Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

50931 Yellowstone Energy LP BLR1 petroleum cokeFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte 50931 Yellowstone Energy LP BLR1 As Received Higher Heating Value 50931 Yellowstone Energy LP BLR1 As Received % Moisture 50931 Yellowstone Energy LP BLR1 As Received % Ash 50931 Yellowstone Energy LP BLR1 As Received % Sulfur 50931 Yellowstone Energy LP BLR1 Dry basis Higher Heating Value 50931 Yellowstone Energy LP BLR1 Dry basis % Ash 50931 Yellowstone Energy LP BLR1 Dry basis % Sulfur 50931 Yellowstone Energy LP BLR1 Dry basis Antim ony 50931 Yellowstone Energy LP BLR1 Dry basis Arsenic 50931 Yellowstone Energy LP BLR1 Dry basis Beryllium 50931 Yellowstone Energy LP BLR1 Dry basis Cadmium 50931 Yellowstone Energy LP BLR1 Dry basis Chlorine 50931 Yellowstone Energy LP BLR1 Dry basis Chromium 50931 Yellowstone Energy LP BLR1 Dry basis Cobalt 50931 Yellowstone Energy LP BLR1 Dry basis Fluorine 50931 Yellowstone Energy LP BLR1 Dry basis Lead 50931 Yellowstone Energy LP BLR1 Dry basis Manganese 50931 Yellowstone Energy LP BLR1 Dry basis Mercury 50931 Yellowstone Energy LP BLR1 Dry basis Nickel 50931 Yellowstone Energy LP BLR1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3173 ASTM D3174 ASTM D4239 ASTM D5865 ASTM D3174 ASTM D4239 ASTM D6357 ASTM D4606 ASTM D6357 ASTM D6357 ASTM D4208 ASTM D6357 ASTM D6357 ASTM D3761 ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 ASTM D4606EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50931 Yellowstone Energy LP BLR1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 5/10/2010 5/10/2010 14632 Btu/lb 2 5/11/2010 5/11/2010 14657 Btu/lb 3 5/11/2010 5/11/2010 14636 Btu/lb 4 5/11/2010 5/11/2010 14657 Btu/lb 5 5/11/2010 5/11/2010 14708 Btu/lb 6 5/12/2010 5/12/2010 14710 Btu/lb 7 5/12/2010 5/12/2010 14752 Btu/lb 8 5/12/2010 5/12/2010 14720 Btu/lb 9 5/12/2010 5/12/2010 14658 Btu/lb 10 5/12/2010 5/12/2010 14699 Btu/lb 11 5/13/2010 5/13/2010 14701 Btu/lb 12 5/13/2010 5/13/2010 14652 Btu/lb 13 5/13/2010 5/13/2010 14653 Btu/lb 14 5/13/2010 5/13/2010 14660 Btu/lb 15 5/14/2010 5/14/2010 14608 Btu/lb 16 5/14/2010 5/14/2010 14559 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 2.54 0.08 5.68 15013 Btu/lb 0.08 5.83 2.85 0.11 5.54 15087 Btu/lb 0.11 5.7 3.13 0.11 5.48 15109 Btu/lb 0.11 5.66 1.95 0.13 5.76 14949 Btu/lb 0.13 5.87 2.35 0.09 5.6 15062 Btu/lb 0.09 5.73 4.01 0.03 5.21 15324 Btu/lb 0.03 5.43 4.03 0.06 5.13 15371 Btu/lb 0.06 5.35 3.94 0.05 5.17 15324 Btu/lb 0.05 5.38 4.08 0.05 5.14 15282 Btu/lb 0.05 5.36 3.90 0.16 5.18 15296 Btu/lb 0.17 5.39 2.60 0.08 5.54 15093 Btu/lb 0.08 5.69 2.65 0.09 5.56 15051 Btu/lb 0.09 5.71 3.05 0.16 5.42 15114 Btu/lb 0.16 5.59 3.53 0.19 5.29 15196 Btu/lb 0.2 5.48 1.34 0.24 5.97 14806 Btu/lb 0.24 6.05 0.86 0.17 6.09 14685 Btu/lb 0.17 6.14Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 119 ppm <0.01 μg/g 0.8 μg/g <0.1 157 ppm <0.01 μg/g 0.7 μg/g <0.1 131 ppm <0.01 μg/g 0.6 μg/g <0.1 110 ppm <0.01 μg/g 0.7 μg/g <0.1 124 ppm <0.01 μg/g 0.6 μg/g <0.1 134 ppm <0.01 μg/g 0.6 μg/g <0.1 126 ppm <0.01 μg/g 0.6 μg/g <0.1 126 ppm <0.01 μg/g 0.6 μg/g <0.1 200 ppm <0.01 μg/g 0.7 μg/g <0.1 120 ppm <0.01 μg/g 0.7 μg/g <0.1 178 ppm <0.01 μg/g 0.7 μg/g <0.1 256 ppm <0.01 μg/g 0.7 μg/g <0.1 227 ppm <0.01 μg/g 0.6 μg/g <0.1 209 ppm <0.01 μg/g 0.7 μg/g <0.1 178 ppm <0.01 μg/g 0.7 μg/g <0.1 183 ppm <0.01 μg/g 0.7 μg/g <0.1Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.5 μg/g 1 μg/g μg/g 0.03 μg/g 1 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.2 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.4 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.4 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/g μg/g 0.03 μg/g 2 μg/g 0.3 μg/g 1 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 272 μg/g 0.3 μg/g 21.5 ppm 264 μg/g 0.3 μg/g 29.6 ppm 260 μg/g 0.5 μg/g 20.6 ppm 263 μg/g 0.7 μg/g 25.7 ppm 251 μg/g 0.6 μg/g 19 ppm 233 μg/g 0.4 μg/g 24.2 ppm 230 μg/g 0.3 μg/g 20.5 ppm 238 μg/g 0.4 μg/g 22.2 ppm 271 μg/g 0.3 μg/g 12.9 ppm 277 μg/g 0.4 μg/g 10.7 ppm 292 μg/g 0.6 μg/g 8.9 ppm 275 μg/g 0.6 μg/g 9.7 ppm 243 μg/g 0.5 μg/g 12.5 ppm 275 μg/g 0.4 μg/g 12.7 ppm 304 μg/g 0.9 μg/g 9.5 ppm 314 μg/g 1 μg/g 8.7 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygenEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50931 Yellowstone Energy LP BLR1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

OxygenEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50931 Yellowstone Energy LP BLR1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50931 Yellowstone Energy LP BLR1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm