## EMISSIONS TEST REPORT FELMANPRODUCTION, INC. FURNACE #5 BAGHOUSE (ID# 001-02) WVDEP DAQ PERMIT # R30-0530004-2007 PLANT ID# 03-54-05300004 LETART, WEST VIRGINIA MARCH2013

TI-1550A

# ~~·TEST, Inc. • www.testincorp.com 

## TechnicalEnvironmentalServices Team

Route 2, Box 33-B, Poca, West Virginia 25159 Ph: (304) 755-1077Fx: (304) 755-1099

## TABLE OF CONTENTS
Introduction 1 Summary ofResults 1 Discussion ofResults 20 Sampling and Analytical Procedures 22 Sampling Location 27
Appendixes 29 A - ComputerDataand Example Calculations B- Pre-flowData C - Analytical Data D - Field Data Sheets E - Calibration Data F - Chain ofCustody

List ofTables Table 1 Summary ofResults HCl 2 Table 2 Summary ofResults Particulate Matter 3 Table 2a Summary ofResults Metals 4 Table 3 Summary ofResults Mercury 5 Table 4 Dioxins/Furans/PCBs Sampling Data 6 Table 4a Summary ofResults PCBs 7 Table 4b Summary ofResults PCBs (cont.) 8 Table 4c Summary ofResults PCBs (cont.) 9 Table 4d SummaryofResults PCBs (cont.) 10 Table 4e SummaryofResults Dioxins 11 Table 4f Summary ofResults Dioxins (cont.) 12 Table 4g Summary ofResults Furans 13 

### Table 4h Summary ofResults Furans (cont.) 14 Table 5 PAHs Sampling Data 15 Table 5a Summary ofResults PAHs 16 Table 5b SummaryofResults PAHs (cont.) 17 Table 5c Summary ofResults PAHs (cont.) 18 Table 5d Summary ofResults PAHs (cont.) 19

### INTRODUCTION 

## Emissions Test Report Felman Production, Inc. Furnace #5 Baghouse (ID#OO 1-02) WVDEP DAQ Permit# R30-0530004-2007 Plant ID# 03-54-05300004 Letart, West Virginia TI-1550A

Emissiontesting was conducted at Felman Production, Inc. located in Letart, West Virginia on March 13, 14, and 15,2013,by TEST, Incorporated, Charleston, West Virginia, underthe direction ofPaul Chinuntdet. The purpose ofthese tests was to determine the concentrations of particulate matter, hydrogen chloride, arsenic, cadmium, chromium, lead, manganese, nickel, mercury, dioxins/furans, polychlorinated biphenyls, andpolycyclic aromatic hydrocarbons being emitted into the atmosphere viathe Furnace #5 Baghouse. Mr. John Konrady ofFelman Productions, LLC. coordinatedthe testing withplant operations.

The testing followed the procedures in the Appendix to the Code ofFederal Regulations, Title 40, Chapter 1, Part 60, Methods 1, 2, 3A, 4, 5d, 26A, 29, and 30B; and CaliforniaAirResources Board Methods 428 (CARB 428), and 429 (CARB 429).

SUMMARY OF RESULTS

The following tables and graphs provide results for the emission rates measured on the Furnace #2 Baghouse. The emission results are presented in micrograms per dry 

### standard cubic meter (ug/dscm), nanograms per dry 

### standard cubic meter (ng/dscm), pounds per hour (lbs/hr), and pounds pertonproduct (lbs/ton). The lbs/ton were calculated usingthe following productionrates: March 13,2013 = 

### 4.85 tons/hr, March 14,2013 = 

### 4.41 tons/hr, and March 15,2013 = 

### 4.08 tons/hr.

# SUMMARY OF RESULTS

Run Number Date Time Carbon Dioxide Cone. - % Vol. Oxygen Concentration- %Vol. Stack Pressure

- "Hg Area ofStack- Sq. in. Volume Dry Gas Sampled

- dscf Volume Dry Gas Sampled

- dscm Stack Temperature- Deg. F Percent Moisture - % Velocity in the Stack

- FPS Volumetric FlowRate

- ACFM Volumetric FlowRate

- DSCFM Isokinetic Sampling Rate - % Hydrogen Chloride Concentrations- ug Hydrogen Chloride Emissions

- ug/dscm Hydrogen Chloride Emissions

- ppm Hydrogen Chloride Emissions

- lbs/hr 

## Table 1 HCl SamplingData Baghouse #5

1 2 3/15/13 3/15/13 1300

- 1535 1655

- 1905 0.40 0.40 20.50 20.40 29.06 29.05 518,400.00 518,400.00 94.809 92.009 2.685 2.605 142.50 133.00

0.77 1.07 1.22 1.20 263,160 261,360 222,266 223,527

104.3 100.6 230.00 200.00 85.66 76.78 0.06 0.05 0.0713 0.0643 Hydrogen Chloride Emissions

- lbs/ton prod. 0.017 0.016 Production Rate (tons/hr) = 

### 4.08

2 

### 3 Average 3/15/13


## ---- 1955

- 2205


## ---- 0.40 

### ---- 20.40


## ---- 28.96 

# ---- 518,400.00


## ---- 91.608


## ---- 2.594


## ---- 137.40


## ----

0.92


## ---- 1.30


## ---- 275,760 

### ---- 233,735 

# ----

95.8


## ---- 200.00 210.00 77.10 79.85 0.05 0.05 0.0675 0.0677 0.017 0.017

# SUMMARY OF RESULTS Table 2 Particulate/Metals Sampling Data Baghouse #5

Run Number 1 2 Date 3/13/13 3/13/13 Time 845

- 1300 845

- 1255 Carbon Dioxide Cone. - % Vol. 0.30 0.30 Oxygen Concentration

- %Vol. 20.60 20.60 Stack Pressure

- "Hg 29.11 29.11 Area ofStack

- Sq. in. 518,400.00 518,400.00 Volume Dry Gas Sampled

- dscf 203.222 205.272 Volume Dry Gas Sampled

- dscm 5.755 5.813 Stack Temperature- Deg. F 128.90 124.20 Percent Moisture - % 0.75 0.71 Velocity in the Stack

- FPS 1.33 1.30 Volumetric Flow Rate

- ACFM 286,200 284,760 Volumetric Flow Rate

- DSCFM 247,784 248,621 Isokinetic Sampling Rate - % 100.3 100.9 Particulate Matter Concentrations- gr/acf 0.0003 0.0003 Particulate Matter Concentrations- gr/dscf 0.0003 0.0004 Particulate Matter Concentrations- ug/dscm 608.17 883.08 Particulate Matter Emissions -lbs/hr 0.64 0.85 Particulate Matter Emissions

- lbs/ton prod. 0.13 0.18 Production Rate (tons/hr) = 4.85

3 

### 3 Average 3/13113


## ---- 1410

- 1820


## ---- 0.30


## ---- 20.50


## ---- 29.26


## ---- 518,400.00


## ----

201.867


## ----

5.716


## ---- 121.60 

### ----

0.55

---- 1.30


## ---- 283,320


## ---- 250,152


## ----

98.6


## ---- 0.0004 0.0003 0.0004 0.0004 857.24 782.83

0.86 0.78 0.18 0.16

# SUMMARY OF RESULTS Table 2a Particulate/Metals Sampling Data Baghouse #5

Run Number 1 2 Arsenic Concentrations

- ug 2.0 2.0 Arsenic Emissions- ug/dscm 0.35 0.34 Arsenic Emissions

- lbslhr 0.0003 0.0003 Arsenic Emissions

- lbs/ton prod. 0.0001 0.0001 Cadmium Concentrations

- ug 0.50 0.50 Cadmium Emissions

- ug/dscm 0.09 0.09 Cadmium Emissions -lbs/hr 0.0001 0.0001 Cadmium Emissions -lbs/tonprod. 1.66E-05 1.65E-05 Chromium Concentrations

- ug 7.40 38.30 Chromium Emissions

- ug/dscm 1.29 6.59 Chromium Emissions

- lbslhr 0.0012 0.0061 Chromium Emissions

- lbs/ton prod. 0.0002 0.0013 Lead Concentrations- ug 25.90 36.20 Lead Emissions- ug/dscm 4.50 6.23 Lead Emissions

- lbslhr 0.0042 0.0058 Lead Emissions

- lbs/ton prod. 0.0009 0.0012 Manganese Concentrations

- ug 607.00 547.00 Manganese Emissions- ug/dscm 105.47 94.10 Manganese Emissions

- lbs/hr 0.0979 0.0877 Manganese Emissions

- lbs/ton prod. 0.0202 0.0181 Nickel Concentrations

- ug 5.70 14.70 Nickel Emissions

- ug/dscm 0.99 2.53 Nickel Emissions

- lbslhr 0.0009 0.0024 Nickel Emissions

- lbs/ton prod. 0.0002 0.0005 Production Rate (tonslhr) 

### = 4.85 3 Average 2.0 2.0 0.35 0.35 0.0003 0.0003 0.0001 0.0001

0.50 0.50 0.09 0.09 0.0001 0.0001 1.69E-05 1.67E-05 3.60 16.43 0.63 2.83 0.0006 0.0026 0.0001 0.0005

14.00 25.37 2.45 4.39 0.0023 0.0041 0.0005 0.0008 400.00 518.00 69.98 89.85 0.0656 0.0837 0.0135 0.0173

4.30 8.23 0.75 1.42 0.0007 0.0013 0.0001 0.0003Vl 

# SUMMARY OF RESULTS

Time Run Trap 945

- 1145 1 A 156021 B 

### 156066 Average % Relative Deviation



# --

Time Run Trap 1230

- 1430 2 A 156064 B 

### 156014 Average % Relative Deviation

-



### Time Run Trap 1500

- 1700 3 A 150797* B 

### 156042 Average %Relative Deviation

------------- 

### *Spiked Production Rate (tonslhr) = 

### 4.41 

## Table 3 Vapor Stage Mercury Test Results Baghouse 5 Sample Sample Volume Volume Flow (1) 

### (dscm) (dscfm) ug 60.507 0.061 193,711 0.0013 58.359 0.058 193,711 0.0010 59.433 0.059 193,711 0.0011
Sample Sample Volume Volume Flow (1) 

### (dscm) (dscfm) ug 53.935 0.054 192,968 0.0015 52.617 0.053 192,968 0.0012 53.276 0.053 192,968 0.0013
Sample Sample Volume Volume Flow (1) 

### (dscm) (dscfm) ug 54.618 0.055 192,448 0.0019 54.580 0.055 192,448 0.0011 54.599 0.055 192,448 0.0015 Mercury Emissions ug/dscm lbslhr lbs/ton prod.

0.0208 1.51E-05 3.43E-06 0.0176 1.28E-05 2.90E-06 0.0192 1.40E-05 3.17E-06

8.25 Mercury Emissions ug/dscm lbslhr lbs/ton prod.

0.0273 1.97E-05 4.47E-06 0.0228 1.65E-05 3.74E-06 0.0250 1.81E-05 4.10E-06

8.89 Mercury Emissions ug/dscm lbslhr lbs/ton prod.

0.0355 2.56E-05 5.81E-06 0.0198 1.43E-05 3.23E-06 0.0277 1.99E-05 4.52E-06 28.44

# SUMMARY OF RESULTS Table 4 Dioxin/Furans/PCB's SamplingData Baghouse #5

Run Number 1 2 Date 3/15/13 3/15/13 Time 755

- 1010 1330- 1540 Carbon Dioxide Cone. - % Vol. 0.40 0.40 Oxygen Concentration

- %Vol. 20.50 20.50 StackPressure

- "Hg 29.46 29.06 Area ofStack- Sq. in. 518,400.00 518,400.00 Volume Dry Gas Sampled

- dscf 89.948 91.404 Volume Dry Gas Sampled

- dscm 2.547 2.588 StackTemperature- Deg. F 133.00 133.10 Percent Moisture - % 0.89 0.94 Velocity inthe Stack

- FPS 1.20 1.20 Volumetric FlowRate

- ACFM 259,560 261,360 Volumetric FlowRate

- DSCFM 225,531 223,860 Isokinetic Sampling Rate - % 97.5 99.8

6 

### 3 3/15/13 1700

- 1915 0.40 20.40 28.96 518,400.00 90.311 2.557 152.80

1.11 1.20 266,040 219,407

100.6

### Run Number 33'44'-TetraCB-(77)

344'5-TetraCB-(81)

233'44'-PentaCB-(105)

2344'5-PentaCB-(114)

23'44'5-PentaCB-(118)

23'44'5'-PentaCB-(123) 

# SUMMARY OF RESULTS Table 4a PCB Sampling Data Baghouse #5

1 2 ng 5.2 8.4 ng/dscm 2.04 3.25 lbs/hr 1.72E-06 2.72E-06 lbs/ton 4.23E-07 6.67E-07 ng 0.31 0.48 ng/dscm 0.12 0.19 lbs/hr 1.03E-07 1.56E-07 lbs/ton 2.52E-08 3.81E-08 ng 5.4 8.3 ng/dscm 2.12 3.21 lbs/hr 1.79E-06 2.69E-06 lbs/ton 4.39E-07 6.59E-07 ng 0.42 0.69 ng/dscm 0.16 0.27 lbs/hr 1.39E-07 2.24E-07 lbs/ton 3.41E-08 5.48E-08 ng 15 23 ng/dscm 5.89 8.89 lbs/hr 4.98E-06 7.45E-06 lbs/ton 1.22E-06 1.83E-06 ng 0.31 0.32 ng/dscm 0.12 0.12 lbs/hr 1.03E-07 1.04E-07 lbs/ton 2.52E-08 2.54E-08 Production Rate (tons/hr) = 

### 4.08 3 Average 6.6 6.7 2.58 2.62 2.12E-06 2.19E-06 5.20E-07 5.37E-07 0.42 0.40 0.16 0.16 1.35E-07 1.31E-07 3.31E-08 3.21E-08 6.2 6.6 2.42 2.58 1.99E-06 2.16E-06 4.88E-07 5.29E-07 0.51 0.54 0.20 0.21 1.64E-07 1.76E-07 4.02E-08 4.30E-08 17 18 6.65 7.14 5.46E-06 5.96E-06 1.34E-06 1.46E-06

0.34 0.32 0.13 0.13 1.09E-07 1.05E-07 2.68E-08 2.58E-08

# SUMMARY OF RESULTS

Run Number 33'44'5-PentaCB-(126)

HexaCB-(156)+(157)

23'44'55'-HexaCB-(167)

33'44'55'-HexaCB-(169)

233'44'55'-HeptaCB-(189)

C13-233'44'55'-HeptaCB-(189) 

## Table 4b PCB Sampling Data Baghouse #5

1 2 ng 0.1 0.16 ng/dscm 0.04 0.06 lbs/hr 3.32E-08 5.18E-08 lbs/ton 8.13E-09 1.27E-08 ng 0.52 0.76 ng/dscm 0.20 0.29 lbs/hr 1.72E-07 2.46E-07 lbs/ton 4.23E-08 6.04E-08 ng 0.22 0.32 ng/dscm 0.09 0.12 lbs/hr 7.30E-08 1.04E-07 lbs/ton 1.79E-08 2.54E-08 ng 0.037 0.036 ng/dscm 0.01 0.01 lbs/hr 1.23E-08 1.17E-08 lbs/ton 3.01E-09 2.86E-09 ng 0.026 0.029 ng/dscm 0.01 0.01 lbs/hr 8.62E-09 9.40E-09 lbs/ton 2.11E-09 2.30E-09 ng 94 101 ng/dscm 36.91 39.03 lbs/hr 3.12E-05 3.27E-05 lbs/ton 7.64E-06 8.02E-06 Production Rate (tons/hr) = 

### 4.08 3 Average 0.17 0.14 0.07 0.06 5.46E-08 4.66E-08 1.34E-08 1.14E-08

0.60 0.63 0.23 0.24 1.93E-07 2.04E-07 4.73E-08 5.00E-08 0.23 0.26 0.09 0.10 7.39E-08 8.35E-08 1.81E-08 2.05E-08

0.04 0.04 0.02 0.01 1.29E-08 1.23E-08 3.15E-09 3.01E-09 0.03 0.03 0.01 0.01 9.64E-09 9.22E-09 2.36E-09 2.26E-09 95 97 37.15 37.70 3.05E-05 3.15E-05 7.48E-06 7.72E-06

### Run Number C13-233'44'5-HexaCB-(156)

C13-233'44'5'-HexaCB-(157)

C13-233'44'-PentaCB-(105)

C13-23'44'55'-HexaCB-(167)

C13-2344'5-PentaCB-(114)

C13-23'44'5-PentaCB-(118) 

# SUMMARY OF RESULTS Table 4c PCB Sampling Data Baghouse #5

1 2 ng 110 120 ng/dscrn 43.19 46.37 lbslhr 3.65E-05 3.89E-05 lbs/ton 8.94E-06 9.53E-06 ng 110 120 ng/dscrn 43.19 46.37 lbslhr 3.65E-05 3.89E-05 lbs/ton 8.94E-06 9.53E-06 ng 112 121 ng/dscrn 43.97 46.75 lbslhr 3.72E-05 3.92E-05 lbs/ton 9.11E-06 9.61E-06 ng 107 120 ng/dscrn 42.01 46.37 lbslhr 3.55E-05 3.89E-05 lbs/ton 8.70E-06 9.53E-06 ng 115 130 ng/dscrn 45.15 50.23 lbslhr 3.81E-05 4.21E-05 lbs/ton 9.35E-06 1.03E-05 ng 115 129 ng/dscrn 45.15 49.85 lbslhr 3.81E-05 4.18E-05 lbs/ton 9.35E-06 1.02E-05 Production Rate (tonslhr) 

### = 4.08 3 Average 114 115 44.58 44.71 3.66E-05 3.73E-05 8.98E-06 9.15E-06 114 115 44.58 44.71 3.66E-05 3.73E-05 8.98E-06 9.15E-06 113 115 44.19 44.97 3.63E-05 3.76E-05 8.90E-06 9.21E-06 112 113 43.80 44.06 3.60E-05 3.68E-05 8.82E-06 9.02E-06 118 121 46.15 47.18 3.79E-05 3.94E-05 9.30E-06 9.66E-06 119 121 46.54 47.18 3.82E-05 3.94E-05 9.37E-06 9.66E-06

### Run Number C13-2'344'5-PentaCB-(123)

C13-33'44'55'-HexaCB-(169)

C13-33'44'5-PentaCB-(126)

C13-33'44'-TetraCB-(77)

C13-344'5-TetraCB-(81) 

# SUMMARY OF RESULTS Table 4d PCB SamplingData Baghouse #5

1 2 ng 114 129 ng/dscm 44.76 49.85 lbs/hr 3.78E-05 4.18E-05 lbs/ton 9.27E-06 1.02E-05 ng 111 113 ng/dscm 43.58 43.66 lbs/hr 3.68E-05 3.66E-05 lbs/ton 9.02E-06 8.97E-06 ng 123 136 ng/dscm 48.29 52.55 lbs/hr 4.08E-05 4.41E-05 lbs/ton 1.00E-05 1.08E-05 ng 123 137 ng/dscm 48.29 52.94 lbs/hr 4.08E-05 4.44E-05 lbs/ton 1.00E-05 1.09E-05 ng 117 127 ng/dscm 45.94 49.07 lbs/hr 3.88E-05 4.12E-05 lbs/ton 9.51E-06 1.01E-05 Production Rate (tons/hr) = 

### 4.08

10 

### 3 Average 114 119 44.58 46.40 3.66E-05 3.88E-05 8.98E-06 9.50E-06 110 111 43.02 43.42 3.54E-05 3.63E-05 8.67E-06 8.89E-06 124 128 48.49 49.78 3.99E-05 4.16E-05 9.77E-06 1.02E-05 121 127 47.32 49.52 3.89E-05 4.14E-05 9.53E-06 1.01E-05 112 119 43.80 46.27 3.60E-05 3.87E-05 8.82E-06 9.47E-06

### Run Number 2,3,7,8-Tetra CDD 

# *

1,2,3,7,8-PentaCDD

1,2,3,4,7,8-Hexa CDD

1,2,3,6,7,8-HexaCDD

1,2,3,7,8,9-HexaCDD 

# SUMMARY OF RESULTS Table 4e Dioxins SamplingData Baghouse #5

1 2 ng 3.5 11.9 ng/dscm 1.37 4.60 lbs/hr 1.16E-06 3.86E-06 lbs/ton 2.85E-07 9.45E-07 ng 3.5 7.8 ng/dscm 1.37 3.01 lbs/hr 1.16E-06 2.53E-06 lbs/ton 2.85E-07 6.19E-07 ng 3.2 4.5 ng/dscm 1.26 1.74 lbs/hr 1.06E-06 1.46E-06 lbs/ton 2.60E-07 3.57E-07 ng 3.1 5.6 ng/dscm 1.22 2.16 lbs/hr 1.03E-06 1.81E-06 lbs/ton 2.52E-07 4.45E-07 ng 3.2 6.0 ng/dscm 1.26 2.32 lbs/hr 1.06E-06 1.94E-06 lbs/ton 2.60E-07 4.76E-07 Production Rate (tons/hr) = 

### 4.08

11 

### 3 Average 9.5 8.3 3.72 3.23 3.05E-06 2.69E-06 7.48E-07 6.59E-07 6.6 6.0 2.58 2.32 2.12E-06 1.94E-06 5.20E-07 4.75E-07 3.3 3.7 1.29 1.43 1.06E-06 1.19E-06 2.60E-07 2.93E-07 3.2 4.0 1.25 1.54 1.03E-06 1.29E-06 2.52E-07 3.16E-07 3.2 4.1 1.25 1.61 1.03E-06 1.34E-06 2.52E-07 3.30E-07

### Run Number 1,2,3,4,6,7,8-Hepta CDD

1,2,3,4,6,7,8,9-0cta CDD 

# SUMMARY OF RESULTS Table 4f Dioxins Sampling Data Baghouse #5

1 2 ng 5.2 13.7 ng/dscm 2.04 5.29 lbslhr 1.72E-06 4.44E-06 lbs/ton 4.23E-07 1.09E-06 ng 11.9 37.8 ng/dscm 4.67 14.61 lbslhr 3.95E-06 1.22E-05 lbs/ton 9.68E-07 3.00E-06 Production Rate (tonslhr) 

### = 4.08

12 

### 3 Average 3.1 7.3 1.21 2.85 9.96E-07 2.39E-06 2.44E-07 5.85E-07 4.7 18.1 1.84 7.04 1.51E-06 5.90E-06 3.70E-07 1.45E-06

### Run Number 2,3,7,8-Tetra CDF 

# **

1,2,3,7,8-Penta CDF

2,3,4,7,8-Penta CDF

1,2,3,4,7,8-Hexa CDF

1,2,3,6,7,8-Hexa CDF 

# SUMMARY OF RESULTS Table 4g Furans Sampling Data Baghouse #5

1 2 ng 220 260 ng/dscm 86.38 100.46 lbslhr 7.30E-05 8.42E-05 lbs/ton 1.79E-05 2.06E-05 ng 23.7 32.9 ng/dscm 9.31 12.71 lbslhr 7.86E-06 1.07E-05 lbs/ton 1.93E-06 2.61E-06 ng 20.6 28.7 ng/dscm 8.09 11.09 lbs/hr 6.83E-06 9.30E-06 lbs/ton 1.67E-06 2.28E-06 ng 13 20.2 ng/dscm 5.10 7.81 lbslhr 4.31E-06 6.55E-06 lbs/ton 1.06E-06 1.60E-06 ng 5.5 11.3 ng/dscm 2.16 4.37 lbs/hr 1.82E-06 3.66E-06 lbs/ton 4.47E-07 8.97E-07 Production Rate (tons/hr) = 

### 4.08

13 

### 3 Average 460 313 179.90 122.25 1.48E-04 1.02E-04 3.62E-05 2.49E-05 46.3 34.3 18.11 13.37 1.49E-05 l.llE-05 3.65E-06 2.73E-06 38.1 29.1 14.90 11.36 1.22E-05 9.46E-06 3.00E-06 2.32E-06 26.8 20.0 10.48 7.80 8.61E-06 6.49E-06 2.11E-06 1.59E-06 13.4 10.1 5.24 3.92 4.31E-06 3.26E-06 1.06E-06 8.00E-07

### RunNumber 2,3,4,6,7,8-Hexa CDF

1,2,3,7,8,9-Hexa CDF

1,2,3,4,6,7,8-Hepta CDF

1,2,3,4,7,8,9-HeptaCDF

1,2,3,4,6,7,8,9-0cta CDF 

# SUMMARY OF RESULTS Table 4h Furans Sampling Data Baghouse#5

1 2 ng 3.4 8.4 ng/dscm 1.33 3.25 lbslhr 1.13E-06 2.72E-06 lbs/ton 2.76E-07 6.67E-07 ng 3.8 4.8 ng/dscm 1.49 1.85 lbslhr 1.26E-06 1.56E-06 lbs/ton 3.09E-07 3.81E-07 ng 4.6 10.9 ng/dscm 1.81 4.21 lbslhr 1.53E-06 3.53E-06 lbs/ton 3.74E-07 8.66E-07 ng 3.5 3.6 ng/dscm 1.37 1.39 lbslhr 1.16E-06 1.17E-06 lbs/ton 2.85E-07 2.86E-07 ng 4.5 17.5 ng/dscm 1.77 6.76 lbslhr 1.49E-06 5.67E-06 lbs/ton 3.66E-07 1.39E-06 Production Rate (tonslhr) = 

### 4.08

14 

### 3 Average 5.1 5.633 1.99 2.19 1.64E-06 1.83E-06 4.02E-07 4.48E-07 3.3 3.967 1.29 1.55 1.06E-06 1.29E-06 2.60E-07 3.17E-07 10.1 8.5 3.95 3.32 3.25E-06 2.77E-06 7.96E-07 6.78E-07 5 4.0 1.96 1.57 1.61E-06 1.31E-06 3.94E-07 3.21E-07 33.6 18.5 13.14 7.22 1.08E-05 5.99E-06 2.65E-06 1.47E-06

# SUMMARY OF RESULTS Table 5 

## PAH SamplingData Baghouse #5

RunNumber 1 Date 3/14/13 Time 930

- 1145 Carbon Dioxide Cone. - % Vol. 0.30 Oxygen Concentration- %Vol. 20.50 Stack Pressure

- "Hg 29.46 Area ofStack

- Sq. in. 518,400.00 Volume Dry Gas Sampled

- dscf 79.204 Volume Dry Gas Sampled

- dscm 2.243 Stack Temperature- Deg. F 117.40 Percent Moisture - % 1.22 Velocity inthe Stack

- FPS 1.01 Volumetric FlowRate

- ACFM 217,800 Volumetric FlowRate

- DSCFM 193,711 Isokinetic Sampling Rate - % 100.0

15 

### 2 3/14113 1240- 1455 0.30 20.60 29.46 518,400.00 81.821 2.317 125.70

0.84 1.00 219,240 192,968

103.7 3 3/14/13 1520

- 1730 0.40 20.40 29.08 518,400.00 76.216 2.158 122.20

0.74 1.00 219,960 192,448

96.8

### Run Number Naphthalene

2-Methylnaphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene 

# SUMMARY OF RESULTS Table 5a PAH Sampling Data Baghouse #5

1 ng 45100 ng/dscrn 20107.00 lbslhr 0.0146 lbs/ton 0.0033 ng 19200 ng/dscrn 8559.96 lbslhr 0.0062 lbs/ton 0.0014 ng 9040 ng/dscrn 4030.32 lbs/hr 0.0029 lbs/ton 0.0007 ng 4030 ng/dscrn 1796.70 lbslhr 0.0013 lbs/ton 0.0003 ng 5080 ng/dscrn 2264.82 lbslhr 0.0016 lbs/ton 0.0004 ng 67100 2 28600 12343.55

0.0089 0.0020 15900 6862.32 0.0050 0.0011

4780 2063.01 0.0015 0.0003

2680 1156.67 0.0008 0.0002

2950 1273.20 0.0009 0.0002 53400 ng/dscrn 29915.29 23047.04 lbslhr 0.0217 0.0167 lbs/ton 0.0049 0.0038 Production Rate (tonslhr) = 

### 4.41 3 Average 31100 34933 14411.49 15620.68

0.0104 0.0113 0.0024 0.0026 19100 18067 8850.79 8091.02 0.0064 0.0059 0.0014 0.0013

3760 5860 1742.35 2611.89 0.0013 0.0019 0.0003 0.0004

2370 3027 1098.24 1350.54 0.0008 0.0010 0.0002 0.0002

2280 3437 1056.53 1531.52 0.0008 0.0011 0.0002 0.0003 36900 52467 17099.17 23353.83

0.0123 0.0169 0.0028 0.0038

### RunNumber Anthracene

Fluoranthene

Pyrene

Benzo(a)anthracene

Chrysene

Benzo(b)fluoranthene 

# SUMMARY OF RESULTS Table 5b PAH Sampling Data Baghouse #5

1 2 ng 2170 2650 ng/dscm 967.45 1143.72 lbs/hr 0.0007 0.0008 lbs/ton 0.0002 0.0002 ng 45700 43000 ng/dscm 20374.50 18558.48 lbs/hr 0.0148 0.0134 lbs/ton 0.0034 0.0030 ng 23000 26600 ng/dscm 10254.12 11480.36 lbs/hr 0.0074 0.0083 lbs/ton 0.0017 0.0019 ng 956 466 ng/dscm 426.21 201.12 lbs/hr 0.0003 0.0001 lbs/ton 7.01E-05 3.30E-05 ng 6850 4500 ng/dscm 3053.95 1942.17 lbs/hr 0.0022 0.0014 lbs/ton 0.0005 0.0003 ng 956 466 ng/dscm 426.21 201.12 lbs/hr 0.0003 0.0001 lbs/ton 7.01E-05 3.30E-05 Production Rate (tons/hr) 

## = 4.41 3 Average 1360 2060 630.21 913.80 0.0005 0.0007 0.0001 0.0001 18200 35633 8433.73 15788.90 0.0061 0.0114 0.0014 0.0026

9510 19703 4406.86 8713.78 0.0032 0.0063 0.0007 0.0014

266 563 123.26 250.20 0.0001 0.0002 2.01E-05 4.11E-05 1620 4323 750.70 1915.60 0.0005 0.0014 0.0001 0.0003

266 563 123.26 250.20 0.0001 0.0002 2.01E-05 4.11E-05

### Run Number Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene 

# SUMMARY OF RESULTS Table 5c 

## PAH Sampling Data Baghouse #5

1 2 ng 344 135 ng/dscm 153.37 58.26 lbs/hr 1.11E-04 4.21E-05 lbs/ton 2.52E-05 9.55E-06 ng 1150 477 ng/dscm 512.71 205.87 lbs/hr 0.0004 0.0001 lbs/ton 8.44E-05 3.37E-05 ng 27 16 ng/dscm 12.04 6.91 lbs/hr 8.74E-06 4.99E-06 lbs/ton 1.98E-06 1.13E-06 ng 18 11 ng/dscm 8.02 4.75 lbs/hr 5.82E-06 3.43E-06 lbs/ton 1.32E-06 7.78E-07 ng 50.6 16.6 ng/dscm 22.56 7.16 lbs/hr 1.64E-05 5.18E-06 lbs/ton 3.71E-06 1.17E-06 ng 8.5 2.8 ng/dscm 3.79 1.21 lbs/hr 2.75E-06 8.74E-07 lbs/ton 6.24E-07 1.98E-07 Production Rate (tons/hr) = 

### 4.41 3 Average 92.7 190.6 42.96 84.86 3.10E-05 6.15E-05 7.02E-06 1.39E-05 273 633 126.51 281.69 0.0001 0.0002 2.07E-05 4.63E-05 10 18 4.63 7.86 3.34E-06 5.69E-06 7.58E-07 1.29E-06 7.2 12.1 3.34 5.37 2.41E-06 3.89E-06 5.45E-07 8.81E-07 8 25 3.71 11.14 2.67E-06 8.07E-06 6.06E-07 1.83E-06 2 4 0.93 1.97 6.68E-07 1.43E-06 1.52E-07 3.24E-07

### Run Number Benzo(g,h,i)perylene 

# SUMMARY OF RESULTS

ng 

## Table 5d 

## PAH Sampling Data Baghouse #5

1 58.9 ng/dscm 26.26 2 25.2 10.88 lbslhr 1.91E-05 7.86E-06 lbs/ton 4.32E-06 1.78E-06 Production Rate (tonslhr) 

### = 4.41

19 

### 3 Average 10.9 31.7 5.05 14.06 3.64E-06 1.02E-05 8.26E-07 2.31E-06

### DISCUSSION OF RESULTS

Three tests for particulate matter, hydrogen chloride, arsenic, cadmium, chromium, lead, manganese, nickel, mercury, dioxins/furans, polychlorinated biphenyls, and polycyclic aromatic hydrocarbons were performed onthe Furnace #5 Baghouse. The results ofthe tests appear to be an accurate and valid representation ofthe actual emissions ofthe stack. Leak checks were performed
onthe sampling systems to maintainthe integrity ofthe samples and no leaks were detected. 

### Hydrogen Chloride The moisture percentages were consistent with the largest variation being 16.3 percent from the
mean value of0.92 percent. The flow rates were consistent with the largest variation being 3.19 percent from the mean value of226,509 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % 

### isokinetic) with the largest variation being 4.3 percent from 100 percent.


### Particulate/Metals The moisture percentages were consistent with the largest variation being 17.91 percent from the
mean value of0.67 percent. The flow rates were consistent with the largest variation being 0.52 percent from the mean value of248,852 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % 

### isokinetic) with the largest variation being 1.4 percent from 100 percent. 

### Mercury Paired samples for mercury were taken simultaneously for eachrun. The relative deviation percentages were withinthe allowable limits ofthe method for eachrun.

20

### Dioxins/Furans/PCBs 

### The moisture percentages were consistent with the largest variation being 13.27 percent from the
mean value of0.98 percent. The flow rates were consistent with the largest variation being 1.58 percent from the mean value of222,933 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % isokinetic) with the largest variation being 2.5 percent from 100 percent.
Polycyclic Aromatic Hydrocarbons 

### (PAH) 

### The moisture percentages were consistent with the largest variation being 30.71 percent from the
mean value of0.93 percent. The flow rates were consistent with the largest variation being 0.35 percent from the mean value of 193,042 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % 

### isokinetic) with the largest variation being 3.7 percent from 100 percent.

21

### SAMPLINGAND ANALYTICAL PROCEDURES

The testing followed the procedures inthe Appendix to the Code ofFederal Regulations, Title 40, Chapter 1, Part 60, Methods 

### 1, 2, 3A, 4, 5d, 26A, 29, and 30B; and CaliforniaAirResources Board Methods 428 (CARB 428), and 429 (CARB 429). Three tests wereperformed for each pollutant. The manometer was zeroed and leak checks wereperformedbefore eachtest. Leak checks were performed onthe sampling systems to maintainthe integrity ofthe samples andno leaks were detected.

A velocity traverse was performed onthe inletto the baghousepriorto thetesting according to EPA Method 5D. The inlet velocity was used to calculate the isokinetic setup and determine the velocity in the outlet ofthe baghouse for each test. Once the preliminary inlet velocity was determined, Equation 5D-3 from Method 5D was used to determine the dilution 

### air flow rate ofthe baghouse and applied to the baghouse velocity.
Hydrogen Chloride The hydrogen chloride samples were taken according to EPA Methods 5D and 26A. Foreach run, samples offive minute duration were taken isokinetically from each ofthe twenty-four traverse points for a total sampling time of 120 minutes. Blank samples were collected for each reagent used during sampling and analyzed for contamination.

The "front-half' ofthe sampling train consisted of a glass nozzle, heated glass probe (248<>p 

## + 25<>p), and heated Teflon filter support with a quartz fiber filter (248°F 

## + 25<>p). The "back-half' of the sampling train containedthe following impingers: Impinger Contents Amount 1 0.1 N. H2S04 100 

### ml 2 0.1 N. H2S04 100 

### ml 3 Empty 4 SilicaGel 400 g

22 

### Parameter HCl HCl Moisture Moisture

### The impingers were measured to determine moisture content and then rinsed and recovered using de-ionized waterinto a leak-free amber glass samplejarwith a Teflon lid.

The samples were analyzed using ion chromatography by Maxxam Analytics, Inc located in Mississauga, Ontario.

Particulate Matter/Multiple Metals The particulate matter and multiple metals samples were taken according to EPA Methods 5D and 29. For each run, 

### samples oftenminute duration were takenisokineticallyfrom eachofthe twentyfour traverse points for a total sampling time of240 minutes. Data was recorded in five minute intervals. Blank samples were collected for each reagent used during sampling and analyzed for contamination.

The "front-half" of the sampling train consisted of a glass nozzle, heated glass probe (248<lp 

## + 25<lp), and heated Teflon filter support with a quartz fiber filter (248<lp 

## +25<lp). The "back-half' of the samplingtrain containedthe following impingers: Im.pinger 1 

### 2 

### 3 4 

### Contents 5%HN03/1O%H202 5%HN03/lO%H202 Empty SilicaGel Amount 100ml 100ml
400g Parameter Metals Metals Metals Moisture

The filter was recovered and collected in a sealed petri dish. The "front-half' ofthe sampling train (nozzle, probe, and :front-halffilterholder) was rinsed with acetone and collected in a leak-free amber glass sampling bottle with teflon lid. The "front-half' ofthe sampling train (nozzle, probe, and :front-halfoffilter holder) was then rinsed three times with a total of 1 

### OOml of0.1 N HN03 and collected in a leak-free amber glass sample bottle with Teflon lid. The impinger contents
were measured to determine the moisture content and then collected in a leak-free amber glass sample bottle with teflon lid. The back-half of the filter holder, impingers, and connecting

23

### glassware were then rinsed with three times with a total of 1 OOml of0.1 N HN03 and collected into the same sample bottle as the impinger contents.

The metals samples were analyzed by ICP-MS and ICP-AES according to EPA Method 29, by Maxxam Analytics, Inc located in Mississauga, Ontario. The particulate samples were analyzed using gravimetric analysis by TEST, Incorporated located inPoca, WestVirginia.
Mercury 

### The mercury samples were taken according to EPA Methods 30B. Samples ofeighteen minute duration were taken from each of the seven traverse points for a total sampling time of 126 minutes on each stack. Each run consisted ofpaired samples. Blank and spiked samples were taken, recovered, and analyzed for contamination. The sampling train consisted ofa two stage sorbent trap, heated probe, sample line, and gas meter and pump. The paired sorbent traps were contained withinthe heated probe.

The samples were analyzed for mercury by Ohio Lumex, Twinsburg, Ohio.
Dioxins/Furans/Polychlorinated Biphenyls 

### The dioxins/furans/PCBs samples were taken according to EPA Method 5D and CARB 428. For each run, samples offive minute duration were taken isokinetically from each ofthe twenty-four traverse points for a total samplingtime of 120 minutes. Datawas recorded infive minute intervals. Blank samples were collected for eachreagent used during sampling and analyzed for contamination. A trainblank was also performed and analyzed for contamination.

The "front-half" ofthe sampling train consisted ofa glass nozzle, heated glassprobe (248Dp

# ± 25Dp), and heated Teflon filter support with a quartz fiber filter (248Dp 

## ±25Dp). The "back-half' of the sampling train contained the following impingers:

24

### Impinger Contents Water-cooled condenser coil Water-cooled XAD-2 adsorbenttube 1 2 

### 3 4 Empty De-ionized water empty Silica Gel Amount

lOOml
400g Parameter

Dioxins/Furans/PCBs Dioxins/Furans/PCBs Dioxins/Furans/PCBs Moisture
The filter was recovered and collected ina sealedpetri dish. The "front-half'' ofthe sampling train (nozzle, probe, and front-halfoffilter holder) wasrinsed andbrushedthree times with methanol, benzene, and methylene chloride and collected in a leak-free amberglass sampling bottle withteflon lid. The impinger contents were measured to determine the moisture content and then collected in a leak-free amber glass sample bottle withteflon lid. The "back-half' of the filter holder, connecting glassware before the condenser, andthe condenserwas rinsed with methanol, benzene, and methylene chloride and collected ina leak-free amberglass sampling bottle withteflon lid. The XAD-2 trap was recovered, covered with aluminum foil and refrigerated.
The dioxins/furans/PCBs samples were analyzed by

### high resolution mass spectrometry according to CARB 428, byMaxxam Analytics, Inc located inMississauga, Ontario.
Polycyclic Aromatic Hydrocarbons 

### Thepolycyclic aromatic hydrocarbon samples were taken accordingto CARB 429. For eachrun, samples offive minute duration were taken isokineticallyfrom each ofthetwenty-fourtraverse points for a total samplingtime of 120 minutes. Datawasrecorded infive minute intervals. Blank samples were collected for eachreagent used during sampling and analyzed for contamination.

The "front-half'' ofthe samplingtrain consisted ofa glass nozzle, heated glassprobe (248op

## ± 25op), andheated Teflon filter supportwith a quartz fiber filter (248°F

## ±25op). The "back-half'' of the sampling train contained the following impingers:

25

### Im2inger Contents Amount Parameter Water-cooled condenser coil Water-cooled XAD-2 adsorbent tube 1 

### Empty



### --------- PAH 2 3mMNaHC03/2.4mMNa2C03 lOOml PAH 3 3mMNaHC03/2.4mMNa2C03 lOOml PAH 4 empty PAH 5 

### Silica Gel 400 g Moisture

The filter was recovered and collected in a sealed petri dish. The impinger contents were measured to determine the moisture content and then collected in a leak-free amber glass sample bottle with Teflon lid. The "front-half' and "back-half' ofthe sampling train (nozzle, probe, and front and back-halfoffilter holder, connecting glassware, and condenser) were rinsed three times each with acetone, hexane, and methylene chloride and collected in a leak-free amber glass sample bottle with Teflon lid. The impingers and connecting glassware were then rinsed three times each with acetone, hexane, and methylene chloride and collected into the same sample bottle as the impinger contents. The XAD-2 trap was recovered, covered with aluminum foil and refrigerated.

The PAH samples were analyzed according to CARB 429 by Maxxam Analytics, Inc located in Mississauga, Ontario.

26N .....:J 

### Baghouse 5 40'

Baghouse 5 Dimensions = 

### 40' Area OfDuct = X 

### 90' 518,400.0 sq. inches

DrawingsNotto Scale 

## 90' 

# • • • • 

# • • •

I I I I i I I I ! I**-------'-------L------~------L------~-------4----** I I I I I i I i 

# • • • 

# • • 

# • •**-------i-------~------:------~------~**_______ j

___ _ I 

# • • • • • • •

I
: : : ; I 1**i------~------,------~-------t-------~-------** 

# • • 

# • • • • •

Traverse Feet from

Points StackWall 1 5 2 15 3 25 

### 4 35N 00 

### Furnace #5 Baghouse Inlet



# - Gas Flow 

# -
8

# I**4----------------------.1~ ~**  

### 491" 240"

Inside Diameter ofStack 

## = 9 

### ft. 0 m. Portto Upstream Distance 

## = 20 ft. 0.0 in. Port to Downstream Distance 

## = 40 ft. 11.0 in. Area OfStack 

## = 9,160.9 sq. inches Portto Upstream Distance 

## = 2.22 Stack Diameters Port to Downstream Distance 

## = 4.55 Stack Diameters Drawings Notto Scale Traverse Percent of Inches From Points Diameter Stack Wall 1 2.1 2 4/16 2 6.7 7 4/16 3 11.8 12 12/16 4 17.7 19 2/16 5 25.0 27 6 35.5 38 5/16 7 64.5 6911116 8 75.0 81 9 

### 82.3 88 14116 10 88.2 95 4/16 11 93.3 100 12/16 12 97.9 105 12116

## APPENDIXES

A - Computer Data and Example Calculations B- Pre-flow Data C - Analytical Data D - Field Data Sheets E - Calibration Data F - Chain ofCustody G - Plant Operational Data

29

### APPENDIX A COMPUTERDATA AND EXAMPLE CALCULATIONS

...·.;

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #5 PROJECT#: TI1550

Run Number 1 2 3 Date 3/15/13 3/15/13 3/15/13 Time 1300

- 1535 1655

- 1905 1955 -2205 0 = Sample time 120 120 120 minutes Pb = Barometric Pressure at Port Elevation 29.05 29.05 28.95 in. Hg Vm =Vol. ofMetered Gas- meter cond., cal corr. 96.547 95.480 93.870 cu. ft. Tm = Meter Temperature 64.5 74.5 65.9 Farenheit Tm =MeterTemperature 524.5 534.5 525.9 Rankine Po = Meter Orifice Pressure 1.79 1.80 1.74 in. H20 Pma = Meter Pressure Absolute 29.18 29.18 29.08 in. Hg Vtwet =Sampled Gas Volume Wet 112.233 107.563 108.063 cu. ft. Vtstd = Sampled Gas Volume at Stand. Cond., dry 94.809 92.009 91.608 cu.ft Vtstd = Sampled Gas Volume at Stand. Cond., dry 2.685 2.605 2.594 cu. Meter C02 =%C02,dry 0.40 0.40 0.40 % 02 =%02,dry 20.50 20.40 20.40 % 

# co =%CO, dry 0.00 0.00 0.00 % N2 = %N2,dry (N2+CO) = 1 OO-(C02+02) 79.10 79.20 79.20 % EA =Excess Air 4,442.0 3,469.4 3,469.4 % Vw =Volume Water 15.6 21.1 18.1 grams H20 =mgas 0.77 1.07 0.92 % H20 = Moisture in Gas at Saturation 21.43 16.75 18.86 % Md =DryMolecular Weight ofStack Gas 28.88 28.88 28.88 Mw = Wet Molecular Weight ofStack Gas 28.80 28.76 28.78 Psg = Stack Pressure, gauge - measured 0.10 0.00 0.10 in. H20 Psa = Stack Pressure, absolute 29.06 29.05 28.96 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #5 PROJECT#: TI1550

Run Number 1 2 3 Ts =StackTemperature 142.50 133.00 137.40 Farenheit Ts = Stack Temperature 334.39 329.11 331.56 Kelvin Ts =StackTemperature 602.5 593 597.4 Rankine 

# \I L'l 

### P = Avg. Sum. ofPressure Square Root 0.02 0.02 0.021

Vs = Velocity in the Stack 73.1 72.6 76.6 ft/min Vs = Velocity in the Stack 1.22 1.20 1.30 ft/sec As = Effective Stack Area 518,400.0 518,400.0 518,400.0 sq.m. Qa = Volumetric FlowRate at stack cond. 263,160 261,360 275,760 acfm Qs = Volumetric FlowRate, stand. cond., dry 

### 222,266 223,527 233,735 dscfm IR = Isokinetic Ratio (Vn!Vs)*100 104.3 100.6 95.8 %

# TEST, Inc. 

# I Comments: 

## HCI Sampling Data Project # TI1550 MeterBox# 2010 mst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC MeterCal. (Y) 1.0302 %02 20.50 1 694.5 673.5 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 709.2 728.1

Operator br Nozzle# %N2 79.10 3 608.4 610 Run# 1 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 900.7 916.8

Date 3/15/13 Stack Dia.(in.) Final Moist. % 0.77 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic % 104.3 6 Min/pt 5 Bar. Press. ("Hg) 29.05 Initial Leak Rate 0.0015 cfm@ 11 "Hg Filter# Leak CheckVol. Final LeakRate 0.001 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1300 982.508 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 4-6 1305 986.045 0.0004 1.70 0.759 3.0 145 264 238 67 61 59

5 1310 990.000 0.0004 1.70 0.759 3.0 153 260 248 54 

### 63 60 4 1315 993.665 0.0004 1.70 0.759 3.0 135 251 250 50 64 61 3 1320 997.455 0.0004 1.80 0.778 3.5 134 256 250 51 65 60 2 1325 1,001.240 0.0004 1.80 0.778 3.5 140 260 250 52 65 59 1 1330 1,005.098 0.0004 1.80 0.778 3.5 141 263 250 53 65 58 3-6 1400 1,008.990 0.0004 1.80 0.778 3.5 112 244 250 49 67 63

5 1405 1,013.005 0.0004 1.80 0.778 3.5 130 240 251 51 67 63 4 1410 1,016.785 0.0004 1.80 0.778 3.5 133 259 254 52 66 61 3 1415 1,020.305 0.0004 1.80 0.778 3.5 133 262 254 52 66 62 2 1420 1,024.310 0.0004 1.80 0.778 3.5 134 264 249 53 68 61 1 1425 1,028.185 0.0004 1.80 0.778 3.5 138 258 250 55 68 63 2-6 1435 1,032.085 0.0004 1.80 0.778 3.5 144 260 252 60 66 63

5 1440 1,036.075 0.0004 1.80 0.778 3.5 151 262 249 57 68 63 4 1445 1,039.875 0.0004 1.80 0.778 3.5 150 259 250 51 69 63 3 1450 1,043.650 0.0004 1.80 0.778 3.5 150 265 251 51 69 64 2 1455 1,047.450 0.0004 1.80 0.778 3.5 149 259 250 50 70 64 1 1500 1,051.275 0.0004 1.80 0.778 3.5 140 259 251 51 69 65 1-6 1510 1,055.080 0.0004 1.80 0.778 3.5 169 259 255 64 66 63 5 1515 1,058.935 0.0004 1.80 0.778 3.5 148 255 250 64 67 63 4 1520 1,063.525 0.0004 1.80 0.778 3.5 147 256 248 62 69 64 3 1525 1,068.430 0.0004 1.80 0.778 3.5 146 252 248 66 69 64 2 1530 1,072.340 0.0004 1.80 0.778 3.5 147 257 249 67 69 63 1 1535 1,076.225 0.0004 1.80 0.778 3.5 151 260 252 68 70 63

## Example Calculations Run Number Pb 29.05 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 15.6 Water weight gain Ds 0 

### m. StackDiameter Pm 1.79 "H20 Meterpressure As 518,400.0 Sq in. StackArea Avg**~** 

### P 0.000 "H20 Differential pressure Dn = 1.5 in Nozzle Diameter Avg Sqrt**~** 

### P 0.020 "H20 SqrtDiff. press. Tt 120 %C02 0.40 Carbon Dioxide %CO = 0.00 %02 20.50 Oxygen

Vm 93.717 acf Ps 0.10 "H20 Tm 64.5 (F) Ts 142.5 (F)

Vmstd = 17.65 * Vm * [ Pb +

# 1~] Tm(R) %N2 79.10 96.547 (acf* Y) Dry Gas Volume 29.06 "Hg StackPressure 524.5 (R) Meter Temperature 602.5 (R) Stack Temperature

[ 1.79 ]= = 17.65 * 96.547 * _29_.0_5--=-::+:"7""::_13_._6_ 524.5

Vwgas = 0.0471 * Vw = 0.0471 * 15.6 = 0.7348 sft 3 

### min Sample Time Carbon Monoxide Nitrogen

94.809 sft j



### 1.580 sc:fin

Bws= Vwgas Bws* 100 = 0.77 

### % Moist. Md = 28.884 Vmstd + Vwgas

Ts (R) 

### Vs= 5129.4 * Cp * \Ps * Mw

5129.4 * 0.84 1-Bws = 0.9923

* sqrt**~** 

### P 602.5 29.06 * 28.800 * MW = 28.800

0.020 = 73.1 fpm 1.22 

## ==== =====
ACFM= Vs *As 144 73.1 * 518400.0 144 263,160 ACFM fps

DSCFM = ACFM * 528 * Ps 

# *(1-Bws) Ts (R) * 29.92 263,160 * 528 * 29.06 * 0.9923 602.5 * 29.92 222,266 DSCFM



### % lso.

## = 1039 * Vmstd * Ts (R) (1-Bws) * Ps * 

### Tt * Vs * (Dn)A2 1,039 * 94.809 * 602.5 0.9923 * 29.06 * 120 * 73.1 * 2.25000 104.3 %

# TEST, Inc. HCI Sampling Data Project # TI1550



## ------- Plant Felman Productions LLC Unit/Stack Baghouse #5 

# I Comments:



### Meter Box # 2010 Meter Cal. (Y) 1.0203 Pitot Cal. (Cp) 0.84



# --- %C02 0.40



## --- %02 20.40 %CO



## --- Operator br Nozzle # %N2 79.20



## --- Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist% 2.00



## --- ---- Date 3/15113 Stack Dia.(in.) Final Moist.% 1.07



# --- Imp. 1 2 3 4 5 Sample Time 120 Static Press.("H20) Final Isokinetic% 100.6 6



## -------- ---- Min/pt 5 Bar. Press. ("Hg) 29.05 

### Initial Leak Rate 0.0018 cfin@ Filter# Leak Check Vol. Final Leak Rate 0.001 cfm@ Dry Gas Pitot Orifice Vacuu Stack Probe Filter Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Point 1655 699.707 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F)

3-8 1700 703.302 0.0004 1.70 0.766 5.0 122 265 264

7 1705 707.406 0.0004 1.80 0.786 5.0 120 255 252 6 1710 710.804 0.0004 1.80 0.786 5.0 122 252 250 5 1715 714.507 0.0004 1.80 0.786 5.0 120 262 252 4 1720 718.307 0.0004 1.80 0.786 5.0 124 253 250 3 1725 722.000 0.0004 1.80 0.786 5.0 126 249 248 2 1730 0.308 0.0004 1.80 0.786 5.0 130 255 250 1 1735 726.102 0.0004 1.80 0.786 5.0 131 248 250 2-8 1745 730.004 0.0004 1.80 0.786 5.0 133 254 251

7 1750 733.908 0.0004 1.80 0.786 5.0 134 252 251 6 1755 737.904 0.0004 1.80 0.786 5.0 133 249 250 5 1800 741.809 0.0004 1.80 0.786 5.0 128 249 250 4 1805 745.804 0.0004 1.80 0.786 5.0 127 248 250 3 1810 749.708 0.0004 1.80 0.786 5.0 132 251 250 2 1815 753.706 0.0004 1.80 0.786 5.0 146 249 251 1 1820 757.908 0.0004 1.80 0.786 5.0 147 249 251 3-8 1830 761.701 0.0004 1.80 0.786 5.0 136 256 251

7 1835 765.603 0.0004 1.80 0.786 5.0 135 250 250 6 1840 769.508 0.0004 1.80 0.786 5.0 137 248 251 5 1845 776.407 0.0004 1.80 0.786 5.0 140 247 248 4 1850 781.404 0.0004 1.80 0.786 5.0 137 249 250 3 1855 785.308 0.0004 1.80 0.786 5.0 143 249 250 2 1900 789.303 0.0004 1.80 0.786 5.0 142 248 251 1 1905 793.287 0.0004 1.80 0.786 5.0 146 253 250 Initial Final 702.7 692.1 712.5 721.9 611.6 614.5 890.6 910

10 "Hg 10 "Hg Imp. 

### Dry 

### Gas Temp. 

### Temp.

(F) 

### In Out 53 79 72 49 

### 78 76 483 73 71 47 71 70 49 72 70 51 72 71 51 75 73 50 73 71 54 76 72 54 76 74 56 77 76 57 74 72 57 72 70 56 77 76 62 81 80 65 83 82 61 76 74 60 78 76 60 80 78 60 78 76 60 72 70 63 73 72 63 69 67 68 78 76

## Example Calculations Run Number 2 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Vw 21.1 Water weight gain Ds 0 Pm 1.8 "H20 Meter pressure As 518,400.0 Avg**~!!.** 

### P 0.000 "H20 Differential pressure On 1.5 Avg Sqrt**~!!.** 

### P 0.020 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen

Vm 93.58 acf Ps 0.00 "H20 Tm 74.5 (F) Ts 133.0 (F)

Vmstd = 17.65 *Vm * [ Pb 

### +

# 1~] Tm(R) %N2 79.20 95.48 (acf* Y) Dry Gas Volume 29.05 "Hg Stack Pressure 534.5 (R) Meter Temperature

593 (R) Stack Temperature

# ~ 17.65 • 95.480 • [ 

## LID! 

# ]= 29.05 

### + 13.6

- 534.5

Vwgas = 0.0471 *Vw = 0.0471 * 21.1 0.9938 sft 3 

### Pitot Cal 

### m. Stack Diameter Sq in. Stack Area 

### m Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

92.009 sft 5



### 1.533 scfm

Bws= Vwgas Bws* 100 = 1.07 % Moist. Md = 28.880 Vmstd 

### +Vwgas

Vs= 5129.4 *

5129.4 * Ts(R) \Ps 

## *Mw

0.84 1-Bws = 0.9893

* sqrt**~!!.** 

### P 593 29.05 * 28.764 * ===== 

### MW = 28.764 =====



### 0.020 

## ===7=2.=6=fpm ===== 

### 1.2

ACFM= Vs *As 144 72.6 * 518400.0 144 261,360 ACFM fps

DSCFM= ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 261,360 * 528 * 29.05 * 0.9893 223,527 DSCFM

%Iso.= 1039 *Vmstd *Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (Dn)"2 1,039 * 92.009 0.9893 * 29.05 * 120 593 * 29.92



## * 593 100.6 % 

## * 72.6 * 2.25000

# TEST, Inc. 

# I Comments: 

## HCI Sampling Data Project# TI1550 Meter Box# 2010 %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0203 %02 20.40 1 701 689.4 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 711.3 721.5

Operator br Nozzle# %N2 79.20 3 613 615.9 Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 910 926.6

Date 3/15/13 Stack Dia.(in.) Final Moist. % 0.92 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 95.8 6 

### Min/pt 5 Bar. Press. ("Hg) 28.95 

### Initial Leak Rate 

### 0 cfm@ 10 "Hg Filter# Leak Check Vol. Final Leak Rate 0 cfm@ 10 

### "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry 

### Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 1955 795.601 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out

2-8 2000 799.604 0.0004 1.80 0.780 5.0 121 255 259 65 70 68

7 2005 803.402 0.0004 1.80 0.780 5.0 120 245 250 67 

### 69 67 6 2010 807.305 0.0004 1.80 0.780 5.0 120 247 248 63 68 66 5 2015 811.206 0.0004 1.80 0.780 5.0 121 251 250 58 70 68 4 2020 815.108 0.0004 1.80 0.780 5.0 121 252 252 56 70 69 3 2025 819.106 0.0004 1.80 0.780 5.0 120 250 249 53 69 67 2 2030 823.007 0.0004 1.80 0.780 5.0 121 249 252 

### 53 67 65 1 2035 826.907 0.0004 1.80 0.780 5.0 121 253 249 56 69 67 4-8 2045 830.902 0.0004 1.80 0.780 5.0 136 251 250 55 69 68

7 2050 834.608 0.0004 1.80 0.780 5.0 142 251 250 56 66 64 6 2055 838.506 0.0004 1.70 0.766 5.0 146 250 253 59 70 68 5 2100 842.105 0.0004 1.70 0.766 5.0 147 251 250 58 67 65 4 2105 846.002 0.0005 1.70 0.766 5.0 144 251 250 59 68 66 3 2110 849.803 0.0005 1.70 0.766 5.0 150 250 249 57 65 63 2 2115 853.503 0.0005 1.70 0.766 5.0 142 250 250 58 66 64 1 2120 857.304 0.0005 1.70 0.766 5.0 143 248 251 58 64 63 6-8 2130 861.008 0.0005 1.70 0.766 5.0 149 253 249 54 64 62

7 2135 864.903 0.0005 1.70 0.766 5.0 150 249 250 54 63 61 6 2140 868.705 0.0005 1.70 0.766 5.0 150 250 250 55 64 63 5 2145 872.404 0.0005 1.70 0.766 5.0 137 251 251 58 64 62 4 2150 876.201 0.0005 1.70 0.766 5.0 147 249 251 60 65 64 3 2155 880.004 0.0005 1.70 0.766 5.0 150 250 249 57 66 65 2 2200 883.806 0.0005 1.70 0.766 5.0 150 251 250 55 64 62 1 2205 887.603 0.0005 1.70 0.766 5.0 149 250 250 55 65 63

## Example Calculations Run Number 3 Ph 28.95 "Hg Barometric Pressure Cp 0.84 Vw 18.1 Water weight gain Ds 0 Pm 1.74 "H20 Meter pressure As 518,400.0 Avg !J.. 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt !J.. 

### P 0.021 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen

Vm 92.002 acf Ps 0.10 "H20 Tm 65.9 (F) Ts 137.4 (F)

Vmstd = 17.65 *Vm * [ Ph+

# 1~] Tm(R) %N2 79.20 93.87 (acf* Y) Dry Gas 

### Volume 28.96 "Hg Stack Pressure 525.9 (R) Meter Temperature 597.4 (R) Stack Temperature

= 17.65 * 93.870 *[ 28.95 +

# ~ ]= 525.9

Vwgas = 0.0471 *Vw = 0.0471 * 18.1 0.8525 sft 3 

### Pitot Cal in. Stack Diameter Sq in. Stack Area in Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

91.608 sft j



### 1.527 scfm

Bws= Vwgas Bws* 100 = 0.92 % Moist. Md = 28.880 Vmstd + Vwgas

Ts (R) 

### Vs=5129.4*Cp* \Ps*Mw

5129.4 * 0.84 ==== ===== 

### 1-Bws = 0.9908 MW = 28.780 =====



### * sqrt !J.. 

### P 597.4 28.96 * 28.780 * 1.3 fps 0.021 ===7=6.=6=fpm =====


### ACFM= Vs *As 144 76.6 * 518400.0 

### = 275,760 ACFM 144

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 275,760 * 528 * 28.96 * 0.9908 597.4 * 29.92

% 

### Iso.= 1039 * Vmstd *Ts (R) (1-Bws) *Ps * Tt 

### * Vs * (Dn)"2 1,039 * 91.608 * 597.4 0.9908 * 28.96 * 120 * 76.6 * 2.25000 95.8 % 233,735 DSCFM

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #5 PROJECT #: TI1550

Run Number 1 2 3 Date 3/13/13 3/13/13 3/13/13 Time 845

- 1300 845- 1255 1410

- 1820 0 = Sample time 240 240 240 minutes Ph = Barometric Pressure at Port Elevation 29.10 29.10 29.25 in. Hg Vm =Vol. ofMetered Gas- meter cond., cal corr. 198.921 206.331 197.059 cu. ft. Tm =MeterTemperature 45.4 59.2 46.5 Farenheit Tm =MeterTemperature 505.4 519.2 506.5 Rankine Po = Meter Orifice Pressure 2.09 2.25 2.00 in. H20 Pma =MeterPressure Absolute 29.25 29.27 29.40 in. Hg Vtwet =Sampled Gas Volume Wet 234.685 235.074 228.606 cu. ft. Vtstd = Sampled Gas Volume at Stand. Cond., dry 203.222 205.272 201.867 cu.ft Vtstd = Sampled Gas Volume at Stand. Cond., dry 5.755 5.813 5.716 cu. Meter C02 =%C02, dry 0.30 0.30 0.30 % 02 =% 02, dry 20.60 20.60 20.50 % 

# co =%CO, dry 0.00 0.00 0.00 % N2 = %N2,dry (N2+CO) = 1OO-(C02+02) 79.10 79.10 79.20 % EA =Excess Air 5,698.5 5,698.5 4,200.8 % Vw = Volume Water 32.5 31.2 23.9 grams H20 =mgas 0.75 0.71 0.55 % H20 = Moisture in Gas at Saturation 14.99 13.19 12.22 % Md =DryMolecular Weight ofStack Gas 28.87 28.87 28.87 Mw = Wet Molecular Weight ofStack Gas 28.79 28.80 28.81 Psg = Stack Pressure, gauge - measured 0.10 0.10 0.10 in. H20 Psa =StackPressure, absolute 29.11 29.11 29.26 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC Baghouse #5 UNIT: 

## PROJECT#: TI1550

Run Number Ts =StackTemperature Ts =StackTemperature Ts =StackTemperature \18 p 

### = Avg. Sum. ofPressure Square Root

Vs = Velocity in the Stack Vs = Velocity in the Stack As = Effective Stack Area Qa = Volumetric FlowRate at stack cond. Qs = Volumetric FlowRate, stand. cond., dry IR = Isokinetic Ratio (Vn!Vs)*IOO Mn = Particulate Matter Catch, grams

= Particulate Matter Catch, milligrams Ca = Particulate Matter Cone.

- Stack Cond. Cs = Particulate Matter Cone.

- Dry Std. Cond.

= Particulate MatterEmissions * ER = Particulate Matter Emissions 1 128.90 326.83 588.9 0.022 79.5 1.33 518,400.0

286,200 247,784

100.3 0.0035 3500.00 0.0003 0.0003 608.17

0.64 2 3 124.20 121.60 324.22 322.78 584.2 581.6 0.022 0.022 79.1 78.7 1.30 1.30 518,400.0 518,400.0

284,760 283,320 248,621 250,152

100.9 98.6 0.0051 0.0049 5133.33 4900.00 0.0003 0.0004 0.0004 0.0004 883.08 857.24

0.85 0.86 Farenheit Kelvin Rankine

ft/min ft/sec sq. m. acfm dscfm % 

### grams ug gr/acf gr/dscf ug/dscm lbs/hr

# TEST, Inc.**~Comments:** Particulate/Metals Sampling Data L...----------------------l Project # TI1550 Meter Box# 2010 MST %C020.30 Imp. Initial Final



### ----- Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.60 1 716.1 681.4 Unit/Stack Baghouse #5 Pitot Cal. (Cp)_0_.8_4

__ %CO



## ----- 2 717.4 745.3

Operator SM Nozzle # %N2 79.10 3 600.2 605



## --- Run# 1 Nozzle Dia. (in.) 1.5 Assumed Moist% 1.17 4 851.3 885.8



### ----- ----- Date 3/13/13 Stack Dia.(in.) Final Moist.% 0.75 5



## ----- Sample Time 240 Static Press.("H20) 0.10 Final Isokinetic % 100.3 6



# --- Min/pt 5 Bar. Press. ("Hg) 29.10 Initial LeakRate 0 cfm@ 11 "Hg



## --- Filter# 1012 Leak Check Vol. Final Leak Rate 0.001 cfm@ 12 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 845 315.475 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 4-6 850 319.520 0.0005 2.10 0.832 3.5 131 258 251 66 41 41

6 855 323.640 0.0005 2.10 0.832 3.5 132 255 252 52 

### 44 43 5 900 327.705 0.0005 2.10 0.832 3.5 130 256 248 54 45 44 5 905 331.800 0.0005 2.10 0.832 3.5 135 256 245 53 46 45 4 910 335.885 0.0005 2.10 0.832 3.5 124 258 248 54 46 46 4 915 339.915 0.0005 2.10 0.832 3.5 120 259 250 54 47 46 3 920 343.590 0.0005 2.10 0.832 3.5 123 259 251 57 46 45 3 925 347.700 0.0005 2.10 0.832 3.5 118 255 248 57 46 45 2 930 351.795 0.0005 2.10 0.832 3.5 122 254 250 58 46 46 2 935 355.910 0.0005 2.10 0.832 3.5 122 259 252 58 46 46 1 940 360.000 0.0005 2.10 0.832 3.5 122 255 247 59 47 46 I 945 363.835 0.0005 2.10 0.832 3.5 127 264 251 60 47 45 3-6 955 367.905 0.0005 2.10 0.832 3.5 126 260 249 60 45 45

6 1000 371.820 0.0005 2.10 0.832 3.5 119 255 250 57 47 46 5 1005 376.090 0.0005 2.10 0.832 4.0 125 254 247 59 47 46 5 1010 380.155 0.0005 2.10 0.832 4.0 124 252 250 59 48 46 4 1015 384.210 0.0005 2.10 0.832 4.0 126 256 248 59 45 45 4 1020 388.250 0.0005 2.10 0.832 4.0 128 259 252 55 47 47 3 1025 392.225 0.0005 2.10 0.832 4.0 125 265 251 58 46 46 3 1030 396.235 0.0005 2.10 0.832 4.0 123 253 248 57 47 47 2 1035 400.270 0.0005 2.10 0.832 4.0 127 255 250 58 47 46 2 1040 404.325 0.0005 2.10 0.832 4.0 126 261 250 56 47 47 1 1045 408.400 0.0005 2.10 0.832 4.0 127 261 250 54 47 47 I 1050 412.590 0.0005 2.10 0.832 4.0 128 258 249 55 48 48 2-6 1100 416.615 0.0005 2.10 0.832 4.0 137 256 248 52 48 47

6 1105 420.650 0.0005 2.10 0.832 4.0 144 255 249 52 48 

### 48 5 IllO 424.700 0.0005 2.10 0.832 4.0 127 258 251 51 48 47 5 1II5 428.770 0.0005 2.10 0.832 4.0 132 258 250 51 47 47 4 1120 432.855 0.0005 2.10 0.832 4.0 147 258 255 52 47 46 4 1125 436.925 0.0005 2.10 0.832 4.0 146 258 251 52 47 47 3 1130 441.010 0.0005 2.10 0.832 4.0 136 265 252 52 48 47

## Example Calculations Run Number 1 Ph 29.10 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 32.5 Water weight gain Ds 0 m. Stack Diameter Pm 2.09 "H20 Meter pressure As 518,400.0 Sq in. Stack Area Avg 11 

### P 0.001 "H20 Differential pressure Dn 1.5 m Nozzle Diameter Avg Sqrt 11 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 240 mm Sample Time %C02 0.30 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.60 Oxygen

Vm 193.09 acf Ps 0.10 "H20 Tm 45.4 (F) Ts 128.9 (F)

Vmstd = 17.65 * Vm * [Ph+

# 1~] Tm(R) 198.921 (acf* Y) 29.11 "Hg 505.4 (R) 588.9 (R)

= 17.65 * 198.921 %N2 79.10 Nitrogen Dry Gas Volume Stack Pressure Meter Temperature Stack Temperature

[ 2.09 * 29.10 + 13.6 505.4 

# J = 203.222 sft j 

### 3.387 scfm

Vwgas = 0.0471 *Vw 

### = 0.0471 * 32.5 1.5308 sft 3



### Bws= Vwgas Vmstd + Vwgas

Ts(R) Vs= 5129.4 * Cp * \Ps *Mw

5129.4 * 0.84 Bws*100 

### = 0.75 %Moist. Md 

### = 28.872 ===== 

### 1-Bws = 0.9925 MW 

### = 28.790 =====



### * sqrt 11 

### P 588.9 29.11 * 28.790 * 0.022 = 79.5 fpm 1.33 fps ==== =====


### ACFM= Vs *As 144 79.5 * 518400.0 

### = 286,200 ACFM 144

DSCFM

### = ACFM * 528 *Ps 

# * (1-Bws) Ts (R) * 29.92 286,200 * 528 * 29.11 * 0.9925 588.9 * 29.92

% 

### Iso.= 1039 * Vmstd * Ts (R) (1-Bws) *Ps * Tt 

### * Vs * (Dn)"2 1,039 * 203.222 * 588.9 0.9925 * 29.11 

## * 240 

## * 79.5 

## * 2.25000 = 100.3 % 247,784 DSCFM

# TEST, Inc. 

# I Comments: 

## Particulate/Metals Sampling Data Project# TI1550 Meter Box# 2010 %C020.30 Imp. Initial Final Plant Felman Productions LLC MeterCal. (Y) 1.0203 %02 20.60 1 714.7 693.3 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 718.2 736.9

Operator br Nozzle# %N2 79.10 3 622.6 627.2 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % 1.80 4 890 919.3

Date 3/13/13 Stack Dia.(in.) Final Moist.% 0.71 5 Sample Time 240 Static Press.("H20) 0.10 Final Isokinetic % 100.9 6 

### Minlpt 5 Bar. Press. ("Hg) 29.10 

### Initial Leak Rate 0.01 cfm@ 18 "Hg Filter# 1011 Leak Check Vol. Final LeakRate 0.01 cfm@ 19 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 845 315.581 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out

7-8 850 319.805 0.0005 2.25 0.832 2.0 133 250 220 62 63 64

8 855 324.304 0.0005 2.25 0.832 2.0 132 250 230 64 

### 62 63 7 900 328.505 0.0005 2.25 0.832 2.0 130 250 245 64 62 63 7 905 332.808 0.0005 2.25 0.832 2.0 126 247 252 66 62 63 6 910 337.203 0.0005 2.25 0.832 2.0 127 251 255 47 61 62 6 915 341.602 0.0005 2.25 0.832 2.0 129 253 254 49 61 63 5 920 345.902 0.0005 2.25 0.832 2.0 131 247 252 62 61 63 5 925 350.203 0.0005 2.25 0.832 2.0 130 246 250 60 60 62 4 930 354.601 0.0005 2.25 0.832 2.0 132 251 251 61 59 61 4 935 359.203 0.0005 2.25 0.832 2.0 130 250 251 65 58 60 3 940 363.506 0.0005 2.25 0.832 2.0 127 250 248 62 57 59 3 945 367.805 0.0005 2.25 0.832 2.0 124 254 248 64 56 59 2 950 372.203 0.0005 2.25 0.832 2.0 122 246 250 57 56 59 2 955 376.702 0.0005 2.25 0.832 2.0 126 252 251 59 57 59 1 1000 380.908 0.0005 2.25 0.832 2.0 127 250 252 59 57 59 1 1005 384.704 0.0005 2.25 0.832 2.0 129 250 250 60 58 59 6-8 1015 388.706 0.0005 2.25 0.848 2.1 126 249 231 60 59 59

8 1020 392.607 0.0005 2.25 0.848 2.1 126 250 248 64 59 59 7 1025 396.509 0.0005 2.25 0.848 2.1 124 250 252 66 60 60 7 1030 400.703 0.0005 2.25 0.848 2.1 124 250 254 66 61 60 6 1035 404.904 0.0005 2.25 0.848 2.1 122 250 251 63 62 61 6 1040 409.108 0.0005 2.25 0.848 2.1 123 251 250 66 64 63 5 1045 413.307 0.0005 2.25 0.848 2.1 121 248 249 66 67 64 5 1050 417.508 0.0005 2.25 0.848 2.1 120 249 250 66 67 65 4 1055 421.802 0.0005 2.25 0.848 2.1 122 250 250 65 68 66 4 1100 426.108 0.0005 2.25 0.848 2.1 122 248 250 66 69 67 3 1105 430.208 0.0005 2.25 0.848 2.1 123 251 250 66 63 67 3 1110 434.503 0.0005 2.25 0.848 2.1 120 247 251 65 

### 65 66 2 1115 438.808 0.0005 2.25 0.848 2.1 121 253 247 66 62 64 2 1120 443.105 0.0005 2.25 0.848 2.1 120 247 249 67 53 65 1 1125 447.202 0.0005 2.25 0.848 2.1 120 250 250 67 54 66

## Example Calculations Run Number 2 Ph 29.10 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 31.2 Water weight gain Ds 0 m. 

### Stack Diameter Pm 2.25 "H20 Meter pressure As 518,400.0 Sq in. Stack Area Avg L\ 

### P 0.001 "H20 Differential pressure Dn 1.5 m 

### Nozzle Diameter Avg Sqrt L\ 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 240 min Sample Time %C02 0.30 Carbon Dioxide %CO = 0.00 Carbon Monoxide %02 20.60 Oxygen

Vm 202.226 acf Ps 0.10 "H20 Tm 59.2 (F) Ts 124.2 (F)

Vmstd = 17.65 * Vm * [ Ph+

# 1~] Tm(R) %N2 = 79.10 206.331 (acf* Y) 

### Dry Gas Volume

29.11 "Hg Stack Pressure 519.2 (R) Meter Temperature 584.2 (R) Stack Temperature

# ~ 17.65 • 206.331 • [

# ~ ]-- 29.10 + 13.6 519.2 Nitrogen

205.272 sft j



### 3.421 scfm

Vwgas = 0.0471 * Vw = 0.0471 * 31.2 1.4695 sft 3



### Bws= Vwgas Vmstd + Vwgas

Vs = 5129.4 *

5129.4 * Ts(R) \Ps 

## *Mw

0.84 Bws*100 = 0.71 %Moist. Md = 28.872 ===== 

### 1-Bws = 0.9929 MW = 28.795 =====



### * sqrt L\ 

### P 584.2 29.11 * 28.795 * 0.022 79.1 fpm 1.3 ==== =====


### ACFM= Vs *As 144 79.1 * 518400.0 144 284,760 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 284,760 * 528 * 29.11 * 0.9929 584.2 * 29.92 248,621 DSCFM

% 

### Iso.= 1039 * Vmstd *Ts (R) (1-Bws) *Ps * Tt 

### * Vs * (DnY'2 1,039 * 205.272 * 584.2 0.9929 * 29.11 * 240 * 79.1 * 2.25000 100.9 %

# TEST, Inc. 

# I Comments: 

## Particulate/Metals Sampling Data Project# Tl1550 Meter Box# 2010 MST %C020.30 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.50 1 706.8 676 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 715.9 732.7

Operator SM Nozzle# %N2 79.20 3 611 614.7 Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 874.7 908.9

Date 3/13/13 Stack Dia.(in.) 0 Final Moist. % 0.55 5 Sample Time 240 Static Press.("H20) 0.10 Final Isokinetic % 98.6 6 

### Min/pt 5 Bar. Press. ("Hg) 29.25 

### Initial Leak Rate 

### 0 cfm@ 10 "Hg Filter# 1010 Leak Check Vol. Final Leak Rate 0 cfm@ 5 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 1410 509.521 ("H20) ("H20) (cfm) ("Hg.) 

### (F) (F) (F) (F) 

### In Out

6-8 1415 513.555 0.0005 2.00 0.814 2.5 128 238 239 58 43 42

8 1420 517.505 0.0005 2.00 0.814 2.5 126 248 249 58 44 43 7 1425 521.435 0.0005 2.00 0.814 2.5 132 260 247 54 45 44 7 1430 525.400 0.0005 2.00 0.814 2.5 131 258 252 54 44 44 6 1435 529.355 0.0005 2.00 0.814 2.5 130 259 247 56 45 44 6 1440 533.320 0.0005 2.00 0.814 2.5 131 257 248 58 45 45 5 1445 537.300 0.0005 2.00 0.814 2.5 121 255 248 

### 59 45 44 5 1450 541.265 0.0005 2.00 0.814 2.5 122 259 250 60 46 44 4 1455 545.200 0.0005 2.00 0.814 2.5 131 257 249 61 47 45 4 1500 549.150 0.0005 2.00 0.814 2.5 144 254 248 61 46 45 3 1505 554.510 0.0005 2.00 0.814 2.5 144 258 250 61 46 43 3 1510 558.105 0.0005 2.00 0.814 2.5 137 255 249 61 47 45 2 1515 562.105 0.0005 2.00 0.814 2.5 140 230 235 57 51 50 2 1520 566.030 0.0005 2.00 0.814 2.5 138 248 247 59 52 54 1 1525 570.080 0.0005 2.00 0.814 2.5 130 259 250 57 52 50 1 1530 573.903 0.0005 2.00 0.814 2.5 137 259 248 59 51 49 4-8 1540 577.900 0.0005 2.00 0.814 2.5 126 258 249 52 47 44

8 1545 581.990 0.0005 2.00 0.814 2.5 129 258 251 51 49 47 7 1550 585.820 0.0005 2.00 0.814 2.5 133 262 249 52 49 46 7 1555 589.960 0.0005 2.00 0.814 2.5 136 263 250 53 50 47 6 1600 593.706 0.0005 2.00 0.814 2.5 125 226 238 55 47 45 6 1605 597.803 0.0005 2.00 0.814 2.5 111 270 240 54 50 48 5 1610 601.803 0.0005 2.00 0.814 2.5 114 263 250 55 53 50 5 1615 605.610 0.0005 2.00 0.814 2.5 119 261 251 57 51 48 4 1620 610.504 0.0005 2.00 0.814 2.5 119 254 249 58 50 47 4 1625 613.502 0.0005 2.00 0.814 2.5 112 262 247 57 47 45 3 1630 617.406 0.0005 2.00 0.814 2.5 117 251 250 59 46 44 3 1635 621.309 0.0005 2.00 0.814 2.5 111 259 248 61 46 44 2 1640 625.202 0.0005 2.00 0.814 2.5 113 259 250 58 47 46 2 1645 629.201 0.0005 2.00 0.814 2.5 109 262 250 57 48 45 I 

### 1650 633.104 0.0005 2.00 0.814 2.5 112 261 248 58 49 47

## Example Calculations Run Number 3 Pb 29.25 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 23.9 Water weight gain Ds 0 10. Stack Diameter Pm 2 "H20 Meter pressure As 518,400.0 Sq in. Stack Area Avg Ll 

### P 0.001 "H20 Differential pressure Dn 1.5 10 Nozzle Diameter Avg Sqrt L1 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 240 m10 Sample Time %C02 0.30 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.50 Oxygen %N2 79.20 Nitrogen

Vm 191.282 acf 197.059 (acf* Y) Dry Gas Volume Ps 0.10 "H20 29.26 "Hg Stack Pressure Tm 46.5 (F) 506.5 (R) Meter Temperature Ts 121.6 (F) 581.6 (R) Stack Temperature

17.65 

## *Vm 

## * [ Pb+

# I~

# J
• 197.059 • [ 2.00 

# } Vmstd = = 17.65 29.25 

### + 13.6 201.867 sft j 

### Tm(R) 506.5 3.364 scfm

Vwgas = 0.0471 * Vw = 0.0471 * 23.9 1.1257 sft 3



### Bws= Vwgas Vmstd 

### +Vwgas

Ts(R) Vs= 5129.4 * Cp * \Ps * Mw

5129.4 * 0.84 Bws*100 = 0.55 %Moist. Md = 28.868 ===== 

### 1-Bws = 0.9945 MW = 28.808 =====



### * sqrt Ll 

### P 581.6 29.26 * 28.808 * 0.022 = 78.7 fpm 1.3 

## ==== =====
ACFM= Vs *As 144 78.7 * 518400.0 144 283,320 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 283,320 * 528 * 29.26 * 0.9945 250,152 DSCFM



### % Iso. 

## = 1039 *Vmstd * Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (Dn)"2 1,039 * 201.867 0.9945 * 29.26 * 240 581.6 * 29.92



## * 581.6 98.6 % 

# * 78.7 * 2.25000

# CALCULATION SUMMARY SHEET
PLANT: FelmanProductions LLC Baghouse #5 UNIT: PROJECT#: TI1550

Run Number Date Time 0 = Sample time Ph = Barometric Pressure at Port Elevation Vm = Vol. ofMetered Gas

- meter cond., cal corr. Tm =MeterTemperature Tm =MeterTemperature Po = Meter Orifice Pressure Pma =MeterPressure Absolute Vtwet =Sampled Gas Volume Wet Vtstd = Sampled Gas Volume at Stand. Cond., dry Vtstd = Sampled Gas Volume at Stand. Cond., dry 

### C02 =% C02, dry 

### 02 =% 02, dry 

# co =%CO, dry 

### N2 = %N2,dry (N2+CO) = 1 OO-(C02+02) EA =ExcessAir Vw =Volume Water H20 =mgas H20 = Moisture in Gas at Saturation Md =Dry Molecular Weight ofStack Gas Mw = Wet Molecular Weight ofStack Gas Psg = Stack Pressure, gauge - measured Psa = Stack Pressure, absolute 1 3/15/13 755

- 1010 120 29.45 89.005

56.4 516.4

1.60 29.57 103.505 89.948 2.547 0.40 20.50 0.00 79.10 4,442.0

17.2 0.89 16.52 28.88 28.79 0.10 29.46 2 3 3/15/13 3/15/13 1330- 1540 1700

- 1915 120 120 29.05 28.95 94.225 93.460

70.9 71.2 530.9 531.2

1.75 1.80 29.18 29.08 106.702 109.487 91.404 90.311 2.588 2.557 0.40 0.40 20.50 20.40 0.00 0.00 79.10 79.20 4,442.0 3,469.4

18.5 21.5 0.94 1.11 16.79 27.82 28.88 28.88 28.78 28.76 0.10 0.10 29.06 28.96 minutes in. Hg
cu. ft. Farenheit Rankine in. H20 in. Hg
cu. ft. cu.ft
cu. Meter % % % % % grams % %

in. H20 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #5 PROJECT#: TI1550

RunNumber 1 2 3 Ts =StackTemperature 133.00 133.10 152.80 Farenheit Ts =StackTemperature 329.11 329.17 340.11 Kelvin Ts =StackTemperature 593 593.1 612.8 Rankine**\I~** 

### P = Avg. Sum. ofPressure Square Root 0.02 0.02 0.02 Vs = Velocity inthe Stack 72.1 72.6 73.9 ft/min Vs = Velocity inthe Stack 1.20 1.20 1.20 ftlsec As = Effective StackArea 518,400.0 518,400.0 518,400.0 sq.m. Qa = Volumetric Flow Rate at stack cond. 259,560 261,360 266,040 acfm Qs = Volumetric FlowRate, stand. cond., dry 225,531 223,860 219,407 dscfm IR = Isokinetic Ratio (Vn/Vs)*100 97.5 99.8 100.6 %

# TEST, Inc. 

# I Comments: 

## Trap #7 Dioxin/Furans/PCB's Sampling Data Project# TI1550 Meter Box# 2010 mst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.50 1 339.8 339.9 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 709 709.8

Operator br Nozzle# %N2 79.10 3 622.6 623.7 Run# 1 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 906.9 922.1

Date 3/15/13 Stack Dia.(in.) Final Moist. % 0.89 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 97.5 6 Min/pt 5 Bar. Press. ("Hg) 29.45 Initial Leak Rate 

### 0.002 cfm@ 10 "Hg Filter#

---- Leak Check Vol. Final Leak Rate 0.002 cfm@ 12 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 755 879.705 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 4-6 800 883.575 0.0004 1.60 0.737 5.0 123 252 251 68 48 47

5 805 886.805 0.0004 1.60 0.737 5.0 127 253 250 67 

### 51 50 4 810 890.435 0.0004 1.60 0.737 5.0 123 263 249 64 52 50 3 815 894.050 0.0004 1.60 0.737 5.0 120 266 249 66 53 53 2 820 897.680 0.0004 1.60 0.737 5.0 125 257 246 68 54 53 1 825 901.290 0.0004 1.60 0.737 5.0 133 257 250 68 56 54 3-6 835 904.980 0.0004 1.60 0.737 5.0 126 267 251 68 49 51

5 840 908.480 0.0004 1.60 0.737 5.0 128 255 246 68 57 55 4 845 912.001 0.0004 1.60 0.737 5.0 129 258 253 68 57 54 3 850 915.604 0.0004 1.60 0.737 5.0 131 263 248 67 57 55 2 855 919.005 0.0004 1.60 0.737 5.0 124 256 253 67 54 52 I 900 922.505 0.0004 1.60 0.737 5.0 127 258 250 39 58 56 2-6 910 926.007 0.0004 1.60 0.737 5.0 142 254 245 43 58 55

5 915 929.609 0.0004 1.60 0.737 5.0 128 267 248 45 61 60 4 920 933.075 0.0004 1.60 0.737 5.0 127 263 249 46 61 59 3 925 936.608 0.0004 1.60 0.737 5.0 131 261 248 47 61 60 2 930 940.303 0.0004 1.60 0.737 5.0 133 260 248 49 60 57 I 935 944.009 0.0004 1.60 0.737 5.0 153 254 257 51 61 60 I-6 945 947.806 0.0004 1.60 0.737 5.0 147 260 254 49 60 58 5 950 951.304 0.0004 1.60 0.737 5.0 156 256 254 49 61 60 4 955 955.002 0.0004 1.60 0.737 5.0 138 255 247 51 61 59 3 1000 958.709 0.0004 1.60 0.737 5.0 140 260 251 52 60 58 2 1005 962.307 0.0004 1.60 0.737 5.0 136 270 251 51 6I 60 1 1010 966.I01 0.0004 1.60 0.737 5.0 144 259 250 50 6I 59

## Example Calculations Run Number Pb 29.45 "Hg Barometric Pressure Cp 0.84 Vw 17.2 Water weight gain Ds 0 Pm 1.6 "H20 Meterpressure As 518,400.0 Avg**~** 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg**Sqrt~** 

### P 0.020 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.50 Oxygen

Vm 86.396 acf Ps 0.10 "H20 Tm 56.4 (F) Ts 133.0 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm(R) %N2 79.10 89.005 (acf* Y) Dry 

### Gas Volume 29.46 "Hg Stack Pressure 516.4 (R) Meter Temperature

593 (R) Stack Temperature

# ~ 17.65 • 89.005 • [ 

### .LQQ ]-- 29.45 

### + 13.6 516.4

Vwgas = 0.0471 * Vw = 0.0471 * 17.2 0.8101 sft 3 

### Pitot Cal m. Stack Diameter Sq in. Stack Area m Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

89.948 sft j 

### 1.499 scfm

Bws= Vwgas Bws*100 = 0.89 %Moist. Md = 28.884 Vmstd 

### +Vwgas

Ts(R) Vs=5129.4*Cp* \Ps*Mw 1-Bws = 0.9911

* sqrt**~** 

### P ===== 

### MW = 28.787 =====



### 5129.4 * 0.84 

# I 593 * \ _2_9_.4_6--*--2-8-.7-8-7 * 0.020 = 72.1 fpm 1.20 tips

ACFM= Vs *As 144 72.1 * 518400.0 144

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92

0 /o 

### lso.

## = 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (DnY'2 1,039 * 89.948 ====


### 259,560 ACFM

259,560 * 528 * 29.46 * 0.9911 593 * 29.92



## * 593 97.5 % 0.9911 * 29.46 * 120 * 72.1 * 2.25000 =====



### 225,531 DSCFM

# TEST, Inc. 

# romments: Trap #8 Dioxin!Furans/PCB's Sampling Data Project# TI1550 Meter Box # 2010 mst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.50 1 333.1 334.2 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 696.7 696.4

Operator br Nozzle# %N2 79.10 3 603.7 605.3 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % 0.94 4 898.4 914.5

Date 3/15/13 Stack Dia.(in.) Final Moist. % 0.94 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 99.8 6 

### Min/pt 5 Bar. Press. ("Hg) 29.05 

### Initial Leak Rate 0.001 cfm@ 11 "Hg Filter#

---- Leak Check Vol. Final Leak Rate 0.001 cfm@ 11 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 1330 607.001 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out

3-8 1335 610.706 0.0004 1.70 0.766 5.0 137 248 256 67 74 73

7 1340 614.402 0.0004 1.70 0.766 5.0 130 255 251 68 

### 69 71 6 1345 618.106 0.0004 1.70 0.766 5.0 136 244 250 68 71 68 5 1350 621.708 0.0004 1.70 0.766 5.0 131 257 248 68 68 66 4 1355 625.407 0.0004 1.70 0.766 5.0 130 253 251 60 66 64 3 1400 629.203 0.0004 1.70 0.766 5.0 132 248 250 44 70 67 2 1405 632.806 0.0004 1.70 0.766 5.0 132 254 251 45 73 70 1 1410 636.465 0.0004 1.70 0.766 5.0 126 250 251 42 73 72 2-8 1420 640.670 0.0004 1.70 0.766 5.0 120 249 252 43 72 70

7 1425 643.809 0.0004 1.70 0.766 5.0 132 248 250 43 74 72 6 1430 647.601 0.0004 1.70 0.766 5.0 134 250 250 53 75 74 5 1435 651.409 0.0004 1.80 0.780 5.0 136 249 246 61 75 73 4 1440 655.501 0.0004 1.80 0.780 5.0 134 246 248 43 75 74 3 1445 659.608 0.0004 1.80 0.780 5.0 130 244 249 44 73 72 2 1450 663.105 0.0004 1.80 0.780 5.0 138 254 250 44 72 70 1 1455 667.001 0.0004 1.80 0.780 5.0 148 250 250 44 74 72 3-8 1505 671.004 0.0004 1.80 0.780 5.0 151 248 250 46 74 73

7 1510 674.800 0.0004 1.80 0.780 5.0 140 254 250 46 6 73 6 1515 678.603 0.0004 1.80 0.780 5.0 134 252 255 55 75 73 5 1520 682.509 0.0004 1.80 0.780 5.0 131 248 249 52 76 74 4 1525 686.506 0.0004 1.80 0.780 5.0 130 245 250 51 75 74 3 1530 690.502 0.0004 1.80 0.780 5.0 128 249 251 50 74 72 2 1535 694.508 0.0004 1.80 0.780 5.0 130 251 247 51 77 75 1 1540 698.464 0.0004 1.80 0.780 5.0 125 246 250 52 75 73

## Example Calculations Run Number 2 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Vw 18.5 Water weight gain Ds 0 Pm 1.75 "H20 Meter pressure As 518,400.0 Avg !:!.. 

### P 0.000 "H20 Differential pressure Dn 1.5 A

vg Sqrt !:!.. 

### P 0.020 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.50 Oxygen

Vm 91.463 acf Ps 0.10 "H20 Tm 70.9 (F) Ts 133.1 (F)

Vmstd =· 17.65 * Vm * [ Pb 

### +

# l~J Tm(R) %N2 79.10 94.225 (acf* Y) Dry Gas Volume 29.06 "Hg Stack Pressure 530.9 (R) Meter Temperature 593.1 (R) Stack Temperature

# ~ 17.65 • 94.225 • [ 

### ill ]-- 29.05 

### + 13.6 530.9

Vwgas = 0.0471 * Vw = 0.0471 * 18.5 0.8713 sft 3 

### Pitot Cal m. 

### Stack Diameter Sq in. Stack Area Ill 

### Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

91.404 sft j



### 1.523 scfm

Bws= Vwgas Bws*100 = 0.94 %Moist. Md = 28.884 ==== ===== Vmstd 

### +Vwgas 1-Bws = 0.9906 MW = 28.782

Vs= 5129.4 * Ts (R) 

### \Ps

# *Mw =====

* sqrt !:!.. 

### P 593.1 5129.4 * 0.84 29.06 * 28.782 * 0.020 = 72.6 fpm ===1.=2==fps

ACFM= Vs *As 144 72.6 * 518400.0 144

DSCFM= ACFM * 528 *Ps * 

### (1-Bws) Ts (R) * 29.92

0 /o 

### lso.

## = 1039 *Vmstd *Ts (R) (1-Bws) *Ps * Tt 

### * Vs * (DnY'2 1,039 * 91.404 0.9906 * 29.06 * 120 

## * 

# * ==== 

### 261,360 ACFM

261,360 * 528 * 29.06 * 0.9906 593.1 * 29.92

593.1 99.8 % 72.6 * 2.25000 223,860 DSCFM

# TEST, Inc.**~Comments:** Dioxin/Furans/PCB's Sampling Data**~--------------------------------------~** 

## Trap #6
Project# TI1550 Meter Box# 2010 MST %C02 0.40 Imp. Initial Final



## ------ Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.40 1 340 343.6 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 721 718.6



## --- 

# ------ Operator br Nozzle # %N2 79.20 3 606.7 610.5



## --- Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist% 2.00 4 922 938.5



# --- ------ Date 3/15/13 Stack Dia.(in.) 0 Final Moist.% 1.11 5



## ------ 

# ------ Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic % 100.6 6



# ------ Min/pt 

### 5 Bar. Press. ("Hg) 28.95 Initial Leak Rate 

### 0.001 cfm@ 10 "Hg Filter# Leak Check Vol. Final Leak Rate 0.001 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuo Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1700 114.158 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 2-8 1705 118.025 0.0004 1.80 0.778 5.0 151 269 249 60 69 68

7 1710 121.850 0.0004 1.80 0.778 5.0 150 251 251 57 

### 70 70 6 1715 125.675 0.0004 1.80 0.778 5.0 154 259 251 59 71 68 5 1720 129.560 0.0004 1.80 0.778 5.0 152 262 250 60 72 68 4 1725 133.500 0.0004 1.80 0.778 5.0 163 260 250 61 71 68 3 1730 137.175 0.0004 1.80 0.778 5.0 162 265 250 63 71 68 2 1735 140.975 0.0004 1.80 0.778 5.0 161 265 252 

### 63 71 68 I 

### 1740 144.843 0.0004 1.80 0.778 5.0 163 259 250 63 71 68 4-8 1750 148.650 0.0004 1.80 0.778 5.0 157 267 246 64 69 68

7 1755 152.420 0.0004 1.80 0.778 5.0 145 260 248 61 69 67 6 1800 156.210 0.0004 1.80 0.778 5.0 157 257 250 62 69 67 5 1805 160.100 0.0004 1.80 0.778 5.0 157 259 250 61 69 66 4 1810 163.765 0.0004 1.80 0.778 5.5 157 260 251 63 69 68 3 1815 167.450 0.0004 1.80 0.778 5.5 148 257 249 63 68 67 2 1820 171.300 0.0004 1.80 0.778 5.5 157 258 249 65 67 66 I 

### 1825 175.078 0.0004 1.80 0.778 5.5 146 262 250 65 67 66 2-8 1840 179.200 0.0004 1.80 0.778 5.5 150 255 248 68 71 67

7 1845 183.135 0.0004 1.80 0.778 5.5 152 256 250 66 76 68 6 1850 187.130 0.0004 1.80 0.778 5.5 152 258 250 57 80 71 5 1855 191.145 0.0004 1.80 0.778 5.5 152 256 250 53 81 72 4 1900 195.185 0.0004 1.80 0.778 5.5 135 260 249 49 83 74 3 1905 199.250 0.0004 1.80 0.778 5.5 146 257 251 48 84 75 2 1910 203.280 0.0004 1.80 0.778 5.5 150 258 253 44 83 77 I 

### 1915 204.878 0.0004 1.80 0.778 5.5 150 258 251 48 86 77

## Example Calculations Run Number 3 Pb 28.95 "Hg Barometric Pressure Cp 0.84 Vw 21.5 Water weight gain Ds 0 Pm 1.8 "H20 Meter pressure As 518,400.0 Avg**~** 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** 

### P 0.020 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen %N2 79.20

Vm 90.72 acf 93.46 (acf* Y) Dry Gas Volume Ps 0.10 "H20 28.96 "Hg Stack Pressure Tm 71.2 (F) 531.2 (R) Meter Temperature Ts 152.8 (F) 612.8 (R) Stack Temperature

Vmstd = 17.65 *Vm * [ Pb 

### +

# 1~] Tm(R)

# ~ 17.65 • 93.460 ·[

# ~ ]-- 28.95 

### + 13.6 531.2

Vwgas = 0.0471 * Vw = 0.0471 * 21.5 1.0127 sft 3 

### Pitot Cal Ill. 

### Stack Diameter Sq in. Stack Area in Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

90.311 sft j



### 1.505 scfm

Bws= Vwgas Bws* 100 = 1.11 % Moist. Md**==,.;2;;8;;.8,;;,80~=** 

### Vmstd 

### +Vwgas

Ts (R) 

### Vs=5129.4*Cp* \Ps*Mw 1-Bws = 0.9889

* sqrt**~** 

### P

5129.4 * 0.84 

# I 612.8 * \ -2-8-.9-6....::....::.=:*:..:.__2_8_. 7-5-9 * MW = 28.759 =====

0.020 = ==7=3=.9=fpm ===== 

### 1.2

ACFM= Vs *As 144 73.9 * 518400.0 144 266,040 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 266,040 * 528 * 28.96 * 0.9889 219,407 DSCFM

% lso.= 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (Dn)"'2 1,039 * 90.311 0.9889 * 28.96 * 120 612.8 * 29.92



## * 612.8 100.6 % 

## * 73.9 * 2.25000

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC Baghouse #5 UNIT: PROJECT#: TI1550

Run Number Date Time 0 = Sample time Pb = Barometric Pressure at Port Elevation Vm = Vol. ofMetered Gas

- meter cond., cal corr. Tm =MeterTemperature Tm = Meter Temperature Po = Meter Orifice Pressure Pma = Meter Pressure Absolute Vtwet =Sampled Gas Volume Wet Vtstd = Sampled Gas Volume at Stand. Cond., dry Vtstd = Sampled Gas Volume at Stand. Cond., dry C02 =%C02, dry 02 =% 02, dry 

# co =%CO, dry N2 = %N2,dry (N2+CO) = 1 OO-(C02+02) EA =ExcessAir Vw =Volume Water H20 =mgas H20 =Moisture in Gas at Saturation Md = Dry Molecular Weight ofStack Gas Mw = Wet Molecular Weight ofStack Gas Psg = Stack Pressure, gauge - measured Psa =StackPressure, absolute 1 3/14/13 930

- 1145 120 29.45 78.281

55.3 515.3

1.22 29.54 89.035 79.204 2.243 0.30 20.50 0.00 79.20 4,200.8

20.7 1.22 10.80 28.87 28.74 0.10 29.46 2 3 3/14/13 3/14/13 1240- 1455 1520

- 1730 120 120 29.45 29.07 80.024 76.032

49.9 53.4 509.9 513.4

1.20 1.20 29.54 29.16 92.950 87.100 81.821 76.216 2.317 2.158 0.30 0.40 20.60 20.40 0.00 0.00 79.10 79.20 5,698.5 3,469.4

14.8 12.1 0.84 0.74 13.58 12.50 28.87 28.88 28.78 28.80 0.10 0.10 29.46 29.08 minutes in. Hg
cu. ft. Farenheit Rankine in. H20 in. Hg
cu. ft. cu.ft
cu. Meter % % % % % grams % %

in. H20 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #5 PROJECT 

## #: TI1550

Run Number 1 2 3 Ts =StackTemperature 117.40 125.70 122.20 Farenheit Ts =StackTemperature 320.44 325.06 323.11 Kelvin Ts =StackTemperature 577.4 585.7 582.2 Rankine**\I~** 

### P = Avg. Sum. ofPressure Square Root 0.017 0.017 0.017 Vs = Velocity inthe Stack 60.5 60.9 61.1 ft/min Vs = Velocity inthe Stack 1.01 1.00 1.00 ft/sec As = Effective Stack Area 518,400.0 518,400.0 518,400.0 sq. m. Qa = Volumetric FlowRate at stack cond. 217,800 219,240 219,960 acfm Qs = Volumetric FlowRate, stand. cond., dry 

### 193,711 192,968 192,448 dscfm IR = Isokinetic Ratio (V

### niVs)* 1 00 100.0 103.7 96.8 %

# TEST, Inc. 

# !Comments: Trap #5 pah PAH Sampling Data Project# TI1550 Meter Box# 2010 %C020.30 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0203 %02 20.50 1 333.1 333.7 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 722.8 723

Operator br Nozzle# %N2 79.20 3 710.7 710.8 Run# 1 Nozzle Dia. (in.) 1.5 Assumed Moist % 1.22 4 607.2 613.4

Date 3/14/13 Stack Dia.(in.) Final Moist. % 1.22 5 902.9 916.5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic % 100.0 6 Min/pt 5 Bar. Press. ("Hg) 29.45 Initial Leak Rate 

### 0.001 cfm@ 12 "Hg Filter#

---- Leak Check Vol. Final Leak Rate 0.001 cfm@ 12 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 930 517.880 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 4-6 935 520.805 0.0003 1.10 0.614 2.5 100 253 255 67 71 64

5 940 523.706 0.0003 1.10 0.614 2.5 106 254 253 66 

### 70 

### 66 4 945 526.707 0.0003 1.10 0.614 2.5 119 250 250 66 69 67 3 950 529.507 0.0003 1.10 0.614 2.5 110 251 251 65 65 63 2 955 532.209 0.0003 1.10 0.614 2.5 112 250 247 63 51 48 1 1000 534.905 0.0003 1.10 0.614 2.5 110 250 250 65 50 60 3-6 1010 537.907 0.0003 1.10 0.614 2.5 119 250 231 59 54 51

5 1015 540.068 0.0003 1.10 0.614 2.5 112 247 245 63 43 50 4 1020 544.006 0.0003 1.10 0.614 2.5 105 244 251 62 48 47 3 1025 547.108 0.0003 1.10 0.614 2.5 109 251 256 57 55 64 2 1030 550.408 0.0003 1.30 0.687 4.0 108 251 253 65 57 66 1 1035 554.003 0.0003 1.30 0.687 4.0 115 247 249 55 42 59 2-6 1045 557.506 0.0003 1.30 0.687 4.0 118 252 248 66 52 59

5 1050 560.809 0.0003 1.30 0.687 4.0 122 245 250 50 43 58 4 1055 564.208 0.0003 1.30 0.687 4.0 126 254 252 60 45 57 3 1100 567.602 0.0003 1.30 0.687 4.0 125 246 249 65 58 61 2 1105 571.003 0.0003 1.30 0.687 4.0 127 247 249 66 57 61 1 1110 574.301 0.0003 1.30 0.687 4.0 127 251 250 64 49 57 1-6 1120 577.703 0.0003 1.30 0.687 4.0 122 251 252 61 46 57 5 1125 581.108 0.0003 1.30 0.687 4.0 124 248 248 60 53 58 4 1130 584.409 0.0003 1.30 0.687 4.0 125 257 251 67 47 58 3 1135 588.209 0.0003 1.30 0.687 4.0 125 247 258 67 44 59 2 1140 591.206 0.0003 1.30 0.687 4.0 127 256 258 66 44 57 1 1145 594.604 0.0003 1.30 0.687 4.0 125 253 258 60 40 56

## Example Calculations Run Number 1 Pb 29.45 "Hg Barometric Pressure Cp 0.84 Vw 20.7 Water weight gain Ds 0 Pm 1.22 "H20 Meter pressure As 518,400.0 Avg**~** 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** 

### P 0.017 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.30 Carbon Dioxide %CO 0.00 %02 20.50 Oxygen

Vm 76.724 acf Ps 0.10 "H20 Tm 55.3 (F) Ts 117.4 (F)

Vmstd = 17.65 *Vm * [ Pb 

### +

# 1~] Tm(R) %N2 79.20 78.281 (acf* Y) Dry Gas Volume 29.46 "Hg Stack Pressure 515.3 (R) Meter Temperature 577.4 (R) Stack Temperature

# ~ 17.65 • 78.281 • [ 

# w ]-- 29.45 

### + 13.6 515.3

Vwgas = 0.0471 * Vw = 0.0471 * 20.7 0.975 sft 3 

### Pitot Cal in. Stack Diameter Sq in. Stack Area in Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

79.204 sft j



### 1.320 scfm

Bws= Vwgas Bws* 100 = 1.22 % Moist. Md = 28.868 Vmstd 

### +Vwgas

Ts(R) Vs=5129.4*Cp* \Ps*Mw

5129.4 * 0.84 ===== 

### 1-Bws = 0.9878 MW = 28.735 =====



### * sqrt**~** 

### P 577.4 29.46 * 28.735 * 1.01 tips 0.017 ===6=0.=5=fpm =====


### ACFM= Vs *As 144 60.5 * 518400.0 144

DSCFM = ACFM * 528 *Ps 

# *(1-Bws) Ts (R) * 29.92

% 

### Iso.= 1039 * Vmstd * Ts (R) (1-Bws) *Ps * Tt

# *Vs * (Dn)/\2 1,039 

## * 79.204 217,800 ACFM

217,800 * 528 * 29.46 

# * 0.9878 577.4 * 29.92

* 577.4 100.0 % 0.9878 * 29.46 * 120 * 60.5 * 2.25000 193,711 DSCFM

# TEST, Inc. !Comments: 

## Trap #8 PAH Sampling Data Project# TI1550 Meter Box# 2010 mst %C02 0.30 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.60 1 339.8 340 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 697.2 693.5

Operator br Nozzle# %N2 79.10 3 708 705.5 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % 1.80 4 609.2 609.8

Date 3/14/13 Stack Dia.(in.) Final Moist. % 0.84 5 880.9 901.1 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic % 103.7 6 Min/pt 5 Bar. Press. ("Hg) 29.45 Initial LeakRate 

### 0.001 cfm@ 11 "Hg Filter #

---- Leak Check Vol. Final Leak Rate 0.001 cfm@ 11 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1240 702.827 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out

7-6 1245 707.108 0.0003 1.20 0.640 5.0 115 256 249 50 48 46

5 1250 710.307 0.0003 1.20 0.640 5.0 117 257 251 49 

### 49 48 4 1255 713.204 0.0003 1.20 0.640 5.0 118 262 253 47 52 48 3 1300 716.401 0.0003 1.20 0.640 5.0 116 259 251 47 53 49 2 1305 719.608 0.0003 1.20 0.640 5.0 120 261 249 47 54 52 1 1310 722.909 0.0003 1.20 0.640 5.0 122 266 250 50 53 51 6-6 1320 726.207 0.0003 1.20 0.640 5.0 129 258 250 46 51 48

5 1325 729.506 0.0003 1.20 0.640 5.0 128 254 248 43 52 51 4 1330 732.707 0.0003 1.20 0.640 5.0 129 258 251 43 51 50 3 1335 736.103 0.0003 1.20 0.640 5.0 126 263 250 43 52 50 2 1340 739.307 0.0003 1.20 0.640 5.0 128 261 251 45 51 51 I 

### 1345 741.609 0.0003 1.20 0.640 5.0 129 262 254 49 51 48 5-6 1355 744.903 0.0003 1.20 0.640 5.0 128 250 248 49 48 47

5 1400 748.405 0.0003 1.20 0.640 5.0 129 263 251 48 49 48 4 1405 751.704 0.0003 1.20 0.640 5.0 132 257 249 48 51 49 3 1410 754.906 0.0003 1.20 0.640 5.0 138 260 250 51 50 49 2 1415 758.508 0.0003 1.20 0.640 5.0 133 255 251 49 51 48 I 

### 1420 761.504 0.0003 1.20 0.640 5.0 117 257 257 49 51 50 4-6 1430 764.603 0.0003 1.20 0.640 5.0 114 270 247 50 51 49

5 1435 767.902 0.0003 1.20 0.640 5.0 126 255 245 51 47 45 4 1440 771.008 0.0003 1.20 0.640 5.0 126 256 251 51 48 46 3 1445 774.903 0.0003 1.20 0.640 5.0 124 258 250 52 53 51 2 1450 777.403 0.0003 1.20 0.640 5.0 133 262 244 54 54 53 1 1455 780.505 0.0003 1.20 0.640 5.0 140 264 248 54 50 48

## Example Calculations Run Number 2 Ph 29.45 "Hg Barometric Pressure Cp 0.84 Vw 14.8 Water weight gain Ds 0 Pm 1.2 "H20 Meterpressure As 518,400.0 Avg**~** 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** 

### P 0.017 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.30 Carbon Dioxide %CO 0.00 %02 20.60 Oxygen

Vm 77.678 acf Ps 0.10 "H20 Tm 49.9 (F) Ts 125.7 (F)

Vmstd = 17.65 * Vm * [Ph+

# ~J Tm(R) %N2 79.10 80.024 (acf* Y) Dry Gas Volume 29.46 "Hg Stack Pressure 509.9 (R) MeterTemperature 585.7 (R) Stack Temperature

# ~ 17.65 • 80.024 • [ 

### UQ 

# ]= 29.45 + 13.6

- 509.9

Vwgas = 0.0471 * Vw = 0.0471 * 14.8 0.6971 sft 3 

### Pitot Cal in. Stack Diameter Sq in. Stack Area in Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

81.821 sft j



### 1.364 scfm

Bws= Vwgas Bws* 100 = 0.84 % Moist. Md = 28.872 Vmstd + Vwgas

Vs = 5129.4 *

5129.4 * Ts (R) 

### \ Ps 

## *Mw

0.84 ==== ===== 1-Bws = 0.9916 MW = 28.781 =====

* sqrt**~** 

### P 585.7 29.46 * 28.781 * 0.017 ===6=0.=9=fpm =====
ACFM= Vs *As 144 60.9 * 518400.0 144 219,240 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 219,240 * 528 * 29.46 * 0.9916 585.7 * 29.92 192,968 DSCFM

0 /o 

### lso.

## = 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (Dn)"2 1,039 * 81.821 0.9916 * 29.46 * 120 

## * 585.7 103.7 % 

## * 60.9 * 2.25000

# TEST, Inc. 

# I Comments: 

## Trap #1 PAH Sampling Data Project # TI1550 Meter Box# 2010 MST %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.40 1 333.3 333.7 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 721.1 714.5

Operator br Nozzle# %N2 79.20 3 712 710.5 Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist% 2.00 4 608.1 611.2

Date 3114/13 Stack Dia.(in.) 0 Final Moist.% 0.74 5 915.9 932.6 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 96.8 6 Min/pt 5 Bar. Press. ("Hg) 29.07 Initial Leak Rate 

### 0.001 cfm@ 10 "Hg Filter# Leak CheckVol. Final LeakRate 0.001 cfm@ 10 "Hg Dry Gas Pi tot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1520 781.500 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out

6-8 1525 786.407 0.0003 1.20 0.640 5.5 120 243 248 61 52 50

7 1530 789.307 0.0003 1.20 0.640 5.5 121 254 249 66 

### 53 52 6 1535 792.504 0.0003 1.20 0.640 5.5 121 253 247 55 54 51 5 1540 795.603 0.0003 1.20 0.640 5.5 120 263 249 64 54 52 4 1545 798.804 0.0003 1.20 0.640 5.5 121 252 250 49 55 53 3 1550 801.907 0.0003 1.20 0.640 5.5 126 261 249 49 54 52 2 1555 805.203 0.0003 1.20 0.640 5.5 128 263 250 

### 56 55 54 1 1600 808.301 0.0003 1.20 0.640 5.5 124 262 249 61 57 55 4-8 1610 810.709 0.0003 1.20 0.640 5.5 124 260 249 63 56 55

7 1615 812.806 0.0003 1.20 0.640 5.5 123 265 249 66 55 52 6 1620 815.304 0.0003 1.20 0.640 5.5 127 256 250 65 54 53 5 1625 817.830 0.0003 1.20 0.640 5.5 125 257 250 67 54 51 4 1630 820.140 0.0003 1.20 0.640 5.5 122 259 251 66 54 52 3 1635 823.340 0.0003 1.20 0.640 5.5 123 261 249 58 54 51 2 1640 826.550 0.0003 1.20 0.640 5.5 120 258 247 60 56 52 1 1645 829.707 0.0003 1.20 0.640 5.5 121 262 251 62 54 51 2-8 1655 832.904 0.0003 1.20 0.640 6.0 120 256 249 63 52 47

7 1700 836.105 0.0003 1.20 0.640 6.0 122 260 248 66 54 53 6 1705 839.504 0.0003 1.20 0.640 6.0 120 259 252 47 57 55 5 1710 842.502 0.0003 1.20 0.640 6.0 120 263 257 46 54 51 4 1715 846.004 0.0003 1.20 0.640 6.5 122 271 250 47 56 52 3 1720 849.208 0.0003 1.20 0.640 6.5 121 256 255 46 55 54 2 1725 852.103 0.0003 1.20 0.640 6.5 120 257 246 47 55 53 1 1730 855.303 0.0003 1.20 0.640 6.5 122 259 249 47 54 52

## Example Calculations Run Number 3 Pb 29.07 "Hg Barometric Pressure Cp 0.84 Vw 12.1 Water weight gain Ds 0 Pm 1.2 "H20 Meter pressure As 518,400.0 Avg**~** 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** 

### P 0.017 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen

Vm 73.803 acf Ps 0.10 "H20 Tm 53.4 (F) Ts 122.2 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm(R) %N2 79.20 76.032 (acf* Y) Dry Gas Volume 29.08 "Hg Stack Pressure 513.4 (R) Meter Temperature 582.2 (R) Stack Temperature

# ~ 17.65 • 76.032 • [ UQ ]-- 

### 29.07 

### + 13.6 513.4

Vwgas = 0.0471 * Vw = 0.0471 * 12.1 0.5699 sft 3 

### Pitot Cal in. Stack Diameter Sq in. Stack Area in Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

76.216 sft j



### 1.270 scfm

Bws= Vwgas Bws*100 = 0.74 %Moist. Md = 28.880 Vmstd 

### +Vwgas

Ts(R) Vs= 5129.4 * Cp * \Ps *Mw 1-Bws = 0.9926

* sqrt**~** 

### P 582.2 ===== MW = 28.799 =====

5129.4 * 0.84 29.08 * 28.799 * 0.017 ===6=1.=1=fpm ===1===fps

ACFM= Vs *As 144 61.1 * 518400.0 144

DSCFM = ACFM * 528 *Ps * 

### (1-Bws) Ts (R) * 29.92

% 

### lso. 

## = 1039 * Vmstd * Ts (R) (1-Bws) *Ps * Tt 

### * Vs * (Dn)"2 1,039 * 76.216 219,960 ACFM

219,960 * 528 * 29.08 * 0.9926 582.2 * 29.92

* 582.2 96.8 % 0.9926 * 29.08 * 120 * 61.1 * 2.25000 192,448 DSCFM

# EXAMPLE CALCULATIONS PAH'S

lbs/hr = __ 

### m_,g"'--- x __ 

### l

......

g._r- x DSCFM x Vmstd 64.8 mg

DSCFM* = 

### StackFlowRate 60min 

### lhr

Vmstd* = 

### Volume ofdry gas sampled at standard conditions dry standard cubic feet

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C) llb 

### x---- 7,000 gr

# EXAMPLE CALCULATIONS DIOXINS/FURANS AND PCB'S

lbslhr=--m-=g- x -- 1 -=gr"--- x DSCFM x Vmstd 64.8 mg

DSCFM* = Stack Flow Rate 60min 

## lhr

Vmstd* = Volume ofdry 

### gas sampled at standard conditions dry 

### standard cubic feet

*29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C) lib 

### x---- 7,000 gr

# EXAMPLE CALCULATIONS MULTIPLE METALS

lbs/hr =--m..l:::.g_ x __ l...:.gr::......__ x DSCFM x Vmstd 64.8 mg

DSCFM* = Stack Flow Rate 60min 

### lhr

Vmstd* = Volume ofdry 

### gas sampled at standard conditions dry 

### standard cubic feet

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C) 

## llb x--- 7,000 gr

# EXAMPLE CALCULATIONS MERCURY

lbslhr=--m-=g- x -- 1 --==gr"---- x DSCFM x Vmstd 64.8 mg

DSCFM* = Stack Flow Rate 60min 

## lhr

Vmstd* = Volume ofdry 

### gas sampled at standard conditions dry 

### standard cubic feet

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C) lib 

### x---- 7,000 gr

# EXAMPLE CALCULATIONS HYDROGEN CHLORIDE

mgHCl 24.04 Hydrogen Chloride ppm= x --- Vmstd (cu.m) 36.45

HCllbs/hr mg HCI 

### x __ l....!:g._r_ 

### x DSCFM 

### x 60 min lib X 

### Vmstd 64.8 mg 1 

### hr 7,000 gr

36.45 =MolecularWeight ofHydrogen Chloride
24.04 = Ideal Gas Constant liters/g-mole
DSCFM* = StackFlowRate

Vmstd* = Volume ofdry gas sampled at standard conditions dry 

### standard cubic feet
Vmstd* (cu.m) = Volume ofdry 

### gas sampled (cubic meters)

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C)

# -- APPENDIXB PRE-FLOW DATA ,·_;

# TEST, Inc. 

# I Comments: 

## Method SD Setup Project# Meter Box# 2010 MST %C02 0.01 Imp. Initial Final Plant Meter Cal. (Y) 1.0283 %02 20.80 1 703.7 695 Unit/Stack Pitot Cal. (Cp) 0.84 %CO 2 711.3 723.5

Operator Nozzle# %N2 79.19 3 597.8 601.3 Run # BH5 Inlet Nozzle Dia. (in.) Assumed Moist % 1.15 4 896.3 908.3

Date 3/12/13 Stack Dia.(in.) 108 Final Moist. % 1.15 5 Sample Time 30 Static Press.("H20) -0.40 Final Isokinetic% #REF! 6 

### Min/pt 5 Bar. Press. ("Hg) 29.15 

### Initial LeakRate 0.006 cfm@ 14 "Hg Filter# Leak Check Vol. Final Leak Rate 0.006 cfm@ 14 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 163.555 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In 

### Out 236.550 0.23 1.20 0.628 2.0 270 42 42 0.25 267 0.41 266 0.48 273 0.48 277 0.46 285 0.45 290 0.42 290 0.40 286 0.35 284 0.35 275 0.35 271 0.23 267 0.23 268 0.30 260 0.30 259 0.30 265 0.32 271 0.42 280 0.44 291 0.45 297 0.43 315 0.40 310 0.34 305

## Example Calculations Run Number BH5 Inlet Ph 29.15 "Hg Barometric Pressure Cp 0.84 Vw 19 Water weight gain Ds 108 Pm 1.2 "H20 Meter pressure As 9,160.9 Avg fl. 

### P 0.366 "H20 Differential pressure Dn 0 A

vg Sqrt fl. 

### P 0.601 "H20 Sqrt Diff. press. Tt 

### 30 %C02 0.01 Carbon Dioxide %CO 0.00 %02 20.80 Oxygen

Vm 72.995 acf Ps -0.40 "H20 Tm 42.0 (F) Ts 280.1 (F)

Vmstd = 17.65 * Vm * [Ph+

# 1~] Tm(R)

Vwgas = 0.0471 * Vw = 0.0471 * %N2 79.19 75.061 (acf* Y) Dry Gas Volume 29.12 "Hg Stack Pressure

502 (R) Meter Temperature 740.1 (R) Stack Temperature

[ 1.20 ]= = 17.65 * 75.061 * _29_._15

___ +
____ 1_3._6_ 502.0

19 0.8949 sft 3 

### Pitot Cal m. Stack Diameter Sq in. Stack Area in Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

77.163 sft 5



### 1.286 scfm

Bws= Vwgas Bws*100 = 1.15 %Moist. Md = 28.834 ===== 

### Vmstd + Vwgas 1-Bws = 0.9885 MW = 28.709

Ts(R) Vs=5129.4*Cp* \Ps*Mw * sqrt fl. 

### P =====



### 5129.4 * 0.84 

# I 740.1 * \ -2-9-.1-2--*--2-8-.7-0-9 * 0.601 

## = 2,436.5 fpm 40.61 tips

ACFM= Vs *As 144 2,436.5 * 9160.9 144

DSCFM= ACFM * 528 * Ps * 

### (1-Bws) Ts (R) *29.92 155,004 ACFM

155,004 * 528 * 29.12 * 0.9885 740.1 * 29.92 =====



### 106,388 DSCFM

# Method 5D Velocity Calculation
Areaofmeasurement site Ao= Temp. at measurement site To= Ambienttemp. Tamb= Inlet temp. Ti = Inlet gas volume flow rate Qi=


### Eq. SD-3 Dilution AirFlow Rate Qd = Qi (Ti-To) To-Tamb Qd = 

### 2858.685 (DSCFS)


### Eq. SD-2 Volumetric Flow Rate Qo = Qi+Qd Qo = 

### 4631.818 (DSCFS)


### Eq. SD-1 Average Gas Velocity Qo 

### v 

## =---==--- Ao

v= 1.286616 (FPS) 3600}ft2 135I(F) 595 ( R) 45j (F) 505 ( R) 280.1 (F) 740.1 ( R) 106,388 (DSCFM) 1773.133 (DSCFS)

## ISOKINETIC PRELIMINARY SETUP CALCULATIONS %Moisture 1.15 % Y= 1.0283 Md 0.9885**~p** 

### = 0.000451 "H20 C02 0.01 %

### \I~ p = 0.021 "H20

02 20.80 % Pb = 29.15 "Hg 

# co % Cp = 0.84 N2 79.19 % Ts 135 OF 595 MWd 28.834 Tm 42 OF 502

MW 28.709 (28.966) Psa -0.400 "H20 29.12 AssumedRm

Assumed Tt Assumed cf = 

### Velocity Calculation Vs

## \I~**~**


### Nozzle Diameter On=



### MeterRate Rm 0.850 (0.60-0.85) cfm 240 mm 204.0 (scfm * Tt)



### 85.49 

# *Cp 

# *l[t< P 

# *\I(MW 

# *

# ~:.) ( 

### 60.5820 *

### \1~ p ) = 1.2866 fps p = 0.02124 p = 0.000451

Rm 

# *Ts 

# *Y 

### \ 0.33 * Vs * Tm * Md



### Desired 1.549 in 

### Actual 1.500 in

0.33 * (Vs *\lAY")* Tm * Md *On 2 

### Ts* Y 0.775 cfm cf*Tt= 185.95 cf Correction factor = cfm = 36.482 @ 

### 42

### \1~ p Rate Correction Multipliers Rm(new)= Tm(new) 

## +460 Tm(old) 

## +460 * Rm(old)

36.482 *

### \I~ P 

## ®

_ ____;;4.::..2

__ 37.209***\I~P** 

## ®

__ 5_2

__ 37.936 ***\1~** 

### P 

## ®

__ 6_2

__ °FTm °FTm °FTm 

## OR OR

"Hg

### 38.663

### *\I~ p 

# ® 72 

### °FTm 39.389 

# ***\1~** p @ 82 

### °FTm 40.116 

# ***\1~** p @ 92 

### °FTm
40.843 

# ***\1~** p @ 102 

### °FTm
41.570 

# ***\1~** p @ 112 

### °FTm

# TEST, Inc.**~Comments:** Method 5D Setup**~----------------------------------------~** 

### Project# Meter Box# 2010 MST %C02 0.01



## ------ Plant Meter Cal. (Y) 1.0283 %02 20.80 Unit/Stack Pitot Cal. (Cp)_0_.8_4

__ _ %CO



## ------ Operator Nozzle # %N2 79.19



# ------ Run# BH5 Inlet Nozzle Dia. (in.) Assumed Moist% 1.15



# ------ ------ Date 3/12/13 Stack Dia.(in.) 108 Final Moist.% 1.18



## ------ Sample Time 30 Static Press.("H20) -0.40 Final Isokinetic % #REF!



### -------------- Min/pt 5 Bar. Press. ("Hg) 29.15 Initial Leak Rate 0.006 Filter# Leak Check Vol. Final Leak Rate 0.006 Dry Gas Pitot Orifice Vacuu Stack Probe Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Point 163.555 ("H20) ("H20) (cfm) ("Hg.) (F) (F) 236.550 0.25 1.20 0.628 2.0 255 0.23 253 0.27 244 0.41 242 0.44 259 0.46 257 0.48 258 0.45 255 0.43 254 0.37 252 0.36 245 0.25 244 0.21 235 0.24 242 0.27 245 0.25 249 0.27 252 0.28 257 0.37 255 0.41 260 0.45 258 0.45 256 0.45 254 0.43 244 Imp. 1 2 3 4 5 

### 6 Initial 703.7 711.3 597.8 896.3 Final 695 723.5 601.3 908.3

cfm@

__ 1_4 _"Hg cfm@ 14 "Hg Filter Imp. 

### Dry Gas Temp. Temp. Temp.

(F) (F) In Out 55 55

## Example Calculations Run Number BH5 Inlet Ph 29.15 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 19 Water weight gain Ds 108 in. Stack Diameter Pm 1.2 "H20 Meter pressure As 9,160.9 Sq in. Stack Area Avg f.. 

### P 0.353 "H20 Differential pressure Dn 0 in Nozzle Diameter Avg Sqrt f.. 

### P 0.589 "H20 Sqrt Diff. press. Tt 

### 30 mm Sample Time %C02 0.01 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.80 Oxygen

Vm 72.995 acf Ps -0.40 "H20 Tm 55.0 (F) Ts 251.0 (F)

Vmstd = 17.65 * Vm * [Ph+

# 1~] Tm(R)

Vwgas = 0.0471 *Vw = 0.0471 *

Bws= Vwgas Vmstd + Vwgas

Ts (R) Vs=5129.4*Cp* \Ps*Mw

5129.4 * 0.84 %N2 = 79.19 75.061 (acf* Y) Dry Gas Volume 29.12 "Hg Stack Pressure

515 (R) Meter Temperature 711 (R) Stack Temperature

# ~ 17.65 • 75.061 • [ .L2.Q 

# ]= 29.15 + 13.6

- 515.0

19 0.8949 sft 3 

### Nitrogen

75.215 sft 5



### 1.254 scfm

Bws* 100 = 1.18 % Moist. Md = 28.834 

## ===== 1-Bws = 0.9882 MW = 28.706 =====



### * sqrt f.. 

### P 711 29.12 * 28.706 * 0.589 = 2,340.5 fpm 39.01 =====


### ACFM= Vs *As 144 2,340.5 * 9160.9 144 148,896 ACFM fps

DSCFM = ACFM * 528 *Ps * 

### (1-Bws) Ts (R) * 29.92 148,896 * 528 * 29.12 * 0.9882 106,346 DSCFM 711 * 29.92

# Method 5D Velocity Calculation
Area ofmeasurement site Ao= Temp. at measurement site To= Ambient temp. Tamb= Inlet temp. Ti= Inlet gas volume flow rate Qi = 

### Eq. SD-3 Dilution AirFlow Rate Qd = Qi (Ti-To) To-Tamb Qd 

### = 2144.644 (DSCFS)


### Eq. SD-2 Volumetric Flow Rate Qo = Qi+Qd Qo = 

### 3917.078 (DSCFS)


### Eq. SD-1 Average Gas Velocity Qo v 

### = ---"'--- Ao

v= 1.088077 (FPS) 3600] ft2 130) (F) 590 ( R)

30j(F) 490 ( R) 251 (F) 711 ( R) 106,346 (DSCFM) 1772.433 (DSCFS)

## ISOKINETIC PRELIMINARY SETUP CALCULATIONS %Moisture = Md C02

02 

# co N2 MWd

MW = AssumedRm

Assumed Tt = Assumed cf = Velocity Calculation Vs

## \I~**~**


### Nozzle Diameter Dn =



### MeterRate Rm 1.18 % Y= 1.0283 0.9882**~p** 

### = 0.000325 "H20

0.01 %

### \1~ p = 0.018 "H20 20.80 % Pb = 29.15 "Hg % Cp 0.84 79.19 % Ts = 130 OF 590 28.834 Tm 55 OF 515 28.706 (28.966) Psa -0.400 "H20 29.12 0.650 (0.60-0.85) cfm

120 mm 78.0 (scfm * Tt)

85.49 

# *Cp 

# *\lt. P 

### *

### \I(MW

# *~:a) ( 

### 60.3304 *

### \1~ p ) = 1.0881 fps p 0.01804 p 0.000325

Rm 

# *Ts 

# * Y 

### \ 0.33 * Vs * Tm * Md

Desired 1.449 in Actual 1.500 in

0.33 * (Vs * 

### \(A"P'") * Tm * Md * Dn 2 

### Ts* Y 0.678 cfm cf* Tt = 81.32 cf Correction factor= cfm

### \1~ p 37.576 

### @ 55

Rate Correction Multipliers Rm(new)= Tm{new) 

## +460 * Rm(old) Tm(old) 

## +460 37.576

### *\I~ p 

## ® 55 °FTm 38.306 *

### \1~ p 

### @ 65 °FTm 39.035

### *\I~ p 

## ® 75 °FTm OR OR

"Hg

### 39.765

### *\I~ p 

## ® 85 

### °FTm 40.495 

# ***\1~** p @ 95 

### °FTm 41.224 

# ***\1~** p @ 105 

### °FTm
41.954 

# ***\1~** p @ 115 

### °FTm
42.684 

# ***\1~** p @ 125 

### °FTm

# TEST, Inc. !Comments: 

## Method 5D Setup**~----------------------------------------~** 

### Project # Meter Box # 2010 MST %C02 0.01 Imp. Initial Final



## --- Plant Meter Cal. (Y) 1.0283 %02 20.80 1 703.7 695 Unit/Stack Pitot Cal. (Cp) 0.84 %CO 2 711.3 723.5



## ----- ---- Operator Nozzle# %N2 79.19 3 597.8 601.3



## ----- Run# BH5 Inlet Nozzle Dia. (in.) Assumed Moist% 1.15 4 896.3 908.3



## ----- ---- Date 3/12/13 Stack Dia.(in.) 108 Final Moist.% 1.15 5



## --- Sample Time 30 Static Press.("H20) -0.40 Final Isokinetic% #REF! 6



## -------- Min/pt 5 Bar. Press. ("Hg) 29.15 Initial Leak Rate 0.006 cfm@ 14 "Hg

------- 

### Filter# Leak Check Vol. Final Leak Rate 0.006 cfm@ 14 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 163.555 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 236.550 0.22 1.20 0.628 2.0 235 45 45 0.24 232 0.25 232 0.30 235 0.34 237 0.34 245 0.45 263 0.45 266 0.45 273 0.45 274 0.42 270 0.45 237 0.25 254 0.25 255 0.37 266 0.42 273 0.45 280 0.45 281 0.45 281 0.45 286 0.38 275 0.35 271 0.34 262 0.32 250

## Example Calculations Run Number BH5 Inlet Pb 29.15 "Hg Barometric Pressure Cp 0.84 Vw 19 Water weight gain Ds 108 Pm 1.2 "H20 Meter pressure As 9,160.9 Avg b. 

### P 0.368 "H20 Differential pressure Dn 0 Avg Sqrt b. 

### P 0.603 "H20 Sqrt Diff. press. Tt 

### 30 %C02 0.01 Carbon Dioxide %CO 0.00 %02 20.80 Oxygen

Vm 72.995 acf Ps -0.40 "H20 Tm 45.0 (F) Ts 259.7 (F)

Vmstd = 17.65 * Vm * [ Pb +

# 1~] Tm(R)

Vwgas = 0.0471 * Vw = 0.0471 * %N2 79.19 75.061 (acf* Y) Dry Gas Volume 29.12 "Hg Stack Pressure

505 (R) Meter Temperature 719.7 (R) Stack Temperature

[ 1.20 ]= = 17.65 * 75.061 * _29_.1_5--::-::+:"::""7_13_._6_ 505.0

19 0.8949 sft 3 

### Pitot Cal in. Stack Diameter Sq in. Stack Area in Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

76.704 sft j



### 1.278 scfm

Bws= Vwgas Bws*100 = 1.15 %Moist. Md = 28.834 ===== 

### Vmstd + Vwgas 1-Bws = 0.9885 MW = 28.709

Ts(R) Vs=5129.4*Cp* \Ps*Mw * sqrt b. 

### P =====



### 5129.4 * 0.84 

# I 719.7 * \ -2-9-.1-2--*--2-8-. 7-0-9 * 0.603 

## = 2,410.7 fpm 40.18 fips

ACFM= Vs *As 144 2,410.7 * 9160.9 144

DSCFM= ACFM * 528 *Ps * (1-Bws) Ts (R) * 29.92 153,362 ACFM

153,362 * 528 * 29.12 * 0.9885 719.7 * 29.92 =====



### 108,245 DSCFM

# Method 5D Velocity Calculation
Areaofmeasurement site Ao= Temp. at measurement site To= Ambient temp. Tamb= Inlet temp. Ti = Inlet gas volume flow rate Qi=


### Eq. 5D-3 Dilution AirFlow Rate Qd = Qi (Ti-To) To-Tamb Qd = 

### 2463.049 (DSCFS)


### Eq. 5D-2 Volumetric Flow Rate Qo = Qi+Qd Qo = 

### 4267.132 (DSCFS)


### Eq. 5D-1 Average Gas 

### Velocity Qo 

### v = _ _;:::,__ 

### Ao

v= 1.185314 (FPS) 3600)ft2 130I(F) 590 ( R)

35l (F) 495 ( R) 259.7 (F) 719.7(R) 108,245 (DSCFM) 1804.083 (DSCFS)

## ISOKINETIC PRELIMINARY SETUP CALCULATIONS %Moisture 1.15 % Y= 1.0283 Md 0.9885**~p** 

### = 0.000386 "H20 C02 = 0.01 %

### \1~ p = 0.020 "H20

02 = 20.80 % Pb = 29.15 "Hg 

## co = % Cp 0.84 N2 = 79.19 % Ts = 130 OF 590 MWd 28.834 Tm 45 OF 505

MW 28.709 (28.966) Psa = -0.400 "H20 29.12 AssumedRm =

Assumed Tt = Assumed cf = Velocity Calculation Vs

## \I~**~**


### Nozzle Diameter Dn =



### MeterRate Rm 0.650 (0.60-0.85) cfm 120 min 78.0 (scfm 

# *Tt)



### 85.49 • 

## cp • lit. P •

# \I(Mw•

# ~':al ( 

### 60.3270

## *'I~ p)= 1.1853 fps p = 0.01965 p 0.000386

Rm 

# * Ts 

# * Y \ 0.33 

# *Vs 

# *Tm

# *Md

Desired 1.401 in Actual 1.500 in

0.33 

# * (Vs *

### \[A"P") * Tm * Md * Dn 2 

### Ts* Y 0.724 cfm cf* Tt= 86.90 cf Correction factor = cfm = 36.856 @ 45

### \1~ p Rate Correction Multipliers Rm(new)= Tm(new) 

## +460 Tm(old) 

### + 460 * Rm(old)

36.856 

# ***,,~** 

### p @

__ 4_5

-- 37.585***\I~P** 

# ®

__ 5_5

__ 38.315 ***,,~** 

### p @

__ 6_5

-- °FTm °FTm °FTm OR OR

"Hg

### 39.045

### *\I~ p 

## ® 75 

### °FTm 39.775 

# ***\1~** p @ 85 

### °FTm 40.505 

# ***\1~** p @ 95 

### °FTm
41.235 

# ***\1~** p @ 105 

### °FTm
41.964 

# ***\1~** p @ 115 

### °FTm

### APPENDIXC ANALYTICAL DATA**.:~_**

:.:.-

### Run Number 1 2 3 

# ANALYTICAL RESULTS

Filter Number

1012 1011 

### 1010 

## Particulate Matter FelmanProductions LLC Baghouse #5

Filter Acetone Rinse Final Weight Final Weight (grams) (grams) 0.0025 0.0010 0.0029 0.0022 0.0033 0.0016 Total Particulate

Matter (grams) 0.0035 0.0051 0.0049' 

### Lab Conditions**~ ·:-~**  -·..·-.
pc.. ,.,_, ,;**·~** '• ,; 0 .-,: • 

# Filter Gravimetric Analysis Temperature: 18 

# oc Bar. Press.: 29.03 "Hg ProjectNumber: TI1550 Location: Baghouse#5 Company: Felman Productions LLC EPA Method: 5 Analyst: JPS Initial Tray FilterTare Tray/Filter Weight Weight Weight Weight Results FilterNumber: 1012 Number Date Time (g} (g} (g} (g} 

### Notes: 1 4115/2013 800 0.9230 0.5504 1.4759 0.0025 2 4/15/2013 1200 0.9230 0.5504 1.4759 0.0025 3 4115/2013 1600 0.9230 0.5504 1.4759 0.0025 

### Final Weight: 0.0025 Initial Tray Filter Tare Tray/Filter Weight Weight Weight Weight Results FilterNumber: 1011 Number Date Time (g} (g} (g} (g} 

### Notes: 1 4/15/2013 800 0.9230 0.5482 1.4742 0.0030 2 4/15/2013 1200 0.9230 0.5482 1.4742 0.0030 3 4115/2013 1600 0.9230 0.5482 1.474 0.0028 

### Final Weight: 0.0029 Initial Tray Filter Tare Tray/Filter Weight Weight Weight Weight Results FilterNumber: 1010 Number Date Time (g} (g} (g} (g} 

### Notes: 1 4/15/2013 800 0.9230 0.5438 1.4701 0.0033 2 4115/2013 1200 0.9230 0.5438 1.4701 0.0033 3 4115/2013 1600 0.9230 0.5438 1.4701 0.0033



## - Final Weight: 0.0033**:_~.** 

# T, Inc. 

# Rinse Gravimetric Analysis

ProjectNumber: TI1550 Lab Conditions



### ---------------- Company: Felman Productions LLC Temperature: 18

# oc

------------ Location: Baghouse #5 Bar. Press.: 29.03 "Hg

Analyst: JPS



### ----------------

Initial Beaker Beaker/Sample Final Filter Beaker Weight Weight Weight Number Number Date Time {g} {g} {g}



### 1012 5-1 4/15/2013 800 108.0241 108.0251 0.0010 1011 5-2 4/15/2013 800 102.2316 102.2338 0.0022 1010 5-3 4/15/2013 800 105.3084 105.31 0.0016

# Ma~am Your P.O.#: 10244

Your Project #: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Your C.O.C. #: NA Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/04/18 

### CERTIFICATE OF ANALYSIS MAXXAM JOB#: 8351189 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train #Samples Received: 8
Analyses Hydrogen Halides in H2S04 Imp. Volume of Sulfuric Acid lmpinger Date Date Quantity Extracted Analyzed Laboratory Method 8 2013/04/12 2013/04/12 BRL SOP-00108 8 N/A 2013/04/12

* RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.
Encryption Key Ancy Sebastian vlt};lia£;,v- 18 Apr 2013 11:13:25 -04:00 Please direct all qu stions regarding this Certificate ofAnalysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Taxies Email: ASebastian@maxxam.ca Phone#(905)817-5831 

## ==================================================================== Method Reference EPA Method 26A

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of?**\i~a:o:nrn** /•,nalyt!GS !mernational Gorporat!on o.:a Maxxam Anatytics 6740 Campobello Roa(J, MISS!SSauga, Ontario, L51\l 2L8 Tel: (905) 817-5700 Toll-free: 300-563-6266 Fax: {905) 817-5777 -.·1\vv-;.maxxam.ca

# Ma?§Zam

Maxxam Job #: 8351189 Report Date: 2013/04/18

Maxxam ID**~ampling** Date 

### roc Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN RC1306 RC1307 RC1308 RC1309 2013/03/27 2013/03/27 2013/03/19 2013/03/19 00:01 00:01 00:01 00:01

NA NA NA NA Units IBLANK-H2S04-M26A**~LANK-H20-M26A** RUN RUN RDL 

## pc Batch 1-BAGH 2-M26A 2-BAGH 2-M26A Sulfuric Acid Volume ml 325 354 360 409 1 3179578 Hydrochloric Acid ug <200 <200 3100 2500 200 3179677 RDL 

## = Reportable Detection Limit QC Batch 

## = Quality Control Batch

Maxxam ID RC1310 RC1311 RC1312 RC1313 Sampling Date 2013/03/19 2013/03/15 2013/03/15 2013/03/15 00:01 00:01 00:01 00:01 COC Number NA NA NA NA Units RUN RUN RUN RUN RDL 

## pc Batch 3-BAGH 2-M26A 1-BAGH 5-M26A 2-BAGH 5-M26A 3-BAGH 5-M26A Sulfuric Acid Volume ml 379 390 357 406 1 3179578 Hydrochloric Acid ug 1900 230 <200 <200 200 3179677
RDL 

## = Reportable Detection Limit QC Batch 

## = Quality Control Batch

Page2of7
''.lla'<x;trn /-mc1lyllcs lrnernational COrporation o!a Maxxam Analytics 6740 Campobello Roacl, MCSS.issauga, Ontario, LSN 2l8 Tel: (905)**817~5700 Toii~Free:** **800~563-6266** Fax: (905) 817-5777**\'V\VW.maxxam.~**

# Ma?§l.am Keika Ventures Maxxam Job #: 8351189 Client Project #: Tl1550 Report Date: 2013/04/18 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Maxxam ID RC1306 Collected 2013/03/27 Sample ID BLANK-H2S04-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A
Maxxam ID RC1307 Collected 2013/03/27 Sample ID BLANK-H20-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A
Maxxam ID RC1308 Collected 2013/03/19 Sample ID RUN 1-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A
Maxxam ID RC1308 Dup Collected 2013/03/19 Sample ID RUN 1-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12

Maxxam ID RC1309 Collected 2013/03/19 Sample ID RUN 2-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Ana zed Anal st IC/SPEC 3179677 2013/04/12 2013/04/12 Ann-Marie Stern 3179578 N/A 2013/04/12

Maxxam ID RC1310 Collected 2013/03/19 Sample ID RUN 3-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st IC/SPEC 3179677 2013/04/12 2013/04/12 Ann-Marie Stern 3179578 N/A 2013/04/12

Page 3 of7

!Vlaxxam 1\nalvucs International COrporation o/a Maxxam Analylics 6740 Campobello Road, MlsSJssauga, Ontano, LSN 21...8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 WWV'I.maxxam.t.a

# Ma?§l.am

Maxxam Job #: 8351189 Report Date: 2013/04/18

Maxxam ID RC1311 Sample ID RUN 1-BAGH 5-M26A Matrix Stack Sampling Train

Maxxam ID RC1312 Sample ID RUN 2-BAGH 5-M26A Matrix Stack Sampling Train

Maxxam ID RC1313 Sample ID RUN 3-BAGH 5-M26A Matrix Stack Sampling Train Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244

Instrumentation IC/SPEC

Instrumentation IC/SPEC

Instrumentation IC/SPEC Test Summary

Batch Extracted 3179677 2013/04/12 3179578 N/A

Batch Extracted 3179677 2013/04/12 3179578 N/A

Batch Extracted 3179677 2013/04/12 3179578 N/A

Page4of7 Collected 2013/03/15 Shipped Received 2013/04/06

Collected 2013/03/15

Shipped Received 2013/04/06

Collected 2013/03/15

Shipped Received 2013/04/06

MauamllnalyUcs lrnernational COrporatiOn o/a Maxxam Analytics 6740 Campobello Road, Mlssissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: BOQ-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Mar;52am

Maxxam Job #: 8351189 Report Date: 2013/04/18

Results relate onlytothe items tested. Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244

GENERAL COMMENTS

Page 5of7

IVla•xam Analylics ltnernational COrporation ola Maxxam Analy1ics 6740 Campobello Road, Mlssissauga, Ontario, L5N 21.8 Tel: (905) 817-5700 Toll-Free: BOQ-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?§i.am

QA/QC Batch Num lnit QCTvoe Parameter 3179677 A_S Matrix Spike (RC1308) Hydrochloric Acid Spiked Blank Hydrochloric Acid Method Blank Hydrochloric AcidRPDSample/Sample Dup Hydrochloric Acid Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC. -FELMAN PRODUCTIONS

QualityAssurance Report Maxxam Job Number: GB351189 Date Analyzed YYW/mm/dd 2013/04/12 2013/04/12 2013/04/12
2013/04/12 Value %Recovery 100 102 <200

0.2 Units % % ug

% Matrix Spike: A sample to which a known amount ofthe analyte of interest has been added. Used to evaluate sample matrix interference. QC Limits 80-120 90- 110

20 Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

Page 6of7
1\ita'(xam /\nalylJCS lrnernaUonal CorporatiOn o!a Maxxam**Anal~ltics** 6740 Campobello Road, Mfssissauga, Onlarlo,l5N 2L8 Tel: (905) 817-5700 Toll-Free: 80Q-563-6266 Fax: (905) 817-5777W\Vw.maxxam.ca

# Ma?:{Jam

Validation Signature Page

Maxxam Job 

### #: 8351189

The analytical data and all QC contained in this reportwere reviewed andvalidatedbythe following individual(s).

FrankMo, B.Sc., Inorganic Lab. Manager

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have therequired "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page 7 of7

Ma.<xam Analylics Jrnernational Corporation o/a Maxxam Analytics 6740 Campobello Road, Mlssissauga, Ontano, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ua

# Ma({52am
Your P.O.#: 10244

Your Project #: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/04/17

MAXXAM JOB#: 8351214 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train # Samples Received: 7 

### CERTIFICATE OF ANALYSIS

Date Date Analyses Quantity Extracted Analyzed Laboratory Method Metals in Combined Train (6020) 7 2013/04/10 2013/04/12 BRL SOP-00103/ BRL

* RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.

Encryption

# Key[~~~ ,1/ Ancy Sebastian

### Vfll~l)al,w- 17 Apr 201314:33:19-04:00 Please direct all qu ""u"" '"'Ha'u"'H"";:; Certificate ofAnalysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Taxies Email: ASebastian@maxxam.ca Phone# (905) 817-5831 

## ==================================================================== SOP-00102 Method Reference EPA 6020 I M29

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of 8

!V1;n:.:xam/\na!vtJc-s lrrrernalional Corporation o/a Maxxam Analy1ics 6740 campobello Road, Mlssissauga, Onlano, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-553-6266 Fax: (905) 817'-5?17 \'VWw.m.:co•am.t,;a

## M 

# ({)2am

Maxxam Job #: 8351214 Report Date: 2013/04/17

Maxxam ID Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN) RC1448 RC1449 RC1450 RC1451 Sampling Date 2013/03/27 2013/03/13 2013/03/13 2013/03/13 00:01 00:01 00:01 00:01 Units BLANK-M29 RDL RUN RUN RUN RDL 1-BAGH 2-M29 2-BAGH 2-M29 3-BAGH 2-M29 Combined Train Arsenic (As) ug <0.40 0.40 <2.0 <2.0 <2.0 2.0 Combined Train Cadmium (Cd) ug <0.10 0.10 <0.50 <0.50 <0.50 0.50 Combined Train Chromium (Cr) ug 1.80 0.30 3.9 11.4 6.5 1.5 Combined Train Lead (Pb) ug 0.84 0.20 50.0 25.0 28.3 1.0 Combined Train Manganese (Mn) ug 8.25 0.75 3370 976 1280 3.8 Combined Train Nickel (Ni) ug 1.69 0.50 4.7 11.1 9.1 2.5 RDL = Reportable Detection Limit QC Batch = Quality Control Batch

Maxxam ID RC1452 RC1453 RC1454 Sampling Date 2013/03/13 2013/03/13 2013/03/13 00:01 00:01 00:01 Units RUN RUN RUN RDL 

## pc Batch 1-BAGH 5-M29 2-BAGH 5-M29 3-BAGH 5-M29 Combined Train Arsenic (As) ug <2.0 <2.0 <2.0 2.0 3177251 Combined Train Cadmium (Cd) ug <0.50 <0.50 <0.50 0.50 3177251 Combined Train Chromium (Cr) ug 7.4 38.3 3.6 1.5 3177251 Combined Train Lead (Pb) ug 25.9 36.2 14.0 1.0 3177251 Combined Train Manganese (Mn) ug 607 547 400 3.8 3177251 Combined Train Nickel (Ni) ug 5.7 14.7 4.3 2.5 3177251 RDL = Reportable Detection Limit QC Batch = Quality Control Batch

Page 2 of 8 

## pc Batch

3177251 3177251 3177251 3177251 3177251 3177251

'Vt::n :.;;;In /•.nc-l!VUCS lmPrnatlonal Corporal!on o:a Maxxam AmlytJcs 6140 Campobello Road, MlssJssauga, Ontano, L5N 2L8 Tel: (905) 817-5700 Toll-free: 800-563-6266 Fax: (905) t3 "ll<"jl i 7 \',JWV'l.rna:.:xan1 t;a

# Ma?§i.am Keika Ventures Maxxam Job #: 8351214 Client Project#: Tl1550 Report Date: 2013/04/17 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Maxxam ID RC1448 Collected 2013/03/27 Sample ID BLANK-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10
Maxxam ID RC1449 Collected 2013/03/13 Sample ID RUN 1-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10

Maxxam ID RC1449 Dup Collected 2013/03/13 Sample ID RUN 1-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st ICP1/MS 3177251 2013/04/10 2013/04/12 Nan Ra kha
Maxxam ID RC1450 Collected 2013/03/13 Sample ID RUN 2-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st ICP1/MS 3177251 2013/04/10 2013/04/12 Nan Ra kha

Maxxam ID RC1451 Collected 2013/03/13 Sample ID RUN 3-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10
Maxxam ID RC1452 Collected 2013/03/13 Sample ID RUN 1-BAGH 5-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10

Maxxam ID RC1453 Collected 2013/03/13 Sample ID RUN 2-BAGH 5-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10

Page 3 of8

Maxxam /\nalyllcs lmernalional Gorporat1on o/a Maxxam**Anal~ltics** 6740 Campobello Road, MISSissauga, Ontario. L5N 2L8 Tel: (905} 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 \Y\Vw.maxxam.C<::I

## Ma({)lam
Maxxam Job #: 8351214 Report Date: 2013/04/17

Maxxam ID RC1454 Sample ID RUN 3-BAGH 5-M29 Matrix Stack Sampling Train Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244 Test Summary

Collected 2013/03/13 Shipped Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10

Page4 of8
f\lla'(,xarn t

...nalylics International Corporation o/a Maxxam Analytics 6740 Campobello Road, Mlssissauga, Ontarlo, L5N 2L8 Tel: (905)**817~5700 Toti~Free:**  800-563-6266 Fax: {905) 817-5777 www.ma'(xam.ca

# Ma?§i.am

Maxxam Job #: 8351214 Report Date: 2013/04/17 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244

ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN) Metals in Combined Train (6020): Extra 5x dilution was required for all samples except RC1448, due to the matrix Post digestion duplicate and spike was done on sample RC1449.

Results relate only to the items tested.

Page5of8

1\!lauam Analylics Jrnernational Corporation o/a Maxxam Analytics 6740 campobello Road, Mlsslssauga, Ontario, L5N 21.8 Tel: (905) 817·5700 Toll-Free: 80Q-563·6266 Fax: (905) 817-5777 www.maxxam.ca

## Ma-§.am

QA/QC Batch Num lnit QCTvoe 3177251 N_R Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSDRPD Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSD RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Method Blank RPD Method Blank RPD Method Blank RPD Method Blank RPD Method Blank RPD Method Blank RPDRPDSample/Sample Dup Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS

Quality Assurance Report Maxxam Job Number: GB351214 Date Analyzed Parameter vvvv/mrn/dd Combined Train Arsenic (As) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Nickel (Ni) 2013104/12
Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Value %Recoverv 98 7.4 103 6.0 104 5.9 109 7.6 126 13.6 105 6.9 98 6.1 99 7.2 98 5.4 102 5.9 101 5.4 101 6.6 <0.40

NC <0.10

NC <0.30

NC <0.20

NC <0.75

NC <0.50

NC

NC NC NC 2.3 1.4 NC Duplicate: Paired analysis of a separate portion ofthe same sample. Used to evaluate the variance in the measurement. Units % % % % % % % % % % % % % % % % % % % % % % % % ug % ug % ug % ug % ug % ug %

% % % % % %

Matrix Spike: A sample to which a known amount ofthe analyte of interest has been added. Used to evaluate sample matrix interference. QC Limits 70- 130 20 70- 130 20 70- 130 20 70- 130 20 70- 130 20 70- 130 20 85- 115 20 85- 115 20 85- 115 20 85- 115 20 85- 115 20 85- 115 20 20 20 20 20 20 20

20 20 20 20 20 20

Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.
Page 6 of8**'V~::l'xx<-~rn** twalvucs lntE'rnational r..orporallon o!a Maxxam Anatytics 67<10 C.arnpobeJio Road, Mlss1ssauga, ontarto,LSN 2L8 Tel: (905) 817

..5700**Toii~Free: 80()..563~6266**  Fax: (905)**817~':..•777** W\Vw.maxxam.t:.a

## Ma"f}i.a m Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS QualityAssurance Report (Continued) Maxxam Job Number: GB351214
NC (RPD): The RPD was not calculated. The level ofanalyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

Page7of8

Ma-.am AnalyUcs lrtternational COrporation o/a Maxxam Analytics 6740 Campobello**Roa~.** Mlssissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## Ma-§.am

Validation Signature Page
Maxxam Job #:8351214

The analytical dataand all QC contained in this reportwerereviewedand validatedbythe following individual(s).

FrankMo, B.Sc., Inorganic Lab. Manager

Maxxam has procedures inplace to guard against improperuse ofthe electronic signature andhave therequired "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing thereports. For Service Group specific validation pleaserefer to the Validation Signature Page.

Page8of8

1\ilaxxam Analytics lmernational COrporation o/a Maxxam Analylics 6740 GampoDello Road, Mlssissauga, Ontario, L5N 2L8 Tel: (905j 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# ,--...,.,_.,I.e-?;~**~.E~ ~**  _..... LJ.**.~·** 

# Sorbent Trap Analysis Report

Client Name 

### Keika Ventures, LLC Contact Name Lorri White Trap J.D. Plant/Source Date Analyzed Scientist 156035 Felman 4/10/2013 John Perko 150823 Felman 4/10/2013 John Perko 156060 Felman 4/10/2013 John Perko 156021 Felman 4/10/2013 John Perko 156066 Felman 4/10/2013 John Perko 156064 Felman 4/10/2013 John Perko 156014 Felman 4/10/2013 John Perko 150797 Felman 4/10/2013 John Perko 156042 Felman 4/10/2013 John Perko 156034 Felman 4/10/2013 John Perko 156058 Felman 4/10/2013 John Perko 156006 Felman 4/10/2013 John Perko 156057 Felman 4/10/2013 John Perko 156069 Felman 4/10/2013 John Perko 150824 Felman 4/10/2013 John Perko

Less than 0.027 ng is considered "< LDL." Which is less than the lowest detection limit. !Calibration ReportAvailable 

### I**~Variability** ±1O'VO! Massng Sect.1 0.86 21.06

0.67 0.65 0.51 0.73 0.65 21.20

0.61 19.31 17.28 28.22 26.06 22.55 45.09 Ohio Lumex Co., Inc. 9263 Ravenna Rd., Unit A-3 Twinsburg, OH 44087 Phone: (330) 405-0837 Fax: (330) 405-0847 v-......J.I'.fi

.. Jhi'J!umex.·.:'Jn:

Project Number 2001307 Turn -Around Time 

# 0 Standard 

# D 48 hour rush Other

Date 

### 4/11/2013 

### 919-933-9569 Phone

__

### ~~~~~~---- Massng Massng Spike Break

### Sect.2 Sect.3 Level (ng) through% Comments 0.74 Field Blank 0.54 20 Train Blank 0.54 Train Blank 0.61 #5 Baahouse, Center 0.52 #5 Baghouse, Center 0.74 #5 Baghouse, Center 0.55 #5 Baghouse, Center 0.74 20 #5 Baghouse, Center 0.47 #5 Baghouse, Center 0.72 #2 Baghouse, Center 0.72 #2 Baghouse, Center 0.87 #2 Baghouse, Center 0.72 #2 Baghouse, Center 0.73 #2 Baghouse, Center 0.57 20 #2 Baghouse, Center

# Mar:{)2.am
Your P.O.#: 10244

Your Project #: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Your C.O.C. #: N/A Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/04/29 

### CERTIFICATE OF ANALYSIS MAXXAM JOB#: 8351227 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train # Samples Received: 7
Analyses 2,3,7,8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A) Quantity 6 7 7 Date Extracted N/A 2013/04/16 2013/04/16 Date Analyzed Laboratory Method 2013/04/24 BRL SOP-00404 2013/04/25 BRL SOP-00404 2013/04/24 BRL SOP-00408, 409

* RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.
Encryption

### Key~ 

### ;/I Ancy Sebastian

### f/(;1.~P¥d.w- 29Apr 2013 23:03:49 -04:00 Please direct all qu O>UVIIO> ICl:JC:UUIII!:I und Certificate ofAnalysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Toxics Email: ASebastian@maxxam.ca Phone# (905) 817-5831 

## ==================================================================== Method Reference EPA1613Bmod(M23/23A) EPA1613Bmod(M23/23A) EPA 1668A (0010) mod

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of29

!\/laxxam Ana!vlics lmernalional COrporatiOn o.'a Maxxam Analytics 6740 Campobello Road, Mlssissauga, Ontano,l5N a..B Tel: (905)**817~5700** Toll-Free: 80o-563-6266 Fax: (905) 817-5777 W\'YW.max:xam.ca

# Ma(552arn

Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1495**~ampling** Date 2013/03/15 00:01 COC Number N/A TOXIC EQUIVALENCY Units TRAIN EDL RDL TEF (2005 WHO) TEQ(DL) BLANK-M23/PCB 33'44'-TetraCB-(77) ng 1.4 0.037 0.30 0.00010 0.00014 344'5-TetraCB-(81) ng 0.081 0.038 0.30 0.00030 0.000024 233'44'-PentaCB-(105) ng 1.4 0.032 0.30 0.000030 0.000042 2344'5-PentaCB-(114) ng 0.12 0.030 0.30 0.000030 0.0000036 23'44'5-PentaCB-(118) ng 3.9 0.032 0.30 0.000030 0.00012 23'44'5'-PentaCB-(123) ng 0.073 0.034 0.30 0.000030 0.0000022 33'44'5-PentaCB-(126) ng <0.031**~.031** 0.30 0.10 0.0031 HexaCB-(156)+(157) ng 0.17 0.033 0.60 0.000030 0.0000051 23'44'55'-HexaCB-(167) ng 0.069 0.035 0.30 0.000030 0.0000021 33'44'55'-HexaCB-(169) ng <0.037 0.037 0.30 0.030 0.0011 233'44'55'-HeptaCB-(189) ng <0.030 0.030 0.30 0.000030 0.00000090 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.0045 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 96 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 107 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 107 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 117 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 104 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 114 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 113 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 113 N/A N/A N/A N/A C13-33'44'55' -HexaCB-(169) % 97 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 117 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 119 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 119 N/A N/A N/A N/A N/A

### =Not Applicable RDL 

### =Reportable Detection Limit EDL 

### =Estimated Detection Limit QC Batch 

### = Quality Control Batch TEF 

### = Toxic Equivalency Factor, TEQ 

### = Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page2of29

l\.ila:o:nm t\na!vucs lmernational COrporation o..'a Max.xam Analylics 6740 Campobello Road, Mlssissauga, Ontario,l5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 8"17-5777**www.maxxam.1~**

# Ma?§i.am

Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
IMaxxam ID RC1497 !Sampling Date 2013/03/19 00:01 COC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) 1-BH2-M23/PCB 33'44'-TetraCB-(77) ng 4.3 0.036 0.30 0.00010 0.00043 344'5-TetraCB-(81) ng 0.26 0.037 0.30 0.00030 0.000078 233'44'-PentaCB-(105) ng 4.4 0.033 0.30 0.000030 0.00013 2344'5-PentaCB-(114) ng 0.36 0.031 0.30 0.000030 0.000011 23'44'5-PentaCB-(118) ng 12 0.033 0.30 0.000030 0.00036 23'44'5'-PentaCB-(123) ng 0.23 0.035 0.30 0.000030 0.0000069 33'44'5-PentaCB-(126) ng 0.081 0.032 0.30 0.10 0.0081 HexaCB-(156)+(157) ng 0.46 0.029 0.60 0.000030 0.000014 23'44'55'-HexaCB-(167) ng 0.18 0.031 0.30 0.000030 0.0000054 33'44'55'-HexaCB-(169) ng <0.033 0.033 0.30 0.030 0.00099 233'44'55'-HeptaCB-(189) ng <0.028 0.028 0.30 0.000030 0.00000084 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.010 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 95 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 109 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 109 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 114 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 107 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 118 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 116 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 115 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 106 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 117 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 121 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 115 N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF =Toxic Equivalency Factor, TEQ =Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page3of29
l\lla'(xam AnalyUcs lmernational COrporatiOn o/a Maxxam Anatytics 6740 campobello Road, Mlssissauga, Ontarto, l5N 2L8 Tel: (905) 817-5700**ToU~Free: 800~563~6266**  Fax: (905) 817-5777 \"11\'IIW.max.x.arn.ca

## Ma'62arn
Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1498 Sampling Date 2013/03/19 00:01 COC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) 2-BH2-M23/PCB 33'44'-TetraCB-(77) ng 2.6 0.036 0.30 0.00010 0.00026 344'5-TetraCB-(81) ng 0.15 0.036 0.30 0.00030 0.000045 233'44'-PentaCB-(105) ng 2.5 0.031 0.30 0.000030 0.000075 2344'5-PentaCB-(114) ng 0.20 0.029 0.30 0.000030 0.0000060 23'44'5-PentaCB-(118) ng 6.7 0.031 0.30 0.000030 0.00020 23'44'5'-PentaCB-(123) ng 0.11 0.033 0.30 0.000030 0.0000033 33'44'5-PentaCB-(126) ng 0.048 0.030 0.30 0.10 0.0048 HexaCB-(156)+(157) ng 0.25 0.034 0.60 0.000030 0.0000075 23'44'55'-HexaCB-(167) ng 0.11 0.036 0.30 0.000030 0.0000033 33'44'55'-HexaCB-(169) ng <0.037 0.037 0.30 0.030 0.0011 233'44'55'-HeptaCB-(189) ng <0.023 0.023 0.30 0.000030 0.00000069 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.0065 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 97 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 110 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 110 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 113 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 106 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 113 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 113 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 111 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 106 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 117 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 115 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 115 N/A N/A N/A N/A N/

A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF = Toxic Equivalency Factor, TEQ =Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page4of29

Ma<Xam Analylics lrnornational COrporation o!a Maxxam Analytics 6740 Campobello Road, Mlssissauga, Ontario, L5N 2L8 Tel: (905) 817·5700 Toii·Free: 800·563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?§}.am

Maxxam Job #: B351227 Report Date: 2013/04/29 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1499 Sampling Date 2013/03/19 00:01 

### roc Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL} 3-BH2-M23/PCB 33'44'-TetraCB-(77) ng 1.5 0.038 0.30 0.00010 0.00015 344'5-TetraCB-(81) ng 0.085 0.038 0.30 0.00030 0.000026 233'44'-PentaCB-(105) ng 1.4 0.032 0.30 0.000030 0.000042 2344'5-PentaCB-(114) ng 0.12 0.030 0.30 0.000030 0.0000036**~3'44'5-PentaCB-(118)** ng 3.9 0.032 0.30 0.000030 0.00012 23'44'5'-PentaCB-(123) ng 0.082 0.034 0.30 0.000030 0.0000025 33'44'5-PentaCB-(126) ng 0.033 0.031 0.30 0.10 0.0033 HexaCB-(156)+(157) ng 0.17 0.035 0.60 0.000030 0.0000051 23'44'55'-HexaCB-(167) ng 0.068 0.038 0.30 0.000030 0.0000020 33'44'55'-HexaCB-(169) ng <0.039 0.039 0.30 0.030 0.0012 233'44'55'-HeptaCB-(189) ng <0.023 0.023 0.30 0.000030 0.00000069 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.0049 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 94 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 102 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 102 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 109 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 100 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 106 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 105 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 103 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 90 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 113 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 110 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 111 N/A N/A N/A N/A N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 5 of29
\rlaxxam/\nalyucs lrnernalional CorporatiOn o:'a Maxxam**Anal~/tics** 6740 Campobello Road, MlsS1ssauga, OntariO, LSN 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.t.:a

# Ma?9-am
Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
IMaxxam ID RC1500**~ampling** Date 2013/03/15 00:01 OC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) 1-BH5-M23/PCB 33'44'-TetraCB-(77) ng 5.2 0.039 0.30 0.00010 0.00052 344'5-TetraCB-(81) ng 0.31 0.040 0.30 0.00030 0.000093 233'44'-PentaCB-(105) ng 5.4 p.031 0.30 0.000030 0.00016**~344'5-PentaCB-(**114) ng 0.42 0.030 0.30 0.000030 0.000013 23'44'5-PentaCB-(118) ng 15 0.031 0.30 0.000030 0.00045 23'44'5'-PentaCB-(123) ng 0.31 0.033 0.30 0.000030 0.0000093 33'44'5-PentaCB-(126) ng 0.10 0.031 0.30 0.10 0.010 HexaCB-(156)+(157) ng 0.52 0.033 0.60 0.000030 0.000016 23'44'55'-HexaCB-(167) ng 0.22 0.036 0.30 0.000030 0.0000066 33'44'55'-HexaCB-(169) ng <0.037 0.037 0.30 0.030 0.0011**~33'44'55'-HeptaCB-(189)** ng <0.026 0.026 0.30 0.000030 0.00000078 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.012 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 94 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 110 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 110 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 112 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 107 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 115 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 115 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 114 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 111 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 123 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 123 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 117 N/A N/A N/A N/A N/

A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ITEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, #of somers 

## pc Batch

N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A N/A

N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506

!The Total Toxic Equivalency (TEQ) value reported is the sum of Toxic Equivalent Quotients for the congeners tested. jwH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page6of29

Ma:o:.am /J,nalyucs lmernallonal COrporation o/a Max.xam Analylics 6740 Campobello Road, Mtssissa-.Jga, OntariO, LSN 2l8 Tel: (905) 8"17-5700 Toll-Free: 800-563-6266 Fax: {905) 817-5717\V\Vw.maxx.am.t:oo.i

## Ma§.am
Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1505 Sampling Date 2013/03/15 00:01 COC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) 2-BH5-M23/PCB 33'44'-TetraCB-(77) ng 8.4 0.037 0.30 0.00010 0.00084 344'5-TetraCB-(81) ng 0.48 0.038 0.30 0.00030 0.00014 233'44'-PentaCB-(105) ng 8.3 0.036 0.30 0.000030 0.00025 2344'5-PentaCB-(114) ng 0.69 0.034 0.30 0.000030 0.000021 23'44'5-PentaCB-(118) ng 23 0.036 0.30 0.000030 0.00069 23'44'5'-PentaCB-(123) ng 0.32 O.Q38 0.30 0.000030 0.0000096 33'44'5-PentaCB-(126) ng 0.16 0.035 0.30 0.10 0.016 HexaCB-(156)+(157) ng 0.76 0.032 0.60 0.000030 0.000023 23'44'55'-HexaCB-(167) ng 0.32 0.035 0.30 0.000030 0.0000096 33'44'55'-HexaCB-(169) ng <0.036 0.036 0.30 0.030 0.0011 233'44'55'-HeptaCB-(189) ng <0.029 0.029 0.30 0.000030 0.00000087 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.019 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 101 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 120 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 120 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 121 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 120 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 130 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 129 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 129 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 113 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 136 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 137 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 127 N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506**~H0(2005):** The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 7 of29**\·~::·ro.am** /•,nalvucs lrrrernauonal Gorporat10n o:a Maxxam Analytics 6"140 CampobeHo Road, MlssiSsauga, Ontario, L5N 2L8 Tel: (905) 817-5700**Toii~Free: 800-563~6266**  Fa>:: (905)**s·H~:)//7** www.rna-.;x.am**~~**

# Mar:{52arn

Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1511 Sampling Date 2013/03/15 00:01 OC Number N/A TOXIC EQUIVALENCY Units RUN EDL**~Dl** TEF (2005 WHO) TEQ(DL) 3-BH5-M23/PCB 33'44'-TetraCB-(77) ng 6.6 0.054 0.30 0.00010 0.00066 344'5-TetraCB-(81) ng 0.42 0.055 0.30 0.00030 0.00013 233'44'-PentaCB-(105) ng 6.2 0.037 0.30 0.000030 0.00019**~344'5-PentaCB-(114)** ng 0.51 0.035 0.30 0.000030 0.000015 23'44'5-PentaCB-(118) ng 17 0.038 0.30 0.000030 0.00051 23'44'5'-PentaCB-(123) ng 0.34 0.039 0.30 0.000030 0.000010 33'44'5-PentaCB-(126) ng 0.17 0.037 0.30 0.10 0.017 HexaCB-(156)+(157) ng 0.60 0.036 0.60 0.000030 0.000018 23'44'55'-HexaCB-(167) ng 0.23 0.038 0.30 0.000030 0.0000069 33'44'55'-HexaCB-(169) ng <0.040 0.040 0.30 0.030 0.0012**~33'44'55'-HeptaCB-(**189) ng <0.030 0.030 0.30 0.000030 0.00000090 ifOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.020 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 95 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 114 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 114 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 113 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 112 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 118 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 119 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 114 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 110 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 124 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 121 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 112 N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum of Toxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page8of29

1\i'.axxam Analyucs Jrnernational COrporatiOn o!a Maxxam Analytics 6740 Campobello Road, Mlss1ssauga, Ontaflo, L5N 2L8 Tel: (905) 817·5700 Toll-Free: SO!l-563·6266 Fax: (905) 817·5777 www.maxxam.ca

## Ma§am
Maxxam Job #: 8351227 Report Date: 2013/04/29

MaxxamiD Sampling Date 

### r-oc Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1495 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units TRAIN EDL RDL TEF (2005 WHO) fEQ(DL) somers BLANK-M23/PCB 2,3,7,8-Tetra COD* pg <3.7 3.7 30 1.00 3.70 N/A 1,2,3,7,8-Penta COD pg <7.7 7.7 30 1.00 7.70 N/A 1,2,3,4,7,8-Hexa COD pg <5.3 5.3 30 0.100 0.530 N/A 1,2,3,6,7,8-Hexa COD pg <5.2 5.2 30 0.100 0.520 N/A 1,2,3,7,8,9-Hexa COD pg <5.2 5.2 30 0.100 0.520 N/A 1,2,3,4,6,7,8-Hepta COD pg <6.4 6.4 30 0.0100 0.0640 N/A 1,2,3,4,6,7,8,9-0cta COD pg 8.2 (1) 5.2 300 0.000300 0.00246 N/A Total Tetra COD pg <3.7 3.7 30 N/A N/A N/A Total Penta COD pg <7.7 7.7 30 N/A N/A N/A Total Hexa COD pg <5.2 5.2 30 N/A N/A N/A Total Hepta COD pg <6.4 6.4 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <2.5 2.5 30 0.100 0.250 N/A 1,2,3,7,8-Penta CDF pg <7.6 7.6 30 0.0300 0.228 N/A 2,3,4,7,8-Penta CDF pg <7.2 7.2 30 0.300 2.16 N/A 1,2,3,4,7,8-Hexa CDF pg <3.9 3.9 30 0.100 0.390 N/A 1,2,3,6,7,8-Hexa CDF pg <3.8 3.8 30 0.100 0.380 N/A 2,3,4,6,7,8-Hexa CDF pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,7,8,9-Hexa CDF pg <5.3 5.3 30 0.100 0.530 N/A 1,2,3,4,6,7,8-Hepta CDF pg <2.9 2.9 30 0.0100 0.0290 N/A 1,2,3,4,7,8,9-Hepta CDF pg <4.0 4.0 30 0.0100 0.0400 N/A 1,2,3,4,6,7,8,9-0cta CDF pg <5.2 5.2 300 0.000300 0.00156 N/A Total Tetra CDF pg <2.5 2.5 30 N/A N/A N/A Total Penta CDF pg <7.4 7.4 30 N/A N/A N/A Total Hexa CDF pg <4.4 4.4 30 N/A N/A N/A Total Hepta CDF pg <3.4 3.4 30 N/A N/A N/A N/A

## = Not Applicable RDL

## = Reportable Detection Limit EDL

## = Estimated Detection Limit QC Batch

## = Quality Control Batch * COD 

## = Chloro Dibenzo-p-Dioxin, ** CDF

## = Chloro Dibenzo-p-Furan TEF

## = Toxic Equivalency Factor, TEO

## = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 9 of29

!Viauam Analyllcs l.nernational corporation o:a Maxxam Analytics 8740 CarnpoDeHo Road, MlssJSsauga, omar1o, L5N 2L8 Tel: (905) 817·5700 Toll-Free: 800..563·6266 Fax: {905) 817-5777 www.maxxam.ca

## Mar§l.am
Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date

OC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
DIOXINS AND FURANS BY HRMS {STACK SAMPLING TRAIN)
RC1495 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units TRAIN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers BLANK-M23/PCB TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 17.5 N/A Surrogate Recovery (%) C13-1234678 HeptaCDD * % 125 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF ** % 130 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 93 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 101 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 85 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 76 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 73 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 44 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 49 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 73 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 99 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 60 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 88 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 120 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 129 N/A N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEO =Toxic Equivalency Quotient, QC Batch

N/A

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 10 of29**\•1a~x!irn** Ana!ytJcs lrnernalional COrporation o/a Maxxam Analytics 6740 Campobello Road, Mlssissauga. Ontario,l5N 2l8 Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: {905) 817-5777**www.maxxam.1~**

# Ma?:{)2am

Maxxam Job #: 8351227 Report Date: 2013/04/29

MaxxamiD Sampling Date 

### roc Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1497 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL rrEF (2005 WHO) fEQ(DL) somers 1-BH2-M23/PCB 2,3,7,8-Tetra COD* pg <3.3 3.3 30 1.00 3.30 N/A 1,2,3,7,8-Penta COD pg <3.5 3.5 30 1.00 3.50 N/A 1,2,3,4,7,8-Hexa COD pg <4.9 4.9 30 0.100 0.490 N/A 1,2,3,6,7,8-Hexa COD pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,7,8,9-Hexa COD pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,4,6,7,8-Hepta COD pg 15.8 5.8 30 0.0100 0.158 N/A 1,2,3,4,6,7,8,9-0cta COD pg 30.4 5.3 300 0.000300 0.00912 N/A Total Tetra COD pg 123 3.3 30 N/A N/A N/A Total Penta COD pg 8.0 3.5 30 N/A N/A N/A Total Hexa COD pg 21.2 4.9 30 N/A N/A N/A Total Hepta COD pg 36.6 5.8 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <190 (1) 190 30 0.100 19.0 N/A 1,2,3,7,8-Penta CDF pg 21.2 4.6 30 0.0300 0.636 N/A 2,3,4,7,8-Penta CDF pg 23.4 (.2) 4.4 30 0.300 7.02 N/A 1,2,3,4,7,8-Hexa CDF pg 33.3 3.2 30 0.100 3.33 N/A 1,2,3,6,7,8-Hexa CDF pg 15.1 3.1 30 0.100 1.51 N/A 2,3,4,6,7,8-Hexa CDF pg 12.2 3.9 30 0.100 1.22 N/A 1,2,3,7,8,9-Hexa CDF pg <4.4 4.4 30 0.100 0.440 N/A 1,2,3,4,6,7,8-Hepta CDF pg 25.7 3.4 30 0.0100 0.257 N/A 1,2,3,4,7,8,9-Hepta CDF pg <4.6 4.6 30 0.0100 0.0460 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 16.1 (.2) 5.2 300 0.000300 0.00483 N/A Total Tetra CDF pg 1210 5.3 30 N/A N/A N/A Total Penta CDF pg 329 4.5 30 N/A N/A N/A Total Hexa CDF pg 124 3.6 30 N/A N/A N/A N/A

## =Not Applicable RDL

## =Reportable Detection Limit EDL

## =Estimated Detection Limit QC Batch 

## = Quality Control Batch * COD

## = Chloro Dibenzo-p-Dioxin, ** CDF

## = Chloro Dibenzo-p-Furan TEF

## = Toxic Equivalency Factor, TEQ

## = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) RT > 3 seconds
- PCDD/DF analysis
- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 2) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 11 of29**M::~·n..,m/-\naJvucs** International COrporation o/a Max.xam Analytics 67-10 Campobello Road, Mlssissauga, Ontarto, L5N 2l8 Tel: (905) 817-5700**Toii~Free:** 800-563-6266 Fax: (905) 817-5777 www.maxxarru..a

# Maf§2am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID !Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1497 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 1-BH2-M23/PCB Total Hepta CDF ** pg 34.9 3.9 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 39.8 3.2 30 0.100 3.98 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 26.9 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 78 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 112 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 115 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 93 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 103 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 91 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 80 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 79 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 77 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 86 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 77 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 97 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 66 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 90 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 112 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 127 N/A N/A N/A N/A N/A N/A

## = Not Applicable RDL 

## = Reportable Detection Limit EDL

## =Estimated Detection Limit QC Batch

## = Quality Control Batch • COD

## = Chloro Dibenzo-p-Dioxin, •• CDF

## = Chloro Dibenzo-p-Furan TEF

## = Toxic Equivalency Factor, TEQ

## = Toxic Equivalency Quotient, 

### pc Batch

3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. jwH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 12 of29**:Vla:~X::tfll/\nalvllcs** International COrporation o/a Maxxam AnalyliCS 6740 Campobello Road, Mlssissauga, Ontano, l5N 2l8 Tel: (905) 817-5700 Toll-Free: 80Q-563-6266 Fax: (905) 817-5777**\~lww.maxxam.ca**

# Ma?.S)2.am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID**~ampling** Date

OC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1498 2013103119 00:01 NIA TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 2-BH2-M231PCB 2,3,7,8-Tetra COD* pg <3.7 3.7 30 1.00 3.70 NIA 1,2,3,7,8-Penta COD pg <3.6 3.6 30 1.00 3.60 NIA 1,2,3,4,7,8-Hexa COD pg <3.6 3.6 30 0.100 0.360 NIA 1,2,3,6,7,8-Hexa COD pg <3.4 3.4 30 0.100 0.340 NIA 1,2,3,7,8,9-Hexa COD pg <3.5 3.5 30 0.100 0.350 NIA 1,2,3,4,6,7,8-Hepta COD pg <3.5 3.5 30 0.0100 0.0350 NIA 1,2,3,4,6,7,8,9-0cta COD pg 12.3 4.1 300 0.000300 0.00369 NIA Total Tetra COD pg 16.1 3.7 30 NIA NIA NIA Total Penta COD pg <4.0 (1) 4.0 30 NIA NIA NIA Total Hexa COD pg <9.6 (1) 9.6 30 NIA NIA NIA Total Hepta COD pg <3.5 3.5 30 NIA NIA NIA 2,3,7,8-Tetra CDF ** pg <53 (.2) 53 30 0.100 5.30 NIA 1,2,3,7,8-Penta CDF pg 5.9 3.5 30 0.0300 0.177 NIA 2,3,4,7,8-Penta CDF pg 6.0 3.3 30 0.300 1.80 NIA 1,2,3,4,7,8-Hexa CDF pg 8.0 3.4 30 0.100 0.800 NIA 1,2,3,6,7,8-Hexa CDF pg <3.2 3.2 30 0.100 0.320 NIA 2,3,4,6,7,8-Hexa CDF pg <4.1 4.1 30 0.100 0.410 NIA 1,2,3,7,8,9-Hexa CDF pg <4.5 4.5 30 0.100 0.450 NIA 1,2,3,4,6,7,8-Hepta CDF pg 5.9@) 2.3 30 0.0100 0.0590 NIA 1,2,3,4,7,8,9-Hepta CDF pg <3.1 3.1 30 0.0100 0.0310 NIA 1,2,3,4,6,7,8,9-0cta CDF pg <5.3 5.3 300 0.000300 0.00159 NIA Total Tetra CDF pg 335 4.5 30 NIA NIA NIA Total Penta CDF pg 67.8 3.4 30 NIA NIA NIA NIA

### =Not Applicable RDL 

### =Reportable Detection Limit EDL 

### =Estimated Detection Limit QC Batch 

### =Quality Control Batch * COD 

### = Chiaro Dibenzo-p-Dioxin, ** CDF

### = Chiaro Dibenzo-p-Furan TEF 

### = Toxic Equivalency Factor, TEQ

### = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I NOR
- Peak detected does not meet ratio criteria and has resulted in an elevated detection limit. ( 2) RT > 3 seconds
- PCDDIDF analysis
- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 3) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 13 of29

'·•la:·c,;.;:.,rn**t\nc-~lvucs** JmE:'rnatronal Gorpora11on o/a Maxxam Anaty-rics 6740 Campobello Road, MISSJSsauga, Ontarto, LSN 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 \Vww.maxxam.t.:a

## Ma"§.am

Maxxam Job #: 8351227 Report Date: 2013/04/29

MaxxamiD**~ampling** Date

OC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1498 I 2013/03/19 

# l 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) fEQ(DL) somers 2-BH2-M23/PCB Total Hexa CDF ** pg 18.3 3.7 30 N/A N/A N/A Total Hepta CDF pg 5.9 (1) 2.6 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 10.1 3.4 30 0.100 1.01 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 13.4 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 76 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 119 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 111 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 106 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 107 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 89 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 73 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 77 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 88 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 93 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 75 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 99 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 65 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 85 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 105 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 129 N/A N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * CDD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, 

## pc Batch

3190066 3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 14of29

Ma.<xam Analyllcs Jrnernalional COrporation o!a Maxxam**Anal~"tics** 6740 Campobello**Roa~.** Mlssissauga. Onlarlo. LSN 21..8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) !117-5117 www.m11uam.t.a

## Ma"§am
Maxxam Job #: 6351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1499 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 3-BH2-M23/PCB 2,3,7,8-Tetra COD* pg <4.1 4.1 30 1.00 4.10 N/A 1,2,3,7,8-Penta COD pg <4.1 4.1 30 1.00 4.10 N/A 1,2,3,4,7,8-Hexa COD pg <3.9 3.9 30 0.100 0.390 N/A 1,2,3,6,7,8-Hexa COD pg <3.8 3.8 30 0.100 0.380 N/A 1,2,3,7,8,9-Hexa COD pg <3.8 3.8 30 0.100 0.380 N/A 1,2,3,4,6,7,8-Hepta COD pg <3.2 3.2 30 0.0100 0.0320 N/A 1,2,3,4,6,7,8,9-0cta COD pg 7.7 3.3 300 0.000300 0.00231 N/A Total Tetra COD pg 24.8 4.1 30 N/A N/A N/A Total Penta COD pg 4.9 4.1 30 N/A N/A N/A Total Hexa COD pg <9.8 (1) 9.8 30 N/A N/A N/A Total Hepta COD pg <3.2 3.2 30 N/A NIA NIA 2,3,7,8-Tetra CDF ** pg <78 (2) 78 30 0.100 7.80 N/A 1,2,3,7,8-Penta CDF pg 9.7 4.4 30 0.0300 0.291 N/A 2,3,4,7,8-Penta CDF pg 12.6 4.2 30 0.300 3.78 NIA 1,2,3,4,7,8-Hexa CDF pg <13 (3) 13 30 0.100 1.30 NIA 1,2,3,6,7,8-Hexa CDF pg <5.2 (3) 5.2 30 0.100 0.520 NIA 2,3,4,6,7,8-Hexa CDF pg <4.1 4.1 30 0.100 0.410 NIA 1,2,3,7,8,9-Hexa CDF pg <4.5 4.5 30 0.100 0.450 N/A 1,2,3,4,6,7,8-Hepta CDF pg 7.2 (4) 2.9 30 0.0100 0.0720 NIA 1,2,3,4,7,8,9-Hepta CDF pg <4.0 4.0 30 0.0100 0.0400 NIA 1,2,3,4,6,7,8,9-0cta CDF pg 5.3 3.6 300 0.000300 0.00159 NIA Total Tetra CDF pg 455 2.9 30 NIA N/A NIA NIA =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chloro Dibenzo-p-Dioxin, •• CDF = Chloro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEQ =Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I NOR
- Peak detected does not meet ratio criteria and has resulted in an elevated detection limit. ( 2) RT > 3 seconds
- PCDD/DF analysis
- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 3) EMPC I OPE
- Diphenylether interference present caused dibenzofuran detected to become a "non-detect" with an elevated detection limit. ( 4) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 15 of29
:>;Ja.xam Analyucs lmernational COrporatiOn o!a Maxxam Analytics 6740 CampoDello Road. MlssiSsauga. Ontario. L5N 2L8 Tel: (905) 817-5700 Toll-Free: BOQ-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?:{)2am

Maxxam Job #: 8351227 Report Date: 2013/04/29

MaxxamiD Sampling Date COG Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1499 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) ITEQ(DL) somers 3·BH2-M23/PCB Total Penta CDF •• pg 126 4.3 30 N/A N/A N/A Total Hexa CDF pg 15.6 3.7 30 N/A N/A N/A Total Hepta CDF pg 7.2 (1) 3.4 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 15.0 3.0 30 0.100 1.50 N/A ifOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 17.7 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 71 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 97 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 101 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 99 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 96 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 93 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 73 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 81 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 84 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 83 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 76 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 105 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 57 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 77 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 98 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 124 N/A N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch • COD = Chloro Dibenzo-p-Dioxin, •• CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 16 of29

v.,·.x•m Anal'/l!GS lmernallollal <.orporatlon o!a Mal<Xam 1\nalyliCS 6740 C<Jrnpobello Road, Mlsslssauga, OntarJO,l5N 21.8 Tel: (905) 8.17·5700 Tofl·free: 80()..563·6266 Fax: (905) 817·5777 V.!Ww.maxxam ca

# Ma?.S}2am

Maxxam Job #: 8351227 Report Date: 2013/04/29

MaxxamiD Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1500 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 1-BH5-M23/PCB 2,3,7,8-Tetra COD* pg 6.7 (1) 3.5 30 1.00 6.70 N/A 1,2,3,7,8-Penta COD pg 3.5 2.8 30 1.00 3.50 N/A 1,2,3,4,7,8-Hexa COD pg <3.2 3.2 30 0.100 0.320 N/A 1,2,3,6,7,8-Hexa COD pg <3.1 3.1 30 0.100 0.310 N/A 1,2,3,7,8,9-Hexa COD pg <3.2 3.2 30 0.100 0.320 N/A 1,2,3,4,6,7,8-Hepta COD pg 5.2 (1) 3.4 30 0.0100 0.0520 N/A 1,2,3,4,6,7,8,9-0cta COD pg 11.9 (1) 3.1 300 0.000300 0.00357 N/A Total Tetra COD pg 121 3.5 30 N/A N/A N/A Total Penta COD pg 31.8 2.8 30 N/A N/A N/A Total Hexa COD pg 11.8 3.2 30 N/A N/A N/A Total Hepta COD pg 10.8 3.4 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg 220 3.1 30 0.100 22.0 N/A 1,2,3,7,8-Penta CDF pg 23.7 3.6 30 0.0300 0.711 N/A 2,3,4,7,8-Penta CDF pg 20.6 3.5 30 0.300 6.18 N/A 1,2,3,4,7,8-Hexa CDF pg 13.0 2.8 30 0.100 1.30 N/A 1,2,3,6,7,8-Hexa CDF pg 5.5 2.7 30 0.100 0.550 N/A 2,3,4,6,7,8-Hexa CDF pg <3.4 3.4 30 0.100 0.340 N/A 1,2,3,7,8,9-Hexa CDF pg <3.8 3.8 30 0.100 0.380 N/A 1,2,3,4,6,7,8-Hepta CDF pg 4.6 (1) 2.6 30 0.0100 0.0460 N/A 1,2,3,4,7,8,9-Hepta CDF pg <3.5 3.5 30 0.0100 0.0350 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 4.5 (1) 3.5 300 0.000300 0.00135 N/A Total Tetra CDF pg 1560 3.1 30 N/A N/A N/A Total Penta CDF pg 396 3.6 30 N/A N/A N/A Total Hexa CDF pg 46.1 3.1 30 N/A N/A N/A**~otal** Hepta CDF pg 4.6(1) 3.0 30 N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * CDD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEO = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 17 of29

Maxx"m AnalyLJcs Jmernational COrporation o1a Maxxarn Analylics 6140 Canpobello Road, Mlssissauga, Ontario, L5N 21..8 Tel: (905) 817-5700 Toll-free: soo-563-6266 fax: (905) 817-5777 www.maxxarn.ca

## Mar{)2am
Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1500 2013/03/15

00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) somers 1-BH5-M23/PCB Confirmation 2,3,7,8-Tetra CDF ** pg 54.4 3.2 30 0.100 5.44 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 26.2 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 65 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 96 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 107 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 106 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 104 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 89 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 91 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 89 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 88 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 84 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 80 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 114 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 58 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 71 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 108 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 127 N/A N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEO = Toxic Equivalency Quotient, 

## pc Batch

3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 18 of29**\·~;.J_x** xi'lrn /\nalyl!cs lnternalional Corporcnron o/a Max.xam Analy·iics 6740 Campobello Road,**MlSsrssa~Jga,** Onlano, L5l\l 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 8 ·n-5777 www.maxxanu
. .:aMaxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam 10 Sampling Date COC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1505 2013/03/15

00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) somers 2-BH5-M23/PCB 2,3,7,8-Tetra COD* pg 11.9 (1) 4.1 30 1.00 11.9 N/A 1,2,3,7,8-Penta COD pg 7.8 (1) 3.6 30 1.00 7.80 N/A 1,2,3,4,7,8-Hexa COD pg 4.5 3.2 30 0.100 0.450 N/A 1,2,3,6,7,8-Hexa COD pg 5.6 3.1 30 0.100 0.560 N/A 1,2,3,7,8,9-Hexa COD pg 6.0 3.2 30 0.100 0.600 N/A 1,2,3,4,6,7,8-Hepta COD pg 13.7 2.6 30 0.0100 0.137 N/A 1,2,3,4,6,7,8,9-0cta COD pg 37.8 5.4 300 0.000300 0.0113 N/A Total Tetra COD pg 194 4.1 30 N/A N/A N/A Total Penta COD pg 79.7 3.6 30 N/A N/A N/A Total Hexa COD pg 27.4 3.2 30 N/A N/A N/A Total Hepta COD pg 25.1 2.6 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <260 (2) 260 30 0.100 26.0 N/A 1,2,3,7,8-Penta CDF pg 32.9 4.9 30 0.0300 0.987 N/A 2,3,4,7,8-Penta CDF pg 28.7 4.6 30 0.300 8.61 N/A 1,2,3,4,7,8-Hexa CDF pg 20.2 (3) 3.6 30 0.100 2.02 N/A 1,2,3,6,7,8-Hexa CDF pg 11.3 (1) 3.4 30 0.100 1.13 N/A 2,3,4,6,7,8-Hexa CDF pg 8.4 4.3 30 0.100 0.840 N/A 1,2,3,7,8,9-Hexa CDF pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,4,6,7,8-Hepta CDF pg 10.9 (1) 2.6 30 0.0100 0.109 N/A 1,2,3,4,7,8,9-Hepta CDF pg <3.6 3.6 30 0.0100 0.0360 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 17.5 3.5 300 0.000300 0.00525 N/A Total Tetra CDF pg 1830 3.5 30 N/A N/A N/A Total Penta CDF pg 465 4.8 30 N/A N/A N/A N/A =Not Applicable RDL 

### =Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD 

### =Chiaro Dibenzo-p-Dioxin, ** CDF = Chiaro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ 

### =Toxic Equivalency Quotient, 

## pc Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical ( 2 ) RT > 3 seconds
- PCDD/DF analysis
- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 3 ) EMPC I Merged Peak

Page 19 of29**\·~~;_-.:..;~r1l/•,nc:~~vtJ;_;s** !mernat1oncll Corpora11on o/a Maxxam Analyt!CS 57<10 Campobello Road, Mlss1ssauga, Ontano, L5N 2L8 Tel· (905) 817-5700 Toll-Free· 800-563-6266 Fax: (905) 81l<J17? \VWw.m;:txxcuni..a

# Ma(!52am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1505 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 2-BH5-M23/PCB Total Hexa CDF •• pg 77.5 4.0 30 N/A N/A N/A Total Hepta CDF pg 10.9 (1) 3.0 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 68.7 6.5 30 0.100 6.87 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 42.5 N/A Surrogate Recovery(%) Confirmation C13-2378 TetraCDF % 53 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 99 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 100 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 104 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 105 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 88 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 79 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 77 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 75 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 66 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 73 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 134 (2) N/A N/A N/A N/A N/A C13-2378 TetraCDD % 49 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 53 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 98 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 165 (2) N/A N/A N/A N/A N/A N/A

## = Not Applicable RDL

## = Reportable Detection Limit EDL

## = Estimated Detection Limit QC Batch

## = Quality Control Batch • CDD

## = Chloro Dibenzo-p-Dioxin, ** CDF

## = Chloro Dibenzo-p-Furan TEF

## = Toxic Equivalency Factor, TEQ

## = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical (2) Field spike exceeds upper control limit (70-130%)

Page20of29

Mauam AnaiVl!CS lmernational COrporatiOn o!a Maxxam**Anal~'lics** 6740 campobello Road, MISSISsauga. 001ar1o, L5N 2L8 Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: (905) 817-5777 wwwmaxxam.ca

# Ma?!.}2am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COG Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1511 2013/03/15

00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) fEQ(DL) somers 3-BH5-M23/PCB 2,3,7,8-Tetra CDD * pg 9.5 (1) 3.5 30 1.00 9.50 N/A 1,2,3,7,8-Penta CDD pg 6.6 3.4 30 1.00 6.60 N/A 1,2,3,4,7,8-Hexa CDD pg <3.3 3.3 30 0.100 0.330 N/A 1,2,3,6,7,8-Hexa CDD pg <3.2 3.2 30 0.100 0.320 N/A 1,2,3,7,8,9-Hexa CDD pg 4.6 3.2 30 0.100 0.460 N/A 1,2,3,4,6,7,8-Hepta CDD pg 5.9 (1) 3.1 30 0.0100 0.0590 N/A 1,2,3,4,6,7,8,9-0cta CDD pg 26.5 (1) 4.7 300 0.000300 0.00795 N/A Total Tetra CDD pg 326 3.5 30 N/A N/A N/A Total Penta CDD pg 105 3.4 30 N/A N/A N/A Total Hexa CDD pg 4.6 3.3 30 N/A N/A N/A Total Hepta CDD pg 5.9 (1) 3.1 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <460 (2) 460 30 0.100 46.0 N/A 1,2,3,7,8-Penta CDF pg 46.3 3.8 30 0.0300 1.39 N/A 2,3,4,7,8-Penta CDF pg 38.1 3.6 30 0.300 11.4 N/A 1,2,3,4,7,8-Hexa CDF pg 26.8 2.5 30 0.100 2.68 N/A 1,2,3,6,7,8-Hexa CDF pg 13.4 2.3 30 0.100 1.34 N/A 2,3,4,6,7,8-Hexa CDF pg 5.1 3.0 30 0.100 0.510 N/A 1,2,3,7,8,9-Hexa CDF pg <3.3 3.3 30 0.100 0.330 N/A 1,2,3,4,6,7,8-Hepta CDF pg 10.1 (1) 3.7 30 0.0100 0.101 N/A 1,2,3,4,7,8,9-Hepta CDF pg <5.0 5.0 30 0.0100 0.0500 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 33.6 5.2 300 0.000300 0.0101 N/A Total Tetra CDF pg 3230 4.0 30 N/A N/A N/A Total Penta CDF pg 757 3.7 30 N/A N/A N/A Total Hexa CDF pg 118 2.7 30 N/A N/A N/A N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * CDD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEO= Toxic Equivalency Quotient, 

### pc Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical ( 2 ) RT > 3 seconds
- PCDD/DF analysis
- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds.

Page 21 of29

Ma.xxi.-lrn /\n<11VlJCS lmernational Corporauon o/a Maxxam Ana!ytics 6740 Campobello Road, Mlsstssauga, Ontario, L5N 2l8 Tel: (905) 817-5700 Toll-Free: 300-563-6266 Fax: (905) 817-5777 \'11\Vw.maxxam.t..a

# Ma~am Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date 

### r.oc Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1511 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 3-BH5-M23/PCB Total Hepta CDF ** pg 16.3 4.2 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 96.0 3.4 30 0.100 9.60 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 44.7 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 71 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 104 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 118 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 109 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 104 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 85 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 79 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 85 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 81 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 86 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 82 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 98 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 59 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 76 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 95 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 125 N/A N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chiaro Dibenzo-p-Dioxin, ** CDF = Chiaro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, QC Batch

3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page22 of29

l\fl.a'<xam t
...nalvucs lrnernational Corporation o:a Maxxam**Anal~"tics** 6740 Campobello Road, Mlssissat.Jga, Ontario, L5N 2LB Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 \'V\'IJW.maxxam.t:;a

# Ma?§).am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Test Maxxam ID RC1495 Sample ID TRAIN BLANK-M23/PCB Matrix Stack Sampling Train

Maxxam ID RC1497 Sample ID RUN 1-BH2-M23/PCB Matrix Stack Sampling Train Descr1pt1on 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Conoeners in Air (1668A)

Maxxam ID RC1498 Sample ID RUN 2-BH2-M23/PCB Matrix Stack Sampling Train T D

est escnpt1on 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air(Method 23) PCB Congeners in Air (1668A)

Maxxam ID RC1499 Sample ID RUN 3-BH2-M23/PCB Matrix Stack Sampling Train Test Description 12 3 7 8-TCDF Confirmation CM23) IDioxins/Furans in Air (Method 23) IPCB Conoeners in Air (1668A)

Maxxam ID RC1500 Sample ID RUN 1-BH5-M23/PCB Matrix Stack Sampling Train T tD

es 't' escnpuon 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A) Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
Test Summary

Instrumentation Batch Extracted HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

nstrumentatlon B h ate E xtracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

I tr ns umen tation B t h ac Ext cted ra HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Instrumentation Batch Extracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

I t ns rumen tat' IOn B t h ac E t ct d x ra e HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Page23of29 A I d na1yze 2013/04/24 2013/04/25 2013/04/24

A I d

na1yze 2013/04/24 2013/04/25 2013/04/24

Analyzed 2013/04/24 2013/04/25 2013/04/24

A I d

na1yze 2013/04/24 2013/04/25 2013/04/24 Collected 2013/03/15 Shipped Received 2013/04/06

Collected 2013/03/19

Shipped Received 2013/04/06 A I

na1yst Vica Cioranic Owen Cosby CathvXu
Collected 2013/03/19

Shipped Received 2013/04/06

A I t

na1ys Vica Cioranic OwenCosbv Cathy Xu
Collected 2013/03/19

Shipped Received 2013/04/06

Analyst Vica Cioranic Owen Cosby CathvXu
Collected 2013/03/15

Shipped Received 2013/04/06

A I t

na1ys Vica Cioranic OwenCosbv Cathy Xu

Ma<>am Analylics lmernational COrporation o!a MaJU<am**Anal~'lics** 6740 GampobeDo Road, MISSISsauga, OntariO, L5N 21.8 Tel: (905) 817-5700 Toll-Free: 80Q-563-6266 Fax: (905) 817-f>777 www.maxxam.ca

# Ma?Y2am
Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID RC1505 Sample ID RUN 2-BH5-M23/PCB Matrix Stack Sampling Train T D

est I i escr1pt on 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A)

Maxxam ID RC1511 Sample ID RUN 3-BH5-M23/PCB Matrix Stack Sampling Train Test Description 12,3,7 8-TCDF Confirmation (M23) 

### IDioxins/Furans in Air (Method 23) 

### IPCB Conaeners in Air C1668A) Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
Test Summary

nstrumentat on B h ate E xtracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Instrumentation Batch Extracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Page24 of29 A I d na1yze 2013/04/24 2013/04/25 2013/04/24

Analvzed 2013/04/24 2013/04/25 2013/04/24 Collected 2013/03/15 Shipped Received 2013/04/06 Analyst Vica Cioranic Owen Cosby Cathy Xu
Collected 2013/03/15

Shipped Received 2013/04/06 Analvst Vica Cioranic Owen Cosby_ CathvXu

Manam AnaiV!IGs lrnernatlonal Corporation ola l\llaxxam Analy!lcs 6740**C<~rnpoDello** Road,l\lllll!!ll!sauga, Ontario, L5N 21.6 Tel: (1105) 817·5700 Toii·Free: 80()-563·6266 Fax: (905) 817·5777 www.ma><"am.r.a

## M 

# af.S52arn

Maxxam Job #: 8351227 Report Date: 2013/04/29

Results relate onlyto the items tested. Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244

GENERAL COMMENTS

Page 25 of29
'\ii:·n;**x~~n /o~,na!vllc-::**  lmernational Gorpor<11.1on o:a**Max:~~;**am Analylics 0740 Campobello Road, MlssJssauga, 0n1ar1o, L5N 2L8 Tel: (905'**817~5700** Toll-Free: 800-563-6266 Fax: {905) a·17-G777 \".1\Vw.maxx.am.i.:a

## Ma[{)2am

QA/QC Batch Num lnit QCType 3182506 

### cxu Spiked Blank

RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Method Blank Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS QualityAssurance Report Maxxam Job Number: GB351227 Date Analyzed Parameter vvvv/mm/dd C13-233'44'55'-HeptaCB-(189) 2013/04/24 C13-233'44'5-HexaCB-(156) 2013/04/24 C13-233'44'5'-HexaCB-(157) 2013/04/24 C13-233'44'-PentaCB-(105) 2013/04/24 C13-23'44'55'-HexaCB-(167) 2013/04/24 C13-2344'5-PentaCB-(114) 2013/04/24 C13-23'44'5-PentaCB-(118) 2013/04/24 C13-2'344'5-PentaCB-(123) 2013/04/24 C13-33'44'55'-HexaCB-(169) 2013/04/24 C13-33'44'5-PentaCB-(126) 2013/04/24 C13-33'44'-TetraCB-(77) 2013/04/24 C13-344'5-TetraCB-(81) 2013/04/24 33'44'-TetraCB-(77) 2013/04/24 33'44'-TetraCB-(77) 2013/04/24 344'5-TetraCB-(81) 2013/04/24 344'5-TetraCB-(81) 2013/04/24 233'44'-PentaCB-(105) 2013/04/24 233'44'-PentaCB-(105) 2013/04/24 2344'5-PentaCB-(114) 2013/04/24 2344'5-PentaCB-(114) 2013/04/24 23'44'5-PentaCB-(118) 2013/04/24 23'44'5-PentaCB-(118) 2013/04/24 23'44'5'-PentaCB-(123) 2013/04/24 23'44'5'-PentaCB-(123) 2013/04/24 33'44'5-PentaCB-(126) 2013/04/24 33'44'5-PentaCB-(126) 2013/04/24 HexaCB-(156)+(157) 2013/04/24 HexaCB-(156)+(157) 2013/04/24 23'44'55'-HexaCB-(167) 2013/04/24 23'44'55'-HexaCB-(167) 2013/04/24 33'44'55'-HexaCB-(169) 2013/04/24 33'44'55'-HexaCB-(169) 2013/04/24 233'44'55'-HeptaCB-(189) 2013/04/24 233'44'55'-HeptaCB-(189) 2013/04/24 C13-233'44'55'-HeptaCB-(189) 2013/04/24 C13-233'44'5-HexaCB-(156) 2013/04/24 C13-233'44'5'-HexaCB-(157) 2013/04/24 C13-233'44'-PentaCB-(105) 2013/04/24 C13-23'44'55'-HexaCB-(167) 2013/04/24 C13-2344'5-PentaCB-(114) 2013/04/24 C13-23'44'5-PentaCB-(118) 2013/04/24 C13-2'344'5-PentaCB-(123) 2013/04/24 C13-33'44'55'-HexaCB-(169) 2013/04/24 C13-33'44'5-PentaCB-(126) 2013/04/24 C13-33'44'-TetraCB-(77) 2013/04/24 C13-344'5-TetraCB-(81) 2013/04/24 33'44'-TetraCB-(77) 2013/04/24 344'5-TetraCB-(81) 2013/04/24 233'44'-PentaCB-(105) 2013/04/24 2344'5-PentaCB-(114) 2013/04/24 23'44'5-PentaCB-(118) 2013/04/24 23'44'5'-PentaCB-(123) 2013/04/24 33'44'5-PentaCB-(126) 2013/04/24 HexaCB-(156)+(157) 2013/04/24 23'44'55'-HexaCB-(167) 2013/04/24

Page26of29 Value %Recoverv 98 108 108 111 107 108 108 107 104 120 112 107 98 0 99 0 99 1.0 96 1.0 98 3.0 99 1.0 93 4.2 100 1.0 100

0 102 0 93 2.1 102 115 115 115 111 115 113 113 106 123 116 113 <0.037, EDL=0.037 <0.037, EDL=0.037 <0.030, EDL=0.030 <0.028, EDL=0.028 <0.030, EDL=0.030 <0.031, EDL=0.031 <0.029, EDL=0.029 <0.036, EDL=0.036 <0.039, EDL=0.039 Units QC Limits % 20- 150 % 20-150 % 20-150 % 20-150 % 20- 150 % 20-150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % N/A % 20- 150 % 20- 150 % 20- 150 % 20-150 % 20-150 % 20-150 % 20- 150 % 20- 150 % 20-150 % 20-150 % 20- 150 % 20- 150 ng ng ng ng ng ng ng ng ng

Mauam Analytics Jrnernational COrporation ola Maxxam Analytics 6740 GampobeHo**Roa~.** MlssiSsauga, Ontano, L5111 2LB Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?§J.am

QNQC Batch Num lnit QCType 3182506 

### cxu Method Blank 3190066 OBC Spiked Blank

RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Method Blank Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O. #: 10244 Site Location: TEST INC. -FELMAN PRODUCTIONS QualityAssurance Report (Continued) Maxxam Job Number: GB351227 Date Analyzed Parameter yyyy/mm/dd 33'44'55'-HexaCB-(169) 2013/04/24 233'44'55'-HeptaCB-(189) 2013/04/24 C13-1234678 HeptaCDD 2013/04/25 C13-1234678 HeptaCDF 2013/04/25 C13-123678 HexaCDD 2013/04/25 C13-123678 HexaCDF 2013/04/25 C13-12378 PentaCDD 2013/04/25 C13-12378 PentaCDF 2013/04/25 C13-123789 HexaCDF 2013/04/25 C13-2378 TetraCDD 2013/04/25 C13-2378 TetraCDF 2013/04/25 C13-0ctachlorodibenzo-p-Dioxin 2013/04/25 2,3,7,8-Tetra COD 2013/04/25 2,3,7,8-Tetra COD 2013/04/25 1,2,3,7,8-Penta COD 2013/04/25 1,2,3,7,8-Penta COD 2013/04/25 1,2,3,4,7,8-Hexa COD 2013/04/25 1,2,3,4,7,8-Hexa COD 2013/04/25 1,2,3,6,7,8-Hexa COD 2013/04/25 1,2,3,6,7,8-Hexa COD 2013/04/25 1,2,3,7,8,9-Hexa COD 2013/04/25 1,2,3,7,8,9-Hexa COD 2013/04/25 1,2,3,4,6,7,8-Hepta COD 2013/04/25 1,2,3,4,6,7,8-Hepta COD 2013/04/25 1,2,3,4,6,7,8,9-0cta COD 2013/04/25 1,2,3,4,6,7,8,9-0cta COD 2013/04/25 2,3,7,8-Tetra CDF 2013/04/25 2,3,7,8-Tetra CDF 2013/04/25 1,2,3,7,8-Penta CDF 2013/04/25 1,2,3,7,8-Penta CDF 2013/04/25 2,3,4,7,8-Penta CDF 2013/04/25 2,3,4,7,8-Penta CDF 2013/04/25 1,2,3,4,7,8-Hexa CDF 2013/04/25 1,2,3,4,7,8-Hexa CDF 2013/04/25 1,2,3,6,7,8-Hexa CDF 2013/04/25 1,2,3,6,7,8-Hexa CDF 2013/04/25 2,3,4,6,7,8-Hexa CDF 2013/04/25 2,3,4,6,7,8-Hexa CDF 2013/04/25 1,2,3,7,8,9-Hexa CDF 2013/04/25 1,2,3,7,8,9-Hexa CDF 2013/04/25 1,2,3,4,6,7,8-Hepta CDF 2013/04/25 1,2,3,4,6,7,8-Hepta CDF 2013/04/25 1,2,3,4,7,8,9-Hepta CDF 2013/04/25 1,2,3,4,7,8,9-Hepta CDF 2013/04/25 1,2,3,4,6,7,8,9-0cta CDF 2013/04/25 1,2,3,4,6,7,8,9-0cta CDF 2013/04/25 C13-1234678 HeptaCDD 2013/04/25 C13-1234678 HeptaCDF 2013/04/25 C13-123678 HexaCDD 2013/04/25 C13-123678 HexaCDF 2013/04/25 C13-12378 PentaCDD 2013/04/25 C13-12378 PentaCDF 2013/04/25 C13-123789 HexaCDF 2013/04/25 C13-2378 TetraCDD 2013/04/25 C13-2378 TetraCDF 2013/04/25

Page27of29 Value %Recovery <0.040, EDL=0.040 <0.014, EDL=0.014 115 115 77 70 70 68 73 41 57 100 113 NC 118 NC 98 NC 109 NC 131 NC 98 NC 95 NC 99 NC 104 NC 114 NC 103 NC 115 NC 122 NC 127 NC 90 NC 87 NC 99 NC 119 114 72 71 67 69 75 45 66 Units QC Limits ng ng % 25- 130 % 25-130 % 40-130 % 40- 130 % 40- 130 % 40-130 % 40- 130 % 40- 130 % 40- 130 % 25-130 % 80-140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80-140 % 20 % 80-140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80-140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80-140 % 20 % 80- 140 % 20 % 25-130 % 25-130 % 40- 130 % 40- 130 % 40-130 % 40- 130 % 40- 130 % 40- 130 % 40- 130

Ma'Xam Analylics Jrnernational Corporation o!a Maxxam Analytics 6740 Campobello Road. Mlss1ssauga. Ontario. L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?§}.am

QNQC Batch Num lnit QCType 3190066 OBC Method Blank

3191218 VCI Method Blank Keika Ventures Attention: lorri L White Client Project #: Tl1550 P.O.#: 10244 Site location: TEST INC. -FELMAN PRODUCTIONS QualityAssurance Report (Continued) Maxxam Job Number: GB351227 Date Analyzed Parameter yyyy/mm/dd C13-0ctachlorodibenzo-p-Dioxin 2013/04/25 2,3,7,8-Tetra CDD 2013/04/25 1,2,3,7,8-Penta CDD 2013/04/25 1,2,3,4,7,8-Hexa CDD 2013/04/25 1,2,3,6,7,8-Hexa CDD 2013/04/25 1,2,3,7,8,9-Hexa CDD 2013/04/25 1,2,3,4,6,7,8-Hepta CDD 2013/04/25 1,2,3,4,6,7,8,9-0cta CDD 2013/04/25 Total Tetra CDD 2013/04/25 Total Penta CDD 2013/04/25 Total Hexa CDD 2013/04/25 Total Hepta CDD 2013/04/25 2,3,7,8-Tetra CDF 2013/04/25 1,2,3,7,8-Penta CDF 2013/04/25 2,3,4,7,8-Penta CDF 2013/04/25 1,2,3,4,7,8-Hexa CDF 2013/04/25 1,2,3,6,7,8-Hexa CDF 2013/04/25 2,3,4,6,7,8-Hexa CDF 2013/04/25 1,2,3,7,8,9-Hexa CDF 2013/04/25 1,2,3,4,6,7,8-Hepta CDF 2013/04/25 1,2,3,4,7,8,9-Hepta CDF 2013/04/25 1,2,3,4,6,7,8,9-0cta CDF 2013/04/25 Total Tetra CDF 2013/04/25 Total Penta CDF 2013/04/25 Total Hexa CDF 2013/04/25 Total Hepta CDF 2013/04/25 Confirmation C13-2378 TetraCDF 2013/04/24 Confirmation 2 3 7 8-Tetra CDF 2013/04/24 Value %Recovery 119 <6.7, EDL=6.7 <7.4, EDL=7.4 <6.5, EDL=6.5 <6.3, EDL=6.3 <6.4, EDL=6.4 <7.4, EDL=7.4 <6.4, EDL=6.4 <6.7, EDL=6.7 <7.4, EDL=7.4 <6.4, EDL=6.4 <7.4, EDL=7.4 <2.9, EDL=2.9 <7.0, EDL=7.0 <6.6, EDL=6.6 <3.0, EDL=3.0 <2.9, EDL=2.9 <3.6, EDL=3.6 <4.0, EDL=4.0 <3.6, EDL=3.6 <4.9, EDL=4.9 <7.1, EDL=7.1 <2.9, EDL=2.9 <6.8, EDL=6.8 <3.3, EDL=3.3 <4.1, EDL=4.1 61 <3.2 EDL=3.2 Duplicate: Paired analysis of a separate portion ofthe same sample. Used to evaluate the variance in the measurement. Units QC Limits % 25-130 pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg % 40-135 PQ Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency. NC (RPD): The RPD was not calculated. The level ofanalyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

Page28of29

Mauam AnalyUos International COrporation o/a Maxxam Analylics 6740 campobello Road. Mlssissauga. Ontario. L5N 2L8 Tel: (905) 817-5700 Toll-Free: 80D-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?SJ.am
Validation Signature Page


### Maxxam Job #:8351227

The analytical data and all QC contained inthis report were reviewed and validated bythe following individual(s).

Branko Vrzic, A.SC.T., Senior Analyst, HRMS Services

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page 29 of29

Ma.xxam AnalvUcs International CorporatJon o!a Max.xam Analytics 5740 Campobello Road, Mlsslssauga, Ontario, L5N 2L8 Tel: {905) 817-5700 Toll-Free:**800~563-6266** Fax: (905) 817-5777 Vif\'YW.maxxam.ca

## Ma"§.am
Your P.O.#: 10244
Your Project #: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Your C.O.C. #: N/A Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/05/02 

### CERTIFICATE OFANALYSIS MAXXAM JOB#: 8351259 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train # Samples Received: 7
Analyses PAH's in Air (CARB429) Date Date Quantity Extracted Analyzed Laboratory Method 7 2013/04/16 2013/05/01 BRL SOP-00418

* RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.
Encryption KeyE 

### ;/I 1 kocy Sebastian**v~~-** 02 May201316:52:06-04:00 Please direct all qu :suum•**""!::l~tunty** um:l Certificate ofAnalysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Toxics Email: ASebastian@maxxam.ca Phone# (905) 817-5831 

## ==================================================================== Method Reference CARB 429mod(CARB429)

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of 12

1\ilaxxam Analytics lmernational Corporation ola Maxxam Analytics 6740 campobeno Roao. Mlssissauga, Ontario. L5N 21.8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817·5717 www.m1"'xam.oo

# Ma62-am
Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1605 RC1606 RC1607**~ampling** Date 2013/03/14 2013/03/18 2013/03/18 00:01 00:01 00:01 COC Number N/A N/A N/A Units TRAIN :;oL RDL RUN 1-BH2-PAH EDL RDL RUN 2-BH2-PAH BLANK-PAH Naphthalene ng 761 24 10 27400 (1) 1400 500 48800 (1) 2-Methylnaphthalene ng 329 18 10 21700 490 500 42900 (1) 2-Chloronaphthalene ng <1.8 1.8 10 46.6 1.2 10 94.2 Acenaphthylene ng <35 35 10 2600 140 500 3060 Acenaphthene ng <62 62 10 1730 940 500 2230 Fluorene ng 166 20 10 2230 300 500 3290 Phenanthrene ng 435 23 10 13400 480 500 25100 (1) Anthracene ng <27 27 10 1040 570 500 1180 Fluoranthene ng 19.6 6.8 10 11100 590 500 73500 (1) Pyrena ng 10.9 6.3 10 5200 550 500 42700 (1) Benzo(a)anthracene ng <5.9 5.9 10 618 150 500 3260 Chrysene ng <6.1 6.1 10 3660 140 500 29000 (1) Benzo(b)fluoranthene ng <2.0 2.0 10 503 60 500 3320 Benzo(k)fluoranthene ng <3.3 3.3 10 172 35 10 1310 Benzo(e)pyrene ng <4.8 4.8 10 364 30 10 1950 Benzo(a)pyrene ng <6.1 6.1 10 <37 37 10 <60 Perylene ng <3.5 3.5 10 <33 33 10 <55 lndeno(1 ,2,3-cd)pyrene ng <5.2 5.2 10 27.7 6.8 10 71.3 Dibenz(a,h)anthracene ng <3.9 3.9 10 <4.7 4.7 10 9.6 Benzo(g,h,i)perylene ng <4.7**~.7** 10 36.4 6.7 10 81.5 Coronene ng <10 10 10 12.6 2.9 10 23.6 Surrogate Recovery (%) 2-Methylnaphthalene-2H10 o/o 66 NtA N/A 55 N/A N/A 43 (2) Acenaphthylene-2H8 o/o 64 NtA N/A 78 N/A N/A 67 Anthracene-2H10 o/o 42 (2) NtA N/A 95 N/A N/A 72 Benz(a)anthracene-2H12 o/o 98**~/A** N/A 74 N/A N/A 142 Benzo(a)pyrene-2H12 o/o 48 (2) N/A N/A 93 N/A N/A 90 Benzo(b)fluoranthene-2H12 o/o 76 N/A N/A 109 N/A N/A 91 Benzo(g,h,i)perylene-2H12 o/o 54 N/A N/A 97 N/A N/A 96 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ( 1 ) EMCL
- PAH analysis
- Exceeds Maximum Calibration Limit FDL RDL**~c** Batch

700 500 3182508 300 500 3182508 1.2 10 3182508 66 500 3182508 550 500 3182508 190 500 3182508 390 500 3182508 450 500 3182508 550 500 3182508 510 500 3182508 130 500 3182508 180 500 3182508 45 500 3182508 87 500 3182508 58 500 3182508 60 10 3182508 55 10 3182508 9.0 10 3182508 4.5 10 3182508 9.5 10 3182508 4.3 10 3182508

N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 2 of 12
!V;,.xxem Analyucs lrnernalional Corporation ora Maxxam Analytics 6740 Campobello Road. Mlssissauga. omar•o. L5N 21.8 Tel: (905) 817-5700 Toll-Free: 800..563-6266 Fax: (905) 817-5777 www.maxxam.r..a

# Ma?§l.am

Maxxam Job #:8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1605 RC1606 RC1607**~ampling** Date 2013/03/14 2013/03/18 2013/03/18 00:01 00:01 00:01 COG Number N/A N/A N/A Units TRAIN i;DL RDL RUN 1-BH2·PAH EDL RDL RUN 2·BH2·PAH BLANK·PAH Benzo(k)fluoranthene-2H12 % 75 1'-JIA N/A 98 N/A N/A 65 Chrysene-2H12 % 80 N!A N/A 59 N/A N/A 91 Dibenzo(a,h)anthracene-2H14 % 53 N!A N/A 115 N/A N/A 120 Fluoranthene-2H10 % 79 NtA N/A 88 N/A N/A 88 Fluorene-2H10 % 123 NtA N/A 70 N/A N/A 68 lndeno(1,2,3-c,d)pyrene-2H12 % 51 NtA N/A 98 N/A N/A 103 Naphthalene-2H8 % 71 NtA N/A 46 (1) N/A N/A 35 (1) Perylene-2H12 % 54**~/A** N/A 83 N/A N/A 75 Phenanthrene-2H10 % 44 (1) NtA N/A 110 N/A N/A 105 Terphenyi-2H14 % 108 N!A N/A 137 N/A N/A 153 (1) N/A

### =Not Applicable RDL

### =Reportable Detection Umit EDL 

### =Estimated Detection Umit QC Batch 

### = Quality Control Batch FDL RDL**~c** Batch

N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 3 of 12

Ma.xxem Ana!yllcs lrnerna1ional C',orporation o/a Maxxam Analyllcs 6740 Campobello Road, Mlssissauga, Ontario, L5N 2LB Tel: (905) 817·5700 Toii·Free: 800·563·6266 Fax: {905) 817·5777 www.maxxam.r.:a

# Ma?:52am

Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1608 RC1609 RC1610 Sampling Date 2013/03/18 2013/03/14 2013/03/14 00:01 00:01 00:01 COC Number N/A N/A N/A Units RUN 3-BH2-PAH EDL RUN 1-BH5-PAH EDL RDL RUN 2-BH5-PAH Naphthalene ng 43800 (1) 480 45100 (1) 330 500 28600 (1) 2-Methylnaphthalene ng 29700 (1) 310 19200 120 500 15900 2-Chloronaphthalene ng 92.6 0.84 81.0 0.40 10 72.8 Acenaphthylene ng 4570 67 9040 89 500 4780 Acenaphthene ng 2520 490 4030 330 500 2680 Fluorene ng 3480 170 5080 220 500 2950 Phenanthrene ng 22400 230 67100 (1) 430 500 53400 (1) Anthracene ng 1630 270 2170 500 500 2650 Fluoranthene ng 15100 440 45700 (1) 310 500 43000 (1) Pyrena ng 7790 410 23000 290 500 26600 Benzo(a)anthracene ng 672 69 1210 110 500 1300 Chrysene ng 3830 80 6850 120 500 4500 Benzo(b)fluoranthene ng 902 30 956 120 500 466 Benzo(k)fluoranthene ng 246 15 344 16 10 135 Benzo(e)pyrene ng 519 33 1150 230 500 477 Benzo(a)pyrene ng 21 16 <27 27 10 <16 Perylene ng <15 15 <18 18 10 <11 lndeno(1 ,2,3-cd)pyrene ng 52.4 7.0 50.6 6.6 10 16.6 Dibenz(a,h)anthracene ng 9.6 3.5 8.5 3.8 10 <2.8 Benzo(g,h,i)perylene ng 64.5 7.0 58.9 6.9 10 25.2 Coronene ng 44.7 4.3 32.2 4.2 10 12.8 Surrogate Recovery (%) 2-Methylnaphthalene-2H10 % 47 (2) N/A 47 (2) N/A N/A 49 (2) Acenaphthylene-2H8 % 62 N/A 52 N/A N/A 57 Anthracene-2H10 % 69 N/A 55 N/A N/A 53 Benz(a)anthracene-2H12 % 127 N/A 95 N/A N/A 107 Benzo(a)pyrene-2H12 % 107 N/A 65 N/A N/A 54 Benzo(b)fluoranthene-2H12 % 111 N/A 111 N/A N/A 115 Benzo(g,h,i)perylene-2H12 % 103 N/A 98 N/A N/A 92 N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ( 1 ) EMCL
- PAH analysis
- Exceeds Maximum Calibration Limit EDL RDL QC Batch 320 500 3182508 130 500 3182508 1.2 10 3182508 49 500 3182508 320 500 3182508 150 500 3182508 330 500 3182508 390 500 3182508 320 500 3182508 300 500 3182508 72 500 3182508 94 500 3182508 5.4 10 3182508 9.1 10 3182508 13 10 3182508 16 10 3182508 11 10 3182508 3.6 10 3182508 2.8 10 3182508 3.7 10 3182508 2.6 10 3182508

N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 4 of 12**1\'~::~'o:.am** Ana!vucs 1mernat1ona1 Corporation ota Maxxam Analytics 6740 CarnpoiJeiJo Roac1, Mlsslssauga, Ontarlo,LSN 2L8 Tel: (905) 817

..5700**Toii~Free:** 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma"62am

Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
MaxxamiD RC1608 RC1609 RC1610 Sampling Date 2013/03/18 2013/03/14 2013/03/14 00:01 00:01 00:01 OC Number N/A N/A N/A Units RUN 3-BH2-PAH EDL RUN 1-BH5-PAH EDL RDL RUN 2-BH5·PAH Benzo(k)fluoranthene-2H12 % 101 N/A 86 N/A N/A 88 Chrysene-2H12 % 85 N/A 70 N/A N/A 87 Dibenzo(a,h)anthracene-2H14 % 137 N/A 130 N/A N/A 126 Fluoranthene-2H10 % 88 N/A 99 N/A N/A 99 Fluorene-2H10 % 66 N/A 70 N/A N/A 72 lndeno(1,2,3-c,d)pyrene-2H12 % 114 N/A 110 N/A N/A 105 Naphthalene-2H8 % 34 (1) N/A 33 (1) N/A N/A 42 (1) Perylene-2H12 % 80 N/A 61 N/A N/A 57 Phenanthrene-2H10 % 92 N/A 97 N/A N/A 112 Terphenyi-2H14 % 151 (1) N/A 159 (1) N/A N/A 168 (1) N/A

### =Not Applicable RDL 

### =Reportable Detection Limit EDL 

### =Estimated Detection Limit QC Batch 

### =Quality Control Batch EDL RDL QC Batch N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 5 of 12**'\11~:**...x2ln1 Ana!Vtlcs JrnE'mational C..orporation o/a Maxxam AnaJyUcs 6740 CampobeJio Road, Mtss1ssauga, Ontarlo,l5N 2l8 Tel: (905) 817-5700**Toti~Free: 800~563~6266**  Fax: (905)**817~5777** v.tww.maxxam.f..a

# Maf§2am

Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1611 !Sampling Date 2013/03/14 00:01 lrQC Number N/A Units RUN 3-BH5-PAH EDL RDL be Batch Naphthalene ng 31100 (1) 330 500 3182508 2-Methylnaphthalene ng 19100 130 500 3182508 2-Chloronaphthalene ng 52.5 0.27 10 3182508**~cenaphthylene** ng 3760 51 500 3182508 Acenaphthene ng 2370 270 500 3182508 Fluorene ng 2280 200 500 3182508 Phenanthrene ng 36900 (1) 120 500 3182508**~nthracene** ng 1360 140 500 3182508 Fluoranthene ng 18200 130 500 3182508 Pyrena ng 9510 120 500 3182508 Benzo(a)anthracene ng 494 5.6 10 3182508 Chrysene ng 1620 68 500 3182508 Benzo(b)fluoranthene ng 266 3.0 10 3182508 Benzo(k)fluoranthene ng 92.7 5.4 10 3182508 Benzo(e)pyrene ng 273 8.1 10 3182508 Benzo(a)pyrene ng <10 10 10 3182508 Perylene ng <7.2 7.2 10 3182508 lndeno(1 ,2,3-cd)pyrene ng 8.0 2.4 10 3182508 Dibenz(a,h)anthracene ng <2.0 2.0 10 3182508 Benzo(g,h,i)perylene ng 10.9 2.5 10 3182508 Coronene ng 6.1 2.2 10 3182508 Surrogate Recovery(%) 2-Methylnaphthalene-2H10 'Yo 42 (2) N/A N/A 3182508 Acenaphthylene-2H8 'Yo 61 N/A N/A 3182508 Anthracene-2H10 'Yo 51 N/A N/A 3182508 Benz(a)anthracene-2H12 'Yo 174 {2) N/A N/A 3182508 Benzo(a)pyrene-2H12 'Yo 54 N/A N/A 3182508 Benzo(b)fluoranthene-2H12 'Yo 128 N/A N/A 3182508 Benzo(g,h,i)perylene-2H12 'Yo 100 N/A N/A 3182508 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ( 1 ) EMCL
- PAH analysis
- Exceeds Maximum Calibration Limit ( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 6 of 12**\·1:-!xx~rn/},lln~vucs** lnwrnalional Gorpora:tJon o:a Maxxam Anaty·ucs 6740 Campobello Road, Mtssissauga, Ontario, L5N 2LB Tel: (905) 817-5700 Toti-Free: 800-563-6266 Fax: (905) 817-5777 \"·tww.maxxam.r.,;a

# Ma'652am
Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1611 Sampling Date 2013/03/14 00:01 

### roc Number N/A Units RUN 3-BH5-PAH EDL RDL QC Batch Benzo(k)fluoranthene-2H12 % 94 N/A N/A 3182508 Chrysene-2H12 % 112 N/A N/A 3182508 Dibenzo(a,h)anthracene-2H14 % 132 N/A N/A 3182508 Fluoranthene-2H10 % 88 N/A N/A 3182508 Fluorene-2H1 0 % 79 N/A N/A 3182508 lndeno(1 ,2,3-c,d)pyrene-2H12 % 112 N/A N/A 3182508 Naphthalene-2H8 % 35 (1) N/A N/A 3182508 Perylene-2H12 % 56 N/A N/A 3182508 Phenanthrene-2H10 % 104 N/A N/A 3182508 Terphenyi-2H14 % 153 (1) N/A N/A 3182508 N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch =Quality Control Batch ( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 7 of 12

Maxxam /;nalvtms lmernational COrporatJon o!a Maxxam**Anal~"tics** 6740 Campobello Road, Mlssissa!J!Ja. Ontario, LSN 2LB Tel: (905j 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma('{)2.arn Keika Ventures Maxxam Job #: 8351259 Client Project#: Tl1550 Report Date: 2013/05/02 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Maxxam ID RC1605 Collected 2013/03/14 Sample ID TRAIN BLANK-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1606 Collected 2013/03/18 Sample ID RUN 1-BH2-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1607 Collected 2013/03/18 Sample ID RUN 2-BH2-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted HRMS/MS 3182508 2013/04/16
Maxxam ID RC1608 Collected 2013/03/18 Sample ID RUN 3-BH2-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted HRMS/MS 3182508 2013/04/16
Maxxam ID RC1609 Collected 2013/03/14 Sample ID RUN 1-BH5-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1610 Collected 2013/03/14 Sample ID RUN 2-BH5-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1611 Collected 2013/03/14 Sample ID RUN 3-BH5-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil

Page 8 of 12**f\r1axx<c~rn /~n?.IVHGS**  lrnernalional Gorporalion o/a Maxxam j!."\naly-lics 6740 Campobello Road, MISSISSauga, Ontario,l51\12l8 Tel: (905)**817~5700** Toll-Free: 800-563-6266 Fax: (905) 8-17-5177 WWWJ'mt.'<X<:llll.t.a

## Ma({)2arn

Maxxam Job #:8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O. #: 10244

GENERAL COMMENTS PAH Analysis: Some ofthe recoveries are outside ofstandard limits 50%- 150-% due to matrix suppression.

Results relate onlyto the items tested.

Page 9 of 12

1\ila.xxam Analylics tmernational COrJJOration ora Max.xarn Analytlcs 6740 Camj)Obeno Road, MlsSISsauga, On!ario, L5N 21.8 Tel: (905) 817-5700 Toll-Free: 80Q-563-6266 Fax: (905) 817-5777 wwwmaxxam.ca

# Ma?§i.am

QA/QC Batch Num lnit QCType 3182508 EM Spiked Blank

RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS

QualityAssurance Report Maxxam Job Number: GB351259 Date Analyzed Parameter ww/mm/dd 2-Methylnaphthalene-2H10 2013/04/30 Acenaphthylene-2H8 2013/04/30 Benz(a)anthracene-2H12 2013/04/30 Benzo(a)pyrene-2H12 2013/04/30 Benzo(b)fluoranthene-2H12 2013/04/30 Benzo(g,h,i)perylene-2H12 2013/04/30 Benzo(k)fluoranthene-2H12 2013/04/30 Chrysene-2H12 2013/04/30 Dibenzo(a,h)anthracene-2H14 2013/04/30 Fluoranthene-2H10 2013/04/30 lndeno(1 ,2,3-c,d)pyrene-2H12 2013/04/30 Naphthalene-2H8 2013/04/30 Perylene-2H12 2013/04/30 Phenanthrene-2H1 0 2013/04/30 Naphthalene 2013/04/30 Naphthalene 2013/04/30 2-Methylnaphthalene 2013/04/30 2-Methylnaphthalene 2013/04/30 2-Chloronaphthalene 2013/04/30 2-Chloronaphthalene 2013/04/30 Acenaphthylene 2013/04/30 Acenaphthylene 2013/04/30 Acenaphthene 2013/04/30 Acenaphthene 2013/04/30 Fluorene 2013/04/30 Fluorene 2013/04/30 Phenanthrene 2013/04/30 Phenanthrene 2013/04/30 Anthracene 2013/04/30 Anthracene 2013/04/30 Fluoranthene 2013/04/30 Fluoranthene 2013/04/30 Pyrene 2013/04/30 Pyrene 2013/04/30 Benzo(a)anthracene 2013/04/30 Benzo(a)anthracene 2013/04/30 Chrysene 2013/04/30 Chrysene 2013/04/30 Benzo(b)fluoranthene 2013/04/30 Benzo(b)fluoranthene 2013/04/30 Benzo(k)fluoranthene 2013/04/30 Benzo(k)fluoranthene 2013/04/30 Benzo(e)pyrene 2013/04/30 Benzo(e)pyrene 2013/04/30 Benzo(a)pyrene 2013/04/30 Benzo(a)pyrene 2013/04/30 Perylene 2013/04/30 Perylene 2013/04/30 lndeno(1 ,2,3-cd)pyrene 2013/04/30 lndeno(1 ,2,3-cd)pyrene 2013/04/30 Dibenz(a,h)anthracene 2013/04/30 Dibenz(a,h)anthracene 2013/04/30 Benzo(g,h,i)perylene 2013/04/30 Benzo(g,h,i)perylene 2013/04/30 Coronene 2013/04/30

Page 10 of 12 Value %Recoverv 84 73 91 81 86 64 93 77 64 86 67 99 77 53 283 (1) 7.3 (1) 111 0.9 85 4.8 110 2.7 110 1.8 169 (1) 17.4 (1) 111

1.8 98 11.5 109 10.6 103 5.0 106

0 132 5.2 107 1.9 98 16.6 115 5.4 79 3.7 110 1.8 131 12.1 124 2.4 134 0.7 126 Units QC Limits % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 60-140 % 50 % 60- 140 % 50 % N/A % 50 % 60- 140 % 50 % 60-140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60- 140 % 50 % N/A

\·13'o..:am/-\na!vllcs Jmernational COrporation o/a Maxxam Anatytics 6740 campobello Road, MISSissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905)**817-~717 www.maxxarn.1~** 

# Ma?§l.am

QAIQC Batch Num lnit QCTvoe 3182508 EM RPD Method Blank Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC. -FELMAN PRODUCTIONS QualityAssurance Report (Continued) Maxxam Job Number: GB351259 Date Analyzed Parameter vvvv/mm/dd Coronene 2013/04/30 2-Methylnaphthalene-2H10 2013/04/30 Acenaphthylene-2H8 2013/04/30 Benz(a)anthracene-2H12 2013/04/30 Benzo(a)pyrene-2H12 2013/04/30 Benzo(b)fluoranthene-2H12 2013/04/30 Benzo(g,h,i)perylene-2H12 2013/04/30 Benzo(k)fluoranthene-2H12 2013/04/30 Chrysene-2H12 2013/04/30 Dibenzo(a,h)anthracene-2H14 2013/04/30 Fluoranthene-2H10 2013/04/30 lndeno(1 ,2,3-c,d)pyrene-2H12 2013/04/30 Naphthalene-2H8 2013/04/30 Perylene-2H12 2013/04/30 Phenanthrene-2H10 2013/04/30 Naphthalene 2013/04/30 2-Methylnaphthalene 2013/04/30 2-Chloronaphthalene 2013/04/30 Acenaphthylene 2013/04/30 Acenaphthene 2013/04/30 Fluorene 2013/04/30 Phenanthrene 2013/04/30 Anthracene 2013/04/30 Fluoranthene 2013/04/30 Pyrene 2013/04/30 Benzo(a)anthracene 2013/04/30 Chrysene 2013/04/30 Benzo(b)fluoranthene 2013/04/30 Benzo(k)fluoranthene 2013/04/30 Benzo(e)pyrene 2013/04/30 Benzo(a)pyrene 2013/04/30 Perylene 2013/04/30 lndeno(1 ,2,3-cd)pyrene 2013/04/30 Dibenz(a,h)anthracene 2013/04/30 Benzo(g,h,i)perylene 2013/04/30 Coronene 2013/04/30 Value %Recoverv 3.9 82 74 83 78 90 59 82 74 57 82 59 112 71 47 (2) 105, EDL=0.81 3.11, EDL=0.56 <0.60, EDL=0.60

<2.1, EDL=2.1 <4.6, EDL=4.6 0.76, EDL=0.40 1.23, EDL=0.34 <0.40, EDL=0.40 <0.53, EDL=0.53 <0.49, EDL=0.49 <0.70, EDL=0.70 <0.76, EDL=0.76 <0.46, EDL=0.46 <0.76, EDL=0.76 <0.53, EDL=0.53 <0.76, EDL=0.76 <0.67, EDL=0.67 <0.38, EDL=0.38 <0.68, EDL=0.68 <0.39, EDL=0.39

<3.2, EDL=3.2 Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement. Units QC Limits % 50 % 50- 150 % 50- 150 % 50- 150 % 50-150 % 50- 150 % 50- 150 % 50- 150 % 50-150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng no Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency. ( 1 ) Recovery Exceeds method acceptance criteria 50%
- 150% due to matrix background ( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 11 of12

Me.u""' Analytic> lrrternauonal C',orporauon o:a Mal<.Xam Analytics 6740 Campobello Road. MISSISSauga. Ontario. LSN 21.8 Tel: (905) 817·5700 Toll·free: 80()-563·6266 Fax: {905) 817·5777 www.maxxam.ca

# Ma?§i.am

Validation Signature Page

Maxxam Job 

### #: 8351259

The analytical dataand all QC contained in this report werereviewed and validatedbythe following individual(s).

Owen Cosby, BSc.C. hem, Supervisor, HRMS Services

Maxxam has procedures in place to guard against improper use ofthe electronic signature andhave the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(£), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page 12 of 12

Manam Analvlics Jrnernatlonal Gorporauon o/a Maxxam AnalytJcs 87411 Campobello Road, Mlss!Ssauga, Ontar10,L5lll 2l6 Tel: (905) 817·5700 Toii·Free: aoo-563·6266 Fax: (905) 817·5777 www.maxxam.ca

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### ff)).:J05 /). /JIJ;i3 

### 1-1 

## t1u·LftJ**/;.~ /~,).**  

## J5'7 ;J

## c..f9 

# -'17 )ii' j-;:). 

## l J-,b

.**-~**

;



# .

. ____ _ ___...

# -·--------------~,. ;,\ ·

# '•'..;Am···~-w ee•;,;k •

# ~:.:.· : •.'

........

# ~**'·.}:....<$~·,;**. . ,..,,.·• ..' ·"£ •

# --~---·'-'---~--~--- ....- __________l.;_

__

_

# Sorbent Trap Chain ofCustody
Plant/Source: -+-f_-e.-:::::____jluvl.....!J0,:....JL::0:...i\-lt-\i"-4-\

_____ _ 

## Bol .ler ID·.

__

## t:t:_~....::::·:---_~1**~1.**__;-

## ~\....:..=.._:_/.:__--- ___ _ v**~.)** h·j V\O•J:> C 

## Trap ID:

# ~ /.

# 5 

# b [J

# )__I Trap 

# =Q B 

## (Circle One) 

# [ZI Unspiked 

# D SpikedAt: Certified Accuracy± I0%, Traceable to NIST 

## QAIQC 

## Signature (Trap

# Maker)~ Spike Date:

___ _ Spike Time:

___ _ QAIQC 

## Signature**(Spiker)·----~----** 

## Estimated Hg in Section 

## 1:

______----'n=g;;lSampled By:

__ C.;;:;;'

### ...;~;...;.r,_,

## ------- 0 High Flow 

## D COIL 

## D Static Prefilter 

## D AGS [81!85 mm 

## Type ofTrap: 

# 30/5 "D-L'-r·e 0240mm 0300mm 0450mm


## T E d ()O\ .I
- 

## L

est n · . n ;

### L.I"J**....&~~** 

## Date/Time 

# e, 1 as Test Start**~- I~-**  13 

## Leak Check •00 1 • 

## ail 

## €**~** 

## Date/Time : 0""1..:-!"J
Date Time

### ~Temp Sorbent**F~Rate** 

### Dry Gas Meter Dry Gas Meter Total Volume roC) tm:emp eel 

### in) Liters Initial Liters Final Pulled r°C) 

## 1(r'i f)**("1-i-~-** lt3**~J::i"-.0** :.tee**c~coo** Co\-. d.\\ ·• G CS**1\~** :) '56 l.\DO

..::\,)\l**I-~.~-)(:** 

## 3/tL-t. ic J")- I ). ").... ;;tSC .!..fQ(; \i•'D·C**~0,<-571** 

## il'i d-SO t-{{.l C' 3.::1' 

### s l 5.-**,o.~** 

### \':?- 

## 3!1'1 iC**~")-**

### 3(t~ ;;l**~** (..) 

## :..tou .:.lJ, .-, l (';**~** (;,·-)c):__ i I 0 'S' 

### l l \

## ~)It

## If**11~"5** I \ 

### '3 

### ;)50 'iOO**~-oS1:i ~O·So'1**  i l "1 ·.) 

### ll"\ :;:l-5"'0 ,0(.) 

### bO.'SD'I 

# ITotal/Average 

# I?o0S07 

# I Chain ofCustody

Date: 

## ··z · i · I 

## 3
Received by:.

__________________________ _ Date:

_______ _ Relinquished by:.

_________________________ _ Date:.

_______ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented atall costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

# EX Sorbent Trap Chain ofCustody
Plant/Source: \:.: 

## -e. \ (""\o.... f'**--~~~~~------------------** .cl- ;-)._ 

### BoilerID:**~** 

### \ :> '(\

### <-~

# n(·**\_~~)** 

# [ZJ Unspiked 

# D SpikedAt: Certified Accuracy± I0%, Traceable to NIST 

### Spike Date:

___ _ Spike Time:

___ _ Estimated Hg in Section 1 :

______ ----=n"""g;>. Sampled By:_L..;;:;

...**;...;·)~C)_.·**--------- 

### Test Start "?> ·· t;..\ 

## -1;

Date/Time : 6 

### v.

### <t5 ('I; 

### Test Location: \_**,J,:..~,** 

### ,_(**\)~(** 

### ;,_ 

# lf**~~~~~~~~~--~-----** 

### Trap

# ID~:_

# _______:O=L~_....~....../**...;;..5...;;b:;__D...;;..6_~_--**_ 

### Trap A (!J(Circle One)



# . _/?" // __/"-? 

### QA/QC Signature (Trap Makerr

## ---~--**-~---z=-· ·~**  

## - \ 

# ·- QA/QC Signature (Spiker),

________ _ 

## 0 High Flow 

## 0 COIL 

## 0 Static Prefilter 

## 0 AGS 181.185 rnrn 

### Type ofTrap: 

# 30/'5**"\-t'i·\?~** 

### TestEnd ,**~C)\** \\**'/1~** 

### Date/Time 0240 rnrn 0300 rnrn 0450 rnrn



### Date Time

### ~Temp 

### Sorbent**~Rate** Dry Gas Meter Dry Gas Meter Total Volume 

### 'VI'f 0

### Eor 0C)

### ~~emp in) Liters Initial Liters Final Pulled 

### r°C) 

# '/1'-f 0'1'1-:\ jl) ""="'J's-0**'J::.>t~** c 

### _oc;o**~\:}-53** 1 

### c**tl'~** I \'{3 ;)'JQ "-100 

### '1' 

### J. )] I

## i .!-11 "')- <""- 

## 3/1( I J. 

### 52- ;l")C**~vo t~;·~i15**  19-0.1; 

### 3"\0 iCJ.') 

# 3Jt'1 l l

### q_ [)'50 '-too**:A.~** 

### }_{j6i 

### 34.
- \ \ <) tu'-15**~** 

### '?1/14 II C ")" 

## t l 

### l 

### ]-<5'0 1.-.1()0

# ~"'' \ lS**"i~,-=11~** 

# 3/fL/ ;I J, .;-**~I** 

### 3 !)5o '-1.00 "i'i$'_r\o5 1)';3''**y;~** q 

### '1'5 j ( '1 ;)"50 '-£00**~~-** 

### y-;o., 

# ITotaVAverage 

### Chain ofCustody

Date: ; 

### t
-- t - 

### 1 )

---------------- Received by:

___________________________________________________ _ Date:

______________ _ Relinquished by:

________________________________________________ _ Date:.

______________ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

# Sorbent Trap Chain ofCustody
T . ., l (....__



### est Locatwn:**C~c.** v1. \I(_**--~~~~~---------------** 

### Trap ID: OL 

# /5

# b D (; L( 

# D Spiked At: Certified Accuracy± 10%, Traceable to NlST 

### Trap 

# @ B (Circle One) QAJQC 

## Signature

# <TrnpMok~~- Spike Date:

___ _ Spike Time:

___ _ QA/QC Signature (Spiker)



### ------------------- 

### Estimated Hg in Section 1 :

______ ____:n=g"'- 

## 0 High Flow 

## 0 COIL 

## 0 Static Prefilter 

## 0 AGS [8ll85 mm 0240mm 0300mm 0450mm 

### Sampled

## By:_C._)_~_·_rY'_\

_______ _ 

### Type ofTrap:

____ 

# 3_0_;./5

_____ _ Test Start**~-** 

### '· "t- l 

### 3



### Date/Time : 1-;7 • :; 0
Date Time

### ~Temp 

### QfoC) 

## 3f\i)-- .!.;)...:>..;;;..- _i,,;;l ';, I ;).-)Q**\(l~** 

# 3) u

### 1 

# n (c l I .;.:-:- 

### " 

# 3j IL-f j:))(J 

## 1**i~** 

## 3j**~~** i**~** 

### ;i(_) t ( !.-(

# ~I '/.,1 1'1 l 

### c 

### '**·;~** i I 30 

### i !(;, j Total/ Average 

### Sorbent**~Temp ~roC)** **~""-""'-~** "!..../ 9-'S G ;.'j-")**c~** 

### d**~ :;~)**  c) 

### "J-C**01~0** Q<Y)**--~** 

### Test End 3.
- 

## l**~-** 

### l 

# 3 Date/Time 1

## '1 

# 3:::? Leak Check -·**~"** 

### Pass/Fail 

# e 3
Flow Rate Dry Gas Meter Dry Gas Meter Total Volume

### ~in) Liters Initial Liters Final Pulled

1-fCC}**~;;.** 

### --oot..J**~ ''-i-~"2.**  -**~((** 0**~** . .!-lc\0 

### 1 l i '7 "-1)- /-lf:J(J l 

### 7' 1 '-! "}**J~.o.~;_-~-o** '-! 

## c r_! ;,} ("" '7;)0**~ ~**  <**'1L(~-**
J-l L '-..- 

### 3') l ,·7 l-j ':} '1-( . 'I'-{ 

### C : "'-tt.:X> !..ILl ·"'11'--10 '5'5 "';')) "t·a0 '5

### 3':1 3 ·:.·


### Chain ofCustody I'! Relinquished by Tech.:

__ _,_··

# L..-~ __

'·_"

# _--:."--.~-~_,. _-.--'.""'.\'-, --'-----'-)-'::_,_?-=;._='·

# --..=:.·-''~· (=··:_:(_/

________________ _ Date:

_______ 

### l_-

__

·; _-::_.
__ _ Received by:

___________________________________________________ _ Date:

______________ _ Relinquished by:

________________________________________________ _ Date:

______________ _ Received for Laboratory by: Date: 

# .I

Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

## ~EX 

# Sorbent Trap Chain ofCustody
Test Location: 

# C_-e /tt

### ~ :-**-=~~~L----------------** 

### Trap ID: OL / 

# 5 b 0/

# cf Trap A 

# m (Circle One) 

# IZJ Unspiked 

# D SpikedAt: Certified Accuracy± I0%, Traceable to NlST

# ~//~ QA/QC Signature (Trap

### Maker)~ 

### c:;7/--- 

### Spike Date:

___ _ Spike Time:

___ _ QA/QC Signature (Spiker).

_________ _ 

### Estimated Hg in Section 1 :

______**____:n~g;:>....** 

## 0 High Flow 

## 0 COIL 

## 0 Static Prefilter 

## 0 AGS 181.185 rnrn 0240 rnrn 0300 rnrn 0450 rnrn 

### SampledBy:.....::...C

.......

## t>~f_VJ....}-------- 

### Type ofTrap:.

___**~3....;0;;......:...;;;6** 

### ____ _ 

### Test Start j
- 1 4 · 1

### 3 

### Date/Time : i

## o-·, 1 0 

### Leak Check1 c.JlO 1 

### ail 

# CS ?>
Date Time

### ~Temp Sorbent roC)

### ~~emp r°C) 

## '?J/li \Ql-:,0**~;).\. ~**  ;t-:>C**\.~so** 

### t-e3t**-~** c.;c 

# J/ti t"3.10 I\ J- do<:) 0 

### 7> /( 

### '1 i

### 3"3 0 

### \ \ 9..**:;~...;u** 

### 3

# /11-f I j S"G l \

## '1. :7 '-iD 

### 3 ;,/;( 1"1! 0 I**;l~ ~L:.;Q**  i"i 

### 30 \ l**~** 95-0

J 

### Total/Average 

### Test End J
- t"-(.- 1J 

### Date/Time Ihf. ; 

### JO 

### Leak Check ,cct 

### Pass/Fail 

# e q Flow Rate Dry Gas Meter Dry Gas Meter Total Volume @in) Liters Initial Liters Final Pulled

tr_-CO 

### o.ooo <3 I <::,"IS 1..-{e:, ·; 

## -s (::i"'i 

### 1**l-'~=-,o** i.fCG 1l.b"10 

### :) (:,, ;J (, :;-**L~oo** )c,,ji,') 

### );), 3.90 L(00 5 

### s·.)::.-:.::**~'-i** r·£-1<

. .: .... : it.._...' ..t .C.tC(_,") '"IJ.i '04':::. S-?.fc. I "7 :..lOt> 'S"d**.~1-1**


### Chain ofCustody

Date: 

## l-t

- l
- l 

## 3
Received by:.

__________________________ _ Date:

_______ _ Date:

-------- Relinquished by:

________________________ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented atall costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool '

# EX Sorbent Trap Chain ofCustody
Plant/Source: 

# Fe.{ 1Y'<2\ {\ 

## Test Location: 

## C.e r\

# t e'f'....._**----------~~-------------** 

## BoilerID:

## ·~**tf~ ~**  \\Vt?'S

### t'.

## ~<:) Dunspiked 

## TrapiD: 

# fb f5077? Trap 

# = BCircleOne) 

## QA/QC Signature

# <TrnpM"'~J~ Spike Date: 2/ti//3SpikeTime:

# /'l/0**~~~/** QAIQC Signature

## <S~/ 0 High Flow 0 COIL 0 240 mm 

## Estimated Hg in Section I :

______**--=n~g;;>..** 0 Static Prefilter 0 AGS 0 300 mm 

### gj 185 mm 0450 mm 

## Sampled By:

__ G_·'2>_-_'("V)

_______ _ 

## Type ofTrap:.

___**...;;;3CJ-=-6~~::::;.....**

### _____ _ 

## Test Start ;)

-**l~..l.** '" 

## 13

Date/Time : 1

### 5•-0() 

### Date Time

### ~Temp or 0

### C) 

## 3

## li·~-- 1f0.0 t-A i 'l)_") J} 

### it'l 

## 3/;t-j i5'io • ,;l(o j 

# /ttt (ioUO t,;;) 

### 0

## 3jl~ tbd.:.:) 

## {'3 t 

## d**;,~** \(.LtO i 

### '3 '1 ''700 

# ITotal/Average Sorbent**~Temp** 

### E or 0C)**,;t~** \.**.~':\0** 

# a-s-o :;-su ..2 -:)(,') &<5-o 

## Test End 

## ·Z>- I.

### '1' ·- (

## 3 Date/Time I

## ·1 :. o 

## o**F~ate** Dry Gas Meter Dry Gas Meter in) Liters Initial Liters Final
t..t.C'C' o.-0DU <;:; 

### "·l J., 

### "3 YCO**~.** l.Y::\ \''1'**~~)** 

## 'toe 11.'?'t5 

# :/7.

# "l'iO
4,00 

### '3-t,£'10 :_)"

..... )'1 -1!) \.

. 

### ..-.0 

### iiOO 

## 3-{ .·)20 

## ·-i t..j. 

## 3'1 ') '-i,tDO '-j '-{ I 

### '3 o, I) 

### "5'1· (?\<? 4.0(.) 

## 5 '"i, 

### <::,\**""'~**


## Chain ofCustody Total Volume Pulled

Date: /..i ·- 

### i**~** 

## t3
Received by:

__________________________________________________ _ Date:

________ _ Relinquished by:

________________________________________________ _ 

### Date:

________ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented atall costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

### APPENDIXE CALIBRATION DATA

## Dry 

## Gas Meter Box Calibration MeterNo. 

### 2010 Barometer PreTest Y 

### 29.4 Date 

### 1.0203 Calibrator 

### 04/02113 csm Po Vac Vw Tw Vd Td y 

### "H20 "Hg ft3 

### °F ft3 

### °F


### •·•••·•••• \ \ ••... 0.000 60 720.339 60.5 •••••••••••••••••••••••••••••••••••• 

### 0.5 10.000 61 730.16 62.5 1.0189 

## ntN 

# <&g• 1o.ooo 60.5 9.821 61.5 

## > ••• 

# H• 1o.ooo 61 730.16 62.5 1.00 20.000 61 739.955 63 1.0218



# :;**~ygl.** 

### 10.000 61 9.795 62.75
•••••·• 20.000 61 739.955 63 1.50 30.000 61 749.72 63 1.0242



## <:/AvK 10.000 61 9.765 63 

## < ••

•••••••• •• • 30.000 61 749.72 63 

# illill2 2.00 40.000 61 759.505 64 10218

# ~:;::··¥···•·#.:¥~!s# ..

# ,·~·~~~·*====*=~~~~:~**o~ o='=~~~~** **=*==7~****59·~~.~~~=5 ='==~** **:;;..;.;4· ~==1+.4-**  2.50 50.000 61 769.38 63.5 1.0117

# ·~~8,(1\yg~ 10.000 61 9.875 63.75

# ~ / / • 50.000 61 769.38 63.5**~=3."""oo==+-----+--6-o.-oo_o_+-_6_1_--+-7-79_.2_1_5**

### -+--6-4-- 1.0145

Average 

### Y = 

### 1.0188

### Barometer 29.4 PreTest Y 1.0468 Po Vac "H20 "Hg

# ~::::::::

0.5
:) 

### 1.00

,•: 

## )
1.50

2.00

2.50

3.00 

## Dry Gas MeterBox Calibration MeterNo. 2010

Vw 

### fP 0.000 10.000 10.000 10.000 20.000 10.000 20.000 30.000 10.000 30.000 40.000 10.000 40.000 50.000 10.000 50.000 60.000 10.000 Tw 

### op 57 58 57.5

58 58 58 58 58 58 58 58 58 58 58 58 58 58 58 Date Calibrator Vd fP 174.528 184.295

9.767 184.295 194.105

9.81 194.105 203.89 9.785 203.89 213.625

9.735 213.625 223.565

9.94 223.565 233.433

9.868 02/20/13 csm Td Y 

### op 61.5 1.0305 61.5 61.5 61.5 1.0237 61.5 61.5

61 1.0245 61.25

61 60.5 1.0275 60.75 60.5

61 1.0051 60.75

61 61 1.0117 61 Average Y = 

### 1.0205

### Barometer 

### 29.3 PreTest Y 

### 1.0342 Po Vac 

## Dry Gas Meter Box Calibration Meter No. 

### 2010 MST Date Calibrator Vw Tw Vd Td "H20**·~** 

### ft3 

### op ft3 

### op

•••••••••••••••• 

### 1 0.000 74 840.515 74 0.5 1 10.000 75 850.28 80 10.000 74.5 9.765 77 2 0.000 75 850.28 80 1.00 2 11.000 75 861.06 83 

# :liN • 

# lf:gl 11.ooo 75 1o.18 81.5

·•·•·• ··••••• 3 0.000 75 861.06 83 1.50 3 10.000 75 870.9 84 n 

# &g; 10.ooo 75 9.84 83.5 10/05112 csm

y



### 1.0276

1.0302

1.0285

•••••• 4 0.000 75 870.9 84 ·•·•••• 2.00 4 20.000 74 890.575 86 1.0313

3.00 6 10.000 74 910.258 86 1.0336
Average Y 

### = 

### 1.0302

## Dry Gas MeterBox Calibration MeterNo. 2010 MST Barometer 29.35 Date PreTest Y 1.0302 Calibrator csm Po Vac Vw Tw Vd Td y 

### ft3 

### op ft3 

### op 1 0.000 66 322.792 71 1 10.000 63 334.735 71 64.5 11.943 71

63 334.735 71 63 344.685 71

10.000 63 4 0.000 63 2.00 4 10.000 62 62.5 5 0.000 62 2.50 5 10.000 62
6 0.000 62 374.45 6 10.000 62 384.338 10.000 9.888 Average Y= 1.0205CHEROKEE INSTRUMENTS INC 30B Hg Dual Console Meter Box Post Calibration

Cherokee#: 3620 Meter# MI-Dual Hg Date: 03/05/13 Serial#: DB 308-1110-2017 Barometric Pressure: 29.73 in.Hg HgSide 1 DRY GAS METER VOLUME Flow Time Initial Final Total Temperature ("F) Initial Final f!nm} (minutes) (Liters) (Liters) (Liters) Initial Final (Liters) (Liters) 0.25 40.0 0.00 10.19 10.19 84 85 17883.00 17893.00 0.50 42.0 0.00 21.72 21.72 82 83 17859.40 17881.50 0.75 31.0 0.00 23.24 23.24 80 81 17831.20 17854.70
HgSide2 DRY GAS METER VOLUME

; Flow Time Initial Final Total Temperature ("F) Initial Final f!nm} (minutes) (Liters) (Liters) (Liters) Initial Final (Liters) (Liters) 0.25 40.0 0.00 12.22 11.52 78 82 17731.80 17742.60 0.50 35.0 0.00 18.07 18.07 80 82 17745.70 17762.80 0.75 35.0 0.00 27.17 27.17 82 84 17770.20 17796.30

Calibration Gamma (Y)* 

### =I 1.0092 

### I Meter I 1.002 1.035 1.023 Deviation -0.018 0.015 0.003 Operator: J McK Vacuum: 0 in.Hg CALIBRATION DEVICE VOLUME Total Temperature (°F) (Liters) Initial Final 10.00 78 78 22.10 77 78 23.50 78 78

CALIBRATION DEVICE VOLUME
Total Temperature ("F) (Liters) Initial Final 10.80 76 78 17.10 76 77 26.10 77 77

Meter2 Deviation 0.951 -0.013 0.962 -0.002 0.979 0.015

# Av.,.,.,Gamma~ l.fl20 

# I Ave<geGommF 0.964 

# I

308 Console-3620 (Dual)

---·- ·-**---~-=;==-<.~-===-"=-=-~---** .--·-----------

### APPENDIXF CHAIN OF CUSTODY

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### d d Vi 

### z 0 (INCLUDE MATRIX) 

### z c..**~** w w**~** co 

### z**~ ~**  <( w ::> 0 0::: 1- 0::: 0 i= u l!) 

### 1 1 3/15/2013 Baghouse #5 Run 1Back-halfRinse H2S04 2 2 3115/2013 Baghouse #5 Run 2 Back-halfRinse H2S04 3 3 3115/2013 Baghouse #5 Run 3 Back-halfRinse H2S04 4 1 3/19/2013 Baghouse #2 Run 1Back-halfRinse H2S04 5 2 3/19/2013 Baghouse #2 Run 2 Back-halfRinse H2S04 6 

### 3 3/19/2013 Baghouse #2 Run 3 Back-halfRinse H2S04 7 3/27/2013 BlankDe-ionized Water 8 3/27/2013 Blank O.lN H2S04 9 10 (,/) 0::: w LL Z 

### '0 0 

### <C :c # 1- <( 

### z 1.0 0 N u**~** 

### 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS !

HCI1 of 1



### BH#5 BH#5 BH#5 BH#2 BH#2 BH#2

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- 

### SAMPLE DESCRIPTION 

### 0 Vi 

### 0 0 

### (INCLUDE MATRIX) 

### z z a.. 

### ::E w w 

### ::E CJ 

### z**~** ::E <! w :::> 0 0::: 1- 0::: Cl i= u**~** 

### 1 1 3/13/2013 Baghouse #5 Run 1Filter 1012 2 1 3/13/2013 Baghouse #5 Run 1Front-halfRinse HN03 3 1 3/13/2013 Baghouse #5 Run 1 Back-halfRinse HN03 4 

### 2 3/13/2013 Baghouse #5 Run 2 Filter 1011 5 2 3/13/2013 Baghouse #5 Run 2 Front-halfRinse HN03 

### 6 2 3/13/2013 Baghouse #5 Run 2 Back-halfRinse HN03 

### 7 3 3/13/2013 Baghouse #5 Run 3 Filter 1010 8 3 3/13/2013 Baghouse #5 Run 3 Front-halfRinse HN03 9 

### 3 3/13/2013 Baghouse #5 Run 3 Back-halfRinse HN03 10 ..!:!! ro oi-l Cll**~** II) Cll 0::: 

# c. w 

### :E u. 

### z**~** 0 <(**~** =1:1: 1- 

### z 0') 0 N u**~** 

### 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 

### RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Metals 1 of 3 arsenic, cadmium, chromium, manganese, nickle, lead

BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#5


### DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

LU 1- SAMPLE DESCRIPTION 

### d Vi 

### d 0 (INCLUDE MATRIX) 

### z z c.. co**~** LU LU**~** 

### z**~ ~**  <( LU ::::> 0 0::: 1- 0::: Q i= u (.!) 

### 1 1 3/13/2013 Baghouse #2 Run 1Filter 1007 2 1 3/13/2013 Baghouse #2 Run 1Front-halfRinse HN03 3 1 3/13/2013 Baghouse #2 Run 1Back-halfRinse HN03 4 

### 2 3/13/2013 Baghouse #2 Run 2 Filter 1006 5 2 3113/2013 Baghouse #2 Run 2 Front-halfRinse HN03 6 2 3/13/2013 Baghouse #2 Run 2 Back-halfRinse HN03 7 3 3/13/2013 Baghouse #2 Run 3 Filter 1005 8 

### 3 3/13/2013 Baghouse #2 Run 3 Front-halfRinse HN03 9 

### 3 3113/2013 Baghouse #2 Run 3 Back-halfRinse HN03 10**~** ro

...... Q) :;E V) Q) 0::: 

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### z 0'1 0 N u :;E 

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### 1 X
RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Metals 2 of 3 arsenic, cadmium, chromium, manganese, nickle, lead



### BH#2 BH#2 BH#2 BH#2 BH#2 BH#2 BH#2 BH#2 BH#2
DATE: TIME:

# ~~· 

# • TEST, Inc. Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 

# Chain of Custody

EMAIL ADDRESS: PCHIN@TESTINCORP.COM

u.J 1- SAMPLE DESCRIPTION 

### d Vi 

### d 0 

### z z c.. (INCLUDE MATRIX) 

### :E u.J u.J 

### :E co 

### z**~** :E <( u.J :::> 0 cr:: 1- cr:: 

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### 1 1 3/27/2013 Blank Filter 2 1 3/27/2013 Blank 5%HN03/10% H202 3 1 3/27/2013 Blank O.lN HN03 4 

### 5 6 

### 7 

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RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Metals 3 of 3 arsenic, cadmium, chromium, manganese, nickle, lead I

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304} 755-1077 EMAIL ADDRESS: PCHIN @TESTINCORP.COM

w 1- 

### SAMPLE DESCRIPTION 

### 0 0 v; 2 0 

### (INCLUDE MATRIX) 2 c..**~** w w**~** cc 2

### ~**~** <( w :::> 0 0::: 1- 0::: 

### c i= u (.!) 

### 1 1 3/15/2013 M23/PCB XAD Trap #7, Baghouse#5 Run 1 2 1 3/15/2013 M23/PCB Filter, Baghouse #5 Run 1 3 2 3/15/2013 M23/PCB Trap #1, Baghouse#5 Run 2 4 2 3/15/2013 M23/PCB Filter, Baghouse#5 Run 2 5 3 3/15/2013 M23/PCB Trap #6, Baghouse#5 Run 3 6 3 3/15/2013 M23/PCB Filter, Baghouse#5 Run 3 7 1 3/19/2013 M23/PCB Trap #8, Baghouse#2 Run 1 8 1 3/19/2013 M23/PCB Filter, Baghouse #2 Run 1 9 2 3/19/2013 M23/PCB Trap #9, Baghouse#2 Run 2 10 2 3/19/2013 M23/PCB Filter, Baghouse #2 Run 2 u c..



### ...... V) c: rtl



### .... :::J u..


## ...... V) c: 

## ·x 0 

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### 1 X 

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### 1 X 

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### RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 1 of 2

I



### BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### d d Vi 

### z 0 (INCLUDE MATRIX) 

### z c.. al**~** w w**~** 

### z**~ ~**  <( w 

### => 0 0:: 1- 0:: Q i= 

### u l!) 

### 1 3 3/19/2013 M23/PCB Trap #3, Baghouse#2 Run 3 2 3 3/19/2013 M23/PCB Filter, Baghouse#2 Run 3 3 3115/2013 M23/PCB Trap #2, Train Blank 4 3115/2013 M23/PCB Filter, Blank 5 M23/PCB Trap #4, Not Used 6 

### M23/PCB Trap #5, Not used 7 

### 8 9 10 u c..

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## ·:x: 0 

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### u**~** 

### 1 X 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 2 of 2



### BH#2 BH#2 Blank Blank

' 

### No analysis No analysis

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN @TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### d d Vi 

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### 1 1 3115/2013 Baghouse #5 D/F/PCB Run 1Front-halfRinse 2 1 3115/2013 Baghouse #5 D/F/PCB Run 1Back-halfRinse 3 2 3115/2013 Baghouse #5 D/F/PCB Run 2 Front-halfRinse 4 

### 2 3/15/2013 Baghouse #5 D/F/PCB Run 2 Back-halfRinse 5 3 3/15/2013 Baghouse #5 D/F/PCB Run 3 Front-halfRinse 6 

### 3 3/15/2013 Baghouse #5 D/F/PCB Run 3 Back-halfRinse 

### 7 1 3/19/2013 Baghouse #2 D/F/PCB Run 1Front-halfRinse 8 

### 1 3119/2013 Baghouse #2 D/F /PCB Run 1Back-halfRinse 9 2 3/19/2013 Baghouse #2 D/F/PCB Run 2 Front-halfRinse 10 2 3/19/2013 Baghouse #2 D/F/PCB Run 2 Back-halfRinse u c..

......... Ill c: ro '- ::J u..

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# ·x 0 

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### 1 X 

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### 1 X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 1 of 2



### BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w I- SAMPLE DESCRIPTION 

### 0 0 v; 

### z 0 (INCLUDE MATRIX) 

### z w 0.. J:C 2: w 2: 

### z**~** 2: <( w ::> 0 c:: I- c:: Cl i= u (.!) 1 3 3/19/2013 Baghouse#2 D/F/PCB Run 3 Front-halfRinse 2 3 3/19/2013 Baghouse #2 D/F /PCB Run 3 Back-halfRinse 3 3115/2013 Train Blank D/F/PCB Front and backhalfRinse 4 5 6 

### 7 8 9 10 :J: tn <( c:: c.. w 

# ""' 1.1- 

### z en 0 

# < N =1:1: I-**~** 

### z c:c 0:::: 0 u <( u 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 2 of 2

BH#2 BH#2 

## I Blank

I I

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- 

### SAMPLE DESCRIPTION 

### d d Vi 0 

### (INCLUDE MATRIX) 

### z z c..**~** w w**~** tC 

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### 1 1 3/14/2013 PAH XAD Trap #5, Baghouse#5 Run 1 2 1 3/14/2013 PAH Filter, Baghouse #5 Run 1 3 2 3/14/2013 PAH XAD Trap #8, Baghouse#5 Run 2 4 2 3/14/2013 PAH Filter, Baghouse #5 Run 2 5 3 3/14/2013 PAHXAD Trap #1, Baghouse#5 Run 3 6 3 3/14/2013 PAH Filter, Baghouse #5 Run 3 7 1 3/18/2013 PAH XAD Trap #7, Baghouse#2 Run 1 8 1 3/18/2013 PAH Filter, Baghouse #2 Run 1 9 

### 2 3/18/2013 PAH XAD Trap #6, Baghouse#2 Run 2 10 2 3/18/2013 PAH Filter, Baghouse #2 Run 2 

### :c V'l <( 0:: c.. w 

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### z 0'1 0 <( N**~** # 1- co 

### z 0 0:: u <( u 

### 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY:

·---· - -·- 

### REQUESTED ANALYSIS COMMENTS

PAH 1 of 2

BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

-- ------

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304} 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### c:i c:i Vi 

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### z**~ ~**  <( w :::> 0 c::: 1- c::: 0 i= u**~** 1 3 3118/2013 PAH XAD Trap#9, Baghouse#2 Run 3 2 3 3/18/2013 PAHFilter, Baghouse #2 Run 3 3 3/14/2013 PAH XAD Trap #2, Train Blank 4 3/14/2013 PAHFilter, Train Blank 5 PAH XAD Trap #3, Not Used 6 PAH XAD Trap#4, Notused 

### 7 8 9 10 

### :c V) <( c::: c.. w 

# """ Ll- 

### z 0'1 0 <( N =1:1: 1- 

## """ z cc 0::: 0 u <( u 1 X 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY:

----- ------------------ ----· - -- - --- REQUESTED ANALYSIS COMMENTS

PAH 2 of 2

BH#2 BH#2 Blank Blank No analysis No analysis

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

LU 1- SAMPLE DESCRIPTION 

### d d Vi 

### z 0 (INCLUDE MATRIX) 

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### z**~ ~**  <( LU 

### => 0 a: 1- a: Cl i= 

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### 1 1 3114/2013 Baghouse #5 PAH Run 1Front-halfRinse 2 1 3114/2013 Baghouse #5 PAH Run 1 Back-halfRinse 3 2 3114/2013 Baghouse #5 PAHRun 2 Front-halfRinse 4 2 3/14/2013 Baghouse #5 PAH Run 2 Back-halfRinse 5 3 3114/2013 Baghouse #5 PAH Run 3 Front-halfRinse 6 

### 3 3114/2013 Baghouse #5 PAH Run 3 Back-halfRinse 

### 7 1 3118/2013 Baghouse #2 PAH Run 1Front-halfRinse 8 1 3118/2013 Baghouse #2 PAH Run 1Back-halfRinse 9 

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### 1 X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY:

---- ------·-· ---- ---- --- REQUESTED ANALYSIS COMMENTS

PAH 1 of 2



### BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-'1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

LU 1- 

### SAMPLE DESCRIPTION 

### ci ci Vi 0 

### (INCLUDE MATRIX) 2 2 c..**~** LU LU**~** co 2

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### 7 8 9 10 

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### ....... u.. 2 0'1 0 

# < N**~** =1:1: 1- 

### c:c 2 0 0::: u <( u 1 X 1 X 1 X



### RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS
!



### PAH 2 of 2

BH#2 BH#2 Blank



### DATE: TIME:

### APPENDIXG PLANT OPERATIONAL DATA

### 3/13/2013

0 #5 Fce Time Opened Time Plugged Tap Number Tap Weight Fines Usage Liquid Metal 7:35 8:00 971 9:30 10:30 972 11:30 11:55 973

1:40 2:05 974 3:45 4:30 975 6:15 6:50 976 8:30 9:00 977 10:30 10:55 978 12:30 1:00 979

2:35 3:00 980 4:40 5:05 981 6:30 6:55 982
Total LBS Total NT 

## Note: Production and Raw Material data submitted separately as Confidential Business Information With Fines 

### Raw materials consumption



# Redacted

### 3/14/2013

0 #5 Fce Time Opened Time Plugged Tap Number Tap Weight Fines Usage Liquid Metal 8:35 9:00 983 10:40 11:05 984 12:40 1:05 985

2:30 3:00 986 4:30 5:00 987 6:20 6:50 988 8:30 9:00 989 10:30 11:00 990 12:30 1:00 991

2:30 3:00 992 4:30 5:00 993 6:30 7:00 994
Total LBS Total NT 

## Note: Production and Raw Material data submitted separately as Confidential Business Information Raw materials consumption
With Fines



# Redacted

### 3/15/2013

0 #5 Fce Time Opened Time Plugged Tap Number Tap Weight Fines Usage Liquid Metal 8:35 9:00 995 10:35 11:00 996 12:35 12:55 997

2:35 2:55 998 4:25 4:55 999 6:30 6:55 1 8:30 9:00 2 10:30 11:00 3 12:55 1:30 4

3:15 3:40 5 5:30 6:00 6

Total LBS Total NT 

## Note: Production and Raw Material data submitted separately as Confidential Business Information Raw materials consumption

With Fines



# Redacted

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EQUWMENTPROBLEMS

____________________________________________**~----**

MECHANICAL WORK PERFORMED

________________________________________ _



### COMMENTS:.. !

. .-

# .."•.:

femperilllig Aiw If,"1fq:r Inlet Temperature Staclk Temperatur:e

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EQUWMENTPROBLEMS

______________________________________________ ___

MECHANICAL WORK PERFORMED

_____________________ -.,--



### COMMENTS:

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i'**t'mperi~g i~.ir** **Tem~; ~:nilet!** **'1f,~mpemhi!rre;** -:·}F' 'JF**~,** ii f: (--,.

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## No~ Hopper l?wessrunre ±__]_lrnlH[zO _iy_InH 20 No WHopper

## l?~ress!l!!Pe_,_HilllH20 No 5 Hopper l?we§SI!lire 

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### No 9**Hoppe~:** No 

### 10 Hopper No ll Hopper


### EQUIPMENT PROBLEMS

________________________ _

MECHANICAL WORKPERFORMED

____________________ _



### COMMENTS:**~ ~i1.m!i:'.** **Oat~;: r~mi:.**  : ·---' Tempeiring Air Temp: Inlet Temperahu·e; 

### StackTemperatrunre; "JF



### MAGNEHEUC GAUGES On Line No UHopper Pressl!.ilre+ 

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## LL_InH20 No 

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### 5 Hopper No 6 Hopper No 7 Hopper No 

### 8 Hopper No 9 Hopper No 

### 10 Hopper No 

### 11 Hopper 

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Screw Conveyor**'~ab** 

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Baghouse Blower Tra!lls1fe;r Biowelf; Ah·**Press~Are:**

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--i--inH 20
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Bags Missing I

EQUWMENTPROBLEMS

________________________________________________ __

MECHANICAL 

### WORK PERFORMED

________________________________________ _



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Screw Conveyor .**;~**



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!Baghm11se Blowe• Transfe1r Blower; Air Pressure:

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Bags Missing

EQUWMENTPROBLEMS.

________________________________________________ __



### MECHANICAL WORK PERFORMED



### COMMENTS:

### 3

__ _

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### »Hopper

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### Hopper On/Off Screw Conveyor Rotary Lock Bags Missing



### EQUWMENTPROBLEMS

________________________________________________ __

.,< .·**MECHANICAL~ORKPERFO~ED**

### __________________________________________ __

COMMENTS:



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EQUWMENTPROBLEMS

________________________________________________ __

MECHANICAL WORK PERFORMED



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_ 

# _t_LInH20 

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On/Off No l Hopper 

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# - No 9 Hopper No 10 Hopper No 11 Hopper 

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EQUWMENTPROBLEMS

_________________________ _

MECHANICAL WORK PERFORMED



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MAGNEHELl!C GAUGES Oi!ll U!rnie Cle21!llillllg Ollll**U~rue Cle~mnng**  No 1 Hoppn JPnss!lliir<e!

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EQUWMENTPROBLEMS

__________________________________________________ _

MECHANICAL WORK PERFORMED



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BaghoMse Blower T1rans1fer BRower: Ai1r Pressanrre: ___ \.: :)

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## +- (.;. InH20 

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## - .S InH20 No JO Hopper Pressure__::_InfizO -=-InHzO No 

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### ,.

EQUIPMENT PROBLEMS.

________________________ _

J1ECHANICAL WORK PERFORMED

_________**~-----------**



### COMMENTS:



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# a No SHopper No 9 Hopper No 10 Hopper No 11 Hopper


### EQUWMENTPROBLEMS

_______________________________________________ __

MECHANICAL WORK PERFORMED



### COMMENTS:T:empedi!!lg Anw Temp; R!!lllet Temnqp>enilli:IUire: "IF BaJgilllmnse l!Uowerr**T~r~uilsfer** Blowerr Air J?wess\Uln·e: , iPSK

--·--- --·--- "IF Si:adk lfemperatillre:
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Clea!!lling

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# ON / 

## ,/ 0 No 8 Hoppel!" No 9 Hopper No 10 Hoppew No 11 Hopper


### EQUIPMENT PROBLEMS

________________________ _

MECHANICAL WORK PERFORMED



### COMMENTS:**p,j~·** Temp·**I!li'H<e~ Tempew~ti!l!!fe:** **Stra~e:::k Temperr:BJ~iLme;**  PSK 

## LO Q )p§ff
MAGNEHJEUC GAUGE§ Oll1i U:rue CHe2l!l1ia!l1ig Orrn Ullll<e CHeaurnhng No ll

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### -+S. 

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________________________ _

MECHANICAL WORK PERFORMED.



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________________________ _

MECHANICAL WORK PERFORMED

___________________ _



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________________________ _

MECHANICAL WORK PERFORMED



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