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Released by: 

Contents: 

Cover Page 

Case Narrative 

Final Report Pages 

Quality Control Summary Forms 

SGS North America Inc. 

Alaska Division 

Level II Laboratory Data Report 

Project: 

Client: 

SGS Work Order: 

3354-003 Red Hill BFSF 

The Environmental Company, Inc. (TEC) 

1095639 

c~SGS 

Charles 

Homestead 

2009.11.03 

15:36:46 -09'00' 

Charles Homestead 

Alaska Division General Manager 

Chain of Custody/Sample Receipt Forms 

Note: 

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 
CASE NARRATIVE Print Date: 11/2/2009 

Client Name: The Environmental Company, Inc. (TEC) 

Project Name: 3354-003 Red Hill BFSF 

Workorder No.: 1095639 

Sample Comments 

Refer to the sample receipt form for information on sample condition. 

Lab Sample ID 

1095639002 

1095639003 

1095639005 

1095639006 

1095639008 

933159 

934050 

934051 

934053 

Sample Type 

8MS 

Client Sample ID 

RHMW2254-WG17 MS 

82608 - MS/MSD recoveries for trichlorofluoromethane and carbontetrachloride do not meet QC criteria. Refer to LCS for 

accuracy. Results for these analytes are estimated in the original sample. 

AK101 - MS recovery for GRO does not meet QC criteria (biased high). See LCS/LCSD for accuracy. 

8MSD RHMW2254-WG17 MSD 

82608 - MS/MSD recoveries for trichlorofluoromethane and carbontetrachloride do not meet QC criteria. Refer to LCS for 

accuracy. Results for these analytes are estimated in the original sample. 

PS RHMW02-WG17 

8015C 102-The pattern is consistent with a weathered middle distillate. 

PS RHMWA01-WG17 

8015C 102-The pattern is consistent with a weathered middle distillate. 

PS RHMW05-WG17 

8015C 102- Unknown hydrocarbon with several peaks is present. 

CCV CCV for H8N 221891 [VMS/10945) 

82608 - CCV recovery for dichlorodifluoromethane does not meet QC criteria {biased high). This analyte was not detected 

above the PQL in the associated samples 

LCS LCS for H8N 222065 [VXX/20165) 

82608 - LCS recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected above 

the PQL in the associated samples 

LCSD LCSD for H8N 222065 [VXX/20165 

82608 - LCSD recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected 

above the PQL in the associated samples 

CCV CCV for H8N 222066 [VMS/10954) 

82608 - CCV recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected 

above the PQL in the associated samples 

SGS North America Inc. 

Member of SGS Group (Societe GBnBrale de Surveillance) 
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Print Date: 11/2/2009 

Enclosed are the analytical results associated with this workorder. 

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request. 

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C). 

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities. 

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343. All work is being provided under SGS general tenns and conditions (http://www.sgs.com/tenns_and_conditions.htm) 

The following descriptors may be found on your report which will serve to further qualify the data. 

MDL 

PQL 

CL 

u 

F 

J 

ND 

B 

D 

GT 

LT 

a 

M 

E 

R 

DF 

JL 

<Surr> 

<Surr/IS> 

QC 

QA 

MB 

LCS(D) 

MS(D) 

BMS(D) 

RPD 

ICV 

CCV 

MSA 

Method Detection Limit 

Practical Quantitation Limit (reporting limit). 

Control Limit 

Indicates the analyte was analyzed for but not detected. 

Indicates value that is greater than or equal to the MDL. 

The quantitation is an estimation. 

Indicates the analyte is not detected 

Indicates the analyte is found in a blank associated with the sample. 

The analyte has exceeded allowable regulatory or control limits. 

The analyte concentration is the result of dilution. 

Greater Than 

Less Than 

QC parameter out of acceptance range. 

A matrix effect was present. 

The analyte result is above the calibrated range. 

Rejected 

Analytical Dilution Factor 

The analyte was positively identified, but the quantitation is a low estimation. 

Surrogate QC spiked standard 

Surrogate/ Internal Standard QC spiked standard 

Quality Control 

Quality Assurance 

Method Blank 

Laboratory Control Sample (Duplicate) 

Matrix Spike (Duplicate) 

Site Specific Matrix Spike (Duplicate) 

Relative Percent Difference 

Initial Calibration Verification 

Continuous Calibration Verification 

Method of Standard Addition 

Notes: Soil samples are reported on a dry weight basis unless otherwise specified 

All DRO/RRO analyses are integrated per SOP. 

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 9951 B 

Member of SGS Group 
SAMPLE SUMMARY 

• Client Name: The Environmental Company, Inc. (TEC) 

Project Name: 3354-003 Red Hill BFSF 

Workorder No.: 1095639 

Analytical Methods 

Method Description 

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 

AFCEE 3.1 8260 (W) 

Dissolved Metals by ICP-MS 

ORO by 8015C (W) 

GRO(W) 

Sample ID Cross Reference 

Lab Sample ID 

1095639001 

1095639002 

1095639003 

1095639004 

1095639005 

1095639006 

1095639007 

1095639008 

1095639009 

Client Sample ID 

RHMW2254-WG 17 

RHMW2254-WG17 MS 

RHMW2254-WG17 MSD 

RHMW03-WG17 

RHMW02-WG17 

RHMWA01-WG17 

RHMW01-WG17 

RHMW05-WG17 

TB01-WG17 

Analytical Method 

82700 SIMS 

SW8260B 

SW6020 

SW8015C 

SW8015C 

Member of SGS Group (Soclete Generale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 
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Laboratory ID 

1095639007 

Client Sample ID 

RHMW01-WG17 

Manual Integration Reason Code Descriptions 

Code 

0 

M 

SS 

BLG 

RP 

PIR 

IT 

SP 

RSP 

FPS 

BLC 

PNF 

Description 

Original Chromatogram 

Modified Chromatogram 

Skimmed surrogate 

Closed baseline gap 

Reassign peak name 

Pattern integration required 

Included tail 

Split peak 

Removed split peak 

Forced peak start/stop 

Baseline correction 

Peak not found by software 

All DRO/RRO analysis are integrated per SOP. 

Report of Manual Integrations 

Analvtical Batch 

VMS10945 

Method 

SW8260B 

Print Date: 11/2/2009 4:48 pm 

Analvte 

4-lsopropyltoluene 

Reason 

RP 

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 

I (907) 562.2343 f (907) 561.5301 www.us.sgs.com 

Member of SGS Group (SoclEttB Generale de Surveillance) 
Client: The Environmental Company, Inc. 

1001 Bishop Street, Suite 1400 

Honolulu, HI 96813 

Attn: Rick Adkisson 

T: (808)528-1445 F:(808)528-0768 

Project: 3354-003 Red Hill BFSF 

Workorder No.: 1095639 

Certification: 

Laboratory Analytical Report 

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory. 

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager. 

Heather Hall 

Heather.Hall@sgs.com 

Quality Assurance Manager 

SGS North America Inc. 

Member of SGS Group 
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Client Sample ID: RHMW2254-WG17 

SGS Ref. #: 1095639001 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Dissolved Metals by ICP/MS 

Parameter B!1fil!!! 

Lead ND 

Batch Information 

Analytical Batch: MMS6169 

Analytical Method: SW6020 

Analysis Daterrime: 11/02/09 00:47 

Dilution Factor: 5 

The Environmental Company, Inc. (TEC) 

Collection Datemme: 10/14/09 09:15 

Receipt Datemme: 10/16/09 10:45 

1.00 0.310 

Prep Batch: MXX22450 

Prep Method: SW3010A 

Prep Daterrime: 10/26/09 17:30 

ug/L 5 

SGS North Ame rice Inc. 

Member of SGS Group (Socil!tl! Gl!nerale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analvtical 

~ qualifiers 

MMS6169 MXX22450 

Initial Prep Wt.Nol.: 50 ml 

Prep Extract Vol. : 50 ml 

Container ID:1095639001-G 

Analyst: NRB 
The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW2254-WG17 

SGS Ref.#: 1095639001 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Volatile Fuels Department 

Parameter 

Gasoline Range Organics 

4-Bromofluorobenzene <surr> 

Batch Information 

Analytical Batch: VFC9728 

Analytical Method: SW8015C 

Analysis DatefTime: 10/24/09 19:02 

Dilution Factor: 1 

ND 

95.3 

SGS North America Inc. 

Collection DatefTime: 10/14/09 09: 15 

Receipt DatefTime: 10/16/09 10:45 

Analytical Prep 

DF Batch Batch Qualifiers 

100 

50-150 

30.0 

Prep Batch: VXX20181 

Prep Method: SW5030B 

Prep DatefTime: 10/24/09 13:29 

ug/l 

"lo 

Member of SGS Group (SociBtB Generale de Surveillance) 

VFC9728 

VFC9728 

VXX20181 

VXX20181 

Initial Prep Wt.Nol.: 5 ml 

Prep Extract Vol.: 5 ml 

Container ID:1095639001-B 

Analyst: KPW 
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The Environmental Company, Inc. (TEC) 

Client Sample ID: RHMW2254-WG17 

SGS Ref. #: 1095639001 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Semivolatile Organic Fuels Department 

Parameter 

Diesel Range Organics 

5a Androstane <surr> 

Batch Information 

Analytical Batch: XFC8990 

Analytical Method: SW8015C 

Analysis Daterfime: 10/26/09 12:29 

Dilution Factor: 1 

ND 

73.5 

SGS North America Inc. 

Collection Daterfime: 10/14/09 09:15 

Receipt Date!Time: 10/16/09 10:45 

0.421 

50-150 

0.158 

Prep Batch: XXX21847 

Prep Method: SW3520C 

Prep Daterfime: 10/19/09 10:35 

mg/L 

"lo 

Member of SGS Group (Soclete Generate de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

Batch 

XFC8990 

XFC8990 

XXX21847 

XXX21847 

qualifiers 

Initial Prep Wt.Nol.: 950 ml 

Prep Extract Vol.: 1 ml 

Container ID: 1095639001-H 

Analyst: KDC 
The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW2254-WG17 

SGS Ref. #: 1095639001 Collection Date/Time: 10/14/09 09:15 

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Anal:ttical Prep 

Parameter Result PQUCL MDL ~ DF Batch Batch qualifiers 

Benzene ND 0.400 0.120 ug/L VMS10954 VXX20165 

Toluene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Ethyl benzene ND 1.00 0.310 ug/L VMS10954 VXX20165 

n-Butylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 

1,4-Dichlorobenzene ND 0.500 0.150 ug/L VMS10954 VXX20165 

1,2-Dichloroethane ND 0.500 0.150 ug/L VMS10954 VXX20165 

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 

4-Chlorotoluene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Chlorobenzene ND 0.500 0.150 ug/L VMS10954 VXX20165 

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L VMS10954 VXX20165 

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10954 VXX20165 

4-lsopropyltoluene ND 1.00 0.310 ug/L VMS10954 VXX20165 

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L VMS10954 VXX20165 

n-Propylbenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Styrene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Dibromomethane ND 1.00 0.310 ug/L VMS10954 VXX20165 

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L VMS10954 VXX20165 

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Acetone ND 10.0 3.10 ug/L VMS10954 VXX20165 

1, 1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10954 VXX20165 

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L VMS10954 VXX20165 

Methyl-I-butyl ether ND 5.00 1.50 ug/L VMS10954 VXX20165 

Tetrachloroethene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Dibromochloromethane ND 0.500 0.150 ug/L VMS10954 VXX20165 

1,3-Dichloropropane ND 0.400 0.120 ug/L VMS10954 VXX20165 

1,2-Dibromoethane ND 1.00 0.310 ug/L VMS10954 VXX20165 

Carbon tetrachloride ND 1.00 0.310 ug/L VMS10954 VXX20165 

1, 1, 1,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10954 VXX20165 

Chloroform ND 1.00 0.300 ug/L VMS10954 VXX20165 

Bromobenzene ND 1.00 0.310 ug/L VMS10954 VXX20165 

Chloromethane ND 1.00 0.310 ug/L VMS10954 VXX20165 

1,2,3-Trichloropropane ND 1.00 0.310 ug/L VMS10954 VXX20165 

Bromomethane ND 3.00 0.940 ug/L VMS10954 VXX20165 

Bromochloromethane ND 1.00 0.310 ug/L VMS10954 VXX20165 

Vinyl chloride ND 1.00 0.310 ug/L VMS10954 VXX20165 

Dichlorodifluoromethane ND 1.00 0.310 ug/L VMS10954 VXX20165 

SGS North America Inc. 

Member of SGS Group (Soclete Generale de Surveillance) 
l 

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The Environmental Company, Inc. (TEC) 

Client Sample ID: RHMW2254-WG17 

SGS Ref.#: 1095639001 Collection DatefTime: 10/14/09 09:15 

Project ID: 3354-003 Red Hill BFSF Receipt DatefTime: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Parameter Result PQUCL MDL Units OF 

Chloroethane ND 1.00 0.310 ug/L 1 

sec-Butylbenzene ND 1.00 0.310 ug/L 1 

Bromodichloromethane ND 0.500 0.1 50 ug/L 

1, 1-Dichloroethene ND 1.00 0.310 ug/L 

2-Butanone (MEK) ND 10.0 3.10 ug/L 

Methylene chloride ND 5.00 1.00 ug/L 

Trichlorofluoromethane ND 1.00 0.310 ug/L 

P & M-Xylene ND 2.00 0.620 ug/L 

Naphthalene ND 2.00 0.620 ug/L 

a-Xylene ND 1.00 0.310 ug/L 

Bromoform ND 1.00 0.310 ug/L 

1-Chlorohexane ND 1.00 0.310 ug/L 

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 

tert-Butylbenzene ND 1.00 0.310 ug/L 

1, 1, 1-Trichloroethane ND 1.00 0.310 ug/L 

1, 1-Dichloroethane ND 1.00 0.310 ug/L 

2-Chlorotoluene ND 1.00 0.310 ug/L 

Trichloroethene ND 1.00 0.310 ug/L 

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 

2,2-Dichloropropane ND 1.00 0.310 ug/L 

Hexachlorobutadiene ND 1.00 0.310 ug/L 

lsopropylbenzene (Cumene) ND 1.00 0.310 ug/L 

1,2-Dichloropropane ND 1.00 0.310 ug/L 

1, 1-Dichloropropene ND 1.00 0.310 ug/L 

1, 1,2-Trichloroethane ND 1.00 0.310 ug/L 

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 

Xylenes (total) ND 2.00 1.00 ug/L 

1,2-Dichloroethane-D4 <surr> 103 73-120 % 

Toluene-dB <surr> 101 80-120 % 

4-Bromofluorobenzene <surr> 104 76-120 % 

SGS North America Inc. 

Member of SGS Group (Soclete Generale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Ani!l~tical Prep 

Batch ~ Qualifieri 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 

VMS10954 VXX20165 
The Environmental Company, Inc. (TEC) 

Client Sample ID: RHMW2254-WG17 

SGS Ref.#: 1095639001 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Parameter 

Batch Information 

Analytical Batch: VMS10954 

Analytical Method: SW8260B 

Analysis Date/Time: 10/20/09 18:10 

Dilution Factor: 1 

SGS North America Inc. 

Collection Date/Time: 10/14/09 09:15 

Receipt Date/Time: 10/16/09 10:45 

Prep Batch: VXX20165 

Prep Method: SW5030B 

Prep Date/Time: 10/20/09 08:22 

Member of SGS Group (Societe Generale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

Batch Qualifiers 

Initial Prep Wt.Nol.: 5 ml 

Prep Extract Vol.: 5 ml 

Container ID: 1095639001-E 

Analyst: SCl 
The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW2254-WG17 

SGS Ref. #: 1095639001 Collection Date/Time: 10/14/09 09:15 

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground) 

Polynuclear Aromatics GC/MS 

Anal~tical f!m 

Parameter ~ PgUCL MDL .!.l.n!!! OF Batch Batch qualifiers 

l Acenaphthylene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Acenaphthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Fluorene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Phenanthrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Anthracene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Fluoranthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Pyrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Benzo(a )Anthracene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Chrysene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Benzo(b)Fluoranthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Benzo(k)fluoranthene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Benzo[a]pyrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

lndeno[1,2,3-c,d] pyrene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Dibenzo[a,h]anthracene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Benzo(g, h, i]perylene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Naphthalene ND 0.114 0.0352 ug/l XMS5164 XXX21842 

1-Methylnaphthalene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

2-Methylnaphthalene ND 0.0568 0.0170 ug/l XMS5164 XXX21842 

Terphenyl-d14 <surr> 104 50-135 % XMS5164 XXX21842 

Batch Information 

Analytical Batch: XMS5164 Prep Batch: XXX21842 Initial Prep Wt.Nol.: 880 ml 

Analytical Method: 82700 SIMS Prep Method: SW3520C Prep Extract Vol.: 1 ml 

Analysis Date/Time: 10/25/09 18:49 Prep Date/Time: 10/18/09 08:40 Container 10:1095639001-J 

Dilution Factor: 1 Analyst: JOH 

J 

SGS North America Inc. Alaska Division 200 West Potter Drive Anchorage Alaska 99518 

Member of SGS Group (Societe GBnerale de Surveillance) 
Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Dissolved Metals by ICP/MS 

Parameter 

Lead 

Batch Information 

Analytical Batch: MMS6169 

Analytical Method: SW6020 

Analysis Date/Time: 11/02/09 00:58 

Dilution Factor: 5 

The Environmental Company, Inc. (TEC) 

Collection Date/Time: 10/14/09 11 :05 

Receipt Date/Time: 10/16/09 10:45 

Print Date: 11/2/2009 4:48 pm 

Analytical Prep 

DF Batch Batch Qualifiers 

ND 

SGS North America Inc. 

1.00 0.310 

Prep Batch: MXX22450 

Prep Method: SW3010A 

Prep Date/Time: 10/26/09 17:30 

ug/L 

Member of SGS Group (Societe Generale de Surveillance) 

5 MMS6169 MXX22450 

Initial Prep Wt.Nol.: 50 ml 

Prep Extract Vol.: 50 ml 

Container ID: 1095639004-G 

Analyst: NRB 
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Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Volatile Fuels Department 

Parameter 

Gasoline Range Organics 

4-Bromofluorobenzene <surr> 

Batch Information 

Analytical Batch: VFC9728 

Analytical Method: SW8015C 

Analysis DatefTime: 10/24/09 20:10 

Dilution Factor: 1 

The Environmental Company, Inc. (TEC) 

ND 

99.7 

SGS North America Inc. 

Collection DatefTime: 10/14/09 11 :05 

Receipt DatefTime: 10/16/09 10:45 

100 

50-150 

30.0 

Prep Batch: VXX20181 

Prep Method: SW5030B 

Prep DatefTime: 10/24/09 13:29 

ug/l 

% 

Member of SGS Group (Soclete Generale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

Batch 

VFC9728 

VFC9728 

VXX20181 

VXX20181 

qualifiers 

Initial Prep Wt.Nol.: 5 ml 

Prep Extract Vol.: 5 ml 

Container ID: 1095639004-B 

Analyst: KPW 
The Environmental Company, Inc. (TEC) 

Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Semivolatlle Organic Fuels Department 

Parameter 

Diesel Range Organics 

Sa Androstane <surr> 

Batch Information 

Analytical Batch: XFC8990 

Analytical Method: SW8015C 

Analysis Date/Time: 10/26/09 13:01 

Dilution Factor: 1 

ND 

79 

SGS North America Inc. 

Collection Date/Time: 10/14/09 11 :05 

Receipt Date/Time: 10/16/09 10:45 

0.435 

50-150 

0.163 

Prep Batch: XXX21847 

Prep Method: SW3520C 

Prep Date/Time: 10/19/09 10:35 

mg/l 

% 

Member of SGS Group (Societe Generals de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

Batch 

XFC8990 

XFC8990 

XXX21847 

XXX21847 

Qualifiers 

Initial Prep Wt.Nol.: 920 ml 

Prep Extract Vol.: 1 ml 

Container ID: 1095639004-H 

Analyst: KOC 
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Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

The Environmental Company, Inc. (TEC) 

Collection Date/Time: 10/14/09 11 :05 

Receipt Date/Time: 10/16/09 10:45 

Volatile Gas Chromatography/Mass Spectroscopy 

J 

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Parameter 

Benzene 

Toluene 

Ethylbenzene 

n-Butylbenzene 

1,4-Dichlorobenzene 

1,2-Dichloroethane 

1,3,5-Trimethylbenzene 

4-Chlorotoluene 

Chlorobenzene 

4-Methyl-2-pentanone (MIBK) 

cis-1,2-Dichloroethene 

4-lsopropyltoluene 

cis-1,3-Dichloropropene 

n-Propylbenzene 

Styrene 

Dibromomethane 

trans-1,3-Dichloropropene 

1,2,4-Trichlorobenzene 

Acetone 

1, 1,2,2-Tetrachloroethane 

1,2-Dibromo-3-chloropropane 

Methyl-t-butyl ether 

Tetrachloroethene 

Dibromochloromethane 

1,3-Dichloropropane 

1,2-Dibromoethane 

Carbon tetrachloride 

1, 1, 1,2-Tetrachloroethane 

Chloroform 

Bromobenzene 

Chloromethane 

1,2,3-Trichloropropane 

Bromomethane 

Bromochloromethane 

_J ~::~ 1:r~~~~:romethane 

j 

J 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

SGS North America Inc. 

0.400 

1.00 

1.00 

1.00 

0.500 

0.500 

1.00 

1.00 

0.500 

10.0 

1.00 

1.00 

0.500 

1.00 

1.00 

1.00 

1.00 

1.00 

10.0 

0.500 

2.00 

5.00 

1.00 

0.500 

0.400 

1.00 

1.00 

0.500 

1.00 

1.00 

1.00 

1.00 

3.00 

1.00 

1.00 

1.00 

0.120 

0.310 

0.310 

0.310 

0.150 

0.150 

0.310 

0.310 

0.150 

3.10 

0.310 

0.310 

0.150 

0.310 

0.310 

0.310 

0.310 

0.310 

3.10 

0.150 

0.620 

1.50 

0.310 

0.150 

0.120 

0.310 

0.310 

0.150 

0.300 

0.310 

0.310 

0.310 

0.940 

0.310 

0.310 

0.310 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

ug/L 

Member of SGS Group (Soclete Generale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

Batch 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS 10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

VMS10945 VXX20145 

qualifiers 
The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 Collection Date!Time: 10/14/09 11 :05 

Project ID: 3354-003 Red Hill BFSF Receipt Date!Time: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Anal:dical f!m 

Parameter Result PQUCL MDL .!!!!i!! DF Batch ~ qualifiers 

Chloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

sec-Butylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Bromodichloromethane ND 0.500 0.150 ug/L VMS10945 VXX20145 

1, 1-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

2-Butanone (MEK) ND 10.0 3.10 ug/L VMS10945 VXX20145 

Methylene chloride ND 5.00 1.00 ug/L VMS10945 VXX20145 

Trichlorofluoromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

P & M -Xylene ND 2.00 0.620 ug/L VMS10945 VXX20145 

Naphthalene ND 2.00 0.620 ug/L VMS10945 VXX20145 

a-Xylene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Bromoform ND 1.00 0.310 ug/L VMS10945 VXX20145 

1-Chlorohexane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

tert-Butylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1, 1-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1-Dichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

2-Chlorotoluene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

2,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 

Hexachlorobutadiene ND 1.00 0.310 ug/L VMS10945 VXX20145 

lsopropylbenzene (Cumene) ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1-Dichloropropene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1,2-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,3-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Xylenes (total) ND 2.00 1.00 ug/L VMS10945 VXX20145 

1,2-Dichloroethane-D4 <surr> 96.9 73-120 % VMS10945 VXX20145 

Toluene-dB <surr> 104 80-120 % VMS10945 VXX20145 

4-Bromofluorobenzene <surr> 106 76-120 % VMS10945 VXX20145 

SGS North America Inc. 

Member of SGS Group (Societe Generale de Surveillance) 
Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

The Environmental Company, Inc. (TEC) 

Collection Date/Time: 10/14/09 11 :05 

Receipt Date/Time: 10/16/09 10:45 

Volatile Gas Chromatography/Mass Spectroscopy 

Parameter 

Batch Information 

1 

Analytical Batch: VMS10945 

Analytical Method: SW8260B 

Analysis Date/Time: 10/19/09 22:38 

Dilution Factor: 1 

1 

1 

) 

] 

J 

j SGS North America Inc. 

Prep Batch: VXX20145 

Prep Method: SW5030B 

Prep Date/Time: 10/19/09 08:11 

Member of SGS Group (Societe Generale de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

~ qualifiers 

Initial Prep Wt.Nol. : 5 ml 

Prep Extract Vol.: 5 ml 

Container ID:1095639004-A 

Analyst: SCl 
The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW03-WG17 

SGS Ref. #: 1095639004 Collection DatefTime: 10/14/09 11 :05 

Project ID: 3354-003 Red Hill BFSF Receipt DatefTime: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground} 

Polynuclear Aromatics GC/MS 

Anall£tical Prep 

Parameter .!fil!!l! PQUCL MDL Units DF Batch Batch Qualifiers 

Acenaphthylene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Acenaphthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Fluorene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Phenanthrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Anthracene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Fluoranthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Pyrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Benzo( a }Anthracene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Chrysene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Benzo(b]Fluoranthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Benzo(k)fluoranthene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Benzo[a)pyrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

lndeno[1 ,2,3-c,d] pyrene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Dibenzo[a,h]anthracene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Benzo[g,h,i]perylene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Naphthalene ND 0.112 0.0348 ug/l XMS5164 XXX21842 

1-Methylnaphthalene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

2-Methylnaphthalene ND 0.0562 0.0169 ug/l XMS5164 XXX21842 

Terphenyl-d14 <surr> 99 50-135 % XMS5164 XXX21842 

Batch Information 

Analytical Batch: XMS5164 Prep Batch: XXX21842 Initial Prep Wt.Nol.: 890 ml 

Analytical Method: 82700 SIMS Prep Method: SW3520C Prep Extract Vol.: 1 ml 

Analysis DatefTime: 10/25/09 20:33 Prep DatefTime: 10/18/09 08:40 Container 10:1095639004-J 

Dilution Factor: 1 Analyst: JOH 

SGS North America Inc. 

Member of SGS Group (Societe Generale de Surveillance) 
l 

l 

Client Sample ID: RHMW02-WG17 

SGS Ref.#: 1095639005 

J 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Dissolved Metals by ICP/MS 

Parameter 

c Lead 

Batch Information 

Analytical Batch: MMS6169 

Analytical Method: SW6020 

Analysis Date/Time: 11/02/09 01 :00 

Dilution Factor: 5 

J 

l 

J 

The Environmental Company, Inc. (TEC) 

Bm!l! 

ND 

SGS North America Inc. 

Collection Date/Time: 10/13/09 16:15 

Receipt Date/Time: 10/16/09 10:45 

1.00 0.310 

Prep Batch: MXX22450 

Prep Method: SW301 OA 

Prep Date/Time: 10/26/09 17:30 

ug/L 

Member of SGS Group (Soclete Generale de Surveillance) 

5 

Print Date: 11/2/2009 4:48 pm 

Analvtical 

~ qualifiers 

MMS6169 MXX22450 

Initial Prep Wt.Nol.: 50 ml 

Prep Extract Vol.: 50 ml 

Container ID: 1095639005-G 

Analyst: NRB 
Client Sample ID: RHMW02-WG17 

SGS Ref. #: 1095639005 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Volatile Fuels Department 

Parameter 

Gasoline Range Organics 

4-Bromofluorobenzene <surr> 

Batch Information 

Analytical Batch: VFC9728 

Analytical Method: SW8015C 

Analysis Date/Time: 10/24/09 20:33 

Dilution Factor: 1 

The Environmental Company, Inc. (TEC) 

Collection Date/Time: 10/13/09 16:15 

Receipt Date/Time: 10/16/09 10:45 

Print Date: 11/2/2009 4:48 pm 

Analytical Prep 

DF Batch Batch Qualifiers 

36.9 J 

119 

SGS North America Inc. 

100 

50-150 

30.0 

Prep Batch: VXX20181 

Prep Method: SW5030B 

Prep Date/Time: 10/24/09 13:29 

ug/l 

% 

Member of SGS Group (Societe Generale de Surveillance) 

VFC9728 

VFC9728 

VXX20181 

VXX20181 

Initial Prep Wt.Nol.: 5 ml 

Prep Extract Vol.: 5 ml 

Container ID:1095639005-B 

Analyst: KPW 
l 

l 

l 

l 

] 

l 

l 

0 

1 

J 

The Environmental Company, Inc. (TEC) 

Client Sample ID: RHMW02-WG17 

SGS Ref. #: 1095639005 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Semivolatile Organic Fuels Department 

Parameter 

Diesel Range Organics 

5a Androstane <surr> 

Batch Information 

Analytical Batch: XFC8990 

Analytical Method: SW8015C 

Analysis Date/Time: 10/26/09 13:12 

Dilution Factor: 1 

2.57 

74.4 

SGS North America Inc. 

Collection Date/Time: 10/13/09 16:15 

Receipt Date/Time: 10/16/09 10:45 

0.449 

50-150 

0.169 

Prep Batch: XXX21847 

Prep Method: SW3520C 

Prep Date/Time: 10/19/09 10:35 

mg/l 

% 

Member of SGS Group (Sochlte Generate de Surveillance) 

Print Date: 11/2/2009 4:48 pm 

Analytical 

Batch 

XFC8990 

XFC8990 

XXX21847 

XXX21847 

qualifiers 

Initial Prep Wt.Nol.: 890 ml 

Prep Extract Vol. : 1 ml 

Container 10:1095639005-H 

Analyst: KOC 
The Environmental Company, Inc. (TEC) Print Date: 11 /2/2009 4:48 pm 

Client Sample ID: RHMW02-WG17 

SGS Ref. #: 1095639005 Collection Date/Time: 10/13/09 16: 15 

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Anall£tical Prep 

Parameter Bm!l! PQUCL MDL Units DF ~ Batch qualifiers 

Benzene ND 0.400 0.120 ug/L VMS10945 VXX20145 

Toluene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Ethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

n-Butylbenzene 2.98 1.00 0.310 ug/L VMS10945 VXX20145 

1,4-Dichlorobenzene ND 0.500 0.150 ug/L VMS10945 VXX20145 

1,2-Dichloroethane ND 0.500 0.150 ug/L VMS10945 VXX20145 

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

4-Chlorotoluene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Chlorobenzene ND 0.500 0.150 ug/L VMS10945 VXX20145 

4-Methyl-2:pentanone (MIBK) ND 10.0 3.10 ug/L VMS10945 VXX20145 

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

4-lsopropyltoluene ND 1.00 0.310 ug/L VMS10945 VXX20145 

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L VMS10945 VXX20145 

n-Propylbenzene 4.16 1.00 0.310 ug/L VMS10945 VXX20145 

Styrene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Dibromomethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Acetone ND 10.0 3.10 ug/L VMS10945 VXX20145 

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10945 VXX20145 

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L VMS10945 VXX20145 

Methyl-I-butyl ether ND 5.00 1.50 ug/L VMS10945 VXX20145 

Tetrachloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Dibromochloromethane ND 0.500 0.150 ug/L VMS10945 VXX20145 

1,3-Dichloropropane ND 0.400 0.120 ug/L VMS10945 VXX20145 

1 ,2-Dibromoethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

Carbon tetrachloride ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1, 1,2-Tetrachloroethane ND 0.500 0.150 ug/L VMS10945 VXX20145 

Chloroform ND 1.00 0.300 ug/L VMS10945 VXX20145 

Bromobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Chloromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2,3-Trichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 

Bromomethane ND 3.00 0.940 ug/L VMS10945 VXX20145 

Bromochloromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

Vinyl chloride ND 1.00 0.310 ug/L VMS10945 VXX20145 

Dichlorodifluoromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

SGS North America Inc. 

Member of SGS Group (Societe Generale de Surveillance) 
1 

l 

l 

The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW02-WG17 

SGS Ref. #: 1095639005 Collection Date/Time: 10/13/09 16: 15 

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 10/16/09 10:45 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Analli'.tical Prep 

Parameter ~ PQUCL MDL .!.!.nim DF ~ ~ qualifiers 

Chloroethane ND 1.00 0.310 ug/L 1 VMS10945 VXX20145 

sec-Butyl benzene 4.71 1.00 0.310 ug/L 1 VMS10945 VXX20145 

Bromodichloromethane ND 0.500 0.150 ug/L VMS10945 VXX20145 

1, 1-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

2-Butanone (MEK) ND 10.0 3.10 ug/L VMS10945 VXX20145 

Methylene chloride ND 5.00 1.00 ug/L VMS10945 VXX20145 

Trichlorofluoromethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

P & M-Xylene ND 2.00 0.620 ug/L VMS10945 VXX20145 

Naphthalene 23.3 2.00 0.620 ug/L VMS10945 VXX20145 ] o-Xylene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Bromoform ND 1.00 0.310 ug/L VMS10945 VXX20145 

1-Chlorohexane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

tert-Butylbenzene 0.820 J 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1, 1-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1 , 1-Dichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

2-Chlorotoluene ND 1.00 0.310 ug/L VMS10945 VXX20145 

Trichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1 1,2-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

2,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 

Hexachlorobutadiene ND 1.00 0.310 ug/L VMS10945 VXX20145 

lsopropylbenzene (Cumene) 3.49 1.00 0.310 ug/L VMS10945 VXX20145 

1,2-Dichloropropane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1-Dichloropropene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1, 1,2-Trichloroethane ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,3-Dichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L VMS10945 VXX20145 

l Xylenes (total) ND 2.00 1.00 ug/L VMS10945 VXX20145 

1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS10945 VXX20145 

Toluene-dB <surr> 101 80-120 % VMS10945 VXX20145 

J 

4-Bromofluorobenzene <surr> 105 76-120 % VMS10945 VXX20145 

J 

J SGS North America Inc. 

Member of SGS Group (Soclete Generale do Surveillance) 

J 
The Environmental Company, Inc. (TEC) Print Date: 11/2/2009 4:48 pm 

Client Sample ID: RHMW02-WG17 

SGS Ref. #: 1095639005 

Project ID: 3354-003 Red Hill BFSF 

Matrix: Water (Surface, Eff., Ground) 

Volatile Gas Chromatography/Mass Spectroscopy 

Parameter 

Batch Information 

Analytical Batch: VMS10945 

Analytical Method: SW8260B 

Analysis Date!Time: 10/19/09 23: 11 

Dilution Factor: 1 

SGS North America Inc. 

Collection Date!Time: 10/13/09 16: 15 

Receipt Date!Time: 10/16/09 10:45 

Analvtical Prep 

OF Batch Batch Qualifiers 

Prep Batch: VXX20145 

Prep Method: SW5030B 

Prep Date!Time: 10/19/09 08: 11 

Member of SGS Group (Soclete Generale de Surveillance) 

Initial Prep Wt.Nol.: 5 ml 

Prep Extract Vol.: 5 ml 

Container ID:1095639005-A 

Analyst: SCl