Kleinfelder, Inc. 

6200 Harris Technology Blvd. 

Charlotte, NC 28269

Tampa Electric Company 

Mulberry, FL 

Client # 109381 

Analytical Report 

(0310-130)

EPA SW-846 Method 8270C 19 Targeted POM (PAH) Compounds 

SW-846 Method 8270C Target Compound List 

Enthalpy Analytical, Inc. 

Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com 

2202 Ellis Road Durham, NC 27703 - 5518
I certify that to the best of my knowledge all analytical data presented in this report: 

 Have been checked for completeness 

 Are accurate, error-free, and legible 

 Have been conducted in accordance with approved protocol, and that all deviations and analytical 

problems are summarized in the appropriate narrative(s) 

This analytical report was prepared in Portable Document Format (.PDF) and contains  pages. 

EA# 0310-130 Page 2 of 129
Narrative Summary

EA# 0310-130 Page 3 of 129
Enthalpy Analytical Narrative Summary 

Company Kleinfelder, Inc. Client # 109381

Analyst DDA Job # 0310-130 

Parameters EPA SW-846 Method 8270C PO # Verbal 

# Samples 3 Runs, 2 Blanks Report Date May 5, 2010 

Custody Heather Tarjeft received the samples on 4/16/10 after being relinquished 

by Kleinfelder, Inc. The samples were received at -1.3 °C and were in 

good condition. Prior to, during, and after analysis, the samples were 

kept under lock with access only to authorized personnel by Enthalpy 

Analytical, Inc. 

Analysis The samples were analyzed for Polyaromatic Hydrocarbons (PAHs) by 

Selected Ion Monitoring (SIM) and for Semi-Volatile ICR target 

anlaytes by scan using the analytical procedures in EPA SW-846 

Method 8270C, Semivolatile Organic Compounds by Gas 

Chromatography/Mass Spectrometry (GC/MS). 

All samples were analyzed in both SIM and Scan modes. 

Prior to sample collection, the XAD-2 traps were spiked with a BN 

Surrogate Mix that consisted of 100 μg of nitrobenzene-d5, 

2-fluorobiphenyl, and terphenyl-d14. 

Each sample train consisted of five fractions: Filter, FH Rinse 

(acetone/methylene chloride), XAD-2 Sorbent Trap, Acetone/Methylene 

chloride (BH) Rinse, and Condensate. The fractions were combined and 

labeled as follows: FH (filter, front half rinse), BH (XAD-2 trap, 

acetone/methylene chloride BH Rinse), and COND (condensate). 

Each FH, BH, COND and QC sample was spiked with 100 μg of the 

acid extraction surrogates (2-fluorophenol, d5-phenol, and 2,4,6-

tribromophenol) and SIM PAH extraction surrogates (fluorene-d10 and 

pyrene-d10). 

Each filter and XAD-2 fraction was Soxhlet extracted for 18 hours using 

the corresponding acetone/methylene chloride and fresh methylene 

chloride combined in the flat bottom flask. Soxhlet extracts were then 

concentrated to a final volume of 5 mL. 

The Condensate fractions were separatory funnel extracted with 

methylene chloride, then concentrated to a final volume of 5 mLs. 

EA# 0310-130 Page 4 of 129
Enthalpy Analytical Narrative Summary 

(continued) 

Analysis 

(continued) 

One laboratory method blank and LCS set consisting of a filter and 

XAD-2 and one method blank and LCS set consisting of lab reagent 

water were prepared with these samples. These laboratory QC samples 

were spiked in the same manner as the samples with the exception of the 

MB COND which was not spiked with the BN Surrogate Mix. 

The water QC samples were separatory funnel extracted and the 

Filter/XAD QC samples were soxhlet extracted. All QC samples were 

concentrated to final volume of 5mL. 

A 100 μL aliquot of each sample extract was spiked with 40 μg/mL of 

SVOA internal standard spiking solution, prior to scan analyses. A 

100 μL aliquot of each sample extract was spiked with 400 ng/mL of 

SVOA internal standard spiking solution, prior to SIM. 

The Agilent Technologies Model 6890N, Gas Chromatograph ("Wiley" 

S/N CN10244010) was equipped with a 5973N Mass Selective Detector 

and a Restek Rxi-5Sil MS, 30m x 0.25mm x 0.5μm (SN 963186) 

capillary column. 

Calibration All analytes met the 15% mean RSD initial calibration requirements. All 

SPCC and CCC criteria were met in the initial and continuing 

calibrations. All other compounds in the continuing calibration met the 

50% difference in-house requirements. 

Chromatographic 

Conditions 

The samples were analyzed using the acquisition methods RXI-2A and 

RXISIM2A. 

QC Notes All samples were prepared within holding times specified in the method. 

All internal standard area response, retention time, and surrogate 

standards QC criteria were met for all samples, except RB Filter which 

had low 2-fluorophenol recovery. This sample was reanalyzed with 

confirming results, therefore, both sets of data have been included in the 

report. 

An aliquot of the extract for sample Unit 1 Run 1 FH was spiked and 

all analytes exhibited recovery values within 50% of the expected value. 

The PAH compounds were spiked at scan levels. The native amounts 

for all compounds were zero. 

Benzidine did not meet QC criteria of 50-150% recovery in LCS 

samples. 

EA# 0310-130 Page 5 of 129
Enthalpy Analytical Narrative Summary 

(continued) 

QC Notes 

(continued) 

An aliquot of the extract for sample Unit 1 Run 1 FH was prepared as a 

lab duplicate for scan analysis and an aliquot of the extract for sample 

Unit 1 Run 3 FH was prepared as a lab duplicate for SIM analysis. No 

compounds were detected in the scan analysis. Naphthalene, 2-

methylnaphthalene and phenanthrene were the only compound detected 

in the SIM analysis and exhibited duplicate analysis % difference of 

3.6%, 2.0% and 2.4% respectively. 

Reporting Notes Reporting units are μg “Catch Weight” for all scan analyses and ng

“Catch Weight” for all SIM analyses.

Due to matrix interference for sample Unit 1 Run 3 BH, results have 

been reported from the 2-fold analysis. 

The results presented in this report are representative of the samples as 

provided to the laboratory. 

EA# 0310-130 Page 6 of 129
General Reporting Notes 

The following are general reporting notes that are applicable to all Enthalpy Analytical, Inc. data 

reports, unless specifically noted otherwise.

 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot 

determine the presence of the analyte of interest reliably. 

 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot 

quantitate the analyte of interest within the criteria of the method. 

 The acronym ND following a value indicates a non-detect or analytical result below the MDL. 

 The letter J following a value indicates an analytical result between the MDL and the LOQ. A J flag 

indicates that the laboratory can positively identify the analyte of interest as present, but the value 

should be considered an estimate. 

 The letter E following a value indicates an analytical result exceeding 100% of the highest calibration 

point. The associated value should be considered as an estimate. 

 The acronym DF represents Dilution Factor. This number represents dilution of the sample during the 

preparation and/or analysis process. The analytical result taken from a laboratory instrument is 

multiplied by the DF to determine the final undiluted sample results. 

 The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual sample is 

spiked with a known amount of analyte so that a percent recovery value can be determined. This shows 

what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample 

matrix interferes with the analysis of the analyte(s). 

 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same 

manner as an MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality 

by showing the consistency of results gained by performing the same steps multiple times. 

 The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares an 

additional aliquot of sample for testing and the results of the duplicate analysis are compared to the 

initial result. The result should have a difference value of within 10% of the initial result (if the results 

of the original analysis are greater than the LOQ). 

 The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an 

additional aliquot at a different dilution factor (usually double the initial factor). This analysis helps 

confirm that no additional compound is present and coeluting or sharing absorbance with the analyte of 

interest, as they would have a different response/absorbance than the analyte of interest. 

 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample 

matrix, prepared and analyzed by the laboratory using the same reagents, spiking standards and 

procedures used for the client samples. The LCS is used to assess the control of the laboratory’s 

analytical system. Whenever spikes are prepared for our client projects, two extra spikes are prepared. 

The extras (randomly chosen) are labeled with the associated project number and kept in-house at the 

appropriate temperature conditions. When the project samples are received for analysis, the LCSs are 

analyzed to confirm that the analyte could be recovered from the media, separate from the samples 

which were used on the project and which may have been affected by source matrix, sample collection 

and/or sample transport. 

EA# 0310-130 Page 7 of 129
General Reporting Notes 

(continued) 

 Significant Figures: Where the reported value is much greater than unity (1.00) in the units expressed, 

the number is rounded to a whole number of units, rather than to 3 significant figures. For example, a 

value of 10,456.45 ug catch is rounded to 10,456 ug. There are five significant digits displayed, but no 

confidence should be placed on more than two significant digits. 

 Manual Integration: The data systems used for processing will flag manually integrated peaks with 

an “M”. There are several reasons a peak may be manually integrated. These reasons will be identified 

by the following two letter designations. The peak was not integrated by the software “NI”, the peak 

was integrated incorrectly by the software “II” or the wrong peak was integrated by the software 

“WP”. These codes will accompany the analyst’s manual integration stamp placed next to the 

compound name. 

EA# 0310-130 Page 8 of 129
Sample Custody

EA# 0310-130 Page 9 of 129

Results

EA# 0310-130 Page 11 of 129
Sample ID: DF: 1.00

Data File: W1000703.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 U1 R1 FH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 12 of 129
Sample ID: DF: 1.00

Data File: W1000703.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R1 FH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 337,148 40.0 N/A

136 6.76 1,160,259 40.0 N/A

164 8.53 645,045 40.0 N/A

188 10.0 1,108,934 40.0 N/A

240 12.9 1,024,218 40.0 N/A

264 15.3 865,105 40.0 N/A

112 4.41 93,888 9.99 49.9 PASS

99 5.13 160,410 14.6 72.9 PASS

330 9.32 39,049 14.4 71.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 337,148

Naphthalene-d8 (I) 1,160,259

Acenaphthene-d10 (I) 645,045

Phenanthrene-d10 (I) 1,108,934

Chrysene-d12 (I) 1,024,218

Perylene-d12 (I) 865,105

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 13 of 129
Sample ID: DF: 1.00

Data File: W1000847.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,860 400 N/A

136 6.76 29,014 400 N/A

164 8.52 15,838 400 N/A

188 10.0 27,708 400 N/A

240 12.9 21,763 400 N/A

264 15.3 10,171 400 N/A

176 9.05 11,761 263 65.9 PASS

212 11.5 16,878 291 72.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.25 8,548 Pass

Compound

0310-130 U1 R1 FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,860

Naphthalene-d8 (I) 29,014

Acenaphthene-d10 (I) 15,838

Phenanthrene-d10 (I) 27,708

Chrysene-d12 (I) 21,763

Perylene-d12 (I) 10,171

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 14 of 129
Sample ID: DF: 1.00

Data File: W1000704.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags % Diff

74 NA 0.00 0.772 3.86 ND 0

94 NA 0.00 0.649 3.25 ND 0

66 NA 0.00 0.694 3.47 ND 0

63 NA 0.00 0.788 3.94 ND 0

128 NA 0.00 0.624 3.12 ND 0

146 NA 0.00 0.558 2.79 ND 0

146 NA 0.00 0.528 2.64 ND 0

108 NA 0.00 0.700 3.50 ND 0

146 NA 0.00 0.558 2.79 ND 0

107 NA 0.00 0.677 3.39 ND 0

107 NA 0.00 0.591 2.95 ND 0

70 NA 0.00 0.832 4.16 ND 0

117 NA 0.00 0.632 3.16 ND 0

77 NA 0.00 0.816 4.08 ND 0

82 NA 0.00 0.748 3.74 ND 0

107 NA 0.00 0.729 3.64 ND 0

139 NA 0.00 0.669 3.35 ND 0

93 NA 0.00 0.732 3.66 ND 0

162 NA 0.00 0.652 3.26 ND 0

180 NA 0.00 0.617 3.09 ND 0

65 NA 0.00 0.849 4.24 ND 0

225 NA 0.00 0.609 3.05 ND 0

107 NA 0.00 0.661 3.31 ND 0

142 NA 0.00 0.613 3.07 ND 0

237 NA 0.00 8.12 40.6 ND 0

196 NA 0.00 0.738 3.69 ND 0

196 NA 0.00 0.541 2.70 ND 0

162 NA 0.00 0.652 3.26 ND 0

168 NA 0.00 0.672 3.36 ND 0

163 NA 0.00 0.809 4.05 ND 0

168 NA 0.00 0.819 4.09 ND 0

165 NA 0.00 0.775 3.88 ND 0

168 NA 0.00 0.777 3.89 ND 0

184 NA 0.00 5.05 25.3 ND 0

139 NA 0.00 5.78 28.9 ND 0

165 NA 0.00 0.804 4.02 ND 0

168 NA 0.00 0.688 3.44 ND 0

232 NA 0.00 0.761 3.80 ND 0

232 NA 0.00 0.701 3.50 ND 0

149 NA 0.00 1.02 5.10 ND 0

204 NA 0.00 0.754 3.77 ND 0

198 NA 0.00 5.16 25.8 ND 0

169 NA 0.00 0.716 3.58 ND 0

77 NA 0.00 0.991 4.96 ND 0

248 NA 0.00 0.671 3.35 ND 0

284 NA 0.00 0.546 2.73 ND 0

266 NA 0.00 0.565 2.83 ND 0

167 NA 0.00 0.705 3.53 ND 0

Compound

0310-130 U1 R1 FH LD

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 15 of 129
Sample ID: DF: 1.00

Data File: W1000704.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags % Diff

0310-130 U1 R1 FH LD

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND 0

184 NA 0.00 22.8 114 ND 0

149 NA 0.00 0.810 4.05 ND 0

212 NA 0.00 10.8 53.9 ND 0

149 NA 0.00 1.74 8.71 ND 0

252 NA 0.00 9.36 46.8 ND 0

149 NA 0.00 0.644 3.22 ND 0

Rec. (%) Flags

152 5.55 417,192 40.0 N/A

136 6.76 1,458,599 40.0 N/A

164 8.52 846,687 40.0 N/A

188 10.0 1,487,544 40.0 N/A

240 12.9 1,405,209 40.0 N/A

264 15.3 1,146,406 40.0 N/A

112 4.41 109,225 9.39 46.9 PASS

99 5.13 187,477 13.8 68.9 PASS

330 9.32 52,694 14.5 72.3 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 417,192

Naphthalene-d8 (I) 1,458,599

Acenaphthene-d10 (I) 846,687

Phenanthrene-d10 (I) 1,487,544

Chrysene-d12 (I) 1,405,209

Perylene-d12 (I) 1,146,406

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 16 of 129
Sample ID: DF: 1.00

Data File: W1000705.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 0.10

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

Native 

Amount 

(ug)

Spike 

Amount 

(ug)

%

Rec.

74 3.43 326,383 54.2 5.42 0.00 5.00 108

94 5.15 676,163 50.3 5.03 0.00 5.00 101

66 5.24 329,313 50.0 5.00 0.00 5.00 100

63 5.26 438,448 50.0 5.00 0.00 5.00 100

128 5.36 620,643 50.1 5.01 0.00 5.00 100

146 5.51 729,139 49.2 4.92 0.00 5.00 98.4

146 5.57 746,370 49.0 4.90 0.00 5.00 98.1

108 5.63 339,693 47.2 4.72 0.00 5.00 94.3

146 5.72 694,336 49.5 4.95 0.00 5.00 99.1

107 5.70 468,856 50.4 5.04 0.00 5.00 101

107 5.84 563,585 47.4 4.74 0.00 5.00 94.9

70 5.87 378,377 46.3 4.63 0.00 5.00 92.5

117 6.04 265,731 49.9 4.99 0.00 5.00 99.7

77 6.07 595,070 49.3 4.93 0.00 5.00 98.6

82 6.28 986,619 47.9 4.79 0.00 5.00 95.8

107 6.36 579,330 47.0 4.70 0.00 5.00 94.0

139 6.38 330,359 48.0 4.80 0.00 5.00 96.0

93 6.45 592,877 46.6 4.66 0.00 5.00 93.2

162 6.60 493,460 46.7 4.67 0.00 5.00 93.3

180 6.70 614,906 49.1 4.91 0.00 5.00 98.2

128 6.79 1,825,821 49.2 4.92 0.00 5.00 98.5

65 6.80 204,907 45.1 4.51 0.00 5.00 90.2

225 6.89 369,715 48.2 4.82 0.00 5.00 96.3

107 7.24 509,033 48.7 4.87 0.00 5.00 97.3

142 7.47 1,126,019 46.1 4.61 0.00 5.00 92.3

142 7.57 1,155,526 48.6 4.86 0.00 5.00 97.2

237 7.62 404,103 51.0 5.10 0.00 5.00 102

196 7.72 372,353 47.2 4.72 0.00 5.00 94.4

196 7.77 400,532 48.7 4.87 0.00 5.00 97.3

162 7.96 1,108,848 48.6 4.86 0.00 5.00 97.2

168 8.15 187,090 48.3 4.83 0.00 5.00 96.6

163 8.18 1,255,761 48.1 4.81 0.00 5.00 96.1

168 8.23 212,919 47.9 4.79 0.00 5.00 95.8

165 8.26 298,446 47.5 4.75 0.00 5.00 95.0

168 8.33 140,112 46.0 4.60 0.00 5.00 92.0

152 8.39 1,768,659 50.1 5.01 0.00 5.00 100

154 8.56 1,140,207 48.4 4.84 0.00 5.00 96.8

184 8.54 145,791 45.0 4.50 0.00 5.00 89.9

139 8.56 221,796 45.5 4.55 0.00 5.00 91.1

165 8.67 379,212 47.6 4.76 0.00 5.00 95.1

168 8.73 1,548,549 48.1 4.81 0.00 5.00 96.3

232 8.80 335,976 47.3 4.73 0.00 5.00 94.5

232 8.84 343,906 48.1 4.81 0.00 5.00 96.1

149 8.88 1,217,399 47.2 4.72 0.00 5.00 94.4

204 9.04 642,246 47.4 4.74 0.00 5.00 94.8

166 9.08 1,282,798 48.8 4.88 0.00 5.00 97.5

198 9.09 216,029 47.9 4.79 0.00 5.00 95.8

169 9.16 1,089,838 47.7 4.77 0.00 5.00 95.4

77 9.20 1,101,960 47.8 4.78 0.00 5.00 95.7

248 9.55 401,388 49.1 4.91 0.00 5.00 98.3

284 9.66 398,775 49.6 4.96 0.00 5.00 99.2

266 9.83 237,102 49.1 4.91 0.00 5.00 98.3

178 10.1 1,778,601 48.8 4.88 0.00 5.00 97.5

178 10.1 1,781,318 50.0 5.00 0.00 5.00 100

167 10.3 1,563,653 49.5 4.95 0.00 5.00 99.0

149 10.5 2,015,226 50.8 5.08 0.00 5.00 102

202 11.3 1,929,380 51.8 5.18 0.00 5.00 104

Compound

0310-130 U1 R1 FH MS

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

Naphthalene

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

2-Methylnaphthalene

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

Acenaphthylene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

Acenaphthene (CCC)

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

Fluoranthene (CCC)

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

Phenanthrene

4-Chlorophenyl-phenylether

Fluorene

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Anthracene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 17 of 129
Sample ID: DF: 1.00

Data File: W1000705.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 0.10

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

Native 

Amount 

(ug)

Spike 

Amount 

(ug)

%

Rec. Compound

0310-130 U1 R1 FH MS

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 2.28 ND 0.00 0.00 NA

202 11.5 2,054,919 51.5 5.15 0.00 5.00 103

149 12.1 904,833 48.3 4.83 0.00 5.00 96.6

212 NA 0.00 10.8 1.08 ND 0.00 0.00 NA

149 12.7 1,300,611 50.8 5.08 0.00 5.00 102

252 NA 0.00 9.36 0.936 ND 0.00 0.00 NA

228 12.9 1,864,727 48.5 4.85 0.00 5.00 97.0

228 13.0 1,758,171 49.0 4.90 0.00 5.00 97.9

149 13.6 2,022,274 52.0 5.20 0.00 5.00 104

252 14.6 1,724,719 49.8 4.98 0.00 5.00 99.5

252 14.6 1,671,279 49.4 4.94 0.00 5.00 98.8

252 NA 0.00 0.340 0.0340 ND 0.00 0.00 NA

252 15.2 1,550,711 49.9 4.99 0.00 5.00 99.8

252 NA 0.00 0.340 0.0340 ND 0.00 0.00 NA

276 17.4 1,335,651 45.9 4.59 0.00 5.00 91.9

278 17.4 1,100,449 45.1 4.51 0.00 5.00 90.2

276 18.1 1,030,074 45.0 4.50 0.00 5.00 90.0

Rec. (%) Flags

152 5.55 407,106 40.0 N/A

136 6.77 1,409,961 40.0 N/A

164 8.53 815,611 40.0 N/A

188 10.0 1,412,925 40.0 N/A

240 12.9 1,496,030 40.0 N/A

264 15.3 1,248,152 40.0 N/A

112 4.41 98,431 8.67 45.6 PASS

99 5.14 170,534 12.8 67.6 PASS

330 9.33 51,501 14.9 78.3 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Pyrene

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

Benzo(a)anthracene

2,4,6-Tribromophenol (surr)

Chrysene

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 407,106

Naphthalene-d8 (I) 1,409,961

Acenaphthene-d10 (I) 815,611

Phenanthrene-d10 (I) 1,412,925

Chrysene-d12 (I) 1,496,030

Perylene-d12 (I) 1,248,152

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 18 of 129
Sample ID: DF: 1.00

Data File: W1000706.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

0310-130 U1 R1 BH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 19 of 129
Sample ID: DF: 1.00

Data File: W1000706.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R1 BH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 404,897 40.0 N/A

136 6.76 1,376,010 40.0 N/A

164 8.53 768,024 40.0 N/A

188 10.0 1,359,307 40.0 N/A

240 12.9 1,397,968 40.0 N/A

264 15.3 1,032,179 40.0 N/A

112 4.42 176,559 15.6 78.2 PASS

99 5.13 219,694 16.6 83.2 PASS

82 6.05 204,465 15.8 78.9 PASS

172 7.80 467,588 18.3 91.4 PASS

330 9.33 55,753 16.7 83.7 PASS

244 11.6 530,276 20.7 103 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 404,897

Naphthalene-d8 (I) 1,376,010

Acenaphthene-d10 (I) 768,024

Phenanthrene-d10 (I) 1,359,307

Chrysene-d12 (I) 1,397,968

Perylene-d12 (I) 1,032,179

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 20 of 129
Sample ID: DF: 1.00

Data File: W1000848.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 8,515 122 610 

142 7.46 858 19.3 96.4 

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 10.1 1,030 13.7 68.3 

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,393 400 N/A

136 6.76 28,595 400 N/A

164 8.52 16,014 400 N/A

188 10.0 28,929 400 N/A

240 12.9 23,689 400 N/A

264 15.2 10,984 400 N/A

176 9.04 14,414 319 79.8 PASS

212 11.5 18,938 313 78.2 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 U1 R1 BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,393

Naphthalene-d8 (I) 28,595

Acenaphthene-d10 (I) 16,014

Phenanthrene-d10 (I) 28,929

Chrysene-d12 (I) 23,689

Perylene-d12 (I) 10,984

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 21 of 129
Sample ID: DF: 1.00

Data File: W1000707.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 U1 R1 COND

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 22 of 129
Sample ID: DF: 1.00

Data File: W1000707.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R1 COND

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 399,253 40.0 N/A

136 6.76 1,378,930 40.0 N/A

164 8.53 755,864 40.0 N/A

188 10.0 1,302,214 40.0 N/A

240 12.9 1,241,327 40.0 N/A

264 15.3 1,005,653 40.0 N/A

112 4.41 159,029 14.3 71.4 PASS

99 5.13 166,669 12.8 64.0 PASS

330 9.32 44,781 14.0 70.2 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 399,253

Naphthalene-d8 (I) 1,378,930

Acenaphthene-d10 (I) 755,864

Phenanthrene-d10 (I) 1,302,214

Chrysene-d12 (I) 1,241,327

Perylene-d12 (I) 1,005,653

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 23 of 129
Sample ID: DF: 1.00

Data File: W1000849.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 7,312 400 N/A

136 6.76 23,886 400 N/A

164 8.52 12,509 400 N/A

188 10.0 21,428 400 N/A

240 12.9 15,666 400 N/A

264 15.3 7,799 400 N/A

176 9.05 8,832 251 62.6 PASS

212 11.5 12,869 287 71.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.92 18,105 Pass

15.23 15.26 8,548 Pass

Compound

0310-130 U1 R1 COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,312

Naphthalene-d8 (I) 23,886

Acenaphthene-d10 (I) 12,509

Phenanthrene-d10 (I) 21,428

Chrysene-d12 (I) 15,666

Perylene-d12 (I) 7,799

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 24 of 129
Sample ID: DF: 1.00

Data File: W1000708.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 U1 R2 FH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 25 of 129
Sample ID: DF: 1.00

Data File: W1000708.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R2 FH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 412,737 40.0 N/A

136 6.77 1,427,227 40.0 N/A

164 8.52 803,129 40.0 N/A

188 10.0 1,358,572 40.0 N/A

240 12.9 1,242,405 40.0 N/A

264 15.2 1,031,914 40.0 N/A

112 4.41 80,660 7.01 35.0 PASS

99 5.13 106,461 7.91 39.5 PASS

330 9.32 49,921 15.0 75.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 412,737

Naphthalene-d8 (I) 1,427,227

Acenaphthene-d10 (I) 803,129

Phenanthrene-d10 (I) 1,358,572

Chrysene-d12 (I) 1,242,405

Perylene-d12 (I) 1,031,914

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 26 of 129
Sample ID: DF: 1.00

Data File: W1000850.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 4,750 69.5 347 

142 7.46 3,317 76.1 380 

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 10.1 1,534 20.9 104 

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,509 400 N/A

136 6.76 28,036 400 N/A

164 8.52 16,090 400 N/A

188 10.0 28,166 400 N/A

240 12.9 21,555 400 N/A

264 15.2 10,947 400 N/A

176 9.05 11,012 243 60.7 PASS

212 11.5 19,280 327 81.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.25 8,548 Pass

Compound

0310-130 U1 R2 FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,509

Naphthalene-d8 (I) 28,036

Acenaphthene-d10 (I) 16,090

Phenanthrene-d10 (I) 28,166

Chrysene-d12 (I) 21,555

Perylene-d12 (I) 10,947

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 27 of 129
Sample ID: DF: 1.00

Data File: W1000709.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

0310-130 U1 R2 BH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 28 of 129
Sample ID: DF: 1.00

Data File: W1000709.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R2 BH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 414,570 40.0 N/A

136 6.77 1,443,874 40.0 N/A

164 8.53 817,967 40.0 N/A

188 10.0 1,448,594 40.0 N/A

240 12.9 1,342,874 40.0 N/A

264 15.2 1,116,446 40.0 N/A

112 4.41 162,975 14.1 70.5 PASS

99 5.13 209,420 15.5 77.4 PASS

82 6.05 181,744 13.7 68.5 PASS

172 7.80 447,931 16.4 82.2 PASS

330 9.32 57,259 16.1 80.7 PASS

244 11.6 510,719 18.7 93.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 414,570

Naphthalene-d8 (I) 1,443,874

Acenaphthene-d10 (I) 817,967

Phenanthrene-d10 (I) 1,448,594

Chrysene-d12 (I) 1,342,874

Perylene-d12 (I) 1,116,446

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 29 of 129
Sample ID: DF: 1.00

Data File: W1000852.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 9,658 130 651 

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 10.1 1,058 13.2 66.2 

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 9,001 400 N/A

136 6.76 30,416 400 N/A

164 8.52 16,799 400 N/A

188 10.0 30,639 400 N/A

240 12.9 24,656 400 N/A

264 15.3 11,924 400 N/A

176 9.04 15,177 321 80.1 PASS

212 11.5 21,303 332 83.1 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.92 18,105 Pass

15.23 15.26 8,548 Pass

Compound

0310-130 U1 R2 BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 9,001

Naphthalene-d8 (I) 30,416

Acenaphthene-d10 (I) 16,799

Phenanthrene-d10 (I) 30,639

Chrysene-d12 (I) 24,656

Perylene-d12 (I) 11,924

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 30 of 129
Sample ID: DF: 1.00

Data File: W1000710.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 U1 R2 COND

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 31 of 129
Sample ID: DF: 1.00

Data File: W1000710.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R2 COND

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 385,067 40.0 N/A

136 6.76 1,329,925 40.0 N/A

164 8.53 746,629 40.0 N/A

188 10.0 1,262,964 40.0 N/A

240 12.9 1,139,506 40.0 N/A

264 15.2 938,933 40.0 N/A

112 4.41 162,693 15.2 75.8 PASS

99 5.13 179,229 14.3 71.3 PASS

330 9.32 44,326 14.3 71.6 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.24 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 385,067

Naphthalene-d8 (I) 1,329,925

Acenaphthene-d10 (I) 746,629

Phenanthrene-d10 (I) 1,262,964

Chrysene-d12 (I) 1,139,506

Perylene-d12 (I) 938,933

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 32 of 129
Sample ID: DF: 1.00

Data File: W1000853.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,702 400 N/A

136 6.76 28,256 400 N/A

164 8.52 14,809 400 N/A

188 10.0 24,804 400 N/A

240 12.9 16,000 400 N/A

264 15.3 7,794 400 N/A

176 9.05 10,583 254 63.4 PASS

212 11.5 13,870 267 66.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.93 18,105 Pass

15.23 15.27 8,548 Pass

Compound

0310-130 U1 R2 COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,702

Naphthalene-d8 (I) 28,256

Acenaphthene-d10 (I) 14,809

Phenanthrene-d10 (I) 24,804

Chrysene-d12 (I) 16,000

Perylene-d12 (I) 7,794

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 33 of 129
Sample ID: DF: 1.00

Data File: W1000711.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 U1 R3 FH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 34 of 129
Sample ID: DF: 1.00

Data File: W1000711.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R3 FH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 416,781 40.0 N/A

136 6.76 1,464,175 40.0 N/A

164 8.53 831,607 40.0 N/A

188 10.0 1,480,046 40.0 N/A

240 12.9 1,427,855 40.0 N/A

264 15.2 1,193,862 40.0 N/A

112 4.42 173,786 15.0 74.8 PASS

99 5.13 216,254 15.9 79.5 PASS

330 9.32 54,785 15.1 75.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 416,781

Naphthalene-d8 (I) 1,464,175

Acenaphthene-d10 (I) 831,607

Phenanthrene-d10 (I) 1,480,046

Chrysene-d12 (I) 1,427,855

Perylene-d12 (I) 1,193,862

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 35 of 129
Sample ID: DF: 1.00

Data File: W1000854.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 10,312 140 699 

142 7.46 6,952 148 739 

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 10.1 1,591 20.3 102 

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,999 400 N/A

136 6.76 30,229 400 N/A

164 8.52 16,755 400 N/A

188 10.0 29,999 400 N/A

240 12.9 24,066 400 N/A

264 15.3 12,813 400 N/A

176 9.04 13,866 294 73.4 PASS

212 11.5 18,809 300 74.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.92 18,105 Pass

15.23 15.25 8,548 Pass

Compound

0310-130 U1 R3 FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,999

Naphthalene-d8 (I) 30,229

Acenaphthene-d10 (I) 16,755

Phenanthrene-d10 (I) 29,999

Chrysene-d12 (I) 24,066

Perylene-d12 (I) 12,813

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 36 of 129
Sample ID: DF: 1.00

Data File: W1000855.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags % Diff

128 6.78 10,260 145 725 3.6

142 7.46 6,809 151 754 2.0

152 NA 0.00 10.0 50.0 ND 0.0

154 NA 0.00 10.0 50.0 ND 0.0

166 NA 0.00 10.0 50.0 ND 0.0

178 10.1 1,518 20.8 104 2.4

178 NA 0.00 10.0 50.0 ND 0.0

202 NA 0.00 10.0 50.0 ND 0.0

202 NA 0.00 10.0 50.0 ND 0.0

228 NA 0.00 10.0 50.0 ND 0.0

228 NA 0.00 10.0 50.0 ND 0.0

252 NA 0.00 10.0 50.0 ND 0.0

252 NA 0.00 10.0 50.0 ND 0.0

252 NA 0.00 10.0 50.0 ND 0.0

252 NA 0.00 10.0 50.0 ND 0.0

252 NA 0.00 10.0 50.0 ND 0.0

276 NA 0.00 10.0 50.0 ND 0.0

278 NA 0.00 10.0 50.0 ND 0.0

276 NA 0.00 10.0 50.0 ND 0.0

Rec. (%) Flags

152 5.55 8,658 400 N/A

136 6.76 29,025 400 N/A

164 8.52 15,893 400 N/A

188 10.0 27,945 400 N/A

240 12.9 21,670 400 N/A

264 15.2 11,889 400 N/A

176 9.05 13,321 297 74.3 PASS

212 11.5 17,912 306 76.6 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.25 8,548 Pass

Compound

0310-130 U1 R3 FH LD

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,658

Naphthalene-d8 (I) 29,025

Acenaphthene-d10 (I) 15,893

Phenanthrene-d10 (I) 27,945

Chrysene-d12 (I) 21,670

Perylene-d12 (I) 11,889

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 37 of 129
Sample ID: DF: 2.00

Data File: W1000921.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 3

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 7.72 ND

94 NA 0.00 0.649 6.49 ND

66 NA 0.00 0.694 6.94 ND

63 NA 0.00 0.788 7.88 ND

128 NA 0.00 0.624 6.24 ND

146 NA 0.00 0.558 5.58 ND

146 NA 0.00 0.528 5.28 ND

108 NA 0.00 0.700 7.00 ND

146 NA 0.00 0.558 5.58 ND

107 NA 0.00 0.677 6.77 ND

107 NA 0.00 0.591 5.91 ND

70 NA 0.00 0.832 8.32 ND

117 NA 0.00 0.632 6.32 ND

77 NA 0.00 0.816 8.16 ND

82 NA 0.00 0.748 7.48 ND

107 NA 0.00 0.729 7.29 ND

139 NA 0.00 0.669 6.69 ND

93 NA 0.00 0.732 7.32 ND

162 NA 0.00 0.652 6.52 ND

180 NA 0.00 0.617 6.17 ND

65 NA 0.00 0.849 8.49 ND

225 NA 0.00 0.609 6.09 ND

107 NA 0.00 0.661 6.61 ND

142 NA 0.00 0.613 6.13 ND

237 NA 0.00 8.12 81.2 ND

196 NA 0.00 0.738 7.38 ND

196 NA 0.00 0.541 5.41 ND

162 NA 0.00 0.652 6.52 ND

168 NA 0.00 0.672 6.72 ND

163 NA 0.00 0.809 8.09 ND

168 NA 0.00 0.819 8.19 ND

165 NA 0.00 0.775 7.75 ND

168 NA 0.00 0.777 7.77 ND

184 NA 0.00 5.05 50.5 ND

139 NA 0.00 5.78 57.8 ND

165 NA 0.00 0.804 8.04 ND

168 NA 0.00 0.688 6.88 ND

232 NA 0.00 0.761 7.61 ND

232 NA 0.00 0.701 7.01 ND

149 NA 0.00 1.02 10.2 ND

204 NA 0.00 0.754 7.54 ND

198 NA 0.00 5.16 51.6 ND

169 NA 0.00 0.716 7.16 ND

77 NA 0.00 0.991 9.91 ND

248 NA 0.00 0.671 6.71 ND

284 NA 0.00 0.546 5.46 ND

266 NA 0.00 0.565 5.65 ND

167 NA 0.00 0.705 7.05 ND

149 NA 0.00 1.04 10.4 ND

Compound

0310-130 U1 R3 BH 2X

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 38 of 129
Sample ID: DF: 2.00

Data File: W1000921.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 3

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R3 BH 2X

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 228 ND

149 NA 0.00 0.810 8.10 ND

212 NA 0.00 10.8 108 ND

149 NA 0.00 1.74 17.4 ND

252 NA 0.00 9.36 93.6 ND

149 NA 0.00 0.644 6.44 ND

Rec. (%) Flags

152 5.54 477,177 40.0 N/A

136 6.76 1,650,012 40.0 N/A

164 8.52 933,670 40.0 N/A

188 10.0 1,678,384 40.0 N/A

240 12.9 1,460,385 40.0 N/A

264 15.2 964,147 40.0 N/A

112 4.41 87,185 6.55 65.5 PASS

99 5.13 115,613 7.43 74.3 PASS

82 6.04 110,558 7.24 72.4 PASS

172 7.79 278,200 8.94 89.4 PASS

330 9.31 35,132 8.54 85.4 PASS

244 11.6 309,492 9.78 97.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.54 5.54 358,096 Pass

6.76 6.76 1,281,171 Pass

8.52 8.52 753,346 Pass

10.03 10.03 1,381,533 Pass

12.91 12.90 1,223,151 Pass

15.25 15.22 988,673 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 477,177

Naphthalene-d8 (I) 1,650,012

Acenaphthene-d10 (I) 933,670

Phenanthrene-d10 (I) 1,678,384

Chrysene-d12 (I) 1,460,385

Perylene-d12 (I) 964,147

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 39 of 129
Sample ID: DF: 2.00

Data File: W1000859.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 4,179 65.1 651 

142 NA 0.00 10.0 100 ND

152 NA 0.00 10.0 100 ND

154 NA 0.00 10.0 100 ND

166 NA 0.00 10.0 100 ND

178 NA 0.00 10.0 100 ND

178 NA 0.00 10.0 100 ND

202 NA 0.00 10.0 100 ND

202 NA 0.00 10.0 100 ND

228 NA 0.00 10.0 100 ND

228 NA 0.00 10.0 100 ND

252 NA 0.00 10.0 100 ND

252 NA 0.00 10.0 100 ND

252 NA 0.00 10.0 100 ND

252 NA 0.00 10.0 100 ND

252 NA 0.00 10.0 100 ND

276 NA 0.00 10.0 100 ND

278 NA 0.00 10.0 100 ND

276 NA 0.00 10.0 100 ND

Rec. (%) Flags

152 5.55 7,865 400 N/A

136 6.76 26,299 400 N/A

164 8.52 13,937 400 N/A

188 10.0 24,790 400 N/A

240 12.9 17,492 400 N/A

264 15.3 4,900 400 N/A

176 9.04 6,888 175 87.7 PASS

212 11.5 7,563 146 72.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.92 18,105 Pass

15.23 15.26 8,548 Pass

Compound

0310-130 U1 R3 BH 2X

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,865

Naphthalene-d8 (I) 26,299

Acenaphthene-d10 (I) 13,937

Phenanthrene-d10 (I) 24,790

Chrysene-d12 (I) 17,492

Perylene-d12 (I) 4,900

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 40 of 129
Sample ID: DF: 1.00

Data File: W1000713.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 U1 R3 COND

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 41 of 129
Sample ID: DF: 1.00

Data File: W1000713.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 U1 R3 COND

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 421,766 40.0 N/A

136 6.76 1,477,497 40.0 N/A

164 8.53 839,776 40.0 N/A

188 10.0 1,515,849 40.0 N/A

240 12.9 1,431,810 40.0 N/A

264 15.2 1,175,332 40.0 N/A

112 4.41 172,575 14.7 73.4 PASS

99 5.13 196,907 14.3 71.6 PASS

330 9.32 51,687 13.9 69.6 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.24 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 421,766

Naphthalene-d8 (I) 1,477,497

Acenaphthene-d10 (I) 839,776

Phenanthrene-d10 (I) 1,515,849

Chrysene-d12 (I) 1,431,810

Perylene-d12 (I) 1,175,332

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 42 of 129
Sample ID: DF: 1.00

Data File: W1000857.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,184 400 N/A

136 6.76 26,871 400 N/A

164 8.52 14,637 400 N/A

188 10.0 25,765 400 N/A

240 12.9 18,446 400 N/A

264 15.3 9,124 400 N/A

176 9.05 12,786 310 77.5 PASS

212 11.5 16,790 311 77.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.93 18,105 Pass

15.23 15.26 8,548 Pass

Compound

0310-130 U1 R3 COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,184

Naphthalene-d8 (I) 26,871

Acenaphthene-d10 (I) 14,637

Phenanthrene-d10 (I) 25,765

Chrysene-d12 (I) 18,446

Perylene-d12 (I) 9,124

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 43 of 129
Sample ID: DF: 1.00

Data File: W1000700.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 FB FH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 44 of 129
Sample ID: DF: 1.00

Data File: W1000700.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 FB FH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 372,707 40.0 N/A

136 6.76 1,300,120 40.0 N/A

164 8.52 746,938 40.0 N/A

188 10.0 1,325,282 40.0 N/A

240 12.9 1,216,138 40.0 N/A

264 15.3 1,007,976 40.0 N/A

112 4.41 126,699 12.2 61.0 PASS

99 5.13 158,501 13.0 65.2 PASS

330 9.32 43,961 13.5 67.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 372,707

Naphthalene-d8 (I) 1,300,120

Acenaphthene-d10 (I) 746,938

Phenanthrene-d10 (I) 1,325,282

Chrysene-d12 (I) 1,216,138

Perylene-d12 (I) 1,007,976

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 45 of 129
Sample ID: DF: 1.00

Data File: W1000844.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 7,460 400 N/A

136 6.76 23,944 400 N/A

164 8.52 12,830 400 N/A

188 10.0 21,577 400 N/A

240 12.9 16,770 400 N/A

264 15.2 7,852 400 N/A

176 9.05 9,571 265 66.2 PASS

212 11.5 14,725 326 81.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 FB FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,460

Naphthalene-d8 (I) 23,944

Acenaphthene-d10 (I) 12,830

Phenanthrene-d10 (I) 21,577

Chrysene-d12 (I) 16,770

Perylene-d12 (I) 7,852

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 46 of 129
Sample ID: DF: 1.00

Data File: W1000701.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

0310-130 FB BH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 47 of 129
Sample ID: DF: 1.00

Data File: W1000701.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 FB BH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 379,499 40.0 N/A

136 6.76 1,283,199 40.0 N/A

164 8.53 701,807 40.0 N/A

188 10.0 1,238,865 40.0 N/A

240 12.9 1,260,022 40.0 N/A

264 15.3 1,116,769 40.0 N/A

112 4.41 82,343 7.78 38.9 PASS

99 5.13 102,761 8.30 41.5 PASS

82 6.05 198,557 16.4 81.8 PASS

172 7.80 477,881 20.4 102 PASS

330 9.32 19,842 6.54 32.7 PASS

244 11.6 509,306 21.8 109 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.76 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 379,499

Naphthalene-d8 (I) 1,283,199

Acenaphthene-d10 (I) 701,807

Phenanthrene-d10 (I) 1,238,865

Chrysene-d12 (I) 1,260,022

Perylene-d12 (I) 1,116,769

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 48 of 129
Sample ID: DF: 1.00

Data File: W1000845.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 3,258 47.0 235 

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,649 400 N/A

136 6.76 28,420 400 N/A

164 8.52 15,438 400 N/A

188 10.0 25,581 400 N/A

240 12.9 19,745 400 N/A

264 15.2 9,435 400 N/A

176 9.05 12,981 298 74.6 PASS

212 11.5 16,202 303 75.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 FB BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,649

Naphthalene-d8 (I) 28,420

Acenaphthene-d10 (I) 15,438

Phenanthrene-d10 (I) 25,581

Chrysene-d12 (I) 19,745

Perylene-d12 (I) 9,435

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 49 of 129
Sample ID: DF: 1.00

Data File: W1000702.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 FB COND

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 50 of 129
Sample ID: DF: 1.00

Data File: W1000702.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 FB COND

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 412,914 40.0 N/A

136 6.77 1,447,154 40.0 N/A

164 8.52 793,772 40.0 N/A

188 10.0 1,353,802 40.0 N/A

240 12.9 1,232,195 40.0 N/A

264 15.3 1,048,144 40.0 N/A

112 4.41 176,707 15.3 76.7 PASS

99 5.13 210,869 15.7 78.3 PASS

330 9.32 44,761 13.5 67.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.91 1,427,833 Pass

15.27 15.25 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 412,914

Naphthalene-d8 (I) 1,447,154

Acenaphthene-d10 (I) 793,772

Phenanthrene-d10 (I) 1,353,802

Chrysene-d12 (I) 1,232,195

Perylene-d12 (I) 1,048,144

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 51 of 129
Sample ID: DF: 1.00

Data File: W1000846.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 7,738 400 N/A

136 6.76 24,526 400 N/A

164 8.52 12,610 400 N/A

188 10.0 20,821 400 N/A

240 12.9 13,175 400 N/A

264 15.2 6,131 400 N/A

176 9.05 9,607 270 67.6 PASS

212 11.5 11,424 262 65.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 FB COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,738

Naphthalene-d8 (I) 24,526

Acenaphthene-d10 (I) 12,610

Phenanthrene-d10 (I) 20,821

Chrysene-d12 (I) 13,175

Perylene-d12 (I) 6,131

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 52 of 129
Sample ID: DF: 1.00

Data File: W1000697.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 RB FILTER

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 53 of 129
Sample ID: DF: 1.00

Data File: W1000697.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 RB FILTER

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 10.5 185,789 5.89 29.4 

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 343,678 40.0 N/A

136 6.77 1,191,271 40.0 N/A

164 8.52 649,761 40.0 N/A

188 10.0 1,124,810 40.0 N/A

240 12.9 1,033,322 40.0 N/A

264 15.3 884,704 40.0 N/A

112 4.41 21,936 2.29 11.4 FAIL

99 5.13 138,962 12.4 62.0 PASS

330 9.32 41,345 15.0 75.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 343,678

Naphthalene-d8 (I) 1,191,271

Acenaphthene-d10 (I) 649,761

Phenanthrene-d10 (I) 1,124,810

Chrysene-d12 (I) 1,033,322

Perylene-d12 (I) 884,704

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 54 of 129
Sample ID: DF: 1.00

Data File: W1000841.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 7,666 400 N/A

136 6.76 24,412 400 N/A

164 8.52 13,688 400 N/A

188 10.0 22,769 400 N/A

240 12.9 16,433 400 N/A

264 15.2 8,041 400 N/A

176 9.04 10,659 276 69.1 PASS

212 11.5 14,887 312 78.1 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 RB FILTER

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,666

Naphthalene-d8 (I) 24,412

Acenaphthene-d10 (I) 13,688

Phenanthrene-d10 (I) 22,769

Chrysene-d12 (I) 16,433

Perylene-d12 (I) 8,041

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 55 of 129
Sample ID: DF: 1.00

Data File: W1000904.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 RB FILTER RR

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 56 of 129
Sample ID: DF: 1.00

Data File: W1000904.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 RB FILTER RR

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 10.5 237,878 5.95 29.7 

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.54 404,847 40.0 N/A

136 6.76 1,428,263 40.0 N/A

164 8.52 814,029 40.0 N/A

188 10.0 1,425,829 40.0 N/A

240 12.9 1,240,068 40.0 N/A

264 15.2 1,025,500 40.0 N/A

112 4.41 23,880 2.12 10.6 FAIL

99 5.13 149,272 11.3 56.5 PASS

330 9.31 54,626 15.6 78.2 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.54 5.54 408,357 Pass

6.76 6.76 1,410,541 Pass

8.52 8.52 845,708 Pass

10.04 10.03 1,540,126 Pass

12.91 12.89 1,379,541 Pass

15.24 15.22 1,173,932 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 404,847

Naphthalene-d8 (I) 1,428,263

Acenaphthene-d10 (I) 814,029

Phenanthrene-d10 (I) 1,425,829

Chrysene-d12 (I) 1,240,068

Perylene-d12 (I) 1,025,500

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 57 of 129
Sample ID: DF: 1.00

Data File: W1000698.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 RB RINSE

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 58 of 129
Sample ID: DF: 1.00

Data File: W1000698.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 RB RINSE

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 404,542 40.0 N/A

136 6.77 1,425,815 40.0 N/A

164 8.52 803,639 40.0 N/A

188 10.0 1,451,937 40.0 N/A

240 12.9 1,331,671 40.0 N/A

264 15.3 1,128,023 40.0 N/A

112 4.42 159,563 14.1 70.7 PASS

99 5.13 142,658 10.8 54.0 PASS

330 9.32 49,081 13.8 69.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 404,542

Naphthalene-d8 (I) 1,425,815

Acenaphthene-d10 (I) 803,639

Phenanthrene-d10 (I) 1,451,937

Chrysene-d12 (I) 1,331,671

Perylene-d12 (I) 1,128,023

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 59 of 129
Sample ID: DF: 1.00

Data File: W1000842.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 9,334 400 N/A

136 6.77 30,111 400 N/A

164 8.52 16,135 400 N/A

188 10.0 28,573 400 N/A

240 12.9 21,058 400 N/A

264 15.2 9,535 400 N/A

176 9.05 10,715 236 58.9 PASS

212 11.5 16,220 271 67.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.77 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 RB RINSE

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 9,334

Naphthalene-d8 (I) 30,111

Acenaphthene-d10 (I) 16,135

Phenanthrene-d10 (I) 28,573

Chrysene-d12 (I) 21,058

Perylene-d12 (I) 9,535

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 60 of 129
Sample ID: DF: 1.00

Data File: W1000699.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

0310-130 RB XAD

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 61 of 129
Sample ID: DF: 1.00

Data File: W1000699.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 RB XAD

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 372,294 40.0 N/A

136 6.77 1,275,792 40.0 N/A

164 8.52 693,778 40.0 N/A

188 10.0 1,177,451 40.0 N/A

240 12.9 1,080,727 40.0 N/A

264 15.3 907,920 40.0 N/A

112 4.41 173,084 16.7 83.4 PASS

99 5.13 216,324 17.8 89.1 PASS

82 6.05 203,560 17.1 85.5 PASS

172 7.80 443,800 19.2 96.0 PASS

330 9.32 43,461 15.1 75.3 PASS

244 11.6 423,188 19.1 95.3 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 372,294

Naphthalene-d8 (I) 1,275,792

Acenaphthene-d10 (I) 693,778

Phenanthrene-d10 (I) 1,177,451

Chrysene-d12 (I) 1,080,727

Perylene-d12 (I) 907,920

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 62 of 129
Sample ID: DF: 1.00

Data File: W1000843.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 3,517 52.6 263 

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,392 400 N/A

136 6.76 27,387 400 N/A

164 8.52 14,503 400 N/A

188 10.0 24,543 400 N/A

240 12.9 19,168 400 N/A

264 15.2 8,853 400 N/A

176 9.05 12,384 303 75.7 PASS

212 11.5 15,898 310 77.4 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.04 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

0310-130 RB XAD

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,392

Naphthalene-d8 (I) 27,387

Acenaphthene-d10 (I) 14,503

Phenanthrene-d10 (I) 24,543

Chrysene-d12 (I) 19,168

Perylene-d12 (I) 8,853

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 63 of 129
Sample ID: DF: 1.00

Data File: W1000695.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

0310-130 MB FH/BH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 64 of 129
Sample ID: DF: 1.00

Data File: W1000695.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 MB FH/BH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 342,488 40.0 N/A

136 6.77 1,190,628 40.0 N/A

164 8.53 667,880 40.0 N/A

188 10.0 1,187,416 40.0 N/A

240 12.9 1,053,908 40.0 N/A

264 15.3 871,945 40.0 N/A

112 4.41 161,285 16.9 84.4 PASS

99 5.13 205,958 18.4 92.2 PASS

82 6.05 190,984 17.4 87.1 PASS

172 7.80 418,662 18.8 94.1 PASS

330 9.32 43,712 15.0 75.1 PASS

244 11.6 421,090 18.8 94.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 342,488

Naphthalene-d8 (I) 1,190,628

Acenaphthene-d10 (I) 667,880

Phenanthrene-d10 (I) 1,187,416

Chrysene-d12 (I) 1,053,908

Perylene-d12 (I) 871,945

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 65 of 129
Sample ID: DF: 1.00

Data File: W1000835.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 6.78 1,984 27.2 136 

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 9,044 400 N/A

136 6.76 29,886 400 N/A

164 8.52 15,939 400 N/A

188 10.0 26,833 400 N/A

240 12.9 20,620 400 N/A

264 15.2 10,675 400 N/A

176 9.04 14,828 330 82.5 PASS

212 11.5 18,397 328 81.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 6,030 Pass

6.77 6.76 19,649 Pass

8.52 8.52 10,380 Pass

10.04 10.04 17,252 Pass

12.92 12.91 14,344 Pass

15.25 15.24 7,069 Pass

Compound

0310-130 MB FH/BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 9,044

Naphthalene-d8 (I) 29,886

Acenaphthene-d10 (I) 15,939

Phenanthrene-d10 (I) 26,833

Chrysene-d12 (I) 20,620

Perylene-d12 (I) 10,675

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 66 of 129
Sample ID: DF: 1.00

Data File: W1000696.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

167 NA 0.00 0.705 3.53 ND

Compound

0310-130 MB COND

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

4-Chlorophenyl-phenylether

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Carbazole

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 67 of 129
Sample ID: DF: 1.00

Data File: W1000696.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

0310-130 MB COND

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 NA 0.00 1.04 5.19 ND

184 NA 0.00 22.8 114 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags

152 5.55 397,614 40.0 N/A

136 6.77 1,366,044 40.0 N/A

164 8.52 762,736 40.0 N/A

188 10.0 1,329,616 40.0 N/A

240 12.9 1,201,168 40.0 N/A

264 15.3 1,018,358 40.0 N/A

112 4.41 152,082 13.7 68.6 PASS

99 5.13 161,331 12.4 62.2 PASS

330 9.32 46,332 14.2 71.1 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.52 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Di-n-butylphthalate

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr)

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 397,614

Naphthalene-d8 (I) 1,366,044

Acenaphthene-d10 (I) 762,736

Phenanthrene-d10 (I) 1,329,616

Chrysene-d12 (I) 1,201,168

Perylene-d12 (I) 1,018,358

EA# 

0310-130 scan summaries 5/14/2010

0310-130 Page 68 of 129
Sample ID: DF: 1.00

Data File: W1000836.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 7,634 400 N/A

136 6.76 24,699 400 N/A

164 8.52 13,088 400 N/A

188 10.0 22,657 400 N/A

240 12.9 15,103 400 N/A

264 15.2 7,037 400 N/A

176 9.05 9,518 258 64.5 PASS

212 11.5 13,616 287 71.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 6,030 Pass

6.77 6.76 19,649 Pass

8.52 8.52 10,380 Pass

10.04 10.04 17,252 Pass

12.92 12.91 14,344 Pass

15.25 15.25 7,069 Pass

Compound

0310-130 MB COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene-d10 (surr)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr)

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,634

Naphthalene-d8 (I) 24,699

Acenaphthene-d10 (I) 13,088

Phenanthrene-d10 (I) 22,657

Chrysene-d12 (I) 15,103

Perylene-d12 (I) 7,037

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 69 of 129
Sample ID: DF: 1.00

Data File: W1000694.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

128 NA 0.00 0.665 3.33 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.618 3.09 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

152 NA 0.00 0.675 3.37 ND

154 NA 0.00 0.934 4.67 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

166 NA 0.00 0.783 3.92 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

178 NA 0.00 0.771 3.86 ND

178 NA 0.00 0.760 3.80 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

ch2cl2 system blank

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

Naphthalene

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

2-Methylnaphthalene

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

Acenaphthylene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

Acenaphthene (CCC)

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

Phenanthrene

4-Chlorophenyl-phenylether

Fluorene

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Anthracene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 70 of 129
Sample ID: DF: 1.00

Data File: W1000694.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

ch2cl2 system blank

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

202 NA 0.00 0.919 4.60 ND

184 NA 0.00 22.8 114 ND

202 NA 0.00 0.937 4.69 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

228 NA 0.00 0.550 2.75 ND

228 NA 0.00 0.556 2.78 ND

149 NA 0.00 0.644 3.22 ND

252 NA 0.00 0.300 1.50 ND

252 NA 0.00 0.356 1.78 ND

252 NA 0.00 0.340 1.70 ND

252 NA 0.00 0.340 1.70 ND

252 NA 0.00 0.340 1.70 ND

276 NA 0.00 0.300 1.50 ND

278 NA 0.00 0.425 2.13 ND

276 NA 0.00 0.352 1.76 ND

Rec. (%) Flags

152 5.55 424,676 40.0 N/A

136 6.77 1,477,035 40.0 N/A

164 8.53 839,683 40.0 N/A

188 10.0 1,468,828 40.0 N/A

240 12.9 1,421,901 40.0 N/A

264 15.3 1,224,708 40.0 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Fluoranthene (CCC)

Pyrene

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

Benzo(a)anthracene

Chrysene

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

1,4-Dichlorobenzene-d4 (I) 424,676

Naphthalene-d8 (I) 1,477,035

Acenaphthene-d10 (I) 839,683

Phenanthrene-d10 (I) 1,468,828

Chrysene-d12 (I) 1,421,901

Perylene-d12 (I) 1,224,708

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 71 of 129
Sample ID: DF: 1.00

Data File: W1000900.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags

74 NA 0.00 0.772 3.86 ND

94 NA 0.00 0.649 3.25 ND

66 NA 0.00 0.694 3.47 ND

63 NA 0.00 0.788 3.94 ND

128 NA 0.00 0.624 3.12 ND

146 NA 0.00 0.558 2.79 ND

146 NA 0.00 0.528 2.64 ND

108 NA 0.00 0.700 3.50 ND

146 NA 0.00 0.558 2.79 ND

107 NA 0.00 0.677 3.39 ND

107 NA 0.00 0.591 2.95 ND

70 NA 0.00 0.832 4.16 ND

117 NA 0.00 0.632 3.16 ND

77 NA 0.00 0.816 4.08 ND

82 NA 0.00 0.748 3.74 ND

107 NA 0.00 0.729 3.64 ND

139 NA 0.00 0.669 3.35 ND

93 NA 0.00 0.732 3.66 ND

162 NA 0.00 0.652 3.26 ND

180 NA 0.00 0.617 3.09 ND

128 NA 0.00 0.665 3.33 ND

65 NA 0.00 0.849 4.24 ND

225 NA 0.00 0.609 3.05 ND

107 NA 0.00 0.661 3.31 ND

142 NA 0.00 0.618 3.09 ND

142 NA 0.00 0.613 3.07 ND

237 NA 0.00 8.12 40.6 ND

196 NA 0.00 0.738 3.69 ND

196 NA 0.00 0.541 2.70 ND

162 NA 0.00 0.652 3.26 ND

168 NA 0.00 0.672 3.36 ND

163 NA 0.00 0.809 4.05 ND

168 NA 0.00 0.819 4.09 ND

165 NA 0.00 0.775 3.88 ND

168 NA 0.00 0.777 3.89 ND

152 NA 0.00 0.675 3.37 ND

154 NA 0.00 0.934 4.67 ND

184 NA 0.00 5.05 25.3 ND

139 NA 0.00 5.78 28.9 ND

165 NA 0.00 0.804 4.02 ND

168 NA 0.00 0.688 3.44 ND

232 NA 0.00 0.761 3.80 ND

232 NA 0.00 0.701 3.50 ND

149 NA 0.00 1.02 5.10 ND

204 NA 0.00 0.754 3.77 ND

166 NA 0.00 0.783 3.92 ND

198 NA 0.00 5.16 25.8 ND

169 NA 0.00 0.716 3.58 ND

77 NA 0.00 0.991 4.96 ND

248 NA 0.00 0.671 3.35 ND

284 NA 0.00 0.546 2.73 ND

266 NA 0.00 0.565 2.83 ND

178 NA 0.00 0.771 3.86 ND

178 NA 0.00 0.760 3.80 ND

167 NA 0.00 0.705 3.53 ND

149 NA 0.00 1.04 5.19 ND

Compound

ch2cl2 system blank

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

Naphthalene

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

2-Methylnaphthalene

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

Acenaphthylene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

Acenaphthene (CCC)

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

Phenanthrene

4-Chlorophenyl-phenylether

Fluorene

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Anthracene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 72 of 129
Sample ID: DF: 1.00

Data File: W1000900.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Compound Flags

ch2cl2 system blank

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

202 NA 0.00 0.919 4.60 ND

184 NA 0.00 22.8 114 ND

202 NA 0.00 0.937 4.69 ND

149 NA 0.00 0.810 4.05 ND

212 NA 0.00 10.8 53.9 ND

149 NA 0.00 1.74 8.71 ND

252 NA 0.00 9.36 46.8 ND

228 NA 0.00 0.550 2.75 ND

228 NA 0.00 0.556 2.78 ND

149 NA 0.00 0.644 3.22 ND

252 NA 0.00 0.300 1.50 ND

252 NA 0.00 0.356 1.78 ND

252 NA 0.00 0.340 1.70 ND

252 NA 0.00 0.340 1.70 ND

252 NA 0.00 0.340 1.70 ND

276 NA 0.00 0.300 1.50 ND

278 NA 0.00 0.425 2.13 ND

276 NA 0.00 0.352 1.76 ND

Rec. (%) Flags

152 5.54 423,823 40.0 N/A

136 6.76 1,475,587 40.0 N/A

164 8.52 838,760 40.0 N/A

188 10.0 1,418,067 40.0 N/A

240 12.9 1,171,268 40.0 N/A

264 15.2 995,224 40.0 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.54 5.54 408,357 Pass

6.76 6.76 1,410,541 Pass

8.52 8.52 845,708 Pass

10.04 10.03 1,540,126 Pass

12.91 12.90 1,379,541 Pass

15.24 15.22 1,173,932 Pass

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Fluoranthene (CCC)

Pyrene

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

Benzo(a)anthracene

Chrysene

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

1,4-Dichlorobenzene-d4 (I) 423,823

Naphthalene-d8 (I) 1,475,587

Acenaphthene-d10 (I) 838,760

Phenanthrene-d10 (I) 1,418,067

Chrysene-d12 (I) 1,171,268

Perylene-d12 (I) 995,224

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 73 of 129
Sample ID: DF: 1.00

Data File: W1000816.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 1.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 10.0 ND

142 NA 0.00 10.0 10.0 ND

152 NA 0.00 10.0 10.0 ND

154 NA 0.00 10.0 10.0 ND

166 NA 0.00 10.0 10.0 ND

178 NA 0.00 10.0 10.0 ND

178 NA 0.00 10.0 10.0 ND

202 NA 0.00 10.0 10.0 ND

202 NA 0.00 10.0 10.0 ND

228 NA 0.00 10.0 10.0 ND

228 NA 0.00 10.0 10.0 ND

252 NA 0.00 10.0 10.0 ND

252 NA 0.00 10.0 10.0 ND

252 NA 0.00 10.0 10.0 ND

252 NA 0.00 10.0 10.0 ND

252 NA 0.00 10.0 10.0 ND

276 NA 0.00 10.0 10.0 ND

278 NA 0.00 10.0 10.0 ND

276 NA 0.00 10.0 10.0 ND

Rec. (%) Flags

152 5.55 7,364 400 N/A

136 6.76 23,705 400 N/A

164 8.53 12,593 400 N/A

188 10.1 20,731 400 N/A

240 12.9 14,294 400 N/A

264 15.3 6,344 400 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 6,030 Pass

6.77 6.76 19,649 Pass

8.52 8.53 10,380 Pass

10.04 10.05 17,252 Pass

12.92 12.92 14,344 Pass

15.25 15.26 7,069 Pass

Compound

ch2cl2 system blank

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 7,364

Naphthalene-d8 (I) 23,705

Acenaphthene-d10 (I) 12,593

Phenanthrene-d10 (I) 20,731

Chrysene-d12 (I) 14,294

Perylene-d12 (I) 6,344

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 74 of 129
Sample ID: DF: 1.00

Data File: W1000840.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ng/mL)

Catch

Weight

(ng)

Flags

128 NA 0.00 10.0 50.0 ND

142 NA 0.00 10.0 50.0 ND

152 NA 0.00 10.0 50.0 ND

154 NA 0.00 10.0 50.0 ND

166 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

178 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

202 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

228 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

252 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

278 NA 0.00 10.0 50.0 ND

276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags

152 5.55 8,180 400 N/A

136 6.76 26,324 400 N/A

164 8.52 14,110 400 N/A

188 10.0 22,781 400 N/A

240 12.9 15,899 400 N/A

264 15.2 7,331 400 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 7,952 Pass

6.76 6.76 26,177 Pass

8.52 8.52 13,968 Pass

10.04 10.05 23,008 Pass

12.90 12.91 18,105 Pass

15.23 15.24 8,548 Pass

Compound

ch2cl2 system blank

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Naphthalene

2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Acenaphthene-d10 (I)

Acenaphthylene

Acenaphthene (CCC)

Fluorene

Phenanthrene-d10 (I)

Phenanthrene

Anthracene

Fluoranthene (CCC)

Perylene

Pyrene

Chrysene-d12 (I)

Benzo(a)anthracene

Chrysene

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Internal Standard Sample

Name IS Area

1,4-Dichlorobenzene-d4 (I) 8,180

Naphthalene-d8 (I) 26,324

Acenaphthene-d10 (I) 14,110

Phenanthrene-d10 (I) 22,781

Chrysene-d12 (I) 15,899

Perylene-d12 (I) 7,331

Company

Analyst

Parameters

# Samples

Kleinfelder, Inc.

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

EA# 

0310-130 sim summaries 5/14/2010

0310-130 Page 75 of 129
Sample ID: DF: 1.00

Data File: W1000692.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags Tag Value % Diff. 

From Tag %Rec

74 3.43 127,857 19.7 98.4 100 1.6 98.4

94 5.15 275,962 19.0 95.0 100 5.0 95.0

66 5.24 129,636 18.2 91.1 100 8.9 91.1

63 5.25 174,122 18.4 92.0 100 8.0 92.0

128 5.36 251,480 18.8 94.0 100 6.0 94.0

146 5.51 293,849 18.4 91.8 100 8.2 91.8

146 5.57 304,163 18.5 92.5 100 7.5 92.5

108 5.63 148,174 19.0 95.2 100 4.8 95.2

146 5.71 282,402 18.7 93.3 100 6.7 93.3

107 5.70 195,301 19.4 97.2 100 2.8 97.2

107 5.83 248,243 19.3 96.7 100 3.3 96.7

70 5.86 163,261 18.5 92.4 100 7.6 92.4

117 6.04 104,939 18.2 91.1 100 8.9 91.1

77 6.07 249,614 19.1 95.7 100 4.3 95.7

82 6.28 421,153 18.8 93.8 100 6.2 93.8

107 6.35 255,759 19.1 95.3 100 4.7 95.3

139 6.37 148,379 19.8 98.9 100 1.1 98.9

93 6.44 256,671 18.5 92.6 100 7.4 92.6

162 6.60 220,597 19.1 95.7 100 4.3 95.7

180 6.70 263,426 19.3 96.5 100 3.5 96.5

128 6.79 787,947 19.5 97.5 100 2.5 97.5

65 6.80 89,485 18.1 90.4 100 9.6 90.4

225 6.88 157,266 18.8 94.1 100 5.9 94.1

107 7.23 218,502 19.2 95.9 100 4.1 95.9

142 7.46 497,095 18.7 93.5 100 6.5 93.5

142 7.57 512,223 19.8 98.8 100 1.2 98.8

237 7.62 158,143 18.3 91.5 100 8.5 91.5

196 7.72 169,905 19.7 98.6 100 1.4 98.6

196 7.76 177,696 19.8 98.8 100 1.2 98.8

162 7.96 497,050 19.9 99.7 100 0.3 99.7

168 8.15 82,679 19.5 97.6 100 2.4 97.6

163 8.17 573,338 20.1 100 100 0.4 100

168 8.23 95,328 19.6 98.1 100 1.9 98.1

165 8.25 136,188 19.8 99.1 100 0.9 99.1

168 8.32 64,201 19.3 96.4 100 3.6 96.4

152 8.39 792,756 20.6 103 100 2.8 103

154 8.56 500,293 19.4 97.2 100 2.8 97.2

184 8.54 54,941 15.5 77.5 100 22.5 77.5

139 8.56 98,415 18.5 92.4 100 7.6 92.4

165 8.66 172,732 19.8 99.1 100 0.9 99.1

168 8.73 702,072 20.0 99.9 100 0.1 99.9

232 8.79 148,491 19.1 95.5 100 4.5 95.5

232 8.84 151,868 19.4 97.1 100 2.9 97.1

149 8.87 559,238 19.8 99.2 100 0.8 99.2

204 9.04 294,461 19.9 99.4 100 0.6 99.4

166 9.08 577,887 20.1 101 100 0.5 101

198 9.09 91,821 18.6 93.1 100 6.9 93.1

169 9.15 505,629 20.2 101 100 1.2 101

77 9.20 475,886 18.9 94.5 100 5.5 94.5

248 9.54 184,636 19.9 99.4 100 0.6 99.4

284 9.65 182,678 20.0 100 100 0.0 100

266 9.83 102,953 18.8 93.9 100 6.1 93.9

178 10.1 830,080 20.0 100 100 0.1 100

178 10.1 830,403 20.5 103 100 2.6 103

167 10.3 711,806 19.8 99.2 100 0.8 99.2

149 10.5 906,502 20.1 101 100 0.6 101

202 11.3 872,641 20.6 103 100 3.1 103

184 NA 0.00 22.8 114 ND 100 13.8 0.0

202 11.5 921,459 20.3 102 100 1.7 102

Compound

0310-130 LCS FH/BH

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

Naphthalene

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

2-Methylnaphthalene

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

Acenaphthylene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

Acenaphthene (CCC)

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

Benzidine

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

Fluoranthene (CCC)

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

Phenanthrene

4-Chlorophenyl-phenylether

Fluorene

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Anthracene

Carbazole

Di-n-butylphthalate

Pyrene

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 76 of 129
Sample ID: DF: 1.00

Data File: W1000692.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags Tag Value % Diff. 

From Tag Compound %Rec

0310-130 LCS FH/BH

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 12.1 383,926 19.7 98.6 100 1.4 98.6

212 12.1 398,801 16.5 82.5 100 17.5 82.5

149 12.7 526,654 19.8 99.0 100 1.0 99.0

252 12.8 226,255 19.8 98.8 100 1.2 98.8

228 12.9 794,102 19.9 99.4 100 0.6 99.4

228 13.0 757,947 20.3 102 100 1.6 102

149 13.6 809,565 20.0 100 100 0.1 100

252 14.6 697,965 19.5 97.6 100 2.4 97.6

252 14.6 720,137 20.6 103 100 3.1 103

252 15.1 640,733 19.2 96.1 100 3.9 96.1

252 15.2 641,709 20.0 100 100 0.0 100

252 15.3 648,171 19.3 96.6 100 3.4 96.6

276 17.4 593,345 19.8 98.9 100 1.1 98.9

278 17.4 488,557 19.4 97.0 100 3.0 97.0

276 18.1 471,657 20.0 99.8 100 0.2 99.8

Rec. (%) Flags

152 5.55 439,735 40.0 N/A

136 6.77 1,535,881 40.0 N/A

164 8.53 891,526 40.0 N/A

188 10.0 1,605,650 40.0 N/A

240 12.9 1,554,374 40.0 N/A

264 15.3 1,287,984 40.0 N/A

112 4.41 208,570 17.0 85.1 PASS

99 5.13 270,393 18.8 94.2 PASS

82 6.05 264,722 18.8 94.1 PASS

172 7.80 590,866 19.9 99.5 PASS

330 9.32 75,831 19.3 96.4 PASS

244 11.6 611,016 20.2 101 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

Benzo(a)anthracene

2,4,6-Tribromophenol (surr)

Chrysene

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 439,735

Naphthalene-d8 (I) 1,535,881

Acenaphthene-d10 (I) 891,526

Phenanthrene-d10 (I) 1,605,650

Chrysene-d12 (I) 1,554,374

Perylene-d12 (I) 1,287,984

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 77 of 129
Sample ID: DF: 1.00

Data File: W1000896.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags Tag Value % Diff. 

From Tag %Rec

74 3.42 106,237 18.2 91.2 100 8.8 91.2

94 5.14 223,019 17.1 85.7 100 14.3 85.7

66 5.23 105,872 16.6 83.1 100 16.9 83.1

63 5.24 142,876 16.9 84.3 100 15.7 84.3

128 5.35 201,776 16.8 84.2 100 15.8 84.2

146 5.50 227,625 15.9 79.4 100 20.6 79.4

146 5.56 234,913 16.0 79.8 100 20.2 79.8

108 5.62 115,484 16.6 82.9 100 17.1 82.9

146 5.71 222,203 16.4 81.9 100 18.1 81.9

107 5.69 159,784 17.8 88.8 100 11.2 88.8

107 5.83 202,848 17.7 88.3 100 11.7 88.3

70 5.85 143,875 18.2 90.9 100 9.1 90.9

117 6.04 86,059 16.7 83.4 100 16.6 83.4

77 6.06 209,033 17.9 89.5 100 10.5 89.5

82 6.27 360,125 17.8 88.8 100 11.2 88.8

107 6.35 211,385 17.4 87.2 100 12.8 87.2

139 6.37 117,660 17.4 86.8 100 13.2 86.8

93 6.44 216,402 17.3 86.4 100 13.6 86.4

162 6.59 174,361 16.8 83.8 100 16.2 83.8

180 6.69 202,108 16.4 82.0 100 18.0 82.0

128 6.78 630,656 17.3 86.4 100 13.6 86.4

65 6.79 73,902 16.5 82.7 100 17.3 82.7

225 6.88 115,982 15.4 76.8 100 23.2 76.8

107 7.23 177,672 17.3 86.3 100 13.7 86.3

142 7.46 395,422 16.5 82.3 100 17.7 82.3

142 7.56 406,692 17.4 86.9 100 13.1 86.9

237 7.61 115,688 14.8 74.1 100 25.9 74.1

196 7.72 129,451 17.0 85.1 100 14.9 85.1

196 7.76 134,579 16.9 84.7 100 15.3 84.7

162 7.95 385,228 17.5 87.5 100 12.5 87.5

168 8.13 65,718 17.6 87.9 100 12.1 87.9

163 8.17 457,433 18.1 90.7 100 9.3 90.7

168 8.22 76,789 17.9 89.5 100 10.5 89.5

165 8.24 108,735 17.9 89.7 100 10.3 89.7

168 8.31 51,426 17.5 87.5 100 12.5 87.5

152 8.38 618,802 18.2 90.9 100 9.1 90.9

154 8.55 390,501 17.2 85.9 100 14.1 85.9

184 8.53 39,365 12.6 62.9 100 37.1 62.9

139 8.55 76,527 16.3 81.4 100 18.6 81.4

165 8.66 138,257 18.0 89.8 100 10.2 89.8

168 8.72 536,719 17.3 86.5 100 13.5 86.5

232 8.79 111,491 16.3 81.3 100 18.7 81.3

232 8.83 117,123 17.0 84.8 100 15.2 84.8

149 8.86 461,199 18.5 92.7 100 7.3 92.7

204 9.03 222,038 17.0 84.9 100 15.1 84.9

166 9.07 444,312 17.5 87.5 100 12.5 87.5

198 9.08 68,634 15.8 78.9 100 21.1 78.9

169 9.14 393,729 17.9 89.3 100 10.7 89.3

77 9.19 394,187 17.7 88.7 100 11.3 88.7

248 9.53 140,691 17.6 88.2 100 11.8 88.2

284 9.64 143,199 18.2 91.2 100 8.8 91.2

266 9.82 73,948 15.7 78.5 100 21.5 78.5

178 10.1 630,165 17.7 88.5 100 11.5 88.5

178 10.1 626,015 18.0 90.1 100 9.9 90.1

167 10.2 549,488 17.8 89.1 100 10.9 89.1

149 10.5 759,097 19.6 98.1 100 1.9 98.1

202 11.3 644,622 17.7 88.7 100 11.3 88.7

184 NA 0.00 22.8 114 ND 100 13.8 0.0

202 11.5 677,184 17.4 87.0 100 13.0 87.0

Compound

0310-130 LCS FH/BH RR

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

Naphthalene

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

2-Methylnaphthalene

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

Acenaphthylene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

Acenaphthene (CCC)

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

Benzidine

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

Fluoranthene (CCC)

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

Phenanthrene

4-Chlorophenyl-phenylether

Fluorene

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Anthracene

Carbazole

Di-n-butylphthalate

Pyrene

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 78 of 129
Sample ID: DF: 1.00

Data File: W1000896.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 2

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags Tag Value % Diff. 

From Tag Compound %Rec

0310-130 LCS FH/BH RR

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

149 12.1 292,101 19.4 96.8 100 3.2 96.8

212 12.1 278,444 14.9 74.4 100 25.6 74.4

149 12.7 396,825 19.3 96.3 100 3.7 96.3

252 12.8 163,697 18.5 92.3 100 7.7 92.3

228 12.9 547,464 17.7 88.4 100 11.6 88.4

228 12.9 524,387 18.1 90.7 100 9.3 90.7

149 13.6 607,766 19.4 97.0 100 3.0 97.0

252 14.5 511,039 17.7 88.7 100 11.3 88.7

252 14.6 488,433 17.4 86.8 100 13.2 86.8

252 15.0 451,093 16.8 84.0 100 16.0 84.0

252 15.1 458,161 17.7 88.6 100 11.4 88.6

252 15.3 458,800 17.0 84.8 100 15.2 84.8

276 17.4 402,769 16.7 83.3 100 16.7 83.3

278 17.4 331,739 16.3 81.7 100 18.3 81.7

276 18.0 323,726 17.0 85.0 100 15.0 85.0

Rec. (%) Flags

152 5.54 393,868 40.0 N/A

136 6.76 1,387,356 40.0 N/A

164 8.52 786,932 40.0 N/A

188 10.0 1,379,461 40.0 N/A

240 12.9 1,204,274 40.0 N/A

264 15.2 1,037,776 40.0 N/A

112 4.41 162,877 14.8 74.2 PASS

99 5.13 217,140 16.9 84.5 PASS

82 6.04 217,980 17.3 86.5 PASS

172 7.79 448,262 17.1 85.5 PASS

330 9.32 57,816 17.1 85.5 PASS

244 11.6 445,651 17.1 85.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.54 5.54 408,357 Pass

6.76 6.76 1,410,541 Pass

8.52 8.52 845,708 Pass

10.04 10.03 1,540,126 Pass

12.91 12.89 1,379,541 Pass

15.24 15.22 1,173,932 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Terphenyl-d14 (surr)

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

Benzo(a)anthracene

2,4,6-Tribromophenol (surr)

Chrysene

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr)

Nitrobenzene-d5 (surr)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 393,868

Naphthalene-d8 (I) 1,387,356

Acenaphthene-d10 (I) 786,932

Phenanthrene-d10 (I) 1,379,461

Chrysene-d12 (I) 1,204,274

Perylene-d12 (I) 1,037,776

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 79 of 129
Sample ID: DF: 1.00

Data File: W1000693.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags Tag Value % Diff. 

From Tag %Rec

74 3.42 81,782 15.2 76.2 100 23.8 76.2

94 5.15 148,790 12.4 62.0 100 38.0 62.0

66 5.24 97,411 16.6 82.9 100 17.1 82.9

63 5.25 123,418 15.8 78.9 100 21.1 78.9

128 5.36 167,081 15.1 75.6 100 24.4 75.6

146 5.51 134,913 10.2 51.0 100 49.0 51.0

146 5.57 142,182 10.5 52.4 100 47.6 52.4

108 5.63 103,792 16.2 80.8 100 19.2 80.8

146 5.71 138,345 11.1 55.3 100 44.7 55.3

107 5.70 135,318 16.3 81.5 100 18.5 81.5

107 5.83 172,647 16.3 81.5 100 18.5 81.5

70 5.86 117,213 16.1 80.3 100 19.7 80.3

117 6.04 47,386 9.97 49.8 100 50.2 49.8

77 6.07 170,635 15.8 79.2 100 20.8 79.2

82 6.28 307,731 16.5 82.7 100 17.3 82.7

107 6.35 181,582 16.3 81.6 100 18.4 81.6

139 6.37 95,024 15.3 76.5 100 23.5 76.5

93 6.44 183,329 16.0 79.8 100 20.2 79.8

162 6.60 148,949 15.6 78.0 100 22.0 78.0

180 6.70 151,174 13.4 66.9 100 33.1 66.9

128 6.79 484,688 14.5 72.4 100 27.6 72.4

65 6.80 70,686 17.2 86.2 100 13.8 86.2

225 6.88 81,453 11.8 58.8 100 41.2 58.8

107 7.23 170,013 18.0 90.1 100 9.9 90.1

142 7.46 324,648 14.7 73.7 100 26.3 73.7

142 7.57 338,189 15.8 78.8 100 21.2 78.8

237 7.62 88,217 12.3 61.6 100 38.4 61.6

196 7.72 123,047 17.3 86.7 100 13.3 86.7

196 7.77 131,625 17.8 88.8 100 11.2 88.8

162 7.96 342,368 16.7 83.3 100 16.7 83.3

168 8.15 65,436 18.8 93.8 100 6.2 93.8

163 8.17 443,300 18.8 94.2 100 5.8 94.2

168 8.23 76,017 19.0 95.0 100 5.0 95.0

165 8.25 105,580 18.7 93.3 100 6.7 93.3

168 8.32 49,124 17.9 89.6 100 10.4 89.6

152 8.39 581,626 18.3 91.6 100 8.4 91.6

154 8.56 368,557 17.4 86.9 100 13.1 86.9

184 8.54 34,159 11.7 58.5 100 41.5 58.5

139 8.56 52,649 12.0 60.0 100 40.0 60.0

165 8.66 135,361 18.9 94.3 100 5.7 94.3

168 8.73 514,397 17.8 88.8 100 11.2 88.8

232 8.79 111,889 17.5 87.4 100 12.6 87.4

232 8.84 116,148 18.0 90.1 100 9.9 90.1

149 8.87 442,399 19.1 95.3 100 4.7 95.3

204 9.04 217,224 17.8 89.0 100 11.0 89.0

166 9.08 445,077 18.8 94.0 100 6.0 94.0

198 9.09 71,516 17.6 88.0 100 12.0 88.0

169 9.15 390,986 19.0 95.0 100 5.0 95.0

77 9.20 396,520 19.1 95.6 100 4.4 95.6

248 9.54 136,241 17.9 89.4 100 10.6 89.4

284 9.65 135,405 18.1 90.3 100 9.7 90.3

266 9.83 76,085 16.9 84.6 100 15.4 84.6

178 10.1 649,385 19.1 95.5 100 4.5 95.5

178 10.1 652,279 19.7 98.3 100 1.7 98.3

167 10.3 579,667 19.7 98.5 100 1.5 98.5

149 10.5 731,172 19.8 98.9 100 1.1 98.9

202 11.3 677,725 19.5 97.6 100 2.4 97.6

Compound

0310-130 LCS COND

3/4-Methylphenol

N-Nitrso-di-n-propylamine (SPCC)

Hexachloroethane

Naphthalene

4-Chloroaniline

1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol

Hexachlorobutadiene (CCC)

2-Methylphenol

N-Nitrosodimethylamine

1,3-Dichlorobenzene

1,4-Dichlorobenzene (CCC)

Benzyl alcohol

1,2-Dichlorobenzene

Phenol (CCC)

Aniline

bis(2-Chloroethyl)ether

2-Chlorophenol

Nitrobenzene

Isophorone

2,4-Dimethylphenol

2-Nitrophenol (CCC)

bis(2-Chloroethoxy)methane

2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC)

2-Methylnaphthalene

1-Methylnaphthalene

Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene

Acenaphthylene

2-Chloronaphthalene

1,4-Dinitrobenzene

2,4,6-Trichlorophenol (CCC)

2,4,5-Trichlorophenol

Acenaphthene (CCC)

2,4-Dinitrophenol (SPCC)

4-Nitrophenol (SPCC)

2,4-Dinitrotoluene

Dibenzofuran

1,3-Dinitrobenzene

2,6-Dinitrotoluene

Dimethylphthalate

2,3,4,6-Tetrachlorophenol

Diethlyphthalate

Fluoranthene (CCC)

4-Bromophenyl-phenylether

Hexachlorobenzene

Pentachlorophenol (CCC)

Phenanthrene

4-Chlorophenyl-phenylether

Fluorene

4,6-Dinitro2-methylphenol

N-Nitrosodiphenylamine (CCC)

Azobenzene

Anthracene

Carbazole

Di-n-butylphthalate

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 80 of 129
Sample ID: DF: 1.00

Data File: W1000693.D Aliquot Factor: 1.00

Tank/Misc ID: Extraction Vol (mL): 5.00

ConCal 1

Quant

Ret.

Time

(min)

Area Conc.

(ug/mL)

Catch

Weight

(ug)

Flags Tag Value % Diff. 

From Tag Compound %Rec

0310-130 LCS COND

Company

Analyst

Parameters

# Samples

Kleinfelder

DDA/GLR

EPA Method 8270C

3 Runs & 2 Blanks

Client #

Job #

PO #

Report Date

109381

0310-130

Verbal

5/4/2010

184 NA 0.00 22.8 114 ND 100 13.8 0.0

202 11.5 716,226 19.3 96.3 100 3.7 96.3

149 12.1 307,167 20.0 99.9 100 0.1 99.9

212 12.1 345,981 18.1 90.7 100 9.3 90.7

149 12.7 412,569 19.6 98.2 100 1.8 98.2

252 12.8 176,991 19.6 97.9 100 2.1 97.9

228 12.9 610,035 19.3 96.7 100 3.3 96.7

228 13.0 561,684 19.1 95.3 100 4.7 95.3

149 13.6 632,235 19.8 99.0 100 1.0 99.0

252 14.6 527,759 19.3 96.3 100 3.7 96.3

252 14.6 499,985 18.7 93.5 100 6.5 93.5

252 15.1 474,575 18.6 93.0 100 7.0 93.0

252 15.2 459,381 18.7 93.5 100 6.5 93.5

252 15.3 466,216 18.1 90.7 100 9.3 90.7

276 17.4 403,039 17.5 87.7 100 12.3 87.7

278 17.4 329,496 17.1 85.4 100 14.6 85.4

276 18.1 318,696 17.6 88.1 100 11.9 88.1

Rec. (%) Flags

152 5.55 363,142 40.0 N/A

136 6.77 1,272,532 40.0 N/A

164 8.53 734,393 40.0 N/A

188 10.0 1,317,276 40.0 N/A

240 12.9 1,227,045 40.0 N/A

264 15.3 986,365 40.0 N/A

112 4.41 132,505 13.1 65.4 PASS

99 5.13 147,386 12.4 62.2 PASS

330 9.32 57,708 17.9 89.4 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec.)

Concal Sample Concal Flag

RT RT IS Area

5.55 5.55 424,824 Pass

6.77 6.77 1,446,379 Pass

8.53 8.53 856,584 Pass

10.04 10.04 1,512,934 Pass

12.93 12.92 1,427,833 Pass

15.27 15.26 1,183,172 Pass

2-Fluorophenol (surr)

1,4-Dichlorobenzene-d4 (I)

Naphthalene-d8 (I)

Acenaphthene-d10 (I)

Benzidine

Pyrene

Chrysene-d12 (I)

Butylbenzylphthalate

3,3-Dimethylbenzidine

bis(2-Ethylhexyl)phthalate

3,3'-Dichlorobenzidine

Benzo(a)anthracene

2,4,6-Tribromophenol (surr)

Chrysene

Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene (CCC)

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene

Benzo(g,h,i)perylene

Internal Standard Sample

Name IS Area

Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 363,142

Naphthalene-d8 (I) 1,272,532

Acenaphthene-d10 (I) 734,393

Phenanthrene-d10 (I) 1,317,276

Chrysene-d12 (I) 1,227,045

Perylene-d12 (I) 986,365

0310-130 scan summaries 5/14/2010

EA# 0310-130 Page 81 of 129
Sample 

Chromatograms

6FDQ

EA# 0310-130 Page 82 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000703.D Vial: 14

 Acq On : 23 Apr 2010 4:41 pm Operator: dda/glr

 Sample : 0310-130 U1 R1 FH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 12:04 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

Time-->

Abundance TIC: W1000703.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

bis(2-Ethylhexyl)phthalate

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000703.D W042610X-SIM-PAH.M Wed Apr 28 17:41:23 2010 Page 3

EA# 0310-130 Page 83 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000704.D Vial: 15

 Acq On : 23 Apr 2010 5:08 pm Operator: dda/glr

 Sample : 0310-130 U1 R1 FH LD Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 12:27 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

4200000

Time-->

Abundance TIC: W1000704.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

bis(2-Ethylhexyl)phthalate

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000704.D W042610X-SIM-PAH.M Wed Apr 28 17:41:31 2010 Page 3

EA# 0310-130 Page 84 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000705.D Vial: 16

 Acq On : 23 Apr 2010 5:35 pm Operator: dda/glr

 Sample : 0310-130 U1 R1 FH MS Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 12:29 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

4200000

4400000

4600000

4800000

5000000

5200000

5400000

5600000

5800000

6000000

6200000

Time-->

Abundance TIC: W1000705.D

Benzo(g,h,i)perylene

Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene

Perylene-d12 (I),I Perylene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Benzo(k)fluoranthene Benzo(b)fluoranthene

Di-n-octylphthalate (CCC)

Chrysene Chrysene-d12 (I),I Benzo(a)anthracene

bis(2-Ethylhexyl)phthalate

3,3-Dimethylbenzidine bis(2-ethylhexyl)adipate Butylbenzylphthalate

Pyrene Pyrene-d10 (surr),S

Fluoranthene (CCC)

Di-n-butylphthalate

Carbazole Anthracene Phenanthrene Phenanthrene-d10 (I),I

Pentachlorophenol (CCC)

Hexachlorobenzene 4-Bromophenyl-phenylether

2,4,6-Tribromophenol (surr),S Azobenzene N-Nitrosodiphenylamine (CCC) 4,6-Dinitro2-methylphenol Fluorene 4-Nitroaniline 4-Chlorophenyl-phenylether Fluorene-d10 (surr),S Diethlyphthalate 2,3,4,6-Tetrachlorophenol 2,3,5,6-Tetrachlorophenol Dibenzofuran 2,4-Dinitrotoluene 4-Nitrophenol (SPCC) Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) Acenaphthene-d10 (I),I 3-Nitroaniline Acenaphthylene 1,2-Dinitrobenzene 2,6-Dinitrotoluene 1,3-Dinitrobenzene Dimethylphthalate 1,4-Dinitrobenzene 2-Nitroaniline 2-Chloronaphthalene

2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (CCC) Hexachlorocyclopentadiene (SPCC) 1-Methylnaphthalene 2-Methylnaphthalene

4-Chloro-3 methylphenol (CCC)

Hexachlorobutadiene (CCC) 4-Chloroaniline Naphthalene Naphthalene-d8 (I),I 1,2,4-Trichlorobenzene 2,4-Dichlorophenol (CCC) bis(2-Chloroethoxy)methane 2-Nitrophenol (CCC) 2,4-Dimethylphenol Benzoic acid Isophorone

Nitrobenzene Nitrobenzene-d5 (surr),S Hexachloroethane

N-Nitrso-di-n-propylamine (SPCC) 3/4-Methylphenol bis(2-Chloroisopropyl) ether 1,2-Dichlorobenzene 2-Methylphenol Benzyl alcohol 1,4-Dichlorobenzene (CCC) 1,4-Dichlorobenzene-d4 (I),I 1,3-Dichlorobenzene 2-Chlorophenol bis(2-Chloroethyl)ether Aniline Phenol (CCC) Phenol-d5 (surr),S

2-Fluorophenol (surr),S

Pyridine N-Nitrosodimethylamine

W1000705.D W042610X-SIM-PAH.M Wed Apr 28 17:41:41 2010 Page 3

EA# 0310-130 Page 85 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000706.D Vial: 17

 Acq On : 23 Apr 2010 6:02 pm Operator: dda/glr

 Sample : 0310-130 U1 R1 BH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 28 9:00 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

1000000

2000000

3000000

4000000

5000000

6000000

7000000

8000000

9000000

 1e+07

 1.1e+07

 1.2e+07

 1.3e+07

 1.4e+07

 1.5e+07

 1.6e+07

Time-->

Abundance TIC: W1000706.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

bis(2-ethylhexyl)adipate

bis(2-Ethylhexyl)phthalate

Terphenyl-d14 (surr),S

Di-n-butylphthalate

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Diethlyphthalate

Acenaphthene-d10 (I),I

2-Fluorobiphenyl (surr),S

Naphthalene-d8 (I),I

Benzoic acid

Nitrobenzene-d5 (surr),S

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000706.D W042610X-SIM-PAH.M Wed Apr 28 17:41:49 2010 Page 3

EA# 0310-130 Page 86 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000707.D Vial: 18

 Acq On : 23 Apr 2010 6:29 pm Operator: dda/glr

 Sample : 0310-130 U1 R1 COND Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 13:46 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

Time-->

Abundance TIC: W1000707.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000707.D W042610X-SIM-PAH.M Wed Apr 28 17:41:59 2010 Page 3

EA# 0310-130 Page 87 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000708.D Vial: 19

 Acq On : 23 Apr 2010 6:56 pm Operator: dda/glr

 Sample : 0310-130 U1 R2 FH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 13:51 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

Time-->

Abundance TIC: W1000708.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

bis(2-Ethylhexyl)phthalate

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000708.D W042610X-SIM-PAH.M Wed Apr 28 17:42:08 2010 Page 3

EA# 0310-130 Page 88 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000709.D Vial: 20

 Acq On : 23 Apr 2010 7:22 pm Operator: dda/glr

 Sample : 0310-130 U1 R2 BH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 13:57 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

4200000

Time-->

Abundance TIC: W1000709.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

bis(2-Ethylhexyl)phthalate

Terphenyl-d14 (surr),S

Di-n-butylphthalate

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Diethlyphthalate

Acenaphthene-d10 (I),I

2-Fluorobiphenyl (surr),S

Naphthalene-d8 (I),I

Benzoic acid

Nitrobenzene-d5 (surr),S

1,4-Dichlorobenzene-d4 (I),I

2-Fluorophenol (surr),S

Phenol-d5 (surr),S

W1000709.D W042610X-SIM-PAH.M Wed Apr 28 17:42:17 2010 Page 3

EA# 0310-130 Page 89 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000710.D Vial: 21

 Acq On : 23 Apr 2010 7:49 pm Operator: dda/glr

 Sample : 0310-130 U1 R2 COND Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 14:16 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

Time-->

Abundance TIC: W1000710.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

Benzoic acid

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000710.D W042610X-SIM-PAH.M Wed Apr 28 17:42:27 2010 Page 3

EA# 0310-130 Page 90 of 129
 Quantitation Report (Not Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000711.D Vial: 22

 Acq On : 23 Apr 2010 8:16 pm Operator: dda/glr

 Sample : 0310-130 U1 R3 FH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 14:23 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

500000

1000000

1500000

2000000

2500000

3000000

3500000

4000000

4500000

5000000

5500000

6000000

6500000

7000000

7500000

8000000

8500000

9000000

Time-->

Abundance TIC: W1000711.D

Perylene Benzo(a)pyrene (CCC) Perylene-d12 (I),I

Chrysene Benzo(a)anthracene Chrysene-d12 (I),I

bis(2-Ethylhexyl)phthalate

Di-n-butylphthalate

Pyrene-d10 (surr),S

Butylbenzylphthalate

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Diethlyphthalate

Fluorene-d10 (surr),S

Acenaphthene (CCC) Acenaphthene-d10 (I),I

2-Methylnaphthalene 1-Methylnaphthalene

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene (CCC) 1,3-Dichlorobenzene 1,4-Dichlorobenzene-d4 (I),I Benzyl alcohol

Phenol (CCC)

2-Fluorophenol (surr),S

Phenol-d5 (surr),S

W1000711.D W042610X-SIM-PAH.M Wed Apr 28 17:42:36 2010 Page 3

EA# 0310-130 Page 91 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050410A\W1000921.D Vial: 18

 Acq On : 4 May 2010 1:30 pm Operator: dda\glr

 Sample : 0310-130 U1 R3 BH 2X Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: May 4 13:52 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 22 16:55:57 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

500000

1000000

1500000

2000000

2500000

3000000

3500000

4000000

4500000

5000000

5500000

6000000

6500000

7000000

7500000

8000000

8500000

9000000

9500000

 1e+07

1.05e+07

Time-->

Abundance TIC: W1000921.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

bis(2-ethylhexyl)adipate

bis(2-Ethylhexyl)phthalate

Terphenyl-d14 (surr),S

Di-n-butylphthalate

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Acenaphthene-d10 (I),I

2-Fluorobiphenyl (surr),S

Naphthalene-d8 (I),I

Benzoic acid

Nitrobenzene-d5 (surr),S

1,4-Dichlorobenzene-d4 (I),I

2-Fluorophenol (surr),S

Phenol-d5 (surr),S

W1000921.D W042210X-8270.M Tue May 04 13:52:47 2010 Page 3

EA# 0310-130 Page 92 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000713.D Vial: 24

 Acq On : 23 Apr 2010 9:10 pm Operator: dda/glr

 Sample : 0310-130 U1 R3 COND Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 14:36 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 22 16:55:57 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

4200000

4400000

Time-->

Abundance TIC: W1000713.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000713.D W042210X-8270.M Mon May 03 21:56:29 2010 Page 3

EA# 0310-130 Page 93 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000700.D Vial: 11

 Acq On : 23 Apr 2010 3:20 pm Operator: dda/glr

 Sample : 0310-130 FB FH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 10:56 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

Time-->

Abundance TIC: W1000700.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000700.D W042610X-SIM-PAH.M Wed Apr 28 17:40:54 2010 Page 3

EA# 0310-130 Page 94 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000701.D Vial: 12

 Acq On : 23 Apr 2010 3:47 pm Operator: dda/glr

 Sample : 0310-130 FB BH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 11:13 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

Time-->

Abundance TIC: W1000701.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Terphenyl-d14 (surr),S Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Fluorobiphenyl (surr),S

Naphthalene-d8 (I),I

Nitrobenzene-d5 (surr),S

1,4-Dichlorobenzene-d4 (I),I

2-Fluorophenol (surr),S

Phenol-d5 (surr),S

W1000701.D W042610X-SIM-PAH.M Wed Apr 28 17:41:04 2010 Page 3

EA# 0310-130 Page 95 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000702.D Vial: 13

 Acq On : 23 Apr 2010 4:14 pm Operator: dda/glr

 Sample : 0310-130 FB COND Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 12:00 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

Time-->

Abundance TIC: W1000702.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000702.D W042610X-SIM-PAH.M Wed Apr 28 17:41:14 2010 Page 3

EA# 0310-130 Page 96 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000697.D Vial: 8

 Acq On : 23 Apr 2010 1:59 pm Operator: dda/glr

 Sample : 0310-130 RB FILTER Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 23 17:15 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

Time-->

Abundance TIC: W1000697.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Di-n-butylphthalate

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000697.D W042610X-SIM-PAH.M Wed Apr 28 17:40:02 2010 Page 3

EA# 0310-130 Page 97 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050310A\W1000904.D Vial: 13

 Acq On : 3 May 2010 9:32 pm Operator: dda\glr

 Sample : 0310-130 RB FILTER RR Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: May 4 10:18 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 22 16:55:57 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

4200000

Time-->

Abundance TIC: W1000904.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Di-n-butylphthalate

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000904.D W042210X-8270.M Tue May 04 20:45:29 2010 Page 3

EA# 0310-130 Page 98 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000698.D Vial: 9

 Acq On : 23 Apr 2010 2:26 pm Operator: dda/glr

 Sample : 0310-130 RB RINSE Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 8:26 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

500000

1000000

1500000

2000000

2500000

3000000

3500000

4000000

4500000

5000000

5500000

6000000

6500000

7000000

7500000

8000000

8500000

9000000

9500000

 1e+07

1.05e+07

 1.1e+07

1.15e+07

 1.2e+07

Time-->

Abundance TIC: W1000698.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000698.D W042610X-SIM-PAH.M Wed Apr 28 17:40:11 2010 Page 3

EA# 0310-130 Page 99 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000699.D Vial: 10

 Acq On : 23 Apr 2010 2:53 pm Operator: dda/glr

 Sample : 0310-130 RB XAD Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 8:33 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

Time-->

Abundance TIC: W1000699.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Terphenyl-d14 (surr),S Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Fluorobiphenyl (surr),S

Naphthalene-d8 (I),I

Nitrobenzene-d5 (surr),S

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000699.D W042610X-SIM-PAH.M Wed Apr 28 17:40:20 2010 Page 3

EA# 0310-130 Page 100 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000695.D Vial: 6

 Acq On : 23 Apr 2010 1:05 pm Operator: dda/glr

 Sample : 0310-130 MB FH/BH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 23 17:10 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

Time-->

Abundance TIC: W1000695.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Terphenyl-d14 (surr),S Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Fluorobiphenyl (surr),S

Naphthalene-d8 (I),I

Nitrobenzene-d5 (surr),S

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000695.D W042610X-SIM-PAH.M Wed Apr 28 17:39:45 2010 Page 3

EA# 0310-130 Page 101 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000696.D Vial: 7

 Acq On : 23 Apr 2010 1:32 pm Operator: dda/glr

 Sample : 0310-130 MB COND Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 23 17:13 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

Time-->

Abundance TIC: W1000696.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

2,4,6-Tribromophenol (surr),S

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

Phenol-d5 (surr),S

2-Fluorophenol (surr),S

W1000696.D W042610X-SIM-PAH.M Wed Apr 28 17:39:53 2010 Page 3

EA# 0310-130 Page 102 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000694.D Vial: 5

 Acq On : 23 Apr 2010 12:38 pm Operator: dda/glr

 Sample : ch2cl2 system blank Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 23 17:08 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

Time-->

Abundance TIC: W1000694.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Acenaphthene-d10 (I),IPhenanthrene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000694.D W042610X-SIM-PAH.M Wed Apr 28 17:39:36 2010 Page 3

EA# 0310-130 Page 103 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050310A\W1000900.D Vial: 9

 Acq On : 3 May 2010 7:44 pm Operator: dda\glr

 Sample : ch3cl2 system blank Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: May 4 9:36 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 22 16:55:57 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

Time-->

Abundance TIC: W1000900.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Acenaphthene-d10 (I),IPhenanthrene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000900.D W042210X-8270.M Tue May 04 20:36:20 2010 Page 3

EA# 0310-130 Page 104 of 129
 Quantitation Report (Not Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000692.D Vial: 3

 Acq On : 23 Apr 2010 11:44 am Operator: dda/glr

 Sample : 0310-130 LCS FH/BH Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 26 8:35 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

4200000

4400000

Time-->

Abundance TIC: W1000692.D

Benzo(g,h,i)perylene

Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene

Perylene Perylene-d12 (I),I Benzo(a)pyrene (CCC) Benzo(e)pyrene

Benzo(k)fluoranthene Benzo(b)fluoranthene

Di-n-octylphthalate (CCC)

Chrysene Chrysene-d12 (I),I Benzo(a)anthracene 3,3'-Dichlorobenzidine bis(2-Ethylhexyl)phthalate

3,3-Dimethylbenzidine bis(2-ethylhexyl)adipate Butylbenzylphthalate

Terphenyl-d14 (surr),S Pyrene Pyrene-d10 (surr),S

Benzidine Fluoranthene (CCC)

Di-n-butylphthalate

Carbazole

Anthracene Phenanthrene Phenanthrene-d10 (I),I

Pentachlorophenol (CCC)

Hexachlorobenzene 4-Bromophenyl-phenylether

2,4,6-Tribromophenol (surr),S Azobenzene N-Nitrosodiphenylamine (CCC) 4,6-Dinitro2-methylphenol Fluorene 4-Nitroaniline Fluorene-d10 (surr),S 4-Chlorophenyl-phenylether Diethlyphthalate 2,3,4,6-Tetrachlorophenol 2,3,5,6-Tetrachlorophenol Dibenzofuran 2,4-Dinitrotoluene Acenaphthene (CCC) 4-Nitrophenol (SPCC) 2,4-Dinitrophenol (SPCC) Acenaphthene-d10 (I),I 3-Nitroaniline Acenaphthylene 1,2-Dinitrobenzene2,6-Dinitrotoluene 1,3-Dinitrobenzene Dimethylphthalate 1,4-Dinitrobenzene 2-Nitroaniline 2-Chloronaphthalene 2-Fluorobiphenyl (surr),S 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (CCC) Hexachlorocyclopentadiene (SPCC) 1-Methylnaphthalene 2-Methylnaphthalene

4-Chloro-3 methylphenol (CCC)

Hexachlorobutadiene (CCC) 4-Chloroaniline Naphthalene Naphthalene-d8 (I),I 1,2,4-Trichlorobenzene 2,4-Dichlorophenol (CCC) bis(2-Chloroethoxy)methane Benzoic acid 2-Nitrophenol (CCC) 2,4-Dimethylphenol Isophorone

Nitrobenzene Nitrobenzene-d5 (surr),S Hexachloroethane

N-Nitrso-di-n-propylamine (SPCC) 3/4-Methylphenol bis(2-Chloroisopropyl) ether 2-Methylphenol 1,2-Dichlorobenzene Benzyl alcohol 1,4-Dichlorobenzene (CCC) 1,4-Dichlorobenzene-d4 (I),I 1,3-Dichlorobenzene 2-Chlorophenol bis(2-Chloroethyl)ether AnilinePhenol (CCC) Phenol-d5 (surr),S

2-Fluorophenol (surr),S

Pyridine N-Nitrosodimethylamine

W1000692.D W042610X-SIM-PAH.M Wed Apr 28 17:39:13 2010 Page 3

EA# 0310-130 Page 105 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050310A\W1000896.D Vial: 5

 Acq On : 3 May 2010 5:55 pm Operator: dda\glr

 Sample : 0310-130 LCS FH/BH RR Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: May 4 9:06 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 22 16:55:57 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

3800000

4000000

Time-->

Abundance TIC: W1000896.D

Benzo(g,h,i)perylene

Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene

Perylene Perylene-d12 (I),I

Benzo(e)pyrene Benzo(a)pyrene (CCC)

Benzo(k)fluoranthene Benzo(b)fluoranthene

Di-n-octylphthalate (CCC)

Chrysene Chrysene-d12 (I),I Benzo(a)anthracene 3,3'-Dichlorobenzidine bis(2-Ethylhexyl)phthalate

3,3-Dimethylbenzidine bis(2-ethylhexyl)adipate Butylbenzylphthalate

Terphenyl-d14 (surr),S Pyrene Pyrene-d10 (surr),S

Benzidine Fluoranthene (CCC)

Di-n-butylphthalate

Carbazole

Anthracene Phenanthrene Phenanthrene-d10 (I),I

Pentachlorophenol (CCC)

Hexachlorobenzene 4-Bromophenyl-phenylether

2,4,6-Tribromophenol (surr),S Azobenzene N-Nitrosodiphenylamine (CCC) 4,6-Dinitro2-methylphenol Fluorene 4-Nitroaniline 4-Chlorophenyl-phenylether Fluorene-d10 (surr),S Diethlyphthalate 2,3,4,6-Tetrachlorophenol 2,3,5,6-Tetrachlorophenol Dibenzofuran 2,4-Dinitrotoluene Acenaphthene (CCC) 4-Nitrophenol (SPCC) 2,4-Dinitrophenol (SPCC) Acenaphthene-d10 (I),I 3-Nitroaniline Acenaphthylene 1,2-Dinitrobenzene 2,6-Dinitrotoluene 1,3-Dinitrobenzene Dimethylphthalate 1,4-Dinitrobenzene 2-Nitroaniline 2-Chloronaphthalene 2-Fluorobiphenyl (surr),S 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (CCC) Hexachlorocyclopentadiene (SPCC)1-Methylnaphthalene 2-Methylnaphthalene

4-Chloro-3 methylphenol (CCC)

Hexachlorobutadiene (CCC) 4-Chloroaniline Naphthalene Naphthalene-d8 (I),I 1,2,4-Trichlorobenzene 2,4-Dichlorophenol (CCC) bis(2-Chloroethoxy)methane Benzoic acid 2-Nitrophenol (CCC) 2,4-Dimethylphenol Isophorone

Nitrobenzene Nitrobenzene-d5 (surr),S Hexachloroethane

N-Nitrso-di-n-propylamine (SPCC) 3/4-Methylphenol bis(2-Chloroisopropyl) ether1,2-Dichlorobenzene 2-Methylphenol Benzyl alcohol 1,4-Dichlorobenzene (CCC) 1,4-Dichlorobenzene-d4 (I),I 1,3-Dichlorobenzene 2-Chlorophenol bis(2-Chloroethyl)ether AnilinePhenol (CCC) Phenol-d5 (surr),S

2-Fluorophenol (surr),S

Pyridine N-Nitrosodimethylamine

W1000896.D W042210X-8270.M Tue May 04 20:44:40 2010 Page 3

EA# 0310-130 Page 106 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000693.D Vial: 4

 Acq On : 23 Apr 2010 12:11 pm Operator: dda/glr

 Sample : 0310-130 LCS COND Inst : Wiley

 Misc : Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 23 17:06 2010 Quant Results File: W042210X-8270.RES

 Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Mon Apr 26 15:48:30 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

200000

400000

600000

800000

1000000

1200000

1400000

1600000

1800000

2000000

2200000

2400000

2600000

2800000

3000000

3200000

3400000

3600000

Time-->

Abundance TIC: W1000693.D

Benzo(g,h,i)perylene

Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene

Perylene Perylene-d12 (I),I Benzo(a)pyrene (CCC) Benzo(e)pyrene

Benzo(k)fluoranthene Benzo(b)fluoranthene

Di-n-octylphthalate (CCC)

Chrysene Chrysene-d12 (I),I Benzo(a)anthracene 3,3'-Dichlorobenzidine bis(2-Ethylhexyl)phthalate

3,3-Dimethylbenzidine bis(2-ethylhexyl)adipate Butylbenzylphthalate

Pyrene Pyrene-d10 (surr),S

Benzidine Fluoranthene (CCC)

Di-n-butylphthalate

Carbazole Anthracene Phenanthrene Phenanthrene-d10 (I),I

Pentachlorophenol (CCC)

Hexachlorobenzene 4-Bromophenyl-phenylether

2,4,6-Tribromophenol (surr),S Azobenzene N-Nitrosodiphenylamine (CCC) 4,6-Dinitro2-methylphenol Fluorene 4-Nitroaniline

Diethlyphthalate Fluorene-d10 (surr),S 4-Chlorophenyl-phenylether 2,3,5,6-Tetrachlorophenol 2,3,4,6-Tetrachlorophenol Dibenzofuran 2,4-Dinitrotoluene Acenaphthene (CCC) 4-Nitrophenol (SPCC) 2,4-Dinitrophenol (SPCC) Acenaphthene-d10 (I),I 3-Nitroaniline Acenaphthylene 1,2-Dinitrobenzene2,6-Dinitrotoluene 1,3-Dinitrobenzene Dimethylphthalate 1,4-Dinitrobenzene 2-Nitroaniline 2-Chloronaphthalene

2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (CCC) Hexachlorocyclopentadiene (SPCC) 1-Methylnaphthalene 2-Methylnaphthalene

4-Chloro-3 methylphenol (CCC)

Hexachlorobutadiene (CCC) 4-Chloroaniline Naphthalene Naphthalene-d8 (I),I

2,4-Dichlorophenol (CCC) 1,2,4-Trichlorobenzene bis(2-Chloroethoxy)methane 2-Nitrophenol (CCC) 2,4-Dimethylphenol Benzoic acid Isophorone

Nitrobenzene Nitrobenzene-d5 (surr),S Hexachloroethane

N-Nitrso-di-n-propylamine (SPCC) 3/4-Methylphenol bis(2-Chloroisopropyl) ether 1,2-Dichlorobenzene 2-Methylphenol Benzyl alcohol 1,4-Dichlorobenzene (CCC) 1,4-Dichlorobenzene-d4 (I),I 1,3-Dichlorobenzene 2-Chlorophenol bis(2-Chloroethyl)ether Aniline Phenol (CCC) Phenol-d5 (surr),S

2-Fluorophenol (surr),S

Pyridine N-Nitrosodimethylamine

W1000693.D W042610X-SIM-PAH.M Wed Apr 28 17:39:27 2010 Page 3

EA# 0310-130 Page 107 of 129
Sample 

Chromatograms

 (SIM)

EA# 0310-130 Page 108 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000847.D Vial: 31

 Acq On : 30 Apr 2010 7:19 am Operator: dda\glr

 Sample : 0310-130 U1 R1 FH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:38 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

38000

Time-->

Abundance TIC: W1000847.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000847.D W042910X-SIM-PAH.M Tue May 04 11:40:42 2010 Page 2

EA# 0310-130 Page 109 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000848.D Vial: 32

 Acq On : 30 Apr 2010 7:46 am Operator: dda\glr

 Sample : 0310-130 U1 R1 BH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:41 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

10000

20000

30000

40000

50000

60000

70000

80000

90000

100000

110000

120000

130000

140000

150000

160000

170000

180000

190000

200000

210000

Time-->

Abundance TIC: W1000848.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene Phenanthrene-d10 (I),I

Fluorene Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Methylnaphthalene

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000848.D W042910X-SIM-PAH.M Tue May 04 11:40:51 2010 Page 2

EA# 0310-130 Page 110 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000849.D Vial: 33

 Acq On : 30 Apr 2010 8:13 am Operator: dda\glr

 Sample : 0310-130 U1 R1 COND Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:41 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

16000

17000

18000

19000

20000

21000

22000

23000

24000

25000

26000

27000

28000

29000

Time-->

Abundance TIC: W1000849.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000849.D W042910X-SIM-PAH.M Tue May 04 11:41:03 2010 Page 2

EA# 0310-130 Page 111 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000850.D Vial: 34

 Acq On : 30 Apr 2010 8:40 am Operator: dda\glr

 Sample : 0310-130 U1 R2 FH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 10:58 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

38000

Time-->

Abundance TIC: W1000850.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene Phenanthrene-d10 (I),I

Fluorene Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Methylnaphthalene

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000850.D W042910X-SIM-PAH.M Tue May 04 11:41:11 2010 Page 2

EA# 0310-130 Page 112 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000852.D Vial: 35

 Acq On : 30 Apr 2010 9:34 am Operator: dda\glr

 Sample : 0310-130 U1 R2 BH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 11:00 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

10000

20000

30000

40000

50000

60000

70000

80000

90000

100000

110000

120000

130000

140000

150000

160000

170000

180000

190000

200000

Time-->

Abundance TIC: W1000852.D

Perylene-d12 (I),I

Benzo(b)fluoranthene

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Methylnaphthalene

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000852.D W042910X-SIM-PAH.M Tue May 04 11:41:31 2010 Page 2

EA# 0310-130 Page 113 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000853.D Vial: 36

 Acq On : 30 Apr 2010 10:03 am Operator: dda\glr

 Sample : 0310-130 U1 R2 COND Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 11:01 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

Time-->

Abundance TIC: W1000853.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000853.D W042910X-SIM-PAH.M Tue May 04 11:41:44 2010 Page 2

EA# 0310-130 Page 114 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000854.D Vial: 37

 Acq On : 30 Apr 2010 10:30 am Operator: dda\glr

 Sample : 0310-130 U1 R3 FH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 11:05 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

38000

40000

Time-->

Abundance TIC: W1000854.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene Phenanthrene-d10 (I),I

Fluorene Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Methylnaphthalene

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000854.D W042910X-SIM-PAH.M Tue May 04 11:41:54 2010 Page 2

EA# 0310-130 Page 115 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000855.D Vial: 38

 Acq On : 30 Apr 2010 10:57 am Operator: dda\glr

 Sample : 0310-130 U1 R3 FH LD Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 11:53 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

38000

Time-->

Abundance TIC: W1000855.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene Phenanthrene-d10 (I),I

Fluorene Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I Acenaphthylene

Naphthalene

2-Methylnaphthalene

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000855.D W042910X-SIM-PAH.M Tue May 04 11:42:05 2010 Page 2

EA# 0310-130 Page 116 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000859.D Vial: 42

 Acq On : 30 Apr 2010 12:45 pm Operator: dda\glr

 Sample : 0310-130 U1 R3 BH 2X Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 13:15 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

5000

10000

15000

20000

25000

30000

35000

40000

45000

50000

55000

60000

65000

70000

75000

80000

85000

90000

95000

100000

105000

Time-->

Abundance TIC: W1000859.D

Perylene-d12 (I),I

Benzo(b)fluoranthene

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

2-Methylnaphthalene

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000859.D W042910X-SIM-PAH.M Tue May 04 11:42:58 2010 Page 2

EA# 0310-130 Page 117 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000857.D Vial: 40

 Acq On : 30 Apr 2010 11:51 am Operator: dda\glr

 Sample : 0310-130 U1 R3 COND Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 12:31 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

Time-->

Abundance TIC: W1000857.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000857.D W042910X-SIM-PAH.M Tue May 04 11:42:38 2010 Page 2

EA# 0310-130 Page 118 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000844.D Vial: 27

 Acq On : 30 Apr 2010 5:58 am Operator: dda\glr

 Sample : 0310-130 FB FH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:34 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

16000

17000

18000

19000

20000

21000

22000

23000

24000

25000

26000

27000

28000

29000

30000

Time-->

Abundance TIC: W1000844.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000844.D W042910X-SIM-PAH.M Tue May 04 11:40:16 2010 Page 2

EA# 0310-130 Page 119 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000845.D Vial: 29

 Acq On : 30 Apr 2010 6:25 am Operator: dda\glr

 Sample : 0310-130 FB BH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:35 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

10000

20000

30000

40000

50000

60000

70000

80000

90000

100000

110000

120000

130000

140000

150000

160000

170000

180000

190000

200000

210000

Time-->

Abundance TIC: W1000845.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000845.D W042910X-SIM-PAH.M Tue May 04 11:40:26 2010 Page 2

EA# 0310-130 Page 120 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000846.D Vial: 30

 Acq On : 30 Apr 2010 6:52 am Operator: dda\glr

 Sample : 0310-130 FB COND Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:37 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

16000

17000

18000

19000

20000

21000

22000

23000

24000

25000

26000

27000

28000

Time-->

Abundance TIC: W1000846.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000846.D W042910X-SIM-PAH.M Tue May 04 11:40:34 2010 Page 2

EA# 0310-130 Page 121 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000841.D Vial: 24

 Acq On : 30 Apr 2010 4:37 am Operator: dda\glr

 Sample : 0310-130 RB FILTER Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:30 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

38000

40000

Time-->

Abundance TIC: W1000841.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000841.D W042910X-SIM-PAH.M Tue May 04 11:39:48 2010 Page 2

EA# 0310-130 Page 122 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000843.D Vial: 26

 Acq On : 30 Apr 2010 5:31 am Operator: dda\glr

 Sample : 0310-130 RB XAD Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:32 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

10000

20000

30000

40000

50000

60000

70000

80000

90000

100000

110000

120000

130000

140000

150000

160000

170000

180000

190000

200000

210000

Time-->

Abundance TIC: W1000843.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000843.D W042910X-SIM-PAH.M Tue May 04 11:40:07 2010 Page 2

EA# 0310-130 Page 123 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000842.D Vial: 25

 Acq On : 30 Apr 2010 5:04 am Operator: dda\glr

 Sample : 0310-130 RB RINSE Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 6:56 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

2000

4000

6000

8000

10000

12000

14000

16000

18000

20000

22000

24000

26000

28000

30000

32000

34000

36000

Time-->

Abundance TIC: W1000842.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000842.D W042910X-SIM-PAH.M Tue May 04 11:39:56 2010 Page 2

EA# 0310-130 Page 124 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000835.D Vial: 22

 Acq On : 30 Apr 2010 1:55 am Operator: dda\glr

 Sample : 0310-130 MB FH/BH Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 9:22 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

10000

20000

30000

40000

50000

60000

70000

80000

90000

100000

110000

120000

130000

140000

150000

160000

170000

180000

190000

200000

210000

220000

230000

240000

Time-->

Abundance TIC: W1000835.D

Perylene-d12 (I),I

Benzo(e)pyrene Benzo(a)pyrene (CCC)

Chrysene Chrysene-d12 (I),I Benzo(a)anthracene

Pyrene-d10 (surr),S

Fluoranthene (CCC)

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000835.D W042910X-SIM-PAH.M Fri Apr 30 13:22:47 2010 Page 2

EA# 0310-130 Page 125 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000836.D Vial: 23

 Acq On : 30 Apr 2010 2:21 am Operator: dda\glr

 Sample : 0310-130 MB COND Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 6:56 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

16000

17000

18000

19000

20000

21000

22000

23000

24000

25000

26000

27000

Time-->

Abundance TIC: W1000836.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Pyrene-d10 (surr),S

Phenanthrene-d10 (I),I

Fluorene-d10 (surr),S

Acenaphthene-d10 (I),I

Naphthalene-d8 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000836.D W042910X-SIM-PAH.M Fri Apr 30 13:22:53 2010 Page 2

EA# 0310-130 Page 126 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000816.D Vial: 3

 Acq On : 29 Apr 2010 5:22 pm Operator: dda\glr

 Sample : ch2cl2 system blank Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 6:59 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

11000

12000

13000

14000

15000

16000

17000

18000

19000

20000

21000

Time-->

Abundance TIC: W1000816.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Phenanthrene-d10 (I),I

Naphthalene-d8 (I),IAcenaphthene-d10 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000816.D W042910X-SIM-PAH.M Tue May 04 16:39:33 2010 Page 2

EA# 0310-130 Page 127 of 129
 Quantitation Report (QT Reviewed)

 Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000840.D Vial: 28

 Acq On : 30 Apr 2010 4:10 am Operator: dda\glr

 Sample : ch2cl2 system blank Inst : Wiley

 Misc : gcmsprep1pg186 Multiplr: 1.00

 MS Integration Params: rteint.p 

 Quant Time: Apr 30 6:56 2010 Quant Results File: W042910X-SIM-PAH.RES

 Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator)

 Title : 8270C - Full List

 Last Update : Thu Apr 29 15:08:49 2010

 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00

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Time-->

Abundance TIC: W1000840.D

Perylene-d12 (I),I

Chrysene-d12 (I),I

Phenanthrene-d10 (I),I

Naphthalene-d8 (I),IAcenaphthene-d10 (I),I

1,4-Dichlorobenzene-d4 (I),I

W1000840.D W042910X-SIM-PAH.M Tue May 04 11:39:39 2010 Page 2

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