Unit 4 Run 3 

Liquid WeighfiHRT TptarWeig'hjfeBRt: X-22 HRT 

12/18/09 12:11 PM 3241.1 11541.1 1097.6 

12/18/09 12:11 PM "3241.3 11518.3 1097.4 

12/18/09 12:11 PM 32415 11518.5 1097.5 

12/18/09 12:11 PM 32417 11495.7 1097.4 

12/18/09 12:12 PM 32418 11495.8 1097.3 

12/18/09 12:12 PM ""3241 9 "11495. 9 1097.3 

12/18/09 12:12 PM ' 3242.3 11496.3 1097.4 

12/18/09 12:12 PM 324274 11496.4 1097.4 

12/18/09 12:13PM 324274 11496.4 1097.3 

12/18/09 12:13PM 3242.3 11496.3 1097.3 

12/18/09 12:13 PM 3242.3 11496.3 1097.1 

12/18/09 12:13 PM. 3242.2 12673.2 1097.2 

12/18/09 12:14PM 3242.0 12673.0 1097.2 

12/18/09 12:14PM 32419 11914.9 1097.2 

12/18/09 12:14 PMl 32417 11914.7! 1097.0 

12/18/09 12:14 PM: 3241.6 11940.6; 1096.9 

12/18/09 12:15 PM; 324151 11940.5! 1097,0 

12/18/09 12:15 PM: 32414 11916.4! 1097.1 

12/18/09 12:15 PM: "32417 3 11919.3 1097.1 

12/1 8/09 12:15 PM! 324679 11918.9! 1097.1 

12/18/09 12:16 PM! 3240.7 11895.7j 1097.2 

12/18/09 12:16 PMl 3240.6] 11921.6! 1097.2 

12/18/09 12:16 PM: 324074 11898.4! 1097.1 

12/18/09 12:16 PMi 3240.4' 11875.4! 1097.0 

12/18/09 12:17 PMi 3240.4. 

324074 

11901.4; 1097.0 

12/18/09 12:17 PM: 

3240.4. 

324074 1 i 901.4- 1097.0 

12/18/09 12:17 PMI 3246.4! 11876.4! 1097.0 

12/18/09 12:17 PMi 3240.3. 11902.3; 1097.0 

• 12/18/09 12:18 PM! 3240.1! 11902.1! 1101.7 

12/18/09 12:18 PMi 3239.8; 11901.8: 1106.3 

12/18/09 12:18 PM; 324671 11928.1; 11110 

12/18/09 12:18 PM, 3240.1 11928.1 1115.7 

12/18/0912:19 PMj 3240.2 11928.2; 1120.4 

12/18/09 12:19 PMi . 3240.3^ 11928.3! 1125.1 

12/18/09 12:19 PMj 3240.5; 11928.5! 1129.7 

12/18/09 12:19 PM; 3240.5 11928.5! 1134.3 

12/18/0912:20 PMi 324675! 11928.5- 1138.9 

12/18/09 12:20 PMi 3240.5 11928.5; 1138.9 

12/18/09 12:20 PMi 1240.71 11928.7! 1138.9 

12/18/09 12:20 PMj 3240.9j 11928.9; 1138.9 

12/18/09 12:2T PM; """3246 1 11928.9! 1138.9 

12/18/09 12:21 PMj " 3241 TT; 11929.1; 1139.0 

12/18/09 12:21 PMj 3241.2! - 11929.2! 1139.1 

12/18/09 12:21 PM! 3241 l j 11929.2! 1139.1 

12/18/09 12:22 PMj '""'"" 3241.3! 11929.31 1139.2 

12/18/09 12:22 PMl 324l'.2j 11929.2! 1139.2 

12/18/09 12:22 PMj 3241.01 11929.0! 1139.3 

12/18/09 12:22 PMj 324617! 12181.7! 1139.4 

12/18/09 12:23 PMi 3240.6! 12181.6; 1139.7 

12/18/09 12:23 PMj 32401 12181.4; 1139.9 
Unit 4 Run 3 I 

. ^$fimelSta>rip->;;.' Liquid Weight'HRT TotaliWeigh.KHRf *-2&HRT 

12/18/09 12:23 PM 3240.4! 12181.4; 1140.0 

12/18/09 12:23 PM 3240.1! 12181.1; 1140.3 

12/18/09 12:24 PM 3240.0! 12181.0! 1140.6 

12/18/09 12:24 PM 3240.6]' 12181.0! 1141.0 

12/18/09 12:24 PM '3240] l] 12207.1! 1141.1 

12/18/09 12:24 PM '3246.0 ! 12207.6! 1141.1 

12/18/09 12:25 PM "3239.8: 12206.8; 1141.1 

12/18/09 12:25 PM '323978] 12232.8; 1141.3 

12/18/09 12:25 PM 3239.4, 12232.4! 1141.4 

12/18/09 12:25 PM 3238.9j 12231.9 1141.4 

12/18/09 12:26 PM 3238.51. 12257.5 1141.4 

12/18/09 12:26 PM 3238.0 12257.0! 1141.2 

12/18/09 12:26 PM 3237.4] 12256.4 1141.0 

12/18/09 12:26 PM, 3236.9 "'"T2281.9 1140.8 

12/18/09 12:27 PMi 3236.4 12281.4 1140.7 

12/18/09 12:27 PM, 3235.9j 12286.9 1140.4 

12/18/09 12:27 PM 3235.7! 12306.7 1140.1 

12/18/09 12:27 PMi 3235.5; 12306.5 1140.0 

12/18/09 12:28 PM; " 3235.5' 12306.5 1139.8 

12/18/09 12:28 PMi 3235.5; 12332.5 1139.6 

12/18/09 12:28 PMj 3235.2 1233272 1139.4 

12/18/09 12:28 PM^ '323572" 12332.2 1139.2 

12/18/09 12:29 PMi 3235 1 12332.1 1139.2 

12/18/09 12:29 PM! 323571! 12332.1 1139.3 

12/18/09 12:29 PMj "" 3235.2 12332.2 1139.3 

12/18/09 12:29 PMj 3235.lT' 12332.1 1139.3 

12/18/09 12:30 PMi 3235.2 12332.2 1139.2 

12/18/09 12:30 PMi 3235:3 '12332.3 1139.1 

12/18/09 12:30 PMj 3235.4: 12332.4 1139.2 

12/18/09 12:30 PMj "3235.4f 13128.4 1139.1 

12/18/09 12:31 PMi 3235.67' 13128.6 1139.2 

12/18/09 12:31 PMi 3235.6; 13128.6 1139.1 

12/18/09 12:31 PMj 3235.7' 13128.7 1139.1 

12/18/09 12:31 PM' 3235.8 12024.8 1139.2 

12/18/09 12:32 PMi 3235.9j 12024.9! 1139.3 

12/18/09 12:32 PM; 323676! 12025.0 1139.3 

12/18/09 12:32 PM' 3236.1 j "12051.1 1139.4 

12/18/09 12:32 PM! 323676: 12051.0 1139.4 

12/18/09 12:33 PM 3235.9! 12050.9 1139.3 

12/18/09 12:33 PM 323578: 1207678 1139.3 

12/18/09 12:33 PM 323578; 12076.8 1139.5 

12/18/09 12:33 PMj 3235.9] 12076.9 1139.6 

12/18/09 12:34 PMi .. 323577T 12076.7 1139.5 

12/18/09 12:34 PMj 3235.6! 12076.6 1139.5 

1.2/18/09 12:34 PM! 3235.5j 12050.5 1139.3 

12/18/09 12:34 PMj 3235.4! 12076.4 1139.3 

12/18/09 12:35 PMi 3235.0; 12076.0 1139.4 

12/18/09 12:35 PMi 3234.91"" 12049.9 1139.2 

12/18/09 12:35 PM; 3234.8! 12075.8 1139.2 

12/18/09 12:35 PMj 3234.7! 12075.7 1139.2 
Unit 4 Run 3 

TimeJStamp Liquid Weight HRT [ total Weight HRT X-22-HRT 

.12/18/09 12:36 PMi 3234.7! 12049.7! 1139.2 12/18/09 12:36 PMI 3234.8! 12049.8; 1139.4 

12/18/09 12:36 PM, 3234.8i 12049.8] 1139.4 

12/18/09 12:36 PMr 

3235.1] 12023.1 1139.3 

12/18/09 12:37 PM; 3235.2; 12623.2 ; 

1139.2 12/18/09 12:37 PM; 3235.3; 12023.3] 1139.3 

12/18/09 12:37 PM! 3235.4; 11997.4 1139.4 

12/18/09 12:37 PM, 3235.5, " ' 11997.5; 1139.5 

12/18/09 12:38 PM; ~32351?"'" " 11997.8! 1139.4 

12/18/09 12:38 PMj 3235.8 11997.8! 1139.4 

12/18/09 12:38 PMj 3236. If""' 11998.1 1139.5 

12/18/09 12:38 PM; 3236.1 11998.1 1139.6 

12/18/09 12:39 PMj 3236.3 11998.3! 1139.5 

12/18/09 12:39 PM! 3236.3! 11998.3! 1139.6 

12/18/09 12:39 PMi 3236.3 11998.3! 1139.7 

12/18/09 12:39 PM 323676; 11793.6! 1139.6 

12/18/09 12:40 PMi 3236777 11793.7: 1139.6 

12/18/0912:40 PMi 3236.97 11793.9 1139.7 

12/18/09 12:40 PM; 3237":0i 11794.0 1139.8 

12/18/09 12:40 PMj 3237.1. 11820.1 1139.8 

12/18/09 12:41 PM; 3237.3 11820.3; 1139.7 

12/18/09 12:41 PM; 3237.3: ' 11820.3 1139.7 

12/18/09 12:41 PMi 3237.4; 11819.4" 1139.8 

12/18/09 12:41 PMi 3237.37 11819.3! 1139.8 

12/18/09 12:42 PM' 3237.4 11819.4. 1139.8 

12/18/09 12:42 PM: 3237.5: 11819.5: 1139.8 

12/18/0912:42 PM! 3237.6; 11819.6] 1139.8 

12/18/0912:42 PM; 323775; 11819.5 1139.8 

12/18/09 12:43 PMj 3237.57' 11819.5 1139.8 

12/18/09 12:43 PM: 3237.7! 11819.7 1139.8 

12/18/09 12:43 PMj 3238.6; 11820.0 1139.8 

12/18/09 12:43 PMi 3238.1 j 11820.1 1139.8 

12/18/09 12:44 PMj 32381; 11820.1 1139.7 

12/18/09 12:44 PMj "~3238.6; 11820.0 1139.6 

12/18/09 12:44 PM: 32387Tf 11820.1 1139.6 

12/18/09 12:44 PMi 3238.1"' 11820.1 1139.6 

12/18/09 12:45 PM 3238.1 11820.1 1139.5 

12/18/09 12:45 PM! 3238.1 ""' 11820.1 1139.5 

12/18/09 12:45 PMi 3238.1 11820.1. 1139.4 

12/18/09 12:45 PM; 3238727 11820.2; 1139.3 

12/18/09 12:46 PM' 3238.57' 11820.5! 1139.3 

12/18/09 12:46 PM: 3238.8; 11820.8! 1139.3 

12/18/09 12:46 PM; "323878! 11820.8! 1139.2 12/18/09 12:46 PMi 3239:0j 10704.0! 1139.3 

12/18/09 12:47 PMj 3239737 10704.3] 1139.3 

12/18/09 12:47 PMj 323975! 10704.5] 1139.3 

12/18/09 12:47 PMj 3239.7; 10704.7! 1139.3 

12/18/09 12:47 PMi 3239.9] 11677.9; 1139.3 

12/18/0912:48 PMj 32407ir 11678.1] 1139.3 

12/18/09 12:48 PMl '3240.2! 11678.2! 1139.4 
Unit 4 Run 3 j 

ls;|limeI|lKp5i i Liqu'idiWeightHR.T' Total WeighrHRT fcX-22 HRT 

12/18/09 12:48 PM 3240.3 11652.3 1139.5 

12/18/09 12:48 PM; 3240.4 i 1678.4 1139.5 

12/18/0912:49 PM; 3240.7 11678.7 1139.5 

12/18/09 12:49 PMj 3240.9 11652.9 1139.4 

12/18/0912:49 PM! '""3241 0 11679.0 1139.3 

12/18/0912:49 PMl """'3241 2 li"679.2H 1139.5 

12/18/0912:50 PM; 32414 11653.4 1139.4 

12/18/0912:50 PM: 32416 11679.6" 1139.5 

12/18/0912:50 PM; 32417 11679.7 1139.6 

12/18/09 12:50 PM; 32417 11679.7 1139.5 

12/18/0912:51 PM """32418 11679.8 1139.4 

12/18/0912:51 PM] 3242.0, 11680.0, 1139.5 

12/18/0912:51 PM; 3242.1 11680.1] 1139.5 

12/18/09 12:51 PM: 3242.3 11680.3; 1139.5 

12/18/0912:52 PMI 3242.5 11680.5; 1139.5 

12/18/0912:52 PMi 3242.6. 11680.6s 1139.6 

12/18/09 12:52 PM! 3242.5 11680.5! 1139.5 

12/18/0912:52 PM, 324Z5! 11680.5 1139.4 

12/18/0912:53 PM! 3242.'2i 11680.2! 1139.4 

12/18/0912:53 PMi " 3242.1 11680.1 1139.4 

1271870912:53 PM; 32417; 11679.7] 1139.6 

12/18/0912:53 PM' 3241.41 11679.4! 1139.6 

12/18/09 12:54 PM! 32411! 11679.1! 1139.6 

12/18/09 12:54 PMi "' 3241.6 "\ 1679.0! 1139.5 

12/18/0912:54 PM; 3240.7; 11678.7! 1139.5 

12/18/09 12:54 PM! '32404] 11678.4; 1139.6 

12/18/0912:55 PMi 3240.3, 11678.3; 1139.6 

12/18/09 12:55 PM| 3240"3| 11678.3! 1139.7 

12/18/09 12:55 PMj ~ 3239.9! 11677.9! 1139.5 

12/18/09 12:55 PMi 3239.7! 11491.7! 1139.5 

"12/18/0912:56 PM! " 3239.'5; 11491.5! 1139.6 

12/18/09 12:56 PM; 3239.4; 11491.4; 1139.7 

12/18/09 12:56 PM; 3239.5! 11491.5! 1139.7 

12/18/09 12:56 PM! ""3239.7; ' 11465.7! 1139.7 

12/18/09 12:57 PM! 3239I9 11491.9: 1139.7 

12/18/09 12:57 PM; 3239.9; 11465.9] . 1139.7 

12/18/09 12:57 PM; 3240.2. ll46"6.2! 1139.7 

12/18/09 12:57 PM; "32407! 11492.7] 1139.8 

12/18/09 12:58 PMi 3241.1 1146711] 1139.7 

12/18/09 12:58 PMi 3241! 8; 11467.8; 1139.6 

12/18/09 12:58 PM! 324221 11494.2! 1139.7 

12/18/09 12:58 PM; 3243?; 11469.0; 1139.7 

12/18/09 12:59 PMi '3243. 6 11469.6! 1139.9 

12/18/09 12:59 PM! "3244.T! 11497.1! 1139.9 

12/18/09 12:59 PM: ""3244.1 . 114711] 1140.3 

12/18/09 12:59 PMl 3244!3! 114713] 1140.6 

12/18/091:00 PM; """"32444; 11497.4! 1140.8 

12/18/091:00 PM! 32444! 11471.4! 1141.2 

12/18/091:00 PM! TM3244?5l 11471.5! 1141.5 

12/18/09 1:00 PM! 3244.5! 11497.5; 1141.9 
Unit A Run 3 

• ' Time' Stamp ,. ^Liquid WeightfHR^ 

12/18/09 1:01 PM 3244.4! 11497.4 . 1142.3 

12/18/09 1:01 PM 3244.4 11497.4 1142.4 

12/18/09 1:01 PM " " ~ 32443! 11497.3 1142.7 

12/18/091:01 PM 3244.2. 11497.2 1143.0 

" "12/18/09 1:02 PM' 3244.1' 11497.1 1143.3 

12/18/09 1:02 PM 324471! 11497.1 1143.6 

12/18/09 1:02 PM 3244.1; 11497.1 1144.0 

12/18/09 1:02 PM 3244.1 11497.1 1144.2 

12/18/09 1:03 PM 3243.9, 11496.9 1144.4 

12/18/09 1:03 PM 324379: I 11496.9 1144.7 

12/18/09 1:03 PM 3244.67 1149770 1145.0 

12/18/09 1:03 PM 3244.2; 12552.2 1145.3 

12/18/09 1:04 PM 324447 12552.4 1145.4 

12/18/09 1:04 PM' 3244.6! 12552.6 1145.5 

12/18/09 1:04 PM 3244.8; 12552.8 1145.7 

12/18/09 1:04 PM 3244.97 11365.9 1146.1 

12/18/09 1:05 PM 3245.47 11366.4 1146.2 

12/18/09 1:05 PM, 324575! 11366,5 1146.5 

12/18/09 1:05 PM. 

3245.9; 11392.9 1146.7 

12/18/09 1:05 PM: 324637 11393.2' 1147.0 

12/18/09 1:06 PMi 324677! 11367.7 1147.3 

12/18/09 1:06 PM; 324716* ' 11394.0 1147.5 

12/18/09 1:06 PM; 3247.3; 11394.3; 1147.7 

12/18/09 1:06 PM. 3247.7; 11368.7; 1147.9 

12/18/09 1:07 PMi 3248.17 11395.1! 1148.1 

12/18/09 1:07 PM; 3248.7; 11395.7; 1148.4 

12/18/09 1:07 PMi 3249.2: 11370.Z 1148.6 

12/18/09 1:07PM| '"732567T7" 11397.11 1148.7 

12/18/09 1:08 PMi 325675: 11371.5] 1149.3 

12/18/09 1:08 PM! 3251.0: 11'372.0! 1149.6 

12/18/09 1:08 PM! 32514, ' 11398.4! 1149.8 

12/18/09 1:08 PM: 3251.7:' 11372.7| 1150.0 

12/18/09 1:09 PMl 3252.1 11373.1; 1150.5 

12/18/09 1:09 PMi 3252.4 i 1373.4; 1150.7 

12/18/09 1:09 PMi 325279: 11347.9! 1151.0 

12/18/09 1:09 PMi ' 32534!" 11348.4! 1151.3 

12/18/09 1:10 PMi "3253.81" l i 348.8! 1151.6 

12/18/09 1:10 PM"! 3254.3"; 11349.3; 1-152.0 

12/18/09 1:10 PMi 3254.7! 11349.7! 1152.4 

12/18/09 1:10 PMi 3255.11 1T350.1I 1152.8 

12/18/09 1:11 PM! " 3255.6, "' ': 11350.6 1153.2 

12/18/09 1:11 PM! 325579." 11350.9! 1153.5 

12/18/09 1:11 PM! 3256.1! 11351.11 1153.7 

12/18/09 1:11 PM; 3256.5' 12573.5! 1153.9 

12/18/09 1:12 PMl 3256.8; 12573.8s 1154.3 

12/18/09 1:12 PM: 3257.1 12574.1! 1154.6 

12/18/09 1:12 PM, 

3257.3; 12574.3; 1154.9 

12/18/09 1:12 PM; 325775! 12574.5; 1155.1 

12/18/09 1:13 PM'i "3257.9 12574.9! 1155.4 

12/18/09 1:13 PMi 3258 3' 12601.31 1155.7 
Unit4 Run 3 

^TfmeOstamp Liquid Weipht'HRT- TotaLWeight HRT, liSii l 

12/18/09 1:13 PM |3258.8 12601.8 1156.1 

12/18/091:13 PM, 3259.2 11425.2 1156.3 

12/18/091:14 PM! 325~9.7 11451.7 1156.7 

12/18/09 1:14 PM| 3260.2 11452.2' 1157.0 

12/18/091:14 PM! 3260.6 11479.6 1157.4 

12/18/091:14 PM: 3261.1 11454.1 1157.7 

12/18/09 1:15 PM 3261.3 11454.3 1158.0 

12/18/09 1:15 PM 32617' 11481.7 1158.3 

12/18/091:15 PM. 3262.0 11456.0 1158.8 

12/18/09 1:15 PMj 3262.5 11456.5 1158.9 

12/18/091:16 PM! 3262.9' 11483.9 1159.1 

12/18/09 1:16 PM 3263.0. 11458.6 1159.4 

12/18/09 1:16 PM 3263.5: 11458.5 1159.6 

T2/18/09 1:16 PM 3264.6 11459.0 1160.0 

12/18/09 1:17 PM 3264.1, 11433.1 1160.2 

12/18/09 1:17 PM 3264.5! 11460.5 11.60.6 

12/18/09 1:17 PM 3264.9 11460.9 1160.9 

12/18/09 1:17 PM 3265.2, 11435.2 1161.3 

12/18/09 1:18 PM 3265.4. 11435.4 1161.7 

12/18/09 1:18 PM| 3265.8| 11435.81 1162.0 

12/18/09 1:18 PM 3266.0: 11410.6' 1162.3 

12/18/09 1:18 PM ' 3266l4i 11410.4! 1162.6 

12/18/09 1:19 PM 3267.0! 11411.0 1163.0 

12/18/09 1:19PM 3267.3! 11411.3 1163.4 

12/18/09 1:19 PM 3267.6; 11411.6! 1163.7 

12/18/09 1:19 PM * " 3268.0 11412.0 1164.2 

12/18/09 1:20 PM "326875 ] 11412.5 1164.7 

12/18/09 1:20 PM "3269761 11413.0 1165.0 

12/18/091:20 PM 3269757 11413.5} 1165.2 

12/18/091:20 PM 3269.8! 12578.81 1165.5 

12/18/091:21 PM 3270.2: 12579.2! 1165.8 

12/18/091:21 PM 3270.6; 12579.6, 1166.0 

12/18/091:21 PM 3271.0; 12580.0: 1166.2 

12/18/09 1:21 PM """32714 ; 12607.4' 1166.4 

12/18/091:22 PM 3271.9; 12607.9: 1166.6 

12/18/091:22 PM 3272.3] 12608.3! 1166.9 

12/18/09 1:22 PM 3272.81 12635.8! 1167.2 

12/18/09 1:22 PM 327373; 11567.3! 1167.3 

12/18/09 1:23 PM 3273.6; 11567.6} 1167.3 

12/18/091:23 PM 3274.6] 11595.6; 1167.4 

12/18/09 1:23 PM 3274.4; Tl 595.4! 1167.7 

12/18/091:23 PM' 3274J] 1159579! 1167.8 

12/18/09 1:24 PM 3275.3] 11623.3! 1167.9 

12/18/09 1:24 PM- 327575! 11623.51 1167.9 

12/18/09 1:24 PM 3275.7! 11597.7! 1168.0 

' 12/18/09 1:24 PM '327672; 11625.2! 1168.3 

12/18/091:25 PM 3276.6| 11625.6! 1168.4 

12/18/09 1:25 PM! 3277.0! 11600.0! 1168.5 

12/18/09 1:25 PM' 3277.4; 11627.4} 1168.5 

12/18/091:25 PM 32778! 11627.8: 1168.8 
Unit4 Run 3 J 

..Liquid WeighfcHRti 

12/18/09 1:26 PM 3278.2j 11602.2 ]. 1169.0 

12/18/09 1:26 PM 3278.5i 11602.5] 1169.0 

12/18/09 1:26 PM 3279.6: 11603.0! 1169.1 

12/18/09 1:26 PM 3279.4] 11577.4! 1169.4 

12/18/09 1:27 PM 3279.9' 11577.9 ' 1169.6 

12/18/09 1:27 PM 3280.3! 11578.3 1169.9 

12/18/09 1:27 PM " 3280.7 "' 11552.7! 1170.3 

12/18/09 1:27 PM 3281 i6T" 11553.0 1170.5 

12/18/09 1:28 PM 3281.3" 11553.3; 1170.7 

12/18/09 1:28 PM 3281.5; 11527.5 1171.0 

12/18/09 1:28 PM 3282.1! li5287T 1171.3 

12/18/09 1:28 PM 3282.7! "'11528. 7 1171.5 

12/18/09 1:29 PM 328372 11529.2 1171.8 

12/18/09 1:29 PM; 3283.9! 11530.0 1172.0 

12/18/09 1:29 PM 3284.4; 11530.4 1172.3 

12/18/09 1:29 PM 3285.1. 12666.1 1172.6 

12/18/09 1:30 PM 328576! 12666.6 1172.9 

12/18/09 1:30 PMi "328579; """1266679' 1173.2 

12/18/09 1:30 PM! i37286.4:'' ' 12667.4 1173.4 

12/18/09 1:30 PM* 3287.0: 11899.6 1173.5 

12/18/09 1:31 PM! 3287.5: 11899.5 1173.7 

12/18/09 1:31 PMi 3288.6["~ 11900.0 1174.0 

12/18/09 1:31 PM; "3288]5i " 11927.5 1174.2 

12/18/091:31 PMi 3288:7: 119017" 1174.4 

12/18/09 1:32 PM! 3289.6; 11902.0 1174.7 

12/18/09 1:32 PMj 3289.'3: "~" 9287*3 1174.9 

12/18/09 1:32 PMi 3289:5: " 11902.5 1175.1 

12/18/09 1:32 PMi 3289.9! 11902.9 1175.4 

12/18/09 1:33 PMi ~"*3296. 3 11930.3 1175.6 

12/18/09 1:33 PMj "32907?""' 11904.7 1175.9 

12/18/091:33 PMj 3290.9! 11904.9 1176.0 

12/18/09 1:33 PMi 32911 11932.1 1176.2 

12/18/09 1:34 PMl 3291.5 11906.5 1176.5 

12/18/09 1:34 PMi 3291.9; 11906.9 1176.7 

12/18/09 1:34 PM; 3292.2] 11934.2 1177.0 

12/18/091:34 PMj 3292.3; 11908.3 1177.2 

12/18/09 1:35 PMj 3292T8TTM" 11908.8 1177.4 

12/18/09 1:35 PM! 329"3]6'''"" 11909.0 1177.8 

12/18/09 1:35 PMj 3293.3 11883.3 1178.0 

12/18/09 1:35 PM] 3293.5! 11883.5 1178.1 

12/18/09 1:36 PMi 32937j 11883.7 1178.4 

12/18/09 1:36 PMj 3294.1] 11884.1, 1178.6 

12/18/09 1:36 PMj "~ ]3294'ir " 11884.2 1179.0 

12/18/09 1:36 PM! 3294.1] 11884.1 1179.3 

12/18/09 1:37 PMj 3294.2: ~" 11884.2 1179.5 

12/18/09 1:37 PM! 3294.2] 11884.2 1179.7 

12/18/09 1:37 PMj i~"329472 ! 13083.2] 1180.0 

12/18/09 1:37 PMj 3294.4! 13683.4] 1180.1 

12/18/09 1:38 PM! 3294.6] 13083.6 1180.4 

12/18/09 1:38 PM; 3294.7] 1308377 1180.7 
Unit4 Run 3 | 

LiqU d?W&gbf;

tfRT: .Totaji:W6ight;,H.RT X-22 HRT 12/18/09 1:38 PM| 3295.0 13084.0 1180.8 

12/18/09 1:38 PMi 329513 13084.6 1181.0 

12/18/09 1:39 PM! 3296.2 13085.2 1181.3 

12/18/09 1:39 PMj 3296! 13112.8 1181.6 

12/18/09 1:39 PMi 3297.3 13113.3 1181.8 

12/18/09 1:39 PM] 3298.1 12179.1 1182.2 

12/18/09 1:40 PMi 3298.7 12206J 1182.4 

12/18/09 1:40 PM i 3299.4 12207.4 1182.6 

12/18/09 1:40 PM i 3300.1 12208.1 . 1182.9 

12/18/09 1:40 PM! 33007 i'2209.7 1183.3 

12/18/09 1:41 PM i 33014; 12210.4 1183.3 

12/18/09 1:41 PM! 33022! 12211.2 1183.5 

12/18/09 1:41 PM i "3302. 8 12212.8 1183.8 

12/18/09 1:41 PM 3303.5 12213.5; 1184.0 

12/18/09 1:42 PM' 3304.4; 12214.4 1184.1 

12/18/09 1:42 PM! 33051! 12216.21 1184.4 

12/18/09 1:42 PMl 3306.0! 12217.0; 1184.7 

12/18/09 1:42 PMi 33067j 12217.7! 1185.0 

12/18/09 1:43 PM! 3307!] 12219.5! 1185.4 

12/18/09 1:43 PM; 3368.2; 12226.2; 1185.4 

12/18/09 1:43 PMj 3308.6; 12220.6! 1185.7 

12/18/09 1:43 PM .. 3309.6j 12221.0} 1185.8 

12/18/09 1:44 PM 3309.7! 12221.7! 1186.1 

12/18/09 1:44 PM 3310.51 12222.5! 1186.6 

12/18/09 1:44 PM! 3311.3! 12223.3! 1186.9 

12/18/09 1:44 PM 3312.0; 12224.0; 1187.2 

12/18/09 1:45 PM 3312.6j 12224.6: 1187.4 

12/18/09 1:45 PM 12225.3} 1187.5 

.12/18/09 1:45 PMj 3314.2] 12226.2; 1187.8 

12/18/091:45 PM 3314.7! 12226.7! 1188.1 

12/18/09 1:46 PM 3315.1; 12227.1j 1188.4 

12/18/09 1:46 PM 3315.7! 12227.7! 1188.8 

12/18/09 1:46 PM 3316.4: 12228.4; 1189.1 

12/18/09 1:46 PM 3316!! 12228.9] 1189.3 

12/18/09 1:47 PM 33i'7.4 12229.4; 1189.6 

12/18/09 1:47 PM 3318.0; 13.496.0; 1189.8 

12/18/09 1:47 PM ""33T8i6f 13496.6! 1190.1 

12/18/09 1:47 PM 3319.3; 12524.3! 1190.4 

12/18/09 1:48 PMI ~ i 3319.9: 12524.9] 1190.6 

12/18/09 1:48 PMi 3320.5T 12552.5; 1190.9 

12/18/09 1:48 PM; "332l6: 12553.6; 11913 

12/18/091:48 PM 33214j 12527.4! 1191.5 

12/18/09 1:49 PMi 3322.0! • 12555.6] 1191.8 

12/18/09 1:49 PMj 332Z6T 12555.6! 1192.1 

12/18/09 1:49 PM 3323.2] 12530.2! 1192.5 

12/18/09 1:49 PMj "* """"3323.8] 12557.8i 1192.7 

12/18/09 1:50 PMj 3324.3; 12558.3] 1192.9 

12/18/09 1:50 PMi 3324.9! 12532.9! 1193.3 

12/18/09 1:50 PMi 3325.7" 12560.71 1193.4 

12/18/09 1:50 PMi "3326.6j " 12535.6! 1193.6 
Unit 4 Run 3 

Time' Stamp ! Liquid Weight HRT Total WeightHrST X-22'H.RT 

12/18/09 1:51 PM 3327.1 12536.1 1193.7 

12/18/09 1:51 PM 3328.1 "T25647T' 1194.0 

12/18/09 1:51 PM 3329.0 12539.6 . 1194.4 

12/18/09 1:51 PM 3329.8 '"1256678 1194.6 

12/18/09 1:52 PM 333074 12567.4 1194.8 

12/18/09 1:52 PM 3331.1 12542.1 1195.0 

12/18/09 1:52 PM 3332.6 12543.0 1195.3 

12/18/09 1:52 PM 333276 12543.6 1195.6 

12/18/09 1:53 PM 3333.6 12544.6 1195.9 

12/18/09 1:53 PM 33343" 12545.3 1196.2 

12/18/09 1:53 PM "3335/1" 12546.1 1196.6 

12/18/09 1:53 PM 3335.8' 12546.8 1196.9 

12/18/09 1:54 PM 33367! 12547.7; 1197.3 

12/18/09 1:54 PM 3337.31 12548.3* 1197.8 

12/18/091:54 PM 3338.0; 12549.0; 1198.1 

12/18/091:54 PM! 333877! 13779.7! 1198.5 

12/18/09 1:55 PM! 3339.3' 13780.3! 1198.8 

12/18/09 1:55 PM' 3339.9! 13780.9! 

. . . ...^ .. i- ... . ,... i 

1199.2 

12/18/09 1:55 PM; 3340.7! 13781.7; 1199.7 

12/18/091:55 PM; 3341.2; 12760.2! 1200.1 

12/18/091:56 PM; '"'3341787 12760.8; 1200.6 

12/18/09 1:56 PM; 334275; 12761.5j 1201.1 

12/18/091:56 PM! 3342.8 12788.8! 1201.5 

12/18/09 1:56 PM; 334"3.i: 12789.1! 1202.0 

12/18/09 1:57 PM, "334319; 12763.9! 1202.5 

12/18/091:57 PM! 334476'j '12790.6 1202.8 

12/18/091:57 PMi ""334573 ; 12791.3! 1203.2 

12/18/09 1:57 PMi 3345.9: 12765.9! 1203.7 

12/18/091:58 PM; 3346.5; 12792.5! 1204.1 

12/18/091:58 PMj 3346.8j 12792.8! 1204.7 

12/18/091:58 PMj 3347.2 12793.2;! 1205.0 

12/18/09 1:58 PM] "3347. 6 12793.6! 1205.4 

12/18/09 1:59 PM! 3347.7; 12793.7: 1205.8 

12/18/09 1:59 PM! 3348.0! 12793.0! 1206.1 

12/18/09 1:59 PMl 3348.3; 12793.3; 1206.2 

12118/091:59 PM; 3348.6! 12793.6' 1206.3 

12/18/09 2:00 PM; 3349.61 12768.0 1206.2 

12/18/09 2:00 PM! 3349.2] 12768.2; 1206.1 

12/18/09 2:00 PMj 3349.6! 12768.6; 1206.1 

12/18/09 2:00 PMj 3350.0; 12743.0; 1206.0 

12/18/09 2:01 PM; 3350.3! 12743.3! 1205.9 

12/18/09 2:01 PM! 3350.61 12743.6; 1206.3 

12/18/09 2:01 PM! '335T6 [ 12744.6! 1206.4 

12/18/09 2:01 PMj 3351.4; 12744.4! 1206.4 

12/18/09 2:02 PMi 3351.8! 12744.8! 1206.4 

• 12/18/09 2:02 PMj '• 335276: 12745.0j 1206.4 

12/18/09 2:02 PMj 335273] T2745.3] 1206.4 

12/18/09 2:02 PM! 335277! 13996.7] 1206.5 

12/18/09 2:03 PM* """""335372 ! 13997.21 1206.6 

12/18/09 2:03 PMi """3353.6! 13997.6! 1206.7 
Unit4 Run 3 I 

' rirne."Stamp Liquid WeightiWRT Total! Weight ffRfi iiiiii i 

12/18/09 2:03 PM 3354.0! 13998.0 1206.7 

12/18/09 2:03 PM 3354.51 12969.5 1206.9 

12/18/09 2:04 PM 3355.6; " '""12976.6 1207.3 

12/18/09 2:04 PM 3355.3; 12970.3 1207.3 

12/18/09 2:04 PM 335578! 12996.8 1207.4 

12/18/09 2:04 PM 3356.3 12971.3 1207.5 

12/18/09 2:05 PM 3356.8! 1297T8 1207.5 

12/18/09 2:05 PM 3357.4! "T2998.4 1207.6 

12/18/09 2:05 PM 335778:' 12972.8 1207.7 

12/18/09 2:05 PM 3358.3 12973.3 1207.9 

12/18/09 2:06 PM 3358.8 12999.8 1208.0 

12/18/09 2:06 PM 3359.3"! 12974.3 1208.0 

12/18/09 2:06 PM ' 335979; 12~974.9 1208.1 

12/18/09 2:06 PM' 3360737 13001.3, 1208.1 

12/18/09 2:07 PM: 336677; 12975.7! 1208.2 

12/18/092:07 PM] 3361767' 12976.0; 1208.3 

12/18/09 2:07 PM| 3361.21 13002.21 1208.4 

12/18/09 2:07 PM: 3361.3! 12976.3! 1208.5 

12/18/09 2:08 PMI ""336176 " 12976.6! 1208.5 

12/18/09 2:08 PM] 3361.6; 12976.6! 1208.6 

12/18/09 2:08 PMi 3361.8; 12950.8! 1208.6 

12/18/09 2:08 PMi 3362.2! 12951.2! 1208.7 

12/18/09 2:09 PM| 3362.4; 12951.4! 1208.5 

12/18/09 2:09 PM; 336275 12951.5; 1208.5 

12/18/09 2:09 PM; 3362.7 12951.7! 1208.7 

12/18/09 2:09 PMI 3362.9! 12951.9! 1208.6 

12/18/09 2:10 PMI 3363.1! 12952.1 1208.8 

12/18/09 2:10 PMI '3363.3: 12952.3! 1208.8 

12/18/09 2:10 PMi 3363.5; 12952.51 1208.8 

12/18/09 2:10 PMi 3363.97 14222.9! 1208.7 

12/18/09 2:11 PMi 336472;" 14223.2! 1208.8 

12/18/09 2:11 PMl 3364.5' 14223.5; 1209.0 

12/18/09 2:11 PMj 3364.8. 14223.8, 1209.2 

12/18/09 2:11 PMj 3365.0! 13028.0! 1209.3 

12/18/09 2:12 PM! '3365.3 13028.3! 1209.4 

12/18/09 2:12 PMI 3365.6! 13028.6! 1209.4 

12/18/09 2:12 PM; 3365.8; 13054.8! 1209.5 

12/18/09 2:12 PM! 336672; "' 1305572! 1209.5 

12/18/09 2:13 PMj ~ 338074; i3669.4j 1209.7 

12/18/09 2:13 PMj "336772 13057.2! 1209.7 

12/18/09 2:13 PMj "'336775 ; 13057.5; 1209.7 

12/18/09 2:13 PM! 3368.0! 13058.0! 1209.9 

12/18/09 2:14 PM! 3368.5] 13059.5; 1209.9 

12/18/09 2:14 PM! 3368.8 13059.8! 1209.8 

12/18/09 2:14 PM! 3369.2; 13033.21 1209.8 

12/18/09 2:14PMr 3369.5'' 13060.5! 1209.9 

12/18/09" 2:15 PM! 3376761 1306101 1209.8 

12/18/09 2:15 PM 3370.6; 13034.6! 1209.8 

12/18/09 2:15 PM^ ""3371.1 ; 13062.1 1209.7 

12/18/09 2:15>M; 337167" 13062.6; 1209.8 

VES018909 
Unit4 Run 3 1 

3§if imelS.tamp:?|?| Liquid Weight HRT: Total Weight'! HRT X^22.HRT 

12/18/09 2:16 PM; 3372.1 13036.1] 1210.0 

12/18/09 2:16 PM 3372.7 13036.7! 1210.1 

12/18/09 2:16 PM 3373.6 13037.O! 1210.3 

12/18/09 2:16 PM 3373.4 13037.4! 1210.4 

12/18/09 2:17 PM 337471 13038.1! 1210.4 

12/18/09 2:17 PM 3374.5 13011.5! 1210.4 

12/18/09 2:17 PM 3374.9 13011.9! 1210.4 

12/18/09 2:17 PM 337574 13012.4; 1210.5 

12/18/09 2:18 PM 3375.9 13012.9! 1210.5 

12/18/09 2:18 PM 3376.4 13013.4] 1210.5 

12/18/09 2:18 PM 3377,1 13014.1] 1210.7 

12/18/09 2:18 PM '3377.3 13014.3! 1210.8 

12/18/09 2:19 PM 3377.6. 13014.6 1210.8 

12/18/09 2:19 PM 3378.0; 13015.0 1210.7 

12/18/09 2:19 PM 337873! 13015.3! 1210.8 

12/18/09 2:19 PM. 3378.3] 14226.3] 1210.8 

12/18/09 2:20 PM, """337875] 14226.5] 1210.9 

12/18/09 2:20 PM! 3378.5: 14226.5] 1211.0 

12/18/09 2:20 PM; 3378.5] 14226.5 1211.0 

12/18/09 2:20 PM 337875 1306175 1211.1 

12/18/09 2:21 PM> "'""3378 ] 8; 13061.8; 1211.1 

12/18/09 2:21 PM: 3378787 13088.8! 1211.3 

12/18/09 2:21 PM: 3378.8 13088.8i 1211.3 

12/18/092:21 PMi 3378.9 '13061.9!" 1211.5 

12/18/09 2:22 PM; 3379.0! 13088.0] 1211.6 

12/18/09 2:22 PM; 337971*1 13088.1 1211.7 

12/18/09 2:22 PMi 3379.3j 13061.3] 1211.7 

12/18/09 2:22 PM; 3379.4 13088.4! 1211.7 

12/18/09 2:23 PM: 33 7976 13088.6] 1211.9 

12/18/09 2:23 PMi 3379781 13087.8! 1212.2 

12/18/09 2:23 PMi 337979 13087.9! 1212.2 

12/18/09 2:23 PM] 3380.1; 13088.1! 1212.3 

12/18/09 2:24 PM| 3380.2! 13087.2! 1212.3 

12/18/09 2:24 PM] 3386.4j 1308774! 1212.4 

12/18/09 2:24 PM] 3386.7: 13087.7! 1212.4 

12/18/09 2:24 PM! 3380.7 13086.7] 1212.4 

12/18/09 2:25 PM] " 338678 13086.8T~ 1212.6 

12/18/09 2:25 PMj ""3380. 8 13086.8 1212.8 

12/18/09 2:25 PMi 3381.1! ~ 13660.1 1212.9 

12/18/09 2:25 PMj '3381.1' 13060.1 1212.7 

12/18/09 2:26 PM; ""338173 ! 13060.3] 1212.8 

12/18/09 2:26 PM; 3381.5; 13060.5! 1213.1 

12/18/09 2:26 PMi 3381.8' 13060.8! 1213.2 

12/18/09 2:26 PM] 3382.1 13061.1] 1213.4 

12/18/09 2:27 PM; 3382.7; 13061.7] 1213.4 

12/18/09 2:27 PMj 3383.17 13062.1! 1213.4 

12/18/09 2:27 PMi ""'"3383.5] 13062.5! 1213.5 

12/18/09 2:27 PMj 3384.0: 13063.0 1213.6 

12/18/09 2:28 PM: 338474 13063.4] 1213.7 

12/18/09 2:28 PM! 33847! 13063.7! 1213.7 
Unit4 Run 3 

fj^)WIi^tjrnfp',^ WeighfrHRT Total Weight HRT X-22 HRT 12/18/09 2:28 PM 

12/18/09 2:28 PM' 

12/18/09 2:29 PMj 

'12/18/09 2:29 PMl" 

"12/18/09 2:29 PM: 

12/18/09 2:29 PM: 

12/18/09 2:30 PMI 

"12/18/09 2:30 PM] 

12/18/09 2:30 PMj 

12/18/09 2:30 PM.' 

12/18/09 2:31 PM 

12/18/09 2:31 PM; 

"12/18/09 2:31 PMi 

12/18/09 2:31 PMj 

12/18/09 2:32 PM! 

12/18/09 2:32 PMi 

12/18/09 2:32 PM: 

12/18/09 2:32 PM; 

12/18/09 2:33 PMj 

12/18/09 2:33 PMj 

"12/18/09 2:33 PMf 

12/18/09 2:33 PMi 

12/18/09 2:34 PMj 

"12/18/09 2:34 PM; 

12/18/09 2:34 PM; 

12/18/09 2:34 PMi 

12/18/09 2:35 PMj 

12/18/09 2:35 PMi 

12/18/09 2:35 PM; 

12/18/09 2:35 PM: 

12/18/09 2:36 PMj 

12/18/09 2:36 PMj 

12/18/09 2:36 PMi 

12/18/09 2:36 PMi 

12/18/09 2:37 PMi" 

12/18/09 2:37 PMj 

12/18/09 2:37 PMj 

12/18/09 2:37 PM; 

12/18/09 2:38 PMi 

"12/18/09 2:38 PM< 

12/18/09 2:38 PMi 

12/18/09 2:38 PMj 

12/18/09 2:39 PMi 

"12/18/09 2:39 PMj ' 

12/18/09 2:39 PMi 

12/18/09 2:39 PMi 

3385.0; 

33l5]0j" 

3385.1';'" 

'1385.2;'" 

338574] 

3385.61 

3385.7; 

12/18/09 2:40 PM; 

12/18/09 2: 

12/18/09 2: 

40 PMj 

40 PMj " 

12/18/09 2:40 PM; 

338579; 

3386.1 

338673;" 

"'338674;' 

'338676;' 

'338677;' 

'338774T' 

"338876j" 

338875!" 

338971]] 

338976] 

3390.01' 

"339675! 

339172 

'"339176 

3392.3 

"33^79" 

'339374 

339471]" 

33945] 

339572" 

339577] 

"339pr 

3397.2; 

"339779!" 

"339877]"" 

"3399751"' 

34667!" 

340173;' 

34027TT 

346376]" 

340376; 

"3464.5; 

3404.97 

13064.0] 

"'1438776[ 

143871] 

13307.1; 

l328673[ 

1330674] 

"Tpd676[ 

"132797'7!_ 

T33674j_ 

"I3308.'6i_ 

1328275] 

13309.1j_ 

T3309"76] 

1328376T 

"il3]67.5!_ 

1330872! 

13281.6"" 

13282.3!_ 

1328279] 

13257.5] 

1325872! 

13258.7 

13259.5 

1326672 

13263.3]_ 

T3264'.3']_ 

1266671] 

1331076T 

3405.3! 

3405.4: 

1405.7]" 

13311.9! 

1333573 

3406.1 

IToao 

'7340672! 

140676 

3405.3 6 

13329.6; 

"I3302]3r 

1213.8 

1214.0 

1214.2 

14387.2] 1214.4 

14387.4; 1214.3 

13279.6! 1214.3 

13279.7! 1214.3 

13306.9! 1214.3 

1214.3 

1214.3 

1214.4 

1214.5 

1214.4 

1214.6 

1214.5 

1214.5 

1214.7 

1214.7 

1214.8 

1214.9 

1214.9 

1215.0 

1215.2 

1215.2 

13256.4! 1215.4 

13257.1] 1215.5 

1215.5 

1215.6 

1215.6 

1215.8 

1215.8 

13260.9! 1215.8 

13261.7] 121676 

13262.5 1216.0 

1216.1 

1216.1 

1216.2 

1216.2 

13310.6] 1216.5 

13311.5j 1216.6 

1216.8 

1217.0 

13335.41 1217.1 

13308.7! 1217.2 

13333.11 1217.2 

13333.0 1217.0 

13306.2] 1217.1 

13330.0! 1217.2 

1217.4 

1217.3 
Unit4 Run 3 

'Wim^steimp; Liquid HRT Total Weight HRT-I X-22 HRJ 

12/18/09 2:41 PM! 

12/18/09 2:41 PMi 

12/18/09 2:41 PMf 

12/18/09 2:41 PMj 

12/18/09 2:42 PM! 

12/18/09 2:42 PMi 

12/18/09 2:42 PM| 

12/18/09 2:42 PM! 

12/18/09 2:43 PM! 

12/18/09 2:43 PMi 

12/18/09 2:43 PMi 

12/18/09 2:43 PM! 

12/18/09 2:44 PM! 

12/18/09 2:44 PM: 

12/18/09 2:44 PMj 

12/18/09 2:44 PMi 

12/18/09 2:45 PM 

"12/18/09 2:45 PM 

12/18/09 2:45 PM! 

12/18/09 2:45 PMl" 

12/18/09 2:46 PMi " 

12/18/09 2:46 PMI 

12/18/09 2:46 PM! 

12/18/09 2:46 PMj 

12/18/09 2:47 PM. 

12/18/09 2:47 PMl 

12/18/09 2:47 PM;" 

12/18/09 2:47 PM! 

12/18/09 2:48 PM! 

12/18/09 2:48 PMj 

12/18/09 2:48 PMl 

12/18/09 2:48 PMf" 

12/18/09 2:49 PM! 

12/18/09 2:49 PMf 

3405.0 

340475] 

340379! 

12/18/09 2:49 PM! 

12/18/09 2:49 PM! 

Maximum 

3402.4! 

3402.lT 

'346272T 

3462I!"' 

'340276: 

340276: 

3402767 

3402167 

•34021!" 

'340273! 

3402737 

7340274!" 

"346272!" 

3402.67 

340117 

"3401.61' 

"340172;"" 

1461767 

3400.9;' 

3466.7!"' 

340073!" 

3466.1! 

3400.0!" 

3399.7!" 

' 339p7 

3399.1;' 

'3398.8:" 

3466721' 

3403.6; 

34 0372" 

3402.5j 

340275 

3462.5! 

13326.0! 1217.6 

1332575! 1217.8 

132979; 1217.7 

13321,6; 1217.8 

"1332172! 1218.0 

13293.5! 1218.1 

13318.5! 1218.2 

13318.5! 1218.2 

J32914!_ 

' 13291. It 

13291.1|_ 

1329176] 

14175.8 

14175.6_ 

J4175.2j_ 

1290976! 

12908.7i_ 

"1296874! 

12881.3!_ 

128jl7i]_ 

1288176 _ 

128 5377 

12853.1! 

12825.8; 

14387.41" 

1218.2 

1218.4 

13291.2; 1218.4 

1218.5 

1218.8 

13291.0; 1218.7 

'13291761 1218.7 

1329176! 1218.6 

13291.1! 1218.6 

13291.3] 1218.8 

14176.3; 1219.1 

14176.4; 1219.2 

1417676! 

1219.2 

1219.0 

1219.2 

1219.3 

1219.3 

1219.3 

12908.9] 1219.4 

1219.6 

1219.7 

1219.6 

1219.6 

1219.5 

1219.5 

12853.51 1219.6 

1219.7 

1219.7 

1219.7 
SPIKE PREPARATION LOG SHEETS 

VES018913 
Ref! No, 80/09-03-102 Date MAR 17f

 2009 

TES T CERTIFICAT E 

(CERTIFICATE OF ANALYSIS) 

PRODUCT HEXACHLOROETHANE 

FORM . WHITE, CRYSTALLINE POWDER 

(FREE-FLOWING MATERIAL) . 

COLpR SNOW-WHITE 

ODOR CAMPHOR-LIKE 

PURITY {% BY GLC) ' 99,9% • ' . 

\{Z) MELTING POINT,. 186 °C 

(3) MOISTURE (%WT.) •0.011%- . 

(4)ASH(%wf.) 0.09% ;•• 

(5) ^REE CHLORINE NIL 

(6)'WATER SOLUBLE 

:

 .'CHLORIDE (% NaCl) 

0.016% 

(7) GRADING -18 +15.0 Mesh BSS 

VES018914 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 11 -A*4 -QQ 

Crew Personnel \oOLj Shift I . 

• Scale zeroed 

Iiiiiii HHE! IIB litfPiWili i 1 BAG * miii i BAG* iHiiHi 

1 5 .6 26 3.0 51 3 . 0 76 3.0 

2 3 . 0 27 3<0 52 3 . 0 77 3.0 

3 3 . 0 28 • 3. 0 53 3.0 78 3.0 

4 3.0 29 3.0 54 3 . 0 79 3.0 

5 3-0 30 3 . 0 55 ,3.0 80 3.0 

6- 3 - 0 31 3.0 56 [ 3 . 0 81. 30 

7 3>B 32 3-0 57 3.0 82 3.0. 

8 3,0 33 3.0 58 3-0 83 3.0 

g . 34 3 - 0 59 3.0 84 S-O 

10 3-0 35 3 . 0 60 3.0 85 3.0 

n 36 3.0 61 3.0 86 3.0 

12 3 .0 37 3.0 62 3-6 87 3.0 

13 38 3,0 63 3.0 88 3.0 

14 3 .0 39 3.0 64 3 .0 89 3.0 

15 40 3.0 65 3.0 90 3-0 

16 .41 3.0 66 3,0 91 3.0 

' -17 42 3.0 67 3.ft . 92 3>b 

18 43 3 0 68- 3.0 93 3.0 

19 S . 0 44 3:0 69 3-0 94 

20 3 . 0 45 3 , 0 70 3.0 95 3.0 

21 46 3.0 71 3.0 96 • 3.0 

. 22 3.o 47 3.0 72 3.0 97 3-0 

23 5 . 0 48 3.0. . 73 • 3. 0 98 3-0 

24 ' 49 3.0 74 3 .0 99 3>0 

25 3. o 50 3D 75 3.0 100 5.0 

VES018915 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 11 -Q 9 

Crew Personnel TCiici c , ft. PrccMr , D . ^cJUlwm^ r shift 1 

Scale zeroed 

m m mmm lliilll ! •am i iHiiii i illllll i 

101 3 . 0 126 3 . 0 151 3 O . 176 3.0 

102 3 . 0 127 .3. 0 152 3 . 0 . 177 S.O 

103 3 , 0 128 3 . 0 153 3 . 0 178 

104 3 . 0 129 3 . 0 154 a o 179 3 . 0 

105 • 3.0 130 3 . 0 155 3 < 0 180 a o 

106 3.0 . 131 3 . 0 156 3 0 181 3.0. 

107 3 . 0 132 3,0 157 3 > G 182 • 3 £ > 

108 3 . 0 133 3 . 0 158 3 . 0 183 Z.O 

109 3 . 0 134 . 3 . 0 159 3 . 0 .184 . 3 . 0 

110 3 , 0 135 3 . 0 160 3 . 0 185 3 . 0 

•111 . 3 - 0 136 3 0 161 3,0 186 30 

112 3 . 0 137 . 3 . 0 162 3 . 0 187 3 . 0 

113 3 . 0 138 3 0 163 3 . 0 188 3 0 

114 3 . 0 139 •3. 0 164 3 . 0 189 3.0 

115 3 . 0 140 3 D 165 3 . 6 . 190 &.Q 

116 5 . 0 141 3 . 0 166 3 . 0 191 3 . 0 

117 3 . 0 • 142 .3. 0 167 3.0 - 192 3 . 0 

• 118 3 - 0 143 3 ; 0 168' 3 . 0 193 3 - D 

119 3 . 0 • 144 3' .0 169 3 . 0 194 3 . 0 

120 3 >0 . -145' 3 . 0 170 3.0 . 195 3 . 0 

121 3 : 0 146 3 . 0 171 3 . 0 196 3 . 0 

122 3 . 0 147' 3 . 0 172 3 . 0 197 3 - 0 

123 3 D 148 3.0 173 3 . 0 198 3 . 0 

124 3 . 0 149 ' 3D 174 • 3 , 0 199 3.0 

' 125 •3. 0 150. 3 0 • 175 3 . 0 200 3 . 0 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date U-&M - fiQ 

Crew Personnel TQitiHc R.Pnm^.S^Qymie r shift i 

Scale zeroed 

: 8A<3# BAG* WEIGHT (i.BS) BAG * WEIGHT <L6Si 

201 3 . 0 226 3.0 251 S O 276 3 . 0 

202 3 - 0 227 3 . o .252 3 - o 277 3 . o 

203 3 - 0 228 3 . o 253 s.o 278 3 . o 

204 3 . 0 229 254 3.o 279 3 . o 

205 s . o 230 S O 255 3.o 280 3 . o 

206 <3-0 231 3 . 0 256 S.o 281 S . o 

207 c3.0 232 3.o 257 3.0 282 3 . o 

208 3.0 233 3 - 0 258 3-D 283 B .O 

209 3 . 0 234 3.o 259 3.0 284 3 . o 

210 3 . 0 235 & o 260 3 . o 285 3 . 0 

211 3.0 236 261 3 . o 286 3 . o 

212 3. 0 237 3 . 0 262 3.0 287 S.o 

213 3-0 238 3.0 263 3 . 0 288 3 . o 

214 3-0 239 S.o 264 S.o 289 3 . o 

215 3.0 240 3 . ° 265 3 . 0 290 3 . o 

216 3,0 241 3 . o 266 3.0 291 3 . o 

217 3.0 242 3 . 0 267 S.o 292 S.o 

218 3.0 243 3 . a 268 3 . 0 293 3 0 

219 3.0 244 3.0 269 3 . 0 294 3 . o 

220 S O 245 c3.0 270 3*0 295 3 . o 

221 3.0 246 3.0 271 S.O 296 3 . o 

222 a o 247 3 . o 272 3 . 0 297 3 . 0 

223 3 . 0 248 3.0 273 B.O 298 3,0 

224 3 . 0 249 3 . 6 274 3.0 299 3 . 0 

225 3 . 0 250 3- 0 275 3. o 300 S . o 

VES018917 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date ll-^-Q^ i 

Crew Personnel I • WW T Shift

 1 

C

~ X V^oJca^v n Scale zeroed 

BAG * BAG# WEIGHT (LBS> BAG # HEIGHT (LBS) 

301 326 351 376 

302 327 352 3 o 377 P>-7S 

303 •VA 328 3 c > 353 A a 378 2>C\ 

304 329 3 o 354 3-A 379 d o 

305 330 a o > 355 3 - a 380 

3D6 331 356 381 

307 3 - 0 332 357 3-A 382 

308 3 D 333 3 A 358 383 

309 334 359 ,3- a 384 BO 

310 335 3 0 360 I 3 0 385 

311 336 "Pt-Cs 361 386 3 - a 

312 337 362 387 3 o 

313 338 363 388 3-f t 

314 3 C > 339 8 a 364 3 d 389 

315 340 r a 365 390 • A O 

316 341 366 391 r o 

317 342 3-C v 367 392 

318 343 RA 368 393 

319 344 3 - 0 369 ,9- a 394 3 ^ 

320 345 3-D 370 395 a o 

321 346 371 396 30) 

322 347 372 3 - 0 397 s o 

323 348 3 - 0 373 3 - D 398 

324 349 3>0 374 3 0 399. 

325 3 - 0 350 B O 375 c*7) 400 30 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date IW^VM.-Q^ 

Crew Personnel \ . Qlvftk , £ • ftcd^ ^^oUsmw - shift I 

O l Scale zeroed 

iiiiiii 1 nn liiiiiii 1111111 iiiiiiis HH 11 Hill•ISII ! ! 

401 426 3> * o 451 3.0 476 3-0 

402 3.o 427 3<0 452 477 3-0 

403 428 3.0 453 3.0 478 3,0 

404 3.o 429 2D 454 3.0 479 5.0 

405 3.0 430 3-C> 455 3.0 480 B.o 

. 406 3-0 431 3 . O 456 481 3.o 

407 432 3.0 457 3.0 482 3.0 

408 433 3.D 458 3-D 483 

409 434 459 3-0 484 

410 a o 435 3-C> 460 3.0 485 3.0 

411 3.o 436 3-0 461 3.0 486 3.0 

412 5.o 437 5,0 462 3.0 487 3.^ 

413 3.0 438 30 463 • 3.0 488 So 

414 3.0 439 3.^ 464 3>.o 489 3<o 

415 3-0 440 3-o 465 3-D 490 3 .0 

416 3 0 441 3-0 466 3.0 491 3.0) 

417 3.o 442 3><0 467 3.0 492 3.0 

418 3-0 443 3«o 468 3>.o 493 a .0 

419 444 469 3.o 494 3.0 

420 445 2-CO 470 •5.0 495 3.0 

421 3.^ 446 3<=> 471 3.0 496 3.0 

422 3.o 447 472 3-D 497 3.0 

423 3.0 448 3.o 473 2>,0 498 3.0 

424 3.o 449 3^0 474 3.0 499 3.0 

425 *>«0 450 3.0 475 3.0 500 3.0 

VES018919 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date //- 23-O^ 

Crew Personnel /•/I//A/<T'STGM J *&cSZC/k. Shift 2hid 

Scale zeroed 

liiiiiii iiiiilllli ISIill iiiliii Biifflil •Hill MIGHT (lilt) 

501 libs 526 3/6$ 551 576 3 /h3 

502 3- I b -5 . 527 • 3 /b.5 552 577 . ? JhS 

503 3 \bS 528 3/b5 553 3 ibs 578 3 /hS 

504 3 W 529 J/As 554 3/h$ 579 3 /f,3 

505 3 lb s 530 3fbl> 555 3/£5 580 3/h 

506 3 \hs 531 556 3/b? 581 3 fhS 

507 3 ibS 532 557 3/b* 582 * lb* 

508 3 \hS 533 Z/65 558 3/SS 583 3/65 

509 3 tbs 534 3/65 559 3/h£ 584 3/hS 

510 3 lb s 535 Kb? 560 3/As 585 3/b? 

511 3 \\>3 536 3/63 561 3Ms 586 3/bi 

512 Sib* 537 3'/As 562 3/bf 587 

513 3 |h * 538 3fb5 563 3/h5 588 3/b? 

514 5lb 5 539 3/6? 564 3fhi 589 3/6-7 

515 3 IV)5 540 3/As 565 3 tb$ 590 3 Ms 

516 3 \ b? 541 3/hf 566 3 Jb S 591 3fhS 

517 3 Ik r 542 Jlhs 567 3 /fc 592 3 IM 

518 3\h5 543 3 /JbS 568 3/bf 593 3/fc 

519 3 \bS 544 3/63 569 3/As 594 3/63 

520 S Ib5 . 545 3/h 5 570 3 /As 595 

521 31bf 546 3/63 571 3 //? 596 3/6? 

522 3\y? 547 ?/hs 572 3/6 597 3 /6i 

523 3 IJ>s 548 3 Ms 573 3 /6 598 3/h 

524 3 lbs 549 ias 574 3 /6 599 3 Us 

525 3 /£ S 550 3/6? 575 600 3/6? 

VES018920 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date }f-23-b><

f 

CrewPersonnel b1(/'f"y-fo-/u /'%o2bi Shift ZAICL 

Scale zeroed 

ISiilS wmmm lillllffl BAG* mmm IIMII IIBIill 

601 3/h 626 3/h 651 3/b 676 3 //> 

602 3/b 627 3/h 652 3/b 677 3 IB 

603 3 Ih 628 3/6 653 3/b 678 3/b 

604 3/h 629 3/b 654 3/h 679 3/b 

605 3/h 630 3/b 655 3/b 680 <s)b 

606 3/b 631 l i b 656 3/b 681 ?/b 

607 3 )b 632 3/b 657 3/b 682 3/b 

608 3/b 633 3/b 658 3/b 683 3/b 

609 Jib 634 3/b 659 3/h 684 3?Jb 

610 3/h 635 3fb 660 3/b 685 3lb 

611 3/6 636 3/b 661 sib 686 3 lb 

612 2 lb 637 31b 662 3 Ib 687 3 lb 

613 3/b 638 3/b 663 3/b 688 3/h 

614 3/h 639 3 lb 664 3(b 689 3 lb 

615 3/b 640 3/b 665 3/b 690 3/b 

616 3 IS 641 lib 666 3 /b 691 z(b 

617 3/h 642 3/b 667 7 Ih 692 3/b 

618 31 h 643 3/h 668 3/b 693 ?fb 

619 31k 644 3 lb 669 3/h 694 3/b 

620 3 lb 645 3/h 670 316 695 3/h 

621 Z/£ 646 3 ih 671 3 lb 696 3/b 

622 3/b 647 • 3 lb 672 3/b 697 3 Jb 

623 3 Ih 648 3/b 673 3/b 698 3/b 

624 iM 649 ?/b 674 3/3) 699 3 ff? 

625 3/b 650 3/i 675 3 / h 700 3>lb 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date /f'Z3-<5'9 

Crew Personnel Lti/ftf$TTQAIJ shift z^rd 

Scale zeroed ]/<£"? 

IHH « Ivi'BA'G '#,!•' WEIGHT, (LBS) BAG P WE!GHTj!(LBS) WEIGHT (LBS) 

701 •3 lb 726 3 lb 751 3/h 776 

702 3 Ih 727 3 ib 752 3/b 777 

703 728 3/b 753 3/S 778 3/6 

704 3 ih 729 3 lb 754 3/b 779 ? t f • 

705 3 lb 730 3 lb 755 lib 780 3/b 

706 3 jb 731 3 lb 756 3 Ib 781 3/b 

707 3 lb 732 3 lb 757 3lh 782 3/b 

708 3\b 733 3ib 758 3lb 783 3/b 

709 3 |f> 734 3 lb 759 3 lb 784 3/b 

710 3 )h 735 3/b 760 3/b 785 3/b 

711 3 ) t> 736 Jlh 761 3 lb 786 3 It? 

712 * l b 737 lib 762 3)b 787 3lb 

713 3 \h 738 lib 763 3/b 788 3 Ib 

714 739 Jib 764 31b 789 3)b 

715 3 )b 740 3 lb 765 3lb 790 3 lb 

716 ? \b 741 3 Ik 766 *lb 791 3li> 

717 3 lb 742 31}? 767 3 lb 792 3)1 

718 3 )b 743 3fb 768 3 lb 793 3\h 

719 3 Ih 744 3 / t 769 3/h 794 3\b 

720 3 lb 745 JA 770 3/b 795 3\b 

721 3 \b 746 3 Ib 771 3 lb 796 Jib 

722 3 h 747 3(b 772 3ib 797 3I& 

723 •3 I h 748 ?lb 773 ?lb 798 7 lb 

724 3 ib 749 774 3lb 799 3lb 

725 3 jb 750 Kb 775 3lb 800 3/b 

VES018922 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel shift /<£T P 

Date 

Scale zeroed 

liiiiiii n n H H msi i lliilllll H i 

801 3 LBS 826 3^5 851 3 876 3 

802 827 852 877 3 LIBS 

803 828 3L%S 853 3 a& 878 3 i&s 

804 829 854 879 3 L&S 

805 , 830 3 as 855 3 880 3 l~&3 

806 313$ 831 3 856 3 i&s 881 

807 *3l£$ 832 857 882 3 UBS 

808 

3 IBS 

833 858 , 3 i&z 883 3 /3 5 

809 < 834 859 , 3 884 3 ms 

810 835 . 3L$S 860 . 885 3 LBS 

811 3 ^ S 836 3L& S 861 886 3 L&S> 

812 3 i&s 837 3L&S 862 3 i&$ 887 , 3 

813 838 863 888 3 

814 839 864 3 i&$ 889 3 L&S 

815 840 3^ 865 890 

816 3 USif 841 866 891 3>L&5 

817 3 LB? 842 i 867 3 L&S 892 

818 3m> 843 868 893 3L&S 

819 3 LBS 844 869 3u$s 894 < 

820 845 3>^s 870 895 3 i~F<: 

821 846 , yl£S 871 -$ug>s 896 3 hB? 

822 847 31-35 872 897 3 L&S 

823 848 v 873 898 3^s824 849 3 ^ 874 3 LBS 899 3 >-&s 

S25 3 850 3 /-B 5 875 3 L^S 900 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel D, UAlAV O HI ; S. 'B&O^ZlZ} 

Date, 

Shift 

Scale zeroed 

IIIIIIH liiiiiii m m m Iiiiiii •iiiiiii Hiiill iiiiiii Iiiliii 

901 3 L&<? 926 3 951 3 L&S 976 4 ? LBS 

902 3 L.-&S 927 3L&? 952 3 LB? 977 3 LBS 

903 3 us>5 928 953 3 LBS 978 1 )~%S 

904 « 3 u&s 929 3 AB> 5 954 3 l&S 979 3 LUS 

905 3 930 955 3 LBS 980 3 LBS 

906 3> LB S 931 3 ms 956 3 LBS 981 3 up< 

907 932 3 LBS 957 3 LVS 982 3 LB<S 

908 3 >LB 5 933 3 Lib? 958 3 Lb? 983 3 LBS 

909 3 U5 5 934 3 LB5 959 3 LQ^ 984 3 Lb? 

910 , 3u&s 935 , 3 LB5 960 3 L&? 985 3 Lh* 

911 936 3L$,i 961 3L&$ 986 3 L&? 

912 3 US>5 937 *> L&? 962 3 Lbs 987 3 L&S 

913 3 i&s 938 3 L&S 963 3^-BX 988 , 3 LBS 

914 3 L&S 939 3 L&S 964 3L&? 989 

915 2>LB5 940 3 LBS 965 3 LB* 990 3 LBS 

916 941. 3 *-B>S 966 3i&? 991 3t-$s 

917 , 942 3LB>J? 967 3 19$ 992 3PB? 

918 3 LB? 943 968 3 LB* 993 3LB? 

919 3 LB 4 ? 944 3t-&> 969 3LB$ 994 3L&S 

920 945 I3L&S 970 3L?>S 995 3 LB<? 

921 3 946 3 LB $ 971 3L3S 996 3 LB? 

922 3 Le>? 947 3L$S 972 3 I & * 997 3 LBS 

923 3 LBS 948 3L%S 973 3 L&S 998 3>L£$ 

924 3 949 3i&s 974 3 w 999 3L&? 

925 3 LBS 950 3L3S 975 3 LBS 1000 ?>LPS 

VES018924 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

CrewPersonnelD, S, B ^C^ T / r r Z> 

Date 

Shift 

Scale zeroed 

NinH mmm •Mill i m llllllHI HIBill Iiiliii iiiiiiii 

1001 . 3^-BS 1026 < 3 ijss 1051 $ Lft* 1076 3/-B5 

1002 1027 < 3JLBS 1052 3 LBS 1077 3 t-BS1003 -3 LBS 1028 3/.BS 1053 3 IBS 1078 3, LB? 

1004 3 LBS 1029 3 i^s 1054 3 L&S 1079 3 LBS 

10C5 t 1030 3i&s 1055 3 iss 1080 3 LR f 

1006 . 3 1031 3u$<? 1056 3 LB? 1081 3L&* 

1007 3> LB? 1032 3 u$s 1057 3 135 1082 3 LS? 

10O8 3 LB< 1033 3L%>? 1058 3 LBS 1083 4 LB? 

1009 3 us? 1034 3 ±.j$? 1059 3 ISS 1084 3 L$S 

1010 . 3 IRS 1035 3 LBS 1060 3 LB? 1085 3 

1011 , 3LZ? 1036 3L5S> 1061 3 1086 {3 LPS 

1012 3 USLS 1037 % LB< 1062 3 L&S 1087 3L$7 

1013 3L&,<> 1038 3LRS 1063 3L&5 1088 3L#S 

1014 3l&S 1039 3XBS 1064 3 LBS 1089 A IMS 

1015 3>L&<? 1040 3 LB? 1065 3 LBS 1090 3 LBS 

1016 (3/35 1041 3u&s 1066 ALB * 1091 3>L1^? 

1017 , 3k& 1042 3L&* 1067 3 LBS 1092 3LBS 

1018 , ILK? 1043 3LBS 1068 3 LBS 1093 3 — 5 

1019 % up? . 1044 3i-BS 1069 3 LBS 1094 3 LBS1020 3 LBS 1045 3L&? 1070 3 LBS 1095 3 L-&S 

1021 3uBS 1046 3L&? 1071 3*-BS 1096 3 ts? 

1022 3>L&? ' 1047 3J-B$ 1072 3 L-pc 1097 3 LBS 

1023 3L£S- 1048 3 UBS 1073 3 LPS 1098 3 ms 

1024 3L&? 1049 3 L ^ 1074 3 LP? 1099 

1025 3 ABS: 1050 3 V&S- 1075 3 L&S 1100 3 LBS 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

CrewPersonnel ft UNMAhUtJi ; 5> ^BCt^P] Shift /<ST 2^ 

Scale zeroed ^^S^ 

IHHIIII 11HHBHR 1 liflll I i 1111111 WEIGHT (LBS) Iiiiiii iiffliiii 

1101 3 LB? 1126 , ^AB? 1151 3 AE? 1176 3 ±B<> 

1102 3 LB?- 1127 t 1152 3^&? 1177 3 LB? 

1103 3 LSS- 1128 3 LBS 1153 3^B? 1178 3*~BS 

1104 3 L&* 1129 3 LBS 1154 3LB? 1179 3 LB? 

1105 3 LBS 1130 3 Lfc< 1155 c3 LB? 1180 3^~Bs 

1106 1131 1156 3AP,? 1181 3L.BS 

1107 3 1132 3 i&s 1157 3u&5 1182 3L-BS 

1108 3 is? 1133 3> LBS 1158 3 LBS 1183 3 LBS 

1109 3 LV><> 1134 3L&? 1159 3L^ 1184 3 LB? 

1110 3 L&S 1135 3LSS 1160 , ^L&S 1185 3LB? 

1111 £ LB* 1136 3LBS 1161 , 3 LBS 1186 3LB^ 

1112 1137 3LBS 1162 < ^7Jp>? 1187 3>LB<5 

1113 3i~B<t 1138 3u&$ 1163 , 3L&? 1188 3L-BS 

1114 3 LB? 1139 3AB? 1164 3L&S 1189 3LBS 

1115 Pi LPS 1140 3)~9? 1165 SLBS 1190 SLB^ 

1116 3 L&<; 1141 3i3S 1166 3 LB? 1191 3LR? 

1117 3 LB * 1142 3LJ*.< 1167 3 LBS 1192 3L$^ 

1118 3 LB? 1143 3LBT 1168 3LBS 1193 3 LBS 

1119 3L&? 1144 3 LBS 1169 3 LBS 1194 3 »~B ? 

1120 3>L&5 1145 3L&? 1170 3 LB<Z 1195 3LBS1121 3 LBS 1146 ALB? 1171 *>L3? 1196 

1122 3>L&iZ 1147 3LBS~ 1172 < ^^LBS 1197 3^&s 

1123 . 3LKS 1148 3 LBS 1173 3 LBS 1198 3L8? 

1124 3 LBS 1149 3 LBS 1174 1199 3LZS 

1125 3iSS 1150 3 LBS 1175 3 1200 3<-Bs 
HEXACHLOROETHANE SPIKE BAGS - Target Weight; 3.0 pounds Date//~ MzP CJ"-, 

Crew Personnel T)* M/JI M fi/ZfJ/, S. TK&ZfCtt. Shift /« y , D 

Y< W/^/rLx/ Scale zeroed \JS<> 

mmm ;1SI31 lilllll Hill 11 1111111 IllSiii 

1201 3 LBS 1226 , 4 LB? 1251 3L&<? 1276 3>J-B? 

1202 . °>LBJT 1.227 3 LBS 1252 3 z^-r 1277 3 LB? 

1203 3 LBS 1228 3 LB* 1253 . ILB? 1278 3 LBS 

1204 3 LSS 1229 3 L&? 1254 3 LBS 1279 3 LBS 

1205 , 3 LBS 1230 3 LBS 1255 3 LBS 1280 3 LPS 

1206 , 3 1231 3LB* 1256 3 L&S 1281 3 LBS 

1207 3 23-7 1232 3 LB< 1257 3LM 1282 3LB3 

1208 3L$S 1233 3LBJS 1258 3 LB? 1283 3LBS 

1209 (3L&5 1234 3LB<T 1259 3 L$Z 1284 3L$S 

1210 3L&J? 1235 3 AB-T 1260 3 LB? 1285 3 LBS 

1211 3 LBS 1236 3LRf 1261 3 LB? 1286 3 LBS 

1212 3 LBS 1237 3 LBS 1262 c3 LBS 1287 3 LB? 

1213 3 LBS 1238 3L£.<> 1263 3m? 1288 3 LBS 

1214 3 LBS 1239 3L$S 1264 3LBJ 1289 3 LBS 

1215 3 LBS 1240 3 Lp< 1265 % LBS 1290 3) LB? 

1216 3LB.$ 1241 3 LB? 1266 3*-B? 1291 3 LB?. 

1217 3LB* 1242 3 LBS 1267 3 LBS 1292 3Lfr? 

1218 3L&S 1243 3>LP>? 1268 1293 3L&S 

1219 3LB* 1244 3^9S 1269 3 LB? 1294 3L&? 

1220 3 LBS 1245 3 LB? 1270 3 LBS 1295 3 IBS 

1221 3uf« 1246 3 L&f 1271 3) LB? 1296 3 LBS 

1222 3^BS 1247 3 LB< T 1272 3 LBS 1297 3 iss 

1223 3LB<Z 1248 3LB<? 1273 3 13? 1298 3 LP<> 

1224 3LRJT 1249 3LRS 1274 3 &3 1299 3 LB? 

1225 \3LQS 1250 3 LBS 1275 3 LBS 1300 3^BS 
HEXACHLOROETHANE SPIKE BAGS-Target Weight: 3.0 pounds 

Crew Personnel 

Date/ / 

Shift /-ST 73 

Scale zeroed 

lililillil mmm IliiS, 

WEIGHT' <LB§|: Iiiiiiii mmm 

1301 3 LB? 1326 , 3 LB? 1351 A LB? 1376 3 ABf 

1302 3 LBS 1327 3 LB ? 1352 3 LBS 1377 , 3 LB? 

1303 3L&<> 1328 3 LB ? 1353 3 LBS 1378 3 LB? 

1304 3 LBS 1329 3 LB? 1354 3 LB? 1379 3 LB? 

1305 1330 3 LB? 1355 3 Lft*7 1380 3 LB? 

1306 3L%? 1331 3 LB? 1356 3 LBS 1381 3 LR? 

1307 3 LB? 1332 3 LB? 1357 3 LB? 1382 3 L&S 

1308 3 LB? 1333 3 LB? 1358 3 LBS 1383 

1309 3i~&? 1334 3 LB? 1359 3 LBS 1384 3 L-B S 

1310 3^B>? 1335 1360 3) LBS 1385 3LB? 

1311 1336 3 LBS 1361 3 LBS 1386 3LBS 

1312 3 LBS 1337 3 LB? 1362 A IB? 1387 3*-br 

1313 3 LB? 1338 3LB? 1363 3>L&? 1388 3L&<? 

1314 3 LB? 1339 3*&5 1364 3LBS 1389 3 L&<S 

1315 3 LB? 1340 . 3 LBS 1365 1390 3 LB? 

1316 3LBS 1341 3LU? 1366 3 LBS 1391 3LB^ 

1317 3 LBS 1342 3LB? 1367 3LB< 1392 3LB? 

1318 3 1343 3 L&? 1368 3 IB? 1393 3 its 

1319 3 LBS 1344 3 LB? 1369 3L&< 1394 3 LBS 

1320 3>i&? 1345 ALB ? 1370 3L<B,? 1395 3LQS 

1321 3 LB? 1346 3 LB? 1371 3LPS 1396 3 LB? 

1322 3 LB? 1347 3 LB-T 1372 3 LB? 1397 3LB<? 

1323 3 LBS 1348 3 LB? 1373 3LB<; 1398 3 LB? 

1324 3 LBS 1349 3 LBS 1374 3 LB? 1399 3LB>S 

1325 3 LBS 1350 3 LBS 1375 3 LBS 1400 3L^ 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel b< MPlAUdfiitCy f 7"7 DdOV^ J Shift 

Scale zeroed 

iliiiiiil mmmm IIKIIiiliii liiiiiii Hlfflili liiiiiii itmaigtimmrrmiium 

1401 1426 3L&* 1451 3LB<Z 1476 3 ups 

1402 3 LB? 1427 3 L&S 1452 3 LB? 1477 3 LB? 

1403 3 LB? 1428 3

 Lh* 1453 3 LB<?> 1478 3 LB? 

1404 31&? 1429 1454 3 LB? 1479 3 LB? 

1405 3 LB? 1430 3 i&? 1455 • 3 L%< 1480 .3 LBS 

1406 3 1431 3 V&t 1456 3 LB? 1481 3 LB? 

1407 3 LB S 1432 3 L&g 1457 3 L&? 1482 3 LB? 

1408 3 LB? 1433 % LBS 1458 3 LB? 1483 3 LPS 

1409 3 LB? 1434 3 L&S 1459 3 LB? 1484 , 3}LBs 

1410 3) LB£ 1435 3 LBS 1460 3 L&f 1485 3 L&r 

1411 3 LBS 1436 3 LB? 1461 3 LB? 1486 3 LBS 

1412 3 LB? 1437 3 L&? 1462 3 LB? 1487 3L$S 

1413 3 LB? 1438 3 ^s 1463 3>LBf 1488 QL& S 

1414 3 LB? 1439 % Lp? 1464 3 LBf 1489 3 LBS 

1415 3 LB? 1440 3LB?- 1465 3 LBS 1490 3) Lb? 

1416 3 LB? 1441 3 LBS 1466 3AB? 1491 3 LB? 

1417 3>LB<- 1442 3 LB? 1467 3t-B? 1492 3 LB? 

1418 3 L&Z 1443 3 LB? 1468 3 LB? 1493 3 LB< 

1419 ( *> LBS 1444 3 LB? 1469 3 ws? 1494 3 LB? 

1420 < 3 JLB * 1445 3 Lb? 1470 3 LB? 1495 , 3>L-B?T 

1421 3 1446 $LBS 1471 3 LB? 1496 c 3 LBS 

1422 3 LB? 1447 3 LBf 1472 3 LB? 1497 3 LB? 

1423 3 LB? 1448 3 L&S 1473 3 LB? 1498 3 LB? 

1424 3> L$$ 1449 3 LB? 1474 5 LBS 1499 3 LB? 

1425 3 AV : 1450 3 LBS 1475 3 LBS 1500 3 LBS 

VES018929 
HEXACHLOROETHANE SPIKE BAGS - Target Weight 3.0 pounds Date /I 

Crew Personnel J>> l^AUWj'6 H lcM j 7^ £>OV ^ 2 , Shift /?H~ X> 

V« \A/f<&Tl l / Scale zeroed V^SZ 

iiiiiill i wmm mmm WEIGHT (LBS) WEIGHT (LBS| llllili l 

1501 3 x& 1526 3 LP>? 1551 , 3 L^,< 1576 3 Lp? 

1502 3 LBS 1527 3 ISS 1552 3 LR? 1577 3 LB? 

1503 3 XB 5 1528 3 /LBS 1553 P> LB? 1578 3 LBS 

1504 , 3 LBS 1529 3L&>S 1554 3 LP? 1579 3LB& 

1505 • 3 L&S 1530 3L^S 1555 3 LB? 1580 ( 3LB? 

1506 , 3 LBS 1531 3 LBS 1556 3 LB? 1581 3L&S 

1507 , 3l&S 1532 f^LB< 1557 ^LB? 1582 ^>Lfr? 

1508 3LB^ 1533 , 3 (SB< 1558 3) LB? 1583 , ^L3 ? 

1509 3 LBS 1534 < 3LB<; 1559 3ut? 1584 3 IBS' 

1510 3) LBS 1535 3L&S 1560 3 L&? 1585 < 

1511 < 3 LBS 1536 3 LB* • 1-561- 3>LB? 1586 3LBS 

1512 1537 3LB>? 1562 3>L;B? 1587 3 LBS •»: 

1513 3 LBS 1538 3)L&S '1563 3u$< 1588 3 LBS 

1514 3 LBS 1539 3LBS 1564 3i&r 1589 3 L&<? 

1515 3 LBS 1540 2>LBS 1565 3 ib? 1590 3 LBS: 

1516 3 LB? 1541 3 LBS 1566 3 LB? 1591 3 L&? 

1517 3 LBS 1542 3 LBS 1567 3 LBS 1592 

1518 3 LBS 1543 1 3 LBS 1568 1593 , 

1519 3 LB< 1544 ' , 3 LBS 1569 1594 

1520 3 LB? 1545 3 LB? 1570 3 LBS 1595 3LB< 

1521 3 LBS 1546 3 LBxS 1571 3 LBS 1596 , 3L&S 

1522 3 ms 1547 3 m 1572 3 L& r 1597 

1523 3 LBS 1548 « 3 LBS • 1573 3LBS 1598 3 /35 * 

1524 3 LBS 1549 < 3LB<S 1574 3LB< 1599 3LBT 

1525 3 LBS 1550 3ta s 1575 3 ms; 1600 . 3 LBS 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds Date 

Crew Personnel D / (4AU\ Vf>/V/s~Lf77 \/<£:gf Shift 2> 

V . \kJ[S£LK/ : Scale zeroed y^£ ^ 

[liilll iWflitBffilllimfu] ISiili! IHIlPS) WEIGHT'<LBS) ..'I'BA'G WEIGHT\LB:! 

1601 3 LB? 1626 3 LBS 1651 3 LVf 1676 3 LIZ? 

1602 ^ 1627 , 3 LB? 1652 3 LB? 1677 3 LBS 

1603 3>LVS 1628 $>LBS 1653 3 LBS 1678 - s 

3 LBS 1604 3 LB? 1629 3 LBS 1654 3 h-br 1679 3 LB? 

1605 3 LB? 1630 3LB>? 1655 3 LB? 1680 , 3 LBS 

1606 3LB>^ 1631 3 LBS 1656 3LB< 1681 3 L&? 

1607 3 LB? 1632 3 LBS 1657 , 3 LBS 1682 3LB<T 

1608 3 LB? 1633 3 LBS 1658 3 LBS 1683 , 3LB<T 

1609 3 LP? 1634 3 LBS 1659 3 LBf 1684 3 LBS 

1610 3 LPS 1635 3L&? 1660 3 LB? 1685 3>L&f 

1611 3 LP? 1636 3 LBf 1661 3 LBf 1686 3LBf 

1612 3 LP? 1637 3 LBf 1662 3 us>.r 1687 3 LBS 

1613 . 3LB? 1638 3 LB? 1663 3LB< 1688 3m< 

1614 3 LB<T 1639 

o ' 

K. *5 LBS 1664 3 LBf 1689 3 LBS 

1515 < 3 LB< 1640 3L&? 1665 3LP><: 1690 3^r 

1516 3 LB? 1641 3i^f 1666 3LB< 1691 

1517 3LP>? 1642 1667 3 LP< 1692 3 LBf 

1518 3 LB? 1643 3 LB? 1668 / 3 A B T 1693 

—* > 

2? LBS 

1S19 . 3 LBS 1644 3 LB? 1669 3 LB? 1694 3 iter 

1S20 3 LBS 1645 3-L9S 1670 3 LBf 1695 3LU?-

1S21 3 LB? 1646 3 LBS 1671 1696 3LBS 

1522 3 LB? 1647 P) LR>< 1672 3 LBS 1697 3 LBS 

1S23 3 LB? 1648 3 LBS 1673 , 1s$>s 1698 Sn ' 

3L&<? 1524 3 LBf 1649 3 i&r 1674 3>LB,f 1699 3ds 

1525 3 LBS 1650 3 LB? 1675 3 m 1700 3 L^S 
1 V 

HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel D>HM AMflhffctf. T,T>£>\{£:&} 

y wis^iy 

shift /s r J P 

Scale zeroed 

Hi mam iiiiiiii Iiiiiiii lllllllli HNM H BAG rf ftBWT.LRB, 

1701 1726 3 A&< 1751 3$ LB? 1776 . ^>Ln? 

1702 3 /-BIT 1727 3 LB? 1752 3L&? 1777 3 LB? 

1703 1728 . 3 IBS 1753 3 LBS 1778 3 IB S 

1704 3 /.s-r 1729 3 LB? 1754 3L&>? 1779 3 ^ B S 

1705 3 2_B,<? 1730 3 LB? 1755 3 LBf 1780 i %LBs~ 

1706 3 UQf 1731 3 LB? 1756 3 LBS 1781 t 3>LB<-

1707 3 i*r 1732 3 LBS 1757 3LBS 1782 , 3uB?r 

1708 3L®4 1733 • 3 LBS 1758 3 LB? 1783 3LT*,< 

1709 3 i&s 1734 3 L B ? 1759 • 3 LB,? 1784 3 LP)<S 

1710 3 L.&S 1735 3 LBS • 1760 3>UB< 1785 , 3 LB? 

1711 3 1736 . 3L&? 1761 , 3 LBS 1786 , 

1712 1737 3LB?? 1762 ( 3>L&S 1787 

——1 ' / 

3LBS_ 

1713 3 L B ? 1738 

E — ' > 

3LB><? 1763 3/JB? 1788 t 3L&? 

1714 3>£^-9 1739 3L&? 1764 , 3&s 1789 3LBS 

1715 3 i-m<; 1740 3LB? 1765 3)Lp<r 1790 , 3L&S 

1716 3 ue>c 1741 3 LB? 1766 , 3tfts? 1791 3L&S 

1717 3 L.BS" 1742 3LB^ 1767 n LR? 1792 , 3LBS 

1718 ^ L9? 1743 1768 L3L&S 1793 3 LPS 

1719 3 LB? 1744 3 LB? 1769 — y 

3 LRS 

1794 . 

1720 ' 3 Lg? 1745 3 y&s 1770 3L%S 1795 3?m<; 

1721 3 LBS 1746 3 LBS 1771 ( n LBS 1796 , 3LR<? 

1722 3 LBf 1747 3 IBS Mil 1797 «• ^LB<T 

1723 3 LB? 1748 °>up>? 1773 2>L£,C 1798 3>^f 

1724 3LV? 1749 3>L&< 1774 3 ^ s 1799 

1725 3 LB? 1750 , 3LBZ 1775 3LB< 1800 3 LBS 

VES018932 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

CrewPersonnelT^^A//4l^A/ ^ T> $X>V£%F 

Date U'M'Cfj 

Shift /%T~ TS> 

Scale zeroed "y' £S^?S 

iiiiii i IIIIIII III Iiilii i HHHHR iimiif! iiiHil l 

1801 3LUS 1826 , 3^&r 1851 L ^ J--&T 1876 3/&>? 

1802 • 3LB? 1827 , 3ip?> 1852 * 3/.T3? 1877 3 LBS 

1803 1828 f ZT- -iips 1853 3 Lpf 1878 3>u*r 

1804 . 1829 3LB< 1854 3L&S* 1879 3 LBS 

1805 3ip r 1830 1855 , 3 LBS 1880 3 LB? 

1806 3}L&? 1831 3L3< 1856 3 LB-? 1881 3 Lbs 

1807 1832 3 LB? 1857 3 LB? 1882 3

 L ^ 

1808 1833 3LBS 1858 c3 L&S 1883 3 LBS 

.1809 1834 3L&S 1859 , 3 LBS 1884 3 LB< 

1810 1835 , 3)L&-<r 1860 3 LBS 1885 3 LBS 

1811 < ^>LB? 1836 < 3 LB? 1861 3 LB? 1886 3 ISBS 

1812 r 3L&? 1837 t 3 £9? 1862 3 ^ s 1887 3L&SI 

1813 < 3 /a5 - 1838 1863 3P>$ 1888 

1814 1839 3AB? 1864 3 LPS 1889 3) LB? 

1815 3 LB? 1840 3L&? 1865 3/L&? 1890 3>L2Zsr 

1816 < -3 /.s<- 1841 ^3 LB? 1866 <^LB* 1891 3b LB? 

1817 r- 1842 3 LB? 1867 3 ivsr 1892 3LZS 

1818 1843 •3 LB? 1868 3MB? 1893 r 3 IB? 

1819 1844 , ^>LBS 1869 1894 3 LBf 

1820 3>L&S 1845 i 5 LBf 1870 3 Lb? 1895 . 3 LBS 

1821 1846 3 LB? 1871 3*&r 1896 3L&S 

1822 3i&c 1847 3 LB? 1872 3LBT 1897 3LB<T 

1823 — — ~ ^ — 

3 L&S 

1848 3LB< 1873 3 LB? 1898 

1824 3L$>C 

1849 3 LB? 1874 3LB< 1899 

1825 1850 < 3 LBS 1875 3^B? 1900 3LB>S~ 

VES018933 
HEXACHLOROETHANE SPIKE BAGS - Target Weight: 3.0 pounds 

Crew Personnel J^'HAl AVW(<~M l~H V^V^, 

Date/^c ^ f 

Shift JL> 

Scale zeroed 

IIIIII I IIIIII I USUI Hiatal IIIIII I IIIIII I 

1901 3L$? 1926 %LBS 1951 3 AT3 < 1976 , 3lBf 

1902 3 LB*? 1927 r ^LB? 1952 3LBS 1977 3 LBS 

1903 3 LB? 1928 3 LBS 1953 3L&<? 1978 3 LB? 

1904 3 LB? 1929 3L&? 1954 2>L&r 1979 3 LBS 

1905 3 LB? 1930 3 LBS 1955 3ms 1980 3 LBS 

1906 3 L&? 1931 3 Z-Bs 1956 3 LB? 1981 3 L & < 

1907 3 LBS 1932 3LB^ 1957 3>LB? 1982 3 LpS 

1908 3 LBf 1933 3LB<S 1958 3LTK 1983 3 LBS 

1909 3iv><? 1934 3LB? 1959 , ^LBS 1984 3LB<; 

1910 3 LBS 1935 3LB>S> 1960 , v>L&r 1985 3LS>^ 

1911 3LB>? 1936 3LB$ 1961 3 LP,? 1986 3LBS~ 

1912 . 1937 3LB? 1962 -•3i&? 1987 %L&<? 

1913 3 LBS 1938 3us>? 1963 <3t&? 1988 3isp>?' 

1914 3>L&? 1939 3L®>5 1964 1989 3b LU1915 3 LBS 1940 3 LbS 1965 3 LIBS' 1990 

1916 ' 3LBe? 1941 3 LB? 1966 3 LBS 1991 3h>m<-. 

1917 3 LB? 1942 3LBS 1967 3 L B ? 1992 3>L^?' 

1918 3LBS 1943 3 LBS 1968 3 LBS 1993 3 LB? 

1919 3L&X 1944 3*>BS 1969 3 L B < 1994 , 3 LUS 

1920 °)^ S 1945 3LB>S 1970 3 L B < 1995 3 LBf 

1921 3LBS 1946 3L&S 1971 3 LBf 1996 3p&<r 

1922 3z&f 1947 3LB>f 1972 3 LBS 1997 3>L&? 

1923 3 LBS 1948 

—* s 

3 LBS 

1973 3 LBS 1998 3LB>? 

1924 3 LB? 1949 „ °)LB>S 1974 3LBS 1999 3^BS 

' 1925 < 3 LB? 1950 3*&<z 1975 3LBS 2000 3 L B ^ 
TEST DATE: \^/\\»fc°i 

TEST UNIT: Mc A 

TEST START TIME: UMfe-OoiT fj ^ £*ycT 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

. a 

a 

> • 

. ^ • 

a. 

a • 2L 

D~ 

a • Z2, 

at • 

3** 

^ • 

a . 5'S 

as 9* 

VES018935 
TEST DATE: / JJ* l&f 

TEST UNIT: ±t"4 

TEST START TIME: \\W iTWET \\\(tfA 

Receiver* Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

) Spike (3.C 

Ibs.) 

) 

; Receiver S Charge # Hex 

Spike (3.C 

Ibs.) 

Hex-

) Spike (3.C 

Ibs.) 

> 

57 

m i * 

,5 mi 

l MI X 

?* 

m& 

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mi 

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\yn 

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(355 

a ° 6 lj3b ,2^ 

(•a. 

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VES018936 
TEST DATE: pAt,/ ^ 

TEST UNIT: & M' 

TEST START TIME: f VftjLV 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.C 

Ibs.) V-3 

Receiver # Charge # Hex 

Spike (3.Q 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3 \m 

1 3 ^ 13 3S-4c>^ 1413 

1.33^ 141^ -

1330 1334 

"< |41 A 

• 141,3 

\3P2> & 1HSU 

l>Gl 13 \ 3 f4bS 

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13 "ii ' 

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ft':--. 

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4 

VES018937 
TEST DATE: \i»/tV»/0^ 

TEST UNIT: tP<4 

TEST START TIME: 

Receiver* Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

> Spike (3.C 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex ' 

Spike (3.C 

Ibs.) 

• 

L H TO 

f >• 

HIE 

mo 

Mil 

/WO 

IHHU W4 

l&U M\o 

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1 

MIL $92 • 

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€15 . 

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VES018938 
TEST DATE: 

TEST UNIT: 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

Spike (3.C 

Ibs.) 

£i 

Receiver # Charge # Hex 

Spike (3.C 

Ibs.) 

Hex 

Spike (3.C 

lbs.) 

IK 

S&S ... 

W • A 

to 

:?l 

»•'*' ?•'•* 

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1% 

v\\ -

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3« 

688 "fife 

& 

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VES018939 
3S~ 54.1 0-3 

TEST DATE: I^/H A H 

TEST UNIT: ^ 

TEST START TIME: 

Receiver # Charge* Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

z 

z 

z 

z 

z 

z 

1 

I & 

z 

z 

z 

2 

Z z 4( 

Z 3S-3b\0 2. 

Z IS 

£ 

z - a. 

z. 

z~ 

u 

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2~ 2%. 

I 

2 . a 

2 it 

I 

2. i 

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VES018940 
TEST DATE: /2//7/0 ? 

TEST UNIT: #1} 

TEST START TIME: SMT i-Kl/p"* 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

lbs.) 

Hex 

Spike (3.0 

Ibs.) 

z m it*, 67 

2 J 45 ,8k 

2 3 %m 

2 Z %i% 

9 3 w 

1 3 

2 • 5 i , */ 

I 7 

% ? l\S 

Z 7&, LL 

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2. |f. J m #08 

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If1; 3 H91 

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.3 ? ii% 

3 S37" / iM //iS. 

5 £3S n J ins in \ 

VES018941 
TEST DATE: U/l l /(tf 

TEST UNIT: ff 4 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

lbs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge* Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3 UV3- \M !l*,^3 CL 

<• 

(US 

• 

u m n i b • S3. 

i m n n 

i n * 

t\-lO 

u s * 

I two 

150 

l\S3 I\S1 

W M . A 

\ \ % 1155 

3 II P . 

3S-3M0 

- • 

-

VES018942 
TEST DATE: <°/ n

/ < # 

TEST UNIT: # H 

TEST START TIME: b^ f Sf&fcc 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

4 \m \m 

-

* ( 

UOl 

• • 

\n cays 

• 

1105 

I'l a* • 

n o w 

H 1 3 Usui 

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1/5'/ 

II 07 

fi (lib 

//A3 - It 15 

11 oH 

//V 7 mo 

in* v. //3 5 

\w\ 

n n 

-• -

VES018943 
TEST DATE: |S>/n fo7 

TEST UNIT: Jt^M; 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

1 

f — •'• 

m <M 

^•71 > 

<m 

<M 

1*1 B ? T S O 

% 5 

f 

S ^S 

^% -

<*% 

J 

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1 °m -

% J?-, r %\ 1 

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w 

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VES018944 
TEST DATE: 

TEST UNIT: #i" 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

assy© 

, * 

^1 

-

• 

4 ^ 

-

VES018945 
TEST DATE: \^/l $/0 9 

TEST UNIT: # 4 

TEST START TIME: 1 >3& U># (KT 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3^4C3b 

i. 

ZL 1' 

fk 

2i 

2> 

&~ • 

3v 

> 

> 

VES018946 
TEST DATE: 1^L/\%/0^ 

TEST UNIT: 4* *-f 

TEST START TIME: °\ \ SfJ . l\e\ / fw\ 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

lbs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

ibs.) 

T t9. 

* 90S 

1b \ 

* 

%°\ 

-

% 3 913 

• > 

4 

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IMS 

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I ioo 

io<H 10 » 

I0£7 

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ica\ lO*S 

/oi£ 

ton 

10&O 

3L IG($ rotS 

Si 

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Ma, H 

VES018947 
TEST DATE: U /ifc M (§> 

TEST UNIT: 4* ^ 

TEST START TIME: ! 4 6 . S'l\tt fc&F 

Receiver # Charge # Hex 

Spike (3.0 

ibs.) 

Hex 

Spike (3.0 

ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

3V&0 

1 0 ^ (OS? 

m to 

10 (b3 • 

a 

to 4$ 

I0SS 

/ 

ft>S4 • 

10SO 1051 

1044 10 51 

IOH5 

10 30 

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torn \m -

io 13 m (4 

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iO OS 10 i s • 

(0 i o n 

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io io io i s 

10M - M r 

lOOys j37 

35^10 "S (043. I02A 

• 2 Mr 

VESO18948 
TEST DATE: lWl&/ 6

T 

TEST UNIT: ±t 4-

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

lbs.) 

Hex 

Spike (3.0 

Ibs.) 

^ 7 * 

>\ 

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a % 

a m 

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1 

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VES018949 
TEST DATE: 

TEST UNIT: # 4 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

+ •J2 it>3 

an? . \ • 

\ 

z\\< 

• 

-

-2t<W 

.2( ot>" • 

• 

• 

• 

•i. -

J207J 

,2 (15" • 

VES018950 
TEST DATE: R 

TEST UNIT: -8s*f 

TEST START TIME: 

Receiver # Charge # Hex 

Spike (3.0 

lbs.) 

Hex 

Spike (3.0 

Ibs.) 

Receiver # Charge # Hex 

Spike (3.0 

Ibs.) 

Hex 

Spike (3.0 

Ibs.) 

i n 

Jell 

2.6 <?3 

VES018951 
Wast e Fee d Profile s 

VES018952 
Report! R7 00B 

DATE: 11/30/OS 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

BUSINESS: ASCHER DANIELS MIDLAND, C0-

DEPT i 

ADDRESS 1: VITAMIN E PLANT 

ADDRESS 2: 37O0 E. DIVISION STREET 

-Y/ST. . : BSCATUR 

'ACT. . : DAVID BROADHACKER 

IL 62526 

WASTE NAME: SOLVENT RECOVERY 

PROCESS GENERATING WASTE; SOLVENT RECOVERY 

SKIP. NAME: WASTE FLAMMABLE LIQUIDS, N.O.S 

ADDL. DESC: (ACETONE, METHANOL) 

Version 06.04 

TWI-028691 

SELLING REGION LAB - MRL 

NUMBER : 142-B-789 

PHONE : 217/451-4392 

EXPIRES 01/11/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: ILE000021550 

STATE EPA ID..: 1150155346 

EPA STATUS CHE RESTRICT 

SALES OFFICE. . i RPK 

CHEMICAL COMPOSITION 

NON-TRI CHEMICALS 

EMULSIFIED OIL 

UNIT DESCRIPTION 

ACETONE 25 35 % 

HEPTANE 25 35 % 

METHYL ALCOHOL 25 35 % 

WATER 1 38 % 

BENZENE 1 38 PPM 

15 25 % 

EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physica l State...: Liqui d 

Flash. Point : > = 200 CL 

pH : 04.0 - 09.0 

Color : VARIES 

Odor : NONE 

Layers .....: Single Layer 

Specifi c Gravity. : 0.950 - 1.150 

Free Liquid s : 99 - 100 

Cyanides ...: < 5 PPM TOTAL 

Sulfide s < 3 PPM TOTAL 

PCB's ppm. Regulated by 40 CFR 761: 

Phenolics : < 10 PPM 

% Taxable' : DOT UN/NA NBR: UN1993 

Treatment Codes..: T07 

CRQ RPT QTY : Materia l Class: 

EPA Permit EXP: 

Hazard Class..... : 3 

State Codes : 090001 

Benzene : 38 NESHAP; Controlled Benzene NESHAP 

Packing Group. .. .: II " 

Process Codes....: CBC 

Cert o f Dstrc t R<j: 

Federa l Codes: DOOl D018 F003 

NEO. GREY GLOVES 

TYPE C RESPIS CONST PLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NirRILE (INNER GLOVE) 

BENZENE NESHAP CONTROLS REQUIRED; NO CERT 

CANCER SUSPECT AGENT: BENZENE ' 

Inhalation : 2 Dermal: 2 

DOT PROPERTIES 

Oral : 2 Flammable: 0 Health: 0 

Waste Type 

Form Code 

B21S 

1 

CHARGE CODE: NS 

BENZENE NESHAP CONTROLS REQUIRED; NO CERT 

COMMENTS 

REVIEWED FOR MACT METALS 

VES018953 
'Report! R700B 

DATE! 09/15/09 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

BUSINESS: 

DEPT 

ADDRESS 1: 

ADDRESS 2: 

^tY/ST. . : 

ACT. . ! 

C0WOCO PHILLIPS COMPANY 

WOOD RIVER REFINERY 

900 SOUTH CENTRAL AVENUE 

ROXANA IL 

TONY SHAN 

WASTE NAME: PRIMARY SOLIDS DEBRIS 

PROCESS GENERATING WASTE: PROCESS SEWER CLEANING 

SHIP. NAME: HAZARDOUS WASTE, SOLID, N.O.S 

ADDL. DESC: RQ(F037, F03B) 

Version 06.04 

TKI-330469 

SELLING REGION LAB 

NUMBER : 143-4-771 

PHONE 618 255 2374 

EXPIRES : 04/29/11 

STATUS APPR FOR SERV 

FEDERAL EPA ID: ILRO0O077115 

STATE EPA ID..: 1190905013 

EPA STATUS : CHK RESTRICT 

SALES OFFICE..: TWI 

CHEMICAL COMPOSITION 

CALCIUM CARBONATE 

WATER 

PETROLEUM HYDROCARBONS 

NON-TRI CHEMICALS 

COMBUSTABLE SOLIDS SAPER/PLASTIC 

INERT SOLIDS SOIL/ROCK ETC 

MIN - MAX 

0 

0 

0 

0 

69 

UNIT DESCRIPTION 

10 % 

10 % 

2 % 

25 % 

99 % 

METALS 

Arsenic as. As 

Cadmium as Cd 

Lead as Pb 

Mercury as Hg 

Selenium as Se 

Chromium Hex 

Nicke l as Ni 

Thallium as 71 

EP TOX/TCLP 

mg/l 

mg/l 

mg/l 

mg/l 

mg/l 

PHYSICAL CHARACTERISTICS 

Physical State...: Soli d 

Flash Point : > = 200 CL 

pH 04.0 - 09.0 

Color. : BLACK/VARIES 

Odor : NONE 

Layers : Single Layer 

Specifi c Gravity. : 0.000 

Free Liquid s : 0 - 1 

Cyanides : < 5 PPM TOTAL 

Sulfide s : < 3 PPM TOTAL 

PCB's : ppm. Regulated by 40 CFR 761: 

Phenolics : < 10 PPH 

% Taxable : DOT UN/NA NBR: NA3077 

Treatment Codes..: T07 

CRQ RPT QTY : 1 Materia l Class; 

EPA Permit . : EXP: 

Hazard Class : 9 

State Codes i 090001 

Benzene ..: > 10 NESHAP: Controlled Benzene NESHAP 

Packing Group....: II I 

Process Codes....: BSH 

Cert of Dstrc t Rq: 

Federal Codes: F037 F038 

HANDLING 

NEO. GREY GLOVES N-DEX INNER GLOVE SARANEX 

Contains Benzene TYPE C RESPIR CONST FLOW 

INDEX/BLUE NITRILE (INNER GLOVE) 

BENZENE NESHAP CONTROLS REQUIRED; CERT REQUIRED WITH EVERY LOAD 

DO NOT ADD TO TAB, DOES NOT CONTAIN >10% WATER + 

POT PROPERTIES 

Inhalation: 2 Dermal: 2 Oral : 2 Flammable: 0 Health: 0 

SUMMARY 

Waste Type B409 

Form Code 1 

COMMENTS 

CHARGE CODE: NS REACTIVE CATEGORY: B--CONTAINS MERCURY 

REVIEWED FOR MACT METALS BENZENE NESHAP CONTROLS REQUIRED; CERT WITH EVERY 

LOAD. DO NOT ADD TO TAB, DOES NOT CONTAIN >10% WATER 

NEED WEIGHT PE UNTIL 12-31-09 PRICE INCREASE EFF 1/22/09 

ONE TIME LDR NOTIFICATION RECD FOR F037 10/27/06 GENERATOR LDR FORM IN TM FILE 1/18/07 

VES018954 
Report: R7 008 

DATE: 11/24/OS 

ONYX ENVIRONMENTAIi SERVICES, 

WASTE PROFILE SUMMARY 

BUSINESS: 

DEPT 

ADDRESS 1 

ADDRESS 2 

"••"T.Y/ST. _ 

\CT. . 

IMPERIAL CLEANERS 

2210 WISCONSIN AVE 

NEW KOLSTEIN 

Km WALKER 

WASTE NAME: TETRACHLOROETHYLENE CONTAMINAT ED SOIL 

PROCESS GENERATING WASTE: CLEANUP OF TETRACHLOROETHYLENE SOIL FROM DRY CLEAN 

SHIP. NAME: HAZARDOUS WASTE, SOLID, N.O.S 

ADDL. DESC: R.Q{TETRACHLOROETHYLENE) 

VerBion 06.04 

TWI-096110 

SELLING REGION LAB - MRL 

NUMBER : 144-0-059 

PHONE 920/B98-4800 

EXPIRES 10/01/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: WID9B1540040 

STATE EPA ID..: 9550019999 

EPA STATUS CHK RESTRICT 

SALES OFFICE..: CSK 

CHEMICAL COMPOSITION 

TETRACHLOROETHYLENE 

SOIL 

NON-TRI CHEMICALS 

PAPER, PLASTIC, 

» - MAX UNIT DESCRIPTION 

0 10000 PPM 

95 100 % 

0 5 % 

EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physica l State...; Soli d 

Flash Point ; > = 200 CL 

pH 05.0 - 10.0 

Color : BROWN 

Odor : NONE 

Layers Single Layer 

Specifi c Gravity.: 0.000 

Free Liquid s : 0 

Cyanides : < 5 PPM TOTAL 

Sulfide s : < 3 PPM TOTAL 

PCB's : ppm. Regulated by 40 CFR 7 61: 

Phenolics, : < 10 PPM 

% Taxable : DOT UN/NA NBR: NA3077 

Treatment Codes..: T07 

CRQ RPT QTY : 100 Materia l Class; 

EPA Permit : EXP: 

Hazard Class 9 

State Codes : 090001 

Benzene : . NESHAP: 

Packing Group Il l 

Process Codes....: BSL 

Cert of Dstrc t Rq: 

Federal Codeas F002 

HANDLING 

NEO. GREY GLOVES N-DEX INNER GLOVE SARANEX 

TYPE C RESPIR CONST FLOW 

INDEX/BLUE NITRILE (INNER GLOVE) 

kapplers chem tape 2 

Inhalation : 2 

DOT PROPERTIES 

Oral : 2 Flammable: 0 Health: 0 

Waste Type 

Form Code 

B301 

1 

CHARGE CODE: NS 

PE EVENT EXPIRES 12-31-09 

COMMENTS 

REVIEWED FOR MACT METALS 

VES018955 
Report! R7 0 0 8 

DATEi 11/21/09 

BASF CORP 

. .HANNIBAL PLANT 

315 0 HWY J J 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

MO S3 4 E l 

BUSINESS: 

DEPT : 

ADDRESS 1: 

ADDRESS 2l 

''.Y/ST. . i 

\CT..: 

WASTE NAME: IMI-2 HERBICIDE ORGANIC WASTE SPILL CLEANUP 

PROCESS GENERATING WASTE: ORGANIC WASTE SPILL CLEANUP 

SHIP. NAME: HAZARDOUS WASTE, SOLID, N.O.S 

ADDL, DESC: (TOLUENE, METHANOL) 

Version 0 6.04 

TWI-097B02 

SELLING REGION LAB 

NUMBER, 105-7-002 

PHONE 

EXPIRES 10/27/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: MOD050226075 

STATE EPA ID..: 9290019999 

EPA STATUS..,.: CHK RESTRICT 

SALES OFFICE..: RPK 

CHEMICAL COMPOSITION 

METHANOL 

TETRAHYDROFUSAN 

TOLUENE 

WATER 

NON-TRI CHEMICALS 

SOIL AND GRAVEL 

SPILL CLEAN-UP DEBRIS 

HERBICIDE BY-PRODUCTS 

0 

0 

.1 

0 

95 

0 

0 

UNIT DESCRIPTION 

.1 % 

.1 % 

2 % 

1 % 

99 % 

1 % 

.1 % 

EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical'State...: Soli d 

Flas h Point : N/A CL 

pH : 04.0 - 09.0 

Color : BROWN 

Odor : NONE 

Layers : Single Layer 

Specifi c Gravity.: 0.000 

Free Liquid s : 0 

Cyanides : < 5 PPM TOTAL 

Sulfide s : < 3 PPM TOTAL 

PCB's : ppm. Regulated by 40 CFR 761: 

Phenolics : < 10 PPM 

% Taxable : DOT UN/NA NBR: NA3077 

Treatment Codes..: T07 

CRQ RPT QTY : Material Class: 

EPA Permit : EXP: 

Hazard Class : 9 

State Codes : 090001 

Benzene : NESHAP: 

Packing Group Il l 

Process Codes....: BSL 

Cert of Dstrct Rg: Y 

Federal Codesz DOOl F003 F005 

NEO. GREY GLOVES 

TYPE C RESPIR CONST FLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NITRILE (INNER GLOVE) 

Inhalation : 2 Dermal: 2 

DOT PROPERTIES 

Oral: 2 Flammable: 0 Health: 0 

Waste Type 

Form Code. 

B301 

1 

CHARGE CODE: NS 

PE 10-28-10 

COMMENTS 

REVIEWED FOR MACT METALS 

REPORT WEIGHT 

VES018956 
Report: R7008 

DATE: 11/30/OS 

ONYX ENVIRONMENTAL SERVICES, 

WASTE PROFILE SUMMARY 

VEOLIA ES TECHNICAL SOLUTIONS 

7 MOBILE AVE 

BUSINESS: 

DEPT 

ADDRESS 1 

ADDRESS 2 

"TTY/ST.. 

•ACT. . 

WASTE NAME: ON-SITE RAINWATER £ ASH WATER 

PROCESS GENERATING WASTE: COLLECTION OF ON-SITE STORMWATER & PRECIPITATION; 

SHIP. NAME: HAZARDOUS WASTE, LIQUID, N.O.S 

ADDL. DESC: 

Version 06.04 

TWI-TW2S19 

SELLING REGION LAB 

NUMBER : 110-9-722 

PHONE : 

EXPIRES : 11/30/14 

STATUS : CONTRACT NOT IN PLACE 

FEDERAL EPA ID: ILD098642424 

STATE EPA ID..: 1631210009 

EPA STATUS....: CHK RESTRICT 

SALES OFFICE..: RPK 

ATER 

CHEMICAL COMPOSITION 

WATER 

NON-TRI CHEMICALS 

ASHWATER 

MISC SOLIDS, WASTE RESIDUES 

MIN - MAX UNIT DESCRIPTION 

99 100 % 

SO % 

1 % 

METALS EP TOX/TCLP 

Arsenic as As 

Cadmium as. Cd 

Lead as Pb 

Mercury as Hg 

Selenium as Se 

Chromium Hex 

Nicke l as Ni 

Thallium as Tl 

mg/l 

mg/l 

mg/l 

mg/l 

mg/l 

PHYSICAL CHARACTERISTICS 

Physica l State...: Liqui d 

Flash Point : > = 200 CL 

pH : 02. 0 - 12.5 

Color : VARIES 

Odor : NONE 

Layers : Single Layer 

Specifi c Gravity.: 0.950 - 1.150 

Free Liquids : S3 - 100 

Cyanides : <: 5 

Sulfide s . : < 3 

PCB's : ppm, Regulated by 

Phenolics '.: < 10 

% Taxable DOT UN/NA NBR: NA3082 

Treatment Codes..: T07 

CRQ RPT QTY Materia l Class: 

EPA Permit : EXP: 

Hazard Class.....: 9 

State Codes 090001 

Benzene : NESHAP: 

Packing Group : III 

Process Codes. . . .: 

Cert of Dstrct Rq: 

PPM TOTAL 

PPM TOTAL 

40 CFR 761: 

PPM 

Federal Codes: D003 D007 D008 D004 D005 D006 D009 DOlO D011 D012 D013 D014 D015 D016 D017 D018 + 

SITE GENERATED WASTE 

DOT PROPERTIES 

Inhalation: 0 Dermal: 0 Oral : 0 Flammable: 0 

TWI Signed Addendum 

SITE GENERATED 

VES018957 
TWI Laboratory Analysis Report 

Receiver #: TK304 Visual Inspection: Glove Box / Hooded Feeder 

# of Drums: 1 

Date: 6/29/2001 

Profile #:ZZZZZZ 

Generator: TRADE WASTE INCINERATION 

Descript: 

Process Code(s): 

Drum Storage Compatibility 

Profiled DOT Hazard Class 9 

P = Pass F-Fait 

8A 8B 4/5 

Sample Number 

Drum Rep / Comp 

303022_[_IL00000001 

1/ ~

1 

IIIIIIII 

303022 

Free Liquid (%) IIIIIIII 

303022 

Profile Conform Date Initials 

Pumpable NO 

IIIIIIII 

303022 wwwwv Yes No 11/06/09 MI 

Layers/Phases -% Ea. \\\\\\\\\ ^ 

Color 

Turbidity wwwwv 

Viscosity L X 

Physical State ^\\\ 

Water Miscibility 

Add. Description 

Water Reactivity 

Radiation Screen =BKG X 

Flam. Pot Screen See Flashpoint X 

pH Screen 5 at 100 pent 2-12.5 X 

Oxidizer Screen 

Paint Filter Test ^\\\ 

Cyanide Screen wwwwv ^\\\ Sulfide Screen wwwwv 

Incidental Odor wwwwv ^ 

Specific Gravity 1.01 11/04/09 MI 

BTU/Lb 1570 11/04/09 BD 

% Chloride 1.2 11/04/09 KD 

Flash Point - Deg F 01/01/00 

PCBs ByGC - mg/kg <50ppm 11/06/09 

pH by Meter 01/01/00 

Arsenic mg/kg 4.768 0 

Beryllium mg/kg 4.765 0 

Cadmium mg/kg - 4.765 0 

Chromium mg/kg 4.805 0 

Lead mg/kg 4.784 0 

Mercury mg/kg 0.056 0 

Profile Review for Appendix WAP-C Consitituents by: 

Date: 

Add. Comments: The data in the sample information section(6/29/2001)is date profile 777777 was created. 

VES018958 
Waste Tracking System 

File Inventory Print Approvals Chemist Receiving Laboratory Tank Farm Process Planning Window Billing Help 

I ?* Laboratory Sample Analysis 

-Sample Number030.22 Update Cancel 

j

-

 Edit Mode Update and 

Submit to Lab 

Manager 

J 

Exit 

f Approval 

Status 

I 3 

Manifest IL0O0D0O01 Sample Status L 

View Profile 

Summary 

Comments 

View PDW 

Cancel Submit 

• Sample Status CodesReSample = S <v 

PCB suspect = P 

lnLaboratoiy = L 

Metals = E 5 . 

Pending Lab Manager Approval = M 

Discrepant = D ^ 

Rejected = R 

Conforms/Accepted = A J£ 

Layers/Phases iTeits! 

p Water Reactivity 

r No RXN T RXN: I 

Radiation Screen 

T =BKG r >BKG: 

• Flam. Pot Screen 

f~ Neg r Pos r BOC 

•pH ScreenValue p p 100^ j= 10£ 

r Oxidizer Screen -

r Neg r Pos 

j Specific Gravity 

i BTU/lb 

I 

I % Chloride 

: Flash Point (Deg. F) 

PCBs bv GC (mg/kg) 

PCB GC Comment 

PCBs-Screen (ppm) 

Value 

jl.01 

jl570 

1.2 

Date 

jl1/4/2009 

|11/4/2009 

ji 1/4/2009 

Initials 

|MT 

[BD° 

w 

J1/1/1900 

1V1/190Q 

"3 

jl/1/1900 

r Paint Filter Test 

r Pass T Fail V V-FaS V N/A 

• Cyanide Screen 

f~ NegP PosjTM N/A T Cyantesmo 

• Sulfide Screen 

r Neg r Pos T N/A 

2,4 S - T (ppm) 

Silvex (ppm) • 

j1/1/19D0 

PCP Screen (ppm) 

pH by Meter 

PUT r EC jl/1/1900 

r IOOX r i(Ki/i/i9oo 

rMetalsP° S4.784 

As (4.768 

Adjust Metals 

• Incidental Odor 

r No r Yes: 

rAshfc2123 

VES018959 
TWI Laboratory Analysis Report 

Receiver #: TK310 Visual Inspection: Glove Box / Hooded Feeder 

# of Drums: 1 

Date: 6/29/2001 

Profile #: 777777 

Generator TRADE WASTE INCINERATION 

Descript 

Process Code(s): 

Drum Storage Compatability 

Profiled DOT Hazard Class 9 

P = Pass F = Fail 

SA 8B 4/5 

Sample Number 

Drum Rep / Comp 

3015561 ILOOOOOOOl 

1/ 

m i n 

301556 

Free Liquid (%) m i n 

301556 

Profile Conform Date Initials 

Pumpable NO 

m i n 

301556 \\\\\\\ W Yes No 10/01/09 SL 

Layers/Phases -% Ea. \\\\\\\ W 

Color .xWWW W 

Turbidity 

Viscosity L X 

Physical State wwwwv 

Water Miscibility \\\\\\\w 

Add. Description 

Water Reactivity w w w \W\ N 

Radiation Screen =BKG X 

Flam. Pot. Screen See Flashpoint X 

pH Screen 3 at 100 pent 2-12.5 X 

Oxidizer Screen \\\\\\\ W 

Paint Filter Test \\\\\\\ W 

Cyanide Screen wwwwv 

Sulfide Screen \\\\\\\\\> 

Incidental Odor 

Specific Gravity 0.83 10/01/09 SL 

BTUTLb 9600 10/01/09 MT 

% Chloride <0.5 10/01/09 JF 

Flash Point - Deg F 01/01/00 

PCBs By GC - mg/kg <50ppm 10/01/09 

pH by Meter 01/01/00 

Arsenic mg/kg 0 0 

Beryllium mg/kg 0 0 

Cadmium mg/kg 0 0 

Chromium mg/kg 0 0 

Lead mg/kg 0 0 

Mercury rng/kg 0 0 

Profile Review for Appendix WAP-C Consitituents by: 

Date: 

Add. Comments: The data in the sample information section(6/29/2001)is date profile 777777 was created. 

VES018960 
1 5 » Waste Tracking System Wi'KCSfe.^ ^ 

Fie Inventory Print Approvals Chemist Receiving Laboratory Tank Farm Process Planning Window Bil }ing Help 

«* I uborufpry Sdmple Analysis J?-Sample NumberR=tiiew Update Caned 

r EditModB 

Update and 

Submit to Lab 

Manager 

Manifest IL00000001 Sample Status W 

•Approval— 

Status View Profile 

Summary 

Comments 

ViewPDW 

Cancel Submit 

•Sample Status CodesReSample=S 

PCBsuspect = P 

In Laboratory = L 

Metals »E 

Pending Lab Manager Approval = M 

Discrepant = D 

Rejected = R 

Conforms/Accepted » A _ 

Layers/Phases •Testa; 

j- Water Reactivity 

rRadiatio No RX

n Screen

N r- RXN: j= 

T =BKG T >BKG: 

• Flam. PoL Screen 

P Neg P Pos r BOC 

•pH ScreenValue I5 

•Oxidizer Screen1-

7 1005! r 10* 

T Neg T Pos 

r Paint Hlter Test — 

P Pass r Fail P V-Fail | ~ N/A 

• Cyanide Screen 

P Negl " Pos P N/A P Cyantesmo 

-Sulfide Screenr Neg T Pos r N/A 

r Incidental Odor-— — 

T No P Yes: JValue 

Specific Gravity 

BTU/lb 

% Chloride 

Flash Point peg. F] 

PCBs by GC (mg/kg) 

PCB BC Comment 

PCBs-Screen (ppm] 

0.85 

9610 

<0.50 

Date Initials 

111/15/2003 |MT 

|11/15/2C03 (MT ' 

111/15/2009 1MT 

(1/1/1900 

11/1/1300 

"3 

1/1/1900 

2.4,5-T (ppm) 

Silvex (ppm) 

1/1/1900 

PCP Screen fppmj 

pH by Mela 

P KIT P GC |1/1/1S0D 

P 100XP KK|1/1/1S00 

r Metals— 

As fg" 

Be jo" 

Cdja 

D jb" 

K

 Jo" 

Naj T 

Adjust Metals 

•AshXVES018961 
C M S Performanc e Evaluatio n 

VES018962 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON; 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

UNIT #4 

QUARTERLY 

PT 

300 

PRESS TRANSM 

KILN HOOD 

FTRNSP 

300 

F015 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

REMARKS: Reranged 1/19/96 PROCESS-SP: 

INSTL-RMKS: 1/2"x 29" SS PIPE inside Kil n INST-SP: 

SPEC-RMKS: ACTION: 

S/N: I/O NUMBER: 

CALIBRATION NOTES 

ROSEMONT 

1151DR2F 

-9.0" TO 1.0" WC 

4-20 ma 

Atmosphere = 18.40 ma 

Set Dampening pot ful l CW 

Nl:25 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT.VALUE INSTRUMENT READING 

Before Calibration ./ „ , A 

- J'wC ° ¥• <TM/7 

/"tic DO.o,f^M 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: ^ee^/en/ (!&••/$'> o n 

Performed by:. _ Date: V-P. -0? Time:/ ^ 

JB Place: 

CALSHEET.WDB (Field or Shop) 

_AM 

VES018963 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

QUARTERLY 

PT 

324 

PRESS TRANSM 

SCC OUTLET 

FLD 

324 

F015 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

ROSEMONT 

1151GP3E 

-15" TO +5" 

4-20 MADC 

WC 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

6 O0C 

After Calibration 

INSTRUMENT READING 

Before Calibration „ ,\ 

o3 

3 n ~o3 /»A 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: /^QCC/tt Jfjf ^ Date: #~/^-09 Time:/-* :/0 

JB Place: 

CALSHEET.WDB (Field or Shop) 

PM 

VES018964 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

PDT 

439 

DP TRANS 

BAGHOUSE PRESSUER 

WAPC 

437 

F017 

W/GAS CLEANING TRAIN 

NORTH/EAST BAGHOUSE 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

FOXBORO 

823 DPI 

0-15" WC 

4-20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affix a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

. Before Calibration . 

rf 4/-Q2 *A 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: (VX- fci'k*, Date :/7- fl-d f Time:^2<n APpPM 

JB Place: 

CALSHEET.WDB (Field or Shop) 

VES018965 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

PDT 

440 

DP TRANS MANUFACT: FOXBORO 

BAGHOUSE PRESSUER MODEL: 823 DPI 

WAPC 

437 

F017 

W/GAS CLEANING TRAIN 

NORTH/CENTRAL BAGHOUSE 

MANUFACT 

MODEL 

SCALE 

CALIB-IN 

CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

0-

4-

15" WC 

20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration ~ ^ ^_ 

2 J.99/*4 

•// . 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: /^j'1^

1

 Date: Time: 

JB Place: 

CALSHEET.WDB (Field or Shop) 

PM 

VES018966 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

PDT 

441 

DP TRANS 

BAGHOUSE PRESSUER 

WAPC 

437 

F017 

W/GAS CLEANING TRAIN 

NORTH/WEST BAGHOUSE 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

FOXBORO 

823 DPI 

0-15" WC 

4-20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

A

 BEFOR E

 Callbratio n

 t/ 'stf-M^ 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: //^ / rr' Date: // ~

 01 Time: ^-CTO 

JB Place:_ 

CALSHEET.WDB (Field or Shop) 

PM 

VES018967 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

PDT 

442 

DP TRANS 

BAGHOUSE PRESSUER 

WAPC 

437 

F017 

W/GAS CLEANING TRAIN 

SOUTH/EAST BAGHOUSE 

MANUFACT 

MODEL 

SCALE 

CALIB-IN 

CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

FOXBORO 

823 DPI 

0-15" WC 

4-20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration * / .„ A & ^ 0/ /#A 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: fl/* steed Crd 

Performed by: /?/?*>/ n,c IS/tn Date^/JL - rf Time: 

JB Place: : 

CALSHEET.WDB (Field or Shop) 

VES018968 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

PDT 

443 

DP TRANS MANUFACT: FOXBORO 

BAGHOUSE PRESSUER MODEL: 823 DPI 

WAPC 

437 

F017 

W/GAS CLEANING TRAIN 

SOUTH/CENTRAL BAGHOUSE 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

-15" WC 

-20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

INPUT VALUE 

0 

CALIBRATION REPORT 

Before Calibration 

INSTRUMENT READING 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: J2-

Performed 'by: J-Ja-e.LaC [d m Date: / I "0*1 Time: PM 

JB 

CALSHEET.WDB 

Place: 

(Field or Shop) 

VES018969 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

PDT 

444 

DP TRANS 

BAGHOUSE PRESSUER 

WAPC 

437 

F017 

W/GAS CLEANING TRAIN 

SOUTH/WEST BAGHOUSE 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

FOXBORO 

823 DPI 

0-15" WC 

4-20 MADC 

CALIBRATION NOTES 

USE PNEUMATIC CALIBRATION BENCH WITH MANOMETER AND LOOP 

CALIBRATOR. INPUT PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

6 

0 

Before Calibration 

INSTRUMENT READING 

After Calibration 

4 / 

CALIBRATION SOURCE REFERENCE 

Coranents: 

Performed by: J/n&L-£L* fSfion T>ate:J/-J2~o9 Time:/fi^30 SMI 

JB Place: 

CALSHEET.WDB (Field or Shop) 

VES018970 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

WIT 

001 

WT TRANS 

SHREDDED SOLIDS 

FTRNSP 

1 

F012 

W/SOLIDS FEED SYSTEM 

E12665900A 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: HI:5 

TOLEDO 

8140 

0-3000# 

0-3000# 

4-20 MADC 

CALIBRATION NOTES 

Check scale,.digital Calibration per. Toledo instructions. 

Then with no weight on scale adjust analog zero. (NOTE: HMI 

wil l not display numbers less than zero). Next add weight 

= to 10% are more of scales range, then adjust analog span, 

to indicate weight on scale, as read on HMI screen. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

n 

INSTRUMENT READING 

Before Calibration 

WO 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: J^JT^TJ^l3^J$ Date: M -&-Q ? Time: H'OQ AM(H 

JB 

CALSHEET.WDB 

R 

Place: 

Held hr Shop) 

VES018971 
TWI INSTRDMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

UNIT #4 

QUARTERLY 

WIT 

014A 

WT TRANS 

DRUM FEED 

FTRNSP 

W/DRUM FEED NEMATRON 

S/N: 42601574NS 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: HI:35 

TOLEDO 

8140 

0-1,000 lb. 

0-1,000 lb. 

4-20 MADC 

CALIBRATION NOTES 

Check scale, digita l Calibration per. Toledo instructions. 

Then with no weight on scale adjust analog zero. (NOTE: HMI 

wil l not display numbers less than zero). Next add weight 

= to 10% are more of scales range, then adjust analog span, 

to indicate weight on scale, as read on HMI screen. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INSTRUMENT READING 

Before Calibration yr\ 

so 

INPUT VALUE 

0 

5t> 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by:. . Date: Time: _AM^?) 

JB Place: 

CALSHEET.WDB ( fFiel)d or Shop) 

1 

VES018972 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

QUARTERLY 

WIT 

014B 

WT TRANS 

AUX. DRUM FEED 

FTRNSP 

NEW AUX DRUM FEED 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

TOLEDO 

8140 

0-200# 

0-200# 

4-20 MADC 

CALIBRATION NOTES 

Check scale, digita l Calibration per. Toledo instructions. 

Then with no weight on scale adjust analog zero. (NOTE: HMI 

wil l not display numbers less than zero) .. Next add weight 

= to 10% are more of scales range, then adjust analog span, 

to indicate weight on scale, as read on HMI screen. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE > INSTRUMENT READING 

Before Calibration 

so 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Date:. Time: 3:

Performed by 3>S~"" AM (pi 

JB 

CALSHEET.WDB 

Place:. 

((Field br Shop) 

VES018973 
TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

QUARTERLY 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

55 OA 

Tribo 

Baghouse Leak Detection. 

FLD 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

Auburn 

TRIBO.dgd 

O-lOOOpa 

0-1000pa 

4-20ma 

CALIBRATION NOTES 

Disconnect the input cable at the BNC connector on the input 

card, and check for zero. Use Auburn, Triboflow, file d test 

unit, model 2902, to input a Pico-Amp signal of 500pa and 

record these values. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

Before Calibration 

INSTRUMENT READING 

O 

TOO pg 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: /f/p r KJ^t/PizX? 

Performed by 

JB 

CALSHEET.WDB 

Date 

7^ 

M 

Place: 

VES018974 
~^U4 (IC4034) PAGE 1 OF 1 

QUARTERLY CARBON INJECTION PREVENTIVE MAINTENANCE CHECK SHEET 

PASS FAIL 

1 Disconnect A C Power to the Digi Drive. / 

2 Inspect A C & Motor drive screw terminal connections for 

signs of wear or corrosion and check that they are tight. / 

3 Replace the two Digi Drive fuses J 

4 Verify any external safety switches or lockouts are still operation / 

5 Remove Screw feeder cover 8& blow out carbon 8B dust. J 

6 Inspect Gears 8s Belts for wear or damage. / 

7 Chec k Operation of Motor 8s Gears for abnormal noise or movement. j 

3 Replace any needed parts, and list any parts used i n comment / 

COMMENTS: 

Name: Date :// - 6~o1 Time: 3 ' ? 0 A M 01 

QUARTER.4 

11/1/06 KF 

VES018975 
TWI INSTRDMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

ANNUAL 

FT 

129 

FLOW TRANS 

PCC LOW GRADE 

P-BMS 

129 

F013 

W/BMS 

101499 

WDF X-10 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

MICRO MOTION 

DS100S 128 

0-7,000 #/HR 

4-20 MADC 

Flush process piping, connect water hose to upstream side of 

flow meter, set control system to appropriate rate control, 

and read totalizer, flow water into a container and compare 

the toltalize r reading to the measured amount in container. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

-0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

t— .. , A .Before Calibration \/i / n 

b lbs. ^er rmn- W 1 n-Hh. l^t.b lbs 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: Ca(iic<a'fifir\ needrJ. 

Performed by:. Date: Time: 2.''00 AM (PM^) 

JB Place: ,"^~=:\ 

CALSHEET.WDB (Field)or Shop) 

I 

VES018976 
TWI INSTRDMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

ANNUAL 

FT 

145 

FLOW TRANS 

PCC SLUDGE X-12 

P-BMS 

145 

F013 

W/BMS 

MANUFACT: MICRO MOTION 

MODEL: DL100S-SS 

103056 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

0-8,000 #/HR 

4-20 MADC 

Nl:28 

CALIBRATION NOTES 

Flush process piping, connect water hose to upstream side of 

flow meter, set control system to appropriate rate control, 

and read totalizer, flow water into a container and compare 

the toltalize r reading to the measured amount i n container. 

-0-. l • lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

i _ ,, ' , A Before Calibration Q qi 

10 IDS., p>r mm, \i)rl rwn _ 111 ibs* 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: No pf i bra f• Ors YlzerJeo/ 

Performed by: E^/DiO Date: \ ~L^Q\ Time: ^j'-OO m g ) 

JB Place: 

CALSHEET.WDB (Field)or Shop) 

VES018977 
TWI INSTRDMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

FT 

212 

FLOW TRANS 

WDF TO X-22 

S-BMS 

212 

F014 

W/BMS 

101775 

MANUFACT 

MODEL 

SCALE 

CALIB-IN 

CALIB-OUT 

PROCESS-SP 

INST-SP 

ACTION 

I/O NUMBER 

MICRO MOTION 

D1D00S-SS 

0-7,000 #/HR 

4-20 MADC 

CALIBRATION NOTES 

Flush process piping, connect water hose to upstream side of 

flow meter, set control system to appropriate rate control, 

and read totalizer, flow water into a container and compare 

the toltalize r reading to the measured amount i n container. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

*Q.l lb/hr- jO^o 

CALIBRATION REPORT 

INPUT VALUE 

IS- lbs. 

INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: IVd C«.l^rgtfitoyv needed. 

Performed by: flflX^ 0 Date:) 2.-^-0 °l Time: H:QO AM(gh 

JB Place: 

CALSHEET.WDB {Field) or Shop) 

7 

VES018978 
TWI INSTRDMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

ANNUAL 

FT 

138 

FLOW TRANS 

PCC AQ LIQ X-l l 

P-BMS 

138 

F013 

W/BMS 

1155343 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CALIBRATION NOTES 

MICRO MOTION 

D100S-HY 

0-6,000 #/HR 

4-20 MADC 

Flush process piping, connect water hose to upstream side of 

flow meter, set control system to appropriate rate control, 

and read totalizer, flow water into a container and compare 

the toltalize r reading to the measured amount i n container. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

lb/hr JV?o 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

I f— i j r I -Before Calibration , u <y u 

IS lis-- pgr m\r\ \b<r I mt^. /"-o IhSAfter Calibration 

CALIBRATION SOURCE REFERENCE 

comments: t^o cal)]oroJr\sir\ nteJeJ. 

Performed by:. Date: Time: [ r O&twTjPM 

JB Place: 

CALSHEET.WDB (Fieldior Shop) 

VES018979 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

TT 

317A 

TC ASSEMBLE 

SCC OUTLET 

FLD 

317 

F015 

TC WELL INCONEL 601 24" 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

CHESSEL 

3510 

Type R TC 

0-3000 F 

4-20 MADC 

24" INCONEL 

N1-.51 

601 WELL 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a temperature signal of 500 deg F. and 2,000 deg.F. 

input of transmitter, then verify this single in control 

room. 

at 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

<.0.l lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

j r 

2050 lOOO 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: _ 

Performed by: CkffhW^^ Date: /hi7-<3 % T_ m e : [/• PT AM^PM ) 

JB Place: 

CALSHEET.WDB (Field or Shop) 

R 

VES018980 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

TT 

317B 

TC ASSEMBLE 

SCC OUTLET 

FLD 

317 

F015 

TC WELL INCONEL 601 24" 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: Nl:52 

CHESSEL 

3510 

Type R TC 

0-3000 F 

4-20 MADC 

24" INCONEL 601 WELL 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a temperature signal of 500 deg F. and '2,000 deg.F. at 

input of transmitter, then verify this single in control 

room. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration m „ 

,-^00 ^ret> 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: Date: f(~~t 7-^^Time: A /*7 AM 

JB Place: f 

CALSHEET.WDB XFiel&or Shop) 

R 

VES018981 
LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRDMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

TAG: TT 

305A 

PYROMETER 

KILN OUTLET 

FLD 

305 

F015 

44-99-F-1-0-1 

55" Target Tube 

MANUFACT: IRCON ' 

MODEL: M0DLINE4 44-99-F-1-0-1 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: Nl:51 

Type R TC 

0-3,000 deg 

4-20 MADC 

EMIS. 85% 

CALIBRATION NOTES 

Install factory calibrated Pyrometer. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by:. 

JB 

CALSHEET.WDB 

S 

. Date:. 

Place: 

Time: _AM PM 

(Field or Shop) 

VES018982 
TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

TAG: TT 

LOOP: 305B 

DESCRIPON: PYROMETER 

SERVICE: KILN OUTLET 

LOCATION: FLD 

LP-SHT: 305 

P&ID: F015 

REMARKS: 44-99-F-1-0-1 

INSTL-RMKS: 55" Target Tube 

SPEC-RMKS: 

S/N: 

MANUFACT: IRCON 

MODEL: M0DLINE4 44-99-F-1-0-1 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: Nl:52 

Type R TC 

0-3,000 deg 

4-20 MADC 

EMIS. 85% 

CALIBRATION NOTES 

Instal l factory calibrated Pyrometer. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by:. 

JB 

CALSHEET.WDB 

S 

_ Date:. 

Place:. 

Time: _AM PM 

(Field or Shop) 

VES018983 
TWI INSTRUMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

ANNUAL 

TT 

404A 

TC TRANS 

TC GAS OUTLET 

WAPC 

404 

F016 

W/GAS CLEANING TRAIN 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: Nl:114 

MOORE 

TIY/K2-0-1-4-20MA 

0-1500 deg F 

Type K TC 

4-20 MADC 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a temperature signal of 200 deg F. and 1,000 deg.F. at 

input of transmitter, then verify this single in control 

room. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

2 Q ^ O Before Calibration <2P§ & 

( D0O D fOOO ° 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: flU Cftii ^ o u (0^€ P 

Performed by: Date: U ' ' "1 Time: //.JltCmJM 

JB Place: , 

CALSHEET.WDB f^ieldjbr Shop) 

I ^ 

VES018984 
TWI INSTRDMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

ANNUAL 

TT 

404B 

TC TRANS 

TC GAS OUTLET 

WAPC 

F016 

W/GAS CLEANING TRAIN 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: Nl:115 

MOORE 

TIY/K2-0-1-4-20MA 

0-1500 deg F 

Type K TC 

4-20 MADC 

CALIBRATION NOTES 

Use cold junction compensated thermocouple calibrator to 

input a temperature signal of 200 deg F. and 1,000 deg.F. at 

input of transmitter, then verify this single in control 

room. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

_ r> Before Calibration _ _. 

?00 P 2oo ° 

| DO Q& . Ve^ - 1003 * * H 

After Calibration 

CALIBRATION SOURCE REFERENCE 

Comments: _ 

Performed by: Date: //-/7-€> Trime: 11'^ ^(ffiQpM 

JB Place: 

CALSHEET.WDB (Field or Shop) 

I 

VES018985 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS : 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

FT 

559A 

dp Transmitter 

STACK FLOW 

FLD 

559 

F018 

PSE averaging pitot tube 

East side of Stack 

1222931 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: N001:0093 

Automation Service 

11S1DR2F22B3 

0-1.73 i n wc 

0-55,000 ACFM 

4-20 MADC 

CALIBRATION NOTES 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

O

Before Calibration / , , ~* , 

H. I ^ r n A 

Q

After Calibration i± ~ zLQ 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: fj^jrT.^ y f^Pf Date:i___L_9_ Time:J______!g)PM 

JB 

CALSHEET.WDB 

Place:. 

(Field oi(Shop)" 

VES018986 
TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

FT 

559B 

dp Transmitter 

STACK FLOW 

FLD 

559 

F018 

PSE averaging pitot tube 

North side of Stack 

1222931 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: 

Automation Service 

11S1DR2F22B3 

0-1.73 i n wC 

0-55,000 ACFM 

4-20 MADC 

N001-.0093 

CALIBRATION NOTES 

-e-:i lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

O Before Calibration / i t •-> / 

1:7-3 " U C l^^GnnA 

Q After Calibration ^ Q ^ 

CALIBRATION SOURCE REFERENCE 

Comments: 

Performed by: _ Date: Time: ll-'OOA AM} PM 

JB Place: 

CALSHEET.WDB 

VES018987 
TWI INSTRDMENT CALIBRATION RECORD 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

UNIT #4 

ANNUAL 

FT 

425 

MAG METER 

X-18 DIL SLURRY 

WAPC 

425 

F016 

W/GAS CLEANING TRAIN 

MANUFACT: 

MODEL: 

SCALE: 

CALIB-IN: 

CALIB-OUT: 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: HI:112 

Fischer & Porter 

1475EN09PL29KD11CACL 

0-20 GPM 

0-20 GPM 

4-20 MADC 

CALIBRATION NOTES 

Flush process piping, connect water hose to upstream side of 

flow meter. Set control system to appropriate control rate, 

and read totalizer, flow water into a container and compare 

the toltalize r reading to the measured amount in container. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

•0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATION SOURCE REFERENCE 

:_______^M^) 

CALSHEET.WDB (Field or Shop) 

VES018988 
TWI INSTRUMENT CALIBRATION RECORD 

UNIT #4 

ANNUAL 

TAG: 

LOOP: 

DESCRIPON: 

SERVICE: 

LOCATION: 

LP-SHT: 

P&ID: 

REMARKS: 

INSTL-RMKS: 

SPEC-RMKS: 

S/N: 

FT 

426 

MAG METER 

X-19 DIL SLURRY 

WAPC 

426 

F016 

W/GAS CLEANING TRAIN 

Size 1: or 25mm 

MANUFACT: Fischer & 

MODEL: 10D1475C 

SCALE: 0-20 GPM 

CALIB-IN: 0-20 GPM 

CALIB-OUT; 4-20 MADC 

PROCESS-SP: 

INST-SP: 

ACTION: 

I/O NUMBER: Nl:113 

Porter 

CALIBRATION NOTES 

Flush process piping, connect water hose to upstream side of 

flow meter. Set control system to appropriate control rate, 

and read totalizer, flow water into a container and compare 

the toltalize r reading to the measured amount in container. 

See Manufactures literature for detailed instructions. 

Fil l out and affi x a new calibration sticker. 

0.1 lb/hr 

CALIBRATION REPORT 

INPUT VALUE 

o c.c4 

3 &CK\ 

INSTRUMENT READING 

Before Calibration 

3 £cx 

After Calibration 

CALIBRATION SOURCE REFERENCE 

VES018989 
BIWEEKLY LIMIT #4 (CMS Task IC4032) PAGE 10F 3 

^'ASTE FEED CUT-OFF PASS FAIL 

1 TSHH-305 KILN HIGH HIGH 

2 TSHH-317 SCC HIGH HIGH 

3 PAHH-3C0 KILN HIGH PRESSURE 

4 PAHH-324 SCC HIGH PRESSURE 

6 TAHHM04 TEMPERING CHAMBER HIGH TEMP 

7 VIOLATION OPACITY HIGH INSTANTATEOUS 

8 PROCESS MONITOR FAILED 

9 WASTE FEED MONITOR FAILED 

12 VIOLATION STACK FLOW HIGH 1 MIN 

13 VIOLATION ZAC-316 (TRV) OPEN 

14 VIOLATION ZAC-026 SURGE VENT OPEN 

15 UA-557 ANALYZER FAIL HCL 

.6 UA-5E8 ANALYZER FAIL CO 

17 UA-560 ANALYZER FAIL 02 

18 UA-562 ANALYZER FAIL HC 

19 PDAL-563 LOW DELTA P. (ID FAN FAILURE) 

20 WFD-OFF CARBON INJECTION SYSTEM FAILED ^ 

21 PSL-10O/PSL-2OO SCC COMB. AIR FAN FAILED 

23 PSL-209 X-14 PRIMARY FUEL LOW PRESS. (ONLY APPLICABLE FOR #2 FUEL OIL) 

25 STACK FLOW HIGH INSTANTANEOUS 

35 VIOLATION SCC TEMP. LOW 1 MIN AVERAGE A 

36 VIOLATION KILN TEMP. LOW 1 MIN AVERAGE ^ 

37 WFD-OFF HCL HIGH 1 MIN AVERAGE / 

38 WFD-OFF OPACrTY HIGH 1 MIN AVERAGE ^ 

39 WFD-OFF CO HIGH 1 MIN AVERAGE <^ 

-iO WFD-OFF HC (THC) HIGH 1 MIN AVERAGE ^ 

41 WFDOFF BAGHOUSE DELTA P HIGH 1 MIN AVERAGE . A 

VES018990 
BIWEEKLY UNIT #4 (CMS Task IC4032) PAGE 2 OF 3 

"•^STE FEED CUT-OFF PASS FAI_L_ 

42 WFD-OFF SDA OUTLET HIGH TEMP. 1 MIN AVERAGE 

43 WFD-OFF OXYGEN (02) LOW 1 MIN AVERAGE 

44 VIOLATION HCL HIGH 1 HOUR AVERAGE 

45 VIOLATION CO HIGH 1 HOUR AVERAGE 

46 VIOLATION SCC TEMP. LOW 1 HOUR AVERAGE X 

HOUR. / 

47 WFD-OFF KILN TEMP. LOW 1 WWI AVERAGE ' 

48 VIOLATION OPACITY HIGH 480 SEC/HOUR / 

49 WFD-OFF BAGHOUSE DELTA P LOW 1 MIN AVERAGE 

52 Bag Leak Detection System (Tribo) 

65 Pumpable 1 Hour Rolling Total OPL S 

66 Non-Pumpable 1 Hour Rolling Total OPL / 

*?7 Total Waste 1 Hour Rolling Total OPL S 

d8 BTU 1 Hour Total OPL / 

69 CL 12 Hour Rolling Total OPL S 

70 Low Violatile 12 Hour Rolling total OPL ^ 

71 Semi Violatile 12 Hour Rolling Total OPL 

72 Mercury 12 Hour Rolling Total OPL 

73 Ash 12 Hour Rolling Total OPL ^ 

74 PCC Temperature 1 Hour Rolling Average Low OPL ^ 

75 SCC Temperature 1 Hour Rolling Average Low OPL 

76 SDA Outlet Temperature 1 Hour Rolling Average High OPL ^ 

77 Baghouse Differential Pressure 1 Minute Average Low OPL ^ -

78 Baghouse Differential Pressure 1 Minute Average High OPL ^ 

79 Stack HCL Corrected 1 Hour Rolling Average High OPL ^~ 

80 Stack CO Corrected 1 Hour Rolling Average High OPL 

31 Stack Flow 1 Hour Rolling Average High OPL ^ 

82 Hrt CIHra Lime Flow 1 Minute Average OPL ^ 

VES018991 
BIWEEKLY UNIT #4 

'VASTE FEED CUT-OFF 

CHECK SHEET PAGE 3 OF 3 

50 WASTE FEED CUT-OFF TEST BY OPERATOR 

UNIT #4 OPERATOR TO CLOSE MANUAL HAND VALVE AT LIQUID INJECTOR BEFORE FLEX LIME & AIR LINE TO 

SCREENED FEEDER XV-013 SLIDE GATE. 

UNIT 14 OPERATOR TO VERIFY CUT-OFF BY PRESSING EACH START BUTTON. 

(THEN INITIAL & SIGN SHEET) 

SHREDDED_ 

X-10 

SCREENED_ 

X-11 

MAIN CONVEYOR 

X-12 

AUX CONVEYOR 

X-22 

VERIFY ATOMIZING AIR ALARM BY MANUALLY SHUTTING AIR TO PRESSURE SWITCH. 

(NOZZEL MUST BEjjOPEN FOR ALARM TO FUNCTION) 

X-10 X-11 X-12 X-22 

ALSO CHECK OPERATION OF RAM COOUNG WATER LOW FLOW ALARM (MSG# >278) 

CHECKED BY: V U UJCX ^TcVu3 CA_X_y,*S 

83 Lime Slurry Density Low 1 Hour Rolling Average Shoutdown 

A LOG CHECKS IN OPERATIONS BOOK. 

85 ROD OUT KILN PRESSURE LINE (PT-3Q0) 

COMMENTS: 

CHECKED BY: O L prl-^rllt ^OL(/-V _ Date: 

APPROVED BY : Place: Control Room 

BIWEEKiY_4 

9/10/07 HK 

VES018992 
BIWEEKLY UM IT #4 (CMS Task IC4032) PAGE 1 OF 3 

•>STE FEED CUT-OFF PASS FAIL 

1 TSHH-305 KILN HIGH HIGH ^ 

2 TSHH-317 SCC HIGH HIGH ^ 

3 PAHH-3O0 KILN HIGH PRESSURE / 

4 PAHH-324 SCC HIGH PRESSURE ^ 

6 TAHH-404 TEMPERING CHAMBER HIGH TEMP ^ 

7 VIOLATION OPACITY HIGH INSTANTATEOUS ^ 

8 PROCESS MONITOR FAILED f 

9 WASTE FEED MONITOR FAILED 

12 VIOLATION STACK FLOW HIGH 1 MIN S 

13 VIOLATION ZAC-316 (TRV) OPEN / 

14 VIOLATION ZAC-026 SURGE VENT OPEN / 

•" 5 UA-557 ANALYZER FAIL HCL / 

16 UA-558 ANALYZER FAIL CO / 

17 UA-560 ANALYZER FAIL 02 f 

18 UA-562 ANALYZER FAIL HC / 

19 PDAL-563 LOW DELTA P. (ID FAN FAILURE) S 

20 WFD-OFF CARBON INJECTION SYSTEM FAILED / 

21 PSL-10O/PSL-2OO SCC COMB. AIR FAN FAILED ^ 

23 PSL-209 X-14 PRIMARY FUEL LOW PRESS. (ONLY APPLICABLE FOR #2 FUEL OIL) ^ 

25 STACK FLOW HIGH INSTANTANEOUS 

35 VIOLATION SCC TEMP. LOW 1 MIN AVERAGE 

36 VIOLATION KILN TEMP. LOW 1 MIN AVERAGE 

37 WFD-OFF HCL HIGH 1 MIN AVERAGE ^ 

38 WFD-OFF OPACITY HIGH 1 MIN AVERAGE / 

39 WFD-OFF CO HIGH 1 MIN AVERAGE S 

40 WFD-OFF HC (THC) HIGH 1 MIN AVERAGE f 

41 WFD-OFF BAGHOUSE DELTA P HIGH 1 MIN AVERAGE . f 

VES018993 
BIWEEKLY UN IT #4 (CMS Task IC4032) PAGE 2 OF 3 

"STE FEED CUT-OFF PASS FAIL 

42 WFD-OFF SDA OUTLET HIGH TEMP. 1 MIN AVERAGE * ^ 

43 WFD-OFF OXYGEN (02) LOW 1 MIN AVERAGE ^ 

44 VIOLATION HCL HIGH 1 HOUR AVERAGE ^ 

45 VIOLATION CO HIGH 1 HOUR AVERAGE ^ 

46 VIOLATION SCC TEMP. LOW 1 HOUR AVERAGE ^ 

HOUR, 

47 WFD-OFF KILN TEMP. LOW 1 ROT AVERAGE 

48 VIOLATION OPACITY HIGH 480 SEC/HOUR / ~ 

49 WFD-OFF BAGHOUSE DELTA P LOW 1 MIN AVERAGE 

52 Bag Leak Detection System (Tribo) 

65 PumpaWe 1 Hour Rolling Total OPL ^ 

66 Non-Pumpable 1 Hour Rolling Total OPt _ 

H7 Total Waste 1 Hour Rolling Total OPL " 

68 BTU 1 Hour Total OPL 

69 CL 12 Hour Rolling Total OPL ^ 

70 Low Volatile 12 Hour Rolling Total OPL 

71 Semi Violatile 12 Hour Rolling Total OPL ^ 

72 Mercury 12 Hour Rolling Total OPL S 

73 Ash 12 Hour Rolling Total OPL ^ 

74 PCC Temperature 1 Hour Rolling Average Low OPL ^ 

75 SCC Temperature 1 Hour Rolling Average Low OPL 

76 SDA Outlet Temperature 1 Hour Rolling Average High OPL 

77 Baghouse Differential Pressure 1 Minute Average Low OPL y 

78 Baghouse Differential Pressure 1 Minute Average High OPL <^ 

79 Stack HCL Corrected 1 Hour Rolling Average High OPL 

80 Stack CO Corrected 1 Hour Rolling Average High OPL S^ 

<51 Stack How 1 Hour Rolling Average High OPL 

82 Hrt Cl/Hra Lime Flow 1 Minute Average OPL 

VES018994 
BIWEEKLY UNIT#4 

STE FEED CUT-OFF 

CHECK SHEET PAGE 3 OF 3 

50 WASTE FEED CUT-OFF TEST BY OPERATOR 

UNIT m OPERATOR TO CLOSE MANUAL HAND VALVE AT LIQUID INJECTOR BEFORE FLEX LIME & AIR LINE TO 

SCREENED FEEDER XV-013 SLIDE GATE. 

UNIT #4 OPERATOR TO VERIFY CUT-OFF BY PRESSING EACH START BUTTON. 

(THEN INITIAL & SIGN SHEET) 

SHREDDED_ 

X-10 

_SCREENED_ 

X-11 

MAIN CONVEYOR 

x-12 y 

AUX CONVEYOR 

X-22 

VERIFV ATOMIZING AIR ALARM BY MANUALLY SHUTTING AIR TO PRESSURE SWITCH. 

(NOZZEL MUST BE OPEN FOR ALARM TO FUNCTION) 

X-10 X-11 X-12 X-22 

ALSO CHECK OPERATION OF RAM COOUNGfWATER LOW FLOW ALARM (MSG* >278) 

CHECKED BY: V VtjucA ^ 7Al_> Q U fAs 

83 Lime Slurry Density Low 1 Hour Rolling Average 

• JA LOG CHECKS IN OPERATIONS BOOK. 

85 ROD OUT KILN PRESSURE LINE (PT-300) 

Shoutdown 

COMMENTS: 

CHECKED BY: QVu-C^W ^jttOO L ^ rSDate: i£> R T_J°f Time: \Q 'SO^rP^ 

APPROVED BY: Place: Control Room 

BIWEEKLY_4 

9/1O/07 HK 

VES018995 
,rUNIT#4 

c FEED CUT-OFF 

(CMS Task IC4032) PAGE 1 OF 3 

PASS FAIL 

1 TSHB-305 KILN HIGH HIGH 

2 TSHH-317 SCC HIGH HIGH 

3 PAHH-30O KILN HIGH PRESSURE 

4 PAHH-324 SCC HIGH PRESSURE 

6 TAHH404 TEMPERING CHAMBER HIGH TEMP 

7 VIOLATION OPACITY HIGH INSTANTATEOUS 

8 PROCESS MONITOR FAILED 

9 WASTE FEED MONITOR FAILED 

12 VIOLATION STACK FLOW HIGH 1 MIN 

13 VIOLATION ZAC-316 (TRV) OPEN 

14 VIOLATION ZAC-026 SURGE VENT OPEN 

15 UA-557 ANALYZER FAIL HCL 

Jj UA-558ANALYZER FAIL CO 

17 UA-560 ANALYZER FAIL 02 

18 UA-562ANALYZER FAIL HC 

19 PDAL-653 LOW DELTA P. (ID FAN FAILURE) 

20 WFD-OFF CARBON INJECTION SYSTEM FAILED 

21 PSL-10WPSL-200 SCC COMB. AIR FAN FAILED 

23 PSL-209 X-14 PRIMARY FUEL LOW PRESS. (ONLY APPLICABLE FOR #2 FUEL OIL) 

25 STACKFLOW HIGH INSTANTANEOUS 

35 VIOLATION SCC TEMP. LOW 1 MIN AVERAGE 

36 VIOLATION KILN TEMP. LOW 1 MIN AVERAGE 

37 WFD-OFF HCL HIGH 1 MIN AVERAGE 

38 WFD-OFF OPACITY HIGH 1 MIN AVERAGE 

39 WFD-OFF CO HIGH 1 MIN AVERAGE 

- WFD-OFF HC (THC) HIGH 1 MIN AVERAGE 

41 WFD-OFF BAGHOUSE DELTA P HIGH 1 MIN AVERAGE 

VES018996 
.r UNIT #4 (CMS Task IC4032) PAGE 2 OF 3 

: FEED CUT-OFF PASS FAIL 

42 WFD-OFF SDA OUTLET HIGH TEMP. 1 MIN AVERAGE 

43 WFD-OFF OXYGEN (02) LOW 1 MIN AVERAGE 

44 VIOLATION HCL HIGH 1 HOUR AVERAGE 

45 VIOLATION CO HIGH 1 HOUR AVERAGE 

48 VIOLATION OPACITY HIGH 480 SEC/HOUR 

49 WFD-OFF BAGHOUSE DELTA P LOW 1 MIN AVERAGE 

52 Bag Leak Detection System (Tribo) 

65 Pumpable 1 Hour Rolling Total OPL 

66 Non-Pumpable 1 Hour Rolling Total OPL 

67 Total Waste 1 Hour Rolling Total OPL 

.J BTU 1 Hour Total OPL 

69 CL 12 Hour Rolling Total OPL 

70 Low Violatile 12 Hour Rolling Total OPL 

71 Semi Violatile 12 Hour Rolling Total OPL 

75 SCC Temperature 1 Hour Rolling Average Low OPL 

78 Baghouse Differential Pressure 1 Minute Average High OPL 

79 Stack HCL Corrected 1 Hour Rolling Average High OPL 

80 Stack CO Corrected 1 Hour Rolling Average High OPL 

^ Stack Flow 1 Hour Rolling Average High OPL 

82 Hit Cl/Hra Lime Flow 1 Minute Average OPL 

46 • VIOLATION SCC TEMP. LOW 1 HOUR AVERAGE ' „ 

47 WFD-OFF KILN TEMP. LOW 1 BWfr AVERAGE 

/ 

72 Mercury 12 Hour Rolling Total OPL X 

7~ 

73 Ash 12 Hour Rolling Total OPL X __ 

74 PCC Temperature 1 Hour Rolling Average Low OPL 

7~ 

76 SDA Outlet Temperature 1 Hour Rolling Average High OPL y 

77 Baghouse Differential Pressure 1 Minute Average Low OPL y 

VES018997 
., UNIT #4 CHECK SHEET 

d FEED CUT-OFF 

PAGE 3 OF 3 

50 WASTE FEED CUT-OFF TEST BY OPERATOR 

UNIT #4 OPERATOR TO CLOSE MANUAL HAND VALVE AT LIQUID INJECTOR BEFORE FLEX LIME & AIR LINE TO 

SCREENED FEEDER XV-013 SLIDE GATE. 

UNIT #4 OPERATOR TO VERIFY CUT-OFF BY PRESSING EACH START BUTTON. 

(THEN INITIAL & SIGN SHEET) 

SHREDDED SCREENED ^ J f MAIN CONVEYOR ^^K - AUX CONVEYOR 

X-10 x-11_^___ " X-12 %*^~«-^ x-22 %~-T^_ _ 

VERIFY ATOMIZING AIR ALARM BY MANUALLY SHUTTING AIR TO PRESSURE SWITCH. 

(NOZZEL MUST BE OPEN FOR ALARM TO FUNCTION) 

X-10 

ALSO CHECK OPERATION OF RAM COOLING WATER LOW FLOW ALARM (MSG* >27S) 

CHECKED BY: 

83 Lime Slurry Density Low 1 Hour Rolling Average Shoutdown 

LOG CHECKS IN OPERATIONS BOOK. 

85 ROD OUT KILN PRESSURE LINE (PT-300) 

COMMENTS: 

CHECKED BY: Date:_j7____"?

 Tim e : 2* VT %£^ M 

APPROVED BY: Place: Control Room 

BIWEEKLY_4 

9/10/07 HK 

VES018998