Uni t 4 Ru n 3 Liqui d WeighfiHR T 

### TptarWeig'hjfeBRt: X-2 2 HR T 12/18/09 12:1 1 P M 3241. 1 11541. 1 1097. 6 12/18/09 12:1 1 P M "3241. 3 11518. 3 1097. 4 12/18/09 12:1 1 P M 3241 5 11518. 5 1097. 5 12/18/09 12:1 1 P M 3241 7 11495. 7 1097. 4 12/18/09 12:1 2 P M 3241 8 11495. 8 1097. 3 12/18/09 12:1 2 P M ""3241 9 "11495. 9 1097. 3 12/18/09 12:1 2 P M ' 3242. 3 11496. 3 1097. 4 12/18/09 12:1 2 P M 32427 4 11496. 4 1097. 4 12/18/09 12:13P M 32427 4 11496. 4 1097. 3 12/18/09 12:13P M 3242. 3 11496. 3 1097. 3 12/18/09 12:1 3 P M 3242. 3 11496. 3 1097. 1 12/18/09 12:1 3 PM

. 3242. 2 12673. 2 1097. 2 12/18/09 12:14P M 3242. 0 12673. 0 1097. 2 12/18/09 12:14P M 3241 9 11914. 9 1097. 2 12/18/09 12:1 4 PM l 3241 7 11914.7 ! 1097. 0 12/18/09 12:1 4 PM : 3241. 6 11940.6 ; 1096. 9 12/18/09 12:1 5 PM ; 32415 1 11940.5 ! 1097, 0 12/18/09 12:1 5 PM : 3241 4 11916.4 ! 1097. 1 12/18/09 12:1 5 PM : "32417 3 11919. 3 1097. 1 12/ 1 8/09 12:1 5 PM ! 32467 9 11918.9 ! 1097. 1 12/18/09 12:1 6 PM ! 3240. 7 11895.7 j 1097. 2 12/18/09 12:1 6 PM l 3240.6 ] 11921.6 ! 1097. 2 12/18/09 12:1 6 PM : 32407 4 11898.4 ! 1097. 1 12/18/09 12:1 6 PM i 3240.4 ' 11875.4 ! 1097. 0 12/18/09 12:1 7 PM i 3240.4

. 32407 4 11901.4 ; 1097. 0 12/18/09 12:1 7 PM : 3240.4

. 32407 4 1 i 901.4- 1097. 0 12/18/09 12:1 7 PM I 3246.4 ! 11876.4 ! 1097. 0 12/18/09 12:1 7 PM i 3240.3

. 11902.3 ; 1097. 0 •12/18/09 12:1 8 PM ! 3240.1 ! 11902.1 ! 1101. 7 12/18/09 12:1 8 PM i 3239.8 ; 11901.8 : 1106. 3 12/18/0 9 12:1 8 PM ; 32467 1 11928.1 ; 1111 0 12/18/09 12:1 8 PM , 3240. 1 11928. 1 1115. 7 12/18/0912:1 9 PMj 3240. 2 11928.2 ; 1120. 4 12/18/09 12:1 9 PM i

. 3240.3 ^ 11928.3 ! 1125. 1 12/18/09 12:1 9 PMj 3240.5 ; 11928.5 ! 1129. 7 12/18/09 12:1 9 PM ; 3240. 5 11928.5 ! 1134. 3 12/18/0912:2 0 PM i 324675 ! 11928.5- 1138. 9 12/18/09 12:2 0 PM i 3240. 5 11928.5 ; 1138. 9 12/18/09 12:20 PM i 

### 1240.7 1 11928.7 ! 1138. 9 12/18/09 12:2 0 PM j 3240.9 j 11928.9 ; 1138. 9 12/18/09 12:2

TPM ; """3246 1 11928.9 ! 1138. 9 12/18/09 12:2 1 PMj " 324 1 

## TT ; 11929.1 ; 1139. 0 12/18/09 12:2 1 PM j 3241.2 !
- 11929.2 ! 1139. 1 12/18/09 12:2 1 PM ! 324 1 l j 11929.2 ! 1139. 1 12/18/09 12:22 PMj '""'" " 3241.3 ! 

### 11929.31 1139. 2 12/18/09 12:22 PM l 324l'.2 j 11929.2 ! 1139. 2 12/18/09 12:22 PMj 3241.0 1 11929.0 ! 1139. 3 12/18/09 12:22 PMj 324617 ! 12181.7 ! 1139. 4 12/18/09 12:2 3 PM i 3240.6 ! 12181.6 ; 1139. 7 12/18/09 12:2 3 PMj 3240 1 12181.4 ; 1139. 9Uni t 4 Ru n 3 I

. ^$fimelSta>rip->; ;
. ' Liqui d Weight'HR TTotaliWeigh.KHRf *-2&HR T 12/18/0 9 12:2 3 P M 3240.4 ! 12181.4 ; 1140. 0 12/18/0 9 12:2 3 P M 3240.1 ! 12181.1 ; 1140. 3 12/18/0 9 12:24 P M 3240.0 ! 12181.0 ! 1140. 6 12/18/0 9 12:24 P M 

### 3240 .6] ' 12181.0 ! 1141. 0 12/18/0 9 12:2 4 P M '3240 ] l ] 12207.1 ! 1141. 1 12/18/0 9 12:24 P M '3246.0 ! 12207.6 ! 1141. 1 12/18/0 9 12:2 5 P M "3239.8 : 12206.8 ; 1141. 1 12/18/0 9 12:2 5 P M '323978 ] 12232.8 ; 1141. 3 12/18/0 9 12:2 5 P M 3239.4 , 12232.4 ! 1141. 4 12/18/0 9 12:2 5 P M 3238.9 j 12231. 9 1141. 4 12/18/0 9 12:2 6 P M 3238.51

. 12257. 5 1141. 4 12/18/0 9 12:2 6 P M 3238. 0 12257.0 ! 1141. 2 12/18/0 9 12:2 6 P M 3237.4 ] 12256. 4 1141. 0 12/18/0 9 12:2 6 PM , 3236. 9 "'"T2281. 9 1140. 8 12/18/0 9 12:2 7 PM i 3236. 4 12281. 4 1140. 7 12/18/0 9 12:2 7 PM , 3235.9 j 12286. 9 1140. 4 12/18/0 9 12:2 7 P M 3235.7 ! 12306. 7 1140. 1 12/18/0 9 12:2 7 PM i 3235.5 ; 12306. 5 1140. 0 12/18/0 9 12:28 PM ; " 3235.5 ' 12306. 5 1139. 8 12/18/0 9 12:2 8 PM i 3235.5 ; 12332. 5 1139. 6 12/18/0 9 12:2 8 PM

j 3235. 2 123327 2 1139. 4 12/18/0 9 12:2 8 PM

^ '323572 " 12332. 2 1139. 2 12/18/0 9 12:2 9 PM i 3235 1 12332. 1 1139. 2 12/18/0 9 12:2 9 PM ! 323571 ! 12332. 1 1139. 3 12/18/0 9 12:2 9 PM

j " " 3235. 2 12332. 2 1139. 3 12/18/0 9 12:2 9 PMj 3235.lT ' 12332. 1 1139. 3 12/18/0 9 12:30 PM i 3235. 2 12332. 2 1139. 2 12/18/0 9 12:30 PM i 3235: 3 '12332. 3 1139. 1 12/18/0 9 12:30 PM

j 3235.4 : 12332. 4 1139. 2 12/18/0 9 12:30 PM

j "3235.4 f 13128. 4 1139. 1 12/18/0 9 12:3 1 PM i 3235.67 ' 13128. 6 1139. 2 12/18/0 9 12:3 1 PM i 3235.6 ; 13128. 6 1139. 1 12/18/0 9 12:3 1 PM

j 3235.7 ' 13128. 7 1139. 1 12/18/0 9 12:3 1 PM ' 3235. 8 12024. 8 1139. 2 12/18/0 9 12:32 PM i 3235.9 j 12024.9 ! 1139. 3 12/18/0 9 12:32 PM ; 323676 ! 12025. 0 1139. 3 12/18/0 9 12:32 PM ' 3236. 1 j "12051. 1 1139. 4 12/18/0 9 12:32 PM ! 323676 : 12051. 0 1139. 4 12/18/0 9 12:33 P M 3235.9 ! 12050. 9 1139. 3 12/18/0 9 12:33 P M 323578 : 120767 8 1139. 3 12/18/0 9 12:33 P M 323578 ; 12076. 8 1139. 5 12/18/0 9 12:33 PMj 3235.9] 12076. 9 1139. 6 12/18/0 9 12:34 PM i

. . 323577 T 12076. 7 1139. 5 12/18/0 9 12:34 PM

j 3235.6 ! 12076. 6 1139. 5 1.2/18/0 9 12:34 PM ! 3235.5 j 12050. 5 1139. 3 12/18/0 9 12:34 PM

j 3235.4 ! 12076. 4 1139. 3 12/18/0 9 12:35 PM i 3235.0 ; 12076. 0 1139. 4 12/18/0 9 12:35 PM i 3234.91" " 12049. 9 1139. 2 12/18/0 9 12:35 PM ; 3234.8 ! 12075. 8 1139. 2 12/18/0 9 12:35 PM

j 3234.7 ! 12075. 7 1139. 2Uni t 4 Ru n 3 TimeJStam p Liqui d Weigh t HR T[ tota l Weigh t HR T X-22-HR T .12/18/0 9 12

:3 6 PM i 3234.7 ! 12049.7 ! 

### 1139 . 2 12/18/0 9 12:36 PM I 3234.8 ! 12049.8 ; 1139. 4 12/18/0 9 12:36 PM , 3234.8 i 12049.8 ] 1139. 4 12/18/0 9 12:36 PM r 

### 3235 .1 ] 12023 . 1 1139. 3 12/18/0 9 12:37 PM ; 

### 3235 .2 ; 

# 12623. 2 ; 

### 1139 . 2 12/18/0 9 12:3 7 PM ; 3235.3 ; 12023.3 ] 1139. 3 12/18/0 9 12:37 PM ! 3235.4 ; 11997. 4 1139. 4 12/18/0 9 12:3 7 PM , 3235.5 , " ' 11997.5 ; 1139. 5 12/18/0 9 12:38 PM ; ~32351?"'" " 11997.8 ! 1139. 4 12/18/0 9 12:38 PMj 3235. 8 11997.8 ! 1139. 4 12/18/0 9 12:38 PMj 3236

. If"" ' 

### 11998 . 1 1139. 5 12/18/0 9 12:38 PM ; 3236. 1 

### 11998 . 1 1139. 6 12/18/0 9 12:39 PMj 3236. 3 11998.3 ! 1139. 5 12/18/0 9 12:3 9 PM ! 3236.3 ! 11998.3 ! 1139. 6 12/18/0 9 12:39 PM i 3236. 3 11998.3 ! 1139. 7 12/18/0 9 12:39 P M 323676 ; 11793.6 ! 1139. 6 12/18/0 9 12:40 PM i 323677 7 11793.7 : 1139. 6 12/18/0912:4 0 PM i 3236.9 7 11793. 9 1139. 7 12/18/0 9 12:40 PM ; 3237":0 i 11794. 0 1139. 8 12/18/0 9 12:40 PM

j 

### 3237 .1 . 11820 . 1 1139. 8 12/18/0 9 12:4 1 PM ; 3237. 3 11820.3 ; 1139. 7 12/18/0 9 12:4 1 PM ; 3237.3 : ' 11820. 3 1139. 7 12/18/0 9 12:4 1 PM i 3237.4 ; 11819.4" 1139. 8 12/18/0 9 12:4 1 PM i 

### 3237 .3 7 11819.3 ! 1139. 8 12/18/0 9 12:42 PM ' 3237. 4 11819.4

. 1139. 8 12/18/0 9 12:42 PM : 3237.5 : 11819.5 : 1139. 8 12/18/0912:4 2 PM ! 3237.6 ; 11819.6 ] 1139. 8 12/18/0912:4 2 PM ; 323775 ; 11819. 5 1139. 8 12/18/0 9 12:43 PM

j 3237.57' 11819. 5 1139. 8 12/18/0 9 12:43 PM : 3237.7 ! 11819. 7 1139. 8 12/18/0 9 12:43 PMj 

### 3238 .6 ; 11820. 0 1139. 8 12/18/0 9 12:43 PM i 

### 3238 . 1 j 11820. 1 1139. 8 12/18/0 9 12:44 PMj 32381 ; 

### 11820 . 1 1139. 7 12/18/0 9 12:44 PMj 

### "~3238 .6 ; 11820. 0 1139. 6 12/18/0 9 12

:4 4 PM : 

# 32387T

f 11820. 1 1139. 6 12/18/0 9 12:44 PM i 

### 3238.1" ' 11820. 1 1139. 6 12/18/0 9 12:45 P M 

### 3238 . 1 11820. 1 1139. 5 12/18/0 9 12:45 PM ! 3238. 1 "" ' 11820. 1 1139. 5 12/18/0 9 12:45 PM i 

### 3238 . 1 11820 .1 . 1139. 4 12/18/0 9 12:45 PM ; 

# 323872

7 11820 .2 ; 1139. 3 12/18/0 9 12:46 PM ' 3238.57 ' 11820.5 ! 1139. 3 12/18/0 9 12:46 PM : 3238.8 ; 11820.8 ! 1139. 3 12/18/0 9 12:46 PM ; 

# "323878

! 11820.8 ! 

### 1139 . 2 12/18/0 9 12:46 PM i 3239:0 j 10704.0 ! 1139. 3 12/18/0 9 12:4 7 PMj 323973 7 10704.3

] 1139. 3 12/18/0 9 12:47 PM

j 323975 ! 10704.5] 1139. 3 

### 12 /1 8/0 9 12:47 PM j 3239.7 ; 10704.7 ! 1139. 3 12/18/0 9 12:47 PM i 3239.9] 11677.9 ; 1139. 3 12/18/0912:4 8 PM

j 32407i r 11678.1 ] 1139. 3 12/18/0 9 12:48 PM l 

### '3240 .2 ! 11678 .2 ! 1139. 4Uni t 4 Ru n 3 j ls;|limeI|lKp5i i Liqu'idiWeightHR.T ' Tota l WeighrHR TfcX-22 HR T 12/18/09 12:4

8 P M 3240. 3 11652. 3 1139. 5 12/18/09 12:4

8 PM ; 3240. 4 i 1678. 4 1139. 5 12/18/0912:4 9 PM ; 3240. 7 11678. 7 1139. 5 12/18/09 12:49 PM j 3240. 9 11652. 9 1139. 4 12/18/0912:4 9 PM ! '""3241 0 11679. 0 1139. 3 12/18/0912:4 9 PM l """'3241 2 li"679.2 H 1139. 5 12/18/0912:5 0 PM ; 3241 4 11653. 4 1139. 4 12/18/0912:5 0 PM : 3241 6 11679.6 " 1139. 5 12/18/0912:5 0 PM ; 3241 7 11679. 7 1139. 6 12/18/0 9 12:50 PM ; 3241 7 11679. 7 1139. 5 12/18/0912:5 1 P M """3241 8 11679. 8 1139. 4 12/18/0912:5 1 PM ] 3242.0 , 11680.0 , 1139. 5 12/18/0912:5 1 PM ; 3242. 1 11680.1 ] 1139. 5 12/18/0 9 12:5 1 PM : 3242. 3 11680.3 ; 1139. 5 12/18/0912:5 2 PM I 3242. 5 11680.5 ; 1139. 5 12/18/0912:5 2 PM i 3242.6

. 11680.6 s 1139. 6 12/18/0 9 12:52 PM ! 3242. 5 11680.5 ! 1139. 5 12/18/0912:5 2 PM , 324Z5 ! 11680. 5 1139. 4 12/18/0912:5 3 PM ! 3242.'2 i 11680.2 ! 1139. 4 12/18/0912:5 3 PM i " 3242. 1 11680. 1 1139. 4 1271870912:5

3 PM ; 32417 ; 11679.7 ] 1139. 6 12/18/0912:5 3 PM ' 3241.4 1 11679.4 ! 1139. 6 12/18/0 9 12:5

4 PM ! 32411 ! 11679.1 ! 1139. 6 12/18/0 9 12:5

4 PM i 

### " ' 3241 .6 "\ 1679.0 ! 1139. 5 12/18/0912:5 4 PM ; 3240.7 ; 11678.7 ! 1139. 5 12/18/0 9 12:5

4 PM ! '32404 ] 11678.4 ; 1139. 6 12/18/0912:5 5 PM i 3240.3 , 11678.3 ; 1139. 6 12/18/0 9 12:55 PM | 3240"3 | 11678.3 ! 1139. 7 12/18/0 9 12:55 PMj ~ 3239.9 ! 11677.9 ! 1139. 5 12/18/0 9 12:55 PM i 3239.7 ! 11491.7 ! 1139. 5 "12/18/0912:5 6 PM! " 3239.'5 ; 11491.5 ! 1139. 6 12/18/0 9 12:56 PM ; 3239.4 ; 11491.4 ; 1139. 7 12/18/0 9 12:56 PM ; 3239.5 ! 11491.5 ! 1139. 7 12/18/0 9 12:56 PM ! ""3239.7; ' 11465.7 ! 1139. 7 12/18/0 9 12:57 PM ! 3239I 9 11491.9 : 1139. 7 12/18/0 9 12:57 PM ; 3239.9 ; 11465.9 ]

. 1139. 7 12/18/0 9 12:57 PM ; 3240.2

. ll46"6.2 ! 1139. 7 12/18/0 9 12:57 PM ; "32407 ! 11492.7 ] 1139. 8 12/18/0 9 12:58 PM i 3241. 1 1146711 ] 1139. 7 12/18/0 9 12:58 PM i 3241 ! 8 ; 11467.8 ; 1139. 6 12/18/0 9 12:58 PM ! 32422 1 11494.2 ! 1139. 7 12/18/0 9 12:58 PM ; 3243? ; 11469.0 ; 1139. 7 12/18/0 9 12:59 PM i '3243. 6 11469.6 ! 1139. 9 12/18/0 9 12:59 PM ! "3244.T ! 11497.1 ! 1139. 9 12/18/0 9 12:5 9 PM : ""3244.1

. 114711 ] 1140. 3 12/18/0 9 12:59 PM l 3244!3 ! 114713 ] 1140. 6 12/18/091:0 0 PM ; """"32444 ; 11497.4 ! 1140. 8 12/18/091:0 0 PM ! 32444 ! 11471.4 ! 1141. 2 12/18/091:0 0 PM ! TM3244?5 l 11471.5 ! 1141. 5 12/18/0 9 1:0

0 PM ! 3244.5 ! 11497.5 ; 1141. 9

### Unit A Ru n 3

•' Time ' Stam p , . ^Liqui d WeightfHR ^ 

### 12 /18/0 9 1 :0 1 P M 3244.4 ! 11497. 4

. 1142. 3 

### 12 /18/0 9 1:0 1 P M 3244. 4 11497. 4 1142. 4 

### 12 /18/0 9 1 :0 1 P M " " ~ 32443 ! 11497. 3 1142. 7 

### 12 /18/091:01 P M 3244.2

. 11497. 2 1143. 0


### " "12 /18/0 9 1 :0 2 PM ' 3244.1 ' 11497. 1 1143. 3 

### 12 /18/0 9 1:0 2 P M 324471 ! 11497. 1 1143. 6 

### 12 /18/0 9 1 :0 2 P M 3244.1 ; 11497. 1 1144. 0 

### 12 /18/0 9 1 :0 2 P M 3244. 1 11497. 1 1144. 2 

### 12 /18/0 9 1:0 3 P M 3243.9 , 11496. 9 1144. 4 

### 12 /18/0 9 1:0 3 P M 324379 : I 11496. 9 1144. 7 

### 12 /18/0 9 1:0 3 P M 3244

.6 7 114977

0 1145. 0 12/18/09 1:0

3 P M 3244.2 ; 12552. 2 1145. 3 12/18/09 1:0

4 P M 32444 7 12552. 4 1145. 4 

### 12 /18/0 9 1:0 4 PM ' 3244.6 ! 12552. 6 1145. 5 

### 12 /18/0 9 1:0 4 P M 3244.8 ; 12552. 8 1145. 7 12/18/09 1:0

4 P M 3244.9

7 11365. 9 1146. 1 

### 12 /18/0 9 1:0 5 P M 3245.47 11366. 4 1146. 2 12/18/09 1:0

5 PM , 324575 ! 11366, 5 1146. 5 

### 12 /18/0 9 1:0 5 PM

. 3245.9 ; 11392. 9 1146. 7 

### 12 /18/0 9 1:0 5 PM : 32463 7 11393.2 ' 1147. 0 

### 12 /18/0 9 1:0 6 PM i 324677 ! 11367. 7 1147. 3 

### 12 /18/0 9 1:0 6 PM ; 324716

* ' 11394. 0 1147. 5 12/18/09 1:0

6 PM ; 3247.3 ; 11394.3 ; 1147. 7 12/18/0 9 1:0

6 PM

. 3247.7 ; 11368.7 ; 1147. 9 

### 12 /18/0 9 1:0 7 PM i 

## 3248 .1

7 11395.1 ! 1148. 1 12/18/0 9 1:0

7 PM ; 3248.7 ; 11395.7 ; 1148. 4 12/18/0 9 1:0

7 PM i 3249.2 : 11370. Z 1148. 6 12/18/0 9 1:07PM | 

# '"732567T7

" 11397.1 1 1148. 7 

### 12 /18/0 9 1:0 8 PM i 

# 325675

: 11371.5] 1149. 3 12/18/0 9 1:0

8 PM ! 3251.0 : 11'372.0 ! 1149. 6 

### 12 /18/0 9 1:0 8 PM ! 32514 , ' 11398.4 ! 1149. 8 

### 12 /18/0 9 1:0 8 PM : 3251.7: ' 11372.7 | 1150. 0 

### 12 /18/0 9 1:0 9 PM l 3252. 1 11373.1 ; 1150. 5 

### 12 /18/0 9 1:0 9 PM i 3252. 4 i 1373.4 ; 1150. 7 12/18/0 9 1:0

9 PM i 325279 : 11347.9 ! 1151. 0 

### 12 /18/0 9 1:0 9 PM i ' 32534! " 11348.4 ! 1151. 3 

### 12 /18/0 9 1 :1 0 PM i "3253.81 " l i 348.8 ! 1151. 6 

### 12 /18/0 9 1 :1 0 PM" ! 3254.3" ; 11349.3 ; 1-152.0 

### 12 /18/0 9 1 :1 0 PM i 3254.7 ! 11349.7 ! 1152. 4 

### 12 /18/0 9 1 :1 0 PM i 3255.1 1 

## 1T350.1 I 1152. 8 

### 12 /18/0 9 1:1 1 PM !

" 3255.6 , " ' ' : 

### 11350. 6 1153. 2 

### 12 /18/0 9 1:1 1 PM ! 325579. " 11350.9 ! 1153. 5 

### 12 /18/0 9 1:1 1 PM ! 3256.1 ! 11351.1 1 1153. 7 

### 12 /18/0 9 1:1 1 PM ; 3256.5 ' 12573.5 ! 1153. 9 

### 12 /18/0 9 1 :1 2 PM l 3256.8 ; 12573.8s 

### 1154. 3 

### 12 /18/0 9 1 :1 2 PM : 3257. 1 12574.1 ! 1154. 6 

### 12 /18/0 9 1 :1 2 PM , 3257.3 ; 12574.3 ; 1154. 9 

### 12 /18/0 9 1 :1 2 PM ; 325775 ! 12574.5 ; 1155. 1 

### 12 /18/0 9 1:1 3 PM' i "3257. 9 12574.9 ! 1155. 4 

### 12 /18/0 9 1:1 3 PM i 325 8 3 ' 

### 12601.31 1155. 7Unit 4 Ru n 3

^TfmeOstam p Liqui d Weipht'HRT
- TotaLWeigh t HRT , 

## liSii l 12/18/09 1:1 3 P M

| 3258. 8 12601. 8 1156. 1 12/18/091:1 3 PM , 3259. 2 11425. 2 1156. 3 12/18/091:1 4 PM ! 325~9.7 11451. 7 1156. 7 12/18/09 1:1 4 PM | 3260. 2 11452.2 ' 1157. 0 12/18/091:1 4 PM ! 3260. 6 11479. 6 1157. 4 12/18/091:1 4 PM : 3261. 1 11454. 1 1157. 7 12/18/09 1:1 5 P M 3261. 3 11454. 3 1158. 0 12/18/09 1:1 5 P M 32617 ' 11481. 7 1158. 3 12/18/091:1 5 PM

. 3262. 0 11456. 0 1158. 8 12/18/09 1:1 5 PMj 3262. 5 11456. 5 1158. 9 12/18/091:1 6 PM ! 3262.9 ' 11483. 9 1159. 1 12/18/09 1:1 6 P M 3263.0

. 

### 11458. 6 1159. 4 12/18/09 1:1 6 P M 3263.5 : 11458. 5 1159. 6 T2/18/0 9 1:1 6 P M 

### 3264.6 11459. 0 1160. 0 12/18/09 1:1 7 P M 3264.1 , 11433. 1 1160. 2 12/18/09 1:1 7 P M 3264.5 ! 11460. 5 11.60. 6 12/18/09 1:1 7 P M 3264. 9 11460. 9 1160. 9 12/18/09 1:1 7 P M 3265.2 , 11435. 2 1161. 3 12/18/0 9 1:1 8 P M 3265.4

. 11435. 4 1161. 7 12/18/09 1:1 8 PM | 3265.8 | 11435.8 1 1162. 0 12/18/0 9 1:1 8 P M 3266.0 : 

### 11410.6 ' 1162. 3 12/18/0 9 1:1 8 P M ' 3266l4 i 11410.4 ! 1162. 6 12/18/09 1:1 9 P M 3267.0 ! 11411. 0 1163. 0 12/18/09 1:19P M 3267.3 ! 11411. 3 1163. 4 12/18/09 1:1 9 P M 3267.6 ; 11411.6 ! 1163. 7 12/18/09 1:1 9 P M * " 3268. 0 11412. 0 1164. 2 12/18/09 1:20 P M "326875 ] 11412. 5 1164. 7 12/18/0 9 1:20 P M "326976 1 11413. 0 1165. 0 12/18/091:2 0 P M 326975 7 11413.5

} 1165. 2 12/18/091:2 0 P M 3269.8 ! 12578.8 1 1165. 5 12/18/091:2 1 P M 3270.2 : 12579.2 ! 1165. 8 12/18/091:2 1 P M 3270.6 ; 12579.6 , 1166. 0 12/18/091:2 1 P M 3271.0 ; 12580.0 : 1166. 2 12/18/0 9 1:2 1 P M """32714 ; 12607.4 ' 1166. 4 12/18/091:2 2 P M 3271.9 ; 12607.9 : 1166. 6 12/18/091:2 2 P M 3272.3 ] 12608.3 ! 1166. 9 12/18/0 9 1:2

2 P M 3272.8 1 12635.8 ! 1167. 2 12/18/0 9 1:2

2 P M 327373 ; 11567.3 ! 1167. 3 12/18/0 9 1:23 P M 3273.6 ; 11567.6 } 1167. 3 12/18/091:2 3 P M 

### 3274 .6 ] 11595 .6 ; 1167. 4 12/18/0 9 1:2

3 P M 3274.4 ; T l 595.4 ! 1167. 7 12/18/091:2 3 PM ' 3274J ] 1159579 ! 1167. 8 12/18/0 9 1:2

4 P M 3275.3] 11623.3 ! 1167. 9 12/18/0 9 1:2

4 PM
- 327575 ! 11623.5 1 1167. 9 12/18/0 9 1:2

4 P M 3275.7 ! 11597.7 ! 1168. 0
' 12/18/0 9 1:2

4 P M '327672 ; 11625.2 ! 1168. 3 12/18/091:2 5 P M 3276.6 | 11625.6 ! 1168. 4 12/18/0 9 1:25 PM ! 3277.0 ! 11600.0 ! 1168. 5 12/18/0 9 1:2

5 PM ' 3277.4 ; 11627.4 } 1168. 5 12/18/091:2 5 P M 32778 ! 11627.8 : 1168. 8Unit4 Ru n 3 J ..Liquid WeighfcHRt i 12/18/09 1:2

6 PM 3278.2 j 11602. 2]

. 1169. 0 12/18/09 1:2

6 PM 3278.5 i 11602.5 ] 1169. 0 12/18/09 1:2

6 PM 

### 3279.6 : 11603.0 ! 1169. 1 12/18/09 1:2

6 PM 3279.4 ] 11577.4 ! 1169. 4 12/18/09 1:2

7 PM 3279.9 ' 11577. 9 ' 1169. 6 12/18/09 1:2

7 PM 3280.3 ! 11578. 3 1169. 9 12/18/09 1:2

7 P M " 3280. 7 " ' 11552.7 ! 1170. 3 12/18/0 9 1:2

7 PM 328 1 

## i6T

" 11553. 0 1170. 5 12/18/09 1:2

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9 PM 3285.1

. 12666. 1 1172. 6 12/18/09 1:3

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0 PM * 3287.0 : 

### 11899. 6 1173. 5 12/18/09 1:3 1 PM ! 3287.5 : 11899. 5 1173. 7 12/18/0 9 1:3 1 PM i 

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2 PM ! 

### 3289 .6 ; 11902. 0 1174. 7 12/18/0 9 1:3

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3 PM i ~"*3296. 3 11930. 3 1175. 6 12/18/09 1:3

3 PM j "32907?"" ' 11904. 7 1175. 9 12/18/091:3 3 PM j 3290.9 ! 11904. 9 1176. 0 12/18/0 9 1:3

3 PM i 3291 1 11932. 1 1176. 2 12/18/0 9 1:3

4 PM l 3291. 5 11906. 5 1176. 5 12/18/09 1:3

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4 PM ; 3292.2] 11934. 2 1177. 0 12/18/091:3 4 PM j 3292.3 ; 11908. 3 1177. 2 12/18/09 1:3

5 PM j 3292T8TTM " 11908. 8 1177. 4 12/18/09 1:3

5 PM ! 

### 329"3

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6 PM i 32937j 11883. 7 1178. 4 12/18/0 9 1:3

6 PM j 3294.1 ] 11884.1 , 1178. 6 12/18/0 9 1:3

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8 PM ; 3294.7 ] 130837

7 1180. 7Unit4 Ru n 3 | Liq U d?W&gbf ;tfRT : .Totaji:W6ight;,H.R T 

## X -2 2 HRT 12/18/0 9 1:3

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### 12 /18/0 9 1:3 8 PM i 32951 3 13084. 6 1181. 0 

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### 12 /18/0 9 1 :3 9 PM i 3297. 3 13113. 3 1181. 8 

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### 1187 . 2 12 /18/0 9 1 :4 5 P M 3312.6 j 12224.6 : 1187. 4 

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5 PMj 3314.2] 

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T 12552.5 ; 1190. 9 

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### 12553.6 ; 1191 3 

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T 12555.6 ! 

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2 P M 33307

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2 P M 33327

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. . . ... ^ . . i - ... . ,.. . i 1199. 2 12/18/09 1:55 PM ; 3340.7 ! 13781.7 ; 1199. 7 12/18/091:5 5 PM ; 3341.2 ; 12760.2 ! 1200. 1 12/18/091:5 6 PM ; '"'3341787 12760.8 ; 1200. 6 12/18/0 9 1:56 PM ; 334275 ; 12761.5 j 1201. 1 12/18/091:5 6 PM ! 3342. 8 12788.8 ! 1201. 5 12/18/09 1:56 PM ; 334"3.i : 12789.1 ! 1202. 0 12/18/0 9 1:57 PM , "334319 ; 12763.9 ! 1202. 5 12/18/091:5 7 PM ! 334476' j '12790. 6 1202. 8 12/18/091:5 7 PM i ""334573 ; 12791.3 ! 1203. 2 12/18/09 1:57 PM i 3345.9 : 12765.9 ! 1203. 7 12/18/091:5 8 PM ; 3346.5 ; 12792.5 ! 1204. 1 12/18/091:5 8 PMj 3346.8 j 12792.8 ! 1204. 7 12/18/091:5 8 PMj 3347. 2 12793.2; ! 1205. 0 12/18/09 1:58 PM ] "3347. 6 12793.6 ! 1205. 4 12/18/09 1:59 PM ! 3347.7 ; 12793.7 : 1205. 8 12/18/0 9 1:59 PM ! 3348.0 ! 12793.0 ! 1206. 1 12/18/0 9 1:59 PM l 3348.3 ; 12793.3 ; 1206. 2 12118/091:5 9 PM ; 3348.6 ! 12793.6 ' 1206. 3 12/18/0 9 2:0 0 PM ; 

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### 12744.6 ! 1206. 4 12/18/0 9 2:0 1 PM j 3351.4 ; 12744.4 ! 1206. 4 12/18/0 9 2:0 2 PM i 3351.8 ! 12744.8 ! 1206. 4 •12/18/0 9 2:0 2 PM j ' •335276 : 12745.0 j 1206. 4 12/18/0 9 2:0 2 PM j 335273 ] T2745.3] 1206. 4 12/18/0 9 2:0 2 PM ! 335277 ! 13996.7 ] 1206. 5 12/18/0 9 2:0 3 PM * """""335372 ! 13997.2 1 1206. 6 12/18/0 9 2:0 3 PM i """3353.6 ! 13997.6 ! 1206. 7Unit 4 Ru n 3 I

' rirne."Stam p Liqui d WeightiWR TTotal ! Weigh t ffRfi iiiiii i 12/18/0 9 2:03 P M 3354.0 ! 13998. 0 1206. 7 12/18/0 9 2:03 PM 3354.5 1 12969. 5 1206. 9 12/18/0 9 2:04 P M 3355.6 ; " '""12976. 6 1207. 3 12/18/0 9 2:0

4 PM 3355.3 ; 12970. 3 1207. 3 12/18/0 9 2:0

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""336176 " 12976.6 ! 1208. 5 12/18/0 9 2:08 PM ] 3361.6 ; 12976.6 ! 1208. 6 12/18/0 9 2:08 PM i 3361.8 ; 12950.8 ! 1208. 6 12/18/0 9 2:08 PM i 3362.2 ! 12951.2 ! 1208. 7 12/18/0 9 2:09 PM | 3362.4 ; 12951.4 ! 1208. 5 12/18/0 9 2:0 9 PM ; 33627 5 12951.5 ; 1208. 5 12/18/0 9 2:09 PM ; 3362. 7 12951.7 ! 1208. 7 12/18/0 9 2:09 PM I 3362.9 ! 12951.9 ! 1208. 6 12/18/0 9 2:1 0 PM I 3363.1 ! 12952. 1 1208. 8 12/18/0 9 2:1 0 PM I '3363.3 : 12952.3 ! 1208. 8 12/18/0 9 2:1 0 PM i 3363.5 ; 12952.5 1 1208. 8 12/18/0 9 2:1 0 PM i 3363.9 7 14222.9 ! 1208. 7 12/18/0 9 2:1 1 PM i 336472; " 14223.2 ! 1208. 8 12/18/0 9 2:1 1 PM l 3364.5 ' 14223.5 ; 1209. 0 12/18/0 9 2:1 1 PM j 3364.8

. 14223.8 , 1209. 2 12/18/0 9 2:1 1 PM j 3365.0 ! 13028.0 ! 1209. 3 12/18/0 9 2:1 2 PM ! '3365. 3 13028.3 ! 1209. 4 12/18/0 9 2:1 2 PM I 3365.6 ! 13028.6 ! 1209. 4 12/18/0 9 2:1 2 PM ; 3365.8 ; 13054.8 ! 1209. 5 12/18/0 9 2:1 2 PM ! 336672 ; " ' 1305572 ! 1209. 5 12/18/0 9 2:1 3 PM j ~ 338074 ; i3669.4j 1209. 7 12/18/0 9 2:1 3 PMj "336772 13057.2 ! 1209. 7 12/18/0 9 2:1 3 PMj "'336775 ; 13057.5 ; 1209. 7 12/18/0 9 2:1 3 PM ! 3368.0 ! 13058.0 ! 1209. 9 12/18/0 9 2:1 4 PM ! 3368.5] 13059.5 ; 1209. 9 12/18/0 9 2:1 4 PM ! 3368. 8 13059.8 ! 1209. 8 12/18/0 9 2:1 4 PM ! 3369.2 ; 13033.2 1 1209. 8 12/18/0 9 2:14PM r 3369.5' ' 13060.5 ! 1209. 9 12/18/09 " 2:1 5 PM ! 337676 1 130610 1 1209. 8 12/18/0 9 2:1 5 PM 3370.6 ; 13034.6 ! 1209. 8 12/18/0 9 2:1 5 PM

^ ""3371.1 ; 13062. 1 1209. 7 12/18/0 9 2:15>M ; 337167 " 13062.6 ; 1209. 8



### VES01890 9Unit 4 Ru n 3 1

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### 3373.6 13037.O ! 1210. 3 12/18/0 9 2:1 6 P M 3373. 4 13037.4 ! 1210. 4 12/18/0 9 2:1 7 P M 33747 1 13038.1 ! 1210. 4 12/18/09 2:1 7 P M 3374. 5 13011.5 ! 1210. 4 12/18/0 9 2:1 7 P M 3374. 9 13011.9 ! 1210. 4 12/18/09 2:1 7 P M 33757 4 13012.4 ; 1210. 5 12/18/0 9 2:1 8 P M 3375. 9 13012.9 ! 1210. 5 12/18/0 9 2:1 8 P M 3376. 4 13013.4 ] 1210. 5 12/18/0 9 2:1 8 P M 3377, 1 13014.1 ] 1210. 7 12/18/09 2:1 8 P M '3377. 3 13014.3 ! 1210. 8 12/18/09 2:1 9 P M 3377.6

. 13014. 6 1210. 8 12/18/0 9 2:1 9 P M 3378.0 ; 13015. 0 1210. 7 12/18/09 2:1 9 P M 337873 ! 13015.3 ! 1210. 8 12/18/09 2:1 9 PM

. 3378.3 ] 14226.3

] 1210. 8 12/18/09 2:2 0 PM , """337875 ] 14226.5 ] 1210. 9 12/18/09 2:2 0 PM ! 3378.5 : 14226.5 ] 1211. 0 12/18/0 9 2:2 0 PM ; 3378.5] 14226. 5 1211. 0 12/18/0 9 2:2 0 PM 33787 5 1306175 1211. 1 12/18/0 9 2:2 1 PM

> "'""3378 ] 8 ; 13061.8 ; 1211. 1 12/18/0 9 2:2 1 PM : 337878 7 13088.8 ! 1211. 3 12/18/09 2:2 1 PM : 3378. 8 13088.8 i 1211. 3 12/18/092:2 1 PM i 3378. 9 '13061.9! " 1211. 5 12 /18/0 9 2:2 2 PM ; 3379.0 ! 13088.0 ] 1211. 6 12/18/0 9 2:2 2 PM ; 337971* 1 13088. 1 1211. 7 12/18/0 9 2:2 2 PM i 3379.3 j 13061.3

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## 3385 .1';' " '1385.2;' " 338574 ] 3385.6 1 3385.7 ;

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'Wim^steimp ; Liqui d HR T Tota l Weigh t HRT - I X-2 2 HR J 12/18/0 9 2:4 1 PM ! 12/18/0 9 2:4 1 PM i 12/18/0 9 2:4 1 PM f 12/18/09 2:4 1 PMj 12/18/0 9 2:42 PM ! 12/18/0 9 2:42 PM i 12/18/0 9 2:42 PM | 12/18/0 9 2:42 PM ! 12/18/0 9 2:4 3 PM ! 12/18/0 9 2:4 3 PM i 12/18/0 9 2:4 3 PM i 12/18/0 9 2:4 3 PM ! 12/18/0 9 2:44 PM ! 12/18/0 9 2:44 PM : 12/18/0 9 2:44 PMj 12/18/0 9 2:44 PM i 12/18/0 9 2:45 PM "12/18/0 9 2:45 PM 12/18/0 9 2:45 PM ! 12/18/0 9 2:45 PMl " 12/18/0 9 2:46 PM i " 12/18/0 9 2:46 PM I 12/18/0 9 2:46 PM ! 12/18/0 9 2:4 6 PM j 12/18/0 9 2:4 7 PM

. 12/18/0 9 2:4 7 PM l 12/18/0 9 2:47 PM; " 12/18/0 9 2:4 7 PM ! 12/18/0 9 2:4 8 PM ! 12/18/09 2:4 8 PM j 12/18/0 9 2:4 8 PM l 12/18/0 9 2:4 8 PMf" 12/18/0 9 2:4 9 PM ! 12/18/0 9 2:4 9 PM f 3405. 0 340475 ] 340379 !

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# SPIK E PREPARATION LO G SHEET S

VES01891 3

### Ref ! No , 80/09-03-10 2 Dat e MA R 17 f

### 200 9


## TES TCERTIFICAT E (CERTIFICAT E O F ANALYSIS ) PRODUC T HEXACHLOROETHAN E FOR M . WHITE , CRYSTALLIN E POWDE R (FREE-FLOWIN G MATERIAL ) . COLp R SNOW-WHIT E ODO R CAMPHOR-LIK E PURIT Y{ % BYGLC ) ' 99,9

% •' . \{Z) MELTIN G POINT, . 18 6 ° C (3 ) MOISTUR E (%WT.) •0.011% - . (4)ASH(%wf. ) 0.09 % ;• • (5 ) ^RE E CHLORIN E NI L (6)'WATE R SOLUBL E

: 

### .'CHLORID E (

% NaCl ) 0.016

% (7 ) GRADIN G -1 8 +15. 0 Mes h BS S

VES01891 4HEXACHLOROETHAN E SPIK E BAG S - Targe t Weight : 3. 0 pound s Date 1 1 -A* 4 -Q Q CrewPersonne l \oOL j Shif t I .
•Scal e zeroe d 

## Iiiiii i HHE ! II B litfPiWili i 1 BAG * 

# miii i BAG * 

## iHiiH i 1 

# 5

. 6 2 6 

# 3. 0 5 1 3 . 0 7 6 

# 3. 0 2 3 . 0 2 7 

# 3<

0 5

2 3 . 0 77 

# 3

. 0 3 

## 3 . 0 2 8 •3. 0 5 3 

# 3. 0 7 8 

# 3. 0 4 

# 3. 0 2 9 

# 3. 0 5 4 3 . 0 7 9 

# 3. 0 5 

# 3- 0 30 3 . 0 55 

# ,3. 0 80 

# 3. 0 6 - 3 - 0 3 1 

# 3. 0 56 

## [ 3

. 0 81

. 

# 3 0 7 

# 3> B 3

2 

# 3- 0 57 

# 3. 0 8 2 

# 3.0

. 8 

# 3, 0 33 

# 3. 0 5 8 

# 3- 0 83 

# 3. 0 

# g

. 3 4 

# 3 - 0 59 

# 3. 0 84 

# S- O 1 0 

# 3- 0 3 5 3 . 0 60 

# 3. 0 85 

# 3. 0
n 3 6 

# 3. 0 6 1 

# 3. 0 86 

# 3. 0 1 2 

# 3

. 0 37 

# 3. 0 6 2 

# 3- 6 8 7 

# 3. 0 1 3 3 8 

# 3, 0 6 3 

# 3. 0 88 

# 3. 0 1 4 

# 3

. 0 39 

# 3. 0 6 4 

# 3

. 0 8 9 

# 3. 0 1 5 40 

# 3. 0 65 

# 3. 0 9 0 

# 3- 0 1 6 .41 

# 3. 0 66 

# 3, 0 9 1 

# 3. 0

' -1 7 42 

# 3. 0 6 7 

# 3.f t

. 92 

## 3>b 1 8 43 

# 3 0 68 - 

# 3. 0 9 3 

# 3. 0 1 9 

# S

. 0 44 

# 3: 0 6 9 

# 3- 0 94 2 0 3 . 0 4 5 3 , 0 70 

# 3. 0 9 5 

## 3.0 2 1 4 6 

# 3. 0 7 1 

# 3. 0 96 • 

## 3.0

. 2 2 

# 3. o 4 7 

# 3. 0 72 

# 3. 0 97 

## 3-0 2 3 5 . 0 4 8 3.0.

. 73 •3. 0 9 8 

# 3- 0 2 4 ' 4 9 

# 3. 0 7 4 

# 3

. 0 9 9 

# 3>

0 2 5 

# 3

. o 5 0 

# 3 D 75 

# 3. 0 10 0 

# 5. 0

VES01891 5HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Dat e 1 1 -Q 9 Cre wPersonne l TCiici c, ft. PrccMr , D

. ^cJUlwm^ r

### shif t 1 Scal e zeroe d
m m 

## mmm 

# lliilll ! •am i 

# iHiiii i illllll i 10 1 3 . 0 126 3

. 0 15 1 

# 3 O

. 17 6 

# 3.0 10 2 3 . 0 127 .3. 0 15 2 3 . 0

. 177 

# S.O 103 3 , 0 128 3

. 0 15 3 3

. 0 178 10 4 3 . 0 12 9 3 . 0 15 4 a o 17 9 3 . 0 105 • 

## 3.0 13 0 3 . 0 15 5 3 < 0 180 a o 10 6 3.0

. 13 1 3 . 0 15 6 3 0 18 1 

# 3.0. 10 7 3

. 0 13 2 

## 3,0 15 7 3 > G 18 2 • 3 £ > 10 8 3 . 0 13 3 3 . 0 158 3 . 0 183 

# Z.O 10 9 3

. 0 13 4

. 3 . 0 15 9 3 . 0 .184

. 3 . 0 11 0 3 , 0 13 5 3

. 0 16 0 3

. 0 18 5 3 . 0 •11 1

. 3 - 0 13 6 3 0 16 1 

# 3 ,0 186 

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. 0 13 7

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# 3.0 11 5 3 . 0 14 0 3 D 16 5 3 . 6
. 190 

# &.Q 11 6 5 . 0 14 1 3 . 0 16 6 3

. 0 19 1 3 . 0 11 7 3 . 0 •14 2 .3. 0 16 7 3.0 - 192 3 . 0

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. 0 16 9 3 . 0 194 3 . 0 12 0 3

# >0

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. 195 3 . 0 12 1 3 : 0 14 6 3 . 0 17 1 3 . 0 19 6 3 . 0 12 2 3 . 0 147 ' 3 . 0 17 2 3 . 0 197 3 - 0 123 3 D 14 8 

# 3 .0 17 3 3 . 0 198 3 . 0 124 3 . 0 14 9 

## ' 3D 17

4 • 3 , 0 199 

# 3.0

' 12 5 •3. 0 150

. 3 0 •17 5 3 . 0 20 0 3 . 0HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Date U-&M
- fiQ CrewPersonne l 

# TQitiH cR.Pnm^.S^Qymie rshif t

# i Scal e zeroe d


### : 8A<3 # BAG * WEIGH T(i.BS ) BAG * WEIGH

T<L6Si 20 1 

### 3 . 0 22 6 

# 3.0 25 1 

### S O 276 

### 3 . 0 20 2 

### 3 - 0 22 7 

### 3 . o .252 

### 3 - o 277 

### 3 . o 20 3 

### 3 - 0 22 8 

### 3 . o 25 3 

### s.o 278 

### 3 . o 20 4 

### 3 . 0 22 9 254 

# 3 .o 27 9 

### 3 . o 20 5 

### s . o 230 

### S O 255 

# 3 .o 28 0 

### 3 . o 206 

### <3- 0 23 1 

### 3 . 0 25 6 

### S.o 28 1 

### S . o 207 

### c3. 0 232 

# 3 .o 25 7 

# 3 .0 282 

### 3 . o 208 

### 3. 0 233 

### 3 - 0 25 8 

### 3-D 28 3 

### B . O 20 9 

### 3 . 0 23 4 

### 3. o 25 9 

# 3.0 284 

### 3 . o 21 0 

### 3 . 0 235 

### & o 26 0 

### 3 . o 28 5 

### 3 . 0 21 1 

### 3. 0 23 6 26 1 

### 3 . o 28 6 

### 3 . o 21 2 

### 3. 0 23 7 

### 3 . 0 262 

### 3. 0 28 7 

### S.o 21 3 

### 3- 0 238 

# 3.0 26 3 

### 3 . 0 28 8 

### 3 . o 21 4 

### 3- 0 239 

### S.o 26 4 

### S.o 28 9 

### 3 . o 21 5 

### 3.0 240 

### 3 . ° 265 

### 3 . 0 29 0 

### 3 . o 21 6 

# 3,0 24 1 

### 3 . o 26 6 

### 3. 0 29 1 

### 3 . o 21 7 

### 3. 0 242 

### 3 . 0 267 

### S.o 29 2 

### S. o 21 8 

### 3. 0 243 

### 3 . a 26 8 

### 3 . 0 29 3 

### 3 0 21 9 

### 3. 0 24 4 

### 3. 0 26 9 

### 3 . 0 294 

### 3 . o 22 0 

### S O 245 

### c3. 0 270 

### 3*0 29 5 

### 3 . o 22 1 

### 3. 0 24 6 

### 3. 0 27 1 

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### 3 . o 22 2 

### a o 24 7 

### 3 . o 27 2 

### 3 . 0 29 7 

### 3 . 0 22 3 

### 3 . 0 248 

### 3. 0 273 

### B.O 29 8 

### 3, 0 22 4 

### 3 . 0 24 9 

### 3

. 6 27 4 

# 3.0 29 9 

### 3 . 0 225 

### 3 . 0 250 

### 3 - 0 27 5 

### 3. o 30 0 

### S . o

VES01891 7HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Date ll-^-Q^ i CrewPersonne l I •WW TShif t 1

C ~ XV^oJca^v n Scal e zeroe d

BAG * BAG # WEIGH T(LBS > BA G # HEIGH

T(LBS ) 30 1 32 6 35 1 37 6 30 2 32 7 352 

# 3 o 377 P>-7 S 303 

# •V A 32 8 3 c > 353 

# A a 37 8 

## 2>C\ 30 4 32 9 3 o 35 4 

## 3 - A 37 9 

### d o 305 33 0 a o > 355 

### 3 - a 38 0 3D 6 33 1 356 38 1 307 3 - 0 332 357 

## 3 - A 38 2 308 

# 3 D 33 3 

### 3 A 358 38 3 309 334 35 9 

### ,3- a 384 

# B O 31 0 33 5 

### 3 0 360 

### I 3 0 38 5 31 1 336 

## "Pt-Cs 36 1 38 6 

### 3 - a 31 2 33 7 362 38 7 

### 3 o 31 3 338 36 3 38 8 3-f t 31 4 3 C > 33 9 

## 8 a 364 

## 3 d 38 9 31 5 340 

# r a 365 39 0 • A O 31 6 34 1 36 6 39 1 

# r o 31 7 342 3-C v 36 7 39 2 31 8 343 

# R A 36 8 39 3 31 9 344 3 - 0 36 9 ,9- a 39 4 3 ^ 32 0 345 

## 3 - D 37 0 39 5 

### a o 32 1 346 37 1 39 6 

# 30 ) 32 2 347 372 3 - 0 39 7 s o 32 3 348 3
- 0 373 3 - D 39 8 32 4 34 9 

# 3> 0 37

4 3 0 399

. 32 5 3
- 0 35 0 

### B O 375 

# c *7 ) 40 0 

# 30HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Date 

# IW ^V M.-Q ^ CrewPersonne l \

. Qlvftk , £

### •ftcd^ ^^oUsmw
- 

### shif t I O l Scal e zeroe d 

# iiiiii i 1 n n liiiiii i



# 111111 1 iiiiiii

s H H 1 1 Hill ! •ISII ! 40 1 42 6 

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# 3.

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# 3- 0 40 3 42 8 

# 3. 0 45 3 

# 3.

0 478 

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## 2D 454 

# 3. 0 47 9 

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## 3-C> 45 5 

# 3. 0 48 0 

### B

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. 40 6 

# 3- 0 43 1 

## 3

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### 3

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# 3.

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# 3.

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# 3.

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# 3- 0 484 41 0 a o 43 5 

## 3 -C > 46 0 

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## 3.0 43 9 

# 3. ^ 464 

### 3

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### 3

< o 41 5 

# 3- 0 440 

## 3

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# 3. 0 49 6 

# 3.

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## 3

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# 3.

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## 3.o 47 3 

# 2>, 0 498 

# 3.

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## 3^0 474 

# 3. 0 499 

# 3.

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## 3.0 475 

# 3. 0 500 

# 3.

0

VES01891 9

### HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Date //
- 23 -O^

CrewPersonne l /•/I//A/<T'ST G M 

# J *&cSZC/k. Shif t

## 2 hid Scal e zeroe d 

## liiiiii i iiiiillll i ISIil l iiilii i Biiffli l •Hil l MIGHT

## (lilt ) 50 1 

# libs 526 

### 3/6$ 55 1 57 6 

### 3 /h3 50 2 

### 3-

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### b - 5 . 52 7 • 

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. 

# ? JhS 50 3 

### 3 \bS 528 

### 3/b5 553 

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# ibs 578 

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### 3 W 52 9 

### J/As 55 4 

### 3/h$ 579 

### 3 /f,3 50 5 

### 3 lb s 530 

### 3fbl> 55 5 

### 3/£5 580 

# 3 /h 50 6 

### 3 \hs 53 1 556 

### 3/b? 58 1 

### 3 fhS 50 7 

### 3 ib S 53

2 557 

### 3/b* 582 

### * lb* 50 8 

### 3 \hS 533 

### Z/65 558 

### 3/SS 583 

### 3/65 50 9 

### 3 tb s 53

4 

### 3/65 559 

### 3/h£ 58 4 

# 3 /hS 51 0 

### 3

lb s 53

5 

# Kb? 560 

# 3

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# 3

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### 3 \\>3 53

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### 3/63 56 1 

# 3

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# 3

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### Sib* 537 

### 3'/As 562 

### 3/bf 587 51 3 

### 3

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### 3fb5 563 

### 3/h5 588 

### 3/b? 51 4 5lb 5 539 

### 3/6? 56 4 

### 3fhi 589 

# 3

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### 3/As 565 

### 3 tb$ 590 

### 3



# Ms 51 6 

### 3

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### 3/hf 566 

### 3 Jb S 59 1 

### 3fhS 51 7 

# 3 Ik r 54 2 

### Jlhs 567 

### 3 /fc 592 

# 3 IM 51 8 

### 3\h5 543 

# 3 /JbS 568 

### 3/bf 593 

# 3/fc 51 9 

### 3

\bS 544 

### 3/63 569 

# 3 /As 594 

### 3/63 52 0 S Ib5

. 54 5 

### 3/h

5 570 

### 3

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### 31bf 546 

### 3/63 57 1 

### 3 //? 596 

### 3/6? 52 2 

### 3\y? 547 

### ?/hs 57 2 

# 3 /6 597 

### 3

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### 3 IJ>s 548 

### 3

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# 3 /6 598 

# 3 /h 52 4 

### 3 lbs 549 

# i

as 57

4 

### 3 

# /6 599 

### 3



# Us 52 5 

### 3 /£ S 550 

### 3/6? 57 5 60 0 

# 3

/6?

VES01892 0HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Dat e 

### }f-23-b> < 

### f CrewPersonne l 

# b 1 (/

'f "y-fo-/u /' %o2bi Shif t ZAICL Scal e zeroe d 

## ISiil S wmmm 

## lillllff l BAG * 

### mmm 

## IIMI I IIBIil l 60 1 

### 3/h 62 6 

### 3/h 65 1 

### 3/b 676 3 // > 60 2 

# 3 /b 62 7 

# 3

/h 65

2 

### 3/b 677 

### 3



# IB 60 3 3 

### Ih 62 8 

### 3/6 653 

### 3/b 678 

### 3/b 60 4 

### 3/h 62 9 

### 3/b 65 4 

### 3/h 67 9 

### 3/b 60 5 

### 3/h 630 

### 3/b 65 5 

### 3/b 680 

### <s)b 60 6 

### 3/b 63 1 

### l i b 656 

### 3/b 68 1 

### ?/b 60 7 

### 3 )b 632 

### 3/b 657 

### 3/b 682 

### 3/b 60 8 

### 3/b 63 3 

### 3/b 658 

### 3/b 68 3 

### 3/b 60 9 

### Jib 634 

### 3/b 659 

### 3/h 684 

### 3?Jb 61 0 

### 3/h 63 5 

### 3fb 660 

### 3/b 685 

### 3lb 61 1 

### 3/6 63 6 

### 3/b 66 1 

### sib 686 

### 3 lb 61 2 

### 2 lb 637 

### 31b 662 

### 3 Ib 68 7 

### 3

lb 61 3 

### 3/b 63 8 

### 3/b 66 3 

### 3/b 688 

### 3/h 61 4 

### 3/h 63 9 

### 3 lb 66

4 

### 3(b 689 

### 3 lb 61 5 

### 3/b 64 0 

### 3/b 665 

### 3/b 690 

### 3/b 61 6 

### 3 

# IS 64 1 

### lib 666 

### 3 /b 69 1 

### z(b 61 7 

### 3/h 64 2 

### 3/b 667 7 

### Ih 692 

### 3/b 61 8 

### 31 h 64 3 

### 3/h 668 

### 3/b 693 

### ?fb 61 9 

### 31k 644 

### 3 lb 669 

### 3/h 694 

### 3/b 620 

### 3 lb 64 5 

### 3/h 67 0 

### 316 695 

### 3/h 62 1 

### Z/£ 64 6 

### 3 ih 67 1 

### 3

lb 69 6 

### 3/b 62 2 

### 3/b 64 7 • 

### 3 lb 67

2 

### 3/b 69 7 

### 3 Jb 623 

### 3 

# Ih 648 

### 3/b 67 3 

### 3/b 698 

### 3/b 62 4 

### iM 64 9 

### ?/b 67 4 

### 3/3) 69 9 

### 3 ff? 62 5 

### 3/b 65 0 

### 3/ i 67 5 

### 3 / h 70 0 

### 3>lbHEXACHLOROETHAN E SPIK E BAG S - Targe t Weight : 3. 0 pound s Date 

# /f'Z3-<5 '9 CrewPersonne l 

# Lti/ftf$ TTQAIJ shif t z^rd Scal e zeroe d ]/<£" ?

IHH « Ivi 'BA' G '#,!•' WEIGHT , (LBS ) BA G 

# P WE!GHTj!(LBS ) WEIGH T(LBS ) 

# 70 1 

# •3 lb 72

6 

# 3 lb 75

1 

# 3/h 77

6 70 2 3

# Ih 72

7 

# 3 

# ib 75

2 

# 3 /b 77 7 70 3 72

8 

# 3/b 75

3 

# 3 /S 77 8 

# 3 /6 70 4 

# 3 

# ih 72

9 

# 3 lb 75

4 

# 3 /b 77 9 ? t f

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# 70 5 

# 3 lb 73

0 

# 3 lb 75

5 

# lib 78

0 

# 3/b 70 6 

# 3 

# jb 73

1 

# 3 lb 75

6 

# 3 Ib 78

1 

# 3 /b 70 7 

# 3 lb 73

2 

# 3 lb 75

7 

# 3lh 78

2 

# 3/b 70 8 

# 3 \b 73

3 

# 3ib 75

8 

# 3lb 78

3 

# 3/b 70 9 

# 3 |f > 73 4 

# 3 lb 75

9 

# 3 lb 78

4 

# 3/b 71 0 

# 3 

# )h 73

5 

# 3/b 76

0 

# 3 /b 78 5 

# 3/b 71 1 

# 3 ) t

> 73 6 

# Jlh 76

1 

# 3 lb 78

6 

# 3 

# It? 71 2 * l b 

# 73

7 

# lib 76

2 

# 3)b 78

7 

# 3lb 71 3 3

# \h 73

8 

# lib 76

3 

# 3 /b 78 8 

# 3 

# Ib 71 4 73

9 

# Jib 76

4 

# 31b 78

9 

# 3 )b 71 5 

# 3

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# 74

0 

# 3 lb 76

5 

# 3lb 79

0 

# 3 

# lb 71 6 

# ? \b 74

1 

# 3 Ik 76

6 

# *lb 79

1 

# 3li> 71 7 

# 3 

# lb 74

2 

# 31}? 76

7 

# 3 lb 79

2 

# 3)1 71 8 

# 3 )b 74 3 

# 3fb 76

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# 3 lb 79

3 

# 3 \h 71 9 

# 3 Ih 74

4 3 / t 

# 76

9 

# 3 /h 79 4 

# 3 \b 72 0 

# 3 

# lb 74 5 J A 77 0 

# 3/b 79

5 

# 3\b 72 1 

# 3 \b 74

6 

# 3 Ib 77

1 

# 3 lb 79

6 

# Jib 72 2 

# 3 

# h 74

7 

# 3(b 77

2 

# 3ib 79

7 

# 3I& 72 3 

# •3 Ih 74

8 

# ?lb 77

3 

# ?lb 79

8 

# 7 lb 72 4 

# 3 

# ib 74

9 77

4 

# 3lb 79

9 

# 3lb 72 5 

# 3 jb 75

0 

# Kb 77

5 

# 3lb 80

0 

# 3/b

VES01892 2HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s CrewPersonne l 

### shif t /<£T P Dat e
Scal e zeroe d 

## liiiiii i 

# n n H H 

# msi i lliilllll H i 80 1 

# 3 LBS 82 6 

# 3^5 85 1 

# 3 876 

# 3 80 2 82 7 852 87 7 3 LIBS 80 3 82 8 

### 3 L%S 853 

# 3 a& 878 

# 3 i&s 80 4 82 9 854 87 9 

# 3 L&S 80 5 , 83 0 

# 3 as 855 

# 3 88 0 

# 3 l~&3 80 6 

# 313$ 83 1 

# 3 856 

# 3 i&s 88 1 80 7 

# *3l£$ 832 857 882 

# 3 UBS 80 8 

# 3 IBS 83 3 858 , 

# 3 

# i&z 88 3 

# 3 /3 5 80 9 < 834 859 , 

# 3 884 

# 3 ms 81 0 83 5

. 

### 3 L$S 860

. 88 5 

# 3 

# LBS 81 1 

# 3 ^ S 836 3L& S 86 1 886 3 L&S> 81 2 

# 3 

# i&s 837 

## 3L &S 862 

# 3 i&$ 88 7 , 

# 3 81 3 83 8 863 88 8 

# 3 81 4 83 9 86 4 

# 3 i&$ 88 9 

# 3 L&S 81 5 84 0 

# 3^ 865 89 0 81 6 

# 3 USif 84 1 866 89 1 

# 3 >L &5 81 7 

# 3 LB? 842 i 867 

# 3 L&S 89 2 81 8 

# 3m> 84 3 868 89 3 

### 3 L&S 81 9 

# 3 LBS 844 869 

# 3u$s 894 < 820 84 5 

# 3>^s 870 89 5 

# 3 i~F< : 82 1 846 , 

## yl £S 87 1 

# -$ug>s 89 6 

# 3 

# hB? 822 84 7 

# 31-35 872 89 7 

# 3 L&S 823 84 8 v 873 89 8 

# 3^s824 84 9 

# 3 ^ 87 4 

# 3 LBS 89 9 

# 3 >-&s S2 5 

# 3 85 0 

### 3 /-B 5 875 

# 3 L^S 90 0HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Cre wPersonne l D

, U AlAV O HI ; S. 'B&O^ZlZ} Date , Shif t Scal e zeroe d 

## IIIIII H liiiiii i

m m m 

## Iiiiii i

•iiiiii i Hiiil l iiiiii i Iiilii i 90 1 3 L&<? 92 6 

# 3 95 1 

# 3 L&S 976 4 ? LBS 90 2 

# 3 L.-&S 92 7 3 L&? 952 

# 3 LB? 97 7 

# 3 LBS 90 3 

# 3 us>5

92 8 953 

# 3 LBS 978 

# 1 )~%S 90 4 « 

# 3 

# u&s 92 9 3 AB> 5 954 

# 3 l &S 979 

# 3 LUS 90 5 

# 3 930 95 5 

# 3 LBS 980 

# 3 LBS 90 6 

# 3> LB S 93 1 

# 3 

# ms 956 

# 3 

# LBS 98 1 

# 3 

# up< 90 7 932 

# 3 LBS 957 

# 3 LVS 982 

## 3 LB <S 90 8 3 >LB 5 93 3 

# 3 Lib? 958 

# 3 Lb? 983 

# 3 LBS 90 9 

# 3 U5 5 934 

# 3 

# LB5 959 

# 3 LQ^ 984 

# 3 Lb? 91 0 , 

# 3 u& s 935 , 

# 3 

# LB5 96 0 

# 3 L&? 985 

# 3 Lh* 91 1 936 

# 3L $,i 96 1 3 L&$ 98 6 

# 3 L&? 91 2 

## 3 US>5 937 *> L&? 96

2 

# 3 Lbs 98 7 

# 3 

# L&S 91 3 

# 3 i&s 938 

# 3 L&S 96 3 3 ^-BX 98 8 , 

# 3 LBS 91 4 

# 3 L&S 939 

# 3 L&S 96 4 3 L&? 98 9 91 5 2 >LB 5 940 

# 3 LBS 96 5 

# 3 LB* 99 0 

# 3 LBS 91 6 941

. 3 *-B> S 96 6 

# 3i&? 99 1 

# 3t-$s 91 7 , 94 2 3 LB>J ? 967 

# 3 19$ 99 2 3 PB? 91 8 

# 3 LB? 943 96 8 

# 3 LB* 99 3 3 LB? 91 9 3 LB 4 ? 94 4 

# 3t-&> 969 3 LB$ 99 4 3 L&S 920 94 5 I 3 L&S 97

0 3 L?>S 99 5 3 LB<? 92 1 

# 3 94 6 

# 3 LB $ 97 1 

## 3 L 3 S 99 6 

# 3 LB? 922 

# 3 Le>? 94 7 3 L$S 97 2 3 I & * 99 7 

# 3 LBS 92 3 

# 3 LBS 948 3 L%S 97 3 

# 3 L&S 99 8 3 >L£$ 92 4 

# 3 949 

# 3i&s 97 4 

# 3 w 99 9 3 L&? 92 5 

# 3 LBS 950 

## 3 L 3 S 97 5 

# 3 LBS 1000 

# ?>LPS

VES01892 4HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s

CrewPersonnelD , S, B ^C^ T / r rZ > Dat e Shif t Scal e zeroe d 

## Nin H 

# mmm •Mil

l i m 

## llllllH

I HIBil l Iiilii i iiiiiii i
100 1 . 

### 3 ^-BS 1026 < 

# 3 ijss 105 1 

## $ Lft* 107

6 

### 3/-B5 100 2 1027 < 

### 3 JLBS 105 2 

# 3 LBS 107 7 

# 3 t-BS100 3 - 

# 3 LBS 1028 

### 3/.BS 1053 

# 3 IBS 107 8 

# 3, LB? 100 4 

# 3 LBS 1029 

# 3 

# i^s 105 4 

# 3 L&S 107 9 

# 3 LBS 10C 5 t 103 0 

# 3i&s 1055 

# 3 iss 1080 

# 3 LR f 100 6

. 

# 3 103 1 

# 3u$<? 1056 

# 3 LB? 108 1 

### 3 L&* 100 7 

# 3> LB? 103 2 

# 3 u$s 105 7 

# 3 13 5 108 2 

# 3 LS? 10O 8 

# 3 LB< 103 3 

### 3 L%>? 1058 

# 3 LBS 108 3 

# 4 LB? 100 9 

# 3 us? 103 4 

# 3 ±.j$?

1059 

# 3 ISS 108 4 

# 3 L$S 101 0

. 

# 3 IRS 103 5 

# 3 LBS 1060 

# 3 LB? 108 5 

# 3
101 1 , 3LZ? 103 6 

### 3 L5S> 106 1 

# 3 108 6 { 

# 3 LPS 101 2 3 USLS 1037 % LB< 106

2 

# 3 L&S 108 7 

### 3 L$7 101 3 

### 3 L&,<> 103 8 

### 3 LRS 1063 

### 3 L&5 108 8 

### 3 L#S 101 4 

## 3l &S 1039 

### 3 XBS 106 4 

# 3 LBS 1089 

# AIMS 101 5 

## 3> L&<? 104 0 

# 3 LB? 1065 

# 3 LBS 109 0 

# 3 LBS 101 6 

### (3 /3 5 104 1 

# 3u&s 106 6 ALB * 109 1 

### 3 >L1^? 101 7 , 

# 3k& 104 2 

### 3 L&* 106 7 

# 3 LBS 109 2 

### 3 LBS 101 8 , ILK? 104 3 

### 3 LBS 106 8 

# 3 LBS 1093 

# 3

—5 101 9 

# % up?

. 104 4 

## 3i -BS 1069 

# 3 LBS 109 4 

# 3 LBS1020 

# 3 LBS 104 5 

### 3 L&? 107 0 

# 3 LBS 1095 

# 3 L-&S 102 1 

# 3uBS 104 6 

### 3 L&? 107 1 

### 3 *-BS 109 6 

# 3 

# ts? 102 2 

## 3 >L&? ' 104 7 

### 3 J-B$ 107 2 

# 3 L-p c 1097 

# 3 LBS 102 3 

### 3 L£S- 104 8 

# 3 UBS 107 3 

# 3 LPS 109 8 

# 3 ms 102 4 

### 3 L&? 104 9 

# 3 L ^ 107 4 

# 3 LP? 1099 1025 

# 3 ABS: 105 0 

# 3 V&S- 107 5 

# 3 L&S 1100 

# 3 LBSHEXACHLOROETHAN E SPIK E BAG S - Targe t Weight : 3. 0 pound s CrewPersonne l ft 

# UNMAhUtJi ; 

# 5 > 

# ^BCt^P ] Shif t /<ST 2^ Scal e zeroe d ^^S^ 

## IHH I II I 11 1 HHBHR I liflll i 111111 1 WEIGH T(LBS ) 

## Iiiiii i

iiffliii i 110 1 

# 3 LB? 1126 , ^AB? 115 1 

# 3 AE? 117 6 3 ±B<> 110 2 

# 3 LB?- 112 7 t 1152 

# 3^&? 117 7 

# 3 LB? 110 3 

# 3 LSS- 1128 

# 3 LBS 1153 

## 3^ B? 117 8 

### 3 *~BS 110 4 

# 3 L&* 1129 

# 3 LBS 1154 

### 3 LB? 117 9 

# 3 LB? 110 5 

# 3 LBS 113 0 

### 3 Lfc< 1155 

# c 3 LB? 118 0 

# 3^~Bs 110 6 113 1 115 6 

### 3 AP,? 118 1 

### 3 L.BS 110 7 

# 3 113 2 

# 3 i&s 1157 

# 3u&5 118 2 

### 3 L-BS 110 8 

# 3 is? 113 3 

# 3> LBS 115 8 

# 3 LBS 118 3 

# 3 LBS 110 9 3 LV><> 113 4 

### 3 L&? 115 9 

## 3 L^ 118 4 

# 3 LB? 111 0 

# 3 L&S 113 5 

### 3 LSS 1160 , ^L&S 118 5 

### 3 LB? 111 1 £

LB* 113

6 

### 3 LBS 116 1 , 

# 3 LBS 118 6 

### 3 LB^ 11 1 2 113 7 

### 3 LBS 1162 < 

# ^7Jp>? 118 7 

## 3 >LB<5 11 1 3 

# 3i ~B<t113 8 

# 3u&$ 1163 , 

### 3 L&? 118 8 

### 3 L-BS 11 1 4 

# 3 LB? 113 9 

### 3 AB? 1164 

### 3 L&S 118 9 

### 3 LBS 111 5 

# Pi LPS 114 0 

# 3)~9?

1165 SLBS 1190 SLB^ 111 6 

# 3 L&<; 114 1 

# 3i3S 1166 

# 3 LB? 119 1 

### 3 LR? 111 7 

# 3 LB * 114 2 

### 3 LJ*.< 116 7 

# 3 LBS 119 2 

### 3 L$^ 111 8 

# 3 LB? 114 3 

### 3 LBT 1168 

### 3 LBS 1193 

# 3 LBS 111 9 

### 3 L&? 114 4 

# 3 LBS 116 9 

# 3 LBS 119 4 

# 3 »~B ? 112 0 

# 3 >L &5 114 5 

### 3 L&? 1170 

# 3 LB<Z 1195 

### 3 LBS112 1 

# 3 LBS 114 6 ALB? 117 1 

## *>L3? 1196 112 2 

# 3 >L &iZ 114 7 

### 3 LBS~ 1172 < ^^LBS 1197 

# 3^&s 1123

. 

### 3 LKS 114 8 

# 3 LBS 1173 

# 3 LBS 119 8 

# 3 L 8? 112 4 

# 3 LBS 114 9 

# 3 LBS 1174 1199 

### 3 LZS 1125 

# 3iSS 1150 

# 3 LBS 1175 

# 3 1200 

# 3<-Bs

### HEXACHLOROETHAN E SPIK E BAG S - Target Weight ; 3. 0 pound s Date// ~MzP CJ"-, CrewPersonne l 

## T)*

M/JI M fi/ZfJ/, S. TK&ZfCtt. Shif t /« y, D 

# Y< W/^/rLx/

Scal e zeroe d 

## \JS<> 

# mmm ;1SI3

1 lillll l Hil l 1 1 111111

1 IllSii i 120 1 

### 3 LBS 122 6 , 

### 4 LB? 125 1 

### 3 L&<? 127 6 

### 3 >J-B? 120 2

. °>LBJT 1.227 

# 3 LBS 125 2 

# 3 z ^- r 127 7 

# 3 LB? 120 3 

# 3 LBS 122 8 

# 3 LB* 125 3
. ILB? 127 8 

# 3 LBS 120 4 

# 3 LSS 122 9 

# 3 L&? 125 4 

# 3 LBS 127 9 

# 3 LBS 120 5 , 

# 3 LBS 123 0 

# 3 LBS 125 5 

# 3 LBS 128 0 

# 3 LPS 120 6 , 

# 3 123 1 

### 3 LB* 1256 

# 3 L&S 128 1 

# 3 LBS 120 7 

# 3 23 -

7 123 2 

# 3 LB< 125 7 

## 3 LM 128 2 

### 3 LB3 120 8 

### 3 L$S 123 3 

# 3LBJS 125 8 

# 3 LB? 128 3 

### 3 LBS 120 9 

## (3 L&5 123 4 

### 3 LB<T 125 9 

# 3 L$Z 128 4 

### 3 L$S 121 0 

### 3 L&J? 123 5 

# 3 AB-T 126 0 

# 3 LB? 128 5 

# 3 LBS 121 1 

# 3 LBS 123 6 

## 3 LRf 126 1 

# 3 LB? 128 6 

# 3 LBS 121 2 

# 3 LBS 123 7 

# 3 LBS 126 2 

# c3 LBS 128 7 

# 3 LB? 121 3 

# 3 LBS 123 8 

### 3 L£.<> 126 3 

# 3m? 128 8 

# 3 LBS 121 4 

# 3 LBS 123 9 

### 3 L$S 126 4 

### 3 LBJ 128 9 

# 3 LBS 121 5 

# 3 LBS 124 0 

# 3 Lp< 126 5 % LBS 129 0 

# 3) LB? 121 6 

### 3 LB.$ 124 1 

# 3 LB? 126 6 

# 3*- B? 129 1 

# 3 LB?. 121 7 

### 3 LB* 124 2 

# 3 LBS 126 7 

# 3 LBS 129 2 

# 3Lfr?
121 8 

### 3 L&S 124 3 

### 3 >LP>? 126 8 129 3 

### 3 L&S 121 9 

### 3 LB* 124 4 

### 3 ^9S 126 9 

# 3 LB? 129 4 

### 3 L&? 122 0 

# 3 LBS 124 5 

# 3 LB? 127 0 

# 3 LBS 129 5 

# 3 IBS 122 1 

# 3uf« 124 6 

# 3 L &f 127 1 

# 3) LB? 129 6 

# 3 LBS 122 2 

## 3 ^BS 124 7 

### 3 LB< T 127 2 

# 3 LBS 129 7 

# 3 iss
122 3 

### 3 LB<Z 124 8 

### 3 LB<? 127 3 

# 3 13? 129 8 3 LP<> 122 4 

### 3 LRJT 124 9 

### 3 LRS 127 4 

# 3 &3 129 9 

# 3 LB? 122 5 

## \3 LQS 125 0 

# 3 LBS 127 5 

# 3 LBS 130 0 

### 3 ^BSHEXACHLOROETHAN E SPIK E BAGS-Targe t Weight : 3. 0 pound s Cre wPersonne l Date/ / Shif t /-ST 73 Scal e zeroe d 

# lilililli l 

# mmm IliiS , WEIGHT ' <LB§| : 

# Iiiiiii i



# mmm 130 1 

# 3 LB? 1326 , 

# 3 LB? 135 1 A LB? 137 6 

# 3 ABf 130 2 

# 3 LBS 1327 

# 3 LB ? 135

2 

# 3 LBS 1377 , 

# 3 LB? 130 3 

### 3 L&<> 1328 

# 3 LB ? 1353 

# 3 LBS 137 8 

# 3 LB? 130 4 

# 3 LBS 1329 

# 3 LB? 1354 

# 3 LB? 137 9 

# 3 LB? 130 5 133 0 

# 3 LB? 1355 

### 3 Lft *7 138 0 

# 3 LB? 130 6 

### 3 L%? 133 1 

# 3 LB? 1356 

# 3 LBS 138 1 

# 3 LR? 130 7 

# 3 LB? 133 2 

# 3 LB? 1357 

# 3 LB? 138 2 

# 3 L&S 130 8 

# 3 LB? 133 3 

# 3 LB? 1358 

# 3 LBS 138 3 130 9 

# 3i~&? 133 4 

# 3 LB? 1359 

# 3 LBS 138 4 

### 3 L-B S 131 0 

# 3 ^B>? 133 5 1360 

# 3) LBS 138 5 

### 3 LB? 131 1 1336 

# 3 LBS 136 1 

# 3 LBS 138 6 

### 3 LBS 131 2 

# 3 LBS 1337 

# 3 LB? 1362 A IB? 1387 

# 3*-br 131 3 

# 3 LB? 133 8 

### 3 LB? 1363 

### 3 >L&? 138 8 

### 3 L&<? 131 4 

# 3 LB? 1339 

### 3 *&5 136 4 

### 3 LBS 138 9 3 L&<S 131 5 

# 3 LB? 1340 

# . 3 LBS 1365 139 0 

# 3 LB? 131 6 

# 3 LB S 134 1 

### 3 LU? 1366 

# 3 LBS 139 1 

### 3 LB^ 131 7 

# 3 LBS 134 2 

### 3 LB? 1367 

### 3 LB< 139 2 

### 3 LB? 131 8 

# 3 134 3 

# 3 L&? 1368 

# 3 IB? 1393 

# 3 its 131 9 

# 3 LBS 134 4 

# 3 LB? 1369 

### 3 L&< 139 4 

# 3 LBS 1320 

# 3 >i&? 134 5 ALB ? 1370 

### 3 L<B,? 139 5 

### 3 LQS 132 1 

# 3 LB? 134 6 

# 3 LB? 137 1 

### 3 LPS 139 6 

# 3 LB? 1322 

# 3 LB? 134 7 

# 3 LB-T 137 2 

# 3 LB? 1397 

### 3 LB<? 1323 

# 3 LBS 134 8 

# 3 LB? 1373 

### 3 LB<; 139 8 

# 3 LB? 1324 

# 3 LBS 1349 

# 3 LBS 137 4 

# 3 LB? 1399 

### 3 LB>S 132 5 

# 3 LBS 1350 

# 3 LBS 137 5 

# 3 LBS 140 0 

## 3 L^HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Cre wPersonne l b < 

## MPlAUdfiitCy f 

### 7" 7 DdOV^ J Shif t Scal e zeroe d 

# iliiiiiil mmmm IIKI

I iilii i liiiiii i Hlfflil i liiiiii i itmaigtimmrrmiiu m 140 1 1426 

### 3 L&* 145 1 

### 3 LB<Z 147 6 

# 3 ups 140 2 

# 3 LB? 1427 

# 3 L&S 145 2 

# 3 LB? 147 7 

# 3 LB? 140 3 

# 3 LB? 1428 

# 3 Lh 

# * 145 3 3 LB<?> 147 8 

# 3 LB? 140 4 

# 31&? 142 9 145 4 

# 3 LB? 147 9 

# 3 LB? 140 5 

# 3 LB? 143 0 

# 3 i&? 145 5 • 

# 3 L%< 1480 

# . 3 LBS 140 6 

# 3 143 1 

# 3 V&t 145 6 

# 3 LB? 148 1 

# 3 LB? 140 7 

# 3 LB S 143 2 

# 3 L &g 145 7 

# 3 L&? 148 2 

# 3 LB? 140 8 

# 3 LB? 143 3 

## %LBS 145 8 

# 3 LB? 148 3 

# 3 LPS 140 9 

# 3 LB? 143 4 

# 3 L &S 145 9 

# 3 LB? 148 4 , 

# 3 }LBs 141 0 

# 3) LB£ 143 5 3 

## LBS 146 0 

# 3 L&f 148 5 

# 3 L&r 141 1 

# 3 LBS 143 6 

# 3 LB? 146 1 

# 3 LB? 148 6 

# 3 LBS 141 2 

# 3 LB? 1437 

# 3 L&? 146 2 

# 3 LB? 1487 

### 3 L$S 141 3 

# 3 LB? 143 8 

# 3 

# ^s 1463 

# 3 >LBf 148 8 QL& S 141 4 

# 3 LB? 1439 

## %Lp? 146 4 

# 3 LBf 148 9 

# 3 LBS 141 5 

# 3 LB? 144 0 

### 3 LB?- 146 5 

# 3 LBS 149 0 

# 3) Lb? 141 6 

# 3 LB? 144 1 

# 3 LBS 146 6 

### 3 AB? 149 1 

# 3 LB? 141 7 

# 3 >LB<- 144 2 

# 3 LB? 146 7 

# 3t -B? 149 2 

# 3 LB? 141 8 

# 3 L&Z 144 3 

# 3 LB? 146 8 

# 3 LB? 149 3 

# 3 LB< 141 9 ( *>

LBS 144

4 

# 3 LB? 146 9 3

# ws? 149 4 

# 3 LB? 142 0 < 3 JLB * 144 5 

# 3 Lb? 147 0 

# 3 LB? 149 5 , 

## 3 >L-B ?T 142 1 

# 3 144 6 $LBS 147 1 

# 3 LB? 149 6 c 3 

## LBS 142 2 

# 3 LB? 144 7 

# 3 LBf 147 2 

# 3 LB? 149 7 

# 3 LB? 142 3 

# 3 LB? 1448 

# 3 L&S 147 3 

# 3 LB? 149 8 

# 3 LB? 142 4 

# 3> L$$ 1449 

# 3 LB? 147 4 

# 5 LBS 1499 

# 3 LB? 142 5 

# 3 AV : 1450 

# 3 LBS 147 5 

# 3 LBS 150 0 

# 3 LBS



### VES01892 9HEXACHLOROETHAN E SPIK E BAG S - Target Weigh t 3. 0 pound s Date / I CrewPersonne l J> > 

### l^AUWj '6 

# H lc 

# M j 

# 7 ^ £>OV ^ 2 

### , Shif t

### /?H~

# X > V « \A/f<&Tl

l / Scal e zeroe d 

### V^SZ iiiiiill i 

### wmm mmm WEIGH T(LBS ) WEIGH T(LBS | llllili l 150 1 

# 3 x& 1526 3 LP>? 155 1 , 

# 3 L^,< 1576 

# 3 Lp? 150 2 

# 3 LBS 1527 

# 3 ISS 155 2 

# 3 

# LR? 1577 

# 3 LB? 150 3 

# 3 XB 5 152 8 

# 3 /LBS 155 3 

# P> LB?

1578 

# 3 LBS 150 4 , 

# 3 LBS 1529 

### 3 L&>S 155 4 

# 3 LP? 157 9 

### 3 LB& 150 5 • 

# 3 

# L&S 153 0 

### 3 L^S 1555 

# 3 LB? 1580 ( 

# 3LB? 150 6 , 

# 3 LBS 153 1 

# 3 LBS 1556 

# 3 LB? 158 1 

### 3 L&S 150 7 , 

# 3l&S 153 2 

# f^LB< 1557 

# ^LB? 158 2 

# ^>Lfr? 150 8 

### 3 LB^ 153 3 , 

# 3 

# (SB<

1558 

# 3) LB? 1583 , ^L3 ? 150 9 

# 3 LBS 153 4 < 

### 3 LB<; 1559 

# 3ut? 158 4 

# 3 IBS' 151 0 

# 3) LBS 153 5 

### 3 L&S 1560 

# 3 

# L&? 158 5 < 151 1 < 

# 3 

# LBS 153 6 

# 3 LB*

•1-561 - 

# 3>LB? 1586 

### 3 LBS 151 2 153 7 

### 3 LB>? 156 2 

### 3> L;B? 1587 

# 3 LBS

•» : 151 3 

# 3 LBS 153 8 

# 3 )L &S '156 3 

# 3u$< 1588 

# 3 LBS 151 4 

# 3 LBS 1539 

### 3 LBS 156 4 

# 3i&r 1589 

# 3 L&<? 151 5 

# 3 LBS 154 0 

# 2>LBS 156 5 

# 3 ib? 1590 

# 3 LBS: 151 6 

# 3 LB? 154 1 

# 3 LBS 1566 

# 3 LB? 159 1 

# 3 L&? 151 7 

# 3 LBS 154 2 

# 3 LBS 1567 

# 3 LBS 159 2 151 8 

# 3 LBS 154 3 1 

# 3 LBS 156 8 159 3 , 151 9 

# 3 

# LB< 154 4 ' , 

# 3 LBS 1569 159 4 152 0 

# 3 LB? 154 5 

# 3 LB? 157 0 

# 3 LBS 159 5 

### 3 LB< 152 1 

# 3 LBS 154 6 

# 3 LBxS

157 1 

# 3 LBS 159 6 , 

### 3 L&S 152 2 

# 3 ms 154 7 

# 3 m 157 2 

# 3 L& r 159 7 1523 

# 3 LBS 154 8 « 

# 3 LBS •157 3 

### 3 LBS 159 8 

### 3 /35 * 152 4 

# 3 LBS 154 9 < 

### 3 LB<S 157 4 

### 3 LB< 159 9 

### 3 LBT 152 5 

# 3 LBS 1550 3ta s 157 5 

# 3 ms; 160 0

. 

# 3 LBSHEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Date Cre wPersonne l D /



## (4AU\ Vf>/V/s~Lf77

\/<£:g f Shif

t

## 2> V

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## \kJ[S£LK/

: Scal e zeroe d y^£ ^ 

## [liill l

iWflitBffilllimfu] 

## ISiili!

IHIlPS ) WEIGHT'<LBS) ..'I'B A' G WEIGHT\LB: ! 160 1 

# 3 LB? 1626 

# 3 LBS 165 1 

# 3 LVf 1676 3 LIZ? 160 2 ^ 1627 , 

# 3 LB? 1652 

# 3 LB? 1677 

# 3 LBS 160 3 

## 3> LVS 162 8 

## $>LBS 1653 

# 3 LBS 1678 

## - s 

# 3 LBS 160 4 

## 3 LB? 1629 

# 3 LBS 1654 

## 3 h-br 1679 

# 3 LB? 160 5 

# 3 LB? 163 0 

### 3 LB>? 1655 

# 3 LB? 1680 , 

# 3 LBS 160 6 

### 3 LB>^ 163 1 

## 3 LBS 1656 

### 3 LB< 168 1 

# 3 L&? 160 7 

# 3 LB? 163 2 

# 3 LBS 1657 , 

# 3 LBS 168 2 

### 3 LB<T 160 8 

# 3 LB? 163 3 

## 3 LBS 1658 

# 3 LBS 1683 , 

### 3 LB<T 160 9 

# 3 LP? 163 4 

# 3 LBS 165 9 

# 3 LBf 168 4 

# 3 LBS 161 0 

# 3 LPS 163 5 

### 3 L&? 1660 

## 3

LB? 1685 

## 3 >L &f 161 1 

# 3 LP? 163 6 

# 3 LBf 166 1 

# 3 LBf 1686 

## 3LBf 161 2 

## 3 LP? 163

7 

# 3 LBf 166 2 

# 3 us>. r 1687 

# 3 LBS 161 3

. 

### 3 LB? 1638 

# 3 LB? 1663 

### 3 LB< 1688 

# 3m< 161 4 3 LB<T 1639 

### o ' K. *5 

## LBS 166

4 

# 3 LBf 1689 

# 3 LBS 151 5 < 

# 3 LB< 1640 

### 3 L&? 1665 

### 3 LP><: 1690 

# 3^r 151 6 

## 3 LB? 164 1 

## 3i^f 166 6 

### 3 LB< 169 1 151 7 

### 3 LP>? 164 2 166 7 

# 3 LP< 1692 

# 3 LBf 151 8 

# 3 LB? 164 3 

# 3 LB? 166 8 

### / 3 A B T 1693 — * >



## 2? LBS 1S1 9

. 

# 3 LBS 164 4 

# 3 LB? 166 9 

# 3 LB? 1694 

## 3 iter 1S2 0 

# 3 LBS 164 5 3-L9S 167 0 

# 3 LBf 1695 

### 3 LU?- 1S2 1 

# 3 LB? 1646 

# 3 LBS 167 1 1696 

### 3 LBS 152 2 

# 3 LB? 1647 

## P)

LR>< 167

2 

## 3 LBS 1697 

# 3 LBS 1S2 3 

# 3 LB? 164 8 

# 3 LBS 167 3 , 

# 1s$>s

1698 

## Sn ' 3 L&<? 152 4 

# 3 LBf 1649 

# 3 i&r 167 4 

## 3 >LB,f 169 9 

# 3ds 152 5 

# 3 LBS 1650 

# 3 LB? 167 5 

## 3 m 1700 

# 3 L^S1 V

HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s Cre wPersonne l D >HM



## AMflhffctf. T,T>£>\{£:& } 

## y wis^iy shif t /s rJ P Scal e zeroe d 

## H i 

# mam iiiiiii i Iiiiiii i lllllllli

HNM H BA G rf ftBWT.LRB, 170 1 1726 

## 3 A&< 175 1 

# 3$ LB? 1776

. 

## ^>Ln? 170 2 

# 3 /-B I T 1727 

# 3 LB? 1752 

### 3 L&? 1777 

# 3 LB? 1703 1728

. 

## 3 IBS 1753 

# 3 LBS 1778 

# 3 IB S 170 4 

# 3 /.s- r 1729 

# 3 LB? 175 4 

### 3 L&>? 1779 3 ^ B S 170 5 3 2

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0 

# 3 LB? 1755 

# 3 LBf 1780 

## i %LBs~ 170 6 

# 3 UQf 173 1 

# 3 LB? 1756 

# 3 LBS 178 1 t 

## 3 >LB<- 170 7 

# 3 i*r 173 2 

# 3 LBS 1757 

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## 3uB?r 170 8 

### 3 L®4 1733 • 

# 3 LBS 1758 

# 3 LB? 1783 

### 3 LT*,< 1709 

# 3 i&s 173 4 3 L B ? 175 9 • 

# 3 LB,? 1784 3 LP )<S 171 0 

# 3 L.&S 173 5 

# 3 LBS •1760 

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## 3 LB? 171 1 

# 3 173 6

. 3 L&? 176 1 , 

# 3 LBS 1786 , 171 2 1737 

### 3 LB?? 1762 ( 

### 3 >L&S 1787 —— 1 ' / 

### 3 LBS_ 171 3 

### 3 L B ? 173 8 E — ' > 

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# 3 i-m<

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# 3 LB? 1769 

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# 3 LBS 1746 

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## n LBS 1796 , 

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# 3 LBf 174 7 

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## 3

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### VES01893 2HEXACHLOROETHAN E SPIK E BAG S - Target Weight : 3. 0 pound s



## CrewPersonnelT^^A//4l^A/ ^ T > $X>V£% F Date

# U'M'Cfj Shif t /%T ~ TS> Scal e zeroe d 

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# Iiilii i HHHH Riimiif ! iiiHil l 180 1 3 LUS 182 6 , 

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# 3 LBS 180 5 

# 3ip r 1830 185 5 , 

## 3 LBS 1880 3 LB? 180 6 

## 3}L&? 183 1 3 L3< 1856 

## 3 LB-? 188 1 

# 3 Lbs 180 7 183 2 

## 3 LB? 1857 

## 3 LB? 188

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# 3 LB< 181 0 183 5 , 

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# 3 LBS 181 1 < ^>LB? 1836 < 

## 3 LB? 186 1 

## 3 LB? 1886 3 ISBS 181 2 r 3 L&? 1837 

## t 3 £9? 186

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## 3

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# - 3 /.s< - 184 1 

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6 <^LB* 189 1 

## 3b LB? 181 7 r- 184 2 

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## 3 LB? 187 1 

## 3*&r 1896 3 L&S 1822 

## 3i&c 1847 

## 3 LB? 187

2 3 LBT 1897 3 LB<T 1823 — — ~ ^ — 

## 3 L&S 1848 3 LB< 187 3 

## 3 LB? 1898 182 4 3 L$> C 1849 

## 3 LB? 187

4 3 LB< 1899 1825 1850 < 

# 3 LBS 187 5 

### 3^B? 1900 3 LB>S~



### VES01893 3HEXACHLOROETHAN E SPIK E BAG S - Targe t Weight : 3. 0 pound s Cre wPersonne l 

# J^'HAl AVW(<~M l~H V^V^, Date/^c ^ f Shif t JL> Scal e zeroe d IIIIII I IIIIII I 

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## 3 LB*? 1927 r ^LB? 195 2 3 LBS 197 7 

## 3 LBS 190 3 

## 3 LB? 1928 

## 3 LBS 1953 3 L&<? 197 8 

## 3 LB? 190 4 

## 3 LB? 1929 3 L&? 195 4 

## 2>L&r 197 9 

## 3 LBS 190 5 

## 3 LB? 193

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## 3 LBS 1955 

## 3ms 198 0 

## 3 LBS 190 6 

## 3 L&? 193 1 

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## 3 LBS 193

2 3 LB^ 1957 

## 3>LB? 198 2 

## 3 LpS 190 8 

## 3 LBf 193

3 3 LB<S 1958 3 LTK 198 3 

## 3 LBS 190 9 

## 3iv><? 193 4 3 LB? 1959 , 

## ^LBS 198 4 3 LB<; 191 0 

## 3

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## 3isp>?' 191 4 

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## 3 LB? 1966 

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## 3h>m<-. 191 7 

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## 3>L^?' 191 8 3 LBS 194 3 

## 3 LBS 1968 

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## 3 LBf 192 1 3 LBS 1946 3 L&S 197 1 

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### VES01895 1

### Wast e Fee d Profile s

VES01895 2Report ! R 7 00 B DATE : 11/30/O S ONY XENVIRONMENTA

L SERVICES , LL C WASTE PROFIL E SUMMAR Y
BUSINESS : ASCHE RDANIEL S MIDLAND , C0 - DEP T i ADDRES S 1 : VITAMI N E PLAN T ADDRES S 2 : 37O0 E . DIVISIO N STREE T -Y/ST . . : BSCATU

R 'ACT . . : DAVI D BROADHACKE R I L 6252 6

WAST E NAME : SOLVENT RECOVER Y PROCES S GENERATIN GWASTE ; SOLVENT RECOVER Y SKIP . NAME : WAST E FLAMMABL E LIQUIDS , N.O. S ADDL . DESC : (ACETONE , METHANOL ) Versio n06.0 4 TWI-02869 1 SELLINGREGION

LA B - MRL NUMBE R: 142-B-78 9 PHON E : 217/451-439 2 EXPIRE S 01/11/1 1 STATU S : APP RFO RSER V FEDERA L EP A

ID : ILE00002155 0 STAT E EP A

ID.. : 115015534 6 EPA STATU S CH E RESTRIC T SALES OFFICE . . i

RPK

CHEMICA

L COMPOSITIO

N

NON-TR I CHEMICAL S EMULSIFIE DOI L UNI T DESCRIPTION ACETON E 2 5 3 5 % HEPTAN E 2 5 3 5 % METHY L ALCOHO

L 2 5 3 5 % WATER 1 3 8 % BENZEN E 1 3 8 PP M
1 5 2 5 %
EP TOX/TCL P PHYSICAL CHARACTERISTIC S Physica l State... : Liqui d Flash . Poin t : > = 20 0 C L p H : 04. 0 - 09. 0 Colo r : VARIE S Odo r : NON E Layer s ..... : Singl e Laye r Specifi c Gravity. : 0.95 0 - 1.15 0 Fre e Liquid s : 9 9 - 10 0 Cyanide s ... : < 5 PP M TOTAL Sulfide s < 3 PP M TOTAL PCB' s ppm . Regulate db y 4 0 CF R761 : Phenolic s : < 1 0 PP M % Taxable ' : DO T UN/N

A NBR : UN199 3 Treatmen t Codes.. : T0 7 CR Q RP T QTY: Materia l Class : EPA Permi t EXP : Hazar dClass..... : 3 Stat e Code s : 09000 1 Benzen e : 3 8 NESHAP ; Controlle dBenzen e NESHAP Packin g Group . . . . : I I " Proces s Codes.... : CBC Cer t o f Dstrc t R<j :

Federa l Codes : DOO l D01 8 F00 3

NEO . GREYGLOVE S TYP E C RESPI S CONS T PLO W HANDLIN G N-DE XINNE RGLOV E

INDEX/BLU E NirRIL E (INNERGLOVE ) BENZEN E NESHA

P CONTROL S REQUIRED ; N O CER T CANCE RSUSPEC T AGENT : BENZENE '

Inhalation : 2 Dermal : 2 DO T PROPERTIE S Oral : 2 Flammable : 0 Health : 0

Wast e Typ e For m Cod e B21 S 1

CHARG E CODE : N S BENZEN E NESHA

P CONTROL S REQUIRED ; N O CER T COMMENT S REVIEWE D FORMACT METAL S



### VES01895 3'Report ! R700 B DATE ! 09/15/0 9 ONY XENVIRONMENTA

L SERVICES , LL C WAST E PROFIL E SUMMAR Y
BUSINESS : DEP T ADDRES S 1 : ADDRES S 2 : ^tY/ST . . : ACT . . ! C0WOC

O PHILLIP S COMPAN Y WOO D RIVE RREFINER Y 90 0 SOUT H CENTRAL AVENUE
ROXAN A I L TON YSHA N
WAST E NAME : PRIMAR YSOLID S DEBRI S PROCES S GENERATIN GWASTE : PROCES S SEWE RCLEANIN

G SHIP . NAME : HAZARDOU S WASTE , SOLID , N.O. S ADDL . DESC : RQ(F037 , F03B ) Versio n06.0 4 TKI-33046 9 SELLINGREGIO

N LA B NUMBE R: 143-4-77 1 PHON E 61 8 25 5 237 4 EXPIRE S : 04/29/1 1 STATU S APP RFO RSER V FEDERAL EPA

ID : ILRO0O07711 5 STAT E EP A

ID.. : 119090501 3 EPA STATU S : CH

KRESTRIC T SALE S OFFICE.. : TW I

CHEMICA

L COMPOSITIO

N CALCIU M CARBONAT E WATE R PETROLEU

M HYDROCARBONS NON-TR I CHEMICAL S COMBUSTABL E SOLID S SAPER/PLASTI C INER T SOLID S SOIL/ROC KET C MI N - MA

X 0 0 0 0 6 9 UNI T DESCRIPTIO N

1 0 % 1 0 % 2 %
2 5 % 9 9 %
METAL S Arseni c as . As Cadmiu m a s C d Lea da s P b Mercur y

a s H g Seleniu m

a s S e Chromiu

m He x Nicke l a s N i Thalliu m

a s 7 1 E P TOX/TCL P mg/ l mg/ l mg/ l mg/ l mg/ l PHYSICAL CHARACTERISTIC S Physica l State... : Soli d Flas hPoin t : > = 20 0 C L p H 04. 0 - 09. 0 Color . : BLACK/VARIE S Odo r : NON E Layer s : Singl e Laye r Specifi c Gravity. : 0.00 0 Fre e Liquid s : 0 - 1 Cyanide s : < 5 PP M TOTAL Sulfide s : < 3 PP M TOTAL PCB' s : ppm . Regulate db y 4 0 CFR761 : Phenolic s : < 1 0 PP H % Taxabl e : DO T UN/N

A NBR : NA307 7 Treatmen t Codes.. : T0 7 CR Q RP T QTY: 1 Materia l Class ; EP A Permi t . : EXP : Hazar dClas s : 9 Stat e Code s i 09000 1 Benzen e .. : > 1 0 NESHAP : Controlle dBenzen e NESHAP Packin g Group.... : II I Proces s Codes.... : BS H Cer t o f Dstrc t Rq :

Federa l Codes : F03 7 F03 8

HANDLIN G NEO . GREYGLOVE S N-DE XINNERGLOV

E SARANEX Contain s Benzen e TYP E C RESPI RCONS T FLO W INDEX/BLU E NITRIL E (INNE RGLOVE ) BENZEN E NESHA

P CONTROL S REQUIRED ; CERT REQUIRE D WIT H EVERYLOA

D D O NOT AD

DT O TAB , DOE S NO T CONTAI N >10 % WATE

R+

POT PROPERTIE S Inhalation : 2 Dermal : 2 Oral : 2 Flammable : 0 Health : 0

SUMMAR Y Wast e Typ e B40 9 For m Cod e 1
COMMENT S CHARG E CODE : N S REACTIV E CATEGORY : B--CONTAIN S MERCUR Y REVIEWE D FO

RMAC T METAL S BENZEN E NESHAP CONTROL S REQUIRED ; CER T WITH EVERY LOAD . D O NOT AD

DTO TAB , DOE S NOT CONTAI N >10 % WATE

R NEED WEIGH T P E UNTI L 12-31-0 9 PRIC E INCREAS E EF F 1/22/0 9 ON E TIM E LD

RNOTIFICATIO N

RECD FO

RF03 7 10/27/0 6 GENERATO RLD RFOR M I N T M FIL E 1/18/0 7



### VES01895 4Report : R 7 00 8 DATE : 11/24/O S ONY XENVIRONMENTAI i SERVICES , WAST E PROFIL E SUMMAR Y
BUSINESS : DEP T ADDRES S 1 ADDRES S 2 "••"T.Y/ST . _ \CT . . IMPERIAL CLEANER S

221 0 WISCONSI N

AVE
NE W KOLSTEI N Km WALKER WAST E NAME : TETRACHLOROETHYLEN E CONTAMINA T EDSOI L PROCES S GENERATIN GWASTE : CLEANUP O F TETRACHLOROETHYLENE SOI L FRO M DR YCLEA N SHIP . NAME : HAZARDOU S WASTE , SOLID , N.O. S ADDL . DESC : R.Q{TETRACHLOROETHYLENE ) VerBio n06.0 4 TWI-09611 0 SELLIN GREGION

LA B - MR L NUMBE R: 144-0-05 9 PHON E 920/B98-480 0 EXPIRE S 10/01/1 1 STATU S : APPRFO RSER V FEDERAL EPA

ID : WID9B154004 0 STAT E EPA

ID.. : 955001999 9 EP A STATU S CH

KRESTRIC T SALE S OFFICE.. : CS K

CHEMICA

L COMPOSITIO

N TETRACHLOROETHYLEN E SOI L NON-TR I CHEMICAL S PAPER , PLASTIC , » - MA XUNI T DESCRIPTION 0 1000 0 PP

M 9 5 10 0 % 0 5 %
EP TOX/TCL P PHYSICAL CHARACTERISTIC S Physica l State... ; Soli d Flas hPoin t ; > = 20 0 C L p H 05. 0 - 10. 0 Colo r : BROW N Odo r : NON E Layer s Singl e Laye r Specifi c Gravity. : 0.00 0 Fre e Liquid s : 0 Cyanide s : < 5 PP M TOTAL Sulfide s : < 3

PP M TOTA L PCB' s : ppm . Regulate db y 4 0 CFR7 61 : Phenolics , : < 1 0 PP M % Taxabl e : DOT UN/N A NBR : NA307 7 Treatmen t Codes.. : T0 7 CR Q RP T QT

Y: 10 0 Materia l Class ; EP A Permi t : EXP : Hazar dClas s 9 Stat e Code s : 09000 1 Benzen e : . NESHAP : Packin g Grou pIl l Proces s Codes.... : BS L Cer t o f Dstrc t Rq :

Federa l Codea s F00 2

HANDLIN G NEO . GREYGLOVE S N-DE XINNE RGLOV E SARANEX TYP E C RESPI RCONS T FLO W INDEX/BLU E NITRIL E (INNE RGLOVE ) kappler s che

m tap e 2

Inhalation : 2 DO T PROPERTIE S Oral : 2 Flammable : 0 Health : 0

Wast e Typ e For m Cod e B30 1 1

CHARGE CODE : NS P E EVENT EXPIRE S 12-31-0 9 COMMENT S REVIEWE DFO

RMAC T METAL S



### VES01895 5Report ! R 7 0 0 8 DATE i 11/21/0 9

BAS F CORP

. .HANNIBA

L PLAN T 31 5 0 HW

YJ J ONY XENVIRONMENTA

L SERVICES , LL C WAST E PROFIL E SUMMAR Y

M O S 3 4 E l BUSINESS : DEP T : ADDRES S 1 : ADDRES S 2 l ''.Y/ST . . i \CT.. :
WAST E NAME : IMI- 2 HERBICID E ORGANI C WAST E SPIL L CLEANU P PROCES S GENERATIN GWASTE : ORGANI C WASTE SPIL L CLEANUP SHIP . NAME : HAZARDOUS WASTE , SOLID , N.O. S ADDL , DESC : (TOLUENE , METHANOL ) Versio n0 6.0 4 TWI-097B0 2 SELLIN GREGION

LA B NUMBER , 105-7-00 2 PHON E EXPIRE S 10/27/1 1 STATU S : APPRFO RSER V FEDERAL EPA

ID : MOD05022607 5 STAT E EPA

ID.. : 929001999 9 EP A STATUS..,. : CH

KRESTRIC T SALE S OFFICE.. : RP K

CHEMICA

L COMPOSITIO

N METHANOL TETRAHYDROFUSA

N TOLUEN E WATER NON-TR I CHEMICAL S SOI L AN

DGRAVE L SPIL L CLEAN-UP DEBRI S HERBICID E BY-PRODUCT S 0 0

. 1 0 9 5 0 0 UNI T DESCRIPTION

. 1 %

. 1 % 2 % 1 % 9 9 % 1 %

. 1 %
E P TOX/TCL P PHYSICA L CHARACTERISTIC S Physical'State... : Soli d Flas hPoin t : N/ A C L pH : 04. 0 - 09. 0 Colo r : BROW N Odo r : NON E Layer s : Singl e Laye r Specifi c Gravity. : 0.00 0 Fre e Liquid s : 0 Cyanide s : < 5 PP M TOTA L Sulfide s : < 3 PP M TOTAL PCB' s : ppm . Regulate db y 4 0 CFR761 : Phenolic s : < 1 0 PP M % Taxabl e : DO T UN/N A NBR : NA307 7 Treatmen t Codes.. : T0 7 CR Q RP T QT

Y: Materia l Class : EPA Permi t : EXP : Hazar dClas s : 9 Stat e Code s : 09000 1 Benzen e : NESHAP : Packin g Grou pIl l Proces s Codes.... : BS L Cer t o f Dstrc t Rg : Y

Federa l Codes z

DOO l F00 3 F00 5

NEO . GRE YGLOVE S TYP E C RESPI RCONS T FLO W HANDLIN G N-DE XINNE RGLOV E

INDEX/BLU E NITRIL E (INNE RGLOVE )

Inhalation : 2 Dermal : 2 DO T PROPERTIE S Oral : 2 Flammable : 0 Health : 0

Wast e Typ e For m Code . B30 1 1

CHARG E CODE : NS P E 10-28-1 0 COMMENT S REVIEWE D FO

RMAC T METAL S REPOR T WEIGH T



### VES01895 6Report : R700 8 DATE : 11/30/O S ONY XENVIRONMENTA

L SERVICES , WAST E PROFIL E SUMMAR Y
VEOLI A E S TECHNICAL SOLUTION S
7 MOBIL E AV E BUSINESS : DEP T ADDRES S 1 ADDRES S 2 "TTY/ST. . •ACT . . WAST E NAME : ON-SIT E RAINWATER£ AS H WATE R PROCES S GENERATIN GWASTE : COLLECTION O F ON-SIT E STORMWATE R& PRECIPITATION ; SHIP . NAME : HAZARDOU S WASTE , LIQUID , N.O. S ADDL . DESC : Versio n06.0 4 TWI-TW2S1 9 SELLIN GREGIO N

LA B NUMBE R: 110-9-72 2 PHON E : EXPIRE S : 11/30/1 4 STATU S : CONTRAC T NO T I N PLAC E FEDERAL EPA

ID : ILD09864242 4 STAT E EP A

ID.. : 163121000 9 EPA STATUS.... : CH

KRESTRIC T SALES OFFICE.. : RP K ATE R

CHEMICA

L COMPOSITIO

N WATE R NON-TR I CHEMICAL S ASHWATE

R MIS C SOLIDS , WAST E RESIDUE S MI N - MA

XUNI T DESCRIPTIO N 9 9 10 0 %

S O % 1 %
METAL S EP TOX/TCL P Arseni c a s As Cadmiu m as . C d Lea da s P b Mercur y

a s H g Seleniu m

a s S e Chromium

He x Nicke l a s N i Thalliu m

a s T l mg/ l mg/ l mg/ l mg/ l mg/ l PHYSICAL CHARACTERISTIC S Physica l State... : Liqui d Flas hPoin t : > = 20 0 C L p H : 02 . 0 - 12. 5 Colo r : VARIE S Odo r : NON E Layer s : Singl e Laye r Specifi c Gravity. : 0.95 0 - 1.15 0 Fre e Liquid s : S 3 - 10 0 Cyanide s : < : 5 Sulfide s . : < 3 PCB' s : ppm , Regulate db y Phenolic s '. : < 1 0 % Taxabl e DOT UN/N A NBR : NA308 2 Treatmen t Codes.. : T0 7 CR Q RP T QT

YMateria l Class : EP A Permi t : EXP : Hazar dClass..... : 9 Stat e Code s 09000 1 Benzen e : NESHAP : Packin g Grou p: II I Proces s Codes . . . . : Cer t o f Dstrc t Rq : PP M TOTAL PP M TOTA L 4 0 CFR761 : PP M

Federa l Codes : D00 3 D00 7 D00 8 D00 4 D00 5 D00 6 D00 9 DOl O D01 1 D01 2 D01 3 D01 4 D01 5 D01 6 D01 7 D01 8 +

SIT E GENERATED WAST E

DO T PROPERTIE S Inhalation : 0 Dermal : 0 Oral : 0 Flammable : 0

TW I Signe dAddendu m

SIT E GENERATED



### VES01895 7TW I Laborator yAnalysi s Repor t Receive r# : TK30 4 Visua l Inspection : Glov e Bo x/ Hoode d Feeder # o fDrums : 1 Date: 6/29/200

1 Profil e #:ZZZZZ

Z Generator

: TRAD E WAST E INCINERATION Descript: Proces s Code(s) :

Dru m Storage Compatibilit y Profile d DO THazar d Clas s 9 P = Pass F-Fait 8 A 8 B 4/

5 Sampl e Numbe r Dru m Re p / Com p 303022_[_IL0000000 1

1 / ~ 1 

# IIIIIII I 30302 2 Fre e Liqui d (% ) 

# IIIIIII I 30302 2 Profil e Confor

m Dat e Initial

s Pumpabl e N

O 

# IIIIIII I 30302 2 

# wwww v Ye s N o 11/06/0 9 MI Layers/Phase

s - % Ea . 

# \\\\\\\\\ ^ Color Turbidit y 

# wwww v Viscosit y L X Physical Stat

e 

# ^\\ \ Wate rMiscibilit y Add . Descriptio

n Wate rReactivit y Radiatio n Scree n =BK G X Flam . Po t Screen Se e Flashpoin

t X p H Scree n 5 a

t 10 0 pen t 2-12.5 X Oxidize rScreen Pain t Filte rTes t 

# ^\\\ Cyanid e Screen 

# wwww v 

# ^\\\ Sulfid e Scree n 

# wwww v Incidenta l Odor 

# wwww v ^ Specific Gravit

y 1.01 11/04/0 9 M I BTU/Lb 157

0 11/04/0 9 B D % Chlorid e 1.

2 11/04/0 9 K D Flas h Poin

t - De g F 01/01/0 0 PCB s ByG C - mg/k

g <50pp m 11/06/0 9 p H b yMete r 01/01/0 0 Arsenic mg/k

g 4.76

8 0 Beryllium mg/k

g 4.76

5 0 Cadmiu m mg/k g - 4.76

5 0 Chromium mg/k

g 4.80

5 0 Lea d mg/k g 4.78

4 0 Mercur ymg/k g 0.05

6 0

Profil e Revie wforAppendi

xWAP- C Consitituent

s by : Date : Add . Comments : The dat a i n th e sampl e informatio

n section(6/29/2001)is dat e profil e 777777

wa s created .



### VES01895 8

### Wast e Trackin g Syste m Fil e Inventor yPrin t Approval s Chemis t Receivin g Laborator yTan k Far m Proces s Plannin g Windo wBillin g Hel p 

### I ? * Laborator

y Sampl e Analysi s -Sampl e Number
030.2 2 Updat e Cance

l j -Edi t Mod e Updat e an d Submi t t o La b Manage r J Exi t f Approva l Statu s 

# I

# 3

Manifes t IL0O0D0O0 1 Sampl

e Statu s L Vie wProfil e Summar y Comment s Vie

wPD W
Cance l Submi

t •Sampl

e Statu s Codes
ReSampl e = S <

v PC B suspec t = P lnLaboratoi y= L Metal s = E 5 . Pendin g La b Manage rApprova l = M Discrepan t = D ^ Rejecte d = R Conforms/Accepte

d = AJ

£ Layers/Phase s iTeits ! p Wate rReactivit y rN o RX N TRXN: I Radiatio n Scree n T=BK G r >BKG

: •Flam

. Po t Scree n f ~ Ne g rPo s rBO C •p H Screen
Valu e p p

100 ^ j = 10 £ rOxidize rScree n - rNe g rPo

s j Specifi

cGravit y i BTU/l b I I % Chlorid e : Flas h Poin t (Deg

. F ) PCB s b vG C (mg/kg ) PC B G C Commen t PCBs-Scree n (ppm ) Valu e jl.0 1 jl57 0 1. 2 Dat e jl1/4/200 9 |11/4/200 9 j i 1/4/200 9 Initial s |M T [BD ° 

# w J1/1/190 0 1V1/190 Q 

# " 3 jl/1/190 0 rPain t Filte rTes t rPas s TFai l V V-Fa S V N/ A
•Cyanid e Scree n f ~ Neg P Posj

TM N/ AT Cyantesm o •Sulfid e Scree n rNe g rPo

s TN/ A 2, 4 S - T(ppm ) Silve x(ppm ) • j1/1/19D 0 PC P Scree n (ppm ) p H b yMete r PU TrE C jl/1/190 0 

# r IOO X r

## i(Ki/i /i9o o rMetals
P ° S4.78 4 A s (4.76 8

Adjus t Metal s

•Incidenta l Odo r rN o 

# r Yes

: rAshfc
212 3



### VES01895 9TW I Laborator yAnalysi s Repor t Receive r# : TK31 0 Visua l Inspection : Glov e Bo x/ Hoode d Feede r # o fDrums : 1 Date : 6/29/200

1 Profile # : 777777 Generato rTRAD E WAST E INCINERATIO N Descrip t Proces s Code(s) :

Dru m Storage Compatabilit y Profile d DO THazar d Clas s 9 P = Pass F = Fail SA 8

B 4/

5 Sampl e Numbe r Dru m Re p / Com p 301556 1 ILOOOOOOOl

1 / 

## m i n 30155 6 Fre e Liqui d (% ) 

## m i n 30155 6 Profil e Confor

m Dat e Initial

s Pumpabl e N

O 

## m i n 30155 6 \\\\\\\ W Ye s N o 10/01/0 9 S L Layers/Phase

s -% Ea . \\\\\\\ W Color .xWWW W Turbidit y Viscosit y L X Physical Stat

e 

# wwww v WaterMiscibilit

y 

# \\\\\\\ w Add . Descriptio

n WaterReactivit

y 

# w w w \W\ N Radiatio n Screen =BK G X Flam . Pot

. Screen Se e Flashpoin

t X pH Screen 3 a

t 10 0 pen t 2-12. 5 X Oxidize rScree n \\\\\\\ W Pain t Filte rTes t \\\\\\\ W Cyanid e Scree n 

# wwww v Sulfide Scree

n 

## \\\\\\\\\ > Incidenta l Odor Specifi c Gravit

y 0.8

3 10/01/0 9 S L BTUTL b 960

0 10/01/0 9 M T % Chlorid

e <0.

5 10/01/0 9 J F Flas h Poin

t - De g F 01/01/0 0 PCB s B yG C - mg/k

g <50pp m 10/01/0 9 p H b yMete r 01/01/0 0 Arseni c mg/k

g 0 0 Beryllium mg/k

g 0 0 Cadmium mg/k

g 0 0 Chromium mg/k

g 0 0 Lea d mg/k g 0 0 Mercur yrng/k g 0 0

Profile Revie

wforAppendi

xWAP- C Consitituent

s by: Date : Add . Comments : Th

e dat a i n th e sample informatio

n section(6/29/2001)is dat e profil e 777777

wa s created .



### VES01896 01 5 » Wast e Trackin g Syste m Wi'KCSfe.^ ^ Fi e InventoryPrin t Approval s Chemist Receivin g Laborator yTan k

Far m Proces s Plannin g Windo wBi l }in g Hel p 

### « * I uborufpr

y Sdmpl e Analysi s J?-Sampl e Number R=tiie w Updat e Cane d

r EditMod B Updat e an d

Submit t o La b Manage r
Manifes t IL0000000 1 Sampl e Statu s W •Approval — Statu s Vie wProfil e

Summar y
Comment

s ViewPD W

Cance l Submi t •Sampl e Statu s Codes ReSample= S PCBsuspec t = P I n Laborator

y= L Metal s » E Pendin g La b Manage rApprova l = M Discrepan t = D Rejecte d = R Conforms/Accepte d » A

_ Layers/Phase s •Testa ; j - Wate rReactivity 

# r N o RX N 

# r RXN : 

# j = Radiatio n Screen -

T =BK

G T >BKG : •Flam . Po L Scree n 

# P Ne g

# P Po s 

# r BO C •p H Screen Valu e I 5 1 7

# 1005 ! r 10 * •Oxidize rScreen - TNe g TPo s rPain t Hlte rTes t —
P Pas s r Fai l P V-Fai l | ~ N/ A •Cyanid e Scree n
P Negl " Po s P N/ A P Cyantesm o -Sulfid e Screen 

# r Ne g

# T Po s 

# r N/ A rIncidenta l Odor- —— 

# T N o

# P Yes : 

# JValu e

Specifi c Gravit

y BTU/l b % Chlorid e Flas h Poin t peg . F ] PCB s b yG C (mg/kg ) PC B B C Commen

t PCBs-Scree n (ppm

] 0.8 5 961 0 <0.50 Date Initial s 111 /15/200

3 |M T |11/15/2C0 3 (M

T ' 111/15/200 9 1M

T (1/1/190 0 11/1/130 0 

## " 3 1/1/190 0 2.4,5- T(ppm

) Silve x(ppm ) 1/1/190 0

PC P Scree n fppm

j p H b yMel a P KITP G C |1/1/1S0 D
P 100X P KK|1/1/1S0 0 rMetals — A s fg "
B e

## jo " Cdj a

D jb "

K

## Jo " Naj T

Adjus t Metal s

•AshX 

### VES01896 1

### C M S Performanc e Evaluatio n

VES01896 2

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON ; SERVICE : LOCATION : LP-SHT : P&ID : UNI T #4 QUARTERL

Y P T 30 0 PRES S TRANS

M KIL N HOO D FTRNS P 30 0 F01 5 MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : REMARKS : Rerange d1/19/9 6 PROCESS-SP : INSTL-RMKS : 1/2" x29 " S S PIP E insid e Kil nINST-SP : SPEC-RMKS : ACTION : S/N : I/ O NUMBER : CALIBRATIO

N NOTE S ROSEMON T 1151DR2 F -9.0 " T O 1.0 " W

C 4-2 0 m a Atmospher e = 18.4 0 m a Se t Dampenin

g po t ful l C

W Nl:2 5

US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

RAN D LOO P CALIBRATOR . INPU

T PNEUMATI C SIGNA

L AN D REA D OUTPU

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Se e Manufacture s literatur e fo r detaile dinstructions . Fil l ou t andaffi xa ne w calibratio nsticker . 0. 1 lb/h r CALIBRATIO N REPOR

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G Before Calibration./ „ , A

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### CALIBRATIO

N SOURC E REFERENCE

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Performe dby: . _Date : V-P. -0 ? Time:/ ^ J B Place : CALSHEET.WD

B (Field or Shop) 

### _A

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VES01896 3

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T # 4 QUARTERL

Y P T 32 4 PRES S TRANS

M SC C OUTLET FLD 32 4 F01 5 MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : CALIBRATIO

N NOTE S ROSEMON T 1151GP3 E -15 " T O +5 " 4-2 0 MAD

C W C

US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

RAN D LOO P CALIBRATOR . INPU

T PNEUMATI C SIGNA L AN D REA D OUTPU

T WIT H LOO P CALIBRATOR .

Se e Manufacture s literatur e fo r detaile dinstructions . Fil l ou t andaffi xa ne w calibratio nsticker . 0. 1 lb/h r CALIBRATIO N REPOR

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# o 3 

# 3 n ~o 3 

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N SOURC E REFERENCE

Comments :

Performe dby : 

# /^QCC/tt Jfjf ^ Date : 

## #~/^-

0 9 Time:/- * :/ 0 J B Place : CALSHEET.WD

B (Field or Shop) 

### P

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VES01896 4

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T #4 QUARTERL

Y PD T 43 9 D P TRAN S BAGHOUSE PRESSUE

R WAP C 43 7 F01 7 W/GA S CLEANIN

GTRAI N NORTH/EAS T BAGHOUSE MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : FOXBOR O 82 3 DP I 0-15 " W C 4-2 0 MAD

C

CALIBRATIO

N NOTE S US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

RAN D LOO P CALIBRATOR . INPU T PNEUMATI C SIGNA L AN D REA D OUTPU

T WIT H LOO P CALIBRATOR .

Se e Manufacture s literatur e fo r detaile dinstructions . Fil l ou t andaffi xa ne w calibratio nsticker . 0. 1 lb/h r CALIBRATIO N REPOR

T INPU T VALU E INSTRUMEN T READIN

G

. Before Calibration

. rf 

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### CALIBRATIO

N SOURC E REFERENCE

Comments :

Performe dby : (VX- fci'k*, 

### Date :/7- fl-d f 

### Time :^2 < nAPpP M J B Place : CALSHEET.WD

B (Field o r Shop)

VES01896 5

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T #4 QUARTERL

Y PD T 44 0 D P TRAN S MANUFACT : FOXBOR O BAGHOUSE PRESSUE

RMODEL : 82 3 DP I WAP C 43 7 F01 7 W/GA S CLEANIN

GTRAI N NORTH/CENTRA

L BAGHOUSE MANUFAC T MODE L SCALE CALIB-I N CALIB-OU

T PROCESS-S P INST-S P ACTIO N I/ O NUMBE

R 0 - 4 - 15 " W C 2 0 MAD C

CALIBRATIO

N NOTE S US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

RAN D LOO P CALIBRATOR . INPU

T PNEUMATI C SIGNA L AN D REA D OUTPU

T WIT H LOO P CALIBRATOR .

Se e Manufacture s literatur e fo r detaile dinstructions . Fil l ou t andaffi xa ne w calibratio nsticker . 0. 1 lb/h r CALIBRATIO N REPOR

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G Before Calibration

~^

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### CALIBRATIO

N SOURC E REFERENCE

Comments :

Performe dby : 

# /^j' 1 

# ^1 

### Date : Time : J B Place : CALSHEET.WD

B (Field or Shop) 

### P

M

VES01896 6

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRUMEN

T CALIBRATIO

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GTRAI N NORTH/WES

T BAGHOUS E MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : FOXBOR O 82 3 DP I 0-15 " W C 4-2 0 MAD

C

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N NOTE S US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

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T WIT H LOO P CALIBRATOR .

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### CALIBRATIO

N SOURC E REFERENCE

Comments :

Performe dby : //^ / rr' Date : // ~0 

### 1 Time : ^-CTO J B Place:
_ CALSHEET.WD

B (Field or Shop) 

### P

M

VES01896 7

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRDMEN

T CALIBRATIO

N RECOR D UNI T # 4 QUARTERL

Y PD T 44 2 D P TRAN S BAGHOUSE PRESSUE

R WAP C 43 7 F01 7 W/GA S CLEANIN

GTRAI N SOUTH/EAS T BAGHOUSE MANUFAC T MODE L SCALE CALIB-I N CALIB-OU

T PROCESS-S P INST-S P ACTIO N I/ O NUMBE

R FOXBOR

O 82 3 DP I 0-15 " W C 4-2 0 MAD

C

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N NOTE S US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

RAN D LOO P CALIBRATOR . INPU

T PNEUMATI C SIGNA

L AN D REA D OUTPU

T WIT H LOO P CALIBRATOR .

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I INSTRUMEN

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N RECOR D UNI T #4 QUARTERL

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[d m Date : / I



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### VES01896 9

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T # 4 QUARTERL

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C

CALIBRATIO

N NOTE S US E PNEUMATI C CALIBRATIO N BENC H WIT H MANOMETE

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### VES01897 0

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRDMEN

T CALIBRATIO

N RECOR D UNI T #4 QUARTERL

Y WIT 00 1 W T TRAN S SHREDDE

D SOLID S FTRNS P 1 F01 2 W/SOLID

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### Time : 

# H'OQAM( H 

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### VES01897 1

### TW I INSTRDMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : UNI T #4 QUARTERL

Y WI T 014 A W T TRAN S DRU M FEED FTRNS P W/DRU M FEE DNEMATRO

N S/N : 42601574NS MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : HI:3 5

TOLED O 814 0 0-1,00 0 lb . 0-1,00 0 lb . 4-2 0 MAD

C

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N NOTE S Chec kscale , digita l Calibratio nper . Toled o instructions . The nwit hno weigh t o nscal e adjus t analo g zero . (NOTE : HM I wil l no t displa y

number s les s tha nzero) . Nex t ad dweigh t = t o 10 % ar e more o f scale s range , the nadjus t analo g span , t o indicat e weigh t o nscale , a s rea donHM I screen .
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Comments :

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B ( fFiel) do r Shop) 1

VES01897 2

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T #4 QUARTERL

Y WIT 014B W T TRAN S AUX . DRU

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N NOTE S Chec kscale , digita l Calibratio nper . Toled o instructions . The nwit hno weigh t onscal e adjus t analo g zero . (NOTE : HM I wil l no t displa y

number s les s tha nzero ) . . Nex t addweigh t = t o 10 % ar e mor e o f scale s range , the nadjus t analo g span , t o indicat e weigh t onscale , a s rea do nHM I screen .
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### CALIBRATIO

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Comments :

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## 3 : 

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M (p i Performe db

y J B CALSHEET.WD

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### VES01897 3

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T # 4 QUARTERL

Y TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : 5 5 O

A Trib o Baghous e Lea kDetection . FL D MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : Aubur n

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B Dat e 

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VES01897 4~^U 4 (IC4034 ) PAG E 1 O F 1

QUARTERL

YCARBO

N INJECTIO

N PREVENTIV

E MAINTENANC E CHEC KSHEE T
PAS S FAI L 1 Disconnec t A C Powe rt o th e Dig i Drive

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4 Verif yan yexterna l safet yswitche s o rlockout s ar e stil l operatio n / 5 Remov e Scre wfeede rcove r8 & blo wou t carbo n 8 B dust

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. j 3 Replac e an yneede d parts , an d lis t an ypart s use d i n commen t /

COMMENTS :

Name : Dat e ://
- 6~o1 Time : 3 ' ? 0 A M 01

QUARTER. 4 11/1/0 6 K

F

VES01897 5

### TW I INSTRDMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T # 4 ANNUA L F T 12 9 FLO W TRAN S PC C LO W GRAD E P-BM S 12 9 F01 3 W/BM S
10149 9 WD

F X-1 0 MANUFACT :

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N NOTE S MICR

O MOTIO N DS100 S 12 8 0-7,00 0 #/H

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Flus hproces s piping , connec t wate r hos e t o upstream sid e o f flo w meter , se t contro l syste m t o appropriat e rat e control , andrea dtotalizer , flo w wate r int o a containe r andcompar e th e toltalize r readin g t o th e measure damount i ncontainer .

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VES01897 6

### TW I INSTRDMEN

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N RECOR D
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N MODEL : DL100S-S S

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C

Nl:2 8 CALIBRATIO

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### VES01897 7

### TW I INSTRDMEN

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VES01897 8

### TW I INSTRDMEN

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N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T # 4 ANNUA L F T 13 8 FLO W TRAN S PC C A Q LI Q X-l l P-BM S 13 8 F01 3 W/BM S
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### VES01897 9

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRDMEN

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N RECOR D UNI T # 4 ANNUA L T T 317A T C ASSEMBL

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VES01898 0

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I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T #4 ANNUA L T T 317 B TC ASSEMBL

E SC C OUTLE

T FL D 31 7 F01 5 T C WEL L INCONE

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### R

VES01898 1

### LOOP :

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N RECOR D UNI T # 4 ANNUA L TAG : T T 305 A PYROMETE

R KIL N OUTLET FL D 30 5 F01 5 44-99-F-1-0- 1 55 " Targe t Tube MANUFACT : IRCO N ' MODEL : M0DLINE 4 44-99-F-1-0- 1 SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : Nl:5 1

Type RT C 0-3,00 0 de g 4-2 0 MAD

C EMIS . 85 %

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N NOTE S Instal l factor y

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### CALIBRATIO

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Comments :

Performe dby: . J B CALSHEET.WD

B S . Date: . Place : Time : _A M P M (Fiel dor

Shop)

VES01898 2

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T #4 ANNUA L TAG : T T LOOP : 305 B DESCRIPON : PYROMETE R SERVICE : KIL

N OUTLET LOCATION : FL

D LP-SHT : 30 5 P&ID : F01 5 REMARKS : 44-99-F-1-0- 1 INSTL-RMKS : 55 " Targe t Tube SPEC-RMKS : S/N : MANUFACT : IRCO N MODEL : M0DLINE 4 44-99-F-1-0- 1 SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : Nl:5 2

Typ e RTC 0-3,00 0 de g 4-2 0 MAD

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N NOTE S Instal l factor y

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### CALIBRATIO

N SOURC E REFERENC

E

Comments :

Performe dby: . J B CALSHEET.WD

B S _Date: . Place: . Time : _A M P M (Field or Shop)



### VES01898 3

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T #4 ANNUA L T T 404 A T C TRAN

S T C GA S OUTLET WAP C 40 4 F01 6 W/GA S CLEANIN

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MOOR E TIY/K2-0-1-4-20M

A 0-150 0 de g F Typ e KT C 4-2 0 MAD

C

CALIBRATIO

N NOTE S Us e col djunctio ncompensate dthermocoupl e calibrato r t o inpu t a temperatur e signa l o f 20 0 de g F . and1,00 0 deg.F . a t inpu t o f transmitter , the nverif y thi s singl e i ncontro l room .

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VES01898 4

### TW I INSTRDMEN

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N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T #4 ANNUA L T T 404 B TC TRAN

S TC GA S OUTLET WAP C F01 6 W/GA S CLEANIN

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MOOR E TIY/K2-0-1-4-20M

A 0-150 0 de g F Typ e KT C 4-2 0 MAD

C

CALIBRATIO

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### I

VES01898 5

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMK

S : S/N : TW

I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T # 4 ANNUA L F T 559A d pTransmitte r STAC KFLO W FL D 55 9 F01 8 PS E averagin g pito t tub e Eas t sid e o f Stac k 122293 1 MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/O NUMBER : N001:009 3

Automatio nServic e 11S1DR2F22B 3 0-1.7 3 i nw

c 0-55,00 0 ACF

M 4-2 0 MAD

C

CALIBRATIO

N NOTE S

0. 1 lb/h r CALIBRATIO N REPOR T INPU T VALU E INSTRUMEN T READIN

G 

# O Befor e Calibration /

, , ~* , H. 

# I ^

r n A 

# Q After Calibration

i±

~ 

# zLQ

CALIBRATIO

N SOURC E REFERENCE

Comments :
fj^jrT.^ y f^Pf Date:i___L_9

_Time:J______!g)P M Performe dby : J B CALSHEET.WD

B Place: . (Field oi(Shop)"



### VES01898 6

### TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : TW

I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T #4 ANNUA L F T 559 B d pTransmitte r STAC KFLO W FL D 55 9 F01 8 PS E averagin g pito t tub e Nort hsid e o f Stac k 122293 1 MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : Automatio nServic e

11S1DR2F22B 3 0-1.7 3 i nw

C 0-55,00 0 ACF

M 4-2 0 MAD

C

N001-.009 3 CALIBRATIO

N NOTE S

-e-: i lb/h r CALIBRATIO N REPOR T INPU T VALU E INSTRUMEN T READIN

G 

# O Before Calibration

/

i t •-> / 

# 1:7- 3 " U C l^^GnnA

Q After Calibration

^

Q ^



### CALIBRATIO

N SOURC E REFERENCE

Comments :

Performe dby : _Date : Time : ll-'OOAAM} P M J B Place : CALSHEET.WD

B

VES01898 7

### TW I INSTRDMEN

T CALIBRATIO

N RECOR D
TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : UNI T #4 ANNUA L F T 42 5 MA GMETE R X-1 8 DI L SLURR

Y WAP C 42 5 F01 6 W/GA S CLEANIN

GTRAI N MANUFACT : MODEL : SCALE : CALIB-IN : CALIB-OUT : PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : HI:11 2

Fische r & Porte r 1475EN09PL29KD11CAC L 0-2 0 GP

M 0-2 0 GP

M 4-2 0 MAD

C

CALIBRATIO

N NOTE S Flus hproces s piping , connec t wate r hos e t o upstream sid e o f flo w meter . Se t contro l system t o appropriat e contro l rate , andrea dtotalizer , flo w wate r int o a containe r an dcompar e th e toltalize r readin g t o th e measure damoun t i ncontainer .

Se e Manufacture s literatur e fo r detaile dinstructions . Fil l ou t andaffi xa ne w calibratio nsticker . •0. 1 lb/h r CALIBRATIO N REPOR

T INPU T VALU E INSTRUMEN T READIN

G Before Calibration



### Afte r Calibration

CALIBRATIO

N SOURC E REFERENCE

:_______^M^ )

CALSHEET.WD

B (Field or Shop)



### VES01898 8

### TW I INSTRUMEN

T CALIBRATIO

N RECOR D UNI T # 4 ANNUA L TAG : LOOP : DESCRIPON : SERVICE : LOCATION : LP-SHT : P&ID : REMARKS : INSTL-RMKS : SPEC-RMKS : S/N : F T 42 6 MA GMETE R X-1 9 DI L SLURR

Y WAP C 42 6 F01 6 W/GA S CLEANIN

GTRAI N Siz e 1 : o r 25m

m MANUFACT : Fische r & MODEL : 10D1475 C SCALE : 0-2 0 GP

M CALIB-IN : 0-2 0 GP M CALIB-OUT ; 4-2 0 MAD C PROCESS-SP : INST-SP : ACTION : I/ O NUMBER : Nl:11 3 Porte r

CALIBRATIO

N NOTE S Flus hproces s piping , connec t wate r hos e t o upstream sid e o f flo w meter . Se t contro l system t o appropriat e contro l rate , an drea dtotalizer , flo w wate r int o a containe r andcompar e th e toltalize r readin g t o th e measure damount i ncontainer .

Se e Manufacture s literatur e fo r detaile dinstructions . Fil l ou t andaffi xa ne w calibratio nsticker . 0. 1 lb/h r CALIBRATIO N REPOR T INPU T VALU E 

# o c .c 4 

# 3 &CK\ 

### INSTRUMEN T READIN

G Before Calibration 

# 3 £c

x Afte r Calibration

CALIBRATIO

N SOURC E REFERENCE

VES01898 9BIWEEKL YLIMI T#4 (CM S Tas k IC4032 ) PAG E 10 F 3 ^'AST E FEE D CUT-OF F PAS S FAI L

1 TSHH-305 KIL N HIG H HIG H 2 TSHH-31 7 SC C HIG H HIG H 3 PAHH-3C

0 KIL N HIG H PRESSUR E 4 PAHH-324 SC C HIG H PRESSUR E 6 TAHHM04 TEMPERIN G CHAMBE R HIG H TEM P 7 VIOLATIO N OPACITYHIG H INSTANTATEOU S 8 PROCES S MONITO R FAILE D 9 WAST E FEE D MONITO R FAILE D 1 2 VIOLATIO N STAC K FLO WHIG H 1 MI N 1 3 VIOLATIO N ZAC-31 6 (TRV ) OPE N 1 4 VIOLATIO N ZAC-02 6 SURG E VEN TOPE N 1 5 UA-557 ANALYZE R FAI L HC L

. 6 UA-5E8 ANALYZE R FAI L C O 1 7 UA-56

0 ANALYZE R FAI L 0 2 1 8 UA-56

2 ANALYZE R FAI L H C 1 9 PDAL-563 LO WDELTAP . (I D FA N FAILURE ) 2 0 WFD-OF F CARBO N INJECTIO N SYSTE M FAILE D ^ 2 1 PSL-10O/PSL-2O O SC C COMB . AI R FA N FAILE D 2 3 PSL-20 9 X-1 4 PRIMARYFUE L LO WPRESS . (ONLYAPPLICABL E FO R # 2 FUE L OIL

) 2 5 STAC KFLO WHIG H INSTANTANEOU S 3 5 VIOLATIO N SC C TEMP . LO W1 MI N AVERAG E A 3 6 VIOLATIO N KIL N TEMP . LO W1 MI N AVERAG E ^ 3 7 WFD-OF F HC L HIG H 1 MI N AVERAG E / 38 WFD-OF F OPACrTYHIG H 1 MI N AVERAG E ^ 3 9 WFD-OF F C O HIG H 1 MI N AVERAG E < ^ -i O WFD-OF F H C (THC ) HIG H 1 MI N AVERAG E ^ 4 1 WFDOF F BAGHOUS E DELT AP HIG H 1 MI N AVERAG E . A



### VES01899 0BIWEEKL YUNI T#4 (CM S Tas k IC4032 ) PAG E 2 O F 3 "•^ST E FEE D CUT-OF F PAS S FAI_L

_

4 2 WFD-OF F SD A OUTLE THIG H TEMP . 1 MI N AVERAG E 4 3 WFD-OF F OXYGE N (02 ) LOW1 MI N AVERAG E 4 4 VIOLATIO N HC L HIG H 1 HOU R AVERAG E 4 5 VIOLATIO N C O HIG H 1 HOU R AVERAG E 4 6 VIOLATIO N SC C TEMP . LO W1 HOU R AVERAG E X HOUR

. / 4 7 WFD-OF F KILN TEMP . LO W1 WW I AVERAG E ' 4 8 VIOLATIO N OPACITYHIG H 480 SEC/HOU R / 4 9 WFD-OF F BAGHOUS E DELTAP LO W1 MI N AVERAG E 5 2 Bag Lea k

Detectio n Syste m (Tribo ) 6 5 Pumpable 1 Hou rRollin g Tota l OP L S 6 6 Non-Pumpabl e 1 Hou rRollin g Tota l OP L / *? 7 Tota l Waste 1 Hou rRollin g Tota l OP L S d 8 BT U 1 Hou rTota l OP L / 6 9 C L 1 2 Hou rRollin g Tota l OP L S 7 0 Lo wViolatil e 1 2 Hou rRollin g tota l OP L ^ 7 1 Sem i Violatil e 1 2 Hou rRollin g Tota l OP L 7 2 Mercur

y1 2 Hou rRollin g Tota l OP L 7 3 As h 1 2 Hou rRollin g Tota l OP L ^ 7 4 PC C Temperatur

e 1 Hou rRollin g Averag e Lo wOP L ^ 7 5 SC C Temperatur

e 1 Hou rRollin g Averag e Lo wOP L 7 6 SD A Outle

t Temperatur

e 1 Hou rRollin g Averag e Hig h OP L ^ 7 7 Baghous

e Differentia l Pressur

e 1 Minut

e Averag e Lo

wOP L ^ - 78 Baghous

e Differentia l Pressur

e 1 Minut

e Averag e Hig h OP L ^ 7 9 Stac k

HC L Corrected 1 Hou rRollin g Averag e Hig h OP L ^ ~ 8 0 Stac k

C O Corrected 1 Hou rRollin g Averag e Hig h OP L 31 Stac k

Flo w1 Hou rRollin g Averag e Hig h OP L ^ 8 2 Hr t CIHra Lim e Flo

w1 Minut

e Averag e OP L ^



### VES01899 1BIWEEKL YUNI T# 4 'VAST E FEE D CUT-OF F CHEC KSHEET PAG E 3 O F 3

5 0 WAST E FEE D CUT-OF F TES TBYOPERATO R UNI T# 4 OPERATO R T O CLOS E MANUA L HAN D VALV E A TLIQUI D INJECTO R BEFOR E FLE XLIM E & AI R LIN E T O SCREENE D FEEDE R XV-01 3 SLID E GATE . UNI T1 4 OPERATO R T O VERIFYCUT-OF F B YPRESSIN G EAC H STAR TBUTTON . (THE N INITIAL & SIG N SHEET ) SHREDDED

_ X-1 0 SCREENED

_ X-1 1 MAI N CONVEYO R

X-1 2 AU XCONVEYO R

X-2 2 VERIF YATOMIZIN G AI R ALAR M B YMANUALL YSHUTTIN G AI R T O PRESSUR E SWITCH

. (NOZZE LMUS TBEjjOPE N FO R ALAR M T O FUNCTION ) X-1 0 X-1 1 X-1 2 X-2 2 ALS O CHEC KOPERATIO N O F RA M COOUN G WATE R LO WFLO WALAR M (MSG# >278 ) CHECKE D BY : 

### V U 

# UJC

X^TcVu 3 CA _X_y,* S 8 3 Lim e Slurr

yDensit yLo w1 Hou rRollin g Averag e Shoutdown ALO G CHECK S I N OPERATION S BOOK

. 8 5 RO D OU TKIL N PRESSUR E LIN E (PT-3Q0) COMMENTS :



# O L prl-^rll t ^OL(/-V

_Date : CHECKE D BY :
APPROVE D B Y: Place : Contro l Roo m BIWEEKiY_ 4 9/10/07 H K



### VES01899 2BIWEEKLYU M I T# 4 (CM S Tas k IC4032 ) PAG E 1 O F 3 •>ST E FEE D CUT-OF F PAS S FAI L

1 TSHH-30 5 KIL N HIG H HIG H ^ 2 TSHH-31 7 SC C HIG H HIG H ^ 3 PAHH-3O0 KIL N HIG H PRESSUR E / 4 PAHH-32 4 SC C HIG H PRESSUR E ^ 6 TAHH-40 4 TEMPERIN G CHAMBE R HIG H TEM P ^ 7 VIOLATIO N OPACITYHIG H INSTANTATEOU S ^ 8 PROCES S MONITO R FAILE D f 9 WAST E FEE D MONITO R FAILE D 1 2 VIOLATIO N STAC KFLO WHIG H 1 MI N S 1 3 VIOLATIO N ZAC-31 6 (TRV ) OPE N / 1 4 VIOLATIO N ZAC-02 6 SURG E VEN TOPE N /

• " 5 UA-557 ANALYZE R FAI L HC L / 1 6 UA-558 ANALYZE R FAI L C O / 1 7 UA-560 ANALYZE R FAI L 0 2 f 1 8 UA-562 ANALYZE R FAI L H C / 1 9 PDAL-56 3 LO WDELTAP . (I D FA N FAILURE ) S 2 0 WFD-OF F CARBO N INJECTIO N SYSTE M FAILE D / 2 1 PSL-10O/PSL-2O O SC C COMB . AI R FA N FAILE D ^ 2 3 PSL-20 9 X-1 4 PRIMARYFUE L LO WPRESS . (ONLYAPPLICABL E FO R # 2 FUE L OIL

) ^ 25 STAC KFLO WHIG H INSTANTANEOU S 35 VIOLATIO N SC C TEMP . LO W1 MI N AVERAG E 36 VIOLATIO N KIL N TEMP . LO W1 MI N AVERAG E 37 WFD-OF F HC L HIG H 1 MI N AVERAG E ^ 38 WFD-OF F OPACIT YHIG H 1 MI N AVERAG E / 39 WFD-OF F C O HIG H 1 MI N AVERAG E S 4 0 WFD-OF F H C (THC ) HIG H 1 MI N AVERAG E f 41 WFD-OF F BAGHOUS E DELT AP HIG H 1 MI N AVERAG E . f



### VES01899 3BIWEEKL YUN I T# 4 (CM S Tas k IC4032 ) PAG E 2 O F 3 "ST E FEE D CUT-OF F PAS S FAI L

4 2 WFD-OF F SD A OUTLE THIG H TEMP . 1 MI N AVERAG E * ^ 4 3 WFD-OF F OXYGE N (02 ) LO W1 MI N AVERAG E ^ 44 VIOLATIO N HC L HIG H 1 HOU R AVERAG E ^ 4 5 VIOLATIO N C O HIG H 1 HOU R AVERAG E ^ 4 6 VIOLATIO N SC C TEMP . LO W1 HOU R AVERAG E ^ HOUR , 4 7 WFD-OF F KIL N TEMP . LO W1 RO T AVERAG E 4 8 VIOLATIO N OPACITYHIG H 48 0 SEC/HOU R / ~ 4 9 WFD-OF F BAGHOUS E DELTAP LOW1 MI N AVERAG E 5 2 Ba g Lea k

Detectio n Syste m (Tribo ) 6 5 PumpaW

e 1 Hou rRollin g Tota l OP L ^ 6 6 Non-Pumpabl e 1 Hou rRollin g Tota l OPt

_ H7 Tota l Waste 1 Hou rRollin g Tota l OP L " 6 8 BT U 1 Hou rTota l OP L 6 9 C L 1 2 Hou rRollin g Tota l OP L ^ 7 0 Lo wVolatil e 1 2 Hou rRollin g Tota l OP L 7 1 Sem i Violatil e 1 2 Hou rRollin g Tota l OP L ^ 7 2 Mercur

y1 2 Hou rRollin g Tota l OP L S 7 3 As h 1 2 Hou rRollin g Tota l OP L ^ 7 4 PC C Temperatur e 1 Hou rRollin g Averag e Lo wOP L ^ 7 5 SC C Temperatur e 1 Hou rRollin g Averag e Lo wOP L 7 6 SD A Outle

t Temperatur

e 1 Hou rRollin g Averag e Hig h OP L 77 Baghouse Differentia l Pressur e 1 Minut

e Averag e Lo

wOP L y 78 Baghouse Differentia l Pressur e 1 Minut

e Averag e Hig h OP L < ^ 7 9 Stac k

HC L Corrected 1 Hou rRollin g Averag e Hig h OP L 8 0 Stac k

C O Corrected 1 Hou rRollin g Averag e Hig h OP L S^ <5 1 Stac k

Ho w1 Hou rRollin g Averag e Hig h OP L 8 2 Hr t Cl/Hra Lim e Flo

w1 Minut

e Averag e OP L



### VES01899 4BIWEEKL YUNIT# 4 ST E FEE D CUT-OF F CHEC KSHEE T PAG E 3 O F 3

5 0 WAST E FEE D CUT-OF F TES TB YOPERATO R UNI Tm OPERATO R T O CLOS E MANUA L HAN D VALV E A TLIQUI D INJECTO R BEFOR E FLE XLIM E & AI R LIN E T O SCREENE D FEEDE R XV-01 3 SLID E GATE . UNI T# 4 OPERATO R T O VERIFYCUT-OF F B YPRESSIN G EAC H STAR TBUTTON . (THE N INITIAL & SIG N SHEET ) SHREDDED

_ X-1 0 _SCREENED

_ X-1 1 MAI N CONVEYO R

x-1 2 

# y AU XCONVEYO R X-2 2 VERIF VATOMIZIN G AI R ALAR M BYMANUALL YSHUTTIN G AI R T O PRESSUR E SWITCH

. (NOZZE LMUS TB E OPE N FO R ALAR M T O FUNCTION ) X-1 0 X-1 1 X-1 2 X-2 2 ALS O CHEC KOPERATIO N O F RA M COOUNGfWATE R LO WFLO WALAR M (MSG * >278 ) CHECKE D BY : 

# V VtjucA ^



# 7Al_ > Q U 

# fA s 8 3 Lim e Slurr

yDensit yLo w1 Hou rRollin g Averag e

• JALO G CHECK S I N OPERATION S BOOK

. 8 5 RO D OU TKIL N PRESSUR E LIN E (PT-300) Shoutdow n

COMMENTS :


# QVu

-C ^ W ^jttOO L^

rSDate : 

## i£> R T_J° fTime : 

# \Q'SO^rP^ CHECKE D BY :

APPROVE D BY : Place : Contro l Roo m
BIWEEKLY_ 4 9/1O/0 7 H K



### VES01899 5,rUNIT# 4 c FEE D CUT-OF F (CM S Tas k IC4032 ) PAG E 1 O F 3

PAS S FAI L

1 TSHB-30 5 KIL N HIG H HIG H 2 TSHH-31 7 SC C HIG H HIG H 3 PAHH-30O KIL N HIG H PRESSUR E 4 PAHH-324 SC C HIG H PRESSUR E 6 TAHH40 4 TEMPERIN G CHAMBE R HIG H TEM P 7 VIOLATIO N OPACIT YHIG H INSTANTATEOU S 8 PROCES S MONITO R FAILE D 9 WAST E FEE D MONITO R FAILE D 1 2 VIOLATIO N STAC KFLO WHIG H 1 MI N 1 3 VIOLATIO N ZAC-31 6 (TRV ) OPE N 1 4 VIOLATIO N ZAC-02 6 SURG E VEN TOPE N 1 5 UA-557 ANALYZE R FAI L HC L Jj UA-558ANALYZE R FAI L C O 1 7 UA-560 ANALYZE R FAI L 0 2 1 8 UA-562ANALYZE R FAI L H C 1 9 PDAL-65 3 LO WDELT AP . (I D FA N FAILURE ) 2 0 WFD-OF F CARBO N INJECTIO N SYSTE M FAILE D 2 1 PSL-10WPSL-20 0 SC C COMB . AI R FA N FAILE D 2 3 PSL-209 X-1 4 PRIMAR YFUE L LO WPRESS . (ONL YAPPLICABL E FO R # 2 FUE L OIL

) 2 5 STACKFLO WHIG H INSTANTANEOU S 3 5 VIOLATIO N SC C TEMP . LO W1 MI N AVERAG E 36 VIOLATIO N KIL N TEMP . LO W1 MI N AVERAG E 3 7 WFD-OF F HC L HIG H 1 MI N AVERAG E 38 WFD-OF F OPACIT YHIG H 1 MI N AVERAG E 39 WFD-OF F C O HIG H 1 MI N AVERAG E

- WFD-OF F H C (THC ) HIG H 1 MI N AVERAG E 41 WFD-OF F BAGHOUS E DELT AP HIG H 1 MI N AVERAG E



### VES01899 6. rUNIT# 4 (CM S Tas k IC4032 ) PAG E 2 O F 3 : FEE D CUT-OF F PAS S FAI L

4 2 WFD-OF F SD A OUTLE THIG H TEMP . 1 MI N AVERAG E 4 3 WFD-OF F OXYGE N (02) LO W1 MI N AVERAG E 4 4 VIOLATIO N HC L HIG H 1 HOU R AVERAG E 4 5 VIOLATIO N C O HIG H 1 HOU R AVERAG E

4 8 VIOLATIO N OPACIT YHIG H 48 0 SEC/HOU R 4 9 WFD-OF F BAGHOUS E DELTAP LO W1 MI N AVERAG E 5 2 Ba g Lea k

Detectio n Syste m (Tribo ) 6 5 Pumpabl e 1 Hou rRollin g Tota l OP L 6 6 Non-Pumpabl e 1 Hou rRollin g Tota l OP L 6 7 Tota l Waste 1 Hou rRollin g Tota l OP L .J BT U 1 Hou rTota l OP L 6 9 C L 1 2 Hou rRollin g Tota l OP L 7 0 Lo wViolatil e 1 2 Hou rRollin g Tota l OP L 7 1 Sem i Violatil e 1 2 Hou rRollin g Tota l OP L

75 SC C Temperatur

e 1 Hou rRollin g Averag e Lo wOP L

78 Baghouse Differentia l Pressure 1 Minut e Averag e Hig h OP L 79 Stac k

HC L Correcte d 1 Hou rRollin g Averag e Hig h OP L 80 Stac k

C O Correcte d 1 Hou rRollin g Averag e Hig h OP L

^ Stac k Flo w1 Hou rRollin g Averag e Hig h OP L 82 Hi t Cl/Hra Lim e Flow1 Minut e Averag e OP L 4 6 •VIOLATIO N SC C TEMP . LO W1 HOU R AVERAG E ' „ 47 WFD-OF F KIL N TEMP . LO W1 BWfrAVERAG E



# /

7 2 Mercur

y1 2 Hou rRollin g Tota l OP L X 

### 7~ 73 As h 1 2 Hou rRollin g Tota l OP L X



# _ _ 74 PC C Temperatur

e 1 Hou rRollin g Averag e Lo wOP L 

### 7~

76 SD A Outle

t Temperatur

e 1 Hou rRollin g Averag e Hig h OP L y 77 Baghouse Differentia l Pressur e 1 Minut

e Averag e Lo

wOP L y



### VES01899 7. , UNI T# 4 CHEC KSHEE T d FEE D CUT-OF F PAG E 3 O F 3

50 WAST E FEE D CUT-OF F TES TB YOPERATO R UNI T# 4 OPERATO R T O CLOS E MANUA L HAN D VALV E A TLIQUI D INJECTO R BEFOR E FLE XLIM E & AI R LIN E T O SCREENE D FEEDE R XV-01 3 SLID E GATE . UNI T# 4 OPERATO R T O VERIFYCUT-OF F B YPRESSIN G EAC H STAR TBUTTON . (THE N INITIA L & SIG N SHEET ) SHREDDE D SCREENE D ^ J f MAI N CONVEYO R ^^K - AU XCONVEYO R X-1 0 x-11_^___ " X-1 2 

### %*^~«-^ x -22 %~-T^_

_ VERIF YATOMIZIN G AI R ALAR M BYMANUALL YSHUTTIN G AI R T O PRESSUR E SWITCH

. (NOZZE LMUS TB E OPE N FO R ALAR M T O FUNCTION ) X-1 0 ALS O CHEC KOPERATIO N O F RA M COOLIN G WATE R LO WFLO WALAR M (MSG * >27S) CHECKE D BY : 8 3 Lim e Slurr

yDensityLo

w1 Hou rRollin g Averag e Shoutdow n LO G CHECK S I N OPERATION S BOOK

. 8 5 RO D OU TKIL N PRESSUR E LIN E (PT-300 )
COMMENTS :

CHECKE D BY : 

### Date :_j7____" ? Tim e : 

### 2* VT %£^ M
APPROVE D BY : Place : Contro l Roo m
BIWEEKLY

_4 9/10/0 7 H K



### VES01899 8