**Kiln No Data Source**  **Run No**  **FA CID**  **Old FA** **CID Test Date**  33 2008 Survey 1 MARR-1 5 4/14/2005 33 2008 Survey 2 MARR-1 5 4/14/2005 33 2008 Survey 3 MARR-1 5 4/14/2005 41 2010 Survey 1 FLOR-1 123 10/13/2010 41 2010 Survey 2 FLOR-1 123 10/13/2010 41 2010 Survey 3 FLOR-1 123 10/13/2010

60, 61, 62 2010 Survey 1 DALT-1 5/14/2010

60, 61, 62 2010 Survey 2 DALT-1 5/14/2010

60, 61, 62 2010 Survey 3 DALT-1 5/14/2010

60 2010 Survey 1 DALT-1 5/14/2010

60 2010 Survey 2 DALT-1 5/14/2010

60 2010 Survey 3 DALT-1 5/14/2010

61 2010 Survey 1 DALT-1 5/14/2010

61 2010 Survey 2 DALT-1 5/14/2010

61 2010 Survey 3 DALT-1 5/14/2010

62 2010 Survey 1 DALT-1 5/14/2010

62 2010 Survey 2 DALT-1 5/14/201062 2010 Survey 3 DALT-1 5/14/2010

79 2008 Survey 1 MARR-2 11/19/2002 79 2008 Survey 2 MARR-2 11/19/2002 79 2008 Survey 3 MARR-2 11/19/2002 79 2008 Survey 1 MARR-2 8/29/2002 79 2008 Survey 2 MARR-2 8/29/2002 79 2008 Survey 3 MARR-2 8/29/2002 80 2008 Survey 1 STPK-1 10/12/2005 80 2008 Survey 2 STPK-1 10/12/2005 80 2008 Survey 3 STPK-1 10/12/2005

64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2008 Survey 1 MOHA-3 50 6/17/2008

64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2008 Survey 2 MOHA-3 50 6/17/2008

64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2008 Survey 3 MOHA-3 50 6/17/2008**Parent Company Facility Name**  **City State**  **Kiln ID**

Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX RK-1 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX RK-1 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1

Dal-Tile Corp. Dal Italia Muskogee OK RK-2, RK-3, RK-4

Dal-Tile Corp. Dal Italia Muskogee OK RK-2, RK-3, RK-4

Dal-Tile Corp. Dal Italia Muskogee OK RK-2, RK-3, RK-4

Dal-Tile Corp. Dal Italia Muskogee OK RK-2

Dal-Tile Corp. Dal Italia Muskogee OK RK-2

Dal-Tile Corp. Dal Italia Muskogee OK RK-2

Dal-Tile Corp. Dal Italia Muskogee OK RK-3

Dal-Tile Corp. Dal Italia Muskogee OK RK-3

Dal-Tile Corp. Dal Italia Muskogee OK RK-3

Dal-Tile Corp. Dal Italia Muskogee OK RK-4

Dal-Tile Corp. Dal Italia Muskogee OK RK-4Dal-Tile Corp. Dal Italia Muskogee OK RK-4

Monarch Ceramic Tile Monarch Florence AL Kiln #3 Monarch Ceramic Tile Monarch Florence AL Kiln #3 Monarch Ceramic Tile Monarch Florence AL Kiln #3 Monarch Ceramic Tile Monarch Florence AL Kiln #3 Monarch Ceramic Tile Monarch Florence AL Kiln #3 Monarch Ceramic Tile Monarch Florence AL Kiln #3 Stonepeak Ceramics, Inc. Stonepeak Crossville TN RK-1 Stonepeak Ceramics, Inc. Stonepeak Crossville TN RK-1 Stonepeak Ceramics, Inc. Stonepeak Crossville TN RK-1

Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-1, RK-2, RK-3, RK4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12

Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-1, RK-2, RK-3, RK4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12

Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-1, RK-2, RK-3, RK4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12**Source Type AP** **CD ID AP** **CD Type Test Methods**  **Production Rate During**  **Test (tph)** Roller Kiln None 1, 2, 3, 4, 320 6.02 Roller Kiln None 1, 2, 3, 4, 320 6.02 Roller Kiln None 1, 2, 3, 4, 320 6.02 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 8.06 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 7.93 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 7.90

Roller Kiln EPN-29 Wet Scrubber320 27.44

Roller Kiln EPN-29 Wet Scrubber320 27.44

Roller Kiln EPN-29 Wet Scrubber320 27.44

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln EPN-29 Wet Scrubber320 9.15Roller Kiln EPN-29 Wet Scrubber320 9.15

Roller Kiln None 1, 2, 3, 4, 320 5.07 Roller Kiln None 1, 2, 3, 4, 320 5.07 Roller Kiln None 1, 2, 3, 4, 320 5.07 Roller Kiln None 1, 2, 3, 4, 26A 6.34 Roller Kiln None 1, 2, 3, 4, 26A 6.34 Roller Kiln None 1, 2, 3, 4, 26A 6.34 Roller Kiln Baghouse #11 DIFF 1, 2, 3, 4, 6, 26 6.51 Roller Kiln Baghouse #11 DIFF 1, 2, 3, 4, 6, 26 6.58 Roller Kiln Baghouse #11 DIFF 1, 2, 3, 4, 6, 26 6.58

Roller Kiln None 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A 27.26

Roller Kiln None 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A 27.68

Roller Kiln None 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A 25.97**Source Flow A** **ctual (acfm) Flow Dry Standard**  **(dscfm) Sample Volume** 

**(dscf)** Test Report 9,565 4,922 24.16 Test Report 10,294 5,351 24.91 Test Report 10,152 5,244 24.54 Separate declassified submittal 22,813 14,832 22.07 Separate declassified submittal 22,955 15,327 21.93 Separate declassified submittal 22,884 15,291 21.97 Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349 Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349 Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349

Separate declassified submittal; hourly production not measured. Kilns identically

sized 72,766 54,349Separate declassified submittal; hourly

production not measured. Kilns identically

sized 72,766 54,349 Test Report 17,180 9,539 Test Report 16,876 9,383 Test Report 16,270 9,112 Test Report 15,029 8,356 Test Report 15,025 8,313 Test Report 14,885 8,206 Last appendix of test report 15,892 10,235 3.91 Last appendix of test report 15,676 10,041 3.78 Last appendix of test report 15,292 10,436 4.01

ICR, production rate worksheet 67,432 35,697 33.75

ICR, production rate worksheet 67,087 35,417 33.53

ICR, production rate worksheet 67,891 35,860 33.96**Sample Volume**

**(dscm) Moisture (%)**  **Temp Stack Gas (deg F)**  **Oxygen (%) HF Concentration**  0.68 12.33 435.00 14.40 71.24 0.71 12.41 425.00 14.40 66.02 0.69 12.37 431.00 14.20 67.17 0.63 4.89 278.5 17.9 33.03 0.62 5.11 281.8 18 28.32 0.62 5.3 281.5 18 23.85

16.13 133.50 19.00 10.664

16.35 133.50 19.00 12.618

16.57 133.50 19.00 6.773

16.13 133.50 19.00 10.664

16.35 133.50 19.00 12.618

16.57 133.50 19.00 6.773

16.13 133.50 19.00 10.664

16.35 133.50 19.00 12.618

16.57 133.50 19.00 6.773

16.13 133.50 19.00 10.664

16.35 133.50 19.00 12.61816.57 133.50 19.00 6.773 5.76 423.00 18.50 32.58 6.00 424.00 18.50 38.62 5.43 426.00 18.50 35.21 8.19 396.00 18.50 0.0122 8.54 397.00 18.50 0.0135 8.65 399.00 18.50 0.0123 0.11 6.50 259.40 19.00 0.22 0.11 7.00 260.00 18.90 0.22 0.11 6.90 260.30 18.90 0.21

0.96 6.75 350.60 17.50 198.228

0.95 6.83 352.20 17.50 227.0971

0.96 6.54 354.30 17.00 192.572**HF Concentration**

**Units HF Concentration** 

**Converted to (** **μ g/dscm)**  **HF Emission Rate (lb/hr)**  **< HF Emission Factor**  **(lb/ton) HCl Concentration**  ppm 59,299.60 1.09 0.180942895 32.32 ppm 54,954.51 1.1 0.182602922 30.73 ppm 55,911.76 1.1 0.182602922 31.82 ppm 27,493.90 1.521189594 0.188781501 8.42 ppm 23,573.34 1.344819786 0.169679223 8.67 ppm 19,852.55 1.124357526 0.142258669 7.91

ppm 8,876.63 1.8 0.065605625 9.4

ppm 10,503.12 2.13 0.077633323 15.103

ppm 5,637.79 1.14 0.041550229 5.965

ppm 8,876.63 0.6 0.065605625 9.4

ppm 10,503.12 0.71 0.077633323 15.103

ppm 5,637.79 0.38 0.041550229 5.965

ppm 8,876.63 0.6 0.065605625 9.4

ppm 10,503.12 0.71 0.077633323 15.103

ppm 5,637.79 0.38 0.041550229 5.965

ppm 8,876.63 0.6 0.065605625 9.4

ppm 10,503.12 0.71 0.077633323 15.103ppm 5,637.79 0.38 0.041550229 5.965

ppm 27,119.33 0.97 0.191434774 9.49 ppm 32,146.97 1.13 0.223011644 10.37 ppm 29,308.52 1 0.197355437 9.32 gr/dscf 27,917.89 0.87 0.137234798 0.0048 gr/dscf 30,892.75 0.96 0.151431501 0.0048 gr/dscf 28,146.73 0.87 0.137234798 0.0045 ppm 183.13 0.0069< 0.001059908 2.2 ppm 183.13 0.007< 0.00106383 1.8 ppm 174.80 0.0069< 0.001048632 1.8

ppm 165,003.38 22.04418 0.808571357 17.36399

ppm 189,033.78 25.05638 0.905212264 16.60777

ppm 160,295.37 21.51282 0.8283924 15.42357**HCl Concentration**

**Units HCl Concentration** 

**Converted to (** **μ g/dscm)**  **HCl Emission Rate (lb/hr)**  **< HCl Emission Factor**  **(lb/ton)** ppm 49,029.31 0.9 0.14940239 ppm 46,617.28 0.93 0.15438247 ppm 48,270.81 0.95 0.157702523 ppm 12,773.11 0.705479232 0.087550841 ppm 13,152.35 0.749571684 0.094575305 ppm 11,999.44 0.683433006 0.086470956

ppm 14,259.76 2.89 0.105333475

ppm 22,911.19 4.65 0.169481197

ppm 9,048.88 1.84 0.067063527

ppm 14,259.76 0.963333333 0.105333475

ppm 22,911.19 1.55 0.169481197

ppm 9,048.88 0.613333333 0.067063527

ppm 14,259.76 0.963333333 0.105333475

ppm 22,911.19 1.55 0.169481197

ppm 9,048.88 0.613333333 0.067063527

ppm 14,259.76 0.963333333 0.105333475

ppm 22,911.19 1.55 0.169481197ppm 9,048.88 0.613333333 0.067063527

ppm 14,396.29 0.51 0.100651273 ppm 15,731.25 0.55 0.10854549 ppm 14,138.40 0.48 0.09473061 gr/dscf 10,984.09 0.35 0.055209401 gr/dscf 10,984.09 0.34 0.05363199 gr/dscf 10,297.58 0.32 0.050477167 ppm 3,337.39 0.13 0.019969278 ppm 2,730.59 0.1 0.015197568 ppm 2,730.59 0.11 0.016717325

ppm 26,341.10 3.524046 0.129260542

ppm 25,193.92 3.344111 0.120812755

ppm 23,397.49 3.144503 0.12108512**Overall Comments**

1 Porcelain 2 Porcelain 3 Porcelain

Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.

RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from

Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1.**Ty pe of Tile** 

Floor Floor Floor Floor Floor Floor

Floor

Floor

Floor

Floor

Floor

Floor

Floor

Floor

Floor

Floor

FloorFloor

Floor Floor Floor Floor Floor Floor Floor Floor Floor

Wall

Wall

Wall**Kiln No Data Source**  **Run No FA** **CID Old**  **FA CID**  36 2010 Survey 1 MARR-1 5 36 2010 Survey 2 MARR-1 5 36 2010 Survey 3 MARR-1 5 41 2010 Survey 1 FLOR-1 123 41 2010 Survey 2 FLOR-1 123 41 2010 Survey 3 FLOR-1 123 59, 60 2008 Survey 1 DALT-1 59, 60 2008 Survey 2 DALT-1 59, 60 2008 Survey 3 DALT-1 59 2008 Survey 1 DALT-1 59 2008 Survey 2 DALT-1 59 2008 Survey 3 DALT-1 60 2008 Survey 1 DALT-1 60 2008 Survey 2 DALT-1 60 2008 Survey 3 DALT-1 59, 60 2008 Survey 1 DALT-1 59, 60 2008 Survey 2 DALT-1 59, 60 2008 Survey 3 DALT-1 59 2008 Survey 1 DALT-1 59 2008 Survey 2 DALT-1 59 2008 Survey 3 DALT-1 60 2008 Survey 1 DALT-1 60 2008 Survey 2 DALT-1 60 2008 Survey 3 DALT-1 59, 60 2008 Survey 1 DALT-1 59, 60 2008 Survey 2 DALT-1 59, 60 2008 Survey 3 DALT-1 59 2008 Survey 1 DALT-1 59 2008 Survey 2 DALT-1 59 2008 Survey 3 DALT-1 60 2008 Survey 1 DALT-1 60 2008 Survey 2 DALT-1 60 2008 Survey 3 DALT-1 61, 62 2008 Survey 1 DALT-1 61, 62 2008 Survey 2 DALT-1 61, 62 2008 Survey 3 DALT-1 61 2008 Survey 1 DALT-1 61 2008 Survey 2 DALT-1 61 2008 Survey 3 DALT-1 62 2008 Survey 1 DALT-1 62 2008 Survey 2 DALT-1 62 2008 Survey 3 DALT-1 60, 61, 62 2010 Survey 1 DALT-1 60, 61, 62 2010 Survey 2 DALT-1 60, 61, 62 2010 Survey 3 DALT-1 60 2010 Survey 1 DALT-1 60 2010 Survey 2 DALT-1 60 2010 Survey 3 DALT-161 2010 Survey 1 DALT-1

61 2010 Survey 2 DALT-1 61 2010 Survey 3 DALT-1 62 2010 Survey 1 DALT-1 62 2010 Survey 2 DALT-1 62 2010 Survey 3 DALT-1 63 2008 Survey 1 DALT-1 63 2008 Survey 2 DALT-1 63 2008 Survey 3 DALT-1 63 2008 Survey 1 DALT-1 63 2008 Survey 2 DALT-1 63 2008 Survey 3 DALT-1 76 2008 Survey 1 MARR-2 76 2008 Survey 2 MARR-2 76 2008 Survey 3 MARR-2 77 2010 Survey 1 MARR-2 77 2010 Survey 2 MARR-2 77 2010 Survey 3 MARR-2 84 2010 Survey 1 MARR-1 5 84 2010 Survey 2 MARR-1 5 84 2010 Survey 3 MARR-1 5 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2008 Survey 1 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2008 Survey 2 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2008 Survey 3 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2010 Survey 1 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2010 Survey 2 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2010 Survey 3 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2010 Survey 1 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2010 Survey 2 MOHA-3 50 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75 2010 Survey 3 MOHA-3 50**Test Date Parent Company**  **Facility Name City**  **State**

12/6-7/2010 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX 12/6-7/2010 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX 12/6-7/2010 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX 5/25/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN 5/25/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN 5/26/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/7/2005 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/12/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/3/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 11/2/2006 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK

5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK 12/8/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/8/2005 Dal-Tile Corp. Dal Italia Muskogee OK 12/8/2005 Dal-Tile Corp. Dal Italia Muskogee OK 4/13/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/13/2006 Dal-Tile Corp. Dal Italia Muskogee OK 4/13/2006 Dal-Tile Corp. Dal Italia Muskogee OK 12/11/2003 Monarch Ceramic Tile Monarch Florence AL 12/11/2003 Monarch Ceramic Tile Monarch Florence AL 12/11/2003 Monarch Ceramic Tile Monarch Florence AL 5/4-5/10 Monarch Ceramic Tile Monarch Florence AL 5/4-5/10 Monarch Ceramic Tile Monarch Florence AL 5/4-5/10 Monarch Ceramic Tile Monarch Florence AL 12/6-7/2010 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX 12/6-7/2010 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX 12/6-7/2010 Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX 6/17/2008 Mohawk Industries Dal-Tile El Paso Plant El Paso TX 6/17/2008 Mohawk Industries Dal-Tile El Paso Plant El Paso TX 6/17/2008 Mohawk Industries Dal-Tile El Paso Plant El Paso TX 12/13-14/2010Mohawk Industries Dal-Tile El Paso Plant El Paso TX 12/13-14/2010Mohawk Industries Dal-Tile El Paso Plant El Paso TX 12/13-14/2010Mohawk Industries Dal-Tile El Paso Plant El Paso TX 12/15-16/2010Mohawk Industries Dal-Tile El Paso Plant El Paso TX 12/15-16/2010Mohawk Industries Dal-Tile El Paso Plant El Paso TX 12/15-16/2010Mohawk Industries Dal-Tile El Paso Plant El Paso TX**Kiln ID Source Type**  **AP CD ID**  **AP CD Type** 

RK-4 Roller Kiln None RK-4 Roller Kiln None RK-4 Roller Kiln None RK-1 Roller Kiln CD-1 DIFF RK-1 Roller Kiln CD-1 DIFF RK-1 Roller Kiln CD-1 DIFF RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1, RK-2 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-1 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-2 Roller Kiln EPN-20 Wet Scrubber RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2 Roller Kiln EPN-29 Wet Scrubber RK-2 Roller Kiln EPN-29 Wet Scrubber RK-2 Roller Kiln EPN-29 Wet ScrubberRK-3 Roller Kiln EPN-29 Wet Scrubber

RK-3 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-5 Roller Kiln None RK-5 Roller Kiln None RK-5 Roller Kiln None RK-5 Roller Kiln None RK-5 Roller Kiln None RK-5 Roller Kiln None Kiln #1 Roller Kiln None Kiln #1 Roller Kiln None Kiln #1 Roller Kiln None RK-2L Roller Kiln None RK-2L Roller Kiln None RK-2L Roller Kiln None RK-5U Roller Kiln None RK-5U Roller Kiln None RK-5U Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None**Test Methods Production**  **Rate During Test (tph)**  1, 2, 3, 3A, 4, 5, 29 7.60599 1, 2, 3, 3A, 4, 5, 29 7.69417 1, 2, 3, 3A, 4, 5, 29 7.73827 1, 2, 3A, 4, 5, 23, 29, 320 5.56670 1, 2, 3A, 4, 5, 23, 29, 320 6.41549 1, 2, 3A, 4, 5, 23, 29, 320 8.07998 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 17.8 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 17.8 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 17.8 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 9.01 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 9.01 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 9.01 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 8.79 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 8.79 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 8.79 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 11.7 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 11.7 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 11.7 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 5.76 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 5.76 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 5.76 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 5.94 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 5.94 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 5.94 1, 2, 3, 5, 202 17.64 1, 2, 3, 5, 202 17.64 1, 2, 3, 5, 202 17.64 1, 2, 3, 5, 202 9.07 1, 2, 3, 5, 202 9.07 1, 2, 3, 5, 202 9.07 1, 2, 3, 5, 202 8.57 1, 2, 3, 5, 202 8.57 1, 2, 3, 5, 202 8.57 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 16.32 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 16.32 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 16.32 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 8.51 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 8.51 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 8.51 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 7.81 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 7.81 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A, 202 7.81 5, 29 27.30439 5, 29 27.43667 5, 29 26.83040 5, 29 9.10146 5, 29 9.14556 5, 29 8.943475, 29 9.10146

5, 29 9.14556 5, 29 8.94347 5, 29 9.10146 5, 29 9.14556 5, 29 8.94347 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 3.2 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 3.2 1, 2, 3, 5, 6C, 7E, 10, 25A, 26A, 202 3.2 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 3.2 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 3.2 1, 2, 3, 5, 6C, 7E, 10, 18, 25A, 26A, 202 3.2 1, 2, 3, 3A, 4, 5, 10 5.65 1, 2, 3, 3A, 4, 5, 10 5.65 1, 2, 3, 3A, 4, 5, 10 5.65 1, 2, 3, 3A, 4, 5, 29 7.99180 1, 2, 3, 3A, 4, 5, 29 7.99180 1, 2, 3, 3A, 4, 5, 29 7.99180 1, 2, 3, 3A, 4, 5, 23, 29 7.03278 1, 2, 3, 3A, 4, 5, 23, 29 6.85641 1, 2, 3, 3A, 4, 5, 23, 29 6.90050 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A 27.26 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A 27.68 1, 2, 3, 4, 5, 6C, 7E, 10, 25A, 26A 25.97 1, 2, 3, 3A, 4, 5, 23, 29 9.31000 1, 2, 3, 3A, 4, 5, 23, 29 9.06000 1, 2, 3, 3A, 4, 5, 23, 29 8.05000 1, 2, 3, 3A, 4, 5, 23, 29 8.04000 1, 2, 3, 3A, 4, 5, 23, 29 7.97000 1, 2, 3, 3A, 4, 5, 23, 29 7.90000**Source Flow A** **ctual (acfm) Flow Dry Standard**  **(dscfm)** Separate from Test Report 12,292 6,125 Separate from Test Report 12,585 6,253 Separate from Test Report 12,173 6,035 Separate declassified submittal 22,813 15,644 Separate declassified submittal 22,778 15,468 Separate declassified submittal 23,767 15,962 ICR, production rate worksheet 33,881 22,584 ICR, production rate worksheet 33,283 22,205 ICR, production rate worksheet 35,192 23,764 ICR, production rate worksheet 33,881 22,584 ICR, production rate worksheet 33,283 22,205 ICR, production rate worksheet 35,192 23,764 ICR, production rate worksheet 33,881 22,584 ICR, production rate worksheet 33,283 22,205 ICR, production rate worksheet 35,192 23,764 ICR, production rate worksheet 35,168 23,445 ICR, production rate worksheet 34,699 24,398 ICR, production rate worksheet 31,703 21,705 ICR, production rate worksheet 35,168 23,445 ICR, production rate worksheet 34,699 24,398 ICR, production rate worksheet 31,703 21,705 ICR, production rate worksheet 35,168 23,445 ICR, production rate worksheet 34,699 24,398 ICR, production rate worksheet 31,703 21,705 ICR, production rate worksheet 33,738 23,899 ICR, production rate worksheet 33,959 24,073 ICR, production rate worksheet 33,805 23,990 ICR, production rate worksheet 33,738 23,899 ICR, production rate worksheet 33,959 24,073 ICR, production rate worksheet 33,805 23,990 ICR, production rate worksheet 33,738 23,899 ICR, production rate worksheet 33,959 24,073 ICR, production rate worksheet 33,805 23,990 ICR, production rate worksheet 42,427 31,521 ICR, production rate worksheet 40,187 31,117 ICR, production rate worksheet 41,167 31,997 ICR, production rate worksheet 42,427 31,521 ICR, production rate worksheet 40,187 31,117 ICR, production rate worksheet 41,167 31,997 ICR, production rate worksheet 42,427 31,521 ICR, production rate worksheet 40,187 31,117 ICR, production rate worksheet 41,167 31,997 Separate declassified submittal. Kilns identically sized 67,009 49,883 Separate declassified submittal. Kilns identically sized 72,811 54,398 Separate declassified submittal. Kilns identically sized 68,960 51,310 Separate declassified submittal. Kilns identically sized 67,009 49,883 Separate declassified submittal. Kilns identically sized 72,811 54,398 Separate declassified submittal. Kilns identically sized 68,960 51,310Separate declassified submittal. Kilns identically sized 67,009 49,883 Separate declassified submittal. Kilns identically sized 72,811 54,398 Separate declassified submittal. Kilns identically sized 68,960 51,310 Separate declassified submittal. Kilns identically sized 67,009 49,883 Separate declassified submittal. Kilns identically sized 72,811 54,398 Separate declassified submittal. Kilns identically sized 68,960 51,310 ICR, production rate worksheet 15,602 8,252 ICR, production rate worksheet 15,313 8,098 ICR, production rate worksheet 15,527 8,072 ICR, production rate worksheet 15,730 8,310 ICR, production rate worksheet 16,137 8,469 ICR, production rate worksheet 15,995 8,462 Test Report 14,146 7,646 Test Report 13,988 7,540 Test Report 14,203 7,684 Separate from Test Report 12,037 5,198 Separate from Test Report 12,330 5,295 Separate from Test Report 12,353 5,322 Separate from Test Report 28,068 20,643 Separate from Test Report 27,404 20,507 Separate from Test Report 28,267 20,816 ICR, production rate worksheet 67,432 35,697 ICR, production rate worksheet 67,087 35,417 ICR, production rate worksheet 67,891 35,860 Separate from Test Report. Kilns identically sized 33,537 19,214 Separate from Test Report. Kilns identically sized 29,939 17,689 Separate from Test Report. Kilns identically sized 33,914 19,289 Separate from Test Report. Kilns identically sized 24,861 14,327 Separate from Test Report. Kilns identically sized 24,120 13,841 Separate from Test Report. Kilns identically sized 24,120 13,935**Sample Volume**

**(dscf) Sample Volume** 

**(dscm) Moisture (%)** **Temp Stack Gas (deg F)**  **Oxygen (%) PM** **Concentration** 214.97 6.09 11.33 480.29 13.34 12.00 151.16 4.28 11.64 473.38 13.05 10.90 149.26 4.23 11.85 473.17 13.21 14.50 124.27 3.52 6.14 265.4 19.1 19.09 122.40 3.47 6.98 266.4 19.3 10.65 128.55 3.64 7.5 269.2 19.3 17.73 39.19 1.11 24.37 138.40 16.00 0.026275 38.82 1.10 24.47 137.10 16.00 0.022011 40.96 1.16 23.31 137.00 16.00 0.019888 39.19 1.11 24.37 138.40 16.00 0.026275 38.82 1.10 24.47 137.10 16.00 0.022011 40.96 1.16 23.31 137.00 16.00 0.019888 39.19 1.11 24.37 138.40 16.00 0.026275 38.82 1.10 24.47 137.10 16.00 0.022011 40.96 1.16 23.31 137.00 16.00 0.019888 37.78 1.07 23.92 137.90 17.50 0.044474 38.37 1.09 19.80 137.50 18.00 0.038196 35.41 1.00 21.84 138.10 17.50 0.034076 37.78 1.07 23.92 137.90 17.50 0.044474 38.37 1.09 19.80 137.50 18.00 0.038196 35.41 1.00 21.84 138.10 17.50 0.034076 37.78 1.07 23.92 137.90 17.50 0.044474 38.37 1.09 19.80 137.50 18.00 0.038196 35.41 1.00 21.84 138.10 17.50 0.034076 38.06 1.08 18.63 137.70 18.00 0.015665 38.28 1.08 18.52 138.10 18.00 0.014557 37.97 1.08 18.43 138.20 18.00 0.012091 38.06 1.08 18.63 137.70 18.00 0.015665 38.28 1.08 18.52 138.10 18.00 0.014557 37.97 1.08 18.43 138.20 18.00 0.012091 38.06 1.08 18.63 137.70 18.00 0.015665 38.28 1.08 18.52 138.10 18.00 0.014557 37.97 1.08 18.43 138.20 18.00 0.012091 34.77 0.98 14.91 129.30 17.00 0.015699 34.34 0.97 14.35 128.60 17.00 0.010497 35.51 1.01 13.89 129.50 17.00 0.013007 34.77 0.98 14.91 129.30 17.00 0.015699 34.34 0.97 14.35 128.60 17.00 0.010497 35.51 1.01 13.89 129.50 17.00 0.013007 34.77 0.98 14.91 129.30 17.00 0.015699 34.34 0.97 14.35 128.60 17.00 0.010497 35.51 1.01 13.89 129.50 17.00 0.013007 141 4.00 16.13 132.88 18.60 0.0092 139 3.92 16.35 133.54 19.00 0.0082 126 3.57 16.57 134.42 18.80 0.0093 141 4.00 16.13 132.88 18.60 0.0092 139 3.92 16.35 133.54 19.00 0.0082 126 3.57 16.57 134.42 18.80 0.0093141 4.00 16.13 132.88 18.60 0.0092 139 3.92 16.35 133.54 19.00 0.0082 126 3.57 16.57 134.42 18.80 0.0093 141 4.00 16.13 132.88 18.60 0.0092 139 3.92 16.35 133.54 19.00 0.0082 126 3.57 16.57 134.42 18.80 0.0093 51.24 1.45 5.50 485.00 17.50 0.009124 49.86 1.41 5.40 486.20 17.00 0.009071 50.06 1.42 6.97 486.50 17.00 0.009559 53.24 1.51 7.51 456.30 18.00 0.013721 53.92 1.53 7.64 461.20 18.00 0.009646 53.17 1.51 6.75 462.70 18.00 0.007194 37 1.05 6.50 463.00 16.80 4.20E-03 36 1.03 6.30 467.00 16.60 3.50E-03 38 1.06 6.10 466.00 16.90 2.50E-03 135 3.83 11.79 617.40 16.00 7.58 144 4.07 11.87 622.50 16.30 8.51 144 4.07 11.57 622.60 16.10 7.96 137.77 3.90 2.99 231.79 19.3 2.20 180.09 5.10 3.37 224.54 19.27 3.41 182.33 5.16 3.2 236.83 19.01 2.81 33.75 0.96 6.75 350.60 17.50 0.017229 33.53 0.95 6.83 352.20 17.50 0.011072 33.96 0.96 6.54 354.30 17.00 0.013403 161.75 4.58 6.19 298.21 16.81 2.97 150.83 4.27 4.25 288.42 16.66 3.21 152.73 4.32 6.62 297.92 16.69 5.60 122.01 3.45 4.98 293.29 19.47 3.68 118.94 3.37 4.99 296.46 19.65 2.52 118.73 3.36 5.03 292.21 17.25 4.25**PM Concentration** 

**Units PM** **Concentration**

**Converted to (** **μ g/dscm)**  **PM Concentration** 

**(gr/dscf) PM** **Concentration**

**(gr/dscf @ 7% O2) PM** **Emission Rate (lb/hr)**  mg/dscm 12,000.00 0.0052 0.0096 0.275577828 mg/dscm 10,900.00 0.0048 0.0084 0.255736224 mg/dscm 14,500.00 0.0063 0.0115 0.328488771 mg/dscm 19,090.00 0.0083 0.0644 1.119948281 mg/dscm 10,650.00 0.0047 0.0404 0.617294328 mg/dscm 17,730.00 0.0077 0.0673 1.060423471 gr/dscf 60,126.45 0.0263 0.0745 5.087779 gr/dscf 50,368.91 0.0220 0.0624 4.190704 gr/dscf 45,510.74 0.0199 0.0564 4.052464 gr/dscf 60,126.45 0.0263 0.0745 2.575330831 gr/dscf 50,368.91 0.0220 0.0624 2.121249609 gr/dscf 45,510.74 0.0199 0.0564 2.051275317 gr/dscf 60,126.45 0.0263 0.0745 2.512448169 gr/dscf 50,368.91 0.0220 0.0624 2.069454391 gr/dscf 45,510.74 0.0199 0.0564 2.001188683 gr/dscf 101,772.16 0.0445 0.1818 8.940003 gr/dscf 87,405.89 0.0382 0.1831 7.990267 gr/dscf 77,977.88 0.0341 0.1393 6.341765 gr/dscf 101,772.16 0.0445 0.1818 4.401232246 gr/dscf 87,405.89 0.0382 0.1831 3.933669908 gr/dscf 77,977.88 0.0341 0.1393 3.122099692 gr/dscf 101,772.16 0.0445 0.1818 4.538770754 gr/dscf 87,405.89 0.0382 0.1831 4.056597092 gr/dscf 77,977.88 0.0341 0.1393 3.219665308 gr/dscf 35,847.03 0.0157 0.0751 3.210118 gr/dscf 33,311.54 0.0146 0.0698 3.004605 gr/dscf 27,668.46 0.0121 0.0580 2.487039 gr/dscf 35,847.03 0.0157 0.0751 1.65055387 gr/dscf 33,311.54 0.0146 0.0698 1.54488477 gr/dscf 27,668.46 0.0121 0.0580 1.278766651 gr/dscf 35,847.03 0.0157 0.0751 1.55956413 gr/dscf 33,311.54 0.0146 0.0698 1.45972023 gr/dscf 27,668.46 0.0121 0.0580 1.208272349 gr/dscf 35,924.84 0.0157 0.0560 4.242949 gr/dscf 24,020.83 0.0105 0.0374 2.800483 gr/dscf 29,764.59 0.0130 0.0464 3.568332 gr/dscf 35,924.84 0.0157 0.0560 2.212469117 gr/dscf 24,020.83 0.0105 0.0374 1.460300878 gr/dscf 29,764.59 0.0130 0.0464 1.860692728 gr/dscf 35,924.84 0.0157 0.0560 2.030479883 gr/dscf 24,020.83 0.0105 0.0374 1.340182122 gr/dscf 29,764.59 0.0130 0.0464 1.707639272 gr/dscf 21,052.84 0.0092 0.0556 3.92 gr/dscf 18,764.49 0.0082 0.0600 3.82 gr/dscf 21,281.67 0.0093 0.0616 4.07 gr/dscf 21,052.84 0.0092 0.0556 1.306666667 gr/dscf 18,764.49 0.0082 0.0600 1.273333333 gr/dscf 21,281.67 0.0093 0.0616 1.356666667gr/dscf 21,052.84 0.0092 0.0556 1.306666667

gr/dscf 18,764.49 0.0082 0.0600 1.273333333 gr/dscf 21,281.67 0.0093 0.0616 1.356666667 gr/dscf 21,052.84 0.0092 0.0556 1.306666667 gr/dscf 18,764.49 0.0082 0.0600 1.273333333 gr/dscf 21,281.67 0.0093 0.0616 1.356666667 gr/dscf 20,878.92 0.0091 0.0373 0.645556 gr/dscf 20,757.64 0.0091 0.0323 0.629771 gr/dscf 21,874.36 0.0096 0.0341 0.661595 gr/dscf 31,398.48 0.0137 0.0658 0.977598 gr/dscf 22,073.44 0.0096 0.0462 0.700419 gr/dscf 16,462.40 0.0072 0.0345 0.521911 gr/dscf 9,611.08 0.0042 0.0142 0.27 gr/dscf 8,009.23 0.0035 0.0113 0.22 gr/dscf 5,720.88 0.0025 0.0087 0.16 mg/dscm 7,580.00 0.0033 0.0094 0.147489253 mg/dscm 8,510.00 0.0037 0.0112 0.168653631 mg/dscm 7,960.00 0.0035 0.0101 0.158732829 mg/dscm 2,200.00 0.0010 0.0084 0.170417329 mg/dscm 3,410.00 0.0015 0.0127 0.262350092 mg/dscm 2,810.00 0.0012 0.0090 0.218919026 gr/dscf 39,426.01 0.0172 0.0704 5.273473 gr/dscf 25,336.63 0.0111 0.0453 3.362278 gr/dscf 30,670.78 0.0134 0.0478 4.120962 mg/dscm 2,970.00 0.0013 0.0044 0.213627932 mg/dscm 3,210.00 0.0014 0.0046 0.212525621 mg/dscm 5,600.00 0.0024 0.0081 0.40344594 mg/dscm 3,680.00 0.0016 0.0156 0.197313725 mg/dscm 2,520.00 0.0011 0.0122 0.130734121 mg/dscm 4,250.00 0.0019 0.0071 0.222666885**PM Emission** 

**Factor (lb/ton)** Below 1 mg check **Comments Ty** **pe of Tile**  0.036231695 73.0 Floor 0.033237649 46.7 Floor 0.042449921 61.3 Floor 0.201187066 67.2 Floor 0.096219428 36.9 Floor 0.131240786 64.5 Floor 0.285830281 66.7 Floor 0.235432809 55.4 Floor 0.227666517 52.8 Floor 0.285830281 66.7 RK-1, RK-2 tested together Floor 0.235432809 55.4 RK-1, RK-2 tested together Floor 0.227666517 52.8 RK-1, RK-2 tested together Floor 0.285830281 66.7 RK-1, RK-2 tested together Floor 0.235432809 55.4 RK-1, RK-2 tested together Floor 0.227666517 52.8 RK-1, RK-2 tested together Floor 0.764102821 108.9 Floor 0.682928803 95.0 Floor 0.542031197 78.2 Floor 0.764102821 108.9 RK-1, RK-2 tested together Floor 0.682928803 95.0 RK-1, RK-2 tested together Floor 0.542031197 78.2 RK-1, RK-2 tested together Floor 0.764102821 108.9 RK-1, RK-2 tested together Floor 0.682928803 95.0 RK-1, RK-2 tested together Floor 0.542031197 78.2 RK-1, RK-2 tested together Floor 0.181979478 38.6 Floor 0.170329082 36.1 Floor 0.140988605 29.7 Floor 0.181979478 38.6 RK-1, RK-2 tested together Floor 0.170329082 36.1 RK-1, RK-2 tested together Floor 0.140988605 29.7 RK-1, RK-2 tested together Floor 0.181979478 38.6 RK-1, RK-2 tested together Floor 0.170329082 36.1 RK-1, RK-2 tested together Floor 0.140988605 29.7 RK-1, RK-2 tested together Floor 0.25998462 35.4 Floor 0.171598223 23.4 Floor 0.218647794 29.9 Floor 0.25998462 35.4 RK-3, RK-4 tested together Floor 0.171598223 23.4 RK-3, RK-4 tested together Floor 0.218647794 29.9 RK-3, RK-4 tested together Floor 0.25998462 35.4 RK-3, RK-4 tested together Floor 0.171598223 23.4 RK-3, RK-4 tested together Floor 0.218647794 29.9 RK-3, RK-4 tested together Floor 0.143566637 84.3 Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.139229715 73.6 Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.151693615 76.0 Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.143566637 84.3 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.139229715 73.6 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.151693615 76.0 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor0.143566637 84.3 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.139229715 73.6 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.151693615 76.0 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.143566637 84.3 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.139229715 73.6 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.151693615 76.0 RK-2, RK-3, RK-4 tested together; Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. Floor 0.20173625 30.3 Floor 0.196803438 29.3 Floor 0.206748438 31.0 Floor 0.307420755 47.3 Floor 0.220257547 33.7 Floor 0.164122956 24.8 Floor 0.047787611 10.1 Floor 0.038938053 8.2 Floor 0.028318584 6.1 Floor 0.018455076 29.0 Floor 0.021103338 34.7 Floor 0.019861965 32.4 Floor 0.024231848 8.6 Floor 0.038263466 17.4 Floor 0.031725074 14.5 Floor 0.193428797 37.7 RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 tested together Wall 0.121469074 24.1 RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 tested together Wall 0.158685547 29.5 RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 tested together Wall 0.022946072 13.6 RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall 0.023457574 13.7 RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall 0.050117508 24.2 RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall 0.024541508 12.7 RK-7, RK-8, RK-11, RK-12 Glost tested together Wall 0.016403277 8.5 RK-7, RK-8, RK-11, RK-12 Glost tested together Wall 0.028185682 14.3 RK-7, RK-8, RK-11, RK-12 Glost tested together Wall**Kiln No Data Source**  **Run No FA** **CID Old**  **FA CID**  **Test Date** 41 2010 Survey 1 FLOR-1 123 5/25/2010 41 2010 Survey 2 FLOR-1 123 5/25/2010 41 2010 Survey 3 FLOR-1 123 5/26/2010 60, 61, 62 2010 Survey 1 DALT-1 5/13-15/2010 60, 61, 62 2010 Survey 2 DALT-1 5/13-15/2010 60, 61, 62 2010 Survey 3 DALT-1 5/13-15/2010 60 2010 Survey 1 DALT-1 5/13-15/2010 60 2010 Survey 2 DALT-1 5/13-15/2010 60 2010 Survey 3 DALT-1 5/13-15/2010 61 2010 Survey 1 DALT-1 5/13-15/2010 61 2010 Survey 2 DALT-1 5/13-15/2010 61 2010 Survey 3 DALT-1 5/13-15/2010 62 2010 Survey 1 DALT-1 5/13-15/2010 62 2010 Survey 2 DALT-1 5/13-15/2010 62 2010 Survey 3 DALT-1 5/13-15/2010 77 2010 Survey 1 MARR-2 5/4-5/10 77 2010 Survey 2 MARR-2 5/4-5/10 77 2010 Survey 3 MARR-2 5/4-5/10 36 2010 Survey 1 MARR-1 5 12/6-7/2010 36 2010 Survey 2 MARR-1 5 12/6-7/2010 36 2010 Survey 3 MARR-1 5 12/6-7/2010 84 2010 Survey 1 MARR-1 5 12/6-7/2010 84 2010 Survey 2 MARR-1 5 12/6-7/2010 84 2010 Survey 3 MARR-1 5 12/6-7/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 1 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 2 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 3 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 1 MOHA-3 50 12/15-16/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 2 MOHA-3 50 12/15-16/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 3 MOHA-3 50 12/15-16/2010**Parent Company Facility Name**  **City State** 

Florim Ceramiche S.p.A Florim USA Clarksville TN Florim Ceramiche S.p.A Florim USA Clarksville TN Florim Ceramiche S.p.A Florim USA Clarksville TN Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Dal-Tile Corp. Dal Italia Muskogee OK Monarch Ceramic Tile Monarch Florence AL Monarch Ceramic Tile Monarch Florence AL Monarch Ceramic Tile Monarch Florence AL Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX**Kiln ID Source Type**  **AP CD ID**  **AP CD Type** 

RK-1 Roller Kiln CD-1 DIFF RK-1 Roller Kiln CD-1 DIFF RK-1 Roller Kiln CD-1 DIFF RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2 Roller Kiln EPN-29 Wet Scrubber RK-2 Roller Kiln EPN-29 Wet Scrubber RK-2 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-3 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-4 Roller Kiln EPN-29 Wet Scrubber RK-2L None RK-2L None RK-2L None RK-4 Roller Kiln None RK-4 Roller Kiln None RK-4 Roller Kiln None RK-5U Roller Kiln None RK-5U Roller Kiln None RK-5U Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None RK-1, RK-2, RK-3, RK-4, RK-5, RK-6, RK-7, RK-8, RK-9, RK-10, RK-11, RK-12 Roller Kiln None**Test Methods Production**  **Rate During Test (tph)**  **Source** 1, 2, 3A, 4, 5, 23, 29, 320 5.56670 Separate declassified submittal 1, 2, 3A, 4, 5, 23, 29, 320 6.41549 Separate declassified submittal 1, 2, 3A, 4, 5, 23, 29, 320 8.07998 Separate declassified submittal 5, 29 27.30439 Separate declassified submittal. Kilns identically sized 5, 29 27.43667 Separate declassified submittal. Kilns identically sized 5, 29 26.83040 Separate declassified submittal. Kilns identically sized 5, 29 9.10146 Separate declassified submittal. Kilns identically sized 5, 29 9.14556 Separate declassified submittal. Kilns identically sized 5, 29 8.94347 Separate declassified submittal. Kilns identically sized 5, 29 9.10146 Separate declassified submittal. Kilns identically sized 5, 29 9.14556 Separate declassified submittal. Kilns identically sized 5, 29 8.94347 Separate declassified submittal. Kilns identically sized 5, 29 9.10146 Separate declassified submittal. Kilns identically sized 5, 29 9.14556 Separate declassified submittal. Kilns identically sized 5, 29 8.94347 Separate declassified submittal. Kilns identically sized 1, 2, 3, 3A, 4, 5, 29 7.99180 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.99180 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.99180 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.60599 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.69417 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.73827 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 7.03278 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 6.85641 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 6.90050 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 9.31000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 9.06000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 8.05000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 8.04000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 7.97000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 7.90000 Separate from Test Report. Kilns identically sized**Flow A ctual (acfm)** **Flow Dry Standard (dscfm)**  **Sample Volume (dscf)**  **Sample Volume**

**(dscm) Moisture (%)**  22,813 15,644 124.27 3.52 6.14 22,778 15,468 122.40 3.47 6.98 23,767 15,962 128.55 3.64 7.5 67,009 49,883 141.32 4.00 16.13 72,811 54,398 138.46 3.92 16.35 68,960 51,310 126.11 3.57 16.57 67,009 49,883 141.32 4.00 16.13 72,811 54,398 138.46 3.92 16.35 68,960 51,310 126.11 3.57 16.57 67,009 49,883 141.32 4.00 16.13 72,811 54,398 138.46 3.92 16.35 68,960 51,310 126.11 3.57 16.57 67,009 49,883 141.32 4.00 16.13 72,811 54,398 138.46 3.92 16.35 68,960 51,310 126.11 3.57 16.57 12,037 5,198 135.11 3.83 11.79 12,330 5,295 143.91 4.08 11.87 12,353 5,322 143.70 4.07 11.57 12,292 6,125 214.97 6.09 11.33 12,585 6,253 151.16 4.28 11.64 12,173 6,035 149.26 4.23 11.85 28,068 20,643 137.77 3.90 2.99 27,404 20,507 180.09 5.10 3.37 28,267 20,816 182.33 5.16 3.2 33,537 19,214 161.75 4.58 6.19 29,939 17,689 150.83 4.27 4.25 33,914 19,289 152.73 4.32 6.62 24,861 14,327 122.01 3.45 4.98 24,120 13,841 118.94 3.37 4.99 24,120 13,935 118.73 3.36 5.03**Temp Stack Gas**

**(deg F) Oxygen (%)**  **< Fraction**  **1 FH (μg) Fraction** 

**1 Status <** **Fraction**

**2B BH[HNO3**  **/H2O2] (μg)**  **Fraction**

**2 Status <** **Fraction**

**3A BH**  **[HNO3] (μg)**  265.4 19.1 0.0522ADL 25.3ADL 0.68 266.4 19.3 0.0516ADL 21.6ADL 0.599 269.2 19.3 0.0903ADL 41.6ADL 1.76 132.88 18.60 0.0408ADL 1.26ADL 0.0732 133.54 19.00 0.0285ADL 0.949ADL 0.0324 134.42 18.80 0.0258ADL 0.765ADL 0.019 132.88 18.60 0.0408ADL 1.26ADL 0.0732 133.54 19.00 0.0285ADL 0.949ADL 0.0324 134.42 18.80 0.0258ADL 0.765ADL 0.019 132.88 18.60 0.0408ADL 1.26ADL 0.0732 133.54 19.00 0.0285ADL 0.949ADL 0.0324 134.42 18.80 0.0258ADL 0.765ADL 0.019 132.88 18.60 0.0408ADL 1.26ADL 0.0732 133.54 19.00 0.0285ADL 0.949ADL 0.0324 134.42 18.80 0.0258ADL 0.765ADL 0.019 617.40 16.00< 0.015BDL 22.8ADL < 0.005 622.50 16.30< 0.015BDL 29.5ADL 1.69 622.60 16.10< 0.015BDL 22.3ADL 0.163 480.29 13.34 0.0666ADL 27.2ADL 2.4 473.38 13.05 0.11ADL 16.5ADL 0.779 473.17 13.21 0.176ADL 20.4ADL 1.16 231.79 19.3< 0.015BDL 4.22ADL 0.0495 224.54 19.27< 0.015BDL 7.85ADL 0.366 236.83 19.01< 0.015BDL 8.7ADL 0.173 298.21 16.81< 0.015BDL 7.61ADL 5.82 288.42 16.66< 0.015BDL 15.8ADL 0.258 297.92 16.69< 0.015BDL 30.9ADL 3.93 293.29 19.47< 0.015BDL 0.2ADL < 0.005 296.46 19.65< 0.015BDL 0.195ADL 0.00583 292.21 17.25< 0.015BDL 0.185ADL < 0.005**Fraction**

**3A Status** **< Fraction** 

**3B BH [KMnO4/**  **H2SO4] (μg)**  **Fraction 3B Status** **< Fraction** 

**3C BH [HCl] (μg)** **Fraction**

**3C Status Subtotal** 

**Filterable Subtotal** 

**Non Filterable**  **Total <**  **Blank Fraction**  **1 FH (μg) <**  ADL 0.63ADL 63.2ADL 0.0522 89.81 89.86< 0.015 ADL 2.43ADL 102ADL 0.0516 126.629 126.68< 0.015 ADL 6.36ADL 96.6ADL 0.0903 146.32 146.41< 0.015 ADL 9.71ADL 51.4ADL 0.0408 62.4432 62.48< 0.015< ADL 9.03ADL 41.1ADL 0.0285 51.1114 51.14< 0.015< ADL 5.1ADL 38.4ADL 0.0258 44.284 44.31< 0.015< ADL 9.71ADL 51.4ADL 0.0408 62.4432 62.48< 0.015< ADL 9.03ADL 41.1ADL 0.0285 51.1114 51.14< 0.015< ADL 5.1ADL 38.4ADL 0.0258 44.284 44.31< 0.015< ADL 9.71ADL 51.4ADL 0.0408 62.4432 62.48< 0.015< ADL 9.03ADL 41.1ADL 0.0285 51.1114 51.14< 0.015< ADL 5.1ADL 38.4ADL 0.0258 44.284 44.31< 0.015< ADL 9.71ADL 51.4ADL 0.0408 62.4432 62.48< 0.015< ADL 9.03ADL 41.1ADL 0.0285 51.1114 51.14< 0.015< ADL 5.1ADL 38.4ADL 0.0258 44.284 44.31< 0.015< BDL 65.3ADL 87.1ADL 0.015 175.205 175.22< 0.015< ADL 22.8ADL 114ADL 0.015 167.99 168.01< 0.015< ADL 10.2ADL 53.3ADL 0.015 85.963 85.98< 0.015< ADL 0.465ADL 37.7ADL 0.0666 67.765 67.83< 0.015 ADL 0.208ADL 33.4ADL 0.11 50.887 51.00< 0.015 ADL 0.737ADL 26.7ADL 0.176 48.997 49.17< 0.015 ADL 0.034ADL 14.5ADL 0.015 18.8035 18.82< 0.015 ADL 2.24ADL 31.4ADL 0.015 41.856 41.87< 0.015 ADL 0.252ADL 22.2ADL 0.015 31.325 31.34< 0.015 ADL 1.78ADL 45.9ADL 0.015 61.11 61.13< 0.015< ADL 0.262ADL 11.6ADL 0.015 27.92 27.94< 0.015< ADL 0.083ADL 36.8ADL 0.015 71.713 71.73< 0.015< BDL < 0.025BDL 0.395ADL 0.015 0.625 0.64< 0.015< ADL < 0.025BDL 0.32ADL 0.015 0.54583 0.56< 0.015< BDL < 0.025BDL 0.392ADL 0.015 0.607 0.62< 0.015<**Blank**

**Fraction 2B**  **BH[HNO3 /H2O2]**  **(μg) <**  **Blank**

**Fraction 3A**  **BH [HNO3]**  **(μg) <**  **Blank**

**Fraction 3B BH**  **[KMnO4/ H2SO4]**  **(μg) <**  **Blank**

**Fraction 3C BH**  **[HCl] (μg) Blank** 

**Fraction 1 FH (μg)**  **Blank**

**Fraction 2B**  **BH[HNO3 /H2O2]**  **(μg) Blank** 

**Fraction 3A**  **BH [HNO3]**  **(μg) Blank** 

**Fraction 3B BH**  **[KMnO4/ H2SO4]**  **(μg) Blank** 

**Fraction 3C BH**  **[HCl] (μg)** 0.2< 0.005< 0.025 0.04 0 0.2 0 0 0.04 0.2< 0.005< 0.025 0.04 0 0.2 0 0 0.04 0.2< 0.005< 0.025 0.04 0 0.2 0 0 0.04 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.0568 0 0 0 0 0.0568 0.005< 0.005< 0.025 0.111 0 0 0 0 0.111 0.005< 0.005< 0.025 0.111 0 0 0 0 0.111 0.005< 0.005< 0.025 0.111 0 0 0 0 0.111 0.113< 0.005< 0.025 0.05 0 0.113 0 0 0.05 0.113< 0.005< 0.025 0.05 0 0.113 0 0 0.05 0.113< 0.005< 0.025 0.05 0 0.113 0 0 0.05 0.113< 0.005< 0.025 0.05 0 0.113 0 0 0.05 0.113< 0.005< 0.025 0.05 0 0.113 0 0 0.05 0.113< 0.005< 0.025 0.05 0 0.113 0 0 0.05 0.005< 0.005< 0.025 0.05 0 0 0 0 0.05 0.005< 0.005< 0.025 0.05 0 0 0 0 0.05 0.005< 0.005< 0.025 0.05 0 0 0 0 0.05 0.005< 0.005< 0.025 0.05 0 0 0 0 0.05 0.005< 0.005< 0.025 0.05 0 0 0 0 0.05 0.005< 0.005< 0.025 0.05 0 0 0 0 0.05**Total**

**Blank (ug)**  **is Mfhb >**

**8.658 is Mfhb >** 

**Mfh Front Half**  **Correction is Mbhb >** 

**1 is Mbhb >** 

**Mbh Back Half**  **Correction is F3A** **b >**

**F3A F3A**  **Correction** 0.24 0.0522 25.1 0.68 0.24 0.0516 21.4 0.599 0.24 0.0903 41.4 1.76 0.0568 0.0408 1.26 0.0732 0.0568 0.0285 0.949 0.0324 0.0568 0.0258 0.765 0.019 0.0568 0.0408 1.26 0.0732 0.0568 0.0285 0.949 0.0324 0.0568 0.0258 0.765 0.019 0.0568 0.0408 1.26 0.0732 0.0568 0.0285 0.949 0.0324 0.0568 0.0258 0.765 0.019 0.0568 0.0408 1.26 0.0732 0.0568 0.0285 0.949 0.0324 0.0568 0.0258 0.765 0.019 0.111 0.015 22.8 0.005 0.111 0.015 29.5 1.69 0.111 0.015 22.3 0.163 0.163 0.0666 27.087 2.4 0.163 0.11 16.387 0.779 0.163 0.176 20.287 1.16 0.163 0.015 4.107 0.0495 0.163 0.015 7.737 0.366 0.163 0.015 8.587 0.173 0.05 0.015 7.61 5.82 0.05 0.015 15.8 0.258 0.05 0.015 30.9 3.93 0.05 0.015 0.2 0.005 0.05 0.015 0.195 0.00583 0.05 0.015 0.185 0.005**is F3Bb >**

**F3B F3B** 

**Correction is F3Cb >** 

**F3C F3C**  **Correction Run Total** 

**Blank Corrected**  **(ug) Run Total** 

**Blank Corrected**  **(ug/dscm) Run Total Blank** 

**Corrected (ug/dscm @7%O2)**  0.63 63.16 89.62 25.47 196.67 2.43 101.96 126.44 36.48 316.92 6.36 96.56 146.17 40.16 348.86 9.71 51.3432 62.43 15.60 94.28 9.03 41.0432 51.08 13.03 95.32 5.1 38.3432 44.25 12.39 82.03 9.71 51.3432 62.43 15.60 94.28 9.03 41.0432 51.08 13.03 95.32 5.1 38.3432 44.25 12.39 82.03 9.71 51.3432 62.43 15.60 94.28 9.03 41.0432 51.08 13.03 95.32 5.1 38.3432 44.25 12.39 82.03 9.71 51.3432 62.43 15.60 94.28 9.03 41.0432 51.08 13.03 95.32 5.1 38.3432 44.25 12.39 82.03 65.3 86.989 175.11 45.77 129.83 22.8 113.889 167.89 41.20 124.50 10.2 53.189 85.87 21.10 61.11 0.465 37.65 67.67 11.12 20.44 0.208 33.35 50.83 11.88 21.03 0.737 26.65 49.01 11.60 20.96 0.034 14.45 18.66 4.78 41.54 2.24 31.35 41.71 8.18 69.75 0.252 22.15 31.18 6.04 44.41 1.78 45.85 61.08 13.33 45.32 0.262 11.55 27.89 6.53 21.40 0.083 36.75 71.68 16.57 54.72 0.025 0.345 0.59 0.17 1.66 0.025 0.27 0.51 0.15 1.69 0.025 0.342 0.57 0.17 0.65**Run Total**

**Blank Corrected**  **(lb/hr) Run Total** 

**Blank Corrected**  **(lb/ton) Detection Level Notes**  **1 2B**  **3A** 1.49E-03 2.68E-04LOR: Limit of Reporting 0.015 0.005 0.005 2.11E-03 3.29E-04LOR: Limit of Reporting 0.015 0.005 0.005 2.40E-03 2.97E-04LOR: Limit of Reporting 0.015 0.005 0.005 2.91E-03 1.07E-04LOR: Limit of Reporting 0.015 0.005 0.005 2.65E-03 9.68E-05LOR: Limit of Reporting 0.015 0.005 0.005 2.38E-03 8.88E-05LOR: Limit of Reporting 0.015 0.005 0.005 9.72E-04 1.07E-04LOR: Limit of Reporting 0.015 0.005 0.005 8.85E-04 9.68E-05LOR: Limit of Reporting 0.015 0.005 0.005 7.94E-04 8.88E-05LOR: Limit of Reporting 0.015 0.005 0.005 9.72E-04 1.07E-04LOR: Limit of Reporting 0.015 0.005 0.005 8.85E-04 9.68E-05LOR: Limit of Reporting 0.015 0.005 0.005 7.94E-04 8.88E-05LOR: Limit of Reporting 0.015 0.005 0.005 9.72E-04 1.07E-04LOR: Limit of Reporting 0.015 0.005 0.005 8.85E-04 9.68E-05LOR: Limit of Reporting 0.015 0.005 0.005 7.94E-04 8.88E-05LOR: Limit of Reporting 0.015 0.005 0.005 8.91E-04 1.12E-04LOR: Limit of Reporting 0.015 0.005 0.005 8.17E-04 1.02E-04LOR: Limit of Reporting 0.015 0.005 0.005 4.21E-04 5.26E-05LOR: Limit of Reporting 0.015 0.005 0.005 2.55E-04 3.35E-05LOR: Limit of Reporting 0.015 0.005 0.005 2.78E-04 3.61E-05LOR: Limit of Reporting 0.015 0.005 0.005 2.62E-04 3.39E-05LOR: Limit of Reporting 0.015 0.005 0.005 3.70E-04 5.26E-05LOR: Limit of Reporting 0.015 0.005 0.005 6.28E-04 9.16E-05LOR: Limit of Reporting 0.015 0.005 0.005 4.71E-04 6.82E-05LOR: Limit of Reporting 0.015 0.005 0.005 9.60E-04 1.03E-04LOR: Limit of Reporting 0.015 0.005 0.005 4.33E-04 4.77E-05LOR: Limit of Reporting 0.015 0.005 0.005 1.20E-03 1.49E-04LOR: Limit of Reporting 0.015 0.005 0.005 9.16E-06 1.14E-06LOR: Limit of Reporting 0.015 0.005 0.005 7.86E-06 9.87E-07LOR: Limit of Reporting 0.015 0.005 0.005 8.88E-06 1.12E-06LOR: Limit of Reporting 0.015 0.005 0.005**3B 3C**  **Sum Lab**  **Status based on fractions**  **Overall**

**Run Status**  0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_BDL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory GroupADL_ADL_ADL_ADL_ADLADL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_ADL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_BDL_BDL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_ADL_BDL_ADLDLL 0.025 0.025 0.075ALS Laboratory Group BDL_ADL_BDL_BDL_ADLDLL**Overall Comments Ty** **pe of Tile**  Floor Floor Floor Floor Floor Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall RK-7, RK-8, RK-11, RK-12 Glost tested together Wall RK-7, RK-8, RK-11, RK-12 Glost tested together Wall RK-7, RK-8, RK-11, RK-12 Glost tested together Wall**Kiln No Data Source**  **Run No FA** **CID Old**  **FA CID**  **Test Date** 41 2010 Survey 1 FLOR-1 123 5/25/2010 41 2010 Survey 2 FLOR-1 123 5/25/2010 41 2010 Survey 3 FLOR-1 123 5/26/2010 60, 61, 62 2010 Survey 1 DALT-1 5/13-15/2010

60, 61, 62 2010 Survey 2 DALT-1 5/13-15/2010

60, 61, 62 2010 Survey 3 DALT-1 5/13-15/2010

60 2010 Survey 5/13-15/2010 60 2010 Survey 5/13-15/2010 60 2010 Survey 5/13-15/2010 61 2010 Survey 5/13-15/2010 61 2010 Survey 5/13-15/2010 61 2010 Survey 5/13-15/2010 62 2010 Survey 5/13-15/2010 62 2010 Survey 5/13-15/2010 62 2010 Survey 5/13-15/2010 77 2010 Survey 1 MARR-2 5/4-5/10 77 2010 Survey 2 MARR-2 5/4-5/10 77 2010 Survey 3 MARR-2 5/4-5/10 36 2010 Survey 1 MARR-1 5 12/6-7/2010 36 2010 Survey 2 MARR-1 5 12/6-7/2010 36 2010 Survey 3 MARR-1 5 12/6-7/2010 84 2010 Survey 1 MARR-1 5 12/6-7/2010 84 2010 Survey 2 MARR-1 5 12/6-7/2010 84 2010 Survey 3 MARR-1 5 12/6-7/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 1 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 2 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 3 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 1 MOHA-3 50 12/15-16/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 2 MOHA-3 50 12/15-16/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 3 MOHA-3 50 12/15-16/2010**Parent Company Facility Name**  **City State** 

Florim Ceramiche S.p.A Florim USA Clarksville TN Florim Ceramiche S.p.A Florim USA Clarksville TN Florim Ceramiche S.p.A Florim USA Clarksville TN Dal-Tile Corp. Dal Italia Muskogee OK

Dal-Tile Corp. Dal Italia Muskogee OK

Dal-Tile Corp. Dal Italia Muskogee OK

Monarch Ceramic Tile Monarch Florence AL Monarch Ceramic Tile Monarch Florence AL Monarch Ceramic Tile Monarch Florence AL Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX Mohawk Industries Dal-Tile El Paso Plant El Paso TX**Kiln ID Source Type**  **AP CD ID**  **AP CD Type** 

RK-1 Roller Kiln CD-1 DIFF RK-1 Roller Kiln CD-1 DIFF RK-1 Roller Kiln CD-1 DIFF RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber

RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber

RK-2, RK-3, RK-4 Roller Kiln EPN-29 Wet Scrubber

RK-2L None RK-2L None RK-2L None RK-4 Roller Kiln None RK-4 Roller Kiln None RK-4 Roller Kiln None RK-5U Roller Kiln None RK-5U Roller Kiln None RK-5U Roller Kiln None RK-1, RK-2, RK-5, RK-6 Bisque tested together Roller Kiln None RK-1, RK-2, RK-5, RK-6 Bisque tested together Roller Kiln None RK-1, RK-2, RK-5, RK-6 Bisque tested together Roller Kiln None RK-7, RK-8, RK-11, RK-12 Glost tested together Roller Kiln None RK-7, RK-8, RK-11, RK-12 Glost tested together Roller Kiln None RK-7, RK-8, RK-11, RK-12 Glost tested together Roller Kiln None**Test Methods Production**  **Rate During Test (tph)**  **Source** 1, 2, 3A, 4, 5, 23, 29, 320 5.56670 Separate declassified submittal 1, 2, 3A, 4, 5, 23, 29, 320 6.41549 Separate declassified submittal 1, 2, 3A, 4, 5, 23, 29, 320 8.07998 Separate declassified submittal 5, 29 27.30439 Separate declassified submittal. Kilns identically

sized 5, 29 27.43667 Separate declassified submittal. Kilns identically

sized 5, 29 26.83040 Separate declassified submittal. Kilns identically

sized 9.10146 9.14556 8.94347 9.10146 9.14556 8.94347 9.10146 9.14556 8.94347 1, 2, 3, 3A, 4, 5, 29 7.99180 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.99180 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.99180 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.60599 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.69417 Separate from Test Report 1, 2, 3, 3A, 4, 5, 29 7.73827 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 7.03278 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 6.85641 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 6.90050 Separate from Test Report 1, 2, 3, 3A, 4, 5, 23, 29 9.31000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 9.06000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 8.05000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 8.04000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 7.97000 Separate from Test Report. Kilns identically sized 1, 2, 3, 3A, 4, 5, 23, 29 7.90000 Separate from Test Report. Kilns identically sized**Flow A ctual (acfm)** **Flow Dry Standard (dscfm)**  **Sample Volume (dscf)**  **Sample Volume**

**(dscm) Moisture (%)**  22,813 15,644 124.27 3.52 6.14 22,778 15,468 122.40 3.47 6.98 23,767 15,962 128.55 3.64 7.5 67,009 49,883 141.32 4.00 16.13

72,811 54,398 138.46 3.92 16.35

68,960 51,310 126.11 3.57 16.57

12,037 5,198 135.11 3.83 11.79 12,330 5,295 143.91 4.08 11.87 12,353 5,322 143.70 4.07 11.57 12,292 6,125 214.97 6.09 11.33 12,585 6,253 151.16 4.28 11.64 12,173 6,035 149.26 4.23 11.85 28,068 20,643 137.77 3.90 2.99 27,404 20,507 180.09 5.10 3.37 28,267 20,816 182.33 5.16 3.2 33,537 19,214 161.75 4.58 6.19 29,939 17,689 150.83 4.27 4.25 33,914 19,289 152.73 4.32 6.62 24,861 14,327 122.01 3.45 4.98 24,120 13,841 118.94 3.37 4.99 24,120 13,935 118.73 3.36 5.03**Temp Stack Gas**

**(deg F) Oxygen (%)**  **< An** **timony Front Half ug**  **< An** **timony Back Half ug**  265.4 19.1 1.36 0.163 266.4 19.3 0.581 0.725 269.2 19.3 1.22 0.205 132.88 18.60 1.18 < 0.1 133.54 19.00 1.36 0.105 134.42 18.80 1.17 0.119

617.40 16.00 0.881 0.345 622.50 16.30 1 0.412 622.60 16.10 0.989 0.409 480.29 13.34 1.29 1.67 473.38 13.05 0.416 1.32 473.17 13.21 1.46 0.922 231.79 19.3< 0.2 0.346 224.54 19.27 0.255 0.26 236.83 19.01 0.363 0.225 298.21 16.81 0.266 0.594 288.42 16.66 0.534 0.207 297.92 16.69 0.293 0.381 293.29 19.47 0.203 0.278 296.46 19.65< 0.2 0.172 292.21 17.25 0.208 0.18**An timony Total ug** **< An** **timony Blank Front Half ug**  **< An** **timony Blank Back Half ug**  **An timony Blank** 

**Front Half ug** 1.523 < 0.2 < 0.1 0 1.306 < 0.2 < 0.1 0 1.425 < 0.2 < 0.1 0

1.28 < 0.2 < 0.1 0

1.465 < 0.2 < 0.1 0

1.289 < 0.2 < 0.1 0

1.226 < 0.2 < 0.1 0 1.412 < 0.2 < 0.1 0 1.398 < 0.2 < 0.1 0 2.96 < 0.2 < 0.1 0 1.736 < 0.2 < 0.1 0 2.382 < 0.2 < 0.1 0 0.546 < 0.2 < 0.1 0 0.515 < 0.2 < 0.1 0 0.588 < 0.2 < 0.1 0 0.86 < 0.2 < 0.1 0 0.741 < 0.2 < 0.1 0 0.674 < 0.2 < 0.1 0 0.481 < 0.2 < 0.1 0 0.372 < 0.2 < 0.1 0 0.388 < 0.2 < 0.1 0**An timony Blank** 

**Back Half ug An** **timony Total Blank ug**  **is Mfhb > 8.658 is Mfhb > Mfh**  **An timony Front**  **Half Correction** 0 0 1.36 0 0 0.581 0 0 1.22

0 0 1.18

0 0 1.36

0 0 1.17

0 0 0.881 0 0 1 0 0 0.989 0 0 1.29 0 0 0.416 0 0 1.46 0 0 0.2 0 0 0.255 0 0 0.363 0 0 0.266 0 0 0.534 0 0 0.293 0 0 0.203 0 0 0.2 0 0 0.208**is Mbhb > 1 is Mbhb > Mbh**  **An timony Back**  **Half Correction An** **timony Total**

**Blank Corrected ug An** **timony Total Blank Corrected**  **ug/dscm** 0.163 1.523 0.432793407 0.725 1.306 0.376803231 0.205 1.425 0.391483516

0.1 1.28 0.319867905

0.105 1.465 0.373647542

0.119 1.289 0.360970967

0.345 1.226 0.320439101 0.412 1.412 0.346503067 0.409 1.398 0.34357336 1.67 2.96 0.486251416 1.32 1.736 0.40557198 0.922 2.382 0.563588541 0.346 0.546 0.139957521 0.26 0.515 0.100991493 0.225 0.588 0.113889537 0.594 0.86 0.187766159 0.207 0.741 0.1735002 0.381 0.674 0.155841141 0.278 0.481 0.139223284 0.172 0.372 0.110452974 0.18 0.388 0.11540935**An timony Total** 

**Blank Corrected lb/hr**  **An timony Total** 

**Blank Corrected lb/ton**  **An timony Fraction** 

**Status An** **timony Run**

**Status An** **timony MDL**

**[other highlighted in pink] Front Half**  **ug** 2.53612E-05 4.55588E-06 ADL_ADL ADL 0.2 2.1831E-05 3.40287E-06 ADL_ADL ADL 0.2 2.34066E-05 2.89686E-06 ADL_ADL ADL 0.2

5.97663E-05 2.18889E-06 ADL_BDL DLL 0.2

7.6134E-05 2.7749E-06 ADL_ADL ADL 0.2

6.9375E-05 2.58569E-06 ADL_ADL ADL 0.2

6.23934E-06 7.80718E-07 ADL_ADL ADL 0.2 6.87212E-06 8.59897E-07 ADL_ADL ADL 0.2 6.84886E-06 8.56986E-07 ADL_ADL ADL 0.2 1.11548E-05 1.46658E-06 ADL_ADL ADL 0.2 9.49843E-06 1.2345E-06 ADL_ADL ADL 0.2 1.27396E-05 1.64631E-06 ADL_ADL ADL 0.2 1.08217E-05 1.53876E-06 BDL_ADL DLL 0.2 7.75734E-06 1.1314E-06 ADL_ADL ADL 0.2 8.87997E-06 1.28686E-06 ADL_ADL ADL 0.2 1.35135E-05 1.4515E-06 ADL_ADL ADL 0.2 1.14958E-05 1.26885E-06 ADL_ADL ADL 0.2 1.12598E-05 1.39873E-06 ADL_ADL ADL 0.2 7.47153E-06 9.29295E-07 ADL_ADL ADL 0.2 5.72632E-06 7.18484E-07 BDL_ADL DLL 0.2 6.02387E-06 7.62515E-07 ADL_ADL ADL 0.2**An timony MDL** 

**[other highlighted in pink] Back Half**  **ug <** **Ar senic Front Half**  **ug <** **Ar senic Back Half**  **ug Ar** **senic Total ug <**  0.1 1.76 6.17 7.93 < 0.1 < 1 16.9 17.9 < 0.1 1.61 12.5 14.11 <

0.1 9.37 2.23 11.6 <

0.1 8.03 1.94 9.97 <

0.1 7.52 1.95 9.47 <

0.1 6.68 44.1 50.78 < 0.1 6.16 38.6 44.76 < 0.1 5.36 30.6 35.96 < 0.1 74.8 51.1 125.9 < 0.1 48.1 29.3 77.4 < 0.1 58.2 39.5 97.7 < 0.1 1.77 25.2 26.97 < 0.1 2.95 45.9 48.85 < 0.1 3.22 35.7 38.92 < 0.1 4.42 31.8 36.22 < 0.1 2.95 8.64 11.59 < 0.1 5.11 22.8 27.91 < 0.1 3.94 4.67 8.61 < 0.1 3.06 4.42 7.48 < 0.1 4.92 3.3 8.22 <**Ar senic Blank** 

**Front Half ug <** **Ar senic Blank Back**  **Half ug Ar** **senic Blank**

**Front Half ug Ar** **senic Blank Back Half ug**  **Ar senic Total Blank**  **ug** 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0

1 < 0.2 0 0 0

1 < 0.2 0 0 0

1 < 0.2 0 0 0

1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0 1 < 0.2 0 0 0**is Mfhb > 8.658 is Mfhb > Mfh**  **Ar senic Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh** 1.76 1 1.61

9.37

8.03

7.52

6.68 6.16 5.36 74.8 48.1 58.2 1.77 2.95 3.22 4.42 2.95 5.11 3.94 3.06 4.92**Ar senic Back Half** 

**Correction Ar** **senic Total Blank**

**Corrected ug Ar** **senic Total Blank**

**Corrected ug/dscm Ar** **senic Total Blank Corrected lb/hr**  **Ar senic Total Blank** 

**Corrected lb/ton** 6.17 7.93 2.253481103 0.000132051 2.37217E-05 16.9 17.9 5.164454703 0.000299216 4.66396E-05 12.5 14.11 3.876373626 0.000231766 2.8684E-05

2.23 11.6 2.89880289 0.000541632 1.98368E-05

1.94 9.97 2.542843684 0.000518127 1.88845E-05

1.95 9.47 2.651974442 0.000509683 1.89965E-05

44.1 50.78 13.2723471 0.000258429 3.23368E-05 38.6 44.76 10.98404908 0.000217844 2.72585E-05 30.6 35.96 8.837552224 0.00017617 2.20438E-05 51.1 125.9 20.68211261 0.000474456 6.23793E-05 29.3 77.4 18.08252954 0.00042349 5.50404E-05 39.5 97.7 23.11612111 0.000522526 6.7525E-05 25.2 26.97 6.913286354 0.000534547 7.60078E-05 45.9 48.85 9.57948438 0.000735818 0.000107318 35.7 38.92 7.538402691 0.000587769 8.51777E-05 31.8 36.22 7.908011958 0.000569138 6.11319E-05 8.64 11.59 2.713721077 0.000179806 1.98461E-05 22.8 27.91 6.453303045 0.000466261 5.79206E-05 4.67 8.61 2.49212573 0.000133742 1.66346E-05 4.42 7.48 2.220936145 0.000115142 1.44469E-05 3.3 8.22 2.445012518 0.000127619 1.61543E-05**Ar senic Fraction** 

**Status Ar** **senic Run Status Ar** **senic MDL [other highlighted in pink]**  **Front Half ug Ar** **senic MDL [other**

**highlighted in pink] Back Half ug**  **< Beryllium Front**  **Half ug** ADL_ADL ADL 1 0.2 < 0.2 BDL_ADL DLL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2

ADL_ADL ADL 1 0.2 < 0.2

ADL_ADL ADL 1 0.2 < 0.2

ADL_ADL ADL 1 0.2 < 0.2

ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 0.264 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2 ADL_ADL ADL 1 0.2 < 0.2**< Beryllium Back Half**  **ug Beryllium Total ug** **< Beryllium Blank**  **Front Half ug <**  **Beryllium Blank Back Half ug** 

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

0.153 0.353 < 0.2 < 0.1 0.189 0.389 < 0.2 < 0.1 0.181 0.381 < 0.2 < 0.1 0.299 0.499 < 0.2 < 0.1 0.181 0.445 < 0.2 < 0.1 0.267 0.467 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1

< 0.1 0.3 < 0.2 < 0.1**Beryllium Blank**

**Front Half ug Beryllium Blank** 

**Back Half ug Beryllium Total**  **Blank ug is Mfhb > 8.658**  **is Mfhb > Mfh** 0 0 0 0 0 0 0 0 0

0 0 0

0 0 0

0 0 0

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0**Beryllium Front**

**Half Correction is Mbhb > 1**  **is Mbhb > Mbh Beryllium Back Half**  **Correction Beryllium Total** 

**Blank Corrected ug** 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3

0.2 0.1 0.3

0.2 0.1 0.3

0.2 0.1 0.3

0.2 0.153 0.353 0.2 0.189 0.389 0.2 0.181 0.381 0.2 0.299 0.499 0.264 0.181 0.445 0.2 0.267 0.467 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3 0.2 0.1 0.3**Beryllium Total**

**Blank Corrected ug/dscm**  **Beryllium Total**

**Blank Corrected lb/hr**  **Beryllium Total**

**Blank Corrected lb/ton**  **Beryllium Fraction**

**Status Beryllium Run** 

**Status** 0.085251492 4.99564E-06 8.97415E-07 BDL_BDL BDL 0.086555107 5.01478E-06 7.81669E-07 BDL_BDL BDL 0.082417582 4.92769E-06 6.09864E-07 BDL_BDL BDL

0.07496904 1.40077E-05 5.13021E-07 BDL_BDL BDL

0.076514855 1.55906E-05 5.68239E-07 BDL_BDL BDL

0.084011862 1.61462E-05 6.01789E-07 BDL_BDL BDL

0.092263461 1.79648E-06 2.24791E-07 BDL_ADL DLL 0.095460123 1.89324E-06 2.36898E-07 BDL_ADL DLL 0.0936348 1.86653E-06 2.33556E-07 BDL_ADL DLL 0.081972789 1.88049E-06 2.47238E-07 BDL_ADL DLL 0.103962864 2.43479E-06 3.16447E-07 ADL_ADL DLL 0.110493639 2.49764E-06 3.22765E-07 BDL_ADL DLL 0.076899737 5.94601E-06 8.45471E-07 BDL_BDL BDL 0.058829996 4.51884E-06 6.59068E-07 BDL_BDL BDL 0.058106907 4.5306E-06 6.5656E-07 BDL_BDL BDL 0.065499823 4.71401E-06 5.06338E-07 BDL_BDL BDL 0.070242996 4.65416E-06 5.13705E-07 BDL_BDL BDL 0.069365493 5.01176E-06 6.22579E-07 BDL_BDL BDL 0.086833649 4.66E-06 5.79602E-07 BDL_BDL BDL 0.089074979 4.618E-06 5.79422E-07 BDL_BDL BDL 0.089234034 4.65763E-06 5.89573E-07 BDL_BDL BDL**Beryllium MDL**

**[other highlighted in pink] Front Half**  **ug Beryllium MDL** 

**[other highlighted in pink] Back Half**  **ug <**  **Cadmium Front**

**Half ug <**  **Cadmium Back Half ug**  0.2 0.1 1.41 0.142 0.2 0.1 0.547 < 0.05 0.2 0.1 0.847 < 0.05

0.2 0.1 1.29 < 0.05

0.2 0.1 1.13 0.0563

0.2 0.1 1.33 < 0.05

0.2 0.1 1.89 0.116 0.2 0.1 3.27 0.962 0.2 0.1 3.48 0.147 0.2 0.1 18.8 0.222 0.2 0.1 5.26 12.1 0.2 0.1 23.6 < 0.05 0.2 0.1 0.611 0.117 0.2 0.1 0.638 < 0.05 0.2 0.1 0.668 0.271 0.2 0.1 2.98 0.496 0.2 0.1 2.65 < 0.05 0.2 0.1 4.33 < 0.05 0.2 0.1 0.321 < 0.05 0.2 0.1 1.16 < 0.05 0.2 0.1 0.279 < 0.05**Cadmium Total ug <**  **Cadmium Blank Front Half ug**  **< Cadmium Blank**  **Back Half ug Cadmium Blank** 

**Front Half ug** 1.552 < 0.1 < 0.05 0 0.597 < 0.1 < 0.05 0 0.897 < 0.1 < 0.05 0

1.34 < 0.1 < 0.05 0

1.1863 < 0.1 < 0.05 0

1.38 < 0.1 < 0.05 0

2.006 < 0.1 < 0.05 0 4.232 < 0.1 < 0.05 0 3.627 < 0.1 < 0.05 0 19.022 < 0.1 < 0.05 0 17.36 < 0.1 < 0.05 0 23.65 < 0.1 < 0.05 0 0.728 < 0.1 < 0.05 0 0.688 < 0.1 < 0.05 0 0.939 < 0.1 < 0.05 0 3.476 < 0.1 < 0.05 0 2.7 < 0.1 < 0.05 0 4.38 < 0.1 < 0.05 0 0.371 < 0.1 < 0.05 0 1.21 < 0.1 < 0.05 0 0.329 < 0.1 < 0.05 0**Cadmium Blank**

**Back Half ug Cadmium Total**  **Blank ug is Mfhb > 8.658**  **is Mfhb > Mfh Cadmium Front**  **Half Correction** 0 0 1.41 0 0 0.547 0 0 0.847

0 0 1.29

0 0 1.13

0 0 1.33

0 0 1.89 0 0 3.27 0 0 3.48 0 0 18.8 0 0 5.26 0 0 23.6 0 0 0.611 0 0 0.638 0 0 0.668 0 0 2.98 0 0 2.65 0 0 4.33 0 0 0.321 0 0 1.16 0 0 0.279**is Mbhb > 1 is Mbhb > Mbh**  **Cadmium Back Half Correction**  **Cadmium Total**

**Blank Corrected ug Cadmium Total**  **Blank Corrected ug/dscm**  0.142 1.552 0.441034385 0.05 0.597 0.172244662 0.05 0.897 0.246428571

0.05 1.34 0.334861713

0.0563 1.1863 0.302565242

0.05 1.38 0.386454565

0.116 2.006 0.524307371 0.962 4.232 1.038527607 0.147 3.627 0.891373802 0.222 19.022 3.124822447 12.1 17.36 4.055719803 0.05 23.65 5.59566289 0.117 0.728 0.186610028 0.05 0.688 0.134916791 0.271 0.939 0.181874618 0.496 3.476 0.758924615 0.05 2.7 0.632186964 0.05 4.38 1.0127362 0.05 0.371 0.107384279 0.05 1.21 0.359269082 0.05 0.329 0.09785999**Cadmium Total**

**Blank Corrected lb/hr**  **Cadmium Total**

**Blank Corrected lb/ton**  **Cadmium Fraction**

**Status Cadmium Run** 

**Status Cadmium MDL** 

**[other highlighted in pink] Front Half**  **ug** 2.58441E-05 4.64263E-06 ADL_ADL ADL 0.1 9.97942E-06 1.55552E-06 ADL_BDL DLL 0.1 1.47338E-05 1.82349E-06 ADL_BDL DLL 0.1

6.25678E-05 2.29149E-06 ADL_BDL DLL 0.1

6.16504E-05 2.24701E-06 ADL_ADL ADL 0.1

7.42727E-05 2.76823E-06 ADL_BDL DLL 0.1

1.02089E-05 1.27742E-06 ADL_ADL ADL 0.1 2.05969E-05 2.57725E-06 ADL_ADL ADL 0.1 1.77688E-05 2.22338E-06 ADL_ADL ADL 0.1 7.16847E-05 9.42477E-06 ADL_ADL ADL 0.1 9.49843E-05 1.2345E-05 ADL_ADL ADL 0.1 0.000126487 1.63456E-05 ADL_BDL DLL 0.1 1.4429E-05 2.05168E-06 ADL_ADL ADL 0.1 1.03632E-05 1.51146E-06 ADL_BDL DLL 0.1 1.41808E-05 2.05503E-06 ADL_ADL ADL 0.1 5.46197E-05 5.86677E-06 ADL_ADL ADL 0.1 4.18875E-05 4.62334E-06 ADL_BDL DLL 0.1 7.31717E-05 9.08965E-06 ADL_BDL DLL 0.1 5.76287E-06 7.16774E-07 ADL_BDL DLL 0.1 1.86259E-05 2.337E-06 ADL_BDL DLL 0.1 5.10787E-06 6.46565E-07 ADL_BDL DLL 0.1**Cadmium MDL**

**[other highlighted in pink] Back Half**  **ug <**  **Chromium Front**

**Half ug <**  **Chromium Back Half ug**  **Chromium Total ug <**  0.05 20.7 1.79 22.49 0.05 15.4 3.64 19.04 0.05 27.2 10.9 38.1

0.05 172 0.634 172.634 <

0.05 178 1.31 179.31 <

0.05 211 0.424 211.424 <

0.05 130 4.29 134.29 < 0.05 105 3.36 108.36 < 0.05 485 2 487 < 0.05 112 4.27 116.27 0.05 66.1 3.9 70 0.05 114 2.94 116.94 0.05 31.9 1.18 33.08 0.05 46.1 2.12 48.22 0.05 44.3 2.17 46.47 0.05 84.3 11.3 95.6 < 0.05 253 4.95 257.95 < 0.05 55.8 4.08 59.88 < 0.05 62 7.49 69.49 < 0.05 11.1 6.84 17.94 < 0.05 30.7 1.86 32.56 <**Chromium Blank**

**Front Half ug <**  **Chromium Blank Back Half ug**  **Chromium Blank**

**Front Half ug Chromium Blank** 

**Back Half ug Chromium Total**  **Blank ug** 1.05 0.488 1.05 0.488 1.538 1.05 0.488 1.05 0.488 1.538 1.05 0.488 1.05 0.488 1.538

1 0.382 0 0.382 0.382

1 0.382 0 0.382 0.382

1 0.382 0 0.382 0.382

1 0.641 0 0.641 0.641 1 0.641 0 0.641 0.641 1 0.641 0 0.641 0.641 2.12 < 0.15 2.12 0 2.12 2.12 < 0.15 2.12 0 2.12 2.12 < 0.15 2.12 0 2.12 2.12 < 0.15 2.12 0 2.12 2.12 < 0.15 2.12 0 2.12 2.12 < 0.15 2.12 0 2.12 1 0.853 0 0.853 0.853 1 0.853 0 0.853 0.853 1 0.853 0 0.853 0.853 1 0.853 0 0.853 0.853 1 0.853 0 0.853 0.853 1 0.853 0 0.853 0.853**is Mfhb > 8.658 is Mfhb > Mfh**  **Chromium Front Half Correction**  **is Mbhb > 1 is Mbhb > Mbh**  19.65 14.35 26.15

172

178

211

130 105 485 109.88 63.98 111.88 29.78 43.98 42.18 84.3 253 55.8 62 11.1 30.7**Chromium Back**

**Half Correction Chromium Total** 

**Blank Corrected ug Chromium Total**  **Blank Corrected ug/dscm**  **Chromium Total**

**Blank Corrected lb/hr**  **Chromium Total**

**Blank Corrected lb/ton**  1.302 20.952 5.953964194 0.000348896 6.26755E-05 3.152 17.502 5.049624928 0.000292563 4.56026E-05 10.412 36.562 10.04450549 0.000600555 7.43262E-05

0.252 172.252 43.04522375 0.008042861 0.000294563

0.928 178.928 45.63549996 0.009298638 0.000338913

0.042 211.042 59.10010457 0.011358448 0.000423342

3.649 133.649 34.93178254 0.000680165 8.51078E-05 2.719 107.719 26.43411043 0.000524262 6.56E-05 1.359 486.359 119.5278938 0.002382693 0.000298142 4.27 114.15 18.75189162 0.000430176 5.65575E-05 3.9 67.88 15.85842513 0.000371402 4.82705E-05 2.94 114.82 27.16676588 0.000614089 7.93574E-05 1.18 30.96 7.936052856 0.000613629 8.72526E-05 2.12 46.1 9.040209414 0.000694395 0.000101277 2.17 44.35 8.590137701 0.000669773 9.70615E-05 10.447 94.747 20.68637242 0.001488795 0.000159913 4.097 257.097 60.1975451 0.003988571 0.00044024 3.227 59.027 13.64812321 0.000986097 0.000122497 6.637 68.637 19.86667059 0.001066161 0.000132607 5.987 17.087 5.073413893 0.000263026 3.3002E-05 1.007 31.707 9.431145003 0.000492265 6.2312E-05**Chromium Fraction**

**Status Chromium Run** 

**Status Chromium MDL** 

**[other highlighted in pink] Front Half**  **ug Chromium MDL** 

**[other highlighted in pink] Back Half**  **ug <**  **Cobalt Front Half ug**  ADL_ADL ADL 1 0.15 0.342 ADL_ADL ADL 1 0.15 0.203 ADL_ADL ADL 1 0.15 0.315

ADL_ADL ADL 1 0.15 0.373

ADL_ADL ADL 1 0.15 0.453

ADL_ADL ADL 1 0.15 0.947

ADL_ADL ADL 1 0.15 0.214 ADL_ADL ADL 1 0.15 0.288 ADL_ADL ADL 1 0.15 3.85 ADL_ADL ADL 1 0.15 0.604 ADL_ADL ADL 1 0.15 0.299 ADL_ADL ADL 1 0.15 0.296 ADL_ADL ADL 1 0.15 < 0.2 ADL_ADL ADL 1 0.15 < 0.2 ADL_ADL ADL 1 0.15 < 0.2 ADL_ADL ADL 1 0.15 0.205 ADL_ADL ADL 1 0.15 0.695 ADL_ADL ADL 1 0.15 0.362 ADL_ADL ADL 1 0.15 0.409 ADL_ADL ADL 1 0.15 < 0.2 ADL_ADL ADL 1 0.15 < 0.2**< Cobalt Back Half**  **ug Cobalt Total ug**  **< Cobalt Blank Front**  **Half ug <** **Cobalt Blank Back Half ug**  0.168 0.51 < 0.2 < 0.1 0.778 0.981 < 0.2 < 0.1 0.531 0.846 < 0.2 < 0.1

0.106 0.479 < 0.2 < 0.1

< 0.1 0.553 < 0.2 < 0.1

< 0.1 1.047 < 0.2 < 0.1

1.05 1.264 < 0.2 < 0.1 0.373 0.661 < 0.2 < 0.1 0.576 4.426 < 0.2 < 0.1 1.64 2.244 < 0.2 < 0.1 1.8 2.099 < 0.2 < 0.1 0.449 0.745 < 0.2 < 0.1 0.261 0.461 < 0.2 < 0.1 0.21 0.41 < 0.2 < 0.1 0.266 0.466 < 0.2 < 0.1 1.45 1.655 < 0.2 < 0.1 0.217 0.912 < 0.2 < 0.1 0.522 0.884 < 0.2 < 0.1 0.32 0.729 < 0.2 < 0.1 0.472 0.672 < 0.2 < 0.1 0.168 0.368 < 0.2 < 0.1**Cobalt Blank Front**

**Half ug Cobalt Blank Back** 

**Half ug Cobalt Total Blank**  **ug is Mfhb > 8.658**  **is Mfhb > Mfh** 0 0 0 0 0 0 0 0 0

0 0 0

0 0 0

0 0 0

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0**Cobalt Front Half**

**Correction is Mbhb > 1**  **is Mbhb > Mbh Cobalt Back Half**  **Correction Cobalt Total Blank** 

**Corrected ug** 0.342 0.168 0.51 0.203 0.778 0.981 0.315 0.531 0.846

0.373 0.106 0.479

0.453 0.1 0.553

0.947 0.1 1.047

0.214 1.05 1.264 0.288 0.373 0.661 3.85 0.576 4.426 0.604 1.64 2.244 0.299 1.8 2.099 0.296 0.449 0.745 0.2 0.261 0.461 0.2 0.21 0.41 0.2 0.266 0.466 0.205 1.45 1.655 0.695 0.217 0.912 0.362 0.522 0.884 0.409 0.32 0.729 0.2 0.472 0.672 0.2 0.168 0.368**Cobalt Total Blank**

**Corrected ug/dscm Cobalt Total Blank**  **Corrected lb/hr Cobalt Total Blank** 

**Corrected lb/ton Cobalt Fraction**  **Status Cobalt Run Status**  0.144927536 8.49259E-06 1.52561E-06 ADL_ADL ADL 0.283035199 1.63983E-05 2.55606E-06 ADL_ADL ADL 0.232417582 1.38961E-05 1.71982E-06 ADL_ADL ADL

0.119700568 2.23657E-05 8.19123E-07 ADL_ADL ADL

0.141042383 2.87386E-05 1.04745E-06 ADL_BDL DLL

0.293201398 5.63504E-05 2.10024E-06 ADL_BDL DLL

0.330371145 6.43273E-06 8.04917E-07 ADL_ADL ADL 0.162208589 3.21705E-06 4.02544E-07 ADL_ADL ADL 1.087736545 2.16832E-05 2.71318E-06 ADL_ADL ADL 0.368631141 8.45655E-06 1.11183E-06 ADL_ADL ADL 0.490377642 1.14846E-05 1.49263E-06 ADL_ADL ADL 0.176269296 3.98446E-06 5.14904E-07 ADL_ADL ADL 0.118169262 9.13704E-06 1.29921E-06 BDL_ADL DLL 0.080400995 6.17575E-06 9.00726E-07 BDL_ADL DLL 0.090259395 7.03753E-06 1.01986E-06 BDL_ADL DLL 0.36134069 2.60056E-05 2.7933E-06 ADL_ADL ADL 0.213538708 1.41487E-05 1.56166E-06 ADL_ADL ADL 0.204396986 1.4768E-05 1.83453E-06 ADL_ADL ADL 0.211005767 1.13238E-05 1.40843E-06 ADL_ADL ADL 0.199527953 1.03443E-05 1.29791E-06 BDL_ADL DLL 0.109460414 5.71336E-06 7.2321E-07 BDL_ADL DLL**Cobalt MDL [other**

**highlighted in pink] Front Half ug**  **Cobalt MDL [other**

**highlighted in pink] Back Half ug**  **< Lead Front Half ug** **< Lead Back Half ug**  0.2 0.1 6.75 0.919 0.2 0.1 4.44 2.44 0.2 0.1 14.2 0.893

0.2 0.1 129 0.608

0.2 0.1 115 0.446

0.2 0.1 83.6 0.844

0.2 0.1 59.6 6.63 0.2 0.1 53.5 4.46 0.2 0.1 56.1 4.61 0.2 0.1 227 13.3 0.2 0.1 73.2 11.4 0.2 0.1 277 10.7 0.2 0.1 20.8 1.37 0.2 0.1 25.3 0.687 0.2 0.1 24.6 1.28 0.2 0.1 7.3 3.45 0.2 0.1 4.63 1.13 0.2 0.1 10.4 1.89 0.2 0.1 6.88 1.7 0.2 0.1 6.29 1.64 0.2 0.1 6.29 0.969**Lead Total ug <**  **Lead Blank Front Half ug**  **< Lead Blank Back**  **Half ug Lead Blank Front** 

**Half ug** 7.669 < 0.5 0.12 0 6.88 < 0.5 0.12 0 15.093 < 0.5 0.12 0

129.608 < 0.5 0.192 0

115.446 < 0.5 0.192 0

84.444 < 0.5 0.192 0

66.23 < 0.5 0.206 0 57.96 < 0.5 0.206 0 60.71 < 0.5 0.206 0 240.3 < 0.5 0.0947 0 84.6 < 0.5 0.0947 0 287.7 < 0.5 0.0947 0 22.17 < 0.5 0.0947 0 25.987 < 0.5 0.0947 0 25.88 < 0.5 0.0947 0 10.75 < 0.5 0.0748 0 5.76 < 0.5 0.0748 0 12.29 < 0.5 0.0748 0 8.58 < 0.5 0.0748 0 7.93 < 0.5 0.0748 0 7.259 < 0.5 0.0748 0**Lead Blank Back**

**Half ug Lead Total Blank**  **ug is Mfhb > 8.658**  **is Mfhb > Mfh Lead Front Half**  **Correction** 0.12 0.12 6.75 0.12 0.12 4.44 0.12 0.12 14.2

0.192 0.192 129

0.192 0.192 115

0.192 0.192 83.6

0.206 0.206 59.6 0.206 0.206 53.5 0.206 0.206 56.1 0.0947 0.0947 227 0.0947 0.0947 73.2 0.0947 0.0947 277 0.0947 0.0947 20.8 0.0947 0.0947 25.3 0.0947 0.0947 24.6 0.0748 0.0748 7.3 0.0748 0.0748 4.63 0.0748 0.0748 10.4 0.0748 0.0748 6.88 0.0748 0.0748 6.29 0.0748 0.0748 6.29**is Mbhb > 1 is Mbhb > Mbh**  **Lead Back Half Correction**  **Lead Total Blank**

**Corrected ug Lead Total Blank** 

**Corrected ug/dscm** 0.799 7.549 2.145211708 2.32 6.76 1.950375072 0.773 14.973 4.113461538

0.416 129.416 32.34064439

0.254 115.254 29.39547702

0.652 84.252 23.59389131

6.424 66.024 17.25666492 4.254 57.754 14.17276074 4.404 60.504 14.86950111 13.2053 240.2053 39.459516 11.3053 84.5053 19.74250108 10.6053 287.6053 68.04830038 1.2753 22.0753 5.658615879 0.5923 25.8923 5.077479701 1.1853 25.7853 4.994346734 3.3752 10.6752 2.3307457 1.0552 5.6852 1.331151602 1.8152 12.2152 2.824377906 1.6252 8.5052 2.461791842 1.5652 7.8552 2.332339253 0.8942 7.1842 2.136917145**Lead Total Blank**

**Corrected lb/hr Lead Total Blank** 

**Corrected lb/ton Lead Fraction**  **Status Lead Run Status**  **Lead MDL [other highlighted in pink]**  **Front Half ug** 0.000125707 2.2582E-05 ADL_ADL ADL 0.5 0.000113 1.76136E-05 ADL_ADL ADL 0.5 0.000245941 3.04383E-05 ADL_ADL ADL 0.5

0.006042745 0.00022131 ADL_ADL ADL 0.5

0.005989589 0.000218306 ADL_ADL ADL 0.5

0.004534509 0.000169006 ADL_ADL ADL 0.5

0.000336008 4.20442E-05 ADL_ADL ADL 0.5 0.000281085 3.51717E-05 ADL_ADL ADL 0.5 0.000296412 3.70895E-05 ADL_ADL ADL 0.5 0.000905217 0.000119014 ADL_ADL ADL 0.5 0.000462366 6.00931E-05 ADL_ADL ADL 0.5 0.001538192 0.000198777 ADL_ADL ADL 0.5 0.000437534 6.22134E-05 ADL_ADL ADL 0.5 0.000390011 5.68826E-05 ADL_ADL ADL 0.5 0.000389409 5.6432E-05 ADL_ADL ADL 0.5 0.000167743 1.80175E-05 ADL_ADL ADL 0.5 8.81995E-05 9.73504E-06 ADL_ADL ADL 0.5 0.000204066 2.53498E-05 ADL_ADL ADL 0.5 0.000132114 1.64321E-05 ADL_ADL ADL 0.5 0.000120918 1.51716E-05 ADL_ADL ADL 0.5 0.000111538 1.41187E-05 ADL_ADL ADL 0.5**Lead MDL [other**

**highlighted in pink] Back Half ug**  **< Ma** **nganese Front Half ug**  **< Ma** **nganese Back Half ug**  **Ma nganese Total**  **ug <**  0.05 3.61 7.44 11.05 0.05 4.3 31.1 35.4 0.05 3.17 29.4 32.57

0.05 2.28 14 16.28

0.05 2.19 33.7 35.89

0.05 2.37 126 128.37

0.05 0.863 28.6 29.463 < 0.05 2.15 25 27.15 < 0.05 36 25.3 61.3 < 0.05 15.1 30.1 45.2 0.05 8.01 99.9 107.91 0.05 6.89 25.5 32.39 0.05 4.68 3.56 8.24 0.05 1.87 2.94 4.81 0.05 2.19 3.08 5.27 0.05 3.17 18.1 21.27 0.05 5.21 10.7 15.91 0.05 7.56 9.01 16.57 0.05 5.4 9.99 15.39 0.05 1.87 32.6 34.47 0.05 3.54 7.01 10.55**Ma nganese Blank** 

**Front Half ug <**  **Ma nganese Blank**  **Back Half ug Ma** **nganese Blank**

**Front Half ug Ma** **nganese Blank**

**Back Half ug Ma** **nganese Total Blank ug**  0.93 0.45 0.93 0.45 1.38 0.93 0.45 0.93 0.45 1.38 0.93 0.45 0.93 0.45 1.38

0.62 1.28 0.62 1.28 1.9

0.62 1.28 0.62 1.28 1.9

0.62 1.28 0.62 1.28 1.9

0.5 0.509 0 0.509 0.509 0.5 0.509 0 0.509 0.509 0.5 0.509 0 0.509 0.509 1.16 0.438 1.16 0.438 1.598 1.16 0.438 1.16 0.438 1.598 1.16 0.438 1.16 0.438 1.598 1.16 0.438 1.16 0.438 1.598 1.16 0.438 1.16 0.438 1.598 1.16 0.438 1.16 0.438 1.598 1.52 1.59 1.52 1.59 3.11 1.52 1.59 1.52 1.59 3.11 1.52 1.59 1.52 1.59 3.11 1.52 1.59 1.52 1.59 3.11 1.52 1.59 1.52 1.59 3.11 1.52 1.59 1.52 1.59 3.11**is Mfhb > 8.658 is Mfhb > Mfh**  **Ma nganese Front**  **Half Correction is Mbhb > 1**  **is Mbhb > Mbh** 2.68 3.37 2.24

1.66 Yes

1.57 Yes

1.75 Yes

0.863 2.15 36 13.94 6.85 5.73 3.52 0.71 1.03 1.65 Yes 3.69 Yes 6.04 Yes 3.88 Yes 0.35 Yes 2.02 Yes**II: lesser of Mbhb**

**or 5% of Mbh greater of I or II**  **Ma nganese Back**  **Half Correction MN Contamination** 

**Check: Ratio of BH/FH**  **Remove Run** 6.99 2.06 no 30.65 7.23 yes 28.95 9.27 yes

0.7 1 13 6.14 yes

1.28 1.28 32.42 15.39 yes

1.28 1.28 124.72 53.16 yes

28.091 33.14 yes 24.491 11.63 yes 24.791 0.70 no 29.662 1.99 no 99.462 12.47 yes 25.062 3.70 no 3.122 0.76 no 2.502 1.57 no 2.642 1.41 no 0.905 1 17.1 5.71 yes 0.535 1 9.7 2.05 no 0.4505 1 8.01 1.19 no 0.4995 1 8.99 1.85 no 1.59 1.59 31.01 17.43 yes 0.3505 1 6.01 1.98 no**Ma nganese Total** 

**Blank Corrected ug Ma** **nganese Total Blank Corrected**  **ug/dscm Ma** **nganese Total**

**Blank Corrected lb/hr**  **Ma nganese Total** 

**Blank Corrected lb/ton**  **Ma nganese** 

**Fraction Status** 9.67 2.747939756 0.000161026 2.89267E-05 ADL_ADL 34.02 31.19

14.66

33.99

126.47

28.954 26.641 60.791 14.94003441 0.000297818 3.72654E-05 ADL_ADL 43.602 7.162680493 0.000164315 2.16033E-05 ADL_ADL 106.312 30.792 7.285482101 0.000164684 2.12818E-05 ADL_ADL 6.642 1.702560177 0.000131645 1.87187E-05 ADL_ADL 3.212 0.629873159 4.83817E-05 7.05642E-06 ADL_ADL 3.672 0.711228538 5.54545E-05 8.0363E-06 ADL_ADL 18.75 13.39 3.135179052 0.000207731 2.29283E-05 ADL_ADL 14.05 3.248617262 0.000234717 2.91574E-05 ADL_ADL 12.87 3.725163548 0.000199914 2.48649E-05 ADL_ADL 31.36 8.03 2.388497631 0.000124669 1.57809E-05 ADL_ADL**Ma nganese Run** 

**Status Ma** **nganese MDL**

**[other highlighted in pink] Front Half**  **ug Ma** **nganese MDL**

**[other highlighted in pink] Back Half**  **ug <**  **Nickel Front Half ug**  **<** ADL 0.5 0.15 1.97 0.5 0.15 1.42 0.5 0.15 1.72

0.5 0.15 2.54

0.5 0.15 1.46

0.5 0.15 2.47

0.5 0.15 1.12 0.5 0.15 1.09 ADL 0.5 0.15 181 ADL 0.5 0.15 6.83 0.5 0.15 5.23 ADL 0.5 0.15 3.48 ADL 0.5 0.15 5.26 ADL 0.5 0.15 2.58 ADL 0.5 0.15 3.39 0.5 0.15 12.8 ADL 0.5 0.15 41.5 ADL 0.5 0.15 23.1 ADL 0.5 0.15 32.8 0.5 0.15 3.43 ADL 0.5 0.15 8.65**Nickel Back Half ug Nickel Total ug**  **< Nickel Blank Front**  **Half ug <** **Nickel Blank Back Half ug**  3.34 5.31 0.83 0.185 1.34 2.76 0.83 0.185 5.7 7.42 0.83 0.185

0.968 3.508 0.429 0.615

1.19 2.65 0.429 0.615

0.901 3.371 0.429 0.615

2.76 3.88 0.51 0.687 2.86 3.95 0.51 0.687 1.88 182.88 0.51 0.687 2.72 9.55 1.45 0.231 2.84 8.07 1.45 0.231 2.1 5.58 1.45 0.231 1.5 6.76 1.45 0.231 1.48 4.06 1.45 0.231 1.33 4.72 1.45 0.231 4.78 17.58 0.636 0.709 2.16 43.66 0.636 0.709 3.83 26.93 0.636 0.709 2.93 35.73 0.636 0.709 2.64 6.07 0.636 0.709 1.69 10.34 0.636 0.709**Nickel Blank Front**

**Half ug Nickel Blank Back** 

**Half ug Nickel Total Blank**  **ug is Mfhb > 8.658**  **is Mfhb > Mfh** 0.83 0.185 1.015 0.83 0.185 1.015 0.83 0.185 1.015

0.429 0.615 1.044

0.429 0.615 1.044

0.429 0.615 1.044

0.51 0.687 1.197 0.51 0.687 1.197 0.51 0.687 1.197 1.45 0.231 1.681 1.45 0.231 1.681 1.45 0.231 1.681 1.45 0.231 1.681 1.45 0.231 1.681 1.45 0.231 1.681 0.636 0.709 1.345 0.636 0.709 1.345 0.636 0.709 1.345 0.636 0.709 1.345 0.636 0.709 1.345 0.636 0.709 1.345**Nickel Front Half**

**Correction is Mbhb > 1**  **is Mbhb > Mbh Nickel Back Half**  **Correction Nickel Total Blank** 

**Corrected ug** 1.14 3.155 4.295 0.59 1.155 1.745 0.89 5.515 6.405

2.111 0.353 2.464

1.031 0.575 1.606

2.041 0.286 2.327

0.61 2.073 2.683 0.58 2.173 2.753 180.49 1.193 181.683 5.38 2.489 7.869 3.78 2.609 6.389 2.03 1.869 3.899 3.81 1.269 5.079 1.13 1.249 2.379 1.94 1.099 3.039 12.164 4.071 16.235 40.864 1.451 42.315 22.464 3.121 25.585 32.164 2.221 34.385 2.794 1.931 4.725 8.014 0.981 8.995**Nickel Total Blank**

**Corrected ug/dscm Nickel Total Blank**  **Corrected lb/hr Nickel Total Blank** 

**Corrected lb/ton Nickel Fraction**  **Status Nickel Run Status**  1.220517192 7.15209E-05 1.2848E-05 ADL_ADL ADL 0.503462204 2.91693E-05 4.54671E-06 ADL_ADL ADL 1.759615385 0.000105206 1.30206E-05 ADL_ADL ADL

0.615745717 0.00011505 4.21361E-06 ADL_ADL ADL

0.409609524 8.34616E-05 3.04197E-06 ADL_ADL ADL

0.651652009 0.000125241 4.66788E-06 ADL_ADL ADL

0.701254574 1.36543E-05 1.70854E-06 ADL_ADL ADL 0.675582822 1.33987E-05 1.67655E-06 ADL_ADL ADL 44.65052839 0.000890072 0.000111373 ADL_ADL ADL 1.292673107 2.96544E-05 3.89883E-06 ADL_ADL ADL 1.492626372 3.49571E-05 4.54332E-06 ADL_ADL ADL 0.922515417 2.08529E-05 2.69478E-06 ADL_ADL ADL 1.301912547 0.000100666 1.43138E-05 ADL_ADL ADL 0.46652187 3.58344E-05 5.22641E-06 ADL_ADL ADL 0.588622964 4.58949E-05 6.65096E-06 ADL_ADL ADL 3.544632086 0.000255107 2.74013E-05 ADL_ADL ADL 9.907774578 0.00065647 7.2458E-05 ADL_ADL ADL 5.915720473 0.00042742 5.30956E-05 ADL_ADL ADL 9.952583418 0.000534114 6.6432E-05 ADL_ADL ADL 1.402930921 7.27334E-05 9.1259E-06 ADL_ADL ADL 2.675533772 0.000139651 1.76774E-05 ADL_ADL ADL**Nickel MDL [other**

**highlighted in pink] Front Half ug**  **Nickel MDL [other**

**highlighted in pink] Back Half ug**  **< Selenium Front**  **Half ug <** **Selenium Back Half ug**  0.2 0.1 8.42 32.2 0.2 0.1 5.23 54.4 0.2 0.1 8.23 70.4

0.2 0.1 68.9 36.9

0.2 0.1 59.8 32.9

0.2 0.1 40.6 30.6

0.2 0.1 4.22 394 0.2 0.1 3.7 405 0.2 0.1 3.95 325 0.2 0.1 43.9 1710 0.2 0.1 32 1100 0.2 0.1 107 1570 0.2 0.1 28.7 904 0.2 0.1 67.3 1580 0.2 0.1 79.3 1340 0.2 0.1 29.6 395 0.2 0.1 18.2 81.3 0.2 0.1 40.4 219 0.2 0.1 6.64 19.1 0.2 0.1 < 2 10.7 0.2 0.1 3.59 13.4**Selenium Total ug <**  **Selenium Blank Front Half ug**  **< Selenium Blank**  **Back Half ug Selenium Blank** 

**Front Half ug** 40.62 < 2 < 1 0 59.63 < 2 < 1 0 78.63 < 2 < 1 0

105.8 < 2 < 1 0

92.7 < 2 < 1 0

71.2 < 2 < 1 0

398.22 < 2 < 1 0 408.7 < 2 < 1 0 328.95 < 2 < 1 0 1753.9 < 2 < 1 0 1132 < 2 < 1 0 1677 < 2 < 1 0 932.7 < 2 < 1 0 1647.3 < 2 < 1 0 1419.3 < 2 < 1 0 424.6 < 2 < 1 0 99.5 < 2 < 1 0 259.4 < 2 < 1 0 25.74 < 2 < 1 0 12.7 < 2 < 1 0 16.99 < 2 < 1 0**Selenium Blank**

**Back Half ug Selenium Total**  **Blank ug is Mfhb > 8.658**  **is Mfhb > Mfh Selenium Front**  **Half Correction** 0 0 8.42 0 0 5.23 0 0 8.23

0 0 68.9

0 0 59.8

0 0 40.6

0 0 4.22 0 0 3.7 0 0 3.95 0 0 43.9 0 0 32 0 0 107 0 0 28.7 0 0 67.3 0 0 79.3 0 0 29.6 0 0 18.2 0 0 40.4 0 0 6.64 0 0 2 0 0 3.59**is Mbhb > 1 is Mbhb > Mbh**  **Selenium Back Half Correction**  **Selenium Total**

**Blank Corrected ug Selenium Total**  **Blank Corrected ug/dscm**  32.2 40.62 11.543052 54.4 59.63 17.20427005 70.4 78.63 21.60164835

36.9 105.8 26.43908154

32.9 92.7 23.64309022

30.6 71.2 19.93881524

394 398.22 104.0825928 405 408.7 100.2944785 325 328.95 80.84295896 1710 1753.9 288.1203916 1100 1132 264.4628351 1570 1677 396.7833685 904 932.7 239.0812823 1580 1647.3 323.0355091 1340 1419.3 274.9037754 395 424.6 92.70408276 81.3 99.5 23.29726032 219 259.4 59.97802974 19.1 25.74 7.450327096 10.7 12.7 3.770840782 13.4 16.99 5.053620765**Selenium Total**

**Blank Corrected lb/hr**  **Selenium Total**

**Blank Corrected lb/ton**  **Selenium Fraction**

**Status Selenium Run** 

**Status Selenium MDL** 

**[other highlighted in pink] Front Half**  **ug** 0.00067641 0.00012151 ADL_ADL ADL 2 0.000996772 0.00015537 ADL_ADL ADL 2 0.001291549 0.000159845 ADL_ADL ADL 2

0.004940057 0.000180925 ADL_ADL ADL 2

0.004817489 0.000175586 ADL_ADL ADL 2

0.00383204 0.000142825 ADL_ADL ADL 2

0.002026616 0.000253587 ADL_ADL ADL 2 0.001989119 0.000248895 ADL_ADL ADL 2 0.00161154 0.000201649 ADL_ADL ADL 2 0.006609598 0.000868999 ADL_ADL ADL 2 0.00619368 0.000804983 ADL_ADL ADL 2 0.008969056 0.001159052 ADL_ADL ADL 2 0.018486159 0.00262857 ADL_ADL ADL 2 0.024812959 0.003618942 ADL_ADL ADL 2 0.021434255 0.003106186 ADL_ADL ADL 2 0.006671897 0.000716638 ADL_ADL ADL 2 0.001543631 0.000170379 ADL_ADL ADL 2 0.004333503 0.000538323 ADL_ADL ADL 2 0.000399828 4.97298E-05 ADL_ADL ADL 2 0.000195495 2.45289E-05 BDL_ADL DLL 2 0.000263777 3.33895E-05 ADL_ADL ADL 2**Selenium MDL**

**[other highlighted in pink] Back Half**  **ug Comments**  Laboratory Analy tical Method Lab Method Listed in

PWMemo 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA

1 Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA

1 Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA

1 Under normal operations, Wet Scrubber #1 controls emissions from Kilns 1 & 2 and Wet Scrubber #2 controls emissions from Kilns 3 & 4. Wet Scrubber #2 was designed to also control emissions from Kilns 2, 3, & 4 in the event of a malfunction of Wet Scrubber #1. ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA

1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 ALS Laboratory GroupICP-MS Method 29 ICP/MS or GFAA 1 RK-1, RK-2, RK-5, RK-6 Bisque tested together ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA 1 RK-1, RK-2, RK-5, RK-6 Bisque tested together ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA 1 RK-1, RK-2, RK-5, RK-6 Bisque tested together ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA 1 RK-7, RK-8, RK-11, RK-12 Glost tested together ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA 1 RK-7, RK-8, RK-11, RK-12 Glost tested together ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAA 1 RK-7, RK-8, RK-11, RK-12 Glost tested together ALS Laboratory

GroupICP-MS Method 29 ICP/MS or GFAAType of

Tile Floor Floor Floor

Floor

Floor

Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Floor Wall Wall Wall Wall Wall Wall**Kiln No Data Source**  **Run No FA** **CID Old**  **FA CID**  **Test Date** 41 2010 Survey 1 FLOR-1 123 5/25/2010 41 2010 Survey 2 FLOR-1 123 5/25/2010 41 2010 Survey 3 FLOR-1 123 5/26/2010 41 2010 Survey 1 FLOR-1 123 10/11-12/2010 41 2010 Survey 2 FLOR-1 123 10/11-12/2010 41 2010 Survey 3 FLOR-1 123 10/11-12/2010 60, 61, 62 2010 Survey 1 DALT-1 5/13/2010 60, 61, 62 2010 Survey 2 DALT-1 5/13/2010 60, 61, 62 2010 Survey 3 DALT-1 5/13/2010 60 2010 Survey 1 DALT-1 5/13/2010 60 2010 Survey 2 DALT-1 5/13/2010 60 2010 Survey 3 DALT-1 5/13/2010 61 2010 Survey 1 DALT-1 5/13/2010 61 2010 Survey 2 DALT-1 5/13/2010 61 2010 Survey 3 DALT-1 5/13/2010 62 2010 Survey 1 DALT-1 5/13/2010 62 2010 Survey 2 DALT-1 5/13/2010 62 2010 Survey 3 DALT-1 5/13/2010 77 2010 Survey 1 MARR-2 5/4-5/2010 77 2010 Survey 2 MARR-2 5/4-5/2010 77 2010 Survey 3 MARR-2 5/4-5/2010 84 2010 Survey 1 MARR-1 5 12/6-7/2010 84 2010 Survey 2 MARR-1 5 12/6-7/2010 84 2010 Survey 3 MARR-1 5 12/6-7/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 1 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 2 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 3 MOHA-3 50 12/13-14/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 1 MOHA-3 50 12/15-16/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 2 MOHA-3 50 12/15-16/2010 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74, 75

2010 Survey 3 MOHA-3 50 12/15-16/2010**Parent Company Facility Name**  **City State**  **Kiln ID**

Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Florim Ceramiche S.p.A Florim USA Clarksville TN RK-1 Dal-Tile Corp. Dal Italia Muskogee OK RK-2, RK-3, RK-4 Dal-Tile Corp. Dal Italia Muskogee OK RK-2, RK-3, RK-4 Dal-Tile Corp. Dal Italia Muskogee OK RK-2, RK-3, RK-4 Dal-Tile Corp. Dal Italia Muskogee OK RK-2 Dal-Tile Corp. Dal Italia Muskogee OK RK-2 Dal-Tile Corp. Dal Italia Muskogee OK RK-2 Dal-Tile Corp. Dal Italia Muskogee OK RK-3 Dal-Tile Corp. Dal Italia Muskogee OK RK-3 Dal-Tile Corp. Dal Italia Muskogee OK RK-3 Dal-Tile Corp. Dal Italia Muskogee OK RK-4 Dal-Tile Corp. Dal Italia Muskogee OK RK-4 Dal-Tile Corp. Dal Italia Muskogee OK RK-4 Monarch Ceramic Tile Monarch Florence AL RK-2L Monarch Ceramic Tile Monarch Florence AL RK-2L Monarch Ceramic Tile Monarch Florence AL RK-2L Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX RK-5U Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX RK-5U Marazzi Group S.p.A. Marazzi, Sunny vale Facility Sunny

vale TX RK-5U Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-1, RK-2, RK-5, RK-6 Bisque tested together Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-1, RK-2, RK-5, RK-6 Bisque tested together Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-1, RK-2, RK-5, RK-6 Bisque tested together Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-7, RK-8, RK-11, RK-12 Glost tested together Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-7, RK-8, RK-11, RK-12 Glost tested together Mohawk Industries Dal-Tile El Paso Plant El Paso TX RK-7, RK-8, RK-11, RK-12 Glost tested together**Source Type AP** **CD ID AP** **CD Type Test Methods**  **Production Rate During**  **Test (tph)** Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 5.28 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 6.42 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 8.05 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 7.93 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 7.96 Roller Kiln CD-1 DIFF 1, 2, 3A, 4, 5, 23, 29, 320 7.89 Roller Kiln EPN-29 Wet Scrubber23 27.30 Roller Kiln EPN-29 Wet Scrubber23 27.44 Roller Kiln EPN-29 Wet Scrubber23 26.83 Roller Kiln EPN-29 Wet Scrubber23 9.10 Roller Kiln EPN-29 Wet Scrubber23 9.15 Roller Kiln EPN-29 Wet Scrubber23 8.94 Roller Kiln EPN-29 Wet Scrubber23 9.10 Roller Kiln EPN-29 Wet Scrubber23 9.15 Roller Kiln EPN-29 Wet Scrubber23 8.94 Roller Kiln EPN-29 Wet Scrubber23 9.10 Roller Kiln EPN-29 Wet Scrubber23 9.15 Roller Kiln EPN-29 Wet Scrubber23 8.94 Roller Kiln None 1, 2, 3/3A, 4, 23 7.99 Roller Kiln None 1, 2, 3/3A, 4, 23 7.99 Roller Kiln None 1, 2, 3/3A, 4, 23 7.99 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 7.03278 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 6.85641 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 6.90050 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 9.31000 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 9.06000 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 8.05000 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 8.04000 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 7.97000 Roller Kiln None 1, 2, 3, 3A, 4, 5, 23, 29 7.90000**Source Flow A** **ctual (acfm)**  **Flow Dry Standard**

**(dscfm) Sample Volume**  **(dscf) Sample Volume** 

**(dscm)** Separate declassified submittal 23,555 16,174 202.21 5.73 Separate declassified submittal 23,943 16,280 198.29 5.62 Separate declassified submittal 24,685 16,704 205.74 5.83 Separate declassified submittal 23,602 15,550 196.0 5.55 Separate declassified submittal 23,968 15,815 198.2 5.61 Separate declassified submittal 24,118 16,123 203.6 5.76 Separate declassified submittal. Kilns identically sized 66,874 50,239 146.72 4.15 Separate declassified submittal. Kilns identically sized 68,621 51,264 161.73 4.58 Separate declassified submittal. Kilns identically sized 68,485 51,356 162.91 4.61 Separate declassified submittal. Kilns identically sized 66,874 50,239 146.72 4.15 Separate declassified submittal. Kilns identically sized 68,621 51,264 161.73 4.58 Separate declassified submittal. Kilns identically sized 68,485 51,356 162.91 4.61 Separate declassified submittal. Kilns identically sized 66,874 50,239 146.72 4.15 Separate declassified submittal. Kilns identically sized 68,621 51,264 161.73 4.58 Separate declassified submittal. Kilns identically sized 68,485 51,356 162.91 4.61 Separate declassified submittal. Kilns identically sized 66,874 50,239 146.72 4.15 Separate declassified submittal. Kilns identically sized 68,621 51,264 161.73 4.58 Separate declassified submittal. Kilns identically sized 68,485 51,356 162.91 4.61 Separate from Test Report 12,036 5,222 148.48 4.20 Separate from Test Report 12,342 5,335 140.71 3.98 Separate from Test Report 12,614 5,465 143.74 4.07 Separate from Test Report 27,726 20,413 165 4.67 Separate from Test Report 27,578 20,639 174 4.93 Separate from Test Report 27,327 20,095 173 4.90 Separate from Test Report. Kilns identically sized 33,823 19,500 158 4.47 Separate from Test Report. Kilns identically sized 30,186 17,578 145 4.10 Separate from Test Report. Kilns identically sized 32,264 18,485 154 4.35 Separate from Test Report. Kilns identically sized 24,913 13,758 115 3.25 Separate from Test Report. Kilns identically sized 24,328 13,992 113 3.19 Separate from Test Report. Kilns identically sized 23,964 13,858 118 3.34**Moisture (%) Temp Stack Gas**  **(deg F) Oxygen (%)**  **Total Dioxin/ Furan Concentration**  **(ng/dscm) Total Dioxin/ Furan** 

**Concentration (ng/dscm @7%O2)**  6.15 265.00 19.10 24.6264 190.1705 6.72 267.70 19.30 26.9437 234.0734 7.42 265.90 19.30 23.5620 204.6952 6.48 280 18.3 23.0030 122.9774 6.10 281 18.4 23.0095 127.9329 6.45 282 18.2 34.8035 179.1735 15.46 132.19 18.60 17.2771 104.4136 15.84 132.83 19.00 13.4572 98.4497 16.14 132.83 18.80 19.1936 127.0435 15.46 132.19 18.60 17.2771 104.4136 15.84 132.83 19.00 13.4572 98.4497 16.14 132.83 18.80 19.1936 127.0435 15.46 132.19 18.60 17.2771 104.4136 15.84 132.83 19.00 13.4572 98.4497 16.14 132.83 18.80 19.1936 127.0435 15.46 132.19 18.60 17.2771 104.4136 15.84 132.83 19.00 13.4572 98.4497 16.14 132.83 18.80 19.1936 127.0435 11.58 615.00 16.00 152.3930 432.2986 11.73 617.20 16.30 133.3391 402.9158 11.19 621.20 16.10 136.3685 394.9006 2.8 232.42 19.3 12.5454 108.9877 3.16 226.42 19.27 16.5012 140.7161 3.26 237.42 19.01 15.1465 111.3952 6.24 293.08 16.81 2.8559 9.7060 5.54 289.13 16.66 2.7355 8.9678 5.61 300.58 16.9 2.4394 8.4767 8.48 297.17 19.47 0.1274 1.2381 4.83 296 19.65 0.1401 1.5579 4.99 291.83 17.25 0.1013 0.3857**Total Dioxin/ Furan**

**Emission Rate (g/hr)**  **Total Dioxin/ Furan**

**Emission Rate (lb/hr)**  **Total Dioxin/ Furan**

**Emission Factor (lb/ton)**  **TEQ Concentration**

**(ng/dscm) TEQ Concentration** 

**(ng/dscm @7%O2)** 6.77E-04 1.49E-06 2.83E-07 0.506792458 3.913563982 7.45E-04 1.64E-06 2.56E-07 0.565299365 4.911038235 6.69E-04 1.47E-06 1.83E-07 0.521102302 4.527076247 6.08E-04 1.34E-06 1.69E-07 0.571049829 3.05292024 6.18E-04 1.36E-06 1.71E-07 0.598602434 3.328229534 9.54E-04 2.10E-06 2.66E-07 0.698651508 3.596761465 1.47E-03 3.25E-06 1.19E-07 0.408458158 2.468508 1.17E-03 2.58E-06 9.42E-08 0.375525485 2.747265391 1.67E-03 3.69E-06 1.38E-07 0.497408832 3.292372743 4.92E-04 1.08E-06 1.19E-07 0.408458158 2.468508 3.91E-04 8.61E-07 9.42E-08 0.375525485 2.747265391 5.58E-04 1.23E-06 1.38E-07 0.497408832 3.292372743 4.92E-04 1.08E-06 1.19E-07 0.408458158 2.468508 3.91E-04 8.61E-07 9.42E-08 0.375525485 2.747265391 5.58E-04 1.23E-06 1.38E-07 0.497408832 3.292372743 4.92E-04 1.08E-06 1.19E-07 0.408458158 2.468508 3.91E-04 8.61E-07 9.42E-08 0.375525485 2.747265391 5.58E-04 1.23E-06 1.38E-07 0.497408832 3.292372743 1.35E-03 2.98E-06 3.73E-07 2.49E+00 7.06E+00 1.21E-03 2.66E-06 3.33E-07 1.89E+00 5.70E+00 1.27E-03 2.79E-06 3.49E-07 1.75E+00 5.08E+00 4.35E-04 9.59E-07 1.36E-07 0.119419122 1.037453622 5.79E-04 1.28E-06 1.86E-07 0.147170892 1.25501558 5.17E-04 1.14E-06 1.65E-07 0.145298857 1.068600061 9.46E-05 2.09E-07 2.24E-08 0.034922898 0.118686622 8.17E-05 1.80E-07 1.99E-08 0.030434929 0.099774884 7.66E-05 1.69E-07 2.10E-08 0.028467809 0.098925637 2.98E-06 6.56E-09 8.16E-10 0.003145666 0.030576752 3.33E-06 7.34E-09 9.21E-10 0.002659802 0.029577002 2.39E-06 5.26E-09 6.66E-10 0.002809432 0.010698935**TEQ Emission Rate**

**(g/hr) TEQ Emission Rate** 

**(lb/hr) TEQ Emission** 

**Factor (lb/ton) Overall Run Status**  1.39E-05 3.07E-08 5.82E-09DLL 1.56E-05 3.45E-08 5.37E-09DLL 1.48E-05 3.26E-08 4.05E-09DLL 1.51E-05 3.33E-08 4.20E-09DLL 1.61E-05 3.55E-08 4.46E-09DLL 1.91E-05 4.22E-08 5.35E-09DLL 3.49E-05 7.69E-08 2.82E-09DLL 3.27E-05 7.21E-08 2.63E-09DLL 4.34E-05 9.57E-08 3.57E-09DLL 1.16E-05 2.56E-08 2.82E-09DLL 1.09E-05 2.40E-08 2.63E-09DLL 1.45E-05 3.19E-08 3.57E-09DLL 1.16E-05 2.56E-08 2.82E-09DLL 1.09E-05 2.40E-08 2.63E-09DLL 1.45E-05 3.19E-08 3.57E-09DLL 1.16E-05 2.56E-08 2.82E-09DLL 1.09E-05 2.40E-08 2.63E-09DLL 1.45E-05 3.19E-08 3.57E-09DLL 2.21E-05 4.87E-08 6.09E-09ADL 1.71E-05 3.77E-08 4.72E-09DLL 1.63E-05 3.59E-08 4.49E-09DLL 4.14E-06 9.13E-09 1.30E-09DLL 5.16E-06 1.14E-08 1.66E-09DLL 4.96E-06 1.09E-08 1.59E-09DLL 1.16E-06 2.55E-09 2.74E-10DLL 9.09E-07 2.00E-09 2.21E-10DLL 8.94E-07 1.97E-09 2.45E-10DLL 7.35E-08 1.62E-10 2.02E-11DLL 6.32E-08 1.39E-10 1.75E-11DLL 6.62E-08 1.46E-10 1.85E-11DLL**Overall Comments** Type of Tile Floor Floor Floor Floor Floor Floor Floor Floor Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor RK-2, RK-3, RK-4 tested together Floor Floor Floor Floor Floor Floor Floor RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall RK-1, RK-2, RK-5, RK-6 Bisque tested together Wall RK-7, RK-8, RK-11, RK-12 Glost tested together Wall RK-7, RK-8, RK-11, RK-12 Glost tested together Wall RK-7, RK-8, RK-11, RK-12 Glost tested together Wall**Glaze_No Data Source**  **Run No FACID**  **Old FACID**  **Test Date Parent_Co**  **Fac_Name City**  **Stat**

**e Glaze_ID**  **Proc_Type No_Booths_**  **per_Line APCD_ID**  **APCD_Type Test Methods**  **Mass of glaze spray**  **applied (tph)**  **Source Flow Actual**  **(acfm) Flow Dry** 

**Standard uncontrolled**  **(dscfm) Sample** 

**Volume (dscf)**  **Sample**

**Volume (dscm)**  **Moisture (%) Temp Stack**  **Gas (deg F) Oxygen (%)**  **PM Concentration**  **PM**

**Concentration Units**  **PM**

**Concentration Converted to**  **( μ** **g/dscm) PM Emission** 

**(lb/hr) <** **PM Emission**

**Factor (lb/ton glaze**  **spray applied)**  **Check PM <1**

**mg PM** 

**Concentration Converted to**  **(μg/dscm) <1mg corrected**  **PM Emission**

**(lb/hr) <1mg corrected**  **PM Emission**

**Factor (lb/ton glaze spray**  **applied) <1mg corrected**  **Overall Comments** 114; 116; 117; 119 2010 Survey 1 DALT-1 5/13-15/2010Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.14Separate declassified submittal 23,508 22,559 177.95 5.04 2.30 75.04 20.80 9.13E-01mg/dscm 913.00 7.72E-02 5.46E-01 4.6 913.0 7.72E-02 5.46E-01

114; 116; 117; 119 2010 Survey 2 DALT-1 5/13-15/2010Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.12Separate declassified submittal 23,177 22,643 180.42 5.11 1.93 73.92 20.80 7.63E-01mg/dscm 763.00 6.48E-02 5.41E-01 3.9 763.0 6.48E-02 5.41E-01

114; 116; 117; 119 2010 Survey 3 DALT-1 5/13-15/2010Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.12Separate declassified submittal 23,587 22,733 181.70 5.15 2.52 78.13 20.80 1.75E-01mg/dscm 175.00 1.49E-02 1.24E-01 0.9 194.4 1.65E-02 1.38E-01

712010 Survey 1 FLOR-1 123 5/26/2010Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric Filter 1, 2, 3, 3A, 4, 5, 29 0.15Separate declassified submittal 11,018 10,135 147.40 4.17 2.56 100.80 20.80 6.08E-01mg/dscm 608.00 2.31E-02 1.52E-01 2.5 608.0 2.31E-02 1.52E-01 712010 Survey 2 FLOR-1 123 5/26/2010Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric Filter 1, 2, 3, 3A, 4, 5, 29 0.10Separate declassified submittal 11,442 10,594 153.76 4.35 2.30 99.80 20.80 5.80E-01mg/dscm 580.00 2.29E-02 2.33E-01 2.5 580.0 2.29E-02 2.33E-01 712010 Survey 3 FLOR-1 123 5/27/2010Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric Filter 1, 2, 3, 3A, 4, 5, 29 0.13Separate declassified submittal 11,689 10,877 157.93 4.47 2.22 97.60 20.80 3.05E-02mg/dscm 30.50 1.24E-03 9.80E-03 0.1 223.6 9.11E-03 7.21E-02 73, 74, 752010 Survey 1 FLOR-1 123 5/24/2010Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.36Separate declassified submittal 13,631 12,713 160.19 4.54 2.99 93.30 20.80 9.4mg/dscm 9,400.00 4.48E-01 1.24E+00 42.6 9400.0 4.48E-01 1.24E+00 73, 74, 752010 Survey 2 FLOR-1 123 5/25/2010Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.40Separate declassified submittal 13,737 12,960 163.79 4.64 2.71 87.00 20.80 13.83mg/dscm 13,830.00 6.70E-01 1.69E+00 64.1 13830.0 6.70E-01 1.69E+00 73, 74, 752010 Survey 3 FLOR-1 123 5/25/2010Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.32Separate declassified submittal 13,702 12,784 160.43 4.54 2.99 91.60 20.80 9.49mg/dscm 9,490.00 4.54E-01 1.40E+00 43.1 9490.0 4.54E-01 1.40E+00

09000064819365ee Glazing - PM Page 1 of 1 12/1/2014**Glaze_No Data**  **Source Run No**  **FACID Old**  **FACID Test Date**  **Parent_Co Fac_Name**  **City Stat** 

**e Glaze_ID**  **Proc_Type No_Booths_**  **per_Line APCD_ID**  **APCD_Type Test Methods**  **Mass of glaze spray**  **applied (tph) Source**  **Flow Actual (acfm)**  **Flow Dry**

**Standard uncontrolle**  **d (dscfm) Sample** 

**Volume (dscf)**  **Sample**

**Volume (dscm)**  **Moisture (%) Temp Stack**  **Gas (deg F) Oxygen (%)**  Fraction 1 FH (μg) Fraction

1 Status Fraction

2B BH[HNO 3/H2O2] (μg) Fraction 2 Status Fraction

3A BH [HNO3] (μg) Fraction

3A Status Fraction

3B BH [KMnO4/ H2SO4] (μg) Fraction

3B Status Fraction

3C BH [HCl] (μg) Fraction

3C Status Subtotal

Filterabl

e Subtotal

NonFilterabl

e Total **<** Blank

Fraction 1 FH (μg) **<** Blank

Fraction 2B BH[HNO 3/H2O2] (μg) **<** Blank

Fraction 3A BH [HNO3] (μg) **<** Blank

Fraction 3B BH [KMnO4/ H2SO4] (μg) **<** Blank

Fraction 3C BH [HCl] (μg) Blank

Fraction 1 FH (μg) Blank

Fraction 2B BH[HNO 3/H2O2] (μg) Blank Fraction 3A BH [HNO3] (μg) Blank

Fraction 3B BH [KMnO4/ H2SO4] (μg) Blank

Fraction 3C BH [HCl] (μg) Total

Blank (ug) **is Mfhb**

**> 8.658 is Mfhb** 

**> Mfh Front Half** 

**Correction is Mbhb** 

**> 1 is Mbhb** 

**> Mbh Back Half** 

**Correction is F3Ab** 

**> F3A F3A** 

**Correction is F3Bb** 

**> F3B F3B** 

**Correction is F3Cb** 

**> F3C F3C** 

**Correctio**

**n** Run

Total Blank Correcte d (ug) Run

Total Blank Correcte d (ug/dsc m) Run

Total Blank Correcte d (ug/dsc

m Run Total

Blank Corrected (lb/hr) Run Total

Blank Corrected (lb/ton) **Lab Detection Level Notes**  **Method Detection Limit [highlighted pink**  **if MDL NOT used] 1**  **2B 3A**  **3B 3C**  **Sum** Status based on fractions Overall

Run Status Type of

Tile 114; 116; 117; 119 2010

Survey 1 DALT-1 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.14 Separate declassified submittal 23,508 22,559 177.95 5.04 2.30 75.04 20.80 < 0.015 BDL 0.15 ADL 0.0072 ADL 0.0725 ADL 0.187 ADL 0.015 0.4167 0.43 < 0.015 < 0.005 < 0.005 < 0.025 0.0568 0 0 0 0 0.0568 0.0568 0.015 0.15 0.0072 0.0725 0.1302 0.37 0.0744 10.3418 6.287E-06 4.452E-05 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_ADL_ADL_ADLDLL Floor 114; 116; 117; 119 2010

Survey 2 DALT-1 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.12 Separate declassified submittal 23,177 22,643 180.42 5.11 1.93 73.92 20.80 < 0.015 BDL < 0.005 BDL < 0.005 BDL < 0.025 BDL 0.077 ADL 0.015 0.112 0.13 < 0.015 < 0.005 < 0.005 < 0.025 0.0568 0 0 0 0 0.0568 0.0568 0.015 0.005 0.005 0.025 0.0202 0.07 0.01374 1.90998 1.165E-06 9.733E-06 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_BDL_BDL_BDL_ADLDLL Floor 114; 116; 117; 119 2010

Survey 3 DALT-1 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.12 Separate declassified submittal 23,587 22,733 181.70 5.15 2.52 78.13 20.80 < 0.015 BDL < 0.005 BDL 0.0296 ADL < 0.025 BDL 0.093 ADL 0.015 0.1526 0.17 < 0.015 < 0.005 < 0.005 < 0.025 0.0568 0 0 0 0 0.0568 0.0568 0.015 0.005 0.0296 0.025 0.0362 0.11 0.02153 2.99328 1.834E-06 1.529E-05 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_BDL_ADL_BDL_ADLDLL Floor 71 2010 1 FLOR-1 123 5/26/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric 1, 2, 3, 3A, 4, 5, 29 0.15 Separate declassified submittal 11,018 10,135 147.40 4.17 2.56 100.80 20.80 < 0.015 BDL 0.233 ADL 0.0434 ADL < 0.025 BDL 0.315 ADL 0.015 0.6164 0.63 < 0.015 0.2 < 0.005 < 0.025 0.04 0 0.2 0 0 0.04 0.24 0.015 0.033 0.0434 0.025 0.275 0.39 0.09377 13.0342 3.56E-06 2.33E-05 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_ADL_BDL_ADLDLL Floor 71 2010 2 FLOR-1 123 5/26/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric 1, 2, 3, 3A, 4, 5, 29 0.10 Separate declassified submittal 11,442 10,594 153.76 4.35 2.30 99.80 20.80 < 0.015 BDL 0.184 ADL 0.0293 ADL < 0.025 BDL 0.428 ADL 0.015 0.6663 0.68 < 0.015 0.2 < 0.005 < 0.025 0.04 0 0.2 0 0 0.04 0.24 0.015 Yes 0.005 0.0293 0.025 0.388 0.46 0.10618 14.7588 4.213E-06 4.278E-05 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_ADL_BDL_ADLDLL Floor 71 2010 3 FLOR-1 123 5/27/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric 1, 2, 3, 3A, 4, 5, 29 0.13 Separate declassified submittal 11,689 10,877 157.93 4.47 2.22 97.60 20.80 < 0.015 BDL 0.254 ADL 0.0263 ADL < 0.025 BDL 0.206 ADL 0.015 0.5113 0.53 < 0.015 0.2 < 0.005 < 0.025 0.04 0 0.2 0 0 0.04 0.24 0.015 0.054 0.0263 0.025 0.166 0.29 0.06402 8.89886 2.608E-06 2.064E-05 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_ADL_BDL_ADLDLL Floor 73, 74, 752010 1 FLOR-1 123 5/24/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.36 Separate declassified submittal 13,631 12,713 160.19 4.54 2.99 93.30 20.80 < 0.015 BDL 0.195 ADL < 0.005 BDL < 0.025 BDL 0.089 ADL 0.015 0.314 0.33 < 0.015 0.2 < 0.005 < 0.025 0.04 0 0.2 0 0 0.04 0.24 0.015 Yes 0.005 0.005 0.025 0.049 0.10 0.02183 3.03373 1.039E-06 2.871E-06 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_BDL_BDL_ADLDLL Floor 73, 74, 752010 2 FLOR-1 123 5/25/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.40 Separate declassified submittal 13,737 12,960 163.79 4.64 2.71 87.00 20.80 < 0.015 BDL 0.186 ADL < 0.005 BDL < 0.025 BDL 0.144 ADL 0.015 0.36 0.38 < 0.015 0.2 < 0.005 < 0.025 0.04 0 0.2 0 0 0.04 0.24 0.015 Yes 0.005 0.005 0.025 0.104 0.15 0.0332 4.61535 1.612E-06 4.075E-06 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_BDL_BDL_ADLDLL Floor 73, 74, 752010 3 FLOR-1 123 5/25/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.32 Separate declassified submittal 13,702 12,784 160.43 4.54 2.99 91.60 20.80 < 0.015 BDL 0.244 ADL 0.11 ADL < 0.025 BDL 0.312 ADL 0.015 0.691 0.71 < 0.015 0.2 < 0.005 < 0.025 0.04 0 0.2 0 0 0.04 0.24 0.015 0.044 0.11 0.025 0.272 0.47 0.10258 14.258 4.912E-06 1.518E-05 ALS Laboratory GroupLOR: Limit of Reporting 0.015 0.005 0.005 0.025 0.025 0.075 BDL_ADL_ADL_BDL_ADLDLL Floor

09000064819365ee Glazing-Hg Page 1 of 1 12/1/2014**Glaze_No Data Source**  **Run No FACID**  **Old FACID**  **Test Date Parent_Co**  **Fac_Name City**  **Stat**

**e Glaze_ID**  **Proc_Type No_Booths_**  **per_Line APCD_ID**  **APCD_Type Test Methods**  **Mass of glaze spray**  **applied (tph) Source**  **Flow Actual (acfm)**  **Flow Dry**

**Standard uncontrolled**  **(dscfm) Sample** 

**Volume (dscf)**  **Sample**

**Volume (dscm)**  **Moisture (%) Temp Stack**  **Gas (deg F) Oxygen (%)**  **Antimony Front Half ug**  **Antimony**

**Back Half ug Antimony** 

**Total ug Antimony** 

**Blank Front Half ug**  **Antimony**

**Blank Back Half ug**  **Antimony**

**Blank Front Half ug**  **Antimony**

**Blank Back Half ug**  **Antimony**

**Total Blank**
**ug is Mfhb >** 

**8.658 is Mfhb > Mfh**  **Antimony Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Antimony**

**Back Half Correction**  **Antimony**

**Total Blank Corrected ug**  **Antimony**

**Total Blank Corrected**  **ug/dscm Antimony** 

**Total Blank Corrected**  **lb/hr Antimony** 

**Total Blank Corrected**  **lb/ton Antimony** 

**Fraction Status**  **Antimony Run**

**Status Antimony** 

**MDL [other highlighted in**  **pink] Front Half ug**  **Antimony**

**MDL [other highlighted in**  **pink] Back Half ug**  **Arsenic**

**Front Half**
**ug Arsenic Back** 

**Half ug Arsenic Total** 

**ug Arsenic** 

**Blank Front Half ug**  **Arsenic**

**Blank Back Half ug**  **Arsenic**

**Blank Front Half ug**  **Arsenic**

**Blank Back Half ug**  **Arsenic Total**

**Blank ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Arsenic Total** 

**Blank Corrected ug**  **Arsenic Total**

**Blank Corrected**  **ug/dscm Arsenic Total** 

**Blank Corrected**  **lb/hr Arsenic Total** 

**Blank Corrected**  **lb/ton Arsenic Run** 

**Status Arsenic Run** 

**Status Arsenic MDL** 

**[other highlighted**  **in pink] Front Half** 
**ug Arsenic MDL** 

**[other highlighted**  **in pink] Back Half ug**  **Beryllium**

**Front Half**
**ug Beryllium** 

**Back Half ug Beryllium** 

**Total ug Beryllium** 

**Blank Front Half ug**  **Beryllium**

**Blank Back Half ug**  **Beryllium**

**Blank Front Half ug**  **Beryllium**

**Blank Back Half ug**  **Beryllium**

**Total Blank**
**ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Beryllium** 

**Total Blank Corrected ug**  **Beryllium**

**Total Blank Corrected**  **ug/dscm Beryllium** 

**Total Blank Corrected**  **lb/hr Beryllium** 

**Total Blank Corrected**  **lb/ton Beryllium** 

**Run Status Beryllium** 

**Run Status Beryllium** 

**MDL [other highlighted**  **in pink] Front Half** 
**ug Beryllium** 

**MDL [other highlighted**  **in pink] Back Half ug**  **Cadmium**

**Front Half**
**ug Cadmium** 

**Back Half ug Cadmium** 

**Total ug Cadmium** 

**Blank Front Half ug**  **Cadmium**

**Blank Back Half ug**  **Cadmium**

**Blank Front Half ug**  **Cadmium**

**Blank Back Half ug**  114; 116; 117; 119 2010 Survey 1 DALT-1 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.14 Separate declassified submittal 23,508 22,559 177.95 5.04 2.30 75.04 20.80 0.769 0.1 0.869 0.2 0.1 0 0 0 0.769 0.1 0.869 0.172458344 1.45726E-05 0.000103196 ADL_BDL DLL 0.2 0.1 1 0.200 1.200 1 2 0 0 0 1 0.2 1.2 0.23814731 2.01233E-05 0.000142504 BDL_ADL DLL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.059536828 5.03083E-06 3.56259E-05 BDL_BDL BDL 0.2 0.1 0.221 0.05 0.271 0.1 0.05 0 0 114; 116; 117; 119 2010 Survey 2 DALT-1 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.12 Separate declassified submittal 23,177 22,643 180.42 5.11 1.93 73.92 20.80 0.22 0.1 0.32 0.2 0.1 0 0 0 0.22 0.1 0.32 0.062636521 5.31232E-06 4.43672E-05 ADL_BDL DLL 0.2 0.1 1 0.2 1.200 1 2 0 0 0 1 0.2 1.2 0.234886953 1.99212E-05 0.000166377 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.058721738 4.9803E-06 4.15943E-05 BDL_BDL BDL 0.2 0.1 0.1 0.0511 0.1511 0.1 0.05 0 0 114; 116; 117; 119 2010 Survey 3 DALT-1 5/13-15/2010 Dal-Tile Corp. Dal Italia Muskogee OK GL 7 - 10 Glaze Line 4; 5; 5; 4 EPN-41 Baghouse/Fabric Filter 1-4, 5, 29 0.12 Separate declassified submittal 23,587 22,733 181.70 5.15 2.52 78.13 20.80 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.058306136 4.96475E-06 4.1403E-05 BDL_BDL BDL 0.2 0.1 1 0.2 1.200 1 2 0 0 0 1 0.2 1.2 0.233224545 1.9859E-05 0.000165612 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.058306136 4.96475E-06 4.1403E-05 BDL_BDL BDL 0.2 0.1 0.1 0.05 0.15 0.1 0.05 0 0

71 2010 Survey 1 FLOR-1 123 5/26/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric Filter 1, 2, 3, 3A, 4, 5, 29 0.15 Separate declassified submittal 11,018 10,135 147.40 4.17 2.56 100.80 20.80 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.071873503 2.72858E-06 1.78614E-05 BDL_BDL BDL 0.2 0.1 1 0.2 1.200 1 2 0 0 0 1 0.2 1.2 0.287494011 1.09143E-05 7.14456E-05 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.071873503 2.72858E-06 1.78614E-05 BDL_BDL BDL 0.2 0.1 0.1 0.05 0.15 0.1 0.05 0 0

71 2010 Survey 2 FLOR-1 123 5/26/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric Filter 1, 2, 3, 3A, 4, 5, 29 0.10 Separate declassified submittal 11,442 10,594 153.76 4.35 2.30 99.80 20.80 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.068902159 2.73426E-06 2.77635E-05 BDL_BDL BDL 0.2 0.1 1 0.2 1.200 1 2 0 0 0 1 0.2 1.2 0.275608636 1.0937E-05 0.000111054 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.068902159 2.73426E-06 2.77635E-05 BDL_BDL BDL 0.2 0.1 0.1 0.05 0.15 0.1 0.05 0 0

71 2010 Survey 3 FLOR-1 123 5/27/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-1 Glaze Line Baghouse/Fabric Filter 1, 2, 3, 3A, 4, 5, 29 0.13 Separate declassified submittal 11,689 10,877 157.93 4.47 2.22 97.60 20.80 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.067084079 2.7331E-06 2.16225E-05 BDL_BDL BDL 0.2 0.1 1 0.2 1.200 1 2 0 0 0 1 0.2 1.2 0.268336315 1.09324E-05 8.64899E-05 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.067084079 2.7331E-06 2.16225E-05 BDL_BDL BDL 0.2 0.1 0.1 0.0932 0.1932 0.1 0.05 0 0

73, 74, 75 2010 Survey 1 FLOR-1 123 5/24/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.36 Separate declassified submittal 13,631 12,713 160.19 4.54 2.99 93.30 20.80 1.28 0.174 1.454 0.2 0.1 0 0 0 1.28 0.174 1.454 0.320546737 1.52644E-05 4.21641E-05 ADL_ADL ADL 0.2 0.1 1.51 0.36 1.870 1 2 0 0 0 1.51 0.36 1.9 0.412257496 1.96316E-05 5.42276E-05 ADL_ADL ADL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.066137566 3.14946E-06 8.69961E-06 BDL_BDL BDL 0.2 0.1 0.153 0.145 0.298 0.1 0.05 0 0

73, 74, 75 2010 Survey 2 FLOR-1 123 5/25/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.40 Separate declassified submittal 13,737 12,960 163.79 4.64 2.71 87.00 20.80 5.97 0.11 6.08 0.2 0.1 0 0 0 5.97 0.11 6.08 1.310909875 6.36392E-05 0.000160889 ADL_ADL ADL 0.2 0.1 1 2 3.000 1 2 0 0 0 1 2 3.0 0.64683053 3.14009E-05 7.93861E-05 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.064683053 3.14009E-06 7.93861E-06 BDL_BDL BDL 0.2 0.1 0.1 0.05 0.15 0.1 0.05 0 0

73, 74, 75 2010 Survey 3 FLOR-1 123 5/25/2010 Florim Ceramiche S.p.A Florim USA Clarksville TN GL-3, 4, 5 Glaze Line Wet Scrubber 1, 2, 3, 3A, 4, 5, 29 0.32 Separate declassified submittal 13,702 12,784 160.43 4.54 2.99 91.60 20.80 0.657 0.1 0.757 0.2 0.1 0 0 0 0.657 0.1 0.757 0.16662998 7.97898E-06 2.46577E-05 ADL_BDL DLL 0.2 0.1 1 2 3.000 1 2 0 0 0 1 2 3.0 0.660356593 3.16208E-05 9.77186E-05 BDL_BDL BDL 1 0.2 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.066035659 3.16208E-06 9.77186E-06 BDL_BDL BDL 0.2 0.1 0.104 0.05 0.154 0.1 0.05 0 0

09000064819365ee Glazing - Non-Hg HAP Page 1 of 3 12/1/2014**Cadmium Total Blank** 
**ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Cadmium** 

**Total Blank Corrected ug**  **Cadmium**

**Total Blank Corrected**  **ug/dscm Cadmium** 

**Total Blank Corrected**  **lb/hr Cadmium** 

**Total Blank Corrected**  **lb/ton Cadmium** 

**Run Status Cadmium** 

**Run Status Cadmium** 

**MDL [other highlighted**  **in pink] Front Half** 
**ug Cadmium** 

**MDL [other highlighted**  **in pink] Back Half ug**  **Chromium**

**Front Half**
**ug Chromium** 

**Back Half ug Chromium** 

**Total ug Chromium** 

**Blank Front Half ug**  **Chromium**

**Blank Back Half ug**  **Chromium**

**Blank Front Half ug**  **Chromium**

**Blank Back Half ug**  **Chromium**

**Total Blank**
**ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Chromium** 

**Total Blank Corrected ug**  **Chromium**

**Total Blank Corrected**  **ug/dscm Chromium** 

**Total Blank Corrected**  **lb/hr Chromium** 

**Total Blank Corrected**  **lb/ton Chromium** 

**Run Status Chromium** 

**Run Status Chromium** 

**MDL [other highlighted**  **in pink] Front Half** 
**ug Chromium** 

**MDL [other highlighted**  **in pink] Back Half ug**  **Cobalt Front**

**Half ug Cobalt Back** 

**Half ug Cobalt Total** 

**ug Cobalt Blank** 

**Front Half**
**ug Cobalt Blank** 

**Back Half ug Cobalt Blank** 

**Front Half**
**ug Cobalt Blank** 

**Back Half ug Cobalt Total** 

**Blank ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Cobalt Total** 

**Blank Corrected ug**  **Cobalt Total**

**Blank Corrected**  **ug/dscm Cobalt Total** 

**Blank Corrected**  **lb/hr Cobalt Total** 

**Blank Corrected**  **lb/ton Cobalt Run** 

**Status Cobalt Run** 

**Status Cobalt MDL** 

**[other highlighted**  **in pink] Front Half** 
**ug Cobalt MDL** 

**[other highlighted**  **in pink] Back Half ug**  **Lead Front**

**Half ug Lead Back** 

**Half ug Lead Total** 

**ug Lead Blank** 

**Front Half**
**ug Lead Blank** 

**Back Half ug Lead Blank** 

**Front Half**
**ug Lead Blank** 

**Back Half ug Lead Total** 

**Blank ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Lead Total** 

**Blank Corrected ug**  **Lead Total**

**Blank Corrected**  **ug/dscm Lead Total** 

**Blank Corrected**  **lb/hr Lead Total** 

**Blank Corrected**  **lb/ton Lead Run** 

**Status Lead Run** 

**Status Lead MDL** 

**[other highlighted**  **in pink] Front Half** 
**ug Lead MDL** 

**[other highlighted**  **in pink] Back Half ug**  **Manganese**

**Front Half**
**ug Manganese** 

**Back Half ug Manganese** 

**Total ug Manganese** 

**Blank Front Half ug**  **Manganese**

**Blank Back Half ug**  **Manganese**

**Blank Front Half ug**  **Manganese**

**Blank Back Half ug**  **Manganese**

**Total Blank**
**ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **II: lesser of**

**Mbhb or 5% of Mbh**  **greater of I**

**or II Back Half** 

**Correction Manganese** 

**Total Blank Corrected ug**  **Manganese**

**Total Blank Corrected**  **ug/dscm Manganese** 

**Total Blank Corrected**  **lb/hr Manganese** 

**Total Blank Corrected**  **lb/ton MN** 

**Contamination Check: Ratio of**  **BH/FH**

0 0.221 0.05 0.271 0.053781601 4.54452E-06 3.21821E-05 ADL_BDL DLL 0.1 0.05 2.23 0.163 2.393 1 0.382 0 0.382 0.382 2.23 Yes 0.15 2.4 0.472325499 3.99113E-05 0.000282632 ADL_ADL ADL 1 0.15 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.059536828 5.03083E-06 3.56259E-05 BDL_BDL BDL 0.2 0.1 1.22 0.305 1.525 0.5 0.192 0 0.192 0.192 1.22 0.113 1.333 0.264541971 2.23537E-05 0.000158298 ADL_ADL ADL 0.5 0.05 1.92 20.1 22.02 0.62 1.28 0.62 1.28 1.9 1.3 Yes 1.005 1.005 19.095 20.395 4.047511997 0.000342013 0.002421969 10.5

0 0.1 0.0511 0.1511 0.029576182 2.50841E-06 2.09496E-05 BDL_ADL DLL 0.1 0.05 1.82 0.364 2.184 1 0.382 0 0.382 0.382 1.82 Yes 0.15 2.0 0.385606082 3.2704E-05 0.000273136 ADL_ADL ADL 1 0.15 0.2 0.264 0.464 0.2 0.1 0 0 0 0.2 0.264 0.464 0.090822955 7.70287E-06 6.43325E-05 BDL_ADL DLL 0.2 0.1 0.799 0.773 1.572 0.5 0.192 0 0.192 0.192 0.799 0.581 1.38 0.270119996 2.29094E-05 0.000191334 ADL_ADL ADL 0.5 0.05 3.48 37.3 40.78 0.62 1.28 0.62 1.28 1.9 2.86 Yes 1.28 1.28 36.02 38.88 7.610337287 0.000645447 0.005390618 10.7

0 0.1 0.05 0.15 0.029153068 2.48238E-06 2.07015E-05 BDL_BDL BDL 0.1 0.05 1 0.392 1.392 1 0.382 0 0.382 0.382 1 0.01 1.0 0.196297325 1.67147E-05 0.00013939 BDL_ADL DLL 1 0.15 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.058306136 4.96475E-06 4.1403E-05 BDL_BDL BDL 0.2 0.1 0.676 0.357 1.033 0.5 0.192 0 0.192 0.192 0.676 0.165 0.841 0.163451535 1.39179E-05 0.000116067 ADL_ADL ADL 0.5 0.05 1.34 1.43 2.77 0.62 1.28 0.62 1.28 1.9 0.72 Yes 0.0715 1 0.43 1.15 0.223506855 1.90316E-05 0.000158712 1.1

0 0.1 0.05 0.15 0.035936751 1.36429E-06 8.9307E-06 BDL_BDL BDL 0.1 0.05 2.52 0.292 2.812 1.05 0.488 1.05 0.488 1.538 1.47 Yes 0.15 1.6 0.388116914 1.47343E-05 9.64516E-05 ADL_ADL ADL 1 0.15 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.071873503 2.72858E-06 1.78614E-05 BDL_BDL BDL 0.2 0.1 1.26 0.207 1.467 0.5 0.12 0 0.12 0.12 1.26 0.087 1.347 0.322712027 1.22513E-05 8.01977E-05 ADL_ADL ADL 0.5 0.05 3.21 0.976 4.186 0.93 0.45 0.93 0.45 1.38 2.28 0.526 2.806 0.672256828 2.55213E-05 0.000167064 0.3

0 0.1 0.05 0.15 0.034451079 1.36713E-06 1.38818E-05 BDL_BDL BDL 0.1 0.05 2.18 0.602 2.782 1.05 0.488 1.05 0.488 1.538 1.13 0.114 1.2 0.285714286 1.13381E-05 0.000115126 ADL_ADL ADL 1 0.15 0.2 0.1 0.3 0.2 0.1 0 0 0 0.2 0.1 0.3 0.068902159 2.73426E-06 2.77635E-05 BDL_BDL BDL 0.2 0.1 0.849 0.137 0.986 0.5 0.12 0 0.12 0.12 0.849 0.017 0.866 0.198897565 7.89289E-06 8.01441E-05 ADL_ADL ADL 0.5 0.05 3.3 17.1 20.4 0.93 0.45 0.93 0.45 1.38 2.37 16.65 19.02 4.368396876 0.000173352 0.001760208 5.2

0 0.1 0.0932 0.1932 0.043202147 1.76012E-06 1.39249E-05 BDL_ADL DLL 0.1 0.05 1.32 0.585 1.905 1.05 0.488 1.05 0.488 1.538 0.27 0.097 0.4 0.08206619 3.34349E-06 2.64515E-05 ADL_ADL ADL 1 0.15 0.2 0.82 1.02 0.2 0.1 0 0 0 0.2 0.82 1.02 0.228085868 9.29254E-06 7.35164E-05 BDL_ADL DLL 0.2 0.1 0.5 0.174 0.674 0.5 0.12 0 0.12 0.12 0.5 0.054 0.554 0.123881932 5.04713E-06 3.99295E-05 BDL_ADL DLL 0.5 0.05 1.99 3.41 5.4 0.93 0.45 0.93 0.45 1.38 1.06 2.96 4.02 0.898926655 3.66236E-05 0.000289741 1.7

0 0.153 0.145 0.298 0.065696649 3.12846E-06 8.64161E-06 ADL_ADL ADL 0.1 0.05 153 0.969 153.969 1.05 0.488 1.05 0.488 1.538 151.95 0.481 152.4 33.60471781 0.001600252 0.0044203 ADL_ADL ADL 1 0.15 17.4 0.134 17.534 0.2 0.1 0 0 0 17.4 0.134 17.534 3.865520282 0.000184075 0.000508463 ADL_ADL ADL 0.2 0.1 15.3 1.93 17.23 0.5 0.12 0 0.12 0.12 15.3 1.81 17.11 3.772045855 0.000179624 0.000496168 ADL_ADL ADL 0.5 0.05 1190 104 1294 0.93 0.45 0.93 0.45 1.38 1189.07 103.55 1292.62 284.9691358 0.013570187 0.037484294 0.1

0 0.1 0.05 0.15 0.032341527 1.57004E-06 3.9693E-06 BDL_BDL BDL 0.1 0.05 344 0.733 344.733 1.05 0.488 1.05 0.488 1.538 342.95 0.245 343.2 73.99633463 0.003592211 0.009081633 ADL_ADL ADL 1 0.15 14.6 0.1 14.7 0.2 0.1 0 0 0 14.6 0.1 14.7 3.169469599 0.000153864 0.000388992 ADL_BDL DLL 0.2 0.1 5.06 0.0675 5.1275 0.5 0.120 0 0.12 0.12 5.06 Yes 0.05 5.11 1.101768003 5.34862E-05 0.000135221 ADL_ADL ADL 0.5 0.05 526 1.83 527.83 0.93 0.45 0.93 0.45 1.38 525.07 1.38 526.45 113.5079776 0.005510334 0.01393093 0.0

0 0.104 0.05 0.154 0.033898305 1.6232E-06 5.01622E-06 ADL_BDL DLL 0.1 0.05 150 0.474 150.474 1.05 0.488 1.05 0.488 1.538 148.95 Yes 0.15 149.1 32.81972265 0.001571553 0.004856616 ADL_ADL ADL 1 0.15 14.6 0.1 14.7 0.2 0.1 0 0 0 14.6 0.1 14.7 3.235747304 0.000154942 0.000478821 ADL_BDL DLL 0.2 0.1 3.51 0.111 3.621 0.5 0.120 0 0.12 0.12 3.51 Yes 0.05 3.56 0.783623157 3.75233E-05 0.000115959 ADL_ADL ADL 0.5 0.05 214 8.94 222.94 0.93 0.45 0.93 0.45 1.38 213.07 8.49 221.56 48.76953555 0.0023353 0.007216847 0.0

09000064819365ee Glazing - Non-Hg HAP Page 2 of 3 12/1/2014**Manganese Run Status**  **Manganese**

**Run Status Manganese** 

**MDL [other highlighted**  **in pink] Front Half** 
**ug Manganese** 

**MDL [other highlighted**  **in pink] Back Half ug**  **Nickel Front**

**Half ug Nickel Back** 

**Half ug Nickel Total** 

**ug Nickel Blank** 

**Front Half**
**ug Nickel Blank** 

**Back Half ug Nickel Blank** 

**Front Half**
**ug Nickel Blank** 

**Back Half ug Nickel Total** 

**Blank ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Nickel Total** 

**Blank Corrected ug**  **Nickel Total**

**Blank Corrected**  **ug/dscm Nickel Total** 

**Blank Corrected**  **lb/hr Nickel Total** 

**Blank Corrected**  **lb/ton Nickel Run** 

**Status Nickel Run** 

**Status Nickel MDL** 

**[other highlighted**  **in pink] Front Half** 
**ug Nickel MDL** 

**[other highlighted**  **in pink] Back Half ug**  **Selenium**

**Front Half**
**ug Selenium** 

**Back Half ug Selenium** 

**Total ug Selenium** 

**Blank Front Half ug**  **Selenium**

**Blank Back Half ug**  **Selenium**

**Blank Front Half ug**  **Selenium**

**Blank Back Half ug**  **Selenium**

**Total Blank**
**ug is Mfhb >** 

**8.658 is Mfhb >** 

**Mfh Front Half** 

**Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Back Half**

**Correction Selenium** 

**Total Blank Corrected ug**  **Selenium**

**Total Blank Corrected**  **ug/dscm Selenium** 

**Total Blank Corrected**  **lb/hr Selenium** 

**Total Blank Corrected**  **lb/ton Selenium** 

**Run Status Selenium** 

**Run Status Selenium** 

**MDL [other highlighted**  **in pink] Front Half** 
**ug Selenium** 

**MDL [other highlighted**  **in pink] Back Half ug**  **Removed Runs**

**Rational** Run Status Run Status Laboratory Analytical Method Lab Method Listed in PW

Memo

0.5 0.15 2.22 0.635 2.855 0.429 0.615 0.429 0.615 1.044 1.791 0.02 1.811 0.359403983 3.03695E-05 0.000215062 ADL_ADL ADL 0.2 0.1 2 1.59 3.59 2 1 0 0 0 2 1.59 3.59 0.71245737 6.02023E-05 0.000426323 BDL_ADL DLL 2 1 Mn Contamination ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

0.5 0.15 6.88 0.758 7.638 0.429 0.615 0.429 0.615 1.044 6.451 0.143 6.594 1.290703808 0.000109467 0.000914242 ADL_ADL ADL 0.2 0.1 2 1 3 2 1 0 0 0 2 1 3 0.587217383 4.9803E-05 0.000415943 BDL_BDL BDL 2 1 Mn Contamination ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

ADL_ADL ADL 0.5 0.15 1.74 0.638 2.378 0.429 0.615 0.429 0.615 1.044 1.311 0.023 1.334 0.259267952 2.20766E-05 0.000184106 ADL_ADL ADL 0.2 0.1 2 1 3 2 1 0 0 0 2 1 3 0.583061362 4.96475E-05 0.00041403 BDL_BDL BDL 2 1 BDL_BDL_BDL_BDL_DLL_BDL_ADL_ADL_ADL_BDL DLL ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

ADL_ADL ADL 0.5 0.15 1.21 0.233 1.443 0.83 0.185 0.83 0.185 1.015 0.38 0.048 0.428 0.10253953 3.89277E-06 2.54823E-05 ADL_ADL ADL 0.2 0.1 2 1 3 2 1 0 0 0 2 1 3 0.718735026 2.72858E-05 0.000178614 BDL_BDL BDL 2 1 BDL_BDL_BDL_BDL_ADL_BDL_ADL_ADL_ADL_BDL DLL ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

0.5 0.15 1.47 0.227 1.697 0.83 0.185 0.83 0.185 1.015 0.64 0.042 0.682 0.156637575 6.21588E-06 6.31158E-05 ADL_ADL ADL 0.2 0.1 2 1.06 3.06 2 1 0 0 0 2 1.06 3.06 0.702802021 2.78894E-05 0.000283188 BDL_ADL DLL 2 1 Mn Contamination ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

ADL_ADL ADL 0.5 0.15 5.19 0.747 5.937 0.83 0.185 0.83 0.185 1.015 4.36 0.562 4.922 1.100626118 4.48411E-05 0.000354753 ADL_ADL ADL 0.2 0.1 2 1 3 2 1 0 0 0 2 1 3 0.670840787 2.7331E-05 0.000216225 BDL_BDL BDL 2 1 BDL_BDL_BDL_DLL_ADL_DLL_DLL_ADL_ADL_BDL DLL ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

ADL_ADL ADL 0.5 0.15 5.72 0.571 6.291 0.83 0.185 0.83 0.185 1.015 4.89 0.386 5.276 1.16313933 5.53885E-05 0.000152997 ADL_ADL ADL 0.2 0.1 2 1.85 3.85 2 1 0 0 0 2 1.85 3.85 0.848765432 4.04181E-05 0.000111645 BDL_ADL DLL 2 1 ADL_ADL_BDL_ADL_ADL_ADL_ADL_ADL_ADL_DLL DLL ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

ADL_ADL ADL 0.5 0.15 10.5 0.407 10.907 0.83 0.185 0.83 0.185 1.015 9.67 0.222 9.892 2.132815869 0.000103539 0.000261762 ADL_ADL ADL 0.2 0.1 2 1.02 3.02 2 1 0 0 0 2 1.02 3.02 0.651142734 3.16102E-05 7.99153E-05 BDL_ADL DLL 2 1 ADL_BDL_BDL_BDL_ADL_DLL_ADL_ADL_ADL_DLL DLL ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

ADL_ADL ADL 0.5 0.15 7.79 0.383 8.173 0.83 0.185 0.83 0.185 1.015 6.96 0.198 7.158 1.57561083 7.54472E-05 0.000233157 ADL_ADL ADL 0.2 0.1 2 1.11 3.11 2 1 0 0 0 2 1.11 3.11 0.684569668 3.27802E-05 0.000101302 BDL_ADL DLL 2 1 DLL_BDL_BDL_DLL_ADL_DLL_ADL_ADL_ADL_DLL DLL ALS Laboratory Group ICP-MS Method 29 ICP/MS or GFAA

09000064819365ee Glazing - Non-Hg HAP Page 3 of 3 12/1/2014**Dryer No. Data Source** **Run No FA** **CID Old**  **FA CID**  **Test Date Parent Company**  SD-101 2008 Survey 1 MARR-2 222 3/23/2005 Monarch Ceramic Tile SD-101 2008 Survey 2 MARR-2 222 3/23/2005 Monarch Ceramic Tile SD-101 2008 Survey 3 MARR-2 222 3/23/2005 Monarch Ceramic Tile PD-200 2008 Survey 1 MARR-2 222 12/12/2003 Monarch Ceramic Tile PD-200 2008 Survey 2 MARR-2 222 12/12/2003 Monarch Ceramic Tile PD-200 2008 Survey 3 MARR-2 222 12/12/2003 Monarch Ceramic Tile**Facility Name City**  **State Dryer ID**  **Source Type AP** **CD ID**

Monarch Florence AL SD-2 Spray Dryer Monarch Florence AL SD-2 Spray Dryer Monarch Florence AL SD-2 Spray Dryer Monarch Florence AL D-1 Press Dryer Monarch Florence AL D-1 Press Dryer Monarch Florence AL D-1 Press Dryer**AP CD Type**  **Productio n Rate**  **During Test (tph)**  **Source Flow A** **ctual (acfm)**  **Flow Dry**

**Standard uncontrolled**  **(dscfm) Sample** 

**Volume (dscf)**  Fabric Filter 28.27 Test Report 34,600 19,439 98.69 Fabric Filter 28.27 Test Report 33,002 19,685 94.16 Fabric Filter 28.27 Test Report 33,948 19,790 94.72 7.07Test Report 4,732 3,336 42.17 7.07Test Report 4,862 3,381 40.65 7.07Test Report 4,799 3,313 40.26**Sample**

**Volume (dscm)**  **Moisture (%) Temp Stack**  **Gas (deg F) Oxygen (%)**  **PM Concentration**  **PM**

**Concentration Units**  **PM**

**Concentration Converted to**  **( μ** **g/dscm)** 2.79 25.00 213.40 19.50 0.0078gr/dscf 17,849.14 2.67 24.90 210.30 19.50 0.0055gr/dscf 12,585.94 2.68 26.50 206.10 19.50 0.0018gr/dscf 4,119.03 1.19 5.40 258.00 18.50 7.60E-03gr/dscf 17,391.47 1.15 6.00 262.00 18.50 1.00E-02gr/dscf 22,883.52 1.14 6.90 261.00 18.50 9.90E-03gr/dscf 22,654.68**PM Emission** 

**Rate (lb/hr) <** **PM Emission** 

**Factor (lb/ton)**  **Check PM**

**<1mg Overall Comments**  **Ty pe of**  **Product** 1.36 0.048107534 49.9 Floor 0.92 0.032543332 33.6 Floor 0.31 0.010965688 11.0 Floor 0.22 0.031117397 20.8 Floor 0.3 0.042432815 26.3 Floor 0.28 0.03960396 25.8 Floor**Dryer No. Data Source** **Run No FA** **CID Old**  **FA CID**  **Test Date Parent Company**  SD-100 2010 Survey 1 MARR-2 222 5/6-7/10 Monarch Ceramic Tile SD-100 2010 Survey 2 MARR-2 222 5/6-7/10 Monarch Ceramic Tile SD-100 2010 Survey 3 MARR-2 222 5/6-7/10 Monarch Ceramic Tile SD-101 2010 Survey 1 MARR-2 222 5/6-7/10 Monarch Ceramic Tile SD-101 2010 Survey 2 MARR-2 222 5/6-7/10 Monarch Ceramic Tile SD-101 2010 Survey 3 MARR-2 222 5/6-7/10 Monarch Ceramic Tile SD-102 2010 Survey 1 DALT-1 5/10-12/2010 Dal-Tile Corp. SD-102 2010 Survey 2 DALT-1 5/10-12/2010 Dal-Tile Corp. SD-102 2010 Survey 3 DALT-1 5/10-12/2010 Dal-Tile Corp. SD-103 2010 Survey 1 FLOR-1 123 10/12-13/2010 Florim Ceramiche S.p.A SD-103 2010 Survey 2 FLOR-1 123 10/12-13/2010 Florim Ceramiche S.p.A SD-103 2010 Survey 3 FLOR-1 123 10/12-13/2010 Florim Ceramiche S.p.A SD-104 2010 Survey 1 MARR-1 5 12/2-3/2010 Marazzi Group S.p.A. SD-104 2010 Survey 2 MARR-1 5 12/2-3/2010 Marazzi Group S.p.A. SD-104 2010 Survey 3 MARR-1 5 12/2-3/2010 Marazzi Group S.p.A. SD-105 2010 Survey 1 MOHA-3 50 4/28-29/2011 Mohawk Industries SD-105 2010 Survey 2 MOHA-3 50 4/28-29/2011 Mohawk Industries SD-105 2010 Survey 3 MOHA-3 50 4/28-29/2011 Mohawk Industries PD-200 2010 Survey 1 MARR-2 222 5/4-5/10 Monarch Ceramic Tile PD-200 2010 Survey 2 MARR-2 222 5/4-5/10 Monarch Ceramic Tile PD-200 2010 Survey 3 MARR-2 222 5/4-5/10 Monarch Ceramic Tile PD-201 2010 Survey 1 DALT-1 5/15-16/2010 Dal-Tile Corp. PD-201 2010 Survey 2 DALT-1 5/15-16/2010 Dal-Tile Corp. PD-201 2010 Survey 3 DALT-1 5/15-16/2010 Dal-Tile Corp. PD-202 2010 Survey 1 FLOR-1 123 10/13-14/2010 Florim Ceramiche S.p.A PD-202 2010 Survey 2 FLOR-1 123 10/13-14/2010 Florim Ceramiche S.p.A PD-202 2010 Survey 3 FLOR-1 123 10/13-14/2010 Florim Ceramiche S.p.A PD-203 2010 Survey 1 MARR-1 5 12/2-3/2010 Marazzi Group S.p.A. PD-203 2010 Survey 2 MARR-1 5 12/2-3/2010 Marazzi Group S.p.A. PD-203 2010 Survey 3 MARR-1 5 12/2-3/2010 Marazzi Group S.p.A. PD-204 2010 Survey 1 MOHA-3 50 12/13-14/2010 Mohawk Industries PD-204 2010 Survey 2 MOHA-3 50 12/13-14/2010 Mohawk Industries PD-204 2010 Survey 3 MOHA-3 50 12/13-14/2010 Mohawk Industries**Facility Name City**  **State Dryer ID**  **Source Type AP** **CD ID**

Monarch Florence AL SD-1 Spray Dryer Monarch Florence AL SD-1 Spray Dryer Monarch Florence AL SD-1 Spray Dryer Monarch Florence AL SD-2 Spray Dryer Monarch Florence AL SD-2 Spray Dryer Monarch Florence AL SD-2 Spray Dryer Dal Italia Muskogee OK SD-1 Spray Dryer EPN 05 Dal Italia Muskogee OK SD-1 Spray Dryer EPN 05 Dal Italia Muskogee OK SD-1 Spray Dryer EPN 05 Florim USA Clarksville TN SD-2 Spray Dryer Florim USA Clarksville TN SD-2 Spray Dryer Florim USA Clarksville TN SD-2 Spray Dryer Marazzi, Sunny

vale Facility

Sunny vale TX SD-3 Spray Dryer BP-5 Marazzi, Sunny

vale Facility

Sunny vale TX SD-3 Spray Dryer BP-5 Marazzi, Sunny

vale Facility

Sunny vale TX SD-3 Spray Dryer BP-5 Dal-Tile El Paso Plant El Paso TX SD-1 Spray Dryer Dal-Tile El Paso Plant El Paso TX SD-1 Spray Dryer Dal-Tile El Paso Plant El Paso TX SD-1 Spray Dryer Monarch Florence AL D-1 Press Dryer Monarch Florence AL D-1 Press Dryer Monarch Florence AL D-1 Press Dryer Dal Italia Muskogee OK VD #9 Press Dryer Dal Italia Muskogee OK VD #9 Press Dryer Dal Italia Muskogee OK VD #9 Press Dryer Florim USA Clarksville TN VD-1 Press Dryer Florim USA Clarksville TN VD-1 Press Dryer Florim USA Clarksville TN VD-1 Press Dryer Marazzi, Sunny

vale Facility

Sunny vale TX DC-10 Press Dryer Marazzi, Sunny

vale Facility

Sunny vale TX DC-10 Press Dryer Marazzi, Sunny

vale Facility

Sunny vale TX DC-10 Press Dryer Dal-Tile El Paso Plant El Paso TX DC-5 Press Dryer Dal-Tile El Paso Plant El Paso TX DC-5 Press Dryer Dal-Tile El Paso Plant El Paso TX DC-5 Press Dryer**AP CD Type**  **Productio n Rate**  **During Test (tph)**  **Source Flow A** **ctual (acfm)**  **Flow Dry**

**Standard uncontrolled**  **(dscfm) Sample** 

**Volume (dscf)**  Wet Scrubber 16.31429Declassified submittal 26,929 20,184 130 Wet Scrubber 16.31429Declassified submittal 27,316 20,278 133 Wet Scrubber 16.31429Declassified submittal 27,108 20,127 134 Fabric Filter 16.64499Declassified submittal 31,372 20,490 178 Fabric Filter 16.64499Declassified submittal 30,861 19,452 173 Fabric Filter 16.64499Declassified submittal 30,726 19,649 168 Fabric Filter 37.36855Declassified submittal 77,055 49,226 147 Fabric Filter 41.82191Declassified submittal 78,737 49,677 146 Fabric Filter 36.70716Declassified submittal 77,649 51,422 144 Wet Scrubber 11.33182Declassified submittal 23,359 15,605 152.1 Wet Scrubber 10.52713Declassified submittal 24,189 16,444 131.0 Wet Scrubber 10.73657Declassified submittal 23,925 16,391 132.0 Fabric Filter 37.83152Declassified submittal 83,762 54,386 149 Fabric Filter 37.29139Declassified submittal 86,390 56,386 157 Fabric Filter 37.50083Declassified submittal 84,099 55,253 151 Wet Scrubber 18.45Declassified submittal 36,973 20,663 149 Wet Scrubber 18.45Declassified submittal 35,573 20,055 150 Wet Scrubber 18.84Declassified submittal 36,486 20,273 147 None 7.991799Declassified submittal 5,407 3,543 172 None 7.991799Declassified submittal 5,401 3,563 173 None 7.991799Declassified submittal 5,320 3,558 167 None 8.212262Declassified submittal 5,457 3,581 150 None 8.256355Declassified submittal 5,463 3,516 148 None 9.501973Declassified submittal 5,448 3,561 147 None 9.601182Declassified submittal 6,074 4,132 172.1 None 6.172976Declassified submittal 6,145 4,450 179.0 None 7.980776Declassified submittal 6,074 4,273 175.7 None 7.617011Declassified submittal 3,893 2,721 170 None 6.53674Declassified submittal 3,808 2,598 165 None 8.520911Declassified submittal 3,802 2,625 167 None 1.96Declassified submittal 1,291 637 166 None 2.33Declassified submittal 1,287 629 156 None 2.32Declassified submittal 1,263 618 153**Sample**

**Volume (dscm)**  **Moisture (%) Temp Stack**  **Gas (deg F) Oxygen (%)**  **Total Dioxin/ Furan**  **Concentration (ng/dscm)**  **Total Dioxin/**

**Furan Concentration**  **(ng/dscm @7%O2)** 3.7 15.38 134.90 19.10 33.42 258.09 3.8 16.09 135.60 19.10 32.42 250.36 3.8 16.40 133.30 19.10 25.97 200.52 5.0 17.77 203.90 18.00 1.10 5.25 4.9 20.01 209.30 18.00 1.14 5.45 4.7 19.49 203.90 18.00 1.27 6.08 4.2 22.53 179.85 18.00 2.15 10.30 4.1 22.74 182.90 18.50 1.94 11.23 4.1 19.17 180.15 18.00 2.82 13.53 4.3 23.10 145 18.3 131.89 705.09 3.7 22.98 143 18.5 101.69 588.95 3.7 21.96 142 18.3 119.03 636.36 4.2 16.42 215.13 18.50 0.03 0.16 4.5 15.92 215.63 18.60 0.03 0.16 4.3 16.37 214.79 19.30 0.01 0.12 4.2 26.87 146.21 18.02 7.45 35.97 4.2 28.09 145.08 17.56 8.51 35.41 4.2 28.93 146.75 17.41 6.29 25.06 4.9 10.84 256.80 18.60 7.36 44.45 4.9 10.33 256.30 18.80 6.83 45.19 4.7 8.43 261.50 19.00 6.00 43.93 4.3 11.17 256.71 18.90 0.56 3.89 4.2 12.78 257.25 18.80 0.27 1.76 4.2 11.55 256.29 18.30 0.48 2.57 4.9 9.26 238 19.0 3.39 24.82 5.1 4.60 240 19.0 1.87 13.70 5.0 6.87 238 19.0 2.74 20.03 4.8 9.84 216.92 18.80 0.05 0.33 4.7 11.33 222.08 18.80 0.06 0.37 4.7 11.69 218.46 18.72 0.06 0.35 4.7 11.94 366.42 17.46 0.22 0.88 4.4 12.64 364.21 17.57 0.27 1.13 4.3 12.68 364.58 17.41 0.20 0.81**Total Dioxin/**

**Furan Emission**  **Rate (g/hr) Total Dioxin/** 

**Furan Emission**  **Rate (lb/hr) Total Dioxin/** 

**Furan Emission Factor (lb/ton)**  **TEQ**

**Concentration (ng/dscm)**  **TEQ**

**Concentratio n (ng/dscm**  **@7%O2) TEQ** 

**Emission Rate (g/hr)**  1.15E-03 2.53E-06 1.55E-07 0.119449784 0.922417773 4.10E-06 1.12E-03 2.46E-06 1.51E-07 0.123227901 0.951593236 4.25E-06 8.88E-04 1.96E-06 1.20E-07 0.099441261 0.767907513 3.40E-06 3.82E-05 8.41E-08 5.05E-09 0.00625296 0.029971086 2.18E-07 3.76E-05 8.29E-08 4.98E-09 0.012137935 0.058178376 4.01E-07 4.24E-05 9.34E-08 5.61E-09 0.012018244 0.057604685 4.01E-07 1.80E-04 3.96E-07 1.06E-08 0.027341899 0.131052552 2.29E-06 1.64E-04 3.61E-07 8.63E-09 0.034573514 0.200238269 2.92E-06 2.47E-04 5.44E-07 1.48E-08 0.025468476 0.122073039 2.23E-06 3.50E-03 7.71E-06 6.80E-07 0.811820459 4.340117069 2.15E-05 2.84E-03 6.26E-06 5.95E-07 0.694779048 4.023928651 1.94E-05 3.32E-03 7.31E-06 6.81E-07 0.508685381 2.719510305 1.42E-05 2.49E-06 5.50E-09 1.45E-10 0.001573516 0.009113278 1.45E-07 2.50E-06 5.50E-09 1.48E-10 0.001703353 0.010294174 1.63E-07 1.34E-06 2.96E-09 7.90E-11 0.001251749 0.010874571 1.18E-07 2.62E-04 5.77E-07 3.13E-08 0.012227967 0.059016924 4.29E-07 2.90E-04 6.39E-07 3.46E-08 0.014299511 0.059509939 4.87E-07 2.17E-04 4.78E-07 2.54E-08 0.009941332 0.039594418 3.42E-07 4.43E-05 9.76E-08 1.22E-08 0.018978064 0.114693514 1.14E-07 4.13E-05 9.11E-08 1.14E-08 0.02150843 0.142365321 1.30E-07 3.63E-05 8.00E-08 1.00E-08 0.018797032 0.137515128 1.14E-07 3.41E-06 7.51E-09 9.15E-10 0.010836027 0.075310386 6.59E-08 1.59E-06 3.50E-09 4.24E-10 0.008842277 0.058527451 5.28E-08 2.90E-06 6.40E-09 6.74E-10 0.022499616 0.120286409 1.36E-07 2.38E-05 5.25E-08 5.47E-09 0.017120982 0.125253499 1.20E-07 1.42E-05 3.12E-08 5.06E-09 0.007639774 0.055890976 5.78E-08 1.99E-05 4.38E-08 5.49E-09 0.011532918 0.084372399 8.37E-08 2.32E-07 5.11E-10 6.70E-11 0.001140006 0.007545755 5.27E-09 2.49E-07 5.50E-10 8.41E-11 0.001144159 0.007573244 5.05E-09 2.46E-07 5.43E-10 6.37E-11 0.000923239 0.005886708 4.12E-09 2.36E-07 5.21E-10 2.66E-10 0.001576948 0.006371971 1.71E-09 2.88E-07 6.35E-10 2.73E-10 0.001572952 0.006565776 1.68E-09 2.15E-07 4.73E-10 2.04E-10 0.001031006 0.004106298 1.08E-09**TEQ**

**Emission Rate (lb/hr)**  **TEQ**

**Emission Factor**  **(lb/ton) Overall Run** 

**Status Overall Comments**  **Ty pe of Product**  9.03E-09 5.54E-10DLL Floor 9.36E-09 5.74E-10DLL Floor 7.50E-09 4.60E-10DLL Floor 4.80E-10 2.88E-11DLL Floor 8.84E-10 5.31E-11DLL Floor 8.85E-10 5.31E-11DLL Floor 5.04E-09 1.35E-10DLL Floor 6.43E-09 1.54E-10DLL Floor 4.91E-09 1.34E-10DLL Floor 4.75E-08 4.19E-09DLL Floor 4.28E-08 4.07E-09DLL Floor 3.12E-08 2.91E-09DLL Floor 3.21E-10 8.47E-12DLL Floor 3.60E-10 9.65E-12DLL Floor 2.59E-10 6.91E-12DLL Floor 9.47E-10 5.13E-11DLL Wall 1.07E-09 5.82E-11DLL Wall 7.55E-10 4.01E-11DLL Wall 2.52E-10 3.15E-11DLL Floor 2.87E-10 3.59E-11DLL Floor 2.51E-10 3.14E-11DLL Floor 1.45E-10 1.77E-11DLL Floor 1.16E-10 1.41E-11DLL Floor 3.00E-10 3.16E-11DLL Floor 2.65E-10 2.76E-11DLL Floor 1.27E-10 2.06E-11DLL Floor 1.85E-10 2.31E-11DLL Floor 1.16E-11 1.53E-12DLL Floor 1.11E-11 1.70E-12DLL Floor 9.08E-12 1.07E-12DLL Floor 3.76E-12 1.92E-12DLL Wall 3.70E-12 1.59E-12DLL Wall 2.39E-12 1.03E-12DLL Wall

Spray Dryer Average

Press Dryer Average**RTI**

**Inventory Kiln ID**  **Data Source FA** **CID Old FA**  **CID Test Date**  **Run Company**  **Plant Location (City**  **/State) AP** **CD Ty pe**  **New-Source ID Source**  **Ty pe**  **Test Methods** 92008 Survey KOHL-SC 82 2/7/2007 1 Kohler Co. Spartanburg, SC Wet ScrubberTK-10 Tunnel Kiln 92008 Survey KOHL-SC 82 2/7/2007 2 Kohler Co. Spartanburg, SC Wet ScrubberTK-10 Tunnel Kiln 92008 Survey KOHL-SC 82 2/7/2007 3 Kohler Co. Spartanburg, SC Wet ScrubberTK-10 Tunnel Kiln 92010 Survey KOHL-SC 82 8/13/2010 1 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 2 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 3 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 1 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 2 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 3 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 1 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 2 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 26A 92010 Survey KOHL-SC 82 8/13/2010 3 Kohler Co. Spartanburg, SC Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 1 Kohler Co. Spartanburg, SC None TK #2 POC stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 2 Kohler Co. Spartanburg, SC None TK #2 POC stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 3 Kohler Co. Spartanburg, SC None TK #2 POC stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 1 Kohler Co. Spartanburg, SC None TK #2 EE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 2 Kohler Co. Spartanburg, SC None TK #2 EE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 3 Kohler Co. Spartanburg, SC None TK #2 EE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 1 Kohler Co. Spartanburg, SC None TK #2 FE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 2 Kohler Co. Spartanburg, SC None TK #2 FE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 3 Kohler Co. Spartanburg, SC None TK #2 FE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 1 Kohler Co. Spartanburg, SC None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 2 Kohler Co. Spartanburg, SC None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 26A 22010 Survey KOHL-SC 82 8/11/2010 3 Kohler Co. Spartanburg, SC None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 26A 72010 Survey KOHL-SC 82 8/13/2010 1 Kohler Co. Spartanburg, SC None TK #8 POC stack Tunnel Kiln EPA Method 26A 72010 Survey KOHL-SC 82 8/13/2010 2 Kohler Co. Spartanburg, SC None TK #8 POC stack Tunnel Kiln EPA Method 26A 72010 Survey KOHL-SC 82 8/13/2010 3 Kohler Co. Spartanburg, SC None TK #8 POC stack Tunnel Kiln EPA Method 26A

19 & 202010 Survey KOHL-TX 203

8/25/2010 1 Kohler Co. Brownwood, TX None TK #6/12 POC stack Tunnel Kiln EPA Method 26A

19 & 202010 Survey KOHL-TX 203

8/25/2010 2 Kohler Co. Brownwood, TX None TK #6/12 POC stack Tunnel Kiln EPA Method 26A

19 & 202010 Survey KOHL-TX 203

8/25/2010 3 Kohler Co. Brownwood, TX None TK #6/12 POC stack Tunnel Kiln EPA Method 26A 192010 Survey KOHL-TX 203 8/25/2010 1 Kohler Co. Brownwood, TX None TK #6 POC stack Tunnel Kiln EPA Method 26A 192010 Survey KOHL-TX 203 8/25/2010 2 Kohler Co. Brownwood, TX None TK #6 POC stack Tunnel Kiln EPA Method 26A 192010 Survey KOHL-TX 203 8/25/2010 3 Kohler Co. Brownwood, TX None TK #6 POC stack Tunnel Kiln EPA Method 26A 202010 Survey KOHL-TX 203 8/25/2010 1 Kohler Co. Brownwood, TX None TK #12 POC stack Tunnel Kiln EPA Method 26A 202010 Survey KOHL-TX 203 8/25/2010 2 Kohler Co. Brownwood, TX None TK #12 POC stack Tunnel Kiln EPA Method 26A 202010 Survey KOHL-TX 203 8/25/2010 3 Kohler Co. Brownwood, TX None TK #12 POC stack Tunnel Kiln EPA Method 26A 332010 Survey KOHL-WI 204 8/4/2010 1 Kohler Co. Kohler, WI None TK #19 POC stack Tunnel Kiln EPA Method 26A 332010 Survey KOHL-WI 204 8/4/2010 2 Kohler Co. Kohler, WI None TK #19 POC stack Tunnel Kiln EPA Method 26A 332010 Survey KOHL-WI 204 8/4/2010 3 Kohler Co. Kohler, WI None TK #19 POC stack Tunnel Kiln EPA Method 26A

09000064819365ee TK-Acid Gas Page 1 of 7 12/1/2014POC = products of combustion stack

EE = Entrance Exshaust stack FE = Fume Exhaust stack RCE = Rapid Cool Exhaust stack WEE = Ware Exit Exhaust stack

09000064819365ee TK-Acid Gas Page 2 of 7 12/1/2014**Production**

**(tph) Flow A** 

**ctual (A** **CFM) Flow Dry** 

**Standard (DSCFM)**  **Sample**

**Volume (DSCF)**  **Sample**

**Volume (DSCM)**  **Moisture (%) Temp (deg F)**  **Oxy gen (%)**  **HF Concentration**  **(ppmd) HF** 

**Concentration (ppmd @ 7%**  **O2) HF** 

**Concentration Converted to**  **(μg/dscm)** 0.74 0.74 0.74 0.40 8,451 6,641 32.06 0.91 9.40 133.60 19.03 0.30 2.41 249.72 0.40 8,329 6,562 31.82 0.90 9.08 134.20 18.96 0.50 3.35 416.20 0.40 8,360 6,574 31.97 0.91 9.26 134.10 18.88 0.40 3.06 332.96 0.40 9,994 5,651 37.02 1.05 4.11 413.00 20.66 0.024 1.41 20.23 0.40 9,842 5,603 35.07 0.99 3.28 414.50 20.04 0.025 0.41 20.89 0.40 9,964 5,690 37.02 1.05 3.30 411.70 19.98 0.019 0.29 15.98 0.40 0.40 0.40 0.82 10,771 4,110 35.17 1.00 10.23 753.50 14.73 10.80 24.33 8,989.83 0.82 10,574 4,035 34.56 0.98 10.05 755.70 14.13 8.50 17.46 7,075.33 0.82 10,653 4,091 34.77 0.98 9.74 752.30 14.09 6.40 13.07 5,327.31 0.82 183 155 38.12 1.08 3.77 125.40 20.28 0.06 1.42 49.94 0.82 183 155 37.97 1.08 3.41 126.80 20.23 0.02 0.39 16.65 0.82 183 156 37.96 1.07 3.36 126.80 20.22 0.02 0.38 16.65 0.82 1,524 1,002 36.13 1.02 4.81 286.00 19.68 1.41 16.12 1,173.67 0.82 1,555 1,020 37.54 1.06 4.63 289.80 19.61 0.70 7.51 582.67 0.82 1,539 1,011 36.70 1.04 4.55 289.30 19.61 0.40 4.36 332.96 0.82 0.82 0.82 1.85 16,709 12,390 41.56 1.18 6.84 188.50 18.21 16.30 84.40 13,567.99 1.85 16,673 12,341 41.45 1.17 6.36 193.00 17.74 18.10 79.48 15,066.29 1.85 16,893 12,517 41.33 1.17 6.19 193.60 18.20 15.90 81.71 13,235.03

5.07 45,913 32,516 41.16 1.17 5.61 234.00 18.07 12.00 59.18 9,988.70

5.07 45,828 32,332 40.68 1.15 5.81 235.20 18.10 12.30 60.83 10,238.42

5.07 45,422 32,137 40.44 1.15 5.41 236.20 18.20 12.50 64.25 10,404.90 1.57 1.57 1.57 3.50 3.50 3.50 0.88 10,739 5,543 39.03 1.11 8.53 455.80 16.00 16.70 47.29 13,900.94 0.88 10,518 5,447 38.31 1.08 8.58 452.30 16.10 17.30 50.18 14,400.38 0.88 10,551 5,500 38.36 1.09 8.13 450.80 15.90 17.00 47.27 14,150.66

09000064819365ee TK-Acid Gas Page 3 of 7 12/1/201409000064819365ee

TK-Acid Gas Page 4 of 7 12/1/2014**HF Concentration**

**Converted to (μg/dscm @ 7%**  **O2) HF Emissions** 

**(kg/hr) HF** 

**Emissions (lb/hr)**  **< HF Emission** 

**Factor (lb/ton)**  **HCl**

**Concentration (ppmd)**  **HCl**

**Concentration (ppmd @ 7%**  **O2) HCl** 

**Concentration Converted to**  **(μg/dscm) HCl Concentration** 

**Converted to (μg/dscm @ 7%**  **O2) HCl Emissions** 

**(kg/hr) HCl** 

**Emissions (lb/hr)**  **< HCl** 

**Emission Factor**  **(lb/ton)** 1.55E-02 2.11E-02 3.23E-02 4.39E-02 1.79E-02 2.44E-02 1.50E-02 2.04E-02 1.52E-02 2.07E-02 1.36E-02 1.85E-02 2,006.06 3.04E-03 6.70E-03 1.68E-02 0.09 0.65 136.53 986.05 1.51E-03 3.33E-03 8.33E-03 2,788.51 4.33E-03 9.55E-03 2.39E-02 0.09 0.62 136.53 940.54 1.46E-03 3.22E-03< 8.06E-03 2,547.12 4.13E-03 9.11E-03 2.28E-02 0.09 0.59 136.53 895.03 1.45E-03 3.20E-03< 8.00E-03 1,173.67 1.90E-04 4.19E-04 1.05E-03 0.07 4.29 106.19 6,507.91 1.08E-03 2.38E-03< 5.96E-03 341.28 2.00E-04 4.41E-04 1.10E-03 0.08 1.27 121.36 1,926.58 1.13E-03 2.49E-03< 6.24E-03 241.39 1.50E-04 3.31E-04< 8.28E-04 0.07 1.12 106.19 1,699.04 1.09E-03 2.40E-03< 6.02E-03 7.12E-03 1.78E-02 5.71E-03 0.01429 9.99E-03 2.50E-02 5.71E-03< 0.01429 9.44E-03 2.36E-02 5.60E-03< 0.01402 20,252.09 6.27E-02 1.38E-01 1.69E-01 0.28 0.63 424.76 955.71 2.96E-03 6.53E-03 7.99E-03 14,533.56 4.85E-02 1.07E-01 1.31E-01 0.33 0.68 500.61 1,031.56 3.43E-03 7.56E-03 9.26E-03 10,879.36 3.70E-02 8.17E-02 1.00E-01 0.39 0.80 591.63 1,213.60 4.13E-03 9.11E-03 1.12E-02 1,182.00 1.00E-05 2.20E-05 2.70E-05 0.08 1.70 121.36 2,578.89 3.00E-05 6.61E-05 8.10E-05 324.63 4.10E-06 9.04E-06< 1.11E-05 0.07 1.50 106.19 2,275.49 3.00E-05 6.61E-05< 8.10E-05 316.31 4.11E-06 9.05E-06< 1.11E-05 0.07 1.48 106.19 2,245.15 3.00E-05 6.61E-05< 8.10E-05 13,418.16 2.00E-03 4.41E-03 5.40E-03 0.39 4.41 591.63 6,689.95 1.00E-03 2.20E-03 2.70E-03 6,251.26 1.01E-03 2.23E-03 2.73E-03 0.35 3.76 530.95 5,703.90 9.20E-04 2.03E-03 2.48E-03 3,629.23 5.80E-04 1.28E-03 1.57E-03 0.38 4.13 576.46 6,265.19 1.00E-03 2.20E-03 2.70E-03 1.43E-01 1.75E-01 8.80E-03 1.08E-02 1.09E-01 1.34E-01 9.66E-03 1.18E-02 8.29E-02 1.02E-01 1.14E-02 1.39E-02 70,253.87 2.86E-01 6.31E-01 3.41E-01 0.63 3.27 955.71 4,960.58 2.02E-02 4.45E-02 2.41E-02 66,158.51 3.15E-01 6.95E-01 3.76E-01 0.62 2.71 940.54 4,111.06 1.96E-02 4.32E-02 2.34E-02 68,014.74 2.81E-01 6.19E-01 3.35E-01 0.54 2.79 819.18 4,232.42 1.75E-02 3.85E-02 2.08E-02

49,260.95 5.54E-01 1.22E+00 2.41E-01 0.52 2.56 788.84 3,883.51 4.36E-02 9.61E-02 1.90E-02

50,634.40 5.60E-01 1.23E+00 2.43E-01 0.56 2.77 849.52 4,202.08 4.64E-02 1.02E-01 2.02E-02

53,481.18 5.67E-01 1.25E+00 2.46E-01 0.58 2.99 879.86 4,535.82 4.80E-02 1.06E-01 2.09E-02 3.78E-01 2.41E-01 2.98E-02 1.90E-02 3.83E-01 2.43E-01 3.17E-02 2.02E-02 3.87E-01 2.46E-01 3.28E-02 2.09E-02 8.43E-01 2.41E-01 6.63E-02 1.90E-02 8.52E-01 2.43E-01 7.06E-02 2.02E-02 8.63E-01 2.46E-01 7.31E-02 2.09E-02 39,363.81 1.31E-01 2.88E-01 3.29E-01 0.56 1.60 849.52 2,427.19 8.06E-03 1.78E-02 2.03E-02 41,769.42 1.33E-01 2.94E-01 3.36E-01 0.48 1.39 728.16 2,108.62 6.72E-03 1.48E-02 1.69E-02 39,347.16 1.32E-01 2.91E-01 3.33E-01 0.56 1.56 849.52 2,366.51 7.95E-03 1.75E-02 2.00E-02

09000064819365ee TK-Acid Gas Page 5 of 7 12/1/201409000064819365ee

TK-Acid Gas Page 6 of 7 12/1/2014**Comments**

did not test the RCE stack did not test the RCE stack did not test the RCE stack add TK #10 POC & RCE stack HF and HCl lb/hr values together add TK #10 POC & RCE stack HF and HCl lb/hr values together add TK #10 POC & RCE stack HF and HCl lb/hr values together add TK #10 POC & RCE stack HF and HCl lb/hr values together add TK #10 POC & RCE stack HF and HCl lb/hr values together add TK #10 POC & RCE stack HF and HCl lb/hr values together

add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together add TK #2 POC, EE, & FE stack HF and HCl lb/hr values together

Split test for each kiln: multiply HF and HCl lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. Split test for each kiln: multiply HF and HCl lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. Split test for each kiln: multiply HF and HCl lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value.

09000064819365ee TK-Acid Gas Page 7 of 7 12/1/2014**RTI**

**Inventory Kiln ID**  **Data Source FA** **CID Old FA**  **CID Test Date**  **Run Company**  **Plant Location (City**  **/State) AP** **CD AP** **CD Ty pe**  **New-Source ID Source Ty** **pe** 92008 Survey KOHL-SC 82 2/7/2007 1 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK-10 Tunnel Kiln 92008 Survey KOHL-SC 82 2/7/2007 2 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK-10 Tunnel Kiln 92008 Survey KOHL-SC 82 2/7/2007 3 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK-10 Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 1 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 POC stack Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 2 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 POC stack Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 3 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 POC stack Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 1 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 2 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 3 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 1 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 2 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln 92010 Survey KOHL-SC 82 8/12-13/2010 3 Kohler Co.Spartanburg, SC Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 1 Kohler Co.Spartanburg, SC No None TK #2 POC stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 2 Kohler Co.Spartanburg, SC No None TK #2 POC stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 3 Kohler Co.Spartanburg, SC No None TK #2 POC stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 1 Kohler Co.Spartanburg, SC No None TK #2 EE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 2 Kohler Co.Spartanburg, SC No None TK #2 EE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 3 Kohler Co.Spartanburg, SC No None TK #2 EE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 1 Kohler Co.Spartanburg, SC No None TK #2 FE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 2 Kohler Co.Spartanburg, SC No None TK #2 FE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 3 Kohler Co.Spartanburg, SC No None TK #2 FE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 1 Kohler Co.Spartanburg, SC No None TK #2 POC + EE + FE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 2 Kohler Co.Spartanburg, SC No None TK #2 POC + EE + FE stack Tunnel Kiln 22010 Survey KOHL-SC 82 8/10-11/2010 3 Kohler Co.Spartanburg, SC No None TK #2 POC + EE + FE stack Tunnel Kiln 72010 Survey KOHL-SC 82 8/12-13/2010 1 Kohler Co.Spartanburg, SC No None TK #8 POC stack Tunnel Kiln 72010 Survey KOHL-SC 82 8/12-13/2010 2 Kohler Co.Spartanburg, SC No None TK #8 POC stack Tunnel Kiln 72010 Survey KOHL-SC 82 8/12-13/2010 3 Kohler Co.Spartanburg, SC No None TK #8 POC stack Tunnel Kiln

19 & 202010 Survey KOHL-TX 203

8/23-24/2010 1 Kohler Co. Brownwood, TX No None TK #6/12 POC stack Tunnel Kiln

19 & 202010 Survey KOHL-TX 203

8/23-24/2010 2 Kohler Co. Brownwood, TX No None TK #6/12 POC stack Tunnel Kiln

19 & 202010 Survey KOHL-TX 203

8/23-24/2010 3 Kohler Co. Brownwood, TX No None TK #6/12 POC stack Tunnel Kiln 192010 Survey KOHL-TX 203 8/23-24/2010 1 Kohler Co. Brownwood, TX No None TK #6 POC stack Tunnel Kiln 192010 Survey KOHL-TX 203 8/23-24/2010 2 Kohler Co. Brownwood, TX No None TK #6 POC stack Tunnel Kiln 192010 Survey KOHL-TX 203 8/23-24/2010 3 Kohler Co. Brownwood, TX No None TK #6 POC stack Tunnel Kiln 202010 Survey KOHL-TX 203 8/23-24/2010 1 Kohler Co. Brownwood, TX No None TK #12 POC stack Tunnel Kiln 202010 Survey KOHL-TX 203 8/23-24/2010 2 Kohler Co. Brownwood, TX No None TK #12 POC stack Tunnel Kiln 202010 Survey KOHL-TX 203 8/23-24/2010 3 Kohler Co. Brownwood, TX No None TK #12 POC stack Tunnel Kiln 332010 Survey KOHL-WI 204 8/3-4/2010 1 Kohler Co. Kohler, WI No None TK #19 POC stack Tunnel Kiln 332010 Survey KOHL-WI 204 8/3-4/2010 2 Kohler Co. Kohler, WI No None TK #19 POC stack Tunnel Kiln 332010 Survey KOHL-WI 204 8/3-4/2010 3 Kohler Co. Kohler, WI No None TK #19 POC stack Tunnel Kiln

POC = products of combustion stack

09000064819365ee TK-PM Page 1 of 7 12/1/2014EE = Entrance Exshaust stack

FE = Fume Exhaust stack RCE = Rapid Cool Exhaust stack WEE = Ware Exit Exhaust stack

09000064819365ee TK-PM Page 2 of 7 12/1/2014**Test Methods Production**  **(tph) Flow A** 

**ctual (A** **CFM) Flow Dry** 

**Standard (DSCFM)**  **Sample**

**Volume (DSCF)**  **Sample**

**Volume (DSCM)**  **Moisture (%) Temp (deg F)**  **Oxy gen (%)**  **PM fil Concentration**  **(gr/dscf) PM fil** 

**Concentration (mg/dscm)**  0.735 0.735 0.735 EPA Method 5 0.41 8,466 6,669 131.21 3.72 9.23 133.20 19.22 0.00162 EPA Method 5 0.41 8,326 6,574 130.07 3.68 8.87 133.00 19.07 0.00127 EPA Method 5 0.40 8,432 6,683 132.93 3.76 8.81 132.40 18.96 0.0013 EPA Method 29 0.41 9,378 5,352 137.83 3.90 3.44 411.00 20.00 0.0007 EPA Method 29 0.41 10,476 5,952 154.88 4.39 3.50 412.50 20.03 0.00055 EPA Method 29 0.40 9,776 5,557 144.61 4.09 3.54 413.60 20.04 0.0006 EPA Method 5 0.41 EPA Method 5 0.41 EPA Method 5 0.40 EPA Method 5 0.79 10,724 4,139 140.83 3.99 9.11 758.20 14.24 0.00201 EPA Method 5 0.79 10,945 4,198 142.91 4.05 9.52 759.10 14.62 0.00188 EPA Method 5 0.82 10,749 4,131 140.15 3.97 9.58 755.90 14.09 0.00277 EPA Method 5 0.79 179 154 149.90 4.24 3.22 122.90 20.54 0.01763 EPA Method 5 0.79 182 155 151.32 4.28 3.24 125.30 20.52 0.00144 EPA Method 5 0.82 182 156 150.64 4.27 3.30 122.10 20.51 0.00045 EPA Method 5 0.79 1,621 1,062 151.79 4.30 5.28 287.80 19.76 0.00327 EPA Method 5 0.79 1,556 1,029 150.23 4.25 3.89 290.80 19.75 0.00121 EPA Method 5 0.82 1,512 1,001 145.68 4.13 4.51 285.40 19.64 0.00085 EPA Method 5 0.79 EPA Method 5 0.79 EPA Method 5 0.82 EPA Method 5 1.85 16,990 12,918 173.48 4.91 6.20 176.80 17.96 0.00109 EPA Method 5 1.85 17,218 12,829 169.41 4.80 6.31 187.80 17.89 0.00668 EPA Method 5 1.85 17,030 12,875 170.21 4.82 6.36 179.40 17.93 0.00123

EPA Method 5 5.088048499 45,474 31,210 156.42 4.43 5.45 253.00 18.19 0.00175

EPA Method 5 5.189571369 45,122 31,085 154.59 4.38 5.46 249.50 18.11 0.00182

EPA Method 5 5.189571369 45,864 31,376 156.40 4.43 5.78 252.10 18.26 0.00177 EPA Method 5 1.576578408 EPA Method 5 1.608036199 EPA Method 5 1.608036199 EPA Method 5 3.511470091 EPA Method 5 3.58153517 EPA Method 5 3.58153517 EPA Method 5 0.83 10,910 5,746 159.95 4.53 7.39 448.70 16.30 0.00176 EPA Method 5 0.83 11,214 5,877 164.64 4.66 8.01 447.00 16.20 0.00174 EPA Method 5 0.88 10,694 5,605 156.18 4.42 7.99 445.30 16.20 0.00161

09000064819365ee TK-PM Page 3 of 7 12/1/201409000064819365ee

TK-PM Page 4 of 7 12/1/2014**PM fil**

**Concentration (gr/dscf) @ 7% O2** **PM fil Concentration**

**(mg/dscm) @ 7% O2 PM fil**  **Concentration Converted to**  **( μ** **g/dscm) PM fil Concentration** 

**Converted to (** **μ g/dscm) @ 7% O2**  **PM fil Emissions**  **(kg/hr) PM fil** 

**Emissions (lb/hr)**  **PM fil**

**Emission Factor (lb/ton)**  **check,**

**calculating mg for < 1**  0.11 0.149659864 0.11 0.149659864 0.131 0.178231293 0.013403571 30.641 3,707.13 30,641.00 0.04196 0.092505965 0.224565161 13.8 0.009646448 22.066 2,906.21 22,066.00 0.03244 0.071517958 0.173615201 10.7 0.009314433 21.3 2,974.86 21,300.00 0.03375 0.074406013 0.18625828 11.2 0.010811111 24.891 1,601.85 24,891.00 0.01465 0.032297721 0.078405139 6.3 0.008787356 20.037 1,258.59 20,037.00 0.01268 0.027954615 0.067861922 5.5 0.009697674 22.301 1,373.01 22,301.00 0.01302 0.028704187 0.071854305 5.6 0.12 0.3029703 20.0 0.10 0.241477123 16.2 0.10 0.258112585 16.8 0.004195045 9.62 4,599.59 9,620.00 0.03241 0.071451819 0.090797031 18.3 0.004161146 9.533 4,302.10 9,533.00 0.03072 0.067726007 0.086062475 17.4 0.005653891 12.936 6,338.73 12,936.00 0.04448 0.098061614 0.120102607 25.2 0.680713889 1558.17 40,343.64 1,558,170.00 0.01053 0.023214676 0.02949993 171.2 0.052673684 120.966 3,295.23 120,966.00 0.00087 0.001918022 0.002437316 14.1 0.016038462 36.932 1,029.76 36,932.00 0.00028 0.000617294 0.000756042 4.4 0.039871053 91.172 7,482.91 91,172.00 0.01349 0.029740359 0.037792408 32.2 0.014625217 33.356 2,768.91 33,356.00 0.00482 0.010626281 0.013503292 11.8 0.009376984 21.474 1,945.10 21,474.00 0.00331 0.007297301 0.008937492 8.0 0.12 0.15808937 221.7 0.08 0.102003083 43.3 0.11 0.12979614 37.6 0.005153401 11.781 2,494.30 11,781.00 0.05468 0.120548765 0.065281758 12.3 0.030847841 70.61 15,286.19 70,610.00 0.33322 0.73462435 0.397827129 73.3 0.005756566 13.148 2,814.67 13,148.00 0.06144 0.135452014 0.073317423 13.6

0.008976015 20.554 4,004.62 20,554.00 0.21246 0.468394122 0.092057716 17.7

0.009067384 20.713 4,164.80 20,713.00 0.21954 0.48400285 0.093264514 18.2

0.009319318 21.281 4,050.38 21,281.00 0.21542 0.474919805 0.091514264 17.9 0.145136207 0.092057716 5.5 0.149972714 0.093264514 5.6 0.147158249 0.091514264 5.6 0.323257915 0.092057716 12.2 0.334030136 0.093264514 12.6 0.327761556 0.091514264 12.4 0.005318261 12.149 4,027.50 12,149.00 0.03925 0.086531438 0.104694586 18.2 0.005145957 11.748 3,981.73 11,748.00 0.03966 0.087435333 0.105788211 18.6 0.004761489 10.907 3,684.25 10,907.00 0.03512 0.077426346 0.0884412 16.3

09000064819365ee TK-PM Page 5 of 7 12/1/201409000064819365ee

TK-PM Page 6 of 7 12/1/2014**Comments**

combine TK#10 POC & RCE PM lb/hr values. combine TK#10 POC & RCE PM lb/hr values. combine TK#10 POC & RCE PM lb/hr values. combine TK#10 POC & RCE PM lb/hr values. combine TK#10 POC & RCE PM lb/hr values. combine TK#10 POC & RCE PM lb/hr values.

combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values. combine TK#2 POC, EE, & FE PM lb/hr values.

Split test for each kiln: multiply PM lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. Split test for each kiln: multiply PM lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. Split test for each kiln: multiply PM lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value.

09000064819365ee TK-PM Page 7 of 7 12/1/2014**RTI**

**Inventory Kiln ID**  **Data Source FA** **CID Old**  **FA CID**  **Test Date Run**  **Company Plant Location**  **(City/State)**

19 & 202010 Survey KOHL-TX 203

8/23-24/2010 1 Kohler Co. Brownwood, TX

19 & 202010 Survey KOHL-TX 203

8/23-24/2010 2 Kohler Co. Brownwood, TX

19 & 202010 Survey KOHL-TX 203

8/23-24/2010 3 Kohler Co. Brownwood, TX 192010 Survey KOHL-TX 2038/23-24/2010 1 Kohler Co. Brownwood, TX 192010 Survey KOHL-TX 2038/23-24/2010 2 Kohler Co. Brownwood, TX 192010 Survey KOHL-TX 2038/23-24/2010 3 Kohler Co. Brownwood, TX 202010 Survey KOHL-TX 2038/23-24/2010 1 Kohler Co. Brownwood, TX 202010 Survey KOHL-TX 2038/23-24/2010 2 Kohler Co. Brownwood, TX 202010 Survey KOHL-TX 2038/23-24/2010 3 Kohler Co. Brownwood, TX 332010 Survey KOHL-WI 204 8/3-4/2010 1 Kohler Co. Kohler, WI 332010 Survey KOHL-WI 204 8/3-4/2010 2 Kohler Co. Kohler, WI 332010 Survey KOHL-WI 204 8/3-4/2010 3 Kohler Co. Kohler, WI 22010 Survey KOHL-SC 828/10-11/2010 1 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 2 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 3 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 1 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 2 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 3 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 1 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 2 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 3 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 1 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 2 Kohler Co. Spartanburg, SC 22010 Survey KOHL-SC 828/10-11/2010 3 Kohler Co. Spartanburg, SC 72010 Survey KOHL-SC 828/12-13/2010 1 Kohler Co. Spartanburg, SC 72010 Survey KOHL-SC 828/12-13/2010 2 Kohler Co. Spartanburg, SC 72010 Survey KOHL-SC 828/12-13/2010 3 Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 1 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 2 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 3 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 1 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 2 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 3 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 1 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 2 Controlled Kohler Co. Spartanburg, SC 9 2010 SurveyKOHL-SC 8/12-13/2010 3 Controlled Kohler Co. Spartanburg, SC

POC = products of combustion stack EE = Entrance Exshaust stackFE = Fume Exhaust stack

RCE = Rapid Cool Exhaust stack WEE = Ware Exit Exhaust stack**AP CD**  **AP CD Type**  **New-Source ID Source Type**  **Test Methods**

No None TK #6/12 POC stack Tunnel Kiln EPA Method 29

No None TK #6/12 POC stack Tunnel Kiln EPA Method 29

No None TK #6/12 POC stack Tunnel Kiln EPA Method 29 No None TK #6 POC stack Tunnel Kiln EPA Method 29 No None TK #6 POC stack Tunnel Kiln EPA Method 29 No None TK #6 POC stack Tunnel Kiln EPA Method 29 No None TK #12 POC stack Tunnel Kiln EPA Method 29 No None TK #12 POC stack Tunnel Kiln EPA Method 29 No None TK #12 POC stack Tunnel Kiln EPA Method 29 No None TK #19 POC stack Tunnel Kiln EPA Method 29 No None TK #19 POC stack Tunnel Kiln EPA Method 29 No None TK #19 POC stack Tunnel Kiln EPA Method 29 No None TK #2 POC stack Tunnel Kiln EPA Method 29 No None TK #2 POC stack Tunnel Kiln EPA Method 29 No None TK #2 POC stack Tunnel Kiln EPA Method 29 No None TK #2 EE stack Tunnel Kiln EPA Method 29 No None TK #2 EE stack Tunnel Kiln EPA Method 29 No None TK #2 EE stack Tunnel Kiln EPA Method 29 No None TK #2 FE stack Tunnel Kiln EPA Method 29 No None TK #2 FE stack Tunnel Kiln EPA Method 29 No None TK #2 FE stack Tunnel Kiln EPA Method 29 No None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 29 No None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 29 No None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 29 No None TK #8 POC stack Tunnel Kiln EPA Method 29 No None TK #8 POC stack Tunnel Kiln EPA Method 29 No None TK #8 POC stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 29 Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 29**Production**

**(tph) Flow A** **ctual**

**(A CFM)**  **Flow Dry**

**Standard (DSCFM)**  **Sample**

**Volume (DSCF)**  **Sample**

**Volume (DSCM)**  **Moisture (%)**

5.09 45,474 31,210 156.42 4.43 5.45

5.19 45,122 31,085 154.59 4.38 5.46

5.19 45,864 31,376 156.40 4.43 5.78 1.58 1.61 1.61 3.51 3.58 3.58 0.83 10,910 5,746 159.95 4.53 7.39 0.83 11,214 5,877 164.64 4.66 8.01 0.88 10,694 5,605 156.18 4.42 7.99 0.79 10,724 4,139 140.83 3.99 9.11 0.79 10,945 4,198 142.91 4.05 9.52 0.82 10,749 4,131 140.15 3.97 9.58 0.79 179 154 149.90 4.24 3.22 0.79 182 155 151.32 4.28 3.24 0.82 182 156 150.64 4.27 3.30 0.79 1,621 1,062 151.79 4.30 5.28 0.79 1,556 1,029 150.23 4.25 3.89 0.82 1,512 1,001 145.68 4.13 4.51 0.79 0.79 0.82 1.85 16,990 12,918 173.48 4.91 6.20 1.85 17,218 12,829 169.41 4.80 6.31 1.85 17,030 12,875 170.21 4.82 6.36 0.41 8,466 6,669 131.21 3.72 9.23 0.41 8,326 6,574 130.07 3.68 8.87 0.40 8,432 6,683 132.93 3.76 8.81 0.41 9,378 5,352 137.83 3.90 3.44 0.41 10,476 5,952 154.88 4.39 3.50 0.40 9,776 5,557 144.61 4.09 3.54 0.41 0.41 0.40**Temp (deg F) Oxygen (%)**  **<**Fraction 1 FH (μg) Fraction

1 Status**<**Fraction 2B

BH[HNO3/H 2O2] (μg) Fraction

2 Status**<**Fraction 3A

BH [HNO3] (μg) Fraction 3A Status**<**

253.00 18.19 0.0531ADL 4.36ADL 0.0237ADL

249.50 18.11 0.0339ADL 3.97ADL 0.0183ADL

252.10 18.26 0.027ADL 4.14ADL 0.0151ADL

448.70 16.30 0.101ADL 0.586ADL 0.00746ADL 447.00 16.20 0.0329ADL 0.971ADL 0.0193ADL 445.30 16.20 0.0407ADL 0.768ADL 0.015ADL 758.20 14.24 0.346ADL 2.97ADL 0.0374ADL 759.10 14.62 0.23ADL 2.16ADL 0.0274ADL 755.90 14.09 0.472ADL 3.43ADL 0.067ADL 122.90 20.54 5.24ADL 0.4ADL < 0.005BDL 125.30 20.52 0.768ADL 0.528ADL < 0.005BDL 122.10 20.51 0.146ADL 0.19ADL < 0.005BDL 287.80 19.76 0.562ADL 1.86ADL < 0.005BDL 290.80 19.75 0.468ADL 2ADL < 0.005BDL 285.40 19.64 0.414ADL 1.78ADL 0.0164ADL

176.80 17.96 0.101ADL 2.24ADL 0.00638ADL 187.80 17.89 0.0747ADL 3.1ADL < 0.005BDL 179.40 17.93 0.208ADL 3.5ADL 0.0162ADL 133.20 19.22 0.174ADL 0.28ADL 0.0116ADL 133.00 19.07 0.339ADL 0.285ADL < 0.005BDL 132.40 18.96 0.263ADL 0.276ADL < 0.005BDL 411.00 20.00 0.0327ADL 0.18ADL 0.011ADL 412.50 20.03< 0.015BDL 0.2ADL < 0.005BDL 413.60 20.04< 0.015BDL 0.19ADL 0.012ADL <Fraction 3B

BH [KMnO4/H2 SO4] (μg) Fraction

3B Status **<** Fraction 3C

BH [HCl] (μg)Fraction

3C Status Subtotal

Filterable Subtotal

NonFilterable Total **<** Blank Fraction 1 FH (μg) **<** Blank

Fraction 2B BH[HNO 3/H2O2] (μg) **<**

2.49ADL 30.2ADL 0.0531 37.0737 37.13< 0.015 0.15<

4.61ADL 30.2ADL 0.0339 38.7983 38.83< 0.015 0.15<

30.9ADL 3.68ADL 0.027 38.7351 38.76< 0.015 0.15<

18.7ADL 4.11ADL 0.101 23.40346 23.50< 0.015 0.15< 25.1ADL 0.492ADL 0.0329 26.5823 26.62< 0.015 0.15< 25.4ADL 0.145ADL 0.0407 26.328 26.37< 0.015 0.15< 5.6ADL 0.196ADL 0.346 8.8034 9.15< 0.015 0.075< 4.52ADL 0.417ADL 0.23 7.1244 7.35< 0.015 0.075< 3.38ADL 0.0525ADL 0.472 6.9295 7.40< 0.015 0.075< 3.89ADL < 0.025BDL 5.24 4.32 9.56< 0.015 0.075< 8.1ADL 0.765ADL 0.768 9.398 10.17< 0.015 0.075< 4.29ADL < 0.025BDL 0.146 4.51 4.66< 0.015 0.075< 20.9ADL < 0.025BDL 0.562 22.79 23.35< 0.015 0.075< 21.4ADL 0.164ADL 0.468 23.569 24.04< 0.015 0.075< 14.1ADL 0.214ADL 0.414 16.1104 16.52< 0.015 0.075<

38.1ADL 0.154ADL 0.101 40.50038 40.60< 0.015 0.075< 27.6ADL 9.43ADL 0.0747 40.135 40.21< 0.015 0.075< 30ADL 7.73ADL 0.208 41.2462 41.45< 0.015 0.075< 7.89ADL 0.326ADL 0.174 8.5076 8.68< 0.015 0.075< 0.652ADL 5.07ADL 0.339 6.012 6.35< 0.015 0.075< 1.11ADL 4.66ADL 0.263 6.051 6.31< 0.015 0.075< 0.119ADL < 0.025BDL 0.0327 0.335 0.37< 0.015 0.075< 0.0435ADL 0.0505ADL 0.015 0.299 0.31< 0.015 0.075< 0.025BDL 0.0395ADL 0.015 0.2665 0.28< 0.015 0.075<Blank

Fraction 3A BH [HNO3] (μg) **<** Blank

Fraction 3B BH [KMnO4/ H2SO4] (μg) **<** Blank

Fraction 3C BH [HCl] (μg) Blank Fraction 1 FH (μg) Blank Fraction 2B BH[HNO 3/H2O2] (μg) Blank Fraction 3A BH [HNO3] (μg) Blank Fraction 3B BH [KMnO4/ H2SO4] (μg) Blank Fraction 3C BH [HCl] (μg) Total

Blank (ug) **is Mfhb >**

**8.658**

0.005< 0.025< 0.025 0 0.15 0 0 0 0.15

0.005< 0.025< 0.025 0 0.15 0 0 0 0.15

0.005< 0.025< 0.025 0 0.15 0 0 0 0.15

0.005< 0.025< 0.025 0 0.15 0 0 0 0.15 0.005< 0.025< 0.025 0 0.15 0 0 0 0.15 0.005< 0.025< 0.025 0 0.15 0 0 0 0.15 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075

0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075 0.005< 0.025< 0.025 0 0.075 0 0 0 0.075**is Mfhb >**

**Mfh Run Front** 

**Half Correction**  **Kiln Front**

**Half Correction**  **is Mbhb >**

**1 is Mbhb**  **> M bh**  **Run Back**

**Half Correction**  **Kiln Back**

**Half Correction** **is F3A b >** 

**F3A Run F3A**  **Correction**

0.0531 0.0531 4.21 4.21 0.0237

0.0339 0.0339 3.82 3.82 0.0183

0.027 0.027 3.99 3.99 0.0151

0.101 0.101 0.436 0.436 0.00746 0.0329 0.0329 0.821 0.821 0.0193 0.0407 0.0407 0.618 0.618 0.015 0.346 6.148 2.895 5.005 0.0374 0.23 1.466 2.085 4.463 0.0274 0.472 1.032 3.355 5.175 0.067 5.24 0.325 0.005 0.768 0.453 0.005 0.146 0.115 0.005 0.562 1.785 0.005 0.468 1.925 0.005 0.414 1.705 0.0164

0.101 0.101 2.165 2.165 0.00638 0.0747 0.0747 3.025 3.025 0.005 0.208 0.208 3.425 3.425 0.0162 0.174 0.205 0.0116 0.339 0.21 0.005 0.263 0.201 0.005 0.0327 0.105 0.011 0.015 0.125 0.005 0.015 0.115 0.012**Kiln F3A**

**Correction is F3Bb >** 

**F3B Run F3B**  **Correction Kiln F3B** 

**Correction is F3Cb** 

**> F3C Run F3C**  **Correction Kiln F3C** 

**Correction** Total

Blank Corrected (ug) Total

Blank Corrected (ug/dscm)

0.0237 2.49 2.49 30.2 30.2 36.98 8.35

0.0183 4.61 4.61 30.2 30.2 38.68 8.84

0.0151 30.9 30.9 3.68 3.68 38.61 8.72

0.00746 18.7 18.7 4.11 4.11 23.35 5.16 0.0193 25.1 25.1 0.492 0.492 26.47 5.68 0.015 25.4 25.4 0.145 0.145 26.22 5.93 0.0474 5.6 30.39 0.196 0.246 9.07 2.28 0.0374 4.52 34.02 0.417 1.346 7.28 1.80 0.0884 3.38 21.77 0.0525 0.2915 7.33 1.85

3.89 0.025 9.49 2.23 8.1 0.765 10.09 2.36 4.29 0.025 4.58 1.07 20.9 0.025 23.28 5.42 21.4 0.164 23.96 5.63 14.1 0.214 16.45 3.99

0.00638 38.1 38.1 0.154 0.154 40.53 8.25 0.005 27.6 27.6 9.43 9.43 40.13 8.37 0.0162 30 30 7.73 7.73 41.38 8.59

7.89 0.326 8.61 2.32 0.652 5.07 6.28 1.70 1.11 4.66 0.119 0.025 0.0435 0.0505 0.025 0.0395 0.21 0.05Total

Blank Corrected (ug/dscm @7%O2) Total

Blank Corrected (lb/hr) Total

Blank Corrected (lb/ton) **Lab Detection Level Notes;**  **Me thod Detection Limit**  **[highlighted pink if MDL NOT used]**  **1 2B** 

42.82 9.76E-04 1.92E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005

44.02 1.03E-03 1.98E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005

45.90 1.02E-03 1.97E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 3.02E-04 1.92E-04 3.19E-04 1.98E-04 3.17E-04 1.97E-04 6.74E-04 1.92E-04 7.10E-04 1.98E-04 7.07E-04 1.97E-04 15.58 1.11E-04 1.34E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 16.79 1.25E-04 1.51E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 17.53 1.24E-04 1.42E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 4.75 3.53E-05 4.48E-05ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 3.98 2.83E-05 3.59E-05ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 3.77 2.86E-05 3.50E-05ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 86.28 1.29E-06 1.63E-06ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 86.14 1.37E-06 1.74E-06ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 38.28 6.28E-07 7.70E-07ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 66.03 2.15E-05 2.74E-05ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 68.08 2.17E-05 2.76E-05ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 43.99 1.49E-05 1.83E-05ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 5.81E-05 7.38E-05 5.14E-05 6.53E-05 4.41E-05 5.41E-05 39.01 3.99E-04 2.16E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 38.64 4.02E-04 2.18E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 40.18 4.14E-04 2.24E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 19.17 5.79E-05 1.40E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 12.94 4.20E-05 1.02E-04ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005 0.82 1.05E-06 2.63E-06ALS EnvironmentalLOR = Limit of Reporting 0.015 0.005**3A 3B**  **3C Sum** 

0.005 0.025 0.025 0.075

0.005 0.025 0.025 0.075

0.005 0.025 0.025 0.075

0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075

0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075 0.005 0.025 0.025 0.075**Comments** Status based on fractions

Split test for each kiln: multiply Hg lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. ADL_ADL_ADL_ADL_ADL Split test for each kiln: multiply Hg lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. ADL_ADL_ADL_ADL_ADL Split test for each kiln: multiply Hg lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. ADL_ADL_ADL_ADL_ADL

ADL_ADL_ADL_ADL_ADL ADL_ADL_ADL_ADL_ADL ADL_ADL_ADL_ADL_ADL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_ADL_ADL_ADL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_ADL_ADL_ADL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_ADL_ADL_ADL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_BDL_ADL_BDL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_BDL_ADL_ADL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_BDL_ADL_BDL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_BDL_ADL_BDL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_BDL_ADL_ADL combine TK#2 POC, EE, & FE Hg lb/hr values. ADL_ADL_ADL_ADL_ADL

ADL_ADL_ADL_ADL_ADL ADL_ADL_BDL_ADL_ADL ADL_ADL_ADL_ADL_ADL ADL_ADL_ADL_ADL_ADL ADL_ADL_BDL_ADL_ADL Run 3 sample compromised ADL_ADL_BDL_ADL_ADL Run 1 sample compromised ADL_ADL_ADL_ADL_BDL Run 2 sample compromised BDL_ADL_BDL_ADL_ADL BDL_ADL_ADL_BDL_ADL not used in MACT analysis because of compromised runs not used in MACT analysis because of compromised runs not used in MACT analysis because of compromised runsStatus based

on fractions

ADL

ADL

ADL

ADL ADL ADL ADL ADL ADL DLL DLL DLL DLL DLL ADL

ADL DLL ADL ADL DLL DLL DLL DLL DLL**RTI**

**Inventory Kiln ID**  **New-Source ID Source Type**  **Test Methods Production**  **(tph) Flow A** **ctual**

**(A CFM)** 

19 & 20TK #6/12 POC stack Tunnel Kiln EPA Method 29 5.09 45,474

19 & 20TK #6/12 POC stack Tunnel Kiln EPA Method 29 5.19 45,122

19 & 20TK #6/12 POC stack Tunnel Kiln EPA Method 29 5.19 45,864 19TK #6 POC stack Tunnel Kiln EPA Method 29 1.58 19TK #6 POC stack Tunnel Kiln EPA Method 29 1.61 19TK #6 POC stack Tunnel Kiln EPA Method 29 1.61 20TK #12 POC stack Tunnel Kiln EPA Method 29 3.51 20TK #12 POC stack Tunnel Kiln EPA Method 29 3.58 20TK #12 POC stack Tunnel Kiln EPA Method 29 3.58 33TK #19 POC stack Tunnel Kiln EPA Method 29 0.83 10,910 33TK #19 POC stack Tunnel Kiln EPA Method 29 0.83 11,214 33TK #19 POC stack Tunnel Kiln EPA Method 29 0.88 10,694 2TK #2 POC stack Tunnel Kiln EPA Method 29 0.79 10,724 2TK #2 POC stack Tunnel Kiln EPA Method 29 0.79 10,945 2TK #2 POC stack Tunnel Kiln EPA Method 29 0.82 10,749 2TK #2 EE stack Tunnel Kiln EPA Method 29 0.79 179 2TK #2 EE stack Tunnel Kiln EPA Method 29 0.79 182 2TK #2 EE stack Tunnel Kiln EPA Method 29 0.82 182 2TK #2 FE stack Tunnel Kiln EPA Method 29 0.79 1,621 2TK #2 FE stack Tunnel Kiln EPA Method 29 0.79 1,556 2TK #2 FE stack Tunnel Kiln EPA Method 29 0.82 1,512 2TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 29 0.79 2TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 29 0.79 2TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 29 0.82 7TK #8 POC stack Tunnel Kiln EPA Method 29 1.85 16,990 7TK #8 POC stack Tunnel Kiln EPA Method 29 1.85 17,218 7TK #8 POC stack Tunnel Kiln EPA Method 29 1.85 17,030 9TK #10 POC stack Tunnel Kiln EPA Method 29 0.41 8,466 9TK #10 POC stack Tunnel Kiln EPA Method 29 0.41 8,326 9TK #10 POC stack Tunnel Kiln EPA Method 29 0.40 8,432 9TK #10 RCE stack Tunnel Kiln EPA Method 29 0.41 9,378 9TK #10 RCE stack Tunnel Kiln EPA Method 29 0.41 10,476 9TK #10 RCE stack Tunnel Kiln EPA Method 29 0.40 9,776 9TK #10 POC + RCE stacks Tunnel Kiln EPA Method 29 0.41 9TK #10 POC + RCE stacks Tunnel Kiln EPA Method 29 0.41 9TK #10 POC + RCE stacks Tunnel Kiln EPA Method 29 0.40

POC = products of combustion stack EE = Entrance Exshaust stackFE = Fume Exhaust stack

RCE = Rapid Cool Exhaust stack WEE = Ware Exit Exhaust stack**Flow Dry**

**Standard (DSCFM)**  **Sample**

**Volume (DSCF)**  **Sample**

**Volume (DSCM)**  **Moisture (%) Temp (deg F)**  **Oxygen (%) <** 

31,210 156.42 4.43 5.45 253.00 18.19

31,085 154.59 4.38 5.46 249.50 18.11

31,376 156.40 4.43 5.78 252.10 18.26

5,746 159.95 4.53 7.39 448.70 16.30 5,877 164.64 4.66 8.01 447.00 16.20 5,605 156.18 4.42 7.99 445.30 16.20 4,139 140.83 3.99 9.11 758.20 14.24 4,198 142.91 4.05 9.52 759.10 14.62 4,131 140.15 3.97 9.58 755.90 14.09 154 149.90 4.24 3.22 122.90 20.54 155 151.32 4.28 3.24 125.30 20.52 156 150.64 4.27 3.30 122.10 20.51 1,062 151.79 4.30 5.28 287.80 19.76 1,029 150.23 4.25 3.89 290.80 19.75< 1,001 145.68 4.13 4.51 285.40 19.64<

12,918 173.48 4.91 6.20 176.80 17.96< 12,829 169.41 4.80 6.31 187.80 17.89< 12,875 170.21 4.82 6.36 179.40 17.93< 6,669 131.21 3.72 9.23 133.20 19.22< 6,574 130.07 3.68 8.87 133.00 19.07< 6,683 132.93 3.76 8.81 132.40 18.96 5,352 137.83 3.90 3.44 411.00 20.00 5,952 154.88 4.39 3.50 412.50 20.03 5,557 144.61 4.09 3.54 413.60 20.04<**An timony** 

**Front Half ug <**  **An timony** 

**Back Half ug An** **timony**

**Total ug <**  **An timony** 

**Blank Front Half ug**  **< An** **timony**

**Blank Back Half ug**  **An timony** 

**Blank Front Half ug** 

6.58 0.268 6.848 6.01 0.143 6.01

5.71 0.321 6.031 6.01 0.143 6.01

5.94 0.25 6.19 6.01 0.143 6.01

2.23 0.129 2.359 2.15< 0.1 2.15 2.6 0.169 2.769 2.15< 0.1 2.15 2.65 4.65 7.3 2.15< 0.1 2.15 0.235 0.288 0.523< 0.2 0.141 0 0.262 0.255 0.517< 0.2 0.141 0 0.278 2.97 3.248< 0.2 0.141 0 1.55 0.238 1.788< 0.2 0.141 0 0.304 0.174 0.478< 0.2 0.141 0 0.204 0.237 0.441< 0.2 0.141 0 0.239 1.69 1.929< 0.2 0.141 0 0.2 0.236 0.436< 0.2 0.141 0 0.2 0.183 0.383< 0.2 0.141 0

0.2 0.305 0.505< 0.2 0.141 0 0.2 0.218 0.418< 0.2 0.141 0 0.2 0.223 0.423< 0.2 0.141 0 0.2 0.203 0.403< 0.2 0.141 0 0.2 0.189 0.389< 0.2 0.141 0

0.2 0.183 0.383< 0.2 0.141 0**An timony** 

**Blank Back Half ug**  **An timony** 

**Total Blank (ug)**  **is Mfhb >**

**8.658 is Mfhb > Mfh**  **An timony**  **Front Half Correction**  **is Mbhb > 1 is Mbhb >**  **Mbh**

0.143 6.153 0.57

0.143 6.153 Yes 0.2

0.143 6.153 Yes 0.2

0 2.15 0.08 0 2.15 0.45 0 2.15 0.5 0.141 0.141 0.235 0.141 0.141 0.262 0.141 0.141 0.278 0.141 0.141 1.55 0.141 0.141 0.304 0.141 0.141 0.204 0.141 0.141 0.239 0.141 0.141 0.2 0.141 0.141 0.2

0.141 0.141 0.2 0.141 0.141 0.2 0.141 0.141 0.2 0.141 0.141 0.2 0.141 0.141 0.2

0.141 0.141 0.2**An timony** 

**Back Half Correction**  **An timony** 

**Total Blank Corrected ug**  **An timony** 

**Total Blank Corrected**  **ug/dscm An** **timony**

**Total Blank Corrected**  **ug/dscm @ 7% O2**  **An timony** 

**Total Blank Corrected**  **lb/hr An** **timony**

**Total Blank Corrected**  **lb/ton An** **timony**

**Fraction Status** 

0.125 0.695 1.57E-01 8.05E-01 1.83E-05 3.61E-06 ADL_ADL

0.178 0.378 8.63E-02 4.30E-01 1.01E-05 1.94E-06 ADL_ADL

0.107 0.307 6.93E-02 3.65E-01 8.15E-06 1.57E-06 ADL_ADL 5.68E-06 3.61E-06 3.12E-06 1.94E-06 2.52E-06 1.57E-06 1.27E-05 3.61E-06 6.94E-06 1.94E-06 5.62E-06 1.57E-06 0.129 0.209 4.61E-02 1.39E-01 9.93E-07 1.20E-06 ADL_ADL 0.169 0.619 1.33E-01 3.93E-01 2.92E-06 3.54E-06 ADL_ADL 4.65 5.15 1.16E+00 3.44E+00 2.45E-05 2.79E-05 ADL_ADL 0.147 0.382 9.58E-02 2.00E-01 1.49E-06 1.89E-06 ADL_ADL 0.114 0.376 9.29E-02 2.06E-01 1.46E-06 1.86E-06 ADL_ADL 2.829 3.107 7.83E-01 1.60E+00 1.21E-05 1.48E-05 ADL_ADL 0.097 1.647 3.88E-01 1.50E+01 2.23E-07 2.84E-07 ADL_ADL 0.033 0.337 7.86E-02 2.88E+00 4.57E-08 5.81E-08 ADL_ADL 0.096 0.3 7.03E-02 2.51E+00 4.11E-08 5.04E-08 ADL_ADL 1.549 1.788 4.16E-01 5.07E+00 1.65E-06 2.10E-06 ADL_ADL 0.095 0.295 6.93E-02 8.38E-01 2.67E-07 3.40E-07 BDL_ADL 0.042 0.242 5.87E-02 6.47E-01 2.20E-07 2.69E-07 BDL_ADL 3.36E-06 4.27E-06 1.77E-06 2.25E-06 1.24E-05 1.52E-05 0.164 0.364 7.41E-02 3.50E-01 3.59E-06 1.94E-06 BDL_ADL 0.077 0.277 5.77E-02 2.67E-01 2.77E-06 1.50E-06 BDL_ADL 0.082 0.282 5.85E-02 2.74E-01 2.82E-06 1.53E-06 BDL_ADL 0.062 0.262 7.05E-02 5.83E-01 1.76E-06 4.28E-06 BDL_ADL 0.048 0.248 6.73E-02 5.11E-01 1.66E-06 4.02E-06 BDL_ADL

0.042 0.242 5.91E-02 9.55E-01 1.23E-06 3.08E-06 BDL_ADL**An timony** 

**Run Status An** **timony**

**MDL [other highlighted in**  **pink] Front Half ug**  **An timony** 

**MDL [other highlighted in**  **pink] Back Half ug**  **< Ar** **senic Front**

**Half ug <** **Ar senic Back** 

**Half ug Ar** **senic Total**

**ug <** 

ADL 0.2 0.1 1.65 7.89 9.54<

ADL 0.2 0.1 1.65 6.74 8.39<

ADL 0.2 0.1 1.85 8.68 10.53<

ADL 0.2 0.1 8.27 8.09 16.36< ADL 0.2 0.1 13.9 16.6 30.5< ADL 0.2 0.1 12.9 22.9 35.8< ADL 0.2 0.1 18.4 3.51 21.91< ADL 0.2 0.1 16.5 2.02 18.52< ADL 0.2 0.1 29 3.97 32.97< ADL 0.2 0.1 2.55< 0.2 2.75< ADL 0.2 0.1< 1< 0.2 1.2< ADL 0.2 0.1< 1< 0.2 1.2< ADL 0.2 0.1 1.06 0.891 1.951< DLL 0.2 0.1 1.14 0.902 2.042< DLL 0.2 0.1 1.01 0.714 1.724<

DLL 0.2 0.1 1.2 4.9 6.1< DLL 0.2 0.1 1.6 6.23 7.83< DLL 0.2 0.1 1.73 5.16 6.89< DLL 0.2 0.1 3.04 0.895 3.935< DLL 0.2 0.1 2.79 0.868 3.658<

DLL 0.2 0.1 1.1< 0.2 1.3<**Ar senic Blank** 

**Front Half ug <** **Ar senic Blank** 

**Back Half ug Ar** **senic Blank**

**Front Half ug Ar** **senic Blank**

**Back Half ug Ar** **senic Total**

**Blank ug is Mfhb >** 

**8.658 is Mfhb > Mfh** 

1< 0.2 0 0 0

1< 0.2 0 0 0

1< 0.2 0 0 0

1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0

1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0 1< 0.2 0 0 0

1< 0.2 0 0 0**Ar senic Front** 

**Half Correction**  **is Mbhb > 1 is Mbhb >**  **Mbh Ar** **senic Back**

**Half Correction**  **Ar senic Total** 

**Blank Corrected ug** **Ar senic Total** 

**Blank Corrected**  **ug/dscm Ar** **senic Total**

**Blank Corrected**  **ug/dscm @ 7% O2** 

1.65 7.89 9.54 2.15E+00 1.10E+01

1.65 6.74 8.39 1.92E+00 9.55E+00

1.85 8.68 10.53 2.38E+00 1.25E+01

8.27 8.09 16.36 3.61E+00 1.09E+01 13.9 16.6 30.5 6.54E+00 1.93E+01 12.9 22.9 35.8 8.10E+00 2.39E+01 18.4 3.51 21.91 5.49E+00 1.15E+01 16.5 2.02 18.52 4.58E+00 1.01E+01 29 3.97 32.97 8.31E+00 1.70E+01 2.55 0.2 2.75 6.48E-01 2.50E+01 1 0.2 1.2 2.80E-01 1.02E+01 1 0.2 1.2 2.81E-01 1.00E+01 1.06 0.891 1.951 4.54E-01 5.53E+00 1.14 0.902 2.042 4.80E-01 5.80E+00 1.01 0.714 1.724 4.18E-01 4.61E+00

1.2 4.9 6.1 1.24E+00 5.87E+00 1.6 6.23 7.83 1.63E+00 7.54E+00 1.73 5.16 6.89 1.43E+00 6.69E+00 3.04 0.895 3.935 1.06E+00 8.76E+00 2.79 0.868 3.658 9.93E-01 7.54E+00

1.1 0.2 1.3 3.17E-01 5.13E+00**Ar senic Total** 

**Blank Corrected**  **lb/hr Ar** **senic Total**

**Blank Corrected**  **lb/ton Ar** **senic**

**Fraction Status**  **Ar senic Run** 

**Status Ar** **senic MDL**

**[other highlighted in**  **pink] Front Half ug**  **Ar senic MDL** 

**[other highlighted in**  **pink] Back Half ug**  **< Beryllium** 

**Front Half ug**

2.52E-04 4.95E-05 ADL_ADL ADL 1 0.2< 0.2

2.23E-04 4.30E-05 ADL_ADL ADL 1 0.2< 0.2

2.79E-04 5.38E-05 ADL_ADL ADL 1 0.2< 0.2 7.80E-05 4.95E-05 6.91E-05 4.30E-05 8.66E-05 5.38E-05 1.74E-04 4.95E-05 1.54E-04 4.30E-05 1.93E-04 5.38E-05 7.77E-05 9.41E-05 ADL_ADL ADL 1 0.2< 0.2 1.44E-04 1.74E-04 ADL_ADL ADL 1 0.2< 0.2 1.70E-04 1.94E-04 ADL_ADL ADL 1 0.2< 0.2 8.52E-05 1.08E-04 ADL_ADL ADL 1 0.2< 0.2 7.20E-05 9.14E-05 ADL_ADL ADL 1 0.2< 0.2 1.29E-04 1.57E-04 ADL_ADL ADL 1 0.2< 0.2 3.73E-07 4.74E-07 ADL_BDL DLL 1 0.2< 0.2 1.63E-07 2.07E-07 BDL_BDL BDL 1 0.2< 0.2 1.65E-07 2.02E-07 BDL_BDL BDL 1 0.2< 0.2 1.81E-06 2.29E-06 ADL_ADL ADL 1 0.2< 0.2 1.85E-06 2.35E-06 ADL_ADL ADL 1 0.2< 0.2 1.57E-06 1.92E-06 ADL_ADL ADL 1 0.2< 0.2 8.74E-05 1.11E-04 7.40E-05 9.40E-05 1.30E-04 1.60E-04 6.01E-05 3.25E-05 ADL_ADL ADL 1 0.2< 0.2 7.84E-05 4.25E-05 ADL_ADL ADL 1 0.2< 0.2 6.89E-05 3.73E-05 ADL_ADL ADL 1 0.2< 0.2 2.65E-05 6.42E-05 ADL_ADL ADL 1 0.2< 0.2 2.45E-05 5.94E-05 ADL_ADL ADL 1 0.2< 0.2

6.61E-06 1.65E-05 ADL_BDL DLL 1 0.2< 0.2**< Beryllium** 

**Back Half ug Beryllium** 

**Total ug <**  **Beryllium**

**Blank Front Half ug**  **< Beryllium** 

**Blank Back Half ug**  **Beryllium**

**Blank Front Half ug**  **Beryllium**

**Blank Back Half ug** 

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0

< 0.1 0.3< 0.2< 0.1 0 0**Beryllium**

**Total Blank ug**  **is Mfhb >**

**8.658 is Mfhb > Mfh**  **Beryllium Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Beryllium**

**Back Half Correction** 

0 0.2 0.1

0 0.2 0.1

0 0.2 0.1

0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1

0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1 0 0.2 0.1

0 0.2 0.1**Beryllium**

**Total Blank Corrected ug**  **Beryllium**

**Total Blank Corrected**  **ug/dscm Beryllium** 

**Total Blank Corrected**  **ug/dscm @ 7% O2**  **Beryllium**

**Total Blank Corrected**  **lb/hr Beryllium** 

**Total Blank Corrected**  **lb/ton Beryllium** 

**Fraction Status**  **Beryllium**

**Run Status**

0.3 6.77E-02 3.47E-01 7.92E-06 1.56E-06 BDL_BDL BDL

0.3 6.85E-02 3.41E-01 7.98E-06 1.54E-06 BDL_BDL BDL

0.3 6.77E-02 3.57E-01 7.96E-06 1.53E-06 BDL_BDL BDL 2.45E-06 1.56E-06 2.47E-06 1.54E-06 2.47E-06 1.53E-06 5.46E-06 1.56E-06 5.51E-06 1.54E-06 5.49E-06 1.53E-06 0.3 6.62E-02 2.00E-01 1.43E-06 1.72E-06 BDL_BDL BDL 0.3 6.43E-02 1.90E-01 1.42E-06 1.71E-06 BDL_BDL BDL 0.3 6.78E-02 2.01E-01 1.42E-06 1.63E-06 BDL_BDL BDL 0.3 7.52E-02 1.57E-01 1.17E-06 1.48E-06 BDL_BDL BDL 0.3 7.41E-02 1.64E-01 1.17E-06 1.48E-06 BDL_BDL BDL 0.3 7.56E-02 1.54E-01 1.17E-06 1.43E-06 BDL_BDL BDL 0.3 7.07E-02 2.73E+00 4.07E-08 5.17E-08 BDL_BDL BDL 0.3 7.00E-02 2.56E+00 4.07E-08 5.17E-08 BDL_BDL BDL 0.3 7.03E-02 2.51E+00 4.11E-08 5.04E-08 BDL_BDL BDL 0.3 6.98E-02 8.51E-01 2.78E-07 3.53E-07 BDL_BDL BDL 0.3 7.05E-02 8.52E-01 2.72E-07 3.45E-07 BDL_BDL BDL 0.3 7.27E-02 8.02E-01 2.73E-07 3.34E-07 BDL_BDL BDL 1.48E-06 1.89E-06 1.48E-06 1.88E-06 1.48E-06 1.82E-06 0.3 6.11E-02 2.89E-01 2.96E-06 1.60E-06 BDL_BDL BDL 0.3 6.25E-02 2.89E-01 3.01E-06 1.63E-06 BDL_BDL BDL 0.3 6.22E-02 2.91E-01 3.00E-06 1.62E-06 BDL_BDL BDL 0.3 8.07E-02 6.68E-01 2.02E-06 4.90E-06 BDL_BDL BDL 0.3 8.15E-02 6.19E-01 2.01E-06 4.87E-06 BDL_BDL BDL

0.3 7.33E-02 1.18E+00 1.52E-06 3.82E-06 BDL_BDL BDL**Beryllium**

**MDL [other highlighted in**  **pink] Front Half ug**  **Beryllium**

**MDL [other highlighted in**  **pink] Back Half ug**  **< Cadmium** 

**Front Half ug <**  **Cadmium**

**Back Half ug Cadmium** 

**Total ug <**  **Cadmium**

**Blank Front Half ug**  **<**

0.2 0.1 0.294< 0.05 0.344< 0.1<

0.2 0.1 0.166 0.14 0.306< 0.1<

0.2 0.1 0.805< 0.05 0.855< 0.1<

0.2 0.1 0.475 0.0523 0.5273< 0.1< 0.2 0.1 0.577 0.275 0.852< 0.1< 0.2 0.1 1.11 0.0643 1.1743< 0.1< 0.2 0.1 0.269 479 479.269< 0.1< 0.2 0.1 0.23 470 470.23< 0.1< 0.2 0.1 0.233 494 494.233< 0.1< 0.2 0.1 2.54 500 502.54< 0.1< 0.2 0.1 0.943 483 483.943< 0.1< 0.2 0.1 0.25 510 510.25< 0.1< 0.2 0.1 0.2 483 483.2< 0.1< 0.2 0.1 0.345 499 499.345< 0.1< 0.2 0.1 0.379 513 513.379< 0.1<

0.2 0.1 0.116 249 249.116< 0.1< 0.2 0.1 0.124 1.23 1.354< 0.1< 0.2 0.1 0.12< 0.05 0.17< 0.1< 0.2 0.1 1.68 0.275 1.955< 0.1< 0.2 0.1 0.807 2.8 3.607< 0.1<

0.2 0.1< 0.1 0.11 0.21< 0.1<**Cadmium**

**Blank Back Half ug**  **Cadmium**

**Blank Front Half ug**  **Cadmium**

**Blank Back Half ug**  **Cadmium**

**Total Blank ug**  **is Mfhb >**

**8.658 is Mfhb > Mfh**  **Cadmium Front Half**  **Correction**

0.02 0 0 0 0.294

0.02 0 0 0 0.166

0.02 0 0 0 0.805

0.02 0 0 0 0.475 0.02 0 0 0 0.577 0.02 0 0 0 1.11 0.02 0 0 0 0.269 0.02 0 0 0 0.23 0.02 0 0 0 0.233 0.02 0 0 0 2.54 0.02 0 0 0 0.943 0.02 0 0 0 0.25 0.02 0 0 0 0.2 0.02 0 0 0 0.345 0.02 0 0 0 0.379

0.02 0 0 0 0.116 0.02 0 0 0 0.124 0.02 0 0 0 0.12 0.02 0 0 0 1.68 0.02 0 0 0 0.807

0.02 0 0 0 0.1**is Mbhb > 1 is Mbhb >**  **Mbh Cadmium** 

**Back Half Correction**  **Cadmium**

**Total Blank Corrected ug**  **Cadmium**

**Total Blank Corrected**  **ug/dscm Cadmium** 

**Total Blank Corrected**  **ug/dscm @ 7% O2**  **Cadmium**

**Total Blank Corrected**  **lb/hr**

0.05 0.34 7.77E-02 3.98E-01 9.08E-06

0.14 0.31 6.99E-02 3.48E-01 8.14E-06

0.05 0.86 1.93E-01 1.02E+00 2.27E-05 2.81E-06 2.52E-06 7.03E-06 6.27E-06 5.62E-06 1.57E-05 0.0523 0.53 1.16E-01 3.52E-01 2.51E-06 0.275 0.85 1.83E-01 5.40E-01 4.02E-06 0.0643 1.17 2.66E-01 7.85E-01 5.58E-06 479 479.27 1.20E+02 2.51E+02 1.86E-03 470 470.23 1.16E+02 2.57E+02 1.83E-03 494 494.23 1.25E+02 2.54E+02 1.93E-03 500 502.54 1.18E+02 4.57E+03 6.81E-05 483 483.94 1.13E+02 4.13E+03 6.57E-05 510 510.25 1.20E+02 4.26E+03 7.00E-05 483 483.20 1.12E+02 1.37E+03 4.47E-04 499 499.35 1.17E+02 1.42E+03 4.52E-04 513 513.38 1.24E+02 1.37E+03 4.67E-04 2.38E-03 2.35E-03 2.46E-03 249 249.12 5.07E+01 2.40E+02 2.45E-03 1.23 1.35 2.82E-01 1.30E+00 1.36E-05 0.05 0.17 3.53E-02 1.65E-01 1.70E-06 0.275 1.96 5.26E-01 4.35E+00 1.31E-05 2.8 3.61 9.79E-01 7.44E+00 2.41E-05

0.11 0.21 5.13E-02 8.29E-01 1.07E-06**Cadmium**

**Total Blank Corrected**  **lb/ton Cadmium** 

**Fraction Status**  **Cadmium**

**Run Status Cadmium** 

**MDL [other highlighted in**  **pink] Front Half ug**  **Cadmium**

**MDL [other highlighted in**  **pink] Back Half ug**  **< Chromium** 

**Front Half ug <** 

1.78E-06 ADL_BDL DLL 0.1 0.05 11.1

1.57E-06 ADL_ADL ADL 0.1 0.05 10.6

4.37E-06 ADL_BDL DLL 0.1 0.05 12.4 1.78E-06 1.57E-06 4.37E-06 1.78E-06 1.57E-06 4.37E-06 3.03E-06 ADL_ADL ADL 0.1 0.05 16.7 4.87E-06 ADL_ADL ADL 0.1 0.05 20.6 6.37E-06 ADL_ADL ADL 0.1 0.05 30.7 2.37E-03 ADL_ADL ADL 0.1 0.05 37.9 2.32E-03 ADL_ADL ADL 0.1 0.05 42.9 2.36E-03 ADL_ADL ADL 0.1 0.05 40.7 8.66E-05 ADL_ADL ADL 0.1 0.05 76.6 8.34E-05 ADL_ADL ADL 0.1 0.05 12.8 8.57E-05 ADL_ADL ADL 0.1 0.05 4.35 5.68E-04 ADL_ADL ADL 0.1 0.05 12.3 5.75E-04 ADL_ADL ADL 0.1 0.05 13.7 5.71E-04 ADL_ADL ADL 0.1 0.05 6.93 3.02E-03 2.98E-03 3.02E-03 1.33E-03 ADL_ADL ADL 0.1 0.05 7.56 7.34E-06 ADL_ADL ADL 0.1 0.05 7.23 9.21E-07 ADL_BDL DLL 0.1 0.05 6.91 3.19E-05 ADL_ADL ADL 0.1 0.05 9.38 5.85E-05 ADL_ADL ADL 0.1 0.05 7.91

2.67E-06 BDL_ADL DLL 0.1 0.05 8.71**Chromium**

**Back Half ug Chromium** 

**Total ug <**  **Chromium**

**Blank Front Half ug**  **< Chromium** 

**Blank Back Half ug**  **Chromium**

**Blank Front Half ug**  **Chromium**

**Blank Back Half ug** 

1.24 12.34 1.76 0.292 1.76 0.292

2.52 13.12 1.76 0.292 1.76 0.292

0.755 13.155 1.76 0.292 1.76 0.292

0.877 17.577 1.47 0.181 1.47 0.181 1.9 22.5 1.47 0.181 1.47 0.181 1.98 32.68 1.47 0.181 1.47 0.181 2.02 39.92 1.92 0.401 1.92 0.401 3.55 46.45 1.92 0.401 1.92 0.401 1.9 42.6 1.92 0.401 1.92 0.401 0.93 77.53 1.92 0.401 1.92 0.401 1.11 13.91 1.92 0.401 1.92 0.401 1.08 5.43 1.92 0.401 1.92 0.401 1.05 13.35 1.92 0.401 1.92 0.401 1.39 15.09 1.92 0.401 1.92 0.401 1.15 8.08 1.92 0.401 1.92 0.401

1.7 9.26 1.92 0.401 1.92 0.401 1.09 8.32 1.92 0.401 1.92 0.401 1.55 8.46 1.92 0.401 1.92 0.401 1.23 10.61 1.92 0.401 1.92 0.401 0.718 8.628 1.92 0.401 1.92 0.401

1.41 10.12 1.92 0.401 1.92 0.401**Chromium**

**Total Blank ug**  **is Mfhb >**

**8.658 is Mfhb > Mfh**  **Chromium Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Chromium**

**Back Half Correction** 

2.052 9.34 0.948

2.052 8.84 2.228

2.052 10.64 0.463

1.651 15.23 0.696 1.651 19.13 1.719 1.651 29.23 1.799 2.321 35.98 1.619 2.321 40.98 3.149 2.321 38.78 1.499 2.321 74.68 0.529 2.321 10.88 0.709 2.321 2.43 0.679 2.321 10.38 0.649 2.321 11.78 0.989 2.321 5.01 0.749

2.321 5.64 1.299 2.321 5.31 0.689 2.321 4.99 1.149 2.321 7.46 0.829 2.321 5.99 0.317

2.321 6.79 1.009**Chromium**

**Total Blank Corrected ug**  **Chromium**

**Total Blank Corrected**  **ug/dscm Chromium** 

**Total Blank Corrected**  **ug/dscm @ 7% O2**  **Chromium**

**Total Blank Corrected**  **lb/hr Chromium** 

**Total Blank Corrected**  **lb/ton Chromium** 

**Fraction Status**  **Chromium**

**Run Status**

10.29 2.32E+00 1.19E+01 2.72E-04 5.34E-05 ADL_ADL ADL

11.07 2.53E+00 1.26E+01 2.94E-04 5.67E-05 ADL_ADL ADL

11.10 2.51E+00 1.32E+01 2.95E-04 5.68E-05 ADL_ADL ADL 8.41E-05 5.34E-05 9.12E-05 5.67E-05 9.13E-05 5.68E-05 1.87E-04 5.34E-05 2.03E-04 5.67E-05 2.03E-04 5.68E-05 15.93 3.52E+00 1.06E+01 7.57E-05 9.16E-05 ADL_ADL ADL 20.85 4.47E+00 1.32E+01 9.85E-05 1.19E-04 ADL_ADL ADL 31.03 7.02E+00 2.08E+01 1.47E-04 1.68E-04 ADL_ADL ADL 37.60 9.43E+00 1.97E+01 1.46E-04 1.86E-04 ADL_ADL ADL 44.13 1.09E+01 2.41E+01 1.71E-04 2.18E-04 ADL_ADL ADL 40.28 1.01E+01 2.07E+01 1.57E-04 1.92E-04 ADL_ADL ADL 75.21 1.77E+01 6.84E+02 1.02E-05 1.30E-05 ADL_ADL ADL 11.59 2.70E+00 9.89E+01 1.57E-06 2.00E-06 ADL_ADL ADL 3.11 7.29E-01 2.60E+01 4.26E-07 5.22E-07 ADL_ADL ADL 11.03 2.57E+00 3.13E+01 1.02E-05 1.30E-05 ADL_ADL ADL 12.77 3.00E+00 3.63E+01 1.16E-05 1.47E-05 ADL_ADL ADL 5.76 1.40E+00 1.54E+01 5.23E-06 6.41E-06 ADL_ADL ADL 1.67E-04 2.12E-04 1.85E-04 2.35E-04 1.63E-04 1.99E-04 6.94 1.41E+00 6.68E+00 6.84E-05 3.70E-05 ADL_ADL ADL 6.00 1.25E+00 5.77E+00 6.01E-05 3.25E-05 ADL_ADL ADL 6.14 1.27E+00 5.96E+00 6.14E-05 3.32E-05 ADL_ADL ADL 8.29 2.23E+00 1.85E+01 5.57E-05 1.35E-04 ADL_ADL ADL 6.31 1.71E+00 1.30E+01 4.22E-05 1.02E-04 ADL_ADL ADL

7.80 1.90E+00 3.08E+01 3.96E-05 9.92E-05 ADL_ADL ADL**Chromium**

**MDL [other highlighted in**  **pink] Front Half ug**  **Chromium**

**MDL [other highlighted in**  **pink] Back Half ug**  **< Cobalt Front** 

**Half ug <**  **Cobalt Back**

**Half ug Cobalt Total** 

**ug <** **Cobalt Blank**

**Front Half ug <** 

1 0.15 0.236 0.397 0.633< 0.2<

1 0.15< 0.2 1.07 1.27< 0.2<

1 0.15< 0.2 0.19 0.39< 0.2<

1 0.15 0.507 0.263 0.77< 0.2< 1 0.15 0.397 0.318 0.715< 0.2< 1 0.15 0.496 0.384 0.88< 0.2< 1 0.15 0.722 1.41 2.132< 0.2< 1 0.15 0.642 1.18 1.822< 0.2< 1 0.15 0.603 0.422 1.025< 0.2< 1 0.15 2.48 0.661 3.141< 0.2< 1 0.15 0.461 0.169 0.63< 0.2< 1 0.15< 0.2 0.189 0.389< 0.2< 1 0.15 0.207 0.274 0.481< 0.2< 1 0.15< 0.2 0.436 0.636< 0.2< 1 0.15< 0.2 0.135 0.335< 0.2<

1 0.15< 0.2 0.429 0.629< 0.2< 1 0.15< 0.2 0.181 0.381< 0.2< 1 0.15< 0.2 0.172 0.372< 0.2< 1 0.15< 0.2 0.704 0.904< 0.2< 1 0.15< 0.2< 0.1 0.3< 0.2<

1 0.15 0.302< 0.1 0.402< 0.2<**Cobalt Blank**

**Back Half ug Cobalt Blank** 

**Front Half ug Cobalt Blank** 

**Back Half ug Cobalt Total** 

**Blank ug is Mfhb >** 

**8.658 is Mfhb > Mfh** **Cobalt Front Half**  **Correction**

0.1 0 0 0 0.236

0.1 0 0 0 0.2

0.1 0 0 0 0.2

0.1 0 0 0 0.507 0.1 0 0 0 0.397 0.1 0 0 0 0.496 0.1 0 0 0 0.722 0.1 0 0 0 0.642 0.1 0 0 0 0.603 0.1 0 0 0 2.48 0.1 0 0 0 0.461 0.1 0 0 0 0.2 0.1 0 0 0 0.207 0.1 0 0 0 0.2 0.1 0 0 0 0.2

0.1 0 0 0 0.2 0.1 0 0 0 0.2 0.1 0 0 0 0.2 0.1 0 0 0 0.2 0.1 0 0 0 0.2

0.1 0 0 0 0.302**is Mbhb > 1 is Mbhb >**  **Mbh Cobalt Back** 

**Half Correction**  **Cobalt Total**

**Blank Corrected ug**  **Cobalt Total**

**Blank Corrected**  **ug/dscm Cobalt Total** 

**Blank Corrected**  **ug/dscm @ 7% O2**  **Cobalt Total**

**Blank Corrected**  **lb/hr**

0.397 0.63 1.43E-01 7.33E-01 1.67E-05

1.07 1.27 2.90E-01 1.45E+00 3.38E-05

0.19 0.39 8.81E-02 4.64E-01 1.03E-05 5.18E-06 1.05E-05 3.21E-06 1.15E-05 2.33E-05 7.14E-06 0.263 0.77 1.70E-01 5.14E-01 3.66E-06 0.318 0.72 1.53E-01 4.54E-01 3.38E-06 0.384 0.88 1.99E-01 5.88E-01 4.18E-06 1.41 2.13 5.35E-01 1.12E+00 8.29E-06 1.18 1.82 4.50E-01 9.97E-01 7.08E-06 0.422 1.03 2.58E-01 5.27E-01 4.00E-06 0.661 3.14 7.40E-01 2.86E+01 4.26E-07 0.169 0.63 1.47E-01 5.38E+00 8.55E-08 0.189 0.39 9.12E-02 3.25E+00 5.34E-08 0.274 0.48 1.12E-01 1.36E+00 4.45E-07 0.436 0.64 1.50E-01 1.81E+00 5.76E-07 0.135 0.34 8.12E-02 8.96E-01 3.04E-07 9.16E-06 7.74E-06 4.35E-06 0.429 0.63 1.28E-01 6.05E-01 6.20E-06 0.181 0.38 7.94E-02 3.67E-01 3.82E-06 0.172 0.37 7.72E-02 3.61E-01 3.72E-06 0.704 0.90 2.43E-01 2.01E+00 6.08E-06 0.1 0.30 8.15E-02 6.19E-01 2.01E-06

0.1 0.40 9.82E-02 1.59E+00 2.04E-06**Cobalt Total**

**Blank Corrected**  **lb/ton Cobalt** 

**Fraction Status**  **Cobalt Run**

**Status Cobalt MDL** 

**[other highlighted in**  **pink] Front Half ug**  **Cobalt MDL**

**[other highlighted in**  **pink] Back Half ug**  **< Lead Front** 

**Half ug <** 

3.28E-06 ADL_ADL ADL 0.2 0.1 45.7

6.51E-06 BDL_ADL DLL 0.2 0.1 36

1.99E-06 BDL_ADL DLL 0.2 0.1 44.7 3.28E-06 6.51E-06 1.99E-06 3.28E-06 6.51E-06 1.99E-06 4.43E-06 ADL_ADL ADL 0.2 0.1 42.7 4.08E-06 ADL_ADL ADL 0.2 0.1 55 4.77E-06 ADL_ADL ADL 0.2 0.1 46.6 1.05E-05 ADL_ADL ADL 0.2 0.1 71.1 9.00E-06 ADL_ADL ADL 0.2 0.1 65.2 4.90E-06 ADL_ADL ADL 0.2 0.1 60 5.41E-07 ADL_ADL ADL 0.2 0.1 183 1.09E-07 ADL_ADL ADL 0.2 0.1 27.6 6.53E-08 BDL_ADL DLL 0.2 0.1 6.18 5.66E-07 ADL_ADL ADL 0.2 0.1 16.3 7.32E-07 BDL_ADL DLL 0.2 0.1 12.2 3.73E-07 BDL_ADL DLL 0.2 0.1 6.55 1.16E-05 9.84E-06 5.33E-06 3.36E-06 BDL_ADL DLL 0.2 0.1 8.46 2.07E-06 BDL_ADL DLL 0.2 0.1 6.95 2.01E-06 BDL_ADL DLL 0.2 0.1 6.99 1.48E-05 BDL_ADL DLL 0.2 0.1 5.8 4.87E-06 BDL_BDL BDL 0.2 0.1 4.95

5.12E-06 ADL_BDL DLL 0.2 0.1 11.2**Lead Back**

**Half ug Lead Total ug** **< Lead Blank**  **Front Half ug <**  **Lead Blank**

**Back Half ug Lead Blank** 

**Front Half ug Lead Blank** 

**Back Half ug**

1.12 46.82 0.523 0.0632 0.523 0.0632

18.7 54.7 0.523 0.0632 0.523 0.0632

0.421 45.121 0.523 0.0632 0.523 0.0632

0.446 43.146< 0.5 0.0611 0 0.0611 0.648 55.648< 0.5 0.0611 0 0.0611 0.753 47.353< 0.5 0.0611 0 0.0611 1.06 72.16 0.528< 0.05 0.528 0 2.43 67.63 0.528< 0.05 0.528 0 0.512 60.512 0.528< 0.05 0.528 0 1.34 184.34 0.528< 0.05 0.528 0 1.38 28.98 0.528< 0.05 0.528 0 0.538 6.718 0.528< 0.05 0.528 0 1.37 17.67 0.528< 0.05 0.528 0 0.705 12.905 0.528< 0.05 0.528 0 0.832 7.382 0.528< 0.05 0.528 0

0.355 8.815 0.528< 0.05 0.528 0 0.271 7.221 0.528< 0.05 0.528 0 0.208 7.198 0.528< 0.05 0.528 0 0.365 6.165 0.528< 0.05 0.528 0 0.15 5.1 0.528< 0.05 0.528 0

0.393 11.593 0.528< 0.05 0.528 0**Lead Total**

**Blank ug is Mfhb >** 

**8.658 is Mfhb > Mfh**  **Lead Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Lead Back**

**Half Correction** 

0.5862 45.177 1.0568

0.5862 35.477 18.6368

0.5862 44.177 0.3578

0.0611 42.7 0.3849 0.0611 55 0.5869 0.0611 46.6 0.6919 0.528 70.572 1.06 0.528 64.672 2.43 0.528 59.472 0.512 0.528 182.472 1.34 0.528 27.072 1.38 0.528 5.652 0.538 0.528 15.772 1.37 0.528 11.672 0.705 0.528 6.022 0.832

0.528 7.932 0.355 0.528 6.422 0.271 0.528 6.462 0.208 0.528 5.272 0.365 0.528 4.422 0.15

0.528 10.672 0.393**Lead Total**

**Blank Corrected ug**  **Lead Total**

**Blank Corrected**  **ug/dscm Lead Total** 

**Blank Corrected**  **ug/dscm @ 7% O2**  **Lead Total**

**Blank Corrected**  **lb/hr Lead Total** 

**Blank Corrected**  **lb/ton Lead Fraction** 

**Status Lead Run** 

**Status**

46.23 1.04E+01 5.35E+01 1.22E-03 2.40E-04 ADL_ADL ADL

54.11 1.24E+01 6.16E+01 1.44E-03 2.77E-04 ADL_ADL ADL

44.53 1.01E+01 5.29E+01 1.18E-03 2.28E-04 ADL_ADL ADL 3.78E-04 2.40E-04 4.46E-04 2.77E-04 3.66E-04 2.28E-04 8.42E-04 2.40E-04 9.93E-04 2.77E-04 8.16E-04 2.28E-04 43.08 9.51E+00 2.87E+01 2.05E-04 2.48E-04 ADL_ADL ADL 55.59 1.19E+01 3.53E+01 2.62E-04 3.18E-04 ADL_ADL ADL 47.29 1.07E+01 3.16E+01 2.25E-04 2.56E-04 ADL_ADL ADL 71.63 1.80E+01 3.75E+01 2.79E-04 3.54E-04 ADL_ADL ADL 67.10 1.66E+01 3.67E+01 2.61E-04 3.31E-04 ADL_ADL ADL 59.98 1.51E+01 3.09E+01 2.34E-04 2.86E-04 ADL_ADL ADL 183.81 4.33E+01 1.67E+03 2.49E-05 3.17E-05 ADL_ADL ADL 28.45 6.64E+00 2.43E+02 3.86E-06 4.91E-06 ADL_ADL ADL 6.19 1.45E+00 5.17E+01 8.49E-07 1.04E-06 ADL_ADL ADL 17.14 3.99E+00 4.86E+01 1.59E-05 2.02E-05 ADL_ADL ADL 12.38 2.91E+00 3.52E+01 1.12E-05 1.42E-05 ADL_ADL ADL 6.85 1.66E+00 1.83E+01 6.23E-06 7.63E-06 ADL_ADL ADL 3.19E-04 4.06E-04 2.76E-04 3.50E-04 2.41E-04 2.95E-04 8.29 1.69E+00 7.98E+00 8.16E-05 4.42E-05 ADL_ADL ADL 6.69 1.40E+00 6.44E+00 6.70E-05 3.63E-05 ADL_ADL ADL 6.67 1.38E+00 6.48E+00 6.67E-05 3.61E-05 ADL_ADL ADL 5.64 1.52E+00 1.26E+01 3.79E-05 9.20E-05 ADL_ADL ADL 4.57 1.24E+00 9.43E+00 3.06E-05 7.42E-05 ADL_ADL ADL

11.07 2.70E+00 4.37E+01 5.62E-05 1.41E-04 ADL_ADL ADL**Lead MDL**

**[other highlighted in**  **pink] Front Half ug**  **Lead MDL**

**[other highlighted in**  **pink] Back Half ug**  **< Ma** **nganese**

**Front Half ug <**  **Ma nganese** 

**Back Half ug Ma** **nganese**

**Total ug <**  **Ma nganese** 

**Blank Front Half ug**  **<**

0.5 0.05 1.99 1.91 3.9 3

0.5 0.05 2.04 265 267.04 3

0.5 0.05 2.15 1.13 3.28 3

0.5 0.05 3 1.13 4.13 1.98< 0.5 0.05 3.79 1.06 4.85 1.98< 0.5 0.05 4.01 0.696 4.706 1.98< 0.5 0.05 3.6 1.21 4.81 2.73< 0.5 0.05 4.09 1.55 5.64 2.73< 0.5 0.05 7.34 1.34 8.68 2.73< 0.5 0.05 59 1.65 60.65 2.73< 0.5 0.05 11 0.833 11.833 2.73< 0.5 0.05 3.82 2.13 5.95 2.73< 0.5 0.05 2.97 2.4 5.37 2.73< 0.5 0.05 3.55 12.4 15.95 2.73< 0.5 0.05 2.18 1.74 3.92 2.73<

0.5 0.05 3.6 1.86 5.46 2.73< 0.5 0.05 5.3 27.7 33 2.73< 0.5 0.05 2.8 1.14 3.94 2.73< 0.5 0.05 8.34 5.13 13.47 2.73< 0.5 0.05 2.56 1.31 3.87 2.73<

0.5 0.05 5.62 5.88 11.5 2.73<**Ma nganese** 

**Blank Back Half ug**  **Ma nganese** 

**Blank Front Half ug**  **Ma nganese** 

**Blank Back Half ug**  **Ma nganese** 

**Total Blank ug**  **MN**

**Contamination Check: Ratio**  **of BH/FH Remove** 

**Run is Mfhb >** 

**8.658**

0.21 3 0.21 3.21 0.96 no

0.21 3 0.21 3.21 129.90 yes

0.21 3 0.21 3.21 0.53 no

0.15 1.98 0 1.98 0.38 no 0.15 1.98 0 1.98 0.28 no 0.15 1.98 0 1.98 0.17 no 0.15 2.73 0 2.73 0.34 no 0.15 2.73 0 2.73 0.38 no 0.15 2.73 0 2.73 0.18 no 0.15 2.73 0 2.73 0.03 no 0.15 2.73 0 2.73 0.08 no 0.15 2.73 0 2.73 0.56 no 0.15 2.73 0 2.73 0.81 no 0.15 2.73 0 2.73 3.49 no 0.15 2.73 0 2.73 0.80 no

0.15 2.73 0 2.73 0.52 no 0.15 2.73 0 2.73 5.23 yes 0.15 2.73 0 2.73 0.41 no 0.15 2.73 0 2.73 0.62 no 0.15 2.73 0 2.73 0.51 no

0.15 2.73 0 2.73 1.05 no**is Mfhb > Mfh Ma** **nganese Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh**  **Ma nganese** 

**Back Half Correction**  **Ma nganese** 

**Total Blank Corrected ug**  **Ma nganese** 

**Total Blank Corrected**  **ug/dscm**

Yes 0.5 1.7 2.20 4.97E-01

Yes 0.5 264.79 265.29

Yes 0.5 0.92 1.42 3.21E-01

1.02 1.13 2.15 4.75E-01 1.81 1.06 2.87 6.16E-01 2.03 0.696 2.73 6.16E-01 0.87 1.21 2.08 5.22E-01 1.36 1.55 2.91 7.19E-01 4.61 1.34 5.95 1.50E+00 56.27 1.65 57.92 1.36E+01 8.27 0.833 9.10 2.12E+00 1.09 2.13 3.22 7.55E-01 0.24 2.4 2.64 6.14E-01 0.82 12.4 13.22 3.11E+00 Yes 0.5 1.74 2.24 5.43E-01

0.87 1.86 2.73 5.56E-01 2.57 27.7 30.27 0.07 1.14 1.21 2.51E-01 5.61 5.13 10.74 2.89E+00 Yes 0.5 1.31 1.81 4.91E-01

2.89 5.88 8.77 2.14E+00**Ma nganese** 

**Total Blank Corrected**  **ug/dscm @ 7% O2**  **Ma nganese** 

**Total Blank Corrected**  **lb/hr Ma** **nganese**

**Total Blank Corrected**  **lb/ton Ma** **nganese**

**Fraction Status**  **Ma nganese** 

**Run Status Ma** **nganese**

**MDL [other highlighted in**  **pink] Front Half ug**  **Ma nganese** 

**MDL [other highlighted in**  **pink] Back Half ug**  **<**

2.55E+00 5.81E-05 1.14E-05 ADL_ADL ADL 0.5 0.15

0.5 0.15

1.69E+00 3.77E-05 7.26E-06 ADL_ADL ADL 0.5 0.15

1.80E-05 1.14E-05

1.17E-05 7.26E-06 4.01E-05 1.14E-05

2.60E-05 7.26E-06 1.43E+00 1.02E-05 1.24E-05 ADL_ADL ADL 0.5 0.15 1.82E+00 1.36E-05 1.64E-05 ADL_ADL ADL 0.5 0.15 1.82E+00 1.29E-05 1.48E-05 ADL_ADL ADL 0.5 0.15 1.09E+00 8.09E-06 1.03E-05 ADL_ADL ADL 0.5 0.15 1.59E+00 1.13E-05 1.44E-05 ADL_ADL ADL 0.5 0.15 3.06E+00 2.32E-05 2.84E-05 ADL_ADL ADL 0.5 0.15 5.27E+02 7.85E-06 9.98E-06 ADL_ADL ADL 0.5 0.15 7.77E+01 1.23E-06 1.57E-06 ADL_ADL ADL 0.5 0.15 2.69E+01 4.42E-07 5.41E-07 ADL_ADL ADL 0.5 0.15 7.49E+00 2.44E-06 3.10E-06 ADL_ADL ADL 0.5 0.15 3.76E+01 1.20E-05 1.52E-05 ADL_ADL ADL 0.5 0.15 5.99E+00 2.04E-06 2.49E-06 ADL_ADL ADL 0.5 0.15

1.84E-05 2.34E-05 2.45E-05 3.12E-05 2.57E-05 3.15E-05 2.63E+00 2.69E-05 1.46E-05 ADL_ADL ADL 0.5 0.15 0.5 0.15 1.17E+00 1.21E-05 6.55E-06 ADL_ADL ADL 0.5 0.15 2.39E+01 7.22E-05 1.75E-04 ADL_ADL ADL 0.5 0.15 3.73E+00 1.21E-05 2.94E-05 ADL_ADL ADL 0.5 0.15

3.46E+01 4.46E-05 1.12E-04 ADL_ADL ADL 0.5 0.15**Nickel Front**

**Half ug <**  **Nickel Back**

**Half ug Nickel Total** 

**ug <** **Nickel Blank**

**Front Half ug <** **Nickel Blank**

**Back Half ug Nickel Blank** 

**Front Half ug**

1.69 0.86 2.55 1.21 0.109 1.21

1.41 1.83 3.24 1.21 0.109 1.21

1.63 0.609 2.239 1.21 0.109 1.21

10.1 0.927 11.027 0.936 0.173 0.936 3.96 1.93 5.89 0.936 0.173 0.936 5.92 1.27 7.19 0.936 0.173 0.936 6.46 1.48 7.94 1.34 0.204 1.34 6.01 2.8 8.81 1.34 0.204 1.34 4.31 1.56 5.87 1.34 0.204 1.34 38.3 1.02 39.32 1.34 0.204 1.34 8.08 0.835 8.915 1.34 0.204 1.34 2.58 1.06 3.64 1.34 0.204 1.34 1.99 1.56 3.55 1.34 0.204 1.34 1.72 3.49 5.21 1.34 0.204 1.34 1.49 1.13 2.62 1.34 0.204 1.34

1.68 1.18 2.86 1.34 0.204 1.34 1.42 0.997 2.417 1.34 0.204 1.34 1.34 1.1 2.44 1.34 0.204 1.34 3.12 2.27 5.39 1.34 0.204 1.34 2.85 1.27 4.12 1.34 0.204 1.34

27.4 2.12 29.52 1.34 0.204 1.34**Nickel Blank**

**Back Half ug Nickel Total** 

**Blank ug is Mfhb >** 

**8.658 is Mfhb > Mfh**  **Nickel Front Half**  **Correction is Mbhb > 1**  **is Mbhb > Mbh** 

0.109 1.319 0.48

0.109 1.319 0.2

0.109 1.319 0.42

0.173 1.109 9.164 0.173 1.109 3.024 0.173 1.109 4.984 0.204 1.544 5.12 0.204 1.544 4.67 0.204 1.544 2.97 0.204 1.544 36.96 0.204 1.544 6.74 0.204 1.544 1.24 0.204 1.544 0.65 0.204 1.544 0.38 0.204 1.544 0.15

0.204 1.544 0.34 0.204 1.544 0.08 0.204 1.544 0 0.204 1.544 1.78 0.204 1.544 1.51

0.204 1.544 26.06**Nickel Back**

**Half Correction**  **Nickel Total**

**Blank Corrected ug**  **Nickel Total**

**Blank Corrected**  **ug/dscm Nickel Total** 

**Blank Corrected**  **ug/dscm @ 7% O2**  **Nickel Total**

**Blank Corrected**  **lb/hr Nickel Total** 

**Blank Corrected**  **lb/ton Nickel** 

**Fraction Status** 

0.751 1.23 2.78E-01 1.43E+00 3.25E-05 6.39E-06 ADL_ADL

1.721 1.92 4.39E-01 2.19E+00 5.11E-05 9.85E-06 ADL_ADL

0.5 0.92 2.08E-01 1.09E+00 2.44E-05 4.70E-06 ADL_ADL 1.01E-05 6.39E-06 1.58E-05 9.85E-06 7.56E-06 4.70E-06 2.24E-05 6.39E-06 3.53E-05 9.85E-06 1.68E-05 4.70E-06 0.754 9.92 2.19E+00 6.62E+00 4.71E-05 5.70E-05 ADL_ADL 1.757 4.78 1.03E+00 3.03E+00 2.26E-05 2.73E-05 ADL_ADL 1.097 6.08 1.38E+00 4.07E+00 2.89E-05 3.30E-05 ADL_ADL 1.276 6.40 1.60E+00 3.35E+00 2.49E-05 3.16E-05 ADL_ADL 2.596 7.27 1.80E+00 3.97E+00 2.82E-05 3.59E-05 ADL_ADL 1.356 4.33 1.09E+00 2.22E+00 1.69E-05 2.07E-05 ADL_ADL 0.816 37.78 8.90E+00 3.44E+02 5.12E-06 6.51E-06 ADL_ADL 0.631 7.37 1.72E+00 6.29E+01 1.00E-06 1.27E-06 ADL_ADL 0.856 2.10 4.91E-01 1.75E+01 2.87E-07 3.52E-07 ADL_ADL 1.356 2.01 4.67E-01 5.69E+00 1.86E-06 2.36E-06 ADL_ADL 3.286 3.67 8.62E-01 1.04E+01 3.32E-06 4.22E-06 ADL_ADL 0.926 1.08 2.61E-01 2.88E+00 9.78E-07 1.20E-06 ADL_ADL 3.18E-05 4.05E-05 3.26E-05 4.14E-05 1.81E-05 2.22E-05 0.976 1.32 2.68E-01 1.27E+00 1.30E-05 7.02E-06 ADL_ADL 0.793 0.87 1.82E-01 8.40E-01 8.74E-06 4.74E-06 ADL_ADL 0.896 0.90 1.86E-01 8.70E-01 8.97E-06 4.85E-06 ADL_ADL 2.066 3.85 1.04E+00 8.56E+00 2.59E-05 6.28E-05 ADL_ADL 1.066 2.58 6.99E-01 5.31E+00 1.72E-05 4.18E-05 ADL_ADL

1.916 27.98 6.83E+00 1.10E+02 1.42E-04 3.56E-04 ADL_ADL**Nickel Run**

**Status Nickel MDL** 

**[other highlighted in**  **pink] Front Half ug**  **Nickel MDL**

**[other highlighted in**  **pink] Back Half ug**  **< Selenium** 

**Front Half ug <**  **Selenium**

**Back Half ug Selenium** 

**Total ug <** 

ADL 0.2 0.1 23.9 102 125.9<

ADL 0.2 0.1 24.4 93 117.4<

ADL 0.2 0.1 23.5 113 136.5<

ADL 0.2 0.1 9.63 12.7 22.33< ADL 0.2 0.1 9.27 34.7 43.97< ADL 0.2 0.1 8.8 33.4 42.2< ADL 0.2 0.1 9.19 53.8 62.99< ADL 0.2 0.1 9.96 40.8 50.76< ADL 0.2 0.1 16.6 82.4 99< ADL 0.2 0.1 10.1< 1 11.1< ADL 0.2 0.1< 2 1.4 3.4< ADL 0.2 0.1< 2< 1 3< ADL 0.2 0.1 6.02 10 16.02< ADL 0.2 0.1 5.53 9.07 14.6< ADL 0.2 0.1 6.03 10.7 16.73<

ADL 0.2 0.1 14.4 84.9 99.3< ADL 0.2 0.1 16.2 103 119.2< ADL 0.2 0.1 16.8 84.1 100.9< ADL 0.2 0.1 7.02 4.73 11.75< ADL 0.2 0.1 9.07 2.98 12.05<

ADL 0.2 0.1< 2< 1 3<**Selenium**

**Blank Front Half ug**  **< Selenium** 

**Blank Back Half ug**  **Selenium**

**Blank Front Half ug**  **Selenium**

**Blank Back Half ug**  **Selenium**

**Total Blank ug**  **is Mfhb >**

**8.658 is Mfhb > Mfh** 

2< 1 0 0 0

2< 1 0 0 0

2< 1 0 0 0

2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0

2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0 2< 1 0 0 0

2< 1 0 0 0**Selenium**

**Front Half Correction**  **is Mbhb > 1 is Mbhb >**  **Mbh Selenium** 

**Back Half Correction**  **Selenium**

**Total Blank Corrected ug**  **Selenium**

**Total Blank Corrected**  **ug/dscm Selenium** 

**Total Blank Corrected**  **ug/dscm @ 7% O2** 

23.9 102 125.90 2.84E+01 1.46E+02

24.4 93 117.40 2.68E+01 1.34E+02

23.5 113 136.50 3.08E+01 1.62E+02

9.63 12.7 22.33 4.93E+00 1.49E+01 9.27 34.7 43.97 9.43E+00 2.79E+01 8.8 33.4 42.20 9.54E+00 2.82E+01 9.19 53.8 62.99 1.58E+01 3.30E+01 9.96 40.8 50.76 1.25E+01 2.78E+01 16.6 82.4 99.00 2.49E+01 5.09E+01 10.1 1 11.10 2.62E+00 1.01E+02 2 1.4 3.40 7.93E-01 2.90E+01 2 1 3.00 7.03E-01 2.51E+01 6.02 10 16.02 3.73E+00 4.54E+01 5.53 9.07 14.60 3.43E+00 4.15E+01 6.03 10.7 16.73 4.06E+00 4.47E+01

14.4 84.9 99.30 2.02E+01 9.56E+01 16.2 103 119.20 2.48E+01 1.15E+02 16.8 84.1 100.90 2.09E+01 9.80E+01 7.02 4.73 11.75 3.16E+00 2.62E+01 9.07 2.98 12.05 3.27E+00 2.49E+01

2 1 3.00 7.33E-01 1.18E+01**Selenium**

**Total Blank Corrected**  **lb/hr Selenium** 

**Total Blank Corrected**  **lb/ton Selenium** 

**Fraction Status**  **Selenium Run**

**Status Selenium** 

**MDL [other highlighted in**  **pink] Front Half ug**  **Selenium**

**MDL [other highlighted in**  **pink] Back Half ug** 

3.32E-03 6.53E-04 ADL_ADL ADL 2 1

3.12E-03 6.02E-04 ADL_ADL ADL 2 1

3.62E-03 6.98E-04 ADL_ADL ADL 2 1 1.03E-03 6.53E-04 9.68E-04 6.02E-04 1.12E-03 6.98E-04 2.29E-03 6.53E-04 2.16E-03 6.02E-04 2.50E-03 6.98E-04 1.06E-04 1.28E-04 ADL_ADL ADL 2 1 2.08E-04 2.51E-04 ADL_ADL ADL 2 1 2.00E-04 2.29E-04 ADL_ADL ADL 2 1 2.45E-04 3.11E-04 ADL_ADL ADL 2 1 1.97E-04 2.51E-04 ADL_ADL ADL 2 1 3.86E-04 4.73E-04 ADL_ADL ADL 2 1 1.50E-06 1.91E-06 ADL_BDL DLL 2 1 4.61E-07 5.86E-07 BDL_ADL DLL 2 1 4.11E-07 5.04E-07 BDL_BDL BDL 2 1 1.48E-05 1.88E-05 ADL_ADL ADL 2 1 1.32E-05 1.68E-05 ADL_ADL ADL 2 1 1.52E-05 1.86E-05 ADL_ADL ADL 2 1 2.61E-04 3.32E-04 2.11E-04 2.68E-04 4.02E-04 4.92E-04 9.78E-04 5.30E-04 ADL_ADL ADL 2 1 1.19E-03 6.47E-04 ADL_ADL ADL 2 1 1.01E-03 5.46E-04 ADL_ADL ADL 2 1 7.90E-05 1.92E-04 ADL_ADL ADL 2 1 8.06E-05 1.96E-04 ADL_ADL ADL 2 1

1.52E-05 3.82E-05 BDL_BDL DLL 2 1**Comments An** **alytical M ethod** 

Split test for each kiln: multiply HAP lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. ICP-MS

Split test for each kiln: multiply HAP lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. Run 2 for manganese suspected contamination and removedICP-MS

Split test for each kiln: multiply HAP lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value. ICP-MS

ICP-MS ICP-MS ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS combine TK#2 POC, EE, & FE HAP lb/hr values. ICP-MS

ICP-MS Run 2 for manganese suspected contamination and removed ICP-MS ICP-MS ICP-MS ICP-MS Run 3 sample compromised ICP-MS Run 1 sample compromised ICP-MS Run 2 sample compromised ICP-MS ICP-MS not used in MACT analysis because of compromised runs not used in MACT analysis because of compromised runs not used in MACT analysis because of compromised runs**RTI**

**Inventory Kiln ID**  **Data Source FA** **CID Old FA** **CID Test Date**  **Run Company** 

19 & 20 2010 SurveyKOHL-TX 203

8/23-24/2010 1 Kohler Co.

19 & 20 2010 SurveyKOHL-TX 203

8/23-24/2010 2 Kohler Co.

19 & 20 2010 SurveyKOHL-TX 203

8/23-24/2010 3 Kohler Co. 19 2010 SurveyKOHL-TX 203 8/23-24/2010 1 Kohler Co. 19 2010 SurveyKOHL-TX 203 8/23-24/2010 2 Kohler Co. 19 2010 SurveyKOHL-TX 203 8/23-24/2010 3 Kohler Co. 20 2010 SurveyKOHL-TX 203 8/23-24/2010 1 Kohler Co. 20 2010 SurveyKOHL-TX 203 8/23-24/2010 2 Kohler Co. 20 2010 SurveyKOHL-TX 203 8/23-24/2010 3 Kohler Co. 33 2010 SurveyKOHL-WI 204 8/3-4/2010 1 Kohler Co. 33 2010 SurveyKOHL-WI 204 8/3-4/2010 2 Kohler Co. 33 2010 SurveyKOHL-WI 204 8/3-4/2010 3 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 1 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 2 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 3 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 1 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 2 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 3 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 1 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 2 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 3 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 1 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 2 Kohler Co. 2 2010 SurveyKOHL-SC 82 8/10-11/2010 3 Kohler Co. 7 2010 SurveyKOHL-SC 82 8/12-13/2010 1 Kohler Co. 7 2010 SurveyKOHL-SC 82 8/12-13/2010 2 Kohler Co. 7 2010 SurveyKOHL-SC 82 8/12-13/2010 3 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 1 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 2 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 3 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 1 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 2 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 3 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 1 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 2 Kohler Co. 9 2010 SurveyKOHL-SC 82 8/12-13/2010 3 Kohler Co.

POC = products of combustion stack EE = Entrance Exshaust stack FE = Fume Exhaust stack RCE = Rapid Cool Exhaust stack WEE = Ware Exit Exhaust stack**Plant Location**

**(City/State) AP** **CD AP** **CD Type New-Source ID**  **Source Type Test Methods** 

Brownwood, TX No None TK #6/12 POC stack Tunnel Kiln EPA Method 23

Brownwood, TX No None TK #6/12 POC stack Tunnel Kiln EPA Method 23

Brownwood, TX No None TK #6/12 POC stack Tunnel Kiln EPA Method 23 Brownwood, TX No None TK #6 POC stack Tunnel Kiln EPA Method 23 Brownwood, TX No None TK #6 POC stack Tunnel Kiln EPA Method 23 Brownwood, TX No None TK #6 POC stack Tunnel Kiln EPA Method 23 Brownwood, TX No None TK #12 POC stack Tunnel Kiln EPA Method 23 Brownwood, TX No None TK #12 POC stack Tunnel Kiln EPA Method 23 Brownwood, TX No None TK #12 POC stack Tunnel Kiln EPA Method 23 Kohler, WI No None TK #19 POC stack Tunnel Kiln EPA Method 23 Kohler, WI No None TK #19 POC stack Tunnel Kiln EPA Method 23 Kohler, WI No None TK #19 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 EE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 EE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 EE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 FE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 FE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 FE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #2 POC + EE + FE stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #8 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #8 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC No None TK #8 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 POC stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 RCE stack Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 23 Spartanburg, SC Yes Wet ScrubberTK #10 POC + RCE stacks Tunnel Kiln EPA Method 23**Production**

**(tph) Flow A** **ctual**

**(A CFM)**  **Flow Dry**

**Standard (DSCFM)**  **Sample Volume**

**(DSCF) Sample Volume** 

**(DSCM) Moisture (%)** 

5.09 45,703 31,570 161.45 4.57 5.22

5.19 45,176 31,415 156.61 4.43 5.30

5.19 46,007 31,903 159.87 4.53 5.22 1.58 1.61 1.61 3.51 3.58 3.58 0.83 11,012 5,746 150.96 4.27 7.82 0.83 11,302 5,931 149.66 4.24 7.84 0.88 10,675 5,585 147.66 4.18 8.18 0.79 10,839 4,141 134.04 3.80 9.73 0.79 10,825 4,150 134.55 3.81 9.35 0.82 10,871 4,178 136.13 3.85 9.66 0.79 175 151 145.99 4.13 2.80 0.79 178 151 147.57 4.18 3.04 0.82 180 155 149.97 4.25 3.09 0.79 1,623 1,084 151.95 4.30 3.75 0.79 1,557 1,033 148.27 4.20 3.65 0.82 1,528 1,022 146.98 4.16 3.85 0.79 0.79 0.82 1.85 17,045 12,956 175.28 4.96 5.96 1.85 17,170 12,674 171.88 4.87 7.02 1.85 16,949 12,871 169.44 4.80 5.93 0.41 8,631 6,860 128.58 3.64 8.30 0.41 8,414 6,669 127.13 3.60 8.48 0.40 8,370 6,653 125.98 3.57 8.40 0.41 9,523 5,455 139.02 3.94 3.15 0.41 9,881 5,651 144.14 4.08 3.07 0.40 10,221 5,818 148.96 4.22 3.38 0.41 0.41 0.40**Temp (deg F) Oxygen (%)**  **Total Dioxin/ Furan**  **(ng/dscm) Total Dioxin/** 

**Furan (ng/dscm @ 7% O2)**  **Total Dioxin/**

**Furan (g/hr) Total Dioxin/** 

**Furan (lb/hr)**

250.10 18.19 17.62 90.35 9.45E-04 2.08E-06

244.10 18.11 17.55 87.45 9.37E-04 2.07E-06

246.70 18.26 18.84 99.18 1.02E-03 2.25E-06 90.35 87.45 99.18 90.35 87.45 99.18 452.90 16.30 14.83 44.82 1.45E-04 3.19E-07 447.60 16.20 14.18 41.93 1.43E-04 3.15E-07 445.00 16.20 16.13 47.71 1.53E-04 3.38E-07 762.30 14.24 0.12 0.24 8.12E-07 1.79E-09 761.80 14.62 0.20 0.45 1.44E-06 3.17E-09 754.90 14.09 0.07 0.14 4.92E-07 1.08E-09 123.90 20.54 160.66 6,203.12 4.12E-05 9.07E-08 130.10 20.52 13.38 489.51 3.44E-06 7.58E-09 123.70 20.51 2.91 103.76 7.65E-07 1.69E-09 285.30 19.76 10.88 132.67 2.00E-05 4.42E-08 290.00 19.75 17.54 212.00 3.08E-05 6.79E-08 282.40 19.64 9.16 101.04 1.59E-05 3.51E-08 6,336.03 701.96 204.94 178.60 17.96 15.71 74.30 3.46E-04 7.63E-07 188.90 17.89 17.37 80.21 3.74E-04 8.25E-07 179.50 17.93 17.94 83.98 3.92E-04 8.65E-07 134.00 19.22 2.94 24.32 3.43E-05 7.55E-08 133.20 19.07 2.43 18.43 2.75E-05 6.06E-08 133.30 18.96 2.09 14.95 2.36E-05 5.20E-08 410.30 20.00 0.18 2.72 1.63E-06 3.60E-09 410.60 20.03 0.07 1.08 6.50E-07 1.43E-09 413.70 20.04 0.04 0.61 3.75E-07 8.27E-10 27.04 19.51 15.56**Total Dioxin/**

**Furan Emission Factor (lb/ton)**  **TEQ**

**(ng/dscm) TEQ (ng/dscm** 

**@ 7% O2) TEQ (g/hr)**  **TEQ (lb/hr) TEQ (lb/ton)** 

4.09E-07 0.24 1.24 1.29E-05 2.85E-08 5.61E-09

3.98E-07 0.22 1.09 1.17E-05 2.59E-08 4.98E-09

4.34E-07 0.24 1.28 1.32E-05 2.90E-08 5.59E-09 1.24 1.09 1.28 1.24 1.09 1.28 3.86E-07 0.16 0.49 1.59E-06 3.51E-09 4.25E-09 3.81E-07 0.15 0.45 1.53E-06 3.38E-09 4.09E-09 3.86E-07 0.19 0.55 1.77E-06 3.89E-09 4.45E-09 2.28E-09 0.00 0.01 2.19E-08 4.84E-11 6.15E-11 4.03E-09 0.00 0.01 2.22E-08 4.90E-11 6.23E-11 1.33E-09 0.00 0.01 1.97E-08 4.34E-11 5.31E-11 1.15E-07 0.88 33.98 2.25E-07 4.97E-10 6.32E-10 9.64E-09 0.09 3.46 2.43E-08 5.36E-11 6.82E-11 2.07E-09 0.03 1.18 8.72E-09 1.92E-11 2.35E-11 5.61E-08 0.10 1.24 1.87E-07 4.13E-10 5.24E-10 8.63E-08 0.13 1.59 2.30E-07 5.08E-10 6.45E-10 4.30E-08 0.09 1.03 1.63E-07 3.59E-10 4.40E-10 35.23 5.05 2.22 4.13E-07 0.17 0.83 3.85E-06 8.48E-09 4.59E-09 4.47E-07 0.20 0.91 4.26E-06 9.39E-09 5.09E-09 4.68E-07 0.20 0.94 4.39E-06 9.68E-09 5.24E-09 1.83E-07 0.03 0.26 3.62E-07 7.99E-10 1.94E-09 1.47E-07 0.02 0.19 2.76E-07 6.09E-10 1.48E-09 1.30E-07 0.03 0.18 2.83E-07 6.23E-10 1.56E-09 8.74E-09 0.00 0.03 1.78E-08 3.92E-11 9.53E-11 3.48E-09 0.00 0.03 2.03E-08 4.47E-11 1.09E-10 2.07E-09 0.00 0.02 1.20E-08 2.64E-11 6.62E-11 0.29 0.22 0.20**Overall Run**

**Status Comments** 

DLL Split test for each kiln: multiply D/F and TEQ lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value.

DLL Split test for each kiln: multiply D/F and TEQ lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value.

DLL Split test for each kiln: multiply D/F and TEQ lb/hr values and prod rate by each kiln's proportion to stack. TK#6 permitted design capacity = 2.2 tph; TK#12 permitted design capacity = 4.9 tph. Emission Factors will be the same value.

DLL DLL DLL DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together DLL add TK #2 POC, EE, & FE stack D/F and TEQ lb/hr values together

outlier, not used in MACT analysis outlier, not used in MACT analysis outlier, not used in MACT analysis DLL DLL DLL DLL add TK #10 POC & RCE stack D/F and TEQ lb/hr values together DLL add TK #10 POC & RCE stack D/F and TEQ lb/hr values together DLL add TK #10 POC & RCE stack D/F and TEQ lb/hr values together DLL add TK #10 POC & RCE stack D/F and TEQ lb/hr values together DLL add TK #10 POC & RCE stack D/F and TEQ lb/hr values together BDL add TK #10 POC & RCE stack D/F and TEQ lb/hr values together**RTI**

**Inventory Glaze line**  **ID Data Source**  **FA CID**  **Old FA CID**  **Test Date Run**  **Company Plant Location**  **(City /State)**  **AP CD Ty** **pe New-Source ID**  22010 Survey KOHL-SC 82 8/16/2010 1 Kohler Co. Spartanburg, SC Water CurtainLBM 22010 Survey KOHL-SC 82 8/16/2010 2 Kohler Co. Spartanburg, SC Water CurtainLBM 22010 Survey KOHL-SC 82 8/16/2010 3 Kohler Co. Spartanburg, SC Water CurtainLBM 142010 Survey KOHL-TX 203 8/26/2010 1 Kohler Co. Brownwood, TX Water Weir EO13 (EPN013-Manual SB) 142010 Survey KOHL-TX 203 8/26/2010 2 Kohler Co. Brownwood, TX Water Weir EO13 (EPN013-Manual SB) 142010 Survey KOHL-TX 203 8/26/2010 3 Kohler Co. Brownwood, TX Water Weir EO13 (EPN013-Manual SB) 572010 Survey KOHL-TX 203 8/26/2010 1 Kohler Co. Brownwood, TX Water CurtainSO3/SO4 572010 Survey KOHL-TX 203 8/26/2010 2 Kohler Co. Brownwood, TX Water CurtainSO3/SO4 572010 Survey KOHL-TX 203 8/26/2010 3 Kohler Co. Brownwood, TX Water CurtainSO3/SO4 32010 Survey KOHL-SC 82 8/16-17/2010 1 Kohler Co. Spartanburg, SC Water CurtainBBM 32010 Survey KOHL-SC 82 8/16-17/2010 2 Kohler Co. Spartanburg, SC Water CurtainBBM 32010 Survey KOHL-SC 82 8/16-17/2010 3 Kohler Co. Spartanburg, SC Water CurtainBBM 152010 Survey KOHL-TX 203 8/26/2010 1 Kohler Co. Brownwood, TX Water Weir EO14 (EPN014-Bowl SM 1) 152010 Survey KOHL-TX 203 8/26/2010 2 Kohler Co. Brownwood, TX Water Weir EO14 (EPN014-Bowl SM 1) 152010 Survey KOHL-TX 203 8/26/2010 3 Kohler Co. Brownwood, TX Water Weir EO14 (EPN014-Bowl SM 1) 82010 Survey KOHL-SC 82 8/16-17/2010 1 Kohler Co. Spartanburg, SC Water CurtainNTM 82010 Survey KOHL-SC 82 8/16-17/2010 2 Kohler Co. Spartanburg, SC Water CurtainNTM 82010 Survey KOHL-SC 82 8/16-17/2010 3 Kohler Co. Spartanburg, SC Water CurtainNTM 192010 Survey KOHL-TX 203 8/25/2010 1 Kohler Co. Brownwood, TX Water CurtainSR1 (EPN 104-1P) 192010 Survey KOHL-TX 203 8/25/2010 2 Kohler Co. Brownwood, TX Water CurtainSR1 (EPN 104-1P) 192010 Survey KOHL-TX 203 8/25/2010 3 Kohler Co. Brownwood, TX Water CurtainSR1 (EPN 104-1P) 392010 Survey KOHL-TX 203 8/26/2010 1 Kohler Co. Brownwood, TX Water CurtainSR5 (EPN251-Robot) 392010 Survey KOHL-TX 203 8/26/2010 2 Kohler Co. Brownwood, TX Water CurtainSR5 (EPN251-Robot) 392010 Survey KOHL-TX 203 8/26/2010 3 Kohler Co. Brownwood, TX Water CurtainSR5 (EPN251-Robot) 482010 Survey KOHL-WI 204 8/5/2010 1 Kohler Co. Kohler, WI Water CurtainP18-Q24/S18 482010 Survey KOHL-WI 204 8/5/2010 2 Kohler Co. Kohler, WI Water CurtainP18-Q24/S18 482010 Survey KOHL-WI 204 8/5/2010 3 Kohler Co. Kohler, WI Water CurtainP18-Q24/S18 52010 Survey KOHL-SC 82 8/16-17/2010 1 Kohler Co. Spartanburg, SC Water CurtainRobot 3 52010 Survey KOHL-SC 82 8/16-17/2010 2 Kohler Co. Spartanburg, SC Water CurtainRobot 3 52010 Survey KOHL-SC 82 8/16-17/2010 3 Kohler Co. Spartanburg, SC Water CurtainRobot 3

09000064819365ee GSB-PM Page 1 of 3 12/1/2014**Source Ty pe**  **Test Methods Glaze Spray**  **Rate (tph) Flow A**  **ctual (A** **CFM) Flow Dry** 

**Standard (DSCFM)**  **Sample**

**Volume (DSCF)**  **Sample**

**Volume (DSCM)**  **Moisture (%) Temp (deg F)**  **Oxy gen (%)**  Spray Booth-Manual EPA Method 5 0.065918216 8,337 7,749 36.44 1.03 3.02 79.70 20.62 Spray Booth-Manual EPA Method 5 0.065918216 8,134 7,552 34.14 0.97 2.89 81.00 20.65 Spray Booth-Manual EPA Method 5 0.065918216 8,008 7,383 33.76 0.96 3.36 82.30 20.65 Spray Booth-Manual EPA Method 5 0.078594796 15,298 14,718 40.58 1.15 2.12 70.00 20.90 Spray Booth-Manual EPA Method 5 0.078594796 15,380 14,805 40.80 1.16 2.09 69.90 20.67 Spray Booth-Manual EPA Method 5 0.078594796 15,184 14,653 40.41 1.14 2.29 67.50 20.67 Spray Booth-Manual EPA Method 5 0.127978342 11,997 11,275 44.19 1.25 2.07 83.30 20.65 Spray Booth-Manual EPA Method 5 0.127978342 12,062 11,314 43.26 1.23 2.14 84.00 20.69 Spray Booth-Manual EPA Method 5 0.127978342 11,886 11,050 41.25 1.17 2.14 88.30 20.67 Spray Booth-Spray Machine EPA Method 5 0.266538872 13,399 12,348 42.96 1.22 3.44 81.90 20.65 Spray Booth-Spray Machine EPA Method 5 0.266538872 12,759 11,712 42.31 1.20 3.52 83.60 20.77 Spray Booth-Spray Machine EPA Method 5 0.163803459 12,822 11,920 46.19 1.31 3.24 78.80 20.65 Spray Booth-Spray Machine EPA Method 5 0.330583159 17,339 16,278 43.54 1.23 2.87 79.00 20.66 Spray Booth-Spray Machine EPA Method 5 0.330583159 17,754 16,717 44.63 1.26 2.58 79.00 20.67 Spray Booth-Spray Machine EPA Method 5 0.330583159 17,769 16,817 45.29 1.28 2.44 77.00 20.66 Spray Booth-Spray Machine EPA Method 5 0.080909649 12,227 11,126 38.33 1.09 3.69 87.10 20.64 Spray Booth-Spray Machine EPA Method 5 0.080909649 12,315 11,207 39.35 1.11 3.60 87.20 20.64 Spray Booth-Spray Machine EPA Method 5 0.107585583 12,478 11,511 40.49 1.15 3.50 81.30 20.65 Spray Booth-Robot EPA Method 5 0.072642315 5,765 5,413 43.89 1.24 2.85 80.10 20.66 Spray Booth-Robot EPA Method 5 0.072642315 5,860 5,481 44.60 1.26 3.15 80.50 20.76 Spray Booth-Robot EPA Method 5 0.072642315 5,847 5,452 44.31 1.25 3.23 81.70 20.67 Spray Booth-Robot EPA Method 5 0.100200097 8,080 7,566 39.85 1.13 2.24 84.50 20.65 Spray Booth-Robot EPA Method 5 0.100200097 8,285 7,808 41.08 1.16 1.80 84.00 20.65 Spray Booth-Robot EPA Method 5 0.100200097 8,691 8,150 42.97 1.22 1.97 85.80 20.66 Spray Booth-Robot EPA Method 5 0.058642961 9,167 8,419 32.85 0.93 3.22 81.70 20.90 Spray Booth-Robot EPA Method 5 0.058642961 8,867 8,143 30.34 0.86 3.04 82.70 20.90 Spray Booth-Robot EPA Method 5 0.058642961 9,182 8,480 34.44 0.98 2.50 82.70 20.90 Spray Booth-Robot EPA Method 5 0.091491838 11,283 10,290 36.03 1.02 3.22 88.90 20.63 Spray Booth-Robot EPA Method 5 0.091491838 11,522 10,450 36.67 1.04 3.56 90.00 20.63 Spray Booth-Robot EPA Method 5 0.067792145 12,051 11,051 38.66 1.09 3.11 87.10 20.62

09000064819365ee GSB-PM Page 2 of 3 12/1/2014**PM fil**

**Concentration (mg/dscm)**  **PM fil**

**Concentration (gr/dscf)**  **PM fil**

**Concentration Converted to**  **( μ** **g/dscm) Calculation** 

**Check PM fil Concentration**  **(μg/dscm) PM fil** 

**Emissions (kg/hr)**  **PM fil**

**Emissions (lb/hr)**  **PM fil Emission**

**Factor (lb/ton of glaze spray** **ed) Check PM <1**  **mg** 34.828 0.01522 34,828.72 34,825.51 0.4585 1.01 15.33 35.93723276 41.267 0.01803 41,258.98 41,258.04 0.5294 1.17 17.71 39.88217232 40.126 0.01753 40,114.81 40,117.62 0.5032 1.11 16.83 38.35264722 24.978 0.01091 24,965.92 24,974.81 0.6245 1.38 17.52 28.6970851 27.139 0.01186 27,139.85 27,133.57 0.6825 1.50 19.14 31.34431127 45.616 0.01993 45,606.85 45,611.70 1.1355 2.50 31.85 52.19531687 10.669 0.00466 10,663.72 10,664.68 0.2043 0.45 3.52 13.34494732 9.592 0.00419 9,588.19 9,588.01 0.1843 0.41 3.17 11.74545429 10.188 0.00445 10,183.17 10,184.72 0.1912 0.42 3.29 11.89588911 34.627 0.01513 34,622.76 34,619.70 0.7263 1.60 6.01 42.11065598 41.945 0.01833 41,945.49 41,937.17 0.8345 1.84 6.90 50.24076659 24.505 0.01071 24,508.25 24,501.03 0.4962 1.09 6.68 32.04555621 11.598 0.00507 11,601.94 11,595.76 0.3207 0.71 2.14 14.29724538 9.061 0.00396 9,061.87 9,059.21 0.2573 0.57 1.72 11.44757818 10.526 0.0046 10,526.42 10,524.13 0.3007 0.66 2.01 13.4980722 20.106 0.00878 20,091.73 20,102.42 0.38 0.84 10.35 21.81601654 19.145 0.00837 19,153.51 19,143.09 0.3645 0.80 9.93 21.32781967 19.164 0.00837 19,153.51 19,159.07 0.3747 0.83 7.68 21.9646486 6.034 0.00264 6,041.25 6,035.30 0.0555 0.12 1.68 7.501515012 4.157 0.00182 4,164.80 4,155.65 0.0387 0.09 1.17 5.247714916 3.906 0.00171 3,913.08 3,907.87 0.0362 0.08 1.10 4.902844112 8.861 0.00387 8,855.92 8,860.44 0.1139 0.25 2.51 9.999111607 9.586 0.00419 9,588.19 9,588.02 0.1272 0.28 2.80 11.15250756 14.71 0.00643 14,714.10 14,710.83 0.2037 0.45 4.48 17.9010227 13.277 0.0058 13,272.44 13,276.35 0.1899 0.42 7.14 12.34901886 13.967 0.0061 13,958.95 13,964.02 0.1932 0.43 7.26 11.99695455 11.279 0.00493 11,281.57 11,279.43 0.1625 0.36 6.11 11.00069776 14.977 0.00654 14,965.82 14,974.85 0.2618 0.58 6.31 15.27817569 10.795 0.00472 10,801.02 10,791.22 0.1916 0.42 4.62 11.20568086 12.945 0.00566 12,952.07 12,942.56 0.243 0.54 7.90 14.16713873

09000064819365ee GSB-PM Page 3 of 3 12/1/2014**RTI**

**Inventory Dryer_No**  **Data Source FA** **CID Old FA** **CID Test Date**  **Run Ty** **pe of Test**

42010 Survey KOHL-TX 203 8/25/2010 1 Uncontrolled 42010 Survey KOHL-TX 203 8/25/2010 2 Uncontrolled 42010 Survey KOHL-TX 203 8/25/2010 3 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 1 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 2 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 3 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 1 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 2 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 3 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 1 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 2 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 3 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 1 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 2 Uncontrolled 52010 Survey KOHL-TX 2038/27&30/2010 3 Uncontrolled 62010 Survey KOHL-WI 204 8/5-6/2010 1 Uncontrolled 62010 Survey KOHL-WI 204 8/5-6/2010 2 Uncontrolled 62010 Survey KOHL-WI 204 8/5-6/2010 3 Uncontrolled**Company Plant Location**  **(City/State) AP** **CD AP** **CD Type Dryer_ID**  **Proc_ Type** Kohler Co.Brownwood, TXNo None E117B Batch Ware Dryer Kohler Co.Brownwood, TXNo None E117B Batch Ware Dryer Kohler Co.Brownwood, TXNo None E117B Batch Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #2 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #2 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #2 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #3 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #3 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #3 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #5 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #5 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #5 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #2 + #3 + #5 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #2 + #3 + #5 Tunnel Ware Dryer Kohler Co.Brownwood, TXNo None E238-Stack #2 + #3 + #5 Tunnel Ware Dryer Kohler Co.Kohler, WI No None WD-1 North Ware Dryer Kohler Co.Kohler, WI No None WD-1 North Ware Dryer Kohler Co.Kohler, WI No None WD-1 North Ware Dryer**Test Methods Stack/A** **PCD ID Production**  **(tph) Flow A** **ctual**

**(A CFM)**  **Flow Dry**

**Standard (DSCFM)**  **Sample**

**Volume (DSCF)**  EPA Method 23 E117B 2.06 8,192 6,979 182.28 EPA Method 23 E117B 2.06 9,721 7,950 208.76 EPA Method 23 E117B 2.06 13,850 11,076 197.99 EPA Method 23 E238-Stack #2 3.99 3,968 3,311 159.99 EPA Method 23 E238-Stack #2 3.99 3,947 3,281 160.43 EPA Method 23 E238-Stack #2 3.95 3,772 3,157 153.72 EPA Method 23 E238-Stack #3 3.99 2,857 2,217 110.64 EPA Method 23 E238-Stack #3 3.99 2,296 1,772 111.19 EPA Method 23 E238-Stack #3 3.95 2,421 1,865 114.14 EPA Method 23 E238-Stack #5 3.99 2,387 1,977 164.94 EPA Method 23 E238-Stack #5 3.99 2,393 1,984 168.98 EPA Method 23 E238-Stack #5 3.95 2,396 1,932 165.09 EPA Method 23 E238-Stack #2 + #3 + #5 EPA Method 23 E238-Stack #2 + #3 + #5 EPA Method 23 E238-Stack #2 + #3 + #5 EPA Method 24 WD-1 1.02 3,360 2,494 148.90 EPA Method 24 WD-1 1.02 3,266 2,444 144.94 EPA Method 24 WD-1 1.42 3,339 2,507 148.93**Sample**

**Volume (DSCM)**  **Moisture (%) Temp (deg F)**  **Oxygen (%) Total Dioxin/**  **Furan (ng/dscm)**  **Total Dioxin/**

**Furan (ng/dscm @ 7% O2)**  5.16 3.23 132.20 20.30 0.19 4.296106823 5.91 2.90 158.90 20.20 0.17 3.44532369 5.61 2.49 174.50 20.25 0.05 0.969177953 4.53 7.48 116.30 19.81 0.14 1.748666355 4.54 7.71 115.90 19.75 0.07 0.867425195 4.35 7.05 116.20 19.83 0.11 1.469934834 3.13 9.73 144.80 19.85 0.07 0.960418407 3.15 9.95 145.50 19.50 0.08 0.827344699 3.23 10.45 143.30 19.44 0.08 0.77962067 4.67 2.83 150.20 20.71 0.12 8.740833514 4.78 2.79 148.70 20.34 0.03 0.852751623 4.67 4.04 157.60 20.14 0.06 1.024417667 11.44991828 2.547521517 3.273973171 4.22 7.91 179.00 20.70 0.39 26.83584307 4.10 7.12 179.10 20.80 0.22 30.52478582 4.22 7.33 177.80 20.80 0.62 86.23060432**Total Dioxin/**

**Furan (g/hr) Total Dioxin/** 

**Furan (lb/hr) Total Dioxin/** 

**Furan Emission Factor (lb/ton)**  **TEQ**

**(ng/dscm) TEQ (ng/dscm** 

**@ 7% O2) TEQ (g/hr)**  2.19901E-06 4.84799E-09 2.35566E-09 0.002375435 0.055030916 2.81682E-08 2.3439E-06 5.16742E-09 2.51087E-09 0.002081259 0.041327864 2.81159E-08 8.52964E-07 1.88046E-09 9.13727E-10 0.001074903 0.022986398 2.02301E-08 7.71538E-07 1.70095E-09 4.26736E-10 0.003371232 0.042990944 1.89683E-08 4.00118E-07 8.82109E-10 2.21304E-10 0.002279001 0.02754619 1.27063E-08 6.06951E-07 1.3381E-09 3.38984E-10 0.003010776 0.039111952 1.61497E-08 2.73297E-07 6.02516E-10 1.5116E-10 0.004771221 0.063161875 1.79734E-08 2.50853E-07 5.53036E-10 1.38746E-10 0.003658071 0.036319423 1.10121E-08 2.5944E-07 5.71968E-10 1.44898E-10 0.004132892 0.039347399 1.30939E-08 4.01376E-07 8.84884E-10 2.22E-10 0.003070493 0.224630807 1.0315E-08 1.15793E-07 2.55279E-10 6.40447E-11 0.001898174 0.047115396 6.39767E-09 1.8389E-07 4.05409E-10 1.02703E-10 0.002144365 0.03921931 7.04015E-09 0.330783627 0.11098101 0.117678662 1.63643E-06 3.60771E-09 3.52831E-09 0.002504609 0.174070302 1.06147E-08 9.1207E-07 2.01077E-09 1.96652E-09 0.003497012 0.48608472 1.4524E-08 2.64295E-06 5.82671E-09 4.10078E-09 0.004072408 0.566064776 1.73498E-08**TEQ (lb/hr) TEQ (lb/ton)** 

6.21002E-11 3.01748E-11 6.1985E-11 3.01188E-11 4.45997E-11 2.16712E-11 4.18179E-11 1.04913E-11 2.80125E-11 7.0278E-12 3.56041E-11 9.01968E-12 3.96245E-11 9.94101E-12 2.42776E-11 6.09078E-12 2.88672E-11 7.313E-12 2.27406E-11 5.70519E-12 1.41044E-11 3.53853E-12 1.55209E-11 3.93195E-12

2.34014E-11 2.28863E-11 3.202E-11 3.13153E-11 3.82497E-11 2.69197E-11**Comments**

combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values combine Stack #2, #3, and #5 D/F & TEQ ng/dscm@ 7% O2 and lb/hr values