Test Report 

Evaluation of Particulate, Total Chromium and Hexavalent Chromium 

Emissions from the Owens Corning Delmar DM1 and DM2 Furnace DEP 

Outlets to satisfy Section 114 Information Collection Request 

January 2011 

Prepared for: 

Owens Corning insulating Systems, LLC 

1277 Feura Bush Road 

Feura Bush, NY 

12067-1719 

Attention: Mr. David Krenitsky

Prepared by: 

LEHDER Environmental Services Limited 

704 Mara Street, Suite 210 

Point Edward, ON 

N7V 1X4 

Project No.: 123987

February 25, 2012

LEHDER Environmental Services Limited 

 704 Mara Street, Suite 210, Point Edward, Ontario, Canada N7V 1X4 Phone: (519) 336-4101 Fax: (519) 336-4311 

 9954 – 62 Avenue, Edmonton, Alberta Canada T6E 0P5 Phone: (780) 462-4099 Fax: (780) 462-4392 

www.lehder.com 
 ii

Executive Summary

LEHDER Environmental Services Limited (LEHDER) of Point Edward, Ontario was retained 

by Owens Corning to conduct a stack testing program at its wool fiberglass insulation 

manufacturing facility located at 1277 Feura Bush Road, Feura Bush (Delmar), New York. 

The purpose of the testing program was to satisfy an Information Collection Request (ICR) 

authorized under Section 114 of the Clean Air Act. Stack emissions from glass melting 

operations are targeted under this initiative. Test contaminants and methods specified by 

the Section 114 request are: 

 

Chromium (7440-47-3) 

 Filterable – EPA Method 29 

 Vaporous – EPA Method 29 

 Total – EPA Method 29 and SW-846 Method 0061 

Hexavalent Chromium (1854-02-99) 

 SW-846 Method 0061 

Particulate Matter 

 EPA Method 5/29 

Exhaust gases from the Owens Corning Delmar DM1 and DM2 glass melting furnaces were 

identified for testing under the Section 114 initiative. Emissions from these sources were 

evaluated during the week of January 23, 2012. A summary of the average test results is 

presented in Table I. 

Table I 

Summary of Emission Data from DM1 & DM2 Furnace DEP Outlets – January 2012 

Method 29 Method 0061 

Pollutant Units 

DM1 DEP DM2 DEP DM1 DEP DM2 DEP 

mg/S.m3 1.5 7.9 Filterable Particulate 

lb/hr 0.045 0.25 

μg/S.m3 4.8 41 Filterable Chromium 

lb/hr 1.4E-04 1.3E-03 

μg/S.m3 0.14 0.22 Vaporous Chromium 

lb/hr 4.1E-06 6.8E-06 

μg/S.m3 4.9 41 4.9 41 Total Chromium 

lb/hr 1.5E-04 1.3E-03 1.5E-04 1.3E-03 

μg/S.m3 2.7 36 Hexavalent Chromium 

lb/hr 8.4E-05 1.1E-03 
iii 

Table of Contents 

Executive Summary............................................................................................ii 

1. Introduction ...................................................................................................................1

1.1 Background .............................................................................................................1 

1.2 Description of Testing Program...............................................................................1 

1.3 Test Program Organization .....................................................................................2 

2. Source Description .......................................................................................................3

3. Description of Sources and Sampling Locations ......................................................5

4. Test Methods .................................................................................................................6

4.1 Total and Hexavalent Chromium – Method 0061....................................................7 

4.2 Filterable Particulate and Total Chromium - EPA Method 29................................12 

5. Test Results.................................................................................................................16

6. Discussion of Results.................................................................................................20

6.1 General..................................................................................................................20

6.2 Particulate Emission Summary .............................................................................20 

6.3 Total Chromium - Method 29 vs. Method 0061 .....................................................21 

6.4 Method 0061 Hexavalent and Total Chromium Data ............................................21 

6.5 QA/QC...................................................................................................................23 

7. Closure.........................................................................................................................24
iv 

List of Tables and Figures 

Table 3-1: Description of Sources and Sampling Locations ...................................................5 

Table 4-1: Summary of Sampling and Analytical Methods .....................................................6 

Table 4-2: Specifications for Hexavalent Chromium (Method 0061).......................................7 

Table 4-3: Specifications for PM/Metals Sampling (EPA Method 29)...................................12 

Table 5-1: Summary of Method 0061 Test Results – DM1 Furnace DEP Outlet..................16 

Table 5-2: Summary of Method 0061 Test Results – DM2 Furnace DEP Outlet..................17 

Table 5-3: Summary of Method 29 Test Results – DM1 Furnace DEP Outlet......................18 

Table 5-4: Summary of Method 29 Test Results – DM2 Furnace DEP Outlet......................19 

Table 6-1: Average Particulate Test Results – DM1 & DM2 Furnace DEP Outlets ..............20 

Table 6-2: Total Chromium Data – Method 29 vs. Method 0061 ..........................................21 

Table 6-3: Method 0061 – Hexavalent Chromium vs. Total Chromium ................................22 

Figure 2-1: General Process Flow Schematic.........................................................................3 

Figure 4-1: Schematic of EPA Method 0061 Sampling Train................................................10 

Figure 4-2: Sample Recovery Flow Chart – Method 0061 Test Runs...................................11 

Figure 4-3: Sample Recovery – Method 29 Test Runs .........................................................14 

Figure 4-4: Schematic of EPA Method 29 Sampling Train....................................................15 

Appendices 

Appendix A: Concentration and Mass Rate Calculations 

 A.1: Method 29 Test Runs 

 A.2: Method 0061 Test Runs 

Appendix B: Analytical Report 

 B.1: Enthalpy PM Report 

 B.2: Element One M29 Report 

 B.3: Element One M0061 Report 

Appendix C: Equipment Calibrations 

Appendix D: Field Data Sheets 

 D.1: Field Run Sheets 

 D.2: Sample Recovery Data Sheets 

 D.3: Cyclonic Flow Data Sheet 

Appendix E: Sample Point Markings & Site Photographs 

Pertinent process data and lb/ton emissions are contained on Confidential CD 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 1 of 24

1. Introduction 

1.1 Background 

The U.S. Environmental Protection Agency (USEPA) is collecting information on particulate 

matter (PM), chromium compounds, hexavalent chromium, and other related information 

from wool fiberglass manufacturing facilities. The information gathered will be used by the 

EPA to perform a review of the maximum achievable control technology (MACT) standard in 

40 CFR Part 63, subpart NNN. The authority to request this information is reference under 

Section 114 of the Clean Air Act (CAA) (42 U.S.C. 7414). 

Stack emissions from glass melting operations are targeted under this initiative. Specifically, 

test compounds and methods specified by the Section 114 request are: 

 

Chromium (7440-47-3) 

 Filterable – EPA Method 29 

 Vaporous – EPA Method 29 

 Total – EPA Method 29 and SW-846 Method 0061 

Hexavalent Chromium (1854-02-99) 

 SW-846 Method 0061 

Particulate Matter 

 EPA Method 5/29 

The DM1 and DM2 Furnace DEP outlets located at the Owens Corning Delmar Plant were 

sources identified for evaluation by the Section 114 initiative. Emission data are required to 

be reported through the USEPA Electronic Reporting Tool (ERT) and are due to applicable 

USEPA offices by the end of February 2012. 

1.2 Description of Testing Program 

Owens Corning retained LEHDER Environmental Services (LEHDER) to conduct the source 

testing required by the Section 114 initiative at its wool fiberglass manufacturing facility in 

Delmar, New York (referred to in this report as OC Delmar). The program involved the 

evaluation of emissions from the DM1 and DM2 Furnace DEP Outlets. DEP is an 

abbreviation for “Dry Electrostatic Precipitator”. 

Both sources were evaluated for filterable particulate, filterable chromium and vaporous 

chromium in accordance with USEPA Method 29. Total and hexavalent chromium 

emissions were also determined in accordance with USEPA Method 0061. 

Three test runs were performed for each of the two test methods. Method 29 test runs could 

not be carried out simultaneously with Method 0061 runs due to physical limitations at the 

test sites. However, one of each test run was conducted on each of the two sources each 

day. To ensure detection of the test compounds, sample runs were initially set for 240 

minutes (4.0 hours). 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 2 of 24

Both DM1 and DM2 furnaces were operating at normal rates during the sampling campaign. 

Process/production data were monitored and collected by Owens Corning personnel. 

Testing was conducted from January 24 to 26, 2012. 

 

1.3 Test Program Organization

Facility ID / Address: 

Owens Corning Delmar Plant 

1277 Feura Bush Road 

Feura Bush, NY USA 12067-1719

Facility ID: 3600100066 

Industry NAICS: 327993 

AFS#: 3600100066 

FRS#: 110000324168 

Air Permit #: 4-0122-00004/00039 

Facility Environmental 

Manager: 

Mr. David Krenitsky 

Tel: 518-475-3673 

Email: david.krenitsky@owenscorning.com 

Facility Site/Project 

Contacts: 

Mr. Rick Cooper 

Owens Corning Science and Technology Center 

Granville, OH 

Tel: 740-321-7628 

Fax: 740-321-4628 

Email: rick.d.cooper@owenscorning.com 

Sampling Company: 

LEHDER Environmental Services Limited 

704 Mara Street, Suite 210 

Point Edward, ON N7V 1X4 

LEHDER Project Manager: 

Mr. Mike Denomme 

Tel: 519-336-4101 Ext. 225 Fax: 519-336-4311 

E-mail: mdenomme@lehder.com 

LEHDER Field Crew: Chris Ungar, Joy Edwards, Jordan Denomme, 

John Haaland, Paul Baker, Rick Seller and Justin Tayles 

Analytical Laboratory #1: 

M29 Particulate Analysis 

Enthalpy Analytical Inc. 

800 Capitola Dr., Ste. 1 

Durham, NC 27713 

Tel: 919-850-4392 Fax: 919-850-9012 

Contact: Mr. Bryan Tyler 

E-mail: bryan.tyler@enthalpy.com 

Analytical Laboratory #2: 

M29 & M0061 Total Chromium/ 

Hexavalent Chromium Analysis 

Element One, Inc. 

5022-C Wrightsville Av., 

Wilmington, NC 28403 

Tel: 910-793-0128 Fax: 910-792-6853 

Contact: Ms. Paula Smith 

E-mail: paula.smith @e1lab.com 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 3 of 24

2. Source Description 

The Owens Corning Delmar plant manufactures rotary spun (RS) fiberglass building 

insulation. There are two production lines designated DM1 and DM2. The manufacture of 

fiberglass insulation is a continuous process that takes place through the following major 

steps: 

  Glass melting 

  Formation of fiber/addition of binder 

  Pack curing 

  Cooling, trimming and packaging 

The major process steps are described in more detail in the following sections and a 

process flow schematic is presented in Figure 2-1 

Figure 2-1: General Process Flow Schematic 

Mixed 

Glass 

Batch 

with 

Cullett 

Fiber Pack 

Forming 

Tunnel 

Curing

Oven 

Cooling, 

Fabrication, 

Packaging & 

Storage 

Operations

Channel/Forehearh

Wet Fiber Pack 

w/ Uncured 

Binder 

Cured 

Pack 

IWS 

Exhaust to atmosphere via 

WEP Stacks (DM1) or 

Mixing Chamber Stack 

(DM1 & DM2)

Forming 

Fans

Molten Glass 

Energy

(electric, gas or 

some combination) 

Combined with forming 

effluent in Mixing Chamber 

Stack and discharged

Gas

Batch Systems 

Veils of 

Coated 

Fibers Air

Exhaust to Atmosphere

Glass 

Melting 

Furnace 

Fiber Coating/ 

Binder Application

Air Gas

Water Binder

Dry Electrostatic 

Precipitator (DEP) 

Exhaust to 

atmosphere via 

Smoke Stripper and 

Cooling Stacks 

 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 4 of 24

Raw materials required to produce glass are mixed together as a batch and continuously 

charged into a refractory bricked glass-melting furnace. The furnaces are oxygen/naturalgas fired units. Effluent combustion gases generated from each of the DM1 and DM2 

furnaces are exhausted to separate control units and discharged after they combine in a 

common stack. Test samples are collected from the individual discharges after the control 

device and before they are combined in the common stack. 

From the glass melting furnace, the molten glass flows through bushings to a rotary fiberizer 

that produces the fibers. After the fibers have been formed, they are directed towards a 

conveyor by an air stream. A binder solution is sprayed on the glass fibers as they descend 

to the forming conveyor chain. The formation of wool product (commonly called a “pack”) is 

accomplished when the binder-coated fibers are drawn onto the perforated forming 

conveyor by suction fans. The air passing through the product is treated prior to release to 

atmosphere via the mixing chamber stacks. 

After forming, the coated fiber mat or "pack" is passed through a convection oven fired by 

natural gas to promote curing. Curing gases from each line oven are treated by linespecific incinerator units. The discharge gases from each incinerator unit are combined with 

air/gases exhausted from the fiber forming process in the mixing chamber prior to release 

via the mixing chamber stacks. 

After leaving the oven, the product is cooled, trimmed, and cut to the desired length and 

width, prior to packaging. The cooling process involves pulling ambient air through the 

product after it leaves the curing oven. The effluent gases on the DM1 and DM2 lines are 

filtered prior to discharge via the cooling stacks. 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 5 of 24

3. Description of Sources and Sampling Locations 

The DM1 and DM2 melting furnaces exhaust to separate dry electrostatic precipitator units 

(DEPs). The outlet ducts from both units combine to a common stack prior to release to 

atmosphere. Emissions sampling was carried out on the vertical “downcomer” discharge of 

each DEP unit, prior to the fan and before both effluent combine into the common DEP 

Stack. 

Since a permanent platform did not exist to access the two DEP outlet sampling locations, a 

mobile “scissor lift” was used to access the sampling ports. The sources and sampling 

locations for the DM1 and DM2 Furnace DEP Outlets are described in Table 3-1. Site 

photographs and sample point markings are presented in Appendix E. 

Table 3-1: Description of Sources and Sampling Locations 

Parameter DM1 Furnace 

DEP Outlet 

DM2 Furnace 

DEP Outlet 

Emission Unit # U-00002 U-00012 

Emission Point # EP00100 EP00200 

Stack Plane Configuration Rectangle Rectangle 

Stack Diameter / Dimensions 3.28ft x 3.28ft 3.28ft x 3.28ft 

Stack Area at Sample Location 10.76 ft2 10.76 ft2

Duct Configuration Vertical  Vertical 

Accessibility for Sampling Mobile ManLift Mobile ManLift 

Number of Sampling Ports 5 5 

Upstream Distance to Ports 5.6 ft 2.7 ft 

Downstream Distance to Ports 10.6 ft 11.3 ft 

Sample Port Size 4 inches ID 4 inches ID 

Sample Port Length 6.5 inches 6.5 inches 

Total # of Sampling Points 30 30 

Sampling Matrix 5 x 6 5 x 6 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 6 of 24

4. Test Methods 

Sampling and analytical protocols are listed in Table 3-1 and are detailed in subsequent 

sections. 

Table 4-1: Summary of Sampling and Analytical Methods 

Parameter Sampling Technique Analytical Technique Laboratory 

Velocity / Flow Rate USEPA Method 2 N/A N/A 

Molecular Weight USEPA Method 3, 3A Instrumentally using 

electrochemical cell analyzer N/A 

Moisture Content Condensation as per 

USEPA Method 4 

Gravimetrically as per 

USEPA Method 4 LEHDER 

Filterable Particulate Isokinetically as per 

USEPA Method 5/29 

Gravimetrically as per 

EPA Method 5/29 Enthalpy 

Filterable/Vapours/Total 

Chromium 

Isokinetically as per 

USEPA Method 5/29 

 Samples prepared as per 

USEPA Method 29 

 Chromium from all train 

fractions analyzed by ICP/MS 

Element One 

Total & Hexavalent 

Chromium 

Isokinetically as per 

USEPA Method 0061 

 Samples prepared as per 

USEPA Method 0061 

 Hex.Chromium analyzed by IC 

 Total Chromium by ICP/MS 

Element One 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 7 of 24

4.1 Total and Hexavalent Chromium – Method 0061 

Emission rates of hexavalent chromium (Cr+6) and total chromium were determined using 

EPA Method 0061: Determination of Hexavalent Chromium Emissions from Stationary 

Sources (January 1996). The specifications for the Method 0061 sampling method are 

presented in Table 4-2 and Figure 4-2. The sampling train is depicted in Figure 4-1. 

Table 4-2: Specifications for Hexavalent Chromium (Method 0061) 

Item Specification 

Test Method

Reference: US EPA Method 0061(Ref: SW-846): Determination of 

Hexavalent Chromium Emissions from Stationary Sources

Method Modifications: Extra nitric acid rinse and filter recovery for total chromium 

analysis 

Sampling Technique: Isokinetic (Recirculation of Impinger Solution) 

Number of Test Runs: 3 (one per day) 

Sampling Parameters

Total # of Sample Points: 30 

Sample Matrix: 5 ports x 6 points/port 

Sample Time / Point (min): 7.0 to 8.0 minutes/point (3.5 to 4.0 minutes per reading) 

Total Test Time / Run (min): 240.0 and 210.0 minutes (4.0 to 3.5 hours) 

Target Sample Rate: 0.75 cfm 

Sampling Train 

Nozzle/Probe: 

One piece nozzle/probe liner constructed of glass by a 

glassblower. Size of extraction nozzle measured before use. 

Glass nozzle/probe liner used to address the high stack gas 

temperature. 

Probe Liner: 3/8 inch OD Teflon® 

Special Probe Type: Air-cooled probe to help keep recirculation solution in liquid 

form. One-piece nozzle/liner inserted into air-cooled probe. 

Filter: No Filter (probe exit connected directly to impingers) 

Recirculation System: Peristaltic pump circulating impinger solution (0.5 N KOH) 

from impinger #1 to the nozzle/probe transition. 

Impingers: 

Full sized Teflon® with 3/8 inch OD Teflon® stems and 

connectors, containing: 

 Impinger #1: 200 mLs of 0.5N KOH 

 Impinger #2: 75 mLs of 0.5 N KOH 

 Impinger #3: 75 mLs of 0.5 N KOH 

 Impinger #4: Empty 

 Impinger #5 (glass): Known quantity of silica gel 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 8 of 24

Table 4-2: Specifications for Hexavalent Chromium (Method 0061) (cont’d) 

Item Specification 

Sampling Procedures

Pre-cleaning: 

 Wash with hot tap water, then hot soapy water, then rinse three 

times with tap water. 

 Train components (up to the silica gel impinger) soaked for a 

minimum of 4 hrs in 10% (v/v) nitric acid solution. 

 Components are then rinsed three times with reagent grade 

water and air dried, then sealed. 

Train Operation: 

 Sample isokinetically at each sample point while KOH solution 

from impinger #1 is circulated to the probe and back into 

impinger #1. 

 Solution circulation required to prevent reduction of Cr+6 to Cr+3 

in the sample gas stream 

Solution pH Check: 

 Check pH of solution in first impinger after first traverse and at 

end of test run. 

 If pH less than 8.5, test run is void. 

Post Test Activities 

 Sample train post test leak check. Criterion is 0.020 cfm at the 

highest vacuum encountered during the test run. 

 Disconnect probe from train prior to nitrogen purge. 

 Purge sampling train from inlet of first impinger to exhaust of 

silica gel with UHP nitrogen at a rate of 10 Lpm for 30 minutes. 

Sample Recovery 

Location: Clean, dry and well lit area 

Recovery Procedure: 

 Impinger catch from impingers #1 - 4 volumetrically measured 

and combined into one sample bottle 

 Glass nozzle, aspirator, all connecting tubing and impingers 

rinsed with DI Water. 

 Rinses volumetrically measured and added to sample bottle. 

 All impingers and connectors rinsed with 0.1 N HNO3 into a 250 

mL bottle for total Cr analysis. 

Filtration: 

 Entire aqueous sample passed through a 0.45 μm acetate filter 

in a Teflon filtration device. 

 Filtration device washed 3 times with DI water and rinses added 

to sample. 

 Final aqueous sample volume recorded. 

 Filter recovered into a separate bottle (60 mLs amber glass) for 

total Cr analysis. Filter holder rinsed with water and HNO3 and 

recovered in same bottle. 

Sample Bottles: 

 1 L polyethylene (PE) bottle for KOH impinger solutions & rinses 

 250 mLs PE bottle for 0.1N nitric acid rinses 

 60 mLs wide-mouth amber glass bottle for acetate filter & rinses. 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 9 of 24

Table 4-2: Specifications for Hexavalent Chromium (Method 0061) (cont’d) 

Item Specification 

Analysis

Laboratory: Element One, Wilmington, NC 

Analytical Technique: 

(Hexavalent Chromium) 

 Samples were prepared and analyzed according to SW-846 

Method 0061 protocol 

 Samples were analyzed for chromium (VI) using a Shimadzu 

2010 HPLC unit and a Timberline RDR-1 Reaction Mode 

 Chromium (IV) Detection Limit: 0.1 μg/L 

Analytical Technique: 

(Total Chromium) 

 Samples were acidified with trace metals grade concentrated 

nitric acid and digested on a hotplate according to the method 

protocol. 

 The digested samples were analyzed for total chromium in a 

PerkinElmer ELAN 6100 ICP MS. 

 Total Chromium Detection limit: 1.0 μg/L 

Hold Time: 14 Days 

QA/QC: 

 1 reagent blank (300 mLs of 0.5N KOH) 

 1 reagent water blank 

 1 0.1N nitric acid blank 

 1 reagent blank (distilled water) 

 1 acetate filter blank 

 Laboratory duplicate analyses relative percent difference (RPD) 

 Laboratory spike sample recovery 

Data Reporting

Volumetric Flow Rate (Qs): 

 Actual flow rate (Acfm) is product of average measured velocity 

(ft/s) and cross-sectional area (ft2

) of stack at sampling plane. 

 Standard flow rate (Scfm) is Actual Flow rate corrected to 68 ̊F 

and 29.92 inches Hg 

 Reference flow rate on a dry basis considers dry gas fraction of 

effluent flow rate only (Water vapour mole fraction removed 

from the total) 

Pollutant Concentration 

(Cs): 

Mass collected in aqueous sample (from Laboratory) divided by 

dry standard sample volume from test run (S.ft3

 or S.m3). 

Pollutant Mass Rate (Es):  Es = Cs x Qs 

 lb/hr = mg/S.ft3

 x scfm x 60 min/hr / 454,000 mg/lb 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 10 of 24

Figure 4-1: Schematic of EPA Method 0061 Sampling Train 

Control Unit 

 Calibrated DGM 

 Rotary Vane Vacuum Pump 

 Orifice Meter 

 Temperature monitoring 

circuitry 

 Effluent velocity pressure 

manometer 

Peristaltic Pump 

(circulates KOH solution from 

Impinger #1, into the probe just 

before probe/nozzle union ) Teflon® Impingers and Connectors

 Impinger #1 has recirculation adaptor on the bottom 

 Impinger #1 contains 150 mL of 0.5N KOH 

 Impingers #2 & #3 contain 75 mL of 0.5N KOH each 

Measured Glass Nozzle 

fused to Glass Liner 

Custom made 5/8 inch OD 

Glass Liner with fused nozzle 

(with 1⁄4 inch OD Teflon® 

recirculation tube inside) 

1⁄4 inch OD Teflon® 

recirculation line Ice Bath 

Impinger Outlet Temperature 

Silica Gel 

(glass impinger) 

Air-cooled probe 

Umbilical 

Line 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 11 of 24

Nozzle/Probe Assembly Impingers

After test run, disconnect 

probe/nozzle assembly from 

impingers and rinse 

probe/nozzle assembly with 

100 mLs of with reagent 

grade water into 1 Liter PE 

bottle (Container #1)

Rinse entire impinger train and connectors with 0.1N 

Nitric Acid and recover into 250 mLs poly bottle 

(Container #2) for total Cr analysis. 

After test run, check 

pH of the first impinger

Attach nitrogen purge to input 

of sampling train. Purge 

system for 30 min at 10 LPM 

Disconnect impingers. Volumetrically measure and 

transfer aqueous solution from impingers 1, 2 & 3 into 1 

Liter PE sample bottle (Container #1). Rinse impingers 

and associated connector pieces 4 times with reagent 

grade water and collect into Container #1. 

Samples to Enthalpy/Element One 

Is pH > 8.5?

YES 

No 

Discard solution 

and redo test run

Transfer entire aqueous volume from Container #1 into 

Teflon filtration unit and filter through a 0.45 μm acetate 

filter. Recover filtrate back into Container #1. Rinse 

container and filtration unit and combine into same bottle 

(Container #1). Record final aqueous sample volume. 

Recover acetate filter into a 60 mLs wide-mouth amber 

glass bottle (Container #3) for total Cr analysis.

Figure 4-2: Sample Recovery Flow Chart – Method 0061 Test Runs 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 12 of 24

4.2 Filterable Particulate and Total Chromium - EPA Method 29 

Emission rates of filterable particulate, filterable chromium and vaporous chromium were 

determined using EPA Method 29: Determination of Metal Emissions from Stationary 

Sources. The specifications for the Method 29 sampling method are presented in Table 4-3 

and Figure 4-3. The sampling train is depicted in Figure 4-4. 

Table 4-3: Specifications for PM/Metals Sampling (EPA Method 29) 

Item Specification 

Test Method 

Reference: EPA Method 29 Determination of Metal Emissions 

from Stationary Sources. 

Method Modifications: None 

Sampling Technique: Isokinetic at multiple points as per EPA Method 1 

Number of Test Runs/Source: 3 (simultaneous with M0061 Test Runs) 

Sampling Parameters

Total # of Sample Points: 12 

Sample Matrix: 2 ports x 6 points/port 

Sample Time / Point (min): 45.0 minutes/point (5.0 minutes per reading) 

Total Test Time / Run (min): 240.0 minutes (4.0 hours) 

Target Sample Rate: 0.75 cfm 

Sampling Train

Nozzle: Glass (size measured) 

Probe liner: Seamless glass heated to 120 ̊C ± 14 ̊C 

Filter: Pre-tared quartz fiber heated to 120 ̊C ± 14 ̊C 

Glass connectors: Ball/socket with O-rings 

Back-half: Full sized impingers chilled in ice bath 

 Imp. #1: 100 mLs 5% nitric/10% H2O2 Sol’n 

 Imp. #2: 100 mLs 5% nitric/10% H2O2 Sol’n 

 Imp. #3: Empty 

 Imp. #4: Known quantity of silica gel 

Sample Recovery 

Location: Clean, dry and well lit area. 

Front-half Recovery Solvents:  Front-half wash for PM/Metals: Acetone 

 Front-half wash for Metals: 0.1N Nitric Acid 

Back-Half Recovery Solvents:  Rinse for Imp. #1, #2 and 3: 0.1N Nitric Acid 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 13 of 24

Table 4-3: Specifications for PM/Metals Sampling (EPA Method 29) (cont’d) 

Item Specification 

Laboratory

Particulate: Enthalpy Analytical – Durham, NC 

Chromium: Element One - Wilmington, NC 

Analysis

Particulate: Gravimetric as per Method 5 (MDL=0.1mg) 

Filterable Chromium: 

(Front-Half) 

 Sample preparation of front-half samples as per 

USEPA Method 29 

 After digestion of filter & probe rinse residue, 

samples analyzed for total chromium on a 

PerkinElmer ELAN 6100 ICP-MS. 

 Chromium Detection limit = 1.0 ug/L 

Vaporous Chromium: 

(Back-Half) 

 Sample preparation of back-half fraction as per 

USEPA Method 29 

 Samples analyzed for total chromium on a 

PerkinElmer ELAN 6100 ICP-MS. 

 Chromium Detection limit = 1.0 ug/L 

QA/QC  0.1N nitric acid reagent blank 

 5% HNO3/10% H2O2 reagent blank 

 Acetone reagent blank 

 Quartz fiber filter 

 Duplicate analyses relative % difference (RPD) 

 Spike sample recovery 

 Second source calibration verification 

Data Reporting

Volumetric Flow Rate (Qs): 

 Actual flow rate (Acfm) is product of average 

measured velocity (ft/s) and cross-sectional area 

(ft2

) of stack at sampling plane. 

 Standard flow rate (Scfm) is Actual Flow rate 

corrected to 68 ̊F and 29.92 inches Hg 

 Reference flow rate on a dry basis considers dry 

gas fraction of effluent flow rate only (Water 

vapour mole fraction removed from the total) 

Pollutant Concentration (Cs): 

Mass collected in aqueous sample (from 

Laboratory) divided by dry standard sample volume 

from test run (S.ft3

 or S.m3). 

Pollutant Mass Rate (Es):  Es = Cs x Qs 

 lb/hr = mg/S.ft3

 x scfm x 60 min/hr / 454,000 mg/lb 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 14 of 24

Figure 4-3: Sample Recovery – Method 29 Test Runs 

Quartz Fiber 

Filter

Impinger Solutions and 

Associated Rinses

Nozzle/Probe & Glassware 

upstream of Quartz Filter

Clean thoroughly using 

acetone and Teflon brush. 

Recover into labeled 250 

mLs glass bottle. 

Recover quartz filter 

into labeled petri dish.

Rinse with 0.1N 

nitric acid and 

recover in labeled 

250 mLs poly bottle. 

Rinse with water 

and acetone and 

discard solutions. 

Evaporate acetone to dryness 

in clean tared container. 

Weigh residue to constant 

weight (± 0.5 mg). 

MDL = 0.1 mg 

Deliver Samples to Enthalpy for PM Analysis 

Condition filters then 

weigh to constant 

weight (± 0.5 mg). 

MDL = 0.1 mg 

Rinse back of filter bell, 

impingers #1, #2 & #3 and 

connecting glassware 3 times 

with 0.1N HNO3 into labeled 

500 mLs poly bottle. 

Digestion of sample fractions and subsequent analysis of designated chromium as per EPA Method 29 

 (Chromium analysis and reporting based on separate front-half and back-half fractions) 

Deliver samples to Enthalpy 

for Chromium Analysis
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 15 of 24

Figure 4-4: Schematic of EPA Method 29 Sampling Train 

 

Temperature Sensors

Dry Gas

Meter 

Manometer 

Orifice 

Temperature Sensors

Air Tight 

Pump 

Main 

Valve 

By-Pass Valve

Vacuum 

Gauge 

Silica

100 mLs each of Gel

5% HNO3/10% H2O2

Heated Glass 

Probe Impingers 

Ice 

Bath

S Type Pitot 

Manometer 

Heated 

Filter 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 16 of 24

5. Test Results 

Test results are presented in Tables 5-1 to 5-4. Detailed sampling data and effluent 

measurements are provided in the appendices. 

Table 5-1: Summary of Method 0061 Test Results – DM1 Furnace DEP Outlet 

Run #1 Run #2 Run #3 

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average 

08:27-12:55 08:03-11:49 07:52-11:22 

Hexavalent Chromium

Concentration μg/S.m3 2.9 2.9 2.1 2.7 

Mass Rate lb./hr 8.8E-05 9.6E-05 6.7E-05 8.4E-05 

Total Chromium 

Concentration μg/S.m3 4.1 5.1 5.4 4.9 

Mass Rate lb./hr 1.3E-04 1.7E-04 1.7E-04 1.5E-04 

Effluent Characteristics 

Avg. Stack Temperature  ̊F 445 425 437 436 

Stack Gas Pressure in Hg 29.32 29.70 29.65 29.56 

Avg. Stack Gas Velocity ft/min 1.49E+03 1.52E+03 1.50E+03 1.50E+03 

O2 Concentration % vol 19.6 20.0 19.9 19.8 

CO2 Concentration % vol 4.9 4.7 4.8 4.8 

Effluent Mol. Weight (dry) lb/mol 29.6 29.5 29.6 29.6 

Effluent Mol. Weight (wet) lb/mol 28.3 28.4 28.3 28.3 

Effluent Moisture Content % vol. 11.2 10.1 11.1 10.8 

Dry Gas Fraction % vol. 88.8 89.9 88.9 89.2 

Actual Effluent Flow Rate Acfm 1.60E+04 1.63E+04 1.62E+04 1.62E+04 

Standard Flow Rate (wet) Scfm 9.14E+03 9.66E+03 9.43E+03 9.41E+03 

Standard Flow Rate (dry) Scfm 8.12E+03 8.69E+03 8.38E+03 8.40E+03 

Sample Parameters 

Sample Period min 240.0 210.0 210.0 220.0 

Sample Period Hours 4.0 3.5 3.5 3.7 

Hexavalent Chromium μg 10.8 10.1 7.2 9.3 

Total Chromium μg 15.4 17.4 18.2 17.0 

Dry Standard Sample Volume Scf 131.27 120.81 118.57 123.55 

Average Delta P in H2O 0.13 0.14 0.13 0.13 

Average Delta H in H2O 1.01 1.09 1.04 1.05 

Average Sample Rate cfm 0.55 0.57 0.56 0.56 

Average Isokinetic Variation % 99.9 98.1 99.6 99.2 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 17 of 24

Table 5-2: Summary of Method 0061 Test Results – DM2 Furnace DEP Outlet 

Run #1 Run #2 Run #3 

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average 

08:27-12:55 08:03-11:49 07:52-11:22 

Hexavalent Chromium

Concentration μg/S.m3 37 40 29 36 

Mass Rate lb./hr 1.2E-03 1.3E-03 9.3E-04 1.1E-03 

Total Chromium 

Concentration μg/S.m3 42 47 35 41 

Mass Rate lb./hr 1.4E-03 1.5E-03 1.1E-03 1.3E-03 

Effluent Characteristics 

Avg. Stack Temperature  ̊F 414 414 420 416 

Stack Gas Pressure in Hg 29.58 29.98 29.91 29.82 

Avg. Stack Gas Velocity ft/min 1.51E+03 1.43E+03 1.47E+03 1.47E+03 

O2 Concentration % vol 20.0 20.1 20.0 20.0 

CO2 Concentration % vol 4.21 4.70 4.40 4.44 

Effluent Mol. Weight (dry) lb/mol 29.5 29.6 29.5 29.5 

Effluent Mol. Weight (wet) lb/mol 28.3 28.4 28.3 28.3 

Effluent Moisture Content % vol. 10.2 10.0 10.4 10.2 

Dry Gas Fraction % vol. 89.8 90.0 89.6 89.8 

Actual Effluent Flow Rate Acfm 1.62E+04 1.54E+04 1.58E+04 1.58E+04 

Standard Flow Rate (wet) Scfm 9.67E+03 9.32E+03 9.45E+03 9.48E+03 

Standard Flow Rate (dry) Scfm 8.68E+03 8.39E+03 8.47E+03 8.52E+03 

Sample Parameters 

Sample Period min 240.0 210.0 210.0 220.0 

Sample Period Hours 4.0 3.5 3.5 3.7 

Hexavalent Chromium μg 143 131 95.3 123 

Total Chromium μg 161 152 113 142 

Dry Standard Sample Volume Scf 135.95 114.49 115.21 121.88 

Average Delta P in H2O 0.14 0.13 0.13 0.13 

Average Delta H in H2O 1.18 1.08 1.11 1.12 

Average Sample Rate cfm 0.57 0.54 0.54 0.55 

Average Isokinetic Variation % 99.7 99.4 99.0 99.4 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 18 of 24

Table 5-3: Summary of Method 29 Test Results – DM1 Furnace DEP Outlet 

Run #1 Run #2 Run #3 

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average 

13:45-17:45 12:25-16:25 12:12-16:12 

Filterable Particulate

Concentration mg/S.m3 1.5 1.7 1.3 1.5 

Mass Rate lb./hr 0.045 0.052 0.039 0.045 

Filterable Chromium 

Concentration μg/S.m3 5.1 4.5 4.8 4.8 

Mass Rate lb./hr 1.5E-04 1.4E-04 1.4E-04 1.4E-04 

Condensable Chromium 

Concentration μg/S.m3 0.15 0.15 0.10 0.14 

Mass Rate lb./hr 4.7E-06 4.7E-06 3.1E-06 4.1E-06 

Total Chromium 

Concentration μg/S.m3 5.2 4.7 4.9 4.9 

Mass Rate lb./hr 1.6E-04 1.4E-04 1.5E-04 1.5E-04 

Effluent Characteristics 

Avg. Stack Temperature  ̊F 439 433 446 439 

Stack Gas Pressure in Hg 29.35 29.71 29.60 29.56 

Avg. Stack Gas Velocity ft/min 1.45E+03 1.44E+03 1.45E+03 1.45E+03 

O2 Concentration % vol. 19.7 19.9 19.9 19.8 

CO2 Concentration % vol. 4.5 4.9 4.8 4.73 

Effluent Mol. Weight (dry) lb/mol 29.5 29.6 29.6 29.6 

Effluent Mol. Weight (wet) lb/mol 28.3 28.4 28.3 28.3 

Effluent Moisture Content % vol. 10.6 10.5 10.9 10.6 

Dry Gas Fraction % vol. 89.4 89.5 89.1 89.4 

Actual Effluent Flow Rate Acfm 1.56E+04 1.55E+04 1.56E+04 1.56E+04 

Standard Flow Rate (wet) Scfm 9.00E+03 9.11E+03 8.97E+03 9.03E+03 

Standard Flow Rate (dry) Scfm 8.048E+03 8.16E+03 8.00E+03 8.07E+03 

Sample Parameters 

Sample Period min 240.0 240.0 240.0 240.0 

Sample Period Hours 4.0 4.0 4.0 4.0 

Filterable PM (Acetone) mg 2.7 3.1 3.1 3.0 

Filterable PM (Filter) mg 3.5 4.0 2.3 3.3 

Filterable Chromium μg 21.2 19.0 19.8 20.0 

Condensable Chromium μg 0.6 0.6 0.4 0.6 

Dry Standard Sample Volume Scf 147.17 148.44 146.74 147.45 

Average Delta P In H2O 0.11 0.11 0.11 0.11 

Average Delta H in H2O 1.28 1.26 1.22 1.25 

Average Sample Rate cfm 0.62 0.61 0.59 0.61 

Average Isokinetic Variation % 99.1 98.6 99.5 99.0 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 19 of 24

Table 5-4: Summary of Method 29 Test Results – DM2 Furnace DEP Outlet 

Run #1 Run #2 Run #3 

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average 

13:45-18:00 12:25-16:25 12:12-16:12 

Filterable Particulate

Concentration mg/S.m3 8.8 7.6 7.2 7.9 

Mass Rate lb./hr 0.27 0.24 0.22 0.25 

Filterable Chromium 

Concentration μg/S.m3 46 41 35 41 

Mass Rate lb./hr 1.4E-03 1.3E-03 1.1E-03 1.3E-03 

Condensable Chromium 

Concentration μg/S.m3 0.18 0.21 0.26 0.22 

Mass Rate lb./hr 5.6E-06 6.7E-06 8.1E-06 6.8E-06 

Total Chromium 

Concentration μg/S.m3 46 41 35 41 

Mass Rate lb./hr 1.4E-03 1.3E-03 1.1E-03 1.3E-03 

Effluent Characteristics 

Avg. Stack Temperature  ̊F 426 421 437 428 

Stack Gas Pressure in Hg 29.62 29.97 29.85 29.81 

Avg. Stack Gas Velocity ft/min 1.46E+03 1.45E+03 1.47E+03 1.46E+03 

O2 Concentration % vol. 20.0 20.2 20.1 20.1 

CO2 Concentration % vol. 4.4 4.6 4.5 4.49 

Effluent Mol. Weight (dry) lb/mol 29.5 29.5 29.5 29.5 

Effluent Mol. Weight (wet) lb/mol 28.3 28.4 28.3 28.3 

Effluent Moisture Content % vol. 10.2 9.93 10.5 10.2 

Dry Gas Fraction % vol. 89.8 90.1 89.5 89.8 

Actual Effluent Flow Rate Acfm 1.57E+04 1.56E+04 1.58E+04 1.57E+04 

Standard Flow Rate (wet) Scfm 9.28E+03 9.39E+03 9.28E+03 9.32E+03 

Standard Flow Rate (dry) Scfm 8.33E+03 8.46E+03 8.30E+03 8.36E+03 

Sample Parameters 

Sample Period min 240.0 240.0 240.0 240.0 

Sample Period Hours 4.0 4.0 4.0 4.0 

Filterable PM (Acetone) mg 1.1 2.7 3.5 2.4 

Filterable PM (Filter) mg 35.3 30.8 27.7 31.3 

Filterable Chromium μg 191.0 180.0 151.0 174.0 

Condensable Chromium μg 0.8 0.9 1.1 0.9 

Dry Standard Sample Volume Scf 146.84 154.98 153.25 151.69 

Average Delta P In H2O 0.11 0.12 0.12 0.11 

Average Delta H in H2O 1.40 1.53 1.45 1.46 

Average Sample Rate cfm 0.61 0.63 0.62 0.62 

Average Isokinetic Variation % 99.3 98.7 99.5 99.1 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 20 of 24

6. Discussion of Results 

6.1 General 

 Reported emission data are believed to be representative of the stack conditions at the 

time of testing. The sampling program was not witnessed by the New York State DEC. 

 Sample recoveries were carried out in a clean, temperature controlled room to maximize 

efficiency and prevent contamination. Train preparation and sample recovery were 

conducted by a single sample recovery specialist to maintain the highest level of 

consistency. 

 There was good communication between the LEHDER field crew and Owens Corning 

during the sampling campaign. Mr. Rick Cooper of the Owens Corning corporate 

environmental department was the liaison between the process and the LEHDER field 

crew. Pertinent process/production data were collected throughout the sampling campaign 

by Owens Corning personnel. Sampling was initiated only when process conditions and 

production rates were reported to be at required levels. 

 An assessment of cyclonic flow was carried out on Tuesday, January 23, 2012. The 

assessment found that both sources were within the EPA Method 1 criteria of 20% 

cyclonic flow or less. 

 The test runs for both methods were initially set for 240 minutes. After the first test, the 

final pH of the KOH solution in the first impinger was at 8.5. A pH below 8.5 deems the 

test run invalid. To reduce the chance of an invalid test, the sample duration for Runs #2 

and #3 were cut to 210 minutes. All subsequent test runs reported final solution pH 

values above 8.5. Factors contributing to the declining pH of the test period are: higher 

effluent moisture content that dilutes the contents of the first impinger and elevated CO2 

concentrations. The CO2 concentrations measured from the DM1 and DM2 Furnace DEP 

Outlets ranged from 4.5% to 4.9%. 

6.2 Particulate Emission Summary 

Particulate data was obtained from the front-half of the Method 29 train. Front-half sample 

fractions were recovered, analyzed and reported in accordance with the procedures 

described in USEP Method 5. A summary of the particulate concentrations and mass rates 

is presented in Table 6-1. 

Table 6-1: Average Particulate Test Results – DM1 & DM2 Furnace DEP Outlets 

Source Concentration 

mg/S.m3

Mass Rate 

lb/hr 

DM1 Furnace DEP Outlet 1.5 0.045 

DM2 Furnace DEP Outlet 7.9 0.25 

Total from Common DEP Stack 0.30 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 21 of 24

6.3 Total Chromium - Method 29 vs. Method 0061 

 Total chromium concentrations and mass rates were measured from the DM1 and DM2 

Furnace DEP Outlets using two test methods: USEPA Method 29 and 0061. Sampling 

was not conducted simultaneously, however, one of each test types were completed each 

day for each of the two sites. A comparison of the two sets of data is presented in Table 

6-2. The total chromium data show are very good correlation between the two test 

methods for low and higher chromium concentrations. 

Table 6-2: Total Chromium Data – Method 29 vs. Method 0061 

Total Chromium 

Concentration Mass Rate 

M29 M0061 Difference M29 M0061 Difference

Stack Run 

# 

ug/S.m3 ug/S.m3 % lb/hr lb/hr % 

1 5.2 4.1 -21% 1.6E-04 1.3E-04 -19% 

2 4.7 5.1 9% 1.4E-04 1.7E-04 21% 

3 4.9 5.4 10% 1.5E-04 1.7E-04 13% 

DM1 Furnace 

DEP Outlet 

Avg. 4.9 4.9 0% 1.5E-04 1.5E-04 0% 

1 46 42 -9% 1.4E-03 1.4E-03 0% 

2 41 47 15% 1.3E-03 1.5E-03 15% 

3 35 35 0% 1.1E-03 1.1E-03 0% 

DM2 Furnace 

DEP Outlet 

Avg. 41 41 0% 1.3E-03 1.3E-03 0% 

% Difference from M29 value = {(M0061 value – M29 value) / M29 value} x 100% 

% Difference = “0” when M0061 value = M29 value 

6.4 Method 0061 Hexavalent and Total Chromium Data 

 Method 0061 is typically used for the determination of hexavalent chromium emissions 

only. However, the Section 114 request requires that both hexavalent and total chromium 

be analyzed for all test runs. To determine total chromium from the train, an extra 

recovery step is required in the field. This involves rinsing the train components with 0.1N 

nitric acid and recovering the acetate filter used during post-test processing. The acid 

rinse is collected along with the filter and submitted for total chromium analysis only. The 

recovered KOH solution is also analyzed for total chromium. 

 Hexavalent and total chromium are analyzed using two different analytical techniques. 

The hexavalent chromium analytical method is approximately 10 times more sensitive 

than the total chromium technique. If hexavalent chromium represents a high fraction of 

the total chromium, the difference in analytical sensitivity could result in hexavalent 

chromium appearing to be greater than 100% of the total. 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 22 of 24

 The impinger solution used for this campaign was 0.5N KOH which is the strongest 

normality identified for use in Method 0061. The stronger normality was used to ensure 

that the final pH of the impinger solution was above the required 8.5. The consequences 

of the stronger KOH solution are: higher chromium levels in the blank, and a higher 

potential for interferences that could affect the total chromium analysis. For this reason, 

there is a level of uncertainty attached to total chromium data when a higher normality 

KOH solution is used. The laboratory has indicated a higher level of confidence with 

hexavalent chromium analysis even with the stronger KOH solution. 

 As indicated in Section 6.1 above, provisions were taken to ensure the post-test pH of the 

KOH solution met the criterion of greater than 8.5. First, it was decided to increase the 

initial volume of 0.5N KOH in the first impinger from 300 mLs to 350 mLs. This 

modification was also beneficial for maintaining an appropriate aqueous volume in the first 

impinger for recirculation of the KOH solution in the probe. This has purportedly been an 

issue when using Method 0061 to sample hot stacks. In addition, the sampling period 

was reduced from 240 minutes to 210 minutes for Test Runs #2 and #3 at both sites. 

 To address the relative high effluent gas temperatures (i.e. ~425 ̊ F), a glass probe liner 

was used instead of Teflon® one. The glass probe liners were modified by fusing an 

appropriately sized glass extraction nozzle on the end of the liner. The size of the nozzle 

was selected based on preliminary effluent measurements made from both sites prior to 

the start of the sampling campaign. The probe/impinger transition was also glass. All 

other parts between the transition and the silica gel were constructed of Teflon®. 

 A summary of the Method 0061 data from the DM1 and DM2 Furnace DEP Oultets is 

presented in Table 6-3. Both the total and hexavalent chromium data were blank 

corrected. Based on the data, the fraction of total chromium that is hexavalent appears to 

vary significantly at lower chromium concentrations (DM1 test runs). The ratio is more 

consistent for the higher chromium concentrations (DM2 test runs). This variability may 

be due to difference in sensitivity between the chromium and hexavalent chromium 

analytical methods, and the uncertainty factors associated with measuring very low instack chromium concentrations. 

Table 6-3: Method 0061 – Hexavalent Chromium vs. Total Chromium 

Method 0061 

Concentration, μg/S.m3 Stack Mass Rate, lb/hr Run 

# 

Date 

2012 

Hex. Cr Total Cr Hex. Cr Total Cr 

% Hex Cr. 

Of Total Cr

1 24-Jan 2.9 4.1 8.8E-05 1.3E-04 70% 

2 25-Jan 2.9 5.1 9.6E-05 1.7E-04 58% 

3 26-Jan 2.1 5.4 6.7E-05 1.7E-04 39% 

DM1 Furnace 

DEP Outlet 

Avg. 2.7 4.9 8.4E-05 1.5E-04 54% 

1 24-Jan 37.2 41.8 1.2E-03 1.4E-03 89% 

2 25-Jan 40.5 46.9 1.3E-03 1.5E-03 86% 

3 26-Jan 29.2 34.7 9.3E-04 1.1E-03 84% 

DM2 Furnace 

DEP Outlet 

Avg. 35.6 41.1 1.1E-03 1.3E-03 87% 

% Hex. Chromium = (Hex. Chromium Value / Total Chromium Value) x 100% 
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 23 of 24

6.5 QA/QC 

 All Teflon train parts employed for sampling were cleaned with soap and water, rinsed 

three times with distilled water and acid soaked overnight. After cleaning all parts were 

sealed prior to use. This cleaning process ensured that the train components were free of 

contamination before they were used for this project. 

 Based on the analytical reports provided by the laboratories, Method 0061 field blanks of 

the 0.5N KOH showed relatively high blank levels of total and hexavalent chromium 

compared to the stack samples. The hexavalent chromium measured in the KOH reagent 

blank was 1.72 ug (based on 350 mLs aqueous volume). Total chromium measured in 

the 0.5 KOH blank was 3.14 μg (based on 350 mLs aqueous volume). Since the aqueous 

volume of the blank was the same as the starting volume of 0.5N KOH in the train, the 

blank volume was simply subtracted from the uncorrected chromium analysis. 

 Analysis of duplicates and laboratory spikes were within applicable requirements. The 

laboratory analytical reports are furnished in Appendix B. 

 As discussed above, the sample period for the Method 0061 test runs was reduced from 

240 minutes to 210 minutes for Runs #2 and #3. The reason for this change was to 

prevent an invalid test caused by a post-test pH less than 8.5 in the first impinger. The 

reduction in sample period resulted in final gas volumes that were less than the minimum 

threshold of 120 dscf (See Table 5-1 and 5-2). The reduced sample volumes did not 

appear to affect the representative quality of the data as all test runs reported chromium 

and hexavalent chromium that were well above detection limits. 

 The temperature of the effluent gases was measured to be approximately 425 ̊F. This is 

near or exceeds the physical integrity of Teflon®. To address this, a glass probe liner was 

selected in lieu of a Teflon one for the Method 0061 train. This modification was 

communicated to Mr. Stef Johnson of the USEPA prior to the start of the sampling 

program. 

 For the Method 0061 train, an air-cooled probe unit was used to maintain a probe 

temperature that would not vaporize the recirculated KOH solution. The air blower moved 

air through the probe at a rate greater than 5 cfm. No problems were encountered in the 

use of this equipment or with maintaining the KOH in liquid form through the entire 

sampling period. 

 The moisture content of the effluent gas stream was determined for each test in 

accordance with the procedures described in EPA Method 4. The moisture content for 

each stack was less than 100% saturation. 

 Sample line leak checks were conducted before and after each test. Sampling did not 

proceed until the integrity of the sampling train was validated. All final leak checks were 

well within the criterion of 0.020 cfm at the highest vacuum recorded during the test run. 

Pitot tube leak checks were conducted before each isokinetic test run. 

 The isokinetic sampling rate was calculated for each point and routinely checked. 

Consequently, all reported average and point by point isokinetic variations are within the 

specification of 100%  10%.
Section 114 ICR Test Report February 25, 2012 

Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets 

Project No. 123987 Page 24 of 24

 Pitot tube, dry gas meter and thermocouple calibrations are furnished in 

Appendix C. Pitot tubes were calibrated in a wind tunnel at LEHDER’s office in Point 

Edward, Ontario. Calibrations were made with various nozzle sizes attached. The Cp 

factor for the specific nozzle size was employed for each test. Pre and post calibrations of 

the dry gas meters were calibrated with critical orifices. 

7. Closure 

The data presented in this report are believed accurate and representative of the effluent 

conditions at the time of testing and the result of best efforts in the field. Comments 

pertaining to the data or to anomalies in the data are made without bias and are based on 

experience and technical judgment. 

Respectfully submitted, 

LEHDER Environmental Services Limited 

Michael Denomme Peter Pakalnis, QSTI 

Project Manager Principal 

 

 
Appendix A 

Concentration and Mass Rate Calculations 

A.1: Method 29 Test Runs 

A.2: Method 0061 Test Runs 
Appendix A.1 

Method 29 Test Runs 
123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xls

LEHDER Environmental Services Ltd Revised by: M.Denomme

Date: 16-Feb-12

Company: Owens Corning 

Plant: Delmar, NY

Stack: DM1 DEP Outlet

Pollutant: TSP / Chromium

Method: EPA Method 29

Project No.: 123987

Operators RS / JH / JT

Data Entry: KH / JE

Reviewed By: MD

Ref.Temperature: 68 deg. F

Ref. Pressure: 29.92 "Hg

Molar Volume: 24.04 l/mol

Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

13:45 - 17:45 12:25 - 16:25 12:12 - 16:12

No. of Sample Points 30 30 30

Sample Time /Point min 8.0 8.0 8.0

Reading / Point min 4.0 4.0 4.0

Total Sample Time, min 240.0 240.0 240.0

Barometric Pressure, Pb "Hg 29.69 30.04 29.91

Stack Gauge Pressure, Pgauge "H2O -4.56 -4.46 -4.23

Absolute Stack Pressure, Ps "Hg 29.35 29.71 29.60

Pitot Tube Coefficient, Cp 0.813 0.813 0.813

Oxygen Content, O2 % 19.7 19.9 19.9

Carbon Dioxide Content, CO2 % 4.5 4.9 4.8

Carbon Monoxide Content, CO % 0.0 0.0 0.0

Nitrogen Content, N2 % 75.8 75.2 75.3

Condensate Collected, WH2O g 368.2 369.1 379.6

Nozzle Diameter, Dn in 0.3897 0.3897 0.3897

Initial DGM Reading ft3 72.384 36.877 98.140

Final DGM Reading ft3 218.375 181.214 239.000

DGM Unity, Y 1.0123 1.0123 1.0123

Stack Width ft 3.280 3.280 3.280

Stack Depth ft 3.280 3.280 3.280

Actual Volume of Dry Gas ft3 147.7867 146.1123 142.5926

Stack Area, As ft2 10.758 10.758 10.758

Particulate/Chromium Analysis

Front-Half Acetone Residue mg 2.7 3.1 3.1

Filter Loading mg 3.5 4.0 2.3

Total Suspended PM mg 6.2 7.1 5.4

Front-Half (Filterable) Chromium μg 21.2 19.0 19.8

Condensable (Back-Half) Chromium μg 0.64 0.64 0.43

Total Chromium μg 21.8 19.6 20.2

Input1
123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xls

LEHDER Environmental Services Ltd

Point by Point Sampling DataCompany: Owens Corning Plant: Delmar, NYStack: DM1 DEP OutletPollutant: TSP / ChromiumProject No.: 123987

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

13:45 - 17:45 12:25 - 16:25 12:12 - 16:12

Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi 

# min ft3 H2O H2O F F F # min ft3 H2O H2O F F F # min ft3 H2O H2O FF

P1-1 0.0 72.38 0.13 1.47 452 66 66 P1-1 0.0 36.88 0.15 1.65 434 61 64 P1-1 0.0 98.14 0.14 1.50 456 52 

4.0 74.81 0.15 1.70 452 66 66 4.0 39.40 0.16 1.80 437 61 63 4.0 100.67 0.14 1.50 456 52 

2 8.0 77.58 0.13 1.50 451 67 67 2 8.0 42.23 0.13 1.45 435 61 63 2 8.0 103.27 0.12 1.30 456 52 

12.0 80.19 0.12 1.35 448 67 67 12.0 44.80 0.13 1.45 435 62 63 12.0 105.72 0.12 1.30 454 52 

3 16.0 82.75 0.11 1.25 447 67 67 3 16.0 47.39 0.13 1.44 435 62 63 3 16.0 108.10 0.12 1.30 450 53 

20.0 85.14 0.11 1.25 446 67 67 20.0 50.00 0.13 1.44 436 62 63 20.0 110.50 0.12 1.30 451 51 

4 24.0 87.60 0.11 1.25 446 68 67 4 24.0 52.58 0.12 1.35 434 62 64 4 24.0 112.92 0.11 1.20 450 53 

28.0 90.02 0.12 1.35 447 68 68 28.0 55.06 0.12 1.35 435 62 64 28.0 115.38 0.11 1.20 451 54 

5 32.0 92.51 0.12 1.35 448 68 68 5 32.0 57.56 0.12 1.35 436 62 64 5 32.0 117.71 0.12 1.30 450 54 

36.0 94.99 0.12 1.35 449 68 68 36.0 60.07 0.12 1.33 436 61 64 36.0 120.11 0.12 1.30 454 54 

6 40.0 97.51 0.12 1.35 443 68 68 6 40.0 62.58 0.11 1.25 430 61 64 6 40.0 122.55 0.11 1.20 454 54 

44.0 100.03 0.12 1.35 443 68 68 44.0 64.97 0.13 1.45 438 61 64 44.0 124.84 0.12 1.30 454 55 

P2-1 48.0 102.50 0.14 1.60 447 68 68 P2-1 48.0 67.44 0.13 1.45 435 62 64 P2-1 48.0 127.23 0.13 1.40 454 55 

52.0 105.04 0.14 1.60 448 68 69 52.0 69.92 0.14 1.55 435 62 64 52.0 129.72 0.14 1.50 452 55 

2 56.0 107.77 0.10 1.15 445 68 69 2 56.0 72.50 0.10 1.10 435 62 64 2 56.0 132.28 0.11 1.20 450 55 

60.0 110.14 0.10 1.15 444 68 69 60.0 74.79 0.11 1.20 433 62 64 60.0 134.75 0.11 1.20 450 55 

3 64.0 112.47 0.09 1.00 441 68 69 3 64.0 77.16 0.10 1.10 432 62 64 3 64.0 137.15 0.10 1.10 450 55 

68.0 114.64 0.09 1.00 440 68 69 68.0 79.43 0.10 1.10 431 62 64 68.0 139.44 0.10 1.10 448 55 

4 72.0 116.84 0.10 1.15 440 68 69 4 72.0 81.78 0.11 1.20 431 62 64 4 72.0 141.65 0.11 1.20 447 56 

76.0 119.15 0.10 1.15 441 68 69 76.0 84.17 0.11 1.20 432 62 64 76.0 144.01 0.11 1.20 446 56 

5 80.0 121.47 0.12 1.35 444 68 69 5 80.0 86.54 0.12 1.30 434 62 64 5 80.0 146.32 0.12 1.30 449 56 

84.0 124.00 0.12 1.35 444 68 69 84.0 89.00 0.12 1.30 436 62 64 84.0 148.78 0.12 1.30 450 56 

6 88.0 126.51 0.10 1.15 444 68 69 6 88.0 91.51 0.13 1.50 437 63 64 6 88.0 151.19 0.12 1.30 452 56 

92.0 128.86 0.09 1.00 445 68 69 92.0 94.04 0.10 1.10 437 63 64 92.0 153.70 0.12 1.30 452 56 

P3-1 96.0 131.14 0.11 1.25 445 68 69 P3-1 96.0 96.34 0.12 1.35 435 62 64 P3-1 96.0 156.10 0.12 1.30 450 56 

100.0 133.38 0.12 1.35 442 66 68 100.0 98.65 0.12 1.35 435 62 64 100.0 158.53 0.12 1.30 449 56 

2 104.0 135.88 0.10 1.15 438 66 68 2 104.0 101.10 0.10 1.10 432 62 64 2 104.0 160.94 0.10 1.10 449 56 

108.0 138.28 0.09 1.00 438 67 68 108.0 103.48 0.10 1.10 432 62 64 108.0 163.25 0.10 1.10 445 56 

3 112.0 140.52 0.09 1.05 433 67 68 3 112.0 105.76 0.10 1.10 432 61 64 3 112.0 165.48 0.09 1.00 445 56 

116.0 142.67 0.09 1.05 434 67 68 116.0 108.03 0.10 1.10 428 61 64 116.0 167.59 0.09 1.00 441 55 

4 120.0 144.89 0.09 1.05 435 67 68 4 120.0 110.30 0.10 1.10 428 61 64 4 120.0 169.74 0.09 1.00 442 55 

124.0 147.12 0.09 1.05 435 67 68 124.0 112.60 0.10 1.10 428 62 64 124.0 171.90 0.09 1.00 442 55 

5 128.0 149.32 0.10 1.15 439 67 68 5 128.0 114.89 0.11 1.25 428 62 64 5 128.0 174.01 0.09 1.00 444 54 

132.0 151.61 0.10 1.15 440 67 68 132.0 117.26 0.10 1.10 428 62 64 132.0 176.18 0.10 1.10 446 54 

6 136.0 153.88 0.09 1.05 435 68 68 6 136.0 119.59 0.10 1.10 435 62 64 6 136.0 178.46 0.11 1.20 449 54 

140.0 156.16 0.10 1.15 430 68 68 140.0 121.89 0.10 1.10 437 62 64 140.0 180.73 0.11 1.20 449 54 

P4-1 144.0 158.50 0.11 1.25 435 68 68 P4-1 144.0 124.13 0.12 1.35 435 62 64 P4-1 144.0 183.07 0.12 1.30 449 54 

148.0 160.71 0.12 1.36 441 68 68 148.0 126.48 0.12 1.35 436 62 64 148.0 185.49 0.12 1.30 449 54 

2 152.0 163.22 0.11 1.25 437 69 69 2 152.0 128.95 0.11 1.20 433 63 64 2 152.0 187.86 0.11 1.20 445 54 

156.0 165.62 0.11 1.25 437 69 69 156.0 131.35 0.11 1.20 433 63 64 156.0 190.23 0.11 1.20 444 54 

3 160.0 168.02 0.12 1.40 437 69 69 3 160.0 133.71 0.10 1.10 433 63 64 3 160.0 192.54 0.10 1.10 440 54 

164.0 170.48 0.11 1.25 433 69 69 164.0 136.00 0.10 1.10 429 63 64 164.0 194.78 0.10 1.10 440 54 

4 168.0 172.88 0.11 1.25 434 69 69 4 168.0 138.27 0.10 1.10 430 63 64 4 168.0 197.02 0.09 1.00 440 54 

172.0 175.39 0.11 1.25 435 68 69 172.0 140.53 0.10 1.10 430 63 64 172.0 199.24 0.09 1.00 440 54 

5 176.0 177.89 0.11 1.25 436 68 69 5 176.0 142.80 0.10 1.10 434 64 65 5 176.0 201.38 0.10 1.10 443 54 

180.0 180.34 0.11 1.25 439 67 69 180.0 145.10 0.10 1.10 435 64 65 180.0 203.50 0.10 1.10 443 54 

6 184.0 182.76 0.09 1.05 432 67 69 6 184.0 147.38 0.10 1.10 436 64 65 6 184.0 205.72 0.10 1.10 444 54 

188.0 185.01 0.10 1.15 438 67 69 188.0 149.67 0.10 1.10 436 64 65 188.0 207.94 0.10 1.10 445 54 

P5-1 192.0 187.26 0.14 1.60 438 66 69 P5-1 192.0 151.88 0.13 1.45 435 64 65 P5-1 192.0 210.18 0.11 1.20 445 54 

196.0 189.82 0.15 1.70 438 66 69 196.0 154.40 0.11 1.20 435 64 65 196.0 212.51 0.14 1.50 444 54 

2 200.0 192.67 0.14 1.60 437 66 68 2 200.0 156.83 0.11 1.20 435 64 65 2 200.0 215.13 0.13 1.40 442 54 

204.0 195.39 0.14 1.60 436 66 68 204.0 159.19 0.10 1.10 430 64 65 204.0 217.60 0.13 1.40 441 54 

3 208.0 198.13 0.10 1.15 431 66 68 3 208.0 161.43 0.12 1.35 425 64 65 3 208.0 220.11 0.10 1.10 438 54 

212.0 200.46 0.10 1.15 427 66 68 212.0 164.02 0.11 1.25 425 64 65 212.0 222.40 0.10 1.10 438 54 

4 216.0 202.78 0.12 1.40 426 66 68 4 216.0 166.42 0.12 1.35 427 64 65 4 216.0 224.61 0.11 1.20 438 54 

220.0 205.29 0.12 1.40 427 66 68 220.0 168.90 0.12 1.35 428 64 66 220.0 226.89 0.11 1.20 435 54 

5 224.0 207.84 0.13 1.50 428 67 68 5 224.0 171.44 0.12 1.35 428 64 66 5 224.0 229.25 0.12 1.30 436 53 

228.0 210.42 0.13 1.50 429 67 68 228.0 173.96 0.13 1.45 428 65 66 228.0 231.64 0.12 1.30 437 53 

6 232.0 213.08 0.13 1.50 429 67 68 6 232.0 176.57 0.10 1.15 424 65 66 6 232.0 234.10 0.12 1.30 436 53 

236.0 215.75 0.12 1.40 428 67 68 236.0 178.95 0.10 1.15 425 65 66 236.0 236.53 0.12 1.30 436 52 240.0 218.375 240.0 181.21 240.0 239.00

Input2
123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xls

LEHDER Environmental Services LtdPoint by Point CalculationsCompany: Owens Corning Plant: Delmar, NYStack: DM1 DEP OutletPollutant: TSP / ChromiumProject No.:Data Entry: KH / JE

Point Period Isokinecity Point Period Isokinecity Point Time 

min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s 

P1-1 4.0 0.069 2.45 8.0 26.3 92.4 P1-1 4.0 0.072 2.55 8.5 27.7 89.9 P1-1 4.0 0.073 2.56 8.3 27.2 

4.0 0.079 2.80 8.6 28.2 98.5 4.0 0.081 2.86 8.7 28.7 98.0 4.0 0.074 2.63 8.3 27.2 

2 4.0 0.075 2.64 8.0 26.2 99.4 2 4.0 0.074 2.60 7.9 25.8 98.3 2 4.0 0.070 2.49 7.7 25.2 

4.0 0.074 2.60 7.7 25.2 101.4 4.0 0.074 2.63 7.9 25.8 99.4 4.0 0.068 2.41 7.7 25.1 

3 4.0 0.068 2.41 7.3 24.1 98.4 3 4.0 0.075 2.64 7.9 25.8 99.9 3 4.0 0.069 2.43 7.6 25.1 

4.0 0.071 2.50 7.3 24.1 101.7 4.0 0.074 2.61 7.9 25.8 98.7 4.0 0.069 2.44 7.7 25.1 

4 4.0 0.069 2.44 7.3 24.1 99.5 4 4.0 0.071 2.51 7.6 24.8 98.7 4 4.0 0.071 2.50 7.3 24.0 

4.0 0.071 2.52 7.7 25.2 98.2 4.0 0.072 2.54 7.6 24.8 99.7 4.0 0.067 2.36 7.3 24.0 

5 4.0 0.071 2.51 7.7 25.2 97.9 5 4.0 0.072 2.54 7.6 24.8 100.0 5 4.0 0.069 2.43 7.6 25.1 

4.0 0.072 2.55 7.7 25.2 99.5 4.0 0.072 2.54 7.6 24.8 99.9 4.0 0.070 2.47 7.7 25.1 

6 4.0 0.072 2.55 7.7 25.1 99.2 6 4.0 0.069 2.42 7.2 23.7 99.4 6 4.0 0.066 2.32 7.3 24.1 

4.0 0.071 2.51 7.7 25.1 97.4 4.0 0.071 2.50 7.9 25.9 94.7 4.0 0.069 2.42 7.7 25.1 

P2-1 4.0 0.073 2.57 8.3 27.2 92.6 P2-1 4.0 0.071 2.51 7.9 25.8 94.7 P2-1 4.0 0.071 2.52 8.0 26.2 

4.0 0.078 2.77 8.3 27.2 99.9 4.0 0.074 2.62 8.2 26.8 95.3 4.0 0.073 2.59 8.3 27.1 

2 4.0 0.068 2.39 7.0 22.9 101.9 2 4.0 0.066 2.31 6.9 22.6 99.6 2 4.0 0.071 2.51 7.3 24.0 

4.0 0.067 2.36 7.0 22.9 100.6 4.0 0.068 2.40 7.2 23.7 98.6 4.0 0.069 2.42 7.3 24.0 

3 4.0 0.062 2.20 6.6 21.7 98.3 3 4.0 0.065 2.30 6.9 22.6 98.8 3 4.0 0.066 2.32 7.0 22.9 

4.0 0.063 2.23 6.6 21.7 99.7 4.0 0.067 2.38 6.9 22.6 102.2 4.0 0.063 2.24 7.0 22.9 

4 4.0 0.066 2.34 7.0 22.9 99.5 4 4.0 0.069 2.42 7.2 23.7 99.1 4 4.0 0.068 2.39 7.3 24.0 

4.0 0.066 2.34 7.0 22.9 99.6 4.0 0.068 2.40 7.2 23.7 98.3 4.0 0.066 2.34 7.3 24.0 

5 4.0 0.073 2.56 7.7 25.1 99.6 5 4.0 0.070 2.49 7.6 24.8 97.7 5 4.0 0.071 2.49 7.6 25.1 

4.0 0.072 2.54 7.7 25.1 98.8 4.0 0.072 2.55 7.6 24.8 100.2 4.0 0.069 2.43 7.6 25.1 

6 4.0 0.067 2.38 7.0 22.9 101.2 6 4.0 0.073 2.56 7.9 25.9 96.8 6 4.0 0.072 2.55 7.7 25.1 

4.0 0.065 2.31 6.6 21.8 103.6 4.0 0.066 2.32 6.9 22.7 100.0 4.0 0.069 2.43 7.7 25.1 

P3-1 4.0 0.064 2.26 7.3 24.1 91.9 P3-1 4.0 0.066 2.34 7.6 24.8 92.2 P3-1 4.0 0.070 2.45 7.6 25.1 

4.0 0.072 2.53 7.6 25.1 98.5 4.0 0.070 2.48 7.6 24.8 97.5 4.0 0.069 2.44 7.6 25.1 

2 4.0 0.069 2.43 7.0 22.9 103.6 2 4.0 0.068 2.41 6.9 22.6 103.6 2 4.0 0.066 2.34 7.0 22.9 

4.0 0.064 2.27 6.6 21.7 101.5 4.0 0.065 2.31 6.9 22.6 99.2 4.0 0.064 2.25 7.0 22.8 

3 4.0 0.062 2.18 6.6 21.6 97.2 3 4.0 0.065 2.29 6.9 22.6 98.6 3 4.0 0.060 2.14 6.6 21.7 

4.0 0.064 2.25 6.6 21.6 100.4 4.0 0.065 2.30 6.9 22.6 98.9 4.0 0.062 2.18 6.6 21.6 

4 4.0 0.064 2.25 6.6 21.6 100.7 4 4.0 0.066 2.33 6.9 22.6 99.9 4 4.0 0.062 2.19 6.6 21.6 

4.0 0.063 2.23 6.6 21.6 99.6 4.0 0.066 2.31 6.9 22.6 99.2 4.0 0.060 2.14 6.6 21.6 

5 4.0 0.066 2.32 7.0 22.9 98.8 5 4.0 0.068 2.40 7.2 23.7 98.3 5 4.0 0.062 2.20 6.6 21.7 

4.0 0.065 2.30 7.0 22.9 97.8 4.0 0.067 2.36 6.9 22.6 101.2 4.0 0.065 2.31 7.0 22.9 

6 4.0 0.065 2.30 6.6 21.6 102.9 6 4.0 0.066 2.32 6.9 22.6 100.0 6 4.0 0.065 2.29 7.3 24.0 

4.0 0.067 2.37 6.9 22.8 100.3 4.0 0.064 2.27 6.9 22.7 98.0 4.0 0.067 2.37 7.3 24.0 

P4-1 4.0 0.063 2.24 7.3 23.9 90.4 P4-1 4.0 0.067 2.37 7.6 24.8 93.4 P4-1 4.0 0.069 2.45 7.6 25.1 

4.0 0.072 2.54 7.6 25.1 98.7 4.0 0.071 2.50 7.6 24.8 98.4 4.0 0.068 2.40 7.6 25.1 

2 4.0 0.069 2.42 7.3 24.0 97.9 2 4.0 0.069 2.43 7.2 23.7 99.6 2 4.0 0.068 2.40 7.3 24.0 

4.0 0.069 2.43 7.3 24.0 98.1 4.0 0.068 2.39 7.2 23.7 98.1 4.0 0.066 2.33 7.3 23.9 

3 4.0 0.071 2.49 7.6 25.0 96.3 3 4.0 0.066 2.31 6.9 22.6 99.4 3 4.0 0.064 2.27 6.9 22.8 

4.0 0.069 2.43 7.3 23.9 98.1 4.0 0.065 2.30 6.9 22.6 98.5 4.0 0.064 2.26 6.9 22.8 

4 4.0 0.072 2.54 7.3 23.9 102.5 4 4.0 0.065 2.29 6.9 22.6 98.3 4 4.0 0.064 2.25 6.6 21.6 

4.0 0.072 2.53 7.3 23.9 102.0 4.0 0.065 2.30 6.9 22.6 98.6 4.0 0.061 2.16 6.6 21.6 

5 4.0 0.070 2.49 7.3 23.9 100.4 5 4.0 0.066 2.32 6.9 22.6 99.7 5 4.0 0.061 2.15 7.0 22.8 

4.0 0.069 2.44 7.3 24.0 99.0 4.0 0.066 2.31 6.9 22.6 99.3 4.0 0.064 2.25 7.0 22.8 

6 4.0 0.065 2.28 6.6 21.6 101.8 6 4.0 0.066 2.32 6.9 22.7 99.6 6 4.0 0.063 2.24 7.0 22.8 

4.0 0.064 2.28 7.0 22.9 96.7 4.0 0.063 2.23 6.9 22.7 95.9 4.0 0.064 2.27 7.0 22.8 

P5-1 4.0 0.073 2.59 8.2 27.0 93.2 P5-1 4.0 0.072 2.56 7.9 25.8 96.3 P5-1 4.0 0.067 2.36 7.3 24.0 

4.0 0.082 2.88 8.5 28.0 100.1 4.0 0.070 2.46 7.2 23.8 100.7 4.0 0.075 2.65 8.2 27.0 

2 4.0 0.078 2.75 8.2 27.0 99.0 2 4.0 0.068 2.38 7.2 23.8 97.6 2 4.0 0.071 2.51 7.9 26.0 

4.0 0.079 2.77 8.2 27.0 99.7 4.0 0.064 2.27 6.9 22.6 97.1 4.0 0.072 2.54 7.9 26.0 

3 4.0 0.067 2.36 6.9 22.8 99.9 3 4.0 0.074 2.62 7.5 24.7 102.2 3 4.0 0.066 2.32 6.9 22.8 

4.0 0.067 2.35 6.9 22.7 99.3 4.0 0.069 2.43 7.2 23.6 98.9 4.0 0.063 2.24 6.9 22.8 

4 4.0 0.072 2.54 7.6 24.9 98.1 4 4.0 0.071 2.52 7.5 24.7 98.2 4 4.0 0.065 2.30 7.3 23.9 

4.0 0.073 2.59 7.6 24.9 99.9 4.0 0.073 2.57 7.5 24.7 100.3 4.0 0.068 2.39 7.3 23.8 

5 4.0 0.074 2.61 7.9 25.9 96.9 5 4.0 0.072 2.55 7.5 24.7 99.6 5 4.0 0.069 2.42 7.6 24.9 

4.0 0.076 2.69 7.9 25.9 99.9 4.0 0.075 2.64 7.8 25.7 98.8 4.0 0.071 2.49 7.6 24.9 

6 4.0 0.077 2.70 7.9 25.9 100.3 6 4.0 0.068 2.41 6.9 22.5 102.8 6 4.0 0.070 2.46 7.6 24.9 

4.0 0.075 2.66 7.6 24.9 102.6 4.0 0.065 2.29 6.9 22.5 97.7 4.0 0.071 2.50 7.6 24.9 

Test #3

26-Jan-12

12:12 - 16:12

123987

Sample Volume Stack Velocity

Test #2

25-Jan-12

12:25 - 16:25

Test #1

24-Jan-12

13:45 - 17:45

Sample Volume Stack Velocity Sample Volume Stack Velocity

ISO-Velocity Calculations
123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xls

Company: Owens Corning Pollutant: TSP / Chromium

Plant: Delmar, NY Method: EPA Method 29

Stack: DM1 DEP Outlet Project No.: 123987

Reviewed by MD

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12 Average

13:45 - 17:45 12:25 - 16:25 12:12 - 16:12

Filterable Particulate Concentration mg/S.m3 1.5 1.7 1.3 1.5

Gr/dscf 0.00065 0.00074 0.00057 0.00065

Filterable Particulate Mass Rate mg/s 5.7 6.5 4.9 5.7

g/s 0.0057 0.0065 0.0049 0.0057

lb./hr 0.045 0.052 0.039 0.045

Filterable Chromium Concentration μg/S.m3 5.1 4.5 4.8 4.8

Filterable Chromium Mass Rate ug/s 1.9E+01 1.7E+01 1.8E+01 1.8E+01

mg/s 1.9E-02 1.7E-02 1.8E-02 1.8E-02

lb./hr 1.5E-04 1.4E-04 1.4E-04 1.4E-04

Condensable Chromium Concentration μg/S.m3 0.15 0.15 0.10 0.14

Condensable Chromium Mass Rate ug/s 5.9E-01 5.9E-01 3.9E-01 5.2E-01

mg/s 5.9E-04 5.9E-04 3.9E-04 5.2E-04

lb./hr 4.7E-06 4.7E-06 3.1E-06 4.1E-06

Total Chromium Concentration μg/S.m3 5.2 4.7 4.9 4.9

Total Chromium Mass Rate ug/s 2.0E+01 1.8E+01 1.8E+01 1.9E+01

mg/s 2.0E-02 1.8E-02 1.8E-02 1.9E-02

lb./hr 1.6E-04 1.4E-04 1.5E-04 1.5E-04

Effluent Characteristics

Area of Sample Plane m2 0.999 0.999 0.999 0.999

Area of Sample Plane ft2 10.758 10.758 10.758 10.758

Average Stack Temperature  ̊C 226 223 230 226

Average Stack Temperature (Ts)  ̊F 439 433 446 439

Average Stack Gas Pressure kPa 99.39 100.60 100.21 100.07

Average Stack Gas Pressure (Psa) in Hg 29.35 29.71 29.60 29.56

Average Stack Gas Velocity m/s 7.4 7.3 7.3 7.4

Average Stack Gas Velocity ft/min 1.45E+03 1.44E+03 1.45E+03 1.45E+03

Oxygen Concentration % vol 19.7 19.9 19.9 19.8

Carbon Dioxide Concentration % vol 4.5 4.9 4.8 4.73

Effluent Molecular Weight (dry) g/gmol 29.5 29.6 29.6 29.6

Effluent Molecular Weight (wet) g/gmol 28.29 28.4 28.3 28.3

Effluent Moisture Content % vol. 10.6 10.5 10.9 10.6

Dry Gas Fraction % vol. 89.4 89.5 89.1 89.4

Actual Effluent Flow Rate A.m3

/s 7.37 7.32 7.35 7.35

Actual Effluent Flow Rate Acfm 1.56E+04 1.55E+04 1.56E+04 1.56E+04

Reference Flow Rate (wet) S.m3

/s 4.25 4.30 4.23 4.26

Standard Flow Rate (wet) Scfm 9.00E+03 9.11E+03 8.97E+03 9.03E+03

Reference Flow Rate (dry) S.m3

/s (dry) 3.80 3.85 3.77 3.81

Standard Flow Rate (dry) Scfm (dry) 8.048E+03 8.16E+03 8.00E+03 8.07E+03

Sample Parameters

Sample Period min 240.0 240.0 240.0 240.0

Sample Period Hours 4.0 4.0 4.0 4.0

Front-Half Filterable Loading (Acetone) mg 2.7 3.1 3.1 3.0

Front-Half Filterable Loading (Filter) mg 3.5 4.0 2.3 3.3

Filterable Chromium (Front-Half) μg 21.2 19.0 19.8 20.0

Condensable Chromium (Back-Half) μg 0.6 0.6 0.4 0.6

Sample Volume A.m3 4.185 4.137 4.038 4.120

Sample Volume acf 147.79 146.11 142.59 145.50

Dry Reference Sample Volume S.m3 4.167 4.203 4.155 4.175

Dry Standard Sample Volume Scf 147.17 148.44 146.74 147.45

Water Vapour Reference Volume S.m3 0.492 0.493 0.507 0.497

Water Vapour Reference Volume scf 17.37 17.41 17.90 17.56

Average Meter Temperature  ̊C 20 17 12 17

Average Meter Temperature  ̊F 68 63 54 62

Average Absolute Meter Pressure in Hg 29.78 30.13 30.00 29.97

Average Absolute Meter Pressure kPa 100.84 102.02 101.57 101.48

Average Delta P in H2O 0.11 0.11 0.11 0.11

Average Delta H in H2O 1.28 1.26 1.22 1.25

Average Sample Rate Lpm 17.4 17.2 16.8 17.2

Average Sample Rate cfm 0.62 0.61 0.59 0.61

Average Isokinetic Variation % 99.1 98.6 99.5 99.0

Measurement Parameter

LEHDER Environmental Services Ltd.

TSP & Chromium Calculations
123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xls

LEHDER Environmental Services Ltd Revised by: M.Denomme

Date: 16-Feb-12

Company: Owens Corning 

Plant: Delmar, NY

Stack: DM2 DEP Outlet

Pollutant: TSP / Chromium

Method: EPA Method 29

Project No.: 123987

Operators RS / JH / JT

Data Entry: KH / JE

Reviewed By: MD

Ref.Temperature: 68 deg. F

Ref. Pressure: 29.92 "Hg

Molar Volume: 24.04 l/mol

Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

13:45 - 18:00 12:25 - 16:25 12:12 - 16:12

No. of Sample Points 30 30 30

Sample Time /Point min 8.0 8.0 8.0

Reading / Point min 4.0 4.0 4.0

Total Sample Time, min 240.0 240.0 240.0

Barometric Pressure, Pb "Hg 29.69 30.04 29.91

Stack Gauge Pressure, Pgauge "H2O -0.91 -0.91 -0.88

Absolute Stack Pressure, Ps "Hg 29.62 29.97 29.85

Pitot Tube Coefficient, Cp 0.822 0.822 0.822

Oxygen Content, O2 % 20.0 20.2 20.1

Carbon Dioxide Content, CO2 % 4.4 4.6 4.5

Carbon Monoxide Content, CO % 0.0 0.0 0.0

Nitrogen Content, N2 % 75.7 75.2 75.4

Condensate Collected, WH2O g 353.3 362.3 382.1

Nozzle Diameter, Dn in 0.3833 0.3908 0.3908

Initial DGM Reading ft3 361.666 625.410 893.055

Final DGM Reading ft3 508.780 777.785 1041.170

DGM Unity, Y 0.9991 0.9991 0.9991

Stack Width ft 3.280 3.280 3.280

Stack Depth ft 3.280 3.280 3.280

Actual Volume of Dry Gas ft3 146.9816 152.2379 147.9817

Stack Area, As ft2 10.758 10.758 10.758

Particulate/Chromium Analysis

Front-Half Acetone Residue mg 1.1 2.7 3.5

Filter Loading mg 35.3 30.8 27.7

Total Suspended PM mg 36.4 33.5 31.2

Front-Half (Filterable) Chromium μg 191 180 151

Condensable (Back-Half) Chromium μg 0.75 0.92 1.1

Total Chromium μg 192 181 152

Input1
123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xls

LEHDER Environmental Services Ltd

Point by Point Sampling DataCompany: Owens Corning Plant: Delmar, NYStack: DM2 DEP OutletPollutant: TSP / ChromiumProject No.: 123987

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

13:45 - 18:00 12:25 - 16:25 12:12 - 16:12

Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi 

# min ft3 H2O H2O F F F # min ft3 H2O H2O F F F # min ft3 H2O H2O FF

P5-1 0.0 361.67 0.12 1.48 420 66 66 P5-1 0.0 625.41 0.12 1.59 420 63 63 P5-1 0.0 893.06 0.13 1.66 438 52 

4.0 364.30 0.11 1.35 427 66 66 4.0 628.03 0.13 1.71 429 62 63 4.0 895.68 0.14 1.77 444 49 

2 8.0 366.84 0.13 1.59 427 66 66 2 8.0 630.72 0.14 1.83 432 62 63 2 8.0 898.41 0.13 1.64 444 49 

12.0 369.59 0.13 1.59 431 66 66 12.0 633.52 0.14 1.83 433 61 63 12.0 901.03 0.14 1.76 445 49 

3 16.0 372.13 0.13 1.58 432 66 66 3 16.0 636.31 0.15 1.89 434 61 63 3 16.0 903.75 0.14 1.70 445 49 

20.0 374.76 0.13 1.58 433 66 66 20.0 639.18 0.15 1.89 433 61 63 20.0 906.42 0.14 1.76 445 49 

4 24.0 377.38 0.14 1.70 434 66 66 4 24.0 642.05 0.14 1.83 434 62 63 4 24.0 909.15 0.14 1.76 446 50 

28.0 380.11 0.14 1.70 438 66 67 28.0 644.91 0.15 1.89 436 62 63 28.0 911.86 0.14 1.76 448 50 

5 32.0 382.84 0.13 1.56 445 66 67 5 32.0 647.79 0.14 1.82 437 62 63 5 32.0 914.60 0.14 1.76 450 50 

36.0 385.47 0.13 1.50 446 67 67 36.0 650.63 0.14 1.82 437 62 63 36.0 917.29 0.15 1.82 451 50 

6 40.0 388.10 0.12 1.46 434 66 67 6 40.0 653.42 0.12 1.57 435 62 63 6 40.0 920.07 0.13 1.63 449 50 

44.0 390.60 0.12 1.44 445 67 67 44.0 656.06 0.12 1.57 435 62 63 44.0 922.73 0.13 1.63 450 51 

P4-1 48.0 393.17 0.13 1.58 438 67 67 P4-1 48.0 658.63 0.12 1.56 421 62 63 P4-1 48.0 925.28 0.14 1.70 443 51 

52.0 395.87 0.14 1.70 439 67 67 52.0 661.19 0.12 1.59 423 62 63 52.0 927.90 0.14 1.77 442 51 

2 56.0 398.53 0.11 1.34 435 67 67 2 56.0 663.78 0.11 1.46 422 62 63 2 56.0 930.69 0.12 1.53 438 51 

60.0 400.99 0.11 1.28 434 67 67 60.0 666.31 0.11 1.46 422 62 63 60.0 933.28 0.12 1.53 439 51 

3 64.0 403.33 0.11 1.28 434 67 67 3 64.0 668.81 0.10 1.32 419 62 63 3 64.0 935.82 0.11 1.40 436 51 

68.0 405.67 0.11 1.28 433 66 67 68.0 671.16 0.10 1.33 419 63 63 68.0 938.25 0.11 1.40 437 51 

4 72.0 408.03 0.12 1.45 440 66 67 4 72.0 673.53 0.12 1.59 422 62 63 4 72.0 940.66 0.13 1.59 441 51 

76.0 410.54 0.13 1.57 441 66 67 76.0 676.20 0.12 1.52 423 61 63 76.0 943.23 0.13 1.59 441 51 

5 80.0 413.17 0.13 1.57 443 66 67 5 80.0 678.69 0.14 1.84 429 61 63 5 80.0 945.81 0.14 1.70 447 51 

84.0 415.81 0.14 1.63 444 66 67 84.0 681.45 0.14 1.83 430 61 63 84.0 948.51 0.14 1.70 448 51 

6 88.0 418.47 0.14 1.68 444 65 67 6 88.0 684.29 0.13 1.70 434 62 63 6 88.0 951.19 0.14 1.76 451 51 

92.0 421.20 0.14 1.69 442 65 66 92.0 687.02 0.14 1.83 435 62 63 92.0 953.89 0.14 1.76 451 51 

P3-1 96.0 423.89 0.10 1.21 430 65 67 P3-1 96.0 689.76 0.11 1.46 419 62 63 P3-1 96.0 956.57 0.12 1.54 434 51 

100.0 426.25 0.11 1.35 427 65 67 100.0 692.21 0.10 1.30 419 62 63 100.0 959.15 0.12 1.53 435 51 

2 104.0 428.66 0.10 1.23 424 65 67 2 104.0 694.60 0.10 1.30 415 62 63 2 104.0 961.69 0.10 1.29 429 51 

108.0 430.96 0.10 1.23 423 66 67 108.0 696.94 0.09 1.20 414 62 63 108.0 964.03 0.10 1.29 429 51 

3 112.0 433.24 0.09 1.11 421 65 67 3 112.0 699.25 0.09 1.20 413 62 63 3 112.0 966.31 0.09 1.16 429 51 

116.0 435.42 0.09 1.11 421 66 67 116.0 701.51 0.09 1.20 412 62 63 116.0 968.50 0.09 1.16 430 51 

4 120.0 437.59 0.10 1.23 424 66 67 4 120.0 703.78 0.10 1.27 414 62 63 4 120.0 970.67 0.10 1.28 433 51 

124.0 439.91 0.10 1.23 423 66 67 124.0 706.11 0.10 1.27 414 62 63 124.0 973.00 0.11 1.34 433 50 

5 128.0 442.22 0.12 1.41 426 66 67 5 128.0 708.45 0.12 1.60 418 62 63 5 128.0 975.33 0.11 1.40 435 49 

132.0 444.69 0.12 1.41 427 66 67 132.0 711.03 0.12 1.60 421 62 63 132.0 977.77 0.11 1.33 437 48 

6 136.0 447.16 0.13 1.59 430 66 67 6 136.0 713.66 0.14 1.78 426 62 63 6 136.0 980.15 0.11 1.39 441 49 

140.0 449.90 0.13 1.59 431 66 67 140.0 716.42 0.14 1.78 426 62 63 140.0 982.58 0.11 1.39 441 49 

P2-1 144.0 452.44 0.09 1.12 416 66 67 P2-1 144.0 719.25 0.11 1.47 414 62 63 P2-1 144.0 984.94 0.10 1.27 433 50 

148.0 454.67 0.11 1.37 417 67 68 148.0 721.74 0.11 1.47 415 62 63 148.0 987.22 0.10 1.28 432 50 

2 152.0 457.07 0.10 1.25 414 67 68 2 152.0 724.22 0.11 1.40 414 62 63 2 152.0 989.55 0.10 1.28 431 50 

156.0 459.43 0.10 1.25 413 67 68 156.0 726.68 0.10 1.34 412 62 63 156.0 991.89 0.10 1.28 430 50 

3 160.0 461.79 0.10 1.25 413 66 67 3 160.0 729.10 0.09 1.21 411 62 63 3 160.0 994.16 0.08 1.03 428 51 

164.0 464.08 0.10 1.18 413 66 67 164.0 731.38 0.09 1.21 411 62 63 164.0 996.23 0.09 1.09 428 51 

4 168.0 466.35 0.10 1.25 413 66 67 4 168.0 733.56 0.10 1.34 413 62 63 4 168.0 998.41 0.09 1.15 431 51 

172.0 468.71 0.10 1.24 416 66 67 172.0 735.92 0.10 1.34 414 62 63 172.0 1000.54 0.09 1.15 432 51 

5 176.0 471.02 0.12 1.49 419 66 67 5 176.0 738.30 0.12 1.53 418 63 63 5 176.0 1002.74 0.11 1.40 435 51 

180.0 473.58 0.12 1.48 419 65 67 180.0 740.80 0.11 1.46 418 62 64 180.0 1005.13 0.11 1.40 436 51 

6 184.0 476.09 0.13 1.54 421 65 67 6 184.0 743.35 0.12 1.60 419 62 64 6 184.0 1007.54 0.11 1.34 438 51 

188.0 478.73 0.13 1.60 422 65 66 188.0 745.93 0.12 1.53 418 62 64 188.0 1009.90 0.11 1.34 439 51 

P1-1 192.0 481.33 0.12 1.49 415 65 66 P1-1 192.0 748.50 0.12 1.60 414 63 64 P1-1 192.0 1012.20 0.11 0.41 433 51 

196.0 483.83 0.12 1.42 417 65 66 196.0 750.96 0.12 1.60 417 63 64 196.0 1014.66 0.11 1.41 434 51 

2 200.0 486.34 0.10 1.25 414 67 66 2 200.0 753.57 0.12 1.53 417 63 64 2 200.0 1017.15 0.11 1.41 432 51 

204.0 488.66 0.10 1.24 414 65 66 204.0 756.15 0.12 1.54 415 63 64 204.0 1019.61 0.11 1.41 431 51 

3 208.0 490.96 0.10 1.25 412 65 66 3 208.0 758.68 0.10 1.34 411 63 64 3 208.0 1022.06 0.10 1.29 428 51 

212.0 493.26 0.10 1.25 412 65 66 212.0 761.06 0.10 1.34 411 63 63 212.0 1024.50 0.10 1.29 428 51 

4 216.0 495.57 0.11 1.30 415 65 66 4 216.0 763.42 0.11 1.41 411 63 64 4 216.0 1026.82 0.11 1.35 429 51 

220.0 497.87 0.10 1.24 415 65 66 220.0 765.86 0.11 1.41 413 63 64 220.0 1029.21 0.11 1.35 430 51 

5 224.0 500.17 0.12 1.43 416 65 66 5 224.0 768.25 0.11 1.47 418 63 64 5 224.0 1031.55 0.11 1.41 431 50 

228.0 502.70 0.12 1.42 418 65 66 228.0 770.65 0.12 1.59 420 63 64 228.0 1033.96 0.11 1.41 434 50 

6 232.0 505.22 0.10 1.25 408 66 66 6 232.0 773.07 0.10 1.33 420 63 64 6 232.0 1036.38 0.11 1.41 434 50 

236.0 507.55 0.10 1.19 408 65 66 236.0 775.48 0.10 1.33 419 63 64 236.0 1038.79 0.11 1.41 434 51 240.0 509.78 240.0 777.79 240.0 1041.17

Input2
123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xls

LEHDER Environmental Services LtdPoint by Point CalculationsCompany: Owens Corning Plant: Delmar, NYStack: DM2 DEP OutletPollutant: TSP / ChromiumProject No.:Data Entry: KH / JE

Point Period Isokinecity Point Period Isokinecity Point Time 

min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s 

P5-1 4.0 0.075 2.63 7.6 24.9 102.9 P5-1 4.0 0.074 2.61 7.5 24.8 99.3 P5-1 4.0 0.074 2.62 8.0 26.1 

4.0 0.072 2.54 7.3 24.0 104.0 4.0 0.076 2.69 7.9 25.9 98.7 4.0 0.077 2.72 8.3 27.2 

2 4.0 0.078 2.75 7.9 26.1 103.6 2 4.0 0.079 2.80 8.2 26.9 99.4 2 4.0 0.074 2.62 8.0 26.2 

4.0 0.072 2.53 8.0 26.1 95.7 4.0 0.079 2.79 8.2 26.9 99.0 4.0 0.077 2.72 8.3 27.2 

3 4.0 0.074 2.63 8.0 26.1 99.4 3 4.0 0.081 2.87 8.4 27.4 100.1 3 4.0 0.075 2.66 8.1 26.7 

4.0 0.074 2.62 8.0 26.1 99.3 4.0 0.081 2.86 8.4 27.4 100.0 4.0 0.077 2.73 8.3 27.2 

4 4.0 0.077 2.73 8.3 27.1 99.5 4 4.0 0.081 2.86 8.2 26.9 101.6 4 4.0 0.077 2.71 8.3 27.2 

4.0 0.077 2.72 8.3 27.2 99.5 4.0 0.081 2.87 8.4 27.5 100.4 4.0 0.078 2.74 8.3 27.3 

5 4.0 0.074 2.63 8.0 26.3 100.0 5 4.0 0.080 2.84 8.2 27.0 101.0 5 4.0 0.076 2.69 8.3 27.3 

4.0 0.074 2.63 7.9 25.8 102.0 4.0 0.079 2.79 8.2 27.0 99.1 4.0 0.079 2.77 8.5 27.8 

6 4.0 0.071 2.50 7.7 25.1 98.4 6 4.0 0.075 2.64 7.6 25.0 101.1 6 4.0 0.075 2.66 8.0 26.3 

4.0 0.073 2.57 7.7 25.3 101.6 4.0 0.073 2.57 7.6 25.0 98.5 4.0 0.072 2.55 8.0 26.3 

P4-1 4.0 0.076 2.70 8.0 26.2 102.2 P4-1 4.0 0.072 2.55 7.5 24.8 97.1 P4-1 4.0 0.074 2.62 8.1 26.7 

4.0 0.075 2.66 8.3 27.2 97.0 4.0 0.073 2.59 7.6 24.8 98.8 4.0 0.079 2.78 8.3 27.2 

2 4.0 0.070 2.46 7.3 24.1 101.1 2 4.0 0.072 2.53 7.2 23.7 100.5 2 4.0 0.074 2.60 7.6 25.1 

4.0 0.066 2.34 7.2 23.5 98.2 4.0 0.071 2.50 7.2 23.7 99.4 4.0 0.072 2.53 7.7 25.1 

3 4.0 0.066 2.34 7.2 23.5 98.2 3 4.0 0.066 2.34 6.9 22.6 97.5 3 4.0 0.069 2.43 7.3 24.0 

4.0 0.067 2.36 7.2 23.5 99.1 4.0 0.067 2.37 6.9 22.6 98.5 4.0 0.068 2.41 7.3 24.0 

4 4.0 0.071 2.50 7.7 25.2 98.8 4 4.0 0.075 2.67 7.6 24.8 101.5 4 4.0 0.073 2.57 7.8 25.7 

4.0 0.075 2.63 8.0 26.3 100.0 4.0 0.070 2.48 7.4 24.3 96.8 4.0 0.073 2.58 7.8 25.7 

5 4.0 0.075 2.64 8.0 26.3 100.4 5 4.0 0.078 2.76 8.2 26.9 97.8 5 4.0 0.076 2.69 8.2 26.8 

4.0 0.075 2.65 8.2 26.8 99.0 4.0 0.080 2.84 8.2 26.9 100.5 4.0 0.076 2.68 8.2 26.8 

6 4.0 0.077 2.73 8.3 27.3 100.3 6 4.0 0.077 2.73 7.9 26.0 100.5 6 4.0 0.076 2.70 8.3 27.3 

4.0 0.076 2.69 8.3 27.3 98.6 4.0 0.077 2.73 8.2 27.0 97.1 4.0 0.076 2.68 8.3 27.3 

P3-1 4.0 0.067 2.35 7.0 22.9 101.3 P3-1 4.0 0.069 2.45 7.2 23.7 97.3 P3-1 4.0 0.073 2.58 7.6 25.0 

4.0 0.068 2.41 7.3 24.0 98.9 4.0 0.067 2.38 6.9 22.6 99.1 4.0 0.072 2.54 7.6 25.1 

2 4.0 0.065 2.30 7.0 22.8 98.6 2 4.0 0.066 2.34 6.7 22.0 99.8 2 4.0 0.066 2.34 6.9 22.8 

4.0 0.064 2.27 6.9 22.8 97.3 4.0 0.065 2.31 6.5 21.4 100.9 4.0 0.065 2.28 6.9 22.8 

3 4.0 0.062 2.18 6.6 21.6 98.3 3 4.0 0.064 2.26 6.5 21.4 98.7 3 4.0 0.062 2.18 6.6 21.6 

4.0 0.061 2.17 6.6 21.6 97.7 4.0 0.064 2.26 6.5 21.3 98.8 4.0 0.061 2.17 6.6 21.6 

4 4.0 0.066 2.32 7.0 22.8 99.3 4 4.0 0.066 2.33 6.7 21.9 99.3 4 4.0 0.066 2.33 7.0 22.8 

4.0 0.065 2.31 6.9 22.8 99.1 4.0 0.066 2.33 6.7 21.9 99.3 4.0 0.066 2.32 7.1 23.4 

5 4.0 0.070 2.46 7.5 24.5 98.6 5 4.0 0.073 2.58 7.5 24.7 98.1 5 4.0 0.069 2.44 7.3 24.0 

4.0 0.070 2.47 7.5 24.5 98.8 4.0 0.074 2.62 7.5 24.8 99.8 4.0 0.067 2.38 7.2 23.5 

6 4.0 0.078 2.74 8.0 26.1 103.3 6 4.0 0.078 2.76 8.0 26.3 99.2 6 4.0 0.069 2.42 7.3 24.1 

4.0 0.072 2.54 8.0 26.1 96.0 4.0 0.080 2.83 8.0 26.3 101.9 4.0 0.067 2.36 7.3 24.1 

P2-1 4.0 0.063 2.23 6.6 21.5 100.2 P2-1 4.0 0.070 2.49 7.2 23.6 98.4 P2-1 4.0 0.065 2.28 7.0 22.8 

4.0 0.068 2.40 7.3 23.8 97.6 4.0 0.070 2.48 7.2 23.6 98.1 4.0 0.066 2.33 7.0 22.8 

2 4.0 0.067 2.35 6.9 22.7 100.1 2 4.0 0.070 2.46 7.0 23.1 99.5 2 4.0 0.066 2.34 7.0 22.8 

4.0 0.067 2.36 6.9 22.7 100.2 4.0 0.068 2.42 6.9 22.5 100.2 4.0 0.064 2.26 7.0 22.8 

3 4.0 0.065 2.29 6.9 22.7 97.6 3 4.0 0.065 2.28 6.5 21.3 99.4 3 4.0 0.059 2.07 6.2 20.4 

4.0 0.064 2.26 6.7 22.1 98.9 4.0 0.062 2.17 6.5 21.3 94.8 4.0 0.062 2.17 6.4 21.0 

4 4.0 0.067 2.36 6.9 22.7 100.4 4 4.0 0.067 2.36 6.9 22.5 97.8 4 4.0 0.060 2.13 6.6 21.6 

4.0 0.065 2.30 6.9 22.7 98.2 4.0 0.067 2.38 6.9 22.5 98.9 4.0 0.062 2.20 6.6 21.7 

5 4.0 0.073 2.56 7.6 24.9 100.0 5 4.0 0.071 2.49 7.4 24.2 96.7 5 4.0 0.068 2.39 7.3 24.0 

4.0 0.071 2.50 7.6 24.9 97.9 4.0 0.072 2.55 7.2 23.7 101.1 4.0 0.068 2.41 7.3 24.0 

6 4.0 0.075 2.64 7.8 25.5 101.3 6 4.0 0.073 2.57 7.5 24.7 97.7 6 4.0 0.067 2.36 7.2 23.5 

4.0 0.073 2.59 7.9 26.0 97.6 4.0 0.073 2.57 7.4 24.2 99.5 4.0 0.065 2.30 7.2 23.5 

P1-1 4.0 0.071 2.51 7.6 24.9 97.8 P1-1 4.0 0.070 2.46 7.5 24.7 93.0 P1-1 4.0 0.069 2.45 7.3 24.0 

4.0 0.071 2.50 7.4 24.4 99.9 4.0 0.074 2.61 7.5 24.7 98.9 4.0 0.071 2.49 7.3 24.0 

2 4.0 0.066 2.32 6.9 22.7 98.8 2 4.0 0.073 2.57 7.4 24.2 99.6 2 4.0 0.070 2.46 7.3 23.9 

4.0 0.065 2.30 6.9 22.7 98.1 4.0 0.072 2.53 7.4 24.2 97.9 4.0 0.069 2.44 7.3 23.9 

3 4.0 0.065 2.30 6.9 22.7 98.0 3 4.0 0.067 2.38 6.9 22.5 98.3 3 4.0 0.069 2.44 6.9 22.8 

4.0 0.065 2.31 6.9 22.7 98.4 4.0 0.067 2.36 6.9 22.5 97.6 4.0 0.065 2.31 6.9 22.8 

4 4.0 0.065 2.30 7.1 23.3 95.8 4 4.0 0.069 2.44 7.0 23.0 98.4 4 4.0 0.068 2.39 7.1 23.4 

4.0 0.065 2.30 6.9 22.7 98.2 4.0 0.068 2.39 7.0 23.1 96.6 4.0 0.066 2.34 7.1 23.4 

5 4.0 0.072 2.53 7.4 24.3 100.8 5 4.0 0.068 2.39 7.2 23.7 94.8 5 4.0 0.068 2.40 7.3 23.9 

4.0 0.071 2.52 7.4 24.4 100.5 4.0 0.068 2.42 7.5 24.8 91.8 4.0 0.069 2.42 7.3 24.0 

6 4.0 0.066 2.33 6.9 22.6 98.9 6 4.0 0.068 2.40 6.9 22.6 99.8 6 4.0 0.068 2.40 7.3 24.0 

4.0 0.063 2.23 6.7 22.0 97.2 4.0 0.065 2.31 6.9 22.6 95.8 4.0 0.067 2.38 7.3 24.0 

Sample Volume Stack Velocity Sample Volume Stack Velocity Sample Volume Stack Velocity

Test #2

25-Jan-12

12:25 - 16:25

Test #1

24-Jan-12

13:45 - 18:00

Test #3

26-Jan-12

12:12 - 16:12

123987

ISO-Velocity Calculations
123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xls

Company: Owens Corning Pollutant: TSP / Chromium

Plant: Delmar, NY Method: EPA Method 29

Stack: DM2 DEP Outlet Project No.: 123987

Reviewed by MD

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12 Average

13:45 - 18:00 12:25 - 16:25 12:12 - 16:12

Filterable Particulate Concentration mg/S.m3 8.8 7.6 7.2 7.9

Gr/dscf 0.0038 0.0033 0.0031 0.0034

Filterable Particulate Mass Rate mg/s 34 30 28 31

g/s 0.034 0.030 0.028 0.031

lb./hr 0.27 0.24 0.22 0.25

Filterable Chromium Concentration μg/S.m3 45.9 41.0 34.8 40.6

Filterable Chromium Mass Rate ug/s 1.81E+02 1.64E+02 1.36E+02 1.60E+02

mg/s 1.81E-01 1.64E-01 1.36E-01 1.60E-01

lb./hr 1.43E-03 1.30E-03 1.08E-03 1.27E-03

Condensable Chromium Concentration μg/S.m3 0.18 0.21 0.26 0.22

Condensable Chromium Mass Rate ug/s 7.10E-01 8.40E-01 1.02E+00 8.57E-01

mg/s 7.10E-04 8.40E-04 1.02E-03 8.57E-04

lb./hr 5.64E-06 6.67E-06 8.10E-06 6.80E-06

Total Chromium Concentration μg/S.m3 46.1 41.2 35.1 40.8

Total Chromium Mass Rate ug/s 1.81E+02 1.65E+02 1.37E+02 1.61E+02

mg/s 1.81E-01 1.65E-01 1.37E-01 1.61E-01

lb./hr 1.44E-03 1.31E-03 1.09E-03 1.28E-03

Effluent Characteristics

Area of Sample Plane m2 0.999 0.999 0.999 0.999

Area of Sample Plane ft2 10.758 10.758 10.758 10.758

Average Stack Temperature  ̊C 219 216 225 220

Average Stack Temperature (Ts)  ̊F 426 421 437 428

Average Stack Gas Pressure kPa 100.29 101.48 101.05 100.94

Average Stack Gas Pressure (Psa) in Hg 29.62 29.97 29.85 29.81

Average Stack Gas Velocity m/s 7.4 7.4 7.5 7.4

Average Stack Gas Velocity ft/min 1.46E+03 1.45E+03 1.47E+03 1.46E+03

Oxygen Concentration % vol 20.0 20.2 20.1 20.1

Carbon Dioxide Concentration % vol 4.4 4.6 4.5 4.49

Effluent Molecular Weight (dry) g/gmol 29.5 29.5 29.5 29.5

Effluent Molecular Weight (wet) g/gmol 28.32 28.4 28.3 28.3

Effluent Moisture Content % vol. 10.2 9.93 10.5 10.2

Dry Gas Fraction % vol. 89.8 90.1 89.5 89.8

Actual Effluent Flow Rate A.m3

/s 7.4 7.4 7.5 7.4

Actual Effluent Flow Rate Acfm 1.57E+04 1.56E+04 1.58E+04 1.57E+04

Reference Flow Rate (wet) S.m3

/s 4.4 4.4 4.4 4.4

Standard Flow Rate (wet) Scfm 9.28E+03 9.39E+03 9.28E+03 9.32E+03

Reference Flow Rate (dry) S.m3

/s (dry) 3.9 4.0 3.9 3.9

Standard Flow Rate (dry) Scfm (dry) 8.33E+03 8.46E+03 8.30E+03 8.36E+03

Sample Parameters

Sample Period min 240.0 240.0 240.0 240.0

Sample Period Hours 4.0 4.0 4.0 4.0

Front-Half Filterable Loading (Acetone) mg 1.1 2.7 3.5 2.4

Front-Half Filterable Loading (Filter) mg 35.3 30.8 27.7 31.3

Filterable Chromium (Front-Half) μg 191.0 180.0 151.0 174.0

Condensable Chromium (Back-Half) μg 0.8 0.9 1.1 0.9

Sample Volume A.m3 4.162 4.311 4.190 4.221

Sample Volume acf 146.98 152.24 147.98 149.07

Dry Reference Sample Volume S.m3 4.158 4.388 4.340 4.295

Dry Standard Sample Volume Scf 146.84 154.98 153.25 151.69

Water Vapour Reference Volume S.m3 0.472 0.484 0.510 0.489

Water Vapour Reference Volume scf 16.66 17.09 18.02 17.26

Average Meter Temperature  ̊C 19 17 11 16

Average Meter Temperature  ̊F 66 63 51 60

Average Absolute Meter Pressure in Hg 29.79 30.15 30.02 29.99

Average Absolute Meter Pressure kPa 100.87 102.09 101.63 101.53

Average Delta P in H2O 0.11 0.12 0.12 0.11

Average Delta H in H2O 1.40 1.53 1.45 1.46

Average Sample Rate Lpm 17.3 18.0 17.5 17.6

Average Sample Rate cfm 0.61 0.63 0.62 0.62

Average Isokinetic Variation % 99.3 98.7 99.5 99.1

Measurement Parameter

LEHDER Environmental Services Ltd.

TSP & Chromium Calculations
Appendix A.2 

Method 0061 Test Runs 
123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls

LEHDER Environmental Services Ltd Mike Denomme

16-Feb-12

Company: Owens Corning 

Plant: Delmar NY

Stack: DM1 DEP Outlet 

Pollutant: Hexavalent/Total Chromium

Method: EPA Method 0061

Project No.: 123987

Operators RS / JH

Data Entry: KH / JE

Reviewed By: MD

Ref.Temperature: 68 deg. F

Ref. Pressure: 29.92 "Hg

Velocity Constant: 85.49

Molar Volume: 24.04 l/mol

Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

No. of Sample Points 30 30 30

Sample Time /Point min 8.0 7.0 7.0

Reading / Point min 4.0 3.5 3.5

Total Sample Time, min 240.0 210.0 210.0

Barometric Pressure, Pb "Hg 29.65 30.04 29.97

Stack Gauge Pressure, Pgauge "H2O -4.43 -4.63 -4.35

Absolute Stack Pressure, Ps "Hg 29.32 29.70 29.65

Pitot Tube Coefficient, Cp 0.779 0.779 0.779

Oxygen Content, O2 % 19.6 20.0 19.9

Carbon Dioxide Content, CO2 % 4.9 4.7 4.8

Carbon Monoxide Content, CO % 0.0 0.0 0.0

Nitrogen Content, N2 % 75.6 75.3 75.3

Condensate Collected, WH2O g 349.4 286.9 313.9

Nozzle Diameter, Dn in 0.3648 0.3648 0.3648

Initial DGM Reading ft3 41.380 18.770 81.563

Final DGM Reading ft3 171.665 136.030 197.757

DGM Unity, Y 1.0123 1.0123 1.0123

Stack Width ft 3.280 3.280 3.280

Stack Depth ft 3.280 3.280 3.280

Actual Volume of Dry Gas ft3 131.8875 118.7023 117.6232

Stack Area, As ft2 10.758 10.758 10.758

Hex Chromium Analysis

Uncorrected Chromium (Cr ) 6+ ug 12.50 11.80 8.87

Blank Correction ug 1.72 1.72 1.72

Corrected Hexavalent Chromium ug 10.8 10.1 7.15

Total Chromium Analysis

Total Chromium - (1) KOH & Rinses ug 17.2 18.9 20.3

Total Chromium - (3) Nitric Rinse ug 0.39 0.355 0.281

Total Chromium - (3) Column Filter ug 0.916 1.24 0.75

Uncorrected Total Chromium ug 18.5 20.5 21.3

Blank Correction (4) ug 3.14 3.14 3.14

Total Chromium (1 + 2 + 3) - 4 ug 15.4 17.4 18.2

Italics indicate values less than method detection

Input1
123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls

LEHDER Environmental Services Ltd

Point by Point Sampling Data

Company: Owens Corning 

Plant: Delmar NY

Stack: DM1 DEP Outlet

Pollutant: Hexavalent/Total Chromium

Project No.: 123987

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo

# min ft3 H2O H2O F F F # min ft3 H2O H2O F F F # min ft3 H2O H2O F F F

P1-1 0.0 41.38 0.160 1.30 444 66 66 P1-1 0.0 18.77 0.160 1.25 433 67 67 P1-1 0.0 81.56 0.170 1.35 440 69 69

4.0 43.68 0.170 1.35 447 63 66 3.5 20.84 0.170 1.32 433 65 67 3.5 83.64 0.170 1.35 442 69 69

2 8.0 46.16 0.140 1.10 447 63 65 2 7.0 23.00 0.150 1.20 432 63 66 2 7.0 85.84 0.150 1.20 441 69 69

12.0 48.46 0.140 1.10 447 64 65 10.5 25.02 0.160 1.25 433 63 66 10.5 87.91 0.150 1.20 442 69 69

3 16.0 50.68 0.130 1.05 447 65 65 3 14.0 27.13 0.140 1.10 429 63 66 3 14.0 89.98 0.150 1.20 442 69 70

20.0 52.88 0.140 1.10 448 65 65 17.5 29.12 0.150 1.20 432 63 65 17.5 92.02 0.150 1.20 442 69 70

4 24.0 55.13 0.130 1.05 448 66 66 4 21.0 31.13 0.140 1.10 432 63 65 4 21.0 94.09 0.140 1.10 442 69 70

28.0 57.33 0.130 1.00 450 67 66 24.5 33.12 0.150 1.20 433 63 65 24.5 96.09 0.140 1.10 442 69 70

5 32.0 59.52 0.140 1.10 450 67 66 5 28.0 35.14 0.160 1.25 433 63 65 5 28.0 98.07 0.140 1.10 444 69 70

36.0 61.77 0.130 1.00 452 67 66 31.5 37.26 0.140 1.10 434 63 65 31.5 100.08 0.140 1.10 443 69 70

6 40.0 63.98 0.120 0.95 450 68 67 6 35.0 39.22 0.140 1.10 430 64 65 6 35.0 102.12 0.140 1.10 440 69 70

44.0 66.11 0.130 1.05 450 68 68 38.5 41.16 0.140 1.10 427 64 65 38.5 104.12 0.140 1.10 440 69 70

P2-1 48.0 68.26 0.140 1.10 447 68 68 P2-1 42.0 43.14 0.140 1.10 429 62 65 P2-1 42.0 106.07 0.160 1.25 434 68 70

52.0 70.43 0.140 1.10 447 68 67 45.5 45.10 0.140 1.10 429 62 65 45.5 108.19 0.160 1.25 440 68 70

2 56.0 72.68 0.120 0.95 447 68 67 2 49.0 47.08 0.130 1.00 428 62 65 2 49.0 110.38 0.140 1.10 439 68 70

60.0 74.81 0.120 0.95 447 68 67 52.5 49.02 0.120 0.95 428 62 65 52.5 112.38 0.140 1.10 440 68 69

3 64.0 76.94 0.110 0.87 447 69 67 3 56.0 50.87 0.120 0.95 428 62 65 3 56.0 114.39 0.130 1.00 439 67 69

68.0 78.98 0.110 0.87 448 68 68 59.5 52.72 0.120 0.95 428 62 65 59.5 116.32 0.130 1.00 439 67 69

4 72.0 81.02 0.110 0.87 448 68 68 4 63.0 54.56 0.120 0.95 428 61 64 4 63.0 118.26 0.130 1.00 439 67 69

76.0 83.04 0.110 0.87 452 68 68 66.5 56.40 0.130 1.00 428 60 64 66.5 120.17 0.130 1.00 441 66 69

5 80.0 85.09 0.130 1.00 456 68 68 5 70.0 58.31 0.140 1.20 428 60 64 5 70.0 122.08 0.140 1.10 441 66 69

84.0 87.28 0.130 1.00 456 68 68 73.5 60.28 0.140 1.10 432 60 63 73.5 124.10 0.140 1.10 443 64 68

6 88.0 89.51 0.130 1.00 452 68 68 6 77.0 62.27 0.150 1.15 430 60 63 6 77.0 126.18 0.140 1.10 440 64 68

92.0 91.69 0.130 1.00 450 68 68 80.5 64.35 0.150 1.20 427 60 63 80.5 128.14 0.140 1.10 439 63 67

P3-1 96.0 93.88 0.120 0.95 450 68 68 P3-1 84.0 66.30 0.140 1.10 427 60 63 P3-1 84.0 130.07 0.140 1.10 435 63 67

100.0 95.95 0.130 1.05 450 67 67 87.5 68.27 0.140 1.10 425 59 63 87.5 132.03 0.140 1.10 436 63 66

2 104.0 98.15 0.110 0.87 448 67 67 2 91.0 70.23 0.120 0.95 425 59 63 2 91.0 134.01 0.120 0.94 433 63 66

108.0 100.20 0.110 0.87 448 67 67 94.5 72.08 0.120 0.95 425 59 63 94.5 135.86 0.120 0.94 434 63 66

3 112.0 102.24 0.100 0.79 447 67 67 3 98.0 73.94 0.110 0.87 422 58 62 3 98.0 137.71 0.120 0.94 433 64 66

116.0 104.21 0.100 0.79 447 67 67 101.5 75.72 0.110 0.87 422 59 62 101.5 139.52 0.120 0.94 433 64 66

4 120.0 106.12 0.100 0.79 447 67 67 4 105.0 77.49 0.110 0.87 422 58 62 4 105.0 141.36 0.120 0.94 432 63 66

124.0 108.07 0.100 0.79 451 67 67 108.5 79.28 0.110 0.87 424 58 62 108.5 143.19 0.120 0.94 436 63 66

5 128.0 110.01 0.110 0.87 454 67 67 5 112.0 81.04 0.120 0.95 424 58 62 5 112.0 145.06 0.120 0.94 436 63 66

132.0 112.07 0.110 0.87 454 67 67 115.5 82.88 0.120 0.95 424 58 62 115.5 146.89 0.120 0.94 441 64 66

6 136.0 114.14 0.100 0.79 450 67 67 6 119.0 84.70 0.140 1.10 422 60 62 6 119.0 148.72 0.130 1.00 441 64 66

140.0 116.10 0.100 0.79 450 68 67 122.5 86.66 0.150 1.20 420 59 62 122.5 150.62 0.130 1.00 441 64 66

P4-1 144.0 118.11 0.140 1.11 450 68 68 P4-1 126.0 88.71 0.150 1.20 422 63 62 P4-1 126.0 152.45 0.140 1.10 440 64 66

148.0 120.21 0.150 1.20 447 68 68 129.5 90.71 0.140 1.10 422 60 62 129.5 154.46 0.140 1.10 436 64 66

2 152.0 122.57 0.130 1.05 443 67 68 2 133.0 92.66 0.140 1.10 419 60 62 2 133.0 156.46 0.130 1.00 436 63 66

156.0 124.86 0.130 1.05 443 67 67 136.5 94.67 0.140 1.10 419 60 62 136.5 158.39 0.130 1.00 433 63 65

3 160.0 127.03 0.110 0.87 443 67 67 3 140.0 96.66 0.130 1.05 419 60 62 3 140.0 160.31 0.120 0.95 433 63 65

164.0 129.07 0.120 0.96 441 67 68 143.5 98.55 0.130 1.05 418 60 62 143.5 162.15 0.120 0.95 433 63 65

4 168.0 131.19 0.120 0.96 444 67 68 4 147.0 100.49 0.120 0.95 421 61 62 4 147.0 164.02 0.110 0.87 434 63 65

172.0 133.34 0.120 0.95 443 67 67 150.5 102.30 0.120 0.95 422 61 62 150.5 165.80 0.110 0.87 436 63 65

5 176.0 135.48 0.120 0.95 443 67 67 5 154.0 104.14 0.120 0.95 422 61 62 5 154.0 167.61 0.110 0.87 436 63 65

180.0 137.63 0.120 0.95 446 67 67 157.5 105.98 0.120 0.95 425 61 62 157.5 169.36 0.110 0.86 439 63 65

6 184.0 139.76 0.120 0.95 446 67 67 6 161.0 107.81 0.120 0.95 422 61 62 6 161.0 171.13 0.100 0.80 435 63 65

188.0 141.86 0.120 0.96 440 67 67 164.5 109.66 0.120 0.95 422 61 62 164.5 172.82 0.100 0.80 435 63 65

P5-1 192.0 143.86 0.150 1.20 440 67 67 P5-1 168.0 111.43 0.170 1.35 420 61 62 P5-1 168.0 174.52 0.150 1.20 435 63 65

196.0 146.18 0.150 1.20 440 67 67 171.5 113.46 0.170 1.35 421 62 63 171.5 176.60 0.160 1.25 435 63 65

2 200.0 148.54 0.150 1.20 440 67 67 2 175.0 115.61 0.160 1.25 420 61 63 2 175.0 178.76 0.140 1.10 435 63 65

204.0 150.92 0.150 1.20 435 67 67 178.5 117.68 0.170 1.35 417 61 63 178.5 180.78 0.150 1.20 435 63 65

3 208.0 153.31 0.130 1.05 434 67 67 3 182.0 119.89 0.140 1.10 417 61 63 3 182.0 182.83 0.120 0.95 435 63 65

212.0 155.53 0.130 1.05 433 67 67 185.5 121.81 0.140 1.10 416 61 63 185.5 184.65 0.120 0.95 430 63 65

4 216.0 157.70 0.140 1.13 435 67 67 4 189.0 123.79 0.140 1.10 417 61 63 4 189.0 186.51 0.130 1.05 430 63 65

220.0 159.99 0.140 1.12 435 67 67 192.5 125.80 0.150 1.20 418 61 63 192.5 188.45 0.130 1.05 433 63 65

5 224.0 162.35 0.150 1.20 434 67 67 5 196.0 127.87 0.160 1.30 418 61 63 5 196.0 190.31 0.130 1.05 433 63 65

228.0 164.65 0.150 1.20 434 67 67 199.5 130.08 0.150 1.20 417 62 63 199.5 192.25 0.130 1.05 431 63 65

6 232.0 167.06 0.130 1.05 434 67 67 6 203.0 132.13 0.130 1.05 415 62 63 6 203.0 194.20 0.110 0.87 431 63 65

236.0 169.44 0.130 1.05 430 67 67 206.5 134.03 0.140 1.10 415 62 63 206.5 195.96 0.110 0.87 431 63 65

240.0 171.67 210.0 136.03 210.0 197.76

Input2
123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls

LEHDER Environmental Services Ltd

Point by Point Calculations

Company: Owens Corning 

Plant: Delmar NY

Stack: DM1 DEP Outlet 

Pollutant: Hexavalent/Total Chromium

Project No.:123987

Data Entry: KH / JE

Point Period Isokinecity Point Period Isokinecity Point Time Isokinecity

min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s %

P1-1 4.0 0.066 2.32 8.5 27.8 94.1 P1-1 3.5 0.059 2.10 8.4 27.4 95.9 P1-1 3.5 0.059 2.10 8.7 28.4 93.9

4.0 0.071 2.52 8.8 28.7 99.3 3.5 0.062 2.19 8.6 28.3 97.3 3.5 0.063 2.23 8.7 28.5 100.0

2 4.0 0.066 2.32 7.9 26.1 101.1 2 3.5 0.058 2.04 8.1 26.5 97.0 2 3.5 0.059 2.10 8.1 26.7 99.9

4.0 0.064 2.25 7.9 26.1 97.9 3.5 0.060 2.13 8.4 27.4 98.0 3.5 0.059 2.09 8.2 26.8 99.7

3 4.0 0.063 2.23 7.7 25.1 100.4 3 3.5 0.057 2.02 7.8 25.6 99.0 3 3.5 0.059 2.07 8.2 26.8 98.6

4.0 0.064 2.27 7.9 26.1 98.8 3.5 0.057 2.03 8.1 26.5 96.4 3.5 0.059 2.09 8.2 26.8 99.6

4 4.0 0.063 2.23 7.7 25.1 100.5 4 3.5 0.057 2.01 7.8 25.6 99.0 4 3.5 0.057 2.02 7.9 25.8 99.8

4.0 0.063 2.21 7.7 25.2 99.5 3.5 0.058 2.04 8.1 26.5 97.2 3.5 0.057 2.00 7.9 25.8 98.8

5 4.0 0.064 2.28 8.0 26.1 98.8 5 3.5 0.061 2.15 8.4 27.4 98.8 5 3.5 0.058 2.03 7.9 25.9 100.4

4.0 0.063 2.24 7.7 25.2 101.0 3.5 0.056 1.98 7.8 25.7 97.6 3.5 0.058 2.07 7.9 25.9 101.9

6 4.0 0.061 2.16 7.4 24.2 100.8 6 3.5 0.056 1.97 7.8 25.6 96.6 6 3.5 0.057 2.03 7.9 25.8 100.0

4.0 0.062 2.18 7.7 25.2 97.7 3.5 0.057 2.00 7.8 25.6 98.1 3.5 0.056 1.97 7.9 25.8 97.0

P2-1 4.0 0.062 2.20 7.9 26.1 94.9 P2-1 3.5 0.056 1.98 7.8 25.6 97.4 P2-1 3.5 0.061 2.15 8.4 27.5 98.9

4.0 0.064 2.27 7.9 26.1 98.2 3.5 0.057 2.00 7.8 25.6 98.2 3.5 0.063 2.22 8.4 27.6 102.3

2 4.0 0.061 2.16 7.4 24.1 100.6 2 3.5 0.056 1.97 7.5 24.6 100.3 2 3.5 0.057 2.02 7.9 25.8 99.5

4.0 0.061 2.16 7.4 24.1 100.6 3.5 0.053 1.87 7.2 23.7 99.0 3.5 0.058 2.03 7.9 25.8 100.4

3 4.0 0.058 2.07 7.0 23.1 100.6 3 3.5 0.053 1.88 7.2 23.7 99.5 3 3.5 0.055 1.96 7.6 24.9 100.3

4.0 0.058 2.07 7.0 23.1 100.6 3.5 0.053 1.86 7.2 23.7 98.7 3.5 0.056 1.96 7.6 24.9 100.6

4 4.0 0.058 2.05 7.0 23.1 99.9 4 3.5 0.053 1.86 7.2 23.7 98.9 4 3.5 0.055 1.93 7.6 24.9 99.0

4.0 0.059 2.08 7.1 23.2 101.3 3.5 0.055 1.93 7.5 24.6 98.5 3.5 0.055 1.93 7.6 24.9 99.0

5 4.0 0.063 2.22 7.7 25.2 99.8 5 3.5 0.056 1.99 7.8 25.6 98.2 5 3.5 0.058 2.05 7.9 25.8 101.4

4.0 0.064 2.26 7.7 25.2 101.6 3.5 0.057 2.01 7.8 25.6 99.5 3.5 0.059 2.10 7.9 25.9 104.3

6 4.0 0.062 2.21 7.7 25.2 99.1 6 3.5 0.060 2.11 8.1 26.5 100.4 6 3.5 0.056 1.98 7.9 25.8 98.4

4.0 0.063 2.21 7.7 25.2 99.3 3.5 0.056 1.98 8.1 26.5 94.2 3.5 0.055 1.96 7.9 25.8 97.3

P3-1 4.0 0.059 2.10 7.4 24.2 98.1 P3-1 3.5 0.056 1.99 7.8 25.6 98.2 P3-1 3.5 0.06 1.98 7.8 25.7 98.0

4.0 0.063 2.22 7.7 25.2 99.9 3.5 0.056 1.98 7.8 25.5 97.4 3.5 0.06 2.01 7.9 25.8 99.7

2 4.0 0.059 2.08 7.0 23.1 101.5 2 3.5 0.053 1.88 7.2 23.6 99.8 2 3.5 0.05 1.87 7.3 23.8 100.1

4.0 0.058 2.07 7.0 23.1 100.8 3.5 0.053 1.88 7.2 23.6 100.1 3.5 0.05 1.87 7.3 23.8 100.2

3 4.0 0.056 1.99 6.7 22.0 101.8 3 3.5 0.051 1.80 6.9 22.6 99.8 3 3.5 0.05 1.83 7.3 23.8 97.9

4.0 0.055 1.94 6.7 22.0 99.2 3.5 0.051 1.80 6.9 22.6 99.7 3.5 0.05 1.86 7.3 23.8 99.5

4 4.0 0.056 1.97 6.7 22.0 100.7 4 3.5 0.051 1.81 6.9 22.6 100.6 4 3.5 0.05 1.85 7.3 23.8 98.7

4.0 0.056 1.97 6.7 22.1 100.9 3.5 0.050 1.78 6.9 22.6 98.8 3.5 0.05 1.89 7.3 23.8 101.4

5 4.0 0.059 2.09 7.1 23.2 102.1 5 3.5 0.053 1.87 7.2 23.6 99.4 5 3.5 0.05 1.86 7.3 23.8 99.5

4.0 0.059 2.10 7.1 23.2 102.6 3.5 0.052 1.84 7.2 23.6 98.1 3.5 0.05 1.85 7.3 23.9 99.1

6 4.0 0.056 1.98 6.7 22.1 101.7 6 3.5 0.056 1.98 7.8 25.5 97.3 6 3.5 0.05 1.93 7.6 24.9 99.4

4.0 0.057 2.03 6.7 22.1 103.9 3.5 0.059 2.08 8.0 26.4 98.6 3.5 0.05 1.85 7.6 24.9 95.5

P4-1 4.0 0.060 2.13 8.0 26.1 92.0 P4-1 3.5 0.057 2.02 8.0 26.4 95.9 P4-1 3.5 0.06 2.03 7.9 25.8 101.1

4.0 0.068 2.39 8.2 27.0 99.9 3.5 0.056 1.98 7.8 25.5 97.3 3.5 0.06 2.02 7.9 25.8 100.3

2 4.0 0.066 2.31 7.6 25.1 103.5 2 3.5 0.057 2.03 7.8 25.4 99.6 2 3.5 0.06 1.95 7.6 24.8 100.3

4.0 0.062 2.20 7.6 25.1 98.6 3.5 0.057 2.01 7.8 25.4 98.9 3.5 0.06 1.95 7.6 24.8 100.2

3 4.0 0.058 2.06 7.0 23.1 100.3 3 3.5 0.054 1.92 7.5 24.5 97.7 3 3.5 0.05 1.86 7.3 23.8 99.4

4.0 0.061 2.15 7.3 24.0 99.8 3.5 0.056 1.96 7.5 24.5 99.9 3.5 0.05 1.90 7.3 23.8 101.6

4 4.0 0.062 2.18 7.3 24.1 101.4 4 3.5 0.052 1.83 7.2 23.6 97.1 4 3.5 0.05 1.80 7.0 22.8 100.8

4.0 0.061 2.17 7.3 24.1 101.0 3.5 0.053 1.86 7.2 23.6 98.8 3.5 0.05 1.83 7.0 22.8 102.6

5 4.0 0.062 2.18 7.3 24.1 101.7 5 3.5 0.053 1.86 7.2 23.6 98.8 5 3.5 0.05 1.77 7.0 22.8 99.2

4.0 0.061 2.16 7.4 24.1 100.7 3.5 0.052 1.85 7.2 23.6 98.4 3.5 0.05 1.79 7.0 22.9 100.5

6 4.0 0.060 2.13 7.4 24.1 99.3 6 3.5 0.053 1.87 7.2 23.6 99.0 6 3.5 0.05 1.71 6.6 21.8 100.4

4.0 0.057 2.02 7.3 24.0 94.0 3.5 0.051 1.80 7.2 23.6 95.3 3.5 0.05 1.72 6.6 21.8 100.7

P5-1 4.0 0.067 2.35 8.2 26.9 97.8 P5-1 3.5 0.058 2.05 8.6 28.1 91.5 P5-1 3.5 0.06 2.11 8.1 26.6 101.2

4.0 0.068 2.39 8.2 26.9 99.7 3.5 0.061 2.17 8.6 28.1 96.6 3.5 0.06 2.19 8.4 27.5 101.6

2 4.0 0.068 2.40 8.2 26.9 100.1 2 3.5 0.059 2.10 8.3 27.2 96.3 2 3.5 0.06 2.04 7.8 25.7 101.2

4.0 0.069 2.42 8.2 26.8 100.5 3.5 0.063 2.24 8.5 28.0 99.4 3.5 0.06 2.08 8.1 26.6 99.5

3 4.0 0.064 2.25 7.6 24.9 100.2 3 3.5 0.055 1.94 7.7 25.4 95.1 3 3.5 0.05 1.84 7.3 23.8 98.7

4.0 0.062 2.20 7.6 24.9 97.9 3.5 0.057 2.00 7.7 25.4 97.8 3.5 0.05 1.89 7.2 23.8 100.9

4 4.0 0.066 2.32 7.9 25.9 99.6 4 3.5 0.058 2.03 7.7 25.4 99.5 4 3.5 0.06 1.96 7.5 24.7 100.9

4.0 0.068 2.39 7.9 25.9 102.7 3.5 0.059 2.10 8.0 26.3 99.1 3.5 0.05 1.88 7.6 24.8 96.6

5 4.0 0.066 2.33 8.2 26.8 96.9 5 3.5 0.063 2.24 8.3 27.2 102.7 5 3.5 0.06 1.96 7.6 24.8 101.0

4.0 0.069 2.43 8.2 26.8 101.1 3.5 0.059 2.07 8.0 26.3 97.8 3.5 0.06 1.98 7.5 24.8 101.7

6 4.0 0.068 2.41 7.6 24.9 107.6 6 3.5 0.055 1.93 7.5 24.5 97.7 6 3.5 0.05 1.78 6.9 22.8 99.5

4.0 0.064 2.25 7.6 24.9 100.2 3.5 0.057 2.02 7.7 25.4 98.8 3.5 0.05 1.82 6.9 22.8 101.6

Sample Volume Stack Velocity Sample Volume Stack Velocity Sample Volume Stack Velocity

Test #2

25-Jan-12

08:03 - 11:49

Test #3

26-Jan-12

07:52 - 11:22

Test #1

24-Jan-12

08:27 - 12:55

ISO-Velocity Calculations
123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls

Company: Owens Corning Pollutant: Hexavalent/Total Chromium

Plant: Delmar NY Method: EPA Method 0061

Stack: DM1 DEP Outlet Project No.: 123987

Reviewed by MD

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12 Average

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Hexavalent Chromium Concentration ug/S.m3 2.90E+00 2.95E+00 2.13E+00 2.66E+00

Hexavalent Chromium Mass Rate ug/s 1.11E+01 1.21E+01 8.43E+00 1.05E+01

mg/s 1.11E-02 1.21E-02 8.43E-03 1.05E-02

g/hr 4.00E-02 4.35E-02 3.03E-02 3.79E-02

lb./hr 8.82E-05 9.59E-05 6.68E-05 8.36E-05

Total Chromium Concentration ug/S.m3 4.13E+00 5.07E+00 5.42E+00 4.87E+00

Total Chromium Mass Rate ug/s 1.58E+01 2.08E+01 2.14E+01 1.94E+01

mg/s 1.58E-02 2.08E-02 2.14E-02 1.94E-02

g/hr 5.70E-02 7.49E-02 7.72E-02 6.97E-02

lb./hr 1.26E-04 1.65E-04 1.70E-04 1.54E-04

Effluent Characteristics

Area of Sample Plane m2 0.999 0.999 0.999 0.999

Area of Sample Plane ft2 10.758 10.758 10.758 10.758

Average Stack Temperature  ̊C 230 218 225 224

Average Stack Temperature (Ts)  ̊F 445 425 437 436

Average Stack Gas Pressure kPa 99.28 100.55 100.39 100.07

Average Stack Gas Pressure (Psa) in Hg 29.32 29.70 29.65 29.56

Average Stack Gas Velocity m/s 7.55 7.70 7.63 7.63

Average Stack Gas Velocity ft/min 1.49E+03 1.52E+03 1.50E+03 1.50E+03

Oxygen Concentration % vol 19.6 20.0 19.9 19.8

Carbon Dioxide Concentration % vol 4.9 4.7 4.8 4.8

Effluent Molecular Weight (dry) g/gmol 29.56 29.55 29.56 29.56

Effluent Molecular Weight (wet) g/gmol 28.27 28.39 28.28 28.31

Effluent Moisture Content % vol. 11.2 10.1 11.1 10.8

Dry Gas Fraction % vol. 88.8 89.9 88.9 89.2

Actual Effluent Flow Rate A.m3

/s 7.54 7.70 7.63 7.62

Actual Effluent Flow Rate Acfm 1.60E+04 1.63E+04 1.62E+04 1.62E+04

Reference Flow Rate (wet) S.m3

/s 4.31 4.56 4.45 4.44

Standard Flow Rate (wet) Scfm 9.14E+03 9.66E+03 9.43E+03 9.41E+03

Reference Flow Rate (dry) S.m3

/s (dry) 3.83 4.10 3.96 3.96

Standard Flow Rate (dry) Scfm (dry) 8.12E+03 8.69E+03 8.38E+03 8.40E+03

Sample Parameters

Sample Period min 240.0 210.0 210.0 220.0

Sample Period Hours 4.0 3.5 3.5 3.7

Sample Volume A.m3 3.735 3.361 3.331 3.476

Sample Volume acf 131.888 118.702 117.623 122.738

Hexavalent Chromium ug 10.8 10.1 7.2 9.3

Total Chromium ug 15.4 17.4 18.2 17.0

Dry Reference Sample Volume S.m3 3.717 3.421 3.358 3.499

Dry Standard Sample Volume Scf 131.27 120.81 118.57 123.55

Water Vapour Reference Volume S.m3 0.467 0.383 0.419 0.423

Water Vapour Reference Volume scf 16.48 13.53 14.80 14.94

Average Meter Temperature  ̊C 19 17 19 18

Average Meter Temperature  ̊F 67 62 66 65

Average Absolute Meter Pressure in Hg 29.72 30.12 30.05 29.96

Average Absolute Meter Pressure kPa 100.64 101.98 101.73 101.45

Average Delta P in H2O 0.13 0.14 0.13 0.13

Average Delta H in H2O 1.01 1.09 1.04 1.05

Average Sample Rate Lpm 15.6 16.0 15.9 15.8

Average Sample Rate cfm 0.55 0.57 0.56 0.56

Average Isokinetic Variation % 99.9 98.1 99.6 99.2

Measurement Parameter

LEHDER Environmental Services Ltd.

Emissions Calculations
123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls

LEHDER Environmental Services Ltd Mike Denomme

16-Feb-12

Company: Owens Corning 

Plant: Delmar NY

Stack: DM2 DEP Outlet 

Pollutant: Hexavalent / Total Chromium

Method: EPA Method 0061

Project No.: 123987

Operators RS / JH

Data Entry: KH / JE

Reviewed By: MD

Ref.Temperature: 68 deg. F

Ref. Pressure: 29.92 "Hg

Velocity Constant: 85.49

Molar Volume: 24.04 l/mol

Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

No. of Sample Points 30 30 30

Sample Time /Point min 8.0 7.0 7.0

Reading / Point min 4.0 3.5 3.5

Total Sample Time, min 240.0 210.0 210.0

Barometric Pressure, Pb "Hg 29.65 30.04 29.97

Stack Gauge Pressure, Pgauge "H2O -0.95 -0.88 -0.88

Absolute Stack Pressure, Ps "Hg 29.58 29.98 29.91

Pitot Tube Coefficient, Cp 0.781 0.781 0.781

Oxygen Content, O2 % 20.0 20.1 20.0

Carbon Dioxide Content, CO2 % 4.21 4.70 4.40

Carbon Monoxide Content, CO % 0.0 0.0 0.0

Nitrogen Content, N2 % 75.8 75.2 75.6

Condensate Collected, WH2O g 328.6 269.6 283.9

Nozzle Diameter, Dn in 0.3595 0.3595 0.3595

Initial DGM Reading ft3 224.486 511.998 778.121

Final DGM Reading ft3 360.941 624.817 892.535

DGM Unity, Y 0.9991 0.9991 0.9991

Stack Width ft 3.280 3.280 3.280

Stack Depth ft 3.280 3.280 3.280

Actual Volume of Dry Gas ft3 136.3322 112.7175 114.3110

Stack Area, As ft2 10.758 10.758 10.758

Hex Chromium Analysis

Uncorrected Chromium (Cr ) 6+ ug 145 133 97.0

Blank Correction ug 1.72 1.72 1.72

Corrected Hexavalent Chromium ug 143 131 95.3

Total Chromium Analysis

Total Chromium - (1) KOH & Rinses ug 162 153 115

Total Chromium - (3) Nitric Rinse ug 1.06 1.22 0.706

Total Chromium - (3) Column Filter ug 1.09 1.08 0.601

Uncorrected Total Chromium ug 164.2 155.3 116.3

Blank Correction (4) ug 3.14 3.14 3.14

Total Chromium (1 + 2 + 3) - 4 ug 161.0 152.2 113.2

Italics indicate values less than method detection

Input1
123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls

LEHDER Environmental Services Ltd

Point by Point Sampling Data

Company: Owens Corning 

Plant: Delmar NY

Stack: DM2 DEP Outlet

Pollutant: Hexavalent / Total Chromium

Project No.: 123987

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo

# min ft3 H2O H2O F F F # min ft3 H2O H2O F F F # min ft3 H2O H2O F F F

P1-1 0.0 224.49 0.140 1.21 420 67 68 P1-1 0.0 512.00 0.140 1.22 412 67 67 P1-1 0.0 778.12 0.135 1.18 412 70 70

4.0 226.82 0.140 1.22 412 67 68 3.5 514.08 0.135 1.18 410 66 67 3.5 780.13 0.140 1.23 412 68 70

2 8.0 229.22 0.135 1.18 412 66 68 2 7.0 516.09 0.130 1.13 411 65 67 2 7.0 782.13 0.120 1.06 406 68 70

12.0 231.54 0.135 1.18 406 65 67 10.5 518.04 0.120 1.05 405 64 67 10.5 784.00 0.120 1.06 406 68 70

3 16.0 233.84 0.120 1.05 407 65 67 3 14.0 519.90 0.110 0.96 406 64 67 3 14.0 785.85 0.110 0.97 407 68 70

20.0 236.03 0.120 1.05 408 65 67 17.5 521.68 0.120 1.05 406 64 66 17.5 787.65 0.110 0.97 408 68 70

4 24.0 238.20 0.135 1.18 407 66 67 4 21.0 523.53 0.130 1.14 406 64 66 4 21.0 789.42 0.135 1.18 412 68 70

28.0 240.50 0.135 1.18 413 66 67 24.5 525.46 0.130 1.14 408 64 66 24.5 791.40 0.135 1.18 412 68 70

5 32.0 242.78 0.140 1.22 413 66 67 5 28.0 527.41 0.135 1.18 409 64 66 5 28.0 793.37 0.135 1.18 413 68 70

36.0 245.14 0.140 1.22 414 66 67 31.5 529.35 0.130 1.13 409 63 66 31.5 795.36 0.135 1.18 414 68 70

6 40.0 247.49 0.120 1.06 405 67 67 6 35.0 531.32 0.110 0.97 397 63 66 6 35.0 797.29 0.130 1.14 413 68 70

44.0 249.65 0.120 1.06 405 67 67 38.5 533.17 0.110 0.97 397 65 66 38.5 799.27 0.130 1.14 413 68 70

P2-1 48.0 251.85 0.130 1.14 405 67 67 P2-1 42.0 534.95 0.120 1.05 405 64 66 P2-1 42.0 801.22 0.130 1.14 412 67 70

52.0 254.05 0.130 1.14 410 67 67 45.5 536.79 0.120 1.05 406 64 66 45.5 803.12 0.130 1.14 412 67 69

2 56.0 256.35 0.120 1.05 410 67 67 2 49.0 538.66 0.110 0.97 403 63 66 2 49.0 805.08 0.115 1.01 410 67 69

60.0 258.52 0.120 1.05 406 67 67 52.5 540.47 0.105 0.92 403 63 65 52.5 806.92 0.115 1.01 409 67 69

3 64.0 260.66 0.110 0.97 407 67 67 3 56.0 542.22 0.095 0.83 404 63 65 3 56.0 808.77 0.100 0.88 409 66 69

68.0 262.77 0.110 0.97 406 67 67 59.5 543.88 0.095 0.83 404 63 65 59.5 810.49 0.100 0.88 410 66 69

4 72.0 264.86 0.115 1.01 409 66 67 4 63.0 545.53 0.110 0.96 407 63 65 4 63.0 812.18 0.115 1.00 414 66 68

76.0 266.99 0.115 1.00 410 66 67 66.5 547.30 0.110 0.96 408 62 65 66.5 814.05 0.115 1.00 415 66 68

5 80.0 269.13 0.135 1.18 410 66 67 5 70.0 549.09 0.120 1.04 411 62 65 5 70.0 815.82 0.130 1.13 418 65 68

84.0 271.38 0.130 1.13 413 66 67 73.5 550.94 0.120 1.04 411 62 64 73.5 817.76 0.130 1.12 419 65 68

6 88.0 273.64 0.140 1.22 416 66 67 6 77.0 552.79 0.120 1.04 413 62 64 6 77.0 819.68 0.130 1.12 422 65 67

92.0 275.94 0.140 1.21 417 66 66 80.5 554.65 0.120 1.04 413 62 64 80.5 821.60 0.130 1.12 423 64 67

P3-1 96.0 278.27 0.110 0.96 407 65 67 P3-1 84.0 556.53 0.120 1.05 406 62 64 P3-1 84.0 823.45 0.120 1.04 412 64 67

100.0 280.35 0.130 1.14 406 65 66 87.5 558.38 0.120 1.05 406 62 64 87.5 825.30 0.120 1.04 412 64 66

2 104.0 282.53 0.110 0.97 404 65 66 2 91.0 560.22 0.100 0.87 404 62 64 2 91.0 827.15 0.100 0.87 410 64 66

108.0 284.62 0.110 0.97 404 65 66 94.5 561.92 0.095 0.83 404 62 64 94.5 828.85 0.100 0.87 411 64 66

3 112.0 286.77 0.110 0.97 403 65 66 3 98.0 563.58 0.090 0.78 405 61 64 3 98.0 830.54 0.100 0.87 412 65 66

116.0 288.85 0.100 0.88 405 65 66 101.5 565.18 0.090 0.78 405 61 63 101.5 832.25 0.100 0.87 412 65 66

4 120.0 290.84 0.120 1.05 408 65 66 4 105.0 566.78 0.100 0.87 408 61 63 4 105.0 833.93 0.110 0.95 416 65 66

124.0 292.91 0.115 1.01 408 66 66 108.5 568.45 0.100 0.87 409 61 63 108.5 835.70 0.110 0.95 418 64 66

5 128.0 295.05 0.130 1.13 413 66 66 5 112.0 570.15 0.125 1.08 412 61 63 5 112.0 837.48 0.125 1.07 423 65 66

132.0 297.19 0.140 1.22 415 66 66 115.5 572.03 0.130 1.12 415 61 63 115.5 839.35 0.125 1.07 424 65 66

6 136.0 299.50 0.140 1.21 418 66 66 6 119.0 573.92 0.130 1.11 420 61 63 6 119.0 841.21 0.130 1.11 425 65 66

140.0 301.77 0.140 1.21 418 67 67 122.5 575.85 0.130 1.11 420 61 63 122.5 843.09 0.130 1.11 426 65 66

P4-1 144.0 304.02 0.170 1.48 412 67 67 P4-1 126.0 577.73 0.120 1.05 405 63 63 P4-1 126.0 844.94 0.150 1.29 422 65 66

148.0 306.45 0.170 1.48 415 66 67 129.5 579.58 0.140 1.21 412 62 63 129.5 846.99 0.150 1.29 422 65 66

2 152.0 308.87 0.140 1.25 412 66 67 2 133.0 581.58 0.110 0.95 411 62 63 2 133.0 849.05 0.120 1.04 419 65 66

156.0 311.23 0.140 1.22 410 66 66 136.5 583.39 0.110 0.95 411 62 63 136.5 850.92 0.120 1.04 419 65 66

3 160.0 313.49 0.130 1.13 411 66 66 3 140.0 585.16 0.105 0.91 412 61 63 3 140.0 852.76 0.115 0.99 421 64 66

164.0 315.70 0.120 1.05 412 66 66 143.5 586.88 0.105 0.91 413 61 63 143.5 854.58 0.115 0.99 421 64 66

4 168.0 317.83 0.140 1.21 417 66 66 4 147.0 588.61 0.120 1.03 416 61 63 4 147.0 856.40 0.120 1.03 422 64 66

172.0 320.09 0.140 1.21 416 66 66 150.5 590.46 0.120 1.03 417 61 63 150.5 858.24 0.120 1.03 424 64 65

5 176.0 322.38 0.150 1.29 420 66 66 5 154.0 592.32 0.140 1.20 422 62 63 5 154.0 860.08 0.135 1.15 431 64 65

180.0 324.75 0.150 1.29 421 66 66 157.5 594.29 0.140 1.19 425 61 63 157.5 862.02 0.140 1.19 431 64 65

6 184.0 327.15 0.145 1.25 421 66 66 6 161.0 596.31 0.140 1.19 427 61 63 6 161.0 864.00 0.140 1.19 434 64 65

188.0 329.51 0.145 1.24 426 65 66 164.5 598.22 0.140 1.19 427 61 63 164.5 865.99 0.140 1.18 435 64 65

P5-1 192.0 331.86 0.160 1.37 426 65 66 P5-1 168.0 600.16 0.160 1.36 427 62 63 P5-1 168.0 867.91 0.160 1.36 433 64 65

196.0 334.33 0.170 1.46 425 65 66 171.5 602.24 0.165 1.40 427 62 63 171.5 870.05 0.165 1.40 435 64 65

2 200.0 336.87 0.160 1.38 423 66 66 2 175.0 604.41 0.160 1.36 426 62 63 2 175.0 872.19 0.155 1.32 431 64 65

204.0 339.35 0.160 1.38 423 66 66 178.5 606.55 0.155 1.32 426 62 63 178.5 874.30 0.155 1.32 430 64 65

3 208.0 341.82 0.160 1.38 423 66 66 3 182.0 608.62 0.155 1.32 427 62 63 3 182.0 876.43 0.150 1.28 431 64 65

212.0 344.25 0.155 1.33 424 66 66 185.5 610.71 0.155 1.32 427 62 63 185.5 878.40 0.150 1.28 431 64 65

4 216.0 346.68 0.160 1.37 428 66 66 4 189.0 612.79 0.155 1.32 428 62 63 4 189.0 880.41 0.155 1.31 436 64 65

220.0 349.12 0.160 1.37 429 66 66 192.5 614.85 0.155 1.31 430 62 63 192.5 882.42 0.155 1.31 437 64 65

5 224.0 351.59 0.160 1.36 432 66 66 5 196.0 616.93 0.150 1.27 431 62 63 5 196.0 884.51 0.155 1.30 440 64 65

228.0 354.05 0.155 1.32 432 66 66 199.5 618.98 0.150 1.27 432 62 63 199.5 886.55 0.155 1.30 441 64 65

6 232.0 356.40 0.140 1.19 430 66 66 6 203.0 620.99 0.140 1.19 429 62 63 6 203.0 888.63 0.145 1.22 440 64 65

236.0 358.68 0.140 1.19 430 66 66 206.5 622.95 0.140 1.19 428 62 63 206.5 890.60 0.145 1.22 439 64 65

240.0 360.94 210.0 624.82 210.0 892.54

Input2
123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls

LEHDER Environmental Services Ltd

Point by Point Calculations

Company: Owens Corning 

Plant: Delmar NY

Stack: DM2 DEP Outlet 

Pollutant: Hexavalent / Total Chromium

Project No.:123987

Data Entry: KH / JE

Point Period Isokinecity Point Period Isokinecity Point Time Isokinecity

min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s % min m3 ft3 m/s ft/s %

P1-1 4.0 0.066 2.33 7.8 25.6 100.6 P1-1 3.5 0.059 2.08 7.7 25.3 102.5 P1-1 3.5 0.057 2.01 7.6 24.9 100.5

4.0 0.068 2.40 7.8 25.5 102.9 3.5 0.057 2.01 7.6 24.8 101.0 3.5 0.056 1.99 7.7 25.4 98.2

2 4.0 0.066 2.31 7.6 25.0 101.2 2 3.5 0.055 1.95 7.4 24.4 99.9 2 3.5 0.053 1.87 7.1 23.4 99.3

4.0 0.065 2.30 7.6 25.0 100.6 3.5 0.053 1.86 7.1 23.3 99.2 3.5 0.052 1.84 7.1 23.4 97.7

3 4.0 0.062 2.19 7.2 23.5 101.3 3 3.5 0.050 1.78 6.8 22.3 99.0 3 3.5 0.051 1.80 6.8 22.4 99.6

4.0 0.061 2.17 7.2 23.6 100.4 3.5 0.052 1.85 7.1 23.3 98.6 3.5 0.050 1.77 6.8 22.4 98.3

4 4.0 0.065 2.30 7.6 25.0 100.4 4 3.5 0.055 1.93 7.4 24.3 98.8 4 3.5 0.056 1.98 7.6 24.9 99.2

4.0 0.065 2.28 7.6 25.1 100.0 3.5 0.055 1.94 7.4 24.3 99.7 3.5 0.056 1.97 7.6 24.9 98.6

5 4.0 0.067 2.36 7.8 25.5 101.5 5 3.5 0.055 1.94 7.6 24.8 97.9 5 3.5 0.056 1.99 7.6 24.9 100.1

4.0 0.066 2.34 7.8 25.5 100.9 3.5 0.056 1.97 7.4 24.3 101.0 3.5 0.055 1.93 7.6 24.9 96.9

6 4.0 0.061 2.16 7.2 23.5 99.9 6 3.5 0.052 1.85 6.8 22.2 102.7 6 3.5 0.056 1.97 7.5 24.4 101.0

4.0 0.062 2.20 7.2 23.5 101.6 3.5 0.050 1.78 6.8 22.2 98.4 3.5 0.055 1.95 7.5 24.4 99.9

P2-1 4.0 0.062 2.20 7.5 24.5 97.7 P2-1 3.5 0.052 1.84 7.1 23.3 97.8 P2-1 3.5 0.054 1.90 7.4 24.4 97.2

4.0 0.065 2.30 7.5 24.5 102.2 3.5 0.053 1.87 7.1 23.3 99.8 3.5 0.055 1.95 7.4 24.4 100.1

2 4.0 0.061 2.17 7.2 23.6 100.6 2 3.5 0.051 1.80 6.8 22.3 100.4 2 3.5 0.052 1.84 7.0 23.0 100.3

4.0 0.060 2.13 7.2 23.5 98.7 3.5 0.050 1.75 6.6 21.8 99.7 3.5 0.052 1.84 7.0 22.9 100.2

3 4.0 0.060 2.11 6.9 22.5 102.0 3 3.5 0.047 1.67 6.3 20.7 100.0 3 3.5 0.049 1.72 6.5 21.4 100.5

4.0 0.059 2.09 6.9 22.5 100.7 3.5 0.047 1.64 6.3 20.7 98.6 3.5 0.048 1.68 6.5 21.4 98.3

4 4.0 0.060 2.12 7.0 23.1 100.5 4 3.5 0.050 1.77 6.8 22.3 98.7 4 3.5 0.053 1.87 7.0 23.0 102.3

4.0 0.061 2.14 7.0 23.1 101.3 3.5 0.051 1.79 6.8 22.4 100.0 3.5 0.050 1.77 7.0 23.0 96.6

5 4.0 0.064 2.25 7.6 25.0 98.6 5 3.5 0.052 1.84 7.1 23.4 98.9 5 3.5 0.055 1.94 7.5 24.5 99.9

4.0 0.064 2.26 7.5 24.6 100.8 3.5 0.052 1.85 7.1 23.4 99.3 3.5 0.054 1.91 7.5 24.5 98.7

6 4.0 0.065 2.30 7.8 25.6 99.1 6 3.5 0.053 1.86 7.1 23.4 100.1 6 3.5 0.054 1.92 7.5 24.6 99.5

4.0 0.066 2.33 7.8 25.6 100.5 3.5 0.053 1.87 7.1 23.4 100.7 3.5 0.052 1.85 7.5 24.6 95.7

P3-1 4.0 0.059 2.08 6.9 22.5 100.6 P3-1 3.5 0.052 1.85 7.1 23.3 99.0 P3-1 3.5 0.05 1.85 7.2 23.5 99.2

4.0 0.062 2.17 7.5 24.5 96.8 3.5 0.052 1.84 7.1 23.3 98.7 3.5 0.05 1.85 7.2 23.5 98.9

2 4.0 0.059 2.09 6.9 22.5 101.2 2 3.5 0.048 1.69 6.5 21.3 99.2 2 3.5 0.05 1.70 6.5 21.4 99.6

4.0 0.061 2.14 6.9 22.5 103.6 3.5 0.047 1.66 6.3 20.7 99.9 3.5 0.05 1.69 6.5 21.4 99.2

3 4.0 0.059 2.08 6.9 22.5 100.7 3 3.5 0.045 1.59 6.2 20.2 98.5 3 3.5 0.05 1.71 6.5 21.4 100.0

4.0 0.056 1.99 6.5 21.5 100.9 3.5 0.045 1.60 6.2 20.2 99.2 3.5 0.05 1.68 6.5 21.4 98.6

4 4.0 0.058 2.06 7.2 23.6 95.8 4 3.5 0.047 1.66 6.5 21.3 97.8 4 3.5 0.05 1.76 6.9 22.5 98.7

4.0 0.061 2.14 7.0 23.1 101.5 3.5 0.048 1.70 6.5 21.3 100.0 3.5 0.05 1.78 6.9 22.6 100.2

5 4.0 0.061 2.14 7.5 24.6 95.6 5 3.5 0.053 1.88 7.3 23.9 99.0 5 3.5 0.05 1.87 7.3 24.1 98.7

4.0 0.065 2.31 7.8 25.5 99.5 3.5 0.054 1.89 7.4 24.4 98.1 3.5 0.05 1.86 7.4 24.1 98.2

6 4.0 0.064 2.27 7.8 25.6 98.0 6 3.5 0.055 1.93 7.5 24.5 100.2 6 3.5 0.05 1.88 7.5 24.6 97.4

4.0 0.064 2.25 7.8 25.6 97.1 3.5 0.053 1.87 7.5 24.5 97.3 3.5 0.05 1.85 7.5 24.6 96.1

P4-1 4.0 0.069 2.42 8.6 28.1 94.6 P4-1 3.5 0.052 1.85 7.1 23.3 99.0 P4-1 3.5 0.06 2.05 8.0 26.4 98.6

4.0 0.068 2.42 8.6 28.1 94.6 3.5 0.057 2.00 7.7 25.3 99.6 3.5 0.06 2.06 8.0 26.4 99.2

2 4.0 0.067 2.36 7.8 25.5 101.4 2 3.5 0.051 1.81 6.8 22.4 101.6 2 3.5 0.05 1.87 7.2 23.6 100.5

4.0 0.064 2.26 7.8 25.5 97.1 3.5 0.050 1.76 6.8 22.4 99.0 3.5 0.05 1.84 7.2 23.6 98.9

3 4.0 0.063 2.21 7.5 24.6 98.6 3 3.5 0.049 1.72 6.7 21.9 98.9 3 3.5 0.05 1.81 7.0 23.1 99.8

4.0 0.060 2.13 7.2 23.6 98.9 3.5 0.049 1.73 6.7 21.9 99.8 3.5 0.05 1.83 7.0 23.1 100.5

4 4.0 0.064 2.26 7.8 25.6 97.5 4 3.5 0.052 1.85 7.2 23.5 99.7 4 3.5 0.05 1.83 7.2 23.6 98.7

4.0 0.065 2.28 7.8 25.6 98.5 3.5 0.052 1.85 7.2 23.5 100.0 3.5 0.05 1.84 7.2 23.6 99.6

5 4.0 0.067 2.37 8.1 26.5 99.0 5 3.5 0.056 1.97 7.8 25.4 98.6 5 3.5 0.05 1.94 7.7 25.2 99.3

4.0 0.068 2.40 8.1 26.5 100.5 3.5 0.057 2.02 7.8 25.5 101.6 3.5 0.06 1.98 7.8 25.6 99.3

6 4.0 0.067 2.35 7.9 26.1 100.1 6 3.5 0.054 1.91 7.8 25.5 95.9 6 3.5 0.06 1.99 7.8 25.7 100.1

4.0 0.066 2.35 8.0 26.2 100.2 3.5 0.055 1.94 7.8 25.5 97.4 3.5 0.05 1.92 7.8 25.7 96.6

P5-1 4.0 0.070 2.47 8.4 27.5 100.4 P5-1 3.5 0.059 2.08 8.3 27.3 97.7 P5-1 3.5 0.06 2.13 8.4 27.4 100.4

4.0 0.072 2.54 8.6 28.3 100.1 3.5 0.061 2.17 8.4 27.7 100.5 3.5 0.06 2.14 8.5 27.9 99.2

2 4.0 0.070 2.47 8.4 27.4 100.2 2 3.5 0.060 2.13 8.3 27.2 100.1 2 3.5 0.06 2.11 8.2 27.0 100.9

4.0 0.070 2.47 8.4 27.4 100.0 3.5 0.059 2.07 8.2 26.8 98.9 3.5 0.06 2.13 8.2 27.0 101.6

3 4.0 0.069 2.43 8.4 27.4 98.4 3 3.5 0.059 2.09 8.2 26.8 99.6 3 3.5 0.06 1.97 8.1 26.5 95.6

4.0 0.069 2.43 8.2 27.0 100.2 3.5 0.059 2.08 8.2 26.8 99.1 3.5 0.06 2.01 8.1 26.5 97.3

4 4.0 0.069 2.44 8.4 27.5 99.1 4 3.5 0.058 2.07 8.2 26.8 98.7 4 3.5 0.06 2.01 8.2 27.0 96.3

4.0 0.070 2.47 8.4 27.5 100.4 3.5 0.059 2.08 8.2 26.9 99.3 3.5 0.06 2.09 8.2 27.1 100.1

5 4.0 0.070 2.46 8.4 27.6 100.1 5 3.5 0.058 2.05 8.1 26.5 99.6 5 3.5 0.06 2.04 8.3 27.1 97.9

4.0 0.066 2.35 8.3 27.1 97.2 3.5 0.057 2.00 8.1 26.5 97.5 3.5 0.06 2.07 8.3 27.1 99.5

6 4.0 0.064 2.27 7.9 25.8 98.9 6 3.5 0.056 1.96 7.8 25.5 98.6 6 3.5 0.06 1.97 8.0 26.2 97.8

4.0 0.064 2.26 7.9 25.8 98.5 3.5 0.053 1.87 7.8 25.5 93.9 3.5 0.05 1.94 8.0 26.2 96.0

Test #3

26-Jan-12

07:52 - 11:22

Test #1

24-Jan-12

08:27 - 12:55

Sample Volume Stack Velocity

Test #2

25-Jan-12

08:03 - 11:49

Sample Volume Stack Velocity Sample Volume Stack Velocity

ISO-Velocity Calculations
123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls

Company: Owens Corning Pollutant: Hexavalent / Total Chromium

Plant: Delmar NY Method: EPA Method 0061

Stack: DM2 DEP Outlet Project No.: 123987

Reviewed by MD

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12 Average

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Hexavalent Chromium Concentration ug/S.m3 3.72E+01 4.05E+01 2.92E+01 3.56E+01

Hexavalent Chromium Mass Rate ug/s 1.53E+02 1.60E+02 1.17E+02 1.43E+02

mg/s 1.53E-01 1.60E-01 1.17E-01 1.43E-01

g/hr 5.49E-01 5.77E-01 4.20E-01 5.16E-01

lb./hr 1.21E-03 1.27E-03 9.26E-04 1.14E-03

Total Chromium Concentration ug/S.m3 4.18E+01 4.69E+01 3.47E+01 4.11E+01

Total Chromium Mass Rate ug/s 1.71E+02 1.86E+02 1.39E+02 1.65E+02

mg/s 1.71E-01 1.86E-01 1.39E-01 1.65E-01

g/hr 6.17E-01 6.69E-01 4.99E-01 5.95E-01

lb./hr 1.36E-03 1.48E-03 1.10E-03 1.31E-03

Effluent Characteristics

Area of Sample Plane m2 0.999 0.999 0.999 0.999

Area of Sample Plane ft2 10.758 10.758 10.758 10.758

Average Stack Temperature  ̊C 212 212 216 213

Average Stack Temperature (Ts)  ̊F 414 414 420 416

Average Stack Gas Pressure kPa 100.15 101.49 101.25 100.96

Average Stack Gas Pressure (Psa) in Hg 29.58 29.98 29.91 29.82

Average Stack Gas Velocity m/s 7.65 7.27 7.45 7.46

Average Stack Gas Velocity ft/min 1.51E+03 1.43E+03 1.47E+03 1.47E+03

Oxygen Concentration % vol 20.0 20.1 20.0 20.0

Carbon Dioxide Concentration % vol 4.2 4.7 4.4 4.4

Effluent Molecular Weight (dry) g/gmol 29.5 29.6 29.5 29.5

Effluent Molecular Weight (wet) g/gmol 28.3 28.4 28.3 28.3

Effluent Moisture Content % vol. 10.2 10.0 10.4 10.2

Dry Gas Fraction % vol. 89.8 90.0 89.6 89.8

Actual Effluent Flow Rate A.m3

/s 7.65 7.27 7.44 7.45

Actual Effluent Flow Rate Acfm 1.62E+04 1.54E+04 1.58E+04 1.58E+04

Reference Flow Rate (wet) S.m3

/s 4.57 4.40 4.46 4.48

Standard Flow Rate (wet) Scfm 9.67E+03 9.32E+03 9.45E+03 9.48E+03

Reference Flow Rate (dry) S.m3

/s (dry) 4.10 3.96 4.00 4.02

Standard Flow Rate (dry) Scfm (dry) 8.68E+03 8.39E+03 8.47E+03 8.52E+03

Sample Parameters

Sample Period min 240.0 210.0 210.0 220.0

Sample Period Hours 4.0 3.5 3.5 3.7

Sample Volume A.m3 3.860 3.192 3.237 3.430

Sample Volume acf 136.332 112.717 114.311 121.120

Hexavalent Chromium ug 143 131 95 123

Total Chromium ug 161 152 113 142

Dry Reference Sample Volume S.m3 3.850 3.242 3.262 3.451

Dry Standard Sample Volume Scf 135.95 114.49 115.21 121.88

Water Vapour Reference Volume S.m3 0.439 0.360 0.379 0.393

Water Vapour Reference Volume scf 15.50 12.72 13.39 13.87

Average Meter Temperature  ̊C 19 17 19 18

Average Meter Temperature  ̊F 66 63 66 65

Average Absolute Meter Pressure in Hg 29.74 30.12 30.05 29.97

Average Absolute Meter Pressure kPa 100.68 101.98 101.75 101.47

Average Delta P in H2O 0.14 0.13 0.13 0.13

Average Delta H in H2O 1.18 1.08 1.11 1.12

Average Sample Rate Lpm 16.1 15.2 15.4 15.6

Average Sample Rate cfm 0.57 0.54 0.54 0.55

Average Isokinetic Variation % 99.7 99.4 99.0 99.4

Measurement Parameter

LEHDER Environmental Services Ltd.

Emissions Calculations
Appendix B 

Analytical Report 

B.1: Enthalpy PM Report 

B.2: Element One M29 Report 

B.3: Element One M0061 Report 
Appendix B.1 

Enthalpy PM Report 












Appendix B.2 

Element One M29 Report 
Enthalpy 

800 Capitola Dr., Ste. 1 

Durham, NC 27713 

Project Number: 123987 

Chromium 

 

EPA Method 29 Analysis 

 

Analytical Report 

18207

Element One, Inc. 

5022-C Wrightsville Av., Wilmington, NC 28403 el1 910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com

elementOne 

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SUMMARY OF RESULTS 
elementOne 

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Summary of Analysis 

DM2 - Front Half - Summary of Method 29 Metals Analysis 

DM2 DEP 

 Outlet-R1 

DM2 DEP 

Outlet-R2 

DM2 DEP 

 Outlet-R2 

DM2 DEP 

Outlet-R3 

e18207-1FH e18207-2FH e18207-2FH dup e18207-3FH 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Chromium 191 180 178 151 

DM2 - Back Half - Summary of Method 29 Metals Analysis 

DM2 DEP 

 Outlet-R1

DM2 DEP 

 Outlet-R2 

DM2 DEP 

 Outlet-R2 

DM2 DEP 

 Outlet-R3 

e18207-1BH e18207-2BH e18207-2BH dup e18207-3BH 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Chromium 0.751 0.924 0.923 1.13 

DM1 - Front Half - Summary of Method 29 Metals Analysis 

DM1 DEP 

 Outlet-R1 

DM1 DEP 

 Outlet-R2 

DM1 DEP 

 Outlet-R2 

DM1 DEP 

 Outlet-R3 

DM1&DM2 

 Blank 

e18207-4FH e18207-5FH e18207-5FH dup e18207-6FH e18207-7FH 

Element Total μg Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- --------------- 

Chromium 21.2 19.0 16.9 19.8 1.55 

DM1 - Back Half - Summary of Method 29 Metals Analysis 

DM1 DEP 

 Outlet-R1 

DM1 DEP 

 Outlet-R2 

DM1 DEP 

 Outlet-R2 

DM1 DEP 

 Outlet-R3 

DM1&DM2 

 Blank 

e18207-4BH e18207-5BH e18207-5BH dup e18207-6BH e18207-7BH 

Element Total μg Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- --------------- 

Chromium 0.644 0.641 0.597 0.425 0.424 

 
elementOne 

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ANALYTICAL NARRATIVE 
elementOne 

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Element One Analytical Narrative 

Client: Enthalpy Element One #: 18207 

Client ID: 123987/OC – Delmar Analyst: DBW 

Method: Method 29 Dates Received: 02/14/12 

Analytes: Cr Dates Analyzed: 02/20/12 

Summary of Analysis 

The Method 29 samples were digested, prepared, and analyzed according to 

Method 29 protocol. Samples were analyzed for total chromium on a 

PerkinElmer ELAN 6100 ICP-MS. 

Detection Limits 

The ICP-MS instrument reporting limit was 1.0μg/L for total chromium. 

Analysis QA/QC 

Duplicate analyses relative percent difference (RPD), spike sample recovery, and 

second source calibration verification data are summarized in the Quality Control 

Section. All QA/QC data was within the criteria of the method. 

Additional Comments 

The reported results have not been corrected for any blank values or spike 

recovery values. The ICP analysis of the Blank samples revealed detectable 

concentrations of chromium. 
elementOne 

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QUALITY CONTROL SUMMARY
elementOne 

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Summary of Quality Control Data 

Metals Duplicate Analysis RPD 

(Method 29 QC limits: < 20% for RPD)

DM2 DEP Outlet-R2 

Front Half 

DM2 DEP Outlet-R2 

Back Half 

DM1 DEP Outlet-R2 

Front Half 

DM1 DEP Outlet-R2 

Back Half 

Element RPD RPD RPD RPD ------------------ ----------------- ----------------- ----------------- ----------------- 

Chromium 1.2% 0.1% 12.0% 7.1% 

Metals Analysis Spike Recoveries 

(Method 29 QC limits: ±25% for Spike Recoveries)

DM2 DEP Outlet-R2 

Front Half 

DM2 DEP Outlet-R2 

Back Half 

DM1 DEP Outlet-R2 

Front Half 

DM1 DEP Outlet-R2 

Back Half 

Element Recovery Recovery Recovery Recovery ------------------ ----------------- ----------------- ----------------- ----------------- 

Chromium 97% 100% 95% 92% 

*See Analytical Narrative, page 12. 

Second Source Calibration Check Recoveries 

(Method 29 QC limits: ±10% for Second Source Continuing Check Standard*) 

Element 1 ppb 50 ppb 100 ppb* 250 ppb ----------------- ----------------- ----------------- ----------------- ----------------- 

Chromium 88% 91% 97% 100% 
elementOne 

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SAMPLE CUSTODY
elementOne 

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elementOne 

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ANALYTICAL DATA 
elementOne 

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Analytical Calculations 

MetalsElement Results (μg) =ICP Results (μg/L)*Dilution*Final Volume (L) 

WhereICP Results= Raw sample concentration (ppb)--ICP-Data Sheet

Dilution= Diluted Volume--ICP-MS Run Sheet

Aliquot 

Final Volume=FH=Final Volume (FV)--Sample Submission

 BH=Received Volume (BV).*Final Volume (FV)--Sample Submission

Aliquot (Used) 

 Combined Results=FH+BH 

MercuryMercury Results (μg) =CVAA Results (μg) *Final Volume (ml) 

 Aliquot (ml) 

WhereCVAA Results= Raw sample reading (μg)--Hg-Data Sheet

Aliquot= Sample Aliquot (Alq.)--Hg-Data Sheet

 

Final Volume=Final Volume (FV)*--Sample Submission

* With the exception of the BH fraction where- 

=Received Volume (BV)--Sample Submission
Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/L) – Sample Result (μg/L)) X100 

 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)--ICP-Data Sheet 

Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet

Spike Amount--ICP-MS Spike Table

Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/L) - Sample Result (μg/L)) X100 

 Average (μg/L)

WhereSample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data 

Sheet

Average=(Duplicate + Sample Results)

 2

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Appendix B.3 

Element One M0061 Report 
Enthalpy Analytical, Inc. 

800 Capitola Dr., Ste. 1 

Durham, NC 27713 

Project No: 123987

Total Chromium and Hexavalent Chromium 

EPA Method 0061 Analysis 

Analytical Report 

18118 

Element One, Inc. 

5022-C Wrightsville Av., Wilmington, NC 28403 el1 910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com

elementOne 

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SUMMARY OF RESULTS 
elementOne 

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Summary of Analysis 

DM2 DEP Outlet - Summary of Chromium (VI) Analysis 

123987-1-R1 123987-4-R2 123987-4-R2 123987-7-R3 

e18118-16 e18118-17 e18118-17 dup e18118-18

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Chromium(VI) 145 133 133 97.0 

Duplicate RPD, % 5.2% 4.8% 2.1% 0.3% 

Spike Recovery, % ------------ ------------ ------------ 107% 

*See Analytical Narrative, page 10. 

DM2 DEP Outlet - 0.1N HNO3 Rinse – 

Summary of Method 0061 Total Chromium Analysis 

123987-2-R1 123987-5-R2 123987-5-R2 123987-8-R3 

e1 Sample ID e18118-1 e18118-2 e18118-2 Dup e18118-3 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium 1.06 1.22 1.45 0.706 

DM2 DEP Outlet - Filter – 

Summary of Method 0061 Total Chromium Analysis 

123987-3-R1 123987-6-R2 123987-6-R2 123987-9-R3 

e1 Sample ID e18118-9 e18118-10 e18118-10 Dup e18118-11 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium 1.09 1.08 1.11 0.601 

DM2 DEP Outlet - 0.5M KOH – 

Summary of Method 0061 Total Chromium Analysis 

123987-1-R1 123987-4-R2 123987-4-R2 123987-7-R3 

e1 Sample ID e18118-16 e18118-17 e18118-17 dup e18118-18 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium 162 153 173 115 

*See Analytical Narrative, page 7. 
elementOne 

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Summary of Analysis 

DM1 DEP Outlet - Summary of Chromium (VI) Analysis 

123987-10-R1 123987-13-R2 123987-13-R2 123987-16-R3 

e18118-19 e18118-20 e18118-20 dup e18118-21

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Chromium(VI) 12.5 11.8 11.7 8.87 

Duplicate RPD, % 0.6% 0.5% 0.3% 1.1% 

Spike Recovery, % ------------ ------------ ------------ 108% 

*See Analytical Narrative, page 10. 

DM1 DEP Outlet - 0.1N HNO3 Rinse – 

Summary of Method 0061 Total Chromium Analysis 

123987-11-R1 123987-14-R2 123987-14-R2 123987-17-R3 

e1 Sample ID e18118-4 e18118-5 e18118-5 Dup e18118-6 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium 0.390 0.355 0.346 0.281 

DM1 DEP Outlet - Filter – 

Summary of Method 0061 Total Chromium Analysis 

123987-12-R1 123987-15-R2 123987-15-R2 123987-18-R3 

e1 Sample ID e18118-12 e18118-13 e18118-13 Dup e18118-14 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium 0.916 1.24 1.04 0.750 

DM1 DEP Outlet - 0.5M KOH – 

Summary of Method 0061 Total Chromium Analysis 

123987-10-R1 123987-13-R2 123987-13-R2 123987-16-R3 

e1 Sample ID e18118-19 e18118-20 e18118-20 dup e18118-21 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium 17.2 18.9 20.3 11.4 
elementOne 

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Summary of Analysis 

Blank - Summary of Chromium (VI) Analysis 

123987-19-KOH 123987-20-DI 

e18118-22KOH e18118-8DI 

Element Total μg Total μg ----------------- --------------- --------------- 

Chromium(VI) 1.72 < 0.04 

Duplicate RPD, % 5.1% NA 

Blank – Summary of Method 0061 Total Chromium Analysis 

123987-21 123987-20-DI 123987-22-RB 123987-19-KOH 

e1 Sample ID e18118-7 e18118-8 e18118-15 e18118-22KOH 

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Total Chromium < 0.2 < 0.2 0.593 3.14 
elementOne 

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ANALYTICAL NARRATIVE 
elementOne 

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Element One Analytical Narrative 

Client: Enthalpy Analytical, Inc. Element One #: 18118 

Client ID: 123987/O.C. Delmar Analyst: DBW & LAL 

Method: M0061 Dates Received: 02/01/12 

Analytes: Total Chromium & Chromium (VI) Dates Analyzed: 02/07 – 09/12 

Summary of Analysis

For Total Chromium analysis the Method 0061 samples were acidified with trace 

metals grade concentrated nitric acid and digested on a hotplate according to 

method protocol. Samples were analyzed for total chromium on a PerkinElmer 

ELAN 6100 ICP-MS. 

For Chromium VI analysis the samples were prepared and analyzed according to 

SW-846 Method 0061 protocol. Samples were analyzed for chromium (VI) using 

a Shimadzu 2010 HPLC unit and a Timberline RDR-1 Reaction Module. 

Detection Limits

The ICP-MS instrument reporting limit was 1.0μg/L for total chromium. 

The Shimadzu 2010 HPLC instrument detection limit for chromium (VI) was 

0.1μg/L. 

Analysis QA/QC 

Duplicate analyses relative percent difference (RPD) and spike sample recovery 

data are summarized with the results. All QA/QC data was within the criteria of 

the method. 

Additional Comments 

The reported results have not been corrected for any blank values or spike 

recovery values. Due to matrix interferences it was necessary to analyze all 

KOH fraction samples for chromium (VI) at a minimum two-fold dilution and for 

total chromium at a minimum five-fold dilution. 

*Ref page 4 and 5; the chromium (VI) result for samples 1007-2001-R1, 1007-2007-R3 

and 1007-B-119-RB were less than the Total Chromium result for those samples. The 

Total Chromium results are at the detection limit. 
elementOne 

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QUALITY CONTROL SUMMARY
elementOne 

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Summary of Quality Control Data 

0.1N HNO3 - Metals Duplicate Analysis RPD 

(Method 0061 QC limits: < 20% for RPD)

123987-5-R2 123987-14-R2 

Element RPD RPD ------------------ ----------------- ----------------- 

Total Chromium 16.9% 2.5% 

 

Filter - Metals Duplicate Analysis RPD 

(Method 0061 QC limits: < 20% for RPD)

123987-6-R2 123987-15-R2 

Element RPD RPD ------------------ ----------------- ----------------- 

Total Chromium 2.0% 17.2% 

0.5M KOH - Metals Duplicate Analysis RPD 

(Method 0061 QC limits: < 20% for RPD)

123987-4-R2 123987-13-R2 

Element RPD RPD ------------------ ----------------- ----------------- 

Total Chromium 12.3% 7.3% 
elementOne 

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Summary of Quality Control Data 

0.1N HNO3 - Metals Analysis Spike Recoveries 

(Method 0061 QC limits: ± 25% for Spike Recoveries.)

123987-8-R3 123987-17-R3 

Element Recovery Recovery ------------------ ----------------- ----------------- 

Total Chromium 118% 105% 

Filter - Metals Analysis Spike Recoveries 

(Method 0061 QC limits: ± 25% for Spike Recoveries.)

123987-9-R3 123987-18-R3 

Element Recovery Recovery ------------------ ----------------- ----------------- 

Total Chromium 123% 104% 

0.5M KOH - Metals Analysis Spike Recoveries 

(Method 0061 QC limits: ± 25% for Spike Recoveries.)

123987-7-R3 123987-16-R3 

Element Recovery Recovery ------------------ ----------------- ----------------- 

Total Chromium 115% 115% 

Second Source Calibration Check Recoveries 

(Method 0061 QC limits: ±10% for Second Source Continuing Check Standard*) 

Element 1 ppb 50 ppb 100 ppb* 250 ppb ----------------- ----------------- ----------------- ----------------- ----------------- 

Total Chromium 118% 110% 108% 99% 
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SAMPLE CUSTODY
elementOne 

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ANALYTICAL DATA 
elementOne 

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Analytical Calculations 

MetalsElement Results (μg) =ICP Results (μg/L)*Dilution*Beginning Volume (L) 

WhereICP Results= Raw sample concentration (ppb)--ICP-Data Sheet

Dilution= Diluted Volume--ICP-MS Run Sheet

Aliquot 

Beginning Volume= (BV)--Sample Submission

Cr (VI)- 

Total Cr+6 (ug) =Cr+6 Results (μg/L)*Dilution*Final Volume (mL)/1000 

WhereCr+6 Results= Raw sample concentration (ppb)—HPLC Data Sheet

Dilution= Diluted Volume—HPLC Data Sheet

Aliquot 

Final Volume--Sample Submission 
elementOne 

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Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/L) – Sample Result (μg/L)) X100 

 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)--ICP-Data Sheet 

Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet

Spike Amount--ICP-MS Spike Table

Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/L) - Sample Result (μg/L)) X100 

 Average (μg/L)

WhereSample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data 

Sheet

Average=(Duplicate + Sample Results)

 2
Appendix C 

Equipment Calibrations 
Dec. 14, 2011 (dgm 16)

LEHDER ENVIRONMENTAL SERVICES LIMITED

DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),

for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.

4) Record readings in outlined boxes below, other columns are automatically calculated.

INITIAL FINAL AVG (Pbar)

DATE: 14-Dec-11 METER SERIAL #: 16 BAROMETRIC PRESSURE (in Hg): 29.57 29.50 29.54 IF Y VARI

- - CRITICAL ORIFICE SET SERIAL #: 1477 ORIFICE SHOU

K' TESTED TEMPERATURES °F ELAPSED

FACTOR VACUUM DGM READINGS (FT3) AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN) DGM H (1) (2) 

ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) INITIAL FINAL INITIAL FINAL AVG  (in H2O) Vm (STD) Vcr (STD) 

1 0.4335 23.0 107.80 111.78 3.98 70 74 73 71 71 72 7 1.15 3.906 3.894 

16 2 0.4335 23.0 111.78 115.74 3.96 70 73 73 71 71 72 7 1.15 3.890 3.894 

3 0.4335 23.0 115.74 119.69 3.96 70 73 73 71 71 72 7 1.15 3.887 3.894 

AVG = 

1 0.5266 21.8 128.00 132.82 4.82 71 73 73 71 71 72 7 1.70 4.738 4.726 

19 2 0.5266 21.8 132.82 137.65 4.83 71 73 73 71 71 72 7 1.70 4.753 4.726 

3 0.5266 21.8 137.65 142.46 4.82 71 73 74 71 71 72 7 1.70 4.736 4.726 

.. AVG = 

1 0.6585 20.5 150.00 156.03 6.03 71 78 78 72 72 75 7 2.45 5.911 5.910 

24 2 0.6585 20.5 156.03 162.05 6.01 71 78 77 73 73 75 7 2.45 5.894 5.910 

3 0.6585 20.5 162.05 168.07 6.02 71 77 73 73 73 74 7 2.45 5.913 5.910 

AVG = 

AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 

AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko= 

dH@= 

(1) Vm (std) = K1 Vm Pbar + (H/13.6) = Net volume of gas sample passed through DGM, corrected to standard conditions

Tm K1 = 17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric)

Tm = Absolute DGM avg. temperature (oR - English, oK - Metric)

Pbar 

(2) Vcr (std) = K' Tamb = Volume of gas sample passed through the critical orifice, corrected to standard conditions

Tamb = Absolute ambient temperature (oR - English, oK - Metric) Calibration performed by: J.H

K' = Average K' factor from Critical Orifice Calibration

(3) Y = Vcr (std) = DGM calibration factor

Vm (std)

METER PART #:

ENVIRONMENTAL SUPP

USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, 

Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.

Unit #16
Jan 02, 2012 (dgm 10)

LEHDER ENVIRONMENTAL SERVICES LIMITED

DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),

for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.

4) Record readings in outlined boxes below, other columns are automatically calculated.

INITIAL FINAL AVG (Pbar)

DATE: 2-Jan-12 METER SERIAL #: 10 BAROMETRIC PRESSURE (in Hg): 29.86 29.88 29.87 IF Y VARI

- - CRITICAL ORIFICE SET SERIAL #: 1477 ORIFICE SHOU

K' TESTED TEMPERATURES °F ELAPSED

FACTOR VACUUM DGM READINGS (FT3) AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN) DGM H (1) (2) 

ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) INITIAL FINAL INITIAL FINAL AVG  (in H2O) Vm (STD) Vcr (STD) 

1 0.4335 19.2 84.20 88.11 3.91 72 71 71 71 71 71 7 1.00 3.892 3.931 

16 2 0.4335 19.1 88.20 92.11 3.91 71 71 71 71 71 71 7 1.00 3.892 3.935 

3 0.4335 19.0 92.30 96.21 3.91 71 71 71 71 71 71 7 1.00 3.887 3.935 

AVG = 

1 0.5266 17.9 25.90 31.33 5.43 71 72 71 71 71 71 8 1.55 5.409 5.462 

19 2 0.5266 17.9 31.60 36.34 4.74 72 71 71 71 71 71 7 1.55 4.724 4.775 

3 0.5266 17.9 36.50 41.24 4.74 72 71 71 71 71 71 7 1.55 4.722 4.775 

 AVG = 

1 0.6585 16.3 0.90 7.64 6.74 73 72 73 71 71 72 8 2.30 6.715 6.818 

24 2 0.6585 16.3 7.80 13.70 5.90 73 73 73 71 71 72 7 2.30 5.880 5.966 

3 0.6585 16.3 13.90 19.80 5.90 72 73 73 71 71 72 7 2.30 5.877 5.971 

AVG = 

AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 

AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko= 

dH@= 

(1) Vm (std) = K1 Vm Pbar + (H/13.6) = Net volume of gas sample passed through DGM, corrected to standard conditions

Tm K1 = 17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric)

Tm = Absolute DGM avg. temperature (oR - English, oK - Metric)

Pbar 

(2) Vcr (std) = K' Tamb = Volume of gas sample passed through the critical orifice, corrected to standard conditions

Tamb = Absolute ambient temperature (oR - English, oK - Metric) Calibration performed by: J.D

K' = Average K' factor from Critical Orifice Calibration

(3) Y = Vcr (std) = DGM calibration factor

Vm (std)

METER PART #:

ENVIRONMENTAL SUPP

USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, 

Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.

Unit #10
Feb.13, 2012 (dgm 16).xls

LEHDER ENVIRONMENTAL SERVICES LIMITED

DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),

for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.

4) Record readings in outlined boxes below, other columns are automatically calculated.

INITIAL FINAL AVG (Pbar)

DATE: Feb. 13/12 METER SERIAL #: 16 BAROMETRIC PRESSURE (in Hg): 29.42 29.41 29.42 IF Y VARI

- - CRITICAL ORIFICE SET SERIAL #: 1477 ORIFICE SHOU

K' TESTED TEMPERATURES °F ELAPSED

FACTOR VACUUM DGM READINGS (FT3) AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN) DGM H (1) (2) 

ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) INITIAL FINAL INITIAL FINAL AVG  (in H2O) Vm (STD) Vcr (STD) 

1 0.4335 22.7 318.00 321.92 3.92 70 72 72 70 70 71 7 1.10 3.843 3.878 

16 2 0.4335 22.7 322.00 325.92 3.92 69 72 71 70 70 71 7 1.10 3.840 3.882 

3 0.4335 22.7 326.00 329.92 3.92 69 72 71 70 70 71 7 1.10 3.845 3.882 

AVG = 

1 0.5266 21.5 330.40 335.17 4.77 69 71 72 70 70 71 7 1.60 4.680 4.716 

19 2 0.5266 21.5 335.30 340.07 4.77 70 72 72 70 70 71 7 1.60 4.683 4.711 

3 0.5266 21.5 340.30 345.08 4.78 69 72 72 70 71 71 7 1.60 4.690 4.716 

.. AVG = 

1 0.6585 20.1 299.10 305.05 5.95 68 71 71 68 68 70 7 2.40 5.869 5.902 

24 2 0.6585 20.1 305.30 311.27 5.96 68 72 72 69 69 71 7 2.40 5.873 5.902 

3 0.6585 20.1 311.40 317.35 5.95 69 72 73 69 69 71 7 2.40 5.855 5.897 

AVG = 

AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 

AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko= 

dH@= 

(1) Vm (std) = K1 Vm Pbar + (H/13.6) = Net volume of gas sample passed through DGM, corrected to standard conditions

Tm K1 = 17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric)

Tm = Absolute DGM avg. temperature (oR - English, oK - Metric)

Pbar 

(2) Vcr (std) = K' Tamb = Volume of gas sample passed through the critical orifice, corrected to standard conditions

Tamb = Absolute ambient temperature (oR - English, oK - Metric) Calibration performed by: R. 

K' = Average K' factor from Critical Orifice Calibration

(3) Y = Vcr (std) = DGM calibration factor

Vm (std)

METER PART #:

ENVIRONMENTAL SUPP

USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, 

Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.

Unit #16
Jan 14, 2012 (dgm 10).xls

LEHDER ENVIRONMENTAL SERVICES LIMITED

DRY GAS METER CALIBRATION USING CRITICAL ORIFICES

1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),

for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.

4) Record readings in outlined boxes below, other columns are automatically calculated.

INITIAL FINAL AVG (Pbar)

DATE: 14-Feb-12 METER SERIAL #: 10 BAROMETRIC PRESSURE (in Hg): 29.27 29.26 29.27 IF Y VARI

- - CRITICAL ORIFICE SET SERIAL #: 1477 ORIFICE SHOU

K' TESTED TEMPERATURES °F ELAPSED

FACTOR VACUUM DGM READINGS (FT3) AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN) DGM H (1) (2) 

ORIFICE # RUN # (AVG) (in Hg) INITIAL FINAL NET (Vm) INITIAL FINAL INITIAL FINAL AVG  (in H2O) Vm (STD) Vcr (STD) 

1 0.4335 19.6 990.90 994.78 3.88 69 71 71 70 70 71 7 1.00 3.782 3.862 

16 2 0.4335 19.5 994.90 998.78 3.88 70 71 72 70 70 71 7 1.00 3.781 3.859 

3 0.4335 19.4 998.90 1002.78 3.88 71 72 72 70 70 71 7 1.00 3.779 3.855 

AVG = 

1 0.5266 18.2 3.30 8.02 4.72 70 72 72 70 71 71 7 1.55 4.605 4.687 

19 2 0.5266 18.2 8.20 12.92 4.72 70 72 72 71 71 72 7 1.55 4.600 4.687 

3 0.5266 18.2 13.10 17.81 4.71 70 72 73 71 71 72 7 1.55 4.588 4.687 

 AVG = 

1 0.6585 16.5 18.10 23.97 5.87 71 73 73 71 71 72 7 2.30 5.732 5.856 

24 2 0.6585 16.5 24.10 29.97 5.87 70 74 74 71 71 73 7 2.30 5.727 5.861 

3 0.6585 16.5 30.10 35.97 5.87 70 74 74 71 71 73 7 2.30 5.727 5.861 

AVG = 

AVERAGE DRY GAS METER CALIBRATION FACTOR, Y = 

AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko= 

dH@= 

(1) Vm (std) = K1 Vm Pbar + (H/13.6) = Net volume of gas sample passed through DGM, corrected to standard conditions

Tm K1 = 17.64 oR/in. Hg (English), 0.3858 oK/mm Hg (Metric)

Tm = Absolute DGM avg. temperature (oR - English, oK - Metric)

Pbar 

(2) Vcr (std) = K' Tamb = Volume of gas sample passed through the critical orifice, corrected to standard conditions

Tamb = Absolute ambient temperature (oR - English, oK - Metric) Calibration performed by: R. 

K' = Average K' factor from Critical Orifice Calibration

(3) Y = Vcr (std) = DGM calibration factor

Vm (std)

METER PART #:

ENVIRONMENTAL SUPP

USING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, V m (std), and the critical orifice, 

Vcr (std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.

Unit #10
(M-29)Pitot Calibration for 4A Jan.03, 2012.xls

DATE: 5-Jan-12 Barometric: 29.3 "Hg

LOCATION: Wind Tunnel Temperature: 48 o

F

OPERATORS: PB Cpstd: 1

Cps = Cpstd X SQRT ( delta Pstd / delta Ps)

Cps = S-type pitot coefficient

Cpstd = Standard pitot coefficient

Pstd = Standard pitot velocity pressure head

Ps = S-Type pitot velocity pressure head 

PITOT TUBE I.D.: 4A(new pitot lines installed May 6/08)

Nozzle Tunnel Standard Pitot S-Type Pitot S-Type Pitot Deviation

Size Setting Reading Reading Coefficient

(delta Pstd) (delta Ps) Cps ICps - CpavgI

inches Hz "H2O "H2O

0.1875 49.2 0.374 0.566 0.813 0.0075

51.8 0.416 0.632 0.811 0.0091

54.5 0.464 0.676 0.828 0.0081

56.5 0.496 0.734 0.822 0.0016

59.3 0.542 0.792 0.827 0.0069

Average 0.820 0.0066

0.3125 30.2 0.144 0.220 0.809 0.0042

32.7 0.162 0.248 0.808 0.0050

34.8 0.186 0.280 0.815 0.0018

36.7 0.206 0.310 0.815 0.0019

39.1 0.236 0.352 0.819 0.0056

Average 0.813 0.0037

0.5000 12.3 0.024 0.036 0.816 0.0052

14.4 0.034 0.050 0.825 0.0030

17.0 0.046 0.068 0.822 0.0008

19.5 0.062 0.092 0.821 0.0007

21.8 0.076 0.112 0.824 0.0021

Average 0.822 0.0024

The pitot tube must have an average deviation (σ) value of ≤0.01. The above calibration values

were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot 

tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was

manufactured by Dwyer Instuments according to ASME specifications.

LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

4A(Jan.05-2012)
(M-0061)Pitot Calibration for 5W-1 Jan.03, 2012.xls

DATE: 10-Jan-12 Barometric: 29.44 "Hg

LOCATION: Wind Tunnel Temperature: 50 o

F

OPERATORS: PB Cpstd: 1

Cps = Cpstd X SQRT ( delta Pstd / delta Ps)

Cps = S-type pitot coefficient

Cpstd = Standard pitot coefficient

Pstd = Standard pitot velocity pressure head

Ps = S-Type pitot velocity pressure head 

PITOT TUBE I.D.: 5W-1 ***(Calibrated in Reverse for OC Delmar project)***

Nozzle Tunnel Standard Pitot S-Type Pitot S-Type Pitot Deviation

Size Setting Reading Reading Coefficient

(delta Pstd) (delta Ps) Cps ICps - CpavgI

inches Hz "H2O "H2O

0.356 30.2 0.140 0.230 0.780 0.0017

32.7 0.164 0.274 0.774 0.0049

34.8 0.184 0.308 0.773 0.0056

36.7 0.210 0.344 0.781 0.0028

39.1 0.240 0.390 0.784 0.0060

Average 0.779 0.0042

The pitot tube must have an average deviation (σ) value of ≤0.01. The above calibration values

were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot 

tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was

manufactured by Dwyer Instuments according to ASME specifications.

LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

5W-1(Jan.10-2012)
(M-29)Pitot Calibration for 4D Jan.03, 2012.xls

DATE: 5-Jan-12 Barometric: 29.36 "Hg

LOCATION: Wind Tunnel Temperature: 48 o

F

OPERATORS: PB Cpstd: 1

Cps = Cpstd X SQRT ( delta Pstd / delta Ps)

Cps = S-type pitot coefficient

Cpstd = Standard pitot coefficient

Pstd = Standard pitot velocity pressure head

Ps = S-Type pitot velocity pressure head 

PITOT TUBE I.D.: 4D

Nozzle Tunnel Standard Pitot S-Type Pitot S-Type Pitot Deviation

Size Setting Reading Reading Coefficient

(delta Pstd) (delta Ps) Cps ICps - CpavgI

inches Hz "H2O "H2O

0.1875 49.2 0.374 0.554 0.822 0.0097

51.8 0.414 0.608 0.825 0.0062

54.5 0.460 0.660 0.835 0.0035

56.5 0.500 0.710 0.839 0.0078

59.3 0.548 0.784 0.836 0.0047

Average 0.831 0.0064

0.3125 30.2 0.138 0.204 0.822 0.0000

32.7 0.164 0.242 0.823 0.0007

34.8 0.186 0.278 0.818 0.0045

36.7 0.208 0.308 0.822 0.0007

39.1 0.238 0.348 0.827 0.0045

Average 0.822 0.0021

0.5000 12.3 0.024 0.036 0.816 0.0036

14.4 0.034 0.050 0.825 0.0046

17.0 0.046 0.068 0.822 0.0024

19.5 0.060 0.090 0.816 0.0036

21.8 0.074 0.110 0.820 0.0001

Average 0.820 0.0028

The pitot tube must have an average deviation (σ) value of ≤0.01. The above calibration values

were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot 

tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was

manufactured by Dwyer Instuments according to ASME specifications.

LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

4D(Jan.05-2012)
(M-0061)Pitot Calibration for 5W-2 Jan.03, 2012.xls

DATE: 10-Jan-12 Barometric: 29.44 "Hg

LOCATION: Wind Tunnel Temperature: 50 o

F

OPERATORS: PB Cpstd: 1

Cps = Cpstd X SQRT ( delta Pstd / delta Ps)

Cps = S-type pitot coefficient

Cpstd = Standard pitot coefficient

Pstd = Standard pitot velocity pressure head

Ps = S-Type pitot velocity pressure head 

PITOT TUBE I.D.: 5W-2 ***(Calibrated in Reverse for OC Delmar project)***

Nozzle Tunnel Standard Pitot S-Type Pitot S-Type Pitot Deviation

Size Setting Reading Reading Coefficient

(delta Pstd) (delta Ps) Cps ICps - CpavgI

inches Hz "H2O "H2O

0.356 30.2 0.140 0.234 0.773 0.0079

32.7 0.166 0.268 0.787 0.0057

34.8 0.188 0.304 0.786 0.0050

36.7 0.210 0.344 0.781 0.0000

39.1 0.234 0.386 0.779 0.0028

Average 0.781 0.0043

The pitot tube must have an average deviation (σ) value of ≤0.01. The above calibration values

were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot 

tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was

manufactured by Dwyer Instuments according to ASME specifications.

LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

5W-2(Jan.10-2012)
LEHDER DGM TC Calibrations - 2012

LEHDER Environmental Services Limited

Equipment CalibrationsControl Unit Dry Gas Meter Thermocouples

Reference Thermometer ID: Specification for UseAmbient Air: Fisherbrand ANSI/SAMA Z236.1-1983 (-30  ̊F - 120  ̊F) Variance less than: 1.5 

Hot Water: Fisherbrand ANSI/SAMA Z236.1-1983 (0  ̊F - 230  ̊F)Ice Water: Fisherbrand ANSI/SAMA Z236.1-1983 (-30  ̊F - 120  ̊F) % Variance = {ABS [(DGM TC Reading+46

Hot Oil: Fisherbrand ANSI/SAMA Z236.1-1983 (25  ̊F - 750  ̊F)

Tech. Date Unit DGM

Name D-M-Y # In/Out DGM T/C Reference DGM T/C Reference DGM T/C Reference % Variance Pass/Fail % Variance 

J.Haaland 12-Dec-11 6 IN 69 71 34 33 212 211 0.38 Pass 0.20 

J.Haaland 12-Dec-11 6 Out 69 71 33 33 214 211 0.38 Pass 0.00 

J.Haaland 12-Dec-11 7 IN 72 72 33 33 212 211 0.00 Pass 0.00 

J.Haaland 12-Dec-11 7 Out 72 72 32 33 209 211 0.00 Pass 0.20 

J.Haaland 12-Dec-11 9 IN 71 71 32 33 210 212 0.00 Pass 0.20 

J.Haaland 12-Dec-11 9 Out 71 71 32 33 211 212 0.00 Pass 0.20 

J. Denomme 2-Jan-12 10 IN 74 73 34 34 191 188 0.19 Pass 0.00 

J. Denomme 2-Jan-12 10 Out 72 73 36 34 193 190 0.19 Pass 0.40 

J. Denomme 2-Jan-12 11 IN 71 71 35 34 201 204 0.00 Pass 0.20 

J. Denomme 2-Jan-12 11 Out 72 71 35 34 203 202 0.19 Pass 0.20 

J.Haaland 12-Dec-11 14 IN 69 71 32 33 211 212 0.38 Pass 0.20 

J.Haaland 12-Dec-11 14 Out 69 71 32 33 211 212 0.38 Pass 0.20 

J.Haaland 12-Dec-11 15 IN 69 69 33 33 204 205 0.00 Pass 0.00 

J.Haaland 12-Dec-11 15 Out 70 70 34 33 206 205 0.00 Pass 0.20 

J.Haaland 12-Dec-11 16 IN 70 71 34 33 205 208 0.19 Pass 0.20 

J.Haaland 12-Dec-11 16 Out 70 71 33 33 206 208 0.19 Pass 0.00 

J.Haaland 14-Dec-11 VOST #1 Single 69 71 31 33 218 210 0.38 Pass 0.41 

P.Baker 8-Mar-11 VOST #2 Single 69 71 31 33 210 212 0.38 Pass 0.41 

J.Haaland 14-Dec-11 M13B#1 Single 70 71 32 33 213 211 0.19 Pass 0.20 J.Haaland 14-Dec-11 M13B#2 Single 70 71 32 33 213 211 0.19 Pass 0.20 

Last Entry:Name: Mike DenommeDate: 6-Jan-12

(Refe

Measurements Calculatio

Ambient ( ̊F) Ice Water ( ̊F) Hot Water ( ̊F) Ambient I

Jan 2012 
Probes & Outlet Stems Thermocouple Cals 2012

Thermometer ID: Calibrated By:Thermometer ID: Date:Thermometer ID: Thermometer ID: 

TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) 

Probe 2C 35 36 0.20% 70 69 0.19% 203 207 0.60% 500 

Probe 2D 37 37 0.00% 70 69 0.19% 198 202 0.60% 481 

Probe 2E 36 37 0.20% 71 70 0.19% 206 211 0.75% 505 

Probe 2X-Flex 36 36 0.00% 71 70 0.09% 206 210 0.60% 492 

Probe 3A (Flex) 33 33 0.00% 71 70 0.19% 205 208 0.45% 505 

Probe 3B 33 33 0.00% 69 69 0.00% 210 211 0.15% 490 

Probe 3C 33 33 0.10% 71 70 0.19% 212 211 0.15% 500 

Probe 3F 33 34 0.20% 70 69 0.19% 212 212 0.00% 490 

Probe 3G 33 33 0.00% 71 70 0.09% 195 198 0.46% 490 

Probe 3H-D 33 34 0.20% 71 71 0.00% 214 213 0.15% 510 

Probe 4A 33 33 0.00% 69 68 0.19% 210 208 0.30% 515 

Probe 4D 33 33 0.00% 69 70 0.19% 211 215 0.59% 520 

Probe 5C 33 34 0.20% 70 70 0.09% 211 213 0.30% 510 

Probe 5D 33 33 0.00% 69 69 0.00% 210 214 0.59% 521 Probe 5G 34 34 0.00% 69 69 0.00% 212 212 0.00% 520 

Probe 5H 33 33 0.00% 70 68 0.28% 202 204 0.30% 520 Probe 5J 33 33 0.00% 70 69 0.09% 211 214 0.45% 495 

Probe 5K 33 33 0.00% 70 70 0.00% 210 215 0.74% 474 

Probe 7B 33 34 0.20% 69 68 0.19% 209 211 0.30% 515 

Probe 7C 34 34 0.00% 70 68 0.28% 206 209 0.45% 509 Probe 7D 0.00% 0.00% 0.00% 

Probe 7E 35 34 0.20% 69 67 0.38% 210 213 0.45% 543 

Probe 7F 34 34 0.10% 69 68 0.19% 211 212 0.15% 498 

Probe 8A 34 34 0.10% 70 69 0.19% 210 214 0.59% 519 

Probe 9A 34 35 0.20% 67 66 0.19% 210 214 0.59% 530 

Probe 10A 35 35 0.00% 68 66 0.38% 210 216 0.89% 525 

Probe 10B 33 34 0.20% 69 65 0.67% 210 212 0.30% 500 

Probe 10C 34 34 0.00% 69 66 0.48% 210 214 0.59% 520 

Probe 14A 0.00% 0.00% 0.00% 

PT 01 33 33 0.00% 68 67 0.09% 211 214 0.45% 477 

PT 02 33 34 0.20% 70 69 0.19% 210 214 0.59% 540 

PT 08 32 33 0.20% 70 69 0.09% 212 214 0.30% 510 

PT 09 32 34 0.40% 69 64 0.95% 210 215 0.74% 484 

PT 10 34 33 0.20% 70 69 0.19% 212 213 0.15% 510 

PT S4 33 33 0.00% 70 69 0.09% 210 215 0.74% 520 

ICE BATH Ambient HO

% DIFFERENCE 

(Absolute)

PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEET

Thermocouple I.D.

 R.S./K.H.January 4, 2

% DIFFERENCE 

(Absolute)

For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0 oF - 230 oF)For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25 oF - 750 oF)

Boiling Water

For Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)

% DIFFERENCE 

(Absolute)
Probes & Outlet Stems Thermocouple Cals 2012

Thermometer ID: Calibrated By:Thermometer ID: Date:Thermometer ID: Thermometer ID: 

TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) 

ICE BATH Ambient HO

% DIFFERENCE 

(Absolute)

PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEET

Thermocouple I.D.

 R.S./K.H.January 4, 2

% DIFFERENCE 

(Absolute)

For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0 oF - 230 oF)For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25 oF - 750 oF)

Boiling Water

For Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)

% DIFFERENCE 

(Absolute)

PT S5 36 36 0.00% 71 71 0.00% 213 208 0.75% 528 

PT S6 33 32 0.20% 70 69 0.19% 210 215 0.74% 500 

PT S7 36 35 0.20% 71 71 0.00% 214 210 0.60% 548 

PT 74 36 35 0.20% 71 71 0.00% 213 208 0.75% 521 

Outlet Stem 1 34 34 0.00% 71 70 0.09% 206 207 0.15% 

Outlet Stem 2 34 35 0.20% 70 71 0.19% 208 210 0.30% 

Outlet Stem 4 33 35 0.40% 69 68 0.19% 210 204 0.90% 

Outlet Stem 5 34 35 0.20% 70 68 0.38% 204 204 0.00% 

Outlet Stem 6 35 36 0.20% 70 70 0.00% 209 210 0.15% 

Outlet Stem 7 33 34 0.20% 70 68 0.38% 210 211 0.15% 

Outlet Stem 8 34 34 0.00% 70 69 0.19% 208 208 0.00% 

Outlet Stem 10 36 36 0.00% 69 68 0.19% 209 210 0.15% 

Outlet Stem 11 33 34 0.20% 70 68 0.38% 210 209 0.15% 

Outlet Stem 12 34 34 0.00% 68 69 0.19% 208 207 0.15% 

Outlet Stem 13 34 34 0.00% 71 71 0.09% 211 212 0.15% 

Outlet Stem 14 35 35 0.00% 67 69 0.38% 210 210 0.00% 

Outlet Stem 15 34 34 0.00% 70 67 0.57% 210 210 0.00% 

Outlet Stem 16 35 35 0.00% 71 70 0.19% 210 210 0.00% 

Outlet Stem 17 33 34 0.20% 69 67 0.38% 210 210 0.00% 

Pitot X-2 35 37 0.50% 68 65 0.57% 209 215 0.89% 522 
Probes & Outlet Stems Thermocouple Cals.xls

Thermometer ID: Calibrated By:Thermometer ID: Date:Thermometer ID: Thermometer ID: 

TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (o

Probe 2C 34 34 0.00% 72 72 0.00% 203 202 0.15% 479 

Probe 2D 36 36 0.00% 75 75 0.00% 204 199 0.76% 482 

Probe 2E 34 34 0.00% 71 71 0.00% 207 202 0.76% 477 

Probe 3A (Flex) 35 35 0.00% 72 71 0.19% 211 210 0.15% 419 

Probe 3B 38 35 0.61% 75 75 0.00% 210 210 0.00% 471 

Probe 3C 36 35 0.20% 75 75 0.00% 214 206 1.20% 466 

Probe 3F 34 33 0.20% 72 73 0.19% 197 197 0.00% 488 

Probe 3G 35 35 0.00% 75 75 0.00% 207 208 0.15% 469 

Probe 3H-D 35 35 0.00% 71 71 0.00% 210 210 0.00% 418 

Probe 4A 33 33 0.00% 71 73 0.38% 205 201 0.61% 491 

Probe 4D 33 33 0.00% 73 73 0.00% 207 202 0.76% 491 

Probe 5C 33 34 0.20% 71 71 0.00% 210 210 0.00% 419 

Probe 5D 34 34 0.00% 70 72 0.38% 208 206 0.30% 464 

Probe 5G 34 34 0.00% 71 71 0.00% 210 210 0.00% 418 

Probe 5H 37 36 0.20% 70 72 0.38% 207 206 0.15% 465 

Probe 5J 35 35 0.00% 71 71 0.00% 203 199 0.61% 478 

Probe 5K 35 34 0.20% 71 71 0.00% 214 212 0.30% 417 

Probe 7B 36 35 0.20% 71 71 0.00% 210 210 0.00% 413 

Probe 7C 35 35 0.00% 73 73 0.00% 206 204 0.30% 485 

Probe 7D 35 35 0.00% 73 73 0.00% 207 204 0.45% 484 

Probe 7E 36 36 0.00% 72 73 0.19% 206 203 0.45% 490 

Probe 7F 36 36 0.00% 72 73 0.19% 205 203 0.30% 485 

Probe 8A 32 34 0.40% 65 68 0.57% 211 210 0.15% 490 

Probe 9A 33 33 0.00% 69 69 0.00% 193 189 0.62% 478 

Probe 10A 35 34 0.20% 71 71 0.00% 214 212 0.30% 417 

Probe 10B 34 34 0.00% 69 69 0.00% 186 184 0.31% 479 

Probe 10C 34 35 0.20% 71 71 0.00% 210 210 0.00% 413 

Probe 14A 35 35 0.00% 71 71 0.00% 213 212 0.15% 415 

PT 01 32 34 0.40% 70 71 0.19% 203 202 0.15% 439 

PT 02 33 34 0.20% 71 71 0.00% 212 210 0.30% 418 

PT 03 33 34 0.20% 67 68 0.19% 212 212 0.00% 490 

PT 08 33 35 0.40% 71 71 0.00% 210 208 0.30% 433 

PT 09 34 34 0.00% 71 71 0.00% 211 210 0.15% 419 

T 10 33 34 0.20% 71 71 0.00% 210 209 0.15% 423 

PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEET

Thermocouple I.D.

 R.S./J.HJan. 201

% DIFFERENCE 

(Absolute)

For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)

For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0 oF - 230 oF)

% DIFFERENCE 

(Absolute)

For Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)

ICE BATH Ambient 

For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25 oF - 750 oF)

Boiling Water % DIFFERENCE 

(Absolute)
Probes & Outlet Stems Thermocouple Cals.xls

Thermometer ID: Calibrated By:Thermometer ID: Date:Thermometer ID: Thermometer ID: 

TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (o

PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEET

Thermocouple I.D.

 R.S./J.HJan. 201

% DIFFERENCE 

(Absolute)

For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)

For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0 oF - 230 oF)

% DIFFERENCE 

(Absolute)

For Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30 oF - 120 oF)

ICE BATH Ambient 

For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25 oF - 750 oF)

Boiling Water % DIFFERENCE 

(Absolute)

PT S4 33 33 0.00% 69 70 0.19% 203 199 0.61% 479 

PT S5 33 33 0.00% 71 71 0.00% 211 210 0.15% 418 

PT S6 32 34 0.40% 66 68 0.38% 214 212 0.30% 496 

PT S7 33 34 0.20% 71 71 0.00% 211 210 0.15% 418 

PT 74 35 35 0.00% 71 71 0.00% 214 210 0.60% 427 

Outlet Stem 1 34 33 0.20% 71 71 0.00% 0.00% 

Outlet Stem 2 34 33 0.20% 71 71 0.00% 0.00% 

Outlet Stem 4 33 33 0.00% 71 71 0.00% 0.00% 

Outlet Stem 5 Out of Service 33 33 0.00% 71 70 0.19% 0.00% 

Outlet Stem 6 33 33 0.00% 72 71 0.19% 0.00% 

Outlet Stem 7 34 33 0.20% 71 70 0.19% 0.00% 

Outlet Stem 8 34 33 0.20% 72 71 0.19% 0.00% 

Outlet Stem 10 33 33 0.00% 72 71 0.19% 0.00% 

Outlet Stem 11 35 35 0.00% 71 71 0.00% 0.00% 

Outlet Stem 12 33 33 0.00% 71 70 0.19% 0.00% 

Outlet Stem 13 35 35 0.00% 72 72 0.00% 0.00% 

Outlet Stem 14 33 33 0.00% 71 70 0.19%

Outlet Stem 15 33 33 0.00% 71 70 0.19%
Unit 11_Jan 2.xls

Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 2-Jan-12

Operator: JD

Control Unit: Unit 11

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference o

F oF % oF oF %

0 0 0.000 0 -1 0.217

50 48 0.392 50 47 0.588

100 98 0.357 100 97 0.536

150 149 0.164 150 148 0.328

200 199 0.152 Average: 0.417

250 250 0.000

300 300 0.000

350 348 0.247 Readout ID: 5-Stack

400 398 0.233

450 446 0.440 Simulator Setting Readout Difference

500 497 0.313 o

F oF %

550 548 0.198 0 -1 0.217

600 598 0.189 50 47 0.588

650 650 0.000 100 97 0.536

700 700 0.000 150 148 0.328

750 750 0.000 200 198 0.303

800 799 0.079 250 249 0.141

850 850 0.000 300 299 0.132

900 899 0.074 350 347 0.370

950 950 0.000 400 397 0.349

1000 1000 0.000 450 446 0.440

Average: 0.135 500 496 0.417

550 546 0.396

600 597 0.283

Readout ID: 2-Probe 650 649 0.090

700 699 0.086

Simulator Setting Readout Difference 750 749 0.083 o

F oF % 800 799 0.079

0 1 0.217 850 849 0.076

50 49 0.196 900 899 0.074

100 99 0.179 950 949 0.071

150 150 0.000 1000 999 0.068

200 200 0.000 Average: 0.244

250 250 0.000

300 301 0.132

350 348 0.247 Readout ID: 6-DGM in

400 399 0.116

450 447 0.330 Simulator Setting Readout Difference

500 498 0.208 o

F oF %

Average: 0.148 0 0 0.000

50 48 0.392

100 98 0.357

Readout ID: 3-Filter 150 150 0.000

200 200 0.000

Simulator Setting Readout Difference 0.150 o

F oF %

0 0 0.000

50 48 0.392 Readout ID: 7-DGM out

100 98 0.357

150 150 0.000 Simulator Setting Readout Difference

200 199 0.152 o

F oF %

250 250 0.000 0 0 0.000

300 300 0.000 50 48 0.392

350 348 0.247 100 98 0.357

400 398 0.233 150 149 0.164

450 447 0.330 200 200 0.000

500 497 0.313 Average: 0.183

Average: 0.184

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE

IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 11

Temperature Simulator ID: Omega Model: CL 300 

Unit
Unit 15_Jan 3.xls

LEHDER Environmental Services Limited

Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 3-Jan-12

Operator: JD

Control Unit: Unit 15

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference o

F oF % oF oF %

0 -1 0.217 0 -1 0.217

50 46 0.784 50 46 0.784

100 96 0.714 100 96 0.714

150 147 0.492 150 147 0.492

200 198 0.303 Average: 0.552

250 248 0.282

300 298 0.263

350 346 0.494 Readout ID: 5-Stack

400 396 0.465

450 445 0.549 Simulator Setting Readout Difference

500 496 0.417 o

F oF %

550 546 0.396 0 -1 0.217

600 597 0.283 50 46 0.784

650 648 0.180 100 96 0.714

700 699 0.086 150 148 0.328

750 749 0.083 200 198 0.303

800 798 0.159 250 248 0.282

850 848 0.153 300 298 0.263

900 898 0.147 350 346 0.494

950 948 0.142 400 396 0.465

1000 999 0.068 450 445 0.549

Average: 0.318 500 496 0.417

550 546 0.396

600 597 0.283

Readout ID: 2-Probe 650 648 0.180

700 699 0.086

Simulator Setting Readout Difference 750 749 0.083 o

F oF % 800 798 0.159

0 0 0.000 850 848 0.153

50 47 0.588 900 898 0.147

100 97 0.536 950 948 0.142

150 148 0.328 1000 999 0.068

200 198 0.303 Average: 0.310

250 249 0.141

300 299 0.132

350 347 0.370 Readout ID: 6-DGM in

400 397 0.349

450 446 0.440 Simulator Setting Readout Difference

500 496 0.417 o

F oF %

Average: 0.328 0 0 0.000

50 47 0.588

100 96 0.714

Readout ID: 3-Filter 150 148 0.328

200 198 0.303

Simulator Setting Readout Difference 0.387 o

F oF %

0 0 0.000

50 47 0.588 Readout ID: 7-DGM out

100 97 0.536

150 148 0.328 Simulator Setting Readout Difference

200 198 0.303 o

F oF %

250 249 0.141 0 0 0.000

300 299 0.132 50 47 0.588

350 346 0.494 100 97 0.536

400 397 0.349 150 148 0.328

450 446 0.440 200 198 0.303

500 497 0.313 Average: 0.351

Average: 0.329

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE.

IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 15

Temperature Simulator ID: Omega Model: CL 300 

Unit
Unit 14_Jan 3.xls

Control Unit Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 3-Jan-12

Operator: JD

Control Unit: Unit 14

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference o

F oF % oF oF %

0 -1 0.217 0 -1 0.217

50 46 0.784 50 46 0.784

100 96 0.714 100 96 0.714

150 148 0.328 150 148 0.328

200 198 0.303 Average: 0.511

250 249 0.141

300 299 0.132

350 347 0.370 Readout ID: 5-Stack

400 397 0.349

450 446 0.440 Simulator Setting Readout Difference

500 497 0.313 o

F oF %

550 548 0.198 0 -1 0.217

600 599 0.094 50 46 0.784

650 650 0.000 100 96 0.714

700 701 0.086 150 148 0.328

750 751 0.083 200 198 0.303

800 800 0.000 250 248 0.282

850 851 0.076 300 299 0.132

900 901 0.074 350 347 0.370

950 951 0.071 400 397 0.349

1000 1001 0.068 450 446 0.440

Average: 0.231 500 497 0.313

550 548 0.198

600 599 0.094

Readout ID: 2-Probe 650 650 0.000

700 701 0.086

Simulator Setting Readout Difference 750 750 0.000 o

F oF % 800 800 0.000

0 -1 0.217 850 851 0.076

50 47 0.588 900 901 0.074

100 97 0.536 950 951 0.071

150 148 0.328 1000 1001 0.068

200 199 0.152 Average: 0.233

250 249 0.141

300 300 0.000

350 348 0.247 Readout ID: 6-DGM in

400 398 0.233

450 447 0.330 Simulator Setting Readout Difference

500 498 0.208 o

F oF %

Average: 0.271 0 -1 0.217

50 46 0.784

100 96 0.714

Readout ID: 3-Filter 150 148 0.328

200 198 0.303

Simulator Setting Readout Difference 0.469 o

F oF %

0 -1 0.217

50 47 0.588 Readout ID: 7-DGM out

100 97 0.536

150 149 0.164 Simulator Setting Readout Difference

200 199 0.152 o

F oF %

250 249 0.141 0 -1 0.217

300 300 0.000 50 46 0.784

350 348 0.247 100 96 0.714

400 398 0.233 150 148 0.328

450 447 0.330 200 198 0.303

500 498 0.208 Average: 0.469

Average: 0.256

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE

IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 14

Temperature Simulator ID: Omega Model: CL 300 

Unit
Unit 7_Jan 3.xls

LEHDER Environmental Services Limited

Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 3-Jan-12

Operator: JD

Control Unit: Unit 7

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference o

F oF % oF oF %

0 -3 0.652 0 -3 0.652

50 48 0.392 50 48 0.392

100 98 0.357 100 98 0.357

150 149 0.164 150 149 0.164

200 198 0.303 Average: 0.391

250 248 0.282

300 299 0.132

350 347 0.370 Readout ID: 5-Stack

400 398 0.233

450 447 0.330 Simulator Setting Readout Difference

500 498 0.208 o

F oF %

550 548 0.198 0 -3 0.652

600 598 0.189 50 48 0.392

650 649 0.090 100 98 0.357

700 699 0.086 150 149 0.164

750 748 0.165 200 198 0.303

800 799 0.079 250 248 0.282

850 849 0.076 300 298 0.263

900 899 0.074 350 346 0.494

950 949 0.071 400 398 0.233

1000 999 0.068 450 447 0.330

Average: 0.215 500 498 0.208

550 548 0.198

600 598 0.189

Readout ID: 2-Probe 650 648 0.180

700 699 0.086

Simulator Setting Readout Difference 750 748 0.165 o

F oF % 800 799 0.079

0 -1 0.217 850 849 0.076

50 49 0.196 900 899 0.074

100 99 0.179 950 949 0.071

150 150 0.000 1000 999 0.068

200 200 0.000 Average: 0.232

250 249 0.141

300 301 0.132

350 348 0.247 Readout ID: 6-DGM in

400 400 0.000

450 449 0.110 Simulator Setting Readout Difference

500 500 0.000 o

F oF %

Average: 0.111 0 -3 0.652

50 48 0.392

100 98 0.357

Readout ID: 3-Filter 150 149 0.164

200 198 0.303

Simulator Setting Readout Difference 0.374 o

F oF %

0 -1 0.217

50 49 0.196 Readout ID: 7-DGM out

100 99 0.179

150 150 0.000 Simulator Setting Readout Difference

200 200 0.000 o

F oF %

250 249 0.141 0 -3 0.652

300 301 0.132 50 48 0.392

350 348 0.247 100 98 0.357

400 400 0.000 150 149 0.164

450 449 0.110 200 198 0.303

500 500 0.000 Average: 0.374

Average: 0.111

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE.

IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 7

Temperature Simulator ID: Omega Model: CL 300 

Unit
Unit 16_Jan 3.xls

LEHDER Environmental Services Limited

Control Unit Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 3-Jan-12

Operator: JD

Control Unit: Unit 16

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference o

F oF % oF oF %

0 -2 0.435 0 -1 0.217

50 46 0.784 50 46 0.784

100 96 0.714 100 96 0.714

150 148 0.328 150 148 0.328

200 197 0.455 Average: 0.511

250 248 0.282

300 298 0.263

350 346 0.494 Readout ID: 5-Stack

400 396 0.465

450 445 0.549 Simulator Setting Readout Difference

500 496 0.417 o

F oF %

550 546 0.396 0 -1 0.217

600 597 0.283 50 46 0.784

650 649 0.090 100 96 0.714

700 699 0.086 150 148 0.328

750 749 0.083 200 198 0.303

800 798 0.159 250 248 0.282

850 849 0.076 300 298 0.263

900 898 0.147 350 346 0.494

950 949 0.071 400 397 0.349

1000 999 0.068 450 445 0.549

Average: 0.316 500 496 0.417

550 546 0.396

600 598 0.189

Readout ID: 2-Probe 650 649 0.090

700 699 0.086

Simulator Setting Readout Difference 750 749 0.083 o

F oF % 800 799 0.079

0 0 0.000 850 849 0.076

50 47 0.588 900 899 0.074

100 97 0.536 950 949 0.071

150 148 0.328 1000 999 0.068

200 198 0.303 Average: 0.282

250 248 0.282

300 299 0.132

350 347 0.370 Readout ID: 6-DGM in

400 398 0.233

450 446 0.440 Simulator Setting Readout Difference

500 497 0.313 o

F oF %

Average: 0.320 0 -1 0.217

50 47 0.588

100 96 0.714

Readout ID: 3-Filter 150 148 0.328

200 198 0.303

Simulator Setting Readout Difference 0.430 o

F oF %

0 0 0.000

50 47 0.588 Readout ID: 7-DGM out

100 97 0.536

150 148 0.328 Simulator Setting Readout Difference

200 198 0.303 o

F oF %

250 248 0.282 0 -1 0.217

300 299 0.132 50 47 0.588

350 347 0.370 100 96 0.714

400 398 0.233 150 148 0.328

450 446 0.440 200 198 0.303

500 497 0.313 Average: 0.430

Average: 0.320

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE

IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 16

Temperature Simulator ID: Omega Model: CL 300 

Unit
123987 Nozzle Calibration Measurements.xls

LEHDER Environmental Services Limited

Nozzle Calibration

Project No.: 123987

Date: Jan.24, 2012

Calibrator: P. Baker

ID 1 2 3 Average 

(inches)

DM1(M-0061) 0.3650 0.3655 0.3640 0.3648 one piece nozzle/probe liner

DM1(M-29) 0.3900 0.3900 0.3890 0.3897

DM2(M-0061) 0.3590 0.3595 0.3600 0.3595 one piece nozzle/probe liner

DM2(M-29) 0.3855 0.3825 0.3820 0.3833

NOTE:

1. Measure inside diameter of nozzle at 3 different diameters - to the nearest 0.001 inch.

2. Obtain the average diameter.

3. The difference between high and low readings cannot exceed 0.004 inches.

1

2

3

Glass Nozzles
02-16-12 barometer cal.xls

Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Black % Difference 

Barometer From Actual

Compensated

°C °F kPa "Hg "Hg

Feb 16/12 10:00 3 37 0.657 101.38 29.94 29.28 29.27 0.04%

11:00 3 37 0.657 101.30 29.91 29.26 29.25 0.02%

12:00 4 39 0.655 101.30 29.91 29.26 29.25 0.03%

13:00 5 41 0.652 101.29 29.91 29.26 29.25 0.03%

AVG. 0.03%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron

BAROMETER CALIBRATION

"Hg %

590†

Feb 16,2012

BK

Temperature

** Correction Factor obtained from National Imagery and Mapping Agency's web page

* Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page) 

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page) Correction Factor**

Date Time

Actual Barometric***

@ Sea Level

Brunton-black (newdigital)
02-16-12 barometer cal.xls

Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Blue % Difference 

Barometer From Actual

Compensated

°C °F kPa "Hg "Hg

Feb 16/12 10:00 3 37 0.657 101.38 29.94 29.28 29.27 0.04%

11:00 3 37 0.657 101.30 29.91 29.26 29.28 0.08%

12:00 4 39 0.655 101.30 29.91 29.26 29.28 0.07%

13:00 5 41 0.652 101.29 29.91 29.26 29.27 0.04%

AVG. 0.06%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron

** Correction Factor obtained from National Imagery and Mapping Agency's web page

* Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page) 

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page) Correction Factor**

Date Time

Actual Barometric***

@ Sea Level

BAROMETER CALIBRATION

"Hg %

590†

Feb 16,2012

BK

Temperature

Brunton-blue (digital)
02-18-11 barometer cal 1.xls

Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Black % Difference 

Barometer From Actual

Compensated

°C °F kPa "Hg "Hg

18-Feb-11 9:00 8 46 0.646 100.81 29.77 29.12 29.12 0.01%

18-Feb-11 10:00 8 46 0.646 100.87 29.79 29.14 29.13 0.04%

18-Feb-11 11:00 8 46 0.646 100.91 29.80 29.15 29.15 0.01%

18-Feb-11 12:00 8 46 0.646 100.91 29.80 29.15 29.16 0.02%

AVG. 0.02%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron

** Correction Factor obtained from National Imagery and Mapping Agency's web page

* Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page) 

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page) Correction Factor**

Date Time

Actual Barometric***

@ Sea Level

BAROMETER CALIBRATION

"Hg %

590†

18-Feb-11

N. Abma

Temperature

Brunton-black (newdigital)
02-18-11 barometer cal 1.xls

Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Blue % Difference 

Barometer From Actual

Compensated

°C °F kPa "Hg "Hg

18-Feb-11 9:00 8 46 0.646 100.81 29.77 29.12 29.06 0.22%

18-Feb-11 10:00 8 46 0.646 100.87 29.79 29.14 29.10 0.14%

18-Feb-11 11:00 8 46 0.646 100.91 29.80 29.15 29.12 0.11%

18-Feb-11 12:00 8 46 0.646 100.91 29.80 29.15 29.13 0.08%

AVG. 0.14%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron

BAROMETER CALIBRATION

"Hg %

590†

18-Feb-11

N. Abma

Temperature

** Correction Factor obtained from National Imagery and Mapping Agency's web page

* Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page) 

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page) Correction Factor**

Date Time

Actual Barometric***

@ Sea Level

Brunton-blue (digital)

Appendix D 

Field Data Sheets 

 

D.1: Field Run Sheets 

D.2: Sample Recovery Data Sheets 

D.3: Cyclonic Flow Data Sheet 
Appendix D.1 

Field Run Sheets 




































Appendix D.2 

Sample Recovery Data Sheets 








Appendix D.3 

Cyclonic Flow Data Sheet 


Appendix E 

Sample Point Markings & Site Photographs 
Appendix E 

DM1 and DM2 Furnace DEP Outlets 

Sample Location Dimensions and Point Locations 

Project 123987 

Table 1: Sample Location Specifications 

Parameter DM1 Furnace 

DEP Outlet 

DM2 Furnace 

DEP Outlet 

Emission Unit # U-00002 U-00012 

Emission Point # EP00100 EP00200 

Stack Plane Configuration Rectangle Rectangle 

Stack Diameter / Dimensions 3.28ft x 3.28ft 3.28ft x 3.28ft 

Duct Configuration Vertical  Vertical 

Accessibility for Sampling Mobile ManLift Mobile ManLift 

Number of Sampling Ports 5 5 

Upstream Distance to Ports 5.6 ft 2.7 ft 

Downstream Distance to Ports 10.6 ft 11.3 ft 

Sample Port Size 4 inches ID 4 inches ID 

Total # of Sampling Points 30 30 

Sampling Matrix 5 x 6 5 x 6 

Figure 1: OC Delmar Furnace DEP Units and Sample Locations 

Common 

DEP Stack

DM1 Furnace DEP DM2 Furnace DEP 

Sample Location 

Sample Location 

Page 1 of 4 
Appendix E 

DM1 and DM2 Furnace DEP Outlets 

Sample Location Dimensions and Point Locations 

Project 123987 

Figure 2: OC Delmar Furnace DEP Outlet – Method 1 Sample Point Locations 

 Port lengths are 6.5 inches 

36.1” 29.5” 23” 16.4” 9.8” 3.3”

3.28 ft

3.28 ft

Port 1 Port 2 Port 3 Port 4 Port 5 

Page 2 of 4 
Appendix E 

DM1 and DM2 Furnace DEP Outlets 

Sample Location Dimensions and Point Locations 

Project 123987 

Figure 3: DM1 Furnace DEP Outlet Sample Location 

Page 3 of 4 
Appendix E 

DM1 and DM2 Furnace DEP Outlets 

Sample Location Dimensions and Point Locations 

Project 123987 

Page 4 of 4 

Figure 4: DM2 Furnace DEP Outlet Sample Location