RE: Conference call access information 

Gary Wood to: Christopher Lambesis 07/08/2010 01:34 PM 

Cc: 'Terri Zick" 

From: "Gary Wood" <woodgl@trimatrixlabs.com> 

To: Christopher Lambesis/R5/USEPA/US@EPA 

Cc: "Terri Zick" <tzick@cticompanies.com> 

Please respond to <woodgl@trimatrixlabs .com> 

History: This message has been forwarded. 

Hello Chris, 

Jeff and I will be speaking with you shortly but I wanted to get the statements of data qualifications to you 

now related to the IS and surrogate items at issue. It is a single page that would replace the like page in 

our initial submission to you. 

Gary Wood 

Senior Project Chemist 

Corporate / Laboratory Main: 616.975.4500 

5560 Corporate Exchange Court SE Direct: 616.940.4206 

Grand Rapids, Michigan 49512 Fax: 616.942.7463 

woodgl@trimatrixlabs.com www.trimatrixlabs.com 

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From: Lambesis.Christopher@epamail.epa.gov [mailto:Lambesis.Christopher@epamail.epa.gov] 

Sent: Thursday, July 08, 2010 12:15 PM 

To: Terri Zick 

Cc: woodgl@trimatrixlabs.com; glaserj@trimatrixlabs.com; Kathy Wilson; Ramaly.Todd@epamail.epa.gov 

Subject: Re: Conference call access information 

Terri, 

Please feel free to have the lab email any documents we will need before the meeting. 

-Chris 

Terri Zick <tzick@cticompanies.com > wrote: 

To: Christopher Lambesis/R5/USEPA/US@EPA 

From: Terri Zick <tzick@cticompanies.com> 

Date: 07/08/2010 08:22AM 

Cc: "woodgl@trimatrixlabs.com " <woodgl@trimatrixlabs.com >, "glaserj@trimatrixlabs.com " 
<glaserj@trimatrixlabs.com >, Kathy Wilson <kathywilson@owossographic.com >, Todd 

Ramaly/R5/USEPA/US@EPA 

Subject: Conference call access information 

The conference call will be conducted at 3pm eastern time (2 pm Central Time). Please use the 

following dial-in information to access the call: 

(866) 213-1863 

Access Code: 5044901 

We look forward to resolving the remaining issues at that time. Please contact me if your schedule 

changes prior to the scheduled call. 

Thank you 

Terri Zick 

313-300-7401 cell 

tzick@cticompanies.com 

CTI and Associates, Inc. 

51331 W. Pontiac Trail, Wixom, Ml 48393 

248.486.5100 Phone / 248.486.5050 Fax 

From: Lambesis.Christopher@epamail.epa.gov [mailto:Lambesis.Christopher@epamail.epa.gov] 

Sent: Thursday, July 08, 2010 10:13 AM 

To: Terri Zick 

Cc: woodgl@trimatrixlabs.com ; Kathy Wilson; glaserj@trimatrixlabs.com ; Ramaly.Todd@epamail.epa.gov 

Subject: RE: Availability for conference call 

Terri, 

We can take a 2pm central time conference call. It is unfortunate that Jody can't make the 

call since she has been most helpful. However, if all the information is available for the 

meeting today we should be able to get through this. 

-Chris 

Terri Zick <tzick@cticompanies.com > wrote: 

To: Christopher Lambesis/R5/USEPA/US@EPA 

From: Terri Zick <tzick@cticompanies.com > 

Date: 07/08/2010 08:O1AM 

Cc: "woodgl@trimatrixlabs.com" <woodgl@trimatrixlabs.com >, Kathy Wilson 

<kathywilson@owossographic.com >, "glaserj@trimatrixlabs.com " 

<glaserj@trimatrixlabs.com >, Todd Ramaly/R5/USEPA/US@EPA 

Subject: RE: Availability for conference call 

Chris- 
Gary Wood and Jeff Glaser from Trimatrix will be available at 3pm eastern time 

(2 pm Central time). Jodie is unfortunately not available today, however, she 

is providing Jeff with the information necessary for our discussion. 

Does this alternate time work for you and Todd? 

Terri Zick 

313-300-7401 cell 

tzick@cticompanies.com 

CTI and Associates, Inc. 

51331 W. Pontiac Trail, Wixom, MI 48393 

248.486.5100 Phone 248.486.5050 Fax 

Original Message 

From: Lambesis.Christopher@epamail.epa.gov[ 

mailto:Lambesis.Christopher@epamail.epa.gov] 

Sent: Wednesday, July 07, 2010 4:55 PM 

To: Terri Zick 

Cc: Kathy Wilson; Ramaly.Todd@epamail.epa.gov 

Subject: Re: Availability for conference call 

Hi Terri, 

We're available for a call tomorrow (Thursday) at 10am central time. It 

will be beneficial if you can include the Semi-volatile Analyst/Manager 

Jody Blouw, and the Extraction Analyst or Manager. They should have the 

project data, bench notes and calculation sheets. Please let us know 

what number to call. Thanks. 

-Chris 

Christopher Lambesis 

Environmental Scientist 

U.S EPA Region 5 

Land and Chemicals Division 

(312) 886-3583 

From: Terri Zick <tzick@cticompanies.com> 

To: Christopher Lambesis/R5/USEPA/US@EPA 

Cc: Kathy Wilson <kathywilson@owossographic.com> 

Date: 07/07/2010 02:59 PM 

Subject: Availability for conference call 
ChrisI am attempting to set up a conference call with Trimatrix to resolve 

the issues we discussed yesterday afternoon. Please let me know what 

your schedule allows (preferably tomorrow 7/8/10). 

Thank you 

Terri Zick 

313-300-7401 cell 

tzick@cticompanies.com 

CTI and Associates, Inc. 

51331 W. Pontiac Trail, Wixom, MI 48393 

248.486.5100 Phone 248.486.5050 Fax 

The information contained in this electronic message is privileged 

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The information contained in this electronic message is privileged and/or 

confidential information intended only for the use of the individual or entity 

named above. If the reader of this message is not the intended recipient, or 

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are hereby notified that any dissemination, distribution or copying of the 

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communication in error, please immediately notify us by return e-mail or by 

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The information contained in this electronic message is privileged and/or confidential information intended only for the use of the 

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SDG CASE NARRATIVE 

Attachment 2 

Statement of Data Qualifications 

Tentatively Identified Compound Scan - EPA Method 8270C 

Qualification: One or more of the internal standards for this sample had recoveries outside of the method 

acceptance windows. However, the internal standard associated with the target analyte has 

acceptable recovery. No qualification is needed. 

Analysis: USEPA-8270C 

Sample/Analyte: 1003151-03 OGA Composite 1 

1003151-04 OGA Composite 2 

1003151-05 OGA Composite 3 

1003151-06 OGA Composite 4 

Qualification: This sample was used for peak identification only. No quantitative result was obtained. Sample 

was prepared by dilution into methylene chloride then directly injected. 

Analysis: USEPA-8270C 

Sample/Analyte: 1003151-01 Raw Product - NMP 

Qualification: This sample had recoveries of the acid surrogates that were out of control due to sample matrix 

interference. The base/neutral surrogate OTP was also out of control due to matrix interference. 

Result should be considered as estimated. 

Analysis: USEPA-8270C 

Sample/Analyte: 1003151-05 OGA Composite 3 

Qualification: This sample had recoveries of the acid surrogates that were out of control due to sample matrix 

interference. The target analyte was not an acidic compound, therefore, no qualification is 

necessary. 

Analysis: USEPA-8270C 

Sample/Analyte: 1003151-03 OGA Composite 1 

1003151-04 OGA Composite 2 

1003151-06 OGA Composite 4