Exhaust Emissions

Sampling Acme Brick, Tulsa,

OK Tunnel Kiln Exhaust September 6, 2002 Armstrong Environmental,

Inc. Project W-2222-02

Report Prepared

For" Mike O'Conner Acme Brick 2821 West Seventh

Street Ft. Worth, TX 76107

Report Prepared

September

12, 2002 By: Armstrong Environmental,

Inc. 7715 Sovereign

Row Dallas, Texas 75247 (214) 631-0021TABLE OF CONTENTS

I, Introduction

12. Summary

II2. Procedures

IV. Appendices

A. Calculation

Summaries

B. Continuous

Emissions

Monitor

Summaries

C. Analytical

Summaries

D. Field Data Sheets

E. Equipment

Calibrations

F. Standard

Gas Certifications Page

1

2-3

4-7

8-10

12 42

43 72

73 75

76 78

79 87I. INTRODUCTION

A series of tests was performed

on the exhaust associated

with the Tunnel Kiln at the Acme Brick facility in Tulsa, OK on September

6, 2002.

The purpose

of this test series was to determine

the exhaust emission

rate of PM, CO, NOx, VOC, SO2, HF and HC1 in terms of lbs/hr. Testing followed

procedures

detailed

in Title 40: Code of Federal Regulations

(40:CFR). Sampling was performed

by Bart Tarbell,

Richard

Taylor and Tom Armstrong

of Armstrong Environmental,

Inc using an Apex Method

5 sampling

train, a Fuji 3300 continuous CO analyzer,

an EcoPhysics

70S continuous

NOx analyzer,

a Western Research 721 AT continuous

SO2 analyzer,

and a ThermoEnvlronmental Model 51 continuous FIX) anaIyzer.

Three one hour test repetitions

were performed,

commencing

at 9:20 AM and ending at 1:11 PM.

Submitted by:II. SUMMARY

A series of tests was performed

on the exhaust associated

with the Tunnel Kiln at the Acme Brick facility in Tulsa, OK on September

6, 2002. Sampling was performed

following

procedures

detailed

in Title 40: Code of Federal Regulations.

Results of this test series are summarized

in Table 1.

Results indicate

the following

emissions

rates:

PM, lbs/hr

2.906

2.272

2.551

2.576 CO, lbs/hr

17.65

16.87

16.39

16.97 NOx, lbs/hr

7.178

6.774

6.629

6.844 VOC, lbs/hr SO2, lbs/hr HF, lbs/hr HC1, lbs/hr

1.935 7.658 11.59 2.976

1.966 9.254 10.69 1.889

2.103 9.510 11.28 2.778

2.001 8.807 11.19 2.548

i
\f i

2SUMMARY OF EMISSIONS.TEST

DATA Tabie: Plant Acme Brick, Tulsa, OK Location Tunnel Kiln Exhaust Operator R. Taylor, B. Tarbell, T. Armstrong Test Date 6.Sep-02 Repetition 2 STACK GAS Temperature, F , 452.6

467.0 Velocity, fps 40.96

40 ::)4 Volume Flow, acfm 35202.8

34420.1 scfm 18487 5

17844 5 scfh 1109252

1070672 Moisture, % 8.17%

7.90% CO2, % 3.00

3.00 02, % 17.00

17.00 SAMPLE Start Time, hrs:min 9:20 AM

10:45 AM Finish Time, hrs:min 10:22 AM

11 '46 AM Sample Volume, scf 41.228

39.571 Isokinetic Ratio, % 99.90021

99.3385 PARTICULATE Front Half Sample Weight, mg 38.72

28.31 Concentration, gr/scf 0.014491

0.011039 Emissions, Ibs/hr 2.297093

1.689007
Back Half S•mple Weight, mg 10.26

9.77 Concentration, gr/scf 0.00384

0.00381 Emissions, Ibs/hr 0.608682

0.58289
Total Particulate,

Ibs/hr

2.905775

2.271897 CARBON MONOXIDE Concentration, ppm 218.89

216.77 Emissions, Ibs/hr 17.64932

16.87047
NITROGEN OXIDE AS NO2 Concentration, ppm 54 19

52 98 Em!ssions, Ibs/hr 7.178289

6.773916
VOC AS Carbon Concentration, ppm as C3H8, WET

17,14

18.10 Concentration, ppm as C, DRY

55.99318

58.957 Emissions, Ibs/hr 1.934908

1.966467
SULFUR DIOXIDE Concentration, ppm 41.55

52.02 Emissions, Ibs/hr 7.657641

9.253805 HYDROGEN FLUORIDE Sample Weight, mg 195.40

179.13 Concentration, ppm 201.2768

192.2472 Emissions, Ibs/hr 11.59225

10.6871 HYDROGEN CHLORIDE Sample Weight, mg 50.16

31.66 Concentration, ppm 28 31156

18.61829 Emissions, Ibs/hr 2.975779

1.888872 451.5 3982 34222.6 18023.2 1081391 8.00% 3.00. 17.00

I2:10 PM 1:11 PM 39.8c•2 99.15214

31.95 0.012358 1.909757

10.72 0.004146 0.64077

2.550527

208.46 16.38616

51 33 6.628655

19.14 62.41334 2.1O2592

52.93 9.509949

188.68 200.8662 11.27803

46.47 27.10759 2.777666

3III. PROCEDURES

The procedure

for emissions

sampling

followed

USEPA

test methods

as detailed

in Title 40: Code of Federal Regulations.

The following

methods

were used:

Method Title Sample and Velocity

Traverses

for Stationary

Sources

2 Determination

of Stack Gas Velocity

and Volumetric

Flow Rate (Type S Pitot Tube)

Gas Analysis

for the Determination

of Dry Molecular

Weight

Determination of Particulate

Emissions

from Stationary

Sources

6C Determination

of Sulfur Dioxide

Emissions

from Stationary

Sources (Instrumental Analyzer

Procedure)

7E Determination

of Nitrogen

Oxides Emissions

from Stationary

Sources (Instrumental Analyzer

Procedure)

10 Determination

of Carbon Monoxide

Emissions

from Stationary

Sources

25A Determination

of Total Gaseous

Organic

Concentration

using a Flame Ionization Analyzer

26A Determination

of Hydrogen

Halides and Halogens

Emissions

from Stationary Sources

02 and CO2 were determined

using FyRite Analyzers.

PM. HF and HC1 sampling

was performed

for 2.5 minutes

at each of 24 points, 12 points per traverse,

making a total run duration

of 60 minutes.

A schematic

of the sampling location is shown in Figure 1. The sampling

train was configured

as follows:

Glass Sampling

Nozzle Heated Glass Lined Probe Heated teflon filter Impinger #1 100 mls H20 Impinger #2 100 mls 0.1 N H2SO4 Impinger #3 100 mls 0.1 N H2SO4 Impinger #4 Empty Impinger #5 200 grams silica GelAnalysis for PM was performed

on the probe wash, t•lter, and solution

from the first impinger. HF and HC1 analysis

was performed

on an aliquot from the first impinger,

and the solution

from the 2nd and 3rd impir•gers.

Analysis

was performed

using a Dionex 500DX IC/HPLC.

Impinger

analysis

includes

total solids and organics

extracted

with methylene chloride

(extractions

performed

after an aliquot was taken for HC1 analysis). Teflon beakers were used for total solids analysis

of the impinger

solutions.
VOC as C3H8 was determined

using a ThermoEnvironmental Model 51 continuous

FID analyzer. The analyzer

was calibrated

with 50.3 pprn, 29.6 ppm, and 14.7 ppm C3H8 in Air USEPA

Protocol

gas standards,

zeroed with N2. Nitrogen Oxides were determined

using a EcoPhysics

70S continuous

NOx analyzer. The analyzer

was calibrated

with 48.8 ppm and 25.1 ppm NOx in N2 EPA Protocol

1 gas standards, and zeroed N2.

Carbon monoxide

was determined

using a Fuji 3300 NDIR continuous

CO analyzer.

The analyzer was calibrated

with 199 ppm and a 99.4 ppm CO in EPA Protocol

1 gas standards, and zeroed with N2.

Sulfur dioxide was determined

on the scrubber

exhaust using a Western

Research

721 AT continuous SO2 analyzer.

The. analyzer

was calibrated

with 91 ppm and a 52.2 ppm SO2 in N2 EPA Protocol

1 gas standards,

zeroed with N2.

A schematic

of CEM contSguration

is shown in Figure 2.///0Appendix AEMISSION TEST SUMMARY

PLANT Acme Brick, Tulsa, OK DATE 6-Sep-02 PLACE Tunnel Kiln Exhaust RUN#

TEST DURATION (MINUTES) NOZZLE DIAMETER (INCH.) METER COEFFICIENT

(Y) PITOT COEFFICIENT

(Cp) GAS METER VOL.(Cu,Ft.) BAROMETRIC PRESSURE

60 LIQUID COLLECTED (mls) 0,3127 PARTICULATE

WEIGF (Front half mg) 0.984 PARTICULATE

WEIGHT (Back halfmg): 0.84 STATIC PRESSURE(m

H20): 44,316 PERCENTC02 29.45 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER (inch):

51.25 STACK AREA (Sq.Ft.)

14,32568 NOZZLE AREA (feet):

0,000533

ENTER THE STACK AREA SHOWN ABOVE:

FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD, CU.FT,): FRACTIONAL MOISTURE CONTENT (%): DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE):

STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH):

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION

(GR,/SCF): PARTICULATE CONCENTRATION

(LBS/SCF): PARTICULATE EMISSION (LBS/HR):

BACK HALF PARTICULATE CONCENTRATION

(GR./SCF): PARTICULATE CONCENTRATION

(LBS/SCF): PARTICULATE EMISSION (LBS/HR):

ISOKINETIC RATIO (%):

FOR RECTANGULAR

STACK STACK LENGTH(inchs) STACK WIDTH(inchs) STACK AREA (Sq.Ft.)

]4.32568

41.2283 3.6668 0.0817 80,0000 29.1600 28.2485

29.5750 40.9554 35202.809 1109252.08

0.0145 2.07E.06 2.2971

0.0038 5.49E-07 0.6087

99.9002

77,9 38.72 10.26 1.73170

POINTS STACKT. DELTAP SQUAR D.P deg DELTA H

400 0.]9 0.43589

0,89 2 408 0.22 0,469842

1,00 3 418 0.27 0.519615

1.30 4 430 0.28 0.52915

1.30 5 455 0.32 0.565685

1.40 6 458 0.34 0.583095

1.50 7 453 0.37 0.608276

1.70 8 440 0,34 0.583095

1.55 9 440 0.33 0.574456

1.50 10 438 0.31 0:556776

1.40 11 433 0.29 0.538516

1,30 12 377 0.42 0,648074

2.t0 13 480 0,18 0.424264

0.78 14 506 0,24 0.489898

1.00 15 538 0.24 0,489898

0.98 16 539 0.27 0.519615

1,10 17 526 0.29 0,538516

1.20 18 550 0.34 0.583095

1.40 19 444 0,35 0,591608

1.60 20 442 0.34 0.583095

1.50 21 450 0.31 •.556776

1.40 22 441 0.30 0.547723

].40 23 435 0.27 0,519615

1.20 24 362 0.41 0.640312

2.10 METER T, INLET

848788929393959796969696959897979797979898989898 METER T. OUTLET

848485858585868787878788888989898989909090909O9O METER T. AVERAGE

452.625 0,5457 1.3583

95.04]7

87.6250 91.3333EMISSION TEST SUMMARY

PEANT Acme Brick, Tulsa, OK DATE 6-Sep-02 PLACE Tuno&l Kiln Exhaust RUN# 2

TEST DURATION (MINUTES) NOZZLE DIAMETER (INCH.) METER COEFFICIENT

(Y) PITOT COEFFICIENT

(Cp) GAS METER VOL.(Cu,Ft.) BAROMETRIC PRESSURE

60 LIQUID COLLECTED (mls) 0.3127 PARTICULATE

WEIGHT {Front half rag)" 0.984 PARTICULATE

WEIGHT (Back half rag): 0.84 STATIC PRESSURE (in. H20): 42.861 PERCENTC02 29.45 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER Cinch): STACK AREA (Sq,Ft.) NOZZLE AREA (feet):

ENTER THE STACK AREA SHOWN ABOVE:

FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD, CU,FT.): FRACTIONAL MOISTURE CONTENT (%): DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT, OF STACK GAS (WET BASE):

STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH):

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION

(GR./SCF): PARTICULATE CONCENTRATION

(LBS/SCF): PARTICULATE EMISSION (LBS/HR):

BACK HALF PARTICULATE CONCENTRATION

(GR./SCF): PARTICULATE CONCENTRATION

(LBS/SCF): PARTICULATE EMISSION (LBS/HR):

ISOKINETIC RATIO (%):

FOR RECTANGULAR

STACK 51,25 STACK LENGTH(inches): 14.32568 STACKWIDTH(mches) 0.000533 STACK AREA(Sq.Ft.):

]4,32568

39.5707 3.3937 0.0790 80.0000 29.1600 28.2785

29.5676 4C 0447 34420,0658 1070671.63

0 0110 1,58E-06 1.6890

0.0038 5,44E-07 0.5829

99.3385

72.1 28,31 9,771.63170

POINTS STACKT. DELTA P SQUARD,P dec

615 0.]8 0,424264 2 583 0.19 0.43589 3 545 0,23 0.479583 4 518 0.25

0.5 5 489 0.29 0,538516 6 478 0.33 0,574456 7 456 0,36

0,6 8 454 0,33 0.574456 9 453 0.31 0.556776 10 452 0.29 0.538516 11 449 0.26 0,509902 12 416 0.40 0.632456 13 546 0,]9 0,43589 14 530 0.19 0.43589 15 515 0,21 0.458258 16 481 0.25

0.5 17 462 0.27 0,519615 18 448 0.32 0.565685 19 313 0.36

0.6 20 352 0.35 0,591608 21 338 0,31 0.556776 22 452 0,30 0.547723 23 448 0.26 0.509902 24 414 0.39 0,6245 DELTA H

0.90 0,75 0.94 1.00 1.26 1,40 1.60 1.50 1.40 1.30 1,20 1,90 0.76 0,79 0.88 1.10 1.20 1.40 1.90 1.80 1,60 1,40 1.20 1,85 METER T NLET

9092959697989899 ]00 !00 ]0099989999 100 100 ]00 ]00 101 ]02 102 102 103 METER T. OUTLET

909O9O9O9091919191929292929393939393939494959595 METER T. AVERAGE

466.95833 0.5296 1,2929

98.7500

92.2083 95.4792EMISSION TEST SUMMARY

PLANT Acme Brick, Tulsa, OK DATE 6-Sep-02 PLACE Tunnel Kiln Exhaust RUN# 3

TEST DURATION (MINUTES) NOZZLE DIAMETER (INCH.) METER COEFFICIENT

(Y) PITOT COEFFICIENT

(Cp) GAS METER VOL.(Cu.Ft.) BAROMETRIC PRESSURE

60 LIQUID COLLECTED (mls) 0,3127 PARTICULATE

WEIGHT (Front halfmg): 0.984 PARTICULATE

WEIGHT (Back half rag): 0.84 STATIC PRESSURE (in. H20): 43.678 PERCENTC02 29,45 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK STACK DIAMETER Cinch): STACK AREA (Sq.Ft.) NOZZLE AREA (feet):

ENTER THE STACK AREA SHOWN ABOVE:

FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD. CU.FT.): FRACTIONAL MOISTURE CONTENT (%): DRY BASE: MOLECULAR WT, OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE):

STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec,): ACTUAL STACK GAS ELOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH)

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION

(GR,/SCF): PARTICULATE CONCENTRATION

(LBS/SCF): PARTICULATE EMISSION (LBS/HR):

BACK HALF PARTICULATE CONCENTRATION

(GR./SCF): PARTICULATE CONCENTRATION

(LBS/SCF): PARTICULATE EMISSION (LBS/HR):

ISOKINETIC RATIO (%):

FOR RECTANGULAR

STACK 51.25 STACKLENGTH(inchs): 14.32568 STACKWIDTH(inchs) 0,000533 STACK AREA(Sq,Ft.):

14.32568

39.8918 3.4691 0.0800 80.0000 29.1600 28.2672

29.5676 39,8150 34222,6101 1081390,57

0.0124 1,77E-06 1,9098

0.0041 5.93E.07 0.6408

99.1521

73.7 31.95 10.721.63170

POINTS STACK T. DELTA P SQUAR D.P DELTA H deg

496 0.17 0.412311

0.72 2 494 0.]8 0,424264

0.77 3 465 0.23 0.479583

0.96 4 467 0.26 0.509902

1.10 5 468 0.28 0.52915

1.30 6 466 0.33 0,574456

1.50 7 467 0,37 0.608276

1.70 8 460 0.34 0.583095

L.55 9 457 0.31 0,556776

1,40 10 420 0,31 0,556776

1.50 11 420 0.26 0.509902

1,30 12 422 0.44 0.663325

2.10 13 464 •.18 0.424264

0.83 14 456 0.20 0.447214

0,93 15 454 0,21 0.458258

0.97 16 455 0.25

0.5 1.20 17 458 0,27 0.519615

1.20 18 455 0,32 0.565685

1,50 19 458 0.35 0.591608

1.60 20 456 0.32 0.565685

L.50 2I 425 0.33 0.574456

[.60 22 419 0.27 0.519615

1,30 23 419 0,27 0.519615

1.30 24 415 0.42 0,648074

2.10
451,5 0.5309 1.3304 METER T. NLET

949899 100 101102 103 104 104 105 105 ]05 104 ]05 106 107 108 108 108 108 ]09 109 !09 ]09

104.5833 METER T. OUTLET

94959595959596969798989999 IO0 IO0 IO0 IO0 IO0 101 101 102 103 103 !03

98,5417 METER T. AVERAGE

101 5625Appendix BSheet1
Summary of CO Analyzer

Calibrations

and Bias

Plant: Acme, Tulsa, OK Source: Tunnel Kiln Date: 9/6/02 Analyzer Calibratrion

Data Cylinder Value Zero Gas 0 Mid Range 99.4 High Range 199 Analyzer

Absolute

% Span Response Difference 2.3 2.3

0.92 103.58 4.18

1.672 194.55 -4.45

-1.78

Run #1

Run #2

Run #3 System Calibration

Bias and Drift Data Analyzer Initial Values

Final Values Calibration System

System

System

System Response Calibration

Calibration

Calibration

Calibration Response Bias

Response

Bias

Drift

Average Calibration Values

Zero Gas

2.3

1.5 -0.32

5.95

1.46

1.78

3.725 Upscale 103.58

94.25

-3.732

92.95

-4.252

-0.52

93.6 Average CO Concentration: Corrected CO Concentration: (Equation 6C-1 201.64 218.8901

Zero Gas

2.3

5.95

1.46

3.25

0.38

-1.08

4.6 Upscale 103.58

92.95

-4.252

93.3

-4.112

0.14 93.125 Average CO Concentration: Corrected CO Concentration: (Equation 6C-1 197.65 216.7655

1.58 91.625 Zero Gas

2.3

3.25 Upscale 103.58

93.3 Average CO Concentration: Corrected CO Concentration: (Equation 6C-1) 191.26 208.4588 2.415 92.4625

PageSheet1

Summary

of NOx Analyzer

Calibrations

and Bias

Plant: Acme, Tulsa, OK Source: Tunnel Kiln Date: 9/6/02 Analyzer Calibratrion

Data Cylinder

Analyzer

Absolute

% Span Value Response

Difference Zero Gas 0

0.2

0.2 0.333333 Mid Range 25.1

24.98

-0.12

-0.2 High Range 48.5

49.15

0.65 1.083333

Run #1

Run #2

Run #3 .System Calibration

Bias and Drift Data Analyzer Initial Values

Final Values Calibration System

System

System

System Response Calibration

Calibration

Calibration

Calibration Response Bias

Response

Bias

Zero Gas Upscale

0.2

0.2

0 1.03 1.383333 24.98 23.125

-3.09167

23.43 -2.58333 Average NOx Concentration: Corrected NOx Concentration: (Equation 6C-1 49.94 54.19493

Zero Gas

0.2

1.03 1.383333 Upscale 24.98

23.43 -2.58333 Drift

Average NOx Concentration: Corrected NOx Concentration: (Equation 6C-1 48.95 52.98213

Zero Gas

0.2

0.8 Upscale 24.98

23.55 -2.38333 1.383333 0.508333

Average NOx Concentration: Corrected NOx Concentration: (Equation 6C-1 46.8 51.33214 Average Calibration Values

0.615 23.2775

0.8 -0.38333

0.915 23.55 -2.38333

0.2 23.49

1.333333 0.333333 22.78 -3.66667

-1.28333

0.9 23.165

PageSheet1
Summary of Sulfur Dioxide Analyzer

Calibrations

and Bias

Plant: Acme Bricl, Tulsa, OK Source: Tunnel Kiln Date: 9/6/02 Analyzer Calibratrion

Data Cylinder

Analyzer

Absolute

% Span Value Response

Difference Zero Gas 0 -0.08

-0.08

-0.08 Mid Range 52.2

50.68

-1.52

-1.52 High Range 91

90,5

-0.5

-0.5

Run #1

Run #2

Run #3 System Calibration

Bias and Drift Data Analyzer Initial Values

Final Values Calibration System

System

System

System Response Calibration

Calibration

Calibration

Calibration Response Bias

Response

Bias

Drift

Average Calibratior. Valuas

Zero Gas

-0.08

0.1

0.18

0.13

0.21

0.03

0.115 Upscale 90.5

86.7

-3.8

86.72

-3.78

0,02

86.71 Average SO2 Concentration: Corrected SO2 Concentration: (Equation 6C-1 39.65 41.54611

-0.425 85.52 Zero Gas

-0,08

0.13 Upscale 90.5

86.72 Average SO2 Concentration: Corrected SO2 Concentration: (Equation 6C-1 0.21 -3.78

49.17 52.02298

Zero Gas

-0,08

-0.425

-0.345

-0.73

-0,65

-0.305

-0.5775 Upscale 90.5

85.52

-4.98

86.5

-4

0,98

86,01

49.18 52.2931z• Average SO2 Concentration: Corrected SO2 Concentration (Equation 6C-1 -0.1475 86.12

O Page _L9/56/02 Calibrations

Date/Time mm/dd/yy hh:mm:ss 0•/06/02 07:51:52 09106/02 07:52:02 09/06102 07:52:12 09/06/02 07:52:22 09/06/02 07:52:32 09/06/02 07:52:42 09106/02 07:52:52 09/06/02 07:53:02 09/06/02 07:53:12 09/06/02 07:53:22 09/06102 07:53:32 09/06/02 07:53:42 09106/02 07:53:52 09/06/02 07:54:02 09/0.6/02 07:54:12 09106/02 07:54:22 09/06/02 07:54:32 09/06/02 07:54:42 09/06/02,07:54:52 09/06102 07:55:02 09/06/02 07:55:12 09/06/02 07:55:22 09106/02 07:55:32 09/06/02 07:55:42 09106/02 07:55:52 09/06102 07:56:02 09/06/02 07:56:12 09106/02 07:56:22 09106/02 07:56:32 09/06/02 07:56:42 09106102 07:56:52 09/06/02 07:57:02 09/06/02 07:57:12 09/06/02 07:57:22 09106102 07:57:32 09/06/02 07:57:42 09/06/02 07:57:52 09/06]02 07:58:02 09/06102 07:58:12 09/06/02 07:58:22 09/06/02 07:58:32 09/06/02 07:58:42 09/06102 07:58:52 09106102 07:59:02 09/06/02 07:59:12 09/06/02 07:59:22 09]06/02 07:59:32 09/06/02 07:59:42 09/06/02 07:59:52 09/06/02 08:00:02 09/06/02 08:00:12 09/06/02 08:00:22 09/06/02 08:00:32 09/06•02 08:00:42 09/06102 08:00:52 09/06/02 08:01:02 09/06]02 08:01:12 09106102 08:01:22 09/06/02 08:01:32 09106/02 08:01:42 09106/02 08:01:52 09/06L02 08:02:02 09/06/02 08:02:12 09/06/02 08;02:22 09/06/02 08:02:32 09/06/02 08:02:42 09/06/02 08:02:52 09/06/02 08:03:02 09/06/02 08:03:12 09/06/02 08:03:22

VOC ppm COppm -0.1 -0,1 -0.1

-0.1

-0.1 -0.1 -0,1 -0.1 -0,1 -0.1 =0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.1 -0.10.0 2.7 0.0 2.6 0.0 2.6 0.0 2.5 0.0 2.5 0.0 2.6 -0.1 2.4 -0.1 2.4 -0,1 2.4 -0.1 2.5 -0.1 2.4 -0.1 2.5 -0.1 2.3 0,0 2.4 -0.1 2.3 -0.1 2.2 -0.1 2.2 0.0 2.2 0.0 2.2 0.0 2.3 0.0 2.1 0.0 2.1 0.0 2.1 0.0 2.1 -0.1 2.2 -0.1 2.1 -0.1 2.2 -0.1 2.3 -0.1 2.3 0.0 2.3 -0.1 2.3 =0,1 2.3 -0.1 2.1 =0.1 2,3 -0.1 2.3 -0.1 2,3 -0.1 2.3 -0.1 2.5 -0.1 2.4 -0.1 2.5 -0.1 2.7 -0.1 2.7 SO2 ppm 6.16.0

6.4 26.1
3.2
2.9 2.92.9 3.1:3.0 3.03.03,13.13.13.02.92,82.6 2.62.7 2.62.72.72•62.7 NOx ppm -0.1 0.1 -0.1 0,1 -0.1 0.2 -0,1 0.2

o.o 0.2

o.o 0.2

o.o 0.2

o.o 0.2 0.0 0.2 0.0 0,1 -0.1 0.1 -0.1 0.2 0.0 0.1 0.0 0.2 -0.1 0.7 0.0 4.1 0.0 9.0 -0.1 14.0 -0.1 18.9 0,0 23.3 0.0 26.9 0.0 30.4 0.0 33.1 -0.1 35.6 0.0 37.7 0.0 39.3 0.0 40.7 -0.1 41.9 0.0 42.9 -0.1 43.8 -0.1 44.4 0.0 45,0 0.0 45.5 -0.1 46.0 -0.1 46.3 -0.1 46.5 -0,1 46.8 0.0 47.0 0.0 47,2 -0.1 47.3 -0.1 47.4 -0.1 47.4 0.0 47.5 0.0 47.5 -0.1 47.7 -0.1 47.8 -0.1 47,9 -0.'1 47.9 -0.'1 48.0 -0.1 48.2 -0.1 48.3 -0,1 48.3 0.0 48.5 -0.1 48.6 -0.1 48.6 -0.1 48.8 0.0 48.8 -0.1 49.0 0.0 49.1
0.0 49.2
0.0 49.3
0.0 49.0 0.0 47.5 0.0 45.1 0.0 42.1 0.0 38.3 0.0 33.6 0.0 28.1 -0.1 22.5 0.0 18,4

Zero NOx

48.7 ppm NOx

Page9/56/02 Calibrations

09/06/02 08:03:32

-0.1 2.7 0.0 18.3 09/06/02 08:03:42

-0.1 2.7 0.0 19.1 09/06/02 08:03:52

-0.1 2.7 0,0 19,9 09/06/02 08:04:02

-0.1 2.6 0.0 20.6 09/06/02 08:04:12

-0.1 2.6 0.0 21,3 09/06/02 08:04 22

-0.1 2.7 -0.1 21.9 09/06/02 08:04:32

-0.1 2.6 -0,1 22.5 09/06/02 08:04:42

-0.1 2.6 -0.1 22.8 09/06/02 08:04:52

-0.1 2,6 -0,1 23.2 09/06/02 08:05:02

-0.1 2,7 0.0 23.5 09/06/02 08:05:12

-0.1 2.8 0.0 23,9 09/06/02 08:05:22

-0.1 2.8 0.0 24.2 09/06/02 08:05:32

-0.1 2.9 0.0 24.3 09/06/02 08:05:42

o0.1 2.7 0.0 24.5 09/06/02 08:05:52

-0.1 2.6 0.0 24.6 09/06/02 08:06:02

-0.1 2.6 0.0 24.7 09/06/02 08:06:12

-0.1 2.5 0.0 24.9 09106/02 08:06:22

-0.1 2.5 -0.1 24.9 09/06/02 08:06:32

-0.1 2,3 -0.1 25.0 09/06/02 08:06:42

-0.1 2.3 -0.1 25.0 09/06/02 08:06:52

-0.1 2.1 0.0 25.0 09/06/02 08:07:02

-0.1 2.1 0.0 24.5 09/06/02.08:07:12 -0.1 2.2 -0.1 23.4 09/06/02 08:07:22

-0.1 2.1 -0.1 21.9 09/06/02 08:07:32

-0.1 2.3 -0.1 19.5 09/06102 08:07:42

-0.1 2.2 0.0 16.1 09/06/02 08:07:52

-0.1 2.5 0.0 12.5 09/06/02 08:08:02

-0.1 2.6 -0.1 9.7 09/06/02 08:08:12

-0.1 2.7 -0.1 7.8 09/06/02 08:08:22

-0.1 2.8 0.0 6.1 09/06/02 08:08:32

-0.1 3.0 1.2 4.6 09/06/02 08:08:42

-0,1 3.0 5. 3.9 09/06/02 08:08:52

-0.1 2.8 9.9 3.4 09/06/02 08:09:02

-0.1 2.8 14.7 3.0 09/06/02 08:09:12

-0.1 2.6 19.2 2.5 09]06/02 08:09:22

-0.1 2.8 23.3 2.2 09/06/02 08:09:32

-0.1 2.7 27.2 1.9 09/06/02 08:09:42

-0.1 2.7 30.7 1.6 09/06/02 08;09:52

-0.1 2.6 33.8 1.5 09/06/02 08:10:02

-0.1 2.7 36.4 1.3 09/06/02 08:10:12

-0.1 2.5 38.7 1.2 09/06/02 08:10:22

-0.1 2.6 40.6 1.0 09/06/02 08:10:32

-0,1 2.6 42.1 0,9 09/06/02 08:10:42

-0.1 2.6 43.3 0.8 09/06/02 08:10:52

-0.1 2.6 44.5 0.8 09/06/02 08:11:02

-0.1 2.5 45.5 0.7 09/06/02 08:11:12

-0.1 2.5 46.2 0.6 09/06/02 08:11:22

-0.1 2.5 46.7 0.6 09/06/02 08:11:32

-0.1 2.6 47.2 0.6 09/06/02 08:11:42

-0.1 2.5 47.8 0.6 09/06/02 08:11:52

-0.1 2.5 48,1 0.6 09106/02 08:12:02

-0.1 2.6 48.4 0.5 09/06/02 08:12:12

-0.1 2.5 48.6 0.5 09/06/02 08:12:22

-0.1 2.5 48.9 0.4 09/06/02 08:12:32

-0.1 2.5 49.1 0.5 09/06/02 08:12:42

-0.1 2.4 49.3 0.4 09/06/02 08:12:52

-0.1 2.3 49.3 0,4 09/06/02 08:13:02

-0,1 2.3 49.4 0.4 09/06/02 08:13:12

-0.1 2.3 49,6 0.4 09/06/02 08:13:22

-0. 2,2 49,7 0.4 09/06/02 08:13:32

-0.1 2.2 49.8 0.4 09/06/02 08:13;42

-0.1 2,1 49.8 0.4 09/06/02 08:13:52

-0.1 2.1 49.8 0.3 09/06/02 08:14:02

-0.1 2.1 49.9 0.4 09/06/02 08:14:12

-0.1 2.2 50.0 0.3 09/06/02 08:14:22

-0.1 2.2 50.0 0.3 09/06/02 08:14:32

-0.1 2.1 50.1 0.3 09/06/02 08:14:42

-0.1 2.3 50.1 0.3 09/06/02 08:14:52

-0.1 2.2 50.2 0.3 09/06/02 08:15:02

-0.1 2.3 50.3 0.4 09/06/02 08:15:12

-0.1 2.2 50.3 0.3 09/06/02 08:15:22

-0.1 2,3 50.3 0.3 09/06/02 08:15:32

-0,1 2.1 50.4 0.3

25.1 ppm NOx Zero CO, $029/56/02 Calibrations

09/06/02 08:15:42 09/06/02 08:15:52 09/06/0:2 08:16:02 09/06/02 06:16:12 09/06/02 08:16:22 09/06/02 08:16:32 09/06/02 08:16:42 09/06/02 08:16:52 09/06/02 08:17:02 09/06/02 08:17:12 09/06/02 08:17:22 09/06/02 08:17:32 09106/02 08:17:42 09/06/02 08:17:52 09/06/02 08:18:02 09/06/02 08:18:12 09/06/02 08:18:22 09/06/02 06;18:32 09/06/02 08:18:42 09/06/02 08:I8:52 09/06102 08:19:02 09/06/02 08:19:12 09/06/02 08:19:22 09/06/02 08:19:32 09106/02 08:19:42 -09106/02 08:19:52 09/06/02 08:20:02 09/06/02 08:20:12 09/06/02 08:20:22 09/06/02 08:20:32 09/06/02 08:20:42 09/06/02 08:20:52 09/06/02 08:21:02 09/06/02 08:21:12 09/06/02 08:21:22 09/06/02 08:21:32 09/06/02 08:21:42 09/06/02 08:21:52 09/06/02 08:22:02 09/06/02 08:22;12 09/06/02 08:22:22 09/06/02 08:22:32 09/06/02 08:22:42 09106/02 06:22:52 09/06/02 08:23:02 09/06/02 06:23:12 09/06/02 08:23:22 09/06/02 08:23:32 09/06/02 08:23:42 09]06/02 08:23:52 09/06/02 08:24:02 09/06/02 08:24:12 09/06/02 08:24:22 09/06/02 08:24:32 09/06/02 08•24:42 09/06/02 08:24:52 09/06/02 08:25:02 09/06/02 08:25:12 09/06/02 08:25:22 09/06/02 08:25:32 09/06/02 08:25:42 09/06/02 08:25:52 09/06/02 08:26:02 09/06/02 08:26:12 09/06/02 08:26:22 09/06/02 08:26:32 09/06/02 08:26:42 09/06/02 08:26:52 09/06/02 08:27:02 09/06/02 08:27:12 09/06/02 08:27:22 09/06/02 08:27:32

-0.1 2.1 50.4 -0.1 2.2 50.4 -0.t 2.3 50.6 -0.1 2.2 50.6 -0.1 2.2 50,7
-0.1 2.4 50.6 -0.1 2.4 49.7 -0.1 2.7 48.1 -0,1 2.8 45.2 -0.1 2.9 41.1 o0.1 3.1 35.6 -0.1 3.2 29.9 -0.1 3.2 28.9 -0.1 3.2 33.9 -0.1 3,1 41.1 -0.1 2.9 48.1 -0.1 2.7 54.4 -0.1 2.6 59.9 -0.1 2.4 64.8 -0.1 2.3 69.1 -0.1 2.3 72.8 -0.1 2.3 75.5 -0.1 2.2 77,9 -0.1 2.2 80.1 -0.1 2.4 81.8 -0.1 2.4 83.4 -0.1 2.4 84.5 -0.1 2.4 85.3 -0.I 2.5 86.2 -0.1 2.4 87.0 -0.1 2.4 87.6 -0.1 2.4 87.9 -0.1 2.5 88.2 -0.1 2.3 88.6 -0,1 2.6 88.8 -0.1 2.5 89.0 -0.1 2.4 89.3 -0.1 2.6 89.5 -0.1 2.5 89.6 -0.1 2.5 89.8 -0,1 2.6 90.0 -0.1 2.7 90.0 -0.1 2.7 90.2 -0,1 2.7 90.3 -0.1 2.7 90.4 -0.1 2.7 90.5 -0.1 2.7 90.5 -0.1 2.7 90.5 -0.1 2,8 90.5 -0.1 2.7 90.4 -0,1 2.9 89.5 0.6 2.9 87.0 0.5 3,1 82.5 0.1 3.2 75.0 0.3 3.3 64.3 0.1 3.6 51.8 0,2 10,1 39.9 0.1 29.8 29.5 0.1 53,6 22.5 0,2 74.6 18.1 0.2 91,9 15,2 0.3 106.5 13.2 0.3 119.1 11.4 0.3 128.8 10.0 0.3 138.0

8.7 0.3 144.7

7.6 O.4 151.8

6.8 0.3 157.7

6.1 0.4 162,3

5,5 0.4 166.7

4,9 0.4 170.2

4,4 0.4 173.0

4,0

0.30.3
0.3 0.30.30.30.4 0.4 0.40.40.40.4 0.3 0.30.20.20.20.20,20.20.10.10.10.'10.'10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.1
0.10.10.10.10.10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.10.10.10,10.10.0

52.2 ppm S02

91 ppm S02

Page3 .• 1,1,1•9/56/02 Calibrations

09/06/02 08:27:42

0.4 175.2 09/06/02 08:27:52

0.4 176.5 09/06/02 08:28:02

0.3 177.7 09/06/02 08:28:12

0.4 179.t 09/06/02 08:28:22

0.4 160.2 09106/02 08:28:32

0.4 181 .I 09/06/02 08:28:42

0.4 181.6 09/06/02 06:28:52

0.5 182.3 09106/02 08:29:02

0.5 182.8 09/06/02 08:29:12

0.5 185,0 09/06/02 06:29:22

0.5 187.6 09/06/02 08:29:32

0.5 18•).1 09/06/02 08:29:42

0.5 189.3 09/06/02 08:29:52

0.5 194.8 09/06/02 08:30:02

0.5 190.0 09106/02 08:30:12

0.5 190.4 09/06/02 08:30:22

0.5 192.7 09/06/02 08:30:32

0.5 192.4 09/06/02 06:30:42

0.5 192.8 09/06/02 08:30:52

0.6 197,3 09/06/02 06:31:02

0.6 193.0 09/06/02 08:31:12

0.5 192.9 09/06/02 08:31:22

0.5 194.1 09106/02 08:31:32

0.5 193.5 09106/02 08:31:42

0.5 193,5 09/06/02 08:31:52

0.5 193.5 09106/02 08:32:02

0.5 193.7 09/06/02 08:32:12

0.6 201.3 09/06/02 08:32:22

0.6 193.8 09/06/02 08:32:32

0.5 194.0 09/06/02 06:32:42

0.6 194.0 09/06/02 08:32:52

0,6 194.1 09/06/02 06:33:02

0.7 194.3 09/06/02 08:33:12

0.5 194.4 09/06/02 08:33:22

0.5 194.5 09/06/02 06:33:32

-0.1 194.7 09/06/02 08:33:42

0.4 194.6 09/06/02 08:33:52

0.6 194.2 09/06/02 08;34:02

0.6 191.9 09/06/02 08:34:12

0.6 185,4 09/06/02 08:34:22

0.6 173.4 09/06/02 08:34:32

0.6 151.8 09/06/02 08:34:42

0.6 123.0 09/06/02 08:34:52

0.7 100.0 09/06/02 08:35:02

0.6 92.1 09/06/02 08:35:12

0.7 91.5 09/06/02 08:35:22

0,7 92.8 09/06/02 08:35:32

0.7 94,0 09/06/02 08:35:42

0.7 95.5 09/06/02 08:35:52

0.7 96.8 09/06/02 08:36:02

0.7 97.9 09/06/02 08:36:12

0.7 99.0 09/06/02 06:36:22

0,7 99.3 09/06/02 08:36:32

0.7 100.6 09/06/02 08:36:42

0.7 100.9 09/06/02 08:36:52

0.7 101.5 09/06/02 08:37:02

0.7 102.0 09/06/02 08:37:12

0.8 102.4 09/06102 08:37:22

0.8 102.6 09/06/02 08:37:32

0.8 102.9 09/06/02 08:37:42

0.8 103.2 09/06/02 08:37:52

0.8 103.1 09/06/02 08:38:02

0.8 103.3 09/06/02 06:38:12

0,8 103.4 09/06/02 06:38:22

0.8 103.4 09/06/02 08:38:32

0.8 03.,• 09/06/02 08:38:42

0.8 103,6 09/06/02 08:38:52

0.8 103.5 09/06/02 08:39:02

0.8 1 03.5 09/06/02 08:39:12

0.8 103.4 09/06/02 08:39:22

0.8 103.3 09/06/02 08:39:32

0.8 103.4

3.7 0.0 3.5 0.0 3.2 0.0 3.0 0.0 2.9 0.1 2.8 0.0 2.6 0.1 2.5 0.0 2.5 0.0 2.4 0.'1 2.2 0.0 2.2 0.1 2.1 0.1 2.1 0.1 2.0 0.1 2.0 0.1 2.0 0.0 2,0 0.0 1.9 0.1 1.8 0.0 1.8 0.1 1.8 0.0 1,8 0.1 1.7 0.1 1.7 0.1 1.7 0.1 1.7 0.1 1.8 0.0 1.8 0.1 1.7 0.'1 1.6 0.1 1.6 0.1 1.5 0,1 1.5 0.0 1,5 0.0 1.5 0.1 1.6 0.1 1.5 0.1 1.6 0.1 1,6 0.1 1.9 0.1 2.3 0.1 2.5 0.1 2.5 0.1 2,2 0.1 2.0 0.1 1.8 0,0 1.6 0.0 1.3 0.1 1.1 0.0 1.1 0.1 1.0 0.0 0.9 0.1 0.8 0.1 0.7 0.0 0.7 0.0 0.6 0.1 0.5 0.1 0.5 0.1 0.4 0.1 0.5 0.1 0.5 0.0 0.5 0.1 0,4 0.1 0.4 0.1 0.4 0.1 0.4 0.0 0.3 0.0 0.4 0.1 0.5 0.1 0.4 0.1 0.4 0.1

199 ppm CO

99.4 ppm CO

Page4 ,,•L t•9/56/02 Calibrations

09/06/02 08:39:42

0.8 103.5

0.4 0.1 09/06/02 08:39:52

0.8 103.2

0.3 0.0 09/06/02 08:40:02

0.8 103.2

0.3 0.1 09/06/02 08:40:12

0.0 103.1

0.4 0.1 09/06/02 08:40:22

-0.1 103.0

0.4 0.1 09/06/02 08:40:32

-0.1 102.7

0.3 0.0 09/06/02 08:40:42

-0.1 101.7

0.3 0.0 09/06/02 08:40:52

0.6 99.3 0.3 0.0 09/06/02 08:41:02

0.7 94.9 0,4 0.0 09/06/02 08141:12

0.7 88.1 0.6 0.1 09/06/02 08:41:22

0.8 81.1 0.6 0.1 09/06/02 08:41:32

0.8 77.2 0.7 0.1 09/06102 08:41:42

0,8 75.8 0.7 0.1 09/06/02 08:41:52

0,8 74.3 0.7 0.1 09/06/02 08:42:02

0.8 71.7 0.7 0,0 09/06/02 08:42:12

0.8 67.6 0.8 0.1 09/06/02 08:42:22

0.9 60.0 0.8 0.1 09/06/02 08:42:32

0.8 51.3 0.7 0.1 09/06/02 08:42:42

0.8 42.3 0,7 0.1 09/06/02 08:42:52

0.8 35.4 0.7 0.1 09/06/02 08:43:02

0.8 30.6 0.6 0.1 09/06/02 08:43:12

0.7 26.5 0.6 0.1 09106/02 08:43:22

-0.1 22.9 0,6 0.1 09/06/02 08:43:32

-0.1 20.2 0.5 0.1 09/06/02 08:43:42

-0.1 18.0 0.5 0.1 09/06/02 08:43:52

-0.1 16.1 0.5 1.6 09/06/02 08:44:02

-0.1 13.7 0.4 4.2 09/06/02 08:44:12

-0.1 11.9 0.3 6.8 09/06/02 08:44:22

-0.1 10.5 0.3 9.2 09/06/02 08:44:32

-0.1 9.2 0.2 11.3 09/06/02 08:44:42

o0.1 8.4 0.2 13.2 09/06/02 08:44:52

-0.1 7.5 0.2 14.8 09/06/02 08;45:02

-0.1 6.7 0.1 16.3 09/06/02 08:45:12

-0.1 6.0 0.1 17.5 09/06/02 08:45:22

-0.1 5.7 0.1 18.5 09/06/02 08:45:32

-0.1 5.1 O. 19.3 09/06/02 08:45:42

-0.1 4.8 0.1 20,0 09/06/02 08:45:52

-0.1 4.3 0,1 20.7 09/06/02 08:46:02

-0.1 4,1 0.1 21.1 09/06/02 08:46:12

-0.1 3.6 0.1 21.5 09/06/02"08:46:22 -0.1 4.0 0.t 21.9 09/06/02 08:46:32

-0.1 3,8 0.1 22,2 09106102 08:46:42

-0.1 3.5 0.1 22,4 09/06/02 08:46:52

-0,1 3.5 0.1 22.6 09/06102 08:47:02

-0.1 3.4 0.1 22:6 09/06/02 08:47:12

-0.1 3.3 0.1 22.7 09/06/02 08:47:22

-0.1 3.2 0.1 22.9 09/06/02 08:47:32

-0.1 3.1 0.1 22.9 09/06/02 08:47:42

-0.1 3.2 0.1 23.0 09/06/02 08:47:52

-0.1 3.1 0.1 23.0 09/06/02 08:48:02

-0.1 3.1 0.1 23.0 09/06/02 08:48:12

-0,1 3,0 0,1 23.1 09/06/02 08:48:22

-0.1 2.9 0.1 23.2 09/06/02 08:48:32

-0.1 3.1 0.1 23.2 09106/02.08:48:42 0.0 3.0 0.1 23.0 09/06/02 08:48:52

O. 2.9 O. 23.0 09/06/02 08:49:02

-0.1 3.1 0,0 23.1 09/06/02 08:49:12

-0.1 2,6 0.0 23.1 09/06/02 08:49:22

-0,1 2.7 0.1 23.1 09/06/02 08:49:32

-0.1 3.0 0.0 22.7 09/06/02 08:49:42

-0.1 4.8 0,0 21.0 09/06/02 08:49:52

-0.1 11.8 0.1 17.6 09/06/02 08:50:02

-0.1 23.6 0.0 13.5 09/06/02 08:50:12

-0.1 37.0 0.0 10.6 09/05/02 08:50:22

-0.1 48.1 0.1 8.6 09/06/02 08:50:32

-0.1 56.2 0.0 6.7 09/06/02 08:50:42

-0,1 63.2 0,0 5.5 09/06/02 08:50:52

-0.1 68.5 0.1 4.4 09/06/02 08:51:02

-0.1 72.2 0.1 3.6 09/06/02 08:51:12

-0.1 75,8 0,1 3.0 09/06/02 08:51:22

-0.1 78.7 0.0 2.4 09/06/02 08:61:32

-0.1 81.2 0.0 1.9 09/06/02 08:51:42

-0.1 82.9 0.0 1.6

25.1 ppm NOx Bias Zero VOC, CO, SO2 Bias

Page 59/56/02 Calibrations

09/06/02 08:51:52 09/06/02 08:52:02 09/06/02 08:52:12 09106/02 08:52:22 09/06/02 08:52:32 09/06102 08:52:42 09/06/02 08:52:52 09/06/02 08:53:02 06/06/02 08:53:12 09/06/02 08:53:22 09/06/02 08:53:32 09/06/02 08:53:42 09/06/02 08:53:52 09/06/02 08:54:02 09/06/02 08:54:12 09/06/02 08:54:22 09/06/02 08:54:32 09/06/02 08:54:42 09/06/02 08:54:52 06/06/02 08:55:02 09/06/02 08:55:12 09/06/02 08:55:22 09/06102 08:55:32 09/06/02 08:55:42 09/06/02 08:55:52 09/06/02 08:56:02 09/06/02 08:56:12 09/06/02 08:56:22 09/06/02 08:56:32 09/06/02 08:56:42 09/06/02 08:56:52 09/06/02 08:57:02 09/06/02 08:57:12 09/06/02 08:57:22 09/06/02 08:57:32 09/06/02 08:57:42 09/06/02 08:57:62 09/06/02 08:58:02 09/06/02 08:58:12 09/06102 08:58:22 09/06102 08:58:32 09/06/02 08:58:42 09/06/02 08:58:52 09/06/02 08:59:02 09/06102 08:59:12 09/06/02 08:59:22 09/06/02 08:59:32 09/06/02 08:59:42 09/06102 08:59:52 09/06/02 09:00:02 09/06/02 09:00:12 09/06/02 09:00:22 09/06/02 09:00:32 09/06/02 09:00:42 09/06/02 09:00:52 09/06/02 09:01:02 09/06/02 09:01:12 09/06/02 09:01:22 09/06102 09:01:32 09/06/02 09:01:42' 09/06/02 09:01:52 09/06/02 09:02:02 09/06/02 09:02:12 09/06/02 09:02:22 09/06/02 09:02:32 09/06/02 09:02:42 09/06/02 09:02:52 09/06/02 09:03:02 09/06/02 09:03:12 09/06/02 09:03:22 09/06/02 09:03:32 09/06/02 09:03:42

-0.1 84.1 0.0 1.4 -0.1 85.1 0.1 1.2 -0.1 85.8 0.1 1.0 -0.1 86.2 0.0 1.0 -0.1 86.6 0.0 0.9 -0.1 88.0 0.0 0.9 -t3.1 89.1 0.0 0.8 -0.1 90.4 0,0 0.7 -0.I 91.4 0.0 0.7 -0.1 92.6 0.0 0.7 -0.1 93.6 0.0 0.7 -0.1 93.6 -0.1 0,6 0.0 93.7 -0.1 0.6 -0.1 94.0 -0.1 0.6 -0.1 95.0 -0.1 0.6 -0.1 94.1 -0.1 0.6 -0.t 93.9

0.0 0.6 -0.1 94.5 1.0 0.7 -0.1 84.2 5.7 0.7 -0.1 62.3 14.3 0.7 -0.1 51.4 23.8 0.6 -0.1 42.0 33.1 0.6 -0.1 34.5 41.0 0.6 -0.1 28.3 47,8 0.5 -0.1 22.8 54.0 0.5 -0.1 18.8 59.0 0.4 -0.1 16,5 62.9 0.4 -0,1 14.1 66.2 0.4 -0.1 12.0 68.8 0.4 -0.1 10.8 70.9 0.4 -0.1 9.7 72.7 0.4 -0.1 8.7 74.1 0.3 -0.1 8.1 75.2 0.3 -0.1 7.8 76.2 0.3 -0.1 7.3 77.1 0.3 -0,1 7.1 77.5 0.3 -0.1 6.8 78.1 0.3 -0.1 6.7 78.5 0.3 -0.1 6.4 78.9 0.3 -0.1 6.3 79.4 0.3 -0.1 6.3 79,6 0.3 -0.1 6.3 79.8 0.3 -0.1 6.2 80,0 0.3 -0.1 6.2 80.2 0.2 -0.1 6.2 80.5 0.3 -0.1 6.0 80.8 0.2 -0.1 6.1 81.1 0.2 -0.1 6.0 81.2 0.2 -0,1 5.9 81.2 0.2 -0.1 6.0 61.4 0.2 -0.1 5.9 81.7 0.2 -0.1 5.9 82.2 0.2 •0.1 5.6 82.8 0.2 -0.1 5.5 83,4 0.2 -0.1 5.1 84.1 0.2 -0.1 4.8 84.6 0.2 -0,1 4.8 85.0 0.2 -0.1 4.8 85,5 0.2 -0.1 4.8 86.0 0.2 -0.1 4.9 86.3 0.2 -0.1 4.9 86.5 0,2 -0,1 4.9 86.8 0.2 -0.1 4.9 86.9 0,2 -0.1 5.0 87.0 0.2 9.4 5,1 86.7 0.2 20.O 4.9 86.6 0.2 20.3 5.0 86,8

0.2 23.1 4.9 86.7

0,2 35,5 4.9 86.8 0.2 36.9 4.9 86.5 0,2 36.3 5.0 85.3 0.2 36.2 5.2 82.6 0.2

99.4 ppm CO Bias

91 ppm S02 Bias Zero NOx Bias

Page 69/56/02 Calibrations

09/06/02 09:03:52 09106102 09:04:02 09106/02 09:04:12 09/06/02 09:04:22 09/06/02 09:04:32 09/06/02 09:04:42 09/06/02 09:04:52 09/06/02 09:05:02 09/06/02 09:05:12 09/06/02 09:05:22 09/06/02 09:05:32 09/06/02 09;05:42 09/06/02 09:05:52 09/06/02 09:06:02 09/06/02 09:06:12 09/06/02 09:06:22 09/06/02 09:06:32 09/06/02 09:06:42 09/06/02 09:06:52 09/06/02 09:07:02 09/06/02 09:07:12 09/06/02 09:07:22 09/06/02 09:07:32 09/06/02 09:07:42 09/06/02 09:07:52 09/06/02 09:08:02 09/06/02 09:08:12 09/06/02 09:08:22 09/06/02 09:08:32 09/06/02 09:08:42 09/06/02 09:08:52

36.3 35.7 29.5 29.6 29.6 29.6 29.6 20.52.11.91.8 33.8 51.7 52.4 52.6 52.5 52.5 26,12.3 2,01.9 11.9 14.0 14.1 14.2 14.2 14,2 14.2 14,27.01.9 5.5 5.8 5.9 5.95.6 5.45.14.9 4.8 4.74.6 4.54.3 4.5
4.34.24.24.0 3.8 3.63.43.23.23.2 3.2 3,53,6
3.63.63.6 3.5 77.4 69.5 59.5 48.9
40.0 33,2 28.0 23.9 20.5 17.7 15.5 13.6 11.8 10.69.78.9
8.27.4 6.8 6.45.5 5.14.8 4.4 4.13.83.6
3.43.22,9 2,7 0.30.30.30.20.30.2
0.20.20.20.10.10,10.20.2
0.20.2
0.20,10.10.10.10.10.10.40.1
0.10.10.10.10.10.1

29.6 ppm C3H8

50.3 ppm C3H8

14.7 ppm C3H8

Page7916101 Run #I

Date/Time VOC CO $02 NOx mm/dd/yy hh:mm:ss ppm ppm ppm ppm 09/06/02 09:16:42

17.5 185.2

0.0 49.3 09/06/02 09:16:52

t7.3 186.9

0.0 49.8 (•9106/02 09:17:02

17.3 189.2 -0.1 50.0 09/06/02 09:17:12

17.1 190.7

-0.1 50.3 09/06/02 09:17:22

17.1 192.3

-0.1 50.5 09/06/02 09:17:32

17.1 193.2

-0.1 50.6 09106/02 09:17:42

17.0 193,9

0.0 50,6 09/06/02 09:17:52

17.0 194.7

0.0 50.7 09/06/02 09:18:02

16.8 195.9

0.0 50.6 09/06/02 09:18:12

16.8 197.0

0.0 50.6 09/06/02 09:18:22

16.6 197.9

.0,1 50.6 09/06102 09:18:32

16.8 199.0

-0.1 50.6 09/06/02 09:18:42

16.7 199.7

-0.1 50.6 09/06/02 09:18:52

16.6 200.5

-0.1 50.6 09/06/02 09:19:02

16.6 201.1

0.0 50.5 09/06/02 09:19:12

16.6 201,6

0.0 50.6 09/06/02 09:19:22

16.6 202.1

0.0 50.6 09/06/02 09:19:32

15.8 202.4

0.0 50.6 09/06/02 09:19:42

16.1 202.8

0.1 50.6 09/06/02 09:19:52

16.6 203,2

0.1 50.7

Start Run #1 09/06f02 09:20:02

16.8 203.7

0.1 50.7 09/06/02 09:20:12

16.7 203.6

0.3 50.5 09/06/02 09:20:22

16.9 202.9

0.4 50.0 09/06/02 09:20:32

16.8 201.6

0.6 49.2 09106/02 09:20:42

16.8 199.8

0.7 48.6 09/06/02 09:20:52

16.9 198.1

0.8 47.9 09/06/02 09:21:02

16.9 196 6 1.0 47.4 09/06/02 09:2:1:12

16.9 195.3

1.1 46.9 09/06/02 09:21:22

17.0 194.3

1.2 46.5 09/06102 09:21:32

17.1 193.5

1.3 46.3 09/06/02 09:21:42

17.1 193.1

1.5 46.0 09/06/02 09:21:52

17.2 192.9

1.6 45.9 09/06/02 09:22:02

17.3 192.8

1.7 45.7 09/06/02 09:22:12

17.4 192.4

1.9 45.6 09106/02 09:22:22

17.2 192.1

2.1 45.6 09106/02 09:22:32

17.3 191.9

2.2 45.5 09/06/02 09:22:42

17.8 191.7

2.5 45.3 09/06/02 09:22:52

17.5 191.5

2.9 45.4 09/06/02 09:23:02

16.8 191.3

3.0 45.4 09/06102 09:23:12

16.7 191.0

3.2 45.3 09/06/02 09:23:22

16,7 191.3

3.4 45.4 09/06/02 09:23:32

16.8 192.3

3.6 45.7 09/06/02 09:23:42

16.9 193.3

3.7 46.3 09/06/02 09:23:52

16.8 194.6

4.0 47.0 09/06/02 09:24:02

16.8 196.1

4.5 47.5 09/06/02 09:24;12

16.8 197.6

5.'1 47.9 09/06/02 09:24:22

16.6 198.9

5.6 48.3 09/06/02 09:24:32

16.5 200.2

6.2 48.6 09/06/02 09:24:42

16.5 201.2

6.9 48.9 09/06/02 09:24:52

16.5. 202.1

7.4 49.1 09/06/02 09:25:02

16.5 202.9

8.1 49.2 09/06/02 09:25:12

16.3 203.4

8.8 49.4 09/06/02 09:25:22

16.2 203.7

9.5 49.6 09/06/02 09:25:32

16.3 204.0 10.2 49.8 09/06/02 09:25:42

16.2 204.3 10.7 49.8 09/06/02 09:25:52

16.5 204.6 11.2 49.8 09/06/02 09:26:02

16.4 204.9 11.7 49.9 09/06/02 09:26:12

16.4 204.9 12.2 50.0 09/06/02 09:26:22

16.5 205.0 12.8 50.0 09/06/02 09:26:32

16.4 205.1 13.4 50.2 09/06/02 09:26:42

16.3 205.2 13.9 50.2 09/06/02 09:26:52

16.3 205:5 14.5 50.2 09/06/02 09:27:02

16.4 205.6 15.1 50.3 09/06/02 09:27:12

16.4 205.7 15.6 50.3 09/06/02 09:27:22

16.5 205.7 16.2 50.4 09/06/02 09:27:32

16.3 205.8 16.9 50.4 09/06/02 09:27:42

16.4 205.9 17.5 60..4 09/06/02 09:27:52

16.3 206.2 18.0 50.5 09/06/02 09:28:02

15.6 206.1 18.6 50.5 09/05/02 09:28:12

15.8 206 0 19.2 50.5

Page9/6/01 Run #1

09106/02 09:28:22

16,1 206.2 19.5 50.6 09106102 09:28:32

16.0 206.1 19.8 50.5 09106/02 09:28:42

16.1 205.9 20.2 50.4 09/06/02 09:28:52

16.2 206,0 20.7 50.5 09/06102 09:29:02

15.8 205.9 21.0 50.5 09/06/02 09:29:12

14.8 205.9 21.3 50.5 09/06/02 09:29:22

15.3 206.1 21.9 50.6 09/06/02 09:29:32

15.5 206.1 22,5 50.6 09/06/02 09:29:42

15.4 205.9 22.9 50,6 09/06/02 09:29:52

15.5 206.0 23.5 50.6 09106102 09:30:02

15.8 206.1 24." 50.6 09/06/02 09:30:12

15.7 206.1 24.5 50.6 09/06/02 09:30:22

15.5 206.1 24.9 50.6 09/06/02 09:30:32

15.5 206.2 25.4 50.6 09/06/02 09:30:42

15.4 206.0 25.9 50.7 09/06/02 09:30:52

15.9 205.9 26.3 50.7 09/06/02 09:31:02

15.5 205.9 26.7 50.6 09/06/02 09:31:12

15.6 205.9 27.3 50.6 09/06/02 09:31:22

15.6 205.8 27.7 50.6 09/06/02 09:31:32

15.4 205.7 28.'1 50.7 09/06/02 09:31:42

15.4 205.8 28,=t 50.6 09/06/02 09:31:52

15.3 205.6 28.7 50.7 09/06/02 09:32:02

15.5 205.7 29.0 50.8 09/06/02 09:32:12

15,3 205,5 29.4 50.8 09/06/02 09:32:22

15.2 205.4 29.7 50.7 09/06/02 09:32:32

15,4 205.3 30.1 50.6 09/06/02 09:32:42

15.3 205.2 30.5 50,7 09/06/02 09:32:52

15.3 205.1 31.0 50.6 09/06/02 09:33:02

15.1 204.8 31.4 50.7 09]06/02 09:33:12

15.5 204.8 31.7 50.6 09106/02 09:33:22

15.3 204.5 31.9 50.6 09/06/02 09:33:32

15.4 204,4 32,3 50.6 09/06/02 09:33:42

15.5 204,3 32.6 50,7 09/06/0209:33:52 15.5 204,2 33.0 50.8 09/06/02 09:34:02

15.3 204.3 33.3 50.7 09/06102 09:34:12

15.1 204.4 33.7 50.7 09/06/02 09:34:22

15.6 204.5 34.0 50.7 09/06/02 09:34:32

15.5 204.6 34.3 50.7 09/06/02 09:34:42

15.2 204.5 34.6 50.7 09/06/02 09:34:52

15.5 204.6 34.8 50.7 09/06/0209:35:02 15.2 204.5 35.1 50.7 09/06/02 09:35:12

15.2 204.5 35.3 50.6 09/06/02 09:35:22

15.1 204.7 35.5 50.7 09/06/02 09:35:32

15,5 204,5 35.7 50.8 09/06/02 09:35:42

15.3 204.4 35.8 50.7 09/06/02 09:35:52

15,4 204.2 35.9 50.8 09/06/02 09:36:02

15.3 204.4 36.1 50,8 09/06/02 09:36:12

15.3 204.1 36.4 50.7 09/06/02 09:36:22

15.2 204.0 36.7 50.8 09/06/02 09:36:32

15.3 203.7 36.8 50.7 09/06/02 09:36:42

15.4 203.4 37.2 50.7 09/06/02 09:36:52

15,5 203.3 37.6 50.7 09/06102 09:37:02

15.5 203.1 37.9 50.7 09/06/02 09:37:12

15.5 202.7 38.2 50.6 09/06/02 09:37:22

15.4 202.6 38.4 50.6 09/06/02 09:37:32

15.3 202.6 38.6 50.6 09/06/02 09:37:42

15.3 202.6 38.7 50.5 09/06/02 09:37:52

15.2 202.5 38.9 50.6 09/06/02 09;38:02

15.0 202.4 39.1 50.6 09/06/02 09;38:12

14.9 202.5 39.4 50.6 09/06/02 09:38:22

14.5 202.4 39,5 50.6 09/06/02 09:38:32

14.7 202.3 39.7 50.6 09/06/02 09:38:42

14.8 202.0 39.7 50.6 09/06/02 09:38:52

15,0 201,6 39.9 50.5 09/06/02 09:39:02

15.1 201.7 40.0 50.6 09/06/02 09:39:12

15.2 201.5 40.1 50.6 09/06/02 09:39:22

15.0 201.8 40.3 50.6 09/06/02 09:39:32

15.0 201.7 40.4 50.6 09/06/02 09:39:42

15.3 201.6 40.5 50.5 09/06/02 09:39:52

15.0 201.6 40.6 50.6 09/06/02 09:40:02

15.0 201,4 40.8 50,5 09/06/02 09:40:12

15.2 201.1 40.9 50.5 09/06/02 09:40:22

15.0 200.9 41.0 50.4 09/06102 09:40:32

14.7 200.9 41.2 50.5

Page 29/6/01 Run #1

09/06/02 09:40:42 09/06/02 09:40:52 09/06/02 09:41:02 09/06/02 09:41:12 09/06/02 09:41:22 09/06/02 09:41:32 09/06/02 09:41:42 09106/02 09:41:52 09/06/02 09:42:02 09/06/02 09:42:12 09/06/02 09:42:22 09/06/02 09:42:32 09/06/02 09:42:42 09/06/02 09:42:52 09/06/02 09:43:02 09/06/02 09:43:12 09/06/02 09:43:22 09/06/02 09:43:32 09/06/02 09:43:42 09/06/02 09:43:52 09/06/02 09;44:02 09/06/02 09:44:12 09/06/02 09:44:22 09/06/02 09:44:32 09/06/02 09:44:42 09/06/02 09:44:52 09/06/02 09:45:02 09/06/02 09:45:12 09/06/02 09:45;22 09/06/02 09:45:32 09/06/02 09:45:42 09/06/02 09:45:52 09/06/02 09:46:02 09/06/02 09:46:12 09/06/02 09:46:22 09106/02 09:46:32 09/06/02 09:46:42 09/06/02 09:46:52 09/06/02 09:47:02 09/06]02 09:47:12 09/06/02 09:47:22 09/06/02 09:47:32 09/06/02 09:47:42 09/06/02 09:47:52 09/06/02 09:48:02 09/06/02 09:48:12 09/06/02 09:48:22 09/06/02 09:48:32 09/06/02 09:48:42 09/06/02 09:48:52 09/06/02 09;49:02 09/06/02 09:49:12 09/06/02 09:49:22 09/06/02 09:49:32 09/06/02 09:49:42 09/06/02 09:49:52 09/06/02 09:50:02 09/06/02 09:50:12 09/06/02 09:50:22 09/06/02 09:50:32 09/06/02 09:50:42 09/06/02 09:50:52 09/06/02 09:51:02 09/06/02 09:51:12 09/06/02 09:51:22 09/06/02 09:51:32 09/06/02 09:51:42 09/06/02 09:51:52 09/06/02 09:52:02 09/06/02 09:52:12 09/06/02 09:52:22 09/06/02 09:52:32 09/06/02 09:52:42 09/06/02 09:52:52

14.7 200.8 41.5 50.6 14.7 201.1 41.8 50.5 14.9 201.0 41.9 50.5 14.8 201.0 42.0 50.5 15.1 200.9 42.2 50.5 14.8 200.6 42.2 50.5 14.8 200.3 42.3 50.4 14.8 200.8 42.3 50.4 14.9 200,1 42.5 50.4 14.8 200.1 42.7 50.4 14.7 199.8 42.7 50.4 14.5 199.7 42.8 50.4 14,9 199.3 42,7 50.4 14.4 199.2 42.8 50.4 14.3 199.1 43.0 50.3 14.7 199.0 43.1 50.3 14.7 199.0 43.2 50.4 14.8 199.0 43.3 50.3 14.6 198.9 43.5 50.3 14.6 198.6 43.7 50.3 14.6 198.6 43.8 50.4 14.6 198.4 43.9 50.3 14.6 198,4 44.0 50.3 14.4 198,3 44.3 50.4 14.5 198.2 44.5 50.4 14.4 198,0 44.6 50.4 14.2 198.0 44.8 50.4 14,4 197.9 45.0 50.4 14.3 197.9 45.0 50.4 14.4 197.9 45.2 50.4 14.2 198.0 45,4 50.4 14.0 198.1 45.5 50.4 13.9 198.2 45.6 50.4 14.2 198.0 45.6 50.3 14.3 197.9 45.7 50.3 14,2 197.6 45.7 50.3 14.3 197.6 45.8 50.3 14.2 197.5 45,8 50.3 14.2 197.4 45.8 50.2 14.3 197.2 45.9 50.2 14.3 197.1 46.1 50.2 14.1 197.0 46.2 50.2 14,2 196.8 46.1 50.2 14.1 196.8 46.1 50.2 14.1 196.5 46.3 50.2 14.0 196.5 46.5 50.2 14.2 196.4 46.5 50.2 14.2 195.9 46.5 50.1 14.3 195.8 46.5 50.2 13.9 195.6 46.5 50.2 14.1 195.5 46.5 50.1 14,0 195.3 46.6 50.1 13.9 195.2 46.6 50.1 14.0 195.2 46.6 50.1 13.9 195.1 46.7 50.1 14.0 195.0 46.7 50.0 14.2 194.8 46.8 50.0 14.0 194.9 46.9 50.0 13.9 194.8 46.8 50.1 13.8 194.7 46.9 50.1 13.7 194.9 47.0 50.0 13.9 194.7 47,0 50.0 13.9 194.6 47.0 50.0 13.9 194.5 47.1 50.0 13,9 194.4 47.0 50.0 13.7 194.5 47.1 49.9 13.8 194.3 47.2 49.9 13.9 194.3 47.2 49.8 13.8 194,0 47.2 49.9 13.6 194.0 47.3 49.8 13.6 193,9 47.2 49,9 13.7 193.7 47.2 49.8 11.6 193.6 47.3 49.8 8.7 193.4 47.4 49.7

Page 3 239/6/0'] Run #1

09/06/02 09:53:02

8.7 193.4 09/06/02 09:53:12

9.0 193.•4 09/06/02 09:53:22

9,2 192.7 09/06/02 09:53:32

9.1 186.7 09/06/02 09:53:42

9.5 182.3 09/06102 09;53:52

11.6 176.2 09/06/02 09:54:02

14.6 171.3 09/06/02 09:54:12

15.7 166.6 09/06102 09:54:22

13.6 163.0 09/06102 09:54:32

11.3 160.5 09/06/02 09:54:42

17.7 158.7 09/06/02 09:54:52

21.0 157.0 09/06/02 09:55:02

21.2 154.0 09/06t02 09:55:12

150.9 09106/02 09:55:22

20.9 151.1 09/06/02 09:55:32

20.9 156.0 09/06/02 09:55:42

20•9 162.9 09/06/02 09:55:52

20.9 170.8 09/06/02 09:56:02

21.0 176.8 09/06/02 09:56:12

21.0 181.7 09/06/02 09:56:22

21.0 165.8 09/06/02 09:56:32

20.9 188.9 09/06/02 09:56:42

21.0 191.2 09/06/02 09:66:52

21.0 193.0 09/06/02 09:67:02

21.1 193.9 09/06102 09:57:12

21,1 195.1 09/06/02 09:57:22

20.8 196,2 09/06/02 09:57:32

20.8 09/06/02 09;57:42

20.8 198.0 09/06/02 09:57:52

20.8 198.8 09/06/02 09:58:02

20.8 199,4 09/06/02 09:58:12

20.9 200.0 09/06/02 09:58:22

20,9 200.9 09/06/02 09:58:32

20.9 202.0 09106/02 09:58:42

20.8 202.9 09106/02 09:58:52

20.8 204.0 09/06/02 09:59:02

20.7 205.0 09/06/02 09:59:12

20.7 205.9 09/06/02 09:59:22

20.4 206,5 09/06/02 09:59:32

20.7 207.0 09/06/02 09:59:42

20.7 207,5 09/06/02 09:59:52

20.8 207.6 09/06/02 10:00:02

20.8 208.2 09/06/02 10:00:12

20.8 208.4 09/06102 10:00:22

20.7 208.5 09/06/02 10:00:32

20.7 209.0 09/06/02 10:00:42

20.8 209.0 09/06/02 10:00:52

20.8 209.2 09/06/02 10:01:02

20.7 209.3 09/06/02 10:01:12

20.7 209.5 09/06/02 10:01:22

20.7 209.7 09/06/02 10:01:32

20.8 209.9 09/06/02 10:01:42

20.8 210.0 09/06/02 10:01:52

20.7 210.3 09/06/02 10:02:02

20.6 210.6 09/06/02 10:02:12

20.7 210,6 09/06/02 10:02:22

20.6 210,8 09/06/02 10:02:32

20.7 210.8 09/06/02 10:02:42

20.7 211.0 09/06/02 10:02:52

20.5 211.1 09/06/02 10:03:02

20.7 211.1 09/06/0210:03:12 20.6 211.3 09/06/02 10:03:22

20.7 211.2 09/06/02 10:03:32

20.6 211.3 09/06/02 10:03:42

20.6 211.3 09106/02 10:03:52

20.6 211,2 09/06/02 10:04:02

20.5 211.1 09/06/02 10:04:12

20,6 211.1 09/06/02 10:04:22

20.5 211.0 09706/02 10:04:32

20.5 211.0 09/06/02 10:04:42

20.4 210.9 09/06/02 10:04:52

20.5 211.0 09/06/02 10:05:02

20.3 211.1 09/06/02 10:05:12

20.0 211.1

47,6 47.6 47.5 47.3 46.3 44.6 42.5 40,5 38.6 37.0 35,6 34.7 33.8 32.9 32.2 31.8 32.0 33.1 34.8 36.7 38.6 40.2 41.8 42.7 43.6 44.5 45.1 45.6 46.0 46.5 46.8 47.1 47,4 47.6 47.8 48.0 48.2 48,3 48.5 48.7 48.9 49.0 49,2 49.3 49.3 49.4 49.6 49.8 49.9 50.0 50.0 50.1 50.2 50.1 50.2 50.4 50.5 50.6 50.7 50.8 50.9 50.9 51.0 51.1 51.2 51.3 51.3 51.3 51.4 51.4 51.4 51.4 51.4 51.7 49.8 49,8 49.0 47.2 45.7 44.6 43.7 42,9 42.3 41.9 41.3 40.7 40.0

40.0 41.4 42.9 44.3 45.4 46.1 46.7 47.2 47.4 47.7 47.9 48.1 48.3 48.5 48.7 48.8 48.9 49.0 49.1 49.3 49.5 49.7 49,9 50.0 50.1 50.3 50.4 50.5 50.5 50.7 50.6 50.7 50.8 50.8 50.9 50.8 50.9 50.9 50.9 50.9 51.0 51.0 51.0 51.1 51.1 51.1 51.2 51.2 51.3 51,3 51.2 61.3 51.2 51.2 51.2 51.3 51.2 51.3 51.3 51.3

Page 4916/01 Run #1

09/06/02 10:05:22

20,2 211.2 09/06/02 10:05:32

20,4 211.4 09/06/02 10:05:42

20,3 211.3 09106/02 10:05:52

20.1 211,2 •3/06/02 10;06:02

20.3 211.3 09/06/02 10:06:1'2

20.3 211.1 09106/02 10:06 22

20.3 211.2 09/06/02 10:06:32

20.1 211.1 09/06/02 10:06:42

20.0 211.1 09/06/02 10:06:52

20.0 211,0 09106/02 10:07:02

20.1 211.0 09/06102 10:07:12

19.9 210.9 09/06/02 10:07:22

19.9 210.9 09/06/02 10:07:32

19.9 210.8 09/06/02 10:07:42

20.0 210.9 09/06/02 10:07:52

20.0 210.8 09/06]02 10:08:02

20.0 210.9 09/06/02 10;08:12

19.9 210.9 09/06/02 10:08:22

19.8 210.8 09/06/02 10:06:32

19.8 210.8 09/06/02 10:08:42

19.9 210.9 09/06102 10:08:52

19.9 210.9 09/06]02 10:09:02

19.7 210.9 09/06]02 10:09:12

19.8 210,8 09/06/02 10:09:22

19.8 210.7 09/06/02 10:09:32

20.0 210.7 09/06/02 10:09:42

19.8 210.5 09/06/02 10:09:52

19.7 210.4 09106/02 10:10:02

19.8 210.3 09106/02 10:10:12

19.6 209,9 09/06102 10:10:22

19.6 210.0 09/06/02 10:10:32

19.7 209.8 09]06/02 10:10:42

19.6 209.6 09/06/02 10:10:52

19.3 209.5 09/06/02 10:11:02

19.4 209.3 09/06/02 10:11:12

19.5 209.2 09/06/02 10:11:22

19.4 209.3 09/06/02 10:11:32

19.4 209.1 09/06/02 10:11:42

19.4 209.0 09/06/02 10:11:52

19.5 209.0 09]06/02 10:12:02

19.6 209.0 09/06/02 10:12:12

19.6 209.0 09/06/02 10:12:22

19.4 208.8 09/06102 10:12:32

19,3 208.9 09/06/02 10:12:42

19.4 208.9 09/06/02 10:12:52

19.4 208,8 09/06/02 10:13:02

19.4 208.8 09]06/02 10:13:12

19.4 208.6 09/06102 10:13:22

19.3 208.4 09/06/02 10:13:32

19,2 208,3 09106/02 10:13:42

19.2 208.2 09/06/02 10;13:52

19.2 208.0 09/06/02 10:14:02

19.2 206.0 09/06/02 10:14:12

19.2 208.0 09106/02 10:14:22

19.2 208.0 09/06/02 10:14:32

19.3 208.0 09/06/02 10:14;42

19.1 207,8 09/06/02 10:14:52

19.2 207,8 09106/02 10:15:02

19.1 207.7 09/06/02 10:15:12

19.1 207.9 09/06/02 10:15:22

19.0 207.8 09/06/02 10:15:32

19.0 207.5 09/06/02 10:15:42

18.9 207.5 09/06/02 10:15:52

19.2 207,5 09/06/02 10:16:02

19.3 207.5 09/06/02 10:16:12

19.1 207.2 09/06/02 10:16:22

19.1 207.0 09/06/02 10:16:32

19.1 206.7 09/06/02 10:16:42

19.0 206.6 09/06/02 10:16:52

18,9 206.4 09/06/02 10:17:02

19.0 206,2 09/06/02 10:17:12

18.9 205.1 09/06/02 10:17:22

18.9 205.6 09/06/02 10:17:32

18.9 205,5

51.7 51.3 51,7 51.3 51.8 51.3 51.8 51.3 51.9 51.3 51.9 51.4 51.9 51.3 51.8 51.3 51.9 51.3 51.9 51.3 51.9 51.3 51.9 51.3 51.9 51.4 52.0 51.2 52.1 51.3 52.1 51.3 52.1 51.3 52.1 51.2 52,2 51.1 52.2 51.2 52.2 51.3 52.1 51.2 52,2 51.2 52.1 51.2 52.1 51 .'1 52.1 51.1 52.2 51.1 52,2 51.1 52.2 51.1 52.'1 51.1 52.1 51.2 52.2 51.2 52.2 51.1 52.2 51 .'1 52.3 51.0 52.3 51.0 52.3 51.1 52.3 51.1 52,3 51.1 52,4 51,1 52.3 51.1 52.2 51.1 52.3 51.2 52.4 51.2 52.4 51.1 52.3 51.1 52.3 51.0 52.3 51.0 52.3 51.1 52.3 51.0 52.4 51.0 52.5 51.0 52.5 51,0 52.4 51.1 52.5 51.0 52.5 51.1 52.5 51.1 52.5 51.0 52.6 51.0 52.7 51.1 52.7 51.1 52.6 51.0 52,6 51.0 52.6 51.0 52.6 51.0 52.6 51.0 52.5 51.0 52.5 51.0 52.4 51 .o 52.5 51.0 52.5 51.0 52.4 51.0 52.5 51.0 52.5 50.9

Page 5 259/6/01 Run #1

09106/02 10:17:42

19.0 205.4 52.5 50,9 09106/02 10:17:52

18.8 205.5 52.5 50.9 09/06/02 !0:16:02

18.6 205.3 52.5 50.8 09/06/02 10:16;12

18.6 205.3 52.5 50.9 09/06/02 10:18:22

18.5 205.4 52.5 50.9 09/06102 10:18:32

18.6 205.4 52.5 50.9 09/06/02 10:16:42

18.5 205.3 52.6 50.6 09/06/02 10:18:52

18.4 205,2 52.6 50.6 09/06/02 10:19:02

18.5 204.7 52.5 50.9 09106/02 10:19:12

18.5 204.7 52.5 50.6 09/06/02 10:19:22

18.5 204.5 52.5 50.6 09/06/02 10:19:32

18.3 204.2 52•3 50.6 09106/02 10:19:42

18.2 204.2 52.2 50.6 09106102 10:19:52

16.2 204.3 52.0 50.7 09/06/02 10:20;02

18.3 204.4 52.0 50.6 09/06/02 10:20:12

18.2 204.4 51.9 50.6 09/06/02 10:20:22

16.1 204.3 52.0 50.6 09/06/02 10:20:32

18.2 204.3 62.0 50,7 09/06/02 10:20:42

18.0 204.1 52.1 50.7 09/06/02 10:20:52

18.9 203.9 52.4 50.8 09/06/02 10:21:02

18.4 203.6 52.5 50.8 09/06/02 10:21:12

18.6 203.5 52.5 50.8 09/06/02 10:21:22

18.3 203.5 52.7 50.8 09/06/02 10:21:32

18.2 203.5 52.7 50.8 09/06/02 10:21:42

18.2 203.2 52.7 50.8 09/06/02 10:21:52

18.1 203.1 52.6 50.8 Stop Run #1

17.14 201.64 39.65 49.94 09/06/02 10:22:02

17.9 203.1 52.6 50.8 09/06/02 10:22:12

17.9 202.9 52.6 50.8 09/06/02 10:22:22

15.4 203.1 52.5 50.8 09/06/02 10:22:32

5.7 201.3 52,5 50.4 09/06102 10:22:42

4.5 201.0 52.0 49.9 09/06/02 10:22:52

4.0 200.8 51.7 50,0 09/06/02 10:23:02

3.8 200.6 51.6 49.6 09/06/02 10:23:12

2.4 197.4 51.6 47.5 09/06/02 10:23:22

2,4 183.6 51.0 42.2 09/06/02 10:23:32

2.3 160.9 48.8 35.7 09/06/02 10:23:42

2.2 13•1 2 45.0 27.9 09/06/02 10;23:52

2.0 108.5 41.1 22.2 09/06/02 10:24:02

1.8 89.1 39.5 18.4 09/06/02 10:24:12

1.7 74.8 41.1 15.4 09/06/02 10:24:22

1.6 63.6 44.4 13.0 09/06/02 10:24:32

1.5 53.8 48.7 10.9 09/06/02 10:24:42

1.4 46.0 53.2 9.2 09/06/02 10:24:52

1.4 38.9 57.5 7.7 09/06/02 10:25:02

1.3 33.7 61.6 6.6 09/06/02 10:25:12

1.3 28.8 65.4 5.6 09/06/02 10:25:22

1,2 24.8 68.6 4.8 09/06/02 10:25:32

1.3 21.7 71,5 4.2 09/06/02 10:25:42

1.2 19.1 74.1 3.6 09/06/02 10:25:52

1.3 17.5 76.5 3.3 09/06/02 10:26:02

1.3 16.5 78.4 3,0 09/06/02 10:26:12

1.3 15.0 80.2 2.8 09/06/02 10:26:22

1.4 14.2 81.4 2.5 09/06102 10:26:32

1.4 13.5 82.6 2.4 09106/02 10:26:42

1.6 13.0 83.5 2.3 09/06/02 10:26:52

1.7 12.6 84,3 2.2 09/06/02 10:27:02

1.9 12.1 84.6 2.1 09/06/02 10:27:12

2.2 11.7 85.0 2.0 09/06/02 10:27:22

2.5 11.3 85.5 1.9 09/06/02 10:27:32

2.4 11,2 85.9 1.8 09/06/02 10:27:42

2.3 10.8 86.3 1.8 09/06/02 10:27:52

2.3 10.6 86.5 1.7 09/06/02 10:28:02

2.4 10.3 86,8 1.6 09/06/02 10:28:12

2.5 10.2 87.0 1.6 09/06/02 10:28:22

2.9 9.8 87.1 1,6 09/0,6/02 10:28:32

3.5 9.5 87.3 1.6 09/06/02 10:28:42

4.2 9.5 87.2 1:5 09/06/02 10:28:52

4.7 9.3 86.8

1.5 09/06/02 10:29:02

3.9 9.2 86.7

1.5 09/06/02 10;29:12

3.5 9.0 86.6

1.5

91 ppm SO2

Page 609/06/02

10:29:22

2.5 8.9 09/06/02 10:29:32

1,0 8.7 09/06/02 10:29:42

0.9 6.6 09/06/02 10:29:52

0.7 9.2 09/06/02 10:30:02

0,6 10.1 09106/02 10:30:12

0.6 11.7 09/06/02 10:30;22

0.6 12.8 09/06/02 10:30:32

0.6 12.8 09/06/02 10:30;42

0.6 12.3 09/06/02 10;30:52

0.6 11.5 09/06/02 10:31:02

0.6 10.6 09/06/02 10:31:12

0.6 10.3 09/06/02 t0:31:22

0,6 9.7 09/06/02 10:31:32

0.5 9.1 09/06/02 10:31:42

0,5 8.7 09/06102 10:31:52

0.5 8.3 09/06/02 10:32:02

0.5 7,9 09/06/02 10:32:12

0.5 7.6 09/06/02 10:32:2.2

0.5 7.4 09/06/02 10:32:32

0.5 7,1 09/06/02 10:32:42

0.5 6.9 09/06102 10:32:52

0,5 6.5 09/06/02 10:33:02

0.5 6.2 09/06/02 10:33:12

0.5 6.2 09/06/02 10:33:22

0.7 5.9 09/06/02 10:33:32

1.1 5.9 09/06/02 10:33:42

0.5 5.9 09/06/02 10:33:52

0.4 6.0 09/06/02 10:34:02

0.4 6.0 09/06/02 10:34:12

0.4 6.4 09/06/02 10:34:22

0.4 9.2 09/06/02 10:34:32

0.4 17.2 09/06/02 10:34:42

0.4 29.5 09/06/02 10:34:52

0.4 41.9 09/06/02 10:35:02

0.4 53.0 09/06/02 10:35:12

0.4 62.1 09/06/02 10:35:22

0.4 69.5 09/06102 10:35:32

0.4 74.8 09/06/02 10:35:42

0.4 79.3 09/06/02 10:35:52

0.4 82.7 09/06/02 10:36:02

0.3 85.4 09/06/02 10:36:12

0.4 87.4 09/06/02 10;36:22

0.4 88.3 09/06/02 10:36:32

0.4 69.2 09/06/02 10:36:42

0.4 90.1 09/06/02 10:36:52

0.4 90.9 09/06/02 10:37:02

0.4 91.3 09/06/02 10:37:12

0.4 92.0 09/06/02 10:37:22

0.4 92.2 09/06/02 10:37:32

0.4 92.6 09/06/02 10:37:42

0.3 92.7 09/06102 10:37:52

0,4 92.9 09/06/02 10:38:02

0,4 92.9 09/06/02 10:38:12

0.4 93.0 09/06/02 10:38:22

0.4 92.9 09/06/02 10:38:32

0,4 93.0 09/06/02 10:38:42

0.4 93.0 09/06/02 10:38:52

0.5 92.7 09/06]02 10:39:02

10.5 92,8 09/06/02 10:39:12

15.2 92.9 09/06/02 10:39122

15,4 92.9 09/06/02 10:39:32

15.4 93.1 09/06/02 10:39:42

15.3 92.7 09/06/02 10:39:52

15.3 91.2 09/06/02 10:40:02

15.3 87.9 09/06/02 10:40:12

4.8 81.9

86.8

1.5 87.2 1.5 87.1 1.5 85.9 1.6 82.5 2.3 74.3 5.2 62.1 8.8 50.6 11.6 42.0 13.8 35.7 15.6 30.9 17.2 27.0 18.5 23.6 19.5 20.7 20.5 18.2 21.1 16.0 21.7 13.9 22.2 12.2 22.5 10.6 22.8 9.3 23.0 8.0 23.1 7.1 23.2 6.4 23.4 5.6 23.5 4.9 23.4 4.4 23.3 4.O 23..6 3.6 23.5
3.3 23.6 3,1 23.1 2.8 21.0 2.6 17.6 2.3 14.3 2.1 11.4 1.9 9.0 1.8 7.2 1.6 5.7 1.5 4.7 1.4 3.8 1,3 3.2 1.1 2.7 1.0 2.2 0.9 2.0 0.9 1.7 0.7 1.6 0.6 1.5 0.5 1.4 0.4 1.3 0.4 1.3 0.3 1.2 0.3 1.2 0.3 1.1 0.2 1.1 0.1 1.1 0.1 1.0 0.'1 0.9 0.0 0.9 0.0 0.9 0.0 1.0 0.0 1.0 -0.1 0.9 -0.1 0.9 -0.1 0,8
-0.I 0.9 0.0 1.0 0.0 1/1

25.1 ppm NOx
Zero CO

99.4 ppm CO Zero VOC. SO2 NOx

14.7 ppm C3H8

Page 79/6/02 Run #3

Date/Time VOC CO mm/drt/yy hh:mm:ss ppm ppm 09106/02 10:41:12

19.8 26.3 09/06/02 10:41:22

20.0 22.8 09/06/02 10:41:32

20.0 22,5 09/06/02 10:41:42

19.8 31.0 09/06102 10:41:52

19.6 50.3 09106/02 10:42:02

19.7 77,3 09/06/02 10:42:12

19.7 102,2 09/06/02 10:42:22

19.7 120.8 09/06102 10:42:32

20.6 133.6 09/06/02 10:42:42

20.2 142.2 09/06102 10:42:52

19.7 149.2 09/06/02 10:43:02

19.7 155.5 09/06/02 10:43:12

19.6 160.0 09/06/02 10:43:22

19.5 165.0 09/06/02 10:43:32

19.4 169.9 09/06/02 10:43:42

19.5 174.5 09/06/02 10:43:52

19.4 177.5 09/06/02 10:44:02

19.3 180.9 09/06/02 10:44:12

19.3 183.9 09/06/02 10:44:22

19.2 186.6 09/06/02 10:44:32

19.2 188.7 09/06102 10;44:42

19.0 190.7 09/06/02 10:44:52

19.t 192.2 $02 NC'x ppm ppm 0.9 1.6 1.1 1,6 1.2 2.5 1.4 6.1 2.1 12.2 3.6 19.2 6,0 24.9 9.1 28.8 12.5 31.7 15.8 33.7 18.8 35.2 21,5 36.5 23.8 37.7 25.8 39.0 27.8 40.4 29.9 41.7 32.1 42, 34.4 43,7 36.4 44.5 38.4 45.2 40.2 45.8 41.8 46.2 43.1 46.7

Start Run #2 09/06/02 10:45:02

19.0 193.3 44.2 47.0 09/06/02 10:45:12

18,9 193.8 45.2 47.4 09/06/02 10:45:22

19.0 194.4 45.9 47.6 09/06/02 10:45:32

18,8 195.2 46.6 47.9 09/06/02 10:45:42

18.7 195.9 47.2 48,1 09/06/02 10:45:52

18.9 196.6 47.7 48.3 09/06/02 10:46:02

18.6 197.2 48,1 48.5 09/06/02 10:46:12

18.6 197.8 48.4 48.6 09/06/02 10:46:22

18.5 198.5 48.8 48.7 09/06/02 10:46:32

18.6 199.0 49.0 48.9 09/06/02 10:46:42

18.3 199.7 49,2 49.0 09/06/02 10:46:52

18.3 200.0 49.3 49.2 09/06/02 10:47:02

18.4 200.4 49.5 49.2 09/06/02 10:47:12

18.4 200.8 49.7 49.3 09/06/02 10:47:22

18.3 201.0 49.9 49.4 09/06/02 10:47:32

18.5 201.4 50.1 49.4 09/06/02 10:47:42

18.3 201,6 50.2 49.5 09/06/02 10:47:52

18.4 201.8 50.3 49.6 09/06/02 10:48:02

18.4 202.1 50.5 49.7 09/06/02 10:48:12

18.4 202.0 50.6 49.7 09/06/02 10:48:22

18.4 201.9 50.7 49.7 09/06/02 10:48:32

18.6 202.0 50.8 49.7 09/06/02 10:48:42

18.4 202.0 50.8 49.7 09/06/02 10:48:52

18.4 201.8 50,9 49.7 09/06/02 10:49:02

18.4 201.9 50.9 49,8 09/06/02 10:49:12

18.2 201,9 50.9 49.7 09/06/02 10:49:22

18.3 201.9 51.0 49.8 09/06/02 10:49:32

18.3 202.3 51.2 49.9 09/06/02 10:49:42

18.3 202.5 51.3 50.0 09/06/02 10:49:52

18,2 202.7 51.4 49.9 09/06/02 10:50:02

18.2 202.7 51,3 50.0 09/06/02 10:50:12

18.1 202.9 51.3 50.0 09/06/02 10:50:22

18.2 203.0 51.4 49.9 09/06/02 10:50:32

18.2 202.9 51.5 50.1 09/06/02 10:50:42

18.2 203.1 51.6 50.1 09/06/02 10:50:52

18.1 203.0 51.6 50.1 09/06/02 10:51:02

18.1 203.1 51.7 50.2 09/06/02 10:51:12

18,0 203.2 51.8 50.1 09/06/02 10:51:22

17.9 202.9 51.9 50.2 09/06/02 10:51:32

18.1 202.7 51.9 50.1 09/06/02 10:51:42

17.9 202.5 51.9 50.1 09/06/02 10:51:52

18.0 202.1 51.9 50.0 09/06/02 10:52:02

18.0 201,9 51.8 50.0 09/06/02 10:52:12

18,0 201,6 51.7 49.9 09/06/02 10:52:22

18,1 201.5 51,7 50.0 09/06/02 10:52:32

17.9 201.2 51.8 49.9 09/06/02 10:52:42

17.8 201.4 51.7 50.0

Page916/02 Run #3

09/05/02 10:52:52 09/06/02 10:53:02 09/06/02,10:53:12 09/06/02 10:53:22 09/06102 10:53:32 09/06/02 10:53:42 09/06/02 10:53:52 09106/02 10:54:02 09/06/02 10:54:12 09/06/02 10:54:22 09/06/02 10:54:32 09/06/02 10:54:42 09/06/02 10:54:52 09/06/02 10:55:02 09/06/02 10:55:12 09/06/02 10:55:22 09/06/02 10:55:32 09/06/02 10:55:42 09/06/02 10:55:52 09/06102 10:56:02 09106/02 10:56:12 09/06/02 10:56:22 09/06/02 10:56:32 09106/02 10:56:42 09/06/02 10:56:52 09/06102 10:57:02 09/06/02 10:57:12 09/06/02 10:57:22 09/06/02 10:57:32 09/06/02 10:57:42 09/06/02 10:57:52 09106/02 10:58:02 09/06/02 10:58:12 09/06/02 10:58:22 09/06/02 10:58:32 09/06102 10:58:42 09106/02 10:58:52 09/06/02 10:59:02 09/06/02 10:59:12 09/06102 10:59:22 09/06/02 10:59:32 09/06/02 10:59:42 09/06/02 10:59:52 09/06/02 11:00:02 09/06/02 11:00:12 09/06/02 11 ;00:22 09106/02 11:00:32 09106/02 11:00:42 09/06/02 11:00:52 09/06/02 11:01:02 09/06/02 11:01:12 09/06/02 11:01:22 09/06/02 11:0t:32 09/06/02 11:01:42 09/06/02 11:01:52 09/06/02 11:02:02 09/06/02 11:02:12 09/06/02 11:02:22 09/06/02 11:02:32 09/06/02 11:02:42 09/06/02 11:02:52 09/06/02 11:03:02 09/06/02 11:03:12 09/06/02 11:03:22 09/06/02 11:03:32 09/06/02 11:03:42 09/06/02 11:03:52 09/06/02 11:04:02 09/06/02 11:04:12 09/06/02 11:04:22 09106/02 11:04:32 09/06/02 11:04:42 09/06/02 11:04:52 09/06/02 11:05:02

17.9 17.7 17.8 17.8 17.8 17.6 17.6 17.6 17.6 17,5 17.5 17.5 17.5 17.5 17.5 17.5 17.5 17.3 17.4 17.4 17.4 17.3 17,3 17,4 17.4 17.2 17.4 17.3 17,3 17.2 17.2 17.0 17.0 17.0 17.1 17.1 17.0 17.2 17.2 17.1 17.0 16:9 16.9 16.9 16.9 16.7 16.9 16.8 16.7 16.9 16.8 16.7 16.7 16.7 16.6 16,6 16.5 16.5 16.6 16.5 16,5 16.5 16.5 16,4 16.4 16.3 16.5 16.3 16.2 16.1 16.2 16.1 16.1 16.1 201.1 201.2 201.2 201,1 200.9 200.9 200.8 200.9 200.9 200.8 200.8 200.9 200.8 200.8 200.7 200.6 200.3 200.3 200.6 200.4 200,6 200.5 200.4 200.3 200.2 200.0 199.7 199.6 199.4 199.3 199.3 198.9 198.7 198.5 198.2 198.2 198.1 198.2 198.1 198.1 198.1 198.0 198.1 197.9 197.9 197.8 197.6 197.6 197.5 197.4 197.4 197.1 197.1 196.8 196.7 196.5 196.4 196.2 196.1 196.0 195.8 195.6 195.1 195.1 194.9 194.8 194.9 194.8 194,8 194.9 194.5 194.6 194.5 194.4 51.7 51.7 51.7 51.6 51.5 51.5 51.6 51.6 51.6 51.6 51.7 51.7 51.8 51.7 51.6 51.5 51.4 51.4 61.4 51.4 51.4 51.4 51.3 51.2 51.3 51.3 51.1 51.1 51.2 51.2 51.2 51,1 51.1 51.0 51.0 51.0 51.0 50.9 50,8 50.8 50.7 50.7 50.7 50.7 50.6 50.6 50.6 50.6 50.5 50.5 50.6 50.6 50.5 50.5 50.4 50.4 50.4 50.3 50.3 50,3 50.3 50.2 50.1 50.1 50.0 49,9 49.9 49,9 49.8 49.8 49.8 49.7 49.7 49.8 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 50.0 49.9 49.8 49.7 49.8 49.8 49,8 49.8 49,9 49.8 49.8 49.8 49.9 49.9 49.9 49.7 49.8 49.8 49.8 49.7 49.7 49.8 49,8 49.8 49.8 49,8 49.7 49.7 49.7 49.8 49.7 49.6 49.7 49.7 49.8 49.7 49.7 49.6 49.6 49.7 49.6 49.6 49.6 49.7 49.6 49.7 49.6 49.5 49.4 49.5 49.6 49.5 49.4 49.4 49.5 49.4 49.4 49.4 49.3 49.3 49.3 49.3 49,3 49.4 49.4 49.39/6/02 Run #3

09/06/02 11:05:12

16,0 194.3 49.8 49.3 09/06/02 1-1:05:22

15.9 194.1 49.7 49.3 09/06/02 11:05:32

15.9 194.2 49.7 49.3 09/06/02 11:05:42

16.0 194.2 49.6 49.2 09/06/02 11:(•3:52

16.0 194.2 49.5 49.3 09/06/02 11:06:02

16.0 194.0 49.5 49.2 09/06/02 11:06:12

15.9 194,0 49.4 49.3 09/06.,'02 11:06:22

16.2 193.8 49.4 49.2 09/06/02 11:06:32

16.1 193.7 49.4 49.3 09/06102 11:06:42

15,8 193.7 49.3 49.2 09/06102 11:06:52

15.8 i93.4 49.3 49.2 09/06/02 11:07:02

15.8 193.4 49.3 49.2 09/06/02 11:07:12

15.8 193.5 49.2 49.2 09/06/02 11:07:22

15.8 193.3 49.1 49.1 09/06/02 11:07:32

15.7 193.2 49.0 49.1 09/06/02 11:07:42

15,7 193.2 49.0 49.1 09/06/02 11:07:52

15.9 193.2 48.9 49.2 09/06/02 11:08:02

15.7 193.1 49.0 49,1 '09/06102 11:08:12

15.7 193.0 48.9 49,1 09/06/02 11:08:22

15.6 192.9 48.9 49.1 09106/02 11:08:32

15.6 192.7 48,8 49.0 09/06/02 11:08:42

15.7 192.6 48.7 49.0 09106/02 11:08:52

15.7 192.6 48.6 49.0 09/06/02 11:09:02

15.7 192.5 48.4 49.0 09/06/02 11:09:12

15.6 192.3 48.4 49.0 09/06/02 11:09:22

15.7 192.3 48.3 49.0 09/06/02 11:09:32

15.6 192.3 48.4 49.0 09/06/02 11:09:42

t5.6 192.3 48.5 49.1 09/06/02 11:09:52

15.4 192.1 48.5 49.0 09/06/02 11:10:02

15.4 192.0 48.5 49.0 09/06/02 11:10:12

15.5 191.8 48.6 49.0 09106/02 11:10:22

15.5 191.8 48.7 48.9 09/06/02 11:10:32

15.5 191.4 48.6 48.9 09/06/02 11:10:42

16.2 191.1 48,5 48.9 09/06102 11:10:52

15.8 190,9 48,5 48,9 .09/06/02 11:11:02

15.5 190.8 48.5 48.9 09/06/0211:11:12 15.4 190.5 48.4 48.9 09/06/02 11:11•22

15.2 190.4 48.3 48.8 09/06/02 11:11:32

15.2 190.3 48.3 48.8 09/06/02 11:11:42

15.1 190,3 48.3 48,9 09/06/02 11:11:52

15.1 190.1 48.2 48.8 09/06/02 11:12:02

15.0 190.1 48.2 48.8 09/06/02 11:12:12

15.0 189.9 48.2 48.8 09/06/02 11:12:22

15,2 189.6 48.1 48.8 09/06/02 11:12:32

15,0 189.5 48.1 48.8 09/06/02 11:12:42

15.0 189.3 48.1 48.8 09106/02 11:12:52

15.0 189.1 48.2 48.7 09/06/02 11:13:02

14.8 189.1 48.2 46.8 09/06/02:11:13:12 12.4 189.0 48.2 48.8 09/06/02 11:13:22

9.8 188.8 48.3 48.8 09/06/02 1t:13:32

10.2 188.6 48.2 48.8 09/06/02 11:13:42

10.2 188,6 48.3 48.7 09/06/02 11:13:52

10.3 187.4 48.3 47.9 09/06/02 11:14:02

10,3 183.2 46.0 46.0 09/06/02 11:14:12

11,2 176.3 47.0 44.2 09/06/02 11:14:22

13.8 169.5 45.6 42.9 09/06/02 11:14:32

17.3 163.4 43.8 42.0 09/06/02 11:14:42

17.4 158.7 41.8 41.2 09/06/02 11:14:52

14.1 155.7 39.8 40,6 09/06/02 !1;15:02

12.2 152.8 38.0 40.2 09/06/02 11:15:12

18.5 150.1 36.4 39.7 09/06/02 11:15:22

21.5 147.3 35.2 39.1 09/06/02 11:15:32

21.6 144.4 34.4 38,4 09/06/02 11:15:42

21.5 142.0 33,3 37.7 09/06/02 11:15:52

21.3 142.1 32.5 38.3 09/06/02 11:16:02

21.1 147.4 32.0 39.9 09/06/02 11:16:12

21,1 156.6 32.0 41.7 09/06/02 t1:16:22

21.2 165.7 32.9 43.2 09/06/02 11:16:32

21.1 173,8 34.3 44.3 09/06/02 11: 6:42

21.3 178.9 35.8 45.2 09/06/02 11:16:52

21.2 183.1 37.6 45.7 09/06102 11:17:02

21.1 186,5 39.2 46.0 09/06/02 11:17:12

21.0 188,6 40.8 46.2 09/06/02 11:17:22

21.1 190.3 42.0 46.4

Page 3 309/6/02 Run #3

09/06/02 11:17:32

21.1 191,9 42.9 46.7 09/06/02 11:17:42

21.1 192.9 43.8 46.8 09/08/02 11:17:52

21,1 193.5 44.6 47.0 .09/06/02 11:18:02

20.9 193.8 45,2 47.1 09/06t02 11:18:12

21.0 194.3 45.:7 47.2 09/06/02 11:18:22

21.0 194.7 46.0 47.3 09/06/02 11:18:32

20.8 195.4 46.4 47.4 09/06/02 11:18:42

20.8. 196.3 46.8 47.6 09/06/02 11:18:52

20.9 197.4 47.1 47.9 09/06/02 11:19:02

20.8 196.4 47.4 48.1 09/06/02 11:19:12

20.9 199,4 47.7 48.4 09/06/02 11:19:22

20.9 200.2 48.0 48.5 09/06/02 11:19:32

20.9 200.9 48,2 48.6 09/06/02 11:19:42

20.9 201.6 48.3 48.8 09/06/02 11:19:52

21.0 202.2 48.5 48.8 09106/02 11:20:02

21.0 202.6 48.6 48.9 09/06/02 11:20:12

21,0 202,8 48.7 49.0 09/06/02 11:20:22

20.9 203.4 48.9 49.1 09/06/02 11:20:32

20.9 203.7 49.1 49.2 09/06/02 11:20:42

20.9 204.2 49.2 49.2 09/06/02 11:20:52

20.9 204.3 49.2 49.2 09/06/02 11:21:02

20.9 204.7 49.2 49.3 09/06/02 11:21:12

20.9 204.8 49.3 49.4 09/06/02 11:21:22

20.9 205.2 49.3 49.4 09/06/02 11:21:32

20.9 205.2 49.3 49.4 09/06/02 11:21:42

20.9 205,2 49.4 49.4 09/06/02 11:21:52

20.7 205.4 49.4 49.5 09/06/02 11:22:02

20.9 205.4 49,4 49.6 09/06/02 11:22:12

20.9 205.5 49.4 49.5 09/06/02 11:22:22

20.9 205.7 49.4 49.5 09/06/02 11:22:32

21.0 205.7 49.5 49.5 09/06/02 11:22:42

20,9 205,8 49.5 49.6 09/06/02 11:22:52

20.9 205,6 49.5 49.5 09/08/02 11:23:02

20.9 205.8 49.6 49.6 09/06/02 11:23:12

20,9 206,1 49.6 49.6 09/06/02 11:23:22

20,8 205.9 49.6 49.6 09/06/02 11:23:32

20.8 205.9 49,6 49.6 09/06/02 11:23:42

20.7 205.9 49.6 49.7 09/06/02 11:23:52

20.7 206.1 49.7 49.7 09/06/02 11:24:02

20.7 206.1 49.8 49.7 09/06/02 11:24:12

20.8 206.2 49.9 49.7 09/06/02 11:24:22

20.7 206.3 49.9 49.8 09/06/02 11:24:32

20.7 206.4 49.9 49.8 09/06/02 11:24:42

20.7 206.4 49.9 49.8 09/06/02 11:24:52

20.5 206.4 50.0 49.8 09/06/02 11:25:02

20.7 206.5 50.0 49.9 09/06/02 11:25:12

20.6 206.5 50.1 49.8 09/06/02 1•1:25:22

20.6 206.4 50.1 49.9 09/06/02 11:25:32

20.6 206.3 50.1 49.9 09/06/02 11:25:42

20.7 206.2 50.1 49.9 09/06/02 11:25:52

20.6 206.2 50.1 49.9 09106/02 11:26:02

20.5 206.2 50. 49.9 09/06/02 11:26:12

20.4 206.1 50.2 49.9 09/06102 11:26:22

20.4 206.2 50.2 49.9 09/06/02 11:26:32

20.5 206.0 50.4 49.8 09/06/02 11:26:42

20.3 205.9 50.4 49.8 09/06/02 11:26:52

20.3 205.7 50.3 49.9 09/06/02 11:27:02

20.5 205.8 50.2 49.9 09/06/02 11:27:12

20.3 205.9 50.2 49.8 09/06/02 11:27:22

20.3 205.9 50.3 49.8 09/06/02 11:27:32

20.4 205.7 50.3 49.8 09106/02 11:27:42

20.3 205.7 50.3 49.8 09/06/02 11:27:52

20.2 205.7 50.3 49.8 09/06/02 11:28:02

20.2 205.9 50.2 49.8 09/06/02 11:28:12

20.2 205.9 50.2 49.9 09/06/02 11:28:22

20.1 205.8 50.2 49,8 09/06/02 11:28:32

20.0 205.8 50.2 49.9 09/06/02 11:28:42

20.0 205.9 50.1 49.9 09/06/02 11:28:52

20.1 206.0 50.2 49.9 09/06/02 11:29:02

20.0 205.8 50.2 49.8 09/06/02 11:29:12

20.1 206.0 50.2 49.8 09/06/02 11:29:22

20.1 205:8 50.2 49.9 09/06/02 11:29:32

20.0 205.6 50.2 49.9 09/06/02 11:29:42

20,1 205.5 50.2 49.8

Page9/6/02 Run #3

09/06/02 11:29:52

20.0 205.3 50.2 49.9 09/06/02 11:30:02

20.0 205.0 50,2 49.9 09/06/02 11:30:12

20,0 204.9 50.2 49.8 09/06/02 11:30:22

19.9 204.9 50,3 49.8 09/06/02 11:30:32

19.9 204.9 50.3 49.8 09/06/02 11:30:42

20.0 204.8 50.4 49.8 09/06/02 11:30:52

19.9 204.7 50.2 49.8 09/06102 11:31:02

19.8 204.5 50.2 49.8 09/06/02 11:31:12

19.8 204.4 50.2 49.8 09/06/02 11:31:22

19.8 204.3 50.1 49.6 09/06/02 11:31:32

19.8 204.3 50.1 49.6 09/06,/02 11:31:42

19.7 204.2 50.1 49.6 09/06/02 11:31:52

19.8 204.3 50,1 49.7 09/06/02 11:32:02

19.7 204.4 50.2 49.7 09/06/02 11:32:12

19.7 204.6 50.3 49.7 09/06/02 11:32:22

19.7 204.5 50.3 49.7 09106/02 11:32:32

19.7 204.6 50.2 49.7 09/06/02 11:32:42

19.7 204.4 50.1 49,6 09/06/02 11:32:52

19.5 204.7 50.1 49.6 09/06102 11:33:02

19.5 204.5 50.0 49.7 09/06/02 11:33:12

19.6 204.1 50.2 49.7 09106/02 11:33:22

19.6 204.0 50.2 49.7 09/06/02 11:33:32

19.5 203,9 50.2 49.6 09/06/02 11:33:42

19.5 203.7 50.2 49.7 09/06102 11:33:52

19.4 203.7 50.1 49.7 09/06/02 11:34:02

19.6 203.9 50.1 49.7 09/06/02 11:34:12

19.5 204.0 50.1 49.7 09/06/02 11:34:22

19.5 204.2 50.2 49.7 09/06/02 11:34:32

19.3 204.0 50.2 49.7 09/06/02 11:34:42

19.3 204.0 50.2 49.7 09/06/02 11:34:52

19.4 204.0 50.2 49.7 09/06/02 11:35:02

19.3 203.7 50.2 49.7 09/06/02 11:35:12

19.3 203.6 50.1 49.6 09/06/02 11:35:22

19.3 203.4 50.1 49.6 09/06/02 11:35:32

19.3 203.4 50.1 49.6 09/06/02 11:35:42

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19.0 202.6 50.2 49.5 09/06/02 11:37:02

19.1 202.6 50.2 49.4 09/06/02 11:37:12

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19.2 202.3 50.2 49.4 09/06/02 11:37:32

19.0 202.1 50.2 49.5 09/06/02 11:37:42

19.0 202.0 50.3 49.5 09/06/02 11:37:52

19.1 201.7 50.3 49.5 09/06/02 11:38:02

19.1 201.7 50.3 49.5 09/06/02 11:38:12

19.0 201.5 50.3 49.5 09/06/02 11:38:22

19.0 201.3 50.2 49.4 09/06/02 11:38:32

19.0 201.2 50.3 49.4 09/06/02 11:38:42

19.0 201.4 50.3 49.4 09/06/02 11:38:52

18.9 201.4 50.3 49.4 09/06/02 11:39:02

18.8 201.4 50.2 49.4 09/06/02 11:39:12

18.8 201.4 50.2 49.4 09/06/02 t1:39:22

18.8 201.3 50.2 49.3 09/06/02 11:39:32

18.8 201,0 50.1 49.3 09/06/02 11:39:42

18.8 200.9 50.0 49.3 09/06/02 11:39:52

16,7 200,9 50.0 49.3 09/06/02 11 ;40:02

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18.6 200.5 50.0 49.3 09/06/02 11:40:22

18.6 200.3 50.0 49.3 09/06/02 11:40:32

18.6 200.5 50,1 49.3 09/06/02 11:40:42

18,5 200.2 50.1 49.3 09/06/02 11:40:52 -•,• 18.4 200.1 50.1 49.4 09/06/02 11:41:02

18.6 200.1 50.1 49.4 09/06/02 11:41:t2

18.6 200.2 50.1 49.4 09/06/02 11:41;22

16.5 200.1 50,1 49.4 09/06/02 11:41:32

18.6 200.0 49.9 49.4 09/06/02 11:41:42

18.4 199.9 49.9 49.3 09/06/02 11:41:52

18.4 200.0 49.9 49.2 09/06/02 11:42:02

16.4 199.9 49.9 49.3

Page 5 ,329/6/02 Run #3

09/06/02 11:42:12 09/06/02 11:42:22 09/06/02 11:42:32 09/06/02 11:42:42 09/06/02 11:42:52 09/06/02 11:43:02 09/06/02 11:43:12 09106/02 11:43:22 09/06/02 11:43:32 09/06/02 11:43:42 09/06/02 :43:52 09/06/02 11:44:02 09/06/02 11:44:12 09/06/02 11:44:22 09/06/02 11:44:32 09/06/02 11:44:42 09/06/02 11:44:52 09/06/02 11:45:02 09/06/02 11:45:12 09106/02 11:45:22 09/06/02 11:45:32 09/06/02 11:45:42 09/06/02 11:45:52 Stop Run #2

09106/02 11:46:02 09/06/02 11:46:12 09/06/02 11:46:22 09/06/02 11:46:32 09/06/02 11:46:42 09/06/02 11:46:52 09/06/02 11:47:02 09/06/02 11:47:12 09/06/02 11:47.'22 09/06/02 11:47:32 09/06/02 11:47:42 09/06/02 11:47:52 09/06/02 11:48:02 09/06/02 11:48:12 09/06/02 11:48:22 09/06/02 11:48:32 09/06/02 11:48:42 09/06/02 11:48:52 09106/02 11:49:02 09/06/02 11:49:12 09/06/02 11:49:22 09106/02 11:49:32 09/06/02 11:49:42 09106/02 11:49:52 09/06/02 11:50:02 09/06/02 11:50:12 09/06/02 11:50:22 09/06/02 11:50:32 09/06/02 11:50:42 09/06/02 11:50:52 09/05/02 11:51:02 09/06/02 11:51:12 09106/02 11:51:22 09/06/02 11:51:32 09/06/02 11:51:42 09/06/02 11:51:52 09/06/02 11:52:02 09/06/02 11:52:12 09/06/02 11:52:22 09/06/02 11:52:32 09/06/02 11:52:42 09/06/02 11:52:52 09/06/02 11:53:02 09/06/02 11:53:12 09/06/02 11:53:22 09/06/02 11:53:32 09/06/02 11:53:42 09/06/02 11 i53:52

18.4 18.5 18.5 18.5 18.5 18.6 18.4 18.3 18.2 18.3 18.2 18.2 18.1 18.1 18.2 14.8 11.1 11.0 11.3 11.3 11.7 11.35.3

18.10

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197.65

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6.76.66.3 6,3 6.66.36.0 49.8 49.8

49.8 49.7 49.7 49.6 49.5 49.5 49.5 49.4 49.4 49.4 49.4 49.4 49.5 49.5 49.6 49.6 49.5 49.2 48.5 47.0

49.17
45,1 43.5 42.0 40.5 39.1 37.5 35.1 32.3 29.5 28.2 29.1 31.7 35.4 39,4 43.5 47.5 51.3 54.9 58.2 61.2 64.0 66.5 68.7 70.6 72.3 73.9 75.2 76.5 77.4 78.2 79.0 79.8 80.6 81.1 81.7 82.3 82.8 83.2 83.6 84.0 84.3 84.4 84.5 84.6 84.8 85.0 85.1 85.2 49.3 49.3 49.3 49.2 49.2 49.1 49.1 49.1 49.1 49.1 49.0 49.1 49.0 49.0 49.0 49.0 48.9 48.9 48.9 47.8 45.9 44.2 42.6

48.95

41.7 41.1 40.5 38.7 35.3 30.5 25.4 20.3 15.9 12.9 10.8 9.17.8 6.75.8 5.0 4.3 3.83.3 3.02.7 2,4 2.2 2.01.9 1.71.6 1,6 1.61,51.51.51.51.4 1,41.3 1.31.21.21,31.21.21.21.2 1.21.21.11.1

Page 6 339/6/02 R•Jn #3

09/06/02 11:54:02

0.9 5.9 85,3 1.0 09/06/02 11:54:12

0,9 5.9 85.4 1.1 09/06/02 11:54:22

0.9 5.9 86,5

.I 09/06/02 11:54:32

0.9 5.6 85.5

1.0 09/06/02 11:54:42

0.9 5.5 85.5

1.0 09/06/02 11:54:52

0.9 5.6 85.6

1.0 09/06/02 11:55:02

1.0 5.5 85.5 1.0 09/06/02 11:55:12

2.8 5.6 85.t 0.9 09/06/02 11:55:22

3,4 5.8 84.7 1.0 09/06/02 11;55:32

3.4 5.5 84.6 1.0 09/06/02 11:55:42

3.3 5.6 84,6 1.0 09/08/02 11:55:52

1.3 5.5 84.8 1.0 09/06/02 11:56:02

1.0 5.6 85.1 1.0 09106/02.11:56:12 1.0 6.0 84.5 1.1 09/06/02 11:56:22

0.9 6.3 81.9 1.4 09/06/02 11:56:32

0.9 7.7 75.4 3.7 09/06/02 11:56:42

0,9 8.7 65.6 7.3 09/06/02 11:56:52

0.9 8.6 56.0 10.6 09/06/02 11:57:02

0.9 8.0 48.2 13.3 09/06/02 11:57:12

0.9 7.2 42.0 15.5 09/06/02 11:57:22

1.0 6.8 37.0 17.4 09/06102 11:57:32

1,0 6,0 32.6 18.9 09/06/02 11:57:42

1.0 5.4 28.6 20.1 09106/02 11:57:52

1.0 5.0 25.0 21.0 09106/02 11:58:02

1.0 4.6 21.9 21.7 09/06/02 11:58:12

1.0 4.2 19.0 22.3 09/06/02 11:58:22

1.0 3.9 16.5 22.7 09/06/02 11:58:32

1.0 3.7 14.2 22.9 09/06/02 11:58:42

1.0 3.6 12.2 23.1 09/06/02 11;58:52

1.0 3,4 10.5 23.3 09/06/02 11:59:02

1.0 3.5 9.0 23.4 09/06/02 11.:59:12

0.9 3.4 7.7 23.5 09/06/02 11:59:22

0.9 3.4 6.8 23.6 09/06/02 11:59:32

0.9 3.3 5.8 23.6 09/06/02 11:59:42

0.9 3.3 4.8 23.6 09/06/02 11:59:52

1.3 3.3 4.0 23,4 09/06/02 12:00:02

1.1 3.2 3.5 23.6 09/06102 12:00:12

1.0 3.3 3,1 23.6 09106/02 12:00:22

1.0 3.2 2.6 23.6 09/05/02 12:00:32

1.0 3.4 2.1 23.4 09/06/02 12:00:42

1.0 5.4 1.8 21.7 09/06/'02 12:00:52

0.9 12.6 1.5 18.4 09106/02 12:01:02

0.9 24.2 1.3 14.7 09/06/02 12:01:12

0,9 37.6 1.0 11.6 09/06/02 12:01:22

0.9 49.9 0.7 9.0 09/06/02 12:01:32

0.9 59.8 0.4 7,0 09/06/02 12:01:42

0.9 68.0 0.2 5.5 09/06/02 12:01:52

0.9 73.7 0.1 4.4 09/06/02 12:02:02

0.9 78.6 0.1 3,5 09/06/02 12:02:12

0.9 82,0 0.0 2.9 09/06/02 12:02:22

0,9 84.7 -0.1 2.4 09/06/02 12:02:32

0.9 86.6 -0.3 2.0 09/06/02 12:02:42

0.9 87.7 -0.4 1.7 09/06/02 12:02:52

0.9 88.4 -0,5 1.6 09/06/02 12:03:02

0.9 89.0 -0.7

,S 09/06/02 12:03:12

0.9 90.0 -0.8 1.3 09/06/02 12:03:22

0.9 90.6 -0.9 1.3 09/06/02 12:03:32

0.9 91.0 -1.0 1.2 09/06/02 12:03:42

0.9 91.4 -1.1 1.1 09/06/02 12:03:52

0.9 91.5 -0,6 1.0 09/06/02 12:04:02

0.9 91.8 -0.1 1.0 09/06/02 12:04:12

0.9 91.9 -0.2 0.9 09/06/02 12:04:22

0.8 92.3 -0.3 1.0 09/06/02 12:04:32

0.9 92.7 -0.3 0.9 09/06/02 12:04:42

0.9 92.8 -0.4 0,9 09/06/02 12:04:52

0.9 93.0 -0.6 0.8 09/0602 12:05:02

0.9 93.4 -0.6 0.8 09/06/02 12:05:12

0,9 93.4 -0.4 0.8 09/06/02 12:05:22

0.9 93.4 -0.1 0,8 09/06/02 12:05:32

0.9 92.9 -0.2 0.7 09/06/02 12:05:42

8.4 93.1 -0.2 0.8

91 oDm $02

25.1 ppm NOx 7ero CO

99.4 opm CO
Zero VOC, CO, SO2

Page 7916102 Run #3

09/06/02 12:05:52

15.7 93.1 -0.2 0,8 09/06/02 12:06:02

15.4 93.1 -0.3 0.8 09106102 12:06:12

!5.3 93.0 -0.3 0,7 09/06/02 12:06:22

15.3 92.8 -0.4 0.7 09/06/02 12:06:32

15.3 91.5 -0.5 0.8 09/06/02 12:06:42

15.3 88.6 -0.4 0.8 09/06/02 12:06:52

12.7 62.5 -0.3 0.9 09/06/02 12:07:02

3.5 72.6 =0.2 1.1

14.7 ppm C3H8

Page 8 35916/O•Ru n #3

Date/Time VOC CO 802 NOx mm/dd/yy hh:mm:ss ppm ppm ppm ppm 09106102 12:07:42

19.2 29.3 0.4 1.2 09/06/02 12:07:52

19.5 23.9 0.6 1.1 09106102 12:08:02

19.2 20.0 0.7 1.0 Q9/06/02 12:08:12

19.0 17.9 0.6 1.1 09106102 12:08:22

18.8 20.5 0.6 3.2 09/06/02 12:08:32

18.9 35.9 1.2 8.9 09/06/02 12:08:42

18.7 62.3 2.8 16.4 09/06/02 12:08:52

18.5 90.7 5.5 23.3 09t06/02 12:09:02

18,4 114.0

9.0 28.9 09/06/02 12:09:12

18.4 131.3 12.8 33.0 09/06/02 12:09:22

18.3 144.0 16.9 36.0 09106102 12:09:32

18.2 155.1 21.0 38.3 09/06/02 12:09:42

18.1 163.1 24.7 40.1 09/06/02 12:09:52

18.2 169.6 28.2 41.4

Start Run #3 09/06/02 12:10:02

18.3 174.7 31.4 42.4 09/06/02 12:10:12

18.2 177.6 34.3 43.3 09/06/02 12:10:22

18.2 180.7 36.8 43.9 09/06/02 12:10:32

18.1 183.2 39.0 44.5 09106/02 12:10:42

18.1 185.3 40.9 45.0 09/06/02 12:10:52

18.0 187.0 42.3 45.3 09106/02 12:11:02

18.0 188.3 43.7 45.7 09/06/02 12:11:12

18.1 189.3 44.9 45.9 09/06102 12 11 22

17.9 190.3 45.8 46.0 09/06102 12:11:32

18.0 190,9 46.6 46,3 09/06/02 12:11:42

18.0 191.7 47.4 46.5 09/06/02 12:11:52

18.0 192.3 48.1 46.6 09/06/02 12:12:02

17.9 192.7 48.7 46.8 09/06/02 12:12:12

17.9 192.8 49.1 46.8 09/06/02 12:12:22

17.7 193.1 49.3 47/ 09/06/02 12:12:32

17.9 193.2 49.6 47.1 09/06/02 12:12:42

17.9 193,3 49.8 47.1 09/06/02 12:12:52

17.6 193.5 50.1 47.2 09/06102 12:13:02

17.6 193.7 50.4 47.3 09/06/02 12:13:12

17.8 193.9 50.5 47.3 09106/02 12:13:22

17.7. 194.0 50.7 47.4 09/06/02 12:13:32

17.6 194.2 50.7 47.4 09/06/02 12:13:42

17.6 194.3 50.8 47.5 09/06102 12:13:52

17.6 194.3 50.9 47.5 09/06/02 12:14:02

17.5 194.4 51.0 47.6 09/06/02 12:14:12

17,5 194.6 51.0 47.6 09/06/02 12:14:22

17.6 194.8 51.1 47.7 09/06/02 12:14:32

17.5 195.0 51.2 47.7 09/06/02 12:14:42

17.5 195.3 51.3 47.8 09/06/02 12:14:52

17.5 195.4 51.4 47,7 09/06/02 12:15:02

17,4 195.5 51.6 47.8 09/06102 12:15:12

17.4 195.3 51.6 47.8 09/06102 12:15:22

17.4 195.5 51.5 47.8 09/06/02 12:15:32

17.5 195,5 51.6 47,7 09/06/02 12:15:42

17.4 195.7 51.5 47.8 09/06/02 12:15:52

17.4 195.6 51.6 47.8 09/06/02 12:16:02

17.4 195,6 51.6 47.8 09106/02 12:16:12

17.4 195,7 51,5 47.8 09/06/02 12:16:22

17.3 195.8 51.6 47.8 09/06/02 12:16:32

17.3 195.7 51.7 47.8 09/06/02 12:16:42

17.3

51.6 09/06/02 12:16:52

17.3 195.7 51.5 47.8 09/06/02 12:17:02

17,3 195.8 51.5 47.8 09/06/02 12:17;12

17.3 195.6 51.5 47.8 09/06/02 12:17:22

17.3 195.8 51.5 47.8 09/06/02 12:17:32

17.2 195.7 51.5 47.8 09/06/02 12:17:42

17.2 195.4 51.5 47.8 09/06/02 12:17:52

17.1 195,5 51.5 47.8 09/06/02 12:18:02

17.2 195.2 51,5 47.8 09/06/02 12:18:12

17.1 195,.2 51.4 47.7 09/06/02 12:18:22

17.0 195.1 51.5 47.8 09/06/02 12:18:32

17.0 195.1 51.6 47.8 09/06/02 1.2:18:42

17.0 195.1 51.6 47,7 09/06/02 12:18:52

17.1 194.9 51.6 47.8 09/06/02 12:19:02

17.1 195.1 51.5 47.8 09/06/02 12:19:12

17.0 194.9 51.5 47.8 3G

Page9/6/02 Run #3

09/05/02 12:19:22

16.9 194.9 51.4 47.8 09/06/02 12:19:32

17.0 194.5 51.3 47,7 09/06/02 12:19:42

17.0 194.5 51.3 47.7 09/06/02 12:19:52

17.0 194.5 51.4 47.7 09/06/02 12:20:02

16.9 194.3 51.3 47.7 09/06/02 12:20:12

17.0 194.2 51.2 47.7 09/06/02 12:20:22

17.0 194.1 51.2 47.7 09/06/02 12:20:32

17.0 194.1 51.2 47.6 09/06/02 12:20:42

16.9 194.1 51.2 47.6 09/06/02 12:20:52

16.9 193.9 51.1 47.6 09/06/02 12:21:02

16.9 193.9 51.0 47.6 09/06/02 12:21:12

17.0 193,8 50.9 47.7 ,09/06/02 12:21:22

16.9 193,8 50.8 47.7 09/06/02 12:21:32

16.8 193.9 50.8 47.7 09/06/02 12:21:42

16.7 194.0 50.7 47.7 ,09/06/02 12:21:52

16.7 193.9 50.6 47.7 09/06/02 12:22:02

16,9 193.9 50.5 47.7 09/06/02 12:22:12

16.7 193.8 50,5 47.7 09/06/02 12:22:22

16.7 193.9 50.4 47.7 09/06/02 12:22:32

16.8 194.0 50.5 47.7 09/06/02 12:22:42

16.9 193,9 50.4 47.6 09106/02 12:22:52

16.8 193.9 50.4 47.7 09/06/02 12:23:02

16.7 193.8 50.3 47.7 09/06/02 12:23:12

16.9 193,6 50.2 47.6 09/06/02 12:23:22

16.8 193.4 50.1 47.5 09/06/02 12:23:32

16.7 193.3 50.0 47.5 09/06/02 12:23:42

16,6 193.3 50.0 47.6 09/06/02 12:23:52

16.5 193.2 50,1 47.5 09/06/02 12:24:02

16.5 193.0 50,1 47.5 09/06/02 12:24:12

16.5 192.9 50.1 47,4 09/06/02 12:24:22

16.3 192.9 50.1 47.4 09/06/02 12:24:32

16.3 192,8 50.2 47.5 09/06/02 12:24:42

16.2 192.6 50.2 47.4 09/06/02 12:24:52

16.3 192.5 50.2 47.4 09/06102 12:25:02

16.3 192.4 50.3 47.4 09/06/02 12:25:12

16.1 192.5 50.2 47.4 09/06/02 12:25:22

16.1 192.2 50.1 47.4 09/06/02 12:25:32

16.2 192.3 50.1 47.4 09/06/02 12:25:42

16.1 192.3 49.9 47.3 09/06/02 12:25:52

16.1 192.4 50.0 47.4 09/06/02 12:26:02

16.0 192.2 49.9 47.3 09/06/02 12:26:12

16.0 192.3 49.9 47.3 09/06/02 12:26:22

16.0 192.1 49.8 47.3 09/06/02 12:26:32

15,9 191.9 49,7 47.3 09/06/02 12:26:42

16.0 191.6 49.7 47.3 09/06/02 12:26:52

16.0 191.5 49.6 47.3 09/06/02 12:27:02

16,0 191.4 49.6 47.3 09/06/02 12:27:12

16.0 191.3 49.6 47.2 09/06/02 12:27:22

15.9 191.3 49.6 47.2 09/06/02 12:27:32

16.0 191.2 49.5 47.0 09/06/02 12:27:42

15.8 191.2 49.4 47.1 09/06/02 12:27:52

15.8 191.1 49.3 47.1 09/06/02 12:28:02

15.8 191.0 49.3 47.1 09/06/02 12:28:12

15.8 191.0 49.3 47.2 09/06/02 12:28:22

15,7 190.7 49.4 47.2 09/06/02 12:28:32

15.8 190.7 49.5 47.3 09/06/02 12:28:42

15.7 190.4 49,5 47.1 09/06/02 12:28:52

15.7 190.1 49.5 47.1 09/06/02 12:29:02

15.7 189.9 49.5 47.1 09/06/02 12:29:12

15.6 189.7 49.5 47.0 09/06/02 12:29:22

15.5 189.8 49.6 47.1 09/06/02 12:29:32

15,5 189.5 49.6 47.1 09/06/02 12:29:42

15.4 189.6 49.6 47.1 09/06/02 12:29:52

15.4 189.3 49.6 47.0 09/06/02 12:30:02

15,4 189.1 49.6 47.1 09/06/02 12:30:12

15.5 189.1 49.6 47.1 09/06/02 12:30:22

15.6 189.1 49.6 47.1 09/06/02 12:30:32

15.7 188.9 49.5 47.0 09/06/02 12:30:42

15.7 188.8 49.4 47.0 09/06102 12:30:52

15.7 188.6 49.4 46.9 09/06/02 12:31:02

15.6 188.6 49.3 47.0 09/06/02 12:31:12

15.6 188.5 49.3 47.0 09/06/02 12:31:22

15.5 188.3 49.3 46.9 09/06/02 12:31:32

15.4 188.0 49.2 46.9

Page 2 3?9/6/02 Rut• #3

09/06/02 12:31:42

11.8 187.8 49.2 47.0 09/06/02 12:31:52

9.8 187.5 49.2 47.0 09/06/02 12:32:02

10.0 187,6 49.3 47.0 09/06/02 12:32:12

10.0 187.0 49.2 46.5 09/06/02 12:32:22

10.0 183.6 49.1 45.0 09/06/02.12:32:32 9.9 177.4 46.5 43.4 09/06/02 12:32:42

11.0 171.2 47.3 42.1 09/06/02 12:32:52

14.6 164.9 45.7 41.1 09/06/02 12:33:02

18.1 160.0 43.8 40.4 09/06/02 12:33:12

18.4 156.9 42.1 39.9 09/06/02 12:33:22

14.3 154.1 40.4 39.4 09/06/02 12:33:32

14.2 151.6 39.0 38.9 09/06/02 12:33:42

21.4 148.9 37.8 38.5 09/06/02 12:33:52

22.8 145.9 36.7 38.0 09/06/02 12:34:02

22.5 143.1 35.7 37.2 09/06/02 12:34:12

22.2 142.0 35.0 37.3 09/06/02 12:34:22

22.0 145.2 34.5 38.5 09/06/02 12:34:32

21.9 152.2 34.3 40.0 09/06/02 12:34:42

21.8 159.4 34.7 41.3 09/06/02 12:34:52

21.8 165.6 35.3 42.4 09/06/02 12:35:02

21.8 171.0 36.5 43.2 09/06/02 12:35:12

21.9 175.1 38.0 43.9 09/06/02 12:35:22

22.0 177.5 39.3 44.3 09/06/02 12:35:32

21.9 179.3 40.6 44.8 09/06/02 12:35:42

21.9 181.4 41.8 45.1 09/06/02 12:35:52

21.9 182.9 42.7 45.3 09/06/02 12:36:02

21.8 184.3 43.7 45.5 09/06/02 12:36:12

21.9 185.5 44.6 45.6 09/06/02 12:36:22

21.9 186.5 45.4 45.7 09/06/02 12:36:32

21.7 187.4 46.0 45.8 09106/02 12:36:42

21.7 187.9 46.5 45.9 09/06/02 12:36:52

21.8 188.6 46.9 46.0 09/06/02 12:37:02

21.9 189.2 47.4 46.1 09/06/0-2 12:37:12

21.7 189.7 47.8 46.4 09/06/02 12:37:22

21.7 190,4 48.2 46.5 09/06/02 12:37:32

21.6 191.1 48.4 46.7 09/06/02 12:37:42

21.7 191.8 48.7 47.0 09/06/02 12:37:52

21.8 192.3 49.0 47,1 09/06/02 12:38:02

21.6 192.7 49.1 47.2 09/06/02 12:38:12

21.6 193.2 49.3 47.3 09/06/02 12:38:22

21.7 193.6 49.4 47.3 09106/02 12:38:32

21.7 194.1 49.5 47.4 09106/02 12:38:42

21.8 194.3 49.7 47.5 09/06/02 12:38:52

21.8 194,6 49.8 47.6 09/06/02 12:39:02

21.7 194.8 50.0 47.6 09/06/02 12:39:12

21.8 194.7 50.2 47.8 09/06/02 12:39:22

21.7 194.8 50,3 47.7 09/06/02 12:39:32

21.7 194.8 50.5 47.8 09/06/02 12:39:42

21.8 194,8 50.6 47.9 09/06/02 12:39:52

21.7 195.3 50.7 47.9 09/06/02 12:40:02

21.8 195.4 50.9 47.9 09/06/02 12:40:12

21.7 195.7 50,9 48.0 09/06/02 12:40:22

21.8 195.8 50.9 47.9 09/06/02 12:40:32

21.6 195.9 51.0 47.9 09/06/02 12:40:42

21.7 195.8 51.1 48.0 09/06/02 12:40:52

21.7 195.8 51.1 48.0 09/06/02 12:41:02

21.8 195.7 51.1 48.0 09/06/02 12:41:12

21.7 196.6 51.1 48.0 09/06/02 12:41:22

21.4 197.0 51.0 48.1 09/06/02 12:41:32

21.5 197.2 51.0 48.1 09/06/02 12:41:42

21.6 197.5 51.1 48.1 09/06/02 12:41:52

21.5 197.7 51.2 48.0 09/06/02 12:42:02

21.5 197.9 51.2 48.0 09/06/02 12:42:12

21.5 197.8 51,2 46.0 09/06/02 12:42:22

21.3 197,6 51,3 48.0 09/06/02 12:42:32

21.3 197.7 51.4 48.0 09/06/02 12:42:42

21.3 197.8 51.3 48.1 09/06/02 12:42:52

21.5 197.8 51.3 48.2 09/06/02 12:43:02

21.6 198.0 51.3 48.0 09/06/02 12:43:12

21.4 198.2 51.3 48.1 09/06/02 12:43:22

21.4 198.2 51.3 48.2 09/06/02 12:43:32

21.3 198.6 51.3 48.1 09/06/02 12:43:42

21.2 198.5 51.3 48.2 09/06/02 12:43:52

21.3 198.6 51.4 48.2

Page 39/6/02 Run #3

09/06/02 12:44:02

21.1 196.5 09/06]02 12:44:12

21.2 198.5 09/06/02 12:44:22

21.2 198.4 09106/02 12:44:32

21.3 198.4 09/06/02 12:44:42

21.2 198.4 09/06/02 12:44:52

21.2 198.5 09/06/02 12:45:02

21.3 198.5 09/06/02 12:45:12

21.3 198.4 09/06/02 12:45:22

21.4 198.5 09106/02 12:45:32

21.2 198.5 09/06/02 12:45:42

21.3 198,5 09/06/02 12:45:52

21.4 198.4 09/06/02 12:46:02

21.3 198.4 09/06/02 12:46:12

21.3 198.4 09/06/02 12:46:22

21.3 198.4 09/06/02 12:46:32

21.2 198.3 09/06/02 12:46:42

21.1 198.4 09/06/02 12:46:52

21.3 198.5 09/06/02 12:47:02

21.2 198.4 09/06/02 12:47:12

21.0 198.4 09/06/02 12:47:22

21.1 198.2 09/06/02 12:47:32

20.9 198.1 09/06/02 12:47:42

20.9 198.1 09/06/02 12:47:52

20.8 198,1 09106102 12:48:02

20.9 198.1 09/06/02 12:48:12

20.8 198.'1 09/06/02 12:48;22

20.9 198.1 09/06/02 12:48:32

20.9 198.1 09/06/02 12:48:42

20.8 198.0 09/06/02 12:48:52

20.9 198.0 09/06/02 12:49:02

20.8 198.0 09/06/02 12:49:12

20.8 197.9 09/06/02 12:49:22

20,8 198.0 09/06/02 12:49:32

20.8 197.8 09/06/02 12:49:42

20.7 197.8 09/06/02 12:49:52

20.7 197.7 09/06/02 12:50:02

20.7 197.5 09/06/02 12:50:12

20.7 197.6 09106102 12:50:22

20,8 197.5 09/06/02 12:50:32

20.8 197.2 09/06/02 12:50:42

20.8 197.1 09/06/02 12:50:52

20.9 197.2 09/06/02 12:51:02

20.8 197.0 09/06/02 12:51:12

20.8 197.0 09/06/02 12:51:22

20.7 196.8 09/06/02 12:51:32

20.8 196.8 09/06/02 12:51:42

20.5 196.8 09/06/02 12:51:52

20.5 196,6 09/06/02 12:52:02

20.5 196.6 09/06/02 12:52:12

20.5 196.5 09/06/02 12:52:22

20.4 196.2 09/06/02 12:52:32

20.5 196.2 09/06/02 12:52:42

20.3 196.2 09/06/02 12:52:52

20.2 196.0 09/06/02 12:53:02

20.2 195.9 09/06/02 12:53:12

20.1 195.8 09/06/02 12:53:22

20.2 195.7 09/06/02 12:53:32

20.2 195.6 09/06/02 12:53:42

20.3 195.2 09106/02 12:53:52

20,1 195.1 09/06/02 12:54:02

20.0 195.1 09/06/02 12:54:12

20.1 194.9 09/06/02 12:54:22

20.0 194.8 -09/06/02 12:54:32

19.9 194.8 09/06/02 12:54:42

19.9 194.5 09/06/02 12:54:52

20.0 194.6 09/06/02 12:55:02

20.0 194.4 09/06]02 12:55:12

19.9 194.3 09/06/02 12:55:22

19.7 194.4 09/06/02 12:55:32

19.9 194.5 09/06/02 12:55:42

19.9 194.5 09/06/02 12:55:52

19.8 194.4 09/06/02 12:56:02

19.9 194.4 09/06/02 12:56:12

19.8 194.4

51.3 48.1 51.4 48.2 51,4 48,2 51.5 48.2 51.5 48.'1 51.4 48.2 51.5 48.2 51,5 48.2 51.6 48.2 51.5 48.2 51.5 48.3 51.6 48.2 51.6 48.2 51.6 48.2 51.6 48.2 51.6 48.2 51.6 48.2 51.6 48.2 51.6 48.2 51.7 48.2 51.7 48.1 51.6 48.1 51,5 48.1 51.6 48.2 51.8 48.1 51.7 48.1 51.7 48.1 51.7 48.2 51.7 48.1 51.7 48.2 51.8 48.2 51.9 48.2 51.9 48.2 51.9 48.2 51.9 48.2 51.8 48.2 51.8 48.2 51.8 48.1 51.8 48.1 51.7 48.1 51.8 48.1 51.9 48.1 51.8 48.1 51.9 48.1 51.9 48.0 51.9 48.0 51.8 48.1 51.8 48.0 51.7 48.0 51.7 48.0 51.7 48.0 51.7 48.0 51.7 47.9 51.6 48.0 51.5 48.0 51.5 48.0 51.5 47.9 51.5 47.9 51.5 47.9 51.4 48.0 51.4 47.9 51.5 47.9 51.4 48.0 51.4 47.9 51.4 47.8 51.4 47.9 51.4 47.9 51.5 47.8 51.4 47.8 51.4 47.8 51.4 47.9 51.4 47.9 51.4 47.9 51.4 47.8

Page 4 399/6102 Ru• #3

09/06/02 12:56:22

19.8 194.4 51,4 47.9 09/06/02 12:56:32

19.8 194.3 51.4 47.9 09/06/02 12:56:42

19.8 194.3 51.4 47.7 09/06/02 12:56:52

19.8 194.1 51.4 47.8 09/06/02 12:57:02

19.7 194.1 51.4 47.8 09106/02 12:57:12

19,7 194.0 51.4 47.8 09/06/02 12:57:22

19.6 193.9 51.5 47,7 09/06/02 12:57:32

19,6 194.0 51.4 47.7 09/06/02 12:57:42

19.5 193.8 51.4 47.7 09/06/02 12:57:52

19.4 193.7 51.4 47.7 09/06/02 12:58:02

19.4 193.7 51.4 47.7 09/06/02 12:58:12

19.3 193.7 51.4 47.7 09/06/02 12:58:22

19,4 193.6 51.3 47.7 09/06102 12:56:32

19.4 193.5 51.3 47.7 09/06/02 12:58:42

19.3 193.5 51.2 47.6 09/06/02 12:58:52

19.3 193.4 51.2 47.6 09/06/02 12:59:02

19.3 193.4 51.2 47.6 09/06/02 12:59:12

19.2 193.3 51.1 47.6 09/06/02 12:59:22

19.3 193.3 51.2 47.6 09106/02 12:59:32

19.3 193.4 51.3 47.6 09/06/02 12:59:42

19.3 193.2 51.2 47.6 09/06/02 12:59:52

19.2 193.2 51.2 47.6 09/06102 13:00:02

19.2 193.2 51.1 47.5 09/06102 13:00:12

19.2 193.3 51.0 47.6 09/06/02 13:00:22

19.2 193.2 51.1 47.6 09/06/02 13:00:32

19.1 193.1 51,1 47.5 09/06/02 13:00:42

15.3 193.1 51.1 47.5 09/06/02 13:00:52

11.7 193.0 51.0 47.5 09/06/02 13:01:02

12.1 192.9 51.0 47.5 09/06102 13:01:12

12.6 192.8 50.9 47.3 09/06102 13:01:22

12.8 190.7 50,8 46.1 09/06/02 13:01:32

13,3 185.3 50.3 44.5 09/06/02 13:01:42

15.6 178.1 49.3 43.0 09/06/02 13:01:52

19.3 172.3 47.8 41.9 09/06/02 13:02:02

20.0 166.8 46.1 41.0 09/06/02 13:02:12

18.1 162.4 44.5 40.4 09/06/02 13:02:22

14.7 159.3 42.8 40.0 09/06/02 13:02:32

19.9 156.8 41.5 39.3 09/06/02 13:02:42

23.1 152.8 40.2 38.7 09/06/02 13:02:52

22.8 148.4 39.2 37.9 09/06/02 13:03:02

22.7 145.5 38.3 37.6 09/06/02 13:03:12

22.6 147.1 37.4 38.4 09/06/02 13:03:22

22,5 153.5 37.0 39.8 09/06/02 13:03:32

22.1 160.9 37.2 41.3 09/06/02 13:03;42

22.2 168.8 38.0 42.5 09/06/02 13:03:52

22.1 174.8 39.0 43.5 09/06/02 13:04:02

22.2 179.1 40.4 44.2 09/06/02 13:04:12

22.3 182.9 41.7 44.7 09/06/02 13:04:22

22.3 186.0 42.7 45,1 09/06/02 13:04:32

22.5 188.6 43.8 45.4 09/06/02 13:04:42

22.3 190.6 44.7 45.6 09/06/02 13:04:52

22.2 192.4 45.5 45.8 09/06/02 13:05:02

22.2 193,3 46.0 46.0 09/06/02 13:05:12

22.2 194.0 46.7 46.1 09/06/02 13:05:22

22.2 194.7 47.2 46.3 09/06/02 13:05:32

22.2 195.6 47.6 46.4 09/06/02 13:05:42

22.2 196.3 47.9 46.5 09/06/02 13:05;52

22.3 197.1 48.3 46.5 09/06/02 13:06:02

22.4 197.6 48.7 46.7 09/06/02 13:06:12

22.4 198.2 48.9 46.8 09/06/02 13:06:22

22.3 198.6 49.1 46.8 09/06/02 13:06:32

22.2 198.9 49.2 46.9 09/06/02 13:06:42

22.3 199.3 49.2 47.0 09/06/02 13:06:52

22.2 199.7 49.3 47.0 09/06/02 13:07:02

22.3 200.1 49.5 47.2 09/06/02 13:07:12

22,4 200.2 49.6 47.2 09/06/02 13:07:22

22,5 200.6 49.7 47.2 09/06/02 13:07:32

22.3 200.8 49•9 47.3 09/06/02 13:07:42

22.2 201.2 49.9 47.3 09/06/02 13:07:52

22.2 201,3 49.9 47.4 .09/06/02 13:08:02

22,1 201.8 50.0 47.4 09/06/02 13:08•12

22.1 201.7 50.1 47.4 09/06/02 13:08:22

22.3 201.8 50.2 47.4 09/06/02 13:08:32

22.1 202.0 50.3 47.4

Page 59/6/02 Run #3

09/06/02 13:08:42 09/06/02 13:08:52 09106/02 13:09:02 09/06/02 13!09:12 09/06/02 13:09:22 09/06/02 13:09:32 09/06/02 13:09:42 09/06/02 13:09:52 09/06/02 13:10:02 09/06/02 13:10:12 09/06/02 13:10:22 09/06/02 13:10:32 Stop Run #3

09/06/02 13:10:42 09/06/02 13:10:52 09/06/02 13:11:02 09/06/02 13:11:12 09/06/02 13:11:22 09/06/02 13:11:32 09/06/02 13:11:42 09/06/02 13:11:52 09/06/02 13:12:02 09/06/02 13:12:12 09/06/02 13:12:22 09/06/02 13:12:32 09/06/02 13:12:42 09/06/02 13:12:52 09/0,6/02 13:13:02 09/06/02 13:13:12 09/06/02 13:13:22 09/06/02 13:13:32 09/06/02 13:13: 42 09/06/02 13:13:52 09/06/02 13:14:02 09106/02 13:14:12 09/06/02 13:14:22 09/06/02 13:14:32 09/06/02 13:14:42 09/06/02 13:14:52 09/06/02 13:15:02 09/06/02 13:15:12 09/06/02 13:15:22 09/06/02 13:15:32 09/06/02 13:15:42 09/06/02 13:15:52 09/06/02 13:16:02 09/06/02 13:16:12 09/06/02 13:16:22 09106/02 13:16:32 09/06/02 13:16:42 09/06/02 13:16:52 09/06102 13:17:02 09/06102 13:17:12 09/06/02 13:17:22 09106/02 13:17:32 09/06/02 13:17:42 09/06/02 13:17:52 09/06/02 13:18:02 09/06/02 13:18:12 09/06/02 13:18:22 09106102 13:18:32 09/06/02 13:18:42 09/06/02 13:18:52 09/06/02 13:19:02 09/06/02 13:19:12 09106/02 13:19:22 09/06/02 13:19:32 09/06102 13:19:42 09/06/02 13:19:52 09/06/02 13:20:02 09/06/02 13:20:12

22.0 22.0 21.9 22.0 21.9 21.8 22.0 21.9 21.8 21.8 21.7 21.7

19.14

17.15.45.24.6 3,8 2.92.42,3 2.12.02.01.91.81.71.71.71.61.61,61.61.51.51.51.51,51.51.51.41.41.41.41.4;4 1.41.41.41.41,41.41.41.41.41.41.41.53,54.0
4.03.01,51.51.51.41.41.41.41.41.4 202.2 202.5 202.8 203.0 203.1 203,3 203.6 203.7 203.7 204.0 204.1 204.1

191.26

204.0 202.3 202,4 203.6 202.8 195.0 174.6 144.8 118.5 98.2 82.4 69.4 58.0 49.2 40.7 34.2 28.2 22.9 18.9 16.5 14.0 12.2 10,99.99.28,6 8.17.77.57.47.37.06.96.66.45.85.65.35.2 5.25.15.25.25.25.15.04.8
4.8
4.5
4.6 5.05.97.4 8.38.17.16.55.8 50.4 50.5 50.5 50.6 50.6 50.6 50.7 50.7 50.8 50.8 50.9 50.9

49.18

50.9 50.7 50.4 50.2 50.4 50.4 49.3 47.3 45.9 46.2 48.0 50.1 52.6 55.1 57.4 59.8 62.2 64.3 66.4 68.2 70.0 71.5 72.9 74.1 75.2 76.2 77:1 77.7 78.3 79.0 79.5 79.9 80.3 80.5 80.9 81.0 81.1 81,1 81,4 81.6 82.7 83.8 84.8 85.0 85,1 85.6 86.3 86.3 86.5 86.9 84.7 80.1 76.0 69.2 61.0 53,9 47.6 42.0 47.4 47.5 47.5 47.5 47.6 47.6 47.6 47.7 47.7 47.7 47.8 47.8

46,80

47,7 47,3 47.1 47.4 46.9 43.3 36.5 29.2 23.7 19.7 16.4 13.8 11.69.7 8.26,8 5.6 4.8 4.0 3.5 3.12.82,5 2.42.12.01.91.81.71.71.71.61.61.51.51.51.5 1.4 1.4 1.41.41.31.31.31.31.31.2
1.2
1.2
1.31.41.62.7 5.99.0 11.7 14.0 15.9

91 ppm S02

Page 6916/02 Run #3

09/06/02 13:20:22 09/06/02 13:20:32 09/06/02 13:20:42 09/06/02 13:20:52 09/06/02 13:21:02 09/06/02 13:21:12 09/06/02 13:21:22 09/06/02 13:21:32 09/06/02 13:21:42 09/06/02 13:21:52 09/06/02 13:22:02 09/06/02 I3:22:12 09/06/02 13:22:22 09/06/02 13:22:32 09/06/02 13:22:42 09/06/02 13:22:52 09/06/02 13:23:02 09/06/02 13:23:12 09/06/02 13:23:22 09/06/02 13:23:32 09/06/02 13:23:42 09/06/02 13:23:52 09/06/02 13:24:02 09/06/02 13:24:12 09/06/02 13:24:22 09/06/02 13:24:32 09/06/02 13:24:42 09/06/02 13:24:52 09/06/02 13:25:02 09/06/02 13:25:12 09/06/02 13:25:22 09/06/02 13:25:32 09/06/02 13:25:42 09/06/02 13:25:52 09/06/02 13:26:02 09/06/02 13:26:12 09/06/02 13:26:22 09/06/02 13:26:32 09/06/02 13:26:42 09/06/02 13:26:52 09/06/02 13:27:02 09/06/02 13:27:12 09/06/02 13:27:22 09/06/02 13:27:32 09/06/02 13:27:42 09/06/02 13:27:52 09/06/02 13:28:02 09/06/02 13:28:12 09/06/02 13:28:22 09/06/02 13:28:32 09/06/02 13:28:42 09/06/02 13:28:52 09/06/02 13:29:02 09/06/02 13:29:12 09/06/02 13:29:22 09/06/02 13:29:32 09/06/02 13:29:42

1.41,4 1.41.41,41,41.41.41.41.41.41,41.41.31.31.31,31,31,3
1.61.51.41.31.3 1.3 1.31.31.41,41,31.31.31.31.31,31.31.31.31,41.41.41.41.31.31.31.31.49.5
15.6 1513 15.3 15.4 15.4 15.4 13.34.34.2 5.5 5.0 4.8 4.54.03.93.63.43,2 2.82.7 2,62.3 2.52.32.22,3 2.01.9 1.71.61.61.42,67.9 17.7 30.1 42.2 53.0 61.7 69.1 74.0 78.5 82.0 84.3 86.2 87,4 88.2 88.8 89,1 89.8 90.2 90.2 90:5 90.7 90.7 91,4 91.5 9i.7 91.8 91.5 89.8 87.9 83,4 75.1 66.5 56.0 37.1 32.9 29.t 25.6 22.5 19.8 17.3 15,0 13,2 11.3 10.08.67,46.65,6 4.6 3.93.32.8 2.2
1.71,3
0.90.7 0.5 0.3 0.10.0 -0.1 -0.4 -0.6 -0,7

-1.1 -0.8
-0.3
-0.5 -0.7 -0.8 -0,5 -0,2 -0.3 -0.4 -0.4 -0.5 -0.6 -0.6 -0.6 -0.7 -0.8 -0.8 -0,8
-0.7
-0.6 -0.4 -0.10.0 17.3 18.6 19.5 20.z. 20,9 21.3 21.7 21,9 22.1 22.4 22.4. 22.6 22.6 22.7 22.7 22,8 22.7 22.8 22.8 22.7 22.8 22.8 22.8 21,9 19.5 16.4 13.3 10.78.5 6.7 5.4 4.3 3.5 3.02.5
2.1
1.8
1.71,5 1.41.4 1,3 1.21.21.21,11.0 1,01.01.01.0
1.1
1.2 1,31.51.6 1.7

25.1 DDm NOx

Zero VOC

99.4 ppm CO Zero SO2. NOx

14.7 uDm C3H8

Page 7Appendix CFILTER ANALITICAL

DATA

Company: Acme Brick, Tulsa, OK Date: 9/6/02 Location: Turnel Kiln Exhaust Run 1

Run 2
Filter ID Number

i•i i/i,i

•_•

Date of Weighing

.:•i i§•!ii•]•i

iiiiiiii•i• •i

Gross Filter Wt.

•i:•:::!,.8.i!• • Run 3

Date or Weighing

Gross Filter Wt.

0.4053

0.4044 Ave. Gross Filter Wt. 0.4071

Date of Weighing

Filter Tare Wt.

ii•)!•3i9•92

Date of Weighing

Filter Tare Wt

Ave. Filter Tare Wt.

Wt. of PM on Filter (grams) 0.4008

0.0036

3.6 0.3993

0.0061

6.1 Total Weight of Particulate

(mg) 0.3993

0.0078

7.8

43PARTICULATE ANALYTICAL

DATA FORM Company: Acme Brick, Tulsa, OK Date: 9/6/02 Location: Tunnel Kiln Exhaust Run Density (Pa)

0.0001 Blank Concentration

(Ca) Rinse Volume (Yaw) Residue in Rinse (Wa) Ca*Vaw×-Pa

Date of Weighing Time Gross Weight

Date of Weighing Time Gross Weight Run 2

0.0001

Run 3

0.0001

Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight

109.9376 0.0001 109.9049

32.62

117.504] 0.0001 117.4792

24.71 Weight of Particulate

in Rinse (mg) 103.2974 0.0001 103.2731

24.15

ACETONE BLANK ANALYTICAL

DATA FORM

Blank Volume (Va) Date of Weighing Time

Date of Weighing Time Gross Weight Average Gross Weight

101.77695

Date of Weighing Time Tare Weight

Date of Weighing Time Tare Weight Average Tare Weight

101.7767 Weight of Blank (Ma) Ca= Ma/(Va*Pa)

g/g

0.0002 1.274E.06

•lote: In no case should a blank residue greater than 0.01 mg/g or 0.001•o of the blank weight be subtracted

from the sample weight.PARTICULATE ANALYTICAL

DATA FORM Company: Acme Brick, Tulsa, OK _Date: 9/6/02 Location: Tunnel Kiln Exhaust Run 1 Density (Pa)

::iii!!::iiiiiiiiii

::i::

Run 2

Blank Concentration

(Ca) Rinse Volume (Vaw) Aliqout Volume Residue in Rinse (Wa) Ca*Vaw*Pa 0.0003

0.0003

Date of Weighing Time Gross Weight

Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight

Date of Weighing Time Beaker Tare Weight
Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate

in Rinse (mg) Total Weight of Particulate

(rag)

127.3560 0.0003 127.3467

9.02

126.0134 0.0003 126.0042

8.92 Run 3

0.0003

130.2283 0.0003 130,2180

10.02

H20 BLANK ANALYTICAL

DATA FORM

Blank Volume (Va) Date of Weighing Time Gross Weight

Date of Weighing Time Gross Weight
Average Gross Weight

129.76455

129.76435

0,0002 8E.07 Date of Weighing Time Tare Weight

Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va-'Pa)

g/g

Jote: In no case should a blank residue greater than 0,01 mg/g or 0.001% of the blank weight be subtracted

from the sample weight.PARTICULATE ANALYTICAL

DATA FORM
Company: Acme Brick. Tulsa OK Date: 9/6/02 Location: Tunnel Kiln Exhaust Run Rum 2 Density (Pa)

Blank Concentration

(Ca) Rinse Volume (Yaw) Residue in Rinse (Wa) Ca*Vaw*Pa Run 3

0.0000

Gross Weight

•:::•i!i•5•:J9•8•

::::iiii ::::199i9•8B

•::::::::ii•t#•i•i•i

Date of Weighing Time Gross Weight

:::: :::::: :7:

"iii:: i•:• •89

::::::::::::::::::::::::::::

lO6.6474 0.0000 106.6467

0.70 Date of Weighing Time Beaker Tare Weight

Date of Weighing Time Beaker Tare Weight
Average Gross Weight
Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate

in Rinse (mg)

105.9686 99.9089 0.0001 0.0000 105.9673 99.9080

],24 0.85

METHYLENE CHLORIDE

BLANK ANALYTICAL

DATA FORM

Blank Volume (Va) Date of Weighing Time Gross Weight

Date of Weighing Time Gross Weight
Average Gross Weight

107.69435

107.6942

0.00015 4.412•.07 Date of Weighing Time Tare Weight

Date of Weighing Time Tare Weight
Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va*Pa)

g/g

Note: In no case should a blank residue greater than 001 •ng/g or 0,001% of the blank weight be subtracted

from the sample weight. 46Sheet1
Summary of HF and HCI Analysis

Plant: Acme Brick, Tulsa, OK Location: Tunnel Kiln Exhaust Date: 9/6/02

Run # Imp # Volume 350 350 Dilution 2O2O FI-, ug/ml 25.87 25.42 Average

2 350

20 23 56 2 350

20 23.32 Average

3 350

20 24.64 3 350

20 24.97 Average

2&3 250 2&3 250

23.87 24.54 Average

2 2 & 3

250

23.93 2 2 & 3

250

24.36 Average

3 2 & 3

250 3 2 & 3

250

22.04 22.36 Average

Totals Run #1 Run #2 Run #3

HF, mg 190.6878 187.3708 189.0293

173.6608 171.8917 172 7762

181.6214 184.0539 182.8377

6.283778 6.460155 6.371966

6.299573 6.41277 6.356171

5.80203 5.88627 5.84415

195.4013 179.1324 188.6818 Clo, ug/ml6.94 6.61

44.25

6.59 5.99

5.3 5.62

4.39 4.25

4.82 4.58 HCI, mg 49 94024 47.56556 48.7529

30.51404 30.583 30.54702

47.42164 43.10404 45.26284

1.3621 1.44434 1.40322

1.12823 1.09225 1.11024

1.23874 1.17706 1.2079

50.15612 31.65726 46.47074

PageConditions 5 ug/ml

CIDate 09/07/2002 Time

Compollent -102.400mV 1024.000mV Retention

•ll 1.1oo t•::::ii ,450 376.25 255.50

External

4.21 3Conditions : 4.£2 u nl

Date 0£/07/2002 Time 08:25:07

Component

Ct- -102.400mV Retention

1,450

51,/ i024.000mV

380,40 257.75

External

4.94 5,01

J•-, 49Conditions

DaLe 09/07/2002 Time 08:32:14

FIColilpo r•eIIT•

-102 o400mV 1024.000mV Retent io,,1

1,100 1.450 :::::::::::::::::::::::::::

5 •rea

725.95 502.85

External

8.70 8,13ComponentConditions 9.84 u nl F1- lO,ug/m• C1- Date 09/07/2002 Time 08:34:41

-102 .#-OOm•J 1024 oO00mV Retention

763.80 548.70

External

10.03 10,31Conditions 24•6 u •IFI25 ug/n•

CIDate 09/07/2002 Time 08:41:49

FIComponent

-•.02.400mV 1024.000mV Retention

I.II•

1.550

2 I942,20
1460,70

External

25,9i

27.37Conditions 24.6 c mLFL25 u9/•1

C1- Date 09707/2002 Time 08=44:16

--202.400mV Retention 102•. O00mv

1.116
1.550

231 External

24.86 25,03

53Conditions 49.2 u •1 F1-

Date 09/02"/2002 Time 09:01•20

FI•

CI- -202 •400mV 1024.000mV Reten[£on

.150[

.533

2

3798.03 3376.9,9

46.83
55,67Conditions

Date 09/07/2002 T•e O9:O3:55

-•., 02 400mV Component -Retention (unknown) •L024 O00mV o.133/. ..: ..............................................................................................................................................................................................................................................................

1.516{

:.1 152.20

3774.90 3301,65

48.89 49,02

$5Calibration file

F .cal

AMOUNT INJECTED AREA -0.000 49.200 0.000,.,

....

460 " 3786 r. ::::,I 1

2

3

5

Avg slome

of curve:

77.01 Y-axis intercept:

0_00 Coeff of J. in regr"

0.93

No. Area

Amount

CF

O: 0.000

0.000

0.000 1: 378.325

4.920

'76.895 2: 744.875

9.840

75.699 3• 1963.250

24.600

79.807 4: 3786•465

49.200

76.961Calibratio• file

AMOUNT INJECTED AREA 0o000 50•000 0..000::::"....,.:.,,...,,.,....,....

3339H32o

12

3

5

Avg slope

of curve:

60.66 Y-axis •ntercept:

0•00 Coeff• 0"• fin •egT•

0.81

No. Area

Amount

CF

O= 0.000

O.O00

0•000 l: 256.625

5.000

51.325 2: 525.775

lO.O00

52.578 3: I461-800

25.000

58.472 4• 3339.320

50_000

66.786

57Conditions Acme 8• ;k, Tulsa,

OK Run #i Imp #i Volume 350 mls Dilution

1/20 bale 09/07/2002 Time 09:1•,:18

ClComponent

:i, 02, 400m•Y • 02•¢ O00mV Retent,•.on

1.550[

2057.05 361,32

ExteFn•1

25.87
6.94

58Condi£ions Aome B ;1<, Tulsa,

OK Run #1-•mp

#1 :Voiume 350 mls Dilution

1/20 Date '09/07/2002 Time 09:13=39

Component -102.4OOrnV iO24.000mV Retent•0n

1.550

A•ea

2024.08 343,52

External

59Conditions Acme B. ok, Tulsa,

OK Run #2•mp

#I. Volume 350 mls Dilution

L/20 Date 09/07/2002 Time 09:20;35

ClComponent

--102.400mV t024 .O00mV Retention

133 ;,,...I ................................................................................. .5.•,01 1877.00

217.50

External

6OConditions Acme B ck• Tulsa,

OK Run #2-Imp

#$ Volume 350 mis Dilution

1/20 Date 09/07/2002 Time 09:30:27

Component

C1- -i02.400m.V 1024.000mV •etent[0n

1500 '•' i857,60 217.95

23.32 4.25Conditions Acme 5 ok, Tulsa,

OK Run #3•imp

#1 Volume 350 mls Dilution

1/20 Date 09/07/2002 Time 09133:24

FIelCo mDol]ell[,

-•1,02.400mV 1024 oO00mV Retenti0•

i. 15C

,, 1.550 ......... 1966.30

342.40

Ex.ternal

24

6Conditions Acme B •k, Tulsa,

OK Run #3 Imp #1 Volume 350 mls Dilutiol•

1/20 Date 09/07/2002 Time 09:35=55

,Coraponent

FICI- -102.400mV Retention

1.550 1024.000rnV

qrea

1990.80
309.80

External

63Conditions Acme B ok, Tulsa,

OK

: Run #l•[mp

#2 & #3 Volume 250 mls Dilution

1/1 Date 09/07/2002 Time 09:39:I8

Component

.15,

.55• -102.400mV 102• ,O00mV Retentlor.

ATea

1902.67
272.51

ExteFna1

23.87 5,30ClRun #l Imp #2 & #3 Volume 250, mls DilutiO•

$/$ Date : 09/07/2002 Time 09:41:32

Component -102.400mV Retent•o LO24.000m•/

Area

1957,95 M 290,07 M External

65Condition• Acme B ol(, Tul•a,

OK Run #2•2mp

#2 & #3 Volume 250 mls Dilution

i/i Date 09/07/2002 Time 09=48:10

Compo#ent -i02 •400mV •i024,000mV Retentio

Area

1907.55 225,20

External

23.93 4,39ConditioT•s Acme B ck.• Tulsa,

OK Run #2 Imp #2 & #3 Volume 2SO mls Dilution

I/I Date 09/07/2002 Time 09:50:39

ClConIponent

-102.400mV 1024.000mV Retenti01•

1943,10
217.90

ExternalConditions Acme B ok, Tulsa•

OK Run #3•mp

#2 & #3 Volume 250 mls Dilution

1/1 Date 09/07/2002 Time 09:57:20

Component

01- -102.400mV .1. 024 •O00mV Retenti0..q11

1.566: External

68Coaditions Acme B_.ck,

Tulsa,

OK Rub #3 Imp #2 & #3 Volume 250 mls Dilution Date : 09/07/2002 Time 09:59:35

Component

FIC1 --102 •4OOmV $024.000mV Retention

2:2211121',227,',:',:2',IIC',:;::::::::,

1.550

3 ,•fea

1778.54

234.88

External

69Conditions Acme. B ok,, Tulsa,

OK

= H2OBI•I( Date 09/07/2002 Time

Component 102,,400mV i024.000n]V Retention

Alea

External

7O= H2S04

Blank Date 09/07/2002 Time i0:08:29

-102.400ram 1024,0OOrnV Retention ExternalConditions Acme E ok, Tulsa,

OK 24.6. u•?ml

F1 2S ug/ml

C1 Da£e 09/07/2002 T•me 10:10:58

Component

72Appendix D_-2

LOCATION

(SOURCE OPE•TOR: &•

•TER BOX #:/•

P•-T•ST LE• CIECK FIELD DATA

r/WPINGERS Initial Final

#4• TT,

POST-TEST LEAK CHECK Meter: o,co cu.ft,

in. HG Pitots." •--

•20FIELD DATA

IMPYNGERS Initial #1 /z ,•

#5 2 •

co•FIELD DATA

C02 Final

li •

02

POST-TEST LEAK CHECK Meter: o. o cu.ft

HG Pit0ts: •

H20
6/0. Oo 0

7•,, •Appendix E0

UJ

• •dd

6dddo

©© g•oddddMeter

Box #:

10 Date: 8/12/02 Calibrated By:

RT

Emtech Thermo Degrees F

Checker

Probe

Stack

Oven

Exit Auxiliary
Point 32

31

31

31

30

31
Point 2

212

211

211

210

211

210 Point 3

752

750

751

750

750

750

Degrees R

Poinl

Point 2

Point 3

Percent Difference

Point

Point 2

Point 3

Emtech Thermo Checker

Probe

Stack

Oven

Exit Auxilla•

492 491

491

491

490

491

672 671

671

670

671

670

1212 1210

1211

1210

1210

1210

Probe

0.203252

0.14881

0.165017 Stack

0.203252

0,14881

0.082508

Oven

0.203252

0.297619

0.165017

Exit

0.406504

0.14881

0.165017 Auxilta•

0.203252

0.297619

O.165017

?778Appendix FDate: CERTiFiCATE of ANALYSTS
Interference-Free Multi-Component

EPA Protocol Gases Cy Document Number: 1900psig 10368234 Expiration Date:

Item Number:

klitric Oxide

25 ppm

24.6 =L-0.5 ppm 05/14/02 05/13/04 Custorner: P.O. Number:

Notes: Environmental Total NOX "Mixture is valid

psig 25.1 ppm Nitrogen Balance

Balance

cal uncertainty andNIST traceability are ih compliance with EPA-600/R-97/123

GMIS 175 GMIS 175 54.9 ppm

0.7

NO N2 CC122371

04/21103

N.A.

Manufacturer: KVB/An.alect

Manufacturer: Manufacturer: Model Number:

EN3024

Model Number: Model Number: r: 3024 Number: Serial Number: Principle: FTIR Principle: VIPC Calibrated:

04/09/02 & 05/09/02

MPC Calibrated: p•e:

Air •.iquide America Corporation 11426 Fairmont Parkway, La Porte, Texas 77571-6000 Phone: (281) 474-8400 Fax: (281) 474-8419
?9--II•yl. Number:

Cyl, Pressure:, II.q ;C49028

1900psig I•'•.ssay Date:

' Expiration Date: 1105/14/02 05/13/04 IICustomer: P,O. Number

Notes: ILArmstrong Environ mental /r*'Mixture is valid onl' 50 psig

CERTIFICATE. of ANALYSIS
Interference-Free Multi-Component

EPA Protocol Gases Document Number: 10368234 item Number:

.e. r•i.n.ty traceability a•e in compliance with EPA-600/R-97/123

GMIS1,,75

GMIS175

54.9 ppm

0.7

NO N2 cci22371

04121/03

N.A,

........................................................................................................................... ,.,..,

Manufacturer: KVB/Analect

Manufacturer: r: Model Number:

EN3024 Number: Model Number: Serial Number:

3024

Serial Number: r: Principle: FTIR pie: Principle: MPC Calibrated:

04/09/02 & 05/09/02

MPC Calibrate•: • MPC Calibrated:

ComBonent

Nitric Oxide

Analys

/

Air Liquide America Corporation 11426 Fairmont Parkway, La Porte. Texas 77571-6000 Phone: (281)474-8400

Fax: (281; 474-8419
8OCERTIFICATE of ANALYSIS

Interference-Free Multi-Component

EPA Protocol Gases --•Cyl. Number: CC122083 Assay Date: 07/31/01.

Expiration Date:

Item Number: Carbon Monoxide

100 ppm

99.4 •1.7 • 07/30104 P.O. Number:

Notes: Nitrogen

Balance

Balance Customer: Armstrong "Mixture is valid only to 150 psig

NOTE: Analytical uncertainty and NIST lraceability are in compliance with EPA-600/R-97/123

Manufacturer: KVB/Analect

JlManufacturet= IIManufacturer: Modal •umber:

EN3024

I/Mo"el Number: /IModel Number: Serial Number:

3024

J•Serial Number: Serial Number: Analytical Princiole:

FTIR

J•Analytical Princ[• J•Analytical Principle: •MPC Calibrated:

07/05/01

I•MPC Calibrated: •MPC Calibrated:

110.25 110.23

110.74 •ili•

Cornponent

107.98 107,49

108.17

Carbon Monoxide 99.57 99.11

99.74

Air Liquide America Corporation 11426 Fairmont Parkway, .a Porte, Texas 77571-6000 Phone: (281) 474-8400 Fax: (281) 474-8419LiQUiDE

TM CERTiFiCATE of ANALYSIS
Interference-Free Multi-Component

EPA Protocol Gases Cyl. Pressure:*

Document Number: 1900psig 9225974 Expiration Date:

Item Number:

CarbonMonoxide08/23/04 Cyl, Number: I[CC36022 IXse.y D,te: I08/24101 --IOustomer:

P.O. Number: I[Armstrong I*Mixtu•e is valid only to 150 psig

Notes: 200 ppm

I99 +3 ppm

Balance Balance

NOTE: Analytical uncertainty and NIST traceability are in compliance with E PA-600/R-97/123 GMIS113 GMIS113

248.0 ppm

2.0

CO N2 CC64210

12/14/02

N.A.

|JManufacturer. KVB/Ana)ect

/Manufacturer" IMa |]Model Number:

EN3024

IModel Number: IMoi•aNC[uUmr•r•r iSerial Number:

3024

ISerial Number: IJSerial Number __Analytical, Principle:

FTIR

IAnalytical Principle: IIAnalytical Principle" I•IPC Calibrated:

08/06/01

•PC Calibrated: IIMPc Calibrated"

266.07 266.60

267.38 •

Component

213.80 212.79

213 54

Carbon Monoxide

Analyst:

Air Liquide America Corporation 426 Fairmont Parkway, La Porte Texas 77571-6000 Phone: (281) 474-8400 Fax: (281) 474-8419.--iiCYl. Number:

Cyl. Pressure:* •C,15056 1900psig, Assay Date:

Expiration Date: 01/29/01 01/29/03 Customer: P,O. Number: •mstrong II*Mixture is valid only to 150 psig

CERTIFICATE of ANALYS S
Interference-Free Multi-Component

EPA Protocol Gases Document Number: 7628314 Item Number:

Notes:

Nitrogen

Balance50 ppm

52.2 ±0.8 ppm

Balance

NOTE: Analytical uncertainty an• NIST •pliance with E PA-600/R-97/123 GMIS116 GMIS116

50.3 ppm

0.7

SO2

N2 CC68565

01/27/02

N.A.

KVB/Analect Model Number:

EN3024 }erial Number:

3024. •,nalytical Princl ole: FTIR JIM PC

01/11/01 Calibrated:

Manufacturer: Manufacturer: Model Number: Model Number: Serial Number: Seriai Number: Principle: Analytical Principle: MPC Calibrated: MPC Calibrated:

50.47 50.59

50.27

Component

Sulfur Dioxide 0.05 0 12 0.27 50.08 50.38

50.23

51.96 51.96

52.31

Air Liquide America Corporation 1429 Fairmont Parkway, La Porte, Texas 77571-6000 Phone: (281) 474-8400 Fax: (281) 474-8419LJQUIDE

TM CERTIFICATE of ANALYSIS

'Mixture is valid only to 150 psig len

Balance

Balance

NOTE: Analytical uncertainty and NIST raceabJlity are in compliance with 'PA-600/R-97/123

GMIS 116 GMIS 116 50.3 ppm

0,7

SO2

N2 CC68565

01/27/02

.................................................................................................. •

,__.

Manufacturer; KVB/Analect Manufacturer: Model Number:

EN3024

Model Number: Model Number: erial Number:

3024

Serial Number: Serial Number: Principle: FTIR

Z•nalytlcal Principle: Analytical Princip]e: MPC Calibrated:

O1/11/O"

k4PC Calibratea. MPC Calibrated:

Analyst: /

Air Liquide America CorBoration 11426 Fairmom Parkway, La Porte. Texas 77571-6000 Phone: (281; 474-8400 =a×' (281) 474-8419Ctyl. Number: 3C20147Date:

Customer: CERTIFICATE of ANALYSIS Interference-Free Multi-Component

EPA Protocol Gases Cyl. Pressure:*

Document Number: 1900psig 9062262 Expiration Date:

Item Number: Propane 50 ppm 08/06104 P.O. Number:

Notes:

*Mixture is valid BalanCe

Balance

NOTE: Analytical uncertainty and NIST traceability are in compliance with EPA-600/R-97/123

SRM14

1666b

9.69 ppm

0',1 C3H8

Air CLM-O05016

04/18/07

84-31-G

•erial Number: pie: Caibrated:

HP

Manufacturer: 6890 Number: Number: 8295 Serial Number: Serial Number: GO.FIB Analytical Principle: Principle: 08/01/01 MPO Calibrated: MPC Calibrated:

Air Liquide America Corporation 11426 Fairmont Parkway, La Porte, Texas 77571-6000 Phone: (281) 474-8400 Fax: (28I) 474-8419 £5-•[•

AiR LIGUIDE•

Cyl. Number: Ilcc114931 /IAssay •ate: /105/i 3/02 IIcustomer; •--JlArmstrong Envionmental CERTIFICATE of ANALYSIS
Interference-Free Multi-C0mponent

EPA Protocol Gases

Notes:
IIAir Cyi. Pressure:* 1900psig Expiration Date: 05/12/05 P.O. Number:

traceability are in Compliance with EPA-600/R-97/123 Balance

Balance

SRM64 1668b

98.8 ppm

0.5 C3H8

Air CAL-010986

11/21/02

82-1-04

...........................................................................................................................................

Vlanufacturer: HP Model Number:

6890 Serial Number:

8295 Analytical Principle:

GC-FID MPC Calibrated:

05/13/02

Manufacturer: Manufacturer: Model Number: Model Number: Serial Number: Serial Number: pie: pie: MPC Calibrated: MPC Calibrated:

27.41 27.34

27.28

Component
Propane

Air Liquide America Corporation 11426 Fairmont Parkway, La Porte, Texas 77571-6000 Phdne: (281) 474-8400 Fax: (281) 474-8419

•6- AIR

LiQUiDE

-TM CERTIFICATE of ANALYSIS
Interference-Free Multi-Component

EPA Protocol Gases Number: Cy!. Pressure:*

Document Number: lC•90523 1900psi•

•0622•2 IAssay Date:

Expiration Date:

item Number: !08/07/01 08/06/04 "--I•Customer: P.O. Number:

Notes: IIArmstrong JlAir "*Mixture is valid only to 150 psig

'traceability are in compliance with ;EPA-600/R-97/'123 Balance

Balance

SRM14 1666b

9.6• I•

6"i• ••1•"•

•i• •' [• :••••:•"::':';:::••:•:•)•'•

]lMan•,fneturer: HP

IIM"nu•acturer: I]• •,••t;•i'd ;'#;;

Serial Number:

8295

•JSeria] Number: JJSerial Number: __Analytical Principle:

GC.FIB

IIAnelylical Principle: •Analytical Principle: ]IMPC "Calibrated:

08/01/01

IIMPc Calibrated: IIMPC Calibrated:

Component
Propane

Air Liquide America Corporation I426 Fairmont Parkway, La Porte, Texas 77571-6000 Phone: (281) 474-8400 Fax: (281) 474-8419