## Appendix B - Mercury Tracking Sheet for Boiler Data Review

**Facility/Unit Fuel**  **Category Run #** **Sample**

**Time (min.)** **Sample Volume**  **(dscf) Filter Temp,** 

**avg. (F) Reported** 

**Value (lb/Mmbtu)**  **(W) Hg - Filter** 

**(1B) Hg - Probe**  **Wash (2B) Hg - Nitric** 

**(3A) Hg -** 

**Permanganate (3B)**  **Hg - HCl**

**Rinse (3C) Count of** 

**Hg Fractions** **SUM of Hg**

**Fractions (ug)**  **(X) Reported Hg** 

**Fraction Value (ug)**  **(Y) % Difference** 

**between Reported and Review Values**  **(X-Y)/(X) Calculated lb/mmBtu** 

**Based on Ratio of Measured Fractions**  **Z = (W*X/Y)** AKDoyonUtilities_AK #4 Solid 1 60 60.192 246 3.36E-07 0.03 0.5 0.01 0.05 0.05 5 0.64 0.64 0.00% 3.36E-07 AKDoyonUtilities_AK #4 Solid 2 60 61.418 247 4.12E-07 0.03 0.68 0.01 0.05 0.05 5 0.82 0.82 0.00% 4.12E-07 AKDoyonUtilities_AK #4 Solid 3 60 59.13 244 3.07E-07 0.03 0.44 0.01 0.05 0.05 5 0.58 0.58 0.00% 3.07E-07 GAGPSRMRiincon EU 002 Solid 1 120 60.459 241 8.14E-07 0.78 0.32 0.04 0.06 0.37 5 1.57 1.57 0.00% 8.14E-07 GAGPSRMRiincon EU 002 Solid 2 120 50.327 246 3.20E-07 0.01 0.17 0.01 0.02 0.31 5 0.52 0.51 1.92% 3.26E-07
IDAmalgamatedSugarCoTwinFalls - SB-1 Solid 1 120 78.341 251 2.41E-04 0.01 0.68 0.01 0.16 0.022 5 0.88 0.65 26.30% 3.27E-04 IDAmalgamatedSugarCoTwinFalls - SB-1 Solid 2 12080.205 255 2.50E-04 0.01 0.84 0.01 0.04 0.022 5 0.92 0.73 20.61% 3.15E-04 IDAmalgamatedSugarCoTwinFalls - SB-1 Solid 3 120 77.571 246 2.76E-04 0.01 0.76 0.01 0.16 0.022 5 0.96 0.77 19.75% 3.44E-04 MITBSimonPowerPlant- Unit 1 (6/13/2007) Solid 1 120 78.628 252 7.28E-07 0.44 0.47 1.69 0.05 0.05 5 2.70 1.83 32.22% 1.07E-06 MITBSimonPowerPlant- Unit 1 (6/13/2007) Solid 2 120 76.747 251 2.36E-07 0.21 0.75 0.05 0.05 0.05 5 1.11 0.63 43.24% 4.16E-07 MITBSimonPowerPlant- Unit 1 (6/13/2007) Solid 3 120 74.277 249 1.22E-07 0.04 0.53 0.05 0.05 0.05 5 0.72 0.24 66.67% 3.66E-07 ALIPCourtland No. 3 Combination Boier / 11CU301 Solid 1 240 127 250 4.12E-07 0.15 0.084 0.017 0.034 1.05 5 1.34 1.10 17.60% 5.00E-07 ALIPCourtland No. 3 Combination Boier / 11CU301 Solid 2 240 125 249 5.22E-07 0.0066 0.0008 0.1938 0.261 1.03 5 1.49 1.29 13.55% 6.04E-07 ALIPCourtland No. 3 Combination Boier / 11CU301 Solid 3 240 119 246 3.08E-07 0.0063 0.21 0.0021 0.063 0.561 5 0.84 0.62 26.40% 4.18E-07 GASPNewsprint - PB2 Solid 1 240 163 253 1.17E-07 0.015 0.45 0.0051 0.025 0.03 5 0.53 0.53 0.02% 1.17E-07 GASPNewsprint - PB2 Solid 2 240 139 251 3.45E-07 0.015 0.5 0.005 0.22 0.583 5 1.32 1.32 0.00% 3.45E-07 GASPNewsprint - PB2 Solid 3 240 139 249 4.19E-07 0.015 0.51 0.0114 0.244 0.807 5 1.59 1.59 0.03% 4.19E-07 IAMonsantoMuscatine - Boiler #8 (EP-195) Solid 1 240 165.27 249 1.11E-07 0.04 0.056 0.325 0.001 0.111 5 0.53 0.53 0.00% 1.11E-07 IAMonsantoMuscatine - Boiler #8 (EP-195) Solid 2 240169.796 251 3.28E-07 0.04 0.082 0.831 0.001 0.654 5 1.61 1.61 0.00% 3.28E-07 IAMonsantoMuscatine - Boiler #8 (EP-195) Solid 3 240166.058 251 2.45E-07 0.04 0.064 0.972 0.055 0.063 5 1.19 1.19 0.00% 2.45E-07 IARoquetteAmerica - Circulating Fluidized Bed Boiler (121) Solid 1 192150.658 249 5.92E-08 0.06 0.12 0.12 0.084 0.089 5 0.47 0.32 32.35% 8.75E-08 IARoquetteAmerica - Circulating Fluidized Bed Boiler (121) Solid 2 192151.674 248 3.59E-08 0.06 0.12 0.14 0.11 0.086 5 0.52 0.20 61.24% 9.27E-08 IARoquetteAmerica - Circulating Fluidized Bed Boiler (121) Solid 3 192148.593 242 7.61E-08 0.06 0.12 0.12 0.088 0.084 5 0.47 0.41 13.14% 8.76E-08
ILPolyOne - B1 Solid 1 240172.203No Data 1.08E-07 0.653 0.28 0.0072 0.025 0.017 5 0.98 0.77 21.20% 1.37E-07 ILPolyOne - B1 Solid 2 240164.574No Data 1.62E-07 0.017 0.8 No Data No Data No Data 2 0.82 0.66 18.73% 1.99E-07 ILPolyOne - B1 Solid 3 240165.647No Data 1.42E-07 0.015 0.3 No Data No Data No Data 2 0.32 0.30 4.76% 1.49E-07
MEFPLEnergyWyman Unit #5 Liquid 1No DataNo Data No Data No Data 0.015 0.4 0.0055 0.025 0.153 5 0.60 0.60 -0.25%
MEFPLEnergyWyman Unit #5 Liquid 2No DataNo Data No Data No Data 0.186 0.34 0.0062 0.025 0.165 5 0.72 0.72 0.30%
MEFPLEnergyWyman Unit #5 Liquid 3No DataNo Data No Data No Data 0.015 0.37 0.0058 0.025 0.104 5 0.52 0.52 -0.04% MITBSimonPowerPlant - Unit 1 (2009) Solid 1 240178.791No Data 2.62E-07 0.056Combined 1.71 0.025 Combined 3 1.79 1.60 10.66% 2.93E-07 MITBSimonPowerPlant - Unit 1 (2009) Solid 2 240 198.23 No Data 1.14E-07 0.136Combined 0.8 0.025 Combined 3 0.96 0.77 19.88% 1.42E-07 MITBSimonPowerPlant - Unit 1 (2009) Solid 3 240196.014No Data 1.54E-07 0.347Combined 0.87 0.025 Combined 3 1.24 1.05 15.46% 1.82E-07 NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid 1 240161.884 248 1.68E-07 0.19 2.4 0.1 0.08 0.058 5 2.83 0.25 91.23% 1.92E-06
NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid 2 240166.996 251 1.81E-07 0.24 0.54 0.1 0.08 0.049 5 1.01 0.83 17.84% 2.20E-07
NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid 3 240157.615 255 1.85E-07 0.25 2.3 0.1 0.1 0.027 5 2.78 0.28 90.03% 1.85E-06 NCTysonHarmony - TYS-ES-21 Solid 1 120 77.941 246 2.70E-07 0.6 0.4 0.2 0.5 0.4 5 2.10 0.60 71.43% 9.45E-07 NCTysonHarmony - TYS-ES-21 Solid 2 120 74.864 248 2.50E-07 0.52 0.4 0.2 0.5 0.4 5 2.02 0.52 74.26% 9.71E-07 NCTysonHarmony - TYS-ES-21 Solid 3 12082.735 251 2.10E-07 0.53 0.4 0.2 0.5 0.4 5 2.03 0.53 73.89% 8.04E-07

NJVinelandMuniElectric-HowardDown - Unit 9 Liquid 1 240147.289 250 1.30E-07 0.1 0.6 0.2 0.5 0.714 5 2.11 0.71 66.27% 3.85E-07

NJVinelandMuniElectric-HowardDown - Unit 9 Liquid 2 240149.988 251 2.60E-07 0.1 0.681 0.2 0.5 0.766 5 2.25 1.45 35.47% 4.03E-07
NJVinelandMuniElectric-HowardDown - Unit 9 Liquid 3 240147.912 249 2.20E-07 0.1 0.804 0.2 0.5 0.403 5 2.01 1.21 39.71% 3.65E-07 PABoeingRidleyPark - 033 Liquid 1 240150.708 251 1.29E-07 0.053 0.0051 0.38 0.025 0.295 5 0.76 0.76 0.00% PABoeingRidleyPark - 033 Liquid 2 240139.304 250 9.68E-08 0.015 0.356 0.0051 0.025 0.131 5 0.53 0.53 1.13% 9.79E-08 PABoeingRidleyPark - 033 Liquid 3 240132.854 252 1.16E-07 0.015 0.336 0.0051 0.025 0.173 5 0.55 0.55 1.08% 1.17E-07 PANorfolkSouthern - 031 and 032 and 033 Solid 1 120 71.466 254 1.63E-04 0.6 No DataNo Data 1.83 No Data 2 2.43 1.83 24.69% 2.16E-04 PANorfolkSouthern - 031 and 032 and 033 Solid 2 120 74.91 255 1.25E-04 0.6 No DataNo Data 1.41 No Data 2 2.01 1.41 29.85% 1.78E-04 PANorfolkSouthern - 031 and 032 and 033 Solid 3 120 75.024 258 1.15E-04 0.6 No DataNo Data 1.28 No Data 2 1.88 1.28 31.91% 1.69E-04 SCBowaterCoatedPaper - Combination Boiler No. 2 Solid 1 240163.973 240 2.97E-07 0.015 0.234 0.0064 0.4 0.025 5 0.68 0.68 0.06% 2.97E-07 SCBowaterCoatedPaper - Combination Boiler No. 2 Solid 2 240 178.41 242 3.64E-07 0.016 0.453 0.0054 0.43 0.025 5 0.93 0.93 0.04% 3.64E-07 SCBowaterCoatedPaper - Combination Boiler No. 2 Solid 3 240177.254 244 9.18E-07 0.043 1.24 0.006 0.36 0.025 5 1.67 1.87 -11.95% 8.20E-07 SCBowaterCoatedPaper - Combination Boiler No. 2 Solid 1 96 52.934 233 2.75E-07 0.086 0.44 No Data No Data 0.15 3 0.68 0.24 65.09% 7.88E-07 SCBowaterCoatedPaper - Combination Boiler No. 2 Solid 2 96 53.144 236 2.11E-07 0.074 0.43 No Data No Data 0.11 3 0.61 0.18 70.03% 7.04E-07 TNBowaterNewsprint - Bubbling Fluidized Bed Boiler Solid 1 6041.8825 246 3.00E-07 0.1 0.91 0.04 0.1 0.32 5 1.47 0.91 38.10% 4.85E-07 TNBowaterNewsprint - Bubbling Fluidized Bed Boiler Solid 2 6040.4945 248 4.00E-07 0.07 0.95 0.03 0.1 0.38 5 1.53 0.91 40.52% 6.73E-07 TNBowaterNewsprint - Bubbling Fluidized Bed Boiler Solid 3 60 38.888 251 3.00E-07 0.08 0.87 0.1 0.1 0.24 5 1.39 0.83 40.29% 5.02E-07 

### Hg fractions from Review

## Appendix B - Mercury Tracking Sheet for Boiler Data Review

**Facility/Unit Fuel**  **Category Run #** **Sample**

**Time (min.)** **Sample Volume**  **(dscf) Filter Temp,** 

**avg. (F) Reported** 

**Value (lb/Mmbtu)**  **(W) Hg - Filter** 

**(1B) Hg - Probe**  **Wash (2B) Hg - Nitric** 

**(3A) Hg -** 

**Permanganate (3B)**  **Hg - HCl**

**Rinse (3C) Count of** 

**Hg Fractions** **SUM of Hg**

**Fractions (ug)**  **(X) Reported Hg** 

**Fraction Value (ug)**  **(Y) % Difference** 

**between Reported and Review Values**  **(X-Y)/(X) Calculated lb/mmBtu** 

**Based on Ratio of Measured Fractions**  **Z = (W*X/Y)** **Hg fractions from Review**

TNNissanSmyrna - Boiler 2 Solid 1 60 40.79 258 8.00E-07 0.29 0.17 0.002 0.56 0.05 5 1.07 1.07 0.00% 8.00E-07 TNNissanSmyrna - Boiler 2 Solid 2 60 44.133 256 5.20E-07 0.29 0.06 0.01 0.36 0.05 5 0.77 0.77 0.00% 5.20E-07 TNNissanSmyrna - Boiler 2 Solid 3 60 42.609 255 3.20E-07 0.3 0.03 0.002 0.07 0.05 5 0.45 0.45 0.00% 3.20E-07 TNNissanSmyrna - Boiler 3 Solid 1 60 43.078 261 5.00E-07 0.33 0.09 0.08 0.05 0.21 5 0.76 0.76 0.00% 5.00E-07 TNNissanSmyrna - Boiler 3 Solid 2 60 44.819 260 3.00E-07 0.32 0.03 0.003 0.05 0.05 5 0.45 0.45 0.00% 3.00E-07 TNNissanSmyrna - Boiler 3 Solid 3 60 43.161 261 4.50E-07 0.31 0.06 0.032 0.05 0.21 5 0.66 0.66 0.00% 4.50E-07 VADukeEnergyNarrows Boiler #2 Solid 1 60 42.371 248 2.50E-06 0.1 1.6 0.2 0.5 0.4 5 2.80 1.60 42.86% 4.38E-06 VADukeEnergyNarrows Boiler #2 Solid 2 60 32.941 250 1.91E-06 0.1 1.17 0.2 0.5 0.4 5 2.37 1.17 50.63% 3.87E-06 VADukeEnergyNarrows Boiler #2 Solid 3 60 41.279 255 2.30E-06 0.1 1.65 0.2 0.5 0.4 5 2.85 1.66 41.75% 3.95E-06 VADukeEnergyNarrows Boiler #7 Solid 1 60 46.005 248 9.37E-07 0.1 1.22 0.2 0.5 0.4 5 2.42 1.22 49.59% 1.86E-06 VADukeEnergyNarrows Boiler #7 Solid 2 60 37.101 249 1.19E-06 0.13 1.13 0.2 0.5 0.4 5 2.36 1.26 46.61% 2.23E-06 VADukeEnergyNarrows Boiler #7 Solid 3 60 47.861 251 9.56E-07 0.1 1.32 0.2 0.5 0.4 5 2.52 1.31 48.02% 1.84E-06
VAUniversityofVirginia - 7103-1-01R Solid 1 240 176.38 255 3.69E-07 No Data 0.1 No Data 1.9 No Data 2 2.00 1.31 34.50% 5.63E-07 VAUniversityofVirginia - 7103-1-01R Solid 2 240169.546 257 3.86E-07 No DataNo DataNo Data 1.9 No Data 1 1.90 1.31 31.05% 5.60E-07 VAUniversityofVirginia - 7103-1-01R Solid 3 240177.945 252 3.77E-07 No Data 0.1 No Data 1.9 No Data 2 2.00 1.31 34.50% 5.76E-07
WIGPGreenBay2818 - Stk 10 - Fluidized Bed Boiler #9 - Aug 2004 Solid 4 60 49.33 255 3.81E-06 No Data 0.1 3.29 0.87 No Data 3 4.26 4.16 2.35% 3.90E-06 WIGPGreenBay2818 - Stk 10 - Fluidized Bed Boiler #9 - Aug 2004 Solid 5 60 48.566 251 3.90E-06 No Data 0.1 3.31 0.99 No Data 3 4.40 4.29 2.50% 4.00E-06 WIGPGreenBay2818 - Stk 10 - Fluidized Bed Boiler #9 - Aug 2004 Solid 6 60 53.436 252 3.24E-06 No Data 0.1 2.85 0.62 No Data 3 3.57 3.48 2.52% 3.32E-06

WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - 2005Solid 4 60 41.043 248 3.55E-06 No Data 0.1 4.06 0.5 0.4 4 5.06 4.06 19.76% 4.42E-06

WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - 2005Solid 5 60 40.631 247 6.29E-06 No Data 2.42 4.71 0.5 0.4 4 8.03 7.13 11.21% 7.08E-06

WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - 2005Solid 6 60 41.2 246 6.92E-06 No Data 3.05 4.83 0.5 0.4 4 8.78 7.88 10.25% 7.71E-06
WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - August 2006 Solid 4 60 44.687 267 5.65E-06 No Data 0.1 4.74 0.5 0.56 4 5.90 5.29 10.34% 6.30E-06 WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - August 2006 Solid 5 60 46.809 264 2.90E-06 No Data 0.1 2.36 0.5 0.47 4 3.43 2.83 17.49% 3.51E-06 WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - August 2006 Solid 6 60 48.759 265 2.25E-06 No Data 0.1 2.51 0.5 0.4 4 3.51 2.51 28.49% 3.15E-06 GATempleInlandRome - WF Biomass 1 240141.451 262 3.30E-07 0.52 0.126 0.054 0.08 0.89 5 1.67 1.68 -0.60% 3.28E-07 GATempleInlandRome - WF Biomass 2 240148.796 262 4.20E-07 0.52 0.194 0.05 0.035 1.43 5 2.23 2.23 -0.04% 4.20E-07 GATempleInlandRome - WF Biomass 3 240153.993 263 3.20E-07 0.5 0.113 0.05 0.025 1.05 5 1.74 1.74 -0.12% 3.20E-07

IAArchersDanielsMidlandDesMoines - Asea Boiler #1 Solid 1 240 218.31 250 6.30E-07 No DataNo DataNo Data No Data No Data 0

IAArchersDanielsMidlandDesMoines - Asea Boiler #1 Solid 2 240 214.84 251 6.10E-07 No DataNo DataNo Data No Data No Data 0
IAArchersDanielsMidlandDesMoines - Asea Boiler #1 Solid 3 240 217.37 250 1.00E-08 No DataNo DataNo Data No Data No Data 0 IAUofIowa - EP7 Boiler 11 Biomass 1 240176.255 NR 3.09E-08 0.015 No Data 0.33 0.05 No Data 3 0.40 0.38 3.04% 3.19E-08 IAUofIowa - EP7 Boiler 11 Biomass 2 240172.864 NR 3.22E-08 0.015 No Data 0.32 0.05 No Data 3 0.39 0.37 3.12% 3.32E-08 IAUofIowa - EP7 Boiler 11 Biomass 3 240174.482 NR 3.06E-08 0.015 No Data 0.32 0.05 No Data 3 0.39 0.37 3.12% 3.16E-08 MNGPDuluth - EU33 Boiler #3 Liquid 1 180 15.87 249 9.66E-08 0.01 0.03 0.03 0.07 0.08 5 0.22 0.15 31.82% 1.42E-07 MNGPDuluth - EU33 Boiler #3 Liquid 2 180 148.38 242 4.31E-08 0.01 0.03 0.01 0.07 0.04 5 0.16 0.07 56.25% 9.85E-08 MNGPDuluth - EU33 Boiler #3 Liquid 3 180 144.35 248 3.59E-08 0.01 0.03 0.01 0.06 0.04 5 0.15 0.06 60.00% 8.98E-08 SCCogenSouth - B001 - Main Boiler Solid 1 120 91.6 248 ? 0.11 No Data 0.4 0.68 0.2 4 1.39 0.80 42.45% SCCogenSouth - B001 - Main Boiler Solid 2 120 93.38 251 ? 0.04 No Data 0.4 0.53 0.2 4 1.17 0.57 51.28% SCCogenSouth - B001 - Main Boiler Solid 3 120 87.44 255 ? 0.06 No Data 0.3 0.59 0.2 4 1.15 0.66 42.61% SCCogenSouth - B001 - Main Boiler Solid 1 120 76.74 247 2.40E-07 0.1 0.56 0.5 0.2 4 1.36 0.60 55.88% 5.44E-07 SCCogenSouth - B001 - Main Boiler Solid 2 120 78.3 249 2.50E-07 0.1 0.66 0.5 0.2 4 1.46 0.60 58.90% 6.08E-07 SCCogenSouth - B001 - Main Boiler Solid 3 120 76.47 250 2.10E-07 0.1 0.63 0.5 0.2 4 1.43 0.50 65.03% 6.01E-07 SCCogenSouth - B001 - Main Boiler Solid 1 120 108.73 265 1.80E-06 0.2 2.4 0.2 1.1 1.5 5 5.40 2.60 51.85% 3.74E-06 SCCogenSouth - B001 - Main Boiler Solid 2 120 107.32 266 8.19E-07 0.2 2.6 0.3 0.6 1.9 5 5.60 2.50 55.36% 1.83E-06 SCCogenSouth - B001 - Main Boiler Solid 3 120 106.37 264 7.37E-07 0.2 2.7 0.2 2.1 1 5 6.20 2.10 66.13% 2.18E-06 SCCogenSouth - B001 - Main Boiler Solid 1 240 155.04 253 1.29E-07 0.1 0.2 1 0.5 0.4 5 2.20 0.60 72.73% 4.71E-07

## Appendix B - Mercury Tracking Sheet for Boiler Data Review

**Facility/Unit Fuel**  **Category Run #** **Sample**

**Time (min.)** **Sample Volume**  **(dscf) Filter Temp,** 

**avg. (F) Reported** 

**Value (lb/Mmbtu)**  **(W) Hg - Filter** 

**(1B) Hg - Probe**  **Wash (2B) Hg - Nitric** 

**(3A) Hg -** 

**Permanganate (3B)**  **Hg - HCl**

**Rinse (3C) Count of** 

**Hg Fractions** **SUM of Hg**

**Fractions (ug)**  **(X) Reported Hg** 

**Fraction Value (ug)**  **(Y) % Difference** 

**between Reported and Review Values**  **(X-Y)/(X) Calculated lb/mmBtu** 

**Based on Ratio of Measured Fractions**  **Z = (W*X/Y)** **Hg fractions from Review**

SCCogenSouth - B001 - Main Boiler Solid 2 240 154.94 251 1.13E-07 0.1 0.2 1 0.5 0.4 5 2.20 0.60 72.73% 4.16E-07 SCCogenSouth - B001 - Main Boiler Solid 3 240 158.45 254 2.50E-07 0.1 0.2 1 1.115 0.4 5 2.82 1.12 60.21% 6.28E-07

WVMountainStateCarbonFollansbee - S1 Process Gas 1 240163.271 243 6.88E-06 0.023 3.89 ok 0.152 30.3 4 34.37 34.36 0.01% 6.88E-06

WVMountainStateCarbonFollansbee - S1 Process Gas 2 240124.385 251 5.82E-06 0.051 4.23 ok 0.14 24.1 4 28.52 28.52 0.00% 5.82E-06

WVMountainStateCarbonFollansbee - S1 Process Gas 3 240143.477 251 5.91E-06 0.015 2.75 ok 0.194 25.5 4 28.46 28.46 0.01% 5.91E-06 NCDomtar - 65-25-0310 (No. 2 Hog Fuel Boiler) 1 120 74.893 237 2.01E-06 0.4 2 0.2 0.4 1.2 5 4.20 4.20 0.00% 2.01E-06 NCDomtar - 65-25-0310 (No. 2 Hog Fuel Boiler) 2 120 78.324 238 1.87E-06 0.4 2.2 0.2 0.4 1.1 5 4.30 4.30 0.00% 1.87E-06 NCDomtar - 65-25-0310 (No. 2 Hog Fuel Boiler) 3 120 77.557 237 1.97E-06 0.4 2 0.2 0.4 1.2 5 4.20 4.20 0.00% 1.97E-06 TNCargillMemphis - Stoker Boiler 8001 1 240169.383 257 4.10E-07 0.2 1.3 0.4 0.16 0.28 5 2.34 1.63 30.34% 5.89E-07 TNCargillMemphis - Stoker Boiler 8001 2 240172.476 257 2.70E-07 0.2 0.86 0.4 0.18 0.28 5 1.92 1.14 40.63% 4.55E-07 TNCargillMemphis - Stoker Boiler 8001 3 240158.663 260 2.10E-07 0.2 0.73 0.4 0.16 0.28 5 1.77 0.81 54.24% 4.59E-07 VADukeEnergyNarrows - Boiler #1 1 60 37.837 258 6.17E-07 0.1 0.4 0.2 0.5 0.4 5 1.60 0.50 68.75% 1.97E-06 VADukeEnergyNarrows - Boiler #1 3 60 38.994 261 2.78E-07 0.228 0.4 0.2 0.5 0.4 5 1.73 0.23 86.69% 2.09E-06 VADukeEnergyNarrows - Boiler #1 4 60 38.585 266 2.54E-07 0.198 0.4 0.2 0.5 0.4 5 1.70 0.20 88.22% 2.16E-06 VADukeEnergyNarrows - Boiler #1 1 60 54.38 251 5.07E-06 0.1 3.98 0.41 0.5 0.4 5 5.39 4.39 18.55% 6.22E-06 VADukeEnergyNarrows - Boiler #1 2 60 51.201 252 4.22E-06 0.1 2.94 0.2 0.5 0.4 5 4.14 2.93 29.23% 5.96E-06 VADukeEnergyNarrows - Boiler #1 3 60 55.212 253 4.02E-06 0.1 2.95 0.2 0.5 0.4 5 4.15 2.95 28.92% 5.66E-06 VADukeEnergyNarrows - Boiler #7 1 60 59.38 235 7.25E-07 0.1 0.97 0.2 0.5 0.4 5 2.17 0.97 55.30% 1.62E-06 VADukeEnergyNarrows - Boiler #7 2 60 41.135 236 5.99E-07 0.1 0.61 0.2 0.5 0.4 5 1.81 0.61 66.30% 1.78E-06 VADukeEnergyNarrows - Boiler #7 3 60 43.425 241 6.90E-07 0.1 0.8 0.2 0.5 0.4 5 2.00 0.80 60.00% 1.73E-06 FLRayonierPerformance Condition 1 1 120 78 No Data 2.39E-07 0.412 0.11 0.005 0.41 0.1 5 1.04 0.52 49.86% 4.77E-07 FLRayonierPerformance Condition 1 2 120 74 No Data 2.11E-07 0.346 0.11 0.006 0.44 0.05 5 0.95 0.16 83.19% 1.26E-06 FLRayonierPerformance Condition 1 3 120 66 No Data 1.50E-07 0.333 0.05 0.005 0.42 0.05 5 0.86 0.33 61.54% 3.90E-07 FLRayonierPerformance Condition 2 1 120 74 No Data 3.48E-07 0.669 0.06 0.003 0.44 0.15 5 1.32 0.88 33.43% 5.23E-07 FLRayonierPerformance Condition 2 2 120 73 No Data 3.15E-07 0.7 0.06 0.006 0.45 0.05 5 1.27 0.73 42.34% 5.46E-07 FLRayonierPerformance Condition 2 3 120 71 No Data 1.89E-07 0.639 0.05 0.004 0.38 0.1 5 1.17 0.34 71.01% 6.52E-07 FLRayonierPerformance Condition 3 1 120 73 No Data 2.13E-07 0.503 0.05 0.002 0.35 0.05 5 0.96 0.50 47.64% 4.07E-07 FLRayonierPerformance Condition 3 2 120 69 No Data 1.86E-07 0.389 0.05 0.004 0.35 0.05 5 0.84 0.45 46.62% 3.48E-07 FLRayonierPerformance Condition 3 3 120 71 No Data 3.61E-07 0.772 0.09 0.005 0.45 0.05 5 1.37 0.86 37.09% 5.74E-07 MINeenahPaperMI Boiler 1- 7/25/2006 Solid 1 60 37.18 No Data 4.30E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.54 #DIV/0! 0.00E+00 MINeenahPaperMI Boiler 1- 7/25/2006 Solid 2 60 37.95 No Data 4.20E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.52 #DIV/0! 0.00E+00 MINeenahPaperMI Boiler 1- 7/25/2006 Solid 3 60 38.35 No Data 3.90E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.43 #DIV/0! 0.00E+00 MINeenahPaperMI Boiler 1 - 8/1/2006 Solid 1 60 38.21 No Data 1.20E-07 No DataNo DataNo Data No Data No Data 0 0.00 1.40 #DIV/0! 0.00E+00 MINeenahPaperMI Boiler 1 - 8/1/2006 Solid 2 60 38.68 No Data 8.00E-08 No DataNo DataNo Data No Data No Data 0 0.00 1.00 #DIV/0! 0.00E+00 MINeenahPaperMI Boiler 1 - 8/1/2006 Solid 3 60 36.49 No Data 1.10E-07 No DataNo DataNo Data No Data No Data 0 0.00 1.20 #DIV/0! 0.00E+00 MNDESPHansONyman EU-07 - 3/6/2007 Solid 1 60 45.26 255 5.20E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.68 #DIV/0! 0.00E+00 MNDESPHansONyman EU-07 - 3/6/2007 Solid 2 60 45.56 258 7.30E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.86 #DIV/0! 0.00E+00 MNDESPHansONyman EU-07 - 3/6/2007 Solid 3 60 43.27 256 7.00E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.86 #DIV/0! 0.00E+00
INPurdueUniverisity - Boiler 5 - 7/21/2009 Solid 1 240210.648No Data 1.15E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.90 #DIV/0! 0.00E+00 INPurdueUniverisity - Boiler 5 - 7/21/2009 Solid 2 240210.413No Data 1.35E-07 No DataNo DataNo Data No Data No Data 0 0.00 1.01 #DIV/0! 0.00E+00 INPurdueUniverisity - Boiler 5 - 7/21/2009 Solid 3 240201.621No Data 1.18E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.87 #DIV/0! 0.00E+00
NCGPRoxboro - ES-1 Wood fired Boiler - 7/14/2004 Solid 1 120 64.01 249 3.23E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.49 #DIV/0! 0.00E+00 NCGPRoxboro - ES-1 Wood fired Boiler - 7/14/2004 Solid 2 120 71.68 251 2.43E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.40 #DIV/0! 0.00E+00 NCGPRoxboro - ES-1 Wood fired Boiler - 7/14/2004 Solid 3 120 67.67 253 2.36E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.36 #DIV/0! 0.00E+00 OHAppletonIdeas - Boiler 4 (B003) - 1/31/2003 Solid 1 12095.988 245 3.37E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.80 #DIV/0! 0.00E+00 OHAppletonIdeas - Boiler 4 (B003) - 1/31/2003 Solid 2 120 101.22 247 4.03E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.90 #DIV/0! 0.00E+00 OHAppletonIdeas - Boiler 4 (B003) - 1/31/2003 Solid 3 12096.171 244 4.13E-07 No DataNo DataNo Data No Data No Data 0 0.00 0.90 #DIV/0! 0.00E+00 OKGPMuskogeeMill B-3 - 5/20/2003 Solid 1 120 73.815 243 4.00E-07 No DataNo DataNo Data No Data No Data 0 0.00 No Data #VALUE! #VALUE! OKGPMuskogeeMill B-3 - 5/20/2003 Solid 2 120 73.411 241 4.00E-07 No DataNo DataNo Data No Data No Data 0 0.00 No Data #VALUE! #VALUE! OKGPMuskogeeMill B-3 - 5/20/2003 Solid 3 120 77.913 258 6.00E-07 No DataNo DataNo Data No Data No Data 0 0.00 No Data #VALUE! #VALUE! WIGPGreenBay2818 - B29 - Fluidized Bed Boiler #9 - 1992 - 10/27/1992 Solid 1 120 90.73 255 2.04E-06 No DataNo DataNo Data 0.5 No Data 1 0.50 No Data #VALUE! #VALUE! WIGPGreenBay2818 - B29 - Fluidized Bed Boiler #9 - 1992 - 10/27/1992 Solid 2 120 92.18 257 2.82E-06 No DataNo DataNo Data No Data No Data 0 0.00 No Data #VALUE! #VALUE! WIGPGreenBay2818 - B29 - Fluidized Bed Boiler #9 - 1992 - 10/27/1992 Solid 3 120 100.79 255 7.83E-06 No DataNo DataNo Data No Data No Data 0 0.00 No Data #VALUE! #VALUE!

## Appendix B - Mercury Tracking Sheet for Boiler Data Review

**Facility/Unit**

AKDoyonUtilities_AK #4 AKDoyonUtilities_AK #4 AKDoyonUtilities_AK #4 GAGPSRMRiincon EU 002 GAGPSRMRiincon EU 002
IDAmalgamatedSugarCoTwinFalls - SB-1
IDAmalgamatedSugarCoTwinFalls - SB-1 IDAmalgamatedSugarCoTwinFalls - SB-1 MITBSimonPowerPlant- Unit 1 (6/13/2007) MITBSimonPowerPlant- Unit 1 (6/13/2007) MITBSimonPowerPlant- Unit 1 (6/13/2007) ALIPCourtland No. 3 Combination Boier / 11CU301 ALIPCourtland No. 3 Combination Boier / 11CU301 ALIPCourtland No. 3 Combination Boier / 11CU301 GASPNewsprint - PB2 GASPNewsprint - PB2 GASPNewsprint - PB2 IAMonsantoMuscatine - Boiler #8 (EP-195) IAMonsantoMuscatine - Boiler #8 (EP-195) IAMonsantoMuscatine - Boiler #8 (EP-195) IARoquetteAmerica - Circulating Fluidized Bed Boiler (121) IARoquetteAmerica - Circulating Fluidized Bed Boiler (121) IARoquetteAmerica - Circulating Fluidized Bed Boiler (121)
ILPolyOne - B1
ILPolyOne - B1 ILPolyOne - B1
MEFPLEnergyWyman Unit #5
MEFPLEnergyWyman Unit #5
MEFPLEnergyWyman Unit #5 MITBSimonPowerPlant - Unit 1 (2009) MITBSimonPowerPlant - Unit 1 (2009) MITBSimonPowerPlant - Unit 1 (2009)
NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler)
NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler)
NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) NCTysonHarmony - TYS-ES-21 NCTysonHarmony - TYS-ES-21 NCTysonHarmony - TYS-ES-21

NJVinelandMuniElectric-HowardDown - Unit 9

NJVinelandMuniElectric-HowardDown - Unit 9
NJVinelandMuniElectric-HowardDown - Unit 9 PABoeingRidleyPark - 033 PABoeingRidleyPark - 033 PABoeingRidleyPark - 033 PANorfolkSouthern - 031 and 032 and 033 PANorfolkSouthern - 031 and 032 and 033 PANorfolkSouthern - 031 and 032 and 033 SCBowaterCoatedPaper - Combination Boiler No. 2 SCBowaterCoatedPaper - Combination Boiler No. 2 SCBowaterCoatedPaper - Combination Boiler No. 2 SCBowaterCoatedPaper - Combination Boiler No. 2 SCBowaterCoatedPaper - Combination Boiler No. 2 TNBowaterNewsprint - Bubbling Fluidized Bed Boiler TNBowaterNewsprint - Bubbling Fluidized Bed Boiler TNBowaterNewsprint - Bubbling Fluidized Bed Boiler 

### Hg - Filter **(1B) Hg - Probe** 

**Wash (2B) Hg - Nitric** 

**(3A) Hg -** 

**Permanganate (3B)**  **Hg - HCl**

**Rinse (3C) Notes**  **ACTION Pre-Corrected**  **Hg Value (lb/mmBtu)** 

0.03 0.42 0.01 0.05 0.05 Do not change 0.03 0.42 0.01 0.05 0.05 Do not change 0.03 0.42 0.01 0.05 0.05 Do not change 0.01 0.3 0.01 0.05 0.05 Do not change 0.01 0.3 0.01 0.05 0.05 Updated value to calculated lb/mmBtu value, Z

0.01 0.01 0.04 0.04 0.022Blank subtraction was 22.7% of sample catch. Did not use DL as sample weight when result less than DL. (bias 2% low) Do not change, facility submitted corrections 2.56E-07

0.01 0.01 0.04 0.04 0.022Blank subtraction was 22.7% of sample catch. Did not use DL as sample weight when result less than DL. (bias 2% low) Do not change, facility submitted corrections 2.80E-07

0.01 0.01 0.04 0.04 0.022Blank subtraction was 22.7% of sample catch. Did not use DL as sample weight when result less than DL. (bias 2% low) Do not change, facility submitted corrections 2.92E-07 0.05 0.05 0.05 0.05 0.0530% blank subtraction Updated value to calculated lb/mmBtu value, Z 0.05 0.05 0.05 0.05 0.0535% blank subtraction Updated value to calculated lb/mmBtu value, Z 0.05 0.05 0.05 0.05 0.0558% blank subtraction Updated value to calculated lb/mmBtu value, Z 0.015 0.005 0.025 0.025 0.025 Updated value to calculated lb/mmBtu value, Z 0.0066 0.008 0.025 0.025 0.025 Updated value to calculated lb/mmBtu value, Z 0.0063 0.0021 0.025 0.025 0.025 Updated value to calculated lb/mmBtu value, Z 0.015 0.45 0.0051 0.025 0.025 Do not change 0.015 0.49 0.0051 0.05 0.025 Do not change 0.015 0.51 0.0049 0.025 0.025 Do not change 0.004 0.03 0.03 0.001 0.003 Do not change 0.004 0.03 0.03 0.001 0.003 Do not change 0.004 0.03 0.03 0.001 0.003 Do not change 0.06 0.12 0.12 0.038 0.089Data reported without considering BDL data Updated value to calculated lb/mmBtu value, Z 0.06 0.12 0.14 0.041 0.086Data reported without considering BDL data Updated value to calculated lb/mmBtu value, Z 0.06 0.12 0.12 0.043 0.084Data reported without considering BDL data Updated value to calculated lb/mmBtu value, Z

0.15 0.015 0.043 No Data No Data17% blank subtraction - Used Hg fractions reported in ERT to update valueUpdated value to calculated lb/mmBtu value, Z

0.15 0.015 0.043 No Data No Data18% blank subtraction - Used Hg fractions reported in ERT to update valueUpdated value to calculated lb/mmBtu value, Z

0.15 0.015 0.043 No Data No DataNon detect on third run, reported as less than MDL (0.3) - Used Hg fractions reported in ERT to update value Updated value to calculated lb/mmBtu value, Z

0.015 0.34 0.0055 0.025 0.025All lab data present, but no test report. No way to confirm volume or mass emissions rate Do not change, data verified through ERT

0.015 0.34 0.0062 0.025 0.025All lab data present, but no test report. No way to confirm volume or mass emissions rate Do not change, data verified through ERT

0.015 0.37 0.0058 0.025 0.025All lab data present, but no test report. No way to confirm volume or mass emissions rate Do not change, data verified through ERT 0.015 0.15 No Data 0.025 No DataNo field data sheets to validate q/a. Do not change, facility submitted corrections 2.70E-07 0.015 0.15 No Data 0.025 No DataNo field data sheets to validate q/a. Do not change, facility submitted corrections 1.22E-07 0.015 0.15 No Data 0.025 No DataNo field data sheets to validate q/a. Do not change, facility submitted corrections 1.61E-07

0.03 2.4 0.1 0.08 0.1Report does not contain enough information to determine how blank subtraction was handled. MDL values for Nitric/Peroxide are very high. Updated value to calculated lb/mmBtu value, Z

0.03 2.2 0.1 0.08 0.1Report does not contain enough information to determine how blank subtraction was handled. MDL values for Nitric/Peroxide are very high. Updated value to calculated lb/mmBtu value, Z

0.03 2.3 0.1 0.1 0.1Report does not contain enough information to determine how blank subtraction was handled. MDL values for Nitric/Peroxide are very high. Updated value to calculated lb/mmBtu value, Z 0.4 0.4 0.2 0.5 0.4High detection limit, 70% blank subtraction Updated value to calculated lb/mmBtu value, Z 0.4 0.4 0.2 0.5 0.4High detection limit, 70% blank subtraction Updated value to calculated lb/mmBtu value, Z 0.4 0.4 0.2 0.5 0.4High detection limit, 70% blank subtraction Updated value to calculated lb/mmBtu value, Z

0.1 0.6 0.2 0.5 0.2High detection limits, blank subtraction % high. Half of field data sheets missing from report Updated value to calculated lb/mmBtu value, Z

0.1 0.6 0.2 0.5 0.2High detection limits, blank subtraction % high. Half of field data sheets missing from report Updated value to calculated lb/mmBtu value, Z

0.1 0.6 0.2 0.5 0.2High detection limits, blank subtraction % high. Half of field data sheets missing from report Updated value to calculated lb/mmBtu value, Z 0.015 0.15 0.005 0.013 0.013 Do not change 0.015 0.15 0.005 0.013 0.013 Updated value to calculated lb/mmBtu value, Z 0.015 0.15 0.005 0.013 0.013 Updated value to calculated lb/mmBtu value, Z No DataNo Data 0.22 1 1 Five Hg fractions not available Remove test data from floor calculations No DataNo DataNo Data No Data No DataFive Hg fractions not available Remove test data from floor calculations No DataNo DataNo Data No Data No DataFive Hg fractions not available Remove test data from floor calculations 0.015 0.025 0.0052 0.4 0.025 Do not change 0.015 0.025 0.0054 0.43 0.025 Do not change 0.015 0.025 0.0049 0.36 0.025Run appears to be reported 11% high. Updated value to calculated lb/mmBtu value, Z No Data 0.3 No Data No Data No Data65 % blank reduction - only 2 runs Remove test data from floor calculations No Data 0.3 No Data No Data No Data70% blank reduction - only 2 runs. Remove test data from floor calculations 0.03 0.9 0.02 0.1 0.1 Updated value to calculated lb/mmBtu value, Z 0.03 0.9 0.02 0.1 0.1 Updated value to calculated lb/mmBtu value, Z 0.03 0.9 0.02 0.1 0.1 Updated value to calculated lb/mmBtu value, Z



### Reported Detection limits (ug)

## Appendix B - Mercury Tracking Sheet for Boiler Data Review

**Facility/Unit**

TNNissanSmyrna - Boiler 2 TNNissanSmyrna - Boiler 2 TNNissanSmyrna - Boiler 2 TNNissanSmyrna - Boiler 3 TNNissanSmyrna - Boiler 3 TNNissanSmyrna - Boiler 3 VADukeEnergyNarrows Boiler #2 VADukeEnergyNarrows Boiler #2 VADukeEnergyNarrows Boiler #2 VADukeEnergyNarrows Boiler #7 VADukeEnergyNarrows Boiler #7 VADukeEnergyNarrows Boiler #7
VAUniversityofVirginia - 7103-1-01R
VAUniversityofVirginia - 7103-1-01R VAUniversityofVirginia - 7103-1-01R
WIGPGreenBay2818 - Stk 10 - Fluidized Bed Boiler #9 - Aug 2004 WIGPGreenBay2818 - Stk 10 - Fluidized Bed Boiler #9 - Aug 2004 WIGPGreenBay2818 - Stk 10 - Fluidized Bed Boiler #9 - Aug 2004

WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - 2005

WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - 2005

WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - 2005
WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - August 2006 WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - August 2006 WIGPGreenBay2818 - Stack 10 - Fluidized Bed Boiler #9 - August 2006 GATempleInlandRome - WF GATempleInlandRome - WF GATempleInlandRome - WF

IAArchersDanielsMidlandDesMoines - Asea Boiler #1

IAArchersDanielsMidlandDesMoines - Asea Boiler #1
IAArchersDanielsMidlandDesMoines - Asea Boiler #1 IAUofIowa - EP7 Boiler 11 IAUofIowa - EP7 Boiler 11 IAUofIowa - EP7 Boiler 11 MNGPDuluth - EU33 Boiler #3 MNGPDuluth - EU33 Boiler #3 MNGPDuluth - EU33 Boiler #3 SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler 

### Hg - Filter **(1B) Hg - Probe** 

**Wash (2B) Hg - Nitric** 

**(3A) Hg -** 

**Permanganate (3B)**  **Hg - HCl**

**Rinse (3C) Notes**  **ACTION Pre-Corrected**  **Hg Value (lb/mmBtu)**  **Reported Detection limits (ug)**

0.03 0.29 0.002 0.05 0.05 Do not change 0.03 0.29 0.002 0.05 0.05 Do not change 0.03 0.3 0.002 0.05 0.05 Do not change 0.03 0.33 0.004 0.05 0.05 Do not change 0.03 0.32 0.002 0.05 0.05 Do not change 0.03 0.31 0.003 0.05 0.05 Do not change 0.1 No Data 0.2 0.5 0.4DL data not reported. Updated value to calculated lb/mmBtu value, Z 0.1 No Data 0.2 0.5 0.4DL data not reported. Updated value to calculated lb/mmBtu value, Z 0.1 No Data 0.2 0.5 0.4DL data not reported. Updated value to calculated lb/mmBtu value, Z 0.1 No Data 0.2 0.5 0.4DL data not reported. Updated value to calculated lb/mmBtu value, Z 0.1 No Data 0.2 0.5 0.4DL data not reported. Updated value to calculated lb/mmBtu value, Z 0.1 No Data 0.2 0.5 0.4DL data not reported. Updated value to calculated lb/mmBtu value, Z

No DataNo DataNo Data No Data No DataScant metals data from lab. Front and back half, no way to tell how blanks were treated. Do not change, data verified through ERT

No DataNo DataNo Data No Data No DataScant metals data from lab. Front and back half, no way to tell how blanks were treated. Do not change, data verified through ERT

No DataNo DataNo Data No Data No DataScant metals data from lab. Front and back half, no way to tell how blanks were treated. Do not change, data verified through ERT

No Data 0.1 0.3 0.5 No DataFive Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

No Data 0.1 0.3 0.5 No DataFive Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

No Data 0.1 0.3 0.5 No DataFive Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

? 0.1 0.3 0.5 0.4Five Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

? 0.1 0.3 0.5 0.4Five Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

? 0.1 0.3 0.5 0.4Five Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

? 0.1 0.5 0.5 0.4Five Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

? 0.1 0.5 0.5 0.4Five Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations

? 0.1 0.5 0.5 0.4Five Hg fractions not reported - 1 reported number for "front half" so it is not clear that both probe rinse and filter were combined or if one was not analyzed. Remove test data from floor calculations 0.52 0.015 0.045 0.05 0.025 Do not change 0.052 0.015 0.045 0.025 0.025 Do not change 0.05 0.015 0.05 0.025 0.025 Do not change

No DataNo DataNo Data No Data No DataLab results in concentration (mg/L) with no correlation to volume submitted. Data presented as <DL Do not change, facility submitted corrections 3.18E-08

No DataNo DataNo Data No Data No DataLab results in concentration (mg/L) with no correlation to volume submitted. Data presented as <DL Do not change, facility submitted corrections 2.80E-08

No DataNo DataNo Data No Data No DataRun 3 very low, sixteen times less than R1 and R2, yet had detection ABOVE R1 and R2. Do not change, facility submitted corrections 5.53E-08 0.015 0.33 No Data 0.025 0.013Five Hg fractions not available Remove test data from floor calculations 0.015 0.32 No Data 0.025 0.013Five Hg fractions not available Remove test data from floor calculations 0.015 0.32 No Data 0.025 0.013Five Hg fractions not available Remove test data from floor calculations 0.01 0.03 0.01 0.04 0.04Reported ND as zero. Do not change, NCASI submitted corrections 1.28E-07 0.01 0.03 0.01 0.04 0.04Reported ND as zero. Do not change, NCASI submitted corrections 9.77E-08 0.01 0.03 0.01 0.04 0.04Reported ND as zero. Do not change, NCASI submitted corrections 8.91E-08 No DataNo Data 0.4 No Data 0.2Reported ND as zero. Do not change, NCASI submitted corrections 4.56E-07 No DataNo Data 0.4 No Data 0.2Reported ND as zero. Do not change, NCASI submitted corrections 3.75E-07 No DataNo Data 0.4 No Data 0.2Reported ND as zero. Do not change, NCASI submitted corrections 3.97E-07 No Data 0.1 0.56 0.5 0.2Reported ND as zero. Do not change, NCASI submitted corrections 5.55E-07 No Data 0.1 0.66 0.5 0.2Reported ND as zero. Do not change, NCASI submitted corrections 6.05E-07 No Data 0.1 0.63 0.5 0.2Reported ND as zero. Do not change, NCASI submitted corrections 5.98E-07 0.2 0.7 0.4 0.1 1 Reported ND as zero. Do not change, NCASI submitted corrections 1.62E-06 0.2 0.7 0.4 0.1 1 Reported ND as zero. Do not change, NCASI submitted corrections 1.78E-06 0.2 0.7 0.4 0.1 1 Reported ND as zero. Do not change, NCASI submitted corrections 1.87E-06 0.1 0.2 1.52 0.5 0.4Reported ND as zero. Do not change, NCASI submitted corrections 4.60E-07

## Appendix B - Mercury Tracking Sheet for Boiler Data Review

**Facility/Unit**

SCCogenSouth - B001 - Main Boiler SCCogenSouth - B001 - Main Boiler

WVMountainStateCarbonFollansbee - S1

WVMountainStateCarbonFollansbee - S1

WVMountainStateCarbonFollansbee - S1 NCDomtar - 65-25-0310 (No. 2 Hog Fuel Boiler) NCDomtar - 65-25-0310 (No. 2 Hog Fuel Boiler) NCDomtar - 65-25-0310 (No. 2 Hog Fuel Boiler) TNCargillMemphis - Stoker Boiler 8001 TNCargillMemphis - Stoker Boiler 8001 TNCargillMemphis - Stoker Boiler 8001 VADukeEnergyNarrows - Boiler #1 VADukeEnergyNarrows - Boiler #1 VADukeEnergyNarrows - Boiler #1 VADukeEnergyNarrows - Boiler #1 VADukeEnergyNarrows - Boiler #1 VADukeEnergyNarrows - Boiler #1 VADukeEnergyNarrows - Boiler #7 VADukeEnergyNarrows - Boiler #7 VADukeEnergyNarrows - Boiler #7 FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance FLRayonierPerformance MINeenahPaperMI Boiler 1- 7/25/2006 MINeenahPaperMI Boiler 1- 7/25/2006 MINeenahPaperMI Boiler 1- 7/25/2006 MINeenahPaperMI Boiler 1 - 8/1/2006 MINeenahPaperMI Boiler 1 - 8/1/2006 MINeenahPaperMI Boiler 1 - 8/1/2006 MNDESPHansONyman EU-07 - 3/6/2007 MNDESPHansONyman EU-07 - 3/6/2007 MNDESPHansONyman EU-07 - 3/6/2007
INPurdueUniverisity - Boiler 5 - 7/21/2009 INPurdueUniverisity - Boiler 5 - 7/21/2009 INPurdueUniverisity - Boiler 5 - 7/21/2009
NCGPRoxboro - ES-1 Wood fired Boiler - 7/14/2004
NCGPRoxboro - ES-1 Wood fired Boiler - 7/14/2004 NCGPRoxboro - ES-1 Wood fired Boiler - 7/14/2004 OHAppletonIdeas - Boiler 4 (B003) - 1/31/2003 OHAppletonIdeas - Boiler 4 (B003) - 1/31/2003 OHAppletonIdeas - Boiler 4 (B003) - 1/31/2003 OKGPMuskogeeMill B-3 - 5/20/2003 OKGPMuskogeeMill B-3 - 5/20/2003 OKGPMuskogeeMill B-3 - 5/20/2003 WIGPGreenBay2818 - B29 - Fluidized Bed Boiler #9 - 1992 - 10/27/1992 WIGPGreenBay2818 - B29 - Fluidized Bed Boiler #9 - 1992 - 10/27/1992 WIGPGreenBay2818 - B29 - Fluidized Bed Boiler #9 - 1992 - 10/27/1992 

### Hg - Filter **(1B) Hg - Probe** 

**Wash (2B) Hg - Nitric** 

**(3A) Hg -** 

**Permanganate (3B)**  **Hg - HCl**

**Rinse (3C) Notes**  **ACTION Pre-Corrected**  **Hg Value (lb/mmBtu)**  **Reported Detection limits (ug)**

0.1 0.2 1.52 0.5 0.4Reported ND as zero. Do not change, NCASI submitted corrections 4.64E-07 0.1 0.2 1.52 0.5 0.4Reported ND as zero. Do not change, NCASI submitted corrections 5.91E-07

0.015 0.57 No Data 0.025 0.25Lab data lacks sample 3A, which is not an optional part of the sample. However, email from testing firm shows that omission of 3A did not affect measurement Do not change

0.015 0.49 No Data 0.025 0.25Lab data lacks sample 3A, which is not an optional part of the sample. However, email from testing firm shows that omission of 3A did not affect measurement Do not change

0.015 0.51 No Data 0.025 0.25Lab data lacks sample 3A, which is not an optional part of the sample. However, email from testing firm shows that omission of 3A did not affect measurement Do not change 0.4 0.9 0.2 0.2 1.2 Do not change 0.4 0.9 0.2 0.2 1.2 Do not change 0.4 0.9 0.2 0.2 1.2 Do not change 0.2 0.4 0.4 0.16 0.28Reported ND as zero. Do not change, NCASI submitted corrections 4.10E-07 0.2 0.4 0.4 0.16 0.28Reported ND as zero. Do not change, NCASI submitted corrections 5.60E-07 0.2 0.4 0.4 0.16 0.28Reported ND as zero. Do not change, NCASI submitted corrections 4.30E-07 0.1 0.4 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 6.17E-07 0.1 0.4 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 2.78E-07 0.1 0.4 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 2.54E-07 0.1 0.2 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 5.07E-06 0.1 0.2 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 4.22E-06 0.1 0.2 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 4.02E-06 0.1 0.2 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 7.25E-07 0.1 0.2 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 5.99E-07 0.1 0.2 0.2 0.5 0.4Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 6.90E-07 0.015 0.05 0.005 0.41 0.1Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.006 0.44 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.005 0.42 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.005 0.41 0.1Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.006 0.44 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.005 0.42 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.002 0.35 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.004 0.35 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z 0.015 0.05 0.004 0.35 0.05Reported ND as zero. Updated value to calculated lb/mmBtu value, Z No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations

No DataNo DataNo Data No Data No DataReport did not provide lab data, however the calculations were able to be confirmed correct. Do not change

No DataNo DataNo Data No Data No DataReport did not provide lab data, however the calculations were able to be confirmed correct. Do not change

No DataNo DataNo Data No Data No DataReport did not provide lab data, however the calculations were able to be confirmed correct. Do not change

No DataNo DataNo Data No Data No DataReport did not provide lab data. Tests for "engineering study" may not have been conducted to meet compliance or all method criteria. Remove test data from floor calculations

No DataNo DataNo Data No Data No DataReport did not provide lab data. Tests for "engineering study" may not have been conducted to meet compliance or all method criteria. Remove test data from floor calculations

No DataNo DataNo Data No Data No DataReport did not provide lab data. Tests for "engineering study" may not have been conducted to meet compliance or all method criteria. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations No DataNo DataNo Data No Data No DataReport did not provide lab data. Remove test data from floor calculations

No DataNo DataNo Data No Data No DataImpossible to confirm data as lab data is poorly labeled. Remove test data from floor calculations

No DataNo DataNo Data No Data No DataImpossible to confirm data as lab data is poorly labeled. Remove test data from floor calculations

No DataNo DataNo Data No Data No DataImpossible to confirm data as lab data is poorly labeled. Remove test data from floor calculations