Quarterly Groundwater Monitoring Report – Outside 

(Non-Tunnel) Wells 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

April 2010 

Prepared by: 

TEC Inc. 

1003 Bishop St. Suite 1550 

Pauahi Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2010 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 3

1.1 Project Objective .............................................................................................................. 3

1.2 Previous Reports .............................................................................................................. 3

1.3 Background ...................................................................................................................... 4

1.3.1 Site Description ......................................................................................................... 4

1.3.2 Facility Information .................................................................................................. 4

1.3.3 UST Information ....................................................................................................... 5

1.4 Regulatory Updates .......................................................................................................... 6

2.0 Sample Collection and Analyses .......................................................................................... 6

2.1 Monitoring Well Purging ................................................................................................. 6

2.2 Groundwater Sample Collection ...................................................................................... 7

2.3 Groundwater Sample Analyses ........................................................................................ 7

3.1 January 2010 Sample Analytical Results ......................................................................... 7

4.0 Summary and Conclusions ................................................................................................... 9

5.0 References .......................................................................................................................... 11

List of Tables 

Table 1 Monitoring Well Information ........................................................................................5 

Table 2 Analytical Results for Quarterly Groundwater Sampling (January 26, 2010) ...............8 

List of Figures 

Figure 1 Groundwater Monitoring Well Locations ....................................................................10 

List of Appendices 

Appendix A – Laboratory Analytical Reports 

Appendix B – Monitoring Well Construction Logs
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2010 

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Executive Summary 

This quarterly groundwater monitoring report presents the results of groundwater sampling 

conducted on January 26, 2010 at locations surrounding the United States (US) Navy Bulk Fuel 

Storage Facility at Red Hill, Oahu, Hawaii (the Facility). The sampling and reporting was 

conducted by TEC Inc. (TEC) for the Fleet and Industrial Supply Center (FISC) at Pearl Harbor, 

Hawaii. This report is part of a series of quarterly groundwater monitoring reports, supplemental 

to the groundwater reports for the groundwater monitoring wells within the Facility, provided by 

the US Navy to the State of Hawaii Department of Health (HDOH) in accordance with HDOH’s 

release response requirements. Currently, there are 18 active and two inactive, 12.5 million 

gallon, field-constructed underground storage tanks (USTs) located at the Facility. 

Background 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from the 

Facility USTs and provides approximately 24% of the potable water to the Pearl Harbor Water 

System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system and a groundwater monitoring well 

within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 2005, these wells 

have been sampled quarterly for Total Petroleum Hydrocarbons (TPH) quantified as DieselRange Organics (DRO) and Gasoline Range Organics (GRO), Volatile Organic Compounds 

(VOCs), Polynuclear Aromatic Hydrocarbons (PAHs), and dissolved lead. 

In response to increasing concentrations of contaminants of potential concern at the groundwater 

monitoring wells within the facility (specifically RHMW02) during 2008, plans were made to 

conduct quarterly sampling at the following monitoring well locations: 

 RHMW04, north of the Facility’s tank 20; 

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01); and 

 Halawa Deep Well 2253-03 (referred to as HDMW2253-03 in this report). 

During the summer and fall of 2008, HDOH updated their Environmental Action Levels (EALs), 

which resulted in significant changes to the action levels associated with methylnaphthalenes. 

The HDOH Drinking Water toxicity EAL for these compounds was 240 g/L. This 

concentration assumed that methylnaphthalenes were not human carcinogens. Once evidence 

emerged and was accepted by the US Environmental Protection Agency (USEPA) that 

methylnaphthalenes are carcinogenic to humans, HDOH adopted more rigorous EALs of 4.7 

g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene (HDOH, 2008). 
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The HDOH Drinking Water EAL for naphthalene was also updated during this process. 

Previously, HDOH based their naphthalene EAL on US Environmental Protection Agency 

(USEPA) Region 9 Preliminary Remediation Goal (PRG) of 6.2 g/L, which is associated with a 

non-cancer Hazard Index (HI) of 1. The USEPA generally considers a Hazard quotient (HQ) of 

1.0 or less to be acceptable. For multiple chemicals or fractions at an exposure point (e.g. for a 

monitoring well) a HI is calculated by summing the HQs. In deference to the California 

Department of Public Health’s Drinking Water Notification Levels, (HDOH, 2008) HDOH 

updated their naphthalene drinking water EAL to 17 g/L. 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the Groundwater Gross Contamination EAL for TPH-DRO remains 100 g/L. 

Current Results 

On January 26, 2010, three groundwater samples (i.e., RHMW04, OWDFMW01, and 

HDMW2253-03), along with the required quality control samples (duplicate, matrix spike, and 

matrix spike duplicate) were collected for analysis. Samples were analyzed for TPH-DRO, 

TPH-GRO, VOCs, PAHs, and dissolved lead. 

TPH-DRO was detected at 322F μg/L [F indicates that the compound was identified at a 

concentration above the method detection limit (MDL), but below the reporting limit (RL), 

therefore is considered an estimate] in HDMW2253-03, and 1,490 μg/L in OWDFMW01. These 

values are above the HDOH Drinking Water EAL (i.e., 210 μg/L) and the HDOH EAL for Gross 

Contamination (i.e., 100 μg/L). No other HDOH Drinking Water EALs were exceeded and no 

other contaminants of concern were detected above the laboratory MDL. 

Conclusions and Recommendations 

Excluding the January 2010 sampling event, TPH-DRO results from the two most recent 

sampling events at OWDFMW01, conducted in October 2009 and August 2009, were non-detect 

(i.e., TPH-DRO was not detected above the MDL). Likewise, excluding the January 2010 

sampling event, TPH-DRO results from the most recent sampling event at HDMW2253-03, 

conducted in October 2009 were non-detect. HDMW2253-03 was not sampled in August 2009 

due to access issues. Although a trend (i.e., two or more consecutive events of detectable 

concentrations) of TPH-DRO for OWDFMW01 and HDMW2253-03 has not yet been 

established, careful attention should be given to subsequent sampling events regarding the 

presence of TPH-DRO. 

Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead 

should continue at the Facility until such time that data indicates that a different monitoring plan 

is warranted. The next quarterly groundwater sampling event will be performed in April 2010. 
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Red Hill Fuel Storage Facility April 2010 

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1.0 Introduction

This report presents the results of the third groundwater sampling event, conducted in January 

2010 at two groundwater monitoring wells (i.e., RHMW04 and OWDFMW01). The first and 

second sampling events for OWDFMW01 were conducted in August and October 2009 

respectively. In addition, this report presents data from the second sampling event conducted in 

January 2010 at HDMW2253-03. The first sampling event at HDMW2253-03 was conducted in 

October 2009. An August 2009 sampling event for HDMW2253-03 was not conducted due to 

access issues. 

These three wells surround the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred 

to as “the Facility”). The Facility consists of 18 active and two inactive USTs operated by FISC, 

Pearl Harbor. This groundwater sampling and analysis event is supplemental to the quarterly 

groundwater sampling and analysis at groundwater monitoring wells within the Facility (i.e., part 

of the groundwater monitoring program for the UST site in response to past UST releases, 

previous environmental investigations, and recommendations from the HDOH). 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater surrounding the Facility. The project was conducted to ensure 

the Navy remains in compliance with HDOH UST release response requirements. The 

groundwater sampling program followed the procedures described in Red Hill Bulk Fuel Storage 

Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008 updated in 2009], also referred to 

as “the Plan”. 

This groundwater sampling event was conducted by TEC under US Navy Contract Number 

N47408-04-D-8514, Task Order No. 54, Amendment/Modification No. 01. 

1.2 Previous Reports 

This is a quarterly sampling event that is being conducted to supplement the quarterly 

groundwater sampling and analysis at groundwater monitoring wells within the Facility, which 

began in 2005. The following groundwater monitoring reports were previously submitted to the 

HDOH, for groundwater monitoring wells within the Facility: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 
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9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); 

14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 

15. Groundwater Monitoring Results, May 2009 (submitted July 2009); 

16. Groundwater Monitoring Results, July 2009 (submitted September 2009); and 

17. Groundwater Monitoring Results, October 2009 (submitted December 2009). 

The following groundwater monitoring reports were previously submitted to the HDOH for 

groundwater monitoring wells outside the Facility: 

1. Groundwater Sampling Results, August 2009 (submitted September 2009); and 

2. Groundwater Monitoring Results, October 2009 (submitted December 2009). 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Red Hill, Oahu, Hawaii. Land adjacent to the north of the Facility is 

occupied by Halawa Correctional Facility and private businesses. Land to the south and west of 

the Facility includes the Coast Guard Reservation. Moanalua Valley is located east of the 

Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet from the Facility (Dawson, 2006). The US Navy Well 2254-01 is located 

approximately 3,000 feet west of the Facility and provides approximately 24% of the potable 

water to the Pearl Harbor Water System, which serves approximately 52,200 military consumers 

(TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and two inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2010 

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aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system, a background groundwater 

monitoring well (RHMW04) north of the Facility adjacent to the US Navy Firing Range, and a 

groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery 

(RHMW2254-01). Since 2005, RHMW01, RHMW02, RHMW03, and RHMW2254-01 have 

been sampled quarterly for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. 

Due to increasing concentrations of contaminants of potential concern at the groundwater 

monitoring wells within the Facility (specifically RHMW02) during 2008, response measures 

were warranted. In April 2009, another groundwater monitoring well (RHMW05) was installed 

within the lower access tunnel between RHMW01 and RHMW2254-01. It was installed to 

identify the extent of contaminant migration before it reaches the infiltration gallery at 

RHMW2254-01. 

Additionally, plans were made to sample three monitoring wells surrounding the Facility, 

RHMW04, OWDFMW01, and HDMW2253-03. RHMW04 was installed to provide 

geochemistry for water moving through the basal aquifer beneath the Facility. OWDFMW01 

(originally known as MW08) was installed into the basal aquifer in 1998 for a Phase II Remedial 

Investigation/ Feasibility Study for the Red Hill Oily Waste Disposal Facility (Earth Tech Inc., 

2000). It is located geographically down-gradient of the USTs and US Navy Well 2254-01. 

HDMW2253-03 is controlled by the State of Hawaii Commission on Water Resource 

Management. It is located between the Facility and the municipal drinking water supply well run 

by the City and County of Honolulu Board of Water Supply (Halawa Shaft pumping station 

2354-01). 

Table 1 summarizes basic groundwater monitoring well information, Figure 1 shows 

groundwater monitoring well locations, and Appendix B includes the well construction logs for 

RHMW04 and OWDFMW01. 

Table 1. Monitoring Well Information 

Groundwater Well TOC Elevation 

(ft msl) 

DTW (ft) TD (ft) 

RHMW04 313.03 293 320 

OWDFMW01 138.94 120 142.8 

HDMW2253-03 225 210 1,575 

Notes: 

 DTW - Distance to water 

 TD - Total depth of well 

 TOC - Top of casing 

ft – Feet 

ft msl - Feet from mean sea level 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel, JP-8, and F-76 (diesel marine fuel). Previously, several tanks 

stored Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 
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measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

The drinking water EAL for naphthalene has also been updated during this process. Previously, 

HDOH based their naphthalene EAL on United States Environmental Protection Agency 

(USEPA) Region 9 Preliminary Remediation Goal (PRG) of 6.2 g/L, which is associated with a 

non-cancer Hazard Index (HI) of 1. The USEPA generally considers a Hazard Quotient (HQ) of 

1.0 or less to be acceptable. For multiple chemicals or fractions at an exposure point (e.g. for a 

monitoring well) a HI is calculated by summing the HQs. HDOH has updated their naphthalene 

drinking water EAL to 17 g/L, in deference to the California Department of Public Health’s 

Drinking Water Notification Levels, a HI of 2.7 (HDOH, 2008). 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 100 

g/L. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on January 26, 2010. 

Groundwater samples were collected from three monitoring wells, RHMW04, OWDFMW01, 

and HDMW2253-03. Sampling and analysis were conducted according to Red Hill Bulk Fuel 

Storage Facility Groundwater Protection Plan (TEC, 2008). A total of six samples were 

collected as follows: 

 one environmental sample from RHMW04, OWDFMW01, and HDMW2253-03; 

 one duplicate sample from RHMW04 (sampled as RHMWA01 and reported as 

RHMW04D); and 

 one matrix spike and matrix spike duplicate from OWDFMW01. 

2.1 Monitoring Well Purging

RHMW04 and OWDFMW01 were purged prior to sampling. Well purging was considered 

complete when no less than three successive water quality parameter measurements had 

stabilized within approximately 10 percent. Field parameters were measured at regular intervals 

during well purging and included pH, temperature, specific conductivity, dissolved oxygen, and 

turbidity. Due to the well construction characteristics of HDMW2253-03, the well was not 

purged prior to sampling, but field parameters were recorded. Rather than purging, a grab 
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sample was collected at a depth below the solid casing (which extends about 50 feet below the 

water table) and within the open-holed portion of the well. 

2.2 Groundwater Sample Collection 

Immediately following purging, RHMW04 was sampled directly from a dedicated bladder pump 

system, and OWDFMW01 was sampled using a disposable bailer. HDMW2253-03 was sampled 

using a disposable bailer designed to collect samples at desired depths. Samples were placed 

into sampling containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile 

organic analysis, nitric acid (HNO3) for dissolved lead]. Dissolved lead samples were filtered in 

the field and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by 

EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

three monitoring wells, RHMW04, OWDFMW01, and HDMW2253-03. Duplicate sample 

results from monitoring well RHMW04 are reported in this document as RHMW04D. A 

summary of groundwater analytical results for TPH-DRO and TPH-GRO, VOCs, PAHs, and 

dissolved lead is included in Table 2. Complete analytical laboratory reports are provided in 

Appendix A. 

3.1 January 2010 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. The results for each groundwater monitoring well are discussed below. 

RHMW04

No potential chemical of concern was detected above the laboratory MDLs in RHMW04 (Table 

2). 

OWDFMW01

TPH-DRO was detected at 1,490 μg/L, exceeding the HDOH Groundwater Gross Contamination 

EAL and Drinking Water EAL (i.e., 100 μg/L and 210 μg/L, respectively). No other potential 

chemical of concern was detected above the laboratory MDLs in OWDFMW01 (Table 2). 

HDMW2253-03

TPH-DRO was detected at 322F μg/L [F indicates that the compound was identified at a 

concentration above the MDL, but below the reporting limit (RL), therefore is considered an 

estimate], exceeding the HDOH Groundwater Gross Contamination EAL and Drinking Water 
Page 1 of 1

Table . Analytical Results for Quarterly Groundwater Monitoring Release Response Report (January 26, 2010)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL

TPH as DIESEL RANGE ORGANICS 210 100 322 F 172 460 1490 165 440 ND U 167 444 ND U 165 440

TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100 ND U 30 100 ND U 30 100 ND U 30 100

1-METHYLNAPHTHALENE 4.7 10 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

2-METHYLNAPHTHALENE 24 10 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

ACENAPHTHENE 370 20 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

ACENAPHTHYLENE 240 2000 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

ANTHRACENE 1800 22 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

BENZO(a)PYRENE 0.2 0.81 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

CHRYSENE 9.2 1 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

FLUORANTHENE 1500 130 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

FLUORENE 240 950 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

NAPHTHALENE 17 21 ND U 0.0517 0.167 ND U 0.0332 0.107 ND U 0.0337 0.109 ND U 0.0348 0.112

PHENANTHRENE 240 410 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

PYRENE 180 68 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562

1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2

1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10

BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4

BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3

CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1

CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2

METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10

METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10

METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5

NAPHTHALENE 17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2

STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

XYLENES, TOTAL 10000 20 ND U 1 2 ND U 1 2 ND U 1 2 ND U 1 2

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method detection limit

U - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzed

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

1

2

UG/L Method

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Chemical

HDMW2253-03

UG/L

January 26, 2010 January 26, 2010 January 26, 2010

OWDFMW01

UG/L

RHMW04

UG/L

RHMW04DFinal Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites 

with Contaminated Soil and Groundwater , HDOH, 2009

Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with 

Contaminated Soil and Groundwater , HDOH, 2009

8015B (Petroleum)

8270C SIM 

(PAHs)

8260B 

(VOCs)

January 26, 2010
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2010 

 ____________________________________________________________________________________________ 

9 

EAL (i.e., 100 μg/L and 210 μg/L, respectively). No other potential chemical of concern was 

detected above the laboratory MDLs in HDMW2253-03 (Table 2). 

4.0 Summary and Conclusions 

Summary

TPH-DRO was detected above the laboratory MDLs, HDOH Drinking Water EALs, and Gross 

Contamination EALs in OWDFMW01 and HDMW2253-03. No other potential chemical of 

concern was detected above the laboratory MDLs in OWDFMW01, HDMW2253-03, or 

RHMW04. 

Conclusions/Recommendations

Excluding the January 2010 sampling event, TPH-DRO results from the two most recent 

sampling events at OWDFMW01, conducted in October 2009 and August 2009, were non-detect 

(i.e., TPH-DRO was not detected above the MDL). Likewise, excluding the January 2010 

sampling event, TPH-DRO results from the most recent sampling event at HDMW2253-03, 

conducted in October 2009, were non-detect. HDMW2253-03 was not sampled in August 2009 

due to access issues. Although a trend (i.e., two or more consecutive events of detectable 

concentrations) of TPH-DRO for OWDFMW01 and HDMW2253-03 has not yet been 

established, careful attention should be given to subsequent sampling events regarding the 

presence of TPH-DRO. Consideration should be given to installing additional groundwater 

monitoring wells at strategic locations to better assess whether or not increases of TPH-DRO at 

OWDFMW01 and HDMW2253-03 may be attributed to the Facility. 

Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead 

should continue at the Facility until such time that data indicates that a different monitoring plan 

is warranted. The next quarterly groundwater sampling event will be performed in April 2010. 

Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility April 2010 

 ____________________________________________________________________________________________ 

11 

5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily 

Waste Disposal Facility, Halawa, Oahu, Hawaii. September 2000. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008 revised in December 2009. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-010 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1100319

1 of 80
CASE NARRATIVE Print Date: 2/5/2010

Workorder No.: 1100319

Project Name: 3354-010 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

1100319001

DRO by 8015C - Unknown hydrocarbon with several peaks is present.

PS OWDFMW01-WG-03

1100319002

AK101 - MS recovery does not meet QC criteria.See the LCS/LCSD for precision and accuracy.

8260B - MS recovery for 1,1-dichloroethane, cis-1,3-dichloropropene and methyl-t-butyl ether does not meet QC criteria 

(biased high). See LCS for accuracy.

8270D SIM - MS recovery is outside of QC criteria for fluoranthene (biased high). Refer to LCS for accuracy.

BMS OWDFMW01-WG-03 MS

1100319003

AK101 - MSD recovery does not meet QC criteria.See the LCS/LCSD for precision and accuracy.

8260B - MSD recovery for 1,1-dichloroethane and methyl-t-butyl ether does not meet QC criteria (biased high). See LCS for 

accuracy.

8270D SIM - MSD recovery is outside of QC criteria for fluoranthene (biased high). Refer to LCS for accuracy.

BMSD OWDFMW01-WG-03 MSD

947497

8270D SIM - Phenanthrene detected in the MB greater than one-half the LOQ. The concentration of phenanthrene in the 

associated samples is less than the LOQ or greater than ten times the MB contamination.

MB MB for HBN 225159 [XXX/22245]

SG S N o rth A m eric a Inc . En vir onm enta l D ivision 200 W e st Potter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs.com M em ber of SG S Group

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Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1100319

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1003 Bishop Street,

Pauahi Tower Suite 1550

Honolulu, HI 96813

Attn: Rick Adkisson

T: (808)528-1445 F:(808)528-0768

Jennifer Serna

Project Manager

3354-010 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

3 of 80
Enclosed are the analytical results associated with the above work order. If you have any questions regarding this report, or if we can be of any 

other assistance, please contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions 

(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties. 

SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this 

program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for 

ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 

8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all 

statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental 

Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits.

! Surrogate out of control limits.

B Indicates the analyte is found in a blank associated with the sample.

CCV Continuing Calibration Verification

CL Control Limit

D The analyte concentration is the result of a dilution.

DF Dilution Factor

DL Detection Limit (i.e., maximum method detection limit)

E The analyte result is above the calibrated range.

F Indicates value that is greater than or equal to the DL

GT Greater Than

ICV Initial Calibration Verification

J The quantitation is an estimation.

JL The analyte was positively identified, but the quantitation is a low estimation.

LCS(D) Laboratory Control Spike (Duplicate)

LOD Limit of Detection (i.e., 2xDL)

LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)

LT Less Than

M A matrix effect was present.

MB Method Blank

MS(D) Matrix Spike (Duplicate)

ND Indicates the analyte is not detected.

Q QC parameter out of acceptance range.

R Rejected

RPD Relative Percent Difference

U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP.

Print Date: 2/5/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-010 Red Hill BFSF

Workorder No.: 1100319

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015C (W) SW8015C

GRO (W) SW8015C

Print Date: 2/5/2010 9:27 am

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1100319001 OWDFMW01-WG-03

1100319002 OWDFMW01-WG-03 MS

1100319003 OWDFMW01-WG-03 MSD

1100319004 RHMW04-WG-03

1100319005 RHMWA01-WG-03

1100319006 HDMW2253-03-WG-03

1100319007 TB01-WG-03

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6300 MXX22714

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6300

Analytical Method: SW6020

Analysis Date/Time: 02/02/10 17:03

Prep Batch: MXX22714

Prep Method: SW3010A

Prep Date/Time: 02/01/10 14:00 Container ID:1100319001-L

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9852 VXX20441

4-Bromofluorobenzene <surr> 100 50-150 % 1 VFC9852 VXX20441

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9852

Analytical Method: SW8015C

Analysis Date/Time: 02/01/10 11:31

Prep Batch: VXX20441

Prep Method: SW5030B

Prep Date/Time: 02/01/10 10:00 Container ID:1100319001-A

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 1.49 0.440 0.165 mg/L 1 XFC9100 XXX22248

5a Androstane <surr> 89.9 50-150 % 1 XFC9100 XXX22248

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9100

Analytical Method: SW8015C

Analysis Date/Time: 02/02/10 17:29

Prep Batch: XXX22248

Prep Method: SW3520C

Prep Date/Time: 02/01/10 10:20 Container ID:1100319001-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11092 VXX20444

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11092 VXX20444

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11092 VXX20444

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11092 VXX20444

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Xylenes (total) 2.00 U 2.00 1.00 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane-D4 <surr> 104 73-120 % 1 VMS11092 VXX20444

Toluene-d8 <surr> 101 80-120 % 1 VMS11092 VXX20444

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

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The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11092

Analytical Method: SW8260B

Analysis Date/Time: 02/01/10 18:48

Prep Batch: VXX20444

Prep Method: SW5030B

Prep Date/Time: 02/01/10 12:35 Container ID:1100319001-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

11 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: OWDFMW01-WG-03

SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Acenaphthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Fluorene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Phenanthrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Anthracene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Fluoranthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Pyrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Benzo(a)Anthracene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Chrysene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Benzo[b]Fluoranthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Benzo[k]fluoranthene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Benzo[a]pyrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Indeno[1,2,3-c,d] pyrene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Dibenzo[a,h]anthracene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Benzo[g,h,i]perylene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Naphthalene 0.0664 U 0.107 0.0332 ug/L 1 XMS5285 XXX22249

1-Methylnaphthalene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

2-Methylnaphthalene 0.0320 U 0.0535 0.0160 ug/L 1 XMS5285 XXX22249

Terphenyl-d14 <surr> 102 50-126 % 1 XMS5285 XXX22249

Batch Information

Initial Prep Wt./Vol.: 935 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5285

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/02/10 11:47

Prep Batch: XXX22249

Prep Method: SW3520C

Prep Date/Time: 02/01/10 11:20 Container ID:1100319001-J

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

12 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6300 MXX22713

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6300

Analytical Method: SW6020

Analysis Date/Time: 02/02/10 16:34

Prep Batch: MXX22713

Prep Method: SW3010A

Prep Date/Time: 02/01/10 14:00 Container ID:1100319004-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

13 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9852 VXX20441

4-Bromofluorobenzene <surr> 104 50-150 % 1 VFC9852 VXX20441

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9852

Analytical Method: SW8015C

Analysis Date/Time: 02/01/10 12:43

Prep Batch: VXX20441

Prep Method: SW5030B

Prep Date/Time: 02/01/10 10:00 Container ID:1100319004-A

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

14 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.334 U 0.444 0.167 mg/L 1 XFC9100 XXX22248

5a Androstane <surr> 86.3 50-150 % 1 XFC9100 XXX22248

Batch Information

Initial Prep Wt./Vol.: 900 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9100

Analytical Method: SW8015C

Analysis Date/Time: 02/02/10 18:32

Prep Batch: XXX22248

Prep Method: SW3520C

Prep Date/Time: 02/01/10 10:20 Container ID:1100319004-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

15 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11092 VXX20444

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11092 VXX20444

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11092 VXX20444

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

16 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11092 VXX20444

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Xylenes (total) 2.00 U 2.00 1.00 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane-D4 <surr> 100 73-120 % 1 VMS11092 VXX20444

Toluene-d8 <surr> 99.6 80-120 % 1 VMS11092 VXX20444

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

17 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11092

Analytical Method: SW8260B

Analysis Date/Time: 02/01/10 19:19

Prep Batch: VXX20444

Prep Method: SW5030B

Prep Date/Time: 02/01/10 12:35 Container ID:1100319004-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

18 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMW04-WG-03

SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Acenaphthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Fluorene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Phenanthrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Anthracene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Fluoranthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Pyrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Benzo(a)Anthracene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Chrysene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Benzo[b]Fluoranthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Benzo[k]fluoranthene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Benzo[a]pyrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Indeno[1,2,3-c,d] pyrene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Dibenzo[a,h]anthracene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Benzo[g,h,i]perylene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Naphthalene 0.0674 U 0.109 0.0337 ug/L 1 XMS5285 XXX22249

1-Methylnaphthalene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

2-Methylnaphthalene 0.0326 U 0.0543 0.0163 ug/L 1 XMS5285 XXX22249

Terphenyl-d14 <surr> 111 50-126 % 1 XMS5285 XXX22249

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5285

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/02/10 13:24

Prep Batch: XXX22249

Prep Method: SW3520C

Prep Date/Time: 02/01/10 11:20 Container ID:1100319004-J

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

19 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6300 MXX22713

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6300

Analytical Method: SW6020

Analysis Date/Time: 02/02/10 16:36

Prep Batch: MXX22713

Prep Method: SW3010A

Prep Date/Time: 02/01/10 14:00 Container ID:1100319005-G

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

20 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9852 VXX20441

4-Bromofluorobenzene <surr> 99.1 50-150 % 1 VFC9852 VXX20441

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9852

Analytical Method: SW8015C

Analysis Date/Time: 02/01/10 13:02

Prep Batch: VXX20441

Prep Method: SW5030B

Prep Date/Time: 02/01/10 10:00 Container ID:1100319005-A

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

21 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.330 U 0.440 0.165 mg/L 1 XFC9100 XXX22248

5a Androstane <surr> 95.2 50-150 % 1 XFC9100 XXX22248

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9100

Analytical Method: SW8015C

Analysis Date/Time: 02/02/10 18:53

Prep Batch: XXX22248

Prep Method: SW3520C

Prep Date/Time: 02/01/10 10:20 Container ID:1100319005-J

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

22 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11092 VXX20444

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11092 VXX20444

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11092 VXX20444

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

23 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11092 VXX20444

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Xylenes (total) 2.00 U 2.00 1.00 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane-D4 <surr> 101 73-120 % 1 VMS11092 VXX20444

Toluene-d8 <surr> 99.4 80-120 % 1 VMS11092 VXX20444

4-Bromofluorobenzene <surr> 106 76-120 % 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

24 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11092

Analytical Method: SW8260B

Analysis Date/Time: 02/01/10 19:51

Prep Batch: VXX20444

Prep Method: SW5030B

Prep Date/Time: 02/01/10 12:35 Container ID:1100319005-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

25 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: RHMWA01-WG-03

SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Acenaphthene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Fluorene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Phenanthrene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Anthracene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Fluoranthene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Pyrene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Benzo(a)Anthracene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Chrysene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Benzo[b]Fluoranthene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Benzo[k]fluoranthene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Benzo[a]pyrene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Indeno[1,2,3-c,d] pyrene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Dibenzo[a,h]anthracene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Benzo[g,h,i]perylene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Naphthalene 0.0696 U 0.112 0.0348 ug/L 1 XMS5282 XXX22245

1-Methylnaphthalene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

2-Methylnaphthalene 0.0338 U 0.0562 0.0169 ug/L 1 XMS5282 XXX22245

Terphenyl-d14 <surr> 103 50-126 % 1 XMS5282 XXX22245

Batch Information

Initial Prep Wt./Vol.: 890 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5282

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/01/10 13:53

Prep Batch: XXX22245

Prep Method: SW3520C

Prep Date/Time: 01/29/10 11:00 Container ID:1100319005-K

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

26 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6300 MXX22714

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6300

Analytical Method: SW6020

Analysis Date/Time: 02/02/10 17:13

Prep Batch: MXX22714

Prep Method: SW3010A

Prep Date/Time: 02/01/10 14:00 Container ID:1100319006-L

Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

27 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9852 VXX20441

4-Bromofluorobenzene <surr> 100 50-150 % 1 VFC9852 VXX20441

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9852

Analytical Method: SW8015C

Analysis Date/Time: 02/01/10 13:22

Prep Batch: VXX20441

Prep Method: SW5030B

Prep Date/Time: 02/01/10 10:00 Container ID:1100319006-A

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

28 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.322 J 0.460 0.172 mg/L 1 XFC9100 XXX22248

5a Androstane <surr> 80.6 50-150 % 1 XFC9100 XXX22248

Batch Information

Initial Prep Wt./Vol.: 870 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9100

Analytical Method: SW8015C

Analysis Date/Time: 02/02/10 19:14

Prep Batch: XXX22248

Prep Method: SW3520C

Prep Date/Time: 02/01/10 10:20 Container ID:1100319006-I

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

29 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11092 VXX20444

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11092 VXX20444

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11092 VXX20444

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

30 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11092 VXX20444

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Xylenes (total) 2.00 U 2.00 1.00 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS11092 VXX20444

Toluene-d8 <surr> 99.7 80-120 % 1 VMS11092 VXX20444

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

31 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11092

Analytical Method: SW8260B

Analysis Date/Time: 02/01/10 20:22

Prep Batch: VXX20444

Prep Method: SW5030B

Prep Date/Time: 02/01/10 12:35 Container ID:1100319006-D

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

32 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: HDMW2253-03-WG-03

SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Acenaphthene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Fluorene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Phenanthrene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Anthracene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Fluoranthene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Pyrene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Benzo(a)Anthracene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Chrysene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Benzo[b]Fluoranthene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Benzo[k]fluoranthene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Benzo[a]pyrene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Indeno[1,2,3-c,d] pyrene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Dibenzo[a,h]anthracene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Benzo[g,h,i]perylene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Naphthalene 0.103 U 0.167 0.0517 ug/L 1 XMS5282 XXX22245

1-Methylnaphthalene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

2-Methylnaphthalene 0.0500 U 0.0833 0.0250 ug/L 1 XMS5282 XXX22245

Terphenyl-d14 <surr> 107 50-126 % 1 XMS5282 XXX22245

Batch Information

Initial Prep Wt./Vol.: 600 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5282

Analytical Method: 8270D SIMS

Analysis Date/Time: 02/01/10 14:26

Prep Batch: XXX22245

Prep Method: SW3520C

Prep Date/Time: 01/29/10 11:00 Container ID:1100319006-K

Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

33 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: TB01-WG-03

SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC9852 VXX20441

4-Bromofluorobenzene <surr> 104 50-150 % 1 VFC9852 VXX20441

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9852

Analytical Method: SW8015C

Analysis Date/Time: 02/01/10 13:41

Prep Batch: VXX20441

Prep Method: SW5030B

Prep Date/Time: 02/01/10 10:00 Container ID:1100319007-A

Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

34 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: TB01-WG-03

SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11092 VXX20444

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11092 VXX20444

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11092 VXX20444

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11092 VXX20444

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

35 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: TB01-WG-03

SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11092 VXX20444

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11092 VXX20444

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11092 VXX20444

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11092 VXX20444

Xylenes (total) 2.00 U 2.00 1.00 ug/L 1 VMS11092 VXX20444

1,2-Dichloroethane-D4 <surr> 99.9 73-120 % 1 VMS11092 VXX20444

Toluene-d8 <surr> 102 80-120 % 1 VMS11092 VXX20444

4-Bromofluorobenzene <surr> 105 76-120 % 1 VMS11092 VXX20444

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

36 of 80
The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: TB01-WG-03

SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 01/28/10 14:45

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11092

Analytical Method: SW8260B

Analysis Date/Time: 02/01/10 17:45

Prep Batch: VXX20444

Prep Method: SW5030B

Prep Date/Time: 02/01/10 12:35 Container ID:1100319007-C

Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

37 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947497 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22245

SW3520C

01/29/2010

QC results affect the following production samples:

1100319005, 1100319006

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Phenanthrene 0.0251 J 0.0500 0.0150 ug/L 02/01/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Fluoranthene 0.0154 J 0.0500 0.0150 ug/L 02/01/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 02/01/10

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 02/01/10

Surrogates 

Terphenyl-d14 <surr> 106 50-126 % 02/01/10

Instrument

Method

Batch XMS5282

8270D SIMS

HP 6890/5973 MS SVQA

38 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947654 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22248

SW3520C

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004, 1100319005, 1100319006

Parameter Results LOQ/CL Units

Analysis

DL Date

Semivolatile Organic Fuels Department

Diesel Range Organics 0.300 U 0.400 0.150 mg/L 02/02/10

Surrogates 

5a Androstane <surr> 93.2 60-120 % 02/02/10

Instrument

Method

Batch XFC9100

SW8015C

HP 7890A FID SV E F

39 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947711 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22249

SW3520C

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 02/02/10

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 02/02/10

Surrogates 

Terphenyl-d14 <surr> 109 50-126 % 02/02/10

Instrument

Method

Batch XMS5285

8270D SIMS

HP 6890/5973 MS SVQA

40 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947724 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20441

SW5030B

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Fuels Department

Gasoline Range Organics 60.0 U 100 30.0 ug/L 02/01/10

Surrogates 

4-Bromofluorobenzene <surr> 104 50-150 % 02/01/10

Instrument

Method

Batch VFC9852

SW8015C

HP 5890 Series II PID+HECD VBA

41 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947759 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

42 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947759 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene 0.240 U 0.400 0.120 ug/L 02/01/10

Toluene 0.620 U 1.00 0.310 ug/L 02/01/10

Ethylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 02/01/10

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 02/01/10

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 02/01/10

Chlorobenzene 0.300 U 0.500 0.150 ug/L 02/01/10

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 02/01/10

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 02/01/10

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 02/01/10

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 02/01/10

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

Styrene 0.620 U 1.00 0.310 ug/L 02/01/10

Dibromomethane 0.620 U 1.00 0.310 ug/L 02/01/10

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 02/01/10

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 02/01/10

Acetone 6.20 U 10.0 3.10 ug/L 02/01/10

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 02/01/10

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 02/01/10

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 02/01/10

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 02/01/10

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 02/01/10

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 02/01/10

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 02/01/10

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 02/01/10

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 02/01/10

Chloroform 0.600 U 1.00 0.300 ug/L 02/01/10

Bromobenzene 0.620 U 1.00 0.310 ug/L 02/01/10

Chloromethane 0.620 U 1.00 0.310 ug/L 02/01/10

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 02/01/10

Bromomethane 1.88 U 3.00 0.940 ug/L 02/01/10

Bromochloromethane 0.620 U 1.00 0.310 ug/L 02/01/10

Vinyl chloride 0.620 U 1.00 0.310 ug/L 02/01/10

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 02/01/10

Chloroethane 0.620 U 1.00 0.310 ug/L 02/01/10

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 02/01/10

43 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947759 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 02/01/10

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 02/01/10

Methylene chloride 2.00 U 5.00 1.00 ug/L 02/01/10

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 02/01/10

P & M -Xylene 1.24 U 2.00 0.620 ug/L 02/01/10

Naphthalene 1.24 U 2.00 0.620 ug/L 02/01/10

o-Xylene 0.620 U 1.00 0.310 ug/L 02/01/10

Bromoform 0.620 U 1.00 0.310 ug/L 02/01/10

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 02/01/10

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 02/01/10

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 02/01/10

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 02/01/10

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 02/01/10

Trichloroethene 0.620 U 1.00 0.310 ug/L 02/01/10

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 02/01/10

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 02/01/10

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 02/01/10

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 02/01/10

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 02/01/10

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 02/01/10

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 02/01/10

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 02/01/10

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 02/01/10

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 02/01/10

Xylenes (total) 2.00 U 2.00 1.00 ug/L 02/01/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 100 73-120 % 02/01/10

Toluene-d8 <surr> 99.1 80-120 % 02/01/10

4-Bromofluorobenzene <surr> 103 76-120 % 02/01/10

Instrument

Method

Batch VMS11092

SW8260B

HP 5890 Series II MS1 VJA

44 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947859 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22713

SW3010A

02/01/2010

QC results affect the following production samples:

1100319004, 1100319005

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 02/02/10

Instrument

Method

Batch MMS6300

SW6020

Perkin Elmer Sciex ICP-MS P3

45 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947864 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22714

SW3010A

02/01/2010

QC results affect the following production samples:

1100319001, 1100319006

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 02/02/10

Instrument

Method

Batch MMS6300

SW6020

Perkin Elmer Sciex ICP-MS P3

46 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947498 Lab Control Sample

947499 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22245

SW3520C

01/29/2010

QC results affect the following production samples:

1100319005, 1100319006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.421 84 ( 50-101 ) 0.5 ug/L 02/01/2010

LCSD 0.394 79 7 (< 30 ) 0.5 ug/L 02/01/2010

Acenaphthene LCS 0.414 83 ( 45-93 ) 0.5 ug/L 02/01/2010

LCSD 0.393 79 5 (< 30 ) 0.5 ug/L 02/01/2010

Fluorene LCS 0.418 84 ( 50-98 ) 0.5 ug/L 02/01/2010

LCSD 0.415 83 1 (< 30 ) 0.5 ug/L 02/01/2010

Phenanthrene LCS 0.426 85 ( 50-104 ) 0.5 ug/L 02/01/2010

LCSD 0.409 82 4 (< 30 ) 0.5 ug/L 02/01/2010

Anthracene LCS 0.421 84 ( 55-105 ) 0.5 ug/L 02/01/2010

LCSD 0.405 81 4 (< 30 ) 0.5 ug/L 02/01/2010

Fluoranthene LCS 0.479 96 ( 58-109 ) 0.5 ug/L 02/01/2010

LCSD 0.472 95 2 (< 30 ) 0.5 ug/L 02/01/2010

Pyrene LCS 0.461 92 ( 56-105 ) 0.5 ug/L 02/01/2010

LCSD 0.458 92 1 (< 30 ) 0.5 ug/L 02/01/2010

Benzo(a)Anthracene LCS 0.520 104 ( 55-120 ) 0.5 ug/L 02/01/2010

LCSD 0.513 103 1 (< 30 ) 0.5 ug/L 02/01/2010

Chrysene LCS 0.469 94 ( 56-109 ) 0.5 ug/L 02/01/2010

LCSD 0.457 91 3 (< 30 ) 0.5 ug/L 02/01/2010

Benzo[b]Fluoranthene LCS 0.535 107 ( 45-120 ) 0.5 ug/L 02/01/2010

LCSD 0.519 104 3 (< 30 ) 0.5 ug/L 02/01/2010

Benzo[k]fluoranthene LCS 0.515 103 ( 56-112 ) 0.5 ug/L 02/01/2010

LCSD 0.508 102 1 (< 30 ) 0.5 ug/L 02/01/2010

Benzo[a]pyrene LCS 0.545 109 ( 57-110 ) 0.5 ug/L 02/01/2010

LCSD 0.551 110 1 (< 30 ) 0.5 ug/L 02/01/2010

Indeno[1,2,3-c,d] pyrene LCS 0.496 99 ( 55-111 ) 0.5 ug/L 02/01/2010

LCSD 0.485 97 2 (< 30 ) 0.5 ug/L 02/01/2010

47 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947498 Lab Control Sample

947499 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22245

SW3520C

01/29/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Dibenzo[a,h]anthracene LCS 0.483 97 ( 54-113 ) 0.5 ug/L 02/01/2010

LCSD 0.488 98 1 (< 30 ) 0.5 ug/L 02/01/2010

Benzo[g,h,i]perylene LCS 0.482 96 ( 49-116 ) 0.5 ug/L 02/01/2010

LCSD 0.494 99 2 (< 30 ) 0.5 ug/L 02/01/2010

Naphthalene LCS 0.382 77 ( 44-89 ) 0.5 ug/L 02/01/2010

LCSD 0.379 76 1 (< 30 ) 0.5 ug/L 02/01/2010

1-Methylnaphthalene LCS 0.394 79 ( 42-92 ) 0.5 ug/L 02/01/2010

LCSD 0.401 80 2 (< 30 ) 0.5 ug/L 02/01/2010

2-Methylnaphthalene LCS 0.365 73 ( 45-89 ) 0.5 ug/L 02/01/2010

LCSD 0.364 73 0 (< 30 ) 0.5 ug/L 02/01/2010

Surrogates 

Terphenyl-d14 <surr> LCS 98 ( 50-126 ) 02/01/2010

LCSD 106 8 02/01/2010

Batch

Method

Instrument

XMS5282

8270D SIMS

HP 6890/5973 MS SVQA

48 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947712 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22249

SW3520C

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

49 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947712 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22249

SW3520C

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.403 81 ( 50-101 ) 0.5 ug/L 02/02/2010

Acenaphthene LCS 0.406 81 ( 45-93 ) 0.5 ug/L 02/02/2010

Fluorene LCS 0.421 84 ( 50-98 ) 0.5 ug/L 02/02/2010

Phenanthrene LCS 0.434 87 ( 50-104 ) 0.5 ug/L 02/02/2010

Anthracene LCS 0.437 87 ( 55-105 ) 0.5 ug/L 02/02/2010

Fluoranthene LCS 0.512 102 ( 58-109 ) 0.5 ug/L 02/02/2010

Pyrene LCS 0.491 98 ( 56-105 ) 0.5 ug/L 02/02/2010

Benzo(a)Anthracene LCS 0.523 105 ( 55-120 ) 0.5 ug/L 02/02/2010

Chrysene LCS 0.464 93 ( 56-109 ) 0.5 ug/L 02/02/2010

Benzo[b]Fluoranthene LCS 0.481 96 ( 45-120 ) 0.5 ug/L 02/02/2010

Benzo[k]fluoranthene LCS 0.493 99 ( 56-112 ) 0.5 ug/L 02/02/2010

Benzo[a]pyrene LCS 0.507 101 ( 57-110 ) 0.5 ug/L 02/02/2010

Indeno[1,2,3-c,d] pyrene LCS 0.456 91 ( 55-111 ) 0.5 ug/L 02/02/2010

Dibenzo[a,h]anthracene LCS 0.461 92 ( 54-113 ) 0.5 ug/L 02/02/2010

Benzo[g,h,i]perylene LCS 0.439 88 ( 49-116 ) 0.5 ug/L 02/02/2010

Naphthalene LCS 0.354 71 ( 44-89 ) 0.5 ug/L 02/02/2010

1-Methylnaphthalene LCS 0.385 77 ( 42-92 ) 0.5 ug/L 02/02/2010

2-Methylnaphthalene LCS 0.363 73 ( 45-89 ) 0.5 ug/L 02/02/2010

Surrogates 

Terphenyl-d14 <surr> LCS 103 ( 50-126 ) 02/02/2010

50 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947712 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22249

SW3520C

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5285

8270D SIMS

HP 6890/5973 MS SVQA

51 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947725 Lab Control Sample

947726 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20441

SW5030B

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 210 105 ( 79-108 ) 200 ug/L 02/01/2010

LCSD 199 100 5 (< 20 ) 200 ug/L 02/01/2010

Surrogates 

4-Bromofluorobenzene <surr> LCS 103 ( 50-150 ) 02/01/2010

LCSD 103 0 02/01/2010

Batch

Method

Instrument

VFC9852

SW8015C

HP 5890 Series II PID+HECD VBA

52 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

53 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 29.9 100 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 28.5 95 5 (< 20 ) 30 ug/L 02/01/2010

Toluene LCS 31.3 104 ( 77-120 ) 30 ug/L 02/01/2010

LCSD 29.7 99 5 (< 20 ) 30 ug/L 02/01/2010

Ethylbenzene LCS 31.4 105 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 29.5 98 6 (< 20 ) 30 ug/L 02/01/2010

n-Butylbenzene LCS 34.9 116 ( 80-124 ) 30 ug/L 02/01/2010

LCSD 33.1 110 5 (< 20 ) 30 ug/L 02/01/2010

1,4-Dichlorobenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 30.3 101 6 (< 20 ) 30 ug/L 02/01/2010

1,2-Dichloroethane LCS 30.9 103 ( 80-129 ) 30 ug/L 02/01/2010

LCSD 30.6 102 1 (< 20 ) 30 ug/L 02/01/2010

1,3,5-Trimethylbenzene LCS 33.8 113 ( 80-128 ) 30 ug/L 02/01/2010

LCSD 31.9 106 6 (< 20 ) 30 ug/L 02/01/2010

4-Chlorotoluene LCS 34.1 114 ( 79-128 ) 30 ug/L 02/01/2010

LCSD 32.3 108 5 (< 20 ) 30 ug/L 02/01/2010

Chlorobenzene LCS 31.1 104 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 29.5 98 5 (< 20 ) 30 ug/L 02/01/2010

4-Methyl-2-pentanone (MIBK) LCS 90.5 101 ( 69-134 ) 90 ug/L 02/01/2010

LCSD 97.4 108 7 (< 20 ) 90 ug/L 02/01/2010

cis-1,2-Dichloroethene LCS 29.8 99 ( 80-125 ) 30 ug/L 02/01/2010

LCSD 28.1 94 6 (< 20 ) 30 ug/L 02/01/2010

4-Isopropyltoluene LCS 34.2 114 ( 80-125 ) 30 ug/L 02/01/2010

LCSD 32.0 107 7 (< 20 ) 30 ug/L 02/01/2010

cis-1,3-Dichloropropene LCS 33.9 113 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 32.9 110 3 (< 20 ) 30 ug/L 02/01/2010

n-Propylbenzene LCS 34.0 113 ( 80-129 ) 30 ug/L 02/01/2010

LCSD 32.0 107 6 (< 20 ) 30 ug/L 02/01/2010

54 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 31.8 106 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 30.1 100 5 (< 20 ) 30 ug/L 02/01/2010

Dibromomethane LCS 30.4 101 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 30.8 103 1 (< 20 ) 30 ug/L 02/01/2010

trans-1,3-Dichloropropene LCS 32.5 108 ( 80-124 ) 30 ug/L 02/01/2010

LCSD 32.4 108 1 (< 20 ) 30 ug/L 02/01/2010

1,2,4-Trichlorobenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 31.4 105 0 (< 20 ) 30 ug/L 02/01/2010

Acetone LCS 72.4 80 ( 50-135 ) 90 ug/L 02/01/2010

LCSD 88.5 98 20 (< 20 ) 90 ug/L 02/01/2010

1,1,2,2-Tetrachloroethane LCS 32.7 109 ( 76-123 ) 30 ug/L 02/01/2010

LCSD 33.7 112 3 (< 20 ) 30 ug/L 02/01/2010

1,2-Dibromo-3-chloropropane LCS 33.1 110 ( 73-130 ) 30 ug/L 02/01/2010

LCSD 36.5 122 10 (< 20 ) 30 ug/L 02/01/2010

Methyl-t-butyl ether LCS 52.3 116 ( 80-120 ) 45 ug/L 02/01/2010

LCSD 53.2 118 2 (< 20 ) 45 ug/L 02/01/2010

Tetrachloroethene LCS 31.2 104 ( 79-122 ) 30 ug/L 02/01/2010

LCSD 28.9 96 8 (< 20 ) 30 ug/L 02/01/2010

Dibromochloromethane LCS 28.7 96 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 28.4 95 1 (< 20 ) 30 ug/L 02/01/2010

1,3-Dichloropropane LCS 32.7 109 ( 80-121 ) 30 ug/L 02/01/2010

LCSD 32.3 108 1 (< 20 ) 30 ug/L 02/01/2010

1,2-Dibromoethane LCS 31.7 106 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 31.8 106 0 (< 20 ) 30 ug/L 02/01/2010

Carbon tetrachloride LCS 31.7 106 ( 80-126 ) 30 ug/L 02/01/2010

LCSD 29.4 98 8 (< 20 ) 30 ug/L 02/01/2010

1,1,1,2-Tetrachloroethane LCS 33.5 112 ( 80-120 ) 30 ug/L 02/01/2010

55 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 31.6 105 6 (< 20 ) 30 ug/L 02/01/2010

Chloroform LCS 30.1 100 ( 80-124 ) 30 ug/L 02/01/2010

LCSD 28.4 95 6 (< 20 ) 30 ug/L 02/01/2010

Bromobenzene LCS 31.1 104 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 30.1 100 3 (< 20 ) 30 ug/L 02/01/2010

Chloromethane LCS 32.1 107 ( 67-125 ) 30 ug/L 02/01/2010

LCSD 32.3 108 1 (< 20 ) 30 ug/L 02/01/2010

1,2,3-Trichloropropane LCS 31.4 105 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 32.0 107 2 (< 20 ) 30 ug/L 02/01/2010

Bromomethane LCS 27.6 92 ( 30-140 ) 30 ug/L 02/01/2010

LCSD 29.6 99 7 (< 20 ) 30 ug/L 02/01/2010

Bromochloromethane LCS 28.0 94 ( 77-129 ) 30 ug/L 02/01/2010

LCSD 27.1 90 3 (< 20 ) 30 ug/L 02/01/2010

Vinyl chloride LCS 28.3 94 ( 72-145 ) 30 ug/L 02/01/2010

LCSD 28.0 93 1 (< 20 ) 30 ug/L 02/01/2010

Dichlorodifluoromethane LCS 32.7 109 ( 62-153 ) 30 ug/L 02/01/2010

LCSD 32.0 107 2 (< 20 ) 30 ug/L 02/01/2010

Chloroethane LCS 29.2 97 ( 67-133 ) 30 ug/L 02/01/2010

LCSD 27.8 93 5 (< 20 ) 30 ug/L 02/01/2010

sec-Butylbenzene LCS 33.8 113 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 32.0 107 6 (< 20 ) 30 ug/L 02/01/2010

Bromodichloromethane LCS 32.8 109 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 31.9 106 3 (< 20 ) 30 ug/L 02/01/2010

1,1-Dichloroethene LCS 27.2 91 ( 76-130 ) 30 ug/L 02/01/2010

LCSD 25.8 86 5 (< 20 ) 30 ug/L 02/01/2010

2-Butanone (MEK) LCS 88.7 99 ( 66-136 ) 90 ug/L 02/01/2010

LCSD 99.9 111 12 (< 20 ) 90 ug/L 02/01/2010

56 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 25.9 86 ( 63-131 ) 30 ug/L 02/01/2010

LCSD 25.1 84 3 (< 20 ) 30 ug/L 02/01/2010

Trichlorofluoromethane LCS 29.0 97 ( 68-145 ) 30 ug/L 02/01/2010

LCSD 27.4 91 6 (< 20 ) 30 ug/L 02/01/2010

P & M -Xylene LCS 64.8 108 ( 80-120 ) 60 ug/L 02/01/2010

LCSD 61.0 102 6 (< 20 ) 60 ug/L 02/01/2010

Naphthalene LCS 31.6 105 ( 75-120 ) 30 ug/L 02/01/2010

LCSD 34.3 114 8 (< 20 ) 30 ug/L 02/01/2010

o-Xylene LCS 30.9 103 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 29.1 97 6 (< 20 ) 30 ug/L 02/01/2010

Bromoform LCS 30.1 100 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 29.6 99 2 (< 20 ) 30 ug/L 02/01/2010

1-Chlorohexane LCS 48.4 108 ( 70-125 ) 45 ug/L 02/01/2010

LCSD 45.2 101 7 (< 20 ) 45 ug/L 02/01/2010

1,2,4-Trimethylbenzene LCS 33.6 112 ( 80-125 ) 30 ug/L 02/01/2010

LCSD 31.9 106 5 (< 20 ) 30 ug/L 02/01/2010

tert-Butylbenzene LCS 32.9 110 ( 80-122 ) 30 ug/L 02/01/2010

LCSD 30.8 103 7 (< 20 ) 30 ug/L 02/01/2010

1,1,1-Trichloroethane LCS 31.8 106 ( 80-122 ) 30 ug/L 02/01/2010

LCSD 29.8 100 7 (< 20 ) 30 ug/L 02/01/2010

1,1-Dichloroethane LCS 36.0 120 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 34.2 114 5 (< 20 ) 30 ug/L 02/01/2010

2-Chlorotoluene LCS 33.5 112 ( 80-125 ) 30 ug/L 02/01/2010

LCSD 31.7 106 6 (< 20 ) 30 ug/L 02/01/2010

Trichloroethene LCS 31.3 104 ( 80-125 ) 30 ug/L 02/01/2010

LCSD 29.6 99 5 (< 20 ) 30 ug/L 02/01/2010

trans-1,2-Dichloroethene LCS 31.9 106 ( 79-132 ) 30 ug/L 02/01/2010

LCSD 30.3 101 5 (< 20 ) 30 ug/L 02/01/2010

57 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichlorobenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 30.2 101 3 (< 20 ) 30 ug/L 02/01/2010

2,2-Dichloropropane LCS 32.4 108 ( 80-132 ) 30 ug/L 02/01/2010

LCSD 30.5 102 6 (< 20 ) 30 ug/L 02/01/2010

Hexachlorobutadiene LCS 31.1 104 ( 77-125 ) 30 ug/L 02/01/2010

LCSD 29.7 99 5 (< 20 ) 30 ug/L 02/01/2010

Isopropylbenzene (Cumene) LCS 32.8 109 ( 80-121 ) 30 ug/L 02/01/2010

LCSD 30.7 102 7 (< 20 ) 30 ug/L 02/01/2010

1,2-Dichloropropane LCS 33.2 111 ( 80-121 ) 30 ug/L 02/01/2010

LCSD 31.8 106 4 (< 20 ) 30 ug/L 02/01/2010

1,1-Dichloropropene LCS 32.7 109 ( 80-122 ) 30 ug/L 02/01/2010

LCSD 30.7 102 6 (< 20 ) 30 ug/L 02/01/2010

1,1,2-Trichloroethane LCS 32.0 107 ( 77-120 ) 30 ug/L 02/01/2010

LCSD 31.9 106 0 (< 20 ) 30 ug/L 02/01/2010

1,3-Dichlorobenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 02/01/2010

LCSD 30.4 101 5 (< 20 ) 30 ug/L 02/01/2010

1,2,3-Trichlorobenzene LCS 29.7 99 ( 77-120 ) 30 ug/L 02/01/2010

LCSD 30.7 102 3 (< 20 ) 30 ug/L 02/01/2010

Xylenes (total) LCS 95.6 106 ( 80-120 ) 90 ug/L 02/01/2010

LCSD 90.1 100 6 (< 20 ) 90 ug/L 02/01/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 97 ( 73-120 ) 02/01/2010

LCSD 99 3 02/01/2010

Toluene-d8 <surr> LCS 97 ( 80-120 ) 02/01/2010

LCSD 96 1 02/01/2010

4-Bromofluorobenzene <surr> LCS 103 ( 76-120 ) 02/01/2010

LCSD 103 1 02/01/2010

58 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947760 Lab Control Sample

947761 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20444

SW5030B

02/01/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS11092

SW8260B

HP 5890 Series II MS1 VJA

59 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947860 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22713

SW3010A

02/01/2010

QC results affect the following production samples:

1100319004, 1100319005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 02/02/2010

Batch

Method

Instrument

MMS6300

SW6020

Perkin Elmer Sciex ICP-MS P3

60 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947865 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22714

SW3010A

02/01/2010

QC results affect the following production samples:

1100319001, 1100319006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1020 102 ( 80-120 ) 1000 ug/L 02/02/2010

Batch

Method

Instrument

MMS6300

SW6020

Perkin Elmer Sciex ICP-MS P3

61 of 80
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Prep

947982 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX22248

SW3520C

02/01/2010

QC results affect the following production samples:

1100319001, 1100319004, 1100319005, 1100319006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.84 97 ( 75-125 ) 5 mg/L 02/02/2010

Surrogates 

5a Androstane <surr> LCS 98 ( 60-120 ) 02/02/2010

Batch

Method

Instrument

XFC9100

SW8015C

HP 7890A FID SV E F

62 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

947861 Matrix Spike

947862 Matrix Spike Duplicate

1100328001

Water (Surface, Eff., Ground)

MXX22713

3010 H20 Digest for Metals ICP-MS

02/01/2010

QC results affect the following production samples:

1100319004, 1100319005

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Metals by ICP/MS

Lead MS (0.620) U 1050 105 ( 80-120 ) 1000 ug/L 02/02/2010

MSD 1010 101 4 (< 15 ) 1000 ug/L 02/02/2010

Batch

Method

Instrument

MMS6300

SW6020

Perkin Elmer Sciex ICP-MS P3

63 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

MXX22714

3010 H20 Digest for Metals ICP-MS

02/01/2010

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS (0.620) U 985 99 ( 80-120 ) 1000 ug/L 02/02/2010

BMSD 1010 101 3 (< 15 ) 1000 ug/L 02/02/2010

Batch

Method

Instrument

MMS6300

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS (60.0) U 494 110* ( 79-108 ) 450 ug/L 02/01/2010

BMSD 498 111* 1 (< 20 ) 450 ug/L 02/01/2010

Surrogates 

4-Bromofluorobenzene <surr> BMS 57.9 116 ( 50-150 ) 02/01/2010

BMSD 53.5 107 8 02/01/2010

Batch

Method

Instrument

VFC9852

SW8015C

HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS 1.49 5.83 80 ( 75-125 ) 5.43 mg/L 02/02/2010

BMSD 6.19 84 6 (< 30 ) 5.62 mg/L 02/02/2010

Surrogates 

5a Androstane <surr> BMS .0941 87 ( 50-150 ) 02/02/2010

BMSD 0.0948 84 1 02/02/2010

Batch

Method

Instrument

XFC9100

SW8015C

HP 7890A FID SV E F

Volatile Gas Chromatography/Mass Spectroscopy

64 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

VXX20444

Volatiles Extraction AFCEE 3.1 8260 (

02/01/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS (0.240) U 31.9 106 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 02/01/2010

Toluene BMS (0.620) U 33.7 112 ( 77-120 ) 30.0 ug/L 02/01/2010

BMSD 33.3 111 1 (< 20 ) 30.0 ug/L 02/01/2010

Ethylbenzene BMS (0.620) U 33.4 111 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 33.1 110 1 (< 20 ) 30.0 ug/L 02/01/2010

n-Butylbenzene BMS (0.620) U 36.5 122 ( 80-124 ) 30.0 ug/L 02/01/2010

BMSD 37.1 124 2 (< 20 ) 30.0 ug/L 02/01/2010

1,4-Dichlorobenzene BMS (0.300) U 33.6 112 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 34.0 113 1 (< 20 ) 30.0 ug/L 02/01/2010

1,2-Dichloroethane BMS (0.300) U 33.5 112 ( 80-129 ) 30.0 ug/L 02/01/2010

BMSD 33.5 112 0 (< 20 ) 30.0 ug/L 02/01/2010

1,3,5-Trimethylbenzene BMS (0.620) U 35.2 117 ( 80-128 ) 30.0 ug/L 02/01/2010

BMSD 35.6 119 1 (< 20 ) 30.0 ug/L 02/01/2010

4-Chlorotoluene BMS (0.620) U 35.3 118 ( 79-128 ) 30.0 ug/L 02/01/2010

BMSD 36.4 121 3 (< 20 ) 30.0 ug/L 02/01/2010

Chlorobenzene BMS (0.300) U 33.2 111 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 32.9 110 1 (< 20 ) 30.0 ug/L 02/01/2010

4-Methyl-2-pentanone (MIBK) BMS (6.20) U 104 116 ( 69-134 ) 90.0 ug/L 02/01/2010

BMSD 98.0 109 6 (< 20 ) 90.0 ug/L 02/01/2010

cis-1,2-Dichloroethene BMS (0.620) U 30.7 102 ( 80-125 ) 30.0 ug/L 02/01/2010

BMSD 31.1 104 1 (< 20 ) 30.0 ug/L 02/01/2010

4-Isopropyltoluene BMS (0.620) U 35.8 119 ( 80-125 ) 30.0 ug/L 02/01/2010

BMSD 36.2 121 1 (< 20 ) 30.0 ug/L 02/01/2010

cis-1,3-Dichloropropene BMS (0.300) U 36.5 122* ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 35.8 119 2 (< 20 ) 30.0 ug/L 02/01/2010

n-Propylbenzene BMS (0.620) U 35.1 117 ( 80-129 ) 30.0 ug/L 02/01/2010

BMSD 36.0 120 3 (< 20 ) 30.0 ug/L 02/01/2010

Styrene BMS (0.620) U 33.3 111 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 32.8 109 1 (< 20 ) 30.0 ug/L 02/01/2010

Dibromomethane BMS (0.620) U 33 110 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 32.9 110 1 (< 20 ) 30.0 ug/L 02/01/2010

trans-1,3-Dichloropropene BMS (0.620) U 34.9 116 ( 80-124 ) 30.0 ug/L 02/01/2010

BMSD 35.2 117 1 (< 20 ) 30.0 ug/L 02/01/2010

1,2,4-Trichlorobenzene BMS (0.620) U 34.4 115 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 34.3 114 0 (< 20 ) 30.0 ug/L 02/01/2010

Acetone BMS (6.20) U 88.4 98 ( 50-135 ) 90.0 ug/L 02/01/2010

BMSD 91.6 102 4 (< 20 ) 90.0 ug/L 02/01/2010

1,1,2,2-Tetrachloroethane BMS (0.300) U 35.8 119 ( 76-123 ) 30.0 ug/L 02/01/2010

BMSD 35.9 120 0 (< 20 ) 30.0 ug/L 02/01/2010

65 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

VXX20444

Volatiles Extraction AFCEE 3.1 8260 (

02/01/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS (1.24) U 37.7 126 ( 73-130 ) 30.0 ug/L 02/01/2010

BMSD 36.9 123 2 (< 20 ) 30.0 ug/L 02/01/2010

Methyl-t-butyl ether BMS (3.00) U 56.4 125* ( 80-120 ) 45.0 ug/L 02/01/2010

BMSD 55.7 124* 1 (< 20 ) 45.0 ug/L 02/01/2010

Tetrachloroethene BMS (0.620) U 33.4 111 ( 79-122 ) 30.0 ug/L 02/01/2010

BMSD 32.6 109 2 (< 20 ) 30.0 ug/L 02/01/2010

Dibromochloromethane BMS (0.300) U 31.3 104 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 30.4 101 3 (< 20 ) 30.0 ug/L 02/01/2010

1,3-Dichloropropane BMS (0.240) U 35 117 ( 80-121 ) 30.0 ug/L 02/01/2010

BMSD 34.4 115 2 (< 20 ) 30.0 ug/L 02/01/2010

1,2-Dibromoethane BMS (0.620) U 33.8 113 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 33.8 113 0 (< 20 ) 30.0 ug/L 02/01/2010

Carbon tetrachloride BMS (0.620) U 33.4 111 ( 80-126 ) 30.0 ug/L 02/01/2010

BMSD 33.1 110 1 (< 20 ) 30.0 ug/L 02/01/2010

1,1,1,2-Tetrachloroethane BMS (0.300) U 35.2 117 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 34.8 116 1 (< 20 ) 30.0 ug/L 02/01/2010

Chloroform BMS (0.600) U 31.8 106 ( 80-124 ) 30.0 ug/L 02/01/2010

BMSD 31.8 106 0 (< 20 ) 30.0 ug/L 02/01/2010

Bromobenzene BMS (0.620) U 32.6 109 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 33.0 110 2 (< 20 ) 30.0 ug/L 02/01/2010

Chloromethane BMS (0.620) U 36.3 121 ( 67-125 ) 30.0 ug/L 02/01/2010

BMSD 35.8 119 1 (< 20 ) 30.0 ug/L 02/01/2010

1,2,3-Trichloropropane BMS (0.620) U 33.2 111 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 33.6 112 1 (< 20 ) 30.0 ug/L 02/01/2010

Bromomethane BMS (1.88) U 33.9 113 ( 30-140 ) 30.0 ug/L 02/01/2010

BMSD 35.6 119 5 (< 20 ) 30.0 ug/L 02/01/2010

Bromochloromethane BMS (0.620) U 29.1 97 ( 77-129 ) 30.0 ug/L 02/01/2010

BMSD 29.3 98 1 (< 20 ) 30.0 ug/L 02/01/2010

Vinyl chloride BMS (0.620) U 30.6 102 ( 72-145 ) 30.0 ug/L 02/01/2010

BMSD 30.8 103 1 (< 20 ) 30.0 ug/L 02/01/2010

Dichlorodifluoromethane BMS (0.620) U 35.9 120 ( 62-153 ) 30.0 ug/L 02/01/2010

BMSD 35.9 120 0 (< 20 ) 30.0 ug/L 02/01/2010

Chloroethane BMS (0.620) U 30.3 101 ( 67-133 ) 30.0 ug/L 02/01/2010

BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 02/01/2010

sec-Butylbenzene BMS (0.620) U 35.5 118 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 36.0 120 1 (< 20 ) 30.0 ug/L 02/01/2010

Bromodichloromethane BMS (0.300) U 34.9 116 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 34.7 116 1 (< 20 ) 30.0 ug/L 02/01/2010

1,1-Dichloroethene BMS (0.620) U 29.1 97 ( 76-130 ) 30.0 ug/L 02/01/2010

BMSD 28.7 96 2 (< 20 ) 30.0 ug/L 02/01/2010

66 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

VXX20444

Volatiles Extraction AFCEE 3.1 8260 (

02/01/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS (6.20) U 100 111 ( 66-136 ) 90.0 ug/L 02/01/2010

BMSD 102 114 2 (< 20 ) 90.0 ug/L 02/01/2010

Methylene chloride BMS (2.00) U 27.9 93 ( 63-131 ) 30.0 ug/L 02/01/2010

BMSD 27.7 93 1 (< 20 ) 30.0 ug/L 02/01/2010

Trichlorofluoromethane BMS (0.620) U 30.8 103 ( 68-145 ) 30.0 ug/L 02/01/2010

BMSD 30.7 102 1 (< 20 ) 30.0 ug/L 02/01/2010

P & M -Xylene BMS (1.24) U 68.2 114 ( 80-120 ) 60.0 ug/L 02/01/2010

BMSD 67.7 113 1 (< 20 ) 60.0 ug/L 02/01/2010

Naphthalene BMS (1.24) U 35.9 120 ( 75-120 ) 30.0 ug/L 02/01/2010

BMSD 36.1 120 0 (< 20 ) 30.0 ug/L 02/01/2010

o-Xylene BMS (0.620) U 32.5 108 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 02/01/2010

Bromoform BMS (0.620) U 32.3 108 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 30.9 103 4 (< 20 ) 30.0 ug/L 02/01/2010

1-Chlorohexane BMS (0.620) U 50.5 112 ( 70-125 ) 45.0 ug/L 02/01/2010

BMSD 50.5 112 0 (< 20 ) 45.0 ug/L 02/01/2010

1,2,4-Trimethylbenzene BMS (0.620) U 34.9 116 ( 80-125 ) 30.0 ug/L 02/01/2010

BMSD 36.1 120 3 (< 20 ) 30.0 ug/L 02/01/2010

tert-Butylbenzene BMS (0.620) U 34.2 114 ( 80-122 ) 30.0 ug/L 02/01/2010

BMSD 34.9 116 2 (< 20 ) 30.0 ug/L 02/01/2010

1,1,1-Trichloroethane BMS (0.620) U 33.5 112 ( 80-122 ) 30.0 ug/L 02/01/2010

BMSD 32.9 110 2 (< 20 ) 30.0 ug/L 02/01/2010

1,1-Dichloroethane BMS (0.620) U 37.9 126* ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 38.0 127* 0 (< 20 ) 30.0 ug/L 02/01/2010

2-Chlorotoluene BMS (0.620) U 35 117 ( 80-125 ) 30.0 ug/L 02/01/2010

BMSD 36.1 120 3 (< 20 ) 30.0 ug/L 02/01/2010

Trichloroethene BMS (0.620) U 33.5 112 ( 80-125 ) 30.0 ug/L 02/01/2010

BMSD 32.7 109 2 (< 20 ) 30.0 ug/L 02/01/2010

trans-1,2-Dichloroethene BMS (0.620) U 33.6 112 ( 79-132 ) 30.0 ug/L 02/01/2010

BMSD 33.3 111 1 (< 20 ) 30.0 ug/L 02/01/2010

1,2-Dichlorobenzene BMS (0.620) U 33 110 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 33.6 112 2 (< 20 ) 30.0 ug/L 02/01/2010

2,2-Dichloropropane BMS (0.620) U 34.6 115 ( 80-132 ) 30.0 ug/L 02/01/2010

BMSD 34.8 116 1 (< 20 ) 30.0 ug/L 02/01/2010

Hexachlorobutadiene BMS (0.620) U 33.2 111 ( 77-125 ) 30.0 ug/L 02/01/2010

BMSD 32.3 108 3 (< 20 ) 30.0 ug/L 02/01/2010

Isopropylbenzene (Cumene) BMS (0.620) U 34.5 115 ( 80-121 ) 30.0 ug/L 02/01/2010

BMSD 34.4 115 0 (< 20 ) 30.0 ug/L 02/01/2010

1,2-Dichloropropane BMS (0.620) U 35.4 118 ( 80-121 ) 30.0 ug/L 02/01/2010

BMSD 35.5 118 0 (< 20 ) 30.0 ug/L 02/01/2010

67 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

VXX20444

Volatiles Extraction AFCEE 3.1 8260 (

02/01/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS (0.620) U 34.8 116 ( 80-122 ) 30.0 ug/L 02/01/2010

BMSD 34.2 114 2 (< 20 ) 30.0 ug/L 02/01/2010

1,1,2-Trichloroethane BMS (0.620) U 34.7 116 ( 77-120 ) 30.0 ug/L 02/01/2010

BMSD 33.7 112 3 (< 20 ) 30.0 ug/L 02/01/2010

1,3-Dichlorobenzene BMS (0.620) U 33.7 112 ( 80-120 ) 30.0 ug/L 02/01/2010

BMSD 34.0 113 1 (< 20 ) 30.0 ug/L 02/01/2010

1,2,3-Trichlorobenzene BMS (0.620) U 31.8 106 ( 77-120 ) 30.0 ug/L 02/01/2010

BMSD 33.6 112 5 (< 20 ) 30.0 ug/L 02/01/2010

Xylenes (total) BMS (2.00) U 101 112 ( 80-120 ) 90.0 ug/L 02/01/2010

BMSD 99.6 111 1 (< 20 ) 90.0 ug/L 02/01/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 29.4 98 ( 73-120 ) 02/01/2010

BMSD 29.7 99 1 02/01/2010

Toluene-d8 <surr> BMS 29.2 97 ( 80-120 ) 02/01/2010

BMSD 29.2 97 0 02/01/2010

4-Bromofluorobenzene <surr> BMS 30.9 103 ( 76-120 ) 02/01/2010

BMSD 31.3 104 1 02/01/2010

Batch

Method

Instrument

VMS11092

SW8260B

HP 5890 Series II MS1 VJA

Polynuclear Aromatics GC/MS

68 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

XXX22249

3520 Liquid/Liquid Ext for 8270 SIM

02/01/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS (0.0320) U .484 88 ( 50-101 ) 0.549 ug/L 02/02/2010

BMSD 0.419 76 14 (< 30 ) 0.549 ug/L 02/02/2010

Acenaphthene BMS (0.0320) U .447 81 ( 45-93 ) 0.549 ug/L 02/02/2010

BMSD 0.411 75 9 (< 30 ) 0.549 ug/L 02/02/2010

Fluorene BMS (0.0320) U .465 85 ( 50-98 ) 0.549 ug/L 02/02/2010

BMSD 0.432 79 7 (< 30 ) 0.549 ug/L 02/02/2010

Phenanthrene BMS (0.0320) U .486 89 ( 50-104 ) 0.549 ug/L 02/02/2010

BMSD 0.471 86 3 (< 30 ) 0.549 ug/L 02/02/2010

Anthracene BMS (0.0320) U .474 86 ( 55-105 ) 0.549 ug/L 02/02/2010

BMSD 0.467 85 1 (< 30 ) 0.549 ug/L 02/02/2010

Fluoranthene BMS (0.0320) U .632 115* ( 58-109 ) 0.549 ug/L 02/02/2010

BMSD 0.646 117* 2 (< 30 ) 0.549 ug/L 02/02/2010

Pyrene BMS (0.0320) U .549 100 ( 56-105 ) 0.549 ug/L 02/02/2010

BMSD 0.558 102 2 (< 30 ) 0.549 ug/L 02/02/2010

Benzo(a)Anthracene BMS (0.0320) U .59 107 ( 55-120 ) 0.549 ug/L 02/02/2010

BMSD 0.601 109 2 (< 30 ) 0.549 ug/L 02/02/2010

Chrysene BMS (0.0320) U .497 91 ( 56-109 ) 0.549 ug/L 02/02/2010

BMSD 0.509 93 2 (< 30 ) 0.549 ug/L 02/02/2010

Benzo[b]Fluoranthene BMS (0.0320) U .557 101 ( 45-120 ) 0.549 ug/L 02/02/2010

BMSD 0.564 103 1 (< 30 ) 0.549 ug/L 02/02/2010

Benzo[k]fluoranthene BMS (0.0320) U .525 96 ( 56-112 ) 0.549 ug/L 02/02/2010

BMSD 0.530 97 1 (< 30 ) 0.549 ug/L 02/02/2010

Benzo[a]pyrene BMS (0.0320) U .588 107 ( 57-110 ) 0.549 ug/L 02/02/2010

BMSD 0.593 108 1 (< 30 ) 0.549 ug/L 02/02/2010

Indeno[1,2,3-c,d] pyrene BMS (0.0320) U .561 102 ( 55-111 ) 0.549 ug/L 02/02/2010

BMSD 0.558 102 1 (< 30 ) 0.549 ug/L 02/02/2010

Dibenzo[a,h]anthracene BMS (0.0320) U .56 102 ( 54-113 ) 0.549 ug/L 02/02/2010

BMSD 0.567 103 1 (< 30 ) 0.549 ug/L 02/02/2010

Benzo[g,h,i]perylene BMS (0.0320) U .545 99 ( 49-116 ) 0.549 ug/L 02/02/2010

BMSD 0.548 100 1 (< 30 ) 0.549 ug/L 02/02/2010

Naphthalene BMS (0.0664) U .363 66 ( 44-89 ) 0.549 ug/L 02/02/2010

BMSD 0.288 52 23 (< 30 ) 0.549 ug/L 02/02/2010

1-Methylnaphthalene BMS (0.0320) U .367 67 ( 42-92 ) 0.549 ug/L 02/02/2010

BMSD 0.312 57 16 (< 30 ) 0.549 ug/L 02/02/2010

2-Methylnaphthalene BMS (0.0320) U .302 55 ( 45-89 ) 0.549 ug/L 02/02/2010

BMSD 0.254 46 17 (< 30 ) 0.549 ug/L 02/02/2010

Surrogates 

Terphenyl-d14 <surr> BMS .577 105 ( 50-126 ) 02/02/2010

BMSD 0.563 102 3 02/02/2010

69 of 80
Matrix

SGS Ref.# Printed Date/Time 02/05/2010 9:27

Batch

Method

Date

Original

Prep

1100319002 Billable Matrix Spike

1100319003 Billable Matrix Spike Dup.

1100319001

Water (Surface, Eff., Ground)

XXX22249

3520 Liquid/Liquid Ext for 8270 SIM

02/01/2010

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5285

8270D SIMS

HP 6890/5973 MS SVQA

70 of 80
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80 of 80
Appendix B 

Monitoring Well Construction Logs 
GEOLOGIC BOREHOLE LOG

Location: RHFSF Station Name: Location Type:

Location Description:

RHMW04

Establishing Company: TEC Inc.

Drilling Foreman: Tomas Fernandez Drilling Company: Valley Well Drilling

Geologist: N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: MSL

Drilling Sampling Method: Borehole Diameter (in): 8

Total Depth (ft): Date Drilling Started: 22 July 2005 Date Drilling Ended: 26 July 2005

Monitoring Well

Remarks: 

Rock Coring

west. access rd., S of Navy Firing Range

313.03

320.5

Page 1 of 2
GEOLOGIC BOREHOLE LOG

Location: RHFSF Station Name: Location Type:

Location Description:

RHMW04

Establishing Company: TEC Inc.

Drilling Foreman: Tomas Fernandez Drilling Company: Valley Well Drilling

Geologist: N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: MSL

Drilling Sampling Method: Borehole Diameter (in): 8

Total Depth (ft): Date Drilling Started: 22 July 2005 Date Drilling Ended: 26 July 2005

Monitoring Well

Remarks: 

Rock Coring

west. access rd., S of Navy Firing Range

313.03

320.5

Page 2 of 2