Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant Report Date: 3/13/2013

Sample Number:130659-001Date Collected:02/13/2013 10:00Date Received:2/15/2013 

### CPS Influent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 37.2 0.050 DPC EPA 200.8 0.010 02/20/2013 14:45 ug/L Arsenic, As 218 0.10 DPC EPA 200.8 0.030 02/20/2013 14:45 ug/L Barium, Ba 177 0.10 DPC EPA 200.8 0.020 02/20/2013 14:45 ug/L Beryllium, Be < 0.1 0.50 DAM EPA 200.7 0.10 02/25/2013 13:00 U ug/L Cadmium, Cd 216 0.050 DPC EPA 200.8 0.010 02/20/2013 14:45 ug/L Chromium, Cr 1170 0.20 DPC EPA 200.8 0.040 02/20/2013 14:45 ug/L Cobalt, Co 243 0.020 DPC EPA 200.8 0.0040 02/20/2013 14:45 ug/L Copper, Cu 444 0.050 DPC EPA 200.8 0.010 02/20/2013 14:45 ug/L Lead, Pb 331 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:45 ug/L Molybdenum, Mo 422 0.050 DPC EPA 200.8 0.010 02/20/2013 14:45 ug/L Nickel, Ni 1450 0.20 DPC EPA 200.8 0.050 02/20/2013 14:45 ug/L Selenium, Se 701 0.50 DPC EPA 200.8 0.20 02/20/2013 14:45 ug/L Silver, Ag 0.269 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:45 ug/L Thallium, Tl 14.1 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:45 ug/L Tin, Sn < 1 5.0 DAM EPA 200.7 1.0 02/25/2013 13:00 U ug/L Titanium, Ti 780 2.0 DAM EPA 200.7 0.30 02/25/2013 13:00 ug/L Zinc, Zn 3800 0.50 DPC EPA 200.8 0.10 02/20/2013 14:45 mg/L Aluminum, Al 73.9 0.0010DPC EPA 200.8 0.0003 02/20/2013 14:45 mg/L Boron, B 379 0.020DAM EPA 200.7 0.0040 02/25/2013 13:00 mg/L Calcium, Ca 1730 0.020DAM EPA 200.7 0.0040 02/25/2013 13:00 mg/L Iron, Fe 245 0.050DAM EPA 200.7 0.010 02/25/2013 13:00 mg/L Magnesium, Mg 3740 0.010DAM EPA 200.7 0.0020 02/25/2013 13:00 mg/L Manganese, Mn 59.8 0.0005DAM EPA 200.7 0.0001 02/25/2013 13:00 mg/L Potassium, K 59.7 0.050DAM EPA 200.7 0.0070 02/25/2013 12:59 mg/L Sodium, Na 275 0.050DAM EPA 200.7 0.0080 02/25/2013 12:59 mg/L Strontium, Sr 13.9 0.0010DAM SW-846 6010C 0.0003 02/25/2013 12:59 mg/L Total Kjeldahl Nitrogen, TKN as N10.2 0.50 DMM EPA 351.2 0.10 02/20/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.08 0.10 DMM SM20 4500NO3 H 0.020 02/19/2013 J mg/L Phosphorus, Total, P 22.2 0.050DMM EPA 365.4 0.010 02/20/2013 mg/L Residue, Filterable, TDS18500 400 MSO SM20 2540C 120 02/20/2013 mg/L Residue, Non-Filterable, TSS19400 200 MSO SM20 2540D 40 02/20/2013 mg/L Sulfate, SO4 8040 50 TDF EPA 300.1 14 02/22/2013 17:28

Mountaineer Plant, 130659 Page 1 of 3

### Location: Mountaineer Plant Report Date: 3/13/2013

Sample Number:130659-002Date Collected:02/13/2013 10:00Date Received:2/15/2013 

### CPS Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.36 0.050 DPC EPA 200.8 0.010 02/20/2013 14:50 ug/L Arsenic, As 2.99 0.10 DPC EPA 200.8 0.030 02/20/2013 14:50 ug/L Barium, Ba 67.1 0.10 DPC EPA 200.8 0.020 02/20/2013 14:50 ug/L Beryllium, Be < 0.1 0.50 DAM EPA 200.7 0.10 02/25/2013 13:05 U ug/L Cadmium, Cd 0.74 0.050 DPC EPA 200.8 0.010 02/20/2013 14:50 ug/L Chromium, Cr 3.3 0.20 DPC EPA 200.8 0.040 02/20/2013 14:50 ug/L Cobalt, Co 1.95 0.020 DPC EPA 200.8 0.0040 02/20/2013 14:50 ug/L Copper, Cu 2.06 0.050 DPC EPA 200.8 0.010 02/20/2013 14:50 ug/L Lead, Pb 0.737 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:50 ug/L Molybdenum, Mo 394 0.050 DPC EPA 200.8 0.010 02/20/2013 14:50 ug/L Nickel, Ni 68.2 0.20 DPC EPA 200.8 0.050 02/20/2013 14:50 ug/L Selenium, Se 63.0 0.50 DPC EPA 200.8 0.20 02/20/2013 14:50 ug/L Silver, Ag 0.005 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:50 J ug/L Thallium, Tl 0.51 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:50 ug/L Tin, Sn < 1 5.0 DAM EPA 200.7 1.0 02/25/2013 13:05 U ug/L Titanium, Ti 3.3 2.0 DAM EPA 200.7 0.30 02/25/2013 13:05 ug/L Zinc, Zn 21.4 0.50 DPC EPA 200.8 0.10 02/20/2013 14:50 mg/L Aluminum, Al 0.278 0.0010DPC EPA 200.8 0.0003 02/20/2013 14:50 mg/L Boron, B 283 0.020DAM EPA 200.7 0.0040 02/25/2013 13:05 mg/L Calcium, Ca 692 0.020DAM EPA 200.7 0.0040 02/25/2013 13:05 mg/L Iron, Fe 1.77 0.050DAM EPA 200.7 0.010 02/25/2013 13:05 mg/L Magnesium, Mg 2450 0.010DAM EPA 200.7 0.0020 02/25/2013 13:05 mg/L Manganese, Mn 34.8 0.0005DAM EPA 200.7 0.0001 02/25/2013 13:05 mg/L Potassium, K 47.3 0.050DAM EPA 200.7 0.0070 02/25/2013 13:03 mg/L Sodium, Na 273 0.050DAM EPA 200.7 0.0080 02/25/2013 13:03 mg/L Strontium, Sr 8.75 0.0010DAM SW-846 6010C 0.0003 02/25/2013 13:03 mg/L Total Kjeldahl Nitrogen, TKN as N7.10 0.50 DMM EPA 351.2 0.10 02/20/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.10 0.10 DMM SM20 4500NO3 H 0.020 02/19/2013 mg/L Phosphorus, Total, P 0.15 0.050DMM EPA 365.4 0.010 02/20/2013 mg/L Residue, Filterable, TDS14200 400 MSO SM20 2540C 120 02/20/2013 mg/L Residue, Non-Filterable, TSS30 10 MSO SM20 2540D 2.0 02/20/2013 mg/L Sulfate, SO4 6600 50 TDF EPA 300.1 14 02/22/2013 17:43

Mountaineer Plant, 130659 Page 2 of 3

### Location: Mountaineer Plant Report Date: 3/13/2013

Sample Number:130659-003Date Collected:02/13/2013 10:00Date Received:2/15/2013 

### Bioreactor Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.16 0.050 DPC EPA 200.8 0.010 02/20/2013 14:55 ug/L Arsenic, As 0.22 0.10 DPC EPA 200.8 0.030 02/20/2013 14:55 ug/L Barium, Ba 47.3 0.10 DPC EPA 200.8 0.020 02/20/2013 14:55 ug/L Beryllium, Be < 0.1 0.50 DAM EPA 200.7 0.10 02/25/2013 13:16 U ug/L Cadmium, Cd 0.83 0.050 DPC EPA 200.8 0.010 02/20/2013 14:55 ug/L Chromium, Cr 0.2 0.20 DPC EPA 200.8 0.040 02/20/2013 14:55 J ug/L Cobalt, Co 0.147 0.020 DPC EPA 200.8 0.0040 02/20/2013 14:55 ug/L Copper, Cu 0.17 0.050 DPC EPA 200.8 0.010 02/20/2013 14:55 ug/L Lead, Pb 0.022 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:55 ug/L Molybdenum, Mo 2160 0.050 DPC EPA 200.8 0.010 02/20/2013 14:55 ug/L Nickel, Ni 4.00 0.20 DPC EPA 200.8 0.050 02/20/2013 14:55 ug/L Selenium, Se 0.9 0.50 DPC EPA 200.8 0.20 02/20/2013 14:55 ug/L Silver, Ag < 0.002 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:55 U ug/L Thallium, Tl 0.03 0.010 DPC EPA 200.8 0.0020 02/20/2013 14:55 ug/L Tin, Sn < 1 5.0 DAM EPA 200.7 1.0 02/25/2013 13:16 U ug/L Titanium, Ti < 0.3 2.0 DAM EPA 200.7 0.30 02/25/2013 13:16 U ug/L Zinc, Zn 1.2 0.50 DPC EPA 200.8 0.10 02/20/2013 14:55 mg/L Aluminum, Al 0.656 0.0010DPC EPA 200.8 0.0003 02/20/2013 14:55 mg/L Boron, B 150 0.020DAM EPA 200.7 0.0040 02/25/2013 13:16 mg/L Calcium, Ca 466 0.020DAM EPA 200.7 0.0040 02/25/2013 13:16 mg/L Iron, Fe 1.24 0.050DAM EPA 200.7 0.010 02/25/2013 13:16 mg/L Magnesium, Mg 1290 0.010DAM EPA 200.7 0.0020 02/25/2013 13:16 mg/L Manganese, Mn 16.7 0.0005DAM EPA 200.7 0.0001 02/25/2013 13:16 mg/L Potassium, K 74.9 0.050DAM EPA 200.7 0.0070 02/25/2013 13:15 mg/L Sodium, Na 936 0.050DAM EPA 200.7 0.0080 02/25/2013 13:15 mg/L Strontium, Sr 6.26 0.0010DAM SW-846 6010C 0.0003 02/25/2013 13:15 mg/L Total Kjeldahl Nitrogen, TKN as N3.93 0.50 DMM EPA 351.2 0.10 02/20/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.12 0.10 DMM SM20 4500NO3 H 0.020 02/19/2013 mg/L Phosphorus, Total, P 0.11 0.050DMM EPA 365.4 0.010 02/20/2013 mg/L Residue, Filterable, TDS10400 400 MSO SM20 2540C 120 02/20/2013 mg/L Residue, Non-Filterable, TSS< 2 10 MSO SM20 2540D 2.0 02/20/2013 U mg/L Sulfate, SO4 5460 50 TDF EPA 300.1 14 02/22/2013 17:59

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Mercury reported under lab number 130656.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224

Fax 614-836-4168Audinet 210-4224

Mountaineer Plant, 130659 Page 3 of 3