Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

883 Wa ukegan 8 subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

883 Waukegan 8 As Received Higher Heating Value 883 Waukegan 8 As Received % Moisture 883 Waukegan 8 As Received % Ash 883 Waukegan 8 As Received % Sulfur 883 Waukegan 8 Dry basis Higher Heating Value 883 Waukegan 8 Dry basis % Ash 883 Waukegan 8 Dry basis % Sulfur 883 Waukegan 8 Dry basis Antim ony 883 Waukegan 8 Dry basis Arsenic 883 Waukegan 8 Dry basis Beryllium 883 Waukegan 8 Dry basis Cadmium 883 Waukegan 8 Dry basis Chlorine 883 Waukegan 8 Dry basis Chromium 883 Waukegan 8 Dry basis Cobalt 883 Waukegan 8 Dry basis Fluorine 883 Waukegan 8 Dry basis Lead 883 Waukegan 8 Dry basis Manganese 883 Waukegan 8 Dry basis Mercury 883 Waukegan 8 Dry basis Nickel 883 Waukegan 8 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 Method B ASTM D5865 ASTM D3174 ASTM D4239 Method B ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6721 ASTM D6357 ASTM D6357 ASTM D3761 ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 SW -846 7740EIA Facility Code Facility

Name Boiler ID 883 Waukegan 8

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) Composite Sample 1 7/13/2010 7/13/2010 8731.00 Composite Sample 3 7/14/2010 7/14/2010 8718.00 Composite Sample 5 7/15/2010 7/15/2010 8718.00 Fuel Testing ResultsHAPs Test Group

Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Btu/lb 26.78 4.67 0.34 11924 Btu/lb Btu/lb 27.23 4.54 0.34 11981 Btu/lb Btu/lb 27.37 4.56 0.36 12003 Btu/lb% A

sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) 6.38 0.46 <10 ppm 0.09 μg/g <1 μg/g <1 6.24 0.46 <10 ppm 0.10 μg/g <1 μg/g <1 6.28 0.50 <10 ppm 0.07 μg/g <1 μg/g <1Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/g μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/g μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/gManganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) 13 μg/g 3 μg/g <1 μg/g 65 ppm 1 16 μg/g 4 μg/g <1 μg/g 58 ppm 1 15 μg/g 5 μg/g <1 μg/g 56 ppm 1Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon μg/g 0 45.92 6.38 47.70 67.34 μg/g 0 45.73 6.24 48.03 67.56 μg/g 0.00 45.61 6.28 48.11 69.03 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen 9.17 1.50 0.46 15.15 9.11 1.47 0.46 15.16 4.87 1.17 0.50 18.15 Ultimate Analy

ses, % by

wtEIA Facility Code Facility

Name Boiler ID 883 Waukegan 8

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) Composite Sample 2 7/13/2010 7/13/2010 8663.00 Composite Sample 4 7/14/2010 7/14/2010 8723.00 Composite Sample 6 7/15/2010 7/15/2010 8544.00 Fuel Testing ResultsHAPs Test Group

Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Btu/lb 27.22 5.27 0.34 11903 Btu/lb Btu/lb 27.63 4.31 0.33 12054 Btu/lb Btu/lb 28.59 4.73 0.42 11965 Btu/lb% A

sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) 7.24 0.47 <10 ppm 0.10 μg/g <1 μg/g <1 5.96 0.46 <10 ppm 0.09 μg/g <1 μg/g <1 6.63 0.59 <10 ppm 0.10 μg/g <1 μg/g <1Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units μg/g 0.3 μg/g < 0.2 μg/g 5 μg/g <2 μg/g μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/g μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/gManganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) 16 μg/g 4 μg/g <1 μg/g 46 ppm 1 14 μg/g 3 μg/g <1 μg/g 52 ppm 1 23 μg/g 4 μg/g <1 μg/g 41 ppm 1Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon μg/g 0 45.19 7.24 47.57 66.82 μg/g 0 46.20 5.96 47.84 67.68 μg/g 0 46.78 6.63 46.59 67.25 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen 8.91 1.48 0.47 15.08 9.26 1.51 0.46 15.13 9.33 1.48 0.59 14.72 Ultimate Analy

ses, % by

wtEIA Facility Code Facility

Name Boiler ID 883 Waukegan 8

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) Composite Sample 7 7/20/2010 7/20/2010 9232.00 Composite Sample 8 7/21/2010 7/21/2010 9877.00 Composite Sample 9 7/22/2010 7/22/2010 9964.00 Fuel Testing ResultsHAPs Test Group

Dioxin/furan HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Btu/lb 23.62 4.10 0.31 12088 Btu/lb Btu/lb 17.71 4.64 0.33 12002 Btu/lb Btu/lb 17.48 4.60 0.36 12075 Btu/lb% A

sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) 5.37 0.40 <10 ppm 0.08 μg/g <1 μg/g <1 5.64 0.41 <10 ppm 0.11 μg/g <1 μg/g <1 4.60 0.36 <10 ppm 0.08 μg/g <1 μg/g <1Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units μg/g 0.2 μg/g < 0.2 μg/g 3 μg/g <2 μg/g μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/g μg/g 0.2 μg/g < 0.2 μg/g 4 μg/g <2 μg/gManganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) 19 μg/g 4 μg/g <1 μg/g 44 ppm 1 28 μg/g 4 μg/g <1 μg/g 48 ppm 1 15 μg/g 3 μg/g <1 μg/g 48 ppm 1Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen μg/g 0 47.01 5.37 47.62 70.28 9.17 μg/g 0 47.05 5.64 47.31 67.08 8.99 μg/g 0 47.13 5.58 47.29 68.88 4.84 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nitrogen Total Sulfur Oxygen 1.52 0.40 13.26 1.47 0.41 16.41 1.13 0.43 19.14 Ultimate Analy

ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm