P.L 

OAR Box 1490 

Prepped hy Charmelle Mathews 

Document Number: 

24) IV-B-26 

Docket Number: 

A-94-52 

Printed 8/4/2008 11:51:46 AM Sheet 24 of 273 
P.2 

K/-B-K 

MEMORANDUM 

TO: Docket for the Reinforced Plastic Composites NESHAP 

FROM: Keith Barnett, U. S. Environmental Protection Agency 

DATE: January 14, 2003 

SUBJECT: Test Data to support the Composites Fabricators Association Vapor Suppressant 

Test Protocol. 

Attached is data provided by the Composites Manufacturers Association too support the accuracy 

ofthe test method to determine the effectiveness of vapor suppressants. This method is included 

in the Reinforced Plastic Composites NESHAP as Appendix A to 40 CFR part 63 subpart 

WWWW. Note that the page numbers on the attachment begin with 22. 
P.3 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 22 of 41 

VSE Test Data 

Ashland Chemical 

Eastman Chemical 

Reichhold Chemical 

2_ 
P.4 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision7.4-July, 2002 

Page 23 of 41 

Ashland Test Data Summary 

Test Pair No. 

1 

2 

3 

4 

5 

6 

Avg. Wt Loss 

% VS Weight Loss 

5.86 

5.63 

5.9 

5.58 

5.42 

5.99 

5.73 

% NVS Weight Loss 

1.59 

1.55 

1.64 

1.61 

1.63 

1.61 

1.61 

1-(% Avg Wt LossNvs / % Avg Wt LossVS) = 

VSE Factor 0.720 

Eastman Test Data Summary 

Test Pair No. 

1 

2 

3 

4 

5 

6 

Avg. Wt. Loss 

% VS Weight Loss 

4.53 

4.83 

4.44 

4.5 

5.1 

4.71 

4.69 

% NVS Weight Loss 

2.26 

1.84 

1.68 

1.58 

1.69 

1.99 

1.84 

1-(% Avg Wt LossNvs / % Avg Wt LossVS) -

VSE Factor 0.607 

Reichhold Test Data Summary 

Test Pair No. 

1 

2 

3 

4 

5 

6 

Avg. Wt. Loss 

% VS Weight Loss 

4.33 

4.32 

4.18 

4.16 

4.34 

4.13 

4.24 

% NVS Weight Loss 

1.13 

1.16 

1.13 

1.18 

1.09 

1.19 

1.15 

1-(% Avg Wt LossNvs / % Avg Wt Lossvs) = 

VSE Factor 0.730 

3 23 
P.5 

'* 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 24 of 41 

Test Pair No. 1 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

82.40 

81.68 

81.32 

80.75 

80.63 

80.28 

79.93 

79.58 

79.08 

78.64 

78.25 

78.06 

77.87 

77.70 

77.67 

77.63 

77.60 

77.59 

77.59 

77.58 

77.58 

77.57 

77.57 

77.58 

77.57 

4.83 

5.86 

37.00 

82.4 

69.0 

31.0 

0.0 

73.7 

60.7 

1.25 

22.9 

Roll-Out 

Time 

(mm:ss) 

02:10 

• 

Final 

Time 

115 min 

Ashland Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

82.38 

81.83 

81.48 

81.37 

81.32 

81.31 

81.28 

81.25 

81.22 

81.20 

81.18 

81.17 

81.16 

81.12 

81.12 

81.11 

81.10 

81.09 

81.08 

81.08 

81.07 

81.07 

81.07 

81.07 

1.31 

1.59 

36.96 

82.38 

69.0 

31.0 

0.0 

73.7 

60.7 

1.25 

24.5 

Roll-Out 

Time 

(mm:ss) 

02:10 

**•'•• . . ' •) , 

Final 

Time 

110 min 

^f 

24 
P.6 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 25 of 41 

Test Pair No. 2 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

83.37 

78.69 

78.68 

78.68 

78.68 

78.68 

4.69 

5.63 

37.33 

83.37 

69.1 

30.9 

0.0 

73.6 

59.9 

1.25 

22.9 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

80 min 

Ashland Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

83.71 

82.45 

82.43 

82.43 

82.42 

82.41 

82.42 

82.41 

1.30 

1.55 

37.28 

83.71 

69.2 

30.8 

0.0 

73.6 

59.9 

1.25 

24.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

85 min 

25 
P.7 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4-July, 2002 

Page 26 of 41 

Test Pair No. 3 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wl. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

86.11 

81.05 

81.05 

81.04 

80.03 

81.04 

81.03 

5.08 

5.90 

38.61 

86.11 

69.1 

30.9 

0.0 

73.6 

61.2 

1.25 

22.9 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

80 min 

Ashland Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wl. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

86.21 

84.86 

84.83 

84.83 

84.80 

84.80 

84.80 

84.80 

1.41 

1.64 

38.72 

86.21 

69.0 

31.0 

0.0 

73.6 

61.2 

1.25 

24.5 

Roll-Out 

Time 

(mm:ss) 

02:10 

Final 

Time 

90 min 

(p 

2« 
P.8 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4-July, 2002 

Page 27 of 41 

Test Pair No. 4 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post Rollout Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

85.06 

80.45 

80.39 

80.37 

80.35 

80.33 

80.32 

80.31 

80.31 

80.32 

80.31 

4.75 

5.58 

38.26 

85.06 

69.0 

31.0 

0.0 

73.9 

61.3 

1.25 

22.9 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

100 min 

Ashland Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature

 UF 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

85.06 

84.58 

84.56 

84.55 

84.55 

84.53 

84.53 

84.54 

84.53 

1.38 

1.61 

38.25 

85.91 

69.2 

30.8 

0.0 

73.9 

61.3 

1.25 

24.5 

Roll-Out 

Time 

(mm:ss) 

02:10 

Final 

Time 

• 90 min 

7 27 
P.9 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 28 of 41 

Test Pair No. 5 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

90.03 

85.20 

85.20 

85.18 

85.17 

85.17 

85.15 

85.15 

85.16 

85.15 

4.88 

5.42 

40.21 

90.03 

69.1 

30.9 

0.0 

73.7 

58.5 

1.25 

22.5 

Roll-Out 

Time 

(mm:ss) 

02:10 

Final 

Time 

95 min 

Ashland Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

89.56 

88.18 

88.12 

88.12 

88.10 

88.10 

88.10 

88.10 

1.46 

1.63 

39.90 

89.56 

69.2 

30.8 

0.0 

73.7 

58.5 

1.25 

24.9 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

90 min 

r 

28 
P.10 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 29 of 41 

Test Pair No. 6 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

81.01 

76.25 

76.25 

76.23 

76.22 

76.22 

76.23 

76.22 

4.79 

5.99 

36.43 

81.01 

69.0 

31.0 

0.0 

73.9 

58.3 

1.25 

22.9 

Roll-Out 

Time 

(mm:ss) 

02:00 

*' *":-'-.:•.. S'SFinal 

Time 

85 min 

Ashland Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

81.12 

79.84 

79.82 

79.82 

79.81 

79.82 

79.81 

1.31 

1.61 

36.48 

81.12 

69.0 

31.0 

0.0 

73.9 

58.3 

1.25 

24.5 

Roll-Out 

Time 

(mm:ss) 

02:10 

Final 

Time 

- 80 min 

°l 29 
P.11 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4-July, 2002 

Page 30 of 41 

Test Pair No. 1 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

135 

140 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

80.33 

80.02 

80.01 

79.91 

79.80 

79.60 

79.42 

79.15 

78.92 

78.67 

78.45 

78.28 

78.08 

77.65 

77.30 

77.09 

76.96 

76.89 

76.84 

76.78 

76.75 

76.73 

76.69 

76.71 

76.69 

3.64 

4.53 

35.7 

80.33 

69.2 

30.8 

0.0 

70.0 

50.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

105 min 

Eastman Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature

 UF 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

135 

140 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

78.72 

78.42 

78.42 

78.28 

77.84 

77.79 

77.79 

77.77 

77.76 

77.72 

77.67 

77.61 

77.57 

77.54 

77.51 

77.47 

77.42 

77.33 

77.25 

77.21 

77.16 

77.11 

77.07 

77.05 

77.01 

76.98 

76.96 

76.95 

76.94 

76.96 

76.94 

1.78 

2.26 

34.82 

78.72 

69.3 

30.6 

0.0 

70.0 

50.0 

1.25 

19.7 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

135 min 

10 

30 
P.12 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 31 of 41 

Test Pair No. 2 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

73.65 

73.30 

70.26 

70.20 

70.16 

70.13 

70.12 

70.10 

70.09 

70.09 

70.10 

70.09 

3.56 

4.83 

31.96 

73.65 

96.7 

30.2 

0.0 , 

71.0 

50.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

Final 

Time 

100 min 

Eastman Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

72.92 

72.62 

71.80 

71.77 

71.75 

71.71 

71.68 

71.64 

71.62 

71.60 

71.59 

71.58 

71.58 

71.58 

71.58 

1.34 

1.84 

30.88 

72.92 

70.2 

29.7 

0.0 

71.0 

50.0 

1.25 

19.7 

Roll-Out 

Time 

(mm:ss) 

Final 

Time 

110 min 

ll 31 
P.13 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 32 of 41 

Test Pair No. 3 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

72.22 

71.95 

69.15 

69.08 

69.05 

69.05 

69.04 

69.03 

69.02 

69.00 

69.02 

69.00 

3.22 

4.44 

30.92 

72.22 

70.1 

29.9 

0.0 

70.0 

50.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

100 min 

Eastman Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

76.25 

75.99 

75.18 

75.13 

75.09 

75.06 

75.02 

75.00 

74.98 

74.97 

74.97 

74.97 

74.97 

1.28 

1.68 

32.93 

76.25 

69.8 

30.16 

0.0 

70.0 

50.0 

1.25 

19.7 

Roll-Out 

Time 

(mm:ss) 

02:00 

y\. •-..-' *. 

Final 

Time 

100 min 

\1 32 
P.14 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 33 of 41 

Test Pair No. 4 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

.10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissipns 

Lost 

% 

Emissions 

Weight 

(g) 

79.99 

79.61 

76.62 

76.53 

76.46 

76.40 

76.40 

76.39 

76.39 

76.39 

76.39 

3.60 

4.50 

34.25 

79.99 

70.02 

29.98 

0.0 

69.0 

50.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:15 

Final 

Time 

100 min 

Eastman Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

81.23 

80.99 

80.14 

80.12 

80.07 

80.03 

80.00 

79.96 

79.95 

79.94 

79.94 

79.94 

79.94 

1.29 

1.58 

35.04 

81.23 

69.86 

30.13 

0.0 

69.0 

50.0 

1.25 

19.7 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

- 100 min 

a 33 
P.15 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4-July, 2002 

Page 34 of 41 

Test Pair No. 5 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature

 UF 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

70.78 

70.49 

67.65 

67.45 

67.36 

67.31 

67.27 

67.25 

67.21 

67.18 

67.17 

67.18 

67.17 

3.61 

5.10 

30.13 

70.78 

70.14 

29.85 

0.0 

70.0 

50.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

105 min 

Eastman Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

InHial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

74.17 

73.74 

73.16 

73.14 

73.10 

73.05 

73.01 

72.97 

72.95 

72.95 

72.94 

72.94 

72.91 

72.92 

72.91 

1.26 

1.69 

31.81 

74.17 

69.98 

30.01 

0.0 

70.0 

50.0 

1.25 

19.7 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

115 min 

/ • / 

34 
P.16 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 35 of 41 

Test Pair No. 6 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

75.22 

74.85 

72.26 

72.04 

71.91 

71.81 

71.77 

71.73 

71.71 

71.69 

71.69 

71.68 

71.68 

71.67 

71.67 

71.67 

71.67 

3.55 

4.71 

32.50 

75.22 

69.82 

30.17 

0.0 

70.0 

50.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:15 

Final 

Time 

120 min 

Eastman Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

76.63 

76.26 

75.29 

75.22 

75.18 

75.15 

75.13 

75.12 

75.11 

75.10 

75.10 

75.10 

75.10 

1.53 

1.99 

32.63 

76.63 

70.13 

29.86 

0.0 

70.0 

50.0 

1.25 

19.7 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

100 min 

IS 35 
P.17 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 36 of 41 

Test Pair No. 1 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

198.09 

197.63 

196.91 

196.82 

195.60 

194.96 

194.20 

193.45 

192.61 

191.77 

191.02 

190.49 

190.15 

189.94 

189.79 

189.79 

189.64 

189.64 

189.57 

189.54 

189.50 

189.50 

189.50 

189.50 

8.59 

4.33 

85.44 

198.09 

69.8 

30.1 

0.0 

72.0 

44.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

95 min 

Reichhold Chemical Test Data 

Vapor Suppressed | 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

198.87 

198.36 

197.72 

197.39 

197.31 

197.28 

197.22 

197.19 

197.12 

197.05 

196.97 

196.91 

196.91 

196.86 

196.83 

196.83 

196.73 

196.73 

196.71 

196.71 

196.62 

196.65 

196.62 

2.25 

1.13 

83.49 

198.87 

70.4 

29.6 

0.0 

72.0 

44.0 

1.25 

21.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

95 min 

It* 36 
P.18 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 37 of 41 

Test Pair No. 2 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

196.38 

196.38 

188.04 

188.01 

187.98 

187.95 

187.93 

187.89 

187.89 

187.91 

187.89 

8.49 

4.32 

86.87 

196.38 

30.6 

69.3 

0.0 

72.0 

44.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

}.S\ ••'••;:;• : :y 

Final 

Time 

90 min 

Reichhold Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

I Emissions 

Weight 

(g) 

198.07 

197.59 

195.95 

195.92 

195.90 

195.88 

195.87 

195.83 

195.78 

195.79 

195.78 

2.29 

1.16 

81.18 

198.07 

71.0 

29.0 

0.0 

72.0 

44.0 

1.25 

21.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

''s', '* . "•'".- ' '. S *-*-''* . 

Final 

Time 

95 min 

I7 37 
P.19 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 38 of 41 

Test Pair No. 3 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature

 UF 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

197.57 

196.91 

189.61 

189.56 

189.51 

189.45 

189.40 

189.37 

189.30 

189.30 

189.30 

189.30 

8.27 

4.18 

80.51 

197.57 

71.1 

28.9 

0.0 

72.0 

44.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

95 min 

Reichhold Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

. 15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

197.27 

196.82 

195.31 

195.22 

195.14 

195.15 

195.16 

195.07 

195.04 

195.04 

195.04 

195.04 

2.23 

1.13 

81.54 

197.27 

70.8 

29.2 

0.0 

72.0 

44.0 

1.25 

21.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

95 min 

Ifr 38 
P.20 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 39 of 41 

Test Pair No. 4 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

196.72 

196.29 

188.88 

188.79 

188.71 

188.65 

188.60 

188.58 

188.52 

188.53 

188.52 

8.20 

4.16 

85.58 

196.72 

30.3 

69.7 

0.0 

72.0 

44.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

95 min 

Reichhold Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

198.16 

197.65 

195.94 

195.87 

195.81 

195.81 

195.82 

195.81 

2.35 

1.18 

82.30 

198.16 

70.7 

29.3 

0.0 

72.0 

43.0 

1.25 

21.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

, . *•-.. . 

Final 

Time 

75 min 

11 39 
P.21 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4 - July, 2002 

Page 40 of 41 

Test Pair No. 5 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

198.74 

198.23 

190.33 

190.28 

190.23 

190.20 

190.17 

190.11 

190.12 

190.11 

8.63 

4.34 

84.18 

198.74 

70.3 

29.7 

0.0 

72.0 

44.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

90 min 

Reichhold Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature

 UF 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

197.54 

197.04 

195.43 

195.37 

195.39 

195.41 

195.37 

2.17 

1.09 

78.8 

197.54 

71.5 

28.5 

0.0 

72.0 

44.0 

1.25 

21.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

••"'•' • ':*'*• ' . 

Final 

Time 

65 min 

ZO 40 
P.22 

CFA Vapor Suppressant Effectiveness Test Protocol 

Revision 7.4-July, 2002 

Page 41 of 41 

Test Pair No. 6 

Non-Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

198.66 

198.17 

190.67 

190.60 

190.53 

190.52 

190.51 

190.45 

190.48 

190.45 

8.21 

4.13 

83.41 

198.66 

0.0 

72.0 

44.0 

1.25 

21.0 

Roll-Out 

Time 

(mm:ss) 

02:00 

•.::*'••'*' .

 ; . ; : .*,.;;*.; * 

Final 

Time 

90 min 

Reichhold Chemical Test Data 

Vapor Suppressed 

Weight of Glass 

Initial Wt. of Resin 

Resin Content 

Glass Content 

Filler Content 

Temperature °F 

Humidity % 

Initiator Level % 

Gel Time 

Time (min) 

Initial Wt. 

Post RollOut Wt. 

5 

10 

15 

20 

25 

30 

35 

40 

45 

50 

55 

60 

65 

70 

75 

80 

85 

90 

95 

100 

105 

110 

115 

120 

125 

130 

Final Wt. 

Emissions 

Lost 

% 

Emissions 

Weight 

(g) 

198.19 

197.64 

196.07 

195.51 

195.95 

195.88 

195.82 

195.82 

195.83 

195.82 

2.37 

1.19 

84.52 

198.19 

0.0 

72.0 

43.0 

1.25 

21.5 

Roll-Out 

Time 

(mm:ss) 

02:00 

Final 

Time 

85 min 

2^1 41