# ca;g;,r . Cedar Rapids, Iowa West Soybean Plant Emission Test Report for Two Soybean Storage Bins - EP 101
January 24, 2007


# Thompson Environmental Consulting, Inc.

Environmental 

## Engineering, Permitting 

## and Compliance Services

### { '

...



## EMISSION TEST REPORT for Cargill Incorporated on the Two Soybean 

### StorageBins (EP 101) located 

### in Cedar Rapids, Iowa on January 24, 2007



### Conducted by Comprehensive Emission Services, Inc. 

### P.O. Box 910 Waukee, Iowa 50263 (515) 987-0200 Project No. 407

. 

## (

"\.. i·

- '... ..:.... ',.,

## TABLE OF CONTENTS

. , (


## CONTENTS
Preface
........................................................................· ................................................2 Introduction
................................................................................................................'3 Summary ofResults
...:...............................................................................................4 Sampling and Analytical Procedures
..........................................................................5 M17 Sampling Apparatus
............................................,.............................................6 Test Results
................................................................................................................7
Appendix A

- Example Calculations Appendix B

- Laboratory Data Forms Appendix C

- Field DataForms Appendix D - Pretest Calibrations Appendix E - Posttest Calibrations Appendix F**~** 

### Process Data Appendix G

- Opacity Certification


## TABLES
Table 1, Summary ofTest Results for the Two Soybean Storage Bins (EP 101)
.... ..4 

### Table 2, Particulate Emission Results for the Two Soybean Storage Bins (EP 101) 7



## .FIGURES
Figure 1, M17 Sampling Apparatus
...........................................................................6

## PREFACE ( 

### This report summarizes the results ofthe data collected for compliance testing performed at the Cargill Incorporated facility in Cedar Rapids, Iowa. To the best ofour knowledge, the data in this report are accurate and complete. Any questions concerning this report should be directed to Mr. Tim Titus or Mr. Matt Milligan. They may be reached by phone at (515) 987-0200.

February 12, 2007
.

2

## INTRODUCTION
An emission test was conducted by Comprehensive Emission Services on the Two Soybean Storage Bins (EP 101) at the Cargill Incorporated facility in Cedar Rapids, Iowa. Three Method 17 with 202 backbalfparticulate sampling runs and three Method 9, Opacityrtins were perfonned. The testing fulfills the requirements for testing 

### in the LCHD Pennit #A TI 5003. The testing was perfonned on January 24, 2007.
Coordinating the field tests:
Tim Titus

- Comprehensive Emission Services, Inc. Amelia Denning

- Cargill Incorporated Lisa Schmidt

- Thompson Environmental Consulting, Inc.
Conducting the field tests: Taylor Daily

- Comprehensive Emission Services, Inc. Mason Woltz

- Comprehensive Emission Services, Inc. Matt Milligan

- Comprehensive Emission Services, Inc.
Witnessing the field tests: Joseph Strahan

- Linn County Air Quality Division

The appendices to this report contain the following information and data: Appendix A: Example Calculations Appendix B:. Laboratory 

### Data Fonus Appendix C: Field Data Fonus Appendix D: Pretest Calibrations Appendix E: Posttest Calibrations Appendix F: Process Data Appendix G: Opacity Certification

. 3

## SUMMARY OF RESULTS
In accordance with current IDNRprotocol, when less 

### than 10 mg ofsample is collected, 10 mg ofsample catch is used for calculations. Sources with sample collections less than 10mg are shown with a '<'symbol inthe following tables to indicate that actual samples were less thanthe assmned 10 mg catch. Both the actual and the assumed emission rates can be found in Appendix C.
Table 1 smnmarizes the testresults for testing performed on the Two Soybean Storage Bins (EP 101). Three Method 

### i 7 with 202 backhalfp.?rticulate sampling runs and three Method 9, Opacity runs were performed. The testing fulfills the requirements for testing in the LeRD Permit #ATI 5003.
The allowable limit for PM is 0.0861blhr and 0.01 gr/dscf. The allowable limit for Opacity is 0%.
No blank corrections were performed.


### Table 1 Summary ofTest 

### Results Two Soybean 

### StorageBins (EP 101) units Run 1 Run 2 Run

### 3 PM Net Weight g <0.0100 <0.0100 <0.0100

PM Emission gr/dscf <0.0024 <0.0024 <0.0025 PM Emission Rate lblhr <0.021 <0.021 <0.021 Flow Rate acfin 952 947 948 Flow Rate dscfm 1,005 991 978 Isokinetics % 99.2 99.5 99.8 Run Start Time 

## HH:MM 9:32 12:08 14:09 Run Stop Time 

## HH:MM 11:38 13:41 15:40

Date ofTest 

### mmldd/yr 01124/07 ·01/24/07 01124107 Opacity % 0.0 ·0.0 ·0.0· Run Start Time 

## HH:MM 9:41 12:22 14:19 Run Stop Time 

## HH:MM 10:41 13:22 15:19

Date ofTest 

## mmlddlyr 01/24/07 

### 01/24/07 01124107

4 

### i

### SAMPLING AND ANALYTICAL PROCEDURES Sampling Procedures
Particulate emissions were determined by U.S. Environmental Protection Agency (EPA) Methods 1,2,3,4,17,202 and 9. These Methods are titled;
Method 1 - "Sample and Velocity Traverse for Stationary Sources" Method 2 - "Determination ofStack Gas Velocity and Volumetric Flow Rate" Method 3 - "Gas Analysis for Carbon Dioxide, Oxygen, Excess Air andDry Molecular Weight" Method 4 - "Determination for Moisture Content in Stack Gases"
. Method 17

- "Determination ofParticulate Emissions from Stationary Sources (In-Stack Filtration Method)" Method 202

- "Condensible Particulate Emissions"
. Method 9 - "Determination ofVisual Emissions from Stationary Sources" These methods appear in detail in Title 40, Code ofFederal Regulations (CFR), Part 60, Appendix A.


### The Sampling Apparatus is shown in Figure 1 on Page 6. All equipment was calibrated at Comprehensive Emission Services' office prior to shipment to the test site. SampliRg Locations A total of 12 sample points were used to determine particulate emissions. The sample time perpoint was 7.5 minutes, for a total sampling time of90 minutes per test run. The stack sampling point locations can be found along with the field data sheets inAppendix 

### C. Analytical Procedures The particulate emissionrate was determined following procedures detailed in EPA Methods 17 and 202. Particulate samples collected onWhatman glass fiber filters were analyzed gravimetrically. Theprobe and nozzles were rinsed with acetone. The rinse was transferred to tared beakers and evaporated to dryness. The back

## -halfwater was collected and separatedjnto organic and in-organic parts. The samples were then transferred to tared beakers and evaporated to dryness
..

5

,**,~** :/ ....--..

. Stack In-stack

### ~ Exit Temp



### Thermocouple 

# "**~I**

# Fi~lta~r~~~~~~s~am~PI~e~p~ro~b~e~=~~=~~~~) Probe Nozzle SType Pitot Tul;le



### Ice Bath .' Sample Line

Thermocouples Fine Vacuum 

# .0 Adjust



### . Gauge Orifice


### Dry Gas 

## Meter Leak Free 

### Pump 

## Schematic of Method 17 Sampling Train Figure 1

### Table 2 ParticulateEmission Results lWo Soybean Storage Bins (EP 

### 101) Parameters Units Run 1 Run 2 PM Emissions Weight Collected g 

### <0.0100 <0.0100 Actual gr/dscf <0.0024 <0.0024 Emission Rate lb/hr <0.021 <0.021 Stack FlowRates Velocity ftlmin 4,849 4,821

Actual acfin 952 947 Standard Conditions dscfin 1,005 991 Sampling Results Isokinetics % 

### 99.2 99.5 Sample Volume dscf 64.023 63.296 Ave. Stack Temperature 

## of 33 36

Ave. Square Root AP inches 

### H20 1.2545 1.2430 Ave. LlH inches 

### H20 1.61 1.61 Ave. Meter Temperature of 72.3 74.2 Oxygen % 

### 21.00 21..00 Carbon Dioxide % 

### '0.00 0.00 Moisture Collected ml 1.0 '·5.0 Moisture % 

### H20 0.1 0.4 Run Start Time 

## HH:MM 9:32
. 12:08 Run Stop Time 

### HH:MM 11:38 13:41 Sampling Time minutes 90 90

Date orfest mmlddlyr 

### 01124/07 01124/07 Opacity 

### % 0.0 0.0 Run Start Time 

### HH:MM 9:41 12:22 Run Stop Time 

## HH:MM 10:41 13:22 Sampling Time minutes 60 60

Date ofTest mmlddlyr 

### 01/24/07 01/24/07 Run 3 <0.0100 <0.0025 <0.021 4,827

948 978 -'.'**~**



### 99.8 62.669

41 1.2375

1.58 73.6 21.00 0.00 10.0 0.7 14:09 15:40

90 

### 01'/24/07 0.0 14:19 15:19

60 01124107

7

# Appendix A Example Calculations

\.

.

### Symbol 

### Qa As 

## Bws Cp Cstd 

## Dn dscfm g 

### gr/dscfin ID 

## Md Ms Qstd 

### Pb 

### Ps SP 

## Tm Ts ·Vi

Vf Vm Vmstd Vs 

### We Wtgain 

### y 

### 8 % 

### H20 % C02 %02 

### %I**~H ~p**  

## NOMENCLATURE . Description Actual cubic feet per minute Area ofstack Percent water Pitot tube calibration coefficient Concetration ofparticulate dry basis, standard conditions Diameter ofnozzle Dry standard cubic feet perminute Grams Grains per 

### dry standard cubic feet per minute
. Inside diameter ofstack Molecular weight, dry stack gas Molecular weight, stack gas Stack flow rate, dry standard conditions Barometric Pressure Stack pressure Static pressure Average meter temperature Temperature ofstack gas Initial meter reading Final meter reading Volume meter, actual Volume meter, standard conditions Average stack gas velocity Total moisture collected Total particulate matter collected Meter condition factor Sampling time Percent moisture by volume Percent carbon dioxide by volume, dry I 

### \­ 

### Percent oxygen by volume, dry 

## i Percent isokinetic Pressure drop across orifice meter Gas.velocity pressure

### PARTICULATE CALCULATION EQUATIONS 

### Run! 1. Volume of meter



## V,1l = 

### (511.636 -446.700)x 1.004

2. Volume of meter, standard conditions (68° ,29.92 in.Hg)**~"** 

### +460 17.65X65.l96X(29.50+ 1.61) 

### V
_ 13.6 m(s/d)

- 

### 72.3 + 460

3. Percent moisture by 

### volume 100 x 0.4707 x



### B 

# = 100 x 

### 0.4707 x 1.0

1VS 

### 0.04707 

### x + 64.023

4. Molecular weight, dry 

### stack gas Md 0.16 X 

### %C02 

### +0.04X%02 +28.0**M~** 

# = O.l6x 0.00+0.04x 21.00+28.0 Mti =28.84 

## .\

### 5. Molecular weight, stack g

-- • ..., >"_ •••• 

## Ms == 

### 28.84x

# (1- 0.1) 

## + 18

# X(l- 0.1 

# 1 100 lOa} M. I. ;::::: 

### 28.83 

### 6. Stack Pressure 

## .P. p. 

## + SP

u b 

### 13.6
P 

# = 29.50 

### + 0.00

.f 

### 13.6 

## P.v = 

### 29.50 inch. Hg 7. VeloCity of stack gas


### V." = 

### 60x 85.49x 

### C x 

### Ts 

## + 460 

# x( tt;;;) p 

## . P x

## M :oJ up o'l'g s .r 

## I . V, 

# = 60 x 85.49 x 0.99 x 

## J 33 

## + 460 

### x 1.2545



### . V29:50x28.83 

### V" 

## = 4,849 ftlmin 

### 8. Percent isokinetic 100 x 

### (Ts 

## + 460)x V,lI(.,Jd) 

### %1 

# =

____---.::..-::...._-..:...._='L-
__ 

### 17.65x

# ex V. x

# Px

# (1- Bw.r)x7fx(Dn)2 s


### . 100 24

100 x 

### (33 

## + 460)x 64.023 

### %1 

# =**------~--..!..-------** 

### 17.65 x 90 x 4,849 x 29.50 x

# (1**~~~** 

# )xn:x(**0.~:O)2** %1 99.2

### 9. Area of stack 

# (ID).2 :TCX

­

### 24
6.00J2 

### A 

# = rex -­

.1' 

### ( 24



## to. Stack volumetric flow rate actual conditions Qa 

### =VxA ,0; S 

## Q 4,849X0.20

a 

### Qa 952 acfm 

### 11. Stack volumetric flowrate, standard conditions (68",29.92 in.Hg)
17.65x 

### V, x

# A, xP.

# X('l- Bw.,) • ,. 100 QSld = 

### ----T- 

### -+-4-6-0-"::"---=­ s 

### 17.65X4,849XO.20X29.50X(1- 0.1) ",' 1 00 Q"ld = 

### ------33-+-4-60---"-----1:­

o."ld 

# = 1,005 dscfm 12. Grains per 

### d.t.] sta.'1dard cubic feet 

### 15.43 x Wtgain Vm(sld) 

### 15.43 x 0.0038 C,\'/d 

### 64.023

:::: 0 .0009 gr/dscf 

## ,C s1d

### 13. 

### Emission rate Ib 60 x Wt g• in 

### x 

### QSld 

## = hr 453.5924x Vm(std) 

### Ib 60 x 0.0038 x 1,005 

## = hr 453.5924x 64.023 

### lb 

## = O.0081b/hr 

## hr



## l,
..

# AppendixB Laboratory Data Forms

### Project Number: ::r-.

### ---=.4..,;:..0....;:7-

__-:---;-__ 

### PlantName: Car;) 

### tl{ 

### 'lJe..s 1­



### . Date:
. 

## /-.9.5**~o** 

## tAnalysis 

### Type: ----I/-'?-:..,.;/:....;2;;..0-=2.

_____ 

## f' 10 

## I Run 1 Type Identification Final Tare Net Number Weight Weight Weight Filter 

# p**/1~** 

### J 

# ;..&01**~** c;l. 

# ·t,ort(; .(}OoJ Probe Rinse ( ml) 

# B LII> Z 

# to 'J. IS"::(,) , '6. IS

# S.'-/

..

## DOI~ Front 

### HalfWeight 

# ,OOlll Organic ( nil) 

# e.. ti7l/J 

# to, .V¥b l 

# /0 {g. fJt{S 

## l 

## • oot\) Inorganic. 

## P**L//~·7** IJD.1

# h 

# lf;;.**130.~l.o31-** . ohiO TotalNetWeight

### /},OO3~ R'Iln2 Type Identification Final Tare Net Number Weight Weight Weight Filter 

# p /1& 

# z. 

# J<. 

# 'o8Lj**~.** 

# &DBLf**~** f}O(J 

### iJ Probe Rinse ( nil) 

## B 

# l/1:J3 

# 7

# «. 0-:). "t' 

# 1S. o-=t-tJJl{**~** 

## oat) Front HalfWeight 

# .00/ 3 Organic ( nil) 

# <: (.jJ'/t/ !OI.'1Jc,,;). 

# I 0 

# I.

# 43.L}'1 •. 00(1 Inorganic 

# p '-111-0 

# l:t'/. 1J**~tl** 

# 1'1- to .32;JG:, ,,( 0 

# ).:2­ Total Net Weight 

# 0,00'1$ Run 3 Type Identifica.tion 

# r:· Final Tare Net Number Weight Weight Weight Filter 

# p 1'"1-&3 

# 2. {,:J-1J 

# J. &>;)10 " (JOO5 

### Probe Rinse ( nil) 

# B . L/ f 

## '3 

## </**7-~.** 

## l-1-YO 

# t to. 

# r=r**~** 

## lb' _.0 

### oj?... Front

### HalfWeight

## ~ 

# OOfS" Organic ( ml) 

### (, L/1t{S 

# 10;1,/100**I.01.·/~94 ~ooe"**  Inorganic 

# D 

# '-Ir+ ( /3'1. 1./1 t). 

# 131-. 43ytf 001] Total NetWeight


# . (), OOJCf

Identification F= 3 inch filter P 47mmfilter B ";' 150m! Beaker C 250ml Beaker . D = 

### 400ml Beaker- 

# - - 

# - - 

## - 

# -- - 

# FINAL WEIGHT WEIGHING SHEET 

# Ej> /0 I Time 

### Date Analyst 

### IDNo.



## I..!IJ'- LIt») 

# I,/(JV t- l.fj 

## Lj

## J VI.( 

## J,Jt

# l5 l//I,p**~** 

### 1-)1 

## TO



# - l-/Irl

Check Weight Check Weight Check Weight 

### Run 

### 1 Weighing (grams) 234 

### 5 

### Average 

### Final Weight

### ~C 

# =E-=== -'- 

# S- ­ Tare 

### Weight Net Weight



### COMPREHENSIVE EMISSION SERVICES

## TARE WEIGHT WEIGHING SHEET
Time I 

# S**~3D** 

### Date

### I~· 1\·6Cn

### 18-18-~ Analyst 

## II \'\ I 

# /11. Weighing (grams) ID No. 

### . 1 ··2 

### 3 

## '2.<'0 tJ38**L,~**



## 'Z.**.4>'Z?.~ '1.-.~**  

## 18e ). (q 

## ZS:7**.~** 

## 27L.l cftJ 

## 2'23**.(C~(** 

# 5

Check Weight. O.;:>S 

# 1.. I :;). J,..:;> 

## 5"'1. 4 

### 5



# C CoMPREHENSIVE

....' 

# =- E EMISSION 

# S SERVICES

# TARE WEIGHT 

# WEIGHING SHEET
Time 

### I



## . !S6 

# 7**~**

# tz. . Date 

# . 11--1**:-()~ Il~**  

## 8"Of:; Analyst 

# /J1.A I/;tfl -,:­ Weighing (grams) 

### ID No. 

## l

# I' I 1 2 

### 3 4 

### 5

Check Weight 

# 1wO. O 

## /2.

# ~ C COMPREHENSIVE 

# . E . EMISSION 

# S SERVICES........--. 

## TARE WEIGHT 

# WEIGHING SHEET
Time 

### Date Analyst 

### IDNo. 1

Check Weight 

### Weighing (grams) 2 3 

### 4 

### 5 

### Average



### {DO. 

# 57-V; "Z­ 

## /01.

CoMPREHENSIVE 

### EMISSION SERVICES**~.~~** ...,••,.,_..__ __ '

____•

__•

___.............._________.._ .. "w_._.
__..___......

# ~**~** 

# a rI) 

## ff3 

# §**~ ~**  ?11

## ~

# ~rT~C/j**c.S~**

# IIIIIII~I~

# ~IIIIIIIIIIIII

# Appendix C Field Data FormsRun No. 1, assumed 10mg Location: Cargill West (EP 101) Date: Jan.24,2007

.Project

### # 407 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight:::

Vet Molecular Weight= Sampling Time (Minutes):::: Nozzle Diameter(lnches)= stack Round or Square= Stack Dimention A (Inches)=
.**St';c~ck** Dimention 8 (lnches)= Equivilent Diameter (inches)= Stack Area (Square Feet) = Pitot Coefficient:::: Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)=

. Flow Rate (Actual, Cubic ftimin)=

Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg 

### (grlscf)= Emission Rate (lbihr)= Particulate Loading - Total Catch Including Impingers "'articulate Weight Net (g)= ,-'articulate Loading, Dry Std. 68 Deg (grJscf)= Emission Rate (Iblhr)= Percent lmpinger Catch= 99.2 

### 446.700 511.636 1.004 0.005 

### 65.196 64.023

29.50

0.00 29.50 21.00



### 0.00

1.0 0.1 72.3 

### 1.61 1.5833 33 

### 28.84 28.83

90.0 

### 0.160 Round

## 6.no. 

## 6.06:. 6.n 0.20 0.99 

### 1.2545 4,849



### 952 1,005

0.0018 0.0004

0.004



### 0.0100 0.0024



### 0.021 82.00Run No. 

### 1 Location: Cargill West (EP 101) Date: Jan. 24,2007 Project 

### # 407 

### % Isokinetic= initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen 

# = Percent Carbon Diqxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)::; Average Stack Temp (F)= Dry Molecular Weight= Vet Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square:::: Stack Dimention A (Inches)= Stack Dimention B (Inches): Equivilent Diameter (inches): Stack Area (Square Feet) 

### = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68Deg (grlscf)=

. Emission Rate (Iblhr)=

Particulate Loading - Total Catch Including Impingers 'articulate Weight Net (g)= rlarticulate Loading, 

### Dry std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Percent Impinger Catch= 99.2 446.700 511.636 1.004 0.005 65.196 64.023

29.50

0.00 29.50 21.00'

0.00

1.0 0.1 72.3 1.61 1.5833 33 

### 28.84 28.83

90.0 0.160 Round6.00 .'..... 6.00 

### 6.77 020 0.99 1.2545

4,849

952 1,005

0.0018 0.0004

0.004

0.0038 0.0009

0.008 52.63Run No. 2, assumed 10mg Location: Cargill West (EP 101) Date: Jan,24,2007 Project 

### # 407 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Oeg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)::: Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide::: Moisture Collected(ml)= Percent Water::: Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average stack Temp (F)= Dry Molecular Weight= Vet Molecular Weight= Sampling Time (Minutes)= Nozzle Oiameter(lnches)= Stack Round or Square= stack Dimention A (Inches)= Stack Dimention B (Inches)= Equivilent Diameter (inches)= Stack Area (Square Feet) = Pitot Coefficient:
. Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)=

. Flow Rate (Actual, Cubic ftlmin)=

Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Oeg (grlscf)= Emission Rate-(Ib/hr)=
. Particulate Loading - Total Catch Including Impingers [ "'articulate Weight Net (g)= " -·,"Particulate Loading, Ory Std. 68 Oeg (grlscf)= Emission Rate (Iblhr)= Percent Impinger Catch=

### Run No. 2 Location: Cargill West (EP 101) Date: Jan.24,2007 .oroject# 407



### % Isokinetic= 99.5 Initial Meter Volume (Cubic Feet)= 512.000 Final Meter Volume (Cubic Feet)= 576.435 Meter Factor= 1.004 Final Leak Rate (cu Ftlmin)= 0.004 Net meter Volume (Cubic Feet)= 64.693 Gas Volume (Dry Std Cubic Feet 68 Deg)= 63.296 Barometric Pressure (in Hg) = 29.50 Static Pressure (Inches H20)= 0.00 Stack Pressure (in Hg)= 29.50 Percent Oxygen 

### = 21.00 Percent Carbon Dioxide= 0.00 Moisture Collected(ml)= 5.0 Percent Water= 0.4 Average Meter Temperature (F)= 74.2 Average Delta H ( in H20)= 1.61 Average Delta P (inches H20)= 1.5742 Average Stack Temp (F)= 36 Dry Molecular Weight= 28.84



### Vet Molecular Weight= 28.80 Sampling Time (Minutes)::= 90.0 Nozzle Diameter(lnches)= 0.160 Stack Round or Square= Round Stack Dimention A (Inches)= 6.00 Stack Dimention B (lm:;hes)= 6.00 Equivilent Diameter (inches)= 6.77 Stack Area (Square Feet) = 0.20 Pitot Coefficient::: 0.99 Average Square Root of Delta P (inches H20)= 1.2430 Stack Velocity (Actual, ftlmin)= 4,821 FIO\AI Rate (Actual, Cubic ftImin)= 947 FIO\AI Rate (Std, Dry, Cubic ftlmin 68 Deg)= 991 Particulate Loading - Front Half Particulate Weight Net (g)= 0.0013 Paticulate Loading, Dry Std. 68 Deg (grlsc1)= 0.0003 Emission Rate (Ib/hr)= 0.003 Particulate Loading - Total. Catch Including Impingers "larticulate Weight Net (g)= 0.0048 ·rlarticulate Loading, Dry Std. 68 Deg (grlscf)= 0.0012

..':: 

### Emission Rate (Ib/hr)= 0.010 Percent Impinger Catch= 72.92

### Run No. 3, assumed 10mg Location: Cargill West (EP101) Date: Jan. 24,2007 Project 

### # 407 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen ::: Percent Carbon Dioxide::: Moisture Collected(ml)= Percent Water- Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight: Vet MolecularWeight= Sampling Time (Minutes)::: Nozzle Diameter(lnches)= Stack Round or Square::: Stack Dimention A (Inches)= Stack Dimention 

### B (inches)= Equivilent Diameter (rnches)= Stack Area (Square Feet)::: Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Fiow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= PartiCUlate Loading - Front Half Particulate Weight Net (9)= Paticulate Loading, Dry Std. 68 Oeg (gr/scf)= Emission Rate (Iblhr)= Particulate Loading - Total Catch Including Impingers 'Jarticulate Weight Net (g)= c'articulate Loading, Dry Std. 68 Deg (gr/scf)= Emission Rate (Iblhr)= Percent lmpinger Catch= 99.8 576.900 640.627 1.004 0.007 63.982 62.669

29.50

0.00 29.50 21.00

0.00 10.0

0.7 73.6 1.58 1.5625 41 28.84 28.76

90.0 0.160 Round6.00 6.00 '. 

### 6.77 0.20 0.99 1.2375

4,827



### 948 978

0.0015 0.0004

0.003

0.0100 0.0025

0.021 85.00Run No. 

### 3 Location: Cargill West (EP 101) Date: Jan. 24, 2007 Project 

### # 407 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)::: Meter Factor=
. Final Leak Rate (cu FtJmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) 

### = Static Pressure (InGhes H20);::: Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature 

### (F)= Average 

### Delta 

### H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= Vet Molecular Weight: Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square= Stack Dimention 

### Po (lnches)= Stack Dimention r.1:·(lnches)= Equivilent Diameter (inches)= Stack Area (Square Feet) ::: Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= 

### Flow Rate (Actual, Cubic fUmin)= Flow Rate (Std, Dry, Cubic ft/min 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 

### 68 Deg (grlscf)= Emission Rate (Iblhr)= Particulate Loading - Total Catch Including Impingers "?articulate Weight Net (g)= \ ..•jarticulate Loading, Dry 

### Std: 68 Deg (grlscf)=

. Emission Rate 

### (lb/hr)=
.

Percent lmpinger Catch= 99.8 576.900 640.627 1.004 0.007 63.982 62.669

29.50

0.00 29.50 21.00

0.00 10.0

0.7 73.6 1.58 1.5625 41 28.84 28.76

90.0 0.160 Round6.00

.. ., 6.00' 6.7.7 0.20 0,99 1.2375 4,827



### 948 978

0.0015 0.0004

0.003

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. Note&:Total Number of POints(B, 12, 16,20,24)= 12 

### EP 101 Stack Diameter or LengthOnches)= 6 Round Square 'oint Distance 

### 1 0.3 1 0.3 2 0.9 

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### 1.8 

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### 2.B 7 

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### 10 

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### 5.3 12 5.8 If stack diameter is less than 24 inches each. point must be greater than 0.5 inches from wall if stack diameter is greater than 24 inches each point must be greater than 1.0 inches from wall



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14 15 

### (J 16 

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# \J 17 

### 19 

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22 

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. 

# AppendixD Pretest CalibrationsMeter Calibration Operator

3.te Meter Number Previous 

### Y Factor

Meter Volume Final Initial

Net Meter Temperature Inlet Initial Final Outlet Initial 'Final 

### Avg. MeterTemp Time

.**~eter** DE;llta 

### H Jarometric Pressure Room Temperature Initial Final Avg.ROMl T!3mperature Pump Vacuum Vcr (std) Vm (std) 

### Y Factor (brackets) Delta H@ +/- 2% Criteria , Bracketing Percent of

### Y Average 

### Y Factor Average Delta H@ D.L ORIFICES: Jan. 10,2007 Orifice No. 1 Low 

### 15 K Factor 0.4146 4 Orifice No.2 Mid 20 1.007 

### K Factor 0.5311 Orifice No. 3 High 23 

### K Factor**0~6181** ORIFICE 1 Low ORIFICE 2 Mid ORIFICE 3 High Cubic Feet 295.123 300.651 306.249, Cubic Feet 289.800 295.200 300.700 Cubic Feet 5.323 5.451 5.549 

### *" must be greater than5 cubic feet Deg. F , 58.0 ' 60.0 61.0 Deg.F 60.0 61.0 62.0 Oeg.F 58.0 59.0 60.0 Deg.F 59.0 60.0 61.0 Deg.F 58.8 60.0 61.0

sec 600.0 480.0 420.0 inches H2O 0.87 1.50 2.00 inches Hg 29.18 29.18 29.18

Deg.F 59.0 59.0 60.0 Deg.F 59.0 60.0 60.0 Deg.F 59.0 ".- 59.5 60.0 'inches 

### Hg 20 18 

### 17 dscf 5.310 5.439 5.537 dscf 5.293 5.416 5.510 1.003 1.004 1.005 1.732 1.822 1.794
0.09 0.07 PASS PASS 

### 1.004 Must be between 0.98 and 1.02 

### 1.783

# - - - -


## - 

# - METER CALIBRATION WORK SHEET Operator:

# ...:b~, 

# L_,-'--

___ 

# y Meter I.D,**~~** 

### ___ ___ 

# I ­ \ o ....

# bl Date: -!...----!.I-----­ 

### K Factor No.1 

### .....;If.'--Y--!....IL-Yu(o:::.--

___ Previous 

## Y Factor 

## J # 

# r.;o

# 1 K Factor No.2 ---IL.1...:::5'::....:3::::;..·..!..!.11

____ 

### Leak Check 

### K Factor NO.3 _"

### _Lu_._\..:::..8....:..\-,..

___
METER VOLUME Units Final 

### ft3 Initial 

### ft3 Meter Temperature 

### INLET Initial OF Final 

### of OUTLET Initial· 

### of Final 

### of Time sec .:.c Meter LlH in.Hp Barometric Pressure in. Hg Room Temperature Initial' 

## OF Final 

## OF Pump Vacuum in. Hg 1 Low 2Mid, , . 3 High

## ;:zq5~**i~3** 

## -=< 01) 

# fo5"/ "} OC:" ';2tt 

# q**2~q.** 

# Bto ;z..o,S- :leO 

## 300.7(fiJ**5~**

## ~O 

# (,., I (gD 

# Col (0:2 

# S'2S'**,~9** 

### (L7D 

# S1 . Coo , tol '00 

# '-180 420**~87** 

# ' ItS 2..0 

## :2**~t** 

# I/J ;l-l), 

## I 

# 1< 

# -:;1. 

# /g

SCf 

# S-q ·7nO 

# SCJ {PO**~O** 

# :2fJ 

# if: 17


# :..c·=

- .- COMPREHENSIVE 

# E= EMISSION



# -- 

# S -
- SERVICES ."**.~.:**

### ( 

# AppendixE Post-test CalibrationsMeter Calibration Operator T.O ORIFICES: 'ate Jan. 25,2007 

### Orifice No. 1 Low 15 K Factor 0.4146 Meter Number 4 Orifice No.2 Mid 20 ' Previous Y Factor 1,004 K Factor 0.5311 Orifice NO.3 High 23 K Factor 

### 0.6181
ORIFICE 1 Low ORIFICE 2 Mid ORIFICE 3 High Meter Volume Final Cubic Feet 646.346 652.003 657.693 Initial Cubic Feet 641.000 646.500 652.100

Net Cubic Feet 5.346 ' 5.503 5.593 * must be greater than 5 cubic feet

," 'Meter Temperature Inlet Initial Oeg.F 60.0 62.0 62.0 Final Deg.F 61.0 62.0 63.0 Outlet " Initial Deg.F 60.0 62.0 62.0 Final Deg.F 61.0 62.0 63.0 ' Avg. Meter Temp Deg.F 60.5 ' 62.0 62.5 Time sec 600.0 480.0 420.0**I\~eter** Delta H inches H2O 0.86 1.50 2.00

arometric Pressure inches Hg 29.30 29.30 29.30 Room Temperature Initial' Deg.F 60.0 61.0 61.0 Final Deg.F 61.0 62.0 62.0 A,vg.Room Temoerature Deg.F 60.5 61}3 61.5 Pump Vacuum, inches Hg 20 18 17 Vcr (std) dscf 5.325 5.451 5.551 Vm (std) dscf 5.320 5.469 5.560 Y Factor (brackets) 1.001 0.997 0,998 Delta H@ 1.695 1.787 1.764 +/- 2% Criteria Bracketing Percentof Y 0.22 0.03 , PASS 'PASS Average Y Factor 

### 0.999 Must be between 0.98 and 1.02 Average Delta H@ 1.749

# METER CALIBRATION WORK SHEET

# operato~C

# n Meter 1.0.

____ 

### Ll--..I·t.....-

__..,.--_ Date: ,)6\t). 

# ?S ?(JO 7 K Factor No. 1

# _",_L-,-IJ_~....:...~

# ____ Previous Y 

### Factor. 

# J. DOl/ K 

### Factor No.2

__ .. 

## _>:_3_1...;..' )

____ K Factor NQ. 3 

# _#_cP......:·

# 1_8_1

____ Leak Check
METER**VOLU~E** Units 1 Low .2Mid 

### 3High Final 

### ff 

### (pl/{P 

# 13 

# 'Ito iPS'2, ()C?3

## 6SZ~/t3 Initial 

### ff 

# u,1/L(}()6 (0 

## llto.SoD 

## 4>.5 Z ,J66 Meter Temperature INLET Initial of 

### (;Pb 

## &7 (;:,2 Final of 

## 6.'1 

# I 

# &2­**~3** OUTlET Initial of 

## (PC) 

# &.-z 

# CRZ Final of 

# (PI cPZ 

# (/3 Time sec 

### 1#00 

# lf8b CfZ6 Meter 

### aH in. 

### H2O .... Ii 

# tJ(p /
.. t;o 2.00 I Barometric Pressure in. 

### Hg

### ~tff36 

## 1Jt;,3rf 

## ct24,50 Room Temperature Initial of 

### (po 

## &f 

# &1 Final 

### of 

## (PI uf2 

# &'2 Pump Vacuum 

### in. Hg 

# dO /8 II

COMPREHENSIVE EMISSION SERVICESi . 

# Appendix F Process DataLYNX Load, wllload Detail Cedar Rapids West Facility: Cedar Rapids West, GOS Truck unload Net Wgt Wgt Cert / Customer /

Date Trace Id SOL Grade C/P Unit Id In Pounds Quantity Til M DKT FM SHBN DEF OKG BCFM PROT For Account; of

SELECTION CRITBRlA: Facilities, Cedar Rapids West, GOS Services: load; Unload Modes, Truck; Rail; Barge; Vessel Weights Affeoting Inventory: 01/24/07 07:00,00 AM
. 01/24/07 03;45,00 PM Commodity I Product Types. + All • Commodi ty I Products, YSB CustOll\ers. • All •**~** 01/24/ 30040466 310549 llSll1 'IS :>543 -1 54,900 915.00 au 57.5 11.1 0.3 0.90 Tame Benton Cooperative**~** 8:05 AM SPL. I 01/24/07 Jl004 0467 310550 l1SII1YS un -2 58,320 972.00 BU .58.0 9.S 0.4 0,70 Innovative Ag Services ,1 8: 12 AM rJ.i**SPL~**
., 01/24/07**~'a004046a** noss] USIIlYS 5443 ·3 57,780 963.00 

### au 57,0 10.0 0.4 0,70 Northeast Iowa Coop**~.** 

### . 

# I**~.** e,17 AM SPLoo 1:: 01/24/07 930040469 310552 l1S111'i'S 1376 ·4 52,8:10 880,33 

### au 56:0 11.8 0.5 0.90 Innovative Ag services 8:23 AM SPLa 01/24/07 830040470 310553 USH2'lS 9282 -5 54,320 ))05.33 au 57.5 a:2 0.5 1.40 Marengo Elevator Company

8:251 AM SPL. 01/24/07 830040471 310554 USIIlYS 9759 ·6' 53,560 892,67 

### au 51.0 11.5 0.5 0.90 Northeast Iowa COop 8,35 AM SI'Ld 01/24/07 830040472 n05s5 USIHYS a837 ·7 53,860**a97,~7** 5U 57.5 12,8 0.5 3.60 waukon Feed Ranch Inc 8:47 AM Sl'L01/24/07 830040473 310556 USfllYS 3524 

### -a 53,180 aS6.33 SU 56.5 11,6 0.6 0.60 Northeast Iowa Coop

8,51 AM BPI.. 01/24/07 830040474 310557 USfl1YS 570 ·9 57,580 95,9.67 BU 57.0 11.4 0.4 1..00 Stoner Grain, Inc. 8.57 AM**SPL~** 01/24/07 830040475 310558 USII1YS 422 ·10 60',460 l,G07.G7 Bl1 56.5 11.3 0.8 0.510 Stoner**Grain~** Inc, lha3 AM SPI.­**01/2~/07'B3004047G** 310559 US#lYS 0120 -11 51,500 BS8.33 

### au 57.0 11.3 0.6 

### o.ao Northeast Iowa Coop 9:06 AM Sl'L= 01/24/07 830040477 310560 US!l2YS 1378 -12 53,760 a96.33 

### au 56.5 10,8 0,5 1,40 Tama Benton Cooperative**~,13** AM SPLm 01/24/07 830040478 110561 USil1YS 14'02 ·13 53,040 884.00 

### au 56.5 11.6 0.8 O.BO Keystone Mercantile Co.

9:20 AM SPlP 01/24/07 830040479 310562 1JSUUS lUI ·H**~:"** 340 922.33 

### au 57.5 10.3 0.7 3.20 West Side Grain 

# r: 9:25 AM SPr.­ 1/24/07 830040480 310563 USIIlY'S 9803 -15 58,140 969.00 SU 56.5 10.2 0.4 0,80 Tama Benton Cooperative 9:37 AM SPL01/24/01 830040482 310564 l1Sft2YS san -17 54,040 900.67 BU 56,5 10.4 0.5 1.90 Tams Benton Cooperative

!h42 AM SPL= 01/24/07 830040481 310565 USillYS 5ao ·16 53,640 894.00 EU 57,S 10.2 0.4 0.60 Interstate Grain Service 

# fl.",,,
!h4? AM SPL=



## 1 .01/24/07 830040483 310566 USIIlYS 1403 ·18 53,080 884,1>7 BU 57.0 11.8 0.9 0.80 Keystone Mercantile Co. 01/24/07 3:52 PM /opt/uxapps/batch/ob1oaunl.sqr ?ageLYNX

- Load/unload Detail Cedar RapidS West Facility: cedar Rapids West, GOB huck UnlQad Net wgt Wgt Cert / Customer 1

Date Trace Id ElOL· Grade C/P Unit 1d In Pounde Quantity TIl M DKT I'M SHill" OSF OKG !lCl?M PROT FC:>T ACcount of 10,04 AM**BP~** .-01/24/07 630040484 310567 l)S1I2YS 1340 -19 55,560 926.00 IlU 55.5 10.9 \.2 0.80 KeYStone**Mercan~ile** Co.

,. 10:09 AM**SPL~** 

### troU 01/24/07 830040465 310568 USIilYS 2462 -20 54,320 905.33 Bl) 57.0 10.4 0.6 0.&0 Tama Benton Cooperative

.... 11-10: 15 AM**SPL~** 01/24/07 830040486 310569 UBIIlYS 174 -21 55,200 920.00 au 56.0 10.7 0.6 1.00 Glandorf, Daniel 10,20 AM SPL= 01/24/07 830040487 310570 USll2YS 9282 -22 53,160 886.00 

### au 58.0 9.1 0.6 1.S0 Marengo Blevator Company 10;26 AM SPL. 01/24/07 830040488 310571 USlIlYS 9909 -23 51,540 S59.00 BU 57.0 10.2 0.4 0.90 Norcheast Iowa Coop 10:31 AM**S~=** 01/24/07 830040489 310572 US1l2YS 8562 -24 57,020 950.33 BU 56.5 10.9 0.6 1.30 Ryan Cooperative

# ~u.t\! 10:36 AM**SPL~** 01/24/07 830040490 :nOS73 USII2.YS 13%

- 25 :.54,940 915.67 BU 58.5 10.9 0.5 1.80 Northeast Iowa Coop 

# l 10:41 AM SPL= 01/24/07 830040491 310574 USlI3YS 1315 -26 51,060 951.00 

### au 57.0 10.0 0.4 2.50 Tama Benton Cooperative lO:46 AM SPL= 

# J.

11 01/24/07 830040492 310575 US1I3YS 9759 -27 54,300 905.00 BU 5S.5 10.7 0.6 2.20 Northeast Iowa Coop 

# 4' 10:52 AM SPL= 01/24/07 630040493 310576 USII2YS 0692 -28 54,660 911.00 BU 58.0 9.4 O.S 1.60 Tams Benton Cooperative 10:58 AM SPLv "? 

### 1,..'1 01/24/07 530040494 310577 USillYS 7763 -29 )
.. '"f 920 965.33 SU 56.5 10.9 0.5 0.80 Tama Benton cooperative



## ... 11:02 AM SPL= 01/24/07 830040495 nOS7S USII1YS 1065 -30 57,400 956.67 BU 57.0 10.1 0.5 0.50 Northeast Iowa Coop 11:09 AM SPL01/24/07 830040496**31057~** USlI2YS 2064 -31 53,660 894.33 BU 56.0 10.7 0.6 1.BO Ryan Cooperative 11;13 AM**S~u** 01/24/07 830040497 nosao USIIIYS 2298 -32 53,640 894.00 IlU 57.0 8.7 O.S O.BO Marengo Elevator Company 11:19 AM SPL= 01/24/07 820040498 310581 USlln:S 4556 -33 55,S80 931.33 BU 56.5 10.1 0.6 0.70 Innovative Ag Services ll:25 AM SPL= 01/24/07 830040499 3105B2 US#2YS 1214 -34 55,220 920.33 SU 57.5 10.7 0.6 1.40 Ryan Cooperative 11,30 AM SPLm 01/24/07 830040500 310583 usltllCS 9356 -35 58,800 980.00 IlU 58.0 10.1 0.5 0_70 Innovative Ag Services 11:36 AM**S~"** .-ol/U/07 830040501 310584 USlt1YS 4399 -36 57.620 960.33 BU 57.5 9.7 0.4 0.90 Edgewood Feed Mill lnc 11:41 AM SPLw 01/24/07 830066002 31(}585 US#1YS 012(}

- 37 50,260 837.67 

### eu 58.0 10.4 0.4 0.80 Northeast Iowa COop 11:46 AM SPL01/24/07 830086003 310586 USillYS 8580 -38 54.**~40** 915.G7 SU 57.S 9.6 0.8 0.90 VanDaele, Rick & Linda 11:51 AM**SI?L~** 01/24/07 830066004 310S87 USlilYS 1257 -3S1 52,960 662.67 BO 57.5 11.0 0.4 0.70 Innovative Ag" Services 11:56 AM SPL= 01/24/07 830086005 310588 USUl'lS 9577 ·40 54,2QO**90~.OO** BU 57.0 9.6 G.Q 0.70 Linn Coop Oil-Alburnett 

# r

12: 04 PM**S~.** Ol/24/07 830086006 310589 USli1YS 570 ·41 57.200 953.33 BU 57.0 11.5 0.5 1. 00 Stoner Grain, Inc. 

## o Vl 01/24/07 3: 52 PM /opt/uxapps/batch!Obloaunl.sqr page 2 

### r-U
.

# ~LYNX

- Loau/un1oad Detail**Ceda~** Rapids Nest Facility, Ceaar Rapids West, GaS Truck Unload Net W9t Wgt cext: / Customer /

Date Trace Id eOL Grade e/p unit Id In Pounds Quantity Til M DKT FM SHBN DEF DKG BCFM PROT For Account of 1;<,09 PM 6P1.= 01/24/07 830Q66007 310590 USlIl;':8 6685**-4~** 53,360**8B~.33** SO' 57.5 11.0 0.4 0..70. 1.1no Coop Oil Co

- Marion 12,H PM BPLu 01/24/07 830086008 310591 USlllYS 1552 -43 58,220 970.33 au 57.5 10.2 0.6 1.00 Innovative 1<g Servicea 12,;<0 PM SPI.­ 01/24/07 B30086009 310592 USII2YS 1246 -44 1'.3,500 891.67 eu 57.0 11.0. 0.7 1.40. Innovative Ag Services 12:24 PM SPI,.. 01/24/07 830066010 310593 U8#2Y8 1340 -45 55,440 924.00. 

### au 55.5 10.6 0.6 1.30 Keystone Mercantile Co. 12,29 PM Spr,.. 01/24/07 830086011 ·310594 USIi:U'S 9803 -46 56,360 939.33 au .57.0 10..5 0..4 0..70. Tama Senton**Coope~ative** 12:35 PM SPI.­ 01/24/07 830086012 310595 US#1YS 1605 -47 51,560 959.33 

### au 56.S 11.1 0..6 0..90. Innovative 1<9 Services 12:42 PM SilL01/24/07 830086013 310596 UBUyS 0120 -48 55,260 921.0.0 au 57.5 9.3 0.5 0.80 VanDaele, Rick & Linda 12:47 11M SIII.-

## RIj~ 01/24/07 830086014 310597 USlI2YS 6112 -49 51,260 B54.33 au 57.5 9.2 0..5 1.60 Devick Enterprises 

# } 12:52 PM SPL01/24/07 830086015 310598 UBII lYS 5834 -50 55,660 927.67 BU 56.5 10.1 O.S 0.80.' Tama Benton Cooperative 12 d;o PM**SPL~** 01/24/07 830086016**31059~** US1I1YS 9759 -51 53,960 699.33 SU 57.S 11.0. 0.6 0.90 Northeast Iowa coop

1:02 PM SPL.**01/2~/07** 630086017 310600 USUlYS 1247 -52 55,500**~2S.00** BU 57.S 10.3 0.5 0..80 Innovative Ag Services 1:07 PM Spt.., 01/24/07 630086018 310601 USn1YS 174

- 53 54,729 912.00. SU 56.0 10.7 0..5 0..90 Glandorf. Daniel

1,1) PM**SPL~** 01/24/07 830086019 310602 UBUYS 9356 -54 60,360 1,0.06.00 eu 57.5 .9.6 0.6 O.SO Innovative Ag**Se~vices**

1.19 PM SPI.­ 01/24/07 830086020 310603 USIIlYS 7902 -55 57,120 952.00. au 57.5 10... 0.5 0.70. Innovative Ag Services

1,30 PM SPL. 01/24/07 830066021 31060i UlHI1YB 8653 -56 57,240**95~.OO** SU 57.0 11.2 0.5 0..80 Ryan Cooperative

1:35 PM SPLa t1/24/07 830086022 310605 US#lYS 1402 -57 54,680 911.33 au 57.0 11.6· 0..8 0.80 Keystone Mercantile Co.

1:40 PM SIlL" 01/24/07 B30086023 UOS06 US!IlYS 465 -58 31.160 519.33 SU 56.0 13.5 0.5 0.70 Serbousek Farma Inc.

1,43 PM**SIlL~** 01/24/07 830086024 310607 USIT1YS 4565 -59 55,120 928.67 SU 57.5 10.9 0.5 O.BO Innovative Ag Services

1:49 PM SPL01/24/07 830066025 310608 USfflYS 1245 -60 56.860 947.67 

### au 57.5 10.9 0.5 0.80 Innovative Ag Services

1:54 filM SPt.­ 01/24/07 830096026 310609 US#lYS 492 -61 63,460 1,057.67 SU 56.5 11.2 0
.. 5 0.70 Keystone Mercantile Co. 2.00 11M**SPL~** 01/24/07 830086027 310610 USUYS 1552 -62 '.,7,400 956.67 SU 57.5 10.0 0.6 0.90 Innovative Ag Services 2,06 PM SPL" Ot/24/07 830086028 310611 USIIlY'S 5877 -63 53,800 896.67·SU 56.5 10.3 0.4 0.80 Tama Benton Cooperative 

### tl.P\ 2:11 PM SPL· [

. 01/24/07 830086029 310612 USlIJ.YS 0692 -664 53,980 699.67 BU 58.0 8.9 0.6 0.90 Tams Benton Cooperative 

## ") 01/24/07' 3:52 PM /opt/uxapps/batch/obloaunl.sqr Page 3LYNX Load/unload**Peta~l** Cedar Rapids west Facility, Cedar Rapids West, GOS Truck Unload Net !lgt Wgt cart / CUstomer /

Dl.\te Trace 1C!**BO~** Grade c/:I' Unit 10. In Pounds Quantity TW to! OKT FM SHBN DSF DKG BCI'M PROT FOr Account of
2,17 PM SPV= Ol/24/07 830086030 3101S13 USlllYS 1374 -65, 56.680 944,67 au 56.S 10,6 O.S 0.90 Tama Benton**Coope~ative** 2 :22 PM' SPLa 01/24/07 830086031 310614 USlIlYS 3769 -66 52,660 877,67 au 57.0 10.4 0,6 0.80 Innovative Ag Services 2,21 :I'M SPLz 01/24/07 830086032 310615 US#lYS 0259 -67 5:2,080 868.00 BU 56.5 11,1 0.5 0,80 F J XrOb « Co
. Walker 2,32 PM**SP~c** 01/44/07 830086033 310616 US#lYS 771S3 -68 57.280 954.67 BU 56.0 10,0 0,6 0.60 Tama Benton Cooperative 2,37 PM**SPL~** 01/24/07 830086034 nOol7 USl/lYS' 1403**-6~** 53,460 891.00 au 56.0**11,~** D,S 0,80 Keystone Mercantile Co. 2,4) PM SPLm 01/24/07 8300860j5 310618 USl/2YS 1375 -70 56.300 938,33 BU 57.0**9.~** 0.6 1.70 Tama Benton Cooperative 2:48, PM SPLQ 01/24/07 830086036 310619 USIIIYS 7238 -11 56,640 944,00 SU 57.5 10.8 0.6 1. 00 Circle J Grain

# ~Uh 

# ') 2:55 PM**SPL~** 01/24/07 830086037 310620 USlilYS , 1065 -12 57,680 961,33 

### au 57.0 lO,3 0.6 O.SO Northeast Iowa Coop 2:59 PM SPL01/24/07 830086038 310621 usltlYS 9356 -7,3 51,600 960.00 BU 56.S 10,5 0.5 0,90 Innovative Ag Se.vices 3:05 PM SPL01/24/07 830086039 310622 USfl1YS 1246 -74 54,620 910,33 au 57.0 10.2 0.5 O.SO Innovative Ag Service. 3: 10 PM SPL01/24/07 830086040 310623 US#lYS 7370 -75 51.160 853.00 

### au 56.5 11.1 0.4 0.70 F J Krob & Co • Walker

­

3,20 PM**SP~** 01/24/07 830086041 310624 USUYS 9759 -76 55,400 923.33 BU 57.5 10.8 0.4 0.60 Northeast Iowa Coop 3:24 PM**SP~_** 01/24/07 830086042 310625 USlllYS 5324 -77 :",,180 936,33 

### au 56.5 12.4 .0.4 0.70 Innovative Ag Services 3: 30 PM SPL= '01/24/07 830086043 310626 l1SlI1YS 9561 -78 57,000 950,00 

### au 56.S lZ.3 0.6 0.60 F J Krob I< Co • Ely

3:35 PM**SE'L~** 01/24/07 830086044 310627 USlI1YS 561 -79 54.040 900.67 

### au 57.5 11.2 0.4 O.BO Gericke, Daryl 3:41 PM SPL· TOtal 79 Units**~.** 342,220 72.310.32

summary of Unloads by Commodity/Product and Transportation Mode •• *
YSB Truck unload 72.370.32 eu 57.0 10.5 0.5 1.02 SPL= Total YSB Unload 12,310.:>2 au 57.0 10.5 0.5 1.02 SPLm

01/24/07 3: 52 'PM /opt/uxaPP9/batch/ohloaunl.sqr Page 4

____.._____. ________...__**~~_** ....._. ... w_ __'_
....**_~,,~'._u_.~_._ .~**  __ ' ••••••**_":'""""-.~---** ••**-.~.-.--** •••••LYNX

- Load/Unload Detail Cedar Rapids West l'a<::ility, Cedar RapidS west, 00$ TlruCk Unload Net Wgt Wgt Cert CUstomer I

Date Trace I d SOL Grade C/F Un1t td In Pounds Quantity TW M DKT FM SHaN OISF OKG BCFM: PROT For Account Of
Total Unload 72,370.32 

# _.* End of Report **.

01/24/07 3,52 PM {opt/uxapps/batch/obloaunl.sqr Page 5

# Appendix G Opacity Certification

i 

# I

# VISIBLE EMISSIONS EVALUATOR
This 

# is to certify that 

# MattMilligan
met the specifications ofFederal Reference Method 9 (40 CFR Part 60, Appendix A, Method 9) and qualified**a~)** 

# a visible emissions evaluator. Maximum deviation on white and black smoke did not exceed 7.5% opacity and no single error exceeding 15% opacity was incurred during the certification test conducted by Opaque Smoke School, LLC ofOverland Park, Kansas. This certificate is valid for six months from date ofissue.
.
Des MQines, IA October 3, 2006 

### 7669 

### Location Date ofIssue Certificate Number 

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