# Kleinfelder, Inc.

6200 Harris Technology Blvd. Charlotte, NC 28269



# Tampa Electric Company Mulberry, FL

Client # 109381



# Analytical Report (0310-130)

EPA SW-846 Method 8270C
19 Targeted POM (PAH) Compounds SW-846 Method 8270C Target Compound List



# Enthalpy Analytical, Inc.

Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com 2202 Ellis Road Durham, NC 27703 - 5518

## I certify that to the best of my knowledge a ll analytical data presented in this report:

 Have been checked for completeness

 Are accurate, error-free, and legible

 Have been conducted in accordance with approved prot ocol, and that all deviations and analytical problems are summarized in the appropriate narrative(s)

This analytical report was prepared in Portable Document Format (.PDF) and contains  pages.

# Narrative Summary

# Enthalpy Analytical Narrative Summary

Company 

## Kleinfelder, Inc. Client # 

## 109381

Analyst 

## DDA Job # 

## 0310-130 Parameters 

## EPA SW-846 Method 8270C PO # 

## Verbal

# Samples 

## 3 Runs, 2 Blanks Report Date 

## May 5, 2010

Custody Heather Tarjeft received the samples on 4/16/10 af ter being relinquished by Kleinfelder, Inc. The samples were received at -1.3 °C and were in good condition. Prior to, during, and af ter analysis, the samples were kept under lock with access only to authorized personnel by Enthalpy Analytical, Inc.
Analysis The samples were analyzed for Polyaromatic Hydrocarbons (PAHs) by Selected Ion Monitoring (SIM) and for Semi-Volatile ICR target anlaytes by scan using the analytical procedures in EPA SW-846 Method 8270C, Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)

. All samples were analyzed in both SIM and Scan modes.
Prior to sample collection, the XAD- 2 traps were spiked with a BN Surrogate Mix that consisted of 100 μg of nitrobenzene-d 5 

## , 2-fluorobiphenyl, and terphenyl-d 14 

## . Each sample train consisted of five fractions: Filter, FH Rinse (acetone/methylene chloride), XAD- 2 Sorbent Trap, Acetone/Methylene chloride (BH) Rinse, and Condensate. The fractions were combined and labeled as follows: FH (filter, fr ont half rinse), BH (XAD-2 trap, acetone/methylene chloride BH Rinse), and COND (condensate).
Each FH, BH, COND and QC sample was spiked with 100 μg of the acid extraction surrogates (2-fluorophenol, d5-phenol, and 2,4,6- tribromophenol) and SIM PAH extr action surrogates (fluorene-d 10 

## and pyrene-d 10 

## ).

Each filter and XAD-2 fraction was Soxhlet extracted for 18 hours using the corresponding acetone/methylene chloride and fresh methylene chloride combined in the flat botto m flask. Soxhlet ex tracts were then concentrated to a final volume of 5 mL.

The Condensate fractions were se paratory funnel extracted with methylene chloride, then concentrated to a final volume of 5 mLs.

# Enthalpy Analytical Narrative Summary (continued)

Analysis

(continued) One laboratory method blank and LC S set consisting of a filter and XAD-2 and one method blank and LCS set consisting of lab reagent water were prepared with these sa mples. These laboratory QC samples were spiked in the same manner as the samples with the exception of the MB COND which was not spiked with the BN Surrogate Mix.
The water QC samples were sepa ratory funnel extracted and the Filter/XAD QC samples were soxhlet extracted. All QC samples were concentrated to final volume of 5mL.
A 100 μL aliquot of each sample extract was spiked with 40 μg/mL of SVOA internal standard spiking solution, prior to scan analyses. A 100 μL aliquot of each sample extract was spiked with 400 ng/mL of SVOA internal standard spik ing solution, pr ior to SIM.
The Agilent Technologies Model 68 90N, Gas Chromatograph ("Wiley" S/N CN10244010) was equipped with a 5973N Mass Selective Detector and a Restek Rxi-5Sil MS, 30m x 0.25mm x 0.5μm (SN 963186) capillary column.

Calibration All analytes met the 15% mean RSD initial calibration requirements. All SPCC and CCC criteria were met in the initial and continuing calibrations. All other compounds in the continuing calibration met the 50% difference in-house requirements.
Chromatographic Conditions The samples were analyzed using the acquisition me thods RXI-2A and RXISIM2A.

QC Notes All samples were prepared within ho lding times specified in the method.
All internal standard area response, retention time, and surrogate standards QC criteria were met for all samples, except RB Filter which had low 2-fluorophenol recovery. This sample was reanalyzed with confirming results, therefore, both sets of data have been included in the report.
An aliquot of the extract for sample Unit 1 Run 1 FH was spiked and all analytes exhibited rec overy values within 50% of the expected value. The PAH compounds were spiked at scan levels. The native amounts for all compounds were zero.

Benzidine did not meet QC crite ria of 50-150% recovery in LCS samples.

# Enthalpy Analytical Narrative Summary (continued)

QC Notes (continued) An aliquot of the extract for sample Unit 1 Run 1 FH was prepared as a lab duplicate for scan anal ysis and an aliquot of the extract for sample Unit 1 Run 3 FH was prepared as a lab dupl icate for SIM analysis. No compounds were detected in the scan analysis. Naphthalene, 2- methylnaphthalene and phenanthrene were the only compound detected in the SIM analysis and exhibited duplicate analysis % difference of 3.6%, 2.0% and 2.4% respectively.
Reporting Notes Reporting units are μg “Catch Weight” for all scan analyses and ng “Catch Weight” for all SIM analyses.
Due to matrix interference for sample Unit 1 Run 3 BH , results have been reported from the 2-fold analysis.
The results presented in this report are representative of the samples as provided to the laboratory.

# General Reporting Notes

The following are general reporting notes that are a pplicable to all Enthalpy Analytical, Inc. data reports, unless specifically noted otherwise.

 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot determine the presence of the analyte of interest reliably.

 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot quantitate the analyte of interest within the criteria of the method.

 The acronym ND following a value indicates a non-detect or analytical result below the MDL.

 The letter J following a value indicates an analytical r esult between the MDL and the LOQ. A J flag indicates that the laboratory can positively identify th e analyte of interest as present, but the value should be considered an estimate.

 The letter E following a value indicates an analytical r esult exceeding 100% of the highest calibration point. The associated value should be considered as an estimate.

 The acronym DF represents Dilution Factor. This number represents dilution of the sample during the preparation and/or analysis process. The analyti cal result taken from a laboratory instrument is multiplied by the DF to determine the final undiluted sample results.

 The addition of MS to the Sample ID represents a Matrix Sp ike. An aliquot of an actual sample is spiked with a known amount of analyte so that a per cent recovery value can be determined. This shows what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample matrix interferes with the analysis of the analyte(s).

 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same manner as an MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality by showing the consistency of results gained by performing the same steps multiple times.

 The addition of LD to the Sample ID represents a Laborat ory Duplicate. The analyst prepares an additional aliquot of sample for testing and the resu lts of the duplicate analysis are compared to the initial result. The result should have a difference value of within 10% of the initial result (if the results of the original analysis are greater than the LOQ).

 The addition of AD to the Sample ID represents an Alte rnate Dilution. The analyst prepares an additional aliquot at a different dilution factor (usu ally double the initial factor). This analysis helps confirm that no additional compound is present and coel uting or sharing absorbance with the analyte of interest, as they would have a different res ponse/absorbance than the analyte of interest.

 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample matrix, prepared and analyzed by the laborator y using the same reagents, spiking standards and procedures used for the client samples. The LCS is used to assess the control of the laboratory’s analytical system. Whenever spikes are prepared for our client projects, two extra spikes are prepared. The extras (randomly chosen) are labeled with the asso ciated project number and kept in-house at the appropriate temperature conditions. When the project samples are received for analysis, the LCSs are analyzed to confirm that the analyte could be recovered from the media, separate from the samples which were used on the project and which may have been affected by source matrix, sample collection and/or sample transport.

# General Reporting Notes
(continued)

 Significant Figures : Where the reported value is much greater than unity (1.00) in the units expressed, the number is rounded to a whole number of units, rather than to 3 significant figures. For example, a value of 10,456.45 ug catch is rounded to 10,456 ug. Ther e are five significant digits displayed, but no confidence should be placed on more than two significant digits.

 Manual Integration : The data systems used for processing w ill flag manually integrated peaks with an “M”. There are several reasons a peak may be manually integrated. These reasons will be identified by the following two letter designations. The peak was not integrated by the software “NI” , the peak

was integrated incorrectly by the software “II” or the wrong peak was integrated by the software “WP” . These codes will accompany the analyst’s ma nual integration stamp placed next to the compound name.

# Sample Custody

# ResultsSample ID: DF: 1.00 Data File: W1000703.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 U1 R1 FH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000703.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R1 FH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 337,148 40.0 N/A 136 6.76 1,160,259 40.0 N/A 164 8.53 645,045 40.0 N/A 188 10.0 1,108,934 40.0 N/A 240 12.9 1,024,218 40.0 N/A 264 15.3 865,105 40.0 N/A 112 4.41 93,888 9.99 49.9 PASS 99 5.13 160,410 14.6 72.9 PASS 330 9.32 39,049 14.4 71.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 337,148 Naphthalene-d8 (I) 1,160,259 Acenaphthene-d10 (I) 645,045 Phenanthrene-d10 (I) 1,108,934

Chrysene-d12 (I) 1,024,218 Perylene-d12 (I) 865,105

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000847.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,860 400 N/A 136 6.76 29,014 400 N/A 164 8.52 15,838 400 N/A 188 10.0 27,708 400 N/A 240 12.9 21,763 400 N/A 264 15.3 10,171 400 N/A 176 9.05 11,761 263 65.9 PASS 212 11.5 16,878 291 72.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.25 8,548 Pass Compound 0310-130 U1 R1 FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,860 Naphthalene-d8 (I) 29,014 Acenaphthene-d10 (I) 15,838 Phenanthrene-d10 (I) 27,708

Chrysene-d12 (I) 21,763 Perylene-d12 (I) 10,171 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000704.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags % Diff

74 NA 0.00 0.772 3.86 ND 0 94 NA 0.00 0.649 3.25 ND 0 66 NA 0.00 0.694 3.47 ND 0 63 NA 0.00 0.788 3.94 ND 0 128 NA 0.00 0.624 3.12 ND 0 146 NA 0.00 0.558 2.79 ND 0 146 NA 0.00 0.528 2.64 ND 0 108 NA 0.00 0.700 3.50 ND 0 146 NA 0.00 0.558 2.79 ND 0 107 NA 0.00 0.677 3.39 ND 0 107 NA 0.00 0.591 2.95 ND 0 70 NA 0.00 0.832 4.16 ND 0 117 NA 0.00 0.632 3.16 ND 0 77 NA 0.00 0.816 4.08 ND 0 82 NA 0.00 0.748 3.74 ND 0 107 NA 0.00 0.729 3.64 ND 0 139 NA 0.00 0.669 3.35 ND 0 93 NA 0.00 0.732 3.66 ND 0 162 NA 0.00 0.652 3.26 ND 0 180 NA 0.00 0.617 3.09 ND 0 65 NA 0.00 0.849 4.24 ND 0 225 NA 0.00 0.609 3.05 ND 0 107 NA 0.00 0.661 3.31 ND 0 142 NA 0.00 0.613 3.07 ND 0 237 NA 0.00 8.12 40.6 ND 0 196 NA 0.00 0.738 3.69 ND 0 196 NA 0.00 0.541 2.70 ND 0 162 NA 0.00 0.652 3.26 ND 0 168 NA 0.00 0.672 3.36 ND 0 163 NA 0.00 0.809 4.05 ND 0 168 NA 0.00 0.819 4.09 ND 0 165 NA 0.00 0.775 3.88 ND 0 168 NA 0.00 0.777 3.89 ND 0 184 NA 0.00 5.05 25.3 ND 0 139 NA 0.00 5.78 28.9 ND 0 165 NA 0.00 0.804 4.02 ND 0 168 NA 0.00 0.688 3.44 ND 0 232 NA 0.00 0.761 3.80 ND 0 232 NA 0.00 0.701 3.50 ND 0 149 NA 0.00 1.02 5.10 ND 0 204 NA 0.00 0.754 3.77 ND 0 198 NA 0.00 5.16 25.8 ND 0 169 NA 0.00 0.716 3.58 ND 0 77 NA 0.00 0.991 4.96 ND 0 248 NA 0.00 0.671 3.35 ND 0 284 NA 0.00 0.546 2.73 ND 0 266 NA 0.00 0.565 2.83 ND 0 167 NA 0.00 0.705 3.53 ND 0 Compound 0310-130 U1 R1 FH LD

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000704.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags % Diff Compound 0310-130 U1 R1 FH LD Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 0 184 NA 0.00 22.8 114 ND 0 149 NA 0.00 0.810 4.05 ND 0 212 NA 0.00 10.8 53.9 ND 0 149 NA 0.00 1.74 8.71 ND 0 252 NA 0.00 9.36 46.8 ND 0 149 NA 0.00 0.644 3.22 ND 0

Rec. (%) Flags 152 5.55 417,192 40.0 N/A 136 6.76 1,458,599 40.0 N/A 164 8.52 846,687 40.0 N/A 188 10.0 1,487,544 40.0 N/A 240 12.9 1,405,209 40.0 N/A 264 15.3 1,146,406 40.0 N/A 112 4.41 109,225 9.39 46.9 PASS 99 5.13 187,477 13.8 68.9 PASS 330 9.32 52,694 14.5 72.3 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 417,192 Naphthalene-d8 (I) 1,458,599 Acenaphthene-d10 (I) 846,687 Phenanthrene-d10 (I) 1,487,544

Chrysene-d12 (I) 1,405,209 Perylene-d12 (I) 1,146,406

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000705.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 0.10 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Native Amount

(ug) Spike Amount

(ug) % Rec.

74 3.43 326,383 54.2 5.42 0.00 5.00 108 94 5.15 676,163 50.3 5.03 0.00 5.00 101 66 5.24 329,313 50.0 5.00 0.00 5.00 100 63 5.26 438,448 50.0 5.00 0.00 5.00 100 128 5.36 620,643 50.1 5.01 0.00 5.00 100 146 5.51 729,139 49.2 4.92 0.00 5.00 98.4 146 5.57 746,370 49.0 4.90 0.00 5.00 98.1 108 5.63 339,693 47.2 4.72 0.00 5.00 94.3 146 5.72 694,336 49.5 4.95 0.00 5.00 99.1 107 5.70 468,856 50.4 5.04 0.00 5.00 101 107 5.84 563,585 47.4 4.74 0.00 5.00 94.9 70 5.87 378,377 46.3 4.63 0.00 5.00 92.5 117 6.04 265,731 49.9 4.99 0.00 5.00 99.7 77 6.07 595,070 49.3 4.93 0.00 5.00 98.6 82 6.28 986,619 47.9 4.79 0.00 5.00 95.8 107 6.36 579,330 47.0 4.70 0.00 5.00 94.0 139 6.38 330,359 48.0 4.80 0.00 5.00 96.0 93 6.45 592,877 46.6 4.66 0.00 5.00 93.2 162 6.60 493,460 46.7 4.67 0.00 5.00 93.3 180 6.70 614,906 49.1 4.91 0.00 5.00 98.2 128 6.79 1,825,821 49.2 4.92 0.00 5.00 98.5 65 6.80 204,907 45.1 4.51 0.00 5.00 90.2 225 6.89 369,715 48.2 4.82 0.00 5.00 96.3 107 7.24 509,033 48.7 4.87 0.00 5.00 97.3 142 7.47 1,126,019 46.1 4.61 0.00 5.00 92.3 142 7.57 1,155,526 48.6 4.86 0.00 5.00 97.2 237 7.62 404,103 51.0 5.10 0.00 5.00 102 196 7.72 372,353 47.2 4.72 0.00 5.00 94.4 196 7.77 400,532 48.7 4.87 0.00 5.00 97.3 162 7.96 1,108,848 48.6 4.86 0.00 5.00 97.2 168 8.15 187,090 48.3 4.83 0.00 5.00 96.6 163 8.18 1,255,761 48.1 4.81 0.00 5.00 96.1 168 8.23 212,919 47.9 4.79 0.00 5.00 95.8 165 8.26 298,446 47.5 4.75 0.00 5.00 95.0 168 8.33 140,112 46.0 4.60 0.00 5.00 92.0 152 8.39 1,768,659 50.1 5.01 0.00 5.00 100 154 8.56 1,140,207 48.4 4.84 0.00 5.00 96.8 184 8.54 145,791 45.0 4.50 0.00 5.00 89.9 139 8.56 221,796 45.5 4.55 0.00 5.00 91.1 165 8.67 379,212 47.6 4.76 0.00 5.00 95.1 168 8.73 1,548,549 48.1 4.81 0.00 5.00 96.3 232 8.80 335,976 47.3 4.73 0.00 5.00 94.5 232 8.84 343,906 48.1 4.81 0.00 5.00 96.1 149 8.88 1,217,399 47.2 4.72 0.00 5.00 94.4 204 9.04 642,246 47.4 4.74 0.00 5.00 94.8 166 9.08 1,282,798 48.8 4.88 0.00 5.00 97.5 198 9.09 216,029 47.9 4.79 0.00 5.00 95.8 169 9.16 1,089,838 47.7 4.77 0.00 5.00 95.4 77 9.20 1,101,960 47.8 4.78 0.00 5.00 95.7 248 9.55 401,388 49.1 4.91 0.00 5.00 98.3 284 9.66 398,775 49.6 4.96 0.00 5.00 99.2 266 9.83 237,102 49.1 4.91 0.00 5.00 98.3 178 10.1 1,778,601 48.8 4.88 0.00 5.00 97.5 178 10.1 1,781,318 50.0 5.00 0.00 5.00 100 167 10.3 1,563,653 49.5 4.95 0.00 5.00 99.0 149 10.5 2,015,226 50.8 5.08 0.00 5.00 102 202 11.3 1,929,380 51.8 5.18 0.00 5.00 104 Compound 0310-130 U1 R1 FH MS

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

Naphthalene 4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 2-Methylnaphthalene 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene Acenaphthylene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

Fluoranthene (CCC) 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) Phenanthrene 4-Chlorophenyl-phenylether Fluorene 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Anthracene Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000705.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 0.10 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Native Amount

(ug) Spike Amount

(ug) % Rec. Compound 0310-130 U1 R1 FH MS Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 2.28 ND 0.00 0.00 NA 202 11.5 2,054,919 51.5 5.15 0.00 5.00 103 149 12.1 904,833 48.3 4.83 0.00 5.00 96.6 212 NA 0.00 10.8 1.08 ND 0.00 0.00 NA 149 12.7 1,300,611 50.8 5.08 0.00 5.00 102 252 NA 0.00 9.36 0.936 ND 0.00 0.00 NA 228 12.9 1,864,727 48.5 4.85 0.00 5.00 97.0 228 13.0 1,758,171 49.0 4.90 0.00 5.00 97.9 149 13.6 2,022,274 52.0 5.20 0.00 5.00 104 252 14.6 1,724,719 49.8 4.98 0.00 5.00 99.5 252 14.6 1,671,279 49.4 4.94 0.00 5.00 98.8 252 NA 0.00 0.340 0.0340 ND 0.00 0.00 NA 252 15.2 1,550,711 49.9 4.99 0.00 5.00 99.8 252 NA 0.00 0.340 0.0340 ND 0.00 0.00 NA 276 17.4 1,335,651 45.9 4.59 0.00 5.00 91.9 278 17.4 1,100,449 45.1 4.51 0.00 5.00 90.2 276 18.1 1,030,074 45.0 4.50 0.00 5.00 90.0

Rec. (%) Flags 152 5.55 407,106 40.0 N/A 136 6.77 1,409,961 40.0 N/A 164 8.53 815,611 40.0 N/A 188 10.0 1,412,925 40.0 N/A 240 12.9 1,496,030 40.0 N/A 264 15.3 1,248,152 40.0 N/A 112 4.41 98,431 8.67 45.6 PASS 99 5.14 170,534 12.8 67.6 PASS 330 9.33 51,501 14.9 78.3 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Are a 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Pyrene

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene

2,4,6-Tribromophenol (surr) Chrysene Di-n-octylphthalate (CCC)

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC) Perylene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Internal Standard Sample Name IS Are a Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 407,106 Naphthalene-d8 (I) 1,409,961 Acenaphthene-d10 (I) 815,611 Phenanthrene-d10 (I) 1,412,925

Chrysene-d12 (I) 1,496,030 Perylene-d12 (I) 1,248,152

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000706.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound 0310-130 U1 R1 BH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000706.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R1 BH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 404,897 40.0 N/A 136 6.76 1,376,010 40.0 N/A 164 8.53 768,024 40.0 N/A 188 10.0 1,359,307 40.0 N/A 240 12.9 1,397,968 40.0 N/A 264 15.3 1,032,179 40.0 N/A 112 4.42 176,559 15.6 78.2 PASS 99 5.13 219,694 16.6 83.2 PASS 82 6.05 204,465 15.8 78.9 PASS 172 7.80 467,588 18.3 91.4 PASS 330 9.33 55,753 16.7 83.7 PASS 244 11.6 530,276 20.7 103 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 404,897 Naphthalene-d8 (I) 1,376,010 Acenaphthene-d10 (I) 768,024 Phenanthrene-d10 (I) 1,359,307

Chrysene-d12 (I) 1,397,968 Perylene-d12 (I) 1,032,179

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000848.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 8,515 122 610 142 7.46 858 19.3 96.4 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 10.1 1,030 13.7 68.3 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,393 400 N/A 136 6.76 28,595 400 N/A 164 8.52 16,014 400 N/A 188 10.0 28,929 400 N/A 240 12.9 23,689 400 N/A 264 15.2 10,984 400 N/A 176 9.04 14,414 319 79.8 PASS 212 11.5 18,938 313 78.2 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 U1 R1 BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,393 Naphthalene-d8 (I) 28,595 Acenaphthene-d10 (I) 16,014 Phenanthrene-d10 (I) 28,929

Chrysene-d12 (I) 23,689 Perylene-d12 (I) 10,984 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000707.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 U1 R1 COND

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000707.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R1 COND Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 399,253 40.0 N/A 136 6.76 1,378,930 40.0 N/A 164 8.53 755,864 40.0 N/A 188 10.0 1,302,214 40.0 N/A 240 12.9 1,241,327 40.0 N/A 264 15.3 1,005,653 40.0 N/A 112 4.41 159,029 14.3 71.4 PASS 99 5.13 166,669 12.8 64.0 PASS 330 9.32 44,781 14.0 70.2 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 399,253 Naphthalene-d8 (I) 1,378,930 Acenaphthene-d10 (I) 755,864 Phenanthrene-d10 (I) 1,302,214

Chrysene-d12 (I) 1,241,327 Perylene-d12 (I) 1,005,653

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000849.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 7,312 400 N/A 136 6.76 23,886 400 N/A 164 8.52 12,509 400 N/A 188 10.0 21,428 400 N/A 240 12.9 15,666 400 N/A 264 15.3 7,799 400 N/A 176 9.05 8,832 251 62.6 PASS 212 11.5 12,869 287 71.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.92 18,105 Pass 15.23 15.26 8,548 Pass Compound 0310-130 U1 R1 COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,312 Naphthalene-d8 (I) 23,886 Acenaphthene-d10 (I) 12,509 Phenanthrene-d10 (I) 21,428

Chrysene-d12 (I) 15,666 Perylene-d12 (I) 7,799 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000708.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 U1 R2 FH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000708.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R2 FH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 412,737 40.0 N/A 136 6.77 1,427,227 40.0 N/A 164 8.52 803,129 40.0 N/A 188 10.0 1,358,572 40.0 N/A 240 12.9 1,242,405 40.0 N/A 264 15.2 1,031,914 40.0 N/A 112 4.41 80,660 7.01 35.0 PASS 99 5.13 106,461 7.91 39.5 PASS 330 9.32 49,921 15.0 75.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 412,737 Naphthalene-d8 (I) 1,427,227 Acenaphthene-d10 (I) 803,129 Phenanthrene-d10 (I) 1,358,572

Chrysene-d12 (I) 1,242,405 Perylene-d12 (I) 1,031,914

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000850.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 4,750 69.5 347 142 7.46 3,317 76.1 380 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 10.1 1,534 20.9 104 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,509 400 N/A 136 6.76 28,036 400 N/A 164 8.52 16,090 400 N/A 188 10.0 28,166 400 N/A 240 12.9 21,555 400 N/A 264 15.2 10,947 400 N/A 176 9.05 11,012 243 60.7 PASS 212 11.5 19,280 327 81.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.25 8,548 Pass Compound 0310-130 U1 R2 FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,509 Naphthalene-d8 (I) 28,036 Acenaphthene-d10 (I) 16,090 Phenanthrene-d10 (I) 28,166

Chrysene-d12 (I) 21,555 Perylene-d12 (I) 10,947 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000709.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound 0310-130 U1 R2 BH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000709.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R2 BH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 414,570 40.0 N/A 136 6.77 1,443,874 40.0 N/A 164 8.53 817,967 40.0 N/A 188 10.0 1,448,594 40.0 N/A 240 12.9 1,342,874 40.0 N/A 264 15.2 1,116,446 40.0 N/A 112 4.41 162,975 14.1 70.5 PASS 99 5.13 209,420 15.5 77.4 PASS 82 6.05 181,744 13.7 68.5 PASS 172 7.80 447,931 16.4 82.2 PASS 330 9.32 57,259 16.1 80.7 PASS 244 11.6 510,719 18.7 93.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 414,570 Naphthalene-d8 (I) 1,443,874 Acenaphthene-d10 (I) 817,967 Phenanthrene-d10 (I) 1,448,594

Chrysene-d12 (I) 1,342,874 Perylene-d12 (I) 1,116,446

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000852.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 9,658 130 651 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 10.1 1,058 13.2 66.2 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 9,001 400 N/A 136 6.76 30,416 400 N/A 164 8.52 16,799 400 N/A 188 10.0 30,639 400 N/A 240 12.9 24,656 400 N/A 264 15.3 11,924 400 N/A 176 9.04 15,177 321 80.1 PASS 212 11.5 21,303 332 83.1 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.92 18,105 Pass 15.23 15.26 8,548 Pass Compound 0310-130 U1 R2 BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 9,001 Naphthalene-d8 (I) 30,416 Acenaphthene-d10 (I) 16,799 Phenanthrene-d10 (I) 30,639

Chrysene-d12 (I) 24,656 Perylene-d12 (I) 11,924 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000710.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 U1 R2 COND

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000710.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R2 COND Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 385,067 40.0 N/A 136 6.76 1,329,925 40.0 N/A 164 8.53 746,629 40.0 N/A 188 10.0 1,262,964 40.0 N/A 240 12.9 1,139,506 40.0 N/A 264 15.2 938,933 40.0 N/A 112 4.41 162,693 15.2 75.8 PASS 99 5.13 179,229 14.3 71.3 PASS 330 9.32 44,326 14.3 71.6 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.24 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 385,067 Naphthalene-d8 (I) 1,329,925 Acenaphthene-d10 (I) 746,629 Phenanthrene-d10 (I) 1,262,964

Chrysene-d12 (I) 1,139,506 Perylene-d12 (I) 938,933

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000853.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,702 400 N/A 136 6.76 28,256 400 N/A 164 8.52 14,809 400 N/A 188 10.0 24,804 400 N/A 240 12.9 16,000 400 N/A 264 15.3 7,794 400 N/A 176 9.05 10,583 254 63.4 PASS 212 11.5 13,870 267 66.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.93 18,105 Pass 15.23 15.27 8,548 Pass Compound 0310-130 U1 R2 COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,702 Naphthalene-d8 (I) 28,256 Acenaphthene-d10 (I) 14,809 Phenanthrene-d10 (I) 24,804

Chrysene-d12 (I) 16,000 Perylene-d12 (I) 7,794 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000711.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 U1 R3 FH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000711.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R3 FH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 416,781 40.0 N/A 136 6.76 1,464,175 40.0 N/A 164 8.53 831,607 40.0 N/A 188 10.0 1,480,046 40.0 N/A 240 12.9 1,427,855 40.0 N/A 264 15.2 1,193,862 40.0 N/A 112 4.42 173,786 15.0 74.8 PASS 99 5.13 216,254 15.9 79.5 PASS 330 9.32 54,785 15.1 75.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 416,781 Naphthalene-d8 (I) 1,464,175 Acenaphthene-d10 (I) 831,607 Phenanthrene-d10 (I) 1,480,046

Chrysene-d12 (I) 1,427,855 Perylene-d12 (I) 1,193,862

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000854.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 10,312 140 699 142 7.46 6,952 148 739 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 10.1 1,591 20.3 102 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,999 400 N/A 136 6.76 30,229 400 N/A 164 8.52 16,755 400 N/A 188 10.0 29,999 400 N/A 240 12.9 24,066 400 N/A 264 15.3 12,813 400 N/A 176 9.04 13,866 294 73.4 PASS 212 11.5 18,809 300 74.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.92 18,105 Pass 15.23 15.25 8,548 Pass Compound 0310-130 U1 R3 FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,999 Naphthalene-d8 (I) 30,229 Acenaphthene-d10 (I) 16,755 Phenanthrene-d10 (I) 29,999

Chrysene-d12 (I) 24,066 Perylene-d12 (I) 12,813 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000855.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags % Diff

128 6.78 10,260 145 725 3.6 142 7.46 6,809 151 754 2.0 152 NA 0.00 10.0 50.0 ND 0.0 154 NA 0.00 10.0 50.0 ND 0.0 166 NA 0.00 10.0 50.0 ND 0.0 178 10.1 1,518 20.8 104 2.4 178 NA 0.00 10.0 50.0 ND 0.0 202 NA 0.00 10.0 50.0 ND 0.0 202 NA 0.00 10.0 50.0 ND 0.0 228 NA 0.00 10.0 50.0 ND 0.0 228 NA 0.00 10.0 50.0 ND 0.0 252 NA 0.00 10.0 50.0 ND 0.0 252 NA 0.00 10.0 50.0 ND 0.0 252 NA 0.00 10.0 50.0 ND 0.0 252 NA 0.00 10.0 50.0 ND 0.0 252 NA 0.00 10.0 50.0 ND 0.0 276 NA 0.00 10.0 50.0 ND 0.0 278 NA 0.00 10.0 50.0 ND 0.0 276 NA 0.00 10.0 50.0 ND 0.0

Rec. (%) Flags 152 5.55 8,658 400 N/A 136 6.76 29,025 400 N/A 164 8.52 15,893 400 N/A 188 10.0 27,945 400 N/A 240 12.9 21,670 400 N/A 264 15.2 11,889 400 N/A 176 9.05 13,321 297 74.3 PASS 212 11.5 17,912 306 76.6 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.25 8,548 Pass Compound 0310-130 U1 R3 FH LD

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,658 Naphthalene-d8 (I) 29,025 Acenaphthene-d10 (I) 15,893 Phenanthrene-d10 (I) 27,945

Chrysene-d12 (I) 21,670 Perylene-d12 (I) 11,889 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 2.00 Data File: W1000921.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 3

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 7.72 ND 94 NA 0.00 0.649 6.49 ND 66 NA 0.00 0.694 6.94 ND 63 NA 0.00 0.788 7.88 ND 128 NA 0.00 0.624 6.24 ND 146 NA 0.00 0.558 5.58 ND 146 NA 0.00 0.528 5.28 ND 108 NA 0.00 0.700 7.00 ND 146 NA 0.00 0.558 5.58 ND 107 NA 0.00 0.677 6.77 ND 107 NA 0.00 0.591 5.91 ND 70 NA 0.00 0.832 8.32 ND 117 NA 0.00 0.632 6.32 ND 77 NA 0.00 0.816 8.16 ND 82 NA 0.00 0.748 7.48 ND 107 NA 0.00 0.729 7.29 ND 139 NA 0.00 0.669 6.69 ND 93 NA 0.00 0.732 7.32 ND 162 NA 0.00 0.652 6.52 ND 180 NA 0.00 0.617 6.17 ND 65 NA 0.00 0.849 8.49 ND 225 NA 0.00 0.609 6.09 ND 107 NA 0.00 0.661 6.61 ND 142 NA 0.00 0.613 6.13 ND 237 NA 0.00 8.12 81.2 ND 196 NA 0.00 0.738 7.38 ND 196 NA 0.00 0.541 5.41 ND 162 NA 0.00 0.652 6.52 ND 168 NA 0.00 0.672 6.72 ND 163 NA 0.00 0.809 8.09 ND 168 NA 0.00 0.819 8.19 ND 165 NA 0.00 0.775 7.75 ND 168 NA 0.00 0.777 7.77 ND 184 NA 0.00 5.05 50.5 ND 139 NA 0.00 5.78 57.8 ND 165 NA 0.00 0.804 8.04 ND 168 NA 0.00 0.688 6.88 ND 232 NA 0.00 0.761 7.61 ND 232 NA 0.00 0.701 7.01 ND 149 NA 0.00 1.02 10.2 ND 204 NA 0.00 0.754 7.54 ND 198 NA 0.00 5.16 51.6 ND 169 NA 0.00 0.716 7.16 ND 77 NA 0.00 0.991 9.91 ND 248 NA 0.00 0.671 6.71 ND 284 NA 0.00 0.546 5.46 ND 266 NA 0.00 0.565 5.65 ND 167 NA 0.00 0.705 7.05 ND 149 NA 0.00 1.04 10.4 ND Compound 0310-130 U1 R3 BH 2X

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 2.00 Data File: W1000921.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 3

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R3 BH 2X Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 228 ND 149 NA 0.00 0.810 8.10 ND 212 NA 0.00 10.8 108 ND 149 NA 0.00 1.74 17.4 ND 252 NA 0.00 9.36 93.6 ND 149 NA 0.00 0.644 6.44 ND

Rec. (%) Flags 152 5.54 477,177 40.0 N/A 136 6.76 1,650,012 40.0 N/A 164 8.52 933,670 40.0 N/A 188 10.0 1,678,384 40.0 N/A 240 12.9 1,460,385 40.0 N/A 264 15.2 964,147 40.0 N/A 112 4.41 87,185 6.55 65.5 PASS 99 5.13 115,613 7.43 74.3 PASS 82 6.04 110,558 7.24 72.4 PASS 172 7.79 278,200 8.94 89.4 PASS 330 9.31 35,132 8.54 85.4 PASS 244 11.6 309,492 9.78 97.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.54 5.54 358,096 Pass 6.76 6.76 1,281,171 Pass 8.52 8.52 753,346 Pass 10.03 10.03 1,381,533 Pass 12.91 12.90 1,223,151 Pass 15.25 15.22 988,673 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 477,177 Naphthalene-d8 (I) 1,650,012 Acenaphthene-d10 (I) 933,670 Phenanthrene-d10 (I) 1,678,384

Chrysene-d12 (I) 1,460,385 Perylene-d12 (I) 964,147

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 2.00 Data File: W1000859.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 4,179 65.1 651 142 NA 0.00 10.0 100 ND 152 NA 0.00 10.0 100 ND 154 NA 0.00 10.0 100 ND 166 NA 0.00 10.0 100 ND 178 NA 0.00 10.0 100 ND 178 NA 0.00 10.0 100 ND 202 NA 0.00 10.0 100 ND 202 NA 0.00 10.0 100 ND 228 NA 0.00 10.0 100 ND 228 NA 0.00 10.0 100 ND 252 NA 0.00 10.0 100 ND 252 NA 0.00 10.0 100 ND 252 NA 0.00 10.0 100 ND 252 NA 0.00 10.0 100 ND 252 NA 0.00 10.0 100 ND 276 NA 0.00 10.0 100 ND 278 NA 0.00 10.0 100 ND 276 NA 0.00 10.0 100 ND

Rec. (%) Flags 152 5.55 7,865 400 N/A 136 6.76 26,299 400 N/A 164 8.52 13,937 400 N/A 188 10.0 24,790 400 N/A 240 12.9 17,492 400 N/A 264 15.3 4,900 400 N/A 176 9.04 6,888 175 87.7 PASS 212 11.5 7,563 146 72.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.92 18,105 Pass 15.23 15.26 8,548 Pass Compound 0310-130 U1 R3 BH 2X

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,865 Naphthalene-d8 (I) 26,299 Acenaphthene-d10 (I) 13,937 Phenanthrene-d10 (I) 24,790

Chrysene-d12 (I) 17,492 Perylene-d12 (I) 4,900 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000713.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 U1 R3 COND

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000713.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 U1 R3 COND Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 421,766 40.0 N/A 136 6.76 1,477,497 40.0 N/A 164 8.53 839,776 40.0 N/A 188 10.0 1,515,849 40.0 N/A 240 12.9 1,431,810 40.0 N/A 264 15.2 1,175,332 40.0 N/A 112 4.41 172,575 14.7 73.4 PASS 99 5.13 196,907 14.3 71.6 PASS 330 9.32 51,687 13.9 69.6 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.24 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 421,766 Naphthalene-d8 (I) 1,477,497 Acenaphthene-d10 (I) 839,776 Phenanthrene-d10 (I) 1,515,849

Chrysene-d12 (I) 1,431,810 Perylene-d12 (I) 1,175,332

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000857.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,184 400 N/A 136 6.76 26,871 400 N/A 164 8.52 14,637 400 N/A 188 10.0 25,765 400 N/A 240 12.9 18,446 400 N/A 264 15.3 9,124 400 N/A 176 9.05 12,786 310 77.5 PASS 212 11.5 16,790 311 77.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.93 18,105 Pass 15.23 15.26 8,548 Pass Compound 0310-130 U1 R3 COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,184 Naphthalene-d8 (I) 26,871 Acenaphthene-d10 (I) 14,637 Phenanthrene-d10 (I) 25,765

Chrysene-d12 (I) 18,446 Perylene-d12 (I) 9,124 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000700.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 FB FH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000700.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 FB FH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 372,707 40.0 N/A 136 6.76 1,300,120 40.0 N/A 164 8.52 746,938 40.0 N/A 188 10.0 1,325,282 40.0 N/A 240 12.9 1,216,138 40.0 N/A 264 15.3 1,007,976 40.0 N/A 112 4.41 126,699 12.2 61.0 PASS 99 5.13 158,501 13.0 65.2 PASS 330 9.32 43,961 13.5 67.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 372,707 Naphthalene-d8 (I) 1,300,120 Acenaphthene-d10 (I) 746,938 Phenanthrene-d10 (I) 1,325,282

Chrysene-d12 (I) 1,216,138 Perylene-d12 (I) 1,007,976

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000844.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 7,460 400 N/A 136 6.76 23,944 400 N/A 164 8.52 12,830 400 N/A 188 10.0 21,577 400 N/A 240 12.9 16,770 400 N/A 264 15.2 7,852 400 N/A 176 9.05 9,571 265 66.2 PASS 212 11.5 14,725 326 81.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 FB FH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,460 Naphthalene-d8 (I) 23,944 Acenaphthene-d10 (I) 12,830 Phenanthrene-d10 (I) 21,577

Chrysene-d12 (I) 16,770 Perylene-d12 (I) 7,852 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000701.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound 0310-130 FB BH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000701.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 FB BH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 379,499 40.0 N/A 136 6.76 1,283,199 40.0 N/A 164 8.53 701,807 40.0 N/A 188 10.0 1,238,865 40.0 N/A 240 12.9 1,260,022 40.0 N/A 264 15.3 1,116,769 40.0 N/A 112 4.41 82,343 7.78 38.9 PASS 99 5.13 102,761 8.30 41.5 PASS 82 6.05 198,557 16.4 81.8 PASS 172 7.80 477,881 20.4 102 PASS 330 9.32 19,842 6.54 32.7 PASS 244 11.6 509,306 21.8 109 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.76 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 379,499 Naphthalene-d8 (I) 1,283,199 Acenaphthene-d10 (I) 701,807 Phenanthrene-d10 (I) 1,238,865

Chrysene-d12 (I) 1,260,022 Perylene-d12 (I) 1,116,769

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000845.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 3,258 47.0 235 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,649 400 N/A 136 6.76 28,420 400 N/A 164 8.52 15,438 400 N/A 188 10.0 25,581 400 N/A 240 12.9 19,745 400 N/A 264 15.2 9,435 400 N/A 176 9.05 12,981 298 74.6 PASS 212 11.5 16,202 303 75.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 FB BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,649 Naphthalene-d8 (I) 28,420 Acenaphthene-d10 (I) 15,438 Phenanthrene-d10 (I) 25,581

Chrysene-d12 (I) 19,745 Perylene-d12 (I) 9,435 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000702.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 FB COND

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000702.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 FB COND Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 412,914 40.0 N/A 136 6.77 1,447,154 40.0 N/A 164 8.52 793,772 40.0 N/A 188 10.0 1,353,802 40.0 N/A 240 12.9 1,232,195 40.0 N/A 264 15.3 1,048,144 40.0 N/A 112 4.41 176,707 15.3 76.7 PASS 99 5.13 210,869 15.7 78.3 PASS 330 9.32 44,761 13.5 67.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.91 1,427,833 Pass 15.27 15.25 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 412,914 Naphthalene-d8 (I) 1,447,154 Acenaphthene-d10 (I) 793,772 Phenanthrene-d10 (I) 1,353,802

Chrysene-d12 (I) 1,232,195 Perylene-d12 (I) 1,048,144

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000846.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 7,738 400 N/A 136 6.76 24,526 400 N/A 164 8.52 12,610 400 N/A 188 10.0 20,821 400 N/A 240 12.9 13,175 400 N/A 264 15.2 6,131 400 N/A 176 9.05 9,607 270 67.6 PASS 212 11.5 11,424 262 65.5 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 FB COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,738 Naphthalene-d8 (I) 24,526 Acenaphthene-d10 (I) 12,610 Phenanthrene-d10 (I) 20,821

Chrysene-d12 (I) 13,175 Perylene-d12 (I) 6,131 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000697.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 RB FILTER

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000697.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 RB FILTER Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 10.5 185,789 5.89 29.4 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 343,678 40.0 N/A 136 6.77 1,191,271 40.0 N/A 164 8.52 649,761 40.0 N/A 188 10.0 1,124,810 40.0 N/A 240 12.9 1,033,322 40.0 N/A 264 15.3 884,704 40.0 N/A 112 4.41 21,936 2.29 11.4 FAIL 99 5.13 138,962 12.4 62.0 PASS 330 9.32 41,345 15.0 75.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 343,678 Naphthalene-d8 (I) 1,191,271 Acenaphthene-d10 (I) 649,761 Phenanthrene-d10 (I) 1,124,810

Chrysene-d12 (I) 1,033,322 Perylene-d12 (I) 884,704

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000841.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 7,666 400 N/A 136 6.76 24,412 400 N/A 164 8.52 13,688 400 N/A 188 10.0 22,769 400 N/A 240 12.9 16,433 400 N/A 264 15.2 8,041 400 N/A 176 9.04 10,659 276 69.1 PASS 212 11.5 14,887 312 78.1 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 RB FILTER

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,666 Naphthalene-d8 (I) 24,412 Acenaphthene-d10 (I) 13,688 Phenanthrene-d10 (I) 22,769

Chrysene-d12 (I) 16,433 Perylene-d12 (I) 8,041 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000904.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 RB FILTER RR

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000904.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 RB FILTER RR Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 10.5 237,878 5.95 29.7 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.54 404,847 40.0 N/A 136 6.76 1,428,263 40.0 N/A 164 8.52 814,029 40.0 N/A 188 10.0 1,425,829 40.0 N/A 240 12.9 1,240,068 40.0 N/A 264 15.2 1,025,500 40.0 N/A 112 4.41 23,880 2.12 10.6 FAIL 99 5.13 149,272 11.3 56.5 PASS 330 9.31 54,626 15.6 78.2 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.54 5.54 408,357 Pass 6.76 6.76 1,410,541 Pass 8.52 8.52 845,708 Pass 10.04 10.03 1,540,126 Pass 12.91 12.89 1,379,541 Pass 15.24 15.22 1,173,932 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 404,847 Naphthalene-d8 (I) 1,428,263 Acenaphthene-d10 (I) 814,029 Phenanthrene-d10 (I) 1,425,829

Chrysene-d12 (I) 1,240,068 Perylene-d12 (I) 1,025,500

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000698.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 RB RINSE

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000698.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 RB RINSE Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 404,542 40.0 N/A 136 6.77 1,425,815 40.0 N/A 164 8.52 803,639 40.0 N/A 188 10.0 1,451,937 40.0 N/A 240 12.9 1,331,671 40.0 N/A 264 15.3 1,128,023 40.0 N/A 112 4.42 159,563 14.1 70.7 PASS 99 5.13 142,658 10.8 54.0 PASS 330 9.32 49,081 13.8 69.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 404,542 Naphthalene-d8 (I) 1,425,815 Acenaphthene-d10 (I) 803,639 Phenanthrene-d10 (I) 1,451,937

Chrysene-d12 (I) 1,331,671 Perylene-d12 (I) 1,128,023

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000842.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 9,334 400 N/A 136 6.77 30,111 400 N/A 164 8.52 16,135 400 N/A 188 10.0 28,573 400 N/A 240 12.9 21,058 400 N/A 264 15.2 9,535 400 N/A 176 9.05 10,715 236 58.9 PASS 212 11.5 16,220 271 67.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.77 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 RB RINSE

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 9,334 Naphthalene-d8 (I) 30,111 Acenaphthene-d10 (I) 16,135 Phenanthrene-d10 (I) 28,573

Chrysene-d12 (I) 21,058 Perylene-d12 (I) 9,535 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000699.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound 0310-130 RB XAD

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000699.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 RB XAD Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 372,294 40.0 N/A 136 6.77 1,275,792 40.0 N/A 164 8.52 693,778 40.0 N/A 188 10.0 1,177,451 40.0 N/A 240 12.9 1,080,727 40.0 N/A 264 15.3 907,920 40.0 N/A 112 4.41 173,084 16.7 83.4 PASS 99 5.13 216,324 17.8 89.1 PASS 82 6.05 203,560 17.1 85.5 PASS 172 7.80 443,800 19.2 96.0 PASS 330 9.32 43,461 15.1 75.3 PASS 244 11.6 423,188 19.1 95.3 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 372,294 Naphthalene-d8 (I) 1,275,792 Acenaphthene-d10 (I) 693,778 Phenanthrene-d10 (I) 1,177,451

Chrysene-d12 (I) 1,080,727 Perylene-d12 (I) 907,920

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000843.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 3,517 52.6 263 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,392 400 N/A 136 6.76 27,387 400 N/A 164 8.52 14,503 400 N/A 188 10.0 24,543 400 N/A 240 12.9 19,168 400 N/A 264 15.2 8,853 400 N/A 176 9.05 12,384 303 75.7 PASS 212 11.5 15,898 310 77.4 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.04 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound 0310-130 RB XAD

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,392 Naphthalene-d8 (I) 27,387 Acenaphthene-d10 (I) 14,503 Phenanthrene-d10 (I) 24,543

Chrysene-d12 (I) 19,168 Perylene-d12 (I) 8,853 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000695.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound 0310-130 MB FH/BH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000695.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 MB FH/BH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 342,488 40.0 N/A 136 6.77 1,190,628 40.0 N/A 164 8.53 667,880 40.0 N/A 188 10.0 1,187,416 40.0 N/A 240 12.9 1,053,908 40.0 N/A 264 15.3 871,945 40.0 N/A 112 4.41 161,285 16.9 84.4 PASS 99 5.13 205,958 18.4 92.2 PASS 82 6.05 190,984 17.4 87.1 PASS 172 7.80 418,662 18.8 94.1 PASS 330 9.32 43,712 15.0 75.1 PASS 244 11.6 421,090 18.8 94.0 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 342,488 Naphthalene-d8 (I) 1,190,628 Acenaphthene-d10 (I) 667,880 Phenanthrene-d10 (I) 1,187,416

Chrysene-d12 (I) 1,053,908 Perylene-d12 (I) 871,945

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000835.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 6.78 1,984 27.2 136 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 9,044 400 N/A 136 6.76 29,886 400 N/A 164 8.52 15,939 400 N/A 188 10.0 26,833 400 N/A 240 12.9 20,620 400 N/A 264 15.2 10,675 400 N/A 176 9.04 14,828 330 82.5 PASS 212 11.5 18,397 328 81.9 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 6,030 Pass 6.77 6.76 19,649 Pass 8.52 8.52 10,380 Pass 10.04 10.04 17,252 Pass 12.92 12.91 14,344 Pass 15.25 15.24 7,069 Pass Compound 0310-130 MB FH/BH

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 9,044 Naphthalene-d8 (I) 29,886 Acenaphthene-d10 (I) 15,939 Phenanthrene-d10 (I) 26,833

Chrysene-d12 (I) 20,620 Perylene-d12 (I) 10,675 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000696.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 167 NA 0.00 0.705 3.53 ND Compound 0310-130 MB COND

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) 4-Chlorophenyl-phenylether 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Carbazole Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000696.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound 0310-130 MB COND Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 NA 0.00 1.04 5.19 ND 184 NA 0.00 22.8 114 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 149 NA 0.00 0.644 3.22 ND

Rec. (%) Flags 152 5.55 397,614 40.0 N/A 136 6.77 1,366,044 40.0 N/A 164 8.52 762,736 40.0 N/A 188 10.0 1,329,616 40.0 N/A 240 12.9 1,201,168 40.0 N/A 264 15.3 1,018,358 40.0 N/A 112 4.41 152,082 13.7 68.6 PASS 99 5.13 161,331 12.4 62.2 PASS 330 9.32 46,332 14.2 71.1 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.52 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Di-n-butylphthalate

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine

2,4,6-Tribromophenol (surr) Di-n-octylphthalate (CCC)

Perylene-d12 (I)

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 397,614 Naphthalene-d8 (I) 1,366,044 Acenaphthene-d10 (I) 762,736 Phenanthrene-d10 (I) 1,329,616

Chrysene-d12 (I) 1,201,168 Perylene-d12 (I) 1,018,358

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000836.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 7,634 400 N/A 136 6.76 24,699 400 N/A 164 8.52 13,088 400 N/A 188 10.0 22,657 400 N/A 240 12.9 15,103 400 N/A 264 15.2 7,037 400 N/A 176 9.05 9,518 258 64.5 PASS 212 11.5 13,616 287 71.8 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 6,030 Pass 6.77 6.76 19,649 Pass 8.52 8.52 10,380 Pass 10.04 10.04 17,252 Pass 12.92 12.91 14,344 Pass 15.25 15.25 7,069 Pass Compound 0310-130 MB COND

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC)

Fluorene-d10 (surr) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene

Pyrene-d10 (surr) Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,634 Naphthalene-d8 (I) 24,699 Acenaphthene-d10 (I) 13,088 Phenanthrene-d10 (I) 22,657

Chrysene-d12 (I) 15,103 Perylene-d12 (I) 7,037 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000694.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 128 NA 0.00 0.665 3.33 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.618 3.09 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 152 NA 0.00 0.675 3.37 ND 154 NA 0.00 0.934 4.67 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 166 NA 0.00 0.783 3.92 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 178 NA 0.00 0.771 3.86 ND 178 NA 0.00 0.760 3.80 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound ch2cl2 system blank

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

Naphthalene 4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 2-Methylnaphthalene 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene Acenaphthylene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) Phenanthrene 4-Chlorophenyl-phenylether Fluorene 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Anthracene Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000694.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound ch2cl2 system blank Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

202 NA 0.00 0.919 4.60 ND 184 NA 0.00 22.8 114 ND 202 NA 0.00 0.937 4.69 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 228 NA 0.00 0.550 2.75 ND 228 NA 0.00 0.556 2.78 ND 149 NA 0.00 0.644 3.22 ND 252 NA 0.00 0.300 1.50 ND 252 NA 0.00 0.356 1.78 ND 252 NA 0.00 0.340 1.70 ND 252 NA 0.00 0.340 1.70 ND 252 NA 0.00 0.340 1.70 ND 276 NA 0.00 0.300 1.50 ND 278 NA 0.00 0.425 2.13 ND 276 NA 0.00 0.352 1.76 ND

Rec. (%) Flags 152 5.55 424,676 40.0 N/A 136 6.77 1,477,035 40.0 N/A 164 8.53 839,683 40.0 N/A 188 10.0 1,468,828 40.0 N/A 240 12.9 1,421,901 40.0 N/A 264 15.3 1,224,708 40.0 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Are a 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Fluoranthene (CCC)

Pyrene

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene Chrysene Di-n-octylphthalate (CCC)

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC) Perylene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

1,4-Dichlorobenzene-d4 (I) 424,676 Naphthalene-d8 (I) 1,477,035 Acenaphthene-d10 (I) 839,683 Phenanthrene-d10 (I) 1,468,828

Chrysene-d12 (I) 1,421,901 Perylene-d12 (I) 1,224,708

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000900.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags

74 NA 0.00 0.772 3.86 ND 94 NA 0.00 0.649 3.25 ND 66 NA 0.00 0.694 3.47 ND 63 NA 0.00 0.788 3.94 ND 128 NA 0.00 0.624 3.12 ND 146 NA 0.00 0.558 2.79 ND 146 NA 0.00 0.528 2.64 ND 108 NA 0.00 0.700 3.50 ND 146 NA 0.00 0.558 2.79 ND 107 NA 0.00 0.677 3.39 ND 107 NA 0.00 0.591 2.95 ND 70 NA 0.00 0.832 4.16 ND 117 NA 0.00 0.632 3.16 ND 77 NA 0.00 0.816 4.08 ND 82 NA 0.00 0.748 3.74 ND 107 NA 0.00 0.729 3.64 ND 139 NA 0.00 0.669 3.35 ND 93 NA 0.00 0.732 3.66 ND 162 NA 0.00 0.652 3.26 ND 180 NA 0.00 0.617 3.09 ND 128 NA 0.00 0.665 3.33 ND 65 NA 0.00 0.849 4.24 ND 225 NA 0.00 0.609 3.05 ND 107 NA 0.00 0.661 3.31 ND 142 NA 0.00 0.618 3.09 ND 142 NA 0.00 0.613 3.07 ND 237 NA 0.00 8.12 40.6 ND 196 NA 0.00 0.738 3.69 ND 196 NA 0.00 0.541 2.70 ND 162 NA 0.00 0.652 3.26 ND 168 NA 0.00 0.672 3.36 ND 163 NA 0.00 0.809 4.05 ND 168 NA 0.00 0.819 4.09 ND 165 NA 0.00 0.775 3.88 ND 168 NA 0.00 0.777 3.89 ND 152 NA 0.00 0.675 3.37 ND 154 NA 0.00 0.934 4.67 ND 184 NA 0.00 5.05 25.3 ND 139 NA 0.00 5.78 28.9 ND 165 NA 0.00 0.804 4.02 ND 168 NA 0.00 0.688 3.44 ND 232 NA 0.00 0.761 3.80 ND 232 NA 0.00 0.701 3.50 ND 149 NA 0.00 1.02 5.10 ND 204 NA 0.00 0.754 3.77 ND 166 NA 0.00 0.783 3.92 ND 198 NA 0.00 5.16 25.8 ND 169 NA 0.00 0.716 3.58 ND 77 NA 0.00 0.991 4.96 ND 248 NA 0.00 0.671 3.35 ND 284 NA 0.00 0.546 2.73 ND 266 NA 0.00 0.565 2.83 ND 178 NA 0.00 0.771 3.86 ND 178 NA 0.00 0.760 3.80 ND 167 NA 0.00 0.705 3.53 ND 149 NA 0.00 1.04 5.19 ND Compound ch2cl2 system blank

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

Naphthalene 4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 2-Methylnaphthalene 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene Acenaphthylene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) Phenanthrene 4-Chlorophenyl-phenylether Fluorene 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Anthracene Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000900.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Compound ch2cl2 system blank Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

202 NA 0.00 0.919 4.60 ND 184 NA 0.00 22.8 114 ND 202 NA 0.00 0.937 4.69 ND 149 NA 0.00 0.810 4.05 ND 212 NA 0.00 10.8 53.9 ND 149 NA 0.00 1.74 8.71 ND 252 NA 0.00 9.36 46.8 ND 228 NA 0.00 0.550 2.75 ND 228 NA 0.00 0.556 2.78 ND 149 NA 0.00 0.644 3.22 ND 252 NA 0.00 0.300 1.50 ND 252 NA 0.00 0.356 1.78 ND 252 NA 0.00 0.340 1.70 ND 252 NA 0.00 0.340 1.70 ND 252 NA 0.00 0.340 1.70 ND 276 NA 0.00 0.300 1.50 ND 278 NA 0.00 0.425 2.13 ND 276 NA 0.00 0.352 1.76 ND

Rec. (%) Flags 152 5.54 423,823 40.0 N/A 136 6.76 1,475,587 40.0 N/A 164 8.52 838,760 40.0 N/A 188 10.0 1,418,067 40.0 N/A 240 12.9 1,171,268 40.0 N/A 264 15.2 995,224 40.0 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Are a 5.54 5.54 408,357 Pass 6.76 6.76 1,410,541 Pass 8.52 8.52 845,708 Pass 10.04 10.03 1,540,126 Pass 12.91 12.90 1,379,541 Pass 15.24 15.22 1,173,932 Pass 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Fluoranthene (CCC)

Pyrene

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene Chrysene Di-n-octylphthalate (CCC)

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC) Perylene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

1,4-Dichlorobenzene-d4 (I) 423,823 Naphthalene-d8 (I) 1,475,587 Acenaphthene-d10 (I) 838,760 Phenanthrene-d10 (I) 1,418,067

Chrysene-d12 (I) 1,171,268 Perylene-d12 (I) 995,224

0310-130 scan summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000816.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 1.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 10.0 ND 142 NA 0.00 10.0 10.0 ND 152 NA 0.00 10.0 10.0 ND 154 NA 0.00 10.0 10.0 ND 166 NA 0.00 10.0 10.0 ND 178 NA 0.00 10.0 10.0 ND 178 NA 0.00 10.0 10.0 ND 202 NA 0.00 10.0 10.0 ND 202 NA 0.00 10.0 10.0 ND 228 NA 0.00 10.0 10.0 ND 228 NA 0.00 10.0 10.0 ND 252 NA 0.00 10.0 10.0 ND 252 NA 0.00 10.0 10.0 ND 252 NA 0.00 10.0 10.0 ND 252 NA 0.00 10.0 10.0 ND 252 NA 0.00 10.0 10.0 ND 276 NA 0.00 10.0 10.0 ND 278 NA 0.00 10.0 10.0 ND 276 NA 0.00 10.0 10.0 ND

Rec. (%) Flags 152 5.55 7,364 400 N/A 136 6.76 23,705 400 N/A 164 8.53 12,593 400 N/A 188 10.1 20,731 400 N/A 240 12.9 14,294 400 N/A 264 15.3 6,344 400 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 6,030 Pass 6.77 6.76 19,649 Pass 8.52 8.53 10,380 Pass 10.04 10.05 17,252 Pass 12.92 12.92 14,344 Pass 15.25 15.26 7,069 Pass Compound ch2cl2 system blank

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 7,364 Naphthalene-d8 (I) 23,705 Acenaphthene-d10 (I) 12,593 Phenanthrene-d10 (I) 20,731

Chrysene-d12 (I) 14,294 Perylene-d12 (I) 6,344 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010

### Sample ID: DF: 1.00 Data File: W1000840.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ng/mL) Catch Weight

(ng) Flags

128 NA 0.00 10.0 50.0 ND 142 NA 0.00 10.0 50.0 ND 152 NA 0.00 10.0 50.0 ND 154 NA 0.00 10.0 50.0 ND 166 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 178 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 202 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 228 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 252 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND 278 NA 0.00 10.0 50.0 ND 276 NA 0.00 10.0 50.0 ND

Rec. (%) Flags 152 5.55 8,180 400 N/A 136 6.76 26,324 400 N/A 164 8.52 14,110 400 N/A 188 10.0 22,781 400 N/A 240 12.9 15,899 400 N/A 264 15.2 7,331 400 N/A

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 7,952 Pass 6.76 6.76 26,177 Pass 8.52 8.52 13,968 Pass 10.04 10.05 23,008 Pass 12.90 12.91 18,105 Pass 15.23 15.24 8,548 Pass Compound ch2cl2 system blank

gcmsprep1pg186

1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Naphthalene 2-Methylnaphthalene

Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Acenaphthene-d10 (I) Acenaphthylene Acenaphthene (CCC) Fluorene

Phenanthrene-d10 (I) Phenanthrene Anthracene Fluoranthene (CCC)

Perylene Pyrene

Chrysene-d12 (I) Benzo(a)anthracene Chrysene

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC)

Internal Standard Sample Name IS Area 1,4-Dichlorobenzene-d4 (I) 8,180 Naphthalene-d8 (I) 26,324 Acenaphthene-d10 (I) 14,110 Phenanthrene-d10 (I) 22,781

Chrysene-d12 (I) 15,899 Perylene-d12 (I) 7,331 Company

Analyst Parameters # Samples Kleinfelder, Inc. DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 sim summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000692.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Tag Value % Diff. From Tag %Rec

74 3.43 127,857 19.7 98.4 100 1.6 98.4 94 5.15 275,962 19.0 95.0 100 5.0 95.0 66 5.24 129,636 18.2 91.1 100 8.9 91.1 63 5.25 174,122 18.4 92.0 100 8.0 92.0 128 5.36 251,480 18.8 94.0 100 6.0 94.0 146 5.51 293,849 18.4 91.8 100 8.2 91.8 146 5.57 304,163 18.5 92.5 100 7.5 92.5 108 5.63 148,174 19.0 95.2 100 4.8 95.2 146 5.71 282,402 18.7 93.3 100 6.7 93.3 107 5.70 195,301 19.4 97.2 100 2.8 97.2 107 5.83 248,243 19.3 96.7 100 3.3 96.7 70 5.86 163,261 18.5 92.4 100 7.6 92.4 117 6.04 104,939 18.2 91.1 100 8.9 91.1 77 6.07 249,614 19.1 95.7 100 4.3 95.7 82 6.28 421,153 18.8 93.8 100 6.2 93.8 107 6.35 255,759 19.1 95.3 100 4.7 95.3 139 6.37 148,379 19.8 98.9 100 1.1 98.9 93 6.44 256,671 18.5 92.6 100 7.4 92.6 162 6.60 220,597 19.1 95.7 100 4.3 95.7 180 6.70 263,426 19.3 96.5 100 3.5 96.5 128 6.79 787,947 19.5 97.5 100 2.5 97.5 65 6.80 89,485 18.1 90.4 100 9.6 90.4 225 6.88 157,266 18.8 94.1 100 5.9 94.1 107 7.23 218,502 19.2 95.9 100 4.1 95.9 142 7.46 497,095 18.7 93.5 100 6.5 93.5 142 7.57 512,223 19.8 98.8 100 1.2 98.8 237 7.62 158,143 18.3 91.5 100 8.5 91.5 196 7.72 169,905 19.7 98.6 100 1.4 98.6 196 7.76 177,696 19.8 98.8 100 1.2 98.8 162 7.96 497,050 19.9 99.7 100 0.3 99.7 168 8.15 82,679 19.5 97.6 100 2.4 97.6 163 8.17 573,338 20.1 100 100 0.4 100 168 8.23 95,328 19.6 98.1 100 1.9 98.1 165 8.25 136,188 19.8 99.1 100 0.9 99.1 168 8.32 64,201 19.3 96.4 100 3.6 96.4 152 8.39 792,756 20.6 103 100 2.8 103 154 8.56 500,293 19.4 97.2 100 2.8 97.2 184 8.54 54,941 15.5 77.5 100 22.5 77.5 139 8.56 98,415 18.5 92.4 100 7.6 92.4 165 8.66 172,732 19.8 99.1 100 0.9 99.1 168 8.73 702,072 20.0 99.9 100 0.1 99.9 232 8.79 148,491 19.1 95.5 100 4.5 95.5 232 8.84 151,868 19.4 97.1 100 2.9 97.1 149 8.87 559,238 19.8 99.2 100 0.8 99.2 204 9.04 294,461 19.9 99.4 100 0.6 99.4 166 9.08 577,887 20.1 101 100 0.5 101 198 9.09 91,821 18.6 93.1 100 6.9 93.1 169 9.15 505,629 20.2 101 100 1.2 101 77 9.20 475,886 18.9 94.5 100 5.5 94.5 248 9.54 184,636 19.9 99.4 100 0.6 99.4 284 9.65 182,678 20.0 100 100 0.0 100 266 9.83 102,953 18.8 93.9 100 6.1 93.9 178 10.1 830,080 20.0 100 100 0.1 100 178 10.1 830,403 20.5 103 100 2.6 103 167 10.3 711,806 19.8 99.2 100 0.8 99.2 149 10.5 906,502 20.1 101 100 0.6 101 202 11.3 872,641 20.6 103 100 3.1 103 184 NA 0.00 22.8 114 ND 100 13.8 0.0 202 11.5 921,459 20.3 102 100 1.7 102 Compound 0310-130 LCS FH/BH

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

Naphthalene 4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 2-Methylnaphthalene 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene Acenaphthylene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

Benzidine 2,3,4,6-Tetrachlorophenol Diethlyphthalate

Fluoranthene (CCC) 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) Phenanthrene 4-Chlorophenyl-phenylether Fluorene 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Anthracene Carbazole Di-n-butylphthalate

Pyrene Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000692.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Tag Value % Diff. From Tag %Rec Compound 0310-130 LCS FH/BH Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 12.1 383,926 19.7 98.6 100 1.4 98.6 212 12.1 398,801 16.5 82.5 100 17.5 82.5 149 12.7 526,654 19.8 99.0 100 1.0 99.0 252 12.8 226,255 19.8 98.8 100 1.2 98.8 228 12.9 794,102 19.9 99.4 100 0.6 99.4 228 13.0 757,947 20.3 102 100 1.6 102 149 13.6 809,565 20.0 100 100 0.1 100 252 14.6 697,965 19.5 97.6 100 2.4 97.6 252 14.6 720,137 20.6 103 100 3.1 103 252 15.1 640,733 19.2 96.1 100 3.9 96.1 252 15.2 641,709 20.0 100 100 0.0 100 252 15.3 648,171 19.3 96.6 100 3.4 96.6 276 17.4 593,345 19.8 98.9 100 1.1 98.9 278 17.4 488,557 19.4 97.0 100 3.0 97.0 276 18.1 471,657 20.0 99.8 100 0.2 99.8

Rec. (%) Flags 152 5.55 439,735 40.0 N/A 136 6.77 1,535,881 40.0 N/A 164 8.53 891,526 40.0 N/A 188 10.0 1,605,650 40.0 N/A 240 12.9 1,554,374 40.0 N/A 264 15.3 1,287,984 40.0 N/A 112 4.41 208,570 17.0 85.1 PASS 99 5.13 270,393 18.8 94.2 PASS 82 6.05 264,722 18.8 94.1 PASS 172 7.80 590,866 19.9 99.5 PASS 330 9.32 75,831 19.3 96.4 PASS 244 11.6 611,016 20.2 101 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I)

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene

2,4,6-Tribromophenol (surr) Chrysene Di-n-octylphthalate (CCC)

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC) Perylene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 439,735 Naphthalene-d8 (I) 1,535,881 Acenaphthene-d10 (I) 891,526 Phenanthrene-d10 (I) 1,605,650

Chrysene-d12 (I) 1,554,374 Perylene-d12 (I) 1,287,984

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000896.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Tag Value % Diff. From Tag %Rec

74 3.42 106,237 18.2 91.2 100 8.8 91.2 94 5.14 223,019 17.1 85.7 100 14.3 85.7 66 5.23 105,872 16.6 83.1 100 16.9 83.1 63 5.24 142,876 16.9 84.3 100 15.7 84.3 128 5.35 201,776 16.8 84.2 100 15.8 84.2 146 5.50 227,625 15.9 79.4 100 20.6 79.4 146 5.56 234,913 16.0 79.8 100 20.2 79.8 108 5.62 115,484 16.6 82.9 100 17.1 82.9 146 5.71 222,203 16.4 81.9 100 18.1 81.9 107 5.69 159,784 17.8 88.8 100 11.2 88.8 107 5.83 202,848 17.7 88.3 100 11.7 88.3 70 5.85 143,875 18.2 90.9 100 9.1 90.9 117 6.04 86,059 16.7 83.4 100 16.6 83.4 77 6.06 209,033 17.9 89.5 100 10.5 89.5 82 6.27 360,125 17.8 88.8 100 11.2 88.8 107 6.35 211,385 17.4 87.2 100 12.8 87.2 139 6.37 117,660 17.4 86.8 100 13.2 86.8 93 6.44 216,402 17.3 86.4 100 13.6 86.4 162 6.59 174,361 16.8 83.8 100 16.2 83.8 180 6.69 202,108 16.4 82.0 100 18.0 82.0 128 6.78 630,656 17.3 86.4 100 13.6 86.4 65 6.79 73,902 16.5 82.7 100 17.3 82.7 225 6.88 115,982 15.4 76.8 100 23.2 76.8 107 7.23 177,672 17.3 86.3 100 13.7 86.3 142 7.46 395,422 16.5 82.3 100 17.7 82.3 142 7.56 406,692 17.4 86.9 100 13.1 86.9 237 7.61 115,688 14.8 74.1 100 25.9 74.1 196 7.72 129,451 17.0 85.1 100 14.9 85.1 196 7.76 134,579 16.9 84.7 100 15.3 84.7 162 7.95 385,228 17.5 87.5 100 12.5 87.5 168 8.13 65,718 17.6 87.9 100 12.1 87.9 163 8.17 457,433 18.1 90.7 100 9.3 90.7 168 8.22 76,789 17.9 89.5 100 10.5 89.5 165 8.24 108,735 17.9 89.7 100 10.3 89.7 168 8.31 51,426 17.5 87.5 100 12.5 87.5 152 8.38 618,802 18.2 90.9 100 9.1 90.9 154 8.55 390,501 17.2 85.9 100 14.1 85.9 184 8.53 39,365 12.6 62.9 100 37.1 62.9 139 8.55 76,527 16.3 81.4 100 18.6 81.4 165 8.66 138,257 18.0 89.8 100 10.2 89.8 168 8.72 536,719 17.3 86.5 100 13.5 86.5 232 8.79 111,491 16.3 81.3 100 18.7 81.3 232 8.83 117,123 17.0 84.8 100 15.2 84.8 149 8.86 461,199 18.5 92.7 100 7.3 92.7 204 9.03 222,038 17.0 84.9 100 15.1 84.9 166 9.07 444,312 17.5 87.5 100 12.5 87.5 198 9.08 68,634 15.8 78.9 100 21.1 78.9 169 9.14 393,729 17.9 89.3 100 10.7 89.3 77 9.19 394,187 17.7 88.7 100 11.3 88.7 248 9.53 140,691 17.6 88.2 100 11.8 88.2 284 9.64 143,199 18.2 91.2 100 8.8 91.2 266 9.82 73,948 15.7 78.5 100 21.5 78.5 178 10.1 630,165 17.7 88.5 100 11.5 88.5 178 10.1 626,015 18.0 90.1 100 9.9 90.1 167 10.2 549,488 17.8 89.1 100 10.9 89.1 149 10.5 759,097 19.6 98.1 100 1.9 98.1 202 11.3 644,622 17.7 88.7 100 11.3 88.7 184 NA 0.00 22.8 114 ND 100 13.8 0.0 202 11.5 677,184 17.4 87.0 100 13.0 87.0 Compound 0310-130 LCS FH/BH RR

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

Naphthalene 4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 2-Methylnaphthalene 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene Acenaphthylene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

Benzidine 2,3,4,6-Tetrachlorophenol Diethlyphthalate

Fluoranthene (CCC) 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) Phenanthrene 4-Chlorophenyl-phenylether Fluorene 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Anthracene Carbazole Di-n-butylphthalate

Pyrene Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000896.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 2

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Tag Value % Diff. From Tag %Rec Compound 0310-130 LCS FH/BH RR Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

149 12.1 292,101 19.4 96.8 100 3.2 96.8 212 12.1 278,444 14.9 74.4 100 25.6 74.4 149 12.7 396,825 19.3 96.3 100 3.7 96.3 252 12.8 163,697 18.5 92.3 100 7.7 92.3 228 12.9 547,464 17.7 88.4 100 11.6 88.4 228 12.9 524,387 18.1 90.7 100 9.3 90.7 149 13.6 607,766 19.4 97.0 100 3.0 97.0 252 14.5 511,039 17.7 88.7 100 11.3 88.7 252 14.6 488,433 17.4 86.8 100 13.2 86.8 252 15.0 451,093 16.8 84.0 100 16.0 84.0 252 15.1 458,161 17.7 88.6 100 11.4 88.6 252 15.3 458,800 17.0 84.8 100 15.2 84.8 276 17.4 402,769 16.7 83.3 100 16.7 83.3 278 17.4 331,739 16.3 81.7 100 18.3 81.7 276 18.0 323,726 17.0 85.0 100 15.0 85.0

Rec. (%) Flags 152 5.54 393,868 40.0 N/A 136 6.76 1,387,356 40.0 N/A 164 8.52 786,932 40.0 N/A 188 10.0 1,379,461 40.0 N/A 240 12.9 1,204,274 40.0 N/A 264 15.2 1,037,776 40.0 N/A 112 4.41 162,877 14.8 74.2 PASS 99 5.13 217,140 16.9 84.5 PASS 82 6.04 217,980 17.3 86.5 PASS 172 7.79 448,262 17.1 85.5 PASS 330 9.32 57,816 17.1 85.5 PASS 244 11.6 445,651 17.1 85.7 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Area 5.54 5.54 408,357 Pass 6.76 6.76 1,410,541 Pass 8.52 8.52 845,708 Pass 10.04 10.03 1,540,126 Pass 12.91 12.89 1,379,541 Pass 15.24 15.22 1,173,932 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I)

Terphenyl-d14 (surr) Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene

2,4,6-Tribromophenol (surr) Chrysene Di-n-octylphthalate (CCC)

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC) Perylene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Internal Standard Sample Name IS Area Phenanthrene-d10 (I)

2-Fluorobiphenyl (surr) Nitrobenzene-d5 (surr) Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 393,868 Naphthalene-d8 (I) 1,387,356 Acenaphthene-d10 (I) 786,932 Phenanthrene-d10 (I) 1,379,461

Chrysene-d12 (I) 1,204,274 Perylene-d12 (I) 1,037,776

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000693.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Tag Value % Diff. From Tag %Rec

74 3.42 81,782 15.2 76.2 100 23.8 76.2 94 5.15 148,790 12.4 62.0 100 38.0 62.0 66 5.24 97,411 16.6 82.9 100 17.1 82.9 63 5.25 123,418 15.8 78.9 100 21.1 78.9 128 5.36 167,081 15.1 75.6 100 24.4 75.6 146 5.51 134,913 10.2 51.0 100 49.0 51.0 146 5.57 142,182 10.5 52.4 100 47.6 52.4 108 5.63 103,792 16.2 80.8 100 19.2 80.8 146 5.71 138,345 11.1 55.3 100 44.7 55.3 107 5.70 135,318 16.3 81.5 100 18.5 81.5 107 5.83 172,647 16.3 81.5 100 18.5 81.5 70 5.86 117,213 16.1 80.3 100 19.7 80.3 117 6.04 47,386 9.97 49.8 100 50.2 49.8 77 6.07 170,635 15.8 79.2 100 20.8 79.2 82 6.28 307,731 16.5 82.7 100 17.3 82.7 107 6.35 181,582 16.3 81.6 100 18.4 81.6 139 6.37 95,024 15.3 76.5 100 23.5 76.5 93 6.44 183,329 16.0 79.8 100 20.2 79.8 162 6.60 148,949 15.6 78.0 100 22.0 78.0 180 6.70 151,174 13.4 66.9 100 33.1 66.9 128 6.79 484,688 14.5 72.4 100 27.6 72.4 65 6.80 70,686 17.2 86.2 100 13.8 86.2 225 6.88 81,453 11.8 58.8 100 41.2 58.8 107 7.23 170,013 18.0 90.1 100 9.9 90.1 142 7.46 324,648 14.7 73.7 100 26.3 73.7 142 7.57 338,189 15.8 78.8 100 21.2 78.8 237 7.62 88,217 12.3 61.6 100 38.4 61.6 196 7.72 123,047 17.3 86.7 100 13.3 86.7 196 7.77 131,625 17.8 88.8 100 11.2 88.8 162 7.96 342,368 16.7 83.3 100 16.7 83.3 168 8.15 65,436 18.8 93.8 100 6.2 93.8 163 8.17 443,300 18.8 94.2 100 5.8 94.2 168 8.23 76,017 19.0 95.0 100 5.0 95.0 165 8.25 105,580 18.7 93.3 100 6.7 93.3 168 8.32 49,124 17.9 89.6 100 10.4 89.6 152 8.39 581,626 18.3 91.6 100 8.4 91.6 154 8.56 368,557 17.4 86.9 100 13.1 86.9 184 8.54 34,159 11.7 58.5 100 41.5 58.5 139 8.56 52,649 12.0 60.0 100 40.0 60.0 165 8.66 135,361 18.9 94.3 100 5.7 94.3 168 8.73 514,397 17.8 88.8 100 11.2 88.8 232 8.79 111,889 17.5 87.4 100 12.6 87.4 232 8.84 116,148 18.0 90.1 100 9.9 90.1 149 8.87 442,399 19.1 95.3 100 4.7 95.3 204 9.04 217,224 17.8 89.0 100 11.0 89.0 166 9.08 445,077 18.8 94.0 100 6.0 94.0 198 9.09 71,516 17.6 88.0 100 12.0 88.0 169 9.15 390,986 19.0 95.0 100 5.0 95.0 77 9.20 396,520 19.1 95.6 100 4.4 95.6 248 9.54 136,241 17.9 89.4 100 10.6 89.4 284 9.65 135,405 18.1 90.3 100 9.7 90.3 266 9.83 76,085 16.9 84.6 100 15.4 84.6 178 10.1 649,385 19.1 95.5 100 4.5 95.5 178 10.1 652,279 19.7 98.3 100 1.7 98.3 167 10.3 579,667 19.7 98.5 100 1.5 98.5 149 10.5 731,172 19.8 98.9 100 1.1 98.9 202 11.3 677,725 19.5 97.6 100 2.4 97.6 Compound 0310-130 LCS COND

3/4-Methylphenol N-Nitrso-di-n-propylamine (SPCC) Hexachloroethane

Naphthalene 4-Chloroaniline 1,2,4-Trichlorobenzene

2,3,5,6-Tetrachlorophenol Hexachlorobutadiene (CCC) 2-Methylphenol N-Nitrosodimethylamine

1,3-Dichlorobenzene 1,4-Dichlorobenzene (CCC) Benzyl alcohol 1,2-Dichlorobenzene Phenol (CCC) Aniline bis(2-Chloroethyl)ether 2-Chlorophenol

Nitrobenzene Isophorone 2,4-Dimethylphenol 2-Nitrophenol (CCC) bis(2-Chloroethoxy)methane 2,4-Dichlorophenol (CCC)

4-Chloro-3 methylphenol (CCC) 2-Methylnaphthalene 1-Methylnaphthalene Hexachlorocyclopentadiene (SPCC)

1,2-Dinitrobenzene Acenaphthylene 2-Chloronaphthalene 1,4-Dinitrobenzene 2,4,6-Trichlorophenol (CCC) 2,4,5-Trichlorophenol

Acenaphthene (CCC) 2,4-Dinitrophenol (SPCC) 4-Nitrophenol (SPCC) 2,4-Dinitrotoluene Dibenzofuran 1,3-Dinitrobenzene 2,6-Dinitrotoluene Dimethylphthalate

2,3,4,6-Tetrachlorophenol Diethlyphthalate

Fluoranthene (CCC) 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol (CCC) Phenanthrene 4-Chlorophenyl-phenylether Fluorene 4,6-Dinitro2-methylphenol N-Nitrosodiphenylamine (CCC) Azobenzene

Anthracene Carbazole Di-n-butylphthalate Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

0310-130 scan summaries 5/14/2010Sample ID: DF: 1.00 Data File: W1000693.D Aliquot Factor: 1.00 Tank/Misc ID: Extraction Vol (mL): 5.00 ConCal 1

Quant Ret. Time (min) Area Conc. (ug/mL) Catch Weight

(ug) Flags Tag Value % Diff. From Tag %Rec Compound 0310-130 LCS COND Company

Analyst Parameters # Samples Kleinfelder DDA/GLR EPA Method 8270C 3 Runs & 2 Blanks Client # Job # PO # Report Date 109381 0310-130 Verbal 5/4/2010

184 NA 0.00 22.8 114 ND 100 13.8 0.0 202 11.5 716,226 19.3 96.3 100 3.7 96.3 149 12.1 307,167 20.0 99.9 100 0.1 99.9 212 12.1 345,981 18.1 90.7 100 9.3 90.7 149 12.7 412,569 19.6 98.2 100 1.8 98.2 252 12.8 176,991 19.6 97.9 100 2.1 97.9 228 12.9 610,035 19.3 96.7 100 3.3 96.7 228 13.0 561,684 19.1 95.3 100 4.7 95.3 149 13.6 632,235 19.8 99.0 100 1.0 99.0 252 14.6 527,759 19.3 96.3 100 3.7 96.3 252 14.6 499,985 18.7 93.5 100 6.5 93.5 252 15.1 474,575 18.6 93.0 100 7.0 93.0 252 15.2 459,381 18.7 93.5 100 6.5 93.5 252 15.3 466,216 18.1 90.7 100 9.3 90.7 276 17.4 403,039 17.5 87.7 100 12.3 87.7 278 17.4 329,496 17.1 85.4 100 14.6 85.4 276 18.1 318,696 17.6 88.1 100 11.9 88.1

Rec. (%) Flags 152 5.55 363,142 40.0 N/A 136 6.77 1,272,532 40.0 N/A 164 8.53 734,393 40.0 N/A 188 10.0 1,317,276 40.0 N/A 240 12.9 1,227,045 40.0 N/A 264 15.3 986,365 40.0 N/A 112 4.41 132,505 13.1 65.4 PASS 99 5.13 147,386 12.4 62.2 PASS 330 9.32 57,708 17.9 89.4 PASS

Internal Standard Acceptance Criteria (Area -50%/+100%, RT +/- 30 sec. )

Concal Sample Concal Flag

RT RT IS Are a 5.55 5.55 424,824 Pass 6.77 6.77 1,446,379 Pass 8.53 8.53 856,584 Pass 10.04 10.04 1,512,934 Pass 12.93 12.92 1,427,833 Pass 15.27 15.26 1,183,172 Pass 2-Fluorophenol (surr) 1,4-Dichlorobenzene-d4 (I) Naphthalene-d8 (I) Acenaphthene-d10 (I) Benzidine Pyrene

Chrysene-d12 (I) Butylbenzylphthalate 3,3-Dimethylbenzidine bis(2-Ethylhexyl)phthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene

2,4,6-Tribromophenol (surr) Chrysene Di-n-octylphthalate (CCC)

Perylene-d12 (I) Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(e)pyrene Benzo(a)pyrene (CCC) Perylene Indeno(1,2,3-cd)pyrene Dibenz(a,h)anthracene Benzo(g,h,i)perylene

Internal Standard Sample Name IS Are a Phenanthrene-d10 (I)

Phenol-d5 (surr)

1,4-Dichlorobenzene-d4 (I) 363,142 Naphthalene-d8 (I) 1,272,532 Acenaphthene-d10 (I) 734,393 Phenanthrene-d10 (I) 1,317,276

Chrysene-d12 (I) 1,227,045 Perylene-d12 (I) 986,365

0310-130 scan summaries 5/14/2010

# Sample Chromatograms 6FDQ

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000703.D Vial: 14 Acq On : 23 Apr 2010 4:41 pm Operator: dda/glr Sample : 0310-130 U1 R1 FH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 12:04 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000

Time--> A bundance TIC: W1000703.DPerylene-d12 (I),IChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalatePyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000703.D W042610X-SIM-PAH.M Wed Apr 28 17:41:23 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000704.D Vial: 15 Acq On : 23 Apr 2010 5:08 pm Operator: dda/glr Sample : 0310-130 U1 R1 FH LD Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 12:27 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000 4200000

Time--> A bundance TIC: W1000704.DPerylene-d12 (I),IChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalatePyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000704.D W042610X-SIM-PAH.M Wed Apr 28 17:41:31 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000705.D Vial: 16 Acq On : 23 Apr 2010 5:35 pm Operator: dda/glr Sample : 0310-130 U1 R1 FH MS Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 12:29 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000 4200000 4400000 4600000 4800000 5000000 5200000 5400000 5600000 5800000 6000000 6200000

Time--> A bundance TIC: W1000705.DBenzo(g,h,i)peryleneDibenz(a,h)anthraceneIndeno(1,2,3-cd)pyrenePerylene-d12 (I),IPeryleneBenzo(e)pyreneBenzo(a)pyrene (CCC)Benzo(k)fluorantheneBenzo(b)fluorantheneDi-n-octylphthalate (CCC)ChryseneChrysene-d12 (I),IBenzo(a)anthracenebis(2-Ethylhexyl)phthalate3,3-Dimethylbenzidinebis(2-ethylhexyl)adipateButylbenzylphthalatePyrenePyrene-d10 (surr),SFluoranthene (CCC)Di-n-butylphthalateCarbazoleAnthracenePhenanthrenePhenanthrene-d10 (I),IPentachlorophenol (CCC)Hexachlorobenzene4-Bromophenyl-phenylether2,4,6-Tribromophenol (surr),SAzobenzeneN-Nitrosodiphenylamine (CCC)4,6-Dinitro2-methylphenolFluorene4-Nitroaniline4-Chlorophenyl-phenyletherFluorene-d10 (surr),SDiethlyphthalate2,3,4,6-Tetrachlorophenol2,3,5,6-TetrachlorophenolDibenzofuran2,4-Dinitrotoluene4-Nitrophenol (SPCC)Acenaphthene (CCC)2,4-Dinitrophenol (SPCC)Acenaphthene-d10 (I),I3-NitroanilineAcenaphthylene1,2-Dinitrobenzene2,6-Dinitrotoluene1,3-DinitrobenzeneDimethylphthalate1,4-Dinitrobenzene2-Nitroaniline2-Chloronaphthalene2,4,5-Trichlorophenol2,4,6-Trichlorophenol (CCC)Hexachlorocyclopentadiene (SPCC)1-Methylnaphthalene2-Methylnaphthalene4-Chloro-3 methylphenol (CCC)Hexachlorobutadiene (CCC)4-ChloroanilineNaphthaleneNaphthalene-d8 (I),I1,2,4-Trichlorobenzene2,4-Dichlorophenol (CCC)bis(2-Chloroethoxy)methane2-Nitrophenol (CCC)2,4-DimethylphenolBenzoic acidIsophoroneNitrobenzeneNitrobenzene-d5 (surr),SHexachloroethaneN-Nitrso-di-n-propylamine (SPCC)3/4-Methylphenolbis(2-Chloroisopropyl) ether1,2-Dichlorobenzene2-MethylphenolBenzyl alcohol1,4-Dichlorobenzene (CCC)1,4-Dichlorobenzene-d4 (I),I1,3-Dichlorobenzene2-Chlorophenolbis(2-Chloroethyl)etherAnilinePhenol (CCC)Phenol-d5 (surr),S2-Fluorophenol (surr),SPyridineN-Nitrosodimethylamine



### W1000705.D W042610X-SIM-PAH.M Wed Apr 28 17:41:41 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000706.D Vial: 17 Acq On : 23 Apr 2010 6:02 pm Operator: dda/glr Sample : 0310-130 U1 R1 BH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 28 9:00 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000000 2000000 3000000 4000000 5000000 6000000 7000000 8000000 9000000 1e+07 1.1e+07 1.2e+07 1.3e+07 1.4e+07 1.5e+07 1.6e+07

Time--> A bundance TIC: W1000706.DPerylene-d12 (I),IChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalatebis(2-ethylhexyl)adipateTerphenyl-d14 (surr),SPyrene-d10 (surr),SDi-n-butylphthalatePhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SDiethlyphthalateAcenaphthene-d10 (I),I2-Fluorobiphenyl (surr),SNaphthalene-d8 (I),IBenzoic acidNitrobenzene-d5 (surr),S1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000706.D W042610X-SIM-PAH.M Wed Apr 28 17:41:49 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000707.D Vial: 18 Acq On : 23 Apr 2010 6:29 pm Operator: dda/glr Sample : 0310-130 U1 R1 COND Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 13:46 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000

Time--> A bundance TIC: W1000707.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000707.D W042610X-SIM-PAH.M Wed Apr 28 17:41:59 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000708.D Vial: 19 Acq On : 23 Apr 2010 6:56 pm Operator: dda/glr Sample : 0310-130 U1 R2 FH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 13:51 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000

Time--> A bundance TIC: W1000708.DPerylene-d12 (I),IChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalatePyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000708.D W042610X-SIM-PAH.M Wed Apr 28 17:42:08 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000709.D Vial: 20 Acq On : 23 Apr 2010 7:22 pm Operator: dda/glr Sample : 0310-130 U1 R2 BH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 13:57 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000 4200000

Time--> A bundance TIC: W1000709.DPerylene-d12 (I),IChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalateTerphenyl-d14 (surr),SPyrene-d10 (surr),SDi-n-butylphthalatePhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SDiethlyphthalateAcenaphthene-d10 (I),I2-Fluorobiphenyl (surr),SNaphthalene-d8 (I),IBenzoic acidNitrobenzene-d5 (surr),S1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000709.D W042610X-SIM-PAH.M Wed Apr 28 17:42:17 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000710.D Vial: 21 Acq On : 23 Apr 2010 7:49 pm Operator: dda/glr Sample : 0310-130 U1 R2 COND Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 14:16 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000

Time--> A bundance TIC: W1000710.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),IBenzoic acid1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000710.D W042610X-SIM-PAH.M Wed Apr 28 17:42:27 2010 Page 3

### Quantitation Report (Not Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000711.D Vial: 22 Acq On : 23 Apr 2010 8:16 pm Operator: dda/glr Sample : 0310-130 U1 R3 FH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 14:23 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 500000 1000000 1500000 2000000 2500000 3000000 3500000 4000000 4500000 5000000 5500000 6000000 6500000 7000000 7500000 8000000 8500000 9000000

Time--> A bundance TIC: W1000711.DPeryleneBenzo(a)pyrene (CCC)Perylene-d12 (I),IChryseneBenzo(a)anthraceneChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalateButylbenzylphthalatePyrene-d10 (surr),SDi-n-butylphthalatePhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SDiethlyphthalateAcenaphthene (CCC)Acenaphthene-d10 (I),I1-Methylnaphthalene2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene (CCC)1,3-Dichlorobenzene1,4-Dichlorobenzene-d4 (I),IBenzyl alcoholPhenol (CCC)Phenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000711.D W042610X-SIM-PAH.M Wed Apr 28 17:42:36 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050410A\W1000921.D Vial: 18 Acq On : 4 May 2010 1:30 pm Operator: dda\glr Sample : 0310-130 U1 R3 BH 2X Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 4 13:52 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 22 16:55:57 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 500000 1000000 1500000 2000000 2500000 3000000 3500000 4000000 4500000 5000000 5500000 6000000 6500000 7000000 7500000 8000000 8500000 9000000 9500000 1e+07 1.05e+07

Time--> A bundance TIC: W1000921.DPerylene-d12 (I),IChrysene-d12 (I),Ibis(2-Ethylhexyl)phthalatebis(2-ethylhexyl)adipateTerphenyl-d14 (surr),SDi-n-butylphthalatePhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SAcenaphthene-d10 (I),I2-Fluorobiphenyl (surr),SNaphthalene-d8 (I),IBenzoic acidNitrobenzene-d5 (surr),S1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000921.D W042210X-8270.M Tue May 04 13:52:47 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000713.D Vial: 24 Acq On : 23 Apr 2010 9:10 pm Operator: dda/glr Sample : 0310-130 U1 R3 COND Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 14:36 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 22 16:55:57 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000 4200000 4400000

Time--> A bundance TIC: W1000713.DPerylene-d12 (I),IChrysene-d12 (I),IPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000713.D W042210X-8270.M Mon May 03 21:56:29 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000700.D Vial: 11 Acq On : 23 Apr 2010 3:20 pm Operator: dda/glr Sample : 0310-130 FB FH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 10:56 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000

Time--> A bundance TIC: W1000700.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000700.D W042610X-SIM-PAH.M Wed Apr 28 17:40:54 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000701.D Vial: 12 Acq On : 23 Apr 2010 3:47 pm Operator: dda/glr Sample : 0310-130 FB BH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 11:13 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000

Time--> A bundance TIC: W1000701.DPerylene-d12 (I),IChrysene-d12 (I),ITerphenyl-d14 (surr),SPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-Fluorobiphenyl (surr),SNaphthalene-d8 (I),INitrobenzene-d5 (surr),S1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000701.D W042610X-SIM-PAH.M Wed Apr 28 17:41:04 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000702.D Vial: 13 Acq On : 23 Apr 2010 4:14 pm Operator: dda/glr Sample : 0310-130 FB COND Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 12:00 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000

Time--> A bundance TIC: W1000702.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000702.D W042610X-SIM-PAH.M Wed Apr 28 17:41:14 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000697.D Vial: 8 Acq On : 23 Apr 2010 1:59 pm Operator: dda/glr Sample : 0310-130 RB FILTER Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 23 17:15 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000

Time--> A bundance TIC: W1000697.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SDi-n-butylphthalatePhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000697.D W042610X-SIM-PAH.M Wed Apr 28 17:40:02 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050310A\W1000904.D Vial: 13 Acq On : 3 May 2010 9:32 pm Operator: dda\glr Sample : 0310-130 RB FILTER RR Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 4 10:18 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 22 16:55:57 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000 4200000

Time--> A bundance TIC: W1000904.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SDi-n-butylphthalatePhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000904.D W042210X-8270.M Tue May 04 20:45:29 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000698.D Vial: 9 Acq On : 23 Apr 2010 2:26 pm Operator: dda/glr Sample : 0310-130 RB RINSE Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 8:26 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 500000 1000000 1500000 2000000 2500000 3000000 3500000 4000000 4500000 5000000 5500000 6000000 6500000 7000000 7500000 8000000 8500000 9000000 9500000 1e+07 1.05e+07 1.1e+07 1.15e+07 1.2e+07

Time--> A bundance TIC: W1000698.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000698.D W042610X-SIM-PAH.M Wed Apr 28 17:40:11 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000699.D Vial: 10 Acq On : 23 Apr 2010 2:53 pm Operator: dda/glr Sample : 0310-130 RB XAD Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 8:33 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000

Time--> A bundance TIC: W1000699.DPerylene-d12 (I),IChrysene-d12 (I),ITerphenyl-d14 (surr),SPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-Fluorobiphenyl (surr),SNaphthalene-d8 (I),INitrobenzene-d5 (surr),S1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000699.D W042610X-SIM-PAH.M Wed Apr 28 17:40:20 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000695.D Vial: 6 Acq On : 23 Apr 2010 1:05 pm Operator: dda/glr Sample : 0310-130 MB FH/BH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 23 17:10 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000

Time--> A bundance TIC: W1000695.DPerylene-d12 (I),IChrysene-d12 (I),ITerphenyl-d14 (surr),SPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-Fluorobiphenyl (surr),SNaphthalene-d8 (I),INitrobenzene-d5 (surr),S1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000695.D W042610X-SIM-PAH.M Wed Apr 28 17:39:45 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000696.D Vial: 7 Acq On : 23 Apr 2010 1:32 pm Operator: dda/glr Sample : 0310-130 MB COND Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 23 17:13 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000

Time--> A bundance TIC: W1000696.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),I2,4,6-Tribromophenol (surr),SFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),IPhenol-d5 (surr),S2-Fluorophenol (surr),S



### W1000696.D W042610X-SIM-PAH.M Wed Apr 28 17:39:53 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000694.D Vial: 5 Acq On : 23 Apr 2010 12:38 pm Operator: dda/glr Sample : ch2cl2 system blank Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 23 17:08 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000

Time--> A bundance TIC: W1000694.DPerylene-d12 (I),IChrysene-d12 (I),IPhenanthrene-d10 (I),IAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000694.D W042610X-SIM-PAH.M Wed Apr 28 17:39:36 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050310A\W1000900.D Vial: 9 Acq On : 3 May 2010 7:44 pm Operator: dda\glr Sample : ch3cl2 system blank Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 4 9:36 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 22 16:55:57 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000

Time--> A bundance TIC: W1000900.DPerylene-d12 (I),IChrysene-d12 (I),IPhenanthrene-d10 (I),IAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000900.D W042210X-8270.M Tue May 04 20:36:20 2010 Page 3

### Quantitation Report (Not Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000692.D Vial: 3 Acq On : 23 Apr 2010 11:44 am Operator: dda/glr Sample : 0310-130 LCS FH/BH Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 26 8:35 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000 4200000 4400000

Time--> A bundance TIC: W1000692.DBenzo(g,h,i)peryleneDibenz(a,h)anthraceneIndeno(1,2,3-cd)pyrenePerylenePerylene-d12 (I),IBenzo(a)pyrene (CCC)Benzo(e)pyreneBenzo(k)fluorantheneBenzo(b)fluorantheneDi-n-octylphthalate (CCC)ChryseneChrysene-d12 (I),IBenzo(a)anthracene3,3'-Dichlorobenzidinebis(2-Ethylhexyl)phthalate3,3-Dimethylbenzidinebis(2-ethylhexyl)adipateButylbenzylphthalateTerphenyl-d14 (surr),SPyrenePyrene-d10 (surr),SBenzidineFluoranthene (CCC)Di-n-butylphthalateCarbazoleAnthracenePhenanthrenePhenanthrene-d10 (I),IPentachlorophenol (CCC)Hexachlorobenzene4-Bromophenyl-phenylether2,4,6-Tribromophenol (surr),SAzobenzeneN-Nitrosodiphenylamine (CCC)4,6-Dinitro2-methylphenolFluorene4-NitroanilineFluorene-d10 (surr),S4-Chlorophenyl-phenyletherDiethlyphthalate2,3,4,6-Tetrachlorophenol2,3,5,6-TetrachlorophenolDibenzofuran2,4-DinitrotolueneAcenaphthene (CCC)4-Nitrophenol (SPCC)2,4-Dinitrophenol (SPCC)Acenaphthene-d10 (I),I3-NitroanilineAcenaphthylene1,2-Dinitrobenzene2,6-Dinitrotoluene1,3-DinitrobenzeneDimethylphthalate1,4-Dinitrobenzene2-Nitroaniline2-Chloronaphthalene2-Fluorobiphenyl (surr),S2,4,5-Trichlorophenol2,4,6-Trichlorophenol (CCC)Hexachlorocyclopentadiene (SPCC)1-Methylnaphthalene2-Methylnaphthalene4-Chloro-3 methylphenol (CCC)Hexachlorobutadiene (CCC)4-ChloroanilineNaphthaleneNaphthalene-d8 (I),I1,2,4-Trichlorobenzene2,4-Dichlorophenol (CCC)bis(2-Chloroethoxy)methaneBenzoic acid2-Nitrophenol (CCC)2,4-DimethylphenolIsophoroneNitrobenzeneNitrobenzene-d5 (surr),SHexachloroethaneN-Nitrso-di-n-propylamine (SPCC)3/4-Methylphenolbis(2-Chloroisopropyl) ether1,2-Dichlorobenzene2-MethylphenolBenzyl alcohol1,4-Dichlorobenzene (CCC)1,4-Dichlorobenzene-d4 (I),I1,3-Dichlorobenzene2-Chlorophenolbis(2-Chloroethyl)etherAnilinePhenol (CCC)Phenol-d5 (surr),S2-Fluorophenol (surr),SPyridineN-Nitrosodimethylamine



### W1000692.D W042610X-SIM-PAH.M Wed Apr 28 17:39:13 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\MAY10\W050310A\W1000896.D Vial: 5 Acq On : 3 May 2010 5:55 pm Operator: dda\glr Sample : 0310-130 LCS FH/BH RR Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 4 9:06 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042210X-8270.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 22 16:55:57 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000 3800000 4000000

Time--> A bundance TIC: W1000896.DBenzo(g,h,i)peryleneDibenz(a,h)anthraceneIndeno(1,2,3-cd)pyrenePerylenePerylene-d12 (I),IBenzo(a)pyrene (CCC)Benzo(e)pyreneBenzo(k)fluorantheneBenzo(b)fluorantheneDi-n-octylphthalate (CCC)ChryseneChrysene-d12 (I),IBenzo(a)anthracene3,3'-Dichlorobenzidinebis(2-Ethylhexyl)phthalate3,3-Dimethylbenzidinebis(2-ethylhexyl)adipateButylbenzylphthalateTerphenyl-d14 (surr),SPyrenePyrene-d10 (surr),SBenzidineFluoranthene (CCC)Di-n-butylphthalateCarbazoleAnthracenePhenanthrenePhenanthrene-d10 (I),IPentachlorophenol (CCC)Hexachlorobenzene4-Bromophenyl-phenylether2,4,6-Tribromophenol (surr),SAzobenzeneN-Nitrosodiphenylamine (CCC)4,6-Dinitro2-methylphenolFluorene4-Nitroaniline4-Chlorophenyl-phenyletherFluorene-d10 (surr),SDiethlyphthalate2,3,4,6-Tetrachlorophenol2,3,5,6-TetrachlorophenolDibenzofuran2,4-DinitrotolueneAcenaphthene (CCC)4-Nitrophenol (SPCC)2,4-Dinitrophenol (SPCC)Acenaphthene-d10 (I),I3-NitroanilineAcenaphthylene1,2-Dinitrobenzene2,6-Dinitrotoluene1,3-DinitrobenzeneDimethylphthalate1,4-Dinitrobenzene2-Nitroaniline2-Chloronaphthalene2-Fluorobiphenyl (surr),S2,4,5-Trichlorophenol2,4,6-Trichlorophenol (CCC)Hexachlorocyclopentadiene (SPCC)1-Methylnaphthalene2-Methylnaphthalene4-Chloro-3 methylphenol (CCC)Hexachlorobutadiene (CCC)4-ChloroanilineNaphthaleneNaphthalene-d8 (I),I1,2,4-Trichlorobenzene2,4-Dichlorophenol (CCC)bis(2-Chloroethoxy)methaneBenzoic acid2-Nitrophenol (CCC)2,4-DimethylphenolIsophoroneNitrobenzeneNitrobenzene-d5 (surr),SHexachloroethaneN-Nitrso-di-n-propylamine (SPCC)3/4-Methylphenolbis(2-Chloroisopropyl) ether1,2-Dichlorobenzene2-MethylphenolBenzyl alcohol1,4-Dichlorobenzene (CCC)1,4-Dichlorobenzene-d4 (I),I1,3-Dichlorobenzene2-Chlorophenolbis(2-Chloroethyl)etherAnilinePhenol (CCC)Phenol-d5 (surr),S2-Fluorophenol (surr),SPyridineN-Nitrosodimethylamine



### W1000896.D W042210X-8270.M Tue May 04 20:44:40 2010 Page 3

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042310A\W1000693.D Vial: 4 Acq On : 23 Apr 2010 12:11 pm Operator: dda/glr Sample : 0310-130 LCS COND Inst : Wiley Misc : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 23 17:06 2010 Quant Results File: W042210X-8270.RES
Method : M:\MS2010\METHODS\WILEY\W042610X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Mon Apr 26 15:48:30 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 200000 400000 600000 800000 1000000 1200000 1400000 1600000 1800000 2000000 2200000 2400000 2600000 2800000 3000000 3200000 3400000 3600000

Time--> A bundance TIC: W1000693.DBenzo(g,h,i)peryleneDibenz(a,h)anthraceneIndeno(1,2,3-cd)pyrenePerylenePerylene-d12 (I),IBenzo(a)pyrene (CCC)Benzo(e)pyreneBenzo(k)fluorantheneBenzo(b)fluorantheneDi-n-octylphthalate (CCC)ChryseneChrysene-d12 (I),IBenzo(a)anthracene3,3'-Dichlorobenzidinebis(2-Ethylhexyl)phthalate3,3-Dimethylbenzidinebis(2-ethylhexyl)adipateButylbenzylphthalatePyrenePyrene-d10 (surr),SBenzidineFluoranthene (CCC)Di-n-butylphthalateCarbazoleAnthracenePhenanthrenePhenanthrene-d10 (I),IPentachlorophenol (CCC)Hexachlorobenzene4-Bromophenyl-phenylether2,4,6-Tribromophenol (surr),SAzobenzeneN-Nitrosodiphenylamine (CCC)4,6-Dinitro2-methylphenolFluorene4-NitroanilineFluorene-d10 (surr),S4-Chlorophenyl-phenyletherDiethlyphthalate2,3,4,6-Tetrachlorophenol2,3,5,6-TetrachlorophenolDibenzofuran2,4-DinitrotolueneAcenaphthene (CCC)4-Nitrophenol (SPCC)2,4-Dinitrophenol (SPCC)Acenaphthene-d10 (I),I3-NitroanilineAcenaphthylene1,2-Dinitrobenzene2,6-Dinitrotoluene1,3-DinitrobenzeneDimethylphthalate1,4-Dinitrobenzene2-Nitroaniline2-Chloronaphthalene2,4,5-Trichlorophenol2,4,6-Trichlorophenol (CCC)Hexachlorocyclopentadiene (SPCC)1-Methylnaphthalene2-Methylnaphthalene4-Chloro-3 methylphenol (CCC)Hexachlorobutadiene (CCC)4-ChloroanilineNaphthaleneNaphthalene-d8 (I),I1,2,4-Trichlorobenzene2,4-Dichlorophenol (CCC)bis(2-Chloroethoxy)methane2-Nitrophenol (CCC)2,4-DimethylphenolBenzoic acidIsophoroneNitrobenzeneNitrobenzene-d5 (surr),SHexachloroethaneN-Nitrso-di-n-propylamine (SPCC)3/4-Methylphenolbis(2-Chloroisopropyl) ether1,2-Dichlorobenzene2-MethylphenolBenzyl alcohol1,4-Dichlorobenzene (CCC)1,4-Dichlorobenzene-d4 (I),I1,3-Dichlorobenzene2-Chlorophenolbis(2-Chloroethyl)etherAnilinePhenol (CCC)Phenol-d5 (surr),S2-Fluorophenol (surr),SPyridineN-Nitrosodimethylamine



### W1000693.D W042610X-SIM-PAH.M Wed Apr 28 17:39:27 2010 Page 3

# Sample Chromatograms (SIM)

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000847.D Vial: 31 Acq On : 30 Apr 2010 7:19 am Operator: dda\glr Sample : 0310-130 U1 R1 FH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:38 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000 38000

Time--> A bundance TIC: W1000847.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrenePhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000847.D W042910X-SIM-PAH.M Tue May 04 11:40:42 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000848.D Vial: 32 Acq On : 30 Apr 2010 7:46 am Operator: dda\glr Sample : 0310-130 U1 R1 BH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:41 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 10000 20000 30000 40000 50000 60000 70000 80000 90000 100000 110000 120000 130000 140000 150000 160000 170000 180000 190000 200000 210000

Time--> A bundance TIC: W1000848.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SFluoranthene (CCC)PhenanthrenePhenanthrene-d10 (I),IFluoreneFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000848.D W042910X-SIM-PAH.M Tue May 04 11:40:51 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000849.D Vial: 33 Acq On : 30 Apr 2010 8:13 am Operator: dda\glr Sample : 0310-130 U1 R1 COND Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:41 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 16000 17000 18000 19000 20000 21000 22000 23000 24000 25000 26000 27000 28000 29000

Time--> A bundance TIC: W1000849.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000849.D W042910X-SIM-PAH.M Tue May 04 11:41:03 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000850.D Vial: 34 Acq On : 30 Apr 2010 8:40 am Operator: dda\glr Sample : 0310-130 U1 R2 FH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 10:58 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000 38000

Time--> A bundance TIC: W1000850.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SFluoranthene (CCC)PhenanthrenePhenanthrene-d10 (I),IFluoreneFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000850.D W042910X-SIM-PAH.M Tue May 04 11:41:11 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000852.D Vial: 35 Acq On : 30 Apr 2010 9:34 am Operator: dda\glr Sample : 0310-130 U1 R2 BH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 11:00 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 10000 20000 30000 40000 50000 60000 70000 80000 90000 100000 110000 120000 130000 140000 150000 160000 170000 180000 190000 200000

Time--> A bundance TIC: W1000852.DPerylene-d12 (I),IBenzo(b)fluorantheneChrysene-d12 (I),IPyrene-d10 (surr),SFluoranthene (CCC)PhenanthrenePhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000852.D W042910X-SIM-PAH.M Tue May 04 11:41:31 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000853.D Vial: 36 Acq On : 30 Apr 2010 10:03 am Operator: dda\glr Sample : 0310-130 U1 R2 COND Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 11:01 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000

Time--> A bundance TIC: W1000853.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000853.D W042910X-SIM-PAH.M Tue May 04 11:41:44 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000854.D Vial: 37 Acq On : 30 Apr 2010 10:30 am Operator: dda\glr Sample : 0310-130 U1 R3 FH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 11:05 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000 38000 40000

Time--> A bundance TIC: W1000854.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SFluoranthene (CCC)PhenanthrenePhenanthrene-d10 (I),IFluoreneFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000854.D W042910X-SIM-PAH.M Tue May 04 11:41:54 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000855.D Vial: 38 Acq On : 30 Apr 2010 10:57 am Operator: dda\glr Sample : 0310-130 U1 R3 FH LD Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 11:53 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000 38000

Time--> A bundance TIC: W1000855.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SFluoranthene (CCC)PhenanthrenePhenanthrene-d10 (I),IFluoreneFluorene-d10 (surr),SAcenaphthene-d10 (I),IAcenaphthylene2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000855.D W042910X-SIM-PAH.M Tue May 04 11:42:05 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000859.D Vial: 42 Acq On : 30 Apr 2010 12:45 pm Operator: dda\glr Sample : 0310-130 U1 R3 BH 2X Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 13:15 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 5000 10000 15000 20000 25000 30000 35000 40000 45000 50000 55000 60000 65000 70000 75000 80000 85000 90000 95000 100000 105000

Time--> A bundance TIC: W1000859.DPerylene-d12 (I),IBenzo(b)fluorantheneChrysene-d12 (I),IPyrene-d10 (surr),SFluoranthene (CCC)PhenanthrenePhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),I2-MethylnaphthaleneNaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000859.D W042910X-SIM-PAH.M Tue May 04 11:42:58 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000857.D Vial: 40 Acq On : 30 Apr 2010 11:51 am Operator: dda\glr Sample : 0310-130 U1 R3 COND Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 12:31 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000

Time--> A bundance TIC: W1000857.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000857.D W042910X-SIM-PAH.M Tue May 04 11:42:38 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000844.D Vial: 27 Acq On : 30 Apr 2010 5:58 am Operator: dda\glr Sample : 0310-130 FB FH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:34 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 16000 17000 18000 19000 20000 21000 22000 23000 24000 25000 26000 27000 28000 29000 30000

Time--> A bundance TIC: W1000844.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000844.D W042910X-SIM-PAH.M Tue May 04 11:40:16 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000845.D Vial: 29 Acq On : 30 Apr 2010 6:25 am Operator: dda\glr Sample : 0310-130 FB BH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:35 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 10000 20000 30000 40000 50000 60000 70000 80000 90000 100000 110000 120000 130000 140000 150000 160000 170000 180000 190000 200000 210000

Time--> A bundance TIC: W1000845.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000845.D W042910X-SIM-PAH.M Tue May 04 11:40:26 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000846.D Vial: 30 Acq On : 30 Apr 2010 6:52 am Operator: dda\glr Sample : 0310-130 FB COND Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:37 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 16000 17000 18000 19000 20000 21000 22000 23000 24000 25000 26000 27000 28000

Time--> A bundance TIC: W1000846.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000846.D W042910X-SIM-PAH.M Tue May 04 11:40:34 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000841.D Vial: 24 Acq On : 30 Apr 2010 4:37 am Operator: dda\glr Sample : 0310-130 RB FILTER Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:30 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000 38000 40000

Time--> A bundance TIC: W1000841.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000841.D W042910X-SIM-PAH.M Tue May 04 11:39:48 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000843.D Vial: 26 Acq On : 30 Apr 2010 5:31 am Operator: dda\glr Sample : 0310-130 RB XAD Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:32 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 10000 20000 30000 40000 50000 60000 70000 80000 90000 100000 110000 120000 130000 140000 150000 160000 170000 180000 190000 200000 210000

Time--> A bundance TIC: W1000843.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000843.D W042910X-SIM-PAH.M Tue May 04 11:40:07 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000842.D Vial: 25 Acq On : 30 Apr 2010 5:04 am Operator: dda\glr Sample : 0310-130 RB RINSE Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 6:56 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 2000 4000 6000 8000 10000 12000 14000 16000 18000 20000 22000 24000 26000 28000 30000 32000 34000 36000

Time--> A bundance TIC: W1000842.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000842.D W042910X-SIM-PAH.M Tue May 04 11:39:56 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000835.D Vial: 22 Acq On : 30 Apr 2010 1:55 am Operator: dda\glr Sample : 0310-130 MB FH/BH Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 9:22 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 10000 20000 30000 40000 50000 60000 70000 80000 90000 100000 110000 120000 130000 140000 150000 160000 170000 180000 190000 200000 210000 220000 230000 240000

Time--> A bundance TIC: W1000835.DPerylene-d12 (I),IBenzo(e)pyreneBenzo(a)pyrene (CCC)ChryseneChrysene-d12 (I),IBenzo(a)anthracenePyrene-d10 (surr),SFluoranthene (CCC)Phenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthaleneNaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000835.D W042910X-SIM-PAH.M Fri Apr 30 13:22:47 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000836.D Vial: 23 Acq On : 30 Apr 2010 2:21 am Operator: dda\glr Sample : 0310-130 MB COND Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 6:56 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 16000 17000 18000 19000 20000 21000 22000 23000 24000 25000 26000 27000

Time--> A bundance TIC: W1000836.DPerylene-d12 (I),IChrysene-d12 (I),IPyrene-d10 (surr),SPhenanthrene-d10 (I),IFluorene-d10 (surr),SAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000836.D W042910X-SIM-PAH.M Fri Apr 30 13:22:53 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000816.D Vial: 3 Acq On : 29 Apr 2010 5:22 pm Operator: dda\glr Sample : ch2cl2 system blank Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 6:59 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 16000 17000 18000 19000 20000 21000

Time--> A bundance TIC: W1000816.DPerylene-d12 (I),IChrysene-d12 (I),IPhenanthrene-d10 (I),IAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000816.D W042910X-SIM-PAH.M Tue May 04 16:39:33 2010 Page 2

### Quantitation Report (QT Reviewed)
Data File : M:\MS2010Q2\WILEY\DATA\APR10\W042910A\W1000840.D Vial: 28 Acq On : 30 Apr 2010 4:10 am Operator: dda\glr Sample : ch2cl2 system blank Inst : Wiley Misc : gcmsprep1pg186 Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Apr 30 6:56 2010 Quant Results File: W042910X-SIM-PAH.RES
Method : M:\MS2010\METHODS\WILEY\W042910X-SIM-PAH.M (RTE Integrator) Title : 8270C - Full List Last Update : Thu Apr 29 15:08:49 2010 Response via : Initial Calibration

3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 13000 14000 15000 16000 17000 18000 19000 20000 21000 22000 23000

Time--> A bundance TIC: W1000840.DPerylene-d12 (I),IChrysene-d12 (I),IPhenanthrene-d10 (I),IAcenaphthene-d10 (I),INaphthalene-d8 (I),I1,4-Dichlorobenzene-d4 (I),I



### W1000840.D W042910X-SIM-PAH.M Tue May 04 11:39:39 2010 Page 2

# This Is The Last Page Of This Report.