### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date 10672 Cedar Bay CBB 5/11/2010 5/12/2010 5/13/2010Fuel Type 1 Fuel Type 2 Fuel Type 3 bitum inous bitum inous bitum inousOther Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte 10672 Cedar Bay CBA As Received Higher Heating Value

Cedar Bay CBB As Received % Moisture Cedar Bay CBB As Received % Ash Cedar Bay CBB As Received % Sulfur Cedar Bay CBB Dry basis Higher Heating Value Cedar Bay CBB Dry basis % Moisture Cedar Bay CBB Dry basis % Ash Cedar Bay CBB Dry basis % Sulfur Cedar Bay CBB Dry basis Antim ony Cedar Bay CBB Dry basis Arsenic Cedar Bay CBB Dry basis Bery llium Cedar Bay CBB Dry basis Cadmium Cedar Bay CBB Dry basis Chlorine Cedar Bay CBB Dry basis Chromium Cedar Bay CBB Dry basis Cobalt Cedar Bay CBB Dry basis Fluorine Cedar Bay CBB Dry basis Lead Cedar Bay CBB Dry basis Manganese Cedar Bay CBB Dry basis Mercury Cedar Bay CBB Dry basis Nickel Cedar Bay CBB Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04)

ASTM D2013-04 ASTM D2691-95

ASTM D6357-04 ASTM D6357-04 ASTM D6357-04 ASTM D6357-04 ASTM 4208-02 ASTM D6357-04 ASTM D6357-04 SW 5050\9056 ASTM D6357-04 ASTM D6357-04 ASTM 3684-01 ASTM D6357-04 ASTM D6357-04EIA

Facility Code Facility Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A , M0031 with SW-846 M6 260B) 10672 Cedar Bay CBB M2 6/033,M0011,M18,M25A

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) CS10-131 5/11/2010 11988.00 Btu/lb 5.93 Fuel Testing Results% A

sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A

sh (Dry Basis) % Sulfur (Dry Basis) 13.44 1.39 12745 Btu/lb 14.29 1.48Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Ar senic (Dry Basis) Ar senic Units Bery llium (Dry Basis) Bery llium

Units Cadmium

(Dry Basis) 599 ppmCadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units ND ppmEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A , M0031 with SW-846 M6 260B) 10672 Cedar Bay CBB M0 27/028,M29,M30B

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) CS10-132 5/12/2010 12394.00 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) Btu/lb 5.69 11.57 1.6 13141 Btu/lbChlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Ar senic (Dry

Basis) Ar senic Units Bery llium (Dry Basis) Bery llium

Units Cadmium

(Dry Basis) 12.27 1.7 575 ppm 0.129 mg /Kg 17.049 mg /Kg 1.098Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units mg /Kg 0.183 mg /Kg 18.043 mg /Kg 6.951 mg /Kg 27.642 mg /KgSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 14.431 mg /Kg 0.046 mg /Kg ND ppm 8.496 mg /KgEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A , M0031 with SW-846 M6 260B) 10672 Cedar Bay CBB M0 27/028,M29,M30B

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) CS10-133 5/13/2010 12016.00 Btu/lb 5.75 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 13.12 1.71 12749 Btu/lb 13.92 1.82Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Ar senic (Dry

Basis) Ar senic Units Bery llium (Dry Basis) Bery llium

Units Cadmium

(Dry Basis) 822 ppm 0.21 mg /Kg 24.654 mg /Kg 1.321 mg /Kg 0.213Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units mg /Kg 19.177 mg /Kg 7.866 mg /Kg 20.366 mg /Kg 16.463 mg /KgSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 1.699 mg /Kg ND ppm 9.533 mg /KgEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A , M0031 with SW-846 M6 260B) 10672 Cedar Bay CBB

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Ar senic (Dry

Basis) Ar senic Units Bery llium (Dry Basis) Bery llium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add y our own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add y our own unit of measure to the orange hightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm