ) 10/30/2008

BMSD 48.6 97 5 10/30/2008

Batch

Method

Instrument

VFC9248

SW8015C

HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS ND 4.89 94 ( 75-125 ) 5.21 mg/L 11/05/2008

BMSD 4.72 94 4 (< 30 ) 5.00 mg/L 11/05/2008

Surrogates 

5a Androstane <surr> BMS .103 99 ( 50-150 ) 11/05/2008

BMSD 0.102 102 1 11/05/2008

Batch

Method

Instrument

XFC8338

SW8015C

HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

VXX18954

Volatiles Extraction AFCEE 3.1 8260 (

10/27/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS ND 27.9 93 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 28.4 95 2 (< 20 ) 30.0 ug/L 10/27/2008

Toluene BMS ND 29.6 99 ( 77-120 ) 30.0 ug/L 10/27/2008

BMSD 29.6 99 0 (< 20 ) 30.0 ug/L 10/27/2008

Ethylbenzene BMS ND 30.6 102 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 31.3 104 2 (< 20 ) 30.0 ug/L 10/27/2008

n-Butylbenzene BMS ND 34.4 115 ( 80-124 ) 30.0 ug/L 10/27/2008

BMSD 35.5 118 3 (< 20 ) 30.0 ug/L 10/27/2008

1,4-Dichlorobenzene BMS ND 29.3 98 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.9 103 5 (< 20 ) 30.0 ug/L 10/27/2008

1,2-Dichloroethane BMS ND 28.3 94 ( 80-129 ) 30.0 ug/L 10/27/2008

BMSD 29.2 97 3 (< 20 ) 30.0 ug/L 10/27/2008

1,3,5-Trimethylbenzene BMS ND 33 110 ( 80-128 ) 30.0 ug/L 10/27/2008

BMSD 34.0 113 3 (< 20 ) 30.0 ug/L 10/27/2008

4-Chlorotoluene BMS ND 31.8 106 ( 79-128 ) 30.0 ug/L 10/27/2008

BMSD 33.0 110 4 (< 20 ) 30.0 ug/L 10/27/2008

Chlorobenzene BMS ND 30 100 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 29.9 100 0 (< 20 ) 30.0 ug/L 10/27/2008

4-Methyl-2-pentanone (MIBK) BMS ND 82.4 92 ( 69-134 ) 90.0 ug/L 10/27/2008

BMSD 87.9 98 7 (< 20 ) 90.0 ug/L 10/27/2008

cis-1,2-Dichloroethene BMS ND 29.4 98 ( 80-125 ) 30.0 ug/L 10/27/2008

BMSD 29.8 99 1 (< 20 ) 30.0 ug/L 10/27/2008

4-Isopropyltoluene BMS ND 33.7 112 ( 80-125 ) 30.0 ug/L 10/27/2008

BMSD 34.4 115 2 (< 20 ) 30.0 ug/L 10/27/2008

cis-1,3-Dichloropropene BMS ND 29.5 98 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.8 103 5 (< 20 ) 30.0 ug/L 10/27/2008

n-Propylbenzene BMS ND 32.5 108 ( 80-129 ) 30.0 ug/L 10/27/2008

BMSD 33.7 112 4 (< 20 ) 30.0 ug/L 10/27/2008

Styrene BMS ND 32 107 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 32.3 108 1 (< 20 ) 30.0 ug/L 10/27/2008

Dibromomethane BMS ND 28.4 95 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 29.7 99 5 (< 20 ) 30.0 ug/L 10/27/2008

trans-1,3-Dichloropropene BMS ND 30.1 100 ( 80-124 ) 30.0 ug/L 10/27/2008

BMSD 31.5 105 5 (< 20 ) 30.0 ug/L 10/27/2008

1,2,4-Trichlorobenzene BMS ND 30.9 103 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 32.2 107 4 (< 20 ) 30.0 ug/L 10/27/2008

Acetone BMS ND 83.2 93 ( 50-135 ) 90.0 ug/L 10/27/2008

BMSD 86.9 97 4 (< 20 ) 90.0 ug/L 10/27/2008

1,1,2,2-Tetrachloroethane BMS ND 29.3 98 ( 76-123 ) 30.0 ug/L 10/27/2008

BMSD 30.7 102 4 (< 20 ) 30.0 ug/L 10/27/2008
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

VXX18954

Volatiles Extraction AFCEE 3.1 8260 (

10/27/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS ND 32.6 109 ( 73-130 ) 30.0 ug/L 10/27/2008

BMSD 34.4 115 5 (< 20 ) 30.0 ug/L 10/27/2008

Methyl-t-butyl ether BMS ND 45.4 101 ( 80-120 ) 45.0 ug/L 10/27/2008

BMSD 47.2 105 4 (< 20 ) 45.0 ug/L 10/27/2008

Tetrachloroethene BMS ND 30.6 102 ( 79-122 ) 30.0 ug/L 10/27/2008

BMSD 30.5 102 0 (< 20 ) 30.0 ug/L 10/27/2008

Dibromochloromethane BMS ND 29.9 100 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 10/27/2008

1,3-Dichloropropane BMS ND 30.2 101 ( 80-121 ) 30.0 ug/L 10/27/2008

BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/27/2008

1,2-Dibromoethane BMS ND 29.8 99 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.4 101 2 (< 20 ) 30.0 ug/L 10/27/2008

Carbon tetrachloride BMS ND 29.4 98 ( 80-126 ) 30.0 ug/L 10/27/2008

BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 10/27/2008

1,1,1,2-Tetrachloroethane BMS ND 30.2 101 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/27/2008

Chloroform BMS ND 29.2 97 ( 80-124 ) 30.0 ug/L 10/27/2008

BMSD 29.7 99 2 (< 20 ) 30.0 ug/L 10/27/2008

Bromobenzene BMS ND 29.9 100 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 31.2 104 4 (< 20 ) 30.0 ug/L 10/27/2008

Chloromethane BMS ND 28.2 94 ( 67-125 ) 30.0 ug/L 10/27/2008

BMSD 28.9 96 2 (< 20 ) 30.0 ug/L 10/27/2008

1,2,3-Trichloropropane BMS ND 30.4 101 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 10/27/2008

Bromomethane BMS ND 32.8 109 ( 30-140 ) 30.0 ug/L 10/27/2008

BMSD 35.7 119 9 (< 20 ) 30.0 ug/L 10/27/2008

Bromochloromethane BMS ND 28.4 95 ( 77-129 ) 30.0 ug/L 10/27/2008

BMSD 29.0 97 2 (< 20 ) 30.0 ug/L 10/27/2008

Vinyl chloride BMS ND 29.6 99 ( 72-145 ) 30.0 ug/L 10/27/2008

BMSD 30.3 101 2 (< 20 ) 30.0 ug/L 10/27/2008

Dichlorodifluoromethane BMS ND 28.7 96 ( 62-153 ) 30.0 ug/L 10/27/2008

BMSD 29.1 97 2 (< 20 ) 30.0 ug/L 10/27/2008

Chloroethane BMS ND 30 100 ( 67-133 ) 30.0 ug/L 10/27/2008

BMSD 34.5 115 14 (< 20 ) 30.0 ug/L 10/27/2008

sec-Butylbenzene BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 34.7 116 4 (< 20 ) 30.0 ug/L 10/27/2008

Bromodichloromethane BMS ND 30.5 102 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 31.8 106 4 (< 20 ) 30.0 ug/L 10/27/2008

1,1-Dichloroethene BMS ND 31.6 105 ( 76-130 ) 30.0 ug/L 10/27/2008

BMSD 32.5 108 3 (< 20 ) 30.0 ug/L 10/27/2008
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

VXX18954

Volatiles Extraction AFCEE 3.1 8260 (

10/27/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS ND 85.1 95 ( 66-136 ) 90.0 ug/L 10/27/2008

BMSD 87.2 97 2 (< 20 ) 90.0 ug/L 10/27/2008

Methylene chloride BMS ND 31.3 104 ( 63-131 ) 30.0 ug/L 10/27/2008

BMSD 32.9 110 5 (< 20 ) 30.0 ug/L 10/27/2008

Trichlorofluoromethane BMS ND 30.7 102 ( 68-145 ) 30.0 ug/L 10/27/2008

BMSD 31.0 103 1 (< 20 ) 30.0 ug/L 10/27/2008

P & M -Xylene BMS ND 64.7 108 ( 80-120 ) 60.0 ug/L 10/27/2008

BMSD 65.1 109 1 (< 20 ) 60.0 ug/L 10/27/2008

Naphthalene BMS ND 28.8 96 ( 75-120 ) 30.0 ug/L 10/27/2008

BMSD 30.2 101 5 (< 20 ) 30.0 ug/L 10/27/2008

o-Xylene BMS ND 31.8 106 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 31.8 106 0 (< 20 ) 30.0 ug/L 10/27/2008

Bromoform BMS ND 29.9 100 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.9 103 3 (< 20 ) 30.0 ug/L 10/27/2008

1-Chlorohexane BMS ND 50.2 111 ( 70-125 ) 45.0 ug/L 10/27/2008

BMSD 50.2 112 0 (< 20 ) 45.0 ug/L 10/27/2008

1,2,4-Trimethylbenzene BMS ND 32.4 108 ( 80-125 ) 30.0 ug/L 10/27/2008

BMSD 33.6 112 4 (< 20 ) 30.0 ug/L 10/27/2008

tert-Butylbenzene BMS ND 32.1 107 ( 80-122 ) 30.0 ug/L 10/27/2008

BMSD 33.6 112 5 (< 20 ) 30.0 ug/L 10/27/2008

1,1,1-Trichloroethane BMS ND 31.3 104 ( 80-122 ) 30.0 ug/L 10/27/2008

BMSD 32.1 107 3 (< 20 ) 30.0 ug/L 10/27/2008

1,1-Dichloroethane BMS ND 31.6 105 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 32.4 108 3 (< 20 ) 30.0 ug/L 10/27/2008

2-Chlorotoluene BMS ND 30.9 103 ( 80-125 ) 30.0 ug/L 10/27/2008

BMSD 32.2 107 4 (< 20 ) 30.0 ug/L 10/27/2008

Trichloroethene BMS ND 29 97 ( 80-125 ) 30.0 ug/L 10/27/2008

BMSD 29.3 98 1 (< 20 ) 30.0 ug/L 10/27/2008

trans-1,2-Dichloroethene BMS ND 32.6 109 ( 79-132 ) 30.0 ug/L 10/27/2008

BMSD 33.0 110 1 (< 20 ) 30.0 ug/L 10/27/2008

1,2-Dichlorobenzene BMS ND 30.2 101 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 31.4 105 4 (< 20 ) 30.0 ug/L 10/27/2008

2,2-Dichloropropane BMS ND 31.9 106 ( 80-132 ) 30.0 ug/L 10/27/2008

BMSD 32.9 110 3 (< 20 ) 30.0 ug/L 10/27/2008

Hexachlorobutadiene BMS ND 29.6 99 ( 77-125 ) 30.0 ug/L 10/27/2008

BMSD 30.0 100 1 (< 20 ) 30.0 ug/L 10/27/2008

Isopropylbenzene (Cumene) BMS ND 32.4 108 ( 80-121 ) 30.0 ug/L 10/27/2008

BMSD 32.7 109 1 (< 20 ) 30.0 ug/L 10/27/2008

1,2-Dichloropropane BMS ND 28.9 96 ( 80-121 ) 30.0 ug/L 10/27/2008

BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 10/27/2008
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

VXX18954

Volatiles Extraction AFCEE 3.1 8260 (

10/27/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS ND 30.3 101 ( 80-122 ) 30.0 ug/L 10/27/2008

BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 10/27/2008

1,1,2-Trichloroethane BMS ND 29.7 99 ( 77-120 ) 30.0 ug/L 10/27/2008

BMSD 30.1 100 2 (< 20 ) 30.0 ug/L 10/27/2008

1,3-Dichlorobenzene BMS ND 29.5 99 ( 80-120 ) 30.0 ug/L 10/27/2008

BMSD 30.5 102 3 (< 20 ) 30.0 ug/L 10/27/2008

1,2,3-Trichlorobenzene BMS ND 27.7 92 ( 77-120 ) 30.0 ug/L 10/27/2008

BMSD 29.3 98 5 (< 20 ) 30.0 ug/L 10/27/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 30.9 103 ( 73-120 ) 10/27/2008

BMSD 31.0 103 0 10/27/2008

Toluene-d8 <surr> BMS 30.9 103 ( 80-120 ) 10/27/2008

BMSD 30.8 103 0 10/27/2008

4-Bromofluorobenzene <surr> BMS 30.3 101 ( 76-120 ) 10/27/2008

BMSD 31.0 103 2 10/27/2008

Batch

Method

Instrument

VMS10242

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

XXX20276

3520 Liquid/Liquid Ext for 8270 SIM

10/28/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS ND .362 68 ( 50-105 ) 0.532 ug/L 10/30/2008

BMSD 0.350 64 3 (< 30 ) 0.549 ug/L 10/30/2008

Acenaphthene BMS ND .345 65 ( 45-110 ) 0.532 ug/L 10/30/2008

BMSD 0.342 62 1 (< 30 ) 0.549 ug/L 10/30/2008

Fluorene BMS ND .36 68 ( 50-110 ) 0.532 ug/L 10/30/2008

BMSD 0.349 64 3 (< 30 ) 0.549 ug/L 10/30/2008

Phenanthrene BMS ND .348 65 ( 50-115 ) 0.532 ug/L 10/30/2008

BMSD 0.343 63 1 (< 30 ) 0.549 ug/L 10/30/2008

Anthracene BMS ND .372 70 ( 55-110 ) 0.532 ug/L 10/30/2008

BMSD 0.363 66 2 (< 30 ) 0.549 ug/L 10/30/2008

Fluoranthene BMS ND .38 71 ( 55-125 ) 0.532 ug/L 10/30/2008

BMSD 0.378 69 1 (< 30 ) 0.549 ug/L 10/30/2008

Pyrene BMS ND .366 69 ( 50-130 ) 0.532 ug/L 10/30/2008

BMSD 0.364 66 1 (< 30 ) 0.549 ug/L 10/30/2008

Benzo(a)Anthracene BMS ND .398 75 ( 55-120 ) 0.532 ug/L 10/30/2008

BMSD 0.380 69 5 (< 30 ) 0.549 ug/L 10/30/2008

Chrysene BMS ND .386 73 ( 55-120 ) 0.532 ug/L 10/30/2008

BMSD 0.387 70 0 (< 30 ) 0.549 ug/L 10/30/2008

Benzo[b]Fluoranthene BMS ND .406 76 ( 46-130 ) 0.532 ug/L 10/30/2008

BMSD 0.408 74 1 (< 30 ) 0.549 ug/L 10/30/2008

Benzo[k]fluoranthene BMS ND .413 78 ( 60-125 ) 0.532 ug/L 10/30/2008

BMSD 0.392 71 5 (< 30 ) 0.549 ug/L 10/30/2008

Benzo[a]pyrene BMS ND .43 81 ( 55-120 ) 0.532 ug/L 10/30/2008

BMSD 0.418 76 3 (< 30 ) 0.549 ug/L 10/30/2008

Indeno[1,2,3-c,d] pyrene BMS ND .416 78 ( 45-125 ) 0.532 ug/L 10/30/2008

BMSD 0.414 75 1 (< 30 ) 0.549 ug/L 10/30/2008

Dibenzo[a,h]anthracene BMS ND .424 80 ( 41-140 ) 0.532 ug/L 10/30/2008

BMSD 0.425 77 0 (< 30 ) 0.549 ug/L 10/30/2008

Benzo[g,h,i]perylene BMS ND .421 79 ( 46-125 ) 0.532 ug/L 10/30/2008

BMSD 0.416 76 1 (< 30 ) 0.549 ug/L 10/30/2008

Naphthalene BMS 0.0466 J .333 54 ( 42-100 ) 0.532 ug/L 10/30/2008

BMSD 0.325 51 3 (< 30 ) 0.549 ug/L 10/30/2008

1-Methylnaphthalene BMS 0.0276 J .341 59 ( 46-115 ) 0.532 ug/L 10/30/2008

BMSD 0.336 56 2 (< 30 ) 0.549 ug/L 10/30/2008

2-Methylnaphthalene BMS ND .336 63 ( 45-105 ) 0.532 ug/L 10/30/2008

BMSD 0.327 60 3 (< 30 ) 0.549 ug/L 10/30/2008

Surrogates 

Terphenyl-d14 <surr> BMS .457 86 ( 50-135 ) 10/30/2008

BMSD 0.454 83 1 10/30/2008
Matrix

SGS Ref.# Printed Date/Time 11/20/2008 8:09

Batch

Method

Date

Original

Prep

1085813002 Billable Matrix Spike

1085813003 Billable Matrix Spike Dup.

1085813001

Water (Surface, Eff., Ground)

XXX20276

3520 Liquid/Liquid Ext for 8270 SIM

10/28/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4761

8270D SIMS

HP 5890 Series II MS2 SVOA
Hager, Barbara (Anchorage)

From: Adkisson, Richard K. [RKAdkisson@tecinc.com]

Sent: Wednesday, October 29, 2008 8:58 AM

To: Hager, Barbara (Anchorage)

Cc: Hart, Jeff; Whitman, William M.C.; Adkisson, Richard K.

Subject: Analysis of Sample RHMW01-WG13

Importance: High

Attachments: image001.jpg

Page 1 of 1

10/29/2008

Barbara,

Please cancel the analysis of sample RHMW01‐WG13 for total lead.  TEC will collect another sample, filter it in the field,

and sent it for dissolved lead analysis.  Please press on with the other requested analysis for RHMW01‐WG13 and all

other samples.  Thank you.

  

Rick Adkisson

TEC, Inc.

1001 Bishop Street, Suite 1400

Honolulu, HI  96813

Phone: 808‐528‐1445

Fax: 808‐528‐0768

  

  









SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS Environmental Services

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

9121-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1086126
CASE NARRATIVE Print Date: 12/11/2008

Workorder No.: 1086126

Project Name: 9121-003 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

There were no analytical anomalies associated with the data reported herein.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1086126

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street Ste 1400

ASB Tower

Honolulu, HI 96813

Attn: Jeff Hart

T: (808)528-1445 F:(808)528-0768

jshart@tecinc.com

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343.

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 12/11/2008

Notes: All DRO/RRO analysese are integrated per SOP.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of SG S G roup
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 9121-003 Red Hill BFSF

Workorder No.: 1086126

Analytical Methods

Method Description Analytical Method

Dissolved Metals by ICP-MS SW6020

Print Date: 12/11/2008 1:06 pm

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1086126001 RHMW01-WG13

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/11/2008 1:06 pm

Client Sample ID: RHMW01-WG13

SGS Ref. #: 1086126001 Collection Date/Time: 11/03/08 13:35

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 11/05/08 09:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead 0.966 J 1.00 0.310 ug/L 5 MMS5721 MXX21078

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5721

Analytical Method: SW6020

Analysis Date/Time: 11/15/08 17:30

Prep Batch: MXX21078

Prep Method: SW3010A

Prep Date/Time: 11/13/08 20:00 Container ID:1086126001-A

Dilution Factor: 5 Analyst: BME

SGS Environmental Services Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 www.us.sgs.com

Member of SGS Group (Société Générale de Surveillance)
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/11/2008 13:06

Batch

Method

Date

Prep

871318 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX21078

SW3010A

11/13/2008

QC results affect the following production samples:

1086126001

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 11/20/08

Instrument

Method

Batch MMS5732

SW6020

Perkin Elmer Sciex ICP-MS P4
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/11/2008 13:06

Batch

Method

Date

Prep

871319 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX21078

SW3010A

11/13/2008

QC results affect the following production samples:

1086126001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1000 100 ( 80-120 ) 1000 ug/L 11/20/2008

Batch

Method

Instrument

MMS5732

SW6020

Perkin Elmer Sciex ICP-MS P4





SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS Environmental Services

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

9121-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1086721
CASE NARRATIVE Print Date: 12/22/2008

Workorder No.: 1086721

Project Name: 9121-003 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

876591

8260B - MS recovery for several analytes does not meet QC goals (biased high). See LCS for accuracy.

MS 1086597003A(876590MS)

876592

8260B - MSD recovery for several analytes does not meet QC goals (biased high). See LCS for accuracy.

MSD 1086597003A(876590MSD)

876594

8260B - ICV recovery for dichlorodifluoromethane and 1,1-dichloroethene does not meet QC goals (biased high). These 

analytes were not detected above the PQL in the associated samples.

CCV CCV for HBN 210083 [VMS/10317]

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 ww w.us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1086721

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street Ste 1400

ASB Tower

Honolulu, HI 96813

Attn: Jeff Hart

T: (808)528-1445 F:(808)528-0768

jshart@tecinc.com

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343.

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 12/22/2008

Notes: All DRO/RRO analysese are integrated per SOP.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 ww w.us.sgs.com

M em ber of SG S G roup
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 9121-003 Red Hill BFSF

Workorder No.: 1086721

Analytical Methods

Method Description Analytical Method

AFCEE 3.1 8260 (W) SW8260B

Print Date: 12/22/2008 11:45 am

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1086721001 RHMW2254-WG13B

1086721002 RHMWA01-WG13B

1086721003 TB01-WG13B

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 ww w.us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: RHMW2254-WG13B

SGS Ref. #: 1086721001 Collection Date/Time: 12/16/08 10:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 12/17/08 11:55

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10317 VXX19107

Toluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Styrene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Acetone ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10317 VXX19107

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10317 VXX19107

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

Chloroform ND 1.00 0.300 ug/L 1 VMS10317 VXX19107

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Chloromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromomethane ND 3.00 0.940 ug/L 1 VMS10317 VXX19107

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: RHMW2254-WG13B

SGS Ref. #: 1086721001 Collection Date/Time: 12/16/08 10:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 12/17/08 11:55

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10317 VXX19107

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

Naphthalene ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

o-Xylene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromoform ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichloroethane-D4 <surr> 99.2 73-120 % 1 VMS10317 VXX19107

Toluene-d8 <surr> 99.6 80-120 % 1 VMS10317 VXX19107

4-Bromofluorobenzene <surr> 100 76-120 % 1 VMS10317 VXX19107

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10317

Analytical Method: SW8260B

Analysis Date/Time: 12/19/08 02:19

Prep Batch: VXX19107

Prep Method: SW5030B

Prep Date/Time: 12/18/08 14:04 Container ID:1086721001-A

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: RHMWA01-WG13B

SGS Ref. #: 1086721002 Collection Date/Time: 12/16/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 12/17/08 11:55

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10317 VXX19107

Toluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Styrene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Acetone ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10317 VXX19107

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10317 VXX19107

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

Chloroform ND 1.00 0.300 ug/L 1 VMS10317 VXX19107

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Chloromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromomethane ND 3.00 0.940 ug/L 1 VMS10317 VXX19107

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: RHMWA01-WG13B

SGS Ref. #: 1086721002 Collection Date/Time: 12/16/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 12/17/08 11:55

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10317 VXX19107

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

Naphthalene ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

o-Xylene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromoform ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichloroethane-D4 <surr> 95.9 73-120 % 1 VMS10317 VXX19107

Toluene-d8 <surr> 102 80-120 % 1 VMS10317 VXX19107

4-Bromofluorobenzene <surr> 99.6 76-120 % 1 VMS10317 VXX19107

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10317

Analytical Method: SW8260B

Analysis Date/Time: 12/19/08 02:52

Prep Batch: VXX19107

Prep Method: SW5030B

Prep Date/Time: 12/18/08 14:04 Container ID:1086721002-A

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: TB01-WG13B

SGS Ref. #: 1086721003 Collection Date/Time: 12/16/08 08:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 12/17/08 11:55

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10317 VXX19107

Toluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Styrene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Acetone ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10317 VXX19107

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10317 VXX19107

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

Chloroform ND 1.00 0.300 ug/L 1 VMS10317 VXX19107

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Chloromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromomethane ND 3.00 0.940 ug/L 1 VMS10317 VXX19107

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 12/22/2008 11:45 am

Client Sample ID: TB01-WG13B

SGS Ref. #: 1086721003 Collection Date/Time: 12/16/08 08:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 12/17/08 11:55

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10317 VXX19107

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10317 VXX19107

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10317 VXX19107

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

Naphthalene ND 2.00 0.620 ug/L 1 VMS10317 VXX19107

o-Xylene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Bromoform ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10317 VXX19107

1,2-Dichloroethane-D4 <surr> 114 73-120 % 1 VMS10317 VXX19107

Toluene-d8 <surr> 99.2 80-120 % 1 VMS10317 VXX19107

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS10317 VXX19107

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10317

Analytical Method: SW8260B

Analysis Date/Time: 12/18/08 20:43

Prep Batch: VXX19107

Prep Method: SW5030B

Prep Date/Time: 12/18/08 14:04 Container ID:1086721003-A

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876587 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

QC results affect the following production samples:

1086721001, 1086721002, 1086721003

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 12/18/08

Toluene ND 1.00 0.310 ug/L 12/18/08

Ethylbenzene ND 1.00 0.310 ug/L 12/18/08

n-Butylbenzene ND 1.00 0.310 ug/L 12/18/08

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 12/18/08

1,2-Dichloroethane ND 0.500 0.150 ug/L 12/18/08

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 12/18/08

4-Chlorotoluene ND 1.00 0.310 ug/L 12/18/08

Chlorobenzene ND 0.500 0.150 ug/L 12/18/08

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 12/18/08

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 12/18/08

4-Isopropyltoluene ND 1.00 0.310 ug/L 12/18/08

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 12/18/08

n-Propylbenzene ND 1.00 0.310 ug/L 12/18/08

Styrene ND 1.00 0.310 ug/L 12/18/08

Dibromomethane ND 1.00 0.310 ug/L 12/18/08

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 12/18/08

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 12/18/08

Acetone ND 10.0 3.10 ug/L 12/18/08

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 12/18/08

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 12/18/08

Methyl-t-butyl ether ND 5.00 1.50 ug/L 12/18/08

Tetrachloroethene ND 1.00 0.310 ug/L 12/18/08

Dibromochloromethane ND 0.500 0.150 ug/L 12/18/08

1,3-Dichloropropane ND 0.400 0.120 ug/L 12/18/08

1,2-Dibromoethane ND 1.00 0.310 ug/L 12/18/08

Carbon tetrachloride ND 1.00 0.310 ug/L 12/18/08

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 12/18/08

Chloroform ND 1.00 0.300 ug/L 12/18/08

Bromobenzene ND 1.00 0.310 ug/L 12/18/08

Chloromethane ND 1.00 0.310 ug/L 12/18/08

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 12/18/08

Bromomethane ND 3.00 0.940 ug/L 12/18/08

Bromochloromethane ND 1.00 0.310 ug/L 12/18/08

Vinyl chloride ND 1.00 0.310 ug/L 12/18/08

Dichlorodifluoromethane ND 1.00 0.310 ug/L 12/18/08
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876587 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Chloroethane ND 1.00 0.310 ug/L 12/18/08

sec-Butylbenzene ND 1.00 0.310 ug/L 12/18/08

Bromodichloromethane ND 0.500 0.150 ug/L 12/18/08

1,1-Dichloroethene ND 1.00 0.310 ug/L 12/18/08

2-Butanone (MEK) ND 10.0 3.10 ug/L 12/18/08

Methylene chloride ND 5.00 1.00 ug/L 12/18/08

Trichlorofluoromethane ND 1.00 0.310 ug/L 12/18/08

P & M -Xylene ND 2.00 0.620 ug/L 12/18/08

Naphthalene ND 2.00 0.620 ug/L 12/18/08

o-Xylene ND 1.00 0.310 ug/L 12/18/08

Bromoform ND 1.00 0.310 ug/L 12/18/08

1-Chlorohexane ND 1.00 0.310 ug/L 12/18/08

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 12/18/08

tert-Butylbenzene ND 1.00 0.310 ug/L 12/18/08

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 12/18/08

1,1-Dichloroethane ND 1.00 0.310 ug/L 12/18/08

2-Chlorotoluene ND 1.00 0.310 ug/L 12/18/08

Trichloroethene ND 1.00 0.310 ug/L 12/18/08

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 12/18/08

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 12/18/08

2,2-Dichloropropane ND 1.00 0.310 ug/L 12/18/08

Hexachlorobutadiene ND 1.00 0.310 ug/L 12/18/08

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 12/18/08

1,2-Dichloropropane ND 1.00 0.310 ug/L 12/18/08

1,1-Dichloropropene ND 1.00 0.310 ug/L 12/18/08

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 12/18/08

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 12/18/08

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 12/18/08

Surrogates 

1,2-Dichloroethane-D4 <surr> 114 73-120 % 12/18/08

Toluene-d8 <surr> 99.4 80-120 % 12/18/08

4-Bromofluorobenzene <surr> 103 76-120 % 12/18/08

Instrument

Method

Batch VMS10317

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876588 Lab Control Sample

876589 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

QC results affect the following production samples:

1086721001, 1086721002, 1086721003

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 32.9 110 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 33.1 110 1 (< 20 ) 30 ug/L 12/18/2008

Toluene LCS 32.5 108 ( 77-120 ) 30 ug/L 12/18/2008

LCSD 32.2 107 1 (< 20 ) 30 ug/L 12/18/2008

Ethylbenzene LCS 32.7 109 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.7 109 0 (< 20 ) 30 ug/L 12/18/2008

n-Butylbenzene LCS 33.4 111 ( 80-124 ) 30 ug/L 12/18/2008

LCSD 33.1 110 1 (< 20 ) 30 ug/L 12/18/2008

1,4-Dichlorobenzene LCS 32.6 109 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.2 107 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dichloroethane LCS 32.6 109 ( 80-129 ) 30 ug/L 12/18/2008

LCSD 32.4 108 1 (< 20 ) 30 ug/L 12/18/2008

1,3,5-Trimethylbenzene LCS 33.3 111 ( 80-128 ) 30 ug/L 12/18/2008

LCSD 32.8 109 2 (< 20 ) 30 ug/L 12/18/2008

4-Chlorotoluene LCS 33.2 111 ( 79-128 ) 30 ug/L 12/18/2008

LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

Chlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 30.5 102 0 (< 20 ) 30 ug/L 12/18/2008

4-Methyl-2-pentanone (MIBK) LCS 93.0 103 ( 69-134 ) 90 ug/L 12/18/2008

LCSD 98.2 109 5 (< 20 ) 90 ug/L 12/18/2008

cis-1,2-Dichloroethene LCS 34.4 115 ( 80-125 ) 30 ug/L 12/18/2008

LCSD 34.1 114 1 (< 20 ) 30 ug/L 12/18/2008

4-Isopropyltoluene LCS 33.3 111 ( 80-125 ) 30 ug/L 12/18/2008

LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

cis-1,3-Dichloropropene LCS 29.5 98 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 30.1 100 2 (< 20 ) 30 ug/L 12/18/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876588 Lab Control Sample

876589 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

n-Propylbenzene LCS 33.1 110 ( 80-129 ) 30 ug/L 12/18/2008

LCSD 32.6 109 2 (< 20 ) 30 ug/L 12/18/2008

Styrene LCS 30.5 102 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 30.8 103 1 (< 20 ) 30 ug/L 12/18/2008

Dibromomethane LCS 31.4 105 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.5 108 3 (< 20 ) 30 ug/L 12/18/2008

trans-1,3-Dichloropropene LCS 32.5 108 ( 80-124 ) 30 ug/L 12/18/2008

LCSD 33.1 110 2 (< 20 ) 30 ug/L 12/18/2008

1,2,4-Trichlorobenzene LCS 30.7 102 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 30.3 101 1 (< 20 ) 30 ug/L 12/18/2008

Acetone LCS 94.2 105 ( 50-135 ) 90 ug/L 12/18/2008

LCSD 101 112 7 (< 20 ) 90 ug/L 12/18/2008

1,1,2,2-Tetrachloroethane LCS 32.1 107 ( 76-123 ) 30 ug/L 12/18/2008

LCSD 33.0 110 3 (< 20 ) 30 ug/L 12/18/2008

1,2-Dibromo-3-chloropropane LCS 34.8 116 ( 73-130 ) 30 ug/L 12/18/2008

LCSD 33.9 113 3 (< 20 ) 30 ug/L 12/18/2008

Methyl-t-butyl ether LCS 49.6 110 ( 80-120 ) 45 ug/L 12/18/2008

LCSD 49.9 111 1 (< 20 ) 45 ug/L 12/18/2008

Tetrachloroethene LCS 31.2 104 ( 79-122 ) 30 ug/L 12/18/2008

LCSD 31.2 104 0 (< 20 ) 30 ug/L 12/18/2008

Dibromochloromethane LCS 33.0 110 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 33.5 112 2 (< 20 ) 30 ug/L 12/18/2008

1,3-Dichloropropane LCS 33.1 110 ( 80-121 ) 30 ug/L 12/18/2008

LCSD 33.4 111 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dibromoethane LCS 32.5 108 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

Carbon tetrachloride LCS 32.9 110 ( 80-126 ) 30 ug/L 12/18/2008

LCSD 32.9 110 0 (< 20 ) 30 ug/L 12/18/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876588 Lab Control Sample

876589 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane LCS 32.4 108 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.6 109 1 (< 20 ) 30 ug/L 12/18/2008

Chloroform LCS 32.2 107 ( 80-124 ) 30 ug/L 12/18/2008

LCSD 33.0 110 3 (< 20 ) 30 ug/L 12/18/2008

Bromobenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 31.4 105 0 (< 20 ) 30 ug/L 12/18/2008

Chloromethane LCS 32.7 109 ( 67-125 ) 30 ug/L 12/18/2008

LCSD 31.8 106 3 (< 20 ) 30 ug/L 12/18/2008

1,2,3-Trichloropropane LCS 31.9 106 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.9 110 3 (< 20 ) 30 ug/L 12/18/2008

Bromomethane LCS 32.2 107 ( 30-140 ) 30 ug/L 12/18/2008

LCSD 31.6 105 2 (< 20 ) 30 ug/L 12/18/2008

Bromochloromethane LCS 32.2 107 ( 77-129 ) 30 ug/L 12/18/2008

LCSD 32.4 108 1 (< 20 ) 30 ug/L 12/18/2008

Vinyl chloride LCS 32.9 110 ( 72-145 ) 30 ug/L 12/18/2008

LCSD 32.0 107 3 (< 20 ) 30 ug/L 12/18/2008

Dichlorodifluoromethane LCS 32.6 109 ( 62-153 ) 30 ug/L 12/18/2008

LCSD 31.8 106 3 (< 20 ) 30 ug/L 12/18/2008

Chloroethane LCS 34.1 114 ( 67-133 ) 30 ug/L 12/18/2008

LCSD 33.5 112 2 (< 20 ) 30 ug/L 12/18/2008

sec-Butylbenzene LCS 33.6 112 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 33.2 111 1 (< 20 ) 30 ug/L 12/18/2008

Bromodichloromethane LCS 31.1 104 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 31.4 105 1 (< 20 ) 30 ug/L 12/18/2008

1,1-Dichloroethene LCS 34.2 114 ( 76-130 ) 30 ug/L 12/18/2008

LCSD 34.4 115 1 (< 20 ) 30 ug/L 12/18/2008

2-Butanone (MEK) LCS 93.1 103 ( 66-136 ) 90 ug/L 12/18/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876588 Lab Control Sample

876589 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 102 114 9 (< 20 ) 90 ug/L 12/18/2008

Methylene chloride LCS 33.1 110 ( 63-131 ) 30 ug/L 12/18/2008

LCSD 31.4 105 5 (< 20 ) 30 ug/L 12/18/2008

Trichlorofluoromethane LCS 35.4 118 ( 68-145 ) 30 ug/L 12/18/2008

LCSD 34.2 114 3 (< 20 ) 30 ug/L 12/18/2008

P & M -Xylene LCS 65.5 109 ( 80-120 ) 60 ug/L 12/18/2008

LCSD 66.5 111 2 (< 20 ) 60 ug/L 12/18/2008

Naphthalene LCS 30.8 103 ( 75-120 ) 30 ug/L 12/18/2008

LCSD 29.8 99 3 (< 20 ) 30 ug/L 12/18/2008

o-Xylene LCS 32.9 110 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.7 109 1 (< 20 ) 30 ug/L 12/18/2008

Bromoform LCS 34.0 113 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 34.4 115 1 (< 20 ) 30 ug/L 12/18/2008

1-Chlorohexane LCS 50.8 113 ( 70-125 ) 45 ug/L 12/18/2008

LCSD 50.4 112 1 (< 20 ) 45 ug/L 12/18/2008

1,2,4-Trimethylbenzene LCS 32.8 109 ( 80-125 ) 30 ug/L 12/18/2008

LCSD 32.4 108 1 (< 20 ) 30 ug/L 12/18/2008

tert-Butylbenzene LCS 34.5 115 ( 80-122 ) 30 ug/L 12/18/2008

LCSD 34.1 114 1 (< 20 ) 30 ug/L 12/18/2008

1,1,1-Trichloroethane LCS 31.0 103 ( 80-122 ) 30 ug/L 12/18/2008

LCSD 31.3 104 1 (< 20 ) 30 ug/L 12/18/2008

1,1-Dichloroethane LCS 33.3 111 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.9 110 1 (< 20 ) 30 ug/L 12/18/2008

2-Chlorotoluene LCS 32.5 108 ( 80-125 ) 30 ug/L 12/18/2008

LCSD 32.3 108 1 (< 20 ) 30 ug/L 12/18/2008

Trichloroethene LCS 32.4 108 ( 80-125 ) 30 ug/L 12/18/2008

LCSD 32.9 110 2 (< 20 ) 30 ug/L 12/18/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876588 Lab Control Sample

876589 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

trans-1,2-Dichloroethene LCS 32.4 108 ( 79-132 ) 30 ug/L 12/18/2008

LCSD 32.2 107 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dichlorobenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 31.6 105 0 (< 20 ) 30 ug/L 12/18/2008

2,2-Dichloropropane LCS 34.5 115 ( 80-132 ) 30 ug/L 12/18/2008

LCSD 33.8 113 2 (< 20 ) 30 ug/L 12/18/2008

Hexachlorobutadiene LCS 32.2 107 ( 77-125 ) 30 ug/L 12/18/2008

LCSD 31.7 106 1 (< 20 ) 30 ug/L 12/18/2008

Isopropylbenzene (Cumene) LCS 34.3 114 ( 80-121 ) 30 ug/L 12/18/2008

LCSD 34.1 114 1 (< 20 ) 30 ug/L 12/18/2008

1,2-Dichloropropane LCS 32.0 107 ( 80-121 ) 30 ug/L 12/18/2008

LCSD 32.7 109 2 (< 20 ) 30 ug/L 12/18/2008

1,1-Dichloropropene LCS 32.4 108 ( 80-122 ) 30 ug/L 12/18/2008

LCSD 32.3 108 0 (< 20 ) 30 ug/L 12/18/2008

1,1,2-Trichloroethane LCS 32.3 108 ( 77-120 ) 30 ug/L 12/18/2008

LCSD 32.5 108 0 (< 20 ) 30 ug/L 12/18/2008

1,3-Dichlorobenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 12/18/2008

LCSD 32.0 107 0 (< 20 ) 30 ug/L 12/18/2008

1,2,3-Trichlorobenzene LCS 31.0 103 ( 77-120 ) 30 ug/L 12/18/2008

LCSD 30.6 102 1 (< 20 ) 30 ug/L 12/18/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 99 ( 73-120 ) 12/18/2008

LCSD 100 2 12/18/2008

Toluene-d8 <surr> LCS 99 ( 80-120 ) 12/18/2008

LCSD 100 1 12/18/2008

4-Bromofluorobenzene <surr> LCS 98 ( 76-120 ) 12/18/2008

LCSD 98 0 12/18/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Prep

876588 Lab Control Sample

876589 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX19107

SW5030B

12/18/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS10317

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.# Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Original

Prep

876591 Matrix Spike

876592 Matrix Spike Duplicate

876590

Water (Surface, Eff., Ground)

VXX19107

Volatiles Extraction AFCEE 3.1 8260 (

12/18/2008

QC results affect the following production samples:

1086721001, 1086721002, 1086721003

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene MS ND 33 110 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.2 114 4 (< 20 ) 30.0 ug/L 12/18/2008

Toluene MS ND 32.2 107 ( 77-120 ) 30.0 ug/L 12/18/2008

MSD 33.4 111 4 (< 20 ) 30.0 ug/L 12/18/2008

Ethylbenzene MS ND 33.1 110 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.1 114 3 (< 20 ) 30.0 ug/L 12/18/2008

n-Butylbenzene MS ND 35.1 117 ( 80-124 ) 30.0 ug/L 12/18/2008

MSD 37.7 126* 7 (< 20 ) 30.0 ug/L 12/18/2008

1,4-Dichlorobenzene MS ND 33 110 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 35.3 118 7 (< 20 ) 30.0 ug/L 12/18/2008

1,2-Dichloroethane MS ND 38 127 ( 80-129 ) 30.0 ug/L 12/18/2008

MSD 34.5 115 10 (< 20 ) 30.0 ug/L 12/18/2008

1,3,5-Trimethylbenzene MS ND 33.8 113 ( 80-128 ) 30.0 ug/L 12/18/2008

MSD 35.4 118 5 (< 20 ) 30.0 ug/L 12/18/2008

4-Chlorotoluene MS ND 33.7 112 ( 79-128 ) 30.0 ug/L 12/18/2008

MSD 35.3 118 5 (< 20 ) 30.0 ug/L 12/18/2008

Chlorobenzene MS ND 30.5 102 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 31.5 105 3 (< 20 ) 30.0 ug/L 12/18/2008

4-Methyl-2-pentanone (MIBK) MS ND 102 113 ( 69-134 ) 90.0 ug/L 12/18/2008

MSD 103 115 1 (< 20 ) 90.0 ug/L 12/18/2008

cis-1,2-Dichloroethene MS ND 38.6 129* ( 80-125 ) 30.0 ug/L 12/18/2008

MSD 36.3 121 6 (< 20 ) 30.0 ug/L 12/18/2008

4-Isopropyltoluene MS ND 34.1 114 ( 80-125 ) 30.0 ug/L 12/18/2008

MSD 36.4 121 7 (< 20 ) 30.0 ug/L 12/18/2008

cis-1,3-Dichloropropene MS ND 31.7 106 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 31.9 106 1 (< 20 ) 30.0 ug/L 12/18/2008

n-Propylbenzene MS ND 33.8 113 ( 80-129 ) 30.0 ug/L 12/18/2008

MSD 35.4 118 5 (< 20 ) 30.0 ug/L 12/18/2008

Styrene MS ND 31.2 104 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 31.5 105 1 (< 20 ) 30.0 ug/L 12/18/2008

Dibromomethane MS ND 37.2 124* ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.1 114 9 (< 20 ) 30.0 ug/L 12/18/2008

trans-1,3-Dichloropropene MS ND 33.6 112 ( 80-124 ) 30.0 ug/L 12/18/2008

MSD 33.5 112 0 (< 20 ) 30.0 ug/L 12/18/2008

1,2,4-Trichlorobenzene MS ND 31.7 106 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.1 114 7 (< 20 ) 30.0 ug/L 12/18/2008

Acetone MS ND 104 116 ( 50-135 ) 90.0 ug/L 12/18/2008
Matrix

SGS Ref.# Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Original

Prep

876591 Matrix Spike

876592 Matrix Spike Duplicate

876590

Water (Surface, Eff., Ground)

VXX19107

Volatiles Extraction AFCEE 3.1 8260 (

12/18/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MSD 102 114 2 (< 20 ) 90.0 ug/L 12/18/2008

1,1,2,2-Tetrachloroethane MS ND 34.1 114 ( 76-123 ) 30.0 ug/L 12/18/2008

MSD 34.8 116 2 (< 20 ) 30.0 ug/L 12/18/2008

1,2-Dibromo-3-chloropropane MS ND 35.2 117 ( 73-130 ) 30.0 ug/L 12/18/2008

MSD 36.1 120 2 (< 20 ) 30.0 ug/L 12/18/2008

Methyl-t-butyl ether MS ND 55 122* ( 80-120 ) 45.0 ug/L 12/18/2008

MSD 53.2 118 3 (< 20 ) 45.0 ug/L 12/18/2008

Tetrachloroethene MS ND 32.4 108 ( 79-122 ) 30.0 ug/L 12/18/2008

MSD 32.9 110 2 (< 20 ) 30.0 ug/L 12/18/2008

Dibromochloromethane MS ND 34.5 115 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 33.4 111 3 (< 20 ) 30.0 ug/L 12/18/2008

1,3-Dichloropropane MS ND 35.1 117 ( 80-121 ) 30.0 ug/L 12/18/2008

MSD 34.4 115 2 (< 20 ) 30.0 ug/L 12/18/2008

1,2-Dibromoethane MS ND 34.5 115 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 33.8 113 2 (< 20 ) 30.0 ug/L 12/18/2008

Carbon tetrachloride MS ND 36.5 122 ( 80-126 ) 30.0 ug/L 12/18/2008

MSD 35.1 117 4 (< 20 ) 30.0 ug/L 12/18/2008

1,1,1,2-Tetrachloroethane MS ND 33.1 110 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 32.6 109 2 (< 20 ) 30.0 ug/L 12/18/2008

Chloroform MS ND 38.5 128* ( 80-124 ) 30.0 ug/L 12/18/2008

MSD 35.1 117 9 (< 20 ) 30.0 ug/L 12/18/2008

Bromobenzene MS ND 32.4 108 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 33.6 112 4 (< 20 ) 30.0 ug/L 12/18/2008

Chloromethane MS ND 28.8 96 ( 67-125 ) 30.0 ug/L 12/18/2008

MSD 31.3 104 8 (< 20 ) 30.0 ug/L 12/18/2008

1,2,3-Trichloropropane MS ND 32.7 109 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.8 116 6 (< 20 ) 30.0 ug/L 12/18/2008

Bromomethane MS ND 32 107 ( 30-140 ) 30.0 ug/L 12/18/2008

MSD 33.8 113 6 (< 20 ) 30.0 ug/L 12/18/2008

Bromochloromethane MS ND 34 113 ( 77-129 ) 30.0 ug/L 12/18/2008

MSD 33.8 113 1 (< 20 ) 30.0 ug/L 12/18/2008

Vinyl chloride MS ND 31 103 ( 72-145 ) 30.0 ug/L 12/18/2008

MSD 32.0 107 3 (< 20 ) 30.0 ug/L 12/18/2008

Dichlorodifluoromethane MS ND 33.3 111 ( 62-153 ) 30.0 ug/L 12/18/2008

MSD 33.8 113 2 (< 20 ) 30.0 ug/L 12/18/2008

Chloroethane MS ND 49.8 166* ( 67-133 ) 30.0 ug/L 12/18/2008

MSD 51.3 171* 3 (< 20 ) 30.0 ug/L 12/18/2008

sec-Butylbenzene MS ND 34.1 114 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 35.9 120 5 (< 20 ) 30.0 ug/L 12/18/2008

Bromodichloromethane MS ND 34.5 115 ( 80-120 ) 30.0 ug/L 12/18/2008
Matrix

SGS Ref.# Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Original

Prep

876591 Matrix Spike

876592 Matrix Spike Duplicate

876590

Water (Surface, Eff., Ground)

VXX19107

Volatiles Extraction AFCEE 3.1 8260 (

12/18/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MSD 32.6 109 5 (< 20 ) 30.0 ug/L 12/18/2008

1,1-Dichloroethene MS ND 37.4 125 ( 76-130 ) 30.0 ug/L 12/18/2008

MSD 35.8 119 5 (< 20 ) 30.0 ug/L 12/18/2008

2-Butanone (MEK) MS ND 105 117 ( 66-136 ) 90.0 ug/L 12/18/2008

MSD 105 116 0 (< 20 ) 90.0 ug/L 12/18/2008

Methylene chloride MS ND 31.4 105 ( 63-131 ) 30.0 ug/L 12/18/2008

MSD 32.3 108 3 (< 20 ) 30.0 ug/L 12/18/2008

Trichlorofluoromethane MS ND 38 127 ( 68-145 ) 30.0 ug/L 12/18/2008

MSD 37.4 125 2 (< 20 ) 30.0 ug/L 12/18/2008

P & M -Xylene MS ND 66.4 111 ( 80-120 ) 60.0 ug/L 12/18/2008

MSD 68.6 114 3 (< 20 ) 60.0 ug/L 12/18/2008

Naphthalene MS ND 31.3 104 ( 75-120 ) 30.0 ug/L 12/18/2008

MSD 34.1 114 8 (< 20 ) 30.0 ug/L 12/18/2008

o-Xylene MS ND 32.9 110 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 33.9 113 3 (< 20 ) 30.0 ug/L 12/18/2008

Bromoform MS ND 34.6 115 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.2 114 1 (< 20 ) 30.0 ug/L 12/18/2008

1-Chlorohexane MS ND 53.6 119 ( 70-125 ) 45.0 ug/L 12/18/2008

MSD 55.6 123 4 (< 20 ) 45.0 ug/L 12/18/2008

1,2,4-Trimethylbenzene MS ND 33.2 111 ( 80-125 ) 30.0 ug/L 12/18/2008

MSD 34.8 116 5 (< 20 ) 30.0 ug/L 12/18/2008

tert-Butylbenzene MS ND 34.8 116 ( 80-122 ) 30.0 ug/L 12/18/2008

MSD 36.8 123* 6 (< 20 ) 30.0 ug/L 12/18/2008

1,1,1-Trichloroethane MS ND 34.5 115 ( 80-122 ) 30.0 ug/L 12/18/2008

MSD 33.0 110 5 (< 20 ) 30.0 ug/L 12/18/2008

1,1-Dichloroethane MS ND 37 123* ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.8 116 6 (< 20 ) 30.0 ug/L 12/18/2008

2-Chlorotoluene MS ND 32.8 109 ( 80-125 ) 30.0 ug/L 12/18/2008

MSD 34.8 116 6 (< 20 ) 30.0 ug/L 12/18/2008

Trichloroethene MS ND 33 110 ( 80-125 ) 30.0 ug/L 12/18/2008

MSD 34.4 115 4 (< 20 ) 30.0 ug/L 12/18/2008

trans-1,2-Dichloroethene MS ND 38.4 128 ( 79-132 ) 30.0 ug/L 12/18/2008

MSD 34.2 114 12 (< 20 ) 30.0 ug/L 12/18/2008

1,2-Dichlorobenzene MS ND 32.4 108 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 33.9 113 4 (< 20 ) 30.0 ug/L 12/18/2008

2,2-Dichloropropane MS ND 39.7 132 ( 80-132 ) 30.0 ug/L 12/18/2008

MSD 38.6 129 3 (< 20 ) 30.0 ug/L 12/18/2008

Hexachlorobutadiene MS ND 33.8 113 ( 77-125 ) 30.0 ug/L 12/18/2008

MSD 35.9 120 6 (< 20 ) 30.0 ug/L 12/18/2008

Isopropylbenzene (Cumene) MS ND 34.8 116 ( 80-121 ) 30.0 ug/L 12/18/2008
Matrix

SGS Ref.# Printed Date/Time 12/22/2008 11:45

Batch

Method

Date

Original

Prep

876591 Matrix Spike

876592 Matrix Spike Duplicate

876590

Water (Surface, Eff., Ground)

VXX19107

Volatiles Extraction AFCEE 3.1 8260 (

12/18/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MSD 35.5 118 2 (< 20 ) 30.0 ug/L 12/18/2008

1,2-Dichloropropane MS ND 33.3 111 ( 80-121 ) 30.0 ug/L 12/18/2008

MSD 34.3 114 3 (< 20 ) 30.0 ug/L 12/18/2008

1,1-Dichloropropene MS ND 34.4 115 ( 80-122 ) 30.0 ug/L 12/18/2008

MSD 34.8 116 1 (< 20 ) 30.0 ug/L 12/18/2008

1,1,2-Trichloroethane MS ND 33.7 112 ( 77-120 ) 30.0 ug/L 12/18/2008

MSD 33.4 111 1 (< 20 ) 30.0 ug/L 12/18/2008

1,3-Dichlorobenzene MS ND 32.7 109 ( 80-120 ) 30.0 ug/L 12/18/2008

MSD 34.6 115 6 (< 20 ) 30.0 ug/L 12/18/2008

1,2,3-Trichlorobenzene MS ND 31.2 104 ( 77-120 ) 30.0 ug/L 12/18/2008

MSD 33.6 112 7 (< 20 ) 30.0 ug/L 12/18/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> MS 34.2 114 ( 73-120 ) 12/18/2008

MSD 29.9 100 13 12/18/2008

Toluene-d8 <surr> MS 29.7 99 ( 80-120 ) 12/18/2008

MSD 29.3 98 2 12/18/2008

4-Bromofluorobenzene <surr> MS 29.3 98 ( 76-120 ) 12/18/2008

MSD 29.6 99 1 12/18/2008

Batch

Method

Instrument

VMS10317

SW8260B

HP 5890 Series II MS3 VNA