### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

667 Northside Unit 1 

### petroleum cokeFuel Type 2 Fuel Type 3 Other Fuel Description



### bituminousEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 667 Northside Unit 1 As Received Higher Heating Value 

### 667 Northside Unit 1 As Received % Moisture 

### 667 Northside Unit 1 As Received % Ash 

### 667 Northside Unit 1 As Received % Sulfur 

### 667 Northside Unit 1 Dry basis Higher Heating Value 

### 667 Northside Unit 1 Dry basis % Ash 

### 667 Northside Unit 1 Dry basis % Sulfur 

### 667 Northside Unit 1 Dry basis Antim ony 

### 667 Northside Unit 1 Dry basis Arsenic 

### 667 Northside Unit 1 Dry basis Beryllium 

### 667 Northside Unit 1 Dry basis Cadmium 

### 667 Northside Unit 1 Dry basis Chlorine 

### 667 Northside Unit 1 Dry basis Chromium 

### 667 Northside Unit 1 Dry basis Cobalt 

### 667 Northside Unit 1 Dry basis Fluorine 

### 667 Northside Unit 1 Dry basis Lead 

### 667 Northside Unit 1 Dry basis Manganese 

### 667 Northside Unit 1 Dry basis Mercury 

### 667 Northside Unit 1 Dry basis Nickel 

### 667 Northside Unit 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 ASTM D5142 ASTM D4239 ASTM D5865 ASTM D5142 ASTM D4239 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 XRF ASTM D6357 ASTM D6357

ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 XRFEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 667 Northside Unit 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 

### 5/18/2010 5/18/2010 13735.00 Btu/lb 2 5/18/2010 5/18/2010 13668.00 Btu/lb 3 5/18/2010 5/18/2010 13745.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.44 2.79 3.2 14680 Btu/lb 2.98 3.42 6.76 2.92 2.79 14659 Btu/lb 3.13 2.99 6.18 3.17 3.23 14650 Btu/lb 3.38 3.44Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 154 mg/kg 0.025 mg/Kg 1.41 mg/Kg 1.04 mg/Kg 0.15 144 mg/Kg 0.005 mg/Kg [<.021] mg/Kg 0.78 mg/Kg [<.021] 134 mg/Kg 0.012 mg/Kg [<.034] mg/Kg 0.98 mg/Kg [<.034]Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg 0.119 mg/Kg 3.59 mg/Kg 0.15 mg/Kg 16.25 mg/Kg mg/Kg 0.1117 mg/Kg 1.851 mg/Kg 0.473 mg/Kg 5.671 mg/Kg mg/Kg 0.1213 mg/Kg 4.509 mg/Kg 0.848 mg/Kg 6.121 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 384.63 mg/Kg 1.2 mg/Kg 3.72 mg/Kg 324.338 mg/Kg 1.1 mg/Kg 2.226 mg/Kg 357.496 mg/Kg 1 mg/Kg 2.978 mg/Kg Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 15.46 2.98 81.56 86.39 3.43 1.79 16.71 2.14 81.15 86.74 3.65 1.72 4.08 13.35 3.38 83.27 86.36 3.37 1.74 3.44 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 1.99 1.67 1.71EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 667 Northside Unit 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 1 

### 5/19/2010 5/19/2010 13751.00 Btu/lb 2 5/20/2010 5/20/2010 13223.00 Btu/lb 3 5/20/2010 5/20/2010 13745.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 5.28 3.97 4.4 14518 Btu/lb 4.19 4.65 6.66 5.2 3.23 14167 Btu/lb 5.57 3.46 6.18 3.17 3.23 14650 Btu/lb 3.38 3.44Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 203 mg/kg 144 mg/kg 0.005 mg/kg [<.021] mg/kg 0.78 mg/kg [<.021] 134 mg/kg 0.012 mg/kg [<.034] mg/kg 0.98 mg/kg [<.034]Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units


### mg/kg 0.1117 mg/kg 1.851 mg/kg 0.473 mg/kg 5.671 mg/kg mg/kg 0.1213 mg/kg 4.509 mg/kg 0.848 mg/kg 6.121 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 25 mg/kg 324.338 mg/kg 1.1 mg/kg [<25] mg/kg 2.226 mg/kg 357.496 mg/kg 1 mg/kg [<25} mg/kg 2.978 mg/kgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 13.06 4.19 82.75 85.33 3.23 1.53 4.65 16.71 2.14 81.15 86.74 3.65 1.72 4.08 13.35 3.38 83.27 86.36 3.37 1.74 3.44 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 1.07 1.67 1.71EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 667 Northside Unit 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 

### 5/20/2010 5/20/2010 13541.00 Btu/lb 2 5/21/2010 5/21/2010 13535.00 Btu/lb 3 5/21/2010 5/21/2010 13745.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 7.01 3.33 3.06 14562 Btu/lb 3.58 3.29 7.92 3.47 3.74 14699 Btu/lb 3.77 4.06 6.18 3.17 3.23 14650 Btu/lb 3.38 3.44Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)



### 144 mg/kg 0.005 mg/kg [<.021] mg/kg 0.78 mg/kg [<.021] 134 mg/kg 0.012 mg/kg [<.034] mg/kg 0.98 mg/kg [<.034]Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units


### mg/kg 0.1117 mg/kg 1.851 mg/kg 0.473 mg/kg 5.671 mg/kg mg/kg 0.1213 mg/kg 4.509 mg/kg 0.848 mg/kg 6.121 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture



### 324.338 mg/kg 1.1 mg/kg 2.226 mg/kg 357.496 mg/kg 1 mg/kg 2.978 mg/kg Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 20.29 3.58 76.13 84.55 3.64 1.75 3.29 3.19 16.71 2.14 81.15 86.74 3.65 1.72 4.08 1.67 13.35 3.38 83.27 86.36 3.37 1.74 3.44 1.71 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 667 Northside Unit 1 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 

### 5/25/2010 5/25/2010 13694.00 Btu/lb 2 5/26/2010 5/26/2010 13786.00 Btu/lb 3 5/27/2010 5/27/2010 13745.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.26 3.86 3.58 14609 Btu/lb 4.12 3.82 7.73 1.97 3.76 14941 Btu/lb 2.14 4.08 6.18 3.17 3.23 14650 Btu/lb 3.38 3.44Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 191 mg/kg 0.01 mg/kg [<.041] mg/kg 0.99 mg/kg [<.041] 144 mg/kg 0.005 mg/kg [<.021] mg/kg 0.78 mg/kg [<.021] 134 mg/kg 0.012 mg/kg [<.034] mg/kg 0.98 mg/kg [<.034]Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/kg 0.1149 mg/kg 3.543 mg/kg 0.935 mg/kg 10.926 mg/kg mg/kg 0.1117 mg/kg 1.851 mg/kg 0.473 mg/kg 5.671 mg/kg mg/kg 0.1213 mg/kg 4.509 mg/kg 0.848 mg/kg 6.121 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 358.695 mg/kg 1 mg/kg 3.152 mg/kg 324.338 mg/kg 1.1 mg/kg 2.226 mg/kg 357.496 mg/kg 1 mg/kg 2.978 mg/kg Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 16.23 4.12 79.65 82.53 3.48 1.68 3.82 4.37 16.71 2.14 81.15 86.74 3.65 1.72 4.08 1.67 13.35 3.38 83.27 86.36 3.37 1.74 3.44 1.71 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm