Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-001 Date Collected: 08/07/2013 Date Received: 8/8/2013

 CPS Primary Clarifier Effluent

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.08 ug/L 0.050 0.010 DPC 08/14/2013 11:32 EPA 200.8

Arsenic, As 1.96 ug/L 0.10 0.030 DPC 08/14/2013 11:32 EPA 200.8

Barium, Ba 58.2 ug/L 0.10 0.020 DPC 08/14/2013 11:32 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 14:29 EPA 200.7

Cadmium, Cd 0.34 ug/L 0.050 0.010 DPC 08/14/2013 11:32 EPA 200.8

Chromium, Cr 5.7 ug/L 0.20 0.040 DPC 08/14/2013 11:32 EPA 200.8

Cobalt, Co 4.07 ug/L 0.020 0.0040 DPC 08/14/2013 11:32 EPA 200.8

Copper, Cu 1.16 ug/L 0.050 0.010 DPC 08/14/2013 11:32 EPA 200.8

Lead, Pb 0.591 ug/L 0.010 0.0020 DPC 08/14/2013 11:32 EPA 200.8

Mercury, Hg 570 ng/L 250 100 TLT 08/16/2013 EPA 1631E

Molybdenum, Mo 160 ug/L 0.050 0.010 DPC 08/14/2013 11:32 EPA 200.8

Nickel, Ni 46.6 ug/L 0.20 0.050 DPC 08/14/2013 11:32 EPA 200.8

Selenium, Se 187 ug/L 0.50 0.20 DPC 08/14/2013 11:32 EPA 200.8

Silver, Ag 0.0050 ug/L J 0.010 0.0020 DPC 08/14/2013 11:32 EPA 200.8

Thallium, Tl 1.55 ug/L 0.050 0.0020 DPC 08/14/2013 11:32 EPA 200.8

Tin, Sn 91.4 ug/L 50 10 DAM 08/20/2013 14:29 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 14:29 EPA 200.7

Zinc, Zn 8.9 ug/L 0.50 0.10 DPC 08/14/2013 11:32 EPA 200.8

Aluminum, Al 0.227 mg/L 0.0010 0.0003 DPC 08/14/2013 11:32 EPA 200.8

Boron, B 298 mg/L 0.20 0.040 DAM 08/20/2013 14:29 EPA 200.7

Calcium, Ca 770 mg/L 0.20 0.040 DAM 08/20/2013 14:29 EPA 200.7

Iron, Fe 0.553 mg/L 0.50 0.10 DAM 08/20/2013 14:29 EPA 200.7

Magnesium, Mg 2540 mg/L 0.10 0.020 DAM 08/20/2013 14:29 EPA 200.7

Manganese, Mn 29.4 mg/L 0.0050 0.0010 DAM 08/20/2013 14:29 EPA 200.7

Potassium, K 47.1 mg/L 0.50 0.070 DAM 08/20/2013 14:28 EPA 200.7

Sodium, Na 226 mg/L 0.50 0.080 DAM 08/20/2013 14:28 EPA 200.7

Strontium, Sr 6.59 mg/L 0.010 0.0030 DAM 08/20/2013 14:28 EPA 200.7

Ammonia, NH3, as N 1.29 mg/L 0.050 0.020 DMM 08/16/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.81 mg/L 0.50 0.10 DMM 08/14/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 29.4 mg/L 0.10 0.020 DMM 08/12/2013 SM20 4500NO3 H

Mountaineer Plant, 133216 Page 1 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-001A Date Collected: 08/07/2013 Date Received: 8/8/2013

 CPS Primary Clarifier Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.04 ug/L 0.050 0.010 DPC 08/14/2013 11:37 EPA 200.8

Arsenic, As 1.65 ug/L 0.10 0.030 DPC 08/14/2013 11:37 EPA 200.8

Barium, Ba 55.8 ug/L 0.10 0.020 DPC 08/14/2013 11:37 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 14:38 EPA 200.7

Cadmium, Cd 0.048 ug/L J 0.050 0.010 DPC 08/14/2013 11:37 EPA 200.8

Chromium, Cr 3.5 ug/L 0.20 0.040 DPC 08/14/2013 11:37 EPA 200.8

Cobalt, Co 3.63 ug/L 0.020 0.0040 DPC 08/14/2013 11:37 EPA 200.8

Copper, Cu 0.39 ug/L 0.050 0.010 DPC 08/14/2013 11:37 EPA 200.8

Lead, Pb 0.0090 ug/L J 0.010 0.0020 DPC 08/14/2013 11:37 EPA 200.8

Molybdenum, Mo 154 ug/L 0.050 0.010 DPC 08/14/2013 11:37 EPA 200.8

Nickel, Ni 43.2 ug/L 0.20 0.050 DPC 08/14/2013 11:37 EPA 200.8

Selenium, Se 181 ug/L 0.50 0.20 DPC 08/14/2013 11:37 EPA 200.8

Selenite, Se+4 (Hydride) 111 ug/L 20 4.0 TLT 08/26/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/14/2013 11:37 EPA 200.8

Thallium, Tl 1.42 ug/L 0.050 0.0020 DPC 08/14/2013 11:37 EPA 200.8

Tin, Sn 90.5 ug/L 50 10 DAM 08/20/2013 14:38 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 14:38 EPA 200.7

Zinc, Zn 4.1 ug/L 0.50 0.10 DPC 08/14/2013 11:37 EPA 200.8

Aluminum, Al 0.0235 mg/L 0.0010 0.0003 DPC 08/14/2013 11:37 EPA 200.8

Boron, B 287 mg/L 0.20 0.040 DAM 08/20/2013 14:38 EPA 200.7

Calcium, Ca 745 mg/L 0.20 0.040 DAM 08/20/2013 14:38 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/20/2013 14:38 EPA 200.7

Magnesium, Mg 2470 mg/L 0.10 0.020 DAM 08/20/2013 14:38 EPA 200.7

Manganese, Mn 28.5 mg/L 0.0050 0.0010 DAM 08/20/2013 14:38 EPA 200.7

Potassium, K 45.2 mg/L 0.50 0.070 DAM 08/20/2013 14:37 EPA 200.7

Sodium, Na 217 mg/L 0.50 0.080 DAM 08/20/2013 14:37 EPA 200.7

Strontium, Sr 6.39 mg/L 0.010 0.0030 DAM 08/20/2013 14:37 EPA 200.7

Mountaineer Plant, 133216 Page 2 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-002 Date Collected: 08/07/2013 Date Received: 8/8/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.01 ug/L 0.050 0.010 DPC 08/14/2013 11:41 EPA 200.8

Arsenic, As 1.72 ug/L 0.10 0.030 DPC 08/14/2013 11:41 EPA 200.8

Barium, Ba 69.2 ug/L 0.10 0.020 DPC 08/14/2013 11:41 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 14:47 EPA 200.7

Cadmium, Cd 0.23 ug/L 0.050 0.010 DPC 08/14/2013 11:41 EPA 200.8

Chromium, Cr 3.8 ug/L 0.20 0.040 DPC 08/14/2013 11:41 EPA 200.8

Cobalt, Co 1.09 ug/L 0.020 0.0040 DPC 08/14/2013 11:41 EPA 200.8

Copper, Cu 0.58 ug/L 0.050 0.010 DPC 08/14/2013 11:41 EPA 200.8

Lead, Pb 0.180 ug/L 0.010 0.0020 DPC 08/14/2013 11:41 EPA 200.8

Mercury, Hg 106 ng/L 20 8.0 TLT 08/16/2013 EPA 1631E

Molybdenum, Mo 174 ug/L 0.050 0.010 DPC 08/14/2013 11:41 EPA 200.8

Nickel, Ni 15.3 ug/L 0.20 0.050 DPC 08/14/2013 11:41 EPA 200.8

Selenium, Se 174 ug/L 0.50 0.20 DPC 08/14/2013 11:41 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 11:41 EPA 200.8

Thallium, Tl 0.74 ug/L 0.050 0.0020 DPC 08/14/2013 11:41 EPA 200.8

Tin, Sn 96.6 ug/L 50 10 DAM 08/20/2013 14:47 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 14:47 EPA 200.7

Zinc, Zn 3.4 ug/L 0.50 0.10 DPC 08/14/2013 11:41 EPA 200.8

Aluminum, Al 0.206 mg/L 0.0010 0.0003 DPC 08/14/2013 11:41 EPA 200.8

Boron, B 235 mg/L 0.20 0.040 DAM 08/20/2013 14:47 EPA 200.7

Calcium, Ca 626 mg/L 0.20 0.040 DAM 08/20/2013 14:47 EPA 200.7

Iron, Fe 0.16 mg/L J 0.50 0.10 DAM 08/20/2013 14:47 EPA 200.7

Magnesium, Mg 2100 mg/L 0.10 0.020 DAM 08/20/2013 14:47 EPA 200.7

Manganese, Mn 24.0 mg/L 0.0050 0.0010 DAM 08/20/2013 14:47 EPA 200.7

Potassium, K 39.5 mg/L 0.50 0.070 DAM 08/20/2013 14:46 EPA 200.7

Sodium, Na 187 mg/L 0.50 0.080 DAM 08/20/2013 14:46 EPA 200.7

Strontium, Sr 5.53 mg/L 0.010 0.0030 DAM 08/20/2013 14:46 EPA 200.7

Ammonia, NH3, as N 1.25 mg/L 0.050 0.020 DMM 08/16/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.79 mg/L 0.50 0.10 DMM 08/14/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 23.9 mg/L 0.10 0.020 DMM 08/12/2013 SM20 4500NO3 H

Mountaineer Plant, 133216 Page 3 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-002A Date Collected: 08/07/2013 Date Received: 8/8/2013

CPS Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.85 ug/L 0.050 0.010 DPC 08/14/2013 11:46 EPA 200.8

Arsenic, As 1.52 ug/L 0.10 0.030 DPC 08/14/2013 11:46 EPA 200.8

Barium, Ba 58.7 ug/L 0.10 0.020 DPC 08/14/2013 11:46 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 14:56 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 08/14/2013 11:46 EPA 200.8

Chromium, Cr 2.8 ug/L 0.20 0.040 DPC 08/14/2013 11:46 EPA 200.8

Cobalt, Co 0.199 ug/L 0.020 0.0040 DPC 08/14/2013 11:46 EPA 200.8

Copper, Cu 0.19 ug/L 0.050 0.010 DPC 08/14/2013 11:46 EPA 200.8

Lead, Pb 0.0060 ug/L J 0.010 0.0020 DPC 08/14/2013 11:46 EPA 200.8

Molybdenum, Mo 154 ug/L 0.050 0.010 DPC 08/14/2013 11:46 EPA 200.8

Nickel, Ni 4.35 ug/L 0.20 0.050 DPC 08/14/2013 11:46 EPA 200.8

Selenium, Se 157 ug/L 0.50 0.20 DPC 08/14/2013 11:46 EPA 200.8

Selenite, Se+4 (Hydride) 101 ug/L 20 4.0 TLT 08/26/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 11:46 EPA 200.8

Thallium, Tl 0.38 ug/L 0.050 0.0020 DPC 08/14/2013 11:46 EPA 200.8

Tin, Sn 92.8 ug/L 50 10 DAM 08/20/2013 14:57 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 14:57 EPA 200.7

Zinc, Zn 1.5 ug/L 0.50 0.10 DPC 08/14/2013 11:46 EPA 200.8

Aluminum, Al 0.0304 mg/L 0.0010 0.0003 DPC 08/14/2013 11:46 EPA 200.8

Boron, B 234 mg/L 0.20 0.040 DAM 08/20/2013 14:56 EPA 200.7

Calcium, Ca 625 mg/L 0.20 0.040 DAM 08/20/2013 14:56 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/20/2013 14:57 EPA 200.7

Magnesium, Mg 2110 mg/L 0.10 0.020 DAM 08/20/2013 14:56 EPA 200.7

Manganese, Mn 24.1 mg/L 0.0050 0.0010 DAM 08/20/2013 14:56 EPA 200.7

Potassium, K 39.4 mg/L 0.50 0.070 DAM 08/20/2013 14:55 EPA 200.7

Sodium, Na 187 mg/L 0.50 0.080 DAM 08/20/2013 14:55 EPA 200.7

Strontium, Sr 5.43 mg/L 0.010 0.0030 DAM 08/20/2013 14:55 EPA 200.7

Mountaineer Plant, 133216 Page 4 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-003 Date Collected: 08/07/2013 Date Received: 8/8/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.0 ug/L 0.050 0.010 DPC 08/14/2013 11:51 EPA 200.8

Arsenic, As 44.2 ug/L 0.10 0.030 DPC 08/14/2013 11:51 EPA 200.8

Barium, Ba 36.6 ug/L 0.10 0.020 DPC 08/14/2013 11:51 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 15:05 EPA 200.7

Cadmium, Cd 1.78 ug/L 0.050 0.010 DPC 08/14/2013 11:51 EPA 200.8

Chromium, Cr 0.3 ug/L 0.20 0.040 DPC 08/14/2013 11:51 EPA 200.8

Cobalt, Co 2.48 ug/L 0.020 0.0040 DPC 08/14/2013 11:51 EPA 200.8

Copper, Cu 0.55 ug/L 0.050 0.010 DPC 08/14/2013 11:51 EPA 200.8

Lead, Pb 0.028 ug/L 0.010 0.0020 DPC 08/14/2013 11:51 EPA 200.8

Mercury, Hg 49.0 ng/L 10 4.0 TLT 08/16/2013 EPA 1631E

Molybdenum, Mo 5270 ug/L 0.050 0.010 DPC 08/14/2013 11:51 EPA 200.8

Nickel, Ni 7.59 ug/L 0.20 0.050 DPC 08/14/2013 11:51 EPA 200.8

Selenium, Se 231 ug/L 0.50 0.20 DPC 08/14/2013 11:51 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/14/2013 11:51 EPA 200.8

Thallium, Tl 2.83 ug/L 0.050 0.0020 DPC 08/14/2013 11:51 EPA 200.8

Tin, Sn 41 ug/L J 50 10 DAM 08/20/2013 15:06 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 15:06 EPA 200.7

Zinc, Zn 2.4 ug/L 0.50 0.10 DPC 08/14/2013 11:51 EPA 200.8

Aluminum, Al 0.0168 mg/L 0.0010 0.0003 DPC 08/14/2013 11:51 EPA 200.8

Boron, B 54.2 mg/L 0.20 0.040 DAM 08/20/2013 15:05 EPA 200.7

Calcium, Ca 432 mg/L 0.20 0.040 DAM 08/20/2013 15:05 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/20/2013 15:06 EPA 200.7

Magnesium, Mg 408 mg/L 0.10 0.020 DAM 08/20/2013 15:05 EPA 200.7

Manganese, Mn 1.67 mg/L 0.0050 0.0010 DAM 08/20/2013 15:05 EPA 200.7

Potassium, K 109 mg/L 0.50 0.070 DAM 08/20/2013 15:04 EPA 200.7

Sodium, Na 1850 mg/L 0.50 0.080 DAM 08/20/2013 15:04 EPA 200.7

Strontium, Sr 5.69 mg/L 0.010 0.0030 DAM 08/20/2013 15:04 EPA 200.7

Ammonia, NH3, as N 1.05 mg/L 0.050 0.020 DMM 08/16/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.57 mg/L 0.50 0.10 DMM 08/14/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 3.72 mg/L 0.10 0.020 DMM 08/12/2013 SM20 4500NO3 H

Mountaineer Plant, 133216 Page 5 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-003A Date Collected: 08/07/2013 Date Received: 8/8/2013

Landfill Leachate Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.3 ug/L 0.050 0.010 DPC 08/14/2013 11:56 EPA 200.8

Arsenic, As 37.7 ug/L 0.10 0.030 DPC 08/14/2013 11:56 EPA 200.8

Barium, Ba 31.3 ug/L 0.10 0.020 DPC 08/14/2013 11:56 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 15:09 EPA 200.7

Cadmium, Cd 1.63 ug/L 0.050 0.010 DPC 08/14/2013 11:56 EPA 200.8

Chromium, Cr 0.17 ug/L J 0.20 0.040 DPC 08/14/2013 11:56 EPA 200.8

Cobalt, Co 1.69 ug/L 0.020 0.0040 DPC 08/14/2013 11:56 EPA 200.8

Copper, Cu 0.26 ug/L 0.050 0.010 DPC 08/14/2013 11:56 EPA 200.8

Lead, Pb 0.012 ug/L 0.010 0.0020 DPC 08/14/2013 11:56 EPA 200.8

Molybdenum, Mo 4740 ug/L 0.050 0.010 DPC 08/14/2013 11:56 EPA 200.8

Nickel, Ni 6.36 ug/L 0.20 0.050 DPC 08/14/2013 11:56 EPA 200.8

Selenium, Se 193 ug/L 0.50 0.20 DPC 08/14/2013 11:56 EPA 200.8

Selenite, Se+4 (Hydride) 120 ug/L 20 4.0 TLT 08/26/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 11:56 EPA 200.8

Thallium, Tl 2.41 ug/L 0.050 0.0020 DPC 08/14/2013 11:56 EPA 200.8

Tin, Sn < 10 ug/L U 50 10 DAM 08/20/2013 15:10 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 15:10 EPA 200.7

Zinc, Zn 2.7 ug/L 0.50 0.10 DPC 08/14/2013 11:56 EPA 200.8

Aluminum, Al 0.0064 mg/L 0.0010 0.0003 DPC 08/14/2013 11:56 EPA 200.8

Boron, B 52.2 mg/L 0.20 0.040 DAM 08/20/2013 15:09 EPA 200.7

Calcium, Ca 416 mg/L 0.20 0.040 DAM 08/20/2013 15:09 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/20/2013 15:10 EPA 200.7

Magnesium, Mg 392 mg/L 0.10 0.020 DAM 08/20/2013 15:09 EPA 200.7

Manganese, Mn 1.49 mg/L 0.0050 0.0010 DAM 08/20/2013 15:10 EPA 200.7

Potassium, K 108 mg/L 0.50 0.070 DAM 08/20/2013 15:08 EPA 200.7

Sodium, Na 1810 mg/L 0.50 0.080 DAM 08/20/2013 15:08 EPA 200.7

Strontium, Sr 5.56 mg/L 0.010 0.0030 DAM 08/20/2013 15:08 EPA 200.7

Mountaineer Plant, 133216 Page 6 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-004 Date Collected: 08/07/2013 Date Received: 8/8/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.54 ug/L 0.050 0.010 DPC 08/14/2013 12:01 EPA 200.8

Arsenic, As 19.7 ug/L 0.10 0.030 DPC 08/14/2013 12:01 EPA 200.8

Barium, Ba 54.6 ug/L 0.10 0.020 DPC 08/14/2013 12:01 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 15:13 EPA 200.7

Cadmium, Cd 1.11 ug/L 0.050 0.010 DPC 08/14/2013 12:01 EPA 200.8

Chromium, Cr 5.0 ug/L 0.20 0.040 DPC 08/14/2013 12:01 EPA 200.8

Cobalt, Co 1.89 ug/L 0.020 0.0040 DPC 08/14/2013 12:01 EPA 200.8

Copper, Cu 2.21 ug/L 0.050 0.010 DPC 08/14/2013 12:01 EPA 200.8

Lead, Pb 0.140 ug/L 0.010 0.0020 DPC 08/14/2013 12:01 EPA 200.8

Mercury, Hg 76.6 ng/L 10 4.0 TLT 08/16/2013 EPA 1631E

Molybdenum, Mo 3130 ug/L 0.050 0.010 DPC 08/14/2013 12:01 EPA 200.8

Nickel, Ni 15.2 ug/L 0.20 0.050 DPC 08/14/2013 12:01 EPA 200.8

Selenium, Se 196 ug/L 0.50 0.20 DPC 08/14/2013 12:01 EPA 200.8

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 08/14/2013 12:01 EPA 200.8

Thallium, Tl 1.67 ug/L 0.050 0.0020 DPC 08/14/2013 12:01 EPA 200.8

Tin, Sn 81.6 ug/L 50 10 DAM 08/20/2013 15:14 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 15:13 EPA 200.7

Zinc, Zn 4.1 ug/L 0.50 0.10 DPC 08/14/2013 12:01 EPA 200.8

Aluminum, Al 0.110 mg/L 0.0010 0.0003 DPC 08/14/2013 12:01 EPA 200.8

Boron, B 172 mg/L 0.20 0.040 DAM 08/20/2013 15:13 EPA 200.7

Calcium, Ca 583 mg/L 0.20 0.040 DAM 08/20/2013 15:13 EPA 200.7

Iron, Fe 0.879 mg/L 0.50 0.10 DAM 08/20/2013 15:14 EPA 200.7

Magnesium, Mg 1440 mg/L 0.10 0.020 DAM 08/20/2013 15:13 EPA 200.7

Manganese, Mn 15.4 mg/L 0.0050 0.0010 DAM 08/20/2013 15:13 EPA 200.7

Potassium, K 71.1 mg/L 0.50 0.070 DAM 08/20/2013 15:12 EPA 200.7

Sodium, Na 917 mg/L 0.50 0.080 DAM 08/20/2013 15:12 EPA 200.7

Strontium, Sr 5.68 mg/L 0.010 0.0030 DAM 08/20/2013 15:12 EPA 200.7

Ammonia, NH3, as N 0.86 mg/L 0.050 0.020 DMM 08/16/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.01 mg/L 0.50 0.10 DMM 08/14/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 15.1 mg/L 0.10 0.020 DMM 08/12/2013 SM20 4500NO3 H

Mountaineer Plant, 133216 Page 7 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-004A Date Collected: 08/07/2013 Date Received: 8/8/2013

1st Stage Feed Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 4.95 ug/L 0.050 0.010 DPC 08/14/2013 12:06 EPA 200.8

Arsenic, As 15.4 ug/L 0.10 0.030 DPC 08/14/2013 12:06 EPA 200.8

Barium, Ba 48.9 ug/L 0.10 0.020 DPC 08/14/2013 12:06 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 15:17 EPA 200.7

Cadmium, Cd 0.52 ug/L 0.050 0.010 DPC 08/14/2013 12:06 EPA 200.8

Chromium, Cr 1.9 ug/L 0.20 0.040 DPC 08/14/2013 12:06 EPA 200.8

Cobalt, Co 0.804 ug/L 0.020 0.0040 DPC 08/14/2013 12:06 EPA 200.8

Copper, Cu 0.15 ug/L 0.050 0.010 DPC 08/14/2013 12:06 EPA 200.8

Lead, Pb 0.0090 ug/L J 0.010 0.0020 DPC 08/14/2013 12:06 EPA 200.8

Molybdenum, Mo 2910 ug/L 0.050 0.010 DPC 08/14/2013 12:06 EPA 200.8

Nickel, Ni 5.78 ug/L 0.20 0.050 DPC 08/14/2013 12:06 EPA 200.8

Selenium, Se 173 ug/L 0.50 0.20 DPC 08/14/2013 12:06 EPA 200.8

Selenite, Se+4 (Hydride) 104 ug/L 20 4.0 TLT 08/26/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 12:06 EPA 200.8

Thallium, Tl 1.26 ug/L 0.050 0.0020 DPC 08/14/2013 12:06 EPA 200.8

Tin, Sn 66.9 ug/L 50 10 DAM 08/20/2013 15:18 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 15:18 EPA 200.7

Zinc, Zn 2.4 ug/L 0.50 0.10 DPC 08/14/2013 12:06 EPA 200.8

Aluminum, Al 0.0207 mg/L 0.0010 0.0003 DPC 08/14/2013 12:06 EPA 200.8

Boron, B 171 mg/L 0.20 0.040 DAM 08/20/2013 15:17 EPA 200.7

Calcium, Ca 579 mg/L 0.20 0.040 DAM 08/20/2013 15:17 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/20/2013 15:18 EPA 200.7

Magnesium, Mg 1430 mg/L 0.10 0.020 DAM 08/20/2013 15:17 EPA 200.7

Manganese, Mn 15.1 mg/L 0.0050 0.0010 DAM 08/20/2013 15:17 EPA 200.7

Potassium, K 69.0 mg/L 0.50 0.070 DAM 08/20/2013 15:16 EPA 200.7

Sodium, Na 892 mg/L 0.50 0.080 DAM 08/20/2013 15:16 EPA 200.7

Strontium, Sr 5.52 mg/L 0.010 0.0030 DAM 08/20/2013 15:16 EPA 200.7

Mountaineer Plant, 133216 Page 8 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-005 Date Collected: 08/07/2013 Date Received: 8/8/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 13.7 ug/L 0.050 0.010 DPC 08/14/2013 12:10 EPA 200.8

Arsenic, As 15.2 ug/L 0.10 0.030 DPC 08/14/2013 12:10 EPA 200.8

Barium, Ba 53.4 ug/L 0.10 0.020 DPC 08/14/2013 12:10 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 15:36 EPA 200.7

Cadmium, Cd 0.58 ug/L 0.050 0.010 DPC 08/14/2013 12:10 EPA 200.8

Chromium, Cr 1.0 ug/L 0.20 0.040 DPC 08/14/2013 12:10 EPA 200.8

Cobalt, Co 2.84 ug/L 0.020 0.0040 DPC 08/14/2013 12:10 EPA 200.8

Copper, Cu 0.44 ug/L 0.050 0.010 DPC 08/14/2013 12:10 EPA 200.8

Lead, Pb 0.015 ug/L 0.010 0.0020 DPC 08/14/2013 12:10 EPA 200.8

Mercury, Hg 8.9 ng/L J 10 4.0 TLT 08/16/2013 EPA 1631E

Molybdenum, Mo 3030 ug/L 0.050 0.010 DPC 08/14/2013 12:10 EPA 200.8

Nickel, Ni 14.5 ug/L 0.20 0.050 DPC 08/14/2013 12:10 EPA 200.8

Selenium, Se 42.0 ug/L 0.50 0.20 DPC 08/14/2013 12:10 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 12:10 EPA 200.8

Thallium, Tl 3.27 ug/L 0.050 0.0020 DPC 08/14/2013 12:10 EPA 200.8

Tin, Sn 118 ug/L 50 10 DAM 08/20/2013 15:36 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 15:36 EPA 200.7

Zinc, Zn 1.2 ug/L 0.50 0.10 DPC 08/14/2013 12:10 EPA 200.8

Aluminum, Al 0.297 mg/L 0.0010 0.0003 DPC 08/14/2013 12:10 EPA 200.8

Boron, B 196 mg/L 0.20 0.040 DAM 08/20/2013 15:36 EPA 200.7

Calcium, Ca 674 mg/L 0.20 0.040 DAM 08/20/2013 15:36 EPA 200.7

Iron, Fe 0.812 mg/L 0.50 0.10 DAM 08/20/2013 15:36 EPA 200.7

Magnesium, Mg 1640 mg/L 0.10 0.020 DAM 08/20/2013 15:36 EPA 200.7

Manganese, Mn 16.9 mg/L 0.0050 0.0010 DAM 08/20/2013 15:36 EPA 200.7

Potassium, K 73.9 mg/L 0.50 0.070 DAM 08/20/2013 15:34 EPA 200.7

Sodium, Na 999 mg/L 0.50 0.080 DAM 08/20/2013 15:34 EPA 200.7

Strontium, Sr 5.81 mg/L 0.010 0.0030 DAM 08/20/2013 15:34 EPA 200.7

Ammonia, NH3, as N 1.73 mg/L 0.050 0.020 DMM 08/16/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.66 mg/L 0.50 0.10 DMM 08/14/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 2.26 mg/L 0.10 0.020 DMM 08/12/2013 SM20 4500NO3 H

Mountaineer Plant, 133216 Page 9 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-005A Date Collected: 08/07/2013 Date Received: 8/8/2013

2nd Stage Feed Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.9 ug/L 0.050 0.010 DPC 08/14/2013 12:44 EPA 200.8

Arsenic, As 12.5 ug/L 0.10 0.030 DPC 08/14/2013 12:44 EPA 200.8

Barium, Ba 46.3 ug/L 0.10 0.020 DPC 08/14/2013 12:44 EPA 200.8

Beryllium, Be < 1.0 ug/L U 5.0 1.0 DAM 08/20/2013 15:40 EPA 200.7

Cadmium, Cd 0.44 ug/L 0.050 0.010 DPC 08/14/2013 12:44 EPA 200.8

Chromium, Cr 0.7 ug/L 0.20 0.040 DPC 08/14/2013 12:44 EPA 200.8

Cobalt, Co 2.41 ug/L 0.020 0.0040 DPC 08/14/2013 12:44 EPA 200.8

Copper, Cu 0.12 ug/L 0.050 0.010 DPC 08/14/2013 12:44 EPA 200.8

Lead, Pb 0.011 ug/L 0.010 0.0020 DPC 08/14/2013 12:44 EPA 200.8

Molybdenum, Mo 2670 ug/L 0.050 0.010 DPC 08/14/2013 12:44 EPA 200.8

Nickel, Ni 12.9 ug/L 0.20 0.050 DPC 08/14/2013 12:44 EPA 200.8

Selenium, Se 12.3 ug/L 0.50 0.20 DPC 08/14/2013 12:44 EPA 200.8

Selenite, Se+4 (Hydride) 5.5 ug/L 2.0 0.40 TLT 08/26/2013 AEP Method

Silver, Ag 0.0040 ug/L J 0.010 0.0020 DPC 08/14/2013 12:44 EPA 200.8

Thallium, Tl 2.84 ug/L 0.050 0.0020 DPC 08/14/2013 12:44 EPA 200.8

Tin, Sn 100 ug/L 50 10 DAM 08/20/2013 15:40 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 15:40 EPA 200.7

Zinc, Zn 1.9 ug/L 0.50 0.10 DPC 08/14/2013 12:44 EPA 200.8

Aluminum, Al 0.249 mg/L 0.0010 0.0003 DPC 08/14/2013 12:44 EPA 200.8

Boron, B 191 mg/L 0.20 0.040 DAM 08/20/2013 15:40 EPA 200.7

Calcium, Ca 654 mg/L 0.20 0.040 DAM 08/20/2013 15:40 EPA 200.7

Iron, Fe 0.705 mg/L 0.50 0.10 DAM 08/20/2013 15:40 EPA 200.7

Magnesium, Mg 1590 mg/L 0.10 0.020 DAM 08/20/2013 15:40 EPA 200.7

Manganese, Mn 16.4 mg/L 0.0050 0.0010 DAM 08/20/2013 15:40 EPA 200.7

Potassium, K 73.2 mg/L 0.50 0.070 DAM 08/20/2013 15:38 EPA 200.7

Sodium, Na 1040 mg/L 0.50 0.080 DAM 08/20/2013 15:38 EPA 200.7

Strontium, Sr 5.88 mg/L 0.010 0.0030 DAM 08/20/2013 15:38 EPA 200.7

Mountaineer Plant, 133216 Page 10 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-006 Date Collected: 08/07/2013 Date Received: 8/8/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.10 ug/L 0.050 0.010 DPC 08/14/2013 12:49 EPA 200.8

Arsenic, As 0.38 ug/L 0.10 0.030 DPC 08/14/2013 12:49 EPA 200.8

Barium, Ba 63.0 ug/L 0.10 0.020 DPC 08/14/2013 12:49 EPA 200.8

Beryllium, Be 1.1 ug/L J 5.0 1.0 DAM 08/20/2013 17:05 EPA 200.7

Cadmium, Cd 0.014 ug/L J 0.050 0.010 DPC 08/14/2013 12:49 EPA 200.8

Chromium, Cr 0.8 ug/L 0.20 0.040 DPC 08/14/2013 12:49 EPA 200.8

Cobalt, Co 0.053 ug/L 0.020 0.0040 DPC 08/14/2013 12:49 EPA 200.8

Copper, Cu 0.06 ug/L 0.050 0.010 DPC 08/14/2013 12:49 EPA 200.8

Lead, Pb 0.0080 ug/L J 0.010 0.0020 DPC 08/14/2013 12:49 EPA 200.8

Mercury, Hg 1.5 ng/L 1.0 0.40 TLT 08/16/2013 EPA 1631E

Molybdenum, Mo 73.1 ug/L 0.050 0.010 DPC 08/14/2013 12:49 EPA 200.8

Nickel, Ni 1.96 ug/L 0.20 0.050 DPC 08/14/2013 12:49 EPA 200.8

Selenium, Se 1.0 ug/L 0.50 0.20 DPC 08/14/2013 12:49 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/14/2013 12:49 EPA 200.8

Thallium, Tl 0.035 ug/L J 0.050 0.0020 DPC 08/14/2013 12:49 EPA 200.8

Tin, Sn 128 ug/L 50 10 DAM 08/20/2013 17:05 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 17:05 EPA 200.7

Zinc, Zn 0.6 ug/L 0.50 0.10 DPC 08/14/2013 12:49 EPA 200.8

Aluminum, Al 1.29 mg/L 0.0010 0.0003 DPC 08/14/2013 12:49 EPA 200.8

Boron, B 177 mg/L 0.20 0.040 DAM 08/20/2013 17:05 EPA 200.7

Calcium, Ca 604 mg/L 0.20 0.040 DAM 08/20/2013 17:05 EPA 200.7

Iron, Fe 0.42 mg/L J 0.50 0.10 DAM 08/20/2013 17:05 EPA 200.7

Magnesium, Mg 1440 mg/L 0.10 0.020 DAM 08/20/2013 17:05 EPA 200.7

Manganese, Mn 14.7 mg/L 0.0050 0.0010 DAM 08/20/2013 17:05 EPA 200.7

Potassium, K 72.5 mg/L 0.50 0.070 DAM 08/20/2013 17:03 EPA 200.7

Sodium, Na 903 mg/L 0.50 0.080 DAM 08/20/2013 17:03 EPA 200.7

Strontium, Sr 5.62 mg/L 0.010 0.0030 DAM 08/20/2013 17:03 EPA 200.7

Ammonia, NH3, as N 2.77 mg/L 0.050 0.020 DMM 08/16/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 6.06 mg/L 0.50 0.10 DMM 08/14/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N < 0.020 mg/L U 0.10 0.020 DMM 08/12/2013 SM20 4500NO3 H

Mountaineer Plant, 133216 Page 11 of 12
Location: Mountaineer Plant Report Date: 8/27/2013

Sample Number: 133216-006A Date Collected: 08/07/2013 Date Received: 8/8/2013

Bioreactor Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.07 ug/L 0.050 0.010 DPC 08/14/2013 12:53 EPA 200.8

Arsenic, As 0.30 ug/L 0.10 0.030 DPC 08/14/2013 12:53 EPA 200.8

Barium, Ba 50.8 ug/L 0.10 0.020 DPC 08/14/2013 12:53 EPA 200.8

Beryllium, Be 2.7 ug/L J 5.0 1.0 DAM 08/20/2013 17:09 EPA 200.7

Cadmium, Cd 0.010 ug/L J 0.050 0.010 DPC 08/14/2013 12:53 EPA 200.8

Chromium, Cr 0.6 ug/L 0.20 0.040 DPC 08/14/2013 12:53 EPA 200.8

Cobalt, Co 0.043 ug/L 0.020 0.0040 DPC 08/14/2013 12:53 EPA 200.8

Copper, Cu 0.040 ug/L J 0.050 0.010 DPC 08/14/2013 12:53 EPA 200.8

Lead, Pb < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 12:53 EPA 200.8

Molybdenum, Mo 57.4 ug/L 0.050 0.010 DPC 08/14/2013 12:53 EPA 200.8

Nickel, Ni 1.71 ug/L 0.20 0.050 DPC 08/14/2013 12:53 EPA 200.8

Selenium, Se 1.0 ug/L 0.50 0.20 DPC 08/14/2013 12:53 EPA 200.8

Selenite, Se+4 (Hydride) < 0.080 ug/L U 0.40 0.080 TLT 08/26/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/14/2013 12:53 EPA 200.8

Thallium, Tl 0.019 ug/L J 0.050 0.0020 DPC 08/14/2013 12:53 EPA 200.8

Tin, Sn 109 ug/L 50 10 DAM 08/20/2013 17:09 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/20/2013 17:09 EPA 200.7

Zinc, Zn 1.4 ug/L 0.50 0.10 DPC 08/14/2013 12:53 EPA 200.8

Aluminum, Al 1.02 mg/L 0.0010 0.0003 DPC 08/14/2013 12:53 EPA 200.8

Boron, B 169 mg/L 0.20 0.040 DAM 08/20/2013 17:09 EPA 200.7

Calcium, Ca 569 mg/L 0.20 0.040 DAM 08/20/2013 17:09 EPA 200.7

Iron, Fe 0.37 mg/L J 0.50 0.10 DAM 08/20/2013 17:09 EPA 200.7

Magnesium, Mg 1360 mg/L 0.10 0.020 DAM 08/20/2013 17:09 EPA 200.7

Manganese, Mn 13.8 mg/L 0.0050 0.0010 DAM 08/20/2013 17:09 EPA 200.7

Potassium, K 71.2 mg/L 0.50 0.070 DAM 08/20/2013 17:07 EPA 200.7

Sodium, Na 867 mg/L 0.50 0.080 DAM 08/20/2013 17:07 EPA 200.7

Strontium, Sr 5.34 mg/L 0.010 0.0030 DAM 08/20/2013 17:07 EPA 200.7

Sample Number: 133216-007 Date Collected: 08/07/2013 Date Received: 8/8/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 0.49 ng/L J 0.50 0.20 TLT 08/16/2013 EPA 1631E

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 133216 Page 12 of 12