### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

1241 La Cygne 2 

## subbituminous

### Fuel Type 2 Fuel Type 3 Other Fuel Description



## No.2 Fuel Oil (distillate) other

### EIA

Facility Code Facility Name Boiler ID Basis An alyte



## 1241 La Cygne 2 As Received Higher Heating Value 

## 1241 La Cygne 2 As Received % Moisture 

## 1241 La Cygne 2 As Received % Ash 

## 1241 La Cygne 2 As Received % Sulfur 

## 1241 La Cygne 2 Dry basis Higher Heating Value 

## 1241 La Cygne 2 Dry basis % Ash 

## 1241 La Cygne 2 Dry basis % Sulfur 

## 1241 La Cygne 2 Dry basis Antim ony 

## 1241 La Cygne 2 Dry basis Arsenic 

## 1241 La Cygne 2 Dry basis Beryllium 

## 1241 La Cygne 2 Dry basis Cadmium 

## 1241 La Cygne 2 Dry basis Chlorine 

## 1241 La Cygne 2 Dry basis Chromium 

## 1241 La Cygne 2 Dry basis Cobalt 

## 1241 La Cygne 2 Dry basis Fluorine 

## 1241 La Cygne 2 Dry basis Lead 

## 1241 La Cygne 2 Dry basis Manganese 

## 1241 La Cygne 2 Dry basis Mercury 

## 1241 La Cygne 2 Dry basis Nickel 

## 1241 La Cygne 2 Dry basis Selenium

### An alysis M ethod for each Analyte

(example: ASTM D5865-04) 

## ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239B ASTM D5865 ASTM D3174 ASTM D4239B ASTM D6357 - ICP-MS ASTM D6357 - ICP-MS ASTM D6357 - ICP-MS ASTM D6357 - ICP-MS ASTM D6721 ASTM D6357 - ICP-MS ASTM D6357 - ICP-MS ASTM D5987 - IC ASTM D6357 - ICP-MS ASTM D6357 - ICP-MS ASTM D6722-01 - DCGA-AA ASTM D6357 - ICP-MS ASTM D4606 - ICP-AES-HYEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 1241 La Cygne 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### R1 

## 5/19/2010 5/19/2010 8618.00 Btu/lb R2 

## 5/19/2010 5/19/2010 8580.00 Btu/lb R3 

## 5/19/2010 5/19/2010 8534.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 28.4 5.4 0.33 12036 Btu/lb 7.54 0.46 29 5.11 0.35 12084 Btu/lb 7.2 0.49 29.2 7.18 0.33 12053 Btu/lb 7.18 0.47Chlorine

(Dry Basis) Chlorine

Units (test results in ug/g) Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

## 28 ppm 0.085 μg/g 0.17 μg/g 1.5 μg/g 0.3 17 ppm 0.083 μg/g 0.16 μg/g 1.7 μg/g 0.2 18 ppm 0.099 μg/g 0.16 μg/g 1.7 μg/g 0.2Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## μg/g 0.09 μg/g 8 μg/g 2.9 μg/g 14 μg/g μg/g 0.1 μg/g 6 μg/g 2.6 μg/g 11 μg/g μg/g 0.07 μg/g 6 μg/g 2.5 μg/g 13 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units (test results in ug/g) Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 8 μg/g 1 μg/g 62 ppm 2.6 μg/g 28.4 6 μg/g 1 μg/g 57 ppm 2.2 μg/g 29 7 μg/g 1.2 μg/g 57 ppm 2.2 μg/g 29.2 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

## 44.2 7.54 48.26 68.96 4.8 0.93 0.46 44.47 7.2 48.33 69 4.84 0.93 0.49 44.49 7.18 48.33 68.99 4.85 0.93 0.47 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



## 17.31 17.54 17.58EIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 1241 La Cygne 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 1 

## 5/20/2010 5/20/2010 8396.00 Btu/lb 2 5/20/2010 5/20/2010 8329.00 Btu/lb 3 5/21/2010 5/21/2010 8455.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 30.08 5.41 0.34 12008 Btu/lb 7.74 0.48 30.24 5.63 0.32 11939 Btu/lb 8.07 0.46 29.61 7.28 0.47 12012 Btu/lb 7.28 0.47Chlorine

(Dry Basis) Chlorine

Units (Test results in ug/g) Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

## 17 ppm 0.11 μg/g 0.17 μg/g 1.7 μg/g 0.2 18 ppm 0.098 μg/g 0.17 μg/g 1.5 μg/g 0.3 18 ppm 0.1 μg/g 0.17 μg/g 1.6 μg/g 0.3Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## μg/g 0.09 μg/g 7 μg/g 2.9 μg/g 13 μg/g μg/g 0.1 μg/g 7 μg/g 3 μg/g 11 μg/g μg/g 0.09 μg/g 7 μg/g 3 μg/g 11 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units (test results in ug/g) Cobalt (Dry

Basis) Cobalt Units 

## 7 μg/g 1.1 μg/g 64 ppm 2.2 μg/g 7 μg/g 1.2 μg/g 66 ppm 2.2 μg/g 7 μg/g 1 μg/g 61 ppm 2.4 μg/g

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



## 30.08 44.17 7.74 48.09 68.83 4.83 0.93 0.48 30.24 44.17 8.07 47.76 68.44 4.77 0.92 0.46 29.61 43.87 7.28 48.85 69.12 4.77 0.93 0.47 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

## 17.19 17.34 17.43EIA Facility Code Facility Name Boiler ID HAPs Test Group 1241 La Cygne 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur

(Dry Basis) 1 5/21/2010 5/21/2010 8666.00 Btu/lb 28.2 5.47 0.29 12070 Btu/lb 7.62 0.4 2 5/21/2010 5/21/2010 8608.00 Btu/lb 29.16 5.21 0.25 12152 Btu/lb 7.36 0.35 3 5/22/2010 5/22/2010 8761.00 Btu/lb 27.67 5.16 0.3 12112 Btu/lb 7.13 0.42 Fuel Testing ResultsChlorine (Dry Basis) Chlorine

Units (Test results in ug/g) Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units(test results in ug/g) Cobalt (Dry

Basis) Cobalt Units 29 ppm 0.078 μg/g 0.16 μg/g 1.3 μg/g 0.2 μg/g 0.08 μg/g 6 μg/g 2.7 μg/g 11 μg/g 6 μg/g 0.9 μg/g 61 ppm 2.1 μg/g 20 ppm 0.071 μg/g 0.12 μg/g 1.3 μg/g 0.2 μg/g 0.07 μg/g 6 μg/g 2.4 μg/g 11 μg/g 6 μg/g 0.7 μg/g 67 ppm 1.9 20 ppm 0.07 μg/g 0.14 μg/g 1.4 μg/g 0.2 μg/g 0.1 μg/g 6 μg/g 2.9 μg/g 12 μg/g 6 μg/g 0.8 μg/g 66 ppm 2.1Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

28.2 43.75 7.62 48.63 69.26 4.81 0.9 0.4 17.01 29.16 43.55 7.36 49.06 69.71 4.82 0.81 0.35 16.95 27.67 43.93 7.13 48.94 69.55 4.84 0.84 0.42 17.22 Proximate Analyses, % by wt Ultimate Analyses, % by wtEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 1241 La Cygne 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm