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Contents: Cover Page Case Narrative Final Report Pages Quality Control Summary Forms 

# SGS North America Inc. Alaska Division Level II Laboratory Data Report Project: Client: SGS Work Order: 3354-003 Red Hill BFSF The Environmental Company, Inc. (TEC) 1095639

# c~SGS Charles Homestead 2009.11.03 15:36:46 -09'00' Charles Homestead Alaska Division General Manager

Chain of Custody/Sample Receipt Forms
Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

## CASE NARRATIVE Print Date: 11/2/2009 Client Name: The Environmental Company, Inc. (TEC) Project Name: 3354-003 Red Hill BFSF Workorder No.: 1095639 

## Sample Comments Refer to the sample receipt form for information on sample condition. Lab Sample ID 1095639002

1095639003

1095639005 1095639006 1095639008 933159

934050

934051

934053 Sample Type 8MS Client Sample ID RHMW2254-WG17 MS 82608 - MS/MSD recoveries for trichlorofluoromethane and carbontetrachloride do not meet QC criteria. Refer to LCS for accuracy. Results for these analytes are estimated in the original sample. AK101 - MS recovery for GRO does not meet QC criteria (biased high). See LCS/LCSD for accuracy. 8MSD RHMW2254-WG17 MSD 82608 - MS/MSD recoveries for trichlorofluoromethane and carbontetrachloride do not meet QC criteria. Refer to LCS for accuracy. Results for these analytes are estimated in the original sample. PS RHMW02-WG17 8015C 102-The pattern is consistent with a weathered middle distillate. PS RHMWA01-WG17 8015C 102-The pattern is consistent with a weathered middle distillate. PS RHMW05-WG17 8015C 102- Unknown hydrocarbon with several peaks is present. CCV CCV for H8N 221891 [VMS/10945) 82608 - CCV recovery for dichlorodifluoromethane does not meet QC criteria {biased high). This analyte was not detected above the PQL in the associated samples LCS LCS for H8N 222065 [VXX/20165) 82608 - LCS recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected above the PQL in the associated samples LCSD LCSD for H8N 222065 [VXX/20165 82608 - LCSD recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected above the PQL in the associated samples CCV CCV for H8N 222066 [VMS/10954) 82608 - CCV recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected above the PQL in the associated samples

SGS North America Inc. Member of SGS Group (Societe GBnBrale de Surveillance)

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# J Print Date: 11/2/2009 Enclosed are the analytical results associated with this workorder. As required by the state ofAlaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS . A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request. The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C). Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities. If you have any questions regarding this report or ifwe can be of any assistance, please contact your SGS Project Manager at 907-562-2343. 

### All work is being provided under 

### SGS general tenns and conditions (http://www.sgs.com/tenns_and_conditions.htm) The following descriptors may be found on your report which will serve to further qualify the data. MDL PQL CL 

## u F 

### J ND B D GT LT 

## a M E 

### R DF JL <Surr> <Surr/IS> QC QA MB LCS(D) MS(D) BMS(D) RPD ICV CCV MSA Method Detection Limit Practical Quantitation Limit (reporting limit). Control Limit Indicates the analyte was analyzed for but not detected. Indicates value that is greater than or equal to the MDL. The quantitation is an estimation . Indicates the analyte is not detected Indicates the analyte is found in a blank associated with the sample. The analyte has exceeded allowable regulatory or control limits. The analyte concentration is the result ofdilution . Greater Than Less Than QC parameter out of acceptance range . A matrix effect was present. The analyte result is above the calibrated range. Rejected Analytical Dilution Factor The analyte was positively identified, but the quantitation is a low estimation . Surrogate QC spiked standard Surrogate/ Internal Standard QC spiked standard Quality Control Quality Assurance Method Blank Laboratory Control Sample (Duplicate) Matrix Spike (Duplicate) Site Specific Matrix Spike (Duplicate) Relative Percent Difference Initial Calibration Verification Continuous Calibration Verification Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified All DRO/RRO analyses are integrated per SOP .

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 9951 B Member of SGS Group

## SAMPLE SUMMARY • Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-003 Red Hill BFSF Workorder No.: 1095639 

## Analytical Methods Method Description 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. AFCEE 3.1 8260 (W) Dissolved Metals by ICP-MS ORO by 8015C (W) GRO(W) 

## Sample ID Cross Reference Lab Sample ID 1095639001 1095639002 1095639003 1095639004 1095639005 1095639006 1095639007 1095639008 1095639009 Client Sample ID RHMW2254-WG17 RHMW2254-WG17 MS RHMW2254-WG17 MSD RHMW03-WG17 RHMW02-WG17 RHMWA01-WG17 RHMW01-WG17 RHMW05-WG17 TB01-WG17 Analytical Method 82700 SIMS SW8260B SW6020 SW8015C SW8015C

Member of SGS Group (Soclete Generale de Surveillance) Print Date: 11/2/2009 4:48 pm

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# J Laboratory ID 1095639007 Client Sample ID RHMW01-WG17 

### Manual Integration Reason Code Descriptions Code 

## 0 M SS 

### BLG RP PIR IT SP RSP FPS 

### BLC PNF Description Original Chromatogram Modified Chromatogram Skimmed surrogate Closed baseline gap Reassign peak name Pattern integration required Included tail Split peak Removed split peak Forced peak start/stop Baseline correction Peak not found by software All DRO/RRO analysis are integrated per SOP. Report of Manual Integrations Analvtical Batch VMS10945 Method SW8260B Print Date: 11/2/2009 4:48 pm Analvte 4-lsopropyltoluene Reason RP

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 I (907) 562.2343 f (907) 561.5301 www.us.sgs.com Member of SGS Group (SoclEttB Generale de Surveillance)

### Client: The Environmental Company, Inc. 1001 Bishop Street, Suite 1400 Honolulu, HI 96813 Attn: Rick Adkisson T: (808)528-1445 F:(808)528-0768 Project: 

### 3354-003 Red Hill BFSF Workorder No.: 

### 1095639

Certification: 

# Laboratory Analytical Report

I certify that this data package is in compliance with the terms and conditions ofthe contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory.

If you have any questions regarding this report, or ifwe can be offurther assistance, please contact your SGS Project Manager. Heather Hall Heather.Hall@sgs.com Quality Assurance Manager

SGS North America Inc. Member of SGS Group

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j .J Client Sample ID : 

### RHMW2254-WG17 SGS Ref. 

### #: 1095639001 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Dissolved Metals by ICP/MS Parameter 

## B!1fil!!! Lead ND Batch Information 

### Analytical Batch: MMS6169 Analytical Method : SW6020 Analysis Daterrime: 11/02/09 00:47 Dilution Factor: 5 

### The Environmental Company, Inc. (TEC)
Collection Datemme: 10/14/09 09: 15 Receipt Datemme: 10/16/09 10:45

1 .00 0.310

Prep Batch: MXX22450 Prep Method: SW3010A Prep Daterrime: 10/26/09 17:30 ug/L 

### 5

SGS North Ame rice Inc. Member of SGS Group (Socil!tl! Gl!nerale de Surveillance) 

### Print Date: 11/2/2009 4:48 pm

Analvtical**~** qualifiers 

### MMS6169 MXX22450 Initial Prep Wt.Nol. : 50 ml Prep Extract Vol. : 50 ml Container ID:1095639001-G Analyst: NRB

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW2254-WG17 SGS Ref.#: 1095639001 Project ID : 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Volatile Fuels Department Parameter Gasoline Range Organics 4-Bromofluorobenzene <surr> Batch Information Analytical Batch: VFC9728 Analytical Method: SW8015C Analysis DatefTime: 10/24/09 19:02 Dilution Factor: 1 ND 95.3

SGS North America Inc. Collection DatefTime: 10/14/09 09:15 Receipt DatefTime: 10/16/09 10:45

Analytical Prep DF Batch Batch Qualifiers 100 50-150 30.0

Prep Batch: VXX20181 Prep Method : SW5030B Prep DatefTime: 10/24/09 13:29 ug/l 

### "lo

Member of SGS Group (SociBtB Generale de Surveillance) VFC9728 VFC9728 VXX20181 VXX20181 Initial Prep Wt.Nol. : 5 ml Prep Extract Vol.: 5 ml Container ID:1095639001-B Analyst: KPW

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J The Environmental Company, Inc. (TEC) Client Sample ID: 

### RHMW2254-WG17 SGS Ref. #: 1095639001 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Semivolatile Organic Fuels Department Parameter Diesel Range Organics 5a Androstane <surr> Batch Information Analytical Batch: XFC8990 Analytical Method : SW8015C Analysis Daterfime: 10/26/09 12:29 Dilution Factor: 1 ND 73.5

SGS North America Inc. Collection Daterfime: 10/14/09 09:15 Receipt Date!Time: 10/16/09 10:45

0.421 50-150 0.158

Prep Batch : XXX21847 Prep Method : SW3520C Prep Daterfime: 10/19/09 10:35 mg/L 

### "lo

Member of SGS Group (Soclete Generate de Surveillance) Print Date: 11/2/2009 4:48 pm

Analytical Batch XFC8990 XFC8990 XXX21847 XXX21847 qualifiers

Initial Prep Wt.Nol. : 950 ml Prep Extract Vol.: 1 ml Container ID: 1095639001-H Analyst: KDC

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW2254-WG17 SGS Ref. 

### #: 1095639001 Collection Date/Time: 10/14/09 09:15 Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Anal:ttical Prep Parameter Result PQUCL MDL**~** DF Batch Batch qualifiers Benzene ND 0.400 0.120 ug/L VMS10954 VXX20165 Toluene ND 1.00 0.310 ug/L VMS10954 VXX20165 Ethylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 n-Butylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 1,4-Dichlorobenzene ND 0.500 0.150 ug/L VMS10954 VXX20165 1,2-Dichloroethane ND 0.500 0.150 ug/L VMS10954 VXX20165 1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 4-Chlorotoluene ND 1.00 0.310 ug/L VMS10954 VXX20165 Chlorobenzene ND 0.500 0.150 ug/L VMS10954 VXX20165 4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L VMS10954 VXX20165 cis-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10954 VXX20165 4-lsopropyltoluene ND 1.00 0.310 ug/L VMS10954 VXX20165 cis-1,3-Dichloropropene ND 0.500 0.150 ug/L VMS10954 VXX20165 n-Propylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 Styrene ND 1.00 0.310 ug/L VMS10954 VXX20165 Dibromomethane ND 1.00 0.310 ug/L VMS10954 VXX20165 trans-1,3-Dichloropropene ND 1.00 0.310 ug/L VMS10954 VXX20165 1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 Acetone ND 10.0 3.10 ug/L VMS10954 VXX20165 1, 1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10954 VXX20165 1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L VMS10954 VXX20165 Methyl-I-butyl ether ND 5.00 1.50 ug/L VMS10954 VXX20165 Tetrachloroethene ND 1.00 0.310 ug/L VMS10954 VXX20165 Dibromochloromethane ND 0.500 0.150 ug/L VMS10954 VXX20165 1,3-Dichloropropane ND 0.400 0.120 ug/L VMS10954 VXX20165 1,2-Dibromoethane ND 1.00 0.310 ug/L VMS10954 VXX20165 Carbon tetrachloride ND 1.00 0.310 ug/L VMS10954 VXX20165 1, 1, 1,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10954 VXX20165 Chloroform ND 1.00 0.300 ug/L VMS10954 VXX20165 Bromobenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 Chloromethane ND 1.00 0.310 ug/L VMS10954 VXX20165 1,2,3-Trichloropropane ND 1.00 0.310 ug/L VMS10954 VXX20165 Bromomethane ND 3.00 0.940 ug/L VMS10954 VXX20165 Bromochloromethane ND 1.00 0.310 ug/L VMS10954 VXX20165 Vinyl chloride ND 1.00 0.310 ug/L VMS10954 VXX20165 Dichlorodifluoromethane ND 1.00 0.310 ug/L VMS10954 VXX20165 SGS North America Inc. Member of SGS Group (Soclete Generale de Surveillance)

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# J The Environmental Company, Inc. (TEC) Client Sample ID: 

### RHMW2254-WG17 SGS Ref.#: 1095639001 Collection DatefTime: 10/14/09 09: 15 Project ID: 3354-003 Red Hill BFSF Receipt DatefTime: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Parameter Result PQUCL MDL Units 

### OF Chloroethane ND 1.00 0.310 ug/L 1 sec-Butylbenzene ND 1.00 0.310 ug/L 1 Bromodichloromethane 

### ND 0 .500 0 .1 50 ug/L 1, 1-Dichloroethene ND 1.00 0.310 ug/L 2-Butanone (MEK) ND 10.0 3.10 ug/L Methylene chloride ND 5.00 1 .00 ug/L Trichlorofluoromethane ND 1.00 0.310 ug/L P & M-Xylene ND 2.00 0.620 ug/L Naphthalene ND 2.00 0.620 ug/L a-Xylene ND 1.00 0.310 ug/L Bromoform ND 1.00 0.310 ug/L 1-Chlorohexane ND 1 .00 0.310 ug/L 1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L tert-Butylbenzene ND 1.00 0.310 ug/L 1, 1, 1-Trichloroethane ND 1.00 0.310 ug/L 1, 1-Dichloroethane ND 1.00 0.310 ug/L 2-Chlorotoluene ND 1.00 0.310 ug/L Trichloroethene ND 1 .00 0.310 ug/L trans-1,2-Dichloroethene ND 1 .00 0.310 ug/L 1,2-Dichlorobenzene ND 1.00 0.310 ug/L 2,2-Dichloropropane ND 1 .00 0.310 ug/L Hexachlorobutadiene ND 1 .00 0.310 ug/L lsopropylbenzene (Cumene) ND 1 .00 0.310 ug/L 1,2-Dichloropropane ND 1 .00 0.310 ug/L 1,1-Dichloropropene ND 1.00 0.310 ug/L 1, 1,2-Trichloroethane ND 1.00 0.310 ug/L 1,3-Dichlorobenzene ND 1 .00 0.310 ug/L 1,2,3-Trichlorobenzene ND 1 .00 0.310 ug/L Xylenes (total) ND 2.00 1 .00 ug/L 1,2-Dichloroethane-D4 <surr> 103 73-120 % Toluene-dB <surr> 101 80-120 % 4-Bromofluorobenzene <surr> 104 76-120 %

SGS North America Inc. Member of SGS Group (Soclete Generale de Surveillance) Print Date: 11/2/2009 4:48 pm**Ani!l~tical** Prep Batch**~** Qualifieri VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165 VMS10954 VXX20165

### The Environmental Company, Inc. (TEC) Client Sample ID: 

### RHMW2254-WG17 SGS Ref.#: 1095639001 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Parameter Batch Information Analytical Batch: VMS10954 Analytical Method: SW8260B Analysis Date/Time: 10/20/09 18:10 Dilution Factor: 1

SGS North America Inc. Collection Date/Time: 10/14/09 09: 15 Receipt Date/Time: 10/16/09 10:45

Prep Batch : VXX20165 Prep Method: SW5030B Prep Date/Time: 10/20/09 08:22

Member of SGS Group (Societe Generale de Surveillance) Print Date: 11/2/2009 4:48 pm



### Analytical Batch Qualifiers Initial Prep Wt.Nol.: 5 ml Prep Extract Vol.: 5 ml Container ID:1095639001-E Analyst: SCl

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW2254-WG17 SGS Ref. 

### #: 1095639001 Collection Date/Time: 10/14/09 09:15 Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground) 

### Polynuclear Aromatics GC/MS**Anal~tical** 

## f!m Parameter**~** PgUCL MDL 

## .!.l.n!!! OF Batch Batch qualifiers 

# l Acenaphthylene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Acenaphthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Fluorene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Phenanthrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Anthracene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Fluoranthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Pyrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Benzo(a)Anthracene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Chrysene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Benzo(b)Fluoranthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Benzo(k)fluoranthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Benzo[a]pyrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 lndeno[1,2,3-c,d] pyrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Dibenzo[a,h]anthracene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Benzo(g,h,i]perylene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Naphthalene ND 0.114 0.0352 ug/l XMS5164 XXX21842 1-Methylnaphthalene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 2-Methylnaphthalene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 Terphenyl-d14 <surr> 104 50-135 

### % XMS5164 XXX21842 Batch Information Analytical Batch: XMS5164 Prep Batch : XXX21842 Initial Prep Wt.Nol. : 880 ml Analytical Method: 82700 SIMS Prep Method : SW3520C Prep Extract Vol.: 1 ml Analysis Date/Time: 10/25/09 18:49 Prep Date/Time: 10/18/09 08:40 Container 10:1095639001-J Dilution Factor: 1 Analyst: JOH



# J SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 Member of SGS Group (Societe GBnerale de Surveillance)Client Sample ID: 

### RHMW03-WG17 SGS Ref. 

### #: 1095639004 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Dissolved Metals by ICP/MS Parameter Lead Batch Information Analytical Batch: MMS6169 Analytical Method : SW6020 Analysis Date/Time: 11/02/09 00:58 Dilution Factor: 5 

### The Environmental Company, Inc. (TEC)
Collection Date/Time: 10/14/09 11 :05 Receipt Date/Time: 10/16/09 10:45 Print Date: 11/2/2009 4:48 pm

Analytical Prep DF Batch Batch Qualifiers ND

SGS North America Inc. 1.00 0.310 Prep Batch : MXX22450 Prep Method : SW3010A Prep Date/Time: 10/26/09 17:30 ug/L

Member of SGS Group (Societe Generale de Surveillance) 

### 5 MMS6169 MXX22450 Initial Prep Wt.Nol.: 50 ml Prep Extract Vol. : 50 ml Container ID:1095639004-G Analyst: NRB

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### RHMW03-WG17 SGS Ref. 

### #: 1095639004 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Volatile Fuels Department Parameter Gasoline Range Organics 4-Bromofluorobenzene <surr> Batch Information Analytical Batch : VFC9728 Analytical Method : SW8015C Analysis DatefTime: 10/24/09 20:10 Dilution Factor: 1 

### The Environmental Company, Inc. (TEC)



## ND 99.7

SGS North America Inc. Collection DatefTime: 10/14/09 11 :05 Receipt DatefTime: 10/16/09 10:45

100 50-150 30.0

Prep Batch: VXX20181 Prep Method: SW5030B Prep DatefTime: 10/24/09 13:29 ug/l 

### %

Member of SGS Group (Soclete Generale de Surveillance) Print Date: 11/2/2009 4:48 pm

Analytical Batch VFC9728 VFC9728 VXX20181 VXX20181 qualifiers

Initial Prep Wt.Nol. : 5 ml Prep Extract Vol. : 5 ml Container ID :1095639004-B Analyst: KPW

### The Environmental Company, Inc. (TEC) Client Sample ID: 

### RHMW03-WG17 SGS Ref. 

### #: 1095639004 Project ID : 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Semivolatlle Organic Fuels Department Parameter Diesel Range Organics Sa Androstane <surr> Batch Information Analytical Batch: XFC8990 Analytical Method : SW8015C Analysis Date/Time: 10/26/09 13:01 Dilution Factor: 1 ND 79

SGS North America Inc. Collection Date/Time: 10/14/09 11 :05 Receipt Date/Time: 10/16/09 10:45

0.435 50-150 0. 163

Prep Batch : XXX21847 Prep Method: SW3520C Prep Date/Time: 10/19/09 10:35 mg/l %

Member of SGS Group (Societe Generals de Surveillance) Print Date: 11/2/2009 4:48 pm

Analytical Batch XFC8990 XFC8990 XXX21847 XXX21847 Qualifiers

Initial Prep Wt.Nol. : 920 ml Prep Extract Vol. : 1 ml Container ID:1095639004-H Analyst: KOC

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### RHMW03-WG17 SGS Ref. 

### #: 1095639004 Project ID : 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### The Environmental Company, Inc. (TEC)
Collection Date/Time: 10/14/09 11 :05 Receipt Date/Time: 10/16/09 10:45


### Volatile Gas Chromatography/Mass Spectroscopy



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### Benzene Toluene Ethylbenzene n-Butylbenzene 1,4-Dichlorobenzene 1,2-Dichloroethane 1 ,3,5-Trimethylbenzene 4-Chlorotoluene Chlorobenzene 4-Methyl-2-pentanone (MIBK) cis-1,2-Dichloroethene 4-lsopropyltoluene cis-1,3-Dichloropropene n-Propylbenzene Styrene Dibromomethane trans-1,3-Dichloropropene 1,2,4-Trichlorobenzene Acetone 1, 1,2,2-Tetrachloroethane 1,2-Dibromo-3-chloropropane Methyl-t-butyl ether Tetrachloroethene Dibromochloromethane 1,3-Dichloropropane 1,2-Dibromoethane Carbon tetrachloride 1, 1 ,1 ,2-Tetrachloroethane Chloroform Bromobenzene Chloromethane 1,2,3-Trichloropropane Bromomethane Bromochloromethane 

# _J

# ~::~**1:r~~~~:romethane** 

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# J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND SGS North America Inc. 

### 0.400 1 .00 1 .00 1 .00 0.500 0.500 1 .00 1 .00 0.500 10.0 1 .00 1 .00 0.500 1 .00 1 .00 1 .00 1 .00 1 .00 10.0 0.500 2.00 5.00 1 .00 0.500 0.400 1.00 1 .00 0.500 1 .00 1 .00 1 .00 1.00 3.00 1 .00 1.00 1 .00 0.120 0.310 0.310 0.310 0. 150 0.150 0.310 0.310 0.150 3.10 0.310 0.310 0. 150 0.310 0.310 0.310 0.310 0.310 3.10 0. 150 0.620 1 .50 0.310 0. 150 0. 120 0.310 0.310 0.150 0.300 0.310 0.310 0.310 0.940 0.310 0.310 0.310 ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L

Member of SGS Group (Soclete Generale de Surveillance) 

### Print Date: 11/2/2009 4:48 pm

Analytical Batch 

### VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 VMS10945 VXX20145 qualifiers

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW03-WG17 SGS Ref. #: 1095639004 Collection Date!Time: 10/14/09 11 :05 Project ID : 3354-003 Red Hill BFSF Receipt Date!Time: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Anal:dical 

## f!m Parameter Result PQUCL MDL 

## .!!!!i!! DF Batch**~** qualifiers Chloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 sec-Butylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 Bromodichloromethane ND 0.500 0.150 ug/L VMS10945 VXX20145 1 ,1-Dichloroethene ND 1 .00 0.310 ug/L VMS10945 VXX20145 2-Butanone (MEK) ND 10.0 3. 10 ug/L VMS10945 VXX20145 Methylene chloride ND 5.00 1.00 ug/L VMS10945 VXX20145 Trichlorofluoromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 P & M -Xylene ND 2.00 0.620 ug/L VMS10945 VXX20145 Naphthalene ND 2.00 0.620 ug/L VMS10945 VXX20145 a-Xylene ND 1.00 0.310 ug/L VMS10945 VXX20145 Bromoform ND 1.00 0.310 ug/L VMS10945 VXX20145 1-Chlorohexane ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2,4-Trimethylbenzene ND 1 .00 0.310 ug/L VMS10945 VXX20145 tert-Butylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 1, 1, 1-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 1,1-Dichloroethane ND 1.00 0 .310 ug/L VMS10945 VXX20145 2-Chlorotoluene ND 1 .00 0.310 ug/L VMS10945 VXX20145 Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 trans-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 2,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 Hexachlorobutadiene ND 1.00 0.310 ug/L VMS10945 VXX20145 lsopropylbenzene (Cumene) ND 1.00 0.310 ug/L VMS10945 VXX20145 1 ,2-Dichloropropane ND 1 .00 0.310 ug/L VMS10945 VXX20145 1, 1-Dichloropropene ND 1.00 0 .310 ug/L VMS10945 VXX20145 1 ,1,2-Trichloroethane ND 1 .00 0.310 ug/L VMS10945 VXX20145 1,3-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 Xylenes (total) ND 2.00 1 .00 ug/L VMS10945 VXX20145 1,2-Dichloroethane-D4 <surr> 96.9 73-120 

### % VMS10945 VXX20145 Toluene-dB <surr> 104 80-120 

### % VMS10945 VXX20145 4-Bromofluorobenzene <surr> 106 76-120 

### % VMS10945 VXX20145

SGS North America Inc. Member of SGS Group (Societe Generale de Surveillance)Client Sample ID : 

### RHMW03-WG17 SGS Ref. 

### #: 1095639004 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### The Environmental Company, Inc. (TEC)
Collection Date/Time: 10/14/09 11 :05 Receipt Date/Time: 10/16/09 10:45


### Volatile Gas Chromatography/Mass Spectroscopy Parameter Batch Information 

# 1 Analytical Batch : VMS10945 Analytical Method: SW8260B Analysis Date/Time: 10/19/09 22:38 Dilution Factor: 1



# 1 

# 1 

# ) 

# ] J 

# j SGS North America Inc. Prep Batch: VXX20145 Prep Method: SW5030B Prep Date/Time: 10/19/09 08:11

Member of SGS Group (Societe Generale de Surveillance) Print Date: 11/2/2009 4:48 pm

Analytical**~** qualifiers Initial Prep Wt.Nol. : 5 ml Prep Extract Vol. : 5 ml Container ID:1095639004-A Analyst: SCl

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW03-WG17 SGS Ref. 

### #: 1095639004 Collection DatefTime: 10/14/09 11 :05 Project ID : 3354-003 Red Hill BFSF Receipt DatefTime: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground} 

### Polynuclear Aromatics GC/MS Anall£tical Prep Parameter 

## .!fil!!l! PQUCL MDL Units DF Batch Batch Qualifiers Acenaphthylene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Acenaphthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Fluorene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Phenanthrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Anthracene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Fluoranthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Pyrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Benzo(a}Anthracene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Chrysene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Benzo(b]Fluoranthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Benzo(k)fluoranthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Benzo[a)pyrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 lndeno[1 ,2,3-c,d] pyrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Dibenzo[a,h]anthracene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Benzo[g ,h,i]perylene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Naphthalene ND 0.112 0.0348 ug/l XMS5164 XXX21842 1-Methylnaphthalene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 2-Methylnaphthalene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 Terphenyl-d14 <surr> 99 50-135 

### % XMS5164 XXX21842 Batch Information Analytical Batch: XMS5164 Prep Batch : XXX21842 Initial Prep Wt.Nol.: 890 ml Analytical Method : 82700 SIMS Prep Method: SW3520C Prep Extract Vol. : 1 ml Analysis DatefTime: 10/25/09 20:33 Prep DatefTime: 10/18/09 08:40 Container 10:1095639004-J Dilution Factor: 1 Analyst: JOH

SGS North America Inc. Member of SGS Group (Societe Generale de Surveillance)

# l l

Client Sample ID: 

### RHMW02-WG17 SGS Ref.#: 1095639005 

# J Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Dissolved Metals by ICP/MS Parameter 

# cLead Batch Information Analytical Batch: MMS6169 Analytical Method : SW6020 Analysis Date/Time: 11/02/09 01 :00 Dilution Factor: 5 

# J



# l

J The Environmental Company, Inc. (TEC)



## Bm!l! ND

SGS North America Inc. Collection Date/Time: 10/13/09 16:15 Receipt Date/Time: 10/16/09 10:45

1.00 0.310

Prep Batch: MXX22450 Prep Method: SW301 OA Prep Date/Time: 10/26/09 17:30 ug/L

Member of SGS Group (Soclete Generale de Surveillance) 

### 5 Print Date: 11/2/2009 4:48 pm

Analvtical**~** qualifiers MMS6169 MXX22450 Initial Prep Wt.Nol.: 50 ml Prep Extract Vol.: 50 ml Container ID: 1095639005-G Analyst: NRBClient Sample ID: 

### RHMW02-WG17 SGS Ref. 

### #: 1095639005 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Volatile Fuels Department Parameter Gasoline Range Organics 4-Bromofluorobenzene <surr> Batch Information Analytical Batch: VFC9728 Analytical Method : SW8015C Analysis Date/Time: 10/24/09 20:33 Dilution Factor: 1 

### The Environmental Company, Inc. (TEC)
Collection Date/Time: 10/13/09 16: 15 Receipt Date/Time: 10/16/09 10:45 Print Date: 11/2/2009 4:48 pm

Analytical Prep DF Batch Batch Qualifiers 36.9 

### J 119

SGS North America Inc. 100 50-150 30.0

Prep Batch: VXX20181 Prep Method: SW5030B Prep Date/Time: 10/24/09 13:29 ug/l %

Member of SGS Group (Societe Generale de Surveillance) VFC9728 VFC9728 VXX20181 VXX20181 Initial Prep Wt.Nol. : 5 ml Prep Extract Vol.: 5 ml Container ID:1095639005-B Analyst: KPW

# l 

# l l
l ] 

# l 

# l 

# 0

1

J The Environmental Company, Inc. (TEC) Client Sample ID: 

### RHMW02-WG17 SGS Ref. 

### #: 1095639005 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Semivolatile Organic Fuels Department Parameter Diesel Range Organics 5a Androstane <surr> Batch Information Analytical Batch: XFC8990 Analytical Method: SW8015C Analysis Date/Time: 10/26/09 13:12 Dilution Factor: 1 2.57 74.4

SGS North America Inc. Collection Date/Time: 10/13/09 16:15 Receipt Date/Time: 10/16/09 10:45

0.449 50-150 0.169

Prep Batch : XXX21847 Prep Method : SW3520C Prep Date/Time: 10/19/09 10:35 mg/l %

Member of SGS Group (Sochlte Generate de Surveillance) Print Date: 11/2/2009 4:48 pm

Analytical Batch XFC8990 XFC8990 XXX21847 XXX21847 qualifiers

Initial Prep Wt.Nol.: 890 ml Prep Extract Vol. : 1 ml Container 10:1095639005-H Analyst: KOC

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW02-WG17 SGS Ref. 

### #: 1095639005 Collection Date/Time: 10/13/09 16:15 Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Anall£tical Prep Parameter 

## Bm!l! PQUCL MDL Units DF**~** Batch qualifiers Benzene ND 0.400 0.120 ug/L VMS10945 VXX20145 Toluene ND 1.00 0.310 ug/L VMS10945 VXX20145 Ethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 n-Butylbenzene 2.98 1.00 0.310 ug/L VMS10945 VXX20145 1,4-Dichlorobenzene ND 0.500 0.150 ug/L VMS10945 VXX20145 1,2-Dichloroethane ND 0.500 0.150 ug/L VMS10945 VXX20145 1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 4-Chlorotoluene ND 1.00 0.310 ug/L VMS10945 VXX20145 Chlorobenzene ND 0.500 0.150 ug/L VMS10945 VXX20145 4-Methyl-2:pentanone (MIBK) ND 10.0 3.10 ug/L VMS10945 VXX20145 cis-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 4-lsopropyltoluene ND 1.00 0.310 ug/L VMS10945 VXX20145 cis-1,3-Dichloropropene ND 0.500 0.150 ug/L VMS10945 VXX20145 n-Propylbenzene 4.16 1.00 0.310 ug/L VMS10945 VXX20145 Styrene ND 1.00 0.310 ug/L VMS10945 VXX20145 Dibromomethane ND 1.00 0.310 ug/L VMS10945 VXX20145 trans-1,3-Dichloropropene ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 Acetone ND 10.0 3.10 ug/L VMS10945 VXX20145 1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10945 VXX20145 1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L VMS10945 VXX20145 Methyl-I-butyl ether ND 5.00 1.50 ug/L VMS10945 VXX20145 Tetrachloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 Dibromochloromethane ND 0.500 0.150 ug/L VMS10945 VXX20145 1,3-Dichloropropane ND 0.400 0.120 ug/L VMS10945 VXX20145 1,2-Dibromoethane ND 1.00 0.310 ug/L VMS10945 VXX20145 Carbon tetrachloride ND 1.00 0.310 ug/L VMS10945 VXX20145 1, 1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10945 VXX20145 Chloroform ND 1.00 0.300 ug/L VMS10945 VXX20145 Bromobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 Chloromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2,3-Trichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 Bromomethane ND 3.00 0.940 ug/L VMS10945 VXX20145 Bromochloromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 Vinyl chloride ND 1.00 0.310 ug/L VMS10945 VXX20145 Dichlorodifluoromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 SGS North America Inc. Member of SGS Group (Societe Generale de Surveillance)

# 1 

# l l The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW02-WG17 SGS Ref. 

### #: 1095639005 Collection Date/Time: 10/13/09 16:15 Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Analli'.tical Prep Parameter**~** PQUCL MDL 

## .!.!.nim DF**~ ~**  qualifiers Chloroethane ND 1.00 0.310 ug/L 1 VMS10945 VXX20145 sec-Butylbenzene 4.71 1.00 0.310 ug/L 1 VMS10945 VXX20145 Bromodichloromethane ND 0.500 0.150 ug/L VMS10945 VXX20145 1, 1-Dichloroethene ND 1 .00 0.310 ug/L VMS10945 VXX20145 2-Butanone (MEK) ND 10.0 3.10 ug/L VMS10945 VXX20145 Methylene chloride ND 5.00 1 .00 ug/L VMS10945 VXX20145 Trichlorofluoromethane ND 1 .00 0.310 ug/L VMS10945 VXX20145 P & M-Xylene ND 2.00 0.620 ug/L VMS10945 VXX20145 Naphthalene 23.3 2.00 0.620 ug/L VMS10945 VXX20145 o-Xylene ND 1.00 0.310 ug/L VMS10945 VXX20145 

# ] Bromoform ND 1.00 0.310 ug/L VMS10945 VXX20145 1-Chlorohexane ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 tert-Butylbenzene 0.820 

### J 1 .00 0.310 ug/L VMS10945 VXX20145 1, 1,1-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 1 ,1-Dichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 2-Chlorotoluene ND 1 .00 0.310 ug/L VMS10945 VXX20145 Trichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 trans-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

# 1 2,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 Hexachlorobutadiene ND 1.00 0.310 ug/L VMS10945 VXX20145 lsopropylbenzene (Cumene) 3.49 1 .00 0.310 ug/L VMS10945 VXX20145 1,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 1, 1-Dichloropropene ND 1.00 0.310 ug/L VMS10945 VXX20145 1, 1,2-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 1,3-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

# l Xylenes (total) ND 2.00 1.00 ug/L VMS10945 VXX20145 1,2-Dichloroethane-D4 <surr> 103 73-120 

### % VMS10945 VXX20145 Toluene-dB <surr> 101 80-120 

### % VMS10945 VXX20145 

# J 4-Bromofluorobenzene <surr> 105 76-120 

### % VMS10945 VXX20145



## J 

# J SGS North America Inc. Member of SGS Group (Soclete Generale do Surveillance)



# J

### The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm Client Sample ID: 

### RHMW02-WG17 SGS Ref. 

### #: 1095639005 Project ID: 3354-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground) 

### Volatile Gas Chromatography/Mass Spectroscopy Parameter Batch Information Analytical Batch: VMS10945 Analytical Method: SW8260B Analysis Date!Time: 10/19/09 23: 11 Dilution Factor: 1

SGS North America Inc. Collection Date!Time: 10/13/09 16: 15 Receipt Date!Time: 10/16/09 10:45

Analvtical Prep OF Batch Batch Qualifiers Prep Batch: VXX20145 Prep Method: SW5030B Prep Date!Time: 10/19/09 08: 11

Member of SGS Group (Soclete Generale de Surveillance) Initial Prep Wt.Nol.: 5 ml Prep Extract Vol.: 5 ml Container ID:1095639005-A Analyst: SCl