M. J. "MIKE" FOSTER, JR.

GOVERNOR

April 30, 1997

Ms. Jane Saginaw, Administrator

U.S. EPA, Region 6

1445 Ross Avenue, Suite 1200

Dallas, TX 75202

Dear Ms. Saginaw:

~tat.e of 'lfioulEilana

OFFICE OF THE GOVERNOR

70804-9004

POST OFFICE BOX 94004

(504) 342-7015

The State of Louisiana has approved and is submitting revisions to our State Implementation Plan

(SIP). Enclosed are Louisiana's Revised Statutes and changes to LAC 33:IILChapters 1, 5, 15,

21, and 25. Also Chapter 30, which repeals Chapter 60, is being added for inclusion in the SIP.

Five (5) copies showing that the rule revision went through the public notice process are

attached. Please contact the Air Quality staff through Gus Von Bodungen at (504) 765-0102 if

you have any questions.

Sincerely,

~.\~.

M.J. "Mike" Foster, Jr.

CJr

Enclosures (5)

c: Mr. Thomas Diggs, EPA, Region 6
COI\lTEI\lTS

Letter to Bob Hannah from Thomas H. Diggs dated.December 2, 1993

Louisiana Revised Statutes with revisions through the 1996

Legislative Session for Titles:

1) 36

2) 49

3) 30

4) 42

5) 44

Chapter 5-A Dept of Environmental Quality

Chapter 24 Implementation of Reorganization

Chapter 13 Administrative Procedure

Subtitle II Environmental Quality

Chapter 1 General

Chapter 2 Dept of Environmental Quality

Chapter 3 LA Air Control Law

Chapter 15 Code of Governmental Ethics

Chapter 1 Public Records

-~-

•.

AQ 145 Incorporation by Reference (LAC 33:III.Chapters 1, 15,

21, 25, 29, 30, 31, 60, 61, and 64)
UNITED STATES ENVlfIOIIIENTAl. PHO IECTION AGENCY

IlEGlON8

1415 ROSS "\/BlUE, SUITE 1200

IW lAS. TX 75202-2133

11·-·· ..... C.,.. ~,'t3 .

Mr. Bob RanMh.. Adalnl.trat.or

Air QUali~y Ilegul.atory Division

t.<>uiai""" Depart_n~ Of Environ-ental QUal1~y

P.o. Box 82135

Baton 1lcu<I8. Louisiana 70884-2135

Dear Jfr~ B.nnah:~1-

This: lertar is: ~o conCi... thn ~"e t.<>u18iana Daparaeat of

Knvlro......tal O,,"li~y _. DO~ Deed to inolude public noUca/=-en~ and public hurin9 cIocImcDta~OIl 10 ita SUIa1~tal

oC State s~atutes as ravlsioD5 to. the State .lJIplAaenta~ion Plan.

Ka have d1scua...ect thh: tSctlCl with ReqlnMl eounae.l and bave

confiDed ~~ the le9lsla~lv8 procaaa to reviee ..tatutua is

functlonally equivalent to notice and ea-.ent.

If you have any Ciuost.iona, plea•• cont:a~ .. At (214) 655-721.4 or

Jeanne McDaniel a a~ (214) 655-7254.

sinceroly y~~ .

- Je.. 400 ~fl s

ThOllas B. Di99~ Chief

Planning Section (<<5T-AP)

ce: ADne~~. Sharp

t.<>uidana Departllent oC

Bnvlronaent.al Quality

00138
RULE

RULE

artment of Environmental Quality

Air Quality and Radiation Prate ion

Air Quality Division

ent New Source Review Proc dUres

AC 33:1II.504) (AQI46)

ofthe Louisiana Envir ental Quality

et seq., and in acco dance with the

provisions ofthe A inistrative Procedur Act, R.S.49:950

et se'!.., the secretary as amended the r Quality Division

regulations, LAC 33:1 .504 (AQI46).

The deparnnent is a pting a provi on in the 1990 Clean

Air Act amendments w ich provid for a special Rule for

modifications ofsources itting I tons or more. Affected

sources are any major s ionary ource of volatile organic

compounds located in are which emits, or has the

potential to emit, 100 to more of volatile organic

compounds (VOCs) per ye enever there is any change

in emissions of VOCs fro y discrete operation, unit, or

other pollutant-emitting a IV at the source, such increase

shall be considered a m ific ion fat purposes of Section

I72(cX5) and"Section I (a). is Rule allows the o,wner or

operator of the sourc to offse the increase by a greater.

reduction in emission of VOCs fr m other operations, units,

or activities within e source at internal offset ratio of at

least 1.3 to I, in li ofthe requirem ts of Section 173(a)(2)

concerning the 10 est achievable eml sian rate (LAER), This

revision is in a ordance with Sectio I82(c)(8) ofthe 1990

Clean Air Act endments.

Title 33

NVIRONMENTAL QU

Part III. Air

Chapter . Permit Procedures

§504. N attainment New Source Reviel:rocedures ... (See Prior TeX! in A-D.2]

3. Notwithstanding Subsection 0.2 of. is Section, in

the c e oCany major stationary Source that emits or has the I

Gus Von Bodungen

Assistant Secretary

rcadlng of \ ,OOG 'P'Pm.., Qt %teater for va(ves~ connectors,

pressure relief devices, and process drains; 5;000 ppmv for

pumps and compressors; or 10,000 ppmv for agitators, as

outlined in Subsection 0 of this Section, when tested by

Method 21 (40 CFR part 60, appendix A, as incorporated by

reference at LAC 33:1I1.3003).

••• [Sec PrIor Text in C.l.b •G.6]

AUTHORITY NOTE: Promulgated in accordance with R.S.

30:20R

.':JJSTORICAL NOTE: Promulgated by the Department of

Environmental Quality, Office of Air Quality and Radiation

Projection, Air Quality Division, LR 20:1102 (October 1994),

rcpromulgated LR 20:1279 (November 1994), amended LR 22: 1129

(November 1996), LR 22:1212 (DeCember 1996), repromulgated

LR 23:197 (February 1997).

(EditO,.'" Nole: AQI4S was referenced IS. final Rule in the December

20, 1996, issue ofthe !tnlUUJM Reguter, The document provided to the

Office ofthe Stale Register c:ontained III incorrect version of the Paragraph

below. The corrected lext. as it should have appeared in AQI4S, is being

published.)

Title 33

ENVIRONMENTAL QUALITY

Part UI. Air

Cbapter 21. Control of Emission of Organic

Compounds

Subcbapter A. General

§2122. Fugitive Emission Control for Ozone

Nonattainment Areas

••• [See Prior Text in A ..c. I]

a. No component in petroleum refineries, SOCMI,

MTIlE, and polymer manufacturing industry shall be allowed

to leak volatile organic compounds exceeding an instrument

Department ofEnvironmental Quality

Office of Air Quality and Radiation Protection

Air Quality Division

Fugitive Emission Control for Ozone

Nonattainment Areas (LAC 33:11I.2122XAQI45)

}o

/ 3.-C.

/ AUTHORITY NOTE: Promulgated in accordance wilb R.S.

3:2093 and R.S. 3:2131.

HI ORICAL NOTE: Promulgated by lbe Departme of

Agricult and Forestry, Livestock Sanitary Board, LR 1:234

, (March 19 ), amended LR 11:61~ (June 198~), L 23:196

(February 19 ).

§11717. Re uiring the Reporting ofContagi S Diseases

A. In order 0 improve the protection a e livestock

industry from th ffects of contagious dise es oflivestock,

all veterinarians 'censed in the state f Louisiana, are

required to report the state veterin . , by telephone or

wire, within 24 hou after diagnosis r tentative diagnosis,

the OCCUTrence of su ected occ ence of the fa1I0wing

contagious diseases: hog c era, anthrax, vesicular

condition, scabies, equ e ephalomyelitis, pulloruml

typhoid, pseudorabies, N Ie (OlE List A Diseases),

Avian Influenza (OlE) st A Diseases), Ornithosis,

Paramyxovirus (Other th weastle Disease), Infectious

Encephalomyelitis, Inf! ious gotracheitis (other than

vaccine induced), or yother d ease condition which may

seriously threaten welfare of e livestock and poultry

industry.

B.-E....

AUTHORITY

3:2093, R.S. 3:

HISTORIC NOTE: Promulgated by lbe Department of

Agriculture d Forestry, Louisiana Livestoc

11:61~ (J e 198~), amended LR 1~:813 (Octo

(May 19 ), LR 23: 197 (February 1997).

)

-.' 197

Louisillnll R~9"stll' Vol. 13, No. 1 F~b,ullry 10, 1997
,

RULE

Gus VOn Bodungen

Assistant S~

RULE

Hermaa Robinson

Assist&Dt secretary

ency Response (LAC 33:1.691S) (OSIIA)

Departmeat ofEDvlroDmeDtal Qnality

Office ofthe Secreta.,.

96121054

•A porIiaD oflbe RaIc wII1cII 1IppCIIId"'_ uribe OCtober 1P96,LtIoIb-.6I*' is boIDI npoblisbed • Lou_A_ Code cIadJoo ID 16915.....)

Title 33

,,1\T\i'mONMENTAL QUALITY

Part Office ofthe Secretary

Subpart 4. E rcency Response R~nlatlonl

Chapter 69. Emq cy Resprmse R~oDl

§6915. Transportatlo Receipt, and S~race of C

Material from e Cleanup anror Abatement of

aD Orr-slte Emer\ency Cond~iOD .

A. Transportation, receip} aad ~ge of aay material

generated as a result ofthe CI~Pdlor abatement ofaay

off-site C1!!ergency condition, n specifically authorized

by the LOtlIsIana Adminlstrat' 'ode, Title 33, Part V.

Subpart I, may be authorized by administrative authority.

B. These regulatious supptim t aad do not replace

requirC1!!ents of 49 CFR. I. 177 that remain ful1y

applicable to the of nus materials.

AUTIIORITY NOTE: ulpled in co with R.S.

30:2011(0)(1),(14), ad (I

HISTORICAL NOTE: ulpled' by •

Eovironmc:nlll Quality, oflbe Secretary,

1996), repromu1plcd :1212 (December I

__..........__...... _ .. ~-W ..._--. _d :-pl~ft'l08n••t-:Oft 01'

delegation ofautbority for the NSPS program. The NSPS and

the authority for EPA to delegate authority ofthat program to

the state is established in the Clem Air Act Amendments of

1m.Secticm III. ThisrulC1!!aking Is applicable to stalill1W)'

sourcesstatewide. .

The full text ofthis Rule may be obtained from the Office

ofthe State Register. 1051 North Third Street, Baton Rouge,

LA 70102.

96121Q62

Department ofEnvironmental Quality

Office of Solid and Hazardous Waste

/ Solid Waste Division

Waste Tire (LAC 33:V1l.Chapler IOS)(SW021) \ (

u fer the aulbority ofthe Louisiana Environmental Quality \

AC'l'::.S. 30:200 I el seq., and in accordance with the / .

1212

lpJIloariD.& ... Plies 1124- is~_bl_'" ·or •.

Gus Von Bodungen

Assistant Secretary

"'rdaace with R.s.

Accidem Prevention Pro

C 33:IU.S901) (AQI2 ~., .

It::=:t~.:~~C orthil Seclion, the la 40 CFR.PIIt 61 (lui)' I.

epartment ofEnvironmental QnaUty

of Air Qnality and Radiation Protec • n

Air QnaUty Division

.. .~.,

·\

RULE

96121010

Department ofEnvironmental Quality

Office of Air Quality and Radiation Protection

Air QuaUty DIvIsJoD

InCOlJlOration by RefereJlce (LAC 33:m.Chapten I, 15.21,

25.29,30.31,60.61 aad 64) (AQI4S)

Underthe authority ofthe LouisiaDa EDvironmcIItal QuaIity

Act, R.S. 30:2001 et seq.. &ad in accordaDce with the

provisioDS ofthe Administrative Procedure Act, R.S. 49:950

et seq., the Secretary has amended the Air Quality Divisioa

reg1,l1atiODS, LAC33:IU.Chaptc:rs I, IS, 21. 15. 29, 3D, 31, 60,

61 aad 64 (AQI4S).

This Rule repeals LAC 33:m.Chapters 31, 60 (except

§6099 which is moved aad renumbered as LAC

33:III:2901.G), 61 (except Subchapter A which is moved aad

renumbered as Subcbapter N in Chapter 21>, and 64 from

LAC 33:III and incorporates by reference into Chapter 30

federal regulatioos in 40 CFR Part 60 - Standards of

Performance for New Stationary Sources. Revisions are also

made in LAC 33:II1.Chapters I, 15,21,25 and 29, so that

referenced LAC cites agree wilb changes per this rulemaking,

and to add 40 CFR references. These changes w!1J expedile
FINAL lWLE/DECEMBER 20, 1996

Tide 33

ENVIRONMENTAL QUALITY

partmAir .

Chapter 1. General Provisions

§111. Definition.

•••

AQ145

-,_.._-_..._._-_..._-,---

• (See Prior Tut]

GoodPerformanceLevel-an operating 1eveI reac:bed when no more than two percent of

the valves in VOC service at a W:ility are leaking at a rate of 10,000 parts per million by volume

(ppmv) or greater as determined by Reference Method 21 "Determination ofVolatile Organic

Compound Leaks" in tile Division's Sowee Test hfauuaf4Q CFR part 60 appendix A. as

iDCOQ)0rated by reference at LAC nW 3003.

•••

[See Prior Tut]

PartiClllate Matter Emi,;:sjons-all finely divided solid or liquid material, other than

uncombined water, emitted to the ambient air as measured by Method 5 (SecLA:C 33.m.6elS)in

40 CPR part 60 ap,pendjx A as ;ncp[porated by reference at LAC nm3003.

•••

[See Prior Tut]

&ferenceMethod-any m~hod of"sampling and analyzing for an air pollutant as

descnbed in die Ail Quant) Division's Test Mllllmd40 CPR part 60 lUlPendjx A. as jnco[porated

by reference at LAC 33·m 3003.

•••

[See Prior Tut]

AUIHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnviromnental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

LR.14:348 (June 1988),LR 15:1061 (December 1989), amended by the Office ofAir Quality and

Radiation Protection, Air Quality Division, LR 17;777 (August 1991), LR21:1081 (October

1995), LR '

1
FINAL RULE/DECEMBER 20, 1996

TIde 33

ENVIRONMENTAL QUALITY

PartllLAir

Olaptcr 15. EmissioD StaDdardJ (or SWf'ur Dioxide

AQ145

§1S03. £minion I.imitations

& used in this Section a thru-hour avuagt means the average emissions for any three

consecutive ooe-bour periods (each commencing on the hour), provided that the number ofthreehour perioda during which the SOl limitation is exceeded is not greater than the number ofonehour periods duringwhich the SOz limitation is exceeded.

•••

[See PriorTmiD A-D.%]

Particulate 1) Methods 1 tLAC 33.HI.68el). 2-(bA€

33:B1:6863).3 (LAC 33.Hi6969). 4

33.HI:6EH3), S(L\C

33:HI:6e1S)(40 CfR pan 60 appenglX

A 1$ incorpD01ed by reference at

LAC 33·m 3003) orb\€

33:1H:3IIS§60 8 of40 CPR part 60 as

inCOtWl'Jted by reference at LAC

2
FINAL ROLE/OECEMBER 20, 1996 AQ145

Sulfur Oxides 1)- Seidman, Analytical Chemistry Volume

30, page 1680 (1958),WOetennination

ofSulfur Oxides in Stack Gases.•

2) Shell Developmcm Company method

for the Determination ofsulfur

Dioxide and Sulfur Trioxide PHS 999

AP-13 Appendix B, pages 85-87,

"Atmospheric Emissions Sulfuric Acid

Manu&cturing-Processes "

3) Reich Test for Sulfur Dioxide,

"Atmospheric Emissionsfrom Sulfuric

Acid Manufacturing Process" PHS 999

AP-13 A enoD( D, a es 7~0.

4) The Modified Monsanto Company

Method, "Atmospheric Emissions from

Sulfuric Acid Manufacturing Process"

PHS 999 AP-13, Appendix B. pages

61-67_

5) Test Methods 1 (LA€33:1£ 6661), 2

(LAC 33.IH:6663). 3i1:*€

33.IH:6e6~.4 (LAC 33.IH.6913), 6

(LAC 33.ffi.66iS), and 8-(b't€

33 .BI:6&4~ (40 CPR part 60.

appendix A as iocOJ;poTlted b;y

reference at LAC 33-m 30031. or b't€

33:lH:311S§6O 8 o£40 CFR part 60 as

incoQ)OI'ilted by reference at LAC

. 300.

3
-

FINAL ROLE/DECEMB&R 20, 1996 AQ145

Oxides or

Nitrogen

1) Test Methods 1 (LA:C 33.::i.:,061), Z

(LA€33:fH:6003), 3-(b\€

33:HI:6OO9), 4 (LA€3J:m:6eIJ), and

7 (LAC 33:HL6e33)(40 CFR part 60

append"nc A as inm»orated by

rcfcrcn<:e at LAC 33·m 300lt or b't€

33:fH:3115§60 8 of4O CfR part 60 u

incm:poratcd by rcferexw;c at LAC

33·m 3003.

VlSloJe Emissions 1)

2)

Total Fluoride 1)

Total Reduced 1)

Sulfur (TRS)

2)

. Methods 1 (LA€J3.Hl:6001). 2 (LAC

3J:HI::6OOJ). 3 (LAC 3J.Hi:6OO9).

13A (LA€33::HI:6e57) and 13B~

J3::H!:6eS9X40 CFR part 60 appcncf1X

A as jncorporated by o:feretlCC ot

Method 16 (Ur:€JJ:HI:606S)(40 CFR

part 60 aPllCDdjx A pr 660 8 ofCFR

Part 60 U incorporated by referencC at

LAC n·m 3003) 01 LA€33:IH:311S.

Coulometric titration by method

specified in NCASI Atmospheric

Quality Improvement Technical

Bulletin Number 91. anu 1978

4
F~ ROLE/DECEMBER 20, 1996 AQ14S

Sulfuric Acid

Mist

1) Test methods 1 (LAC 33:HI:6ee1). 2

(LA:C 33 .IH:6oe3~ 3~

33:HI:6009), 4 tLAC 33iH:6613}. 6

(LAC 3J.IB:682Sh and a~

33.ffi:6&4S) (40 CPR pArt 60.

appendix A or tOO 8 ofCFB, Part 60 as

incoQ)Ql'8ted by reference M LAC

AUTHORITYNOTE: Promulgated accordance with R..S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality. Office

ofAir Quality and NuclearEnergy. Air Quality Division, LR 13:741 (December 1987). amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 18:374 (April

1992). LR

§lS11.. Continuous Emissions Monitoring

•••

[See PriorTatiD A]

B. These measurement systems shall be certified according to the performance

specifications in LAC 33:HI:618S (performance Specification 2) (40 CFR pan 60 appendix B as

incorporated by [ere! en" at LAC 33·m 3003) and quality assured by the procedures in 40 CFR

60, appendix "F".

••• . (See PriorTw in C]

AUTHORITY NOTE: Promulgated in accordance with RS. 30-.2054.

IDSTORICAL NOTE: Promulgated by the Department ofEnvironmentaJ Quality. Office

ofAir Quality and Radiation Protection, Air Quality Division, LR 18:375 (Apri11992). amended

LR

S
FrNAL RULE/DECEMBER 20, 1996

TIde 33

ENVIRONMENTAL QUALITY

Part m. Air

Chapter 11. Control orEmission orOrganic Compoundl

Subchapter A-Geaenl

§1103. Storage orVolatile Organic Compoundl

•••

AQ145

[See Prior Test la A-IU)

. L Test Methods 1-4 (LAC 33.BL6991, 6ge3, 6999 and 6913,

rcspeeti,ely4Q CFR part 60 IPpendix A 15 incm:pprated by reference llt LAC 33-m 3003) ror

determining flow rates, as necessaJy,

b. Test Method 18 (LAC 33.BL69714Q CFR part 60 IPpendix A. as

inco!]20rated by reference It LAC nm3OOJ) for measuring gaseous organic compound

emissions by gas chromatographic analysis;

c. Test Method 21 (LAC 33.m.69?14Q CFR part 60. appendix A. as

jncolJ)orated by reference at LAC JJ·m JQQJ) ror determination orvolatilc organic compound

leaks', d. Test Method 25 (LAC 33.m.69S54Q CFR part 60 Allpendjx A. IS

jnColJ)orated by reference at LAC JJ'm JQQ3) ror detcnnining total gaseous norunethanc organic emissi~as~~ .

•••

[See Prior Text in B.1.c-L5)

AUlHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department orEnvirorunental Quality, Office

orAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended,

LR 15:1061 (December 1989), amended by the Office orAir Quality and Radiation Protection,

Air Quality Division, LR 17:360 (April 1991), LR 18:1121 (October 1992), LR20:1376

(December 1994), LR 21:1223 (November 1995), repromulgated LR 21:1333 (December 1995),

amcndedLR

§2107. Volatile Organic Compounds- Loading

•••

[See Prior Text in A-E)

1. Test Methods 1-4 (LAC 33:m 6091 6003 6899 Aod 6113 icspCCtiydy4Q CfR

Ilart 60 appendix A. as jnco(poTated hy reference at LAC 3J·m 3003) ror determining flow rates,

as necessary;

2. Test Method 25 (LAC 33.m.6eS540 crn part 60 appendix A as jncolJ)oraled

by reference at LAC JJ'lU 300J) ror determining total gaseous norunethane organic emissions as

carbon.

•••

6
FrNAL RULE/DECEMBER 20, 1996 AQ145

[See Prior Ten in F]

AumORITYNOTE: Pronmlgated ill accordance with lLS. 30:205"4.

HISTORICAL NOTE: Promulgated by the Department ofEnviionrnental Quality, Office

ofAir Quality IIId NuclearEnergy, QualRy Division, LR.13:741 (December 1987), amended

LR. 16:116 (February 1990), amended by the Office ofAir Quality and Radiation Protection, LR.

17:360 (April 1991), LR. .

12101. Marine Vapor Recovery

•••

[See PriorTen in A-E.l.a]

i. Method 2B (40 CFR part 60 appendjx A 8$ inC0W9rated by

remenee at LAC nm3003) for combustion vapor processing systems (except flare stacks).

it Method 2A (40 CFR part 6Q appendjx A. as incorporated by

refelenee at LAC 33·m 3003) for an other vapor processing systems.'

b. for the determination oftotal organic compounds concentration at the

exhaust vent, Method 2SA or 25B (4Q CFR part 6Q appendjx!L as incorporated by reference at

LAC 33·m 3003). The calibration gas shall be either propane or butane.

•••

[See Prior Text in £.2]

3. Immediately prior to the performance test for determination ofcompliance, an

potential sources ofvapor leakage in the faci1ity'~ vapor collection system equipment shall be

monitored for Ieab using Method 21 (4Q CFR part 60 appendix A. as incorporated by reference

at LAC 33'1U 3003). The monitoring shall be conducted only while a ship or barge is being

loaded and should cover an parts oflhe vapor system, including tank hatches, that operate at

pressures above atmospheric pressure. All leaks shall be repaired prior to conducting the

performance test.

•••

[See Prior Text in E.4-4.g]

5. The owner or operator may adjust the emission results to exclude the methane

and ethane content ill the exhaust vent by the chromatographic methC':! shown in Method 25~

CFR part 6Q lwendix A as incorporated by reference at ',AC 3J'W 3003)

•••

[See Prior Text in F-H.2]

AUIlIORITY NOTE: Promulgated ill accordance with lLS. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 14:704 (October 1988), amended by

the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959 (November

1990), LR

§2109. OillWater-Separation

•••

[See Prior Text in A-q

7
FrNAL RULE/DECEMBER 20, 1996 AQ145

1. Test MethocM-4 (LA:C 33.m.6991, 6993, 6999 /Iud 6913, Itspeetivcly40 CFR

part 60 aPPendix A. as jnccitporated by metence at LAC :n'm 3003) for dctcnnining tlow rates,

u necessary;

2. Test Method 18 Q;;h€33.HL697140 CFR Par160 appendix A. as incorPorated

by reference at LAC um3003) for measuring gaseous organic compound emissions by &IS

chromatosraPhic analysis;

3. Test Method 21 (LM; 33.HL69mO CFR part 60 apPenA;v A as incOJ:porated

by reference at LAC 33·m 3003) for determination ofvo1atile or&~",;.: cor. :,~ ..nd lcaIcs;

• 4. Test Method 25 (LA:C 33.HL69SS40 CFR part 60 allP ,djx A as incorporated

by reference at LAC 33·m 3003) for determining total gaseous nonmetha:.e organic emissions as

carbon;

•••

[See Prior Text la <:.5-D.3]

AUIHORlTY NOTE: Promulgated in accordance with R.S. 30:2054.

lnSTORICAL NOTE: Promulgated by the Department ofEnvironmcntal Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

LR 16:117 (Fe~ruary 1990), amended by the Office ofAir Quality and Radiation Protection, Air

Quality Division, LR 16:959 (November 1990), LR 17:360 (Apri11991), LR 18:1122 (October

1992), LR

§211S. Waste Gas Disposal

Any wute gas disposal stream containing organic compounds from any emission source

including those emissions from process unit upsets, start-ups and shutdowns shall be controlled by

one ofthe following methods:

•••

[See Prior Text in A-I]

1. Test Methods 1-4 (LAC 33.m.6991, 6993, 6999, aud 6913, Itspcctive1)~

CPR part 60 appendix A. as incorporated by reference at J,AC 33'm 3003) for determining tlow

rates, as IIcccssary;

2. Test Method 18 (LAC 33.m.697140 CFR part 60 apPendix A as jncorporated

by reference at J,AC 33·m 3003) for determining gaseous organic compounds emissions by gas

chromatography; ,

3. Test Method 25 (LAC 33.m.69SS40 CFR part 60 apPendix A as incorporated

by reference at LAC 33·m 3003) for determining total gaseous nonmethane organic emissions as

carbon;

4. Test Method 25A or 25B (LAC 33 .m.6986 01 668740 CPR part 60 appendix

A. as incorporated by reference at LAC 33·m 3003) for detennining total gaseous orgailic .

concentration usingtlame ionization or nondispersive infrared analysis; and

•• •

[See Prior Text in L5-L]

AUIHORlTY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmentaJ Quality, Office

8
FrNAL RULE/DECEMBER 20, 1996 AQ145

•

., ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959

(November 1990), LR 17:654 (July 1991), LR 18:1122 (October 1992), LR 19:317 (March

1993),LR .

§1116. Glycol Debydraton

•••

[See Prior Text ia A-D.3]

4. conventional stack measurements using Lz\€33.HI.•68'i'1 and 6885 ~ethods

18 and 2S (40 CFR part 60 appendix A. as incorporated by reference at LAC nill 3003) for

determining volatDe organic compound emissions; or

•••

[See Prior Text ia D.5-G.2]

AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office .

ofAir Quality and Radiation Protection, Air Quality Division, LR 20:1106 (October 1994),

repromulgated LR 20: 1279 (November 1994), amended LR 21 :941 (September 1995), LR

§1111. Fugitive Emission Control

•••

[See Prior Text in A-B)

1. No component shall be allowed to leak organic compounds exceeding 10,000

parts per million by volume (ppmv), as defined in LAC 33:m.ll1, when tested by Method 21

"Determination ofVolatile Organic Compound Leaks" in the Division's SOUl ee Test Manual

('LIte, 'folume 12!)40 CFR part 60 apPendix A. as incorporated by reference at LAC nill 3003.

Any regulated component observed leaking by sight, sound, or smell must be repaired according

to Lz\€33.HI.2!I2!1.Subsection B.3 ofthjs Section. regardless ofthe leak's concentration. This

includes flange and coMection leaks found per LAC 33.Hl:2!I2!l.Subsection C.3.b ofthis Section.

pump and compressor seal leaks found during the weekly visual inspections, and other regulated

component found leaking.

•••

[See Prior Text in B.2-G]

AUTIiORITY NOTE: Promulgated in accordance with R.S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959

(November 1990), LR 17:654 (July 1991), LR 21:1330 (December 1995), LR

§2122. Fugitive Emission Control for Ozone Nonattainment Areas

•••

[See Prior Text in A-A.6.d)

B. Definitions. Terms in this Section are used as defined in LAC 33 :III.lll with the

9
FXNAL ROLE/oECEHBER 20, 1996

Cltccption ofthose terms speci1ic:aUy defined below as foDows:

•••

AQ145

[See Prior Test]

GoodPerjorlnanuLneI-atJ. operating level reached when no more than 2.0

... pa-c:ent oca component in YOCaervic:e in • process unit are leaking at the leak rate !fetinition or

greater as determined byLAC 33.BL6811 (RefbdICe Method 21, "Determination ofVolatiJe

Organic Compound Leaks" (40 CFR Plrt 60 l])Jlendix!L IS incon'QrJted by reference at LAC

n m 3003).

••• • [See PriorTest In B.Bea"YlJquid Service - C.l]

L No component in petroleum refineries, SOCMJ. MTBE, and polymer

manuflu:turing industry sbaJl be allowed to leak volatile organic compounds CltCeed:ng an

instrument readin..l2f 1,0005~~for valves, connectors, pressure relief devices,

process drains, ~;rV81Yes and :=5,000 ppmv for pumps and compressors; or

10,000 ppmv foiagitators In Su on D ofthis Section, when tested by I::JIte

33.m.6811 ~ethod 21 (40 CFR part 60 apPendix!L IS ineon'Qrated In' reference at I A.C

n m3OO3).

b. No component in natural gas processing plants shall be allowed to

leak volatiJe organic compounds Cltc:eeding an instrument reading offof2,500 ppmv for valves,

connectors, pressure relief devices, process drains, and open-ended valves and lines; 5,000 ppmv

for pumps and compressors; or 10,000 ppmv for agi~ors as outlined in Subsection D ofthis

Section, when tested by LAC 33.m.6811 (Method 21 (40 CFR part 60, appendix A as

incorporated by reference at LAC nm3OOJ).

•••

[See Prior Test in C.l.c-G.Ii]

AUlHORITY NOTE: Promulgated in accordance with ll.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmentaJ Quality, Office

ofAir Quality and Radiation Protection, Air Quality !:'ivision, LR 20:1102 (October 1994),

repromulgated LR 20:1279 (November 1994), amended LR

Subchapter B-Organic Solvents

§2113. Organic Solvents

•••

[See PriorTest in A-E)

1. Test Method 24 (LAC 33.1H.668340 CFR part 60 appendjx A as incorporated

by reference at LAC JJ,m JOOJ) with a one-hour bake;

. 2. Test Method 1-4 (LAC 33.m.688l, 6663, 6669 and 6813, rCSpCCbYeIy£)..cEB.

part 60 appendix!L as incon'orated by reference at LAC umJOOJ) for determining flow rates;

3. Test Method 18 ( (LAC 33,m,66714Q CFR part 60 appendix!L as

incorporated by reference at LAC JHiI J003) for measuring gaseous organic compound

emissions by gas chromatographic analysis; .

4. Test Method 25 (LA€ 33.HI.66854Q CFR part 60 appendix A. as jncorporated

10
FrNAL RULE/DECEMBER 20, 1996 AQ145

by reference al LAC 33·m 3oo:t) for detennining total ~us nonmethane organic emissions as carbon; . •

••• . [See Prior Text ia E.5-F.4] - .

AtrrHORlTY NOTE: Pronwlgated in accordance with R.S. 30:2054.

lUSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

orAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

LR 16:119 (February 1990). amended by the Office orAir Quality and Radiation Protection, Air

Quality DiVision, LR 17:654 (July 1991). LR 18:1122 (October 1992). LR 22:340 (May 1996),

L1l

Subchapter e-VaporDegreasen

§2115. Vapor Degreasen

•••

[See Prior Text ia A-E)

1. A5l1d Test Method D323-82 ror detennining Reid vapor pressure;

2. Test Methods 1-4 (LA€33.fH.6661, 6663, 6669 and 661340 CfR part 60

appendix A. as inCO[porated by reference at LAC 33·m 3003) for detennining flow rates;

3. Test Method 18 (LA€33.fH.667140 CFR part 60 apPendix A as incorporated

by reference at LAC 33·m 3003) for detennining gaseous organic compound emissions by gas

chromatography;

4. Test Method 25 (LA€33.fH.66S540 CfR part 60 .apPendjx A. as incorporated

by reference at LAC 33·m 3003) for detennining total gaseous nonmethane organic emissions as

carbon.

•••

[See Prior Text in F-G]

AtrrHORlTY NOTE: Promulgated in accordance with R.S. 30:2054.

lUSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959

(November 1990), LR 18:1122 (October 1992), LR

Subchapter E-Percbloroetbylene Dry Cleaning Systems

§2129. Percbloroethylene Dry Cleaning Systems

•••

[See Prior Text in A~q . 1. Test Methods 1-4 (LAC 33.fH.6661, 6663, 6669 and 6613, iCSPCCtively1Q.

CPR part 60 appendix A. as incorporated by reference at LAC nm 3003) for determining flow

rates, as necessary;

2. Test Method 18 (LAC 33.ffi.667140 CfR part 60 appendix A as incorporated

by reference at LAC 33·m 3003) for measuring gaseous organic compound emissions by gas

chromatographic analysis;

11
FINAL RULE/DECEMBER 20, 1996 AQ145

3. Test Method 21 (LA€33.Hi:697740 CFR part 60 appendjx A as jnCOO!0rated

by refel e,,'r at LAC nm30(3) for determination ofvo1atile organic compoundsleaks;

4. Test Method 2S (LA€33.Hi:698S40 CFR part 60 appendix A. as inCOO!orated

by reference at LAC 33·m 30(3) for determining total gaseous nonmethane organic emissions as

carbon;

•••

[See Prior Test In c.5-D.3]

AUlHORITY NOTE: Promulgated in acc:ordance with RS. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959

(November 1990), LR

Subchapter F-Gasoline Handling

12131. Filling or Gasoline Storage Vessels

•••

[See Prior Test In A-E]

1. Test Method 27 (LAC 33.HI.698940 CFR Part 60 appendjx A as jncm:pprated

by reference at LAC 33"1II 3003) for detennination of~por 'ftightness of6&uoline Bdelivery

lftanlcs eusing PIl~um lftesl.

•••

[See Prior Test in E.2]

3. Test Method 21 (LA€33.Hi:69'i'740 em part 60 appendjx A as jncorpprated

by reference at LAC 33·m 30(3) for determination of~olatile 6prganic ~mpound f:leaks.

•••

[See Prior Test in F-G]

AUTHORITY NOTE: Promulgated.in accordance with RS. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

LR 16:609 (July 1990), amended by the Office ofAir Quality and Radiation Protection, Air

Quality Division, LR 17:654 (July 1991), LR 18:1122 (October 1992), LR 19:1564 (December

1993), LR

§2133. Gasoline Bulk Plants

•••

(See Prior Text in A-D.l]

2. Test Method 21 (I::AC 33.HI.6B'i''i'40 CFR part 60 appendlx"A; as jncQl;p6ra.ted

by reference at LAC 33·m 3003) for determination of~olati1e 6prganic €kompoundf:leaks;

•••

(See Prior Text in D.3-F]

AUTHORlTY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

12
FINAL RULE/DECEMBER 20, 1996 AQ145

ofAjr Qua1ity and Nuclear Energy, Ajr Quality Division, LR 13:741 (December 1987), amended,

LR 16:610 (July 1990), amended by the Office ofAjr Quality and Radiation Protection, Ajr

Quality Division, LR 21:SS2 (June 1995). LR

11135. Bulk Guoline Terminals

•••

[See Prior Test iD A-D)

1. Test Methoda 1-4 (LAe 33.Hl:6981, 6883, 6889 aud 6813,lespeeti.e!)!ll

CFR part j;o awendjx A as incorporated by reference at I e\C J3'm 3003) for determining flow

rates. u necessary;

2. Test Method 18 (LAe 33.Hl:69"f4Q CFR part 60 IPJ)CI!d"1X A M inGQTJl0rated

by reference at LAC ~:l·m 3003) for measuring gaseous organic compound emissions by gas

chromatographic analysis;

3. Test Method 21 (LAe 33.1H:69"'i'40 CFR part 60 apPendjx A as inGQTJlorated

by reference at LAC 33·m 3003) for determination ofvolatile organic compound leaks;

4. Test Method 25 (LA<: 33.m.69S540 CFR part 60 appendjx A as incorporated

by reference at LAC 33·m 3003) for determining total gaseous nonmethane organic emissions as

carbon;

•••

[See Prior Text in D.5-E.5.c)

AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the DePartment ofEnvironmental Quality, Office

ofAjr Quality and Nuclear Energy, J.Jr Quality Division, LR 13:741 (December 1987), amended

LR 16:609 (July 1990), amended by the Office ofAjr Quality and Radiation Protection, Ajr

Quality Division, LR 17:654 (July 1991), LR 18:1123 (October 1992), LR

§2137. Gasoline Terminal Vapor-Tight Control Procedure

A Gasoline Tank Trucks

1. Testing Procedure. Gasoline tank trucks and their vapor collection systems

shall not sustain a pressure change ofmore than three inches ofwater (0.75 \cPa) in five minutes

when pressurized to 18 inches ofwater (4.5 Kpa) or evacuated to six inches ofwater (1.5 Kpa)

using the test ploceduiC dCSCiibed it•.Im.Method 27 ofd" D;;isiou's SOUlee Test !wfailU~

CPR Part 60 lijlPendix A as incQrporated by reference at LAC 33"1U 3003) fQr detenninatjQn Qf

vapor tightness QfBaSQUne deliyery tanks usjnB pressure-vacuum test.

•••

13
FINAL RULE/DECEMBER 20, 1996

detmnjDntion peyo1att1, Qrpnic; compoynd 1eikS oftit, c10CWUUlt Ieraeileed in U£. 33:H1:2131.Al. • .

•••

~145

[See PriorTest III B.2-D]

.. . . AurHORlTY NOTE: Promulgated in accordance with ll.S. 30:2054.

lfiSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR. 13:741 (December 1987), amended

LllI6:609 (July 1990), amended by the Office ofAir Quality and Radiation Protection, Air

Quality Droaoll, LR.

SubchapterB-Gnphic Arts

11143. Gnphic Arb (PrIndn&) by Roto&nvuft and F1exo&nphic Processes

•••

[See PriorText ill A.q

1. Test Method 24 (fA.C 33.HL66834Q CFR part 60 appendjx A as jncQlJlorateci

by reference at LAC 33·m 3003) for determination ofvolatile matter content, water content, .

density volume solids and weight ofsolidS;

2. Test Methods 1-4 (LAC 33.m.GSSI, 6SS3, 6SS9 and 691340 CPR part 60

appendjx A. as jncolJlorated by reference at LAC nm3003) for determining flow rates;

3. Test Method 25 (LA€33.HL6S8540 CFR part 60 appendix A as jncolJlorated

by reference at LAC 33·m 3003) for detennining total gaseous nonmethane organic emissions as

carbon; and '

•••

(See Prior Text in C.4-D.3]

AurHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmenta1 Quality, Office

of Air Quality and Nuclear Energy, Air Quality Division, LR. 13:741 (December 1987), amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR. 16:959

(November 1990), LR. 18:1123 (October 1992), LR.

Subchapter ~PharmaceudcalManufacturing FacUities

§1145. Pharmaceutical Manufacturing FacUities

•••

[See Prior Text in A-F.1]

2. Test Methods 1-4 (LA€33.m.GSSI, 6SS3, 6999 mid 691340 CFR part 60

appendjx A. as jncolJlorated by reference at LAC nm3003) for df~ermining flow rates;

3. 'TeSt Method 18 (LAC 33.ffi.6S7140 CFR part 60 appendix A. as jncorporated

by reference at LAC 33"IU 3003) for determining gaseous organic compound emissions by gas

chromatography;

4. Test Method 24 (LAC 33.m.688540 CFR part 60 appendix A as jncolJlorated

by reference at LAC 33·m 3003) for determining total gaseous nonmethane organic emissions as

carbon.

14
FrNAL RULE/DECEMBER 20, 1996 AQ145

•••

(See PriorTat ill G-G.41

AUIHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality.Oflice

ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended

by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959

(Novanber 1990).

SubchapterI. LimitinC Volatile Orpnic Compound (VOC) Emissions from Reactor

Processes and Distillation Operations ill the Synthetic Orcanic Chemical ManufacturiDc

IDdumy (SOCMI)

§2147. LimitinC VOC Emissions from SOCMI Reactor Processes and Distillation

Operations

•••

(See Prior Text ill A]

B. Definitions. Unless specifically defined in LAC 33:m.lll, the tenns in this

Subchapter shall have the meanings commonly used in the field ofair pollution control.

Additiona1ly, the following meanings apply, unless the context clearly indicates otherwise.

•••

(See PriorText]

Halogenated Vent Stream-any vent stream containing a total concentration of

halogen atoms (by volume) contained in halogenated organic compounds of2oo ppm by volume

or greater determined by using LAC 33.1H.58?! (Method 18 (40 CFB part 60 IIppendix A IS

jncorporated by reference at LAC 33·m 3003) or other test or validated data by the United States

Environmental Protection Agency's (EPA) Method 301 of40 CFR part 63, appendix A, or by

engineering assessment or process knowledge that no halogenated organic compounds are

present. For example, 150 ppm by volume ofethylene dichloride would contain 300 ppm by

volume oftotal halogen atoms.

•••

(See Prior Text]

Total Organic Compounds (7OC)-those compounds measured according to the

procedures ofLAC 33.1H.58?! (Method 18 (40 CFR Pllrt 60 IIppendix A IS jncorpoCl!ted by

reference It LAC 33·m 3003), for the purpose ofmeasuring molar composition as required in

Subsection D.5.b ofthis Section, hourly emission rate as required in Subsection D.2 and 5.d of

this Section, and TOC concentration as required in Subsection F.l.d and 2 ofthis Section. The

definition ofTOC excludes those compounds that the-administrative authority· designates as

having negligible photochemical reactivity as listed in 40 CFR 51.100(5).

•••

(See Prior Text]

C. Control Requirements

•••

(See Prior Text in C.I-D.3]

15
FrNAL RULE/DECEMBER 20, 1996 AQ145

basis, ppm by volume.

L LAC 33.&6991 ~ethod 1 (40 CFR part 60 appendjx A as

iDcOl;porated bY reference at LAC um 3003) or LAC 33.&6992 (Method lA (40 em pan 60

appendix A. U inCOQlOTllted bY reference at LAC um3003), as appropriate, shaD be used for

selection ofthe sampling sites. The control device inlet sampling site for determination ofvent

stream molar composition or TOC (less methane and ethane) reduction efficiency_shaD be located

after the last RJ:,Overy device but prior to the inlet ofthe control device, prior to any dilution of

the process ventstream. and prior to release to the atmosphere.

b. LA€33.&6993 ~ethod 2 (40 CFR Part 60 appendix A as

iDCO!Jl0rated by reference at LAC 33·m 3003), LAC 33.&6995 ~ethod 2A (40 CfR part 60

appendix A. as iDCO[pOrated by reference at LAC 33·m 3003), LAC 33.m.6996 ~ethod 2C~

CFR part 60 appendix A as iDcotPPTated bY weren!.'t at LAC urn 3003), or LAC 33.Hl:6998

(Method 2D (40 CfR part 60 appendix A. as inco!J)Ojated bY reference at I,AC 33·m 3003), as

appropriate, shaD be used for determination ofthe gas stream volumetric flow rate.

. c. The emission rate correction factor, integrated sampling and analysis

procedure ofLAC 33.&6989 ~ethod 3 (40 CFR part 60 appendix A. as ;nco!J)0rated by

reference at LAC 33·m 3003) shaD be used to determine the oxygen concentration (''100U> for the

purpose ofdetermining compliance with the 20 ppm by volume limit. The sampling site sba11 be

the same as that for the TOC samples, and samples shaD be taken during the same time that the

TOC samples are taken. The TOC concentration corrected to three percent oxygen (C.) sba1l be

computed using the following equation:

C = C % 17.9

roc 20.9 - % 0211

where:

C. = Concentration ofTOC (minus methane and ethane) corrected

to three percent dry basis, ppm by volume.

Croc = Concentration ofTOC (minus methane and ethane), dry

% .. Concentration ofoxygen. dry basis, percent by volum!".

d. LAC 33.m.69'T1 ~ethod 18 (40 CfR part 60 appendix A U

iDc0!Jl0rated by reference at LAC 33·m 3003) shall be used to determine the concentration of

TOC (minus methane and ethane) at the outlet ofthe control device when determining compliance

with the 20 ppm by volume limit, or at both the control device inlet and outlet when the reduction

efficiency ofthe control device is to be determined.

••• , [See Prior Text in D.3;d;1-D.S] .,".•"., .,. .._.- -"_.

a. LA€33.m.6991 ~ethod 1 (40 CFR Part 60 appendjx A as

incorporated by reference at I,AC nm 3003) or LAC 33.m.6992 (Method lA (40 CFR part 60

appendix A. as ;nc0!J)oTated by reference at LAC 33·m 3003), as appropriate, shall be used for

selection ofthe sampling site.

•••

16
FLNAL RULE/DECEMBER 20, 1996 AQ145

(See Prior Text in"D.5.a.i-D.5.Lii]

(a). the iampling site for the vent stream flow rate and

molar composition sbIl1 be prior to the final recovery device and prior to the point at which any

nomeactor or nondistil1ation stream.or stream from a nonaft'ected reactor or cfistjl1ation UJlit is .

introduced. Method 18 (fJrC 33.lH:D9T}40 CFB Part 60 l,PJIendix A as incoeporated by

refecllce at LAC 33·m 3QQ3) shall be used to measure organic compound concentrations at this

site;

(b). the efficiency ofthe final recovery device is determined

by measuring the organic compound concentrations using Ute 33.m.D9T} (Method 18 (40 CFR

Part 60 appendix A as incm:porated by reference at LAC 33·m 3QQ3) at the inlet to the final

recovery device after the introduction ofaD vent streams and at the outlet ofthe final recovery

device;

•••

(See Prior Text in D.5.a.ii.(c)-D.5.b]

i. LAC 33.lH:D911 (Method 18 (40 CFB part 60 appendix A. as

incoeporated by reference at LAC urn 3003) shaD be used to measure the concentration of

organic compounds including those containing halogens.

•••

(See Prior Text in D.S.b.ii]

iii. LAC 33.m.DeB (Method 4 (40 CFR part 60 appendix A as

incorporated by reference at LAC 33·m 3003) shall be used to measure the content ofwater

vapor.

c. The volumetric flow rate shaD be determined using Ute 33.HI.6ge3

(Method 2~, Ute 33.m.6995 (Method 2A~. Ute 33.m.DeeD (Method 2q or LAC 33.m.6eeS

(Method pf40 CFR part 60 appendix A. as incorporated by reference at LAC urn 3003.

as appropriate.

d. The emission rate ofTOC (minus methane and ethane) <Eroc> in the

vent stream shaD be calodated using the following equation:

where:

Eroc: = Emission rate ofTOC (minus methane and ethane) in the

sample, kilograms per hour.

Kz =Constant, 2.494 x 10-6 (liters per ppm) x (gram-moles per.

standard cubic meter [scm]) (kilograms per gram) (minutes per hour). where standard

temperature for (gram-mole per scm) x (gram-mole per scm) is 20°C.

CJ = Concentration ofsample component "j", on a dry basis, in ppm

as measured by LAC 33.HI.6eTi (Method 18 (40 CFR part 60 appendix A. as incorporated by

reference at LAC 33·m 3003), as indicated in Subsection D.3.d ofthis Section.

Mj = Molecular weight ofsample component "j", grams per gram17
FrNAL ROLE/DECEMBER 20, 1996

mole.

AQ145.

Q." Vent stream flow rate (scm pee minute) at a temperature of

20·C, on adJy basis.

e. The total process vent stream concentration (by volume) ofcompounds

.cont:'.ining halogens (ppm by.volume, by compound) shaD be summed from the individual

concentrations ofcompounds containing halogens which were measured by : ...0 33.5.6611

tMethod 18 (40 CFR plll16Q Ippendjx A. IS inCOQlOT!lted byrefercnce ItI. ~r. 33-m 3003).

£ The net heating value ofthe vent stream shall be calculated using the

equation:

where:

Hr" net heating value ofthe sample (megajoules pee standard

cubic meter), where the net enthalpy per mole ofvent stream is based on combustion at 2S·C and

760 mi11imeters ofmercwy, but the standard temperature for determining the volume

corresponding to one mole is 20·C, as in the definition ofQ. (vent stream flow rate).

KJ = Constant, 1.740 x ur7 (ppm)"J (gram-mole per standard cubic

meter), (megajoules per kilocalorie). where standard temperature for (gram-mole per standard

cubic meter) is 20·C.

B...Water vapor content ofthe vent stream, proportion by

volume; except that ifthe vent stream passes through a fina\ stream jet and is not condensed. it

shal1 be assumed that B... 0.023 in order to correct 2.3 percent moisture.

CJ= Concentration on a dry basis ofsample compon~ 'It "j" in parts

per million, as measured for all organic compounds by LAC 33.HI.6611 (Method It (40 CFB.

part 60 IpPendix A as jnco[JlQrate4 by reference at LAC 33-m 3003) and measured for

hydrogen and carbon monoxide by ASTM DI946-77.

II;. .. Net heat ofcombustion ofsample component"l. kilocalories

per gram-mole, based on combustion at 2S·C and 760 mi11imeters ofmercury. The heats of

combustion ofvent stream components shal1 be determined using ASTM D2382-76 ifpublished

values are not available or cannot be calculated.

000

[See Prior Text in D.6-D.9.a]

b. LAC 33.HI.6611 (Method 18 (40 CPR part 60 appendix A. as

.jncorporated by reference at LAC 33·m 3003) orLA:C 33.HI.66S6 (Method 2SA (40 CER part

60 appendix A. as incol7"?rated by refe-ence at LAC J3"m 3003) shall be used to measure

concentration; alternativelY. any other method or data that has been validated according to the

protocol in EPA Method 301 of40 CFR part 63. appendix A may be used.

c. Where LAC 33.HI.66i'1 (Method 18 (40 CER part 60 appendix A. as

incorporated by reference at LAC 33"III 3003) is used. the following procedures shall be used to

18
FrNAL RULE/DECEMBER 20, 1996

calculate parts per million by volume concentration.

•••

AQ145

[See Prior Test in D.9.c.i]

.it The concentration of.TOC.(minus methane and ethane) shaD be

cal",lated using UR: 33.HL6811 {Method 18 (40 CFR Part 60 appcodix A as inco[JlQrated by

reference at LAC nm3003) according to Subsection D.3.d ofthis Section.

d. Where UC 33£6686 {Method 2SA (40 CFR part 60 appendjx A A!!

ineotJlorated by reference at LAC 33·m 3003) is used, the fonowing procedures shaD be used to

calculate pirts per million by volume TOC concentration.

Lf:jdJ 33.HL6686 {Method 2SA (40 CFR part 60 appcodix A !l$

jnem:pnratl!!! by reference at LAC 33·m 3003) shaD be used only ifa single VOC is greater than

50 percent oftotal Voc. by volume, in the process vent stream.

•••

[See Prior Text iDD.9.d.ii]

iii. The VOC used as the calibration gas forUR: 33.HL68S6

(Method 25A (40 CFR part 60 appendix A as incOJ:porated by reference at LAC J30m 3003)

sball be the single VOC present at greater than 50 percent ofthe total VOC by volume.

iv. The span value for LA€33.m.6eS6 (Method 25A (40 CFR

part 60 aJlJlendjx A as inco[Jlorated by reference at LAC J30m 3003) shaD be 50 ppm by

volume.

v. Use ofLAC 33.m.68S6 {Method 25A (4Q CFR part 60

apPendjx A aSinCO[JlOTated by reference at LAC 33·m 3003) is acceptable ifthe response from

the high level calibration gas is at least 20 tim..-s the standard deviation ofthe response from the

zero cah'bration gas when the instnunent is zeroed on the most sensitive scale.

•••

[See Prior Text in D.9.vi]

e.The owner or operator shaD demonstrate that the concentration ofTOe

including methane and ethane measured by UR: 33.HL6eS6 {Method 25A (4Q CFR part 60

appendjx A !l$ jnco[JlOTated by reference at I.AC nm3003) is below 250 ppm by volume with

VOC concentration below 500 ppm by volume to qualifY for the low concentration exclusion.

•••

[See Prior Text in E-F.4]

AUTHORIlY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Radiation Protection, Air Quality Division, LR 21:380 (April 1995), amended

LR ' '. . . .,

Subchapter K. Limiting Volatile Organic Compound Emissions from Batch Processing

§2149. Limiting Volatile Organic Compound Emissions from Batch Processing

•••

(See Prior Text in A-E.2]

a. LAC 33.m.Geel (Method I) or 6ee2 (Method IA in 40 ern part 60

19
FXNAL RULE/DECEMBER 20, 1996 AQ14S

appendjx A. as inCOlllorated by reference at LAC nm3003}, as appropriate, shall be used for

selection ofthe sampling sites ifthe flow rate measuring device is a rotameter. No traverse is

necesSlry when the flow measuring device is an ultrasonic probe. The control device inlet

sampling siteI for determination ofvent stream VOC composition reduction efficiency shall be

prior to the control device and after the control device.. " . _. .. _ _ ..

b. LAC 33:H1:6e63 (Method 2~, 6665 (Method 2A~, 6666 (Method 2q

or 6El6S (Method 2D} in 40 CFR part 60 aPJlendix A ::s jnCOlllorated by reference at LAC

33·m 3003 as appropriate, shaI1 be used for determination ofgas stream volumetric flow rate.

Flow rate should be made continuously.

Co Ute 33.1H:6686 (Method 25A~ or 66'71 (Method 18~ in 40 CFR part

60 IPJlCDdix A. U jncgmorated by reference at LAC 33·m 3003 ifapplicable, shall be used to

determine the concentration ofVOC in the control device inlet and outlet.

i. The sampling time for each run will be the entire length ofthe

batch cycle in which readings will be talcen continuously ifUtC 33.1H:66S6 (Method 25A.,££l .

CFR part 60 appeodix A as incp[p0rated by rer.,elICC at LAC 33·m 3003) is used or as often as

is possible using LAC 33.1H:66'71 (Method 18 (40 CFR part 60 I12Peodix A as incpQ20Tlted by

reference at LAC 33'm 3003), with a maximum ofone-minute intervals between measurements

throughout the batch cycle.

•••

[See Prior Text in E.2.c.ii-G.1.c.v]

A~ORITY NOTE: Promulgated in accordance with R.S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Radiation Protection, Air Quality Division, LR 21:387 (April 1995), amended

LR

§1153. limiting Volatile Organic Compound Emissions From Industrial Wastewater

•••

[See Prior Text in A-E)

1. for determination ofgas flow rate- Test Methods 1-4 (LA€33.ffi.6661=

661340 CFR part 60 appendix A as incQCPprated by reference at LAC nm3003);

2. for determination ofgaseous organic compound emissions by gas

chromatography - Test Method 18 (LAC 33.ffi.66'7140 CFR part 60 apPendix A as

inco[poTlted by reference at I,AC nm3003);

3. for determination ofVOC leaks and for monitoring a carbon canister in

accordance with Subsection D.3 ofthis Section - Test Method 21 (LAC 33.ffi.66'7'740 CFR part

60 appendix A. as inco[porated by reference at I,AC nm3003);

4. for determination·oftotal gaseous nonmethane organic ernisslonsas carbonTest Method 25 (LAC 33.ffi.66S540 CFR part 60 appendix A as jncorporated by reference at

LAC nm 3003);

5. for determination oftotal gaseous organic concentration using a flame

ionization or a nondispersive infrared analyzer - Test Method 25A or 25B (LAC 33.ffi.6eS6 0,

6e&'i'40 CFR part 60 appendjx A as incorporated by reference at LAC 3HU 3003);

10
FrNAL RULE/DECEMBER 20, 1996

•••

AQ145

-....-:. '::"

[See PriorTest ID E.6-I)

AUTIiOlUTY NOTE: Promulgated in accordance with R.S. 30:2054.

.. HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality. Office

ofAir Quality and Radiation Protection, Air Quality Division, LR 21:936 (September 1995)•..

amendedLR

[Editor'. Note: Subchapter N below will contaID aD text currently located ID Subchapter A

ofChapter 6L The aectiODl will be renumbered u .boWJl below.] •

Subcbapter N. Method 43-Capture Efl'ic:iency Test Procedures

Old SectionINew SectiQa

6121J2155

6123/1156

611S11151

6117/1158

6119/1159

6131/1160

21
FrNAL RULE/DECEMBER 20, 1996 AQ145

..•..-. :-...

Tide 33

ENVIRONMENTAL QUALITY

partmAir

Chapter 2S. Miscel1aDeoUllDciDentioD Rules

SubcbapterB. BiomedlcllWute IDdaenton

• 12511. Studardl olPerf'ol'llUUlce lor Biomedical Wute IDdnenton

•••

d. Method 26 - Determination ofHydrogen Chloride Emissions from'

StatiollllJY Sources(LAC 33.1H:69BB40 CFR part 60 appendix A as jnco[porated by reference at

LAC nm3003); and/or

[See Prior Test Ia A-E.')

L Method 5 • Determination ofParticulate Emissions from Stati01lllJY

Sources (LAC 33.1H:69iS40 CFR part 60 appendix A as jncm:porated by reference at LAC

33·m3003);

b. Method 6 - Determination ofSulfur Dioxide Emissions from

StatiollllJY Sources (LAC 33.1H:682S40 CFR part 60 appendix A as jncm:porated by reference at

LAC 33·m 3003);

c. Method 7 • Determination ofNitrogen Oxide Emissions from

StatiollllJY Sources (LA€33.lH.693340 CFR part 60 appendix A as jncomorated by reference at

I AC nw3003));

•••

[See Prior Test in E.6.e-L]

AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Qua1ity, Office

ofAir Quality and Radiation Protection. Air Qua1ity Division. LR 20:1098 (October 1994),

amended LR 21:1081 (October 1995), LR

Subchapter C. Reluse IDcineraton

11511. Reluse IDcineraton

•••

."~ ..

[See Prior Text in A-D]

E. Allowable Emissions from Incinerator. The amount ofparticulate matter (PM.'>

emiiteobY a refuse incinerator shall be deterinined using the test methods from 40 CFRpart 60,

appendix A, as jnco[porated by referen;e at LAC nm 3003: Method 5 - Determination of

Particulate Emissions from Stationary Sources (LAC 33.lH.691540 CPR part 60 appendix A. as

;nCQ[porated by reference at LAC nID 3003).

•••

[See Prior Text in F-F.9]

22
FINAL ROLE/DECEMBER 20, 1996 AQ145

L Method S - Determination ofParticulate_Enu~ons from Stationary

Soun:ea (LAoS 33.1H:681S40 CFR part 60 appendix A as incOI:poraied by reference at LAC

33·m3003);

- b. -Method 6- Determination ofSulfur Dioxide Emissions from

Stationary Sources (LA:e 33.1H:682S40 CFR part 60 appendjx A as incQI:porated by reference at

LAC 33·m 3003);

c. Method 7 • Determination ofN'rtrogen Oxide Emissions from

Stationary Sources (LA:S 33.1H:683340 CFR part 60 appendix A as incQOIQRtc<! by reference at

LAC J30m'JOOJ);

d. Method 26 • Determination ofHydrogen ChlorideEmissions from

Stationary Sources (LAoS 33.1H:68884Q CFR part 60 DWCOdjx A as incQI:poratc<! by reference at

LAC 33·m3003); and/or

•••

[See-Prior Text in F.9.e-H]

AurHORITY NOTE: Promulgated in accordance with R. S. 30:2054.

HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Radiation Protection, Air Quality Division, LR 20:1100 (October 1994),

amendedLR

Subchapter D. Crematories

§2531. Standards of Performance for Crematories • •••

[See Prior Text in A - K.l)

L LAS 33.m.681S (Method S - Determination of Particulate Emissions

from Stationary Sources (40 CFB. part 60 apPendix A as incoIj)Qrated by reference at LAC

33·m 3OO3);

b. Method )0 - DetenDination Qf CarbQn Monoxide Emissions from

StatjOQluy Sources (40 CFR JW1.60 apPendix A as incQIj)oRtc<! by reference at LAC

33·m 30(3) (Method 18 • Dctuuaiuatioll of C1uboil ftfOilOxidc Ennssiolis BOlli S~tjonar)

Sowecs},

c. L!£ 33.m.6e41 (Method 9· Visual Determination ofthe Opacity of

Emissions from Stationary Sources (40 CFR Part 60 appendix A as inooIj)oratc<! by reference at

LAC nID3003); and

•••

[See Prior Text in K.l.d-K.2)

AurHORITY NOTE: -Promulgated in accordance with R.S. 30:2054.--

mSTORICAL NOTE: Promulgated bythe Department ofEnvironmental Quality, Office

ofAir Quality and Radiation Protection, Air Quality Division, LR 20: 1107 (October 1994),

amendedLR

23
FXNAL RULE/DECEMBER 20, 1996

TIde 33

ENVIRONMENTAL QUALITY

PartID.Air

Chapter2'. Odor ReguladoDi

12901. OdoroUi Substances

•••

AQ145

(See PriorText in A-F.I]

• 2. An samples shall be eveJUBted u soon after collection u possible in accordance

with the procedures set forth in tie Bi.ision's SOW" Test Manual f.U£, 'lvluillC 11)Sybsest;iQD

G gftbjs Section

EDITOR'S NOTE: fIbe foDowing tut b81 been moved in its entirety from LAC

33:ID.60" la Chapter 60 and renumbered 81 Subsection G below.]

a. Method 41. Odor Test Methods

*- 1. Butanol OdorEvaluation Procedure

+ .. Sampling and Storage. Odorous gas sampling is no more than typical

integrated bag samjlling. Figure Ishows the sampling train used by the department. A sample bag

is placed inside the rigid leak-proofcontainer. Bag material shall be manufactured ofFEP Teflon,

Tedlar.orMylar.

2 h. The bag is filled by partially evacuating the rigid container. After partial

filling, the air in the bag is expelled by pumping air into the container until the bag is empty. This

serves to precondition the bag walls.

3' ,. The bag is then totally filled by evacuating the container with a pump.

The bag is removed, capped or sealed, and tagged for storage and eventual transport to the odor

lab for sample evaluation. See Figure Ifor apparatus setup.

.. i1. Ifthe odorous air is very humid, and it is suspected that condensation of

water will occur in the bags, an additional procedure, predilution, can be used to prevent

condensation. The bag is ba1ffilled ·..nth odor-free air using a cylinder and flowmeter. This will

allow exact metering ofa known amount ofodor-free air; the odorous air san:pie can then be

taken per previous instructions. -

~. Odorous samples should be stored in containers for a minimum oftime

after collection. This should be adhered to wherever pOSSIble and the time ofstorage, before odor

measurement, must be recorded for each sample. Ideal storage conditions are less than four hours;

acceptable conditions for most odor mixtures'are 8"16hourrStorage oyer 24-hours is- --

unacceptable. In general, to prevent sample deterioration:

a i. use FEP Teflon, Tedlar, or Mylar bags;

b ii. minimize sample storage time; and

e iii. predilute sample bag or use other suitable means to remove

moisture ifcondensation is evident on the bag wall.

24
FINAL RULE/DECEMBER 20, 1996 AQ145

B 1. The department uses butanol referencing techniques for quantifYing odors in

terms ofinteosity. The method parallelsthat specified in ASTM ES44-7S. A complete description

oCtile method follows: , .,.' + a. Description .....', _ , .

a i. Figure 2 depicts the olfiu:tometer. Adjustable air flow controls

an:: mounted on the rectangular base plate. The odorant vapor generator, flow splitters, and ports

that deliver the prepared stimuli (butanol) Ire mounted on an aluminum plate disc that can be

rotated within an almost fW1 revolution. A bandle is positioned to tum the sample ports and is set

to limit the rotation ofthe disc to one turn.

b i. There Ire two air flow systems within the olfiu:tometer, each is

controlled by • separate vIlve (V) and monitored by separate in-Iine flowmeters (Flo FJ. Both can

be supplied &om the same air supply. .

e iii. Odorant vapor flow system is supplied with air at. rate onso

mlImin (left flowmeter). This air flow is delivered to the odorant vapor generator through. '

flexible food-grade (almost odorless) Tygon tubing (1'). The odorant vapor generator consists of. '

glass vessel (G) and several flow-controlling capillaries. This section is shown separately

schematically in Figure 3.

d The odorant vapor/air mixture from the generator is supplied to

the upper cavity ofthe ·odorsplitter" (0) through the upper tubular spout ofthis splitter. The

splitter distn"butes the generator-prepared vapor/air mixture to eight stainless steel capillaries. The

other ends ofthe capillaries COMect via Teflon tubing to the corresponding glass snifling ports.

The capillaries Ire calibrated so that Port No.8 (highest odorant concentration) receives .

mominally 160 mlImin ofthe vapor/air mixture, and the next Port, No.7. receives nominally 80

mlImin ofthe same mixture. Other ports receive odorant volumes as per Table 1.

e x. The make-up air flow system, which is controlled by the valve -

. Flowmeter assembly (FJ. is fed at 9S0 mlImin. It is distn"buted by the lower level ofthe splitter

(0). The make-up air is delivered to this level via Tygon tubing attached to the spout ofthe

splitter under,the olfiu:tometer disc. There is no coMection between the lower level.and upper

level ofthe splitter. The lower splitter provides additional air to Ports No.7 through No. I so that

the total flow to each port is nominally 160 mlImin. Mixing occurs in the port. Rapid flow rate

changes occur on emergence from the Teflon tubing and from the lower smaller cross section of

the glass port into the wider vertical glass tube portion. This action assures sufficient turbulence

for adequate mixing.

-''''-J~,&:'''''!,'_'' .: ..••-.--... .••.

25
Fr.NAL RULE/DECEMBER 20, 1996

.. AQ145

. 1·,,1._-- •.

i £a). Flow rates are measured, if'necessary. by attaching a

Buck Calibratorflowmeter to ends ofthe Tet10D tubings temporarily pulled out ofthe ports.

Nominal flow rates should be:

Table I

.. 0cI&nal vapar.canyioa Mako-UpAk TbbiNzPai

PoRNo. TubimrBad (mLiDia) TIabiM Bod (mIImia)

I 160

7 80 . 80

6 40 120

, 20 140

4 10 150

3 5 ISS

2 2.5 157.5

1 1.25 158.5

ii au. The actual flow rates may differ, usually not more than

within a few percent, and are measured and included in calculations in more exact experiments.

f n. Vapor generator section, Figure 3, contains a saturator, (Vessel

G) which consists ofa horizontal 16 nun o.d. by 170 nun long Pyrex tube with closed ends and

three side tubes. each 4 nun o.d. and 2S nun long. The middle tube is used to introduce the

odorant (butanol) and is then closed with a glass rod plu& p. COMected to the side tube by a short

length ofblack neoprene tubing.

g m. Important SafetyNote: When slipping the neoprene tubing

onto the glass side tubes, hold the side tube with fingers using short neoprene tubing collar with

which the tube is equipped. Twist the attachable neoprene tubing to and fro, to facilitate the

connection. Ifthe glass vessel is held instead, the small glass side tubes may break otT. Use the

same precautions when removing the attachable tubing. Same applies to the other glass

" tlib1ngfneoprene sIip-on' COMectiOns. GoDars are not shown in Figure 3. ' .

It ~. The two other glass side tubes on the vessel are connected to

the flow control capillaries. Capillary C is the principal vapor flow control capillary, while

Capillary E is simply an exit capillary, with much less flow resistance than C. CapillaryB is for air

bypass; it is always ofthe same size and length, while capillary C may be changed to provide Sx,

2Sx, SOx, and lOOx flow split ratio. The department wiD use the nominal Sx flow split ratio in

16
FrNAL ROLE/DECEMBER 20, 1996 .AQ145

estab~ its butanol scale. The ratio offlow rates through bypass B and through the saturator

veSsel vapor space depend on the flow resi~ ofB and C. Capillary C is upstream ofthe

vapor space to maintain air pressure in the saturator vessel close to atmospheric.

.... ·i . ilt. The desirable volume ofodorant in the saturator vessel is 8-:10

mI. which fills the lower halfofthe'vessel and prOvidesthe widest surface. At up to 60 m1/min air

flow, the air leawig the saturator is practically saturaied with the odorant vapor, as bu been

established by mass-transfer calculations and direct measurements oCl-butanol concentrations by

hydrogen fIamc ionization detector; at 60 m1/min, 98 percent plus saturation is reached. The

degree ofsBturation is not a fimc:rion ofthe vapor pressure (which varies with odorants by several

orders ofmagnitude), but ofthe diffiJsion constant for the odorant in air, and this constant varies

from odorant to odorant within a li'acrion ofone order ofmagnitude. The method ofair pusage

over the surtice c:in:umvents the need for mist filters needed when the saturation is by bubbling

the air through the odorant At lower flow rates, a few drops ofthe odorant may provide enough

evaporation surface.

j x. Vaporization rates are too low to produce significant cooli:lg

except for the most volatile odorants. Hence, for simpUcity, no thermostating is provided. but the

temperature at the saturator vessel is measured for use in vapor pressure calculations. The

temperature in the area ofthe apparatus will be maintained at 2S·C.

. k xi. The vapor dilution immediately after the saturation in the vessel

produces a margin ofsafety in preventing condensation in the 8-way splitter, in cue of a

temperature change or sudden pressure drop.

I xii. Connections to the stainless steel capillaries are via slip

connectors, as shown in Figure 3. A short (S MM) length offood-grade Tygon tubing fits tightly

around the capillary. A piece ofblack neoprene tubing overlaps this tubing and the larger

connecting tube (brass 'flee, or glass side tube, or multi-way air or odorant-side splitter) so that

the small Tygon tubing tits tightly against the larger tube. This system permits only a limited

contact between the odorant vapor and Tygon and neoprene. These materials can be reached by

vapors only by a non-connective diffiJsion through stagnant aMular space between the o.d. ofthe

capillary and the larger connecting tube; thus, depletion ofvapor by sorption into Tygon or

neoprene is negligibly small. In reverse, when the odorant vapor is discontinued. contamination of

air flow by desorption ofthe odorant from Tygon or neoprene is slow and usually does not

generate a prolonged contamination problem ofany significance. 8til1, it is desirable to flush the

odorant vapor flow system during the shutdown.

m xiii. Connections between B and E capillaries are via brass tees and

slip on connectors. To check the generator system splitter ratio, brass tee (T) is pulled offB and

E, and the flow rates out ofB and E are meascred using.the same total odorant vapor flow rate as

normal (the splitter ratio may be slightly affected on the absolute flow rates).

n ltbl. Important: Only soap film flowmeters are suitable for

measuring the flow rates in ports and at B and E. Other flowmeters produce some flow resistance

which, in the low-pressure flow system ofthe olfactometer, will influence the flow rates and yield

wrong values. Figure 3, bottom, illustrates connections to the soap film flowmeter for two

situations:

27
FLNAL RULE/DECEMBER 20, 1996 AQ145

i £a). connecting to Teflon tubing ends pulled backward out -.

ofthe ports for measuring flow rates to the ports; and

ii au. connecting to ends ofB orE when the brass Tee

(Figure 3) is pulled offfor measuring the flow ratesfrom B and E, to check split ratio in the vapor

generatorsection. - _.- .~. -. .- ..,

o r£. Very Impottant-To Prevent Undesirable Contamination ofthe

System

. i £a). With the odorant in the vapor-generating vessel. the

flow ofair the odorant part ofthe system must be immediately set in operation. Ifthis is not

done. odorant vapon from the vessel may drift into the splitter bypus, condense there, and result

in a much higher odorant concentration than in the regular operation. It is best to place the

odorant into the vessel through the ceitter spout (c£ Figure 3) with the bypass system (two brass

tees with capillaries B. C. and E attached) removed from the vessel. then plug the center spout of

the vessel, begin air flow and then connect the bypass system to the vessel.

i au. The same applies to shutting-down ofthe olfactometer.

Farst, the by-pass system is removed from the vessel. and the end spouts ofthe odorant ve:se1 are'

plugged with pieces ofneoprene tubing and glass rod plugs. With air flow still continuing, the

capillary C is connected to capillary E by a shon piece ofTet1on tubing. This permits flushing the

odorant vapon from the odorant side ofthe system. Flushing is continued until the

bighest-concentration pon does not exru"bit odor.

e 1. ProblemslBaclcflow. Failure to observe need for continuous air flow while the

odorant vessel is connected to the splitter (see preceding section) can easily result in diffusion of

the odorant throughout the system, including baclc-diffusion into the Tygon tubing connecting

flowmeter to the disc assembly. Such contamination is difficult to remove, and replacement of

some components may become necessary. A list ofsources for the components is attached

(SubsectionE!U ofthis Section).

B Sample Calculation ofDilutions

+ .. Saturated Butanol

a . i. Odorant: I· Butanol

b ii. Temperature: 2S·C

e iii. Vapor pressure. from Chemistry and Physics Handbook or

other source, for 2S·C is 6.97 mm.

d This corresponds to:

~OOO.OOO x 6.97n60 = 9170 ppm in air saturated with I-butanol vapor at

2S·C; (I atm = 760 mm).

!l h. Dilution Factor in GeneratorlBypass System. Dilution Factor: 4.66:l:

.20 ". '.:··_·~.i";., -.~--,:...~ ..', ,,_.,;,_ •.. _-_._-~.~----"-'-"'•. ,'",---- .

a i. The concentration oft-butanol in the flow supplied to the round

splitter is then:

9170/4.66 = 1966:l: 16 ppm

b ii. This is also the concentration supplied to Pon No.8.

e ill. Measurements for other pons are conducted by pulling the

28
FrNAL RULE/DECEMBER 20, 1996 AQ145

•

Teflon tubing out from the ports and connecting the Buck calibrator to these lines.

11 ix. The conowing set oCdata illustrates the calCulations. (See Table

2)

e X. The brass tee is sequentially pulled offcapillaries B and E and

the air ftow from each is measured.

E i. Components and Sources

+ a. Stainless Steel Capillaries

a i. 1/16 o.eL. 0.030 LeL

b ii. 1/16 D.eL. 0.020 LeL

e iii. 1/16 D.eL. 0.010 LeL

II. Teflon Tubing. Teflon tubing AW Gage No. IS. standard wa1l, natura1

color.

:t G. Tygon Tubing

a i. Tygon Food Grade 0.031S in. tel For s1ip-on-connectors-Cor

stainless steel capi1laries.

b ii. Tygon tubing, Food Grade Formulation B-44-4X, S/32 in. Ld.•

7/32 in. D.d.• 1132 in. wall. For flowmeter-to-disc: co~.:Iection.

e iii. Tygon Food Grade tubing, 0.0655 in. i.d.• 0.1945 in. o.d. For

connection ofsoap film flowmeter tubing to Teflon tubing ends.

.. d. Neoprene Tubing. Black neoprene tubing, 1/4 in. o.d., 1/16 in. wall, Cor

s1ip-on connectors and for. plug.

5 .G. Glass Ports, Odorant Vessel. Pyrex glass, custom-made by glass

blowers.

6 f: Fiowmeters

a i. 50-500 e:cImin

b ii. 100-1000 e:cImin

29
FXNAL IWLE/DECEMBER 20, 1996

. Table 2

B-Port I-Butanol Otmctomctcr

Port Concentration in J) m

Date . 7 6· 5 4 .3·· . ··2' 1

12-13 '1038 ·533· 274 138 70 35 17

12-15 1034 517 272 137 71 34 18 • 12-15 1042 524 268 137 71 34 19

12-15 1042 520 271 132 72 35 18

12-16 1010 513 271 136 70 35 17

12-16 1040 529 278 137 73 36 18

12-16 1032 516 272 134 72 35 18

TOTAL 7238 3652 1906 951 499 244 125

AVO. 1034 522 272 136 71 35 18

=10 =7 :J :2 =1 =1 =1

AQ145

F 6. Odor Panel

t I. An odor panel consisting of eight members sha11 be selected by the

department. Panelists sha11 not use perfume or perfumed shaving lotion within two hours prior to

the test. Panelists sha11 not smoke, eat. or chew tobacco or gum for at least one hour before

testing. Panelists sha11 not be tested for prolonged periods oftime. A loose schedule with long

resting periods for panelists is recorrunended.

2 h. Panelist candidates are screened for their ability to judge intensity. This

is usua1Iy done using the butanol intensity olfactometer. A bag sample is taken from one ofthe

eight butanol ports (usuaI\yNo. 4 or No. 5) and the candidate must sniffthe bag sample and

select the port they feel hasthe same intensity. Panelists·should be able to match

butanol-to-butanol within two scale units. As with a1I sensory odor evaluations, the screening tests

. should be conducted in as nearly an odor-free envirorunent as possible.

:I' .c. The testing room will be supplied with activated carbon filtered air of

. __. _.~ntrolled constant temperature and humidity (25·C and RH 50 percent).

.... .".. ..11. EaCh panelist compares the intensity ciftlic undiluted ambient sample

being evaluated to the eight point butanol scale, specified in this procedure starting from the low

end ofscale, i.e.• l::levels between two values on the scale may be selected by each panelist (i.e.

2.5,6.5. etc). The arithmetic average ofthe values chosen by the eight panelists win detennine

compliance with the standard specified in the regulations.

30
-

FLNAL RULE/DECEMBER 20, 1996 AQ14S

RIGIDr LEAK pnoo,

CONTAINER

rFEMALE

VACUUII

LINe

·cQUICK

CO~MICT L. - ..AU

II

TIPLON .AIIPU

LINe

TI'LOIf

..noae

31
FrNAL RULE/DECEMBER 20, 1996

,.....

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AQ145

. ~..... .

31

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Fr.NAL RULE/DECEMBER 20, 1996 AQ145

..

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33

oren_ f ..~la&

/ f&'IM'Drc

Qt~
F~ RULE/DECEMBER 20, 1996 AQ145

AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

InSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office

ofAir Quality and Nuclear Energy, Air Quality Division, LR. 13:741 (December 1987), amended

by the Office ofAir Quality and ]hdjatiOD Protection, AU: Quality Division, LR.

•

34
FINAL ROLE/DECEMBER 20, 1996

Title 33

ENVIRONMENTAL QUAIJTY

PartID. Air

Chapter 30 Standards ofPerformance forNew StatioDUY SQurces (NSPS) . . .-...

13101._cal gd Rcagmhcri0l'

AQ145

. ,

The folJowi01 dvurtm. u they appeared on June 30. 1996, are hereby repealed or

renumbered u jodiqtcd belOW;

A.. Chapter 31 is mpcaJcd

B. Chapter 60 i'rcpcaJod with the exception ofLAC 33·m 6099 which is moved and

mmmbered u LAC 33·m 2901 ,G,

c.. Chapter 61 is repealed with the exception ofS~hzurterA which is moved and

renumbered as Subc;bapter N in ctapter 21 ,

D... Chapter 64 is repealed.

AUTHORITY NOTE: Promulgated in accordance with R.S..30:2054.

mSTORlCAL NOTE: Promulgated by the Department ofEnviromnental Quality, Office

ofAir Quality and Radiation Protection, Air Quality Divi~on, LR

Subdaaptcr A. IpCOrpODtjoo by Reference aBR)

13003•mR 40 Code gfFdmlRezu1atioCf (CFR) Part 60

A, Except U modified in this section. rcauJatjOD$ at 40 CFR Part 60 as revised July 1,

129S, and sPecified below in Tables 1 and 1,A are hereby inco[pOrated by reference as they ~ply

40CFB

Part 60

Subpart Beldin:

Emi .

3S
FINAL RULE/DECEMBER 20, 1996 AQ145

'. . TABLEt .

40~

40QB, Sgbpltt HcadinC

Part '0 ..

-. .. . .

.J:h . . .- .... :llod ., - •f'nr~A,.;tf. . . I Unit!t •

...n StllDdards ofPerfQDDllDce fpr Fos!lIl-Fud Ere<! Team GeneratoR for Which - • ,T. After 17 1071

....Da Standards ofPerfonnance fpr Electric Utjf'lY Stearn C".eneratinc Units for Which

• IJ~ After ·1f1 10711

....DIl Standards ofPerfonnancc for Indnstrial-Commcn;ial-InstjtutjonaJ Steam

..Q! · ,Unit!t

Standllrds ofPcrformance for SmaJl Jndustrial-CommerciaJ-Jnstitutional Steam

· ,Unit!t

.E ,f'nr 9 .

..Ea - · • lof A

,for .. . .

...E I for'

..G • A,.;tf

...H _. • • :of- A I for - 'A • Aci~

,I ,,- ,fnr A....10.1. -

..l · · A' A

,for IV, A .

...K StllDdards Ofperformance for Storace vessels for petroleum Liquids for Which

CoOstruction. Reconstruction. or ModifiCatioo Commenced After June 11.

1071 an~ Prior.n Mav 19, 1978

....KIl Standards ofPerformance for Storage Vessels for petroleum liquids for Wbich

Construction Reconstruction or Modification commenced Mer May 18 1°78

lin" Prlnr tn T"lv"1 .

....Kh Standards ofperformance for Yolatjle Organic IJQuid Stomge Vessels

OncJudinc Petroleum Liquid Stomge Vessels) for Which Construction

1), • nr" J;~ • "ft..rJlllv21191l4

L Standards of A

ance for SecondarY T....tf ~melters

36
FINAL RULE/DECEMBER 20, 1996 AQ145

TABU; 1

1~60

40Q1l Sp~p.rt"UndiD' -... . -

p,rt60

~- .. .'

.M • . 'bQ{. - ! fOr- , - ,aR" .

..H Standards ofperfbrmanljQ for PrimmEmission, fipm Basjc Oxxam Prom' - ,&.~ • lig'Aft_T"R_l1 1Q71 .

...lia Standan!g ofperfonnance for Secondll)' Emjssjong fjpm Basjc Oxxam Procesg

stcc1m8JrjuIJ FaplitiCS for Which Constmction is Commenced After Jlnula 20 00 .

0 •for

p ~- •for~ • - .

0 ~- - ~. - .

R - . - . ,T _tl- . 'tor

S ·for . A . - .

....:I Standards ofPertbrmance for the Pho:;pbate Fertilizer Industry: Wet-Process .l!! . . A,.;tl

....ll Standards ofperformancc for the Pho!ijlhate Fertilizer Industry;

• A";~ .

..:L Standards ofperfimnans;e for the pho!ijlhate Fertilizer IndustJy: Diammonjum

~'~ .

...:if. Standards ofPerfonnancc for the phosphate Ferttlizer IndustJy: Triple

-

.l' Standards ofperformance for the phosphate Fertilizer lndustO'· Granular . " ...

.tnr;'0.("- '..=';" . ... ,-_.~. . .. - . - J.

z •for .. • D._,f.~ ...:_., 'I:'~,.;Ji'i..

--AA Standards ofperformance for Steel plants' Electric Arc Furnaces Constructed

After l , , 1 1Q74 ~ntl on or Reforf! Anm••• 17 1983

37
FrNAL RULE/DECEMBER 20, 1996 AQ145

TABI,E I - An~60 -

40CFB. Subpart IlcadjD~ ._", rlrtiO

- -

.A&. Standards ofPerformance for Steel Plants' Eldric Arc Furnaces and Arion- , bR .. - A~.... A ..,7 J.gg

• 1'..... Tl'... 1»0,1"

, . -- , ,f'nr~ _. - . ....tC

DD •f'n.. r.....l" -

...EB .. ,tnr - - - . .. .- .

FF fR .n

--.00 • • -- ,f'nr - . ,r...~- ..

...HH .~ ..~; nt •f'nr T.im.. M ~ft, - .

KK •f'nr T..~tl_A,.;tf • .

LL • .~ •f'n.. - ..- .- . _.

.MM Standards ofPerfonnance for Automobile and liibt-puty Truck Surface

· ·

...IDi . .f'nr , Rndr

..H - • • -- ,fhr • .

....QQ Standards pfPCIfuanance for the C'l1'8,pbic Arts IndustO" Publication ...- · . ,

....B.B. Standards ofPerformance for Pressure Sensitjye Tape and Label Surface

· ·

--SS _. • ': nf ·fnr . ..- .r', 0

o T,arne Annr

.:.rr .. . ~t~rirl~rrl. nt~ •f'n.. M,;to1 r<in - . . .. "_J-. ..... _ • -..

...!lll Standards pfPerformance for Asphalt Processing and Asphalt Roofing

M~n

38
FXNAL ROLE/DECEMBER 20, 1996 AQ145

. . UBLEt

•O~

'·QUB Sgbpart Bcadin,

',rtO ..

-.

...l!l! • Standards ofperfgnnanGC fnr FquiprnentTnU ofyOC in the Synthetic ..Q! '!.Q ' -~ ,

WW ,fnr th,,- , 9

..xx ..§!i , , !fhr RII"" - . " bI! ,

AAA , ' ... !for' ,'D, , , .

..§!i · , . • !forth.. • • .Tire .. , 9 ,

CCC ,.,

PDP Standards ofperfonnance fnr yoIatUe Organic Compound (YOC) Emissions

fTomthe""··"~ •

lrnF. ,.,

-fEE • • .~ . •f'nr - ~', V,nvl .nll T' .• . . and . .

GC',Q Standards ofperfonnance for Equipment Leaks ofyoe in Petroleym -- ,

HHH • ': of ,for , . ...

....III Standards ofPerfonnance fhr Yolattle OJpnjc Compound (YOe) Emissions

Fmm the Synthetic Orpnic Chemica! Manufacturini Industty (SOCMD Ajr

, , I TJnit

JJJ ,..,. ,for- • Inrv£!!

KKK Standards ofPerfonnance for Equipment Leaks ofYOC From Onshore NaMa!

r...~- 'n"-'

- LLL ~t.nrl-rds(l--...er"'n _for"" _L , r.... . . so" Emissions

MMM I J)

NNN Standards ofperfonnance for WatUe Organic compound CVOe) Emissjons

fonn Synthetjc Organjc Chemical Manufacturing IndustO' (SOCW) Djstj1)atjon

( JDeration~

39
FrNAL RULE/DECEHBER 20, 1996 .\0145

TABLEt

..n~

40U'B Sgbp.rt Beadjnr

Part 60 ..- _.- -

.

000 • ~'" ...... .. .

PPP • _. • · ~, ,for Wool.§l1 . ~. . ..

000 Standards ofPerfnnnBuM for YOC Emissions From petmJCUm Refinery

RRa Standards ofPerfonnance for volatile 0mnic Compound Emissions From

Synthetic 0mnic Chemica! Manufacturinz IndusttY (SOCMD Reactor

- !':!':S · ,fnr'M: • :Tane . - ....

W Standards ofPerfonnance for Industria! Surface Coatin:" Surface Coatin: of

~Partsfnr' . .~ .

umJ ~., fnr .•. , ..nd~· ,in .

YYV Standards ofperfunnance for Polymeric Coatin: ofSupportini Substrates

Facilities

TABLEJ.A

.sn rFR 'PA'RT,;n '-~

40QR Appendjx Headjn: ,

Part 6Q

A . .

-A Test Methods

B. . .. ti"".· .. ~- .•... _____ L_.. ..

...c · . lofb . . ,RM..

...D . .."missinn Tnv 'jnn

E (R"S"IV"'!)

4Q
FZNAL RULE/DECEMBER 20, ~996 AQ145

4QCFB

Part 6Q

..

Appendix UndlDI

"

--G Provisions for an AlternativeMethod ofDemonstratina Compliance Wrth 40

CPR 60 43 for the Ncwtpn Power StJ!jgn gfCentraJ minail Public Service

B Fina! repletions published in Federal Re~from July 2. 1995. tbrou~ June 30.

1996. and specified betow in Table 2. are hereby incorporated by reference as they apply to the

State ofLoujsjana

Subpan w

Subpart Hcadjnz'Appcndjl

Federal

Rezistq

Citation

60FR

43258

nm

Promulpted

August J8, J995

Subpart

OOQ

Standards QfPerformance for yoe ..... ..... ,-: 60JR ...._.r August 18. 1995

Emissions from petroleum Refinery .. 43259

41
FINAL lUJLE/DECEMBER 20, 1996 AQ145

i. December] 9.

.l22S.

mER

6S414,~

OeneraJ Provisions

F(/mI Dale

SgbpartBcadin:lAppcndg Ra&t« PrpmuJ:atcd

CtatjoQ

ApgendiM Standardl olPcrfprrnJmee for New 60ER september J1.

StatiODID' Sggrccs Appendjx A - 47096 l221

Reference Methods; Amendment to

Method 24 for the Determination of

VoJ,tDe Matter content. Water Content. Denm Yolume SoUd$. and Weiaht Solids

Sub,part Standards gfPerformance for YoJatUe mER November 27.

Htni Orpmc Compound (YOC) Emissions 58237 l221

From Synthetic Orpnic Chemical

Manuticturini Industty (SOCMI) . .

Subpart StandardS OfPerfonnance for YoJatUe &.ED. November 27.

B.B.B. Orpnic Compound (YOC) EmissioDs 58238 .l.22S.

From Synthetic Orpnic Chemical

Manufacturina Industty (SOCMI) Reactor

SubpartEa mER December 19.

65384 .l.22S.

Subpart A

Subpart B

Subpart C

41
FINAL RULE/DECEMBER 20, 1996 AQ145

March J2. )996

December 19

1221

61 FR. 2918

60ER

65419

Oeneral Provisions

0- Fdmll Dm

Sgbpart BeadtnlfA,ppcndjl Rezist« PromgJ&atesl

CitatioQ

SubpartCa 60FR December 19.

6S414 1221 .

Subpart Cb 60FR December 19.

6S414 1221

Sulwart Cc 60FR Decembec J2.

65414

Subpart Cd Emission Guidelines and Compliance 60FR December 19

Iimes for Sulfuric Acid Production Units 65414 .L22i

SubpartCb 60FR D~erJ9.

65415 .L22i

SubpartC Emission Guidelines and Compliance

l:im§

61 FR 9919 March 12 1996

Subpart

61 FR 9919 March 12 1926

61 FR 9919 March 12, 1996

43
FXNAL RULE/DECEHBER 20, 1996 AQ145

Fda llm· , - . Subpart BcadinlfAppcudjx Ruist". ;pmmulptcd·

CUaUop

SubartQ& 61FR March 29. 1926

1403J

Sub,partf Standard' ofPerfpnnanee for Portland 61FR Apn13.1996

J4637

SuJuJart A General PmvisiOM April 25.. J996

Appendix A rest Methods 6JFR April 25, 1996

18262

SubpartI2c §liB. h1a:Y 8, 1996

20736

c correctjye modification and clarification are made as foJJaws:

J. 40 CFR part §O SUQpart A Section 60.4 O!)(D, to read as follows: State of

Louisiana" Pmprn Administrator. Air DuaJity Division. Loujsiana Department ofE~' yironmental

Quality.. Post Office BOl 82135. Baton Rou~ Louisiana 7088+2J35; and

2. The milabilitx to the public ofiofonnation provided to or otherwise obtajned

by the state underthis Chaptershall be eovemed by LAC 33:1 501-509.

D. Copies ofdQCUments ioco[P'orated by reference in this Chapter may be ~taiOed from

the Syperintepdent QfDocuments. U S Government Printi0i Office;, Washington. D C, 20242

AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054.

mSTORICAL NOTE: Promulgated by the Department ofEnviroMlental Quality, Office

ofAir Quality and·R.idiationProtection, Air Quality DiviSion, LR' ..... _~_.. ,... ,.

44
FINAL RULE/DECEMBER 20, 1996

TIde 33

ENVIRONMENTAL QUALITY

PartID.Air .

Chapter 31. Repealed la its entiret)'.

4S

AQ145

-,
- FINAL ROLE/DECEMBER 20, 1996

Tide 33

ENVIRONMENTAL QU.u.nY

Partm.Alr .

AQ145

Chapter 60. (Editor'. Note: Chapter 60 repealed ucept for Section 6099 which wiD be

moved to LAC 33:m.2901.G}

•

"-,;; ',,- ",_. •••-. - ...-.-.~.. 110" • .,k.--'- -,-".

46
FINAL RULE/DECEMBER 20, 1996

nde33

ENVIRONMENTAL QUAUTY

Part m. Air

AQ145

Chapter 'I. [Editor's Note: Chapter 'I repealed except for Subchapter A which wiD he

moved to SubchapterN ofChapter 21.]

•

47

_. I ."
FrNAL RULE/DECEMBER 20, 1996

TIde 33

ENVIRONMENTAL QUALITY

Part ID. Air

.... Chapter 64. Repealed in its entirety•.

•

48

AQ145
NOTICE OF INTENT

Incorporation by Reference (LAC 33:III.Chapters I, 15.21,

25,29,30,31,60,61 and 64) (AQ 145)

Department of Environmental Quality

Office of Air Quality and Radiation Protection

Air Quality Division

IV .

Under the authority ofthe Louisiana Environmental Quality

Act, R.S. 30:200 I 'et seq., and in accordance with the

provisions ofthe Administrative Ptocedure Act, R.S. 49:950,

et seq., the secretary gives notice that rulemaking procedures

have been initiated to amend the Air Quality Division

regulations, LAC 33:III.Chapters I, 15,21,25,29,30,31,60,

61 and 64 (AQI45).

This proposed rule repeals LAC 33:III.Chapters 31, 60

(except section 6099 which will be moved and renumbered as

LAC 33:111:2901.0), 61 (except Subchapter A which will be

moved and renumbered as SUbchapter N in Chapter 21), and

64 from LAC 33:111 and to incorporate by reference into

Chapter 30 federal regulations in 40 CFR Part 60 - Standards

of Performance for New Stationary Sources. Revisions will

also be made in LAC 33:III.Chapters I, 15,21,25 and 29, so

that referenced LAC cites agree with changes per this

rulemaking, and to add 40 CFR references. These changes

will expedite both the EPA approval process, and state

implementation of delegation of authority for the NSPS

program. The NSPS and the authority for EPA to delegate

authority of that program to the state is established in the

Clean Air Act Amendments of 1990, Section 111. This

rulemaking is applicable to stationary sources statewide.

This proposed rule meets the exceptions listed in R.S.

30:2019(0)(3) and R.S. 49:953(0)(3), therefore, no report

regarding environmentallhealth benefits and sociaVeconomic

costs is required.

A public hearing will be held on September 26, 1996. at

I:30 p.m. in the Maynard Ketcham Building, Room 326,

7290 Bluebonnet Boulevard, Baton Rouge, LA 70810.

Interested persons are invited to attend and submit oral

comments on the proposed amendments. Should individuals

with a disability need an accommodation in order to

participate please contact Patsy Deaville at the address given

below or at (504) 765-0399.

All interested persons are invited to submit written

comments on the proposed regulations. Commentors should

reference this proposed regulation by AQ145. Such

comments should be submitted no later than October 3, 1996,

at 4:30 p.m., to Patsy Deaville, Investigations and Regulation

Development Division, Box 82282, Baton Rouge, LA, 70810

or to FAX (504) 765-0486.

I. ESTIMATED MPLEMENTATION COS (SAVINGS)TO

STATE OR CAL GOVERNMENTAL ITS (Summary)

The est! ted implementation costs to addi g two members

to the Teo er Certification Couneil is appro ately $4.000

per year, ascd on state travel regulations. The ouocH meets

approxi tely 10 times a year, based on number fappeals to

be revi cd.

The stimated costs for printing this policy rcvisi n and first

page fiscal and economic statement in the Louisian Register

is $1 O.

II. ES MATED EFFECT ON REVENUE COLLECTI NS OF

Sl: TE OR LOCAL GOVERNMENTAL UNITS (Su aryl

here is no effect on revenue collections of state or local

ovcmmental units associated with this rule.

STiMATED COSTS AND/OR ECONOMIC BENEF TS

TO DIRECTLY AFFECTED PERSONS R

NONGOVERNMENTAL GROUPS (Summary)

There arc no costs or economic benefits to directly affecte

persons or nOJlgovemmental units associated with this rule.

FISCAL AND E ONOMIC IMPA

FOR MINISTRATIVE

RULE TITLE: eoeber Certifieation

Title 28

EDUCATION

Board of Elementary and Secondary Edu alion

Chapte I, Organization

1107. Bo d Appeals Council

A. Tea er Certification Appeals Council

I. Co position. A Teacher Certificati Appeals

Council sha be appointed by the board and sh I consist of

nine membe three of whom shall be represe tatives from

the universities one of whom shall be a repre ntative ofthe

Parish Superint dents' Association, one of om shall be a

representative of e PeT\onnel Directors' As ociation, one of

whom shall be a resentative ofthe Princi Is' Association,

and three of wh shall be classroo teachers. The

classroom teachers hall consist of one presentative each

from the Louisiana Federation of eachers, Louisiana

Association of Educa rs, and the A ociated Professional

Educators of Louisian The board II be responsible only

for paying travel expen of coun I members at the state

rate.

ertification Appeals Council to include a personnel a"eCIor

r presentative ofthe Personnel Directors' Association and

p cipal representative ofthe Principals' Association. s

is revision to the Louisiana Administrative Code as no

belo :

AUTHORITY NOTE: Pro ulga in accordance with R.S.

17:3(0) and R.S. 17:6(A)(9).

Interested persons may co nt on the proposed revision

until 4:30 p.m. October 9,199 to: Jeannie Stokes, Board of

Elementary and Secondary d cation, Box 94064, Capitol

Station, Baton Rouge, LA 7 80 9064.

727 Louisiana R_g;sr., Vol. 22. No.8 Augusr 20. 1996
(

f

v.

d phrases, when used in

NOTICE OF INTENT

[S.. Prior Textl

the selling and transferring 0 waste tires or

rial for recycling and/or benefici I use or reuse.

•••

Department of Environmental Quality

Office of Solid and Hazardous Waste

Solid Waste Division

aste Tire (LAC 33:VII.Chapter 105)(SW021

Under e authority ofthe Louisiana Environmen Quality

Act, R.S. 0:200 I et seq., and in accordanc with the

provisions the Administrative Procedure Act, .S. 49:950,

et seq., the s gives notice that rulemakin procedures

have been i tiated to amend the Solid W te Division

regulations, L C 33:VII.Chapter 105 (SW02 ).

The propose rule will make modificati to the Waste

Tire Managemen Fund Prioritization Syste providing more

equity in cleanup and make the emerg cy rule in effect

permanenL The rul also provides for matical cleanup of

the waste tire regula ·ons.

This proposed rul meets the exc tions listed in R.S.

30:2019(DX3) and R. . 49:953(GX , therefore, no repan

regarding environmenta ealth bene ts and social/economic

costs is required.

[S.. Prior Tex'l

II asphaltic co crete and concrete

te highwa)'s and ro s maintained by the

United States go rnment or Louisiana s te government, or

cies or depanments ther f.

•••

[Sec: Prior Tex.)

Prom' ous Tire Pi/e---mt unauthorized waste 're pile that

has res ted from storage or disposal activities

other an the landowner without the landowner's kn

•••

[See Prior Text]

THORITY NOTE: Promulgated in accordance

30' 411-2422.

ISTORICAL NOTE: Promulgated b)' the Departmen

nvironmental Quality, Office ofSolid and Hazardous Waste, S

aste Division, LR 18:37 (January 1992), amended LR 20:1

(September 1994), LR 22:

Richard W. England

Assistant io the

Legislative Fiscal Officer

Gus Von Bodungen

Assistant Secretary

FISCAL AND ECONOMIC IMPACT STATEMENT

FOR ADMINISTRATIVE RULES

RULE TITLE: Incorporotlon b)' Reference

I. ESTIMATED IMPLEMENTATION COSTS (SAVINGS) TO

STATE OR LOCAL GOVERNMENTAL UNITS (Summary)

Incorporation b)' reference eliminates the need to codif)'

federal regulatory requirements. verbatim, into Louisiana

regulations, and thereb)' eliminates extra volumes of printed

regulations. The result is that the same regulations will be

enforced without duplicating the printing ofthose regulations.

The outcome will be savingsto SlBte government b)' eliminating

Ii volume ofregulations that would be purchased (or printed).

A significant reduction in man-hours will be achieved b)'

eliminating the need to type, proof. and correct federal

regulations promulgated as state regUlations.

11. ESTIMATED EFFECT ON REVENUE COLLECTIONS OF

STATE OR LOCAL GOVERNMENTAL UNITS (Summary)

There is no anticipated impact on revenue collections ofstate

or local governmental units.

III. ESTIMATED COSTS AND/OR ECONOMIC BENEFITS

TO DIRECTLY AFFECTED PERSONS OR

NONGOVERNMENTAL GROUPS (Summary)

Incorporation b)' reference eliminates the need to codif)'

federal regulatory requirements, verbatim. into Louisiana

regulations, and thereby eliminates extra volumes of printed

regulations. The result is that the same regulations will be

enforced without duplicating the printing ofthose regulations.

The outcome will be a savings to the regulated community by

eliminating a volume ofrcgulations that would be purchased (or

printed).

IV. ESTIMATED EFFECT ON COMPETITION AND

EMPLOYMENT (Summary)

There is no effect on competition and employment.

Copies ofthis proposed regulation can be purchased at the

above referenced address and also at the Office of the State

Register, 105 I North Third Street, Baton Rouge, LA 70802 at

(504) 342-5015. Contact the Investigations and Regulation

Development Division at (504) 765-0399 for pricing

information. Check or money order is required in advance for

each copy of AQ145.

This proposed regulation is available for inspection at the

following DEQ office locations from 8 a.m. until 4:30 p.m.:

7290 Bluebonnet Boulevard, Fourth Floor, Baton Rouge, LA

70810; 804 31st Street, Monroe, LA 71203; State Office

Building, 1525 Fairfield Avenue, Shreveport, LA 711 0I; 3519

Patrick Street, Lake Charles, LA 70605; 350 I Chateau

Boulevard West Wing. Kenner, LA 70065; 100 Asma

Boulevard, Suite 151, Lafayette, LA 70508.

Gus Von Bodungen

Assistanl Secretary

9605#045

728
L

"-JBuIHEI) NClIlNlNGS

221 J~SON sn:tEET

!.AI"AY£TTE. 1"OUlSIAHA

~G.coltal:

".O.8OX:P"

'-NAYETT'I. LA. '7O:IOa

~ONE: (311) 21e-e300 "AX:. (:II II 28~~

AFFIDAVITOFPUBUCATION

In order to ....proper cndlt.

pl.... ~,. to your ad number

when making payrMRt.

-

- do solemnly Nearthat I., the LEGAL CLERK

of 1M! ADVERTISER. • newspaper printed Uld pUbllsJ1ed at Lafayetbl, In the Parish of Lafayltte,

STATE OF LOUISIANA

PARISH OF LAFAYETTE

"~Q..

State of Loul_lana, and that from my personal knowledge and reference to the ftl.. of uld

pubncaUon the advertisement of:

was published in THE ADVERTISER on the following dates:

/.JwMd()tJ_...=lII:~~'-=~-LJL-I'I~9' *

*

*

* , *

* *

Sworn to and subscribed before me this d& ~ay of . a~L...;t: ,199&

d!h'AL~ NOTARVPC

l->wIlrn und Sl1hscrihcd .\1 my "ffke in !..:lk(' Charll·s.

Betore me. the undersignro authority. Pf!rsonaUy came and

State of Louisiana

Notary Puhli('.

day of __ _

PARISH OF CALCASIEU

KATHY IGUESS

IH __ ,

J=_ . I

NOTICE OF INTENT A public: hearlno wi I be I ~''''of helden ~ber26.1996. at

tal Quelllty, 0ffIc. of Air 1:30 p.m. In th~ Maynord . Quality ond R.adlatlon Ketcham Bulldin;. Room'

Protection, Air QUOllty 326. 7290 Bluebonnet

Division. .' Boultvarcl. Bolon Rauue, La.

Under1tle DUthority at 1tIe 108!O. Interested Il8r'SClnS ore Louislano Environmental ' Invlt~ to attend oncl submIt

QualifY Ad, Lo. R.S. 30:2001 oral c:omments on the pr~ ~t $C!Cl•• ancl In oc:c:arClanc:e . omendmenlS. Should

wIth the provisions of the ·lndlvldualswlfl'lOdlsobility Administrative Proc:~ure need on ac:c:ommodation In

Act, Lo. R.S. A9:950, et seq.. order to PCIrtleiPCIte olease

the sKretary elv" notice contoct Patsy Deavilleat1tle

that rulemakine Pr'OCedWes oddress given below or ot hOve been initioteel toornencl l500Cl 765-0399. lppeared th~ Air Quality Division ~Ji interest~Personsore R~eulofionl, LAC 33: Ill. InVited to submit written who being duly !iworn, depo!ieS and says: That he is the duly Chapters 1, 15. 21 25 29 30 comments on the PrclPOSed '

31. 60. 61 ond' iJ lLog re;ulotlonl. Commentors authorized "-ntotTHE LAKE CHARLES AMERICAN PRESS 4tAQI45l. should ref~renee thls pr~ ...... •

ThISPt"OPCIMdrulweoeals OClSltClre;ulCitionbytheLCIll . br h d da'! . t Lak Ch! '-'.' :.AC 33:llI.ChODlel'l 31.60 #AQ1.c5. Such comments a newspaper pu lS elY a e ar eli.....'ul:;lana.

,exeept sedi,.., 6099 which should be submltt~no lat~r (Add So 2893 Lak Ch I LA - )('02) ....i1i be moy~ and renum- than OCtOber 3, 1996. ot A:30 ress: X • f! ar es. I ( l

~redClS LAC 33' 1lI.29ll1 G l p.m,. to PotSY DeovlJle

,1 (exceDt SUbehoDter'A In~esll;otlons ond Reeu: , ,. . • vhleh will "'. mov~d Ond plotlOl'l~~D1vlllon. That tht> attae:hf!d .....as pul)hshf!d III said nt>.....spapN In ILeo

enurntlrred..,£sSubchaDter N ost OffIce Box 82282. Baton "l ChaDter 21). and 6A from Rouge. La., 70810 or to fox

_AC 33;III oncl to ;ncorpo. (S04l CCIPift • e() d d AUG 16 1996 Cite by reference Into of this ProOClSltCl reoulation ISSU S atf! ....::~~~.:::...;::....:l'I.-..:.'O::~..l::.. _

,:hClpter 30 ~ral reoula- eCin be Durchosed ot th~

,ons In 40 CFR Part 60. above "'ferl!.llC~ oCklre5ll.

ICindordSOf Performonce You.rnclYCDnt.xtthe Investj. 33756801-S30 00 Jr N_Stotionary Sources Ilotlons 'ond Re;ulotion - "'"'"'''-=-.;..:._~:..=.~~~'o.:~ _

:evllions wlU also be madli Development Division Cit 1 LAC 33:III.ChClPters 1. IS. I

ISOAI 1.25 and 29. SO 76:5.0399 for prlcin; thOt refer' nfllrmation. ChIcltormo..v _

nc~ LAC cites oeree With order IS recaui...clln CIdvonce ~anll" wr this rulemok. for ea.eh COPY of AQ104S. •g, Clnd to·odd 40 CFR ref. I ThIS ProPOSed regulation -enees. TtleSeChclnHs will Sovollabi41 tor 1rl5PeCtlon at -------- - ~- _

<pedlte both the EPA thefolfO'Ning DEQOffa locoOlprOvol Dracess. and stat. tlons trom 8:00 a.m. until

"1Dlementation of deiello- A:30 p.m.; 7290 Bluebon~

)n of outhOf1fY fOr the NSPS BoulevClrd. Ath floor. Baton I-~------------------------­ ogrom. The NSPSand fhe Rou;e. Lo. 70810; eo.. 31st

Jthorlty for EPA to dele- Str~f, Monr~, La. 71203;

,Ie authority of thot pr~ Sto.te.Offlce Bulldlnll. 1525 am to the sfot~ is estob- FCI,rfleld Avenue, Shrevehed in the Cleon Air Act DOrt. La. n 101; 3519 PCI1rlck

nend"!8"'Sof 1990. SKtion Street. Loke Chorles, LCI. I. ThiS rulemClkjng Is 70605; 3501 ChoteCiu Boul~-

plicCible to StOlionory 7

vOord West Wlnll. Kenner, LCI.

Jrces stoTewide_ 0,65; 100 AsmCi Boulevard.

This proposed rule meets Su,te 151. LafaYette. La.

,exceptions liSTed in R S 70506.

2019 (D) (J) and R."S: ; GU~ Von BDdungen, 953 CG) (3), therefore. no ' ASSISTanT secreTorY,

'ort regarding environ-I AUgUSI16. .IT

ntallheolth bene/its Clnd 118.16.05

:lal/economiC costs is I Louisiana. Ihis

""1 '

LAST0100
GANNETT CO.'INC.

Publisher of

The hereto attached advertisement

dally newspaper of general circulaAD

,

mACiD~

Th.e News-Star

MONROE, LOUISIANA.

PROOF OF PUBLlCATION

was published in The N EWS-5TAR, a

Parish of Ouachita, in the Issues of:

(ly..f;uBf

tion, published In Monroe, Louisiana,

the person whose signature appears

above in M.onroe, La. on this

Sworn and subscribed before me by

--1-/....... 1_.__day Of~~9V

56
3800 HOWARD AVENUE, NEW ORLEANS. LOUISIANA 70140-1097 TELEPHONE (504) 826-3206

State of Louisiana

Parish of Orleans

P.O. Box 82282

3800 Howard Ave..

City of New Orleans

August ] 4. 1996

Legal. Notices:

Personally app~ared before me, a Notary in and

for the parish of Orleans, Robert-J. Chiasson

who deposes and says that he is the Accounts

Receivable Manager, of the Times-Picayune

Publishing Corporation, a Louisiana Corporation, Publishers of The Times-Picayune, Daily

and Sunday, of general circulation; doing

business in the City of New Orleans and the

State of Louisiana, and that the attached

Sworn to and subscribed before me this

Baton Rouge, Ia. 70804

l&:RlilEIiiiikiiiq iiroeedures have been initiated to anend

the Air Quality Division Regulations UC 33 :U1. Cbapt

1, 15, 25, 29, 30, 31, 60, 61, & 64 Log NO. AQ145

Advertisement of Investigation & Requa1t.ian

New orleans, La. 70Jr40

Was published in b Times Picayune

on the following dates

---:1::..:4=.=th:.::-__dayof August A.D.. 19_9_6__

No(M~1 My commission expires at my death.

FOA"1~

C EAST JEFFERSON I

_._----- --------
llliJ

..

STATE OF LoUISIANA

PARISH OF CADDO

August 25, 1996

Before me, the uodentped authorltJ. perIODIlly came aDd appeared

PROOF OF PUBLICATION

Advertising MaDagerof'l11e Times. aDd that the attacbed advertismeat eatitled:

NOTICE OF INTENT- Department of Environmental QU~

Office of Air Quality and Radiation Prot;ection

Air QUa]ft;y Division (Log*AQ145) t:f=. V43-9 '}- otf9

to me. wbo beiDgdulysworn. deposes aDdsaysthatshe Isthe AaslstaDtto theCIasslfled

following dates towit:

....,jAc...LJ 1tl..Jhu;e...."'i:lsl."",JC_c.L..I.I·tt:......nol.ln..... I perscma1Iy bawD

as per copy of advertisement bereto anDeJ:ed. was published in The Times OD the

SWOrD to aadsubscribed before me

thlolll1lli.~__26_~dlAa,yo'"'f__A-u.... g_u_st •19--!6
· .' CAPITAL CITY PRESS

Publisher of

Sworn and subscribed before me by the person

Indefinite

THE ADVOCATE

PROOF OF PUBLICATION

My Commillion Expires:

..

1007797

V03-97-046, AQ145

whose signature appears above in Baton

~uge, La. on this AUGUST 96

day of AD.

The hereto attached notice was published in

THE ADVOCATE, a daily newspaper of general

circulation, published in Baton Rouge, louisia~

na and the Official Journal of the State of

Lo~isiana, the City of Baton Rouge and the

Parish of East Baton Rouge, in the issues of:
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DEPARTMENT OF ENVIRONMENTAL QUALITY

AIR QUALITY REGULATIONS - LOG NO. AQ145

PUBLIC HEARING

SEPTEMBER 26, 1996

HR. SKY-PECK,

Good afternoon. My name is Steve Sky-Peck. I'm

employed with the Louisiana Department of Environmental

Quality. I'll be serving as Hearing Officer this

afternoon to receive comments regarding proposed

amendments to the Air Quality, Solid waste and Water

Quality Division regulations.

The comment period for these amendments began on

August 20, 1996, when the Notice of Intent was published

in the Louisiana Register. The comment period will

close at 4:30 p.m., October 3, 1996. It would be

helpful to us if all oral comments received today were

followed up in writing.

This public hearing provides a forum for all

interested parties to present comments on the proposed

changes. I'll ask that each commenter begin by stating

their name and affiliation for the record.

The first amendment is designated by Log No. AQ14S.

This rule-making proposes to repeal LAC 33, Part III,

Chapters 31, 60, except for sections 6099, 61, except

subchapter A, and 64, from LAC 33, Part III, and to

incorporate by reference into Chapter 30, federal

regulations in 40 CFR Part 60, the standards of

performance for new stationary sources.

Revisions will also be made in LAC 33, Part ·111,

-1-

ACADIANA REPORTING SERVICE 9498 HOOPER ROAD

BATON ROUGE. LOUISIANA 70818

""041261 -9356
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Chapters 1, 15, 21, 25, and 29, so that referenced LAC

cites agree wi~h changes per this rule-making and to add

40 CFR references. These changes will expedite both the

EPA approval process, and State impl~mentation of

delegation of authority for the NSPS Program.

The NSPS and the authority for EPA to delegate

authority of that program to the State is established in

the Clean Air Act Amendments of 1990, Section 111. This

rule-making is applicable to stationary sources

statewide.

If the rule is not adopted, U. S. EPA must continue

to review each regulation, new and revised, in detail

for possible deficiencies prior to giving Louisiana

approval for delegation. This would significantly delay

the delegation of authority to implement the regulation

as adopted into Louisiana law.

Louisiana would also fail to meet its 1995-96, and

1996-97 EPA grant ob1ectives related to this rulemaking, and to delegation revisions. The State must

continue to print volumes of regulations that are not

significantly different from the federal regulations on

which they are based. An industry must continue to use

23 two sets of regulations which may contain only slightly

24 different recordkeeping and reporting requirements.

25 Our comments will begin with Richard Metcalf.

26 MR • METCALF.

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Good afternoon. My name is Richard Metcalf. I'm

the Health, Safety and Environmental Affairs Coordinator

for the Louisiana Mid-Continent Oil and Gas Association.

Mid-Continent is an industry organization which

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ACADIANA REPORTING SERVICE

94ge HOOPER ROAO

BATON ROUGE, LOUISIANA 70B18

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represents individuals and companies that together

produce, transport, refin! and market approximately 90

percent of the oil and"natural gas in Louisiana.

Virtually all of Mid-Continent members are affected by

the EPA and State New Source Performance Standards.

Mid-Continent strongly supports the Department's

strategy to adopt the federal rules by reference. We

• believe this strategy will provide efficiencies for both

the State and for industry in the implementation of

these regulations.

It is Mid-Continent's understanding that when the

Department adopts rules by reference, or these rules by

reference, the Department 'must also respect the

interpretations and guidance given by the EPA in any

formal preambles or background documents. Mid-Continent

would like for the Department to state this in the

response to comments.

Once again, Mid-Continent strongly supports the

adoption of this regulation and the opportunity to

provide these comments. Thank you.

HR. SKY-PECK.

~hank you. Does anyone else care to comment On

AQ145?

(No response.)

If not, the hearing on AQl45 is closed. I'd like

to thank you all for your attention and participation.

CERTIFICATE

1, MARGARET MORVANT, Certified Court Reporter, do

hereby certify that the foregoing testimony was heard

before the Honorable Steve Sky-Peck, Hearing Officer, on

-3-

ACADIANA REPORTING SERVICE 9498 HOOPER ROAO

BATON ROUGE. LOUISIANA 708' B

",041215 1·~356
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September 26, 1996, in Room 326, Maynard Ketcham

Building, Baton Rouge, Louisiana; that I did report the

proceedings thereof; that the foregoing pages, numbered

1 through 4, inclusive, constitute a true and correct

transcript of the proceedings thereof.

-4-

ACAOIANA REPORTING SERVICE

9496 HOOPER ROAD

SATON ROUGE. LOUISIANA 70616

"',0,",'211; I -9J56
Comments Submitted For

Incorporation by Reference - 40 CFR. Part 60

LAC 33:m.Chapters 1, 15, 21, 25, 29, 30, 31, 60

Log # AQI4S

-4',',--,

COMMENT #

1 and 2

SUBMIllJID BY

Richard Metcalf I L>uisiana MidContinent Oil and Gas Association
COMMENT 1:

RESPONSE 1:

COMMENT 2:

RESPONSE 2:

Comments Submitted For

Incorporation by Reference - 40 CFR Part 60

LAC 33:ID.Cbapters 1, 15, 21, 25, 29, 30, 31,-60

. Log # AQ145

General. The commentor supports the adoption of the regulation by

reference. The adoption of the regulation by reference reduces the

burden to implement these regulations because it reduces the amount

of time to prepare and review proposed amendments to the NSPS

regulations at the state level.

No response required.

General. It is suggested that the department confirm in the response to

comments that the department must respect the interpretations/guidance

given by the EPA in any formal preambles or background documents

associated with the rule being adopted. This clarification would ensure

that the department could not interpret a provision more strictly than

the EPA and impose costs to the regulated community in excess of the

EPA regulations.

The Department of Environmental Quality (DEQ) agrees to follow all

interpretations, past and future, made by EPA of 40 CFR part 60,

when part 60 standards are incorporated by reference and delegated

allthority by the straight delegation mechanism. A statement of such

agreement will be contained in the "Terms and Conditions" of the

delegation Agreement to be signed by EPA and DEQ.