Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

6041 Spurlock 3 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

6041 Spurlock 3 As Received Higher Heating Value 6041 Spurlock 3 As Received % Moisture 6041 Spurlock 3 As Received % Ash 6041 Spurlock 3 As Received % Sulfur 6041 Spurlock 3 Dry basis Higher Heating Value 6041 Spurlock 3 Dry basis % Ash 6041 Spurlock 3 Dry basis % Sulfur 6041 Spurlock 3 Dry basis Antim ony 6041 Spurlock 3 Dry basis Arsenic 6041 Spurlock 3 Dry basis Beryllium 6041 Spurlock 3 Dry basis Cadmium 6041 Spurlock 3 Dry basis Chlorine 6041 Spurlock 3 Dry basis Chromium 6041 Spurlock 3 Dry basis Cobalt 6041 Spurlock 3 Dry basis Fluorine 6041 Spurlock 3 Dry basis Lead 6041 Spurlock 3 Dry basis Manganese 6041 Spurlock 3 Dry basis Mercury 6041 Spurlock 3 Dry basis Nickel 6041 Spurlock 3 Dry basis SeleniumAnalysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865-04 ASTM D3302-05 ASTM D3174-04 ASTM D4239-05 C ASTM D5865-04 ASTM D3174-04 ASTM D4239-05 C ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D4208-02 ASTM D6357-04 B ASTM D6357-04 B ASTM D3761-96 ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 CEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6041 Spurlock 3 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 5/11/2010 5/11/2010 10902.00 Btu/lb 2 5/11/2010 5/11/2010 10840.00 Btu/lb 3 5/11/2010 5/11/2010 10922.00 Btu/lb 1 5/12/2010 5/12/2010 10805.00 Btu/lb 2 5/12/2010 5/12/2010 10903.00 Btu/lb 3 5/12/2010 5/12/2010 10482.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 6.83 18.17 3.47 11701 Btu/lb 19.5 3.72 7.72 17.89 3.6 11747 Btu/lb 19.39 3.9 7.8 18.06 3.89 11846 Btu/lb 19.59 4.22 6.77 19.3 3.71 11590 Btu/lb 20.7 3.98 6.81 18.71 3.75 11700 Btu/lb 20.08 4.02 6.57 20.17 3.55 11219 Btu/lb 21.59 3.8Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ABeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ANickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 36.26 19.5 44.24 63.5 4.34 1.18 3.72 35.75 19.39 44.86 63.96 4.33 1.17 3.9 36.8 19.59 43.61 64.08 4.4 1.07 4.22 36.39 20.7 42.91 64.39 4.4 1.18 3.98 36.94 20.08 42.98 63.57 4.4 1.07 4.02 34.52 21.59 43.89 62.17 4.23 1.06 3.8 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

7.76 7.25 6.64 5.35 6.86 7.15EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6041 Spurlock 3 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 1 5/18/2010 5/18/2010 10344.00 Btu/lb 2 5/18/2010 5/18/2010 10573.00 Btu/lb 3 5/19/2010 5/19/2010 10459.00 Btu/lb 1 5/18/2010 5/18/2010 10344.00 Btu/lb 3 5/19/2010 5/19/2010 10459.00 Btu/lb 3 5/19/2010 5/19/2010 10675.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 7.91 21.39 2.05 11233 Btu/lb 23.23 2.23 7.33 20.29 2.79 11409 Btu/lb 21.9 3.01 7.4 20.67 2.72 11295 Btu/lb 22.32 2.94 7.91 21.39 2.05 11233 Btu/lb 23.23 2.23 7.4 20.67 2.72 11295 Btu/lb 22.32 2.94 7.96 19.13 2.3 11598 Btu/lb 20.78 2.82Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 713 ppm 0.13 μg/g 0.93 μg/g 14.27 μg/g 1.74 953 ppm 0.15 μg/g 0.6 μg/g 14.46 μg/g 1.88 610 ppm 0.14 μg/g 0.99 μg/g 13.87 μg/g 1.83 713 ppm 0.13 μg/g 0.93 μg/g 14.27 μg/g 1.74 610 ppm 0.14 μg/g 0.99 μg/g 13.87 μg/g 1.83 804 ppm 0.17 μg/g 0.73 μg/g 15.29 μg/g 1.9Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g 0.24 μg/g 26.97 μg/g 7.53 μg/g 45.08 μg/g μg/g 0.11 μg/g 31.81 μg/g 9.26 μg/g 43.71 μg/g μg/g 0.19 μg/g 27.63 μg/g 8.75 μg/g 49.66 μg/g μg/g 0.24 μg/g 26.97 μg/g 7.53 μg/g 45.08 μg/g μg/g 0.19 μg/g 27.63 μg/g 8.75 μg/g 49.66 μg/g μg/g 0.27 μg/g 29.14 μg/g 7.75 μg/g 45.12 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 17.03 μg/g 5.52 μg/g 110 ppm 8.1 μg/g 16.88 μg/g 3.99 μg/g 124 ppm 9.45 μg/g 17.18 μg/g 4.18 μg/g 114 ppm 8.07 μg/g 17.03 μg/g 5.52 μg/g 110 ppm 8.1 μg/g 17.18 μg/g 4.18 μg/g 114 ppm 8.07 μg/g 16.94 μg/g 4.86 μg/g 126 ppm 7.58 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur N/A 32.27 23.23 44.5 61.86 4.12 1.13 2.23 N/A 33.64 21.93 44.46 62.38 4.19 1.13 3.01 N/A 33.14 22.32 44.54 61.38 4.1 1.09 2.94 N/A 32.27 23.23 44.5 61.86 4.12 1.13 2.23 N/A 33.14 22.32 44.54 61.38 4.1 1.09 2.94 N/A 31.78 20.78 47.44 63.38 4.26 1.4 2.82 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 7.43 7.39 8.17 7.43 8.17 7.36EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6041 Spurlock 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 5/19/2010 5/19/2010 10329.00 Btu/lb 2 5/20/2010 5/20/2010 10670.00 Btu/lb 3 5/20/2010 5/20/2010 10763.00 Btu/lb 1 5/20/2010 5/20/2010 10670.00 Btu/lb 2 5/20/2010 5/20/2010 10763.00 Btu/lb 3 5/20/2010 5/20/2010 10763.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 7.98 21.48 2.48 11225 Btu/lb 23.34 2.69 7.48 19.4 3.15 11533 Btu/lb 20.97 3.41 7.36 19.21 2.76 11618 Btu/lb 20.74 2.98 7.48 19.4 3.15 11533 Btu/lb 20.97 3.41 7.36 19.21 2.76 11618 Btu/lb 20.74 2.98 7.64 19.53 2.43 11653 Btu/lb 21.15 2.63Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ABeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ANickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 32.04 23.34 44.62 61.56 4.04 1.1 2.69 7.27 34.68 20.97 44.35 63.37 4.23 1.16 3.41 6.86 33.32 20.74 45.94 63.35 4.45 1.14 2.98 7.34 34.68 20.97 44.35 63.37 4.23 1.16 3.41 6.86 33.32 20.74 45.94 63.35 4.45 1.14 2.98 7.34 33.45 21.15 45.4 63.92 4.29 1.19 2.63 6.82 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6041 Spurlock 3

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm