### NOTIFICATION OF COMPLIANCE STATUS Page 1 of 3 Applicable Rule: 40 CFR Part 63, Subpart N-National Emission Standards for Chromium Emissions from Hard and Decorative Chromium Electroplating and Chromium Anodizing Tanks 

### I. Print or type**~e** 

### following for each plant in which chromium electroplating and/or chromium anodizing operations are performed. Owner/Operatorrritle Mr. Whitby Ellsworth Street Address 10 Senexet Road' City Putnam State CT Zip Code 06260 Plant Name National Chromium Company, Inc. 

### " Plant Phone**Number~(8~6~O.l-) ~92=8=..;;.-7~9~6~S**  

### _________________ _ 

### Plant Contactlfitle,
________________________ _ Plant Address (if different than owner/operator's): Street Address,
___________________________ ___ City
_________________ __ Stare.
______________ _ Zip Code,
______ __ 2. Complete the following table. If additional lines are needed, make copies of this page.
Tank Type ofTank Applicable Type of Control Control Method to Test Method Type and Quantity 101# Emission Limit Technique System Dctcnnine Followed of HAP Emitted' 101# Compllancel ECI34 Hard Chrome 0.015 mgldscm CMPS ECI34 Puformance EPA MJ06 er"'0.0096 Test mgldscm
If 8 pertonnance test was conaucted, suomlt me test report containmg me elements requllC4 oy 4U**~r** K. 0,,-''I4(8J.

, If the compliance proccdUICS of 40 CFR 63.344(e) are being followed. aIIach the calculations needed to support the emission limit expressed in mg/hr. 

### 3. Complete the following table for each control technique used. If additional lines are needed, make copies of this page. Control System 10 1# Tank 10 I#(s) Range of slle'specific opmtlng parameter valuesl

EC·134 Pressure Drop Velocity Pressure Surface Tension Foam Blanket Thlekness EC·134 5.6 In w.C. NA NA NA :tl In.

If the applicable monitoring and reporting requirements to demonslrale continuous compliance differ &om those In 40 CFR Part 63. subpart N. attach D description. Parameter value ranges are established through Initial perfonnancc testing and are those that correspond to emissions at or below the level of the standard(s).

# I I I I 

# I I I 

# I 4. NOTIFICATION OF COMPLIANCE STATUS (Continued) Page 2 of3 Complete the following ifhard chromium electroplating tanks are opened (check the box(es) that apply):



# o

o

o The maximum cumulative potential rectifier capacity ofthe hard chromium electroplating tanks is greater than or equal to 60 million amp-hr/yr. This was detennined by taking the sum ofthe total installed rectifier capacity (amperes) multiplied by 8,400 hourslyr and by 0.7 for each' tank. The maximum cumulative potential rectifier capacity ofthe hard chromium electroplating tanks is less than 60 million amp-hr/yr. This 

### was determined by taking the 

### sum of the total installed rectifier· capacity (amperes) multiplied by 8,400 hourslyr and by 0.7 for each tank. Records show that the facility's previous 

### annual actual rectifier capacity of the hard chromium electroplating tanks was less than 60 million amp-yrlhr. If so, submit the records' that support this rectifier capacity for any 12-montlr period preceding the compliance date, or submit a description of how operations will change to meet this rectifier capacity limit. For new sources, the capacity can be that projected for the first 12-month period of tank operation. The facility has accepted or will accept a Federally-enforceable limit of 60 million amphr/yr. on the maximum cumulative potential rectifier capacity of the hard chromium electroplating tanks. 5. Check on of the following boxes that describes the facility's compliance status:

## ~ The facility is in compliance with the provisions of 40 CFR Part 63, subpart N. 

# o The facility is not 

### in compliance with the provisions of 40 CFR Part 63, subpart N. 6. Print or type the name and title of the Responsible Official' for the plant: Whitby K. Ellsworth President Name Title A Responsible Official can be:
• The president, vice-president, secretary, or treasurer of the company that owns the plant; • The owner of the plant; • The plant engineer or supervisor; • A government official if the plant is owned by the Federal, State, City or County government; or • A ranking military officer if the plant is located on a military base.

### NOTIFICATION OF COMPLIANCE STATUS (Continued) Page 3 of 3 I Certify That An Operation And Maintenance Plan Has Been Completed And The Plan And Other Work Practice St dards of 40 CFR 63.342(0 Are Being Followed. 

# I Date I Certify That The Information Contained In This Report Is Accurate And True To The Best Of My Knowledge.

Date

### Po lutant 

# - 

# - 

# -_ ... 

# -_ .......

Table B HazardousAir Pollutant Analysis National Chromium EC 

### -134
9.14 

# = Stack Height (m) 54.86 

### = 

### Property Une (m) 54.86 

### = XMAX

2.51 

### = VOl flow 

### (acm/s)

CAS No. 

### HLV Alternate Units: 30 

### = Stack Height 

### (ft) 180 = 

### Property Une 

### (ft) 5 1 315 

### = Flow 

### (acfm)

TableSummary of He x Chrom e T es t Re s ults



# I National Chromium Comp a ny, Inc . Putnam , Connecticut 

# I RUN NO. : M306 -0- 11 M306-0-12 M306-0-q AVERAGE DATE : 1 2113/96 12 1 13/96 1 2113/96 TIM E: 0807 - 1 020 1 1 02-1308 134 1 -1546 

# I IN PUT S PBAR, ( ' Hg) 29.90 29.90 29
.90 29.9 STACK AREA, (f1') 1 .230 1 .230 1.230 1 .2 

# I NOZZLE DIA
.. (inches) 0
. 187 0. 187 0
. 187 0 . 187 TOTAL TI M E , (minutes) 120 1 20 120 1 20 CA LIBRATIO N FACTOR 1 . 003 1 .00 3 1 .00 3 1 .0030 

# I PITOT COEFFICIENT 0
. 84 0
. 84 0.84 0
. 84 SO
. RT
. DELTA p, ('H,0) 1.3022 1.2390 1 .2580 1 .2664 DELTA H , ( ' H , O) 2.08 1 .9 1 1. 99 1
.99 METER TEMP ., ( ' F) 92 95 96 94 

# I STATIC PRESS
.. ( ' H , O) - 11. 00 -11 .00 -11.00 -11 .0 STACK TEMP
. , ( ' F) 66 61 60 · 62 METER VO LUME , 

### (ft') 98 .531 96.699 96 .377 97.202 TOTAL H , O VAPOR, (rill) 37
. 1 38
. 1 37.1 37 .4 CO , IN STACK GAS , (% ) 0
. 0 0.0 0 .0 0 .0 0 , I N STACK GAS
. (%) 20.9 20.9 20 .9 20
.9 CO IN S TACK GAS, (%) 0.0 0 .0 0.0 0
.0 N , IN STACK GAS , (%) 79.1 79.1 79.1 79 .1 C r " CATCH , (mg) 0
.0259 0.0260 0.0241 0.0253
OUTPUTS METER VOL. STD, (f1') 94
.95 92.64 92
. 18 93
.26 H , O IN STACK GAS, (%) 1
.81 1 .90 1.86 1 .85 STACK GAS MOLECULAR WT 28
.64 28.63 28.63 28.64 E XC E SS**'** (%) -118750.0 -1187 50.0 -118750.0 -118 2 50
.0 ' G K;G S E( ) 4458.07 4222.24 4282.55 320
.95 GAS FbOWRA, , Befm ) 5483 5193 5268 3 1S ST P FLOWRATE , ( dsefm) 5255 5020 5104 5126 ISOKINETIC, (%) 97
.2 99.2 97.1 97.B Cr'" CONC
. , (ug l .em) 9.23 1 E +oo 9.579 E +OO B.944E+00 9.252E+OO Cr+6 CONC . , (ug / dscm) 9.632 E +OO 9.910E+OO 9.23 1E +00 9.591 E +OO Cr '" CONC., (g rl .efj 4.034E-06 4.186E-06 3 .908E-06 4.043 E -06 Cr '" CONC
.. (grl dsefj 4.209E-06 4 .330 E- 06 4.034E-06 4.191E-06

.r EMI SSI O I'IRATE , ( 1 1!1llr ) 1
. B96E-04 1.B63E-04 1.765E-04 

# . ' lE ejs\a: \ 5219c134 .wk3 14-Jan-97 En vi ronmenta l Aisk Li m ited

• C ._EXAMPLE CAlCUlATIONS 

# I RUn No.: M306-0-11 Date: 12/13198 location: National ChromLimCompany, Inc. 

# I INPUTS EMISSION CALOJLA11ON SYMBOLS Pbar "" 29.90 -Barometric pressure, "Hg As '" 1.23 -Cross sec:llenal area of cl.Ict. square faot On 

# .. 0.187 -Nozzle DIameter, indies 

# I Ttot :: 120 - Total samplhg time, mhutes y 1.003 -Dry gas meter calibration factor Cp "" 0.84 -Pilot tube coeffi:lent. dlm_lenlass DPavg ::0 1.3022 -Averago
.. are root of velocity head, sqrt(" H2O) DHavg 2.08 -Average orifice pressure drop, "H2O 

# I Tmavg 92 -Average dry gas meter temperature, degrees F Psavg 

# .. -11 -Average duct static p,..sure, "H2O Tsavg 

# .. 68 -Average Stack Temperature, degrees F Vmtot Q 98.531 - Total meter sample vcWme, cubic feet 

# I V1+Vsg :: 37.1 - Total voume of liquid collectlld "CO2 :: 0.0 -Percent CO2 by VolUme (dry basis), " "02 

# .. 20.9 -Percent 02 by yclume (dry basis), " "CO 0.0 -Percent CO by voLime (dry bals), " 

# I "N2 "" 7&.1
- Percent N2 by volume (dry basis), " Mn 1:1 0.0259 - Total er+ 6 collected, mg Fuel Input 

### "H :: -Percent by weight of hydrogen In fuel "C -Percent by weight of carbcn In fuel 

### "8 -Percent by weight of sulfur h fuel "N 

# .. -Percent by weight of nHrogen In fuel 

# "0 Q -Percent by weight of oxygen In fuel GCV ::0 -Gross calorific value offuel, BTUJlb Tstd 

# .. 68 -Standard Temperature, degrees F Pstd 

### = 29.92 -Standard Pressure,**~g** Lp 

# .. -Frea/ Leak Rate of Samplhg Train, cfm La -Allowable Leak Rate d Sampling Train, cfm t. Volume d Sample Measured By Dry Gas Meter, Corrected to Standard Conditions 

### rim ltd)

.. Vmtotal x Y x Tstd + 460 x Pbar + DH§ £13.8 Tmavg + 460 Psld
98.531 x 1.003 x 68 + 460 x 29.& + 2.08£13.8 92 + 460 29.92 Vmsld= 94.&5 dscf
2. Molstlre Content at Duct Gas ("H20)

.. 0.04707 x (VI + Vsg'

Vm std + 0.04707 x (VI + Vsg)
0.04707 x 37.1 94.9498 + 0.04707 x 37.1 "H2O
.. 1.81 "

ejs\a:\M308caIc.wk3 14-Jan-&7 environmental Risk Umited

# JI I I II I I 3. Molecular Weight of Stack GAS (MWa)

.. {( 0.44 X "C02) + (0.28 l( 

## =

{( 0.44 X 0.0 ) + (0.28 X MWs EO 28.64 Ibllb molo

4. AI/Vage Ouct Gas Density (0"

.. 0.0458 X MWs

=0.0458 X 28.6403 Ost
.. 0.073 Iba I cubic 1eot %CO ) + (0.28 l( "N2 ) + (0.32 X 0.0 ) + (0.28 X 79.1) + (0.32 l(

X Pbar + ( Ps avg l13.8) Taavg + 480 X 29.9 + ( -11 l13.8) 88 + 480 'J(,02 )} X (1

- "H2O) + (0.18 X "H20) 100 2O.9)} X (1 -....!.:!!J + (0.18 X 1.806) 100



# I 5. Excess Air (EA) 

# I I 

# , .. 100 0.284

a 100 0.284
EA '" -118750"
8. Average Duct Velocity (Vs)


### = 5129.4 X

'" 5129.4 X x X
X X

Cp

0.84 Va.. 4458.1 1tImin

7. OUctVCllumetrb Fbw Rate, (a) Vs X

.. 4458.07 x A.. 5483 acfm

o;S\a:\M308cIllc.wk3 ( 0.5 X "CO ) ( %02

- (0.5 X "CO)) 20.9 - ( O.S X 0 ) 79.1 - ( 20.9

- (0.5 X 

## 0»

X OPavg l( SORT { Ts avg + 460 } ( P b. + Ps avg /13.6) l( MW

X 1.302 x SORT { 88+460 } 29.9 + -11 /13.6} X 28.8

1.23

14-Jan-97 Environmental Risk Umhd8. Cuct VofumeCri: Fbw RIa, Ccmcted to Dry S1IIndarct Condlllons, (Osta)

=> Q x (1

- .. H20 I x (",T8::.:tet=-_..,.:+
...**48~O;,....o)** X (
.... P-=b""
........-:-:-+:--.:..P..:S-=II
.. 1tIS

.......

/:,:13

.....8:.-..J 100 Ts avg + 480 P std
5483.43 x (1

- Qstet a 5255 dscfm

9. lsokincrtfc Fc1cr.**~)** 1.80598 I X 100 88 + 480 I x (_-=29:,:.::::,9.......,...;;+-=-
__ -..,.:1:,:.1..1./,!;13:,: • .:::.6--J 66 + 480 29.92**::::~**_________**~~**___**~**___**..:5~.87~=X~rn..:s..:eN** ..

g __**~+~~~~x**____**V~m~s=td~~~~**___**~~~~~~** ( P b. + Ps eNg ) X Vs X Ttot X (1 - "H20) X ( Dn '2 X 0.7854 ) 13.8 100 144

=> ______**~----------~----..:5~.87~~x~(--...:66~-+-480~~)~X~--~~94~.~95:.-~~~**____**~~~~~~** 29.9 + __**':':-~1,~)** X 4458.1 X 120 X (1

- 1.808 ) X 0.03 X 0.7854 ) 13.8 100 144 I=> 97.2"

1 O. Actual Conc:entraIfon, grains/acf, (C) 0.01543 x Mn X (TStd + 480) X (P b. + PSeNS X (1 

## - "H2O) 13.8 100 Vm stet X (Ts eNg + 480) X Pstct a _________**~~~~----~~--** __**--~~--~~~-** __**-----~~---**

0.01543 X 0.0259 X (88 + 460) X ( 29.9 + -11 X (1 

## - 1.808 ) 13.6 100 94.9498 X ( 66 + 460) X 29.92**::::----------.......,~~~--~---'="-~~-~--~~~---------~:.----** C :::: 4.03E-08 grans/act

10&. Actual CCl'lContrstlcn bead en stack ccndlllcns, uglacm. (C t ) 1000 X Mn X (Tstd + 460) X (P b. + PlleNg X (1 

## - .. H20 ) :::: 13.8 100 0.02832 Vmstd X ( Tsavg + 480) X P Std
1000 x 0.0259 X (88 + 480) X ( 29.9 + -11 X (1 

# - 1.808 ) :::: 13.8 100 0.02832 94.9498 X ( 68 + 480) X 29.92 C , :r 9.23 ug/acm

ejJ\a:\M306calc.wk3 14-Jan-97 EnvIronmen1al RIsk Umled

# • 

# I 

# I 

# I I 

# I I 

# I I I I I 

# I I 11. eaicenfratlOn, ComIcted ID Dry Standard CondItIoN, (Ca) '" 0.01543 x

'" 0.01543 x

Cs'" 4.21E-06 grJd&ef
12. Emiiak:n Ru, (ER)
'" 0.008S71 x '" 0.008S71 x ER", 1.90E-04 /bsJhr

ep\a:\M306ca/c wk3 Mn Vmstd

0.0259 94.9498

Cs x 4.21E-08 ic Qstd
52SS.1

14-Jan-97 Envircnmen1al RIsk Umllltd

# I 

# I I I 

# I I I I t TEST OF TANKS EC 1, 3, AND 4 COMPOSITE MESH PAD CONTROL DEVICE DECEMBER 13, 1996 

### RECORD OF TANK Ee

- 

# 1 .;.- 

### COMPOSITE MESH TANK TIME ' VOLTAGE AMPERAGE PAD 

### DBLTA P TEMP " STAGES 1 .THRU • 4:--_..:..'_ ttl .,; 

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# -----------------------------------------------------------------------------**FILENAM~:** 

### EPATEST1 Decembe= 13, 1996, 8:18 AM

# ·1 

# I TEST OF TANKS EC 1, 3, AND 4 COMPOSITE MESH PAD CONTROL DEVICE DECEMBER 13, 

### 1996 

# I RECORD 'OF TANK EC 

# -3 COMPOSITE MESH TANK 

# I 

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### TEMP '. 

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AVERAGE FILENAME: EPATEST1 December 13, 1996, 8:18 AM

### •



# I TEST OF TANKS EC 1, 3, AND 4 COMPOSITE MESH PAD CONTROL DEVICE 

# I DECEMBER 13, 1996 

# I RECORD OF TANK EC

-

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## • STAGES 1 

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### 1996, 8:18 

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### n , i'; Jj./13/96 

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### IN SQUARE FEE! VELOCITY ACROSS ROUND IINRE CONTROL PADS

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# I TEST CONTROL DATA FOR TESTING OF EC-134 OK DEC 13, 1996 SAltPlIHG SITE 

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. VELOCITY ACROSS ROUND 

### KINRE COITAOL PADS

- FP"**.~.**



### TEST RUN RECTIfiER VOLTAGE AREA 

### or RECTANGULAR ACS CONTROL PADS IN SQUARE FEET TANK TEHPERATURE VELOCITY ACROSS SQUARE ACS COHTROl PADS

- fPH



# ......**~:.:~OlNGS** 

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### Of READING 

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# ,l1 dP-lst STAGE 

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# ·1 t**~",-** 

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## or CONTROL DEY 

## '2.,( 

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## ")~ dP-3rd STAGE Of CONTROL DEY

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# - d -4th 

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### STAGE Of CONTROL DEY d -4th 

### STAGE Of CONTROL DEV 

# ,**17~** 

# 5
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### ~.3 

## ,.. dP-CDltPlETE CONTROL OEVICE dP-COltPLETE CONTROL DEVICE 

## t;", ,/-Z) dP

- HOOD AND CONTROL DEVICE , 

### 0, 

# B dP

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# 10. '0 dP

- HOOD AND CONTROL DEVICE 

# I 0 

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### PSI AIR PRESSURE OM WILDEH PUHP. WASHOO.! LIQUID BEING USED IS FIRST CHROltE RINSE, CONTINUOUSLY RE-CIRCULATED.

fILE: AIRTEST/TESTOOCS/TSTECIJ4 Deceiber 13, 1996, 8:58 

### Alt

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## J? 

## Y (."1 PROBE 10 NO.
__ """+._C""l/
___ _ fILTER ID 1110. NA 

# --......**~!""----** fiLTER TARE UT. 

### A/A NOZZLE NO./DIA.Cln.) :: •. 

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TRAVERSE SAMPLE CLOCK

POINT TIME TIME (_In) (hours)



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20 COLLECTED 10 _l. S. G. "EIGHT 

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... ' I fiLTER 10 10.**~'~** fiLTER TARE WT.**'V·~** NOZZlE NO./DIA.(ln.) S
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# ,,- Date:

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## 91c Bar. Ps., (Pb): 

### 3'L·S,Q in. Hg

Standard Merer Moctale Velum. 

### Temp. Pressure Oritice 

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### (·(,,=--9 

## fDf' 

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For 

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## 1 (Tm 

### + 460) 

### V. 

## Va

Q Q
OrtIce factor 

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### + AH ) (T. 

### + 460) 13.8 (0.0317) AH Pb (tm 

### + 460)

V (17.64) Vm [(f. 

### + 460) AH ( Pb ((Is 

### + 460) @ 

### P (VI VIJa (pb 

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### + 460) @ 

## .J¥a**I~ ~**  ) . 

# ......,., UalhociS Module Calibration

ModJJe#: 

## 1399 Std. Meter: 51<>4IS 

### P,.-tat 

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Moctale Meter Velume 

### Temperatures 

# nme Mowle

Vm 1mI bno @ AHa Ftowrata (ft3) (Of) f'F) (arin) Y (In. H2O) Q



## . {SCFMl OF 5 144 

# r4 7'1 

### IcJ. OJ3 J. 0010 llDl 10.411
.. ) 30t>h9 5" Jlb9 

### i>w 

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### •CfCJ70 I 

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### 7-9 14.9513 10 ;)101 1(')**~4** I_O,.""h}S



## .'**~** 

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### ?3 10
. 

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### /. to't_ 

# I:: AcceptMce Cdterla: Conelation Una Equalion Q GI 

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### + b Each V 

### nustbe 1.00 

# = 0.01 AverageAtial1'llltbe 1.84 % 0.25 EadlAHa l11li1 be 

### wbhIn 0.15 

### ofthe 

### awnageAHa 

# [1;1 

# l::fl**U;-~a.kl** . D.OOO 

## I

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### OK: MocUe Cleaned: 

# SF Ppot Tube ManometIr LMk 

### Check: 1&,0443 7. 4J• .J9



### CaIibratad

## ~d 

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# J"€C. Date: 

### 7- ot3 - 

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- 

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...... 1'",...- 

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..... "' 

## t. <;-,.t In. Hg 

# .
Standard Meter Moctde Volume Temp. P
.... 

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### rFl (In. H2O) 

### (In. H2O)

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## + AH ) (Ta 

### + 460 ) 

### 13.6 

### AHa
.. (0.03171 

### AH ((Is 

### + 460) @ 

### )2 Pb (1m 

### + 460) 

### ( V. Va 

### p (pb 

## + AH ) Q 

## • Y (17.64) Vm 13.6 (bn 

## + 460) @ 

### Oritc. factor 

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# -- Method 5 Moclile Calibration

ModIle 

### #:**J.~~'i** 

## i Std. Meter:**F~**

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Vm tmI 

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# as 8. Cia**~wraa** 

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# I~ tmo If 

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.. geAHa
.... 

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.... 

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## or ..

... ge6Ha



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### Heater LoveCantrd 0(:--- MoclIIe CIeIned: 

## \7, PIlot Tube 

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### \7' OF



### CeUbrated and Checked 

## by: L 

# tIc>. Data:

### /~.:r~"" 

### "f R..tewadby:

## 6~=<**~** Data:

## /~Jd'\ 97-

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# , , I I

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S. ·S-TYPE PITOT GEOMETRIC CALIBRATION PART 1

- PROBE CONFIGURAiION

## ~Identif1caticn**_~_i1_/** __ _ Pi tat Ident; fi 

### c:a 

### tion 

# _V4_"_r
__ _ iechnicat Specialfst**~~"** 

## Date

## ~~
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# ) 

# ..**~** Probe l Nozzle 

### J: r- 

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### Specifications (EPA Method 2) 

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## B.



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# - d D D • .,'" If 

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# = L:!!s-.
6 

# = 91.-s- 

# - e ·

# ='1/, 

### I



# --- TECHNICIAN:

### ~~ OATE: 

# 11'46

a 2 +d 2 

### -e 2

------**~COS8'** 

### 2ad ( 80°<8<100°) (80"(8'(100")



## a 2 +b 2 

## -c 2 

### 2ab DeOSe


### a 2 +d 2 

### -e 2 

### 2ad =cos8' (85°<6<95") (85°<6'<95°)



### D. (9 

## < 1J32? 

## !'IToT 

# Coo'O NOTE: Values In parentheses are EPA Method 2 specIfications.

# ,I .. 

# I I I 

# I I I I I 

# I TABLE OF CONTENTS QUANTERRA PROJECT NUMBER 091103
Case Narrative' Quanterra's Quality 

### Assurance Program Sample Description Information Chain of Custody Documentation 

# fLhanter-'" Enviroament1J/ Services**Hexava1en~** 

### Chromium by Ion Chromatography (with PCR)

- Method EPA 306 

### Includes Samples: 1 through 4' Sample Data Sheets Method Blank Report Laboratory QC Reports

# . .. 

# .**~IX** SPIKE/MATRIX SPIKE DUPLICATE QC REPORT : Chemistry Analysis and Preparation ,'oject: 091103 lJegory: CRS-IC-AIR Ion Chromatography Inorganics ")t : 

### CRS-IC-30S-AIR ttrix : AQUEOUS IIPulen : 091103-0001 

## PlR : 09 JAN 97-JA Dlts : ug/sampl e



## ., ---------Concentrat 1 on--------- ocnalyte

.:omium, 

## ,exavalent 

# , I 

# I . Sample Result

25.9 MS" Result 45.3 MSD Result 45.2 'Method: EPA 30S 

# fI.)".n'.rr. EnviiolJlDentll/ Services



### Amount Spiked MS MSD Acceptance %Recovery %RPD Limit MS MSD Recov. RPD 19.9 " 19.9 97 97 0.22 85-115 15

culations are performed before rounding to avoid round-off errors in calculated results.

# ,. EPA Method 1 Sample and Velocity Travera for**Statlo~ary** 

### Sources' 

## Fi rm NatiO'lal 

## O'Ironiun Tota 1 

## Traverse Poi nts Requ1 red 12 

# j location Et - 134 LIne 

## Number of 'Ports 2 

## Diameters Upstream**_--;:5;.;.;.O~**

### __ 

## Points Per Port 6 

## Diameters Downstream 15.0 

## Traverse ( Horizontal 

## or Vertical) &fth



## 'MINIMUM NUMBER OF TRAVERSE POINTS FOR PARTICULATE AND NONPARTICULATE TRAVERSES 

# . 1+--15"**-~** 

## Duct Diameters Upstream from Flow Disturbance

# ~ 0.5
.....::.... ·1.0
..

# (Dist:~;e A) 2.0**~** 

### 50 

# I 14 PARTICULATE
18 1. 

# ---l--------------. 12 

# '-**.--------~--------~** NONPARTICULATE 8 or • STACK D&AMI'R"-"" TO o.n •**I'~ZC** W 

# ·1

... 

# ". 

# 1 

# 1 D • 

## lli.=

eq 

### L+W'-- 

## Sample Port

.'Z25"

# °2~--~--~~--~--~----~--~----~--1~O r--- __

# ----------------~ Duct Diameters Downstream from Flow Disturbance CROSS-SECTIONAL LAYOUT (Distance 8)**FORT:~;r~GULAR** 

## STACKS Traverse Points' LOCATION OF TRAVERSE POINTS IN CIRCULAR STACKS 9 Matrix 3x3· 4x3 

## 4x4 5x4 5x5 Point {Percent of stack diameter from Number inside wall to traverse point}

On A Number Of Traverse Points On A Diameter Diameter 4 

## 6 8 

### 10 12 1 6.7 4.4 3.2 2.6 2.1 2 25.0 14.6 10.5 8.2 

## 6.7 3 75.0 29.6 19.4' 14.6 11.8 

### 4 93.3 70.4 32.3 22.6 17.7 5 

### 85.4 61.7 34.2 25.0 6 95.6 80.6 65.8 35.6 7 

### 89.5 77.4 64.4 8 

### 96.8 85.4 75.0 9 

### 91.8 82.3 10 97.4 88.2 11 

### 93.3 12 91.9 

## No. 1 

### 2 3 

### 4 

### 5 6 

### 7 

### 8 9 

### 10 11 

## 12 12 16 

### 20 

### 25 

## 'TRAVERSE POINT LOCATIONS Distance NipP'e . Tota' From Wa" Size Distance 0.7 2.2 

### 4.4 10.6 12.8 14.3



# - 

# - o 

# t

3 

## 9



# ....

# I 

# I LABORATORY CONTROL SAMPLE REPORT

. Wet Chemistry Analysis and Preparation

Project: 091103 

# J, Category: CR6-IC-AIR Ion Chromatography Test: CR6-IC-306-AIR 

# I Matrix: AQUEOUS QC Lot: 09 JAN 97-JX Concentration Units: ug/sample 

# I Analyte 

# I Chromium, Hexavalent

.,.. 

# I t Inorganics QC Run: 09 JAN 97-J Concentration Spiked Measured 2.50 2.57 

### Accuracy(%) LCS Limits

103 85-115

Calculations are performed before rounding to avoid round-off errors in calculated results.

# ·, I ,. 

## .. 

# .

METHOD BLANK REPORT lIet Chemistry Analysis ""roject: 091103

# ~est: CR6-IC-306-AIR

, ethOd: EPA 306 atrix: AQUEOUS Clot: 09 JAN 97-JX

# ~nalYte .Chromium. Hexavalent



# - I I

NO 

## = Not Detected and Preparation

. Hexavalent Chromium by Ion Chromatography (with PCR) QC Run: 09 JAN 97-J Result Units NO ug/sample Reporting Limit 0.50

# , I

,



### ' QC LOT ASS IGNMENT REPORT

- MS QC

.. Wet Chemistry Analysis and Preparation

Laboratory 

# J Sampl e Number 091103-0001-MS 091103-0001-SA
, 091103-0001-S0

. 091103-0002-SA

091103-0003-SA
, 091103-0004-SA 

# I I 

# I QC Matrix AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS QC Category CR6-IC-AIR CR6-IC-AIR CR6-IC-AIR**CR6-IC~AIR** 

### CR6-IC-AIR CR6-IC-AIR QC Lot Number (OCS) 09 JAN 97-JX 09 JAN 97-JX 09 JAN 97-JX 09 JAN 97-JX 09 JAN 97-JX 09 JAN 97-JX 

## . 

# fI.»'aD'.rra**~** Services



### QC Run Number
. MS QC Run Number (SCS/BLANK/LCS) (SA,MS,SD,DU) 09 JAN 97-J 09 JAN 97-JA 09 JAN 97-J 09 JAN 97-JA 09 JAN 97-J 09 JAN 97-JA 09 JAN 97-J 09 JAN 97-JA 09 JAN 97-J 09 JAN 97-JA 09 JAN 97-J 09 JAN 97-JA

# .1 

# I· 

# 'I I I I. ". 

# I I ,**~.** 

# -**Q)"anter~a** £nvininmental Services 

### Hexavalent Chromium by Ion Chromatography (with PCR) Client Name: Client 10: Lab 10: Matrix: Authorized: Environmental Risk Limited M306-0-B2 091103-0004-SA AIRTRAIN 18 DEC 96 Sampled: 13 DEC 96 Received: 18 DEC 96 Prepared: See Below Analyzed: See Below Parameter Result Reporting Analytical Prepared Analyzed Units limit Method Date Date Chromium, Hexavalent NO

NO Q 

### Not detected NA D 

### Not applicable ug/sample 0.36 EPA 306 NA

Reported By: Lori Ann Upton Approved By: Josefina Jones The cover letter is an integral part of this report. Rev 230787 09 JAN 97

# - I Hexavalent Chromium by Ion Chromatography (with PCR) 

# fI.,))uanterra EnvirolUDeDtU Services 

# I Client Name: Client 10: Lab 10: 

### Environmental Risk Limited M306-0-13 091103-0003-SA AIRTRAIN Matrix: Sampled: 13 DEC 96 Received: 18 DEC 96 

# I Authori zed: 18 DEC 96 Prepared: See Below Analyzed: See Below Reporting Analytical Prepared Analyzed



# - I I I I I Parameter Result Units Limit Method Date Date Chromium, Hexavalent 24.1 ug/sample 5.2 

### EPA 306

Note R : Raised reporting limit(s) due to high analyte level(s). NO 

## = Not detected NA 

## = Not applicable NA

Reported By: Lori Ann Upton Approved By: Josefina Jones 

## , , The cover letter is an integral part of this report. Rev 230787 09 JAN 97 R

# · , 

### Hexavalent Chromium by Ion Chromatography (with PCR) 

# fLA.anterr. Environment:J1 Services



### ,. Client Name: Client 10: lab 10: 

### Environmental Risk Limited M306-0-12 091103-0002-SA AIRTRAIN Matrix: 

# I Authori zed: 18 

### DEC 96 Sampled: 13 DEC 96 

### Received: 18 

### DEC 96 

### Prepared: See Below Analyzed: See Below 

# I 

# , I I Parameter Result Units Reporting Analytical Prepared Analyzed Limit Method Date Date Chromium, Hexavalent 26.0 ugfsample 5.3 

### EPA 306

Note R : Raised reporting limit(s) due to high analyte level(s). NO 

## = Not detected NA 

## = Not applicable NA

Reported By: Lori Ann Upton Approved By: Josefina Jones The cover letter is an integral part of this report. Rev 230787 09 

### JAN 97 R

# t I 

# I '" #. • 3.3 

### Summary of Results 

### The average**Cr~** 

### concentration was 

### 0.0096 milligrams per dry 

### standard cubic meter (mgldscm). 

### All test 

### results are well below the USEPA emission 

### llinit of0.015 mgldscm. Table 3-2 summarizes the' test results and compares the maximum allowable stack concentration (MASC) to 

### the**ac~** 

### stack concentration (ASC).

TABLE 3-2



# . Summary of Emfssioa Results

. Nadoaal CIaromiam CompaDY, IDe. ElectropJaUaa LID. EC-134 BeuvaJeat CIIromiam Test Program Pumam, Coaaectlc:ut Uaits Method/Component \ DATE: TIME:



# . Method 2 - Flow dsctin actin Ml06· Cr'" mgfdscm IbIhr MASC pg/acm 

### ASe pg/acm dscfin • dry standard cubic feet per minute acfin

- actUal cubic feet per minute Raa 1 12113196 0807-1020**525~** 5483 0.0096 1.901:-04

mgldscm

- milligrams per dry standard cubic meter Iblbr - pounds per hour "g/acm

- micrograms per actual cubic meter Raul 12113/96 1102-1308 5020 5193 0.0099 1.861:-04 

# .
Raa3 Average 12113196 1341-1546 5104 5126 5268 5315 0.0092 0.0096 1.17E-04 1.841:-04 48 9.3



### The hazardous air 

### pollutant analysis (Appendix B) pertains to 

### the CTDEP'air regulations. As 

### indicated, the average actual stack concentration is 

### 18.5% ofthe allowable**Cr~** 

### concentration and clearly demonstrates compliance.


# ..

S219c134.rpt 

### 6 January 1997