# Appendix D



# 3M/Dyneon Gendorf Facility Report
on Product Content
for 2010

## 2010/15 PFOA Stewardship Program 

# 3M/Dyneon Gendorf Facility Report on Product
Content

I. CHEMICAL IDENTIFICATION

Identify the product (e.g fluoropolymer dispersion) for which you are submitting
information:

Product name:_Liquid PTFE dispersions

__

Product description (including concentrations of perfluoroalkyl chemicals
identified in Section IV be low and year of production):

This product family consists of the commercia lly available aqueous PTFE dispersions. The PTFE dispersions contain an average of 59 % by wei ght of PTFE in water. The use of APFO for the manufacture of the Liquid PTFE dispersi ons ceased on April 1, 2008, and the new APFO replacement emulsifier was used exclusively after that date. All dispersions sold in 2010 were made without using APFO.

II. COMPANY IDENTIFICATION

Identify the company and location of the facility submitting information:

Company name:___ Dyneon/3M

__________________

Site location:_____ Gendorf, Germany____

Identify a company technical contact who can respond to inquiries about the information
submitted:
Technical contact:_ George H. Millet___________________ Phone:_____ 651-733-5637

__________________________ Address:__ 6744 33 rd St N., Oakdale, MN, 55082

_________

III. PRODUCTION

Calendar year for which you are reporting: Jan 1, 2010 to Dec 31, 2010

Provide the amount of the product for the reporting year at ea ch specific site:Imported ____ 0 ____kg/yr

Manufactured APFO Containing Dispersions 0 kg/yr (wet weight)

IV. PRODUCT CONTENT

A. CONCENTRATIONS OF RELEVANT PERFLUOROALKYL CHEMICALS

Please provide the concentrations (ppb) of various perfluoroalkyl chemicals in your product. For chemicals for which you do not have actual data, please provide range
estimates.

Not applicable – Dyneon no longer uses APFO or any higher homologue or precursor for the manufacture of any fluoropolymer.

The following is a nonexhaustive list of chemicals that should be included:

PFOA and its salts

• Octanoic acid, pentadecaf luoro- (CAS 335-67-1)

• Octanoic acid, pentadecafluoro- ammonium salt (CAS 3825-26-1)

PFOA precursors

• Octane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7, 8,8-heptadecafl uoro-8-iodo- (CAS 507-63-1)

• 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecaf luoro- (CAS 678-39-7)

• 1-Decene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 21652-58- 4)

• 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 27905-45-9)

• 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 1996-88-9)

• 2-Decenoic acid, 3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-hexa decafluoro- (CAS 70887- 84-2)

• Decanoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 27854- 31-5)

Higher homologues

• Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12- pentacosafluoro-12-iodo- (CAS 307-60-8)

• Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-10-iodo-(CAS 423-62-1)

• Nonanoic acid, heptadecaf luoro- (CAS 375-95-1)

• Decanoic acid, nonadecafluoro- (CAS 335-76-2)

• 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecaf luoro- (CAS 678-39-7)

• Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-heptadecafluoro-10-iodo- (CAS 2043- 53-0)

• Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-12-iodo- (CAS 2043-54-1)

• 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl ester (CAS 4980-53-4)

• 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12- heneicosafluorododecyl ester (CAS 17741-60-5) Part IV (cont.)

B. ANALYTICAL METHODS

Analyses should be conducted using the most accurate instrumentation and procedures available as of the time of testing. Please provide detailed information on the methods used (including analytical standards used, sampling, sample treatment, analysis), assumptions made, uncertainties and detecti on limits (LOD, LOQ) for the data provided.

## 2010/15 PFOA Stewardship Program 

# 3M/Dyneon Gendorf Facility Report on
Product Content

I. CHEMICAL IDENTIFICATION

Identify the product (e.g fluoropolymer dispersion) for which you are submitting
information:

Product name:__ Liquid Fluoroplastic dispersions

__

Product description (including conc entrations of perfluoroalkyl
chemicals identified in Section IV below and year of production):

This product family consisted of the commerc ially available aqueous dispersions of melt processible fluoroplastics (PFA, FEP, ETFE, THV, etc.). The fluoroplastic dispersions contained an average of 38% by weight of fluoroplastic in wa ter. The use of APFO for the manufacture of these dispersions ceased on April 1, 2008, and the new APFO replacement emulsifier was used exclusively after that date. All of the products made using APFO were sold in 2008. All dispersi ons sold in 2010 were made without using
APFO.

II. COMPANY IDENTIFICATION

Identify the company and location of the facility submitting information:

Company name:___ Dyneon/3M

__________________

Site location:_____ Gendorf, Germany____

Identify a company technical contact who can respond to inquiries about the
information submitted:
Technical contact:_ George H. Millet___________________ Phone:_____ 651-733-5637

__________________________ Address:__ 6744 33 rd St N., Oakdale, MN, 55082

_________

III. PRODUCTION

Calendar year for which you are reporting: Jan 1, 2010 to Dec 31, 2010Provide the amount of the product for the reporting year at ea ch specific site:

Imported ____ 0 ____kg/yr

Manufactured APFO Containing Dispersions ____ 0 ____kg/yr (wet Weight)

IV. PRODUCT CONTENT

A. CONCENTRATIONS OF RELEVANT PERFLUOROALKYL
CHEMICALS

Please provide the concentrations (ppb) of various perfluoroalkyl chemicals in your product. For chemicals for which you do not have actual data, please provide range estimates.

Not applicable – Dyneon no longer uses APFO or any higher homologue or precursor for the manufacture of any fluoropolymer.

The following is a nonexhaustive list of chemicals that should be included:

PFOA and its salts

• Octanoic acid, pentadecaf luoro- (CAS 335-67-1)

• Octanoic acid, pentadecafluoro- ammonium salt (CAS 3825-26-1)

PFOA precursors

• Octane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7, 8,8-heptadecafluoro-8-iodo- (CAS 507-63-1)

• 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7)

• 1-Decene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 21652-58-4)

• 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 27905-45-9)

• 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 1996-88-9)

• 2-Decenoic acid, 3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-he xadecafluoro- (CAS 70887-84-2)

• Decanoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 27854-31-5)

Higher homologues

• Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12-pentacosafluoro-12-iodo- (CAS 307-60-8)

• Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-10- iodo- (CAS 423-62-1)

• Nonanoic acid, heptadecaf luoro- (CAS 375-95-1)

• Decanoic acid, nonadecafluoro- (CAS 335-76-2)

• 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7)

• Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-heptadecafluoro-10-iodo- (CAS 2043-53-0)

• Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-12- iodo- (CAS 2043-54-1)

• 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 4980-53-4)

• 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluorododecyl ester (CAS 17741-60-5) Part IV (cont.)

B. ANALYTICAL METHODS

Analyses should be conducted using the most accurate instrumentation and procedures available as of the time of test ing. Please provide detailed information on the methods used (including analytic al standards used, sampling, sample treatment, analysis), assumptions made , uncertainties and detection limits (LOD, LOQ) for the data provided.

## 2010/15 PFOA Stewardship Program 

# 3M/Dyneon Gendorf Facility Report on
Product Content

I. CHEMICAL IDENTIFICATION

Identify the product (e.g fluoropolymer dispersion) for which you are submitting
information:

Product name: Dry Resin Products_

Product description (including conc entrations of perfluoroalkyl
chemicals identified in Section IV below and year of production):

This product family consisted of the commercially available melt processible fluoroplastics (PFA, FEP, ETFE, THV, etc.) and PTFE, all sold as dry pellets or powders. The average APFO content of these products were all very simila r, typically below 5 ppm, based on the weight of product. The us e of APFO for the ma nufacture of the melt processible fluoroplastics was discontinued in July 2008. The use of APFO for the manufacture of PTFE dry resin products was discontinued at the end of December, 2008. The new APFO replacement emulsifier was us ed to manufacture these products after the
dates mentioned above.

During 2010, the remaining inventory of dry resin products made in 2008 using APFO was sold; by the end of the year, we were selling only products made using our new
emulsifier.

II. COMPANY IDENTIFICATION

Identify the company and location of the facility submitting information:

Company name:___ Dyneon/3M

__________________

Site location:_____ Gendorf, Germany____

Identify a company technical contact who can respond to inquiries about the
information submitted:
Technical contact:_ George H. Millet___________________ Phone:_____ 651-733-5637

__________________________ Address:__ 6744 33 rd St N., Oakdale, MN, 55082

_________III. PRODUCTION

Calendar year for which you are reporting: Jan 1, 2010 to Dec 31, 2010

Provide the amount of the product for the reporting year at ea ch specific site:

Imported ___ 0___ kg/yr

Manufactured

Dry Resin Products 23,000 kg/yr

IV. PRODUCT CONTENT

A. CONCENTRATIONS OF RELEVANT PERFLUOROALKYL
CHEMICALS

Please provide the concentrations (ppb) of various perfluoroalkyl chemicals in your product. For chemicals for which you do not have actual data, please provide range estimates.

Concentration of APFO in the products ma de using APFO was an average of 3 ppm based on dry weight of product.

The following is a nonexhaustive list of chemicals that should be included:

PFOA and its salts

• Octanoic acid, pentadecaf luoro- (CAS 335-67-1)

• Octanoic acid, pentadecafluoro- ammonium salt (CAS 3825-26-1)

PFOA precursors

• Octane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7, 8,8-heptadecafluoro-8-iodo- (CAS 507-63-1)

• 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7)

• 1-Decene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 21652-58-4)

• 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 27905-45-9)

• 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 1996-88-9)

• 2-Decenoic acid, 3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-he xadecafluoro- (CAS70887-84-2)

• Decanoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 27854-31-5)

Higher homologues

• Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12- pentacosafluoro-12-iodo- (CAS 307-60-8)

• Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-10- iodo- (CAS 423-62-1)

• Nonanoic acid, heptadecaf luoro- (CAS 375-95-1)

• Decanoic acid, nonadecafluoro- (CAS 335-76-2)

• 1-Decanol, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro- (CAS 678-39-7)

• Decane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-heptadecafluoro-10-iodo- (CAS 2043-53-0)

• Dodecane, 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10-heneicosafluoro-12- iodo- (CAS 2043-54-1)

• 2-Propenoic acid, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10- heptadecafluorodecyl ester (CAS 4980-53-4)

• 2-Propenoic acid, 2-methyl-, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heneicosafluorododecyl ester (CAS 17741-60-5) Part IV (cont.)

B. ANALYTICAL METHODS

Analyses should be conducted using the most accurate instrumentation and procedures available as of the time of test ing. Please provide detailed information on the methods used (including analytic al standards used, sampling, sample treatment, analysis), assumptions made , uncertainties and detection limits (LOD, LOQ) for the data provided.