Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-001 Date Collected: 08/21/2013 Date Received: 8/21/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 16.6 ug/L 0.050 0.010 DPC 09/05/2013 12:33 EPA 200.8

Arsenic, As 132 ug/L 0.10 0.030 DPC 09/05/2013 12:33 EPA 200.8

Barium, Ba 1010 ug/L 0.10 0.020 DPC 09/05/2013 12:33 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 08/29/2013 15:38 EPA 200.7

Cadmium, Cd 267 ug/L 0.050 0.010 DPC 09/05/2013 12:33 EPA 200.8

Chromium, Cr 722 ug/L 0.20 0.040 DPC 09/05/2013 12:33 EPA 200.8

Cobalt, Co 330 ug/L 0.020 0.0040 DPC 09/05/2013 12:33 EPA 200.8

Copper, Cu 377 ug/L 0.050 0.010 DPC 09/05/2013 12:33 EPA 200.8

Lead, Pb 191 ug/L 0.010 0.0020 DPC 09/05/2013 12:33 EPA 200.8

Mercury, Hg 194000 ng/L 5000 2000 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 302 ug/L 0.050 0.010 DPC 09/05/2013 12:33 EPA 200.8

Nickel, Ni 1690 ug/L 0.20 0.050 DPC 09/05/2013 12:33 EPA 200.8

Selenium, Se 949 ug/L 0.50 0.20 DPC 09/05/2013 12:33 EPA 200.8

Silver, Ag 0.435 ug/L 0.010 0.0020 DPC 09/05/2013 12:33 EPA 200.8

Thallium, Tl 13.0 ug/L 0.050 0.0020 DPC 09/05/2013 12:33 EPA 200.8

Tin, Sn 1010 ug/L 500 150 DAM 08/29/2013 15:39 EPA 200.7

Titanium, Ti 419 ug/L 100 15 DAM 08/29/2013 15:39 EPA 200.7

Zinc, Zn 3680 ug/L 0.50 0.10 DPC 09/05/2013 12:33 EPA 200.8

Aluminum, Al 56.6 mg/L 0.0010 0.0003 DPC 09/05/2013 12:33 EPA 200.8

Boron, B 461 mg/L 1.0 0.20 DAM 08/29/2013 15:38 EPA 200.7

Calcium, Ca 3730 mg/L 1.0 0.20 DAM 08/29/2013 15:38 EPA 200.7

Iron, Fe 223 mg/L 2.5 0.50 DAM 08/29/2013 15:38 EPA 200.7

Magnesium, Mg 4390 mg/L 0.50 0.10 DAM 08/29/2013 15:38 EPA 200.7

Manganese, Mn 87.1 mg/L 0.025 0.0050 DAM 08/29/2013 15:38 EPA 200.7

Potassium, K 91.3 mg/L 2.5 0.35 DAM 08/29/2013 15:37 EPA 200.7

Sodium, Na 346 mg/L 1.5 0.40 DAM 08/29/2013 15:37 EPA 200.7

Strontium, Sr 13.4 mg/L 0.050 0.015 DAM 08/29/2013 15:37 EPA 200.7

Ammonia, NH3, as N 2.27 mg/L 0.050 0.020 DMM 08/26/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 0.96 mg/L 0.50 0.10 DMM 08/28/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 35.4 mg/L 0.10 0.020 DMM 08/27/2013 SM20 4500NO3 H

Mountaineer Plant, 133429 Page 1 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-001A Date Collected: 08/21/2013 Date Received: 8/21/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.58 ug/L 0.050 0.010 DPC 09/05/2013 12:38 EPA 200.8

Arsenic, As 3.82 ug/L 0.10 0.030 DPC 09/05/2013 12:38 EPA 200.8

Barium, Ba 68.9 ug/L 0.10 0.020 DPC 09/05/2013 12:38 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 08/29/2013 15:42 EPA 200.7

Cadmium, Cd 171 ug/L 0.050 0.010 DPC 09/05/2013 12:38 EPA 200.8

Chromium, Cr 1.2 ug/L 0.20 0.040 DPC 09/05/2013 12:38 EPA 200.8

Cobalt, Co 216 ug/L 0.020 0.0040 DPC 09/05/2013 12:38 EPA 200.8

Copper, Cu 9.21 ug/L 0.050 0.010 DPC 09/05/2013 12:38 EPA 200.8

Lead, Pb 0.885 ug/L 0.010 0.0020 DPC 09/05/2013 12:38 EPA 200.8

Mercury, Hg 67.8 ng/L 10 4.0 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 181 ug/L 0.050 0.010 DPC 09/05/2013 12:38 EPA 200.8

Nickel, Ni 1100 ug/L 0.20 0.050 DPC 09/05/2013 12:38 EPA 200.8

Selenium, Se 326 ug/L 0.50 0.20 DPC 09/05/2013 12:38 EPA 200.8

Selenite, Se+4 (Hydride) 230 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag 0.019 ug/L 0.010 0.0020 DPC 09/05/2013 12:38 EPA 200.8

Thallium, Tl 7.00 ug/L 0.050 0.0020 DPC 09/05/2013 12:38 EPA 200.8

Tin, Sn 410 ug/L J 500 150 DAM 08/29/2013 15:43 EPA 200.7

Titanium, Ti < 15 ug/L U 100 15 DAM 08/29/2013 15:42 EPA 200.7

Zinc, Zn 528 ug/L 0.50 0.10 DPC 09/05/2013 12:38 EPA 200.8

Aluminum, Al 0.0440 mg/L 0.0010 0.0003 DPC 09/05/2013 12:38 EPA 200.8

Boron, B 448 mg/L 1.0 0.20 DAM 08/29/2013 15:42 EPA 200.7

Calcium, Ca 822 mg/L 1.0 0.20 DAM 08/29/2013 15:42 EPA 200.7

Iron, Fe < 0.50 mg/L U 2.5 0.50 DAM 08/29/2013 15:43 EPA 200.7

Magnesium, Mg 3760 mg/L 0.50 0.10 DAM 08/29/2013 15:42 EPA 200.7

Manganese, Mn 79.4 mg/L 0.025 0.0050 DAM 08/29/2013 15:42 EPA 200.7

Potassium, K 74.9 mg/L 2.5 0.35 DAM 08/29/2013 15:41 EPA 200.7

Sodium, Na 341 mg/L 1.5 0.40 DAM 08/29/2013 15:41 EPA 200.7

Strontium, Sr 7.75 mg/L 0.050 0.015 DAM 08/29/2013 15:41 EPA 200.7

Mountaineer Plant, 133429 Page 2 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-002 Date Collected: 08/21/2013 Date Received: 8/21/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.24 ug/L 0.050 0.010 DPC 09/05/2013 12:43 EPA 200.8

Arsenic, As 3.42 ug/L 0.10 0.030 DPC 09/05/2013 12:43 EPA 200.8

Barium, Ba 77.3 ug/L 0.10 0.020 DPC 09/05/2013 12:43 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 15:47 EPA 200.7

Cadmium, Cd 0.25 ug/L 0.050 0.010 DPC 09/05/2013 12:43 EPA 200.8

Chromium, Cr 4.4 ug/L 0.20 0.040 DPC 09/05/2013 12:43 EPA 200.8

Cobalt, Co 0.860 ug/L 0.020 0.0040 DPC 09/05/2013 12:43 EPA 200.8

Copper, Cu 0.82 ug/L 0.050 0.010 DPC EPA 200.8

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

09/05/2013 12:43

Lead, Pb 0.233 ug/L 0.010 0.0020 DPC EPA 200.8

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

09/05/2013 12:43

Mercury, Hg 183 ng/L 20 8.0 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 211 ug/L 0.050 0.010 DPC 09/05/2013 12:43 EPA 200.8

Nickel, Ni 21.3 ug/L 0.20 0.050 DPC 09/05/2013 12:43 EPA 200.8

Selenium, Se 362 ug/L 0.50 0.20 DPC 09/05/2013 12:43 EPA 200.8

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 09/05/2013 12:43 EPA 200.8

Thallium, Tl 1.10 ug/L 0.050 0.0020 DPC 09/05/2013 12:43 EPA 200.8

Tin, Sn 190 ug/L 100 30 DAM 08/29/2013 15:47 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 15:47 EPA 200.7

Zinc, Zn 5.5 ug/L 0.50 0.10 DPC 09/05/2013 12:43 EPA 200.8

Aluminum, Al 0.140 mg/L 0.0010 0.0003 DPC 09/05/2013 12:43 EPA 200.8

Boron, B 325 mg/L 0.20 0.040 DAM 08/29/2013 15:47 EPA 200.7

Calcium, Ca 810 mg/L 0.20 0.040 DAM 08/29/2013 15:47 EPA 200.7

Iron, Fe 0.26 mg/L J 0.50 0.10 DAM 08/29/2013 15:47 EPA 200.7

Magnesium, Mg 2790 mg/L 0.10 0.020 DAM 08/29/2013 15:47 EPA 200.7

Manganese, Mn 37.6 mg/L 0.0050 0.0010 DAM 08/29/2013 15:47 EPA 200.7

Potassium, K 54.0 mg/L 0.50 0.070 DAM 08/29/2013 15:45 EPA 200.7

Sodium, Na 268 mg/L 0.30 0.080 DAM 08/29/2013 15:45 EPA 200.7

Strontium, Sr 6.18 mg/L 0.010 0.0030 DAM 08/29/2013 15:45 EPA 200.7

Ammonia, NH3, as N 13.6 mg/L 0.050 0.020 DMM 08/26/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.34 mg/L 0.50 0.10 DMM 08/28/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 23.7 mg/L 0.10 0.020 DMM 08/27/2013 SM20 4500NO3 H

Mountaineer Plant, 133429 Page 3 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-002A Date Collected: 08/21/2013 Date Received: 8/21/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.22 ug/L 0.050 0.010 DPC 09/05/2013 12:47 EPA 200.8

Arsenic, As 3.17 ug/L 0.10 0.030 DPC 09/05/2013 12:47 EPA 200.8

Barium, Ba 69.7 ug/L 0.10 0.020 DPC 09/05/2013 12:47 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 15:56 EPA 200.7

Cadmium, Cd 0.08 ug/L 0.050 0.010 DPC 09/05/2013 12:47 EPA 200.8

Chromium, Cr 2.9 ug/L 0.20 0.040 DPC 09/05/2013 12:47 EPA 200.8

Cobalt, Co 0.387 ug/L 0.020 0.0040 DPC 09/05/2013 12:47 EPA 200.8

Copper, Cu 4.76 ug/L 0.050 0.010 DPC EPA 200.8

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

09/05/2013 12:47

Lead, Pb 0.502 ug/L 0.010 0.0020 DPC EPA 200.8

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

09/05/2013 12:47

Mercury, Hg 2.9 ng/L 2.0 0.80 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 194 ug/L 0.050 0.010 DPC 09/05/2013 12:47 EPA 200.8

Nickel, Ni 12.8 ug/L 0.20 0.050 DPC 09/05/2013 12:47 EPA 200.8

Selenium, Se 332 ug/L 0.50 0.20 DPC 09/05/2013 12:47 EPA 200.8

Selenite, Se+4 (Hydride) 321 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/05/2013 12:47 EPA 200.8

Thallium, Tl 0.86 ug/L 0.050 0.0020 DPC 09/05/2013 12:47 EPA 200.8

Tin, Sn 174 ug/L 100 30 DAM 08/29/2013 15:56 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 15:56 EPA 200.7

Zinc, Zn 5.8 ug/L 0.50 0.10 DPC 09/05/2013 12:47 EPA 200.8

Aluminum, Al 0.0196 mg/L 0.0010 0.0003 DPC 09/05/2013 12:47 EPA 200.8

Boron, B 314 mg/L 0.20 0.040 DAM 08/29/2013 15:56 EPA 200.7

Calcium, Ca 777 mg/L 0.20 0.040 DAM 08/29/2013 15:56 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/29/2013 15:56 EPA 200.7

Magnesium, Mg 2670 mg/L 0.10 0.020 DAM 08/29/2013 15:56 EPA 200.7

Manganese, Mn 36.1 mg/L 0.0050 0.0010 DAM 08/29/2013 15:56 EPA 200.7

Potassium, K 52.1 mg/L 0.50 0.070 DAM 08/29/2013 15:54 EPA 200.7

Sodium, Na 255 mg/L 0.30 0.080 DAM 08/29/2013 15:54 EPA 200.7

Strontium, Sr 5.89 mg/L 0.010 0.0030 DAM 08/29/2013 15:54 EPA 200.7

Mountaineer Plant, 133429 Page 4 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-003 Date Collected: 08/21/2013 Date Received: 8/21/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.8 ug/L 0.050 0.010 DPC 09/05/2013 12:52 EPA 200.8

Arsenic, As 44.8 ug/L 0.10 0.030 DPC 09/05/2013 12:52 EPA 200.8

Barium, Ba 29.4 ug/L 0.10 0.020 DPC 09/05/2013 12:52 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:05 EPA 200.7

Cadmium, Cd 1.88 ug/L 0.050 0.010 DPC 09/05/2013 12:52 EPA 200.8

Chromium, Cr 0.4 ug/L 0.20 0.040 DPC EPA 200.8

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

09/05/2013 12:52

Cobalt, Co 1.73 ug/L 0.020 0.0040 DPC 09/05/2013 12:52 EPA 200.8

Copper, Cu 0.66 ug/L 0.050 0.010 DPC 09/05/2013 12:52 EPA 200.8

Lead, Pb 0.041 ug/L 0.010 0.0020 DPC 09/05/2013 12:52 EPA 200.8

Mercury, Hg 46.6 ng/L 10 4.0 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 7550 ug/L 0.050 0.010 DPC 09/05/2013 12:52 EPA 200.8

Nickel, Ni 8.14 ug/L 0.20 0.050 DPC 09/05/2013 12:52 EPA 200.8

Selenium, Se 249 ug/L 0.50 0.20 DPC 09/05/2013 12:52 EPA 200.8

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 09/05/2013 12:52 EPA 200.8

Thallium, Tl 3.00 ug/L 0.050 0.0020 DPC 09/05/2013 12:52 EPA 200.8

Tin, Sn 196 ug/L 100 30 DAM 08/29/2013 16:05 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 16:05 EPA 200.7

Zinc, Zn 2.6 ug/L 0.50 0.10 DPC 09/05/2013 12:52 EPA 200.8

Aluminum, Al 0.0211 mg/L 0.0010 0.0003 DPC 09/05/2013 12:52 EPA 200.8

Boron, B 59.3 mg/L 0.20 0.040 DAM 08/29/2013 16:05 EPA 200.7

Calcium, Ca 492 mg/L 0.20 0.040 DAM 08/29/2013 16:05 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/29/2013 16:05 EPA 200.7

Magnesium, Mg 456 mg/L 0.10 0.020 DAM 08/29/2013 16:05 EPA 200.7

Manganese, Mn 0.718 mg/L 0.0050 0.0010 DAM 08/29/2013 16:05 EPA 200.7

Potassium, K 121 mg/L 0.50 0.070 DAM 08/29/2013 16:03 EPA 200.7

Sodium, Na 2010 mg/L 0.30 0.080 DAM 08/29/2013 16:03 EPA 200.7

Strontium, Sr 6.26 mg/L 0.010 0.0030 DAM 08/29/2013 16:03 EPA 200.7

Ammonia, NH3, as N 3.39 mg/L 0.050 0.020 DMM 08/26/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.18 mg/L 0.50 0.10 DMM 08/28/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 4.14 mg/L 0.10 0.020 DMM 08/27/2013 SM20 4500NO3 H

Mountaineer Plant, 133429 Page 5 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-003A Date Collected: 08/21/2013 Date Received: 8/21/2013

Landfill Leachate Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.2 ug/L 0.050 0.010 DPC 09/06/2013 10:27 EPA 200.8

Arsenic, As 41.6 ug/L 0.10 0.030 DPC 09/06/2013 10:27 EPA 200.8

Barium, Ba 27.6 ug/L 0.10 0.020 DPC 09/06/2013 10:27 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:09 EPA 200.7

Cadmium, Cd 2.11 ug/L 0.050 0.010 DPC 09/06/2013 10:27 EPA 200.8

Chromium, Cr 0.6 ug/L 0.20 0.040 DPC EPA 200.8

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

09/06/2013 10:27

Cobalt, Co 1.45 ug/L 0.020 0.0040 DPC 09/06/2013 10:27 EPA 200.8

Copper, Cu 0.45 ug/L 0.050 0.010 DPC 09/06/2013 10:27 EPA 200.8

Lead, Pb 0.012 ug/L 0.010 0.0020 DPC 09/06/2013 10:27 EPA 200.8

Mercury, Hg 13.3 ng/L 2.0 0.80 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 7030 ug/L 0.050 0.010 DPC 09/06/2013 10:27 EPA 200.8

Nickel, Ni 7.10 ug/L 0.20 0.050 DPC 09/06/2013 10:27 EPA 200.8

Selenium, Se 229 ug/L 0.50 0.20 DPC 09/06/2013 10:27 EPA 200.8

Selenite, Se+4 (Hydride) 146 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag 0.0040 ug/L J 0.010 0.0020 DPC 09/06/2013 10:27 EPA 200.8

Thallium, Tl 2.77 ug/L 0.050 0.0020 DPC 09/06/2013 10:27 EPA 200.8

Tin, Sn 155 ug/L 100 30 DAM 08/29/2013 16:09 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 16:09 EPA 200.7

Zinc, Zn 2.7 ug/L 0.50 0.10 DPC 09/06/2013 10:27 EPA 200.8

Aluminum, Al 0.0075 mg/L 0.0010 0.0003 DPC 09/06/2013 10:27 EPA 200.8

Boron, B 58.7 mg/L 0.20 0.040 DAM 08/29/2013 16:09 EPA 200.7

Calcium, Ca 486 mg/L 0.20 0.040 DAM 08/29/2013 16:09 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/29/2013 16:09 EPA 200.7

Magnesium, Mg 451 mg/L 0.10 0.020 DAM 08/29/2013 16:09 EPA 200.7

Manganese, Mn 0.663 mg/L 0.0050 0.0010 DAM 08/29/2013 16:09 EPA 200.7

Potassium, K 124 mg/L 0.50 0.070 DAM 08/29/2013 16:07 EPA 200.7

Sodium, Na 2050 mg/L 0.30 0.080 DAM 08/29/2013 16:07 EPA 200.7

Strontium, Sr 6.34 mg/L 0.010 0.0030 DAM 08/29/2013 16:07 EPA 200.7

Mountaineer Plant, 133429 Page 6 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-004 Date Collected: 08/21/2013 Date Received: 8/21/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.64 ug/L 0.050 0.010 DPC 09/06/2013 10:31 EPA 200.8

Arsenic, As 19.4 ug/L 0.10 0.030 DPC 09/06/2013 10:31 EPA 200.8

Barium, Ba 52.1 ug/L 0.10 0.020 DPC 09/06/2013 10:31 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:13 EPA 200.7

Cadmium, Cd 1.06 ug/L 0.050 0.010 DPC 09/06/2013 10:31 EPA 200.8

Chromium, Cr 2.7 ug/L 0.20 0.040 DPC 09/06/2013 10:31 EPA 200.8

Cobalt, Co 1.48 ug/L 0.020 0.0040 DPC 09/06/2013 10:31 EPA 200.8

Copper, Cu 0.74 ug/L 0.050 0.010 DPC 09/06/2013 10:31 EPA 200.8

Lead, Pb 0.132 ug/L 0.010 0.0020 DPC 09/06/2013 10:31 EPA 200.8

Mercury, Hg 115 ng/L 10 4.0 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 3340 ug/L 0.050 0.010 DPC 09/06/2013 10:31 EPA 200.8

Nickel, Ni 14.8 ug/L 0.20 0.050 DPC 09/06/2013 10:31 EPA 200.8

Selenium, Se 276 ug/L 0.50 0.20 DPC 09/06/2013 10:31 EPA 200.8

Silver, Ag 0.0040 ug/L J 0.010 0.0020 DPC 09/06/2013 10:31 EPA 200.8

Thallium, Tl 1.82 ug/L 0.050 0.0020 DPC 09/06/2013 10:31 EPA 200.8

Tin, Sn 112 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

08/29/2013 16:13

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 16:13 EPA 200.7

Zinc, Zn 3.9 ug/L 0.50 0.10 DPC 09/06/2013 10:31 EPA 200.8

Aluminum, Al 0.181 mg/L 0.0010 0.0003 DPC 09/06/2013 10:31 EPA 200.8

Boron, B 200 mg/L 0.20 0.040 DAM 08/29/2013 16:13 EPA 200.7

Calcium, Ca 656 mg/L 0.20 0.040 DAM 08/29/2013 16:13 EPA 200.7

Iron, Fe 0.34 mg/L J 0.50 0.10 DAM 08/29/2013 16:13 EPA 200.7

Magnesium, Mg 1680 mg/L 0.10 0.020 DAM 08/29/2013 16:13 EPA 200.7

Manganese, Mn 20.3 mg/L 0.0050 0.0010 DAM 08/29/2013 16:13 EPA 200.7

Potassium, K 85.2 mg/L 0.50 0.070 DAM 08/29/2013 16:11 EPA 200.7

Sodium, Na 1080 mg/L 0.30 0.080 DAM 08/29/2013 16:11 EPA 200.7

Strontium, Sr 6.10 mg/L 0.010 0.0030 DAM 08/29/2013 16:11 EPA 200.7

Ammonia, NH3, as N 11.1 mg/L 0.050 0.020 DMM 08/26/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 2.97 mg/L 0.50 0.10 DMM 08/28/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 14.8 mg/L 0.10 0.020 DMM 08/27/2013 SM20 4500NO3 H

Mountaineer Plant, 133429 Page 7 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-004A Date Collected: 08/21/2013 Date Received: 8/21/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 4.94 ug/L 0.050 0.010 DPC 09/06/2013 10:36 EPA 200.8

Arsenic, As 15.4 ug/L 0.10 0.030 DPC 09/06/2013 10:36 EPA 200.8

Barium, Ba 43.9 ug/L 0.10 0.020 DPC 09/06/2013 10:36 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:22 EPA 200.7

Cadmium, Cd 0.86 ug/L 0.050 0.010 DPC 09/06/2013 10:36 EPA 200.8

Chromium, Cr 1.7 ug/L 0.20 0.040 DPC 09/06/2013 10:36 EPA 200.8

Cobalt, Co 0.680 ug/L 0.020 0.0040 DPC 09/06/2013 10:36 EPA 200.8

Copper, Cu 0.39 ug/L 0.050 0.010 DPC 09/06/2013 10:36 EPA 200.8

Lead, Pb 0.034 ug/L 0.010 0.0020 DPC 09/06/2013 10:36 EPA 200.8

Mercury, Hg 5.0 ng/L 2.0 0.80 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 2880 ug/L 0.050 0.010 DPC 09/06/2013 10:36 EPA 200.8

Nickel, Ni 8.78 ug/L 0.20 0.050 DPC 09/06/2013 10:36 EPA 200.8

Selenium, Se 239 ug/L 0.50 0.20 DPC 09/06/2013 10:36 EPA 200.8

Selenite, Se+4 (Hydride) 236 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 09/06/2013 10:36 EPA 200.8

Thallium, Tl 1.54 ug/L 0.050 0.0020 DPC 09/06/2013 10:36 EPA 200.8

Tin, Sn 131 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

08/29/2013 16:22

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 16:22 EPA 200.7

Zinc, Zn 2.5 ug/L 0.50 0.10 DPC 09/06/2013 10:36 EPA 200.8

Aluminum, Al 0.0173 mg/L 0.0010 0.0003 DPC 09/06/2013 10:36 EPA 200.8

Boron, B 200 mg/L 0.20 0.040 DAM 08/29/2013 16:22 EPA 200.7

Calcium, Ca 656 mg/L 0.20 0.040 DAM 08/29/2013 16:22 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/29/2013 16:22 EPA 200.7

Magnesium, Mg 1670 mg/L 0.10 0.020 DAM 08/29/2013 16:22 EPA 200.7

Manganese, Mn 20.2 mg/L 0.0050 0.0010 DAM 08/29/2013 16:22 EPA 200.7

Potassium, K 86.0 mg/L 0.50 0.070 DAM 08/29/2013 16:20 EPA 200.7

Sodium, Na 1090 mg/L 0.30 0.080 DAM 08/29/2013 16:20 EPA 200.7

Strontium, Sr 6.23 mg/L 0.010 0.0030 DAM 08/29/2013 16:20 EPA 200.7

Mountaineer Plant, 133429 Page 8 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-005 Date Collected: 08/21/2013 Date Received: 8/21/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.77 ug/L 0.050 0.010 DPC 09/06/2013 10:41 EPA 200.8

Arsenic, As 12.0 ug/L 0.10 0.030 DPC 09/06/2013 10:41 EPA 200.8

Barium, Ba 55.1 ug/L 0.10 0.020 DPC 09/06/2013 10:41 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:31 EPA 200.7

Cadmium, Cd 0.70 ug/L 0.050 0.010 DPC 09/06/2013 10:41 EPA 200.8

Chromium, Cr 1.4 ug/L 0.20 0.040 DPC 09/06/2013 10:41 EPA 200.8

Cobalt, Co 2.05 ug/L 0.020 0.0040 DPC 09/06/2013 10:41 EPA 200.8

Copper, Cu 0.19 ug/L 0.050 0.010 DPC 09/06/2013 10:41 EPA 200.8

Lead, Pb 0.011 ug/L 0.010 0.0020 DPC 09/06/2013 10:41 EPA 200.8

Mercury, Hg 7.3 ng/L J 10 4.0 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 2310 ug/L 0.050 0.010 DPC 09/06/2013 10:41 EPA 200.8

Nickel, Ni 15.6 ug/L 0.20 0.050 DPC 09/06/2013 10:41 EPA 200.8

Selenium, Se 8.7 ug/L 0.50 0.20 DPC 09/06/2013 10:41 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/06/2013 10:41 EPA 200.8

Thallium, Tl 0.93 ug/L 0.050 0.0020 DPC 09/06/2013 10:41 EPA 200.8

Tin, Sn 149 ug/L 100 30 DAM 08/29/2013 16:31 EPA 200.7

Titanium, Ti < 3.0 ug/L 20 3.0 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

U 08/29/2013 16:31

Zinc, Zn 1.1 ug/L 0.50 0.10 DPC 09/06/2013 10:41 EPA 200.8

Aluminum, Al 0.570 mg/L 0.0010 0.0003 DPC 09/06/2013 10:41 EPA 200.8

Boron, B 207 mg/L 0.20 0.040 DAM 08/29/2013 16:31 EPA 200.7

Calcium, Ca 649 mg/L 0.20 0.040 DAM 08/29/2013 16:31 EPA 200.7

Iron, Fe 0.784 mg/L 0.50 0.10 DAM 08/29/2013 16:31 EPA 200.7

Magnesium, Mg 1720 mg/L 0.10 0.020 DAM 08/29/2013 16:31 EPA 200.7

Manganese, Mn 20.5 mg/L 0.0050 0.0010 DAM 08/29/2013 16:31 EPA 200.7

Potassium, K 76.6 mg/L 0.50 0.070 DAM 08/29/2013 16:29 EPA 200.7

Sodium, Na 879 mg/L 0.30 0.080 DAM 08/29/2013 16:29 EPA 200.7

Strontium, Sr 6.13 mg/L 0.010 0.0030 DAM 08/29/2013 16:29 EPA 200.7

Ammonia, NH3, as N 10.5 mg/L 0.050 0.020 DMM 08/26/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.49 mg/L 0.50 0.10 DMM 08/28/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N < 0.020 mg/L U 0.10 0.020 DMM 08/27/2013 SM20 4500NO3 H

Mountaineer Plant, 133429 Page 9 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-005A Date Collected: 08/21/2013 Date Received: 8/21/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.62 ug/L 0.050 0.010 DPC 09/06/2013 10:46 EPA 200.8

Arsenic, As 11.2 ug/L 0.10 0.030 DPC 09/06/2013 10:46 EPA 200.8

Barium, Ba 52.6 ug/L 0.10 0.020 DPC 09/06/2013 10:46 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:40 EPA 200.7

Cadmium, Cd 0.63 ug/L 0.050 0.010 DPC 09/06/2013 10:46 EPA 200.8

Chromium, Cr 1.3 ug/L 0.20 0.040 DPC 09/06/2013 10:46 EPA 200.8

Cobalt, Co 1.97 ug/L 0.020 0.0040 DPC 09/06/2013 10:46 EPA 200.8

Copper, Cu 0.17 ug/L 0.050 0.010 DPC 09/06/2013 10:46 EPA 200.8

Lead, Pb 0.010 ug/L 0.010 0.0020 DPC 09/06/2013 10:46 EPA 200.8

Mercury, Hg 2.8 ng/L 2.0 0.80 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 2200 ug/L 0.050 0.010 DPC 09/06/2013 10:46 EPA 200.8

Nickel, Ni 15.0 ug/L 0.20 0.050 DPC 09/06/2013 10:46 EPA 200.8

Selenium, Se 4.0 ug/L 0.50 0.20 DPC 09/06/2013 10:46 EPA 200.8

Selenite, Se+4 (Hydride) < 1.0 ug/L U 5.0 1.0 TLT 09/04/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 09/06/2013 10:46 EPA 200.8

Thallium, Tl 0.86 ug/L 0.050 0.0020 DPC 09/06/2013 10:46 EPA 200.8

Tin, Sn 111 ug/L 100 30 DAM 08/29/2013 16:40 EPA 200.7

Titanium, Ti 3.1 ug/L 20 3.0 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

J 08/29/2013 16:40

Zinc, Zn 1.8 ug/L 0.50 0.10 DPC 09/06/2013 10:46 EPA 200.8

Aluminum, Al 0.537 mg/L 0.0010 0.0003 DPC 09/06/2013 10:46 EPA 200.8

Boron, B 207 mg/L 0.20 0.040 DAM 08/29/2013 16:40 EPA 200.7

Calcium, Ca 650 mg/L 0.20 0.040 DAM 08/29/2013 16:40 EPA 200.7

Iron, Fe 0.715 mg/L 0.50 0.10 DAM 08/29/2013 16:40 EPA 200.7

Magnesium, Mg 1730 mg/L 0.10 0.020 DAM 08/29/2013 16:40 EPA 200.7

Manganese, Mn 20.6 mg/L 0.0050 0.0010 DAM 08/29/2013 16:40 EPA 200.7

Potassium, K 77.0 mg/L 0.50 0.070 DAM 08/29/2013 16:38 EPA 200.7

Sodium, Na 866 mg/L 0.30 0.080 DAM 08/29/2013 16:38 EPA 200.7

Strontium, Sr 6.05 mg/L 0.010 0.0030 DAM 08/29/2013 16:38 EPA 200.7

Mountaineer Plant, 133429 Page 10 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-006 Date Collected: 08/21/2013 Date Received: 8/21/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.08 ug/L 0.050 0.010 DPC 09/06/2013 10:51 EPA 200.8

Arsenic, As 1.19 ug/L 0.10 0.030 DPC 09/06/2013 10:51 EPA 200.8

Barium, Ba 64.1 ug/L 0.10 0.020 DPC 09/06/2013 10:51 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:49 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 09/06/2013 10:51 EPA 200.8

Chromium, Cr 1.2 ug/L 0.20 0.040 DPC 09/06/2013 10:51 EPA 200.8

Cobalt, Co 0.068 ug/L 0.020 0.0040 DPC 09/06/2013 10:51 EPA 200.8

Copper, Cu 0.10 ug/L 0.050 0.010 DPC 09/06/2013 10:51 EPA 200.8

Lead, Pb 0.017 ug/L 0.010 0.0020 DPC 09/06/2013 10:51 EPA 200.8

Mercury, Hg 2.5 ng/L 1.0 0.40 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 10.1 ug/L 0.050 0.010 DPC 09/06/2013 10:51 EPA 200.8

Nickel, Ni 1.92 ug/L 0.20 0.050 DPC 09/06/2013 10:51 EPA 200.8

Selenium, Se 1.3 ug/L 0.50 0.20 DPC 09/06/2013 10:51 EPA 200.8

Silver, Ag 0.0040 ug/L J 0.010 0.0020 DPC 09/06/2013 10:51 EPA 200.8

Thallium, Tl 0.015 ug/L J 0.050 0.0020 DPC 09/06/2013 10:51 EPA 200.8

Tin, Sn 147 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

08/29/2013 16:49

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 16:49 EPA 200.7

Zinc, Zn 1.2 ug/L 0.50 0.10 DPC 09/06/2013 10:51 EPA 200.8

Aluminum, Al 2.72 mg/L 0.0010 0.0003 DPC 09/06/2013 10:51 EPA 200.8

Boron, B 229 mg/L 0.20 0.040 DAM 08/29/2013 16:49 EPA 200.7

Calcium, Ca 663 mg/L 0.20 0.040 DAM 08/29/2013 16:49 EPA 200.7

Iron, Fe 0.792 mg/L 0.50 0.10 DAM 08/29/2013 16:49 EPA 200.7

Magnesium, Mg 1770 mg/L 0.10 0.020 DAM 08/29/2013 16:49 EPA 200.7

Manganese, Mn 20.7 mg/L 0.0050 0.0010 DAM 08/29/2013 16:49 EPA 200.7

Potassium, K 83.5 mg/L 0.50 0.070 DAM 08/29/2013 00:07 EPA 200.7

Sodium, Na 900 mg/L 0.30 0.080 DAM 08/29/2013 16:47 EPA 200.7

Strontium, Sr 6.51 mg/L 0.010 0.0030 DAM 08/29/2013 16:47 EPA 200.7

Ammonia, NH3, as N 23.2 mg/L 0.050 0.020 DMM 08/26/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.15 mg/L 0.50 0.10 DMM 08/28/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N < 0.020 mg/L U 0.10 0.020 DMM 08/27/2013 SM20 4500NO3 H

Mountaineer Plant, 133429 Page 11 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

Sample Number: 133429-006A Date Collected: 08/21/2013 Date Received: 8/21/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.09 ug/L 0.050 0.010 DPC 09/06/2013 10:55 EPA 200.8

Arsenic, As 1.01 ug/L 0.10 0.030 DPC 09/06/2013 10:55 EPA 200.8

Barium, Ba 58.4 ug/L 0.10 0.020 DPC 09/06/2013 10:55 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/29/2013 16:58 EPA 200.7

Cadmium, Cd < 0.010 ug/L U 0.050 0.010 DPC 09/06/2013 10:55 EPA 200.8

Chromium, Cr 0.9 ug/L 0.20 0.040 DPC 09/06/2013 10:55 EPA 200.8

Cobalt, Co 0.074 ug/L 0.020 0.0040 DPC 09/06/2013 10:55 EPA 200.8

Copper, Cu 0.13 ug/L 0.050 0.010 DPC 09/06/2013 10:55 EPA 200.8

Lead, Pb 0.030 ug/L 0.010 0.0020 DPC 09/06/2013 10:55 EPA 200.8

Mercury, Hg 1.0 ng/L 0.50 0.20 TLT 09/03/2013 EPA 1631E

Molybdenum, Mo 7.55 ug/L 0.050 0.010 DPC 09/06/2013 10:55 EPA 200.8

Nickel, Ni 2.00 ug/L 0.20 0.050 DPC 09/06/2013 10:55 EPA 200.8

Selenium, Se 1.0 ug/L 0.50 0.20 DPC 09/06/2013 10:55 EPA 200.8

Selenite, Se+4 (Hydride) 0.084 ug/L J 0.40 0.080 TLT 09/04/2013 AEP Method

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 09/06/2013 10:55 EPA 200.8

Thallium, Tl 0.0090 ug/L J 0.050 0.0020 DPC 09/06/2013 10:55 EPA 200.8

Tin, Sn 233 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there may be a matrix interference present.

08/29/2013 16:58

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/29/2013 16:58 EPA 200.7

Zinc, Zn 1.4 ug/L 0.50 0.10 DPC 09/06/2013 10:55 EPA 200.8

Aluminum, Al 2.41 mg/L 0.0010 0.0003 DPC 09/06/2013 10:55 EPA 200.8

Boron, B 227 mg/L 0.20 0.040 DAM 08/29/2013 16:58 EPA 200.7

Calcium, Ca 658 mg/L 0.20 0.040 DAM 08/29/2013 16:58 EPA 200.7

Iron, Fe 0.759 mg/L 0.50 0.10 DAM 08/29/2013 16:58 EPA 200.7

Magnesium, Mg 1760 mg/L 0.10 0.020 DAM 08/29/2013 16:58 EPA 200.7

Manganese, Mn 20.6 mg/L 0.0050 0.0010 DAM 08/29/2013 16:58 EPA 200.7

Potassium, K 83.2 mg/L 0.50 0.070 DAM 08/29/2013 16:56 EPA 200.7

Sodium, Na 883 mg/L 0.30 0.080 DAM 08/29/2013 16:56 EPA 200.7

Strontium, Sr 6.40 mg/L 0.010 0.0030 DAM 08/29/2013 16:56 EPA 200.7

Sample Number: 133429-007 Date Collected: 08/21/2013 Date Received: 8/21/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg < 0.20 ng/L U 0.50 0.20 TLT 09/03/2013 EPA 1631E

Mountaineer Plant, 133429 Page 12 of 13
Location: Mountaineer Plant Report Date: 9/11/2013

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 133429 Page 13 of 13