Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

676 C.D. McIntosh, Jr. 2 

## No.6 Fuel Oil (residual or bunker C)

### Fuel Type 2 Fuel Type 3 Other Fuel Description 

## No.6 Fuel Oil (residual or bunker C) other natural gas

### EIA

Facility Code Facility Name Boiler ID Basis An alyte An alysis M ethod for each Analyte (example: ASTM D5865-04) 

## 676 C.D. McIntosh, Jr. 2 As Received Higher Heating Value 

## ASTM D-240 676 C.D. McIntosh, Jr. 2 As Received % Moisture 

## ASTM D95 676 C.D. McIntosh, Jr. 2 As Received % Ash 

## ASTM D-482 676 C.D. McIntosh, Jr. 2 As Received % Sulfur 

## ASTM D-1552 676 C.D. McIntosh, Jr. 2 Dry basis Higher Heating Value 

## ASTM D-240 676 C.D. McIntosh, Jr. 2 Dry basis % Ash 

## ASTM D-482 676 C.D. McIntosh, Jr. 2 Dry basis % Sulfur 

## ASTM D-1552 676 C.D. McIntosh, Jr. 2 Dry basis Antim ony 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Arsenic 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Bery llium 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Cadmium 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Chlorine 

## EPA 5050/9056 676 C.D. McIntosh, Jr. 2 Dry basis Chromium 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Cobalt 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Fluorine 

## EPA 5050/9056 676 C.D. McIntosh, Jr. 2 Dry basis Lead 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Manganese 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Mercury 

## EPA 7470 676 C.D. McIntosh, Jr. 2 Dry basis Nickel 

## EPA 6010 676 C.D. McIntosh, Jr. 2 Dry basis Selenium 

## EPA 6010EIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 676 C.D. McIntosh, Jr. 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 1 

## 7/23/2010 7/23/2010 18777.00 Btu/lb 2 7/23/2010 7/23/2010 18740.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0 0.03 0.69 18777 Btu/lb 0.03 0.69 0 0.034 0.69 18740 Btu/lb 0.034 0.69Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

## 23.1 ppm <0.10 mg/Kg <0.65 mg/Kg <0.8 mg/Kg <0.48 39.2 ppm <0.10 mg/Kg 1.28 mg/Kg <0.8 mg/Kg <0.48Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg 0.4 mg/Kg mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg 0.622 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 3.82 mg/Kg <1.2 mg/Kg <10 ppm <57 mg/Kg 0 17.8 mg/Kg <1.2 mg/Kg <10 ppm <57 mg/Kg 0 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



## 0.03 87.6 10.3 0.2 0.69 0.03 87.6 10.3 0.2 0.69 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygenEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 676 C.D. McIntosh, Jr. 2 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### 1 

## 7/20/2010 7/22/2010 18712.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0 0.036 0.69 18712 Btu/lb 0.036 0.69Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

## 31.2 ppm <0.10 mg/Kg <0.65 mg/Kg <0.8 mg/Kg <0.48Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg <0.2 mg/Kg <0.8 mg/Kg 1.4 mg/Kg 0.65 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

## 16.6 mg/Kg 3.42 mg/Kg <10 ppm <57 mg/Kg

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



## 0 0.036 87.6 10.3 0.2 0.69 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

OxygenEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 676 C.D. McIntosh, Jr. 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 1 

## 7/20/2010 7/20/2010 18704.00 Btu/lb 2 7/21/2010 7/21/2010 18696.00 Btu/lb 3 7/22/2010 7/22/2010 18696.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0 0.042 0.68 18704 Btu/lb 0.042 0.68 0 0.038 0.69 18696 Btu/lb 0.038 0.69 0 0.034 0.68 18696 Btu/lb 0.034 0.68Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

## 75.7 ppm <10 mg/Kg 0.91 mg/Kg <0.8 mg/Kg <0.48 76 ppm <10 mg/Kg 0.92 mg/Kg <0.8 mg/Kg <0.48 65.1 ppm <10 mg/Kg 0.9 mg/Kg <0.8 mg/Kg <0.48Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg 0.56 mg/Kg mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg 0.78 mg/Kg mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg 0.42 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 12.8 mg/Kg 2.7 mg/Kg <10 ppm <57 mg/Kg 0 15 mg/Kg 2.32 mg/Kg <10 ppm <57 mg/Kg 0 9.07 mg/Kg 1.86 mg/Kg <10 ppm <57 mg/Kg 0 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 0.042 87.9 10.3 0.2 0.68 0.038 88.9 10.4 0.2 0.69 0.034 87.9 10.3 0.2 0.68 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

## 676 C.D. McIntosh, Jr. 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### 1 

## 6/4/2010 6/4/2010 18728.00 Btu/lb 2 6/4/2010 6/5/2010 18698.00 Btu/lb Fuel Testing Results

## Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

## 0 0.032 0.69 18728 Btu/lb 0.032 0.69 0 0.018 0.67 18698 Btu/lb 0.018 0.67Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

## 21.9 ppm 0.005 mg/Kg 0.38 mg/Kg <0.8 mg/Kg <0.10 29.7 ppm <0.001 mg/Kg 0.32 mg/Kg <0.8 mg/Kg <0.10Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

## mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg <1 mg/Kg mg/Kg <0.2 mg/Kg <0.8 mg/Kg <1.4 mg/Kg <1 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

## 21.6 mg/Kg 1.4 mg/Kg <9.9 ppm 0.33 mg/Kg 0 19.7 mg/Kg 1.03 mg/Kg <9.9 ppm 0.251 mg/Kg 0 Proximate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen



## 0.032 88.7 12.8 <0.2 0.69 0.018 88.7 12.9 <0.2 0.67 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary.

Fuel Units of Measure - HHV Units of Measure - Cl, Fl anthracite Btu/lb % bituminous Btu/gallon ppm subbituminous mg/Kg lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg