### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

47 Colbert 3 

### otherFuel Type 2 Fuel Type 3 Other Fuel Description 

### subbituminous/bituminous blendEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 47 Colbert 3 As Received Higher Heating Value 

### 47 Colbert 3 As Received % Moisture 

### 47 Colbert 3 As Received % Ash 

### 47 Colbert 3 As Received % Sulfur 

### 47 Colbert 3 Dry basis Higher Heating Value 

### 47 Colbert 3 Dry basis % Ash 

### 47 Colbert 3 Dry basis % Sulfur 

### 47 Colbert 3 Dry basis Antim ony 

### 47 Colbert 3 Dry basis Arsenic 

### 47 Colbert 3 Dry basis Bery llium 

### 47 Colbert 3 Dry basis Cadmium 

### 47 Colbert 3 Dry basis Chlorine 

### 47 Colbert 3 Dry basis Chromium 

### 47 Colbert 3 Dry basis Cobalt 

### 47 Colbert 3 Dry basis Fluorine 

### 47 Colbert 3 Dry basis Lead 

### 47 Colbert 3 Dry basis Manganese 

### 47 Colbert 3 Dry basis Mercury 

### 47 Colbert 3 Dry basis Nickel 

### 47 Colbert 3 Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865/D3180 ASTM D3302 ASTM D5142/D3180 ASTM D4239/D3180 ASTM D5865/D3180 ASTM D5142/D3180 ASTM D4239/D3180 EPA 6010B EPA 6010B EPA 6010B EPA 6010B ASTM D6721 EPA 6010B EPA 6010B ASTM D3761/D3180 EPA 6010B EPA 6010B CLS-127.01-013/D3180 EPA 6010B EPA 6010BEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 47 Colbert 3 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units AL19367 

### 6/3/2010 6/3/2010 10759.00 Btu/lb AL19368 6/4/2010 6/4/2010 10896.00 Btu/lb AL19369 6/4/2010 6/4/2010 10924.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 16.33 5.73 0.33 12858 Btu/lb 6.85 0.4 13.9 7.55 0.36 12655 Btu/lb 8.77 0.41 15.08 6.37 0.35 12864 Btu/lb 7.5 0.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 16.33 13.9 15.08 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 41.04 6.85 52.11 72.7 5.11 1.36 0.4 13.7 39.99 8.77 51.25 71.4 5.05 1.42 0.41 13 40.29 7.5 52.21 72.2 5.09 1.41 0.41 13.4 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 47 Colbert 3 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units AL19364 

### 5/25/2010 5/25/2010 10433.00 Btu/lb AL19365 5/26/2010 5/26/2010 10564.00 Btu/lb AL19366 5/27/2010 5/27/2010 10643.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 16.44 7.65 0.33 12485 Btu/lb 9.15 0.39 17.02 6.78 0.39 12731 Btu/lb 8.17 0.48 16.43 6.15 0.36 12736 Btu/lb 7.36 0.43Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 0.024 % 0.023 ppm 3.8 mg/Kg 3.8 mg/Kg 0.39 0.057 % 0.027 ppm 4 mg/Kg 4 mg/Kg 0.46 0.032 % 0.028 ppm 4.5 mg/Kg 4.5 mg/Kg 0.45Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg 0.95 mg/Kg 2.7 mg/Kg 3.4 mg/Kg 8.8 mg/Kg mg/Kg 1 mg/Kg 2.9 mg/Kg 4 mg/Kg 17 mg/Kg mg/Kg 1.1 mg/Kg 2.6 mg/Kg 3.6 mg/Kg 8.4 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 3.8 mg/Kg 3.8 mg/Kg 0.008 % 1.9 mg/Kg 4 mg/Kg 4 mg/Kg 0.0077 % 2 mg/Kg 4.5 mg/Kg 4.5 mg/Kg 0.0068 % 2.2 mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen



### 16.44 39.62 9.15 51.22 71 5.02 1.37 17.02 40.61 8.17 51.22 72.6 4.98 1.37 16.43 40.34 7.36 52.31 72.5 5.12 1.41 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Sulfur Oxygen 

### 0.39 13.1 0.48 12.4 0.43 13.1 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 47 Colbert 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units AL19370 

### 6/5/2010 6/5/2010 11336.00 Btu/lb AL19371 6/5/2010 6/5/2010 11389.00 Btu/lb AL19372 6/6/2010 6/6/2010 10987.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 13.28 7.59 0.56 13072 Btu/lb 8.76 0.65 12.6 7.32 0.53 13031 Btu/lb 8.37 0.61 14.58 6.77 0.42 12862 Btu/lb 7.93 0.49Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 0.045 % 0.029 % 0.029 %Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 0.0096 % 13.28 0.0097 % 12.6 0.0089 % 14.58 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 39.36 8.76 51.88 72.9 5.15 1.48 0.65 11.1 40.03 8.37 51.59 72.5 5.18 1.46 0.61 11.9 40.69 7.93 51.39 72.2 5.08 1.42 0.49 12.9 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 47 Colbert 3

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg subbituminous/bituminous blend ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm