M. J. "MIKE" FOSTER, JR. GOVERNOR

April 30, 1997

Ms. Jane Saginaw, Administrator U.S. EPA, Region 6 1445 Ross Avenue, Suite 1200 Dallas, TX 75202 Dear Ms. Saginaw:**~tat.e** 

### of 'lfioulEilana
OFFICE OF THE GOVERNOR

70804-9004 POST OFFICE BOX 94004 (504) 342-7015

The State ofLouisiana has approved and is submitting revisions to our State Implementation Plan (SIP). Enclosed are Louisiana's Revised Statutes and changes to LAC 33:IILChapters 1, 5, 15, 21, and 25. Also Chapter 30, which repeals Chapter 60, is being added for inclusion in the SIP. Five (5) copies showing that the rule revision went through the public notice process are attached. Please contact the Air Quality staff through Gus Von Bodungen at (504) 765-0102 if you have any questions. Sincerely,

# ~.\~. M.J. "Mike" Foster, Jr. 

### CJr Enclosures (5)

c: Mr. Thomas Diggs, EPA, Region 6

## COI\lTEI\lTS

Letter to Bob Hannah from Thomas H. Diggs dated.December 2, 1993
Louisiana Revised Statutes with revisions through the 1996 Legislative Session for Titles: 1) 36
2) 49 3) 30

4) 42 5) 44 Chapter 5-A Dept of Environmental Quality Chapter 24 Implementation of Reorganization Chapter 13 Administrative Procedure Subtitle II Environmental Quality Chapter 1 General Chapter 2 Dept of Environmental Quality Chapter 3 LA Air Control Law Chapter 15 Code of Governmental Ethics Chapter 1 Public Records**-~-** 

### •. AQ 145 Incorporation by Reference (LAC 33:III.Chapters 1, 15, 21, 25, 29, 30, 31, 60, 61, and 64)UNITED STATES ENVlfIOIIIENTAl. PHOIECTION AGENCY IlEGlON8 1415 ROSS "\/BlUE, SUITE 1200 IW lAS. TX 75202-2133



### 11·-·· C.,**~,'t3**



# ..... 

# .. 

# . Mr. 

### Bob RanMh.. Adalnl.trat.or Air**QUali~y** 

### Ilegul.atory Division t.<>uiai"""**Depart_n~** 

### Of Environ-ental**QUal1~y** 

### P.o. Box 

### 82135 

### Baton 

### 1lcu<I8. Louisiana 70884-2135 

### Dear

## Jfr~**B.nnah:~1-** This: lertar is:**~o** 

### conCi

... thn**~"e** 

### t.<>u18iana Daparaeat 

### of Knvlro

......tal**O,,"li~y** 

### _.**DO~** Deed to 

### inolude public**noUca/=-en~** 

### and public hurin9**cIocImcDta~OIl** 

### 10 ita**SUIa1~tal** 

### oC State**s~atutes** 

### as ravlsioD5 to. the State**.lJIplAaenta~ion** 

### Plan. Ka have d1scua...

### ect thh: tSctlCl with ReqlnMl eounae.l and bave 

### confiDed**~~** 

### the**le9lsla~lv8** 

### procaaa to reviee ..tatutua is functlonally equivalent to notice and ea-.ent. If you have any Ciuost.iona, plea••**cont:a~** .. At (214) 655-721.4 or 

### Jeanne McDaniela**a~** 

### (214) 655-7254. 

### sinceroly

### y~~ .



# - Je.. 400

# ~fl s ThOllas B.

## Di99~ Chief Planning Section (<<5T-AP)
ce:**ADne~~.** Sharp 

### t.<>uidana Departllent oC Bnvlronaent.al Quality



# 00138RULE RULE
artment ofEnvironmental Quality

Air Quality and Radiation Prate ion Air Quality Division
ent New Source Review Proc dUres AC 33:1II.504) (AQI46) ofthe LouisianaEnvir ental Quality et seq., and in acco dance with the provisions ofthe A inistrative Procedur Act, R.S.49:950 et se'!.., the secretary as amended the r Quality Division regulations, LAC 33:1 .504 (AQI46).

The deparnnent is a pting a provi on in the 1990 Clean Air Act amendments w ich provid for a special Rule for modifications ofsources itting I tons or more. Affected sources are any major s ionary ource ofvolatile organic compounds located in are which emits, or has the potential to emit, 100 to more of volatile organic compounds (VOCs) perye enever there is any change in emissions ofVOCs fro y discrete operation, unit, or other pollutant-emitting a IV at the source, such increase shall be considered a m ific ion fat purposes of Section I72(cX5) and" Section I (a). is Rule allows the o,wner or operator of the sourc to offse the increase by a greater. reduction in emission ofVOCs fr m other operations, units, or activities within e source at internal offset ratio ofat least 1.3 to I, in li ofthe requirem ts ofSection 173(a)(2) concerning the 10 est achievable eml sian rate (LAER), This revision is in a ordance with Sectio I82(c)(8) ofthe 1990 Clean Air Act endments. Title 33 NVIRONMENTAL QU Part III. Air Chapter

. Permit Procedures §504. N attainment New Source Reviel:rocedures 

# ... (See PriorTeX! in A-D.2] 3. Notwithstanding Subsection 0.2 of. is Section, in the c e oCany major stationary Source that emits or has the 

## I Gus Von Bodungen Assistant Secretary rcadlng of \ ,OOG 'P'Pm.., Qt %teater for**va(ves~** connectors, pressure relief devices, and process drains; 5;000 ppmv for pumps and compressors; or 10,000 ppmv for agitators, as outlined in Subsection 0 of this Section, when tested by Method 21 (40 CFR part 60, appendix A, as incorporated by reference at LAC 33:1I1.3003). 

## • •• [Sec PrIorText in C.l.b •G.6] AUTHORITY NOTE: Promulgated in accordance with R.S. 30:20R

.':JJSTORICAL NOTE: Promulgated by the Department of Environmental Quality, Office of Air Quality and Radiation Projection, Air Quality Division, LR 20:1102 (October 1994), rcpromulgated LR 20: 1279 (November 1994), amended LR 22: 1129 (November 1996), LR 22:1212 (DeCember 1996), repromulgated LR 23:197 (February 1997).

(EditO,.'" Nole: AQI4S was referenced

# IS. final Rule in the December 20, 1996, issue ofthe !tnlUUJM Reguter, The document provided to the Office ofthe Stale Registerc:ontained III incorrectversion of the Paragraph below. The corrected lext. as it should have appeared in AQI4S, is being published.) Title 33 ENVIRONMENTAL QUALITY Part UI. Air Cbapter 21. Control ofEmission of Organic Compounds Subcbapter A. General §2122. Fugitive Emission Control for Ozone Nonattainment Areas 

## ••• [See Prior Text in A

### ..c. I] a. No component in petroleum refineries, SOCMI, MTIlE, and polymer manufacturing industry shall be allowed to leak volatile organic compounds exceeding an instrument Department ofEnvironmental Quality Office ofAir Quality and Radiation Protection Air Quality Division Fugitive Emission Control for Ozone Nonattainment Areas (LAC 33:11I.2122XAQI45) }o / 3.-C. / AUTHORITY NOTE: Promulgated in accordance wilb R.S. 3:2093 and R.S. 3:2131.

HI ORICAL NOTE: Promulgated by lbe Departme of Agricult and Forestry, Livestock Sanitary Board, LR 1:234

, (March 19 ), amended LR**11:61~** (June**198~),** L 23:196 (February 19 ). §11717. Re uiring the Reporting ofContagi S Diseases

A. In order 0 improve the protection a e livestock industry from th ffects ofcontagious dise es oflivestock, all veterinarians 'censed in the state f Louisiana, are required to report the state veterin . , by telephone or wire, within 24 hou after diagnosis r tentative diagnosis, the OCCUTrence of su ected occ ence of the fa1I0wing contagious diseases: hog c era, anthrax, vesicular condition, scabies, equ e ephalomyelitis, pulloruml typhoid, pseudorabies, N Ie (OlE List A Diseases), Avian Influenza (OlE) st A Diseases), Ornithosis, Paramyxovirus (Other th weastle Disease), Infectious Encephalomyelitis, Inf! ious gotracheitis (other than vaccine induced), or yother d ease condition which may seriously threaten welfare of e livestock and poultry industry.

B.-E

.... AUTHORITY 3:2093, R.S. 3:

HISTORIC NOTE: Promulgated by lbe Department of Agriculture d Forestry, LouisianaLivestoc**11:61~** (J e**198~),** amended LR**1~:813** (Octo (May 19 ), LR 23: 197 (February 1997).



## )

-.' 197 Louisillnll**R~9"stll'** Vol. 13, No. 1**F~b,ullry** 10, 1997

# ,

RULE Gus VOn Bodungen Assistant**S~** RULE

Hermaa Robinson Assist&Dt secretary ency Response (LAC 33:1.691S) (OSIIA) Departmeat ofEDvlroDmeDtal Qnality Office ofthe 

### Secreta.,. 96121054

•A porIiaDoflbe RaIcwII1cII 

# 1IppCIIId"'_ uribe OCtober 1P96, LtIoIb-.6I*'is boIDI npoblisbed
• Lou_A_ Code cIadJoo ID 16915

.....) Title 33 ,,1\T\i'mONMENTAL QUALITY

Part Office ofthe Secretary Subpart4. E rcency Response**R~nlatlonl** Chapter 69. Emq cy Resprmse**R~oDl** §6915. Transportatlo Receipt, and**S~race** of 

## C Material from e Cleanup anror Abatement of aD Orr-slte Emer\ency**Cond~iOD** . A. Transportation, receip} aad**~ge** of aay material generated as a result ofthe**CI~P** dlor abatement ofaay off-site C1!!ergency condition, n specifically authorized by the LOtlIsIana Adminlstrat' 'ode, Title 33, Part V. Subpart I, may be authorized by administrative authority.

B. These regulatious supptim t aad do not replace requirC1!!ents of 49 CFR. I. 177 that remain ful1y applicable to the of nus materials.

AUTIIORITY NOTE: ulpled in co with R.S. 30:2011(0)(1),(14), ad (I

HISTORICAL NOTE: ulpled' by • Eovironmc:nlll Quality, oflbe Secretary, 1996), repromu1plcd :1212 (December I __..........__...... _ ..**~-W** ..._--. _d**:-pl~ft'l08n** ••t-:Oft 01' delegation ofautbority for the NSPS program. The NSPS and the authority forEPA to delegate authority ofthat program to the state is established in the Clem Air ActAmendments of 1m. Secticm III. This ru lC1!!aking Is applicableto stalill1W)' sources statewide.

.

The full text ofthis Rule may be obtained from the Office ofthe State Register. 1051 North Third Street, Baton Rouge, LA 70102.

96121Q62

Department ofEnvironmental Quality Office ofSolid and Hazardous Waste / Solid Waste Division Waste Tire (LAC 33:V1l.Chapler IOS)(SW021) \ ( 

### u fer the aulbority ofthe Louisiana Environmental Quality \ AC'l'::.S. 30:200 I el seq., and in accordance with the



### /

. 1212 lpJIloariD.&

... Plies 1124-**is~_bl_'"**

·or •.

Gus Von Bodungen Assistant Secretary "'rdaace with R.s. AccidemPrevention Pro C 33:IU.S901) (AQI2**~.,** .

It

## ::=:t~.:~~ C 

### orthil Seclion, the la 40 CFR. PIIt 61 (lui)' I. epartment ofEnvironmental QnaUty

ofAir Qnality and Radiation Protec • n Air QnaUty Division

..**.~.,** 

# ·\

RULE 96121010

Department ofEnvironmental Quality Office ofAir Quality and Radiation Protection Air QuaUty DIvIsJoD InCOlJlOration by RefereJlce (LAC 33:m.Chapten I, 15.21, 25.29,30.31,60.61 aad 64) (AQI4S) Underthe authority ofthe LouisiaDa EDvironmcIItal QuaIity Act, R.S. 30:2001 et seq
.. &ad in accordaDce with the provisioDS ofthe Administrative Procedure Act, R.S. 49:950 et seq., the Secretary has amended the Air Quality Divisioa reg1,l1atiODS, LAC 33:IU.Chaptc:rs I, IS, 21. 15. 29, 3D, 31, 60, 61 aad 64 (AQI4S).

This Rule repeals LAC 33:m.Chapters 31, 60 (except §6099 which is moved aad renumbered as LAC 33:III:2901.G), 61 (except Subchapter A which is moved aad renumbered as Subcbapter N in Chapter 21

## >, and 64 from LAC 33:III and incorporates by reference into Chapter 30 federal regulatioos in 40 CFR Part 60

- Standards of Performance for New Stationary Sources. Revisions are also made in LAC 33:II1.Chapters I, 15,21,25 and 29, so that referenced LAC cites agree wilb changes perthis rulemaking, and to add 40 CFR references. These changes w!1J expedileFINAL lWLE/DECEMBER 20, 1996 

### Tide 33 

### ENVIRONMENTAL QUALITY 

### partmAir

. Chapter 1. General Provisions 

### § 111. Definition. 

# ••• AQ145



## -,_ ..

# _-_

...

# _._-_
..._-,---
• (See 

### PriorTut] 

### Good

### Performance

### Level-an operating 

### 1eveI reac:bed when 

### no more than 

### two percent of the 

### valves inVOC service at 

### a W:ility are leaking at 

### a rate of10,000 

### parts per millionby volume (ppmv) or 

### greater as 

### determined by Reference

### Method 21 

### "Determination ofVolatile Organic 

### Compound 

### Leaks" in tileDivision's Sowee Testhfauuaf4Q CFR part 

### 60 appendix A. as iDCOQ)0rated by reference at LAC nW3003

.

# ••• [See 

### PriorTut] 

### PartiClllateMatterEmi,;:sjons-all 

### finely divided solid or liquid material, other than 

### uncombined water, emitted to the ambient air as 

### measured by

### Method 5 (SecLA:C 

### 33.m.6elS)in 40 

### CPR part 60 ap,pendjx A as ;ncp[porated 

### by reference at LAC

# nm 3003

. 

# ••• [See 

### PriorTut] 

### &ferenceMethod-any**m~hod** 

### of"sampling and analyzing for an air

### pollutant as descnbed 

### in die 

### Ail Quant) 

### Division's 

### Test Mllllmd40 CPR part 

## 60 lUlPendjx 

### A. as jnco[porated 

### by reference at LAC 

### 33·m 3003. 

# ••• [See Prior Tut] AUIHORITY NOTE: Promulgated 

### in accordance with R.S. 30:2054. 

### mSTORICAL NOTE: Promulgated by

### the Department ofEnviromnental Quality, Office ofAir 

### Quality and NuclearEnergy, Air 

### Quality Division, LR 13:741 

### (December 1987), 

### amended LR.14:348 

### (June 1988),LR 15:1061 

### (December 1989), 

### amended by the Office ofAir 

### Quality and Radiation Protection, Air 

### Quality Division, LR 17;777 (August 1991), LR21:1081 

### (October 1995), LR '

1FINAL RULE/DECEMBER 20, 1996 TIde 33 

### ENVIRONMENTAL QUALITY PartllLAir Olaptcr 15. EmissioD StaDdardJ (or SWf'ur Dioxide AQ145

§

### 1S03. £minionI.imitations 

### & used 

### in this 

### Section athru-hour avuagt

### means the 

### average emissions forany three consecutive 

### ooe-bourperiods (each 

### commencing on the hour), 

### provided that 

### the numberofthree

### hour

### perioda duringwhich the SOl limitation is exceeded is not greater than the number ofonehourperiods during

### whichthe 

## SOz limitation is exceeded. 

# ••• [See Prior

### TmiD A-D.%]

Particulate 1) Methods 1 

### tLAC 33.HI.68el). 2-(bA€ 33:B1:6863).3 (LAC 33.Hi6969). 4 33.HI:6EH3), S(L\C 33:HI:6e1S)(40 

### CfR 

### pan 60 appenglX A 1$ incorpD01ed by reference at LAC 33·m 3003) orb\€ 33:1H:3IIS§60 8 of40 CPR part 60 as inCOtWl'Jted by reference at LAC

2

### FINAL ROLE/OECEMBER 20, 1996 AQ145

Sulfur Oxides 1)

- Seidman, Analytical Chemistry Volume 30, page 1680 (1958),WOetennination 

### ofSulfur 

### Oxides in 

### Stack Gases.• 2) Shell Developmcm Company 

### method for theDetermination of

### sulfur Dioxide and 

### SulfurTrioxidePHS 999 AP-13 AppendixB, pages 85-87,
"Atmospheric Emissions Sulfuric Acid Manu&cturing-Processes " 3) Reich Testfor SulfurDioxide,
"Atmospheric Emissions from Sulfuric 

### Acid Manufacturing 

### Process" PHS 999 AP-13 A enoD( D, a es**7~0.** 4) The Modified Monsanto Company Method, "Atmospheric Emissions from Sulfuric Acid Manufacturing Process" PHS 999 AP-13, Appendix B. pages 61-67_ 5) Test Methods 1 (LA€33:1£ 6661), 2 (LAC 33.IH:6663). 3i1:*€**33.IH:6e6~.** 4 (LAC 33.IH.6913), 6 (LAC 33.ffi.66iS), and 8-(b't€ 33**.BI:6&4~** (40 CPR part 

### 60. appendix 

### A as iocOJ;poTlted b;y reference at

### LAC 33-m

### 30031. or b't€ 33:lH:311S§6O 8 o£40 

### CFR part 

### 60 as 

### incoQ)OI'ilted by reference at LAC

. 300.

3

### - 

### FINAL ROLE/DECEMB&R 20, 1996 AQ145

Oxides

# or Nitrogen 1) TestMethods 1 (LA:C 33.::i. :,061), Z (LA€33 :fH:6003), 3-(b\€ 33:HI:6OO9), 4 (LA€3J:m:6eIJ), and 7 (LAC 33:HL6e33)(40 CFR part 

### 60 append"nc A as 

## inm»orated by rcfcrcn<:e at

### LAC 33·m

### 300lt or b't€ 33:fH:3115§60 8 of4O 

### CfR part 

### 60 u incm:poratcd by rcferexw;c at LAC 33·m 3003. VlSloJe Emissions 1)
2)

Total Fluoride 1)



### Total Reduced 1)

Sulfur (TRS)
2) 

### . Methods 1 (LA€J3.Hl:6001). 2 (LAC 3J:HI::6OOJ). 3 (LAC 3J.Hi:6OO9). 13A (LA€33::HI:6e57) and**13B~** J3::H!:6eS9X40 CFR part 60 appcncf1X A 

## as jncorporated by o:feretlCC ot
Method 16 (Ur:€JJ:HI:606S)(40 

### CFR part 60 aPllCDdjx A pr 660 8 ofCFR Part 

### 60 U incorporated by

### referencC at LAC n·m 3003) 01 LA€33:IH:311S. Coulometric titration by method specified in NCASI Atmospheric Quality Improvement Technical Bulletin Number 91. anu 1978

4**F~** ROLE/DECEMBER 20, 1996 AQ14S

Sulfuric Acid Mist 1) Test methods 1 (LAC 33:HI:6ee1). 2 (LA:C 33**.IH:6oe3~ 3~**  33:HI:6009), 4 tLAC 33iH:6613}. 6 (LAC 3J.IB:682Sh and**a~** 33.ffi:6&4S) (40 

### CPR pArt 

### 60. appendix A or tOO 8 ofCFB, Part 60 as incoQ)Ql'8ted by reference M LAC

AUTHORITYNOTE: Promulgated accordance with R..S. 30:2054. HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality. Office ofAir Quality and Nuclear

### Energy. Air Quality Division, LR 13:741 (December 1987). amended by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 18:374 (April 1992). LR §lS11.. Continuous Emissions Monitoring 

# ••• [See PriorTat iD A] B. These measurement systems shall be certified according to the performance specifications 

### in LAC 33:HI:618S (performance Specification2) (40 CFR pan 60 appendix B as incorporated by [ere! en" at LAC 33·m 3003) and quality assured by 

### the procedures in 40 CFR 60, appendix "F". 

# •

# ••

. (See PriorTw in C] AUTHORITYNOTE: Promulgated in accordance with RS. 30-.2054. IDSTORICALNOTE: Promulgated by the Department ofEnvironmentaJ Quality. Office ofAir Quality and Radiation Protection, Air Quality Division, LR 18:375 (Apri11992). amended 

### LR

S

### FrNAL RULE/DECEMBER 20, 1996 TIde 33 ENVIRONMENTAL QUALITY 

### Part

## m. Air Chapter 

### 11. Control orEmission orOrganic Compoundl SubchapterA-Geaenl 

### §1103. Storage orVolatile Organic Compoundl 

# ••• AQ145



### [See PriorTest la 

### A-IU)

. L 

### Test Methods 1-4 (LAC 33.BL6991, 6ge3, 6999 and 6913, rcspeeti,ely4Q 

### CFR part 

### 60 IPpendix A 15 incm:pprated 

### byreference llt LAC 

### 33-m 3003) ror determining flow rates, 

### as necessaJy, b. Test 

### Method 18 (LAC 

### 33.BL69714Q 

### CFR part 

### 60 IPpendix 

### A. as 

### inco!]20rated by reference It LAC 

### nm 3OOJ) for measuring 

### gaseous organic compound emissions by 

### gas chromatographic analysis; 

### c. Test Method 21 (LAC 33.m.69?14Q 

### CFR part 60. appendix 

### A. 

## as jncolJ)orated 

### by reference 

### at LAC 

### JJ·m JQQJ) ror determination orvolatilc organic compound leaks' 

## , d. Test Method 25 (LAC 

### 33.m.69S54Q CFR 

### part 

### 60 Allpendjx 

### A. IS jnColJ)oratedby reference 

### at LAC 

### JJ'm JQQ3) ror detcnnining total gaseous norunethanc organic**emissi~as~~** 

### . 

# ••• [See 

### PriorText in B.1.c-L5) AUlHORITYNOTE: Promulgated 

### in accordance with R.S. 30:2054. HISTORICALNOTE: Promulgated

### by the Department orEnvirorunental Quality, Office or

### Air Quality 

### and NuclearEnergy, 

### Air QualityDivision, LR 13:741 (December 1987), amended, LR 

### 15: 1061 (December 1989), amended by the Office or

### Air Quality 

### and Radiation Protection, 

### Air Quality Division, LR 17:360 (April 1991), LR 18:1121 (October 1992), LR20:1376 (December 1994), LR 21:1223 (November 1995), repromulgated LR 21:1333 (December 1995), amcndedLR §2107. Volatile Organic Compounds

- Loading 

# ••• [See Prior Text in A-E) 1. Test Methods 1-4 (LAC 33:m 6091 6003 6899 Aod 6113 icspCCtiydy4Q CfR 

### Ilart 60 appendix A. 

### as jnco(poTated 

### hy reference at LAC 

### 3J·m 3003) ror determining flow rates, 

### as necessary; 2. Test Method 25 (LAC 

### 33.m.6eS540 

## crn part 60 appendix A 

### as jncolJ)oraled by 

### reference at LAC 

### JJ'lU 300J) ror determining total gaseous norunethane organic emissions as 

### carbon. 

# ••• 6

### FrNAL RULE/DECEMBER 20, 1996 AQ145 

### [See

### Prior Ten 

### in F] AumORITYNOTE: Pronmlgated ill accordance withlLS. 30:205"4. HISTORICALNOTE: Promulgated 

### by the 

### Department ofEnviionrnental Quality, Office of

### Air Quality 

### IIIdNuclear

### Energy, QualRyDivision, LR.13:741 (December 1987), amended 

### LR. 16:116 (February 1990), 

### amended by the Office of

### Air 

### Quality and Radiation Protection, LR. 17:360 

### (April 1991), 

### LR.

. 12101. Marine VaporRecovery 

# ••• [See

### PriorTen 

### in A-E.l.a] 

### i. Method 2B (40 

### CFR part 60 appendjx A 8$ 

### inC0W9rated by 

# remenee atLAC

# nm 3003) for combustionvapor processing systems 

### (except flare stacks). 

### it Method 2A (40 

### CFR part 6Q 

### appendjx A. 

### as incorporated by 

### refelenee at LAC 33·m 

### 3003) for

# an othervapor processing systems.' b. for the determination oftotal organic compounds concentration at the exhaustvent, Method 2SA or 25B (4Q 

### CFR part 6Q 

### appendjx!L as incorporated by 

### reference at LAC

# 33·m 3003). The 

### calibration gas shall 

### be either propane orbutane

. 

# ••• [See PriorText in £.2] 

### 3. Immediately priorto the performance test for determination ofcompliance, 

# an potential sources ofvapor leakage in the**faci1ity'~** 

### vapor collection system equipment shall be monitored for 

### Ieab using Method 21 (4Q 

### CFR part 60 

### appendix A. 

### as incorporated by 

### reference at LAC 33'1U 3003). 

### The monitoring shall be conducted only while a ship orbarge is being loaded and should cover

# an parts oflhe vapor system, including tank 

### hatches, that operate at pressures above atmospheric pressure. All leaks 

### shall be repaired prior to conducting the performance test. 

# ••• [See PriorText 

### in E.4-4.g] 

### 5. The owner or operator may adjust the emission results to exclude the methane and ethane content ill the exhaustventby the chromatographic methC':! shown inMethod**25~** 

### CFR part 6Q 

### lwendix A 

### as incorporated by 

### reference 

### at ',AC 

### 3J'W 3003) 

# ••• [See PriorText in F-H.2] AUIlIORITY NOTE: Promulgated ill accordance with lLS. 30:2054. mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office ofAir 

### Quality and Nuclear Energy, Air 

### Quality Division, LR 14:704 (October 1988), amended by the Office ofAir 

### Quality and Radiation Protection, Air 

### Quality Division, LR 16:959 (November 1990), LR §2109. OillWater-Separation 

# ••• [See Prior Text in A-q 7

### FrNAL RULE/DECEMBER 20, 

### 1996 AQ145 

### 1. Test MethocM-4 (LA:C 33.m.6991, 6993, 6999 /Iud 6913, Itspeetivcly40 CFR part 

### 60 aPPendix A. as jnccitporated by metence 

### at LAC 

## :n'm 3003) for dctcnnining tlow rates, 

### u necessary; 2. Test Method 18 

### Q;;h€33.HL697140 CFR Par160 appendix A. 

## as incorPorated by reference at LAC

# um 3003) for 

### measuring gaseous organic compound emissions 

### by &IS 

### chromatosraPhic analysis; 3. Test Method 21 

### (LM; 33.HL69mO CFR part 60 apPenA;v A as incOJ:porated by reference at

### LAC 33·m 3003) for determination ofvo1atile**or&~",;.:** cor.**:,~** ..

### nd lcaIcs;

• 4. Test 

### Method 25 (LA:C 33.HL69SS40 CFR part 60 allP ,djx A as incorporated by reference 

### at LAC 33·m 3003) for determining 

### total gaseous nonmetha:.e organic emissions as 

### carbon; 

# ••• [See PriorText la <:.5-D.3] AUIHORlTYNOTE: Promulgated in accordance with R.S. 30:2054. lnSTORICAL NOTE: Promulgated 

### by 

### the Department 

### ofEnvironmcntal Quality, Office ofAir Quality and NuclearEnergy, Air Quality Division, 

### LR 13:741 (December 1987), amended 

### LR 16: 117**(Fe~ruary** 1990), amended 

### by the Office ofAir Quality and Radiation Protection, Air Quality Division, 

### LR 16:959 (November 1990), 

### LR 17:360 (Apri11991), 

### LR 18:1122 (October 1992), 

### LR 

### §211S. Waste Gas Disposal 

### Any wute 

### gas disposal stream containing organic compounds from any emission source including those emissions from process unit upsets, start-ups and shutdowns shall be controlled by one ofthe following methods: 

# ••• [See 

### PriorText in 

### A-I] 1. Test Methods 1-4 (LAC 33.m.6991, 6993, 6999, aud 6913,**Itspcctive1)~** 

### CPR part 

### 60 appendix A. as incorporated byreference at J,AC 

### 33'm 3003) for determining tlow rates, as 

### IIcccssary; 2. Test Method 18 (LAC 33.m.697140 

### CFR part 60 apPendix A as jncorporated by reference 

### at J,AC 33·m 3003) for determining gaseous organic compounds emissions by 

### gas chromatography; , 3. Test Method 25 (LAC 33.m.69SS40 

### CFR part 60 apPendix A as incorporated by reference at LAC 33·m 3003) for determining total gaseous nonmethane organic emissions as carbon; 4. Test Method 25A or 25B (LAC 33 .m.6986 01 668740 CPR part 60 appendix A. 

## as incorporated by reference at LAC 33·m 3003) for detennining total gaseous orgailic

. concentration usingtlame ionization or nondispersive infrared analysis; and 

# • 

# • • [See 

### Prior Text in L5-L] AUIHORlTY NOTE: Promulgated in accordance with R.S. 30:2054. mSTORICAL NOTE: Promulgated by the Department ofEnvironmentaJ Quality, Office 

### 8FrNAL RULE/DECEMBER 20, 1996 AQ145

• 

### ., of

### Air Quality and Nuclear Energy, 

### Air Quality Division, LR 13:741 (December 1987), amended by 

### the Office of

### Air Quality and Radiation Protection, 

### Air Quality Division, LR 16:959 (November 1990), LR 17:654 (July 1991), LR 18:1122 (October 1992), LR 19:317 (March 

### 1993),LR

. §1116. Glycol Debydraton 

# ••• [See Prior Text ia A-D.3] 4. conventional stack measurements using 

### Lz\€ 33.HI.•68'i'1 and 6885**~ethods** 18 

### and 2S (40 CFR part 60 appendix 

### A. as incorporated by reference at LAC 

### nill 3003) for determining volatDe organic compound emissions; or 

# ••• [See Prior Text 

### ia D.5-G.2] AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054. HISTORICAL NOTE: Promulgated by the Department of Environmental Quality, Office

. of

### Air Quality and Radiation Protection, 

### Air Quality Division, LR 20: 11 06 (October 1994), repromulgated LR 20: 1279 (November 1994), amended LR 21 :941 (September 1995), LR 

### §1111. Fugitive Emission Control 

# ••• [See PriorText in A-B) 1. No component shall be allowed to leak organic compounds exceeding 10,000 parts per million by volume (ppmv), as defined in LAC 33:m.ll1, when tested by Method 21 "Determination ofVolatile Organic Compound Leaks" in the Division's SOUl ee Test Manual 

### ('LIte, 'folume 12!)40 CFR part 60 apPendix 

### A. as incorporated by reference at LAC 

### nill 3003. Anyregulated component observed leaking by sight, sound, or smell must be repaired according to 

### Lz\€ 33.HI.2!I2!1.Subsection B.3 ofthjs Section. regardless of the leak's concentration. This includes flange and coMection leaks found perLAC 33.Hl:2!I2!l.Subsection C.3.b ofthis Section. pump and compressor 

### seal leaks found during the weekly visual inspections, and other regulated component found leaking. 

# ••• [See Prior Text in B.2-G] AUTIiORITY NOTE: Promulgated in accordance with R.S. 30:2054. HISTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office ofAir Quality and Nuclear Energy, Air Quality Division, LR 13:741 (December 1987), amended by the Office ofAir Quality and Radiation Protection, Air Quality Division, LR 16:959 (November 1990), LR 17:654 (July 1991), LR 21:1330 (December 1995), LR 

### §2122. Fugitive Emission Control for Ozone Nonattainment Areas 

# ••• [See Prior Text in A-A.6.d) B. Definitions. Terms in this Section are used as defined in LAC 33 :III.lll with the 9

### FXNAL ROLE/oECEHBER 20, 

### 1996 Cltccption ofthose terms speci1ic:aUy defined below 

### as foDows: 

# ••• AQ145



### [See PriorTest] 

### Good 

### PerjorlnanuLneI-atJ. operating level reached when 

### no more than 

### 2.0

... pa-c:ent 

### oca componentin YOCaervic:e 

### in • 

### process unit 

### are leaking at 

### the leakrate !fetinition or

greater

### as determined by

### LAC 33.BL6811 (Refb dICe

### Method 21, "Determination ofVolatiJe Organic CompoundLeaks" (40

### CFR Plrt 

### 60 l])Jlendix!L IS 

### incon'QrJted by

### reference at LAC 

# n m 3003). 

# •

# •• • 

### [See 

### PriorTest 

### In B.Bea"YlJquid Service

- C.l] L 

### No component 

### in petroleum refineries, 

### SOCMJ. MTBE, 

### and polymer manuflu:turing industry 

### sbaJl be 

### allowed 

### to leakvolatile organic compounds CltCeed:ng an instrument 

### readin..l2f1,000**5~~** 

### forvalves, 

### connectors, pressurereliefdevices, process drains,

### ~;r 

## V81Yes and

# :=5,000 ppmvfor pumps and compressors; or 10,000 ppmv foiagitators In 

### Su on D ofthis Section, when tested by

### I::JIte 33.m.6811**~ethod** 

### 21 (40 CFR 

### part 60 

### apPendix!L IS 

### ineon'Qrated 

## In' reference at I A.C 

# n m3

### OO3). b. No component in natural gas 

### processing plants shall 

### be allowed to leakvolatiJe organic compounds Cltc:eeding an instrument reading offof2,500 ppmv forvalves, connectors, pressure reliefdevices, process drains, 

### and open-ended valves and lines; 5,000 ppmv for pumps and compressors; or 10,000 ppmv for**agi~ors** 

### as outlined in Subsection D ofthis Section, when tested by 

### LAC 33.m.6811 (Method21 (40 CFR 

### part 60, appendix A 

### as incorporated by 

### reference at LAC

# nm 3OOJ)

. 

# ••• [See PriorTest in C.l.c-G.Ii] AUlHORITYNOTE: Promulgated in accordance withll.S. 30:2054. 

### mSTORICALNOTE: Promulgated by the Department ofEnvironmentaJ Quality, 

### Office ofAir 

### Quality and 

### Radiation Protection, Air Quality !:'ivision, LR 20:1102 (October 1994), repromulgated LR 20:1279 

### (November 1994), amended LR SubchapterB-Organic Solvents §2113. Organic Solvents 

# ••• [See PriorTest in 

### A-E) 1. 

### TestMethod 24 (LAC 

### 33.1H.668340 CFR 

### part 60 appendjx A as incorporated by 

### reference at LAC 

### JJ,m JOOJ) with a one-hourbake;

. 2. TestMethod 1-4 (LAC 

### 33.m.688l, 6663, 6669 and 6813, rCSpCCbYeIy£)..cEB. 

### part 60 appendix!L as incon'orated 

### by reference at LAC 

### um JOOJ) for determining flow rates; 3. Test Method 18 ( (LAC 33,m,66714Q CFR 

### part 60 appendix!L as incorporated by 

### reference 

### at LAC 

### JHiI J003) for measuring gaseous organic compound emissions by gas chromatographic analysis;

. 4. TestMethod 25 (LA€ 

### 33.HI.66854Q CFR 

### part 60 appendix A. 

### as jncorporated 10

### FrNAL RULE/DECEMBER 20, 1996 AQ145 by

## reference al LAC 33·m 3oo:t) for detennining total**~us** nonmethane organic emissions 

## as carbon;

. • 

# •••

. [See PriorText 

### ia E.5-F.4]

- . AtrrHORlTYNOTE: Pronwlgated 

### in accordance with R.S. 30:2054. lUSTORICALNOTE: Promulgated by the Department ofEnvironmental Quality, Office orAir 

### Quality andNuclear

### Energy, Air Quality Division, LR 13:741 (December 1987), amended LR 16:119 (February 1990). 

### amended by the Office or

### Air Quality and Radiation Protection, 

### Air Quality 

### DiVision, LR 17:654 (July 1991). LR 18:1122 (October 1992). LR 22:340 (May 1996), 

### L1l 

### Subchaptere-VaporDegreasen §2115. VaporDegreasen 

# ••• [See PriorText 

### ia A-E) 1. 

### A5l1d TestMethod D323-82 ror detennining Reid vapor pressure; 2. Test Methods 1-4 

### (LA€33.fH.6661, 6663, 6669 and 661340 CfR part 60 appendix A. as inCO[porated 

### by reference at LAC 33·m 3003) for detennining flow rates; 3. TestMethod 18 

### (LA€33.fH.667140 

### CFR part 60 apPendix A as incorporated 

### by reference at LAC 33·m 3003) for detennining gaseous organic compound emissions by gas chromatography; 4. Test Method 25 

### (LA€33.fH.66S540 CfR part 60

.apPendjx A. as incorporated by

## reference at LAC 33·m 3003) for detennining total gaseous nonmethane organic emissions as 

### carbon. 

# ••• [See Prior Text in F-G] AtrrHORlTYNOTE: Promulgated 

### in accordance with R.S. 30:2054. lUSTORICALNOTE: Promulgated by theDepartment ofEnvironmental Quality, Office ofAir Quality and Nuclear

### Energy, Air Quality Division, LR 13:741 (December 1987), amended 

### by 

### the Office of

### Air Quality and Radiation Protection, 

### Air Quality Division, LR 16:959 (November 1990), LR 18:1122 (October 1992), LR Subchapter E-Percbloroetbylene 

### Dry Cleaning Systems §2129. Percbloroethylene 

### Dry Cleaning Systems 

# ••• [See Prior Text in**A~q** 

### . 1. TestMethods 1-4 (LAC 33.fH.6661, 6663, 6669 and 6613, iCSPCCtively1Q. CPR part 60 appendix A. as incorporated by reference at LAC

# nm 3003) for determining flow rates, as necessary; 2. Test Method 18 (LAC 33.ffi.667140 CfR part 60 appendix A as incorporated by reference at LAC 33·m 3003) for measuring gaseous organic compound emissions by gas chromatographic analysis; 11

### FINAL RULE/DECEMBER 20, 

### 1996 AQ145 

### 3. TestMethod 21 (LA€33.Hi:697740 CFR part 60 appendjx A as jnCOO!0rated by

### refele,,'r at LAC

# nm 30(3) for 

### determination ofvo1atile organic compounds 

### leaks; 4. TestMethod 

### 2S (LA€33.Hi:698S40 CFR part 60 appendix 

## A. as inCOO!orated by

### reference at LAC 33·m 

### 30(3) for determining total 

### gaseous nonmethane organic emissions as 

### carbon; 

# ••• [See PriorTest In c.5-D.3] AUlHORITYNOTE: Promulgated in 

### acc:ordance with 

### RS. 30:2054. HISTORICALNOTE: Promulgated by the Department ofEnvironmental Quality, Office of

### Air

## Quality and NuclearEnergy, 

### Air Quality Division, LR 13:741 (December 1987), amended by the Office of

### Air Quality 

### and Radiation Protection, 

### Air Quality Division, LR 16:959 (November 1990), LR SubchapterF-Gasoline Handling 12131. Filling orGasoline Storage Vessels 

# ••• [See PriorTest In A-E] 1. TestMethod 27 (LAC 33.HI.698940 

### CFR Part 60 appendjx A as jncm:pprated by

### reference at LAC 33"1II 3003) for detennination**of~por** 

### 'ftightness of6&uoline Bdelivery 

### lftanlcs 

## eusing**PIl~um** 

### lftesl. 

# ••• [See PriorTest in E.2] 3. Test Method 21 (LA€33.Hi:69'i'740

# em part 60 appendjx A as jncorpprated by

### reference at LAC 

### 33·m 30(3) for determination**of~olatile** 

### 6prganic**~mpound** f:leaks

. 

# ••• [See PriorTest in F-G] AUTHORITYNOTE: Promulgated.in accordance with RS. 30:2054. mSTORICAL NOTE: Promulgated by the Department of Environmental Quality, Office of

### Air Quality 

### and NuclearEnergy, 

### Air Quality Division, LR 13 :741 (December 1987), amended LR 16:609 (July 1990), amended by the Office of

### Air Quality and Radiation Protection, 

### Air Quality Division, LR 17:654 (July 1991), LR 18:1122 (October 1992), LR 19:1564 (December 1993), LR §2133. Gasoline BulkPlants 

# ••• (See PriorText in A-D.l] 2. Test Method 21 (I::AC 33 .HI.6B'i''i'40 

### CFR part 60 appendlx"A; as jncQl;p6ra.ted by 

### reference at LAC 33·m 

### 3003) for determination**of~olati1e** 

### 6prganic €kompoundf:leaks; 

# ••• (See Prior Text in D.3-F] AUTHORlTY NOTE: Promulgated in accordance with R.S. 30:2054. 

### mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office 12

### FINAL RULE/DECEMBER 20, 

### 1996 AQ145 

### ofAjr 

### Qua1ity 

### and NuclearEnergy, Ajr 

### Quality 

### Division, LR 13:741 

### (December 1987), 

### amended, LR 16:610 

### (July 1990), 

### amended by 

### the 

### Office ofAjr 

### Quality 

### and Radiation Protection, Ajr 

### Quality Division, LR21:SS2 (June 1995). LR 11135. BulkGuoline Terminals 

# ••• [See PriorTest 

### iD 

### A-D) 1. TestMethoda 1-4 (LAe 

### 33.Hl:6981, 6883, 6889 aud 6813,lespeeti.e!)!ll CFR part j;o 

### awendjx A as incorporated by

### reference at 

### I e\C 

### J3'm 3003) 

### for determining flow 

## rates. u 

### necessary; 2. TestMethod 18 

### (LAe 

### 33.Hl:69"f4Q CFR part 60 IPJ)CI!d"1X 

### A M 

### inGQTJl0rated by

### reference 

### atLAC**~:l·m** 3003) 

### for measuring 

### gaseous organic compound emissions by 

### gas 

### chromatographic 

### analysis; 3. Test 

### Method 21 

### (LAe 

### 33.1H:69"'i'40 CFR part 60 apPendjx A as inGQTJlorated by 

### reference at LAC 33·m 3003) 

### for determination ofvolatile organic compound leaks; 4. TestMethod 25 (LA<: 

### 33.m.69S540 CFR part 60 appendjx A as incorporated by 

### reference 

### at LAC 33·m 3003) 

### for determining total gaseous nonmethane organic emissions as carbon; 

# ••• [See Prior Text 

### in D.5-E.5.c) AUTHORITY NOTE: Promulgated in accordance with R.S. 30:2054. 

### mSTORICAL NOTE: Promulgated by the DePartment ofEnvironmental Quality, 

### Office ofAjr 

### Quality and NuclearEnergy, 

### J.Jr Quality 

### Division, LR 13:741 

### (December 1987), 

### amended LR 16:609 

### (July 1990), 

### amended by the Office ofAjr 

### Quality 

### and Radiation Protection, Ajr 

### Quality 

### Division, LR 17:654 

### (July 1991), 

### LR 18:1123 

### (October 1992), 

### LR §2137. Gasoline Terminal Vapor-Tight Control 

### Procedure A 

### Gasoline TankTrucks 

### 1. Testing 

### Procedure. 

### Gasoline tank trucks and theirvapor collection systems 

### shall not sustain 

### a pressure change ofmore 

### than three inches ofwater (0.75 

### \cPa) in five minutes when pressurized to 18 

### inches ofwater (4.5 

### Kpa) or evacuated to 

### six inches ofwater (1.5 

### Kpa) using the 

### test ploceduiC 

### dCSCiibed it•.Im.Method 27 ofd" D;;isiou's 

### SOUlee Test**!wfailU~** 

### CPR Part 

### 60 lijlPendix A as incQrporated by 

### reference at LAC 33"1U 3003) 

### fQr detenninatjQn Qf vapor tightness QfBaSQUne deliyery tanks usjnB pressure-vacuum test
. 

# •••

13FINAL RULE/DECEMBER 20, 1996 detmnjDntion 

### peyo1att1, Qrpnic; compoynd 1eikS of

### tit, c10CWUUlt I

## eraeileed 

### in 

### U£

. 33:H1:2131.Al. • . 

# •••**~145**



### [See PriorTest III B.2-D]

.. . . AurHORlTYNOTE: 

### Promulgated 

### in accordance with

### ll.S. 30:2054. 

### lfiSTORICALNOTE: Promulgated by 

### the Department ofEnvironmental 

### Quality, Office ofAir 

### Quality and Nuclear

### Energy, Air 

### Quality Division, 

### LR. 13:741 

### (December 1987), 

### amended LllI6:609 (July 1990), 

### amended by 

### the Office of

### Air Quality and Radiation Protection, 

### Air QualityDroaoll, 

### LR. SubchapterB-Gnphic Arts 

### 11143. 

### Gnphic Arb 

### (PrIndn&) by Roto&nvuft and F1exo&nphic Processes 

# ••• [See PriorText 

### ill A.q 1. 

### Test Method 24 

### (fA.C 33.HL66834Q 

### CFR part 60 

### appendjx A 

### as jncQlJlorateci by 

### reference at LAC 33·m 3003) 

### for determination ofvolatile matter content, water content,
. densityvolume solids 

### and weight ofsolidS; 2. 

### Test Methods 1-4 

### (LAC 33.m.GSSI, 6SS3, 6SS9 

### and 691340 

### CPR part 60 

### appendjx A. 

### as jncolJlorated by 

### reference at LAC

# nm 3003) 

### for determining flow rates; 3. 

### Test Method 25 (LA€33.HL6S8540 

### CFR part 60 

### appendix A 

### as jncolJlorated by 

### reference at LAC 

## 33·m 3003) for detennining total gaseous nonmethane organic emissions as carbon; 

### and ' 

# ••• (See PriorText in 

### C.4-D.3] AurHORITY NOTE: Promulgated 

### in accordance with R.S. 30:2054. 

### mSTORICAL NOTE: Promulgated by the 

### Department ofEnvironmenta1 Quality, Office of

### Air Quality and Nuclear Energy, Air 

### Quality Division, 

### LR. 13:741 

### (December 1987), 

### amended by the Office ofAir 

### Quality andRadiation Protection, Air 

### Quality Division, 

### LR. 16:959 

### (November 1990), 

### LR. 18:1123 

### (October 1992), 

### LR. Subchapter**~Pharmaceudcal** 

### Manufacturing FacUities §1145. 

### Pharmaceutical Manufacturing FacUities 

# ••• [See PriorText in A-F. 1] 2. 

### Test Methods 1-4 (LA€33.m.GSSI, 6SS3, 6999 

### mid 691340 

### CFR part 60 

### appendjx A. 

### as jncolJlorated by reference at LAC nm 3003) 

### for**df~ermining** 

### flow rates; 3. 

### 'TeStMethod 18 (LAC 33.ffi.6S7140 CFR 

### part 60 

### appendix A. 

### as jncorporated 

### by reference at 

### LAC 33"IU 3003) 

### for determining gaseous organic compound emissions by gas chromatography; 4. 

### Test Method 24 

### (LAC 33.m.688540 

### CFR part 60 

### appendix A as jncolJlorated 

### by reference at LAC 33·m 3003) 

### for determining total gaseous nonmethane organic emissions as carbon. 

### 14

### FrNAL RULE/DECEMBER 20, 1996 AQ145 

# ••• (See PriorTat ill 

### G-G.41 AUIHORITYNOTE: Promulgated in 

### accordance with R.S. 30:2054. HISTORICALNOTE: Promulgated by the Department ofEnvironmental Quality.Oflice ofAir 

### Quality 

### and Nuclear

### Energy, Air 

### Quality Division, LR 13:741 (December 1987), amended by the 

### Office ofAir

### Quality and Radiation Protection, Air 

### QualityDivision, LR 16:959 (Novanber 

### 1990). Subchapter I. 

### LimitinC Volatile Orpnic Compound (VOC) Emissions from Reactor Processes and Distillation Operations ill 

### the Synthetic Orcanic Chemical ManufacturiDc IDdumy 

### (SOCMI) 

### §2147. LimitinC VOC Emissions from SOCMIReactorProcesses and Distillation Operations 

# ••• (See 

### PriorText ill 

### A] B. Definitions. Unless specifically defined inLAC 33:m.lll, the tenns in this Subchapter 

### shall have the meanings commonly used in the field of

### air pollution control. Additiona1ly, 

### the following meanings apply, unless the context clearly indicates otherwise

. 

# ••• (See PriorText] Halogenated Vent Stream-any 

### vent stream containing a total concentration of halogen atoms (by volume) contained in 

### halogenated organic compounds of2oo ppm by 

### volume or greater determined by using LAC 33.1H.58?! (Method 18 (40 CFB part 60 IIppendix A IS 

### jncorporated by 

### reference at LAC 

### 33·m 3003) or other test or validated data by 

### the United States Environmental Protection Agency's (EPA) Method 301 of 40 CFR part 63, appendix A, 

### or by engineering assessment or process knowledge 

### that no halogenated organic compounds are present. Forexample, 150 ppm by volume ofethylene dichloride would contain 300 ppm by volume oftotal halogen atoms. 

# ••• (See PriorText] 

### Total Organic Compounds (7OC)-those compounds measured according to the procedures ofLAC 33.1H.58?! (Method 18 (40 CFR Pllrt 

### 60 IIppendix A IS 

### jncorpoCl!ted 

### by reference It LAC 33·m 

### 3003), for the purpose ofmeasuring molar composition as required in SubsectionD.5.b ofthis Section, hourly emission rate as required in Subsection D.2 and 5.d of this Section, and TOC concentration as required in Subsection F.l.d and 2 ofthis Section. The definition ofTOC excludes those compounds that the-administrative authority· designates as having negligible photochemical reactivity as listed in 40 CFR 51.100(5). 

# ••• (See Prior Text] C. Control Requirements 

# ••• (See Prior Text in C.I-D.3] 

### 15

### FrNAL RULE/DECEMBER 20, 

### 1996 AQ145



### basis, ppm by

### volume. L 

### LAC 33.&6991**~ethod** 

### 1 (40 CFR part 60 appendjx A as iDcOl;porated 

## bYreference at LAC 

### um 3003) orLAC 

### 33.&6992 (Method lA (40

# em pan 60 appendix A. U 

### inCOQlOTllted 

## bY reference at LAC 

### um 3003), as appropriate, shaD be used for selection ofthe 

### sampling sites. The 

### control device inlet sampling site 

### for determination ofvent stream 

### molar composition orTOC (less 

### methane and ethane) reduction 

### efficiency_shaD be 

### located afterthe 

### last RJ:,Overy device but prior to 

### the inlet ofthe control device, priorto any 

### dilution of the 

### process vent

# stream. and priorto 

### release to the 

### atmosphere. b. LA€

### 33.&6993**~ethod** 

### 2 (40 CFR Part 60 appendix A as iDCO!Jl0rated by

### reference at LAC 

### 33·m 3003), LAC 

### 33.&6995**~ethod** 2A 

### (40 CfR 

### part 60 

### appendix 

### A. as iDCO[pOrated by

### reference at 

### LAC 33·m 3003), 

### LAC 33.m.6996**~ethod 2C~**  

## CFR part 

## 60 appendix A 

### as iDcotPPTated 

## bYweren!.'t at LAC 

### urn 3003), or

### LAC 33.Hl:6998 (Method 

### 2D (40 CfR 

### part 

## 60 appendix A. 

### as inco!J)Ojated 

## bY reference at I,AC 

### 33·m 3003), as appropriate, shaD be used 

### for determination ofthe 

### gas stream 

### volumetric flow rate.

. c. 

### The emission rate correction factor, integrated sampling and 

### analysis procedure 

### of LAC 

### 33.&6989**~ethod** 3 

### (40 CFR 

### part 

## 60 appendix A. 

### as ;nco!J)0rated by 

### reference at LAC 

### 33·m 3003) shaD be used 

### to determine the oxygen concentration (''100U> 

### for the 

### purpose ofdetermining compliancewith the 20 ppmby volume limit. The sampling site sba11 be the same as that 

### for the TOC samples, 

### and samples shaD 

### be taken during the same time that 

### the TOC samples are taken. The TOC concentration corrected to three percent oxygen (C.) sba1l be computed usingthe following equation: C = 

### C % 

### 17.9 roc 

### 20.9

- % 

### 0211
where: C. = 

### Concentration ofTOC (minus methane and ethane) corrected to three 

### percent dry 

### basis, ppm by

### volume. 

## Croc = 

### Concentration ofTOC (minus methane and ethane), dry 

### %

.. 

### Concentration ofoxygen. dry basis, percentby volum!". d. LAC 

### 33.m.69'T1**~ethod** 

### 18 (40 CfR 

### part 60 appendix A U 

### iDc0!Jl0rated by

### reference at LAC 

### 33·m 3003) shall be used to determine the concentration of TOC (minus methane and ethane) at the outlet ofthe control device when determining compliance with the 20 ppm by

### volume limit, 

### or at both the 

### control device inlet and outlet when the reduction efficiency ofthe control device is to be determined

. 

# •

# ••

, [See Prior Text 

### in D.3;d;1-D.S] .," .•"., .,. .._.- -"_. 

### a. LA€33.m.6991**~ethod** 

### 1 (40 CFR 

### Part 60 appendjx A as incorporated by reference at I,AC 

### nm 3003) 

### orLAC 33.m.6992 

### (Method lA (40 CFR 

### part 60 appendix 

### A. as ;nc0!J)oTated by reference at LAC 

### 33·m 3003), as appropriate, shall be used for selection ofthe sampling site. 

# •

# •• 16

### FLNAL RULE/DECEMBER 20, 1996 AQ145 (See Prior Text in"D.5.a.i-D.5.Lii] 

### (a). the iampling site for thevent stream flow rate and 

### molar composition

## sbIl1 be prior to 

### the final recovery device 

### and prior to the point 

### at 

### which any 

### nomeactor or nondistil1ation stream.

### or stream 

### from

### a nonaft'ected

### reactoror cfistjl1ation

### UJlit is

. 

### introduced. Method 18 

### (fJrC 33.lH:D9T}40 CFB Part 

## 60 l,PJIendix A as incoeporated by refecllce at LAC 33·m 3QQ3) 

### shall be used to measure organic compound concentrations 

### at 

### this site; (b). 

### the efficiency ofthe 

### final recovery device 

### is determined 

### by 

### measuring 

### the organic compound concentrations using 

### Ute 33.m.D9T} (Method 18 (40 

### CFR Part 

## 60 appendix A as incm:porated by reference 

### at LAC 33·m 3QQ3) 

### at the inlet to the 

### final recovery device 

### afterthe introduction of

### aD vent 

### streams 

### and at 

### the outlet of

### the final recovery 

### device; 

# ••• (See Prior Text in D.5.a.ii.(c)-D.5.b] 

### i. LAC 33.lH:D911 (Method 18 (40 CFB part 60 appendix A. as incoeporated by reference 

### at LAC

## urn 3003) 

### shaD be used to measure the concentration of organic compounds including those containing halogens

. 

# ••• (See PriorText in D.S.b.ii] 

### iii. LAC 33.m.DeB (Method 4 (40 CFR part 60 appendix A 

## as incorporated by reference 

### at LAC 33·m 3003) shall be used to measure the content ofwater 

### vapor. c. The volumetric flow rate 

### shaD be determined using 

### Ute 33.HI.6ge3 (Method**2~,** 

### Ute 33.m.6995 (Method**2A~.** 

### Ute 33.m.DeeD (Method 2q orLAC 33.m.6eeS (Method pf40 CFR part 60 appendix 

### A. 

## as incorporated by reference at LAC 

## urn 3003. as appropriate. d. The emission rate ofTOC (minus methane and ethane) 

## <Eroc> in 

### the vent 

### stream shaD 

### be calodated using 

### the following equation:

where: 

### Eroc: = Emission rate ofTOC (minus methane and ethane) in the sample, kilograms per hour. 

## Kz =Constant, 2.494 x 10-6 (liters per ppm) x (gram-moles per. standard cubic meter [scm]) (kilograms per gram) (minutes per hour). where standard temperature for (gram-mole per scm) x (gram-mole per scm) is 20°C. C

J = Concentration ofsample component 

### "j", on a dry basis, in ppm as measured by LAC 33.HI.6eTi (Method 18 (40 CFR part 60 appendix 

### A. as incorporated by reference at LAC 33·m 3003), as indicated in Subsection D.3.d ofthis Section. 

### Mj = Molecular weight ofsample component 

### "j", grams per gram17

### FrNAL ROLE/DECEMBER 20, 1996 mole. AQ145. 

### Q." Vent stream 

### flow rate (scm pee 

### minute) at 

### atemperature of 20·C, on a

### dJy

### basis. 

### e. The 

### total process vent 

### stream concentration (by 

### volume) ofcompounds

.cont:'.ining halogens (ppm by.

### volume, by 

### compound) 

### shaD be summed from the individual concentrations ofcompounds containing halogens 

### which were measured by :
...0 33.5.6611 

## tMethod 18 (40 CFR plll16Q Ippendjx A. IS 

### inCOQlOT!lted

## byrefercnce It I.**~r.** 

### 33-m 3003). £ 

### The net 

### heating value ofthe vent stream 

### shall 

### be calculated using the 

### equation:



### where: 

## Hr" net heating value ofthe 

### sample (mega joules pee 

### standard cubic meter), where the net enthalpy per mole ofvent stream 

### is based on combustion at 2S·C 

### and 760 mi11imeters ofmercwy, but the standard temperature for determining the volume corresponding to one mole is 20·C, as in the definition ofQ. (vent stream 

### flow rate). K

J= 

### Constant, 1.740 x 

## ur 7 

### (ppm)"J (gram-mole per 

### standard cubic meter), (mega joules perkilocalorie). where standard temperature for (gram-mole per standard cubic meter) is 20·C. B

... Watervaporcontent ofthe vent stream, 

### proportion by volume; except that 

### ifthe vent stream 

### passes through a 

### fina\ streamjet and is not condensed. it shal1 

### be assumed that 

### B

... 0.023 in 

### orderto correct 2.3 percent moisture. C

J

### = Concentration on a dry basis ofsample**compon~** 'It 

### "j" in 

### parts per million, as measured for all organic compounds byLAC 33.HI.6611 (Method It (40 CFB. part 60 IpPendix A 

### as jnco[JlQrate4 by

## reference at LAC 

### 33-m 3003) and measured for hydrogen and carbon monoxide by ASTM DI946-77. 

### II;.

.. Net heat ofcombustion ofsample component 

## "l. kilocalories per gram-mole, based on combustion at 2S·C 

### and 760 mi11imeters ofmercury. The 

### heats of combustion ofvent stream 

### components 

### shal1 be determined using ASTM D2382-76 ifpublished values are not available or cannot be 

### calculated.

000 

### [See Prior

### Text in D.6-D.9.a] b. 

## LAC 33.HI.6611 (Method 18 (40 CPR part 60 appendix 

### A. as .jncorporated by 

### reference at LAC 

### 33·m 3003) orLA:C 33.HI.66S6 (Method 2SA 

### (40 CER 

### part 60 appendix 

### A. as incol7"?rated by 

### refe-ence at LAC 

### J3"m 3003) shall be used to measure concentration; alternativelY. any other method or data that has been validated according to the protocol in 

### EPA Method 301 of40 CFRpart 63. appendix A may be used. c. Where LAC 33.HI.66i'1 (Method 18 (40 CER 

### part 60 appendix 

### A. as incorporated by 

### reference at LAC 

### 33"III 3003) is used. the following procedures shall be used to 18

### FrNAL RULE/DECEMBER 20, 1996 calculate parts 

### per million

### by volume concentration. 

# ••• AQ145

[See PriorTest 

### in D.9.c.i]



### . it The concentration of.TOC.(minus methane and ethane) 

### shaD be cal",lated 

### using UR: 33.HL6811 {Method 18 (40 

### CFR Part 60 appcodix A as inco[JlQrated by reference at LAC nm 3003) according to SubsectionD.3.d ofthis Section. 

### d. 

### Where 

### UC 33£6686 {Method 2SA (40 

### CFR part 

### 60 appendjx 

### A A!! ineotJlorated by reference at LAC 33·m 3003) 

### is used, the fonowing procedures 

### shaD be used to 

### calculate

## pirts per million

### byvolume TOC concentration. 

### Lf:jdJ 33.HL6686 {Method 2SA (40 

### CFR part 60 appcodix 

### A !l$ jnem:pnratl!!! by reference at LAC 33·m 3003) 

### shaD be 

### used only 

### ifa single VOC 

### is greater

### than 50 percent of

### total Voc. 

### by volume, in the process vent stream. 

# ••• [See PriorText iDD.9.d.ii] 

### iii. The VOC 

### used as the calibration 

### gas forUR: 33.HL68S6 (Method 25A (40 

### CFR part 60 appendix 

### A as incOJ:porated by reference at LAC J30m 3003) sball 

### be the 

### single VOC present at greater

### than 50 percent ofthe total VOC 

### by volume. iv. The span 

### value for 

### LA€33.m.6eS6 (Method 25A (40 

### CFR part 60 aJlJlendjx 

### A as inco[Jlorated by reference at LAC J30m 3003) 

### shaD be 50 ppm by volume. v. Use of

### LAC 33.m.68S6 {Method 25A 

### (4Q 

### CFR part 60 apPendjx A aSinCO[JlOTated 

### by reference at LAC 33·m 3003) 

### is acceptable 

### ifthe response from the high level calibration gas is at least 20 tim

.. 

### -s the standard deviation ofthe response from the 

### zero cah'bration 

### gas when the instnunent is zeroed on the most sensitive scale

. 

# ••• [See PriorText in D.9.vi] e.The owner or operator 

### shaD demonstrate that the concentration ofTOe including methane and ethane measured 

### by UR: 33.HL6eS6 {Method 25A 

### (4Q 

### CFR part 60 appendjx A !l$ jnco[JlOTated by

### reference at I.AC nm 3003) is below 250 ppm

### by volume with VOC concentration below 500 ppm

### by volume to 

## qualifY for 

### the low concentration exclusion. 

# ••• [See PriorText in E-F.4] AUTHORIlY NOTE: Promulgated in accordance with R.S. 30:2054. mSTORICAL NOTE: Promulgated by the Department ofEnvironmental Quality, Office of

### Air Quality and Radiation Protection, 

### Air Quality Division, LR 21:380 (April 1995), amended 

### LR ' '.

. . ., Subchapter 

### K. Limiting Volatile Organic Compound Emissions from Batch Processing §2149. Limiting Volatile Organic Compound Emissions from Batch Processing 

# ••• (See Prior Text in A-E.2] a. LAC 33.m.Geel (Method I) or 6ee2 (Method IA 

### in 40 

## ern part 60 19

### FXNAL RULE/DECEMBER 20, 1996 AQ14S 

### appendjx A. 

### as inCOlllorated by 

### reference at LAC

# nm 3003}, as appropriate, shall be 

### used for selection ofthe sampling sites ifthe flow rate 

### measuring

# device is 

### arotameter. No traverse is 

### necesSlry when 

### the flow measuring device is 

### anultrasonic probe. The control device inlet sampling 

### siteI for 

### determination ofvent stream 

### VOC composition reduction efficiency shall 

### be priorto the 

### control device 

### and after

### the control device.. "

. _. .. _ _ .. b. LAC 

### 33:H1:6e63 (Method**2~,** 

### 6665 (Method**2A~,** 

### 6666 (Method 2q or 6El6S (Method 2D} 

### in 40 CFR part 60 

### aPJlendix A 

## ::sjnCOlllorated by 

### reference at LAC 

### 33·m 3003 

### as appropriate, 

### shaI1 beused for determination ofgas stream 

### volumetric flow rate. 

### Flow rate 

### should be 

### made continuously. Co 

### Ute 33.1H:6686 (Method**25A~** 

### or 66'71 (Method**18~** 

### in 40 CFR 

### part 60 

## IPJlCDdix A. U 

### jncgmorated by

### reference at LAC 

### 33·m 3003 ifapplicable, 

### shall be used to determine 

### the concentration ofVOC 

### in the control device inlet 

### and outlet. 

### i. The sampling time for 

### each run

### will bethe entire length ofthe batch cycle 

### in which readings 

### willbe talcen continuously ifUtC 33.1H:66S6 (Method 25A.,££l

. 

### CFR part 

### 60 appeodix A as incp[p0rated by rer.,elICC 

### at LAC 

### 33·m 3003) is 

### used or as often as is possible using LAC 33.1H:66'71 (Method 18 (40 CFR part 

### 60 I12Peodix A as incpQ20Tlted by 

### reference at LAC 

### 33'm 3003), with 

### a maximum ofone-minute intervals between measurements throughoutthe batch cycle. 

# ••• [See PriorText in E.2.c.ii-G.1.c.v]**A~ORITY** 

### NOTE: Promulgated in accordance with 

### R.S. 30:2054. HISTORICALNOTE: Promulgated by

### the Department ofEnvironmental Quality, 

### Office ofAir Quality 

### and 

### Radiation Protection, Air Quality

### Division, LR 21 :387 (April 

### 1995), amended LR §1153. limiting Volatile Organic Compound Emissions From Industrial Wastewater 

# ••• [See PriorText 

### in A-E) 

### 1. 

### for determination ofgas flow rate- 

### Test Methods 1-4 (LA€33.ffi.6661= 661340 CFR part 

## 60 appendix A 

### as incQCPprated by

### reference at LAC

# nm 3003); 2. for determination ofgaseous organic compound emissions by 

### gas chromatography

- TestMethod 18 (LAC 33.ffi.66'7140 CFR part 60 apPendix 

### A as inco[poTlted by 

### reference at I,AC 

### nm 3003); 3. for determination ofVOC leaks and 

### for monitoring a carbon canister in accordance with 

### Subsection D.3 ofthis Section

- Test Method 21 (LAC 33.ffi.66'7'740 CFR part 60 appendix A. 

### as inco[porated by 

### reference at I,AC 

### nm 3003); 4. for determination· oftotal gaseous nonmethane organic ernisslonsas carbonTest Method 25 (LAC 33.ffi.66S540 

### CFR part 60 appendix A as jncorporated by 

### reference at LAC 

### nm 3003); 5. for determination oftotal gaseous organic concentration using a flame ionization or a nondispersive infrared analyzer

- Test Method 25A or 25B (LAC 33.ffi.6eS6 0, 

### 6e&'i'40 CFR part 60 appendjx 

### A as incorporated 

### by reference at LAC 

### 3HU 3003); 10

### FrNAL RULE/DECEMBER 20, 1996


# ••• AQ145



# -

....-:. '::" 

### [See PriorTest ID E.6-I) 

### AUTIiOlUTYNOTE: Promulgated 

### in accordance 

### with R.S. 30:2054.

.. HISTORICALNOTE: Promulgatedby

### the Department 

### of 

### Environmental Quality. Office ofAir 

### Quality and 

### RadiationProtection, 

### Air QualityDivision, LR 21:936 (September 1995)•.. 

### amendedLR [Editor'. Note: SubchapterN below 

### will contaID 

### aD text currently located ID SubchapterA 

### ofChapter 

### 6L The aectiODl 

### will be renumbered 

### u .boWJl below.] • 

### SubcbapterN. Method 43-Capture Efl'ic:iency 

### Test Procedures Old SectionINew SectiQa 6121J2155 6123/1156 611S11151 6117/1158 6119/1159 6131/1160

21

### FrNAL RULE/DECEMBER 20, 1996 AQ145

..•..

# -

. :- ... Tide 33 

### ENVIRONMENTAL QUALITY 

### partmAir
Chapter

### 2S. Miscel1aDeoUllDciDentioD Rules SubcbapterB. Biomedlcll

### Wute IDdaenton

• 12511. Studardl olPerf'ol'llUUlce lorBiomedicalWute IDdnenton 

# •••

d. Method 26

- Determination ofHydrogen ChlorideEmissions from' StatiollllJY Sources (LAC 33.1H:69BB40 

### CFR part 60 

### appendix A 

### as jnco[porated by reference at LAC

# nm 3003); 

### and/or [See PriorTest 

### Ia A-E.') L 

### Method 5 • Determination ofParticulate Emissions from Stati01lllJY Sources (LAC 33.1H:69iS40 CFR 

### part 60 

### appendix A 

### as jncm:porated by 

### reference at LAC 33·m3003); 

### b. Method 6 - 

### Determination ofSulfurDioxideEmissions from StatiollllJY Sources (LAC 33.1H:682S40 

### CFR part 

### 60 appendix A 

### as jncm:porated by 

### reference at LAC 33·m 3003); 

### c. 

### Method 7 • Determination ofNitrogen OxideEmissions from StatiollllJY Sources (LA€33.lH.693340 

### CFR part 60 

### appendix A 

### as jncomorated by 

### reference at I AC

# nw 3003));



# ••• [See PriorTest 

### in E.6.e-L] 

### AUTHORITYNOTE: Promulgated in accordance with R.S. 30:2054. 

### HISTORICALNOTE: Promulgated by the 

### Department of Environmental Qua1ity, 

### Office of

### Air Quality 

### and Radiation Protection. 

### Air Qua1ity 

### Division. LR 20: 1098 

### (October 1994), 

### amended LR 21:1081 (October 1995), LR Subchapter

### C. Reluse IDcineraton 11511. Reluse IDcineraton 

# •••**."~** .. [See PriorText in 

### A-D] E. AllowableEmissions from Incinerator. The amount ofparticulate matter (PM.'> emiiteobY a refuseincinerator shallbe deterinined using the test methods from 40 

### CFRpart 60, 

### appendix A, 

### as jnco[porated by referen;e at LAC

# nm 3003: 

### Method 5 - Determination of Particulate Emissions from Stationary Sources (LAC 33.lH.691540 

### CPR part 60 

### appendix 

### A. as ;nCQ[porated by reference at LAC nID 3003)

. 

# ••• [See Prior Text in F-F.9] 

### 22

### FINAL ROLE/DECEMBER 20, 1996 AQ145
L 

### Method S

- 

### Determination**ofParticulate_Enu~ons** 

### from Stationary Soun:ea 

### (LAoS 33.1H:681S40 

### CFR part 60 

### appendix A as 

### incOI:poraied byreference 

### at LAC 33·m3003);

-b. 

### -Method 

### 6- Determination ofSulfurDioxideEmissions from Stationary Sources 

### (LA:e 33.1H:682S40 

### CFR part 

### 60 appendjx A as incQI:porated by reference at LAC 

### 33·m 3003); c. 

### Method 

### 7 • Determination ofN'rtrogen OxideEmissions from Stationary Sources 

### (LA:S 33.1H:683340 

### CFR part 

### 60 appendix A as 

### incQOIQRtc<! by reference 

### at LAC 

### J30m'JOOJ); d. Method 26 • Determination ofHydrogen ChlorideEmissions from Stationary Sources 

### (LAoS 33.1H:68884Q 

### CFR part 60 

### DWCOdjx A as incQI:poratc<! by reference at LAC 33·m3003); and/or 

# ••• [See-PriorText in F.9.e-H] AurHORITYNOTE: Promulgated in accordance with R. S. 30:2054. HISTORICALNOTE: Promulgated by the Department of Environmental Quality, Office of

### Air Quality and 

### Radiation Protection, 

### Air Quality Division, LR 20: 1100 (October 1994), amendedLR SubchapterD. Crematories §2531. Standards ofPerformance for Crematories

• 

# ••• [See PriorText in 

### A - K.l) L 

### LAS 33.m.681S (Method 

### S

- 

### Determination of Particulate Emissions from Stationary Sources (40 

### CFB. part 60 

### apPendix A 

### as incoIj)Qrated by 

### reference 

### at LAC 33·m 3OO3); b. Method )0 - DetenDination Qf CarbQn MonoxideEmissions from StatjOQluy Sources (40 CFRJW1.60 apPendix A as incQIj)oRtc<! by 

### reference 

### at LAC 33·m 30(3) 

### (Method 18 • 

### Dctuuaiuatioll of 

### C1uboilftfOilOxidc Ennssiolis BOlli**S~tjonar)** Sowecs}, 

### c. L!£ 33.m.6e41 

### (Method 9· 

### Visual Determination ofthe Opacity of Emissions from Stationary Sources (40 

### CFR Part 60 

### appendix A as inooIj)oratc<! by reference at LAC 

## nID 3003); and 

# ••• [See Prior Text in K.l.d-K.2) AurHORITY NOTE:

-Promulgated in accordance with R.S. 30:2054.-- mSTORICAL NOTE: Promulgated bythe Department ofEnvironmental Quality, Office of

### Air Quality and Radiation Protection, 

### Air Quality Division, LR 20: 1107 (October 1994), amendedLR

23

### FXNAL RULE/DECEMBER 20, 1996 TIde 33 

### ENVIRONMENTAL QUALITY PartID.Air 

### Chapter

# 2'. OdorReguladoDi 12901. OdoroUi Substances 

# ••• AQ145



### (See PriorText in A-F.I]

• 2. An 

### samples 

### shall be 

### eveJUBted u soon after collection 

### u possible in accordance with 

### the

### procedures set

### forth in 

### tieBi.ision's SOW" 

### TestManual 

## f.U£, 'lvluillC 11)Sybsest;iQD G gftbjs Section 

### EDITOR'S NOTE: fIbe foDowing 

### tut b81 

### been moved in 

### its entirety from LAC 33:ID.60" 

### la 

### Chapter 60 and renumbered 81 

### Subsection G below.] 

# a. Method 41. OdorTestMethods 

## *- 1. Butanol OdorEvaluationProcedure 

# +
.. Sampling and 

### Storage. Odorous gas sampling is no more than 

### typical integrated bag samjlling. 

### Figure I shows the sampling 

### train used by the department. A sample bag is placed inside the rigid leak-proofcontainer. Bag material shall be manufactured ofFEP Teflon, Tedlar.orMylar. 2 

### h. The 

### bag is 

### filled by 

### partially evacuating the rigid container. After partial filling, 

### the 

### airin the bag is expelled by pumping airinto the containeruntil the bag is empty. This serves 

### to preconditionthe bag walls. 3' ,. The 

### bag is 

### then 

### totally filled by evacuating the containerwith a pump. The bag is 

### removed, 

### capped or sealed, and taggedfor storage and eventual transport to the odor lab for sample evaluation. See 

### FigureIfor apparatus setup.



### .. i1. Ifthe odorous air is 

### very humid, and it is suspected that condensation of water

### will 

### occurin the bags, an additional procedure, predilution, canbe used to prevent condensation. The 

### bag is 

### ba1ffilled ·..nth odor-free air using a cylinder and flowmeter. This will allow exact 

### metering ofaknown amount ofodor-free air; the 

### odorous air san:

### pie can then be taken per

### previous instructions.

-**~.** 

### Odorous samples shouldbe stored in containers for a minimum oftime after collection. This should be adhered to whereverpOSSIble and the time ofstorage, before odor measurement, must be recorded for each sample. Ideal storage conditions are less than four hours; acceptable conditions for most odor mixtures'are 8"16hourrStorage oyer 24-hours is-

-- unacceptable. In general, to prevent sample deterioration: a 

### i. use FEP Teflon, Tedlar, orMylarbags; b 

### ii. minimize sample storage time; and e 

### iii. predilute sample bag oruse other suitable means to remove moisture if

### condensation is evident on the bag wall. 24

### FINAL RULE/DECEMBER 20, 1996 AQ145 

### B 

### 1. The departmentuses butanol referencing techniques for quantifYing odors 

### in terms 

### ofinteosity. The method parallels that specified 

### in ASTM ES44-7S. Acomplete description 

### oCtile method follows:


## , .,.' + a. Description

.... .', _ , . a 

## i. Figure 2 depicts the 

### olfiu:tometer. Adjustable airflow controls an:: 

### mounted on the 

### rectangularbase 

### plate. The odorantvaporgenerator, flow splitters, 

### and ports 

### that 

### deliverthe 

### prepared stimuli 

### (butanol) Ire 

### mounted on an 

### aluminum plate 

### discthat canbe 

### rotated 

### within an almost

### fW1 revolution. A 

### bandle is positioned to tum 

### the 

### sample ports and is set 

### to 

### limit the 

### rotation ofthe 

### disc to one turn. 

### b 

## i. There Ire two 

### air flow systems 

### within the 

### olfiu:tometer, each is controlled 

### by • separate 

### vIlve (V) 

### and monitored by separate 

### in-Iine flowmeters (Flo 

### FJ. Both can be 

### supplied &om the same air supply.

. e 

### iii. Odorantvapor flow system is supplied with air at. 

### rate onso mlImin (left 

### flowmeter). This 

### air flow is delivered to the 

### odorantvaporgeneratorthrough. ' flexible food-grade (almost odorless) Tygon tubing (1'). 

### The odorantvaporgeneratorconsists of. ' glass vessel (G) 

### and several flow-controlling capillaries. This section is 

### shown separately schematically in Figure 3. d The odorantvapor/air 

### mixture from the 

### generator is supplied to the upper cavity ofthe ·odor splitter" (0) 

### through the upper tubular spout ofthis splitter. The splitter distn"butes the 

### generator-prepared vapor/air

### mixture to eight stainless steel capillaries. The other ends ofthe capillaries COMect viaTeflon tubing to the corresponding glass snifling ports. The capillaries Ire 

### calibrated so that Port No.8 (highest odorant concentration) receives

. mominally 160 mlImin ofthe vapor/air

### mixture, and the next Port, No.7. receives nominally 80 mlImin ofthe same mixture. Otherports receive odorant volumes as perTable 1. e 

## x. The make-up airflow system, 

### which is controlled by the valve

-

. Flowmeter assembly (FJ. 

### is fed at 9S0 

### mlImin. It is distn"buted by the 

### lowerlevel ofthe splitter

(0). 

### The make-up air is delivered to this level viaTygon tubing attached to the spout ofthe splitterunder,the olfiu:tometer disc. There is no coMection between the lowerlevel.

### and upper level ofthe 

### splitter. The lower splitterprovides additional air to Ports No.7 through No. I so that the total 

### flow to each port is nominally 160 mlImin. Mixing occurs in the port. Rapid flow rate changes occuron emergence from the Teflon tubing and from the lower smaller cross section of the glass port into the wider vertical glass tube portion. This action assures sufficientturbulence for adequate mixing.**-''''-J~,&:'''''!,'_''** .: ..•• -.--... . ••.

25

### Fr.NAL RULE/DECEMBER 20, 1996



# .. AQ145

. 1·,,1._-- •. 

### i £a). 

### Flow rates 

### are 

### measured, 

### if'necessary. 

## by attaching a Buck 

### Calibratorflowmeter to 

### ends ofthe Tet10D tubings temporarily pulled out ofthe ports. Nominal flow 

### rates shouldbe:

Table I



## .. 0cI&nal vapar.canyioa Mako-UpAk 

### TbbiNzPai PoRNo. TubimrBad (mLiDia) TIabiM Bod (mIImia) I 160 7 80 

## . 80 6 40 120 

# , 20 140 4 10 150 3 5 ISS 2 2.5 157.5 1 1.25 158.5 

### ii 

# au. The actual flow rates may differ, usually not more than 

### within a few 

### percent, and are measured and included in calculations in more exact 

### experiments. 

### f 

# n. Vapor generator section, Figure 3, contains a saturator, (Vessel G) 

### which consists ofahorizontal 16 

### nun o.d. by 

### 170 

### nun long

### Pyrex tube with closed ends and three 

### side

## tubes. each4 nun o.d. and 2S nun long. The middle tube is used to introduce the odorant (butanol) and is then closed with a glass rod 

### plu& 

### p. COMected 

### to the sidetube by a short length of blackneoprene tubing. g 

# m. Important SafetyNote: When slipping the neoprenetubing onto the glass 

### side tubes, hold the sidetube with fingers using short neoprenetubing collarwith which the tube is equipped. Twist the attachable neoprene tubing to and fro, to facilitate the connection. If

### the glass vessel is held instead, the small glass side tubes may 

### break otT. Use the same precautions when removing the attachabletubing. Same applies to the otherglass
" tlib1ngfneoprene sIip-on' COMectiOns. GoDars are not shown in 

### Figure 3. ' . It**~.** 

### The two otherglass side tubes on the vessel are connected to the flow control capillaries. Capillary C is the principal vapor flow control capillary, while Capillary E is simply an exit capillary, with much less flow resistance than C. CapillaryB is for air bypass; it is always ofthe same size and length, while capillary C may be changed to provide Sx, 2Sx, SOx, 

### and lOOx 

### flow split ratio. The department wiD use the nominal Sx flow split ratio in 

### 16

### FrNAL ROLE/DECEMBER 20, 1996 .AQ145**estab~** 

### itsbutanol scale. The ratio offlow rates 

### through bypass B 

### and through the 

### saturator 

### veSsel vapor space depend onthe flow**resi~** 

### ofB 

### and C. Capillary C is 

### upstream ofthe vapor space

### to maintain 

### air pressure in the saturatorvessel close 

### to atmospheric.



### .... ·i

. 

### ilt. The desirable volume ofodorant inthe 

### saturator

### vessel is 

### 8-:

### 10 

## mI. which fills 

### the 

### lower

### halfofthe'

### vessel 

### and prOvides the 

### widest surface. At 

### up 

### to 60 

### m1/min 

### air flow, the 

### airleawig the saturator is 

### practically 

## saturaiedwiththe odorant vapor, as bu 

### been established by

### mass-transfer calculations and direct measurements oCl-butanol concentrations by 

### hydrogen

### fIamc ionization detector; at 60 

### m1/min, 98 percentplus saturation is 

### reached. The degree ofsBturation is not 

### a fimc:rion of the 

### vapor pressure (which varies with odorants by 

### several orders ofmagnitude), but 

### of the diffiJsion 

### constant for the 

### odorant in air, 

### and this constantvaries from 

### odorantto odorantwithin a li'acrion ofone order ofmagnitude. The method of

### air pusage over the 

### surtice c:in:umvents the need for mist

### filters needed when 

### the saturation is by

### bubbling the 

### air

### through the odorant At 

### lower flow rates, a few drops of

### the odorant may provide enough evaporation surface. j 

## x. Vaporization rates 

### are too low to produce significant cooli:lg except forthe 

### most volatile odorants. Hence, for simpUcity, no thermostating is provided. but the temperature at the saturatorvessel is 

### measured for use in vaporpressure calculations. The temperature 

### in the area ofthe apparatus will 

### be maintained at 2S·C

.



### .k 

## xi. The vapor dilution immediately 

### after the saturation in the vessel produces a 

### margin ofsafety 

### in preventing condensation in 

### the 8-way splitter, in cue ofa temperature change or sudden pressure drop. I 

## xii. Connections to 

### the stainless steel capillaries are via slip connectors, as shown 

### inFigure 3. A short 

### (S MM) 

### length offood-grade Tygon tubing fits tightly around the 

### capillary. A piece ofblack neoprene tubing overlaps this tubing and the larger connecting tube (brass 'flee, or glass side tube, ormulti-way air orodorant-side splitter) so that 

### the small Tygon tubing tits 

### tightly against the largertube. This system permits only a limited contactbetween 

### the odorant vapor and Tygon and neoprene. These materials can be reached by vapors only by 

### a non-connective diffiJsion 

### through stagnant aMular spacebetween the o.d. ofthe capillary 

### and the 

### larger connecting tube; thus, depletion ofvaporby sorption into Tygon or neoprene is 

### negligibly small. In 

### reverse, when 

### the odorant vaporis discontinued. contamination of air 

### flow by 

### desorption of

### the odorant from Tygon orneoprene is slow 

### and usually does not generate a prolonged contamination problem ofany 

### significance. 8til1, it is desirable 

### to flush the odorant vaporflow system during the shutdown. m 

### xiii. Connections betweenB and E capillaries are via brass tees and slip on connectors. To check the generator system splitter ratio, brass tee (T) 

### is pulled offB and E, 

### and the flow rates out ofB and E are meascred using.the same total odorant vapor flow rate as normal (the splitter ratio may be slightly affected on the absolute flow rates). n 

### ltbl. Important: Only soap film flowmeters are suitable for measuring the flow rates in 

### ports and at B and E. Other flowmeters produce some flow resistance which, in the low-pressure flow system ofthe olfactometer, will influence the flow rates and yield wrong values. Figure 3, bottom, illustrates connections to the soap film flowmeter for two situations: 27

### FLNAL RULE/DECEMBER 20, 1996 AQ145 

### i £a). 

### connecting to 

### Teflon tubing ends 

### pulled backward out -. 

### ofthe ports for measuring flow 

### rates to the 

### ports; 

### and 

### ii 

# au. connecting to 

### ends ofB orE 

### when the brass Tee (Figure 3) is 

### pulled offfor measuring the 

### flow rates 

### from B 

### and E, to 

### check splitratio in the vapor generator 

### section.

- _.- .**~.** 

### -. .- .. , o r£. 

### Very 

### Impottant- To PreventUndesirable Contamination ofthe System



### . i £a). 

### With the 

### odorant 

### in the 

### vapor-generating

## vessel. the flow of

### air the 

### odorant part of the 

### system 

### mustbe immediately set

### in operation. If

### this is 

### not 

## done. odorantvapon from the 

### vessel may drift 

### into the splitterbypus, condense there, 

### and result 

### in a much higherodorant concentrationthan 

### in the 

### regular

### operation. It is 

### best to 

### place the odorantinto the

### vessel through

### the 

## ceitter spout (c£ 

### Figure 3) with the bypass system (two 

### brass 

### tees with 

### capillaries B. 

## C. and E attached) 

### removed from the

## vessel. then plug the center spout of the 

### vessel, 

### begin air flow and then connect the

### bypass system 

### to 

### the 

### vessel. i 

# au. The same applies to 

### shutting-down ofthe olfactometer. Farst, 

### the by-pass system is removed from the

## vessel. and the end spouts ofthe odorant ve:se1 are' plugged with pieces ofneoprene tubing and glass rod 

### plugs. With air 

### flow 

### still continuing, the capillary C is 

### connected to capillary 

### E by a shon piece ofTet1on tubing. This permits flushing the odorant vapon from the 

### odorant side ofthe system. 

### Flushing is continued until the bighest-concentration pon does not exru"bit odor. 

## e 1. ProblemslBaclcflow. Failure to observe need for continuous air 

### flow while the odorant vessel is 

### connected to 

### the splitter (see preceding section) can easily result in diffusion of the odorant throughoutthe system, 

### including baclc-diffusion into the Tygon tubing connecting flowmeterto 

### the disc assembly. Such contamination is difficult to remove, 

### and replacement of some components may become necessary. Alist ofsources for the components is attached (Subsection 

### E!U ofthis Section). 

### B Sample Calculation ofDilutions 

# +
.. Saturated Butanol a . 

## i. Odorant: 

### I· Butanol b 

### ii. Temperature: 

### 2S·C e 

### iii. Vapor pressure. from Chemistry 

### and Physics Handbook or other source, for 

### 2S·C is 6.97 

### mm. d This corresponds to:**~OOO.OOO** 

### x 6.97n60 = 

### 9170 ppm in air 

### saturated with I-butanol vapor at 

### 2S·C; (I 

### atm = 

### 760 mm). !l 

### h. Dilution Factor in GeneratorlBypass System. DilutionFactor: 4.66:l: .20 ".**'.:··_·~.i";., -.~--,:...~**  .. ', ,,_.,;,_ •..**_-_._-~.~----"-'-"'**•. ,'",----

. 

### a 

### i. The concentration oft-butanol in the 

### flow supplied to the round splitter is then: 9170/4.66 = 

### 1966:l: 16 ppm b 

### ii. This is also the concentration supplied to Pon No.8. e 

### ill. Measurements for other pons are conducted by pulling the 28

### FrNAL RULE/DECEMBER 20, 1996 AQ145

• 

### Teflon tubing out from the ports 

### and connecting the 

### Buckcalibrator to 

### these 

## lines. 11 

### ix. The 

### conowing set oC

### data illustrates 

### the calCulations. (See Table 

### 2) 

### e X. 

### The

### brass tee 

### is sequentially 

### pulled offcapillaries B and E and the air

### ftow from 

### eachis measured. E 

### i. Components 

### and 

### Sources 

# + a. Stainless Steel Capillaries a 

### i. 1/16 o.eL. 0.030 LeL b 

### ii. 1/16 D.eL. 0.020 LeL e 

### iii. 1/16 D.eL. 0.010 LeL 

### II. Teflon Tubing. 

### Teflon tubing 

### AW GageNo. IS. standard 

### wa1l, natura1 

### color. :t G. 

### TygonTubing a 

### i. TygonFood Grade 0.031S in. 

### tel For s1ip-on-connectors-Cor 

### stainless steel 

### capi1laries. b 

### ii. Tygon tubing, Food Grade Formulation B-44-4X, S/32 

### in. Ld.• 7/32 in. D.d.• 1132 in. wall. Forflowmeter-to-disc:**co~.:Iection.** 

### e 

### iii. Tygon Food Grade tubing, 0.0655 

### in. i.d.• 0.1945 in. o.d. For connection ofsoap film 

### flowmetertubing to Teflon tubing ends.



### .. d. Neoprene Tubing. Black neoprene tubing, 1/4 in. o.d., 1/16 in. wall, 

### Cor s1ip-on connectors and for. plug. 

### 5 .G. 

### Glass Ports, Odorant Vessel. Pyrex glass, custom-madeby glass blowers. 6 

### f: Fiowmeters 

### a 

### i. 50-500 

### e:cImin b 

### ii. 100-1000 

### e:cImin

29

### FXNAL IWLE/DECEMBER 20, 1996



# . Table 

### 2 B-Port I-Butanol Otmctomctcr

Port Concentration in J) 

### m Date

. 

### 7 6· 5 4 .3··

. 

### ··2' 1 12-13 '1038 ·533· 274 138 70 35 17 12-15 1034 517 272 137 71 34 18

• 

### 12-15 1042 524 268 137 71 34 19 12-15 1042 520 271 132 72 35 18 12-16 1010 513 271 136 70 35 17 12-16 1040 529 278 137 73 

### 36 18 12-16 1032 516 272 134 72 35 18 

### TOTAL 

### 7238 3652 1906 951 499 244 125

AVO. 

### 1034 522 272 136 71 35 18 =10 =7 :J :2 

### =1 =1 =1 AQ145



### F 

### 6. OdorPanel t I. 

### An odor panel consisting ofeight members sha11 be selected by the department. Panelists sha11 not use perfume orperfumed shaving lotion within two hours priorto the test. Panelists 

### sha11 not smoke, 

### eat. or chew tobacco orgum for at least one hourbefore testing. Panelists 

### sha11 notbe tested for prolonged periods oftime. Aloose schedule with long resting periods for panelists is 

### recorrunended. 2 

## h. Panelist candidates are screened for

### their ability tojudge intensity. This is 

### usua1Iy done using the butanol intensity olfactometer. Abag sample is 

### taken from one of the eight butanol ports (usuaI\yNo. 4 orNo. 5) and the candidate must sniffthe bag sample and select the 

### portthey feel hasthe same intensity. Panelists ·should be able to match butanol-to-butanol withintwo scale units. As 

### with 

### a1I sensory odor evaluations, the screening tests

. should be conducted in as nearly an odor-free envirorunent as possible. :I' 

## .c. The testing room will 

### be supplied with activated carbon filtered air 

### of

. __.**_.~ntrolled** 

### constant temperature and humidity 

### (25·C and 

### RH 50 percent).



## .... .".. ..11. EaChpanelist compares the intensity ciftlic undiluted ambient sample being evaluated to the eight point butanol scale, specified in this procedure starting from the low end ofscale, i.e.• l::levels between two values on the scale may be selected by each panelist (i.e. 

### 2.5,6.5. etc). The arithmetic average ofthe values chosen by the eight panelists

## win detennine compliance with the standard specified in the regulations.
30

# - FLNAL RULE/DECEMBER 20, 1996 AQ14S

RIGID r LEAK 

### pnoo, CONTAINER

### rFEMALE VACUUII

LINe 

# ·c QUICK

# CO~MICT L.
- .. AU II TIPLON .AIIPU LINe TI'LOIf



### ..noae

31

### FrNAL RULE/DECEMBER 20, 1996



# ,..... 

# ,

# ......,..."'

# ....... 

# ........, . ...ou.e...... T 

### AQ145

.**~.....** 

## .

31 -)' . _ .......Fr.NAL 

### RULE/DECEMBER 20, 1996 AQ145



## .. 

# ....- CWIrWII ""-**a-wt~** e:.-.u-1Ir --.,.-.

............... n--
........ 

# ,

f

&



# t,.. 0.06'" l •• O.LU" ••

## l&:.J

33 

### oren_ f

..**~la&** / f&'IM'Drc**Qt~ F~**  

### RULE/DECEMBER 20, 1996 AQ145 AUTHORITYNOTE: Promulgated in 

### accordance with

### R.S. 30:2054. InSTORICALNOTE: Promulgated by

### the Department 

### ofEnvironmental Quality, Office ofAir 

### Quality and NuclearEnergy, 

### Air QualityDivision, LR. 

### 13:741 (December 1987), amended by

### the Office ofAir 

### Quality and ]hdjatiOD

### Protection, 

## AU: QualityDivision, LR.

•



### 34

### FINAL ROLE/DECEMBER 20, 1996 Title 33 ENVIRONMENTAL QUAIJTY 

### PartID. Air Chapter 30 

### Standards of

### Performance for

### New StatioDUY SQurces (NSPS)



### .
. 

### . -... 

### 13101.

# _cal gd Rcagmhcri0l' 

### AQ145



### . ,

The 

### folJowi01 

## dvurtm. u 

### they appeared 

### on June 30. 1996, 

### are hereby 

### repealed or 

## renumbered u jodiqtcd belOW; 

### A.. Chapter31 is 

### mpcaJcd 

### B. Chapter

## 60 i' 

### rcpcaJod with 

### the exception 

### ofLAC 33·m 

### 6099 which 

### is moved and 

### mmmbered u LAC 33·m 2901 ,G, 

# c.. Chapter 61 is 

### repealed 

## with the exception**ofS~hzurter** A which is moved and 

### renumbered as Subc;bapter

### N 

### in ctapter21 , 

### D... Chapter 64 

### is repealed. AUTHORITYNOTE: Promulgated in 

### accordance with R.S

..30:2054. mSTORlCALNOTE: Promulgated by 

### the Department ofEnviromnental Quality, 

### Office of

### Air Quality 

### and Radiation Protection, 

### Air Quality**Divi~on,** 

### LR Subdaaptcr A. IpCOrpODtjoo by Reference aBR) 

## 13003• mR 40 Code gfFdmlRezu1atioCf(CFR) Part 60 

### A, Except U 

### modified in this section. rcauJatjOD$ 

### at 40 

### CFR Part 60 as 

### revised July 

### 1, 129S, 

### and 

### sPecified below in 

## Tables 1 and 1,A 

### are hereby 

### inco[pOrated by reference as 

### they**~ply**

40CFB Part 60 

### Subpart Beldin:

Emi

. 3S

### FINAL RULE/DECEMBER 20, 1996 AQ145 '.



# . TABLEt


### .**40~** 40QB, SgbplttHcadinC Part '0 .. 

# - . .. 

### . . .J:h 

# . . .- 

# .... :llod 

### ., 

# - •**f'nr~A,.;tf** . 

# . . I Unit!t
• 

# ...n StllDdards ofPerfQDDllDce fpr Fos!lIl-Fud

## Ere<! Team GeneratoR for Which

- • ,T. After 17 1071 

### ....Da Standards ofPerfonnance fprElectric

### Utjf'lY Stearn C".eneratinc Units forWhich • I**J~** After ·1f1 10711 

### ....DIl Standards 

### ofPerfonnancc for Indnstrial-Commcn;ial-InstjtutjonaJ 

### Steam 

### ..Q! 

# · ,Unit!t Standllrds ofPcrformance for SmaJl Jndustrial-CommerciaJ-Jnstitutional Steam



# · ,Unit!t 

## .E ,f'nr 9 

# . ..Ea 

# - · • lof A ,for 

# .. . . ...E I for' 

### ..G • A,.;tf 

### ...H 

# _. • • :of- A I for

- 'A •

### Aci~ 

### ,I 

### ,,- ,fnr A

....10.1.

- 

### ..l 

# · 

# · A' A , for 

## IV, A 

# . ...K StllDdards Ofperformance for Storace vessels for petroleum Liquids for Which CoOstruction. Reconstruction. orModifiCatioo Commenced AfterJune 1 1. 1071**an~** Prior.n Mav 19, 1978 

### ....KIl Standards ofPerformance for Storage Vessels for petroleum liquids for Wbich Construction Reconstruction orModification commenced MerMay 18 1°78 lin" Prlnrtn T"lv"1

. 

### ....Kh Standards ofperformance for Yolatjle Organic IJQuid Stomge Vessels OncJudinc Petroleum Liquid Stomge Vessels) for Which Construction 1), • nr"**J;~** • "ft

..rJlllv21191l4 L Standards of A ance for SecondarY T

....tf**~melters** 

### 36

### FINAL RULE/DECEMBER 20, 1996 AQ145 

### TABU; 1**1~60** 40Q1l**Sp~p.rt** 

### "UndiD' -... . 

### - p,rt60**~-** .. 

### .' 

### .M • 

## . 'bQ{. 

# - ! fOr- , 

# - ,aR" 

# . ..H Standards ofperfbrmanljQ

### forPrimmEmission, fipm Basjc 

## Oxxam 

## Prom'

-**,&.~** • lig' Aft_T"R_l1 1Q71

. 

### ...lia Standan!g ofperfonnance for Secondll)'Emjssjong fjpm Basjc

## OxxamProcesg stcc1m8JrjuIJ FaplitiCS for Which Constmction is Commenced After Jlnula 20 

# 00

. 0 •for p**~-** •**for~** • 

# - . 0**~-** 

# -**~.** 

# - . R 

# - . 

# - . ,T _tl- 

### . 'tor S
· for 

# . A 

# . 

# - . ....:I Standards ofPertbrmance for the Pho:;pbate Fertilizer Industry: Wet-Process 

## .l!!

. . A,.;tl 

### ....ll Standards ofperformancc for the Pho!ijlhate Fertilizer Industry;

•**A";~** 

## . ..:L Standards ofperfimnans;e for the pho!ijlhate FertilizerIndustJy: Diammonjum

### ~'~ . ...:if. Standards ofPerfonnancc for the phosphate FerttlizerIndustJy: Triple



# - .l' Standards of performance for the phosphate Fertilizer lndustO'· Granular



# . " 

## ... .tnr ;'0.("- '

..=';"

. ...**,-_.~.** 

## . .. 

# - . - 

### J.



## z •for 

# .. •**D._,f.~** ... :_.,**'I:'~,.;Ji'i** .. 

### --AA Standards ofperformance for Steel plants' Electric 

### Arc Furnaces Constructed After l , , 1 1Q74**~ntl** on or Reforf! Anm••• 17 1983

37

### FrNAL RULE/DECEMBER 20, 1996 AQ145 

### TABI,E I 

# -**An~60** 

## - 40CFB. 

### Subpart**IlcadjD~** ._", rlrtiO



# - - .A&. Standards ofPerformance for Steel Plants' Eldric 

### Arc Furnaces and 

## Arion-

, 

## bR

.. -**A~** .... A ..,7 

### J.gg

• 1'

..... Tl'

... 1»0,1"

, 

# . 

# -- ,**,f'nr~** _. 

# - . ....tC

DD •f'n

.. 

### r
.....l"

- 

### ...EB 

# .. ,tnr

- 

# - - . .. 

# .- .

FF fR .n 

### --.00 • • 

# -- ,f'nr

- 

# . ,r ...**~-** 

## .. ...HH**.~** ..**~;** nt •f'nr T.im

.. M**~ft,** - 

# .

KK •f'nr T

..**~tl_A,.;tf** • 

# . LL •**.~** •f'n

.. - 

# ..

# - .

# - . 

# _ 

# . .MM Standards ofPerfonnance for Automobile and liibt-puty 

### Truck Surface



# · · ...IDi 

# . .f'nr , Rndr 

### ..H 

# - • 

### • 

# -- ,fhr • 

# . ....QQ Standards pfPCIfuanance for the C'l1'8,pbic Arts IndustO" Publication


# ...- · 

# . , 

### ....B.B. Standards ofPerformance for Pressure Sensitjye Tape and Label Surface



# · · --SS 

# _. • ': nf ·fnr 

## . 

# .. 

# - .r', 0 o T,arne Annr 

# .:.rr
..
.**~t~rirl~rrl. nt~**  •f'n

.. M,;to1 r<in - . 

# . .. "_J-.

..... _ • 

## -
.. 

### ...!lll Standards pfPerformance for Asphalt Processing and Asphalt Roofing**M~n**



### 38

### FXNAL ROLE/DECEMBER 20, 

### 1996 AQ145



## .
. UBLEt

•

### O~ 

### '·QUB Sgbpart Bcadin, 

## ',rtO

.. 

# - . ...l!l! • Standards ofperfgnnanGC fnrFquiprnent

## TnU ofyOC in the Synthetic 

## ..Q! '!.Q '**-~** 

## , WW ,fnr th,,- , 9 

# ..xx ..§!i , , !fhr RII""

- . " 

## bI! ,



### AAA , ' 

# ... !for' ,'D, , , 

# . ..§!i 

# · , 

# . • !forth

.. • •
.Tire

.. , 9 , CCC 

### ,., 

### PDP Standards ofperfonnance fnr yoIatUe Organic Compound (YOC) Emissions**fTomthe""··"~** • lrnF. 

### ,., 

### -fEE • •**.~** 

# . •f'nr

-**~',** V,nvl .nll T' .• 

# .
. and 

# . .

GC',Q Standards ofperfonnance for Equipment Leaks ofyoe in Petroleym



# - -
, HHH • ': of ,for , 

# . ... ....III Standards ofPerfonnance fhr Yolattle OJpnjc Compound 

### (YOe) Emissions Fmm the Synthetic Orpnic Chemica! Manufacturini Industty (SOCMD Ajr , , I TJnit 

### JJJ 

### , .. ,. ,for- 

### • 

### Inrv£!! 

### KKK Standards ofPerfonnance for Equipment Leaks ofYOC From Onshore NaMa! 

## r

...**~-** 'n"-'

- LLL**~t.nrl-rds(l--** ...er"'n

_ for"" _L 

## , r .... 

## .

. so" Emissions MMM I J) 

### NNN Standards ofperfonnance for WatUe Organic compound CVOe) Emissjons fonn Synthetjc Organjc Chemical Manufacturing IndustO' (SOCW) Djstj1)atjon (**JDeration~** 

### 39

### FrNAL RULE/DECEHBER 20, 1996 .\0145
TABLEt



### ..**n~** 40U'B Sgbp.rt Beadjnr 

### Part 60 ..

# - _.-

### -



# . 000 •**~'"** 

# ...... 

# .. . PPP • 

# _. • 

# ·**~,** ,forWool.§l1 

# .**~.** 

# .. . 000 Standards ofPerfnnnBuM for

### YOC EmissionsFrom petmJCUm Refinery
RRa Standards ofPerfonnance for volatile 0mnic Compound Emissions 

### From Synthetic 0mnic Chemica! Manufacturinz IndusttY (SOCMD Reactor



# - !':!':S 

# · ,fnr'M: • :Tane 

# . 

# - .... W Standards ofPerfonnance for Industria! Surface Coatin:" Surface Coatin: of**~Partsfnr'** 

# .**.~** 

# . umJ**~.,** fnr .•. , ..**nd~·** ,in 

# . YYV Standards ofperfunnance for Polymeric Coatin: ofSupportini Substrates Facilities

TABLEJ.A .sn rFR 'PA'RT,;n**'-~** 40QR Appendjx Headjn: , 

### Part 6Q A 

# .

. 

### -A Test Methods B. 

# . ti"".·


### .. 

### ..**~-** .•...

_____ L_
.. 

### .. 

# ...c 

# · . lofb 

## . 

# . ,RM

.. 

### ...D 

# . .."missinn Tnv 'jnn E (R

## "S"IV"'!) 4Q

### FZNAL RULE/DECEMBER 20,**~996** 

### AQ145

4QCFB Part 

### 6Q



## .. Appendix 

### UndlDI

" 

### --G Provisions for an 

### Alternative

## Method ofDemonstratina ComplianceWrth 40 CPR 60 43 for theNcwtpn 

### PowerStJ!jgn gfCentraJ minail Public 

## Service

B Fina! repletions published in Federal**Re~** from July 2. 1995.**tbrou~** June 30. 1996. and specified betow in Table 2. are hereby incorporated 

### by reference as they 

### apply to the State ofLoujsjana



### Subpan 

## w Subpart Hcadjnz'Appcndjl Federal 

## Rezistq Citation
60FR 43258 

# nm Promulpted


### August J8, J995

Subpart OOQ Standards QfPerformance for

## yoe
..... ..... ,-: 60JR

...._.r 

### August 18. 1995 

### Emissions from petroleum Refinery

.. 43259



### 41

### FINAL lUJLE/DECEMBER 20, 1996 AQ145

i. December] 9. 

### .l22S. mER**6S414,~** 

## OeneraJ Provisions F(/mI 

### Dale Sgbpart

### Bcadin:lAppcndg 

## Ra&t« PrpmuJ:atcd CtatjoQ 

### ApgendiM 

### Standardl 

### olPcrfprrnJmeeforNew 60ER 

### september J 1. 

### StatiODID' Sggrccs 

### Appendjx A - 

### 47

## 096 l221 Reference Methods; 

### Amendment to Method 24 

### for the Determination of VoJ,tDeMatter

### content. Water 

### Content. 

# Denm Yolume SoUd$. and

## Weiaht Solids Sub,part 

### Standards gfPerformance for 

### YoJatUe 

### mER 

### November 27. 

### Htni Orpmc Compound (YOC) Emissions 58237 

### l221 

### From Synthetic Orpnic Chemical Manuticturini Industty (SOCMI)



# . 

# . Subpart StandardS OfPerfonnance for 

### YoJatUe 

### &.ED. November27. 

### B.B.B. Orpnic Compound (YOC) EmissioDs 58238 

### .l.22S. From Synthetic Orpnic Chemical Manufacturina Industty (SOCMI) 

### Reactor SubpartEa 

### mER 

### December 19. 65384 

### .l.22S.

Subpart A Subpart B Subpart C



### 41

### FINAL RULE/DECEMBER 20, 1996 AQ145

March J 2. )996 

## December 19 

### 1221
61 

### FR. 2918 

### 60ER 65419
Oeneral Provisions 0- 

### Fdmll 

## Dm Sgbpart BeadtnlfA,ppcndjl 

## Rezist« PromgJ&atesl CitatioQ SubpartCa 

### 60FR December 19. 

### 6S414 

### 1221

. Subpart

### Cb 60FR December 19. 

### 6S414 

### 1221
Sulwart Cc 

### 60FR 

## Decembec J

### 2. 65414 Subpart Cd Emission Guidelines and Compliance 

### 60FR December 19 Iimes for Sulfuric Acid Production Units 

### 65414 

### .L22i SubpartCb 

### 60FR**D~erJ9.** 

### 65415 

### .L22i

SubpartC 

### Emission Guidelines and Compliance l:im§ 61 

### FR 9919 

### March 12 1996

Subpart 61 

### FR 9919 March 12 1926
61 FR 9919 March 12, 1996



### 43

### FXNAL RULE/DECEHBER 20, 1996 AQ145



## Fda llm·

,

- . Subpart BcadinlfAppcudjx 

### Ruist". ;pmmulptcd· CUaUop SubartQ& 

### 61FR 

### March 29. 1926 1403J 

### Sub,partf 

### Standard' ofPerfpnnanee 

### forPortland 

### 61FR Apn13.1996 

### J4637 SuJuJart A 

### General PmvisiOM April 25.. J996 Appendix A 

### rest Methods 

### 6JFR April 

### 25, 1996 18262 SubpartI2c §liB. 

## h1a:Y 8, 1996 

### 20736



## c correctjye modification and 

### clarification are made

## as foJJ

### aws: J. 

### 40 CFR part 

### §O SUQpart A Section 

### 60.4 O!)(D, to read as follows: State 

### of Louisiana" 

### Pmprn Administrator. Air

### DuaJityDivision. LoujsianaDepartment**ofE~'** 

### yironmental 

### Quality.. Post 

## Office BOl 82135. 

## Baton**Rou~** 

### Louisiana 7088+2J35; 

## and 2. The milabilitxto 

### the public ofiofonnation 

### provided to 

### or otherwise obtajned by the 

## stateunderthis 

## Chapter shall 

### be

## eovemed byLAC 33:1 501-509. D. Copies ofdQCUments 

### ioco[P'orated by

### reference in this 

### Chapter may be**~taiOed** from the Syperintepdent QfDocuments. U S Government 

### Printi0i Office;, 

### Washington. D C, 20242 

### AUTHORITY NOTE: Promulgated 

### in accordance with R.S. 30:2054. mSTORICAL NOTE: Promulgated 

### by the Department ofEnviroMlental Quality, Office 

### ofAir Quality and·R.idiationProtection, 

### Air Quality 

### DiviSion, LR'

.....**_~_** 

### ..,... ,.



### 44

### FINAL RULE/DECEMBER 20, 1996 TIde 33 

### ENVIRONMENTAL QUALITY PartID.Air

. Chapter31. 

### Repealed la its entiret)'.

4S 

### AQ145 

### -,

# - FINAL ROLE/DECEMBER 20, 1996 Tide 33 

### ENVIRONMENTAL QU.u.nY 

### Partm.Alr

. AQ145

Chapter 60. (Editor'. Note: Chapter 60 repealed ucept for Section 6099 which 

### wiD be moved to LAC 33:m.2901.G}

•

"-,;; ',,- ",_. •••-. - ...**-.-.~..** 110" • .,k.--'

- -,-".

46

### FINAL RULE/DECEMBER 20, 1996 nde33 

### ENVIRONMENTAL QUAUTY 

### Part

## m. Air AQ145



### Chapter 'I. [Editor's Note: Chapter 'I repealed except for SubchapterA which wiD he 

### moved 

### to SubchapterN ofChapter21.]

•



### 47 _. I ."

### FrNAL RULE/DECEMBER 20, 1996 TIde 33 ENVIRONMENTAL QUALITY 

### Part ID. Air



### .... Chapter 64. Repealed 

### in its entirety•.

•



### 48 AQ145NOTICE OF INTENT

Incorporation by Reference (LAC 33:III.Chapters I, 15.21, 25,29,30,31,60,61 and 64) (AQ 145) Department ofEnvironmental Quality Office ofAir Quality and Radiation Protection Air Quality Division IV

.

Under the authority ofthe Louisiana Environmental Quality Act, R.S. 30:200 I 'et seq., and in accordance with the provisions ofthe Administrative Ptocedure Act, R.S. 49:950, et seq., the secretary gives notice that rulemaking procedures have been initiated to amend the Air Quality Division regulations, LAC 33:III.Chapters I, 15,21,25,29,30,31,60, 61 and 64 (AQI45).

This proposed rule repeals LAC 33:III.Chapters 31, 60 (except section 6099 which will be moved and renumbered as LAC 33:111:2901.0), 61 (except Subchapter A which will be moved and renumbered as SUbchapter N in Chapter 21), and 64 from LAC 33:111 and to incorporate by reference into Chapter 30 federal regulations in 40 CFR Part 60

- Standards ofPerformance for New Stationary Sources. Revisions will also be made in LAC 33:III.Chapters I, 15,21,25 and 29, so that referenced LAC cites agree with changes per this rulemaking, and to add 40 CFR references. These changes will expedite both the EPA approval process, and state implementation of delegation of authority for the NSPS program. The NSPS and the authority for EPA to delegate authority of that program to the state is established in the Clean Air Act Amendments of 1990, Section 111. This rulemaking is applicable to stationary sources statewide.

This proposed rule meets the exceptions listed in R.S. 30:2019(0)(3) and R.S. 49:953(0)(3), therefore, no report regarding environmentallhealth benefits and sociaVeconomic costs is required.

A public hearing will be held on September 26, 1996. at I:30 p.m. in the Maynard Ketcham Building, Room 326, 7290 Bluebonnet Boulevard, Baton Rouge, LA 70810. Interested persons are invited to attend and submit oral comments on the proposed amendments. Should individuals with a disability need an accommodation in order to participate please contact Patsy Deaville at the address given below or at (504) 765-0399.

All interested persons are invited to submit written comments on the proposed regulations. Commentors should reference this proposed regulation by AQ145. Such comments should be submitted no laterthan October 3, 1996, at 4:30 p.m., to Patsy Deaville, Investigations and Regulation Development Division, Box 82282, Baton Rouge, LA, 70810 or to FAX (504) 765-0486. I. ESTIMATED MPLEMENTATION COS (SAVINGS)TO STATE OR CAL GOVERNMENTAL ITS (Summary)

The est! ted implementation costs to addi g two members to the Teo er Certification Couneil is appro ately $4.000 per year, ascd on state travel regulations. The ouocH meets approxi tely 10 times ayear, based on number fappeals to be revi cd.

The stimated costs for printing this policy rcvisi n and first page fiscal and economic statement in the Louisian Register is $1 O. II. ES MATED EFFECT ON REVENUE COLLECTI NS OF Sl: TE OR LOCAL GOVERNMENTAL UNITS (Su aryl here is no effect on revenue collections of state or local ovcmmental units associated with this rule. STiMATED COSTS AND/OR ECONOMIC BENEF TS TO DIRECTLY AFFECTED PERSONS R NONGOVERNMENTAL GROUPS (Summary)

There arc no costs or economic benefits to directly affecte persons or nOJlgovemmental units associated with this rule. FISCAL AND E ONOMIC IMPA FOR MINISTRATIVE RULE TITLE: eoeber Certifieation Title 28 EDUCATION Board ofElementary and Secondary Edu alion Chapte I, Organization 1107. Bo d Appeals Council

A. Tea er Certification Appeals Council I. Co position. A Teacher Certificati Appeals Council sha be appointed by the board and sh I consist of nine membe three ofwhom shall be represe tatives from the universities one ofwhom shall be a repre ntative ofthe Parish Superint dents' Association, one of om shall be a representative of e PeT\onnel Directors' As ociation, one of whom shall be a resentative ofthe Princi Is' Association, and three of wh shall be classroo teachers. The classroom teachers hall consist of one presentative each from the Louisiana Federation of eachers, Louisiana Association of Educa rs, and the A ociated Professional Educators of Louisian The board II be responsible only for paying travel expen ofcoun I members at the state rate.

ertification Appeals Council to include a personnel a"eCIor r presentative ofthe Personnel Directors' Association and p cipal representative ofthe Principals' Association. s is revision to the Louisiana Administrative Code as no belo :

AUTHORITY NOTE: Pro ulga in accordance with R.S. 17:3(0) and R.S. 17:6(A)(9).

Interested persons may co nt on the proposed revision until 4:30 p.m. October 9,199 to: Jeannie Stokes, Board of Elementary and Secondary d cation, Box 94064, Capitol Station, Baton Rouge, LA 7 80 9064.

727 Louisiana R_g;sr., Vol. 22. No.8 Augusr 20. 1996

## (

f
v. d phrases, when used in NOTICE OF INTENT

[S

.. PriorTextl the selling and transferring 0 waste tires or rial forrecycling and/or benefici Iuse orreuse. 

## ••• Department ofEnvironmental Quality Office ofSolid and Hazardous Waste Solid Waste Division
aste Tire (LAC 33:VII.Chapter 105)(SW021 Under e authority ofthe Louisiana Environmen Quality Act, R.S. 0:200I et seq., and in accordanc with the provisions the Administrative Procedure Act, .S. 49:950, et seq., the s gives notice that rulemakin procedures have been i tiated to amend the Solid W te Division regulations, L C 33:VII.Chapter 105 (SW02 ).

The propose rule will make modificati to the Waste Tire Managemen Fund Prioritization Syste providing more equity in cleanup and make the emerg cy rule in effect permanenL The rul also provides for matical cleanup of the waste tire regula ·ons.

This proposed rul meets the exc tions listed in R.S. 30:2019(DX3) and R.

. 49:953(GX , therefore, no repan regarding environmenta ealth bene ts and social/economic costs is required.

[S

.. PriorTex'l II asphaltic co crete and concrete te highwa)'s and ro s maintained by the United States go rnment or Louisiana s te government, or cies or depanments ther f. 

## •••

[Sec: PriorTex.) Prom' ous Tire Pi/e---mt unauthorized waste 're pile that has res ted from storage or disposal activities other an the landownerwithoutthe landowner's kn 

## ••• [See Prior Text] THORITY NOTE: Promulgated in accordance 30' 411-2422. ISTORICAL NOTE: Promulgated b)' the Departmen nvironmental Quality, Office ofSolid and Hazardous Waste, S aste Division, LR 18:37 (January 1992), amended LR 20:1 (September 1994), LR 22: Richard W. England Assistant io the Legislative Fiscal Officer Gus Von Bodungen Assistant Secretary

FISCAL AND ECONOMIC IMPACT STATEMENT FORADMINISTRATIVE RULES RULE TITLE: Incorporotlon b)' Reference I. ESTIMATED IMPLEMENTATION COSTS (SAVINGS) TO STATE OR LOCAL GOVERNMENTAL UNITS (Summary)

Incorporation b)' reference eliminates the need to codif)' federal regulatory requirements. verbatim, into Louisiana regulations, and thereb)' eliminates extra volumes ofprinted regulations. The result is that the same regulations will be enforced without duplicating the printing ofthose regulations. The outcome will be savings to SlBte governmentb)' eliminating Ii volume ofregulations that would be purchased (or printed). A significant reduction in man-hours will be achieved b)' eliminating the need to type, proof. and correct federal regulations promulgated as state regUlations. 11. ESTIMATED EFFECT ON REVENUE COLLECTIONS OF STATE OR LOCAL GOVERNMENTAL UNITS (Summary)

There is no anticipated impact on revenue collections ofstate or local governmental units. III. ESTIMATED COSTS AND/OR ECONOMIC BENEFITS TO DIRECTLY AFFECTED PERSONS OR NONGOVERNMENTAL GROUPS (Summary)

Incorporation b)' reference eliminates the need to codif)' federal regulatory requirements, verbatim. into Louisiana regulations, and thereby eliminates extra volumes ofprinted regulations. The result is that the same regulations will be enforced without duplicating the printing ofthose regulations. The outcome will be a savings to the regulated community by eliminating a volume ofrcgulations that would be purchased (or printed). IV. ESTIMATED EFFECT ON COMPETITION AND EMPLOYMENT (Summary)

There is no effect on competition and employment. Copies ofthis proposed regulation can be purchased at the above referenced address and also at the Office ofthe State Register, 105 I North Third Street, Baton Rouge, LA 70802 at (504) 342-5015. Contact the Investigations and Regulation Development Division at (504) 765-0399 for pricing information. Check or money order is required in advance for each copy of AQ145.

This proposed regulation is available for inspection at the following DEQ office locations from 8 a.m. until 4:30 p.m.: 7290 Bluebonnet Boulevard, Fourth Floor, Baton Rouge, LA 70810; 804 31st Street, Monroe, LA 71203; State Office Building, 1525 FairfieldAvenue, Shreveport, LA 711 0I; 3519 Patrick Street, Lake Charles, LA 70605; 350I Chateau Boulevard West Wing. Kenner, LA 70065; 100 Asma Boulevard, Suite 151, Lafayette, LA 70508.

Gus Von Bodungen Assistanl Secretary 9605#045

728L "-JBuIHEI) NClIlNlNGS 221**J~SON** sn:tEET !.AI"A Y£TTE. 1"OUlSIAHA**~G.coltal:** ".O.8OX:P" '-NAYETT'I. LA. '7O:IOa**~ONE:** (311) 21e-e300 

### "AX:. (:II II**28~~** 

### AFFIDAVITOFPUBUCATION

In orderto
.... propercndlt. pl

....**~,.** to yourad number when making payrMRt. 

# -
- do solemnly Nearthat I., the LEGAL CLERK of 1M! ADVERTISER. • newspaperprinted Uld pUbllsJ1ed at Lafayetbl, In the Parish ofLafayltte, 

### STATE

### OF LOUISIANA PARISH

### OF LAFAYETTE

# "~Q..
State ofLoul_lana, and that from my personal knowledge and reference to the ftl

.. ofuld pubncaUon the advertisement of:

was published in THE ADVERTISER on the following dates:

# /.JwMd()tJ_...=lII:~~'-=~-LJL-I'I~9' * *

*

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Sworn to and subscribed before me this 

# d&**~ay** of

.

### a~ L...;t: ,199&

# d!h'AL~ NOTARVPCl->wIlrn und Sl1hscrihcd .\1 my "ffke in !..:lk(' Charll·s. Bet ore me. the undersignro authority. Pf!rsonaUy came and 

# State ofLouisiana

Notary Puhli('. day of

__ _ PARISH OF CALCASIEU

KATHY IGUESS

IH

__ , 

# J=_

. I

NOTICE OF INTENT A public: hearlno wi I be 

# I**~''''of** helden**~ber26.** 1996. at tal Quelllty, 0ffIc. of Air 1: 30 p.m. In**th~** Maynord

. Quality ond R.adlatlon Ketcham Bulldin;. Room' Protection, Air QUOllty 326. 7290 Bluebonnet Division. .' Boultvarcl. Bolon Rauue, La. Under1tle DUthorityat 1tIe 108!O. Interested Il8r'SClnS ore Louislano Environmental '**Invlt~** to attend oncl submIt QualifY Ad, Lo. R.S. 30:2001 oral c:omments on the**pr~ ~t**  $C!Cl•• ancl In oc:c:arClanc:e

. omendmenlS. Should wIth the provisions of the ·lndlvldualswlfl'lOdlsobility Administrative**Proc:~ure** need on ac:c:ommodation In Act, Lo. R.S. A9:950, et seq.. order to PCIrtleiPCIte olease the sKretary elv" notice contoct Patsy Deavilleat1tle that rulemakine Pr'OCedWes oddress given below or ot hOve been initioteel toornencl l500Cl 765-0399. lppeared**th~** Air Quality Division**~Ji interest~Personsore** **R~eulofionl,** LAC 33: Ill. InVited to submit written who being duly !iworn, depo!ieS and says: That he is the duly Chapters 1, 15. 21 25 29 30 comments on the PrclPOSed ' 31. 60. 61 ond' iJ lLog re;ulotlonl. Commentors authorized "-ntotTHE LAKE CHARLES AMERICAN PRESS 4tAQI45l. should**ref~renee** thls**pr~** ...... •

ThISPt"OPCIMdrulweoeals OClSltClre;ulCitionbytheLCIll

. br h d da'! . t Lak Ch! '-'.' :.AC 33:llI.ChODlel'l 31.60 #AQ1.c5. Such comments a newspaper pu lS elY a e ar eli

.....'ul:;lana.

,exeept sedi,.., 6099 which should be**submltt~** no**lat~r** (Add So 2893 Lak Ch I LA
- )('02)

....i1i be**moy~** and renum- than OCtOber 3, 1996. ot A:30 ress: X • f! ar es. I ( l**~redClS** LAC 33' 1lI.29ll1 G l p.m,. to PotSY DeovlJle ,1 (exceDt SUbehoDter'A I**n~esll;otlons** ond Reeu: , ,. . • vhleh will "'.**mov~d** Ond plotlOl'l**~~** D1vlllon. That tht> attae:hf!d

.....as pul)hshf!d III said nt>
.....spapN In ILeo enurntlrred..,£s SubchaDter N ostOffIce Box82282. Baton "l ChaDter 21). and 6A from Rouge. La., 70810 or to fox _AC 33; III oncl to ;ncorpo. (S04l CCIPift • e() d d AUG 16 1996 Cite by reference Into of this ProOClSltCl reoulation ISSU S atf!**....::~~~.:::...;::....:l'I.-..:.'O::~..l::..** _ ,:hClpter 30**~ral** reoula- eCin be Durchosed ot**th~** ,ons In 40 CFR Part 60. above**"'ferl!.llC~** oCklre5ll. ICindordSOf Performonce You.rnclYCDnt.xtthe Investj. 33756801- 

### S30 00 Jr N_Stotionary Sources Ilotlons 'ond Re;ulotion

-**"'"'"'''-=-.;..:._~:..=.~~~'o.:~** _ :evllions wlU also bemadli Development Division Cit 1 LAC 33: III.ChClPters 1. IS. I ISOAI 76:5.0399 for prlcin; 1.25 and 29. SO thOt refer' nfllrmation. ChIcltormo..v

_**nc~** LAC cites oeree With orderIS recaui...cllnCIdvonce**~anll"** wr this rulemok. for

### ea.eh COPY of AQ104S

. • g, Clnd to·odd 40 CFR ref. I ThIS ProPOSed regulation -enees. TtleSeChclnHs will Sovollabi41 tor 1rl5PeCtlon at

-------- -**~-** _ <pedlte both the EPA thefolfO'Ning DEQOffa locoOlprOvol Dracess. and stat. tlons trom 8:00 a.m. until "1Dlementation of deiello- A:30 p.m.; 7290**Bluebon~** )n ofouthOf1fY fOrthe NSPS BoulevClrd. Ath floor. Baton**I-~------------------------­** ogrom. The NSPSandfhe Rou;e. Lo. 70810; eo.. 31st Jthorlty for EPA to dele-**Str~f, Monr~,**  La. 71203; ,Ie authority of thot**pr~** Sto.te.Offlce Bulldlnll. 1525 am to the**sfot~** is estob- FCI,rfleld Avenue, Shrevehed in the Cleon Air Act DOrt. La. n 101; 3519 PCI1rlck nend"!8"'Sof 1990. SKtion Street. Loke Chorles, LCI. I. ThiS rulemClkjng Is 70605; 3501 ChoteCiu**Boul~-** plicCible to StOlionory 7 vO ord WestWlnll. Kenner, LCI. Jrces stoTewide_ 0,65; 100 AsmCi Boulevard. This proposed rule meets Su,te 151. LafaYette. La. ,exceptions liSTed in R S 70506. 2019 (D) (J) and R."S: ;**GU~** Von BDdungen, 953 CG) (3), therefore. no ' ASSISTanT secreTorY, 'ort regarding environ-I AUgUSI16. .IT ntallheolth bene/its Clnd 118.16.05 :lal/economiC costs is I Louisiana. Ihis 

# ""1 '

LAST0100

### GANNETT CO.'INC. Publisher of

The hereto attached advertisement

dally newspaper of general circulaAD 

# ,

# mACiD~ Th.e News-Star MONROE, LOUISIANA. PROOF OF PUBLlCATION

was published in The N EWS-5TAR, a

Parish of Ouachita, in the Issues of:



# (ly..f;uBf tion, published In Monroe, Louisiana,

the person whose signature appears above in M.onroe, La. on this Sworn and subscribed before me by



# --1-/

....... 

# 1_.

__day

# Of~~9V

563800 HOWARD AVENUE, NEW ORLEANS. LOUISIANA 70140-1097 TELEPHONE (504) 826-3206


### State of Louisiana Parish of Orleans

P.O. Box 82282

3800 Howard Ave

.. 

### City of New Orleans

August ] 4. 1996 Legal. 

### Notices: 

### Personally**app~ared** 

### before me, a Notary in and for the parish of Orleans, Robert-J. Chiasson who deposes and says that he is the Accounts Receivable Manager, of the Times-Picayune Publishing Corporation, a Louisiana Corporation, Publishers of The Times-Picayune, Daily and Sunday, of general circulation; doing business in the City of New Orleans and the State of Louisiana, and that the attached

Sworn to and subscribed before me this Baton Rouge, Ia. 

### 70804 

### l&:RlilEIiiiikiiiq iiroeedures have been initiated to anend the 

### Air Quality 

### Division Regulations UC 33 :U1. Cbapt 

### 1, 

### 15, 25, 29, 30, 31, 60, 61, & 

### 64 Log NO. 

### AQ145 Advertisement of Investigation & Requa1t.ian

New 

### orleans, La. 

### 70Jr40 Was published in b 

### Times Picayune

on the following dates

---:1::..:4=.=th:.::-

__ dayof August A.D.. 19_ 9

_ 6

__

# No(M~1 My commission expires at my death.**FOA"1~**

C EAST JEFFERSON I

_._----- 

## --------

# llliJ .. STATE OF LoUISIANA PARISH OF CADDO

August 25, 1996 Before me, the uodentped authorltJ. perIODIlly came aDd appeared 

### PROOF OF PUBLICATION

Advertising MaDagerof'l11eTimes. aDd thatthe attacbed advertismeateatitled:

NOTICE OF INTENT- Department of Environmental**QU~** Office of Air Quality and Radiation Prot;ection Air QUa]ft;y Division (Log 

# * AQ145) t:f=. 

### V43-9 '}- otf9 tome. wbobeiDgduly

### sworn. deposesaDdsaysthatsheIstheAaslstaDttotheCIasslfled

following datestowit: ....,jAc...LJ 1tl..J

h u;e

....

"'i:lsl."",JC_c.L..I.I·tt:

......

n ol.l n ..... I perscma1Iy bawD

as per copy of advertisement bereto anDeJ:ed. was published in The Times OD the

SWOrDto aad subscribed before me**thlolll1lli.~**__**26_~dlAa,yo'"'f**__ A-u

.... g_u_st •19--!6

### · .' 

### CAPITAL CITY PRESS Publisher of

Sworn and subscribed before me by the person

Indefinite 

### THE ADVOCATE PROOF OF PUBLICATION

My Commillion Expires:



## ..

1007797 V03-97-046, AQ145 

### whose signature appears above in Baton**~uge,** 

### La. on this AUGUST 96 

### day of AD. The hereto attached notice was published in THE ADVOCATE, a daily newspaper of general circulation, published in Baton Rouge,

### louisia~ na and the Official Journal of the State of

### Lo~isiana, the City of Baton Rouge and the Parish of East Baton Rouge, in the issues of:2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 I 29 

### I 30 

## I il DEPARTMENT OF ENVIRONMENTAL QUALITY AIR QUALITY REGULATIONS

- LOG NO. AQ145 PUBLIC HEARING SEPTEMBER 26, 1996

HR. SKY-PECK, Good afternoon. My name is Steve Sky-Peck. I'm employed with the Louisiana Department of Environmental Quality. I'll be serving as Hearing Officer this afternoon to receive comments regarding proposed amendments to the Air Quality, Solid waste and Water Quality Division regulations. The comment period for these amendments began on August 20, 1996, when the Notice of Intent was published in the Louisiana Register. The comment period will close at 4:30 p.m., October 3, 1996. It would be helpful to us if all oral comments received today were followed up in writing. This public hearing provides a forum for all interested parties to present comments on the proposed changes. I'll ask that each commenter begin by stating their name and affiliation for the record. The first amendment is designated by Log No. AQ14S. This rule-making proposes to repeal LAC 33, Part III, Chapters 31, 60, except for sections 6099, 61, except subchapter A, and 64, from LAC 33, Part III, and to incorporate by reference into Chapter 30, federal regulations in 40 CFR Part 60, the standards of performance for new stationary sources. Revisions will also be made in LAC 33, Part ·111,

-1-

ACADIANA REPORTING SERVICE 9498 HOOPER ROAD BATON ROUGE. LOUISIANA 70818 ""041261 -93562 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 Chapters 1, 15, 21, 25, and 29, so that referenced LAC cites agree**wi~h** changes per this rule-making and to add 40 CFR references. These changes will expedite both the EPA approval process, and State**impl~mentation** of delegation of authority for the NSPS Program. The NSPS and the authority for EPA to delegate authority of that program to the State is established in the Clean Air Act Amendments of 1990, Section 111. This rule-making is applicable to stationary sources statewide. If the rule is not adopted, U. S. EPA must continue to review each regulation, new and revised, in detail for possible deficiencies prior to giving Louisiana approval for delegation. This would significantly delay the delegation of authority to implement the regulation

as adopted into Louisiana law. Louisiana would also fail to meet its 1995-96, and 1996-97 EPA grant ob1ectives related to this rulemaking, and to delegation revisions. The State must continue to print volumes of regulations that are not significantly different from the federal regulations on which they are based. An industry must continue to use 23 two sets of regulations which may contain only slightly 24 different recordkeeping and reporting requirements. 25 Our comments will begin with Richard Metcalf. 26 MR • METCALF. 27 26 29 30 Good afternoon. My name is Richard Metcalf. I'm the Health, Safety and Environmental Affairs Coordinator for the Louisiana Mid-Continent Oil and Gas Association. Mid-Continent is an industry organization which
-2-

ACADIANA REPORTING SERVICE 94ge HOOPER ROAO BATON ROUGE, LOUISIANA 70B18 <;04/21'i I ·93'562 3 4 5 6 7 8 g 10 11 12 13 14 15 16 17 18 Ig 20 21 22 23 24 25 26 27 iI 28 :1 I· 2g :1 30 

### II :1 :1 :1 

### il 'I I, 

### II II l' :1

" represents individuals and companies that together produce, transport, refin! and market approximately 90 percent of the oil and"natural gas in Louisiana. Virtually all of Mid-Continent members are affected by the EPA and State New Source Performance Standards. Mid-Continent strongly supports the Department's strategy to adopt the federal rules by reference. We • believe this strategy will provide efficiencies for both the State and for industry in the implementation of these regulations. It is Mid-Continent's understanding that when the Department adopts rules by reference, or these rules by reference, the Department 'must also respect the interpretations and guidance given by the EPA in any formal preambles or background documents. Mid-Continent would like for the Department to state this in the response to comments. Once again, Mid-Continent strongly supports the adoption of this regulation and the opportunity to provide these comments. Thank you. HR. SKY-PECK.**~hank** you. Does anyone else care to comment On AQ145? (No response.) If not, the hearing on AQl45 is closed. I'd like to thank you all for your attention and participation. CERTIFICATE 1, MARGARET MORVANT, Certified Court Reporter, do hereby certify that the foregoing testimony was heard before the Honorable Steve Sky-Peck, Hearing Officer, on
-3-

ACADIANA REPORTING SERVICE 9498 HOOPER ROAO BATON ROUGE. LOUISIANA 708' B ",041215**1·~356**2 3 4 5 6 7 8 9 10
11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 September 26, 1996, in Room 326, Maynard Ketcham Building, Baton Rouge, Louisiana; that I did report the proceedings thereof; that the foregoing pages, numbered 1 through 4, inclusive, constitute a true and correct transcript of the proceedings thereof.

-4-

ACAOIANA REPORTING SERVICE 9496 HOOPER ROAD SATON ROUGE. LOUISIANA 70616 "',0,",'211; I -9J56

### Comments Submitted For Incorporation by Reference

- 40 CFR. 

### Part 60 LAC 33:m.Chapters 1, 15, 21, 25, 29, 30, 31, 60 Log 

### # 

### AQI4S -4',',--,

COMMENT 

### # 1 and 2 

### SUBMIllJID BY 

### Richard Metcalf I 

### L>uisiana MidContinent Oil and Gas AssociationCOMMENT 1:

RESPONSE 1: COMMENT 2:

RESPONSE 2: Comments Submitted For Incorporation by Reference

- 40 CFR 

### Part 60 LAC 33:ID.Cbapters 1, 15, 21, 25, 29, 30, 31,-60

. Log # AQ145 General. The commentor supports the adoption of the regulation by reference. The adoption of 

### the regulation by reference reduces the burden to implement these regulations because it reduces the amount of time to prepare and review proposed amendments to the NSPS regulations at the state level. No response required. General. It is suggested that the department confirm in the response to comments that the department must respect the interpretations/guidance given by the EPA in any formal preambles or background documents associated with the rule being adopted. This clarification would ensure that the department could not interpret a provision more strictly than the EPA and impose costs to the regulated community in excess of the EPA regulations. The Department of Environmental Quality (DEQ) agrees to follow all interpretations, past and future, made by EPA of40 CFR part 60, when part 60 standards are incorporated by reference and delegated allthority by the straight delegation mechanism. A statement of such agreement will be contained in the "Terms and Conditions" of the delegation Agreement to be signed by EPA and DEQ.