## Instructions for Emissions Testing Template

**1) Three different tabs are provided based on the type of test performed:**  **Emissions source test results should be entered in the "Emissions_Data" tab Wastewater sampling data should be entered in the "Wastewater_Data" tab**  **Cooling water system sampling data should be entered in the "CoolingWater_Data" tab**

***** Fuel gas sampling data should be entered in Refinery Testing Supplement – Version 2 for Fuel Gas**

**2) Data should be entered into the white cells only; blue cells are intended for calculations** 

**3) A list of pollutants, their CAS No./Pollutant Code, and their pollutant category are provided in the "Pollutants" tab** 

**4) Guidance for process data to report is provided below:** 

**For fluid or thermal catalytic cracking units** , “throughput/production”(in bbl/hr) is determined in terms of charged liquid material, including both fresh and recycle feed. Use coke burn

-off rate (lb/hr) as the secondary process data element. For fluid coking units, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material. Use coke burn the secondary process data element. **For delayed coking units**, “throughput/production”is determined in terms of charged liquid material over the course of a drum cycle (bbl/cycle). Use coke production rate (lb dry coke/drumcycle) as the secondary process data element. **For catalytic reforming units** , “throughput/production”is determined in terms of charged liquid material. For continuous reformers,provide actual charge rate during the test (in bbl/hr); for cyclic and semi

-regenerativereformers,provide cumulativecharge quantity s **For fluid or thermal catalytic cracking units** , “throughput/production”(in bbl/hr) is determined in terms of charged liquid material, including both fresh and recycle feed. Use coke burn

-off rate (lb/hr) as the secondary process data element. For fluid coking units, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material. Use coke burn the secondary process data element. **For delayed coking units**, “throughput/production”is determined in terms of charged liquid material over the course of a drum cycle (bbl/cycle). Use coke production rate (lb dry coke/drumcycle) as the secondary process data element. **For catalytic reforming units** , “throughput/production”is determined in terms of charged liquid material. For continuous reformers,provide actual charge rate during the test (in bbl/hr); for cyclic and semi

-regenerativereformers,provide cumulativecharge quantity s regeneration(MMbbl/charge cycle). Use coke burn

-off rate (lb/hr) as the secondary process data elementfor the coke burn chording agent addition rate (lb/hr) for rejuvenation purge as the secondary process data element. **For catalytic hydrocracking** **units**, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material (i.e., excluding hydrogen). Use hydrogen addition rate coke production rate (scf/hr using 32°F (0°C) and 1 atmosphereas “standard conditions”)as the secondaryprocess data element. **For hydrogen production units**, “throughput/production”(scf/hr using 32°F (0°C) and 1 atmosphereas “standard conditions”)is based on quantity of purified hydrogen produced. No secondary process data are required. **For asphalt blowing units**, “throughput/production”is based on quantity of asphalt in blowing still (bbl/batch). Use blowing air inlet flow rate (scf/hr using 68°F (20°C) and 1 atmosphereas “standard conditions”) as the secondaryprocess data. **For sulfur recovery units**, “throughput/production”is based on quantity of elementalsulfur (for Claus units) or other sulfur product produced***** Fuel gas sampling data should be entered in Refinery Testing Supplement – Version 2 for Fuel Gas**

**A list of pollutants, their CAS No./Pollutant Code, and their pollutant category are provided in the "Pollutants" tab** Form Approved 03/28/2011 OMB Control No. 2060-0657 Approval Expires 03/31/2014

, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material, including

For fluid coking units, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material. Use coke burn

-off rate (lb/hr) as

, “throughput/production”is determined in terms of charged liquid material over the course of a drum cycle

, “throughput/production”is determined in terms of charged liquid material. For continuous reformers,provide regenerativereformers,provide cumulativecharge quantity since last , “throughput/production”(in bbl/hr) is determined in terms of charged liquid material, including

For fluid coking units, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material. Use coke burn

-off rate (lb/hr) as

, “throughput/production”is determined in terms of charged liquid material over the course of a drum cycle

, “throughput/production”is determined in terms of charged liquid material. For continuous reformers,provide regenerativereformers,provide cumulativecharge quantity since last off rate (lb/hr) as the secondary process data elementfor the coke burn

-off vent. Use

, “throughput/production”(in bbl/hr) is determined in terms of charged liquid material (i.e., excluding C) and 1 atmosphereas “standard conditions”)as the

C) and 1 atmosphereas “standard conditions”)is based on

, “throughput/production”is based on quantity of asphalt in blowing still (bbl/batch). Use blowing air inlet flow rate

, “throughput/production”is based on quantity of elementalsulfur (for Claus units) or other sulfur product produced**Emissions Test Data**

**Instruction:** Enter APCD used during test. Enter more than 1 APCD if needed (e.g., ESP1/WS1) Enter other source

reduction measures used during emission test (e.g., low NOx burners or catalyst additives) General source description,

e.g., Fluid catalytic cracking unit; semiregenerative catalytic reforming unit; etc. Assign a unique ID for each test report Enter start date **Field:**

Facility ID

Number Unit ID

Number APCD ID(s) Combustion controls used to reduce air pollution (from combustion sources) General Description Test Report ID Test Date

(mm/dd/yyyy) PA1A1030 1232 SCR/WGS Fluid Catalytic Cracking M OH 06/22/2011 CTM027 06/24/2011 M18 07/08/2011 Form Approved 03/28/2011 OMB Control No. 2060-0657 Approval Expires 03/31/2014M29 06/23/2011 M0061 06/27/2011 M0010 07/08/2011 M0011 07/08/2011

M23 06/21/2011 M7E 06/24/2011 M6C 06/24/2011 M5/202 06/24/2011

M25A 07/08/2011 M26A 06/21/2011

M10 06/24/2011Enter the feed input rate or production rate in units as specified in table for Question 16 of Part I (see instructions tab for details) Process Throughput or Production Rate

Pollutant Name Pollutant CAS No. Pollutant Class Test Method Run 1 Hourly Production Rate (value) Run 2

Hourly Production Rate (value) Run 3

Hourly Production Rate (value) Average

Hourly Production Rate (value) Mercury 7439-97-6 Metal HAP ASTM D6784- 2813.58757 2916.48079 2916.48079 2882.183051 Ammonia 7664-41-7 Other Compounds EPA CTM027 3021.027995 3021.027995 3021.027995 3021.027995 Ethane 74-84-0 Other Compounds EPA M 18 3413.702148 3389.332357 3358.299154 3387.11122 Methane 3413.702148 3389.332357 3358.299154 3387.11122 2,2,4-Trimethylpentane 540-84-1 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Carbon Disulfide 75-15-0 Other Inorganic HAP 3413.702148 3389.332357 3358.299154 3387.11122 1,3-Butadiene 106-99-0 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 2-Propanone 3413.702148 3389.332357 3358.299154 3387.11122 Methyle Isobutyl Ketone 108-10-1 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Methylene Chloride 75-09-2 3413.702148 3389.332357 3358.299154 3387.11122 Ethylene Dibromide 106-93-4 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 1,1,1-Trichloroethane 3413.702148 3389.332357 3358.299154 3387.11122 Trichloroethylene 79-01-6 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Tetrachloroethylene 127-18-4 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Benzene 71-43-2 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Enter the pollutant information for each pollutant measured (see

pollutant tab for list of possible pollutants)Toluene 108-88-3 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122

Ethylbenzene 100-41-4 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 p+m-Xylene 106-42-3 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 o-Xylene 95-47-6 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Chlorobenzene 108-90-7 3413.702148 3389.332357 3358.299154 3387.11122 Cumene (isopropylbenzene) 98-82-8 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Hexane 110-54-3 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Total Xylene 1330-20-7 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Total Metals Metals 2813.587565 2916.480794 2916.480794 2882.183051 Hexavalent Chrome 18540-29-9 Metal HAP SW-846 M0061 3169.92513 3169.92513 3169.92513 3169.92513 Total SVOCs VOC SW-846 M00103413.702148 3389.332357 3358.299154 3387.11122 Formaldehyde 50-00-0 Volatile Organic HAP SW-846 M00113413.702148 3389.332357 3358.299154 3387.11122 Acetaldehyde 75-07-0 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Acrolein 107-02-8 Volatile Organic HAP 3413.702148 3389.332357 3358.299154 3387.11122 Propionaldehyde 3413.702148 3389.332357 3358.299154 3387.11122

Dioxins Furans and PCBs Dioxins Furans and PCBs EPA M23 2810.86263 2810.86263 2813.587565 2811.770942 NOx NOX Criteria Pollutants EPA M7E 3021.027995 3021.027995 3021.027995 3021.027995 SO2 7446-09-5 Criteria Pollutants EPA 6C 3021.027995 3021.027995 3021.027995 3021.027995 Filterable Grains/DSCF Criteria Pollutants EPA M5/M202 3021.027995 3021.027995 3021.027995 3021.027995 Organic CPM Grains/DSCF Criteria Pollutants 3021.027995 3021.027995 3021.027995 3021.027995 Inorganic CPM Grains/DSCF Criteria Pollutants 3021.027995 3021.027995 3021.027995 3021.027995 Total PM Grains/DSCF Criteria Pollutants 3021.027995 3021.027995 3021.027995 3021.027995 Total Hydrocarbon (THC) THC Surrogate EPA M25A 3413.702148 3389.332357 3358.299154 3387.11122 Hydrogen chloride 7647-01-0 Other Inorganic HAP EPA M26A 2810.86263 2810.86263 2813.587565 2811.770942 Hydrogen fluoride 7664-39-3 Other Inorganic HAP 2810.86263 2810.86263 2813.587565 2811.770942 Chlorine 7782-50-5 Other Inorganic HAP 2810.86263 2810.86263 2813.587565 2811.770942 Hydrogen cyanide (& cyanide compounds) 74-90-8 Other Inorganic HAP 2810.86263 2810.86263 2813.587565 2811.770942 Carbon monoxide 630-08-0 Criteria Pollutants EPA M10 3021.027995 3021.027995 3021.027995 3021.027995Enter the feed input rate or production rate in units as specified in table for Question 16 of Part I (see instructions tab for details) Provide other processing rate data as specified in the instructions for the type of unit tested. Secondary Processing Rate Data Outlet - Run 1 Stack Gas Parameters

Hourly Production Rate (units) Production

comment Run 1

Hourly Production Rate (value) Run 2

Hourly Production Rate (value) Run 3

Hourly Production Rate (value) Average

Hourly Production Rate (value) Hourly

Production Rate (units) Production

comment Run 1

Airflow Rate Outlet (acfm) Run 1

Airflow Rate Outlet (scfm) BBL/HR 561378 490698 BBL/HR 575210 499778 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139BBL/HR 574759 501139

BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 575890 50534 BBL/HR 580499 510841 BBL/HR 578289 505856 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139 BBL/HR 574759 501139

BBL/HR 553009 483977 BBL/HR 574656 499297 BBL/HR 574656 499297 BBL/HR 557670 485376 BBL/HR 557670 485376 BBL/HR 557670 485376 BBL/HR 557670 485376 BBL/HR 574759 501139 BBL/HR 523192 458049 BBL/HR 523192 458049 BBL/HR 523192 458049 BBL/HR 523192 458049 BBL/HR 574849 498918Outlet - Run 1 Stack Gas Parameters Outlet - Run 2 Stack Gas Parameters

Run 1 Airflow Rate Outlet (dscfm) Run 1

Gas Moisture Outlet (%) Run 1

Gas Temp Outlet (F) Run 1

Gas Pressure Outlet (in. Hg) Run 1

Gas Oxygen Outlet (%) Run 2

Airflow Rate Outlet (acfm) Run 2

Airflow Rate Outlet (scfm) Run 2

Airflow Rate Outlet (dscfm) Run 2

Gas Moisture Outlet (%) 381696 22.21 143 0.06 4 597016 520242 403982 22.35 393739 21.22 143.8 0.06 3.7 571745 496905 392288 21.05 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93393166 21.55 144.25 0.06 4 569865 502267 397151 20.93

393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 393166 21.55 144.25 0.06 4 569865 502267 397151 20.93 387774 22.99 143.67 0.06 4 580723 507012 389088 23.26 397596 22.17 143 0.06 4 581378 511041 404320 20.88 396402 21.64 144.25 0.06 4 578894 506417 393383 22.32 393166 21.55 145 0.06 4 569865 502267 397151 20.93 393166 21.55 145 0.06 4 569865 502267 397151 20.93 393166 21.55 145 0.06 4 569865 502267 397151 20.93 393166 21.55 145 0.06 4 569865 502267 397151 20.93

380441 21.39 142.375 0.06 4 572951 500633 391445 21.81 393359 21.22 143.83 0.06 4 571745 496905 392288 21.05 393359 21.22 143.83 0.06 4 571745 496905 392288 21.05 389173 19.82 142.79 0.06 4 577671 502992 395094 21.45 389173 19.82 142.79 0.06 4 577671 502992 395094 21.45 389173 19.82 142.79 0.06 4 577671 502992 395094 21.45 389173 19.82 142.79 0.06 4 577671 502992 395094 21.45 393166 21.55 145 0.06 4 569865 502267 397151 20.93 359028 21.62 143.63 0.06 4 523192 458049 359028 21.53 359028 21.62 143.63 0.06 4 523192 458049 359028 21.53 359028 21.62 143.63 0.06 4 523192 458049 359028 21.53 359028 21.62 143.63 0.06 4 523192 458049 359028 21.53 393148 21.2 145 0.06 4 572379 502194 395729 21.2Outlet - Run 3 Stack Gas Parameters

Run 2 Gas Temp Outlet (F) Run 2

Gas Pressure Outlet (in. Hg) Run 2

Gas Oxygen Outlet (%) Run 3

Airflow Rate Outlet (acfm) Run 3

Airflow Rate Outlet (scfm) Run 3

Airflow Rate Outlet (dscfm) Run 3

Gas Moisture Outlet (%) Run 3

Gas Temp Outlet (F) Run 3

Gas Pressure Outlet (in. Hg) 143 0.06 4 576091 503710 393090 21.96 143.8 0.06 143.7 0.06 3.7 574995 500040 403108 19.38 143.3 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06

142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 142.9 0.06 4 574052 501315 394952 21.22 142.7 0.06 143.75 0.06 4 569831 486644 379581 22 145.042 0.06 143.208 0.06 4 580503 510562 402041 21.26 143.33 0.06 142.95 0.06 4 562211 490745 382523 22.05 142.66 0.06 138.46 0.06 4 574052 501315 394952 21.22 144 0.06 138.46 0.06 4 574052 501315 394952 21.22 144 0.06 138.46 0.06 4 574052 501315 394952 21.22 144 0.06 138.46 0.06 4 574052 501315 394952 21.22 144 0.06

143.33 0.06 4 576091 503710 393090 21.96 143.667 0.06 143.67 0.06 4 574565 499666 402806 19.38 143.29 0.06 143.67 0.06 4 574565 499666 402806 19.38 143.29 0.06 142.54 0.06 4 586685 511159 400914 21.57 142.16 0.06 142.54 0.06 4 586685 511159 400914 21.57 142.16 0.06 142.54 0.06 4 586685 511159 400914 21.57 142.16 0.06 142.54 0.06 4 586685 511159 400914 21.57 142.16 0.06 143.9 0.06 4 574052 501315 394952 21.22 144 0.06 143.54 0.06 4 573478 500679 391148 21.88 143.83 0.06 143.54 0.06 4 573478 500679 391148 21.88 143.83 0.06 143.54 0.06 4 573478 500679 391148 21.88 143.83 0.06 143.54 0.06 4 573478 500679 391148 21.88 143.83 0.06 143.9 0.06 4 575130 501059 394334 21.3 144 0.06Outlet - Average Stack Gas Parameters Outlet - Run 1 Emissions Data

Run 3 Gas Oxygen Outlet (%) Average

Airflow Rate Outlet (acfm) Average

Airflow Rate Outlet (scfm) Average

Airflow Rate Outlet (dscfm) Average

Gas Moisture Outlet (%) Average

Gas Temp Outlet (F) Average Gas

Pressure Outlet (in. Hg) Average

Gas Oxygen Outlet (%) Run 1 Outlet

concentration 4 578161.6667 504883.3333 392922.667 22.17333333 143.2666667 0.06 4 0.0011 3.82 573983.3333 498907.6667 396378.333 20.55 143.6 0.06 3.74[<2.2] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4 5400 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4 2000 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4 1230 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.7] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4 40.14 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4 2230 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 572892 501573.6667 395089.667 21.23333333 143.2833333 0.06 4[<0.1] 4 575481.3333 348063.3333 385481 22.75 144.154 0.06 4 0.1946 4 580793.3333 510814.6667 401319 21.43666667 143.1793333 0.06 4 0.00035 4 573131.3333 501006 390769.333 22.00333333 143.2866667 0.06 4 0.000182 4 572892 501573.6667 395089.667 21.23333333 142.4866667 0.06 4 0.0072 4 572892 501573.6667 395089.667 21.23333333 142.4866667 0.06 4 0.00168 4 572892 501573.6667 395089.667 21.23333333 142.4866667 0.06 4[<0.4] 4 572892 501573.6667 395089.667 21.23333333 142.4866667 0.06 4 0

4 567350.3333 496106.6667 388325.333 21.72 143.124 0.06 4 0.0012 4 573655.3333 498622.6667 396151 20.55 143.5966667 0.06 4 4.99 4 573655.3333 498622.6667 396151 20.55 143.5966667 0.06 4 4.41 4 574008.6667 499842.3333 395060.333 20.94666667 142.4966667 0.06 4 0.0205 4 574008.6667 499842.3333 395060.333 20.94666667 142.4966667 0.06 4 0.0004 4 574008.6667 499842.3333 395060.333 20.94666667 142.4966667 0.06 4 0.0182 4 574008.6667 499842.3333 395060.333 20.94666667 142.4966667 0.06 4 0.0391 4 572892 501573.6667 395089.667 21.23333333 144.3 0.06 4 0.53 4 539954 472259 369734.667 21.67666667 143.6666667 0.06 4[<60ug] 4 539954 472259 369734.667 21.67666667 143.6666667 0.06 4[<110ug] 4 539954 472259 369734.667 21.67666667 143.6666667 0.06 4[<130ug] 4 539954 472259 369734.667 21.67666667 143.6666667 0.06 4[<3ug] 4 574119.3965 500723.6667 394403.667 21.23333333 144.3 0.06 4 13.1Enter BDL, DDL, or ADL Enter BDL, DDL, or ADL Outlet - Run 1 Emissions Data Outlet - Run 2 Emissions Data Outlet - Run 3 Emissions Data

Run 1 Outlet concentration units Run 1

Outlet Detect Flag Run 1 Outlet (lb/hr) Run 2 Outlet

concentration Run 2 Outlet

concentration units Run 2

Outlet Detect Flag Run 2 Outlet (lb/hr) Run 3 Outlet

concentration mg/dscm ADL 0.001575 8.99E-05mg/dscm ADL 0.000136 0.00026683 mg/dscm BDL 0 [<2.2] mg/dscm BDL 0 [<2.2] ppbv ADL 12.61611605 5400ppbv ADL 12.64451332 5400 ppbv ADL 2.492486685 2000ppbv ADL 2.498096955 2000 ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv DDL 0 918ppbv DDL 3.866647601 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv ADL 9.571894753 0ppbv ADL 0 687 ppbv BDL 0 [<0.7] ppbv BDL 0 [<0.7] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv ADL 0.287072154 33.5 ppbv ADL 0.240363182 27ppbv ADL 18.39522769 [<0.1] ppbv ADL 0 0

ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] ppbv BDL 0 [<0.1] mg/dscm ADL 0.2827 0.1146mg/dscm ADL 0.1669 0.06746 mg/dscm ADL 0.000521 [<0.03] mg/dscm ADL 0 [<0.03] mg/dscm ADL 0.000000058 [<1] mg/dscm ADL 0 [<1] mg/dscm ADL 0.010707 0.00784mg/dscm ADL 0.011669 0.00668 mg/dscm ADL 0.002471 0.0028mg/dscm ADL 0.004168 0.00223 mg/dscm BDL 0 [<0.4] mg/dscm BDL 0 [<0.4] mg/dscm 0 0mg/dscm 0 0

TEQ@7%02 Ng/M3 total

ADL 0.0009TEQ@7%02 Ng/M3 total ADL 0.0012 ppm ADL 13.9987 4.78ppm ADL 13.3731 3.59 ppm ADL 17.228162 6.88ppm ADL 26.8053 9.27 grain/dscf ADL 68.4922 0.0244grain/dscf ADL 82.5758 0.0276 grain/dscf ADL 1.3354 0.0004grain/dscf ADL 1.3109 0.0004 grain/dscf ADL 60.7603 0.0033grain/dscf ADL 11.143 0.0078 grain/dscf ADL 130.5879 0.0281grain/dscf ADL 95.0297 7.5559E-06 ppm ADL 1.238 0.17ppm ADL 0.39717 0.13 mg/dscm DDL 0 0.88108mg/dscm DDL 1.293851 0.71047 mg/dscm BDL 0 [<110ug] mg/dscm BDL 0 [<110ug] mg/dscm BDL 0 [<130ug] mg/dscm BDL 0 [<130ug] mg/dscm BDL 0 [<3ug] mg/dscm BDL 0 [<3ug] ppm ADL 22.39 14.9 ppm ADL 25.64 13.3Enter BDL, DDL, or ADL Note any sample collection method deviations Outlet - Run 3 Emissions Data Outlet - Average Emissions Data Comments

Run 3 Outlet concentration units Run 3

Outlet Detect Flag Run 3 Outlet (lb/hr) Average Outlet

concentration Average Outlet

concentration units Count

Outlet NonDetect Runs Average Outlet

(lb/hr) Sampling comments mg/dscm ADL 0.000417 0.000485577mg/dscm 0 0.000709333 mg/dscm BDL 0 3 0 ppbv ADL 12.62054683 0 12.62705874 ppbv ADL 2.493362047 0 2.494648562 ppbv BDL 0 3 0 ppbv DDL 0 0 1.288882534 ppbv BDL 0 3 0 ppbv ADL 5.348131015 0 4.973341922 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv ADL 0.193358361 0 0.240264566ppbv ADL 0 0 6.131742564

ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 ppbv BDL 0 3 0 mg/dscm ADL 0.09593 0 0.181843333 mg/dscm ADL 0 0 0.000173667 mg/dscm ADL 0 0 1.93333E-08 mg/dscm ADL 0.009876 0 0.010750667 mg/dscm ADL 0.003292 0 0.003310333 mg/dscm BDL 0 3 0 mg/dscm 0 0 TEQ@7%02 Ng/M3 total ADL 0 ppm ADL 10.313088 0 12.56162933 ppm ADL 37.0854 0 27.03962067 grain/dscf ADL 94.8666 0 81.9782 grain/dscf ADL 1.3078 0 1.318033333 grain/dscf ADL 26.8096 0 32.9043 grain/dscf ADL 122.984 0 116.2005333 ppm ADL 0.64638 0 0.760516667 mg/dscm DDL 1.04092 0 0.778257 mg/dscm BDL 0 3 0 mg/dscm BDL 0 3 0 mg/dscm BDL 0 3 0 ppm ADL 22.83 0 23.62Note any analytical

deviations Note any QA issues,

such as unusal blanks

Analytical comments QA Comments Other comments**Well-Mixed Assessment**

**Criteria or Description Value**  Meets definition of EBU Meets characteristics in Table 1 Meets specifications in Table 2 Calculated mixing time Forms used to calculate mixing time

**Waste Water Sampling Data**

**Instruction:** General source description, e.g., submerged aeration activated sludge unit; UNOX system; etc. Assign a unique ID for each test report **Field:**

Facility ID

Number Unit ID

Number General Description Test Report ID PA1A1030 1232 WGS Recirc Agglo Filter

Quench Form Approved 03/28/2011 OMB Control No. 2060-0657 Approval Expires 03/31/2014**F_bio Determination**

**Compound F_bio**  **First-order biorate, k1**  **(L/gMLVSS-hr) Benzene Only Spike** 

Benzene **Multi-compound Spike**

Benzene Toluene Xylene Naphthalene

Enter start date

Test Date (mm/dd/yyyy) Pollutant Name Pollutant CAS No. Pollutant Class Test Method 06/24/2011Total Dissolved Solids ATSM D5907

Total Suspended Solids ATSM D5907 06/24/2011Total Dissolved Solids ATSM D5907

Total Suspended Solids ATSM D5907 Enter the pollutant information for each pollutant measured (see

pollutant tab for list of possible pollutants)Enter the wastewater flow rate and other parameters of the wastewater of unit tested.

Process Throughput or Production Rate Average wastewater flow rate during test (m3/s) Wastewater

pH Wastewater

temperature (deg, F) Volatile suspended

solids in biological treatment unit (g/L) Total

horsepower to surface aerators (HP) Total air flow

rate to diffused aerators (scfm at 68°F) 0.018N/A N/A N/A N/A N/A 0.018 N/A N/A N/A N/A N/A 0.048 N/A N/A N/A N/A N/A 0.048 N/A N/A N/A N/A N/AEnter the wastewater flow rate and other parameters of the wastewater of unit tested. Influent Sample Results Within Biological Treatment Unit Results

Other information or comment Concentration

Value Concentration

units (μg/L or mg/L) Concentration Value Concentration units (μg/L or mg/L) 2560Mg/L N/A N/A 6376Mg/L N/A N/A 1400Mg/L N/A N/A 32170Mg/L N/A N/ANote any sample collection method deviations Note any analytical

deviations Note any QA issues,

such as unusal blanks Effluent Sample Results Comments

Concentration Value Concentration

units (μg/L or mg/L) Sampling comments Analytical comments QA Comments N/A N/A N/A N/A N/A N/A N/A N/AOther comments

Sampling is conducted**Cooling Water System Test Data**

**Instruction:** If sampling separate return lines for a single cooling tower, assign a unique ID for each return line General source description, e.g.,

cooling tower for X,Y,Z units; east heat exchange return line (serving unit XX) to cooling tower 1; etc. Assign a unique ID for each test report Enter start date **Field:**

Facility ID

Number Cooling Tower

(HE System) ID Return Line ID General Description Test Report ID Test Date

(mm/dd/yyyy) Form Approved 03/28/2011 OMB Control No. 2060-0657 Approval Expires 03/31/2014Enter the appropriate flow rate (in gallons per minute, gpm) from

measurement data, company records, or engineering analyses during the testing period

Cooling Tower Recirculation Rate (gpm) Cooling Tower

Water Make-up Rate (gpm) Return Line Flow

Rate (if sampling separate return line to a singe cooling tower) (gpm) Flow rate

comment Pollutant Name Pollutant CAS No. Pollutant Class

Enter the pollutant information for each pollutant measured (see

pollutant tab for list of possible pollutants)Note any sample collection method deviations Note any analytical

deviations Note any QA issues,

such as unusal blanks Stripping Air Concentration Liquid Concentration Comments

Measured Air Concentration (ppmv, dry basis) Test Method Liquid Concentration (ppmw) Test Method

(enter "backcalculated" if not directly measured) Sampling comments Analytical comments QA CommentsOther comments**Substance CAS Number** 

1Carbon monoxide 630-08-0 2 Particulate matter (PM)≤ 10 μm PM10-PRI 3 Filterable PM≤ 10 μm PM10-FIL 4PM≤ 2.5 μm PM25-PRI 5 Filterable PM≤ 2.5 μm PM25-FIL 6Condensable PM PM-CON 7 Nitrogen dioxide 10102-44-0 8 Nitrogen oxides NOX 9Sulfur dioxide 7446-09-5 10Volatile organic compounds VOC 11 Ethylene 74-85-1 12Acetylene 74-86-2 13 Propane 74-98-6 14Propylene 115-07-1 15 Propadiene 463-49-0 16n-Butane 106-97-8 17 Isobutane 75-28-5 18 1-Butene 106-98-9 192-Butene 107-01-7 20Isobutene 115-11-7 21 1,2-Butadiene 590-19-2 22 n-pentane 109-66-0 232-Methylbutane 78-78-4 24Cyclopentane 287-92-3 25 1,2-Pentadiene 591-95-7 26 1-cis-3-Pentadiene 1574-41-0 27 1-trans-3-Pentadiene 2004-70-8 28 1,4-Pentadiene 591-93-5 292,3-Pentadiene 591-96-8 303-Methyl-1,2-butadiene 598-25-4 312-Methyl-1,3-butadiene 78-79-5 32Cyclopentadiene 542-92-7 33Cyclohexane 110-82-7 34Methylcylcohexane 108-87-2 35 Heptane (and isomers) 142-82-5 36Octane (and isomers) 111-65-9 37 Methyl ethyl ketone 78-93-3 38Trimethylbenzene(s) 25551-13-7 39Acetaldehyde 75-07-0 40Acrolein 107-02-8 41Analine 62-53-3 42 Benzene 71-43-2 43 Bromomethane 74-83-9441,3-Butadiene 106-99-0

45Chloroethane 75-00-3 46Chloroform 67-66-3 47Chloromethane 74-87-3 48Cumene 98-82-8 49 1,2-Dibromoethane 106-93-4 501,4-Dichlorobenzene 106-46-7 51 1,1-Dichloroethane 75-34-3 52 1,2-Dichloroethane 107-06-2 53 1,1-Dichloroethylene 75-35-4 541,2-Dichloropropane 78-87-5 55 1,3-Dichloropropene 542-75-6 56 Diethanolamine 111-42-2 57 Ethylbenzene 100-41-4 58 Formaldehyde 50-00-0 59 Hexachloroethane 67-72-1 60n-Hexane 110-54-3 61 Methanol 67-56-1 62 Methyl isobutyl ketone 108-10-1 63 Methyl tert-butyl ether 1634-04-4 64Styrene 100-42-5 65 1,1,2,2-Tetrachloroethane 79-34-5 66Tetrachloroethylene 127-18-4 67Toluene 108-88-3 68 1,1,2-Trichloroethane 79-00-5 69Trichloroethylene 79-01-6 70Triethylamine 121-44-8 712,2,4-Trimethylpentane 540-84-1 72Vinyl bromide 593-60-2 73Vinyl chloride 75-01-4 74o-Xylene 95-47-6 75 m-Xylene 108-38-3 76p-Xylene 106-42-3 77Xylenes (total) 1330-20-7 78Acenaphthene 83-32-9 79Acenaphthylene 208-96-8 80Anthracene 120-12-7 81 Benzo(a)anthracene 56-55-3 82 Benzo(a)pyrene 50-32-8 83 Benzo(b)fluoranthene 205-99-2 84Benzo(e)pyrene 192-97-2 85 Benzo(g,h,i)perylene 191-24-2 86 Benzo(k)fluoranthene 207-08-9 87 Biphenyl 92-52-488 Bis(2-ethyl hexyl)phthalate 117-81-7

892-Chloronaphthalene 91-58-7 90m-Cresol 108-39-4 91o-Cresol 95-48-7 92 p-Cresol 106-44-5 93Cresols (total) 1319-77-3 94Chrysene 218-01-9 95 Dibenz(a,h)anthracene 53-70-3 96di-n-Butyl phthalate 84-74-2 97 Diethyl-phthalate 84-66-2 987,12-Dimethylbenz(a) anthracene 57-97-6 99 Fluoranthene 206-44-0 100Fluorene 86-73-7 101 Indeno(1,2,3-cd) pyrene 193-39-5 1023-Methylchloranthrene 56-49-5 1032-Methylnaphthalene 91-57-6 104Chrysene 218-01-9 105 Naphthalene 91-20-3 106Perylene 198-55-0 107 Phenanthrene 85-01-8 108 Phenol 108-95-2 109 Pyrene 129-00-0 110Dioxin: 4D 2378 1746-01-6 111 Dioxin: 5D 12378 40321-76-4 112 Dioxin: 6D 123478 39227-28-6 113 Dioxin: 6D 123678 57653-85-7 114Dioxin: 6D 123789 19408-74-3 115 Dioxin: 7D 1234678 35822-46-9 116Dioxin: 8D 3268-87-9 117 Dibenzofurans 132-64-9 118 Furan: 4F 2378 51207-31-9 119 Furan: 5F 12378 57117-41-6 120Furan: 5F 23478 57117-31-4 121 Furan: 6F 123478 70648-26-9 122 Furan: 6F 123678 57117-44-9 123 Furan: 6F 123789 72918-21-9 124Furan: 6F 234678 60851-34-5 125 Furan: 7F 1234678 67562-39-4 126Furan: 7F 1234789 55673-89-7 127 Furan: 8F 39001-02-0 128 Polychlorinated biphenyls (total) 1336-36-3 129Antimony 7440-36-0 130Arsenic 7440-38-2 131 Beryllium 7440-41-7132Cadmium 7440-43-9

133Chromium (hexavalent) 18540-29-9 134Chromium (total) 7440-47-3 135Cobalt 7440-48-4 136Lead 7439-92-1 137 Manganese 7439-96-5 138 Mercury 7439-97-6 139 Nickel 7440-02-0 140Selenium 7782-49-2 141Carbon disulfide 75-15-0 142Carbonyl sulfide 463-58-1 143Chlorine 7782-50-5 144Hydrogen chloride 7647-01-0 145 Hydrogen cyanide (& cyanide compounds) 74-90-8 146Hydrogen fluoride 7664-39-3 147 Phosphorus 7723-14-0 148Ammonia 7664-41-7 149 Ethane 74-84-0 150Hydrogen sulfide 7783-06-4 151 Barium 7440-39-3 152Copper 7440-50-8 153 Molybdenum 7439-98-7 154Vanadium 7440-62-2 155Zinc 7440-66-6 156Higher Heating Value (HHV) HHV 157Total Hydrocarbon (THC) THC 158Total Reduced Sulfur (TRS) TRS 159Sulfide Sulfide 1605-day Biological Oxygen Demand BOD5 161Chemical Oxygen Demand COD**Pollutant Class**

Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants Criteria Pollutants VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC VOC Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Form Approved 03/28/2011 OMB Control No. 2060-0657 Approval Expires 03/31/2014Volatile Organic HAP

Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAPSemi-Volatile/Non-Volatile Organic HAP

Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Semi-Volatile/Non-Volatile Organic HAP Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Dioxins Furans and PCBs Metal HAP Metal HAP Metal HAPMetal HAP

Metal HAP Metal HAP Metal HAP Metal HAP Metal HAP Metal HAP Metal HAP Metal HAP Other Inorganic HAP Other Inorganic HAP Other Inorganic HAP Other Inorganic HAP Other Inorganic HAP Other Inorganic HAP Other Inorganic HAP Other Compounds Other Compounds Other Compounds Other Compounds Other Compounds Other Compounds Other Compounds Other Compounds Surrogate Surrogate Surrogate Surrogate Surrogate Surrogate