('.l)al-. I"!,#1:.)/- CHAIN OF CUSTODY

Project I Sample Location: - -

Coal~Fired Boilers 1 and 2

Copy (1 of 4)

Client / Project Name:

TransAlta Centralia Generation

Project No.

10072.2p

Sent Analytical Report To:

Kevin Donahoe (kdonahoe@avogadrogroyp,com)

Purchase Order No. Quote No.

Test / Analytical Method:

EPA UtilitylCR: various ASTM, SW-846, and EPAMethods

Special Analysis / Reporting Instructions: _

Group 1: Proximate / Ultimate, Chlorine

Group 2:Proximate/ Ultimale;Chlorine, Fluorine

Group 4: Proxima Ie I UII/mate, Chlorine, merCllry, total

selected metals (As, Be, Cd, Co, Cr, Pb, Mn, Ni, Sb), Se

Run / Sample # Date Time Containers Lab / Sample ID #

1-fuel-1 3/23/10 600 1

1-fuel-2 3/23/10 600 1

2-fuel-1 3/23/10 2045 1

2-fuel-2 3/23/10 2045 1

3-fuel-1 3/24/10 530 1

3-fuel-2 3/24/10 530 1

4-fuel-1 3/24/10 1800 1

-fuel-2 3/24/10 1800 1

-fuel-1 3/25/10 600 1

-fuel-1 3/25/10 1800 1

Moisture, HHV, Sulfur, Ash,Volatile, Carbon, Nitrogen): ASTM 03302, 04239, 05865, 05142,05373

072 -45044 -0 0 1-------------------- 072 -45 044 ..0 10

Be, Cd, Co, Cr, Pb, Mn, Ni, ASTM 06357 1-fuel-1 --~----- 6-fuel-1

~JewCustomer None -- ------------- New Customer None

---- ----------- Due 04/21/20'10 Rec 04/08/201 0= ~ ~~~~~:~Due: 04/21/2010 Rec: 04/08/2010

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Date Time

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Relinquished by: (signature) Date Time Received by: (signature) Date Time

Yt:J'" no"

Billing:

The Avogadro Group, LLC

2825 Verne Roberts Circle

Antioch, CA 94509

Phone - (925) 680-4300

Fax - (925) 680-4416

Shipping / Questions:

The Avogadro Group, LLC

3003 SW 153rd Dr. Ste. 215

Beaverton, OR 97006

Phone - (503) 658-2091

Fax - (503) 427-1153

Preliminary results due: 4/19/"10

Final lab report due:
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2-HCI-1

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3-HCI-1

1-HCI-2

2-HCI-2

3-HCI-2

4-HCI-2

RB-HCI

Total Containers

3/25/10

3/25/10

3/23/10

3/23/10

3/24/10

3/24/10

3/22/10

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1

1

2

2

2

2

2

2

1

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CHAIN OF CUSTODY

Fraction 1 - (Impingers <1-2> contents, BY2rinse)

Fraction 2 - (Impingers <3-4> contents and rinses)

Same as Run 1

Same as Run 1

Same as Run 1

Same as Run 1

Same as Run 1

Same as Run 1

Reagent blank

Reagent blank

O.iN H2S04

2N NaOH

0.1 N H2S04

2N NaOH

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lng:

The Avogadro Group, LLC

2825 Verne Roberts Circle

Antioch, CA 94509

Phone - (925) 680-4300

OJ)

Shipping / Questions:

The Avogadro Group, LLC

3003 SW 153rd Dr. Ste.215

Beaverton, OR 97006

Phone - (503) 658-2091

Analysis due:

Final lab report due:

4/22/10
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1-MM 1 Container 1- (filter)

1 Container 3 - (front-half rinse -1 Op ml) 0.1N HN03

1 Container 4 - (Impingers 1-3 contents and 100 mL rinse) 5% HN03/10% HzOz

3 same fractions as Run 1

3 Same fractions as Run 1

3 Same fractions as Run 1

3 Same fractions as Run 1

3 Same fractions as Run 1

1 Container 3 - (front-half rinse - 100 mL)

1 Container 4 - (!mpingers 1-3 contents and 100 mL rinse)

1 Reagent blank - 300 mL

11 '\ Reagent Reagent blankblank - 200 ml

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2-MM-1

3/25/10

3-MM-1 12

3/23/10

3-MM-2 2

3/24/10

FB-MM

3/23/10

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CHAIN OF CUSTODY

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0.1N HN03

5% HN03/1 0% HzOz

0.1N HN03

5% HN03/1 0% HzOz

Filter

Total Containers

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Final lab report due: en

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23

ling: '§~iPPing / Questions~ - t) 1 S)

The Avogadro Group, LLC The Avogadro Group, LLC Preliminary results due:

2825 Verne Roberts Circle 3003 SW 153rd Dr. Ste.215

Antioch, CA 94509 Beaverton, OR 97006

Phone - (925) 680-4300 Phone - (503) 658-2091

_____________________________________ • ,_r-_r.·' _u~_~ ~ --

CORPORATEHEADQUARTERS

12423 NE WhitakerWay

Portland,OR97230

Phone:(503)254-1794 Fax: (503)254-1452

PYXIS LABORATORIES, LLC

CHAIN OF CUSTODY RECORD

CENTRALOREGONBRANCH

2392 S. Hwy 97, SuiteB

Redmond,OR 97756

Phone: (541) 390-2372

Page of _

Some or all of this analyses may be

subcontracted to an ORELAP

accredited laboratory.

Company: ,hp; L1 ~-"r;,- J___Jl'Jr:"t .,1 ) Lr-: Analysis Requested

Purchase Order Number:

Pro~ect Number: f DO 7) .,::' ~J 

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PrOject Name: T ("0'1/15 4I./.-J:! :r~~

17000c'> )1

~ Email Results

0 State Compliance Format 

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Fax Preliminary Results 0

Fax Final Results 0

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0 Verbal Results:

Other: 

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Date/Time Collected Matrix Comments #Btls Loc ID

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Relinquished By:

Time Date /R~Y1() gate

Laboratory Use Only:

~/E./ .-Custabbr: /:?O~ I:?.f> ~L1 ,-?1z/:/;'7 '311///10 ~~ iZ//~

/ I I .' I I II 7 •..... Job Number:

o Proper Container 

oo Temperature Sample Condition 4+ 2°C

o Shipped Via:

D Cash/Check/CC/Net 30/

SUBMISSION OF SAMPLES WITH TESTING REQUIREMENTS TO PYXIS WILL BE UNDERSTOOD TO BE AN AGREEMENT FOR SERVICES

IN ACCORDANCE WITH THE CONDITIONS LISTED ON THE BACK OF THIS FORM.