# Test Report

Evaluation of Particulate, Total Chromium and Hexavalent Chromium Emissions from the Owens Corning Delmar DM1 and DM2 Furnace DEP Outlets to satisfy Se ction 114 Information Collection Request

January 2011

Prepared for:

Owens Corning insulating Systems, LLC
1277 Feura Bush Road Feura Bush, NY
12067-1719 Attention: Mr. David Krenitsky

Prepared by:

LEHDER Environmental Services Limited 704 Mara Street, Suite 210 Point Edward, ON
N7V 1X4

Project No.: 123987

February 25, 2012

LEHDER Environmental Services Limited 704 Mara Street, Suite 210, Point Edward, Ontario, Canada N7V 1X4 Phone: (519) 336-4101 Fax: (519) 336-4311
9954 – 62 Avenue, Edmonton, Alberta Canada T6E 0P5 Phone: (780) 462-4099 Fax: (780) 462-4392 

## www.l e h de r. co m

# ii

Executive Summary

LEHDER Environmental Services Limited (LEHDE R) of Point Edward, Ontario was retained by Owens Corning to conduct a stack testing program at its wool fiberglass insulation manufacturing facility located at 1277 Feura Bush Road, Feura Bush (Delmar), New York.

The purpose of the testing program was to satisfy an Information Collection Request (ICR) authorized under Section 114 of the Clean Air Act. Stack emissions from glass melting operations are targeted under this initiative. Test contaminants and methods specified by the Section 114 request are:

Chromium (7440-47-3)

 Filterable – EPA Method 29

 Vaporous – EPA Method 29

 Total – EPA Method 29 and SW-846 Method 0061

Hexavalent Chromium (1854-02-99)

 SW-846 Method 0061

Particulate Matter

 EPA Method 5/29

Exhaust gases from the Owens Corning Delmar DM1 and DM2 glass melting furnaces were identified for testing under the Section 114 initiative. Emissions from these sources were evaluated during the week of January 23, 2012. A summary of the average test results is presented in Table I.

Table I Summary of Emission Data from DM1 & DM2 Furnace DEP Outlets – January 2012

Method 29 Method 0061 Pollutant Units DM1 DEP DM2 DEP DM1 DEP DM2 DEP

mg/S.m 3 

# 1.5 7.9 Filterable Particulate lb/hr 0.045 0.25

μ g/S.m 3 

# 4.8 41 Filterable Chromium lb/hr 1.4E-04 1.3E-03

μ g/S.m 3 

# 0.14 0.22 Vaporous Chromium lb/hr 4.1E-06 6.8E-06

μ g/S.m 3 

# 4.9 41 4.9 41 Total Chromium lb/hr 1.5E-04 1.3E- 03 1.5E-04 1.3E-03

μ g/S.m 3 

# 2.7 36 Hexavalent Chromium lb/hr 8.4E-05 1.1E-03

# iii

Table of Contents

Executive Summary........................... .................................................................ii

1. Introduction ................................................................................................................... 1

1.1 Background .............................................................................................................1

1.2 Description of Testing Program...............................................................................1

1.3 Test Program Organization .....................................................................................2

2. Source Description .......................................................................................................3

3. Description of Sources and Sampling Locations ......................................................5

4. Test Methods .................................................................................................................6

4.1 Total and Hexavalent Chromium – Method 0061....................................................7

4.2 Filterable Particulate and Total Chromium - EPA Method 29................................12

5. Test Results.................................................................................................................16

6. Discussion of Results.................................................................................................20

6.1 General..................................................................................................................20

6.2 Particulate Emission Summary .............................................................................20

6.3 Total Chromium - Method 29 vs. Method 0061 .....................................................21

6.4 Method 0061 Hexavalent and Total Chromium Data ............................................21

6.5 QA/QC...................................................................................................................23

7. Closure........................................................................................................................ .24

# iv

List of Tables and Figures

Table 3-1: Description of Sources and Sampling Locations ...................................................5 Table 4-1: Summary of Sampling and Analytical Methods .....................................................6 Table 4-2: Specifications for Hexavalent Chromium (Method 0061).......................................7 Table 4-3: Specifications for PM/Metals Sampling (EPA Method 29)...................................12 Table 5-1: Summary of Method 0061 Test Results – DM1 Furnace DEP Outlet..................16 Table 5-2: Summary of Method 0061 Test Results – DM2 Furnace DEP Outlet..................17 Table 5-3: Summary of Method 29 Test Results – DM1 Furnace DEP Outlet......................18 Table 5-4: Summary of Method 29 Test Results – DM2 Furnace DEP Outlet......................19 Table 6-1: Average Particulate Test Results – DM1 & DM2 Furnace DEP Outlets ..............20 Table 6-2: Total Chromium Data – Method 29 vs. Method 0061 ..........................................21 Table 6-3: Method 0061 – Hexavalent Chromium vs. Total Chromium ................................22

Figure 2-1: General Process Flow Schematic .........................................................................3 Figure 4-1: Schematic of EPA Method 0061 Sampling Train................................................10 Figure 4-2: Sample Recovery Flow Chart – Method 0061 Test Runs ...................................11 Figure 4-3: Sample Recovery – Method 29 Test Runs .........................................................14 Figure 4-4: Schematic of EPA Method 29 Sampling Train ....................................................15



# Appendices

Appendix A: Concentration and Mass Rate Calculations

A.1: Method 29 Test Runs

A.2: Method 0061 Test Runs

Appendix B: Analytical Report B.1: Enthalpy PM Report B.2: Element One M29 Report B.3: Element One M0061 Report

Appendix C: Equipment Calibrations

Appendix D: Field Data Sheets

D.1: Field Run Sheets D.2: Sample Recovery Data Sheets D.3: Cyclonic Flow Data Sheet

Appendix E: Sample Point Markings & Site Photographs

Pertinent process data and lb/ton emissions are contained on Confidential CD

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 1 of 24



# 1. Introduction

1 .1 Background

The U.S. Environmental Protection Agency (USEPA) is collecting information on particulate matter (PM), chromium compounds, hexavalent chromium, and other related information from wool fiberglass manufacturing facilities. The information gathered will be used by the EPA to perform a review of the maximum achievable control technology (MACT) standard in 40 CFR Part 63, subpart NNN. The authority to request this information is reference under Section 114 of the Clean Air Act (CAA) (42 U.S.C. 7414).

Stack emissions from glass melting operations are targeted under this initiative. Specifically, test compounds and methods specified by the Section 114 request are:

Chromium (7440-47-3)

 Filterable – EPA Method 29

 Vaporous – EPA Method 29

 Total – EPA Method 29 and SW-846 Method 0061

Hexavalent Chromium (1854-02-99)

 SW-846 Method 0061

Particulate Matter

 EP A Method 5/29

The DM1 and DM2 Furnace DEP outlets located at the Owens Corning Delmar Plant were sources identified for evaluation by the Section 114 initiative. Emission data are required to be reported through the USEPA Electronic Reporting Tool (ERT) and are due to applicable USEPA offices by the end of February 2012.



# 1.2 Description of Testing Program

Owens Corning retained LEHDER Environmental Services (LEHDER) to conduct the source testing required by the Section 114 initiative at its wool fiberglass manufacturing facility in Delmar, New York (referred to in this report as OC Delmar). The program involved the
evaluation of emissions from the DM1 and DM2 Furnace DEP Outlets. DEP is an abbreviation for “Dry Electrostatic Precipitator”.

Both sources were evaluated for filterable particulate, filterable chromium and vaporous chromium in accordance with USEPA Method 29. Total and hexavalent chromium emissions were also determined in accordance with USEPA Method 0061.

Three test runs were performed for each of the two test methods. Method 29 test runs could not be carried out simultaneously with Method 0061 runs due to physical limitations at the test sites. However, one of each test run was conducted on each of the two sources each day. To ensure detection of the test compounds, sample runs were initially set for 240 minutes (4.0 hours).

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 2 of 24



# Both DM1 and DM2 furnaces were operating at normal rates during the sampling campaign. Process/production data were monitored and collected by Owens Corning personnel.

Testing was conducted from January 24 to 26, 2012.



# 1. 3 Test Program Organization

Facility ID / Address: Owens Corning Delmar Plant
1277 Feura Bush Road Feura Bush, NY USA 12067-1719

Facility ID: 3600100066

Industry NAICS: 327993

AFS#: 3600100066

FRS#: 110000324168

Air Permit #: 4-0122-00004/00039

Facility Environmental Manager: Mr. David Krenitsky
Tel: 518-475-3673
Email: david.krenitsky@owenscorning.com

Facility Site/Project Contacts: Mr. Rick Cooper Owens Corning Science and Technology Center Granville, OH
Tel: 740-321-7628
Fax: 740-321-4628
Email: rick.d.cooper@owenscorning.com

Sampling Company: LEHDER Environmental Services Limited 704 Mara Street, Suite 210 Point Edward, ON N7V 1X4

LEHDER Project Manager: Mr. Mike Denomme
Tel: 519-336-4101 Ext. 225 Fax: 519-336-4311
E-mail: mdenomme@lehder.com

LEHDER Field Crew: Chris Ungar, Joy Edwards, Jordan Denomme, John Haaland, Paul Baker, Rick Seller and Justin Tayles

Analytical Laboratory #1: M29 Particulate Analysis Enthalpy Analytical Inc. 800 Capitola Dr., Ste. 1 Durham, NC 27713
Tel: 919-850-4392 Fax: 919-850-9012 Contact: Mr. Bryan Tyler
E-mail: bryan.tyler@enthalpy.com

Analytical Laboratory #2: M29 & M0061 Total Chromium/ Hexavalent Chromium Analysis Element One, Inc. 5022-C Wrightsville Av., Wilmington, NC 28403
Tel: 910-793-0128 Fax: 910-792-6853 Contact: Ms. Paula Smith E-mail: paula.smith @e1lab.com

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 3 of 24



# 2. Source Description

The Owens Corning Delmar plant manufactures rotary spun (RS) fiberglass building insulation. There are two production lines designated DM1 and DM2. The manufacture of fiberglass insulation is a continuous process that takes place through the following major steps:

 Glass melting

 Formation of fiber/addition of binder

 Pack curing

 Cooling, trimming and packaging

The major process steps are described in more detail in the following sections and a process flow schematic is presented in Figure 2-1

Figure 2-1: General Process Flow Schematic

Mixed G lass
Batch
wi th Cullett



# Fiber Pack Forming
Tunnel 

# Curing Oven Cooling, Fabrication, Packaging & Storage O p erations Channel/Forehearh

Wet Fiber Pack w/ Uncured

Binder Cured
Pack 

## IWS

Exhaust to atmosphere via

WEP Stacks (DM1) or Mixing Chamber Stack (DM1 & D M2 ) 

## Forming
F ans Molten Glass



## Energy (electric, gas or some combination) Combined with forming effluent in Mixing Chamber

Stack and dischar g ed



## Gas Batch Systems

Veils of Coated
Fibers 

## Air Exh aust t o A tmosph ere



# Glass Melting
Furnace

Fiber Coating/
Binder A pp lication Air Gas

Water Binder Dry Electrostatic Precipitator (DEP)

Exhaust to atmosphere via Smoke Stripper and

Cooling Stacks

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 4 of 24



# Raw materials required to produce glass are mixed together as a batch and continuouslycharged into a refractory bricked glass-melting furnace. The furnaces are oxygen/naturalgas fired units. Effluent combustion gases generated from each of the DM1 and DM2 furnaces are exhausted to separate control units and discharged after they combine in a common stack. Test samples are collected from the individual discharges after the control device and before they are combined in the common stack.

From the glass melting furnace, the molten glass flows through bushings to a rotary fiberizer that produces the fibers. After the fibers have been formed, they are directed towards a conveyor by an air stream. A binder solution is sprayed on the glass fibers as they descend to the forming conveyor chain. The formation of wool product (commonly called a “pack”) is accomplished when the binder-coated fibers are drawn onto the perforated forming conveyor by suction fans. The air passing through the product is treated prior to release to atmosphere via the mixing chamber stacks.

After forming, the coated fiber mat or "pack" is passed through a convection oven fired bynatural gas to promote curing. Curing gases from each line oven are treated by linespecific incinerator units. The discharge gases from each incinerator unit are combined with air/gases exhausted from the fiber forming proc ess in the mixing chamber prior to release via the mixing chamber stacks.

After leaving the oven, the product is cooled, trimmed, and cut to the desired length and width, prior to packaging. The cooling process involves pulling ambient air through the product after it leaves the curing oven. The effluent gases on the DM1 and DM2 lines are filtered prior to discharge via the cooling stacks.

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 5 of 24



# 3. Description of Sources and Sampling Locations

The DM1 and DM2 melting furnaces exhaust to separate dry electrostatic precipitator units (DEPs). The outlet ducts from both units comb ine to a common stack prior to release to atmosphere. Emissions sampling was carried out on the vertical “downcomer” discharge of each DEP unit, prior to the fan and before both effluent combine into the common DEP Stack.

Since a permanent platform did not exist to access the two DEP outlet sampling locations, a mobile “scissor lift” was used to access the sampling ports. The sources and sampling locations for the DM1 and DM2 Furnace DEP Outlets are described in Table 3-1. Site photographs and sample point markings are presented in Appendix E.

Table 3-1: Description of Sources and Sampling Locations

Parameter DM1 Furnace
DEP Outlet DM2 Furnace
DEP Outlet

Emission Unit # U-00002 U-00012

Emission Point # EP00100 EP00200

Stack Plane Configuration Rectangle Rectangle

Stack Diameter / Dimensions 3.28ft x 3.28ft 3.28ft x 3.28ft

Stack Area at Sample Location 10.76 ft 2 

# 10.76 ft 2



# Duct Configuration Vertical  Vertical 

Accessibility for Sampling Mobile ManLift Mobile ManLift

Number of Sampling Ports 5 5

Upstream Distance to Ports 5.6 ft 2.7 ft

Downstream Distance to Ports 10.6 ft 11.3 ft

Sample Port Size 4 inches ID 4 inches ID

Sample Port Length 6.5 inches 6.5 inches

Total # of Sampling Points 30 30

Sampling Matrix 5 x 6 5 x 6

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 6 of 24



# 4

. Test Methods

Sampling and analytical protocols are listed in Table 3-1 and are detailed in subsequent
sections.

Table 4-1: Summary of Sampling and Analytical Methods

Parameter Sampling Technique Analytical Technique Laboratory

Velocity / Flow Rate USEPA Method 2 N/A N/A

Molecular Weight USEPA Method 3, 3A Instrumentally using electrochemical cell analyzer N/A

Moisture Content Condensation as per USEPA Method 4 Gravimetrically as per USEPA Method 4 LEHDER

Filterable Particulate Isokinetically as per USEPA Method 5/29 Gravimetrically as per EPA Method 5/29 Enthalpy

Filterable/Vapours/Total Chromium Isokinetically as per USEPA Method 5/29  Samples prepared as per USEPA Method 29

 Chromium from all train

fractions analyzed by ICP/MS Element One

Total & Hexavalent Chromium Isokinetically as per USEPA Method 0061  Samples prepared as per USEPA Method 0061

 Hex.Chromium analyzed by IC

 To tal Chromium by ICP/MS Element One

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 7 of 24



# 4 .1 Total and Hexavalent Chromium – Method 0061

Emission rates of hexavalent chromium (Cr +6 

# ) and total chromium were determined using
EPA Method 0061: Determination of Hexavalent Chromium Emissions from Stationary Sources (January 1996). The specifications for the Method 0061 sampling method are presented in Table 4-2 and Figure 4-2. The sampling train is depicted in Figure 4-1.

Table 4-2: Specifications for Hexavalent Chromium (Method 0061)

Item Specification

Test Method

Reference: US EPA Method 0061(Ref: SW-846): Determination of Hexavalent Chromium Emissions from Stationary Sources

Method Modifications: Extra nitric acid rinse and filter recovery for total chromium analysis Sampling Technique: Isokinetic (Recirculation of Impinger Solution)

Number of Test Runs: 3 (one per day)

Sampling Parameters Total # of Sample Points: 30 Sample Matrix: 5 ports x 6 points/port Sample Time / Point (min): 7.0 to 8.0 minutes/point (3.5 to 4.0 minutes per reading) Total Test Time / Run (min): 240.0 and 210.0 minutes (4.0 to 3.5 hours) Target Sample Rate: 0.75 cfm

Sampling Train

Nozzle/Probe: One piece nozzle/probe liner constructed of glass by a glassblower. Size of extraction nozzle measured before use. Glass nozzle/probe liner used to address the high stack gas temperature.

Probe Liner: 3/8 inch OD Teflon®

Special Probe Type: Air-cooled probe to help keep recirculation solution in liquid form. One-piece nozzle/liner inserted into air-cooled probe.

Filter: No Filter (probe exit connected directly to impingers)

Recirculation System: Peristaltic pump circulating impinger solution (0.5 N KOH) from impinger #1 to the nozzle/probe transition.

Impingers: Full sized Teflon® with 3/8 inch OD Teflon® stems and connectors, containing:

 Impinger #1: 200 mLs of 0.5N KOH

 Impinger #2: 75 mLs of 0.5 N KOH

 Impinger #3: 75 mLs of 0.5 N KOH

 Impinger #4: Empty

 Impinger #5 (glass): Known quantity of silica gel

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 8 of 24



# Table 4-2: Specifications for Hexavalent Chromium (Method 0061) (cont’d)

Item Specification

Sampling Procedures

Pre-cleaning:  Wash with hot tap water, then hot soapy water, then rinse three times with tap water.

 Train components (up to the silica gel impinger) soaked for a

minimum of 4 hrs in 10% (v/v) nitric acid solution.

 Components are then rinsed three times with reagent grade

water and air dried, then sealed.

Train Operation:  Sample isokinetically at each sample point while KOH solution from impinger #1 is circulated to the probe and back into impinger #1.

 Solution circulation required to prevent reduction of Cr+6 to Cr+3

in the sample gas stream

Solution pH Check:  Check pH of solution in first impinger after first traverse and at
end of test run.

 If pH less than 8.5, test run is void.

Post Test Activities  Sample train post test leak check. Criterion is 0.020 cfm at the highest vacuum encountered during the test run.

 Disconnect probe from train prior to nitrogen purge.

 Purge sampling train from inlet of first impinger to exhaust of

silica gel with UHP nitrogen at a rate of 10 Lpm for 30 minutes.

Sample Recovery

Location: Clean, dry and well lit area

Recovery Procedure:  Impinger catch from impingers #1 - 4 volumetrically measured and combined into one sample bottle

 Glass nozzle, aspirator, all connecting tubing and impingers

rinsed with DI Water.

 Rinses volumetrically measured and added to sample bottle.

 All impingers and connectors rinsed with 0.1 N HNO 3 

# into a 250

mL bottle for total Cr analysis.

Filtration:  Entire aqueous sample passed through a 0.45 μ m acetate filter
in a Teflon filtration device.

 Filtration device washed 3 times with DI water and rinses added

to sample.

 Final aqueous sample volume recorded.

 Filter recovered into a separate bottle (60 mLs amber glass) for

total Cr analysis. Filter holder rinsed with water and HNO 3 

# and
recovered in same bottle.

Sample Bottles:  1 L polyethylene (PE) bottle for KOH impinger solutions & rinses

 250 mLs PE bottle for 0.1N nitric acid rinses

 60 mLs wide-mouth amber glass bottle for acetate filter & rinses.

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 9 of 24



# Table 4-2: Specifications for Hexavalent Chromium (Method 0061) (cont’d)

Item Specification



# Analysis

Laboratory: Element One, Wilmington, NC

Analytical Technique: (Hexavalent Chromium)  Samples were prepared and analyzed according to SW-846 Method 0061 protocol

 Samples were analyzed for chromium (VI) using a Shimadzu

2010 HPLC unit and a Timberline RDR-1 Reaction Mode

 Chromium (IV) Detection Limit: 0.1 μ g/L

Analytical Technique: (Total Chromium)  Samples were acidified with trace metals grade concentrated nitric acid and digested on a hotplate according to the method protocol.

 The digested samples were analyzed for total chromium in a

PerkinElmer ELAN 6100 ICP MS.

 Total Chromium Detection limit: 1.0 μ g/L

Hold Time: 14 Days

QA/QC:  1 reagent blank (300 mLs of 0.5N KOH)

 1 reagent water blank

 1 0.1N nitric acid blank

 1 reagent blank (distilled water)

 1 acetate filter blank

 Laboratory duplicate analyses relative percent difference (RPD)

 Laboratory spike sample recovery

Data Reporting

Volumetric Flow Rate (Qs): 

#  Actual flow rate (Acfm) is product of average measured velocity (ft/s) and cross-sectional area (ft 2 

# ) of stack at sampling plane.

 Standard flow rate (Scfm) is Actual Flow rate corrected to 68  ̊ F

and 29.92 inches Hg

 Reference flow rate on a dry basis considers dry gas fraction of

effluent flow rate only (Water vapour mole fraction removed from the total)

Pollutant Concentration (Cs): 

# Mass collected in aqueous sample (from Laboratory) divided by dry standard sample volume from test run (S.ft 3 

# or S.m 3 

# ).

Pollutant Mass Rate (Es): 

#  Es = Cs x Qs

 lb /hr = mg/S.ft 3 

# x scfm x 60 min/hr / 454,000 mg/lb

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 10 of 24



# Figure 4-1: Schematic of EPA Method 0061 Sampling Train

Control Unit

 Calibrated DGM

 Rotary Vane Vacuum Pump

 Orifice Meter

 Temperature monitoring

circuitry

 Effluent velocity pressure

manometer Peristaltic Pump (circulates KOH solution from Impinger #1, into the probe just

before probe/nozzle union ) 

## Teflon® Impingers and Connectors

 Impinger #1 has recirculation adaptor on the bottom

 Impinger #1 contains 150 mL of 0.5N KOH

 Impingers #2 & #3 contain 75 mL of 0.5N KOH each Measured Glass Nozzle

fused to Glass Liner

Custom made 5/8 inch OD Glass Liner with fused nozzle

(with 1⁄4 inch OD Teflon® recirculation tube inside)

1⁄4 inch OD Teflon®
recirculation line 

## Ice Bath Impinger Outlet Temperature

Silica Gel (glass impinger) Air-cooled probe



## Umbilical
Line

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 11 of 24

Nozzle/Probe Assembly Impingers

After test run, disconnect probe/nozzle assembly from impingers and rinse probe/nozzle assembly with

100 mLs of with reagent grade water into 1 Liter PE
bottle ( Container #1 )

Rinse entire impinger train and connectors with 0.1N Nitric Acid and recover into 250 mLs poly bottle (Container #2) for total Cr analysis. After test run, check

p H of the first im p in g er

Attach nitrogen purge to input of sampling train. Purge system for 30 min at 10 LPM

Disconnect impingers. Volumetrically measure and transfer aqueous solution from impingers 1, 2 & 3 into 1 Liter PE sample bottle (Container #1). Rinse impingers and associated connector pieces 4 times with reagent grade water and collect into Container #1.

Samples to Enthalpy/Element One Is pH 

# > 8.5?



# YES No Discard solution
and redo test run

Transfer entire aqueous volume from Container #1 into Teflon filtration unit and filter through a 0.45 μ m acetate

filter. Recover filtrate back into Container #1. Rinse
container and filtration unit and combine into same bottle

(Container #1). Record final aqueous sample volume.

Recover acetate filter into a 60 mLs wide-mouth amber glass bottle (Container #3) for total Cr analysis. 

# Figure 4-2: Sample Recovery Flow Chart – Method 0061 Test Runs

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 12 of 24



# 4 .2 Filterable Particulate and Total Chromium - EPA Method 29

Emission rates of f ilterable particulate, filterable chromium and vaporous chromium were determined using EPA Method 29: Determination of Metal Emissions from Stationary Sources . The specifications for the Method 29 sampling method are presented in Table 4-3 and Figure 4-3. The sampling train is depicted in Figure 4-4.

Table 4-3: Specifications for PM/Metals Sampling (EPA Method 29)

Item Specification

Test Method

Reference: EPA Method 29 Determination of Metal Emissions from Stationary Sources

. Method Modifications: None Sampling Technique: Isokinetic at multiple points as per EPA Method 1

Number of Test Runs/Source: 3 (simultaneous with M0061 Test Runs)

Sampling Parameters Total # of Sample Points: 12 Sample Matrix: 2 ports x 6 points/port Sample Time / Point (min): 45.0 minutes/point (5.0 minutes per reading) Total Test Time / Run (min): 240.0 minutes (4.0 hours) Target Sample Rate: 0.75 cfm

Sampling Train

Nozzle: Glass (size measured)

Probe liner: Seamless glass heated to 120  ̊ C ± 14  ̊ C

Filter: Pre-tared quartz fiber heated to 120  ̊ C ± 14  ̊ C

Glass connectors: Ball/socket with O-rings

Back-half: Full sized impingers chilled in ice bath

 Imp. #1: 100 mLs 5% nitric/10% H 2 

# O 2 

# Sol’n

 Imp. #2: 100 mLs 5% nitric/10% H 2 

# O 2 

# Sol’n

 Imp. #3: Empty

 Imp. #4: Known quantity of silica gel

Sample Recovery

Location: Clean, dry and well lit area. Front-half Recovery Solvents:  Front-half wash for PM/Metals: Acetone

 Front-half wash for Metals: 0.1N Nitric Acid Back-Half Recovery Solvents:  Rinse for Imp. #1, #2 and 3: 0.1N Nitric Acid

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 13 of 24



# Table 4-3: Specifications for PM/Metals Sampling (EPA Method 29) (cont’d)

Item Specification

Laboratory

Particulate: Enthalpy Analytical – Durham, NC

Chromium: Element One - Wilmington, NC

Analysis

Particulate: Gravimetric as per Method 5 (MDL=0.1mg)

Filterable Chromium: (Front-Half)  Sample preparation of front-half samples as per USEPA Method 29

 After digestion of filter & probe rinse residue,

samples analyzed for total chromium on a PerkinElmer ELAN 6100 ICP-MS.

 Chromium Detection limit = 1.0 ug/L Vaporous Chromium: (Back-Half)  Sample preparation of back-half fraction as per USEPA Method 29

 Samples analyzed for total chromium on a

PerkinElmer ELAN 6100 ICP-MS.

 Chromium Detection limit = 1.0 ug/L

QA/QC  0.1N nitric acid reagent blank

 5% HNO 3 

# /10% H 2 

# O 2 

# reagent blank

 Acetone reagent blank

 Quartz fiber filter

 Duplicate analyses relative % difference (RPD)

 Spike sample recovery

 Second source calibration verification

Data Reporting

Volumetric Flow Rate (Qs):  Actual flow rate (Acfm) is product of average measured velocity (ft/s) and cross-sectional area (ft 2 

# ) of stack at sampling plane.

 Standard flow rate (Scfm) is Actual Flow rate

corrected to 68  ̊ F and 29.92 inches Hg

 Reference flow rate on a dry basis considers dry

gas fraction of effluent flow rate only (Water vapour mole fraction removed from the total)

Pollutant Concentration (Cs): Mass collected in aqueous sample (from Laboratory) divided by dry standard sample volume from test run (S.ft 3 

# or S.m 3 

# ).

Pollutant Mass Rate (Es):  Es = Cs x Qs

 l b/hr = mg/S.ft 3 

# x scfm x 60 min/hr / 454,000 mg/lb

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 14 of 24



# Figure 4-3: Sample Recovery – Method 29 Test Runs

Quartz Fiber
Filter Impinger Solutions and
Associated Rinses Nozzle/Probe & Glassware upstream of Quartz Filter

Clean thoroughly using
acetone and Teflon brush.
Recover into labeled 250 mLs glass bottle. Recover quartz filter
into labeled p etri dish.

Rinse with 0.1N
nitric acid and
recover in labeled
250 mLs p ol y bottle.

Rinse with water
and acetone and
discard solutions.



# Evaporate acetone to dryness
in clean tared container.

Weigh residue to constant weight (± 0.5 mg).

MDL = 0.1 mg Deliver Samples to Enthalpy for PM Analysis

Condition filters then

weigh to constant weight (± 0.5 mg).

MDL = 0.1 mg Rinse back of filter bell, impingers #1, #2 & #3 and connecting glassware 3 times with 0.1N HNO 3 

# into labeled 500 mLs poly bottle.

Digestion of sample fractions and subsequent an alysis of designated chromium as per EPA Method 29 (Chromium analysis and reporting based on separate front-half and back-half fractions) Deliver samples to Enthalpy for Chromium Anal y sis

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 15 of 24



# Figure 4-4: Schematic of EPA Method 29 Sampling Train

Temperature Sensors

Dry Gas

Meter

Manometer

Orifice Temperature Sensors

Air Tight Pump Main
Valve By-Pass 

# Valve

Vacuum Gauge 

## Silica Gel 100 mLs each of 5% HNO 3 

## / 10% H 2 

## O 2 

## Heated Glass
Probe Impingers

Ice
Bath S Type Pitot

Manometer

Heated
Filter

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 16 of 24



# 5. Test Results

Test results are presented in Tables 5-1 to 5-4. Detailed sampling data and effluent measurements are provided in the appendices.

Table 5-1: Summary of Method 0061 Test Results – DM1 Furnace DEP Outlet

Run #1 Run #2 Run #3

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average

08:27-12:55 08:03-11:49 07:52-11:22

Hexavalent Chromium
Concentration μ g/S.m 3 

# 2.9 2.9 2.1 2.7

Mass Rate lb./hr 8.8E-05 9.6E-05 6.7E-05 8.4E-05

Total Chromium
Concentration μ g/S.m 3 

# 4.1 5.1 5.4 4.9

Mass Rate lb./hr 1.3E-04 1.7E-04 1.7E-04 1.5E-04

Effluent Characteristics Avg. Stack Temperature  ̊ F 445 425 437 436
Stack Gas Pressure in Hg 29.32 29.70 29.65 29.56 Avg. Stack Gas Velocity ft/min 1.49E+03 1.52E+03 1.50E+03 1.50E+03
O 2 

# Concentration % vol 19.6 20.0 19.9 19.8
CO 2 

# Concentration % vol 4.9 4.7 4.8 4.8 Effluent Mol. Weight (dry) lb/mol 

# 29.6 29.5 29.6 29.6 Effluent Mol. Weight (wet) lb/mol 

# 28.3 28.4 28.3 28.3
Effluent Moisture Content % vol. 11.2 10.1 11.1 10.8 Dry Gas Fraction % vol. 88.8 89.9 88.9 89.2
Actual Effluent Flow Rate Acfm 1.60E+04 1.63E+04 1.62E+04 1.62E+04 Standard Flow Rate (wet) Scfm 9. 14E+03 9.66E+03 9.43E+03 9.41E+03 Standard Flow Rate (dry) Scfm 8.12E+03 8.69E+03 8.38E+03 8.40E+03

Sample Parameters Sample Period min 240.0 210.0 210.0 220.0 Sample Period Hours 4.0 3.5 3.5 3.7
Hexavalent Chromium μ g 10.8 10.1 7.2 9.3
Total Chromium μ g 15.4 17.4 18.2 17.0 Dry Standard Sample Volume Scf 131.27 120.81 118.57 123.55 Average Delta P in H 2 

# O 0.13 0.14 0.13 0.13 Average Delta H in H 2 

# O 1.01 1.09 1.04 1.05 Average Sample Rate cfm 0.55 0.57 0.56 0.56 Average Isokinetic Variation % 99.9 98.1 99.6 99.2

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 17 of 24



# Table 5-2: Summary of Method 0061 Test Results – DM2 Furnace DEP Outlet

Run #1 Run #2 Run #3

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average

08:27-12:55 08:03-11:49 07:52-11:22

Hexavalent Chromium
Concentration μ g/S.m 3 

# 37 40 29 36

Mass Rate lb./hr 1.2E-03 1.3E-03 9.3E-04 1.1E-03

Total Chromium
Concentration μ g/S.m 3 

# 42 47 35 41

Mass Rate lb./hr 1.4E-03 1.5E-03 1.1E-03 1.3E-03

Effluent Characteristics Avg. Stack Temperature  ̊ F 414 414 420 416
Stack Gas Pressure in Hg 29.58 29.98 29.91 29.82 Avg. Stack Gas Velocity ft/min 1.51E+03 1.43E+03 1.47E+03 1.47E+03
O 2 

# Concentration % vol 20.0 20.1 20.0 20.0
CO 2 

# Concentration % vol 4.21 4.70 4.40 4.44 Effluent Mol. Weight (dry) lb/mol 

# 29.5 29.6 29.5 29.5 Effluent Mol. Weight (wet) lb/mol 

# 28.3 28.4 28.3 28.3
Effluent Moisture Content % vol. 10.2 10.0 10.4 10.2 Dry Gas Fraction % vol. 89.8 90.0 89.6 89.8
Actual Effluent Flow Rate Acfm 1.62E+04 1.54E+04 1.58E+04 1.58E+04 Standard Flow Rate (wet) Scfm 9. 67E+03 9.32E+03 9.45E+03 9.48E+03 Standard Flow Rate (dry) Scfm 8.68E+03 8.39E+03 8.47E+03 8.52E+03

Sample Parameters Sample Period min 240.0 210.0 210.0 220.0 Sample Period Hours 4.0 3.5 3.5 3.7
Hexavalent Chromium μ g 143 131 95.3 123
Total Chromium μ g 161 152 113 142 Dry Standard Sample Volume Scf 135.95 114.49 115.21 121.88 Average Delta P in H 2 

# O 0.14 0.13 0.13 0.13 Average Delta H in H 2 

# O 1.18 1.08 1.11 1.12 Average Sample Rate cfm 0.57 0.54 0.54 0.55 Average Isokinetic Variation % 99.7 99.4 99.0 99.4

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 18 of 24



# Table 5-3: Summary of Method 29 Test Results – DM1 Furnace DEP Outlet

Run #1 Run #2 Run #3

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average

13:45-17:45 12:25-16:25 12:12-16:12

Filterable Particulate
Concentration mg/S.m 3 

# 1.5 1.7 1.3 1.5

Mass Rate lb./hr 

# 0.045 0.052 0.039 0.045

Filterable Chromium
Concentration μ g/S.m 3 

# 5.1 4.5 4.8 4.8

Mass Rate lb./hr 

# 1.5E-04 1.4E-04 1.4E-04 1.4E-04

Condensable Chromium

Concentration μ g/S.m 3 

# 0.15 0.15 0.10 0.14

Mass Rate lb./hr 

# 4.7E-06 4.7E-06 3.1E-06 4.1E-06

Total Chromium

Concentration μ g/S.m 3 

# 5.2 4.7 4.9 4.9

Mass Rate lb./hr 

# 1.6E-04 1.4E-04 1.5E-04 1.5E-04

Effluent Characteristics Avg. Stack Temperature  ̊ F 

# 439 433 446 439
Stack Gas Pressure in Hg 

# 29.35 29.71 29.60 29.56 Avg. Stack Gas Velocity ft/min 

# 1.45E+03 1.44E+03 1.45E+03 1.45E+03
O 2 

# Concentration % vol. 

# 19.7 19.9 19.9 19.8
CO 2 

# Concentration % vol. 

# 4.5 4.9 4.8 4.73 Effluent Mol. Weight (dry) lb/mol 

# 29.5 29.6 29.6 29.6 Effluent Mol. Weight (wet) lb/mol 

# 28.3 28.4 28.3 28.3
Effluent Moisture Content % vol. 

# 10.6 10.5 10.9 10.6 Dry Gas Fraction % vol. 

# 89.4 89.5 89.1 89.4
Actual Effluent Flow Rate Acfm 

# 1.56E+04 1.55E+04 1.56E+04 1.56E+04 Standard Flow Rate (wet) Scfm 

# 9.00E+03 9.11E+03 8.97E+03 9.03E+03 Standard Flow Rate (dry) Scfm 

# 8.048E+03 8.16E+03 8.00E+03 8.07E+03

Sample Parameters Sample Period min 

# 240.0 240.0 240.0 240.0 Sample Period Hours 

# 4.0 4.0 4.0 4.0 Filterable PM (Acetone) mg 

# 2.7 3.1 3.1 3.0 Filterable PM (Filter) mg 

# 3.5 4.0 2.3 3.3
Filterable Chromium μ g 

# 21.2 19.0 19.8 20.0
Condensable Chromium μ g 

# 0.6 0.6 0.4 0.6 Dry Standard Sample Volume Scf 

# 147.17 148.44 146.74 147.45 Average Delta P In H 2 

## O 

# 0.11 0.11 0.11 0.11 Average Delta H in H 2 

## O 

# 1.28 1.26 1.22 1.25 Average Sample Rate cfm 

# 0.62 0.61 0.59 0.61 Average Isokinetic Variation % 

# 99.1 98.6 99.5 99.0

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 19 of 24



# Table 5-4: Summary of Method 29 Test Results – DM2 Furnace DEP Outlet

Run #1 Run #2 Run #3

Test Parameters 24-Jan-12 25-Jan-12 26-Jan-12 Average

13:45-18:00 12:25-16:25 12:12-16:12

Filterable Particulate
Concentration mg/S.m 3 

# 8.8 7.6 7.2 7.9

Mass Rate lb./hr 

# 0.27 0.24 0.22 0.25

Filterable Chromium
Concentration μ g/S.m 3 

# 46 41 35 41

Mass Rate lb./hr 

# 1.4E-03 1.3E-03 1.1E-03 1.3E-03

Condensable Chromium

Concentration μ g/S.m 3 

# 0.18 0.21 0.26 0.22

Mass Rate lb./hr 

# 5.6E-06 6.7E-06 8.1E-06 6.8E-06

Total Chromium

Concentration μ g/S.m 3 

# 46 41 35 41

Mass Rate lb./hr 

# 1.4E-03 1.3E-03 1.1E-03 1.3E-03

Effluent Characteristics Avg. Stack Temperature  ̊ F 

# 426 421 437 428
Stack Gas Pressure in Hg 

# 29.62 29.97 29.85 29.81 Avg. Stack Gas Velocity ft/min 

# 1.46E+03 1.45E+03 1.47E+03 1.46E+03
O 2 

# Concentration % vol. 

# 20.0 20.2 20.1 20.1
CO 2 

# Concentration % vol. 

# 4.4 4.6 4.5 4.49 Effluent Mol. Weight (dry) lb/mol 

# 29.5 29.5 29.5 29.5 Effluent Mol. Weight (wet) lb/mol 

# 28.3 28.4 28.3 28.3
Effluent Moisture Content % vol. 

# 10.2 9.93 10.5 10.2 Dry Gas Fraction % vol. 

# 89.8 90.1 89.5 89.8
Actual Effluent Flow Rate Acfm 

# 1.57E+04 1.56E+04 1.58E+04 1.57E+04 Standard Flow Rate (wet) Scfm 

# 9.28E+03 9.39E+03 9.28E+03 9.32E+03 Standard Flow Rate (dry) Scfm 

# 8.33E+03 8.46E+03 8.30E+03 8.36E+03

Sample Parameters Sample Period min 

# 240.0 240.0 240.0 240.0 Sample Period Hours 

# 4.0 4.0 4.0 4.0 Filterable PM (Acetone) mg 

# 1.1 2.7 3.5 2.4 Filterable PM (Filter) mg 

# 35.3 30.8 27.7 31.3
Filterable Chromium μ g 

# 191.0 180.0 151.0 174.0
Condensable Chromium μ g 

# 0.8 0.9 1.1 0.9 Dry Standard Sample Volume Scf 

# 146.84 154.98 153.25 151.69 Average Delta P In H 2 

## O 

# 0.11 0.12 0.12 0.11 Average Delta H in H 2 

## O 

# 1.40 1.53 1.45 1.46 Average Sample Rate cfm 

# 0.61 0.63 0.62 0.62 Average Isokinetic Variation % 

# 99.3 98.7 99.5 99.1

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 20 of 24



# 6. Discussion of Results

6 .1 General

 Reported emission dat a are believed to be representative of the stack conditions at the time of testing. The sampling program was not witnessed by the New York State DEC.

 Sample recoveries were carried out in a clean, temperature controlled room to maximize efficiency and prevent contamination. Train preparation and sample recovery were conducted by a single sample recovery specialist to maintain the highest level of consistency.

 There was good communication between the LEHDER field crew and Owens Corning during the sampling campaign. Mr. Rick Cooper of the Owens Corning corporate environmental department was the liaison between the process and the LEHDER field crew. Pertinent process/production data were collected throughout the sampling campaign by Owens Corning personnel. Sampling was initiated only when process conditions and production rates were reported to be at required levels.

 An assessment of cyclonic flow was carried out on Tuesday, January 23, 2012. The
assessment found that both sources were within the EPA Method 1 criteria of 20% cyclonic flow or less.

 Th e test runs for both methods were initially set for 240 minutes. After the first test, the final pH of the KOH solution in the first impinger was at 8.5. A pH below 8.5 deems the test run invalid. To reduce the chance of an invalid test, the sample duration for Runs #2 and #3 were cut to 210 minutes. All subsequent test runs reported final solution pH values above 8.5. Factors contributing to the declining pH of the test period are: higher effluent moisture content that dilutes the contents of the first impinger and elevated CO 2 

# concentrations. The CO 2 

# concentrations measured from the DM1 and DM2 Furnace DEP Outlets ranged from 4.5% to 4.9%.

6.2 Particulate Emission Summary

Particulate data was obtained from the front-half of the Method 29 train . Front-half sample fractions were recovered, analyzed and reported in accordance with the procedures described in USEP Method 5. A summary of the particulate concentrations and mass rates is presented in Table 6-1.

Table 6-1: Average Particulate Test Results – DM1 & DM2 Furnace DEP Outlets

Source Concentration mg/S.m 3 

# Mass Rate lb/hr

DM1 Furnace DEP Outlet 1.5 0.045

DM2 Furnace DEP Outlet 7.9 0.25

Total from Common DEP Stack 0.30

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 21 of 24



# 6 .3 Total Chromium - Method 29 vs. Method 0061

 To tal chromium concentrations and mass rates were measured from the DM1 and DM2 Furnace DEP Outlets using two test methods: USEPA Method 29 and 0061. Sampling was not conducted simultaneously, however, one of each test types were completed each day for each of the two sites. A comparison of the two sets of data is presented in Table 6-2. The total chromium data show are very good correlation between the two test methods for low and higher chromium concentrations.

Table 6-2: Total Chromium Data – Method 29 vs. Method 0061

Total Chromium

Concentration Mass Rate

M29 M0061 Difference M29 M0061 Difference Stack Run
#

ug/S.m 3 

# ug/S.m 3 

# % lb/hr lb/hr %

1 5.2 4.1 -21% 1.6E -04 1.3E-04 -19%

2 4.7 5.1 9% 1.4E-04 1.7E-04 21%

3 4.9 5.4 10% 1.5E-04 1.7E-04 13% DM1 Furnace DEP Outlet

Avg. 4.9 4.9 0% 1.5E-04 1.5E-04 0%

1 46 42 -9% 1.4E-03 1.4E-03 0%

2 41 47 15% 1.3E-03 1.5E-03 15%

3 35 35 0% 1.1E-03 1.1E-03 0% DM2 Furnace DEP Outlet

Avg. 41 41 0% 1.3E-03 1.3E-03 0%

% Difference from M29 value = {(M0061 value – M29 value) / M29 value} x 100%

% Difference = “0” when M0061 value = M29 value



# 6 .4 Method 0061 Hexavalent and Total Chromium Data

 Method 0061 is typically used for the determi nation of hexavalent chromium e missions only. However, the Section 114 request requires that both hexavalent and total chromium be analyzed for all test runs. To determine total chromium from the train, an extra recovery step is required in the field. This involves rinsing the train components with 0.1N nitric acid and recovering the acetate filter used during post-test processing. The acid rinse is collected along with the filter and submitted for total chromium analysis only. The recovered KOH solution is also analyzed for total chromium.

 Hexavalent and total chromium are analyzed using two different analytical techniques. The hexavalent chromium analytical method is approximately 10 times more sensitive than the total chromium technique. If hexavalent chromium represents a high fraction of the total chromium, the difference in analytical sensitivity could result in hexavalent chromium appearing to be greater than 100% of the total.

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 22 of 24



#  The impinger solution used for this campaign was 0.5N KOH which is the strongest normality identified for use in Method 0061. The stronger normality was used to ensure that the final pH of the impinger solution was above the required 8.5. The consequences of the stronger KOH solution are: higher chromium levels in the blank, and a higher potential for interferences that could affect the total chromium analysis. For this reason, there is a level of uncertainty attached to total chromium data when a higher normality KOH solution is used. The laboratory has indicated a higher level of confidence with hexavalent chromium analysis even with the stronger KOH solution.

 As indicated in Section 6.1 above, provisions were taken to ensure the post-test pH of the KOH solution met the criterion of greater than 8.5. First, it was decided to increase the initial volume of 0.5N KOH in the first impinger from 300 mLs to 350 mLs. This modification was also beneficial for maintaining an appropriate aqueous volume in the first impinger for recirculation of the KOH solution in the probe. This has purportedly been an issue when using Method 0061 to sample hot stacks. In addition, the sampling period was reduced from 240 minutes to 210 minutes for Test Runs #2 and #3 at both sites.

 To address the relative high effluent gas temperatures (i.e. ~425  ̊ F), a glass probe liner was used instead of Teflon® one. The glass probe liners were modified by fusing an appropriately sized glass extraction nozzle on the end of the liner. The size of the nozzle was selected based on preliminary effluent measurements made from both sites prior to the start of the sampling campaign. The probe/impinger transition was also glass. All other parts between the transition and the silica gel were constructed of Teflon®.

 A s ummary of the Method 0061 data from the DM1 and DM2 Furnace DEP Oultets is presented in Table 6-3. Both the total and hexavalent chromium data were blank corrected. Based on the data, the fraction of total chromium that is hexavalent appears to vary significantly at lower chromium concentrations (DM1 test runs). The ratio is more consistent for the higher chromium concentrati ons (DM2 test runs). This variability may be due to difference in sensitivity between the chromium and hexavalent chromiumanalytical methods, and the uncertainty factors associated with measuring very low instack chromium concentrations.

Table 6-3: Method 0061 – Hexavalent Chromium vs. Total Chromium

Method 0061

Concentration, μ g/S.m 3 

# Mass Rate, lb/hr Stack Run
# Date
2012 Hex. Cr Total Cr Hex. Cr Total Cr % Hex Cr. Of Total Cr

1 24-Jan 2.9 4.1 8. 8E-05 1.3E-04 70%

2 25-Jan 2.9 5.1 9. 6E-05 1.7E-04 58%

3 26-Jan 2.1 5.4 6. 7E-05 1.7E-04 39% DM1 Furnace DEP Outlet

Avg. 2.7 4.9 8.4E-05 1.5E-04 54%

1 24-Jan 37.2 41.8 1. 2E-03 1.4E-03 89%

2 25-Jan 40.5 46.9 1. 3E-03 1.5E-03 86%

3 26-Jan 29.2 34.7 9. 3E-04 1.1E-03 84% DM2 Furnace DEP Outlet

Avg. 35.6 41.1 1.1E-03 1.3E-03 87%

% Hex. Chromium = (Hex. Chromium Value / Total Chromium Value) x 100%

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 23 of 24



# 6.5 QA/QC

 All Teflon train parts employed for sampling were cleaned with soap and water, rinsed three times with distilled water and acid soaked overnight. After cleaning all parts were sealed prior to use. This cleaning process ensured that the train components were free of contamination before they were used for this project.

 Based on the analytical reports provided by the laboratories, Method 0061 field blanks of the 0.5N KOH showed relatively high blank levels of total and hexavalent chromium compared to the stack samples. The hexavalent chromium measured in the KOH reagent blank was 1.72 ug (based on 350 mLs aqueous volume). Total chromium measured in the 0.5 KOH blank was 3.14 μ g (based on 350 mLs aqueous volume). Since the aqueous volume of the blank was the same as the starting volume of 0.5N KOH in the train, the blank volume was simply subtracted from the uncorrected chromium analysis.

 Analysis of duplicates and laboratory spikes were within applicable requirements. The laboratory analytical reports are furnished in Appendix B.

 As discussed above, the sample period for the Method 0061 test runs was reduced from 240 minutes to 210 minutes for Runs #2 and #3. The reason for this change was to prevent an invalid test caused by a post-test pH less than 8.5 in the first impinger. The reduction in sample period resulted in final gas volumes that were less than the minimum threshold of 120 dscf (See Table 5-1 and 5-2). The reduced sample volumes did not appear to affect the representative quality of the data as all test runs reported chromium
and hexavalent chromium that were well above detection limits.

 The temperature of the effluent gases was measured to be approximately 425  ̊ F. This is near or exceeds the physical integrity of Teflon®. To address this, a glass probe liner was
selected in lieu of a Teflon one for the Method 0061 train. This modification was communicated to Mr. Stef Johnson of the USEPA prior to the start of the sampling

program.

 For the Method 0061 train, an air-cooled probe unit was used to maintain a probe temperature that would not vaporize the reci rculated KOH solution. The air blower moved air through the probe at a rate greater than 5 cfm. No problems were encountered in the use of this equipment or with maintaining the KOH in liquid form through the entire sampling period.

 The moisture content of the effluent gas stream was determined for each test in accordance with the procedures described in EPA Method 4. The moisture content for
each stack was less than 100% saturation.

 Sample line leak checks were conducted before and after each test. Sampling did not proceed until the integrity of the sampling train was validated. All final leak checks were well within the criterion of 0.020 cfm at the highest vacuum recorded during the test run.
Pitot tube leak checks were conducted before each isokinetic test run.



#  The isokinetic sampling rate was calculated for each point and routinely checked. Consequently, all reported average and point by point isokinetic variations are within the specification of 100%  10%.

# Section 114 ICR Test Repo rt February 25, 2012 Owens Corning Delmar Plant – DM1 & DM2 Furnace DEP Outlets Project No. 123987 Page 24 of 24



#  Pitot tube, dry gas meter and thermocouple calibrations are furnished in Appendix C. Pitot tubes were calibrated in a wind tunnel at LEHDER’s office in Point Edward, Ontario. Calibrations were made with various nozzle sizes attached. The Cp factor for the specific nozzle size was employed for each test. Pre and post calibrations of the dry gas meters were calibrated with critical orifices.



# 7. Closure

The data presented in this report are believed accurate and representative of the effluent conditions at the time of testing and the result of best efforts in the field. Comments pertaining to the data or to anomalies in the data are made without bias and are based on experience and technical judgment.

Respectfully submitted,

LEHDER Environmental Services Limited

Michael Denomme Peter Pakalnis, QSTI Project Manager Principal

# Appendix A

Concentration and Mass Rate Calculations

A.1: Method 29 Test Runs

A.2: Method 0061 Test Runs

# Appendix A.1

Method 29 Test Runs

# 123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xls



# LEHDER Environmental Services Ltd Revised by: M.Denomme

Date: 16-Feb-12 

# Company: Owens Corning


# Plant: Delmar, NY 

# Stack: DM1 DEP Outlet


# Pollutant: TSP / Chromium


# Method: EPA Method 29 

# Project No.: 123987 

# Operators RS / JH / JT 

# Data Entry: KH / JE 

# Reviewed By: MD

Ref.Temperature: 68 deg. F
Ref. Pressure: 29.92 "Hg
Molar Volume: 24.04 l/mol



# Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

13:45 - 17:45 12:25 - 16:25 12:12 - 16:12 No. of Sample Points 30 30 30 Sample Time /Point min 8.0 8.0 8.0 Reading / Point min 4.0 4.0 4.0 Total Sample Time, min 240.0 240.0 240.0 Barometric Pressure, Pb "Hg 29.69 30.04 29.91 Stack Gauge Pressure, Pgauge "H 2 

# O -4.56 -4.46 -4.23 Absolute Stack Pressure, Ps "Hg 29.35 29.71 29.60 Pitot Tube Coefficient, Cp 0.813 0.813 0.813 Oxygen Content, O2 % 19.7 19.9 19.9 Carbon Dioxide Content, CO2 % 4.5 4.9 4.8 Carbon Monoxide Content, CO % 0.0 0.0 0.0 Nitrogen Content, N2 % 75.8 75.2 75.3 Condensate Collected, W H2O 

# g 368.2 369.1 379.6 Nozzle Diameter, Dn in 0.3897 0.3897 0.3897 Initial DGM Reading ft 3 

# 72.384 36.877 98.140 Final DGM Reading ft 3 

# 218.375 181.214 239.000 DGM Unity, Y 1.0123 1.0123 1.0123
Stack Width ft 3.280 3.280 3.280 Stack Depth ft 3.280 3.280 3.280 Actual Volume of Dry Gas ft 3 

# 147.7867 146.1123 142.5926
Stack Area, As ft 2 

# 10.758 10.758 10.758



# Particulate/Chromium Analysis

Front-Half Acetone Residue mg 2.7 3.1 3.1 Filter Loading mg 3.5 4.0 2.3 Total Suspended PM mg 6.2 7.1 5.4

Front-Half (Filterable) Chromium μ g 21.2 19.0 19.8 Condensable (Back-Half) Chromium μ g 0.64 0.64 0.43
Total Chromium μ g 21.8 19.6 20.2

Input1123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xlsLEHDER Environmental Services LtdPoint by Point Sampling DataCompany:Owens CorningPlant:Delmar, NYStack:DM1 DEP OutletPollutant:TSP / ChromiumProject No.:123987Test #1Test #2Test #324-Jan-1225-Jan-1226-Jan-1213:45 - 17:4512:25 - 16:2512:12 - 16:12Time Vd Delta P Delta H Ts Tmi TmoTime Vd Delta P Delta H Ts Tmi TmoTime Vd Delta P Delta H Ts Tmi Tmo# minft3H2O H2OF F F # minft3H2O H2OF F F # minft3H2O H2OFFFP1-1 0.0 72.38 0.13 1.47 452 66 66P1-1 0.0 36.88 0.15 1.65 434 61 64P1-10.0 98.14 0.14 1.50 456 52 554.0 74.81 0.15 1.70 452 66 664.0 39.40 0.16 1.80 437 61 634.0 100.67 0.14 1.50 456 52 552 8.0 77.58 0.13 1.50 451 67 672 8.0 42.23 0.13 1.45 435 61 6328.0 103.27 0.12 1.30 456 52 5512.0 80.19 0.12 1.35 448 67 6712.0 44.80 0.13 1.45 435 62 6312.0 105.72 0.12 1.30 454 52 553 16.0 82.75 0.11 1.25 447 67 673 16.0 47.39 0.13 1.44 435 62 63316.0 108.10 0.12 1.30 450 53 5420.0 85.14 0.11 1.25 446 67 6720.0 50.00 0.13 1.44 436 62 6320.0 110.50 0.12 1.30 451 51 544 24.0 87.60 0.11 1.25 446 68 674 24.0 52.58 0.12 1.35 434 62 64424.0 112.92 0.11 1.20 450 53 5428.0 90.02 0.12 1.35 447 68 6828.0 55.06 0.12 1.35 435 62 6428.0 115.38 0.11 1.20 451 54 545 32.0 92.51 0.12 1.35 448 68 685 32.0 57.56 0.12 1.35 436 62 64532.0 117.71 0.12 1.30 450 54 5436.0 94.99 0.12 1.35 449 68 6836.0 60.07 0.12 1.33 436 61 6436.0 120.11 0.12 1.30 454 54 546 40.0 97.51 0.12 1.35 443 68 686 40.0 62.58 0.11 1.25 430 61 64640.0 122.55 0.11 1.20 454 54 5444.0 100.03 0.12 1.35 443 68 6844.0 64.97 0.13 1.45 438 61 6444.0 124.84 0.12 1.30 454 55 55P2-1 48.0 102.50 0.14 1.60 447 68 68P2-1 48.0 67.44 0.13 1.45 435 62 64P2-148.0 127.23 0.13 1.40 454 55 5552.0 105.04 0.14 1.60 448 68 6952.0 69.92 0.14 1.55 435 62 6452.0 129.72 0.14 1.50 452 55 552 56.0 107.77 0.10 1.15 445 68 692 56.0 72.50 0.10 1.10 435 62 64256.0 132.28 0.11 1.20 450 55 5560.0 110.14 0.10 1.15 444 68 6960.0 74.79 0.11 1.20 433 62 6460.0 134.75 0.11 1.20 450 55 543 64.0 112.47 0.09 1.00 441 68 693 64.0 77.16 0.10 1.10 432 62 64364.0 137.15 0.10 1.10 450 55 5568.0 114.64 0.09 1.00 440 68 6968.0 79.43 0.10 1.10 431 62 6468.0 139.44 0.10 1.10 448 55 554 72.0 116.84 0.10 1.15 440 68 694 72.0 81.78 0.11 1.20 431 62 64472.0 141.65 0.11 1.20 447 56 5576.0 119.15 0.10 1.15 441 68 6976.0 84.17 0.11 1.20 432 62 6476.0 144.01 0.11 1.20 446 56 555 80.0 121.47 0.12 1.35 444 68 695 80.0 86.54 0.12 1.30 434 62 64580.0 146.32 0.12 1.30 449 56 5684.0 124.00 0.12 1.35 444 68 6984.0 89.00 0.12 1.30 436 62 6484.0 148.78 0.12 1.30 450 56 566 88.0 126.51 0.10 1.15 444 68 696 88.0 91.51 0.13 1.50 437 63 64688.0 151.19 0.12 1.30 452 56 5692.0 128.86 0.09 1.00 445 68 6992.0 94.04 0.10 1.10 437 63 6492.0 153.70 0.12 1.30 452 56 56P3-1 96.0 131.14 0.11 1.25 445 68 69P3-1 96.0 96.34 0.12 1.35 435 62 64P3-196.0 156.10 0.12 1.30 450 56 56100.0 133.38 0.12 1.35 442 66 68100.0 98.65 0.12 1.35 435 62 64100.0 158.53 0.12 1.30 449 56 562 104.0 135.88 0.10 1.15 438 66 682 104.0 101.10 0.10 1.10 432 62 642104.0 160.94 0.10 1.10 449 56 56108.0 138.28 0.09 1.00 438 67 68108.0 103.48 0.10 1.10 432 62 64108.0 163.25 0.10 1.10 445 56 563 112.0 140.52 0.09 1.05 433 67 683 112.0 105.76 0.10 1.10 432 61 643112.0 165.48 0.09 1.00 445 56 56116.0 142.670.09 1.05 434 67 68116.0 108.03 0.10 1.10 428 61 64116.0 167.59 0.09 1.00 441 55 564 120.0 144.89 0.09 1.05 435 67 684 120.0 110.30 0.10 1.10 428 61 644120.0 169.74 0.09 1.00 442 55 56124.0 147.12 0.09 1.05 435 67 68124.0 112.60 0.10 1.10 428 62 64124.0 171.90 0.09 1.00 442 55 555 128.0 149.32 0.10 1.15 439 67 685 128.0 114.89 0.11 1.25 428 62 645128.0 174.01 0.09 1.00 444 54 55132.0 151.61 0.10 1.15 440 67 68132.0 117.26 0.10 1.10 428 62 64132.0 176.18 0.10 1.10 446 54 556 136.0 153.88 0.09 1.05 435 68 686 136.0 119.59 0.10 1.10 435 62 646136.0 178.46 0.11 1.20 449 54 55140.0 156.16 0.10 1.15 430 68 68140.0 121.89 0.10 1.10 437 62 64140.0 180.73 0.11 1.20 449 54 55P4-1 144.0 158.50 0.11 1.25 435 68 68P4-1 144.0 124.13 0.12 1.35 435 62 64P4-1144.0 183.07 0.12 1.30 449 54 54148.0 160.71 0.12 1.36 441 68 68148.0 126.48 0.12 1.35 436 62 64148.0 185.49 0.12 1.30 449 54 542 152.0 163.22 0.11 1.25 437 69 692 152.0 128.95 0.11 1.20 433 63 642152.0 187.86 0.11 1.20 445 54 54156.0 165.62 0.11 1.25 437 69 69156.0 131.35 0.11 1.20 433 63 64156.0 190.23 0.11 1.20 444 54 543 160.0 168.02 0.12 1.40 437 69 693 160.0 133.71 0.10 1.10 433 63 643160.0 192.54 0.10 1.10 440 54 54164.0 170.48 0.11 1.25 433 69 69164.0 136.00 0.10 1.10 429 63 64164.0 194.78 0.10 1.10 440 54 544 168.0 172.88 0.11 1.25 434 69 694 168.0 138.27 0.10 1.10 430 63 644168.0 197.02 0.09 1.00 440 54 54172.0 175.39 0.11 1.25 435 68 69172.0 140.53 0.10 1.10 430 63 64172.0 199.24 0.09 1.00 440 54 545 176.0 177.89 0.11 1.25 436 68 695 176.0 142.80 0.10 1.10 434 64 655176.0 201.38 0.10 1.10 443 54 54180.0 180.34 0.11 1.25 439 67 69180.0 145.10 0.10 1.10 435 64 65180.0 203.50 0.10 1.10 443 54 546 184.0 182.76 0.09 1.05 432 67 696 184.0 147.38 0.10 1.10 436 64 656184.0 205.72 0.10 1.10 444 54 54188.0 185.01 0.10 1.15 438 67 69188.0 149.67 0.10 1.10 436 64 65188.0 207.94 0.10 1.10 445 54 54P5-1 192.0 187.26 0.14 1.60 438 66 69P5-1 192.0 151.88 0.13 1.45 435 64 65P5-1192.0 210.18 0.11 1.20 445 54 54196.0 189.82 0.15 1.70 438 66 69196.0 154.40 0.11 1.20 435 64 65196.0 212.51 0.14 1.50 444 54 542 200.0 192.67 0.14 1.60 437 66 682 200.0 156.83 0.11 1.20 435 64 652200.0 215.13 0.13 1.40 442 54 54204.0 195.39 0.14 1.60 436 66 68204.0 159.19 0.10 1.10 430 64 65204.0 217.60 0.13 1.40 441 54 543 208.0 198.13 0.10 1.15 431 66 683 208.0 161.43 0.12 1.35 425 64 653208.0 220.11 0.10 1.10 438 54 54212.0 200.46 0.10 1.15 427 66 68212.0 164.02 0.11 1.25 425 64 65212.0 222.40 0.10 1.10 438 54 544 216.0 202.78 0.12 1.40 426 66 684 216.0 166.42 0.12 1.35 427 64 654216.0 224.61 0.11 1.20 438 54 54220.0 205.29 0.12 1.40 427 66 68220.0 168.90 0.12 1.35 428 64 66220.0 226.89 0.11 1.20 435 54 545 224.0 207.84 0.13 1.50 428 67 685 224.0 171.44 0.12 1.35 428 64 665224.0 229.25 0.12 1.30 436 53 54228.0 210.42 0.13 1.50 429 67 68228.0 173.96 0.13 1.45 428 65 66228.0 231.64 0.12 1.30 437 53 546 232.0213.08 0.13 1.50 429 67 686 232.0 176.57 0.10 1.15 424 65 666232.0 234.10 0.12 1.30 436 53 54236.0 215.75 0.12 1.40 428 67 68236.0 178.95 0.10 1.15 425 65 66236.0 236.53 0.12 1.30 436 52 53240.0218.375240.0181.21240.0239.00Input2123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xlsLEHDER Environmental Services LtdPoint by Point CalculationsCompany:Owens CorningPlant:Delmar, NYStack:DM1 DEP OutletPollutant:TSP / ChromiumProject No.:Data Entry:KH / JEPoint PeriodIsokinecity Point PeriodIsokinecity Point TimeIsokinecityminm3ft3m/s ft/s %minm3ft3m/s ft/s %minm3ft3m/s ft/s %P1-14.0 0.069 2.45 8.0 26.3 92.4P1-14.0 0.072 2.55 8.5 27.7 89.9P1-14.0 0.073 2.56 8.3 27.2 96.24.0 0.079 2.80 8.6 28.2 98.5 4.0 0.081 2.86 8.7 28.7 98.0 4.0 0.074 2.63 8.3 27.2 98.724.0 0.075 2.64 8.0 26.2 99.424.0 0.074 2.60 7.9 25.8 98.324.0 0.070 2.49 7.7 25.2 100.84.0 0.074 2.60 7.7 25.2 101.4 4.0 0.074 2.63 7.9 25.8 99.4 4.0 0.068 2.41 7.7 25.1 97.634.0 0.068 2.41 7.3 24.1 98.434.0 0.075 2.64 7.9 25.8 99.934.0 0.069 2.43 7.6 25.1 98.24.0 0.071 2.50 7.3 24.1 101.7 4.0 0.074 2.61 7.9 25.8 98.7 4.0 0.069 2.44 7.7 25.1 99.144.0 0.069 2.44 7.3 24.1 99.544.0 0.071 2.51 7.6 24.8 98.744.0 0.071 2.50 7.3 24.0 105.34.0 0.071 2.52 7.7 25.2 98.2 4.0 0.072 2.54 7.6 24.8 99.7 4.0 0.067 2.36 7.3 24.0 99.554.0 0.071 2.51 7.7 25.2 97.954.0 0.072 2.54 7.6 24.8 100.054.0 0.069 2.43 7.6 25.1 98.14.0 0.072 2.55 7.7 25.2 99.5 4.0 0.072 2.54 7.6 24.8 99.9 4.0 0.070 2.47 7.7 25.1 100.064.0 0.072 2.55 7.7 25.1 99.264.0 0.069 2.42 7.2 23.7 99.464.0 0.066 2.32 7.3 24.1 98.04.0 0.071 2.51 7.7 25.1 97.4 4.0 0.071 2.50 7.9 25.9 94.7 4.0 0.069 2.42 7.7 25.1 97.7P2-14.0 0.073 2.57 8.3 27.2 92.6P2-14.0 0.071 2.51 7.9 25.8 94.7P2-14.0 0.071 2.52 8.0 26.2 97.64.0 0.078 2.77 8.3 27.2 99.9 4.0 0.074 2.62 8.2 26.8 95.3 4.0 0.073 2.59 8.3 27.1 96.824.0 0.068 2.39 7.0 22.9 101.924.0 0.066 2.31 6.9 22.6 99.624.0 0.071 2.51 7.3 24.0 105.44.0 0.067 2.36 7.0 22.9 100.6 4.0 0.068 2.40 7.2 23.7 98.6 4.0 0.069 2.42 7.3 24.0 102.134.0 0.062 2.20 6.6 21.7 98.334.0 0.065 2.30 6.9 22.6 98.834.0 0.066 2.32 7.0 22.9 102.34.0 0.063 2.23 6.6 21.7 99.7 4.0 0.067 2.38 6.9 22.6 102.2 4.0 0.063 2.24 7.0 22.9 98.644.0 0.066 2.34 7.0 22.9 99.544.0 0.069 2.42 7.2 23.7 99.144.0 0.068 2.39 7.3 24.0 100.54.0 0.066 2.34 7.0 22.9 99.6 4.0 0.068 2.40 7.2 23.7 98.3 4.0 0.066 2.34 7.3 24.0 98.154.0 0.073 2.56 7.7 25.1 99.654.0 0.070 2.49 7.6 24.8 97.754.0 0.071 2.49 7.6 25.1 100.14.0 0.072 2.54 7.7 25.1 98.8 4.0 0.072 2.55 7.6 24.8 100.2 4.0 0.069 2.43 7.6 25.1 97.964.0 0.067 2.38 7.0 22.9 101.264.0 0.073 2.56 7.9 25.9 96.864.0 0.072 2.55 7.7 25.1 102.54.0 0.065 2.31 6.6 21.8 103.6 4.0 0.066 2.32 6.9 22.7 100.0 4.0 0.069 2.43 7.7 25.1 97.8P3-14.0 0.064 2.26 7.3 24.1 91.9P3-14.0 0.066 2.34 7.6 24.8 92.2P3-14.0 0.070 2.45 7.6 25.1 98.74.0 0.072 2.53 7.6 25.1 98.5 4.0 0.070 2.48 7.6 24.8 97.5 4.0 0.069 2.44 7.6 25.1 98.324.0 0.069 2.43 7.0 22.9 103.624.0 0.068 2.41 6.9 22.6 103.624.0 0.066 2.34 7.0 22.9 102.94.0 0.064 2.27 6.6 21.7 101.5 4.0 0.065 2.31 6.9 22.6 99.2 4.0 0.064 2.25 7.0 22.8 98.934.0 0.062 2.18 6.6 21.6 97.234.0 0.065 2.29 6.9 22.6 98.634.0 0.060 2.14 6.6 21.7 98.94.0 0.064 2.25 6.6 21.6 100.4 4.0 0.065 2.30 6.9 22.6 98.9 4.0 0.062 2.18 6.6 21.6 100.844.0 0.064 2.25 6.6 21.6 100.744.0 0.066 2.33 6.9 22.6 99.944.0 0.062 2.19 6.6 21.6 101.14.0 0.063 2.23 6.6 21.6 99.6 4.0 0.066 2.31 6.9 22.6 99.2 4.0 0.060 2.14 6.6 21.6 98.954.0 0.066 2.32 7.0 22.9 98.854.0 0.068 2.40 7.2 23.7 98.354.0 0.062 2.20 6.6 21.7 101.94.0 0.065 2.30 7.0 22.9 97.8 4.0 0.067 2.36 6.9 22.6 101.2 4.0 0.065 2.31 7.0 22.9 101.764.0 0.065 2.30 6.6 21.6 102.964.0 0.066 2.32 6.9 22.6 100.064.0 0.065 2.29 7.3 24.0 96.54.0 0.067 2.37 6.9 22.8 100.3 4.0 0.064 2.27 6.9 22.7 98.0 4.0 0.067 2.37 7.3 24.0 99.7P4-14.0 0.063 2.24 7.3 23.9 90.4P4-14.0 0.067 2.37 7.6 24.8 93.4P4-14.0 0.069 2.45 7.6 25.1 98.94.0 0.072 2.54 7.6 25.1 98.7 4.0 0.071 2.50 7.6 24.8 98.4 4.0 0.068 2.40 7.6 25.1 97.024.0 0.069 2.42 7.3 24.0 97.924.0 0.069 2.43 7.2 23.7 99.624.0 0.068 2.40 7.3 24.0 100.94.0 0.069 2.43 7.3 24.0 98.1 4.0 0.068 2.39 7.2 23.7 98.1 4.0 0.066 2.33 7.3 23.9 98.134.0 0.071 2.49 7.6 25.0 96.334.0 0.066 2.31 6.9 22.6 99.434.0 0.064 2.27 6.9 22.8 99.94.0 0.069 2.43 7.3 23.9 98.1 4.0 0.065 2.30 6.9 22.6 98.5 4.0 0.064 2.26 6.9 22.8 99.544.0 0.072 2.54 7.3 23.9 102.544.0 0.065 2.29 6.9 22.6 98.344.0 0.064 2.25 6.6 21.6 104.44.0 0.072 2.53 7.3 23.9 102.0 4.0 0.065 2.30 6.9 22.6 98.6 4.0 0.061 2.16 6.6 21.6 100.15 4.0 0.070 2.49 7.3 23.9 100.4 5 4.0 0.066 2.32 6.9 22.6 99.7 5 4.0 0.061 2.15 7.0 22.8 94.74.0 0.069 2.44 7.3 24.0 99.0 4.0 0.066 2.31 6.9 22.6 99.3 4.0 0.064 2.25 7.0 22.8 99.06 4.0 0.065 2.28 6.6 21.6 101.8 6 4.0 0.066 2.32 6.9 22.7 99.6 6 4.0 0.063 2.24 7.0 22.8 98.84.0 0.064 2.28 7.0 22.9 96.7 4.0 0.063 2.23 6.9 22.7 95.9 4.0 0.064 2.27 7.0 22.8 100.0P5-1 4.0 0.073 2.59 8.2 27.0 93.2 P5-1 4.0 0.072 2.56 7.9 25.8 96.3 P5-1 4.0 0.067 2.36 7.3 24.0 99.24.0 0.082 2.88 8.5 28.0 100.1 4.0 0.070 2.46 7.2 23.8 100.7 4.0 0.075 2.65 8.2 27.0 98.92 4.0 0.078 2.75 8.2 27.0 99.0 2 4.0 0.068 2.38 7.2 23.8 97.6 2 4.0 0.071 2.51 7.9 26.0 96.84.0 0.079 2.77 8.2 27.0 99.7 4.0 0.064 2.27 6.9 22.6 97.1 4.0 0.072 2.54 7.9 26.0 98.13 4.0 0.067 2.36 6.9 22.8 99.9 3 4.0 0.074 2.62 7.5 24.7 102.2 3 4.0 0.066 2.32 6.9 22.8 101.84.0 0.067 2.35 6.9 22.7 99.3 4.0 0.069 2.43 7.2 23.6 98.9 4.0 0.063 2.24 6.9 22.8 98.24 4.0 0.072 2.54 7.6 24.9 98.1 4 4.0 0.071 2.52 7.5 24.7 98.2 4 4.0 0.065 2.30 7.3 23.9 96.54.0 0.073 2.59 7.6 24.9 99.9 4.0 0.073 2.57 7.5 24.7 100.3 4.0 0.068 2.39 7.3 23.8 100.15 4.0 0.074 2.61 7.9 25.9 96.9 5 4.0 0.072 2.55 7.5 24.7 99.6 5 4.0 0.069 2.42 7.6 24.9 97.04.0 0.076 2.69 7.9 25.9 99.9 4.0 0.075 2.64 7.8 25.7 98.8 4.0 0.071 2.49 7.6 24.9 99.96 4.0 0.077 2.70 7.9 25.9 100.3 6 4.0 0.068 2.41 6.9 22.5 102.8 6 4.0 0.070 2.46 7.6 24.9 98.74.0 0.075 2.66 7.6 24.9 102.6 4.0 0.065 2.29 6.9 22.5 97.7 4.0 0.071 2.50 7.6 24.9 100.5Test #326-Jan-1212:12 - 16:12123987Sample Volume Stack VelocityTest #225-Jan-1212:25 - 16:25Test #124-Jan-1213:45 - 17:45Sample Volume Stack VelocitySample Volume Stack VelocityISO-Velocity Calculations

## 123987 DM1 DEP Outlet M29 Part-Chromium Calculations-Feb 21.xls

Company: Owens Corning Pollutant: TSP / Chromium

Plant: Delmar, NY Method: EPA Method 29
Stack: DM1 DEP Outlet Project No.: 123987

Reviewed by MD

Test #1 Test #2 Test #3 24-Jan-12 25-Jan-12 26-Jan-12 Average

13:45 - 17:45 12:25 - 16:25 12:12 - 16:12

Filterable Particulate Concentration mg/S.m 3 

## 1.5 1.7 1.3 1.5

Gr/dscf 

## 0.00065 0.00074 0.00057 0.00065
Filterable Particulate Mass Rate mg/s 

## 5.7 6.5 4.9 5.7 g/s 

## 0.0057 0.0065 0.0049 0.0057

lb./hr 

## 0.045 0.052 0.039 0.045

Filterable Chromium Concentration μ g/S.m 3 

## 5.1 4.5 4.8 4.8
Filterable Chromium Mass Rate ug/s 

## 1.9E+01 1.7E+01 1.8E+01 1.8E+01 mg/s 

## 1.9E-02 1.7E-02 1.8E-02 1.8E-02

lb./hr 

## 1.5E-04 1.4E-04 1.4E-04 1.4E-04

Condensable Chromium Concentration μ g/S.m 3 

## 0.15 0.15 0.10 0.14
Condensable Chromium Mass Rate ug/s 

## 5.9E-01 5.9E-01 3.9E-01 5.2E-01 mg/s 

## 5.9E-04 5.9E-04 3.9E-04 5.2E-04

lb./hr 

## 4.7E-06 4.7E-06 3.1E-06 4.1E-06

Total Chromium Concentration μ g/S.m 3 

## 5.2 4.7 4.9 4.9
Total Chromium Mass Rate ug/s 

## 2.0E+01 1.8E+01 1.8E+01 1.9E+01 mg/s 

## 2.0E-02 1.8E-02 1.8E-02 1.9E-02

lb./hr 

## 1.6E-04 1.4E-04 1.5E-04 1.5E-04

Effluent Characteristics Area of Sample Plane m 2 

## 0.999 0.999 0.999 0.999 Area of Sample Plane ft 2 

## 10.758 10.758 10.758 10.758 Average Stack Temperature  ̊ C 

## 226 223 230 226 Average Stack Temperature (Ts)  ̊ F 

## 439 433 446 439 Average Stack Gas Pressure kPa 

## 99.39 100.60 100.21 100.07 Average Stack Gas Pressure (Psa) in Hg 

## 29.35 29.71 29.60 29.56 Average Stack Gas Velocity m/s 

## 7.4 7.3 7.3 7.4 Average Stack Gas Velocity ft/min 

## 1.45E+03 1.44E+03 1.45E+03 1.45E+03 Oxygen Concentration % vol 

## 19.7 19.9 19.9 19.8
Carbon Dioxide Concentration % vol 

## 4.5 4.9 4.8 4.73 Effluent Molecular Weight (dry) g/gmol 

## 29.5 29.6 29.6 29.6 Effluent Molecular Weight (wet) g/gmol 

## 28.29 28.4 28.3 28.3
Effluent Moisture Content % vol. 

## 10.6 10.5 10.9 10.6 Dry Gas Fraction % vol. 

## 89.4 89.5 89.1 89.4

Actual Effluent Flow Rate A.m 3 

### /s 

## 7.37 7.32 7.35 7.35
Actual Effluent Flow Rate Acfm 

## 1.56E+04 1.55E+04 1.56E+04 1.56E+04 Reference Flow Rate (wet) S.m 3 

### /s 

## 4.25 4.30 4.23 4.26 Standard Flow Rate (wet) Scfm 

## 9.00E+03 9.11E+03 8.97E+03 9.03E+03 Reference Flow Rate (dry) S.m 3 

### /s (dry) 

## 3.80 3.85 3.77 3.81 Standard Flow Rate (dry) Scfm (dry) 

## 8.048E+03 8.16E+03 8.00E+03 8.07E+03 Sample Parameters Sample Period min 

## 240.0 240.0 240.0 240.0 Sample Period Hours 

## 4.0 4.0 4.0 4.0 Front-Half Filterable Loading (Acetone) mg 

## 2.7 3.1 3.1 3.0 Front-Half Filterable Loading (Filter) mg 

## 3.5 4.0 2.3 3.3 Filterable Chromium (Front-Half) μ g 

## 21.2 19.0 19.8 20.0 Condensable Chromium (Back-Half) μ g 

## 0.6 0.6 0.4 0.6 Sample Volume A.m 3 

## 4.185 4.137 4.038 4.120 Sample Volume acf 

## 147.79 146.11 142.59 145.50 Dry Reference Sample Volume S.m 3 

## 4.167 4.203 4.155 4.175 Dry Standard Sample Volume Scf 

## 147.17 148.44 146.74 147.45 Water Vapour Reference Volume S.m 3 

## 0.492 0.493 0.507 0.497 Water Vapour Reference Volume scf 

## 17.37 17.41 17.90 17.56 Average Meter Temperature  ̊ C 

## 20 17 12 17 Average Meter Temperature  ̊ F 

## 68 63 54 62 Average Absolute Meter Pressure in Hg 

## 29.78 30.13 30.00 29.97 Average Absolute Meter Pressure kPa 

## 100.84 102.02 101.57 101.48 Average Delta P in H 2 

### O 

## 0.11 0.11 0.11 0.11 Average Delta H in H 2 

### O 

## 1.28 1.26 1.22 1.25 Average Sample Rate Lpm 

## 17.4 17.2 16.8 17.2 Average Sample Rate cfm 

## 0.62 0.61 0.59 0.61 Average Isokinetic Variation % 

## 99.1 98.6 99.5 99.0 Measurement Parameter 

## LEHDER Environmental Services Ltd.

TSP & Chromium Calculations

# 123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xls



# LEHDER Environmental Services Ltd Revised by: M.Denomme

Date: 16-Feb-12 

# Company: Owens Corning


# Plant: Delmar, NY 

# Stack: DM2 DEP Outlet


# Pollutant: TSP / Chromium


# Method: EPA Method 29 

# Project No.: 123987 

# Operators RS / JH / JT 

# Data Entry: KH / JE 

# Reviewed By: MD

Ref.Temperature: 68 deg. F
Ref. Pressure: 29.92 "Hg
Molar Volume: 24.04 l/mol



# Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

13:45 - 18:00 12:25 - 16:25 12:12 - 16:12 No. of Sample Points 30 30 30 Sample Time /Point min 8.0 8.0 8.0 Reading / Point min 4.0 4.0 4.0 Total Sample Time, min 240.0 240.0 240.0 Barometric Pressure, Pb "Hg 29.69 30.04 29.91 Stack Gauge Pressure, Pgauge "H 2 

# O -0.91 -0.91 -0.88 Absolute Stack Pressure, Ps "Hg 29.62 29.97 29.85 Pitot Tube Coefficient, Cp 0.822 0.822 0.822 Oxygen Content, O2 % 20.0 20.2 20.1 Carbon Dioxide Content, CO2 % 4.4 4.6 4.5 Carbon Monoxide Content, CO % 0.0 0.0 0.0 Nitrogen Content, N2 % 75.7 75.2 75.4 Condensate Collected, W H2O 

# g 353.3 362.3 382.1 Nozzle Diameter, Dn in 0.3833 0.3908 0.3908 Initial DGM Reading ft 3 

# 361.666 625.410 893.055 Final DGM Reading ft 3 

# 508.780 777.785 1041.170 DGM Unity, Y 0.9991 0.9991 0.9991
Stack Width ft 3.280 3.280 3.280 Stack Depth ft 3.280 3.280 3.280 Actual Volume of Dry Gas ft 3 

# 146.9816 152.2379 147.9817
Stack Area, As ft 2 

# 10.758 10.758 10.758



# Particulate/Chromium Analysis

Front-Half Acetone Residue mg 1.1 2.7 3.5 Filter Loading mg 35.3 30.8 27.7 Total Suspended PM mg 36.4 33.5 31.2

Front-Half (Filterable) Chromium μ g 191 180 151 Condensable (Back-Half) Chromium μ g 0.75 0.92 1.1
Total Chromium μ g 192 181 152

Input1123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xlsLEHDER Environmental Services LtdPoint by Point Sampling DataCompany:Owens CorningPlant:Delmar, NYStack:DM2 DEP OutletPollutant:TSP / ChromiumProject No.:123987Test #1Test #2Test #324-Jan-1225-Jan-1226-Jan-1213:45 - 18:0012:25 - 16:2512:12 - 16:12Time Vd Delta P Delta H Ts Tmi TmoTime Vd Delta P Delta H Ts Tmi TmoTime Vd Delta P Delta H Ts Tmi Tmo# minft3H2O H2OF F F # minft3H2O H2OF F F # minft3H2O H2OFFFP5-1 0.0 361.67 0.12 1.48 420 66 66P5-1 0.0 625.41 0.12 1.59 420 63 63P5-10.0 893.06 0.13 1.66 438 52 524.0 364.30 0.11 1.35 427 66 664.0 628.03 0.13 1.71 429 62 634.0 895.68 0.14 1.77 444 49 532 8.0 366.84 0.13 1.59 427 66 662 8.0 630.72 0.14 1.83 432 62 6328.0 898.41 0.13 1.64 444 49 5212.0 369.59 0.13 1.59 431 66 6612.0 633.52 0.14 1.83 433 61 6312.0 901.03 0.14 1.76 445 49 523 16.0 372.13 0.13 1.58 432 66 663 16.0 636.31 0.15 1.89 434 61 63316.0 903.75 0.14 1.70 445 49 5220.0 374.76 0.13 1.58 433 66 6620.0 639.18 0.15 1.89 433 61 6320.0 906.42 0.14 1.76 445 49 524 24.0 377.38 0.14 1.70 434 66 664 24.0 642.05 0.14 1.83 434 62 63424.0 909.15 0.14 1.76 446 50 5228.0 380.11 0.14 1.70 438 66 6728.0 644.91 0.15 1.89 436 62 6328.0 911.86 0.14 1.76 448 50 525 32.0 382.84 0.13 1.56 445 66 675 32.0 647.79 0.14 1.82 437 62 63532.0 914.60 0.14 1.76 450 50 5236.0 385.47 0.13 1.50 446 67 6736.0 650.63 0.14 1.82 437 62 6336.0 917.29 0.15 1.82 451 50 526 40.0 388.10 0.12 1.46 434 66 676 40.0 653.42 0.12 1.57 435 62 63640.0 920.07 0.13 1.63 449 50 5244.0 390.60 0.12 1.44 445 67 6744.0 656.06 0.12 1.57 435 62 6344.0 922.73 0.13 1.63 450 51 52P4-1 48.0 393.17 0.13 1.58 438 67 67P4-1 48.0 658.63 0.12 1.56 421 62 63P4-148.0 925.28 0.14 1.70 443 51 5252.0 395.87 0.14 1.70 439 67 6752.0 661.19 0.12 1.59 423 62 6352.0 927.90 0.14 1.77 442 51 522 56.0 398.53 0.11 1.34 435 67 672 56.0 663.78 0.11 1.46 422 62 63256.0 930.69 0.12 1.53 438 51 5360.0 400.99 0.11 1.28 434 67 6760.0 666.31 0.11 1.46 422 62 6360.0 933.28 0.12 1.53 439 51 533 64.0 403.33 0.11 1.28 434 67 673 64.0 668.81 0.10 1.32 419 62 63364.0 935.82 0.11 1.40 436 51 5368.0 405.67 0.11 1.28 433 66 6768.0 671.16 0.10 1.33 419 63 6368.0 938.25 0.11 1.40 437 51 534 72.0 408.03 0.12 1.45 440 66 674 72.0 673.53 0.12 1.59 422 62 63472.0 940.66 0.13 1.59 441 51 5376.0 410.54 0.13 1.57 441 66 6776.0 676.20 0.12 1.52 423 61 6376.0 943.23 0.13 1.59 441 51 535 80.0 413.17 0.13 1.57 443 66 675 80.0 678.69 0.14 1.84 429 61 63580.0 945.81 0.14 1.70 447 51 5384.0 415.81 0.14 1.63 444 66 6784.0 681.45 0.14 1.83 430 61 6384.0 948.51 0.14 1.70 448 51 536 88.0 418.47 0.14 1.68 444 65 676 88.0 684.29 0.13 1.70 434 62 63688.0 951.19 0.14 1.76 451 51 5392.0 421.20 0.14 1.69 442 65 6692.0 687.02 0.14 1.83 435 62 6392.0 953.89 0.14 1.76 451 51 53P3-1 96.0 423.89 0.10 1.21 430 65 67P3-1 96.0 689.76 0.11 1.46 419 62 63P3-196.0 956.57 0.12 1.54 434 51 53100.0 426.25 0.11 1.35 427 65 67100.0 692.21 0.10 1.30 419 62 63100.0 959.15 0.12 1.53 435 51 532 104.0 428.66 0.10 1.23 424 65 672 104.0 694.60 0.10 1.30 415 62 632104.0 961.69 0.10 1.29 429 51 53108.0 430.96 0.10 1.23 423 66 67108.0 696.94 0.09 1.20 414 62 63108.0 964.03 0.10 1.29 429 51 533 112.0 433.24 0.09 1.11 421 65 673 112.0 699.25 0.09 1.20 413 62 633112.0 966.31 0.09 1.16 429 51 53116.0 435.420.09 1.11 421 66 67116.0 701.51 0.09 1.20 412 62 63116.0 968.50 0.09 1.16 430 51 534 120.0 437.59 0.10 1.23 424 66 674 120.0 703.78 0.10 1.27 414 62 634120.0 970.67 0.10 1.28 433 51 53124.0 439.91 0.10 1.23 423 66 67124.0 706.11 0.10 1.27 414 62 63124.0 973.00 0.11 1.34 433 50 535 128.0 442.22 0.12 1.41 426 66 675 128.0 708.45 0.12 1.60 418 62 635128.0 975.33 0.11 1.40 435 49 52132.0 444.69 0.12 1.41 427 66 67132.0 711.03 0.12 1.60 421 62 63132.0 977.77 0.11 1.33 437 48 526 136.0 447.16 0.13 1.59 430 66 676 136.0 713.66 0.14 1.78 426 62 636136.0 980.15 0.11 1.39 441 49 51140.0 449.90 0.13 1.59 431 66 67140.0 716.42 0.14 1.78 426 62 63140.0 982.58 0.11 1.39 441 49 51P2-1 144.0 452.44 0.09 1.12 416 66 67P2-1 144.0 719.25 0.11 1.47 414 62 63P2-1144.0 984.94 0.10 1.27 433 50 51148.0 454.67 0.11 1.37 417 67 68148.0 721.74 0.11 1.47 415 62 63148.0 987.22 0.10 1.28 432 50 522 152.0 457.07 0.10 1.25 414 67 682 152.0 724.22 0.11 1.40 414 62 632152.0 989.55 0.10 1.28 431 50 52156.0 459.43 0.10 1.25 413 67 68156.0 726.68 0.10 1.34 412 62 63156.0 991.89 0.10 1.28 430 50 523 160.0 461.79 0.10 1.25 413 66 673 160.0 729.10 0.09 1.21 411 62 633160.0 994.16 0.08 1.03 428 51 52164.0 464.08 0.10 1.18 413 66 67164.0 731.38 0.09 1.21 411 62 63164.0 996.23 0.09 1.09 428 51 524 168.0 466.35 0.10 1.25 413 66 674 168.0 733.56 0.10 1.34 413 62 634168.0 998.41 0.09 1.15 431 51 52172.0 468.71 0.10 1.24 416 66 67172.0 735.92 0.10 1.34 414 62 63172.0 1000.54 0.09 1.15 432 51 525 176.0 471.02 0.12 1.49 419 66 675 176.0 738.30 0.12 1.53 418 63 635176.0 1002.74 0.11 1.40 435 51 52180.0 473.58 0.12 1.48 419 65 67180.0 740.80 0.11 1.46 418 62 64180.0 1005.13 0.11 1.40 436 51 526 184.0 476.09 0.13 1.54 421 65 676 184.0 743.35 0.12 1.60 419 62 646184.0 1007.54 0.11 1.34 438 51 53188.0 478.73 0.13 1.60 422 65 66188.0 745.93 0.12 1.53 418 62 64188.0 1009.90 0.11 1.34 439 51 53P1-1 192.0 481.33 0.12 1.49 415 65 66P1-1 192.0 748.50 0.12 1.60 414 63 64P1-1192.0 1012.20 0.11 0.41 433 51 53196.0 483.83 0.12 1.42 417 65 66196.0 750.96 0.12 1.60 417 63 64196.0 1014.66 0.11 1.41 434 51 532 200.0 486.34 0.10 1.25 414 67 662 200.0 753.57 0.12 1.53 417 63 642200.0 1017.15 0.11 1.41 432 51 53204.0 488.66 0.10 1.24 414 65 66204.0 756.15 0.12 1.54 415 63 64204.0 1019.61 0.11 1.41 431 51 533 208.0 490.96 0.10 1.25 412 65 663 208.0 758.68 0.10 1.34 411 63 643208.0 1022.06 0.10 1.29 428 51 53212.0 493.26 0.10 1.25 412 65 66212.0 761.06 0.10 1.34 411 63 63212.0 1024.50 0.10 1.29 428 51 534 216.0 495.57 0.11 1.30 415 65 664 216.0 763.42 0.11 1.41 411 63 644216.0 1026.82 0.11 1.35 429 51 53220.0 497.87 0.10 1.24 415 65 66220.0 765.86 0.11 1.41 413 63 64220.0 1029.21 0.11 1.35 430 51 535 224.0 500.17 0.12 1.43 416 65 665 224.0 768.25 0.11 1.47 418 63 645224.0 1031.55 0.11 1.41 431 50 53228.0 502.70 0.12 1.42 418 65 66228.0 770.65 0.12 1.59 420 63 64228.0 1033.96 0.11 1.41 434 50 536 232.0505.22 0.10 1.25 408 66 666 232.0 773.07 0.10 1.33 420 63 646232.0 1036.38 0.11 1.41 434 50 52236.0 507.55 0.10 1.19 408 65 66236.0 775.48 0.10 1.33 419 63 64236.0 1038.79 0.11 1.41 434 51 52240.0509.78240.0777.79240.01041.17Input2123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xlsLEHDER Environmental Services LtdPoint by Point CalculationsCompany:Owens CorningPlant:Delmar, NYStack:DM2 DEP OutletPollutant:TSP / ChromiumProject No.:Data Entry:KH / JEPoint PeriodIsokinecity Point PeriodIsokinecity Point TimeIsokinecityminm3ft3m/s ft/s %minm3ft3m/s ft/s %minm3ft3m/s ft/s %P5-14.0 0.075 2.63 7.6 24.9 102.9P5-14.0 0.074 2.61 7.5 24.8 99.3P5-14.0 0.074 2.62 8.0 26.1 99.14.0 0.072 2.54 7.3 24.0 104.0 4.0 0.076 2.69 7.9 25.9 98.7 4.0 0.077 2.72 8.3 27.2 99.724.0 0.078 2.75 7.9 26.1 103.624.0 0.079 2.80 8.2 26.9 99.424.0 0.074 2.62 8.0 26.2 99.64.0 0.072 2.53 8.0 26.1 95.7 4.0 0.079 2.79 8.2 26.9 99.0 4.0 0.077 2.72 8.3 27.2 99.734.0 0.074 2.63 8.0 26.1 99.434.0 0.081 2.87 8.4 27.4 100.134.0 0.075 2.66 8.1 26.7 99.44.0 0.074 2.62 8.0 26.1 99.3 4.0 0.081 2.86 8.4 27.4 100.0 4.0 0.077 2.73 8.3 27.2 100.044.0 0.077 2.73 8.3 27.1 99.544.0 0.081 2.86 8.2 26.9 101.644.0 0.077 2.71 8.3 27.2 99.24.0 0.077 2.72 8.3 27.2 99.5 4.0 0.081 2.87 8.4 27.5 100.4 4.0 0.078 2.74 8.3 27.3 100.654.0 0.074 2.63 8.0 26.3 100.054.0 0.080 2.84 8.2 27.0 101.054.0 0.076 2.69 8.3 27.3 98.64.0 0.074 2.63 7.9 25.8 102.0 4.0 0.079 2.79 8.2 27.0 99.1 4.0 0.079 2.77 8.5 27.8 100.264.0 0.071 2.50 7.7 25.1 98.464.0 0.075 2.64 7.6 25.0 101.164.0 0.075 2.66 8.0 26.3 101.24.0 0.073 2.57 7.7 25.3 101.6 4.0 0.073 2.57 7.6 25.0 98.5 4.0 0.072 2.55 8.0 26.3 97.2P4-14.0 0.076 2.70 8.0 26.2 102.2P4-14.0 0.072 2.55 7.5 24.8 97.1P4-14.0 0.074 2.62 8.1 26.7 97.34.0 0.075 2.66 8.3 27.2 97.0 4.0 0.073 2.59 7.6 24.8 98.8 4.0 0.079 2.78 8.3 27.2 101.624.0 0.070 2.46 7.3 24.1 101.124.0 0.072 2.53 7.2 23.7 100.524.0 0.074 2.60 7.6 25.1 102.14.0 0.066 2.34 7.2 23.5 98.2 4.0 0.071 2.50 7.2 23.7 99.4 4.0 0.072 2.53 7.7 25.1 99.634.0 0.066 2.34 7.2 23.5 98.234.0 0.066 2.34 6.9 22.6 97.534.0 0.069 2.43 7.3 24.0 99.54.0 0.067 2.36 7.2 23.5 99.1 4.0 0.067 2.37 6.9 22.6 98.5 4.0 0.068 2.41 7.3 24.0 98.744.0 0.071 2.50 7.7 25.2 98.844.0 0.075 2.67 7.6 24.8 101.544.0 0.073 2.57 7.8 25.7 99.34.0 0.075 2.63 8.0 26.3 100.0 4.0 0.070 2.48 7.4 24.3 96.8 4.0 0.073 2.58 7.8 25.7 99.554.0 0.075 2.64 8.0 26.3 100.454.0 0.078 2.76 8.2 26.9 97.854.0 0.076 2.69 8.2 26.8 100.34.0 0.075 2.65 8.2 26.8 99.0 4.0 0.080 2.84 8.2 26.9 100.5 4.0 0.076 2.68 8.2 26.8 100.164.0 0.077 2.73 8.3 27.3 100.364.0 0.077 2.73 7.9 26.0 100.564.0 0.076 2.70 8.3 27.3 98.94.0 0.076 2.69 8.3 27.3 98.6 4.0 0.077 2.73 8.2 27.0 97.1 4.0 0.076 2.68 8.3 27.3 98.2P3-14.0 0.067 2.35 7.0 22.9 101.3P3-14.0 0.069 2.45 7.2 23.7 97.3P3-14.0 0.073 2.58 7.6 25.0 101.14.0 0.068 2.41 7.3 24.0 98.9 4.0 0.067 2.38 6.9 22.6 99.1 4.0 0.072 2.54 7.6 25.1 99.624.0 0.065 2.30 7.0 22.8 98.624.0 0.066 2.34 6.7 22.0 99.824.0 0.066 2.34 6.9 22.8 100.14.0 0.064 2.27 6.9 22.8 97.3 4.0 0.065 2.31 6.5 21.4 100.9 4.0 0.065 2.28 6.9 22.8 97.734.0 0.062 2.18 6.6 21.6 98.334.0 0.064 2.26 6.5 21.4 98.734.0 0.062 2.18 6.6 21.6 98.34.0 0.061 2.17 6.6 21.6 97.7 4.0 0.064 2.26 6.5 21.3 98.8 4.0 0.061 2.17 6.6 21.6 97.944.0 0.066 2.32 7.0 22.8 99.344.0 0.066 2.33 6.7 21.9 99.344.0 0.066 2.33 7.0 22.8 100.14.0 0.065 2.31 6.9 22.8 99.1 4.0 0.066 2.33 6.7 21.9 99.3 4.0 0.066 2.32 7.1 23.4 97.454.0 0.070 2.46 7.5 24.5 98.654.0 0.073 2.58 7.5 24.7 98.154.0 0.069 2.44 7.3 24.0 100.44.0 0.070 2.47 7.5 24.5 98.8 4.0 0.074 2.62 7.5 24.8 99.8 4.0 0.067 2.38 7.2 23.5 100.364.0 0.078 2.74 8.0 26.1 103.364.0 0.078 2.76 8.0 26.3 99.264.0 0.069 2.42 7.3 24.1 99.94.0 0.072 2.54 8.0 26.1 96.0 4.0 0.080 2.83 8.0 26.3 101.9 4.0 0.067 2.36 7.3 24.1 97.3P2-14.0 0.063 2.23 6.6 21.5 100.2P2-14.0 0.070 2.49 7.2 23.6 98.4P2-14.0 0.065 2.28 7.0 22.8 98.04.0 0.068 2.40 7.3 23.8 97.6 4.0 0.070 2.48 7.2 23.6 98.1 4.0 0.066 2.33 7.0 22.8 100.324.0 0.067 2.35 6.9 22.7 100.124.0 0.070 2.46 7.0 23.1 99.524.0 0.066 2.34 7.0 22.8 100.44.0 0.067 2.36 6.9 22.7 100.2 4.0 0.068 2.42 6.9 22.5 100.2 4.0 0.064 2.26 7.0 22.8 97.134.0 0.065 2.29 6.9 22.7 97.634.0 0.065 2.28 6.5 21.3 99.434.0 0.059 2.07 6.2 20.4 99.24.0 0.064 2.26 6.7 22.1 98.9 4.0 0.062 2.17 6.5 21.3 94.8 4.0 0.062 2.17 6.4 21.0 100.944.0 0.067 2.36 6.9 22.7 100.444.0 0.067 2.36 6.9 22.5 97.844.0 0.060 2.13 6.6 21.6 96.44.0 0.065 2.30 6.9 22.7 98.2 4.0 0.067 2.38 6.9 22.5 98.9 4.0 0.062 2.20 6.6 21.7 99.35 4.0 0.073 2.56 7.6 24.9 100.0 5 4.0 0.071 2.49 7.4 24.2 96.7 5 4.0 0.068 2.39 7.3 24.0 97.94.0 0.071 2.50 7.6 24.9 97.9 4.0 0.072 2.55 7.2 23.7 101.1 4.0 0.068 2.41 7.3 24.0 99.06 4.0 0.075 2.64 7.8 25.5 101.3 6 4.0 0.073 2.57 7.5 24.7 97.7 6 4.0 0.067 2.36 7.2 23.5 99.04.0 0.073 2.59 7.9 26.0 97.6 4.0 0.073 2.57 7.4 24.2 99.5 4.0 0.065 2.30 7.2 23.5 96.6P1-1 4.0 0.071 2.51 7.6 24.9 97.8 P1-1 4.0 0.070 2.46 7.5 24.7 93.0 P1-1 4.0 0.069 2.45 7.3 24.0 100.14.0 0.071 2.50 7.4 24.4 99.9 4.0 0.074 2.61 7.5 24.7 98.9 4.0 0.071 2.49 7.3 24.0 102.02 4.0 0.066 2.32 6.9 22.7 98.8 2 4.0 0.073 2.57 7.4 24.2 99.6 2 4.0 0.070 2.46 7.3 23.9 100.64.0 0.065 2.30 6.9 22.7 98.1 4.0 0.072 2.53 7.4 24.2 97.9 4.0 0.069 2.44 7.3 23.9 99.93 4.0 0.065 2.30 6.9 22.7 98.0 3 4.0 0.067 2.38 6.9 22.5 98.3 3 4.0 0.069 2.44 6.9 22.8 104.54.0 0.065 2.31 6.9 22.7 98.4 4.0 0.067 2.36 6.9 22.5 97.6 4.0 0.065 2.31 6.9 22.8 99.04 4.0 0.065 2.30 7.1 23.3 95.8 4 4.0 0.069 2.44 7.0 23.0 98.4 4 4.0 0.068 2.39 7.1 23.4 100.04.0 0.065 2.30 6.9 22.7 98.2 4.0 0.068 2.39 7.0 23.1 96.6 4.0 0.066 2.34 7.1 23.4 97.85 4.0 0.072 2.53 7.4 24.3 100.8 5 4.0 0.068 2.39 7.2 23.7 94.8 5 4.0 0.068 2.40 7.3 23.9 98.34.0 0.071 2.52 7.4 24.4 100.5 4.0 0.068 2.42 7.5 24.8 91.8 4.0 0.069 2.42 7.3 24.0 99.36 4.0 0.066 2.33 6.9 22.6 98.9 6 4.0 0.068 2.40 6.9 22.6 99.8 6 4.0 0.068 2.40 7.3 24.0 98.64.0 0.063 2.23 6.7 22.0 97.2 4.0 0.065 2.31 6.9 22.6 95.8 4.0 0.067 2.38 7.3 24.0 97.7Sample Volume Stack VelocitySample Volume Stack VelocitySample Volume Stack VelocityTest #225-Jan-1212:25 - 16:25Test #124-Jan-1213:45 - 18:00Test #326-Jan-1212:12 - 16:12123987ISO-Velocity Calculations

## 123987 DM2 DEP Outlet M29 Part-Chromium Calculations.xls

Company: Owens Corning Pollutant: TSP / Chromium

Plant: Delmar, NY Method: EPA Method 29
Stack: DM2 DEP Outlet Project No.: 123987

Reviewed b y MD

Test #1 Test #2 Test #3 24-Jan-12 25-Jan-12 26-Jan-12 Average
13:45 - 18:00 12:25 - 16:25 12:12 - 16:12

Filterable Particulate Concentration mg/S.m 3 

## 8.8 7.6 7.2 7.9

Gr/dscf 

## 0.0038 0.0033 0.0031 0.0034
Filterable Particulate Mass Rat e mg/s 

## 34 30 28 31 g/s 

## 0.034 0.030 0.028 0.031

lb./hr 

## 0.27 0.24 0.22 0.25

Filterable Chromium Concentration μ g/S.m 3 

## 45.9 41.0 34.8 40.6
Filterable Chromium Mass Rat e ug/s 

## 1.81E+02 1.64E+02 1.36E+02 1.60E+02 mg/s 

## 1.81E-01 1.64E-01 1.36E-01 1.60E-01

lb./hr 

## 1.43E-03 1.30E-03 1.08E-03 1.27E-03
Condensable Chromium Concentration μ g/S.m 3 

## 0.18 0.21 0.26 0.22
Condensable Chromium Mass Rat e ug/s 

## 7.10E-01 8.40E-01 1.02E+00 8.57E-01 mg/s 

## 7.10E-04 8.40E-04 1.02E-03 8.57E-04

lb./hr 

## 5.64E-06 6.67E-06 8.10E-06 6.80E-06
Total Chromium Concentration μ g/S.m 3 

## 46.1 41.2 35.1 40.8
Total Chromium Mass Rat e ug/s 

## 1.81E+02 1.65E+02 1.37E+02 1.61E+02 mg/s 

## 1.81E-01 1.65E-01 1.37E-01 1.61E-01

lb./hr 

## 1.44E-03 1.31E-03 1.09E-03 1.28E-03

Effluent Characteristic s Area of Sample Plane m 2 

## 0.999 0.999 0.999 0.999 Area of Sample Plane ft 2 

## 10.758 10.758 10.758 10.758 Average Stack Temperature  ̊ C 

## 219 216 225 220 Average Stack Temperature (Ts)  ̊ F 

## 426 421 437 428 Average Stack Gas Pressure kPa 

## 100.29 101.48 101.05 100.94 Average Stack Gas Pressure (Psa) in Hg 

## 29.62 29.97 29.85 29.81 Average Stack Gas Velocity m/s 

## 7.4 7.4 7.5 7.4 Average Stack Gas Velocity ft/min 

## 1.46E+03 1.45E+03 1.47E+03 1.46E+03 Oxygen Concentration % vol 

## 20.0 20.2 20.1 20.1
Carbon Dioxide Concentration % vol 

## 4.4 4.6 4.5 4.49 Effluent Molecular Weight (dry) g/gmol 

## 29.5 29.5 29.5 29.5 Effluent Molecular Weight (wet) g/gmol 

## 28.32 28.4 28.3 28.3
Effluent Moisture Content % vol. 

## 10.2 9.93 10.5 10.2 Dry Gas Fraction % vol. 

## 89.8 90.1 89.5 89.8

Actual Effluent Flow Rate A.m 3 

### /s 

## 7.4 7.4 7.5 7.4
Actual Effluent Flow Rate Acfm 

## 1.57E+04 1.56E+04 1.58E+04 1.57E+04 Reference Flow Rate (wet) S.m 3 

### /s 

## 4.4 4.4 4.4 4.4 Standard Flow Rate (wet) Scfm 

## 9.28E+03 9.39E+03 9.28E+03 9.32E+03 Reference Flow Rate (dry) S.m 3 

### /s (dry) 

## 3.9 4.0 3.9 3.9 Standard Flow Rate (dry) Scfm (dry) 

## 8.33E+03 8.46E+03 8.30E+03 8.36E+03 Sample Parameter s Sample Period min 

## 240.0 240.0 240.0 240.0 Sample Period Hours 

## 4.0 4.0 4.0 4.0 Front-Half Filterable Loading (Acetone) mg 

## 1.1 2.7 3.5 2.4 Front-Half Filterable Loading (Filter) mg 

## 35.3 30.8 27.7 31.3 Filterable Chromium (Front-Half) μ g 

## 191.0 180.0 151.0 174.0 Condensable Chromium (Back-Half) μ g 

## 0.8 0.9 1.1 0.9 Sample Volume A.m 3 

## 4.162 4.311 4.190 4.221 Sample Volume acf 

## 146.98 152.24 147.98 149.07 Dry Reference Sample Volume S.m 3 

## 4.158 4.388 4.340 4.295 Dry Standard Sample Volume Scf 

## 146.8 4 154.98 153.25 151.69 Water Vapour Reference Volume S.m 3 

## 0.472 0.484 0.510 0.489 Water Vapour Reference Volume scf 

## 16.66 17.09 18.02 17.26 Average Meter Temperature  ̊ C 

## 19 17 11 16 Average Meter Temperature  ̊ F 

## 66 63 51 60 Average Absolute Meter Pressure in Hg 

## 29.79 30.15 30.02 29.99 Average Absolute Meter Pressure kPa 

## 100.87 102.09 101.63 101.53 Average Delta P in H 2 

### O 

## 0.11 0.12 0.12 0.11 Average Delta H in H 2 

### O 

## 1.40 1.53 1.45 1.46 Average Sample Rate Lpm 

## 17.3 18.0 17.5 17.6 Average Sample Rate cfm 

## 0.61 0.63 0.62 0.62 Average Isokinetic Variation % 

## 99.3 98.7 99.5 99.1 Measurement Parameter 

# LEHDER Environmental Services Ltd.

TSP & Chromium Calculations

# Appendix A.2

Method 0061 Test Runs

# 123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls



# LEHDER Environmental Services Ltd Mike Denomme

16-Feb-12 

# Company: Owens Corning


# Plant: Delmar NY


# Stack: DM1 DEP Outlet


# Pollutant: Hexavalent/Total Chromium


# Method: EPA Method 0061 

# Project No.: 123987 

# Operators RS / JH 

# Data Entry: KH / JE 

# Reviewed By: MD

Ref.Temperature: 68 deg. F
Ref. Pressure: 29.92 "Hg Velocity Constant: 85.49
Molar Volume: 24.04 l/mol



# Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22 No. of Sample Points 30 30 30 Sample Time /Point min 8.0 7.0 7.0 Reading / Point min 4.0 3.5 3.5 Total Sample Time, min 240.0 210.0 210.0 Barometric Pressure, Pb "Hg 29.65 30.04 29.97 Stack Gauge Pressure, Pgauge "H2O -4.43 -4.63 -4.35 Absolute Stack Pressure, Ps "Hg 29.32 29.70 29.65 Pitot Tube Coefficient, Cp 0.779 0.779 0.779 Oxygen Content, O2 % 19.6 20.0 19.9 Carbon Dioxide Content, CO2 % 4.9 4.7 4.8 Carbon Monoxide Content, CO % 0.0 0.0 0.0 Nitrogen Content, N2 % 75.6 75.3 75.3 Condensate Collected, W H2O 

# g 349.4 286.9 313.9 Nozzle Diameter, Dn in 0.3648 0.3648 0.3648 Initial DGM Reading ft 3 

# 41.380 18.770 81.563 Final DGM Reading ft 3 

# 171.665 136.030 197.757 DGM Unity, Y 1.0123 1.0123 1.0123
Stack Width ft 3.280 3.280 3.280 Stack Depth ft 3.280 3.280 3.280 Actual Volume of Dry Gas ft 3 

# 131.8875 118.7023 117.6232
Stack Area, As ft 2 

# 10.758 10.758 10.758



# Hex Chromium Analysis

Uncorrected Chromium (Cr ) 6+ 

# ug 12.50 11.80 8.87
Blank Correction ug 1.72 1.72 1.72

Corrected Hexavalent Chromium ug 10.8 10.1 7.15



# Total Chromium Analysis

Total Chromium - (1) KOH & Rinses ug 17.2 18.9 20.3 Total Chromium - (3) Nitric Rinse ug 0.39 0.355 0.281 Total Chromium - (3) Column Filter ug 0.916 1.24 0.75
Uncorrected Total Chromium ug 18.5 20.5 21.3 Blank Correction (4) ug 3.14 3.14 3.14 Total Chromium (1 + 2 + 3) - 4 ug 15.4 17.4 18.2

Italics indicate values less than method detection

Input1123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls



### LEHDER Environmental Services Ltd Point by Point Sampling Data

Company: Owens Corning

Plant: Delmar NY

Stack: DM1 DEP Outlet

Pollutant: Hexavalent/Total Chromium Project No.: 123987

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo

# min ft 3 H 2 O H 2 O F F F # min ft 3 H 2 O H 2 O F F F # min ft 3 H 2 O H 2 O F F F

P1-1 0.0 41.38 0.160 1.30 444 66 66 P1-1 0.0 18.77 0.160 1.25 433 67 67 P1-1 0.0 81.56 0.170 1.35 440 69 69

4.0 43.68 0.170 1.35 447 63 66 3.5 20.84 0.170 1.32 433 65 67 3.5 83.64 0.170 1.35 442 69 69

2 8.0 46.16 0.140 1.10 447 63 65 2 7.0 23.00 0.150 1.20 432 63 66 2 7.0 85.84 0.150 1.20 441 69 69

12.0 48.46 0.140 1.10 447 64 65 10.5 25.02 0.160 1.25 433 63 66 10.5 87.91 0.150 1.20 442 69 69

3 16.0 50.68 0.130 1.05 447 65 65 3 14.0 27.13 0.140 1.10 429 63 66 3 14.0 89.98 0.150 1.20 442 69 70

20.0 52.88 0.140 1.10 448 65 65 17.5 29.12 0.150 1.20 432 63 65 17.5 92.02 0.150 1.20 442 69 70

4 24.0 55.13 0.130 1.05 448 66 66 4 21.0 31.13 0.140 1.10 432 63 65 4 21.0 94.09 0.140 1.10 442 69 70

28.0 57.33 0.130 1.00 450 67 66 24.5 33.12 0.150 1.20 433 63 65 24.5 96.09 0.140 1.10 442 69 70

5 32.0 59.52 0.140 1.10 450 67 66 5 28.0 35.14 0.160 1.25 433 63 65 5 28.0 98.07 0.140 1.10 444 69 70

36.0 61.77 0.130 1.00 452 67 66 31.5 37.26 0.140 1.10 434 63 65 31.5 100.08 0.140 1.10 443 69 70

6 40.0 63.98 0.120 0.95 450 68 67 6 35.0 39.22 0.140 1.10 430 64 65 6 35.0 102.12 0.140 1.10 440 69 70

44.0 66.11 0.130 1.05 450 68 68 38.5 41.16 0.140 1.10 427 64 65 38.5 104.12 0.140 1.10 440 69 70

P2-1 48.0 68.26 0.140 1.10 447 68 68 P2-1 42.0 43.14 0.140 1.10 429 62 65 P2-1 42.0 106.07 0.160 1.25 434 68 70

52.0 70.43 0.140 1.10 447 68 67 45.5 45.10 0.140 1.10 429 62 65 45.5 108.19 0.160 1.25 440 68 70

2 56.0 72.68 0.120 0.95 447 68 67 2 49.0 47.08 0.130 1.00 428 62 65 2 49.0 110.38 0.140 1.10 439 68 70

60.0 74.81 0.120 0.95 447 68 67 52.5 49.02 0.120 0.95 428 62 65 52.5 112.38 0.140 1.10 440 68 69

3 64.0 76.94 0.110 0.87 447 69 67 3 56.0 50.87 0.120 0.95 428 62 65 3 56.0 114.39 0.130 1.00 439 67 69

68.0 78.98 0.110 0.87 448 68 68 59.5 52.72 0.120 0.95 428 62 65 59.5 116.32 0.130 1.00 439 67 69

4 72.0 81.02 0.110 0.87 448 68 68 4 63.0 54.56 0.120 0.95 428 61 64 4 63.0 118.26 0.130 1.00 439 67 69

76.0 83.04 0.110 0.87 452 68 68 66.5 56.40 0.130 1.00 428 60 64 66.5 120.17 0.130 1.00 441 66 69

5 80.0 85.09 0.130 1.00 456 68 68 5 70.0 58.31 0.140 1.20 428 60 64 5 70.0 122.08 0.140 1.10 441 66 69

84.0 87.28 0.130 1.00 456 68 68 73.5 60.28 0.140 1.10 432 60 63 73.5 124.10 0.140 1.10 443 64 68

6 88.0 89.51 0.130 1.00 452 68 68 6 77.0 62.27 0.150 1.15 430 60 63 6 77.0 126.18 0.140 1.10 440 64 68

92.0 91.69 0.130 1.00 450 68 68 80.5 64.35 0.150 1.20 427 60 63 80.5 128.14 0.140 1.10 439 63 67
P3-1 96.0 93.88 0.120 0.95 450 68 68 P3-1 84.0 66.30 0.140 1.10 427 60 63 P3-1 84.0 130.07 0.140 1.10 435 63 67

100.0 95.95 0.130 1.05 450 67 67 87.5 68.27 0.140 1.10 425 59 63 87.5 132.03 0.140 1.10 436 63 66

2 104.0 98.15 0.110 0.87 448 67 67 2 91.0 70.23 0.120 0.95 425 59 63 2 91.0 134.01 0.120 0.94 433 63 66

108.0 100.20 0.110 0.87 448 67 67 94.5 72.08 0.120 0.95 425 59 63 94.5 135.86 0.120 0.94 434 63 66

3 112.0 102.24 0.100 0.79 447 67 67 3 98.0 73.94 0.110 0.87 422 58 62 3 98.0 137.71 0.120 0.94 433 64 66

116.0 104.21 0.100 0.79 447 67 67 101.5 75.72 0.110 0.87 422 59 62 101.5 139.52 0.120 0.94 433 64 66

4 120.0 106.12 0.100 0.79 447 67 67 4 105.0 77.49 0.110 0.87 422 58 62 4 105.0 141.36 0.120 0.94 432 63 66

124.0 108.07 0.100 0.79 451 67 67 108.5 79.28 0.110 0.87 424 58 62 108.5 143.19 0.120 0.94 436 63 66

5 128.0 110.01 0.110 0.87 454 67 67 5 112.0 81.04 0.120 0.95 424 58 62 5 112.0 145.06 0.120 0.94 436 63 66

132.0 112.07 0.110 0.87 454 67 67 115.5 82.88 0.120 0.95 424 58 62 115.5 146.89 0.120 0.94 441 64 66

6 136.0 114.14 0.100 0.79 450 67 67 6 119.0 84.70 0.140 1.10 422 60 62 6 119.0 148.72 0.130 1.00 441 64 66

140.0 116.10 0.100 0.79 450 68 67 122.5 86.66 0.150 1.20 420 59 62 122.5 150.62 0.130 1.00 441 64 66

P4-1 144.0 118.11 0.140 1.11 450 68 68 P4-1 126.0 88.71 0.150 1.20 422 63 62 P4-1 126.0 152.45 0.140 1.10 440 64 66

148.0 120.21 0.150 1.20 447 68 68 129.5 90.71 0.140 1.10 422 60 62 129.5 154.46 0.140 1.10 436 64 66

2 152.0 122.57 0.130 1.05 443 67 68 2 133.0 92.66 0.140 1.10 419 60 62 2 133.0 156.46 0.130 1.00 436 63 66

156.0 124.86 0.130 1.05 443 67 67 136.5 94.67 0.140 1.10 419 60 62 136.5 158.39 0.130 1.00 433 63 65

3 160.0 127.03 0.110 0.87 443 67 67 3 140.0 96.66 0.130 1.05 419 60 62 3 140.0 160.31 0.120 0.95 433 63 65

164.0 129.07 0.120 0.96 441 67 68 143.5 98.55 0.130 1.05 418 60 62 143.5 162.15 0.120 0.95 433 63 65

4 168.0 131.19 0.120 0.96 444 67 68 4 147.0 100.49 0.120 0.95 421 61 62 4 147.0 164.02 0.110 0.87 434 63 65

172.0 133.34 0.120 0.95 443 67 67 150.5 102.30 0.120 0.95 422 61 62 150.5 165.80 0.110 0.87 436 63 65

5 176.0 135.48 0.120 0.95 443 67 67 5 154.0 104.14 0.120 0.95 422 61 62 5 154.0 167.61 0.110 0.87 436 63 65

180.0 137.63 0.120 0.95 446 67 67 157.5 105.98 0.120 0.95 425 61 62 157.5 169.36 0.110 0.86 439 63 65

6 184.0 139.76 0.120 0.95 446 67 67 6 161.0 107.81 0.120 0.95 422 61 62 6 161.0 171.13 0.100 0.80 435 63 65

188.0 141.86 0.120 0.96 440 67 67 164.5 109.66 0.120 0.95 422 61 62 164.5 172.82 0.100 0.80 435 63 65
P5-1 192.0 143.86 0.150 1.20 440 67 67 P5-1 168.0 111.43 0.170 1.35 420 61 62 P5-1 168.0 174.52 0.150 1.20 435 63 65

196.0 146.18 0.150 1.20 440 67 67 171.5 113.46 0.170 1.35 421 62 63 171.5 176.60 0.160 1.25 435 63 65

2 200.0 148.54 0.150 1.20 440 67 67 2 175.0 115.61 0.160 1.25 420 61 63 2 175.0 178.76 0.140 1.10 435 63 65

204.0 150.92 0.150 1.20 435 67 67 178.5 117.68 0.170 1.35 417 61 63 178.5 180.78 0.150 1.20 435 63 65

3 208.0 153.31 0.130 1.05 434 67 67 3 182.0 119.89 0.140 1.10 417 61 63 3 182.0 182.83 0.120 0.95 435 63 65

212.0 155.53 0.130 1.05 433 67 67 185.5 121.81 0.140 1.10 416 61 63 185.5 184.65 0.120 0.95 430 63 65

4 216.0 157.70 0.140 1.13 435 67 67 4 189.0 123.79 0.140 1.10 417 61 63 4 189.0 186.51 0.130 1.05 430 63 65

220.0 159.99 0.140 1.12 435 67 67 192.5 125.80 0.150 1.20 418 61 63 192.5 188.45 0.130 1.05 433 63 65

5 224.0 162.35 0.150 1.20 434 67 67 5 196.0 127.87 0.160 1.30 418 61 63 5 196.0 190.31 0.130 1.05 433 63 65

228.0 164.65 0.150 1.20 434 67 67 199.5 130.08 0.150 1.20 417 62 63 199.5 192.25 0.130 1.05 431 63 65

6 232.0 167.06 0.130 1.05 434 67 67 6 203.0 132.13 0.130 1.05 415 62 63 6 203.0 194.20 0.110 0.87 431 63 65

236.0 169.44 0.130 1.05 430 67 67 206.5 134.03 0.140 1.10 415 62 63 206.5 195.96 0.110 0.87 431 63 65

240.0 171.67 210.0 136.03 210.0 197.76

Input2

### 123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls



### LEHDER Environmental Services Ltd Point by Point Calculations

Company: Owens Corning

Plant: Delmar NY

Stack: DM1 DEP Outlet

Pollutant: Hexavalent/Total Chromium Project No. : 123987 

### Data Entry: KH / JE

Point Period Isokinecity Point Period Isokinecity Point Time Isokinecity

min m 3 ft 3 m/s ft/s % min m 3 ft 3 m/s ft/s % min m 3 ft 3 m/s ft/s %



### P1-1 4.0 0.066 2.32 8.5 27.8 94.1 

### P1-1 3.5 0.059 2.10 8.4 27.4 95.9 

### P1-1 3.5 0.059 2.10 8.7 28.4 93.9

4.0 0.071 2.52 8.8 28.7 99.3 3.5 0.062 2.19 8.6 28.3 97.3 3.5 0.063 2.23 8.7 28.5 100.0



### 2 4.0 0.066 2.32 7.9 26.1 101.1 

### 2 3.5 0.058 2.04 8.1 26.5 97.0 

### 2 3.5 0.059 2.10 8.1 26.7 99.9

4.0 0.064 2.25 7.9 26.1 97.9 3.5 0.060 2.13 8.4 27.4 98.0 3.5 0.059 2.09 8.2 26.8 99.7


### 3 4.0 0.063 2.23 7.7 25.1 100.4 

### 3 3.5 0.057 2.02 7.8 25.6 99.0 

### 3 3.5 0.059 2.07 8.2 26.8 98.6

4.0 0.064 2.27 7.9 26.1 98.8 3.5 0.057 2.03 8.1 26.5 96.4 3.5 0.059 2.09 8.2 26.8 99.6



### 4 4.0 0.063 2.23 7.7 25.1 100.5 

### 4 3.5 0.057 2.01 7.8 25.6 99.0 

### 4 3.5 0.057 2.02 7.9 25.8 99.8

4.0 0.063 2.21 7.7 25.2 99.5 3.5 0.058 2.04 8.1 26.5 97.2 3.5 0.057 2.00 7.9 25.8 98.8



### 5 4.0 0.064 2.28 8.0 26.1 98.8 

### 5 3.5 0.061 2.15 8.4 27.4 98.8 

### 5 3.5 0.058 2.03 7.9 25.9 100.4

4.0 0.063 2.24 7.7 25.2 101.0 3.5 0.056 1.98 7.8 25.7 97.6 3.5 0.058 2.07 7.9 25.9 101.9


### 6 4.0 0.061 2.16 7.4 24.2 100.8 

### 6 3.5 0.056 1.97 7.8 25.6 96.6 

### 6 3.5 0.057 2.03 7.9 25.8 100.0

4.0 0.062 2.18 7.7 25.2 97.7 3.5 0.057 2.00 7.8 25.6 98.1 3.5 0.056 1.97 7.9 25.8 97.0


### P2-1 4.0 0.062 2.20 7.9 26.1 94.9 

### P2-1 3.5 0.056 1.98 7.8 25.6 97.4 

### P2-1 3.5 0.061 2.15 8.4 27.5 98.9

4.0 0.064 2.27 7.9 26.1 98.2 3.5 0.057 2.00 7.8 25.6 98.2 3.5 0.063 2.22 8.4 27.6 102.3



### 2 4.0 0.061 2.16 7.4 24.1 100.6 

### 2 3.5 0.056 1.97 7.5 24.6 100.3 

### 2 3.5 0.057 2.02 7.9 25.8 99.5

4.0 0.061 2.16 7.4 24.1 100.6 3.5 0.053 1.87 7.2 23.7 99.0 3.5 0.058 2.03 7.9 25.8 100.4


### 3 4.0 0.058 2.07 7.0 23.1 100.6 

### 3 3.5 0.053 1.88 7.2 23.7 99.5 

### 3 3.5 0.055 1.96 7.6 24.9 100.3

4.0 0.058 2.07 7.0 23.1 100.6 3.5 0.053 1.86 7.2 23.7 98.7 3.5 0.056 1.96 7.6 24.9 100.6



### 4 4.0 0.058 2.05 7.0 23.1 99.9 

### 4 3.5 0.053 1.86 7.2 23.7 98.9 

### 4 3.5 0.055 1.93 7.6 24.9 99.0

4.0 0.059 2.08 7.1 23.2 101.3 3.5 0.055 1.93 7.5 24.6 98.5 3.5 0.055 1.93 7.6 24.9 99.0



### 5 4.0 0.063 2.22 7.7 25.2 99.8 

### 5 3.5 0.056 1.99 7.8 25.6 98.2 

### 5 3.5 0.058 2.05 7.9 25.8 101.4

4.0 0.064 2.26 7.7 25.2 101.6 3.5 0.057 2.01 7.8 25.6 99.5 3.5 0.059 2.10 7.9 25.9 104.3


### 6 4.0 0.062 2.21 7.7 25.2 99.1 

### 6 3.5 0.060 2.11 8.1 26.5 100.4 

### 6 3.5 0.056 1.98 7.9 25.8 98.4

4.0 0.063 2.21 7.7 25.2 99.3 3.5 0.056 1.98 8.1 26.5 94.2 3.5 0.055 1.96 7.9 25.8 97.3

P3-1 4.0 0.059 2.10 7.4 24.2 98.1 P3-1 3.5 0.056 1.99 7.8 25.6 98.2 P3-1 3.5 0.06 1.98 7.8 25.7 98.0

4.0 0.063 2.22 7.7 25.2 99.9 3.5 0.056 1.98 7.8 25.5 97.4 3.5 0.06 2.01 7.9 25.8 99.7

2 4.0 0.059 2.08 7.0 23.1 101.5 2 3.5 0.053 1.88 7.2 23.6 99.8 2 3.5 0.05 1.87 7.3 23.8 100.1

4.0 0.058 2.07 7.0 23.1 100.8 3.5 0.053 1.88 7.2 23.6 100.1 3.5 0.05 1.87 7.3 23.8 100.2

3 4.0 0.056 1.99 6.7 22.0 101.8 3 3.5 0.051 1.80 6.9 22.6 99.8 3 3.5 0.05 1.83 7.3 23.8 97.9

4.0 0.055 1.94 6.7 22.0 99.2 3.5 0.051 1.80 6.9 22.6 99.7 3.5 0.05 1.86 7.3 23.8 99.5

4 4.0 0.056 1.97 6.7 22.0 100.7 4 3.5 0.051 1.81 6.9 22.6 100.6 4 3.5 0.05 1.85 7.3 23.8 98.7

4.0 0.056 1.97 6.7 22.1 100.9 3.5 0.050 1.78 6.9 22.6 98.8 3.5 0.05 1.89 7.3 23.8 101.4

5 4.0 0.059 2.09 7.1 23.2 102.1 5 3.5 0.053 1.87 7.2 23.6 99.4 5 3.5 0.05 1.86 7.3 23.8 99.5

4.0 0.059 2.10 7.1 23.2 102.6 3.5 0.052 1.84 7.2 23.6 98.1 3.5 0.05 1.85 7.3 23.9 99.1

6 4.0 0.056 1.98 6.7 22.1 101.7 6 3.5 0.056 1.98 7.8 25.5 97.3 6 3.5 0.05 1.93 7.6 24.9 99.4

4.0 0.057 2.03 6.7 22.1 103.9 3.5 0.059 2.08 8.0 26.4 98.6 3.5 0.05 1.85 7.6 24.9 95.5

P4-1 4.0 0.060 2.13 8.0 26.1 92.0 P4-1 3.5 0.057 2.02 8.0 26.4 95.9 P4-1 3.5 0.06 2.03 7.9 25.8 101.1

4.0 0.068 2.39 8.2 27.0 99.9 3.5 0.056 1.98 7.8 25.5 97.3 3.5 0.06 2.02 7.9 25.8 100.3

2 4.0 0.066 2.31 7.6 25.1 103.5 2 3.5 0.057 2.03 7.8 25.4 99.6 2 3.5 0.06 1.95 7.6 24.8 100.3

4.0 0.062 2.20 7.6 25.1 98.6 3.5 0.057 2.01 7.8 25.4 98.9 3.5 0.06 1.95 7.6 24.8 100.2

3 4.0 0.058 2.06 7.0 23.1 100.3 3 3.5 0.054 1.92 7.5 24.5 97.7 3 3.5 0.05 1.86 7.3 23.8 99.4

4.0 0.061 2.15 7.3 24.0 99.8 3.5 0.056 1.96 7.5 24.5 99.9 3.5 0.05 1.90 7.3 23.8 101.6

4 4.0 0.062 2.18 7.3 24.1 101.4 4 3.5 0.052 1.83 7.2 23.6 97.1 4 3.5 0.05 1.80 7.0 22.8 100.8

4.0 0.061 2.17 7.3 24.1 101.0 3.5 0.053 1.86 7.2 23.6 98.8 3.5 0.05 1.83 7.0 22.8 102.6

5 4.0 0.062 2.18 7.3 24.1 101.7 5 3.5 0.053 1.86 7.2 23.6 98.8 5 3.5 0.05 1.77 7.0 22.8 99.2

4.0 0.061 2.16 7.4 24.1 100.7 3.5 0.052 1.85 7.2 23.6 98.4 3.5 0.05 1.79 7.0 22.9 100.5

6 4.0 0.060 2.13 7.4 24.1 99.3 6 3.5 0.053 1.87 7.2 23.6 99.0 6 3.5 0.05 1.71 6.6 21.8 100.4

4.0 0.057 2.02 7.3 24.0 94.0 3.5 0.051 1.80 7.2 23.6 95.3 3.5 0.05 1.72 6.6 21.8 100.7

P5-1 4.0 0.067 2.35 8.2 26.9 97.8 P5-1 3.5 0.058 2.05 8.6 28.1 91.5 P5-1 3.5 0.06 2.11 8.1 26.6 101.2

4.0 0.068 2.39 8.2 26.9 99.7 3.5 0.061 2.17 8.6 28.1 96.6 3.5 0.06 2.19 8.4 27.5 101.6

2 4.0 0.068 2.40 8.2 26.9 100.1 2 3.5 0.059 2.10 8.3 27.2 96.3 2 3.5 0.06 2.04 7.8 25.7 101.2

4.0 0.069 2.42 8.2 26.8 100.5 3.5 0.063 2.24 8.5 28.0 99.4 3.5 0.06 2.08 8.1 26.6 99.5

3 4.0 0.064 2.25 7.6 24.9 100.2 3 3.5 0.055 1.94 7.7 25.4 95.1 3 3.5 0.05 1.84 7.3 23.8 98.7

4.0 0.062 2.20 7.6 24.9 97.9 3.5 0.057 2.00 7.7 25.4 97.8 3.5 0.05 1.89 7.2 23.8 100.9

4 4.0 0.066 2.32 7.9 25.9 99.6 4 3.5 0.058 2.03 7.7 25.4 99.5 4 3.5 0.06 1.96 7.5 24.7 100.9

4.0 0.068 2.39 7.9 25.9 102.7 3.5 0.059 2.10 8.0 26.3 99.1 3.5 0.05 1.88 7.6 24.8 96.6

5 4.0 0.066 2.33 8.2 26.8 96.9 5 3.5 0.063 2.24 8.3 27.2 102.7 5 3.5 0.06 1.96 7.6 24.8 101.0

4.0 0.069 2.43 8.2 26.8 101.1 3.5 0.059 2.07 8.0 26.3 97.8 3.5 0.06 1.98 7.5 24.8 101.7

6 4.0 0.068 2.41 7.6 24.9 107.6 6 3.5 0.055 1.93 7.5 24.5 97.7 6 3.5 0.05 1.78 6.9 22.8 99.5

4.0 0.064 2.25 7.6 24.9 100.2 3.5 0.057 2.02 7.7 25.4 98.8 3.5 0.05 1.82 6.9 22.8 101.6 Sample Volume Stack Velocity Sample Volume Stack Velocity Sample Volume Stack Velocity 

### Test #2

25-Jan-12

08:03 - 11:49 Test #3

26-Jan-12

07:52 - 11:22 Test #1

24-Jan-12

08:27 - 12:55

ISO-Velocity Calculations

## 123987 DM1 DEP Outlet M0061 Hex-Chromium Calculations.xls

Company: Owens Corning Pollutant: Hexavalent/Total Chromium
Plant: Delmar NY Method: EPA Method 0061
Stack: DM1 DEP Outlet Project No.: 123987

Reviewed b y MD

Test #1 Test #2 Test #3
24-Jan-12 25-Jan-12 26-Jan-12 Average
08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Hexavalent Chromium Concentration ug/S.m 3 

## 2.90E+00 2.95E+00 2.13E+00 2.66E+00
Hexavalent Chromium Mass Rate ug/s 

## 1.11E+01 1.21E+01 8.43E+00 1.05E+01 mg/s 

## 1.11E-02 1.21E-02 8.43E-03 1.05E-02 g/hr 

## 4.00E-02 4.35E-02 3.03E-02 3.79E-02

lb./hr 

## 8.82E-05 9.59E-05 6.68E-05 8.36E-05

Total Chromium Concentration ug/S.m 3 

## 4.13E+00 5.07E+00 5.42E+00 4.87E+00
Total Chromium Mass Rate ug/s 

## 1.58E+01 2.08E+01 2.14E+01 1.94E+01 mg/s 

## 1.58E-02 2.08E-02 2.14E-02 1.94E-02 g/hr 

## 5.70E-02 7.49E-02 7.72E-02 6.97E-02

lb./hr 

## 1.26E-04 1.65E-04 1.70E-04 1.54E-04


# Effluent Characteristics
Area of Sample Plane m 2 

## 0.999 0.999 0.999 0.999 Area of Sample Plane ft 2 

## 10.758 10.758 10.758 10.758 Average Stack Temperature  ̊ C 

## 230 218 225 224 Average Stack Temperature (Ts)  ̊ F 

## 445 425 437 436 Average Stack Gas Pressure kPa 

## 99.28 100.55 100.39 100.07 Average Stack Gas Pressure (Psa) in Hg 

## 29.32 29.70 29.65 29.56 Average Stack Gas Velocity m/s 

## 7.55 7.70 7.63 7.63 Average Stack Gas Velocity ft/min 

## 1.49E+03 1.52E+03 1.50E+03 1.50E+03 Oxygen Concentration % vol 

## 19.6 20.0 19.9 19.8
Carbon Dioxide Concentration % vol 

## 4.9 4.7 4.8 4.8 Effluent Molecular Weight (dry) g/gmol 

## 29.56 29.55 29.56 29.56 Effluent Molecular Weight (wet) g/gmol 

## 28.27 28.39 28.28 28.31
Effluent Moisture Content % vol. 

## 11.2 10.1 11.1 10.8 Dry Gas Fraction % vol. 

## 88.8 89.9 88.9 89.2
Actual Effluent Flow Rate A.m 3 

## /s 

## 7.54 7.70 7.63 7.62
Actual Effluent Flow Rate Acfm 

## 1.60E+04 1.63E+04 1.62E+04 1.62E+04 Reference Flow Rate (wet) S.m 3 

## /s 

## 4.31 4.56 4.45 4.44 Standard Flow Rate (wet) Scfm 

## 9.14E+03 9.66E+03 9.43E+03 9.41E+03 Reference Flow Rate (dry) S.m 3 

## /s (dry) 

## 3.83 4.10 3.96 3.96 Standard Flow Rate (dry) Scfm (dry) 

## 8.12E+03 8.69E+03 8.38E+03 8.40E+03
Sample Parameters Sample Period min 

## 240.0 210.0 210.0 220.0 Sample Period Hours 

## 4.0 3.5 3.5 3.7 Sample Volume A.m 3 

## 3.735 3.361 3.331 3.476 Sample Volume acf 

## 131.888 118.702 117.623 122.738
Hexavalent Chromium ug 

## 10.8 10.1 7.2 9.3
Total Chromium ug 

## 15.4 17.4 18.2 17.0 Dry Reference Sample Volume S.m 3 

## 3.717 3.421 3.358 3.499 Dry Standard Sample Volume Scf 

## 131.27 120.81 118.57 123.55 Water Vapour Reference Volume S.m 3 

## 0.467 0.383 0.419 0.423 Water Vapour Reference Volume scf 

## 16.48 13.53 14.80 14.94 Average Meter Temperature  ̊ C 

## 19 17 19 18 Average Meter Temperature  ̊ F 

## 67 62 66 65 Average Absolute Meter Pressure in Hg 

## 29.72 30.12 30.05 29.96 Average Absolute Meter Pressure kPa 

## 100.64 101.98 101.73 101.45 Average Delta P in H 2 

## O 

## 0.13 0.14 0.13 0.13 Average Delta H in H 2 

## O 

## 1.01 1.09 1.04 1.05 Average Sample Rate Lpm 

## 15.6 16.0 15.9 15.8 Average Sample Rate cfm 

## 0.55 0.57 0.56 0.56
A verage Isokinetic Variation % 

## 99.9 98.1 99.6 99.2 Measurement Parameter 

# LEHDER Environmental Services Ltd.

Emissions Calculations

# 123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls



# LEHDER Environmental Services Ltd Mike Denomme

16-Feb-12 

# Company: Owens Corning


# Plant: Delmar NY


# Stack: DM2 DEP Outlet


# Pollutant: Hexavalent / Total Chromium


# Method: EPA Method 0061 

# Project No.: 123987 

# Operators RS / JH 

# Data Entry: KH / JE 

# Reviewed By: MD

Ref.Temperature: 68 deg. F
Ref. Pressure: 29.92 "Hg Velocity Constant: 85.49
Molar Volume: 24.04 l/mol



# Sampling Data Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22 No. of Sample Points 30 30 30 Sample Time /Point min 8.0 7.0 7.0 Reading / Point min 4.0 3.5 3.5 Total Sample Time, min 240.0 210.0 210.0 Barometric Pressure, Pb "Hg 29.65 30.04 29.97 Stack Gauge Pressure, Pgauge "H2O -0.95 -0.88 -0.88 Absolute Stack Pressure, Ps "Hg 29.58 29.98 29.91 Pitot Tube Coefficient, Cp 0.781 0.781 0.781 Oxygen Content, O2 % 20.0 20.1 20.0 Carbon Dioxide Content, CO2 % 4.21 4.70 4.40 Carbon Monoxide Content, CO % 0.0 0.0 0.0 Nitrogen Content, N2 % 75.8 75.2 75.6 Condensate Collected, W H2O 

# g 328.6 269.6 283.9 Nozzle Diameter, Dn in 0.3595 0.3595 0.3595 Initial DGM Reading ft 3 

# 224.486 511.998 778.121 Final DGM Reading ft 3 

# 360.941 624.817 892.535 DGM Unity, Y 0.9991 0.9991 0.9991
Stack Width ft 3.280 3.280 3.280 Stack Depth ft 3.280 3.280 3.280 Actual Volume of Dry Gas ft 3 

# 136.3322 112.7175 114.3110
Stack Area, As ft 2 

# 10.758 10.758 10.758



# Hex Chromium Analysis

Uncorrected Chromium (Cr ) 6+ 

# ug 145 133 97.0
Blank Correction ug 1.72 1.72 1.72

Corrected Hexavalent Chromium ug 143 131 95.3



# Total Chromium Analysis

Total Chromium - (1) KOH & Rinses ug 162 153 115 Total Chromium - (3) Nitric Rinse ug 1.06 1.22 0.706 Total Chromium - (3) Column Filter ug 1.09 1.08 0.601
Uncorrected Total Chromium ug 164.2 155.3 116.3 Blank Correction (4) ug 3.14 3.14 3.14 Total Chromium (1 + 2 + 3) - 4 ug 161.0 152.2 113.2

Italics indicate values less than method detection

Input1123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls



### LEHDER Environmental Services Ltd Point by Point Sampling Data

Company: Owens Corning

Plant: Delmar NY

Stack: DM2 DEP Outlet

Pollutant: Hexavalent / Total Chromium Project No.: 123987

Test #1 Test #2 Test #3

24-Jan-12 25-Jan-12 26-Jan-12

08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo Time Vd Delta P Delta H Ts Tmi Tmo

# min ft 3 H 2 O H 2 O F F F # min ft 3 H 2 O H 2 O F F F # min ft 3 H 2 O H 2 O F F F

P1-1 0.0 224.49 0.140 1.21 420 67 68 P1-1 0.0 512.00 0.140 1.22 412 67 67 P1-1 0.0 778.12 0.135 1.18 412 70 70

4.0 226.82 0.140 1.22 412 67 68 3.5 514.08 0.135 1.18 410 66 67 3.5 780.13 0.140 1.23 412 68 70

2 8.0 229.22 0.135 1.18 412 66 68 2 7.0 516.09 0.130 1.13 411 65 67 2 7.0 782.13 0.120 1.06 406 68 70

12.0 231.54 0.135 1.18 406 65 67 10.5 518.04 0.120 1.05 405 64 67 10.5 784.00 0.120 1.06 406 68 70

3 16.0 233.84 0.120 1.05 407 65 67 3 14.0 519.90 0.110 0.96 406 64 67 3 14.0 785.85 0.110 0.97 407 68 70

20.0 236.03 0.120 1.05 408 65 67 17.5 521.68 0.120 1.05 406 64 66 17.5 787.65 0.110 0.97 408 68 70

4 24.0 238.20 0.135 1.18 407 66 67 4 21.0 523.53 0.130 1.14 406 64 66 4 21.0 789.42 0.135 1.18 412 68 70

28.0 240.50 0.135 1.18 413 66 67 24.5 525.46 0.130 1.14 408 64 66 24.5 791.40 0.135 1.18 412 68 70

5 32.0 242.78 0.140 1.22 413 66 67 5 28.0 527.41 0.135 1.18 409 64 66 5 28.0 793.37 0.135 1.18 413 68 70

36.0 245.14 0.140 1.22 414 66 67 31.5 529.35 0.130 1.13 409 63 66 31.5 795.36 0.135 1.18 414 68 70

6 40.0 247.49 0.120 1.06 405 67 67 6 35.0 531.32 0.110 0.97 397 63 66 6 35.0 797.29 0.130 1.14 413 68 70

44.0 249.65 0.120 1.06 405 67 67 38.5 533.17 0.110 0.97 397 65 66 38.5 799.27 0.130 1.14 413 68 70

P2-1 48.0 251.85 0.130 1.14 405 67 67 P2-1 42.0 534.95 0.120 1.05 405 64 66 P2-1 42.0 801.22 0.130 1.14 412 67 70

52.0 254.05 0.130 1.14 410 67 67 45.5 536.79 0.120 1.05 406 64 66 45.5 803.12 0.130 1.14 412 67 69

2 56.0 256.35 0.120 1.05 410 67 67 2 49.0 538.66 0.110 0.97 403 63 66 2 49.0 805.08 0.115 1.01 410 67 69

60.0 258.52 0.120 1.05 406 67 67 52.5 540.47 0.105 0.92 403 63 65 52.5 806.92 0.115 1.01 409 67 69

3 64.0 260.66 0.110 0.97 407 67 67 3 56.0 542.22 0.095 0.83 404 63 65 3 56.0 808.77 0.100 0.88 409 66 69

68.0 262.77 0.110 0.97 406 67 67 59.5 543.88 0.095 0.83 404 63 65 59.5 810.49 0.100 0.88 410 66 69

4 72.0 264.86 0.115 1.01 409 66 67 4 63.0 545.53 0.110 0.96 407 63 65 4 63.0 812.18 0.115 1.00 414 66 68

76.0 266.99 0.115 1.00 410 66 67 66.5 547.30 0.110 0.96 408 62 65 66.5 814.05 0.115 1.00 415 66 68

5 80.0 269.13 0.135 1.18 410 66 67 5 70.0 549.09 0.120 1.04 411 62 65 5 70.0 815.82 0.130 1.13 418 65 68

84.0 271.38 0.130 1.13 413 66 67 73.5 550.94 0.120 1.04 411 62 64 73.5 817.76 0.130 1.12 419 65 68

6 88.0 273.64 0.140 1.22 416 66 67 6 77.0 552.79 0.120 1.04 413 62 64 6 77.0 819.68 0.130 1.12 422 65 67

92.0 275.94 0.140 1.21 417 66 66 80.5 554.65 0.120 1.04 413 62 64 80.5 821.60 0.130 1.12 423 64 67
P3-1 96.0 278.27 0.110 0.96 407 65 67 P3-1 84.0 556.53 0.120 1.05 406 62 64 P3-1 84.0 823.45 0.120 1.04 412 64 67

100.0 280.35 0.130 1.14 406 65 66 87.5 558.38 0.120 1.05 406 62 64 87.5 825.30 0.120 1.04 412 64 66

2 104.0 282.53 0.110 0.97 404 65 66 2 91.0 560.22 0.100 0.87 404 62 64 2 91.0 827.15 0.100 0.87 410 64 66

108.0 284.62 0.110 0.97 404 65 66 94.5 561.92 0.095 0.83 404 62 64 94.5 828.85 0.100 0.87 411 64 66

3 112.0 286.77 0.110 0.97 403 65 66 3 98.0 563.58 0.090 0.78 405 61 64 3 98.0 830.54 0.100 0.87 412 65 66

116.0 288.85 0.100 0.88 405 65 66 101.5 565.18 0.090 0.78 405 61 63 101.5 832.25 0.100 0.87 412 65 66

4 120.0 290.84 0.120 1.05 408 65 66 4 105.0 566.78 0.100 0.87 408 61 63 4 105.0 833.93 0.110 0.95 416 65 66

124.0 292.91 0.115 1.01 408 66 66 108.5 568.45 0.100 0.87 409 61 63 108.5 835.70 0.110 0.95 418 64 66

5 128.0 295.05 0.130 1.13 413 66 66 5 112.0 570.15 0.125 1.08 412 61 63 5 112.0 837.48 0.125 1.07 423 65 66

132.0 297.19 0.140 1.22 415 66 66 115.5 572.03 0.130 1.12 415 61 63 115.5 839.35 0.125 1.07 424 65 66

6 136.0 299.50 0.140 1.21 418 66 66 6 119.0 573.92 0.130 1.11 420 61 63 6 119.0 841.21 0.130 1.11 425 65 66

140.0 301.77 0.140 1.21 418 67 67 122.5 575.85 0.130 1.11 420 61 63 122.5 843.09 0.130 1.11 426 65 66

P4-1 144.0 304.02 0.170 1.48 412 67 67 P4-1 126.0 577.73 0.120 1.05 405 63 63 P4-1 126.0 844.94 0.150 1.29 422 65 66

148.0 306.45 0.170 1.48 415 66 67 129.5 579.58 0.140 1.21 412 62 63 129.5 846.99 0.150 1.29 422 65 66

2 152.0 308.87 0.140 1.25 412 66 67 2 133.0 581.58 0.110 0.95 411 62 63 2 133.0 849.05 0.120 1.04 419 65 66

156.0 311.23 0.140 1.22 410 66 66 136.5 583.39 0.110 0.95 411 62 63 136.5 850.92 0.120 1.04 419 65 66

3 160.0 313.49 0.130 1.13 411 66 66 3 140.0 585.16 0.105 0.91 412 61 63 3 140.0 852.76 0.115 0.99 421 64 66

164.0 315.70 0.120 1.05 412 66 66 143.5 586.88 0.105 0.91 413 61 63 143.5 854.58 0.115 0.99 421 64 66

4 168.0 317.83 0.140 1.21 417 66 66 4 147.0 588.61 0.120 1.03 416 61 63 4 147.0 856.40 0.120 1.03 422 64 66

172.0 320.09 0.140 1.21 416 66 66 150.5 590.46 0.120 1.03 417 61 63 150.5 858.24 0.120 1.03 424 64 65

5 176.0 322.38 0.150 1.29 420 66 66 5 154.0 592.32 0.140 1.20 422 62 63 5 154.0 860.08 0.135 1.15 431 64 65

180.0 324.75 0.150 1.29 421 66 66 157.5 594.29 0.140 1.19 425 61 63 157.5 862.02 0.140 1.19 431 64 65

6 184.0 327.15 0.145 1.25 421 66 66 6 161.0 596.31 0.140 1.19 427 61 63 6 161.0 864.00 0.140 1.19 434 64 65

188.0 329.51 0.145 1.24 426 65 66 164.5 598.22 0.140 1.19 427 61 63 164.5 865.99 0.140 1.18 435 64 65
P5-1 192.0 331.86 0.160 1.37 426 65 66 P5-1 168.0 600.16 0.160 1.36 427 62 63 P5-1 168.0 867.91 0.160 1.36 433 64 65

196.0 334.33 0.170 1.46 425 65 66 171.5 602.24 0.165 1.40 427 62 63 171.5 870.05 0.165 1.40 435 64 65

2 200.0 336.87 0.160 1.38 423 66 66 2 175.0 604.41 0.160 1.36 426 62 63 2 175.0 872.19 0.155 1.32 431 64 65

204.0 339.35 0.160 1.38 423 66 66 178.5 606.55 0.155 1.32 426 62 63 178.5 874.30 0.155 1.32 430 64 65

3 208.0 341.82 0.160 1.38 423 66 66 3 182.0 608.62 0.155 1.32 427 62 63 3 182.0 876.43 0.150 1.28 431 64 65

212.0 344.25 0.155 1.33 424 66 66 185.5 610.71 0.155 1.32 427 62 63 185.5 878.40 0.150 1.28 431 64 65

4 216.0 346.68 0.160 1.37 428 66 66 4 189.0 612.79 0.155 1.32 428 62 63 4 189.0 880.41 0.155 1.31 436 64 65

220.0 349.12 0.160 1.37 429 66 66 192.5 614.85 0.155 1.31 430 62 63 192.5 882.42 0.155 1.31 437 64 65

5 224.0 351.59 0.160 1.36 432 66 66 5 196.0 616.93 0.150 1.27 431 62 63 5 196.0 884.51 0.155 1.30 440 64 65

228.0 354.05 0.155 1.32 432 66 66 199.5 618.98 0.150 1.27 432 62 63 199.5 886.55 0.155 1.30 441 64 65

6 232.0 356.40 0.140 1.19 430 66 66 6 203.0 620.99 0.140 1.19 429 62 63 6 203.0 888.63 0.145 1.22 440 64 65

236.0 358.68 0.140 1.19 430 66 66 206.5 622.95 0.140 1.19 428 62 63 206.5 890.60 0.145 1.22 439 64 65

240.0 360.94 210.0 624.82 210.0 892.54

Input2

### 123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls



### LEHDER Environmental Services Ltd Point by Point Calculations

Company: Owens Corning

Plant: Delmar NY

Stack: DM2 DEP Outlet

Pollutant: Hexavalent / Total Chromium Project No. : 123987 

### Data Entry: KH / JE

Point Period Isokinecity Point Period Isokinecity Point Time Isokinecity

min m 3 ft 3 m/s ft/s % min m 3 ft 3 m/s ft/s % min m 3 ft 3 m/s ft/s %



### P1-1 4.0 0.066 2.33 7.8 25.6 100.6 

### P1-1 3.5 0.059 2.08 7.7 25.3 102.5 

### P1-1 3.5 0.057 2.01 7.6 24.9 100.5

4.0 0.068 2.40 7.8 25.5 102.9 3.5 0.057 2.01 7.6 24.8 101.0 3.5 0.056 1.99 7.7 25.4 98.2



### 2 4.0 0.066 2.31 7.6 25.0 101.2 

### 2 3.5 0.055 1.95 7.4 24.4 99.9 

### 2 3.5 0.053 1.87 7.1 23.4 99.3

4.0 0.065 2.30 7.6 25.0 100.6 3.5 0.053 1.86 7.1 23.3 99.2 3.5 0.052 1.84 7.1 23.4 97.7


### 3 4.0 0.062 2.19 7.2 23.5 101.3 

### 3 3.5 0.050 1.78 6.8 22.3 99.0 

### 3 3.5 0.051 1.80 6.8 22.4 99.6

4.0 0.061 2.17 7.2 23.6 100.4 3.5 0.052 1.85 7.1 23.3 98.6 3.5 0.050 1.77 6.8 22.4 98.3



### 4 4.0 0.065 2.30 7.6 25.0 100.4 

### 4 3.5 0.055 1.93 7.4 24.3 98.8 

### 4 3.5 0.056 1.98 7.6 24.9 99.2

4.0 0.065 2.28 7.6 25.1 100.0 3.5 0.055 1.94 7.4 24.3 99.7 3.5 0.056 1.97 7.6 24.9 98.6



### 5 4.0 0.067 2.36 7.8 25.5 101.5 

### 5 3.5 0.055 1.94 7.6 24.8 97.9 

### 5 3.5 0.056 1.99 7.6 24.9 100.1

4.0 0.066 2.34 7.8 25.5 100.9 3.5 0.056 1.97 7.4 24.3 101.0 3.5 0.055 1.93 7.6 24.9 96.9


### 6 4.0 0.061 2.16 7.2 23.5 99.9 

### 6 3.5 0.052 1.85 6.8 22.2 102.7 

### 6 3.5 0.056 1.97 7.5 24.4 101.0

4.0 0.062 2.20 7.2 23.5 101.6 3.5 0.050 1.78 6.8 22.2 98.4 3.5 0.055 1.95 7.5 24.4 99.9


### P2-1 4.0 0.062 2.20 7.5 24.5 97.7 

### P2-1 3.5 0.052 1.84 7.1 23.3 97.8 

### P2-1 3.5 0.054 1.90 7.4 24.4 97.2

4.0 0.065 2.30 7.5 24.5 102.2 3.5 0.053 1.87 7.1 23.3 99.8 3.5 0.055 1.95 7.4 24.4 100.1



### 2 4.0 0.061 2.17 7.2 23.6 100.6 

### 2 3.5 0.051 1.80 6.8 22.3 100.4 

### 2 3.5 0.052 1.84 7.0 23.0 100.3

4.0 0.060 2.13 7.2 23.5 98.7 3.5 0.050 1.75 6.6 21.8 99.7 3.5 0.052 1.84 7.0 22.9 100.2


### 3 4.0 0.060 2.11 6.9 22.5 102.0 

### 3 3.5 0.047 1.67 6.3 20.7 100.0 

### 3 3.5 0.049 1.72 6.5 21.4 100.5

4.0 0.059 2.09 6.9 22.5 100.7 3.5 0.047 1.64 6.3 20.7 98.6 3.5 0.048 1.68 6.5 21.4 98.3



### 4 4.0 0.060 2.12 7.0 23.1 100.5 

### 4 3.5 0.050 1.77 6.8 22.3 98.7 

### 4 3.5 0.053 1.87 7.0 23.0 102.3

4.0 0.061 2.14 7.0 23.1 101.3 3.5 0.051 1.79 6.8 22.4 100.0 3.5 0.050 1.77 7.0 23.0 96.6



### 5 4.0 0.064 2.25 7.6 25.0 98.6 

### 5 3.5 0.052 1.84 7.1 23.4 98.9 

### 5 3.5 0.055 1.94 7.5 24.5 99.9

4.0 0.064 2.26 7.5 24.6 100.8 3.5 0.052 1.85 7.1 23.4 99.3 3.5 0.054 1.91 7.5 24.5 98.7


### 6 4.0 0.065 2.30 7.8 25.6 99.1 

### 6 3.5 0.053 1.86 7.1 23.4 100.1 

### 6 3.5 0.054 1.92 7.5 24.6 99.5

4.0 0.066 2.33 7.8 25.6 100.5 3.5 0.053 1.87 7.1 23.4 100.7 3.5 0.052 1.85 7.5 24.6 95.7

P3-1 4.0 0.059 2.08 6.9 22.5 100.6 P3-1 3.5 0.052 1.85 7.1 23.3 99.0 P3-1 3.5 0.05 1.85 7.2 23.5 99.2

4.0 0.062 2.17 7.5 24.5 96.8 3.5 0.052 1.84 7.1 23.3 98.7 3.5 0.05 1.85 7.2 23.5 98.9

2 4.0 0.059 2.09 6.9 22.5 101.2 2 3.5 0.048 1.69 6.5 21.3 99.2 2 3.5 0.05 1.70 6.5 21.4 99.6

4.0 0.061 2.14 6.9 22.5 103.6 3.5 0.047 1.66 6.3 20.7 99.9 3.5 0.05 1.69 6.5 21.4 99.2

3 4.0 0.059 2.08 6.9 22.5 100.7 3 3.5 0.045 1.59 6.2 20.2 98.5 3 3.5 0.05 1.71 6.5 21.4 100.0

4.0 0.056 1.99 6.5 21.5 100.9 3.5 0.045 1.60 6.2 20.2 99.2 3.5 0.05 1.68 6.5 21.4 98.6

4 4.0 0.058 2.06 7.2 23.6 95.8 4 3.5 0.047 1.66 6.5 21.3 97.8 4 3.5 0.05 1.76 6.9 22.5 98.7

4.0 0.061 2.14 7.0 23.1 101.5 3.5 0.048 1.70 6.5 21.3 100.0 3.5 0.05 1.78 6.9 22.6 100.2

5 4.0 0.061 2.14 7.5 24.6 95.6 5 3.5 0.053 1.88 7.3 23.9 99.0 5 3.5 0.05 1.87 7.3 24.1 98.7

4.0 0.065 2.31 7.8 25.5 99.5 3.5 0.054 1.89 7.4 24.4 98.1 3.5 0.05 1.86 7.4 24.1 98.2

6 4.0 0.064 2.27 7.8 25.6 98.0 6 3.5 0.055 1.93 7.5 24.5 100.2 6 3.5 0.05 1.88 7.5 24.6 97.4

4.0 0.064 2.25 7.8 25.6 97.1 3.5 0.053 1.87 7.5 24.5 97.3 3.5 0.05 1.85 7.5 24.6 96.1

P4-1 4.0 0.069 2.42 8.6 28.1 94.6 P4-1 3.5 0.052 1.85 7.1 23.3 99.0 P4-1 3.5 0.06 2.05 8.0 26.4 98.6

4.0 0.068 2.42 8.6 28.1 94.6 3.5 0.057 2.00 7.7 25.3 99.6 3.5 0.06 2.06 8.0 26.4 99.2

2 4.0 0.067 2.36 7.8 25.5 101.4 2 3.5 0.051 1.81 6.8 22.4 101.6 2 3.5 0.05 1.87 7.2 23.6 100.5

4.0 0.064 2.26 7.8 25.5 97.1 3.5 0.050 1.76 6.8 22.4 99.0 3.5 0.05 1.84 7.2 23.6 98.9

3 4.0 0.063 2.21 7.5 24.6 98.6 3 3.5 0.049 1.72 6.7 21.9 98.9 3 3.5 0.05 1.81 7.0 23.1 99.8

4.0 0.060 2.13 7.2 23.6 98.9 3.5 0.049 1.73 6.7 21.9 99.8 3.5 0.05 1.83 7.0 23.1 100.5

4 4.0 0.064 2.26 7.8 25.6 97.5 4 3.5 0.052 1.85 7.2 23.5 99.7 4 3.5 0.05 1.83 7.2 23.6 98.7

4.0 0.065 2.28 7.8 25.6 98.5 3.5 0.052 1.85 7.2 23.5 100.0 3.5 0.05 1.84 7.2 23.6 99.6

5 4.0 0.067 2.37 8.1 26.5 99.0 5 3.5 0.056 1.97 7.8 25.4 98.6 5 3.5 0.05 1.94 7.7 25.2 99.3

4.0 0.068 2.40 8.1 26.5 100.5 3.5 0.057 2.02 7.8 25.5 101.6 3.5 0.06 1.98 7.8 25.6 99.3

6 4.0 0.067 2.35 7.9 26.1 100.1 6 3.5 0.054 1.91 7.8 25.5 95.9 6 3.5 0.06 1.99 7.8 25.7 100.1

4.0 0.066 2.35 8.0 26.2 100.2 3.5 0.055 1.94 7.8 25.5 97.4 3.5 0.05 1.92 7.8 25.7 96.6

P5-1 4.0 0.070 2.47 8.4 27.5 100.4 P5-1 3.5 0.059 2.08 8.3 27.3 97.7 P5-1 3.5 0.06 2.13 8.4 27.4 100.4

4.0 0.072 2.54 8.6 28.3 100.1 3.5 0.061 2.17 8.4 27.7 100.5 3.5 0.06 2.14 8.5 27.9 99.2

2 4.0 0.070 2.47 8.4 27.4 100.2 2 3.5 0.060 2.13 8.3 27.2 100.1 2 3.5 0.06 2.11 8.2 27.0 100.9

4.0 0.070 2.47 8.4 27.4 100.0 3.5 0.059 2.07 8.2 26.8 98.9 3.5 0.06 2.13 8.2 27.0 101.6

3 4.0 0.069 2.43 8.4 27.4 98.4 3 3.5 0.059 2.09 8.2 26.8 99.6 3 3.5 0.06 1.97 8.1 26.5 95.6

4.0 0.069 2.43 8.2 27.0 100.2 3.5 0.059 2.08 8.2 26.8 99.1 3.5 0.06 2.01 8.1 26.5 97.3

4 4.0 0.069 2.44 8.4 27.5 99.1 4 3.5 0.058 2.07 8.2 26.8 98.7 4 3.5 0.06 2.01 8.2 27.0 96.3

4.0 0.070 2.47 8.4 27.5 100.4 3.5 0.059 2.08 8.2 26.9 99.3 3.5 0.06 2.09 8.2 27.1 100.1

5 4.0 0.070 2.46 8.4 27.6 100.1 5 3.5 0.058 2.05 8.1 26.5 99.6 5 3.5 0.06 2.04 8.3 27.1 97.9

4.0 0.066 2.35 8.3 27.1 97.2 3.5 0.057 2.00 8.1 26.5 97.5 3.5 0.06 2.07 8.3 27.1 99.5

6 4.0 0.064 2.27 7.9 25.8 98.9 6 3.5 0.056 1.96 7.8 25.5 98.6 6 3.5 0.06 1.97 8.0 26.2 97.8

4.0 0.064 2.26 7.9 25.8 98.5 3.5 0.053 1.87 7.8 25.5 93.9 3.5 0.05 1.94 8.0 26.2 96.0 

### Test #3

26-Jan-12

07:52 - 11:22 Test #1

24-Jan-12

08:27 - 12:55

Sample Volume Stack Velocity 

### Test #2

25-Jan-12

08:03 - 11:49

Sample Volume Stack Velocity Sample Volume Stack Velocity



### ISO-Velocity Calculations

## 123987 DM2 DEP Outlet M0061 Hex-Chromium Calculations.xls

Company: Owens Corning Pollutant: Hexavalent / Total Chromium
Plant: Delmar NY Method: EPA Method 0061
Stack: DM2 DEP Outlet Project No.: 123987

Reviewed b y MD

Test #1 Test #2 Test #3
24-Jan-12 25-Jan-12 26-Jan-12 Average
08:27 - 12:55 08:03 - 11:49 07:52 - 11:22

Hexavalent Chromium Concentration ug/S.m 3 

## 3.72E+01 4.05E+01 2.92E+01 3.56E+01
Hexavalent Chromium Mass Rate ug/s 

## 1.53E+02 1.60E+02 1.17E+02 1.43E+02 mg/s 

## 1.53E-01 1.60E-01 1.17E-01 1.43E-01 g/hr 

## 5.49E-01 5.77E-01 4.20E-01 5.16E-01

lb./hr 

## 1.21E-03 1.27E-03 9.26E-04 1.14E-03

Total Chromium Concentration ug/S.m 3 

## 4.18E+01 4.69E+01 3.47E+01 4.11E+01
Total Chromium Mass Rate ug/s 

## 1.71E+02 1.86E+02 1.39E+02 1.65E+02 mg/s 

## 1.71E-01 1.86E-01 1.39E-01 1.65E-01 g/hr 

## 6.17E-01 6.69E-01 4.99E-01 5.95E-01

lb./hr 

## 1.36E-03 1.48E-03 1.10E-03 1.31E-03


# Effluent Characteristics
Area of Sample Plane m 2 

## 0.999 0.999 0.999 0.999 Area of Sample Plane ft 2 

## 10.758 10.758 10.758 10.758 Average Stack Temperature  ̊ C 

## 212 212 216 213 Average Stack Temperature (Ts)  ̊ F 

## 414 414 420 416 Average Stack Gas Pressure kPa 

## 100.15 101.49 101.25 100.96 Average Stack Gas Pressure (Psa) in Hg 

## 29.58 29.98 29.91 29.82 Average Stack Gas Velocity m/s 

## 7.65 7.27 7.45 7.46 Average Stack Gas Velocity ft/min 

## 1.51E+03 1.43E+03 1.47E+03 1.47E+03 Oxygen Concentration % vol 

## 20.0 20.1 20.0 20.0
Carbon Dioxide Concentration % vol 

## 4.2 4.7 4.4 4.4 Effluent Molecular Weight (dry) g/gmol 

## 29.5 29.6 29.5 29.5 Effluent Molecular Weight (wet) g/gmol 

## 28.3 28.4 28.3 28.3
Effluent Moisture Content % vol. 

## 10.2 10.0 10.4 10.2 Dry Gas Fraction % vol. 

## 89.8 90.0 89.6 89.8
Actual Effluent Flow Rate A.m 3 

## /s 

## 7.65 7.27 7.44 7.45
Actual Effluent Flow Rate Acfm 

## 1.62E+04 1.54E+04 1.58E+04 1.58E+04 Reference Flow Rate (wet) S.m 3 

## /s 

## 4.57 4.40 4.46 4.48 Standard Flow Rate (wet) Scfm 

## 9.67E+03 9.32E+03 9.45E+03 9.48E+03 Reference Flow Rate (dry) S.m 3 

## /s (dry) 

## 4.10 3.96 4.00 4.02 Standard Flow Rate (dry) Scfm (dry) 

## 8.68E+03 8.39E+03 8.47E+03 8.52E+03
Sample Parameters Sample Period min 

## 240.0 210.0 210.0 220.0 Sample Period Hours 

## 4.0 3.5 3.5 3.7 Sample Volume A.m 3 

## 3.860 3.192 3.237 3.430 Sample Volume acf 

## 136.332 112.717 114.311 121.120
Hexavalent Chromium ug 

## 143 131 95 123
Total Chromium ug 

## 161 152 113 142 Dry Reference Sample Volume S.m 3 

## 3.850 3.242 3.262 3.451 Dry Standard Sample Volume Scf 

## 135.95 114.49 115.21 121.88 Water Vapour Reference Volume S.m 3 

## 0.439 0.360 0.379 0.393 Water Vapour Reference Volume scf 

## 15.50 12.72 13.39 13.87 Average Meter Temperature  ̊ C 

## 19 17 19 18 Average Meter Temperature  ̊ F 

## 66 63 66 65 Average Absolute Meter Pressure in Hg 

## 29.74 30.12 30.05 29.97 Average Absolute Meter Pressure kPa 

## 100.68 101.98 101.75 101.47 Average Delta P in H 2 

## O 

## 0.14 0.13 0.13 0.13 Average Delta H in H 2 

## O 

## 1.18 1.08 1.11 1.12 Average Sample Rate Lpm 

## 16.1 15.2 15.4 15.6 Average Sample Rate cfm 

## 0.57 0.54 0.54 0.55
A verage Isokinetic Variation % 

## 99.7 99.4 99.0 99.4 Measurement Parameter 

# LEHDER Environmental Services Ltd.

Emissions Calculations

# Appendix B
Analytical Report

B.1: Enthalpy PM Report B.2: Element One M29 Report B.3: Element One M0061 Report

# Appendix B.1

Enthalpy PM Report

# Appendix B.2

Element One M29 Report

# Enthalpy
800 Capitola Dr., Ste. 1 Durham, NC 27713



# Project Number: 123987

Chromium

EPA Method 29 Analysis

Analytical Report
18207

Element One, Inc. 5022-C Wrightsville Av., Wilmington, NC 28403
910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com 

# el 1

# element One
18207 Enthalpy M29 Report Packet.doc Page 3 of 23 

# SUMMARY OF RESULTS

# element One
18207 Enthalpy M29 Report Packet.doc Page 4 of 23 

# Summary of Analysis

DM2 - Front Half - Summary of Method 29 Metals Analysis

DM2 DEP Outlet-R1 DM2 DEP Outlet-R2 DM2 DEP Outlet-R2 DM2 DEP Outlet-R3

e18207-1FH e18207-2FH e18207-2FH dup e18207-3FH 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Chromium 191 180 178 151

DM2 - Back Half - Summary of Method 29 Metals Analysis

DM2 DEP Outlet-R1 DM2 DEP Outlet-R2 DM2 DEP Outlet-R2 DM2 DEP Outlet-R3

e18207-1BH e18207-2BH e18207-2BH dup e18207-3BH 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Chromium 0.751 0.924 0.923 1.13

DM1 - Front Half - Summary of Method 29 Metals Analysis

DM1 DEP Outlet-R1 DM1 DEP Outlet-R2 DM1 DEP Outlet-R2 DM1 DEP Outlet-R3 DM1&DM2
Blank

e18207-4FH e18207-5FH e18207-5FH dup e18207-6FH e18207-7FH 

# Element Total μg Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- --------------- 

# Chromium 21.2 19.0 16.9 19.8 1.55

DM1 - Back Half - Summary of Method 29 Metals Analysis

DM1 DEP Outlet-R1 DM1 DEP Outlet-R2 DM1 DEP Outlet-R2 DM1 DEP Outlet-R3 DM1&DM2
Blank

e18207-4BH e18207-5BH e18207-5B H dup e18207-6BH e18207-7BH 

# Element Total μg Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- --------------- 

# Chromium 0.644 0.641 0.597 0.425 0.424

# element One
18207 Enthalpy M29 Report Packet.doc Page 5 of 23 

# ANALYTICAL NARRATIVE

# element One
18207 Enthalpy M29 Report Packet.doc Page 6 of 23 

# Element One Analytical Narrative

Client: Enthalpy 

# Element One #: 18207



# Client ID: 123987/OC – Delmar 

# Analyst: DBW



# Method: Method 29 

# Dates Received: 02/14/12


# Analytes: Cr 

# Dates Analyzed: 02/20/12



# Summary of Analysis

The Method 29 samples were digested, prepared, and analyzed according to Method 29 protocol. Samples were analyzed for total chromium on a PerkinElmer ELAN 6100 ICP-MS.

Detection Limits

The ICP-MS instrument reporting lim it was 1.0μg/L for total chromium.

Analysis QA/QC

Duplicate analyses relative percent diffe rence (RPD), spike sample recovery, and
second source calibration verification data are summarized in the Quality Control Section. All QA/QC data was within the criteria of the method.

Additional Comments

The reported results have not been correct ed for any blank values or spike recovery values. The ICP analysis of the Blank samples revealed detectable
concentrations of chromium.

# element One
18207 Enthalpy M29 Report Packet.doc Page 7 of 23 

# QUALITY CONTROL SUMMARY

# element One
18207 Enthalpy M29 Report Packet.doc Page 8 of 23 

# Summary of Quality Control Data

Metals Duplicate Analysis RPD

(Method 29 QC limits: < 20% for RPD) 

# DM2 DEP Outlet-R2
Front Half DM2 DEP Outlet-R2
Back Half DM1 DEP Outlet-R2
Front Half DM1 DEP Outlet-R2
Back Half
Element RPD RPD RPD RPD

------------------ ----------------- ----------------- ----------------- ----------------- 

# Chromium 1.2% 0.1% 12.0% 7.1%

Metals Analysis Spike Recoveries

(Method 29 QC limits: ±25% for Spike Recoveries) 

# DM2 DEP Outlet-R2
Front Half DM2 DEP Outlet-R2
Back Half DM1 DEP Outlet-R2
Front Half DM1 DEP Outlet-R2
Back Half
Element Recovery Recovery Recovery Recovery

------------------ ----------------- ----------------- ----------------- ----------------- 

# Chromium 97% 100% 95% 92% *See Analytical Narrative, page 12.



# Second Source Calibration Check Recoveries
(Method 29 QC limits: ±10% for Second Source Continuing Check Standard*) 

# Element 1 ppb 50 ppb 100 ppb* 250 ppb

----------------- ----------------- ----------------- ----------------- ----------------- 

# Chromium 88% 91% 97% 100%

# element One
18207 Enthalpy M29 Report Packet.doc Page 9 of 23 

# SAMPLE CUSTODY

# element One
18207 Enthalpy M29 Report Packet.doc Page 10 of 23

# element One
18207 Enthalpy M29 Report Packet.doc Page 11 of 23 

# ANALYTICAL DATA

# element One
18207 Enthalpy M29 Report Packet.doc Page 12 of 23 

# Analytical Calculations

MetalsElement Results (μg) =ICP Result s (μg/L)*Dilution*Final Volume (L)

WhereICP Results= Raw sample concentration (ppb)-- ICP-Data Sheet



# Dilution= Diluted Volume

-- ICP-MS Run Sheet 

# Aliquot

Final Volume=FH=Final Volume (FV)-- Sample Submission 

# BH=Received Volume (BV) .*Final Volume (FV)-- Sample Submission 

# Aliquot (Used) Combined Results=FH+BH

MercuryMercury Results (μg) =CVAA Results (μg) *Final Volume (ml) Aliquot (ml)

WhereCVAA Results= Raw sample reading (μg)-- Hg-Data Sheet



# Aliquot= Sample Aliquot (Alq.)-- Hg-Data Sheet



# Final Volume=Final Volume (FV)*-- Sample Submission 

# * With the exception of the BH fraction where- =Received Volume (BV)-- Sample Submission

# Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/ L) – Sample Result (μg/L)) X100 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)-- ICP-Data Sheet



# Sample Result = Raw sample concentration (ppb)-- ICP-Data Sheet



# Spike Amount-- ICP-MS Spike Table



# Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/ L) - Sample Result (μg/L)) X100 Average (μg/L)

WhereSample Result and Duplicate Result s=Raw sample concentration (ppb)-- ICP-Data
Sheet



# Average= (Duplicate + Sample Results)

2



# element One
18207 Enthalpy M29 Report Packet.doc Page 13 of 23

# Appendix B.3

Element One M0061 Report

# Enthalpy Analytical, Inc.
800 Capitola Dr., Ste. 1 Durham, NC 27713



# Project No: 123987

Total Chromium and Hexavalent Chromium

EPA Method 0061 Analysis

Analytical Report
18118

Element One, Inc. 5022-C Wrightsville Av., Wilmington, NC 28403
910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com 

# el 1

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 3 of 35 

# SUMMARY OF RESULTS

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 4 of 35 

# Summary of Analysis

DM2 DEP Outlet - Summary of Chromium (VI) Analysis

123987-1-R1 123987-4-R2 123987-4-R2 123987-7-R3

e18118-16 e18118-17 e18118-17 du p e18118-18 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Chromium(VI) 145 133 133 97.0 Duplicate RPD, % 5.2% 4.8% 2.1% 0.3% Spike Recovery, %

----------- - ------------ --- --------- 107% *See Analytical Narrative, page 10.



# DM2 DEP Outlet - 0.1N HNO3 Rinse – Summary of Method 0061 Total Chromium Analysis

123987-2-R1 123987-5-R2 123987-5-R2 123987-8-R3
e1 Sample ID e18118-1 e18118-2 e18118-2 Dup e18118-3 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium 1.06 1.22 1.45 0.706

DM2 DEP Outlet - Filter – Summary of Method 0061 Total Chromium Analysis

123987-3-R1 123987-6-R2 123987-6-R2 123987-9-R3
e1 Sample ID e18118-9 e18118-10 e18118-10 Dup e18118-11 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium 1.09 1.08 1.11 0.601

DM2 DEP Outlet - 0.5M KOH – Summary of Method 0061 Total Chromium Analysis

123987-1-R1 123987-4-R2 123987-4-R2 123987-7-R3
e1 Sample ID e18118-16 e18118-17 e18118-17 dup e18118-18 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium 162 153 173 115 *See Analytical Narrative, page 7.

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 5 of 35 

# Summary of Analysis

DM1 DEP Outlet - Summary of Chromium (VI) Analysis

123987-10-R1 123987-13-R2 123987-13-R2 123987-16-R3

e18118-19 e18118-20 e18118-20 du p e18118-21 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Chromium(VI) 12.5 11.8 11.7 8.87 Duplicate RPD, % 0.6% 0.5% 0.3% 1.1% Spike Recovery, %

----------- - ------------ --- --------- 108% *See Analytical Narrative, page 10.



# DM1 DEP Outlet - 0.1N HNO3 Rinse – Summary of Method 0061 Total Chromium Analysis

123987-11-R1 123987-14-R2 123987-14-R2 123987-17-R3
e1 Sample ID e18118-4 e18118-5 e18118-5 Dup e18118-6 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium 0.390 0.355 0.346 0.281

DM1 DEP Outlet - Filter – Summary of Method 0061 Total Chromium Analysis

123987-12-R1 123987-15-R2 123987-15-R2 123987-18-R3
e1 Sample ID e18118-12 e18118-13 e18118-13 Dup e18118-14 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium 0.916 1.24 1.04 0.750

DM1 DEP Outlet - 0.5M KOH – Summary of Method 0061 Total Chromium Analysis

123987-10-R1 123987-13-R2 123987-13-R2 123987-16-R3
e1 Sample ID e18118-19 e18118-20 e18118-20 dup e18118-21 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium 17.2 18.9 20.3 11.4

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 6 of 35 

# Summary of Analysis

Blank - Summary of Chromium (VI) Analysis

123987-19-KOH 123987-20-DI

e18118-22KOH e18118-8DI 

# Element Total μg Total μg

----------------- --------------- --------------- 

# Chromium(VI) 1.72 < 0.04 Duplicate RPD, % 5.1% NA

Blank – Summary of Method 0061 Total Chromium Analysis

123987-21 123987-20-DI 123987- 22-RB 123987-19-KOH
e1 Sample ID e18118-7 e18118-8 e18118-15 e18118-22KOH 

# Element Total μg Total μg Total μg Total μg

----------------- --------------- --------------- --------------- --------------- 

# Total Chromium < 0.2 < 0.2 0.593 3.14

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 7 of 35 

# ANALYTICAL NARRATIVE

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 8 of 35 

# Element One Analytical Narrative

Client: Enthalpy Analytical, Inc. Element One #: 18118

Client ID: 123987/O.C. Delmar Analyst: DBW & LAL

Method: M0061 Dates Received: 02/01/12

Analytes: Total Chromium & Chromium (VI) Dates Analyzed: 02/07 – 09/12

Summary of Analysis

For Total Chromium analysis the Method 0061 samples were acidified with trace metals grade concentrated nitric acid and digested on a hotplate according to method protocol. Samples were analyz ed for total chromium on a PerkinElmer ELAN 6100 ICP-MS. For Chromium VI analysis the samples were prepared and analyzed according to SW-846 Method 0061 protocol. Samples we re analyzed for chro mium (VI) using a Shimadzu 2010 HPLC unit and a Ti mberline RDR-1 Reaction Module.

Detection Limits

The ICP-MS instrument reporting lim it was 1.0μg/L for total chromium. The Shimadzu 2010 HPLC instrument det ection limit for chromium (VI) was 0.1μg/L.

Analysis QA/QC

Duplicate analyses relative percent diffe rence (RPD) and spike sample recovery
data are summarized with the results. A ll QA/QC data was withi n the criteria of
the method.

Additional Comments

The reported results have not been correct ed for any blank values or spike recovery values. Due to matrix interf erences it was necessary to analyze all KOH fraction samples for chromium (VI) at a minimum two-fold dilution and for
total chromium at a minimu m five-fold dilution. *Ref page 4 and 5; the chromium (VI) result for samples 1007-2001-R1, 1007-2007-R3 and 1007-B-119-RB were less than the Total Chromium result for those samples. The Total Chromium results are at the detection limit.

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 9 of 35 

# QUALITY CONTROL SUMMARY

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 10 of 35 

# Summary of Quality Control Data

0.1N HNO 3 

# - Metals Duplicate Analysis RPD

(Method 0061 QC limits: < 20% for RPD)


# 123987-5-R2 123987-14-R2
Element RPD RPD

------------------ ----------------- ----------------- 

# Total Chromium 16.9% 2.5%

Filter - Metals Duplicate Analysis RPD

(Method 0061 QC limits: < 20% for RPD)


# 123987-6-R2 123987-15-R2
Element RPD RPD

------------------ ----------------- ----------------- 

# Total Chromium 2.0% 17.2%

0.5M KOH - Metals Duplicate Analysis RPD

(Method 0061 QC limits: < 20% for RPD)


# 123987-4-R2 123987-13-R2
Element RPD RPD

------------------ ----------------- ----------------- 

# Total Chromium 12.3% 7.3%

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 11 of 35 

# Summary of Quality Control Data

0.1N HNO 3 

# - Metals Analysis Spike Recoveries

(Method 0061 QC limits: ± 25% for Spike Recoveries.)


# 123987-8-R3 123987-17-R3
Element Recovery Recovery

------------------ ----------------- ----------------- 

# Total Chromium 118% 105%

Filter - Metals Analysis Spike Recoveries

(Method 0061 QC limits: ± 25% for Spike Recoveries.)


# 123987-9-R3 123987-18-R3
Element Recovery Recovery

------------------ ----------------- ----------------- 

# Total Chromium 123% 104%

0.5M KOH - Metals Analysis Spike Recoveries

(Method 0061 QC limits: ± 25% for Spike Recoveries.)


# 123987-7-R3 123987-16-R3
Element Recovery Recovery

------------------ ----------------- ----------------- 

# Total Chromium 115% 115%

Second Source Calibration Check Recoveries
(Method 0061 QC limits: ±10% for Second Source Continuing Check Standard*) 

# Element 1 ppb 50 ppb 100 ppb* 250 ppb

----------------- ----------------- ----------------- ----------------- ----------------- 

# Total Chromium 118% 110% 108% 99%

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 12 of 35 

# SAMPLE CUSTODY

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 13 of 35

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 14 of 35 

# ANALYTICAL DATA

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 15 of 35 

# Analytical Calculations

MetalsElement Results (μg) =ICP Results (μg/L)*Dilution*Begi nning Volume (L)

WhereICP Results= Raw sample concentration (ppb)-- ICP-Data Sheet



# Dilution= Diluted Volume

-- ICP-MS Run Sheet 

# Aliquot

Beginning Volume= (BV)-- Sample Submission



# Cr (VI)-

Total Cr +6 

# (ug) =Cr +6 

# Results (μg/L)*Dilution*Final Volume (mL)/1000

WhereCr +6 

# Results= Raw sample concentration (ppb)— HPLC Data Sheet



# Dilution= Diluted Volume

— HPLC Data Sheet 

# Aliquot

Final Volume-- Sample Submission

# element One 18118 Enthalpy M0061 TCr and Cr6 Report Packet.doc Page 16 of 35 

# Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/L) – Sample Result (μg/L)) X100 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)-- ICP-Data Sheet



# Sample Result = Raw sample concentration (ppb)-- ICP-Data Sheet



# Spike Amount-- ICP-MS Spike Table



# Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/L) - Sample Result (μg/L)) X100 Average (μg/L)

WhereSample Result and Duplicate Result s=Raw sample concentration (ppb)-- ICP-Data
Sheet



# Average= ( Duplicate + Sample Results)

2

# Appendix C

Equipment CalibrationsDec. 14, 2011 (dgm 16)LEHDER ENVIRONMENTAL SERVICES LIMITEDDRY GAS METER CALIBRATION USING CRITICAL ORIFICES1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.4) Record readings in outlined boxes below, other columns are automatically calculated.INITIAL FINALAVG (Pbar)DATE:14-Dec-11METER SERIAL #:16BAROMETRIC PRESSURE (in Hg):29.5729.5029.54 IF Y VARIATION EXCEEDS 2.00%,- - CRITICAL ORIFICE SET SERIAL #: 1477ORIFICE SHOULD BE RECALIBRATEDK' TESTEDTEMPERATURES °F ELAPSEDFACTOR VACUUMDGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGMH(1) (2) (3)% YORIFICE # RUN # (AVG) (in Hg) INITIAL FINALNET (Vm)INITIAL FINAL INITIAL FINAL AVG(in H2O) Vm(STD) Vcr(STD)Y VARIATION KodH@1 0.433523.0107.80 111.783.9870 74 73 71 717271.153.906 3.894 0.99690.6706 2.11016 2 0.433523.0111.78 115.743.9670 73 73 71 717271.153.890 3.894 1.00120.6703 2.1103 0.433523.0115.74 119.693.9670 73 73 71 717271.153.887 3.894 1.00200.6703 2.110AVG = 1.0000 0.09 0.6704 2.1101 0.526621.8 128.00 132.824.8271 73 73 71 717271.704.738 4.726 0.99740.6686 2.12619 2 0.526621.8132.82 137.654.8371 73 73 71 717271.704.753 4.726 0.99430.6686 2.1263 0.526621.8137.65 142.464.8271 73 74 71 717271.704.736 4.726 0.99790.6689 2.126..AVG=0.9966 -0.25 0.6687 2.1261 0.658520.5 150.00 156.036.0371 78 78 72 727572.455.911 5.910 0.99970.6990 1.95524 2 0.658520.5 156.03 162.056.0171 78 77 73 737572.455.894 5.910 1.00270.6987 1.9523 0.658520.5162.05 168.076.0271 77 73 73 737472.455.913 5.910 0.99950.6971 1.952AVG = 1.0006 0.16 0.6983 1.953AVERAGE DRY GAS METER CALIBRATION FACTOR, Y =0.9991AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko=0.6791dH@= 2.063(1) Vm(std) =K1VmPbar+ (H/13.6) =Net volume of gas sample passed through DGM, corrected to standard conditionsTmK1=17.64oR/in. Hg (English), 0.3858oK/mm Hg (Metric)Tm=Absolute DGM avg. temperature (oR - English,oK - Metric)Pbar(2) Vcr(std) =K' Tamb=Volume of gas sample passed through the critical orifice, corrected to standard conditionsTamb=Absolute ambient temperature (oR - English,oK - Metric)Calibration performed by:J.HaalandK' = Average K' factor from Critical Orifice Calibration(3) Y =Vcr(std) =DGM calibration factorVm(std)METER PART #:ENVIRONMENTAL SUPPLY COMPANYUSING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm(std), and the critical orifice,Vcr(std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.Unit #16Jan 02, 2012 (dgm 10)LEHDER ENVIRONMENTAL SERVICES LIMITEDDRY GAS METER CALIBRATION USING CRITICAL ORIFICES1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.4) Record readings in outlined boxes below, other columns are automatically calculated.INITIAL FINALAVG (Pbar)DATE:2-Jan-12METER SERIAL #:10BAROMETRIC PRESSURE (in Hg):29.8629.8829.87 IF Y VARIATION EXCEEDS 2.00%,- - CRITICAL ORIFICE SET SERIAL #: 1477ORIFICE SHOULD BE RECALIBRATEDK' TESTEDTEMPERATURES °F ELAPSEDFACTOR VACUUMDGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGMH(1) (2) (3)% YORIFICE # RUN # (AVG) (in Hg) INITIAL FINALNET (Vm)INITIAL FINAL INITIAL FINAL AVG(in H2O) Vm(STD) Vcr(STD)Y VARIATION KodH@1 0.433519.284.20 88.113.9172 71 71 71 717171.003.892 3.931 1.01010.7203 1.79416 2 0.433519.188.20 92.113.9171 71 71 71 717171.003.892 3.935 1.01100.7209 1.7843 0.433519.092.30 96.213.9171 71 71 71 717171.003.887 3.935 1.01230.7209 1.784AVG = 1.0111 -0.12 0.7207 1.7871 0.526617.925.90 31.335.4371 72 71 71 717181.555.409 5.462 1.00980.7033 1.87419 2 0.526617.931.60 36.344.7472 71 71 71 717171.554.724 4.775 1.01080.7023 1.8843 0.526617.936.50 41.244.7472 71 71 71 717171.554.722 4.775 1.01120.7023 1.884AVG=1.0106 -0.17 0.7026 1.8811 0.658516.30.90 7.646.7473 72 73 71 717282.306.715 6.818 1.01530.7206 1.79824 2 0.658516.37.80 13.705.9073 73 73 71 717272.305.880 5.966 1.01450.7210 1.7983 0.658516.313.90 19.805.9072 73 73 71 717272.305.877 5.971 1.01600.7216 1.788AVG = 1.0153 0.29 0.7211 1.795AVERAGE DRY GAS METER CALIBRATION FACTOR, Y =1.0123AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko=0.7148dH@= 1.821(1) Vm(std) =K1VmPbar+ (H/13.6) =Net volume of gas sample passed through DGM, corrected to standard conditionsTmK1=17.64oR/in. Hg (English), 0.3858oK/mm Hg (Metric)Tm=Absolute DGM avg. temperature (oR - English,oK - Metric)Pbar(2) Vcr(std) =K' Tamb=Volume of gas sample passed through the critical orifice, corrected to standard conditionsTamb=Absolute ambient temperature (oR - English,oK - Metric)Calibration performed by:J.DenommeK' = Average K' factor from Critical Orifice Calibration(3) Y =Vcr(std) =DGM calibration factorVm(std)METER PART #:ENVIRONMENTAL SUPPLY COMPANYUSING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm(std), and the critical orifice,Vcr(std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.Unit #10Feb.13, 2012 (dgm 16).xlsLEHDER ENVIRONMENTAL SERVICES LIMITEDDRY GAS METER CALIBRATION USING CRITICAL ORIFICES1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.4) Record readings in outlined boxes below, other columns are automatically calculated.INITIAL FINALAVG (Pbar)DATE:Feb. 13/12METER SERIAL #:16BAROMETRIC PRESSURE (in Hg):29.4229.4129.42 IF Y VARIATION EXCEEDS 2.00%,- - CRITICAL ORIFICE SET SERIAL #: 1477ORIFICE SHOULD BE RECALIBRATEDK' TESTEDTEMPERATURES °F ELAPSEDFACTOR VACUUMDGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGMH(1) (2) (3)% YORIFICE # RUN # (AVG) (in Hg) INITIAL FINALNET (Vm)INITIAL FINAL INITIAL FINAL AVG(in H2O) Vm(STD) Vcr(STD)Y VARIATION KodH@1 0.433522.7318.00 321.923.9270 72 72 70 707171.103.843 3.878 1.00910.6833 2.04716 2 0.433522.7322.00 325.923.9269 72 71 70 707171.103.840 3.882 1.01090.6836 2.0353 0.433522.7326.00 329.923.9269 72 71 70 707171.103.845 3.882 1.00960.6836 2.035AVG = 1.0099 0.25 0.6835 2.0391 0.526621.5 330.40 335.174.7769 71 72 70 707171.604.680 4.716 1.00770.6882 2.00619 2 0.526621.5335.30 340.074.7770 72 72 70 707171.604.683 4.711 1.00590.6878 2.0173 0.526621.5340.30 345.084.7869 72 72 70 717171.604.690 4.716 1.00550.6885 2.004..AVG=1.0064 -0.10 0.6882 2.0091 0.658520.1 299.10 305.055.9568 71 71 68 687072.405.869 5.902 1.00570.7022 1.92124 2 0.658520.1 305.30 311.275.9668 72 72 69 697172.405.873 5.902 1.00510.7029 1.9173 0.658520.1311.40 317.355.9569 72 73 69 697172.405.855 5.897 1.00710.7026 1.928AVG = 1.0059 -0.14 0.7026 1.922AVERAGE DRY GAS METER CALIBRATION FACTOR, Y =1.0074AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko=0.6914dH@= 1.990(1) Vm(std) =K1VmPbar+ (H/13.6) =Net volume of gas sample passed through DGM, corrected to standard conditionsTmK1=17.64oR/in. Hg (English), 0.3858oK/mm Hg (Metric)Tm=Absolute DGM avg. temperature (oR - English,oK - Metric)Pbar(2) Vcr(std) =K' Tamb=Volume of gas sample passed through the critical orifice, corrected to standard conditionsTamb=Absolute ambient temperature (oR - English,oK - Metric)Calibration performed by:R. SellerK' = Average K' factor from Critical Orifice Calibration(3) Y =Vcr(std) =DGM calibration factorVm(std)METER PART #:ENVIRONMENTAL SUPPLY COMPANYUSING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm(std), and the critical orifice,Vcr(std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.Unit #16Jan 14, 2012 (dgm 10).xlsLEHDER ENVIRONMENTAL SERVICES LIMITEDDRY GAS METER CALIBRATION USING CRITICAL ORIFICES1) Select three critical orifices to calibrate the dry gas meter which bracket the expected operating range.2) Record barometric pressure before and after calibration procedure.3) Run at maximum attainable vacuum (open coarse valve, close fine valve),for period of 5 minutes minimum for large orifice up to 10 minutes for smallest orifice.4) Record readings in outlined boxes below, other columns are automatically calculated.INITIAL FINALAVG (Pbar)DATE:14-Feb-12METER SERIAL #:10BAROMETRIC PRESSURE (in Hg):29.2729.2629.27 IF Y VARIATION EXCEEDS 2.00%,- - CRITICAL ORIFICE SET SERIAL #: 1477ORIFICE SHOULD BE RECALIBRATEDK' TESTEDTEMPERATURES °F ELAPSEDFACTOR VACUUMDGM READINGS (FT3)AMBIENT DGM INLET DGM OUTLET DGM TIME (MIN)DGMH(1) (2) (3)% YORIFICE # RUN # (AVG) (in Hg) INITIAL FINALNET (Vm)INITIAL FINAL INITIAL FINAL AVG(in H2O) Vm(STD) Vcr(STD)Y VARIATION KodH@1 0.433519.6990.90 994.783.8869 71 71 70 707171.003.782 3.862 1.02110.7149 1.87916 2 0.433519.5994.90 998.783.8870 71 72 70 707171.003.781 3.859 1.02060.7146 1.8893 0.433519.4998.90 1002.783.8871 72 72 70 707171.003.779 3.855 1.02010.7143 1.900AVG = 1.0206 -0.04 0.7146 1.8891 0.526618.23.30 8.024.7270 72 72 70 717171.554.605 4.687 1.01780.6971 1.98319 2 0.526618.28.20 12.924.7270 72 72 71 717271.554.600 4.687 1.01890.6971 1.9813 0.526618.213.10 17.814.7170 72 73 71 717271.554.588 4.687 1.02160.6974 1.981AVG=1.0194 -0.15 0.6972 1.9821 0.658516.518.10 23.975.8771 73 73 71 717272.305.732 5.856 1.02150.7149 1.89024 2 0.658516.524.10 29.975.8770 74 74 71 717372.305.727 5.861 1.02350.7163 1.8803 0.658516.530.10 35.975.8770 74 74 71 717372.305.727 5.861 1.02350.7163 1.880AVG = 1.0228 0.18 0.7158 1.883AVERAGE DRY GAS METER CALIBRATION FACTOR, Y =1.0210AVERAGE DRY GAS METER ORIFICE COEFFICIENT, Ko=0.7092dH@= 1.918(1) Vm(std) =K1VmPbar+ (H/13.6) =Net volume of gas sample passed through DGM, corrected to standard conditionsTmK1=17.64oR/in. Hg (English), 0.3858oK/mm Hg (Metric)Tm=Absolute DGM avg. temperature (oR - English,oK - Metric)Pbar(2) Vcr(std) =K' Tamb=Volume of gas sample passed through the critical orifice, corrected to standard conditionsTamb=Absolute ambient temperature (oR - English,oK - Metric)Calibration performed by:R. SellerK' = Average K' factor from Critical Orifice Calibration(3) Y =Vcr(std) =DGM calibration factorVm(std)METER PART #:ENVIRONMENTAL SUPPLY COMPANYUSING THE CRITICAL ORIFICES AS CALIBRATION STANDARDS:The following equations are used to calculate the standard volumes of air passed through the DGM, Vm(std), and the critical orifice,Vcr(std), and the DGM calibration factor, Y. These equations are automatically calculated in the spreadsheet above.Unit #10

## (M-29)Pitot Calibration for 4A Jan.03, 2012.xls

DATE: 5-Jan-12 Barometric: 29.3 "Hg

LOCATION: Wind Tunnel Temperature: 48 o 

## F
OPERATORS: PB Cp std 

## : 1

Cp s 

## = Cp std 

## X SQRT ( delta P std 

## / delta P s 

## )

Cp s 

## = S-type pitot coefficient Cp std 

## = Standard pitot coefficient

P std 

## = Standard pitot velocity pressure head

P s 

## = S-Type pitot velocity pressure head

PITOT TUBE I.D.: 4A(new pitot lines installed May 6/08)

Nozzle Tunnel Standard Pitot S-Type Pito t S-Type Pito t Deviation

Size Setting Reading Reading Coefficient (delta P std 

## ) (delta P s 

## ) Cp s 

## ICp s 

## - Cp av g 

## I

inches Hz "H 2 

## O " H 2 

## O

0.1875 49.2 0.374 0.566 0.813 0.0075

51.8 0.416 0.632 0.811 0.0091

54.5 0.464 0.676 0.828 0.0081

56.5 0.496 0.734 0.822 0.0016

59.3 0.542 0.792 0.827 0.0069

Average 0.820 0.0066

0.3125 30.2 0.144 0.220 0.809 0.0042

32.7 0.162 0.248 0.808 0.0050

34.8 0.186 0.280 0.815 0.0018

36.7 0.206 0.310 0.815 0.0019

39.1 0.236 0.352 0.819 0.0056

Average 0.813 0.0037

0.5000 12.3 0.024 0.036 0.816 0.0052

14.4 0.034 0.050 0.825 0.0030

17.0 0.046 0.068 0.822 0.0008

19.5 0.062 0.092 0.821 0.0007

21.8 0.076 0.112 0.824 0.0021

Average 0.822 0.0024

The pitot tube must have an average deviation ( σ ) value of ≤ 0.01. The above calibration values were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was manufactured by Dwyer Instuments according to ASME specifications. 

# LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

4A(Jan.05-2012)

# (M-0061)Pitot Calibration for 5W-1 Jan.03, 2012.xls

DATE: 10-Jan-12 Barometric: 29.44 "Hg

LOCATION: Wind Tunnel Temperature: 50 o 

# F
OPERATORS: PB Cp std 

# : 1

Cp s 

# = Cp std 

# X SQRT ( delta P std 

# / delta P s 

# )

Cp s 

# = S-type pitot coefficient Cp std 

# = Standard pitot coefficient

P std 

# = Standard pitot velocity pressure head

P s 

# = S-Type pitot velocity pressure head

PITOT TUBE I.D.: 5W-1 ***(Calibrated in Reverse for OC Delmar project)***

Nozzle Tunnel Standard Pitot S-Type Pito t S-Type Pito t Deviation

Size Setting Reading Reading Coefficient (delta P std 

# ) (delta P s 

# ) Cp s 

# ICp s 

# - Cp av g 

# I

inches Hz "H 2 

# O " H 2 

# O

0.356 30.2 0.140 0.230 0.780 0.0017

32.7 0.164 0.274 0.774 0.0049

34.8 0.184 0.308 0.773 0.0056

36.7 0.210 0.344 0.781 0.0028

39.1 0.240 0.390 0.784 0.0060

Average 0.779 0.0042

The pitot tube must have an average deviation ( σ ) value of ≤ 0.01. The above calibration values were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was manufactured by Dwyer Instuments according to ASME specifications. 

# LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

5W-1(Jan.10-2012)

## (M-29)Pitot Calibration for 4D Jan.03, 2012.xls

DATE: 5-Jan-12 Barometric: 29.36 "Hg

LOCATION: Wind Tunnel Temperature: 48 o 

## F
OPERATORS: PB Cp std 

## : 1

Cp s 

## = Cp std 

## X SQRT ( delta P std 

## / delta P s 

## )

Cp s 

## = S-type pitot coefficient Cp std 

## = Standard pitot coefficient

P std 

## = Standard pitot velocity pressure head

P s 

## = S-Type pitot velocity pressure head

PITOT TUBE I.D.: 4D

Nozzle Tunnel Standard Pitot S-Type Pito t S-Type Pito t Deviation

Size Setting Reading Reading Coefficient (delta P std 

## ) (delta P s 

## ) Cp s 

## ICp s 

## - Cp av g 

## I

inches Hz "H 2 

## O " H 2 

## O

0.1875 49.2 0.374 0.554 0.822 0.0097

51.8 0.414 0.608 0.825 0.0062

54.5 0.460 0.660 0.835 0.0035

56.5 0.500 0.710 0.839 0.0078

59.3 0.548 0.784 0.836 0.0047

Average 0.831 0.0064

0.3125 30.2 0.138 0.204 0.822 0.0000

32.7 0.164 0.242 0.823 0.0007

34.8 0.186 0.278 0.818 0.0045

36.7 0.208 0.308 0.822 0.0007

39.1 0.238 0.348 0.827 0.0045

Average 0.822 0.0021

0.5000 12.3 0.024 0.036 0.816 0.0036

14.4 0.034 0.050 0.825 0.0046

17.0 0.046 0.068 0.822 0.0024

19.5 0.060 0.090 0.816 0.0036

21.8 0.074 0.110 0.820 0.0001

Average 0.820 0.0028

The pitot tube must have an average deviation ( σ ) value of ≤ 0.01. The above calibration values were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was manufactured by Dwyer Instuments according to ASME specifications. 

# LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

4D(Jan.05-2012)

# (M-0061)Pitot Calibration for 5W-2 Jan.03, 2012.xls

DATE: 10-Jan-12 Barometric: 29.44 "Hg

LOCATION: Wind Tunnel Temperature: 50 o 

# F
OPERATORS: PB Cp std 

# : 1

Cp s 

# = Cp std 

# X SQRT ( delta P std 

# / delta P s 

# )

Cp s 

# = S-type pitot coefficient Cp std 

# = Standard pitot coefficient

P std 

# = Standard pitot velocity pressure head

P s 

# = S-Type pitot velocity pressure head

PITOT TUBE I.D.: 5W-2 ***(Calibrated in Reverse for OC Delmar project)***

Nozzle Tunnel Standard Pitot S-Type Pito t S-Type Pito t Deviation

Size Setting Reading Reading Coefficient (delta P std 

# ) (delta P s 

# ) Cp s 

# ICp s 

# - Cp av g 

# I

inches Hz "H 2 

# O " H 2 

# O

0.356 30.2 0.140 0.234 0.773 0.0079

32.7 0.166 0.268 0.787 0.0057

34.8 0.188 0.304 0.786 0.0050

36.7 0.210 0.344 0.781 0.0000

39.1 0.234 0.386 0.779 0.0028

Average 0.781 0.0043

The pitot tube must have an average deviation ( σ ) value of ≤ 0.01. The above calibration values were obtained by calibrating the s-type pitot against a standard pitot tube. The standard pitot tube used was series 160, with an assigned calibration factor of "1". The standard pitot tube was manufactured by Dwyer Instuments according to ASME specifications. 

# LEHDER ENVIRONMENTAL SERVICES LIMITED

PITOT TUBE CALIBRATION

5W-2(Jan.10-2012)LEHDER DGM TC Calibrations - 2012LEHDER Environmental Services LimitedEquipment CalibrationsControl Unit Dry Gas Meter ThermocouplesReference Thermometer ID:Specification for UseAmbient Air:Fisherbrand ANSI/SAMA Z236.1-1983 (-30 ̊F - 120 ̊F)Variance less than:1.5%Hot Water:Fisherbrand ANSI/SAMA Z236.1-1983 (0 ̊F - 230 ̊F)Ice Water:Fisherbrand ANSI/SAMA Z236.1-1983 (-30 ̊F - 120 ̊F)% Variance ={ABS [(DGM TC Reading+460) - (Reference Reading+460)] x 100%Hot Oil:Fisherbrand ANSI/SAMA Z236.1-1983 (25 ̊F - 750 ̊F)Tech.DateUnitDGMNameD-M-Y#In/OutDGM T/CReferenceDGM T/CReferenceDGM T/CReference% VariancePass/Fail% VariancePass/Fail% VariancePass/FailJ.Haaland12-Dec-116IN697134332122110.38Pass0.20Pass0.15PassJ.Haaland12-Dec-116Out697133332142110.38Pass0.00Pass0.45PassJ.Haaland12-Dec-117IN727233332122110.00Pass0.00Pass0.15PassJ.Haaland12-Dec-117Out727232332092110.00Pass0.20Pass0.30PassJ.Haaland12-Dec-119IN717132332102120.00Pass0.20Pass0.30PassJ.Haaland12-Dec-119Out717132332112120.00Pass0.20Pass0.15PassJ. Denomme2-Jan-1210IN747334341911880.19Pass0.00Pass0.46PassJ. Denomme2-Jan-1210Out727336341931900.19Pass0.40Pass0.46PassJ. Denomme2-Jan-1211IN717135342012040.00Pass0.20Pass0.45PassJ. Denomme2-Jan-1211Out727135342032020.19Pass0.20Pass0.15PassJ.Haaland12-Dec-1114IN697132332112120.38Pass0.20Pass0.15PassJ.Haaland12-Dec-1114Out697132332112120.38Pass0.20Pass0.15PassJ.Haaland12-Dec-1115IN696933332042050.00Pass0.00Pass0.15PassJ.Haaland12-Dec-1115Out707034332062050.00Pass0.20Pass0.15PassJ.Haaland12-Dec-1116IN707134332052080.19Pass0.20Pass0.45PassJ.Haaland12-Dec-1116Out707133332062080.19Pass0.00Pass0.30PassJ.Haaland14-Dec-11VOST #1Single697131332182100.38Pass0.41Pass1.19PassP.Baker8-Mar-11VOST #2Single697131332102120.38Pass0.41Pass0.30PassJ.Haaland14-Dec-11M13B#1Single707132332132110.19Pass0.20Pass0.30PassJ.Haaland14-Dec-11M13B#2Single707132332132110.19Pass0.20Pass0.30PassLast Entry:Name:Mike DenommeDate:6-Jan-12(Reference Reading + 460)MeasurementsCalculations / StatusIceHot WaterAmbient ( ̊F)Ice Water ( ̊F)Hot Water ( ̊F)AmbientJan 2012Probes & Outlet Stems Thermocouple Cals 2012Thermometer ID:Calibrated By:Thermometer ID:Date:Thermometer ID:Thermometer ID:TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF)Probe 2C 35 360.20%70 690.19%203 2070.60%500 5000.00%Probe 2D 37 370.00%70 690.19%198 2020.60%481 4850.42%Probe 2E 36 370.20%71 700.19%206 2110.75%505 5060.10%Probe 2X-Flex 36 360.00%71 700.09%206 2100.60%492 4950.31%Probe 3A (Flex) 33 330.00%71 700.19%205 2080.45%505 5050.00%Probe 3B 33 330.00%69 690.00%210 2110.15%490 4910.11%Probe 3C 33 330.10%71 700.19%212 2110.15%500 4980.21%Probe 3F 33 340.20%70 690.19%212 2120.00%490 4910.11%Probe 3G 33 330.00%71 700.09%195 1980.46%490 4910.11%Probe 3H-D 33 340.20%71 710.00%214 2130.15%510 5080.21%Probe 4A 33 330.00%69 680.19%210 2080.30%515 5140.10%Probe 4D 33 330.00%69 700.19%211 2150.59%520 5250.51%Probe 5C33340.20%70700.09%2112130.30%510 5130.31%Probe 5D33330.00%69690.00%210 2140.59%521 5210.00%Probe 5G34340.00%69690.00%212 2120.00%520 5200.00%Probe 5H33330.00%70680.28%202 2040.30%520 5210.10%Probe 5J33330.00%70690.09%211 2140.45%495 4950.00%Probe 5K33330.00%70700.00%210 2150.74%474 4710.32%Probe 7B33340.20%69680.19%209 2110.30%515 5120.31%Probe 7C34340.00%70680.28%206 2090.45%509 5080.10%Probe 7D0.00%0.00%0.00%0.00%Probe 7E35340.20%69670.38%210 2130.45%543 5420.10%Probe 7F34340.10%69680.19%211 2120.15%498 4940.42%Probe 8A34340.10%70690.19%210 2140.59%519 5190.00%Probe 9A34350.20%67660.19%210 2140.59%530 5300.00%Probe 10A35350.00%68660.38%210 2160.89%5255260.10%Probe 10B33340.20%69650.67%210 2120.30%500 5000.00%Probe 10C34340.00%69660.48%210 2140.59%520 5230.31%Probe 14A0.00%0.00%0.00%0.00%PT 0133330.00%68670.09%211 2140.45%477 4800.32%PT 0233340.20%70690.19%210 2140.59%540 5400.00%PT 0832330.20%70690.09%212 2140.30%510 5120.21%PT 0932340.40%69640.95%210 2150.74%484 4850.11%PT 1034330.20%70690.19%212 2130.15%510 5100.00%PT S433330.00%70690.09%210 2150.74%520 5200.00%AmbientICE BATHHOT OIL% DIFFERENCE(Absolute)% DIFFERENCE(Absolute)PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEETThermocouple I.D.R.S./K.H.January 4, 2012% DIFFERENCE(Absolute)For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0oF - 230oF)For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25oF - 750oF)Boiling WaterFor Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)% DIFFERENCE(Absolute)Probes & Outlet Stems Thermocouple Cals 2012Thermometer ID:Calibrated By:Thermometer ID:Date:Thermometer ID:Thermometer ID:TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF)AmbientICE BATHHOT OIL% DIFFERENCE(Absolute)% DIFFERENCE(Absolute)PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEETThermocouple I.D.R.S./K.H.January 4, 2012% DIFFERENCE(Absolute)For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0oF - 230oF)For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25oF - 750oF)Boiling WaterFor Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)% DIFFERENCE(Absolute)PT S536360.00%71710.00%213 2080.75%528 5270.10%PT S633320.20%70690.19%210 2150.74%500 5050.52%PT S736350.20%71710.00%214 2100.60%548 5500.20%PT 7436350.20%71710.00%213 2080.75%521 5170.41%Outlet Stem 134340.00%71700.09%206 2070.15%0.00%Outlet Stem 234350.20%70710.19%208 2100.30%0.00%Outlet Stem 433350.40%69680.19%210 2040.90%0.00%Outlet Stem 534350.20%70680.38%204 2040.00%0.00%Outlet Stem 635360.20%70700.00%209 2100.15%0.00%Outlet Stem 733340.20%70680.38%210 2110.15%0.00%Outlet Stem 834340.00%70690.19%208 2080.00%0.00%Outlet Stem 1036360.00%69680.19%209 2100.15%0.00%Outlet Stem 1133340.20%70680.38%210 2090.15%0.00%Outlet Stem 1234340.00%68690.19%208 2070.15%0.00%Outlet Stem 1334340.00%71710.09%211 2120.15%0.00%Outlet Stem 1435350.00%67690.38%210 2100.00%0.00%Outlet Stem 1534340.00%70670.57%210 2100.00%0.00%Outlet Stem 1635350.00%71700.19%210 2100.00%0.00%Outlet Stem 1733340.20%69670.38%210 2100.00%0.00%Pitot X-235370.50%68650.57%209 2150.89%522 5200.20%Probes & Outlet Stems Thermocouple Cals.xlsThermometer ID:Calibrated By:Thermometer ID:Date:Thermometer ID:Thermometer ID:TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF)Probe 2C 34 340.00%72 720.00%203 2020.15%479 4750.43%Probe 2D 36 360.00%75 750.00%204 1990.76%482 4770.53%Probe 2E 34 340.00%71 710.00%207 2020.76%477 4770.00%Probe 3A (Flex) 35 350.00%72 710.19%211 2100.15%419 4180.11%Probe 3B 38 350.61%75 750.00%210 2100.00%471 4690.22%Probe 3C 36 350.20%75 750.00%214 2061.20%466 4660.00%Probe 3F 34 330.20%72 730.19%197 1970.00%488 4860.21%Probe 3G 35 350.00%75 750.00%207 2080.15%469 4650.43%Probe 3H-D 35 350.00%71 710.00%210 2100.00%418 4180.00%Probe 4A 33 330.00%71 730.38%205 2010.61%491 4850.63%Probe 4D 33 330.00%73 730.00%207 2020.76%491 4850.63%Probe 5C 33 340.20%71 710.00%210 2100.00%419 4180.11%Probe 5D34340.00%70720.38%2082060.30%464 4650.11%Probe 5G34340.00%71710.00%210 2100.00%418 4180.00%Probe 5H37360.20%70720.38%207 2060.15%465 4650.00%Probe 5J35350.00%71710.00%203 1990.61%478 4740.43%Probe 5K35340.20%71710.00%214 2120.30%417 4180.11%Probe 7B36350.20%71710.00%210 2100.00%413 4150.23%Probe 7C35350.00%73730.00%206 2040.30%485 4850.00%Probe 7D35350.00%73730.00%207 2040.45%484 4840.00%Probe 7E36360.00%72730.19%206 2030.45%490 4860.42%Probe 7F36360.00%72730.19%205 2030.30%485 4860.11%Probe 8A32340.40%65680.57%211 2100.15%490 4900.00%Probe 9A33330.00%69690.00%193 1890.62%478 4810.32%Probe 10A35340.20%71710.00%214 2120.30%4174150.23%Probe 10B34340.00%69690.00%1861840.31%479 4790.00%Probe 10C34350.20%71710.00%210 2100.00%413 4150.23%Probe 14A35350.00%71710.00%213 2120.15%415 4150.00%PT 0132340.40%70710.19%203 2020.15%439 4360.33%PT 0233340.20%71710.00%212 2100.30%418 4180.00%PT 0333340.20%67680.19%212 2120.00%490 4900.00%PT 0833350.40%71710.00%210 2080.30%433 4300.34%PT 0934340.00%71710.00%211 2100.15%419 4180.11%T 1033340.20%71710.00%210 2090.15%423 4250.23%PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEETThermocouple I.D.R.S./J.H./P.B./B.K.Jan. 2011% DIFFERENCE(Absolute)For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0oF - 230oF)% DIFFERENCE(Absolute)For Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)AmbientICE BATHHOT OIL% DIFFERENCE(Absolute)For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25oF - 750oF)Boiling Water% DIFFERENCE(Absolute)Probes & Outlet Stems Thermocouple Cals.xlsThermometer ID:Calibrated By:Thermometer ID:Date:Thermometer ID:Thermometer ID:TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF) TC (oF) REF. (oF)PROBE & OUTLET STEMS THERMOCOUPLE CALIBRATION SHEETThermocouple I.D.R.S./J.H./P.B./B.K.Jan. 2011% DIFFERENCE(Absolute)For Ambient Air - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)For Hot Water - Fisherbrand ANSI/SAMA Z236.1-1983 (0oF - 230oF)% DIFFERENCE(Absolute)For Ice Water - Fisherbrand ANSI/SAMA Z236.1-1983 (-30oF - 120oF)AmbientICE BATHHOT OIL% DIFFERENCE(Absolute)For Hot Oil - Fisherbrand ANSI/SAMA Z236.1-1983 (25oF - 750oF)Boiling Water% DIFFERENCE(Absolute)PT S433330.00%69700.19%203 1990.61%479 4770.21%PT S533330.00%71710.00%211 2100.15%418 4180.00%PT S632340.40%66680.38%214 2120.30%496 4920.42%PT S733340.20%71710.00%211 2100.15%418 4180.00%PT 7435350.00%71710.00%214 2100.60%427 4200.80%Outlet Stem 134330.20%71710.00%0.00%0.00%Outlet Stem 234330.20%71710.00%0.00%0.00%Outlet Stem 433330.00%71710.00%0.00%0.00%Outlet Stem 5 Out of Service33330.00%71700.19%0.00%0.00%Outlet Stem 633330.00%72710.19%0.00%0.00%Outlet Stem 734330.20%71700.19%0.00%0.00%Outlet Stem 834330.20%72710.19%0.00%0.00%Outlet Stem 1033330.00%72710.19%0.00%0.00%Outlet Stem 1135350.00%71710.00%0.00%0.00%Outlet Stem 1233330.00%71700.19%0.00%0.00%Outlet Stem 1335350.00%72720.00%0.00%0.00%Outlet Stem 1433330.00%71700.19%Outlet Stem 1533330.00%71700.19%

### Unit 11_Jan 2.xls



## Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 2-Jan-12 Operator : JD
Control Unit : Unit 11

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Settin g Readou t Differenc e Simulator Settin g Readou t Differenc e

o 

### F o 

### F % o 

### F o 

### F %

0 0 0.000 0 -1 0.217

50 48 0.392 50 47 0.588

100 98 0.357 100 97 0.536

150 149 0.164 150 148 0.328

200 199 0.152 Average: 0.417

250 250 0.000

300 300 0.000

350 348 0.247 Readout ID: 5-Stack

400 398 0.233

450 446 0.440 Simulator Settin g Readou t Differenc e
500 497 0.313 o 

### F o 

### F %

550 548 0.198 0 -1 0.217

600 598 0.189 50 47 0.588

650 650 0.000 100 97 0.536

700 700 0.000 150 148 0.328

750 750 0.000 200 198 0.303

800 799 0.079 250 249 0.141

850 850 0.000 300 299 0.132

900 899 0.074 350 347 0.370

950 950 0.000 400 397 0.349

1000 1000 0.000 450 446 0.440 Average: 0.135 500 496 0.417

550 546 0.396

600 597 0.283
Readout ID: 2-Probe 650 649 0.090

700 699 0.086
Simulator Settin g Readou t Differenc e 750 749 0.083

o 

### F o 

### F % 800 799 0.079

0 1 0.217 850 849 0.076

50 49 0.196 900 899 0.074

100 99 0.179 950 949 0.071

150 150 0.000 1000 999 0.068

200 200 0.000 Average: 0.244

250 250 0.000

300 301 0.132

350 348 0.247 Readout ID: 6-DGM in

400 399 0.116

450 447 0.330 Simulator Settin g Readou t Differenc e
500 498 0.208 o 

### F o 

### F % Average: 0.148 0 0 0.000

50 48 0.392

100 98 0.357
Readout ID: 3-Filter 150 150 0.000

200 200 0.000
Simulator Settin g Readou t Differenc e 0.150

o 

### F o 

### F %

0 0 0.000

50 48 0.392 Readout ID: 7-DGM out

100 98 0.357

150 150 0.000 Simulator Settin g Readou t Differenc e
200 199 0.152 o 

### F o 

### F %

250 250 0.000 0 0 0.000

300 300 0.000 50 48 0.392

350 348 0.247 100 98 0.357

400 398 0.233 150 149 0.164

450 447 0.330 200 200 0.000

500 497 0.313 Average: 0.183 Average: 0.184

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE
IF THEY ARE NOT THE READOUT MUST BE REPLACED

.

Temperature Readout ID: Unit 11 Temperature Simulator ID: Omega Model: CL 300

Unit

### Unit 15_Jan 3.xls



# LEHDER Environmental Services Limited
Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 3-Jan-12 Operator: JD
Control Unit: Unit 15

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference

o 

### F o 

### F % o 

### F o 

### F %

0 -1 0.217 0 -1 0.217

50 46 0.784 50 46 0.784

100 96 0.714 100 96 0.714

150 147 0.492 150 147 0.492

200 198 0.303 Average: 0.552

250 248 0.282

300 298 0.263

350 346 0.494 Readout ID: 5-Stack

400 396 0.465

450 445 0.549 Simulator Setting Readout Difference

500 496 0.417 o 

### F o 

### F %

550 546 0.396 0 -1 0.217

600 597 0.283 50 46 0.784

650 648 0.180 100 96 0.714

700 699 0.086 150 148 0.328

750 749 0.083 200 198 0.303

800 798 0.159 250 248 0.282

850 848 0.153 300 298 0.263

900 898 0.147 350 346 0.494

950 948 0.142 400 396 0.465

1000 999 0.068 450 445 0.549 Average: 0.318 500 496 0.417

550 546 0.396

600 597 0.283

Readout ID: 2-Probe 650 648 0.180

700 699 0.086 Simulator Setting Readout Difference 750 749 0.083

o 

### F o 

### F % 800 798 0.159

0 0 0.000 850 848 0.153

50 47 0.588 900 898 0.147

100 97 0.536 950 948 0.142

150 148 0.328 1000 999 0.068

200 198 0.303 Average: 0.310

250 249 0.141

300 299 0.132

350 347 0.370 Readout ID: 6-DGM in

400 397 0.349

450 446 0.440 Simulator Setting Readout Difference

500 496 0.417 o 

### F o 

### F % Average: 0.328 0 0 0.000

50 47 0.588

100 96 0.714

Readout ID: 3-Filter 150 148 0.328

200 198 0.303 Simulator Setting Readout Difference 0.387

o 

### F o 

### F %

0 0 0.000

50 47 0.588 Readout ID: 7-DGM out

100 97 0.536

150 148 0.328 Simulator Setting Readout Difference

200 198 0.303 o 

### F o 

### F %

250 249 0.141 0 0 0.000

300 299 0.132 50 47 0.588

350 346 0.494 100 97 0.536

400 397 0.349 150 148 0.328

450 446 0.440 200 198 0.303

500 497 0.313 Average: 0.351 Average: 0.329

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE.
IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 15 Temperature Simulator ID: Omega Model: CL 300

Unit

### Unit 14_Jan 3.xls

Control Unit Temperature Readout Calibratio n

Location : LEHDER Laboratory

Date: 3-Jan-12 Operator : JD
Control Unit : Unit 14

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Settin g Readou t Differenc e Simulator Settin g Readou t Differenc e

o 

### F o 

### F % o 

### F o 

### F %

0 -1 0.217 0 -1 0.217

50 46 0.784 50 46 0.784

100 96 0.714 100 96 0.714

150 148 0.328 150 148 0.328

200 198 0.303 Average: 0.511

250 249 0.141

300 299 0.132

350 347 0.370 Readout ID: 5-Stack

400 397 0.349

450 446 0.440 Simulator Settin g Readou t Differenc e
500 497 0.313 o 

### F o 

### F %

550 548 0.198 0 -1 0.217

600 599 0.094 50 46 0.784

650 650 0.000 100 96 0.714

700 701 0.086 150 148 0.328

750 751 0.083 200 198 0.303

800 800 0.000 250 248 0.282

850 851 0.076 300 299 0.132

900 901 0.074 350 347 0.370

950 951 0.071 400 397 0.349

1000 1001 0.068 450 446 0.440 Average: 0.231 500 497 0.313

550 548 0.198

600 599 0.094
Readout ID: 2-Probe 650 650 0.000

700 701 0.086
Simulator Settin g Readou t Differenc e 750 750 0.000

o 

### F o 

### F % 800 800 0.000

0 -1 0.217 850 851 0.076

50 47 0.588 900 901 0.074

100 97 0.536 950 951 0.071

150 148 0.328 1000 1001 0.068

200 199 0.152 Average: 0.233

250 249 0.141

300 300 0.000

350 348 0.247 Readout ID: 6-DGM in

400 398 0.233

450 447 0.330 Simulator Settin g Readou t Differenc e
500 498 0.208 o 

### F o 

### F % Average: 0.271 0 -1 0.217

50 46 0.784

100 96 0.714
Readout ID: 3-Filter 150 148 0.328

200 198 0.303
Simulator Settin g Readou t Differenc e 0.469

o 

### F o 

### F %

0 -1 0.217

50 47 0.588 Readout ID: 7-DGM out

100 97 0.536

150 149 0.164 Simulator Settin g Readou t Differenc e
200 199 0.152 o 

### F o 

### F %

250 249 0.141 0 -1 0.217

300 300 0.000 50 46 0.784

350 348 0.247 100 96 0.714

400 398 0.233 150 148 0.328

450 447 0.330 200 198 0.303

500 498 0.208 Average: 0.469 Average: 0.256

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE
IF THEY ARE NOT THE READOUT MUST BE REPLACED

.

Temperature Readout ID: Unit 14 Temperature Simulator ID: Omega Model: CL 300

Unit

### Unit 7_Jan 3.xls



# LEHDER Environmental Services Limited
Temperature Readout Calibration

Location : LEHDER Laboratory

Date: 3-Jan-12 Operator: JD
Control Unit: Unit 7

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Setting Readout Difference Simulator Setting Readout Difference

o 

### F o 

### F % o 

### F o 

### F %

0 -3 0.652 0 -3 0.652

50 48 0.392 50 48 0.392

100 98 0.357 100 98 0.357

150 149 0.164 150 149 0.164

200 198 0.303 Average: 0.391

250 248 0.282

300 299 0.132

350 347 0.370 Readout ID: 5-Stack

400 398 0.233

450 447 0.330 Simulator Setting Readout Difference

500 498 0.208 o 

### F o 

### F %

550 548 0.198 0 -3 0.652

600 598 0.189 50 48 0.392

650 649 0.090 100 98 0.357

700 699 0.086 150 149 0.164

750 748 0.165 200 198 0.303

800 799 0.079 250 248 0.282

850 849 0.076 300 298 0.263

900 899 0.074 350 346 0.494

950 949 0.071 400 398 0.233

1000 999 0.068 450 447 0.330 Average: 0.215 500 498 0.208

550 548 0.198

600 598 0.189

Readout ID: 2-Probe 650 648 0.180

700 699 0.086 Simulator Setting Readout Difference 750 748 0.165

o 

### F o 

### F % 800 799 0.079

0 -1 0.217 850 849 0.076

50 49 0.196 900 899 0.074

100 99 0.179 950 949 0.071

150 150 0.000 1000 999 0.068

200 200 0.000 Average: 0.232

250 249 0.141

300 301 0.132

350 348 0.247 Readout ID: 6-DGM in

400 400 0.000

450 449 0.110 Simulator Setting Readout Difference

500 500 0.000 o 

### F o 

### F % Average: 0.111 0 -3 0.652

50 48 0.392

100 98 0.357

Readout ID: 3-Filter 150 149 0.164

200 198 0.303 Simulator Setting Readout Difference 0.374

o 

### F o 

### F %

0 -1 0.217

50 49 0.196 Readout ID: 7-DGM out

100 99 0.179

150 150 0.000 Simulator Setting Readout Difference

200 200 0.000 o 

### F o 

### F %

250 249 0.141 0 -3 0.652

300 301 0.132 50 48 0.392

350 348 0.247 100 98 0.357

400 400 0.000 150 149 0.164

450 449 0.110 200 198 0.303

500 500 0.000 Average: 0.374 Average: 0.111

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE.
IF THEY ARE NOT THE READOUT MUST BE REPLACED.

Temperature Readout ID: Unit 7 Temperature Simulator ID: Omega Model: CL 300

Unit

### Unit 16_Jan 3.xls



# LEHDER Environmental Services Limited
Control Unit Temperature Readout Calibratio n

Location : LEHDER Laboratory

Date: 3-Jan-12 Operator : JD
Control Unit : Unit 16

Readout ID: 1-Stack Readout ID: 4-Impinger Outlet

Simulator Settin g Readou t Differenc e Simulator Settin g Readou t Differenc e

o 

### F o 

### F % o 

### F o 

### F %

0 -2 0.435 0 -1 0.217

50 46 0.784 50 46 0.784

100 96 0.714 100 96 0.714

150 148 0.328 150 148 0.328

200 197 0.455 Average: 0.511

250 248 0.282

300 298 0.263

350 346 0.494 Readout ID: 5-Stack

400 396 0.465

450 445 0.549 Simulator Settin g Readou t Differenc e
500 496 0.417 o 

### F o 

### F %

550 546 0.396 0 -1 0.217

600 597 0.283 50 46 0.784

650 649 0.090 100 96 0.714

700 699 0.086 150 148 0.328

750 749 0.083 200 198 0.303

800 798 0.159 250 248 0.282

850 849 0.076 300 298 0.263

900 898 0.147 350 346 0.494

950 949 0.071 400 397 0.349

1000 999 0.068 450 445 0.549 Average: 0.316 500 496 0.417

550 546 0.396

600 598 0.189
Readout ID: 2-Probe 650 649 0.090

700 699 0.086
Simulator Settin g Readou t Differenc e 750 749 0.083

o 

### F o 

### F % 800 799 0.079

0 0 0.000 850 849 0.076

50 47 0.588 900 899 0.074

100 97 0.536 950 949 0.071

150 148 0.328 1000 999 0.068

200 198 0.303 Average: 0.282

250 248 0.282

300 299 0.132

350 347 0.370 Readout ID: 6-DGM in

400 398 0.233

450 446 0.440 Simulator Settin g Readou t Differenc e
500 497 0.313 o 

### F o 

### F % Average: 0.320 0 -1 0.217

50 47 0.588

100 96 0.714
Readout ID: 3-Filter 150 148 0.328

200 198 0.303
Simulator Settin g Readou t Differenc e 0.430

o 

### F o 

### F %

0 0 0.000

50 47 0.588 Readout ID: 7-DGM out

100 97 0.536

150 148 0.328 Simulator Settin g Readou t Differenc e
200 198 0.303 o 

### F o 

### F %

250 248 0.282 0 -1 0.217

300 299 0.132 50 47 0.588

350 347 0.370 100 96 0.714

400 398 0.233 150 148 0.328

450 446 0.440 200 198 0.303

500 497 0.313 Average: 0.430 Average: 0.320

ALL READINGS MUST BE WITHIN 1.5% OF THE ABSOLUTE TEMPERATURE
IF THEY ARE NOT THE READOUT MUST BE REPLACED

.

Temperature Readout ID: Unit 16 Temperature Simulator ID: Omega Model: CL 300

Unit

## 123987 Nozzle Calibration Measurements.xls



# LEHDER Environmental Services Limited

Nozzle Calibration

Project No.: 123987

Date: Jan.24, 2012
Calibrator: P. Baker

ID 1 2 3 Average (inches)

DM1(M-0061) 0.3650 0.3655 0.3640 0.3648 one piece nozzle/probe liner

DM1(M-29) 0.3900 0.3900 0.3890 0.3897



# DM2(M-0061) 0.3590 0.3595 0.3600 0.3595 one piece nozzle/probe liner



# DM2(M-29) 0.3855 0.3825 0.3820 0.3833



# NOTE:

1. Measure inside diameter of nozzle at 3 different diameters - to the nearest 0.001 inch. 2. Obtain the average diameter. 3. The difference between high and low readings cannot exceed 0.004 inches. 1 

### 2

3



## Glass Nozzles

### 02-16-12 barometer cal.xls



## Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Black % Difference

Barometer From Actual Compensated

°C °F kPa "Hg "Hg

Feb 16/12 10:00 3 37 0.657 101.38 29.94 29.28 29.27 0.04%

11:00 3 37 0.657 101.30 29.91 29.26 29.25 0.02%

12:00 4 39 0.655 101.30 29.91 29.26 29.25 0.03%

13:00 5 41 0.652 101.29 29.91 29.26 29.25 0.03%

AVG. 0.03%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron 

## BAROMETER CALIBRATION

"Hg % 

## 590 † 

## Feb 16,2012

BK

Temperature

** Correction Factor obtained from National Imagery and Mapping Agency's web page * Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page)

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page)CorrectionFactor**


## Date Time Actual Barometric***

@ Sea Level

Brunton-black (newdigital)

### 02-16-12 barometer cal.xls



## Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Blue % Difference

Barometer From Actual Compensated

°C °F kPa "Hg "Hg

Feb 16/12 10:00 3 37 0.657 101.38 29.94 29.28 29.27 0.04%

11:00 3 37 0.657 101.30 29.91 29.26 29.28 0.08%

12:00 4 39 0.655 101.30 29.91 29.26 29.28 0.07%

13:00 5 41 0.652 101.29 29.91 29.26 29.27 0.04%

AVG. 0.06%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron ** Correction Factor obtained from National Imagery and Mapping Agency's web page * Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page)

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page)CorrectionFactor**


## Date Time Actual Barometric***

@ Sea Level 

## BAROMETER CALIBRATION

"Hg % 

## 590 † 

## Feb 16,2012

BK

Temperature

Brunton-blue (digital)

### 02-18-11 barometer cal 1.xls



## Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Black % Difference

Barometer From Actual Compensated

°C °F kPa "Hg "Hg

18-Feb-11 9:00 8 46 0.646 100.81 29.77 29.12 29.12 0.01%

18-Feb-11 10:00 8 46 0.646 100.87 29.79 29.14 29.13 0.04%

18-Feb-11 11:00 8 46 0.646 100.91 29.80 29.15 29.15 0.01%

18-Feb-11 12:00 8 46 0.646 100.91 29.80 29.15 29.16 0.02%

AVG. 0.02%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron ** Correction Factor obtained from National Imagery and Mapping Agency's web page * Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page)

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page)CorrectionFactor**


## Date Time Actual Barometric***

@ Sea Level 

## BAROMETER CALIBRATION

"Hg % 

## 590 † 

## 18-Feb-11

N. Abma

Temperature

Brunton-black (newdigital)

### 02-18-11 barometer cal 1.xls



## Calibration Date:

Calibrator:

Height Above Sea Level (ft):

Brunton Blue % Difference

Barometer From Actual Compensated

°C °F kPa "Hg "Hg

18-Feb-11 9:00 8 46 0.646 100.81 29.77 29.12 29.06 0.22%

18-Feb-11 10:00 8 46 0.646 100.87 29.79 29.14 29.10 0.14%

18-Feb-11 11:00 8 46 0.646 100.91 29.80 29.15 29.12 0.11%

18-Feb-11 12:00 8 46 0.646 100.91 29.80 29.15 29.13 0.08%

AVG. 0.14%

† Elevation Approximated based on benchmark elevation of 576.8 ft of Lake Huron 

## BAROMETER CALIBRATION

"Hg % 

## 590 † 

## 18-Feb-11

N. Abma

Temperature

** Correction Factor obtained from National Imagery and Mapping Agency's web page * Outdoor Temperature measured at Sarnia Airport (as shown on Environment Canada's Web Page)

*** Actual barometric obtained from the most recent barometric pressure measured at the Sarnia Airport (as shown on Environment Canada's Web Page)CorrectionFactor**


## Date Time Actual Barometric***

@ Sea Level

Brunton-blue (digital)

# Appendix D

Field Data Sheets

D.1: Field Run Sheets D.2: Sample Recovery Data Sheets D.3: Cyclonic Flow Data Sheet

# Appendix D.1

Field Run Sheets

# Appendix D.2

Sample Recovery Data Sheets

# Appendix D.3

Cyclonic Flow Data Sheet

# Appendix E

Sample Point Markings & Site Photographs

# Appendix E
DM1 and DM2 Furnace DEP Outlets Sample Location Dimensions and Point Locations Project 123987

Table 1: Sample Location Specifications

Parameter DM1 Furnace
DEP Outlet DM2 Furnace
DEP Outlet

Emission Unit # U-00002 U-00012

Emission Point # EP00100 EP00200

Stack Plane Configuration Rectangle Rectangle

Stack Diameter / Dimensions 3.28ft x 3.28ft 3.28ft x 3.28ft

Duct Configuration Vertical  Vertical 

Accessibility for Sampling Mobile ManLift Mobile ManLift

Number of Sampling Ports 5 5

Upstream Distance to Ports 5.6 ft 2.7 ft

Downstream Distance to Ports 10.6 ft 11.3 ft

Sample Port Size 4 inches ID 4 inches ID

Total # of Sampling Points 30 30

Sampling Matrix 5 x 6 5 x 6

Figure 1: OC Delmar Furnace DEP Units and Sample Locations

Common
DEP Stack

DM1 Furnace DEP DM2 Furnace DEP

Sample Location Sample Location



# Page 1 of 4

# Appendix E
DM1 and DM2 Furnace DEP Outlets Sample Location Dimensions and Point Locations Project 123987 Figure 2: OC Delmar Furnace DEP Outlet – Method 1 Sample Point Locations

Port lengths are 6.5 inches 3.3” 9.8” 16.4” 23” 29.5” 36.1” 

# 3.28 ft

3.28 ft

Port 1 Port 2 Port 3 Port 4 Port 5



# Page 2 of 4

# Appendix E
DM1 and DM2 Furnace DEP Outlets Sample Location Dimensions and Point Locations Project 123987 Figure 3: DM1 Furnace DEP Outlet Sample Location

Page 3 of 4

# Appendix E
DM1 and DM2 Furnace DEP Outlets Sample Location Dimensions and Point Locations Project 123987

Page 4 of 4 Figure 4: DM2 Furnace DEP Outlet Sample Location