## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028** 

AK Doyon Utilities/ Unit 4
Solid/Coal 4 5 60 60.2 246 9.6 0.8 2.8

AK Doyon Utilities/ Unit 4 Solid/Coal 5 5 60 61.4 246 11.2 0.6 3.9 AK Doyon Utilities/ Unit 4 Solid/Coal 6 5 60 59.1 247 10.3 0.7 4.4 AK Doyon Utilities/ Unit 7 Solid/Coal 1 5 60 60.7 255 10.1 1.9 3.9 AK Doyon Utilities/ Unit 7 Solid/Coal 2 5 60 59.7 252 10.9 3 4.2 AK Doyon Utilities/ Unit 7 Solid/Coal 3 5 60 56.6 250 9.9 1.3 5.2 AR Weyerhaeuser Dierks Mill / Unit 5 (1997) Solid/Biomass 1 5 60 52.1 255 12.44 7.2 17.4 AR Weyerhaeuser Dierks Mill / Unit 5 (1997) Solid/Biomass 2 5 60 54.4 255 12.48 7.5 12.4 AR Weyerhaeuser Dierks Mill / Unit 5 (1997) Solid/Biomass 3 5 60 50.8 255 13.37 3.5 6.9 AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) Solid/Biomass 1 5 120 77.8 200 17.34 2.2 58.6 AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) Solid/Biomass 2 5 120 80.9 255 19.08 1.8 32.1 AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) Solid/Biomass 3 5 120 78.5 250 18.75 1.1 24.3 FL Smurfit-Stone Solid/Coal 1 5/26a 60 45.5 250 4.93 1.3 2.7 FL Smurfit-Stone Solid/Coal 2 5/26a 60 46.2 250 4.3 0 2.1

FL Smurfit-Stone Solid/Coal 3 5/26a 60 44.3 252 4.08 0 7.1 GA GP Monticello Plywood (2/21/08) Solid/Biomass 1 5 120 91.9 245 13.01 3.8 0 GA GP Monticello Plywood (2/21/08) Solid/Biomass 2 5 120 100.0 245 12.41 1.8 1.1 GA GP Monticello Plywood (2/21/08) Solid/Biomass 3 5 120 95.1 235 14.32 1.2 0.4 GA GP Monticello Plywood (2/7/07) Solid/Biomass 1 5 120 92.8 250 20.05 6.7 8.3 GA GP Monticello Plywood (2/7/07) Solid/Biomass 2 5 120 89.2 250 18.68 8.1 13.6 GA GP Monticello Plywood (2/7/07) Solid/Biomass 3 5 120 93.1 250 17.02 0.9 15 IA ADM Corn Processing Cedar Rapids Solid/Coal 1 5 120 67.6 265 11.7 0 4.3 IA ADM Corn Processing Cedar Rapids Solid/Coal 2 5 120 62.9 267 9.83 0 8.6 IA ADM Corn Processing Cedar Rapids Solid/Coal 3 5 120 64.8 265 11.41 0 2.2 IA Iowa State University B1 Solid/Coal 117/202 62.5 35.6 6 0.5 0.2 IA Iowa State University B1 Solid/Coal 217/202 62.5 35.5 7.7 0.6 0.4 IA Iowa State University B1 Solid/Coal 317/202 62.5 34.5 7.8 0.6 1.1
IA Iowa State University B2 Solid/Coal 117/202 62.5 35.4 7.4 0.3 0.3 1
IA Iowa State University B2 Solid/Coal 217/202 62.5 36.5 8.2 0 0.7
IA Iowa State University B2 Solid/Coal 317/202 62.5 35.3 8.4 0.4 0.1 1

IA Monsanto Muscatine #8 Cond. 1 (5/2007) Solid/Biomass 2 5 60 40.6 10.2 1.15 7.4 IA Monsanto Muscatine #8 Cond. 1 (5/2007) Solid/Biomass 3 5 60 40.8 10.7 2.05 5.5 IA Monsanto Muscatine #8 Cond. 1 (5/2007) Solid/Biomass 10 5 60 39.2 10.4 4.2 6.8 IA Monsanto Muscatine #8 Cond. 3 (5/2007) Solid/Biomass 7 5 60 39.8 7.2 1.1 6.5 IA Monsanto Muscatine #8 Cond. 3 (5/2007) Solid/Biomass 8 5 60 39.5 7.4 1.7 4.55 IA Monsanto Muscatine #8 Cond. 3 (5/2007) Solid/Biomass 9 5 60 40.6 7.6 3.45 7.95 IA Monsano Muscatine #8 Cond. 1 (8/2007) Solid/Biomass 1 5 60 41.8 11.9 2.25 6.3 IA Monsano Muscatine #8 Cond. 1 (8/2007) Solid/Biomass 2 5 60 40.4 12.6 1.95 8.75 IA Monsano Muscatine #8 Cond. 1 (8/2007) Solid/Biomass 3 5 60 40.7 11.9 0.95 6.15 ID Amalgamated Suger Co. Twin Falls Solid/Coal 1 5/202 120 77.5 250 6.7 0 5.6 ID Amalgamated Suger Co. Twin Falls Solid/Coal 2 5/202 120 76.9 245 6.67 2 6.9 ID Amalgamated Suger Co. Twin Falls Solid/Coal 3 5/202 120 78.9 245 7.22 1.8 9.3

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028**  IA Monsano Muscatine #8 Cond. 1 (10/2009) Solid/Biomass 1 5/29 240 168.2 10.2 1.65 n/a IA Monsano Muscatine #8 Cond. 1 (10/2009) Solid/Biomass 2 5/29 240 176.7 10.1 3.45 n/a IA Monsano Muscatine #8 Cond. 1 (10/2009) Solid/Biomass 3 5/29 240 169.5 10.4 2.15 n/a IA U of Northern Iowa #3 (10/2009) Solid/Coal 1 29 240 157.2 7 0.5 3.7 IA U of Northern Iowa #3 (10/2009) Solid/Coal 2 29 240 158.0 7.6 0 3.3 IA U of Northern Iowa #3 (10/2009) Solid/Coal 3 29 240 162.2 7.3 0 2 IL PilyOne Boiler 1 (9/2009) Solid/Coal 1 5 240 160.2 250 7.8 0 20.4 IL PilyOne Boiler 1 (9/2009) Solid/Coal 2 5 240 179.0 247 7.7 0 27.1 IL PilyOne Boiler 1 (9/2009) Solid/Coal 3 5 240 172.9 255 7.4 0 61.2 IN Purdue University Boiler 5 (7/2009) Solid/Coal 1 5 240 207.3 6.78 n/a n/a
IN Purdue University Boiler 5 (7/2009) Solid/Coal 2 5 240 204.5 6.91 n/a n/a IN Purdue University Boiler 5 (7/2009) Solid/Coal 3 5 240 200.9 6.8 n/a n/a ME Boralex Stratton Boiler 1 (10/2009) Solid/Biomass 1 5/202 55.6 20.2 240 18.7 n/a n/a 1 ME Boralex Stratton Boiler 1 (10/2009) Solid/Biomass 2 5/202 61.3 20.4 240 18.6 n/a n/a ME Boralex Stratton Boiler 1 (10/2009) Solid/Biomass 3 5/202 63.5 20.3 235 18.2 n/a n/a MI Consumer Energy Co - Campbell (9/2009) liquid 1 MI Consumer Energy Co - Campbell (9/2009) liquid 2 MI Consumer Energy Co - Campbell (9/2009) liquid 3 OH Smart Papers Holdings LLC (10/2005) Solid/Coal 1 5/29 120 84.8 265 7.3 0.1 2.3 OH Smart Papers Holdings LLC (10/2005) Solid/Coal 2 5/29 120 83.2 260 9.6 0.1 1.2 OH Smart Papers Holdings LLC (10/2005) Solid/Coal 3 5/29 120 86.0 261 10 2.35 1 SC GP Chem Russellville (8/2009) liquid/liquid 1 26A 120 104.2 250 10.3 1.1 1.3 SC GP Chem Russellville (8/2009) liquid/liquid 2 26A 120 102.2 250 10.8 1.1 0.7 SC GP Chem Russellville (8/2009) liquid/liquid 3 26A 120 81.8 248 10.6 0.4 1 SC Marlboro Paper (7/2009) Solid/Biomass 1 5/29 180 142.3 256 20.7 4.6 4.6 SC Marlboro Paper (7/2009) Solid/Biomass 2 5/29 180 136.0 252 19.8 6.1 3.9 SC Marlboro Paper (7/2009) Solid/Biomass 3 5/29 180 146.6 252 20.4 5.7 2.5 TN Eastman NO CBI DATA Solid/Coal 1 5/29 225 162.4 260 13.8 14.7 9.9 TN Eastman NO CBI DATA Solid/Coal 2 5/29 225 163.7 260 13.5 4.7 4.5 TN Eastman NO CBI DATA Solid/Coal 3 5/29 225 165.4 260 12.6 2.9 4.7 VADukeEnergyNarrows Boiler 2 Solid/Coal 1 5/26A 60 57.2 3.2 0.6 2.6 VADukeEnergyNarrows Boiler 2 Solid/Coal 2 5/26A 60 45.0 2.6 0.1 2.3 VADukeEnergyNarrows Boiler 2 Solid/Coal 3 5/26A 60 57.1 5 0.7 3.8 VADukeEnergyNarrows Boiler 3 Solid/Coal 1 5/26A 60 42.8 268 7.6 0.1 1.8 VADukeEnergyNarrows Boiler 3 Solid/Coal 2 5/26A 60 45.7 270 7.1 0.1 5.3 VADukeEnergyNarrows Boiler 3 Solid/Coal 3 5/26A 60 43.5 270 8.3 0.6 7.5 VA University of Virginia 7103-1-01R (12/2007) Solid/Coal 1 5/202 60 35.2 257 9.44 0.1 0.9 VA University of Virginia 7103-1-01R (12/2007) Solid/Coal 2 60 35.4 257 9.74 0.3 0.2 1 VA University of Virginia 7103-1-01R (12/2007) Solid/Coal 3 60 33.4 257 8.92 0.1 0.3 1 VA University of Virginia 7103-1-01R Solid/Coal 1 5/29 240 263 VA University of Virginia 7103-1-01R Solid/Coal 2 5/29 240 260 VA University of Virginia 7103-1-01R Solid/Coal 3 5/29 240 264 VA University of Virginia 7103-1-02R Solid/Coal 1 5/202 60 42.7 255 8.9 0.7 4.1 VA University of Virginia 7103-1-02R Solid/Coal 2 5/202 60 41.6 258 8.8 0.1 1.8 VA University of Virginia 7103-1-02R Solid/Coal 3 5/202 60 41.6 258 8.4 0.5 1.6
VA University of Virginia 7103-1-05 Solid/Coal 1 5/202 60 42.4 253 10 0.5 1.86
VA University of Virginia 7103-1-05 Solid/Coal 2 5/202 60 42.7 255 9.4 0.5 1.76 VA University of Virginia 7103-1-05 Solid/Coal 3 5/202 60 42.4 255 10.3 1.9 8.58

WA Grays Harbor Paper (6/2006) Solid/Biomass 1 5/202 60 36.6 245 21.9 175 44.1

WA Grays Harbor Paper (6/2006) Solid/Biomass 2 5/202 60 38.1 250 21.09 179.6 37.5 WA Grays Harbor Paper (6/2006) Solid/Biomass 3 5/202 60 36.7 248 20.54 172 43.5

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028**  AR Potlatch Forest Warren (8/2006) Solid/Biomass 1 5/26A 60 46.3 250 22 1.5 0.5 AR Potlatch Forest Warren (8/2006) Solid/Biomass 2 5/26A 60 45.4 253 20.97 1.2 0 AR Potlatch Forest Warren (8/2006) Solid/Biomass 3 5/26A 60 47.0 250 22.61 1.1 0 AR Potlatch Forest Warren (9/2009) Solid/Biomass 1 5/29 240 204.3 248 21.06 227 19.2 AR Potlatch Forest Warren (9/2009) Solid/Biomass 2 5/29 240 214.1 248 20.23 34.3 4.5 AR Potlatch Forest Warren (9/2009) Solid/Biomass 3 5/29 240 213.8 245 21.47 24.4 2.6 AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) Solid/Biomass 1 5 60 45.2 245 20.65 4.8 1.2 AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) Solid/Biomass 2 5 60 44.7 243 18.9 4.3 1.1 AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) Solid/Biomass 3 5 60 43.8 240 18.93 4.8 0.1 AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) Solid/Biomass 1 5/29 240 193.6 255 17.99

. AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) Solid/Biomass 2 5/29 240 178.9 252 18.99 AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) Solid/Biomass 3 5/29 240 176.5 250 18.79 IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)Solid/Coal 1 5 100 75.5 12.48 0.2 1.6625 IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)Solid/Coal 2 5 100 78.6 11.42 0.1 1.3625 IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)Solid/Coal 3 5 100 77.9 12.97 0.1 1.3 IA Archers Daniels Midland Des Moines Boiler 1 (8/2009)Solid/Coal 1 5/29 240 218.3 250 11.8 0.55 1.4 IA Archers Daniels Midland Des Moines Boiler 1 (8/2009)Solid/Coal 2 5/29 240 214.8 250 12.1 0.4 1.2 IA Archers Daniels Midland Des Moines Boiler 1 (8/2009)Solid/Coal 3 5/29 240 217.4 250 12 0.4 0.95 ID Potlatch (7/2009) Solid/Biomass 1 5/29 240 159.5 260 9.5 6 2.03 ID Potlatch (7/2009) Solid/Biomass 2 5/29 240 170.7 264 9.4 4.7 1.21 ID Potlatch (7/2009) Solid/Biomass 3 5/29 240 161.1 260 9.5 5 1.72 ME New Page-Rumford Cogen #6 and #7(12/2009) Solid/Biomass 1 5/29 240 189.2 250 11.71 2.9 3.1 ME New Page-Rumford Cogen #6 and #7(12/2009) Solid/Biomass 2 5/29 240 185.7 251 11.28 3.5 3 ME New Page-Rumford Cogen #6 and #7(12/2009) Solid/Biomass 3 5/29 240 187.8 250 11.7 4.6 3 MSWeyerhaeuserBruce Boiler 2 (8/2009) Solid/Biomass 1 5/29 180 171.1 255 24.6 24.4 12.8 MSWeyerhaeuserBruce Boiler 2 (8/2009) Solid/Biomass 2 5/29 180 176.4 250 25.5 22.5 23.8 MSWeyerhaeuserBruce Boiler 2 (8/2009) Solid/Biomass 3 5/29 180 174.7 252 25.1 11.7 11.6 ID Riley Creek Lumber Boiler 1/Solid Biomass 1 5 60 40.9 250 0.171 1.6 4.4 ID Riley Creek Lumber Boiler 1/Solid Biomass 2 5 60 40.6 256 0.161 1.1 2.7 ID Riley Creek Lumber Boiler 1/Solid Biomass 3 5 60 40.3 253.5 0.171 0.1 2.8 ID Riley Creek Lumber Boiler 2/Solid Biomass 1 5 60 not reportednot reportednot reported78.6 38.4 ID Riley Creek Lumber Boiler 2/Solid Biomass 2 5 60 not reportednot reportednot reported49 29.4 ID Riley Creek Lumber Boiler 2/Solid Biomass 3 5 60 not reportednot reportednot reported23.5 12.7 ID Tasco Nampa, Riley Boiler Solid/Coal 1 5/26A 60 44.7 260 0.077 6.8 5.5 ID Tasco Nampa, Riley Boiler Solid/Coal 2 5/26A 60 45.9 260 0.0756 6.4 6.4/-0.4 ? ID Tasco Nampa, Riley Boiler Solid/Coal 3 5/26A 60 46.3 258 0.0767 4.9 6.7 ID Tasco Nampa Solid/Coal 1 5 120 89.9 260 0.081 11.3 4.9 ID Tasco Nampa Solid/Coal 2 5 120 94.1 262 0.793 13.4 3.8 ID Tasco Nampa Solid/Coal 3 5 120 94.0 260 0.0396 9.5 3.8 IN Purdue Univ. Unit 5 Solid/Coal (Nov 2006) 1 5 64 45.6 258 0.1113 0.7 7.7 IN Purdue Univ. Unit 5 Solid/Coal (Nov 2006) 2 5 70 45.1 252 0.1108 1.1 1.5 IN Purdue Univ. Unit 5 Solid/Coal (Nov 2006) 3 5 75 45.0 255 0.1153 0.8 0.7 IN Purdue Univ. Unit 5 Solid/Coal (Nov 2008) 1 5 64 42.7 253 0.0572 5.7 9.9 IN Purdue Univ. Unit 5 Solid/Coal (Nov 2008) 2 5 63 44.7 253 0.076 1.8 10.7 IN Purdue Univ. Unit 5 Solid/Coal (Nov 2008) 3 5 63 44.8 253 0.082 1.3 11.1 IN Purdue Univ. Unit 5 Solid/Coal (July 2009) 1 5 287 210.6 0.0605 IN Purdue Univ. Unit 5 Solid/Coal (July 2009) 2 5 259 210.4 0.0645 IN Purdue Univ. Unit 5 Solid/Coal (July 2009) 3 5 250 201.6 0.0619 IN SABIC Plastics Solid/Coal Boiler House 1 (Apr 2005) 1 5/29 121 91.4 265 0.088 540.8 428.1 IN SABIC Plastics Solid/Coal Boiler House 1 (Apr 2005) 2 5/29 121 91.4 267 0.077 672.9 324.7 IN SABIC Plastics Solid/Coal Boiler House 1 (Apr 2005) 3 5/29 121 92.0 261 0.077 669.7 341.3 IN SABIC Plastics Solid/Coal Boiler House 2 (Apr 2005) 1 5/29 123 88.8 256 0.081 0 3.8 IN SABIC Plastics Solid/Coal Boiler House 2 (Apr 2005) 2 5/29 123 92.4 257 0.076 0 2.4 IN SABIC Plastics Solid/Coal Boiler House 2 (Apr 2005) 3 5/29 123 91.3 254 0.085 0 5.9

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028**  IN SABIC Plastics Solid/Coal Boiler House 2 (Jun 2006) 1 5/29 125 91.7 259 0.063 0.1 4.2 IN SABIC Plastics Solid/Coal Boiler House 2 (Jun 2006) 2 5/29 125 89.7 260 0.068 0.1 2.2 IN SABIC Plastics Solid/Coal Boiler House 2 (Jun 2006) 3 5/29 125 86.6 258 0.072 6.8 0.7 LA Port Hudson 100% MCR Biomass/Dry scrubber on (Condition 1) 1 5 64 48.2 253 0.1276 4.1 4.9 LA Port Hudson 100% MCR Biomass/Dry scrubber on 2 5 62 47.5 253 0.1217 11.3 6.2 LA Port Hudson 100% MCR Biomass/Dry scrubber on 3 5 64 47.1 255 0.1239 54 23.4 LA Port Hudson 100% MCP Pet Coke/Dry scrubber on (Condition 4) 1 5 70 41.5 250 0.0816 0.5 3.1 LA Port Hudson 100% MCP Pet Coke/Dry scrubber on 2 5 70 41.7 248 0.081 0.3 2.1 LA Port Hudson 100% MCP Pet Coke/Dry scrubber on 3 5 70 42.0 246 0.0778 0.2 2.6 MI City of Escanaba Solid/Coal Boiler #1 4 5/26A 60 42.7 ? 0.071 34.8 12.3 MI City of Escanaba Solid/Coal Boiler #1 5 5/26A 60 43.3 ? 0.07 39.6 10.9 MI City of Escanaba Solid/Coal Boiler #1 6 5/26A 60 43.8 ? 0.067 36.7 12.8 MN Andersen Corp Bayport Boiler 11 Solid/Biomass (wood fuel) 4/20081 5 60 42.9 263 0.099 -2.5 5.7 5.7
MN Andersen Corp Bayport Boiler 11 Solid/Biomass (wood fuel) 4/20082 5 60 43.1 262 0.1056 -2.8 3.6 3.6
MN Andersen Corp Bayport Boiler 11 Solid/Biomass (wood fuel) 4/20083 5 60 42.4 263 0.0955 -1.2 3.3 3.3
MN Andersen Corp Bayport Boiler 12 Solid/Biomass (wood fuel) 4/20081 5 60 40.0 268 0.1065 -4.5 5.3 5.3
MN Andersen Corp Bayport Boiler 12 Solid/Biomass (wood fuel) 4/20082 5 60 39.6 263 0.1035 -3.3 4.3 4.3
MN Andersen Corp Bayport Boiler 12 Solid/Biomass (wood fuel) 4/20083 5 60 39.0 262 0.1087 -1.8 2.3 2.3
MN Boise Paper 1212 Boiler #2 6/2005 (TPM) 1 5/202 60 36.2 255 0.211 -1.4 25.9 25.9
MN Boise Paper 1212 Boiler #2 6/2005 (TPM) 2 5/202 60 35.1 255 0.224 -0.7 20.5 20.5
MN Boise Paper 1212 Boiler #2 6/2005 (TPM) 3 5/202 60 34.5 257 0.203 -2.1 28.9 28.9 WA Grays Harbor Paper Boiler #6 Solid/Biomass 1 5 240 181.4 256 0.1134457.8 49.33 WA Grays Harbor Paper Boiler #6 Solid/Biomass 2 5 240 144.1 252 0.1301 369 41.01
WA Grays Harbor Paper Boiler #6 Solid/Biomass 3 5 240 188.8 252 0.1056 627 55.72 WA Weyerhaeuser Co. Solid/Biomass 1 5 60 43.4 259 0.1866 -2.7 2.4 WA Weyerhaeuser Co. Solid/Biomass 2 5 60 42.9 255 0.1769 1.6 2.36 WA Weyerhaeuser Co. Solid/Biomass 3 5 60 38.7 258 0.1836 0.6 3.08 WI Domtar 2814 Solid/Biomass 1 5/202 60 37.1 250 0.176 0.7 <1.06 1 WI Domtar 2814 Solid/Biomass 2 5/202 60 36.9 250 0.195 0.3 1.4 WI Domtar 2814 Solid/Biomass 3 5/202 60 34.6 250 0.161 0.5 3 WI GPGreenBay 2818 Boiler #10 Solid/Biomass (1999) 1 5/202 120 60.5 250 0.253not found ? WI GPGreenBay 2818 Boiler #10 Solid/Biomass (1999) 2 5/202 120 63.6 250 0.252 only impinger weights are recorded ? WI GPGreenBay 2818 Boiler #10 Solid/Biomass (1999) 3 5/202 120 64.5 250 0.248 ? WI GPGreenBay 2818 Boiler #10 Solid/Biomass (2007) 1 5 60 50.2 263 0.0611 11.8 3.3 WI GPGreenBay 2818 Boiler #10 Solid/Biomass (2007) 2 5 60 56.1 263 0.0667 11 13.3 WI GPGreenBay 2818 Boiler #10 Solid/Biomass (2007) 3 5 60 57.7 264 0.0512 1.7 6.7 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1992) 1 5 120 100.8 336 0.0696not foundnot found WI GPGreenBay 2818 Boiler #9 Solid/Coal (1992) 2 5 120 102.8 322 0.0673not foundnot found WI GPGreenBay 2818 Boiler #9 Solid/Coal (1992) 3 5 120 106.1 328 0.0688not foundnot found WI GPGreenBay 2818 Boiler #9 Solid/Coal (1999) 1 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1999) 2 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1999) 3 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) 1 5/202 60 35.2 249 0.028 1.4 1.9 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) 2 5/202 60 35.6 251 0.0311 1.2 3.1 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) 3 5/202 60 36.2 252 0.0299 2.2 2.3

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028**  WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) Stack 11 1 5/202 60 47.7 247 0.0381 0.9 3.1 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) Stack 11 2 5/202 60 32.8 251 0.0542 0 2.4 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) Stack 11 3 5/202 60 33.3 249 0.0427 0.2 6.2 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1998) Stack 11 1 5 60 49.4 307 0.0408 2.3 5.8 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1998) Stack 11 2 5 60 50.7 312 0.0408 1.4 0.7 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1998) Stack 11 3 5 60 49.8 313 0.0408 1.1 2.2 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2004) Stack 11 1 5/202 60 38.7 318 0.0465 15 12 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2004) Stack 11 2 5/202 60 37.5 317 0.0404 13.5 26.2 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2004) Stack 11 3 5/202 60 39.6 318 0.0407 15.4 30.9 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2002) Stack 11 1 5/202 60 50.4 323 0.0458 2 8.8 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2002) Stack 11 2 5/202 60 50.1 323 0.0469 4.1 1.9 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2002) Stack 11 3 5/202 60 50.4 323 0.0466 9.5 1.8 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) Stack 11 1 5/202 60 37.7 248 0.0488 1.7 6 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) Stack 11 2 5/202 60 38.0 250 0.0452 3.1 17.3 WI GPGreenBay 2818 Boiler #9 Solid/Coal (2000) Stack 11 3 5/202 60 38.1 250 0.0512 0 1.3 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1994) Stack 11 1 5 120 74.3 ?? 0.0531 2.7 6 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1994) Stack 11 2 5 120 72.8 ? 0.0498 1.5 7.9 WI GPGreenBay 2818 Boiler #9 Solid/Coal (1994) Stack 11 3 5 120 73.3 ? 0.0468 0 9.8 WIGreenBayPackagingMillDivision Boiler B26/Coal fired (2006) 1 5 120 85.1 258 0.063 2.8 0 WIGreenBayPackagingMillDivision Boiler B26/Coal fired (2006) 2 5 120 84.7 249 0.054 0 0.1 1 WIGreenBayPackagingMillDivision Boiler B26/Coal fired (2006) 3 5 120 84.7 250 0.073 1.1 1 WI New Page Biron Boiler 5 Solid/Coal (Sept, 12 2007) 1 5 60 59.2 249 0.058 7.1 0.9 WI New Page Biron Boiler 5 Solid/Coal (Sept, 12 2007) 2 5 60 39.3 254 0.069 3.4 0.1 WI New Page Biron Boiler 5 Solid/Coal (Sept, 12 2007) 3 5 60 36.7 251 0.084 2.9 1 SC Milliken Dewey Plant D30 Liquid/Liquid (2009) 1 29 180 164.1 250 0.12 8 3.3 SC Milliken Dewey Plant D30 Liquid/Liquid (2009) 2 29 180 146.0 249 0.123 1.8 1.6 SC Milliken Dewey Plant D30 Liquid/Liquid (2009) 3 29 180 150.9 250 0.122 1.6 0.9 TN Milan Army Ammunition Plant Boiler D88-L1 Liquid/Liquid (2009) 1 5 216 166.7 247 0.085 0.8 3.9 TN Milan Army Ammunition Plant Boiler D88-L1 Liquid/Liquid (2009) 2 5 216 167.3 244 0.1 0.7 2 TN Milan Army Ammunition Plant Boiler D88-L1 Liquid/Liquid (2009) 3 5 216 168.6 244 0.09 <0.30 2.2 VA GP Big Island 2703 Solid/Coal Boiler 4 (2007) 1 5/29 120 82.3 254 0.076 4.4 6.3 VA GP Big Island 2703 Solid/Coal Boiler 4 (2007) 2 5/29 120 71.6 253 0.089 3.2 4.7 VA GP Big Island 2703 Solid/Coal Boiler 4 (2007) 3 5/29 120 65.7 254 0.098 2.1 5 WA Weyerhaeuser Raymond Solid/Biomass (2009) 1 29 240 not reportednot reported0.1245not reportednot reported WA Weyerhaeuser Raymond Solid/Biomass (2009) 2 29 240 not reportednot reported0.1438not reportednot reported WA Weyerhaeuser Raymond Solid/Biomass (2009) 3 29 240 not reportednot reported0.1434not reportednot reported WI GPGreenBay 2818 Boiler #10 Solid/Biomass (2009) 1 5/29 240 155.6 263 0.2894 WI GPGreenBay 2818 Boiler #10 Solid/Biomass (2009) 2 5/29 240 155.1 263 0.2683 WI GPGreenBay 2818 Boiler #10 Solid/Biomass (2009) 3 5/29 240 147.7 262 0.2965 WI New Page Biron Solid/Coal B24 (2009) 1 5 240 167.0 252 0.095 1.5 2.6 WI New Page Biron Solid/Coal B24 (2009) 2 5 240 149.0 254 0.12 3.1 4.3 WI New Page Biron Solid/Coal B24 (2009) 3 5 240 150.0 254 0.117 3.1 2.6

WI Wausau Solid/Coal (boiler 5) 1 5 60 35.9 250 0.11 <0.3 <1.06 ?

WI Wausau Solid/Coal (boiler 5) 2 5 60 35.8 251 0.075 1.5 1.3

WI Wausau Solid/Coal (boiler 5) 3 5 60 36.8 249 0.089 <0.3 1.6 ?

WV Mountain State Carbon Follansbee S1 Process Gas/ Process Gas 1 5 240 144.3 246 0.201 26 3.8 WV Mountain State Carbon Follansbee S1 Process Gas/ Process Gas 2 5 240 130.9 247 0.207 26.1 0.4 WV Mountain State Carbon Follansbee S1 Process Gas/ Process Gas 3 5 240 131.0 249 0.208 24.1 2.5

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028** 

TN Eastman NO CBI DATA Solid/Coal (11/9/2004) Condition 1 1 5 120 111.2 0.062
TN Eastman NO CBI DATA Solid/Coal (11/9/2004) Condition 1 2 5 120 107.8 0.064 TN Eastman NO CBI DATA Solid/Coal (11/9/2004) Condition 1 3 5 120 101.6 0.065
TN Eastman NO CBI DATA Solid/Coal (11/9/2004) Condition 2 1 5 120 107.2 0.06 TN Eastman NO CBI DATA Solid/Coal (11/9/2004) Condition 2 2 5 120 111.2 0.065 TN Eastman NO CBI DATA Solid/Coal (11/9/2004) Condition 2 3 5 120 103.0 0.067
TN Eastman NO CBI DATA Solid/Coal (6/2004) Voided5 TN Eastman NO CBI DATA Solid/Coal (6/2004) 2 5 60 33.12 250 0.071 1.2 19.8 TN Eastman NO CBI DATA Solid/Coal (6/2004) 3 5 60 33.31 250 0.073 1.3 2.1 TN Eastman NO CBI DATA Solid/Coal (7/2008) 1 5 60 37.9 225 0.076 0.9 5.1 TN Eastman NO CBI DATA Solid/Coal (7/2008) 3 5 60 38.3 225 0.0761 3.4 4 TN Eastman NO CBI DATA Solid/Coal (7/2008) 4 5 60 39.3 226 0.0708 1 9.8 TN Eastman NO CBI DATA Solid/Coal (8/1996) 1 5 64 37.0mislabeled Run 2 (p60)0.0744 10.1 10.3 TN Eastman NO CBI DATA Solid/Coal (8/1996) 2 5 64 37.9 255 0.0761 10.6 3.6 TN Eastman NO CBI DATA Solid/Coal (8/1996) 3 5 64 37.4 256 0.0807 47.5 15.5
TN Eastman NO CBI DATA Solid/Coal (8/2000) 2 5 64 38.9 248 0.0847 7.1 65
TN Eastman NO CBI DATA Solid/Coal (8/2000) 3 5 64 41.5 248 0.085 11.1 16.7 TN Eastman NO CBI DATA Solid/Coal (8/2000) 4 5 64 41.7 248 0.0813 8.9 7.2
TN Eastman NO CBI DATA Solid/Coal (3/2005) 1 5 120
TN Eastman NO CBI DATA Solid/Coal (3/2005) 2 5 120 TN Eastman NO CBI DATA Solid/Coal (3/2005) 3 5 120 TN Eastman NO CBI DATA Solid/Coal (5/2005) 1 5 60 38.9 255 0.0688 0 4 TN Eastman NO CBI DATA Solid/Coal (5/2005) 2 5 60 38.9 255 0.0718 0 7.5 TN Eastman NO CBI DATA Solid/Coal (5/2005) 3 5 60 38.3 260 0.0614 0 3.4 TN Eastman NO CBI DATA Solid/Coal (7/1993) 1 5 64 54.2 255 0.0731 3.3 18.7 TN Eastman NO CBI DATA Solid/Coal (7/1993) 2 5 64 54.1 255 0.0703 2.4 12.3 TN Eastman NO CBI DATA Solid/Coal (7/1993) 3 5 64 53.0 255 0.0725 0 15.2 TN Eastman NO CBI DATA Solid/Coal (8/2001) 1 5 60 39.9 254 0.084 5.1 10.7 TN Eastman NO CBI DATA Solid/Coal (8/2001) 2 5 60 40.9 251 0.0808 1.1 3.9 TN Eastman NO CBI DATA Solid/Coal (8/2001) 3 5 60 39.5 253 0.0845 0.5 5.5 TN Eastman NO CBI DATA Solid/Coal (9/1997) 1 5 64 41.5 251 0.0705 0 15.4 TN Eastman NO CBI DATA Solid/Coal (9/1997) 2 5 64 43.0 248 0.076 2.6 5 TN Eastman NO CBI DATA Solid/Coal (9/1997) 3 5 64 40.3 250 0.0726 0 4.9 TN Eastman NO CBI DATA Solid/Coal (11/8/1994) 1 5 75 50.3 251 0.0905 1.3 15.9 TN Eastman NO CBI DATA Solid/Coal (11/8/1994) 2 5 75 50.9 247 0.0943 3.2 11.2 TN Eastman NO CBI DATA Solid/Coal (11/8/1994) 4 5 75 47.6 250 0.1024 2.8 10.8 TN Eastman NO CBI DATA Solid/Coal (9/2002) 1 5 60 36.5 237 0.125 0.8 6.3 TN Eastman NO CBI DATA Solid/Coal (9/2002) 2 5 60 34.7 227 0.13 0.9 3.8 TN Eastman NO CBI DATA Solid/Coal (9/2002) 4 5 60 34.3 256 0.11 0.5 6.6

TN Eastman NO CBI DATA Solid/Coal (9/2006) 1 5 60 35.9 250 0.1088 0.7 11.2

TN Eastman NO CBI DATA Solid/Coal (9/2006) 2 5 60 35.1 251 0.1076 0.7 14.8 TN Eastman NO CBI DATA Solid/Coal (9/2006) 3 5 60 35.1 254 0.1131 0.5 10.4 TN Eastman NO CBI DATA Solid/Coal (12/1994) 1 5 125 87.3 259 0.1192 17.1 10 TN Eastman NO CBI DATA Solid/Coal (12/1994) 2 5 125 83.5 244 0.1179 0.1 8.8 TN Eastman NO CBI DATA Solid/Coal (12/1994) 3 5 125 83.3 254 0.1142 0 19.3 TN Eastman NO CBI DATA Solid/Coal (12/2006) 1 5 125 94.8 255 0.1102 8.5 6.5 TN Eastman NO CBI DATA Solid/Coal (12/2006) 2 5 125 93.3 256 0.1108 0 8.9 TN Eastman NO CBI DATA Solid/Coal (12/2006) 3 5 125 94.2 257 0.1138 1.9 8.9
TN Eastman NO CBI DATA Solid/Coal (7/2006) 2 5 125 77.6 255 0.128 135.4 34.2
TN Eastman NO CBI DATA Solid/Coal (7/2006) 3 5 125 79.6 263 0.129 31.3 30.8 TN Eastman NO CBI DATA Solid/Coal (7/2006) 4 5 125 81.1 261 0.127 82.9 35.9

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028** 
TN Eastman NO CBI DATA Solid/Coal (8/2006) 1 5 125 73.9 260 0.1283 63.1 44.3 TN Eastman NO CBI DATA Solid/Coal (8/2006) 2 5 125 78.6 255 0.1312 74.5 51 TN Eastman NO CBI DATA Solid/Coal (8/2006) 3 5 125 77.9 252 0.1333 114.1 31.4 TN Eastman NO CBI DATA Solid/Coal (8/1994) 1 5 125 101.8 252 0.1005 0.7 8.6 TN Eastman NO CBI DATA Solid/Coal (8/1994) 2 5 125 97.7 247 0.1104 3.9 4.3 TN Eastman NO CBI DATA Solid/Coal (8/1994) 3 5 125 119.4 230 0.1168 2.3 14.8 TN Eastman NO CBI DATA Solid/Coal (9/1998) 1 5 125 62.7 250 0.1162 10.3 14.6 TN Eastman NO CBI DATA Solid/Coal (9/1998) 2 5 125 64.9 250 0.1192 0 13.6 TN Eastman NO CBI DATA Solid/Coal (9/1998) 3 5 125 66.3 251 0.1186 0 20.7

VA Duke Energy Narrows Solid/Coal (Boiler 3) 1 5/26A 60 45.6 250 0.072 9.7 40.1

VA Duke Energy Narrows Solid/Coal (Boiler 3) 2 5/26A 60 47.0 250 0.075 10.1 20.4 VA Duke Energy Narrows Solid/Coal (Boiler 3) 3 5/26A 60 48.1 249 0.075 VA Duke Energy Narrows Solid/Coal (Boiler 3) 4 5/26A 60 47.3 251 0.067 11.1 23.3 VA Duke Energy Narrows Solid/Coal (Boiler 7) 1 5/26A 60 60.8 251 0.075 38.6 26 VA Duke Energy Narrows Solid/Coal (Boiler 7) 2 5/26A 60 47.3 250 0.077 31.9 37.1 VA Duke Energy Narrows Solid/Coal (Boiler 7) 3 5/26A 60 38.4 251 0.093 33.1 24.8 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (2/2004) 1 5 60 49.1 250 0.122 6.9 3.9 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (2/2004) 2 5 60 52.1 250 0.106 6.4 1.7 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (2/2004) 3 5 60 50.2 2500 0.103 7.7 2.1 VA Georgia Pacific Big Island Solid/Woodwaste Boiler 5 (2/2004) 1 5 60 43.7 257 0.139 7.3 10.4 VA Georgia Pacific Big Island Solid/Woodwaste Boiler 5 (2/2004) 2 5 60 45.3 251 0.14 9.7 14.4 VA Georgia Pacific Big Island Solid/Woodwaste Boiler 5 (2/2004) 3 5 60 48.2 250 0.123 12 13.2 VA Georgia Pacific Big Island Solid/Woodwaste Boiler 5 (3/2009) 1 5 60 VA Georgia Pacific Big Island Solid/Woodwaste Boiler 5 (3/2009) 2 5 60 VA Georgia Pacific Big Island Solid/Woodwaste Boiler 5 (3/2009) 3 5 60 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (3/2009) 1 5 60 55.9 252 0.39 107.7 49.7 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (3/2009) 2 5 60 54.2 252 0.047 94.2 40.6 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (3/2009) 3 5 60 59.7 252 0.04 129.6 46.1 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (4/2009) 1 5 60 22.8 257 0.093 10.6 3.4 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (4/2009) 2 5 60 22.8 253 0.081 2.9 5 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (4/2009) 3 5 60 21.7 254 0.097 2.6 3.8 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (5/2005) 1 5 60 39.6 not found0.133 11.6 7.1 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (5/2005) 2 5 60 38.1 not found0.098 9.5 5.2 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (5/2005) 3 5 60 37.7 not found0.127 9.2 7.4 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (7/2006) 1 5 120 81.3 257 0.078 2.3 8.8 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (7/2006) 2 5 120 78.9 258 0.081 0 7.9 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (7/2006) 3 5 120 79.1 258 0.077 2.3 2.5
VA Georgia Pacific Big Island Solid/Coal Boiler 4 (9/2008) 1 5 48 46.3 258 0.103 16.8 2.5
VA Georgia Pacific Big Island Solid/Coal Boiler 4 (9/2008) 2 5 48 38.0 256 0.123 10 3.6 VA Georgia Pacific Big Island Solid/Coal Boiler 4 (9/2008) 3 5 48 38.3 256 0.095 10 4 Solid/Coal 4 5 48 42.6 253 0.093 10.2 1.4 Solid/Coal 5 5 48 34.4 255 0.073 45 13.7 Solid/Coal 6 5 48 34.6 264 0.071 37.1 18.5 Solid/Coal 1 5 48 37.8 254 0.067 32.3 12.6 Solid/Coal 2 5 48 37.1 253 0.059 28.2 13.2 Solid/Coal 1 5 48 33.5 255 0.061 39.6 15.5 Solid/Coal 2 5 48 32.6 255 0.066 33.5 11.1 WI Thilmany Paper Solid Coal 2/22/2006 1 5 60 51.4 223-273 0.061 2.9 3.6 WI Thilmany Paper Solid Coal 2/22/2006 2 5 60 52.2 223-273 0.063 2.3 0 WI Thilmany Paper Solid Coal 2/22/2006 3 5 60 51.2 223-273 0.057 2.2 1 WI Thilmany Paper Solid Coal 2/23/2006 1 5 60 51.2 223-273 0.06 3.7 1.7 WI Thilmany Paper Solid Coal 2/23/2006 2 5 60 51.8 223-273 0.064 4.2 2.7 WI Thilmany Paper Solid Coal 2/23/2006 3 5 60 52.6 223-273 0.065 3.3 0.7 WA Weyerhaeuser Raymond (11/2004) Solid/Biomass - Fuel Cell 1 5/202 60 60.3 265 15.52 0 1.3 WA Weyerhaeuser Raymond (11/2004) Solid/Biomass - Fuel Cell 2 5/202 60 60.4 262 15.93 0.1 1

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028**  WA Weyerhaeuser Raymond (11/2004) Solid/Biomass - Fuel Cell 3 5/202 60 41.6 16.52 0 6 1 WA Weyerhaeuser Raymond (9/1996) Solid/Biomass - Fuel Cell 1 5 120 90.0 316 15.27 0 4.6 WA Weyerhaeuser Raymond (9/1996) Solid/Biomass - Fuel Cell 2 5 120 87.3 318 16.16 0 3.3 WA Weyerhaeuser Raymond (9/1996) Solid/Biomass - Fuel Cell 3 5 120 78.7 318 14.99 0 4.5 FL US Sugar Corp Boiler 8 (12/2009) Solid/Biomass - Suspension/ Grate 1 5 60 43.9 234 30 7 8.7 FL US Sugar Corp Boiler 8 (12/2009) Solid/Biomass - Suspension/ Grate 2 5 60 42.9 230 29 7.5 4.9 FL US Sugar Corp Boiler 8 (12/2009) Solid/Biomass - Suspension/ Grate 3 5 60 41.4 230 30.2 3.1 3.5

FL US Sugar Corp Boiler 8 (6/2006) Solid/Biomass - Suspension/ Grate 1 5 60 29.1 255 26.73 0.5 3

FL US Sugar Corp Boiler 8 (6/2006) Solid/Biomass - Suspension/ Grate 2 5 60 25.7 253 24.13 0.4 1.5 FL US Sugar Corp Boiler 8 (6/2006) Solid/Biomass - Suspension/ Grate 3 5 60 32.0 255 21.61 0.5 1.1 FL US Sugar Corp Boiler 8 (6/2006) Solid/Biomass - Suspension/ Grate 4 5 60 29.4 255 21.65 0.6 1.2 FL US Sugar Corp Boiler 8 (6/2006) Solid/Biomass - Suspension/ Grate 5 5 60 26.1 253 20.04 0.6 0.9 FL US Sugar Corp Boiler 8 (8/2006) Solid/Biomass - Suspension/ Grate 1 5 64 32.8 254 21.33 2.4 4.4 FL US Sugar Corp Boiler 8 (8/2006) Solid/Biomass - Suspension/ Grate 2 5 64 33.6 253 21.12 7.8 5 FL US Sugar Corp Boiler 8 (8/2006) Solid/Biomass - Suspension/ Grate 3 5 64 33.7 255 20.86 7.6 4.2 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 1 5 60 52.2 258 24.23 4.7 11.3 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 2 5 60 53.7 258 23.85 6.6 6.9 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 3 5 60 53.3 258 24.35 9.9 7.8 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 1 5 60 55.4 265 26.36 3.6 3.9 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 2 5 60 51.7 263 27.44 2.3 3 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 3 5 60 25.4 263 41.86 2.6 3.8 FL US Sugar Corp Boiler 8 (1/2007) Solid/Biomass - Suspension/ Grate 4 5 60 52.4 264 27.33 4.5 2.3 GA GP Madison Ply (10/2004) Solid/Biomass - Stoker/Other 1 5 60 40.4 250 15.11 -0.5 3.1 3.1 GA GP Madison Ply (10/2004) Solid/Biomass - Stoker/Other 2 5 60 39.9 250 15.96 -0.1 3.8 3.8 GA GP Madison Ply (10/2004) Solid/Biomass - Stoker/Other 3 5 60 40.8 253 15.82 -0.4 2.3 2.3 GA GP Madison Ply (6/2006) Solid/Biomass - Stoker/Other 1 5 60 51.7 260 12.26 1.3 4 GA GP Madison Ply (6/2006) Solid/Biomass - Stoker/Other 2 5 60 56.0 258 13.68 2 4.9 GA GP Madison Ply (6/2006) Solid/Biomass - Stoker/Other 3 5 60 57.0 260 13.83 1.9 3.2 GA GP Madison Ply (9/2007) Solid/Biomass - Stoker/Other 1 5 60 39.1 252 14.68 12.5 14.2 GA GP Madison Ply (9/2007) Solid/Biomass - Stoker/Other 2 5 60 35.9 252 10.65 5.9 2.6 GA GP Madison Ply (9/2007) Solid/Biomass - Stoker/Other 3 5 60 37.1 253 14.64 14.9 4.1 GA GP Madison Ply (6/2003) Solid/Biomass - Stoker/Other 1 5 120 84.0 250 15.2 2.5 6.1 GA GP Madison Ply (6/2003) Solid/Biomass - Stoker/Other 2 5 120 80.1 248 15.1 1.3 2.3 GA GP Madison Ply (6/2003) Solid/Biomass - Stoker/Other 3 5 120 72.9 240 15.64 1.1 2.3 GA GP Madison Ply (8/2009) Solid/Biomass - Stoker/Other 1 5/29 240 156.9 252 12.85 4.5 5.4 GA GP Madison Ply (8/2009) Solid/Biomass - Stoker/Other 2 5/29 240 154.1 252 14 0 0.1 1 GA GP Madison Ply (8/2009) Solid/Biomass - Stoker/Other 3 5/29 240 159.9 253 3.77 0.4 5.4 IL Abbott Abbott Park Solid/Coal - Stoker/Other 1 5 60 33.7 255 6.5 9 18.9 IL Abbott Abbott Park Solid/Coal - Stoker/Other 2 5 60 34.0 255 7.6 4.2 11.7 IL Abbott Abbott Park Solid/Coal - Stoker/Other 3 5 60 35.1 255 7.7 3 6.8 MN American Crystal Crookston Boiler 1 (10/2005) Solid/Coal - Stoker/Other 1 5 60 47.3 252 8.4 1.8 1.8 MN American Crystal Crookston Boiler 1 (10/2005) Solid/Coal - Stoker/Other 2 5 60 46.9 252 8.2 1.4 0.9 MN American Crystal Crookston Boiler 1 (10/2005) Solid/Coal - Stoker/Other 3 5 60 45.5 250 8.1 1.9 2.8 OH U of Cincinnati B108 (4/2006) Solid/Coal - Stoker/Other 1 5 OH U of Cincinnati B108 (4/2006) Solid/Coal - Stoker/Other 2 5 OH U of Cincinnati B108 (4/2006) Solid/Coal - Stoker/Other 3 5 SC International Paper Eastover Boiler 1(10/2004) Solid/Coal - PC 1 5 60 37.9 270 10.6 7.6 10 SC International Paper Eastover Boiler 1(10/2004) Solid/Coal - PC 2 5 60 37.7 268 11.5 3.2 3.1

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit Category/ sub-category**  **Run # Method**  **used (5, 17, 26A,**  **29,) Sample time** 

**(min.) Sample** 

**volume (dscf)**  **Filter**

**temperature (avg. deg. f)** **Percent**

**H2O (Bws) Mass - Filter** 

**(mg) Mass - Rinse** 

**(mg) Re-calculated Based** 

**on zero filter for negative values** **Revised Catch**

**based on 64 FR 53028**  SC International Paper Eastover Boiler 1(10/2004) Solid/Coal - PC 3 5 60 39.4 270 11.3 1.4 2.5 SC International Paper Eastover Boiler 1(10/2000) Solid/Coal - PC 1 5 60 38.2 250 8.3 29.7 44.3 SC International Paper Eastover Boiler 1(10/2000) Solid/Coal - PC 2 5 60 38.2 248 12.3 15.1 12.6 SC International Paper Eastover Boiler 1(10/2000) Solid/Coal - PC 3 5 60 39.2 245 13.5 37.1 20.6 SC International Paper Eastover Boiler 1(10/2006) Solid/Coal - PC 1 5 60 39.8 252 10.4 2.2 3 SC International Paper Eastover Boiler 1(10/2006) Solid/Coal - PC 2 5 60 39.9 254 11.3 2.7 3.8 SC International Paper Eastover Boiler 1(10/2006) Solid/Coal - PC 3 5 60 38.9 252 10.2 1.2 0.5 SC International Paper Eastover Boiler 1(10/2002) Solid/Coal - PC 1 5 60 38.6 250 10.4 36.3 8.7 SC International Paper Eastover Boiler 1(10/2002) Solid/Coal - PC 2 5 60 38.2 252 11.6 43.1 12.4 SC International Paper Eastover Boiler 1(10/2002) Solid/Coal - PC 3 5 60 36.9 250 12.1 40.1 2.5 SC International Paper Eastover Boiler 2(10/2002) Solid/Biomass - Stoker/Other 1 5 125 78.4 255 14.8 6.5 5.9 SC International Paper Eastover Boiler 2(10/2002) Solid/Biomass - Stoker/Other 2 5 125 81.0 258 15.6 5.3 3.3 SC International Paper Eastover Boiler 2(10/2002) Solid/Biomass - Stoker/Other 3 5 125 79.9 256 16.4 7 2.7 SC International Paper Eastover Boiler 2(3/2008) Solid/Biomass - Stoker/Other 1 5 125 79.4 244 16 13.2 10.1 SC International Paper Eastover Boiler 2(3/2008) Solid/Biomass - Stoker/Other 2 5 125 82.2 248 16 7 17.3 SC International Paper Eastover Boiler 2(3/2008) Solid/Biomass - Stoker/Other 3 5 125 80.9 246 16 4.6 3.1 SC International Paper Eastover Boiler 2(3/2004) Solid/Biomass - Stoker/Other 1 5 125 82.1 315 20 16 2.6 SC International Paper Eastover Boiler 2(3/2004) Solid/Biomass - Stoker/Other 2 5 125 77.3 315 18 12.1 4.2 SC International Paper Eastover Boiler 2(3/2004) Solid/Biomass - Stoker/Other 3 5 125 75.0 315 20 20.5 5.4 SC International Paper Eastover Boiler 2(6/1999) Solid/Biomass - Stoker/Other 1 5 125 67.9 326 21 1.5 1.8 SC International Paper Eastover Boiler 2(6/1999) Solid/Biomass - Stoker/Other 2 5 125 65.4 325 20 3.9 4.8 SC International Paper Eastover Boiler 2(6/1999) Solid/Biomass - Stoker/Other 3 5 125 66.8 328 20 0.4 5.7 SC International Paper Eastover Boiler 2(6/2003) Solid/Biomass - Stoker/Other 1 5 125 76.2 310 17.1 15.3 10.2 SC International Paper Eastover Boiler 2(6/2003) Solid/Biomass - Stoker/Other 2 5 125 76.9 320 16.4 5.4 9.3 SC International Paper Eastover Boiler 2(6/2003) Solid/Biomass - Stoker/Other 3 5 125 79.2 300 17.9 1 10.6 SC International Paper Eastover Boiler 2(8/1997) Solid/Biomass - Stoker/Other 1 5 125 72.1 22.04 6.7 34.1 SC International Paper Eastover Boiler 2(8/1997) Solid/Biomass - Stoker/Other 2 5 125 23.81 4.8 19.2 SC International Paper Eastover Boiler 2(8/1997) Solid/Biomass - Stoker/Other 3 5 125 24.1 20.3 41 SC International Paper Eastover Boiler 2(8/1995) Solid/Biomass - Stoker/Other 1 5 120 66.2 250 20.6 3.75 7.7 SC International Paper Eastover Boiler 2(8/1995) Solid/Biomass - Stoker/Other 2 5 120 65.1 251 21.4 1.85 7 SC International Paper Eastover Boiler 2(8/1995) Solid/Biomass - Stoker/Other 3 5 120 66.7 255 22 3.6 3.65

SC International Paper Eastover Boiler 2(8/1993)
Solid/Biomass - Stoker/Other 1 5 90 46.9 262 20.4 3.9 104.1

SC International Paper Eastover Boiler 2(8/1993) Solid/Biomass - Stoker/Other 2 5 90 52.6 268 21.1 6.6 50.8 SC International Paper Eastover Boiler 2(8/1993) Solid/Biomass - Stoker/Other 3 5 90 47.0 266 20.3 1.95 40.95 TN Cargill Memphis Boiler 8001(8/2009) Solid/Coal - Stoker/Other 1 5/29 240 169.4 6.7 0.5 2.2 TN Cargill Memphis Boiler 8001(8/2009) Solid/Coal - Stoker/Other 2 5/29 240 172.5 7.2 0.5 2.5 TN Cargill Memphis Boiler 8001(8/2009) Solid/Coal - Stoker/Other 3 5/29 240 158.7 7.4 0.5 1.9 TN Cargill Memphis Boiler 8001(7/2007) Solid/Coal - Stoker/Other 1 5 60 53.1 255 5.5 9.8 11.1 TN Cargill Memphis Boiler 8001(7/2007) Solid/Coal - Stoker/Other 2 5 60 52.4 251 5.5 8.3 9.6 TN Cargill Memphis Boiler 8001(7/2007) Solid/Coal - Stoker/Other 3 5 60 52.5 253 5.7 6.7 7.1

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

AK Doyon Utilities/ Unit 4

AK Doyon Utilities/ Unit 4 AK Doyon Utilities/ Unit 4 AK Doyon Utilities/ Unit 7 AK Doyon Utilities/ Unit 7 AK Doyon Utilities/ Unit 7 AR Weyerhaeuser Dierks Mill / Unit 5 (1997) AR Weyerhaeuser Dierks Mill / Unit 5 (1997) AR Weyerhaeuser Dierks Mill / Unit 5 (1997) AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) FL Smurfit-Stone FL Smurfit-Stone

FL Smurfit-Stone GA GP Monticello Plywood (2/21/08) GA GP Monticello Plywood (2/21/08)
GA GP Monticello Plywood (2/21/08) GA GP Monticello Plywood (2/7/07) GA GP Monticello Plywood (2/7/07)
GA GP Monticello Plywood (2/7/07) IA ADM Corn Processing Cedar Rapids IA ADM Corn Processing Cedar Rapids IA ADM Corn Processing Cedar Rapids IA Iowa State University B1 IA Iowa State University B1 IA Iowa State University B1
IA Iowa State University B2
IA Iowa State University B2
IA Iowa State University B2

IA Monsanto Muscatine #8 Cond. 1 (5/2007) IA Monsanto Muscatine #8 Cond. 1 (5/2007) IA Monsanto Muscatine #8 Cond. 1 (5/2007)
IA Monsanto Muscatine #8 Cond. 3 (5/2007)
IA Monsanto Muscatine #8 Cond. 3 (5/2007) IA Monsanto Muscatine #8 Cond. 3 (5/2007) IA Monsano Muscatine #8 Cond. 1 (8/2007) IA Monsano Muscatine #8 Cond. 1 (8/2007) IA Monsano Muscatine #8 Cond. 1 (8/2007) ID Amalgamated Suger Co. Twin Falls ID Amalgamated Suger Co. Twin Falls ID Amalgamated Suger Co. Twin Falls **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

3.6
7 % O2, 12.8% CO2 100 0.3 0.0020 y y 96.6 y 4.5 6.67 %O2, 13.13%CO2 100 0.3 0.0023 y y 97.5 y 5.1 6.6% O2, 13.2%CO2 100 0.3 0.0027 y y 96.6 y 5.8 7.6% o2, 12.2% CO2 100 0.3 0.0033 y y 95.4 y 7.2 7.93% O2, 12.0% CO2 100 0.3 0.0042 y y 95.5 y 6.5 8.0% O2, 12.0% CO2 100 0.3 0.0040 y y 95.4 y 24.6 9% O2, 10% CO2 100 0.77.200E-03 y y 69.89 19.9 9% O2, 10% CO2 100 0.75.400E-03 y y 99.73 10.4 9% O2, 10% CO2 100 0.73.200E-03 y y 100.11 60.5 6.7% O2, 13.9%CO2 100 0.71.200E-02 0.0243 y y 100.68 25 6.4%O2, 14.0% CO2 100 0.76.500E-03 0.0128 y y 102.23 25.4 6.4% O2, 13.9% CO2 100 0.74.900E-03 0.0097 y y 100.47 4 7.05% O2, 12.5% CO2 100 0.81.360E-03 0.0029 y 93.43 y 2.1 7.29% O2, 12.17% CO2 100 0.87.010E-040.0015 y 95.25 y 7.1 7.41% O2, 12.10% CO2 100 0.82.470E-03 0.0054 y 93.01 y 3.8 10.71% O2, 9.42% CO2 131 1 6.000E-040.0017 y 96.3 y 2.9 10.73% O2, 9.83% CO2 122 1 4.000E-040.0012 y 95.92 y 1.6 11.35% O2, 8.88% CO2 118 0.93.000E-040.0008 y 96.91 y 15 5.89% O2, 14.0% CO2 198 1.52.500E-03 0.0050 101.63 y 21.7 6.80% O2, 13.54% CO2 140 1.13.800E-03 0.0070 101.13 y 15.9 6.44% O2, 14.04% CO2 162 1.22.600E-03 0.0050 99.71 y 4.3 4.5% O2, 15.0% CO2 130 0 1.000E-03 0.0017 y y 1.04 y 8.6 4.5% O2, 15.0% CO2 170 0 2.100E-03 0.0038 y y 1.01 y 2.2 4.5% O2, 15.0% CO2 130 0 5.000E-040.0009 y y 1.02 y 0.7 4.3, 14.6 50 0 0.000E+000.0010 y y 95.6 0.9 3.9, 15.0 65 0 0.000E+000.0010 y y 98.8 1.6 4.4, 14.5 50 0 1.000E-03 0.0010 y y 97.2

0.6 4.0, 14.9 50 0 0.000E+000.0000 y y 98.2 0.7 3.9, 15.0 65 0 0.000E+000.0010 y y 101.2

0.4 3.7, 15.1 50 0 0.000E+000.0000 y y 97
8.55 8.3, 11.8 400 0 3.300E-03 0.0077 y y 98.1 7.55 7.9, 11.6 400 0 2.900E-03 0.0065 y y 99 11 8.3, 11.4 425 0 4.300E-03 0.0102 y y 97.3

7.6 8.3, 11.4 450 0 2.900E-03 0.0067 y y 95.9 6.25 8.1, 11.1 500 0 2.400E-03 0.0055 y y 96.1 11.4 8.3, 11.5 500 0 4.300E-03 0.0099 y y 101.7 8.55 9.3, 11.5 450 0 3.200E-03 0.0080 99.3 10.7 9.0, 11.3 450 0 4.100E-03 0.0101 99.9 7.1 9.0, 11.0 500 0 2.700E-03 0.0067 99.4 5.6 6.9, 9.6 50 0 1.100E-03 y y 103 8.9 6.9, 9.5 55 0 1.800E-03 y y 102 11.1 6.0, 13.5 70 0 2.200E-03 y y 103

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

IA Monsano Muscatine #8 Cond. 1 (10/2009) IA Monsano Muscatine #8 Cond. 1 (10/2009) IA Monsano Muscatine #8 Cond. 1 (10/2009) IA U of Northern Iowa #3 (10/2009) IA U of Northern Iowa #3 (10/2009) IA U of Northern Iowa #3 (10/2009) IL PilyOne Boiler 1 (9/2009) IL PilyOne Boiler 1 (9/2009) IL PilyOne Boiler 1 (9/2009)
IN Purdue University Boiler 5 (7/2009)
IN Purdue University Boiler 5 (7/2009) IN Purdue University Boiler 5 (7/2009) ME Boralex Stratton Boiler 1 (10/2009) ME Boralex Stratton Boiler 1 (10/2009) ME Boralex Stratton Boiler 1 (10/2009) MI Consumer Energy Co - Campbell (9/2009) MI Consumer Energy Co - Campbell (9/2009) MI Consumer Energy Co - Campbell (9/2009) OH Smart Papers Holdings LLC (10/2005) OH Smart Papers Holdings LLC (10/2005) OH Smart Papers Holdings LLC (10/2005) SC GP Chem Russellville (8/2009) SC GP Chem Russellville (8/2009) SC GP Chem Russellville (8/2009) SC Marlboro Paper (7/2009) SC Marlboro Paper (7/2009) SC Marlboro Paper (7/2009) TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA VADukeEnergyNarrows Boiler 2 VADukeEnergyNarrows Boiler 2 VADukeEnergyNarrows Boiler 2 VADukeEnergyNarrows Boiler 3 VADukeEnergyNarrows Boiler 3 VADukeEnergyNarrows Boiler 3 VA University of Virginia 7103-1-01R (12/2007) VA University of Virginia 7103-1-01R (12/2007) VA University of Virginia 7103-1-01R (12/2007) VA University of Virginia 7103-1-01R VA University of Virginia 7103-1-01R VA University of Virginia 7103-1-01R VA University of Virginia 7103-1-02R VA University of Virginia 7103-1-02R VA University of Virginia 7103-1-02R
VA University of Virginia 7103-1-05
VA University of Virginia 7103-1-05 VA University of Virginia 7103-1-05

WA Grays Harbor Paper (6/2006)

WA Grays Harbor Paper (6/2006) WA Grays Harbor Paper (6/2006) **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

1.65 7.00, 11.90 1.510E-040.0003 y y 99.9 3.45 6.80, 12.00 3.010E-040.0007 y y 101 2.15 6.90, 11.80 1.960E-040.0004 y y 100.3 4.2 5.80, 13.40 78 0 4.000E-040.0008 y y 97.3 y 3.3 5.30, 13.80 108 0 3.000E-040.0006 y y 97.8 y 2 6.00, 12.30 95 0 2.000E-040.0004 y y 98.9 y 20.4 8.4, 11.2 0.0046 y 101.9 y 27.1 8.1, 11.5 0.0053 y 102.6 y 61.2 8.3, 11.4 0.0126 y 101.2 y

21.3 4.4, 15 1.590E-03 0.0030 y y 102.2 y 21.1 4.4, 15 1.590E-03 0.0030 y y 102 y 20.2 4.3, 15 1.550E-03 0.0030 y y 102.2 y 0.65 6.3, 14.6 0.000E+000.0010 y y 107.9 y 2.9 5.9, 14.8 0.000E+000.0030 y y 97 y 3.8 5.9, 15.0 0.000E+000.0040 y y 92 y

2.4 7.9, 11.7 4.370E-040.0011 y 94.6 y 1.3 7.8, 11.9 2.410E-040.0005 y 96.1 y 3.4 7.8, 11.9 6.010E-040.0014 y 96.9 y 2.4 8.06, 9.86 85.3 -0.14.000E-040.0008 y y 99.9 y 1.8 7.26, 10.43 84.6 -0.13.000E-040.0005 y y 100.6 y 1.4 7.31, 10.31 84 -0.13.000E-040.0005 y y 100.4 y 9.3 9.74, 11.42 84.36 0.11.000E-03 0.0025 y 98.2 y 10 9.38, 11.73 88.61 0.11.100E-03 0.0027 y 97.3 y 8.2 9.11, 11.97 86.22 0.19.000E-03 0.0020 y 97.4 y 24.6 6.3, 13.2 64 0.0047 y y 99.4 y 9.2 6.3, 13.4 71 0.0017 y y 100.2 y 7.6 6.3, 13.3 83 0.0014 y y 100.1 y 3.2 14.10, 5.60 138 0.19.000E-040.0040 y y 95 y 2.4 12.53, 6.77 135.99 0.18.000E-040.0030 y y 96.9 y 4.5 13.03, 6.63 136.38 0.11.200E-03 0.0040 y y 96.3 y 1.9 7.73, 11.47 139.13 0.17.000E-040.0020 y y 102.3 y 5.4 7.07, 12.17 140.11 0.11.800E-03 0.0040 y y 106.1 y 8.1 9.63, 9.80 130.98 0.12.900E-03 0.0070 y y 102 y 1 7.07, 12.21 140 0 4.000E-040.0009 y y 101 y 0.5 7.03, 12.34 140 0 2.000E-040.0005 y y 103.1 y 0.4 6.98, 12.54 140 0 2.000E-040.0004 y y 96.5 y

4.8 6.64, 12.62 100 0 2.000E-03 0.0040 y y 102 y 1.9 6.96, 12.36 100 0 1.000E-03 0.0010 y y 102.1 y 3.1 6.74, 12.57 110 0 1.000E-03 0.0020 y y 101.9 y

2.36 6.8, 12.8 120 0.949.000E-040.0018 y y 102 y 1.26 7.5, 11.9 120 0.948.000E-040.0018 y y 102.3 y 10.48 8.5, 11.0 130 1.023.800E-03 0.0090 y y 103.2 y

219.1 6.3, 14.5 0.5 120 0.19.200E-02 0.1950 y 217.1 6.9, 13.9 0.5 95 0 9.000E-02 0.1940 y 215.5 7.4, 13.3 0.5 110 0.19.400E-02 0.1960 y

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

AR Potlatch Forest Warren (8/2006) AR Potlatch Forest Warren (8/2006) AR Potlatch Forest Warren (8/2006) AR Potlatch Forest Warren (9/2009) AR Potlatch Forest Warren (9/2009) AR Potlatch Forest Warren (9/2009) AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) IA Archers Daniels Midland Des Moines Boiler 1 (6/2008) IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)
IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)
IA Archers Daniels Midland Des Moines Boiler 1 (8/2009) IA Archers Daniels Midland Des Moines Boiler 1 (8/2009)
IA Archers Daniels Midland Des Moines Boiler 1 (8/2009) ID Potlatch (7/2009) ID Potlatch (7/2009) ID Potlatch (7/2009) ME New Page-Rumford Cogen #6 and #7(12/2009) ME New Page-Rumford Cogen #6 and #7(12/2009) ME New Page-Rumford Cogen #6 and #7(12/2009) MSWeyerhaeuserBruce Boiler 2 (8/2009) MSWeyerhaeuserBruce Boiler 2 (8/2009) MSWeyerhaeuserBruce Boiler 2 (8/2009) ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Tasco Nampa, Riley Boiler ID Tasco Nampa, Riley Boiler ID Tasco Nampa, Riley Boiler ID Tasco Nampa ID Tasco Nampa ID Tasco Nampa IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

2 16.00, 22.00 121 0 7.000E-040.0011 y y 100.06 y 1.2 15.50, 20.97 148 0 4.000E-040.0007 y y 98.24 y 1.1 16.00, 22.61 103 0 4.000E-040.0006 y y 103.78 y 246 4.22, 15.81 0 0.0355 y y 91.37 y 38.8 4.90, 15.12 0 0.0048 y y 96.17 y 27 4.39, 15.60 0 0.0033 y y 93.67 y 5.9 8.07, 12.45 0.001 118 0.16.000E-04 y 100.85 4.2 7.84, 12.50 0.001 158 0.27.000E-04 y 99.86 4.7 7.84, 12.41 0.001 166 0.26.000E-04 y 99.29 17 9.18, 11.79 0.0032 y y 97.62 y 19 9.23, 11.58 0.0039 y y 98.69 y 20 9.33, 11.53 0.0042 y y 98.94 y 1.8625 6.90, 13.00 0.0015 2250.33754.000E-040.0007 y 101.7 y 1.4625 7.90, 12.00 0.0015 2250.33753.000E-040.0006 y 100.5 y 1.4 7.90, 12.00 0.0015 200 0.33.000E-040.0005 y 104.1 y 1.95 5.58, 14.24 0 100 0 <.0001 <.00025 y y 100.2 y 1.6 5.56, 14.11 0 100 0 <.0001 <.00021 y y 96.7 y 1.35 5.66, 14.29 0 100 0 <.0001 <.00017 y y 103.6 y 8.03 13.2, 7.1 0.0031 86 0.278.000E-040.0028 y y 97 y 5.91 13.8, 6.7 0.0031 92 0.295.000E-040.0021 y y 100 y 6.72 13.0, 7.5 0.0031 91 0.286.000E-040.0023 y y 98 y 6 7.5, 12.2 0 36 0 5.000E-040.0010 y y 102.3 y 6.5 7.6, 12.2 0 68 0 5.000E-040.0010 y y 99.6 y 7.6 7.7, 12.0 0 95 0 6.000E-040.0020 y y 101.5 y 37.2 8.06, 12.51 0.0008 85.5 -0.13.300E-03 0.0074 y y 99.6 y 46.3 7.25, 13.24 0.0008 86.7 -0.14.000E-03 0.0084 y y 102.4 y 23.3 7.63, 12.80 0.0008 84.9 -0.12.100E-03 0.0044 y y 100.7 y 6 8% O2 0.001 150 0.22.700E-03 0.2200 Y N Y N 3.8 8% O2 0.001 150 0.21.600E-03 0.1400 Y N Y N 2.9 8% O2 0.001 150 0.21.300E-03 0.1100 Y N Y N 117 8% O2 0.001 150 0.25.370E-02 5.3900 Y N Y N 78.4 8% O2 0.001 150 0.23.940E-024.0000 Y N Y N 36.2 8% O2 0.001 150 0.21.800E-02 1.8200 Y N Y N 12.3 8% O2 0 75 0 3.800E-03 2.1200 Y N Y N 6.4 8% O2 0 100/75 0 1.900E-03 1.0900 Y Y 11.6 8% O2 0 95 0 3.200E-03 1.9900 Y Y 16.2 8% O2 0 100 0 2.400E-03 1.4000 Y Y 17.2 8% O2 0 100 0 2.400E-03 1.4300 Y Y 13.3 8% O2 0 100 0 1.800E-03 1.1600 Y Y 8.2 not reported 0.001 150 0.22.780E-03 1.4200 Y N y Y 2.5 not reported 0.001 130 0.18.570E-040.4300 Y N y Y 1.4 not reported 0.001 55 0.14.810E-040.2400 Y N y Y 15.3 not reported 0.002 128.3 0.35.530E-03 2.7800 Y y 12.3 not reported 0.002 113.5 0.24.250E-03 2.2100 y 12.1 not reported 0.002 115.8 0.24.170E-03 2.1400 y

1.590E-03 0.8900 y 1.590E-03 0.8800 y 1.550E-03 0.8400 y 968.9 0.07 170 0 1.637E-01130.4150 y y 997.6 0.07 155 0 1.684E-01134.9410 y y 1011 0.07 165 0 1.697E-01137.0540 y y 3.8 0.07 100 0 7.000E-040.7010 y y 2.4 0.07 84 0 4.000E-040.4450 y y 5.9 0.07 69 0 1.000E-03 1.0930 y y

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics LA Port Hudson LA Port Hudson LA Port Hudson LA Port Hudson LA Port Hudson LA Port Hudson MI City of Escanaba MI City of Escanaba MI City of Escanaba MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Boise Paper 1212
MN Boise Paper 1212
MN Boise Paper 1212 WA Grays Harbor Paper WA Grays Harbor Paper
WA Grays Harbor Paper WA Weyerhaeuser Co. WA Weyerhaeuser Co. WA Weyerhaeuser Co. WI Domtar 2814 WI Domtar 2814 WI Domtar 2814 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

4.1 ? 0.00333333360 0.27.000E-040.8310 y y y 2.2 ? 0.00270270337 0.14.000E-040.4440 y y y 7.2 ? 0.00392156951 0.21.300E-03 1.4700 y y y 9 0.07 0 414 0 2.500E-03 6.8000 y y y 17.5 0.07 0 392 0 4.900E-0314.1000 y y y 77.4 0.07 0 396 0 1.970E-0257.2000 y y y 3.6 0.07 0 323 0 1.200E-03 3.1960 y y y 2.4 0.07 0 311 0 1.200E-03 3.2170 y y y 2.8 0.07 0 314 0 1.200E-03 3.2540 y y y 47.1 ? 0 ? 0 1.700E-02 7.3800 y y y 50.5 ? 0 ? 0 1.800E-02 7.8700 y y y 49.5 ? 0 ? 0 1.740E-02 7.7700 y y y 5.7 0 65 0 1.150E-03 0.1360 y y y 3.6 0 70 0 2.900E-040.0330 y y y 3.3 0 60 0 7.600E-040.0890 y y y 5.3 0 60 0 3.100E-040.0330 y y y 4.3 0 60 0 3.900E-040.0420 y y y 2.3 0 50 0 2.000E-040.0210 y y y 24.5 0.000238095840 0.1+0.1 (organic + inorganic condensibles) 0.0098 (0.0003)6.6 (0.2) y y y 19.8 0.000235294850 0.1+0.1 (organic + inorganic condensibles) 0.0112 (0.0009)6.4 (0.6) y y y 26.8 0.000236686845 0.1+0.1 (organic + inorganic condensibles) 0.012 (0.0015)7.5 (1.0) y y y 507 0.07 0.00135 123 0.179.520E-0220.8000 ALT-009 was used - Meter box 8 didn't pass. Meter box 3 was used here. y 409.84 0.07 0.00135 103 0.178.240E-0216.7000 ALT-009 was used - Meter box 8 didn't pass. Meter box 3 was used here. y 682.55 0.07 0.00135200 0.171.292E-0127.8000 ALT-009 was used - Meter box 8 didn't pass. Meter box 3 was used here. y 2.4 0.07 0 85 0 9.000E-04 1.5400 y y 0.4 0.07 0 94 0 1.500E-03 2.4800 y y 3.7 0.07 0 95 0 1.500E-03 2.3300 y y 0.7 7% 12% 0 125 0 8.300E-03 2.8000 y y 1.7 7% 12% 0 150 0 7.800E-03 2.5000 y y 3.5 7% 12% 0 150 0 1.100E-02 3.5000 y y

both, so there are two sets of results. ? ? ?0.00047, 0.000410.0900 y y (7% O2, 12%CO2) ? ? ?0.00063, 0.000540.1200 y y (7% O2, 12%CO2) ? ? ?0.00046, 0.000390.0800 y y 15.1 ? 0.00666666730 0.24.900E-0313.0300 y y y y 23.3 ? 0.00806451662 0.56.800E-0320.8700 y y y y 8.4 ? 0.00806451662 0.52.300E-03 7.1400 y y y y not found not found not foundnot foundnot found5.000E-03 5.1200 ynot foundnot foundnot found not found not found not foundnot foundnot found7.000E-03 6.4000 ynot foundnot foundnot found not found not found not foundnot foundnot found7.000E-03 6.6100 ynot foundnot foundnot found

3.3 both 0.001 100 0.11.700E-03 1.7500 ytwo points during run 1 were <90% y 4.3 both 0.0008 125 0.12.150E-03 2.2300 y y y 4.5 both 0.001 100 0.12.100E-03 2.2100 y y y

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WIGreenBayPackagingMillDivision WIGreenBayPackagingMillDivision WIGreenBayPackagingMillDivision WI New Page Biron WI New Page Biron WI New Page Biron SC Milliken Dewey Plant SC Milliken Dewey Plant SC Milliken Dewey Plant TN Milan Army Ammunition Plant TN Milan Army Ammunition Plant TN Milan Army Ammunition Plant VA GP Big Island 2703 VA GP Big Island 2703 VA GP Big Island 2703 WA Weyerhaeuser Raymond WA Weyerhaeuser Raymond WA Weyerhaeuser Raymond WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI New Page Biron WI New Page Biron WI New Page Biron

WI Wausau

WI Wausau

WI Wausau

WV Mountain State Carbon Follansbee WV Mountain State Carbon Follansbee WV Mountain State Carbon Follansbee **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

4 both 0.0024 125 0.31.300E-03 1.6300 y y no way to tell b'c of bad sample calcs 2.4 both 0.0024 125 0.31.100E-03 1.4000 y y no way to tell b'c of bad sample calcs 6.4 both 0.0024 125 0.33.000E-03 3.7400 y y no way to tell b'c of bad sample calcs
8.1 not found 0.008421053190 1.61.500E-03 1.4900 y y 2.1 not found 0.008247423194 1.62.400E-03 2.4200 y y 3.3 not found 0.008695652184 1.63.800E-03 3.9000 y y 28.36% and 12.46%? (pg 95)0.000877193114 0.11.182E-02 9.0460 y not found 39.4 6% and 12.46%? 0.001 200 0.21.686E-0212.8480 y not found 46.8 6% and 12.46%?0.000851064235 0.21.902E-0214.8990 y not found 10.3 not found 0 158 0 3.000E-03 3.2500 0.967 y 9.6 not found 0 120 0 3.000E-03 3.0500 0.967 y 14.4 not found 0 154 0 4.000E-03 4.6100 0.967 y 7.7 both 0.001 100 0.13.100E-03 4.4200 y y 20.4 both 0.001 100 0.18.300E-0311.7000 y y 1.3 both 0.001 100 0.15.000E-040.7400 y y 8.7 ? 0 90 0 6.600E-03 6.8000 y n y 9.4 ? 0 70 0 5.600E-03 5.5600 y n y 9.8 ? 0 100 0 1.290E-0213.1300 y n y 2.8 ? 0 90 0 5.000E-040.2000 y y 0.1 ? 0 75 0 2.000E-05 0.0070 y y 2.1 ? 0 55 0 4.000E-040.1510 y y 8 y 0 95 0 2.100E-03 2.2890 y y y 3.5 y 0 55 0 1.400E-03 1.4740 y y y 3.9 y 0 76 0 1.600E-03 1.6990 y y y 11.3 ? not found0 1.100E-03 0.0139 y y y 3.4 ? not found0 4.000E-040.0051 y y y 2.4 ? not found0.13.000E-040.0037 y y y 4.7 0 72.8 0 ? 0.0007 y y y 2.7 0 33.8 0 ? 0.0004 y y y 2.2 0 57 0 ? 0.0004 y y y 10.7 0 96 0 2.000E-03 1.2040 y y 7.9 0 96 0 1.700E-03 0.8800 y y 7.1 0 90 0 1.700E-03 0.7990 y y not reported 7% O2 not reportednot reportednot reported7.300E-040.0900not reportedynot reported not reported 7% O2 not reportednot reportednot reported8.500E-040.1090not reportedynot reported not reported 7% O2 not reportednot reportednot reported2.700E-040.0370not reportedynot reported 4.2 7% O2 not foundnot foundnot found4.200E-040.0910 y y 5.8 7% O2 not foundnot foundnot found5.800E-040.1280 y y 5.4 7% O2 not foundnot foundnot found5.600E-040.1200 y y 4.1 not foundnot found, assume 054not found, assume 0 .000E+000.4049not found y 7.4 not foundnot found, assume 063not found, assume 0 1.000E-03 0.7338not found y 5.7 not foundnot found, assume 079not found, assume 0 1.000E-03 0.5657not found y

<1.06 0 50 0 <0.0004560.0008 y y

2.8 0 75 0 1.210E-03 0.0016 y y 1.6 0 500.3 was treated as 0. 6.700E-040.0013 y y 29.8 ? 0 265 0 3.180E-03 0.4120 y y 26.5 ? 0 260 0 3.120E-03 0.3680 y y 26.6 ? 0 255 0 3.130E-03 0.3730 y y

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA

TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

6.000E-040.8800 y

1.100E+011.5500 y 9.000E-04 1.2200 y

4.000E-040.5200 y 7.000E-040.9600 y 2.000E-040.2600 y

2.210E-0222.2400 21 0.07 0.003 200 0.69.800E-0311.3000 y y y 3.4 0.07 0.003 200 0.61.600E-03 1.7800 y y y 6 0.07 0.0005 200 0.12.300E-03 2.5800 y y y 7.4 0.07 0.0005 200 0.12.800E-03 3.1600 y y y 10.8 0.07 0.0005 200 0.14.100E-03 4.6300 y y y 20.4 both 0 250 0 8.000E-0310.0900 y y y 14.2 both 0 250 0 5.300E-03 6.8000 y y y 63 both 0 250 0 2.350E-0230.5900 y y y 72.1 0.07 0 200 0 2.820E-0235.4100 y y y 27.8 0.07 0 200 0 1.030E-0213.6500 y y y 16.1 0.07 0 200 0 6.000E-03 7.9200 y y y 0.74 cond. 1 average
1.07 cond. 2 average

4 0.07 0.0005 200 0.11.600E-03 1.6800 y y y 7.5 0.07 0.0005 200 0.13.000E-03 3.1000 y y y 3.4 0.07 0.0005 200 0.11.400E-03 1.4500 y y y 22.3 0.07 0 100 0 8.500E-03 8.9100 y y y 14.7 0.07 0 100 0 4.300E-03 5.7900 y y y 18.2 0.07 0 100 0 6.700E-03 7.2300 y y y 15.8 0.07 0.0005 200 0.16.100E-03 6.4600 y y y 5 0.07 0.0005 200 0.11.900E-03 2.0300 y y y 6 0.07 0.0005 200 0.12.200E-03 2.4300 y y y 15.4 0.07 0 200 0 5.730E-03 5.8400 y y y 7.6 0.07 0 200 0 2.730E-03 2.9400 y y y 4.9 0.07 0 200 0 1.880E-03 1.9300 y y y 13.4 0.07 0.038 100 3.83.900E-03 7.2300 y y y 10.6 0.07 0.038 100 3.83.000E-03 5.6300 y y y 10 0.07 0.036 100 3.63.200E-03 5.5100 y y y 7.1 0.07 0 200 0 3.000E-03 4.3100 y y y 4.7 0.07 0 200 0 2.100E-03 2.9500 y y y 7.1 0.07 0 200 0 3.200E-03 4.5400 y y y

11.9 0.07 0 200 0 4.900E-03 7.8500 y y y 15.5 0.07 0 200 0 6.600E-0310.4700 y y y 10.9 0.07 0 200 0 4.600E-03 7.2400 y y y 27.1 0.07 0 155 0 4.100E-03 6.2700 y y y 8.9 0.07 0 100 0 1.400E-03 2.1500 y y y 19.3 0.07 0 100 0 3.100E-03 4.7200 y y y 15 0.07 0.002 200 0.42.100E-03 3.1900 y y y 8.9 0.07 0.002 200 0.41.300E-03 1.9200 y y y 10.8 0.07 0.002 200 0.41.600E-03 2.3200 y y y 169.6 0.07 0 200 0 3.370E-0245.3800 y y y 62.1 0.07 0 200 0 3.120E-0116.1600 y y y 118.8 0.07 0 200 0 2.260E-0230.8500 y y y

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA

VA Duke Energy Narrows

VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island
VA Georgia Pacific Big Island
VA Georgia Pacific Big Island VA Georgia Pacific Big Island

WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WA Weyerhaeuser Raymond (11/2004) WA Weyerhaeuser Raymond (11/2004) **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

107.4 0.07 0 200 0 2.090E-0229.8700 y y y 125.5 0.07 0 200 0 2.280E-0233.2400 y y y 145.5 0.07 0 200 0 2.710E-0238.8500 y y y 8.9 0.07 0.002666667150 0.41.300E-03 4.7100 y y y 7.8 0.07 0.002666667150 0.41.200E-03 4.1100 y y y 17.5 0.07 0.002666667150 0.42.300E-03 8.9800 y y y 24.9 0.07 0 200 0 6.130E-03 5.8600 y y y 13.6 0.07 0 200 0 3.240E-03 3.1600 y y y 20.7 0.07 0 200 0 4.820E-03 4.8200 y y y

49.8 not found 0 150 0 1.680E-02 6.1600 y y y y 30.5 not found 0 150 0 1.000E-02 3.9100 y y y y

- not found

- - y y y y 34.4 not found 0 150 0 1.120E-024.3600 y y y y 64.6 not found 0 150 0 1.640E-0212.8000 y y y y 69 not found 0 150 0 2.240E-0221.4500 y y y y 57.9 not found 0 150 0 2.320E-0217.7400 y y y y 10.7 not found 0.01333333330 0.43.400E-03 2.0760not foundy y 8.1 not found 0.0125 40 0.52.400E-03 1.5180not foundy y 9.8 not found 0.01333333330 0.43.000E-03 1.8860not foundy y 17.7 not found 0.015 20 0.36.300E-03 4.5560not foundy y 24.1 not found 0.01333333330 0.48.200E-03 5.8600not foundn y 25.2 not found 0.0125 40 0.58.100E-03 5.8860not foundn y

157.3 not found 0.00208333348 0.14.340E-0225.4460 y y 134.8 not found 0.00322580662 0.23.840E-0223.9720 y y 175.7 not found 0.00307692365 0.24.540E-0228.4080 y y 14 not found 0.00833333348 0.45.700E-03 3.0820 y y 7.9 not found 0.0095238142 0.43.400E-03 1.4750 y y 6.5 not found 0.00925925954 0.52.800E-03 1.2060 y y 18.7 not found 0 200 0 7.290E-03 4.0900 y y 14.7 not found 0 200 0 5.960E-03 3.4200 y y 16.7 not found 0 210 0 6.830E-03 3.7500 y y 11.1 not found not reportednot reportednot reported2.100E-03 0.9860 y y y 7.9 not found not reportednot reportednot reported1.500E-03 0.7040 y y y 4.8 not found not reportednot reportednot reported9.000E-040.4250 y y y

19.3 not found 0.0095238142 0.46.400E-03 4.5030 y y y 13.6 not found 0.00930232643 0.45.500E-03 3.7510 y y y 14 not found 0.01 40 0.45.600E-03 3.7220 y y y 11.5 not found 0.00975609841 0.44.200E-03 2.8400 y y y 58.7 not found 0.00909090944 0.42.630E-0215.8010 y y y 55.5 not found 0.0095238142 0.42.470E-0216.1250 y y n 44.9 not found 0.0095238142 0.41.830E-0211.9420 y y y 41.4 not found 0.00930232643 0.41.720E-0211.3380 y y y 55.1 not found 0.0095238142 0.42.530E-0212.2110 y y y 44.6 not found 0.00930232643 0.42.110E-02 9.9600 y y y 6.5 not found 0 30 0not reported0.8134 y y y 2.3 not found 0 30 0not reported0.2884 y y y 3.2 not found 0 38 0not reported0.4033 y y y 5.4 not found 0 18 0not reported0.6797 y y y 6.9 not found 0 23 0not reported0.8644 y y y 4 not found 0 38 0not reported0.5000 y y y 1.3 9.5, 11.4 0 120 0 3.000E-040.0100 y y 97 1.1 9.3, 11.4 0 120 0 3.000E-040.0030 y y 98

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

WA Weyerhaeuser Raymond (11/2004) WA Weyerhaeuser Raymond (9/1996) WA Weyerhaeuser Raymond (9/1996) WA Weyerhaeuser Raymond (9/1996) FL US Sugar Corp Boiler 8 (12/2009) FL US Sugar Corp Boiler 8 (12/2009) FL US Sugar Corp Boiler 8 (12/2009)

FL US Sugar Corp Boiler 8 (6/2006)

FL US Sugar Corp Boiler 8 (6/2006) FL US Sugar Corp Boiler 8 (6/2006) FL US Sugar Corp Boiler 8 (6/2006) FL US Sugar Corp Boiler 8 (6/2006)
FL US Sugar Corp Boiler 8 (8/2006)
FL US Sugar Corp Boiler 8 (8/2006) FL US Sugar Corp Boiler 8 (8/2006)
FL US Sugar Corp Boiler 8 (1/2007)
FL US Sugar Corp Boiler 8 (1/2007) FL US Sugar Corp Boiler 8 (1/2007)
FL US Sugar Corp Boiler 8 (1/2007)
FL US Sugar Corp Boiler 8 (1/2007) FL US Sugar Corp Boiler 8 (1/2007) FL US Sugar Corp Boiler 8 (1/2007) GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) GA GP Madison Ply (6/2006) GA GP Madison Ply (6/2006) GA GP Madison Ply (6/2006) GA GP Madison Ply (9/2007) GA GP Madison Ply (9/2007) GA GP Madison Ply (9/2007) GA GP Madison Ply (6/2003) GA GP Madison Ply (6/2003) GA GP Madison Ply (6/2003) GA GP Madison Ply (8/2009) GA GP Madison Ply (8/2009) GA GP Madison Ply (8/2009) IL Abbott Abbott Park IL Abbott Abbott Park IL Abbott Abbott Park MN American Crystal Crookston Boiler 1 (10/2005) MN American Crystal Crookston Boiler 1 (10/2005) MN American Crystal Crookston Boiler 1 (10/2005) OH U of Cincinnati B108 (4/2006) OH U of Cincinnati B108 (4/2006) OH U of Cincinnati B108 (4/2006) SC International Paper Eastover Boiler 1(10/2004) SC International Paper Eastover Boiler 1(10/2004) **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

0.6 8.7, 11.9 0 110 0 2.000E-040.0040 101 4.6 10.7, 10.2 0 140 0 8.000E-040.0040 y y 106 3.3 10.6, 10.3 0 118 0 9.000E-040.0030 y y 103 4.5 9.4, 11.4 0 130 0 9.000E-040.0030 y y 101
15.6 6.4, 14.4 0 0 5.000E-03 0.0100 y y 104.5 y 12.4 7.0, 13.5 0 0 4.000E-03 0.0080 y y 100.7 y 6.6 5.6, 14.9 0 0 2.000E-03 0.0040 y y 100.7 y

3.5
7.58, 13.18 0.0053 160 0 1.900E-03 0.0041 y y 109.95 1.9 7.99, 12.67 0.0053 175 0 1.100E-03 0.0025 y y 104.1 1.6 9.22, 11.23 0.0053 165 0 8.000E-040.0019 y y 98.27 1.8 9.84, 10.63 0.0053 190 0 9.000E-040.0026 y y 94.96 1.5 9.10, 11.40 0.0053 150 0 9.000E-040.0022 y y 102.7

6.8 10.36, 10.03 0.015 100 0 3.200E-03 0.0101 y 93.17 12.8 10.43, 10.03 0.015 100 0 5.900E-03 0.0193 y 96.79 11.8 10.3, 9.89 0.015 100 0 5.400E-03 0.0167 y 95.71

15 7.73, 12.78 0.014 110 0 4.700E-03 0.0117 y 100.02 13.5 7.65, 12.71 0.014 95 0 3.900E-03 0.0094 y 99.95 17.7 7.25, 13.17 0.014 125 0 5.100E-03 0.0122 y 101.98

7.5 6.52, 14.44 0.004 130 0 0.0040 y y 102.27 y 5.3 6.96, 14.09 0.004 120 0 0.0030 y y 103.02 y 6.4 0.004 140 0 y y y 6.8 6.53, 14.57 0.004 110 0 0.0040 y y 104.6 y 2.6 8.82, 11.68 177 0 1.000E-03 0.0020 y y 96.45 y 3.7 8.76, 11.83 165 0 1.500E-03 0.0030 y y 100.52 y 1.9 9.06, 11.42 175 0 7.000E-040.0020 y y 100.8 y 5.3 7.75, 12.59 160 0 1.600E-03 0.0033 y y 100.37 y 6.9 8.13, 12.38 120 0 1.900E-03 0.0042 y y 102.18 y 5.1 8.46, 12.10 130 0 1.400E-03 0.0032 y y 102.05 y 26.7 7.35, 12.0 150 0 1.050E-02 0.0215 y y 99.3 y 8.5 6.60, 12.5 125 0 3.600E-03 0.0071 y y 97.85 y 19 7.51, 12.0 125 0 7.900E-03 0.0164 y y 95.96 y 8.6 9.78, 10.85 350 0 1.600E-03 0.0040 y y 95.27 y 3.6 9.55, 11.06 275 0 7.000E-040.0020 y y 95.44 y 3.4 7.91, 12.64 275 0 7.000E-040.0020 y y 97.39 y 9.9 8.88, 11.52 100 0 y y 98.3 0.1 8.21, 12.04 100 0 y y 102.9 5.8 7.21, 12.79 100 0 y y 92.1 27.9 9.93, 10.90 4.9 0 1.270E-02 0.0340 y y 100.2 y 15.9 9.77, 9.34 4.9 0 7.200E-03 0.0190 y y 101.4 y 9.8 9.61, 10.04 4.9 0 4.300E-03 0.0110 y y 102.5 y 3.6 11.5, 9.0 150 0 1.200E-03 0.0037 y y 100.5 2.3 11.5, 9.0 150 0 8.000E-040.0024 y y 101 4.7 11.5, 9.0 150 0 1.600E-03 0.0050 y y 99.6

17.6 5.60, 13.50 0 7.200E-03 0.0137 y y 99.9 y 6.3 5.90, 13.20 0 2.600E-03 0.0051 y y 100.7 y

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

SC International Paper Eastover Boiler 1(10/2004) SC International Paper Eastover Boiler 1(10/2000) SC International Paper Eastover Boiler 1(10/2000) SC International Paper Eastover Boiler 1(10/2000) SC International Paper Eastover Boiler 1(10/2006) SC International Paper Eastover Boiler 1(10/2006) SC International Paper Eastover Boiler 1(10/2006) SC International Paper Eastover Boiler 1(10/2002) SC International Paper Eastover Boiler 1(10/2002) SC International Paper Eastover Boiler 1(10/2002) SC International Paper Eastover Boiler 2(10/2002) SC International Paper Eastover Boiler 2(10/2002) SC International Paper Eastover Boiler 2(10/2002) SC International Paper Eastover Boiler 2(3/2008) SC International Paper Eastover Boiler 2(3/2008) SC International Paper Eastover Boiler 2(3/2008) SC International Paper Eastover Boiler 2(3/2004) SC International Paper Eastover Boiler 2(3/2004) SC International Paper Eastover Boiler 2(3/2004) SC International Paper Eastover Boiler 2(6/1999) SC International Paper Eastover Boiler 2(6/1999) SC International Paper Eastover Boiler 2(6/1999) SC International Paper Eastover Boiler 2(6/2003) SC International Paper Eastover Boiler 2(6/2003) SC International Paper Eastover Boiler 2(6/2003) SC International Paper Eastover Boiler 2(8/1997) SC International Paper Eastover Boiler 2(8/1997) SC International Paper Eastover Boiler 2(8/1997) SC International Paper Eastover Boiler 2(8/1995) SC International Paper Eastover Boiler 2(8/1995) SC International Paper Eastover Boiler 2(8/1995)

SC International Paper Eastover Boiler 2(8/1993)

SC International Paper Eastover Boiler 2(8/1993) SC International Paper Eastover Boiler 2(8/1993) TN Cargill Memphis Boiler 8001(8/2009) TN Cargill Memphis Boiler 8001(8/2009) TN Cargill Memphis Boiler 8001(8/2009) TN Cargill Memphis Boiler 8001(7/2007) TN Cargill Memphis Boiler 8001(7/2007) TN Cargill Memphis Boiler 8001(7/2007) **Mass Total (mg) Diluent correction (7%**  **O2? 12% CO2?) Reagent** 

**blank value (mg/ml)** **Total**

**reagent used (ml)** **Blank**

**correction value** **Reported**

**Gr/dscf Reported** 

**Mass/Unit (lbs/mmbtu)** **Meter cal**

**y/n Leak check** 

**y/n Iso Check** 

**y/n Nozzle**  **check y/n**

3.9 5.40, 13.70 0 1.500E-03 0.0028 y y 100.7 y 74 6.0, 13.0 152 0.33.000E-02 0.0590 y y 99 y 27.7 6.1, 13.0 111 0.21.100E-02 0.0220 y y 105 y 57.7 5.9, 13.2 94 0.22.300E-02 0.0440 y y 106 y 5.2 3.2, 15.1 0 2.000E-03 0.0033 y y 100.3 y 6.5 3.6, 17.0 0 2.500E-03 0.0042 y y 101.6 y 1.7 3.8, 17.1 0 7.000E-040.0012 y y 100.6 y 45 6.1, 13.3 0.0044 68 0.61.800E-02 0.0360 y y 99 y 55.5 3.1, 13.3 0.0044 74 0.62.200E-02 0.0440 y y 98 y 42.6 5.8, 13.4 0.0044 38 0.51.800E-02 0.0340 y y 99 y 12.4 7.66, 12.62 0.0052 88.2 0.52.500E-03 0.0053 y y 97.7 y 8.6 7.67, 12.61 0.0052102.3 0.51.600E-03 0.0034 y y 100.6 y 9.7 7.48, 13.26 0.0052 78.6 0.51.900E-03 0.0040 y y 101.2 y 23.3 10.1, 10.3 0.0005 130 -0.14.500E-03 0.0118 y y 100 y 24.4 9.8, 10.0 0.0005 125 -0.14.600E-03 0.0117 y y 100 y 7.8 10.1, 10.2 0.0005 98 0 1.500E-03 0.0039 y y 99 y 18.6 7.5, 12.8 0.0011 84 1.23.500E-03 0.0074 y y 100 y 16.3 7.3, 12.9 0.0011 92 1.23.300E-03 0.0068 y y 101 y 25.9 6.8, 12.5 0.0011 64 1 5.300E-03 0.0107 y y 101 y 3.3 6.5, 12.9 0.0027 125 0.32.000E-03 0.0014 y 107 y 8.7 6.3, 13.1 0.0027 154 0.43.000E-03 0.0039 y 105 y 6.1 6.1, 13.9 0.0027 140 0.43.000E-03 0.0026 y 104 y 25.5 8.7, 11.4 0.0019 74 1.45.000E-03 0.0117 y y 93.4 y 14.7 8.3, 11.8 0.0019 72 1.43.000E-03 0.0065 y y 94 y 11.6 8.4, 11.8 0.0019 74 1.42.000E-03 0.0050 y y 98.7 y 40.8 3.60, 11.70 0.00078200 0.18.700E-03 0.0140 109.85 24 3.30, 12.30 0.00078 140 0.15.800E-03 0.0090 102.96 61.3 3.10, 13.70 0.00078200 0.11.480E-02 0.0230 103.83
11.4 8.3, 10.8 137 2.152.700E-03 0.0058 y y 113 y 8.8 7.1, 12.3 134 2.152.100E-03 0.0042 y y 112 y 7.25 6.3, 13.1 132 2.151.700E-03 0.0032 y y 113 y

108
7.1, 13.1 0.55 0.23.550E-02 0.0710 y y 102 y 57.4 7.1, 13.0 0.19 0.21.650E-02 0.0336 y y 103 y 42.9 7.5, 12.7 0.97 0.21.400E-02 0.0289 y y 102 y 2.7 10.84, 8.98 2.000E-040.0007 y y 101 y 3 10.31, 9.35 3.000E-040.0007 y y 100 y 2.4 10.25, 9.39 2.000E-040.0006 y y 101 y 20.9 12.4, 7.5 0.001 65 0.66.100E-03 0.0210 y y 106.7 17.9 12.2, 7.8 0.001 60 0.55.300E-03 0.0178 y y 105.9 13.9 11.9, 8.0 0.001 45 0.44.100E-03 0.0133 y y 105.6

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

AK Doyon Utilities/ Unit 4

AK Doyon Utilities/ Unit 4 AK Doyon Utilities/ Unit 4 AK Doyon Utilities/ Unit 7 AK Doyon Utilities/ Unit 7 AK Doyon Utilities/ Unit 7 AR Weyerhaeuser Dierks Mill / Unit 5 (1997) AR Weyerhaeuser Dierks Mill / Unit 5 (1997) AR Weyerhaeuser Dierks Mill / Unit 5 (1997) AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) AR Weyerhaeuser Dierks Mill/ Unit 7 (1997) FL Smurfit-Stone FL Smurfit-Stone

FL Smurfit-Stone GA GP Monticello Plywood (2/21/08) GA GP Monticello Plywood (2/21/08)
GA GP Monticello Plywood (2/21/08) GA GP Monticello Plywood (2/7/07) GA GP Monticello Plywood (2/7/07)
GA GP Monticello Plywood (2/7/07) IA ADM Corn Processing Cedar Rapids IA ADM Corn Processing Cedar Rapids IA ADM Corn Processing Cedar Rapids IA Iowa State University B1 IA Iowa State University B1 IA Iowa State University B1
IA Iowa State University B2
IA Iowa State University B2
IA Iowa State University B2

IA Monsanto Muscatine #8 Cond. 1 (5/2007) IA Monsanto Muscatine #8 Cond. 1 (5/2007) IA Monsanto Muscatine #8 Cond. 1 (5/2007)
IA Monsanto Muscatine #8 Cond. 3 (5/2007)
IA Monsanto Muscatine #8 Cond. 3 (5/2007) IA Monsanto Muscatine #8 Cond. 3 (5/2007) IA Monsano Muscatine #8 Cond. 1 (8/2007) IA Monsano Muscatine #8 Cond. 1 (8/2007) IA Monsano Muscatine #8 Cond. 1 (8/2007) ID Amalgamated Suger Co. Twin Falls ID Amalgamated Suger Co. Twin Falls ID Amalgamated Suger Co. Twin Falls **Notes: Action** 

In calculating the PM a 0.05 mg was added to the final value after the acetone blank raw data does not support this, it is listed as .3 mg in raw data but .25 mg in final spreadsheet. Individual water vapor percents were calculated based upon weights of the water recovered. Reported Values are in lbs/dscf

Run 1 very high probe rinse component.
For this value they had 25.0 mg reported

values kept as is, resultant lb/mmBtu value ok values kept as is, resultant lb/mmBtu value ok
The values for gr/dscf and lbs/MMBtu went below the number of significant figures carried throughout the calculations the lb/dscf was (3.74, 4.23, 2.50)e-8 respectively Database updated, see A-2 for calcs. values kept as is, resultant lb/mmBtu value ok The values for gr/dscf and lbs/MMBtu went below the number of significant figures carried throughout the calculations the lb/dscf was (3.74, 4.23, 2.50)e-8 respectively Database updated, see A-2 for calcs.

This is the lowest polluting of the two permited operating conditions.

Lowest of the runs even though this situation was not used for compliance. This was a combination of coal/corn which was not typical according to the report

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

IA Monsano Muscatine #8 Cond. 1 (10/2009) IA Monsano Muscatine #8 Cond. 1 (10/2009) IA Monsano Muscatine #8 Cond. 1 (10/2009) IA U of Northern Iowa #3 (10/2009) IA U of Northern Iowa #3 (10/2009) IA U of Northern Iowa #3 (10/2009) IL PilyOne Boiler 1 (9/2009) IL PilyOne Boiler 1 (9/2009) IL PilyOne Boiler 1 (9/2009)
IN Purdue University Boiler 5 (7/2009)
IN Purdue University Boiler 5 (7/2009) IN Purdue University Boiler 5 (7/2009) ME Boralex Stratton Boiler 1 (10/2009) ME Boralex Stratton Boiler 1 (10/2009) ME Boralex Stratton Boiler 1 (10/2009) MI Consumer Energy Co - Campbell (9/2009) MI Consumer Energy Co - Campbell (9/2009) MI Consumer Energy Co - Campbell (9/2009) OH Smart Papers Holdings LLC (10/2005) OH Smart Papers Holdings LLC (10/2005) OH Smart Papers Holdings LLC (10/2005) SC GP Chem Russellville (8/2009) SC GP Chem Russellville (8/2009) SC GP Chem Russellville (8/2009) SC Marlboro Paper (7/2009) SC Marlboro Paper (7/2009) SC Marlboro Paper (7/2009) TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA VADukeEnergyNarrows Boiler 2 VADukeEnergyNarrows Boiler 2 VADukeEnergyNarrows Boiler 2 VADukeEnergyNarrows Boiler 3 VADukeEnergyNarrows Boiler 3 VADukeEnergyNarrows Boiler 3 VA University of Virginia 7103-1-01R (12/2007) VA University of Virginia 7103-1-01R (12/2007) VA University of Virginia 7103-1-01R (12/2007) VA University of Virginia 7103-1-01R VA University of Virginia 7103-1-01R VA University of Virginia 7103-1-01R VA University of Virginia 7103-1-02R VA University of Virginia 7103-1-02R VA University of Virginia 7103-1-02R
VA University of Virginia 7103-1-05
VA University of Virginia 7103-1-05 VA University of Virginia 7103-1-05

WA Grays Harbor Paper (6/2006)

WA Grays Harbor Paper (6/2006) WA Grays Harbor Paper (6/2006) **Notes: Action** 

There was no Rinse value associated with this test. All of the mass came from filter weight.

No filter temp.

Could not find supporting documents for lab analysis. Only had summary tables with weight gain of the method 5 runs. No determination based upon filter or rinse.

No information regarding analytical rinse. Data was only seperated between filterable and condensable. Database updated, see A-2 for calcs.

Boiler is an Auxilary boiler and was run not at full load. The boiler also does not have any controls on the stack.

No statement on the calculation of the analytical rinse

Run 1 much higher than 2,3 Blank values for the acetone rinse were high.

Low sample mass / volume Low sample mass / volume Database updated, see A-2 for calcs. Low sample mass / volume Database updated, see A-2 for calcs. PM data not presented PM data not presented PM data not presented

For Run 1, 2 they got an acetone blank of 1.48 mg but then used the maximum allowable blank of .94 in the calculations. For run 3 they got an acetone blank of 1.6 mg and used 1.02

These values are very high in comparison to the other tests. This is a dutch oven and the emissions values are from the stack and not the stack/duct combination (which would likely lower emissions concentration numbers reported from the unit).

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

AR Potlatch Forest Warren (8/2006) AR Potlatch Forest Warren (8/2006) AR Potlatch Forest Warren (8/2006) AR Potlatch Forest Warren (9/2009) AR Potlatch Forest Warren (9/2009) AR Potlatch Forest Warren (9/2009) AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) AR Weyerhaeuser Dierks Mill/ Unit 7 (12/2002) AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) AR Weyerhaeuser Dierks Mill/ Unit 7 (2/2009) IA Archers Daniels Midland Des Moines Boiler 1 (6/2008) IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)
IA Archers Daniels Midland Des Moines Boiler 1 (6/2008)
IA Archers Daniels Midland Des Moines Boiler 1 (8/2009) IA Archers Daniels Midland Des Moines Boiler 1 (8/2009)
IA Archers Daniels Midland Des Moines Boiler 1 (8/2009) ID Potlatch (7/2009) ID Potlatch (7/2009) ID Potlatch (7/2009) ME New Page-Rumford Cogen #6 and #7(12/2009) ME New Page-Rumford Cogen #6 and #7(12/2009) ME New Page-Rumford Cogen #6 and #7(12/2009) MSWeyerhaeuserBruce Boiler 2 (8/2009) MSWeyerhaeuserBruce Boiler 2 (8/2009) MSWeyerhaeuserBruce Boiler 2 (8/2009) ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Riley Creek Lumber ID Tasco Nampa, Riley Boiler ID Tasco Nampa, Riley Boiler ID Tasco Nampa, Riley Boiler ID Tasco Nampa ID Tasco Nampa ID Tasco Nampa IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN Purdue Univ. IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics **Notes: Action** 

No gr/dscf but mg/dscm were 49.13, 6.40, 4.46 respectively

No description of acetone rinse and or filter/rinse components.

Less signs were used in the report.

discrepancy between field data sheet and results page Database updated, see A-2 for calcs. discrepancy between field data sheet and results page Database updated, see A-2 for calcs. discrepancy between field data sheet and results page Database updated, see A-2 for calcs.

they did a nozzle calc, but I don’t know if it passed not very complete

not a full report, only results, no example calcs, filter or rinse masses, etc

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

IN SABIC Plastics IN SABIC Plastics IN SABIC Plastics LA Port Hudson LA Port Hudson LA Port Hudson LA Port Hudson LA Port Hudson LA Port Hudson MI City of Escanaba MI City of Escanaba MI City of Escanaba MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Boise Paper 1212
MN Boise Paper 1212
MN Boise Paper 1212 WA Grays Harbor Paper WA Grays Harbor Paper
WA Grays Harbor Paper WA Weyerhaeuser Co. WA Weyerhaeuser Co. WA Weyerhaeuser Co. WI Domtar 2814 WI Domtar 2814 WI Domtar 2814 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 **Notes: Action** 

Database updated, see A-2 for calcs.
Database updated, see A-2 for calcs.
Database updated, see A-2 for calcs.
Database updated, see A-2 for calcs.
Database updated, see A-2 for calcs.
Database updated, see A-2 for calcs. Mass is reported as TPM (dry catch + organic condensibles + aqueous phase condensibles) filterable is in ()s Database updated, see A-2 for calcs. Mass is reported as TPM (dry catch + organic condensibles + aqueous phase condensibles) filterable is in ()s Database updated, see A-2 for calcs. Mass is reported as TPM (dry catch + organic condensibles + aqueous phase condensibles) filterable is in ()s Database updated, see A-2 for calcs. OTM 28 and M29 were done simultaneously. OTM 28 and M29 were done simultaneously. Only run 1 shows the blank correction. OTM 28 and M29 were done simultaneously. Only run 1 shows the blank correction. ok, calcs in report are correct

A soot blow, which typically occurs 3xs/day, happened in run 2. Database updated, see A-2 for calcs. the total pm results include M202 data. the total pm results include M202 data. Masses are front half only. I didn't include back half which was much greater. No actual sample calcs, just equations missing data: filter weight, rinse weight, volume of reagent, sample calc filter blank of 0.1mg filter blank of 0.1mg filter blank of 0.1mg Left side of page is missing in first ~20 pages. Filter temp is too high Filter temp is too high Filter temp is too high

Boiler #9 goes through stack 11 no actual values in the sample calcs, just formulas no actual values in the sample calcs, just formulas

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WIGreenBayPackagingMillDivision WIGreenBayPackagingMillDivision WIGreenBayPackagingMillDivision WI New Page Biron WI New Page Biron WI New Page Biron SC Milliken Dewey Plant SC Milliken Dewey Plant SC Milliken Dewey Plant TN Milan Army Ammunition Plant TN Milan Army Ammunition Plant TN Milan Army Ammunition Plant VA GP Big Island 2703 VA GP Big Island 2703 VA GP Big Island 2703 WA Weyerhaeuser Raymond WA Weyerhaeuser Raymond WA Weyerhaeuser Raymond WI GPGreenBay 2818 WI GPGreenBay 2818 WI GPGreenBay 2818 WI New Page Biron WI New Page Biron WI New Page Biron

WI Wausau

WI Wausau

WI Wausau

WV Mountain State Carbon Follansbee WV Mountain State Carbon Follansbee WV Mountain State Carbon Follansbee **Notes: Action** 

no way to tell b'c of bad sample calcs no way to tell b'c of bad sample calcs no way to tell b'c of bad sample calcs high temp to prevent sulfate from forming on the filter. Actual rinse wgt was 7.4mg (1.6 was subtracted). net weight of rinse was -0.1. corrected wt = 0.0mg backup filter was 1.3mg. backup filter was -0.3mg. backup filter was 0.5mg. high temp to prevent sulfate from forming on the filter

Highlighted areas are totals (front and back half), not just filterable No field data sheets.
Run 2 much lower than other two runs (1 and 3). Removing this test, broken vacuum suspected and no final leadk detection in report. Database updated, see A-2 for calcs.

No controls lab said moisture was on filters so they were baked at 105C until dry. ok, calcs in report are correct

Mass fractions for which the lab results was 0 were assigned the DL of 0.1mg. highlighted areas are values that had BDL fractions

no actual values in the sample calcs, just formulas no actual values in the sample calcs, just formulas

Boiler #5 has two IK soot blowers that operate once, for 5 minutes each, per 8-hour shift and a third IK soot blower that is operated for 5 minutes once every 24 hours. Database updated, see A-2 for calcs.
During Run 2 on Boiler #5 all three soot blowers will be operated, one after the other, for a total soot blow duration of 15 minutes. For all Boiler #5 particulate test runs CleanAir performed 2.5 minute points yielding 6 points (50%) of the duct traversed during the soot blow. Database updated, see A-2 for calcs. Reports states that filterable front-half emissions are also PM2.5 emissions (p 11)

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA

TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA
TN Eastman NO CBI DATA
TN Eastman NO CBI DATA TN Eastman NO CBI DATA **Notes: Action** 

Two conditions were tested: 1. non-ozone season and 2. low-NOx mode inside the ozone season. NO FIELD DATA, FILTER/RINSE DATA, OR M5 RESULTS. VERY INCOMPLETE

NO FIELD DATA, FILTER/RINSE DATA, OR M5 RESULTS. VERY INCOMPLETE

The leak check of run 1 failed. Due to time constraints the TDAPC contact allowed test certification on the basis of runs 2 and 3 only.

Soot blowing was conducted during run 3. Run 2 was void after the 2nd port change due to a broken impinger

Run 1 was voided b'c a probe liner broke. Soot blowing was performed during Run 4.

Two conditions were tested: 1. non-ozone season and 2. low-NOx mode inside the ozone season. NO FIELD DATA, FILTER/RINSE DATA, OR M5 RESULTS. VERY INCOMPLETE

Run 3 was voided due to an operational upset Database updated, see A-2 for calcs. Database updated, see A-2 for calcs. Database updated, see A-2 for calcs. Leak check failed on Run 3, so it was voided. The pm catch was less than the DL of 6mg, so 4.7mg was used.
Small shards of glass were found in the filter housing of runs 2 and 3, but the observer from TDAPC said it was ok and the shards were removed before weighing.

Soot blow during run 1

During run 1 a glass connector between the filter and impinger 1 broke, so the run was terminated.

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA TN Eastman NO CBI DATA

VA Duke Energy Narrows

VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Duke Energy Narrows VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island VA Georgia Pacific Big Island
VA Georgia Pacific Big Island
VA Georgia Pacific Big Island VA Georgia Pacific Big Island

WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WI Thilmany Paper WA Weyerhaeuser Raymond (11/2004) WA Weyerhaeuser Raymond (11/2004) **Notes: Action** 

Soot blow during run 3

17.5mg is erroneous. It should be 16.7 soot blowing during run 3

4 runs were done but the test report doesn't document why. There is no front half data for run 3, so I assume there was an issue. The lab only reports data for 3 runs, so I'm assuming those samples are from runs 1,2, and 4.

Sample volume is <30dscf Sample volume is <30dscf Sample volume is <30dscf The test location is only 1.4 and 1.7 equivalent diameters up and downstream from disturbances.

this is not well documented. They did 6 runs plus two sets of two but no discussion of why. Runs were 48 minutes each but the report states they were 60 minutes.

Isokinetics ~88%, void this run.

Soot blowing occurred during run 2 for thirty minutes Soot blowing occurs three times per day for 30 minutes each.
Soot blowing occurred during run 2 for thirty minutes Soot blowing occurs three times per day for 30 minutes each.

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

WA Weyerhaeuser Raymond (11/2004) WA Weyerhaeuser Raymond (9/1996) WA Weyerhaeuser Raymond (9/1996) WA Weyerhaeuser Raymond (9/1996) FL US Sugar Corp Boiler 8 (12/2009) FL US Sugar Corp Boiler 8 (12/2009) FL US Sugar Corp Boiler 8 (12/2009)

FL US Sugar Corp Boiler 8 (6/2006)

FL US Sugar Corp Boiler 8 (6/2006) FL US Sugar Corp Boiler 8 (6/2006) FL US Sugar Corp Boiler 8 (6/2006) FL US Sugar Corp Boiler 8 (6/2006)
FL US Sugar Corp Boiler 8 (8/2006)
FL US Sugar Corp Boiler 8 (8/2006) FL US Sugar Corp Boiler 8 (8/2006)
FL US Sugar Corp Boiler 8 (1/2007)
FL US Sugar Corp Boiler 8 (1/2007) FL US Sugar Corp Boiler 8 (1/2007)
FL US Sugar Corp Boiler 8 (1/2007)
FL US Sugar Corp Boiler 8 (1/2007) FL US Sugar Corp Boiler 8 (1/2007) FL US Sugar Corp Boiler 8 (1/2007) GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) GA GP Madison Ply (6/2006) GA GP Madison Ply (6/2006) GA GP Madison Ply (6/2006) GA GP Madison Ply (9/2007) GA GP Madison Ply (9/2007) GA GP Madison Ply (9/2007) GA GP Madison Ply (6/2003) GA GP Madison Ply (6/2003) GA GP Madison Ply (6/2003) GA GP Madison Ply (8/2009) GA GP Madison Ply (8/2009) GA GP Madison Ply (8/2009) IL Abbott Abbott Park IL Abbott Abbott Park IL Abbott Abbott Park MN American Crystal Crookston Boiler 1 (10/2005) MN American Crystal Crookston Boiler 1 (10/2005) MN American Crystal Crookston Boiler 1 (10/2005) OH U of Cincinnati B108 (4/2006) OH U of Cincinnati B108 (4/2006) OH U of Cincinnati B108 (4/2006) SC International Paper Eastover Boiler 1(10/2004) SC International Paper Eastover Boiler 1(10/2004) **Notes: Action** 

lb/MMBtu includes condesnable. Run 3 does not have supporting material in the report Database updated, see A-2 for calcs. lb/MMBtu includes condensable

Volume of Acetone used was not recorded for all runs. Only run 1 which used 71.6595 g

Runs 3,4,5 were used for compliace. Acetone Blank was not used to correct wash values. There was only one blank weighed but I noted it for each run. The boiler was also only running at 50% load which is "normal" for non-peak season load. Only Bagasse was used for firing.

The boiler was firing only wood chips this test. There was only one blank weighed but I noted it for each run. No blank correction was made

The boiler was firing only Bagasse this test. There was only one blank weighed but I noted it for each run. No blank correction was made

The boiler was firing only on Bagasse this test. Run 3 was aborted due to plant malfunction. There was only one blank weighed but I noted it for each run. No blank correction was made

Subtracted a negative filter weight from the Acetone Wash values. Database updated, see A-2 for calcs. Subtracted a negative filter weight from the Acetone Wash values. Database updated, see A-2 for calcs. Subtracted a negative filter weight from the Acetone Wash values. Database updated, see A-2 for calcs. No blanks

The grates were raked during run 3. No blanks were reported

No Blanks

No blanks and the report did not have gr/dscf or lbs/MMBtu Database updated, see A-2 for calcs.
The summary for the boiler does not match the supporting data.

No blanks

Weight of Acetone wash was only recorded not the volume of the wash. A blank was done and no correction was recorded.

## Appendix A-1 - PM Tracking Sheet for Boiler Data Review

**Facility/Unit**

SC International Paper Eastover Boiler 1(10/2004) SC International Paper Eastover Boiler 1(10/2000) SC International Paper Eastover Boiler 1(10/2000) SC International Paper Eastover Boiler 1(10/2000) SC International Paper Eastover Boiler 1(10/2006) SC International Paper Eastover Boiler 1(10/2006) SC International Paper Eastover Boiler 1(10/2006) SC International Paper Eastover Boiler 1(10/2002) SC International Paper Eastover Boiler 1(10/2002) SC International Paper Eastover Boiler 1(10/2002) SC International Paper Eastover Boiler 2(10/2002) SC International Paper Eastover Boiler 2(10/2002) SC International Paper Eastover Boiler 2(10/2002) SC International Paper Eastover Boiler 2(3/2008) SC International Paper Eastover Boiler 2(3/2008) SC International Paper Eastover Boiler 2(3/2008) SC International Paper Eastover Boiler 2(3/2004) SC International Paper Eastover Boiler 2(3/2004) SC International Paper Eastover Boiler 2(3/2004) SC International Paper Eastover Boiler 2(6/1999) SC International Paper Eastover Boiler 2(6/1999) SC International Paper Eastover Boiler 2(6/1999) SC International Paper Eastover Boiler 2(6/2003) SC International Paper Eastover Boiler 2(6/2003) SC International Paper Eastover Boiler 2(6/2003) SC International Paper Eastover Boiler 2(8/1997) SC International Paper Eastover Boiler 2(8/1997) SC International Paper Eastover Boiler 2(8/1997) SC International Paper Eastover Boiler 2(8/1995) SC International Paper Eastover Boiler 2(8/1995) SC International Paper Eastover Boiler 2(8/1995)

SC International Paper Eastover Boiler 2(8/1993)

SC International Paper Eastover Boiler 2(8/1993) SC International Paper Eastover Boiler 2(8/1993) TN Cargill Memphis Boiler 8001(8/2009) TN Cargill Memphis Boiler 8001(8/2009) TN Cargill Memphis Boiler 8001(8/2009) TN Cargill Memphis Boiler 8001(7/2007) TN Cargill Memphis Boiler 8001(7/2007) TN Cargill Memphis Boiler 8001(7/2007) **Notes: Action** 

Weight of Acetone wash was only recorded not the volume of the wash. A blank was done and no correction was recorded.

The blank correction values include .3 mg for the filter blank.

Negative Acetone blanks

High temperatures. The blank correction value includes a .5 mg correction for the filter blank

High temperatures. A filter blank of .5 mg was found but was not applied to the samples

High temperatures

No flow data for runs 2 and 3

Volume of rinse was calculated based upon the mass and a density of .79 provided by the report

A note was made about the Acetone wash values that it was suspected to be high because of contamination but it will still be used because it biases the values high. Also the rinse mL seem to be low but were calculated base upon weight and a report density of .79.

The filterable pm values were reported as .5 because that seemed to be the detection level of the instrument making the reading.

# Appendix A-2 - Calculations for PM Data Revisions

**Facility/Unit Category/ sub-category** **Run ID FacilityID**  **Unit ID Test Date** **Run ID Data Source**  **Source Tab Oxygen%** **F-Factor**

WIGreenBayPackagingMillDivi sion Boiler B26/Coal fired (2006) 2WIGreenBayPackagingMillDi vision Boiler B26- Coal Fired Boiler 5/16/2006ALL ICR Phase I PM and Metals{PM & HgB26} 10.759780

IA Iowa State University B2solid/coal 1IAIAStateUnivPowerPlantB2 3/27/2008Sample #1ICR Phase I PM and Metals (2) 4 9780 IA Iowa State University B2solid/coal 3IAIAStateUnivPowerPlantB2 3/27/2008Sample #3ICR Phase I PM and Metals (2) 3.7 9780 ME Boralex Stratton Boiler 1 (10/2009) solid/biomass 1MEBoralexStratton Boiler #1 10/21/2009Sample #1ICR Phase II - Templates PM Additions from Test

Report 6.3 9600
VA University of Virginia 7103- 1-01R (12/2007) solid/coal 2VAUniversityofVirginia 7103-1-01R 12/6/2007Sample #2ICR Phase I PM and Metals 7.039780 VA University of Virginia 7103- 1-01R (12/2007) solid/coal 3VAUniversityofVirginia 7103-1-01R 12/6/2007Sample #3ICR Phase I PM and Metals 6.989780

WI Domtar 2814 Solid/Biomass 1WIDomtar2814 B11, S11 8/29/2007Sample #1ICR Phase I PM and Metals (B11) 9.413680

GA GP Madison Ply (8/2009)solid/biomass 2GAGPMadisonPly 800 Wood Waste Boiler8/12/20092 ICR Phase II - ERTERT 8.219600

WI Wausau Solid/Coal (boiler 5) 1WIWausau # 5 Power Boiler (B24)7/24/2007Sample #1ICR Phase I PM (B24) 11 9780 WI Wausau Solid/Coal (boiler 5) 3WIWausau # 5 Power Boiler (B24)7/24/2007Sample #3ICR Phase I PM (B24) 11.29780 ID Tasco Nampa Solid/Coal 1IDTASCONampa Riley Boiler 1/12/2004Sample #1ICR Phase I PM and Metals (3) 6.3 9780 ID Tasco Nampa Solid/Coal 2IDTASCONampa Riley Boiler 1/12/2004Sample #2ICR Phase I PM and Metals (3) 6.4 9780 ID Tasco Nampa Solid/Coal 3IDTASCONampa Riley Boiler 1/12/2004Sample #3ICR Phase I PM and Metals (3) 6.4 9780

MN Boise Paper 1212 Boiler #2 6/2005 (PM10) 1MNBoisePaper1212 EU 430 Boiler #2 6/7/2005Sample #1ICR Phase I PM and Metals #2 Boiler 2005 5.6 9585

MN Boise Paper 1212 Boiler #2 6/2005 (PM10) 2MNBoisePaper1212 EU 430 Boiler #2 6/7/2005Sample #2ICR Phase I PM and Metals #2 Boiler 2005 5.4 9585

MN Boise Paper 1212 Boiler #2 6/2005 (PM10) 3MNBoisePaper1212 EU 430 Boiler #2 6/7/2005Sample #3ICR Phase I PM and Metals #2 Boiler 2005 6.8 9585

GA GP Madison Ply (10/2004)solid/biomass 1GAGPMadisonPly 800 Wood Waste Boiler10/14/2004Sample #1ICR Phase II - Comments Additional PM from

Comments - 2004 8.829280 GA GP Madison Ply (10/2004)solid/biomass 2GAGPMadisonPly 800 Wood Waste Boiler10/14/2004Sample #2ICR Phase II - Comments Additional PM from

Comments - 2004 8.769280 GA GP Madison Ply (10/2004)solid/biomass 3GAGPMadisonPly 800 Wood Waste Boiler10/14/2004Sample #3ICR Phase II - Comments Additional PM from

Comments - 2004 9.069280 

### From Sheet A-1 **From Database**

# Appendix A-2 - Calculations for PM Data Revisions

**Facility/Unit Category/ sub-category** **Run ID FacilityID**  **Unit ID Test Date** **Run ID Data Source**  **Source Tab Oxygen%** **F-Factor**



### From Sheet A-1 **From Database**

WA Weyerhaeuser Raymond (11/2004) Solid/Biomass 3WAWeyerhaeuser_RaymondHog Fuel Boiler EU1 11/10/2004Sample #3ICR Phase I PM and Metals 8.711300

TN Eastman NO CBI DATASolid/Coal (11/8/1994) 1TNEastman_NO_CBIDATABoiler 30 11/8/1994Sample #1ICR Phase I PM and Metals (UDBlr30) (2) 11.61800

TN Eastman NO CBI DATASolid/Coal (11/8/1994) 2TNEastman_NO_CBIDATABoiler 30 11/8/1994Sample #2ICR Phase I PM and Metals (UDBlr30) (2) 12.61800

TN Eastman NO CBI DATASolid/Coal (11/8/1994) 4TNEastman_NO_CBIDATABoiler 30 11/8/1994Sample #3ICR Phase I PM and Metals (UDBlr30) (2) 11.81800
MN Andersen Corp BayportBoiler 11 Solid/Biomass (wood fuel) 4/2008 1MNAndersonCorpBayportBoiler 11 EU620 4/22/2008Sample #1ICR Phase I PM and Metals
MN Andersen Corp BayportBoiler 11 Solid/Biomass (wood fuel) 4/2008 2MNAndersonCorpBayportBoiler 11 EU620 4/22/2008Sample #2ICR Phase I PM and Metals
MN Andersen Corp BayportBoiler 11 Solid/Biomass (wood fuel) 4/2008 3MNAndersonCorpBayportBoiler 11 EU620 4/22/2008Sample #3ICR Phase I PM and Metals
MN Andersen Corp BayportBoiler 12 Solid/Biomass (wood fuel) 4/2008 1MNAndersonCorpBayportBoiler 12 EU621 4/22/2008Sample #1ICR Phase I PM and Metals (5)
MN Andersen Corp BayportBoiler 12 Solid/Biomass (wood fuel) 4/2008 2MNAndersonCorpBayportBoiler 12 EU621 4/22/2008Sample #2ICR Phase I PM and Metals (5)
MN Andersen Corp BayportBoiler 12 Solid/Biomass (wood fuel) 4/2008 3MNAndersonCorpBayportBoiler 12 EU621 4/22/2008Sample #3ICR Phase I PM and Metals (5)

# Appendix A-2 - Calculations for PM Data Revisions

**Facility/Unit**

WIGreenBayPackagingMillDivi sion
IA Iowa State University B2 IA Iowa State University B2 ME Boralex Stratton Boiler 1 (10/2009) VA University of Virginia 7103- 1-01R (12/2007) VA University of Virginia 7103- 1-01R (12/2007)

WI Domtar 2814

GA GP Madison Ply (8/2009)

WI Wausau WI Wausau ID Tasco Nampa ID Tasco Nampa ID Tasco Nampa

MN Boise Paper 1212

MN Boise Paper 1212

MN Boise Paper 1212

GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) 

### From Sheet A-1

**Fuel 1 Sample** 

**volume (dscf)** **Mass - Filter (mg)** **Mass -**

**Rinse (mg) Re-calculated** 

**Based on zero filter for negative**  **values Revised** 

**Catch based on 64 FR**  **53028 Mass Total** 

**(mg) Reported** 

**Mass/Unit (lbs/mmbtu)** **Reported Total**

**Mass (based on negative filter**  **weight) Revised** 

**lb/mmBtu value using site**  **specific factor**

Coal-100% bituminous 84.67 0 0.1 1 1 0.007 5.23E-04

Coal-100% bituminous 35.400.3 0.3 1 1 0 1.00E-03 Coal-100% bituminous 35.290.4 0.1 1 1 0 1.00E-03 Wet biomass-100% Wood: Bark/Wood: Unadulterated Timber 20.20n/a n/a 1 1 0.001 1.50E-03

Coal-100% bituminous 35.360.3 0.2 1 1 0.0005 9.18E-04

Coal-100% bituminous 33.440.1 0.3 1 1 0.0004 9.67E-04 Wet biomass-100% /Wood: Unadulterated Timber/ 37.13 0.7 <1.06 ? 1.76 2.8 2.59E-03
Wet biomass-82%; Dry biomass 18% (Wood: Bark/Wood: Plywood, Particleboard (containing glues or resins)/Wood: Unadulterated Lumber) 154.06 0 0.1 1 1 2.26E-04

Bituminous coal 35.90<0.3 <1.06 ? 1.360.000835 1.72E-03 Bituminous coal 36.84<0.3 1.6 ? 1.9 0.00125 2.39E-03 Coal-100% subbituminous31.12 1.5 4.4 ? 5.9 1.09 5.85E-03 Coal-100% subbituminous29.29 1.1 3.9 5 5.30E-03 Coal-100% subbituminous31.51 1 3.8 4.8 4.73E-03 Wet biomass-87.6%; Heavy liquid-12.04% (Industrial Sludge - Primary/Industrial Sludge - Secondary/Natural gas/Wood: Bark) 36.19-5.8 6.4 6.4 6.4 5.10E-03

Wet biomass-87.6%; Heavy liquid-12.04% (Industrial Sludge - Primary/Industrial Sludge - Secondary/Natural gas/Wood: Bark) 35.06-1.3 3.3 3.3 3.3 2.68E-03

Wet biomass-87.6%; Heavy liquid-12.04% (Industrial Sludge - Primary/Industrial Sludge - Secondary/Natural gas/Wood: Bark) 34.46-2.5 5.8 5.8 5.8 5.27E-03

Wet biomass-100% Bark 40.38-0.5 3.1 3.1 3.1 0.002 2.72E-03

Wet biomass-100% Bark 39.91-0.1 3.8 3.8 3.8 0.003 3.35E-03

Wet biomass-100% Bark 40.78-0.4 2.3 2.3 2.3 0.002 2.04E-03

# Appendix A-2 - Calculations for PM Data Revisions

**Facility/Unit**

### From Sheet A-1

WA Weyerhaeuser Raymond (11/2004)

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport **Fuel 1 Sample**  **volume (dscf)** **Mass - Filter (mg)** **Mass -**

**Rinse (mg) Re-calculated** 

**Based on zero filter for negative**  **values Revised** 

**Catch based on 64 FR**  **53028 Mass Total** 

**(mg) Reported** 

**Mass/Unit (lbs/mmbtu)** **Reported Total**

**Mass (based on negative filter**  **weight) Revised** 

**lb/mmBtu value using site**  **specific factor**
Dry Biomass-100% hog fuel41.58 0 0.6 1 1 0.004 1.03E-03

Coal: Bituminous 50.29 1.3 15.9 16.4 1.12E-02

Coal: Bituminous 50.903.2 11.2 13.6 8.41E-03

Coal: Bituminous 47.57 2.8 10.8 12.8 9.05E-03 /Natural gas/Wood: Unadulterated Lumber/ 42.89-2.5 5.7 5.7 5.7 0.002 3.2 3.56E-03 /Natural gas/Wood: Unadulterated Lumber/ 43.14-2.8 3.6 3.6 3.6 0.001 0.8 4.50E-03 /Natural gas/Wood: Unadulterated Lumber/ 42.44-1.2 3.3 3.3 3.3 0.002 2.1 3.14E-03 /Natural gas/Wood: Unadulterated Lumber/ 39.95-4.5 5.3 5.3 5.3 0.006 0.8 3.98E-02 /Natural gas/Wood: Unadulterated Lumber/ 39.63-3.3 4.3 4.3 4.3 0.008 1 3.44E-02 /Natural gas/Wood: Unadulterated Lumber/ 39.04-1.8 2.3 2.3 2.3 0.004 0.5 1.84E-02

# Appendix A-2 - Calculations for PM Data Revisions

**Facility/Unit**

WIGreenBayPackagingMillDivi sion
IA Iowa State University B2 IA Iowa State University B2 ME Boralex Stratton Boiler 1 (10/2009) VA University of Virginia 7103- 1-01R (12/2007) VA University of Virginia 7103- 1-01R (12/2007)

WI Domtar 2814

GA GP Madison Ply (8/2009)

WI Wausau WI Wausau ID Tasco Nampa ID Tasco Nampa ID Tasco Nampa

MN Boise Paper 1212

MN Boise Paper 1212

MN Boise Paper 1212

GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) GA GP Madison Ply (10/2004) 

### From Sheet A-1

**Notes:**

Removing this entire test, broken vacuum suspected and no final leak detection in report. Run 2 much lower than other two runs (1 and 3).

No information regarding analytical rinse. Data was only seperated between filterable and condensable.

discrepancy between field data sheet and results page

Subtracted a negative filter weight from the Acetone Wash values. Subtracted a negative filter weight from the Acetone Wash values. Subtracted a negative filter weight from the Acetone Wash values.

# Appendix A-2 - Calculations for PM Data Revisions

**Facility/Unit**

### From Sheet A-1

WA Weyerhaeuser Raymond (11/2004)

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA

TN Eastman NO CBI DATA
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport
MN Andersen Corp Bayport **Notes:**

lb/MMBtu includes condesnable. Run 3 does not have supporting material in the report? Total mass <1 mg. Did a back calc using gr/dscf number. adjusted as report subtracted too much for blank, added 2.8mg. adjusted as report subtracted too much for blank, added 3mg. adjusted as report subtracted too much for blank, added 3mg. Corrected lb/mmBtu based on a ratio of catches
Corrected lb/mmBtu based on a ratio of catches
Corrected lb/mmBtu based on a ratio of catches
Corrected lb/mmBtu based on a ratio of catches
Corrected lb/mmBtu based on a ratio of catches
Corrected lb/mmBtu based on a ratio of catches