# Quarterly Groundwater Monitoring Report – Outside (Non-Tunnel) Wells Red Hill Fuel Storage Facility Pearl Harbor, Oahu, Hawaii Latitude: 21 o

# 22’15” N Longitude: 157o

# 53’33” W
HDOH Facility ID No. 9-102271 HDOH Release ID No. 99051, 010011, 020028
April 2010

Prepared by:

TEC Inc. 1003 Bishop St. Suite 1550 Pauahi Tower Honolulu, Hawaii 96813

Prepared for:

Commander Navy Region Hawaii Environmental Department, Code N45 850 Ticonderoga Street, Suite 110 Pearl Harbor, Hawaii 96860-5101

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility April 2010

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## i 

# Table of Contents
Table of Contents

............................................................................................................................. i Executive Summary......................................................................................................................... 1 1.0 Introduction.......................................................................................................................... 3 1.1 Project Objective ............................................................................................................. . 3 1.2 Previous Reports ..............................................................................................................3 1.3 Background .................................................................................................................... .. 4 1.3.1 Site Description......................................................................................................... 4 1.3.2 Facility Information.................................................................................................. 4 1.3.3 UST Information....................................................................................................... 5 1.4 Regulatory Updates .......................................................................................................... 6 2.0 Sample Collection and Analyses.......................................................................................... 6 2.1 Monitoring Well Purging ................................................................................................. 6 2.2 Groundwater Sample Collection ...................................................................................... 7 2.3 Groundwater Sample Analyses ........................................................................................ 7 3.1 January 2010 Sample Analytical Results ......................................................................... 7 4.0 Summary and Conclusions................................................................................................... 9 5.0 References.......................................................................................................................... 11
List of Tables Table 1 Monitoring Well Information ........................................................................................5 Table 2 Analytical Results for Quarterly Groundwater Sampling (January 26, 2010) ...............8 List of Figures Figure 1 Groundwater Monitoring Well Locations ....................................................................10 List of Appendices Appendix A – Laboratory Analytical Reports Appendix B – Monitoring Well Construction Logs

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## 1 

# Executive Summary This quarterly groundwater monitoring report presents the results of groundwater sampling conducted on January 26, 2010 at locations surrounding the United States (US) Navy Bulk Fuel Storage Facility at Red Hill, Oahu, Hawaii (the Facility). The sampling and reporting was conducted by TEC Inc. (TEC) for the Fleet and Industrial Supply Center (FISC) at Pearl Harbor, Hawaii. This report is part of a series of quarterly groundwater monitoring reports, supplemental to the groundwater reports for the groundwater monitoring wells within the Facility, provided by the US Navy to the State of Hawaii Department of Health (HDOH) in accordance with HDOH’s release response requirements. Currently, there are 18 active and two inactive, 12.5 million gallon, field-constructed underground storage tanks (USTs) located at the Facility. Background In 2002, the US Navy installed a groundwater monitoring well (cur rently named RHMW01) into the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. Groundwater samples from this wellindicated that petroleum from the Facility has migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 2254-01. US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from the Facility USTs and provides approximately 24% of the potable water to the Pearl Harbor Water System (PHWS). By September 2005, the US Navy had installed two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facility UST system and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 2005, these wellshave been sampled quarterly for Total Petroleum Hydrocarbons (TPH) quantified as DieselRange Organics (DRO) and Gasoline Range Organics (GRO), Volatile Organic Compounds (VOCs), Polynuclear Aromatic Hydrocarbons (PAHs), and dissolved lead. In response to increasing concentrations of contaminants of potential concern at the groundwater monitoring wells within the facility (specifically RHMW02) during 2008, plans were made to conduct quarterly sampling at the following monitoring well locations:

 RHMW04, north of the Facility’s tank 20;

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01); and

 Halawa Deep Well 2253-03 (referred to as HDMW2253-03 in this report). During the summer and fall of 2008, HDOH updated their Environmental Action Levels (EALs), which resulted in significant changes to the action levels associated withmethylnaphthalenes. The HDOH Drinking Water toxicityEAL for these compounds was 240 g/L. This concentration assumed that methylnaphthalenes were not human carcinogens. Once evidence emerged and was accepted by the US Environmental Protection Agency (USEPA) that methylnaphthalenes are carcinogenic to humans,HDOH adopted more rigorous EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene (HDOH, 2008).

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## 2 The HDOH Drinking Water EAL for naphthalenewas also updated during this process. Previously, HDOH based their naphthalene EAL on US Environmental Protection Agency (USEPA) Region 9 Preliminary Remediation Goal (PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index (HI) of 1. The USEPA generally considers a Hazard quotient (HQ) of 1.0 or less to be acceptable. For multiple chemicals or fractions at an exposure point (e.g. for a monitoring well) a HI is calculated by summing the HQs. In deference to the California Department of Public Health’s Drinking Water Notification Levels, (HDOH, 2008) HDOH updated their naphthalene drinking water EAL to 17 g/L. Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 g/L, although the Groundwater Gross Contamination EAL for TPH-DRO remains 100 g/L.
Current Results On January 26, 2010, three groundwater samples (i.e., RHMW04, OWDFMW01, and HDMW2253-03), along with the required quality control samples (duplicate, matrix spike, and matrix spike duplicate) were collected for analysis. Samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead.
TPH-DRO was detected at 322F μg/L [F indicates that the compound was identified at a concentration above the method detection limit (MDL), but below the reporting limit (RL), therefore is considered an estimate] in HDMW2253-03, and 1,490 μg/L in OWDFMW01. These values are above the HDOH Drinking Water EAL (i.e., 210 μg/L) and the HDOH EAL for Gross Contamination (i.e., 100 μg/L). No other HDOH Drinking Water EALs were exceeded and no other contaminants of concern were detected above the laboratory MDL.
Conclusions and Recommendations Excluding the January 2010 sampling event, TPH-DRO results from the two most recent sampling events at OWDFMW01, conducted in October 2009 and August 2009, were non-detect (i.e., TPH-DRO was not detected above the MDL). Likewise, excluding the January 2010 sampling event, TPH-DRO results from the most recent sampling event at HDMW2253-03, conducted in October 2009 were non-detect. HDMW2253-03 was not sampled in August 2009 due to access issues. Although a trend (i.e., two or more consecutive events of detectable concentrations) of TPH-DRO for OWDFMW01 and HDMW2253-03 has not yet been established, careful attention should be given to subsequentsampling events regarding the presence of TPH-DRO. Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead should continue at the Facility untilsuch time that data indicates that a different monitoring plan is warranted. The next quarterly groundwater sampling event will be performed in April 2010.

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## 3 

# 1.0 Introduction This report presents the resultsof the third groundwater sampling event, conducted in January 2010 at two groundwater monitoring wells (i.e., RHMW04 and OWDFMW01). The first and second sampling events for OWDFMW01 were conducted in August and October 2009 respectively. In addition, thisreport presents data from the second sampling event conducted in January 2010 at HDMW2253-03. The first sampling event at HDMW2253-03 was conducted in October 2009. An August 2009 sampling event for HDMW2253-03 was not conducted due to access issues.
These three wells surround the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). The Facility consists of 18 active and two inactive USTs operated by FISC, Pearl Harbor. This groundwater sampling and analysis event issupplemental to the quarterly groundwater sampling and analysis at groundwater monitoring wells within the Facility(i.e., part of the groundwater monitoring program for the UST site in response to past UST releases, previous environmental investigations, and recommendations from the HDOH). 

# 1.1 Project Objective This groundwater sampling project was performed to evaluate the presence of chemicals of potential concern in groundwater surrounding the Facility. The project was conducted to ensure the Navy remains in compliance with HDOH UST release response requirements. The groundwater sampling program followed the procedures described in Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan[TEC Inc. (TEC), 2008 updated in 2009], also referred to as “the Plan”. This groundwater sampling event was conducted by TEC under US Navy Contract Number N47408-04-D-8514, Task Order No. 54, Amendment/Modification No. 01. 

# 1.2 Previous Reports This is a quarterly sampling event that is being conducted to supplement the quarterly groundwater sampling and analysis at groundwater monitoring wells within the Facility, which began in 2005. The following groundwater monitoring reports were previously submitted to the HDOH, for groundwater monitoring wells within the Facility:

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 8. Groundwater Monitoring Results, June 2007 (submitted August 2007);

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## 4 9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 13. Groundwater Monitoring Results, October and December 2008 (submitted February 2009); 14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 15. Groundwater Monitoring Results, May 2009 (submitted July 2009); 16. Groundwater Monitoring Results, July 2009 (submitted September 2009); and 17. Groundwater Monitoring Results, October 2009 (submitted December 2009). The following groundwater monitoring reports were previously submitted to the HDOH for groundwater monitoring wells outside the Facility:

1. Groundwater Sampling Results, August 2009 (submitted September 2009); and 2. Groundwater Monitoring Results, October 2009 (submitted December 2009). 

# 1.3 Background The following sections provide a description of the site and information on the Facility and USTs.
1.3.1 Site Description The Facility is located in Red Hill, Oahu, Hawaii. Land adjacent to the north of the Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east of the Facility (Dawson, 2006). The Navy Public Works Department operates a potable water infiltration tunnel approximately 1,550 feet from the Facility (Dawson, 2006) . The US Navy Well 2254-01 is located approximately 3,000 feet west of the Facility and provides approximately 24% of the potable water to the Pearl Harbor Water System, which serves approximately 52,200 military consumers (TEC, 2008).
1.3.2 Facility Information The Facility consists of 18 active and two inactive USTs operated by Navy FISC Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006). In 2002, the US Navy installed a groundwater monitoring well (cur rently named RHMW01) into the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. Groundwater samples from this wellindicated that petroleum from the Facility has migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the

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## 5 aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 2254-01. By September 2005, the US Navy had installed two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facility UST system, a background groundwater monitoring well (RHMW04) north of the Facilityadjacent to the US Navy Firing Range, and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 2005, RHMW01, RHMW02, RHMW03, and RHMW2254-01 have been sampled quarterly for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. Due to increasing concentrations of contaminants of potential concern at the groundwater monitoring wells within the Facility (specifically RHMW02) during 2008, response measures were warranted. In April 2009, another groundwater monitoring well (RHMW05) was installed within the lower access tunnel between RHMW01 and RHMW2254-01. It was installed to identify the extent of contaminant migration before it reaches the infiltration gallery at RHMW2254-01. Additionally, plans were made to sample three monitoring wells surrounding the Facility, RHMW04, OWDFMW01, and HDMW2253-03. RHMW04 was installed to provide geochemistry for water moving through the basal aquifer beneath the Facility. OWDFMW01 (originally known as MW08) was installed into the basal aquifer in 1998 for a Phase II Remedial Investigation/ Feasibility Study for the Red Hill Oily Waste Disposal Facility (Earth Tech Inc., 2000). It is located geographically down-gradient of the USTs and US Navy Well 2254-01. HDMW2253-03 is controlled by the State of Hawaii Commission on Water Resource Management. It is located between the Facility and the municipal drinking water supply well run by the City and County of Honolulu Board of Water Supply (Halawa Shaft pumping station 2354-01). Table 1 summarizes basic groundwater monitoring well information, Figure 1 shows groundwater monitoring well locations, and Appendix B includes the well construction logs for RHMW04 and OWDFMW01. Table 1. Monitoring Well Information

Groundwater Well TOC Elevation (ft msl) DTW (ft) TD (ft)

RHMW04 313.03 293 320 OWDFMW01 138.94 120 142.8 HDMW2253-03 225 210 1,575 Notes: DTW - Distance to water TD- Total depth of well TOC- Top of casing ft – Feet ft msl- Feet from mean sea level



## 1.3.3 UST Information The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently contain Jet Propulsion (JP)–5 fuel, JP-8, and F-76 (diesel marine fuel). Previously, several tanks stored Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank

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## 6 measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the tanks lie at depths varying between approximately 100 feet and 200 feet below the existing ground surface (TEC, 2006). 

# 1.4 Regulatory Updates During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant changes to the action levels associated with methylnaphthalenes. The drinking water toxicity EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the US Environmental Protection Agency (USEPA).As a result, HDOH adopted more rigorous EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). The drinking water EAL for naphthalene has also been updated during this process. Previously, HDOH based their naphthalene EAL on United States Environmental Protection Agency (USEPA) Region 9 Preliminary Remediation Goal (PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index (HI) of 1. The USEPA generally considers a Hazard Quotient (HQ) of 1.0 or less to be acceptable. For multiple chemicals or fractions at an exposure point (e.g. for a monitoring well) a HI is calculated by summing the HQs. HDOH has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California Department of Public Health’s Drinking Water Notification Levels, a HI of 2.7 (HDOH, 2008). Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 100 g/L. 

# 2.0 Sample Collection and Analyses Field activities relating to groundwater sample collection were conducted on January 26, 2010. Groundwater samples were collected from three monitoring wells, RHMW04, OWDFMW01, and HDMW2253-03. Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan(TEC, 2008). A total of six samples were collected as follows:

 one environmental sample from RHMW04, OWDFMW01, and HDMW2253-03;

 one duplicate sample from RHMW04 (sampled as RHMWA01 and reported as RHMW04D); and

 one matrix spike and matrix spike duplicate from OWDFMW01. 

# 2.1 Monitoring Well Purging RHMW04 and OWDFMW01 were purged prior tosampling. Well purging was considered complete when no less than three successive water quality parameter measurements had stabilized within approximately 10 percent. Field parameters were measured at regular intervals during well purging and includedpH, temperature, specific conductivity, dissolved oxygen, and turbidity. Due to the well construction characteristics of HDMW2253-03, the well was not purged prior to sampling, but field parameters were recorded. Rather than purging, a grab

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## 7 sample was collected at a depth below the solidcasing (which extends about 50 feet below the water table) and within the open-holed portion of the well. 

# 2.2 Groundwater Sample Collection Immediately following purging, RHMW04 was sampled directly from a dedicated bladder pump system, and OWDFMW01 was sampled using a disposable bailer. HDMW2253-03 was sampled using a disposable bailer designed to collect samples at desired depths. Samples were placed into sampling containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile organic analysis, nitric acid (HNO3

## ) for dissolved lead]. Dissolved lead samples were filtered in the field and placed in preserved bottles. Sample containers were labeled with the date, sample identification number, type of analysis, and sampler’s name. The containers were placed on ice in sample coolers and transported under chain-of-custody procedures to the certified laboratory for analysis. 

# 2.3 Groundwater Sample Analyses Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

# 3.0 Groundwater Sample Analytical Results This section provides a summary of analytical results for groundwater samples collected from three monitoring wells, RHMW04, OWDFMW01, and HDMW2253-03. Duplicate sample results from monitoring well RHMW04 are reported in this document as RHMW04D. A summary of groundwater analytical results for TPH-DRO and TPH-GRO, VOCs, PAHs, and dissolved lead is included in Table 2. Completeanalytical laboratory reports are provided in Appendix A. 

# 3.1 January 2010 Sample Analytical Results All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. The results for each groundwater monitoring well are discussed below.
RHMW04 No potential chemical of concern was detected above the laboratory MDLs in RHMW04 (Table 2).
OWDFMW01 TPH-DRO was detected at 1,490 μg/L, exceeding the HDOH Groundwater Gross Contamination EAL and Drinking Water EAL (i.e., 100 μg/L and 210 μg/L, respectively). No other potential chemical of concern was detected above the laboratory MDLs in OWDFMW01 (Table 2).
HDMW2253-03 TPH-DRO was detected at 322F μg/L [F indicates that the compound was identified at a concentration above the MDL, butbelow the reporting limit (RL), therefore is considered an estimate], exceeding the HDOH Groundwater Gross Contamination EAL and Drinking WaterPage 1 of 1 Table 

. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (January 26, 2010)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL TPH as DIESEL RANGE ORGANICS 210 100 **322** F 172 460 **1490** 165 440 ND U 167 444 ND U 165 440 TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100 ND U 30 100 ND U 30 100 ND U 30 100 1-METHYLNAPHTHALENE 4.7 10 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 2-METHYLNAPHTHALENE 24 10 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 ACENAPHTHENE 370 20 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 ACENAPHTHYLENE 240 2000 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 ANTHRACENE 1800 22 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 BENZO(a)PYRENE 0.2 0.81 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 CHRYSENE 9.2 1 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 FLUORANTHENE 1500 130 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 FLUORENE 240 950 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 NAPHTHALENE 17 21 ND U 0.0517 0.167 ND U 0.0332 0.107 ND U 0.0337 0.109 ND U 0.0348 0.112 PHENANTHRENE 240 410 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 PYRENE 180 68 ND U 0.025 0.0833 ND U 0.016 0.0535 ND U 0.0163 0.0543 ND U 0.0169 0.0562 1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 NAPHTHALENE 17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 XYLENES, TOTAL 10000 20 ND U 1 2 ND U 1 2 ND U 1 2 ND U 1 2 6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit VOCs - Volatile organic compounds RL - Reporting limit UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method detection limit U - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzed F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs 1

2 UG/L Method HDOH Drinking Water EALs 1 for Human Toxicity UG/L HDOH Groundwater Gross Contamination EALs2 UG/L Chemical HDMW2253-03 UG/L January 26, 2010 January 26, 2010 January 26, 2010 OWDFMW01 UG/L RHMW04 UG/L RHMW04DFinal Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009 Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009 8015B (Petroleum)

8270C SIM

(PAHs)

8260B (VOCs) January 26, 2010

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## 9 EAL (i.e., 100 μg/L and 210 μg/L, respectively). No other potential chemical of concern was detected above the laboratory MDLs in HDMW2253-03 (Table 2). 

# 4.0 Summary and Conclusions Summary TPH-DRO was detected above the laboratory MDLs, HDOH Drinking Water EALs, and Gross Contamination EALs in OWDFMW01 and HDMW2253-03. No other potential chemical of concern was detected above the laboratory MDLs in OWDFMW01, HDMW2253-03, or RHMW04.
Conclusions/Recommendations Excluding the January 2010 sampling event, TPH-DRO results from the two most recent sampling events at OWDFMW01, conducted in October 2009 and August 2009, were non-detect (i.e., TPH-DRO was not detected above the MDL). Likewise, excluding the January 2010 sampling event, TPH-DRO results from the most recent sampling event at HDMW2253-03, conducted in October 2009, were non-detect. HDMW2253-03 was not sampled in August 2009 due to access issues. Although a trend (i.e., two or more consecutive events of detectable concentrations) of TPH-DRO for OWDFMW01 and HDMW2253-03 has not yet been established, careful attention should be given to subsequentsampling events regarding the presence of TPH-DRO. Consideration should be given to installing additional groundwater monitoring wells at strategic locations to better assess whether or not increases of TPH-DRO at OWDFMW01 and HDMW2253-03 may be attributed to the Facility. Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead should continue at the Facility untilsuch time that data indicates that a different monitoring plan is warranted. The next quarterly groundwater sampling event will be performed in April 2010.

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility April 2010

____________________________________________________________________________________________



## 11 

# 5.0 References AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC Pacific, August 2002. Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sam pling Report, Red Hill Fuel Storage Facility, Hawaii.February 2006.
Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily Waste Disposal Facility, Halawa, Oahu, Hawaii. September 2000.
Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7.

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, Summary Lookup Tables. March 2009.

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground Storage Tank Sites. Memo. July 2005.

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and Groundwater. Summer 2008 (updated October 2008).
TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl Harbor, Hawaii.May 2006.
TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl Harbor, Hawaii.January 2008 revised in December 2009.

# Appendix A Laboratory Analytical Reports

## SGS Work Order:

Contents: Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS North America Inc. Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 3354-010 Red Hill BFSF The Environmental Company, Inc. (TEC) 1100319

## CASE NARRATIVE Print Date: 2/5/2010

Workorder No.: 1100319 Project Name: 3354-010 Red Hill BFSF Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID 

## Sample Comments

Sample Type Client Sample ID Refer to the sample receipt form for information on sample condition.

1100319001 DRO by 8015C - Unknown hydrocarbon with several peaks is present.

PS OWDFMW01-WG-03

1100319002 AK101 - MS recovery does not meet QC criteria.See the LCS/LCSD for precision and accuracy.

8260B - MS recovery for 1,1-dichloroethane, cis-1,3-dichloropropene and methyl-t-butyl ether does not meet QC criteria (biased high). See LCS for accuracy. 8270D SIM - MS recovery is outside of QC criteria for fluoranthene (biased high). Refer to LCS for accuracy. BMS OWDFMW01-WG-03 MS

1100319003 AK101 - MSD recovery does not meet QC criteria.See the LCS/LCSD for precision and accuracy.

8260B - MSD recovery for 1,1-dichloroethane and methyl-t-butyl ether does not meet QC criteria (biased high). See LCS for accuracy. 8270D SIM - MSD recovery is outside of QC criteria for fluoranthene (biased high). Refer to LCS for accuracy. BMSD OWDFMW01-WG-03 MSD

947497 8270D SIM - Phenanthrene detected in the MB greater than one-half the LOQ. The concentration of phenanthrene in the

associated samples is less than the LOQ or greater than ten times the MB contamination. MB MB for HBN 225159 [XXX/22245]

SG S N o rth A m eric a Inc . En vir onm enta l D ivision 200 W e st Potter D rive A nc hora ge A K 99518 t (907 )562.2343 f( 907)561 .5301 w w w .us.sgs.com M em ber of SG S Group

# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1100319

Certification: I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1003 Bishop Street, Pauahi Tower Suite 1550 Honolulu, HI 96813 Attn: Rick Adkisson T: (808)528-1445 F:(808)528-0768

Jennifer Serna

Project Manager 

### 3354-010 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343f( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

### Enclosed are the analytical results associated with the above work order. If you have any questions regarding this report, or if we can be of any other assistance, please contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions (<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits. ! Surrogate out of control limits. B Indicates the analyte is found in a blank associated with the sample. CCV Continuing Calibration Verification CL Control Limit D The analyte concentration is the result of a dilution. DF Dilution Factor DL Detection Limit (i.e., maximum method detection limit) E The analyte result is above the calibrated range. F Indicates value that is greater than or equal to the DL GT Greater Than ICV Initial Calibration Verification J The quantitation is an estimation. JL The analyte was positively identified, but the quantitation is a low estimation. LCS(D) Laboratory Control Spike (Duplicate) LOD Limit of Detection (i.e., 2xDL) LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit) LT Less Than M A matrix effect was present. MB Method Blank MS(D) Matrix Spike (Duplicate) ND Indicates the analyte is not detected. Q QC parameter out of acceptance range. R Rejected RPD Relative Percent Difference U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP. Print Date: 2/5/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 3354-010 Red Hill BFSF Workorder No.: 1100319 

## Analytical Methods

Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS AFCEE 3.1 8260 (W) SW8260B Dissolved Metals by ICP-MS SW6020 DRO by 8015C (W) SW8015C GRO (W) SW8015C Print Date: 2/5/2010 9:27 am



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1100319001 OWDFMW01-WG-03 1100319002 OWDFMW01-WG-03 MS 1100319003 OWDFMW01-WG-03 MSD 1100319004 RHMW04-WG-03 1100319005 RHMWA01-WG-03 1100319006 HDMW2253-03-WG-03 1100319007 TB01-WG-03

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6300 MXX22714 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6300 Analytical Method: SW6020 Analysis Date/Time: 02/02/10 17:03 Prep Batch: MXX22714 Prep Method: SW3010A Prep Date/Time: 02/01/10 14:00 Container ID:1100319001-L Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9852 VXX20441 30.0 1 4-Bromofluorobenzene <surr> 100 50-150 % VFC9852 VXX20441 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9852 Analytical Method: SW8015C Analysis Date/Time: 02/01/10 11:31 Prep Batch: VXX20441 Prep Method: SW5030B Prep Date/Time: 02/01/10 10:00 Container ID:1100319001-A Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 1.49 0.440 mg/L XFC9100 XXX22248 0.165 1 5a Androstane <surr> 89.9 50-150 % XFC9100 XXX22248 1
Batch Information Initial Prep Wt./Vol.: 910 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9100 Analytical Method: SW8015C Analysis Date/Time: 02/02/10 17:29 Prep Batch: XXX22248 Prep Method: SW3520C Prep Date/Time: 02/01/10 10:20 Container ID:1100319001-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 Toluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromomethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Acetone 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11092 VXX20444 1.50 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 Chloroform 0.600 U 1.00 ug/L VMS11092 VXX20444 0.300 1 Bromobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11092 VXX20444 0.940 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 Methylene chloride 2.00 U 5.00 ug/L VMS11092 VXX20444 1.00 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Naphthalene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 o-Xylene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromoform 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Xylenes (total) 2.00 U 2.00 ug/L VMS11092 VXX20444 1.00 1 1,2-Dichloroethane-D4 <surr> 104 73-120 % VMS11092 VXX20444 1 Toluene-d8 <surr> 101 80-120 % VMS11092 VXX20444 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS11092 VXX20444 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11092 Analytical Method: SW8260B Analysis Date/Time: 02/01/10 18:48 Prep Batch: VXX20444 Prep Method: SW5030B Prep Date/Time: 02/01/10 12:35 Container ID:1100319001-D Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### OWDFMW01-WG-03 SGS Ref. #: 1100319001 Collection Date/Time: 01/26/10 09:20 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Acenaphthene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Fluorene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Phenanthrene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Anthracene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Fluoranthene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Pyrene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Benzo(a)Anthracene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Chrysene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Benzo[b]Fluoranthene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Benzo[k]fluoranthene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Benzo[a]pyrene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Indeno[1,2,3-c,d] pyrene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Dibenzo[a,h]anthracene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Benzo[g,h,i]perylene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Naphthalene 0.0664 U 0.107 ug/L XMS5285 XXX22249 0.0332 1 1-Methylnaphthalene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 2-Methylnaphthalene 0.0320 U 0.0535 ug/L XMS5285 XXX22249 0.0160 1 Terphenyl-d14 <surr> 102 50-126 % XMS5285 XXX22249 1
Batch Information Initial Prep Wt./Vol.: 935 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5285 Analytical Method: 8270D SIMS Analysis Date/Time: 02/02/10 11:47 Prep Batch: XXX22249 Prep Method: SW3520C Prep Date/Time: 02/01/10 11:20 Container ID:1100319001-J Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6300 MXX22713 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6300 Analytical Method: SW6020 Analysis Date/Time: 02/02/10 16:34 Prep Batch: MXX22713 Prep Method: SW3010A Prep Date/Time: 02/01/10 14:00 Container ID:1100319004-G Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9852 VXX20441 30.0 1 4-Bromofluorobenzene <surr> 104 50-150 % VFC9852 VXX20441 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9852 Analytical Method: SW8015C Analysis Date/Time: 02/01/10 12:43 Prep Batch: VXX20441 Prep Method: SW5030B Prep Date/Time: 02/01/10 10:00 Container ID:1100319004-A Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.334 U 0.444 mg/L XFC9100 XXX22248 0.167 1 5a Androstane <surr> 86.3 50-150 % XFC9100 XXX22248 1
Batch Information Initial Prep Wt./Vol.: 900 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9100 Analytical Method: SW8015C Analysis Date/Time: 02/02/10 18:32 Prep Batch: XXX22248 Prep Method: SW3520C Prep Date/Time: 02/01/10 10:20 Container ID:1100319004-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 Toluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromomethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Acetone 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11092 VXX20444 1.50 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 Chloroform 0.600 U 1.00 ug/L VMS11092 VXX20444 0.300 1 Bromobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11092 VXX20444 0.940 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 Methylene chloride 2.00 U 5.00 ug/L VMS11092 VXX20444 1.00 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Naphthalene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 o-Xylene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromoform 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Xylenes (total) 2.00 U 2.00 ug/L VMS11092 VXX20444 1.00 1 1,2-Dichloroethane-D4 <surr> 100 73-120 % VMS11092 VXX20444 1 Toluene-d8 <surr> 99.6 80-120 % VMS11092 VXX20444 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS11092 VXX20444 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11092 Analytical Method: SW8260B Analysis Date/Time: 02/01/10 19:19 Prep Batch: VXX20444 Prep Method: SW5030B Prep Date/Time: 02/01/10 12:35 Container ID:1100319004-D Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMW04-WG-03 SGS Ref. #: 1100319004 Collection Date/Time: 01/26/10 14:10 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Acenaphthene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Fluorene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Phenanthrene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Anthracene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Fluoranthene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Pyrene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Benzo(a)Anthracene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Chrysene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Benzo[b]Fluoranthene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Benzo[k]fluoranthene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Benzo[a]pyrene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Indeno[1,2,3-c,d] pyrene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Dibenzo[a,h]anthracene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Benzo[g,h,i]perylene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Naphthalene 0.0674 U 0.109 ug/L XMS5285 XXX22249 0.0337 1 1-Methylnaphthalene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 2-Methylnaphthalene 0.0326 U 0.0543 ug/L XMS5285 XXX22249 0.0163 1 Terphenyl-d14 <surr> 111 50-126 % XMS5285 XXX22249 1
Batch Information Initial Prep Wt./Vol.: 920 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5285 Analytical Method: 8270D SIMS Analysis Date/Time: 02/02/10 13:24 Prep Batch: XXX22249 Prep Method: SW3520C Prep Date/Time: 02/01/10 11:20 Container ID:1100319004-J Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6300 MXX22713 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6300 Analytical Method: SW6020 Analysis Date/Time: 02/02/10 16:36 Prep Batch: MXX22713 Prep Method: SW3010A Prep Date/Time: 02/01/10 14:00 Container ID:1100319005-G Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9852 VXX20441 30.0 1 4-Bromofluorobenzene <surr> 99.1 50-150 % VFC9852 VXX20441 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9852 Analytical Method: SW8015C Analysis Date/Time: 02/01/10 13:02 Prep Batch: VXX20441 Prep Method: SW5030B Prep Date/Time: 02/01/10 10:00 Container ID:1100319005-A Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.330 U 0.440 mg/L XFC9100 XXX22248 0.165 1 5a Androstane <surr> 95.2 50-150 % XFC9100 XXX22248 1
Batch Information Initial Prep Wt./Vol.: 910 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9100 Analytical Method: SW8015C Analysis Date/Time: 02/02/10 18:53 Prep Batch: XXX22248 Prep Method: SW3520C Prep Date/Time: 02/01/10 10:20 Container ID:1100319005-J Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 Toluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromomethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Acetone 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11092 VXX20444 1.50 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 Chloroform 0.600 U 1.00 ug/L VMS11092 VXX20444 0.300 1 Bromobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11092 VXX20444 0.940 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 Methylene chloride 2.00 U 5.00 ug/L VMS11092 VXX20444 1.00 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Naphthalene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 o-Xylene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromoform 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Xylenes (total) 2.00 U 2.00 ug/L VMS11092 VXX20444 1.00 1 1,2-Dichloroethane-D4 <surr> 101 73-120 % VMS11092 VXX20444 1 Toluene-d8 <surr> 99.4 80-120 % VMS11092 VXX20444 1 4-Bromofluorobenzene <surr> 106 76-120 % VMS11092 VXX20444 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11092 Analytical Method: SW8260B Analysis Date/Time: 02/01/10 19:51 Prep Batch: VXX20444 Prep Method: SW5030B Prep Date/Time: 02/01/10 12:35 Container ID:1100319005-D Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### RHMWA01-WG-03 SGS Ref. #: 1100319005 Collection Date/Time: 01/26/10 12:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Acenaphthene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Fluorene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Phenanthrene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Anthracene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Fluoranthene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Pyrene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Benzo(a)Anthracene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Chrysene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Benzo[b]Fluoranthene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Benzo[k]fluoranthene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Benzo[a]pyrene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Indeno[1,2,3-c,d] pyrene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Dibenzo[a,h]anthracene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Benzo[g,h,i]perylene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Naphthalene 0.0696 U 0.112 ug/L XMS5282 XXX22245 0.0348 1 1-Methylnaphthalene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 2-Methylnaphthalene 0.0338 U 0.0562 ug/L XMS5282 XXX22245 0.0169 1 Terphenyl-d14 <surr> 103 50-126 % XMS5282 XXX22245 1
Batch Information Initial Prep Wt./Vol.: 890 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5282 Analytical Method: 8270D SIMS Analysis Date/Time: 02/01/10 13:53 Prep Batch: XXX22245 Prep Method: SW3520C Prep Date/Time: 01/29/10 11:00 Container ID:1100319005-K Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 ug/L MMS6300 MXX22714 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6300 Analytical Method: SW6020 Analysis Date/Time: 02/02/10 17:13 Prep Batch: MXX22714 Prep Method: SW3010A Prep Date/Time: 02/01/10 14:00 Container ID:1100319006-L Dilution Factor: 5 Analyst: NRB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9852 VXX20441 30.0 1 4-Bromofluorobenzene <surr> 100 50-150 % VFC9852 VXX20441 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9852 Analytical Method: SW8015C Analysis Date/Time: 02/01/10 13:22 Prep Batch: VXX20441 Prep Method: SW5030B Prep Date/Time: 02/01/10 10:00 Container ID:1100319006-A Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.322 J 0.460 mg/L XFC9100 XXX22248 0.172 1 5a Androstane <surr> 80.6 50-150 % XFC9100 XXX22248 1
Batch Information Initial Prep Wt./Vol.: 870 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC9100 Analytical Method: SW8015C Analysis Date/Time: 02/02/10 19:14 Prep Batch: XXX22248 Prep Method: SW3520C Prep Date/Time: 02/01/10 10:20 Container ID:1100319006-I Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 Toluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromomethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Acetone 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11092 VXX20444 1.50 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 Chloroform 0.600 U 1.00 ug/L VMS11092 VXX20444 0.300 1 Bromobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11092 VXX20444 0.940 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 Methylene chloride 2.00 U 5.00 ug/L VMS11092 VXX20444 1.00 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Naphthalene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 o-Xylene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromoform 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Xylenes (total) 2.00 U 2.00 ug/L VMS11092 VXX20444 1.00 1 1,2-Dichloroethane-D4 <surr> 102 73-120 % VMS11092 VXX20444 1 Toluene-d8 <surr> 99.7 80-120 % VMS11092 VXX20444 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS11092 VXX20444 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11092 Analytical Method: SW8260B Analysis Date/Time: 02/01/10 20:22 Prep Batch: VXX20444 Prep Method: SW5030B Prep Date/Time: 02/01/10 12:35 Container ID:1100319006-D Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### HDMW2253-03-WG-03 SGS Ref. #: 1100319006 Collection Date/Time: 01/26/10 11:00 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

DL DF

Acenaphthylene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Acenaphthene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Fluorene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Phenanthrene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Anthracene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Fluoranthene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Pyrene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Benzo(a)Anthracene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Chrysene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Benzo[b]Fluoranthene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Benzo[k]fluoranthene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Benzo[a]pyrene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Indeno[1,2,3-c,d] pyrene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Dibenzo[a,h]anthracene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Benzo[g,h,i]perylene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Naphthalene 0.103 U 0.167 ug/L XMS5282 XXX22245 0.0517 1 1-Methylnaphthalene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 2-Methylnaphthalene 0.0500 U 0.0833 ug/L XMS5282 XXX22245 0.0250 1 Terphenyl-d14 <surr> 107 50-126 % XMS5282 XXX22245 1
Batch Information Initial Prep Wt./Vol.: 600 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5282 Analytical Method: 8270D SIMS Analysis Date/Time: 02/01/10 14:26 Prep Batch: XXX22245 Prep Method: SW3520C Prep Date/Time: 01/29/10 11:00 Container ID:1100319006-K Dilution Factor: 1 Analyst: JDH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### TB01-WG-03 SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 ug/L VFC9852 VXX20441 30.0 1 4-Bromofluorobenzene <surr> 104 50-150 % VFC9852 VXX20441 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9852 Analytical Method: SW8015C Analysis Date/Time: 02/01/10 13:41 Prep Batch: VXX20441 Prep Method: SW5030B Prep Date/Time: 02/01/10 10:00 Container ID:1100319007-A Dilution Factor: 1 Analyst: HM

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### TB01-WG-03 SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Benzene 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 Toluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Ethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 n-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dichloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chlorobenzene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 4-Isopropyltoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 n-Propylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Styrene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromomethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Acetone 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS11092 VXX20444 1.50 1 Tetrachloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dibromochloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,3-Dichloropropane 0.240 U 0.400 ug/L VMS11092 VXX20444 0.120 1 1,2-Dibromoethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Carbon tetrachloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 Chloroform 0.600 U 1.00 ug/L VMS11092 VXX20444 0.300 1 Bromobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Chloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromomethane 1.88 U 3.00 ug/L VMS11092 VXX20444 0.940 1 Bromochloromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Vinyl chloride 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### TB01-WG-03 SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Chloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 sec-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromodichloromethane 0.300 U 0.500 ug/L VMS11092 VXX20444 0.150 1 1,1-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Butanone (MEK) 6.20 U 10.0 ug/L VMS11092 VXX20444 3.10 1 Methylene chloride 2.00 U 5.00 ug/L VMS11092 VXX20444 1.00 1 Trichlorofluoromethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 P & M -Xylene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 Naphthalene 1.24 U 2.00 ug/L VMS11092 VXX20444 0.620 1 o-Xylene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Bromoform 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1-Chlorohexane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 tert-Butylbenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2-Chlorotoluene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Trichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 2,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Hexachlorobutadiene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2-Dichloropropane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1-Dichloropropene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS11092 VXX20444 0.310 1 Xylenes (total) 2.00 U 2.00 ug/L VMS11092 VXX20444 1.00 1 1,2-Dichloroethane-D4 <surr> 99.9 73-120 % VMS11092 VXX20444 1 Toluene-d8 <surr> 102 80-120 % VMS11092 VXX20444 1 4-Bromofluorobenzene <surr> 105 76-120 % VMS11092 VXX20444 1

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

### The Environmental Company, Inc. (TEC) Print Date: 2/5/2010 9:27 am

Client Sample ID: 

### TB01-WG-03 SGS Ref. #: 1100319007 Collection Date/Time: 01/26/10 08:05 Receipt Date/Time: 01/28/10 14:45 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch LOQ/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

DL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS11092 Analytical Method: SW8260B Analysis Date/Time: 02/01/10 17:45 Prep Batch: VXX20444 Prep Method: SW5030B Prep Date/Time: 02/01/10 12:35 Container ID:1100319007-C Dilution Factor: 1 Analyst: DSH

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t (907 )562.2343 f ( 907)561 .5301 w ww.us.sgs.com M ember of SG S GroupMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947497 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22245 SW3520C 01/29/2010 QC results affect the following production samples: 

### 1100319005, 1100319006

Parameter Results LOQ/CL Units Analysis Date DL


### Polynuclear Aromatics GC/MS


### Acenaphthylene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Acenaphthene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Fluorene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Phenanthrene 0.0251 J 0.0500 ug/L 02/01/10 

### 0.0150 Anthracene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Fluoranthene 0.0154 J 0.0500 ug/L 02/01/10 

### 0.0150 Pyrene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Benzo(a)Anthracene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Chrysene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Benzo[b]Fluoranthene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Benzo[k]fluoranthene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Benzo[a]pyrene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Dibenzo[a,h]anthracene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Benzo[g,h,i]perylene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 Naphthalene 0.0620 U 0.100 ug/L 02/01/10 

### 0.0310 1-Methylnaphthalene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150 2-Methylnaphthalene 0.0300 U 0.0500 ug/L 02/01/10 

### 0.0150
Surrogates 

### Terphenyl-d14 <surr> 106 50-126 % 02/01/10

Instrument Method Batch XMS5282

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947654 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22248 SW3520C 02/01/2010 QC results affect the following production samples: 

### 1100319001, 1100319004, 1100319005, 1100319006

Parameter Results LOQ/CL Units Analysis Date DL



### Semivolatile Organic Fuels Department 

### Diesel Range Organics 0.300 U 0.400 mg/L 02/02/10 

### 0.150
Surrogates


### 5a Androstane <surr> 93.2 60-120 % 02/02/10

Instrument Method Batch XFC9100

SW8015C HP 7890A FID SV E FMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947711 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22249 SW3520C 02/01/2010 QC results affect the following production samples: 

### 1100319001, 1100319004

Parameter Results LOQ/CL Units Analysis Date DL


### Polynuclear Aromatics GC/MS


### Acenaphthylene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Acenaphthene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Fluorene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Phenanthrene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Anthracene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Fluoranthene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Pyrene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Benzo(a)Anthracene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Chrysene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Benzo[b]Fluoranthene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Benzo[k]fluoranthene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Benzo[a]pyrene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Dibenzo[a,h]anthracene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Benzo[g,h,i]perylene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 Naphthalene 0.0620 U 0.100 ug/L 02/02/10 

### 0.0310 1-Methylnaphthalene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150 2-Methylnaphthalene 0.0300 U 0.0500 ug/L 02/02/10 

### 0.0150
Surrogates 

### Terphenyl-d14 <surr> 109 50-126 % 02/02/10

Instrument Method Batch XMS5285

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947724 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20441 SW5030B 02/01/2010 QC results affect the following production samples: 

### 1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter Results LOQ/CL Units Analysis Date DL



### Volatile Fuels Department 

### Gasoline Range Organics 60.0 U 100 ug/L 02/01/10 

### 30.0
Surrogates


### 4-Bromofluorobenzene <surr> 104 50-150 % 02/01/10

Instrument Method Batch VFC9852

SW8015C HP 5890 Series II PID+HECD VBAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947759 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010 QC results affect the following production samples: 

### 1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947759 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene 0.240 U 0.400 ug/L 02/01/10 

### 0.120 Toluene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Ethylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 n-Butylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,4-Dichlorobenzene 0.300 U 0.500 ug/L 02/01/10 

### 0.150 1,2-Dichloroethane 0.300 U 0.500 ug/L 02/01/10 

### 0.150 1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 4-Chlorotoluene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Chlorobenzene 0.300 U 0.500 ug/L 02/01/10 

### 0.150 4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 02/01/10 

### 3.10 cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 4-Isopropyltoluene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 02/01/10 

### 0.150 n-Propylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Styrene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Dibromomethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Acetone 6.20 U 10.0 ug/L 02/01/10 

### 3.10 1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 02/01/10 

### 0.150 1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 02/01/10 

### 0.620 Methyl-t-butyl ether 3.00 U 5.00 ug/L 02/01/10 

### 1.50 Tetrachloroethene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Dibromochloromethane 0.300 U 0.500 ug/L 02/01/10 

### 0.150 1,3-Dichloropropane 0.240 U 0.400 ug/L 02/01/10 

### 0.120 1,2-Dibromoethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Carbon tetrachloride 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 02/01/10 

### 0.150 Chloroform 0.600 U 1.00 ug/L 02/01/10 

### 0.300 Bromobenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Chloromethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,2,3-Trichloropropane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Bromomethane 1.88 U 3.00 ug/L 02/01/10 

### 0.940 Bromochloromethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Vinyl chloride 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Dichlorodifluoromethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Chloroethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 sec-Butylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Bromodichloromethane 0.300 U 0.500 ug/L 02/01/10 

### 0.150Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947759 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter Results LOQ/CL Units Analysis Date DL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1-Dichloroethene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 2-Butanone (MEK) 6.20 U 10.0 ug/L 02/01/10 

### 3.10 Methylene chloride 2.00 U 5.00 ug/L 02/01/10 

### 1.00 Trichlorofluoromethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 P & M -Xylene 1.24 U 2.00 ug/L 02/01/10 

### 0.620 Naphthalene 1.24 U 2.00 ug/L 02/01/10 

### 0.620 o-Xylene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Bromoform 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1-Chlorohexane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 tert-Butylbenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,1,1-Trichloroethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,1-Dichloroethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 2-Chlorotoluene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Trichloroethene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,2-Dichlorobenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 2,2-Dichloropropane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Hexachlorobutadiene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,2-Dichloropropane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,1-Dichloropropene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,1,2-Trichloroethane 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,3-Dichlorobenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 02/01/10 

### 0.310 Xylenes (total) 2.00 U 2.00 ug/L 02/01/10 

### 1.00
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 100 73-120 % 02/01/10 

### Toluene-d8 <surr> 99.1 80-120 % 02/01/10 

### 4-Bromofluorobenzene <surr> 103 76-120 % 02/01/10

Instrument Method Batch VMS11092

SW8260B HP 5890 Series II MS1 VJAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947859 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22713 SW3010A 02/01/2010 QC results affect the following production samples: 

### 1100319004, 1100319005

Parameter Results LOQ/CL Units Analysis Date DL


### Metals by ICP/MS



### Lead 0.620 U 1.00 ug/L 02/02/10 

### 0.310

Instrument Method Batch MMS6300

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947864 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22714 SW3010A 02/01/2010 QC results affect the following production samples: 

### 1100319001, 1100319006

Parameter Results LOQ/CL Units Analysis Date DL


### Metals by ICP/MS



### Lead 0.620 U 1.00 ug/L 02/02/10 

### 0.310

Instrument Method Batch MMS6300

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947498 Lab Control Sample 947499 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22245 SW3520C 01/29/2010

QC results affect the following production samples: 

### 1100319005, 1100319006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Acenaphthylene LCS 0.421 84 ( 50-101 ) 0.5 ug/L 02/01/2010 LCSD 0.394 79 7 (< 30 ) 0.5 ug/L 02/01/2010
Acenaphthene LCS 0.414 83 ( 45-93 ) 0.5 ug/L 02/01/2010 LCSD 0.393 79 5 (< 30 ) 0.5 ug/L 02/01/2010

Fluorene LCS 0.418 84 ( 50-98 ) 0.5 ug/L 02/01/2010 LCSD 0.415 83 1 (< 30 ) 0.5 ug/L 02/01/2010

Phenanthrene LCS 0.426 85 ( 50-104 ) 0.5 ug/L 02/01/2010 LCSD 0.409 82 4 (< 30 ) 0.5 ug/L 02/01/2010

Anthracene LCS 0.421 84 ( 55-105 ) 0.5 ug/L 02/01/2010 LCSD 0.405 81 4 (< 30 ) 0.5 ug/L 02/01/2010

Fluoranthene LCS 0.479 96 ( 58-109 ) 0.5 ug/L 02/01/2010 LCSD 0.472 95 2 (< 30 ) 0.5 ug/L 02/01/2010
Pyrene LCS 0.461 92 ( 56-105 ) 0.5 ug/L 02/01/2010 LCSD 0.458 92 1 (< 30 ) 0.5 ug/L 02/01/2010
Benzo(a)Anthracene LCS 0.520 104 ( 55-120 ) 0.5 ug/L 02/01/2010 LCSD 0.513 103 1 (< 30 ) 0.5 ug/L 02/01/2010
Chrysene LCS 0.469 94 ( 56-109 ) 0.5 ug/L 02/01/2010 LCSD 0.457 91 3 (< 30 ) 0.5 ug/L 02/01/2010
Benzo[b]Fluoranthene LCS 0.535 107 ( 45-120 ) 0.5 ug/L 02/01/2010 LCSD 0.519 104 3 (< 30 ) 0.5 ug/L 02/01/2010
Benzo[k]fluoranthene LCS 0.515 103 ( 56-112 ) 0.5 ug/L 02/01/2010 LCSD 0.508 102 1 (< 30 ) 0.5 ug/L 02/01/2010
Benzo[a]pyrene LCS 0.545 109 ( 57-110 ) 0.5 ug/L 02/01/2010 LCSD 0.551 110 1 (< 30 ) 0.5 ug/L 02/01/2010
Indeno[1,2,3-c,d] pyrene LCS 0.496 99 ( 55-111 ) 0.5 ug/L 02/01/2010 LCSD 0.485 97 2 (< 30 ) 0.5 ug/L 02/01/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947498 Lab Control Sample 947499 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22245 SW3520C 01/29/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Dibenzo[a,h]anthracene LCS 0.483 97 ( 54-113 ) 0.5 ug/L 02/01/2010 LCSD 0.488 98 1 (< 30 ) 0.5 ug/L 02/01/2010
Benzo[g,h,i]perylene LCS 0.482 96 ( 49-116 ) 0.5 ug/L 02/01/2010 LCSD 0.494 99 2 (< 30 ) 0.5 ug/L 02/01/2010
Naphthalene LCS 0.382 77 ( 44-89 ) 0.5 ug/L 02/01/2010 LCSD 0.379 76 1 (< 30 ) 0.5 ug/L 02/01/2010
1-Methylnaphthalene LCS 0.394 79 ( 42-92 ) 0.5 ug/L 02/01/2010 LCSD 0.401 80 2 (< 30 ) 0.5 ug/L 02/01/2010
2-Methylnaphthalene LCS 0.365 73 ( 45-89 ) 0.5 ug/L 02/01/2010 LCSD 0.364 73 0 (< 30 ) 0.5 ug/L 02/01/2010

Surrogates 

### Terphenyl-d14 <surr> LCS 98 ( 50-126 ) 02/01/2010 LCSD 106 8 02/01/2010

Batch Method Instrument 

### XMS5282

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947712 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22249 SW3520C 02/01/2010

QC results affect the following production samples: 

### 1100319001, 1100319004

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MSMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947712 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22249 SW3520C 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Acenaphthylene LCS 0.403 81 ( 50-101 ) 0.5 ug/L 02/02/2010
Acenaphthene LCS 0.406 81 ( 45-93 ) 0.5 ug/L 02/02/2010

Fluorene LCS 0.421 84 ( 50-98 ) 0.5 ug/L 02/02/2010

Phenanthrene LCS 0.434 87 ( 50-104 ) 0.5 ug/L 02/02/2010

Anthracene LCS 0.437 87 ( 55-105 ) 0.5 ug/L 02/02/2010

Fluoranthene LCS 0.512 102 ( 58-109 ) 0.5 ug/L 02/02/2010
Pyrene LCS 0.491 98 ( 56-105 ) 0.5 ug/L 02/02/2010
Benzo(a)Anthracene LCS 0.523 105 ( 55-120 ) 0.5 ug/L 02/02/2010
Chrysene LCS 0.464 93 ( 56-109 ) 0.5 ug/L 02/02/2010
Benzo[b]Fluoranthene LCS 0.481 96 ( 45-120 ) 0.5 ug/L 02/02/2010
Benzo[k]fluoranthene LCS 0.493 99 ( 56-112 ) 0.5 ug/L 02/02/2010
Benzo[a]pyrene LCS 0.507 101 ( 57-110 ) 0.5 ug/L 02/02/2010
Indeno[1,2,3-c,d] pyrene LCS 0.456 91 ( 55-111 ) 0.5 ug/L 02/02/2010
Dibenzo[a,h]anthracene LCS 0.461 92 ( 54-113 ) 0.5 ug/L 02/02/2010
Benzo[g,h,i]perylene LCS 0.439 88 ( 49-116 ) 0.5 ug/L 02/02/2010
Naphthalene LCS 0.354 71 ( 44-89 ) 0.5 ug/L 02/02/2010
1-Methylnaphthalene LCS 0.385 77 ( 42-92 ) 0.5 ug/L 02/02/2010
2-Methylnaphthalene LCS 0.363 73 ( 45-89 ) 0.5 ug/L 02/02/2010

Surrogates 

### Terphenyl-d14 <surr> LCS 103 ( 50-126 ) 02/02/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947712 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22249 SW3520C 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5285

8270D SIMS HP 6890/5973 MS SVQAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947725 Lab Control Sample 947726 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20441 SW5030B 02/01/2010

QC results affect the following production samples: 

### 1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Fuels Department 

### Gasoline Range Organics LCS 210 105 ( 79-108 ) 200 ug/L 02/01/2010 LCSD 199 100 5 (< 20 ) 200 ug/L 02/01/2010

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 103 ( 50-150 ) 02/01/2010 LCSD 103 0 02/01/2010

Batch Method Instrument 

### VFC9852

SW8015C HP 5890 Series II PID+HECD VBAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

QC results affect the following production samples: 

### 1100319001, 1100319004, 1100319005, 1100319006, 1100319007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene LCS 29.9 100 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 28.5 95 5 (< 20 ) 30 ug/L 02/01/2010

Toluene LCS 31.3 104 ( 77-120 ) 30 ug/L 02/01/2010 LCSD 29.7 99 5 (< 20 ) 30 ug/L 02/01/2010
Ethylbenzene LCS 31.4 105 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 29.5 98 6 (< 20 ) 30 ug/L 02/01/2010
n-Butylbenzene LCS 34.9 116 ( 80-124 ) 30 ug/L 02/01/2010 LCSD 33.1 110 5 (< 20 ) 30 ug/L 02/01/2010
1,4-Dichlorobenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 30.3 101 6 (< 20 ) 30 ug/L 02/01/2010
1,2-Dichloroethane LCS 30.9 103 ( 80-129 ) 30 ug/L 02/01/2010 LCSD 30.6 102 1 (< 20 ) 30 ug/L 02/01/2010
1,3,5-Trimethylbenzene LCS 33.8 113 ( 80-128 ) 30 ug/L 02/01/2010 LCSD 31.9 106 6 (< 20 ) 30 ug/L 02/01/2010

4-Chlorotoluene LCS 34.1 114 ( 79-128 ) 30 ug/L 02/01/2010 LCSD 32.3 108 5 (< 20 ) 30 ug/L 02/01/2010

Chlorobenzene LCS 31.1 104 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 29.5 98 5 (< 20 ) 30 ug/L 02/01/2010
4-Methyl-2-pentanone (MIBK) LCS 90.5 101 ( 69-134 ) 90 ug/L 02/01/2010 LCSD 97.4 108 7 (< 20 ) 90 ug/L 02/01/2010
cis-1,2-Dichloroethene LCS 29.8 99 ( 80-125 ) 30 ug/L 02/01/2010 LCSD 28.1 94 6 (< 20 ) 30 ug/L 02/01/2010
4-Isopropyltoluene LCS 34.2 114 ( 80-125 ) 30 ug/L 02/01/2010 LCSD 32.0 107 7 (< 20 ) 30 ug/L 02/01/2010
cis-1,3-Dichloropropene LCS 33.9 113 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 32.9 110 3 (< 20 ) 30 ug/L 02/01/2010
n-Propylbenzene LCS 34.0 113 ( 80-129 ) 30 ug/L 02/01/2010 LCSD 32.0 107 6 (< 20 ) 30 ug/L 02/01/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 31.8 106 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 30.1 100 5 (< 20 ) 30 ug/L 02/01/2010

Dibromomethane LCS 30.4 101 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 30.8 103 1 (< 20 ) 30 ug/L 02/01/2010
trans-1,3-Dichloropropene LCS 32.5 108 ( 80-124 ) 30 ug/L 02/01/2010 LCSD 32.4 108 1 (< 20 ) 30 ug/L 02/01/2010
1,2,4-Trichlorobenzene LCS 31.5 105 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 31.4 105 0 (< 20 ) 30 ug/L 02/01/2010

Acetone LCS 72.4 80 ( 50-135 ) 90 ug/L 02/01/2010 LCSD 88.5 98 20 (< 20 ) 90 ug/L 02/01/2010
1,1,2,2-Tetrachloroethane LCS 32.7 109 ( 76-123 ) 30 ug/L 02/01/2010 LCSD 33.7 112 3 (< 20 ) 30 ug/L 02/01/2010
1,2-Dibromo-3-chloropropane LCS 33.1 110 ( 73-130 ) 30 ug/L 02/01/2010 LCSD 36.5 122 10 (< 20 ) 30 ug/L 02/01/2010
Methyl-t-butyl ether LCS 52.3 116 ( 80-120 ) 45 ug/L 02/01/2010 LCSD 53.2 118 2 (< 20 ) 45 ug/L 02/01/2010

Tetrachloroethene LCS 31.2 104 ( 79-122 ) 30 ug/L 02/01/2010 LCSD 28.9 96 8 (< 20 ) 30 ug/L 02/01/2010

Dibromochloromethane LCS 28.7 96 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 28.4 95 1 (< 20 ) 30 ug/L 02/01/2010
1,3-Dichloropropane LCS 32.7 109 ( 80-121 ) 30 ug/L 02/01/2010 LCSD 32.3 108 1 (< 20 ) 30 ug/L 02/01/2010
1,2-Dibromoethane LCS 31.7 106 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 31.8 106 0 (< 20 ) 30 ug/L 02/01/2010

Carbon tetrachloride LCS 31.7 106 ( 80-126 ) 30 ug/L 02/01/2010 LCSD 29.4 98 8 (< 20 ) 30 ug/L 02/01/2010
1,1,1,2-Tetrachloroethane LCS 33.5 112 ( 80-120 ) 30 ug/L 02/01/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 31.6 105 6 (< 20 ) 30 ug/L 02/01/2010

Chloroform LCS 30.1 100 ( 80-124 ) 30 ug/L 02/01/2010 LCSD 28.4 95 6 (< 20 ) 30 ug/L 02/01/2010

Bromobenzene LCS 31.1 104 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 30.1 100 3 (< 20 ) 30 ug/L 02/01/2010

Chloromethane LCS 32.1 107 ( 67-125 ) 30 ug/L 02/01/2010 LCSD 32.3 108 1 (< 20 ) 30 ug/L 02/01/2010
1,2,3-Trichloropropane LCS 31.4 105 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 32.0 107 2 (< 20 ) 30 ug/L 02/01/2010

Bromomethane LCS 27.6 92 ( 30-140 ) 30 ug/L 02/01/2010 LCSD 29.6 99 7 (< 20 ) 30 ug/L 02/01/2010

Bromochloromethane LCS 28.0 94 ( 77-129 ) 30 ug/L 02/01/2010 LCSD 27.1 90 3 (< 20 ) 30 ug/L 02/01/2010
Vinyl chloride LCS 28.3 94 ( 72-145 ) 30 ug/L 02/01/2010 LCSD 28.0 93 1 (< 20 ) 30 ug/L 02/01/2010

Dichlorodifluoromethane LCS 32.7 109 ( 62-153 ) 30 ug/L 02/01/2010 LCSD 32.0 107 2 (< 20 ) 30 ug/L 02/01/2010

Chloroethane LCS 29.2 97 ( 67-133 ) 30 ug/L 02/01/2010 LCSD 27.8 93 5 (< 20 ) 30 ug/L 02/01/2010
sec-Butylbenzene LCS 33.8 113 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 32.0 107 6 (< 20 ) 30 ug/L 02/01/2010

Bromodichloromethane LCS 32.8 109 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 31.9 106 3 (< 20 ) 30 ug/L 02/01/2010
1,1-Dichloroethene LCS 27.2 91 ( 76-130 ) 30 ug/L 02/01/2010 LCSD 25.8 86 5 (< 20 ) 30 ug/L 02/01/2010
2-Butanone (MEK) LCS 88.7 99 ( 66-136 ) 90 ug/L 02/01/2010 LCSD 99.9 111 12 (< 20 ) 90 ug/L 02/01/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Methylene chloride LCS 25.9 86 ( 63-131 ) 30 ug/L 02/01/2010 LCSD 25.1 84 3 (< 20 ) 30 ug/L 02/01/2010

Trichlorofluoromethane LCS 29.0 97 ( 68-145 ) 30 ug/L 02/01/2010 LCSD 27.4 91 6 (< 20 ) 30 ug/L 02/01/2010
P & M -Xylene LCS 64.8 108 ( 80-120 ) 60 ug/L 02/01/2010 LCSD 61.0 102 6 (< 20 ) 60 ug/L 02/01/2010
Naphthalene LCS 31.6 105 ( 75-120 ) 30 ug/L 02/01/2010 LCSD 34.3 114 8 (< 20 ) 30 ug/L 02/01/2010
o-Xylene LCS 30.9 103 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 29.1 97 6 (< 20 ) 30 ug/L 02/01/2010

Bromoform LCS 30.1 100 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 29.6 99 2 (< 20 ) 30 ug/L 02/01/2010

1-Chlorohexane LCS 48.4 108 ( 70-125 ) 45 ug/L 02/01/2010 LCSD 45.2 101 7 (< 20 ) 45 ug/L 02/01/2010
1,2,4-Trimethylbenzene LCS 33.6 112 ( 80-125 ) 30 ug/L 02/01/2010 LCSD 31.9 106 5 (< 20 ) 30 ug/L 02/01/2010
tert-Butylbenzene LCS 32.9 110 ( 80-122 ) 30 ug/L 02/01/2010 LCSD 30.8 103 7 (< 20 ) 30 ug/L 02/01/2010
1,1,1-Trichloroethane LCS 31.8 106 ( 80-122 ) 30 ug/L 02/01/2010 LCSD 29.8 100 7 (< 20 ) 30 ug/L 02/01/2010
1,1-Dichloroethane LCS 36.0 120 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 34.2 114 5 (< 20 ) 30 ug/L 02/01/2010

2-Chlorotoluene LCS 33.5 112 ( 80-125 ) 30 ug/L 02/01/2010 LCSD 31.7 106 6 (< 20 ) 30 ug/L 02/01/2010

Trichloroethene LCS 31.3 104 ( 80-125 ) 30 ug/L 02/01/2010 LCSD 29.6 99 5 (< 20 ) 30 ug/L 02/01/2010
trans-1,2-Dichloroethene LCS 31.9 106 ( 79-132 ) 30 ug/L 02/01/2010 LCSD 30.3 101 5 (< 20 ) 30 ug/L 02/01/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichlorobenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 30.2 101 3 (< 20 ) 30 ug/L 02/01/2010
2,2-Dichloropropane LCS 32.4 108 ( 80-132 ) 30 ug/L 02/01/2010 LCSD 30.5 102 6 (< 20 ) 30 ug/L 02/01/2010

Hexachlorobutadiene LCS 31.1 104 ( 77-125 ) 30 ug/L 02/01/2010 LCSD 29.7 99 5 (< 20 ) 30 ug/L 02/01/2010
Isopropylbenzene (Cumene) LCS 32.8 109 ( 80-121 ) 30 ug/L 02/01/2010 LCSD 30.7 102 7 (< 20 ) 30 ug/L 02/01/2010
1,2-Dichloropropane LCS 33.2 111 ( 80-121 ) 30 ug/L 02/01/2010 LCSD 31.8 106 4 (< 20 ) 30 ug/L 02/01/2010
1,1-Dichloropropene LCS 32.7 109 ( 80-122 ) 30 ug/L 02/01/2010 LCSD 30.7 102 6 (< 20 ) 30 ug/L 02/01/2010
1,1,2-Trichloroethane LCS 32.0 107 ( 77-120 ) 30 ug/L 02/01/2010 LCSD 31.9 106 0 (< 20 ) 30 ug/L 02/01/2010
1,3-Dichlorobenzene LCS 32.1 107 ( 80-120 ) 30 ug/L 02/01/2010 LCSD 30.4 101 5 (< 20 ) 30 ug/L 02/01/2010
1,2,3-Trichlorobenzene LCS 29.7 99 ( 77-120 ) 30 ug/L 02/01/2010 LCSD 30.7 102 3 (< 20 ) 30 ug/L 02/01/2010
Xylenes (total) LCS 95.6 106 ( 80-120 ) 90 ug/L 02/01/2010 LCSD 90.1 100 6 (< 20 ) 90 ug/L 02/01/2010

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 97 ( 73-120 ) 02/01/2010 LCSD 99 3 02/01/2010

Toluene-d8 <surr> LCS 97 ( 80-120 ) 02/01/2010 LCSD 96 1 02/01/2010

4-Bromofluorobenzene <surr> LCS 103 ( 76-120 ) 02/01/2010 LCSD 103 1 02/01/2010Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947760 Lab Control Sample 947761 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20444 SW5030B 02/01/2010

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS11092

SW8260B HP 5890 Series II MS1 VJAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947860 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22713 SW3010A 02/01/2010

QC results affect the following production samples: 

### 1100319004, 1100319005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS


### Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 02/02/2010

Batch Method Instrument 

### MMS6300

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947865 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22714 SW3010A 02/01/2010

QC results affect the following production samples: 

### 1100319001, 1100319006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS


### Lead LCS 1020 102 ( 80-120 ) 1000 ug/L 02/02/2010

Batch Method Instrument 

### MMS6300

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Prep 

### 947982 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX22248 SW3520C 02/01/2010

QC results affect the following production samples: 

### 1100319001, 1100319004, 1100319005, 1100319006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.84 97 ( 75-125 ) 5 mg/L 02/02/2010

Surrogates 

### 5a Androstane <surr> LCS 98 ( 60-120 ) 02/02/2010

Batch Method Instrument 

### XFC9100

SW8015C HP 7890A FID SV E FMatrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep



### 947861 Matrix Spike 947862 Matrix Spike Duplicate

1100328001 Water (Surface, Eff., Ground) MXX22713 3010 H20 Digest for Metals ICP-MS 02/01/2010

QC results affect the following production samples: 

### 1100319004, 1100319005

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Metals by ICP/MS


### Lead MS (0.620) U 1050 105 ( 80-120 ) 1000 ug/L 02/02/2010 MSD 1010 101 4 (< 15 ) 1000 ug/L 02/02/2010
Batch Method Instrument 

### MMS6300

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) MXX22714 3010 H20 Digest for Metals ICP-MS 02/01/2010

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS (0.620) U 985 99 ( 80-120 ) 1000 ug/L 02/02/2010 BMSD 1010 101 3 (< 15 ) 1000 ug/L 02/02/2010
Batch Method Instrument 

### MMS6300

SW6020 Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department 

### Gasoline Range Organics BMS (60.0) U 494 110 * ( 79-108 ) 450 ug/L 02/01/2010 BMSD 498 111 * 1 (< 20 ) 450 ug/L 02/01/2010 Surrogates 

### 4-Bromofluorobenzene <surr> BMS 57.9 116 ( 50-150 ) 02/01/2010 BMSD 53.5 107 8 02/01/2010
Batch Method Instrument 

### VFC9852

SW8015C HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS 1.49 5.83 80 ( 75-125 ) 5.43 mg/L 02/02/2010 BMSD 6.19 84 6 (< 30 ) 5.62 mg/L 02/02/2010 Surrogates 

### 5a Androstane <surr> BMS .0941 87 ( 50-150 ) 02/02/2010 BMSD 0.0948 84 1 02/02/2010
Batch Method Instrument 

### XFC9100

SW8015C HP 7890A FID SV E F

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) VXX20444 Volatiles Extraction AFCEE 3.1 8260 (W) 02/01/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene BMS (0.240) U 31.9 106 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 02/01/2010 Toluene BMS (0.620) U 33.7 112 ( 77-120 ) 30.0 ug/L 02/01/2010 BMSD 33.3 111 1 (< 20 ) 30.0 ug/L 02/01/2010 Ethylbenzene BMS (0.620) U 33.4 111 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 33.1 110 1 (< 20 ) 30.0 ug/L 02/01/2010 n-Butylbenzene BMS (0.620) U 36.5 122 ( 80-124 ) 30.0 ug/L 02/01/2010 BMSD 37.1 124 2 (< 20 ) 30.0 ug/L 02/01/2010 1,4-Dichlorobenzene BMS (0.300) U 33.6 112 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 34.0 113 1 (< 20 ) 30.0 ug/L 02/01/2010 1,2-Dichloroethane BMS (0.300) U 33.5 112 ( 80-129 ) 30.0 ug/L 02/01/2010 BMSD 33.5 112 0 (< 20 ) 30.0 ug/L 02/01/2010 1,3,5-Trimethylbenzene BMS (0.620) U 35.2 117 ( 80-128 ) 30.0 ug/L 02/01/2010 BMSD 35.6 119 1 (< 20 ) 30.0 ug/L 02/01/2010 4-Chlorotoluene BMS (0.620) U 35.3 118 ( 79-128 ) 30.0 ug/L 02/01/2010 BMSD 36.4 121 3 (< 20 ) 30.0 ug/L 02/01/2010 Chlorobenzene BMS (0.300) U 33.2 111 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 32.9 110 1 (< 20 ) 30.0 ug/L 02/01/2010 4-Methyl-2-pentanone (MIBK) BMS (6.20) U 104 116 ( 69-134 ) 90.0 ug/L 02/01/2010 BMSD 98.0 109 6 (< 20 ) 90.0 ug/L 02/01/2010 cis-1,2-Dichloroethene BMS (0.620) U 30.7 102 ( 80-125 ) 30.0 ug/L 02/01/2010 BMSD 31.1 104 1 (< 20 ) 30.0 ug/L 02/01/2010 4-Isopropyltoluene BMS (0.620) U 35.8 119 ( 80-125 ) 30.0 ug/L 02/01/2010 BMSD 36.2 121 1 (< 20 ) 30.0 ug/L 02/01/2010 cis-1,3-Dichloropropene BMS (0.300) U 36.5 122 * ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 35.8 119 2 (< 20 ) 30.0 ug/L 02/01/2010 n-Propylbenzene BMS (0.620) U 35.1 117 ( 80-129 ) 30.0 ug/L 02/01/2010 BMSD 36.0 120 3 (< 20 ) 30.0 ug/L 02/01/2010 Styrene BMS (0.620) U 33.3 111 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 32.8 109 1 (< 20 ) 30.0 ug/L 02/01/2010 Dibromomethane BMS (0.620) U 33 110 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 32.9 110 1 (< 20 ) 30.0 ug/L 02/01/2010 trans-1,3-Dichloropropene BMS (0.620) U 34.9 116 ( 80-124 ) 30.0 ug/L 02/01/2010 BMSD 35.2 117 1 (< 20 ) 30.0 ug/L 02/01/2010 1,2,4-Trichlorobenzene BMS (0.620) U 34.4 115 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 34.3 114 0 (< 20 ) 30.0 ug/L 02/01/2010 Acetone BMS (6.20) U 88.4 98 ( 50-135 ) 90.0 ug/L 02/01/2010 BMSD 91.6 102 4 (< 20 ) 90.0 ug/L 02/01/2010 1,1,2,2-Tetrachloroethane BMS (0.300) U 35.8 119 ( 76-123 ) 30.0 ug/L 02/01/2010 BMSD 35.9 120 0 (< 20 ) 30.0 ug/L 02/01/2010Matrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) VXX20444 Volatiles Extraction AFCEE 3.1 8260 (W) 02/01/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,2-Dibromo-3-chloropropane BMS (1.24) U 37.7 126 ( 73-130 ) 30.0 ug/L 02/01/2010 BMSD 36.9 123 2 (< 20 ) 30.0 ug/L 02/01/2010 Methyl-t-butyl ether BMS (3.00) U 56.4 125 * ( 80-120 ) 45.0 ug/L 02/01/2010 BMSD 55.7 124 * 1 (< 20 ) 45.0 ug/L 02/01/2010 Tetrachloroethene BMS (0.620) U 33.4 111 ( 79-122 ) 30.0 ug/L 02/01/2010 BMSD 32.6 109 2 (< 20 ) 30.0 ug/L 02/01/2010 Dibromochloromethane BMS (0.300) U 31.3 104 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 30.4 101 3 (< 20 ) 30.0 ug/L 02/01/2010 1,3-Dichloropropane BMS (0.240) U 35 117 ( 80-121 ) 30.0 ug/L 02/01/2010 BMSD 34.4 115 2 (< 20 ) 30.0 ug/L 02/01/2010 1,2-Dibromoethane BMS (0.620) U 33.8 113 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 33.8 113 0 (< 20 ) 30.0 ug/L 02/01/2010 Carbon tetrachloride BMS (0.620) U 33.4 111 ( 80-126 ) 30.0 ug/L 02/01/2010 BMSD 33.1 110 1 (< 20 ) 30.0 ug/L 02/01/2010 1,1,1,2-Tetrachloroethane BMS (0.300) U 35.2 117 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 34.8 116 1 (< 20 ) 30.0 ug/L 02/01/2010 Chloroform BMS (0.600) U 31.8 106 ( 80-124 ) 30.0 ug/L 02/01/2010 BMSD 31.8 106 0 (< 20 ) 30.0 ug/L 02/01/2010 Bromobenzene BMS (0.620) U 32.6 109 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 33.0 110 2 (< 20 ) 30.0 ug/L 02/01/2010 Chloromethane BMS (0.620) U 36.3 121 ( 67-125 ) 30.0 ug/L 02/01/2010 BMSD 35.8 119 1 (< 20 ) 30.0 ug/L 02/01/2010 1,2,3-Trichloropropane BMS (0.620) U 33.2 111 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 33.6 112 1 (< 20 ) 30.0 ug/L 02/01/2010 Bromomethane BMS (1.88) U 33.9 113 ( 30-140 ) 30.0 ug/L 02/01/2010 BMSD 35.6 119 5 (< 20 ) 30.0 ug/L 02/01/2010 Bromochloromethane BMS (0.620) U 29.1 97 ( 77-129 ) 30.0 ug/L 02/01/2010 BMSD 29.3 98 1 (< 20 ) 30.0 ug/L 02/01/2010 Vinyl chloride BMS (0.620) U 30.6 102 ( 72-145 ) 30.0 ug/L 02/01/2010 BMSD 30.8 103 1 (< 20 ) 30.0 ug/L 02/01/2010 Dichlorodifluoromethane BMS (0.620) U 35.9 120 ( 62-153 ) 30.0 ug/L 02/01/2010 BMSD 35.9 120 0 (< 20 ) 30.0 ug/L 02/01/2010 Chloroethane BMS (0.620) U 30.3 101 ( 67-133 ) 30.0 ug/L 02/01/2010 BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 02/01/2010 sec-Butylbenzene BMS (0.620) U 35.5 118 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 36.0 120 1 (< 20 ) 30.0 ug/L 02/01/2010 Bromodichloromethane BMS (0.300) U 34.9 116 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 34.7 116 1 (< 20 ) 30.0 ug/L 02/01/2010 1,1-Dichloroethene BMS (0.620) U 29.1 97 ( 76-130 ) 30.0 ug/L 02/01/2010 BMSD 28.7 96 2 (< 20 ) 30.0 ug/L 02/01/2010Matrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) VXX20444 Volatiles Extraction AFCEE 3.1 8260 (W) 02/01/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) BMS (6.20) U 100 111 ( 66-136 ) 90.0 ug/L 02/01/2010 BMSD 102 114 2 (< 20 ) 90.0 ug/L 02/01/2010 Methylene chloride BMS (2.00) U 27.9 93 ( 63-131 ) 30.0 ug/L 02/01/2010 BMSD 27.7 93 1 (< 20 ) 30.0 ug/L 02/01/2010 Trichlorofluoromethane BMS (0.620) U 30.8 103 ( 68-145 ) 30.0 ug/L 02/01/2010 BMSD 30.7 102 1 (< 20 ) 30.0 ug/L 02/01/2010 P & M -Xylene BMS (1.24) U 68.2 114 ( 80-120 ) 60.0 ug/L 02/01/2010 BMSD 67.7 113 1 (< 20 ) 60.0 ug/L 02/01/2010 Naphthalene BMS (1.24) U 35.9 120 ( 75-120 ) 30.0 ug/L 02/01/2010 BMSD 36.1 120 0 (< 20 ) 30.0 ug/L 02/01/2010 o-Xylene BMS (0.620) U 32.5 108 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 02/01/2010 Bromoform BMS (0.620) U 32.3 108 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 30.9 103 4 (< 20 ) 30.0 ug/L 02/01/2010 1-Chlorohexane BMS (0.620) U 50.5 112 ( 70-125 ) 45.0 ug/L 02/01/2010 BMSD 50.5 112 0 (< 20 ) 45.0 ug/L 02/01/2010 1,2,4-Trimethylbenzene BMS (0.620) U 34.9 116 ( 80-125 ) 30.0 ug/L 02/01/2010 BMSD 36.1 120 3 (< 20 ) 30.0 ug/L 02/01/2010 tert-Butylbenzene BMS (0.620) U 34.2 114 ( 80-122 ) 30.0 ug/L 02/01/2010 BMSD 34.9 116 2 (< 20 ) 30.0 ug/L 02/01/2010 1,1,1-Trichloroethane BMS (0.620) U 33.5 112 ( 80-122 ) 30.0 ug/L 02/01/2010 BMSD 32.9 110 2 (< 20 ) 30.0 ug/L 02/01/2010 1,1-Dichloroethane BMS (0.620) U 37.9 126 * ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 38.0 127 * 0 (< 20 ) 30.0 ug/L 02/01/2010 2-Chlorotoluene BMS (0.620) U 35 117 ( 80-125 ) 30.0 ug/L 02/01/2010 BMSD 36.1 120 3 (< 20 ) 30.0 ug/L 02/01/2010 Trichloroethene BMS (0.620) U 33.5 112 ( 80-125 ) 30.0 ug/L 02/01/2010 BMSD 32.7 109 2 (< 20 ) 30.0 ug/L 02/01/2010 trans-1,2-Dichloroethene BMS (0.620) U 33.6 112 ( 79-132 ) 30.0 ug/L 02/01/2010 BMSD 33.3 111 1 (< 20 ) 30.0 ug/L 02/01/2010 1,2-Dichlorobenzene BMS (0.620) U 33 110 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 33.6 112 2 (< 20 ) 30.0 ug/L 02/01/2010 2,2-Dichloropropane BMS (0.620) U 34.6 115 ( 80-132 ) 30.0 ug/L 02/01/2010 BMSD 34.8 116 1 (< 20 ) 30.0 ug/L 02/01/2010 Hexachlorobutadiene BMS (0.620) U 33.2 111 ( 77-125 ) 30.0 ug/L 02/01/2010 BMSD 32.3 108 3 (< 20 ) 30.0 ug/L 02/01/2010 Isopropylbenzene (Cumene) BMS (0.620) U 34.5 115 ( 80-121 ) 30.0 ug/L 02/01/2010 BMSD 34.4 115 0 (< 20 ) 30.0 ug/L 02/01/2010 1,2-Dichloropropane BMS (0.620) U 35.4 118 ( 80-121 ) 30.0 ug/L 02/01/2010 BMSD 35.5 118 0 (< 20 ) 30.0 ug/L 02/01/2010Matrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) VXX20444 Volatiles Extraction AFCEE 3.1 8260 (W) 02/01/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1-Dichloropropene BMS (0.620) U 34.8 116 ( 80-122 ) 30.0 ug/L 02/01/2010 BMSD 34.2 114 2 (< 20 ) 30.0 ug/L 02/01/2010 1,1,2-Trichloroethane BMS (0.620) U 34.7 116 ( 77-120 ) 30.0 ug/L 02/01/2010 BMSD 33.7 112 3 (< 20 ) 30.0 ug/L 02/01/2010 1,3-Dichlorobenzene BMS (0.620) U 33.7 112 ( 80-120 ) 30.0 ug/L 02/01/2010 BMSD 34.0 113 1 (< 20 ) 30.0 ug/L 02/01/2010 1,2,3-Trichlorobenzene BMS (0.620) U 31.8 106 ( 77-120 ) 30.0 ug/L 02/01/2010 BMSD 33.6 112 5 (< 20 ) 30.0 ug/L 02/01/2010 Xylenes (total) BMS (2.00) U 101 112 ( 80-120 ) 90.0 ug/L 02/01/2010 BMSD 99.6 111 1 (< 20 ) 90.0 ug/L 02/01/2010 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 29.4 98 ( 73-120 ) 02/01/2010 BMSD 29.7 99 1 02/01/2010 Toluene-d8 <surr> BMS 29.2 97 ( 80-120 ) 02/01/2010 BMSD 29.2 97 0 02/01/2010 4-Bromofluorobenzene <surr> BMS 30.9 103 ( 76-120 ) 02/01/2010 BMSD 31.3 104 1 02/01/2010
Batch Method Instrument 

### VMS11092

SW8260B HP 5890 Series II MS1 VJA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) XXX22249 3520 Liquid/Liquid Ext for 8270 SIM 02/01/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### Acenaphthylene BMS (0.0320) U .484 88 ( 50-101 ) 0.549 ug/L 02/02/2010 BMSD 0.419 76 14 (< 30 ) 0.549 ug/L 02/02/2010 Acenaphthene BMS (0.0320) U .447 81 ( 45-93 ) 0.549 ug/L 02/02/2010 BMSD 0.411 75 9 (< 30 ) 0.549 ug/L 02/02/2010 Fluorene BMS (0.0320) U .465 85 ( 50-98 ) 0.549 ug/L 02/02/2010 BMSD 0.432 79 7 (< 30 ) 0.549 ug/L 02/02/2010 Phenanthrene BMS (0.0320) U .486 89 ( 50-104 ) 0.549 ug/L 02/02/2010 BMSD 0.471 86 3 (< 30 ) 0.549 ug/L 02/02/2010 Anthracene BMS (0.0320) U .474 86 ( 55-105 ) 0.549 ug/L 02/02/2010 BMSD 0.467 85 1 (< 30 ) 0.549 ug/L 02/02/2010 Fluoranthene BMS (0.0320) U .632 115 * ( 58-109 ) 0.549 ug/L 02/02/2010 BMSD 0.646 117 * 2 (< 30 ) 0.549 ug/L 02/02/2010 Pyrene BMS (0.0320) U .549 100 ( 56-105 ) 0.549 ug/L 02/02/2010 BMSD 0.558 102 2 (< 30 ) 0.549 ug/L 02/02/2010 Benzo(a)Anthracene BMS (0.0320) U .59 107 ( 55-120 ) 0.549 ug/L 02/02/2010 BMSD 0.601 109 2 (< 30 ) 0.549 ug/L 02/02/2010 Chrysene BMS (0.0320) U .497 91 ( 56-109 ) 0.549 ug/L 02/02/2010 BMSD 0.509 93 2 (< 30 ) 0.549 ug/L 02/02/2010 Benzo[b]Fluoranthene BMS (0.0320) U .557 101 ( 45-120 ) 0.549 ug/L 02/02/2010 BMSD 0.564 103 1 (< 30 ) 0.549 ug/L 02/02/2010 Benzo[k]fluoranthene BMS (0.0320) U .525 96 ( 56-112 ) 0.549 ug/L 02/02/2010 BMSD 0.530 97 1 (< 30 ) 0.549 ug/L 02/02/2010 Benzo[a]pyrene BMS (0.0320) U .588 107 ( 57-110 ) 0.549 ug/L 02/02/2010 BMSD 0.593 108 1 (< 30 ) 0.549 ug/L 02/02/2010 Indeno[1,2,3-c,d] pyrene BMS (0.0320) U .561 102 ( 55-111 ) 0.549 ug/L 02/02/2010 BMSD 0.558 102 1 (< 30 ) 0.549 ug/L 02/02/2010 Dibenzo[a,h]anthracene BMS (0.0320) U .56 102 ( 54-113 ) 0.549 ug/L 02/02/2010 BMSD 0.567 103 1 (< 30 ) 0.549 ug/L 02/02/2010 Benzo[g,h,i]perylene BMS (0.0320) U .545 99 ( 49-116 ) 0.549 ug/L 02/02/2010 BMSD 0.548 100 1 (< 30 ) 0.549 ug/L 02/02/2010 Naphthalene BMS (0.0664) U .363 66 ( 44-89 ) 0.549 ug/L 02/02/2010 BMSD 0.288 52 23 (< 30 ) 0.549 ug/L 02/02/2010 1-Methylnaphthalene BMS (0.0320) U .367 67 ( 42-92 ) 0.549 ug/L 02/02/2010 BMSD 0.312 57 16 (< 30 ) 0.549 ug/L 02/02/2010 2-Methylnaphthalene BMS (0.0320) U .302 55 ( 45-89 ) 0.549 ug/L 02/02/2010 BMSD 0.254 46 17 (< 30 ) 0.549 ug/L 02/02/2010 Surrogates 

### Terphenyl-d14 <surr> BMS .577 105 ( 50-126 ) 02/02/2010 BMSD 0.563 102 3 02/02/2010Matrix SGS Ref.# Printed Date/Time 

### 02/05/2010 9:27 Batch Method Date Original Prep 

### 1100319002 Billable Matrix Spike 1100319003 Billable Matrix Spike Dup.

1100319001 Water (Surface, Eff., Ground) XXX22249 3520 Liquid/Liquid Ext for 8270 SIM 02/01/2010

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5285

8270D SIMS HP 6890/5973 MS SVQA

# Appendix B Monitoring Well Construction Logs

# GEOLOGIC BOREHOLE LOG

Location: 

### RHFSF Station Name: Location Type: Location Description: 

### RHMW04 Establishing Company: 

### TEC Inc. Drilling Foreman: 

### Tomas Fernandez Drilling Company: 

### Valley Well Drilling Geologist: 

### N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: 

### MSL Drilling Sampling Method: Borehole Diameter (in): 

### 8 Total Depth (ft): Date Drilling Started: 

### 22 July 2005 Date Drilling Ended: 

### 26 July 2005 Monitoring Well

Remarks: Rock Coring west. access rd., S of Navy Firing Range



### 313.03

320.5

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# GEOLOGIC BOREHOLE LOG

Location: 

### RHFSF Station Name: Location Type: Location Description: 

### RHMW04 Establishing Company: 

### TEC Inc. Drilling Foreman: 

### Tomas Fernandez Drilling Company: 

### Valley Well Drilling Geologist: 

### N. Griffin/S. MacMillan Ground Surface Elevation (ft): Datum: 

### MSL Drilling Sampling Method: Borehole Diameter (in): 

### 8 Total Depth (ft): Date Drilling Started: 

### 22 July 2005 Date Drilling Ended: 

### 26 July 2005 Monitoring Well

Remarks: Rock Coring west. access rd., S of Navy Firing Range



### 313.03

320.5

Page 2 of 2