1884 PMNX130122167661810 TTRRPP

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Page 2 SANITIZED SUBMISSIONMarta Martinez Vice-President Tire Recycling & Processing LLC 1309 Industrial Way Harlingen TX 78550 rborrel@borrelengineering.com

Rene Borrel Subordinate TRP 406 North Monroe Street Marksville LA 71351 rborrel@borrelengineering.com 318-253-0196



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Proposed name: Crude Tire Oil Definition: The volatile organic liquid extracted from the gas evolved from pyrolysis of waste tires at a decomposition temperature of 500c .



### X 330182 CAS Inventory Search.pdf Pyrolysis Tire oil is no single chemical within the mixture. Pyrolysis tire oil contains a large variety of organic compounds.
See Attachment 013 (Limonene.doc)

Limonene.doc
Page 4 SANITIZED SUBMISSIONSee attachment ID 005

Waste tires will be shredded with metal and fibers being removed, leaving crumb rubber. Crumb rubber will be put in reactor where they will undergo pyrolysis.The thermal converter technology depolymerizes the waste tire crumb rubber in an oxygen free, externally heated reaction vessel in a temperature controlled environment. Oxidation or "burning"does not occur because the process maintains an oxygen free environment. The tire components are converted to molecular gas and oil by indirect high temperature heating, and then condensing the oil for commercial use. Complete control of the time (12-15 hours), temperature (up to 500c), and pressure (up to 7.5 psi) for the batch process ensures product decomposition. This process seperates tire condensate from char material left at the end of process.

Bulk of composition consist of C2 - C 15 olefins and aromatics Chemical Assignment TSCA.xls

Page 5 SANITIZED SUBMISSIONPage 6 SANITIZED SUBMISSIONPage 7 SANITIZED SUBMISSIONTire oil, Pyro Oil, Pyrolysis Tire Oil, Tire Derived Oil

Yamels Oil Water 7732-18-5 3 Carbon Black 7440-44-0 2

Page 8 SANITIZED SUBMISSION3628500 5079900



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Raw feed stock for refineries 100 100 0 0 100 0

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14514 24 350 

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See Attachments - TRP Operations Part II Section A 1d operations Tire Recycling and Processing LLC 1309 Industrial Way Harlingen Cameron TX 78550

Page 10 SANITIZED SUBMISSIONSee Attachment 004 (Flow Diagram -TSCA.xls)

Flow Diagram -TSCA.xls
Page 11 SANITIZED SUBMISSIONFilling tanker truck Safety Glasses,Safety gloves Automatic shut off,containment Liquid 100% 2 1 240 Line Purging Safety glasses,Safety gloves 100 5 2 8 Sampling Saety glasses,Safety gloves 100 1 1 50

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### X Arroyo Colorado TX 2202

T-001 .0049895

kg /day Fugitive Air
FUGL01 .0022

kg/day Fugitive Air
FUGE01 .0802

kg/day Fugitive Air
SSM-01 .0022

kg/day Fugitive Air
MSS-02 .1944 g/day Fugitive Air
MSS-03 .00498

g/day Fugitive Air

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Page 14 SANITIZED SUBMISSIONPage 15 SANITIZED SUBMISSION1. Reduction in waste tire sites in south Texas and the environmental impact from such sites

2. Scrap tires must be managed to control fires and human disease vectors ( mosquitoes, rats, snakes ) 3. Recycling of a waste stream ( tires ) into oil to reduce dependence on foriegn oil.

Page 16 SANITIZED SUBMISSION001 Part II Section A 1d operations TRP Operation Description41040795182936366 4 002 Part 1 Section B 1(c)CAS Inventory Expert Service Report CAS Inventory Search.pdf Pt.I, Sec.B, 1c. 1 003 MSDS Yamels Oil MATERIAL SAFETY DATA SHEET Yamels Oil.doc 4 004 Part II Section A 1d Process Description Flow Diagram -TSCA.xls Pt.2, Sec.A, 1d. 2 005 Part 1 Section B 1e(1) Precursor Substances Chemical Assignment TSCA.xls Pt.I, Sec.B, 1e(1). 1 006 Part 1 Section C part 1 Production Production.doc Pt.I, Sec.C, 1. 1 007 Physical/ Chemical Properties TRP Oil sample test.xls 1 008 Scientific Literature Innovations in Pyrolysis Technology.pdf 8 009 Scientific Literature Thermal Conversion of Scrap Tyres.pdf 8 010 Physical / Properties Certificate of Analysis img034 Test Sample 1of 2.pdf 1 011 Physical/Properties Certificate of Analysis img033 Test Sample 2 of 2.pdf 1 012 Physical/Chemical Properties Certificate of img031 Test Sample.pdf 1 013 Chemical Structure Diagram Limonene.doc Pt.I, Sec.B, 1e. 1

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### ATTACHMENT HEADER SHEET
Attachment Number 001 Attachment Name Part II Section A 1d operations 

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N/A Does not contain CBI 

### Report Number PMNX130122167661810

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Pt.I, Sec.B, 1c. Does not contain CBI 

### Report Number PMNX130122167661810

### ATTACHMENT HEADER SHEET
Attachment Number 003 Attachment Name MSDS Yamels Oil 

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Attachment Number 004 Attachment Name Part II Section A 1d Process Description 

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### ATTACHMENT HEADER SHEET
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### Report Number PMNX130122167661810

### ATTACHMENT HEADER SHEET
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Attachment Number 007 Attachment Name Physical/ Chemical Properties 

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Attachment Number 009 Attachment Name Scientific Literature 

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Attachment Number 010 Attachment Name Physical / Properties Certificate of Analysis 

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Attachment Number 011 Attachment Name Physical/Properties Certificate of Analysis 

### Associated PMN Section Number

N/A Does not contain CBI 

### Report Number PMNX130122167661810

### ATTACHMENT HEADER SHEET
Attachment Number 012 Attachment Name Physical/Chemical Properties Certificate of Analysis 

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N/A Does not contain CBI 

### Report Number PMNX130122167661810

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Attachment Number 013 Attachment Name Chemical Structure Diagram 

### Associated PMN Section Number

Pt.I, Sec.B, 1e. Does not contain CBI 

### Report Number PMNX130122167661810