NOTIFICATION OF COMPLIANCE STATUS 

Page 1 of 3 

Applicable Rule: 40 CFR Part 63, Subpart N-National Emission Standards for Chromium 

Emissions from Hard and Decorative Chromium Electroplating and 

Chromium Anodizing Tanks 

I. Print or type ~e following for each plant in which chromium electroplating and/or 

chromium anodizing operations are performed. 

Owner/Operatorrritle Mr. Whitby Ellsworth 

Street Address 10 Senexet Road' 

City Putnam State CT Zip Code 06260 

Plant Name National Chromium Company, Inc. 

Plant Phone Number~(8~6~O.l-) " ~92=8=..;;.-7~9~6~S _________________ _ 

Plant Contactlfitle, ________________________ _ 

Plant Address (if different than owner/operator's): 

Street Address, ___________________________ ___ 

City _________________ __ Stare. ______________ _ Zip Code, ______ __ 

2. Complete the following table. If additional lines are needed, make copies of this page. 

Tank Type of Tank Applicable Type of Control Control Method to Test Method Type and Quantity 

101# Emission Limit Technique System Dctcnnine Followed of HAP Emitted' 

101# Compllancel 

ECI34 Hard Chrome 0.015 mgldscm CMPS ECI34 Puformance EPA MJ06 er"'0.0096 

Test mgldscm 

If 8 pertonnance test was conaucted, suomlt me test report containmg me elements requllC4 oy 4U ~r K. 0,,-''I4(8J. 

, If the compliance proccdUICS of 40 CFR 63.344(e) are being followed. aIIach the calculations needed to support the emission limit expressed in mg/hr. 

3. Complete the following table for each control technique used. If additional lines are needed, 

make copies of this page. 

Control System 10 1# Tank 10 I#(s) Range of slle'specific opmtlng parameter valuesl 

EC·134 

Pressure Drop Velocity Pressure Surface Tension Foam Blanket 

Thlekness 

EC·134 5.6 In w.C. NA NA NA 

:tl In. 

If the applicable monitoring and reporting requirements to demonslrale continuous compliance differ &om those In 40 CFR Part 63. subpart N. 

attach D description. Parameter value ranges are established through Initial perfonnancc testing and are those that correspond to emissions at or 

below the level of the standard(s). 
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NOTIFICATION OF COMPLIANCE STATUS (Continued) 

Page 2 of3 

Complete the following if hard chromium electroplating tanks are opened (check the box(es) that 

apply): 

o 

o 

o 

The maximum cumulative potential rectifier capacity of the hard chromium electroplating 

tanks is greater than or equal to 60 million amp-hr/yr. This was detennined by taking the 

sum of the total installed rectifier capacity (amperes) multiplied by 8,400 hourslyr and by 

0.7 for each' tank. 

The maximum cumulative potential rectifier capacity of the hard chromium electroplating 

tanks is less than 60 million amp-hr/yr. This was determined by taking the sum of the 

total installed rectifier· capacity (amperes) multiplied by 8,400 hourslyr and by 0.7 for 

each tank. 

Records show that the facility's previous annual actual rectifier capacity of the hard 

chromium electroplating tanks was less than 60 million amp-yrlhr. If so, submit the 

records' that support this rectifier capacity for any 12-montlr period preceding the 

compliance date, or submit a description of how operations will change to meet this 

rectifier capacity limit. For new sources, the capacity can be that projected for the first 

12-month period of tank operation. 

The facility has accepted or will accept a Federally-enforceable limit of 60 million amphr/yr. on the maximum cumulative potential rectifier capacity of the hard chromium 

electroplating tanks. 

5. Check on of the following boxes that describes the facility's compliance status: 

~ The facility is in compliance with the provisions of 40 CFR Part 63, subpart N. 

o The facility is not in compliance with the provisions of 40 CFR Part 63, subpart N. 

6. Print or type the name and title of the Responsible Official' for the plant: 

Whitby K. Ellsworth President 

Name Title 

A Responsible Official can be: 

• The president, vice-president, secretary, or treasurer of the company that owns the plant; 

• The owner of the plant; 

• The plant engineer or supervisor; 

• A government official if the plant is owned by the Federal, State, City or County 

government; or 

• A ranking military officer if the plant is located on a military base. 
NOTIFICATION OF COMPLIANCE STATUS (Continued) 

Page 3 of 3 

I Certify That An Operation And Maintenance Plan Has Been Completed And The Plan And Other Work 

Practice St dards of 40 CFR 63.342(0 Are Being Followed. 

I 

Date 

I Certify That The Information Contained In This Report Is Accurate And True To The Best Of My 

Knowledge. 

Date 
Po lutant 

Table B 

Hazardous Air Pollutant Analysis 

National Chromium EC -134 

9.14 = Stack Height (m) 

54.86 = Property Une (m) 

54.86 = XMAX 

2.51 = VOl flow (acm/s) 

CAS No. HLV 

Alternate Units: 

30 = Stack Height (ft) 

180 = Property Une (ft) 

51315 = Flow (acfm) 

Table 
Summary of Hex Chrom e Test Results 

I National Chromium Company, Inc. 

Putnam, Connecticut 

I RUN NO.: M306 -0- 11 M306-0-12 M306-0-q AVERAGE 

DATE: 12113/96 12113/96 12113/96 

TIME: 0807 - 1020 1102-1308 1341-1546 

I INPUTS 

PBAR, ( ' Hg) 29.90 29.90 29.90 29.9 

STACK AREA, (f1') 1.230 1.230 1.230 1.2 

I NOZZLE DIA .. (inches) 0.187 0.187 0.187 0.187 

TOTAL TIME, (minutes) 120 120 120 120 

CALIBRATION FACTOR 1.003 1.003 1.003 1.0030 

I PITOT COEFFICIENT 0.84 0.84 0.84 0.84 

SO.RT.DELTA p, ('H,0) 1.3022 1.2390 1.2580 1.2664 

DELTA H, ( ' H, O) 2.08 1.91 1.99 1.99 

METER TEMP., ( ' F) 92 95 96 94 

I STATIC PRESS .. ( ' H, O) - 11.00 -11.00 -11.00 -11 .0 STACK TEMP., ( ' F) 66 61 60 · 62 

METER VOLUME, (ft') 98.531 96.699 96.377 97.202 

TOTAL H, O VAPOR, (rill) 37.1 38.1 37.1 37.4 

CO, IN STACK GAS, (%) 0.0 0.0 0.0 0.0 

0 , IN STACK GAS. (%) 20.9 20.9 20.9 20.9 

CO IN STACK GAS, (%) 0.0 0.0 0.0 0.0 

N, IN STACK GAS, (%) 79.1 79.1 79.1 79.1 

Cr" CATCH, (mg) 0.0259 0.0260 0.0241 0.0253 

OUTPUTS 

METER VOL. STD, (f1') 94.95 92.64 92.18 93.26 

H, O IN STACK GAS, (%) 1.81 1.90 1.86 1.85 

STACK GAS MOLECULAR WT 28.64 28.63 28.63 28.64 

EXCESS ' (%) -118750.0 -118750.0 -118750.0 -1182 50.0 

' GK;G S E( ) 4458.07 4222.24 4282.55 320.95 

GAS FbOWRA, , Befm) 5483 5193 5268 31S 

STP FLOWRATE, (dsefm) 5255 5020 5104 5126 

ISOKINETIC, (%) 97.2 99.2 97.1 97.B 

Cr'" CONC., (ugl .em) 9.231 E+oo 9.579E+OO B.944E+00 9.252E+OO 

Cr+6 CONC., (ug/dscm) 9.632E+OO 9.910E+OO 9.231E+00 9.591 E+OO 

Cr'" CONC., (grl.efj 4.034E-06 4.186E-06 3.908E-06 4.043E-06 

Cr'" CONC .. (grldsefj 4.209E-06 4.330E-06 4.034E-06 4.191E-06 

.r EMISSIOI'IRATE, (11!1llr) 1.B96E-04 1.B63E-04 1.765E-04 . 'lEejs\a:\ 5219c134.wk3 14-Jan-97 Environmental Aisk Limited 

• C ._ 
EXAMPLE CAlCUlATIONS 

I RUn No.: M306-0-11 

Date: 12/13198 

location: National ChromLimCompany, Inc. 

I INPUTS EMISSION CALOJLA 11 ON SYMBOLS 

Pbar "" 29.90 -Barometric pressure, "Hg 

As '" 1.23 -Cross sec:llenal area of cl.Ict. square faot 

On .. 0.187 -Nozzle DIameter, indies 

I Ttot :: 120 - Total samplhg time, mhutes 

y 1.003 -Dry gas meter calibration factor 

Cp "" 0.84 -Pilot tube coeffi:lent. dlm_lenlass 

DPavg ::0 1.3022 -Averago .. are root of velocity head, sqrt(" H2O) 

DHavg 2.08 -Average orifice pressure drop, "H2O 

I Tmavg 92 -Average dry gas meter temperature, degrees F 

Psavg .. -11 -Average duct static p,..sure, "H2O 

Tsavg .. 68 -Average Stack Temperature, degrees F 

Vmtot Q 98.531 - Total meter sample vcWme, cubic feet 

I V1+Vsg :: 37.1 - Total voume of liquid collectlld 

"CO2 :: 0.0 -Percent CO2 by VolUme (dry basis), " 

"02 .. 20.9 -Percent 02 by yclume (dry basis), " 

"CO 0.0 -Percent CO by voLime (dry bals), " 

I "N2 "" 7&.1 - Percent N2 by volume (dry basis), " 

Mn 1:1 0.0259 - Total er+6 collected, mg 

Fuel Input 

"H :: -Percent by weight of hydrogen In fuel 

"C -Percent by weight of carbcn In fuel 

"8 -Percent by weight of sulfur h fuel 

"N .. -Percent by weight of nHrogen In fuel "0 Q -Percent by weight of oxygen In fuel 

GCV ::0 -Gross calorific value of fuel, BTUJlb 

Tstd .. 68 -Standard Temperature, degrees F 

Pstd = 29.92 -Standard Pressure, ~g 

Lp .. -Frea/ Leak Rate of Samplhg Train, cfm 

La -Allowable Leak Rate d Sampling Train, cfm 

t. Volume d Sample Measured By Dry Gas Meter, Corrected to Standard Conditions rim ltd) 

.. Vmtotal x Y x Tstd + 460 x Pbar + DH§ £13.8 

Tmavg + 460 Psld 

98.531 x 1.003 x 68 + 460 x 29.& + 2.08£13.8 

92 + 460 29.92 

Vmsld= 94.&5 dscf 

2. Molstlre Content at Duct Gas ("H20) 

.. 0.04707 x (VI + Vsg' 

Vm std + 0.04707 x (VI + Vsg) 

0.04707 x 37.1 

94.9498 + 0.04707 x 37.1 

"H2O .. 1.81 " 

ejs\a:\M308caIc.wk3 14-Jan-&7 environmental Risk Umited 
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3. Molecular Weight of Stack GAS (MWa) 

.. {( 0.44 X "C02) + (0.28 l( 

= {( 0.44 X 0.0 ) + (0.28 X 

MWs EO 28.64 Ibllb molo 

4. AI/Vage Ouct Gas Density (0" 

.. 0.0458 X MWs 

=0.0458 X 28.6403 

Ost .. 0.073 Iba I cubic 1eot 

%CO ) + (0.28 l( "N2 ) + (0.32 X 

0.0 ) + (0.28 X 79.1) + (0.32 l( 

X Pbar + ( Ps avg l13.8) 

Taavg + 480 

X 29.9 + ( -11 l13.8) 

88 + 480 

'J(,02 )} X (1 - "H2O) + (0.18 X "H20) 

100 

2O.9)} X (1 -....!.:!!J + (0.18 X 1.806) 

100 

I 5. Excess Air (EA) 

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.. 100 

0.284 

a 100 

0.284 

EA '" -118750" 

8. Average Duct Velocity (Vs) 

= 5129.4 X 

'" 5129.4 X 

x 

X 

X 

X 

Cp 

0.84 

Va.. 4458.1 1tImin 

7. OUctVCllumetrb Fbw Rate, (a) 

Vs X 

.. 4458.07 x 

A.. 5483 acfm 

o;S\a:\M308cIllc. wk3 

( 0.5 X "CO ) 

( %02 - (0.5 X "CO)) 

20.9 - ( O.S X 0 ) 

79.1 - ( 20.9 - (0.5 X 0» 

X OPavg l( SORT { Ts avg + 460 } 

( P b. + Ps avg /13.6) l( MW 

X 1.302 x SORT { 88+460 } 

29.9 + -11 /13.6} X 28.8 

1.23 

14-Jan-97 Environmental Risk Umhd 
8. Cuct VofumeCri: Fbw RIa, Ccmcted to Dry S1IIndarct Condlllons, (Osta) 

=> Q x (1 - .. H20 I x (",T8::.:tet=-_..,.:+ ... 48~O;,....o) X ( .... P-=b"" ........ -:-:-+:--.:..P..:S-=II .. 1tIS ....... /:,:13 ..... 8:.-..J 

100 Ts avg + 480 P std 

5483.43 x (1 -

Qstet a 5255 dscfm 

9. lsokincrtfc Fc1cr. ~) 

1.80598 I X 

100 

88 + 480 I x (_-=29:,:.::::,9.......,...;;+-=-__ -..,.:1:,:.1..1./,!;13:,: • .:::.6--J 

66 + 480 29.92 

::::~ _________ ~~ ___ ~ ___ ..:5~.87~=X~rn..:s..:eN .. g __ ~+~~~~x ____ V~m~s=td~~~~ ___ ~~~~~~ 

( P b. + Ps eNg ) X Vs X Ttot X (1 - "H20) X ( Dn '2 X 0.7854 ) 

13.8 100 144 

=> ______ ~----------~----..:5~.87~~x~(--...:66~-+-480~~)~X~--~~94~.~95:.-~~~ ____ ~~~~~~ 

29.9 + __ ':':-~1,~) X 4458.1 X 120 X (1 - 1.808 ) X 0.03 X 0.7854 ) 

13.8 100 144 

I=> 97.2" 

1 O. Actual Conc:entraIfon, grains/acf, (C) 

0.01543 x Mn X (TStd + 480) X (P b. + PSeNS X (1 - "H2O) 

13.8 100 

Vm stet X (Ts eNg + 480) X Pstct a _________ ~~~~----~~--__ --~~--~~~-__ -----~~---

0.01543 X 0.0259 X (88 + 460) X ( 29.9 + -11 X (1 - 1.808 ) 

13.6 100 ::::----------.......,~~~--~---'="-~~-~--~~~---------~:.---- 94.9498 X ( 66 + 460) X 29.92 

C :::: 4.03E-08 grans/act 

10&. Actual CCl'lContrstlcn bead en stack ccndlllcns, uglacm. (Ct) 

1000 X Mn X (Tstd + 460) X (P b. + PlleNg X (1 - .. H20 ) :::: 13.8 100 

0.02832 Vmstd X ( Tsavg + 480) X P Std 

1000 x 0.0259 X (88 + 480) X ( 29.9 + -11 X (1 - 1.808 ) :::: 13.8 100 

0.02832 94.9498 X ( 68 + 480) X 29.92 

C, :r 9.23 ug/acm 

ejJ\a:\M306calc. wk3 14-Jan-97 EnvIronmen1al RIsk Umled 
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11. eaicenfratlOn, ComIcted ID Dry Standard CondItIoN, (Ca) 

'" 0.01543 x 

'" 0.01543 x 

Cs'" 4.21E-06 grJd&ef 

12. Emiiak:n Ru, (ER) 

'" 0.008S71 x 

'" 0.008S71 x 

ER", 1.90E-04 /bsJhr 

ep\a:\M306ca/c wk3 

Mn 

Vmstd 

0.0259 

94.9498 

Cs x 

4.21E-08 ic 

Qstd 

52SS.1 

14-Jan-97 Envircnmen1al RIsk Umllltd 
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TEST OF TANKS EC 1, 3, AND 4 COMPOSITE MESH PAD CONTROL DEVICE 

DECEMBER 13, 1996 

RECORD OF TANK Ee - 1 

.;.-

COMPOSITE MESH TANK 

TIME ' VOLTAGE AMPERAGE PAD DBLTA P TEMP 

" 

STAGES 1 .THRU • 4:--_..:..'_ ttl .,; 

1ST RUN 

-----------------------------------------------------------------------------

..... 

2ND RUN 

------------------------------------------------------------------------------

__ ::~~: _ ----lJ-:-@.A---~-----~!.-3_ ----~---6~~- __ ~ ______________ ~_! 11 __ _ _ _ ~:=~~= ____ -I-LS-~-- __ ~ _____ ~-'-1;."--- _ ~ ___ k~'[£ ____ ~ ______________ ~_~_~'i .. ,_ 

." _:~~ ________ J_~ J~~ ____ ~ _____ 9!J ______ ~ ___ te}_lL ____ : ______________ ~ __ ~?3 __ RUN A\"G 

3RD RUN 

--~;~;;--------:-----\~~1;--------,t;----~----C56b-----~-- --~---------~-J3-----·: 

-------------~-----------~----------------------------------------~---. -_~:~~~~ ______ ~~~~ ____ ~ ______ 1~~ _____ : ____ ~~~ _____ ~ ______________ ~_~~~---: 

--~~~-------~-~~\----~-----i-·~----~- ___ (p_~Jm.---_~ ______________ :_!1~ __ 

RUN A\"G 

------------------------------------------------------------------------------ THREE R:JN 

AVERAG!; 

-----------------------------------------------------------------------------

FILENAM~: EPATEST1 

Decembe= 13, 1996, 8:18 AM 
·1 

I 

TEST OF TANKS EC 1, 3, AND 4 COMPOSITE MESH PAD CONTROL DEVICE 

DECEMBER 13, 1996 

I RECORD 'OF TANK EC -3 

COMPOSITE MESH TANK 

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TIME , VOLTAGE AMPERAGE PAD DELTA P TEMP 

'. STAGES 1 THRU 4 F · " 

1ST RUN 

MIDDLE 

END "' ~ , W : : '-'1 (j7): . : / 3 'J 

--------------~---------------------------------------------------------~---- RUN AVG" . 

RUN AVG 

3RD RUN 

__ ~:~~~ _____ _L~_~L----~-----~~-t2----~-----~-~~--~------ ________ ~ __ ~_~~ -_~:~~~: _____ Z:.~~1@. ___ ~ ____ j31~-----~-----?:@!:C--~------ ________ ~ __ !_~_~_.: 

--~~~---------~-~-~--~-----:r~L-----~-----~1ta2----~----- _________ ~ __ 1~_~~ RUN AVG 

THREE RUN 

AVERAGE 

FILENAME: EPATEST1 

December 13, 1996, 8:18 AM 
• 

I 

TEST OF TANKS EC 1, 3, AND 4 COMPOSITE MESH PAD CONTROL DEVICE 

I DECEMBER 13, 1996 

I RECORD OF TANK EC - ~ 

1ST RUN 

RUN AVG 

• 

. ~ 

TIME VOLTAGE 

'., 

COMPOSITE MESH TANK 

AMPERAGE PAD DELTA P TEMP 

• STAGES 1 THRU ·4 F 'oJ 

" 

I ~~;~~;;-----_J~-~------:q------~--~-~-S:C;----~---~:~-----~-~~Z--. --------------LD-~---------~-------------------------- -------- ___________ ~_. --~ =:~ ~ ~ ------Lt-'L ~ ---~ ----j Q .i ~ - - _ - ~ - __ 31 d'D _ -___ ~ ____ ~ :. ~ ______ ~ __ t }I _ . ...... . 

--:~: _________ J_'!_~_') ____ ~ ____ LQ-·5.-----~---~j-@-----~ ----~~~----:_~-L-~i.- RUN AVG 

3RD RUN 

~~~~~~~~~~~]~~~~~~~~~~~~~~:l~:~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~[~~~: --~~~~~:_· ___ k~,_'i~ ____ ~ ____ L~·_k_ ____ ~ __ 3~~~ ____________________ : __ ~~_ . 

--:~~---- ____ ~~~~1 ___ ~ ____ J_Q_~~ ___ ~ ___ :s_E?_~ __________ ____________ !_~ 

RUN AVG 

----------------------------------------------------------------------------_. 

THREE RUN 

AVERAGE 

-----------------------------------------------------------------------------

FILENAME: EPATEST1 

December 13, 1996, 8:18 AM 
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:~~~~Cl DATA FOR JESTING OF EC-!3~ OK ore 13, 1996 

• ·!~/~:';-::6 l~! SiAGE ~Aj) C:l:;~j;';':iiD/j 

" .. 

c 0 ' .,. ~" 

t~,L3,;:£ =nc STAGE ~:.O CO!-fSTn~:~:~:t 

~.~: !~~ STAGE PAD CONSTRUCTIOH 

~t~ STAGE PAD CONSiRUCTION 

BlONER enl 

AREA OF ROUND mIRE CONTROL PAD IN SQUARE fEET . 

VELOCITY ACROSS ROUND ~IKRE CONTROL PADS - FPH 

ARE~ OF ~EC;~NGUL;'F. ;.:: :CIiTROL PADS IN SQUARE fEET 

'1£~JCiT'; ~CR9S£' SC!JAR£ ;;CS CONTROL PADS - FPrt 

~.-----" 

\ '. ' -

q : lIL 

dF - HullD ;.r,~ Fi\t -~G:iTRGl ~ ,8 ~9-1st STAGE JF CON!EC~ ~~~ dP-ls t STAGE DF COHiROL OEV 0 . q 

or. ~- •• -,~. "If ·O .... ROl "IE"" \ .• ~-.; ..... :.~\!, IJ : ... i1, :'" L... ~~-2nd STAGE QF CONTROL ~E~ dP-2nd ST~GE Of COH;~Ot DEV ~,~ S" 

: .::~ ~-~~E OF C~NTROl DEY 

dP-3rd STAGE OF CONTROL )EV 1, OE:' dP-3rd STAGE IJF CONTROL DEV 

: -Hh ~TAGE OF t;ONir.C~ f.fV I .05 d -4th STAGE OF CONTROL DEV 

,j?-~~"PlETE eOHTRO~ ~EY::E 5. S dP-COrtPLETE CONTROL DEnCE 

~p - ~~~: ~:IC CGHTROL DEVICE (b.L> tiP - HOOD AHD CONTROL Dr,;iC£ I O. ~ dP - HOOD AND CCHiROL DEVICE 

::;g;"il ,.[VI;£ Ii HOOD auiG .mE' ;DNN CDNTlH DUS Y ~r ~~ I~ r:/ '11/ :~!:l :~:::~'~: OH IfILDEN PUtfP. IfASHOOWN ~rQUrD BErHG I:SED rs F:~$~ 

,~riRG~! ~H'SE. ,:OHTlHIJIJUSLY RE-CI::tCUl~i(i), 

FILE: ~i~rEST/TESTDOCS/TSTECll4 

De:~~ter 13. 1996, 8:58 A~ 

( .f>$"' 

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TEST CONTROL DATA fOR TESTING OF Ee-134 ON DEC 13, 1996 

SAHPLIHG SITE AHD TEST HO. EC134 PRE-COHTROL PAD.CONSTRUCTION 

TANI NUHBERS EC I, 3, AHD 4 

DATE AND TIllE n , i'; Jj./13/96 I V' . ..,Oft ~ TEST OPERATORS , lG,LG~lfE 

STACK RADIUS IN IN. 7.81 

BAROKETER, Pbar, in Hg 

INSIDE TEHPERATURE 

OUTSIDE TEHPERATURE , 

TEST RUN RECTIFIER AHPS "I', 

TEST RUN RECTIFIER VOLTAGE 

TANK TEHPERATURE 

dP REA[\!NG~ ~r ~~~~r OF ::,:L 

1st STAGE PAD CONSTRUCTION 

2nd'STAGE PAD CONSTRUCTION " 

lrd STAGE PAD CONSTRUCTION 

4th STAGE PAO CONSTRUCTION 

BLOIER CFII 

ARE~ OF ROUND KIHRE CONTROL PAD IN SQUARE FEE! 

VELOCITY ACROSS ROUND IINRE CONTROL PADS - FPH 

AREA Of RECTANGULAR ACS CONTROL PADS IN SQUARE FEET 

VELOCITY ACROSS SQUARE ACS CONTROL PAOS - fPII 

dP R(~C:HGS AFTER TIfO HGl'?$ ~f !\:.:; 

TIHE Of REAO!~G I~r 1.'DS

dP - HOOD AHO PRE -COtHROl L}. t; 

dP-lst STAGE OF CONTROL DEY • G)~­

ItP - HOOD AHD PRE-CONTROL 5, ~ dP - HOOD AHD PRE-CONTROL 

.., 

dP-!st STAGE OF CONTROL DEV • GJ~ dP-lst STAGE OF CONTROL OEV 

dP-2nd STAGE Of CONTROL DEV ~,~ dP-2nd STAGE or CONTROL DEY 

dP-lrd STAGE Of CONTROL DEV I. 6t{' dP-3rd STAGE Of CONTROL DEY 

(" . 

"2... S.I dP-2nd STAGE OF CONTROL DEV 

/ 

· q ~ dP-3rd STAGE OF CONTROL OEV 

d -4th STAGE OF CONTROL DEV } ·b ~ d -4th STAGE Of CONTROL DEV J,e> d -4th STAGE OF CONTROL OEV 

dP-CDIIPlETE COHTROl DEVICE 5. ~ dP-CDHPl£TE CONTROL DEVICE !5. 4 dP-COllPlETE CONTROL DEVICE 

dP - HOOD ANIl CONTROL DEVICE 10 .ll dP - HOOD AHD CONTROL DEVICE f () · ~ dP - HOOD AND CONTROL DEVICE 

:::~~rRDL DEVICE IN HOGO BEING lASHED DO •• ~US~) 1 ~ ~ (~(:, /16 

AIR PRESSURE ON N!tOEH PUftP .• ASHDOlfN LIQUID eE!NG USED IS FIRST 

CHRDftE RINSE, COHiIHUOUSLY RE-CIRCULATED. 

fILE: AIRTEST/TESTOOCS/TSTECI34 

Decelber Il, 1996. 8:58 AH 

~5-, 

.q 

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,<15 - , 1~-

5~~ 

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TEST CONTROL DATA FOR TESTING OF EC-134 OK DEC 13, 1996 

SAltPlIHG SITE AHD TEST NO. ECll4 PRE-CONTROL PAD CONSTRUCTION 

TANK HUHBERS 

DATE AHD TIllE 

TEST OPERATORS " 

STACK RADIUS IN IN. 

BAROMETER. Pbar. in Hg 

IHSIDE TEMPERATURE 

OUTSIDE TEMPERATURE . 

TEST RUM RECTIFIER AKPS 

EC 1, 3. AHD 4 5 rLD (2).11'1 

12/13/96 1st STAGE PAD COHSTAUCTIOI i . 

~ lG.lG.'E 2nd' STAGE PAD COKSTRUCTIOI 

7.81 lrd STAGE PAD CONSTRUCTION 

4th STAGE PAD CONSTRUCTION 

BlOWER CfN 

AREA 9F ROUND UtlRE CONTROL PAD II SQUARE rEET . 

VELOCITY ACROSS ROUND KINRE COITAOL PADS - FP" 

.~. 

TEST RUN RECTIfiER VOLTAGE AREA or RECTANGULAR ACS CONTROL PADS IN SQUARE FEET 

TANK TEHPERATURE VELOCITY ACROSS SQUARE ACS COHTROl PADS - fPH 

...... ~:.:~OlNGS AT START or RUN dP READ!NGS AriER OH£ l:2.JR OF RUH dP READINGS Af7ER THO HOURS Of RUN 

TIllE Of READING \ '.~J P ~'I~~ 3:Y8 

dP - HOO~ AHD PRE-CONTROL ~I) dP - HOOD AND PRE-CONTROL 5.~ dP - HOOD AND PRE-CONTROL $,5 

dP-lst STAGE Of CONTROL OEY ,l1 dP-lst STAGE or CONTROL DEV . ~z.!' dP-1st STAGE Of CONTROL OEV ·1 t ~",-

dP-2nd STAGE Of CONTROL OEV 2,$'"' dP-2nd STAGE or CONTROL DEY '2.,( dP-2nd STAGE Of CONTROL DEY 2, rl.~ - / , 

dP-3rd STAGE Of CONTROL OEV • ")~ dP-3rd STAGE Of CONTROL DEY ·tJ~ dP-3rd STAGE Of CONTROL DEY ,17r 

d -4th STAGE Of CONTROL DEY .'11~ " d -4th STAGE Of CONTROL DEY .&)( d -4th STAGE Of CONTROL DEV , 17~ - 5 . .3( dP-COItPlETE COHTROL DEVICE ~.3 

,.. dP-CDltPlETE CONTROL OEVICE dP-COltPLETE CONTROL DEVICE t;", ,/-Z) 

dP - HOOD AND CONTROL DEVICE , 0, B dP - HOOD AND CONTROL DEVICE 10. '0 dP - HOOD AND CONTROL DEVICE I 0 .g 

HOTES; 

PRECONTROL DEVICE 1M HOOD BEING lASHED OOIN CONTINUOUSLY AT 20 PSI 

AIR PRESSURE OM WILDEH PUHP. WASHOO.! LIQUID BEING USED IS FIRST 

CHROltE RINSE, CONTINUOUSLY RE-CIRCULATED. 

fILE: AIRTEST/TESTOOCS/TSTECIJ4 

Deceiber 13, 1996, 8:58 Alt 
cC -' /_,1-

/'19ft.,..., I (Iva,.., ......... 

fiRM lAME 111} ... ~1r - (\" 1/ 

PUMT LOCATION tt,;.,.,.,.,..... ( T 

IUN NUMBER "YJ ,~~_ (,' . C. I •• II 

flELP PAl A 'HEET 

SAMPLING LOCATION ___ _ 

C'fA I-/ C' r ,. 

. '. 

TESTER ___ -...;. ____ _ 

t i 

I 'RAVERSE I SAMPLE 

TIME 

(1IIn) 

CLOCIC 

TIME 

MODULE NO. 1,':1"/,/ 

SlAcr; PRESSURE (In'"20) .• d.o 

BAl. PRESSURE J? Y (."1 

PROBE 10 NO. __ """+._C""l/ ___ _ 

fILTER ID 1110. NA --...... ~!""---- fiLTER TARE UT. A/A 

NOZZLE NO./DIA.Cln.) :: •. ,87 C, 

DUC' AREA (,,2) I· ..t ..l 

) 

ASSUMED MOISTURE (I) ~_' ... "'__ _ 

I £S T DURA Tl 011 / ~' .:) 

IRAVERSE POINT INTERVAL ;'() 

PIOBE HEATER SETTIIiG ___ N_'_,f.~_ 

flLlEl HEATING SETTING __ N ... '_.f_ 

LEAIC CHECIC: 

INNIfIAL O.~ I -_ t,., 

.. _--

fiNAL (f, tJ " 8 _i'-,,--__ _ 

DR' GAS M£TEI Y ____ i. CO ~~ ... 

PlTOt COEFfiCIENT _ C· ii't 

NOMOGRAPH C fACTOR ' 151. ( 

MODULE AHA / 4' r 

TEST STAIT TIME )7~~u;Z TEST fiNAL TIME • ~ ~ 

AMBI Ell TEMP. "j "f 

£c"- /3., 

i 

VELOCITY I 

HEAD(6P) t 

(In. H20) , 

OlU ICE 

OM 

Iii I 

1 DGN I DGM I STACIC I GAS SAMPLE 

Iii iii 

t fiLTER I CONDENSOR l HEATER , PROBE I PUMP I 

1 Til 1" 1 T. outl TEMP. I VOLUME V. 

1 0, I Of 

, 1 I 

I I I Z4 I I 

OUTlET 0; BOX 'TEMP. 0, I , 

I 

I 

i

fl

r--~~--~~-r~r.-~~~~--~~~~-r~~~~r-~~~~~~---r-T---r--~~-+~~-+~~~~-i(~

~--~~~~---+~----+=~~~-r~~~-+-~~~~~~~~~~~~-+--~-+~~~-+--~~----~~~~ r

I 1 I 1 I 1 1 1 I 1 

I 1 I I I I 1 1 1 I 

1 I I 1 I I I I 1 I 

I I I 1 'I I 1 I I I 

I I I 1 I I 1 I I I 

, I I I 1 I I 1 I I 

I t I I , I I I I I 

i , I 

AVERAGE 1 L{Ei I' 

1 t 

L 

g 

I ' ,*0')" 

"20 COLLECTED .t. 

:i!:!I' I I S. G. W£lGH' gr. 

TOTAL VOLU"E 111 f _l. '6~ COLLECTED (,) 

/.5" ~O 11.., 

~) , f) • 

I 1 I I I I I 

1 TOTAL I 1 I .1 , I 

1 I I I 

I ~~I >Jl 

d:,s - ft ,..,..,ro c../-e ,;, 1~,.."."".1). 

COM"EIITS ~ 

;'" f'" 511-").. 

cI ... ot k ~{" .1. of"-F 

ff'uJ.. 

I royJ. {J II ':' / cJ • .:--:t . 

, I , 

J . Q 9 ORSAT BAG ANAfIrtt S ~~ TRIPLICATE ANALYSIS 

CO2 02 CO liZ 

0 .)f1.' r~.1 

0 ,1tJ.' 1', I 

0 ~(J.1 7-.,. I 
E( - / 3.:j FIELD pAT A SHEET 

, 

ASSUMED MOISTURE (I) "" 

TEST DURU ION t.fi!..C' 

TRAVERSE POINT INTERVAL Ie 

PRoaE HEATER SETTING ,Aj.# 

FILTER HEATING SETTING . .v~ 

.' "~'~'i FIRM lAME Nu 1-, ••.. .,:.:/ ( ;,': .... -ltODULE NO. I ) .• 

PUN'LOCATION / .... )" .• .,,..\,, :.~ STACIC PRESSURE (In.H20) "/1.<::.' 

RUN NUMBER ,YI. ?~"cl.. - <. I - / ). BAR. PRESSURE ; J '/. "; \ 

SAMPL ING LOCAl ION PROBE 10 NO. :} (.. .. i ------~~------ "b I- I (I f f I LT£R 10 110. A/A 

PROJECT NUMBER . '5ln~f - S·;: - FILTER TARE \IT. Ai .. LEAIC CMECIC: 

INNITIAL O,elC) a lFIliAL 0, "0 a ~ 

DATE ,JJ, JI<jb IIOZZLE 1I0./0IA.On.) .. :" lEo? (z 

TESTER .J... .4 s., DUCT AREA (f,2) / . .,) ~ 

I I 

TRAVERSE I SAMPLE CLOCK VELOCITY ORI flCE , FILTER 

POJNT I TIME TIME HEADCAP) AH , OUTLET 

I (IIItn) (hour.) Cln. H2O) 0, 

I (j 

13- I I , I .... 

I I I I I 

I I I I I 

I I I I I 

I I I I I 

I I I I I 

I I I , I 

I , I I I I 

I AVERAGE 

I I I I I 

I L"~p r I I I I , , 

I 

I TOTAL 

I I 

IlII OASU BAa f..AUS I S (" 

I %.~,t1 

"ZO COLLECTED 

S. G. WEIGHT 

TOTAL VOLUME 

COLLECtED 

1.3 -,. A'~' I gr. 

_·1 __ ~.:..' "",' __ -, • 

/,.1 31 TRIPLICATE ANALYSIS 

CO2 O2 CO liZ . COMMENTS 

0 -'D. 1 ~'l. ( 

0 !J".~ .,. ft. I 

~ ~.;I··I Y. "I. ( 

/f.f'" 

Sl~) ,Ft" oS 

':;J4J Ju 

DRY GAS METER Y /. c't) J 

PITOT COEFFICIENT (,. elf 

MOMOGRAPH C FACTOR ~Z~L...I! 

MODULE AHA I 1£.1 

TEST START TIME 'l (.J.)... 

TEST FINAL TIME / ?('fl 

AMBI Ellt TEMP. 0'" 

Ec I.J1 

I i I i i 

I CONDEIISOR I .HEATER I PROBE I PUMP I 

I OUTLn BOX 

I OF of 

I I I I I 

I I I I I 

I I I I I 

I I I I I 

I I I I I 

I I I , I 

I I I I I 

I I I I I 

I I I I I 

.:r ,....,e.. ill 1.;)·(' 
fIRM lAME N . .,I"I '·A/., ~-.I""'" 

PLANT LOCA II Oil '-1 hI:" '~', (. i o 

RUN NUMIER ,..., 3(1"" - (J - I' 1 

SAMPLiNG LOCATION ___ _ 

O ...... f/~ f 

PROJECT IIUM~ER .;feoJ l r ~!;.-

DATE I,,! Ir 1 / 'f <.. 

TESTER 0 L_ ',4 9 

TRAVERSE SAMPLE CLOCK 

POINT TIME TIME 

(_In) (hours) 

I 

I 

I 

I 

I 

I 

I 

I 

I AVERAGE 

H20 COLLECTED 10 _l. 

S. G. "EIGHT :Z. ;tel gr. 

TOTAL VOLUME .,J.1JIl. l _l • 

• COLLECTED 

3 ' c.;". L,.) 

~b1. 1 

£(. - t.? f-

/_.' / 1 

f'ELD DATA SHEE! 

MODULE NO. ___ -_____ _ 

STACK PRESSURE (In.H20) - //. ,-l 

BAR. PRESSURE . ~ ? .. (f.. .. 

PROBE ID 110. t' ... ' I 

fiLTER 10 10. ~'~ 

fiLTER TARE WT. 'V·~ 

NOZZlE NO./DIA.(ln.) S .... I c:.7 e;; 

DUCT AREA Cft2) I. ~ ~ 

I I 

ASSUMED MOISTURE (I) _..;;.&A_' __ _ 

tEST DURATlOII / ,,"', 

TRAVERSE POI.' IlInRVAL __ .I~(~I _ 

PROlE HEATER SEIfUIG _~cV~'+:-._ 

fiLTER HEATlIG SETTIIG _~<\~/:..· f,,--_ 

LEAIC CHECIC: 

INNIT IAL 

'INAL 

I 

Q. c./e:" 

I 

I C _ a --,/~,.;.." ('-(~i_ 

I I 

DRY GAS METER Y /# CJcJ.? 

PltOT COEfflCIEliT 9.' £>1-

NOMOGRAPH C fAC!OR7~~ !: 

MODULE AHA J. ~ 'l 

TEST STAn TIME I, l' ., i 

TEST fiNAL TIME ' .t) teo 

AMIIENT TEMP. (,4 

Fe: - /.31-

I I I i 

VElOCITY ORIfiCE I DGM I DGIt I STACIC I GAS SAMPLE I filTER I CONDENSOI I HEATER I PROBE I PUMP I 

HEAD(I1P) ~H I Tm In I ,. outl tEMP. I VOLUME V. I OUTLET I OUTLET I 'lOX I TEMP. I VAC. I 

(In. H2O) I Of I Of I ,. 0, I CUIIC 'EET I OF I 0, I 0, I f lin. HII 

I I I , . . ..]1.1 I , , I I I 

I I I I I I I I I , 

I I I I I I I I I , 

I I I I I I I I I I 

I I I I I I I I I I 

I . I I I I I I I I I 

I I I I I I I I I I 

I I t I I I I I I I 

I I I I I I I I 

I I I I TOTAL I I I I I , I I I , 

I. 9 .J ilORSAT BAG ANl~ tys I S Coo I Zb.3..;r;z.. I 

I r:.{E.P I 

I r 

I I 

/ • .J S? TRIPLICATE ANALYSIS 

1U CO2 O2 CO "2 COMMENTS 

'-7 ~ r .. ) ;).. 

-- (.) 1,2(},1 2-1./ 

d i,.tu. '1 r9, I 

t5 .,.J.D· , "7Y,/ 

01&0 

- -9 c",-/ 
,,-

Date: ~- 073· 91c 

Bar. Ps., (Pb): 3'L·S,Q in. Hg 

Standard Merer 

Moctale Velum. Temp. Pressure 

Oritice Va Factor ts fa 

Setting tIP) Va rF) (in. H2O) 

(in. H2O) 

0.5 :5.003 1 (·(,,=--9 fDf' -D.' 

1 ."5.003 I. o()~,:J "If -f) J 

1.5 16.CO.5 1.0001 (oy -0 I 

2 10.IDlo loo(o4 1011' -{} I 

3 10 109' /.01)109 fR1l. -6.1 

For cMck. use She average6Ha for AH 

Va(Pb + Ps 1 (Tm + 460) V. 

Va 

Q Q 

OrtIce factor = 

13.6 

Vm (pb + AH ) (T. + 460) 

13.8 

(0.0317) AH 

Pb (tm + 460) 

V (17.64) Vm 

[(f. + 460) AH 

( Pb 

((Is + 460) @ P 

(VI VIJa 

(pb + AH 

13.6 

(tm + 460) @ 

.J¥a 

I~ 

~ 

) 

,, 

UalhociS Module Calibration 

ModJJe#: 1399 

Std. Meter: 51<>4IS P,.-tat I Peat-test 

Moctale Meter 

Velume Temperatures nme Mowle 

Vm 1mI bno @ AHa Ftowrata 

(ft3) (Of) f'F) (arin) Y (In. H2O) Q 

. {SCFMl OF 

5 144 r4 7'1 IcJ. OJ3 J. 0010 llDl 10.411 .. ) 30t>h9 

5" Jlb9 i>w 7?' ~,PS • CfCJ70 I fo9 O.5w 7-9 14.9513 

10 ;)101 

1(') ~4 

I_O,.""h}S 

.' 

~ -rq 14.0? j, OC>(P~ L73. IO.Inf-4.~ I, ~4'l 

rl. PI /.:J. Ps 1. 005? I. '73 10.790/ g~ ?3 10 . .3i' i I. AIO.AJ. J fo9 oq7~ 

AveraS- I. 0030 /. to't_ 

I:: 

AcceptMce Cdterla: 

Conelation Una Equalion 

Q GI m (Of) + b 

Each V nust be 1.00 = 0.01 

AverageAtial1'llltbe 1.84 % 0.25 

EadlAHa l11li1 be wbhIn 0.15 of the 

awnageAHa 

[1;1 l::fl . D.OOO U;-~a.kl I ;;i~ 

Heater Box ~CCIntrd a<: 

Probe Heater Low Contra OK: 

MocUe Cleaned: 

Ppot Tube ManometIr LMk Check: SF 

1&,0443 

7. 4J • .J9 

CaIibratad ~d Chec:Md ~ J"€C. Date: 7- ot3 -9" 

R8\4ewed~ -7~c Dm,: 7-~3'9b 
'. 

D t / .. - ,!) -

•• : _~IfO:_._-_: "'4_. _"-.--7 ...... 1'",...-

Bar. P ••• (Pb): ..... "' t. <;-,.t In. Hg . 

Standard Meter 

Moctde Volume Temp. P .... ure 

Orile. Vs Factor Is Pa 

SetUng (ft') Va rFl (In. H2O) 

(In. H2O) 

,).0 6._~ ,'. c:c.:·b 7~ -0. ,...!.. - ,.J.e 4/ 0/4- L ,OcJ "'" 7..< -O.~ 

f..J·e _~ lc...~ /,.~ub '9.;1. - cJ .ol 

For check. ",e1he awrageAHa for AH 

Y. 

Vs (pb + PI ) (1m + 460) Y. 

13.6 

Vm (pb + AH ) (Ta + 460 ) 

13.6 

AHa .. (0.03171 AH ((Is + 460) @ )2 

Pb (1m + 460) ( V. Va p 

(pb + AH ) 

Q • Y (17.64) Vm 13.6 

(bn + 460) @ 

Oritc. factor = (Cr. + 460) AH J~ 

( Pb )~ 

Method 5 Moclile Calibration 

ModIle #: J.~~'i i 

Std. Meter: F~ la -II SMowle Meter 

Volume TemperabJres 11me 

Vm tmI tmo @ 

(ft') rF) rF) (nin) 

~.S';.·-:- 9b f).;l 8,"" 

4.113 t:t;z. 33 !!:",uv 

(,. Six 'J'S' as 8. Cia 

~wraaMoctII. 

AHa Flowrate 

Y (In. H2O) Q 

. (SCFM) 

I,Oi3 /.70 cJ 73' 

I.O()9 1,{Q't o , l'1a 

j. '9% /. 'i.4. c,. 7(PC) 

. 

I. adl /, ~.,.. 

~"'"C"""a: Conalallon Una Equation 

Qmm{OF) + b 

Each Y .... t be 1.00 + or - 0.01 

I~ tmo 

If 

7t 

A .. geAHa .... tbe 1.84 :t 0.25 

Each AHa .... t be within 0.15 or .. ... ge6Ha 

Heeter Box lJwe Cantrd 0<: 

Prcbe Heater LoveCantrd 0(:---

MoclIIe CIeIned: \7, 

PIlot Tube Manometer .... Check: \7' 

OF 

CeUbrated and Checked by: L tIc>. Data: /~.:r~"" "f 

R..tewadby: 6~=< ~ Data: /~Jd'\ 97-
~I 

, 

, 

I 

I 

, 

I 

I ... 

, 

I 

1 

.-

A. 

S. 

·S-TYPE PITOT GEOMETRIC CALIBRATION 

PART 1 - PROBE CONFIGURAiION 

~Identif1caticn _~_i1_/ __ _ Pi tat Ident; fi c:a ti on _V4_"_r __ _ iechnicat Specialfst ~~" 

Date ~~ 

P1tot 

) .. ~ Probe l Nozzle J: r-

\ 

Probe .. ---- 1 tot -_ ... -~., 

" 

d 

.J.t .=H ~ ) , D 

-t 

n . 

Pa 

Pb 

b 

'--i 

e 

D,s 

0t:~ .,.7 -

~'L61 0 ~, 0.,...,., n -

a ~.S 

-

pO,S

a-

~b~ 

b 6.S

C.(L) It 

c $,/1

d #.f. 71

e o.9

CO(22 

.' 

Probe 

OR 

-

Probe 

• 

c I 

r

l f---{ 

.~ :, 

l 

Specifications (EPA Method 2) 

o • 3/16d

• ta 3/8" O~ • 1/21

• 

I ~ 3/4" b~O 

c ~ 3" 

d > 3" 

e i: 3/." 

f l. 2" 

PI • Pb 

t.05 0't !. P .ii.SO Dt 

If these spec:1fh:a.t1ons are met, proceed with Part 2 Pi tot a 1i gnme"t. 
I 

I 

I 

I 

I 

I 

I 

J 

t 

S·TYPE PITOT GEOMETRIC CAlf BRA TION 

P~ • PITOT ALIGNMENT 

(fB6'se10ENTtFICA nON: '10 ( 

PITOT IOENnFICATION: "f()( 

B. 

c. (f < lIS, 

a ~ q!!!o 

b ~ c... J,.~ 

c= -41J~ 

d :I!JJ:1-0 

e=~$ 

e =~8 

e':: 6V.8 -

a=O.~ 

b =O.~c:D - c =(.09/ - d D D -• .,'" If - e = L:!!s-. 

6 = 91.-s-

-

e · = '1/, I 

---

TECHNICIAN: ~~ 

OATE: 11'46 

a 2 +d2 -e 2 

------~COS8' 2ad 

( 80°<8<100°) 

(80"(8'(100") 

a 2+b2 -c2 

2ab DeOSe 

a 2 +d2 -e 2 

2ad =cos8' 

(85°<6<95") 

(85°<6'<95°) 

D. (9 < 1J32? 

!'IToT Coo'O 

NOTE: Values In parentheses are EPA Method 2 specIfications. 
,I .. 

I 

I 

I 

I 

I 

I 

I 

I 

I 

TABLE OF CONTENTS 

QUANTERRA PROJECT NUMBER 091103 

Case Narrative' 

Quanterra's Quality Assurance Program 

Sample Description Information 

Chain of Custody Documentation 

fLhanter-'" 

Enviroament1J/ 

Services 

Hexava1en~ Chromium by Ion Chromatography (with PCR) - Method EPA 306 

Includes Samples: 1 through 4' 

Sample Data Sheets 

Method Blank Report 

Laboratory QC Reports 
. .. . 

~IX SPIKE/MATRIX SPIKE DUPLICATE QC REPORT 

: Chemistry Analysis and Preparation ,'oject: 091103 

lJegory: CRS-IC-AIR Ion Chromatography Inorganics ")t : CRS-IC-30S-AIR 

ttrix : AQUEOUS IIPulen : 091103-0001 PlR : 09 JAN 97-JA 

Dlts : ug/sampl e 

., ---------Concentrat 1 on---------

ocnalyte 

.:omium, 

,exavalent 

, 

I 

I 

. Sample 

Result 

25.9 

MS" Result 

45.3 

MSD 

Result 

45.2 

'Method: EPA 30S 

fI.)".n'.rr. 

EnviiolJlDentll/ 

Services 

Amount 

Spiked 

MS MSD 

Acceptance %Recovery %RPD Limit 

MS MSD Recov. RPD 

19.9 " 19.9 97 97 0.22 85-115 15 

culations are performed before rounding to avoid round-off errors in calculated results. 
,. 

EPA Method 1 Sample and Velocity Travera 

for Statlo~ary Sources' 

Fi rm NatiO'lal O'Ironiun Tota 1 Traverse Poi nts Requ1 red 12 

j location Et - 134 LIne Number of 'Ports 2 

Diameters Upstream _--;:5;.;.;.O~ __ Points Per Port 6 

Diameters Downstream 15.0 Traverse ( Horizontal or Vertical) &fth 

'MINIMUM NUMBER OF TRAVERSE POINTS FOR PARTICULATE 

AND NONPARTICULATE TRAVERSES 

. 

1+--15" -~ 

Duct Diameters Upstream from Flow Disturbance 

~ 0.5 ..... :: .... ·1.0 .. (Dist:~;e A) 2.0 

~ 50 

I 

14 

PARTICULATE 

18 1. ---l--------------. 12 '-NONPARTICULATE .--------~--------~ 8 or • 

STACK D&AMI'R"-"" TO o.n • I'~ZC W 

·1 ... ". 1 

1 

D • lli.= 

eq L+W'--

Sample 

Port 

.'Z25" 

°2~--~--~~--~--~----~--~----~--1~O r---__ ----------------~ Duct Diameters Downstream from Flow Disturbance CROSS-SECTIONAL LAYOUT 

(Distance 8) FORT:~;r~GULAR STACKS 

Traverse Points' LOCATION OF TRAVERSE POINTS IN CIRCULAR STACKS 9 

Matrix 

3x3· 

4x3 

4x4 

5x4 

Point 5x5 {Percent of stack diameter from 

Number inside wall to traverse point} 

On A Number Of Traverse Points On A Diameter 

Diameter 4 6 8 10 12 

1 6.7 4.4 3.2 2.6 2.1 

2 25.0 14.6 10.5 8.2 6.7 

3 75.0 29.6 19.4' 14.6 11.8 

4 93.3 70.4 32.3 22.6 17.7 

5 85.4 61.7 34.2 25.0 

6 95.6 80.6 65.8 35.6 

7 89.5 77.4 64.4 

8 96.8 85.4 75.0 

9 91.8 82.3 

10 97.4 88.2 

11 93.3 

12 91.9 

No. 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

12 

16 

20 

25 

'TRAVERSE POINT LOCATIONS 

Distance NipP'e . Tota' 

From Wa" Size Distance 

0.7 

2.2 

4.4 

10.6 

12.8 

14.3 

-

-

o 

t 

3 

9 

.... 
I 

I LABORATORY CONTROL SAMPLE REPORT . Wet Chemistry Analysis and Preparation Project: 091103 

J, Category: CR6-IC-AIR Ion Chromatography Test: CR6-IC-306-AIR 

I Matrix: AQUEOUS QC Lot: 09 JAN 97-JX 

Concentration Units: ug/sample 

I Analyte 

I Chromium, Hexavalent 

.,.. 

I 

t 

Inorganics 

QC Run: 09 JAN 97-J 

Concentration 

Spiked Measured 

2.50 2.57 

Accuracy(%) 

LCS Limits 

103 85-115 

Calculations are performed before rounding to avoid round-off errors in calculated results. 
·, 

I 

,. .. . 

METHOD BLANK REPORT 

lIet Chemistry Analysis ""roject: 091103 

~est: CR6-IC-306-AIR 

,

ethOd: EPA 306 

atrix: AQUEOUS Clot: 09 JAN 97-JX 

~nalYte 

.Chromium. Hexavalent 

-

I 

I 

NO = Not Detected 

and Preparation 

. Hexavalent Chromium by Ion Chromatography (with PCR) 

QC Run: 09 JAN 97-J 

Result Units 

NO ug/sample 

Reporting Limit 

0.50 
, 

I 

, 

'

QC LOT ASS I GNMENT REPORT - MS QC .. Wet Chemistry Analysis and Preparation 

Laboratory J Sampl e Number 

091103-0001-MS 

091103-0001-SA , 091103-0001-S0 

. 091103-0002-SA 

091103-0003-SA , 091103-0004-SA 

I 

I 

I 

QC Matrix 

AQUEOUS 

AQUEOUS 

AQUEOUS 

AQUEOUS 

AQUEOUS 

AQUEOUS 

QC Category 

CR6-IC-AIR 

CR6-IC-AIR 

CR6-IC-AIR 

CR6-IC~AIR 

CR6-IC-AIR 

CR6-IC-AIR 

QC Lot Number 

(OCS) 

09 JAN 97-JX 

09 JAN 97-JX 

09 JAN 97-JX 

09 JAN 97-JX 

09 JAN 97-JX 

09 JAN 97-JX 

fI.»'aD'.rra 

Services 

~ 

QC Run Number . MS QC Run Number 

(SCS/BLANK/LCS) (SA,MS,SD,DU) 

09 JAN 97-J 09 JAN 97-JA 

09 JAN 97-J 09 JAN 97-JA 

09 JAN 97-J 09 JAN 97-JA 

09 JAN 97-J 09 JAN 97-JA 

09 JAN 97-J 09 JAN 97-JA 

09 JAN 97-J 09 JAN 97-JA 
.1 

I· 

'I 

I 

I 

I. ". 

I 

I 

, ~. - Q)"anter~a £nvininmental 

Services 

Hexavalent Chromium by Ion Chromatography (with PCR) 

Client Name: 

Client 10: 

Lab 10: 

Matrix: 

Authorized: 

Environmental Risk Limited 

M306-0-B2 

091103-0004-SA 

AIRTRAIN 

18 DEC 96 Sampled: 13 DEC 96 Received: 18 DEC 96 Prepared: See Below Analyzed: See Below 

Parameter Result Reporting Analytical Prepared Analyzed Units limit Method Date Date 

Chromium, Hexavalent NO 

NO Q Not detected 

NA D Not applicable 

ug/sample 0.36 EPA 306 NA 

Reported By: Lori Ann Upton Approved By: Josefina Jones 

The cover letter is an integral part of this report. Rev 230787 

09 JAN 97 
-

I Hexavalent Chromium by Ion Chromatography (with PCR) 

fI.,))uanterra 

EnvirolUDeDtU 

Services 

I Client Name: 

Client 10: 

Lab 10: 

Environmental Risk Limited 

M306-0-13 

091103-0003-SA 

Matrix: AIRTRAIN Sampled: 13 DEC 96 Received: 18 DEC 96 I Authori zed: 18 DEC 96 Prepared: See Below Analyzed: See Below 

Reporting Analytical Prepared Analyzed 

-

I 

I 

I 

I 

I 

Parameter Result Units Limit Method Date Date 

Chromium, Hexavalent 24.1 ug/sample 5.2 EPA 306 

Note R : Raised reporting limit(s) due to high analyte level(s). 

NO = Not detected 

NA = Not applicable 

NA 

Reported By: Lori Ann Upton Approved By: Josefina Jones , 

, The cover letter is an integral part of this report. Rev 230787 

09 JAN 97 R 
· , 

Hexavalent Chromium by Ion Chromatography (with PCR) 

fLA.anterr. 

Environment:J1 

Services 

,. Client Name: 

Client 10: 

lab 10: 

Environmental Risk Limited 

M306-0-12 

091103-0002-SA 

Matrix: AIRTRAIN I Authori zed: 18 DEC 96 Sampled: 13 DEC 96 Received: 18 DEC 96 

Prepared: See Below Analyzed: See Below 

I 

, 

I 

I 

Parameter Result Units Reporting Analytical Prepared Analyzed Limit Method Date Date 

Chromium, Hexavalent 26.0 ugfsample 5.3 EPA 306 

Note R : Raised reporting limit(s) due to high analyte level(s). 

NO = Not detected 

NA = Not applicable 

NA 

Reported By: Lori Ann Upton Approved By: Josefina Jones 

The cover letter is an integral part of this report. Rev 230787 

09 JAN 97 R 
t 

I 

I 

'" #. • 

3.3 Summary of Results 

The average Cr~ concentration was 0.0096 milligrams per dry standard cubic meter 

(mgldscm). All test results are well below the USEPA emission llinit of 0.015 mgldscm. Table 

3-2 summarizes the' test results and compares the maximum allowable stack concentration 

(MASC) to the ac~ stack concentration (ASC). 

TABLE 3-2 

. Summary of Emfssioa Results 

. Nadoaal CIaromiam CompaDY, IDe. 

ElectropJaUaa LID. EC-134 

BeuvaJeat CIIromiam Test Program 

Pumam, Coaaectlc:ut 

Uaits 

Method/Component \ 

DATE: 

TIME: 

. Method 2 - Flow dsctin 

actin 

Ml06· Cr'" mgfdscm 

IbIhr 

MASC pg/acm 

ASe pg/acm 

dscfin • dry standard cubic feet per minute 

acfin - actUal cubic feet per minute 

Raa 1 

12113196 

0807-1020 

525~ 

5483 

0.0096 

1.901:-04 

mgldscm - milligrams per dry standard cubic meter 

Iblbr - pounds per hour 

"g/acm - micrograms per actual cubic meter 

Raul 

12113/96 

1102-1308 

5020 

5193 

0.0099 

1.861:-04 

. 

Raa3 Average 

12113196 

1341-1546 

5104 5126 

5268 5315 

0.0092 0.0096 

1.17E-04 1.841:-04 

48 

9.3 

The hazardous air pollutant analysis (Appendix B) pertains to the CTDEP'air regulations. 

As indicated, the average actual stack concentration is 18.5% of the allowable Cr~ concentration 

and clearly demonstrates compliance. .. 

S219c134.rpt 6 January 1997