) 

I 

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) 

2011 Primary Aluminum 

Potline and Anode Bake Furnace MACT Test Program 

Report Certification 

I certify that to the best of my knowledge: 

o Testing data and all corresponding information have been checked for 

accuracy and completeness. 

o Sampling and analysis have been conducted in accordance with the approved 

protocol and applicable reference methods (as applicable). 

o All deviations, method modincations, or sampling and analytical anomalies 

are summarized in the appropriate report p.arrative(s). 

1:2 ~;2- /l 

Date 

TRC was operating in conformance with the requirements of ASTM D7036-04 during 

this test program. 

9.v0Bp.:i Jeffrey . Burdette · 

TRC Air Measurements Technical Director 
( ) 

----

TABLE 1-2 

TEST RUN TIMES- POM TEST RUNS 

ALCOA WARRICK OPERATIONS 

Date 

Anode Baking Ring Furnace (A-446) Reactor# 1 

Run 1 24-0ct 

Run 2 24-0ct 

Run 3 24-0ct 

Anode Baking Ring Furnace (A-446) Reactor# 3 

Run 1 24-0ct 

Run 2 24-0ct 

Run 3 24-0ct 

· Start Stop 

10:30 13:24 

14:30 17:25. 

19:35 21:44 

10:30 12:59 

14:30 17:25 

19:35 22:26 
Alcoa- iFarrick Operations 

Ne1vburs;h, LN -

SECTION2.0 

SUMMARY OF TEST RESULTS 

Table 2-1 summarizes the POM results for the reactors. The mass emission.rate of POM from 

each reactor and the combined mass emission rate from both reactors are shown as lb/hr values 

as well as on the basis of lbs/ton of green anode throughput. The average POM emission rate 

from the A-446 Reactor# 1 was 0.0515 lbs/ton of green anode. The average POM emission rate 

from the A-446 Reactor # 3 was 0.0377 lbs/ton of green anode (after adjustment for: low 

isokinetic rates). As di~cussed further in Section 7, the POM emission rates for Reactor#. 3 for· 

Run 1 and Run 2 were adjusted (increased) to correct for the low isokinetic sampling rates for 

these two ljlillS. The combiried POM emission rate for the A-446 Reactors was 0.0893 lb/ton of·· 

green anode (adjusted values) .. 

Table 2-2 summarizes the PM r~sults derived from Method 315 for the reactors. The .mass 

emission rate of PM from e!lch reactor and th~ combined mass emission rate from both reactors 

are shown as lb/h! values as well as on the basis of lbs/ton of green anode throughput. · The 

average PM emission rate from the A-446 Reactor# 1 was 0.0179 lbs/ton of green anode. The 

average PM emission rate from the A-446 Reactor# 3 was 0.0628 lbs/ton of green anode (after 

adjustmeny for low isokinetic rates). As discussed further in Section 7, the PM emission rates for 

Reactor # 3 for Run 1 and Run 2 were adjusted (increased) to correct for the low isokinetic 

sampling rates for these two runs. The combined PM emission rate for the A-446 Reactors was 

0.0808 lb/tpn of green. anode (adjusted values). ! . . . . 

The stack test data and te.st results for each test method and each test run conducted are provided .. 

in more detailed tables through this report. 

. ·•·· ·-·-·-.-··-· '•·•··•·•· .r--'7-' 

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tons/hr 

lblhr 

Ibs/ton of Green Anode 

( 

---..___./ 

TABLE 2-1 

POM TEST RESULTS 

A-446 REACTORS 

ALCOA-WARRICK OPERATIONS 

NEWBURGH, IN 

A-446 REACTOR# 1 

Green Anode Throughput 

Reactor Emission Rate 

Emission Rate 

Run#1 

19.85 

1.111 

0.0560 

Run#2 

19.85 

0.896 

0.0451 

Run#3 A

19.85 

1.062 

0.0535 ! 0

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tons/hr 

lb/hr 

lbs/ton of Green Anode 

lblhr 

lbs/ton of Green Anode 

A-446 REACTOR# 3 

Green Anode Throughput 

Reactor Emission Rate 

Emission Rate 

Reactor Emission Rate, iso adjusted 

Emission Rate, iso adjusted 

19.85 

0.665 

0.0335 

0.759 

0.0382 

19.85 

0.785 

0.0395 

0.913. 

0.0460 

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19.85 l 

0.576 

0.0290 

0.576 

0.0290 

. ' . 

0

0

0

--------------------------------------------.-----------------------=------------------------------------------------:-----------;,..-________________ ,_ ______

tonslhr 

lb/hr 

lbs/ton of Green Anode 

NOTE: 

COMBINED A-446· REACTORS # 1 & # 3 

Green Anode Throughput 19.85 19.85 19.85 

Reactor Emission Rate 1.776 1.681 1.638 

Emission Rate 0.0895 0.0847 0.0825 

Reactor Emission Rate, iso adjusted 1.870 1.809 1.638 

Emission Rate, -iso adjusted 0.0942 0.0911 0.0825 

The Run 1 and Run 2 POM emission results for Reactor# 3 were adjusted (increased) to correct' for the low isoki.netic sampling rate during those two test runs. 

0

0
tons/hr 

lb/hr 

lbs/ton of Green Anode 

TABLE2-2 

PM TEST RESULTS 

A-446 REACTORS 

ALCOA- WARRICK OPERATIONS 

NEWBURGH, IN 

A-446 REACTOR# 1 

Green Anode Throughput 

Reactor Emission Rate 

Emission Rate 

Run#1 

19.85 

0.281 

0.0141 

Run#2 

19.85 

0.356 

0.0179 

Run#3 

19

0.4

0.02

~~---------------------------------------------------------------------------------------------------------------------------------------------------

tons/hr 

lb/hr 

lbs/ton of Green Anode 

lb/hr 

lbs/ton of Green Anode 

A-446 REACTOR# 3 

Green Anode Throughput 19.85 

Reactor Emission Rate 0.822 

Emission Rate 0.0414 

Reactor Emission Rate, iso adjusted 0.939 

Emission Rate, iso adjusted 0.0473 

19.85 

1.166 

0.0587 

1.355 

0.0683 

19

1.4

0.07

1.4

0.07

1~---------------------------------------------------------------------------------------------------------------------------------------------------

·tons/hr 

lb/hr 

lbs/ton of Green Anode 

lb/hr. 

lbs/ton of Green Anode 

NOTE 

COMBINED A-446 :REACTORS # 1 & # 3 

Green Anode Throughput . ~9.85 19.85 19

Reactor Emission Rate 1.103 1.522 1.8

Emission Rate 0.0556 0.0767 0.09

Reactor Emission Rate, iso adjusted 1.219 1.712 1.8

Emission Rate, isb adjusted 0.0614 0.0862 0.09

The Rtm 1 and Run 2 PM emisison results for Reactor # 3 were adj1.1sted (increased

to correct for the low isokinetic sampling rate during those two test runs 
) 

·._ ) 

Alcoa- Warrick Operations 

Newburgh, IN 

SECTION 3.0 

DESCRIPTION OF SOURCES AND SAMPLING LOCATIONS 

. 3.1 DESCRIPTION OF PROCESS 

---~---------------------------· ·--=----------------------- The anode baking furnace is comprised of one green anode ring baking furnace controlled by a 

common Alcoa designed A-446 emission control device. The baking furnace structure is a series 

of interconnected refractory flues connected to side main exhaust manifolds. Ptoducts of 

combustion and other ~missions created .in the baking fumace are drawn into the refractory flues_· 

and exhausted to the- common control equipment through a se1ies of ducts. The furnace is fueled 

with natural gas. 

In the baking furnace, green anodes are stacked into sub-surface pits foim-ed by -the 

interconnecting flue. structures. After being placed in the pits, the green anode material is 

surrounded and covered with petroleum coke referred to as "packing material". The baking 

process is operated to allow recently filled pits to be preheated for a period of time bef0re being 

actively fired. Likewise, after firing, baked anodes are allowed to cool in the pits before they are 

removed and used in the smelting process. Natural gas burners supply heat to the furnace and 

promote the combustion of organic constituents drawn into the flues during the baking,process. 

The preheating, heating, and cooling processes are sequenced around the fumace im.either a 

clockwise or counter clockwise direction. 

Emissions from the anode bake furnace are collected and treated by an integrated system of 

ducting and a -pollution control system. The control system employed at the Warrick Operation 

anode baking furnace is a multi-unit, fluid-bed reactor type system with fabric :filtration 

downstrean1 of the re~ctor beds. Smelting grade alumina is introduced into one -enctoftb:~, Alcoa.. · · 

designed A-446 reactors. -The alumina is fluidized by an auxiliary fluid~zing fan blowing. 

ambient air through a s·eries of perforated plates in the bottom of the reactor .Chamber. A.p.ode· · 

baking_ furnace emissions are introduced into ,tlie fluidized bed through exhaust gas map.i,iqlds > 

along each side of the reactor. The fluid bed provides a site for fluoride to rea~t with the alm$ina · 

and for the gas stream to be cooled. The fabric filtration devices are positimied atop .of the ~uid 

beds to collect entrained alumina particles and -other particulate matter present in the ·gas stre~. 

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Newburo-Jz, IN 

"·-·-··-····--· ----······-···----..,..-------------

3.2 SAMPLING LOCATIONS 

Metho.d 1 datasheets and traverse point locations are provided in Appendix A for each of the 

sampling locations. ----

) 

..' 

The anode bake furnace primary system consists of a single dry alumina scrubber .control. device. 

with three (3) reactor sections or compartments. Two compartments (Reactor No. 1 and Reactor 

No.2) on the anode furnace control device have three stacks and one compartment (Reactor No. 

3) has only one stack. 

The Green Anode Baking Ring Furnace exhausts through seven (7) separate stacks. Three stacks 

- . 

for Reactor No. 1 and three stacks for Reactor No.2 and one stack for Reactor No.3. The stacks 

for Reactor No. 1 and Reactor No. 2 are identical. These vertical stacks have an internal 

diameter of 26.25-inches. The location of the two test ports (90° apart) are 60-inches (2.3 duct 

diameters) do,wnstream from the nearest d~sturbance, and 232-inc.hes (8.8 duct diameters) 

upstream from the exhaust. "For Reactor No. 3, the inside diameter of the stack is 46-inches, and 

it has two test ports (90° apart). The ports are Q2.5-inches (2 duct diameters) downstream frorri 

the nearest disturbance, and 192-inches (4.2 duct diameters) upstream from the exhaust. For 

particulat~ measurements conforming to Method 5 (as referenced in Method 13A and Method 

315) a total of 24 traverse points were used at each stack for the velocity and TF and POM 

measurements, 12 traverse points per port. 

:.·:0 __ _ 

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1._ ) , __ _...,. 

Alcoa- Warrick Operations 

Newburgh, IN 

.• 

·.c 

26.25inches 

.Sample Ports 

0 

FLOW 

' . . , 

232 inches 

6.0~ches 

Figure 3-3. A-446 Reactor No. 1 Stack Sampling Locations 

C:IALCOA PROJECTS\186567-Warrick PMACT 2011\Reports\Test Report-Pot lines & Bake Furnace Rpt.doc 

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Alcoa- Warrick Operations 

Newburgh, IN 

46 · :inches 

Sample Ports 

-0 

FLOW ,.. .. 

192 inches 

92.5 inches 

Roof 

Figure 3-4. A-446 Reactor No. 3 Stack Sampling Location 

C:\ALCOA PROJECTS\186567-Wanick PMACT 201 1\ReportsiTest Report-Potlines & Bake Furnace Rpt.doc 

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Alcoa- Warrick Operations 

Newburgh, IN 

SECTION 4.0 

SAMPLING AND ANALYTICAL PROCEDURES 

The sampling and analytical procedures that were used in this test program are described below. 

The referenced EPA sampling and analytical procedures are available from the EPA TTN 

EMTIC electronic bulletin board. 

4.1 SAMPLING TRAVERSE POINTS 

The number and location of the sampling traverse points were detem1ined according to the 

procedures outlined in EPA Method 1. Prior to conducting the emission tests, TRC measured the 

stack dimensions and distances to gas flow disturbances. The actual number and location of the 

traverse points were dete1mined using EPA Method 1. 

4.2 VOLUMETRIC FLOW 

4.2.1 Flue Gas Velocity 

The velocity was determined according to the procedures outlined in EPA Method 2. Velocity 

head (delta P) measurements were made using TypeS Pitot tubes conforming to the geometric 

specifications outlined in EPA Method 2 and having a coefficient of 0. 84. The differential 

pressures were measured using a fluid manometer. The exhaust gas temperatures were measured 

using chromel-alumel thermocouples and associated digital readouts. 

4.2.2 Exhaust Gas Composition 

The potline flue gas contains ambient air that is drawn from hoods above the pots inside of the 

smeltin·g building. The oxygen content was assumed to be 20.9% and the carbon dioxide was 

assumed to be 0%. The anode furnace A-446 reactor flue gas composition was measured by 

collecting integrated Tedlar bag samples during each test run. These bag samples were analyzed 

onsite with an Orsat. 

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Alcoa - Warrick Operations 

Newburalz, IN 

4.4 POLYCYCLIC ORGANIC MATTER 

Method 315 "Determination of Patiiculate and Methylene Chloride Extractable Matter (MCEM) 

from Selected Sources at Primary Aluminum Production Facilities" was used to measure the 

polycyclic organic matter (POM) emissions. This method uses a Method 5 style sampling train. 

4.4.1 Sample Collection 

Samples were collected isokinetically (90% to 110%) from the stack using an EPA Method 5 · 

style sampling train. The sampling train consisted of a glass nozzle, connected to a glass-lined 

probe with a Type S Pitot tube attached. The sample was passed through a heated filter 

maintained at 248 °F (within 25 °F) provided by Alcoa. After passing through the filter, the 

sample stream was connected to the Method 5 style back -half which consisted of four impingers. 

The first two impingers each contained 1 00-ml of deionized distilled (DI) water, the third 

impinger was empty and the fourth impinger contained silica gel. Each impinge!' was weighed 

( ) prior to sample train assembly. The sample train was connected to a standard Method 5 metering ·· ... _./ 

console. 

4.4.2 Sample Recovery 

After the completion of the test run and following the post..:test leak check, the filter was removed 

from the filter holder and placed in a glass sample jar or petri dish. Following the test run, each 

of the impingers was weighed to determine the post-test weight. The ·weight of water vapor 

condensed in the impingers and the weight of water vapor collected in the silica gel was summed 

and subsequently entered into moisture content calculations. The nozzle, probe, and front.;.. half of 

the filter holder were rinsed with acetone into a glass sample jar. Following the acetone rinses 

the front half of the satnple train was rinsed with methylene chloride· which was collected in· 

another glass jar. The impinger catch was poured into a glass sample jar and then tl1e sample 

train back-half glassware was 1insed first with water, acetone and then with methylene chloride. 

The water rinse was added to the impinger catch sample jar. The two solvent rinses were placed 

in a separate glass sample jar. The filter, impinger catch and DI and solvent rinses were analyzed 

by Alcoa laboratory personnel per Method 315 procedures to determine the polycyclic organic 

matter (POM) content. 

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Alcoa- Warrick Operations 

Newburgh, IN 

SECTION 5.0 

QA/QC PROCEDURES AND RESULTS • 

As a guide, TRC uses the EPA do.cument Quality Assurance Handbook for Air Pollution 

Measurement System, Volume III. TRC's QA/QC plan has incorporated certain considerations to 

the production of quality data in all of its sampling work regardless of the scope and purpose of the 

testing. These considerations include: 

• Planning the testing program; 

• Use of reliable and well-maintained equipment; 

• Use of appropriate fmms for recording sampling data; 

• Establishing . a sample coding system to ensure proper chain of custody (i.e., sample 

identification, laboratory tracing and storage, analysis and reporting); 

e Use of calibration and audit gases traceable to the National Institute of Standards and 

Technology (NIST); 

• Control errors by checking data inputs and perfonning redundant calculations; 

• Adherence to established protocol. 

5.1 BAROMETER 

Barometric pressure values for the testing period were recorded fi:om a calibrated digital barometer 

on-site and verified by side by side comparison to a mercurial barometer located in the TRC Field 

Office in Raleigh, NC. 

5.2 PITOT TUBES 

'\"-) Each Pitot tube used in this sampling program met the design specifications for Type S Pitot tubes 

in EPA Method 2. Therefore in accordance with Method 2 procedures, a baseline coefficient (Cp) 

J:\180000-209999 _Job#•l86567 -Warrick PMACT 2011 \Repo11siTest Report-Potlines & Bake Fumncc Rpt.doc 
Alcoa- Warrick Operations 

Newburaft, IN 

of 0.84 was assigned to each Pitot tube. Calibration at the manufacturer for Pitot face-opening 

alignment included measuring the extemal tubing diameter (dimension D1), the base-to-opening ~ ~ . 

misalignment angles, with all tenns as described in Figures 2-2 and 2-3 of EPA Method 2. Pitot 

tubes were visually inspected prior to and at the completion of the test to insure structural integrity. 

5.3 CALIBRATION METER AND METERING SYSTEM 

TRC calibrates meter boxes at least once per year. The calibration set-up for the dry gas metering 

system using the secondary reference meter in lieu of the wet test meter is given in Figure 5.5 of 

EPA Method 5. A leak check of the metering system before calibration was performed as shown in 

Figure 5.4 of EPA Method 5. The metering system's pump was operated for5 minutes at an orifice 

manometer setting of 0.5 inches H20 to heat up the pump and system to stabilize the meter. inlet 

and outlet temperatures. Values for the orifice setting (delta H), wet test meter volume (V w), 

conesponding dry test meter volume (V ct), dty test meter inlet and outlet gas temperatures (tcti and 

tctn), and time were recorded for the initial calibration. The ratio of the wet test meter to the dry test 

meter (y or gamma) and the orifice pressure differential that equates to the desired sampling rate at· 

standard conditions (delta H@) was then calculated. A copy of the pre-test metering system 

calibration is included in Appendix C to this Test Report. 

5.4 POST-TEST METER CALIBRATION 

As an altemative to performing post-test meter calibration checks, TRC follows EPA Altemative009. This procedure is performed on-site using the data collected for each of the test runs. It is 

prefen·ed by EPA because it eliminates the questions about possible meter damage during transport 

after the emission test and, because the calibration data is available in the field immediately 

following the test, it eliminates the costly travel, remobilization, and scheduling of a retest should 

the meter fail the post-test calibration. These calibration checks are included with ·the field 

datasheets in Appendix A of this. Test Report. 

5.5 THERMOCOUPLES AND DIGITAL INDICATORS 

Them1ocouples were calibrated by comparing them against an ASTM-3F mercury-in-glass 

thennometer at approximately 32°F (ice water), ambient temperature and approximately 212°F 

(boiling water). Each thermocouple was calibrated against temperature ranges to which it was to be 

typically exposed during test conditions, and they must agree within 1.5 percent (expressed in °R) 

of the reference thermometer throughout the entire calibration range. A post calibration was 

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Alcoa- Warrick Operations 

Newburgh, IN 

perfonned in accordance with EPA ALT-OII using a single point calibration against an ASTM 

;nercury-in-glass thern101~eter in addition to a contin,.nity check of the the1mocouple. The 

continuity check involves verifying that the thennocouple read-out trends in the appropriate 

direction when exposed to a temperature change. 

Digital indicators were checked by introducing a series of millivolt signal strengths to the input and 

comparing the indicator reading with the actual signal strength. Acceptable calibration error does 

not exceed 0.5 percent when temperatures are expressed in °R. 

5.6 ANALYTICAL BALANCE 

The analytical- balance was calibrated by comparing readings from its own internal calibration 

weight against a I 00 gram NIST (formerly NBS) Class-S I standard weight. Linearity of the 

balance was demonstrated by further comparison of its readings against other selected (0.5g, lg, 

lOg, 50g) NIST Class S-I weights. The NIST class S-1 weights were calibrated by the NC 

Department of Agricultural Standards Laboratory in Raleigh, NC. 

5.7 REAGENT BLANKS AND FIELD BLANKS 

TRC collected reagent blank samples for Methods 13A and 3I5. These reagent blanks were 

analyzed along with the field samples. 

5.8 CHAIN OF CUSTODY 

A list or log of all samples was prepared and used to maintain the chain of custody of the 

san1ples. Copies of each "sample log" or chain of custody form are included with the laboratory 

report. The field team leader· prepared the satnple log onsite during or at the conclusion of 

sample recovery activities. Samples were carefully packed for transport .to the analytical 

laborato1y. . The samples were transp01ied to the laboratory by TRC. 

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Alcoa- Warrick Operations 

Newburalt, IN 

SECTION :6.0 

CALCULATION OF.RESULTS · 

. .,. ... 

Emission rates in terms of pounds per hour (lbs/lu·) were calculated using the pollutant emission 

concentration expressed in ternis of grruns per dry standard cubic feet and ·milligrams p(:)J:· c1;1bic, 

meter timesthe volumetric gas flow rate expi·essed in terms of dry standard cubicfeetpermin:ute ... · . · 

Emission rates in terms of.powds per hour {lbs/hr).were calculated using the. pollutant emission 

rate in terms of micrograms per dry standard cubic foot (ug/dscf), flowrate ·"" dsc:fi:n (Qs), .60 

minutes/hour, divided by 453,~00,000 ug/lb. 

lbs/hr = (ug/dscf) X ·Qs X 60 

453.6 X 106 

Emission rates in terms of pounds per hour (lbs/hr) were calculated using the pollutant emission 

rate in terms of parts per million (ppm/dry), flowrate - dscfm (Qs), molecular weight of the 

pollutant (MW), 60 minutes/hour, divided by 385.3 X 106 dscf/lb-mole@ 68°F (20°C). 

lbs/hr = ppm X Qs X MW X 60 

385.3 X 106 

For test runs which had isokinetic sampling rates below 90% the emission rates were adjusted 

(increased) by dividing the emission rate by the low isokinetic rate. For example, if the 

isokinetic rate was 86%, then the emission rate was divided by 0.86. For test runs which had 

isokinetic san1pling rates above 110% the emission rates were adjusted (increased) by 

multiplying the emission rate by the high isokinetic rate. For example, if the isokinetic rate was 

114%, then the emission rate was multiplied by 1.14. 

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Alcoa - Warrick Operations 

Newburalz, IN 

: SECTION 7.0 

DISCUSSION 'OF TEST RESULTS 

Table 7-7 provides the POM test data and resul.t's for the A-446 Reactor .. No. 1 stacks. The POM .. 

emission rate averaged 1.023 lb/hr with a range from 0.896 to l.llllb/hr. 

Table 7-8 provides the POM test data and results for the A-446 Reactor No. 3 stack. The POM 

emission ·rate averaged 0.675 lb/hr with a range from 0.576 to 0.785 lb/hr. The isolcinetic rate for 

Run 1 was 87.6% and the isolcinetic rate for Run 2 was 86.0%. In Table 2-3 the POM test results 

for Run 1 and Run 2 were adjusted for these low isolcinetic sampling rates by dividing the Run I··· 

POM mass emission rate by the 0.876 and by dividing the Run 2 POM mass emission rate by 

0.860. This adjustment increases the POM emission rates for these two test runs. 

The field datasheets, laboratory analytical report and procedures, along with the equipment 

calibration documentation are provided in the appendices to this report. 

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TABLE 7-7 

i-

-- "· 

l METHOD 315 POM TEST RESULTS 

ALCOA- WARRICK OPERATIONS 

A-446 REACTOR# 1 (Three Stacks) 

' NEWBURGH, IN ' 

·' •' 

RUN NUMBER ' M315-BH#1-1 M315-BH#1-2 M315-BH#1-3 I AV.ERAGE 

RlUN DATE ·' 10/24/2011 10/24/2011 10/24/2011 ! •' 

RUNTIME 1030-1324 1430-1725 1935-2144 ! 

! 

MEASURED DATA i 

(Y) Meter BoxY 0.9912 0.9912 0.9912 : 

(DeltaH) · Avg Delta H, inches H20 1.11 1.19 1.17 

(Pbar) Barometric Pressure, inches Hg 29.60 29.60 29.60 I 

(Vm) Meter Volume, ft3 85.201 88.809 85.757 

I (Tm) A vg Meter Temp, deg F 73 80 57 

(Pg) Static Pressure, inches H20 -0.22 -0.25 -0.22 I .. 

! 

(Ts) A vg Stack Temp, deg F 173 172 176 ! (Vlc) Water Collected, mL 199.8 159.5 188.9 

I (%C02) Carbon Dioxide; % 3.0 2.6 2.6 2.7 

(%02) Oxygen,% 17.0 17.7 17.0 ! 17.2 

(%N2) Nitrogen,% 80.0 79.7 80.4 ! 80.0 ! 

(Cp) Pitot Tube Coefficient 0.84 0.84 0.84 : 

! 

(DeltaP) Avg Sqrt Delta P, (inches H20)Y, 0.756 0.787 0.800 : 

(Theta) Sample Time, min 144 144 144 i· 

: (Dn) Nozzle Diameter, inches 0.216 0.216 0.214 

I CALCULATED DATA 

} (An) Nozzle Area, square feet 0.000254469 0.000254469 0.000249778 

(Vmstd) Standard Meter Volume, ft3 82.895 85.302 86_052 ! ...... : (Ps) Stack Pressure, inches Hg 29.58 29.58 29.58 ! 

(%H20) Moisture,% 10.2 8.1 9.4 ! 9.2 ! 

(Vwstd) Standard Water Vapor Volume, ft 3 9.421 7.520 8.907 ! 

(Mfd) Dry Mole Fraction 0.898 0.919 0.906 j 

(Md) Molecular Weight-dry, lbllb-mole 29.16 29.12 29.10 I 

(Ms) Molecular Weight-wet, lb/lb-mole 28.02 28.22 28.06 

(Vs) Velocity, ft/s ! 47.5 49.2 50.3 49.0 

(A) Stack Area of Three Stacks, ft2 11.27 11.27 11.27 j 

(Qa) VolumetTic flow, acfm 32,102 33,271 34,032 : 33;135 : (Qs) Volumetric flow, dscfm 23,767 25,233 25,310 

I 

24,770 

(I) Isokinetic Rate, % 107.3 104.0 106.6 

EMISSIONS DATA 

! 

: 

! 

POLYCYCLIC ORGANIC MATTER (POM) ! 

I. (grams) Total POM Catch, g 0:0293 0.0229 0.0273 0.0265 

(mg/dscm) Concen., mg/dscm 12.5 9.5 11.2 I 11.1 

(mg/acm) Concen., mg/actual m3 9.2 7.2 8.3 I 8.3 . 

(gridscf) . Concen., gr/dscf 0.00545 0.00414 0:00490 !' 0.00483 

(gr/acf) Concen., gr/actual cf 0.00404 0.00314 0.00364 ! 0;00361 ! 

(lb/hr) Emission Rate, lb/hr 1.111 0,896 1.062 : 1.-023 

!( 

' I· 

f 

I 

PARTICULATE MATTER (PM) I 

I 

I 

I 

I 

I 

I 

(grams) Total PM Catch, g 0.00740001 0.0091 0.01109999 I 0.0092 I 

I 

I 

(mg/dscm) Concen., mg/dscm 3.2 3.8 4.6 I 3.8 ' I 

I ' 

Concen., mg/ actual m3 ·' I •' (mg/acm) 2.3 2.9 3.4 I 

I .2.9 I 

(gr/dscf) Concen., gr/dscf 0.00138 0.00165 0.00199 I 

.6':00167 I 

I 

I ;;,:.::·· 

(gr/acf) Concen., gr/actual cf 0.00102 0.00125 0.00148 I 

·. ·1w~t~,~:~ I· 

I 5 I 

(lblhr) Emission Rate, lb/hr 0.281 0.356 0.432 I. 

' 

C:!t¥rfi/i 
TABLE 7-8 

METHOD 315 POM TEST RESULTS 

ALCOA- WARRICK OPERATIONS 

A-446 REACTOR# 3 (One Stack) 

NEWBURGH, IN . . .. I' 

RUN NUMBER M315-BH#3-1 M315-BH#3-2 M315-BH#3-3 I AVERAGE 

RUN DATE ' 10/24/2011 10/24/2011 10/24/2011 ~ •' .•I 

RUNTIME 1030- 1259 1430 - 1725 1935- 2226 I 

I 

l 

MEASURED DATA 

I (Y) Meter BoxY 0.9874 0.9874 0.9874· 

(DeltaH). A vg Delta H, inches H20 1.76 1.80 2.25 

(Pbar) Barometric Pressure, inches Hg 29.60 29.60 29.60 I 

(Vm) Meter Volume, ftl 103.111 103.366 111.978 I '! 

(Tm) Avg Meter Temp, deg F 72 73 59 j 

(Pg) ' Static Pressure, inches H20 -0.31 -0.30 . -0.32 ! 

(Ts) A vg Stack Temp, deg F 170 170 169 I 

(VIc) Water Collected, mL 235.6 201.0 239.7 . I. 

(%C02) Carbon Dioxide, % 1.7 2.6 2.4 j 2.2 

(%02) Oxygen,% 18.6 17.3 18.1 i 18.0 i 

(%N2) Nitrogen,% 79.7 80.1 79.5 I 79.8 

(Cp) Pitot Tube Coefficient 0.84 0.84 0.84 ! 

(DeltaP) Avg Sqrt Delta P, (inches H20)Yz 0.775 0.781 0.829. I 

(Theta) Sample Time, min 144 144 144 ! 

(Dn) Nozzle Diameter, inches 0.259 0.259 0.259 I 

I CALCULATED DATA 

(An) Nozzle Area, square feet 0.00036587 0.00036587 0.00036587 I 

(Vmstd) Standard Meter Volume, ft3 100.293 100.399 111.814 

(Ps) Stack Pressure, inches Hg 29.58 29.58 29.58 ! 

I 

(%H20) Moisture,% 10.0 8.6 9.2 I 9.3 

(Vwstd) Standard Water Vapor Volume, ft3 11.109 9.477 11.302 i 

(Mfd) Dry Mole Fraction 0.900 0.914 0.908 I 

(Md) Molecular Weight-dry, lb/lb-rnole 29.02 29.11 29.11 I 

I 

(Ms) Molecular Weight-wet; lbllb-mole 27.92 28.15 28.09 

I (Vs) Velocity, ft/s 48.6 48.8 51.8 -49.7 

(A) Stack Area, ff 11.54 11.54 11.54 

(Qa) Volumetric flow, acfm 33,630 33,785 35,885 I 34,433 

(Qs) Volumetric flow, dscfm 25,092 25,582 27,034 l. 25,903 

(I) Isokinetic Rate, % 87.6 86.0 90.6 \j 

I 

EMISSIONS DATA I 

I 

POLYCYCLIC ORGANIC MATTER (POM) !: 

0.0233 " (grams) Total POM Catch, g 0.0201 0.0180 " 0.0205 J; 

(mg/dscm) Concen., mg/dscm 7.1 8.2 5.7 !-: 7.0 

(mg/acm) Concen., mg/actualm3 5.3 6.2 . 4.3 L· 5.3 

(gr/dsct) Concen., gr/dscf 0.00309 0.00358 0.00248 1: .. 0.00305 

(gr/act) Concen., ,ir/actual cf 0.00231 0.00271 0.00187 1 0.00230 I 

(lb/hr) Emission Rate, lb/hr 0.665 0.785 0.576 I 0.675 I 

! 

PARTICULATE MATTER (PM) 

(grams) Total PM Catch, g 0.02485787 0.0346 0.04519998 0.0349 

(mg/dscm) Concen., mg/dscm 8.8 12.2 14.3 11.8 

(mg/acm) Concen., mg/ actual m3 6.6 9.2 10.8 8.9 

(gr/dsct) Concen., gr/dscf 0.00382 0.00532 0.00623 0.00512 

(gr/act) Concen., gr/actual cf 0.00286 0.00402 . 0.00470 0.00386 

(lb/hr) Emission Rate, lb/hr 0.822 1.166 1.446. 1.145 
(--, 

-. __ ) 

C_J 

METHOD 1 WORKSHEET 

Summary of Location Setup 

COMPANY NAME: 

FACILiTY LOCATION (City, State)·. 

SAMPLING LOCATION: 

Circumference 

Far Wall to Outside of Port 

Inside Wall to Outside of Port 

DIAMETER OF STACK 

DIAMETER OF STACK 

Nearest Upstream Disturbance 

Nearest Dowstream Disturbance 

Nearest Upstream Disturbance 

Nearest Dowstream Disturbance 

Enter Information Below: 

ALCOA- WARRICK OPERATIONS 

Newburgh, IN 

A-446 REACTOR# 1 or #2 (Each of 3 Stacks) 

Inches· 

30 Inches · 

3.75 Inches 

26.25 Inches 

2.19 Feet 

60 Inches 

232 Inches 

2.3 Diameters. 

8.8 Diameters . 

USE 12 TRAVERSE POINTS PER PORT 

TOTAL TRAVERSE POINTS 

EXPECTED RUN DURATION 

TIME PER TRAVERSE POINT 

READINGS EVERY 

EXPECTED READINGS 

24 

144 

6 

6 

24 

24 pt X 3 Stacks 

minutes 

minutes 

minutes 
METHOD 1 

TRAVERSE POINTS 

ALCOA· WARRICK OPERATIONS 

Newburgh, IN 

A-446 REACTOR# 1 or# 2 (Each of 3 Stacks) 

Far Wall to Outside of Port 30 Inches 

Inside Wall to Outside of Port 3.75 Inches 

DIAMETER OF STACK 26.25 Inches 

Nearest Upstream Disturbance 60 Inches 

Nearest Dowstream Disturbance 232 Inches 

NUMBER of Traverse Points per Port. 12 

POINT %of Depth Diameter ··Distance Distance 

from Inside w/ Nipple 

1 0.021 26.25 0.551 4.301 

2 0.067 26.25 1.759 5.509 

3 0.118 26.25 3.098 6.848 

4 0.177 26.25 . 4.646 8.396 

5 0.25 26.25 6.563 10.313 

6 0.356 26.25 9.345 13.095 

7 0.644 26.25 16.905 20.655 

8 0.75 26.25 19.688 23.438 

9 0.823 26.25 21.604 25.354 

10 0.882 ; 26.25 23.153 26.903 

11 0.933 26.25 24.491 28.241 

12 0.979 26.25 25.699 29.449 

All measurements were verified in the ·field. 

Two Available Ports with 12 Traverse Points per Port 

Expecting 3 to 4 hour runs 

SAMPLE EACH POINT FOR 6 

READINGS EVERY· 6 

AREA OF STACK: 3.7583 ft.l\2 

REACTOR#1 or #2-M1 

Diameters 

2.3 

8.8 

. 4 2/8 

54/8 

6 7/8 

8 3/8 

10 3/8 

13 1/8 

20 5/8· 

23 4/8 

25 3/8 

26 7/8 

28 2/8 

29 4/8 

Minutes 

Minutes 

I 

I 

I 

I 

~ 

I 

I 

I 
C)· 

l_) 

Meter Box Post Test Calibration Check 

ALCOA- WARRICK OPERATIONS 

NEWBURGH, IN 

. A-446 REACTOR # 1 (Three Stacks) 

... 

Meter Box#: M-12 

----

Calibrated by: 

5-Pt Cal Date: 

Richey Lowe 

10/12/2011 

Delta H @ ---=-1::-:.9,_,.4..,..6 

Gamma, initial 0.9934 

Calculate Y qa for each test run using the folloviing equation: 

where: 

Yqa 

q 

Vm 

Tm 

Pb 

0.0319 

DHavg 

DH@ 

Md 

29 

13.6 

dry gas meter calibration check value, dimensionless. 

to tal run time, min. 

total sample volume measured by dry gas meter, dcf. 

· absolute average dry gas meter temp., 0

R. 

barometric pressure, in. Hg. 

= (29.92/528)(0.75)2 (in. Hg/0

/R) cfm2. 

average orifice meter differential, in. H20. 

orifice meter calibration coefficient, in. H20. 

dry molecular weight of stack gas, lb/lb-mole. 

dry molecular weight of air, Ib/lb-mole. 

specific gravity of mercury. 

After each test run series, do the following: 

Average the three or more Yqa's obtained from the test run series and 

compare this average with the dry gas meter calibration factor, Y. 

The average Yqa must be within 5 percent of Y. 

If the average Y qa does not meet the +5 percent criterion, recalibrate the 

meter over the full range of orifice settings, as detailed in Section 5.3 .1 of 

Method 5. Then follow the procedure in Section 5:3.3 of Method 5. 

Test I Test 2 

time. •' 144 144 

Vm- total 101.619 106.257 

Tmavg 78.1 80.9 

Tm-R 538 541 

Barometric 29.6 29.6 

DHavg 1.514 1.804 

DH@ 1.9460 1.9460 

Md stack gas 29.16 29.12 

MdAir 29.00 29.00 

Meter Box Gamma 0;9934 0.9934 

QAGamma 0.9295 0.9839 

Difference: 6.4% 1.0% 

within 5%? FAIL PASS 

AVERAGE DIFFERENCE 2.8% 

----

Test3 

144 

103.784 

60.7 

521 

29.6 

1.779 

1.9460 

29.10 

29.00 

0.9934 

0.9821 

1.1% 

PASS 

. I 

.. 
) 

I. 

ISOKINETIC FIELD DATA SHEET 

METHOD 1031> 

RAL-IS01.xls 

0TRC 

Date: _/'-'-(~_5:::....__~-'--'-1/--
() 

( j' 

·--

ISOKINETIC FIELD DATA SHEET 

METHOD Page_2 _of_3_ 

·.CT!RC 

:,;· .. 

I 

I 

--- .. - I 

I 

I 

I 

I 

I • I 

. ! 
ISOKINETIC FIELD DATA SHEET 

METHOD 

RAL-IS02.xls 

Page_3_of_3_ t\)TRC 

i ,'i ., 
(J 

ISOKINETIC FIELD DATA SHEET 

METHOD }(JisChecked By: ----:-:::-:---:-t.n'+' . ......)=''--. -=...,..,.--------,--- Date: I{- 5"_.,. ll 

(Projec(£{anager or OA Manager ) 

CTRC i 

I 
ISOKINETIC 

, METHOD 

Checked By: --...,.,;:=;;.<;,0-<~=.,_.....,=-----:---­ (ProJect:}''t;;Q'er or QA Manager ) 

RAI -l~n? vic: 

I 

I 

1-

Date: -~/"--{ -~· )'--".:__/.:__/ __ 
Page_3 _of_3_ 

0 
ISOKINETIC FIEL')f;ATA SHEET 

METHOD 3/S: CTRC 

Date: II-s-It 

RAL-IS01.xls 
()· 

.ISOKINETIC FIELD .DATA SHEET 

METHOD Page_2_of_3_ ().T!RC 
' ' ,, 

.... 

ISOKINETIC FIELD DATA SHEET 

METHOD 

RAL-IS02.xls 

Page_3_of_3 _ 

;I 

.: 

I 

I 
/ J METHOD4· MOISTUREANALYSISDATASHEET 0TRC 

Run Number 

Test Date 

Recovery Date 

Recovered By 

lmpinger 1 Dl Water 

Final Weight, g 

Initial Weight, g 1-

Net weight, g 

lmpinger 2 Dl Water 

Final Weight, g 

Initial Weight, g 

() Net wei 

lmpinger 3 Empty 

Final Weight, g 

initial Weight, g 

Net ht, g 

· lmpinger 4 Silica Gel 

Final Weight, g 

Initial Weight, g 

Net weight, g . 

lmpinger 5 

Final Weight, g ~e 

lnitiaiWeight, g 

Net weight, g 

lmpinger 6 

Final Weight, g 

Checked By: tn __ , __ ,.,.:;2~.M()fl u~nanor\ Date:___,/__,_/_-~']_-_{_{----
METHOD 3 • ORSAT ANALYSIS FIELD DATA (JTRC 

. Run No. 

. Start 

Run 

Time . 

Chk 

i=o ___ _ 

Run No. 

Run 

Time 

Leak Chk 

F 0 

. Run No. 

Run 

Time 

·Leak Chk 

Fo 

Checked By: 

RAI .M::\ XI~ 

Avg 

--3 

;·.· 

Avg 

ALCOA 186567 

WARRICK OPERATIONS 

Avg 

~--~--~------~ 

QC Validation 

Fa= (20.9- %02) I %C02 

Distillate Oil 1.260 - 1.413 

Residual Oil 1.210 - 1.370 

Natural Gas 1.600 - 1.836 

Wood/Bark 1.000-1.130 

Expected Fa Ranges 

. Anthracite/Lignite Coal 1.015 - 1.130 

Bituminous Coal 1.083 - 1.230 

Municipal Solid Waste 1.043- 1.177 

~S Date: __,_,_/1_-s+-,...__,-t+-r __ _ 

(Project ~anager or QA Manager) 
C' 

•LCOA-W~A~R=nl=cK~o=p=e=RA,.!:~~~~~~LlTY NAME 

SAMPLING LOCATION-

,-446 REACTOR #1 IThreo Stacks) 

CITY AND STATE 

IEWBURGH.IN 

STACK DIMENSIONS 

lote Calc is for 3 sta' StnckiO Lenath 

" ENTER IN INCHES 26.25 

RUN SPECIFICS DATA 

Runt Run2 

EST DATE 10/2412011 1012412011 

·EsrnMes 1030-1324 1430-1725 

'EST DURATION 144 144 

'EST RUN ID'$ M315-BH1t1-1 M315-9Hfl.1·2 

NOZZLE INSIDE DIAMETER 

G-4-144 Ruu I Run2 

JOZZLE DIAMETER 0.216 0.216 

DRY GAS METER DATA 

M-10 Run I Rnn3 

Aeterbox# M-10 M-10 

JGM Gamma (Y) 0.9912 0.9912 

lGMDeltafH) 1.815 1.915 

VOLUME METERED 

l\h:lerRendin!!'l Run I R11n2 

tunS1nrt 131.440 217.290 

t\mllirl 216.641 306.089 

..e.1k Check I Stnn 0.000 0.000 

. e.1k Check l EOO. o.nno 0.000 

..cnkChcck2Start 0.000 O.ooo 

.cnkChcck:!f:n:J 0.000 0.000 

Volume Metered. 85.201 88.809 

OK 

PRESSURE DATA 

Run! Run:! 

3aromelric Pressure 29.60 29.60 

3tatlc PressU're ·0.22 

MOLECULAR WEJGIIT DATA 

Runt RlDI1 

:lXVQen 17.0 17.7 

:arbon Oio>dde 3.0 2.6 

MOISTURE DATA 

Runt Runl 

3rams/mls Collected 199.8 159.5 

Width 

Ruu 

10/24/2011 

1935-2144 

144 

M315-BH#1-3 

Run3 

0.214 

Run 

M-10 

0.9912 

1.815 

Run 

306.430 

392.187 

o.noo 

o.oon 

o.ooo 

0.000 

85.757 

OK 

"'"' 17.0 

2.6 

Run 

188.9 

POLYCYCLIC ORGANIC l\IATITERCPOM) 

I RunlD.02931 :;rnms Collected Run:! 0.02191 Rm• 0.0273 

TOTAL FLUORIDES LAB DATA 

Rnnl Rnn2 R•m 

\olitllornms Conected IN/A N/A N/A 

I R1m I j R1!!!1__j Rlut / 

K- Facio• ( I j 

2 

I 

. . /--'-\··· 

. DornEnl~) 

·,;._,,· 

NUMBER OF TRAVERSE POINTS= l72j 12j nl 

DELTA P ----

RUN III RUNHl 'RUNII3 RUN/II 

I 0.47 0.(,8G I 0.41 0.(>40 I ·~· 0.762 I 0.89 2 0~2 0.721 2 052 0.721 2 058 0.761 ' 0.98 J 056 0.748 J 0.45 0.671 ' 0.72 O.lW9 J t.on 4 0.72 0.849 4 050 0.707 4 0,78 0.8SJ 4 138 

5 0.65 0.806 5 052 0.711 5 0.85 0.922 5 1.25 

6 0.79 0.889 6 0.78 0,883 6 0.80 0.894 ' 1.49 7 0.81 0.900 7 ·0.78 0.88) 7 0.78 O.RRJ 7 !53 

• 0.64 0.800 R 0.70 0.837 • 0.69 0,8.11 R 1.25 9 0~9 0.768 9 0..42 0.648 9 0.40 0.632 9 1.10 

10 032 0.566 10 0.48 0.69) 10 0.40 0.632 10 0.60 

II 0.40 O,Ci;\2 II 0.42 0.648 II 035 0.592 II 0.78 

" 036 0.600 " 0.40 0.6.12 12 030 0.548 " 058 13 0.60 0.175 " 0.63 0.794 13 0.61: 0,787 13 1.20 " 0.65 0.806 14 0.72 0.849 " 0.75 0.8(11i 14 1.25 IS 0~6 n.~t2 IS 0.85 0.922 IS 0.85 0.922 IS 1.25 

16 D;74 0.860 16 us 0.9.22 16 0.88 0.938 16 1.40 

11 0.81 0.9011 17 0~1 0.900 17 0.91 . 0.954 17 153 

18 0.83 0.911 IR 0.70 0.8J7 18 0.87 0.9)) IR 1.60 

: 19 0.84 (1,9\7 19 052 0.721 19 0.76 0.872 19 1.60 

20 f!.6& 0.812 .20 0.40 0.6.12 20 0.60 0.715 20 1.26 

" o ..... 0.663 " 0.40 ll.liJ2 " 0.48 0.693 " ·~I " 033 0.574 22 0.45 0.671 22 0.41 0.640 22 0.60 2.1 033 0.574 2.1. 0.41 0.640 2.1 037 0.608 2:\ O.fiO 

24 0.30 0.548 ,. 032 o.sr.r. 24 0.38 0.616 24 058 

" 0.47 o.6sr; " 0.61 0.781 " 0.48 0.693 " O.fl9 26 0.47 0.681i 26 058 0.762 2!i 0.62 0.787 2 26 0.89 

27 058 0.7!i2 " 0.78 0.883 27 0.78 0.883 27 I.JO '" 0.60 0.775 28 0~5 0.922 " 0,90 .0.949 '" uo 29 O.fiO 0.775 29 o~s 0.922 29 0.85 0.922 " 1.20 JO 0.83 0.911 30 0~5 0.912 30 0.88 0.938 JO 1.60 

31 0.72 0,849 31 0.8! 0.900 31 0~5 0.922 31 132 

32 050 0.707 J2 0.78 0.8Rl 32 0.78 0.8113 32 035 

33 050 0.707 33 0.46 fl.!i78 33' 0.75 0.866 33 0.95 .34 ·0.48 ll.fi9J'• J4 033 0.574 . . 14· . o.fit 0.781 " 0.92 )5 031 0.5116 JS 0.33 0574 )5 0~7 . 0.608 35 0.60 

36 0.29 0.539 36 035 . 0.592 J6 035 0.592 36 055 

37 0.48 0.69) )7 0.7 0.8)7 37 0.43 0.656 J7 0.92 

JS 050 0.707 38 0.72 0.849' JS O.fi2 0,787 )8 035 

39 0_"6 0.7411 39" 0.85 0.9.!2 39 0.69 0.8)1 )9 1.10 

40 ·~' 0.787 40 0.85 0.922 40 0~5 0.922 40 1.25 •t· 0.64 . 0.800 " 0.72 0.849 " 0.89 0.943 41 uo " 0.75 0.8r.!i 42 0.8 0.1194 42 0.91 0.954 " us 43 0.68 0.825 .43 o.ti8 0.825 41 0.86 0.927 43 130 

44 0.65 0,806 44 0.7 0.837 44 0~3 0.911 44 i.30 

45 0.45 0.671 45 0.7 0.837 45 0.70 0.837 45 0.85 

46 0.45 0,671 ... o.sa 0.762 46 051 0.714 46 0~5 47 0.46 0.678 " 05 0.707 " 050 0.707 " ... , 48 052 0.721 48 05 0.707 4R. 0.41 0.~40 4R 038 

49 0.60. 0.775 49 0,6[ 0.781 .,. 0.4fl . o.r.93 " 1.20 50 o.ss· 0.762 50 0.71 0.843 50 057 0.755 50 J.IS 

5I 0.68 0.825 5I ·0.89 0.943 5I 0.71 0.849 5I 1.30 

52 D.li5 0.806 52 031 0.95<1 52· 0.84 0.917 52 130 

5J 0.84 o9i7" · .,·53 0.95 0.975 53 0.84 0.917 53 1.60 

54 0~2 0,906 54 0.83 0.911 ... 031 0.95<1 54 t.fiO 

ss· 0.60 0.175 55 ·~· 0.900 55 0.87 0.9JJ 55 1.20 sr. 0~0 0,775 56 0.68 0.825 56 0.80 0.894 56 1.20 

57 0.43 0,656 57 0~1 0.787 57 0.75 0.866 51 0.85 

5R 0,46 0:,678 .... 58 05 0.707 .58 0.85 0.922 5R ~.as S9 0.50 0,707 S9 0.41 0.(>40 S9 O~l 0,906 3 S9 035 

, .. "·"' 11.632 , .. 035 0.592 G<i 056 0.748 GO 0.76 61 054 0.735 61 059 0.7!i8 61 0.46 0.678 61 1.00 

62 057 O.iSS .62 0.73 0.854 62 0.46 0.678 62 1.05 

(,1 0~3 0.794 "' 0.75 0JIIi6 "' 056 0.748 6) 1.25 64 0.63 0.794 64 0~5 0.922 (~ 0.65 0.806 (~ 1.25 

65 0.12 0.849 65 0.83 0.911 65 0.70 o.s.n 65 1.32 

66 0.75 0,8GG 66 0.91 0.954 66 0.82 0.906 66 135 

67 0.83 0.911 67 o.ss 0.922 67 0.72 0.849 67 1.60 

.. 0.65 o:so6 68 0.7 OJU7 68 n.Gs 0.806 68 1.25 

'" 0.70 0.837 69 052 0.721 " 05Z 0.721 69 138 70 0.70 0.8J7 70 o.s 0.707 70 0.4Z 0.648 70 1.3R 

71 0.43 O.GSii 71 0.41 0.640 71 OJ6 Cl.600 71 0.86 

12 0.43 0.6Sii 12 0.35 0.592 72 0.30 0.548 12 0.86 

7) 0.000 7) 0.000 73 0.000 7) 

74 0.000 74 0.000 74 0.000 74 

75 0.(1{10 75 0.000 15 o.ono 75. 

76 o.ono 76 11.000 76 0,000 76 

77 0.000 77 0.000 77 0.1100 77 

78 0.000 78 0.000 78 0.000 78 

79 11.000 79 0.000 79 0.000 79 

80 0.000 80 0.000 '" 0.000 80 

54.450 56.662 57,(125 c:JJI AvgSq11 

~ L..l!:Z!l.!!. ~ 

D ELTA ....... n.u FLUE GAS TEMP 

RUN/12 RUN#3 ' RUN/II RONII2 RUNfl3 

I 0.77 I t.n5 1 169 I 170 I 172 

2 us 2 I. OS ., l7l 2 In 2 In 

J 0.80 J 1.28 ' 171. J 172 ' 173 

4 0.95 4• 135 4 171 4 172 4 173 

5 1.00 5 !53 5 172 5 172 5 173 

·6 1.47 6 ,15 6 172 ' 172 ' 173 

7 1.47 7 135 7 172 7 171 7 173 

R 1.40 8 1.25 R m R 173 .R 173" 

9 0.80 9 0.72 9 171 9 173 9- 113 

10 0~5 10 0.72 10 "' 10 173 10 173 

II 0~0 II 0.62 II 166 II 174 II 't73 

" 0.78 " 0.6 12 164 " 171 " -·173 

" 1.19 13 1.1 13 172 13 175 IJ 172 

14 1.36 14 13 14 m 14 175 " 173 

IS 1.60 IS 1.6 IS 173 .IS 173 IS m 

16 1.60 16 ..• 16 173 16 173 16 173 

11 1.60 17 1.61 17 173 11 173 11 173 

18 1.40 IR 1.6 '18 113 18 173. 18 173 

19 t.oo 19 13 19 172 19 173 19 . 173" 

20 0~0 20 1.06 20 172 20 173 20 172 

" 0.78 21 0.85 " 171 21 171 " ·173 

" 

0.90 " 0.73 '22 164 22 172 " l7l 

2.1 0.80 23 0.65 2.1 164 2.1 171 2.i •170 

,. o~o 24 0.65 24 160 24 172 24. 'i6B 

" 1.18 " 0~5 .2S 11S 25 174 25 179 

21i 1.15 26 1.1 2 26 176 . :!G 175 26 179 

27 135 27 13R " 177 27 178 27 179 

,. 

28 uo 2B 159 28 17R 28 178 28 179 

L60 " 155 ,. 178 29 178 29 178 

30 l.fiO JO 159 JO 179 JO 178 30 179 

31 1~0 31 I.SS 31 177 " 177 " ·179 

32 1.35 n 15 ·)2 177 )2 177 32 179 

33 us 33 1.48 33 176 3) 111 33 179 

" 0.60 34 1.1 " 176 )4 nii J4 t79 

35. 0~0 .35 0.65 J5 112 35 176 JS 179 

36 0~0 36 · ~ o.6s -~6 172 36 175 )6 175. 

37 1.30 ')7 0.83 J7 176 37 174 "37. 180 

JS 1.35 38 i.J JR 175 J8 174 .18 179- 

39 1.60 39 1.23 39 178. J9 174 )9 179. 

40 MD 40 155 40 178 40 174 40 179 

" us 41 1.6 41 178 41 174 41 179 

42 155 42 1.6 42 17R 42 175 42 179 ~ 

43 130 43 155 . ., 117 43 175 43 179 

44 130 44 15 44 117 44 175 44 ISO· 

45 130 45 _1.24 45 176 1> 113 45 180. 

46 036 46 0.9 46 175 4(,_ ·173 ·46 180 

" 0.95 " ·o3 47 175 4i '" " 179 

4R 035 48 ri:fi8 '" 176 48 166 ·48 17~ 

49 1.18 49 0.85 49 174 49 170 .. 174 

50 135 so t.o8 50 174 50 170 50. 176 

51 1.65 5I 1.25· 5I 176 51 171 5I 176 

52 1.68 ·52 1.55 . 51 176 52 170 52 176 

5J t:70 SJ 155 5J 175 5J 170 ·SJ 176 

54 . uo .54 1.6 54 175 54. 170 54 175 

55 1.60 55 155 55 172 55 170 55 175 

56 130 56 1.4 56 172 ·SG. 170 56 176 

57 1.:20 57 1.25. 57 171" ·st 168 57 175 

58 0.95 5R 15 58 170 ·,58 168 58 174 

S9 uo S9 1.45 3 S9 170 S9 "" S9 174 

r.n 0.60 GO 0.99 , .. 170 60 "' 60 112 

61 1.07 61 0.81 61 '172 61 '" 61 178 

62 1.33 62 0.85 62 113 62" l7l 62 178 

6) us 6) 0.99 6) 173 ~1 171 6) • 178 

64 155 64 1.15 64 113 64. 171 64 180 

65 155 65 1.25 65 173 65 170 65 180 

66 1.60 66 1.45 (,6 173 lili 171 66 180 

67 1.55 67 1.25 67 113 67 1;1 67 180 

68 1~0 68 1.15· 68 174 68 17t" 68 179 

69 1.00 69 032 " 174 69 l7l 69 179 

70 1,00 70 0.74 70 "i70 70 '" 70 177 

71 0.75 71 0.65 71 172 71 '" 71 173· 

12 0.63 72 '0.53· 71 172 ·72 168 12 173 

7) 13 7) 7) 13 

74 74 74 74 74 

75 75 75 15 75 

76 76 76 76 76 

77 11 .11 17 11 

78 78 78 78 78 

79 79 79 " 79 

80 80 80 80 80 

L____ld2. L.___ill L...ill.2. ~ L...!m 
Meter Box Post Test Calibt·ation Check 

ALCOA- WARRICK OPERATIONS 

NEWBURGH, IN 

. A-446 REACTOR # 1 (Three Stacks) 

Meter Box#: M-10 • 

· Calibrated by: 

5-Pt CalDate: · 

Greg Byrd 

6/6/2011 

Delta H ®_--,..:1:,:.:.8o-::17

5 

. Gamma, initia1_--"0-'-'.9....:.9....:.12:o:... 

Calculate Yqa for each testrun using the following equation: 

where: 

. .Yqa 

q 

Vm 

. Tm 

Pb 

0.0319 

DHavg 

. DH@ 

Md 

29 

13.6 

. __ = ~ _ 0.0319 Tm 29 (-JMi) 

Yqa H al'g 

Vm1/ b. H (P + il·~-) M d 

v @ b 13.6 

dry gas meter calibration check value, dimensionless. · 

.totalrun time, min. 

· total sample volume measured by dry gas meter, dcf. 

absolute average dry gas meter temp., 0

R . 

barometric pressure, in. Hg. 

= (29.92/528)(0.75)2 (in. Hg/0

/R) cfm2. 

average orifice meter differential, in. H20. 

orifice meter calibration coefficient, in. H20 . 

dry molecular weight of stack gas, lb/lb-mo1e. 

dry molecular weight of air, lb/lb-mole. 

specific gravity of mercury. 

After each test run series, do the following: 

Average the three or more Yqa's obtained from the test run series and 

compare this average. with the dry gas meter calibration factor, Y. 

The average Yqa must be within 5 percerit of Y. 

If the average Yqa does not meet the +5 percent criterion, recalibrate the 

meter over the full range of orifice settings, as detailed in Section 5.3 .1 of 

Method 5. Then follow the procedure in Section 5.3.3 of Method 5. 

.. Test 1 Test2 

time 144 144 

Vm ~total 85.201 88.809 

Tm avg 73.4 80.4 

Tm-R 533 540 

Barometric ... 29.6 29.6 

DHavg 1.115 1.187 

DH@. 1.8150 1.8150 

Md stack gas 29.16 29.12 

MdAir 29.00 29.00 

Meter Box Gamma 0.9912 0.9912 

QAGamma 0.9904 0.9852 

Difference: 0.1% 0.6% 

within 5%? PASS PASS 

AVERAGE DIFFERENCE 0.3% 

Test 3 

144 

85.757 

57.3 

517 

29.6 

1.174 

1.8150 

29.10 

29.00 

0.9912 

0.9929 

0.2% 

PASS 
() 

( ·. ,'-._) 

COMPANY NAME: 

METHOD 1 WORKSHEET 

Summary of Location Setup 

Enter Information Below: 

ALCOA- WARRICK OPERATIONS 

FACILITY LOCATION (City, State) Newburgh, IN 

SAMPLING LOCATION: A-446 REACTOR# 3 Stack 

Circumference 

·Far Wall to Outside of Port 56.5 

Inside Wall to Outside of Port .10.5 

DIAMETER OF STACK 46 

. DIAMETER OF, STACK 3.83 

·Nearest Upstream Disturbance 92.5 

· Nearest Dowstream Disturbance 192 

Nearest Upstream Disturbance 2.0 

Nearest Dowstream Disturbance 4.2 

USE 12 TRAVERSE POINTS PER PORT 

rnches 

Inches 

Inches 

Inches. 

Feet 

Inches 

Inches 

Diameters· 

Diameters 

TOTAL TRAVERSE POINTS 

EXPECTED RUN DURATION 

TIME PER TRAVERSE POINT 

24 

144 

6 

6 

24 

.24 pt X 3 Stacks 

minutes 

READINGS EVERY 

EXPECTED READINGS 

,.-' 

minutes 

minutes 
METHOD 1 

TRAVERSE POINTS 

ALCOA· WARRICK OPERATIONS 

NewburQ,h, IN 

:A-446REACTOR # 3 Stack 

Far Wall to Outside of Port 56.5 

Inside Wall to Outside of Port 10.5 

DIAMETER OF STACK . 46 

Nearest Upstream Disturbance 92.5 

Nearest Dowstream Disturbance 192 

NUMBER of Traverse Points per Port 12 

POINT %of Depth Diameter Distance Distance 

from Inside w/ Nipple -

1 0.021 46 0.966 11.466 

2 0.067 46 3.082 13.582 

3 0.118 46 5.428 15.928 

4 . 0.177 46 8.142 18.642 

5 0.25 46 11.500 22.000 

6 0.356 46 16.376 26.876 

7 0.644 46 29.624 40.124 

8 0.75 46 34.500 45.000 

9 0.823 46 37.858 48.358 

10 0.882 46 40.572 51.072 

11 0.933 46 42.918 53.418 

12 0.979 46 45.034 55.534 

All measurements were verified in the field. 

Inches 

Inches 

Inches 

Inches 

Inches 

Two Available Ports with 12 Traverse Points per Port 

Expecting 3 to 4 hour runs 

SAMPLE EACH POINT FOR 6 

READINGS EVERY 6 

AREA OF STACK: 11.5410 ftA2 

REACTOR#3-M1 

Diameters 

2.0 

4.2 

11 4/8 

13 5/8 

15 7/8 

18 5/8 

22 

26 7/8 

40 1/8 

45 

48 3/8 

51 1/8 

53 3/8 

55 4/8 

Minutes 

Minutes 
(]··~ 

--

u 

METHOD 1- TRAVERSE POINT LOCATIONS CTRC 

3 

4 

5 

.6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

Note: When using 4 ports in a circular duct, the probe is marked 

with on I the points for the first half of the full diameter traverse. 

r 

Test Port 

. If more than 8 and 2 'diameters. and If duct 

diameter is less than.24", use 8 or 9 points . . . ~ 

-! 

'· :DIAMETERS 

Velocity UP DOWN Particulate 

24 or 25 

2 0.5 ~-~---...J · Disturbance 

DRAW HORIZONTAL LINES THROUGH UPSTREAM AND-DOWNSTREAM 

DIAMETERS AND USE THE HIGHER NUMBER OF POINTS •. 

Equivalent Diameter (for rectangular ducts): 

De= 2 *Depth *Width I (Depth+ Width) 

De = 2 * ( ) ~ ) I ( ) + ( ) = I 

LOCATION OF POINTS IN CIRCULAR STACKS OR DUCTS 

(Fraction of st~!ameter from inside wall to traverse point) 

2 4 ""!!"' 8 10 \,12_) 14 16 18 20 

1 .146 .067 .044 .032 .026 .021 .018 .016 .014 .013 

2 .854 .250 .146 .1 05 .082 .067 .057 .049 .044 .039 

3 .750 .296 .194 .146 .118 .099 .085 .075 .067 

4 .933 .704 .323 .226 .177 .146 .125 .109 .097 

5 .854 .677 .342 .250 .201 .169 .146 .129 

6 .956 .806 .658 .356 .269 .220 .188 .. 165 

7 .895 .774 .644 .366 .283 .236 .204 

8 .968 .854 . 750 .634 .375 .296 .250 

9 .918 .823 .731 .625 .~82 .306 

10 .974 .882 .799 .717 .618 .388 

11 .933 .854 .780 .704 .612 

12 .979 .991 .831 .. 764 .694 

13 --- .943 .. 875 .. 812 .750 

14 For 22 or 24 test points, ·.982 .915 .. 854 . 796 

15 .951 .891 .835 

16 see Method 1 table in .984 .925 .871 

17 CFR .956 .903' 

18 .986 .933 

19 .961 

20 . :: .. 987 

LOCATION OF POINTS IN RECTANGULAR STACKS ORDUCTS ( 

(F rae r 10 n of stack diam e r te f ro m ·ns·d I 1 ewa II t t o rave rse point) 

2 3 4 5 6 7 8 9. .10 11 12 

1 .250 .167 .125 .100 .083 .071 .063 .056 .050 .045 .042 

2 .750 .500 .375 .300 .250 .214 .188 .167 .150 .136 .125 

3 .833 .625 .500 .417 .357 .313 .278 .250 .227 .208 

4 .875 .700 .583 .500 .438 .389 .350 .318 .292 

5 .900 . 750 .643 .563 .. 500 .450 .409 .375 

6 .917 .786 .688 .611 .550 .500 .458 

7 .929 .813 .722 .650 .591 .542 

8 .938 .833 .750 .682 .625 

9 .944 .850 .773 .708 

10 .950 .864 . 792 

11 .955 .875 

12 .958 

I 

I 

I 
~· ... 

..... ~·. 

TEST LOCATION SCHEMATIC DIAGRAMS 

1 . Make a separate drawing for each Method 1 Sheet 

2. Show distances to upstream and downstream disturbances. Show or note what the disturbances are. 

3. All ports must be shown and labeled. Note which ports were used and for what type of testing. 

4. Indicate the number of points per port and the total points that were sampled 

.5. Be sure to indicate the air flow direction. 

Plant 

"' 

Test Location ~~~~----~-

. k 4 t{ G Date . I o/z 'fIll Initials Ao ' I 

CROSS SECTION 

DIMENSIONS 

EXAMPLE 62"Dinmolor1V: .. ~r· 8· 40 .. -JI 12• 0 \1 ~ 

. ..._ .... ~ .. ~ .. : ... A fm+·++.. : 

: . 1oo ""!"'T"T"" c 

"T"T"j'"' _o 

1 From i' 

Jl Boohouso -

. TRAVERSE POINTS 

4 Ports 

Indicate View (top, side, etc.} 

4 Points per Port 

16 polnls Tolal 

03" 

_L 

TolD Fen 
· . ........ / 

CJ 

CYCLONIC FLOWDETERMINATION DATA SHEET 

(WITH PRELIMIN~RY VELOCITY AND MOISTURE) . . 

CTRC 

'----"'"'-· -----------"-----' Gas·Parameters 

Balance No. ___ _ · Total Catch ...._ _____ ... 

Fyrite Orsat GEM Meter Pre Post 

02% in. Hg 

C02% cfm 

Pitot 

Delta P avg is square of the average of the individual square roots 

Location is acceptable if avg of ABS(Yaw) ~ 20° 

Checked By: ,., __ , __ , .. ___ ,g_,~- "'' "------, 

/ 

Date: _--....J(u...j-_")_-"'-1 \,___ 

'.· 
(~' 

~· 

LCOA~-~W~A~R~R~IC~K~O~P"'ERA~;~I~!l;~;!,!~LITY NAME 

-44S"'R~EA"'c=r~o~R~#~

~IO"nS"' 0 A~St;,!.'.t:!;'~'!.!l I""NG LOCATION 

EWBURGH. IN CITY AND STATE ==:::1 

STACK DIMENSIONS 

· ENTER IN INCHES I St::lck ID 461 lenath I Width I 

EST DATE 

EST TIMES 

EST DURATION 

EST RUN ID'S 

7F·1 

IOZZLE DIAMETER 

IYJ 

Mt:terRcftd[ne, 

:tatStnrt ~tnt Eni 

.cak Check I S1o1r1 

.cnk Check 1 Etxl 

.en k Clu~ck 1 S1art 

.cnkChcck:?Etd 

~ 

larametrlc Pr~ure 

31atic Pressure 

)xvaen 

;arbon Dlo)lide 

RUN SPECIFICS DATA 

Runt Run2 

10/24/2011 10124/2011 

.. 

1030-1259 1430 -1725 

144 144 

M13A-1 M13A-2 

NOZZLE INSIDE DIAMETER 

I Ru~:~l0.2471 Runl 0.247 

DRY GAS ?o.IETER DATA 

Runl 

M1 

0.9965 

1.713 

VOLUME METERED 

0.000 

n.ooo 

0,000 

0.000 

'ffi:7o7 

OK 

Run3 

M1 

0.9965 

1.713 

Rnn2 

919.400 

1044.176 

0.000 

0.000 

0.000 

....!!&QQ. 

124.776 

PRESSURE DATA 

~ 

Rtntl 

-0.31 

Run2 

----=-29.60 

-<>.30 

MOLECULAR WEIGHT DATA 

Rtml RID12 

18.6 17.3 

1.7 2.6 

MOISTURE DATA 

Run 

10/24/2011 

1935·2226 

144 

M13A..J 

Run3 

0.24.7 

Run 

M1 

0.9965 

1.713 

Run 

CITE(K 

44.78fl 

160.719 

0.000 

0.0110 

0.000 

0.000 

115.939 

Rtm 

-----zg:eo 

-0.32 

R•m 

18.1 

2.4 

3ramslmlsCollecled I Rn1lll93.91 Ru1l 2 zso.zl Ru1l 258.61 

FILTERABLE PARTICULATE DATA 

Rtml Run2 RtDl 

3rams Collected 0.0000 o.onno 0.0000 

TOTAL FLUORIDES LAB DATA 

Rtml Run:! Rtm 

WlliQrams Colleclcd 0.34 0.21 0.30 

I "'·- 1 I ~h!!!..L____I_ Run I K-Faclo, I ..... I I ~ 

' 

,,....-·-........ 

. i \ 

DataEnt~ 

. ·NUMBER OF TRAVERSE POINTS : I >4 I ,. I ,.I 

..................... DELTAP 

RUNHI RVNIIZ RUN//3 

I 0.34 0.583 I 0.38 0.616 I 0.46 0.678 I 

2 0.43 0.(,56 2 0.50 0.707 2 o.so 0.707 ., 

J 0.49 0.700 J o.so 0.707 3 0.54 0.735 3 

4 0.57 0.755 4 0.56 0.748 ' 0.66 0.812 4 5 0.73 0.854 5 0.64 0.800 5 0.74 0.8(10 5 

6 0.75 0.866 6 0.72 0.849 6 0~4 0.917 6 

7 uo O.fl94 7 us 0.922 7 0.89 0.943 7 

• 0.76 0,872 • 0~0 0.894 • 0.80 0.894 8 9 0.61 0.781 9 0.70 o.a:n 9 0.63 0.794 

10 0.66 0.812 10 . 0,60 0.775 10 0.63 0.794 10 ' 

II 0.57 0.755 II 0.57 0.755 II 0.57 0.75!i II 

12 0.54 0.735 " 0.53 0.728 12 0.55 0.742 12 13 .0.38 0.616 13 . 0.41 O.ft48 13 0,40 o:6~2 13 

14 0.43 0.656 14 0.42 O.f..tR 14 0.47 .O.GRii 14 

IS 0.60 0.775 15 051 0.714 IS 0.61 0.781 IS 

16 0.61 0.781 " 0.62 0.787 " 0.63 0.794 16 17 0.70 0.837 17 0.73 0.854 17 0.68 0.825 17 

·18 0~4 0.917 ... 0~6 0.927 '" 0~5 0.921 18 19 0 ... 0.943 19 0~6 0.927 19 0~0 0.894 19 

20 0~78 0.883 20 0~3 0.911 20 0.7R . 0.883 

21 0.62 0.787 21' 0.73 0,854 21 0.61 0.781 '" 21 

" 0~60 '0.775 :u ~66 0.812 " 0.60 0.775 " ~· 0.54 0.735 23 0.63 0.794 23 0.56 0,748 24 0.54 0.735 24 058 0.762 24 053 0.729 ~· 24 

25 0.000 2S 0.000 2S 0.000 2S 

26 0.000 26 0,000 26 0.000 2 26 

27 0.\'100 27 0.01'10 27 0,000 27 

28 0.000 28 0.000 28 0,000 2R 

29 .. 0.000 29 0.000 29 0.000 29 

30 0.000 )0 0,000 30 0,000 30 

31 0.000 31 0.000 31 0.000 31 

32 o.ooo. '32" 0.000 n 0.000 32 

• 33 0.000 33 0,000 .-J,l 0.000 .1;1 

34 0.000 .34 0,0\'10 34 0.000 34 

35 0.000 35 ·0.000 3S 0.000 3S 

36 0.000. 36 0.000 ·36 0.000 36 

37 0.000 :31 ·o.ooo. 37.· 0.000 37 

'" 0.000 38 .' 0.000 38 0.000 38 39 0.000 . 39 0.000 39 0.000 39 

. 40 ,0,000 ·'" 0.000 40 0.000 40 41 0.000 41 0.000 41 . o.ouo 41 

42 0.000 42 0.000 42 0.000 42 ~) 0.000 4) 0.000 4) 0.000 4) 

.. .0.000 .. O.ooo 44 0.000 ,44 

45 0.000 45 0.000 45. o.ooo. 45 

46 0.000 46 0.000 46 0.000 46 

47' 0,000 47 0.000 47 0.000 47 

48 0.000 4R 0.000 48 . 0.000 48 

49 0.000 . 49" 0.000 49 0.000 49 

50 0,000 50 0.000 sn 0.000 so 

51 0.000 5I 0.000 51 0.000 5I 

52 o.ooo- 52 0.000 52 . 0.000 52 

53 0.000 ·5J fl.ODO 53 . 0.000 53 

54 ·o.ooo 54 0.000 54 0.000 54 

55 ·o.ooo 55 0.000 55 0.000 55 

56 0.000 56 0.000 56 0.000 56 

57 0.000 57 0.000 57 ' 0.000 57 

58 0,000 ·58 0.000 '58 0.000 58 

59 0.000 59 0,0011 59 0.000 3 59 

(,0 0.000 60 0.000 60 0,000 60 

61 0.000 61 0.000 61 0.000 61 

62 . 0,000 "62 0.000 62 0,000 62 

63 o.uoo 63 0.000 63 0.0011 63 

(>4 0,000 (>4 0.000 (o4 0.000 64 

65 0.000 65 0.000 liS· 0.000 65 

66 o.noo 66 0.000 66 0.000 66 

67 0.000 G7 0.000 67 0.000 67 

68 0.000 '" 0.000 68 0.000 •• ri.ooo 69 0.0(10 69 0,0110 '" 69 

70 o.ooo 70 0,000 70 0.000 70 

71 0,000 71 0.000 71 0.000 71 

n 0.000 7' 0.000 n OJ)()() 72 

73 0.00{} 73 0.000 73 0.000 73 

74 0.000 74 0.000 74 0.000 . 74 

75 0.000 75 0.000 75 Q.OOO 75 

76 o.ooo 76 0,000 76 0.000 76 

77 0.000 77 0,000 77 0.000 77 

78 0.000 '78 0.000 78 0.000 78 

i9 - 0.000 79 0.000 79 0.000 79 

80 o.ono 80 0,000 80 0.0110 80 

18.70J 1R.978 19.080 

Al:gSqrt LQ.lliL L.!1ll!!!! 

~ 

ltt.'\Cf'OI\•Jo~U>,\.~1• 

..,a:....,an.n ' 

RUNHl RUNIIZ RUNif3 RUNI#1 RUN liZ RUNII3 

1.35 I I .SO I ·~· I 171 I "' I 171 

1.70 2 2~0 2 2 ., m 2 171 2 "171 

1.95 3 l.OO 3 2.15 3 m· 3 171 3 m 

2.30 4 2.25 4 1.65 4 173 4 ·17Z 4 172 

2~0 5 255 5 2.05 5 174 5 173·. 5.· 172 

~no 6 2.90 6 2.35 6 174 ' 173 6 . 173 

3.20 7 3.40 7 '2.5 7 173 7 173 7 ·~. 

til 

3.05 8. 3.20 • 2.25 8 173 a·.·. 173 .. 172 

2.45 9 2.80 9 '1.75 9 171 9 173 9 171 

2.65 10 2.40 10 1.15 10 171 IO 172 10 171 

2.30 II 230 II 1.6. u 170 II 1.73 · II 170 

1.15 12 1.10 12 :t.ss 12 170 12 .111 12 170 

I .SO 13 1.70 13 1.6 13 170 13 171 13. 168 

1.70 14 1.70 14 1.85 14 170 ·14 111 14 '169 

2.40 15 2.05 IS 2,45 IS 171 IS:· 172 15 170 

2.45 16 2.50 16 2.5 " 172 16 172 16 171 

z~o 17 2.110 " 2.7 17 173 17 172 17 172 

335 18 3.45 18 3.4 '" 173 18 172 18' 171 

3.55 19 3.45 19 3.2 19 173 19 171 19 .t~ .. 

3.10 20 3.30 20 3.1 20 173 2CI 171 20 173 

2.50 21 2.110 21 :z;45 21 i73 21 170 21 l7Z 

2.40 22 2.65 22 2,4 22 173 22 "' 22 172. 

2.15 ~· 2.50 23 2.25 23 173 .?J 168 :z.i 172 

2.15 24 230 24 2.1 24 172 24 168 24 170 

25 2S 25 25 2S 

26 26 2 26 26 26 

27 27 27 27 27 

28 28 28 '28 '28 

29 29 29 " 29 

30 30 30 30 30 

31 31 Jl. 31 31 

32 32 32 32 32 

33 33 33 33 33 

34 34 34 34 34 

35 35 · .. . : 35 35 35 

36 )li 36 36 36 

37 37 )7 37 37'' 

38 '" )8 )8 '" 

39 39 ,. 39 39 : 

40 40 40 40 40 

41 41 41 41 41 

4~· 42 42 42 42 

43 43 .· I 43 43 43 

" 44. 44 44, .. , 

45 45: .. ·' 45 45. 45 

46 46 • 46 '461 46 

47 47 . -~ .. 47 47 47 

48 48. 48 48 48. 

49 49 

-:~9 

49 49 :·. 

sn 50 50 so 50 

51 5I 51 5I 5.1 

'52 52 52 52 52 

5) 53 53 53 53 

54 54 54 54 54 

55 55 55 55 5S 

56 56 '56 .56 56 

57 57 57 57 57 

58 58 58 ·sa 58 

S9 59 3 59 59 59 

60 60 611 GO (,0 

61 61 61 61 61 

., ., ., ., ., 

63 63 63 63 63 

64 64 64 (o4 64 

65 65 ., 65 65 

66 66 66 66 (,0 

G7 G7 G7 67 67 

'" 68 6R 68 68 

.. 69 .. 69 69 

70 70 70 70 70 

71 71 71 71 71 

72 n n n 72 

73 73 73 73 73 

74 74 74 74'· 74 

75 75 75 75 75 

76 ! 76 76 76 76 

77 77 77 77 77 

78 78 78 78 78 

79 79 .79 79 79 

.. 80 80 811 80 

DEL TAB FLUE GAS TE~tr 

~ L....,lJL L....bti l.._11b! L.Jill. L..__!11l 
. ' ' 

Meter Box Post Test Calibration Check 

ALCOA- WARRICK OPERATIONS 

NEWBURGH, IN 

A-446 REACTOR# 3 (One Stack) 

Meter Box#; ..:cM..::.l __ _ 

· Calibrated by: 

5-Pt Cal Date: 

Chris Abbott 

4/15/2011 

Delta H @ ---::-=1=.:::-:. 7::-::17

3 

Gamma, initial 0.9965 ·. 

Calculate Yqa for each test run using the following equation: 

where: 

Yqa 

q 

Vm 

Tm 

Pb 

0.0319 

DHavg 

DH@ 

Md 

29 

13.6 

dry.gas meter caJibration check value, dimensionless. 

· .~ tot<il run. time, min. 

total sample volume measured by dry gas meter, dcf. 

absolute average dry gas myter temp., 0

R. 

barometric pressure, in. Hg. 

= (29.92/528)(0.75)2 (in. Hg/0

/R) cfm2. 

average orifice meter differential, in. H20. 

orifice meter calibration coefficient, in. H20. 

dry molecular weight of stack gas, lbllb-mole. 

ciry molecular weight of air, lbllb-mole. 

specific gravity of mercury. 

After each testrun series, do the following: 

Average the three or more Y qa's obtained from the test run series and 

compare this average with the dry gas meter calibration factor, Y. 

The average Yqa must be within 5percent ofY. 

If the average Yqa does not meet the +5 percent criterion, recalibrate the 

meter over the full range of orifice settings, as detailed in Section 5.3 .1 of 

Method 5. Then follow the procedure in Section 5.3.3 of Method 5. 

Test 1 Test 2 

time· 144 144 

Vm- total 123.707 124.776 

Tmavg 71.2 72.4 

Tm-R· 531 . 532 

Barometric 29.6 29.6 

DHavg' 2.460 2.533 

DH@· .• 1.7130 1.7130 

Md stack gas 29.02 29.11 

MdAir 29.00 29.00 

Meter Box Gamma 0.9965 0.9965 

QA Gamma 1.0455 1.0412 

Difference: 4.9% 4.5% 

within 5%? PASS PASS 

AVERAGE DIFFERENCE 4.7% 

Test 3 

144 

115.939 

58.7 

. 519 

29.6 

2.269 

1.7130 

~9.11 

29.00 

0.9965 

1.0436 

4.7% 

PASS 

I 

I 
ISOKINETIC FIELD DATA SHEET 

·; METHOD(S} ~t"tt 1/s- Page ____ 1 __ ot__jl__ 

. / -----------------

(j 

_CTRC 

• 

, 
• 

·~ 

ISOKINETIC FIELD DATA SHEET 

METHOD(S) __ 1:::...~1:.:..r _____ _ 

RAL-IS01.xls 

erR.C 

I 

I 

I 

I 

.I 
'\ ' 

ISOKINf:TIC FIELD DATA SHEET 

METH ____ 1~/~r~----~----- Page_1_-_of_l_. C'TRC 

() 
..... , : 

METHOD 4- MOISTURE ANALYSIS DATA SHEET 

lmpirigei" 1 Dl Water · 

· Final Weight, g 

· ·l!iltial Weight, g 

Net weight, g 

lmplnger 2 Dl WatEir 

Final Weight, g 

Initial weight •. g 

Net weight, 

lmpinger 3 Empty 

Final Weight, g 

Initial Weight, g 

Netwe ht, g 

lmpinger 4 Silica Gel 

Final Weight, g 

Initial Weight, g 

Net weight, 

ALCOA 

WARRICK OPERATIONS. 

(JTRC 

lmpinger 5 ____ 1-~--.--......:::~--t--:---:-----r-----;---_.:....-+--------l 

. Final Weight, g 

Initial Weight, g 

Net weight, 

lmpinger 6 __ _ 

Final Weight, g 

Initial Weight, g 

Net weight, 

Filter ID # 

Final Weight, g 

1-----~--+------~-------r-----~~ 

.~ 

Checked By: Q ~ Date: If-£- {I ----(P-ro-je-ct-M-an-ag+~+o~r-QA_M_a-na-g-er) 

CAl f.AAI\J..JI\1 VI C'o 

. ! 

· .• I 

I 

I 
·~ ~. 

(-) 

''----' 

.-

r\ ___ ) 

METHOD 3 • ORSAT ANALYSIS FIELD DATA 

Run 

Time 

Leak Chk 

Fo 

Run No. .M~Jr-2-

Run Time of 

Time 

Leak Chk 

Fo __ _ 

. Run No. ~3/S"'-3 

Run 

Time 

Leak Chk 

Fo 

Checked By: ~-< 

Avg 

; 

,:(-:- - .. 

· AV[j 

Reading Reading 

y Avg 

Distillate Oil 

Residual Oil 

Natural Gas 

Wood/Bark 

Date: 

186567 

.. · ~, 

·,.: 

/F, -- -Avg 

Value Reading Value Value 

I 

I 

Avg 

QC Validation 

F0 = (20.9- %02) I %C02 

ExQected F0 Ranges 

1.260-1.413 Anthracite/Lignite Coal 1.015-1.130 

1.210-1.370 Bituminous Coal 1.083 - :1 .230 

1.600- 1.836 Municipal Solid Waste 1.043- 1 '177 

1 .000 - 1.130 

ff-s-~ll 
FACILITY NAME 

IALCOA-WARRJCKOPERATIONS I 

SAMPLING LOCATION 

)A-446 REACTOR# 3 (One Stack) ) 

CITY AND STATE I NEWBURGH. IN I 

STACK DIMENSIONS 

I .O::::f!:!r:k ID I I anath I Width I 

, •• ENTER IN INCHES I 46 I I I 

TEST DATE 

TEsT TIMES 

TEST DURATION 

TEST RUN ID'S 

G-S-61 

NOZZLE DIAMETER 

(Yl 

Leak Check I Stan 

leak Check I Ea1 

Leak Check 2 St:an 

l..cakChc..:k2F ...nl ~ered Barometric Pressure 

Static Pressure 

OXVQen 

Carbon Dio»de 

Grams/mls Conected 

RUN SPECIFICS DATA 

Runt Rnn2 

10124/2011 10/2412011 

1030-1259 1430 -1725 

144 144 

M315-BHII3-1 M315-BH#3-2 

NOZZLE INSIDE DIAJ\IF.TF.R 

I Ruu ~.2591 Run2 0.259 

DRY GAS METER DATA 

Run 1 Run3 

M-16 M-16 

0.9874 0.9874 

1.952 1.952 

VOLUME METERED 

0.000 

0.000 

0.000 

0.000 

IOJ.lll 

OK 

Ruu2 

142.400 

245.766 

0.000 

0.000 

0.000 

0.000 

103.366 

PRESSURE DATA 

Run I. 

29.60 

.0.31 

Rtol2 ~9.60 -0.30 

MOLECULAR WEIGHT DATA 

Runt 

----:;a:eo 

Run2 

-----:r7:3o 

Ron 

10/24/2011 

1sJs-··.u.Za 

1 ... 

'-M31S·BHII3-3 

OK 

Run3 

0.259 

Ron 

M-16 

Q,g874 

Us2 

Rnn 

246.208 

358.18& 

0.000 

o.ono 

0.000 

0.000 

111.978 

Rtm 

"29.60 

·0.32 

B!.!!L 

18.10 

1.70 2.60 " 2.40 

MOISTURE DATA 

Run I Run:Z Rnn 235~ 201.0 239.7 

POLYCYCLIC ORGANIC MA TITER (POI\1 

Runt I Run2 I Run 

Grams conected I 0.02011 0.02331 0.0180 

TOTAL FLUORIDES LAB DATA 

j Rom I I D·~2 I Run I l11.1illiarams CoDected INIA INJA .. , ,jN/A · I 

I R•n•l ) D·m2 I Run· I I K-Faolor I I I I 

Data Entry NU~IBER OF TRAVERSE POINTS = I ,. I ul ,.1 

DEL TAP 

..,."" ..... '"" 14 L.......... DELTAH ... 

RUNI#l RUN;'12 RUN§3 R1JNI'l RL'Nfl . RtlND RUS.Il Rt:X._~ 

I .0.54 0.135 I 051 0.714 I 0.53 0.718 I I.SS 1 1.50 I LSS I. 170 I ·170 

2 o..s6 o.748 2 o.s6 0.748 2 o..s& o.748 2 uo 2 -!.60 2 u 2 . 111 2 tn 

3 o.so o.748 3 o.tio o.11s 3 o.o 0.7'14· J uo 3 us 3 us 3 , 111 3 112· . 

4 0.66 o.s12 4 0.67 0.819 4 o.n om 4 1.90 4 us 4 2.25 4 111 :"' ··: · .-l7I · . 

s 0.74 · 0.860 s 0.16 o.s12 · s o.90 0.949 s 1.16 s uo s 3.6 s tn s 111 

6 0.89 0.943 6 Q.BO 0.894 6 0~ .0.9j1J 6 1.60 6 2.:30 6 . 3.55 6 i10 6 -IJZ . 

1 0.88 • . 0.938 7 0.76 0.8?2 7 032 0.959 7 .;5S ' 1 l.lO 7 -- 3.55 ·7 liD 7 171 · 

8 -- · ·o.73 ; 0..854 8 D.ti6 o.su 8 o.16 o.S11 8 uo · 8 ·uo 8 u s 110 s tn 

9 o.sz o.nr 9 o.s& o.74& 9 0.16 o.m 9 t.so : 9 1.60 9 u 9 16! 9 1n 

io O.Sl . 0.714 10 0..4& O.G78 10 0..68 0.825 10 I.SO 10 1..35 10 2..6 10 10' 10. i7D 

II 0.42 . 0.648 II MJ 0.640 II 0.60 0.715 II ·t.lO ·.II l.lO 'II .!.3 II 167 11 169 

12 0..34 o..58J 12 0.37 o.608 . 12 o.s1 0.714 12 o.99 12 J.OS 12 · :; us 12 165 . 12 167 

13 0.53 0.728 13 0.55. 0.742 13 0..56 0.748 IJ 1.55 13 1..60 13 . LS5 I) liO 13 1&9 

14 · · o".SS o)42 14 o.57 o.755 14 o.ss 0.162 14 1.6o 14 us ).; · 1..1 14 169 .,4 169 

15 0.59 0.768 I.S 0.64 · 0.800 15 0.64 0.800 IS 1.70 IS 1.85 :15 US 15 171 IS 170 

16 0.59 . 0.768 16 0.67 0.819 16 0.78 0.883 16 1.70 lfi . 1..95 . 16 2.2S 16 169 16 170 

17 0.72 OJI49 17 0.79 0.889 17 0..!7 0.933 17 2.10 17 2.30 17 2.5 17 171 17 170 

18 0.85 0.922 18 0.88 0.938 18 0.89 0.943 18 2.45 18 ' 2.5S 18 2.6 18 1i0 18 liO 

19 0.81 0.900 19 0.88 0.938 19 O.B-t 0.917 19 2.35 19 2.55 19 2..45 19 170 19 169 

20 0.11 o.s-o 20 0.79 0.889 .20 0.78 o.sRJ 20 z.os 20 2.30 2.25 . 20 111 20 169 

21 0.62 0.787 21 0.64 0.800 21 0.7U 0.837 21 1.80 21 1.85 21 2JtS 21 liD 21 168 

22 0.52 0.121 .,., 0.52 O.P-1 .,., 0.62 0.787 .,., 1.50 22 150 i2 I.& .,., 170 il 167 

23 0.44 0.66.1 2.1 0.44 0.663 13 0.49 0,700 2.1 1.30 23 1.30 23 u 23 168 23 166 "

24 o.Js · 0.592 24 o.Js o.616 24 OAt o.64o 24 t.Oo 24 1.10 24 1.2 2.; 1&7 24 l&s 

25 0.000 2S 0.000 2S 0.000 25 15 2.5 25 2S 

2 26 0.000 26 0.000 26 0.000 2 26 26 26 2. u. 26 

21 o.ooo 21 o.ooo 21 o.ooo 21 21 n n n . 

28 0.000 28 0.000 28 0.000 28 28 18 18 !.8 • . 

29 ·0.000 19 . 0.000 19 0.000 29 29 29 29 ':!9 

30 0.000 30 0.000 JO 0.000 JO 30 JO 30 JO 

31 o.poo 31 0.000 31 o.ooo 31 31 31 31 31 J

J2 0.000 )2 0.000 32 0.000 32 32 32 32 32 

33 0.000 J3 . 0.000 JJ 0.000 J] 33 JJ :o -JJ . 

34 0.000 34 0.000 H 0.000 34 34 34 34 }4 

J5 0.000 35 0.000 35 0.000 35 35 35 35 JS 

36 0.000 36 0.000 J6 0.000 36 36 J6 36 36 

37 11.000 37 0.000 )7 0.000 37 37 37 37 37 

38 0.000 38 0.000 38 0.000 38 38 J8 )S 38 J

39 0.000 39 0.000 39 0.000 J9 39 39 ]9 39 

40 0.000 0.000 40 0.000 40 40 40 40 40 

41 0.000 -U 0.000 41 0.000 41 41 41 -U 41 

42 · 0.000 .(! O.OOtJ 42 0.000 42 42 42 4:? 42 . '

-D 0.000 43 0.000 43 0.000 43 43 -(1 43 -o 

44 0.000 -14 0.000 -14 0.000 44 44 44 44 44 • . 

45 - : o.ooo 45 o.ooo 45 O.ooo 4S · 45 4S 45 45 '

46 0.000 46 0.000 46 0.000 46 46 46 46 46 • -4

47 . 0.000 47 0.000 47 0.000 47 47 47 47 4i 

48 0.000 48 0.000 48. 0.000 48 48 48 .;g 48 4

49 0.000 49 0.000 49 0.000 49 49 49 49 49 4

50 0.000 0.000 so 0.000 50 so 50 so so 

51 0.000 Sl 0.000 51 !1.000 51 51 51 51 51 

52 0.000 52 ' 0.000 52 0.000 52 52 52 - 52 52 

53 0.000 53 0.000 53 0.000 53 53 53 53 53 

54 . 0.000 S4 0.000 s..: 0.000 54 54 54 . .s..: S4. 

55 0.000 SS 0.000 -'S 0.000 55 55 55. S.S SS 

56 • o.ooo 56 -o.ooo 56 o.ooo 56 ·sG : · 56 56 S6 

. 57 . 0.000 57 0.000 S7 0.000 57 57 57 57 57 

58 0.000 58 0.000 58 0.000 58 58 58 58 58 

159 ·o.ooo 59 o.ooo 59 o.ooo 3.59 59· 59 35!1 S9 

60 · o.ooo 60 o.ooo 60 o.ooo 60 oo w ro 60 

61 0.000 61 0.000 GJ 0.000 61 61 61 61 61 

62 . 0.000 62 0.000 62 0.000 62 62 62 62 6:2 

63 0.000 63 0.000 63 0.000 6J 63 63 63 &3 . 

64 0.000 64 0.000 64 0.000 64 G4 . I 6.-t 64 64 

65 0.000 6S 0.000 6S 0.000 6S 65.' 6S 6S 6S 

66 0.000 66 0.000 (lfi 0.000 66 Ci5 ·66 65 ·66 

67. 0.000 67 0.000 67 0.000 67 67 : 67 G7 67 

68 0.000 68 0.000 68 IJ.OOO 68 68 '• 68 68 68 

69 0.000 69. 0.000 69 0.000 69 69 69 69 f/1 . : f

70 0.000 70 0.000 70 0.000 70 70 70 • : iD iD . 7

71 0.000 71 0.000 71 0.000 71 71 - 71 71 71 7

71 0.000 71 0.000 72 O.OCIO 72 72 7' 72 72 . 7

7J 0.000 13 0.000 73 0.000 73 73 . 73 73 73 7

74 0.000 74 0.000 74 0.000 74 74 74' 74 74 7

15 0.000 15 0.000 75 0.000 1S 75 7S 75 15 

76 0.000 76 0.000 76 0.000 76 76 76 76 76 7

11 o.ooo 77 o.ooo n· o..ooo n , 11 n 11 n· n 

78 0.000 18 0.000 78 0.000 78 ·. 78 78 7& 78 7

'79 0.000 79 0.000 79 0.000 ?9 79 19 19 19 1

80 0.000 80 0.000 SO 0.000 HO 80 80 SO 80 8

FLUE GAS TEll 

Al-gSqrt ~ 18.589 1__QJ!Q_ 18.151 ~ 19.905 ~____!_]§_ L..J&Q. ~ ~ ~ 
'~ ' ) 

(j·-.. '·· 

(_) 

Meter Box Post Test Calibration. Check 

ALCOA- WARRICK OPERATIONS 

NEWBURGH, IN 

A-446 REACTOR #3 (0\}e Stack) 

~ 

Meter Box#: M-16 _..:.;....:..._--,-

CaJibrated by: 

·. 5-Pt Cal :bate: 

Richey Lowe 

10/12/2011 

Delta H @_--::-'1~.9::-;:5,:;;:-2 

Gamma, initial 0.9874 

Calculate Y qa for each test run using the following equation: 

where: 

Yqa 

q· 

Vm 

Tm 

Pb 

0.0319 

DHavg 

DH@ 

Md 

29 

13.6 

dry gas meter calibration check value, dimensionless. 

total run time, min. 

total sample volume measured by dry gas meter, dcf. 

absolute average dry gas meter temp., 0

R. 

barometric pressure, in. Hg. 

= (29.92/528)(0.75)2 (in. Hg/0

/R) cfm2. 

average orifice meter differential, in. H20. 

·orifice meter calibration coefficient, in: H20. 

dry molecular weight of stack gas, lb/lb-mole. 

dry molecular weight of air, lb/lb-mole. 

specific-gravity of mercury. 

After each test run series, do the following: 

Average the three or more Y qa's obtained from the test run series and 

compare this average with the dry gas meter calibration factor, Y. 

The average Yqa must be within 5 percent ofY. 

If the average Y qa does not meet the +5 percent criterion, recalibrate the 

meter over the full range of orifice settings, as detailed ·in Section 5.3 .1 of · 

Method 5. Then follow the procedure in Section 5.3.3 of Method 5. 

Test 1 Test2 

time 144 144 

Vm- total. 103.111 103.366 

Tmavg .. 72.4 73.2 

Tm-R 532 533 

Barometric 29.6 29.6 

DHava 1.765 1.796 

DH@ 1.9520 1.9520 

Md stack gas 29.02 29.11 

MdAir 29.00 29.00 

Meter Box Gamma 0.9874 0.9874 

QAGamma 0.9950 1.0011 

Difference: 0.8% 1.4% 

within 5%? PASS PASS 

AVERAGE DIFFERENCE 1.8% 

_ ____.::,.;.:,..,:.~ 

Test 3 

144 

111.978 

59.2 

519 

29.6 

2.252 

1.9520 

29.11 

29.00 

0.9874 

1.0183 

3.1% 

PASS 
POM CONCENTRATION. MILLIGRAMS PER DRY STANDARD CUBIC METER 

mgldscm = 

mgldscnz = 

grams * 

Vmstd 

1,000 * 35.314 

0.0293 * 1,000 * 35.314 

82.895 

POM EMISSION RATE. POUNDS PER HOUR 

/blltr = 60 * grams * Qs 

453.592 Vmstd 

/b/111' = .60 * 0.0293 * 23.767 

453.59 82.89544 

12.5 mgldscm 

1.111 lblhr 

Example Equations 

REACTOR#!-· · ·.Is 
· ··--c------ SAMPLE LOG and CHAIN OF CUSTODY RECORD ·---·-

. ·---------------------------··--· 

TR.c Environme~tal C~!Jloi"atio-n ~ ~-r-==· -=~-=~- -=-~=~ == ~~- ~~ -~~ --~---q -~ -=~~~ .. l'RCPro}ectMariager :· ·-. - -- - --·--;--·Jim seme- -.- Alcoa Lab 

554g_ Centervi~~~uite ~ --~ --·-

--~--------

-----·- - --· -- . - 'Telephone No. ··--- ----W919) 25~~~.!.·~-=~ n ~~=-~=--

==-~-;~;;.~~=~~:~_ 

t~-~~!- ~ :~ 

-~:=_~~~~~--~=~~~-:=__==-==~~= 

~~:=~·I"' 1 ~ : 

1 ' ' · • Carrier or Delivery: Sam ;TRC to lab lei.D.No.andDescri tion Date Delivered to La&:··· .. 

---~-· ··· 

-~--·---- ·-· -·-

---------±-

---~ 

-----·-: _____ i=-=~=---_---------t Sample s::ple ;--~;P~~-~~~i~n~l~~;s-~e~~e_:;~eiC 

. ::~:::-~-L_-:_ __ T_:-~;:~=-----.,--_:_~1:~-T-----~-----F:F;;r~~----. ----h-:~-e~_--=_-=_-_-=_=T:-~-t:r~--~---:---C-on-:~~~:~+-.-_-_:_ ___ P~iv(_-:-·~-

t' 

--3&aeks~-

3 Stacks 

~--

·--~f5 

M315 ---·---;-· ··-1 ·; -----... FHAcetone Rinse :· 24-0ct Acetone Rinse ; 250 ml Amber.,.! - POM ___ ----

--~~~ 

::.::::~T~---=---- FH Meth:YierleChiOiideRiriS_e ___ l_~4-0c( Methylene Chloride RinseT_-255-rrifAmber. ·t -· ~_§M-= -~ :~~:.: 

_ 

__ + __ 3 3 Stac~=~~---~~1.§__ Stack~_--~~!?.______ . ____ 1___ . _; ____ lmpinger Catch ~.Q!_~nse 'I 24-0ct ' Water \ 500 ml Amber __ ~~--- _ _£OM .. __ _ .. 

_ _;__ _ '!_ __ . __ : ----· ~f::!.~cetone & Hexane Rinse _______ _:___24-0ct : Acetone & Hexane Rinses ! 250 ml Amber _j _____ ...!:_Q~--- __ .. . .. 

;~:~~!-~-1=___ 

~;~~ 

~~~~~--- r==· ~- ~=:·=~~~~~:~~Tnse 

~-=--i-~tg~-=~=::et:~!f~in:~ ~ ~-- ~~~:~~~~~~e~r~= 

-~-

~-~-g~ =-:. 

--~-­

--·11!:~:-±~=_:-·=~~; _-:: ~- ==-; ~~~~= F::n~~::~e~=t3,h~~~~~::e --T ~tg~~ • Methylene~:t~:de Rinse-~=:~=~ ! 

--~=~~g~ · -~ _. 

_ 

__ -·3stacks-_-_c·:_:::~31·i:=_-=:::_~-:_-~=? ----BH AceiOne& Hexane Rinse 24-0ct Acetone_&_H_e-xa_n_e-Rin-se_s_,_2_5_0_ml ~~rj-:_:_-___ :~_-=:£og~_---- ·· · 

3Stacks----M315 ___ -- -- -T-: ' ====-~=ilt~--==-~-~-:-+24-oct...l ----Riter _____ -'-!_- .. Petri _____ ~ -·- ---···p-aM:=::...::. -

 ,. 3Sta<!_~·-f----

M31~-----~---~----·- FHAcetoneRinse 

_BStacks . \ 24-0ct AcetoneRinse ; 250ri11Amber .L.:. ___ ______EQ~--- _ 

3 Stacks ____ M3~----- M315 _ ~---- FH Methylene Chloride Rinse 24-0ct- .. Methylene Chloride Rinse ;. 250 ml Amber L.- ___ POM ... _ .. 

-·---3Stacks M315 ---~---"3---~ 

' 3 . lmpinger Catch & Dl Rinse . 24-0ct Water 500 ml Amber _L__ POM BHAcetone&HexaneRinse 

~~t--fACetOne&HexaneRiilses: 250m1Amber I ____ POM-~~=-· 

------1--------------------------------------------:---------'------------------------------t·----- : ---------------+------------·-------

~:~f-· 1 

_ _ _! Stac~----1---- ~~-~~~r-··=-~~:~- . M31~--- ____ _!____ --~~~-=~-~---~::::~=~--- ! ~tg~ : Acet:;~e~inse ~~f~::;.:f------{g~-~~=~~-~ 

! 1 Stack FH Methylene Chloride Rinse I 24-0ct · ·Methylene Chloride Rinse . 250 ml Amber L__-~- . __ 

I M315 1 lmpinger Catch & Dl Rinse 24-0ct Water ! 500 ml Amber j ______ POM __ . 1 Stack __ _=t= M31~-=-.:_· ____ i.-=.·=~-= B!:f.Acetone & Hexane Rinse 24-0ct Acetone & He~ne Rinses: 250 ~~Amber 

~---·---!'.Q.I\i!.. 

 

1 stack j---- M315----;·-·-2··------ ----~ilter _______ i 24-0ct 

-~-~-- ·t-··- - Petri-· ·- .1 

___ ··-·· F>orvc· · --1-s-tack--+- ..... -----M-3-15-···- ~-- ·z-: ··• · -- · -FHAceton_e_R_irise·--~-· i 24-0ct Aceto_n_e_Ri ___ n_se----~~2-5-o-~-,A-m-ber ····· 

__ P_O_M_ 

1 Stack 

_ _ _____ M315_~~:=·~- 2 · 

-=~--_FH.Methylene Chloride Rinse I 24-0ct . Methylene Chloride Rinse i 250 ml Ambe':_1 

_____ 1 Stack 1 ___ -~~- ___ POM --·· 

 

~~.,:--i--·- M315 ---·f ___ .L 

___ 

__ . -~--.:_ __ ~pinger Catch & Dl Rinse . 24-0ct Water : .500 ml Amber -+-- ···-

PO~ 

______ _ 2_ __ ; ___ . ___ BH Acetone & Hexane Rinse I 24-0ct r Acetone & Hexane Rinses 250 ml Amber f--·· 

__ POM __ . 

--·-f-------··----·---------·~-

· 1 Stack --.-; -. -M315- ----: ····-3 

-·-··---

__ ; _______ 

·-·-···-···--·-------·-

·- Filter --·-----:---t 24-0ct Riter Petri ·---r--Pcirv1 ____ - ------1- I ·---·--·-

t- 1 1 Stack Stack. ~-~~!? ____ . .)_. ___ 3 __ .__ FH Acetone Rinse _J_. 24-0ct Acetone Rinse --,-! 250 ml Amber ·"1 ~ ___ POfl!_ _____ c 

1 Stack 

--J I ___ M315 M315 ____ _-__L ____ }__ _ FH Methylene Chloride Rinse ___J_. 24-0ct Methylene Chloride Rinse·. 250 ml Amber __1___ ____ ..!:~. ---.- . · 3 . lmpingerCatch&DIRinse J 24-0ct Water 500m1Amber ! 

___ POM ________ _ 

~~=-~-~~~:~-----~-~~=~---~~-~~~=~=--~~=?~~~-~~---~-

_ --~~-~~~-=-=~~~-~~-:~~:~---------~- 24-0ct . Acetone & Hexane Rins:--~~~-=~~=~-~:---t-~~=-==~~~~~=~~~-== 

-~------+----===t===~~~~~~-=-==~~==~~-=~-~~--~-~:~.--~~~=~~==--~------ 

Reagent Blank ! 100 ml , RB Acetone .. 

------

-

___..1,... _______ -- --~-~--=-------

-- ·-- -- ----· 

Reagent8i~inrZ-t---1oorill i 24-0ct Acetone Blank 250 ml Glass . POM 

Reagent Blank 

___ r- .. RB .J...:::=·=---=:-MEithyleneChiortd-~ 

___ __j_ 24-0ct or Water Blank 250 ml Glass . L _- ==POM -~ ... ' 100 ml/ ! RB i . Dl Water ! 24-0ct Hexane Blank 250 ml Glass _j____ __ POM __ 

--- - AI --f--------~-------:.-----------

1 

_--1-·--w~~. 

lv/v-~pc i 

 ___ ·--·------· -~---- -----------· 

__ .:_ _________ . _ . _!)'!_te ..... .. . ...... + __ ---,---- ---·--·--- '· 

Chain of Custody-M315 10/1;j/2011 
.... •': 

. If : 

Method 315 Bl~nk Analysis ;.; ,I' • 

: . '• .. " .. ,o 0 ....... . 

Blank Analysis ~ Partioulate .. '•' .:• •': :'. :•'··· : ·• ·, 0 ·": •• 

tl)/tllr-it.rjejr,f Time:-·/· f'" .. ... .. .... .. .. .. . ' 

Date: . •. .. ; . : .... .. ... . ... ,., ······· ,, . .. • .. o•'• •• 

• 0 ... :· ...... "0 ••• 

... · .... 

.... ·. ': . 

. . ' . . ~ 

Filter No, .f/k. : 

' ; /:: ::_:.: .. .. 

Room .. ·.··· "_ .. I ... , ........ .. '·· . ... , ..... ·.·. ••'\ . HtimJdity .. ·Final-Weight (g) J ,r,•l Tare.Welgbt (g) Weight Gain ·{g) 

.:.·. .. : (%RH). ' ; 

'• .. .... , ... . 

.. ... , ,o,, .••• 

· .• }·,.:0'· . • :, .:.~~ =:,,, • :, •• 

0 .f !o· ···~·. ... 0 .. ,, ••••• 

:?5'1~7 rs.gf15 g~, !f£6 ·- () 00 .5'"" ' .. ,, .. ,. ' ... 

'•, .. .. .. .. . 

Container No. ··1 .. ' .. .. .. . '· -~,··:: ., ., .... .. ... ... , .... 

· . . :. .. . . 

~ .. ~· 0 0 

.. ' ··" 

.. (] .. 

.. 

"Blank Analysis- MCEM .. . .. . . 

. Date:·/ .. ". 

Time: . .... - ' .. 

........ ~ 

Room .. '!·:.· . . ... 

FJnal 

·-.Container 'Hamidlty · Weight (~1). · . .Tare of.· :.Weight Gain Wash :Blank' ~ "' o ' o o ' ~ I 

·. (%f={H) . Aluminum·:: .. =Velum~··· ~ -Pass/FaJJ · ·No:· Dish (g) (L:) l. .(mg/L:). ,, . . . 

'• (g) (mg) 

·fi!h~~~lk .p.;; if.., Jk... 3SI:?Lf. ln. 43!./.3 (p;L.f3'f ~ ,ooo I I l (J ,r.Bs- ,7 .P 

I . . .. .. ' . 

A.etoneBik Jt /3 L{ L ·~~ :J.3 (_ ·. 

f 

-t ({( ~ &.- /, J.f ;;_;;._ 7 ~._fJOtJ If .60 306 Lw .. Methylene . . 

f ~l~~~t~~ 34l5lf. (, q. ss.3 .. t·.'f5i-.>. ,tlt,b ' 3 ()(j" .: .. 

·,dfl_· '60 f .. ..~ 

' 

w~~~Bik 

(0-llk .. &.6lc'?S (p. 46 rtf ~-4/1(3 ,(jjd{ . r o '1"5""" ,~:, ... 

f 

Notes: . . 

·.· ,. .. Blank ar:~alysis must be·c:ompleter:l.before sample analysi~ is started. . .. ·· .... • • •• "' ·,. 0 • 

•• ·Filter Preparation Blank must not exceed 1 mgffilter. ·. 

·• Acetone wa:sn 8eagent Blank must not exceed 1 mg/L. 

. • -Methylene :cJiloride Reageri(Biank ·musfticit exoeeo 1,5 mg/L. 

• · lmpiJ:Jger \fl/~fer Reagent Blank must not exoeed 1.5 mg/L. 

. ... 

: I • .- o ,• ; o " 

·• Room Relauv·e· Humidity must be belew.SD% 'llhen samples--S~t-t>re-b~slnHi!QI-"V''l"i::.'e~igiH'ha="d.,..., -'-:--:----............,-....:--. 
J '·, 

.. · ... 

·' ··' . ,. •'• ~ . .. ' ( . 

• 0 '' 'ol o•, 

"' 

... 

.... ··, 

. : . 

Method 315 BJank Analysis .: ~ .. ~ . ·• 

.. : 

• 4,, o)• .. . :' . .t•',·. · Blank Analysis ~ Particulate . ., • . . ' .. 

Date: t I :-l·-1_ I I Time: I ~~oJ.~" £. ( {~ .. -~~i ·~ 4!.;.pjJ' . ... . . ... . . ~ . . 

" I .. .:•.._,,,., ( o 

• ,,;.., .... • u 

F.lller No. : 

-_ .. :·:·: :.•""•,: 

" R:oom . .. - -~ 0 .. ..... T 

" .. ... ... . Htimldlty ··Finai..W:elght (g) . .' , .... ; \'' ~ :', :-.. ·\' j, ,fi' '· Tare.Weigbt (g) Weight Gain (g) . .' _Co/oRr.n· I ! .. '• .. ... 

...... , ··.· 

; •, .:~·· ~,, . :, . ·. .,.~: ..... ' 

'-• .,,, " I' 

. . .... • ... 

.. .. 

Container No, ·1 .. '• ··.,1'''' .. : . .... •, . "' '". ~' . .. .. . 

,,, "' - -

'·' ;:• .. 

.. ' ' Blank Analysis - M.CEM " 

Date: I .. ... 

·TJme: ..... 

. ' 

Room .. . . - " 

. Final . •'· . .' 

··Container ·Humidity ·Weight@. Tare of.·· ,.Weight .Gain Wash .B,Iank· ~ .. :p~~·siF~il · · 

··'(o/oRH) Aluminum·:· .. ·:velum~:· No: .Dish (g) (L) (mg/L? t. • ..• 

.. {g) .(mg) 

t 

Filter Blk 

.. 

Acet~6Bik 

~- ·IlL Qb' /.Jl-, .. ~ .. Jf'3 tfl ?.''f Jt-f~ . ,01Jt1~ ,~0 1 { (j {) I;, a tF .. 

:. Methylene 

~~w~~k f )G7Jtr l,, 3fl~ /,;.3~1l 1- ()tJ/) ( tt~M ~loa:··. ,CJ 0 .I 

Water Blk 

Notes: 

·, · -o· . Blarik ar.~alysis must be·cc:>mplsted,bsfore sample analysis is started. 

·• ·Filter Preparation Blank must not exceed 1 mg/filter.-

• Acetone Wash Reagent Blank must not exceed 1 mg/L 

·• Methyle.ne~Cnlorfd'e· ReagerifBlahk musftiot exc·eed 1:s·mgtt: ,.. · lmpinger Water Reagent.Biank must not exceed 1.5 mg/L. 

·• RuUJ11 Relatl\fe; l Jumidit)' must be below 50% vJF!sn samples arn balng 'Neighed, 

' 

.... 

·~ . . .. . . . I o •'t ,•, 

. . ' 
• 

, 

Plant: 

Filter No. 

Amount liquid lost 

durinq tran~ort 

Acetone Blank 

Volume (ml) 

Acetone blank 

c.oncentratlon (Eq. · ·315-4) (m~/mg) 

Acetone wash 

blank (Eq. 315·5) 

(mm 

Container No. ·1 

Container No . .2 

rA 

Total 

Method·315 Particulate and. MCEM Ana/ysJs . . . . · ... " 

Partioulate Analysis·· 11 1 1 

U I. 

Room 

Humidity 

(%RH1 

./ Date; J "'· -7..:'-( _ tr ... Run No.. . {( ~d; r-J -/2u.~.i 

() 6 

300M ( 

a 

Final Weight (g) Tare Weight (g) 

.... ,, . 

.. . ,· 

••••• 00 , 

Weight Gain (mg) .. · · 

3.~ 

.3,k. 

14 

Less Acetone blank . -_{_o· ~ oJ . Weight of Particulate matter _J:.4 .. 

. Moisture An~ lysis 

Final Volume (~g) Initial Volume (mg) Liquid Collected .(mg)_ 

lmpingers Note 1 Note 1 

Silica Gel 

Total 

/ - Note 1: ·Oonvert-voJume ·of. wateF tG .weight by multiplyit:Jg_by .tbe.d.ensJty .c:>f_water. _ .. · 

\~- 1 g/m/). 
·. 

.. .MCEM AnaiY.sis . . 

Date:·/.. .. ·· .. '' . . 

Time: . . . .. ~ 

Container' Room Final· Tare of Weighi AoetoneWash · Metby.let:Je 

No. Humidity ,Welght(g) Aluminum Gain Volume(mL) Chloride Wash 

(%RH) Dish (g) (mg) VoJU,mer (mL) · 

: L3:f" 

1 

3s/33 .. . . 

. I~ if7tJt_ G>t ~ ']oi. L ' 

/-( I t'Vl 

( ,. 

f(r; /'3{" ~o..~-~r 

2+2M 

$3 (/;/;3. ''128~ r:~.'f~&3 /J.;{;h 4-5" I LfS" 

1-1 i),_M • .. 

3W . z.~ltLf' ' Lf ,;{, '7 5 6. C/2. o'{ · 3,~ ' . 1- I 3 ltJ' 

§':' . 90 ~'L) . 

'3 s· . : c .. Lf.t &.7-..:· • ;\1 (.) vol' r.• .r: . ·1:"· l' • t 2r/ 3L( &, Lj39sl ~~~-3 .f' 

t-rJS 

1""'' ~ .. .,.,.J • ... ~ .... ·l~ t . . ,. :'1 

.. ;B~r1P .~OM--{;5 Total 

J:mlal:tl rv .. w .. 

Less Aoetsl'le Wash Blank (mg) : 

(not to exoeed 1 mf;J/L of acetone used) -[tJ ,o]. 

Ws.:::: CeP~IVsw 

Less Methylene Chloride Wash Blank (m,g) (not to 

-cc>,.o) -:-

exceed 1.5 mgfL of melhylene chloride used) .-

Wr = o,P,rv~~~' 

Less Filter Blank (mg) ' 

(not to exc~ed 1 mgffilter) ~(6,72 · Fb 

MCEM Wei!;lht (mg) 

mMCEOM = Zmtotsl- Wa- Wr- Fb _(i·7t,~} 

Notes: ~ 

'" Blank analysts must be completed before sample analysis ls started. 

· • Filter ~reparation Blank must not e~c:;eed.1 mgffllter. · 

• Acetone Wash Reagent Blank must not exceed 1 mgfL. 

·• Methylsn~ Chloride Reagent Bh:mk musi: not exceed 1.5 mg/L, 

·• lmplnger Water Reagent-Bl~nk must not exceed 1.5 i-ng/L. 

.. 

-

.. 

SJ~ rv..\5 

!'Vtw 

'' 

.. -

.. 

·.· 

,~; Room Relative Humidity must be below 50% when samples are bsln,g weighed . 

. --·---.... -- --... --- . -... 
!~\ 

'{ ) 

() 

( 

\ Jl '-___, 

' 

·Method· 31'S Particulate and MCEM Analysi-s ~ 

Partioulats Analysis ·. 

A J 

. -Plant ···fo~t~:J,"~"'-'(-:,,j_ Run No . · IT 71~ . ... 'f(f'~br- i ~f2v:"' .. ' 

Filter No, '-/A ,; 

Amoun1 liquid lost · 

during transport rJo ' . ;. 

Acetone Blank 

· 3co ~I .. ., 

Volume (ml) .. ' . 

Acetone blank 

. concentration (Eq. 

. ll{) M_Q..lrn C; . 315-4) (mglmg) ., 

Acetone wash ~ () . ·• .. . . 

blank (Eq. 315·5) '· .. .- :: ~; 

(mg) .. 00~. .... 

Room u ·• 

Humidity: ·Final Weight.(g) 

· (%RH) 

Tare Weight (g) Weight Gain (mg) 

'J~k7 I 

I'd...~, ~O,t::;"" I 2..~ .tp 4-'3 2..: 

Container No, ·1 2..'6 }~~ I 9-.i, I# 4-.t:;C/ / f '2." .~ If 3 ( 

;s- I '2.~; t# tt?... '? ,/ 3 . ')--

7.r"/3i.f. 13¥, f.)~ 5'[, 13 •f. '"s-89le / ... 

Container No . .2 :34- !3'-l-.s9 6:5/ .:;: .• j_ '. ~~-~ 

Total q J 

·l ess Acetone blank ,_ (o '.-a\ · .. 

Weight of'Particulate matter 9.: I .. 

Moisture An~lysis 

... Final Volume (mg) Initial Volume (mg) Liquid Collected 

(mg) 

Jmpingers Note 1 Note 1 

Si Jica Gel 

To tal 

Note 1: · Cot'lvert·volume -of. water -to-weight .by multip!y.ing. by the . .density Q.f. WE;!ter . 

1 g/mf), 

g__ 

... 

----------

. . . ' 

, 
.... 

.. .l0GEM Analy,sls 

Date: {. .. • TJrnB: .. .. .. I! 

.. Methylene 

Container· · Room Final Tare of Weight AcetoneWash 

No. · Humidity . Weight (g) Aluminum Gain Volume(mq Chloride .Wash 

(%RH) Dish (g)· (rng) Vol~me (mL) 

: (I/~ 1 . 28 13~ .. ,(e, l-{· f r"? 1-~ /IV! (/) tfPf4- ·~- I .. r-s-,l-I . ror'J...r 

2+2M 

~.31.713 lh,ll?.k/78 ~~ Lf&(Jf" &. r,v y5 11 rj 

!-?.. :JrVI . ,. 

3W 9,6/34_ 

. ., 

'&. 4-il7 t!: ·lf~St: · !..f. I .. 1-2.. .3 lA{ 

·. G,.~~~'3·· -~ ~~-+- 2.r . 38" .· '-r(3i.J. 6, 'f!etJ 7 j:J,,i A/$ \Ia (u ~·.:e :· 

_/ -'L _3_ 5 ,. ( J 

+ ( r l'i! ·o:.··r1, ~~ f..·,<·'' 

'Total ~~~~ ·q { .f\". ( .5 . 4-&! 7 IVl Ls .. 2m role/ .!'veil, Xv'"' 

Less AceteAe Wash Blank (mg) 

(not to sxc:eed 1 mg/L of acetone used) 

· ~ (6.o} .. W8 = C11P efVaw 

Less Methylene Chloride Wash Blank (mg) (not to .. ') .. exceed 1.5 mg/L of methylene chloride used) . . .. 

-{o, o). . . .. 

Wt = .o,P~Vtw •.. .. 

Less Filter Blank (mg) 

(not to exaesd ·1 mg/flltar) .. -(o,7). · Fb -. 

MCEM Welght (mg) 

mMDI:DM -::::: Zmtwer- We- Wt ~ F.b (~:iR) 

Notes: ~ 

·• Blank analysis must be completed before sample analysis Is started. 

• Filter ~reparation Blank must not e:xc:Md: 1· mg/fllter. 

• Acetone Wash Reagent Blank must not exceed i mg/L. 

·• Methylene Chloride Reagent Blank must not exceed 1.5 mg/L. 

.e lmpingerW~ter Reagent.Biank must not exceed 1.5 mg/L. 

..., Room Relative Humidity must be below 50% when samples are being weighed. 

---------- --· --- ..... 
Method 315 Particulate and. MCEM Analysis . '.. ... . . . . 

P.artlc::ulate Analysis A. ~-Ltl_ .. 

Plant: . { Date: { ,Q ~'2.'f.-d 1 · Run No.· . R-e~Jr)~~ -R·u·V\ 3 

Filter No. 2.A ' - .. 

Amount liquid lost , 6 () .. 

during transport . '· ,, 

Acetone Blank I 

·~ 6D CAA.-• I .. Volume (ml2 ' . . Acetone blank 

oonoentratlon (Eq. .. , {) 0 A J m:~ 315-4)J_m~/h'it:Il .. Acetone wash .. () . ·, .. 

blank (Eq .. 315-5) .. :·. :· : 

(mg) . ( () {J M..v : 

·Room·. \\. 

Humidity Final Weight (g) 'Tare Weight (g) Weight Gain (mg) • 

(%RH). 

>~/Qr-; 

I ........ I 

/3tJtpqt,~ . '_[~ f' I lf:lj.!j'· I 

() Container No.1 k~/33 / 3 (),l .. J/1/o 0 -· I 3,r> . .l.f&f '1.3 

J~/: IJ.o.'f~'f~., l/-f 

f)~/'3!-1 I fJ I .·t.,-p_7?_ J~l. G-7~!l .r ... container No·:..z~· ·- · Btf j~l_ L,j/_'?7/ .9.7. 

'2.A 

Total I { 1 

Less Acetone blank . ~r o~o 'J 

Weight of Particulate. matter. J.l:' ., 

Moisture An~lysis 

" 

Liquid .. Collected ,. Final Volume (mg) initial Volume (mg) .. 

(ing) . .··.·. 

Jm pingers Note 1 Note 1 

Si fica Gel 

To tal 

· u/ . ·-.. .. Note .1 ;- Convert volume· of water-to· weight- by-multiplying by the density G>f water. ..... · 

1 /mf, 

' 

.. 
. . . . . . 

·. 

.. .I\!IC~M Analysis 

Date: J ' . '' ... 

~ .. '' Time: 

Room Container· Final 

No.· Humidity Welght(g) (%RH) 

'1 '-fo(stf · J<~rM '. 4?/o~ 

2~2M 

!..-."?. ~ ·M '33}t;Rg_ &/1~(,)~ , 

3W 

zds'f ?.'fbt(3 I ·'3 ..;> 

?.w . 

' 

~:.P/s~ ~ 0 ~ 5(/ ~ 

Total 

Less Ac::atefle Wash Blank (mg) 

(not to exceed 1 mg/L of acetone used) 

Ws::: o~P,J:Vaw 

" 

·' 

Tare of 

Aluminum .. Dish (g) 

''' . ' 

(,, t-{~1,3 •' 

-~ tff LJ-P 

r;. 'f"t...'o· 

Less Methylene Chloride Wash Blank (mg) (not to 

exceed 1.5 mg/L of msthyleme chloride used) · · · 

Wr··= o,P~Vtw 

Lass Filter Blank (mg) 

(not to exoesa 1 · m,g/filter) 

· Fb 

MCEM Weight (mg) 

mMCSDM =Imtolal- Wa.-w,- Fb 

Notes: 

Weight 

Gain 

. (mg) 

,3 

·. 

·§)f 

:3,3, 

.. 

Acetone Wash 

Volume (mq 

oe Blank arialysls must l:ie complsted before sample analysis is started. 

.. Filter Preparation Blank must not excee£1 mg/filter. 

·• Acetone Wash Reagent Blank must not exceed 1 mg/L. 

·• Methylene Chloride Reagent Bla.nk must not exceed. 1.5 m.g/L 

• lmpingerWater Reagent-Blank must not exoeed 1.5 mg/L ... 

·• Room Relative Humidity must be below 50%. when sampl~s are .bslng weighed. 

MethY,Iens 

Chloride .Wash 

Vo!t-~me (mL) 
Method 315PartlcuJate atJd. MCEM Analysis . . . . . .. . . ..:· . 

P~rtlculate Analysis .4.. t._n I I 

Plant:. ./Date: { 1o ... 2..'1~il Run No. . . "~!I ( ( y PI 1P~a ~- 6 r ~ tA'"" :::1-. 

P:i/ter No. GA . .., 

Amount liquid Jost . '() () durinq transport 

' '·· 

Acetone Blank •. 

· s O(Jfr\ .} · .. .. 

Volume (ml) .. . . 

Acetone blank 

concentration (Eq. 

I. () 0 M.J_M' ·. 315·4) (mg/m.rJ) . 

Acetone wash u . 0 .. . i 

! 

·I 

blank (Eq. 315-5) . - ~ ." .. ': ,• 

(mal ,.60 J>V} I 

Room l .. 

Humidity · · Final Weight (g) · Tare Weight (g) Weight Gain (mg) I " 

Jo/oRHl 

JJ! rJ7 .~~.Usr· (! .Z.. I 7' 7 '7 

CJ Container No.1 · 2-t/) 3 5~ 2~./.hl fz_. I o/7:Z--

Jrh_'-f· .K~ .//nJ!i/ !$").., I '177 / t3,7 

2.!'"/9'1 lj$'7 LjqQ_~ 137·'1-612../ 

Container No: 2 :~'+ 1.~ 7 l.f73/ ,/ ·fief" 

CA ' . l· 

Total ~l, .. 

Less Acetone blank ~ro :e) .. . . 

Welght of Particulat~ matter . ,!JS.'h 

· · Moisture An~Jysis 

' Liquid Collected 

Final Volume (mg) Initial Volume (mg) (mg) 

Jm pingers Note 1 Note 1 

Si Ilea Gel 

To tal · 

r · ·-- · Note·1;· Gonverf·vo)ume- GJf.water.to-welght by multip.lyingJJ.)! .tbe_de.nsJty. C?LWf3t~L _. _: _ \J · (1 g/ml). 
.- ·. 

" .... ... .MCEM Anai.Y.sls 

• Pate:j 0 0 

0 0 

~ . Time.: 0. ' . ' • 0 ' .. • 0 

0 "' 

Container' Room Flrial . Tare of Weight AcstoneWash 

Humidity Aluminum Gain 

No. (%RH) WeibJht(r;l) Dish (g) (mg) Volume (mL) 

.. 

: 

1 ·s3/33 

o I • o \ 

.'3-1 I#! ~ 41.. !"F ~./i~ rz~ I~ • 

I .. So, '3 s> . · 2+2M 

J~/lf/(1 1/ .. 4'1(/!d 4 ., Lft.f 55" 3!5/ g,.....f ~'M 

. 3W W s w( J ?.S/3'1 t/tltt9 t.t.ftJ"o 3.~ 

3 S· zr/Jt.f' (,,ff35 t . '1. e ' (') · . n::o .. ,AI() 1/ tA:..J. S!?i 0 "t: 0 

'3 -r 3S. f~.~ "*" t 1'; t't' [! :,t;~,.}- r , . 

Total '&.~'$ I~'[' nvl-5 

·rmcolsl LV11w 

Less AoetCJne Wash Blank (mg). 

(not to exceed 1 mg/L of acetone used) -(a,~). Ws :;; ofP s'ZVaw 

Less Methylene Chloride Wash Blank (mg) (not to ~· 

exceed 1.5 mg/L: of methylene chloride used) · ,. 

·- (o:.o).·. 

Wt = o,PiZVtw 

Lass Filter Blank (mg} 

(notto exceed 1 mgffllter) ~ (b ."7J · Fb 

mMCEOM 

MCEM Weight 

= Zmlolsl-

(mr;i) 

Ws- Wt r Fb (~ J-.01, 'f ' -..... 

-- Notes; 

,., Blank·analysls ·must be completed before sample analysis is started. 

• Filter J:reparation Blank must not ex('}eed.1 mg/fiiter, 

•• Acetone Wash Reagent Blank must not exceed 1 mgfL. 

·• Methylene Chloride Reagent Blank must not exceed 1.5 mgfL. 

·• Jmpinger V\fater Re13gent -Blank .must not exoaed 1 .5 rng/L. 

.. -- ' 

• 0 

' 

'. 

Metl:wlene 

Chloride .Wash . 

Volt.une (mL) 

'1'35 . 0 • ' 

~,.~'2.!"" 

qs- !C?O 

.. 

~0-z..r.; .. 0 • 

.( r'' 

SLJG""-1.5 

1'Vtw 

0 0 

... 

' 

.. 

• · Room Relative Humidity must be below 50% when samples are being weighed. 

-. -· .. 

- -·· ......... 

-..... 

-..... -- ............ 

-........... --- .. --

-.... 

--- . 

-

- .. ----------·-·-·· 

,I 

. i 
f)' / 

• 

, · Method 315 Particulate and. MCEM Analysis· 

I . 

Filter No. 

Amount liquid lost 

during transport 

Acetone Blank 

Volume (ml) · 

Acetone blank 

ooncentration (Eq . 

. 315-4) (mr~lmr:J) 

Acetone wash 

blank (Eq. 315-5) 

(mQ) 

I A . 

Room . · Humidity 

(%RH) 

·"' 

.Particulate Analysis · .4-LI_U./:. · · 

·.on .. 

SCI6M/ 

" 

Final Wsfght (g) Tare Weight (g) 

:. 

.. 

. .. 

, ,"··::. ; 

Weight Gain (mg) .. · · 

~(=) --- ··~ cC>ntainei'-No~;;r--il?/33 

-1 Tf.~-ot-l.fl:/- --!;&t-.~.fl.s-s1r·'3:.r r's'i. 3~5'7 / 

Total 

Less Acetone blank 

Weight of Particulate matter 

Moisture An~Jysis 

Final Volume (mg) Initial Volume (1}19) Liquid Collected {mg) . 

lmpingers Note 1 Notei 

Silica Gel 

Total 

(j- ~ote .. 1: Convert volume of water·to weight by. multiplyJng by. the density .r.:>f water. .. 

'- 1 /mf. 

. . 

., . 
·. 

Date:· f. ·,. f •·. . . ' •· 

.li.me.: . 

"I! 

Container· Room ' Final ·. T~re of 

No. Humidity \1\leit;Jht (g) Aluminum 

(%RH) Dish (g) 

'( ' I 

3W 

j~Z... J w zr--j3Y ~/1tr93 ~~ ¥¥ 1./ '> 

iota! 

Less Acetr:me Wash Blank (mg) 

(npt to exoeed 1 mg/L of acetone .use~) 

We·= CePsZVaw · · ·. · · 

Less lvlathyle'ne Chloride Wash .Blank (mg) (not to 

-exceed 1.5 mg/L of methylene chloride used) '· 

Wt= o1P;Zvrw 

J..ess Filter Blank (mg) 

{not fo exoeBd '1 mgffllter) · Fb . · 

IIIICEM Weight (mg) 

mMO!EDM = Imtwsr Wa- Wt ~ F.b 

Notes: 

. We.ight 

Galn 

(mg) 

I :t· 

s 

AoatoneWash 

Volume{mq 

f'/6' Vc·(: ., "'{r.•.r,•· t 

r l-f. 1 M l_;; 

.· 

-(o,q)·· ... 

·• Blank analysis must be completed before sample analysis Is started. · . 

·• Fllter'~rsparation Blank musl not excesd:1 mg/fllter. 

• Acetone Wash Reagant Blank must not exceed 1 mg/L 

·• Me1hylene Chloride Reagent Blank must not exceed 1.5 mg/L. 

·• lmp!ngar Water Reagent.Biank must not exceed 1.5 mr;1/L 

Metb>t.lene 

Chloride ·Wash . · Vol~rne· (mL) 

. I 

l r::; 

'!I 7 M.(.:S 

··:oJ Room RE!Iative Humidity must ~e below 50% when samples are .being weighed . 

. -.... -............ - ... .. 
Method 315 Particulate and. MCEM Analysis , .. 

' PartlouJate Analysis Auu_i· 

"· Plant . J Date; {t£) -'2..~~ 1(. Run No. _fRe_cu.t-~; 3 ·:_ !<u:·,., 3 

' .. . Filter No.. "J'A . . .. 

Amount liquid lost 6() durinG tran~Q_ort . .; . . : . 

Acetone Blank 

'3_/)tJ M I .. ~ ., . 

Volume (ml) · . ; 

Acetone blank 

concentration (Eq. 

...- LJ {j fVLJ-1 M I_ . 315-4) (mq/mg) 

Acetone wash . ~ {j -- ., . ' . ~-

blank. (Eq. 315-5) .. .. /'• ::· . 

·.(mal . otJ,~ ... Room u 

Humidity Final Weight (9) Tare Wei_ght {9) Weight Gain (mg) ·' 4: 

(%RHl 

'"31 /,o']_ X?t-~m3 s- trj;' tf. Q? ::-s-o 

(~) '/!:. " 

Container No. 1 'i..B 3 -~ If _l/7 _3__'d--_./ 'ft¥. _, 'S''SP- ,q: G- I 

'3.r· .€ 'f •. 6t r¥ 4 

?,r.!J'f 133. (rC{ s-~ I 3 'J · ~-' tp 7 / 

Container No.2 34- 133.~9 5"'7 / . ~-7.8. 

~A 

Total . tf5',~ 

.Less Acetone blank -(_a,o) 

Weight of Particulate m,atter ·4k., d-; . 

Moisture An~lysis 

Final Volume (mg) lnttial Volume (mg) Liquid Collected .. (mg) 

lm plngers Note 1 Note·1 

Sl lica Gel 

To tal 

() Note :1·; -Convert -volume of water-to- weight .by multiplyln,g-by the .densriy. Gf .water. ____ : _ 

1 /mi. 
.. .M.CE:M Analysis 

Date:·/. .. Time,:_ ·• .. ~ .. , 

Container' Room Final Tare of Weight Aceto neW ash Metby.lene . 

No: Humidity Weight (g) Aluminum Gain Volume (mq · Chloride .Wash 

(%RHJ Dish (g) ... (mg) Vol4me(ml) 

I ; t5fJ 

1 

'4-t& . , .... 

J ... J lilA /,.., 4 7&t'J G, l.f1j h 0 'If . I I .. ~o.,'3/p 7~ *'~s- 2+2M 

·33/t:;~· I (jJ-ftCf ~ Yf) I& lj ~If 7 g_,/~ •l(-&.) I '5'5'" _3.-,~ ::J 'AA 

0 ( 

~~5 SW 

/).6/ t}d_ ~,t.flrt~~ t;, ' '( 4> 'f S" Lf, - ' 0 

3"3 '3W ~ 

I 

s' ., -,o +'Lr · 

3 S· ·: 

~iJi u.J73'B 0' 

1/ry ;/•; '/[' I ·( I {.I • •, ..... 

&. 6FC'f ~ '·· \ '"'" J { • ,,.,, .. , 

. $-'3 > -~ ~ c:s . . ' ·f I ~'' - -~· ,- ~- , .. I 

}'8 ,iJ L 3/ Ml5 706 ttA{S 

Total r 

Imtchll !Vaw I~ : Less Aoetene ~ash Blank (mg) 

(not to exceed 1 mg/L of acetone_used) - {o,~)·. w~ = c,.P,.rv~w 

Less Methylene Chloride Wash Blank (mg) (not to 

-(0, ;·) ~· 

exaaed 1.5 mg/L of methylene chloride used) ·' 0. 

W, ::: GtPtZVtw 

Less Filter Blank (mg) .. 

(not to exceed 1 mg/fllter) - (cL7) · Fb 

MCEM Weight (mg). 

(tl .. a) · 

mMcEOM-= Imto1ar We- Wt ~ Fb 

Notes: 

.e Blank analysis must be compfeted before sample a~alysls Is started . 

.. · Filter preparation Blank must not excreect: 1 mg/fllter. 

• Acetone Wash Reagent Blank must not exceed 1 mgfL. 

·• Mathylene Chloride Reagent B)ank must not exceed 1.5 mg/L, 

·• · lmplnger Water Reagent -Blank .must not .exceed 1.5 mg/L. 

-

0. 

,, Room Relative Humidity must be below 50% when samples are baing weigh'ed. 

-.. .. ... .. . ... .. -.. .. .. . .. . . 

'' 

-

.. 

.. •' 
10 Minute Pretest Audit Form 

.... I • --· • ' 

·•· ....... :."· . · .. · 

--. i . I 

. ' . . . . 

Yq a ( E>J * ~ 0.03 19* (r772 + 460) 

· VTn- . Pbar 

0.5 

[ 

14 + ( 0.0 /60 ) J [ 0.0319. ( 73.5 + 460} J 

min sec * T meter = I 0.9868 I 

10.713 . 29.85 . 

Volume Metered Pbar 

0.97 * 0.9874 =I 0.9578 

Y gamma 

1.03 * 0.9874 =I 1.0170 

Y gamma 

TRC 

Environmental Corporation 
10 Minute Pretest Audit Form 

. . ~ '! 

' ' 

M-10 , -··' t '-· •I' "', ' t 

~- -- - -- - - ~ -- - 1.815 

0~9912 . ·; .. _ ... ·. 

. .... • ... 

· ...... 

,.;. 

--; 

' ' ' 

' ' 

~a . ( E>J * ~ 0.03 19"' (rnz + 46<?} 

Vln . Pbar · 

0.5 

[

-16_m_in_+ _(_a_. a s-~6- 0 o_) -] * [ 0.0319 * ( 69.0 T :e:~o ) J = l._ __ o_.s_s_42 _ __.1. 

12.151 . 29.60 

Volume Metered Pbar 

0.97 * 0.9912 =I 0.9615 

Y gamma 

1.03 * 0.9912 =I 1.0209 . 

Y gamma 

TRC 

Environmental Corporation 
C' 

MeterBoxiD 

Gas Meter Number 

Calibrated By 

Orifice lD 

Orifice Coefficient K' 

Ambient Temperature 

Vacuum t:':l4.1" Hg) 

Delta H 

Initial Volume Ft3 

Final Volume Fe 

Total (;::5 Fe) 

Initial DGM Temperature °F 

Final DGM Temperature °F 

Average Temperature °F 

Time Minutes 

Time Seconds 

DeltaH@ 

Gamma(Y) 

Average Gamma (Y) 

Delta H@ tolerance ~~. RC~·~:~. : ..... -... ~-· .. -. '. -~ .. - '.- . ~~ M10 6839401 .G. Byrd Run#l Run#2 Pass 

!,-,, 

u 

Dry Gas Meter 5-Point Full Test 

I 

Run#l Run#2 

Pass 

Calibration Date 

Barometric Pressure 

Orifice Set Calibration Date 

Run#l 

Pass 

Run #2 · Run #1 

Gamma(Y) 

DeltaH@ 

Pass 

6/6/2

29.

2/16/2

Run#2 

1

-- 0.9

1.

QA/QCCheck: SignandDate. ~'l u 

I 
I Dry Gas Meter Temperature Display Calibration 

MeterBoxiD 

Date 

Calibrated By 

Input Temperature 

M10 

6/6/2011 

G. Byrd 

1

- Channel temperatures must agree with+/- 5 °F or 3 °C 

2

- Acceptable temperature difference is less than 1.5 % 

-J 

Reference Calibrato

Serial Numb

Reference Calibration Da

Temperature Reading from Individual Thermocouple Inpu.t

Dry Gas Meter Thermocouple Calibratio

Reference Thermometer

75 . 75 

3 

- Dry gas meter thermicouple is compared to an ASTM type mercury in:glass ref

QA I QC Check: Sign and Date ·{U·)-~ 
---

 

 

 

. 

_M16 

14435277. 

G.Byrd 

Run#l Run#2 

Pass 

0 

Dry Gas Meter 5-Point Full Test: · · 

l 

Run#l Run#2 

Pass 

Calibration Date 

., 

Barometric Pressure 

Orifice Set Calibration Date 

Run#l 

Pass 

Run#2 Run#l 

Gamnia (Y) 

DeltaH@ 

Pass 

8/5/2011 

29.48 

2/16/2011 

Run#2. Run#l 

Pass 

I 

-

QA I QC Check: and Date 08-05-11 . 

. ....._, 

) 

"-'../ 

Run#2 
Dry Gas Meter Temperature Display Calibration 

iD 

ate 

By 

re 

M16 

8/5i2011 

G. Byrd 

Pass Pass 

must agree with +/- 5 °F or 3 °C 

e difference is less than 1.5 % 

RC- 

-----~-

l 

Reference Calibrator 

---Serial Number 

Reference Calibration Date 

Temperature Reading from Individual Thermocouple Input? 

Pass Pass Pass Pass Pass Pass 

Dry Gas Meter Thermocouple CalibratiQn3 

Reference Thermometer 

73 74 

_ Omega-CL23A 

~T-235647 

8/16/2010 

Pass Pass 

Pass 

3

- Dry gas meter thermicouple is compared to an ASTM type mercury in glassreference thermometer 

QA I QC Check: Sign and Date (2e)_U 08-05-11 

-.· .. · 
() 

() 

(~) 

Pitot Tube Inspection Sheet _ i!'·TRC 

:.~ .· ·.~---

Pi tot Number: 

Inspection :O'ate: 

.RPT-AO 

·. 01/04/2011 

Calibrated By: __ ·. ------=0~·-=B~y_rd:--------

Reviewed By:._ -'""'------...:C:....:.':....:.F:....:.in:..:.:k:..:.:__;..._ __ _ 

Pit?t Type: . Detachable TiJl ~..I __ X-'--...J Fixed L..'------l PMlO I .. l---'--___,.., -' . . . 

Wind Tunnel Calibration? 

I 

I 

Diagram 1 

-~a1 

. 

a; ./ .· 

. 

Degree indicating le~el position 

for deten'ni~ing a1 and Cl:!. ' 

Diagram 2 

Degree indicating level position 

for determining P1 and P2• 

Degree-Indicating level position fcir 

determining y then ca}culate z. 

~--- . . . ~"' -~"!--~-

. t / 

Degree indicating level position for 

determining e then calculate w. 

_No[KJ 

Comments: Installed on Probe RP-4B 

TC: RT-4B 

Yes L-1 ----~ ==,._ ·Coefficient:_ A s~dec=] 

.. Bstdec=J 

Level? ·YES 

Obstructions? NO 

Damaged? NO 

" 

Diagram 1 - -10° < a 1 < +10° = 2 

-10° < a 2 < + 10° = 1 

Diagram 2 

-50< ~1 <+50= ,2 

-5°< ~2 < +5° = 0 

Diagram 3 

y= 1 

0= 1 

A= 0.949 

Pa:::: pb = A/2= 0.475 

0.188 11 _:::: D1 _::: 0.375 11 = 0.375 

1.05 D1 < A/2 < 1.5 D1 = .. YES 

z =A tan y < 0.12511 = 0.0166 

w =A tan e < 0.03125 11 = 0.0166 

w and z meet specs? " 

YES 

The pitot tube/probe meets or exceeds all specifications criteria and/or applicable design features and is hereby assigned 

a pi tot tube coefficient factor of 0.84, unless a specific wind tunnel calibration· coefficient has been detennined. 

40 CFR 60, Appendix A, Method 2. Verify the minimum 3/4 inch separation between the pi tot tube and the nozzle and minimum 2 inch setback 

of the thermocouple (or 3/4" separation) in the assembled probe. 
Pitot Tube Inspection Sheet 

Probe Configuratio~ 

Pitot Number: RPT-40 

Inspection Date: 1/ 01/04/2011 

A. 

B. 

c. 

OR 

D. 

CTlRC 

Calibrated By: ____ G_. _B.:...yr_d ___ _ 

Reviewed By: C. Fink -----------

Dt=l 0.375 

Dn=l 0.500 

a =I 1.500 

p a =I . 0.475. 

Pb=l 0.475 

b=l 1.000 

c=l 4.500 

d=l 4.000 

e=l 2.000 

OR 

c=l 

f=l 

Specifications (EPA Method 2) · .. 

Dt = 3/16" to 3/8" 

Dn= 112" 

a 2: 3/4" 

b 2: 0 

c 2: 3" 

d 2: 3" 

e 2: 3/4" 

f 2: 2" 

Pa=Pb 

1.05 Dt :S P :S 1.50 Dt 

IDOES PITOT CONFIGURATION MEET SPECIFICATIONS? YES 
( 

~) 

Pitot Tube Inspection Sheet 

PitotNumber: 

Inspection Date: 

, 

RPT-78 

·. 01/04/2011 

Calibrated By: ______ J._L_o;_w_e _____ __ 

Reviewed By~ C. Fink , ~----------~-----------------

Pitot Type: Detachable Tip I . X Fixed ._I __ __. PM10.,__1 _ ___. 

Wind Tunnel Calibration? 

Diagram 1 

· Degree'indicating.level position 

for determining a; ·and a2. 

Diagram 2 

Degree indicating level position 

for determining P1 and P2• 

Degree Indicating level position for 

determining r then calculate z. 

Degree Indicating level position for · 

determining e then calculate w. 

No[TI 

Comments: Installed on M5 probe RP-3K 

TC: RT-3K 

Yes I._ __ _. ===I~ Coefficient: A side~ 

Bsidec=J 

Level? YES 

Obstructions? NO 

Damaged? NO 

Diagram 1 

-1 0° < a 1 < + 10° = •1 

-1 0° < Uz < + 1 0° = 0 

Diagram 2 

-5°< ~I <+5°= 0 

-50 < ~2 <+50= 0 

Diagram 3 

y= 0 

®= 0 

A= 0,906 

Pa = pb = A/2 = . 0.453 

0.188":::; Dt:::; 0.375" = 0.375 

1.05 Dt < A/2 < 1.5 D1 = YES 

z =A tan y < 0.125" = 0.0000 

w =A tan e < 0.03125" = 0.0000 

w and z meet specs? YES 

The pitot tube/probe meets or exceeds all specifications criteria and/or applicable design features and is hereby assigned 

a pitot tube coefficient factor of0.84, unless a specific wind tunnel calibration coefficient has been detennined. 

40 CFR 60, Appendix A, Method 2. Verify the minimum 3/4 inch separation between the pitot tube and the nozzle and minimum 2 inch setback 

of the thermocouple (or 3/4" separation) in the assembled probe. 

.I 

i 
Pitot Tube Inspection Sheet 

Probe Configuration 

Pitot Number: RPT-78 

Inspection Date: . 01/04/2011 ----------~~~~-----------

A. 

B. 

c. 

OR 

D. 

CTrc. 

Calibrated By: J. Lowe ---------------~~~------------ Reviewed By: C. Fink , ----------------------------------------

D1 =j 0.375 

Dn=l 0.500 

a=l 0.875 

Pa =j 0.453 

Pb=j 0.453 

b=l 0.375 

c=l 4.750 

d =I 5.000 

e=L 2.000 

OR 

c =I 

f=l 

Specificatiqns (EPA M~tltod 2) ·. 

Dt = 3/16" to 3/8" 

Dn = 1/2" 

a ?:3/4" 

b ?: 0 

c ?:3" 

d ?: 3" 

e?: 3/4" 

f?: 2" 

Pa=Pb 

1.05 Dt .:S P .:S 1.50 Dt 

I DOES PITOT CONFIGURATION MEET SPECIFICATIONS? YES 
lnA-?!l-11) Glass Master for printinQ.xlsx 

11/5/2011 

,. 

I 

' : .I 
(09-29-11) Glass Master for printing.xlsx 11/5/2011 

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