### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

3809 Yorktown 3 

### No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description 

### No.6 Fuel Oil (residual or bunker C)EIA

Facility Code Facility Name Boiler ID Basis An alyte



### 3809 Yorktown 3 As Received Higher Heating Value 

### 3809 Yorktown 3 As Received % Moisture 

### 3809 Yorktown 3 As Received % Ash 

### 3809 Yorktown 3 As Received % Sulfur 

### 3809 Yorktown 3 Dry basis Higher Heating Value 

### 3809 Yorktown 3 Dry basis % Ash 

### 3809 Yorktown 3 Dry basis % Sulfur 

### 3809 Yorktown 3 Dry basis Antim ony 

### 3809 Yorktown 3 Dry basis Arsenic 

### 3809 Yorktown 3 Dry basis Bery llium 

### 3809 Yorktown 3 Dry basis Cadmium 

### 3809 Yorktown 3 Dry basis Chlorine 

### 3809 Yorktown 3 Dry basis Chromium 

### 3809 Yorktown 3 Dry basis Cobalt 

### 3809 Yorktown 3 Dry basis Fluorine 

### 3809 Yorktown 3 Dry basis Lead 

### 3809 Yorktown 3 Dry basis Manganese 

### 3809 Yorktown 3 Dry basis Mercury 

### 3809 Yorktown 3 Dry basis Nickel 

### 3809 Yorktown 3 Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D 240

ASTM D-482 ASTM D 1552 ASTM D 240 ASTM D-482 ASTM D 1552

SW 846 7060A SW 846 6010B SW 846 6010B SW 846 9076 SW 846 6010B

ASTM D3761 SW 846 6010B SW 846 6010B SW 846 7470A SW 846 6010BEIA Facility Code Facility Name Boiler ID 

### 3809 Yorktown 3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) U3-Oil #1 

### 6/2/2010 6/2/2010 18114.00 U3-Oil #2 

### 6/3/2010 6/3/2010 18179.00 U3-Oil #3 

### 6/4/2010 6/4/2010 18162.00 Fuel Testing ResultsHA Ps Test Group



### Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 0.09 0.83 Btu/lb 0.07 0.82 Btu/lb 0.08 0.83HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### 69.1 ppm < 0.02 ppm 91.8 ppm < 0.02 ppm 98.7 ppm < 0.02 ppmAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00 < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00 < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm < 5.00 ppm < 5.00 ppm 47.5 ppm ppm < 5.00 ppm < 5.00 ppm 46.3 ppm ppm < 5.00 ppm < 5.00 ppm 47.1 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 30.5 ppm 0.09 17.1 ppm 0.07 15.2 ppm 0.08 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 87.83 11 0.25 0.83 < 0.10 88.25 10.61 0.25 0.82 < 0.10 88.93 9.91 0.25 0.83 < 0.10 Ultimate Analy

ses, % by

wtEIA Facility Code Facility

Name Boiler ID 

### 3809 Yorktown 3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) U3-Oil #2 

### 6/3/2010 6/3/2010 18179.00 U3-Oil #3 

### 6/4/2010 6/4/2010 18162.00 Fuel Testing ResultsHA Ps Test Group



### Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 0.07 0.82 Btu/lb 0.08 0.83HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### 91.8 ppm < 0.02 ppm 98.7 ppm < 0.02 ppmAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00 < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm < 5.00 ppm < 5.00 ppm 46.3 ppm ppm < 5.00 ppm < 5.00 ppm 47.1 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 17.1 ppm 0.07 15.2 ppm 0.08 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 88.25 10.61 0.25 0.82 < 0.10 88.93 9.91 0.25 0.83 < 0.10

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 

### 3809 Yorktown 3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) U3-Oil #2 

### 6/3/2010 6/3/2010 18179.00 U3-Oil #3 

### 6/4/2010 6/4/2010 18162.00 Fuel Testing ResultsHA Ps Test Group



### Non-dioxin/furan organic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 0.07 0.82 Btu/lb 0.08 0.83HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### 91.8 ppm < 0.02 ppm 98.7 ppm < 0.02 ppmAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00 < 0.50 ppm < 5.00 ppm < 1.00 ppm < 5.00Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm < 5.00 ppm < 5.00 ppm 46.3 ppm ppm < 5.00 ppm < 5.00 ppm 47.1 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon 

### 17.1 ppm 0.07 88.25 15.2 ppm 0.08 88.93 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen 

### 10.61 0.25 0.82 < 0.10 9.91 0.25 0.83 < 0.10 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 3809 Yorktown 3 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units U3-Oil #1 

### 6/2/2010 6/2/2010 18114.00 Btu/lb U3-Oil #2 

### 6/3/2010 6/3/2010 18179.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 0.09 0.83 0.07 0.82Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 69.1 ppm < 0.02 ppm < 0.50 ppm < 5.00 91.8 ppm < 0.02 ppm < 0.50 ppm < 5.00Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm < 1.00 ppm < 5.00 ppm < 5.00 ppm < 5.00 ppm ppm < 1.00 ppm < 5.00 ppm < 5.00 ppm < 5.00 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 47.5 ppm 30.5 ppm 46.3 ppm 17.1 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 0.09 87.83 11 0.25 0.83 < 0.10 0.07 88.25 10.61 0.25 0.82 < 0.10 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm