July 17,1997 James G. Cra wford 11 25 N. Military Av e . Box 104 48 Gree n Bay, WI 54307-0448

Dear Mr . Crawfo rd :**~** 

# ,.,-" • • Please find enclosed th e results of stack**tes~ing** f o r chromium emiss i o n s at Ult r a P l ati ng. The r esults sho w that Ultra P l ating is in compliance, fo r the NES HA P limit of
. 015 m g/dscm
. 'r he c lo se ag r eement o f these test results wi th previous testing done at U ltra**Platin~** lend a high deg re e of co nfi dence in the val i dity and reproducability of these res ul ts . The raw data and calculations are included in tllis report. I f you should**eq uire**  a ny o ther i nf or mati on, please call me. Very T ru ly yours,



# w-- 

# n - . \.J l.lY"

## , Ste v e Preisler Plan t Chemist

UURA PlATI N G

,**COR~** 345 S
. PEARL STREET· P
. O

. BOX 2423 • GnEEN BIIY. WI SW N S

IN 54306 TELEPHONE 414 .437
. 9108 FAX 414 437.1992S'J'ACK ' l 'ES1'ING RESULTS AT ULTRA PLATING In May and June, off icial s upervised stack emissio n testin g was don e o n the n o r th and sout h stacks respectively. The samp l e gathering was done according t o EPA M et h od 306A, a nd the samples collected**we~e** s ent to Sc ientifi c Co ntrol Labs in Chicago for analysis of ch r om ium content by g raphite furnace AA. Their test results**ar~** included her ein a nd ccnstitute Appendix I. The north stack serves the horizontal plating tank , This tank h as maximum r ectif ier capacity of 10,000 am p hours, and was run at a little ove r 6 000 amps du rin g t h e stack test to r epresent a high end typi c al usage s i tuat i o n. The north stack , S02 whi c h se r ves POI, has a diameter o f 2 4 in ches
. The samp lin g point was pla ced 5 s tack diameter s downs tream fr o m any stack disturbance, a n d one s tack diameter up strea m rro t tt the exit. Se e Appendix II for diag ram s of the processes and stacks. The sout h stack, S03, s!2rves hard chrome plat in g tanks P02-P09. The f were run at the f o ll ow ing amperages, whi c h a l so re p resent hi g h e nd typical u sages. Very seldo m will all tanks be running simul tan e ou s ly, so the test w as a maximum discharge s i tuation. 

### P02 lO, lOO amps 

### P0 3 9300 amps 

### P04 370 0 amps 

### P05 6500 amps 

### P06 8000 am p s 

### P 07 lO ,OOO a m ps 

### P08 450 a mp s 

### P09 350 amps The sout h stack, 

### 503 has a**~~** inch diameter, and in this case too, a s amplin g location was chosen which was five d i ameters downstream f r om any disturbance, and or.e diamete r up st ream from disturban ce . O n both stacks, a pitot velocity traverse o f 24 po ints wa s d o n e, an d then sampling traverses of 2 - \ sa mp l ing**poin~s** w a s done
. The raw data UURA PLATING , CORP. 345 S
. PEARL STREET · P
. O

. BOX 2423 • GRE W BAY
. Yl ISCOt I S IN 5 <1 306 TE LEPHONE 414.437
. 9108 fAX 414.4371992gathered during the sampling is included, and c'onstitutes Appendix III. CALCULATED RESULTS: NORTH STACK S02 Both the concentration of chromium, mg/m 3 , and the discharge rate in kg/hr were calculated. Chromium concentration 

### M (T + 460) 

## =**_c~** 

### ___ m __________ _ 499.8(Y m )(V m )(Pbar) where: C cr 

# = chromium concentration in mg/dscm Tm = mf!ter gas discharge temperature in F Y

m = meter correction factor (see Appendix IV) Vm =meter volume in ft 3

. Pbar 

# = barometric pressure Mcr = micrograms of chromium in catch sample RUN 1**_!~~!_~~_i~~~_~_~~Ql** 

# __________ _ 499.8

### (1.02~)(77.36ft3)(30.30 inHg)
RUN 2**_~~_~2_iZ~~_!_~~Ql** 

# _____________ _ 499.8(1.029)(74.47ft 3 )(30.30 inHg)
'RUN 3 10 ug (74F 

### + 460) 

# ---------------------3----------

499,8(1.029)(58.43ft )(30.30 inHg) 

### ULTRA PLATING, CORP. 345 S. PEARL STREET • P.O. BOX 2423 • GREEN RAY. WISCONSIN 54306 TELEPHONE 414.437.9108 FAX 414.437.1992 =.0073 mg/dscm

=.011 mg/dscm



# = .0058 mg/dscmAverage chromium co ncentration = . 008 mg/dscm Discharge Rat.e :

Ts 

# = stack temperature 

### r 

## = stack radius**'\oJ=** av o sq. rt . inches of water


### RUN 1 kg/hr =.000 093 kg/ hr 

### RUN 2 kg/hr =.00014 kg/he 

### RUN 3 kg/he = . 000073 kg/he 

### average discharge rate = .00001

SOUTH STACK chromium concentration C cr 

### Run C 

### cr = .00 23 mg/ds c m ULJRA PLATING , C ORP. 345 S
. PEARL STREET · P
. O

. BOX 2423 • GnEEN BAY, WISCONSIN 54306 TELEPHONE 4 1 4.437.9108 FAX 414
. 437
. 1992**_!s_:~~ Q**  

## _ __ _ Pbar (28.73)

kg/he 3

where :RUN 2 C cr = .0031 mg/dscm RUN 3 C 

### cr =.0024 mg/dscm
average chromium concentration = . 0026 mg/dscm Discharge Rate kg/he
RUN 1 kg/hr 

# = . 0001 kg/hr RUN 2 kg/he 

## = . 000129 kg/he RUN 3 kg/he 

## = . 0001 kg/he Average discharge Rate = . 00011 kg/hr

UIJRA PLATING , CORP.**3~5** S
. PEARL S T

REET · P
. O

. BOX 2423 • GREEtI BAY, WISCONSIN 54306 TELEPHONE 414.437
. 91(18 FAX 414.437
. 1992RESULTS AND DISCUSSION: Test results indicate that Ultra Plating is in compliance with NESHAP chromium emission standards. The average chromium concentration from the north stack, S02, is .008 mg/dscm. The south stack, S03, averages .0026 mg/dscm. These results are in close agreement with previous testing done both by myself, and Scientific Control Labs on these stacks. See Appendix V for these results. This close agreement of results lends a high confidence factor to the results obtained on this occasion.



### ULTRA PLATING, CORP. 345 S. PEARL STREET • P.O. BOX 2423 • GREEN BAY, WISCONSIN 54306 TELEPHONE 414.437.9108 FAX 414.437.1992**~f~6i~** .J.. hoC"""**-J;~4t.** 

### c.1e. 

## P":J e .L**r«!~..c.'** 

### t s 

# ;£cienti 1 

# ic**CONTROL~·LABORATORIE9,** INC. Samuel Wright Laboratory Manager 3168 S. Kolin Ave. Chicago IL 80823·4889 Phono: 773-254·2408 Extension 3041 FAX: 773·254-8881 

### Report To:

' 

# ..**'.'.'~** .

"
, .**~".~** . TESTING - CONSULTING 

### Mr. Steve Preisher. Ultra Plating Corporation 345 South Pearl Street Green Bay WI 54306



### . . .**Pi:'O~** 

### 'Number: 

# ::?rbJ;ct Type: Stack Testing 

# '..**.~;** 

# .. :IDENTIFICATION OE MATERIAL: Three (3) samples, identified below. PROCEDURE: Project Number: Project Inception: Report Date: 05-773 05-28-97 06-10-97

All analyses were performed in accordance with the EPA/IEPA approved test pro.cedures as specified in 40 CER, Part 60, Method 306A •



# . ' 

### Scientific Control Labs, Inc., is a certified laboratory for analysis of potable water -(IEPA Cert. #100183), and a certified laboratory for wastewater analysis (State of Washington Cert. #C165, State of Wisconsin DNR #998091930). This means we - have 

### a quality control program in effect and that this quality control program Is monitored and reviewed annually by the certifying agencies. RESULTS; Sample 10: 

### RUN #1 RUN #2**RU~#3** 

### QUALITY CONTROL 

### DAIAl Concentration In ppm (mglU 

### TOTAL CHROMIUM VOLUME (mn 0.067 250 0.090 269 0.038 265 The samples were analyzed by Graphite Furnace Atomic Absorption for detection of Total Chromium.

SW:clm CERTIFICATION: Sample: Duplicate: Spike: LFB:**LR~:** 

### 13.39 ppb 14.69 ppb 

### = 34.53 ppb 

# =

9.66 ppb = 

### -0.63 ppb 

### = relative percent difference 

### = 9.71 

### % 106% spike recovery 96.6% recovery 

## < minimum detection limit Respectfully submitted, SelENTIE 

### C CONTROL**LABOR~TORIES,** 

### INC. /1
. t' I 

### By
__**~~~~'~-~~~~~~~** 

### ___________ _ Samuel-Wright The above statements and report were subscribed and sworn to before me this**T~NTH** 

### day of JUNE, 1997.

### Report To: TESTING - CONSULTING 

### Mr. Steve Preisher Ultra Plating Corporation 345 South Pearl Street Green Bay WI 54306 

## rt,p"'tt. 

# 6. w ..J..**~** 

### fAJ. -.. c**..sc)I4~ ~TAGk.** **('CS~\ts** Samuel Wright Laboratory Manager 3158 S. kolin Ave. Chicago IL 60623·4889 Phone: 773·254·2406 Extension 3041 FAX: 173·254·6661



### Project Number: P. O. Number: 03519 Project Inception: 06-257 06-20-97 06-30-97 Project Type: Stack Testing Report Date: IPENTIFICATION OF**MATFJllA~** 

### Three (3) samples, identified below. PROCEDURE: All analyses were performed in accordance with the EPAIIEPA approved test procedures as specified in 40 CFR, Part 60, Method 306A. Scientific Control Labs, Inc., is a certified laboratory for analysis of potable water (lEPA Cert. #100183), and a certified laboratory for wastewater analysis (State of Washington Cert. #C165, State of Wisconsin DNR #998091930). This means we have a quality control program in effect and that this quality control program is monitored and reviewed annually by the certifying agencies. RESULTS: Sample 10: RUN #1 RUN #2 RUN #3 QUALITY CONTROL DATA Concentration in ppm 

### (mg/U ntTAL CHROMIUM VOLUME (mn 0.018 290 0.025 260 0.043 256 The samples were analyzed by Graphite Furnace Atomic Absorption for detection of Total Chromium. Sample: Duplicate: Spike: LFB: LRB 3.7.9 ppb 2.83 ppb 

# = 22.05 ppb 

# = 20.96 ppb 

# = 1.01 ppb 

## = relative percent difference 

### = N.A. 91.3% spike recovery 104.8% recovery minimum detection limit = 2.00 ppb Respectfully submitted, SCIENTIFIC·,CONTROL LABORATORIES, INC. 

### j' ,

. 

# ."

-- -:::(--,/. 

### - . - . 

### By 

### x.."
. '---"- l , . (.0
.. -- 

### SW:llc Samuel Wright CERTIFICATION: The above statements and report were**subsqrib~d** 

### and sworn to**bJefor~** 

### me this THIRTIETH day of JUNE, 1997. 

# \/J \ / ./ I • ( 1<
.. ,"J 

# It 1 /1 

# f'. ( {i'. i / " 

### "OFFICIAL SEAL"
. I • VA, "'&\ .• ,.;l --"- l· ,,{. 

### LAURA 

### L. CAIRO Notary Public 

### Nftiliry Public, Slate of Illinois • Note: II is au l"'rl(hMNJIJ
..... 

### amflGi\ n nths. The data is kept on file for up tll three years, Samrles (ir applicable) are kerll fnr Ihree weeks, to the client. If Ihis policy roses a difficulty, I,l ease contact us to make OIher arrangements, If reproduced, our report, musl be reproduced complelely, Any unauthorized alteratinll of Ihis repmt invalidates Ihe Cnllle"I.

### Report To: TESTING - CONSULTING 

### Mr. Steve Preisher Ultra Plating Corporation 345 South Pearl Street Green Bay WI 54306**~f~di)~** -l.: hor""

### ~""Q. c.k. Samuel Wright Laboratory Manager 3158 S. Kolin Ava. Chicago IL 80823·4889 Phono: 773-254·2408 Exton.lon 3041 FAX: 773·254·8881



### Project Number: 05-773 05-28-97 06-10-97 Project Inception: Report Date:

. 'IDENTIFICATION OF MATERIAL: Three (3) samples, identified below. PROCEDURE: All analyses were performed in accordance with the EPA/I EPA approved test pro.cedures as specified in 40 CFR, Part 60, Method 306A. Scientific Control Labs, Inc., is a certified laboratory for analysis of potable water**~IEPA** 

### Cert. #100183), and a certified laboratory for wastewater analysis (State of Washington Cert. #C165, State of Wisconsin DNR #998091930). This means we have a quality control program in effect and that this quality control program Is monitored and reviewed annually by the certifying agencies. BE$ULTS: Sample 10: 

### RUN #1 RUN #2**RU~#3** 

### QUALITY CONTROL**DAIA~** 

### Concentration In 

### ppm fmg/U 

### TOTAL CHROMIUM VOLUME 

### (mil 0.067 250 0.090 269 0.038 265 The samples were analyzed by Graphite Furnace Atomic Absorption for detection of Total Chromium.

SW:clm CERTIFICATION: Sample: Duplicate: Spike: LFB: LRt3: 13.39 ppb 14.69 ppb 

# = 34.53 ppb =

9.66 ppb = -0.63 ppb 

# = relative percent difference 106% spike recovery 96.6% recovery 

## < minimum detection limit Respectfully submitted, 

### = 9.71 

### %

SCIENTIFC CONTROL**LABOR~** 

### TORIES, INC. ,,"
.**~".**

J .,tI' / 

### By
__**~~** 

### __**~~~~~~~~** 

### ______ __ The above statements and report were subscribed and sworn to before me this

.**T~NTH** 

### day of JUNE, 1997.

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## ISOURCE AND SITE DESCR.IPTIONS AIR POllUTION CONTROL PERMIT APPLICA nOJ:{ Form 4530-102 11·93 Infonnation aaacbed? Y.:.j1n) of this form is required by the Department for any air poJlution conb'ol pennit application filed pursuant to s. 144.392 or 414.3925, Wis Slats. Completion of this fonn is mandatory. The Department will not consider or act upOn your application unless you complete and submit this form. It is not the Department's intention to 

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