# PREMANUFACTURE NOTIFICATION

TS-PR23MI
EPA SANITIZED COpy

July 25, 2006

I OJ



# LUBRIZOL METALWORKING ADDITIVES SPARTANBURG, SC

### PMN Page 1 ; Page 1 of 19 Form A roved. 

### U.S. 

### ENVIRONMENTAL PROTECTION AGENCY 

## AGENCY USE ONLY Dale ofrecelpt 

# PREMANUFACTURE NOTICE 05 JUL 3: prel 

# 12: 02 :S 

# COIT:pany Sanitized

i

# III!II:II!!IIHI

# H:Hli,

# II::II.IIHll 

# it "lll :' I (J n u () : I I; <1 HI in the Premanufacture Notice 

### GENERAL INSTRUCTIONS
• You mustprovide all information requestedinthis form to the extentthat it is known toorreasonably ascertainable by you. Make reasonable estimates ifyou do not have actual data. • Before youcomplete this form, you should read the "Instructions Manual for PremanufactureNotification" (the Instructions Manual is available from the Toxic Substances Control Act (TSCA) Information Service by calling 202-554-1404, or faxing 202-554-5603). • Ifa user fee has been remitted for this notice (40 CFR 700.45), indicate in the boxes above the TS-user fee identification numberyou have generated. Remember, your userfee lD numbermust also appear on your corresponding fee remittance, which is sent to EPA, Washington Financial Management Center (3303), P.O. 360399M, Pittsburgh, PA 15251-6399, Attn. TSCA User fee.
Part 1-GENERAL INFORMATION Vou must provide the currently correct Chemical Abstracts (CA) Name ofthe new chemical substance. even ifyou claim the identity as confidential. Vou may authorize another person to submit chemical identity information foryou, but your submission will not be complete and the review wiU not begin Wltil EPA receives this information. A letter in support ofyour submission should reference your TS userfee identification number. Vou must submit an original and two copies ofthis notice including all test data. Ifyou claimed any information as confidential, a single sanitized copy must also be submitted.
Part 11- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE ,fthere are scveral manufacrure, processing, oruse operations to be described in Part II, sections A and Bofthis notice, reproduce the sections as needed.

Part 111-LIST OF A ITACHMENTS Attach additional sheets ifthere is not enough space to answeraquestion fully. Label each continuation sheet with the corresponding section heading. In Part III, list these attachments, any test data or other data and any optional information included in the notice.

OPTIONAL INFORMATION Vou may include any information that you want EPA to consider in evaluating the new substance. On page 11 ofthis form, space has been provided furyou to deseribe pollution prevention and recycling information you may have regarding the new substance. So-called "binding" boxes are included throughoutthis form for you to indicate your willingness to be bound to certain statements you make in this section, such as usc, production volume. protective equipment.. This option is intended to reduce delays that routinely accompany the development ofconsent orders or Significant New Use Rules. Except in the case ofexemption applications (such as TMEA, LYE, LOREX) where ecrtain information provided in such notification is binding on the submitterwhen thc Agency approves the exemption application, chccking abioding box in this notice does not by itselfprohibit the submitter from laterdeviating from the information (except chemical identity) reported in the furm.
CONFIDENTIALITV CLAIMS Vou may claim any information in this notice as confidential. To assert a claim on the form. mark (X) the confidential box nextto the information that you claim as confidential. To assert aclaim in an attachment, eirele orbracket the information you claim as confidential. Ifyou claim information in the notices as confidential. you must also provide a sanitized version ofthe notice (including attachments). Foradditional instructions on claiming information as confidential. read the Instructions Manual. Mark (x) ifany information in this notice is elaimed as confidential. TEST DATA AND OTHER DATA You arerequired to submit all test data in your possession orcontrol and to provide a description ofall other dataknown to or reasonably ascertainable by you. ifthese data are related to the health and environmental effects on the manufacture. processing. distribution in commerce, use, or disposal ofthe new chemical substance. Standard literature citations may be submitted for data in the open scientific literature. Complete test data (written in English). not summaries ofdata, must be submitted ifthey do not appear in the open literature. You should clearly identify whether test data is on the substance oron an analog. Also, the chemical composition ofthe tested material should be characterized. Following are examples oftest data and otherdata. Data should be submitted according to the requirements of§nO.50ofthe Premanufacture Notification Rule (40 CFR Part nO).

Test Data (Check Below any included in this notice) Environmental fate data 

# o Ves Otherdata 

# 0 Ves Health effects data 

# o Ves Risk assessments 

# 0 Environmental effects data 

# 0 Ves Structure/activity relationshiPSO Physical/Chemical Properties' Ves Test data not in the possession 

# 0 orcontrol ofthe submitter

# 0

• Aphysical and chemical properties worksheet is located on the Illstpage olllllis form. C·--· TVPE OF NOTICE (Cbeck Only One) 

# o PMN (Prernanufacture Notice) 

# o INTERMEDIATE PMN (submitted in sequence with final product PMN). 

# o SNUN (Significant New Use Notice) 

# o TMEA (Test Marketing Exemption Application) 

## w LVE (Low Volume Exemption) @40 CFR 723.5O(c)(l) 

# D w 

# o LOREX (Low ReleaselLow Exposure Exemption) @ 40 CFR 723.5O(c)(2) L VE Modification WREX Modification 

# o o IS THIS ACONSOLIDATED PMN? Ves 

# D 1 # ofchemicals or polymers Prenotice CommWlication II
EPA FORM 7710-25 (Rev. 5-95) Replaces previous editions ofEPA Form 7710-25. 

# 181The accuracy ofthe statementsyou make in tbis notice sbould reflect your best prediction oftbe anticipated facts regarding the cbemlcal substance described berein. An knowln and willful mi.lnte rotation is sub'cct to criminal enal orlzed (Original Signature Required) 

# '-" J,,,I t'Pllltl,'d;1

# r~ 

# N1't

, 'I' ' PMN 

### Page 2 ; Page 2 of 19 Public reporting burden for this collection ofinformation is estimated to average 110 hours perresponse, including time for reviewing instructions, searching existing data sources, gathering and maintaining the data needed, and completing and reviewing the collection of information. Sendcomments regarding the burden estimate or any other aspect ofthis collection ofinformation, including suggestions for reducing this burden, to Director, Collection Strategies Division (2822), U.S. Environmental Protection Agency, 1200 Pennsylvania Ave., N.W., Washington, D.C. 20460; and to the Office ofManagement and Budget, Paperwork Reduction Act (2070-0012), Washington, D.C. 20503. 

## CERTIFICATION

- A Printed copy ofthis signature page. with original signature. must be submitted 

### I certify that to the best ofmy knowledge and belief: 1. The company named in Part I, section A, subsection 1 a ofthis notice fonn intends to manufacture orimport for a commercial purpose, other than in small quantities solely for research and development, the substance identified in Part 

### I, Section 

### B. 2. All infonnation provided in this notice is complete and truthful 

### as ofthe date ofsubmission. 3. I am submitting with this notice all test data in mypossession or control and a description ofall other data known to or reasonably ascertainable by me as required by §720.50 ofthe Premanufacture Notification Rule.
Additional Certification Statements: Ifyou are submitting a PMN, Intennediate PMN, Consolidated PMN, or SNUN, checkthe following userfee certification statement that applies: The Company named in Part I, Section A has remitted the fee of$2500 specified in 40 CFR700.45(b), or 

# D The Company named in Part I, Section A 

### has remitted the fee of$1000 for an Intennediate PMN (defined @ 

### 40 CFR 700.43) in accordance with 40 CFR700.45(b), or 

# o The Company named in Part I Section A 

### is a small business concern under 40 CFR 700.43 and has remitted a fee of$100 in accordance with 40 CFR 700.45(b). Ifyou are submitting a low volume exemption (L

### VE) application in accordance with 40 CFR723.50(c)(1) or a Low release and low exposure exemption (LoRex) application in accordance with 40 CFR723.50(c)(2), check the following certification statements: 

# o The manufacturer submitting this notice intends to manufacture orimport the new chemical substance for commercial purposes, other than in small quantities solely for research and development, under the tenns of40 CFR723.50. 

# oThe manufacturer is familiar with the tenns ofthis section and will comply with those terms; and 

# oThe new chemical substance for which the notice is submitted meets all applicable exemption conditions. 

# o Ifthis application is for an LVE in accordance with 40 CFR723.50(c)(1), the manufacturer intends to commence manufacture ofthe exempted substance for commercialpurposes within 1yearofthe date ofthe expiration ofthe 30 day review period.

unuantto 18 

### usc 1001. Confidential Date July 25, 2006 

## '111'5 

# D Date 

# D

EPA FORM 7710-25 (Rev. 5-95) Page 2____ 

### PMN Page 3 ; Page 3 

### of 

### 19
Confidential


### , Person Position Global Compliance Manager 

# D

-----1......­

_____

Telephone (include area code)
Ifyou are submitting this notice 

### as part ofajoint submission, mark (X) this box.

_____________________....,..

2. Contact (in U.s.) Name Philip R. Miller Company Lubrizol Metalworking Additives and street) 110 Corporate Drive, Suite C City, State Telephone (include country or area code)
Position Global Compliance Manager

City, State Spartanburg, 

## se Postal Code Telephone (include area code) (864) 578-8966x14 3.

4.

5. 29303 Ifyou had a prenotice communication (PC) concerning this notice and EPA assigned a PC Number to the notice, enter ;;;th;;;.e.;.;n;;;;um.;.;b;;.;c;.;.;r.

____... Ifyou an exemption application for the chemical substance covered by this notice, enter the exemption number assigned by EPA. Ifyou previously submitted a PMN for this substance enter the PMN number EPA withdrawn or . ; Ifyou have submitted a notice ofBona fide intent to for the chemical substance covered by this notice, enter the notice assigned by EPA. Mark (X) ifnone Mark (X) ifnone Mark (X) ifnone Submitting Notice (in U.S.)

b. Agent (if applicable)

c. Joint Submitter (if applicable) Philip R. Miller Company Lubrizol Metalworking Additives Mailing address (number and street) 110 Corporate Drive, City, State Spartanburg, 

## se Name Company Suite C Postal Code 29303

City, State

Name of

Mailing address (number and street)

1. 

# [B] Manufacture 1 2

. Import I 

# D 6. Type ofNotice

- Mark (X) 

# D Only I Only 13. Both I I 

# D Binding Option 

# D Binding Option I I Mark Mark

EPA FORM 7710-25 (Rev. 5-95) Page 3

## I PMN Page 4 ; Page 4 of 19 

### Part I - GENERAL INFORMATION - Continued Section B - CHEMICAL IDENTITY INFORMATION: 

# I You mustprovide a currently COrTect Chemical Abstracts (CA) name ofthe substance based onthe ninth Collective Ind.x (9Cl) ofCAnomenclature rules and conventions. Mark IX)the "Confidential" box next to any item you claim as confidential Complete either item I (Class I or 2 substances) or 2 (polymers) as appropriate. Complete all other items. Ifanother person will submitchemical identity information foryou (foreither Item I or 2), mark (X) the box at the right. 

# 0 IdentifY the name, company, and address ofthatperson in a continuation sheet. II I. Class I or2chemical substances (for**definition~** class I and class 2**substan~see** the Instructions Manual) a. Class ofsubstance

- Mark (X) 

### L.J Class I or**~** Class 2 b. Chemical name (Currently correct Chemical Abstracts (CA) Name that is consistent with TSCA Inventory listings for similar substances. For Class 1 substances a CA Index Name mustbe provided. rorClass 2 substances either a CA Index Name orCA Preferred Name must be provided, which ever is appropriate based onCA 9CI nomenclature rules and conventions). Confidential 

# D D Phosphoric acid, mixed mono- and diesters with 2-ethyl-l-hexanol and polyethylene glycol mono-C12-16 alkyl ethers

c. Please identifY which method you used to develop or obtain the specified chemical**identi~.** in.formation reported in this notice: (check one). 

# 1";1 Method I (CAS Inventory Expert Service· a copy ofthe Identification 

# U Method 2 (Other Source) 

### L.:J report obtained from the CAS Inventory Expert Services must be submitted as an attachment to this notice) d. Molecularformula 

### eBI 

# D CAS RegistryNumber (ifanumber already 

# I I exists for the substance) 

### 882693-50-7 e. For a class 1substance, provide a complete and correct chemical structure diagram. Fora class 2 substance, provide a correct representative or partial chemical structure diagram, as complete as can be known, ifone can be reasonably ascertained. Please see the E-PMN Instruction Manual for discussion of"native format" diagram software which can be helpful in reviewing your substance.



# o Mark (X) this box ifyou attach a continuation sheet.
EPA FORM 7110-25 (Rev. 5·95) Page 4



# I

### PMN Page 4a ; Page 5 of 19 Fora class 2 substance

- (I) List the immediate precursor substances with theirrespective CAS Registry Numbers. (2) Describe the nature ofthe reaction orprocess. (3) Indicate therange ofcomposition and the typical composition (where appropriate).

e. (1) List the immediate precursor substances with their respective CAS Registry Numbers. 

### ConfiName (CAS #) 

### dential

e. (2) Describe the nature ofthereaction orprocess.

e. (3) Indicate the range ofcomposition and thetypical composition (where appropriate).



# IL] Mark (X) this box ifyou attach a continuation sheet. EPAFORM7710-25 (Rev. 5-95) Page 4a

### PMN Page 5 ; Page 6 of 19 Part I -- GENERAL INFORMATION -- Continued Seetion B - CHEMICAL IDENTITY INFORMATION ­ Continued 2. Polymers (For a definition ofpolymer, see the Instructions Manual.) Confidential a. Indicate the number-average weight ofthe lowest molecularweight composition ofthe polymer you intend to manufacture. 

# D Indicate maximumweight percentoflow molecular weight species (not including residual monomers, reactants, or solvents) below 500 and below 1,000 absolute molecular weight ofthat composition. Describe the methods ofmeasurement orthebasis for your estimates: GPCU Other U: (Specify below) (i) lowest number average molecularweight: 

# I I (ii) maximum weight% below 500 molecularweight: (iii) maximum weight % below 1000 molecular weight: 

# 0 Mark (X) this box ifyou attach a continuation sheet. b. You must make separate confidentiality claims for monomer or otherreactant identity, composition information, and residual information. Mark (X) the "Confidential" box next to any item you claim as confidential (I) 

# - Provide the specific chemical name and CAS Registry Number (ifa numberexists) ofeach monomerorother reactantused in the manufacture of thepolymer. (2) 

## - Mark (X) this column ifentry in column (I)is confidential. (3) 

# - Indicate the typical weight percentofeach monomer or otherreactant in the polymer. (4) 

## - Choose "yes" from drop down menu ifyou want a monomerorotherreactant used at two weight percent or less to be listed as part ofthepolymer description on the TSCAChemical Substance Inventory. (5) 

## - Mark (X) this column ifentries in columns (3) and (4) are confidential. (6)


### - Indicate the maximum weightpercent ofeach monomer orotherreactant that may bepresent as a residual in thepolymer as manufactured for commercialpurposes. (7)

- Mark (X) this column ifentry in column (6) is confidential. Monomeror other reactant and CAS RegistryNumber Confi- Typical Include in Confi- Maximum Confidential composition identity dential residual dential (I) (2) (3) (4) (5) (6) (7) 

# 0 % 

# "0 %

# D 

# D % 

# D %

# D 

# 0 %

# D

# 0 % 

# D %

# D

# D %

# D D %

# D

# D %

# D D %

# D %

# D .L % 

# 0 %

# D CJ % 

# c=::J % 

# I I 

# CJ % 

# [ % 

# I I 

# c=::J % 

# [ % 

# CJ % 

# c= % 

# I I 

# CJ % 

# [ 

# - % 

# ,CJ % 

# c= % 

# I I D Mark (X) this box ifyou attach a continuation sheet.
EPAFORM 7710-25 (Rev. 5-95) Page 5

### PMN Page 5a; Page 7 

### of 19
c. Please identifY which method you used to develop or obtain the specified chemical identioormation reported in this notice (check one). 

# o Method I (CAS Inventory Expert Service - a copy ofthe identification report Method 2 (other source) obtained from CAS Inventory Expert Service must be submirted as an attachmentto this notice) 

### CRI 

# D
d. The currently correct Chemical Abstracts (CA) name for the polymer that is consistentwith TSCA Inventory listings for similar polymers. 

# D

CAS Registry Number (ifa numberalready exists for the substance) 

# I

e. Provide a correctrepresentative orpartial chemical structure diagram, as complete as can be known, ifone canbe reasonably ascertained. Please see the E-PMN Instruction Manual for discussion of"native format" diagram software which can be helpful in reviewing your substance. 

# I

[ ]Mark (X) this box ifyou attach a continuation sheet.

EPA FORM 7710-25 (Rev. 5-95) Page Sa

### 08/04/2086 09:34 

## 1-854-578-8277 GATEl,,1AV ADDITIVE CO PAGE 04



### PMN PageS ; Page 6 of 19 

### Part 1-- GE%'Io"ERAL INFORMATION

- Contioued**S~tion** l3

­ CHEMICALlDEN'JTI'YINFORMATION

- COlllinutd 2. Polymers (FOI'a definitKm ofpolymC'r. liee the InS!/UCtions 1I,.1anual.) 

### a. tndic£te thc numba-nvemgc.' weigh.t ofthe**IO~lt** molecl.ll:lrWl:ightc.:>mpo$itloll of'thc:polymerY(lU inllmdto lTWIuli!.cture. tndi.:.ttc: muimUIIl wcightPefC4'Qt onow 11101=!arweight**~pe'ie~** (n()l. ineludingu*iulll mOQomers, reactants, or solve!lU) below SOO and below 1.000absolutr:: rnolecnl;l.f**wej~ht** of**th~t c:om'PO~illOl\,**  Contidentisl

Des<:ribc the mC"thoo9 of1IlC'1lS'UJ'em.eotortl\e buis foryour egcim.ttes: C;PC

# 0 Other**~'** (Specify below) (I) 

### lowestnumber 1v.:ngC

# mOI~l)J:lr weight:
_______ 

# Ir-:...:..-:.--....:.....------------.I (H)**~,i_** 

# ..." % bolow ."**"""~"'"** .. ",,, (iii) m.:Wmlltn weigh! %below 1000 moJeclllOl.f**weigtl!~** . 

# o b, Mark (Xl 

### mig box it

### you attach**~**continuation 

### .neel.. You m.wtt conficclltiaJiry clailllil fur mOIlOIna' or othe:uQctant identity, COmpo.ilion inCotnl:1ciOll, $JIdrc:sidu:u infocm1ti011, M3rlc (X) lhe "ContidentW" box. next tolIlY item you c!,llm;13 COJ\fidcnri31 (1)

- Provide Ibe**~ific** chc:roicnl name:lnd CAS RegistryNlltnbr.r (!fa !lumber**cxi"t~)** ofe:ICh monomer or other mlJ:bJl.tUstd in t.l)c manulXturt of the: polymer, twtark (X) this c:ollltnn itentry in column (1) if; cODfidaltisl. k\di(;:I1e thfrtypical wcigbt**per'~ttt** 

### otc£citrnooomet' ClI'alher f(:2.CWlt in !.hepolymer. (2) • (3)

- (4) • 

### Choose KYfS" 

### from drop down menu it

### you wont 0. 

### rcol\O;ner orothe< 

### n:netant used at tw()

### weightpercentOf

### less to 

### be li9u:d lIS 

### part ofthe polymer desc:riptton OIl the !SeA**Ch~rn.i"'l** S\lbsWlce: Inventory. (5)

- Mark. (X) this column ift'otries in**colum.n~** (3) lind (4) 3re confidcnuill. (6)

- Indicate**~)e** muimum "'c:iglttpercent ofcschmonomer Ofother fcacWll!b.lC ma)! b!**pr~cnt** III> Il**~idual** in the polymer III>**~Tcd** for 

### commercial puIP<lS!'" (7). M'.at!c (X)this oolumn 

### ifentry ill column (6) ilcoofidcntial MonomCl' 01' other re3.CUIll s.ndCAS**Reb-i~t:y**Number (I) 

# ! Confidential

(2)**T~'Pjcal** composition (3) Includl: in idC'lltiLy

(4) 

### Confi· dential

(S) 

# %0 )(," Mwmuro 

### ! residual '

(6)

:"",%

-_% Confidcruul

(T)

:-:: :'::J**v>~ ;-;.~:**  

# F**IIIIIIJ~I**

# Iii**~II**J!i

# ~I**'I~**tIl,II

# JIOI

# JillJ

# II~111111 

# :=**~. P-()~-fiI11**  % % 

# CJ % 

# IC ]

- % 

# c:J

- 

# 1c:J % % 

# %/ I

# 0 Mark (X) 

### this

### bo~ ifyoo. altiltb s continU1llion sheel:. 

### I

EPA J!'ORM 111 Q·25 (RCII. 5-95) PageS 

# ;,:lANY 

# SANITIZED 

# COMPANYSANITIZED

## 88/84/2885 09:34 

## 1-854-578-8277 GATEWAV ADDITI\/E CO 

## PAGE 85
PMN Page 5a: Page 7 of 19 

# I c. PleilSe Identify wbicllmethod you used to develop or obtain !he specified chemical**idrnti~ormation** reponed in thili notice (check one), 

# o Method I (CAS inventory expert Service· a ropy crib", idcntifi.:atiollreport 

# LJ**~ttllod** l**(~c:r** sO\ll'(e) obta.i1lCdfrom**c.~S** !ovcnlory Expert Service must be submiltNu 8113t1.1chmcnt Ibis nolicc) '",
. 

### CBI 

# D.

Q. The currmtlycorrectOIcmical Abstl1l:ts (CA) Mille for the poh"ltll!!r thatis COn&lStCllt withrSCA

### Inventory li6ril1gs for similar polymers.**Pbosphoricaci9~** 

### mixed 

### mono- and diesters with 

### 2-ethyl-l-haxanol and po

### lye

### chylene 

### glycol mono-C12-16 

### alkyl.ethers 

# o

882693-S0-7 

# I I

c. Provldt a correctreprcsentlllive or pu:ial chemical structw"e diagram. IS camplete**~s** C3n be 1.:110"11, it'ooe C3./l bitrusouably35cemined., Ple4S<: SC'C the .E·PMN lAswetion Manu.J £Or diSCUSSion of"native format" disgr.utl SQ.f\:wClfC which embe- helpful inrevie"
..ing yomsubstMee.

[ JMack (X)**thi~** box ifyou atllleh a eOctillulltion sheet.

EPA FORM 7710-25 (Rev. 5-95)

### PMN Page 6 ; Page 

### 8 of 19

(a) IdentiJY each impurity that may be reasonably anticipated to be present in the chemical substance as manufactured for commercial purpose. Provide the CAS Registry Number ifavailable. Ifthere are unidentified impurities, enter "unidentified." Ifthere are unidentified estimate their total %. Impurity and CAS Registry Number Phosphoric acid (CAS# 7664-38-2) 0.4% 1-hexanol, 2-ethyl­ (CAS# 104-76-7) 0.1% Alcohols, C12-16, ethoxylated (CAS# 68551-12-2) 0.1%

Mark (X) this box ifyou attach a continuation sheet. Trade identification

- List trade names for the new chemical substance identified in subsection I or2. ADDCO(R) 365-P 

# D Mark (X) this box ifyou attach a continuation sheet. 6. you must a generic name your that reveals the specific chemical identity ofthe new chemical substance to the maximum extentpossible. Refer to the dential % 

# D % 

# D % 

# D % 

# D %
% 

# D % 

# D

Confidential 

# D

TSCA Chemical Substance Inventory, 1985 Edition, Appendix B for guidance on developing generic names.

attach a continuation sheet. Numberifavailable. Describe any byproducts resulting from the manufacture, processing, use, ordisposal ofthe new substance. Provide the CAS Registry CAS None known 

# D D D D

EPA FORM 7710-25 (Rev. 5-95) Page 6

## 07/31/2005 13:29 1-854-578-8277 GATEWAY ADDITIVE CO PAGE 02
PMN Page 7 ; Page 9 of 19 

## PartI - GENERAL INFORMATION

- Contioued Section C

-- PRODUCTION, IMPORT, AND USE INFORMATION: Mark (X) 

### the "Confidential" box next to 

### any ilem you claimas confidential. 1­ Productionvolume

­ Estimate the

### maximum production volume during the Ii,st [2 months ofproductioll. Also estimate the maximum production volume for

### any consecutive J2-month period during dle 

### first three years o{proouclion. Estimates 

### should be on 

### 100% Dew chemical substance buis. Fora Lo'" Volume Exemption application, ify01J. ehoose to have your notice reviewed at :l lowerproduction volume than 

### 10.000 kll:/yr,**specif~** the volume**~d** mad:: (x) 

### in the binding box. 

### Ifgranted,y_ou 9Ie bound to this volume 

### Maximum first 

### 12-month

### production (kg/yr) Maximum 12-month production (kglyr) Confi- Binding dcnti31 Option 

### (100% new chemical substance basis) (100% new chemical 

### substance basis) Mark (.) 

# [K] 

# D 2. Use Information

-- YClu must m.'lke :iCp:lIlItc confidentiality claims fOr !hed.e,cripticn of!he ca.tegory ofus¢, the per"'cnt ofproduction volt/me devoted to each CIItegory. the ronnubtion of the new**~ubS!.'lnce,** aDd otber \o.SC infolTlUltion, Mnrk (X) the "Confldcncsl"Box next to 3II}' ircnY<lU claim 3S confidential.**~.** (I) --Dc8Cribc each**in~nded** caugory cruse ofthe new chemical subsQIlce byfucction aDd sl'plil:ation. (2) --Msrk (X) this column ifeatryrolumn (I)**i~** cocfu1ential busincu illfOltllation (C81), (3) --Indicau your willingness 10 have tbe i.oforml11ion provided in column (I) biDding. (4) -EstimslC the percent oftOW production for the first three )'1!II1'S d!VOted to uch calegory ofuse.**(~)** -Mark (X) this column ifentry iD column (4) i& confidential**bU3I1W:S~** information. (eEl). (6)-­ ':stimuc the perceDt oftho new**sub~u(lCe** :IS**formuJ~ted** in miXtl.ll'l!S,**~1I,pc:Q;,ioD"** emulsions, soluti=.orgels 113 rNIllufs.c:rurcd for cOlnmcrcial**purpose~** at sires unda YI)Ill colltroll.Ssociau:d with each CS!$goryoflIU. (7) --Mark (X) tlus column ifentry in CO]WDIl(6)**i~** canfidcntilll busine'lS infortMtion (C)3l). (8) --llldic:.te % Clf productvolume cxpcctOd for the ljsted wu!e"**~Clors.** Mark: more trun one box ifappropriate. Mutt (X) 10 indicate your "'iUingncss to have dlCuse type provided III (8)**~cdicg.** (9) --Marlc (X) tbis oohlmn 

### ifeatryfjes) 

### in CQ[UOlll (8) 

### Is**(3C~)** cOIltide.otlnl businC'>s icf'onnDtioc (CBI). Categoryofute (I) (byfiluction alld application i.c. a CBI Oi""i", Prad· CBI %ia CBI % ofsubs!llIl.eC: expected per use CBT dispel'8ivc dye for**tini~hjn8** polyester**fi~rs)** OpIJon u(tion FOMU (8) Mill: 'I. J.ti"" (-) (2) 0) (4) (5) (6) (7) Sitt'- Co",,"
...&.... Com
.. BIIId'"£ (9) limittd umet IIioI merci41 Opu•• 

# D % % 

# D 0 X 2-3 100 

# [ ;--­ % % 

# D [ Corrosion inhibitor/EP ,additivG for IIlG'l:alworking fluids 

### 5 1-10 100 

# D D %

# D**~~**

# D - 

# 0

- 

# [ %

# [ % 

# D .--­

'--­ 

# DD %

# D % 

# D 0

- 

# D % % ;--­

# [ 

# D %

# D % 

# D 0

• Ifyou have: identified a "consumer" uoe, pJeOUC! provide on a continuation :o./Iccta dcuilcd cle&cciption ofthe**u:;e(~)** ofthis**,h.e:mic~** sub$Wlce in cotlsumerproduc:u.

In addition include estimates Dfthe coDCelrtmtiOll ofthe new chem.ic:ll substance as expectedin COCS\II11CI' products and dCM:ribc the chemical ructions by which this subf.ta.cce lOAeS its identity in the COc.sUIDc:T produa. DMark (X) this box ifyou att;tcil
.. continU:ltion sheet. b. Genmc usc lfyou claim any C<ltegory**ofu~** description in sub&CClion 2a :IScDc.fidentinl, coler;ll goeneric description oftlwcategory Rcad the lnsiIuaioll dt'SCription Manual for examples ofgeneric usc cicscriptions. Hydraulic fluid 

# D**~,Ii:** 

### OQ**dti~** box ifyou amelia COIlOllll3tioD sheet. I 3. HazardInformation -Includeinthe noliee**~** copyofrC!l.SOn.ablcfacsimile ohnyh:wtrd 'OIOInlmg statement, label, rmtcrilil safety dara sbcet. or othCT Bln.lng

illfoIl'llationwhichwill be: provided 10 lillY penCIl! who is Tc.1Bcnably likely tobe expo..cd 10 tIllS**~ubsu1\Ce**regarding pr<l!CC1ive C<1,WpmcDt orpractices:£or o,.tl
..., rile safe tuoding, transport, 11se, ordisposal ofthe nI!WrubEWlCe. List in. port III haurd ill1'ormation you includc. Mar.(><)

# ~ M""I< (X) \hi:< bll)c' ,{you**3~ell**hlWlrd infonnnnon. 

# C]
EPA FORM 7710-25 (Rev. 5-95) P3gc 7

### PMN Page 8 ; Page 10 of 19 Section A - INDUSTRIAL SITES CONTROLLED BY THE SUBMITTER (X) the "Confidential" box next to any item you as confidential Complete section A for each type ofmanufacture, processing, or use operation involving the new chemical substance at industrial sites you control. Importers do nothave to complete this section for operations outside the U.S.; however, you may still have reporting requirements if after You must describe these See instructions manual will occur. Name 

### Lubrizol Performance Products Spartanburg Site address (number and street) 

### 195 Brooks Boulevard ZIP code 

### Ifthe same operation will occur at more than one site, enterthe number ofsites. Identify the additional sites on a continuation sheet, and ifany ofthe sites have significantly different production rates or operations, include all the information requested in this section for those

1. Batch
2. Continuous Hourslbatch
Maximumkg/day (100% new chemical Hours/day substanee)
d. Process description Mark (X) to indicate your willingness to have yourprocess description binding. 

### 9307

Use Batcheslyear Days/year Confidential 

# D



# D D
(I) Diagram the majorunit operation steps and chemical conversions. Include interim storage andtransport containers (specify- e.g. 5 gallonpails, 55 gallon drum, rail car, tank truck, etc.). (2) Provide the identity, the approximate weight (by kg/day orkg/batch on a 100% newchemical substance basis), and entry point ofall starting materials and feedstocks (including reactants, solvents, catalysts, etc.), and ofall products, recycle streams, and wastes. Include cleaning chemicals (note frequency ifnot used daily orperbatch.). (3) Identify by number the points ofrelease, including small or intermittent releases, to the environment ofthe new chemical substance. Ifreleasing to two media at the same step, assign a second release numberfor the second medium.

attach a continuation sheet. EPA FORM 7710-25 (Rev. 5-95) Page 8

### PMN Page 8a; Page 11 of 19 Confidential

EPA FORM 7710-25 (Rev. 5-95) Page 8a

### PMN Page 9 ; Page 12 of 1 9 

### Part 11- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE

- Continued ,ection A - INDUSTRIAL SITES CONTROLLEDBY THE SUBMITTER

-- Continued 2. Occupational Exposure

- You must make separate confidentialityclaims for the description ofworker activity, physical fonn ofthe new chemical substance, number of works exposed, and duration ofactivity. Mark (X) the "Confidential" box next to any item you claim as confidential. (I) .-Describe the activities (i.e. bag dumping, tote filling, unloading drums, sampling, cleaning. etc,) in which workers may be exposed to the substance. (2) ••Mark (X) this column ifentry in column (I)is confidential business infonnation (CBI). (3) _. Describe any protective equipment and engineering controls used to protect workers. (4) and (6)

-- Indicate yourwillingness to have the infonnation provided in column (3) or (5) binding. (5)·- Indicate the physical fonnCs) ofthenew chemical substance (e.g., solid: crystal, granule, powder, or dust) and % new chemical substance (ifpartofamixture) at the time ofexposure. (7)

-- Mark (X) this column ifentry in column (5) is confidential business infonnation (CBI), (8) .- Estimate the maximum numberofworkers involved in each activity for all sites combined. (9) _. Mark (X) this column ifentry in column (8) is confidential business infonnation (CBI). (10) and (11) _. Estimate the maximum duration ofthe activity for any worker in hours per day and days per year. (12) _. Mark (X) this column ifentries in columns (10) and (II) are confidential business infonnation (C

## in. Worker activity CBI Protective Equipment! Binding Physical Binding CBI #of CBI Maximum duration CBI fonns(s) (i.e., bag dumping, filling drums) Engineering Controls Op!ion and % new Op!ion Workers Hrslday Dayslyr Mark (.) substance Mark(.) Exposed (I) (2) (3) (4) (5) (6) (7) (8) (9) (10) (11) (12) 

### A. Sampling (Process Gloves, goggles liquid Steps 11,12,14,19) 95­ 100% 1 0.5 45
'---­ 

### B. QC Analysis Gloves, safety glasses liquid (Process Steps 100% 11,12,14,19) 2 2 45
C. Filling drums Gloves, goggles liquid (Process step 19) 100% 1 4 45



# - 

# 0 - 

# 0

I.-­ 

# D

I.-­ 

# D D D ,....-­ 

# D**~** 

# 0 - - 10 Mark (X) this box ifyou attach a continuation sheet. EPA FORM 7710-25 (Rev. 5-95) Page 9

### PMN Page 9a; 

### Page 13 of 19 

## 13. Environmental Release andDisposal-- You must make separate confidentiality claims for the release number and the amount ofthe new chemical substance released and other release and disposal information. Mark (X) the "Confidential" box next to each item you claim as confidential. (l) -- Enter the number ofeach release point identified in the process description, partJI, section A, subsection Id(3). (2)

--Estimate the amount ofthe new substance released (a) directly to the environment or (b) into control technology (in kg/day or kglbatch). (3)

--Mark (X) this column ifentries in columns (l)and (2) are confidential business information (CBI). (4)

-- Identify the media (stack air, fugitive air (optional-see Instruction Manual), surface water, on-site or off-site land or incineration, POTW, orother (specify» to which the new substance will be released from that release point. (5)

-- a. Describe control technology, ifany, and control efficiency that will be used to limit the release ofthe new substance to the environment. Forreleases disposed ofon land, characterize the disposal method and statewhether it is approved for disposal ofRCRA hazardous waste. On a continuation sheet, for each site describe any additional disposal methods that will be used and whether the waste is subject to secondary or tertiary on-site treatment. b. Estimate the amount released to the environment after control technology (in kg/day). (6)

--Mark (X) this column ifentries in columns (4) and (5) are confidential business information (CBI). (7)

-- Identify the destination(s) ofreleases to water. Please supply NPDES (National Pollutant Discharge Elimination System) numbers for direct discharges or NPDES numbers ofthe POTW (Publiclv Owned Treatment Works). Mark (X) ifthe POTW name or NPDES # is confidential business information (CBI). Release Amount ofnew Cl I Medium of Control technology and efficiency (you may wish to optionally attach CBI Number substance released release efficiencydata)

(1) (2a) (2b) e.g.stacl.air ( ) (4) (Sa) (5b) (6) 

# D On site bio/mechanical 

### r--­ 0 0 20 kg 1 tank washing lined treatment pond


# --­ '--­ 

### r--­ r--­ 

# D 0 

### 5 kg On site bio/mechanical 

### 0 2 drumming spillage lined treatment pond
'--­


# - 

# D D 

# D D D

- 

# D D D**~** 

# - 

# D == 

# D -



# - - 

# D D
(7) Mark (X) the destination(s) ofreleases to water. 

### NPDES# 

### CBI 

# D POTW--provide name(s) 

# D Navigable waterway-­ provide name(s) 

# D Other--Specify
] Mark (X) this box ifyou attach a continuation sheet.

EPA FORM 7710-25 (Rev. 5-95) Page9a

### PMN Page 10; Page 14 of 19 Part 11- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE

- Continued I 

### <1ection B - INDUSTRIAL SITES CONTROLLED BY OTHERS mplete section B for typical processing oruse operations involving the new chemical substance at sites you do not control. Importers do not have to complete this section for operations outside the U.S.; however, you must report any processing oruse activities after import. See the Instructions Manual. Complete a separatesection Bfor each type of processing. or use operation involving the new chemicalsubstance. Ifthe same operation is perfonned at more than one site describe the typical operation common to these sites. Identify additional sites on a continuation sheet. 1(a). Operation Description

-- To claim information in this section as confidential, circle orbracket the specific information thatyou claim as confidential. (I)

-- Diagram the major unit operation steps and chemical conversions, including interim storage and transport containers (specify

- e.g. 5 gallon pails, 55 gallon drums, rail cars, tank trucks, etc). On the diagram, identify by letter and briefly describe each worker activity. (2)

-- Either in the diagram or in the text field I(b) below, provide the identity, the approximate weight (by kg/day or kglbatch, on an 100% new chemical substance basis), and entry point ofall feedstocks (including reactants, solvents and catalysts, etc) and all products, recycle streams, and wastes. Include cleaning chemicals (note frequency ifnotused daily orperbatch). (3)

-- Either in the diagram or in the text field I(b) below, identify by numberthe points ofrelease, including small or intennittent releases. to the environment ofthe new chemical substance. (4) Please enter the # ofsites (remember to identify the locations ofthese sites on a continuation sheet): .."..:::1,-:-:--_ # ofsites 

# Attachment

# 3: Operation Description BOP Fluid Performance Package CBI 

# o

(ActivityA) ADDC0365-P

(5-15% by weight) 

## Release 

## 1
....----1 

### Water (balan**~r:}** 

### 'III: 

## Release 2 

## (Activity C)

....... t------I 

## QC Testing 

# Blend Tank (BOP Performance**l»~d~:.il.!.e ~**  

# 1 Drumming of BOP Performance Package I 

### Corrosion Inhibitor (30-50% by weight)



## t------+Re/ease 3 

## Activity B
l(b). (Optional) This space is for a text description to clarify the diagram above. Activity A: transfer of ADDCO 365-P from totes or tank truck to blend tank (100% new substance)
. Activity B: transfer from blend tank to drums or isotainers (10% new substance)
. Activity C: Various QC tests to ensure quality (10% new substance)
. 

# o

Release 1: Washing of residual material from totes or tank trucks (the latter performed by contract tanker washing service). 100% new substance. Release 2: Washing of blend tank after completed processing. 10% new substance. Release 3: Any material spilled in the drumming process. 10% new substance.

] Mark (X) this box ifyou attach a continuation sheet. EPA FORM 7710-25 (Rev. 5-95) Page 10



# I

### PMN Page 

### 10a ; Page 15 of 19 2. Worker ExposurelEnvironmental Release (\) From the diagram above, provide the letter for each worker activity. Complete 2-8 for each worker activity described. (2)

-- Estimate the number ofworkers exposed for all sites combined. (4) Estimate the typical duration ofexposure per worker in (a) hours perday and (b) days peryear. (6) Describe physical form ofexposure and % new chemical substance (ifin mixture), and any protective equipment and engineering controls, ifany, used to protect workers. (7)

-- Estimate the percent ofthe new substance 

### as formulated when packaged orused 

### as a final product. (9)

-- From the process diagram above, enter the number ofeach release point. Complete 9-13 for each release point identified. (10) Estimate the amount ofthe new substancereleased (a) directlyto the environment or(b) into control technologyto the environment(in kg/dayorkglbatch). (12)

-- Describe media ofrelease i.e. stack air, fugitive air (optional-see Instructions Manual), surface water, on-site oroff-site land orincineration, POTW, or other (specify) and control technology, ifany, that will be used to limit the release ofthe new substance to the environment. (14) Identify byproducts which may result from the operation. (3), (5), (8 :(11), 13) and (15)

-- Mark (X) this column ifanyofthe proceeding entries are confidential business information (CBI), Letter # of CBI Duration Of CBI 

### Protective Equip. IEngineering ControlslPhysical Form and! 

### % new substance %in CHI

of Workers FormActi- Exposed Exposure ulation vity i (I) (2) (3) (4a) (4b) (5) (6) (7) (8) 

## --. 

## IA 1 2.00

# 25~B Gloves, goggles, apron 100 

# iD

--, B 1 4.00 25·1W

# ~ -. C 2 1.00 25·1W

# D**~** 

# D D 

# B D D
Release Amount of CBI 

### Media ofRelease 

### & Control Technology CBI I Number New Substance Released (9) (lOa) (lOb) (II) (12) (13) 1 0 10 

### kg/batch 

# D 

# O!

0 5



# - kg/batch 

# 10 0

3 0 1 

### kg/batch 

# 0 0

- 

# 0 '-­ 

### r-­ 

# 0 (14) Byproducts: (15) 

# D 0 Mark (X) this box ifyou attach a continuation sheet, 

# OPTIONAL POLLUTION PREVENTION INFORMATION To claiminformation in the following section as confidential circle or bracket the specific information that you claim as confidential. In this section youmayprovide information not reported elsewhere in this form regarding your efforts to reduce or minimize potential risks associated with activities surrounding manufacmring, processing, use and disposal ofthe PMN substance. Please include new information pertinent to pollution prevention, including source reduction, recycling activities and safer processes orproducts available due to the new chemical substance. Source reduction includes the reduction in the amount ortoxicity ofchemicalwastes by technological modification, process and procedure modification, product reformulation, raw materials substimtion, and/or inventory control. Recycling refers to the reclamation ofuseful chemical components from wastes that would otherwise be treated or released as air emissions orwater discharges, or land disposal. Descriptions ofpollution prevention, source reduction and recycling should emphasize potential risk reduction subsequent to compliance with existing regulatory requirements and can be either quantitative orqualitative. The EPA is interested in the information to assess overall net reductions in toxicity orenvironmental releases and exposures, not the shifting ofrisks to otherenvironmental media or nonenvironmental areas (e.g., occupational or consumer exposure). In addition, information on the relative cost or performance characteristics of the PMN substance to potential alternatives maybe provided. 

### All information provided in this section will be 

### taken into consideration during tbe review oftbis substance. See PMN Instructions 'nual and Pollution Prevention Guidance manual for guidance and examples.

EPA FORM 7710-25 (Rev. 5-95) Page lOa

### PMN Page 11 ; 

### Page 16 of 19 

# IOptional Pollution Prevention Information (Continued) Describe the expected net benefits, such as (I) 

### an overall reduction in risk to human health orthe environment; (2) a reduction in the volume manufactured; (3) a reduction in the generation ofwaste materials through recycling, source reduction or other means; (4) a reduction in potential toxicity orhuman exposure and/or environmental release; (5) an increase in product performance, a decrease in the cost ofproduction and/or improved operation efficiency ofthe new chemical substance in comparison to existing chemical substances used in similar application; or (6) the extent to which the new chemical substance maybe a substitute for an existing substance thatposes a greater overall riskto human health orthe environment. 

### CBI Blow-out Prevention In offshore oil fields, "kicks· or blow-outs due to downhole pressure surges can result in an 

# D uncontrolled flow of fluids from a well, and may cause serious formation damage. To guard against these events, a Blow-out Preventor (BOP) consisting of a set of hydraulically-operated valves or rams is placed at the well opening and is used to safely shut-in the well. In this application, turbine flowmeters are used for precise sensing of hydraulic fluid flow during activation of the BOP. Meters monitor flow on the surface at the hydraulic power unit (HPU) , and on the sea floor at the BOP. These meters are specifically designed to withstand the extreme water hammer effect within the hydraulic system, as well as the demanding external environment on the ocean floor. This equipment provides accurate flow information which allows leakage or other problems within the hydraulic system to be detected prior to a catastrophic failure. In the event of leakage of the BOP fluid, it should have a good degree of biodegadability, no significant bioaccumulation and have relatively low toxicity to marine life. The data contained in attachments 9-14 supports these criteria.



# [J Mark (X) this box ifyou attach a continuation sheet. EPA FORM 7710-25 (Rev. 5-95) Page 11

### PMN Page 12 ; Page 17 of 19 

# Part III -- LIST OF ATTACHMENTS Attach continuation sheets for sections ofthe fonn and test data and other data (including physicaVchemical properties and structure/activity infonnation), and optional infonnation after this page. Clearly identify the attachment and the section ofthe fonn to which it relates, ifappropriate. Number consecutively the pages ofany paperattachments. In the column below, enter the inclusive page numbers ofeach attachment. Electronic attachments canbe identified by filename. Mark (X) the "Confidential" box next to any attachment name you claim as confidential. Read the Instructions Manual for guidance on how to claim any infonnation in an attachment as confidential. You must include with the sanitized copy ofthe notice fonn a sanitized version ofany attachment in which you claim information as confidential. 

## I # Attachment name AttachmentFilename Attachment Confipage number(s) dential 

### 1 ADDCO(R) 

### 365-P MSDS 

### 21-28 

# D 2

# ~ 3 

# illL 4 Octanol Solublity Report 

### 29 

# D 5 Octanol solublity Method 

### 30-31 

# D 6 Water solubility Report 

### 32 

# D
7 Water solublity Method 

### 33-34 

# D
ectrum scan 

### 35 

# D



# -=­ 

# tm-1

10 11

# ~ I 12

# ~ , 

### 13

# ~ I 

### 14

# ~ ntory Expert Service Report 

### 86 

# D 

# m D D D D D

[ ] Mark (X) this box ifyou attach acontinuation sheet. Enter the attachment name and number.

# ~ EPA FORM 7710-25 (Rev. 5-95) Page 12

### PMN Page 13 ; Page 18 of 19 PHYSICAL AND CHEMICAL PROPERTIESWORKSHEET To assist EPA's review ofphysical and chemical properties data, please complete the following worksheet for data you provide and include it in the notice. IdentifY the property measured, the page ofthe notice on which the property appears, the value ofthe property, the units in which the property is measured (as necessary), and whether or not the property is claimed as confidential. Ifthe attachments are electronic, give the attachment number (found on page 12) at (b). The physical state ofthe neat substance should be provided. These measured properties should be for the neat (100% pure) chemical substance. Properties that are measured for mixtures or formulations should be so noted (% PMN substance in

# -->. You are not required to submit this worksheet; however, EPA strongly recommends that you do so, as it will simplifY review and ensure that confidential information is properly protected. You should submit this worksheet as a sUJ:)plementto your submission oftestdata. This worksheet is not a substitute for submission oftest data. Property Mark (X Page Value Measured () Confi· if number Estimate denlial (a) provided (b) (c) Mark (X) (M orE) (d) 

### Physical state ofneat substance 

# D Q (s) 

# 0(1) D(g) M 

# 0 Vaporpressure 

# D 0 @ Temperature 

### °C Torr Density/relative density 

# D 1. 02@15. 6C 

### I!Icm3 

# M 

# 0 Solubility 23.5 

### @ Temperature 

### °C 

# M

# ~

Sit l-octanol completely sol

# ~

oven



# - Solubility in water @ Temperature 

### °C

# ~ 

# 0 Melting temperature 

# D °C 

# 0 Boiling 

### I sublimation temperature(@' torrpressure 

# D °C 

# 0 Spectra FTIR

# ~ M 

# 0
Dissociation constant 

# D 0 Particle size distribution 

# D 0
Octanol / water partition coefficient 

# D See attachment 9 

# M 

# 0 I Henry's Law constant 

# D 0 ation from water 

# D 0
ation from soil 

# D 0 I pH@ concentration 

# D 10

Flammability 

# D COC Flash Point=158C 

# 1M 

# 0 Explodability 

# D 0 Adsorption 

### I coefficient 

# D Other
_Specify Acid Number 

# D 240-280 mgKOH/gm 

# 1M Other
_Specify Brookfield Viscosity @25C 

# D 275 (#3 pin, 20 rpm 

# D Marl< (X) this box if you attach a continuation sheet Enter the attachment oame and number. 

### ATTACHMENT PAGE 13

## Premanufacture Notice Electronic Continuation Sheet Continued From: Part II, Section A 1 d, pg 8 Continuation Title: 

### Process Description Continuation Insert narrative continuation here 

### Confidential 

# [K]

Insert any picture here (PDF) 

### Confidential 

# D



# o Check here to add another continuation sheet 

### Page 20

### of 20 0

## 1 ADDCO(R) 365-P Page 1of 8

Material Safety Data Sheet ADDCO(R) 36S-P 

# LUBRIZOL Metalworking Additives Prepared according to 29CFR 1910.1200. Chemical Product and Company Identification LubrizolMetalworkingAdditives 110 Corporate Drive, Suite 

# C Spartanburg, SC

## 29303 Tel: (864) 578-8966 This material is to be used for research purposes only under the supervision ofa technically qualified individual. The toxicological properties may have not been completely characterized. To determine yourresponsibilities under the Toxic Substances Control Act (TSCA), please see the Regulatory Information Section. Ifthis material has been supplied to you under the terms of a secrecy ornon­ analysis agreement, the information included in this MSDS is hereby identified as "Confidential Information." Product Trade Name ADDCO(R) 365-P CAS Number Not applicable for mixtures. Synonyms None. Generic Chemical Mixture. Name ProductType Experimental. PreparationiRevision 25 July 2006 Date Transportation Emergency Phone No. (CHEMTREC) 1-800-424-9300. Outside the U.S. (703) 527-3887 MSDS No. 14132636-6522097-3023610-811103 

# IHazards Identification

7/25/06 

## Appearance Clear yellow to amber liquid. Odor Mild Principal Hazards DANGER
. • VERY CORROSIVE. CAUSES SKIN BURNS. • CAUSES EYE**BUR..~S.** 

## • MAY CAUSE RESPIRATORY TRACT IRRITATION.
This material is considered hazardous by the OSHA Hazard Communication Standard 29CFR
htto:llmsds/SearchIDisolavMsds.asox

# 15 ADDCO(R) 365-P Page 2 of 8
1910.1200. See Section 11 for complete health hazard information. 

## 3 Composition/Information on Ingredients Hazardous Ingredients Comp CAS No. Percentage**(~y** 

## wt.) Carcinoe;en Phosphate ester Confidential. From 10 to 100 percent NIE (NIE) - 

## None established 

# I FirstAid Measures Eyes Flush immediately with waterfor at least 15 minutes. Get immediate medical attention. Skin Wash with soap and water. Get medical attention ifirritation develops. Launder contaminated clothing before reuse. Inhalation Remove exposed person to fresh air if adverse effects are observed. If 

## breathing is labored, administer oxygen. If 

## breathing has stopped, apply artificial respiration. If

## irritation persists or iftoxic symptoms are observed, get medical attention. Oral DO NOT INDUCE VOMITING. If

## conscious give 2 glasses ofwater and get immediate medical attention to perform gastric lavage. Additional Information Note to physician: Treat symptomatically. 

# I FireFightingMeasures Flash Point 158°C, 316.4 OF COC 

## (Typical) Extinguishing Media C02, 

## dry chemical, orfoam. Water can be used to cool and protect exposed material. FirefightingProcedures Recommend wearing self-contained breathing apparatus. Unusual Fire 

## & None known. Explosion Hazards 

# IAccidental Release Measures Spill Procedures Personal Protective Equipment must be worn, see Personal Protection Section for PPE recommendations. Ventilate area if spilled in confined space or other poorly ventilated areas. Prevent entry into sewers and waterways. Pick up free liquid for recycle and/or disposal. Residual liquid can be absorbed on inert material. 

# IHandling and Storage
7125/06 

## http://msds/Search/Disp\ayMsds.aspx

## 8 ADDCO(R) 365-P Page 3 of 8
Pumping Temperature Not detennined. Maximum Handling Temperature Not determined. Handling Procedures Keep containers closed when not in use. Wash thoroughly after handling. Empty container contains product residue which may exhibit hazards of product. Maximum Storage Temperature Not detennined. Storage Procedures No special storage precautions required. Loading Temperature Not detennined. Exposure ControlslPersonalProtection Exposure Limits OtherExposure Limits Engineering Controls
Gloves Procedures Eye Protection Respiratory Protection
Clothing Recommendation

FlashPoint Upper Flammable Limit LowerFlammable Limit Autoignition Point Explosion Data VaporPressure pH Specific Gravity BulkDensity Water Solubility Percent Solid Percent Volatile 

# I Physical and Chemical Properties None established None known. Use local exhaust ventilation to control mists or vapors. Additional ventilation orexhaust may be required to maintain air concentrations below recommended exposure limits. Use nitrile orneoprene gloves. Chemical goggles orfaceshield. Use NIOSHIMSHA approved full face respirator with a combination organic vapor and dust/mist cartridge ifthe recommended exposure limit is exceeded. Use self-contained breathing apparatus for entry into confined space, for other poorly ventilated areas and for large spill clean-up sites. Long sleeve shirt is recommended. Launder contaminated clothing before reuse.

7/25106 

## 158°C, 316.4 

# OF COC (Typical) Not detennined. Not determined. Not detennined. Material does not have explosive properties. Not detennined. Not detennined. 1.02 (15.6 °C) Not detennined. Insoluble. Not detennined. Unknown. http://msds/SearchlDisplayMsds.aspx

## ADDCO(R) 365-P Page 4 of 8


## Percent VOC VaporDensity Evaporation Rate Odor Appearance Viscosity OdorThreshold BoilingPoint PourPoint Temperature Melting 1

## Freezing Point

Stability Decomposition Temperature Incompatibility Polymerization Thermal Decomposition Conditions to Avoid Material is normally stable at moderately elevated temperatures and pressures. Not determined. None known, avoid contact with reactive chemicals. Will not occur. Smoke, carbon monoxide, carbon dioxide, aldehydes and otherproducts of incomplete combustion. Not determined. 

# In I Toxicological Information
Eye Irritation Skin Irritation Respiratory Irritation
Dermal Toxicity Inhalation Toxicity OralToxicity Not determined. Not determined. Not determined. Mild Clear yellow to amber liquid. 275 Centipoise (25°C) Unknown. Not determined. Not determined. Not determined. The above data are typical values anddo notconstitute a specification. Vaporpressuredata are calculated unless otherwise noted. 

# IStability and Reactivity

-- ACUTE EXPOSURE

-­ Corrosive to eyes. Based on data from components or similar materials. Very corrosive to the skin. Based on data on components and similar materials. Ifmaterial is misted or ifvapors are generated from heating, exposure may cause irritation ofmucous membranes and the upper respiratory tract. Based on data from components and similarmaterials. The LD50 in rabbits is 

## > 2000 mg/Kg. Based on data from components or similarmaterials. No data available to indicate product orcomponents may be a toxic inhalation hazard. The LD50 in rats is 

## > 5000 mglkg. Basedon data from components or similar materials. Swallowing this material causes severe irritation and may cause htto:llmsds/SearchIDisplayMsds.aspx 7/25/06

## ADDCO(R) 365-P Page 5 of 8
bums ofthe mouth, esophagus and stomach, abdominal pain, nausea, vomiting and diarrhea. 

## Dermal Sensitization No data available to indicate product orcomponents may be a skin sensitizer. 

## Inhalation Sensitization No data available to indicate product orcomponents may be respiratory sensitizers.



## -­ CHRONIC EXPOSURE -­ Chronic Toxicity No data available to indicate product or components present at greater than 1% 

## are chronic health hazards. 

## Carcinogenicity Mutagenicity Reproductive Toxicity Teratogenicity No data available to indicate any components present at greaterthan 0.1% 

## may present a carcinogenic hazard. No data available to indicate product or any components present at greater than 0.1% 

## are mutagenic orgenotoxic. No data available to indicate eitherproduct orcomponents present at greater than 0.1% 

## that may cause reproductive toxicity. No data available to indicate product or any components contained at greater than 0.1% 

## may cause birth defects.


## Other _. ADDITIONAL**INFO~\fA** 

## TION .­ No other health hazards known. 

# I Ecological Information

Freshwater Fish Toxicity Freshwater Invertebrates Toxicity Algal Inhibition .- ENVIRONMENTAL TOXICITY -­ Not determined. Not determined. Not determined. 

## Saltwater Fish Toxicity Not determined. 

## Saltwater Invertebrates N t 

## d t . 

## d ""t 0 

## e ermIne
. TOXICI 

## Y Bacteria Toxicity Not determined. 

## Miscellaneous Toxicity Not determined. 

## Biodegradation Bioaccumulation Soil Mobility _. ENVIRONMENTAL FATE _. Adequate datais not available to estimate the biodegradation potential ofthis materiaL Less than 1.0% ofthe components display no potential to bioconcentrate. Not determined. 

# I Disposal Consideration

## ADDCO(R) 365-P Page 6 of 8


## Waste Disposal This material, ifdiscarded, is not a hazardous waste under RCRA Regulation 40 CFR 261. 

# ITransport Information ICAOIIATA (US) ICAOIIATA (International) IMDG IMDG EMS Fire IMDG EMS Spill IMDGMFAG IMO Marine Vessel USCG Compatibility U.S. DOT Bulk U.S. DOT Non-Bulk DOTNAERG TDGBulk TDG Non-Bulk Mexico Mexico**NO!J~Bulk** 

## Bulk Quantity Non-Bulk Quantity Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, PO II Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, PO II Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, PO II F-A S-B 760 DO NOT TRANSPORT

- ADDITIONAL INFORMATION REQUIRED Not determined. Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, PO II Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, POII 154 Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, POII Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, PO II Corrosive liquid, n.o.s. (Phosphate ester), Class 8, UN1760, PO II Corrosive liquid, n.o.s. (phosphate ester), Class 8, UN 1760, PO II 85000 liters, 22457 gal. 207.8 liters, 55 gaL 

## Review classification requirements before shippingmaterials atelevated temperatures. 

# I Regulatory Information

•• Global Chemical Inventories .­ Requires notification in the U.S. Commercial shipments from Lubrizol's U.S. location must be exported to non U.S. customers only. Research and development quantities must bear special labels and shipping papers. Sample recipients must comply with the requirements for an R&D exemption under TSCA. None known. All components are in compliance with the EC Seventh amendmentDirective 

## 92/321EEC. All components are in compliance with the Chemical Substances Control Law ofJapan. This product requires notification before sale in Australia. This productrequires notification before sale in Canada.
htt :llmsds/SearchlDis la Msds.as x 7125/06 

## USA

OtherTSCA Reg. EEC Japan Australia Canada

## ADDCO(R) 365-P


## Switzerland Korea Philippines China
SARA Ext. Haz. Subst. SARA Section 313
SARA 311 Classifications
CERCLA Hazardous Substances FDA Approval
Cal. Prop. 65

U.S. Fuel Registration U.S. Dept of Agriculture NSF Nonfood Compounds Registration Finnish Registration Number Swedish Registration Number Norwegian Registration N t 

## R . t 

## d 0 

## egls ere N

## umb

## er Danish Registration Not Registered 

## Number Swiss Registration Not Registered 

## Number Italian Registration Not Registered 

## Number
http://msds/Search/DisplavMsds.aspx Page 7 of8
All components are in compliance with the Environmentally Hazardous Substances Ordinance in Switzerland. This product requires notification before sale in Korea. All components are in compliance with the Philippines Toxic Substances and Hazardous and Nuclear Wastes Control Act of 1990 (R.A. 

## 6969). This product requires notification in China.



## -- OtherU.S. Federal Regulations

-­ This product does not contain greater than 1.0% ofany chemical substance on the SARA Extremely Hazardous Substances list. This product does not contain greater than 1.0% (greater than 0.1% for carcinogenic substance) ofany chemical substances listed under SARA Section 313. IAcute Hazard Yes Chronic Hazard No lFire Hazard No lReactivity Hazard No None known. Not applicable.



## -- StateRegulations

-­ This product does not intentionally contain any chemicals known by the State ofCalifornia to cause cancer and/or birth defects. Moreover, we do not routinely analyze its products for impurities which may be such chemicals.



## -- ProductRegistrations

-­ Not applicable. This product has not been filed with the USDA to support H2 approvals. This product has not been filed with the NSF to support HI orH2 approvals. Not Registered Not Registered

7f')'i1Of)

## ADDCO(R) 365-P
Korean Registration Number New Zealand Registration Number
TDG Regulated Limit. U.S. TariffHeading Number Schedule B Number Not Registered Not Registered

-- Other I 

## International

-­ None known. Not determined. Not determined. 

# IOther Information Page 8 of8

US NFPA Codes Reactivity Special 

# o NIE (NIE) - 

## None established HMISCodes Health Fire Reactivity 

## 3 1 

# o Precautionary Labels DANGER. • VERY CORROSIVE. CAUSES SKINBURNS. • CAUSES EYE BURNS. • MAY CAUSE RESPIRATORY TRACTIRRITATION. Revision Indicators This MSDS has no revisions since 

## 25 July 2006 The informationpresented herein has been compiledJrom sources consideredto bedependable andis accurate to the bestof The Lubrizol Corporation's knowledge; however, The Lubrizol Corporation makes no warranty whatsoever, expressed or implied of MERCHANT ABILITYOR FITNESS FOR THEPA.RTICULAR PURPOSE, regarding the accuracy of such data orthe results to be obtained from use thereof. The Lubrizol Corporation assumes no responsibility for injury to recipient orto thirdpersons or for anydamage to anyproperty and recipientassumes allsuch risks.



## http://msds/Search/DisplayMsds.asDx 7/25106

## ATTACHMENT 4

Octanol Solubility Test Report 118U92 

## 1. 

## Method This report is based on the attached n-octanol solubility test, GAC 107-A. 

## 2. Sample Identification The sample is identified as a reaction product ofP205 with 2-ethylhexanol and a C12-16 ethoxylated alcohol. Data obtained in this report was determined on pilot scale material made on 2110/2006. 

## 3. Temperature The n-octanol solubility was measured at 23.5± 1DC 

## 4. Test result The test sample was soluble in n-octanol at the following concentrations at the reported temperature: 800 mgIL 41,900 mgIL 105,400 mgIL 190,200 mgIL 420,020 mgIL 646,900 mgIL 787,500 mgIL At all concentrations solutions were clear and no separation occurred after 24 hours. The solubility ofthis material in n-octanol is considered to be 00 

## at 

## 23.5D

## C.

Julv 8,2006 Signature ofAnalyst Date ofTest Completion

## ATTACHMENT 5

Octanol Solubility Test 

## GAC l07-A
Introduction 

## 1. This test method was devised to detennine the solubility in n-octanol ofsubstances that have a water solubility not greater than 50 mg[L. Initial Considerations 

## 2. The specific substances tested by this method are medium to high molecular weight polymeric esters ranging from 500 molecular weight to about 2,100,000 molecular weight. They were, by using GAC method 105-M, detennined to have water solubility not greater than 50 mgJL. 3. All analytical methods attempted failed to provide detection at very low concentration. These included titration, GPC, Ultraviolet spectroscopy and FTIR. Since these are non-volatile materials, gas chromatography was not attempted. 4. This method is intended to be used for substances having water solubility less than 50mg/L. Definitions and Units 

## 5. The octanol solubility ofa substance is the saturation mass concentration ofthe substance in octanol at a given temperature. 6. Octanol solubility is expressed in mass ofsolute pervolume ofsolution. Milligrams/liter is the unit used in this method. Ifthe substance is soluble at all concentrations, it is recorded as 

## a (infinite). Reference Substances 

## 7. Reference substances do not need to be employedwhen investigating a substance Apparatus 

## 8. The following is required: Analytical balance, capable ofaccurately weighing to the nearest O. 

## 1mg a. 50.0 ml volumetric flask b. ASTM Thennometer c. Acetone, reagent grade d. n-octanol, analytical grade

## Description ofthe Method 9. The test is run at the ambient temperature (20-25°C) which is controlled to 

## +1

# 0c. The temperature is recorded and shown in the test report. 10. All glassware is thoroughly cleaned with detergent, rinsed 3 times with distilled water, rinsed 2 times with acetone and finally rinsed 3more times with distilled water and dried in an oven set at 100°C. All glassware must be allowed to equilibrate to ambient temperature before use. 11. The test sample (5.0 grams) is transferred to a tarred 50 ml stoppered volumetric flask and weighed to the nearest O. 1 milligram. 12. The weighed test sample is diluted to the 50 ml mark with n-octanol, stoppered and shaken for 10 minutes. The sample is placed in an ultrasonic bath for 5 minutes, removed and shaken for an additional 10 minutes to ensure complete homogeneity. Ifany particulate matter is observed, this step mustbe repeated before going to the next step. Very high viscosity materials may require additional shaking or ultrasonic treatment. 13. The sample is allowed to stand for 6 hours to re-equilibrate to ambient temperature. 14. Ifthe solution is hazy, the sample is re-shaken for 10 minutes and allowed to stand overnight. Ifthe haze pen:ists or layering is observed, the sample is considered to be insoluble 

## in n­ octanol at the calculated concentration. Note the temperature using the ASTM thermometer. 15. Repeat procedure steps 11 -14 using 10,20,30 and 40 grams oftest sample 

## Test Report 16. The test report must contain the following information:

- The identity ofthe test substance

- The test temperature

- The concentration (s) in mg/L at which n-octanol solubility was observed

## ATTACHMENT 6 Water Solubility Test Report



## 118U93 (ADDCO® 

## 365.P) 

## 1. Method This report is based on the attached water solubility test, GAC 105-M. Since solubility was difficult to discern by visual techniques, the method was modified by using light scattering to determine insolubility. Initial sample was dissolved (0.0659 g) in 50 ml acetone and further dilution was done in 01 

## water. Prior work showed no interference due to acetone. For this substance, some foaming was noted at 2.60 and 1.30 ppm concentrations in water. To ensure accurate ntu readings the sample was placed in an ultrasonic bath for 5-10 seconds to de-gas the samples. 2. Sample Identification The sample is identified as 118U93 is a mixed (2-ethylhexanol and C12-16 alcohol ethoxylate) mono and di-phosphate ester. 3. Temperature The water solubility was measured at 22.2± 1°C. 4. Test result The water solubility was determined to be not greater than 0.6 mgIL at the reported temperature. Light scattering was used to detect solubility. 5. Raw Data Sample Ntu reading Sample ntu, corrected (forblank) <0.1 ntu standard 0.082

. 20 ntu standard 20.8

01

## WaterBlank 0.092 2.60 ppm sample 118U93 0.409,0.387 0.317,0.295 01 

## Water Blank 0.088 <0.1 ntu standard 0.148,0.137 1.30 ppm sample 118U93 0.129,0.132 0.041,0.044 0.65 ppm sample 118U93 0.081,0.087 0,0 i 

## 01 

## Waterblank 0.075 i 

## 20 ntu standard 20.8 i 

## <0.1 ntu standard 0.085

July 13, 2006 Signature ofAnalyst Date ofTest Completion

## ATTACHMENT 7

Water Solubility Test Method GAC 105-:\1 Introduction 1. This test method was devised as an alternative to the two techniques cited in OECD Guideline 105. 

## Initial Considerations 2. The specific substance testedby this method is a medium to high molecular weight polymeric esterranging from 500 molecular weight to about 2,100,000 molecular weight. It was determined to 

## be soluble in l-octanol at all concentrations. It is also, by experience, known to be insoluble in most common polar solvents, and quite insoluble in water. 3, All analytical methods attempted failed to provide detection at very low concentration. These included titration, GPC, Ultraviolet spectroscopy and FfIR. Since this is a non-volatile material, gas chromatography was not attempted. 4. This method is intended to be usedfor substances having water solubility less than lOmgIL. 

## Itis assumed that the introduction of 1-2ml maximum ofacetone ormethanol (steps 12-14 ofthe procedure) may bias the results in the direction ofgreater apparent water solubility and therefore be valid when repcrtmg values less than 10 mgIL. 

## Definitions and Units 5. The water solubility ofa substance is the saturation mass concentration ofthe substance in water at a given temperature. 6. Water solubility is expressedin mass of solute pervolume ofsolution. Milligrams/liter is the unit used in this method. 

## Reference Substances 7. Reference substances do not need to 

## be employed when investigating a substance. 

## Apparatus 8. The following is required: a. Analytical balance, capable ofaccurately weighing to the nearest 

## O. 1 mg. b. 50.0 ml volumetric flask c. 1.0 ml pipette d. 1000 ml graduated cylinder with ground glass stopper. e. Ultrasonic bath f. ASTM Thermometer g. Single distilled water h. Acetone, reagent grade j. Methanol, reagent grade

# ATTACHl\tIENT 7 k. HACH 2100ANTurbidometer (or equivalent) and HACHntu standards 

## Description ofthe Method 9. The test is run at the ambient temperature, which is controlled to ±1°C. The temperature is recorded and shown in the test report. 10. All glassware is thoroughly cleaned with detergent, rinsed 3 times with distilled water, rinsed 2 times with acetone andfinally rinsed 3 more times with distilled water and dried in an oven set at 100°C. All glassware must be allowed to equilibrate to ambient temperature before use. I 1. The test sample (0. 1 to 0.4 grams) is transferred to a tared 50 ml stoppered volumetric flask and weighed to the nearest O. 1 milligram. 12. The weighed test sample is diluted to the 50 ml mark with acetone or methanol, stoppered, and shaken for 10 minutes. The sample is placed in an ultrasonic bath for 5 minutes, removed and shaken for an additional 10 minutes to ensure complete homogeneity. If

## any particulate matter is observed, this step must be repeated before going to the next step. 13. The sample is allowed to standfor 6 hours to re-equilibrate to ambient temperature. Before an aliquot is taken for the next step, the temperature is checked with an ASTM thermometer. 14. Using a calibrated 1.0 ml pipette, an aliquot is transferred to a 1000 nil graduated cylinder. This is then diluted to volume with distilled water, stoppered and shaken forlO minutes. 15. 

## Ifthe solution is hazy after I hour (allowing for entrained air to escape from the liquid), the sample is re-shaken for 10 minutes and allowed to stand overnight. 

## Ifthe haze persists oran "oily" film is observed on the surface, the sample is considered to be insoluble in water. Note the temperature using the ASTM thermometer. 16. 

## Ifthe sample appears clearorifthe analyst is uncertain as to the clarity, the "tubidity" ofthe sample solution is read using the HACHTurbidometerinstrument. Forreference, the distilled water used for dilution in step 14 is read as a "blank" and the <0.1 ntu standard is read. 

## Ifthe ntu reading ofthe sample is greater than 10% above the blank, the sample is considered to be insoluble in water. 

## Test Report 16. The test report must contain the following information:

- The identity ofthe test substance

- The test temperature

- The concentration in mgIL at which insolubility was observed

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# rm InventoryExpert Service
Phone:**80~631.1884,** 

## 614-447·3870 A division of the American Chemical Society 

## Fax: 

## 614-447·3747 E-mail: answers@cas.org Internet: http://www.cas.org/Supportfclient.html 

# ATTA

# CHl\tIENT 15

INVENTORY EXPERT SE::r:ICE RE?ORT

IES-ORDER NUMBER: 920·10
REGISTRY NUMBER: 882693-50-7

CA 

### INDEX NAME 

## Phosphoric acid, mixed mono- and dieste=s with 2-ethyl-l-hexanol and polyethylene glycol mono-C12-16-alkyl e:hers

Please print the above CA Index Name on the appropriate page of your PMN. 

# o If this box is checked, CAS has made correction(s) marked in red to your IES order. Please make the same correction(s) to your PMN before submitting it to the EPA.1

### 12805 87:15 

## 1-854-578-8277 r:5ATEWA\' ADDITI''/E CO PAGE 83


### PMN Page 7 ; Page 9 of 19



# I
I



# I
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## PartI

-- GENERAL INFORMATION

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