Exhaust Emissions Sampling 

Acme Brick, Tulsa, OK 

Tunnel Kiln Exhaust 

September 6, 2002 

Armstrong Environmental, Inc. 

Project W-2222-02 

Report Prepared For" 

Mike O'Conner 

Acme Brick 

2821 West Seventh Street 

Ft. Worth, TX 76107 

Report Prepared September 12, 2002 By: 

Armstrong Environmental, Inc. 

7715 Sovereign Row 

Dallas, Texas 75247 

(214) 631-0021 
TABLE OF CONTENTS 

I, Introduction 

12. Summary 

II2. Procedures 

IV. Appendices 

A. Calculation Summaries 

B. Continuous Emissions Monitor Summaries 

C. Analytical Summaries 

D. Field Data Sheets 

E. Equipment Calibrations 

F. Standard Gas Certifications 

Page 

1 

2-3 

4-7 

8-10 

12 42 

43 72 

73 75 

76 78 

79 87 
I. INTRODUCTION 

A series of tests was performed on the exhaust associated with the Tunnel Kiln at the Acme Brick facility in Tulsa, OK on September 6, 2002. 

The purpose of this test series was to determine the exhaust emission rate of PM, CO, NOx, VOC, SO2, HF and HC1 in terms of lbs/hr. 

Testing followed procedures detailed in Title 40: Code of Federal Regulations (40:CFR). 

Sampling was performed by Bart Tarbell, Richard Taylor and Tom Armstrong of 

Armstrong Environmental, Inc using an Apex Method 5 sampling train, a Fuji 3300 continuous CO analyzer, an EcoPhysics 70S continuous NOx analyzer, a Western 

Research 721 AT continuous SO2 analyzer, and a ThermoEnvlronmental Model 51 

continuous FIX) anaIyzer. 

Three one hour test repetitions were performed, commencing at 9:20 AM and ending at 

1:11 PM. 

Submitted by: 
II. SUMMARY 

A series of tests was performed on the exhaust associated with the Tunnel Kiln at the 

Acme Brick facility in Tulsa, OK on September 6, 2002. 

Sampling was performed following procedures detailed in Title 40: Code of Federal 

Regulations. 

Results of this test series are summarized in Table 1. 

Results indicate the following emissions rates: 

PM, lbs/hr 2.906 2.272 2.551 2.576 

CO, lbs/hr 17.65 16.87 16.39 16.97 

NOx, lbs/hr 7.178 6.774 6.629 6.844 

VOC, lbs/hr 

SO2, lbs/hr 

HF, lbs/hr 

HC1, lbs/hr 

1.935 

7.658 

11.59 

2.976 

1.966 

9.254 

10.69 

1.889 

2.103 

9.510 

11.28 

2.778 

2.001 

8.807 

11.19 

2.548 

i 

\f i 

2 
SUMMARY OF EMISSIONS.TEST DATA 

Tabie: 

Plant Acme Brick, Tulsa, OK 

Location Tunnel Kiln Exhaust 

Operator R. Taylor, B. Tarbell, T. Armstrong Test Date 6.Sep-02 

Repetition 2 

STACK GAS 

Temperature, F , 452.6 467.0 Velocity, fps 40.96 40 ::)4 Volume Flow, acfm 35202.8 34420.1 scfm 18487 5 17844 5 scfh 1109252 1070672 Moisture, % 8.17% 7.90% CO2, % 3.00 3.00 02, % 17.00 17.00 

SAMPLE 

Start Time, hrs:min 9:20 AM 10:45 AM Finish Time, hrs:min 

Sample 

10:22 AM 11 '46 AM Volume, scf 41.228 39.571 Isokinetic Ratio, % 99.90021 99.3385 

PARTICULATE 

Front Half 

Sample Weight, mg 38.72 28.31 Concentration, gr/scf 0.014491 0.011039 Emissions, Ibs/hr 2.297093 1.689007 

Back Half 

S•mple Weight, mg 10.26 9.77 Concentration, gr/scf 0.00384 0.00381 Emissions, Ibs/hr 0.608682 0.58289 

Total Particulate, Ibs/hr 2.905775 2.271897 

CARBON MONOXIDE 

Concentration, ppm 218.89 216.77 Emissions, Ibs/hr 17.64932 16.87047 

NITROGEN OXIDE AS NO2 

Concentration, ppm 54 19 52 98 Em!ssions, Ibs/hr 7.178289 6.773916 

VOC AS Carbon 

Concentration, ppm as C3H8, WET 17,14 18.10 Concentration, ppm as C, DRY 55.99318 58.957 Emissions, Ibs/hr 1.934908 1.966467 

SULFUR DIOXIDE 

Concentration, ppm 41.55 52.02 Emissions, Ibs/hr 7.657641 9.253805 

HYDROGEN FLUORIDE 

Sample Weight, mg 195.40 179.13 Concentration, ppm 201.2768 192.2472 Emissions, Ibs/hr 11.59225 10.6871 

HYDROGEN CHLORIDE 

Sample Weight, mg 50.16 31.66 Concentration, ppm 28 31156 18.61829 Emissions, Ibs/hr 2.975779 1.888872 

451.5 

3982 

34222.6 

18023.2 

1081391 

8.00% 

3.00. 

17.00 

I2:10 PM 

1:11 PM 

39.8c•2 

99.15214 

31.95 

0.012358 

1.909757 

10.72 

0.004146 

0.64077 

2.550527 

208.46 

16.38616 

51 33 

6.628655 

19.14 

62.41334 

2.1O2592 

52.93 

9.509949 

188.68 

200.8662 

11.27803 

46.47 

27.10759 

2.777666 

3 
III. PROCEDURES 

The procedure for emissions sampling followed USEPA test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method Title 

Sample and Velocity Traverses for Stationary Sources 

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

Gas Analysis for the Determination of Dry Molecular Weight 

Determination of Particulate Emissions from Stationary Sources 

6C Determination of Sulfur Dioxide Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

7E Determination of Nitrogen Oxides Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

10 Determination of Carbon Monoxide Emissions from Stationary Sources 

25A Determination of Total Gaseous Organic Concentration using a Flame 

Ionization Analyzer 

26A Determination of Hydrogen Halides and Halogens Emissions from 

Stationary Sources 

02 and CO2 were determined using FyRite Analyzers. 

PM. HF and HC1 sampling was performed for 2.5 minutes at each of 24 points, 12 points 

per traverse, making a total run duration of 60 minutes. A schematic of the sampling location is shown in Figure 1. The sampling train was configured as follows: 

Glass Sampling Nozzle 

Heated Glass Lined Probe 

Heated teflon filter 

Impinger #1 100 mls H20 

Impinger #2 100 mls 0.1 N H2SO4 

Impinger #3 100 mls 0.1 N H2SO4 

Impinger #4 Empty 

Impinger #5 200 grams silica Gel 
Analysis for PM was performed on the probe wash, t•lter, and solution from the first impinger. HF and HC1 analysis was performed on an aliquot from the first impinger, and the solution from the 2nd and 3rd impir•gers. Analysis was performed using a Dionex 500DX IC/HPLC. Impinger analysis includes total solids and organics extracted with methylene chloride (extractions performed after an aliquot was taken for HC1 analysis). Teflon beakers were used for total solids analysis of the impinger solutions. 

VOC as C3H8 was determined using a ThermoEnvironmental Model 51 continuous FID analyzer. The analyzer was calibrated with 50.3 pprn, 29.6 ppm, and 14.7 ppm C3H8 in Air USEPA Protocol gas standards, zeroed with N2. 

Nitrogen Oxides were determined using a EcoPhysics 70S continuous NOx analyzer. The analyzer was calibrated with 48.8 ppm and 25.1 

standards, ppm NOx in N2 EPA Protocol 1 gas and zeroed N2. 

Carbon monoxide was determined using a Fuji 3300 NDIR continuous CO analyzer. The analyzer was calibrated with 199 ppm and a 99.4 ppm CO in EPA Protocol 1 gas standards, and zeroed with N2. 

Sulfur dioxide was determined on the scrubber exhaust using a Western Research 721 AT continuous SO2 analyzer. The. analyzer was calibrated with 91 ppm and a 52.2 ppm SO2 in N2 EPA Protocol 1 gas standards, zeroed with N2. 

A schematic of CEM contSguration is shown in Figure 2. 
// 

/ 
0 
Appendix A 
EMISSION TEST SUMMARY 

PLANT Acme Brick, Tulsa, OK 

DATE 6-Sep-02 

PLACE Tunnel Kiln Exhaust 

RUN# 

TEST DURATION (MINUTES) 

NOZZLE DIAMETER (INCH.) 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu,Ft.) 

BAROMETRIC PRESSURE 

60 LIQUID COLLECTED (mls) 

0,3127 PARTICULATE WEIGF (Front half mg) 

0.984 PARTICULATE WEIGHT (Back halfmg): 

0.84 STATIC PRESSURE(m H20): 

44,316 PERCENTC02 

29.45 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 51.25 

STACK AREA (Sq.Ft.) 14,32568 

NOZZLE AREA (feet): 0,000533 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD, CU.FT,): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR,/SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO (%): 

FOR RECTANGULAR STACK 

STACK LENGTH(inchs) 

STACK WIDTH(inchs) 

STACK AREA (Sq.Ft.) 

]4.32568 

41.2283 

3.6668 

0.0817 

80,0000 

29.1600 

28.2485 

29.5750 

40.9554 

35202.809 

1109252.08 

0.0145 

2.07E.06 

2.2971 

0.0038 

5.49E-07 

0.6087 

99.9002 

77,9 

38.72 

10.26 

1.7 

3 

17 

0 

POINTS STACKT. DELTAP SQUAR D.P 

deg 

DELTA H 

400 0.]9 0.43589 0,89 

2 408 0.22 0,469842 1,00 

3 418 0.27 0.519615 1.30 

4 430 0.28 0.52915 1.30 

5 455 0.32 0.565685 1.40 

6 458 0.34 0.583095 1.50 

7 453 0.37 0.608276 1.70 

8 440 0,34 0.583095 1.55 

9 440 0.33 0.574456 1.50 

10 438 0.31 0:556776 1.40 

11 433 0.29 0.538516 1,30 

12 377 0.42 0,648074 2.t0 

13 480 0,18 0.424264 0.78 

14 506 0,24 0.489898 1.00 

15 538 0.24 0,489898 0.98 

16 539 0.27 0.519615 1,10 

17 526 0.29 0,538516 1.20 

18 550 0.34 0.583095 1.40 

19 444 0,35 0,591608 1.60 

20 442 0.34 0.583095 1.50 

21 450 0.31 •.556776 1.40 

22 441 0.30 0.547723 ].40 

23 435 0.27 0,519615 1.20 

24 362 0.41 0.640312 2.10 

METER T, 

INLET 

84 

87 

88 

92 

93 

93 

95 

97 

96 

96 

96 

96 

95 

98 

97 

97 

97 

97 

97 

98 

98 

98 

98 

98 

METER T. 

OUTLET 

84 

84 

85 

85 

85 

85 

86 

87 

87 

87 

87 

88 

88 

89 

89 

89 

89 

89 

90 

90 

90 

90 

9O 

9O 

METER T. 

AVERAGE 

452.625 0,5457 1.3583 95.04]7 87.6250 91.3333 
EMISSION TEST SUMMARY 

PEANT Acme Brick, Tulsa, OK 

DATE 6-Sep-02 

PLACE Tuno&l Kiln Exhaust 

RUN# 2 

TEST DURATION (MINUTES) 

NOZZLE DIAMETER (INCH.) 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu,Ft.) 

BAROMETRIC PRESSURE 

60 LIQUID COLLECTED (mls) 

0.3127 PARTICULATE WEIGHT {Front half rag)" 

0.984 PARTICULATE WEIGHT (Back half rag): 

0.84 STATIC PRESSURE (in. H20): 

42.861 PERCENTC02 

29.45 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER Cinch): 

STACK AREA (Sq,Ft.) 

NOZZLE AREA (feet): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD, CU,FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT, OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO (%): 

FOR RECTANGULAR STACK 

51,25 STACK LENGTH(inches): 

14.32568 STACKWIDTH(mches) 

0.000533 STACK AREA(Sq.Ft.): 

]4,32568 

39.5707 

3.3937 

0.0790 

80.0000 

29.1600 

28.2785 

29.5676 

4C 0447 

34420,0658 

1070671.63 

0 0110 

1,58E-06 

1.6890 

0.0038 

5,44E-07 

0.5829 

99.3385 

72.1 

28,31 

9,77 

1.6 

3 

17 

0 

POINTS STACKT. DELTA P SQUARD,P 

dec 

615 0.]8 0,424264 

2 583 0.19 0.43589 

3 545 0,23 0.479583 

4 518 0.25 0.5 

5 489 0.29 0,538516 

6 478 0.33 0,574456 

7 456 0,36 0,6 

8 454 0,33 0.574456 

9 453 0.31 0.556776 

10 452 0.29 0.538516 

11 449 0.26 0,509902 

12 416 0.40 0.632456 

13 546 0,]9 0,43589 

14 530 0.19 0.43589 

15 515 0,21 0.458258 

16 481 0.25 0.5 

17 462 0.27 0,519615 

18 448 0.32 0.565685 

19 313 0.36 0.6 

20 352 0.35 0,591608 

21 338 0,31 0.556776 

22 452 0,30 0.547723 

23 448 0.26 0.509902 

24 414 0.39 0,6245 

DELTA H 

0.90 

0,75 

0.94 

1.00 

1.26 

1,40 

1.60 

1.50 

1.40 

1.30 

1,20 

1,90 

0.76 

0,79 

0.88 

1.10 

1.20 

1.40 

1.90 

1.80 

1,60 

1,40 

1.20 

1,85 

METER T 

NLET 

90 

92 

95 

96 

97 

98 

98 

99 

]00 

!00 

]00 

99 

98 

99 

99 

100 

100 

]00 

]00 

101 

]02 

102 

102 

103 

METER T. 

OUTLET 

90 

9O 

9O 

9O 

90 

91 

91 

91 

91 

92 

92 

92 

92 

93 

93 

93 

93 

93 

93 

94 

94 

95 

95 

95 

METER T. 

AVERAGE 

466.95833 0.5296 1,2929 98.7500 92.2083 95.4792 
EMISSION TEST SUMMARY 

PLANT Acme Brick, Tulsa, OK 

DATE 6-Sep-02 

PLACE Tunnel Kiln Exhaust 

RUN# 3 

TEST DURATION (MINUTES) 

NOZZLE DIAMETER (INCH.) 

METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL.(Cu.Ft.) 

BAROMETRIC PRESSURE 

60 LIQUID COLLECTED (mls) 

0,3127 PARTICULATE WEIGHT (Front halfmg): 

0.984 PARTICULATE WEIGHT (Back half rag): 

0.84 STATIC PRESSURE (in. H20): 

43.678 PERCENTC02 

29,45 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER Cinch): 

STACK AREA (Sq.Ft.) 

NOZZLE AREA (feet): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT, OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec,): 

ACTUAL STACK GAS ELOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH) 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR,/SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO (%): 

FOR RECTANGULAR STACK 

51.25 STACKLENGTH(inchs): 

14.32568 STACKWIDTH(inchs) 

0,000533 STACK AREA(Sq,Ft.): 

14.32568 

39.8918 

3.4691 

0.0800 

80.0000 

29.1600 

28.2672 

29.5676 

39,8150 

34222,6101 

1081390,57 

0.0124 

1,77E-06 

1,9098 

0.0041 

5.93E.07 

0.6408 

99.1521 

73.7 

31.95 

10.72 

1.6 

3 

17 

0 

POINTS STACK T. DELTA P SQUAR D.P DELTA H 

deg 

496 0.17 0.412311 0.72 

2 494 0.]8 0,424264 0.77 

3 465 0.23 0.479583 0.96 

4 467 0.26 0.509902 1.10 

5 468 0.28 0.52915 1.30 

6 466 0.33 0,574456 1.50 

7 467 0,37 0.608276 1.70 

8 460 0.34 0.583095 L.55 

9 457 0.31 0,556776 1,40 

10 420 0,31 0,556776 1.50 

11 420 0.26 0.509902 1,30 

12 422 0.44 0.663325 2.10 

13 464 •.18 0.424264 0.83 

14 456 0.20 0.447214 0,93 

15 454 0,21 0.458258 0.97 

16 455 0.25 0.5 1.20 

17 458 0,27 0.519615 1.20 

18 455 0,32 0.565685 1,50 

19 458 0.35 0.591608 1.60 

20 456 0.32 0.565685 L.50 

2I 425 0.33 0.574456 [.60 

22 419 0.27 0.519615 1,30 

23 419 0,27 0.519615 1.30 

24 415 0.42 0,648074 2.10 

451,5 0.5309 1.3304 

METER T. 

NLET 

94 

98 

99 

100 

101 

102 

103 

104 

104 

105 

105 

]05 

104 

]05 

106 

107 

108 

108 

108 

108 

]09 

109 

!09 

]09 

104.5833 

METER T. 

OUTLET 

94 

95 

95 

95 

95 

95 

96 

96 

97 

98 

98 

99 

99 

IO0 

IO0 

IO0 

IO0 

IO0 

101 

101 

102 

103 

103 

!03 

98,5417 

METER T. 

AVERAGE 

101 5625 
Appendix B 
Sheet1 

Summary of CO Analyzer Calibrations and Bias 

Plant: Acme, Tulsa, OK 

Source: Tunnel Kiln 

Date: 9/6/02 

Analyzer Calibratrion Data 

Cylinder 

Value 

Zero Gas 0 

Mid Range 99.4 

High Range 199 

Analyzer Absolute % Span 

Response Difference 

2.3 2.3 0.92 

103.58 4.18 1.672 

194.55 -4.45 -1.78 

Run #1 

Run #2 

Run #3 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Drift Average 

Calibration 

Values 

Zero Gas 2.3 1.5 -0.32 5.95 1.46 1.78 3.725 

Upscale 103.58 94.25 -3.732 92.95 -4.252 -0.52 93.6 

Average CO Concentration: 

Corrected CO Concentration: 

(Equation 6C-1 

201.64 

218.8901 

Zero Gas 2.3 5.95 1.46 3.25 0.38 -1.08 4.6 

Upscale 103.58 92.95 -4.252 93.3 -4.112 0.14 93.125 

Average CO Concentration: 

Corrected CO Concentration: 

(Equation 6C-1 

197.65 

216.7655 

1.58 

91.625 

Zero Gas 2.3 3.25 

Upscale 103.58 93.3 

Average CO Concentration: 

Corrected CO Concentration: 

(Equation 6C-1) 

191.26 

208.4588 

2.415 

92.4625 

Page 
Sheet1 

Summary of NOx Analyzer Calibrations and Bias 

Plant: Acme, Tulsa, OK 

Source: Tunnel Kiln 

Date: 9/6/02 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 0.2 0.2 0.333333 

Mid Range 25.1 24.98 -0.12 -0.2 

High Range 48.5 49.15 0.65 1.083333 

Run #1 

Run #2 

Run #3 

.System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 

Upscale 

0.2 0.2 0 1.03 1.383333 

24.98 23.125 -3.09167 23.43 -2.58333 

Average NOx Concentration: 

Corrected NOx Concentration: 

(Equation 6C-1 

49.94 

54.19493 

Zero Gas 0.2 1.03 1.383333 

Upscale 24.98 23.43 -2.58333 

Drift 

Average NOx Concentration: 

Corrected NOx Concentration: 

(Equation 6C-1 

48.95 

52.98213 

Zero Gas 0.2 0.8 

Upscale 24.98 23.55 -2.38333 

1.383333 

0.508333 

Average NOx Concentration: 

Corrected NOx Concentration: 

(Equation 6C-1 

46.8 

51.33214 

Average 

Calibration 

Values 

0.615 

23.2775 

0.8 -0.38333 0.915 

23.55 -2.38333 0.2 23.49 

1.333333 0.333333 

22.78 -3.66667 -1.28333 

0.9 

23.165 

Page 
Sheet1 

Summary of Sulfur Dioxide Analyzer Calibrations and Bias 

Plant: Acme Bricl, Tulsa, OK 

Source: Tunnel Kiln 

Date: 9/6/02 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 -0.08 -0.08 -0.08 

Mid Range 52.2 50.68 -1.52 -1.52 

High Range 91 90,5 -0.5 -0.5 

Run #1 

Run #2 

Run #3 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Drift Average 

Calibratior. 

Valuas 

Zero Gas -0.08 0.1 0.18 0.13 0.21 0.03 0.115 

Upscale 90.5 86.7 -3.8 86.72 -3.78 0,02 86.71 

Average SO2 Concentration: 

Corrected SO2 Concentration: 

(Equation 6C-1 

39.65 

41.54611 

-0.425 

85.52 

Zero Gas -0,08 0.13 

Upscale 90.5 86.72 

Average SO2 Concentration: 

Corrected SO2 Concentration: 

(Equation 6C-1 

0.21 

-3.78 

49.17 

52.02298 

Zero Gas -0,08 -0.425 -0.345 -0.73 -0,65 -0.305 -0.5775 

Upscale 90.5 85.52 -4.98 86.5 -4 0,98 86,01 

49.18 

52.2931z• 

Average SO2 Concentration: 

Corrected SO2 Concentration 

(Equation 6C-1 

-0.1475 

86.12 

O 

Page _L 
9/56/02 Calibrations 

Date/Time 

mm/dd/yy hh:mm:ss 

0•/06/02 07:51:52 

09106/02 07:52:02 

09/06102 07:52:12 

09/06/02 07:52:22 

09/06/02 07:52:32 

09/06/02 07:52:42 

09106/02 07:52:52 

09/06/02 07:53:02 

09/06/02 07:53:12 

09/06/02 07:53:22 

09/06102 07:53:32 

09/06/02 07:53:42 

09106/02 07:53:52 

09/06/02 07:54:02 

09/0.6/02 07:54:12 

09106/02 07:54:22 

09/06/02 07:54:32 

09/06/02 07:54:42 

09/06/02,07:54:52 

09/06102 07:55:02 

09/06/02 07:55:12 

09/06/02 07:55:22 

09106/02 07:55:32 

09/06/02 07:55:42 

09106/02 07:55:52 

09/06102 07:56:02 

09/06/02 07:56:12 

09106/02 07:56:22 

09106/02 07:56:32 

09/06/02 07:56:42 

09106102 07:56:52 

09/06/02 07:57:02 

09/06/02 07:57:12 

09/06/02 07:57:22 

09106102 07:57:32 

09/06/02 07:57:42 

09/06/02 07:57:52 

09/06]02 07:58:02 

09/06102 07:58:12 

09/06/02 07:58:22 

09/06/02 07:58:32 

09/06/02 07:58:42 

09/06102 07:58:52 

09106102 07:59:02 

09/06/02 07:59:12 

09/06/02 07:59:22 

09]06/02 07:59:32 

09/06/02 07:59:42 

09/06/02 07:59:52 

09/06/02 08:00:02 

09/06/02 08:00:12 

09/06/02 08:00:22 

09/06/02 08:00:32 

09/06•02 08:00:42 

09/06102 08:00:52 

09/06/02 08:01:02 

09/06]02 08:01:12 

09106102 08:01:22 

09/06/02 08:01:32 

09106/02 08:01:42 

09106/02 08:01:52 

09/06L02 08:02:02 

09/06/02 08:02:12 

09/06/02 08;02:22 

09/06/02 08:02:32 

09/06/02 08:02:42 

09/06/02 08:02:52 

09/06/02 08:03:02 

09/06/02 08:03:12 

09/06/02 08:03:22 

VOC 

ppm 

CO 

ppm 

-0.1 

-0,1 

-0.1 

-0.1 

-0.1 

-0.1 

-0,1 

-0.1 

-0,1 

-0.1 

=0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

-0.1 

0.0 2.7 

0.0 2.6 

0.0 2.6 

0.0 2.5 

0.0 2.5 

0.0 2.6 

-0.1 2.4 

-0.1 2.4 

-0,1 2.4 

-0.1 2.5 

-0.1 2.4 

-0.1 2.5 

-0.1 2.3 

0,0 2.4 

-0.1 2.3 

-0.1 2.2 

-0.1 2.2 

0.0 2.2 

0.0 2.2 

0.0 2.3 

0.0 2.1 

0.0 2.1 

0.0 2.1 

0.0 2.1 

-0.1 2.2 

-0.1 2.1 

-0.1 2.2 

-0.1 2.3 

-0.1 2.3 

0.0 2.3 

-0.1 2.3 

=0,1 2.3 

-0.1 2.1 

=0.1 2,3 

-0.1 2.3 

-0.1 2,3 

-0.1 2.3 

-0.1 2.5 

-0.1 2.4 

-0.1 2.5 

-0.1 2.7 

-0.1 2.7 

SO2 

ppm 

6.1 

6.0 

6.4 

26.1 

3.2 

2.9 

2.9 

2.9 

3.1 

:3.0 

3.0 

3.0 

3,1 

3.1 

3.1 

3.0 

2.9 

2,8 

2.6 

2.6 

2.7 

2.6 

2.7 

2.7 

2•6 

2.7 

NOx 

ppm 

-0.1 0.1 

-0.1 0,1 

-0.1 0.2 

-0,1 0.2 

o.o 0.2 

o.o 0.2 

o.o 0.2 

o.o 0.2 

0.0 0.2 

0.0 0,1 

-0.1 0.1 

-0.1 0.2 

0.0 0.1 

0.0 0.2 

-0.1 0.7 

0.0 4.1 

0.0 9.0 

-0.1 14.0 

-0.1 18.9 

0,0 23.3 

0.0 26.9 

0.0 30.4 

0.0 33.1 

-0.1 35.6 

0.0 37.7 

0.0 39.3 

0.0 40.7 

-0.1 41.9 

0.0 42.9 

-0.1 43.8 

-0.1 44.4 

0.0 45,0 

0.0 45.5 

-0.1 46.0 

-0.1 46.3 

-0.1 46.5 

-0,1 46.8 

0.0 47.0 

0.0 47,2 

-0.1 47.3 

-0.1 47.4 

-0.1 47.4 

0.0 47.5 

0.0 47.5 

-0.1 47.7 

-0.1 47.8 

-0.1 47,9 

-0.'1 47.9 

-0.'1 48.0 

-0.1 48.2 

-0.1 48.3 

-0,1 48.3 

0.0 48.5 

-0.1 48.6 

-0.1 48.6 

-0.1 48.8 

0.0 48.8 

-0.1 49.0 

0.0 49.1 

0.0 49.2 

0.0 49.3 

0.0 49.0 

0.0 47.5 

0.0 45.1 

0.0 42.1 

0.0 38.3 

0.0 33.6 

0.0 28.1 

-0.1 22.5 

0.0 18,4 

Zero NOx 

48.7 ppm NOx 

Page 
9/56/02 Calibrations 

09/06/02 08:03:32 -0.1 2.7 0.0 18.3 

09/06/02 08:03:42 -0.1 2.7 0.0 19.1 

09/06/02 08:03:52 -0.1 2.7 0,0 19,9 

09/06/02 08:04:02 -0.1 2.6 0.0 20.6 

09/06/02 08:04:12 -0.1 2.6 0.0 21,3 

09/06/02 08:04 22 -0.1 2.7 -0.1 21.9 

09/06/02 08:04:32 -0.1 2.6 -0,1 22.5 

09/06/02 08:04:42 -0.1 2.6 -0.1 22.8 

09/06/02 08:04:52 -0.1 2,6 -0,1 23.2 

09/06/02 08:05:02 -0.1 2,7 0.0 23.5 

09/06/02 08:05:12 -0.1 2.8 0.0 23,9 

09/06/02 08:05:22 -0.1 2.8 0.0 24.2 

09/06/02 08:05:32 -0.1 2.9 0.0 24.3 

09/06/02 08:05:42 o0.1 2.7 0.0 24.5 

09/06/02 08:05:52 -0.1 2.6 0.0 24.6 

09/06/02 08:06:02 -0.1 2.6 0.0 24.7 

09/06/02 08:06:12 -0.1 2.5 0.0 24.9 

09106/02 08:06:22 -0.1 2.5 -0.1 24.9 

09/06/02 08:06:32 -0.1 2,3 -0.1 25.0 

09/06/02 08:06:42 -0.1 2.3 -0.1 25.0 

09/06/02 08:06:52 -0.1 2.1 0.0 25.0 

09/06/02 08:07:02 -0.1 2.1 0.0 24.5 

09/06/02.08:07:12 -0.1 2.2 -0.1 23.4 

09/06/02 08:07:22 -0.1 2.1 -0.1 21.9 

09/06/02 08:07:32 -0.1 2.3 -0.1 19.5 

09/06102 08:07:42 -0.1 2.2 0.0 16.1 

09/06/02 08:07:52 -0.1 2.5 0.0 12.5 

09/06/02 08:08:02 -0.1 2.6 -0.1 9.7 

09/06/02 08:08:12 -0.1 2.7 -0.1 7.8 

09/06/02 08:08:22 -0.1 2.8 0.0 6.1 

09/06/02 08:08:32 -0.1 3.0 1.2 4.6 

09/06/02 08:08:42 -0,1 3.0 5. 3.9 

09/06/02 08:08:52 -0.1 2.8 9.9 3.4 

09/06/02 08:09:02 -0.1 2.8 14.7 3.0 

09/06/02 08:09:12 -0.1 2.6 19.2 2.5 

09]06/02 08:09:22 -0.1 2.8 23.3 2.2 

09/06/02 08:09:32 -0.1 2.7 27.2 1.9 

09/06/02 08:09:42 -0.1 2.7 30.7 1.6 

09/06/02 08;09:52 -0.1 2.6 33.8 1.5 

09/06/02 08:10:02 -0.1 2.7 36.4 1.3 

09/06/02 08:10:12 -0.1 2.5 38.7 1.2 

09/06/02 08:10:22 -0.1 2.6 40.6 1.0 

09/06/02 08:10:32 -0,1 2.6 42.1 0,9 

09/06/02 08:10:42 -0.1 2.6 43.3 0.8 

09/06/02 08:10:52 -0.1 2.6 44.5 0.8 

09/06/02 08:11:02 -0.1 2.5 45.5 0.7 

09/06/02 08:11:12 -0.1 2.5 46.2 0.6 

09/06/02 08:11:22 -0.1 2.5 46.7 0.6 

09/06/02 08:11:32 -0.1 2.6 47.2 0.6 

09/06/02 08:11:42 -0.1 2.5 47.8 0.6 

09/06/02 08:11:52 -0.1 2.5 48,1 0.6 

09106/02 08:12:02 -0.1 2.6 48.4 0.5 

09/06/02 08:12:12 -0.1 2.5 48.6 0.5 

09/06/02 08:12:22 -0.1 2.5 48.9 0.4 

09/06/02 08:12:32 -0.1 2.5 49.1 0.5 

09/06/02 08:12:42 -0.1 2.4 49.3 0.4 

09/06/02 08:12:52 -0.1 2.3 49.3 0,4 

09/06/02 08:13:02 -0,1 2.3 49.4 0.4 

09/06/02 08:13:12 -0.1 2.3 49,6 0.4 

09/06/02 08:13:22 -0. 2,2 49,7 0.4 

09/06/02 08:13:32 -0.1 2.2 49.8 0.4 

09/06/02 08:13;42 -0.1 2,1 49.8 0.4 

09/06/02 08:13:52 -0.1 2.1 49.8 0.3 

09/06/02 08:14:02 -0.1 2.1 49.9 0.4 

09/06/02 08:14:12 -0.1 2.2 50.0 0.3 

09/06/02 08:14:22 -0.1 2.2 50.0 0.3 

09/06/02 08:14:32 -0.1 2.1 50.1 0.3 

09/06/02 08:14:42 -0.1 2.3 50.1 0.3 

09/06/02 08:14:52 -0.1 2.2 50.2 0.3 

09/06/02 08:15:02 -0.1 2.3 50.3 0.4 

09/06/02 08:15:12 -0.1 2.2 50.3 0.3 

09/06/02 08:15:22 -0.1 2,3 50.3 0.3 

09/06/02 08:15:32 -0,1 2.1 50.4 0.3 

25.1 ppm NOx 

Zero CO, $02 
9/56/02 Calibrations 

09/06/02 08:15:42 

09/06/02 08:15:52 

09/06/0:2 08:16:02 

09/06/02 06:16:12 

09/06/02 08:16:22 

09/06/02 08:16:32 

09/06/02 08:16:42 

09/06/02 08:16:52 

09/06/02 08:17:02 

09/06/02 08:17:12 

09/06/02 08:17:22 

09/06/02 08:17:32 

09106/02 08:17:42 

09/06/02 08:17:52 

09/06/02 08:18:02 

09/06/02 08:18:12 

09/06/02 08:18:22 

09/06/02 06;18:32 

09/06/02 08:18:42 

09/06/02 08:I8:52 

09/06102 08:19:02 

09/06/02 08:19:12 

09/06/02 08:19:22 

09/06/02 08:19:32 

09106/02 08:19:42 

-09106/02 08:19:52 

09/06/02 08:20:02 

09/06/02 08:20:12 

09/06/02 08:20:22 

09/06/02 08:20:32 

09/06/02 08:20:42 

09/06/02 08:20:52 

09/06/02 08:21:02 

09/06/02 08:21:12 

09/06/02 08:21:22 

09/06/02 08:21:32 

09/06/02 08:21:42 

09/06/02 08:21:52 

09/06/02 08:22:02 

09/06/02 08:22;12 

09/06/02 08:22:22 

09/06/02 08:22:32 

09/06/02 08:22:42 

09106/02 06:22:52 

09/06/02 08:23:02 

09/06/02 06:23:12 

09/06/02 08:23:22 

09/06/02 08:23:32 

09/06/02 08:23:42 

09]06/02 08:23:52 

09/06/02 08:24:02 

09/06/02 08:24:12 

09/06/02 08:24:22 

09/06/02 08:24:32 

09/06/02 08•24:42 

09/06/02 08:24:52 

09/06/02 08:25:02 

09/06/02 08:25:12 

09/06/02 08:25:22 

09/06/02 08:25:32 

09/06/02 08:25:42 

09/06/02 08:25:52 

09/06/02 08:26:02 

09/06/02 08:26:12 

09/06/02 08:26:22 

09/06/02 08:26:32 

09/06/02 08:26:42 

09/06/02 08:26:52 

09/06/02 08:27:02 

09/06/02 08:27:12 

09/06/02 08:27:22 

09/06/02 08:27:32 

-0.1 2.1 50.4 

-0.1 2.2 50.4 

-0.t 2.3 50.6 

-0.1 2.2 50.6 

-0.1 2.2 50,7 

-0.1 2.4 50.6 

-0.1 2.4 49.7 

-0.1 2.7 48.1 

-0,1 2.8 45.2 

-0.1 2.9 41.1 

o0.1 3.1 35.6 

-0.1 3.2 29.9 

-0.1 3.2 28.9 

-0.1 3.2 33.9 

-0.1 3,1 41.1 

-0.1 2.9 48.1 

-0.1 2.7 54.4 

-0.1 2.6 59.9 

-0.1 2.4 64.8 

-0.1 2.3 69.1 

-0.1 2.3 72.8 

-0.1 2.3 75.5 

-0.1 2.2 77,9 

-0.1 2.2 80.1 

-0.1 2.4 81.8 

-0.1 2.4 83.4 

-0.1 2.4 84.5 

-0.1 2.4 85.3 

-0.I 2.5 86.2 

-0.1 2.4 87.0 

-0.1 2.4 87.6 

-0.1 2.4 87.9 

-0.1 2.5 88.2 

-0.1 2.3 88.6 

-0,1 2.6 88.8 

-0.1 2.5 89.0 

-0.1 2.4 89.3 

-0.1 2.6 89.5 

-0.1 2.5 89.6 

-0.1 2.5 89.8 

-0,1 2.6 90.0 

-0.1 2.7 90.0 

-0.1 2.7 90.2 

-0,1 2.7 90.3 

-0.1 2.7 90.4 

-0.1 2.7 90.5 

-0.1 2.7 90.5 

-0.1 2.7 90.5 

-0.1 2,8 90.5 

-0.1 2.7 90.4 

-0,1 2.9 89.5 

0.6 2.9 87.0 

0.5 3,1 82.5 

0.1 3.2 75.0 

0.3 3.3 64.3 

0.1 3.6 51.8 

0,2 10,1 39.9 

0.1 29.8 29.5 

0.1 53,6 22.5 

0,2 74.6 18.1 

0.2 91,9 15,2 

0.3 106.5 13.2 

0.3 119.1 11.4 

0.3 128.8 10.0 

0.3 138.0 8.7 

0.3 144.7 7.6 

O.4 151.8 6.8 

0.3 157.7 6.1 

0.4 162,3 5,5 

0.4 166.7 4,9 

0.4 170.2 4,4 

0.4 173.0 4,0 

0.3 

0.3 

0.3 

0.3 

0.3 

0.3 

0.4 

0.4 

0.4 

0.4 

0.4 

0.4 

0.3 

0.3 

0.2 

0.2 

0.2 

0.2 

0,2 

0.2 

0.1 

0.1 

0.1 

0.'1 

0.'1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.2 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0,1 

0.1 

0.0 

52.2 ppm S02 

91 ppm S02 

Page3 

.• 1,1,1• 
9/56/02 Calibrations 

09/06/02 08:27:42 0.4 175.2 

09/06/02 08:27:52 0.4 176.5 

09/06/02 08:28:02 0.3 177.7 

09/06/02 08:28:12 0.4 179.t 

09/06/02 08:28:22 0.4 160.2 

09106/02 08:28:32 0.4 181 .I 

09/06/02 08:28:42 0.4 181.6 

09/06/02 06:28:52 0.5 182.3 

09106/02 08:29:02 0.5 182.8 

09/06/02 08:29:12 0.5 185,0 

09/06/02 06:29:22 0.5 187.6 

09/06/02 08:29:32 0.5 18•).1 

09/06/02 08:29:42 0.5 189.3 

09/06/02 08:29:52 0.5 194.8 

09/06/02 08:30:02 0.5 190.0 

09106/02 08:30:12 0.5 190.4 

09/06/02 08:30:22 0.5 192.7 

09/06/02 08:30:32 0.5 192.4 

09/06/02 06:30:42 0.5 192.8 

09/06/02 08:30:52 0.6 197,3 

09/06/02 06:31:02 0.6 193.0 

09/06/02 08:31:12 0.5 192.9 

09/06/02 08:31:22 0.5 194.1 

09106/02 08:31:32 0.5 193.5 

09106/02 08:31:42 0.5 193,5 

09/06/02 08:31:52 0.5 193.5 

09106/02 08:32:02 0.5 193.7 

09/06/02 08:32:12 0.6 201.3 

09/06/02 08:32:22 0.6 193.8 

09/06/02 08:32:32 0.5 194.0 

09/06/02 06:32:42 0.6 194.0 

09/06/02 08:32:52 0,6 194.1 

09/06/02 06:33:02 0.7 194.3 

09/06/02 08:33:12 0.5 194.4 

09/06/02 08:33:22 0.5 194.5 

09/06/02 06:33:32 -0.1 194.7 

09/06/02 08:33:42 0.4 194.6 

09/06/02 08:33:52 0.6 194.2 

09/06/02 08;34:02 0.6 191.9 

09/06/02 08:34:12 0.6 185,4 

09/06/02 08:34:22 0.6 173.4 

09/06/02 08:34:32 0.6 151.8 

09/06/02 08:34:42 0.6 123.0 

09/06/02 08:34:52 0.7 100.0 

09/06/02 08:35:02 0.6 92.1 

09/06/02 08:35:12 0.7 91.5 

09/06/02 08:35:22 0,7 92.8 

09/06/02 08:35:32 0.7 94,0 

09/06/02 08:35:42 0.7 95.5 

09/06/02 08:35:52 0.7 96.8 

09/06/02 08:36:02 0.7 97.9 

09/06/02 08:36:12 0.7 99.0 

09/06/02 06:36:22 0,7 99.3 

09/06/02 08:36:32 0.7 100.6 

09/06/02 08:36:42 0.7 100.9 

09/06/02 08:36:52 0.7 101.5 

09/06/02 08:37:02 0.7 102.0 

09/06/02 08:37:12 0.8 102.4 

09/06102 08:37:22 0.8 102.6 

09/06/02 08:37:32 0.8 102.9 

09/06/02 08:37:42 0.8 103.2 

09/06/02 08:37:52 0.8 103.1 

09/06/02 08:38:02 0.8 103.3 

09/06/02 06:38:12 0,8 103.4 

09/06/02 06:38:22 0.8 103.4 

09/06/02 08:38:32 0.8 03.,• 

09/06/02 08:38:42 0.8 103,6 

09/06/02 08:38:52 0.8 103.5 

09/06/02 08:39:02 0.8 1 03.5 

09/06/02 08:39:12 0.8 103.4 

09/06/02 08:39:22 0.8 103.3 

09/06/02 08:39:32 0.8 103.4 

3.7 0.0 

3.5 0.0 

3.2 0.0 

3.0 0.0 

2.9 0.1 

2.8 0.0 

2.6 0.1 

2.5 0.0 

2.5 0.0 

2.4 0.'1 

2.2 0.0 

2.2 0.1 

2.1 0.1 

2.1 0.1 

2.0 0.1 

2.0 0.1 

2.0 0.0 

2,0 0.0 

1.9 0.1 

1.8 0.0 

1.8 0.1 

1.8 0.0 

1,8 0.1 

1.7 0.1 

1.7 0.1 

1.7 0.1 

1.7 0.1 

1.8 0.0 

1.8 0.1 

1.7 0.'1 

1.6 0.1 

1.6 0.1 

1.5 0,1 

1.5 0.0 

1,5 0.0 

1.5 0.1 

1.6 0.1 

1.5 0.1 

1.6 0.1 

1,6 0.1 

1.9 0.1 

2.3 0.1 

2.5 0.1 

2.5 0.1 

2,2 0.1 

2.0 0.1 

1.8 0,0 

1.6 0.0 

1.3 0.1 

1.1 0.0 

1.1 0.1 

1.0 0.0 

0.9 0.1 

0.8 0.1 

0.7 0.0 

0.7 0.0 

0.6 0.1 

0.5 0.1 

0.5 0.1 

0.4 0.1 

0.5 0.1 

0.5 0.0 

0.5 0.1 

0,4 0.1 

0.4 0.1 

0.4 0.1 

0.4 0.0 

0.3 0.0 

0.4 0.1 

0.5 0.1 

0.4 0.1 

0.4 0.1 

199 ppm CO 

99.4 ppm CO 

Page4 ,,•L t• 
9/56/02 Calibrations 

09/06/02 08:39:42 0.8 103.5 0.4 0.1 

09/06/02 08:39:52 0.8 103.2 0.3 0.0 

09/06/02 08:40:02 0.8 103.2 0.3 0.1 

09/06/02 08:40:12 0.0 103.1 0.4 0.1 

09/06/02 08:40:22 -0.1 103.0 0.4 0.1 

09/06/02 08:40:32 -0.1 102.7 0.3 0.0 

09/06/02 08:40:42 -0.1 101.7 0.3 0.0 

09/06/02 08:40:52 0.6 99.3 0.3 0.0 

09/06/02 08:41:02 0.7 94.9 0,4 0.0 

09/06/02 08141:12 0.7 88.1 0.6 0.1 

09/06/02 08:41:22 0.8 81.1 0.6 0.1 

09/06/02 08:41:32 0.8 77.2 0.7 0.1 

09/06102 08:41:42 0,8 75.8 0.7 0.1 

09/06/02 08:41:52 0,8 74.3 0.7 0.1 

09/06/02 08:42:02 0.8 71.7 0.7 0,0 

09/06/02 08:42:12 0.8 67.6 0.8 0.1 

09/06/02 08:42:22 0.9 60.0 0.8 0.1 

09/06/02 08:42:32 0.8 51.3 0.7 0.1 

09/06/02 08:42:42 0.8 42.3 0,7 0.1 

09/06/02 08:42:52 0.8 35.4 0.7 0.1 

09/06/02 08:43:02 0.8 30.6 0.6 0.1 

09/06/02 08:43:12 0.7 26.5 0.6 0.1 

09106/02 08:43:22 -0.1 22.9 0,6 0.1 

09/06/02 08:43:32 -0.1 20.2 0.5 0.1 

09/06/02 08:43:42 -0.1 18.0 0.5 0.1 

09/06/02 08:43:52 -0.1 16.1 0.5 1.6 

09/06/02 08:44:02 -0.1 13.7 0.4 4.2 

09/06/02 08:44:12 -0.1 11.9 0.3 6.8 

09/06/02 08:44:22 -0.1 10.5 0.3 9.2 

09/06/02 08:44:32 -0.1 9.2 0.2 11.3 

09/06/02 08:44:42 o0.1 8.4 0.2 13.2 

09/06/02 08:44:52 -0.1 7.5 0.2 14.8 

09/06/02 08;45:02 -0.1 6.7 0.1 16.3 

09/06/02 08:45:12 -0.1 6.0 0.1 17.5 

09/06/02 08:45:22 -0.1 5.7 0.1 18.5 

09/06/02 08:45:32 -0.1 5.1 O. 19.3 

09/06/02 08:45:42 -0.1 4.8 0.1 20,0 

09/06/02 08:45:52 -0.1 4.3 0,1 20.7 

09/06/02 08:46:02 -0.1 4,1 0.1 21.1 

09/06/02 08:46:12 -0.1 3.6 0.1 21.5 

09/06/02"08:46:22 -0.1 4.0 0.t 21.9 

09/06/02 08:46:32 -0.1 3,8 0.1 22,2 

09106102 08:46:42 -0.1 3.5 0.1 22,4 

09/06/02 08:46:52 -0,1 3.5 0.1 22.6 

09/06102 08:47:02 -0.1 3.4 0.1 22:6 

09/06/02 08:47:12 -0.1 3.3 0.1 22.7 

09/06/02 08:47:22 -0.1 3.2 0.1 22.9 

09/06/02 08:47:32 -0.1 3.1 0.1 22.9 

09/06/02 08:47:42 -0.1 3.2 0.1 23.0 

09/06/02 08:47:52 -0.1 3.1 0.1 23.0 

09/06/02 08:48:02 -0.1 3.1 0.1 23.0 

09/06/02 08:48:12 -0,1 3,0 0,1 23.1 

09/06/02 08:48:22 -0.1 2.9 0.1 23.2 

09/06/02 08:48:32 -0.1 3.1 0.1 23.2 

09106/02.08:48:42 0.0 3.0 0.1 23.0 

09/06/02 08:48:52 O. 2.9 O. 23.0 

09/06/02 08:49:02 -0.1 3.1 0,0 23.1 

09/06/02 08:49:12 -0.1 2,6 0.0 23.1 

09/06/02 08:49:22 -0,1 2.7 0.1 23.1 

09/06/02 08:49:32 -0.1 3.0 0.0 22.7 

09/06/02 08:49:42 -0.1 4.8 0,0 21.0 

09/06/02 08:49:52 -0.1 11.8 0.1 17.6 

09/06/02 08:50:02 -0.1 23.6 0.0 13.5 

09/06/02 08:50:12 -0.1 37.0 0.0 10.6 

09/05/02 08:50:22 -0.1 48.1 0.1 8.6 

09/06/02 08:50:32 -0.1 56.2 0.0 6.7 

09/06/02 08:50:42 -0,1 63.2 0,0 5.5 

09/06/02 08:50:52 -0.1 68.5 0.1 4.4 

09/06/02 08:51:02 -0.1 72.2 0.1 3.6 

09/06/02 08:51:12 -0.1 75,8 0,1 3.0 

09/06/02 08:51:22 -0.1 78.7 0.0 2.4 

09/06/02 08:61:32 -0.1 81.2 0.0 1.9 

09/06/02 08:51:42 -0.1 82.9 0.0 1.6 

25.1 ppm NOx Bias 

Zero VOC, CO, SO2 Bias 

Page 5 
9/56/02 Calibrations 

09/06/02 08:51:52 

09/06/02 08:52:02 

09/06/02 08:52:12 

09106/02 08:52:22 

09/06/02 08:52:32 

09/06102 08:52:42 

09/06/02 08:52:52 

09/06/02 08:53:02 

06/06/02 08:53:12 

09/06/02 08:53:22 

09/06/02 08:53:32 

09/06/02 08:53:42 

09/06/02 08:53:52 

09/06/02 08:54:02 

09/06/02 08:54:12 

09/06/02 08:54:22 

09/06/02 08:54:32 

09/06/02 08:54:42 

09/06/02 08:54:52 

06/06/02 08:55:02 

09/06/02 08:55:12 

09/06/02 08:55:22 

09/06102 08:55:32 

09/06/02 08:55:42 

09/06/02 08:55:52 

09/06/02 08:56:02 

09/06/02 08:56:12 

09/06/02 08:56:22 

09/06/02 08:56:32 

09/06/02 08:56:42 

09/06/02 08:56:52 

09/06/02 08:57:02 

09/06/02 08:57:12 

09/06/02 08:57:22 

09/06/02 08:57:32 

09/06/02 08:57:42 

09/06/02 08:57:62 

09/06/02 08:58:02 

09/06/02 08:58:12 

09/06102 08:58:22 

09/06102 08:58:32 

09/06/02 08:58:42 

09/06/02 08:58:52 

09/06/02 08:59:02 

09/06102 08:59:12 

09/06/02 08:59:22 

09/06/02 08:59:32 

09/06/02 08:59:42 

09/06102 08:59:52 

09/06/02 09:00:02 

09/06/02 09:00:12 

09/06/02 09:00:22 

09/06/02 09:00:32 

09/06/02 09:00:42 

09/06/02 09:00:52 

09/06/02 09:01:02 

09/06/02 09:01:12 

09/06/02 09:01:22 

09/06102 09:01:32 

09/06/02 09:01:42' 

09/06/02 09:01:52 

09/06/02 09:02:02 

09/06/02 09:02:12 

09/06/02 09:02:22 

09/06/02 09:02:32 

09/06/02 09:02:42 

09/06/02 09:02:52 

09/06/02 09:03:02 

09/06/02 09:03:12 

09/06/02 09:03:22 

09/06/02 09:03:32 

09/06/02 09:03:42 

-0.1 84.1 0.0 1.4 

-0.1 85.1 0.1 1.2 

-0.1 85.8 0.1 1.0 

-0.1 86.2 0.0 1.0 

-0.1 86.6 0.0 0.9 

-0.1 88.0 0.0 0.9 

-t3.1 89.1 0.0 0.8 

-0.1 90.4 0,0 0.7 

-0.I 91.4 0.0 0.7 

-0.1 92.6 0.0 0.7 

-0.1 93.6 0.0 0.7 

-0.1 93.6 -0.1 0,6 

0.0 93.7 -0.1 0.6 

-0.1 94.0 -0.1 0.6 

-0.1 95.0 -0.1 0.6 

-0.1 94.1 -0.1 0.6 

-0.t 93.9 0.0 0.6 

-0.1 94.5 1.0 0.7 

-0.1 84.2 5.7 0.7 

-0.1 62.3 14.3 0.7 

-0.1 51.4 23.8 0.6 

-0.1 42.0 33.1 0.6 

-0.1 34.5 41.0 0.6 

-0.1 28.3 47,8 0.5 

-0.1 22.8 54.0 0.5 

-0.1 18.8 59.0 0.4 

-0.1 16,5 62.9 0.4 

-0,1 14.1 66.2 0.4 

-0.1 12.0 68.8 0.4 

-0.1 10.8 70.9 0.4 

-0.1 9.7 72.7 0.4 

-0.1 8.7 74.1 0.3 

-0.1 8.1 75.2 0.3 

-0.1 7.8 76.2 0.3 

-0.1 7.3 77.1 0.3 

-0,1 7.1 77.5 0.3 

-0.1 6.8 78.1 0.3 

-0.1 6.7 78.5 0.3 

-0.1 6.4 78.9 0.3 

-0.1 6.3 79.4 0.3 

-0.1 6.3 79,6 0.3 

-0.1 6.3 79.8 0.3 

-0.1 6.2 80,0 0.3 

-0.1 6.2 80.2 0.2 

-0.1 6.2 80.5 0.3 

-0.1 6.0 80.8 0.2 

-0.1 6.1 81.1 0.2 

-0.1 6.0 81.2 0.2 

-0,1 5.9 81.2 0.2 

-0.1 6.0 61.4 0.2 

-0.1 5.9 81.7 0.2 

-0.1 5.9 82.2 0.2 

•0.1 5.6 82.8 0.2 

-0.1 5.5 83,4 0.2 

-0.1 5.1 84.1 0.2 

-0.1 4.8 84.6 0.2 

-0,1 4.8 85.0 0.2 

-0.1 4.8 85,5 0.2 

-0.1 4.8 86.0 0.2 

-0.1 4.9 86.3 0.2 

-0.1 4.9 86.5 0,2 

-0,1 4.9 86.8 0.2 

-0.1 4.9 86.9 0,2 

-0.1 5.0 87.0 0.2 

9.4 5,1 86.7 0.2 

20.O 4.9 86.6 0.2 

20.3 5.0 86,8 0.2 

23.1 4.9 86.7 0,2 

35,5 4.9 86.8 0.2 

36.9 4.9 86.5 0,2 

36.3 5.0 85.3 0.2 

36.2 5.2 82.6 0.2 

99.4 ppm CO Bias 

91 ppm S02 Bias 

Zero NOx Bias 

Page 6 
9/56/02 Calibrations 

09/06/02 09:03:52 

09106102 09:04:02 

09106/02 09:04:12 

09/06/02 09:04:22 

09/06/02 09:04:32 

09/06/02 09:04:42 

09/06/02 09:04:52 

09/06/02 09:05:02 

09/06/02 09:05:12 

09/06/02 09:05:22 

09/06/02 09:05:32 

09/06/02 09;05:42 

09/06/02 09:05:52 

09/06/02 09:06:02 

09/06/02 09:06:12 

09/06/02 09:06:22 

09/06/02 09:06:32 

09/06/02 09:06:42 

09/06/02 09:06:52 

09/06/02 09:07:02 

09/06/02 09:07:12 

09/06/02 09:07:22 

09/06/02 09:07:32 

09/06/02 09:07:42 

09/06/02 09:07:52 

09/06/02 09:08:02 

09/06/02 09:08:12 

09/06/02 09:08:22 

09/06/02 09:08:32 

09/06/02 09:08:42 

09/06/02 09:08:52 

36.3 

35.7 

29.5 

29.6 

29.6 

29.6 

29.6 

20.5 

2.1 

1.9 

1.8 

33.8 

51.7 

52.4 

52.6 

52.5 

52.5 

26,1 

2.3 

2,0 

1.9 

11.9 

14.0 

14.1 

14.2 

14.2 

14,2 

14.2 

14,2 

7.0 

1.9 

5.5 

5.8 

5.9 

5.9 

5.6 

5.4 

5.1 

4.9 

4.8 

4.7 

4.6 

4.5 

4.3 

4.5 

4.3 

4.2 

4.2 

4.0 

3.8 

3.6 

3.4 

3.2 

3.2 

3.2 

3.2 

3,5 

3,6 

3.6 

3.6 

3.6 

3.5 

77.4 

69.5 

59.5 

48.9 

40.0 

33,2 

28.0 

23.9 

20.5 

17.7 

15.5 

13.6 

11.8 

10.6 

9.7 

8.9 

8.2 

7.4 

6.8 

6.4 

5.5 

5.1 

4.8 

4.4 

4.1 

3.8 

3.6 

3.4 

3.2 

2,9 

2,7 

0.3 

0.3 

0.3 

0.2 

0.3 

0.2 

0.2 

0.2 

0.2 

0.1 

0.1 

0,1 

0.2 

0.2 

0.2 

0.2 

0.2 

0,1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.4 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

29.6 ppm C3H8 

50.3 ppm C3H8 

14.7 ppm C3H8 

Page7 
916101 Run #I 

Date/Time VOC CO $02 NOx 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

09/06/02 09:16:42 17.5 185.2 0.0 49.3 

09/06/02 09:16:52 t7.3 186.9 0.0 49.8 

(•9106/02 09:17:02 17.3 189.2 -0.1 50.0 

09/06/02 09:17:12 17.1 190.7 -0.1 50.3 

09/06/02 09:17:22 17.1 192.3 -0.1 50.5 

09/06/02 09:17:32 17.1 193.2 -0.1 50.6 

09106/02 09:17:42 17.0 193,9 0.0 50,6 

09/06/02 09:17:52 17.0 194.7 0.0 50.7 

09/06/02 09:18:02 16.8 195.9 0.0 50.6 

09/06/02 09:18:12 16.8 197.0 0.0 50.6 

09/06/02 09:18:22 16.6 197.9 .0,1 50.6 

09/06102 09:18:32 16.8 199.0 -0.1 50.6 

09/06/02 09:18:42 16.7 199.7 -0.1 50.6 

09/06/02 09:18:52 16.6 200.5 -0.1 50.6 

09/06/02 09:19:02 16.6 201.1 0.0 50.5 

09/06/02 09:19:12 16.6 201,6 0.0 50.6 

09/06/02 09:19:22 16.6 202.1 0.0 50.6 

09/06/02 09:19:32 15.8 202.4 0.0 50.6 

09/06/02 09:19:42 16.1 202.8 0.1 50.6 

09/06/02 09:19:52 16.6 203,2 0.1 50.7 

Start Run #1 

09/06f02 09:20:02 16.8 203.7 0.1 50.7 

09/06/02 09:20:12 16.7 203.6 0.3 50.5 

09/06/02 09:20:22 16.9 202.9 0.4 50.0 

09/06/02 09:20:32 16.8 201.6 0.6 49.2 

09106/02 09:20:42 16.8 199.8 0.7 48.6 

09/06/02 09:20:52 16.9 198.1 0.8 47.9 

09/06/02 09:21:02 16.9 196 6 1.0 47.4 

09/06/02 09:2:1:12 16.9 195.3 1.1 46.9 

09/06/02 09:21:22 17.0 194.3 1.2 46.5 

09/06102 09:21:32 17.1 193.5 1.3 46.3 

09/06/02 09:21:42 17.1 193.1 1.5 46.0 

09/06/02 09:21:52 17.2 192.9 1.6 45.9 

09/06/02 09:22:02 17.3 192.8 1.7 45.7 

09/06/02 09:22:12 17.4 192.4 1.9 45.6 

09106/02 09:22:22 17.2 192.1 2.1 45.6 

09106/02 09:22:32 17.3 191.9 2.2 45.5 

09/06/02 09:22:42 17.8 191.7 2.5 45.3 

09/06/02 09:22:52 17.5 191.5 2.9 45.4 

09/06/02 09:23:02 16.8 191.3 3.0 45.4 

09/06102 09:23:12 16.7 191.0 3.2 45.3 

09/06/02 09:23:22 16,7 191.3 3.4 45.4 

09/06/02 09:23:32 16.8 192.3 3.6 45.7 

09/06/02 09:23:42 16.9 193.3 3.7 46.3 

09/06/02 09:23:52 16.8 194.6 4.0 47.0 

09/06/02 09:24:02 16.8 196.1 4.5 47.5 

09/06/02 09:24;12 16.8 197.6 5.'1 47.9 

09/06/02 09:24:22 16.6 198.9 5.6 48.3 

09/06/02 09:24:32 16.5 200.2 6.2 48.6 

09/06/02 09:24:42 16.5 201.2 6.9 48.9 

09/06/02 09:24:52 16.5. 202.1 7.4 49.1 

09/06/02 09:25:02 16.5 202.9 8.1 49.2 

09/06/02 09:25:12 16.3 203.4 8.8 49.4 

09/06/02 09:25:22 16.2 203.7 9.5 49.6 

09/06/02 09:25:32 16.3 204.0 10.2 49.8 

09/06/02 09:25:42 16.2 204.3 10.7 49.8 

09/06/02 09:25:52 16.5 204.6 11.2 49.8 

09/06/02 09:26:02 16.4 204.9 11.7 49.9 

09/06/02 09:26:12 16.4 204.9 12.2 50.0 

09/06/02 09:26:22 16.5 205.0 12.8 50.0 

09/06/02 09:26:32 16.4 205.1 13.4 50.2 

09/06/02 09:26:42 16.3 205.2 13.9 50.2 

09/06/02 09:26:52 16.3 205:5 14.5 50.2 

09/06/02 09:27:02 16.4 205.6 15.1 50.3 

09/06/02 09:27:12 16.4 205.7 15.6 50.3 

09/06/02 09:27:22 16.5 205.7 16.2 50.4 

09/06/02 09:27:32 16.3 205.8 16.9 50.4 

09/06/02 09:27:42 16.4 205.9 17.5 60..4 

09/06/02 09:27:52 16.3 206.2 18.0 50.5 

09/06/02 09:28:02 15.6 206.1 18.6 50.5 

09/05/02 09:28:12 15.8 206 0 19.2 50.5 

Page 

9/6/01 Run #1 

09106/02 09:28:22 16,1 206.2 19.5 50.6 09106102 09:28:32 16.0 206.1 19.8 50.5 09106/02 09:28:42 16.1 205.9 20.2 50.4 09/06/02 09:28:52 16.2 206,0 20.7 50.5 09/06102 09:29:02 15.8 205.9 21.0 50.5 09/06/02 09:29:12 14.8 205.9 21.3 50.5 09/06/02 09:29:22 15.3 206.1 21.9 50.6 09/06/02 09:29:32 15.5 206.1 22,5 50.6 09/06/02 09:29:42 15.4 205.9 22.9 50,6 09/06/02 09:29:52 15.5 206.0 23.5 50.6 09106102 09:30:02 15.8 206.1 24." 50.6 09/06/02 09:30:12 15.7 206.1 24.5 50.6 09/06/02 09:30:22 15.5 206.1 24.9 50.6 09/06/02 09:30:32 15.5 206.2 25.4 50.6 09/06/02 09:30:42 15.4 206.0 25.9 50.7 09/06/02 09:30:52 15.9 205.9 26.3 50.7 09/06/02 09:31:02 15.5 205.9 26.7 50.6 09/06/02 09:31:12 15.6 205.9 27.3 50.6 09/06/02 09:31:22 15.6 205.8 27.7 50.6 09/06/02 09:31:32 15.4 205.7 28.'1 50.7 09/06/02 09:31:42 15.4 205.8 28,=t 50.6 09/06/02 09:31:52 15.3 205.6 28.7 50.7 09/06/02 09:32:02 15.5 205.7 29.0 50.8 09/06/02 09:32:12 15,3 205,5 29.4 50.8 

09/06/02 09:32:22 15.2 205.4 29.7 50.7 09/06/02 09:32:32 15,4 205.3 30.1 50.6 09/06/02 09:32:42 15.3 205.2 30.5 50,7 09/06/02 09:32:52 15.3 205.1 31.0 50.6 09/06/02 09:33:02 15.1 204.8 31.4 50.7 

09]06/02 09:33:12 15.5 204.8 31.7 50.6 09106/02 09:33:22 15.3 204.5 31.9 50.6 09/06/02 09:33:32 15.4 204,4 32,3 50.6 09/06/02 09:33:42 15.5 204,3 32.6 50,7 09/06/0209:33:52 15.5 204,2 33.0 50.8 

09/06/02 09:34:02 15.3 204.3 33.3 50.7 09/06102 09:34:12 15.1 204.4 33.7 50.7 

09/06/02 09:34:22 15.6 204.5 34.0 50.7 

09/06/02 09:34:32 15.5 204.6 34.3 50.7 

09/06/02 09:34:42 15.2 204.5 34.6 50.7 09/06/02 09:34:52 15.5 204.6 34.8 50.7 09/06/0209:35:02 15.2 204.5 35.1 50.7 

09/06/02 09:35:12 15.2 204.5 35.3 50.6 

09/06/02 09:35:22 15.1 204.7 35.5 50.7 

09/06/02 09:35:32 15,5 204,5 35.7 50.8 

09/06/02 09:35:42 15.3 204.4 35.8 50.7 

09/06/02 09:35:52 15,4 204.2 35.9 50.8 

09/06/02 09:36:02 15.3 204.4 36.1 50,8 

09/06/02 09:36:12 15.3 204.1 36.4 50.7 

09/06/02 09:36:22 15.2 204.0 36.7 50.8 

09/06/02 09:36:32 15.3 203.7 36.8 50.7 

09/06/02 09:36:42 15.4 203.4 37.2 50.7 

09/06/02 09:36:52 15,5 203.3 37.6 50.7 

09/06102 09:37:02 15.5 203.1 37.9 50.7 

09/06/02 09:37:12 15.5 202.7 38.2 50.6 

09/06/02 09:37:22 15.4 202.6 38.4 50.6 

09/06/02 09:37:32 15.3 202.6 38.6 50.6 

09/06/02 09:37:42 15.3 202.6 38.7 50.5 

09/06/02 09:37:52 15.2 202.5 38.9 50.6 

09/06/02 09;38:02 15.0 202.4 39.1 50.6 

09/06/02 09;38:12 14.9 202.5 39.4 50.6 

09/06/02 09:38:22 14.5 202.4 39,5 50.6 

09/06/02 09:38:32 14.7 202.3 39.7 50.6 

09/06/02 09:38:42 14.8 202.0 39.7 50.6 

09/06/02 09:38:52 15,0 201,6 39.9 50.5 

09/06/02 09:39:02 15.1 201.7 40.0 50.6 

09/06/02 09:39:12 15.2 201.5 40.1 50.6 

09/06/02 09:39:22 15.0 201.8 40.3 50.6 09/06/02 09:39:32 15.0 201.7 40.4 50.6 

09/06/02 09:39:42 15.3 201.6 40.5 50.5 

09/06/02 09:39:52 15.0 201.6 40.6 50.6 

09/06/02 09:40:02 15.0 201,4 40.8 50,5 

09/06/02 09:40:12 15.2 201.1 40.9 50.5 

09/06/02 09:40:22 15.0 200.9 41.0 50.4 

09/06102 09:40:32 14.7 200.9 41.2 50.5 

Page 2 
9/6/01 Run #1 

09/06/02 09:40:42 

09/06/02 09:40:52 

09/06/02 09:41:02 

09/06/02 09:41:12 

09/06/02 09:41:22 

09/06/02 09:41:32 

09/06/02 09:41:42 

09106/02 09:41:52 

09/06/02 09:42:02 

09/06/02 09:42:12 

09/06/02 09:42:22 

09/06/02 09:42:32 

09/06/02 09:42:42 

09/06/02 09:42:52 

09/06/02 09:43:02 

09/06/02 09:43:12 

09/06/02 09:43:22 

09/06/02 09:43:32 

09/06/02 09:43:42 

09/06/02 09:43:52 

09/06/02 09;44:02 

09/06/02 09:44:12 

09/06/02 09:44:22 

09/06/02 09:44:32 

09/06/02 09:44:42 

09/06/02 09:44:52 

09/06/02 09:45:02 

09/06/02 09:45:12 

09/06/02 09:45;22 

09/06/02 09:45:32 

09/06/02 09:45:42 

09/06/02 09:45:52 

09/06/02 09:46:02 

09/06/02 09:46:12 

09/06/02 09:46:22 

09106/02 09:46:32 

09/06/02 09:46:42 

09/06/02 09:46:52 

09/06/02 09:47:02 

09/06]02 09:47:12 

09/06/02 09:47:22 

09/06/02 09:47:32 

09/06/02 09:47:42 

09/06/02 09:47:52 

09/06/02 09:48:02 

09/06/02 09:48:12 

09/06/02 09:48:22 

09/06/02 09:48:32 

09/06/02 09:48:42 

09/06/02 09:48:52 

09/06/02 09;49:02 

09/06/02 09:49:12 

09/06/02 09:49:22 

09/06/02 09:49:32 

09/06/02 09:49:42 

09/06/02 09:49:52 

09/06/02 09:50:02 

09/06/02 09:50:12 

09/06/02 09:50:22 

09/06/02 09:50:32 

09/06/02 09:50:42 

09/06/02 09:50:52 

09/06/02 09:51:02 

09/06/02 09:51:12 

09/06/02 09:51:22 

09/06/02 09:51:32 

09/06/02 09:51:42 

09/06/02 09:51:52 

09/06/02 09:52:02 

09/06/02 09:52:12 

09/06/02 09:52:22 

09/06/02 09:52:32 

09/06/02 09:52:42 

09/06/02 09:52:52 

14.7 200.8 41.5 50.6 

14.7 201.1 41.8 50.5 

14.9 201.0 41.9 50.5 

14.8 201.0 42.0 50.5 

15.1 200.9 42.2 50.5 

14.8 200.6 42.2 50.5 

14.8 200.3 42.3 50.4 

14.8 200.8 42.3 50.4 

14.9 200,1 42.5 50.4 

14.8 200.1 42.7 50.4 

14.7 199.8 42.7 50.4 

14.5 199.7 42.8 50.4 

14,9 199.3 42,7 50.4 

14.4 199.2 42.8 50.4 

14.3 199.1 43.0 50.3 

14.7 199.0 43.1 50.3 

14.7 199.0 43.2 50.4 

14.8 199.0 43.3 50.3 

14.6 198.9 43.5 50.3 

14.6 198.6 43.7 50.3 

14.6 198.6 43.8 50.4 

14.6 198.4 43.9 50.3 

14.6 198,4 44.0 50.3 

14.4 198,3 44.3 50.4 

14.5 198.2 44.5 50.4 

14.4 198,0 44.6 50.4 

14.2 198.0 44.8 50.4 

14,4 197.9 45.0 50.4 

14.3 197.9 45.0 50.4 

14.4 197.9 45.2 50.4 

14.2 198.0 45,4 50.4 

14.0 198.1 45.5 50.4 

13.9 198.2 45.6 50.4 

14.2 198.0 45.6 50.3 

14.3 197.9 45.7 50.3 

14,2 197.6 45.7 50.3 

14.3 197.6 45.8 50.3 

14.2 197.5 45,8 50.3 

14.2 197.4 45.8 50.2 

14.3 197.2 45.9 50.2 

14.3 197.1 46.1 50.2 

14.1 197.0 46.2 50.2 

14,2 196.8 46.1 50.2 

14.1 196.8 46.1 50.2 

14.1 196.5 46.3 50.2 

14.0 196.5 46.5 50.2 

14.2 196.4 46.5 50.2 

14.2 195.9 46.5 50.1 

14.3 195.8 46.5 50.2 

13.9 195.6 46.5 50.2 

14.1 195.5 46.5 50.1 

14,0 195.3 46.6 50.1 

13.9 195.2 46.6 50.1 

14.0 195.2 46.6 50.1 

13.9 195.1 46.7 50.1 

14.0 195.0 46.7 50.0 

14.2 194.8 46.8 50.0 

14.0 194.9 46.9 50.0 

13.9 194.8 46.8 50.1 

13.8 194.7 46.9 50.1 

13.7 194.9 47.0 50.0 

13.9 194.7 47,0 50.0 

13.9 194.6 47.0 50.0 

13.9 194.5 47.1 50.0 

13,9 194.4 47.0 50.0 

13.7 194.5 47.1 49.9 

13.8 194.3 47.2 49.9 

13.9 194.3 47.2 49.8 

13.8 194,0 47.2 49.9 

13.6 194.0 47.3 49.8 

13.6 193,9 47.2 49,9 

13.7 193.7 47.2 49.8 

11.6 193.6 47.3 49.8 

8.7 193.4 47.4 49.7 

Page 3 

23 
9/6/0'] Run #1 

09/06/02 09:53:02 8.7 193.4 

09/06/02 09:53:12 9.0 193.•4 

09/06/02 09:53:22 9,2 192.7 

09/06/02 09:53:32 9.1 186.7 

09/06/02 09:53:42 9.5 182.3 

09/06102 09;53:52 11.6 176.2 

09/06/02 09:54:02 14.6 171.3 

09/06/02 09:54:12 15.7 166.6 

09/06102 09:54:22 13.6 163.0 

09/06102 09:54:32 11.3 160.5 

09/06/02 09:54:42 17.7 158.7 

09/06/02 09:54:52 21.0 157.0 

09/06/02 09:55:02 21.2 154.0 

09/06t02 09:55:12 150.9 

09106/02 09:55:22 20.9 151.1 

09/06/02 09:55:32 20.9 156.0 

09/06/02 09:55:42 20•9 162.9 

09/06/02 09:55:52 20.9 170.8 

09/06/02 09:56:02 21.0 176.8 

09/06/02 09:56:12 21.0 181.7 

09/06/02 09:56:22 21.0 165.8 

09/06/02 09:56:32 20.9 188.9 

09/06/02 09:56:42 21.0 191.2 

09/06/02 09:66:52 21.0 193.0 

09/06/02 09:67:02 21.1 193.9 

09/06102 09:57:12 21,1 195.1 

09/06/02 09:57:22 20.8 196,2 

09/06/02 09:57:32 20.8 

09/06/02 09;57:42 20.8 198.0 

09/06/02 09:57:52 20.8 198.8 

09/06/02 09:58:02 20.8 199,4 

09/06/02 09:58:12 20.9 200.0 

09/06/02 09:58:22 20,9 200.9 

09/06/02 09:58:32 20.9 202.0 

09106/02 09:58:42 20.8 202.9 

09106/02 09:58:52 20.8 204.0 

09/06/02 09:59:02 20.7 205.0 

09/06/02 09:59:12 20.7 205.9 

09/06/02 09:59:22 20.4 206,5 

09/06/02 09:59:32 20.7 207.0 

09/06/02 09:59:42 20.7 207,5 

09/06/02 09:59:52 20.8 207.6 

09/06/02 10:00:02 20.8 208.2 

09/06/02 10:00:12 20.8 208.4 

09/06102 10:00:22 20.7 208.5 

09/06/02 10:00:32 20.7 209.0 

09/06/02 10:00:42 20.8 209.0 

09/06/02 10:00:52 20.8 209.2 

09/06/02 10:01:02 20.7 209.3 

09/06/02 10:01:12 20.7 209.5 

09/06/02 10:01:22 20.7 209.7 

09/06/02 10:01:32 20.8 209.9 

09/06/02 10:01:42 20.8 210.0 

09/06/02 10:01:52 20.7 210.3 

09/06/02 10:02:02 20.6 210.6 

09/06/02 10:02:12 20.7 210,6 

09/06/02 10:02:22 20.6 210,8 

09/06/02 10:02:32 20.7 210.8 

09/06/02 10:02:42 20.7 211.0 

09/06/02 10:02:52 20.5 211.1 

09/06/02 10:03:02 20.7 211.1 

09/06/0210:03:12 20.6 211.3 

09/06/02 10:03:22 20.7 211.2 

09/06/02 10:03:32 20.6 211.3 

09/06/02 10:03:42 20.6 211.3 

09106/02 10:03:52 20.6 211,2 

09/06/02 10:04:02 20.5 211.1 

09/06/02 10:04:12 20,6 211.1 

09/06/02 10:04:22 20.5 211.0 

09706/02 10:04:32 20.5 211.0 

09/06/02 10:04:42 20.4 210.9 

09/06/02 10:04:52 20.5 211.0 

09/06/02 10:05:02 20.3 211.1 

09/06/02 10:05:12 20.0 211.1 

47,6 

47.6 

47.5 

47.3 

46.3 

44.6 

42.5 

40,5 

38.6 

37.0 

35,6 

34.7 

33.8 

32.9 

32.2 

31.8 

32.0 

33.1 

34.8 

36.7 

38.6 

40.2 

41.8 

42.7 

43.6 

44.5 

45.1 

45.6 

46.0 

46.5 

46.8 

47.1 

47,4 

47.6 

47.8 

48.0 

48.2 

48,3 

48.5 

48.7 

48.9 

49.0 

49,2 

49.3 

49.3 

49.4 

49.6 

49.8 

49.9 

50.0 

50.0 

50.1 

50.2 

50.1 

50.2 

50.4 

50.5 

50.6 

50.7 

50.8 

50.9 

50.9 

51.0 

51.1 

51.2 

51.3 

51.3 

51.3 

51.4 

51.4 

51.4 

51.4 

51.4 

51.7 

49.8 

49,8 

49.0 

47.2 

45.7 

44.6 

43.7 

42,9 

42.3 

41.9 

41.3 

40.7 

40.0 

40.0 

41.4 

42.9 

44.3 

45.4 

46.1 

46.7 

47.2 

47.4 

47.7 

47.9 

48.1 

48.3 

48.5 

48.7 

48.8 

48.9 

49.0 

49.1 

49.3 

49.5 

49.7 

49,9 

50.0 

50.1 

50.3 

50.4 

50.5 

50.5 

50.7 

50.6 

50.7 

50.8 

50.8 

50.9 

50.8 

50.9 

50.9 

50.9 

50.9 

51.0 

51.0 

51.0 

51.1 

51.1 

51.1 

51.2 

51.2 

51.3 

51,3 

51.2 

61.3 

51.2 

51.2 

51.2 

51.3 

51.2 

51.3 

51.3 

51.3 

Page 4 
916/01 Run #1 

09/06/02 10:05:22 20,2 211.2 

09/06/02 10:05:32 20,4 211.4 

09/06/02 10:05:42 20,3 211.3 

09106/02 10:05:52 20.1 211,2 

•3/06/02 10;06:02 20.3 211.3 

09/06/02 10:06:1'2 20.3 211.1 

09106/02 10:06 22 20.3 211.2 

09/06/02 10:06:32 20.1 211.1 

09/06/02 10:06:42 20.0 211.1 

09/06/02 10:06:52 20.0 211,0 

09106/02 10:07:02 20.1 211.0 

09/06102 10:07:12 19.9 210.9 

09/06/02 10:07:22 19.9 210.9 

09/06/02 10:07:32 19.9 210.8 

09/06/02 10:07:42 20.0 210.9 

09/06/02 10:07:52 20.0 210.8 

09/06]02 10:08:02 20.0 210.9 

09/06/02 10;08:12 19.9 210.9 

09/06/02 10:08:22 19.8 210.8 

09/06/02 10:06:32 19.8 210.8 

09/06/02 10:08:42 19.9 210.9 

09/06102 10:08:52 19.9 210.9 

09/06]02 10:09:02 19.7 210.9 

09/06]02 10:09:12 19.8 210,8 

09/06/02 10:09:22 19.8 210.7 

09/06/02 10:09:32 20.0 210.7 

09/06/02 10:09:42 19.8 210.5 

09/06/02 10:09:52 19.7 210.4 

09106/02 10:10:02 19.8 210.3 

09106/02 10:10:12 19.6 209,9 

09/06102 10:10:22 19.6 210.0 

09/06/02 10:10:32 19.7 209.8 

09]06/02 10:10:42 19.6 209.6 

09/06/02 10:10:52 19.3 209.5 

09/06/02 10:11:02 19.4 209.3 

09/06/02 10:11:12 19.5 209.2 

09/06/02 10:11:22 19.4 209.3 

09/06/02 10:11:32 19.4 209.1 

09/06/02 10:11:42 19.4 209.0 

09/06/02 10:11:52 19.5 209.0 

09]06/02 10:12:02 19.6 209.0 

09/06/02 10:12:12 19.6 209.0 

09/06/02 10:12:22 19.4 208.8 

09/06102 10:12:32 19,3 208.9 

09/06/02 10:12:42 19.4 208.9 

09/06/02 10:12:52 19.4 208,8 

09/06/02 10:13:02 19.4 208.8 

09]06/02 10:13:12 19.4 208.6 

09/06102 10:13:22 19.3 208.4 

09/06/02 10:13:32 19,2 208,3 

09106/02 10:13:42 19.2 208.2 

09/06/02 10;13:52 19.2 208.0 

09/06/02 10:14:02 19.2 206.0 

09/06/02 10:14:12 19.2 208.0 

09106/02 10:14:22 19.2 208.0 

09/06/02 10:14:32 19.3 208.0 

09/06/02 10:14;42 19.1 207,8 

09/06/02 10:14:52 19.2 207,8 

09106/02 10:15:02 19.1 207.7 

09/06/02 10:15:12 19.1 207.9 

09/06/02 10:15:22 19.0 207.8 

09/06/02 10:15:32 19.0 207.5 

09/06/02 10:15:42 18.9 207.5 

09/06/02 10:15:52 19.2 207,5 

09/06/02 10:16:02 19.3 207.5 

09/06/02 10:16:12 19.1 207.2 

09/06/02 10:16:22 19.1 207.0 

09/06/02 10:16:32 19.1 206.7 

09/06/02 10:16:42 19.0 206.6 

09/06/02 10:16:52 18,9 206.4 

09/06/02 10:17:02 19.0 206,2 

09/06/02 10:17:12 18.9 205.1 

09/06/02 10:17:22 18.9 205.6 

09/06/02 10:17:32 18.9 205,5 

51.7 51.3 

51,7 51.3 

51.8 51.3 

51.8 51.3 

51.9 51.3 

51.9 51.4 

51.9 51.3 

51.8 51.3 

51.9 51.3 

51.9 51.3 

51.9 51.3 

51.9 51.3 

51.9 51.4 

52.0 51.2 

52.1 51.3 

52.1 51.3 

52.1 51.3 

52.1 51.2 

52,2 51.1 

52.2 51.2 

52.2 51.3 

52.1 51.2 

52,2 51.2 

52.1 51.2 

52.1 51 .'1 

52.1 51.1 

52.2 51.1 

52,2 51.1 

52.2 51.1 

52.'1 51.1 

52.1 51.2 

52.2 51.2 

52.2 51.1 

52.2 51 .'1 

52.3 51.0 

52.3 51.0 

52.3 51.1 

52.3 51.1 

52,3 51.1 

52,4 51,1 

52.3 51.1 

52.2 51.1 

52.3 51.2 

52.4 51.2 

52.4 51.1 

52.3 51.1 

52.3 51.0 

52.3 51.0 

52.3 51.1 

52.3 51.0 

52.4 51.0 

52.5 51.0 

52.5 51,0 

52.4 51.1 

52.5 51.0 

52.5 51.1 

52.5 51.1 

52.5 51.0 

52.6 51.0 

52.7 51.1 

52.7 51.1 

52.6 51.0 

52,6 51.0 

52.6 51.0 

52.6 51.0 

52.6 51.0 

52.5 51.0 

52.5 51.0 

52.4 51 .o 

52.5 51.0 

52.5 51.0 

52.4 51.0 

52.5 51.0 

52.5 50.9 

Page 5 

25 
9/6/01 Run #1 

09106/02 10:17:42 19.0 205.4 52.5 50,9 09106/02 10:17:52 18.8 205.5 52.5 50.9 09/06/02 !0:16:02 18.6 205.3 52.5 50.8 09/06/02 10:16;12 18.6 205.3 52.5 50.9 09/06/02 10:18:22 18.5 205.4 52.5 50.9 09/06102 10:18:32 18.6 205.4 52.5 50.9 

09/06/02 10:16:42 18.5 205.3 52.6 50.6 09/06/02 10:18:52 18.4 205,2 52.6 50.6 09/06/02 10:19:02 18.5 204.7 52.5 50.9 09106/02 10:19:12 18.5 204.7 52.5 50.6 09/06/02 10:19:22 18.5 204.5 52.5 50.6 09/06/02 10:19:32 18.3 204.2 52•3 50.6 09106/02 10:19:42 18.2 204.2 52.2 50.6 09106102 10:19:52 16.2 204.3 52.0 50.7 09/06/02 10:20;02 18.3 204.4 52.0 50.6 

09/06/02 10:20:12 18.2 204.4 51.9 50.6 09/06/02 10:20:22 16.1 204.3 52.0 50.6 09/06/02 10:20:32 18.2 204.3 62.0 50,7 09/06/02 10:20:42 18.0 204.1 52.1 50.7 09/06/02 10:20:52 18.9 203.9 52.4 50.8 

09/06/02 10:21:02 18.4 203.6 52.5 50.8 09/06/02 10:21:12 18.6 203.5 52.5 50.8 

09/06/02 10:21:22 18.3 203.5 52.7 50.8 09/06/02 10:21:32 18.2 203.5 52.7 50.8 09/06/02 10:21:42 18.2 203.2 52.7 50.8 09/06/02 10:21:52 18.1 203.1 52.6 50.8 

Stop Run #1 17.14 201.64 39.65 49.94 

09/06/02 10:22:02 17.9 203.1 52.6 50.8 

09/06/02 10:22:12 17.9 202.9 52.6 50.8 09/06/02 10:22:22 15.4 203.1 52.5 50.8 

09/06/02 10:22:32 5.7 201.3 52,5 50.4 09/06102 10:22:42 4.5 201.0 52.0 49.9 09/06/02 10:22:52 4.0 200.8 51.7 50,0 

09/06/02 10:23:02 3.8 200.6 51.6 49.6 

09/06/02 10:23:12 2.4 197.4 51.6 47.5 

09/06/02 10:23:22 2,4 183.6 51.0 42.2 

09/06/02 10:23:32 2.3 160.9 48.8 35.7 

09/06/02 10:23:42 2.2 13•1 2 45.0 27.9 

09/06/02 10;23:52 2.0 108.5 41.1 22.2 

09/06/02 10:24:02 1.8 89.1 39.5 18.4 

09/06/02 10:24:12 1.7 74.8 41.1 15.4 

09/06/02 10:24:22 1.6 63.6 44.4 13.0 

09/06/02 10:24:32 1.5 53.8 48.7 10.9 

09/06/02 10:24:42 1.4 46.0 53.2 9.2 

09/06/02 10:24:52 1.4 38.9 57.5 7.7 

09/06/02 10:25:02 1.3 33.7 61.6 6.6 

09/06/02 10:25:12 1.3 28.8 65.4 5.6 

09/06/02 10:25:22 1,2 24.8 68.6 4.8 

09/06/02 10:25:32 1.3 21.7 71,5 4.2 

09/06/02 10:25:42 1.2 19.1 74.1 3.6 

09/06/02 10:25:52 1.3 17.5 76.5 3.3 

09/06/02 10:26:02 1.3 16.5 78.4 3,0 

09/06/02 10:26:12 1.3 15.0 80.2 2.8 

09/06/02 10:26:22 1.4 14.2 81.4 2.5 

09/06102 10:26:32 1.4 13.5 82.6 2.4 

09106/02 10:26:42 1.6 13.0 83.5 2.3 

09/06/02 10:26:52 1.7 12.6 84,3 2.2 

09/06/02 10:27:02 1.9 12.1 84.6 2.1 

09/06/02 10:27:12 2.2 11.7 85.0 2.0 

09/06/02 10:27:22 2.5 11.3 85.5 1.9 

09/06/02 10:27:32 2.4 11,2 85.9 1.8 09/06/02 10:27:42 2.3 10.8 86.3 1.8 09/06/02 10:27:52 2.3 10.6 86.5 1.7 09/06/02 10:28:02 2.4 10.3 86,8 1.6 09/06/02 10:28:12 2.5 10.2 87.0 1.6 

09/06/02 10:28:22 2.9 9.8 87.1 1,6 

09/0,6/02 10:28:32 3.5 9.5 87.3 1.6 09/06/02 10:28:42 4.2 9.5 87.2 1:5 

09/06/02 10:28:52 4.7 9.3 86.8 1.5 

09/06/02 10:29:02 3.9 9.2 86.7 1.5 

09/06/02 10;29:12 3.5 9.0 86.6 1.5 

91 ppm SO2 

Page 6 
09/06/02 10:29:22 2.5 8.9 

09/06/02 10:29:32 1,0 8.7 

09/06/02 10:29:42 0.9 6.6 

09/06/02 10:29:52 0.7 9.2 

09/06/02 10:30:02 0,6 10.1 

09106/02 10:30:12 0.6 11.7 

09/06/02 10:30;22 0.6 12.8 

09/06/02 10:30:32 0.6 12.8 

09/06/02 10:30;42 0.6 12.3 

09/06/02 10;30:52 0.6 11.5 

09/06/02 10:31:02 0.6 10.6 

09/06/02 10:31:12 0.6 10.3 

09/06/02 t0:31:22 0,6 9.7 

09/06/02 10:31:32 0.5 9.1 

09/06/02 10:31:42 0,5 8.7 

09/06102 10:31:52 0.5 8.3 

09/06/02 10:32:02 0.5 7,9 

09/06/02 10:32:12 0.5 7.6 

09/06/02 10:32:2.2 0.5 7.4 

09/06/02 10:32:32 0.5 7,1 

09/06/02 10:32:42 0.5 6.9 

09/06102 10:32:52 0,5 6.5 

09/06/02 10:33:02 0.5 6.2 

09/06/02 10:33:12 0.5 6.2 

09/06/02 10:33:22 0.7 5.9 

09/06/02 10:33:32 1.1 5.9 

09/06/02 10:33:42 0.5 5.9 

09/06/02 10:33:52 0.4 6.0 

09/06/02 10:34:02 0.4 6.0 

09/06/02 10:34:12 0.4 6.4 

09/06/02 10:34:22 0.4 9.2 

09/06/02 10:34:32 0.4 17.2 

09/06/02 10:34:42 0.4 29.5 

09/06/02 10:34:52 0.4 41.9 

09/06/02 10:35:02 0.4 53.0 

09/06/02 10:35:12 0.4 62.1 

09/06/02 10:35:22 0.4 69.5 

09/06102 10:35:32 0.4 74.8 

09/06/02 10:35:42 0.4 79.3 

09/06/02 10:35:52 0.4 82.7 

09/06/02 10:36:02 0.3 85.4 

09/06/02 10:36:12 0.4 87.4 

09/06/02 10;36:22 0.4 88.3 

09/06/02 10:36:32 0.4 69.2 

09/06/02 10:36:42 0.4 90.1 

09/06/02 10:36:52 0.4 90.9 

09/06/02 10:37:02 0.4 91.3 

09/06/02 10:37:12 0.4 92.0 

09/06/02 10:37:22 0.4 92.2 

09/06/02 10:37:32 0.4 92.6 

09/06/02 10:37:42 0.3 92.7 

09/06102 10:37:52 0,4 92.9 

09/06/02 10:38:02 0,4 92.9 

09/06/02 10:38:12 0.4 93.0 

09/06/02 10:38:22 0.4 92.9 

09/06/02 10:38:32 0,4 93.0 

09/06/02 10:38:42 0.4 93.0 

09/06/02 10:38:52 0.5 92.7 

09/06]02 10:39:02 10.5 92,8 

09/06/02 10:39:12 15.2 92.9 

09/06/02 10:39122 15,4 92.9 

09/06/02 10:39:32 15.4 93.1 

09/06/02 10:39:42 15.3 92.7 

09/06/02 10:39:52 15.3 91.2 

09/06/02 10:40:02 15.3 87.9 

09/06/02 10:40:12 4.8 81.9 

86.8 1.5 

87.2 1.5 

87.1 1.5 

85.9 1.6 

82.5 2.3 

74.3 5.2 

62.1 8.8 

50.6 11.6 

42.0 13.8 

35.7 15.6 

30.9 17.2 

27.0 18.5 

23.6 19.5 

20.7 20.5 

18.2 21.1 

16.0 21.7 

13.9 22.2 

12.2 22.5 

10.6 22.8 

9.3 23.0 

8.0 23.1 

7.1 23.2 

6.4 23.4 

5.6 23.5 

4.9 23.4 

4.4 23.3 

4.O 23..6 

3.6 23.5 

3.3 23.6 

3,1 23.1 

2.8 21.0 

2.6 17.6 

2.3 14.3 

2.1 11.4 

1.9 9.0 

1.8 7.2 

1.6 5.7 

1.5 4.7 

1.4 3.8 

1,3 3.2 

1.1 2.7 

1.0 2.2 

0.9 2.0 

0.9 1.7 

0.7 1.6 

0.6 1.5 

0.5 1.4 

0.4 1.3 

0.4 1.3 

0.3 1.2 

0.3 1.2 

0.3 1.1 

0.2 1.1 

0.1 1.1 

0.1 1.0 

0.'1 0.9 

0.0 0.9 

0.0 0.9 

0.0 1.0 

0.0 1.0 

-0.1 0.9 

-0.1 0.9 

-0.1 0,8 

-0.I 0.9 

0.0 1.0 

0.0 1/1 

25.1 ppm NOx 

Zero CO 

99.4 ppm CO 

Zero VOC. SO2 NOx 

14.7 ppm C3H8 

Page 7 
9/6/02 Run #3 

Date/Time VOC CO 

mm/drt/yy hh:mm:ss ppm ppm 

09106/02 10:41:12 19.8 26.3 

09/06/02 10:41:22 20.0 22.8 

09/06/02 10:41:32 20.0 22,5 

09/06/02 10:41:42 19.8 31.0 

09/06102 10:41:52 19.6 50.3 

09106/02 10:42:02 19.7 77,3 

09/06/02 10:42:12 19.7 102,2 

09/06/02 10:42:22 19.7 120.8 

09/06102 10:42:32 20.6 133.6 

09/06/02 10:42:42 20.2 142.2 

09/06102 10:42:52 19.7 149.2 

09/06/02 10:43:02 19.7 155.5 

09/06/02 10:43:12 19.6 160.0 

09/06/02 10:43:22 19.5 165.0 

09/06/02 10:43:32 19.4 169.9 

09/06/02 10:43:42 19.5 174.5 

09/06/02 10:43:52 19.4 177.5 

09/06/02 10:44:02 19.3 180.9 

09/06/02 10:44:12 19.3 183.9 

09/06/02 10:44:22 19.2 186.6 

09/06/02 10:44:32 19.2 188.7 

09/06102 10;44:42 19.0 190.7 

09/06/02 10:44:52 19.t 192.2 

$02 NC'x 

ppm ppm 

0.9 1.6 

1.1 1,6 

1.2 2.5 

1.4 6.1 

2.1 12.2 

3.6 19.2 

6,0 24.9 

9.1 28.8 

12.5 31.7 

15.8 33.7 

18.8 35.2 

21,5 36.5 

23.8 37.7 

25.8 39.0 

27.8 40.4 

29.9 41.7 

32.1 42, 

34.4 43,7 

36.4 44.5 

38.4 45.2 

40.2 45.8 

41.8 46.2 

43.1 46.7 

Start Run #2 

09/06/02 10:45:02 19.0 193.3 44.2 47.0 

09/06/02 10:45:12 18,9 193.8 45.2 47.4 

09/06/02 10:45:22 19.0 194.4 45.9 47.6 

09/06/02 10:45:32 18,8 195.2 46.6 47.9 

09/06/02 10:45:42 18.7 195.9 47.2 48,1 

09/06/02 10:45:52 18.9 196.6 47.7 48.3 

09/06/02 10:46:02 18.6 197.2 48,1 48.5 

09/06/02 10:46:12 18.6 197.8 48.4 48.6 

09/06/02 10:46:22 18.5 198.5 48.8 48.7 

09/06/02 10:46:32 18.6 199.0 49.0 48.9 

09/06/02 10:46:42 18.3 199.7 49,2 49.0 

09/06/02 10:46:52 18.3 200.0 49.3 49.2 

09/06/02 10:47:02 18.4 200.4 49.5 49.2 

09/06/02 10:47:12 18.4 200.8 49.7 49.3 

09/06/02 10:47:22 18.3 201.0 49.9 49.4 

09/06/02 10:47:32 18.5 201.4 50.1 49.4 

09/06/02 10:47:42 18.3 201,6 50.2 49.5 

09/06/02 10:47:52 18.4 201.8 50.3 49.6 

09/06/02 10:48:02 18.4 202.1 50.5 49.7 

09/06/02 10:48:12 18.4 202.0 50.6 49.7 

09/06/02 10:48:22 18.4 201.9 50.7 49.7 

09/06/02 10:48:32 18.6 202.0 50.8 49.7 

09/06/02 10:48:42 18.4 202.0 50.8 49.7 

09/06/02 10:48:52 18.4 201.8 50,9 49.7 

09/06/02 10:49:02 18.4 201.9 50.9 49,8 

09/06/02 10:49:12 18.2 201,9 50.9 49.7 

09/06/02 10:49:22 18.3 201.9 51.0 49.8 

09/06/02 10:49:32 18.3 202.3 51.2 49.9 

09/06/02 10:49:42 18.3 202.5 51.3 50.0 

09/06/02 10:49:52 18,2 202.7 51.4 49.9 

09/06/02 10:50:02 18.2 202.7 51,3 50.0 

09/06/02 10:50:12 18.1 202.9 51.3 50.0 

09/06/02 10:50:22 18.2 203.0 51.4 49.9 

09/06/02 10:50:32 18.2 202.9 51.5 50.1 

09/06/02 10:50:42 18.2 203.1 51.6 50.1 

09/06/02 10:50:52 18.1 203.0 51.6 50.1 

09/06/02 10:51:02 18.1 203.1 51.7 50.2 

09/06/02 10:51:12 18,0 203.2 51.8 50.1 

09/06/02 10:51:22 17.9 202.9 51.9 50.2 

09/06/02 10:51:32 18.1 202.7 51.9 50.1 

09/06/02 10:51:42 17.9 202.5 51.9 50.1 

09/06/02 10:51:52 18.0 202.1 51.9 50.0 

09/06/02 10:52:02 18.0 201,9 51.8 50.0 

09/06/02 10:52:12 18,0 201,6 51.7 49.9 

09/06/02 10:52:22 18,1 201.5 51,7 50.0 

09/06/02 10:52:32 17.9 201.2 51.8 49.9 

09/06/02 10:52:42 17.8 201.4 51.7 50.0 

Page 
916/02 Run #3 

09/05/02 10:52:52 

09/06/02 10:53:02 

09/06/02,10:53:12 

09/06/02 10:53:22 

09/06102 10:53:32 

09/06/02 10:53:42 

09/06/02 10:53:52 

09106/02 10:54:02 

09/06/02 10:54:12 

09/06/02 10:54:22 

09/06/02 10:54:32 

09/06/02 10:54:42 

09/06/02 10:54:52 

09/06/02 10:55:02 

09/06/02 10:55:12 

09/06/02 10:55:22 

09/06/02 10:55:32 

09/06/02 10:55:42 

09/06/02 10:55:52 

09/06102 10:56:02 

09106/02 10:56:12 

09/06/02 10:56:22 

09/06/02 10:56:32 

09106/02 10:56:42 

09/06/02 10:56:52 

09/06102 10:57:02 

09/06/02 10:57:12 

09/06/02 10:57:22 

09/06/02 10:57:32 

09/06/02 10:57:42 

09/06/02 10:57:52 

09106/02 10:58:02 

09/06/02 10:58:12 

09/06/02 10:58:22 

09/06/02 10:58:32 

09/06102 10:58:42 

09106/02 10:58:52 

09/06/02 10:59:02 

09/06/02 10:59:12 

09/06102 10:59:22 

09/06/02 10:59:32 

09/06/02 10:59:42 

09/06/02 10:59:52 

09/06/02 11:00:02 

09/06/02 11:00:12 

09/06/02 11 ;00:22 

09106/02 11:00:32 

09106/02 11:00:42 

09/06/02 11:00:52 

09/06/02 11:01:02 

09/06/02 11:01:12 

09/06/02 11:01:22 

09/06/02 11:0t:32 

09/06/02 11:01:42 

09/06/02 11:01:52 

09/06/02 11:02:02 

09/06/02 11:02:12 

09/06/02 11:02:22 

09/06/02 11:02:32 

09/06/02 11:02:42 

09/06/02 11:02:52 

09/06/02 11:03:02 

09/06/02 11:03:12 

09/06/02 11:03:22 

09/06/02 11:03:32 

09/06/02 11:03:42 

09/06/02 11:03:52 

09/06/02 11:04:02 

09/06/02 11:04:12 

09/06/02 11:04:22 

09106/02 11:04:32 

09/06/02 11:04:42 

09/06/02 11:04:52 

09/06/02 11:05:02 

17.9 

17.7 

17.8 

17.8 

17.8 

17.6 

17.6 

17.6 

17.6 

17,5 

17.5 

17.5 

17.5 

17.5 

17.5 

17.5 

17.5 

17.3 

17.4 

17.4 

17.4 

17.3 

17,3 

17,4 

17.4 

17.2 

17.4 

17.3 

17,3 

17.2 

17.2 

17.0 

17.0 

17.0 

17.1 

17.1 

17.0 

17.2 

17.2 

17.1 

17.0 

16:9 

16.9 

16.9 

16.9 

16.7 

16.9 

16.8 

16.7 

16.9 

16.8 

16.7 

16.7 

16.7 

16.6 

16,6 

16.5 

16.5 

16.6 

16.5 

16,5 

16.5 

16.5 

16,4 

16.4 

16.3 

16.5 

16.3 

16.2 

16.1 

16.2 

16.1 

16.1 

16.1 

201.1 

201.2 

201.2 

201,1 

200.9 

200.9 

200.8 

200.9 

200.9 

200.8 

200.8 

200.9 

200.8 

200.8 

200.7 

200.6 

200.3 

200.3 

200.6 

200.4 

200,6 

200.5 

200.4 

200.3 

200.2 

200.0 

199.7 

199.6 

199.4 

199.3 

199.3 

198.9 

198.7 

198.5 

198.2 

198.2 

198.1 

198.2 

198.1 

198.1 

198.1 

198.0 

198.1 

197.9 

197.9 

197.8 

197.6 

197.6 

197.5 

197.4 

197.4 

197.1 

197.1 

196.8 

196.7 

196.5 

196.4 

196.2 

196.1 

196.0 

195.8 

195.6 

195.1 

195.1 

194.9 

194.8 

194.9 

194.8 

194,8 

194.9 

194.5 

194.6 

194.5 

194.4 

51.7 

51.7 

51.7 

51.6 

51.5 

51.5 

51.6 

51.6 

51.6 

51.6 

51.7 

51.7 

51.8 

51.7 

51.6 

51.5 

51.4 

51.4 

61.4 

51.4 

51.4 

51.4 

51.3 

51.2 

51.3 

51.3 

51.1 

51.1 

51.2 

51.2 

51.2 

51,1 

51.1 

51.0 

51.0 

51.0 

51.0 

50.9 

50,8 

50.8 

50.7 

50.7 

50.7 

50.7 

50.6 

50.6 

50.6 

50.6 

50.5 

50.5 

50.6 

50.6 

50.5 

50.5 

50.4 

50.4 

50.4 

50.3 

50.3 

50,3 

50.3 

50.2 

50.1 

50.1 

50.0 

49,9 

49.9 

49,9 

49.8 

49.8 

49.8 

49.7 

49.7 

49.8 

50.0 

50.0 

50.0 

50.0 

50.0 

50.0 

50.0 

50.0 

50.0 

49.9 

49.8 

49.7 

49.8 

49.8 

49,8 

49.8 

49,9 

49.8 

49.8 

49.8 

49.9 

49.9 

49.9 

49.7 

49.8 

49.8 

49.8 

49.7 

49.7 

49.8 

49,8 

49.8 

49.8 

49,8 

49.7 

49.7 

49.7 

49.8 

49.7 

49.6 

49.7 

49.7 

49.8 

49.7 

49.7 

49.6 

49.6 

49.7 

49.6 

49.6 

49.6 

49.7 

49.6 

49.7 

49.6 

49.5 

49.4 

49.5 

49.6 

49.5 

49.4 

49.4 

49.5 

49.4 

49.4 

49.4 

49.3 

49.3 

49.3 

49.3 

49,3 

49.4 

49.4 

49.3 
9/6/02 Run #3 

09/06/02 11:05:12 16,0 194.3 49.8 49.3 09/06/02 1-1:05:22 15.9 194.1 49.7 49.3 09/06/02 11:05:32 15.9 194.2 49.7 49.3 09/06/02 11:05:42 16.0 194.2 49.6 49.2 09/06/02 11:(•3:52 16.0 194.2 49.5 49.3 09/06/02 11:06:02 16.0 194.0 49.5 49.2 09/06/02 11:06:12 15.9 194,0 49.4 49.3 09/06.,'02 11:06:22 16.2 193.8 49.4 49.2 09/06/02 11:06:32 16.1 193.7 49.4 49.3 09/06102 11:06:42 15,8 193.7 49.3 49.2 09/06102 11:06:52 15.8 i93.4 49.3 49.2 09/06/02 11:07:02 15.8 193.4 49.3 49.2 09/06/02 11:07:12 15.8 193.5 49.2 49.2 09/06/02 11:07:22 15.8 193.3 49.1 49.1 09/06/02 11:07:32 15.7 193.2 49.0 49.1 09/06/02 11:07:42 15,7 193.2 49.0 49.1 09/06/02 11:07:52 15.9 193.2 48.9 49.2 

'09/06102 

09/06/02 11:08:02 15.7 193.1 49.0 49,1 11:08:12 15.7 193.0 48.9 49,1 09/06/02 11:08:22 15.6 192.9 48.9 49.1 09106/02 11:08:32 15.6 192.7 48,8 49.0 09/06/02 11:08:42 15.7 192.6 48.7 49.0 09106/02 11:08:52 15.7 192.6 48.6 49.0 09/06/02 11:09:02 15.7 192.5 48.4 49.0 09/06/02 11:09:12 15.6 192.3 48.4 49.0 09/06/02 11:09:22 15.7 192.3 48.3 49.0 09/06/02 11:09:32 15.6 192.3 48.4 49.0 09/06/02 11:09:42 t5.6 192.3 48.5 49.1 09/06/02 11:09:52 15.4 192.1 48.5 49.0 09/06/02 11:10:02 15.4 192.0 48.5 49.0 09/06/02 11:10:12 15.5 191.8 48.6 49.0 09106/02 11:10:22 15.5 191.8 48.7 48.9 09/06/02 11:10:32 15.5 191.4 48.6 48.9 09/06/02 11:10:42 16.2 191.1 48,5 48.9 09/06102 11:10:52 15.8 190,9 48,5 48,9 .09/06/02 11:11:02 15.5 190.8 48.5 48.9 09/06/0211:11:12 15.4 190.5 48.4 48.9 09/06/02 11:11•22 15.2 190.4 48.3 48.8 09/06/02 11:11:32 15.2 190.3 48.3 48.8 09/06/02 11:11:42 15.1 190,3 48.3 48,9 09/06/02 11:11:52 15.1 190.1 48.2 48.8 09/06/02 11:12:02 15.0 190.1 48.2 48.8 09/06/02 11:12:12 15.0 189.9 48.2 48.8 09/06/02 11:12:22 15,2 189.6 48.1 48.8 09/06/02 11:12:32 15,0 189.5 48.1 48.8 09/06/02 11:12:42 15.0 189.3 48.1 48.8 09106/02 11:12:52 15.0 189.1 48.2 48.7 09/06/02 11:13:02 14.8 189.1 48.2 46.8 09/06/02:11:13:12 12.4 189.0 48.2 48.8 09/06/02 11:13:22 9.8 188.8 48.3 48.8 09/06/02 1t:13:32 10.2 188.6 48.2 48.8 

09/06/02 11:13:42 10.2 188,6 48.3 48.7 09/06/02 11:13:52 10.3 187.4 48.3 47.9 09/06/02 11:14:02 10,3 183.2 46.0 46.0 09/06/02 11:14:12 11,2 176.3 47.0 44.2 09/06/02 11:14:22 13.8 169.5 45.6 42.9 09/06/02 11:14:32 17.3 163.4 43.8 42.0 09/06/02 11:14:42 17.4 158.7 41.8 41.2 09/06/02 11:14:52 14.1 155.7 39.8 40,6 09/06/02 !1;15:02 12.2 152.8 38.0 40.2 09/06/02 11:15:12 18.5 150.1 36.4 39.7 09/06/02 11:15:22 21.5 147.3 35.2 39.1 09/06/02 11:15:32 21.6 144.4 34.4 38,4 09/06/02 11:15:42 21.5 142.0 33,3 37.7 09/06/02 11:15:52 21.3 142.1 32.5 38.3 09/06/02 11:16:02 21.1 147.4 32.0 39.9 09/06/02 11:16:12 21,1 156.6 32.0 41.7 09/06/02 t1:16:22 21.2 165.7 32.9 43.2 09/06/02 11:16:32 21.1 173,8 34.3 44.3 09/06/02 11: 6:42 21.3 178.9 35.8 45.2 09/06/02 11:16:52 21.2 183.1 37.6 45.7 09/06102 11:17:02 21.1 186,5 39.2 46.0 09/06/02 11:17:12 21.0 188,6 40.8 46.2 09/06/02 11:17:22 21.1 190.3 42.0 46.4 

Page 3 

30 
9/6/02 Run #3 

09/06/02 11:17:32 21.1 191,9 42.9 46.7 

09/06/02 11:17:42 21.1 192.9 43.8 46.8 

09/08/02 11:17:52 21,1 193.5 44.6 47.0 

.09/06/02 11:18:02 20.9 193.8 45,2 47.1 

09/06t02 11:18:12 21.0 194.3 45.:7 47.2 

09/06/02 11:18:22 21.0 194.7 46.0 47.3 

09/06/02 11:18:32 20.8 195.4 46.4 47.4 

09/06/02 11:18:42 20.8. 196.3 46.8 47.6 

09/06/02 11:18:52 20.9 197.4 47.1 47.9 

09/06/02 11:19:02 20.8 196.4 47.4 48.1 

09/06/02 11:19:12 20.9 199,4 47.7 48.4 

09/06/02 11:19:22 20.9 200.2 48.0 48.5 

09/06/02 11:19:32 20.9 200.9 48,2 48.6 

09/06/02 11:19:42 20.9 201.6 48.3 48.8 

09/06/02 11:19:52 21.0 202.2 48.5 48.8 

09106/02 11:20:02 21.0 202.6 48.6 48.9 

09/06/02 11:20:12 21,0 202,8 48.7 49.0 

09/06/02 11:20:22 20.9 203.4 48.9 49.1 

09/06/02 11:20:32 20.9 203.7 49.1 49.2 

09/06/02 11:20:42 20.9 204.2 49.2 49.2 

09/06/02 11:20:52 20.9 204.3 49.2 49.2 

09/06/02 11:21:02 20.9 204.7 49.2 49.3 

09/06/02 11:21:12 20.9 204.8 49.3 49.4 

09/06/02 11:21:22 20.9 205.2 49.3 49.4 

09/06/02 11:21:32 20.9 205.2 49.3 49.4 

09/06/02 11:21:42 20.9 205,2 49.4 49.4 

09/06/02 11:21:52 20.7 205.4 49.4 49.5 

09/06/02 11:22:02 20.9 205.4 49,4 49.6 

09/06/02 11:22:12 20.9 205.5 49.4 49.5 

09/06/02 11:22:22 20.9 205.7 49.4 49.5 

09/06/02 11:22:32 21.0 205.7 49.5 49.5 

09/06/02 11:22:42 20,9 205,8 49.5 49.6 

09/06/02 11:22:52 20.9 205,6 49.5 49.5 

09/08/02 11:23:02 20.9 205.8 49.6 49.6 

09/06/02 11:23:12 20,9 206,1 49.6 49.6 

09/06/02 11:23:22 20,8 205.9 49.6 49.6 

09/06/02 11:23:32 20.8 205.9 49,6 49.6 

09/06/02 11:23:42 20.7 205.9 49.6 49.7 

09/06/02 11:23:52 20.7 206.1 49.7 49.7 

09/06/02 11:24:02 20.7 206.1 49.8 49.7 

09/06/02 11:24:12 20.8 206.2 49.9 49.7 

09/06/02 11:24:22 20.7 206.3 49.9 49.8 

09/06/02 11:24:32 20.7 206.4 49.9 49.8 

09/06/02 11:24:42 20.7 206.4 49.9 49.8 

09/06/02 11:24:52 20.5 206.4 50.0 49.8 

09/06/02 11:25:02 20.7 206.5 50.0 49.9 

09/06/02 11:25:12 20.6 206.5 50.1 49.8 

09/06/02 1•1:25:22 20.6 206.4 50.1 49.9 

09/06/02 11:25:32 20.6 206.3 50.1 49.9 

09/06/02 11:25:42 20.7 206.2 50.1 49.9 

09/06/02 11:25:52 20.6 206.2 50.1 49.9 

09106/02 11:26:02 20.5 206.2 50. 49.9 

09/06/02 11:26:12 20.4 206.1 50.2 49.9 

09/06102 11:26:22 20.4 206.2 50.2 49.9 

09/06/02 11:26:32 20.5 206.0 50.4 49.8 

09/06/02 11:26:42 20.3 205.9 50.4 49.8 

09/06/02 11:26:52 20.3 205.7 50.3 49.9 

09/06/02 11:27:02 20.5 205.8 50.2 49.9 

09/06/02 11:27:12 20.3 205.9 50.2 49.8 

09/06/02 11:27:22 20.3 205.9 50.3 49.8 

09/06/02 11:27:32 20.4 205.7 50.3 49.8 

09106/02 11:27:42 20.3 205.7 50.3 49.8 

09/06/02 11:27:52 20.2 205.7 50.3 49.8 

09/06/02 11:28:02 20.2 205.9 50.2 49.8 

09/06/02 11:28:12 20.2 205.9 50.2 49.9 

09/06/02 11:28:22 20.1 205.8 50.2 49,8 

09/06/02 11:28:32 20.0 205.8 50.2 49.9 

09/06/02 11:28:42 20.0 205.9 50.1 49.9 

09/06/02 11:28:52 20.1 206.0 50.2 49.9 

09/06/02 11:29:02 20.0 205.8 50.2 49.8 

09/06/02 11:29:12 20.1 206.0 50.2 49.8 

09/06/02 11:29:22 20.1 205:8 50.2 49.9 

09/06/02 11:29:32 20.0 205.6 50.2 49.9 

09/06/02 11:29:42 20,1 205.5 50.2 49.8 

Page 
9/6/02 Run #3 

09/06/02 11:29:52 20.0 205.3 50.2 49.9 

09/06/02 11:30:02 20.0 205.0 50,2 49.9 

09/06/02 11:30:12 20,0 204.9 50.2 49.8 

09/06/02 11:30:22 19.9 204.9 50,3 49.8 

09/06/02 11:30:32 19.9 204.9 50.3 49.8 

09/06/02 11:30:42 20.0 204.8 50.4 49.8 

09/06/02 11:30:52 19.9 204.7 50.2 49.8 

09/06102 11:31:02 19.8 204.5 50.2 49.8 

09/06/02 11:31:12 19.8 204.4 50.2 49.8 

09/06/02 11:31:22 19.8 204.3 50.1 49.6 

09/06/02 11:31:32 19.8 204.3 50.1 49.6 

09/06,/02 11:31:42 19.7 204.2 50.1 49.6 

09/06/02 11:31:52 19.8 204.3 50,1 49.7 

09/06/02 11:32:02 19.7 204.4 50.2 49.7 

09/06/02 11:32:12 19.7 204.6 50.3 49.7 

09/06/02 11:32:22 19.7 204.5 50.3 49.7 

09106/02 11:32:32 19.7 204.6 50.2 49.7 

09/06/02 11:32:42 19.7 204.4 50.1 49,6 

09/06/02 11:32:52 19.5 204.7 50.1 49.6 

09/06102 11:33:02 19.5 204.5 50.0 49.7 

09/06/02 11:33:12 19.6 204.1 50.2 49.7 

09106/02 11:33:22 19.6 204.0 50.2 49.7 

09/06/02 11:33:32 19.5 203,9 50.2 49.6 

09/06/02 11:33:42 19.5 203.7 50.2 49.7 

09/06102 11:33:52 19.4 203.7 50.1 49.7 

09/06/02 11:34:02 19.6 203.9 50.1 49.7 

09/06/02 11:34:12 19.5 204.0 50.1 49.7 

09/06/02 11:34:22 19.5 204.2 50.2 49.7 

09/06/02 11:34:32 19.3 204.0 50.2 49.7 

09/06/02 11:34:42 19.3 204.0 50.2 49.7 

09/06/02 11:34:52 19.4 204.0 50.2 49.7 

09/06/02 11:35:02 19.3 203.7 50.2 49.7 

09/06/02 11:35:12 19.3 203.6 50.1 49.6 

09/06/02 11:35:22 19.3 203.4 50.1 49.6 

09/06/02 11:35:32 19.3 203.4 50.1 49.6 

09/06/02 11:35:42 19.3 203.1 50.1 49.6 

09106/02 11:35:52 19.3 203.0 50.1 49.6 

09/06/02 11:36:02 19.3 202.9 50.1 49.6 

09/06/02 11:36:12 19.2 202.6 50.0 49.5 

09/06102 11:36:22 19,2 202.7 50.1 49.5 

09/06/02 :36:32 19,2 202.7 50.3 49.5 

09/06102 11:36:42 19.1 202,7 50.2 49.5 

09/06/02 11:36:52 19.0 202.6 50.2 49.5 

09/06/02 11:37:02 19.1 202.6 50.2 49.4 

09/06/02 11:37:12 19.1 202.6 50.2 49.5 

09/06/02 11:37:22 19.2 202.3 50.2 49.4 

09/06/02 11:37:32 19.0 202.1 50.2 49.5 

09/06/02 11:37:42 19.0 202.0 50.3 49.5 

09/06/02 11:37:52 19.1 201.7 50.3 49.5 

09/06/02 11:38:02 19.1 201.7 50.3 49.5 

09/06/02 11:38:12 19.0 201.5 50.3 49.5 

09/06/02 11:38:22 19.0 201.3 50.2 49.4 

09/06/02 11:38:32 19.0 201.2 50.3 49.4 

09/06/02 11:38:42 19.0 201.4 50.3 49.4 

09/06/02 11:38:52 18.9 201.4 50.3 49.4 

09/06/02 11:39:02 18.8 201.4 50.2 49.4 

09/06/02 11:39:12 18.8 201.4 50.2 49.4 

09/06/02 t1:39:22 18.8 201.3 50.2 49.3 

09/06/02 11:39:32 18.8 201,0 50.1 49.3 

09/06/02 11:39:42 18.8 200.9 50.0 49.3 

09/06/02 11:39:52 16,7 200,9 50.0 49.3 

09/06/02 11 ;40:02 18.7 200.8 50.0 49.3 

09/06/02 11:40:12 18.6 200.5 50.0 49.3 

09/06/02 11:40:22 18.6 200.3 50.0 49.3 

09/06/02 11:40:32 18.6 200.5 50,1 49.3 

09/06/02 11:40:42 18,5 200.2 50.1 49.3 

09/06/02 11:40:52 -•,• 18.4 200.1 50.1 49.4 

09/06/02 11:41:02 18.6 200.1 50.1 49.4 

09/06/02 11:41:t2 18.6 200.2 50.1 49.4 

09/06/02 11:41;22 16.5 200.1 50,1 49.4 

09/06/02 11:41:32 18.6 200.0 49.9 49.4 

09/06/02 11:41:42 18.4 199.9 49.9 49.3 

09/06/02 11:41:52 18.4 200.0 49.9 49.2 

09/06/02 11:42:02 16.4 199.9 49.9 49.3 

Page 5 

,32 
9/6/02 Run #3 

09/06/02 11:42:12 

09/06/02 11:42:22 

09/06/02 11:42:32 

09/06/02 11:42:42 

09/06/02 11:42:52 

09/06/02 11:43:02 

09/06/02 11:43:12 

09106/02 11:43:22 

09/06/02 11:43:32 

09/06/02 11:43:42 

09/06/02 :43:52 

09/06/02 11:44:02 

09/06/02 11:44:12 

09/06/02 11:44:22 

09/06/02 11:44:32 

09/06/02 11:44:42 

09/06/02 11:44:52 

09/06/02 11:45:02 

09/06/02 11:45:12 

09106/02 11:45:22 

09/06/02 11:45:32 

09/06/02 11:45:42 

09/06/02 11:45:52 

Stop Run #2 

09106/02 11:46:02 

09/06/02 11:46:12 

09/06/02 11:46:22 

09/06/02 11:46:32 

09/06/02 11:46:42 

09/06/02 11:46:52 

09/06/02 11:47:02 

09/06/02 11:47:12 

09/06/02 11:47.'22 

09/06/02 11:47:32 

09/06/02 11:47:42 

09/06/02 11:47:52 

09/06/02 11:48:02 

09/06/02 11:48:12 

09/06/02 11:48:22 

09/06/02 11:48:32 

09/06/02 11:48:42 

09/06/02 11:48:52 

09106/02 11:49:02 

09/06/02 11:49:12 

09/06/02 11:49:22 

09106/02 11:49:32 

09/06/02 11:49:42 

09106/02 11:49:52 

09/06/02 11:50:02 

09/06/02 11:50:12 

09/06/02 11:50:22 

09/06/02 11:50:32 

09/06/02 11:50:42 

09/06/02 11:50:52 

09/05/02 11:51:02 

09/06/02 11:51:12 

09106/02 11:51:22 

09/06/02 11:51:32 

09/06/02 11:51:42 

09/06/02 11:51:52 

09/06/02 11:52:02 

09/06/02 11:52:12 

09/06/02 11:52:22 

09/06/02 11:52:32 

09/06/02 11:52:42 

09/06/02 11:52:52 

09/06/02 11:53:02 

09/06/02 11:53:12 

09/06/02 11:53:22 

09/06/02 11:53:32 

09/06/02 11:53:42 

09/06/02 11 i53:52 

18.4 

18.5 

18.5 

18.5 

18.5 

18.6 

18.4 

18.3 

18.2 

18.3 

18.2 

18.2 

18.1 

18.1 

18.2 

14.8 

11.1 

11.0 

11.3 

11.3 

11.7 

11.3 

5.3 

18.10 

4.5 

5.0 

5.7 

5.9 

4.1 

3.3 

2.8 

2.5 

2,2 

2,1 

2.0 

1.9 

1.8 

1.8 

1.8 

1,8 

1.7 

1.6 

1.6 

1.5 

1.4 

1.3 

1.3 

1.3 

1.3 

1.8 

1.4 

1.3 

1.3 

1.2 

1.2 

1.2 

1.2 

1.2 

1.1 

1.0 

1.1 

1.0 

1.0 

1.0 

0.9 

1.0 

0.9 

1.0 

1.0 

0.9 

0.9 

1.0 

199.9 

199.8 

199.7 

199.7 

199.5 

199,3 

199.1 

199,0 

198.9 

198.7 

198.5 

198.2 

198.2 

197.9 

197.6 

197.6 

197.4 

197.3 

197.1 

195.8 

19t .5 

183.9 

176.1 

197.65 

171.4 

166.8 

162.9 

158.7 

149.1 

134.5 

117.3 

98.6 

80.0 

64.5 

53,1 

44.9 

37.9 

33.2 

28.5 

24.4 

21,0 

18.4 

16.9 

15.2 

13.7 

12,6 

11.6 

10.6 

9.8 

9.0 

8.5 

8.0 

7,8 

7.9 

7.8 

7,8 

8.0 

8.0 

7.7 

7,5 

7,3 

7.1 

6.9 

6.7 

6.7 

6.6 

6.3 

6,3 

6.6 

6.3 

6.0 

49.8 

49.8 

49.8 

49.7 

49.7 

49.6 

49.5 

49.5 

49.5 

49.4 

49.4 

49.4 

49.4 

49.4 

49.5 

49.5 

49.6 

49.6 

49.5 

49.2 

48.5 

47.0 

49.17 

45,1 

43.5 

42.0 

40.5 

39.1 

37.5 

35.1 

32.3 

29.5 

28.2 

29.1 

31.7 

35.4 

39,4 

43.5 

47.5 

51.3 

54.9 

58.2 

61.2 

64.0 

66.5 

68.7 

70.6 

72.3 

73.9 

75.2 

76.5 

77.4 

78.2 

79.0 

79.8 

80.6 

81.1 

81.7 

82.3 

82.8 

83.2 

83.6 

84.0 

84.3 

84.4 

84.5 

84.6 

84.8 

85.0 

85.1 

85.2 

49.3 

49.3 

49.3 

49.2 

49.2 

49.1 

49.1 

49.1 

49.1 

49.1 

49.0 

49.1 

49.0 

49.0 

49.0 

49.0 

48.9 

48.9 

48.9 

47.8 

45.9 

44.2 

42.6 

48.95 

41.7 

41.1 

40.5 

38.7 

35.3 

30.5 

25.4 

20.3 

15.9 

12.9 

10.8 

9.1 

7.8 

6.7 

5.8 

5.0 

4.3 

3.8 

3.3 

3.0 

2.7 

2,4 

2.2 

2.0 

1.9 

1.7 

1.6 

1,6 

1.6 

1,5 

1.5 

1.5 

1.5 

1.4 

1,4 

1.3 

1.3 

1.2 

1.2 

1,3 

1.2 

1.2 

1.2 

1.2 

1.2 

1.2 

1.1 

1.1 

Page 6 

33 
9/6/02 R•Jn #3 

09/06/02 11:54:02 0.9 5.9 85,3 1.0 

09/06/02 11:54:12 0,9 5.9 85.4 1.1 

09/06/02 11:54:22 0.9 5.9 86,5 .I 

09/06/02 11:54:32 0.9 5.6 85.5 1.0 

09/06/02 11:54:42 0.9 5.5 85.5 1.0 

09/06/02 11:54:52 0.9 5.6 85.6 1.0 

09/06/02 11:55:02 1.0 5.5 85.5 1.0 

09/06/02 11:55:12 2.8 5.6 85.t 0.9 

09/06/02 11:55:22 3,4 5.8 84.7 1.0 

09/06/02 11;55:32 3.4 5.5 84.6 1.0 

09/06/02 11:55:42 3.3 5.6 84,6 1.0 

09/08/02 11:55:52 1.3 5.5 84.8 1.0 

09/06/02 11:56:02 1.0 5.6 85.1 1.0 

09106/02.11:56:12 1.0 6.0 84.5 1.1 

09/06/02 11:56:22 0.9 6.3 81.9 1.4 

09/06/02 11:56:32 0.9 7.7 75.4 3.7 

09/06/02 11:56:42 0,9 8.7 65.6 7.3 

09/06/02 11:56:52 0.9 8.6 56.0 10.6 

09/06/02 11:57:02 0.9 8.0 48.2 13.3 

09/06/02 11:57:12 0.9 7.2 42.0 15.5 

09/06/02 11:57:22 1.0 6.8 37.0 17.4 

09/06102 11:57:32 1,0 6,0 32.6 18.9 

09/06/02 11:57:42 1.0 5.4 28.6 20.1 

09106/02 11:57:52 1.0 5.0 25.0 21.0 

09106/02 11:58:02 1.0 4.6 21.9 21.7 

09/06/02 11:58:12 1.0 4.2 19.0 22.3 

09/06/02 11:58:22 1.0 3.9 16.5 22.7 

09/06/02 11:58:32 1.0 3.7 14.2 22.9 

09/06/02 11:58:42 1.0 3.6 12.2 23.1 

09/06/02 11;58:52 1.0 3,4 10.5 23.3 

09/06/02 11:59:02 1.0 3.5 9.0 23.4 

09/06/02 11.:59:12 0.9 3.4 7.7 23.5 

09/06/02 11:59:22 0.9 3.4 6.8 23.6 

09/06/02 11:59:32 0.9 3.3 5.8 23.6 

09/06/02 11:59:42 0.9 3.3 4.8 23.6 

09/06/02 11:59:52 1.3 3.3 4.0 23,4 

09/06/02 12:00:02 1.1 3.2 3.5 23.6 

09/06102 12:00:12 1.0 3.3 3,1 23.6 

09106/02 12:00:22 1.0 3.2 2.6 23.6 

09/05/02 12:00:32 1.0 3.4 2.1 23.4 

09/06/02 12:00:42 1.0 5.4 1.8 21.7 

09/06/'02 12:00:52 0.9 12.6 1.5 18.4 

09106/02 12:01:02 0.9 24.2 1.3 14.7 

09/06/02 12:01:12 0,9 37.6 1.0 11.6 

09/06/02 12:01:22 0.9 49.9 0.7 9.0 

09/06/02 12:01:32 0.9 59.8 0.4 7,0 

09/06/02 12:01:42 0.9 68.0 0.2 5.5 

09/06/02 12:01:52 0.9 73.7 0.1 4.4 

09/06/02 12:02:02 0.9 78.6 0.1 3,5 

09/06/02 12:02:12 0.9 82,0 0.0 2.9 

09/06/02 12:02:22 0,9 84.7 -0.1 2.4 

09/06/02 12:02:32 0.9 86.6 -0.3 2.0 

09/06/02 12:02:42 0.9 87.7 -0.4 1.7 

09/06/02 12:02:52 0.9 88.4 -0,5 1.6 

09/06/02 12:03:02 0.9 89.0 -0.7 ,S 

09/06/02 12:03:12 0.9 90.0 -0.8 1.3 

09/06/02 12:03:22 0.9 90.6 -0.9 1.3 

09/06/02 12:03:32 0.9 91.0 -1.0 1.2 

09/06/02 12:03:42 0.9 91.4 -1.1 1.1 

09/06/02 12:03:52 0.9 91.5 -0,6 1.0 

09/06/02 12:04:02 0.9 91.8 -0.1 1.0 

09/06/02 12:04:12 0.9 91.9 -0.2 0.9 

09/06/02 12:04:22 0.8 92.3 -0.3 1.0 

09/06/02 12:04:32 0.9 92.7 -0.3 0.9 

09/06/02 12:04:42 0.9 92.8 -0.4 0,9 

09/06/02 12:04:52 0.9 93.0 -0.6 0.8 

09/0602 12:05:02 0.9 93.4 -0.6 0.8 

09/06/02 12:05:12 0,9 93.4 -0.4 0.8 

09/06/02 12:05:22 0.9 93.4 -0.1 0,8 

09/06/02 12:05:32 0.9 92.9 -0.2 0.7 

09/06/02 12:05:42 8.4 93.1 -0.2 0.8 

91 oDm $02 

25.1 ppm NOx 

7ero CO 

99.4 opm CO 

Zero VOC, CO, SO2 

Page 7 
916102 Run #3 

09/06/02 12:05:52 15.7 93.1 -0.2 0,8 09/06/02 12:06:02 15.4 93.1 -0.3 0.8 

09106102 12:06:12 !5.3 93.0 -0.3 0,7 

09/06/02 12:06:22 15.3 92.8 -0.4 0.7 

09/06/02 12:06:32 15.3 91.5 -0.5 0.8 

09/06/02 12:06:42 15.3 88.6 -0.4 0.8 

09/06/02 12:06:52 12.7 62.5 -0.3 0.9 09/06/02 12:07:02 3.5 72.6 =0.2 1.1 

14.7 ppm C3H8 

Page 8 

35 
916/O•Ru n #3 

Date/Time VOC CO 802 NOx 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

09106102 12:07:42 19.2 29.3 0.4 1.2 

09/06/02 12:07:52 19.5 23.9 0.6 1.1 

09106102 12:08:02 19.2 20.0 0.7 1.0 

Q9/06/02 12:08:12 19.0 17.9 0.6 1.1 

09106102 12:08:22 18.8 20.5 0.6 3.2 

09/06/02 12:08:32 18.9 35.9 1.2 8.9 

09/06/02 12:08:42 18.7 62.3 2.8 16.4 

09/06/02 12:08:52 18.5 90.7 5.5 23.3 

09t06/02 12:09:02 18,4 114.0 9.0 28.9 

09/06/02 12:09:12 18.4 131.3 12.8 33.0 

09/06/02 12:09:22 18.3 144.0 16.9 36.0 

09106102 12:09:32 18.2 155.1 21.0 38.3 

09/06/02 12:09:42 18.1 163.1 24.7 40.1 

09/06/02 12:09:52 18.2 169.6 28.2 41.4 

Start Run #3 

09/06/02 12:10:02 18.3 174.7 31.4 42.4 

09/06/02 12:10:12 18.2 177.6 34.3 43.3 

09/06/02 12:10:22 18.2 180.7 36.8 43.9 

09/06/02 12:10:32 18.1 183.2 39.0 44.5 

09106/02 12:10:42 18.1 185.3 40.9 45.0 

09/06/02 12:10:52 18.0 187.0 42.3 45.3 

09106/02 12:11:02 18.0 188.3 43.7 45.7 

09/06/02 12:11:12 18.1 189.3 44.9 45.9 

09/06102 12 11 22 17.9 190.3 45.8 46.0 

09/06102 12:11:32 18.0 190,9 46.6 46,3 

09/06/02 12:11:42 18.0 191.7 47.4 46.5 

09/06/02 12:11:52 18.0 192.3 48.1 46.6 

09/06/02 12:12:02 17.9 192.7 48.7 46.8 

09/06/02 12:12:12 17.9 192.8 49.1 46.8 

09/06/02 12:12:22 17.7 193.1 49.3 47/ 

09/06/02 12:12:32 17.9 193.2 49.6 47.1 

09/06/02 12:12:42 17.9 193,3 49.8 47.1 

09/06/02 12:12:52 17.6 193.5 50.1 47.2 

09/06102 12:13:02 17.6 193.7 50.4 47.3 

09/06/02 12:13:12 17.8 193.9 50.5 47.3 

09106/02 12:13:22 17.7. 194.0 50.7 47.4 

09/06/02 12:13:32 17.6 194.2 50.7 47.4 

09/06/02 12:13:42 17.6 194.3 50.8 47.5 

09/06102 12:13:52 17.6 194.3 50.9 47.5 

09/06/02 12:14:02 17.5 194.4 51.0 47.6 

09/06/02 12:14:12 17,5 194.6 51.0 47.6 

09/06/02 12:14:22 17.6 194.8 51.1 47.7 

09/06/02 12:14:32 17.5 195.0 51.2 47.7 

09/06/02 12:14:42 17.5 195.3 51.3 47.8 

09/06/02 12:14:52 17.5 195.4 51.4 47,7 

09/06/02 12:15:02 17,4 195.5 51.6 47.8 

09/06102 12:15:12 17.4 195.3 51.6 47.8 

09/06102 12:15:22 17.4 195.5 51.5 47.8 

09/06/02 12:15:32 17.5 195,5 51.6 47,7 

09/06/02 12:15:42 17.4 195.7 51.5 47.8 

09/06/02 12:15:52 17.4 195.6 51.6 47.8 

09/06/02 12:16:02 17.4 195,6 51.6 47.8 

09106/02 12:16:12 17.4 195,7 51,5 47.8 

09/06/02 12:16:22 17.3 195.8 51.6 47.8 

09/06/02 12:16:32 17.3 195.7 51.7 47.8 

09/06/02 12:16:42 17.3 51.6 

09/06/02 12:16:52 17.3 195.7 51.5 47.8 

09/06/02 12:17:02 17,3 195.8 51.5 47.8 

09/06/02 12:17;12 17.3 195.6 51.5 47.8 

09/06/02 12:17:22 17.3 195.8 51.5 47.8 

09/06/02 12:17:32 17.2 195.7 51.5 47.8 

09/06/02 12:17:42 17.2 195.4 51.5 47.8 

09/06/02 12:17:52 17.1 195,5 51.5 47.8 

09/06/02 12:18:02 17.2 195.2 51,5 47.8 

09/06/02 12:18:12 17.1 195,.2 51.4 47.7 

09/06/02 12:18:22 17.0 195.1 51.5 47.8 

09/06/02 12:18:32 17.0 195.1 51.6 47.8 

09/06/02 1.2:18:42 17.0 195.1 51.6 47,7 

09/06/02 12:18:52 17.1 194.9 51.6 47.8 

09/06/02 12:19:02 17.1 195.1 51.5 47.8 

09/06/02 12:19:12 17.0 194.9 51.5 47.8 

3G 

Page 
9/6/02 Run #3 

09/05/02 12:19:22 16.9 194.9 51.4 47.8 09/06/02 12:19:32 17.0 194.5 51.3 47,7 09/06/02 12:19:42 17.0 194.5 51.3 47.7 

09/06/02 12:19:52 17.0 194.5 51.4 47.7 09/06/02 12:20:02 16.9 194.3 51.3 47.7 09/06/02 12:20:12 17.0 194.2 51.2 47.7 09/06/02 12:20:22 17.0 194.1 51.2 47.7 09/06/02 12:20:32 17.0 194.1 51.2 47.6 09/06/02 12:20:42 16.9 194.1 51.2 47.6 09/06/02 12:20:52 16.9 193.9 51.1 47.6 09/06/02 12:21:02 16.9 193.9 51.0 47.6 09/06/02 12:21:12 17.0 193,8 50.9 47.7 ,09/06/02 12:21:22 16.9 193,8 50.8 47.7 09/06/02 12:21:32 16.8 193.9 50.8 47.7 09/06/02 12:21:42 16.7 194.0 50.7 47.7 ,09/06/02 12:21:52 16.7 193.9 50.6 47.7 09/06/02 12:22:02 16,9 193.9 50.5 47.7 09/06/02 12:22:12 16.7 193.8 50,5 47.7 09/06/02 12:22:22 16.7 193.9 50.4 47.7 09/06/02 12:22:32 16.8 194.0 50.5 47.7 09/06/02 12:22:42 16.9 193,9 50.4 47.6 09106/02 12:22:52 16.8 193.9 50.4 47.7 09/06/02 12:23:02 16.7 193.8 50.3 47.7 09/06/02 12:23:12 16.9 193,6 50.2 47.6 09/06/02 12:23:22 16.8 193.4 50.1 47.5 09/06/02 12:23:32 16.7 193.3 50.0 47.5 09/06/02 12:23:42 16,6 193.3 50.0 47.6 09/06/02 12:23:52 16.5 193.2 50,1 47.5 09/06/02 12:24:02 16.5 193.0 50,1 47.5 09/06/02 12:24:12 16.5 192.9 50.1 47,4 09/06/02 12:24:22 16.3 192.9 50.1 47.4 09/06/02 12:24:32 16.3 192,8 50.2 47.5 

09/06/02 12:24:42 16.2 192.6 50.2 47.4 09/06/02 12:24:52 16.3 192.5 50.2 47.4 09/06102 12:25:02 16.3 192.4 50.3 47.4 09/06/02 12:25:12 16.1 192.5 50.2 47.4 09/06/02 12:25:22 16.1 192.2 50.1 47.4 09/06/02 12:25:32 16.2 192.3 50.1 47.4 

09/06/02 12:25:42 16.1 192.3 49.9 47.3 

09/06/02 12:25:52 16.1 192.4 50.0 47.4 09/06/02 12:26:02 16.0 192.2 49.9 47.3 09/06/02 12:26:12 16.0 192.3 49.9 47.3 

09/06/02 12:26:22 16.0 192.1 49.8 47.3 09/06/02 12:26:32 15,9 191.9 49,7 47.3 

09/06/02 12:26:42 16.0 191.6 49.7 47.3 

09/06/02 12:26:52 16.0 191.5 49.6 47.3 

09/06/02 12:27:02 16,0 191.4 49.6 47.3 09/06/02 12:27:12 16.0 191.3 49.6 47.2 

09/06/02 12:27:22 15.9 191.3 49.6 47.2 09/06/02 12:27:32 16.0 191.2 49.5 47.0 

09/06/02 12:27:42 15.8 191.2 49.4 47.1 09/06/02 12:27:52 15.8 191.1 49.3 47.1 09/06/02 12:28:02 15.8 191.0 49.3 47.1 

09/06/02 12:28:12 15.8 191.0 49.3 47.2 

09/06/02 12:28:22 15,7 190.7 49.4 47.2 

09/06/02 12:28:32 15.8 190.7 49.5 47.3 09/06/02 12:28:42 15.7 190.4 49,5 47.1 09/06/02 12:28:52 15.7 190.1 49.5 47.1 09/06/02 12:29:02 15.7 189.9 49.5 47.1 09/06/02 12:29:12 15.6 189.7 49.5 47.0 09/06/02 12:29:22 15.5 189.8 49.6 47.1 09/06/02 12:29:32 15,5 189.5 49.6 47.1 09/06/02 12:29:42 15.4 189.6 49.6 47.1 09/06/02 12:29:52 15.4 189.3 49.6 47.0 09/06/02 12:30:02 15,4 189.1 49.6 47.1 09/06/02 12:30:12 15.5 189.1 49.6 47.1 09/06/02 12:30:22 15.6 189.1 49.6 47.1 09/06/02 12:30:32 15.7 188.9 49.5 47.0 09/06/02 12:30:42 15.7 188.8 49.4 47.0 09/06102 12:30:52 15.7 188.6 49.4 46.9 09/06/02 12:31:02 15.6 188.6 49.3 47.0 09/06/02 12:31:12 15.6 188.5 49.3 47.0 09/06/02 12:31:22 15.5 188.3 49.3 46.9 09/06/02 12:31:32 15.4 188.0 49.2 46.9 

Page 2 

3? 
9/6/02 Rut• #3 

09/06/02 12:31:42 11.8 187.8 49.2 47.0 09/06/02 12:31:52 9.8 187.5 49.2 47.0 09/06/02 12:32:02 10.0 187,6 49.3 47.0 09/06/02 12:32:12 10.0 187.0 49.2 46.5 09/06/02 12:32:22 10.0 183.6 49.1 45.0 09/06/02.12:32:32 9.9 177.4 46.5 43.4 09/06/02 12:32:42 11.0 171.2 47.3 42.1 09/06/02 12:32:52 14.6 164.9 45.7 41.1 09/06/02 12:33:02 18.1 160.0 43.8 40.4 09/06/02 12:33:12 18.4 156.9 42.1 39.9 09/06/02 12:33:22 14.3 154.1 40.4 39.4 

09/06/02 

09/06/02 12:33:32 14.2 151.6 39.0 38.9 12:33:42 21.4 148.9 37.8 38.5 09/06/02 12:33:52 22.8 145.9 36.7 38.0 09/06/02 12:34:02 22.5 143.1 35.7 37.2 09/06/02 12:34:12 22.2 142.0 35.0 37.3 09/06/02 12:34:22 22.0 145.2 34.5 38.5 09/06/02 12:34:32 21.9 152.2 34.3 40.0 09/06/02 12:34:42 21.8 159.4 34.7 41.3 09/06/02 12:34:52 21.8 165.6 35.3 42.4 09/06/02 12:35:02 21.8 171.0 36.5 43.2 09/06/02 12:35:12 21.9 175.1 38.0 43.9 09/06/02 12:35:22 22.0 177.5 39.3 44.3 09/06/02 12:35:32 21.9 179.3 40.6 44.8 09/06/02 12:35:42 21.9 181.4 41.8 45.1 09/06/02 12:35:52 21.9 182.9 42.7 45.3 09/06/02 12:36:02 21.8 184.3 43.7 45.5 09/06/02 12:36:12 21.9 185.5 44.6 45.6 09/06/02 12:36:22 21.9 186.5 45.4 45.7 09/06/02 12:36:32 21.7 187.4 46.0 45.8 09106/02 12:36:42 21.7 187.9 46.5 45.9 09/06/02 12:36:52 21.8 188.6 46.9 46.0 09/06/02 12:37:02 21.9 189.2 47.4 46.1 09/06/0-2 12:37:12 21.7 189.7 47.8 46.4 09/06/02 12:37:22 21.7 190,4 48.2 46.5 09/06/02 12:37:32 21.6 191.1 48.4 46.7 09/06/02 12:37:42 21.7 191.8 48.7 47.0 09/06/02 12:37:52 21.8 192.3 49.0 47,1 09/06/02 12:38:02 21.6 192.7 49.1 47.2 09/06/02 12:38:12 21.6 193.2 49.3 47.3 09/06/02 12:38:22 21.7 193.6 49.4 47.3 09106/02 12:38:32 21.7 194.1 49.5 47.4 09106/02 12:38:42 21.8 194.3 49.7 47.5 09/06/02 12:38:52 21.8 194,6 49.8 47.6 09/06/02 12:39:02 21.7 194.8 50.0 47.6 09/06/02 12:39:12 21.8 194.7 50.2 47.8 09/06/02 12:39:22 21.7 194.8 50,3 47.7 09/06/02 12:39:32 21.7 194.8 50.5 47.8 09/06/02 12:39:42 21.8 194,8 50.6 47.9 09/06/02 12:39:52 21.7 195.3 50.7 47.9 09/06/02 12:40:02 21.8 195.4 50.9 47.9 09/06/02 12:40:12 21.7 195.7 50,9 48.0 09/06/02 12:40:22 21.8 195.8 50.9 47.9 09/06/02 12:40:32 21.6 195.9 51.0 47.9 09/06/02 12:40:42 21.7 195.8 51.1 48.0 09/06/02 12:40:52 21.7 195.8 51.1 48.0 09/06/02 12:41:02 21.8 195.7 51.1 48.0 09/06/02 12:41:12 21.7 196.6 51.1 48.0 09/06/02 12:41:22 21.4 197.0 51.0 48.1 09/06/02 12:41:32 21.5 197.2 51.0 48.1 09/06/02 12:41:42 21.6 197.5 51.1 48.1 09/06/02 12:41:52 21.5 197.7 51.2 48.0 09/06/02 12:42:02 21.5 197.9 51.2 48.0 09/06/02 12:42:12 21.5 197.8 51,2 46.0 09/06/02 12:42:22 21.3 197,6 51,3 48.0 09/06/02 12:42:32 21.3 197.7 51.4 48.0 09/06/02 12:42:42 21.3 197.8 51.3 48.1 09/06/02 12:42:52 21.5 197.8 51.3 48.2 09/06/02 12:43:02 21.6 198.0 51.3 48.0 09/06/02 12:43:12 21.4 198.2 51.3 48.1 09/06/02 12:43:22 21.4 198.2 51.3 48.2 09/06/02 12:43:32 21.3 198.6 51.3 48.1 09/06/02 12:43:42 21.2 198.5 51.3 48.2 09/06/02 12:43:52 21.3 198.6 51.4 48.2 

Page 3 
9/6/02 Run #3 

09/06/02 12:44:02 21.1 196.5 

09/06]02 12:44:12 21.2 198.5 

09/06/02 12:44:22 21.2 198.4 

09106/02 12:44:32 21.3 198.4 

09/06/02 12:44:42 21.2 198.4 

09/06/02 12:44:52 21.2 198.5 

09/06/02 12:45:02 21.3 198.5 

09/06/02 12:45:12 21.3 198.4 

09/06/02 12:45:22 21.4 198.5 

09106/02 12:45:32 21.2 198.5 

09/06/02 12:45:42 21.3 198,5 

09/06/02 12:45:52 21.4 198.4 

09/06/02 12:46:02 21.3 198.4 

09/06/02 12:46:12 21.3 198.4 

09/06/02 12:46:22 21.3 198.4 

09/06/02 12:46:32 21.2 198.3 

09/06/02 12:46:42 21.1 198.4 

09/06/02 12:46:52 21.3 198.5 

09/06/02 12:47:02 21.2 198.4 

09/06/02 12:47:12 21.0 198.4 

09/06/02 12:47:22 21.1 198.2 

09/06/02 12:47:32 20.9 198.1 

09/06/02 12:47:42 20.9 198.1 

09/06/02 12:47:52 20.8 198,1 

09106102 12:48:02 20.9 198.1 

09/06/02 12:48:12 20.8 198.'1 

09/06/02 12:48;22 20.9 198.1 

09/06/02 12:48:32 20.9 198.1 

09/06/02 12:48:42 20.8 198.0 

09/06/02 12:48:52 20.9 198.0 

09/06/02 12:49:02 20.8 198.0 

09/06/02 12:49:12 20.8 197.9 

09/06/02 12:49:22 20,8 198.0 

09/06/02 12:49:32 20.8 197.8 

09/06/02 12:49:42 20.7 197.8 

09/06/02 12:49:52 20.7 197.7 

09/06/02 12:50:02 20.7 197.5 

09/06/02 12:50:12 20.7 197.6 

09106102 12:50:22 20,8 197.5 

09/06/02 12:50:32 20.8 197.2 

09/06/02 12:50:42 20.8 197.1 

09/06/02 12:50:52 20.9 197.2 

09/06/02 12:51:02 20.8 197.0 

09/06/02 12:51:12 20.8 197.0 

09/06/02 12:51:22 20.7 196.8 

09/06/02 12:51:32 20.8 196.8 

09/06/02 12:51:42 20.5 196.8 

09/06/02 12:51:52 20.5 196,6 

09/06/02 12:52:02 20.5 196.6 

09/06/02 12:52:12 20.5 196.5 

09/06/02 12:52:22 20.4 196.2 

09/06/02 12:52:32 20.5 196.2 

09/06/02 12:52:42 20.3 196.2 

09/06/02 12:52:52 20.2 196.0 

09/06/02 12:53:02 20.2 195.9 

09/06/02 12:53:12 20.1 195.8 

09/06/02 12:53:22 20.2 195.7 

09/06/02 12:53:32 20.2 195.6 

09/06/02 12:53:42 20.3 195.2 

09106/02 12:53:52 20,1 195.1 

09/06/02 12:54:02 20.0 195.1 

09/06/02 12:54:12 20.1 194.9 

09/06/02 12:54:22 20.0 194.8 

-09/06/02 12:54:32 19.9 194.8 

09/06/02 12:54:42 19.9 194.5 

09/06/02 12:54:52 20.0 194.6 

09/06/02 12:55:02 20.0 194.4 

09/06]02 12:55:12 19.9 194.3 

09/06/02 12:55:22 19.7 194.4 

09/06/02 12:55:32 19.9 194.5 

09/06/02 12:55:42 19.9 194.5 

09/06/02 12:55:52 19.8 194.4 

09/06/02 12:56:02 19.9 194.4 

09/06/02 12:56:12 19.8 194.4 

51.3 48.1 

51.4 48.2 

51,4 48,2 

51.5 48.2 

51.5 48.'1 

51.4 48.2 

51.5 48.2 

51,5 48.2 

51.6 48.2 

51.5 48.2 

51.5 48.3 

51.6 48.2 

51.6 48.2 

51.6 48.2 

51.6 48.2 

51.6 48.2 

51.6 48.2 

51.6 48.2 

51.6 48.2 

51.7 48.2 

51.7 48.1 

51.6 48.1 

51,5 48.1 

51.6 48.2 

51.8 48.1 

51.7 48.1 

51.7 48.1 

51.7 48.2 

51.7 48.1 

51.7 48.2 

51.8 48.2 

51.9 48.2 

51.9 48.2 

51.9 48.2 

51.9 48.2 

51.8 48.2 

51.8 48.2 

51.8 48.1 

51.8 48.1 

51.7 48.1 

51.8 48.1 

51.9 48.1 

51.8 48.1 

51.9 48.1 

51.9 48.0 

51.9 48.0 

51.8 48.1 

51.8 48.0 

51.7 48.0 

51.7 48.0 

51.7 48.0 

51.7 48.0 

51.7 47.9 

51.6 48.0 

51.5 48.0 

51.5 48.0 

51.5 47.9 

51.5 47.9 

51.5 47.9 

51.4 48.0 

51.4 47.9 

51.5 47.9 

51.4 48.0 

51.4 47.9 

51.4 47.8 

51.4 47.9 

51.4 47.9 

51.5 47.8 

51.4 47.8 

51.4 47.8 

51.4 47.9 

51.4 47.9 

51.4 47.9 

51.4 47.8 

Page 4 

39 
9/6102 Ru• #3 

09/06/02 12:56:22 19.8 194.4 51,4 47.9 09/06/02 12:56:32 19.8 194.3 51.4 47.9 09/06/02 12:56:42 19.8 194.3 51.4 47.7 09/06/02 12:56:52 19.8 194.1 51.4 47.8 09/06/02 12:57:02 19.7 194.1 51.4 47.8 09106/02 12:57:12 19,7 194.0 51.4 47.8 09/06/02 12:57:22 19.6 193.9 51.5 47,7 09/06/02 12:57:32 19,6 194.0 51.4 47.7 09/06/02 12:57:42 19.5 193.8 51.4 47.7 09/06/02 12:57:52 19.4 193.7 51.4 47.7 09/06/02 12:58:02 19.4 193.7 51.4 47.7 09/06/02 12:58:12 19.3 193.7 51.4 47.7 09/06/02 12:58:22 19,4 193.6 51.3 47.7 09/06102 12:56:32 19.4 193.5 51.3 47.7 09/06/02 12:58:42 19.3 193.5 51.2 47.6 09/06/02 12:58:52 19.3 193.4 51.2 47.6 09/06/02 12:59:02 19.3 193.4 51.2 47.6 09/06/02 12:59:12 19.2 193.3 51.1 47.6 09/06/02 12:59:22 19.3 193.3 51.2 47.6 09106/02 12:59:32 19.3 193.4 51.3 47.6 09/06/02 12:59:42 19.3 193.2 51.2 47.6 09/06/02 12:59:52 19.2 193.2 51.2 47.6 09/06102 13:00:02 19.2 193.2 51.1 47.5 09/06102 13:00:12 19.2 193.3 51.0 47.6 09/06/02 13:00:22 19.2 193.2 51.1 47.6 09/06/02 13:00:32 19.1 193.1 51,1 47.5 09/06/02 13:00:42 15.3 193.1 51.1 47.5 09/06/02 13:00:52 11.7 193.0 51.0 47.5 09/06/02 13:01:02 12.1 192.9 51.0 47.5 09/06102 13:01:12 12.6 192.8 50.9 47.3 09/06102 13:01:22 12.8 190.7 50,8 46.1 09/06/02 13:01:32 13,3 185.3 50.3 44.5 09/06/02 13:01:42 15.6 178.1 49.3 43.0 09/06/02 13:01:52 19.3 172.3 47.8 41.9 09/06/02 13:02:02 20.0 166.8 46.1 41.0 09/06/02 13:02:12 18.1 162.4 44.5 40.4 09/06/02 13:02:22 14.7 159.3 42.8 40.0 09/06/02 13:02:32 19.9 156.8 41.5 39.3 09/06/02 13:02:42 23.1 152.8 40.2 38.7 09/06/02 13:02:52 22.8 148.4 39.2 37.9 09/06/02 13:03:02 22.7 145.5 38.3 37.6 09/06/02 13:03:12 22.6 147.1 37.4 38.4 09/06/02 13:03:22 22,5 153.5 37.0 39.8 09/06/02 13:03:32 22.1 160.9 37.2 41.3 09/06/02 13:03;42 22.2 168.8 38.0 42.5 09/06/02 13:03:52 22.1 174.8 39.0 43.5 09/06/02 13:04:02 22.2 179.1 40.4 44.2 09/06/02 13:04:12 22.3 182.9 41.7 44.7 09/06/02 13:04:22 22.3 186.0 42.7 45,1 09/06/02 13:04:32 22.5 188.6 43.8 45.4 09/06/02 13:04:42 22.3 190.6 44.7 45.6 09/06/02 13:04:52 22.2 192.4 45.5 45.8 09/06/02 13:05:02 22.2 193,3 46.0 46.0 09/06/02 13:05:12 22.2 194.0 46.7 46.1 09/06/02 13:05:22 22.2 194.7 47.2 46.3 09/06/02 13:05:32 22.2 195.6 47.6 46.4 09/06/02 13:05:42 22.2 196.3 47.9 46.5 09/06/02 13:05;52 22.3 197.1 48.3 46.5 09/06/02 13:06:02 22.4 197.6 48.7 46.7 09/06/02 13:06:12 22.4 198.2 48.9 46.8 09/06/02 13:06:22 22.3 198.6 49.1 46.8 09/06/02 13:06:32 22.2 198.9 49.2 46.9 09/06/02 13:06:42 22.3 199.3 49.2 47.0 09/06/02 13:06:52 22.2 199.7 49.3 47.0 09/06/02 13:07:02 22.3 200.1 49.5 47.2 09/06/02 13:07:12 22,4 200.2 49.6 47.2 09/06/02 13:07:22 22,5 200.6 49.7 47.2 09/06/02 13:07:32 22.3 200.8 49•9 47.3 09/06/02 13:07:42 22.2 201.2 49.9 47.3 09/06/02 13:07:52 22.2 201,3 49.9 47.4 .09/06/02 13:08:02 22,1 201.8 50.0 47.4 09/06/02 13:08•12 22.1 201.7 50.1 47.4 09/06/02 13:08:22 22.3 201.8 50.2 47.4 09/06/02 13:08:32 22.1 202.0 50.3 47.4 

Page 5 
9/6/02 Run #3 

09/06/02 13:08:42 

09/06/02 13:08:52 

09106/02 13:09:02 

09/06/02 13!09:12 

09/06/02 13:09:22 

09/06/02 13:09:32 

09/06/02 13:09:42 

09/06/02 13:09:52 

09/06/02 13:10:02 

09/06/02 13:10:12 

09/06/02 13:10:22 

09/06/02 13:10:32 

Stop Run #3 

09/06/02 13:10:42 

09/06/02 13:10:52 

09/06/02 13:11:02 

09/06/02 13:11:12 

09/06/02 13:11:22 

09/06/02 13:11:32 

09/06/02 13:11:42 

09/06/02 13:11:52 

09/06/02 13:12:02 

09/06/02 13:12:12 

09/06/02 13:12:22 

09/06/02 13:12:32 

09/06/02 13:12:42 

09/06/02 13:12:52 

09/0,6/02 13:13:02 

09/06/02 13:13:12 

09/06/02 13:13:22 

09/06/02 13:13:32 

09/06/02 13:13: 42 

09/06/02 13:13:52 

09/06/02 13:14:02 

09106/02 13:14:12 

09/06/02 13:14:22 

09/06/02 13:14:32 

09/06/02 13:14:42 

09/06/02 13:14:52 

09/06/02 13:15:02 

09/06/02 13:15:12 

09/06/02 13:15:22 

09/06/02 13:15:32 

09/06/02 13:15:42 

09/06/02 13:15:52 

09/06/02 13:16:02 

09/06/02 13:16:12 

09/06/02 13:16:22 

09106/02 13:16:32 

09/06/02 13:16:42 

09/06/02 13:16:52 

09/06102 13:17:02 

09/06102 13:17:12 

09/06/02 13:17:22 

09106/02 13:17:32 

09/06/02 13:17:42 

09/06/02 13:17:52 

09/06/02 13:18:02 

09/06/02 13:18:12 

09/06/02 13:18:22 

09106102 13:18:32 

09/06/02 13:18:42 

09/06/02 13:18:52 

09/06/02 13:19:02 

09/06/02 13:19:12 

09106/02 13:19:22 

09/06/02 13:19:32 

09/06102 13:19:42 

09/06/02 13:19:52 

09/06/02 13:20:02 

09/06/02 13:20:12 

22.0 

22.0 

21.9 

22.0 

21.9 

21.8 

22.0 

21.9 

21.8 

21.8 

21.7 

21.7 

19.14 

17.1 

5.4 

5.2 

4.6 

3,8 

2.9 

2.4 

2,3 

2.1 

2.0 

2.0 

1.9 

1.8 

1.7 

1.7 

1.7 

1.6 

1.6 

1,6 

1.6 

1.5 

1.5 

1.5 

1.5 

1,5 

1.5 

1.5 

1.4 

1.4 

1.4 

1.4 

1.4 

;4 

1.4 

1.4 

1.4 

1.4 

1,4 

1.4 

1.4 

1.4 

1.4 

1.4 

1.4 

1.5 

3,5 

4.0 

4.0 

3.0 

1,5 

1.5 

1.5 

1.4 

1.4 

1.4 

1.4 

1.4 

1.4 

202.2 

202.5 

202.8 

203.0 

203.1 

203,3 

203.6 

203.7 

203.7 

204.0 

204.1 

204.1 

191.26 

204.0 

202.3 

202,4 

203.6 

202.8 

195.0 

174.6 

144.8 

118.5 

98.2 

82.4 

69.4 

58.0 

49.2 

40.7 

34.2 

28.2 

22.9 

18.9 

16.5 

14.0 

12.2 

10,9 

9.9 

9.2 

8,6 

8.1 

7.7 

7.5 

7.4 

7.3 

7.0 

6.9 

6.6 

6.4 

5.8 

5.6 

5.3 

5.2 

5.2 

5.1 

5.2 

5.2 

5.2 

5.1 

5.0 

4.8 

4.8 

4.5 

4.6 

5.0 

5.9 

7.4 

8.3 

8.1 

7.1 

6.5 

5.8 

50.4 

50.5 

50.5 

50.6 

50.6 

50.6 

50.7 

50.7 

50.8 

50.8 

50.9 

50.9 

49.18 

50.9 

50.7 

50.4 

50.2 

50.4 

50.4 

49.3 

47.3 

45.9 

46.2 

48.0 

50.1 

52.6 

55.1 

57.4 

59.8 

62.2 

64.3 

66.4 

68.2 

70.0 

71.5 

72.9 

74.1 

75.2 

76.2 

77:1 

77.7 

78.3 

79.0 

79.5 

79.9 

80.3 

80.5 

80.9 

81.0 

81.1 

81,1 

81,4 

81.6 

82.7 

83.8 

84.8 

85.0 

85,1 

85.6 

86.3 

86.3 

86.5 

86.9 

84.7 

80.1 

76.0 

69.2 

61.0 

53,9 

47.6 

42.0 

47.4 

47.5 

47.5 

47.5 

47.6 

47.6 

47.6 

47.7 

47.7 

47.7 

47.8 

47.8 

46,80 

47,7 

47,3 

47.1 

47.4 

46.9 

43.3 

36.5 

29.2 

23.7 

19.7 

16.4 

13.8 

11.6 

9.7 

8.2 

6,8 

5.6 

4.8 

4.0 

3.5 

3.1 

2.8 

2,5 

2.4 

2.1 

2.0 

1.9 

1.8 

1.7 

1.7 

1.7 

1.6 

1.6 

1.5 

1.5 

1.5 

1.5 

1.4 

1.4 

1.4 

1.4 

1.3 

1.3 

1.3 

1.3 

1.3 

1.2 

1.2 

1.2 

1.3 

1.4 

1.6 

2.7 

5.9 

9.0 

11.7 

14.0 

15.9 

91 ppm S02 

Page 6 
916/02 Run #3 

09/06/02 13:20:22 

09/06/02 13:20:32 

09/06/02 13:20:42 

09/06/02 13:20:52 

09/06/02 13:21:02 

09/06/02 13:21:12 

09/06/02 13:21:22 

09/06/02 13:21:32 

09/06/02 13:21:42 

09/06/02 13:21:52 

09/06/02 13:22:02 

09/06/02 I3:22:12 

09/06/02 13:22:22 

09/06/02 13:22:32 

09/06/02 13:22:42 

09/06/02 13:22:52 

09/06/02 13:23:02 

09/06/02 13:23:12 

09/06/02 13:23:22 

09/06/02 13:23:32 

09/06/02 13:23:42 

09/06/02 13:23:52 

09/06/02 13:24:02 

09/06/02 13:24:12 

09/06/02 13:24:22 

09/06/02 13:24:32 

09/06/02 13:24:42 

09/06/02 13:24:52 

09/06/02 13:25:02 

09/06/02 13:25:12 

09/06/02 13:25:22 

09/06/02 13:25:32 

09/06/02 13:25:42 

09/06/02 13:25:52 

09/06/02 13:26:02 

09/06/02 13:26:12 

09/06/02 13:26:22 

09/06/02 13:26:32 

09/06/02 13:26:42 

09/06/02 13:26:52 

09/06/02 13:27:02 

09/06/02 13:27:12 

09/06/02 13:27:22 

09/06/02 13:27:32 

09/06/02 13:27:42 

09/06/02 13:27:52 

09/06/02 13:28:02 

09/06/02 13:28:12 

09/06/02 13:28:22 

09/06/02 13:28:32 

09/06/02 13:28:42 

09/06/02 13:28:52 

09/06/02 13:29:02 

09/06/02 13:29:12 

09/06/02 13:29:22 

09/06/02 13:29:32 

09/06/02 13:29:42 

1.4 

1,4 

1.4 

1.4 

1,4 

1,4 

1.4 

1.4 

1.4 

1.4 

1.4 

1,4 

1.4 

1.3 

1.3 

1.3 

1,3 

1,3 

1,3 

1.6 

1.5 

1.4 

1.3 

1.3 

1.3 

1.3 

1.3 

1.4 

1,4 

1,3 

1.3 

1.3 

1.3 

1.3 

1,3 

1.3 

1.3 

1.3 

1,4 

1.4 

1.4 

1.4 

1.3 

1.3 

1.3 

1.3 

1.4 

9.5 

15.6 

1513 

15.3 

15.4 

15.4 

15.4 

13.3 

4.3 

4.2 

5.5 

5.0 

4.8 

4.5 

4.0 

3.9 

3.6 

3.4 

3,2 

2.8 

2.7 

2,6 

2.3 

2.5 

2.3 

2.2 

2,3 

2.0 

1.9 

1.7 

1.6 

1.6 

1.4 

2,6 

7.9 

17.7 

30.1 

42.2 

53.0 

61.7 

69.1 

74.0 

78.5 

82.0 

84.3 

86.2 

87,4 

88.2 

88.8 

89,1 

89.8 

90.2 

90.2 

90:5 

90.7 

90.7 

91,4 

91.5 

9i.7 

91.8 

91.5 

89.8 

87.9 

83,4 

75.1 

66.5 

56.0 

37.1 

32.9 

29.t 

25.6 

22.5 

19.8 

17.3 

15,0 

13,2 

11.3 

10.0 

8.6 

7,4 

6.6 

5,6 

4.6 

3.9 

3.3 

2.8 

2.2 

1.7 

1,3 

0.9 

0.7 

0.5 

0.3 

0.1 

0.0 

-0.1 

-0.4 

-0.6 

-0,7 

-1.1 

-0.8 

-0.3 

-0.5 

-0.7 

-0.8 

-0,5 

-0,2 

-0.3 

-0.4 

-0.4 

-0.5 

-0.6 

-0.6 

-0.6 

-0.7 

-0.8 

-0.8 

-0,8 

-0.7 

-0.6 

-0.4 

-0.1 

0.0 

17.3 

18.6 

19.5 

20.z. 

20,9 

21.3 

21.7 

21,9 

22.1 

22.4 

22.4. 

22.6 

22.6 

22.7 

22.7 

22,8 

22.7 

22.8 

22.8 

22.7 

22.8 

22.8 

22.8 

21,9 

19.5 

16.4 

13.3 

10.7 

8.5 

6.7 

5.4 

4.3 

3.5 

3.0 

2.5 

2.1 

1.8 

1.7 

1,5 

1.4 

1.4 

1,3 

1.2 

1.2 

1.2 

1,1 

1.0 

1,0 

1.0 

1.0 

1.0 

1.1 

1.2 

1,3 

1.5 

1.6 

1.7 

25.1 DDm NOx 

Zero VOC 

99.4 ppm CO 

Zero SO2. NOx 

14.7 uDm C3H8 

Page 7 
Appendix C 
FILTER ANALITICAL DATA 

Company: Acme Brick, Tulsa, OK 

Date: 9/6/02 

Location: Turnel Kiln Exhaust 

Run 1 Run 2 

Filter ID Number i•i i/i,i •_• 

Date of Weighing .:•i i§•!ii•]•i iiiiiiii•i• •i 

Gross Filter Wt. •i:•:::!,.8.i!• • 

Run 3 

Date or Weighing 

Gross Filter Wt. 

0.4053 0.4044 Ave. Gross Filter Wt. 0.4071 

Date of Weighing 

Filter Tare Wt. ii•)!•3i9•92 

Date of Weighing 

Filter Tare Wt 

Ave. Filter Tare Wt. 

Wt. of PM on Filter (grams) 

0.4008 

0.0036 

3.6 

0.3993 

0.0061 

6.1 Total Weight of Particulate (mg) 

0.3993 

0.0078 

7.8 

43 
PARTICULATE ANALYTICAL DATA FORM 

Company: Acme Brick, Tulsa, OK 

Date: 9/6/02 

Location: Tunnel Kiln Exhaust 

Run 

Density (Pa) 

0.0001 

Blank Concentration (Ca) 

Rinse Volume (Yaw) 

Residue in Rinse (Wa) Ca*Vaw×-Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Run 2 

0.0001 

Run 3 

0.0001 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

109.9376 

0.0001 

109.9049 

32.62 

117.504] 

0.0001 

117.4792 

24.71 Weight of Particulate in Rinse (mg) 

103.2974 

0.0001 

103.2731 

24.15 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 101.77695 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 101.7767 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) g/g 

0.0002 

1.274E.06 

•lote: In no case should a blank residue greater than 0.01 mg/g or 0.001•o of the blank 

weight be subtracted from the sample weight. 
PARTICULATE ANALYTICAL DATA FORM 

Company: Acme Brick, Tulsa, OK 

_Date: 9/6/02 

Location: Tunnel Kiln Exhaust 

Run 1 

Density (Pa) ::iii!!::iiiiiiiiii ::i:: 

Run 2 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Aliqout Volume 

Residue in Rinse (Wa) Ca*Vaw*Pa 0.0003 0.0003 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

Total Weight of Particulate (rag) 

127.3560 

0.0003 

127.3467 

9.02 

126.0134 

0.0003 

126.0042 

8.92 

Run 3 

0.0003 

130.2283 

0.0003 

130,2180 

10.02 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 129.76455 

129.76435 

0,0002 

8E.07 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va-'Pa) g/g 

Jote: In no case should a blank residue greater than 0,01 mg/g or 0.001% of the blank 

weight be subtracted from the sample weight. 
PARTICULATE ANALYTICAL DATA FORM 

Company: Acme Brick. Tulsa OK 

Date: 9/6/02 

Location: Tunnel Kiln Exhaust 

Run Rum 2 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Yaw) 

Residue in Rinse (Wa) Ca*Vaw*Pa 

Run 3 

0.0000 

Gross Weight •:::•i!i•5•:J9•8• ::::iiii ::::199i9•8B •::::::::ii•t#•i•i•i 

Date of Weighing 

Time 

Gross Weight :::: :::::: :7: "iii:: i•:• •89 

:::::::::::::::::::::::::::: 

lO6.6474 

0.0000 

106.6467 

0.70 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

105.9686 99.9089 

0.0001 0.0000 

105.9673 99.9080 

],24 0.85 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 107.69435 

107.6942 

0.00015 

4.412•.07 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) g/g 

Note: In no case should a blank residue greater than 001 •ng/g or 0,001% of the blank 

weight be subtracted from the sample weight. 

46 
Sheet1 

Summary of HF and HCI Analysis 

Plant: Acme Brick, Tulsa, OK 

Location: Tunnel Kiln Exhaust 

Date: 9/6/02 

Run # Imp # Volume 

350 

350 

Dilution 

2O 

2O 

FI-, ug/ml 

25.87 

25.42 

Average 

2 350 20 23 56 

2 350 20 23.32 

Average 

3 350 20 24.64 

3 350 20 24.97 

Average 

2&3 250 

2&3 250 

23.87 

24.54 

Average 

2 2 & 3 250 23.93 

2 2 & 3 250 24.36 

Average 

3 2 & 3 250 

3 2 & 3 250 

22.04 

22.36 

Average 

Totals 

Run #1 

Run #2 

Run #3 

HF, mg 

190.6878 

187.3708 

189.0293 

173.6608 

171.8917 

172 7762 

181.6214 

184.0539 

182.8377 

6.283778 

6.460155 

6.371966 

6.299573 

6.41277 

6.356171 

5.80203 

5.88627 

5.84415 

195.4013 

179.1324 

188.6818 

Clo, ug/ml 

6.94 

6.61 

4 

4.25 

6.59 

5.99 

5.3 

5.62 

4.39 

4.25 

4.82 

4.58 

HCI, mg 

49 94024 

47.56556 

48.7529 

30.51404 

30.583 

30.54702 

47.42164 

43.10404 

45.26284 

1.3621 

1.44434 

1.40322 

1.12823 

1.09225 

1.11024 

1.23874 

1.17706 

1.2079 

50.15612 

31.65726 

46.47074 

Page 
Conditions 

5 ug/ml CIDate 09/07/2002 

Time 

Compollent 

-102.400mV 1024.000mV 

Retention 

•ll 

1.1oo t•::::ii ,450 376.25 

255.50 

External 

4.21 

3 
Conditions : 4.£2 u nl 

Date 0£/07/2002 

Time 08:25:07 

Component 

Ct- 

-102.400mV 

Retention 

1,450 

51 

,/ 

i024.000mV 

380,40 

257.75 

External 

4.94 

5,01 

J•-, 49 
Conditions 

DaLe 09/07/2002 

Time 08:32:14 

FIColilpo r•eIIT• 

-102 o400mV 1024.000mV 

Retent io,,1 

1,100 

1.450 ::::::::::::::::::::::::::: 

5 

•rea 

725.95 

502.85 

External 

8.70 

8,13 
Component 

Conditions 9.84 u nl F1- 

lO,ug/m• C1- 

Date 09/07/2002 

Time 08:34:41 

-102 .#-OOm•J 1024 oO00mV Retention 

763.80 

548.70 

External 

10.03 

10,31 
Conditions 24•6 u •I FI25 ug/n• CIDate 09/07/2002 

Time 08:41:49 

FIComponent 

-•.02.400mV 1024.000mV 

Retention 

I.II• 

1.550 

2 

I942,20 

1460,70 

External 

25,9i 

27.37 
Conditions 24.6 c mL FL25 u9/•1 C1- 

Date 09707/2002 

Time 08=44:16 

--202.400mV 

Retention 102•. O00mv 

1.116 

1.550 

2 

31 

External 

24.86 

25,03 

53 
Conditions 49.2 u •1 F1- 

Date 09/02"/2002 

Time 09:01•20 

FI• 

CI- 

-202 •400mV 1024.000mV Reten[£on 

.150[ 

.533 

2 

3798.03 

3376.9,9 

46.83 

55,67 
Conditions 

Date 09/07/2002 

T•e O9:O3:55 

-•., 02 400mV 

Component -Retention (unknown) 

•L024 O00mV 

o.133/. ..: .............................................................................................................................................................................................................................................................. 

1.516{ 

:.1 

152.20 

3774.90 

3301,65 

48.89 

49,02 

$5 
Calibration file F .cal 

AMOUNT INJECTED 

AREA -0.000 49.200 

0.000,., 

.... 

460 

" 

3786 r. ::::,I 

1 

2 

3 

5 

Avg slome of curve: 77.01 

Y-axis intercept: 0_00 

Coeff of J. in regr" 0.93 

No. Area Amount CF 

O: 0.000 0.000 0.000 

1: 378.325 4.920 '76.895 

2: 744.875 9.840 75.699 

3• 1963.250 24.600 79.807 

4: 3786•465 49.200 76.961 
Calibratio• file 

AMOUNT INJECTED 

AREA 

0..000::::"....,.:.,,...,,.,....,.... 0o000 50•000 

3339H32o 

1 

2 

3 

5 

Avg slope of curve: 60.66 

Y-axis •ntercept: 0•00 

Coeff• 0"• fin •egT• 0.81 

No. Area Amount CF 

O= 0.000 O.O00 0•000 

l: 256.625 5.000 51.325 

2: 525.775 lO.O00 52.578 

3: I461-800 25.000 58.472 

4• 3339.320 50_000 66.786 

57 
Conditions Acme 8• ;k, Tulsa, OK 

Run #i Imp #i 

Volume 350 mls Dilution 1/20 

bale 09/07/2002 

Time 09:1•,:18 

ClComponent 

:i, 02, 400m•Y • 02•¢ O00mV 

Retent,•.on 

1.550[ 

2057.05 

361,32 

ExteFn•1 

25.87 

6.94 

58 
Condi£ions Aome B ;1<, Tulsa, OK 

Run #1-•mp #1 

:Voiume 350 mls Dilution 1/20 

Date '09/07/2002 

Time 09:13=39 

Component 

-102.4OOrnV iO24.000mV Retent•0n 

1.550 

A•ea 

2024.08 

343,52 

External 

59 
Conditions Acme B. ok, Tulsa, OK 

Run #2•mp #I. 

Volume 350 mls Dilution L/20 

Date 09/07/2002 

Time 09:20;35 

ClComponent 

--102.400mV t024 .O00mV 

Retention 

133 ;,,...I ................................................................................. 

.5.•,01 

1877.00 

217.50 

External 

6O 
Conditions Acme B ck• Tulsa, OK 

Run #2-Imp #$ 

Volume 350 mis Dilution 1/20 

Date 09/07/2002 

Time 09:30:27 

Component 

C1- 

-i02.400m.V 1024.000mV •etent[0n 

1500 '•' i857,60 

217.95 

23.32 

4.25 
Conditions Acme 5 ok, Tulsa, OK 

Run #3•imp #1 

Volume 350 mls Dilution 1/20 

Date 09/07/2002 

Time 09133:24 

FIelCo mDol]ell[, 

-•1,02.400mV 1024 oO00mV Retenti0• 

i. 15C 

,, 

1.550 ......... 

1966.30 

342.40 

Ex.ternal 

24 

6 
Conditions Acme B •k, Tulsa, OK 

Run #3 Imp #1 

Volume 350 mls Dilutiol• 1/20 

Date 09/07/2002 

Time 09:35=55 

,Coraponent 

FICI- 

-102.400mV 

Retention 

1.550 

1024.000rnV 

qrea 

1990.80 

309.80 

External 

63 

Conditions Acme B ok, Tulsa, OK 

: Run #l•[mp #2 & #3 

Volume 250 mls Dilution 1/1 

Date 09/07/2002 

Time 09:39:I8 

Component 

.15, 

.55• 

-102.400mV 102• ,O00mV Retentlor. 

ATea 

1902.67 

272.51 

ExteFna1 

23.87 

5,30 
ClRun #l Imp #2 & #3 

Volume 250, mls DilutiO• $/$ 

Date : 09/07/2002 

Time 09:41:32 

Component 

-102.400mV 

Retent•o LO24.000m•/ 

Area 

1957,95 M 

290,07 M 

External 

65 
Condition• Acme B ol(, Tul•a, OK 

Run #2•2mp #2 & #3 

Volume 250 mls Dilution i/i 

Date 09/07/2002 

Time 09=48:10 

Compo#ent 

-i02 •400mV •i024,000mV Retentio Area 

1907.55 

225,20 

External 

23.93 

4,39 
ConditioT•s Acme B ck.• Tulsa, OK 

Run #2 Imp #2 & #3 

Volume 2SO mls Dilution I/I 

Date 09/07/2002 

Time 09:50:39 

ClConIponent 

-102.400mV 1024.000mV Retenti01• 

1943,10 

217.90 

External 
Conditions Acme B ok, Tulsa• OK 

Run #3•mp #2 & #3 

Volume 250 mls Dilution 1/1 

Date 09/07/2002 

Time 09:57:20 

Component 

01- 

-102.400mV .1. 024 •O00mV Retenti0..q 

11 

1.566: 

External 

68 
Coaditions Acme B_.ck, Tulsa, OK 

Rub #3 Imp #2 & #3 

Volume 250 mls Dilution 

Date : 09/07/2002 

Time 09:59:35 

Component 

FIC1 

--102 •4OOmV $024.000mV Retention 

2:2211121',227,',:',:2',IIC',:;::::::::, 

1.550 

3 

,•fea 

1778.54 

234.88 

External 

69 
Conditions Acme. B ok,, Tulsa, OK 

= H2OBI•I( 

Date 09/07/2002 

Time 

Component 

102,,400mV i024.000n]V 

Retention Alea External 

7O 
= H2S04 Blank 

Date 09/07/2002 

Time i0:08:29 

-102.400ram 1024,0OOrnV Retention External 
Conditions Acme E ok, Tulsa, OK 

24.6. u•?ml F1 

2S ug/ml C1 

Da£e 09/07/2002 

T•me 10:10:58 

Component 

72 
Appendix D 
_-2 

LOCATION (SOURCE 

OPE•TOR: &• 

•TER BOX #:/• 

P•-T•ST LE• CIECK 

FIELD DATA 

r/WPINGERS 

Initial Final 

#4• 

TT, 

POST-TEST LEAK CHECK 

Meter: o,co cu.ft, in. HG 

Pitots." •-- •20 
FIELD DATA 

IMPYNGERS 

Initial 

#1 /z ,• 

#5 2 • 

co• 
FIELD DATA 

C02 

Final 

li • 

02 

POST-TEST LEAK CHECK 

Meter: o. o cu.ft HG 

Pit0ts: • H20 

6/0. Oo 0 

7•,, • 
Appendix E 
0 

UJ 

• •dd 

6dddo 

©© 

g•odddd 
Meter Box #: 10 

Date: 8/12/02 

Calibrated By: RT 

Emtech Thermo 

Degrees F Checker Probe Stack Oven Exit Auxiliary 

Point 32 31 31 31 30 31 

Point 2 212 211 211 210 211 210 

Point 3 752 750 751 750 750 750 

Degrees R 

Poinl 

Point 2 

Point 3 

Percent Difference 

Point 

Point 2 

Point 3 

Emtech Thermo 

Checker Probe Stack Oven Exit Auxilla• 

492 491 491 491 490 491 

672 671 671 670 671 670 

1212 1210 1211 1210 1210 1210 

Probe 

0.203252 

0.14881 

0.165017 

Stack 

0.203252 

0,14881 

0.082508 

Oven 

0.203252 

0.297619 

0.165017 

Exit 

0.406504 

0.14881 

0.165017 

Auxilta• 

0.203252 

0.297619 

O.165017 

?7 
78 
Appendix F 
Date: 

CERTiFiCATE of ANALYSTS 

Interference-Free Multi-Component EPA Protocol Gases 

Cy Document Number: 

1900psig 10368234 

Expiration Date: Item Number: klitric Oxide 25 ppm 24.6 =L-0.5 ppm 05/14/02 05/13/04 

Custorner: P.O. Number: Notes: 

Environmental Total NOX "Mixture is valid psig 25.1 ppm 

Nitrogen Balance Balance 

cal uncertainty andNIST 

traceability are ih compliance with 

EPA-600/R-97/123 

GMIS 175 GMIS 175 54.9 ppm 0.7 NO N2 CC122371 04/21103 N.A. 

Manufacturer: KVB/An.alect Manufacturer: 

Model Number: Manufacturer: EN3024 Model Number: Model Number: r: 3024 Number: 

Principle: Serial Number: FTIR Principle: VIPC Calibrated: 04/09/02 & 05/09/02 MPC Calibrated: p•e: 

Air •.iquide America Corporation 

11426 Fairmont Parkway, La Porte, Texas 77571-6000 

Phone: (281) 474-8400 Fax: (281) 474-8419 

?9 
--II•yl. Number: Cyl, Pressure:, 

II.q ;C49028 1900psig I•'•.ssay Date: ' Expiration Date: 

1105/14/02 05/13/04 

IICustomer: P,O. Number Notes: 

ILArmstrong Environ mental 

/r*'Mixture is valid onl' 50 psig 

CERTIFICATE. of ANALYSIS 

Interference-Free Multi-Component EPA Protocol Gases 

Document Number: 

10368234 

item Number: 

.e. r•i.n.ty 

traceability a•e in compliance with 

EPA-600/R-97/123 

GMIS1,,75 GMIS175 54.9 ppm 0.7 NO N2 cci22371 04121/03 N.A, 

........................................................................................................................... ,.,.., 

Manufacturer: KVB/Analect Manufacturer: 

Model Number: r: 

EN3024 Number: Model Number: Serial Number: 3024 Serial Number: 

Principle: r: 

FTIR pie: MPC Calibrated: Principle: 

• 

04/09/02 & 05/09/02 MPC Calibrate•: MPC Calibrated: 

ComBonent 

Nitric Oxide 

Analys 

/ 

Air Liquide America Corporation 

11426 Fairmont Parkway, La Porte. Texas 77571-6000 

Phone: (281)474-8400 Fax: (281; 474-8419 

8O 
CERTIFICATE of ANALYSIS 

Interference-Free Multi-Component EPA Protocol Gases 

--•Cyl. Number: 

CC122083 

Assay Date: 

07/31/01. 

Expiration Date: Item Number: Carbon Monoxide 100 ppm 99.4 •1.7 • 

07/30104 

P.O. Number: Notes: 

Nitrogen Balance Balance 

Customer: 

Armstrong 

"Mixture is valid only to 150 psig 

NOTE: Analytical uncertainty and NIST 

lraceability are in compliance with 

EPA-600/R-97/123 

Manufacturer: KVB/Analect JlManufacturet= IIManufacturer: Modal •umber: EN3024 I/Mo"el Number: /IModel Number: 

Serial Number: 3024 J•Serial Number: Serial Number: 

Analytical Princiole: FTIR J•Analytical Princ[• J•Analytical Principle: •MPC Calibrated: 07/05/01 I•MPC Calibrated: •MPC Calibrated: 

110.25 110.23 110.74 •ili• Cornponent 

107.98 107,49 108.17 Carbon Monoxide 

99.57 99.11 99.74 

Air Liquide America Corporation 

11426 Fairmont Parkway, .a Porte, Texas 77571-6000 

Phone: (281) 474-8400 Fax: (281) 474-8419 
LiQUiDE 

TM 

CERTiFiCATE of ANALYSIS 

Interference-Free Multi-Component EPA Protocol Gases 

Cyl. Pressure:* Document Number: 

1900psig 9225974 

Expiration Date: Item Number: Carbon Monoxide08/23/04 

Cyl, Number: 

I[CC36022 IXse.y D,te: 

I08/24101 

--IOustomer: P.O. Number: 

I[Armstrong 

I*Mixtu•e is valid only to 150 psig 

Notes: 

200 ppm I99 +3 ppm 

Balance Balance 

NOTE: Analytical uncertainty and NIST 

traceability are in compliance with 

E PA-600/R-97/123 

GMIS113 GMIS113 248.0 ppm 2.0 CO N2 CC64210 12/14/02 N.A. 

|JManufacturer. KVB/Ana)ect /Manufacturer" IMa |]Model Number: EN3024 IModel Number: IMoi•aNC[uUmr•r•r iSerial Number: 3024 ISerial Number: IJSerial Number __Analytical, Principle: FTIR IAnalytical Principle: IIAnalytical I•IPC Principle" Calibrated: 08/06/01 •PC Calibrated: IIMPc Calibrated" 

266.07 266.60 267.38 • Component 

213.80 212.79 213 54 Carbon Monoxide 

Analyst: 

Air Liquide America Corporation 

426 Fairmont Parkway, La Porte Texas 77571-6000 

Phone: (281) 474-8400 Fax: (281) 474-8419 
.--iiCYl. Number: Cyl. Pressure:* 

•C,15056 1900psig, 

Assay Date: Expiration Date: 

01/29/01 01/29/03 

•mstrong Customer: P,O. Number: 

II*Mixture is valid only to 150 psig 

CERTIFICATE of ANALYS S 

Interference-Free Multi-Component EPA Protocol Gases 

Document Number: 

7628314 

Item Number: 

Notes: 

Nitrogen Balance 

50 ppm 52.2 ±0.8 ppm 

Balance 

NOTE: Analytical uncertainty an• NIST 

•pliance with 

E PA-600/R-97/123 

GMIS116 GMIS116 50.3 ppm 0.7 SO2 N2 CC68565 01/27/02 N.A. 

KVB/Analect 

Model Number: EN3024 

}erial Number: 3024. 

•,nalytical Princl ole: FTIR 

JIM PC Calibrated: 01/11/01 

Manufacturer: Manufacturer: 

Model Number: Model Number: 

Serial Number: Seriai Number: 

Principle: Analytical Principle: 

MPC Calibrated: MPC Calibrated: 

50.47 50.59 50.27 Component 

Sulfur Dioxide 

0.05 0 12 0.27 

50.08 50.38 50.23 

51.96 51.96 52.31 

Air Liquide America Corporation 

1429 Fairmont Parkway, La Porte, Texas 77571-6000 

Phone: (281) 474-8400 Fax: (281) 474-8419 
LJQUIDE 

TM 

CERTIFICATE of ANALYSIS 

'Mixture is valid only to 150 psig len Balance Balance 

NOTE: Analytical uncertainty and NIST 

raceabJlity are in compliance with 

'PA-600/R-97/123 

GMIS 116 GMIS 116 50.3 ppm 0,7 SO2 N2 CC68565 01/27/02 

.................................................................................................. • ,__. 

Manufacturer; KVB/Analect 

Manufacturer: Model Number: EN3024 Model Number: 

erial Model Number: Number: 3024 Serial Number: 

Principle: Serial Number: FTIR Z•nalytlcal Principle: MPC Calibrated: Analytical Princip]e: O1/11/O" k4PC Calibratea. MPC Calibrated: 

Analyst: 

/ 

Air Liquide America CorBoration 

11426 Fairmom Parkway, La Porte. Texas 77571-6000 

Phone: (281; 474-8400 =a×' (281) 474-8419 
Ctyl. Number: 

3C20147 

Date: 

Customer: 

CERTIFICATE of ANALYSIS 

Interference-Free Multi-Component EPA Protocol Gases 

Cyl. Pressure:* Document Number: 

1900psig 9062262 

08/06104 

Expiration Date: Item Number: Propane 50 ppm 

P.O. Number: Notes: 

*Mixture is valid 

BalanCe Balance 

NOTE: Analytical uncertainty and NIST 

traceability are in compliance with 

EPA-600/R-97/123 

SRM14 1666b 9.69 ppm 0',1 C3H8 Air CLM-O05016 04/18/07 84-31-G 

•erial Number: 

pie: 

Caibrated: 

HP Manufacturer: 

6890 Number: Number: 8295 Serial Number: Serial Number: GO.FIB Analytical Principle: Principle: 08/01/01 MPO Calibrated: MPC Calibrated: 

Air Liquide America Corporation 

11426 Fairmont Parkway, La Porte, Texas 77571-6000 

Phone: (281) 474-8400 Fax: (28I) 474-8419 £5 
-•[• AiR LIGUIDE• 

Cyl. Number: 

Ilcc114931 

/IAssay •ate: 

/105/i 3/02 

IIcustomer; 

•--JlArmstrong Envionmental 

CERTIFICATE of ANALYSIS 

Interference-Free Multi-C0mponent EPA Protocol Gases 

Notes: 

IIAir 

Cyi. Pressure:* 

1900psig 

Expiration Date: 

05/12/05 

P.O. Number: 

traceability are in Compliance with 

EPA-600/R-97/123 

Balance Balance 

SRM64 1668b 98.8 ppm 0.5 C3H8 Air CAL-010986 11/21/02 82-1-04 

........................................................................................................................................... 

Vlanufacturer: HP 

Model Number: 6890 

Serial Number: 8295 

Analytical Principle: GC-FID 

MPC Calibrated: 05/13/02 

Manufacturer: Manufacturer: 

Model Number: Model Number: 

Serial Number: Serial Number: 

pie: pie: MPC Calibrated: MPC Calibrated: 

27.41 27.34 27.28 

Component 

Propane 

Air Liquide America Corporation 

11426 Fairmont Parkway, La Porte, Texas 77571-6000 

Phdne: (281) 474-8400 Fax: (281) 474-8419 

•6 
- AIR LiQUiDE 

-TM 

CERTIFICATE of ANALYSIS 

Interference-Free Multi-Component EPA Protocol Gases 

Number: Cy!. Pressure:* Document Number: 

lC•90523 1900psi• •0622•2 

IAssay Date: Expiration Date: item Number: 

!08/07/01 08/06/04 

"--I•Customer: P.O. Number: Notes: 

IIArmstrong 

JlAir "*Mixture is valid only to 150 psig 

'traceability are in compliance with 

;EPA-600/R-97/'123 

Balance Balance 

SRM14 1666b 9.6• I• 6"i• ••1•"• •i• •' [• :••••:•"::':';:::••:•:•)•'• 

]lMan•,fneturer: HP IIM"nu•acturer: I]• •,••t;•i'd ;'#;; 

Serial Number: 8295 •JSeria] Number: JJSerial Number: 

__Analytical ]IMPC Principle: GC.FIB IIAnelylical Principle: •Analytical Principle: "Calibrated: 08/01/01 IIMPc Calibrated: IIMPC Calibrated: 

Component 

Propane 

Air Liquide America Corporation 

I426 Fairmont Parkway, La Porte, Texas 77571-6000 

Phone: (281) 474-8400 Fax: (281) 474-8419