Vinyl Institute 30 Day Concentration Database for Suspension Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column N for Revisions to Data Base Analyte Categor y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water

from Stripper Water

from Stripper Wet Resin

from Stripper Wet

Resin from Dry PVC

Resin from Dry

PVC Resin Formaldehyde (See Note 4) Aldehyde50-00-0Shintech TX 12/10/2009 Suspension GP 0.670 M 0.690 M 0.450 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.670 M 0.690 M 0.450 M Chloroethane VOC 75-00-3Shintech TX 12/10/2009 Suspension GP 0.034 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.034 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/10/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/10/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/10/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/10/2009 Suspension GP 0.114 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.114 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/10/2009 Suspension GP NM NM NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM NM NM Acetophenone SVOC 98-86-2Shintech TX 12/10/2009 Suspension GP 0.069 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.069 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/10/2009 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/10/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/10/2009 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/10/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/10/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/10/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/10/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/11/2009 Suspension GP 0.730 M 0.450 M 0.310 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.730 M 0.450 M 0.310 M Chloroethane VOC 75-00-3Shintech TX 12/11/2009 Suspension GP 0.033 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.033 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/11/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/11/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/11/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/11/2009 Suspension GP 0.140 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.140 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/11/2009 Suspension GP NM 7.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 7.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/11/2009 Suspension GP 0.128 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.128 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/11/2009 Suspension GP 0.010 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.010 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/11/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/11/2009 Suspension GP 3.000 U 25.000 U 104.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U ##### M PCBs SVOC 1336-36-3 Shintech TX 12/11/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/11/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/11/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/11/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/12/2009 Suspension GP 0.900 M 0.520 M 0.250 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.900 M 0.520 M 0.250 M Chloroethane VOC 75-00-3Shintech TX 12/12/2009 Suspension GP 0.043 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.043 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/12/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/12/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/12/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/12/2009 Suspension GP 0.148 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.148 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/12/2009 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/12/2009 Suspension GP 0.108 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.108 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/12/2009 Suspension GP 0.010 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.010 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/12/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/12/2009 Suspension GP 3.000 U 25.000 U 140.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U ##### M PCBs SVOC 1336-36-3 Shintech TX 12/12/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/12/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/12/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/12/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/13/2009 Suspension GP 0.680 M 0.350 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.680 M 0.350 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/13/2009 Suspension GP 0.053 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.053 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/13/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/13/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/13/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/13/2009 Suspension GP 0.152 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.152 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/13/2009 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/13/2009 Suspension GP 0.142 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.142 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/13/2009 Suspension GP 0.010 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.010 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/13/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/13/2009 Suspension GP 3.000 U 25.000 U 52.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 52.000 M PCBs SVOC 1336-36-3 Shintech TX 12/13/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/13/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/13/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/13/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/14/2009 Suspension GP 0.620 M 0.430 M 0.640 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.620 M 0.430 M 0.640 M Chloroethane VOC 75-00-3Shintech TX 12/14/2009 Suspension GP 0.029 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.029 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/14/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/14/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/14/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/14/2009 Suspension GP 0.085 M 1.220 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.085 M 1.220 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/14/2009 Suspension GP NM 5.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 5.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/14/2009 Suspension GP 0.112 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.112 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/14/2009 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/14/2009 Suspension GP 5.000 U 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 5.000 U 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/14/2009 Suspension GP 3.000 U 74.000 M 162.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 74.000 M ##### M PCBs SVOC 1336-36-3 Shintech TX 12/14/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/14/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/14/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/14/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/15/2009 Suspension GP 0.700 M 0.500 M 0.290 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.700 M 0.500 M 0.290 M Chloroethane VOC 75-00-3Shintech TX 12/15/2009 Suspension GP 0.046 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.046 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/15/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/15/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/15/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/15/2009 Suspension GP 0.133 M 0.854 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.133 M 0.854 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/15/2009 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/15/2009 Suspension GP 0.155 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.155 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/15/2009 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/15/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/15/2009 Suspension GP 3.000 U 25.000 M 52.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 M 52.000 M PCBs SVOC 1336-36-3 Shintech TX 12/15/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/15/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/15/2009 Suspension Acetaldehyde Aldehyde75-07-0Shintech TX Suspension 1,3-butadiene VOC 106-99-0 Shintech TX 12/15/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/15/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/16/2009 Suspension GP 0.510 M 0.250 M 0.470 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.510 M 0.250 M 0.470 M Chloroethane VOC 75-00-3Shintech TX 12/16/2009 Suspension GP 0.042 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.042 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/16/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/16/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/16/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/16/2009 Suspension GP 0.117 M 0.632 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.117 M 0.632 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/16/2009 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/16/2009 Suspension GP 0.130 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.130 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/16/2009 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/16/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/16/2009 Suspension GP 3.000 U 28.000 M 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 28.000 M 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/16/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/16/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/16/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/16/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/17/2009 Suspension GP 0.620 M 0.630 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.620 M 0.630 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/17/2009 Suspension GP 0.043 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.043 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/17/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/17/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/17/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/17/2009 Suspension GP 0.138 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.138 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/17/2009 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/17/2009 Suspension GP 0.137 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.137 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/17/2009 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/17/2009 Suspension GP 9.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 9.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/17/2009 Suspension GP 3.000 U 25.000 U 68.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 68.000 M PCBs SVOC 1336-36-3 Shintech TX 12/17/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/17/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/17/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/17/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/18/2009 Suspension GP 0.690 M 0.580 M 0.370 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.690 M 0.580 M 0.370 M Chloroethane VOC 75-00-3Shintech TX 12/18/2009 Suspension GP 0.035 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.035 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/18/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/18/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/18/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/18/2009 Suspension GP 0.132 M 0.614 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.132 M 0.614 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/18/2009 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/18/2009 Suspension GP 0.090 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.090 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/18/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/18/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/18/2009 Suspension GP 3.000 U 25.000 U 0.054 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.054 M PCBs SVOC 1336-36-3 Shintech TX 12/18/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/18/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/18/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/18/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/19/2009 Suspension GP 0.610 M 0.520 M 0.230 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.610 M 0.520 M 0.230 M Chloroethane VOC 75-00-3Shintech TX 12/19/2009 Suspension GP 0.029 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.029 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/19/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/19/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/19/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/19/2009 Suspension GP 0.099 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.099 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/19/2009 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/19/2009 Suspension GP 0.116 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.116 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/19/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/19/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/19/2009 Suspension GP 3.000 U 27.000 M 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 27.000 M 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/19/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/19/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/19/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/19/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/20/2009 Suspension GP 0.760 M 0.250 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.760 M 0.250 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/20/2009 Suspension GP 0.035 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.035 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/20/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/20/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/20/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/20/2009 Suspension GP 0.121 M 0.764 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.121 M 0.764 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/20/2009 Suspension GP NM 7.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 7.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/20/2009 Suspension GP 0.117 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.117 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/20/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/20/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/20/2009 Suspension GP 3.000 U 31.000 M 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 31.000 M 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/20/2009 Suspension GP 0.0005 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0005 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/20/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/20/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U

Suspension Conc. Data Agg 0900006480f92db5.xls 1 of 3Vinyl Institute 30 Day Concentration Database for Suspension Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column N for Revisions to Data Base Analyte Categor y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water

from Stripper Water

from Stripper Wet Resin

from Stripper Wet

Resin from Dry PVC

Resin from Dry

PVC Resin Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/20/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/21/2009 Suspension GP 0.770 M 0.700 M 0.250 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.770 M 0.700 M 0.250 M Chloroethane VOC 75-00-3Shintech TX 12/21/2009 Suspension GP 0.026 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.026 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/21/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/21/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/21/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/21/2009 Suspension GP 0.103 M 0.939 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.103 M 0.939 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/21/2009 Suspension GP NM 7.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 7.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/21/2009 Suspension GP 0.051 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.051 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/21/2009 Suspension GP 0.010 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.010 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/21/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/21/2009 Suspension GP 3.000 U 27.000 M 62.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 27.000 M 62.000 M PCBs SVOC 1336-36-3 Shintech TX 12/21/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/21/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/21/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/21/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/22/2009 Suspension GP 0.680 M 0.760 M 0.250 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.680 M 0.760 M 0.250 M Chloroethane VOC 75-00-3Shintech TX 12/22/2009 Suspension GP 0.048 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.048 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/22/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/22/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/22/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/22/2009 Suspension GP 0.180 M 0.595 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.180 M 0.595 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/22/2009 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/22/2009 Suspension GP 0.181 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.181 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 12/22/2009 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 12/22/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/22/2009 Suspension GP 3.000 U 26.000 M 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 26.000 M 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/22/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/22/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/22/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/22/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/23/2009 Suspension GP 0.690 M 0.660 M 0.390 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.690 M 0.660 M 0.390 M Chloroethane VOC 75-00-3Shintech TX 12/23/2009 Suspension GP 0.045 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.045 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/23/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/23/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/23/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/23/2009 Suspension GP 0.167 M 0.696 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.167 M 0.696 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/23/2009 Suspension GP NM 9.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 9.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/23/2009 Suspension GP 0.115 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.115 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/23/2009 Suspension GP 0.010 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.010 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/23/2009 Suspension GP 9.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 9.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/23/2009 Suspension GP 3.000 U 27.000 M 60.000 M Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 27.000 M 60.000 M PCBs SVOC 1336-36-3 Shintech TX 12/23/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/23/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/23/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/23/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/24/2009 Suspension GP 0.560 M 0.440 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.560 M 0.440 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/24/2009 Suspension GP 0.059 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.059 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/24/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/24/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/24/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/24/2009 Suspension GP 0.131 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.131 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/24/2009 Suspension GP NM 7.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 7.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/24/2009 Suspension GP 0.095 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.095 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/24/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/24/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/24/2009 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/24/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/24/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/24/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/24/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/25/2009 Suspension GP 0.810 M 0.410 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.810 M 0.410 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/25/2009 Suspension GP 0.037 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.037 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/25/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/25/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/25/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/25/2009 Suspension GP 0.100 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.100 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/25/2009 Suspension GP NM 5.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 5.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/25/2009 Suspension GP 0.091 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.091 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/25/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/25/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/25/2009 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/25/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/25/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/25/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/25/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/26/2009 Suspension GP 0.990 M 0.450 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.990 M 0.450 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/26/2009 Suspension GP 0.039 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.039 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/26/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/26/2009 Suspension GP 0.005 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.005 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/26/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/26/2009 Suspension GP 0.117 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.117 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/26/2009 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/26/2009 Suspension GP 0.138 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.138 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/26/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/26/2009 Suspension GP 7.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 7.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/26/2009 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/26/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U 1336-36-3 Shintech TX 12/26/2009 Suspension 1336-36-3 Shintech TX Suspension Acetaldehyde Aldehyde75-07-0Shintech TX 12/26/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/26/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/26/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 12/27/2009 Suspension GP 0.820 M 0.400 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.820 M 0.400 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 12/27/2009 Suspension GP 0.051 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.051 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 12/27/2009 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 12/27/2009 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 12/27/2009 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 12/27/2009 Suspension GP 0.095 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.095 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 12/27/2009 Suspension GP NM 3.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 3.00 M NM Acetophenone SVOC 98-86-2Shintech TX 12/27/2009 Suspension GP 0.127 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.127 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 12/27/2009 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 12/27/2009 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 12/27/2009 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 12/27/2009 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 12/27/2009 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 12/27/2009 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 12/27/2009 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/1/2010 Suspension GP 1.000 M 0.760 M 0.230 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 1.000 M 0.760 M 0.230 M Chloroethane VOC 75-00-3Shintech TX 1/1/2010 Suspension GP 0.047 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.047 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/1/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/1/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/1/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/1/2010 Suspension GP 0.119 M 0.837 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.119 M 0.837 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/1/2010 Suspension GP NM NM NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM NM NM Acetophenone SVOC 98-86-2Shintech TX 1/1/2010 Suspension GP 0.145 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.145 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 1/1/2010 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 1/1/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/1/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/1/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/1/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/1/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/1/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/2/2010 Suspension GP 0.890 M 0.360 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.890 M 0.360 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 1/2/2010 Suspension GP 0.061 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.061 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/2/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/2/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/2/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/2/2010 Suspension GP 0.172 M 0.893 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.172 M 0.893 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/2/2010 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/2/2010 Suspension GP 0.147 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.147 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/2/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/2/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/2/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/2/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/2/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/2/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/2/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/3/2010 Suspension GP 1.100 M 0.370 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 1.100 M 0.370 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 1/3/2010 Suspension GP 0.049 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.049 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/3/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/3/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/3/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/3/2010 Suspension GP 0.173 M 1.550 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.173 M 1.550 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/3/2010 Suspension GP NM 9.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 9.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/3/2010 Suspension GP 0.122 M 50.000 U 74.900 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.122 M 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX 1/3/2010 Suspension GP 0.020 U 50.000 U 74.900 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 74.900 U Methanol Alcohol 67-56-1 Shintech TX 1/3/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/3/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/3/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/3/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/3/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/3/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/4/2010 Suspension GP 0.940 M 0.120 M 0.630 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.940 M 0.120 M 0.630 M Chloroethane VOC 75-00-3Shintech TX 1/4/2010 Suspension GP 0.033 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.033 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/4/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/4/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/4/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/4/2010 Suspension GP 0.174 M 1.210 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.174 M 1.210 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/4/2010 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/4/2010 Suspension GP 0.165 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.165 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/4/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/4/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/4/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/4/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/4/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U

Suspension Conc. Data Agg 0900006480f92db5.xls 2 of 3Vinyl Institute 30 Day Concentration Database for Suspension Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column N for Revisions to Data Base Analyte Categor y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water

from Stripper Water

from Stripper Wet Resin

from Stripper Wet

Resin from Dry PVC

Resin from Dry

PVC Resin 1,3-butadiene VOC 106-99-0 Shintech TX 1/4/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/4/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/5/2010 Suspension GP 1.100 M 0.940 M 0.600 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 1.100 M 0.940 M 0.600 M Chloroethane VOC 75-00-3Shintech TX 1/5/2010 Suspension GP 0.040 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.040 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/5/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/5/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/5/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/5/2010 Suspension GP 0.157 M 1.390 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.157 M 1.390 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/5/2010 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/5/2010 Suspension GP 0.159 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.159 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/5/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/5/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/5/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/5/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/5/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/5/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/5/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/6/2010 Suspension GP 0.950 M 0.110 M 0.320 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.950 M 0.110 M 0.320 M Chloroethane VOC 75-00-3Shintech TX 1/6/2010 Suspension GP 0.043 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.043 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/6/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/6/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/6/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/6/2010 Suspension GP 0.163 M 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.163 M 0.500 U 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/6/2010 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/6/2010 Suspension GP 0.188 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.188 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/6/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/6/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/6/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/6/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/6/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/6/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/6/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/7/2010 Suspension GP 0.620 M 0.600 M 0.120 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.620 M 0.600 M 0.120 M Chloroethane VOC 75-00-3Shintech TX 1/7/2010 Suspension GP 0.038 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.038 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/7/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/7/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/7/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/7/2010 Suspension GP 0.141 M 0.888 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.141 M 0.888 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/7/2010 Suspension GP NM 6.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 6.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/7/2010 Suspension GP 0.103 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.103 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/7/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/7/2010 Suspension GP 9.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 9.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/7/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/7/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/7/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/7/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/7/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/8/2010 Suspension GP 0.250 M 0.480 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.250 M 0.480 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 1/8/2010 Suspension GP 0.027 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.027 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/8/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/8/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/8/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/8/2010 Suspension GP 0.109 M 1.070 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.109 M 1.070 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/8/2010 Suspension GP NM 7.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 7.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/8/2010 Suspension GP 0.107 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.107 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/8/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/8/2010 Suspension GP 9.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 9.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/8/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/8/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/8/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/8/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/8/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/9/2010 Suspension GP 0.190 M 0.580 M 0.030 U Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.190 M 0.580 M 0.030 U Chloroethane VOC 75-00-3Shintech TX 1/9/2010 Suspension GP 0.030 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.030 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/9/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/9/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/9/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/9/2010 Suspension GP 0.134 M 0.984 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.134 M 0.984 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/9/2010 Suspension GP NM 7.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 7.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/9/2010 Suspension GP 0.067 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.067 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/9/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/9/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/9/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U PCBs SVOC 1336-36-3 Shintech TX 1/9/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/9/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/9/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/9/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Formaldehyde Aldehyde50-00-0Shintech TX 1/10/2010 Suspension GP 0.990 M 0.770 M 0.290 M Formaldehyde Aldehyde50-00-0Shintech TX ##### Suspension

GP 0.990 M 0.770 M 0.290 M Chloroethane VOC 75-00-3Shintech TX 1/10/2010 Suspension GP 0.037 M 1.000 U 2.000 U Chloroethane VOC 75-00-3Shintech TX ##### Suspension

GP 0.037 M 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX 1/10/2010 Suspension GP 0.005 U 1.000 U 2.000 U Chloromethane (Methyl chloride) VOC 74-87-3Shintech TX ##### Suspension

GP 0.005 U 1.000 U 2.000 U Ethylene Dichloride VOC 107-06-2 Shintech TX 1/10/2010 Suspension GP 0.001 U 0.250 U 0.500 U 1,1-dichloroethene VOC 107-06-02 Shintech TX

##### Suspension

GP 0.001 U 0.250 U 0.500 U Vinyl acetate VOC 108-05-4 Shintech TX 1/10/2010 Suspension GP 0.010 U 0.500 U 1.000 U Vinyl acetate VOC 108-05-4 Shintech TX

##### Suspension

GP 0.010 U 0.500 U 1.000 U Vinyl chloride VOC 75-01-4Shintech TX 1/10/2010 Suspension GP 0.123 M 0.983 M 1.000 U Vinyl chloride VOC 75-01-4Shintech TX ##### Suspension

GP 0.123 M 0.983 M 1.000 U Vinyl chloride Method 107* VOC 75-01-4Shintech TX 1/10/2010 Suspension GP NM 8.00 M NM Vinyl chloride Method 107* VOC 75-01-4Shintech TX ##### Suspension

GP NM 8.00 M NM Acetophenone SVOC 98-86-2Shintech TX 1/10/2010 Suspension GP 0.132 M 50.000 U 50.000 U Acetophenone SVOC 98-86-2Shintech TX ##### Suspension

GP 0.132 M 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX 1/10/2010 Suspension GP 0.020 U 50.000 U 50.000 U Phenol SVOC 108-95-2 Shintech TX

##### Suspension

GP 0.020 U 50.000 U 50.000 U Methanol Alcohol 67-56-1 Shintech TX 1/10/2010 Suspension GP 8.000 M 5.000 U 0.010 U Methanol Alcohol 67-56-1 Shintech TX ##### Suspension

GP 8.000 M 5.000 U 0.010 U Total Petroleum Hydrocarbons TPH TPH Shintech TX 1/10/2010 Suspension GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons TPH TPH Shintech TX ##### Suspension

GP 3.000 U 25.000 U 0.050 U Total Petroleum Hydrocarbons Shintech TX 1/10/2010 Suspension Total Petroleum Hydrocarbons Shintech TX Suspension PCBs SVOC 1336-36-3 Shintech TX 1/10/2010 Suspension GP 0.0025 U 0.835 U 0.835 U PCBs SVOC 1336-36-3 Shintech TX

##### Suspension

GP 0.0025 U 0.835 U 0.835 U Acetaldehyde Aldehyde75-07-0Shintech TX 1/10/2010 Suspension GP 0.200 U 10.000 U 20.000 U Acetaldehyde Aldehyde75-07-0Shintech TX ##### Suspension

GP 0.200 U 10.000 U 20.000 U 1,3-butadiene VOC 106-99-0 Shintech TX 1/10/2010 Suspension GP 0.020 U 1.000 U 2.000 U 1,3-butadiene VOC 106-99-0 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX 1/10/2010 Suspension GP 0.020 U 1.000 U 2.000 U Vinyl bromide (Bromoethene) VOC 593-60-2 Shintech TX

##### Suspension

GP 0.020 U 1.000 U 2.000 U

Suspension Conc. Data Agg 0900006480f92db5.xls 3 of 3

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 12/14/2009Suspension Blending GP NM 22 U 12 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 12/14/2009Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 12/14/2009Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 12/14/2009Suspension Blending GP NM 0.43 U 0.25 U

2-Nitropropane VOC 79-46-9P1-Henry 12/14/2009Suspension Blending GP NM 1.1 U 0.62 U

Acetaldehyde Aldehyde75-07-0P1-Henry 12/14/2009Suspension Blending GP NM 50 U 50 U

Suspension Blending Conc. Data 0900006480f92db5.xls 1 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Acetonitrile VOC 75-05-8P1-Henry 12/14/2009Suspension Blending GP NM 4.3 U 2.5 U

Acetophenone SVOC 98-86-2 P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 12/14/2009Suspension Blending GP NM 2.2 U 1.2 U

Acrylonitrile VOC 107-13-1 P1-Henry 12/14/2009Suspension Blending GP NM 2.2 U 1.2 U

Allyl Chloride VOC 107-05-1 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Benzene VOC 71-43-2P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Bromoform VOC 75-25-2P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Bromomethane VOC 74-83-9P1-Henry 12/14/2009Suspension Blending GP NM 0.43 U 0.25 U

Carbon Disulfide VOC 75-15-0P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Chlorobenzene VOC 108-90-7 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Chloroethane VOC 75-00-3P1-Henry 12/14/2009Suspension Blending GP NM 2.5M 0.73 M

Chloroform VOC 67-66-3P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Chloromethane VOC 74-87-3P1-Henry 12/14/2009Suspension Blending GP NM 0.43 U 0.25 U

Chloroprene VOC 126-99-8 P1-Henry 12/14/2009Suspension Blending GP NM 1.1 U 0.62 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Dibenzofuran SVOC 132-64-9 P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 12/14/2009Suspension Blending GP NM 0.086 U 0.05 U

Formaldehyde Aldehyde50-00-0P1-Henry 12/14/2009Suspension Blending GP NM 50 U 50 U

Suspension Blending Conc. Data 0900006480f92db5.xls 2 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Hexachlorobenzene SVOC 118-74-1P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Iodomethane VOC 74-88-4P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Isophorone SVOC 78-59-1 P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

m,p-Xylene VOC 106-42-3 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Methanol Alcohol 67-56-1P1-Henry 12/14/2009Suspension Blending GP NM 50Q< 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Methylene Chloride VOC 75-09-2P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Naphthalene SVOC 91-20-3P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 12/14/2009Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Pentachlorophenol SVOC 87-86-5P1-Henry 12/14/2009Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Tetrachloroethene VOC 127-18-4 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Toluene VOC 108-88-3 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Suspension Blending Conc. Data 0900006480f92db5.xls 3 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Trichloroethene VOC 79-01-6P1-Henry 12/14/2009Suspension Blending GP NM 0.22 U 0.12 U

Vinyl Acetate VOC 108-05-4 P1-Henry 12/14/2009Suspension Blending GP NM 0.43 U 0.25 U

Vinyl Chloride VOC 75-01-4P1-Henry 12/14/2009Suspension Blending GP NM 1.7 M 0.44 M

Xylenes (Total) VOC 1330-20-7 P1-Henry 12/14/2009Suspension Blending GP NM 0.43 U 0.25 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 12/16/2009Suspension Blending GP NM 24 U 25 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 12/16/2009Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Suspension Blending Conc. Data 0900006480f92db5.xls 4 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 12/16/2009Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 12/16/2009Suspension Blending GP NM 0.48 U 0.5 U

2-Nitropropane VOC 79-46-9P1-Henry 12/16/2009Suspension Blending GP NM 1.2 U 1.2 U

Acetaldehyde Aldehyde75-07-0P1-Henry 12/16/2009Suspension Blending GP NM 50 U 50 U

Acetonitrile VOC 75-05-8P1-Henry 12/16/2009Suspension Blending GP NM 4.8 U 5 U

Acetophenone SVOC 98-86-2 P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 12/16/2009Suspension Blending GP NM 2.4 U 2.5 U

Acrylonitrile VOC 107-13-1 P1-Henry 12/16/2009Suspension Blending GP NM 2.4 U 2.5 U

Allyl Chloride VOC 107-05-1 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Benzene VOC 71-43-2P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Bromoform VOC 75-25-2P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Bromomethane VOC 74-83-9P1-Henry 12/16/2009Suspension Blending GP NM 0.48 U 0.5 U

Carbon Disulfide VOC 75-15-0P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Chlorobenzene VOC 108-90-7 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Chloroethane VOC 75-00-3P1-Henry 12/16/2009Suspension Blending GP NM 0.87 M 0.59M

Chloroform VOC 67-66-3P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Chloromethane VOC 74-87-3P1-Henry 12/16/2009Suspension Blending GP NM 0.48 U 0.5 U

Suspension Blending Conc. Data 0900006480f92db5.xls 5 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Chloroprene VOC 126-99-8 P1-Henry 12/16/2009Suspension Blending GP NM 1.2 U 1.2 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Dibenzofuran SVOC 132-64-9 P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 12/16/2009Suspension Blending GP NM 0.096 U 0.1 U

Formaldehyde Aldehyde50-00-0P1-Henry 12/16/2009Suspension Blending GP NM 50 U 50 U

Hexachlorobenzene SVOC 118-74-1P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Iodomethane VOC 74-88-4P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Isophorone SVOC 78-59-1 P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

m,p-Xylene VOC 106-42-3 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Methanol Alcohol 67-56-1P1-Henry 12/16/2009Suspension Blending GP NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Methylene Chloride VOC 75-09-2P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Naphthalene SVOC 91-20-3P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 12/16/2009Suspension Blending GP NM 1000 U 1000 U

Suspension Blending Conc. Data 0900006480f92db5.xls 6 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

o-Xylene VOC 95-47-6P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Pentachlorophenol SVOC 87-86-5P1-Henry 12/16/2009Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Tetrachloroethene VOC 127-18-4 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Toluene VOC 108-88-3 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Trichloroethene VOC 79-01-6P1-Henry 12/16/2009Suspension Blending GP NM 0.24 U 0.25 U

Vinyl Acetate VOC 108-05-4 P1-Henry 12/16/2009Suspension Blending GP NM 0.48 U 0.5 U

Vinyl Chloride VOC 75-01-4P1-Henry 12/16/2009Suspension Blending GP NM 1.4 M 0.5 U

Xylenes (Total) VOC 1330-20-7 P1-Henry 12/16/2009Suspension Blending GP NM 0.48 U 0.5 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Suspension Blending Conc. Data 0900006480f92db5.xls 7 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

1,2-Dichloropropane VOC 78-87-5P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 12/20/2009Suspension Blending GP NM 21 U 13 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 12/20/2009Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 12/20/2009Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 12/20/2009Suspension Blending GP NM 0.41 U 0.26 U

2-Nitropropane VOC 79-46-9P1-Henry 12/20/2009Suspension Blending GP NM 1 U 0.66 U

Acetaldehyde Aldehyde75-07-0P1-Henry 12/20/2009Suspension Blending GP NM 50 U 50 U

Acetonitrile VOC 75-05-8P1-Henry 12/20/2009Suspension Blending GP NM 4.1 U 2.6 U

Acetophenone SVOC 98-86-2 P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 12/20/2009Suspension Blending GP NM 2.1 U 1.3 U

Acrylonitrile VOC 107-13-1 P1-Henry 12/20/2009Suspension Blending GP NM 2.1 U 1.3 U

Allyl Chloride VOC 107-05-1 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Benzene VOC 71-43-2P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Bromoform VOC 75-25-2P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Bromomethane VOC 74-83-9P1-Henry 12/20/2009Suspension Blending GP NM 0.41 U 0.26 U

Carbon Disulfide VOC 75-15-0P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Suspension Blending Conc. Data 0900006480f92db5.xls 8 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Carbon Tetrachloride VOC 56-23-5P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Chlorobenzene VOC 108-90-7 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Chloroethane VOC 75-00-3P1-Henry 12/20/2009Suspension Blending GP NM 1.5M 0.54 M

Chloroform VOC 67-66-3P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Chloromethane VOC 74-87-3P1-Henry 12/20/2009Suspension Blending GP NM 0.41 U 0.26 U

Chloroprene VOC 126-99-8 P1-Henry 12/20/2009Suspension Blending GP NM 1 U 0.66 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Dibenzofuran SVOC 132-64-9 P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 12/20/2009Suspension Blending GP NM 0.082 U 0.053 U

Formaldehyde Aldehyde50-00-0P1-Henry 12/20/2009Suspension Blending GP NM 50 U 50 U

Hexachlorobenzene SVOC 118-74-1P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Iodomethane VOC 74-88-4P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Isophorone SVOC 78-59-1 P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

m,p-Xylene VOC 106-42-3 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Methanol Alcohol 67-56-1P1-Henry 12/20/2009Suspension Blending GP NM 50 U 50 U

Suspension Blending Conc. Data 0900006480f92db5.xls 9 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Methyl Methacrylate VOC 80-62-6P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Methylene Chloride VOC 75-09-2P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Naphthalene SVOC 91-20-3P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 12/20/2009Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Pentachlorophenol SVOC 87-86-5P1-Henry 12/20/2009Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Tetrachloroethene VOC 127-18-4 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Toluene VOC 108-88-3 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Trichloroethene VOC 79-01-6P1-Henry 12/20/2009Suspension Blending GP NM 0.21 U 0.13 U

Vinyl Acetate VOC 108-05-4 P1-Henry 12/20/2009Suspension Blending GP NM 0.41 U 0.26 U

Vinyl Chloride VOC 75-01-4P1-Henry 12/20/2009Suspension Blending GP NM 1.5M 0.15M

Xylenes (Total) VOC 1330-20-7 P1-Henry 12/20/2009Suspension Blending GP NM 0.41 U 0.26 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Suspension Blending Conc. Data 0900006480f92db5.xls 10 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

1,1-Dichloroethene VOC 75-35-4P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 1/6/2010Suspension Blending GP NM 23 U 13 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 1/6/2010Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 1/6/2010Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 1/6/2010Suspension Blending GP NM 0.45 U 0.26 U

2-Nitropropane VOC 79-46-9P1-Henry 1/6/2010Suspension Blending GP NM 1.1 U 0.66 U

Acetaldehyde Aldehyde75-07-0P1-Henry 1/6/2010Suspension Blending GP NM 50X< 50 U

Acetonitrile VOC 75-05-8P1-Henry 1/6/2010Suspension Blending GP NM 4.5 U 2.6 U

Acetophenone SVOC 98-86-2 P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 1/6/2010Suspension Blending GP NM 2.3 U 1.3 U

Acrylonitrile VOC 107-13-1 P1-Henry 1/6/2010Suspension Blending GP NM 2.3 U 1.3 U

Suspension Blending Conc. Data 0900006480f92db5.xls 11 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Allyl Chloride VOC 107-05-1 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Benzene VOC 71-43-2P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Bromoform VOC 75-25-2P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Bromomethane VOC 74-83-9P1-Henry 1/6/2010Suspension Blending GP NM 0.45 U 0.26 U

Carbon Disulfide VOC 75-15-0P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Chlorobenzene VOC 108-90-7 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Chloroethane VOC 75-00-3P1-Henry 1/6/2010Suspension Blending GP NM 1.9M 1.2 M

Chloroform VOC 67-66-3P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Chloromethane VOC 74-87-3P1-Henry 1/6/2010Suspension Blending GP NM 0.45 U 0.26 U

Chloroprene VOC 126-99-8 P1-Henry 1/6/2010Suspension Blending GP NM 1.1 U 0.66 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Dibenzofuran SVOC 132-64-9 P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 1/6/2010Suspension Blending GP NM 0.091 U 0.053 U

Formaldehyde Aldehyde50-00-0P1-Henry 1/6/2010Suspension Blending GP NM 50 U 50 U

Hexachlorobenzene SVOC 118-74-1P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Suspension Blending Conc. Data 0900006480f92db5.xls 12 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Iodomethane VOC 74-88-4P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Isophorone SVOC 78-59-1 P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

m,p-Xylene VOC 106-42-3 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Methanol Alcohol 67-56-1P1-Henry 1/6/2010Suspension Blending GP NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Methylene Chloride VOC 75-09-2P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Naphthalene SVOC 91-20-3P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 1/6/2010Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Pentachlorophenol SVOC 87-86-5P1-Henry 1/6/2010Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Tetrachloroethene VOC 127-18-4 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Toluene VOC 108-88-3 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Trichloroethene VOC 79-01-6P1-Henry 1/6/2010Suspension Blending GP NM 0.23 U 0.13 U

Vinyl Acetate VOC 108-05-4 P1-Henry 1/6/2010Suspension Blending GP NM 0.45 U 0.26 U

Vinyl Chloride VOC 75-01-4P1-Henry 1/6/2010Suspension Blending GP NM 1.3 M 0.52 M

Suspension Blending Conc. Data 0900006480f92db5.xls 13 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Xylenes (Total) VOC 1330-20-7 P1-Henry 1/6/2010Suspension Blending GP NM 0.45 U 0.26 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 F<

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 F<

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 F<

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 1/8/2010Suspension Blending GP NM 21 U 10 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 1/8/2010Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 1/8/2010Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 1/8/2010Suspension Blending GP NM 0.42 U 0.2 U

2-Nitropropane VOC 79-46-9P1-Henry 1/8/2010Suspension Blending GP NM 1 U 0.5 U

Suspension Blending Conc. Data 0900006480f92db5.xls 14 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Acetaldehyde Aldehyde75-07-0P1-Henry 1/8/2010Suspension Blending GP NM 50X< 50X<

Acetonitrile VOC 75-05-8P1-Henry 1/8/2010Suspension Blending GP NM 4.2 U 2 U

Acetophenone SVOC 98-86-2 P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 1/8/2010Suspension Blending GP NM 2.1 U 1 U

Acrylonitrile VOC 107-13-1 P1-Henry 1/8/2010Suspension Blending GP NM 2.1 U 1 U

Allyl Chloride VOC 107-05-1 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Benzene VOC 71-43-2P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Bromoform VOC 75-25-2P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Bromomethane VOC 74-83-9P1-Henry 1/8/2010Suspension Blending GP NM 0.42 U 0.2 U

Carbon Disulfide VOC 75-15-0P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Chlorobenzene VOC 108-90-7 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Chloroethane VOC 75-00-3P1-Henry 1/8/2010Suspension Blending GP NM 4.1 M 0.7 M

Chloroform VOC 67-66-3P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Chloromethane VOC 74-87-3P1-Henry 1/8/2010Suspension Blending GP NM 0.42 U 0.2 U

Chloroprene VOC 126-99-8 P1-Henry 1/8/2010Suspension Blending GP NM 1 U 0.5 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Dibenzofuran SVOC 132-64-9 P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 1/8/2010Suspension Blending GP NM 0.083 U 0.04 U

Suspension Blending Conc. Data 0900006480f92db5.xls 15 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Formaldehyde Aldehyde50-00-0P1-Henry 1/8/2010Suspension Blending GP NM 50X< 50X<

Hexachlorobenzene SVOC 118-74-1P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Iodomethane VOC 74-88-4P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Isophorone SVOC 78-59-1 P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 F<

m,p-Xylene VOC 106-42-3 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Methanol Alcohol 67-56-1P1-Henry 1/8/2010Suspension Blending GP NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Methylene Chloride VOC 75-09-2P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Naphthalene SVOC 91-20-3P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 1/8/2010Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Pentachlorophenol SVOC 87-86-5P1-Henry 1/8/2010Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Tetrachloroethene VOC 127-18-4 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Suspension Blending Conc. Data 0900006480f92db5.xls 16 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Toluene VOC 108-88-3 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Trichloroethene VOC 79-01-6P1-Henry 1/8/2010Suspension Blending GP NM 0.21 U 0.1 U

Vinyl Acetate VOC 108-05-4 P1-Henry 1/8/2010Suspension Blending GP NM 0.42 U 0.2 U

Vinyl Chloride VOC 75-01-4P1-Henry 1/8/2010Suspension Blending GP NM 0.42 M 0.28M

Xylenes (Total) VOC 1330-20-7 P1-Henry 1/8/2010Suspension Blending GP NM 0.42 U 0.2 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 1/9/2010Suspension Blending GP NM 19 U 11 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 1/9/2010Suspension Blending GP NM 5000 U 5000 U

Suspension Blending Conc. Data 0900006480f92db5.xls 17 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 1/9/2010Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 1/9/2010Suspension Blending GP NM 0.38 U 0.22 U

2-Nitropropane VOC 79-46-9P1-Henry 1/9/2010Suspension Blending GP NM 0.96 U 0.54 U

Acetaldehyde Aldehyde75-07-0P1-Henry 1/9/2010Suspension Blending GP NM 50 U 50 U

Acetonitrile VOC 75-05-8P1-Henry 1/9/2010Suspension Blending GP NM 3.8 U 2.2 U

Acetophenone SVOC 98-86-2 P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 1/9/2010Suspension Blending GP NM 1.9 U 1.1 U

Acrylonitrile VOC 107-13-1 P1-Henry 1/9/2010Suspension Blending GP NM 1.9 U 1.1 U

Allyl Chloride VOC 107-05-1 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Benzene VOC 71-43-2P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Bromoform VOC 75-25-2P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Bromomethane VOC 74-83-9P1-Henry 1/9/2010Suspension Blending GP NM 0.38 U 0.22 U

Carbon Disulfide VOC 75-15-0P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Chlorobenzene VOC 108-90-7 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Chloroethane VOC 75-00-3P1-Henry 1/9/2010Suspension Blending GP NM 1.6 M 0.88M

Chloroform VOC 67-66-3P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Suspension Blending Conc. Data 0900006480f92db5.xls 18 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Chloromethane VOC 74-87-3P1-Henry 1/9/2010Suspension Blending GP NM 0.38 U 0.22 U

Chloroprene VOC 126-99-8 P1-Henry 1/9/2010Suspension Blending GP NM 0.96 U 0.54 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Dibenzofuran SVOC 132-64-9 P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 1/9/2010Suspension Blending GP NM 0.077 U 0.043 U

Formaldehyde Aldehyde50-00-0P1-Henry 1/9/2010Suspension Blending GP NM 50 U 50 U

Hexachlorobenzene SVOC 118-74-1P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Iodomethane VOC 74-88-4P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Isophorone SVOC 78-59-1 P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

m,p-Xylene VOC 106-42-3 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Methanol Alcohol 67-56-1P1-Henry 1/9/2010Suspension Blending GP NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Methylene Chloride VOC 75-09-2P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Naphthalene SVOC 91-20-3P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

Suspension Blending Conc. Data 0900006480f92db5.xls 19 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Nitrobenzene SVOC 98-95-3P1-Henry 1/9/2010Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Pentachlorophenol SVOC 87-86-5P1-Henry 1/9/2010Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Tetrachloroethene VOC 127-18-4 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Toluene VOC 108-88-3 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Trichloroethene VOC 79-01-6P1-Henry 1/9/2010Suspension Blending GP NM 0.19 U 0.11 U

Vinyl Acetate VOC 108-05-4 P1-Henry 1/9/2010Suspension Blending GP NM 0.38 U 0.22 U

Vinyl Chloride VOC 75-01-4P1-Henry 1/9/2010Suspension Blending GP NM 0.72 M 0.49M

Xylenes (Total) VOC 1330-20-7 P1-Henry 1/9/2010Suspension Blending GP NM 0.38 U 0.22 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Suspension Blending Conc. Data 0900006480f92db5.xls 20 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 1/11/2010Suspension Blending GP NM 18 U 11 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 1/11/2010Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 1/11/2010Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 1/11/2010Suspension Blending GP NM 0.36 U 0.22 U

2-Nitropropane VOC 79-46-9P1-Henry 1/11/2010Suspension Blending GP NM 0.89 U 0.54 U

Acetaldehyde Aldehyde75-07-0P1-Henry 1/11/2010Suspension Blending GP NM 50 U 50 U

Acetonitrile VOC 75-05-8P1-Henry 1/11/2010Suspension Blending GP NM 3.6 U 2.2 U

Acetophenone SVOC 98-86-2 P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 1/11/2010Suspension Blending GP NM 1.8 U 1.1 U

Acrylonitrile VOC 107-13-1 P1-Henry 1/11/2010Suspension Blending GP NM 1.8 U 1.1 U

Allyl Chloride VOC 107-05-1 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Benzene VOC 71-43-2P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Bromoform VOC 75-25-2P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Bromomethane VOC 74-83-9P1-Henry 1/11/2010Suspension Blending GP NM 0.36 U 0.22 U

Suspension Blending Conc. Data 0900006480f92db5.xls 21 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Carbon Disulfide VOC 75-15-0P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Chlorobenzene VOC 108-90-7 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Chloroethane VOC 75-00-3P1-Henry 1/11/2010Suspension Blending GP NM 2.9M 0.89M

Chloroform VOC 67-66-3P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Chloromethane VOC 74-87-3P1-Henry 1/11/2010Suspension Blending GP NM 0.36 U 0.22 U

Chloroprene VOC 126-99-8 P1-Henry 1/11/2010Suspension Blending GP NM 0.89 U 0.54 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Dibenzofuran SVOC 132-64-9 P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 1/11/2010Suspension Blending GP NM 0.071 U 0.043 U

Formaldehyde Aldehyde50-00-0P1-Henry 1/11/2010Suspension Blending GP NM 50 U 50 U

Hexachlorobenzene SVOC 118-74-1P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Iodomethane VOC 74-88-4P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Isophorone SVOC 78-59-1 P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

m,p-Xylene VOC 106-42-3 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Suspension Blending Conc. Data 0900006480f92db5.xls 22 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Methanol Alcohol 67-56-1P1-Henry 1/11/2010Suspension Blending GP NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Methylene Chloride VOC 75-09-2P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Naphthalene SVOC 91-20-3P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 1/11/2010Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Pentachlorophenol SVOC 87-86-5P1-Henry 1/11/2010Suspension Blending GP NM NM NM

Styrene VOC 100-42-5 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Tetrachloroethene VOC 127-18-4 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Toluene VOC 108-88-3 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Trichloroethene VOC 79-01-6P1-Henry 1/11/2010Suspension Blending GP NM 0.18 U 0.11 U

Vinyl Acetate VOC 108-05-4 P1-Henry 1/11/2010Suspension Blending GP NM 0.36 U 0.22 U

Vinyl Chloride VOC 75-01-4P1-Henry 1/11/2010Suspension Blending GP NM 2.7 M 0.22 M

Xylenes (Total) VOC 1330-20-7 P1-Henry 1/11/2010Suspension Blending GP NM 0.36 U 0.22 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Suspension Blending Conc. Data 0900006480f92db5.xls 23 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

1,1-Dichloroethane VOC 75-34-3P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 1/12/2010Suspension Blending GP NM 25 U 11 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 1/12/2010Suspension Blending GP NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 1/12/2010Suspension Blending GP NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 1/12/2010Suspension Blending GP NM 0.5 U 0.22 U

2-Nitropropane VOC 79-46-9P1-Henry 1/12/2010Suspension Blending GP NM 1.2 U 0.54 U

Acetaldehyde Aldehyde75-07-0P1-Henry 1/12/2010Suspension Blending GP NM 50 U 50 U

Acetonitrile VOC 75-05-8P1-Henry 1/12/2010Suspension Blending GP NM 5 U 2.2 U

Acetophenone SVOC 98-86-2 P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 1/12/2010Suspension Blending GP NM 2.5 U 1.1 U

Suspension Blending Conc. Data 0900006480f92db5.xls 24 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Acrylonitrile VOC 107-13-1 P1-Henry 1/12/2010Suspension Blending GP NM 2.5 U 1.1 U

Allyl Chloride VOC 107-05-1 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Benzene VOC 71-43-2P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Bromoform VOC 75-25-2P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Bromomethane VOC 74-83-9P1-Henry 1/12/2010Suspension Blending GP NM 0.5 U 0.22 U

Carbon Disulfide VOC 75-15-0P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Chlorobenzene VOC 108-90-7 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Chloroethane VOC 75-00-3P1-Henry 1/12/2010Suspension Blending GP NM 3.5M 0.71 M

Chloroform VOC 67-66-3P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Chloromethane VOC 74-87-3P1-Henry 1/12/2010Suspension Blending GP NM 0.5 U 0.22 U

Chloroprene VOC 126-99-8 P1-Henry 1/12/2010Suspension Blending GP NM 1.2 U 0.54 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Dibenzofuran SVOC 132-64-9 P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Ethylbenzene VOC 100-41-4 P1-Henry 1/12/2010Suspension Blending GP NM 0.1 U 0.043 U

Formaldehyde Aldehyde50-00-0P1-Henry 1/12/2010Suspension Blending GP NM 50 U 50 U

Hexachlorobenzene SVOC 118-74-1P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Suspension Blending Conc. Data 0900006480f92db5.xls 25 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Hexane VOC 110-54-3 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Iodomethane VOC 74-88-4P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Isophorone SVOC 78-59-1 P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

m,p-Xylene VOC 106-42-3 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Methanol Alcohol 67-56-1P1-Henry 1/12/2010Suspension Blending GP NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Methylene Chloride VOC 75-09-2P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Naphthalene SVOC 91-20-3P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 1/12/2010Suspension Blending GP NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Pentachlorophenol SVOC 87-86-5P1-Henry 1/12/2010Suspension Blending GP NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Tetrachloroethene VOC 127-18-4 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Toluene VOC 108-88-3 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Trichloroethene VOC 79-01-6P1-Henry 1/12/2010Suspension Blending GP NM 0.25 U 0.11 U

Vinyl Acetate VOC 108-05-4 P1-Henry 1/12/2010Suspension Blending GP NM 0.5 U 0.22 U

Suspension Blending Conc. Data 0900006480f92db5.xls 26 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Vinyl Chloride VOC 75-01-4P1-Henry 1/12/2010Suspension Blending GP NM 2.2 M 0.49M

Xylenes (Total) VOC 1330-20-7 P1-Henry 1/12/2010Suspension Blending GP NM 0.5 U 0.22 U

1,1,1-Trichloroethane VOC 71-55-6P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,1,2,2-Tetrachloroethane VOC 79-34-5P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 F<

1,1,2-Trichloroethane VOC 79-00-5P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,1-Dichloroethane VOC 75-34-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,1-Dichloroethene VOC 75-35-4P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 F<

1,2-Dibromo-3-chloropropane VOC 96-12-8P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 F<

1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,2-Dichloropropane VOC 78-87-5P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

1,4-Dioxane VOC 123-91-1 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 21 U 14 U

2,4,5-Trichlorophenol SVOC 95-95-4P1-Henry 1/21/2010Suspension Blending GP/HMW NM 5000 U 5000 U

2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

2,4-Dinitrophenol SVOC 51-28-5P1-Henry 1/21/2010Suspension Blending GP/HMW NM 5000 U 5000 U

2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

MEK VOC 78-93-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.42 U 0.28 U

Suspension Blending Conc. Data 0900006480f92db5.xls 27 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

2-Nitropropane VOC 79-46-9P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1 U 0.69 U

Acetaldehyde Aldehyde75-07-0P1-Henry 1/21/2010Suspension Blending GP/HMW NM 50 U 50 U

Acetonitrile VOC 75-05-8P1-Henry 1/21/2010Suspension Blending GP/HMW NM 4.2 U 2.8 U

Acetophenone SVOC 98-86-2 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Acrolein VOC 107-02-8 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 2.1 U 1.4 U

Acrylonitrile VOC 107-13-1 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 2.1 U 1.4 U

Allyl Chloride VOC 107-05-1 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Benzene VOC 71-43-2P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Bromoform VOC 75-25-2P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Bromomethane VOC 74-83-9P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.42 U 0.28 U

Carbon Disulfide VOC 75-15-0P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Carbon Tetrachloride VOC 56-23-5P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Chlorobenzene VOC 108-90-7 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Chloroethane VOC 75-00-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 3.2 M 0.95M

Chloroform VOC 67-66-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Chloromethane VOC 74-87-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.42 U 0.28 U

Chloroprene VOC 126-99-8 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1 U 0.69 U

cis-1,3-Dichloropropene VOC 10061-01-5 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Dibenzofuran SVOC 132-64-9 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Suspension Blending Conc. Data 0900006480f92db5.xls 28 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Ethylbenzene VOC 100-41-4 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.083 U 0.056 U

Formaldehyde Aldehyde50-00-0P1-Henry 1/21/2010Suspension Blending GP/HMW NM 50X< 50X<

Hexachlorobenzene SVOC 118-74-1P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Hexachlorobutadiene SVOC 87-68-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Hexachloroethane SVOC 67-72-1P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Hexane VOC 110-54-3 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Iodomethane VOC 74-88-4P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Isophorone SVOC 78-59-1 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Isopropylbenzene VOC 98-82-8P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 F<

m,p-Xylene VOC 106-42-3 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Methanol Alcohol 67-56-1P1-Henry 1/21/2010Suspension Blending GP/HMW NM 50 U 50 U

Methyl Methacrylate VOC 80-62-6P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Methylene Chloride VOC 75-09-2P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Naphthalene SVOC 91-20-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

Nitrobenzene SVOC 98-95-3P1-Henry 1/21/2010Suspension Blending GP/HMW NM 1000 U 1000 U

o-Xylene VOC 95-47-6P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Pentachlorophenol SVOC 87-86-5P1-Henry 1/21/2010Suspension Blending GP/HMW NM 5000 U 5000 U

Styrene VOC 100-42-5 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Suspension Blending Conc. Data 0900006480f92db5.xls 29 of 30

## Vinyl Institute 30 Day Concentration Database for Suspension Blending Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analy te Analy te Categor
y CAS No. Reporting Plant Sample

Date Resin Type Resin Grade Water from Stripper Bottoms, mg/L Water from

Stripper Bottoms Measureme nt Type Wet

Resin from Stripper Bottoms , ppm Wet Resin

from Stripper Bottoms, Measureme nt Type Dry

PVC Resin from Dryer, ppm Dry

PVC Resin from Dryer Measureme nt Type

Tetrachloroethene VOC 127-18-4 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Toluene VOC 108-88-3 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Trichloroethene VOC 79-01-6P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.21 U 0.14 U

Vinyl Acetate VOC 108-05-4 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.42 U 0.28 U

Vinyl Chloride VOC 75-01-4P1-Henry 1/21/2010Suspension Blending GP/HMW NM 2.7 M 0.16 M

Xylenes (Total) VOC 1330-20-7 P1-Henry 1/21/2010Suspension Blending GP/HMW NM 0.42 U 0.28 U

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/14/2009Suspension Blending HMW NM 7.11 M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/16/2009Suspension Blending HMW NM 10.08M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/20/2009Suspension Blending HMW NM 4.25M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/6/2010Suspension Blending HMW NM 12.85M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/8/2010Suspension Blending HMW NM 0.02 U NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/9/2010Suspension Blending HMW NM 5.98M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/11/2010Suspension Blending HMW NM 12.2 M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/12/2010Suspension Blending HMW NM 13.13 M NM

Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/21/2010Suspension Blending GP/HMW NM 11.51 M NM

Suspension Blending Conc. Data 0900006480f92db5.xls 30 of 30Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/12/2010Dispersion GP 0.08U 0.88U 0.33U Notes: 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/12/2010Dispersion GP 0.07U 0.79M 0.17U Chloroethane VOC 75-00-3 FPC DE 1/12/2010Dispersion GP 0.07U 6.25M 0.87M Chloroform VOC 67-66-3 FPC DE 1/12/2010Dispersion GP 0.05U 0.42 U 0.16U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/12/2010Dispersion GP 0.06U 0.22 U 0.08U Chloroprene VOC 126-99-8 FPC DE 1/12/2010Dispersion GP 0.19U 1.50U 0.56U Vinyl acetate VOC 108-05-4 FPC DE 1/12/2010Dispersion GP 0.25U 1.40U 0.53U Vinyl Bromide VOC 593-60-2 FPC DE 1/12/2010Dispersion GP 0.02 U 0.18U 0.07U Vinyl chloride VOC 75-01-4 FPC DE 1/12/2010Dispersion GP 0.09U 153.00M 1.85M Hydroquinone SVOC 123-31-9 FPC DE 1/12/2010Dispersion GP 0.10U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/12/2010Dispersion GP 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/12/2010Dispersion GP 3.40U 11.00U 9.50U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/12/2010Dispersion GP 0.19M 10.60M 2.62M Formaldehyde Aldehyd 50-00-0 FPC DE 1/12/2010Dispersion GP 0.01 U 0.25M 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/13/2010Dispersion GP 0.40U 0.90U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/13/2010Dispersion GP 0.33U 1.15M 0.91 M Chloroethane VOC 75-00-3 FPC DE 1/13/2010Dispersion GP 0.37U 10.10M 3.00M Chloroform VOC 67-66-3 FPC DE 1/13/2010Dispersion GP 0.23U 0.43U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/13/2010Dispersion GP 0.29U 0.36M 0.17U Chloroprene VOC 126-99-8 FPC DE 1/13/2010Dispersion GP 0.93U 1.50U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 1/13/2010Dispersion GP 1.30U 1.40U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/13/2010Dispersion GP 0.10U 0.18U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 1/13/2010Dispersion GP 0.44U 216.00M 6.53M Hydroquinone SVOC 123-31-9 FPC DE 1/13/2010Dispersion GP 0.10U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/13/2010Dispersion GP 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/13/2010Dispersion GP 3.40U 5.90U 1.60U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/13/2010Dispersion GP 0.74M 9.29M 3.48M Formaldehyde Aldehyd 50-00-0 FPC DE 1/13/2010Dispersion GP 0.01 U 0.71 M 0.16M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/14/2010Dispersion GP 0.10U 0.43U 1.30U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/14/2010Dispersion GP 0.08U 1.03M 0.69U Chloroethane VOC 75-00-3 FPC DE 1/14/2010Dispersion GP 0.09U 5.81 M 2.30M Chloroform VOC 67-66-3 FPC DE 1/14/2010Dispersion GP 0.06U 0.21 U 0.64U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/14/2010Dispersion GP 0.07U 0.21 M 0.33U Chloroprene VOC 126-99-8 FPC DE 1/14/2010Dispersion GP 0.23U 0.73U 2.20U Vinyl acetate VOC 108-05-4 FPC DE 1/14/2010Dispersion GP 0.32 U 0.69U 2.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/14/2010Dispersion GP 0.03U 0.09U 0.27U Vinyl chloride VOC 75-01-4 FPC DE 1/14/2010Dispersion GP 0.11 U 155.00M 4.10M Hydroquinone SVOC 123-31-9 FPC DE 1/14/2010Dispersion GP 0.10U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/14/2010Dispersion GP 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/14/2010Dispersion GP 3.40U 11.00U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/14/2010Dispersion GP 0.74M 11.60M 3.39M Formaldehyde Aldehyd 50-00-0 FPC DE 1/14/2010Dispersion GP 0.01 U 0.46M 0.12M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/15/2010Dispersion GP/HMW 0.04U 0.96U 0.33U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/15/2010Dispersion GP/HMW 0.03U 0.68M 0.57M Chloroethane VOC 75-00-3 FPC DE 1/15/2010Dispersion GP/HMW 0.09M 6.10M 1.75M Chloroform VOC 67-66-3 FPC DE 1/15/2010Dispersion GP/HMW 0.02 U 0.46U 0.16U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/15/2010Dispersion GP/HMW 0.03U 0.24U 0.08U Chloroprene VOC 126-99-8 FPC DE 1/15/2010Dispersion GP/HMW 0.09U 1.60U 0.56U Vinyl acetate VOC 108-05-4 FPC DE 1/15/2010Dispersion GP/HMW 0.13U 1.50U 0.53U Vinyl Bromide VOC 593-60-2 FPC DE 1/15/2010Dispersion GP/HMW 0.01 U 0.20U 0.07U Vinyl chloride VOC 75-01-4 FPC DE 1/15/2010Dispersion GP/HMW 1.82M 60.20M 1.46M Hydroquinone SVOC 123-31-9 FPC DE 1/15/2010Dispersion GP/HMW 0.10U 2.60U 20.00U Phenol SVOC 108-95-2 FPC DE 1/15/2010Dispersion GP/HMW 0.01 U 1.30U 9.60U Methanol Alcohol 67-56-1 FPC DE 1/15/2010Dispersion GP/HMW 3.40U 12.00U 16.00U (1) Removed Formosa VACO Copolymer data to separate tab - 7-21- (2) Removed Formosa DE comingled VACO and Dispersion data from data base - 7-21-11

(3) There is an anomoly in the values for PolyOne Pedricktow n vinyl chloride based on M8260B

on December 5, 2009. It appears the results for wet

Dispersion Conc. Data Agg 0900006480f92db5.xls 1 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Acetaldehyde Aldehyd 75-07-0 FPC DE 1/15/2010Dispersion GP/HMW 1.23M 6.69M 2.21 M Formaldehyde Aldehyd 50-00-0 FPC DE 1/15/2010Dispersion GP/HMW 0.01 U 0.14U 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/16/2010Dispersion HMW 0.04U 0.51 U 0.33U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/16/2010Dispersion HMW 0.03U 0.65M 0.48M Chloroethane VOC 75-00-3 FPC DE 1/16/2010Dispersion HMW 0.05M 10.20M 1.55M Chloroform VOC 67-66-3 FPC DE 1/16/2010Dispersion HMW 0.02 U 0.24U 0.16U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/16/2010Dispersion HMW 0.03U 0.13U 0.08U Chloroprene VOC 126-99-8 FPC DE 1/16/2010Dispersion HMW 0.09U 0.85U 0.56U Vinyl acetate VOC 108-05-4 FPC DE 1/16/2010Dispersion HMW 0.13U 0.81 U 0.53U Vinyl Bromide VOC 593-60-2 FPC DE 1/16/2010Dispersion HMW 0.01 U 0.10U 0.07U Vinyl chloride VOC 75-01-4 FPC DE 1/16/2010Dispersion HMW 1.04M 150.00M 1.14M Hydroquinone SVOC 123-31-9 FPC DE 1/16/2010Dispersion HMW 0.10U 2.70U 2.10U Phenol SVOC 108-95-2 FPC DE 1/16/2010Dispersion HMW 0.01 U 1.30U 1.10U Methanol Alcohol 67-56-1 FPC DE 1/16/2010Dispersion HMW 0.03U 0.12 U 0.15U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/16/2010Dispersion HMW 3.10M 12.90M 3.13M Formaldehyde Aldehyd 50-00-0 FPC DE 1/16/2010Dispersion HMW 0.06M 0.21 M 0.25M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/17/2010Dispersion HMW 0.04U 1.00U 0.33U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/17/2010Dispersion HMW 0.03U 0.57M 0.35M Chloroethane VOC 75-00-3 FPC DE 1/17/2010Dispersion HMW 0.05M 14.40M 1.29M Chloroform VOC 67-66-3 FPC DE 1/17/2010Dispersion HMW 0.02 U 0.49U 0.16U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/17/2010Dispersion HMW 0.03U 0.25U 0.08U Chloroprene VOC 126-99-8 FPC DE 1/17/2010Dispersion HMW 0.09U 1.70U 0.56U Vinyl acetate VOC 108-05-4 FPC DE 1/17/2010Dispersion HMW 0.13U 1.60U 0.53U Vinyl Bromide VOC 593-60-2 FPC DE 1/17/2010Dispersion HMW 0.01 U 0.21 U 0.07U Vinyl chloride VOC 75-01-4 FPC DE 1/17/2010Dispersion HMW 0.77M 189.00M 0.81 M Hydroquinone SVOC 123-31-9 FPC DE 1/17/2010Dispersion HMW 0.10U 14.00U 2.10U Phenol SVOC 108-95-2 FPC DE 1/17/2010Dispersion HMW 0.01 U 6.70U 1.10U Methanol Alcohol 67-56-1 FPC DE 1/17/2010Dispersion HMW 0.03U 0.12 U 0.16U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/17/2010Dispersion HMW 9.72M 23.80M 1.89M Formaldehyde Aldehyd 50-00-0 FPC DE 1/17/2010Dispersion HMW 0.01 U 0.28M 0.28M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/18/2010Dispersion HMW 0.02 U 0.99U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/18/2010Dispersion HMW 0.02 U 0.59M 0.35U Chloroethane VOC 75-00-3 FPC DE 1/18/2010Dispersion HMW 0.09M 12.40M 1.59M Chloroform VOC 67-66-3 FPC DE 1/18/2010Dispersion HMW 0.01 U 0.48U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/18/2010Dispersion HMW 0.01 U 0.25U 0.17U Chloroprene VOC 126-99-8 FPC DE 1/18/2010Dispersion HMW 0.05U 1.70U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 1/18/2010Dispersion HMW 0.06U 1.60U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/18/2010Dispersion HMW 0.01 U 0.20U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 1/18/2010Dispersion HMW 1.29M 176.00M 1.26M Hydroquinone SVOC 123-31-9 FPC DE 1/18/2010Dispersion HMW 0.10U 2.70U 11.00U Phenol SVOC 108-95-2 FPC DE 1/18/2010Dispersion HMW 0.01 U 1.30U 5.30U Methanol Alcohol 67-56-1 FPC DE 1/18/2010Dispersion HMW 3.40U 5.90U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/18/2010Dispersion HMW 2.37M 14.10M 1.72M Formaldehyde Aldehyd 50-00-0 FPC DE 1/18/2010Dispersion HMW 0.01 U 0.14U 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/19/2010Dispersion HMW 0.02 U 0.10U 0.13U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/19/2010Dispersion HMW 0.02 U 0.36M 0.33M Chloroethane VOC 75-00-3 FPC DE 1/19/2010Dispersion HMW 0.08M 4.38M 0.54M Chloroform VOC 67-66-3 FPC DE 1/19/2010Dispersion HMW 0.01 U 0.05U 0.06U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/19/2010Dispersion HMW 0.01 U 0.16M 0.03U Chloroprene VOC 126-99-8 FPC DE 1/19/2010Dispersion HMW 0.05U 0.17U 0.22 U Vinyl acetate VOC 108-05-4 FPC DE 1/19/2010Dispersion HMW 0.06U 0.16U 0.21 U Vinyl Bromide VOC 593-60-2 FPC DE 1/19/2010Dispersion HMW 0.01 U 0.02 U 0.03U Vinyl chloride VOC 75-01-4 FPC DE 1/19/2010Dispersion HMW 1.08M 149.00M 1.16M Hydroquinone SVOC 123-31-9 FPC DE 1/19/2010Dispersion HMW 0.50U 13.00U 2.10U

Dispersion Conc. Data Agg 0900006480f92db5.xls 2 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Phenol SVOC 108-95-2 FPC DE 1/19/2010Dispersion HMW 0.06U 6.50U 1.10U Methanol Alcohol 67-56-1 FPC DE 1/19/2010Dispersion HMW 3.40U 9.80U 7.40U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/19/2010Dispersion HMW 3.60M 16.90M 2.52M Formaldehyde Aldehyd 50-00-0 FPC DE 1/19/2010Dispersion HMW 0.01 U 0.14U 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/20/2010Dispersion HMW 0.04U 0.88U 0.33U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/20/2010Dispersion HMW 0.03U 0.89M 0.40M Chloroethane VOC 75-00-3 FPC DE 1/20/2010Dispersion HMW 0.05M 16.30M 2.01 M Chloroform VOC 67-66-3 FPC DE 1/20/2010Dispersion HMW 0.02 U 0.42 U 0.16U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/20/2010Dispersion HMW 0.03U 0.22 U 0.08U Chloroprene VOC 126-99-8 FPC DE 1/20/2010Dispersion HMW 0.09U 1.50U 0.56U Vinyl acetate VOC 108-05-4 FPC DE 1/20/2010Dispersion HMW 0.13U 1.40U 0.53U Vinyl Bromide VOC 593-60-2 FPC DE 1/20/2010Dispersion HMW 0.01 U 0.18U 0.07U Vinyl chloride VOC 75-01-4 FPC DE 1/20/2010Dispersion HMW 0.85M 235.00M 1.99M Hydroquinone SVOC 123-31-9 FPC DE 1/20/2010Dispersion HMW 0.50U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/20/2010Dispersion HMW 0.06U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/20/2010Dispersion HMW 0.03U 9.10U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/20/2010Dispersion HMW 4.82M 12.80M 1.63M Formaldehyde Aldehyd 50-00-0 FPC DE 1/20/2010Dispersion HMW 0.01 U 0.15M 0.16M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/29/2010Dispersion GP 0.04U 1.50U 0.51 U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/29/2010Dispersion GP 0.03U 1.12M 0.26U Chloroethane VOC 75-00-3 FPC DE 1/29/2010Dispersion GP 0.06M 19.60M 0.77U Chloroform VOC 67-66-3 FPC DE 1/29/2010Dispersion GP 0.02 U 0.74U 0.24U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/29/2010Dispersion GP 0.03U 0.85M 0.13U Chloroprene VOC 126-99-8 FPC DE 1/29/2010Dispersion GP 0.09U 2.60U 0.85U Vinyl acetate VOC 108-05-4 FPC DE 1/29/2010Dispersion GP 0.13U 2.40U 52.60M Vinyl Bromide VOC 593-60-2 FPC DE 1/29/2010Dispersion GP 0.01 U 0.32 U 0.10U Vinyl chloride VOC 75-01-4 FPC DE 1/29/2010Dispersion GP 1.14M 319.00M 0.81 M Hydroquinone SVOC 123-31-9 FPC DE 1/29/2010Dispersion GP 1.00U 30.00U 22.00U Phenol SVOC 108-95-2 FPC DE 1/29/2010Dispersion GP 0.12 U 15.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/29/2010Dispersion GP 3.40U 10.00U 8.00U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/29/2010Dispersion GP 2.89M 47.00M 6.03M Formaldehyde Aldehyd 50-00-0 FPC DE 1/29/2010Dispersion GP 0.01 U 0.37M 0.24M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/30/2010Dispersion GP 0.40U 0.54U 0.50U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/30/2010Dispersion GP 0.33U 0.45M 0.26U Chloroethane VOC 75-00-3 FPC DE 1/30/2010Dispersion GP 0.37U 7.29M 0.75U Chloroform VOC 67-66-3 FPC DE 1/30/2010Dispersion GP 0.23U 0.26U 0.24U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/30/2010Dispersion GP 0.29U 0.28M 0.12 U Chloroprene VOC 126-99-8 FPC DE 1/30/2010Dispersion GP 0.93U 0.91 U 0.84U Vinyl acetate VOC 108-05-4 FPC DE 1/30/2010Dispersion GP 1.30U 0.86U 0.79U Vinyl Bromide VOC 593-60-2 FPC DE 1/30/2010Dispersion GP 0.10U 0.11 U 0.10U Vinyl chloride VOC 75-01-4 FPC DE 1/30/2010Dispersion GP 4.26M 121.00M 0.69M Hydroquinone SVOC 123-31-9 FPC DE 1/30/2010Dispersion GP 0.10U 28.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/30/2010Dispersion GP 0.01 U 14.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/30/2010Dispersion GP 3.40U 10.00U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/30/2010Dispersion GP 3.47M 36.20M 3.79M Formaldehyde Aldehyd 50-00-0 FPC DE 1/30/2010Dispersion GP 0.01 U 0.15U 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/31/2010Dispersion GP 0.20U 0.51 U 0.51 U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/31/2010Dispersion GP 0.17U 0.27M 0.26U Chloroethane VOC 75-00-3 FPC DE 1/31/2010Dispersion GP 0.20M 4.30M 0.95M Chloroform VOC 67-66-3 FPC DE 1/31/2010Dispersion GP 0.12 U 0.24U 0.24U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/31/2010Dispersion GP 0.14U 0.23M 0.13U Chloroprene VOC 126-99-8 FPC DE 1/31/2010Dispersion GP 0.46U 0.85U 0.85U Vinyl acetate VOC 108-05-4 FPC DE 1/31/2010Dispersion GP 0.64U 0.81 U 0.80U Vinyl Bromide VOC 593-60-2 FPC DE 1/31/2010Dispersion GP 0.05U 0.10U 0.10U

Dispersion Conc. Data Agg 0900006480f92db5.xls 3 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Vinyl chloride VOC 75-01-4 FPC DE 1/31/2010Dispersion GP 4.13M 109.00M 1.00M Hydroquinone SVOC 123-31-9 FPC DE 1/31/2010Dispersion GP 0.10U 29.00U 22.00U Phenol SVOC 108-95-2 FPC DE 1/31/2010Dispersion GP 0.01 U 14.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/31/2010Dispersion GP 3.40U 13.00U 8.00U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/31/2010Dispersion GP 6.38M 31.80M 2.79M Formaldehyde Aldehyd 50-00-0 FPC DE 1/31/2010Dispersion GP 0.01 U 0.18M 0.12 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/1/2010Dispersion GP 0.04U 0.48U 1.00U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/1/2010Dispersion GP 0.03U 0.38M 0.52 U Chloroethane VOC 75-00-3 FPC DE 2/1/2010Dispersion GP 0.04U 6.36M 2.07M Chloroform VOC 67-66-3 FPC DE 2/1/2010Dispersion GP 0.02 U 0.23U 0.48U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/1/2010Dispersion GP 0.03U 0.29M 0.25U Chloroprene VOC 126-99-8 FPC DE 2/1/2010Dispersion GP 0.09U 0.80U 1.70U Vinyl acetate VOC 108-05-4 FPC DE 2/1/2010Dispersion GP 0.13U 0.75U 1.60U Vinyl Bromide VOC 593-60-2 FPC DE 2/1/2010Dispersion GP 0.01 U 0.10U 0.21 U Vinyl chloride VOC 75-01-4 FPC DE 2/1/2010Dispersion GP 0.04U 109.00M 1.49M Hydroquinone SVOC 123-31-9 FPC DE 2/1/2010Dispersion GP 1.00U 26.00U 22.00U Phenol SVOC 108-95-2 FPC DE 2/1/2010Dispersion GP 0.12 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/1/2010Dispersion GP 3.40U 5.80U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/1/2010Dispersion GP 0.99M 11.40M 3.58M Formaldehyde Aldehyd 50-00-0 FPC DE 2/1/2010Dispersion GP 0.01 U 0.14U 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/2/2010Dispersion GP 0.04U 0.87U 0.67U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/2/2010Dispersion GP 0.03U 1.35M 0.48M Chloroethane VOC 75-00-3 FPC DE 2/2/2010Dispersion GP 0.04U 11.20M 1.00U Chloroform VOC 67-66-3 FPC DE 2/2/2010Dispersion GP 0.02 U 0.42 U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/2/2010Dispersion GP 0.03U 0.22 U 0.17U Chloroprene VOC 126-99-8 FPC DE 2/2/2010Dispersion GP 0.09U 1.50U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 2/2/2010Dispersion GP 0.13U 1.40U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 2/2/2010Dispersion GP 0.01 U 0.18U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 2/2/2010Dispersion GP 0.64M 194.00M 0.63M Hydroquinone SVOC 123-31-9 FPC DE 2/2/2010Dispersion GP 1.00U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/2/2010Dispersion GP 0.12 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/2/2010Dispersion GP 1.70U 0.18U 0.16U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/2/2010Dispersion GP 0.85M 4.00M 1.26M Formaldehyde Aldehyd 50-00-0 FPC DE 2/2/2010Dispersion GP 0.01 U 0.69U 0.57U 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/3/2010Dispersion GP 0.04U 1.70U 1.00U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/3/2010Dispersion GP 0.03U 1.35M 0.55M Chloroethane VOC 75-00-3 FPC DE 2/3/2010Dispersion GP 0.04U 10.30M 1.50U Chloroform VOC 67-66-3 FPC DE 2/3/2010Dispersion GP 0.02 U 0.82 U 0.48U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/3/2010Dispersion GP 0.03U 0.42 U 0.25U Chloroprene VOC 126-99-8 FPC DE 2/3/2010Dispersion GP 0.09U 2.90U 1.70U Vinyl acetate VOC 108-05-4 FPC DE 2/3/2010Dispersion GP 0.13U 2.70U 1.60U Vinyl Bromide VOC 593-60-2 FPC DE 2/3/2010Dispersion GP 0.01 U 0.35U 0.20U Vinyl chloride VOC 75-01-4 FPC DE 2/3/2010Dispersion GP 0.80M 173.00M 1.53M Hydroquinone SVOC 123-31-9 FPC DE 2/3/2010Dispersion GP 1.00U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/3/2010Dispersion GP 0.12 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/3/2010Dispersion GP 1.70U 0.11 U 0.16U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/3/2010Dispersion GP 0.71 M 2.53M 1.11 M Formaldehyde Aldehyd 50-00-0 FPC DE 2/3/2010Dispersion GP 0.01 U 0.68U 0.57U 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/4/2010Dispersion GP 0.04U 0.85U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/4/2010Dispersion GP 0.03U 1.35M 0.43M Chloroethane VOC 75-00-3 FPC DE 2/4/2010Dispersion GP 0.04M 8.99M 1.01 M Chloroform VOC 67-66-3 FPC DE 2/4/2010Dispersion GP 0.02 U 0.41 U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/4/2010Dispersion GP 0.03U 0.21 U 0.17U Chloroprene VOC 126-99-8 FPC DE 2/4/2010Dispersion GP 0.09U 1.40U 1.10U

Dispersion Conc. Data Agg 0900006480f92db5.xls 4 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Vinyl acetate VOC 108-05-4 FPC DE 2/4/2010Dispersion GP 0.13U 1.30U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 2/4/2010Dispersion GP 0.01 U 0.17U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 2/4/2010Dispersion GP 0.95M 157.00M 0.84M Hydroquinone SVOC 123-31-9 FPC DE 2/4/2010Dispersion GP 1.00U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/4/2010Dispersion GP 0.12 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/4/2010Dispersion GP 1.70U 0.11 U 0.15U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/4/2010Dispersion GP 0.30M 2.68M 1.15M Formaldehyde Aldehyd 50-00-0 FPC DE 2/4/2010Dispersion GP 0.01 U 0.68U 0.57U 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/6/2010Dispersion GP 0.04U 0.90U 0.67U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/6/2010Dispersion GP 0.03U 1.14M 0.60M Chloroethane VOC 75-00-3 FPC DE 2/6/2010Dispersion GP 0.04U 9.72M 1.56M Chloroform VOC 67-66-3 FPC DE 2/6/2010Dispersion GP 0.02 U 0.43U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/6/2010Dispersion GP 0.03U 0.22 U 0.17U Chloroprene VOC 126-99-8 FPC DE 2/6/2010Dispersion GP 0.09U 1.50U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 2/6/2010Dispersion GP 0.13U 1.40U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 2/6/2010Dispersion GP 0.01 U 0.18U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 2/6/2010Dispersion GP 1.05M 181.00M 1.29M Hydroquinone SVOC 123-31-9 FPC DE 2/6/2010Dispersion GP 0.10U 25.00U 22.00U Phenol SVOC 108-95-2 FPC DE 2/6/2010Dispersion GP 0.01 U 12.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/6/2010Dispersion GP 3.40U 1.10U 1.50U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/6/2010Dispersion GP 0.38M 5.32M 1.76M Formaldehyde Aldehyd 50-00-0 FPC DE 2/6/2010Dispersion GP 0.01 U 0.39M 0.33M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/7/2010Dispersion GP 0.04U 2.30U 0.67U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/7/2010Dispersion GP 0.03U 1.20U 0.49M Chloroethane VOC 75-00-3 FPC DE 2/7/2010Dispersion GP 0.04U 9.04M 2.19M Chloroform VOC 67-66-3 FPC DE 2/7/2010Dispersion GP 0.02 U 1.10U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/7/2010Dispersion GP 0.03U 0.58U 0.17U Chloroprene VOC 126-99-8 FPC DE 2/7/2010Dispersion GP 0.09U 3.90U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 2/7/2010Dispersion GP 0.13U 3.70U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 2/7/2010Dispersion GP 0.01 U 0.47U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 2/7/2010Dispersion GP 1.23M 155.00M 1.52M Hydroquinone SVOC 123-31-9 FPC DE 2/7/2010Dispersion GP 0.10U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/7/2010Dispersion GP 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/7/2010Dispersion GP 3.40U 1.10U 1.60U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/7/2010Dispersion GP 0.99M 3.84M 1.92M Formaldehyde Aldehyd 50-00-0 FPC DE 2/7/2010Dispersion GP 0.03U 0.36M 0.33M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/10/2010Dispersion HMW 0.20U 0.50U 1.70U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/10/2010Dispersion HMW 0.17U 0.48M 0.86U Chloroethane VOC 75-00-3 FPC DE 2/10/2010Dispersion HMW 0.19U 8.09M 2.50U Chloroform VOC 67-66-3 FPC DE 2/10/2010Dispersion HMW 0.12 U 0.24U 0.80U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/10/2010Dispersion HMW 0.14U 0.12 U 0.41 U Chloroprene VOC 126-99-8 FPC DE 2/10/2010Dispersion HMW 0.46U 0.83U 2.80U Vinyl acetate VOC 108-05-4 FPC DE 2/10/2010Dispersion HMW 0.64U 0.79U 2.60U Vinyl Bromide VOC 593-60-2 FPC DE 2/10/2010Dispersion HMW 0.05U 0.10U 0.34U Vinyl chloride VOC 75-01-4 FPC DE 2/10/2010Dispersion HMW 2.45M 176.00M 1.56M Hydroquinone SVOC 123-31-9 FPC DE 2/10/2010Dispersion HMW 0.05U 27.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/10/2010Dispersion HMW 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/10/2010Dispersion HMW 3.40U 1.20U 3.20U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/10/2010Dispersion HMW 0.14M 1.43M 0.45M Formaldehyde Aldehyd 50-00-0 FPC DE 2/10/2010Dispersion HMW 0.01 U 0.34M 0.20M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/11/2010Dispersion HMW 0.20U 0.91 U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/11/2010Dispersion HMW 0.17U 0.72M 0.35U Chloroethane VOC 75-00-3 FPC DE 2/11/2010Dispersion HMW 0.19U 14.60M 1.76M Chloroform VOC 67-66-3 FPC DE 2/11/2010Dispersion HMW 0.12 U 0.44U 0.32 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 5 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/11/2010Dispersion HMW 0.14U 0.23U 0.17U Chloroprene VOC 126-99-8 FPC DE 2/11/2010Dispersion HMW 0.46U 1.50U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 2/11/2010Dispersion HMW 0.64U 1.50U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 2/11/2010Dispersion HMW 0.05U 0.19U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 2/11/2010Dispersion HMW 3.44M 357.00M 2.11 M Hydroquinone SVOC 123-31-9 FPC DE 2/11/2010Dispersion HMW 0.05U 27.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/11/2010Dispersion HMW 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/11/2010Dispersion HMW 3.40U 1.20U 1.50U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/11/2010Dispersion HMW 0.07M 2.26M 0.39M Formaldehyde Aldehyd 50-00-0 FPC DE 2/11/2010Dispersion HMW 0.01 U 0.54M 0.47M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/13/2010Dispersion HMW 0.08U 0.50U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/13/2010Dispersion HMW 0.07U 0.44M 0.35U Chloroethane VOC 75-00-3 FPC DE 2/13/2010Dispersion HMW 0.08M 6.33M 1.73M Chloroform VOC 67-66-3 FPC DE 2/13/2010Dispersion HMW 0.05U 0.24U 0.32 U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/13/2010Dispersion HMW 0.06U 0.12 U 0.17U Chloroprene VOC 126-99-8 FPC DE 2/13/2010Dispersion HMW 0.19U 0.84U 1.10U Vinyl acetate VOC 108-05-4 FPC DE 2/13/2010Dispersion HMW 0.25U 0.79U 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 2/13/2010Dispersion HMW 0.02 U 0.10U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 2/13/2010Dispersion HMW 1.84M 137.00M 1.82M Hydroquinone SVOC 123-31-9 FPC DE 2/13/2010Dispersion HMW 0.05U 27.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/13/2010Dispersion HMW 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/13/2010Dispersion HMW 3.40U 1.20U 1.50U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/13/2010Dispersion HMW 0.19M 0.52M 0.17M Formaldehyde Aldehyd 50-00-0 FPC DE 2/13/2010Dispersion HMW 0.03U 0.14U 0.11 U Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/12/2010Dispersion GP NM 429 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/13/2010Dispersion GP NM 503 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/14/2010Dispersion GP NM 410 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/15/2010Dispersion GP/HMW NM 517 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/16/2010Dispersion HMW NM 691 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/17/2010Dispersion HMW NM 666 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/18/2010Dispersion HMW NM 1162 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/19/2010Dispersion HMW NM 951 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/20/2010Dispersion HMW NM 709 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/29/2010Dispersion GP NM 866 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/30/2010Dispersion GP NM 901 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 1/31/2010Dispersion GP NM 522 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/1/2010Dispersion GP NM 572 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/2/2010Dispersion GP NM 541 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/3/2010Dispersion GP NM 706 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/4/2010Dispersion GP NM 560 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/6/2010Dispersion GP NM 522 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/7/2010Dispersion GP NM 693 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/10/2010Dispersion HMW NM 614 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/11/2010Dispersion HMW NM 628 M NM Vinyl chloride Method 107* VOC 75-01-4VOCFPC DE 2/13/2010Dispersion HMW NM 313 M NM 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.055 MDL 0.177 M 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.26 MDL 0.21 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.142J 0.411 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.31 MDL 0.25 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.78 MDL 0.991 J Acetaldehyde Aldehyde75-07-0 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.06 MDL 0.0528J Acetophenone SVOC 98-86-2 P1-Ptown 2-Dec-09 Dispersion HMW NM 1.1 MDL 6.13J Benzene VOC 71-43-2 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.13 MDL 0.11 MDL Chloroethane VOC 75-00-3 P1-Ptown 2-Dec-09 Dispersion HMW NM 6.4 M 2.89 M Chloroform VOC 67-66-3 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.13 MDL 0.099 MDL Chloromethane VOC 74-87-3 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.773 M 0.051 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 6 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Formaldehyde Aldehyde50-00-0 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.473J 0.538J Hydroquinone SVOC 123-31-9 P1-Ptown 2-Dec-09 Dispersion HMW NM 14 MDL 11 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.2 MDL 1.45 M Methanol Alcohol 67-56-1 P1-Ptown 2-Dec-09 Dispersion HMW NM 15.7 M 0.097 MDL Phenol SVOC 108-95-2 P1-Ptown 2-Dec-09 Dispersion HMW NM 6.8 MDL 5.4 MDL Toluene VOC 108-88-3 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.12 MDL 0.091 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.054 MDL 0.042 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 2-Dec-09 Dispersion HMW NM 22.7 M 0.377 M Xylene (total) VOC 1330-20-7 P1-Ptown 2-Dec-09 Dispersion HMW NM 0.19 MDL 0.15 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.055 MDL 0.112J 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.26 MDL 0.2 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.14 MDL 0.261 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.31 MDL 0.24 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.78 MDL 0.6 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.06 MDL 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.14 MDL 0.1 MDL Chloroethane VOC 75-00-3 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 6.3 M 2.98 M Chloroform VOC 67-66-3 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.13 MDL 0.096 MDL Chloromethane VOC 74-87-3 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.643 M 0.05 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.523J 0.123J Hydroquinone SVOC 123-31-9 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.21 MDL 0.308 M Methanol Alcohol 67-56-1 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 11.1 M 0.1 MDL Phenol SVOC 108-95-2 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.12 MDL 0.089 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.054 MDL 0.041 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 21.1 M 0.603 M Xylene (total) VOC 1330-20-7 P1-Ptown 3-Dec-09 Dispersion HMW/LMW NM 0.19 MDL 0.14 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.0754J 0.1 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.27 MDL 0.5 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.238 M 0.26 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.32 MDL 0.742J 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.79 MDL 1.5 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.0956J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 4-Dec-09 Dispersion HMW NM 1.1 MDL 8.9 MDL Benzene VOC 71-43-2 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.14 MDL 0.26 MDL Chloroethane VOC 75-00-3 P1-Ptown 4-Dec-09 Dispersion HMW NM 17.4 M 3.24 M Chloroform VOC 67-66-3 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.13 MDL 0.24 MDL Chloromethane VOC 74-87-3 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.966 M 0.12 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.636J 0.226J Hydroquinone SVOC 123-31-9 P1-Ptown 4-Dec-09 Dispersion HMW NM 14 MDL 110 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.21 MDL 0.39 MDL Methanol Alcohol 67-56-1 P1-Ptown 4-Dec-09 Dispersion HMW NM 12.2 M 0.099 MDL Phenol SVOC 108-95-2 P1-Ptown 4-Dec-09 Dispersion HMW NM 6.9 MDL 53 MDL Toluene VOC 108-88-3 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.12 MDL 0.22 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.055 MDL 0.1 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 4-Dec-09 Dispersion HMW NM 45.2 M 0.463 M Xylene (total) VOC 1330-20-7 P1-Ptown 4-Dec-09 Dispersion HMW NM 0.19 MDL 0.35 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.0922J 0.0748J 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.2 MDL 0.26 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.207 M 0.297 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.24 MDL 0.31 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.6 MDL 0.78 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.047 MDL 0.127J Acetophenone SVOC 98-86-2 P1-Ptown 5-Dec-09 Dispersion HMW NM 1.8 MDL 26.1 M Benzene VOC 71-43-2 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.1 MDL 0.13 MDL Chloroethane VOC 75-00-3 P1-Ptown 5-Dec-09 Dispersion HMW NM 3.68 M 20.6 M

Dispersion Conc. Data Agg 0900006480f92db5.xls 7 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Chloroform VOC 67-66-3 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.097 MDL 0.13 MDL Chloromethane VOC 74-87-3 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.05 MDL 2.24 M Formaldehyde Aldehyde50-00-0 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.156J 0.638J Hydroquinone SVOC 123-31-9 P1-Ptown 5-Dec-09 Dispersion HMW NM 22 MDL 2.8 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.16 MDL 0.41 M Methanol Alcohol 67-56-1 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.048 MDL 5.7 MDL Phenol SVOC 108-95-2 P1-Ptown 5-Dec-09 Dispersion HMW NM 11 MDL 1.4 MDL Toluene VOC 108-88-3 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.089 MDL 0.12 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.041 MDL 0.054 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.779 M 72.8 M Xylene (total) VOC 1330-20-7 P1-Ptown 5-Dec-09 Dispersion HMW NM 0.14 MDL 0.18 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.11 MDL 0.07 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.52 MDL 0.34 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.442 M 0.222J 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.62 MDL 0.4 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 6-Dec-09 Dispersion HMW NM 1.5 MDL 1 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.267J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 6-Dec-09 Dispersion HMW NM 27.5J 16.8J Benzene VOC 71-43-2 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.27 MDL 0.17 MDL Chloroethane VOC 75-00-3 P1-Ptown 6-Dec-09 Dispersion HMW NM 36.8 M 6.04 M Chloroform VOC 67-66-3 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.25 MDL 0.16 MDL Chloromethane VOC 74-87-3 P1-Ptown 6-Dec-09 Dispersion HMW NM 4.42 M 0.084 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.395J 0.111 J Hydroquinone SVOC 123-31-9 P1-Ptown 6-Dec-09 Dispersion HMW NM 28 MDL 11 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.674J 0.836 M Methanol Alcohol 67-56-1 P1-Ptown 6-Dec-09 Dispersion HMW NM 3.1 MDL 0.092 MDL Phenol SVOC 108-95-2 P1-Ptown 6-Dec-09 Dispersion HMW NM 13 MDL 5.3 MDL Toluene VOC 108-88-3 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.23 MDL 0.15 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.11 MDL 0.069 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 6-Dec-09 Dispersion HMW NM 105 M 1.31 M Xylene (total) VOC 1330-20-7 P1-Ptown 6-Dec-09 Dispersion HMW NM 0.37 MDL 0.24 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.213J 0.14 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.47 MDL 0.66 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.756 M 0.35 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.56 MDL 0.8 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 7-Dec-09 Dispersion HMW NM 2.18J 2 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.552J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 7-Dec-09 Dispersion HMW NM 2.2 MDL 16.3J Benzene VOC 71-43-2 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.24 MDL 0.34 MDL Chloroethane VOC 75-00-3 P1-Ptown 7-Dec-09 Dispersion HMW NM 54.3 M 7.89 M Chloroform VOC 67-66-3 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.22 MDL 0.32 MDL Chloromethane VOC 74-87-3 P1-Ptown 7-Dec-09 Dispersion HMW NM 5.55 M 0.17 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.341 J 0.11 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 7-Dec-09 Dispersion HMW NM 27 MDL 11 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.932 M 2.42 M Methanol Alcohol 67-56-1 P1-Ptown 7-Dec-09 Dispersion HMW NM 202 M 0.091 MDL Phenol SVOC 108-95-2 P1-Ptown 7-Dec-09 Dispersion HMW NM 13 MDL 5.3 MDL Toluene VOC 108-88-3 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.21 MDL 0.29 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.096 MDL 0.14 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 7-Dec-09 Dispersion HMW NM 119 M 0.802 M Xylene (total) VOC 1330-20-7 P1-Ptown 7-Dec-09 Dispersion HMW NM 0.33 MDL 0.47 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.122J 0.0927J 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.52 MDL 0.33 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.472 M 0.257 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.62 MDL 0.4 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 8-Dec-09 Dispersion HMW NM 1.5 MDL 0.99 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.264J 0.094 MDL Note: There is an anomoly in the values for PolyOne Pedricktow n vinyl chloride based on M8260B. It appears the results for wet resin and

Dispersion Conc. Data Agg 0900006480f92db5.xls 8 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Acetophenone SVOC 98-86-2 P1-Ptown 8-Dec-09 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.27 MDL 0.17 MDL Chloroethane VOC 75-00-3 P1-Ptown 8-Dec-09 Dispersion HMW NM 21 M 3.73 M Chloroform VOC 67-66-3 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.25 MDL 0.16 MDL Chloromethane VOC 74-87-3 P1-Ptown 8-Dec-09 Dispersion HMW NM 1.16 M 0.083 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.631 JB 0.15JB Hydroquinone SVOC 123-31-9 P1-Ptown 8-Dec-09 Dispersion HMW NM 28 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.4 MDL 0.802 M Methanol Alcohol 67-56-1 P1-Ptown 8-Dec-09 Dispersion HMW NM 28.5 M 0.095 MDL Phenol SVOC 108-95-2 P1-Ptown 8-Dec-09 Dispersion HMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.23 MDL 0.15 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.11 MDL 0.068 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 8-Dec-09 Dispersion HMW NM 29.7 M 0.352 M Xylene (total) VOC 1330-20-7 P1-Ptown 8-Dec-09 Dispersion HMW NM 0.37 MDL 0.24 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.129J 0.112J 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.47 MDL 0.5 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.601 M 0.331 J 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.56 MDL 0.6 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 9-Dec-09 Dispersion HMW NM 2.07J 1.51 J Acetaldehyde Aldehyde75-07-0 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.342JB 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 9-Dec-09 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.24 MDL 0.26 MDL Chloroethane VOC 75-00-3 P1-Ptown 9-Dec-09 Dispersion HMW NM 28.4 M 2.97 M Chloroform VOC 67-66-3 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.23 MDL 0.24 MDL Chloromethane VOC 74-87-3 P1-Ptown 9-Dec-09 Dispersion HMW NM 3.2 M 0.126J Formaldehyde Aldehyde50-00-0 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.51 JB 0.149JB Hydroquinone SVOC 123-31-9 P1-Ptown 9-Dec-09 Dispersion HMW NM 27 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.37 MDL 0.415J Methanol Alcohol 67-56-1 P1-Ptown 9-Dec-09 Dispersion HMW NM 5.8 MDL 0.099 MDL Phenol SVOC 108-95-2 P1-Ptown 9-Dec-09 Dispersion HMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.21 MDL 0.22 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.097 MDL 0.1 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 9-Dec-09 Dispersion HMW NM 102 M 0.731 M Xylene (total) VOC 1330-20-7 P1-Ptown 9-Dec-09 Dispersion HMW NM 0.33 MDL 0.35 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.2 MDL 0.14 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.98 MDL 0.66 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.517J 0.35 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 10-Dec-09 Dispersion HMW NM 1.2 MDL 0.8 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 10-Dec-09 Dispersion HMW NM 2.9 MDL 2 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.414JB 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 10-Dec-09 Dispersion HMW NM 2.3 MDL 0.18 MDL Benzene VOC 71-43-2 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.51 MDL 0.34 MDL Chloroethane VOC 75-00-3 P1-Ptown 10-Dec-09 Dispersion HMW NM 39.4 M 2.97 M Chloroform VOC 67-66-3 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.47 MDL 0.32 MDL Chloromethane VOC 74-87-3 P1-Ptown 10-Dec-09 Dispersion HMW NM 5.45 M 0.17 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.389JB 0.11 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 10-Dec-09 Dispersion HMW NM 28 MDL 2.1 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.77 MDL 0.52 MDL Methanol Alcohol 67-56-1 P1-Ptown 10-Dec-09 Dispersion HMW NM 6.3 MDL 0.091 MDL Phenol SVOC 108-95-2 P1-Ptown 10-Dec-09 Dispersion HMW NM 14 MDL 1.1 MDL Toluene VOC 108-88-3 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.43 MDL 0.29 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.2 MDL 0.14 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 10-Dec-09 Dispersion HMW NM 166 M 0.616 M Xylene (total) VOC 1330-20-7 P1-Ptown 10-Dec-09 Dispersion HMW NM 0.69 MDL 0.47 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.13J 0.1 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.48 MDL 0.5 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.829 M 0.407 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.57 MDL 0.735J

Dispersion Conc. Data Agg 0900006480f92db5.xls 9 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 11-Dec-09 Dispersion HMW NM 2.12J 1.5 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.482JB 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 11-Dec-09 Dispersion HMW NM 15.9J 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.24 MDL 0.26 MDL Chloroethane VOC 75-00-3 P1-Ptown 11-Dec-09 Dispersion HMW NM 54.4 M 5.41 M Chloroform VOC 67-66-3 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.23 MDL 0.24 MDL Chloromethane VOC 74-87-3 P1-Ptown 11-Dec-09 Dispersion HMW NM 3.41 M 0.13 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.343JB 0.11 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 11-Dec-09 Dispersion HMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 11-Dec-09 Dispersion HMW NM 1.81 M 0.39 MDL Methanol Alcohol 67-56-1 P1-Ptown 11-Dec-09 Dispersion HMW NM 12 MDL 0.96 MDL Phenol SVOC 108-95-2 P1-Ptown 11-Dec-09 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.21 MDL 0.22 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.098 MDL 0.1 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 11-Dec-09 Dispersion HMW NM 93 M 1.15 M Xylene (total) VOC 1330-20-7 P1-Ptown 11-Dec-09 Dispersion HMW NM 0.34 MDL 0.36 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Acetaldehyde Aldehyde75-07-0 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Acetophenone SVOC 98-86-2 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Benzene VOC 71-43-2 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Chloroethane VOC 75-00-3 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Chloroform VOC 67-66-3 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Chloromethane VOC 74-87-3 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Formaldehyde Aldehyde50-00-0 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Hydroquinone SVOC 123-31-9 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Isopropylbenzene VOC 98-82-8 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Methanol Alcohol 67-56-1 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Phenol SVOC 108-95-2 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Toluene VOC 108-88-3 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Vinyl Bromide VOC 593-60-2 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Vinyl chloride VOC 75-01-4 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM Xylene (total) VOC 1330-20-7 P1-Ptown 12-Dec-09 Dispersion HMW NM NM NM 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.11 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.51 MDL 1 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.595 M 0.52 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.62 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 13-Dec-09 Dispersion HMW NM 1.5 MDL 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.42J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 13-Dec-09 Dispersion HMW NM 2.2 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.27 MDL 0.51 MDL Chloroethane VOC 75-00-3 P1-Ptown 13-Dec-09 Dispersion HMW NM 47.3 M 13.6 M Chloroform VOC 67-66-3 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.25 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 13-Dec-09 Dispersion HMW NM 4.1 M 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.381 JB 0.11 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 13-Dec-09 Dispersion HMW NM 27 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.4 MDL 2.81 M Methanol Alcohol 67-56-1 P1-Ptown 13-Dec-09 Dispersion HMW NM 13 MDL 7.9 MDL Phenol SVOC 108-95-2 P1-Ptown 13-Dec-09 Dispersion HMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.23 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.11 MDL 0.2 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 13-Dec-09 Dispersion HMW NM 126 M 3.96 M Xylene (total) VOC 1330-20-7 P1-Ptown 13-Dec-09 Dispersion HMW NM 0.36 MDL 0.71 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.2 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.95 MDL 1 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 10 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.954 M 0.97 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 14-Dec-09 Dispersion HMW NM 1.1 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 14-Dec-09 Dispersion HMW NM 2.8 MDL 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.109J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 14-Dec-09 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.49 MDL 0.737J Chloroethane VOC 75-00-3 P1-Ptown 14-Dec-09 Dispersion HMW NM 41.6 M 33.1 M Chloroform VOC 67-66-3 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.46 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 14-Dec-09 Dispersion HMW NM 2.1 M 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.15 MDL 0.137JB Hydroquinone SVOC 123-31-9 P1-Ptown 14-Dec-09 Dispersion HMW NM 28 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.74 MDL 2.57 M Methanol Alcohol 67-56-1 P1-Ptown 14-Dec-09 Dispersion HMW NM 3.1 MDL 7.9 MDL Phenol SVOC 108-95-2 P1-Ptown 14-Dec-09 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.42 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.2 MDL 0.2 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 14-Dec-09 Dispersion HMW NM 57.6 M 12.9 M Xylene (total) VOC 1330-20-7 P1-Ptown 14-Dec-09 Dispersion HMW NM 0.67 MDL 0.71 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.2 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.95 MDL 1 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.973 M 0.553J 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 15-Dec-09 Dispersion HMW NM 1.1 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 15-Dec-09 Dispersion HMW NM 2.8 MDL 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.434J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 15-Dec-09 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.49 MDL 0.51 MDL Chloroethane VOC 75-00-3 P1-Ptown 15-Dec-09 Dispersion HMW NM 15.5 M 5.68 M Chloroform VOC 67-66-3 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.45 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.24 MDL 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.172J 0.11 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 15-Dec-09 Dispersion HMW NM 28 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.74 MDL 0.78 MDL Methanol Alcohol 67-56-1 P1-Ptown 15-Dec-09 Dispersion HMW NM 12 MDL 0.95 MDL Phenol SVOC 108-95-2 P1-Ptown 15-Dec-09 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.42 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.19 MDL 0.21 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 15-Dec-09 Dispersion HMW NM 6.29 M 0.27 MDL Xylene (total) VOC 1330-20-7 P1-Ptown 15-Dec-09 Dispersion HMW NM 0.67 MDL 0.71 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.0691 J 0.1 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.26 MDL 0.5 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.51 M 0.484 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.31 MDL 0.6 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.78 MDL 1.5 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 16-Dec-09 Dispersion HMW NM 1.3 M 0.0725J Acetophenone SVOC 98-86-2 P1-Ptown 16-Dec-09 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.14 MDL 0.26 MDL Chloroethane VOC 75-00-3 P1-Ptown 16-Dec-09 Dispersion HMW NM 36.2 M 5.93 M Chloroform VOC 67-66-3 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.13 MDL 0.24 MDL Chloromethane VOC 74-87-3 P1-Ptown 16-Dec-09 Dispersion HMW NM 3.58 M 0.12 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.502J 0.138J Hydroquinone SVOC 123-31-9 P1-Ptown 16-Dec-09 Dispersion HMW NM 28 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.21 MDL 0.39 MDL Methanol Alcohol 67-56-1 P1-Ptown 16-Dec-09 Dispersion HMW NM 12 MDL 7.9 MDL Phenol SVOC 108-95-2 P1-Ptown 16-Dec-09 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.12 MDL 0.22 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.054 MDL 0.1 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 16-Dec-09 Dispersion HMW NM 57.7 M 0.375J Xylene (total) VOC 1330-20-7 P1-Ptown 16-Dec-09 Dispersion HMW NM 0.19 MDL 0.35 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 11 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.053 MDL 0.0325J 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.25 MDL 0.067 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.36 M 0.208 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.31 MDL 0.081 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.76 MDL 0.2 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.293J 0.065J Acetophenone SVOC 98-86-2 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 2.2 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.13 MDL 0.035 MDL Chloroethane VOC 75-00-3 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 18.2 M 4.87 M Chloroform VOC 67-66-3 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.12 MDL 0.033J Chloromethane VOC 74-87-3 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.67 M 0.017 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.387J 0.203J Hydroquinone SVOC 123-31-9 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 27 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.2 MDL 0.053 MDL Methanol Alcohol 67-56-1 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 13 MDL 7.5 MDL Phenol SVOC 108-95-2 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.11 MDL 0.03 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.052 MDL 0.014 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 15.2 M 0.532 M Xylene (total) VOC 1330-20-7 P1-Ptown 17-Dec-09 Dispersion HMW/LMW NM 0.18 MDL 0.048 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.11 MDL 0.0537J 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.52 MDL 0.2 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.631 M 0.528 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.62 MDL 1.06 M 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 18-Dec-09 Dispersion HMW NM 1.5 MDL 0.6 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.362J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 18-Dec-09 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.27 MDL 0.1 MDL Chloroethane VOC 75-00-3 P1-Ptown 18-Dec-09 Dispersion HMW NM 51.7 M 3.49 M Chloroform VOC 67-66-3 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.25 MDL 0.097 MDL Chloromethane VOC 74-87-3 P1-Ptown 18-Dec-09 Dispersion HMW NM 5.32 M 0.05 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.321 J 0.278J Hydroquinone SVOC 123-31-9 P1-Ptown 18-Dec-09 Dispersion HMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.41 MDL 0.188J Methanol Alcohol 67-56-1 P1-Ptown 18-Dec-09 Dispersion HMW NM 12 MDL 30 MDL Phenol SVOC 108-95-2 P1-Ptown 18-Dec-09 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.23 MDL 0.089 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.11 MDL 0.041 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 18-Dec-09 Dispersion HMW NM 89.9 M 0.375 M Xylene (total) VOC 1330-20-7 P1-Ptown 18-Dec-09 Dispersion HMW NM 0.37 MDL 0.14 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.23 MDL 0.069 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 4-Jan-10 Dispersion HMW NM 1.1 MDL 0.33 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.965 M 0.17 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 4-Jan-10 Dispersion HMW NM 1.3 MDL 0.4 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 4-Jan-10 Dispersion HMW NM 3.3 MDL 0.99 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.619JB 0.0731 JB Acetophenone SVOC 98-86-2 P1-Ptown 4-Jan-10 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.57 MDL 0.17 MDL Chloroethane VOC 75-00-3 P1-Ptown 4-Jan-10 Dispersion HMW NM 59.1 M 2.44 M Chloroform VOC 67-66-3 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.53 MDL 0.16 MDL Chloromethane VOC 74-87-3 P1-Ptown 4-Jan-10 Dispersion HMW NM 4.71 M 0.083 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.511 J 0.197J Hydroquinone SVOC 123-31-9 P1-Ptown 4-Jan-10 Dispersion HMW NM 27 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.86 MDL 0.518 M Methanol Alcohol 67-56-1 P1-Ptown 4-Jan-10 Dispersion HMW NM 27.1 M 0.95 MDL Phenol SVOC 108-95-2 P1-Ptown 4-Jan-10 Dispersion HMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.49 MDL 0.15 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.23 MDL 0.068 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 12 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Vinyl chloride VOC 75-01-4 P1-Ptown 4-Jan-10 Dispersion HMW NM 110 M 0.384 M Xylene (total) VOC 1330-20-7 P1-Ptown 4-Jan-10 Dispersion HMW NM 0.78 MDL 0.24 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.2 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.95 MDL 1 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.49 MDL 0.52 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 1.1 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 2.8 MDL 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.834JB 0.059 MDL Acetophenone SVOC 98-86-2 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.49 MDL 0.51 MDL Chloroethane VOC 75-00-3 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 37.9 M 4.14 M Chloroform VOC 67-66-3 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.46 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 3.13 M 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.616J 0.14 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 27 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.74 MDL 1.59 M Methanol Alcohol 67-56-1 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 37.5 M 0.99 MDL Phenol SVOC 108-95-2 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.42 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.19 MDL 0.2 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 91.2 M 0.27 MDL Xylene (total) VOC 1330-20-7 P1-Ptown 5-Jan-10 Dispersion HMW/LMW NM 0.67 MDL 0.71 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 0.57 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 2.8 MDL 0.99 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 1.4 MDL 0.52 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 3.3 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 8.2 MDL 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 1.09 B 0.15JB Acetophenone SVOC 98-86-2 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 1.4 MDL 0.51 MDL Chloroethane VOC 75-00-3 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 65.7 M 4.29 M Chloroform VOC 67-66-3 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 1.3 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 5.4 M 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 0.632J 0.219J Hydroquinone SVOC 123-31-9 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 28 MDL 21 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 2.2 MDL 1.06J Methanol Alcohol 67-56-1 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 10.7 M 0.91 MDL Phenol SVOC 108-95-2 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 1.2 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 0.57 MDL 0.2 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 169 M 0.27 MDL Xylene (total) VOC 1330-20-7 P1-Ptown 6-Jan-10 Dispersion HMW/LMW NM 2 MDL 0.7 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.11 MDL 0.07 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.53 MDL 0.33 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.327J 0.17 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.63 MDL 0.4 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 7-Jan-10 Dispersion HMW NM 1.6 MDL 1 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.836JB 0.198JB Acetophenone SVOC 98-86-2 P1-Ptown 7-Jan-10 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.27 MDL 0.17 MDL Chloroethane VOC 75-00-3 P1-Ptown 7-Jan-10 Dispersion HMW NM 16.6 M 1.69 M Chloroform VOC 67-66-3 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.25 MDL 0.16 MDL Chloromethane VOC 74-87-3 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.695 M 0.083 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 7-Jan-10 Dispersion HMW NM 1.18 M 0.279J Hydroquinone SVOC 123-31-9 P1-Ptown 7-Jan-10 Dispersion HMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.41 MDL 0.26 MDL Methanol Alcohol 67-56-1 P1-Ptown 7-Jan-10 Dispersion HMW NM 8.11 M 13.1 M Phenol SVOC 108-95-2 P1-Ptown 7-Jan-10 Dispersion HMW NM 14 MDL 11 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 13 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Toluene VOC 108-88-3 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.23 MDL 0.15 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.11 MDL 0.069 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 7-Jan-10 Dispersion HMW NM 27.2 M 0.212J Xylene (total) VOC 1330-20-7 P1-Ptown 7-Jan-10 Dispersion HMW NM 0.37 MDL 0.24 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.093 MDL 0.1 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.45 MDL 0.5 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.23 MDL 0.26 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.54 MDL 0.6 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 8-Jan-10 Dispersion HMW NM 1.3 MDL 1.5 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 8-Jan-10 Dispersion HMW NM 1 M 0.0948J Acetophenone SVOC 98-86-2 P1-Ptown 8-Jan-10 Dispersion HMW NM 2.2 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.23 MDL 0.26 MDL Chloroethane VOC 75-00-3 P1-Ptown 8-Jan-10 Dispersion HMW NM 37.5 M 8.32 M Chloroform VOC 67-66-3 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.22 MDL 0.24 MDL Chloromethane VOC 74-87-3 P1-Ptown 8-Jan-10 Dispersion HMW NM 3.67 M 0.13 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.398J 0.112J Hydroquinone SVOC 123-31-9 P1-Ptown 8-Jan-10 Dispersion HMW NM 26 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.35 MDL 0.617J Methanol Alcohol 67-56-1 P1-Ptown 8-Jan-10 Dispersion HMW NM 7.84 M 0.37 MDL Phenol SVOC 108-95-2 P1-Ptown 8-Jan-10 Dispersion HMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.2 MDL 0.22 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.092 MDL 0.1 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 8-Jan-10 Dispersion HMW NM 126 M 1.62 M Xylene (total) VOC 1330-20-7 P1-Ptown 8-Jan-10 Dispersion HMW NM 0.32 MDL 0.36 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.21 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 9-Jan-10 Dispersion HMW NM 1 MDL 1 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.54 MDL 0.52 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 9-Jan-10 Dispersion HMW NM 1.2 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 9-Jan-10 Dispersion HMW NM 3.1 MDL 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.937J 0.0992J Acetophenone SVOC 98-86-2 P1-Ptown 9-Jan-10 Dispersion HMW NM 2.2 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.53 MDL 0.52 MDL Chloroethane VOC 75-00-3 P1-Ptown 9-Jan-10 Dispersion HMW NM 44.7 M 2.95 M Chloroform VOC 67-66-3 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.5 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 9-Jan-10 Dispersion HMW NM 4.53 M 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.903J 0.11 MDL Hydroquinone SVOC 123-31-9 P1-Ptown 9-Jan-10 Dispersion HMW NM 27 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.81 MDL 1.36J Methanol Alcohol 67-56-1 P1-Ptown 9-Jan-10 Dispersion HMW NM 25.7 M 8.7 M Phenol SVOC 108-95-2 P1-Ptown 9-Jan-10 Dispersion HMW NM 13 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.45 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.21 MDL 0.21 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 9-Jan-10 Dispersion HMW NM 86.5 M 0.27 MDL Xylene (total) VOC 1330-20-7 P1-Ptown 9-Jan-10 Dispersion HMW NM 0.73 MDL 0.71 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Acetaldehyde Aldehyde75-07-0 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Acetophenone SVOC 98-86-2 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Benzene VOC 71-43-2 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Chloroethane VOC 75-00-3 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Chloroform VOC 67-66-3 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Chloromethane VOC 74-87-3 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Formaldehyde Aldehyde50-00-0 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Hydroquinone SVOC 123-31-9 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Isopropylbenzene VOC 98-82-8 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM

Dispersion Conc. Data Agg 0900006480f92db5.xls 14 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Methanol Alcohol 67-56-1 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Phenol SVOC 108-95-2 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Toluene VOC 108-88-3 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Vinyl Bromide VOC 593-60-2 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Vinyl chloride VOC 75-01-4 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM Xylene (total) VOC 1330-20-7 P1-Ptown 10-Jan-10 Dispersion HMW NM NM NM 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.14 MDL 0.21 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.69 MDL 1 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 11-Jan-10 Dispersion HMW NM 1.21 M 0.888 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.83 MDL 1.2 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 11-Jan-10 Dispersion HMW NM 4.14J 3 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 11-Jan-10 Dispersion HMW NM 1.84 M 0.113J Acetophenone SVOC 98-86-2 P1-Ptown 11-Jan-10 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.36 MDL 0.52 MDL Chloroethane VOC 75-00-3 P1-Ptown 11-Jan-10 Dispersion HMW NM 81.6 M 16.9 M Chloroform VOC 67-66-3 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.33 MDL 0.48 MDL Chloromethane VOC 74-87-3 P1-Ptown 11-Jan-10 Dispersion HMW NM 5.92 M 0.25 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.738J 0.446J Hydroquinone SVOC 123-31-9 P1-Ptown 11-Jan-10 Dispersion HMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.541 J 0.819J Methanol Alcohol 67-56-1 P1-Ptown 11-Jan-10 Dispersion HMW NM 6.1 MDL 3.2 MDL Phenol SVOC 108-95-2 P1-Ptown 11-Jan-10 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.3 MDL 0.44 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.14 MDL 0.21 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 11-Jan-10 Dispersion HMW NM 117 M 1.98 M Xylene (total) VOC 1330-20-7 P1-Ptown 11-Jan-10 Dispersion HMW NM 0.49 MDL 0.71 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.2 MDL 0.42 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.95 MDL 2 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.585J 1 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 12-Jan-10 Dispersion HMW NM 1.1 MDL 2.4 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 12-Jan-10 Dispersion HMW NM 2.8 MDL 5.9 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 12-Jan-10 Dispersion HMW NM 3.51 J 0.0725J Acetophenone SVOC 98-86-2 P1-Ptown 12-Jan-10 Dispersion HMW NM 46.4 M 18.8J Benzene VOC 71-43-2 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.49 MDL 1 MDL Chloroethane VOC 75-00-3 P1-Ptown 12-Jan-10 Dispersion HMW NM 45.3 M 15.1 M Chloroform VOC 67-66-3 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.46 MDL 0.96 MDL Chloromethane VOC 74-87-3 P1-Ptown 12-Jan-10 Dispersion HMW NM 1.76 M 0.5 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 12-Jan-10 Dispersion HMW NM 2.71 J 0.142J Hydroquinone SVOC 123-31-9 P1-Ptown 12-Jan-10 Dispersion HMW NM 11 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.853J 1.6 MDL Methanol Alcohol 67-56-1 P1-Ptown 12-Jan-10 Dispersion HMW NM 6.1 MDL 3.2 MDL Phenol SVOC 108-95-2 P1-Ptown 12-Jan-10 Dispersion HMW NM 5.6 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.42 MDL 0.88 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.2 MDL 0.41 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 12-Jan-10 Dispersion HMW NM 84.2 M 1.52 M Xylene (total) VOC 1330-20-7 P1-Ptown 12-Jan-10 Dispersion HMW NM 0.67 MDL 1.4 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.059 MDL 0.78 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.28 MDL 3.7 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.316 M 1.9 MDL 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.34 MDL 4.5 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.84 MDL 11 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 13-Jan-10 Dispersion HMW NM 1.06J 0.537J Acetophenone SVOC 98-86-2 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.24 MDL 10 MDL Benzene VOC 71-43-2 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.15 MDL 1.9 MDL Chloroethane VOC 75-00-3 P1-Ptown 13-Jan-10 Dispersion HMW NM 27.2 M 36.8 M Chloroform VOC 67-66-3 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.14 MDL 1.8 MDL Chloromethane VOC 74-87-3 P1-Ptown 13-Jan-10 Dispersion HMW NM 5.89 M 0.93 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.783J 0.67 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 15 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Hydroquinone SVOC 123-31-9 P1-Ptown 13-Jan-10 Dispersion HMW NM 2.9 MDL 130 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.22 MDL 2.9 MDL Methanol Alcohol 67-56-1 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.63 MDL 9.3 MDL Phenol SVOC 108-95-2 P1-Ptown 13-Jan-10 Dispersion HMW NM 1.4 MDL 62 MDL Toluene VOC 108-88-3 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.12 MDL 1.6 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.058 MDL 0.77 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 13-Jan-10 Dispersion HMW NM 134 M 8.52 M Xylene (total) VOC 1330-20-7 P1-Ptown 13-Jan-10 Dispersion HMW NM 0.2 MDL 2.6 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.1 MDL 0.042 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.48 MDL 0.2 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.436 M 0.307 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.58 MDL 0.24 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 14-Jan-10 Dispersion HMW NM 1.4 MDL 0.6 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.723J 0.069J Acetophenone SVOC 98-86-2 P1-Ptown 14-Jan-10 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.25 MDL 0.1 MDL Chloroethane VOC 75-00-3 P1-Ptown 14-Jan-10 Dispersion HMW NM 17.9 M 2.92 M Chloroform VOC 67-66-3 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.23 MDL 0.097 MDL Chloromethane VOC 74-87-3 P1-Ptown 14-Jan-10 Dispersion HMW NM 1.97 M 0.05 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.69J 0.17J Hydroquinone SVOC 123-31-9 P1-Ptown 14-Jan-10 Dispersion HMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.826 M 0.938 M Methanol Alcohol 67-56-1 P1-Ptown 14-Jan-10 Dispersion HMW NM 12 MDL 8 MDL Phenol SVOC 108-95-2 P1-Ptown 14-Jan-10 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.21 MDL 0.089 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.099 MDL 0.041 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 14-Jan-10 Dispersion HMW NM 68.3 M 0.565 M Xylene (total) VOC 1330-20-7 P1-Ptown 14-Jan-10 Dispersion HMW NM 0.34 MDL 0.14 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.1 MDL 0.07 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.48 MDL 0.33 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.725 M 0.444 M 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.57 MDL 0.4 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 15-Jan-10 Dispersion HMW NM 1.4 MDL 1.55J Acetaldehyde Aldehyde75-07-0 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.749J 0.047 MDL Acetophenone SVOC 98-86-2 P1-Ptown 15-Jan-10 Dispersion HMW NM 2.3 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.25 MDL 0.17 MDL Chloroethane VOC 75-00-3 P1-Ptown 15-Jan-10 Dispersion HMW NM 26.4 M 1.5 M Chloroform VOC 67-66-3 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.23 MDL 0.16 MDL Chloromethane VOC 74-87-3 P1-Ptown 15-Jan-10 Dispersion HMW NM 2.38 M 0.083 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.611 J 0.231 J Hydroquinone SVOC 123-31-9 P1-Ptown 15-Jan-10 Dispersion HMW NM 28 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.37 MDL 2.65 M Methanol Alcohol 67-56-1 P1-Ptown 15-Jan-10 Dispersion HMW NM 12 MDL 16 MDL Phenol SVOC 108-95-2 P1-Ptown 15-Jan-10 Dispersion HMW NM 14 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.21 MDL 0.15 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.098 MDL 0.069 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 15-Jan-10 Dispersion HMW NM 90.6 M 0.26 M Xylene (total) VOC 1330-20-7 P1-Ptown 15-Jan-10 Dispersion HMW NM 0.34 MDL 0.24 MDL 1,1-Dichloroethane VOC 75-34-3 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.38 MDL 0.14 MDL 1,1-Dichloroethene VOC 75-35-4 P1-Ptown 16-Jan-10 Dispersion HMW NM 1.8 MDL 0.67 MDL 1,2-Dichloroethane VOC 107-06-2 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.95 MDL 0.467J 2,2,4-Trimethylpentane VOC 540-84-1 P1-Ptown 16-Jan-10 Dispersion HMW NM 2.2 MDL 0.8 MDL 2-Butanone (MEK) VOC 78-93-3 P1-Ptown 16-Jan-10 Dispersion HMW NM 5.4 MDL 2 MDL Acetaldehyde Aldehyde75-07-0 P1-Ptown 16-Jan-10 Dispersion HMW NM NM NM Acetophenone SVOC 98-86-2 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.22 MDL 1.8 MDL Benzene VOC 71-43-2 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.94 MDL 0.34 MDL Chloroethane VOC 75-00-3 P1-Ptown 16-Jan-10 Dispersion HMW NM 112 M 3.1 M Chloroform VOC 67-66-3 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.88 MDL 0.32 MDL

Dispersion Conc. Data Agg 0900006480f92db5.xls 16 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Chloromethane VOC 74-87-3 P1-Ptown 16-Jan-10 Dispersion HMW NM 19.5 M 0.17 MDL Formaldehyde Aldehyde50-00-0 P1-Ptown 16-Jan-10 Dispersion HMW NM NM NM Hydroquinone SVOC 123-31-9 P1-Ptown 16-Jan-10 Dispersion HMW NM 2.7 MDL 22 MDL Isopropylbenzene VOC 98-82-8 P1-Ptown 16-Jan-10 Dispersion HMW NM 1.4 MDL 0.595J Methanol Alcohol 67-56-1 P1-Ptown 16-Jan-10 Dispersion HMW NM 12 MDL 16 MDL Phenol SVOC 108-95-2 P1-Ptown 16-Jan-10 Dispersion HMW NM 1.3 MDL 11 MDL Toluene VOC 108-88-3 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.81 MDL 0.29 MDL Vinyl Bromide VOC 593-60-2 P1-Ptown 16-Jan-10 Dispersion HMW NM 0.38 MDL 0.14 MDL Vinyl chloride VOC 75-01-4 P1-Ptown 16-Jan-10 Dispersion HMW NM 517 M 0.517 M Xylene (total) VOC 1330-20-7 P1-Ptown 16-Jan-10 Dispersion HMW NM 1.3 MDL 0.47 MDL Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/2/2009 Dispersion HMW NM 148.79 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/3/2009 Dispersion HMW/LMW NM 178.43 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/4/2009 Dispersion HMW NM 241.18 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/5/2009 Dispersion HMW NM 120.38 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/6/2009 Dispersion HMW NM 256.17 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/7/2009 Dispersion HMW NM 188.26 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/8/2009 Dispersion HMW NM 184.87 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/9/2009 Dispersion HMW NM 110.25 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/10/2009 Dispersion HMW NM 190.25 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/11/2009 Dispersion HMW NM 352.98 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/12/2009 Dispersion HMW NM 270.71 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/13/2009 Dispersion HMW NM 144.98 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/14/2009 Dispersion HMW NM 142.75 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/15/2009 Dispersion HMW NM 237.24 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/16/2009 Dispersion HMW NM 90.94 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/17/2009 Dispersion HMW/LMW NM 151.21 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 12/18/2009 Dispersion HMW NM 216.76 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/4/2010 Dispersion HMW NM 166.06 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/5/2010 Dispersion HMW/LMW NM 163.5 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/6/2010 Dispersion HMW/LMW NM 159.33 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/7/2010 Dispersion HMW NM 242.89 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/8/2010 Dispersion HMW NM 351.79 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/9/2010 Dispersion HMW NM 202.98 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/10/2010 Dispersion HMW NM 200.59 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/11/2010 Dispersion HMW NM 144.78 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/12/2010 Dispersion HMW NM 232.57 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/13/2010 Dispersion HMW NM 138.13 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/14/2010 Dispersion HMW NM 219.19 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/15/2010 Dispersion HMW NM 212.59 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Ptown 1/16/2010 Dispersion HMW NM 211.52 M NM 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.36 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/9/2009 Dispersion HMW NM 660 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/9/2009 Dispersion HMW NM 500 U 500 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/9/2009 Dispersion HMW NM 500 U 500 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U MEK VOC 78-93-3 P1-Henry 12/9/2009 Dispersion HMW NM 13 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/9/2009 Dispersion HMW NM 33 U 1.1 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 17 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Acetaldehyde Aldehyde75-07-0 P1-Henry 12/9/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/9/2009 Dispersion HMW NM 130 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Acrolein VOC 107-02-8 P1-Henry 12/9/2009 Dispersion HMW NM 66 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 12/9/2009 Dispersion HMW NM 66 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Benzene VOC 71-43-2 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 12/9/2009 Dispersion HMW NM 13 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 12/9/2009 Dispersion HMW NM 13 U 0.45 U Chloroform VOC 67-66-3 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 12/9/2009 Dispersion HMW NM 13 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 12/9/2009 Dispersion HMW NM 33 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Ethylbenzene VOC 100-41-4 P1-Henry 12/9/2009 Dispersion HMW NM 2.6 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/9/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Hexane VOC 110-54-3 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 12/9/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/9/2009 Dispersion HMW NM 100 U 100 U o-Xylene VOC 95-47-6 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/9/2009 Dispersion HMW NM 500 U 500 U Styrene VOC 100-42-5 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Toluene VOC 108-88-3 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 12/9/2009 Dispersion HMW NM 6.6 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/9/2009 Dispersion HMW NM 13 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/9/2009 Dispersion HMW NM 94 M 2.5 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/9/2009 Dispersion HMW NM 13 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/10/2009 Dispersion HMW NM 370 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/10/2009 Dispersion HMW NM 500 U 500 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 18 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/10/2009 Dispersion HMW NM 500 U 500 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U MEK VOC 78-93-3 P1-Henry 12/10/2009 Dispersion HMW NM 7.4 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/10/2009 Dispersion HMW NM 18 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/10/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/10/2009 Dispersion HMW NM 74 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Acrolein VOC 107-02-8 P1-Henry 12/10/2009 Dispersion HMW NM 37 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 12/10/2009 Dispersion HMW NM 37 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Benzene VOC 71-43-2 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 12/10/2009 Dispersion HMW NM 7.4 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 12/10/2009 Dispersion HMW NM 7.4 U 0.45 U Chloroform VOC 67-66-3 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 12/10/2009 Dispersion HMW NM 7.4 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 12/10/2009 Dispersion HMW NM 18 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Ethylbenzene VOC 100-41-4 P1-Henry 12/10/2009 Dispersion HMW NM 1.5 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/10/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Hexane VOC 110-54-3 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U m,p-Xylene VOC 106-42-3 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 12/10/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/10/2009 Dispersion HMW NM 100 U 100 U o-Xylene VOC 95-47-6 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/10/2009 Dispersion HMW NM 500 U 500 U Styrene VOC 100-42-5 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Toluene VOC 108-88-3 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 12/10/2009 Dispersion HMW NM 3.7 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/10/2009 Dispersion HMW NM 7.4 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/10/2009 Dispersion HMW NM 100 M 1.7 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/10/2009 Dispersion HMW NM 7.4 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 19 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/11/2009 Dispersion HMW NM 140 U 28 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/11/2009 Dispersion HMW NM 500 U 500 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/11/2009 Dispersion HMW NM 500 U 500 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U MEK VOC 78-93-3 P1-Henry 12/11/2009 Dispersion HMW NM 2.8 U 0.56 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/11/2009 Dispersion HMW NM 6.9 U 1.4 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/11/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/11/2009 Dispersion HMW NM 28 U 5.6 U Acetophenone SVOC 98-86-2 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Acrolein VOC 107-02-8 P1-Henry 12/11/2009 Dispersion HMW NM 14 U 2.8 U Acrylonitrile VOC 107-13-1 P1-Henry 12/11/2009 Dispersion HMW NM 14 U 2.8 U Allyl Chloride VOC 107-05-1 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Benzene VOC 71-43-2 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Bromoform VOC 75-25-2 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Bromomethane VOC 74-83-9 P1-Henry 12/11/2009 Dispersion HMW NM 2.8 U 0.56 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Chlorobenzene VOC 108-90-7 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Chloroethane VOC 75-00-3 P1-Henry 12/11/2009 Dispersion HMW NM 2.8 U 0.56 U Chloroform VOC 67-66-3 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Chloromethane VOC 74-87-3 P1-Henry 12/11/2009 Dispersion HMW NM 2.8 U 0.56 U Chloroprene VOC 126-99-8 P1-Henry 12/11/2009 Dispersion HMW NM 6.9 U 1.4 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Ethylbenzene VOC 100-41-4 P1-Henry 12/11/2009 Dispersion HMW NM 0.56 U 0.11 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/11/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Hexane VOC 110-54-3 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Iodomethane VOC 74-88-4 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Isophorone SVOC 78-59-1 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U m,p-Xylene VOC 106-42-3 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Methanol Alcohol 67-56-1 P1-Henry 12/11/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Methylene Chloride VOC 75-09-2 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Naphthalene SVOC 91-20-3 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/11/2009 Dispersion HMW NM 100 U 100 U o-Xylene VOC 95-47-6 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/11/2009 Dispersion HMW NM 500 U 500 U Styrene VOC 100-42-5 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Toluene VOC 108-88-3 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Trichloroethene VOC 79-01-6 P1-Henry 12/11/2009 Dispersion HMW NM 1.4 U 0.28 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/11/2009 Dispersion HMW NM 2.8 U 0.56 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/11/2009 Dispersion HMW NM 110 M 0.56 U Xylenes (Total) VOC 1330-20-7 P1-Henry 12/11/2009 Dispersion HMW NM 2.8 U 0.56 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 F<

Dispersion Conc. Data Agg 0900006480f92db5.xls 20 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/12/2009 Dispersion HMW NM 180 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/12/2009 Dispersion HMW NM 5000 U 500 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/12/2009 Dispersion HMW NM 5000 U 500 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U MEK VOC 78-93-3 P1-Henry 12/12/2009 Dispersion HMW NM 3.5 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/12/2009 Dispersion HMW NM 8.8 U 1.2 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/12/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/12/2009 Dispersion HMW NM 35 U 5 U Acetophenone SVOC 98-86-2 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Acrolein VOC 107-02-8 P1-Henry 12/12/2009 Dispersion HMW NM 18 U 2.5 U Acrylonitrile VOC 107-13-1 P1-Henry 12/12/2009 Dispersion HMW NM 18 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Benzene VOC 71-43-2 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Bromomethane VOC 74-83-9 P1-Henry 12/12/2009 Dispersion HMW NM 3.5 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Chloroethane VOC 75-00-3 P1-Henry 12/12/2009 Dispersion HMW NM 3.5 U 0.5 U Chloroform VOC 67-66-3 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Chloromethane VOC 74-87-3 P1-Henry 12/12/2009 Dispersion HMW NM 3.5 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 12/12/2009 Dispersion HMW NM 8.8 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Ethylbenzene VOC 100-41-4 P1-Henry 12/12/2009 Dispersion HMW NM 0.7 U 0.1 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/12/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Hexane VOC 110-54-3 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Methanol Alcohol 67-56-1 P1-Henry 12/12/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Methylene Chloride VOC 75-09-2 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/12/2009 Dispersion HMW NM 1000 U 100 U o-Xylene VOC 95-47-6 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/12/2009 Dispersion HMW NM 5000 U 500 U Styrene VOC 100-42-5 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Toluene VOC 108-88-3 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 12/12/2009 Dispersion HMW NM 1.8 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/12/2009 Dispersion HMW NM 3.5 U 0.5 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/12/2009 Dispersion HMW NM 99 M 0.5 U Xylenes (Total) VOC 1330-20-7 P1-Henry 12/12/2009 Dispersion HMW NM 3.5 U 0.5 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 F<

Dispersion Conc. Data Agg 0900006480f92db5.xls 21 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/13/2009 Dispersion HMW NM 180 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/13/2009 Dispersion HMW NM 500 U 500 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/13/2009 Dispersion HMW NM 500 U 500 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U MEK VOC 78-93-3 P1-Henry 12/13/2009 Dispersion HMW NM 3.5 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/13/2009 Dispersion HMW NM 8.8 U 1.2 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/13/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/13/2009 Dispersion HMW NM 35 U 5 U Acetophenone SVOC 98-86-2 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Acrolein VOC 107-02-8 P1-Henry 12/13/2009 Dispersion HMW NM 18 U 2.5 U Acrylonitrile VOC 107-13-1 P1-Henry 12/13/2009 Dispersion HMW NM 18 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Benzene VOC 71-43-2 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Bromomethane VOC 74-83-9 P1-Henry 12/13/2009 Dispersion HMW NM 3.5 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Chloroethane VOC 75-00-3 P1-Henry 12/13/2009 Dispersion HMW NM 3.5 U 0.5 U Chloroform VOC 67-66-3 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Chloromethane VOC 74-87-3 P1-Henry 12/13/2009 Dispersion HMW NM 3.5 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 12/13/2009 Dispersion HMW NM 8.8 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Ethylbenzene VOC 100-41-4 P1-Henry 12/13/2009 Dispersion HMW NM 0.7 U 0.1 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/13/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Hexane VOC 110-54-3 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Methanol Alcohol 67-56-1 P1-Henry 12/13/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Methylene Chloride VOC 75-09-2 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/13/2009 Dispersion HMW NM 100 U 100 U o-Xylene VOC 95-47-6 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/13/2009 Dispersion HMW NM 500 U 500 U Styrene VOC 100-42-5 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Toluene VOC 108-88-3 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 12/13/2009 Dispersion HMW NM 1.8 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/13/2009 Dispersion HMW NM 3.5 U 0.5 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 22 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Vinyl Chloride VOC 75-01-4 P1-Henry 12/13/2009 Dispersion HMW NM 350 M 0.5 U Xylenes (Total) VOC 1330-20-7 P1-Henry 12/13/2009 Dispersion HMW NM 3.5 U 0.5 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.28 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/14/2009 Dispersion HMW NM 17 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/14/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/14/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.35 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/14/2009 Dispersion HMW NM 0.86 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/14/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/14/2009 Dispersion HMW NM 3.5 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/14/2009 Dispersion HMW NM 1.7 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 12/14/2009 Dispersion HMW NM 1.7 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Benzene VOC 71-43-2 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 12/14/2009 Dispersion HMW NM 0.35 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.35 U 0.45 U Chloroform VOC 67-66-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.35 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 12/14/2009 Dispersion HMW NM 0.86 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.069 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/14/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 12/14/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/14/2009 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/14/2009 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 23 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Toluene VOC 108-88-3 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 12/14/2009 Dispersion HMW NM 0.17 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/14/2009 Dispersion HMW NM 0.35 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/14/2009 Dispersion HMW NM 100 M 1.5 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/14/2009 Dispersion HMW NM 0.35 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.26 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/15/2009 Dispersion HMW NM 180 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/15/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/15/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/15/2009 Dispersion HMW NM 3.6 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/15/2009 Dispersion HMW NM 8.9 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/15/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/15/2009 Dispersion HMW NM 36 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/15/2009 Dispersion HMW NM 18 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 12/15/2009 Dispersion HMW NM 18 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Benzene VOC 71-43-2 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 12/15/2009 Dispersion HMW NM 3.6 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 12/15/2009 Dispersion HMW NM 3.6 U 0.45 U Chloroform VOC 67-66-3 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 12/15/2009 Dispersion HMW NM 3.6 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 12/15/2009 Dispersion HMW NM 8.9 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 12/15/2009 Dispersion HMW NM 0.71 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/15/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 12/15/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/15/2009 Dispersion HMW NM 1000 U 1000 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 24 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type o-Xylene VOC 95-47-6 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/15/2009 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Toluene VOC 108-88-3 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 12/15/2009 Dispersion HMW NM 1.8 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/15/2009 Dispersion HMW NM 3.6 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/15/2009 Dispersion HMW NM 96 M 0.66 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/15/2009 Dispersion HMW NM 3.6 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/16/2009 Dispersion HMW NM 160 U 31 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/16/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/16/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/16/2009 Dispersion HMW NM 3.2 U 0.62 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/16/2009 Dispersion HMW NM 7.9 U 1.6 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/16/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/16/2009 Dispersion HMW NM 32 U 6.2 U Acetophenone SVOC 98-86-2 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/16/2009 Dispersion HMW NM 16 U 3.1 U Acrylonitrile VOC 107-13-1 P1-Henry 12/16/2009 Dispersion HMW NM 16 U 3.1 U Allyl Chloride VOC 107-05-1 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Benzene VOC 71-43-2 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Bromoform VOC 75-25-2 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Bromomethane VOC 74-83-9 P1-Henry 12/16/2009 Dispersion HMW NM 3.2 U 0.62 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Chlorobenzene VOC 108-90-7 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Chloroethane VOC 75-00-3 P1-Henry 12/16/2009 Dispersion HMW NM 3.2 U 0.62 U Chloroform VOC 67-66-3 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Chloromethane VOC 74-87-3 P1-Henry 12/16/2009 Dispersion HMW NM 3.2 U 0.62 U Chloroprene VOC 126-99-8 P1-Henry 12/16/2009 Dispersion HMW NM 7.9 U 1.6 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 12/16/2009 Dispersion HMW NM 0.63 U 0.12 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/16/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Iodomethane VOC 74-88-4 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Isophorone SVOC 78-59-1 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Methanol Alcohol 67-56-1 P1-Henry 12/16/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 25 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Methylene Chloride VOC 75-09-2 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Naphthalene SVOC 91-20-3 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/16/2009 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/16/2009 Dispersion HMW NM 5000 U NM Styrene VOC 100-42-5 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Toluene VOC 108-88-3 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Trichloroethene VOC 79-01-6 P1-Henry 12/16/2009 Dispersion HMW NM 1.6 U 0.31 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/16/2009 Dispersion HMW NM 3.2 U 0.62 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/16/2009 Dispersion HMW NM 63 M 0.71 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/16/2009 Dispersion HMW NM 3.2 U 0.62 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/17/2009 Dispersion HMW NM 19 U 19 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/17/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/17/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.38 U 0.38 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/17/2009 Dispersion HMW NM 0.96 U 0.96 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/17/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/17/2009 Dispersion HMW NM 3.8 U 3.8 U Acetophenone SVOC 98-86-2 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/17/2009 Dispersion HMW NM 1.9 U 1.9 U Acrylonitrile VOC 107-13-1 P1-Henry 12/17/2009 Dispersion HMW NM 1.9 U 1.9 U Allyl Chloride VOC 107-05-1 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Benzene VOC 71-43-2 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Bromoform VOC 75-25-2 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Bromomethane VOC 74-83-9 P1-Henry 12/17/2009 Dispersion HMW NM 0.38 U 0.38 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Chlorobenzene VOC 108-90-7 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Chloroethane VOC 75-00-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.38 U 0.38 U Chloroform VOC 67-66-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Chloromethane VOC 74-87-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.38 U 0.38 U Chloroprene VOC 126-99-8 P1-Henry 12/17/2009 Dispersion HMW NM 0.96 U 0.96 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.077 U 0.077 U Formaldehyde Aldehyde50-00-0 P1-Henry 12/17/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Iodomethane VOC 74-88-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Isophorone SVOC 78-59-1 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 26 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Isopropylbenzene VOC 98-82-8 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U m,p-Xylene VOC 106-42-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Methanol Alcohol 67-56-1 P1-Henry 12/17/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Methylene Chloride VOC 75-09-2 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Naphthalene SVOC 91-20-3 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/17/2009 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Pentachlorophenol SVOC 87-86-5 P1-Henry 12/17/2009 Dispersion HMW NM 5000 U NM Styrene VOC 100-42-5 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Tetrachloroethene VOC 127-18-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Toluene VOC 108-88-3 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Trichloroethene VOC 79-01-6 P1-Henry 12/17/2009 Dispersion HMW NM 0.19 U 0.19 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/17/2009 Dispersion HMW NM 0.38 U 0.38 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/17/2009 Dispersion HMW NM 5 M 0.32 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/17/2009 Dispersion HMW NM 0.38 U 0.38 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.26 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/18/2009 Dispersion HMW NM 440 U 12 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/18/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/18/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/18/2009 Dispersion HMW NM 8.8 U 0.24 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/18/2009 Dispersion HMW NM 22 U 0.6 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/18/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/18/2009 Dispersion HMW NM 88 U 2.4 U Acetophenone SVOC 98-86-2 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/18/2009 Dispersion HMW NM 44 U 1.2 U Acrylonitrile VOC 107-13-1 P1-Henry 12/18/2009 Dispersion HMW NM 44 U 1.2 U Allyl Chloride VOC 107-05-1 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Benzene VOC 71-43-2 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Bromoform VOC 75-25-2 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Bromomethane VOC 74-83-9 P1-Henry 12/18/2009 Dispersion HMW NM 8.8 U 0.24 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Chlorobenzene VOC 108-90-7 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Chloroethane VOC 75-00-3 P1-Henry 12/18/2009 Dispersion HMW NM 8.8 U 0.16 M Chloroform VOC 67-66-3 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Chloromethane VOC 74-87-3 P1-Henry 12/18/2009 Dispersion HMW NM 8.8 U 0.24 U Chloroprene VOC 126-99-8 P1-Henry 12/18/2009 Dispersion HMW NM 22 U 0.6 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 12/18/2009 Dispersion HMW NM 1.8 U 0.048 F< Formaldehyde Aldehyde50-00-0 P1-Henry 12/18/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 27 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Hexachloroethane SVOC 67-72-1 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Iodomethane VOC 74-88-4 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Isophorone SVOC 78-59-1 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Methanol Alcohol 67-56-1 P1-Henry 12/18/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Methylene Chloride VOC 75-09-2 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Naphthalene SVOC 91-20-3 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/18/2009 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Pentachlorophenol SVOC 87-86-5 P1-Henry 12/18/2009 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Tetrachloroethene VOC 127-18-4 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 F< Toluene VOC 108-88-3 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Trichloroethene VOC 79-01-6 P1-Henry 12/18/2009 Dispersion HMW NM 4.4 U 0.12 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/18/2009 Dispersion HMW NM 8.8 U 0.24 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/18/2009 Dispersion HMW NM 62 M 0.197 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/18/2009 Dispersion HMW NM 8.8 U 0.24 F< 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.36 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/19/2009 Dispersion HMW NM 270 U 21 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/19/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/19/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/19/2009 Dispersion HMW NM 5.5 U 0.42 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/19/2009 Dispersion HMW NM 14 U 1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/19/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/19/2009 Dispersion HMW NM 55 U 4.2 U Acetophenone SVOC 98-86-2 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/19/2009 Dispersion HMW NM 27 U 2.1 U Acrylonitrile VOC 107-13-1 P1-Henry 12/19/2009 Dispersion HMW NM 27 U 2.1 U Allyl Chloride VOC 107-05-1 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Benzene VOC 71-43-2 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Bromoform VOC 75-25-2 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Bromomethane VOC 74-83-9 P1-Henry 12/19/2009 Dispersion HMW NM 5.5 U 0.42 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Chlorobenzene VOC 108-90-7 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Chloroethane VOC 75-00-3 P1-Henry 12/19/2009 Dispersion HMW NM 5.5 U 0.42 U Chloroform VOC 67-66-3 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Chloromethane VOC 74-87-3 P1-Henry 12/19/2009 Dispersion HMW NM 5.5 U 0.42 U Chloroprene VOC 126-99-8 P1-Henry 12/19/2009 Dispersion HMW NM 14 U 1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 28 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Ethylbenzene VOC 100-41-4 P1-Henry 12/19/2009 Dispersion HMW NM 1.1 U 0.083 F< Formaldehyde Aldehyde50-00-0 P1-Henry 12/19/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Iodomethane VOC 74-88-4 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Isophorone SVOC 78-59-1 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Methanol Alcohol 67-56-1 P1-Henry 12/19/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Methylene Chloride VOC 75-09-2 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Naphthalene SVOC 91-20-3 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/19/2009 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Pentachlorophenol SVOC 87-86-5 P1-Henry 12/19/2009 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Tetrachloroethene VOC 127-18-4 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 F< Toluene VOC 108-88-3 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Trichloroethene VOC 79-01-6 P1-Henry 12/19/2009 Dispersion HMW NM 2.7 U 0.21 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/19/2009 Dispersion HMW NM 5.5 U 0.42 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/19/2009 Dispersion HMW NM 55 M 0.31 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/19/2009 Dispersion HMW NM 5.5 U 0.42 F< 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< 1,2-Dichloroethane VOC 107-06-2 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.35 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 12/20/2009 Dispersion HMW NM 520 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 12/20/2009 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 12/20/2009 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 12/20/2009 Dispersion HMW NM 10 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 12/20/2009 Dispersion HMW NM 26 U 1.2 U Acetaldehyde Aldehyde75-07-0 P1-Henry 12/20/2009 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 12/20/2009 Dispersion HMW NM 100 U 5 U Acetophenone SVOC 98-86-2 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 12/20/2009 Dispersion HMW NM 52 U 2.5 U Acrylonitrile VOC 107-13-1 P1-Henry 12/20/2009 Dispersion HMW NM 52 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Benzene VOC 71-43-2 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Bromomethane VOC 74-83-9 P1-Henry 12/20/2009 Dispersion HMW NM 10 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Chloroethane VOC 75-00-3 P1-Henry 12/20/2009 Dispersion HMW NM 10 U 0.5 U Chloroform VOC 67-66-3 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 29 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Chloromethane VOC 74-87-3 P1-Henry 12/20/2009 Dispersion HMW NM 10 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 12/20/2009 Dispersion HMW NM 26 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 12/20/2009 Dispersion HMW NM 2.1 U 0.1 F< Formaldehyde Aldehyde50-00-0 P1-Henry 12/20/2009 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< m,p-Xylene VOC 106-42-3 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Methanol Alcohol 67-56-1 P1-Henry 12/20/2009 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Methylene Chloride VOC 75-09-2 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 12/20/2009 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Pentachlorophenol SVOC 87-86-5 P1-Henry 12/20/2009 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Tetrachloroethene VOC 127-18-4 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 F< Toluene VOC 108-88-3 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 12/20/2009 Dispersion HMW NM 5.2 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 12/20/2009 Dispersion HMW NM 10 U 0.5 U Vinyl Chloride VOC 75-01-4 P1-Henry 12/20/2009 Dispersion HMW NM 64 M 0.37 M Xylenes (Total) VOC 1330-20-7 P1-Henry 12/20/2009 Dispersion HMW NM 10 U 0.5 F< 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/5/2010 Dispersion HMW NM 810 U 28 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/5/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/5/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/5/2010 Dispersion HMW NM 16 U 0.56 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/5/2010 Dispersion HMW NM 40 U 1.4 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/5/2010 Dispersion HMW NM 50X< 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/5/2010 Dispersion HMW NM 160 U 5.6 U Acetophenone SVOC 98-86-2 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/5/2010 Dispersion HMW NM 81 U 2.8 U Acrylonitrile VOC 107-13-1 P1-Henry 1/5/2010 Dispersion HMW NM 81 U 2.8 U Allyl Chloride VOC 107-05-1 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Benzene VOC 71-43-2 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Bromoform VOC 75-25-2 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Bromomethane VOC 74-83-9 P1-Henry 1/5/2010 Dispersion HMW NM 16 U 0.56 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 30 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Chlorobenzene VOC 108-90-7 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Chloroethane VOC 75-00-3 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.42 M Chloroform VOC 67-66-3 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Chloromethane VOC 74-87-3 P1-Henry 1/5/2010 Dispersion HMW NM 16 U 0.56 U Chloroprene VOC 126-99-8 P1-Henry 1/5/2010 Dispersion HMW NM 40 U 1.4 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/5/2010 Dispersion HMW NM 3.2 U 0.11 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/5/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Iodomethane VOC 74-88-4 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Isophorone SVOC 78-59-1 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Methanol Alcohol 67-56-1 P1-Henry 1/5/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Methylene Chloride VOC 75-09-2 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Naphthalene SVOC 91-20-3 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/5/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/5/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Toluene VOC 108-88-3 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Trichloroethene VOC 79-01-6 P1-Henry 1/5/2010 Dispersion HMW NM 8.1 U 0.28 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/5/2010 Dispersion HMW NM 16 U 0.56 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/5/2010 Dispersion HMW NM 110 M 2.5 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/5/2010 Dispersion HMW NM 16 U 0.56 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/6/2010 Dispersion HMW NM 340 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/6/2010 Dispersion HMW NM NM 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/6/2010 Dispersion HMW NM NM 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U MEK VOC 78-93-3 P1-Henry 1/6/2010 Dispersion HMW NM 6.8 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/6/2010 Dispersion HMW NM 17 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/6/2010 Dispersion HMW NM 50X< 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/6/2010 Dispersion HMW NM 68 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Acrolein VOC 107-02-8 P1-Henry 1/6/2010 Dispersion HMW NM 34 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/6/2010 Dispersion HMW NM 34 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 31 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Benzene VOC 71-43-2 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 1/6/2010 Dispersion HMW NM 6.8 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.33 M Chloroform VOC 67-66-3 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 1/6/2010 Dispersion HMW NM 6.8 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 1/6/2010 Dispersion HMW NM 17 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/6/2010 Dispersion HMW NM 1.4 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/6/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Hexane VOC 110-54-3 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 1/6/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/6/2010 Dispersion HMW NM NM 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/6/2010 Dispersion HMW NM NM 5000 U Styrene VOC 100-42-5 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Toluene VOC 108-88-3 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 1/6/2010 Dispersion HMW NM 3.4 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/6/2010 Dispersion HMW NM 6.8 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/6/2010 Dispersion HMW NM 95 M 3.3 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/6/2010 Dispersion HMW NM 6.8 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.38 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/7/2010 Dispersion HMW NM 360 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/7/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/7/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/7/2010 Dispersion HMW NM 7.1 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/7/2010 Dispersion HMW NM 18 U 1.2 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/7/2010 Dispersion HMW NM 50X< 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/7/2010 Dispersion HMW NM 71 U 5 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 32 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Acetophenone SVOC 98-86-2 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/7/2010 Dispersion HMW NM 36 U 2.5 U Acrylonitrile VOC 107-13-1 P1-Henry 1/7/2010 Dispersion HMW NM 36 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Benzene VOC 71-43-2 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Bromomethane VOC 74-83-9 P1-Henry 1/7/2010 Dispersion HMW NM 7.1 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Chloroethane VOC 75-00-3 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 M Chloroform VOC 67-66-3 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Chloromethane VOC 74-87-3 P1-Henry 1/7/2010 Dispersion HMW NM 7.1 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 1/7/2010 Dispersion HMW NM 18 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/7/2010 Dispersion HMW NM 1.4 U 0.1 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/7/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Methanol Alcohol 67-56-1 P1-Henry 1/7/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Methylene Chloride VOC 75-09-2 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/7/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/7/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Toluene VOC 108-88-3 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 1/7/2010 Dispersion HMW NM 3.6 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/7/2010 Dispersion HMW NM 7.1 U 0.5 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/7/2010 Dispersion HMW NM 79 M 1.4 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/7/2010 Dispersion HMW NM 7.1 U 0.5 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.29 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/8/2010 Dispersion HMW NM 640 U 18 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/8/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/8/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 33 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type MEK VOC 78-93-3 P1-Henry 1/8/2010 Dispersion HMW NM 13 U 0.36 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/8/2010 Dispersion HMW NM 32 U 0.89 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/8/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/8/2010 Dispersion HMW NM 130 U 3.6 U Acetophenone SVOC 98-86-2 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/8/2010 Dispersion HMW NM 64 U 1.8 U Acrylonitrile VOC 107-13-1 P1-Henry 1/8/2010 Dispersion HMW NM 64 U 1.8 U Allyl Chloride VOC 107-05-1 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Benzene VOC 71-43-2 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Bromoform VOC 75-25-2 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Bromomethane VOC 74-83-9 P1-Henry 1/8/2010 Dispersion HMW NM 13 U 0.36 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Chlorobenzene VOC 108-90-7 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Chloroethane VOC 75-00-3 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.23 M Chloroform VOC 67-66-3 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Chloromethane VOC 74-87-3 P1-Henry 1/8/2010 Dispersion HMW NM 13 U 0.36 U Chloroprene VOC 126-99-8 P1-Henry 1/8/2010 Dispersion HMW NM 32 U 0.89 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/8/2010 Dispersion HMW NM 2.6 U 0.071 F< Formaldehyde Aldehyde50-00-0 P1-Henry 1/8/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Iodomethane VOC 74-88-4 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Isophorone SVOC 78-59-1 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Methanol Alcohol 67-56-1 P1-Henry 1/8/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Methylene Chloride VOC 75-09-2 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Naphthalene SVOC 91-20-3 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/8/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Pentachlorophenol SVOC 87-86-5 P1-Henry 1/8/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Tetrachloroethene VOC 127-18-4 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 F< Toluene VOC 108-88-3 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Trichloroethene VOC 79-01-6 P1-Henry 1/8/2010 Dispersion HMW NM 6.4 U 0.18 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/8/2010 Dispersion HMW NM 13 U 0.36 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/8/2010 Dispersion HMW NM 15 M 0.56 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/8/2010 Dispersion HMW NM 13 U 0.36 F< 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/9/2010 Dispersion HMW NM 540 U 23 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 34 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/9/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/9/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/9/2010 Dispersion HMW NM 11 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/9/2010 Dispersion HMW NM 27 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/9/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/9/2010 Dispersion HMW NM 110 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/9/2010 Dispersion HMW NM 54 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/9/2010 Dispersion HMW NM 54 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Benzene VOC 71-43-2 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 1/9/2010 Dispersion HMW NM 11 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Chloroform VOC 67-66-3 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 1/9/2010 Dispersion HMW NM 11 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 1/9/2010 Dispersion HMW NM 27 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/9/2010 Dispersion HMW NM 2.2 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/9/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 1/9/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/9/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/9/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Toluene VOC 108-88-3 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 1/9/2010 Dispersion HMW NM 5.4 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/9/2010 Dispersion HMW NM 11 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/9/2010 Dispersion HMW NM 76 M 0.59 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/9/2010 Dispersion HMW NM 11 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 F < 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 F < 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 F < 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 35 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.26 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/10/2010 Dispersion HMW NM 370 U 21 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/10/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/10/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/10/2010 Dispersion HMW NM 7.4 U 0.42 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/10/2010 Dispersion HMW NM 18 U 1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/10/2010 Dispersion HMW NM 50X< 50X< Acetonitrile VOC 75-05-8 P1-Henry 1/10/2010 Dispersion HMW NM 74 U 4.2 U Acetophenone SVOC 98-86-2 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/10/2010 Dispersion HMW NM 37 U 2.1 U Acrylonitrile VOC 107-13-1 P1-Henry 1/10/2010 Dispersion HMW NM 37 U 2.1 U Allyl Chloride VOC 107-05-1 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Benzene VOC 71-43-2 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Bromoform VOC 75-25-2 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Bromomethane VOC 74-83-9 P1-Henry 1/10/2010 Dispersion HMW NM 7.4 U 0.42 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Chlorobenzene VOC 108-90-7 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Chloroethane VOC 75-00-3 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Chloroform VOC 67-66-3 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Chloromethane VOC 74-87-3 P1-Henry 1/10/2010 Dispersion HMW NM 7.4 U 0.42 U Chloroprene VOC 126-99-8 P1-Henry 1/10/2010 Dispersion HMW NM 18 U 1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/10/2010 Dispersion HMW NM 1.5 U 0.083 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/10/2010 Dispersion HMW NM 50X< 50X< Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Iodomethane VOC 74-88-4 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Isophorone SVOC 78-59-1 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 F < m,p-Xylene VOC 106-42-3 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Methanol Alcohol 67-56-1 P1-Henry 1/10/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Methylene Chloride VOC 75-09-2 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Naphthalene SVOC 91-20-3 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/10/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/10/2010 Dispersion HMW NM NM NM Styrene VOC 100-42-5 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Toluene VOC 108-88-3 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Trichloroethene VOC 79-01-6 P1-Henry 1/10/2010 Dispersion HMW NM 3.7 U 0.21 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/10/2010 Dispersion HMW NM 7.4 U 0.42 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/10/2010 Dispersion HMW NM 130 M 0.27 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/10/2010 Dispersion HMW NM 7.4 U 0.42 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 F < 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 36 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 F < 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 F < 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/11/2010 Dispersion HMW NM 420 U 13 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/11/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/11/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/11/2010 Dispersion HMW NM 8.5 U 0.26 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/11/2010 Dispersion HMW NM 21 U 0.66 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/11/2010 Dispersion HMW NM 50 U 50X< Acetonitrile VOC 75-05-8 P1-Henry 1/11/2010 Dispersion HMW NM 85 U 2.6 U Acetophenone SVOC 98-86-2 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/11/2010 Dispersion HMW NM 42 U 1.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/11/2010 Dispersion HMW NM 42 U 1.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Benzene VOC 71-43-2 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Bromoform VOC 75-25-2 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Bromomethane VOC 74-83-9 P1-Henry 1/11/2010 Dispersion HMW NM 8.5 U 0.26 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Chlorobenzene VOC 108-90-7 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Chloroethane VOC 75-00-3 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Chloroform VOC 67-66-3 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Chloromethane VOC 74-87-3 P1-Henry 1/11/2010 Dispersion HMW NM 8.5 U 0.26 U Chloroprene VOC 126-99-8 P1-Henry 1/11/2010 Dispersion HMW NM 21 U 0.66 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/11/2010 Dispersion HMW NM 1.7 U 0.053 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/11/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Iodomethane VOC 74-88-4 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Isophorone SVOC 78-59-1 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 F < m,p-Xylene VOC 106-42-3 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Methanol Alcohol 67-56-1 P1-Henry 1/11/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Methylene Chloride VOC 75-09-2 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Naphthalene SVOC 91-20-3 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/11/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/11/2010 Dispersion HMW NM NM NM Styrene VOC 100-42-5 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Toluene VOC 108-88-3 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Trichloroethene VOC 79-01-6 P1-Henry 1/11/2010 Dispersion HMW NM 4.2 U 0.13 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/11/2010 Dispersion HMW NM 8.5 U 0.26 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/11/2010 Dispersion HMW NM 250 E 0.4 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/11/2010 Dispersion HMW NM 8.5 U 0.26 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 37 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 F < 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 F < 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 F < 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.36 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/12/2010 Dispersion HMW NM 420 U 18 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/12/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/12/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/12/2010 Dispersion HMW NM 8.3 U 0.36 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/12/2010 Dispersion HMW NM 21 U 0.89 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/12/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/12/2010 Dispersion HMW NM 83 U 3.6 U Acetophenone SVOC 98-86-2 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/12/2010 Dispersion HMW NM 42 U 1.8 U Acrylonitrile VOC 107-13-1 P1-Henry 1/12/2010 Dispersion HMW NM 42 U 1.8 U Allyl Chloride VOC 107-05-1 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Benzene VOC 71-43-2 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Bromoform VOC 75-25-2 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Bromomethane VOC 74-83-9 P1-Henry 1/12/2010 Dispersion HMW NM 8.3 U 0.36 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Chlorobenzene VOC 108-90-7 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Chloroethane VOC 75-00-3 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Chloroform VOC 67-66-3 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Chloromethane VOC 74-87-3 P1-Henry 1/12/2010 Dispersion HMW NM 8.3 U 0.36 U Chloroprene VOC 126-99-8 P1-Henry 1/12/2010 Dispersion HMW NM 21 U 0.89 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/12/2010 Dispersion HMW NM 1.7 U 0.071 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/12/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Iodomethane VOC 74-88-4 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Isophorone SVOC 78-59-1 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 F < m,p-Xylene VOC 106-42-3 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Methanol Alcohol 67-56-1 P1-Henry 1/12/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Methylene Chloride VOC 75-09-2 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Naphthalene SVOC 91-20-3 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/12/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/12/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Toluene VOC 108-88-3 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 38 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Trichloroethene VOC 79-01-6 P1-Henry 1/12/2010 Dispersion HMW NM 4.2 U 0.18 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/12/2010 Dispersion HMW NM 8.3 U 0.36 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/12/2010 Dispersion HMW NM 150 M 0.78 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/12/2010 Dispersion HMW NM 8.3 U 0.36 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/13/2010 Dispersion HMW NM 510 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/13/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/13/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/13/2010 Dispersion HMW NM 10 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/13/2010 Dispersion HMW NM 26 U 1.2 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/13/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/13/2010 Dispersion HMW NM 100 U 5 U Acetophenone SVOC 98-86-2 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/13/2010 Dispersion HMW NM 51 U 2.5 U Acrylonitrile VOC 107-13-1 P1-Henry 1/13/2010 Dispersion HMW NM 51 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Benzene VOC 71-43-2 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Bromomethane VOC 74-83-9 P1-Henry 1/13/2010 Dispersion HMW NM 10 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Chloroethane VOC 75-00-3 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Chloroform VOC 67-66-3 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Chloromethane VOC 74-87-3 P1-Henry 1/13/2010 Dispersion HMW NM 10 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 1/13/2010 Dispersion HMW NM 26 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/13/2010 Dispersion HMW NM 2 U 0.1 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/13/2010 Dispersion HMW NM 50Q< 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U m,p-Xylene VOC 106-42-3 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Methanol Alcohol 67-56-1 P1-Henry 1/13/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Methylene Chloride VOC 75-09-2 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/13/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/13/2010 Dispersion HMW NM 5000 U 5000 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 39 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Styrene VOC 100-42-5 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Toluene VOC 108-88-3 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 1/13/2010 Dispersion HMW NM 5.1 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/13/2010 Dispersion HMW NM 10 U 0.5 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/13/2010 Dispersion HMW NM 140 M 1.2 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/13/2010 Dispersion HMW NM 10 U 0.5 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 F < 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 F < 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 F < 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.3 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/14/2010 Dispersion HMW NM 490 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/14/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/14/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/14/2010 Dispersion HMW NM 9.8 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/14/2010 Dispersion HMW NM 24 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/14/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/14/2010 Dispersion HMW NM 98 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/14/2010 Dispersion HMW NM 49 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/14/2010 Dispersion HMW NM 49 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Benzene VOC 71-43-2 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 1/14/2010 Dispersion HMW NM 9.8 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Chloroform VOC 67-66-3 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 1/14/2010 Dispersion HMW NM 9.8 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 1/14/2010 Dispersion HMW NM 24 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/14/2010 Dispersion HMW NM 2 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/14/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 F < m,p-Xylene VOC 106-42-3 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 1/14/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 40 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Naphthalene SVOC 91-20-3 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/14/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/14/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Toluene VOC 108-88-3 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 1/14/2010 Dispersion HMW NM 4.9 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/14/2010 Dispersion HMW NM 9.8 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/14/2010 Dispersion HMW NM 210 E 0.68 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/14/2010 Dispersion HMW NM 9.8 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 F < 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 F < 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 F < 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.25 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/15/2010 Dispersion HMW NM 510 U 21 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/15/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/15/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/15/2010 Dispersion HMW NM 10 U 0.42 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/15/2010 Dispersion HMW NM 26 U 1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/15/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/15/2010 Dispersion HMW NM 100 U 4.2 U Acetophenone SVOC 98-86-2 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/15/2010 Dispersion HMW NM 51 U 2.1 U Acrylonitrile VOC 107-13-1 P1-Henry 1/15/2010 Dispersion HMW NM 51 U 2.1 U Allyl Chloride VOC 107-05-1 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Benzene VOC 71-43-2 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Bromoform VOC 75-25-2 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Bromomethane VOC 74-83-9 P1-Henry 1/15/2010 Dispersion HMW NM 10 U 0.42 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Chlorobenzene VOC 108-90-7 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Chloroethane VOC 75-00-3 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.25 M Chloroform VOC 67-66-3 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Chloromethane VOC 74-87-3 P1-Henry 1/15/2010 Dispersion HMW NM 10 U 0.42 U Chloroprene VOC 126-99-8 P1-Henry 1/15/2010 Dispersion HMW NM 26 U 1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/15/2010 Dispersion HMW NM 2 U 0.083 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/15/2010 Dispersion HMW NM 50 U 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Iodomethane VOC 74-88-4 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Isophorone SVOC 78-59-1 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 F < m,p-Xylene VOC 106-42-3 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 41 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Methanol Alcohol 67-56-1 P1-Henry 1/15/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Methylene Chloride VOC 75-09-2 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Naphthalene SVOC 91-20-3 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/15/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/15/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Toluene VOC 108-88-3 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Trichloroethene VOC 79-01-6 P1-Henry 1/15/2010 Dispersion HMW NM 5.1 U 0.21 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/15/2010 Dispersion HMW NM 10 U 0.42 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/15/2010 Dispersion HMW NM 170 M 1.4 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/15/2010 Dispersion HMW NM 10 U 0.42 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.27 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/16/2010 Dispersion HMW NM 330 U 13 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/16/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/16/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/16/2010 Dispersion HMW NM 6.7 U 0.26 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/16/2010 Dispersion HMW NM 17 U 0.66 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/16/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/16/2010 Dispersion HMW NM 67 U 2.6 U Acetophenone SVOC 98-86-2 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/16/2010 Dispersion HMW NM 33 U 1.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/16/2010 Dispersion HMW NM 33 U 1.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Benzene VOC 71-43-2 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Bromoform VOC 75-25-2 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Bromomethane VOC 74-83-9 P1-Henry 1/16/2010 Dispersion HMW NM 6.7 U 0.26 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Chlorobenzene VOC 108-90-7 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Chloroethane VOC 75-00-3 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.17 M Chloroform VOC 67-66-3 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Chloromethane VOC 74-87-3 P1-Henry 1/16/2010 Dispersion HMW NM 6.7 U 0.26 U Chloroprene VOC 126-99-8 P1-Henry 1/16/2010 Dispersion HMW NM 17 U 0.66 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/16/2010 Dispersion HMW NM 1.3 U 0.053 F< Formaldehyde Aldehyde50-00-0 P1-Henry 1/16/2010 Dispersion HMW NM 50X< 50 U Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 42 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Iodomethane VOC 74-88-4 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Isophorone SVOC 78-59-1 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Methanol Alcohol 67-56-1 P1-Henry 1/16/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Methylene Chloride VOC 75-09-2 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Naphthalene SVOC 91-20-3 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/16/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Pentachlorophenol SVOC 87-86-5 P1-Henry 1/16/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Tetrachloroethene VOC 127-18-4 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 F< Toluene VOC 108-88-3 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Trichloroethene VOC 79-01-6 P1-Henry 1/16/2010 Dispersion HMW NM 3.3 U 0.13 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/16/2010 Dispersion HMW NM 6.7 U 0.26 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/16/2010 Dispersion HMW NM 120 M 1.4 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/16/2010 Dispersion HMW NM 6.7 U 0.26 F< 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.31 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/17/2010 Dispersion HMW NM 1100 U 19 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/17/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/17/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/17/2010 Dispersion HMW NM 22 U 0.38 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/17/2010 Dispersion HMW NM 54 U 0.96 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/17/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/17/2010 Dispersion HMW NM 220 U 3.8 U Acetophenone SVOC 98-86-2 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/17/2010 Dispersion HMW NM 110 U 1.9 U Acrylonitrile VOC 107-13-1 P1-Henry 1/17/2010 Dispersion HMW NM 110 U 1.9 U Allyl Chloride VOC 107-05-1 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Benzene VOC 71-43-2 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Bromoform VOC 75-25-2 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Bromomethane VOC 74-83-9 P1-Henry 1/17/2010 Dispersion HMW NM 22 U 0.38 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Chlorobenzene VOC 108-90-7 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Chloroethane VOC 75-00-3 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.2 M Chloroform VOC 67-66-3 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Chloromethane VOC 74-87-3 P1-Henry 1/17/2010 Dispersion HMW NM 22 U 0.38 U Chloroprene VOC 126-99-8 P1-Henry 1/17/2010 Dispersion HMW NM 54 U 0.96 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/17/2010 Dispersion HMW NM 4.3 U 0.077 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/17/2010 Dispersion HMW NM 50X< 50 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 43 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Iodomethane VOC 74-88-4 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Isophorone SVOC 78-59-1 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Methanol Alcohol 67-56-1 P1-Henry 1/17/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Methylene Chloride VOC 75-09-2 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Naphthalene SVOC 91-20-3 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/17/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/17/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Toluene VOC 108-88-3 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Trichloroethene VOC 79-01-6 P1-Henry 1/17/2010 Dispersion HMW NM 11 U 0.19 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/17/2010 Dispersion HMW NM 22 U 0.38 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/17/2010 Dispersion HMW NM 100 M 0.72 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/17/2010 Dispersion HMW NM 22 U 0.38 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.24 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/18/2010 Dispersion HMW NM 1100 U 17 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/18/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/18/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/18/2010 Dispersion HMW NM 23 U 0.33 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/18/2010 Dispersion HMW NM 57 U 0.83 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/18/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/18/2010 Dispersion HMW NM 230 U 3.3 U Acetophenone SVOC 98-86-2 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/18/2010 Dispersion HMW NM 110 U 1.7 U Acrylonitrile VOC 107-13-1 P1-Henry 1/18/2010 Dispersion HMW NM 110 U 1.7 U Allyl Chloride VOC 107-05-1 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Benzene VOC 71-43-2 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Bromoform VOC 75-25-2 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Bromomethane VOC 74-83-9 P1-Henry 1/18/2010 Dispersion HMW NM 23 U 0.33 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Chlorobenzene VOC 108-90-7 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Chloroethane VOC 75-00-3 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Chloroform VOC 67-66-3 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Chloromethane VOC 74-87-3 P1-Henry 1/18/2010 Dispersion HMW NM 23 U 0.33 U Chloroprene VOC 126-99-8 P1-Henry 1/18/2010 Dispersion HMW NM 57 U 0.83 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 44 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/18/2010 Dispersion HMW NM 4.5 U 0.067 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/18/2010 Dispersion HMW NM 50X< 50X< Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Iodomethane VOC 74-88-4 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Isophorone SVOC 78-59-1 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Methanol Alcohol 67-56-1 P1-Henry 1/18/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Methylene Chloride VOC 75-09-2 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Naphthalene SVOC 91-20-3 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/18/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/18/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Toluene VOC 108-88-3 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Trichloroethene VOC 79-01-6 P1-Henry 1/18/2010 Dispersion HMW NM 11 U 0.17 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/18/2010 Dispersion HMW NM 23 U 0.33 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/18/2010 Dispersion HMW NM 160 M 0.36 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/18/2010 Dispersion HMW NM 23 U 0.33 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/19/2010 Dispersion HMW NM 460 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/19/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/19/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/19/2010 Dispersion HMW NM 9.2 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/19/2010 Dispersion HMW NM 23 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/19/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/19/2010 Dispersion HMW NM 92 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/19/2010 Dispersion HMW NM 46 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/19/2010 Dispersion HMW NM 46 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Benzene VOC 71-43-2 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Bromomethane VOC 74-83-9 P1-Henry 1/19/2010 Dispersion HMW NM 9.2 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 45 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Chloroethane VOC 75-00-3 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Chloroform VOC 67-66-3 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 1/19/2010 Dispersion HMW NM 9.2 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 1/19/2010 Dispersion HMW NM 23 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/19/2010 Dispersion HMW NM 1.8 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/19/2010 Dispersion HMW NM 50X< 50X< Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 1/19/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/19/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/19/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Toluene VOC 108-88-3 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 1/19/2010 Dispersion HMW NM 4.6 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/19/2010 Dispersion HMW NM 9.2 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/19/2010 Dispersion HMW NM 61 M 0.63 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/19/2010 Dispersion HMW NM 9.2 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/20/2010 Dispersion HMW NM 380 U 23 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/20/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/20/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/20/2010 Dispersion HMW NM 7.6 U 0.45 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/20/2010 Dispersion HMW NM 19 U 1.1 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/20/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/20/2010 Dispersion HMW NM 76 U 4.5 U Acetophenone SVOC 98-86-2 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/20/2010 Dispersion HMW NM 38 U 2.3 U Acrylonitrile VOC 107-13-1 P1-Henry 1/20/2010 Dispersion HMW NM 38 U 2.3 U Allyl Chloride VOC 107-05-1 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Benzene VOC 71-43-2 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Bromoform VOC 75-25-2 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 46 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Bromomethane VOC 74-83-9 P1-Henry 1/20/2010 Dispersion HMW NM 7.6 U 0.45 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Chlorobenzene VOC 108-90-7 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Chloroethane VOC 75-00-3 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Chloroform VOC 67-66-3 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Chloromethane VOC 74-87-3 P1-Henry 1/20/2010 Dispersion HMW NM 7.6 U 0.45 U Chloroprene VOC 126-99-8 P1-Henry 1/20/2010 Dispersion HMW NM 19 U 1.1 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/20/2010 Dispersion HMW NM 1.5 U 0.091 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/20/2010 Dispersion HMW NM 50X< 50X< Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Iodomethane VOC 74-88-4 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Isophorone SVOC 78-59-1 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Methanol Alcohol 67-56-1 P1-Henry 1/20/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Methylene Chloride VOC 75-09-2 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Naphthalene SVOC 91-20-3 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/20/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/20/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Toluene VOC 108-88-3 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Trichloroethene VOC 79-01-6 P1-Henry 1/20/2010 Dispersion HMW NM 3.8 U 0.23 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/20/2010 Dispersion HMW NM 7.6 U 0.45 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/20/2010 Dispersion HMW NM 120 M 0.32 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/20/2010 Dispersion HMW NM 7.6 U 0.45 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/21/2010 Dispersion HMW NM 170 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/21/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/21/2010 Dispersion HMW NM 5000 U 5000 U 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/21/2010 Dispersion HMW NM 3.3 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/21/2010 Dispersion HMW NM 8.3 U 1.2 U Acetaldehyde Aldehyde75-07-0 P1-Henry 1/21/2010 Dispersion HMW NM 50 U 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/21/2010 Dispersion HMW NM 33 U 5 U Acetophenone SVOC 98-86-2 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/21/2010 Dispersion HMW NM 17 U 2.5 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 47 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Acrylonitrile VOC 107-13-1 P1-Henry 1/21/2010 Dispersion HMW NM 17 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Benzene VOC 71-43-2 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Bromomethane VOC 74-83-9 P1-Henry 1/21/2010 Dispersion HMW NM 3.3 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Chloroethane VOC 75-00-3 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Chloroform VOC 67-66-3 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Chloromethane VOC 74-87-3 P1-Henry 1/21/2010 Dispersion HMW NM 3.3 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 1/21/2010 Dispersion HMW NM 8.3 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/21/2010 Dispersion HMW NM 0.67 U 0.1 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/21/2010 Dispersion HMW NM 50X< 50X< Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Methanol Alcohol 67-56-1 P1-Henry 1/21/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Methylene Chloride VOC 75-09-2 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/21/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/21/2010 Dispersion HMW NM 5000 U 5000 U Styrene VOC 100-42-5 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Toluene VOC 108-88-3 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 1/21/2010 Dispersion HMW NM 1.7 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/21/2010 Dispersion HMW NM 3.3 U 0.5 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/21/2010 Dispersion HMW NM 70 E 0.3 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/21/2010 Dispersion HMW NM 3.3 U 0.5 U 1,1,1-Trichloroethane VOC 71-55-6 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U 1,1,2,2-Tetrachloroethane VOC 79-34-5 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 F< 1,1,2-Trichloroethane VOC 79-00-5 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U 1,1-Dichloroethane VOC 75-34-3 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U 1,1-Dichloroethene VOC 75-35-4 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U 1,2,4-Trichlorobenzene VOC 120-82-1 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 F< 1,2-Dibromo-3-chloropropaneVOC 96-12-8 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 F< 1,2-Dibromoethane (EDB) VOC 106-93-4 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U 1,2-Dichloroethane VOC 107-06-2 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.35 M 1,2-Dichloropropane VOC 78-87-5 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U 1,4-Dichlorobenzene SVOC 106-46-7 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U 1,4-Dioxane VOC 123-91-1 P1-Henry 1/22/2010 Dispersion HMW NM 530 U 25 U 2,4,5-Trichlorophenol SVOC 95-95-4 P1-Henry 1/22/2010 Dispersion HMW NM 5000 U 5000 U 2,4,6-Trichlorophenol SVOC 88-89-1 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U 2,4-Dinitrophenol SVOC 51-28-5 P1-Henry 1/22/2010 Dispersion HMW NM 5000 C< 5000 C< 2,4-Dinitrotoluene SVOC 121-14-2 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U MEK VOC 78-93-3 P1-Henry 1/22/2010 Dispersion HMW NM 11 U 0.5 U 2-Nitropropane VOC 79-46-9 P1-Henry 1/22/2010 Dispersion HMW NM 26 U 1.2 U

Dispersion Conc. Data Agg 0900006480f92db5.xls 48 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Acetaldehyde Aldehyde75-07-0 P1-Henry 1/22/2010 Dispersion HMW NM 50 H< 50 U Acetonitrile VOC 75-05-8 P1-Henry 1/22/2010 Dispersion HMW NM 110 U 5 U Acetophenone SVOC 98-86-2 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Acrolein VOC 107-02-8 P1-Henry 1/22/2010 Dispersion HMW NM 53 U 2.5 U Acrylonitrile VOC 107-13-1 P1-Henry 1/22/2010 Dispersion HMW NM 53 U 2.5 U Allyl Chloride VOC 107-05-1 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Benzene VOC 71-43-2 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Bromoform VOC 75-25-2 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Bromomethane VOC 74-83-9 P1-Henry 1/22/2010 Dispersion HMW NM 11 U 0.5 U Carbon Disulfide VOC 75-15-0 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Carbon Tetrachloride VOC 56-23-5 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Chlorobenzene VOC 108-90-7 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Chloroethane VOC 75-00-3 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Chloroform VOC 67-66-3 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Chloromethane VOC 74-87-3 P1-Henry 1/22/2010 Dispersion HMW NM 11 U 0.5 U Chloroprene VOC 126-99-8 P1-Henry 1/22/2010 Dispersion HMW NM 26 U 1.2 U cis-1,3-Dichloropropene VOC 10061-01-5P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Dibenzofuran SVOC 132-64-9 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Ethylbenzene VOC 100-41-4 P1-Henry 1/22/2010 Dispersion HMW NM 2.1 U 0.1 U Formaldehyde Aldehyde50-00-0 P1-Henry 1/22/2010 Dispersion HMW NM 50 H< 50X< Hexachlorobenzene SVOC 118-74-1 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Hexachlorobutadiene SVOC 87-68-3 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Hexachloroethane SVOC 67-72-1 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Hexane VOC 110-54-3 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Iodomethane VOC 74-88-4 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Isophorone SVOC 78-59-1 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Isopropylbenzene VOC 98-82-8 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 F< m,p-Xylene VOC 106-42-3 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Methanol Alcohol 67-56-1 P1-Henry 1/22/2010 Dispersion HMW NM 50 U 50 U Methyl Methacrylate VOC 80-62-6 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Methylene Chloride VOC 75-09-2 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Methyl-tert-Butyl Ether VOC 1634-04-4 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Naphthalene SVOC 91-20-3 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U Nitrobenzene SVOC 98-95-3 P1-Henry 1/22/2010 Dispersion HMW NM 1000 U 1000 U o-Xylene VOC 95-47-6 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Pentachlorophenol SVOC 87-86-5 P1-Henry 1/22/2010 Dispersion HMW NM NM NM Styrene VOC 100-42-5 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Tetrachloroethene VOC 127-18-4 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Toluene VOC 108-88-3 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U trans-1,3-Dichloropropene VOC 10061-02-6 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Trichloroethene VOC 79-01-6 P1-Henry 1/22/2010 Dispersion HMW NM 5.3 U 0.25 U Vinyl Acetate VOC 108-05-4 P1-Henry 1/22/2010 Dispersion HMW NM 11 U 0.5 U Vinyl Chloride VOC 75-01-4 P1-Henry 1/22/2010 Dispersion HMW NM 160 M 0.82 M Xylenes (Total) VOC 1330-20-7 P1-Henry 1/22/2010 Dispersion HMW NM 11 U 0.5 U Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/9/2009 Dispersion HMW NM 305.51 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/10/2009 Dispersion HMW NM 648.65 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/11/2009 Dispersion HMW NM 78.19 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/12/2009 Dispersion HMW NM 303.91 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/13/2009 Dispersion HMW NM 406.69 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/14/2009 Dispersion HMW NM 285.26 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/15/2009 Dispersion HMW NM 305.95 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/16/2009 Dispersion HMW NM 63 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/17/2009 Dispersion HMW NM 228.32 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/18/2009 Dispersion HMW NM 260.96 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/19/2009 Dispersion HMW NM 245.81 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 12/20/2009 Dispersion HMW NM 64 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/5/2010 Dispersion HMW NM 555.19 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/6/2010 Dispersion HMW NM 359.91 M NM

Dispersion Conc. Data Agg 0900006480f92db5.xls 49 of 50Vinyl Institute 30 Day Concentration Database for Dispersion Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte See Notes in Column P for Revisions to Data Base CategoryCAS Reportin g Plant Date Resin Type Resin Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/7/2010 Dispersion HMW NM 320.01 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/8/2010 Dispersion HMW NM 320.49 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/9/2010 Dispersion HMW NM 196.71 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/10/2010 Dispersion HMW NM 306.42 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/11/2010 Dispersion HMW NM 271.64 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/12/2010 Dispersion HMW NM 193.62 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/13/2010 Dispersion HMW NM 419.06 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/14/2010 Dispersion HMW NM 436.75 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/15/2010 Dispersion HMW NM 492.37 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/16/2010 Dispersion HMW NM 334.69 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/17/2010 Dispersion HMW NM 273.88 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/18/2010 Dispersion HMW NM 268.13 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/19/2010 Dispersion HMW NM 443.85 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/20/2010 Dispersion HMW NM 512.09 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/21/2010 Dispersion HMW NM 394.27 M NM Vinyl chloride Method 107* VOC 75-01-4VOC P1-Henry 1/22/2010 Dispersion HMW NM 900.08 M NM

Dispersion Conc. Data Agg 0900006480f92db5.xls 50 of 50

## Vinyl Institute 30 Day Concentration Database for Vinyl Acetate Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor
y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/22/2010Copolyme VACO 0.08U 4.30U 1.30U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/22/2010Copolyme VACO 0.07U 2.20U 0.69U Chloroethane VOC 75-00-3 FPC DE 1/22/2010Copolyme VACO 0.07U 10.40M 2.00U Chloroform VOC 67-66-3 FPC DE 1/22/2010Copolyme VACO 0.05U 2.10U 0.64U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/22/2010Copolyme

r VACO 0.06U 1.10U 0.33U Chloroprene VOC 126-99-8FPC DE 1/22/2010Copolyme VACO 0.19U 7.20U 2.20U Vinyl acetate VOC 108-05-4FPC DE 1/22/2010Copolyme VACO 16.10M 1020.00M 134.00M Vinyl Bromide VOC 593-60-2 FPC DE 1/22/2010Copolyme VACO 0.02U 0.89U 0.27U Vinyl chloride VOC 75-01-4 FPC DE 1/22/2010Copolyme VACO 0.82M 136.00M 1.44M Hydroquinone SVOC 123-31-9FPC DE 1/22/2010Copolyme VACO 1.00U 26.00U 43.00U Phenol SVOC 108-95-2 FPC DE 1/22/2010Copolyme VACO 0.12U 13.00U 21.00U Methanol Alcohol 67-56-1 FPC DE 1/22/2010Copolyme VACO 3.40U 5.70U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/22/2010Copolyme VACO 1.32M 20.90M 1.63M Formaldehyde Aldehyd 50-00-0 FPC DE 1/22/2010Copolyme VACO 0.03M 0.41 M 0.38M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/23/2010Copolyme VACO 0.08U 4.70U 3.30U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/23/2010Copolyme VACO 0.07U 2.50U 1.70U Chloroethane VOC 75-00-3 FPC DE 1/23/2010Copolyme VACO 0.09M 7.10U 5.00U Chloroform VOC 67-66-3 FPC DE 1/23/2010Copolyme VACO 0.05U 2.30U 1.60U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/23/2010Copolyme

r VACO 0.06U 1.20U 0.83U Chloroprene VOC 126-99-8FPC DE 1/23/2010Copolyme VACO 0.19U 7.90U 5.60U Vinyl acetate VOC 108-05-4FPC DE 1/23/2010Copolyme VACO 16.20M 653.00M 5.30U Vinyl Bromide VOC 593-60-2 FPC DE 1/23/2010Copolyme VACO 0.02U 0.97U 0.68U Vinyl chloride VOC 75-01-4 FPC DE 1/23/2010Copolyme VACO 2.00M 30.70M 1.99M Hydroquinone SVOC 123-31-9FPC DE 1/23/2010Copolyme VACO 0.10U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/23/2010Copolyme VACO 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/23/2010Copolyme VACO 3.40U 0.11 U 0.15U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/23/2010Copolyme VACO 3.49M 37.20M 1.92M Formaldehyde Aldehyd 50-00-0 FPC DE 1/23/2010Copolyme VACO 0.02M 0.65M 0.27M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/24/2010Copolyme VACO 0.08U 4.70U 3.30U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/24/2010Copolyme VACO 0.07U 2.50U 1.70U Chloroethane VOC 75-00-3 FPC DE 1/24/2010Copolyme VACO 0.07U 7.10U 5.00U Chloroform VOC 67-66-3 FPC DE 1/24/2010Copolyme VACO 0.05U 2.30U 1.60U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/24/2010Copolyme

r VACO 0.06U 1.20U 0.83U Chloroprene VOC 126-99-8FPC DE 1/24/2010Copolyme VACO 0.19U 7.90U 5.60U Vinyl acetate VOC 108-05-4FPC DE 1/24/2010Copolyme VACO 15.30M 716.00M 5.30U Vinyl Bromide VOC 593-60-2 FPC DE 1/24/2010Copolyme VACO 0.02U 0.97U 0.68U Vinyl chloride VOC 75-01-4 FPC DE 1/24/2010Copolyme VACO 1.21 M 51.60M 0.89U Hydroquinone SVOC 123-31-9FPC DE 1/24/2010Copolyme VACO 1.00U 26.00U 21.00U

VACO Copolymer 0900006480f92db5.xls 1 of 5

## Vinyl Institute 30 Day Concentration Database for Vinyl Acetate Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor
y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Phenol SVOC 108-95-2 FPC DE 1/24/2010Copolyme VACO 0.12U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/24/2010Copolyme VACO 3.40U 11.00U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/24/2010Copolyme VACO 0.77M 23.60M 1.43M Formaldehyde Aldehyd 50-00-0 FPC DE 1/24/2010Copolyme VACO 0.01 M 0.74M 0.54M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/25/2010Copolyme VACO 0.02U 4.30U 1.30U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/25/2010Copolyme VACO 0.02U 2.30U 0.69U Chloroethane VOC 75-00-3 FPC DE 1/25/2010Copolyme VACO 0.04M 10.50M 2.00U Chloroform VOC 67-66-3 FPC DE 1/25/2010Copolyme VACO 0.01 U 2.10U 0.64U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/25/2010Copolyme

r VACO 0.01 U 1.10U 0.33U Chloroprene VOC 126-99-8FPC DE 1/25/2010Copolyme VACO 0.05U 7.20U 2.20U Vinyl acetate VOC 108-05-4FPC DE 1/25/2010Copolyme VACO 15.90M 1250.00M 2.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/25/2010Copolyme VACO 0.01 U 0.89U 0.27U Vinyl chloride VOC 75-01-4 FPC DE 1/25/2010Copolyme VACO 0.58M 106.00M 1.32M Hydroquinone SVOC 123-31-9FPC DE 1/25/2010Copolyme VACO 1.00U 26.00U 43.00U Phenol SVOC 108-95-2 FPC DE 1/25/2010Copolyme VACO 0.12U 13.00U 21.00U Methanol Alcohol 67-56-1 FPC DE 1/25/2010Copolyme VACO 3.40U 8.90U 15.00U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/25/2010Copolyme VACO 2.32M 21.80M 0.81 M Formaldehyde Aldehyd 50-00-0 FPC DE 1/25/2010Copolyme VACO 0.01 M 0.34M 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/26/2010Copolyme VACO 2.00U 4.60U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/26/2010Copolyme VACO 1.70U 2.40U 0.35U Chloroethane VOC 75-00-3 FPC DE 1/26/2010Copolyme VACO 1.90U 10.70M 1.31 M Chloroform VOC 67-66-3 FPC DE 1/26/2010Copolyme VACO 1.20U 2.20U 0.32U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/26/2010Copolyme

r VACO 1.40U 1.10U 0.17U Chloroprene VOC 126-99-8FPC DE 1/26/2010Copolyme VACO 4.60U 7.70U 1.10U Vinyl acetate VOC 108-05-4FPC DE 1/26/2010Copolyme VACO 63.20M 977.00M 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/26/2010Copolyme VACO 0.50U 0.95U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 1/26/2010Copolyme VACO 23.90M 114.00M 0.90M Hydroquinone SVOC 123-31-9FPC DE 1/26/2010Copolyme VACO 1.00U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/26/2010Copolyme VACO 0.12U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/26/2010Copolyme VACO 3.40U 5.70U 16.00U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/26/2010Copolyme VACO 0.63M 11.50M 0.73M Formaldehyde Aldehyd 50-00-0 FPC DE 1/26/2010Copolyme VACO 0.01 U 0.17M 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/27/2010Copolyme VACO 0.10U 4.50U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/27/2010Copolyme VACO 0.08U 2.30U 0.35U Chloroethane VOC 75-00-3 FPC DE 1/27/2010Copolyme VACO 0.09U 6.80U 1.03M Chloroform VOC 67-66-3 FPC DE 1/27/2010Copolyme VACO 0.06U 2.20U 0.32U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/27/2010Copolyme

r VACO 0.07U 1.10U 0.17U Chloroprene VOC 126-99-8FPC DE 1/27/2010Copolyme VACO 0.23U 7.50U 1.10U

VACO Copolymer 0900006480f92db5.xls 2 of 5

## Vinyl Institute 30 Day Concentration Database for Vinyl Acetate Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor
y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Vinyl acetate VOC 108-05-4FPC DE 1/27/2010Copolyme VACO 12.00M 956.00M 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/27/2010Copolyme VACO 0.03U 0.92U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 1/27/2010Copolyme VACO 0.69M 69.50M 0.64M Hydroquinone SVOC 123-31-9FPC DE 1/27/2010Copolyme VACO 1.00U 25.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/27/2010Copolyme VACO 0.12U 12.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/27/2010Copolyme VACO 3.40U 9.30U 15.00U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/27/2010Copolyme VACO 1.74M 12.20M 0.92M Formaldehyde Aldehyd 50-00-0 FPC DE 1/27/2010Copolyme VACO 0.01 M 0.24M 0.21 M 1,1-Dichloroethene VOC 75-35-4 FPC DE 1/28/2010Copolyme VACO 0.10U 4.40U 0.66U 1,2-Dichloroethane VOC 107-06-2 FPC DE 1/28/2010Copolyme VACO 0.08U 2.30U 0.35U Chloroethane VOC 75-00-3 FPC DE 1/28/2010Copolyme VACO 0.09U 6.60U 1.00U Chloroform VOC 67-66-3 FPC DE 1/28/2010Copolyme VACO 0.06U 2.10U 0.32U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 1/28/2010Copolyme

r VACO 0.07U 1.10U 0.17U Chloroprene VOC 126-99-8FPC DE 1/28/2010Copolyme VACO 0.23U 7.30U 1.10U Vinyl acetate VOC 108-05-4FPC DE 1/28/2010Copolyme VACO 16.60M 719.00M 1.10U Vinyl Bromide VOC 593-60-2 FPC DE 1/28/2010Copolyme VACO 0.03U 0.89U 0.14U Vinyl chloride VOC 75-01-4 FPC DE 1/28/2010Copolyme VACO 0.72M 36.60M 0.54M Hydroquinone SVOC 123-31-9FPC DE 1/28/2010Copolyme VACO 1.00U 25.00U 21.00U Phenol SVOC 108-95-2 FPC DE 1/28/2010Copolyme VACO 0.12U 12.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 1/28/2010Copolyme VACO 3.40U 5.50U 7.40U Acetaldehyde Aldehyd 75-07-0 FPC DE 1/28/2010Copolyme VACO 2.10M 12.80M 2.08M Formaldehyde Aldehyd 50-00-0 FPC DE 1/28/2010Copolyme VACO 0.10M 0.38M 0.63M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/14/2010Copolyme VACO 0.08U 1.20U 1.70U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/14/2010Copolyme VACO 0.07U 0.63U 0.87U Chloroethane VOC 75-00-3 FPC DE 2/14/2010Copolyme VACO 0.07U 6.13M 2.50U Chloroform VOC 67-66-3 FPC DE 2/14/2010Copolyme VACO 0.05U 0.58U 0.80U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/14/2010Copolyme

r VACO 0.06U 0.30U 0.41 U Chloroprene VOC 126-99-8FPC DE 2/14/2010Copolyme VACO 0.19U 2.00U 2.80U Vinyl acetate VOC 108-05-4FPC DE 2/14/2010Copolyme VACO 0.25U 72.40M 2.60U Vinyl Bromide VOC 593-60-2 FPC DE 2/14/2010Copolyme VACO 0.02U 0.25U 0.34U Vinyl chloride VOC 75-01-4 FPC DE 2/14/2010Copolyme VACO 1.15M 132.00M 2.61 M Hydroquinone SVOC 123-31-9FPC DE 2/14/2010Copolyme VACO 0.05U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/14/2010Copolyme VACO 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/14/2010Copolyme VACO 3.40U 2.20U 7.90U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/14/2010Copolyme VACO 0.51 M 4.90M 0.16M Formaldehyde Aldehyd 50-00-0 FPC DE 2/14/2010Copolyme VACO 0.03U 0.19M 0.11 U 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/15/2010Copolyme VACO 0.08U 0.88U 1.00U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/15/2010Copolyme VACO 0.07U 0.46U 0.52U Chloroethane VOC 75-00-3 FPC DE 2/15/2010Copolyme VACO 0.07U 6.63M 2.20M

VACO Copolymer 0900006480f92db5.xls 3 of 5

## Vinyl Institute 30 Day Concentration Database for Vinyl Acetate Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor
y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Chloroform VOC 67-66-3 FPC DE 2/15/2010Copolyme VACO 0.05U 0.42U 0.48U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/15/2010Copolyme

r VACO 0.06U 0.22U 0.25U Chloroprene VOC 126-99-8FPC DE 2/15/2010Copolyme VACO 0.19U 1.50U 1.70U Vinyl acetate VOC 108-05-4FPC DE 2/15/2010Copolyme VACO 0.25U 1010.00M 256.00M Vinyl Bromide VOC 593-60-2 FPC DE 2/15/2010Copolyme VACO 0.02U 0.18U 0.20U Vinyl chloride VOC 75-01-4 FPC DE 2/15/2010Copolyme VACO 1.16M 197.00M 3.00M Hydroquinone SVOC 123-31-9FPC DE 2/15/2010Copolyme VACO 0.10U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/15/2010Copolyme VACO 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/15/2010Copolyme VACO 3.40U 1.10U 1.50U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/15/2010Copolyme VACO 9.05M 5.10M 1.42M Formaldehyde Aldehyd 50-00-0 FPC DE 2/15/2010Copolyme VACO 0.03U 1.15M 0.55M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/16/2010Copolyme VACO 0.08U 0.85U 1.70U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/16/2010Copolyme VACO 0.07U 0.44U 0.86U Chloroethane VOC 75-00-3 FPC DE 2/16/2010Copolyme VACO 0.07U 5.04M 2.50U Chloroform VOC 67-66-3 FPC DE 2/16/2010Copolyme VACO 0.05U 0.41 U 0.80U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/16/2010Copolyme

r VACO 0.06U 0.21 U 0.41 U Chloroprene VOC 126-99-8FPC DE 2/16/2010Copolyme VACO 0.19U 1.40U 2.80U Vinyl acetate VOC 108-05-4FPC DE 2/16/2010Copolyme VACO 21.80M 1080.00M 2.60U Vinyl Bromide VOC 593-60-2 FPC DE 2/16/2010Copolyme VACO 0.02U 0.17U 0.34U Vinyl chloride VOC 75-01-4 FPC DE 2/16/2010Copolyme VACO 1.54M 120.00M 1.52M Hydroquinone SVOC 123-31-9FPC DE 2/16/2010Copolyme VACO 0.05U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/16/2010Copolyme VACO 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/16/2010Copolyme VACO 1.70U 1.10U 7.40U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/16/2010Copolyme VACO 31.90M 12.30M 0.84M Formaldehyde Aldehyd 50-00-0 FPC DE 2/16/2010Copolyme VACO 0.29M 1.58M 0.44M 1,1-Dichloroethene VOC 75-35-4 FPC DE 2/17/2010Copolyme VACO 0.08U 1.20U 1.70U 1,2-Dichloroethane VOC 107-06-2 FPC DE 2/17/2010Copolyme VACO 0.07U 0.60U 0.86U Chloroethane VOC 75-00-3 FPC DE 2/17/2010Copolyme VACO 0.07U 4.47M 2.50U Chloroform VOC 67-66-3 FPC DE 2/17/2010Copolyme VACO 0.05U 0.55U 0.80U Chloromethane (Methyl chloride) VOC 74-87-3 FPC DE 2/17/2010Copolyme

r VACO 0.06U 0.29U 0.41 U Chloroprene VOC 126-99-8FPC DE 2/17/2010Copolyme VACO 0.19U 1.90U 2.80U Vinyl acetate VOC 108-05-4FPC DE 2/17/2010Copolyme VACO 14.00M 1110.00M 2.60U Vinyl Bromide VOC 593-60-2 FPC DE 2/17/2010Copolyme VACO 0.02U 0.24U 0.34U Vinyl chloride VOC 75-01-4 FPC DE 2/17/2010Copolyme VACO 1.28M 90.50M 2.90M Hydroquinone SVOC 123-31-9FPC DE 2/17/2010Copolyme VACO 0.05U 26.00U 21.00U Phenol SVOC 108-95-2 FPC DE 2/17/2010Copolyme VACO 0.01 U 13.00U 11.00U Methanol Alcohol 67-56-1 FPC DE 2/17/2010Copolyme VACO 1.70U 2.20U 3.00U Acetaldehyde Aldehyd 75-07-0 FPC DE 2/17/2010Copolyme VACO 19.00M 7.29M 0.69M

VACO Copolymer 0900006480f92db5.xls 4 of 5

## Vinyl Institute 30 Day Concentration Database for Vinyl Acetate Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor
y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type PVC

Resin, ppm PVC Resin

Measureme nt Type Formaldehyde Aldehyd 50-00-0 FPC DE 2/17/2010Copolyme VACO 0.41 M 0.21 M 0.15M Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/22/2010Copolyme VACO NM 745M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/23/2010Copolyme VACO NM 502 M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/24/2010Copolyme VACO NM 546M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/25/2010Copolyme VACO NM 407M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/26/2010Copolyme VACO NM 509M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/27/2010Copolyme VACO NM 534 M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 1/28/2010Copolyme VACO NM 886M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 2/14/2010Copolyme VACO NM 484 M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 2/15/2010Copolyme VACO NM 586M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 2/16/2010Copolyme VACO NM 538M NM Vinyl chloride Method 107* VOC 75-01-4VOC FPC DE 2/17/2010Copolyme VACO NM 435M NM

VACO Copolymer 0900006480f92db5.xls 5 of 5

## Vinyl Institute 30 Day Concentration Database for Vinylidene Chloride Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/18/09 Copolyme VDCO NM 0.40 M Notes: Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/18/09 Copolyme VDCO NM 0.21 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/19/09 Copolyme VDCO NM 0.38 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/19/09 Copolyme VDCO NM NM Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/19/09 Copolyme VDCO NM 0.18 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/20/09 Copolyme VDCO NM 0.68 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/20/09 Copolyme VDCO NM 0.19 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/20/09 Copolyme VDCO NM 0.53 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/21/09 Copolyme VDCO NM 0.19 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/21/09 Copolyme VDCO NM 0.31 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/22/09 Copolyme VDCO NM 0.18 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/22/09 Copolyme VDCO NM 0.39 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/23/09 Copolyme VDCO NM 0.30 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/23/09 Copolyme VDCO NM 0.71 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/24/09 Copolyme VDCO NM 0.23 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/24/09 Copolyme VDCO NM 0.38 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/24/09 Copolyme VDCO NM 1.36 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/25/09 Copolyme VDCO NM 0.29 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/26/09 Copolyme VDCO NM 0.54 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/26/09 Copolyme VDCO NM 0.38 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/27/09 Copolyme VDCO NM 0.40 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/27/09 Copolyme VDCO NM 0.23 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/27/09 Copolyme VDCO NM 0.31 M (1) Added Dow Vinyliden Copolymer data to database 7-21-11

Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/28/09 Copolyme VDCO NM 0.40 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/29/09 Copolyme VDCO NM 0.10 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/29/09 Copolyme VDCO NM 0.40 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/30/09 Copolyme VDCO NM 0.12 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/30/09 Copolyme VDCO NM 0.30 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 12/31/09 Copolyme VDCO NM 0.06 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/01/10 Copolyme VDCO NM 0.31 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/01/10 Copolyme VDCO NM 0.37 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/01/10 Copolyme VDCO NM 1.14 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/02/10 Copolyme VDCO NM 0.15 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/02/10 Copolyme VDCO NM 0.24 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/03/10 Copolyme VDCO NM 0.24 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/03/10 Copolyme VDCO NM 1.07 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/04/10 Copolyme VDCO NM 0.09 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/04/10 Copolyme VDCO NM 0.27 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/05/10 Copolyme VDCO NM 0.78 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/05/10 Copolyme VDCO NM 0.37 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/06/10 Copolyme VDCO NM 0.23 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/06/10 Copolyme VDCO NM 0.42 M

VDCO Copolymer 0900006480f92db5.xls 1 of 4

## Vinyl Institute 30 Day Concentration Database for Vinylidene Chloride Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/07/10 Copolyme VDCO NM 0.13 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/07/10 Copolyme VDCO NM 0.60 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/08/10 Copolyme VDCO NM 0.29 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/08/10 Copolyme VDCO NM 0.34 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/09/10 Copolyme VDCO NM 0.95 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/09/10 Copolyme VDCO NM 0.37 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/10/10 Copolyme VDCO NM 0.08 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/10/10 Copolyme VDCO NM 0.26 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/11/10 Copolyme VDCO NM 0.23 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/11/10 Copolyme VDCO NM 0.14 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/12/10 Copolyme VDCO NM 0.07 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/12/10 Copolyme VDCO NM 0.16 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/13/10 Copolyme VDCO NM 0.15 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/13/10 Copolyme VDCO NM 0.45 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/14/10 Copolyme VDCO NM 0.10 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/14/10 Copolyme VDCO NM 0.18 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/14/10 Copolyme VDCO NM 0.23 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/15/10 Copolyme VDCO NM 0.56 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/15/10 Copolyme VDCO NM 0.27 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/16/10 Copolyme VDCO NM 0.21 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/17/10 Copolyme VDCO NM 0.87 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/17/10 Copolyme VDCO NM 0.34 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/17/10 Copolyme VDCO NM 0.13 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/18/10 Copolyme VDCO NM 0.14 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/19/10 Copolyme VDCO NM 1.09 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/20/10 Copolyme VDCO NM 0.30 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/20/10 Copolyme VDCO NM 0.15 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/20/10 Copolyme VDCO NM 0.27 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/21/10 Copolyme VDCO NM 0.46 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/21/10 Copolyme VDCO NM 0.17 M Vinyl chloride Dow Method 101549-ME98B VOC 75-01-4VOC Dow MI 01/22/10 Copolyme VDCO NM 0.95 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/18/09 Copolyme VDCO NM 1.00 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/18/09 Copolyme VDCO NM 0.00 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/19/09 Copolyme VDCO NM 3.80 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/19/09 Copolyme VDCO NM NM Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/19/09 Copolyme VDCO NM 0.70 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/20/09 Copolyme VDCO NM 2.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/20/09 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/20/09 Copolyme VDCO NM 3.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/21/09 Copolyme VDCO NM 0.70 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/21/09 Copolyme VDCO NM 4.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/22/09 Copolyme VDCO NM 0.40 M

VDCO Copolymer 0900006480f92db5.xls 2 of 4

## Vinyl Institute 30 Day Concentration Database for Vinylidene Chloride Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/22/09 Copolyme VDCO NM 3.20 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/23/09 Copolyme VDCO NM 0.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/23/09 Copolyme VDCO NM 1.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/24/09 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/24/09 Copolyme VDCO NM 1.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/24/09 Copolyme VDCO NM 3.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/25/09 Copolyme VDCO NM 0.80 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/26/09 Copolyme VDCO NM 1.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/26/09 Copolyme VDCO NM 2.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/27/09 Copolyme VDCO NM 0.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/27/09 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/27/09 Copolyme VDCO NM 0.70 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/28/09 Copolyme VDCO NM 2.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/29/09 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/29/09 Copolyme VDCO NM 0.80 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/30/09 Copolyme VDCO NM 0.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/30/09 Copolyme VDCO NM 4.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 12/31/09 Copolyme VDCO NM 0.00 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/01/10 Copolyme VDCO NM 0.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/01/10 Copolyme VDCO NM 0.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/01/10 Copolyme VDCO NM 7.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/02/10 Copolyme VDCO NM 9.00 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/02/10 Copolyme VDCO NM 0.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/03/10 Copolyme VDCO NM 0.70 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/03/10 Copolyme VDCO NM 4.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/04/10 Copolyme VDCO NM 0.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/04/10 Copolyme VDCO NM 0.80 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/05/10 Copolyme VDCO NM 3.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/05/10 Copolyme VDCO NM 3.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/06/10 Copolyme VDCO NM 0.80 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/06/10 Copolyme VDCO NM 1.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/07/10 Copolyme VDCO NM 0.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/07/10 Copolyme VDCO NM 4.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/08/10 Copolyme VDCO NM 1.20 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/08/10 Copolyme VDCO NM 0.70 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/09/10 Copolyme VDCO NM 3.20 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/09/10 Copolyme VDCO NM 3.10 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/10/10 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/10/10 Copolyme VDCO NM 0.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/11/10 Copolyme VDCO NM 0.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/11/10 Copolyme VDCO NM 3.20 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/12/10 Copolyme VDCO NM 0.50 M

VDCO Copolymer 0900006480f92db5.xls 3 of 4

## Vinyl Institute 30 Day Concentration Database for Vinylidene Chloride Copolymer Type Resins Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

Analyte Categor y CAS Reportin

g Plant Date Resin

Type Resin

Grade Slurry

Water, mg/L Slurry Water

Measuremen t Type Wet Resin

from Stripper Bottoms, ppm Wet Resin

from Stripper Bottoms, Measuremen t Type Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/12/10 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/13/10 Copolyme VDCO NM 0.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/13/10 Copolyme VDCO NM 3.10 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/14/10 Copolyme VDCO NM 0.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/14/10 Copolyme VDCO NM 0.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/14/10 Copolyme VDCO NM 0.70 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/15/10 Copolyme VDCO NM 4.00 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/15/10 Copolyme VDCO NM 0.90 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/16/10 Copolyme VDCO NM 0.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/17/10 Copolyme VDCO NM 3.60 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/17/10 Copolyme VDCO NM 3.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/17/10 Copolyme VDCO NM 0.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/18/10 Copolyme VDCO NM 0.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/19/10 Copolyme VDCO NM 3.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/20/10 Copolyme VDCO NM 2.10 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/20/10 Copolyme VDCO NM 0.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/20/10 Copolyme VDCO NM 5.40 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/21/10 Copolyme VDCO NM 1.30 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/21/10 Copolyme VDCO NM 1.50 M Vinylidene Chloride Dow Method 101549-ME98B VOC 75-35-4VOC

Dow MI 01/22/10 Copolyme VDCO NM 3.70 M

VDCO Copolymer 0900006480f92db5.xls 4 of 4

## Vinyl Institute 30 Day Concentration Database Resin Grades Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011



# Resin Grade (See Note 1) Low Molecular

Weight (LMW) Homopolymer General

Purpose (GP) (See note 3) High Molecular

Weight (HMW) Homopolymer VACO VDCO Resin Inherent Viscosity (IV) (See Note 2) Less than 0.85 0.85 to 1.0 Greater than 1.0 Vinyl Acetate/

Vinyl Chloride Copolymer Vinylidene

Chloride/ Vinyl Chloride Copolymer

Note 1 - The PVC industry produces well over 100 grades of resin that can be subcategorized in general according to these guidelines

Note 2 - Resin inherent viscosity is in a sense a measurement of molecular weight (MW), but no direct correlation is available to convert to MW

Note 3 - Some manufacturers distinguish HMWfor flexible PVC use at a resin IV corresponding to 0.95, with corresponding recipe adjustments

**Product Category Resin Type** 

Homopolymer Suspension - indicates resin polymerized with suspension technology

Homopolymer Dispersion - indicates resin polymerized with dispersion technology

Homopolymer Suspension Blending - indicates resin polymerized with modified suspension technology for particle size control

Copolymer Suspension - indicates resin polymerized with suspension technology

Copolymer Dispersion - indicates resin polymerized with dispersion technology

Copolymer Suspension Blending - indicates resin polymerized with modified suspension technology for particle size control

Resin Grade 0900006480f92db5.xls 1 of 1

## Vinyl Institute 30 Day Concentration Database Reporting Plant Identifiers Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

**Suspension Reporting**  **Description** FPC- LA Formosa Plastics Company - Baton Rouge, LA FPC-TX Formosa Plastics Company - Point Comfort, TX GG-Plaquemine Georgia Gulf Corporation - Plaquemine, LA GG-Aberdeen Georgia Gulf Corporation - Aberdeen, MS Oxy DP Oxy

Vinyls, LP - Deep Park, TX Oxy Pas Oxy

Vinyls, LP- Pasadena, TX Oxy Ptown Oxy

Vinyls, LP - Pedricktown, NJ Shintech AD Shintech - Addis, LA Shintech TX Shintech - Freeport, TX Shintech PL Shintech - Plaquemine, LA Westlake -LA Westlake - Geismar, LA Westlake-KY Westlake - Calvert City, KY

**Dispersion Reporting**  **Description** FPC DE Formosa Plastics Company - Delaware City, DE P1-Ptown PolyOne Corporation - Pedricktown, NJ P1-Henry PolyOne Corporation - Henry, IL

**Copolymer Reporting**  **Description** FPC DE Formosa Plastics Company - Delaware City, DE Dow MI The Dow Chemical Company - Midland, MI

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### Vinyl Institute 30 Day Concentration Database Measurement Types for Reported Data Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

**Measurement Type Descriptions**
DL = The compound was analyzed for, but was not detected ("Non-detect") at or above the Minimum Reporting Limit/Minimum Detection Limit (MRL/MDL).

J = The result is an estimated concentration that is less than the MRL but greater than or equal to the MDL.

D = The reported value is from a dilution.

JD = The result is a from a dilution, and the concentration is estimated, i.e. it is less than the dilution adjusted (MRL, RL, MQL) but greater than or equal to the dilution adjusted MDL.

B = the target analyte appeared above the MDL in the method blank run. Sometimes the Lab adds the additional qualifier that the Blank response is greater than 10% of the sample concentration

JB = Analyte appeared in method blank run, and the estimated concentration that is less than the MRL but greater than or equal to the MDL.
U - means not detected at or above the associated value. Usually the same as the ND(xx) descriptor.

UJ = the associated value is an estimated detection limit.
M = Measured above the RL, MRL, MQL. This is not a flag added to lab data, since data above the RL is simply the number. However, it can be used to positively indicate the results was above the RL.

NM = Not Measured, (not analyzed for or sample not submitted that day)

RL - Reporting Limit - laboratory designated meaning - usually means the number is equal to the lowest calibration standard for that method, or is at least some value well above the MDL where results are reliable.

R = Rejected data - do not use.

E = indicates the value exceeds the calibration range. It could be diluted and re-run to bring the reported value within the calibration range.
ND - Not Detected or ND(xx) is Not Detected at the detection limit in parentheses, e.g. ND(3.1)

NA - means this analyte had at least one detect but loadings were dominated by phantom ND load calcs Oxy meaning only for loading report to EPA. NA can also mean not analyzed or not applicable.

NL - means this analyte had at least one detect but calculated loadings indicated a negative value for air emission. Oxy meaning only for loading report to EPA. No other known common usage.

NS - do not use HAP data for this day due to implausible % solids data impacting the HAP loadings. Oxy meaning only for loading report to EPA. No other known common usage.

EMPC - Estimated Maximum Possible Concentration. Used in high resolution mass spec analyses for dioxins and PCBs to indicate that a positive interference is likely present because theion ratios do not match criteria

C - co-elution of target analytes has occurred and the result is the sum of the co-eluters.

MDL - method detection limit, usually obtained from the procedure set forth at 40 CFR 136, Appendix B.

**Analyte Notes**
* Average of NESHAP grabs or process control grabs for sampling day.

(Mod 8260B) = Indicates analyte was testing using the modificatitons to Method 8260B approved by EPA for Georgia Gulf's test plan

PolyOne Henry Data Qualifier Explanations A The presence of this analyte was confirmed using a second column but there was a disparity (> 40% RPD) between the two sets of results with no apparent chromatographic anomalies. The lower of the two results was reported. B present in the method blank at __ . C The batch control sample failed to meet the required acceptance criteria. D Result obtained through analysis of a sample dilution. E Concentration exceeds the instrument calibration range. F Internal standard area failed to meet the required acceptance criteria in repeat instrumental analyses. Results should be interpreted as estimated concentrations. G The Method of Standard Additions (MSA) was used to quantify the concentration.

Measurement Type Descriptions 0900006480f92db5.xls 1 of 2

### Vinyl Institute 30 Day Concentration Database Measurement Types for Reported Data Submitted to EPA in Support of VI Comments on the Proposed PVC MACT Rule, August 2, 2011

**Measurement Type Descriptions** H Test performed after the expiration of the appropriate regulatory/advisory maximum allowable hold time. J Estimated value; value between the MOL and the RDL. M Analyte failed to meet the required acceptance criteria for duplicate analysis. P Chemical preservation discrepancy noted at the time of analysis. Q Analyte failed to meet the required acceptance criteria for spike recovery in the Matrix Spike (MS) and Matrix Spike Duplicate (MSD) due to apparent matrix effects. R Analyte failed to meet the required acceptance criteria for relative percent difference (RPD) between the Matrix Spike and Matrix Spike Duplicate (MS/MSD). S Surrogate compound diluted below a reliable quantitation level. T Surrogate recovery failed to meet the required acceptance criteria in initial analysis. Sample was reextracted (if applicable) and re-analyzed, and the surrogate recovery was outside of the required acceptance criteria on the second analysis, also. Results should be interpreted as estimated concentrations. U Parameter was analyzed for, but not detected above the reporting limit. V Verification standard recovery failed to meet the required acceptance criteria on repeat instrumental analyses. WSurrogate recovery failed to meet the required acceptance criteria in initial analysis. Sample was reextracted (if applicable) beyond the maximum allowable hold time, and re-analyzed. The surrogate recovery was within the required acceptance criteria on this second analysis. NA Not analyzed. NR Not requested. X Miscellaneous; see comments.

Measurement Type Descriptions 0900006480f92db5.xls 2 of 2