13339 Hagers Ferry Road

Huntersville, NC 28078-7929

McGuire Nuclear Complex - MG03A2

Phone: 980-875-5245 Fax: 980-875-4349

Order Summary Report

Analytical Laboratory

Order Number: J13060391

Project Name:

Lab Contact: Jason C Perkins

Date: 7/2/2013

Customer Address: 573 Duke Power Rd

Customer Name(s): josh Quinn, Zack Hall

Mail Code: Clliffside Steam Station

Mooresboro, NC 28024

Phone: 980-875-5348

Report Authorized By:

(Signature)

Program Comments:

Please contact the Program Manager (Jason C Perkins) with any questions regarding this report.

Data Flags & Calculations:

Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality 

system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) 

under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data 

included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the 

subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have 

been qualified by Duke Energy to perform these analyses except where noted.

Data Package:

This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of 

the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except 

in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The 

order of individual sections within this report is as follows:

Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, 

Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & 

Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)

Certification:

The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina 

(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of 

specific methods. 

Jason C Perkins

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Sample ID's & Descriptions:

Sample ID Plant/Station

Collection 

Date and Time Collected By Sample Description

2013014682 CLIFFSIDE 21-Jun-13 9:15 AM GLENN LONG BOTTOM ASH SLUICE 0.3m

2013014683 CLIFFSIDE 21-Jun-13 8:14 AM GLENN LONG FLYASH SLUICE 0.3m

2013014684 CLIFFSIDE 21-Jun-13 10:55 AM GLENN LONG SOURCE WATER (INTAKE 0.3m

2013014685 CLIFFSIDE 21-Jun-13 10:50 AM GLENN LONG ASH BASIN 0.3m

4 Total Samples

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COC and .pdf report are in agreement with sample totals 

and analyses (compliance programs and procedures).

All Results are less than the laboratory reporting limits.

All laboratory QA/QC requirements are acceptable.

Yes No

Technical Validation Review

Checklist:

Yes No

Yes No

Report Sections Included:

Job Summary Report Sub-contracted Laboratory Results

Sample Identification Customer Specific Data Sheets, Reports, & Documentation

Technical Validation of Data Package Customer Database Entries

Analytical Laboratory Certificate of Analysis

Analytical Laboratory QC Report

Chain of Custody

Reviewed By: DBA Account Date: 7/2/2013

Electronic Data Deliverable (EDD) Sent Separately

Page 3 of 9
Certificate of Laboratory Analysis

This report shall not be reproduced, except in full.

Order # J13060391

2013014682

Collection Date: 21-Jun-13 9:15 AM

Site: BOTTOM ASH SLUICE 0.3m

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

DF Analyst

SULFIDE - (Analysis Performed by Element One)

Vendor Parameter Complete Vendor Method V_ELE1

2013014683

Collection Date: 21-Jun-13 8:14 AM

Site: FLYASH SLUICE 0.3m

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

DF Analyst

SULFIDE - (Analysis Performed by Element One)

Vendor Parameter Complete Vendor Method V_ELE1

2013014684

Collection Date: 21-Jun-13 10:55 AM

Site: SOURCE WATER (INTAKE 0.3m

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

DF Analyst

SULFIDE - (Analysis Performed by Element One)

Vendor Parameter Complete Vendor Method V_ELE1

2013014685

Collection Date: 21-Jun-13 10:50 AM

Site: ASH BASIN 0.3m

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

DF Analyst

SULFIDE - (Analysis Performed by Element One)

Vendor Parameter Complete Vendor Method V_ELE1

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