Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-001 Date Collected: 08/28/2013 Date Received: 8/28/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 17.6 ug/L 0.050 0.010 DPC 09/11/2013 14:35 EPA 200.8

Arsenic, As 115 ug/L 0.10 0.030 DPC 09/11/2013 14:35 EPA 200.8

Barium, Ba 976 ug/L 0.10 0.020 DPC 09/11/2013 14:35 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 09/12/2013 08:24 EPA 200.7

Cadmium, Cd 210 ug/L 0.050 0.010 DPC 09/11/2013 14:35 EPA 200.8

Chromium, Cr 336 ug/L 0.20 0.040 DPC 09/11/2013 14:35 EPA 200.8

Cobalt, Co 255 ug/L 0.020 0.0040 DPC 09/11/2013 14:35 EPA 200.8

Copper, Cu 266 ug/L 0.050 0.010 DPC 09/11/2013 14:35 EPA 200.8

Lead, Pb 153 ug/L 0.010 0.0020 DPC 09/11/2013 14:35 EPA 200.8

Mercury, Hg 184000 ng/L 5000 2000 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 364 ug/L 0.050 0.010 DPC 09/11/2013 14:35 EPA 200.8

Nickel, Ni 1460 ug/L 0.20 0.050 DPC 09/11/2013 14:35 EPA 200.8

Selenium, Se 916 ug/L 0.50 0.20 DPC 09/11/2013 14:35 EPA 200.8

Silver, Ag 0.168 ug/L 0.010 0.0020 DPC 09/11/2013 14:35 EPA 200.8

Thallium, Tl 13.5 ug/L 0.050 0.0020 DPC 09/11/2013 14:35 EPA 200.8

Tin, Sn 1380 ug/L 500 150 DAM 09/12/2013 08:25 EPA 200.7

Titanium, Ti 157 ug/L 100 15 DAM 09/12/2013 08:25 EPA 200.7

Zinc, Zn 2440 ug/L 0.50 0.10 DPC 09/11/2013 14:35 EPA 200.8

Aluminum, Al 12.2 mg/L 0.0010 0.0003 DPC 09/11/2013 14:35 EPA 200.8

Boron, B 386 mg/L 1.0 0.20 DAM 09/12/2013 08:24 EPA 200.7

Calcium, Ca 5680 mg/L 1.0 0.20 DAM 09/12/2013 08:24 EPA 200.7

Iron, Fe 123 mg/L 2.5 0.50 DAM 09/12/2013 08:24 EPA 200.7

Magnesium, Mg 3600 mg/L 0.50 0.10 DAM 09/12/2013 08:24 EPA 200.7

Manganese, Mn 73.5 mg/L 0.025 0.0050 DAM 09/12/2013 08:24 EPA 200.7

Potassium, K 65.1 mg/L 2.5 0.35 DAM 09/12/2013 08:23 EPA 200.7

Sodium, Na 324 mg/L 1.5 0.40 DAM 09/12/2013 08:23 EPA 200.7

Strontium, Sr 36.2 mg/L 0.050 0.015 DAM 09/12/2013 08:23 EPA 200.7

Ammonia, NH3, as N < 0.20 mg/L U 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.11 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 3.30 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 1 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-001A Date Collected: 08/28/2013 Date Received: 8/28/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.03 ug/L 0.050 0.010 DPC 09/11/2013 14:40 EPA 200.8

Arsenic, As 3.21 ug/L 0.10 0.030 DPC 09/11/2013 14:40 EPA 200.8

Barium, Ba 64.7 ug/L 0.10 0.020 DPC 09/11/2013 14:40 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 09/12/2013 08:28 EPA 200.7

Cadmium, Cd 120 ug/L 0.050 0.010 DPC 09/11/2013 14:40 EPA 200.8

Chromium, Cr 0.6 ug/L 0.20 0.040 DPC 09/11/2013 14:40 EPA 200.8

Cobalt, Co 166 ug/L 0.020 0.0040 DPC 09/11/2013 14:40 EPA 200.8

Copper, Cu 3.86 ug/L 0.050 0.010 DPC 09/11/2013 14:40 EPA 200.8

Lead, Pb 0.100 ug/L 0.010 0.0020 DPC 09/11/2013 14:40 EPA 200.8

Mercury, Hg 51.9 ng/L 10 4.0 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 206 ug/L 0.050 0.010 DPC 09/11/2013 14:40 EPA 200.8

Nickel, Ni 963 ug/L 0.20 0.050 DPC 09/11/2013 14:40 EPA 200.8

Selenium, Se 228 ug/L 0.50 0.20 DPC 09/11/2013 14:40 EPA 200.8

Selenite, Se+4 (Hydride) 142 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.017 ug/L 0.010 0.0020 DPC 09/11/2013 14:40 EPA 200.8

Thallium, Tl 6.83 ug/L 0.050 0.0020 DPC 09/11/2013 14:40 EPA 200.8

Tin, Sn 552 ug/L 500 150 DAM 09/12/2013 08:29 EPA 200.7

Titanium, Ti < 15 ug/L U 100 15 DAM 09/12/2013 08:29 EPA 200.7

Zinc, Zn 421 ug/L 0.50 0.10 DPC 09/11/2013 14:40 EPA 200.8

Aluminum, Al 0.0529 mg/L 0.0010 0.0003 DPC 09/11/2013 14:40 EPA 200.8

Boron, B 384 mg/L 1.0 0.20 DAM 09/12/2013 08:28 EPA 200.7

Calcium, Ca 753 mg/L 1.0 0.20 DAM 09/12/2013 08:28 EPA 200.7

Iron, Fe < 0.50 mg/L U 2.5 0.50 DAM 09/12/2013 08:29 EPA 200.7

Magnesium, Mg 3230 mg/L 0.50 0.10 DAM 09/12/2013 08:28 EPA 200.7

Manganese, Mn 68.9 mg/L 0.025 0.0050 DAM 09/12/2013 08:28 EPA 200.7

Potassium, K 59.8 mg/L 2.5 0.35 DAM 09/12/2013 08:27 EPA 200.7

Sodium, Na 320 mg/L 1.5 0.40 DAM 09/12/2013 08:27 EPA 200.7

Strontium, Sr 11.2 mg/L 0.050 0.015 DAM 09/12/2013 08:27 EPA 200.7

Mountaineer Plant, 133553 Page 2 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-002 Date Collected: 08/28/2013 Date Received: 8/28/2013

 CPS Primary Clarifier Effluent

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.43 ug/L 0.050 0.010 DPC 09/11/2013 14:45 EPA 200.8

Arsenic, As 4.05 ug/L 0.10 0.030 DPC 09/11/2013 14:45 EPA 200.8

Barium, Ba 85.5 ug/L 0.10 0.020 DPC 09/11/2013 14:45 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 08:33 EPA 200.7

Cadmium, Cd 0.94 ug/L 0.050 0.010 DPC 09/11/2013 14:45 EPA 200.8

Chromium, Cr 7.3 ug/L 0.20 0.040 DPC 09/11/2013 14:45 EPA 200.8

Cobalt, Co 13.0 ug/L 0.020 0.0040 DPC 09/11/2013 14:45 EPA 200.8

Copper, Cu 1.86 ug/L 0.050 0.010 DPC 09/11/2013 14:45 EPA 200.8

Lead, Pb 1.02 ug/L 0.010 0.0020 DPC 09/11/2013 14:45 EPA 200.8

Mercury, Hg 819 ng/L 250 100 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 281 ug/L 0.050 0.010 DPC 09/11/2013 14:45 EPA 200.8

Nickel, Ni 124 ug/L 0.20 0.050 DPC 09/11/2013 14:45 EPA 200.8

Selenium, Se 301 ug/L 0.50 0.20 DPC 09/11/2013 14:45 EPA 200.8

Silver, Ag 0.0060 ug/L J 0.010 0.0020 DPC 09/11/2013 14:45 EPA 200.8

Thallium, Tl 3.27 ug/L 0.050 0.0020 DPC 09/11/2013 14:45 EPA 200.8

Tin, Sn 177 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be matrix interference present.

09/12/2013 08:33

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 08:33 EPA 200.7

Zinc, Zn 15.2 ug/L 0.50 0.10 DPC 09/11/2013 14:45 EPA 200.8

Aluminum, Al 0.336 mg/L 0.0010 0.0003 DPC 09/11/2013 14:45 EPA 200.8

Boron, B 338 mg/L 0.20 0.040 DAM 09/12/2013 08:32 EPA 200.7

Calcium, Ca 851 mg/L 0.20 0.040 DAM 09/12/2013 08:32 EPA 200.7

Iron, Fe 0.968 mg/L 0.50 0.10 DAM 09/12/2013 08:33 EPA 200.7

Magnesium, Mg 2850 mg/L 0.10 0.020 DAM 09/12/2013 08:32 EPA 200.7

Manganese, Mn 42.3 mg/L 0.0050 0.0010 DAM 09/12/2013 08:32 EPA 200.7

Potassium, K 55.7 mg/L 0.50 0.070 DAM 09/12/2013 08:31 EPA 200.7

Sodium, Na 293 mg/L 0.30 0.080 DAM 09/12/2013 08:31 EPA 200.7

Strontium, Sr 9.95 mg/L 0.010 0.0030 DAM 09/12/2013 08:31 EPA 200.7

Ammonia, NH3, as N 9.03 mg/L 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 5.55 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 28.8 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 3 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-002A Date Collected: 08/28/2013 Date Received: 8/28/2013

 CPS Primary Clarifier Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.23 ug/L 0.050 0.010 DPC 09/11/2013 14:49 EPA 200.8

Arsenic, As 3.00 ug/L 0.10 0.030 DPC 09/11/2013 14:49 EPA 200.8

Barium, Ba 78.7 ug/L 0.10 0.020 DPC 09/11/2013 14:49 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 08:37 EPA 200.7

Cadmium, Cd 0.37 ug/L 0.050 0.010 DPC 09/11/2013 14:49 EPA 200.8

Chromium, Cr 3.3 ug/L 0.20 0.040 DPC 09/11/2013 14:49 EPA 200.8

Cobalt, Co 11.9 ug/L 0.020 0.0040 DPC 09/11/2013 14:49 EPA 200.8

Copper, Cu 0.40 ug/L 0.050 0.010 DPC 09/11/2013 14:49 EPA 200.8

Lead, Pb 0.011 ug/L 0.010 0.0020 DPC 09/11/2013 14:49 EPA 200.8

Mercury, Hg 9.6 ng/L J 10 4.0 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 265 ug/L 0.050 0.010 DPC 09/11/2013 14:49 EPA 200.8

Nickel, Ni 112 ug/L 0.20 0.050 DPC 09/11/2013 14:49 EPA 200.8

Selenium, Se 284 ug/L 0.50 0.20 DPC 09/11/2013 14:49 EPA 200.8

Selenite, Se+4 (Hydride) 222 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/11/2013 14:49 EPA 200.8

Thallium, Tl 3.17 ug/L 0.050 0.0020 DPC 09/11/2013 14:49 EPA 200.8

Tin, Sn 241 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be matrix interference present.

09/12/2013 08:37

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 08:37 EPA 200.7

Zinc, Zn 5.9 ug/L 0.50 0.10 DPC 09/11/2013 14:49 EPA 200.8

Aluminum, Al 0.0289 mg/L 0.0010 0.0003 DPC 09/11/2013 14:49 EPA 200.8

Boron, B 338 mg/L 0.20 0.040 DAM 09/12/2013 08:37 EPA 200.7

Calcium, Ca 842 mg/L 0.20 0.040 DAM 09/12/2013 08:37 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/12/2013 08:37 EPA 200.7

Magnesium, Mg 2850 mg/L 0.10 0.020 DAM 09/12/2013 08:37 EPA 200.7

Manganese, Mn 42.2 mg/L 0.0050 0.0010 DAM 09/12/2013 08:37 EPA 200.7

Potassium, K 55.1 mg/L 0.50 0.070 DAM 09/12/2013 08:35 EPA 200.7

Sodium, Na 293 mg/L 0.30 0.080 DAM 09/12/2013 08:35 EPA 200.7

Strontium, Sr 9.84 mg/L 0.010 0.0030 DAM 09/12/2013 08:35 EPA 200.7

Mountaineer Plant, 133553 Page 4 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-003 Date Collected: 08/28/2013 Date Received: 8/28/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.91 ug/L 0.050 0.010 DPC 09/11/2013 14:54 EPA 200.8

Arsenic, As 2.91 ug/L 0.10 0.030 DPC 09/11/2013 14:54 EPA 200.8

Barium, Ba 79.9 ug/L 0.10 0.020 DPC 09/11/2013 14:54 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 08:48 EPA 200.7

Cadmium, Cd 0.33 ug/L 0.050 0.010 DPC 09/11/2013 14:54 EPA 200.8

Chromium, Cr 3.7 ug/L 0.20 0.040 DPC 09/11/2013 14:54 EPA 200.8

Cobalt, Co 2.88 ug/L 0.020 0.0040 DPC 09/11/2013 14:54 EPA 200.8

Copper, Cu 0.75 ug/L 0.050 0.010 DPC 09/11/2013 14:54 EPA 200.8

Lead, Pb 0.229 ug/L 0.010 0.0020 DPC 09/11/2013 14:54 EPA 200.8

Mercury, Hg 185 ng/L 20 8.0 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 254 ug/L 0.050 0.010 DPC 09/11/2013 14:54 EPA 200.8

Nickel, Ni 40.4 ug/L 0.20 0.050 DPC 09/11/2013 14:54 EPA 200.8

Selenium, Se 247 ug/L 0.50 0.20 DPC 09/11/2013 14:54 EPA 200.8

Silver, Ag 0.0040 ug/L J 0.010 0.0020 DPC 09/11/2013 14:54 EPA 200.8

Thallium, Tl 1.52 ug/L 0.050 0.0020 DPC 09/11/2013 14:54 EPA 200.8

Tin, Sn 186 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be matrix interference present.

09/12/2013 08:48

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 08:48 EPA 200.7

Zinc, Zn 4.4 ug/L 0.50 0.10 DPC 09/11/2013 14:54 EPA 200.8

Aluminum, Al 0.285 mg/L 0.0010 0.0003 DPC 09/11/2013 14:54 EPA 200.8

Boron, B 285 mg/L 0.20 0.040 DAM 09/12/2013 08:48 EPA 200.7

Calcium, Ca 726 mg/L 0.20 0.040 DAM 09/12/2013 08:48 EPA 200.7

Iron, Fe 0.28 mg/L J 0.50 0.10 DAM 09/12/2013 08:48 EPA 200.7

Magnesium, Mg 2410 mg/L 0.10 0.020 DAM 09/12/2013 08:48 EPA 200.7

Manganese, Mn 35.1 mg/L 0.0050 0.0010 DAM 09/12/2013 08:48 EPA 200.7

Potassium, K 47.6 mg/L 0.50 0.070 DAM 09/12/2013 08:47 EPA 200.7

Sodium, Na 250 mg/L 0.30 0.080 DAM 09/12/2013 08:47 EPA 200.7

Strontium, Sr 8.51 mg/L 0.010 0.0030 DAM 09/12/2013 08:47 EPA 200.7

Ammonia, NH3, as N 10.0 mg/L 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 5.17 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 23.2 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 5 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-003A Date Collected: 08/28/2013 Date Received: 8/28/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.81 ug/L 0.050 0.010 DPC 09/11/2013 15:33 EPA 200.8

Arsenic, As 2.61 ug/L 0.10 0.030 DPC 09/11/2013 15:33 EPA 200.8

Barium, Ba 75.6 ug/L 0.10 0.020 DPC 09/11/2013 15:33 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 08:57 EPA 200.7

Cadmium, Cd 0.09 ug/L 0.050 0.010 DPC 09/11/2013 15:33 EPA 200.8

Chromium, Cr 2.5 ug/L 0.20 0.040 DPC 09/11/2013 15:33 EPA 200.8

Cobalt, Co 0.294 ug/L 0.020 0.0040 DPC 09/11/2013 15:33 EPA 200.8

Copper, Cu 0.35 ug/L 0.050 0.010 DPC 09/11/2013 15:33 EPA 200.8

Lead, Pb 0.010 ug/L 0.010 0.0020 DPC 09/11/2013 15:33 EPA 200.8

Mercury, Hg 2.9 ng/L 2.0 0.80 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 251 ug/L 0.050 0.010 DPC 09/11/2013 15:33 EPA 200.8

Nickel, Ni 16.4 ug/L 0.20 0.050 DPC 09/11/2013 15:33 EPA 200.8

Selenium, Se 243 ug/L 0.50 0.20 DPC 09/11/2013 15:33 EPA 200.8

Selenite, Se+4 (Hydride) 194 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/11/2013 15:33 EPA 200.8

Thallium, Tl 1.13 ug/L 0.050 0.0020 DPC 09/11/2013 15:33 EPA 200.8

Tin, Sn 251 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be matrix interference present.

09/12/2013 08:57

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 08:57 EPA 200.7

Zinc, Zn 1.4 ug/L 0.50 0.10 DPC 09/11/2013 15:33 EPA 200.8

Aluminum, Al 0.0220 mg/L 0.0010 0.0003 DPC 09/11/2013 15:33 EPA 200.8

Boron, B 284 mg/L 0.20 0.040 DAM 09/12/2013 08:57 EPA 200.7

Calcium, Ca 724 mg/L 0.20 0.040 DAM 09/12/2013 08:57 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/12/2013 08:57 EPA 200.7

Magnesium, Mg 2400 mg/L 0.10 0.020 DAM 09/12/2013 08:57 EPA 200.7

Manganese, Mn 35.0 mg/L 0.0050 0.0010 DAM 09/12/2013 08:57 EPA 200.7

Potassium, K 47.4 mg/L 0.50 0.070 DAM 09/12/2013 08:56 EPA 200.7

Sodium, Na 250 mg/L 0.30 0.080 DAM 09/12/2013 08:56 EPA 200.7

Strontium, Sr 8.51 mg/L 0.010 0.0030 DAM 09/12/2013 08:56 EPA 200.7

Mountaineer Plant, 133553 Page 6 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-004 Date Collected: 08/28/2013 Date Received: 8/28/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 12.8 ug/L 0.050 0.010 DPC 09/11/2013 15:37 EPA 200.8

Arsenic, As 40.8 ug/L 0.10 0.030 DPC 09/11/2013 15:37 EPA 200.8

Barium, Ba 31.5 ug/L 0.10 0.020 DPC 09/11/2013 15:37 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:06 EPA 200.7

Cadmium, Cd 1.79 ug/L 0.050 0.010 DPC 09/11/2013 15:37 EPA 200.8

Chromium, Cr 0.3 ug/L 0.20 0.040 DPC 09/11/2013 15:37 EPA 200.8

Cobalt, Co 2.72 ug/L 0.020 0.0040 DPC 09/11/2013 15:37 EPA 200.8

Copper, Cu 0.50 ug/L 0.050 0.010 DPC 09/11/2013 15:37 EPA 200.8

Lead, Pb 0.082 ug/L 0.010 0.0020 DPC 09/11/2013 15:37 EPA 200.8

Mercury, Hg 56.9 ng/L 10 4.0 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 7470 ug/L 0.050 0.010 DPC 09/11/2013 15:37 EPA 200.8

Nickel, Ni 8.03 ug/L 0.20 0.050 DPC 09/11/2013 15:37 EPA 200.8

Selenium, Se 295 ug/L 0.50 0.20 DPC 09/11/2013 15:37 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/11/2013 15:37 EPA 200.8

Thallium, Tl 2.48 ug/L 0.050 0.0020 DPC 09/11/2013 15:37 EPA 200.8

Tin, Sn 133 ug/L 100 30 DAM 09/12/2013 09:06 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:06 EPA 200.7

Zinc, Zn 3.6 ug/L 0.50 0.10 DPC 09/11/2013 15:37 EPA 200.8

Aluminum, Al 0.0370 mg/L 0.0010 0.0003 DPC 09/11/2013 15:37 EPA 200.8

Boron, B 54.1 mg/L 0.20 0.040 DAM 09/12/2013 09:06 EPA 200.7

Calcium, Ca 434 mg/L 0.20 0.040 DAM 09/12/2013 09:06 EPA 200.7

Iron, Fe 0.13 mg/L J 0.50 0.10 DAM 09/12/2013 09:06 EPA 200.7

Magnesium, Mg 406 mg/L 0.10 0.020 DAM 09/12/2013 09:06 EPA 200.7

Manganese, Mn 1.38 mg/L 0.0050 0.0010 DAM 09/12/2013 09:06 EPA 200.7

Potassium, K 113 mg/L 0.50 0.070 DAM 09/12/2013 09:05 EPA 200.7

Sodium, Na 1860 mg/L 0.30 0.080 DAM 09/12/2013 09:05 EPA 200.7

Strontium, Sr 5.65 mg/L 0.010 0.0030 DAM 09/12/2013 09:05 EPA 200.7

Ammonia, NH3, as N 2.34 mg/L 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.61 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.33 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 7 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-004A Date Collected: 08/28/2013 Date Received: 8/28/2013

Landfill Leachate Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 12.8 ug/L 0.050 0.010 DPC 09/11/2013 15:42 EPA 200.8

Arsenic, As 39.5 ug/L 0.10 0.030 DPC 09/11/2013 15:42 EPA 200.8

Barium, Ba 30.4 ug/L 0.10 0.020 DPC 09/11/2013 15:42 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:10 EPA 200.7

Cadmium, Cd 1.49 ug/L 0.050 0.010 DPC 09/11/2013 15:42 EPA 200.8

Chromium, Cr 0.2 ug/L 0.20 0.040 DPC 09/11/2013 15:42 EPA 200.8

Cobalt, Co 2.05 ug/L 0.020 0.0040 DPC 09/11/2013 15:42 EPA 200.8

Copper, Cu 0.34 ug/L 0.050 0.010 DPC 09/11/2013 15:42 EPA 200.8

Lead, Pb 0.052 ug/L 0.010 0.0020 DPC 09/11/2013 15:42 EPA 200.8

Mercury, Hg 9.7 ng/L 2.0 0.80 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 7650 ug/L 0.050 0.010 DPC 09/11/2013 15:42 EPA 200.8

Nickel, Ni 7.20 ug/L 0.20 0.050 DPC 09/11/2013 15:42 EPA 200.8

Selenium, Se 284 ug/L 0.50 0.20 DPC 09/11/2013 15:42 EPA 200.8

Selenite, Se+4 (Hydride) 147 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/11/2013 15:42 EPA 200.8

Thallium, Tl 2.42 ug/L 0.050 0.0020 DPC 09/11/2013 15:42 EPA 200.8

Tin, Sn 143 ug/L 100 30 DAM 09/12/2013 09:10 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:10 EPA 200.7

Zinc, Zn 2.9 ug/L 0.50 0.10 DPC 09/11/2013 15:42 EPA 200.8

Aluminum, Al 0.0083 mg/L 0.0010 0.0003 DPC 09/11/2013 15:42 EPA 200.8

Boron, B 52.9 mg/L 0.20 0.040 DAM 09/12/2013 09:10 EPA 200.7

Calcium, Ca 425 mg/L 0.20 0.040 DAM 09/12/2013 09:10 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/12/2013 09:10 EPA 200.7

Magnesium, Mg 396 mg/L 0.10 0.020 DAM 09/12/2013 09:10 EPA 200.7

Manganese, Mn 0.982 mg/L 0.0050 0.0010 DAM 09/12/2013 09:10 EPA 200.7

Potassium, K 110 mg/L 0.50 0.070 DAM 09/12/2013 09:09 EPA 200.7

Sodium, Na 1820 mg/L 0.30 0.080 DAM 09/12/2013 09:09 EPA 200.7

Strontium, Sr 5.51 mg/L 0.010 0.0030 DAM 09/12/2013 09:09 EPA 200.7

Mountaineer Plant, 133553 Page 8 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-005 Date Collected: 08/28/2013 Date Received: 8/28/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.77 ug/L 0.050 0.010 DPC 09/11/2013 15:47 EPA 200.8

Arsenic, As 17.0 ug/L 0.10 0.030 DPC 09/11/2013 15:47 EPA 200.8

Barium, Ba 57.8 ug/L 0.10 0.020 DPC 09/11/2013 15:47 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:14 EPA 200.7

Cadmium, Cd 0.91 ug/L 0.050 0.010 DPC 09/11/2013 15:47 EPA 200.8

Chromium, Cr 2.3 ug/L 0.20 0.040 DPC 09/11/2013 15:47 EPA 200.8

Cobalt, Co 2.21 ug/L 0.020 0.0040 DPC 09/11/2013 15:47 EPA 200.8

Copper, Cu 0.54 ug/L 0.050 0.010 DPC 09/11/2013 15:47 EPA 200.8

Lead, Pb 0.156 ug/L 0.010 0.0020 DPC 09/11/2013 15:47 EPA 200.8

Mercury, Hg 120 ng/L 10 4.0 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 3110 ug/L 0.050 0.010 DPC 09/11/2013 15:47 EPA 200.8

Nickel, Ni 21.2 ug/L 0.20 0.050 DPC 09/11/2013 15:47 EPA 200.8

Selenium, Se 244 ug/L 0.50 0.20 DPC 09/11/2013 15:47 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/11/2013 15:47 EPA 200.8

Thallium, Tl 2.10 ug/L 0.050 0.0020 DPC 09/11/2013 15:47 EPA 200.8

Tin, Sn 172 ug/L 100 30 DAM 09/12/2013 09:14 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:14 EPA 200.7

Zinc, Zn 2.8 ug/L 0.50 0.10 DPC 09/11/2013 15:47 EPA 200.8

Aluminum, Al 0.101 mg/L 0.0010 0.0003 DPC 09/11/2013 15:47 EPA 200.8

Boron, B 190 mg/L 0.20 0.040 DAM 09/12/2013 09:14 EPA 200.7

Calcium, Ca 600 mg/L 0.20 0.040 DAM 09/12/2013 09:14 EPA 200.7

Iron, Fe 0.20 mg/L J 0.50 0.10 DAM 09/12/2013 09:14 EPA 200.7

Magnesium, Mg 1550 mg/L 0.10 0.020 DAM 09/12/2013 09:14 EPA 200.7

Manganese, Mn 20.9 mg/L 0.0050 0.0010 DAM 09/12/2013 09:14 EPA 200.7

Potassium, K 73.7 mg/L 0.50 0.070 DAM 09/12/2013 09:13 EPA 200.7

Sodium, Na 923 mg/L 0.30 0.080 DAM 09/12/2013 09:13 EPA 200.7

Strontium, Sr 7.27 mg/L 0.010 0.0030 DAM 09/12/2013 09:13 EPA 200.7

Ammonia, NH3, as N 5.20 mg/L 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.57 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 15.7 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 9 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-005A Date Collected: 08/28/2013 Date Received: 8/28/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.28 ug/L 0.050 0.010 DPC 09/11/2013 15:52 EPA 200.8

Arsenic, As 14.8 ug/L 0.10 0.030 DPC 09/11/2013 15:52 EPA 200.8

Barium, Ba 53.7 ug/L 0.10 0.020 DPC 09/11/2013 15:52 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:18 EPA 200.7

Cadmium, Cd 0.71 ug/L 0.050 0.010 DPC 09/11/2013 15:52 EPA 200.8

Chromium, Cr 1.7 ug/L 0.20 0.040 DPC 09/11/2013 15:52 EPA 200.8

Cobalt, Co 0.927 ug/L 0.020 0.0040 DPC 09/11/2013 15:52 EPA 200.8

Copper, Cu 0.22 ug/L 0.050 0.010 DPC 09/11/2013 15:52 EPA 200.8

Lead, Pb 0.017 ug/L 0.010 0.0020 DPC 09/11/2013 15:52 EPA 200.8

Mercury, Hg 4.6 ng/L 2.0 0.80 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 2950 ug/L 0.050 0.010 DPC 09/11/2013 15:52 EPA 200.8

Nickel, Ni 12.2 ug/L 0.20 0.050 DPC 09/11/2013 15:52 EPA 200.8

Selenium, Se 229 ug/L 0.50 0.20 DPC 09/11/2013 15:52 EPA 200.8

Selenite, Se+4 (Hydride) 172 ug/L 20 4.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/11/2013 15:52 EPA 200.8

Thallium, Tl 1.85 ug/L 0.050 0.0020 DPC 09/11/2013 15:52 EPA 200.8

Tin, Sn 200 ug/L 100 30 DAM 09/12/2013 09:18 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:18 EPA 200.7

Zinc, Zn 2.0 ug/L 0.50 0.10 DPC 09/11/2013 15:52 EPA 200.8

Aluminum, Al 0.0135 mg/L 0.0010 0.0003 DPC 09/11/2013 15:52 EPA 200.8

Boron, B 188 mg/L 0.20 0.040 DAM 09/12/2013 09:18 EPA 200.7

Calcium, Ca 599 mg/L 0.20 0.040 DAM 09/12/2013 09:18 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 09/12/2013 09:18 EPA 200.7

Magnesium, Mg 1540 mg/L 0.10 0.020 DAM 09/12/2013 09:18 EPA 200.7

Manganese, Mn 20.7 mg/L 0.0050 0.0010 DAM 09/12/2013 09:18 EPA 200.7

Potassium, K 74.7 mg/L 0.50 0.070 DAM 09/12/2013 09:17 EPA 200.7

Sodium, Na 924 mg/L 0.30 0.080 DAM 09/12/2013 09:17 EPA 200.7

Strontium, Sr 7.27 mg/L 0.010 0.0030 DAM 09/12/2013 09:17 EPA 200.7

Mountaineer Plant, 133553 Page 10 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-006 Date Collected: 08/28/2013 Date Received: 8/28/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.67 ug/L 0.050 0.010 DPC 09/11/2013 15:57 EPA 200.8

Arsenic, As 8.96 ug/L 0.10 0.030 DPC 09/11/2013 15:57 EPA 200.8

Barium, Ba 56.5 ug/L 0.10 0.020 DPC 09/11/2013 15:57 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:34 EPA 200.7

Cadmium, Cd 0.54 ug/L 0.050 0.010 DPC 09/11/2013 15:57 EPA 200.8

Chromium, Cr 1.4 ug/L 0.20 0.040 DPC 09/11/2013 15:57 EPA 200.8

Cobalt, Co 2.61 ug/L 0.020 0.0040 DPC 09/11/2013 15:57 EPA 200.8

Copper, Cu 0.15 ug/L 0.050 0.010 DPC 09/11/2013 15:57 EPA 200.8

Lead, Pb 0.028 ug/L 0.010 0.0020 DPC 09/11/2013 15:57 EPA 200.8

Mercury, Hg 7.9 ng/L 2.0 0.80 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 2070 ug/L 0.050 0.010 DPC 09/11/2013 15:57 EPA 200.8

Nickel, Ni 21.3 ug/L 0.20 0.050 DPC 09/11/2013 15:57 EPA 200.8

Selenium, Se 12.4 ug/L 0.50 0.20 DPC 09/11/2013 15:57 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/11/2013 15:57 EPA 200.8

Thallium, Tl 0.97 ug/L 0.050 0.0020 DPC 09/11/2013 15:57 EPA 200.8

Tin, Sn 124 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be matrix interference present.

09/12/2013 09:34

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:34 EPA 200.7

Zinc, Zn 1.3 ug/L 0.50 0.10 DPC 09/11/2013 15:57 EPA 200.8

Aluminum, Al 1.07 mg/L 0.0010 0.0003 DPC 09/11/2013 15:57 EPA 200.8

Boron, B 180 mg/L 0.20 0.040 DAM 09/12/2013 09:34 EPA 200.7

Calcium, Ca 587 mg/L 0.20 0.040 DAM 09/12/2013 09:34 EPA 200.7

Iron, Fe 1.55 mg/L 0.50 0.10 DAM 09/12/2013 09:34 EPA 200.7

Magnesium, Mg 1480 mg/L 0.10 0.020 DAM 09/12/2013 09:34 EPA 200.7

Manganese, Mn 19.1 mg/L 0.0050 0.0010 DAM 09/12/2013 09:34 EPA 200.7

Potassium, K 75.0 mg/L 0.50 0.070 DAM 09/12/2013 09:32 EPA 200.7

Sodium, Na 920 mg/L 0.30 0.080 DAM 09/12/2013 09:32 EPA 200.7

Strontium, Sr 7.03 mg/L 0.010 0.0030 DAM 09/12/2013 09:32 EPA 200.7

Ammonia, NH3, as N 18.6 mg/L 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.69 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.41 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 11 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-006A Date Collected: 08/28/2013 Date Received: 8/28/2013

2nd Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.35 ug/L 0.050 0.010 DPC 09/11/2013 16:01 EPA 200.8

Arsenic, As 8.47 ug/L 0.10 0.030 DPC 09/11/2013 16:01 EPA 200.8

Barium, Ba 51.9 ug/L 0.10 0.020 DPC 09/11/2013 16:01 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:38 EPA 200.7

Cadmium, Cd 0.48 ug/L 0.050 0.010 DPC 09/11/2013 16:01 EPA 200.8

Chromium, Cr 1.1 ug/L 0.20 0.040 DPC 09/11/2013 16:01 EPA 200.8

Cobalt, Co 2.37 ug/L 0.020 0.0040 DPC 09/11/2013 16:01 EPA 200.8

Copper, Cu 0.10 ug/L 0.050 0.010 DPC 09/11/2013 16:01 EPA 200.8

Lead, Pb 0.016 ug/L 0.010 0.0020 DPC 09/11/2013 16:01 EPA 200.8

Mercury, Hg 3.2 ng/L 1.0 0.40 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 1930 ug/L 0.050 0.010 DPC 09/11/2013 16:01 EPA 200.8

Nickel, Ni 19.7 ug/L 0.20 0.050 DPC 09/11/2013 16:01 EPA 200.8

Selenium, Se 4.2 ug/L 0.50 0.20 DPC 09/11/2013 16:01 EPA 200.8

Selenite, Se+4 (Hydride) < 1.0 ug/L U 5.0 1.0 TLT 09/24/2013 AEP Method

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 09/11/2013 16:01 EPA 200.8

Thallium, Tl 0.90 ug/L 0.050 0.0020 DPC 09/11/2013 16:01 EPA 200.8

Tin, Sn 161 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be matrix interference present.

09/12/2013 09:38

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:38 EPA 200.7

Zinc, Zn 2.4 ug/L 0.50 0.10 DPC 09/11/2013 16:01 EPA 200.8

Aluminum, Al 0.985 mg/L 0.0010 0.0003 DPC 09/11/2013 16:01 EPA 200.8

Boron, B 176 mg/L 0.20 0.040 DAM 09/12/2013 09:38 EPA 200.7

Calcium, Ca 573 mg/L 0.20 0.040 DAM 09/12/2013 09:38 EPA 200.7

Iron, Fe 1.52 mg/L 0.50 0.10 DAM 09/12/2013 09:38 EPA 200.7

Magnesium, Mg 1440 mg/L 0.10 0.020 DAM 09/12/2013 09:38 EPA 200.7

Manganese, Mn 18.6 mg/L 0.0050 0.0010 DAM 09/12/2013 09:38 EPA 200.7

Potassium, K 73.5 mg/L 0.50 0.070 DAM 09/12/2013 09:36 EPA 200.7

Sodium, Na 899 mg/L 0.30 0.080 DAM 09/12/2013 09:36 EPA 200.7

Strontium, Sr 6.85 mg/L 0.010 0.0030 DAM 09/12/2013 09:36 EPA 200.7

Mountaineer Plant, 133553 Page 12 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-007 Date Collected: 08/28/2013 Date Received: 8/28/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.040 ug/L J 0.050 0.010 DPC 09/11/2013 16:06 EPA 200.8

Arsenic, As 0.85 ug/L 0.10 0.030 DPC 09/11/2013 16:06 EPA 200.8

Barium, Ba 65.5 ug/L 0.10 0.020 DPC 09/11/2013 16:06 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:42 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 09/11/2013 16:06 EPA 200.8

Chromium, Cr 0.8 ug/L 0.20 0.040 DPC 09/11/2013 16:06 EPA 200.8

Cobalt, Co 0.059 ug/L 0.020 0.0040 DPC 09/11/2013 16:06 EPA 200.8

Copper, Cu 0.05 ug/L 0.050 0.010 DPC 09/11/2013 16:06 EPA 200.8

Lead, Pb 0.019 ug/L 0.010 0.0020 DPC 09/11/2013 16:06 EPA 200.8

Mercury, Hg 1.9 ng/L 1.0 0.40 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 14.9 ug/L 0.050 0.010 DPC 09/11/2013 16:06 EPA 200.8

Nickel, Ni 2.45 ug/L 0.20 0.050 DPC 09/11/2013 16:06 EPA 200.8

Selenium, Se 0.8 ug/L 0.50 0.20 DPC 09/11/2013 16:06 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/11/2013 16:06 EPA 200.8

Thallium, Tl 0.024 ug/L J 0.050 0.0020 DPC 09/11/2013 16:06 EPA 200.8

Tin, Sn 194 ug/L 100 30 DAM 09/12/2013 09:42 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:42 EPA 200.7

Zinc, Zn 0.7 ug/L 0.50 0.10 DPC 09/11/2013 16:06 EPA 200.8

Aluminum, Al 2.40 mg/L 0.0010 0.0003 DPC 09/11/2013 16:06 EPA 200.8

Boron, B 196 mg/L 0.20 0.040 DAM 09/12/2013 09:42 EPA 200.7

Calcium, Ca 581 mg/L 0.20 0.040 DAM 09/12/2013 09:42 EPA 200.7

Iron, Fe 0.932 mg/L 0.50 0.10 DAM 09/12/2013 09:42 EPA 200.7

Magnesium, Mg 1500 mg/L 0.10 0.020 DAM 09/12/2013 09:42 EPA 200.7

Manganese, Mn 20.9 mg/L 0.0050 0.0010 DAM 09/12/2013 09:42 EPA 200.7

Potassium, K 75.4 mg/L 0.50 0.070 DAM 09/12/2013 09:40 EPA 200.7

Sodium, Na 882 mg/L 0.30 0.080 DAM 09/12/2013 09:40 EPA 200.7

Strontium, Sr 6.80 mg/L 0.010 0.0030 DAM 09/12/2013 09:40 EPA 200.7

Ammonia, NH3, as N 26.9 mg/L 0.50 0.20 TJK 09/05/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 5.35 mg/L 0.50 0.10 DMM 09/04/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.11 mg/L 0.10 0.020 DMM 09/03/2013 SM20 4500NO3 H

Mountaineer Plant, 133553 Page 13 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

Sample Number: 133553-007A Date Collected: 08/28/2013 Date Received: 8/28/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.06 ug/L 0.050 0.010 DPC 09/11/2013 16:11 EPA 200.8

Arsenic, As 0.65 ug/L 0.10 0.030 DPC 09/11/2013 16:11 EPA 200.8

Barium, Ba 57.6 ug/L 0.10 0.020 DPC 09/11/2013 16:11 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 09/12/2013 09:46 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 09/11/2013 16:11 EPA 200.8

Chromium, Cr 0.9 ug/L 0.20 0.040 DPC 09/11/2013 16:11 EPA 200.8

Cobalt, Co 0.052 ug/L 0.020 0.0040 DPC 09/11/2013 16:11 EPA 200.8

Copper, Cu 0.12 ug/L 0.050 0.010 DPC 09/11/2013 16:11 EPA 200.8

Lead, Pb 0.015 ug/L 0.010 0.0020 DPC 09/11/2013 16:11 EPA 200.8

Mercury, Hg 1.2 ng/L 0.50 0.20 TLT 09/12/2013 EPA 1631E

Molybdenum, Mo 11.2 ug/L 0.050 0.010 DPC 09/11/2013 16:11 EPA 200.8

Nickel, Ni 1.95 ug/L 0.20 0.050 DPC 09/11/2013 16:11 EPA 200.8

Selenium, Se 0.9 ug/L 0.50 0.20 DPC 09/11/2013 16:11 EPA 200.8

Selenite, Se+4 (Hydride) < 0.080 ug/L U 0.40 0.080 TLT 09/24/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/11/2013 16:11 EPA 200.8

Thallium, Tl 0.011 ug/L J 0.050 0.0020 DPC 09/11/2013 16:11 EPA 200.8

Tin, Sn 238 ug/L 100 30 DAM 09/12/2013 09:46 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 09/12/2013 09:46 EPA 200.7

Zinc, Zn 1.8 ug/L 0.50 0.10 DPC 09/11/2013 16:11 EPA 200.8

Aluminum, Al 2.10 mg/L 0.0010 0.0003 DPC 09/11/2013 16:11 EPA 200.8

Boron, B 192 mg/L 0.20 0.040 DAM 09/12/2013 09:46 EPA 200.7

Calcium, Ca 571 mg/L 0.20 0.040 DAM 09/12/2013 09:46 EPA 200.7

Iron, Fe 0.911 mg/L 0.50 0.10 DAM 09/12/2013 09:46 EPA 200.7

Magnesium, Mg 1480 mg/L 0.10 0.020 DAM 09/12/2013 09:46 EPA 200.7

Manganese, Mn 20.5 mg/L 0.0050 0.0010 DAM 09/12/2013 09:46 EPA 200.7

Potassium, K 74.1 mg/L 0.50 0.070 DAM 09/12/2013 09:44 EPA 200.7

Sodium, Na 868 mg/L 0.30 0.080 DAM 09/12/2013 09:44 EPA 200.7

Strontium, Sr 6.69 mg/L 0.010 0.0030 DAM 09/12/2013 09:44 EPA 200.7

Sample Number: 133553-008 Date Collected: 08/28/2013 Date Received: 8/28/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 0.45 ng/L J 0.50 0.20 TLT 09/12/2013 EPA 1631E

Mountaineer Plant, 133553 Page 14 of 15
Location: Mountaineer Plant Report Date: 10/8/2013

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 133553 Page 15 of 15