### Name: Jim Burke

Title: IC&E Supervisor Company: Schuylkill Energy Resources Sign Date: 9/2/2010 Name: Stephen Schell Title: President Company: Air Analysis, LLC Sign Date: 9/2/2010 Permitted Facility Representative / Date Testing Company Representative / Date 

## Schuylkill Energy Resources - ICR

Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

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### Schuylkill Energy Resources - ICR 9/2/2010 Facility Information: St. Nicholas Cogen Project P.O. Box 112

Shenandoah PA, 17976 Contact: Jim Burke Phone: 570-462-2822 ext 12 Fax: 570-462-3244 Email: cemser@verizon.net Testing Company: Analysis, LLC 189 Hausman Road

Lenhartsville PA 19534 Contact: Stephen Schell Phone: 610-756-3490 Fax: 610-756-3491 Email: sschell@hughes.net

Air Permit Number: 54-00003 Permitted Source ID/Name: CFB Unit ID 1 Permitted Maximum Process Rate: N/A Max. Normal Operation Process Rate: 825 klbs/hr steam Target Process Test Rate 90% of maximum load

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: St. Nicholas Cogeneration Plant operates a circulating fluidized bed (CFB) boiler firing crushed anthracite culm to produce steam and generate electricity. The boiler is manufactured by Combustion Engineering, Inc. and is rated at 825 klbs.hr steam flow at full load. Emission controls on the unit consist of limestone injection into the bed material to control sulfur dioxide emissions and a Combustion Engineering, Inc. Baghouse connected in seies to control particulate emissions Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: FRS #: 110030903164

SCC / Description 10102018 External Combustion Boilers - Electric Generation - Waste Coal - Circulating Fluidized Bed Combustion
The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width Exhaust Duct 0 144 240 1 114.59 3 99 136 Stack Exit 156 2172 1620 2 156 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location Carbon Monoxide Method 10 3 120 0 Exhaust Duct Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Exhaust Duct

Co2 Method 3A CO2 3 0 Exhaust Duct O2 Method 3A O2 3 120 0 Exhaust Duct 

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### Schuylkill Energy Resources - ICR 9/2/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. A teflon lined probe will be used for the determination of Formaldehyde emissions. This is due to only two test ports being available on a 165 inch diameter stack.

% H2O Method 1 - 4 3 120 0 Stack Exit Formaldehyde Method 0011 3 120 0 Stack Exit



### Wednesday, February 02, 2011 Page 3 of 9

### Schuylkill Energy Resources - ICR 9/2/2010 Sampling / Stack Data Results Summary 

### Location Exhaust Duct - Method 10 Average Run Number 1 2 3 Test Date 4/15/2010 4/15/2010 4/15/2010 Run Start Time 9:10:00 AM 12:40:00 PM 3:35:00 PM

Run Finish Time 11:09:00 AM 2:39:00 PM 5:34:00 PM Carbon Dioxide, % 15.17 15.25 15.23 15.217 Oxygen, % 5.24 5.07 5.15 5.153 Dry Volumetric Flow Rate, dry scfm 350130 346013 337201 344,448.000 F-Factor, dscfm/MMBtu @ %O2 10100 10100 10100 10,100.000 Moisture, % 7.46 7.68 7.04 7.393 Fuel Type Coal - Anthracite Coal -

Anthracite Coal -

Anthracite Fw 10540 10540 10540 10,540.000 Fc 1970 1970 1970 1,970.000



### Location Exhaust Duct - Method 25A Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type Fw Fc



### Wednesday, February 02, 2011 Page 4 of 9

### Schuylkill Energy Resources - ICR 9/2/2010 Emissions Summary

Process Run Data 

### Location: Exhaust Duct - Method 10 Compound: Carbon Monoxide Average Run 1 2 3 lb/mmBtuO2 3.67E-02 3.60E-02 3.64E-02 0.036 ppm 3.75E+01 3.72E+01 3.73E+01 37.333 ppm@7%O2 3.33E+01 3.27E+01 3.29E+01 32.967


### Location: Exhaust Duct - Method 25A Compound: Total organic compounds (TOC) as Average Run 1 2 3 lb/mmBtuO2 1.35E-03 1.69E-03 1.50E-03 0.002 ppm 8.72E-01 1.11E+00 9.80E-01 0.987 ppm@7%O2 7.74E-01 9.75E-01 8.65E-01 0.871



### Wednesday, February 02, 2011 Page 5 of 9

### Schuylkill Energy Resources - ICR 9/2/2010 Process Run Data



### Run Name Value UOM Comments Target Value 1 Average Heat Input 1239 MMBtu/hr 0 

### 4 Average Heat Input 1244 MMBtu/hr 0 5 Average Heat Input 1264.8 MMBtu/hr 0 1 Steam Output 738 1000 lb steam/hr 0 

### 4 Steam Output 738 1000 lb steam/hr 0 5 Steam Output 740 1000 lb steam/hr 0 1 Flue Gas Flow Rate 2E+07 scfh 0 

### 4 Flue Gas Flow Rate 2E+07 scfh 0 5 Flue Gas Flow Rate 2E+07 scfh 0 1 Flue Gas Oxygen Content 5.3 % 0 

### 4 Flue Gas Oxygen Content 5.2 % 0 5 Flue Gas Oxygen Content 5.2 % 0 1 Flue Gas Carbon Dioxide Content 14.3 % 0 

### 4 Flue Gas Carbon Dioxide Content 14.4 % 0 5 Flue Gas Carbon Dioxide Content 14.4 % 0 1 Flue Gas Moisture Content 7.4 % 0 

### 4 Flue Gas Moisture Content 7.6 % 0 5 Flue Gas Moisture Content 7.9 % 0 1 Flue Gas Sampling Point Temperature 374.4 Deg F 0 

### 4 Flue Gas Sampling Point Temperature 377.1 Deg F 0 5 Flue Gas Sampling Point Temperature 359.7 Deg F 0 1 Flue Gas Pressure 0 atm 0 

### 4 Flue Gas Pressure 0 atm 0 5 Flue Gas Pressure 0 atm 0 

### 1 Standard Pressure 0 atm 0 4 Standard Pressure 0 atm 0 5 Standard Pressure 0 atm 0 

### 1 Standard Temperature 0 Deg F 0 4 Standard Temperature 0 Deg F 0 5 Standard Temperature 0 Deg F 0 

### 1 Unit Net Electric Generation 96.17 MWh 0 0 4 Unit Net Electric Generation 95.61 MWh M25A, M10 and M0011 Test Run No. 2 0

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### Schuylkill Energy Resources - ICR 9/2/2010

APCD Run Data

Process Lab Run Data 5 Unit Net Electric Generation 96.41 MWh M25A, M10 and M0011 Test Run No. 3 0

1 Anthracite Culm 291.15 1000 pph M25A, M10 ans M0011 Test Run No. 1 0

Run Name Value UOM Comments Target Value 1 BAGHOUSE 7 " H2O 0 2 BAGHOUSE 7 " H2O 0 

### 3 BAGHOUSE 7 " H2O 0 4 BAGHOUSE 0 " H2O 0 5 BAGHOUSE 0 " H2O 0 

### 1 DRY LIMESTONE INJECTION 8000 lbs./hr 0 2 DRY LIMESTONE INJECTION 8000 lbs./hr 0 3 DRY LIMESTONE INJECTION 8000 lbs./hr 0 

### 4 DRY LIMESTONE INJECTION 0 lbs./hr 0 5 DRY LIMESTONE INJECTION 0 lbs./hr 0 1 0 0 

### 2 0 0 3 0 0 4 0 0 

### 5 0 0

Run Name Value UOM Comments 1 Fuel Higher Heating Value 0 Btu/lb 2 Fuel Higher Heating Value 3810 Btu/lb 

### 3 Fuel Higher Heating Value 3788 Btu/lb 1 Ultimate/Proximate Analysis 0 2 Ultimate/Proximate Analysis 0 

### 3 Ultimate/Proximate Analysis 0

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### Schuylkill Energy Resources - ICR 9/2/2010 Sampling / Stack Data Results Detail 

### Location Exhaust Duct - Method 10 Average Run Number 1 2 3 Test Date 4/15/2010 4/15/2010 4/15/2010 Run Start Time 9:10:00 AM 12:40:00 PM 3:35:00 PM Run Finish Time 11:09:00 AM 2:39:00 PM 5:34:00 PM Carbon Dioxide, % 15.17 15.25 15.23 15.217 Oxygen, % 5.24 5.07 5.15 5.153 Fuel Factor 1.03 1.04 1.03 Dry Volumetric Flow Rate, dry scfm 350130 346013 337201 344,448.000 F-Factor, dscfm/MMBtu @ %O2 10100 10100 10100 10,100.000 Moisture, % 7.46 7.68 7.04 7.393 Analyzer Make Thermo Electron Thermo

Electron Thermo

Electron Analyzer Model 48C 48C 48C Analyzer Serial Number 48c-54732301 48C-54732- 301 48C-54732-

301 Operating Range 130 130 130 130.000 Operating Units ppm ppm ppm No. Readings/Avg. 60 60 60 60.000 Calibration Set 1 2 3 2.000 Calibration Pre Zero Cylinder ID CC-133012 CC-133012 CC-133012 Calibration Pre Zero Cylinder Instrument Response 0.28 0.41 0.41 0.367 Calibration Pre Zero Cylinder Bias 0.13 0 0.23 0.120 Calibration Pre Zero Cylinder Drift 0 0 0 0.000 Calibration Pre High Cylinder ID CC-91200 CC-91200 CC-91200 Calibration Pre High Cylinder Instrument Response 49.25 50 49.9 49.717 Calibration Pre High Cylinder Bias -0.12 0.28 0.38 0.180 Calibration Pre High Cylinder Drift 0 0 0 0.000 Calibration Post Zero Cylinder ID CC-133012 CC-133012 CC-133012 Calibration Post Zero Cylinder Instrument Response 0.54 0.41 0.4 0.450 Calibration Post Zero Cylinder Bias 0.33 0 0.22 0.183 Calibration Post Zero Cylinder Drift 0.2 0 0.01 0.070 Calibration Post High Cylinder ID CC-91200 CC-91200 CC-91200 Calibration Post High Cylinder Instrument Response 50.42 49.9 49.8 50.040 Calibration Post High Cylinder Bias 0.78 0.2 0.31 0.430 Calibration Post High Cylinder Drift 0.9 0.08 0.07 0.350 Cavg 37.7 37.46 37.56 37.573 Cavg Units ppmvd ppmvd ppmvd Cgas 37.4975 37.1697 37.3466 37.338 Cgas Units ppmvd ppmvd ppmvd Fuel Type Coal - Anthracite Coal -

Anthracite Coal -

Anthracite Fw 10540 10540 10540 10,540.000 Fc 1970 1970 1970 1,970.000 Cgasw 0 0 0 0.000 Cgasw Units



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### Schuylkill Energy Resources - ICR 9/2/2010 Location Exhaust Duct - Method 25A Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 9 of 9