### 13339 Hagers Ferry Road Huntersville, NC 28078-7929 McGuire Nuclear Complex - MG03A2 Phone: 980-875-5245 Fax: 980-875-4349 

# Order Summary Report 

# Analytical Laboratory

Order Number: J13060391 Project Name:

Lab Contact: Jason C Perkins 

## Date: 7/2/2013 Customer Address: 573 Duke Power Rd Customer Name(s): josh Quinn, Zack Hall

Mail Code: Clliffside Steam Station Mooresboro, NC 28024
Phone: 980-875-5348 Report Authorized By: (Signature) 

### Program Comments: Please contact the Program Manager (Jason C Perkins) with any questions regarding this report. Data Flags & Calculations: Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have been qualified by Duke Energy to perform these analyses except where noted. Data Package: This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows: Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC) Certification: The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina (DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods. Jason C Perkins

# Sample ID's & Descriptions:

Sample ID Plant/Station Collection Date and Time Collected By Sample Description 2013014682 CLIFFSIDE 21-Jun-13 9:15 AM GLENN LONG BOTTOM ASH SLUICE 0.3m 2013014683 CLIFFSIDE 21-Jun-13 8:14 AM GLENN LONG FLYASH SLUICE 0.3m 2013014684 CLIFFSIDE 21-Jun-13 10:55 AM GLENN LONG SOURCE WATER (INTAKE 0.3m 2013014685 CLIFFSIDE 21-Jun-13 10:50 AM GLENN LONG ASH BASIN 0.3m 4 Total Samples

### COC and .pdf report are in agreement with sample totals

and analyses (compliance programs and procedures). All Results are less than the laboratory reporting limits. All laboratory QA/QC requirements are acceptable. Yes No



# Technical Validation Review Checklist:

Yes No Yes No


# Report Sections Included:

Job Summary Report Sub-contracted Laboratory Results Sample Identification Customer Specific Data Sheets, Reports, & Documentation Technical Validation of Data Package Customer Database Entries Analytical Laboratory Certificate of Analysis Analytical Laboratory QC Report Chain of Custody

Reviewed By: 

### DBA Account Date:

### 7/2/2013 Electronic Data Deliverable (EDD) Sent Separately

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J13060391

2013014682 Collection Date: 21-Jun-13 9:15 AM 

## Site:BOTTOM ASH SLUICE 0.3m Matrix: OTHER
Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst DF SULFIDE - (Analysis Performed by Element One) Vendor Parameter Complete Vendor Method V_ELE1 

## 2013014683 Collection Date: 21-Jun-13 8:14 AM 

## Site:FLYASH SLUICE 0.3m Matrix: OTHER
Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst DF SULFIDE - (Analysis Performed by Element One) Vendor Parameter Complete Vendor Method V_ELE1 

## 2013014684 Collection Date: 21-Jun-13 10:55 AM 

## Site:SOURCE WATER (INTAKE 0.3m Matrix: OTHER
Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst DF SULFIDE - (Analysis Performed by Element One) Vendor Parameter Complete Vendor Method V_ELE1 

## 2013014685 Collection Date: 21-Jun-13 10:50 AM 

## Site:ASH BASIN 0.3m Matrix: OTHER
Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst DF SULFIDE - (Analysis Performed by Element One) Vendor Parameter Complete Vendor Method V_ELE1