P. L



# OAR Box 1490
Prepped hyCharmelle Mathews



## Document

Number: 

# 24 ) IV-B-2 6

Docket Number: 

# A-94-5 2

Printed 8/4/200811:51:46

AM Sheet 24of 273P. 2


# K/-B- K

MEMORANDU

M

TO : Docket

fo r theReinforce

dPlastic Composite s NESHA P

FROM : Keit

hBarnett , U

. S

. Environmenta lProtectionAgenc

y
DATE : Januar

y 14 , 200 3

SUBJECT : Test

Datato suppor

t theComposite s Fabricators AssociationVapor Suppressan

t Tes t Protocol

. Attachedi s dataprovidedb y theComposite s Manufacturers Associationto o suppor t theaccurac

y ofth etes t methodto determin

etheeffectivenes s o

f vapo r suppressants

. Thi s methodi s include d i ntheReinforce

dPlastic Composite s NESHA Pas Appendi

xAto 40 CF

Rpar t 63 subpar t WWWW

. Notetha

t thepagenumber

s o ntheattachmen

t begi nwit h22

.P. 3

CF AVapo r Suppressan

t Effectivenes s Test

Protoco l Revision7. 4 - July , 2002

Page2 2 o f 4 1



# VS E Tes t Data

Ashlan d Chemica l Eastma n Chemica l Reichhol d Chemica l

2

_P. 4

CF AVapo r Suppressan

t Effectivenes s Test

Protoco l Revision7.4-July , 2002

Page2 3 of

4 1

Ashlan d Tes t Dat a Summar y

Tes t Pai rNo

. 1 2 3 4 5 6 Avg

. W t Los s % V S Weigh t Los s
5.8 6 5.6 3 5. 9 5.5 8 5.4 2 5.9 9 5.7 3 % NV S Weigh t Los s

1.5 9 1.5 5 1.64 1.6 1 1.6 3 1.6 1 1.6 1 1-(% Av g W t Loss N v s / % Av g W t Loss VS ) = VS E Facto r0.72 0

Eastma n Tes t Dat a Summar y

Tes t Pai rNo

. 1 2 3 4 5 6 Avg

. Wt

. Los s % V S Weigh t Los s
4.5 3 4.8 3 4.4 4 4. 5 5. 1 4.7 1 4.6 9 % NV S Weigh t Los s

2.2 6 1.84 1.6 8 1.5 8 1.6 9 1.9 9 1.8 4 1-( % Av g W t Loss N v s / % Av g W t Loss VS ) - VS E Facto r0.60 7

Reichhol d Tes t Dat a Summary

Tes t Pai rNo

. 1 2 3 4 5 6 Avg

. Wt

. Los s % V S Weigh t Los s
4.3 3 4.3 2 4.1 8 4.1 6 4.3 4 4.1 3 4.2 4 % NV S Weigh t Los s

1.1 3 1.1 6 1.1 3 1.1 8 1.0 9 1.1 9 1.1 5 1-(% Av g W t Loss N v s / % Av g W t Lossvs ) = VS E Facto r0.73 0



# 3 23P. 5

' *

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page2 4 of 4 1

Tes t Pai rNo

. 1 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. PostRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
82.4 0

81.6 8 81.3 2 80.7 5 80.6 3 80.2 8 79.9 3 79.5 8 79.0 8 78.6 4 78.2 5 78.0 6 77.8 7 77.7 0 77.6 7 77.6 3 77.6 0 77.5 9 77.5 9 77.5 8 77.5 8 77.5 7 77.5 7 77.5 8

77.5 7

4.8 3

5.8 6 37.0 0

82. 4 69. 0 31. 0 0. 0 73. 7 60. 7 1.2 5 22. 9 Roll-Ou t Tim e (mm:ss )

02:1 0

•

Fina l Tim e

11 5 mi n Ashlan d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
82.3 8

81.8 3 81.4 8 81.3 7 81.3 2 81.3 1 81.2 8 81.2 5 81.2 2 81.2 0 81.1 8 81.1 7 81.1 6 81.1 2 81.1 2 81.1 1 81.1 0 81.0 9 81.0 8 81.0 8 81.0 7 81.0 7 81.0 7

81.0 7

1.3 1

1.5 9 36.9 6

82.3 8 69. 0 31. 0 0. 0 73. 7 60. 7 1.2 5 24. 5 Roll-Ou t Tim e (mm:ss )

02:1 0

**•'••

. . ' •) ,

Fina l Tim e

11 0 mi n



# ^ f 24P. 6

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page2 5 of

4 1

Tes t Pai rNo

. 2 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
83.3 7

78.6 9 78.6 8 78.6 8 78.6 8

78.6 8

4.6 9

5.6 3 37.3 3

83.3 7 69. 1 30. 9 0. 0 73. 6 59. 9 1.2 5 22. 9 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

8 0 mi n Ashlan d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
83.7 1

82.4 5 82.4 3 82.4 3 82.4 2 82.4 1 82.4 2

82.4 1

1.3 0

1.5 5 37.2 8

83.7 1 69. 2 30. 8 0. 0 73. 6 59. 9 1.2 5 24. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

8 5 mi n



## 25P. 7

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7.4-July , 2002

Pag e2 6 of 4 1
Tes t Pai rNo

. 3 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos t Roll
Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wl

. Emission s Los t % Emission s Weigh t

(g )
86.1 1

81.0 5 81.0 5 81.0 4 80.0 3 81.0 4

81.0 3

5.0 8

5.9 0 38.6 1

86.1 1 69. 1 30. 9 0. 0 73. 6 61. 2 1.2 5 22. 9 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

8 0 mi n Ashlan d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos t Roll
Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wl

. Emission s Los t % Emission s Weigh t

(g )
86.2 1

84.8 6 84.8 3 84.8 3 84.8 0 84.8 0 84.8 0

84.8 0

1.4 1

1.64 38.7 2

86.2 1 69. 0 31. 0 0. 0 73. 6 61. 2 1.2 5 24. 5 Roll-Ou t Tim e (mm:ss )

02:1 0

Fina l Tim e

9 0 mi n



## (p 2 «P. 8

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7.4-July , 2002

Page2 7 o f 4 1
Tes t Pai rNo

. 4 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
85.0 6

80.4 5 80.3 9 80.3 7 80.3 5 80.3 3 80.3 2 80.3 1 80.3 1 80.3 2

80.3 1

4.7 5

5.5 8 38.2 6

85.0 6 69. 0 31. 0 0. 0 73. 9 61. 3 1.2 5 22. 9 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

10 0 mi n Ashlan d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e U F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
85.0 6

84.5 8 84.5 6 84.5 5 84.5 5 84.5 3 84.5 3 84.5 4

84.5 3

1.3 8

1.6 1 38.2 5

85.9 1 69. 2 30. 8 0. 0 73. 9 61. 3 1.2 5 24. 5 Roll-Ou t Tim e (mm:ss )

02:1 0

Fina l Tim e

•9 0 mi n



# 7 27P. 9

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page2 8 of 4 1
Tes t Pai rNo

. 5 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % 

### Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
90.0 3

85.2 0 85.2 0 85.1 8 85.1 7 85.1 7 85.1 5 85.1 5 85.1 6

85.1 5

4.8 8

5.4 2 40.2 1

90.0 3 69. 1 30. 9 0. 0 73. 7 58. 5 1.2 5 22. 5 Roll-Ou t Tim e (mm:ss )

02:1 0

Fina l Tim e

9 5 mi n Ashlan d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
89.5 6

88.1 8 88.1 2 88.1 2 88.1 0 88.1 0 88.1 0

88.1 0

1.4 6

1.6 3 39.9 0

89.5 6 69. 2 30. 8 0. 0 73. 7 58. 5 1.2 5 24. 9 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 0 mi n



# r 28P.1 0

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page29 o f 4 1
Tes t Pai rNo

. 6 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
81.0 1

76.2 5 76.2 5 76.2 3 76.2 2 76.2 2 76.2 3

76.2 2

4.7 9

5.9 9 36.4 3

81.0 1 69. 0 31. 0 0. 0 73. 9 58. 3 1.2 5 22. 9 Roll-Ou t Tim e (mm:ss )

02:0 0

* ' *" : -'-.:•.

. S'SFina l Tim e

8 5 mi n Ashlan d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
81.1 2

79.8 4 79.8 2 79.8 2 79.8 1 79.8 2

79.8 1

1.3 1

1.6 1 36.4 8

81.1 2 69. 0 31. 0 0. 0 73. 9 58. 3 1.2 5 24. 5 Roll-Ou t Tim e (mm:ss )

02:1 0

Fina l Tim e

- 8 0 mi n



# °l 2 9P.1 1

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7.4-July , 2002

Page3 0 of 4 1
Tes t Pai rNo

. 1 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 13 5 14 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
80.3 3
80.0 2 80.0 1 79.9 1 79.8 0 79.6 0 79.4 2 79.1 5 78.9 2 78.6 7 78.4 5 78.2 8 78.0 8 77.6 5 77.3 0 77.0 9 76.9 6 76.8 9 76.8 4 76.7 8 76.7 5 76.7 3 76.6 9 76.7 1

76.6 9

3.6 4

4.5 3 35. 7

80.3 3 69. 2 30. 8 0. 0 70. 0 50. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

10 5 mi n Eastma n Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e U F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 13 5 14 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
78.7 2
78.4 2 78.4 2 78.2 8 77.8 4 77.7 9 77.7 9 77.7 7 77.7 6 77.7 2 77.6 7 77.6 1 77.5 7 77.5 4 77.5 1 77.4 7 77.4 2 77.3 3 77.2 5 77.2 1 77.1 6 77.1 1 77.0 7 77.0 5 77.0 1 76.9 8 76.9 6 76.9 5 76.9 4 76.9 6 76.9 4

1.78

2.2 6 34.8 2

78.7 2 69. 3 30. 6 0. 0 70. 0 50. 0 1.2 5 19. 7 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

13 5 mi n



# 10 30P.1 2

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page3 1 o f 4 1

Tes t Pai rNo

. 2 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
73.6 5
73.3 0

70.2 6 70.2 0 70.1 6 70.1 3 70.1 2 70.1 0 70.0 9 70.0 9 70.1 0

70.0 9

3.5 6

4.8 3 31.9 6

73.6 5 96. 7 30. 2 0. 0 , 71. 0 50. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

Fina l Tim e

10 0 mi n Eastma n Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
72.9 2
72.6 2

71.8 0 71.7 7 71.7 5 71.7 1 71.6 8 71.6 4 71.6 2 71.6 0 71.5 9 71.5 8 71.5 8 71.5 8

71.5 8

1.34

1.84 30.8 8

72.9 2 70. 2 29. 7 0. 0 71. 0 50. 0 1.2 5 19. 7 Roll-Ou t Tim e (mm:ss )

Fina l Tim e

11 0 mi n



# ll 31P.1 3

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revisio n7. 4 - July , 2002

Page3 2 o f 4 1

Tes t Pai rNo

. 3 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
72.2 2
71.9 5

69.1 5 69.0 8 69.0 5 69.0 5 69.0 4 69.0 3 69.0 2 69.0 0 69.0 2

69.0 0

3.2 2

4.4 4 30.9 2

72.2 2 70. 1 29. 9 0. 0 70. 0 50. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

10 0 mi n Eastma n Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
76.2 5
75.9 9

75.1 8 75.1 3 75.0 9 75.0 6 75.0 2 75.0 0 74.9 8 74.9 7 74.9 7 74.9 7

74.9 7

1.2 8

1.6 8 32.9 3

76.2 5 69. 8 30.1 6 0. 0 70. 0 50. 0 1.2 5 19. 7 Roll-Ou t Tim e (mm:ss )

02:0 0

y\. •-..- ' *

.

Fina l Tim e

10 0 mi n



# \1 32P.1 4

CF AVapo r Suppressan

t Effectivenes s Tes t

Protocol Revision7. 4 - July , 2002

Page3 3 of

4 1

Tes t Pai rNo

. 4 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 .1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emissipn s Los t % Emission s Weigh t

(g )
79.9 9
79.6 1

76.6 2 76.5 3 76.4 6 76.4 0 76.4 0 76.3 9 76.3 9 76.3 9

76.3 9

3.6 0

4.5 0 34.2 5

79.9 9 70.0 2 29.9 8 0. 0 69. 0 50. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:1 5

Fina l Tim e

10 0 mi n Eastma n Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
81.2 3
80.9 9

80.1 4 80.1 2 80.0 7 80.0 3 80.0 0 79.9 6 79.9 5 79.9 4 79.9 4 79.9 4

79.9 4

1.2 9

1.5 8 35.0 4

81.2 3 69.8 6 30.1 3 0. 0 69. 0 50. 0 1.2 5 19. 7 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

- 10 0 mi n



# a 33P.1 5

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7.4-July , 2002

Page3 4 of

4 1
Tes t Pai rNo

. 5 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e U F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
70.7 8
70.4 9

67.6 5 67.4 5 67.3 6 67.3 1 67.2 7 67.2 5 67.2 1 67.1 8 67.1 7 67.1 8

67.1 7

3.6 1

5.1 0 30.1 3

70.7 8 70.1 4 29.8 5 0. 0 70. 0 50. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

10 5 mi n Eastma n Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s InHia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
74.1 7
73.7 4

73.1 6 73.1 4 73.1 0 73.0 5 73.0 1 72.9 7 72.9 5 72.9 5 72.9 4 72.9 4 72.9 1 72.9 2

72.9 1

1.2 6

1.6 9 31.8 1

74.1 7 69.9 8 30.0 1 0. 0 70. 0 50. 0 1.2 5 19. 7 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

11 5 mi n

/ • / 

## 34P.1 6

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page3 5 of

4 1
Tes t Pai rNo

. 6 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
75.2 2 74.8 5

72.2 6 72.0 4 71.9 1 71.8 1 71.7 7 71.7 3 71.7 1 71.6 9 71.6 9 71.6 8 71.6 8 71.6 7 71.6 7 71.6 7 71.6 7

3.5 5

4.7 1 32.5 0

75.2 2 69.8 2 30.1 7 0. 0 70. 0 50. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:1 5

Fina l Tim e

12 0 mi n Eastma n Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
76.6 3
76.2 6

75.2 9 75.2 2 75.1 8 75.1 5 75.1 3 75.1 2 75.1 1 75.1 0 75.1 0 75.1 0

75.1 0

1.5 3

1.9 9 32.6 3

76.6 3 70.1 3 29.8 6 0. 0 70. 0 50. 0 1.2 5 19. 7 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

10 0 mi n



# I S 35P.1 7

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page3 6 of 4 1
Tes t Pai rNo

. 1 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
198.0 9
197.6 3 196.9 1 196.8 2 195.6 0 194.9 6 194.2 0 193.4 5 192.6 1 191.7 7 191.0 2 190.4 9 190.1 5 189.9 4 189.7 9 189.7 9 189.6 4 189.6 4 189.5 7 189.5 4 189.5 0 189.5 0 189.5 0

189.5 0

8.5 9

4.3 3 85.4 4

198.0 9 69. 8 30. 1 0. 0 72. 0 44. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 5 mi n Reichhol d Chemica l Tes t Dat a

Vapo rSuppresse d | Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
198.8 7
198.3 6 197.7 2 197.3 9 197.3 1 197.2 8 197.2 2 197.1 9 197.1 2 197.0 5 196.9 7 196.9 1 196.9 1 196.8 6 196.8 3 196.8 3 196.7 3 196.7 3 196.7 1 196.7 1 196.6 2 196.6 5

196.6 2

2.2 5

1.1 3 83.4 9

198.8 7 70. 4 29. 6 0. 0 72. 0 44. 0 1.2 5 21. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 5 mi n



# It* 36P.1 8

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page3 7 of 4 1
Tes t Pai rNo

. 2 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
196.3 8
196.3 8

188.0 4 188.0 1 187.9 8 187.9 5 187.9 3 187.8 9 187.8 9 187.9 1

187.8 9

8.4 9

4.3 2 86.8 7

196.3 8 30. 6 69. 3 0. 0 72. 0 44. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

}.S\ ••'••;:;•

: : y

Fina l Tim e

9 0 mi n Reichhol d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % I Emission s Weigh t

(g )
198.0 7
197.5 9

195.9 5 195.9 2 195.9 0 195.8 8 195.8 7 195.8 3 195.7 8 195.7 9

195.7 8

2.2 9

1.1 6 81.1 8

198.0 7 71. 0 29. 0 0. 0 72. 0 44. 0 1.2 5 21. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

''s', '*

. "•'".- ' '. S *-*-''*

.

Fina l Tim e

9 5 mi n



# I 7 37P.1 9

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page3 8 of 4 1
Tes t Pai rNo

. 3 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e U F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou t Wt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
197.5 7
196.9 1

189.6 1 189.5 6 189.5 1 189.4 5 189.4 0 189.3 7 189.3 0 189.3 0 189.3 0

189.3 0

8.2 7

4.1 8 80.5 1

197.5 7 71. 1 28. 9 0. 0 72. 0 44. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 5 mi n Reichhol d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0

. 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
197.2 7
196.8 2

195.3 1 195.2 2 195.1 4 195.1 5 195.1 6 195.0 7 195.0 4 195.0 4 195.0 4

195.0 4

2.2 3

1.1 3 81.5 4

197.2 7 70. 8 29. 2 0. 0 72. 0 44. 0 1.2 5 21. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 5 mi n



# If r 38P.2 0

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page3 9 o f 4 1
Tes t Pai rNo

. 4 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
196.7 2
196.2 9

188.8 8 188.7 9 188.7 1 188.6 5 188.6 0 188.5 8 188.5 2 188.5 3

188.5 2

8.2 0

4.1 6 85.5 8

196.7 2 30. 3 69. 7 0. 0 72. 0 44. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 5 mi n Reichhol d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
198.1 6
197.6 5

195.9 4 195.8 7 195.8 1 195.8 1 195.8 2

195.8 1

2.3 5

1.1 8 82.3 0

198.1 6 70. 7 29. 3 0. 0 72. 0 43. 0 1.2 5 21. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

, . *•-..

.

Fina l Tim e

7 5 mi n



# 11 39P.2 1

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7. 4 - July , 2002

Page4 0 of 4 1

Tes t Pai rNo

. 5 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
198.7 4
198.2 3

190.3 3 190.2 8 190.2 3 190.2 0 190.1 7 190.1 1 190.1 2

190.1 1

8.6 3

4.3 4 84.1 8

198.7 4 70. 3 29. 7 0. 0 72. 0 44. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

9 0 mi n Reichhol d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e U F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
197.5 4
197.0 4

195.4 3 195.3 7 195.3 9 195.4 1

195.3 7

2.1 7

1.0 9 78. 8

197.5 4 71. 5 28. 5 0. 0 72. 0 44. 0 1.2 5 21. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

••"'•' •':*'*• '

.

Fina l Tim e

6 5 mi n



## ZO 40P.2 2

CF AVapo r Suppressan

t Effectivenes s Test

Protocol Revision7.4-July , 2002

Page4 1 of 4 1

Tes t Pai rNo

. 6 Non-Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
198.6 6
198.1 7

190.6 7 190.6 0 190.5 3 190.5 2 190.5 1 190.4 5 190.4 8

190.4 5

8.2 1

4.1 3 83.4 1

198.6 6

0. 0 72. 0 44. 0 1.2 5 21. 0 Roll-Ou t Tim e (mm:ss )

02:0 0

•.::*'••'*'

. ; . ; : .*,.;;*.; *

Fina l Tim e

9 0 mi n Reichhol d Chemica l Tes t Dat a

Vapo rSuppresse d Weigh t o fGlas s Initia l Wt

. o fResi n Resi n Conten t Glas s Conten t Fille rConten t Temperatur e ° F Humidit y% Initiato rLeve l % Ge l Tim e

Tim e (min )

Initia l Wt

. Pos tRoll

Ou tWt

. 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 4 5 5 0 5 5 6 0 6 5 7 0 7 5 8 0 8 5 9 0 9 5 10 0 10 5 11 0 11 5 12 0 12 5 13 0 Fina l Wt

. Emission s Los t % Emission s Weigh t

(g )
198.1 9
197.6 4

196.0 7 195.5 1 195.9 5 195.8 8 195.8 2 195.8 2 195.8 3

195.8 2

2.3 7

1.1 9 84.5 2

198.1 9

0. 0 72. 0 43. 0 1.2 5 21. 5 Roll-Ou t Tim e (mm:ss )

02:0 0

Fina l Tim e

8 5 mi n



# 2^1 41