U.S. EPA Data Request 

Emissions Test Report 

Prepared for: 

Johns Manville 

Winder Plant 

713 Bankhead Hwy. 

Winder, GA 30680 

Project No. 11-4191.05 

February 22, 2012 

BT Environmental Consulting, Inc. 

4949 Fernlee Avenue 

Royal Oak, Michigan 48073 

(248) 548-8070 
Johns Manville Winder BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

i

Executive Summary

For the purpose of assisting in the development of any emission standard under Section 7412 of 

the Clean Air Act (CAA), Section 114 of the CAA gives the United States Environmental 

Protection Agency (U.S. EPA) authority to require that persons who operate any emission source 

“sample such emissions (in accordance with such procedures or methods, at such locations, at 

such intervals, during such periods and in such manner as the Administrator shall prescribe)”. 

Consistent with this authority, U.S. EPA has required that Johns Manville (JM) sample emissions 

for the purpose of providing residual risk-related data for the National Emission Standards for 

Hazardous Air Pollutants (NESHAP) for Wool Fiberglass Manufacturing1. 

To assist in collecting the agreed upon data, BT Environmental Consulting, Inc. (BTEC) was 

retained by JM to evaluate emission rates of the following pollutants from two exhaust stacks 

associated with Lines 105 and 106 located at the JM plant in Winder, Georgia: 

• Filterable particulate matter (PM) using U.S. EPA Methods 5/29 

• Filterable chromium (FCr) using U.S. EPA Method 29 

• Vaporous chromium (VCr) using U.S. EPA Method 29 

• Total chromium (TCr) using U.S. EPA Method 29 

• Hexavalent chromium (Cr+6) using SW-846 Method 0061 

• TCr using SW-846 Method 0061 

Tables I and II on the following page summarize the overall results of the emissions test program 

for Lines 105 and 106, respectively. 

 

1

 Codified at 40 CFR 63, Subpart NNN 
Johns Manville Winder BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

ii

Table I 

Overall Emissions Test Results Summary 

Line 105 

Test Dates: January 25th and 26th, 2012 

Test Methods Pollutant MDL 

used 

Emission 

Rate 

(lbs/hour) 

Emission 

Rate 

(lbs/ton) 

Emission 

Rate 

(mg/dscm) 

USEPA 

Method 5/29 Filterable PM < 5.8 x 10-2 4.9 x 10-1

Filterable Chromium 

(FCr) 3.2 x 10-5 2.6 x 10-4

Vaporous Chromium 

(VCr) < 2.8 x 10-6 2.4 x 10-5

USEPA 

Method 29 

Total Chromium (TCr) < 3.4 x 10-5 2.9 x 10-4

Hexavalent Chromium 

(Cr+6) < 5.6 x 10-6 4.9 x 10-5 USEPA 

Method 0061 Total Chromium (TCr) < 9.9 x 10-5 8.7 x 10-4

Table II 

Overall Emissions Test Results Summary 

Line 106 

Test Dates: January 23rd and 24th, 2012 

Test Methods Pollutant MDL 

used 

Emission 

Rate 

(lbs/hour) 

Emission 

Rate 

(lbs/ton) 

Emission 

Rate 

(mg/dscm) 

USEPA 

Method 5/29 Filterable PM < 1.3 x 10-2 1.8 x 10-1

Filterable Chromium 

(FCr) 8.4 x 10-5 7.3 x 10-4

Vaporous Chromium 

(VCr) < 3.6 x 10-6 3.1 x 10-5

USEPA 

Method 29 

Total Chromium (TCr) < 4.3 x 10-5 3.7 x 10-4

Hexavalent Chromium 

(Cr+6) < 8.5 x 10-6 7.2 x 10-5 USEPA 

Method 0061 Total Chromium (TCr) < 1.6 x 10-4 1.4 x 10-3

Notes: (1) Pollutant emission rates in terms of mg/dscm were not corrected to 7% O2 because exhaust from the 

process is essentially ambient (i.e., approximately 20.9% O2). 

(2) The “less than” symbol (<) included in the table indicates that the emission rate was calculated using the method 

detection limit (MDL) value instead of zero because the analytical result was below the MDL for one or more of the 

sample fractions. 
Johns Manville Winder BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

iii

TABLE OF CONTENTS 

1.0 INTRODUCTION............................................................................................................... 1

2.0 PROCESS DESCRIPTION ............................................................................................... 2

2.1 PROCESS MONITORING ....................................................................................................... 2 

3.0 SAMPLING AND ANALYTICAL METHODOLOGIES.............................................. 2

3.1 EXHAUST GAS VELOCITY, MOLECULAR WEIGHT, AND MOISTURE CONTENT .................... 2 

3.2 PM, FCR, VCR, AND TCR CONCENTRATIONS AND EMISSION RATES ................................. 3 

3.3 CR+6 AND TCR CONCENTRATIONS AND EMISSION RATES................................................... 3 

4.0 TEST RESULTS ................................................................................................................. 3

TABLES

Table 1 –Test Personnel 

Table 2 – Line 105 Overall Emission Test Results Summary 

Table 3 – Line 106 Overall Emission Test Results Summary 

Table 4 – Line 105 Method 0061 Emission Rate Results Summary 

Table 5 – Line 105 Method 5/29 Emission Rate Results Summary 

Table 6 – Line 106 Method 0061 Emission Rate Results Summary 

Table 7 – Line 106 Method 5/29 Emission Rate Results Summary 

FIGURES

Figure 1 – Line 106 Exhaust Stack Traverse Point Diagram 

Figure 2 – Method 3A Sampling Train Schematic Drawing 

Figure 3 – Method 5/29 Sampling Train Schematic Drawing 

Figure 4 – Method 0061 Sampling Train Schematic Drawing 

APPENDICES

Appendix A – Field and Computer Generated Raw Data and Field Notes 

Appendix B – Process Data 

Appendix C – Equipment Calibration Documents 

Appendix D – Laboratory Analytical Reports 
Johns Manville Willows BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

1

1.0 Introduction 

For the purpose of assisting in the development of any emission standard under Section 7412 of 

the Clean Air Act (CAA), Section 114 of the CAA gives the United States Environmental 

Protection Agency (U.S. EPA) authority to require that persons who operate any emission source 

“sample such emissions (in accordance with such procedures or methods, at such locations, at 

such intervals, during such periods and in such manner as the Administrator shall prescribe)”. 

Consistent with this authority, U.S. EPA has required that Johns Manville (JM) sample emissions 

for the purpose of providing residual risk-related data for the National Emission Standards for 

Hazardous Air Pollutants (NESHAP) for Wool Fiberglass Manufacturing2. 

To assist in collecting the agreed upon data, BT Environmental Consulting, Inc. (BTEC) was 

retained by JM to evaluate emission rates of the following pollutants from two exhaust stacks 

associated with Line 105 and 106 located at the JM plant in Winder, Georgia: 

• Filterable particulate matter (PM) using U.S. EPA Methods 5/29 

• Filterable chromium (FCr) using U.S. EPA Method 29 

• Vaporous chromium (VCr) using U.S. EPA Method 29 

• Total chromium (TCr) using U.S. EPA Method 29 

• Hexavalent chromium (Cr+6) using SW-846 Method 0061 

• TCr using SW-846 Method 0061 

The emissions test program was conducted on January 23 through 26, 2012. The test program 

consisted of triplicate emission tests for each parameter. The field sampling portion of the 

emissions test program included the personnel summarized by Table 1.

Table 1 

Emissions Test Program Personnel

Personnel Affiliation 

Jim Sharp BTEC 

Paul Molenda BTEC 

Paul Draper BTEC 

Jeff Peitzsch BTEC 

Patti Blevins Johns Manville 

 

2

 Codified at 40 CFR 63, Subpart NNN 
Johns Manville Willows BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

2

2.0 Process Description

Line 106 electric melters are charged with batch and cullet feeds. The glass melt is then sent to 

the forming and curing sections. The three melters in Line 105 all exhaust through a common 

baghouse to a single stack. The two melters in Line 106 both exhaust through a common 

baghouse to one stack. 

2.1 Process Monitoring 

Process and control equipment data collected during the emissions test program includes the 

following: 

(1) Melter Rate (lbs/hr) 

(2) Melter dust collector pressure drop (inches H2O) 

Process production data is available in Appendix B. Control equipment data will be available to 

U.S. EPA on request. 

3.0 Sampling and Analytical Methodologies 

Sampling and analytical methodologies for the emissions test program can be separated into 

three categories as follows: 

(1) Measurement of exhaust gas velocity, molecular weight, and moisture content; 

(2) Measurement of exhaust gas PM, FCr, VCr, and TCr concentrations and emission rates 

using Methods 5/29; and 

(3) Measurement of exhaust gas CR+6 and TCr concentrations and emission rates using 

Method 0061. 

Descriptions of sampling and analytical methodologies by category are summarized by Sections 

3.1 through 3.3, respectively. 

3.1 Exhaust Gas Velocity, Molecular Weight, and Moisture Content 

Measurement of exhaust gas velocity, molecular weight, and moisture content were conducted 

using the following reference test methods codified at Title 40, Part 60, Appendix A of the Code 

of Federal Regulations (40 CFR 60, Appendix A): 

• Method 1 - “Sample and Velocity Traverses for Stationary Sources” 

• Method 2 - “Determination of Stack Gas Velocity and Volumetric Flowrate” 

• Method 3A - “Determination of Molecular Weight of Dry Stack Gas” 

(Integrated tedlar bags) 

• Method 4 - “Determination of Moisture Content in Stack Gases”

These test methods were used to evaluate exhaust gas flowrates in conjunction with the 

isokinetic sampling methodologies. 
Johns Manville Willows BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

3

Stack gas velocity traverses were conducted in accordance with the procedures outlined in 

Method 1 and Method 2 (see Figure 1 for a traverse location drawing). An S-type pitot tube with 

a thermocouple assembly, calibrated in accordance with Method 2, Section 4.1.1, was used to 

measure exhaust gas velocity pressures (using a manometer) and temperatures at each location 

during testing. The S-type pitot tube dimensions was within specified limits, therefore, a 

baseline pitot tube coefficient of 0.84 (dimensionless) was assigned. 

Molecular weight was determined according to USEPA Method 3A, “Determination of Oxygen 

and Carbon Dioxide Concentrations in Emissions from Stationary Sources”. The O2 content of 

the exhaust gas was measured using an M&C Products PMA 100-L O2 gas analyzer and the CO2

content of the exhaust gas was measured using a California Analytical Instruments (CAI) 600 

Series CO2 gas analyzer. A sample of the gas stream was drawn through an insulated stainlesssteel probe into a heated sample line. The sample was then connected to sample conditioner to 

remove the moisture from the sample before it entered the analyzers. Data was recorded at 4-

second intervals on a PC equipped with data acquisition software. 

 

Exhaust gas moisture content was evaluated using Method 4. Exhaust gas moisture content was 

determined gravimetrically. 

3.2 PM, FCr, VCr, and TCr Concentrations and Emission Rates

PM, FCr, VCr, and TCr concentrations and emission rates were measured using the procedures 

of 40 CFR 60, Appendix A, Methods 5 and 29. Selected metals concentrations and emission 

rates were measured using BTEC’s Nutech® Model 2010 modular isokinetic stack sampling 

system. This system consisted of (1) a borosilicate glass or quartz nozzle, (2) a steel probe 

w/glass liner, (3) a heated quartz fiber filter assembly, (4) a set of four GS impingers, (5) a 

length of sample line, and (6) a Nutech® control case equipped with a pump, dry gas meter, and 

calibrated orifice. Prior to each test, the first two impingers were filled with 100 ml of a 5% 

nitric acid (HNO3)/10% hydrogen peroxide solution, the third impinger was empty, and the 

fourth contained approximately 300 g of silica gel desiccant. A schematic drawing of the 

PM/metals sampling train is provided as Figure 3. 

3.3 Cr+6 and TCr Concentrations and Emission Rates 

Measurement of Cr+6 and TCr concentrations and emission rates were measured using the 

procedures Method 0061. Cr+6 and TCr concentrations and emission rates were measured using 

BTEC’s Nutech® Model 2010 modular isokinetic stack sampling system. This system consisted 

of (1) a glass nozzle, (2) a heated steel probe with a glass probe liner, (4) a Teflon tee with a 

recirculating pump, (5) five GS impingers, (6) a length of sample line, and (7) a Nutech® control 

case equipped with a pump, dry gas meter, and calibrated orifice. Prior to each test, the first 

impinger was filled with 150 mL of 0.1N KOH, the next two were filled with 75 mL of 0.1 N 

KOH, the fourth was empty, and the last impinger contained approximately 300 g of silica gel 

desiccant. A schematic drawing of the Method 0061 sampling train is provided as Figure 4. 

4.0 Test Results 
Johns Manville Willows BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

4

The overall results of the emissions test program for Lines 105 and 106 are summarized by 

Tables 2 and 3, respectively. 

Table 2 

Overall Emissions Test Results Summary 

Line 105 

Test Dates: January 25th and 26th, 2012 

Test Methods Pollutant MDL 

used 

Emission 

Rate 

(lbs/hour) 

Emission 

Rate 

(lbs/ton) 

Emission 

Rate 

(mg/dscm) 

USEPA 

Method 5/29 Filterable PM < 5.8 x 10-2 4.9 x 10-1

Filterable Chromium 

(FCr) 3.2 x 10-5 2.6 x 10-4

Vaporous Chromium 

(VCr) < 2.8 x 10-6 2.4 x 10-5

USEPA 

Method 29 

Total Chromium (TCr) < 3.4 x 10-5 2.9 x 10-4

Hexavalent Chromium 

(Cr+6) < 5.6 x 10-6 4.9 x 10-5 USEPA 

Method 0061 Total Chromium (TCr) < 9.9 x 10-5 8.7 x 10-4

Notes: (1) Pollutant emission rates in terms of mg/dscm were not corrected to 7% O2 because exhaust from the 

process is essentially ambient (i.e., approximately 20.9% O2). 

(2) The “less than” symbol (<) included in the table indicates that the emission rate was calculated using the method 

detection limit (MDL) value instead of zero because the analytical result was below the MDL for one or more of the 

sample fractions. 
Johns Manville Willows BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

5

Table 3 

Overall Emissions Test Results Summary 

Line 106 

Test Dates: January 23rd and 24th, 2012 

Test Methods Pollutant MDL 

used 

Emission 

Rate 

(lbs/hour) 

Emission 

Rate 

(lbs/ton) 

Emission 

Rate 

(mg/dscm) 

USEPA 

Method 5/29 Filterable PM < 1.3 x 10-2 1.8 x 10-1

Filterable Chromium 

(FCr) 8.4 x 10-5 7.3 x 10-4

Vaporous Chromium 

(VCr) < 3.6 x 10-6 3.1 x 10-5

USEPA 

Method 29 

Total Chromium (TCr) < 4.3 x 10-5 3.7 x 10-4

Hexavalent Chromium 

(Cr+6) < 8.5 x 10-6 7.2 x 10-5 USEPA 

Method 0061 Total Chromium (TCr) < 1.6 x 10-4 1.4 x 10-3

Notes: (1) Pollutant emission rates in terms of mg/dscm were not corrected to 7% O2 because exhaust from the 

process is essentially ambient (i.e., approximately 20.9% O2). 

(2) The “less than” symbol (<) included in the table indicates that the emission rate was calculated using the method 

detection limit (MDL) value instead of zero because the analytical result was below the MDL for one or more of the 

sample fractions. 

Detailed results for individual emission test runs are summarized in Tables 3 and 4. Field and 

computer-generated data sheets are included in Appendix A. Process data associated with the 

emissions test program is provided in Appendix B. Equipment calibration documents are 

provided in Appendix C. Laboratory analytical results are available in Appendix D. 
Johns Manville Willows BTEC Project No. 11-4191.05 

U.S. EPA Emissions Test Report February 22, 2012 

6

Limitations

The information and opinions rendered in this report are exclusively for use by Johns Manville. 

BTEC will not distribute or publish this report without Johns Manville’s consent except as 

required by law or court order. BTEC accepts responsibility for the competent performance of 

its duties in executing the assignment and preparing reports in accordance with the normal 

standards of the profession, but disclaims any responsibility for consequential damages. 

This report was prepared by: 

Brandon Chase 

Staff Environmental Engineer 

This report was reviewed by: 

Randal J. Tysar 

Senior Environmental Engineer 
Tables 
Table 3

Line 89 Melter Dust Collector Method 5/29 Emission Rate Results Summary

Company JM Winder

Source Designation 105

Test Date 1/25/2012 1/26/2012 1/26/2012

Meter/Nozzle Information P-1 P-2 P-3 Average

Meter Temperature Tm (F) 79.8 76.9 87.6 81.4

Meter Pressure - Pm (in. Hg) 30.5 30.3 30.3 30.4

Measured Sample Volume (Vm) 226.6 222.0 231.6 226.7

Sample Volume (Vm-Std ft3) 225.5 220.8 225.8 224.0

Sample Volume (Vm-Std m3) 6.39 6.25 6.39 6.34

Condensate Volume (Vw-std) 3.739 4.885 5.946 4.856

Gas Density (Ps(std) lbs/ft3) (wet) 0.0741 0.0739 0.0739 0.0740

Gas Density (Ps(std) lbs/ft3) (dry) 0.0745 0.0745 0.0746 0.0745

Total weight of sampled gas (m g lbs) (wet) 16.98 16.68 17.13 16.93

Total weight of sampled gas (m g lbs) (dry) 16.80 16.45 16.85 16.70

Nozzle Size - An (sq. ft.) 0.000369 0.000369 0.000369 0.000369

Isokinetic Variation - I 99.8 98.3 100.6 99.6

Production Data

Production Data (lb/hr)

Stack Data

Average Stack Temperature - Ts (F) 114.0 112.7 117.7 114.8

Molecular Weight Stack Gas- dry (Md) 28.83 28.8 28.9 28.8

Molecular Weight Stack Gas-wet (Ms) 28.65 28.6 28.6 28.6

Stack Gas Specific Gravity (Gs) 0.989 0.987 0.987 0.988

Percent Moisture (Bws) 1.63 2.16 2.57 2.12

Water Vapor Volume (fraction) 0.0163 0.0216 0.0257 0.0212

Pressure - Ps ("Hg) 30.3 30.1 30.1 30.1

Average Stack Velocity -Vs (ft/sec) 46.5 46.6 47.2 46.8

Area of Stack (ft2) 12.6 12.6 12.6 12.6

Exhaust Gas Flowrate

Flowrate ft

3

(Actual) 35,058 35,152 35,595 35,269

Flowrate ft

3 (Standard Wet) 32,606 32,573 32,698 32,626

Flowrate ft

3 (Standard Dry) 32,074 31,867 31,860 31,934

Flowrate m3 (standard dry) 908 902 902 904

Total Particulate Weights (mg)

Acetone Rinse 3.6 1.8 2.5 2.6

Filter < 0.3 < 0.3 < 0.3 0.3

Total < 3.9 < 2.1 < 2.8 2.9

Total Particulate Concentration

 lb/1000 lb (wet) < 5.1E-04 < 2.8E-04 < 3.6E-04 3.8E-04

 lb/1000 lb (dry) < 5.1E-04 < 2.8E-04 < 3.7E-04 3.9E-04

mg/dscm (dry) < 6.1E-01 < 3.4E-01 < 4.4E-01 4.6E-01

gr/dscf < 2.7E-04 < 1.5E-04 < 1.9E-04 2.0E-04

Total Particulate Emission Rate

 lb/ hr < 7.37E-02 < 4.0E-02 < 5.2E-02 5.5E-02

 lb/ ton product

Filterable Chromium Weights (ug)

Front Half Chromium (Filterable) 3.26 1.22 0.52 1.67

Filterable Chromium Concentrations

 lb/1000 lb (wet) 4.2E-07 1.6E-07 6.7E-08 2.2E-07

 lb/1000 lb (dry) 4.3E-07 1.6E-07 6.8E-08 2.2E-07

mg/dscm (dry) 5.1E-04 2.0E-04 8.1E-05 2.6E-04

gr/dscf 2.2E-07 8.5E-08 3.6E-08 1.1E-07

Filterable Chromium Emission Rate

 lb/ hr 6.16E-05 2.3E-05 9.7E-06 3.2E-05

 lb/ ton product

Vaporous Chromium Weights (ug)

Back Half Chromium (Vaporous) < 0.15 0.15 0.15 0.15

Vaporous Chromium Concentrations

 lb/1000 lb (wet) < 1.9E-08 2.0E-08 1.9E-08 2.0E-08

 lb/1000 lb (dry) < 2.0E-08 2.0E-08 2.0E-08 2.0E-08

mg/dscm (dry) < 2.3E-05 2.4E-05 2.3E-05 2.4E-05

gr/dscf < 1.0E-08 1.0E-08 1.0E-08 1.0E-08

Vaporous Chromium Emission Rate

 lb/ hr < 2.8E-06 2.9E-06 2.8E-06 2.8E-06

 lb/ ton product

Total Chromium Weights (ug)

Total Chromium < 3.41 1.37 0.67 1.82

Total Chromium Concentrations

 lb/1000 lb (wet) < 4.4E-07 1.8E-07 8.6E-08 2.4E-07

 lb/1000 lb (dry) < 4.5E-07 1.8E-07 8.8E-08 2.4E-07

mg/dscm (dry) < 5.3E-04 2.2E-04 1.0E-04 2.9E-04

gr/dscf < 2.3E-07 9.6E-08 4.6E-08 1.2E-07

Total Chromium Emission Rate

 lb/ hr < 6.44E-05 2.6E-05 1.3E-05 3.4E-05

 lb/ ton product
Table 4

Line 105 Method 0061 Emission Rate Results Summary

Company JM Winder

Source Designation 105

Test Date 1/25/2012 1/26/2012 1/26/2012

Meter/Nozzle Information P-1 P-2 P-3 Average

Meter Temperature Tm (F) 71.5 74.3 77.2 74.3

Meter Pressure - Pm (in. Hg) 30.5 30.3 30.3 30.3

Measured Sample Volume (Vm) 223.9 225.0 196.6 215.2

Sample Volume (Vm-Std ft3) 227.0 225.5 195.8 216.1

Sample Volume (Vm-Std m3) 6.43 6.39 5.55 6.12

Condensate Volume (Vw-std) 5.375 5.427 5.686 5.496

Gas Density (Ps(std) lbs/ft3) (wet) 0.0740 0.0740 0.0738 0.0739

Gas Density (Ps(std) lbs/ft3) (dry) 0.0746 0.0746 0.0746 0.0746

Total weight of sampled gas (m g lbs) (wet) 17.19 17.08 14.88 16.38

Total weight of sampled gas (m g lbs) (dry) 16.94 16.83 14.61 16.13

Nozzle Size - An (sq. ft.) 0.000369 0.000369 0.000369 0.000369

Isokinetic Variation - I 100.5 100.4 100.6 100.5

Production Data

Production Data (lb/hr)

Stack Data

Average Stack Temperature - Ts (F) 116.0 114.1 110.4 113.5

Oxygen Concentration (%) 20.6 20.6 20.6

Molecular Weight Stack Gas- dry (Md) 28.9 28.9 28.9 28.9

Molecular Weight Stack Gas-wet (Ms) 28.6 28.6 28.6 28.6

Stack Gas Specific Gravity (Gs) 0.988 0.988 0.986 0.988

Percent Moisture (Bws) 2.31 2.35 2.82 2.49

Water Vapor Volume (fraction) 0.0231 0.0235 0.0282 0.0249

Pressure - Ps ("Hg) 30.3 30.1 30.1 30.1

Average Stack Velocity -Vs (ft/sec) 47.0 46.9 40.6 44.8

Area of Stack (ft2) 12.6 12.6 12.6 12.6

Exhaust Gas Flowrate

Flowrate ft3

(Actual) 35,416 35,323 30,569 33,769

Flowrate ft3 (Standard Wet) 32,827 32,654 28,439 31,307

Flowrate ft3

 (Standard Dry) 32,067 31,886 27,637 30,530

Flowrate m3 (standard dry) 908 903 783 865

Total Hexavalent Chromium Weight (ug)

Hexavalent Chromium < 0.30 < 0.30 < 0.30 0.30

Total Hexavalent Chromium Concentration

 lb/1000 lb (wet) < 3.8E-08 < 3.9E-08 < 4.4E-08 4.1E-08

 lb/1000 lb (dry) < 3.9E-08 < 3.9E-08 < 4.5E-08 4.1E-08

mg/dscm (dry) < 4.7E-05 < 4.7E-05 < 5.4E-05 4.9E-05

Total Hexavalent Chromium Emission Rate

 lb/ hr < 5.6E-06 < 5.6E-06 < 5.6E-06 5.6E-06

 lb/ ton product

Total Chromium Weight (ug)

Back Half Chromium < 4.00 < 4.00 < 4.00 4.00

Front Half Chromium 0.30 < 0.30 < 0.30 0.30

Rinse Chromium < 1.00 < 1.00 < 1.00

Total Chromium < 5.30 < 5.30 < 5.30 5.30

Total Chromium Concentration

 lb/1000 lb (wet) < 6.8E-07 < 6.8E-07 < 7.9E-07 7.2E-07

 lb/1000 lb (dry) < 6.9E-07 < 6.9E-07 < 8.0E-07 7.3E-07

mg/dscm (dry) < 8.2E-04 < 8.3E-04 < 9.6E-04 8.7E-04

Total Chromium Emission Rate

 lb/ hr < 9.9E-05 < 9.9E-05 < 9.9E-05 9.9E-05

 lb/ ton product
Table 6

Line 106 Method 0061 Emission Rate Results Summary

Company JM Winder

Source Designation 106

Test Date 1/23/2012 1/24/2012 1/24/2012

Meter/Nozzle Information P-1 P-2 P-3 Average

Meter Temperature Tm (F) 59.2 76.6 83.8 73.2

Meter Pressure - Pm (in. Hg) 30.0 30.3 30.3 30.2

Measured Sample Volume (Vm) 170.2 173.6 173.6 172.5

Sample Volume (Vm-Std ft3) 174.0 173.2 171.0 172.7

Sample Volume (Vm-Std m3) 4.93 4.90 4.84 4.89

Condensate Volume (Vw-std) 3.711 3.711 0.000 2.474

Gas Density (Ps(std) lbs/ft3) (wet) 0.0739 0.0739 0.0745 0.0741

Gas Density (Ps(std) lbs/ft3) (dry) 0.0745 0.0745 0.0745 0.0745

Total weight of sampled gas (m g lbs) (wet) 13.14 13.07 12.74 12.98

Total weight of sampled gas (m g lbs) (dry) 12.96 12.90 12.74 12.87

Nozzle Size - An (sq. ft.) 0.000369 0.000369 0.000369 0.000369

Isokinetic Variation - I 100.0 100.1 98.4 99.5

Production Data

Production Data (lb/hr)

Stack Data

Average Stack Temperature - Ts (F) 121.4 124.7 132.4 126.2

Oxygen Concentration (%) 20.6 20.6 20.6

Molecular Weight Stack Gas- dry (Md) 28.8 28.8 28.8 28.8

Molecular Weight Stack Gas-wet (Ms) 28.6 28.6 28.8 28.7

Stack Gas Specific Gravity (Gs) 0.988 0.988 0.995 0.990

Percent Moisture (Bws) 2.09 2.10 0.00 1.40

Water Vapor Volume (fraction) 0.0209 0.0210 0.0000 0.0140

Pressure - Ps ("Hg) 29.9 30.2 30.2 30.1

Average Stack Velocity -Vs (ft/sec) 36.8 36.5 36.4 36.6

Area of Stack (ft2) 15.9 15.9 15.9 15.9

Exhaust Gas Flowrate

Flowrate ft3

(Actual) 35,114 34,841 34,685 34,880

Flowrate ft3 (Standard Wet) 31,913 31,749 31,197 31,620

Flowrate ft3 (Standard Dry) 31,247 31,083 31,197 31,175

Flowrate m3 (standard dry) 885 880 883 883

Total Hexavalent Chromium Weight (ug)

Hexavalent Chromium 0.36 < 0.40 < 0.30 0.35

Total Hexavalent Chromium Concentration

 lb/1000 lb (wet) 6.0E-08 < 6.7E-08 < 5.2E-08 6.0E-08

 lb/1000 lb (dry) 6.1E-08 < 6.8E-08 < 5.2E-08 6.0E-08

mg/dscm (dry) 7.3E-05 < 8.2E-05 < 6.2E-05 7.2E-05

Total Hexavalent Chromium Emission Rate

 lb/ hr 8.6E-06 < 9.5E-06 < 7.3E-06 8.5E-06

 lb/ ton product

Total Chromium Weight (ug)

Back Half Chromium < 4.00 < 5.00 < 4.00 4.33

Front Half Chromium < 0.30 < 0.30 0.90 0.50

Rinse Chromium < 2.00 < 2.00 < 2.00

Total Chromium < 6.30 < 7.30 < 6.90 6.83

Total Chromium Concentration

 lb/1000 lb (wet) < 1.1E-06 < 1.2E-06 < 1.2E-06 1.2E-06

 lb/1000 lb (dry) < 1.1E-06 < 1.2E-06 < 1.2E-06 1.2E-06

mg/dscm (dry) < 1.3E-03 < 1.5E-03 < 1.4E-03 1.4E-03

Total Chromium Emission Rate

 lb/ hr < 1.5E-04 < 1.7E-04 < 1.7E-04 1.6E-04

 lb/ ton product
Table 7

Line 106 Method 5/29 Emission Rate Results Summary

Company JM Winder

Source Designation 106

Test Date 1/23/2012 1/24/2012 1/24/2012

Meter/Nozzle Information P-1 P-2 P-3 Average

Meter Temperature Tm (F) 64.5 84.7 96.6 82.0

Meter Pressure - Pm (in. Hg) 30.1 30.3 30.3 30.2

Measured Sample Volume (Vm) 174.9 173.7 177.4 175.4

Sample Volume (Vm-Std ft3) 176.8 170.1 170.1 172.3

Sample Volume (Vm-Std m3) 5.01 4.82 4.82 4.88

Condensate Volume (Vw-std) 3.145 3.112 2.150 2.802

Gas Density (Ps(std) lbs/ft3) (wet) 0.0740 0.0740 0.0742 0.0741

Gas Density (Ps(std) lbs/ft3) (dry) 0.0745 0.0745 0.0745 0.0745

Total weight of sampled gas (m g lbs) (wet) 13.32 12.82 12.77 12.97

Total weight of sampled gas (m g lbs) (dry) 13.17 12.68 12.67 12.84

Nozzle Size - An (sq. ft.) 0.000369 0.000369 0.000369 0.000369

Isokinetic Variation - I 101.2 99.9 99.4 100.2

Production Data

Production Data (lb/hr)

Stack Data

Average Stack Temperature - Ts (F) 120.0 123.0 131.8 124.9

Molecular Weight Stack Gas- dry (Md) 28.8 28.8 28.8 28.8

Molecular Weight Stack Gas-wet (Ms) 28.6 28.6 28.7 28.7

Stack Gas Specific Gravity (Gs) 0.989 0.989 0.991 0.989

Percent Moisture (Bws) 1.75 1.80 1.25 1.60

Water Vapor Volume (fraction) 0.0175 0.0180 0.0125 0.0160

Pressure - Ps ("Hg) 30.0 30.2 30.2 30.1

Average Stack Velocity -Vs (ft/sec) 36.7 35.8 36.2 36.2

Area of Stack (ft2) 15.9 15.9 15.9 15.9

Exhaust Gas Flowrate

Flowrate ft

3

(Actual) 34,991 34,099 34,562 34,550

Flowrate ft

3 (Standard Wet) 31,944 31,163 31,116 31,408

Flowrate ft

3 (Standard Dry) 31,386 30,604 30,728 30,906

Flowrate m3 (standard dry) 889 867 870 875

Total Particulate Weights (mg)

Acetone Rinse 3.4 2.7 6.0 4.0

Filter < 0.3 < 0.3 < 0.3 0.3

Total < 3.7 < 3.0 < 6.3 4.3

Total Particulate Concentration

 lb/1000 lb (wet) < 6.1E-04 < 5.2E-04 < 1.1E-03 7.4E-04

 lb/1000 lb (dry) < 6.2E-04 < 5.2E-04 < 1.1E-03 7.5E-04

mg/dscm (dry) < 7.4E-01 < 6.2E-01 < 1.3E+00 8.9E-01

gr/dscf < 3.2E-04 < 2.7E-04 < 5.7E-04 3.9E-04

Total Particulate Emission Rate

 lb/ hr < 8.7E-02 < 7.2E-02 < 1.5E-01 1.0E-01

 lb/ ton product

Filterable Chromium Weights (ug)

Front Half Chromium (Filterable) 1.78 6.11 2.67 3.52

Filterable Chromium Concentrations

 lb/1000 lb (wet) 2.9E-07 1.1E-06 4.6E-07 6.0E-07

 lb/1000 lb (dry) 3.0E-07 1.1E-06 4.6E-07 6.1E-07

mg/dscm (dry) 3.6E-04 1.3E-03 5.5E-04 7.3E-04

gr/dscf 1.6E-07 5.5E-07 2.4E-07 3.2E-07

Filterable Chromium Emission Rate

 lb/ hr 4.2E-05 1.5E-04 6.4E-05 8.4E-05

 lb/ ton product

Vaporous Chromium Weights (ug)

Back Half Chromium (Vaporous) < 0.15 < 0.15 < 0.15 0.15

Vaporous Chromium Concentrations

 lb/1000 lb (wet) < 2.5E-08 < 2.6E-08 < 2.6E-08 2.6E-08

 lb/1000 lb (dry) < 2.5E-08 < 2.6E-08 < 2.6E-08 2.6E-08

mg/dscm (dry) < 3.0E-05 < 3.1E-05 < 3.1E-05 3.1E-05

gr/dscf < 1.3E-08 < 1.4E-08 < 1.4E-08 1.3E-08

Vaporous Chromium Emission Rate

 lb/ hr < 3.5E-06 < 3.6E-06 < 3.6E-06 3.6E-06

 lb/ ton product

Total Chromium Weights (ug)

Total Chromium < 1.93 < 6.26 < 2.82 3.67

Total Chromium Concentrations

 lb/1000 lb (wet) < 3.2E-07 < 1.1E-06 < 4.9E-07 6.3E-07

 lb/1000 lb (dry) < 3.2E-07 < 1.1E-06 < 4.9E-07 6.3E-07

mg/dscm (dry) < 3.9E-04 < 1.3E-03 < 5.9E-04 7.6E-04

gr/dscf < 1.7E-07 < 5.7E-07 < 2.6E-07 3.3E-07

Total Chromium Emission Rate

 lb/ hr < 4.5E-05 < 1.5E-04 < 6.8E-05 8.8E-05

 lb/ ton product
Figures 
Diameter:

54.00 in

Points Distance "

12 1.1

11 3.6

10 6.4

9 9.6

8 13.5

7 19.2

6 34.8

5 40.5

4 44.4

3 47.6

2 50.4

1 52.9

Site:

Johns Manville

Winder, GA

Line 106 Melter

Figure 1

BT Environmental Consulting, Inc.

4949 Fernlee 

Royal Oak, Michigan 48073

Not to Scale 

 

<0.5 diameters 

 <2 diameters 
Bags Samples

to analyzers

Figure 2

Site:

USEPA Method 3A

Johns Manville

Winder, Georgia

BT Environmental Consulting, 

Inc.

4949 Fernlee 

Royal Oak, Michigan 48073

Data Acquisition System 

Calibration Gases 

(Fed to Probe Tip) 

 

Environics Gas 

Dilution System 

M&C Model 100-L 

O2 Analyzer 

CAI Series 600 

CO2 Analyzer 

pump 

tedlar 

bag 
Figure 3

Site:USEPA Methods 5/29Johns ManvilleWinder, Georgia

BT Environmental Consult4949 Fernlee Michigan 48073

Silica gel 

100 mL 5% HNO3 / 10% H2O2 solution 

Heated Filter Box 

S-Type Pitot w/ Thermocouple 

Heated Probe w/ Glass Liner & Nozzle 

Meter Rig 

Temp. 

ProbeFilter 

On 

Off -+

00:00 

1 2 3 4 5 
Figure 4

Site:USEPA Method 0061Johns ManvilleWinder, Georgia

BT Environmental Cons4949 Fernlee Royal Oak, Michigan 48

Meter Rig 

Temp. 

ProbeFilter 

On 

Off -+

00:00 

1 2 3 4 5 

150 mL 0.1 N KOH Empty Silica Gel 

Perastaltic pump 

Teflon tee 

75 mL 0.1 N KOH 
Appendix A 

Field and Computer Generated Raw Data and Field Notes 
Company JM Winder

Source Designation 105Test Date 1/25/2012 Assumed Moisture (Bws) 2

Test Number 1 Condensate Volume (Vlc) 58.3

Operator PM Silica Gel Weight Gain (Vlc) 21

Filter Number 11121405 Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.29 Leak Rate Initial .000@10"'

Stack Static Pressure (Pg) -0.52 Leak Rate Final .001@10"

Stack Dimensions 1 (in.) 48 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5ft B Meter Corr. Factor (Y) 0.998

Meter Number MB 3 Orsat Results (%)

Meter Isokinetic Factor (Kiso) CO2 0.03

Delta ∆H@ 1.77 O2 20.57

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Actual Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Expected 

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature DGM 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (cubic feet) 

1 0 9:48 0 110 0.56 2.44 2.35 184.90 54 53 52 250 251 189.13 2 5 3 110 0.56 2.44 2.35 189.14 62 54 52 248 251 193.41 3 10 3 110 0.57 2.49 2.40 193.41 64 56 53 247 248 197.73 4 15 3 110 0.57 2.49 2.41 197.75 68 58 53 252 251 202.10 5 20 3 110 0.61 2.66 2.59 202.10 70 59 57 251 251 206.61 6 25 3 110 0.61 2.66 2.60 206.61 72 61 61 250 249 211.14 7 30 4 111 0.65 2.84 2.78 211.13 73 62 62 248 249 215.81 8 35 4 111 0.65 2.84 2.78 215.82 75 63 63 248 251 220.51 9 40 4 111 0.71 3.10 3.05 220.52 76 65 65 249 251 225.44 

10 45 4 111 0.71 3.10 3.05 225.44 78 67 64 247 250 230.38 11 50 4 111 0.73 3.18 3.15 230.37 79 68 64 248 250 235.39 12 55 4 111 0.73 3.18 1.15 235.39 81 69 63 250 249 240.42 13 60 4 111 0.70 3.05 3.05 240.43 82 71 62 252 249 245.37 14 65 4 111 0.70 3.05 3.04 245.36 83 72 62 253 251 250.31 15 70 4 111 0.65 2.84 2.84 250.31 84 73 61 250 252 255.09 16 75 4 111 0.65 2.84 2.84 255.09 86 75 60 250 251 259.89 17 80 4 111 0.61 2.66 2.68 259.90 86 76 60 248 250 264.55 18 85 4 111 0.61 2.66 2.68 264.55 87 77 59 247 251 269.21 19 90 4 113 0.57 2.49 2.52 269.21 87 78 59 248 250 273.71 20 95 4 113 0.57 2.49 2.51 273.70 87 79 59 247 251 278.20 21 100 4 114 0.55 2.40 2.44 278.22 87 79 60 249 250 282.64 22 105 4 114 0.55 2.40 2.43 282.66 88 80 60 250 251 287.09 23 110 3 114 0.54 2.36 2.40 287.09 88 80 61 250 250 291.48 24 115 3 114 0.54 2.36 2.40 291.48 88 80 62 247 249 295.87 

120 11:48 295.87

1 120 11:53 3 114 0.60 2.62 2.68 295.87 83 80 60 252 250 300.47 2 125 3 115 0.60 2.62 2.68 300.47 87 81 61 249 251 305.09 3 130 3 115 0.61 2.66 2.73 305.10 88 81 61 247 250 309.76 4 135 3 116 0.61 2.66 2.73 309.77 89 81 62 250 250 314.43 5 140 4 116 0.67 2.92 3.01 314.44 89 82 62 248 251 319.33 6 145 4 116 0.67 2.92 3.00 319.33 90 82 62 250 249 324.23 7 150 4 116 0.69 3.01 3.11 324.23 90 82 63 252 250 329.20 8 155 4 116 0.69 3.01 3.11 329.21 90 83 63 250 250 334.18 9 160 4 116 0.74 3.23 3.35 334.19 90 83 63 248 249 339.34 

10 165 4 116 0.74 3.23 3.34 339.35 90 82 63 247 249 344.50 11 170 4 116 0.77 3.36 3.49 344.50 90 83 64 250 251 349.76 12 175 4 116 0.77 3.36 3.49 349.75 90 82 63 250 250 355.00 13 180 4 116 0.74 3.23 3.36 355.01 90 83 64 248 251 360.16 14 185 4 117 0.74 3.23 3.36 360.17 90 83 63 247 250 365.32 15 190 4 117 0.71 3.10 3.24 365.32 91 83 63 249 249 370.37 16 195 4 117 0.71 3.11 3.24 370.37 91 83 64 250 249 375.42 17 200 4 117 0.65 2.85 2.97 375.44 90 83 63 250 250 380.26 18 205 4 118 0.65 2.85 2.97 380.26 89 83 64 247 251 385.08 19 210 4 118 0.57 2.50 2.61 385.08 89 82 63 246 251 389.59 20 215 4 118 0.57 2.51 2.61 389.58 89 83 64 247 251 394.09 21 220 4 118 0.55 2.42 2.53 394.10 89 82 64 250 250 398.53 22 225 4 118 0.55 2.42 2.53 398.53 89 83 64 253 250 402.96 23 230 4 118 0.51 2.25 2.35 402.96 89 83 65 250 251 407.23 24 235 4 118 0.51 2.25 2.35 407.26 89 83 64 250 250 411.53 

240 13:53 411.53

Average 240 114.0 0.64 2.78 2.78 226.630 83.9 75.6 61.4 249.1 250.2 299.7 

79.76
Company JM Winder

Source Designation 105Test Date 1/26/2012 Assumed Moisture (Bws) 2

Test Number 2 Condensate Volume (Vlc) 53

Operator PM Silica Gel Weight Gain (Vlc) 50.6

Filter Number 11121407 Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.11 Leak Rate Initial .001@10"

Stack Static Pressure (Ps) -0.52 Leak Rate Final .000@8"

Stack Dimensions 1 (in.) 48 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5ft B Meter Corr. Factor (Y) 0.998

Meter Number MB 3 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0.03Delta ∆H@ 1.77 O2 20.57

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Expected 

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature DGM 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (cubic feet) 

1 0 7:56 0 110 0.54 2.35 2.26 411.40 53 53 51 250 251 415.56 2 5 5 110 0.54 2.35 2.26 415.56 60 56 50 250 249 419.77 3 10 5 110 0.55 2.40 2.32 419.77 63 57 51 247 249 424.03 4 15 5 111 0.55 2.40 2.32 424.03 67 58 51 247 251 428.31 5 20 5 111 0.64 2.80 2.72 428.30 69 60 52 249 250 432.93 6 25 6 113 0.64 2.80 2.72 432.93 71 61 53 247 250 437.57 7 30 6 113 0.68 2.98 2.91 437.57 73 62 53 250 251 442.36 8 35 6 113 0.68 2.98 2.91 442.35 74 64 53 249 250 447.16 9 40 6 113 0.70 3.07 3.01 447.16 75 64 55 248 251 452.04 

10 45 6 113 0.70 3.08 3.01 452.03 76 66 56 249 251 456.93 11 50 6 113 0.73 3.21 3.15 456.93 77 67 57 249 250 461.94 12 55 6 113 0.73 3.22 3.15 461.93 78 68 58 251 250 466.95 13 60 6 113 0.71 3.13 3.08 466.94 79 69 58 253 250 471.90 14 65 6 113 0.71 3.13 3.08 471.92 80 70 60 252 251 476.89 15 70 6 112 0.69 3.05 3.01 476.88 80 71 59 251 250 481.79 16 75 6 112 0.69 3.05 3.00 481.79 81 71 59 251 250 486.70 17 80 6 112 0.66 2.92 2.89 486.69 81 72 60 249 252 491.50 18 85 6 113 0.66 2.93 2.88 491.50 82 73 61 252 249 496.31 19 90 6 113 0.65 2.89 2.86 496.31 82 73 60 251 250 501.09 20 95 6 113 0.65 2.89 2.85 501.08 83 74 61 251 250 505.86 21 100 6 113 0.56 2.49 2.46 505.85 83 74 60 251 251 510.29 22 105 5 113 0.56 2.50 2.46 510.31 83 75 60 249 250 514.75 23 110 5 113 0.55 2.45 2.43 514.77 83 75 61 249 249 519.17 24 115 5 113 0.55 2.46 2.43 519.18 83 75 61 251 251 523.58 

120 9:56 523.58

1 120 10:01 0 112 0.53 2.37 2.36 523.58 78 76 58 252 250 527.89 2 125 5 112 0.53 2.38 2.35 527.91 80 75 60 247 249 532.23 3 130 5 113 0.55 2.47 2.45 532.24 82 76 60 249 251 536.64 4 135 5 113 0.55 2.47 2.45 536.66 83 76 57 249 250 541.07 5 140 5 113 0.60 2.70 2.68 541.07 83 76 57 249 250 545.67 6 145 5 113 0.60 2.70 2.68 545.70 84 76 57 250 250 550.31 7 150 5 113 0.64 2.88 2.87 550.32 84 77 56 251 249 555.08 8 155 6 113 0.64 2.89 2.87 555.10 85 77 58 249 250 559.87 9 160 6 113 0.71 3.21 3.20 559.87 86 78 59 251 250 564.90 

10 165 6 113 0.71 3.21 3.20 564.91 86 78 58 250 251 569.94 11 170 6 113 0.75 3.40 3.38 569.94 86 78 59 248 248 575.11 12 175 6 113 0.75 3.40 3.39 575.13 87 79 58 248 249 580.31 13 180 6 114 0.77 3.49 3.49 580.32 87 79 58 248 251 585.57 14 185 6 114 0.77 3.50 3.48 585.56 88 80 60 249 250 590.82 15 190 6 114 0.73 3.32 3.32 590.82 88 80 60 249 249 595.94 16 195 6 114 0.73 3.32 3.32 595.96 88 80 59 249 250 601.08 17 200 6 113 0.65 2.96 2.95 601.08 88 80 60 251 251 605.91 18 205 6 113 0.65 2.97 2.96 605.94 89 81 60 252 250 610.78 19 210 6 113 0.61 2.79 2.79 610.79 89 81 60 250 249 615.48 20 215 6 113 0.61 2.79 2.78 615.48 89 81 61 249 251 620.17 21 220 6 113 0.55 2.52 2.52 620.17 89 81 60 251 250 624.62 22 225 6 113 0.55 2.52 2.52 624.63 89 82 61 251 250 629.09 23 230 5 113 0.51 2.34 2.34 629.09 89 82 61 249 251 633.38 24 235 5 113 0.51 2.34 2.34 633.38 89 82 61 251 250 637.67 

240 12:09 260.840

Average 240 112.7 0.64 2.84 2.81 221.980 81 73 58 250 250 526 

76.89
Company JM Winder

Source Designation 105Test Date 1/26/2012 Assumed Moisture (Bws) 2

Test Number 3 Condensate Volume (Vlc) 78.6

Operator PM Silica Gel Weight Gain (Vlc) 47.5

Filter Number 11081871 Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.11 Leak Rate Initial .000@10"

Stack Static Pressure (Ps) -0.52 Leak Rate Final .000@10"

Stack Dimensions 1 (in.) 48 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5ft B Meter Corr. Factor (Y) 0.998

Meter Number MB 3 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0.3Delta ∆H@ 1.77 O2 20.57

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Expected 

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature DGM 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (cubic feet) 

1 0 12:47 0 109 0.54 2.37 2.37 638.09 77 77 54 249 252 642.45 2 5 3 109 0.54 2.37 2.37 642.48 79 78 57 252 252 646.85 3 10 3 110 0.55 2.42 2.42 646.86 81 78 56 251 253 651.28 4 15 3 110 0.55 2.42 2.42 651.28 83 78 52 252 250 655.70 5 20 3 111 0.58 2.55 2.56 655.70 87 78 53 249 250 660.26 6 25 3 113 0.58 2.55 2.56 660.26 85 78 53 249 251 664.80 7 30 3 114 0.61 2.68 2.70 664.83 86 79 53 252 251 669.49 8 35 3 115 0.61 2.68 2.70 669.49 87 79 54 253 250 674.15 9 40 3 116 0.68 2.99 3.02 674.17 87 79 54 251 250 679.09 

10 45 3 116 0.68 2.99 3.01 679.09 87 80 54 251 250 684.01 11 50 3 117 0.72 3.17 3.20 684.00 88 80 54 251 250 689.06 12 55 4 117 0.72 3.17 3.20 689.07 89 81 55 251 250 694.14 13 60 4 117 0.75 3.30 3.34 694.15 89 81 55 248 251 699.33 14 65 4 117 0.75 3.30 3.33 699.32 90 82 56 248 250 704.51 15 70 4 117 0.70 3.08 3.12 704.50 90 82 57 250 250 709.51 16 75 4 117 0.70 3.08 3.12 709.54 90 82 57 250 250 714.55 17 80 4 117 0.68 2.99 3.04 714.56 91 83 58 249 250 719.51 18 85 4 118 0.68 2.99 3.04 719.53 91 83 58 251 250 724.47 19 90 4 118 0.65 2.86 2.92 724.47 92 84 58 251 249 729.31 20 95 3 119 0.65 2.86 2.92 729.32 92 84 58 249 250 734.16 21 100 3 118 0.61 2.68 2.74 734.18 93 85 58 249 251 738.88 22 105 3 118 0.61 2.68 2.74 738.88 94 86 58 250 250 743.59 23 110 3 118 0.57 2.51 2.57 743.59 94 86 59 251 251 748.14 24 115 3 118 0.57 2.51 2.57 748.16 94 86 59 250 250 752.71 

120 14:47 752.70

1 120 14:52 0 120 0.60 2.64 2.73 752.70 89 87 62 252 251 757.34 2 125 3 120 0.60 2.64 2.73 757.37 92 87 60 251 250 762.03 3 130 3 120 0.61 2.68 2.77 762.01 93 87 60 249 250 766.71 4 135 3 120 0.61 2.68 2.76 766.71 93 87 60 248 250 771.41 5 140 4 120 0.68 2.99 3.09 771.42 93 87 59 251 250 776.38 6 145 4 120 0.68 2.99 3.09 776.39 93 87 61 249 250 781.35 7 150 4 119 0.69 3.03 3.15 781.36 93 87 61 250 250 786.36 8 155 4 119 0.69 3.03 3.15 786.37 93 87 61 250 249 791.37 9 160 4 119 0.73 3.21 3.34 791.37 93 87 62 251 250 796.52 

10 165 4 119 0.73 3.21 3.33 796.52 93 87 62 250 249 801.67 11 170 4 120 0.76 3.34 3.47 801.68 94 87 61 249 250 806.93 12 175 4 120 0.76 3.34 3.48 806.93 94 87 63 250 251 812.18 13 180 4 120 0.74 3.25 3.40 812.19 94 87 63 251 251 817.37 14 185 4 120 0.74 3.26 3.39 817.38 95 87 64 251 249 822.57 15 190 4 120 0.71 3.13 3.27 822.57 95 88 63 249 250 827.65 16 195 4 120 0.71 3.13 3.27 827.66 95 88 63 251 249 832.74 17 200 4 121 0.65 2.87 3.00 832.74 96 88 63 251 250 837.61 18 205 4 121 0.65 2.87 2.99 837.61 96 88 62 249 250 842.48 19 210 4 121 0.61 2.70 2.81 842.46 96 88 62 249 250 847.17 20 215 3 121 0.61 2.70 2.81 847.20 95 88 62 251 252 851.91 21 220 3 120 0.56 2.49 2.59 851.91 94 88 61 251 251 856.42 22 225 3 120 0.56 2.49 2.59 856.42 94 88 61 250 250 860.93 23 230 3 120 0.52 2.31 2.41 860.95 94 88 61 249 249 865.30 24 235 3 120 0.52 2.32 2.41 865.29 93 88 61 250 250 869.63 

240 16:52 869.64

Average 240 117.7 0.65 2.84 2.92 231.550 91.0 84.3 58.7 250.2 250.3 755.7 

87.64

Company JM Winder

Source Designation 105Test Date 1/25/2012 Assumed Moisture (Bws) 2

Test Number 1 Condensate Volume (Vlc) 53.1

Operator JP Silica Gel Weight Gain (Vlc) 60.9

Filter Number Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.29 Leak Rate Initial 0.000 @ 10"

Stack Static Pressure (Pg) -0.52 Leak Rate Final 0.000 @ 6"

Stack Dimensions 1 (in.) 48 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5 ft C Meter Corr. Factor (Y) 1.002

Meter Number MB 5 Orsat Results (%)

Meter Isokinetic Factor (Kiso) CO2 0.3

Delta ∆H@ 1.55 O2 20.57

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Actual Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Filter Box Exit E

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature Temperature 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (F) (cu

1 0 9:48 3.5 111 0.62 2.33 2.25 253.37 51 50 56 NA NA NA 2 5 3.5 112 0.62 2.33 2.26 257.75 55 51 52 NA NA NA 3 10 3.5 112 0.63 2.37 2.31 262.15 58 51 52 NA NA NA 4 15 3.5 112 0.63 2.37 2.31 266.65 61 52 53 NA NA NA 5 20 4 113 0.67 2.52 2.47 271.13 63 53 55 NA NA NA 6 25 4 113 0.67 2.53 2.47 275.76 65 54 58 NA NA NA 7 30 4 113 0.68 2.57 2.52 280.43 68 55 60 NA NA NA 8 35 4 113 0.68 2.57 2.52 285.17 70 57 61 NA NA NA 9 40 4 113 0.72 2.72 2.68 289.87 72 58 63 NA NA NA 

10 45 4 113 0.72 2.73 2.69 294.76 73 59 63 NA NA NA 11 50 4 114 0.76 2.88 2.84 299.69 75 61 63 NA NA NA 12 55 4 114 0.76 2.88 2.85 304.75 76 62 63 NA NA NA 13 60 4 114 0.72 2.74 2.71 309.79 77 63 63 NA NA NA 14 65 4 115 0.72 2.74 2.71 314.71 79 65 63 NA NA NA 15 70 4 115 0.68 2.59 2.57 319.66 80 66 63 NA NA NA 16 75 4 115 0.68 2.59 2.57 324.48 80 67 61 NA NA NA 17 80 4 115 0.61 2.33 2.31 329.28 81 69 61 NA NA NA 18 85 4 116 0.61 2.33 2.32 333.88 81 69 60 NA NA NA 19 90 3.5 116 0.58 2.22 2.21 338.42 81 71 59 NA NA NA 20 95 3.5 116 0.58 2.22 2.21 342.90 81 71 59 NA NA NA 21 100 3.5 116 0.56 2.15 2.14 347.37 80 72 58 NA NA NA 22 105 3.5 116 0.56 2.15 2.15 351.79 79 71 58 NA NA NA 23 110 3.5 116 0.54 2.08 2.07 356.19 78 71 57 NA NA NA 24 115 3.5 116 0.54 2.08 2.08 360.47 77 71 57 NA NA NA 

120 11:48 364.75

1 120 11:53 3.5 116 0.56 2.16 2.16 364.75 73 70 55 NA NA NA 2 125 3.5 116 0.56 2.16 2.16 369.14 79 70 57 NA NA NA 3 130 3.5 116 0.59 2.28 2.28 373.50 80 71 56 NA NA NA 4 135 3.5 117 0.59 2.28 2.29 377.98 80 71 57 NA NA NA 5 140 3.5 117 0.63 2.44 2.44 382.49 81 72 58 NA NA NA 6 145 3.5 117 0.63 2.44 2.45 387.11 81 72 57 NA NA NA 7 150 4 117 0.67 2.60 2.61 391.76 81 72 58 NA NA NA 8 155 4 117 0.67 2.61 2.61 396.60 81 73 58 NA NA NA 9 160 4 118 0.71 2.76 2.77 401.43 80 73 58 NA NA NA 

10 165 4 118 0.71 2.77 2.77 406.33 80 73 58 NA NA NA 11 170 4 118 0.74 2.89 2.90 411.29 80 72 58 NA NA NA 12 175 4 118 0.74 2.89 2.90 416.33 81 73 58 NA NA NA 13 180 4 118 0.72 2.82 2.83 421.38 81 73 59 NA NA NA 14 185 4 118 0.72 2.82 2.83 426.32 81 73 59 NA NA NA 15 190 4 118 0.68 2.67 2.68 431.28 80 73 58 NA NA NA 16 195 4 118 0.68 2.67 2.68 436.14 79 72 58 NA NA NA 17 200 4 118 0.67 2.63 2.64 440.94 79 73 58 NA NA NA 18 205 4 118 0.67 2.64 2.65 445.74 78 72 58 NA NA NA 19 210 4 119 0.64 2.52 2.53 450.55 79 72 58 NA NA NA 20 215 4 119 0.64 2.52 2.53 455.25 79 72 59 NA NA NA 21 220 3.5 119 0.57 2.25 2.26 459.92 78 72 59 NA NA NA 22 225 3.5 119 0.57 2.25 2.26 464.34 78 71 59 NA NA NA 23 230 3.5 119 0.54 2.14 2.14 468.75 79 72 59 NA NA NA 24 235 3.5 119 0.54 2.14 2.15 473.04 79 72 59 NA NA NA 

240 13:53 477.31

Average 240 116.0 0.65 2.49 2.47 223.945 76.0 67.0 58.5 #DIV/0! #DIV/0! #DIV/0! 

71.52
Company JM Winder

Source Designation Line 105Test Date 1/26/2012 Assumed Moisture (Bws) 2

Test Number 2 Condensate Volume (Vlc) 65.5

Operator JP Silica Gel Weight Gain (Vlc) 49.6

Filter Number Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.11 Leak Rate Initial .000 @ 11"

Stack Static Pressure (Ps) -0.52 Leak Rate Final .000 @ 8"

Stack Dimensions 1 (in.) 48 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5 ft C Meter Corr. Factor (Y) 1.002

Meter Number 5 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0.3Delta ∆H@ 1.55 O2 20.57

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Filter Box Exit Expec

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature Temperature DG

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (F) (cubic 

1 0 7:56 5.5 109 0.60 2.27 2.20 477.95 52 52 48 NA NA NA 482.2 5 5.5 112 0.61 2.31 2.23 482.30 59 55 47 NA NA NA 486.3 10 5.5 113 0.63 2.39 2.32 486.71 64 56 51 NA NA NA 491.4 15 5.5 113 0.63 2.39 2.33 491.22 67 57 51 NA NA NA 495.5 20 5.5 114 0.66 2.51 2.45 495.79 69 58 51 NA NA NA 500.6 25 5.5 114 0.66 2.51 2.46 500.49 71 59 51 NA NA NA 505.7 30 6 114 0.68 2.59 2.53 505.15 72 60 50 NA NA NA 509.8 35 6 114 0.68 2.59 2.54 509.90 73 61 51 NA NA NA 514.9 40 6 114 0.70 2.67 2.62 514.66 74 61 50 NA NA NA 519.

10 45 6 115 0.70 2.68 2.63 519.52 74 62 50 NA NA NA 524.11 50 6.5 115 0.74 2.83 2.78 524.33 75 63 50 NA NA NA 529.12 55 6.5 115 0.74 2.84 2.79 529.33 76 64 50 NA NA NA 534.13 60 6 115 0.72 2.76 2.72 534.33 77 65 51 NA NA NA 539.14 65 6 115 0.72 2.77 2.72 539.25 78 66 51 NA NA NA 544.15 70 6 114 0.65 2.50 2.46 544.17 78 66 51 NA NA NA 548.16 75 6 114 0.65 2.50 2.47 548.90 79 67 51 NA NA NA 553.17 80 5.5 114 0.61 2.35 2.32 553.60 79 68 51 NA NA NA 558.18 85 5.5 114 0.61 2.35 2.33 558.17 79 68 51 NA NA NA 562.19 90 5.5 114 0.58 2.24 2.22 562.75 79 68 51 NA NA NA 567.20 95 5.5 114 0.58 2.24 2.22 567.24 79 69 51 NA NA NA 571.21 100 5 115 0.55 2.13 2.11 571.68 80 69 51 NA NA NA 576.22 105 5 114 0.55 2.13 2.11 576.05 80 70 51 NA NA NA 580.23 110 5 114 0.52 2.02 2.00 580.40 80 70 52 NA NA NA 584.24 115 5 114 0.52 2.02 2.00 584.65 81 70 51 NA NA NA 588.

120 9:56 588.90

1 120 10:01 5 114 0.55 2.14 2.13 588.90 74 71 51 NA NA NA 593.2 125 5 114 0.55 2.15 2.13 593.26 80 71 51 NA NA NA 597.3 130 5 114 0.58 2.26 2.25 597.61 81 72 50 NA NA NA 602.4 135 5 114 0.58 2.27 2.25 602.07 83 72 50 NA NA NA 606.5 140 5.5 114 0.64 2.50 2.49 606.60 84 73 50 NA NA NA 611.6 145 5.5 114 0.64 2.51 2.49 611.34 84 73 51 NA NA NA 616.7 150 6 114 0.66 2.59 2.58 616.08 85 74 51 NA NA NA 620.8 155 6 114 0.66 2.59 2.58 620.92 85 74 51 NA NA NA 625.9 160 6 115 0.70 2.75 2.74 625.75 85 75 51 NA NA NA 630.

10 165 6 115 0.70 2.76 2.75 630.72 85 75 52 NA NA NA 635.11 170 6.5 115 0.74 2.92 2.91 635.70 85 75 52 NA NA NA 640.12 175 6.5 115 0.74 2.92 2.91 640.79 85 75 52 NA NA NA 645.13 180 6 115 0.71 2.80 2.80 645.85 85 75 53 NA NA NA 650.14 185 6 115 0.71 2.81 2.80 650.86 86 76 53 NA NA NA 655.15 190 6 114 0.68 2.69 2.69 655.85 86 76 54 NA NA NA 660.16 195 6 114 0.68 2.69 2.69 660.77 86 76 55 NA NA NA 665.17 200 6 114 0.68 2.70 2.70 665.65 86 76 55 NA NA NA 670.18 205 6 114 0.68 2.70 2.70 670.58 87 77 55 NA NA NA 675.19 210 6 114 0.65 2.58 2.59 675.46 87 77 56 NA NA NA 680.20 215 6 114 0.65 2.59 2.59 680.28 87 77 56 NA NA NA 685.21 220 5.5 114 0.57 2.27 2.27 685.08 87 78 57 NA NA NA 689.22 225 5.5 114 0.57 2.27 2.27 689.59 87 78 57 NA NA NA 694.23 230 5.5 114 0.56 2.24 2.24 694.05 87 78 57 NA NA NA 698.24 235 5.5 114 0.56 2.24 2.24 698.50 88 78 57 NA NA NA 702.

240 12:01 702.95

Average 240 114.1 0.64 2.49 2.47 225.000 79 69 52 #DIV/0! #DIV/0! #DIV/0! 

74.33
Company JM Winder

Source Designation Line 105Test Date 1/26/2012 Assumed Moisture (Bws) 2

Test Number 3 Condensate Volume (Vlc) 62

Operator JP Silica Gel Weight Gain (Vlc) 58.6

Filter Number Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.11 Leak Rate Initial .008 @ 13"

Stack Static Pressure (Ps) -0.52 Leak Rate Final .000 @ 7"

Stack Dimensions 1 (in.) 48 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5 ft C Meter Corr. Factor (Y) 1.002

Meter Number 5 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0.3Delta ∆H@ 1.55 O2 20.57

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Filter Box Exit Expec

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature Temperature DG

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (F) (cubic 

1 0 12:45 4 111 0.50 1.92 2.23 892.25 72 72 59 na na na 896.2 5 4 111 0.50 1.92 2.23 896.39 73 72 55 na na na 900.3 10 4 110 0.49 1.88 2.19 900.48 75 72 53 na na na 904.4 15 4 110 0.49 1.88 2.19 904.60 77 72 54 na na na 908.5 20 4 110 0.48 1.84 2.15 908.70 78 72 55 na na na 912.6 25 4 110 0.48 1.84 2.15 912.78 78 72 57 na na na 916.7 30 4 110 0.48 1.84 2.15 916.84 79 72 58 na na na 920.8 35 4 110 0.46 1.76 2.06 920.92 79 72 58 na na na 924.9 40 4 110 0.48 1.84 2.15 924.89 79 73 59 na na na 928.

10 45 4 110 0.48 1.84 2.15 928.96 80 73 60 na na na 933.11 50 4 110 0.50 1.92 2.25 933.02 80 73 61 na na na 937.12 55 4 110 0.50 1.92 2.25 937.19 80 73 61 na na na 941.13 60 4 111 0.54 2.07 2.43 941.34 80 74 62 na na na 945.14 65 4 111 0.54 2.07 2.43 945.64 81 74 62 na na na 949.15 70 4 111 0.52 1.99 2.34 949.96 81 74 62 na na na 954.16 75 4 111 0.53 2.03 2.38 954.21 81 74 63 na na na 958.17 80 4 110 0.54 2.07 2.43 958.51 81 74 63 na na na 962.18 85 4 110 0.54 2.07 2.43 962.86 81 74 64 na na na 967.19 90 4 110 0.54 2.07 2.43 967.21 81 74 64 na na na 971.20 95 4 110 0.54 2.07 2.43 971.58 81 74 64 na na na 975.21 100 4 110 0.49 1.88 2.21 975.94 81 74 64 na na na 980.22 105 4 110 0.49 1.88 2.21 980.06 81 74 64 na na na 984.23 110 4 109 0.47 1.80 2.12 984.15 81 75 64 na na na 988.24 115 4 110 0.47 1.80 2.12 988.24 81 75 65 na na na 992.

120 14:45 992.34 na na na

1 120 14:52 4 111 0.52 1.99 2.34 992.34 77 74 64 na na na 996.2 125 4 111 0.52 1.99 2.34 996.55 78 74 64 na na na 10003 130 4 111 0.51 1.95 2.30 1000.80 80 74 63 na na na 10054 135 4 111 0.50 1.92 2.25 1005.04 81 74 64 na na na 10095 140 4 111 0.49 1.88 2.21 1009.22 81 75 65 na na na 10136 145 4 111 0.49 1.88 2.21 1013.35 81 75 65 na na na 10177 150 4 111 0.50 1.92 2.25 1017.49 82 75 66 na na na 10218 155 4 111 0.50 1.92 2.25 1021.71 82 75 65 na na na 10259 160 4 111 0.52 1.99 2.34 1025.94 82 75 61 na na na 1030

10 165 4 111 0.52 1.99 2.34 1030.200 82 75 57 na na na 103411 170 4 111 0.54 2.07 2.43 1034.470 82 75 55 na na na 103812 175 4 111 0.54 2.07 2.43 1038.800 82 75 53 na na na 104313 180 4 111 0.47 1.80 2.12 1043.110 82 75 52 na na na 104714 185 4 111 0.47 1.80 2.12 1047.170 82 75 52 na na na 105115 190 4 111 0.45 1.73 2.03 1051.300 82 76 51 na na na 105516 195 4 110 0.45 1.73 2.04 1055.200 82 76 51 na na na 105917 200 4 110 0.42 1.62 1.9 1059.100 82 76 51 na na na 106218 205 4 110 0.42 1.62 1.9 1062.950 82 76 51 na na na 106619 210 4 110 0.4 1.54 1.82 1066.760 82 76 51 na na na 107020 215 4 110 0.35 1.35 1.59 1070.580 81 70 51 na na na 107421 220 4 110 0.37 1.43 1.68 1074.220 81 76 51 na na na 107722 225 4 110 0.37 1.43 1.69 1077.880 81 76 51 na na na 108123 230 4 110 0.38 1.47 1.73 1081.510 81 76 51 na na na 108524 235 4 110 0.38 1.47 1.74 1085.160 81 76 51 na na na 1088

240 16:52 1088.800

Average 240 110.4 0.48 1.85 2.17 196.550 80.2 74.1 58.5 #DIV/0! #DIV/0! #DIV/0! 

77.17
Company JM Winder

Source Designation 106Test Date 1/23/2012 Assumed Moisture (Bws) 2

Test Number 1 Condensate Volume (Vlc) 27.7

Operator PM Silica Gel Weight Gain (Vlc) 39

Filter Number 11121401 Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 29.98 Leak Rate Initial .001@15"

Stack Static Pressure (Pg) 0.31 Leak Rate Final .000@8"

Stack Dimensions 1 (in.) 54 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5ft B Meter Corr. Factor (Y) 0.998

Meter Number MB 3 Orsat Results (%)

Meter Isokinetic Factor (Kiso) CO2 0

Delta ∆H@ 1.77 O2 20.63

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Actual Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Expected 

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature DGM 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (cubic feet) 

1 0 16:47 0 119 0.49 2.06 2.00 657.46 47 47 43 250 250 661.37 2 5 4 120 0.49 2.06 2.00 661.46 54 50 41 250 251 665.41 3 10 4 120 0.50 2.11 2.05 665.46 59 51 39 249 249 669.47 4 15 4 120 0.50 2.11 2.06 669.49 61 52 40 249 252 673.51 5 20 4 121 0.48 2.03 1.99 673.58 63 54 43 248 251 677.53 6 25 4 120 0.48 2.03 1.99 677.59 64 54 44 250 251 681.55 7 30 4 120 0.49 2.08 2.04 681.59 64 56 47 248 250 685.60 8 35 4 120 0.49 2.08 2.04 685.65 65 56 49 249 252 689.66 9 40 4 121 0.47 2.00 1.97 689.72 66 58 53 250 250 693.66 

10 45 4 120 0.47 2.00 1.97 693.70 66 58 54 248 251 697.64 11 50 4 121 0.45 1.92 1.89 697.69 67 59 57 249 250 701.55 12 55 4 121 0.45 1.92 1.89 701.60 67 60 59 252 251 705.47 13 60 4 120 0.43 1.84 1.81 705.54 67 60 58 250 250 709.32 14 65 4 120 0.43 1.84 1.81 709.35 68 60 58 248 250 713.14 15 70 4 121 0.35 1.50 1.48 713.21 68 61 59 249 248 716.63 16 75 3 121 0.35 1.50 1.48 716.67 68 61 57 252 251 720.09 17 80 3 120 0.37 1.59 1.57 720.15 68 61 57 250 250 723.67 18 85 3 120 0.37 1.59 1.57 723.72 68 62 58 250 250 727.24 19 90 3 120 0.33 1.42 1.41 727.28 68 62 57 252 252 730.60 20 95 3 120 0.33 1.42 1.41 730.66 68 62 56 248 249 733.98 21 100 3 121 0.28 1.21 1.20 734.04 69 63 56 249 249 737.10 22 105 3 118 0.28 1.21 1.20 737.16 68 63 53 249 250 740.23 23 110 3 118 0.27 1.17 1.16 740.26 68 63 52 251 250 743.27 24 115 3 118 0.27 1.17 1.16 743.33 68 63 54 248 250 746.34 

120 18:47 746.39

1 120 18:52 0 118 0.37 1.60 1.59 746.39 65 63 49 252 251 749.91 2 125 3 118 0.37 1.61 1.59 749.98 67 63 50 248 251 753.50 3 130 3 118 0.39 1.69 1.69 753.57 68 64 51 249 251 757.20 4 135 3 118 0.39 1.70 1.69 757.25 69 64 53 250 250 760.88 5 140 3 120 0.42 1.83 1.82 760.93 69 64 53 248 250 764.69 6 145 3 120 0.42 1.83 1.82 764.73 69 64 55 249 250 768.49 7 150 3 121 0.43 1.88 1.87 768.53 70 64 56 248 241 772.33 8 155 3 121 0.43 1.88 1.87 772.38 70 64 56 250 249 776.18 9 160 3 120 0.42 1.84 1.83 776.24 70 64 57 248 249 780.00 

10 165 3 120 0.42 1.84 1.83 780.06 70 64 57 249 250 783.82 11 170 3 121 0.39 1.71 1.70 783.89 70 65 58 248 250 787.52 12 175 3 120 0.39 1.71 1.70 787.56 70 65 57 250 250 791.19 13 180 3 120 0.37 1.63 1.62 791.24 71 65 58 251 251 794.78 14 185 3 120 0.37 1.63 1.62 794.83 71 65 56 249 250 798.37 15 190 3 121 0.36 1.59 1.58 798.43 71 65 57 251 250 801.92 16 195 3 120 0.36 1.59 1.58 801.98 71 65 55 248 251 805.47 17 200 3 120 0.35 1.54 1.54 805.52 71 66 55 249 250 808.96 18 205 3 120 0.35 1.55 1.54 809.02 71 66 54 251 249 812.46 19 210 3 121 0.33 1.46 1.46 812.51 71 66 54 250 250 815.85 20 215 3 121 0.33 1.46 1.46 815.91 71 66 52 252 252 819.25 21 220 3 120 0.31 1.37 1.37 819.30 72 66 53 251 250 822.55 22 225 3 120 0.31 1.38 1.37 822.58 72 66 52 248 250 825.83 23 230 3 120 0.30 1.33 1.33 825.87 72 67 52 251 251 829.07 24 235 3 120 0.30 1.33 1.33 829.12 72 67 51 250 250 832.32 

240 20:52 832.36

Average 240 120.0 0.39 1.68 1.67 174.900 67.5 61.5 53.0 249.5 250.1 749.1 

64.54
Company JM Winder

Source Designation 106Test Date 1/24/2012 Assumed Moisture (Bws) 2

Test Number 2 Condensate Volume (Vlc) 21.9

Operator PM Silica Gel Weight Gain (Vlc) 44.1

Filter Number 11121402 Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.17 Leak Rate Initial .001 @10"

Stack Static Pressure (Ps) 0.31 Leak Rate Final .000 @7"

Stack Dimensions 1 (in.) 54 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5ft B Meter Corr. Factor (Y) 0.998

Meter Number MB 3 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0Delta ∆H@ 1.77 O2 20.63

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Expected 

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature DGM 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (cubic feet) 

1 0 9:12 0 118 0.29 1.26 1.19 833.21 49 49 49 250 251 836.23 2 5 3 118 0.29 1.26 1.19 836.24 59 55 49 250 251 839.30 3 10 3 118 0.30 1.31 1.25 839.31 62 56 47 249 248 842.44 4 15 3 118 0.30 1.31 1.24 842.44 64 57 46 250 252 845.58 5 20 3 119 0.33 1.44 1.39 845.56 67 59 46 249 250 848.86 6 25 3 119 0.33 1.45 1.38 848.87 69 60 45 250 251 852.18 7 30 3 121 0.34 1.49 1.43 852.18 71 62 47 252 251 855.55 8 35 3 122 0.34 1.49 1.43 855.56 73 63 47 249 251 858.94 9 40 3 122 0.36 1.58 1.53 858.93 74 65 50 248 250 862.41 

10 45 3 122 0.36 1.58 1.53 862.40 76 67 51 250 252 865.90 11 50 3 122 0.38 1.67 1.62 865.90 78 68 54 249 250 869.50 12 55 3 122 0.38 1.68 1.62 869.52 79 70 56 252 250 873.13 13 60 10:12 3 122 0.46 2.03 1.97 873.13 81 71 56 248 250 877.12 14 65 10:23 3 122 0.46 2.03 1.97 877.10 80 75 55 250 251 881.10 15 70 3 122 0.49 2.17 2.11 881.10 82 76 56 248 250 885.24 16 75 3 122 0.49 2.17 2.11 885.23 84 76 55 248 251 889.38 17 80 3 122 0.47 2.09 2.03 889.36 86 78 57 251 250 893.43 18 85 3 121 0.47 2.09 2.03 893.43 88 79 60 248 250 897.52 19 90 3 120 0.43 1.91 1.87 897.53 89 80 62 248 251 901.45 20 95 3 122 0.43 1.91 1.87 901.45 90 81 62 248 252 905.37 21 100 3 123 0.40 1.78 1.75 905.36 91 82 63 249 250 909.15 22 105 3 124 0.40 1.79 1.75 909.14 92 84 63 248 249 912.93 23 110 3 124 0.38 1.70 1.67 912.94 93 85 63 250 250 916.64 24 115 3 124 0.38 1.70 1.67 916.64 93 86 63 250 251 920.35 

120 11:22 920.35

1 120 3 122 0.31 1.39 1.37 920.35 90 88 60 250 251 923.70 2 125 3 124 0.31 1.39 1.37 923.71 93 88 61 251 251 927.07 3 130 3 124 0.32 1.44 1.42 927.06 94 88 60 250 250 930.47 4 135 3 124 0.32 1.44 1.42 930.48 94 89 60 248 250 933.90 5 140 3 124 0.31 1.40 1.38 933.90 95 89 59 249 252 937.26 6 145 3 124 0.31 1.40 1.38 937.25 95 90 58 248 249 940.62 7 150 3 124 0.33 1.49 1.47 940.61 96 90 58 251 251 944.09 8 155 3 124 0.33 1.49 1.48 944.09 96 91 57 250 250 947.57 9 160 3 124 0.33 1.49 1.48 947.58 97 91 59 251 249 951.06 

10 165 3 124 0.33 1.49 1.48 951.07 98 92 58 248 249 954.56 11 170 3 125 0.37 1.68 1.67 954.55 98 92 59 251 248 958.24 12 175 3 125 0.37 1.68 1.67 958.26 99 93 58 252 241 961.96 13 180 3 124 0.43 1.95 1.94 961.96 99 93 59 251 250 965.95 14 185 3 125 0.43 1.96 1.94 965.97 99 94 60 252 251 969.96 15 190 3 125 0.40 1.82 1.81 969.96 100 94 61 248 251 973.81 16 195 3 125 0.40 1.82 1.82 973.82 101 94 62 248 249 977.68 17 200 3 126 0.41 1.87 1.87 977.69 101 94 62 251 250 981.59 18 205 3 126 0.41 1.87 1.87 981.60 101 95 63 253 251 985.50 19 210 3 126 0.39 1.78 1.78 985.49 101 96 62 247 248 989.30 20 215 3 126 0.39 1.79 1.78 989.31 102 96 62 250 252 993.12 21 220 3 126 0.33 1.51 1.51 993.12 102 96 63 250 249 996.63 22 225 3 126 0.33 1.52 1.51 996.63 102 96 63 251 248 1000.14 23 230 3 126 0.31 1.43 1.42 1000.15 102 96 62 250 250 1003.55 24 235 3 126 0.31 1.43 1.43 1003.55 102 97 62 248 252 1006.95 

240 13:32 1006.95

Average 240 123.0 0.37 1.66 1.62 173.740 88 81 57 250 250 921 

84.72
Company JM Winder

Source Designation 106Test Date 1/24/2012 Assumed Moisture (Bws) 2

Test Number 3 Condensate Volume (Vlc) 13

Operator PM Silica Gel Weight Gain (Vlc) 32.6

Filter Number 11121404 Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.17 Leak Rate Initial .001@10"

Stack Static Pressure (Ps) 0.31 Leak Rate Final .000@7"Stack Dimensions 1 (in.) 54 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5ft B Meter Corr. Factor (Y) 0.998

Meter Number MB 3 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0Delta ∆H@ 1.77 O2 20.63

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Expected 

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature DGM 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (cubic feet) 

1 0 14:07 0 122 0.31 1.36 1.38 7.25 95 94 60 250 251 10.63 2 5 4 123 0.31 1.36 1.38 10.64 96 94 60 251 252 14.03 3 10 4 125 0.32 1.40 1.42 14.04 97 95 60 250 252 17.48 4 15 4 125 0.32 1.41 1.42 17.49 99 95 58 250 251 20.94 5 20 4 127 0.35 1.54 1.56 20.94 99 95 58 250 249 24.54 6 25 4 128 0.35 1.54 1.56 24.54 100 95 59 248 251 28.14 7 30 4 130 0.34 1.50 1.51 28.14 100 95 58 249 250 31.68 8 35 4 131 0.34 1.50 1.51 31.69 101 96 59 251 250 35.23 9 40 4 131 0.35 1.55 1.56 35.22 101 96 60 249 250 38.81 

10 45 4 131 0.35 1.55 1.56 38.81 101 96 61 251 250 42.40 11 50 4 131 0.37 1.64 1.65 42.42 101 96 60 253 252 46.12 12 55 4 131 0.37 1.64 1.65 46.13 101 96 61 249 250 49.83 13 60 4 131 0.40 1.78 1.79 49.84 101 96 60 248 250 53.68 14 65 4 131 0.40 1.78 1.79 53.68 101 96 60 250 252 57.52 15 70 4 132 0.43 1.91 1.93 57.53 101 96 61 249 251 61.51 16 75 4 132 0.43 1.92 1.93 61.51 101 96 60 248 249 65.49 17 80 4 132 0.45 2.01 1.97 65.48 101 96 61 250 252 69.55 18 85 4 132 0.45 2.01 1.97 69.55 101 96 60 248 251 73.62 19 90 4 133 0.43 1.92 1.93 73.61 101 96 60 248 252 77.59 20 95 5 133 0.43 1.92 1.94 77.59 101 96 61 249 249 81.57 21 100 5 133 0.37 1.66 1.67 81.58 101 96 62 249 250 85.27 22 105 5 133 0.37 1.66 1.67 85.27 101 96 61 253 252 88.96 23 110 5 133 0.35 1.57 1.58 88.95 101 96 62 252 249 92.54 24 115 5 133 0.35 1.57 1.58 92.54 101 96 62 253 249 96.13 

120 16:07 96.13

1 120 16:15 4 132 0.29 1.31 1.31 96.13 96 95 62 249 251 99.38 2 125 4 132 0.29 1.31 1.31 99.37 97 95 62 249 249 102.62 3 130 4 132 0.30 1.36 1.36 102.61 97 95 61 251 249 105.92 4 135 4 132 0.30 1.36 1.36 105.93 98 94 61 249 250 109.24 5 140 4 132 0.32 1.45 1.45 109.24 98 94 59 247 251 112.66 6 145 4 132 0.32 1.45 1.46 112.65 99 94 58 252 250 116.07 7 150 4 132 0.35 1.59 1.59 116.08 99 94 58 253 251 119.66 8 155 4 132 0.35 1.59 1.60 119.68 99 94 58 247 249 123.26 9 160 4 133 0.33 1.50 1.51 123.26 99 95 56 248 252 126.74 

10 165 4 133 0.33 1.50 1.51 126.75 99 95 57 247 250 130.23 11 170 4 134 0.32 1.46 1.46 130.24 99 95 58 249 250 133.66 12 175 4 134 0.32 1.46 1.46 133.67 98 94 57 251 251 137.08 13 180 4 133 0.42 1.92 1.92 137.07 98 94 58 249 251 140.98 14 185 4 133 0.42 1.92 1.93 140.97 98 94 57 250 251 144.88 15 190 4 134 0.44 2.02 2.02 144.89 98 94 58 249 249 148.89 16 195 4 134 0.44 2.02 2.02 148.89 97 93 57 248 251 152.89 17 200 4 135 0.46 2.11 2.12 152.90 97 93 57 251 250 156.98 18 205 4 135 0.46 2.11 2.12 156.98 97 93 58 250 250 161.06 19 210 4 135 0.45 2.07 2.07 161.07 97 93 59 249 251 165.11 20 215 4 135 0.45 2.07 2.07 165.12 96 92 58 248 249 169.15 21 220 4 135 0.43 1.98 1.98 169.14 96 92 59 250 250 173.08 22 225 4 135 0.43 1.99 1.99 173.08 95 91 58 248 248 177.01 23 230 4 135 0.41 1.89 1.90 177.01 94 91 60 249 252 180.85 24 235 4 135 0.41 1.90 1.90 180.83 93 90 59 248 250 184.66 

240 184.66

Average 240 131.8 0.37 1.69 1.69 177.410 98.7 94.6 59.4 249.6 250.4 96.6 

96.63
Company JM Winder

Source Designation 106Test Date 1/23/2012 Assumed Moisture (Bws) 2

Test Number 1 Condensate Volume (Vlc) 44

Operator JP Silica Gel Weight Gain (Vlc) 34.7

Filter Number Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 29.92 Leak Rate Initial .003 @ 15 "

Stack Static Pressure (Pg) 0.31 Leak Rate Final .000 @ 6"

Stack Dimensions 1 (in.) 54 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number Meter Corr. Factor (Y) 1.002

Meter Number 5 Orsat Results (%)

Meter Isokinetic Factor (Kiso) CO2 0

Delta ∆H@ 1.55 O2 20.63

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Actual Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Filter Box Exit E

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature Temperature 

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (F) (cu

1 0 16:47 4 122 0.42 1.53 1.50 732.80 49 49 46 NA NA NA 2 5 4 123 0.42 1.53 1.50 736.42 49 49 45 NA NA NA 3 10 4 123 0.41 1.50 1.46 740.04 50 49 45 NA NA NA 4 15 4 123 0.41 1.50 1.47 743.63 52 49 45 NA NA NA 5 20 4 123 0.44 1.60 1.58 747.19 53 49 46 NA NA NA 6 25 4 122 0.44 1.60 1.58 750.91 55 49 47 NA NA NA 7 30 4 122 0.45 1.64 1.62 754.64 56 50 48 NA NA NA 8 35 4 123 0.45 1.64 1.62 758.40 57 50 48 NA NA NA 9 40 4 122 0.41 1.50 1.48 762.16 58 51 48 NA NA NA 

10 45 4 122 0.41 1.50 1.48 765.79 59 51 48 NA NA NA 11 50 4 122 0.38 1.39 1.38 769.43 59 51 48 NA NA NA 12 55 4 122 0.38 1.39 1.38 772.93 60 52 48 NA NA NA 13 60 4 122 0.36 1.31 1.31 776.41 60 52 49 NA NA NA 14 65 4 121 0.36 1.31 1.31 779.81 61 53 48 NA NA NA 15 70 3.5 121 0.35 1.28 1.28 783.22 61 53 49 NA NA NA 16 75 3.5 121 0.35 1.28 1.28 786.59 61 53 48 NA NA NA 17 80 3.5 120 0.35 1.28 1.28 789.98 62 54 48 NA NA NA 18 85 3.5 120 0.35 1.28 1.28 793.35 62 54 48 NA NA NA 19 90 3.5 121 0.32 1.17 1.18 796.70 62 55 48 NA NA NA 20 95 3.5 121 0.32 1.17 1.18 799.94 63 55 48 NA NA NA 21 100 3.5 121 0.31 1.13 1.14 803.14 63 55 48 NA NA NA 22 105 3.5 121 0.31 1.13 1.15 806.30 63 55 48 NA NA NA 23 110 3.5 121 0.30 1.09 1.11 809.50 63 56 47 NA NA NA 24 115 3.5 121 0.30 1.09 1.11 812.59 63 56 47 NA NA NA 

120 18:47 815.70

1 120 18:52 4.5 120 0.45 1.64 1.67 815.70 58 56 46 NA NA NA 2 125 4.5 120 0.45 1.64 1.68 819.48 61 57 46 NA NA NA 3 130 4.5 120 0.48 1.75 1.79 823.29 63 57 47 NA NA NA 4 135 4.5 121 0.48 1.75 1.79 827.24 64 57 48 NA NA NA 5 140 4.5 121 0.49 1.79 1.83 831.21 65 57 48 NA NA NA 6 145 4.5 121 0.49 1.79 1.84 835.20 65 58 49 NA NA NA 7 150 4.5 121 0.48 1.75 1.80 839.20 66 58 50 NA NA NA 8 155 4.5 122 0.48 1.75 1.80 843.16 66 58 50 NA NA NA 9 160 4.5 121 0.45 1.64 1.69 847.13 66 59 51 NA NA NA 

10 165 4.5 121 0.45 1.64 1.70 850.99 67 59 51 NA NA NA 11 170 4.5 122 0.45 1.64 1.70 854.85 68 60 52 NA NA NA 12 175 4.5 122 0.45 1.64 1.70 858.72 68 60 52 NA NA NA 13 180 4 122 0.41 1.50 1.55 862.59 68 60 52 NA NA NA 14 185 4 122 0.41 1.50 1.55 866.30 68 60 51 NA NA NA 15 190 4 122 0.36 1.32 1.37 869.99 68 61 52 NA NA NA 16 195 4 122 0.36 1.32 1.37 873.46 68 61 50 NA NA NA 17 200 3.5 122 0.35 1.28 1.33 876.90 68 61 50 NA NA NA 18 205 3.5 122 0.35 1.28 1.33 880.30 68 61 50 NA NA NA 19 210 3.5 122 0.32 1.18 1.22 883.70 69 62 49 NA NA NA 20 215 3.5 122 0.32 1.18 1.22 886.98 69 62 49 NA NA NA 21 220 3.5 122 0.32 1.18 1.23 890.21 69 62 50 NA NA NA 22 225 3.5 121 0.32 1.18 1.23 893.45 69 62 49 NA NA NA 23 230 3.5 118 0.29 1.07 1.11 896.71 69 62 49 NA NA NA 24 235 3.5 118 0.29 1.07 1.12 899.85 69 63 49 NA NA NA 

240 20:52 902.95

Average 240 121.4 0.39 1.42 1.44 170.150 62.5 55.9 48.5 #DIV/0! #DIV/0! #DIV/0! 

59.20
Company JM Winder

Source Designation Line 106Test Date 1/24/2012 Assumed Moisture (Bws) 2

Test Number 2 Condensate Volume (Vlc) 44

Operator JP Silica Gel Weight Gain (Vlc) 34.7

Filter Number Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.17 Leak Rate Initial .000 @ 12"

Stack Static Pressure (Ps) 0.31 Leak Rate Final .000 @ 6"

Stack Dimensions 1 (in.) 54 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5 ft C Meter Corr. Factor (Y) 1.002

Meter Number 5 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0Delta ∆H@ 1.55 O2 20.63

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Filter Box Exit Expec

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature Temperature DG

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (F) (cubic 

1 0 9:12 2.5 122 0.30 1.12 1.08 904.90 52 51 60 NA NA NA 907.2 5 2.5 122 0.30 1.13 1.08 907.97 53 51 56 NA NA NA 911.3 10 2.5 122 0.30 1.13 1.08 911.02 55 52 56 NA NA NA 914.4 15 2.5 122 0.30 1.13 1.08 914.09 57 52 56 NA NA NA 917.5 20 2.5 122 0.31 1.17 1.12 917.18 59 53 57 NA NA NA 920.6 25 2.5 123 0.31 1.17 1.12 920.29 61 53 58 NA NA NA 923.7 30 2.5 123 0.34 1.28 1.23 923.43 62 54 58 NA NA NA 926.8 35 2.5 123 0.34 1.28 1.24 926.71 63 55 58 NA NA NA 930.9 40 2.5 123 0.35 1.32 1.28 930.01 65 56 57 NA NA NA 933.

10 45 2.5 123 0.35 1.33 1.28 933.35 65 56 58 NA NA NA 936.11 50 2.5 123 0.37 1.40 1.36 936.73 66 57 58 NA NA NA 940.12 55 2.5 123 0.37 1.40 1.36 940.18 67 58 59 NA NA NA 943.13 60 10:12/10:22 3 123 0.40 1.52 1.47 943.65 67 58 59 NA NA NA 947.14 65 3 124 0.40 1.52 1.47 947.25 69 60 57 NA NA NA 950.15 70 3 124 0.41 1.56 1.52 950.87 72 62 57 NA NA NA 954.16 75 3 125 0.42 1.60 1.55 954.52 75 63 56 NA NA NA 958.17 80 3 124 0.44 1.68 1.63 958.29 78 65 56 NA NA NA 962.18 85 3 124 0.44 1.68 1.64 962.11 80 66 56 NA NA NA 965.19 90 3 124 0.44 1.68 1.64 965.95 81 68 56 NA NA NA 969.20 95 3 124 0.44 1.69 1.64 969.85 82 70 57 NA NA NA 973.21 100 3 124 0.41 1.57 1.53 973.74 84 71 57 NA NA NA 977.22 105 3 124 0.41 1.57 1.54 977.51 84 72 58 NA NA NA 981.23 110 3 125 0.39 1.50 1.47 981.27 85 73 58 NA NA NA 984.24 115 3 125 0.39 1.50 1.47 984.92 87 75 57 NA NA NA 988.

120 11:22 988.62

1 120 11:31 2.5 122 0.30 1.16 1.13 988.62 82 78 53 NA NA NA 991.2 125 2.5 124 0.30 1.16 1.14 991.82 88 79 56 NA NA NA 995.3 130 2.5 125 0.31 1.20 1.18 995.05 90 80 56 NA NA NA 998.4 135 2.5 125 0.31 1.20 1.18 998.39 91 81 54 NA NA NA 10015 140 2.5 125 0.32 1.24 1.22 1001.66 91 81 54 NA NA NA 10056 145 2.5 125 0.32 1.24 1.22 1005.01 91 82 54 NA NA NA 10087 150 2.5 126 0.34 1.32 1.30 1008.36 92 82 55 NA NA NA 10118 155 2.5 126 0.34 1.32 1.31 1011.85 92 83 55 NA NA NA 10159 160 2.5 126 0.36 1.40 1.39 1015.31 93 84 56 NA NA NA 1018

10 165 2.5 126 0.36 1.40 1.39 1018.90 94 84 56 NA NA NA 102211 170 3 126 0.40 1.56 1.55 1022.47 94 84 57 NA NA NA 102612 175 3 127 0.40 1.56 1.55 1026.28 94 85 56 NA NA NA 103013 180 3 127 0.44 1.72 1.71 1030.09 93 86 56 NA NA NA 103414 185 3 127 0.44 1.72 1.71 1034.07 94 86 57 NA NA NA 103815 190 3 127 0.45 1.76 1.75 1038.00 94 86 57 NA NA NA 104216 195 3 127 0.45 1.77 1.76 1042.02 94 86 58 NA NA NA 104617 200 3 127 0.47 1.85 1.84 1046.01 94 86 58 NA NA NA 105018 205 3 128 0.47 1.85 1.84 1050.10 94 87 58 NA NA NA 105419 210 3 127 0.47 1.85 1.84 1054.22 94 86 59 NA NA NA 105820 215 3 127 0.47 1.85 1.85 1058.30 94 87 60 NA NA NA 106221 220 3 127 0.46 1.82 1.81 1062.40 93 87 60 NA NA NA 106622 225 3 126 0.46 1.82 1.81 1066.48 93 87 61 NA NA NA 107023 230 3 126 0.44 1.74 1.74 1070.51 93 87 61 NA NA NA 107424 235 3 126 0.44 1.74 1.74 1074.50 92 87 62 NA NA NA 1078

240 1078.48

Average 240 124.7 0.38 1.48 1.46 173.580 81 72 57 #DIV/0! #DIV/0! #DIV/0! 

76.61
Company JM Winder

Source Designation Line 106Test Date 1/24/2012 Assumed Moisture (Bws) 2

Test Number 3 Condensate Volume (Vlc)Operator JP Silica Gel Weight Gain (Vlc)Filter Number Nozzle Diameter (in.) 0.26

Barometric Pressure (Pb) 30.17 Leak Rate Initial .000 @ 12"

Stack Static Pressure (Ps) 0.31 Leak Rate Final .000 @ 6"

Stack Dimensions 1 (in.) 54 Traverse points 24

*Stack Dimensions 2 (in.) Pitot Corr. Factor (Cp) 0.84

Pitot Tube Number 5 ft C Meter Corr. Factor (Y) 1.002

Meter Number 5 Orsat Results (%)Meter Isokinetic Factor (Kiso) CO2 0Delta ∆H@ 1.55 O2 20.63

Traverse Sampling Time Sampling Stack Temp.Velocity Pres. Desired Orifice Orifice Sample Volume Dry Gas Meter Temp. Last Impinger Probe Filter Box Filter Box Exit Expec

Point (Minutes) Clock Time Train Vac. (F) ("H2O) Differential Differential (cubic feet) Inlet Outlet Temperature Temperature Temperature Temperature DG

Number ø (24 hour) ("Hg) Ts ∆Ps ("H2O) ∆H ("H2O) ∆H Vm (F) Tm (F) Tm (F) (F) (F) (F) (cubic 

1 0 14:07 3 122 0.30 1.12 1.14 78.67 83 83 66 NA NA NA 81.92 5 3 123 0.30 1.12 1.14 81.90 84 83 65 NA NA NA 85.13 10 3 124 0.30 1.12 1.14 85.12 85 83 65 NA NA NA 88.34 15 3 124 0.30 1.12 1.14 88.38 86 83 65 NA NA NA 91.65 20 3 123 0.32 1.20 1.22 91.63 86 83 65 NA NA NA 94.96 25 3 132 0.32 1.20 1.22 94.97 87 83 65 NA NA NA 98.37 30 3 132 0.33 1.24 1.26 98.34 87 83 64 NA NA NA 101.8 35 3 132 0.33 1.24 1.26 101.71 87 83 64 NA NA NA 105.9 40 3 132 0.35 1.31 1.34 105.12 88 83 64 NA NA NA 108.

10 45 3 132 0.35 1.31 1.34 108.59 87 83 64 NA NA NA 112.11 50 3.5 132 0.39 1.46 1.49 112.09 87 83 64 NA NA NA 115.12 55 3.5 132 0.39 1.46 1.49 115.80 88 83 64 NA NA NA 119.13 60 3.5 132 0.42 1.57 1.61 119.47 88 83 64 NA NA NA 123.14 65 3.5 132 0.42 1.57 1.61 123.32 88 83 64 NA NA NA 127.15 70 3.5 133 0.45 1.69 1.73 127.16 88 83 64 NA NA NA 131.16 75 3.5 133 0.45 1.69 1.73 131.11 88 83 64 NA NA NA 135.17 80 3.5 133 0.46 1.72 1.77 135.08 88 83 65 NA NA NA 139.18 85 3.5 133 0.46 1.72 1.77 139.10 88 84 64 NA NA NA 143.19 90 3.5 133 0.46 1.72 1.77 143.08 89 84 65 NA NA NA 147.20 95 3.5 133 0.46 1.72 1.77 147.11 89 84 64 NA NA NA 151.21 100 3.5 133 0.45 1.69 1.74 151.10 88 84 63 NA NA NA 155.22 105 3.5 133 0.45 1.69 1.74 155.06 88 84 63 NA NA NA 159.23 110 3.5 133 0.44 1.65 1.70 159.03 88 84 63 NA NA NA 162.24 115 3.5 133 0.44 1.65 1.70 162.98 88 84 64 NA NA NA 166.

120 16:07 166.91

1 120 16:15 3 133 0.29 1.09 1.12 166.91 84 83 60 NA NA NA 170.2 125 3 133 0.29 1.09 1.12 170.06 85 83 61 NA NA NA 173.3 130 3 133 0.30 1.12 1.16 173.25 86 83 59 NA NA NA 176.4 135 3 133 0.30 1.12 1.17 176.45 86 83 57 NA NA NA 179.5 140 3 134 0.30 1.12 1.17 179.72 86 82 55 NA NA NA 182.6 145 3 134 0.30 1.12 1.17 182.95 86 82 55 NA NA NA 186.7 150 3 134 0.34 1.27 1.33 186.16 86 82 55 NA NA NA 189.8 155 3 134 0.34 1.27 1.33 189.61 86 82 55 NA NA NA 193.9 160 3 134 0.35 1.31 1.37 193.02 86 82 55 NA NA NA 196.

10 165 3 134 0.35 1.31 1.37 196.51 85 82 55 NA NA NA 199.11 170 3 135 0.38 1.42 1.49 200.02 85 81 55 NA NA NA 203.12 175 3 135 0.38 1.42 1.49 203.66 85 81 55 NA NA NA 207.13 180 3 135 0.40 1.50 1.57 207.29 85 81 55 NA NA NA 211.14 185 3 135 0.40 1.50 1.57 211.03 85 80 55 NA NA NA 214.15 190 3 135 0.40 1.50 1.57 214.76 84 80 55 NA NA NA 218.16 195 3 135 0.41 1.54 1.61 218.42 84 80 54 NA NA NA 222.17 200 3.5 135 0.43 1.62 1.69 222.18 83 79 55 NA NA NA 226.18 205 3.5 135 0.43 1.62 1.69 226.02 83 79 54 NA NA NA 229.19 210 3.5 135 0.43 1.62 1.69 229.83 83 78 53 NA NA NA 233.20 215 3.5 135 0.43 1.63 1.70 233.66 82 78 53 NA NA NA 237.21 220 3 133 0.40 1.51 1.58 237.49 82 78 52 NA NA NA 241.22 225 3 134 0.40 1.52 1.58 241.20 81 77 52 NA NA NA 244.23 230 3 134 0.40 1.52 1.58 244.91 81 77 52 NA NA NA 248.24 235 3 134 0.40 1.52 1.58 248.61 80 76 51 NA NA NA 252.

240 252.30

Average 240 132.4 0.38 1.42 1.47 173.630 85.7 81.8 59.6 #DIV/0! #DIV/0! #DIV/0! 

83.75





































Appendix B 

 Process Data 
Appendix C 

Equipment Calibration Documents 
Oxygen and Carbon Dioxide Concentration Results Summary

Johns Manville - Winder, GA

BTEC Project No. 11-4191.01

Sampling Dates: 1/23/12-1/26/12

Source: 106

Parameter Run 1 Run 2 Run 3 Average

Test Run Date 1/23/2012 1/24/2012 1/24/2012Test Time 21:24 15:35 19:22Oxygen concentration (%) 20.73 20.75 20.75 20.74Oxygen concentration (%) (corrected as per USEPA 3A) 20.63 20.65 20.62 20.63Carbon Dioxide concentration (%) 0.00 0.01 0.02 0.01Carbon Dioxide concentration (%) (corrected as per USEPA 3A) -0.07 0.00 0.01 -0.02CO2 Correction O2 Corr

1 2 3 

Co 0.07 0.01 0.01 Co 

Cma 10.20 10.20 10.20 Cma 

Cm 10.14 10.16 10.05 Cm 

Co= Average of initial and final zero gasesCma=Actual concentration of the calibration gasCm= Average of initial and final calibration gases
Oxygen and Carbon Dioxide Concentration Results Summary

Johns Manville - Winder, GA

BTEC Project No. 11-4191.01

Sampling Dates: 1/23/12-1/26/12

Source: 105

Parameter Run 1 Run 2 Run 3 Average

Test Run Date 1/25/2012 1/26/2012 1/26/2012Test Time 14:40 14:33 14:36Oxygen concentration (%) 20.76 20.67 20.73 20.72Oxygen concentration (%) (corrected as per USEPA 3A) 20.65 20.51 20.57 20.57Carbon Dioxide concentration (%) 0.02 0.01 0.10 0.04Carbon Dioxide concentration (%) (corrected as per USEPA 3A) 0.01 0.00 0.09 0.03CO2 Correction O2 Corr

1 2 3 

Co 0.01 0.01 0.02 Co 

Cma 10.20 10.20 10.20 Cma 

Cm 10.26 10.32 10.22 Cm 

Co= Average of initial and final zero gasesCma=Actual concentration of the calibration gasCm= Average of initial and final calibration gases
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at tested vacuum (from Orifice Calibration Report), for a period of time

necessary to achieve a minimum total volume of 5 cubic feet.

4) Record data and information in the GREEN cells, YELLOW cells are calculated.

INITIAL FINAL AVG (Pbar

)

DATE: 1/13/2012 METER SERIAL #: C-5000 BAROMETRIC PRESSURE (in Hg): 29.54 29.54 29.54 

METER PART #: MB3 CRITICAL ORIFICE SET SERIAL #: 1447 

K' TESTED TEMPERATURES °F ELAPSED

FACTOR VACUUM DGM READINGS (FT

3

) AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN) DGM ∆H (1) 

ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) INITIAL FINAL INITIAL FINAL AVG θ (in H2O) Vm (STD) Vcr 

1 0.8778 16 602.70 609.330 6.630 67 52 54 50 52 52 6.00 4.1 6.8206 6.2 0.8778 16 609.330 615.980 6.650 66 54 57 52 53 54 6.00 4.1 6.8146 6.3 0.8778 16 615.980 622.670 6.690 66 57 61 53 55 56.5 6.00 4.1 6.8224 6.1 0.5057 16 623.0 628.760 5.760 65 60 63 56 58 59.25 9.00 1.3 5.8025 5.2 0.5057 16 628.760 634.550 5.790 66 63 66 58 60 61.75 9.00 1.3 5.8048 5.3 0.5057 16 634.550 640.340 5.790 67 66 68 60 62 64 9.00 1.3 5.7798 5.1 0.3367 16 640.50 645.810 5.310 66 66 68 62 64 65 12.00 0.58 5.2811 5.2 0.3367 16 645.810 651.120 5.310 67 68 70 64 65 66.75 12.00 0.58 5.2636 5.3 0.3367 16 651.120 656.460 5.340 67 70 70 65 67 68 12.00 0.58 5.2808 5.

AVERAGE DRY GAS METER CALIBRATION FACT

AVERAG

(1) = Net volume of gas sample passed through DGM, corrected to standard conditions

K1 = 17.64 

oR/in. Hg (English), 0.3858 

oK/mm Hg (Metric)

Tm = Absolute DGM avg. temperature (

oR - English, oK - Metric) ∆H@ = 0.

Vcr

(2) = Volume of gas sample passed through the critical orifice, corrected to standard conditions

Tamb = Absolute ambient temperature (

oR - English, oK - Metric)

K' = Average K' factor from Critical Orifice Calibration

(3) = DGM calibration factor

321812

ENVIRONMENTAL 

USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical 

orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. 

( 

Tm

HPbar

std VmKVm )6.13/( 1)(

+

∆

∗∗=

Tamb

Pbar KVcr std

∗ Θ

)(

'∗=

)(

)(

stdstd

Vm

Vcr

Y

=
METHOD 5 DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at tested vacuum (from Orifice Calibration Report), for a period of time

necessary to achieve a minimum total volume of 5 cubic feet.

4) Record data and information in the GREEN cells, YELLOW cells are calculated.

INITIAL FINAL AVG (Pbar

)

DATE: 1/20/2012 METER SERIAL #: 1672 BAROMETRIC PRESSURE (in Hg): 30.27 30.29 30.28 

METER PART #: MB5 CRITICAL ORIFICE SET SERIAL #: 1447 

K' TESTED TEMPERATURES °F ELAPSED

FACTOR VACUUM DGM READINGS (FT

3

) AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN) DGM ∆H (1) 

ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) INITIAL FINAL INITIAL FINAL AVG θ (in H2O) Vm (STD) Vcr 

1 0.8778 15 679.220 685.945 6.725 55 55 55 55 55 55 6.00 3.7 7.0418 7.2 0.8778 15 685.945 692.708 6.763 55 55 56 55 55 55.25 6.00 3.7 7.0782 7.3 0.8778 15 692.708 699.442 6.734 55 56 59 55 56 56.5 6.00 3.7 7.0308 7.1 0.5057 16 699.442 705.210 5.768 55 59 61 56 56 58 9.00 1.2 5.9686 6.2 0.5057 16 705.210 710.990 5.780 60 61 62 56 57 59 9.00 1.2 5.9695 6.3 0.5057 16 710.990 716.767 5.777 61 62 64 57 58 60.25 9.00 1.2 5.9521 6.1 0.3367 16 716.767 722.024 5.257 62 64 65 58 60 61.75 12.00 0.53 5.3920 5.2 0.3367 16 722.024 727.285 5.261 62 65 66 60 61 63 12.00 0.53 5.3832 5.3 0.3367 16 727.285 732.552 5.267 63 66 67 61 63 64.25 12.00 0.53 5.3764 5.

AVERAGE DRY GAS METER CALIBRATION FACT

AVERAG

(1) = Net volume of gas sample passed through DGM, corrected to standard conditions

K1 = 17.64 

oR/in. Hg (English), 0.3858 

oK/mm Hg (Metric)

Tm = Absolute DGM avg. temperature (

oR - English, oK - Metric) ∆H@ = 0.

Vcr

(2) = Volume of gas sample passed through the critical orifice, corrected to standard conditions

Tamb = Absolute ambient temperature (

oR - English, oK - Metric)

K' = Average K' factor from Critical Orifice Calibration

(3) = DGM calibration factor

321812

ENVIRONMENTAL 

USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm (std), and the critical 

orifice, Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above. 

( 

Tm

HPbar

std VmKVm )6.13/( 1)(

+

∆

∗∗=

Tamb

Pbar KVcr std

∗ Θ

)(

'∗=

)(

)(

stdstd

Vm

Vcr

Y

=








Appendix D 

Laboratory Analytical Results 
Acetone 

Rinse 

Volume 

(mL)

Particulate 

Weight in 

Acetone 

Rinse (mg)

Particulate 

Weight on 

Filter (mg)

Particulate 

Weight in 

Acetone 

Rinse (mg)

Combined 

Particulate 

Weight 

(mg)

Run 1 87 3.8 0.06 3.6 3.9Run 2 89 2.0 0.06 1.8 2.1Run 3 95 2.7 0.06 2.5 2.8

Blank 240 0.5 0.06

Note: Run detection limits of 0.3 mg on the filter were used.

Method 5 PM Lab Results

Corrected

Sampling Date: January 23-26, 2012

BTEC job #11-4191.05

Winder, Georgia Line 105

Johns Manville
Acetone 

Rinse 

Volume 

(mL)

Particulate 

Weight in 

Acetone 

Rinse (mg)

Particulate 

Weight on 

Filter (mg)

Particulate 

Weight in 

Acetone 

Rinse (mg)

Combined 

Particulate 

Weight 

(mg)

Run 1 120 3.6 0.06 3.4 3.7Run 2 120 2.9 0.10 2.7 3.0

Run 3 87 6.2 0.06 6.0 6.3

Blank 240 0.5 0.06

Note: Run detection limits of 0.3 mg on the filter were used.

Method 5 PM Lab Results

Corrected

Sampling Date: January 23 and 26, 2012

BTEC job #11-4191.05

Winder, Georgia

Johns Manville
Compound/Fraction

Blank 

Filter 

Result

(μg)

Blank 

Filter 

Detection 

Limit

(μg)

Run 1 

Result

(μg)

Run 2 

Result

(μg)

Run 3 

Result

(μg)

Test Run 

Detection 

Limit

(μg)

Run 1

(μg)

Ru

(μ

Back Half Chromium (Vaporous) 1.11 0.15 1.04 1.12 0.97 0.15 0.15 0

Front Half Chromium (Filterable) 1.56 0.30 3.34 7.67 4.23 0.60 1.78 6

Note: For Runs 1, 2, and 3, the test run detection limit of 0.15 μg was used for the back half result.

Johns Manville

Method 29 Lab Results

Corr

Sampling Date: January 23 and 26, 2012

BTEC job #11-4191.05

Winder, Georgia
Corrected

Total Volume 

(ml)

Impinger KOH 

(ml)

Hexavalent 

Chromium, 

Cr6+ [μg] RDL

Hexavalent 

Chromium, 

Cr6+ [μg]

Run 1 937 657 0.80 0.30 0.36

Run 2 1043 773 0.80 0.40 0.40

Run 3 952 672 0.60 0.30 0.30

Blank KOH 600 0.40 0.20

Total Volume 

(ml)

Impinger KOH 

(ml)

Back Half 

Chromium 

(μg)

Back Half 

RDL

Front Half 

Chromium 

(μg)

Front Half 

RDL

Rinse 

Chromium 

(μg)

Run 1 937 657 2.00 4.00 0.20 0.30 1.00 

Run 2 1043 773 3.00 5.00 0.20 0.30 1.00 Run 3 952 672 2.00 4.00 0.90 0.30 1.00 

Blank KOH 600 1.00 2.00 0.20 0.30 1.00 

Note: No blank correction applied. RDL used for all fractions except Run 3 front half.

Method 0061 Lab Results

Sampling Date: January 23 and 26, 2012

BTEC job #11-4191.05

Winder, Georgia

Johns Manville
Your Project #: 11-4191.05 

Site Location: JM WINDER - LINE 105 & 106 

Attention: Barry Boulianne

BT Environmental Consulting

4949 Fernlee Avenue

Royal Oak, MI

USA 48073

Report Date: 2012/02/10

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B213471

Received: 2012/01/28, 11:35

Sample Matrix: Stack Sampling Train

# Samples Received: 8

Date Date Method

Analyses Quantity Extracted Analyzed Laboratory Method Reference

Hexavalent Chromium (M0061) 8 2012/02/01 2012/02/01 BRL SOP-00106 EPA 7199 (M0061) 

Chromium on Filter by ICP 7 2012/02/03 2012/02/03 CAM SOP-00408 / BRL EPA M0061 

SOP-00102

Chromium in Impinger by ICP 8 2012/02/03 2012/02/04 CAM SOP-00408 / BRL EPA M0061 

SOP-00102

Chromium in Train Rinse by ICP 7 2012/02/03 2012/02/04 CAM SOP-00408 / BRL EPA M0061 

SOP-00102

Final Volume of KOH Impinger 8 N/A 2012/02/01 

Final Volume of Train Rinse 7 N/A 2012/02/03 

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

U = Undetected at the limit of quantitation.

J = Estimated concentration between the EDL & RDL.

B = Blank Contamination.

Q = One or more quality control criteria failed.

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

CLAYTON JOHNSON, Project Manager

Email: CJohnson@maxxam.ca

Phone# (905) 817-5769

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section

5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 1 of 8
BT Environmental Consulting

Maxxam Job #: B213471 Client Project #: 11-4191.05

Report Date: 2012/02/10 Site Location: JM WINDER - LINE 105 & 106

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID M J 5 2 8 3 M J 5 2 8 4 M J 5 2 8 5 M J 5 2 8 5 M J 5 2 8 6

Sampling Date 2012/01/26 2012/01/26 2012/01/25 2012/01/25 2012/01/26

 U n i t s BLANK BLANK-M0061 RDL RUN RUN RUN RDL QC Batch

H20-M0061 1-105-M0061 1-105-M0061 2-105-M0061

Lab-Dup

Potassium Hydroxide Volume ml 411 300 1 696 646 1 2751510

Rinse Volume ml 300 1 220 230 1 2754786

Hexavalent Chromium (Cr 6+) ug 0.03 U 0.4 0.2 0.3 0.4 0.4 0.3 2752204

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID M J 5 2 8 7 M J 5 2 8 8 M J 5 2 8 9 M J 5 2 9 0

Sampling Date 2012/01/26 2012/01/23 2012/01/24 2012/01/24

 U n i t s RUN RDL RUN RDL RUN RDL RUN RDL QC Batch

3-105-M0061 1-106-M0061 2-106-M0061 3-106-M0061

Potassium Hydroxide Volume ml 713 1 657 1 773 1 672 1 2751510

Rinse Volume ml 230 1 280 1 270 1 280 1 2754786

Hexavalent Chromium (Cr 6+) ug 0.29 J 0.4 0.8 0.3 0.8 0.4 0.6 0.3 2752204

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 2 of 8
BT Environmental Consulting

Maxxam Job #: B213471 Client Project #: 11-4191.05

Report Date: 2012/02/10 Site Location: JM WINDER - LINE 105 & 106

ELEMENTS BY ICP-AES (STACK SAMPLING TRAIN)

Maxxam ID M J 5 2 8 3 M J 5 2 8 4 M J 5 2 8 5 M J 5 2 8 5 M J 5 2 8 6

Sampling Date 2012/01/26 2012/01/26 2012/01/25 2012/01/25 2012/01/26

 U n i t s BLANK BLANK-M0061 RDL RUN RUN RUN RDL QC Batch

H20-M0061 1-105-M0061 1-105-M0061 2-105-M0061

Lab-Dup

Back Half Chromium (Cr) ug 1 U 1 U 2 2 U 2 U 2 U 4 2754781

Front Half Chromium (Cr) ug 0.2 U 0.3 0.2 U 0.2 U 0.2 U 0.3 2754784

Rinse Chromium (Cr) ug 1 U 2 0.5 U 0.5 U 0.5 U 1 2754785

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID M J 5 2 8 7 M J 5 2 8 8 M J 5 2 8 9 M J 5 2 9 0

Sampling Date 2012/01/26 2012/01/23 2012/01/24 2012/01/24

 U n i t s RUN RDL RUN RDL RUN RDL RUN RDL QC Batch

3-105-M0061 1-106-M0061 2-106-M0061 3-106-M0061

Back Half Chromium (Cr) ug 2 U 4 2 U 4 3 U 5 2 U 4 2754781

Front Half Chromium (Cr) ug 0.2 U 0.3 0.2 U 0.3 0.2 U 0.3 0.9 0.3 2754784

Rinse Chromium (Cr) ug 0.5 U 1 1 U 2 1 U 2 1 U 2 2754785

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 3 of 8
BT Environmental Consulting

Maxxam Job #: B213471 Client Project #: 11-4191.05

Report Date: 2012/02/10 Site Location: JM WINDER - LINE 105 & 106

Test Summary

Maxxam ID MJ5283 Collected 2012/01/26

Sample ID BLANK H20-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Maxxam ID MJ5284 Collected 2012/01/26

Sample ID BLANK-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Maxxam ID MJ5285 Collected 2012/01/25

Sample ID RUN 1-105-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Maxxam ID MJ5285 D u p Collected 2012/01/25

Sample ID RUN 1-105-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Maxxam ID MJ5286 Collected 2012/01/26

Sample ID RUN 2-105-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Page 4 of 8
BT Environmental Consulting

Maxxam Job #: B213471 Client Project #: 11-4191.05

Report Date: 2012/02/10 Site Location: JM WINDER - LINE 105 & 106

Test Summary

Maxxam ID MJ5287 Collected 2012/01/26

Sample ID RUN 3-105-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Maxxam ID MJ5288 Collected 2012/01/23

Sample ID RUN 1-106-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Maxxam ID MJ5289 Collected 2012/01/24

Sample ID RUN 2-106-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Maxxam ID MJ5290 Collected 2012/01/24

Sample ID RUN 3-106-M0061 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2752204 2012/02/01 2012/02/01 LANG LE

Chromium on Filter by ICP ICP 2754784 2012/02/03 2012/02/03 SUBAN KANAPATHIPPLLAI

Chromium in Impinger by ICP ICP 2754781 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Chromium in Train Rinse by ICP ICP 2754785 2012/02/03 2012/02/04 SUBAN KANAPATHIPPLLAI

Final Volume of KOH Impinger 2751510 N/A 2012/02/01 FRANK MO

Final Volume of Train Rinse 2754786 N/A 2012/02/03 FRANK MO

Page 5 of 8
BT Environmental Consulting

Maxxam Job #: B213471 Client Project #: 11-4191.05

Report Date: 2012/02/10 Site Location: JM WINDER - LINE 105 & 106

GENERAL COMMENTS

Results relate only to the items tested.

Page 6 of 8
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 11-4191.05

P.O. #: 

Site Location: JM WINDER - LINE 105 & 106

Quality Assurance Report

Maxxam Job Number: GB213471

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2752204 LLE Matrix Spike

(MJ5285) Hexavalent Chromium (Cr 6+) 2012/02/01 113 % 80 - 120

Spiked Blank Hexavalent Chromium (Cr 6+) 2012/02/01 95 % 90 - 110

Method Blank Hexavalent Chromium (Cr 6+) 2012/02/01 0.03 U, MDL=0.03 ug

RPD -

Sample/Sample

Dup Hexavalent Chromium (Cr 6+) 2012/02/01 NC % 20

2754781 SUK Matrix Spike

(MJ5285) Back Half Chromium (Cr) 2012/02/04 97 % 80 - 120

Matrix Spike DUP

(MJ5285) Back Half Chromium (Cr) 2012/02/04 95 % 80 - 120

MS/MSD RPD Back Half Chromium (Cr) 2012/02/04 1.6 % 20

Spiked Blank Back Half Chromium (Cr) 2012/02/04 96 % 90 - 110

Spiked Blank DUP Back Half Chromium (Cr) 2012/02/04 95 % 90 - 110

RPD Back Half Chromium (Cr) 2012/02/04 1.6 % 20

Method Blank Back Half Chromium (Cr) 2012/02/04 0.3 U, MDL=0.3 ug

RPD -

Sample/Sample

Dup Back Half Chromium (Cr) 2012/02/04 NC % 20

2754784 SUK Matrix Spike

(MJ5285) Front Half Chromium (Cr) 2012/02/03 108 % 80 - 120

Spiked Blank Front Half Chromium (Cr) 2012/02/03 105 % 90 - 110

Spiked Blank DUP Front Half Chromium (Cr) 2012/02/03 106 % 90 - 110

RPD Front Half Chromium (Cr) 2012/02/03 0.6 % 20

Method Blank Front Half Chromium (Cr) 2012/02/03 0.2 U, MDL=0.2 ug

RPD -

Sample/Sample

Dup Front Half Chromium (Cr) 2012/02/03 NC % 20

2754785 SUK Matrix Spike

(MJ5285) Rinse Chromium (Cr) 2012/02/04 102 % 80 - 120

Matrix Spike DUP

(MJ5285) Rinse Chromium (Cr) 2012/02/04 103 % 80 - 120

MS/MSD RPD Rinse Chromium (Cr) 2012/02/04 1.4 % 20

Spiked Blank Rinse Chromium (Cr) 2012/02/04 103 % 90 - 110

Spiked Blank DUP Rinse Chromium (Cr) 2012/02/04 102 % 90 - 110

RPD Rinse Chromium (Cr) 2012/02/04 0.4 % 20

Method Blank Rinse Chromium (Cr) 2012/02/04 0.3 U, MDL=0.3 ug

RPD -

Sample/Sample

Dup Rinse Chromium (Cr) 2012/02/04 NC % 20

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.

Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.

Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a

reliable calculation.

Page 7 of 8
Validation Signature Page

Maxxam Job #: B213471

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

FRANK MO, B.Sc., Inorganic Lab. Manager 

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 of

ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page 8 of 8


Your Project #: 11-4191.05 

Site Location: JM WINDER - LINE 105 & 106 

Attention: Barry Boulianne

BT Environmental Consulting

4949 Fernlee Avenue

Royal Oak, MI

USA 48073

Report Date: 2012/02/09

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B213506

Received: 2012/01/28, 11:35

Sample Matrix: Stack Sampling Train

# Samples Received: 7

Date Date Method

Analyses Quantity Extracted Analyzed Laboratory Method Reference

Metals B.H. in H2O2/HNO3 Imp.(6020) 7 2012/02/07 2012/02/08 BRL SOP-00103 / BRL EPA 6020 / M29 

SOP-00102

Metals F.H. in Filter + Rinses (6020) 7 2012/02/07 2012/02/08 BRL SOP-00103/ BRL EPA 6020 / M29 

SOP-00102

Particulates/Acetone Rinse (M5/315/M201) 7 2012/02/01 2012/02/06 BRL SOP-00109 EPA 5/315 

Particulates/Filter (M5/315/NJATM1/M201) 7 N/A 2012/02/01 BRL SOP-00109 EPA 5/315/NJATM1 

Final Volume of Acetone Probe Rinse 7 N/A 2012/02/02 BRL SOP-00109 

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

U = Undetected at the limit of quantitation.

J = Estimated concentration between the EDL & RDL.

B = Blank Contamination.

Q = One or more quality control criteria failed.

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

CLAYTON JOHNSON, Project Manager

Email: CJohnson@maxxam.ca

Phone# (905) 817-5769

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section

5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 1 of 8
BT Environmental Consulting

Maxxam Job #: B213506 Client Project #: 11-4191.05

Report Date: 2012/02/09 Site Location: JM WINDER - LINE 105 & 106

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID M J 5 3 9 7 M J 5 3 9 8 M J 5 3 9 9 M J 5 4 0 0

Sampling Date 2012/01/23 2012/01/25 2012/01/26 2012/01/26

 U n i t s FIELD RUN RUN RUN RDL QC Batch

BLANK-M5/29 1-105-M5/29 2-105-M5/29 3-105-M5/29

Acetone Rinse Particulate Weight in Acetone Rinse mg 0.5 3.8 2.0 2.7 0.5 2752043

Front Half Particulate Weight on Filter mg 0.060 U 0.060 U 0.060 U 0.060 U 0.30 2752042

Acetone Rinse Volume ml 240 87 89 95 1 2752044

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID M J 5 4 0 1 M J 5 4 0 2 M J 5 4 0 3

Sampling Date 2012/01/23 2012/01/24 2012/01/24

 U n i t s RUN RUN RUN RDL QC Batch

1-106-M5/29 2-106-M5/29 3-106-M5/29

Acetone Rinse Particulate Weight in Acetone Rinse mg 3.6 2.9 6.2 0.5 2752043

Front Half Particulate Weight on Filter mg 0.060 U 0.100 J 0.060 U 0.30 2752042

Acetone Rinse Volume ml 120 120 87 1 2752044

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 2 of 8
BT Environmental Consulting

Maxxam Job #: B213506 Client Project #: 11-4191.05

Report Date: 2012/02/09 Site Location: JM WINDER - LINE 105 & 106

ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN)

Maxxam ID M J 5 3 9 7 M J 5 3 9 8 M J 5 3 9 8 M J 5 3 9 9 M J 5 4 0 0 M J 5 4 0 1

Sampling Date 2012/01/23 2012/01/25 2012/01/25 2012/01/26 2012/01/26 2012/01/23

 U n i t s FIELD RDL RUN RUN RUN RUN RUN RDL QC Batch

BLANK-M5/29 1-105-M5/29 1-105-M5/29 2-105-M5/29 3-105-M5/29 1-106-M5/29

Lab-Dup

Back Half Chromium (Cr) ug 1.11 0.15 0.86 0.89 1.07 1.20 1.04 0.15 2757470

Front Half Chromium (Cr) ug 1.56 0.30 4.82 4.88 2.78 2.08 3.34 0.60 2757471

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID M J 5 4 0 2 M J 5 4 0 3

Sampling Date 2012/01/24 2012/01/24

 U n i t s RUN RUN RDL QC Batch

2-106-M5/29 3-106-M5/29

Back Half Chromium (Cr) ug 1.12 0.97 0.15 2757470

Front Half Chromium (Cr) ug 7.67 4.23 0.60 2757471

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 3 of 8
BT Environmental Consulting

Maxxam Job #: B213506 Client Project #: 11-4191.05

Report Date: 2012/02/09 Site Location: JM WINDER - LINE 105 & 106

Test Summary

Maxxam ID MJ5397 Collected 2012/01/23

Sample ID FIELD BLANK-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Maxxam ID MJ5398 Collected 2012/01/25

Sample ID RUN 1-105-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Maxxam ID MJ5398 D u p Collected 2012/01/25

Sample ID RUN 1-105-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/09 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/09 2012/02/08 NAN RAYKHA

Maxxam ID MJ5399 Collected 2012/01/26

Sample ID RUN 2-105-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Maxxam ID MJ5400 Collected 2012/01/26

Sample ID RUN 3-105-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Page 4 of 8
BT Environmental Consulting

Maxxam Job #: B213506 Client Project #: 11-4191.05

Report Date: 2012/02/09 Site Location: JM WINDER - LINE 105 & 106

Test Summary

Maxxam ID MJ5401 Collected 2012/01/23

Sample ID RUN 1-106-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Maxxam ID MJ5402 Collected 2012/01/24

Sample ID RUN 2-106-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Maxxam ID MJ5403 Collected 2012/01/24

Sample ID RUN 3-106-M5/29 Shipped

Matrix Stack Sampling Train Received 2012/01/28

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals B.H. in H2O2/HNO3 Imp.(6020) ICP1/MS 2757470 2012/02/07 2012/02/08 NAN RAYKHA

Metals F.H. in Filter + Rinses (6020) ICP1/MS 2757471 2012/02/07 2012/02/08 NAN RAYKHA

Particulates/Acetone Rinse (M5/315/M201) BAL 2752043 2012/02/01 2012/02/06 BRENDA MOORE

Particulates/Filter (M5/315/NJATM1/M201) BAL 2752042 N/A 2012/02/01 BRENDA MOORE

Final Volume of Acetone Probe Rinse 2752044 N/A 2012/02/02 BRENDA MOORE

Page 5 of 8
BT Environmental Consulting

Maxxam Job #: B213506 Client Project #: 11-4191.05

Report Date: 2012/02/09 Site Location: JM WINDER - LINE 105 & 106

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Particulates/Filter (M5/315/NJATM1/M201): Negative results observed

ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN)

Metals B.H. in H2O2/HNO3 Imp.(6020): Post digestion duplicate and spike was done on sample MJ5398.

Metals F.H. in Filter + Rinses (6020): Extra 2x dilution was required for all samples except MJ5397, due to the matrix

Post digestion duplicate and spike was done on sample MJ5398.

Results relate only to the items tested.

Page 6 of 8
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 11-4191.05

P.O. #: 

Site Location: JM WINDER - LINE 105 & 106

Quality Assurance Report

Maxxam Job Number: GB213506

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2752043 RSU Method Blank Acetone Rinse Particulate Weight in Acetone 2012/02/06 0.1 J, MDL=0.1 mg

2757470 N_R Matrix Spike

(MJ5398) Back Half Chromium (Cr) 2012/02/08 99 % 70 - 130

Matrix Spike DUP

(MJ5398) Back Half Chromium (Cr) 2012/02/08 101 % 70 - 130

MS/MSD RPD Back Half Chromium (Cr) 2012/02/08 2.0 % 20

Spiked Blank Back Half Chromium (Cr) 2012/02/08 108 % 85 - 115

Spiked Blank DUP Back Half Chromium (Cr) 2012/02/08 102 % 85 - 115

RPD Back Half Chromium (Cr) 2012/02/08 6.0 % 20

Method Blank Back Half Chromium (Cr) 2012/02/08 0.070 U, MDL=0.070 ug

Method Blank DUP Back Half Chromium (Cr) 2012/02/08 0.070 U, MDL=0.070 ug

RPD Back Half Chromium (Cr) 2012/02/08 NC % 20

RPD -

Sample/Sample

Dup Back Half Chromium (Cr) 2012/02/08 3.1 % 20

2757471 N_R Matrix Spike

(MJ5398) Front Half Chromium (Cr) 2012/02/08 104 % 70 - 130

Matrix Spike DUP

(MJ5398) Front Half Chromium (Cr) 2012/02/08 104 % 70 - 130

MS/MSD RPD Front Half Chromium (Cr) 2012/02/08 0 % 20

Spiked Blank Front Half Chromium (Cr) 2012/02/08 100 % 85 - 115

Spiked Blank DUP Front Half Chromium (Cr) 2012/02/08 101 % 85 - 115

RPD Front Half Chromium (Cr) 2012/02/08 1.7 % 20

Method Blank Front Half Chromium (Cr) 2012/02/08 0.10 U, MDL=0.10 ug

Method Blank DUP Front Half Chromium (Cr) 2012/02/08 0.10 U, MDL=0.10 ug

RPD Front Half Chromium (Cr) 2012/02/08 NC % 20

RPD -

Sample/Sample

Dup Front Half Chromium (Cr) 2012/02/08 1.4 % 20

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.

Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.

Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a

reliable calculation.

Page 7 of 8
Validation Signature Page

Maxxam Job #: B213506

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

FRANK MO, B.Sc., Inorganic Lab. Manager 

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 of

ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page 8 of 8