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Table of Contents 

INTRODUCTION 

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SUMMARY OF RESULTS 

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ANALYTICAL TECHNIQUE 

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QUALITY ASSURANCE ACTIVITIES 



APPENDICES

 A Detailed Summary of Results 

 B Discussion of Errors and Example Calculations 

 C Instrumental Quality Assurance 

 D Datalog Records and Chromatograms 

 E Sample Gas Extraction Diagram 

 F Calibration Certificates 






Introduction 

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Test Matrix 

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Determination of the Inlet Flare Gas Composition and Mass Rate 

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Determination of the Outlet (Flue Gas) Flare Gas Composition and Mass Rate 

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Calculation of Destruction Rate Efficiency (DRE) 



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Calculation of Combustion Efficiency (CE) 



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TABLE1

Background Information



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SUMMARY OF RESULTS



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TABLE 2: STEAM ASSISTED FLARE SUMMARY OF RESULTS

Run S1 S2 S3 S4 S5 

Date 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2Steam Rate (lbs/hr) 582.0 0.0 124.2 130.1 304.

Heating Value (Btu/scf) 1015 1020 564 700 631 

Heat Rate (MMBtu/hr) 121.27 121.17 10.89 34.44 13.8

Mass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr) 28.54 27.45 0.84 5.12 1.32 

CO (lbs/hr) 10.73 2.25 2.41 2.16 7.52 

THC (lbs/hr) 3.52 0.62 3.37 1.37 7.85 

Propylene (lbs/hr) Direct 3.56 3.96 2.77 3.58 5.14 

Propylene (lbs/hr) Bag 8.41 0.71 7.84 2.54 11.8NOx (lbs/MMBTU) 0.235 0.227 0.077 0.149 0.09CO (lbs/MMBTU) 0.088 0.019 0.221 0.063 0.54

THC (lbs/MMBTU) 0.029 0.005 0.310 0.040 0.56Propylene (lbs/MMBTU) Direct 0.029 0.033 0.255 0.104 0.37

Propylene (lbs/MMBTU) Bag 0.069 0.006 0.720 0.074 0.85

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr) 27.13 28.96 0.83 5.28 1.35 

CO (lbs/hr) 10.20 2.38 2.38 2.23 7.67 

THC (lbs/hr) 3.35 0.65 3.32 1.41 8.00 

Propylene (lbs/hr) Direct 3.38 4.18 2.73 3.69 5.25 

Propylene (lbs/hr) Bag 7.99 0.75 7.73 2.62 12.0

NOx (lbs/MMBTU) 0.224 0.239 0.076 0.153 0.09CO (lbs/MMBTU) 0.084 0.020 0.218 0.065 0.55

THC (lbs/MMBTU) 0.028 0.005 0.305 0.041 0.57Propylene (lbs/MMBTU) Direct 0.028 0.034 0.251 0.107 0.37

Propylene (lbs/MMBTU) Bag 0.066 0.006 0.710 0.076 0.87

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%) 99.94% 99.99% 99.39% 99.92% 98.96

Propylene DE Direct (%) 99.94% 99.94% 99.50% 99.80% 99.32Propylene DE Bag (%) 99.86% 99.99% 98.58% 99.86% 98.44

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%) 99.95% 99.99% 99.40% 99.92% 98.94

Propylene DE Direct (%) 99.94% 99.93% 99.50% 99.80% 99.31Propylene DE Bag (%) 99.87% 99.99% 98.60% 99.85% 98.41

Combustion Efficeincy (%) 99.90% 99.98% 99.59% 99.91% 99.08
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TABLE 3: PRESSURE ASSISTED FLARE SUMMARY OF RESULT

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Heating Value (Btu/scf) 2145 2133 776 711 698 Heat Rate (MMBtu/hr) 163.25 106.17 71.45 41.03 71.21 

Mass Emission Rates(Based on O2 F‐Factor)

NOx (lbs/hr) 21.46 11.40 14.73 7.91 11.48 

CO (lbs/hr) 2.54 1.69 2.49 3.54 4.36 

THC (lbs/hr) 1.80 0.78 0.63 1.16 1.56 

Propylene (lbs/hr) Direct 7.55 2.54 2.78 0.85 1.80 

Propylene (lbs/hr) Bag 6.81 1.22 0.86 1.13 2.69 

NOx (lbs/MMBTU) 0.131 0.107 0.206 0.193 0.161 CO (lbs/MMBTU) 0.016 0.016 0.035 0.086 0.061 

THC (lbs/MMBTU) 0.011 0.007 0.009 0.028 0.022 

Propylene (lbs/MMBTU) Direct 0.046 0.024 0.039 0.021 0.025 

Propylene (lbs/MMBTU) Bag 0.042 0.012 0.012 0.027 0.038 

Mass Emission Rates(Based on CO2 F‐Factor)NOx (lbs/hr) 23.01 12.18 15.60 8.15 11.76 

CO (lbs/hr) 2.77 1.80 2.64 3.65 4.49 

THC (lbs/hr) 1.97 0.84 0.67 1.20 1.60 

Propylene (lbs/hr) Direct 8.12 2.66 2.95 0.88 1.85 

Propylene (lbs/hr) Bag 7.34 1.31 0.91 1.16 2.76 

NOx (lbs/MMBTU) 0.140 0.115 0.218 0.199 0.165 

CO (lbs/MMBTU) 0.017 0.017 0.037 0.089 0.063 

THC (lbs/MMBTU) 0.012 0.008 0.009 0.029 0.022 

Propylene (lbs/MMBTU) Direct 0.049 0.025 0.041 0.021 0.026 

Propylene (lbs/MMBTU) Bag 0.045 0.013 0.013 0.028 0.039 

Efficiencies(Based on O2 F‐Factor)

Destruction Efficiency (%) 99.98% 99.99% 99.98% 99.95% 99.96% Propylene DE Direct (%) 99.91% 99.95% 99.93% 99.96% 99.95% 

Propylene DE Bag (%) 99.92% 99.98% 99.98% 99.95% 99.93% 

Efficiencies(Based on CO2 F‐Factor)

Destruction Efficiency (%) 99.98% 99.98% 99.98% 99.95% 99.96% Propylene DE Direct (%) 99.90% 99.95% 99.92% 99.96% 99.95% 

Propylene DE Bag (%) 99.91% 99.98% 99.98% 99.95% 99.92% 

Combustion Efficeincy (%) 99.98% 99.98% 99.96% 99.89% 99.92% 




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Appendix A:

Detailed Summary of Results



 

15
Detailed Summary of Results

Run S1 S2 S3 S4 S5 S6

Date 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013Start Time 9:19 9:45 11:29 13:36 14:18 14:56

End Time 9:39 10:05 11:56 13:56 14:48 15:16

Flare Feed paused 41‐48 paused 28‐38

Propylene Flow rate (lbs/hr) 6122.8 6109.1 551.2 1802.3 757.8 1969.4

Nitrogen Flow rate (lbs/hr) 4635.3 4595.5 1040.8 2366.6 1076.5 0.0

Natural Gas Flow rate (lbs/hr) 0.0 0.0 0.0 0.0 0.0 0.0

Total Fuel Flow Rate (lbs/hr) 10758.1 10704.8 1592.0 4168.8 1834.3 1969.4

Steam Rate (lbs/hr) 582.0 0.0 124.2 130.1 304.3 643.1

Heating Value (Btu/lb) 11272 11320 6840 8262 7550 19593

Heating Value (Btu/scf) 1015 1020 564 700 631 2136

Heat Rate (MMBtu/hr) 121.27 121.17 10.89 34.44 13.85 38.59

O2 F‐Factor 9837 9831 10644 10291 10451 9304

CO2 F‐Factor 1398 1398 1398 1398 1398 1397

Exhaust Flow Rate (DSCFH) O2 F‐factor 20,740,514 18,933,793 3,323,103 4,978,617 3,372,093 7,641,384

Exhaust Flow Rate (DSCFH @ 0% O2) 1,192,828 1,191,289 115,911 354,458 144,726 359,035

Exhaust Flow Rate (DSCFH) CO2 F‐factor 19,713,348 19,977,101 3,275,139 5,134,872 3,439,597 8,157,100

EmissionsNOx (ppmv) 11.527 12.142 2.113 8.610 3.279 4.503

CO (ppmv) 7.119 1.638 9.986 5.983 30.694 4.779

THC (ppmv) 1.558 0.300 9.305 2.526 21.347 0.689O2 (%) 19.698 19.585 20.171 19.412 20.003 19.918

CO2 (%) 0.860 0.848 0.465 0.938 0.563 0.661

Direct M18 methane (ppmv) 1.408 1.474 2.377 2.911 1.932 2.491

Direct M18 ethane (ppmv) 0.000 0.000 0.000 0.000 0.000 0.000

Direct M18 propylene (ppmv) 1.573 1.919 7.652 6.590 13.992 0.669

Bag M18 methane (ppmv) 1.092 2.078 3.174 2.287 2.855 1.094

Bag M18 ethane (ppmv) 0.000 0.000 0.000 0.000 0.000 0.000

Bag M18 propylene (ppmv) 3.720 0.346 21.643 4.685 32.175 3.963

NOx (ppmv @ 0% O2) 200.428 192.979 60.578 120.933 76.400 95.838

CO (ppmv @ 0% O2) 123.783 26.034 286.293 84.035 715.167 101.712

THC (ppmv @ 0% O2) 27.090 4.768 266.769 35.479 497.383 14.664

Testing by TRC, Austin, Texas

16
Detailed Summary of Results

Run S1 S2 S3 S4 S5 S6

Date 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013Start Time 9:19 9:45 11:29 13:36 14:18 14:56

End Time 9:39 10:05 11:56 13:56 14:48 15:16

Mass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr) 28.54 27.45 0.84 5.12 1.32 4.11

CO (lbs/hr) 10.73 2.25 2.41 2.16 7.52 2.65

THC (lbs/hr) 3.52 0.62 3.37 1.37 7.85 0.57

Propylene (lbs/hr) Direct 3.56 3.96 2.77 3.58 5.14 0.56Propylene (lbs/hr) Bag 8.41 0.71 7.84 2.54 11.83 3.30NOx (lbs/MMBTU) 0.235 0.227 0.077 0.149 0.095 0.106

CO (lbs/MMBTU) 0.088 0.019 0.221 0.063 0.543 0.069

THC (lbs/MMBTU) 0.029 0.005 0.310 0.040 0.567 0.015

Propylene (lbs/MMBTU) Direct 0.029 0.033 0.255 0.104 0.371 0.014Propylene (lbs/MMBTU) Bag 0.069 0.006 0.720 0.074 0.854 0.086

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr) 27.13 28.96 0.83 5.28 1.35 4.39

CO (lbs/hr) 10.20 2.38 2.38 2.23 7.67 2.83

THC (lbs/hr) 3.35 0.65 3.32 1.41 8.00 0.61

Propylene (lbs/hr) Direct 3.38 4.18 2.73 3.69 5.25 0.60Propylene (lbs/hr) Bag 7.99 0.75 7.73 2.62 12.06 3.52NOx (lbs/MMBTU) 0.224 0.239 0.076 0.153 0.097 0.114

CO (lbs/MMBTU) 0.084 0.020 0.218 0.065 0.554 0.073

THC (lbs/MMBTU) 0.028 0.005 0.305 0.041 0.578 0.016

Propylene (lbs/MMBTU) Direct 0.028 0.034 0.251 0.107 0.379 0.015Propylene (lbs/MMBTU) Bag 0.066 0.006 0.710 0.076 0.871 0.091

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%) 99.94% 99.99% 99.39% 99.92% 98.96% 99.97%

Propylene DE Direct (%) 99.94% 99.94% 99.50% 99.80% 99.32% 99.97%

Propylene DE Bag (%) 99.86% 99.99% 98.58% 99.86% 98.44% 99.83%

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%) 99.95% 99.99% 99.40% 99.92% 98.94% 99.97%

Propylene DE Direct (%) 99.94% 99.93% 99.50% 99.80% 99.31% 99.97%

Propylene DE Bag (%) 99.87% 99.99% 98.60% 99.85% 98.41% 99.82%

Combustion Efficeincy (%) 99.90% 99.98% 99.59% 99.91% 99.08% 99.92%

Testing by TRC, Austin, Texas

17
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P1H‐1 P1H‐2 P1H‐3 P1H Average

11/19/2013 11/20/2013 11/21/2013 11/19 ‐11/21

15:45 14:09 13:4816:05 14:29 14:08

8575.4 8200.9 8145.9 8307.4

0.0 0.0 0.0 0.0

0.0 0.0 0.0 0.0

8575.4 8200.9 8145.9 8307.4

0.0 0.0 0.0 0.0

19800 19476 19670 19649

2170 2117 2149 2145

169.80 159.72 160.23 163.25

9297 9309 9302 9302

1397 1397 1397 1397

29,222,469 43,705,437 16,937,928 29,955,278

1,578,573 1,486,821 1,490,376 1,518,590

31,013,562 49,050,915 17,698,423 32,587,634

7.503 3.286 10.412 7.0671.017 1.182 1.397 1.199

0.011 0.794 0.851 0.552

19.771 20.189 19.061 19.674

0.765 0.455 1.265 0.828

2.213 2.328 4.198 2.913

0.000 0.000 0.000 0.000

3.283 1.434 2.901 2.539

2.408 2.976 5.676 3.687

0.000 0.000 0.000 0.000

1.999 1.590 3.510 2.367

138.895 96.593 118.331 117.940

18.827 34.745 15.877 23.150

0.204 23.340 9.672 11.072

Testing by TRC, Austin, Texas

18
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P1H‐1 P1H‐2 P1H‐3 P1H Average

11/19/2013 11/20/2013 11/21/2013 11/19 ‐11/21

15:45 14:09 13:4816:05 14:29 14:08

26.18 17.15 21.05 21.46

2.16 3.75 1.72 2.540.04 3.78 1.57 1.80

10.46 6.83 5.36 7.55

6.37 7.58 6.48 6.81

0.154 0.107 0.131 0.131

0.013 0.024 0.011 0.016

0.000 0.024 0.010 0.011

0.062 0.043 0.033 0.046

0.038 0.047 0.040 0.042

27.78 19.24 22.00 23.01

2.29 4.21 1.80 2.770.04 4.25 1.64 1.97

11.10 7.67 5.60 8.12

6.76 8.50 6.77 7.34

0.164 0.120 0.137 0.140

0.013 0.026 0.011 0.017

0.000 0.027 0.010 0.012

0.065 0.048 0.035 0.049

0.040 0.053 0.042 0.045

100.00% 99.95% 99.98% 99.98%

99.88% 99.92% 99.93% 99.91%99.93% 99.91% 99.92% 99.92%

100.00% 99.95% 99.98% 99.98%

99.87% 99.91% 99.93% 99.90%99.92% 99.90% 99.92% 99.91%99.99% 99.96% 99.98% 99.98%

Testing by TRC, Austin, Texas

19
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P1L‐1 P1L‐2 P1L‐3 P1L Average

11/20/2013 11/21/2013 11/21/2013 11/20 ‐ 11/21

14:57 9:44 16:32

15:17 10:04 16:52

5240.5 5394.0 5632.7 5422.4

0.0 0.0 0.0 0.0

0.0 0.0 0.0 0.0

5240.6 5397.3 5632.7 5423.5

0.0 0.0 0.0 0.0

19577 19579 19570 19575

2133 2134 2132 2133

102.59 105.67 110.23 106.17

9305 9305 9305 9305

1397 1397 1397 1397

15,809,862 11,193,125 18,370,446 15,124,478

954,643 983,281 1,025,757 987,894

17,741,972 11,644,847 19,181,822 16,189,547

5.803 8.641 5.340 6.595

1.157 2.008 1.582 1.582

0.543 0.386 0.468 0.466

19.638 19.064 19.733 19.478

0.808 1.268 0.803 0.960

2.649 1.311 0.934 1.631

0.000 0.000 0.000 0.000

0.352 2.312 2.089 1.584

2.899 2.969 0.000 1.956

0.000 0.000 0.000 0.000

0.954 1.644 0.000 0.866

96.104 98.364 95.635 96.70119.161 22.858 28.332 23.450

8.993 4.394 8.381 7.256

Testing by TRC, Austin, Texas

20
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P1L‐1 P1L‐2 P1L‐3 P1L Average

11/20/2013 11/21/2013 11/21/2013 11/20 ‐ 11/21

14:57 9:44 16:32

15:17 10:04 16:52

10.95 11.55 11.71 11.40

1.33 1.63 2.11 1.690.94 0.47 0.94 0.780.61 2.82 4.18 2.541.64 2.01 0.00 1.22

0.107 0.109 0.106 0.107

0.013 0.015 0.019 0.016

0.009 0.004 0.009 0.007

0.006 0.027 0.038 0.024

0.016 0.019 0.000 0.012

12.29 12.01 12.23 12.18

1.49 1.70 2.21 1.801.05 0.49 0.98 0.840.68 2.93 4.37 2.661.85 2.09 0.00 1.31

0.120 0.114 0.111 0.115

0.015 0.016 0.020 0.017

0.010 0.005 0.009 0.008

0.007 0.028 0.040 0.025

0.018 0.020 0.000 0.013

99.98% 99.99% 99.98% 99.99%99.99% 99.95% 99.93% 99.95%99.97% 99.96% 100.00% 99.98%99.98% 99.99% 99.98% 99.98%99.99% 99.95% 99.92% 99.95%99.96% 99.96% 100.00% 99.98%99.98% 99.98% 99.97% 99.98%

Testing by TRC, Austin, Texas

21
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P2H‐1* P2H‐1b P2H‐2 P2H‐3 P2H Average

11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/21

14:01 16:37 10:56 16:02

14:06 16:57 11:16 16:22

1638.8 3820.9 3786.7 3755.0 3787.5

0.5 4144.2 4130.3 4103.5 4126.00.0 0.0 0.0 0.0 0.0

1638.9 7965.1 7917.0 7859.3 7913.8

0.0 0.0 0.0 0.0 0.0

8723 8979 9145 8961 9028

746 771 788 770 776

14.30 71.52 72.40 70.43 71.45

10201 10155 10127 10158 10147

1398 1398 1398 1398 1398

1,886,027 8,213,579 11,608,173 10,008,135 9,943,296

145,829 726,253 733,148 715,414 724,938

1,979,139 8,650,402 12,360,155 10,611,690 10,540,749

15.508 16.526 10.243 11.546 12.772

1.710 1.770 2.997 5.325 3.364

0.422 0.376 0.390 0.967 0.578

19.284 19.052 19.580 19.406 19.346

1.010 1.156 0.819 0.928 0.968

3.517 2.303 3.516 1.427 2.415

0.000 0.000 0.000 0.000 0.000

7.993 1.630 3.403 2.352 2.462

N/A 2.698 2.567 1.701 2.322

N/A 0.000 0.000 0.000 0.000

N/A 0.545 0.623 1.199 0.789

200.568 186.901 162.181 161.520 170.201

22.116 20.018 47.453 74.493 47.321

5.458 4.252 6.175 13.528 7.985

*Only 5 minutes of data. Not included in average

Testing by TRC, Austin, Texas

22
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)

Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P2H‐1* P2H‐1b P2H‐2 P2H‐3 P2H Average

11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/21

14:01 16:37 10:56 16:02

14:06 16:57 11:16 16:22

3.49 16.21 14.20 13.80 14.73

0.23 1.06 2.53 3.87 2.490.09 0.34 0.49 1.05 0.631.64 1.46 4.31 2.57 2.78

N/A 0.49 0.79 1.31 0.86

0.244 0.227 0.196 0.196 0.206

0.016 0.015 0.035 0.055 0.035

0.006 0.005 0.007 0.015 0.009

0.115 0.020 0.059 0.036 0.039

N/A 0.007 0.011 0.019 0.012

3.66 17.07 15.12 14.63 15.60

0.25 1.11 2.69 4.11 2.640.09 0.35 0.53 1.12 0.671.72 1.54 4.59 2.72 2.95

N/A 0.51 0.84 1.39 0.91

0.256 0.239 0.209 0.208 0.218

0.017 0.016 0.037 0.058 0.037

0.006 0.005 0.007 0.016 0.009

0.121 0.021 0.063 0.039 0.041

N/A 0.007 0.012 0.020 0.013

99.99% 99.99% 99.99% 99.97% 99.98%99.90% 99.96% 99.89% 99.93% 99.93%

N/A 99.99% 99.98% 99.97% 99.98%

99.99% 99.99% 99.99% 99.97% 99.98%99.89% 99.96% 99.88% 99.93% 99.92%

N/A 99.99% 99.98% 99.96% 99.98%

99.98% 99.98% 99.96% 99.93% 99.96%

*Only 5 minutes of data. Not included in average

Testing by TRC, Austin, Texas

23
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P2L‐1* P2L‐1b P2L‐2 P2L‐3 P2L Average

11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/21

17:23 17:39 11:31 14:38

17:26 17:59 11:51 14:58

1984.9 2217.4 2175.5 2112.5 2168.52852.4 2738.0 2746.4 2705.7 2730.0

0.0 0.0 0.0 0.0 0.0

4837.3 4955.4 4921.9 4818.2 4898.5

0.0 0.0 0.0 0.0 0.0

7753 8255 8433 8445 8378

650 699 717 718 711

37.50 40.91 41.51 40.69 41.03

10402 10292 10256 10254 10267

1398 1398 1398 1398 1398

7,523,997 7,017,078 7,286,650 5,372,700 6,558,810

390,120 421,025 425,694 417,220 421,313

6,411,214 7,268,371 7,498,419 5,513,134 6,759,975

9.216 9.208 9.015 12.757 10.327

16.066 7.505 7.372 7.396 7.424

5.631 1.833 1.837 1.062 1.577

19.816 19.646 19.679 19.277 19.534

0.818 0.787 0.774 1.032 0.864

0.881 2.492 2.301 1.468 2.087

0.000 0.000 0.000 0.000 0.000

7.390 1.068 1.395 1.063 1.175

N/A 2.535 2.914 1.103 2.184

N/A 0.000 0.000 0.000 0.000

N/A 1.104 1.945 1.692 1.580

177.737 153.467 154.311 164.277 157.351309.861 125.083 126.187 95.241 115.504108.608 30.550 31.444 13.676 25.223

*Only 3 minutes of data. Not included in average

Testing by TRC, Austin, Texas

24
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)

Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P2L‐1* P2L‐1b P2L‐2 P2L‐3 P2L Average

11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/21

17:23 17:39 11:31 14:38

17:26 17:59 11:51 14:58

8.28 7.71 7.84 8.18 7.91

8.78 3.83 3.90 2.89 3.54

4.62 1.40 1.46 0.62 1.16

6.06 0.82 1.11 0.62 0.85

N/A 0.84 1.54 0.99 1.13

0.221 0.189 0.189 0.201 0.193

0.234 0.094 0.094 0.071 0.086

0.123 0.034 0.035 0.015 0.028

0.162 0.020 0.027 0.015 0.021

N/A 0.021 0.037 0.024 0.027

7.05 7.99 8.07 8.40 8.157.49 3.96 4.02 2.96 3.653.94 1.45 1.50 0.64 1.205.16 0.85 1.14 0.64 0.88

N/A 0.87 1.59 1.02 1.16

0.188 0.195 0.194 0.206 0.199

0.200 0.097 0.097 0.073 0.089

0.105 0.036 0.036 0.016 0.029

0.138 0.021 0.027 0.016 0.021

N/A 0.021 0.038 0.025 0.028

99.77% 99.94% 99.93% 99.97% 99.95%99.69% 99.96% 99.95% 99.97% 99.96%

N/A 99.96% 99.93% 99.95% 99.95%

99.80% 99.93% 99.93% 99.97% 99.95%99.74% 99.96% 99.95% 99.97% 99.96%

N/A 99.96% 99.93% 99.95% 99.95%

99.74% 99.88% 99.88% 99.92% 99.89%

*Only 3 minutes of data. Not included in average

Testing by TRC, Austin, Texas

25
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P3H‐1 P3H‐2 P3H‐3 P3H Average

11/20/2013 11/21/2013 11/21/2013 11/20‐11/21

19:18 12:45 15:3419:38 13:05 15:54

2598.8 2523.9 2512.4 2545.03882.5 3871.0 3824.3 3859.31103.2 1107.9 1113.5 1108.27584.4 7502.7 7450.2 7512.4

0.0 0.0 0.0 0.0

9440 9419 9578 9479

697 693 705 698

71.60 70.67 71.36 71.21

10176 10181 10156 10171

1312 1310 1310 1311

7,069,322 11,072,933 9,042,647 9,061,634

728,580 719,476 724,710 724,255

7,076,371 11,305,490 9,531,890 9,304,584

15.005 7.951 10.441 11.132

8.361 3.736 8.795 6.964

1.725 1.204 1.916 1.615

18.746 19.542 19.225 19.171

1.327 0.819 0.981 1.042

3.783 0.000 1.539 1.774

0.000 0.000 0.000 0.000

2.264 1.163 2.270 1.899

5.881 3.258 4.576 4.572

0.000 0.000 0.000 0.000

3.066 2.734 2.451 2.751

145.592 122.368 130.279 132.746

81.126 57.498 109.741 82.78816.737 18.530 23.907 19.725

Testing by TRC, Austin, Texas

26
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P3H‐1 P3H‐2 P3H‐3 P3H Average

11/20/2013 11/21/2013 11/21/2013 11/20‐11/21

19:18 12:45 15:3419:38 13:05 15:54

12.66 10.51 11.27 11.48

4.30 3.01 5.78 4.361.33 1.45 1.89 1.561.74 1.40 2.24 1.802.36 3.30 2.42 2.69

0.177 0.149 0.158 0.161

0.060 0.043 0.081 0.061

0.019 0.021 0.026 0.022

0.024 0.020 0.031 0.025

0.033 0.047 0.034 0.038

12.68 10.73 11.88 11.76

4.30 3.07 6.09 4.491.33 1.48 1.99 1.601.75 1.43 2.36 1.852.37 3.37 2.55 2.76

0.177 0.152 0.167 0.165

0.060 0.043 0.085 0.063

0.019 0.021 0.028 0.022

0.024 0.020 0.033 0.026

0.033 0.048 0.036 0.039

99.96% 99.96% 99.95% 99.96%99.95% 99.96% 99.94% 99.95%99.94% 99.91% 99.93% 99.93%99.96% 99.96% 99.95% 99.96%99.95% 99.96% 99.93% 99.95%99.94% 99.91% 99.93% 99.92%99.92% 99.94% 99.89% 99.92%

Testing by TRC, Austin, Texas

27
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P3L‐1b P3L‐2 P3L‐3 P3L Average

11/21/2013 11/21/2013 11/21/2013 11/21/2013

9:06 13:17 15:069:26 13:37 15:26

1539.3 1533.2 1579.6 1550.72393.7 2386.8 2354.6 2378.3

665.7 656.8 666.6 663.0

4598.6 4576.8 4600.8 4592.1

0.0 0.0 0.0 0.0

9278 9327 9599 9401

679 684 708 690

42.67 42.69 44.16 43.17

10207 10198 10152 10186

1307 1308 1311 1309

4,386,722 5,934,951 4,436,776 4,919,483

435,524 435,324 448,348 439,732

4,489,683 6,081,884 4,498,741 5,023,436

12.018 8.562 12.356 10.979

5.315 3.896 7.098 5.436

0.160 1.095 1.268 0.841

18.825 19.367 18.788 18.993

1.242 0.918 1.287 1.149

1.039 2.663 0.000 1.234

0.000 0.000 0.000 0.000

1.066 0.558 0.464 0.696

2.952 2.886 3.026 2.955

0.000 0.000 0.000 0.000

2.344 0.177 0.465 0.996

121.049 116.729 122.273 120.017

53.534 53.116 70.241 58.964

1.612 14.929 12.548 9.696

Testing by TRC, Austin, Texas

28
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P3L‐1b P3L‐2 P3L‐3 P3L Average

11/21/2013 11/21/2013 11/21/2013 11/21/2013

9:06 13:17 15:069:26 13:37 15:26

6.29 6.07 6.54 6.30

1.69 1.68 2.29 1.89

0.08 0.71 0.61 0.47

0.51 0.36 0.22 0.37

1.12 0.11 0.23 0.49

0.148 0.142 0.148 0.1460.040 0.039 0.052 0.0440.002 0.017 0.014 0.0110.012 0.008 0.005 0.0080.026 0.003 0.005 0.011

6.44 6.22 6.64 6.43

1.73 1.72 2.32 1.93

0.08 0.73 0.62 0.48

0.52 0.37 0.23 0.37

1.15 0.12 0.23 0.50

0.151 0.146 0.150 0.1490.041 0.040 0.053 0.0450.002 0.017 0.014 0.0110.012 0.009 0.005 0.0090.027 0.003 0.005 0.012

100.00% 99.97% 99.97% 99.98%

99.98% 99.98% 99.99% 99.98%99.95% 99.99% 99.99% 99.98%

100.00% 99.97% 99.97% 99.98%

99.98% 99.98% 99.99% 99.98%99.95% 99.99% 99.99% 99.98%99.96% 99.95% 99.94% 99.95%

Testing by TRC, Austin, Texas

29
Detailed Summary of Results

RunDateStart TimeEnd TimeFlare FeedPropylene Flow rate (lbs/hr)

Nitrogen Flow rate (lbs/hr)

Natural Gas Flow rate (lbs/hr)

Total Fuel Flow Rate (lbs/hr)

Steam Rate (lbs/hr)

Heating Value (Btu/lb)

Heating Value (Btu/scf)

Heat Rate (MMBtu/hr)

O2 F‐Factor

CO2 F‐Factor

Exhaust Flow Rate (DSCFH) O2 F‐factor

Exhaust Flow Rate (DSCFH @ 0% O2)

Exhaust Flow Rate (DSCFH) CO2 F‐factor

EmissionsNOx (ppmv)

CO (ppmv)THC (ppmv)O2 (%)

CO2 (%)

Direct M18 methane (ppmv)

Direct M18 ethane (ppmv)

Direct M18 propylene (ppmv)

Bag M18 methane (ppmv)

Bag M18 ethane (ppmv)

Bag M18 propylene (ppmv)

NOx (ppmv @ 0% O2)

CO (ppmv @ 0% O2)

THC (ppmv @ 0% O2)

P4

11/22/2013

10:0910:23

0.00.0

1227.0

2703†

0.0

N/A

327

37.84

N/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/A

†Total flow rate includes hydrogen

Testing by TRC, Austin, Texas

30
Detailed Summary of Results

RunDateStart TimeEnd TimeMass Emission Rates (Based on O2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Mass Emission Rates (Based on CO2 F‐Factor)

NOx (lbs/hr)

CO (lbs/hr)THC (lbs/hr)Propylene (lbs/hr) Direct

Propylene (lbs/hr) Bag

NOx (lbs/MMBTU)

CO (lbs/MMBTU)THC (lbs/MMBTU)Propylene (lbs/MMBTU) Direct

Propylene (lbs/MMBTU) Bag

Efficiencies (Based on O2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Efficiencies (Based on CO2 F‐Factor)

Destruction Efficiency (%)

Propylene DE Direct (%)

Propylene DE Bag (%)

Combustion Efficeincy (%)

P4

11/22/2013

10:0910:23

N/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/A

†Total flow rate includes hydrogen

Testing by TRC, Austin, Texas

31
99.99%

99.98%

99.97%

99.96%

99.95%

99.94%

99.93%

99.92%

99.91%

99.90%

99.89%

99.88%

100.00%

P1H Average P1L Average P2H Average P2L Average P3H Average P3L Average

Destruction Effic

Propylene DE Dir

Propylene DE Ba

Destruction Effic

Propylene DE Dir

Propylene DE Ba

Combustion Effic

32
Fuel Analysis

Page 1

Component Volume O2 F Factor (dry) 9836.53 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

S1 Nitrogen 52.8377 O2 F Factor (wet) 11237.52 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.99 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.47 volume % water in flue gas @ 0% excess air

Propylene 47.1623 CO2 F Factor 1398.05 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 47.1623 Heating Value 11272.02 Net Heating Value Btu/lb

Heating Value 1014.93 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9831.29 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

S2 Nitrogen 52.5917 O2 F Factor (wet) 11232.27 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.98 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.47 volume % water in flue gas @ 0% excess air

Propylene 47.4083 CO2 F Factor 1398.05 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 47.4083 Heating Value 11319.54 Net Heating Value Btu/lb

Heating Value 1020.23 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10643.60 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

S3 Nitrogen 73.8077 O2 F Factor (wet) 12044.99 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.38 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 11.63 volume % water in flue gas @ 0% excess air

Propylene 26.1923 CO2 F Factor 1398.45 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 26.1923 Heating Value 6840.45 Net Heating Value Btu/lb

Heating Value 563.66 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10290.57 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

S4 Nitrogen 67.4772 O2 F Factor (wet) 11691.83 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.26 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 11.98 volume % water in flue gas @ 0% excess air

Propylene 32.5228 CO2 F Factor 1398.32 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 32.5228 Heating Value 8262.50 Net Heating Value Btu/lb

Heating Value 699.89 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10450.96 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

S5 Nitrogen 70.6944 O2 F Factor (wet) 11852.28 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.32 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 11.82 volume % water in flue gas @ 0% excess air

Propylene 29.3056 CO2 F Factor 1398.38 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 29.3056 Heating Value 7549.62 Net Heating Value Btu/lb

Heating Value 630.66 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9304.47 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

S6 Nitrogen 0.7426 O2 F Factor (wet) 10704.71 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air

Propylene 99.2574 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 99.2574 Heating Value 19593.28 Net Heating Value Btu/lb

Heating Value 2136.02 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9296.89 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1H-1 Nitrogen -0.8353 O2 F Factor (wet) 10697.11 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.22 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.09 volume % water in flue gas @ 0% excess air

Propylene 100.8353 CO2 F Factor 1397.29 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 100.8353 Heating Value 19800.34 Net Heating Value Btu/lb

Heating Value 2169.97 Net Heating Value Btu/SCF

33
Fuel Analysis

Page 2

Component Volume O2 F Factor (dry) 9308.83 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1H-2 Nitrogen 1.6279 O2 F Factor (wet) 10709.09 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.25 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air

Propylene 98.3721 CO2 F Factor 1397.32 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 98.3721 Heating Value 19476.13 Net Heating Value Btu/lb

Heating Value 2116.97 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9305.08 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1L-1 Nitrogen 0.8670 O2 F Factor (wet) 10705.32 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air

Propylene 99.1330 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 99.1330 Heating Value 19576.85 Net Heating Value Btu/lb

Heating Value 2133.34 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10200.92 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2H-1 Nitrogen 65.3517 O2 F Factor (wet) 11602.13 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.22 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.08 volume % water in flue gas @ 0% excess air

Propylene 34.6483 CO2 F Factor 1398.28 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 34.6483 Heating Value 8722.75 Net Heating Value Btu/lb

Heating Value 745.63 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10155.02 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2H-1b Nitrogen 64.1527 O2 F Factor (wet) 11556.21 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.19 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.13 volume % water in flue gas @ 0% excess air

Propylene 35.8473 CO2 F Factor 1398.26 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 35.8473 Heating Value 8978.72 Net Heating Value Btu/lb

Heating Value 771.43 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10402.20 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2L-1 Nitrogen 69.7856 O2 F Factor (wet) 11803.50 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.30 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 11.87 volume % water in flue gas @ 0% excess air

Propylene 30.2144 CO2 F Factor 1398.37 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 30.2144 Heating Value 7753.01 Net Heating Value Btu/lb

Heating Value 650.21 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10292.07 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2L-1b Nitrogen 67.5104 O2 F Factor (wet) 11693.32 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.26 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 11.98 volume % water in flue gas @ 0% excess air

Propylene 32.4896 CO2 F Factor 1398.32 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 32.4896 Heating Value 8255.25 Net Heating Value Btu/lb

Heating Value 699.18 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10176.28 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P3H-1 Nitrogen 53.9824 O2 F Factor (wet) 11838.18 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane 22.9790 Moisture F Factor 1661.90 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane 1.0784 Combust. Moisture 14.04 volume % water in flue gas @ 0% excess air

Propylene 21.9602 CO2 F Factor 1311.58 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 46.0176 Heating Value 9439.90 Net Heating Value Btu/lb

Heating Value 696.54 Net Heating Value Btu/SCF

34
Fuel Analysis

Page 3

Component Volume O2 F Factor (dry) 10207.32 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P3L-1b Nitrogen 54.4037 O2 F Factor (wet) 11883.31 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane 23.6735 Moisture F Factor 1675.99 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane 1.0438 Combust. Moisture 14.10 volume % water in flue gas @ 0% excess air

Propylene 20.8790 CO2 F Factor 1306.88 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 45.5963 Heating Value 9278.49 Net Heating Value Btu/lb

Heating Value 678.95 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9305.01 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1L-2 Nitrogen 0.8528 O2 F Factor (wet) 10705.25 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air

Propylene 99.1472 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 99.1472 Heating Value 19578.74 Net Heating Value Btu/lb

Heating Value 2133.65 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10126.65 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2H-2 Nitrogen 63.3693 O2 F Factor (wet) 11527.83 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.18 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.15 volume % water in flue gas @ 0% excess air

Propylene 36.6307 CO2 F Factor 1398.24 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 36.6307 Heating Value 9144.56 Net Heating Value Btu/lb

Heating Value 788.29 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10256.25 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2L-2 Nitrogen 66.6949 O2 F Factor (wet) 11657.49 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.02 volume % water in flue gas @ 0% excess air

Propylene 33.3051 CO2 F Factor 1398.30 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 33.3051 Heating Value 8432.87 Net Heating Value Btu/lb

Heating Value 716.73 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10181.05 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P3H-2 Nitrogen 53.9767 O2 F Factor (wet) 11846.96 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane 23.2506 Moisture F Factor 1665.91 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane 1.0650 Combust. Moisture 14.06 volume % water in flue gas @ 0% excess air

Propylene 21.7078 CO2 F Factor 1310.24 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 46.0233 Heating Value 9419.03 Net Heating Value Btu/lb

Heating Value 693.33 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10198.35 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P3L-2 Nitrogen 54.2551 O2 F Factor (wet) 11871.08 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane 23.5331 Moisture F Factor 1672.74 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane 1.0656 Combust. Moisture 14.09 volume % water in flue gas @ 0% excess air

Propylene 21.1462 CO2 F Factor 1307.97 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 45.7449 Heating Value 9326.51 Net Heating Value Btu/lb

Heating Value 683.79 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9301.66 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1H-3 Nitrogen 0.1626 O2 F Factor (wet) 10701.89 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.23 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air

Propylene 99.8374 CO2 F Factor 1397.30 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 99.8374 Heating Value 19669.64 Net Heating Value Btu/lb

Heating Value 2148.50 Net Heating Value Btu/SCF

35
Fuel Analysis

Page 4

Component Volume O2 F Factor (dry) 10253.88 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2L-3 Nitrogen 66.6395 O2 F Factor (wet) 11655.12 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.02 volume % water in flue gas @ 0% excess air

Propylene 33.3605 CO2 F Factor 1398.30 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 33.3605 Heating Value 8444.89 Net Heating Value Btu/lb

Heating Value 717.92 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10152.20 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P3L-3 Nitrogen 53.1446 O2 F Factor (wet) 11815.66 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane 23.5523 Moisture F Factor 1663.46 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane 1.0356 Combust. Moisture 14.08 volume % water in flue gas @ 0% excess air

Propylene 22.2675 CO2 F Factor 1311.04 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 46.8554 Heating Value 9598.95 Net Heating Value Btu/lb

Heating Value 707.61 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10156.09 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P3H-3 Nitrogen 53.1985 O2 F Factor (wet) 11821.40 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane 23.6534 Moisture F Factor 1665.30 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane 1.0245 Combust. Moisture 14.09 volume % water in flue gas @ 0% excess air

Propylene 22.1236 CO2 F Factor 1310.42 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 46.8015 Heating Value 9577.82 Net Heating Value Btu/lb

Heating Value 705.24 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 10158.09 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P2H-3 Nitrogen 64.2356 O2 F Factor (wet) 11559.29 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1401.19 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 12.12 volume % water in flue gas @ 0% excess air

Propylene 35.7644 CO2 F Factor 1398.26 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 35.7644 Heating Value 8961.11 Net Heating Value Btu/lb

Heating Value 769.65 Net Heating Value Btu/SCF

Component Volume O2 F Factor (dry) 9305.32 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1L-3 Nitrogen 0.9158 O2 F Factor (wet) 10705.56 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air

Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air

Propylene 99.0842 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air

HC total 99.0842 Heating Value 19570.41 Net Heating Value Btu/lb

Heating Value 2132.29 Net Heating Value Btu/SCF

36
Appendix B: 

Discussion of Errors and Example Calculations





 

37
Discussion of Errors

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38
Example Calculations for Run S1

Calculation of Heat Input

QF = flare waste gas flow, lbs/hr = 10758.1

GHV = lower heating value, Btu/lb = 11272

IHF = heat input, MMBtu/hr

= (QF x GHV)/ 1000000

IH = 121.27 MMBtu/HR

Calculation of Flare Exhaust Flow Rate via EPA Method 19

IH = heat input, MMBtu/hr = 121.27

FO2 = O2 F-Factor, DSCF exhaust/MMBtu = 9837

CO2 = exhaust O2 concentration, % = 19.70

QS = dry stack flow rate, standard conditions, DSCF/hr

20.9

20.9 - CO2

QS = 2.07E+07 DSCFH

= IH X FO2 X

39
Example Calculations for Run S1

Mass Emission Rates using EPA Method 19, lbs/hr

CCO = exhaust CO concentration, ppmv = 7.12

CTHC = exhaust THC concentration, ppmv = 1.56

Cpropyl = exhaust propylene concentration (direct), ppmv = 1.57

QSd = stack flow rate, DSCF/hr = 2.07E+07

MWCO = molecular weight of CO = 28

MWTHC = molecular weight of THC as C3H6 = 42

MWpropyl = molecular weight of propylene = 42

K = gas constant, SCF/lb-mole at EPA STP = 385.3

E"X" = mass emssion rate of "X", lbs/hour

ECO = 10.73 lbs/hr

ETHC = 3.52 lbs/hr

Epropyl = 3.56 lbs/hr (direct)

Propylene Destruction Rate Efficiency Calculation

MPI = Mass of propylene to flare, lbs/hr = 6122.8

MPO = Mass of propylene in exhaust, lbs/hr = 3.56

MPI - MPO

MPI

DRE % = 99.94%

Combustion Efficiency

CCO = exhaust CO concentration, ppmv = 7.12

CCO2 = exhaust CO2 concentration, ppmv = 8600

CTHC = exhaust THC concentration, ppmv = 1.56

CCO2

CCO2 + CCO +CTHC

CE % = 99.90%

 x 100

=

DRE % =

C"X" * QS * 10-6 * MW"X" / K

CE % = x 100

40
Appendix C: 

Instrumental Quality Assurance





 

41
Initial Cal Error Instrumantal QA

Testing by TRC, Austin, Texas

199009 November 19 

Initial Calibration Error Test 

Date/Time: 11/19/2013 7:33:51 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Zero ID: Low ID: Mid ID: High ID: 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 CC427175 X02NI99P15A3LE2 X02NI99P15A51P7

Calibration Error Results 

Channel: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200 200 25 25 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Zero Ref: 0.000 0.000 0.000 0.000 0

Zero Cal: -0.043 0.124 0.044 -0.024 -0.001

Zero Error: 0.000 0.001 0.002 -0.001 0.00%

 

Low Ref: 30.35

Low Cal: 30.416

Low Error: 0.20%

 

Mid Ref: 51.010 49.660 9.969 9.950 50.2

Mid Cal: 51.798 50.545 10.059 9.989 49.709

Mid Error: 0.008 0.009 0.004 0.002 -1.00%

 

High Ref: 100.100 100.100 20.000 19.600 84.96

High Cal: 99.994 101.116 20.039 19.750 85.063

High Error: -0.10% 1.00% 0.20% 0.80% 0.10%

 

Cal Result: PASSED PASSED PASSED PASSED PASSED

42
Initial System Bias Instrumantal QA

Testing by TRC, Austin, Texas

199009 November 19 

Initial System Bias Check 

Date/Time: 11/19/2013 7:43:45 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: 0.750 0.058 0.107 0.117 0.055

Low Bias: 0.008 -0.001 0.003 0.007 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 51.294 50.560 9.904 9.941 50.081

Upscale Bias -0.50% 0.00% -0.80% -0.20% 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

43
Run S1 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 1 

Run S1 Final Bias and Drift Check

Date/Time: 11/19/2013 9:43:31 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: 0.844 -0.295 0.098 0.074 -0.91

Low Bias: 0.009 -0.004 0.003 0.005 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 51.901 50.622 10.071 9.894 49.147

Upscale Bias 0.001 0.001 0.001 -0.005 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.001 -0.004 0.000 -0.002 -1.00%

Mid Drift: 0.006 0.001 0.008 -0.002 -0.90%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 1 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.750 0.058 0.107 0.117 

Low final: 0.844 -0.295 0.098 0.074 

Mid Init: 51.294 50.560 9.904 9.941 

Mid Final: 51.901 50.622 10.071 9.894 

Run Avg: 12.277 7.151 19.634 0.944 1.558

Co: 0.797 -0.119 0.103 0.095 

Cm: 51.598 50.591 9.987 9.918 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 11.527 7.119 19.698 0.86 

44
Run S2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 2 

Run S2 Final Bias and Drift Check

Date/Time: 11/19/2013 10:12:51 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: 0.174 -0.378 0.102 0.057 -0.187

Low Bias: 0.002 -0.005 0.003 0.004 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 51.089 50.295 10.053 9.910 50.362

Upscale Bias -0.007 -0.002 0.000 -0.004 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.007 -0.001 0.000 -0.001 0.70%

Mid Drift: -0.008 -0.003 -0.001 0.001 1.20%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 2 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.844 -0.295 0.098 0.074 

Low final: 0.174 -0.378 0.102 0.057 

Mid Init: 51.901 50.622 10.071 9.894 

Mid Final: 51.089 50.295 10.053 9.910 

Run Avg: 12.645 1.338 19.671 0.904 0.3

Co: 0.509 -0.337 0.100 0.065 

Cm: 51.495 50.459 10.062 9.902 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 12.142 1.638 19.585 0.848 

45
Run S3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 3 

Run S3 Final Bias and Drift Check

Date/Time: 11/19/2013 12:07:02 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: -0.023 -0.549 0.082 0.052 -0.671

Low Bias: 0.000 -0.007 0.002 0.004 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 50.177 50.041 10.015 9.879 49.079

Upscale Bias -0.016 -0.005 -0.002 -0.006 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.002 -0.002 -0.001 0.000 -0.50%

Mid Drift: -0.009 -0.003 -0.002 -0.002 -1.30%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 3 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.174 -0.378 0.102 0.057 

Low final: -0.023 -0.549 0.082 0.052 

Mid Init: 51.089 50.295 10.053 9.910 

Mid Final: 50.177 50.041 10.015 9.879 

Run Avg: 2.169 9.718 20.209 0.514 9.305

Co: 0.075 -0.464 0.092 0.055 

Cm: 50.633 50.168 10.034 9.894 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 2.113 9.986 20.171 0.465 

46
Run S4 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 4 

Run S4 Final Bias and Drift Check

Date/Time: 11/19/2013 2:01:42 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: 0.290 -0.529 0.092 0.061 -0.482

Low Bias: 0.003 -0.007 0.002 0.004 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 50.858 50.107 10.013 9.856 49.694

Upscale Bias -0.009 -0.004 -0.002 -0.007 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.003 0.000 0.000 0.000 0.20%

Mid Drift: 0.007 0.001 0.000 -0.001 0.60%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 4 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: -0.023 -0.549 0.082 0.052 

Low final: 0.290 -0.529 0.092 0.061 

Mid Init: 50.177 50.041 10.015 9.879 

Mid Final: 50.858 50.107 10.013 9.856 

Run Avg: 8.638 5.559 19.419 0.981 2.526

Co: 0.133 -0.539 0.087 0.057 

Cm: 50.518 50.074 10.014 9.867 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 8.61 5.983 19.412 0.938 

47
Run S5 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 5 

Run S5 Final Bias and Drift Check

Date/Time: 11/19/2013 2:53:17 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: -0.071 -0.551 0.090 0.073 -0.475

Low Bias: 0.000 -0.007 0.002 0.005 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 50.105 49.883 9.989 9.830 50.509

Upscale Bias -0.017 -0.007 -0.003 -0.008 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.004 0.000 0.000 0.001 0.00%

Mid Drift: -0.008 -0.002 -0.001 -0.001 0.80%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 5 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.290 -0.529 0.092 0.061 

Low final: -0.071 -0.551 0.090 0.073 

Mid Init: 50.858 50.107 10.013 9.856 

Mid Final: 50.105 49.883 9.989 9.830 

Run Avg: 3.347 30.694 19.976 0.620 21.347

Co: 0.109 -0.540 0.091 0.067 

Cm: 50.482 49.995 10.001 9.843 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 3.279 30.694 20.003 0.563 

48
Run S6 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 6 

Run S6 Final Bias and Drift Check

Date/Time: 11/19/2013 3:20:35 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: 0.167 -0.545 0.071 0.045 -0.456

Low Bias: 0.002 -0.007 0.001 0.004 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 51.404 49.925 10.015 9.806 50.39

Upscale Bias -0.004 -0.006 -0.002 -0.009 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.002 0.000 -0.001 -0.001 0.00%

Mid Drift: 0.013 0.000 0.001 -0.001 -0.10%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 6 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: -0.071 -0.551 0.090 0.073 

Low final: 0.167 -0.545 0.071 0.045 

Mid Init: 50.105 49.883 9.989 9.830 

Mid Final: 51.404 49.925 10.015 9.806 

Run Avg: 4.524 4.307 19.904 0.707 0.689

Co: 0.048 -0.548 0.080 0.059 

Cm: 50.754 49.904 10.002 9.818 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 4.503 4.779 19.918 0.661 

49
Run P1H-1 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 19 Run 7 

Run P1H-1 Final Bias and Drift Check

Date/Time: 11/19/2013 4:09:40 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: -0.043 0.124 0.044 -0.024 

Low Sys: 0.314 -0.532 0.107 0.044 -0.406

Low Bias: 0.004 -0.007 0.003 0.003 

 

Upscale Cal: 51.798 50.545 10.059 9.989 

Upscale Sys: 50.889 50.157 10.018 9.812 50.705

Upscale Bias -0.009 -0.004 -0.002 -0.009 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.001 0.000 0.002 0.000 0.10%

Mid Drift: -0.005 0.002 0.000 0.000 0.30%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 7 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.167 -0.545 0.071 0.045 

Low final: 0.314 -0.532 0.107 0.044 

Mid Init: 51.404 49.925 10.015 9.806 

Mid Final: 50.889 50.157 10.018 9.812 

Run Avg: 7.728 0.498 19.778 0.795 0.011

Co: 0.241 -0.538 0.089 0.045 

Cm: 51.147 50.041 10.016 9.809 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 7.503 1.017 19.771 0.765 

50
Initial Cal Error Instrumantal QA

Testing by TRC, Austin, Texas

199009 November 20 

Initial Calibration Error Test 

Date/Time: 11/20/2013 11:57:34 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Zero ID: Low ID: Mid ID: High ID: 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 CC427175 X02NI99P15A3LE2 X02NI99P15A51P7

Calibration Error Results 

Channel: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200 200 25 25 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Zero Ref: 0.000 0.000 0.000 0.000 0

Zero Cal: 0.045 0.058 0.064 -0.001 -0.666

Zero Error: 0.000 0.001 0.003 0.000 -0.70%

 

Low Ref: 30.35

Low Cal: 30.7

Low Error: 1.20%

 

Mid Ref: 51.010 49.660 9.969 9.950 50.2

Mid Cal: 51.991 50.105 9.963 10.131 49.707

Mid Error: 0.010 0.004 0.000 0.009 -1.00%

 

High Ref: 100.100 100.100 20.000 19.600 84.96

High Cal: 100.868 99.663 19.812 19.525 85.157

High Error: 0.80% -0.40% -0.90% -0.40% 0.20%

 

Cal Result: PASSED PASSED PASSED PASSED PASSED

51
Initial System Bias Instrumantal QA

Testing by TRC, Austin, Texas

199009 November 20 

Initial System Bias Check 

Date/Time: 11/20/2013 12:04:42 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 0.932 -0.466 0.073 0.063 -0.737

Low Bias: 0.009 -0.005 0.000 0.003 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 50.157 49.787 9.944 10.084 50.303

Upscale Bias -1.80% -0.30% -0.10% -0.20% 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

52
Run P1H-2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 20 Run 1 

Run P1H-2 Final Bias and Drift Check 

Date/Time: 11/20/2013 2:33:25 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 0.823 0.027 0.112 0.048 0.07

Low Bias: 0.008 0.000 0.002 0.003 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 50.940 52.697 9.981 9.922 52.986

Upscale Bias -0.011 0.026 0.001 -0.011 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.001 0.005 0.002 -0.001 0.80%

Mid Drift: 0.008 0.029 0.002 -0.008 2.70%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 1 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.932 -0.466 0.073 0.063 

Low final: 0.823 0.027 0.112 0.048 

Mid Init: 50.157 49.787 9.944 10.084 

Mid Final: 50.940 52.697 9.981 9.922 

Run Avg: 4.077 1.006 20.081 0.510 0.794

Co: 0.877 -0.219 0.093 0.055 

Cm: 50.548 51.242 9.963 10.003 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 3.286 1.182 20.189 0.455 

53
Run P1L-1 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 20 Run 2 

Run P1L-1 Final Bias and Drift Check 

Date/Time: 11/20/2013 3:23:03 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 1.175 0.132 0.077 0.045 -0.022

Low Bias: 0.011 0.001 0.001 0.002 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 51.367 50.173 10.076 10.020 50.364

Upscale Bias -0.006 0.001 0.006 -0.006 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.004 0.001 -0.002 0.000 -0.10%

Mid Drift: 0.004 -0.025 0.005 0.005 -2.60%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 2 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.823 0.027 0.112 0.048 

Low final: 1.175 0.132 0.077 0.045 

Mid Init: 50.940 52.697 9.981 9.922 

Mid Final: 51.367 50.173 10.076 10.020 

Run Avg: 6.705 1.276 19.664 0.853 0.543

Co: 0.999 0.080 0.094 0.047 

Cm: 51.153 51.435 10.028 9.971 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 5.803 1.157 19.638 0.808 

54
Run P2H-1 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 20 Run 3 

Run P2H-1 Final Bias and Drift Check 

Date/Time: 11/20/2013 4:13:29 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 0.540 0.126 0.112 0.068 -0.328

Low Bias: 0.005 0.001 0.002 0.003 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 50.670 49.958 10.086 10.004 49.157

Upscale Bias -0.013 -0.001 0.006 -0.006 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.006 0.000 0.002 0.001 -0.30%

Mid Drift: -0.007 -0.002 0.000 -0.001 -1.20%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 3 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 1.175 0.132 0.077 0.045 

Low final: 0.540 0.126 0.112 0.068 

Mid Init: 51.367 50.173 10.076 10.020 

Mid Final: 50.670 49.958 10.086 10.004 

Run Avg: 16.107 1.849 19.412 1.067 0.422

Co: 0.858 0.129 0.095 0.056 

Cm: 51.018 50.065 10.081 10.012 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 15.508 1.71 19.284 1.01 

55
Run P2H-1b Instrumental QA

Testing by TRC, Austin, Texas

199009 November 20 Run 4 

Run P2H-1b Final Bias and Drift Check 

Date/Time: 11/20/2013 5:01:37 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 1.022 0.117 0.101 0.076 -0.083

Low Bias: 0.010 0.001 0.002 0.004 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 50.659 50.010 10.084 10.030 50.058

Upscale Bias -0.013 -0.001 0.006 -0.005 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.005 0.000 -0.001 0.000 0.20%

Mid Drift: 0.000 0.001 0.000 0.001 0.90%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 4 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.540 0.126 0.112 0.068 

Low final: 1.022 0.117 0.101 0.076 

Mid Init: 50.670 49.958 10.086 10.004 

Mid Final: 50.659 50.010 10.084 10.030 

Run Avg: 16.942 1.898 19.177 1.227 0.376

Co: 0.781 0.121 0.107 0.072 

Cm: 50.664 49.984 10.085 10.017 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 16.526 1.77 19.052 1.156 

56
Run P2L-1(b) Instrumental QA

Testing by TRC, Austin, Texas

199009 November 20 Run 5 

Run P2L-1(b) Final Bias and Drift Check 

Date/Time: 11/20/2013 6:01:44 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 1.029 0.058 0.093 0.071 -0.153

Low Bias: 0.010 0.000 0.001 0.004 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 51.137 49.791 10.065 10.034 50.098

Upscale Bias -0.009 -0.003 0.005 -0.005 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.000 -0.001 0.000 0.000 -0.10%

Mid Drift: 0.005 -0.002 -0.001 0.000 0.00%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 5 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 1.022 0.117 0.101 0.076 

Low final: 1.029 0.058 0.093 0.071 

Mid Init: 50.659 50.010 10.084 10.030 

Mid Final: 51.137 49.791 10.065 10.034 

Run Avg: 10.106 7.615 19.760 0.861 1.833

Co: 1.025 0.087 0.097 0.073 

Cm: 50.898 49.901 10.075 10.032 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 9.288 7.505 19.646 0.787 

57
Run P3H-1 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 20 Run 6 

Run P3H-1 Final Bias and Drift Check 

Date/Time: 11/20/2013 7:42:28 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A3LE2 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.045 0.058 0.064 -0.001 

Low Sys: 0.750 0.010 0.076 0.063 0.282

Low Bias: 0.007 0.000 0.001 0.003 

 

Upscale Cal: 51.991 50.105 9.963 10.131 

Upscale Sys: 51.468 49.719 10.067 10.034 51.606

Upscale Bias -0.005 -0.004 0.005 -0.005 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.003 0.000 -0.001 0.000 0.40%

Mid Drift: 0.003 -0.001 0.000 0.000 1.50%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 6 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 1.029 0.058 0.093 0.071 

Low final: 0.750 0.010 0.076 0.063 

Mid Init: 51.137 49.791 10.065 10.034 

Mid Final: 51.468 49.719 10.067 10.034 

Run Avg: 15.719 8.405 18.854 1.397 1.725

Co: 0.889 0.034 0.084 0.067 

Cm: 51.302 49.755 10.066 10.034 

Coa: 0.000 0.000 0.000 0.000 

Cma: 51.010 49.660 9.969 9.950 

Corrected: 15.005 8.361 18.746 1.327 

58
Initial Cal Error Instrumantal QA

Testing by TRC, Austin, Texas

199009 November 21 

Initial Calibration Error Test 

Date/Time: 11/21/2013 6:59:13 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Zero ID: Low ID: Mid ID: High ID: 

NOx CC351249 CC335400 CC403079 

CO CC351249 CC335400 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 CC427175 X02NI99P15A3LE2 X02NI99P15A51P7

Calibration Error Results 

Channel: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200 200 25 25 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Zero Ref: 0.000 0.000 0.000 0.000 0

Zero Cal: 0.106 0.086 0.056 0.016 -0.144

Zero Error: 0.001 0.001 0.003 0.001 -0.10%

 

Low Ref: 30.35

Low Cal: 30.438

Low Error: 0.30%

 

Mid Ref: 51.010 49.660 9.969 9.950 50.2

Mid Cal: 50.635 50.431 10.088 10.169 50.354

Mid Error: -0.004 0.008 0.006 0.011 0.30%

 

High Ref: 100.100 100.100 20.000 19.600 84.96

High Cal: 100.349 99.970 20.074 19.586 85.09

High Error: 0.20% -0.10% 0.40% -0.10% 0.20%

 

Cal Result: PASSED PASSED PASSED PASSED PASSED

59
Initial System Bias Instrumantal QA

Testing by TRC, Austin, Texas

199009 November 21 

Initial System Bias Check 

Date/Time: 11/21/2013 7:07:08 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 1.140 -0.608 0.088 0.066 -0.005

Low Bias: 0.010 -0.007 0.002 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 101.043 100.756 10.068 10.116 84.656

Upscale Bias 0.70% 0.80% -0.10% -0.30% 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

60
Run P3L-1b Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 1 

Run P3L-1b Final Bias and Drift Check 

Date/Time: 11/21/2013 9:30:36 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 1.026 -0.470 0.091 0.081 -0.61

Low Bias: 0.009 -0.006 0.002 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.211 99.810 10.096 10.102 86.282

Upscale Bias -0.001 -0.002 0.000 -0.003 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.001 0.001 0.000 0.001 -0.60%

Mid Drift: -0.008 -0.009 0.001 -0.001 1.60%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 1 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 1.140 -0.608 0.088 0.066 

Low final: 1.026 -0.470 0.091 0.081 

Mid Init: 101.043 100.756 10.068 10.116 

Mid Final: 100.211 99.810 10.096 10.102 

Run Avg: 13.035 4.814 18.959 1.327 0.16

Co: 1.083 -0.539 0.090 0.074 

Cm: 100.627 100.283 10.082 10.109 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 12.018 5.315 18.825 1.242 

61
Run P1L-2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 2 

Run P1L-2 Final Bias and Drift Check 

Date/Time: 11/21/2013 10:08:32 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.553 -0.523 0.074 0.074 -0.222

Low Bias: 0.004 -0.006 0.001 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 99.814 100.406 10.084 10.118 86.165

Upscale Bias -0.005 0.004 0.000 -0.003 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.005 -0.001 -0.001 0.000 0.40%

Mid Drift: -0.004 0.006 -0.001 0.001 -0.10%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 2 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 1.026 -0.470 0.091 0.081 

Low final: 0.553 -0.523 0.074 0.074 

Mid Init: 100.211 99.810 10.096 10.102 

Mid Final: 99.814 100.406 10.084 10.118 

Run Avg: 9.355 1.522 19.220 1.356 -0.386

Co: 0.790 -0.497 0.082 0.078 

Cm: 100.012 100.108 10.090 10.110 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 8.641 2.008 19.064 1.268 

62
Run P2H-2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 3 

Run P2H-2 Final Bias and Drift Check 

Date/Time: 11/21/2013 11:20:51 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.485 -0.529 0.085 0.061 0.456

Low Bias: 0.004 -0.006 0.001 0.002 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.993 99.770 10.107 10.104 86.528

Upscale Bias 0.006 -0.002 0.001 -0.003 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.001 0.000 0.001 -0.001 0.70%

Mid Drift: 0.012 -0.006 0.001 -0.001 0.40%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 3 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.553 -0.523 0.074 0.074 

Low final: 0.485 -0.529 0.085 0.061 

Mid Init: 99.814 100.406 10.084 10.118 

Mid Final: 100.993 99.770 10.107 10.104 

Run Avg: 10.740 2.486 19.752 0.894 0.39

Co: 0.519 -0.526 0.079 0.067 

Cm: 100.403 100.088 10.096 10.111 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 10.243 2.997 19.58 0.819 

63
Run P2L-2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 4 

Run P2L-2 Final Bias and Drift Check 

Date/Time: 11/21/2013 11:55:51 AM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.463 -0.475 0.097 0.065 0.448

Low Bias: 0.004 -0.006 0.002 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.833 99.943 10.094 10.098 85.22

Upscale Bias 0.005 0.000 0.000 -0.004 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.000 0.001 0.001 0.000 0.00%

Mid Drift: -0.002 0.002 -0.001 0.000 -1.30%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 4 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.485 -0.529 0.085 0.061 

Low final: 0.463 -0.475 0.097 0.065 

Mid Init: 100.993 99.770 10.107 10.104 

Mid Final: 100.833 99.943 10.094 10.098 

Run Avg: 9.520 6.889 19.850 0.843 1.837

Co: 0.474 -0.502 0.091 0.063 

Cm: 100.913 99.857 10.100 10.101 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 9.015 7.372 19.679 0.774 

64
Run P3H-2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 5 

Run P3H-2 Final Bias and Drift Check 

Date/Time: 11/21/2013 1:10:18 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.463 -0.527 0.089 0.053 -0.091

Low Bias: 0.004 -0.006 0.002 0.002 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 101.146 99.696 10.094 10.070 85.004

Upscale Bias 0.008 -0.003 0.000 -0.005 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.000 -0.001 0.000 -0.001 -0.50%

Mid Drift: 0.003 -0.002 0.000 -0.001 -0.20%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 5 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.463 -0.475 0.097 0.065 

Low final: 0.463 -0.527 0.089 0.053 

Mid Init: 100.833 99.943 10.094 10.098 

Mid Final: 101.146 99.696 10.094 10.070 

Run Avg: 8.448 3.244 19.697 0.884 1.204

Co: 0.463 -0.501 0.093 0.059 

Cm: 100.990 99.819 10.094 10.084 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 7.951 3.736 19.542 0.819 

65
Run P3L-2 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 6 

Run P3L-2 Final Bias and Drift Check 

Date/Time: 11/21/2013 1:41:26 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.647 -0.529 0.088 0.082 0.613

Low Bias: 0.005 -0.006 0.002 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.208 99.924 10.090 10.109 85.391

Upscale Bias -0.001 0.000 0.000 -0.003 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.002 0.000 0.000 0.001 0.70%

Mid Drift: -0.009 0.002 0.000 0.002 0.40%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 6 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.463 -0.527 0.089 0.053 

Low final: 0.647 -0.529 0.088 0.082 

Mid Init: 101.146 99.696 10.094 10.070 

Mid Final: 100.208 99.924 10.090 10.109 

Run Avg: 9.119 3.377 19.523 0.992 1.095

Co: 0.555 -0.528 0.088 0.067 

Cm: 100.677 99.810 10.092 10.089 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 8.562 3.896 19.367 0.918 

66
Run P1H-3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 7 

Run P1H-3 Final Bias and Drift Check 

Date/Time: 11/21/2013 2:19:06 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.492 -0.519 0.054 0.029 0.187

Low Bias: 0.004 -0.006 0.000 0.001 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 101.280 100.119 10.104 10.104 84.584

Upscale Bias 0.009 0.001 0.001 -0.003 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.002 0.000 -0.002 -0.003 -0.40%

Mid Drift: 0.011 0.002 0.001 0.000 -0.80%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 7 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.647 -0.529 0.088 0.082 

Low final: 0.492 -0.519 0.054 0.029 

Mid Init: 100.208 99.924 10.090 10.109 

Mid Final: 101.280 100.119 10.104 10.104 

Run Avg: 10.989 0.879 19.242 1.333 0.851

Co: 0.569 -0.524 0.071 0.055 

Cm: 100.744 100.021 10.097 10.106 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 10.412 1.397 19.061 1.265 

67
Run P2L-3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 8 

Run P2L-3 Final Bias and Drift Check 

Date/Time: 11/21/2013 3:03:59 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.987 -0.525 0.080 0.069 -0.253

Low Bias: 0.009 -0.006 0.001 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.804 99.840 10.084 10.122 84.352

Upscale Bias 0.005 -0.001 0.000 -0.002 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.005 0.000 0.001 0.002 -0.40%

Mid Drift: -0.005 -0.003 -0.001 0.001 -0.20%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 8 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.492 -0.519 0.054 0.029 

Low final: 0.987 -0.525 0.080 0.069 

Mid Init: 101.280 100.119 10.104 10.104 

Mid Final: 100.804 99.840 10.084 10.122 

Run Avg: 13.522 6.904 19.456 1.092 1.062

Co: 0.739 -0.522 0.067 0.049 

Cm: 101.042 99.979 10.094 10.113 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 12.757 7.396 19.277 1.032 

68
Run P3L-3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 9 

Run P3L-3 Final Bias and Drift Check 

Date/Time: 11/21/2013 3:31:16 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.483 -0.586 0.083 0.072 0.224

Low Bias: 0.004 -0.007 0.001 0.003 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.721 99.779 10.089 10.142 85.034

Upscale Bias 0.004 -0.002 0.000 -0.001 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.005 -0.001 0.000 0.000 0.50%

Mid Drift: -0.001 -0.001 0.000 0.001 0.70%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 9 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.987 -0.525 0.080 0.069 

Low final: 0.483 -0.586 0.083 0.072 

Mid Init: 100.804 99.840 10.084 10.122 

Mid Final: 100.721 99.779 10.089 10.142 

Run Avg: 13.082 6.561 18.937 1.372 1.268

Co: 0.735 -0.556 0.081 0.070 

Cm: 100.763 99.810 10.086 10.132 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 12.356 7.098 18.788 1.287 

69
Run P3H-3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 10 

Run P3H-3 Final Bias and Drift Check 

Date/Time: 11/21/2013 3:59:39 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.400 -0.540 0.090 0.092 0.127

Low Bias: 0.003 -0.006 0.002 0.004 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 100.154 99.211 10.098 10.164 85.315

Upscale Bias -0.002 -0.008 0.001 0.000 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.001 0.000 0.000 0.001 -0.10%

Mid Drift: -0.006 -0.006 0.000 0.001 0.30%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 10 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.483 -0.586 0.083 0.072 

Low final: 0.400 -0.540 0.090 0.092 

Mid Init: 100.721 99.779 10.089 10.142 

Mid Final: 100.154 99.211 10.098 10.164 

Run Avg: 10.871 8.228 19.385 1.075 1.916

Co: 0.441 -0.563 0.087 0.082 

Cm: 100.437 99.495 10.094 10.153 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 10.441 8.795 19.225 0.981 

70
Run P2H-3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 11 

Run P2H-3 Final Bias and Drift Check 

Date/Time: 11/21/2013 4:27:25 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.555 -0.525 0.079 0.048 0.047

Low Bias: 0.004 -0.006 0.001 0.002 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 101.282 99.498 10.118 10.147 84.357

Upscale Bias 0.009 -0.005 0.002 -0.001 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: 0.002 0.000 -0.001 -0.002 -0.10%

Mid Drift: 0.011 0.003 0.001 -0.001 -1.00%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 11 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.400 -0.540 0.090 0.092 

Low final: 0.555 -0.525 0.079 0.048 

Mid Init: 100.154 99.211 10.098 10.164 

Mid Final: 101.282 99.498 10.118 10.147 

Run Avg: 12.040 4.781 19.597 1.011 0.967

Co: 0.477 -0.533 0.085 0.070 

Cm: 100.718 99.355 10.108 10.155 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 11.546 5.325 19.406 0.928 

71
Run P1L-3 Instrumental QA

Testing by TRC, Austin, Texas

199009 November 21 Run 12 

Run P1L-3 Final Bias and Drift Check 

Date/Time: 11/21/2013 4:57:14 PM

Result: PASS 

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 Reference Cylinder IDs

 Low ID Upscale ID Span ID 

NOx CC351249 CC403079 CC403079 

CO CC351249 CC403079 CC403079 

O2 CC335400 CC351249 EB0045768 

CO2 CC335400 CC351249 EB0045768 

C3H8-Propyl CC351249 X02NI99P15A51P7 

System Bias Check Results 

Analyte: NOx CO O2 CO2 C3H8-Propyl

Units: ppm ppm % % ppm

Span: 100.100 100.100 20.000 19.600 100

Range: 200.000 200.000 25.000 25.000 100

Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

 

Low Cal: 0.106 0.086 0.056 0.016 

Low Sys: 0.395 -0.519 0.078 0.061 -0.279

Low Bias: 0.003 -0.006 0.001 0.002 

 

Upscale Cal: 100.349 99.970 10.088 10.169 

Upscale Sys: 101.589 99.777 10.122 10.152 84.487

Upscale Bias 0.012 -0.002 0.002 -0.001 

 

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results 

Low Drift: -0.002 0.000 0.000 0.001 -0.30%

Mid Drift: 0.003 0.003 0.000 0.000 0.10%

Drift Result: PASSED PASSED PASSED PASSED PASSED

 

Cal Result: OK OK OK OK OK

Test Run 12 Bias Correction Calculations:

 NOx CO O2 CO2 C3H8-Propyl

Low init: 0.555 -0.525 0.079 0.048 

Low final: 0.395 -0.519 0.078 0.061 

Mid Init: 101.282 99.498 10.118 10.147 

Mid Final: 101.589 99.777 10.122 10.152 

Run Avg: 5.861 1.061 19.955 0.870 0.468

Co: 0.475 -0.522 0.078 0.055 

Cm: 101.436 99.638 10.120 10.149 

Coa: 0.000 0.000 0.000 0.000 

Cma: 100.100 100.100 9.969 9.950 

Corrected: 5.34 1.582 19.733 0.803 

72
Appendix D: 

Datalog Records and Chromatograms





 

73
Run S1 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run S1 

Start: 11/19/2013 9:18:55 AM

End: 11/19/2013 9:38:55 AM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 9:19:55 AM 1min avg: 10.154 7.485 19.520 1.024 0.376

 9:20:55 AM 1min avg: 10.148 5.376 19.722 0.890 1.486

 9:21:55 AM 1min avg: 14.289 8.979 18.929 1.439 2.440

 9:22:55 AM 1min avg: 14.182 9.542 19.025 1.337 2.099

 9:23:55 AM 1min avg: 17.549 9.870 19.286 1.152 1.753

 9:24:55 AM 1min avg: 12.625 5.722 20.119 0.654 0.769

 9:25:55 AM 1min avg: 9.961 5.574 19.605 0.941 0.286

 9:26:55 AM 1min avg: 7.076 2.774 20.434 0.429 1.633

 9:27:55 AM 1min avg: 13.429 9.586 18.936 1.383 2.692

 9:28:55 AM 1min avg: 12.671 6.940 19.875 0.806 -0.052

 9:29:55 AM 1min avg: 10.035 4.296 19.773 0.834 2.045

 9:30:55 AM 1min avg: 13.290 7.056 20.046 0.712 1.191

 9:31:55 AM 1min avg: 10.219 7.134 19.369 1.120 2.429

 9:32:55 AM 1min avg: 13.386 10.491 19.298 1.118 1.953

 9:33:55 AM 1min avg: 13.523 7.678 19.748 0.889 1.466

 9:34:55 AM 1min avg: 10.092 5.554 20.211 0.571 -0.165

 9:35:55 AM 1min avg: 4.708 1.734 20.445 0.403 0.704

 9:36:55 AM 1min avg: 14.929 6.846 19.566 0.994 2.750

 9:37:55 AM 1min avg: 16.336 10.424 19.190 1.200 3.312

 9:38:55 AM 1min avg: 16.933 9.954 19.576 0.977 2.001

 9:38:55 AM Test Avgs: 12.277 7.151 19.634 0.944 1.558

74
Run S2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run S2 

Start: 11/19/2013 9:45:00 AM

End: 11/19/2013 10:05:01 AM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 9:46:00 AM 1min avg: 12.228 1.070 19.635 0.908 -0.464

 9:47:00 AM 1min avg: 15.192 1.336 19.575 0.967 -0.397

 9:48:00 AM 1min avg: 12.773 1.333 19.927 0.733 -0.448

 9:49:00 AM 1min avg: 13.123 1.490 19.229 1.177 -0.098

 9:50:00 AM 1min avg: 16.778 1.831 19.211 1.199 0.419

 9:51:00 AM 1min avg: 16.299 1.578 19.402 1.073 0.368

 9:52:00 AM 1min avg: 9.547 0.947 20.247 0.543 0.397

 9:53:00 AM 1min avg: 8.067 0.826 20.133 0.635 0.337

 9:54:00 AM 1min avg: 4.705 0.606 20.478 0.368 0.560

 9:55:00 AM 1min avg: 14.435 1.643 19.208 1.185 0.577

 9:56:00 AM 1min avg: 15.722 1.765 19.214 1.196 0.337

 9:57:00 AM 1min avg: 14.990 1.760 19.242 1.181 0.358

 9:58:00 AM 1min avg: 11.582 1.051 19.881 0.803 0.261

 9:59:00 AM 1min avg: 15.895 1.262 19.375 1.092 0.584

10:00:00 AM 1min avg: 16.953 1.782 19.352 1.092 1.134

10:01:00 AM 1min avg: 18.801 2.017 19.665 0.976 0.613

10:02:00 AM 1min avg: 7.888 1.253 19.815 0.828 0.341

10:03:00 AM 1min avg: 6.233 0.591 20.796 0.178 0.304

10:04:00 AM 1min avg: 7.019 0.994 19.571 0.929 0.392

10:05:00 AM 1min avg: 14.670 1.633 19.465 1.014 0.434

10:05:01 AM Test Avgs: 12.645 1.338 19.671 0.904 0.300

75
Run S3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run S3 

Start: 11/19/2013 11:29:00 AM

End: 11/19/2013 12:01:01 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

11:30:00 AM 1min avg: 1.710 9.653 20.131 0.571 10.631

11:31:00 AM 1min avg: 2.178 14.209 19.820 0.743 10.925

11:32:00 AM 1min avg: 3.143 11.245 20.184 0.543 7.587

11:33:00 AM 1min avg: 2.489 12.785 19.887 0.710 8.342

11:34:00 AM 1min avg: 2.967 12.430 20.123 0.586 9.248

11:35:00 AM 1min avg: 2.465 12.952 20.189 0.558 6.162

11:36:00 AM 1min avg: 1.602 7.412 20.328 0.462 14.189

11:37:00 AM 1min avg: 1.039 5.490 20.723 0.195 30.427

11:38:00 AM 1min avg: 0.012 0.108 20.861 0.082 8.899

11:39:00 AM 1min avg: -0.049 0.109 20.883 0.081 0.918

11:40:00 AM 1min avg: -0.230 0.147 20.899 0.080 1.337

11:41:00 AM 1min avg: -0.254 0.164 20.864 0.079 29.781

11:42:00 AM 1min avg: -0.042 2.115 20.443 0.336 12.701

11:43:00 AM 1min avg: 4.063 18.388 19.432 0.998 7.310

11:44:00 AM 1min avg: 2.719 9.453 20.357 0.449 7.815

11:45:00 AM 1min avg: 1.567 9.563 20.417 0.409 2.884

11:46:00 AM 1min avg: 1.237 7.115 20.261 0.471 8.785

11:47:00 AM 1min avg: 2.748 14.666 19.972 0.683 6.467

11:48:00 AM 1min avg: 2.964 11.790 19.868 0.700 10.056

11:49:00 AM 1min avg: 2.797 17.313 19.904 0.683 10.660

11:50:00 AM 1min avg: 4.269 14.043 19.911 0.700 10.853

11:51:00 AM 1min avg: 2.392 10.854 20.393 0.423 3.741

11:52:00 AM 1min avg: 0.318 1.955 20.819 0.144 0.532

11:53:00 AM 1min avg: 1.332 7.363 19.912 0.646 11.505

11:54:00 AM 1min avg: 4.159 15.437 19.844 0.750 6.309

11:55:00 AM 1min avg: 2.319 9.361 20.558 0.324 7.087

11:56:00 AM 1min avg: 1.558 5.620 20.353 0.415 6.406

11:57:00 AM 1min avg: 4.695 14.037 19.849 0.757 9.277

11:58:00 AM 1min avg: 3.158 11.280 19.945 0.664 10.534

11:59:00 AM 1min avg: 3.375 15.043 19.930 0.699 8.772

12:00:00 PM 1min avg: 3.853 15.785 19.652 0.852 9.261

12:01:00 PM 1min avg: 2.861 13.074 19.972 0.668 8.359

12:01:01 PM Test Avgs: 2.169 9.718 20.209 0.514 9.305

76
Run S4 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run S4 

Start: 11/19/2013 1:36:01 PM

End: 11/19/2013 1:56:01 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 1:37:01 PM 1min avg: 8.805 5.067 19.180 1.127 1.449

 1:38:01 PM 1min avg: 11.953 6.503 19.216 1.134 2.700

 1:39:01 PM 1min avg: 5.701 5.044 19.677 0.796 0.709

 1:40:01 PM 1min avg: 7.205 3.509 19.784 0.760 0.657

 1:41:01 PM 1min avg: 9.858 4.192 18.824 1.335 1.857

 1:42:01 PM 1min avg: 12.111 7.185 19.619 0.905 1.646

 1:43:01 PM 1min avg: 5.211 3.282 20.399 0.389 6.705

 1:44:01 PM 1min avg: 8.398 4.763 19.312 1.051 1.185

 1:45:01 PM 1min avg: 7.336 4.739 19.774 0.755 1.702

 1:46:01 PM 1min avg: 6.911 5.568 19.118 1.167 0.805

 1:47:01 PM 1min avg: 7.842 5.041 19.700 0.799 1.699

 1:48:01 PM 1min avg: 9.549 6.076 19.611 0.867 4.180

 1:49:01 PM 1min avg: 6.711 4.897 19.434 0.951 2.410

 1:50:01 PM 1min avg: 10.829 7.753 18.963 1.266 1.865

 1:51:01 PM 1min avg: 9.169 5.814 19.181 1.126 2.784

 1:52:01 PM 1min avg: 6.335 5.476 19.775 0.725 4.978

 1:53:01 PM 1min avg: 12.173 6.640 18.864 1.366 3.967

 1:54:01 PM 1min avg: 6.928 6.890 19.339 1.002 2.951

 1:55:01 PM 1min avg: 10.475 7.800 18.948 1.262 1.463

 1:56:01 PM 1min avg: 9.263 4.931 19.652 0.842 4.814

 1:56:01 PM Test Avgs: 8.638 5.559 19.419 0.981 2.526

77
Run S5 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run S5 

Start: 11/19/2013 2:18:47 PM

End: 11/19/2013 2:47:38 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 2:19:47 PM 1min avg: 4.034 38.593 19.971 0.619 26.935

 2:20:47 PM 1min avg: 3.662 35.488 19.625 0.824 31.287

 2:21:47 PM 1min avg: 4.449 36.253 20.024 0.601 15.380

 2:22:47 PM 1min avg: 4.959 32.585 19.708 0.757 23.552

 2:23:47 PM 1min avg: 4.277 36.981 19.800 0.733 16.466

 2:24:47 PM 1min avg: 3.777 22.371 20.007 0.588 21.033

 2:25:47 PM 1min avg: 3.426 31.400 20.046 0.597 22.274

 2:26:47 PM 1min avg: 2.950 36.226 19.787 0.729 29.157

 2:27:47 PM 1min avg: 3.266 46.902 19.744 0.759 31.510

 2:28:47 PM 1min avg: 2.545 31.814 20.216 0.482 25.990

 2:38:37 PM 1min avg: 2.615 28.017 20.356 0.391 18.111

 2:39:37 PM 1min avg: 2.241 24.726 19.980 0.614 17.302

 2:40:37 PM 1min avg: 2.870 22.330 20.131 0.542 20.472

 2:41:37 PM 1min avg: 3.091 33.476 19.801 0.726 16.267

 2:42:37 PM 1min avg: 2.727 25.737 20.108 0.554 18.716

 2:43:37 PM 1min avg: 2.360 21.238 20.476 0.326 6.886

 2:44:37 PM 1min avg: 1.318 10.848 20.382 0.371 16.551

 2:45:37 PM 1min avg: 2.941 23.932 20.092 0.549 24.981

 2:46:37 PM 1min avg: 4.387 38.881 19.656 0.811 24.471

 2:47:37 PM 1min avg: 4.998 36.064 19.602 0.839 19.889

 2:47:38 PM Test Avgs: 3.347 30.694 19.976 0.620 21.347

78
Run S6 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run S6 

Start: 11/19/2013 2:56:01 PM

End: 11/19/2013 3:16:02 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 2:57:01 PM 1min avg: 5.548 3.160 19.927 0.722 0.232

 2:58:01 PM 1min avg: 3.889 3.690 19.750 0.812 1.034

 2:59:01 PM 1min avg: 3.625 5.331 20.030 0.596 1.281

 3:00:01 PM 1min avg: 3.742 4.025 20.041 0.623 0.628

 3:01:01 PM 1min avg: 5.710 5.788 19.338 1.078 0.231

 3:02:01 PM 1min avg: 5.311 3.045 20.132 0.565 0.184

 3:03:01 PM 1min avg: 2.712 3.038 19.777 0.764 0.937

 3:04:01 PM 1min avg: 4.541 5.217 20.135 0.566 0.278

 3:05:01 PM 1min avg: 1.967 1.180 20.412 0.366 0.216

 3:06:01 PM 1min avg: 1.904 1.562 20.190 0.481 0.196

 3:07:01 PM 1min avg: 5.758 2.063 19.690 0.847 0.669

 3:08:01 PM 1min avg: 5.503 7.153 19.988 0.674 0.669

 3:09:01 PM 1min avg: 3.624 3.802 19.775 0.787 0.726

 3:10:01 PM 1min avg: 4.369 5.671 19.809 0.751 0.985

 3:11:01 PM 1min avg: 5.726 4.810 19.922 0.713 0.627

 3:12:01 PM 1min avg: 5.894 4.838 19.459 0.986 0.228

 3:13:01 PM 1min avg: 7.322 4.557 19.804 0.795 0.882

 3:14:01 PM 1min avg: 4.744 6.454 19.545 0.957 2.303

 3:15:01 PM 1min avg: 3.975 6.386 20.301 0.437 0.862

 3:16:01 PM 1min avg: 4.668 4.389 20.050 0.618 0.608

 3:16:02 PM Test Avgs: 4.524 4.307 19.904 0.707 0.689

79
Run P1H-1 Datalog Records

Testing by TRC, Austin, Texas

199009 November 19 

Run P1H-1 

Start: 11/19/2013 3:45:01 PM

End: 11/19/2013 4:05:02 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 3:46:01 PM 1min avg: 6.452 0.394 20.235 0.514 0.081

 3:47:01 PM 1min avg: 3.951 0.271 20.138 0.529 -0.019

 3:48:01 PM 1min avg: 8.024 0.730 19.801 0.762 0.037

 3:49:01 PM 1min avg: 8.813 0.476 19.432 1.056 0.032

 3:50:01 PM 1min avg: 4.153 0.384 20.260 0.466 -0.025

 3:51:01 PM 1min avg: 6.138 0.415 19.995 0.624 0.053

 3:52:01 PM 1min avg: 10.556 0.609 19.310 1.132 -0.048

 3:53:01 PM 1min avg: 11.904 0.650 19.231 1.133 -0.020

 3:54:01 PM 1min avg: 13.203 0.637 18.908 1.379 -0.002

 3:55:01 PM 1min avg: 10.557 0.688 19.470 1.026 -0.043

 3:56:01 PM 1min avg: 10.010 0.650 19.568 0.933 0.006

 3:57:01 PM 1min avg: 10.284 0.649 19.401 1.049 0.026

 3:58:01 PM 1min avg: 8.648 0.711 19.955 0.690 0.059

 3:59:01 PM 1min avg: 6.018 0.227 20.459 0.353 0.062

 4:00:01 PM 1min avg: 1.489 0.279 20.312 0.424 0.044

 4:01:01 PM 1min avg: 4.499 0.301 20.383 0.409 0.081

 4:02:01 PM 1min avg: 3.947 0.320 19.790 0.772 0.003

 4:03:01 PM 1min avg: 9.213 0.669 19.748 0.816 -0.007

 4:04:01 PM 1min avg: 9.104 0.519 19.800 0.776 -0.043

 4:05:01 PM 1min avg: 7.439 0.381 19.386 1.049 -0.048

 4:05:02 PM Test Avgs: 7.728 0.498 19.778 0.795 0.011

80
Run P1H-2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 20 

Run P1H-2 

Start: 11/20/2013 2:09:01 PM

End: 11/20/2013 2:29:01 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 2:10:01 PM 1min avg: 7.003 1.370 19.754 0.763 0.920

 2:11:01 PM 1min avg: 2.142 1.037 20.277 0.366 0.855

 2:12:01 PM 1min avg: 5.958 1.124 19.775 0.728 0.900

 2:13:01 PM 1min avg: 3.297 1.033 20.297 0.373 0.839

 2:14:01 PM 1min avg: 4.694 1.082 19.930 0.589 0.806

 2:15:01 PM 1min avg: 7.290 1.365 19.552 0.865 0.795

 2:16:01 PM 1min avg: 9.990 1.314 19.389 0.960 0.787

 2:17:01 PM 1min avg: 8.142 1.226 19.573 0.895 0.833

 2:18:01 PM 1min avg: 7.952 1.152 19.592 0.828 0.833

 2:19:01 PM 1min avg: 2.527 0.884 20.208 0.462 0.833

 2:20:01 PM 1min avg: 1.953 0.796 20.487 0.230 0.810

 2:21:01 PM 1min avg: 0.678 0.725 20.663 0.089 0.821

 2:22:01 PM 1min avg: 0.594 0.717 20.604 0.132 0.831

 2:23:01 PM 1min avg: 1.458 0.785 20.410 0.270 0.782

 2:24:01 PM 1min avg: 1.932 0.799 20.461 0.230 0.766

 2:25:01 PM 1min avg: 4.194 0.944 19.919 0.649 0.714

 2:26:01 PM 1min avg: 3.909 0.951 20.009 0.558 0.691

 2:27:01 PM 1min avg: 3.586 1.046 20.243 0.426 0.713

 2:28:01 PM 1min avg: 2.334 0.884 20.230 0.398 0.700

 2:29:01 PM 1min avg: 1.912 0.876 20.246 0.395 0.641

 2:29:01 PM Test Avgs: 4.077 1.006 20.081 0.510 0.794

81
Run P1L-1 Datalog Records

Testing by TRC, Austin, Texas

199009 November 20 

Run P1L-1 

Start: 11/20/2013 2:57:01 PM

End: 11/20/2013 3:17:01 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 2:58:01 PM 1min avg: 2.837 1.005 20.434 0.281 0.693

 2:59:01 PM 1min avg: 1.506 0.894 20.527 0.190 0.594

 3:00:01 PM 1min avg: 4.030 1.092 20.056 0.520 0.666

 3:01:01 PM 1min avg: 4.024 1.178 20.014 0.568 0.625

 3:02:01 PM 1min avg: 4.801 1.419 19.748 0.737 0.573

 3:03:01 PM 1min avg: 5.163 1.159 19.977 0.576 0.570

 3:04:01 PM 1min avg: 2.852 0.964 20.164 0.432 0.566

 3:05:01 PM 1min avg: 9.534 1.637 18.610 1.567 0.480

 3:06:01 PM 1min avg: 9.564 1.508 19.166 1.134 0.499

 3:07:01 PM 1min avg: 9.788 1.551 18.916 1.307 0.514

 3:08:01 PM 1min avg: 8.467 1.335 19.435 0.978 0.589

 3:09:01 PM 1min avg: 8.313 1.300 19.744 0.747 0.515

 3:10:01 PM 1min avg: 7.526 1.378 19.084 1.169 0.546

 3:11:01 PM 1min avg: 6.674 1.284 19.572 0.918 0.440

 3:12:01 PM 1min avg: 8.656 1.336 19.089 1.251 0.473

 3:13:01 PM 1min avg: 12.364 1.537 19.438 1.195 0.540

 3:14:01 PM 1min avg: 5.075 0.949 20.502 0.407 0.544

 3:15:01 PM 1min avg: 7.726 1.286 19.103 1.364 0.514

 3:16:01 PM 1min avg: 8.163 1.411 19.583 1.030 0.469

 3:17:01 PM 1min avg: 7.033 1.291 20.109 0.688 0.443

 3:17:01 PM Test Avgs: 6.705 1.276 19.664 0.853 0.543

82
Run P2H-1 Datalog Records

Testing by TRC, Austin, Texas

199009 November 20 

Run P2H-1 

Start: 11/20/2013 4:01:12 PM

End: 11/20/2013 4:09:16 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 4:02:12 PM 1min avg: 14.857 1.708 19.574 0.961 0.442

 4:03:12 PM 1min avg: 17.259 1.781 19.203 1.188 0.451

 4:04:12 PM 1min avg: 16.293 1.815 19.346 1.109 0.398

 4:05:12 PM 1min avg: 14.149 2.250 19.323 1.136 0.430

 4:09:16 PM Test Avgs: 16.107 1.849 19.412 1.067 0.422

83
Run P2H-1b Datalog Records

Testing by TRC, Austin, Texas

199009 November 20 

Run P2H-1b 

Start: 11/20/2013 4:37:01 PM

End: 11/20/2013 4:56:57 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 4:38:01 PM 1min avg: 14.238 1.576 18.991 1.370 0.357

 4:39:01 PM 1min avg: 11.018 1.382 19.411 1.098 0.372

 4:40:01 PM 1min avg: 11.701 1.502 19.402 1.076 0.326

 4:41:01 PM 1min avg: 12.839 1.298 19.500 0.998 0.369

 4:42:01 PM 1min avg: 12.285 1.608 19.720 0.883 0.340

 4:43:01 PM 1min avg: 14.748 1.997 19.434 1.049 0.426

 4:44:01 PM 1min avg: 13.354 2.001 19.466 1.041 0.399

 4:45:01 PM 1min avg: 15.468 2.193 19.104 1.237 0.326

 4:46:01 PM 1min avg: 22.783 2.028 18.638 1.588 0.418

 4:47:01 PM 1min avg: 22.836 2.185 19.185 1.263 0.458

 4:48:01 PM 1min avg: 12.534 1.203 19.259 1.164 0.351

 4:49:01 PM 1min avg: 20.398 2.014 18.851 1.470 0.383

 4:50:01 PM 1min avg: 17.094 2.161 19.201 1.203 0.331

 4:51:01 PM 1min avg: 18.661 1.485 19.270 1.160 0.417

 4:52:01 PM 1min avg: 18.111 2.089 18.985 1.335 0.321

 4:53:01 PM 1min avg: 19.363 2.346 18.770 1.495 0.401

 4:54:01 PM 1min avg: 22.847 2.205 18.929 1.408 0.439

 4:55:01 PM 1min avg: 19.383 2.591 19.094 1.263 0.365

 4:56:01 PM 1min avg: 19.243 1.660 19.111 1.239 0.324

 4:56:57 PM Test Avgs: 16.942 1.898 19.177 1.227 0.376

84
Run P2L-1(b) Datalog Records

Testing by TRC, Austin, Texas

199009 November 20 

Run P2L-1(b) 

Start: 11/20/2013 5:23:05 PM

End: 11/20/2013 5:55:52 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 5:24:04 PM 1min avg: 10.066 19.477 19.815 0.841 3.509

 5:25:04 PM 1min avg: 5.963 11.275 20.215 0.561 5.483

 5:26:04 PM 1min avg: 11.024 17.447 19.419 1.052 7.902

 5:39:51 PM 1min avg: 10.903 9.986 19.284 1.186 0.991

 5:40:51 PM 1min avg: 8.773 4.534 20.410 0.461 0.679

 5:41:51 PM 1min avg: 2.988 1.501 20.822 0.171 0.909

 5:42:51 PM 1min avg: 6.249 3.929 20.223 0.563 0.724

 5:43:51 PM 1min avg: 5.100 2.999 20.405 0.464 0.838

 5:44:51 PM 1min avg: 3.675 2.783 20.466 0.390 1.037

 5:45:51 PM 1min avg: 7.811 5.107 19.756 0.879 0.974

 5:46:51 PM 1min avg: 17.235 8.730 18.770 1.473 1.592

 5:47:51 PM 1min avg: 16.675 7.523 19.515 1.061 0.993

 5:48:51 PM 1min avg: 9.529 5.025 19.815 0.819 1.481

 5:49:51 PM 1min avg: 9.220 8.458 19.560 1.002 0.945

 5:50:51 PM 1min avg: 8.784 4.719 19.629 0.937 1.391

 5:51:51 PM 1min avg: 13.241 7.892 19.267 1.158 1.444

 5:52:51 PM 1min avg: 21.098 9.005 18.978 1.353 1.745

 5:53:51 PM 1min avg: 10.591 8.670 19.640 0.932 1.530

 5:54:51 PM 1min avg: 13.435 7.167 19.493 1.055 0.942

 5:55:51 PM 1min avg: 9.733 6.050 19.738 0.847 1.569

 5:55:52 PM Test Avgs: 10.106 7.615 19.760 0.861 1.833

85
Run P3H-1 Datalog Records

Testing by TRC, Austin, Texas

199009 November 20 

Run P3H-1 

Start: 11/20/2013 7:18:05 PM

End: 11/20/2013 7:38:05 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 7:19:04 PM 1min avg: 19.182 12.605 18.317 1.761 1.943

 7:20:04 PM 1min avg: 14.636 8.022 19.596 0.930 1.236

 7:21:04 PM 1min avg: 8.795 3.669 19.556 0.934 1.800

 7:22:04 PM 1min avg: 17.506 11.669 18.152 1.841 2.859

 7:23:04 PM 1min avg: 22.318 13.812 18.669 1.522 1.592

 7:24:04 PM 1min avg: 8.836 4.966 19.761 0.858 1.426

 7:25:04 PM 1min avg: 7.938 5.849 19.403 1.022 1.524

 7:26:04 PM 1min avg: 14.067 4.040 19.577 0.940 1.646

 7:27:04 PM 1min avg: 14.252 8.160 18.501 1.603 2.017

 7:28:04 PM 1min avg: 19.888 8.417 18.609 1.518 1.809

 7:29:04 PM 1min avg: 16.740 9.877 18.476 1.638 1.514

 7:30:04 PM 1min avg: 15.866 6.504 18.894 1.423 1.325

 7:31:04 PM 1min avg: 12.329 7.285 18.888 1.356 2.175

 7:32:04 PM 1min avg: 19.602 11.307 18.309 1.752 1.424

 7:33:04 PM 1min avg: 15.049 8.460 18.696 1.478 2.327

 7:34:04 PM 1min avg: 17.341 9.091 19.159 1.215 1.333

 7:35:04 PM 1min avg: 16.352 8.684 18.444 1.656 1.778

 7:36:04 PM 1min avg: 12.335 6.749 18.873 1.364 1.928

 7:37:04 PM 1min avg: 20.670 12.322 18.504 1.657 1.581

 7:38:04 PM 1min avg: 20.689 6.668 18.695 1.466 1.276

 7:38:05 PM Test Avgs: 15.719 8.405 18.854 1.397 1.725

86
Run P3L-1b Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P3L-1b 

Start: 11/21/2013 8:54:00 AM

End: 11/21/2013 9:25:34 AM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 9:06:33 AM 1min avg: 12.902 4.475 19.426 1.082 0.356

 9:07:33 AM 1min avg: 11.889 3.823 19.030 1.290 0.230

 9:08:33 AM 1min avg: 12.375 5.129 18.720 1.469 0.151

 9:09:33 AM 1min avg: 13.655 4.330 19.021 1.278 0.065

 9:10:33 AM 1min avg: 15.460 5.542 18.697 1.519 0.093

 9:11:33 AM 1min avg: 9.998 3.877 19.272 1.110 0.032

 9:12:33 AM 1min avg: 10.066 3.587 19.410 1.027 0.036

 9:13:33 AM 1min avg: 11.001 3.290 19.396 1.045 0.097

 9:14:33 AM 1min avg: 10.136 3.732 19.405 1.030 0.144

 9:15:33 AM 1min avg: 11.647 4.127 19.106 1.196 0.074

 9:16:33 AM 1min avg: 11.126 4.492 19.040 1.262 0.101

 9:17:33 AM 1min avg: 12.875 4.502 19.202 1.167 0.131

 9:18:33 AM 1min avg: 11.329 4.749 18.996 1.290 0.141

 9:19:33 AM 1min avg: 15.443 5.421 18.457 1.636 0.203

 9:20:33 AM 1min avg: 18.514 6.593 18.410 1.701 0.117

 9:21:33 AM 1min avg: 12.625 4.489 19.333 1.087 0.026

 9:22:33 AM 1min avg: 11.950 4.663 18.701 1.494 0.274

 9:23:33 AM 1min avg: 13.590 5.213 18.779 1.448 0.067

 9:24:33 AM 1min avg: 17.403 5.822 18.495 1.620 0.611

 9:25:33 AM 1min avg: 16.621 8.381 18.288 1.787 0.246

 9:25:34 AM Test Avgs: 13.035 4.814 18.959 1.327 0.160

87
Run P1L-2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P1L-2 

Start: 11/21/2013 9:44:00 AM

End: 11/21/2013 10:04:01 AM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 9:45:00 AM 1min avg: 10.088 1.853 19.370 1.276 -0.235

 9:46:00 AM 1min avg: 6.870 1.490 19.011 1.474 -0.264

 9:47:00 AM 1min avg: 8.103 1.619 19.558 1.098 -0.212

 9:48:00 AM 1min avg: 8.860 1.369 19.648 1.042 -0.214

 9:49:00 AM 1min avg: 4.134 0.794 20.279 0.607 -0.185

 9:50:00 AM 1min avg: 3.405 0.581 20.342 0.569 -0.266

 9:51:00 AM 1min avg: 4.986 0.717 20.003 0.797 -0.245

 9:52:00 AM 1min avg: 6.457 0.857 20.208 0.664 -0.285

 9:53:00 AM 1min avg: 2.166 0.343 20.635 0.354 -0.305

 9:54:00 AM 1min avg: 5.375 1.128 19.460 1.129 -0.426

 9:55:00 AM 1min avg: 9.259 1.576 19.285 1.296 -0.398

 9:56:00 AM 1min avg: 11.910 1.594 19.102 1.415 -0.440

 9:57:00 AM 1min avg: 13.263 2.269 18.439 1.946 -0.462

 9:58:00 AM 1min avg: 11.216 1.851 18.485 1.855 -0.523

 9:59:00 AM 1min avg: 12.355 2.007 18.862 1.636 -0.510

10:00:00 AM 1min avg: 10.855 1.718 18.681 1.744 -0.499

10:01:00 AM 1min avg: 15.099 2.022 18.242 2.099 -0.550

10:02:00 AM 1min avg: 13.069 2.196 18.675 1.735 -0.617

10:03:00 AM 1min avg: 15.007 2.121 18.358 1.988 -0.521

10:04:00 AM 1min avg: 14.630 2.322 17.759 2.393 -0.557

10:04:01 AM Test Avgs: 9.355 1.522 19.220 1.356 -0.386

88
Run P2H-2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P2H-2 

Start: 11/21/2013 10:56:00 AM

End: 11/21/2013 11:16:00 AM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

10:57:00 AM 1min avg: 7.539 2.260 19.774 0.849 0.257

10:58:00 AM 1min avg: 11.631 2.000 19.634 0.917 0.204

10:59:00 AM 1min avg: 11.981 1.842 19.489 1.002 0.294

11:00:00 AM 1min avg: 9.945 2.041 19.546 0.976 0.225

11:01:00 AM 1min avg: 13.263 2.345 19.299 1.180 0.193

11:02:00 AM 1min avg: 9.138 1.099 20.118 0.681 0.241

11:03:00 AM 1min avg: 15.092 1.440 19.519 1.042 0.257

11:04:00 AM 1min avg: 10.703 1.465 19.799 0.871 0.279

11:05:00 AM 1min avg: 11.612 1.566 19.790 0.889 0.282

11:06:00 AM 1min avg: 8.880 1.979 19.849 0.837 0.196

11:07:00 AM 1min avg: 11.352 0.771 19.894 0.827 0.192

11:08:00 AM 1min avg: 12.638 1.331 19.619 1.018 0.311

11:09:00 AM 1min avg: 5.917 0.454 20.774 0.272 0.382

11:10:00 AM 1min avg: 11.658 4.025 19.550 1.015 0.516

11:11:00 AM 1min avg: 11.626 4.701 19.721 0.919 0.476

11:12:00 AM 1min avg: 12.309 6.286 19.459 1.070 0.498

11:13:00 AM 1min avg: 10.282 3.353 19.950 0.783 0.420

11:14:00 AM 1min avg: 10.166 4.339 19.722 0.919 0.912

11:15:00 AM 1min avg: 11.169 3.621 19.901 0.833 0.884

11:16:00 AM 1min avg: 7.897 2.799 19.638 0.988 0.784

11:16:00 AM Test Avgs: 10.740 2.486 19.752 0.894 0.390

89
Run P2L-2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P2L-2 

Start: 11/21/2013 11:31:03 AM

End: 11/21/2013 11:51:03 AM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

11:32:03 AM 1min avg: 3.203 2.600 20.805 0.244 1.203

11:33:03 AM 1min avg: 1.247 0.605 20.803 0.235 1.218

11:34:03 AM 1min avg: 1.567 1.025 20.732 0.276 1.269

11:35:03 AM 1min avg: 5.304 3.088 20.153 0.636 1.398

11:36:03 AM 1min avg: 7.177 6.341 19.965 0.744 1.477

11:37:03 AM 1min avg: 5.384 3.919 20.384 0.515 1.105

11:38:03 AM 1min avg: 8.789 4.639 19.398 1.118 1.200

11:39:03 AM 1min avg: 13.575 5.667 19.979 0.780 2.846

11:40:03 AM 1min avg: 10.448 11.449 19.175 1.262 2.234

11:41:03 AM 1min avg: 15.761 10.361 19.390 1.128 2.809

11:42:03 AM 1min avg: 16.209 11.235 19.324 1.199 1.941

11:43:03 AM 1min avg: 15.921 4.683 20.055 0.729 1.218

11:44:03 AM 1min avg: 7.163 4.558 19.332 1.169 1.389

11:45:03 AM 1min avg: 16.654 10.027 19.352 1.172 2.049

11:46:03 AM 1min avg: 11.194 9.708 19.929 0.809 1.163

11:47:03 AM 1min avg: 6.317 6.150 20.013 0.724 1.819

11:48:03 AM 1min avg: 9.274 8.629 19.807 0.863 1.497

11:49:03 AM 1min avg: 14.876 8.474 19.221 1.240 3.319

11:50:03 AM 1min avg: 9.241 12.055 19.641 0.957 2.436

11:51:03 AM 1min avg: 11.091 12.569 19.533 1.063 3.149

11:51:03 AM Test Avgs: 9.520 6.889 19.850 0.843 1.837

90
Run P3H-2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P3H-2 

Start: 11/21/2013 12:45:01 PM

End: 11/21/2013 1:05:02 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

12:46:01 PM 1min avg: 7.354 2.896 19.828 0.789 1.171

12:47:01 PM 1min avg: 6.795 2.571 20.061 0.667 1.051

12:48:01 PM 1min avg: 8.850 3.062 19.446 1.003 1.090

12:49:01 PM 1min avg: 10.528 3.874 19.356 1.094 1.076

12:50:01 PM 1min avg: 6.764 3.255 19.997 0.710 1.126

12:51:01 PM 1min avg: 5.668 3.376 20.134 0.650 1.156

12:52:01 PM 1min avg: 5.768 2.909 19.630 0.894 1.205

12:53:01 PM 1min avg: 12.075 4.100 19.123 1.214 1.205

12:54:01 PM 1min avg: 8.029 3.832 19.673 0.897 1.199

12:55:01 PM 1min avg: 8.697 3.780 19.575 0.939 1.173

12:56:01 PM 1min avg: 11.629 4.045 18.860 1.412 1.103

12:57:01 PM 1min avg: 14.725 4.086 19.608 0.966 1.147

12:58:01 PM 1min avg: 6.188 2.219 19.617 0.937 1.214

12:59:01 PM 1min avg: 10.179 3.036 20.230 0.566 1.177

 1:00:01 PM 1min avg: 5.245 2.437 19.992 0.706 1.385

 1:01:01 PM 1min avg: 4.580 2.644 20.252 0.541 1.288

 1:02:01 PM 1min avg: 6.246 2.999 19.997 0.730 1.377

 1:03:01 PM 1min avg: 9.647 2.711 19.860 0.783 1.242

 1:04:01 PM 1min avg: 6.564 3.012 19.436 0.988 1.342

 1:05:01 PM 1min avg: 13.439 4.026 19.273 1.190 1.364

 1:05:02 PM Test Avgs: 8.448 3.244 19.697 0.884 1.204

91
Run P3L-2 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P3L-2 

Start: 11/21/2013 1:16:57 PM

End: 11/21/2013 1:36:57 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 1:17:56 PM 1min avg: 10.370 3.872 19.183 1.173 0.858

 1:18:56 PM 1min avg: 9.858 3.216 19.827 0.810 0.932

 1:19:56 PM 1min avg: 4.198 1.504 20.151 0.593 0.896

 1:20:56 PM 1min avg: 7.434 2.423 19.424 1.008 0.870

 1:21:56 PM 1min avg: 8.350 1.730 20.295 0.541 0.924

 1:22:56 PM 1min avg: 1.126 0.236 20.948 0.118 0.905

 1:23:56 PM 1min avg: 3.097 0.466 20.363 0.484 0.952

 1:24:56 PM 1min avg: 7.367 1.738 19.551 0.948 1.108

 1:25:56 PM 1min avg: 14.838 5.761 18.108 1.861 1.458

 1:26:56 PM 1min avg: 20.400 9.881 18.034 1.946 1.614

 1:27:56 PM 1min avg: 14.176 7.813 18.737 1.465 1.238

 1:28:56 PM 1min avg: 12.187 6.405 19.143 1.205 1.324

 1:29:56 PM 1min avg: 5.358 2.182 20.672 0.316 1.004

 1:30:56 PM 1min avg: 3.869 1.549 20.008 0.674 1.148

 1:31:56 PM 1min avg: 4.889 2.147 20.660 0.322 1.045

 1:32:56 PM 1min avg: 0.680 0.299 20.863 0.180 1.106

 1:33:56 PM 1min avg: 5.720 1.593 19.168 1.184 0.971

 1:34:56 PM 1min avg: 11.352 2.525 19.558 0.965 1.111

 1:35:56 PM 1min avg: 14.846 4.118 18.079 1.884 1.268

 1:36:56 PM 1min avg: 22.108 8.037 17.697 2.164 1.161

 1:36:57 PM Test Avgs: 9.119 3.377 19.523 0.992 1.095

92
Run P1H-3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P1H-3 

Start: 11/21/2013 1:48:07 PM

End: 11/21/2013 2:08:08 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 1:49:07 PM 1min avg: 8.015 0.963 18.737 1.659 0.900

 1:50:07 PM 1min avg: 17.713 1.575 17.867 2.338 0.913

 1:51:07 PM 1min avg: 18.562 1.322 18.405 1.910 0.881

 1:52:07 PM 1min avg: 16.961 1.373 18.600 1.815 0.963

 1:53:07 PM 1min avg: 15.375 1.165 17.738 2.403 0.915

 1:54:07 PM 1min avg: 11.775 0.780 19.975 0.818 0.925

 1:55:07 PM 1min avg: 14.869 1.205 18.133 2.142 0.819

 1:56:07 PM 1min avg: 9.490 0.674 20.199 0.684 0.923

 1:57:07 PM 1min avg: 4.513 0.345 20.285 0.546 0.759

 1:58:07 PM 1min avg: 12.799 0.853 18.777 1.616 0.780

 1:59:07 PM 1min avg: 15.837 1.074 18.340 2.023 0.752

 2:00:07 PM 1min avg: 13.487 0.917 19.078 1.446 0.814

 2:01:07 PM 1min avg: 12.060 0.948 19.116 1.444 0.909

 2:02:07 PM 1min avg: 4.976 0.341 20.600 0.371 0.896

 2:03:07 PM 1min avg: 6.441 0.559 20.200 0.659 0.992

 2:04:07 PM 1min avg: 0.905 0.145 20.920 0.156 0.985

 2:05:07 PM 1min avg: 2.067 0.329 20.398 0.523 0.839

 2:06:07 PM 1min avg: 7.410 0.611 19.728 0.957 0.718

 2:07:07 PM 1min avg: 9.396 0.876 19.099 1.380 0.637

 2:08:07 PM 1min avg: 17.000 1.520 18.647 1.775 0.708

 2:08:08 PM Test Avgs: 10.989 0.879 19.242 1.333 0.851

93
Run P2L-3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P2L-3 

Start: 11/21/2013 2:38:00 PM

End: 11/21/2013 2:58:01 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 2:39:00 PM 1min avg: 18.320 6.338 19.585 1.074 0.511

 2:40:00 PM 1min avg: 9.637 2.385 19.783 0.875 0.751

 2:41:00 PM 1min avg: 12.875 4.824 19.032 1.336 0.845

 2:42:00 PM 1min avg: 17.104 8.382 18.984 1.389 1.802

 2:43:00 PM 1min avg: 18.278 11.824 19.195 1.240 1.317

 2:44:00 PM 1min avg: 9.694 4.652 19.986 0.766 0.762

 2:45:00 PM 1min avg: 8.866 3.823 19.927 0.775 1.490

 2:46:00 PM 1min avg: 13.800 8.692 19.256 1.201 1.255

 2:47:00 PM 1min avg: 15.343 6.672 19.879 0.822 0.882

 2:48:00 PM 1min avg: 7.167 2.475 20.016 0.720 0.640

 2:49:00 PM 1min avg: 10.474 4.447 19.667 0.959 1.119

 2:50:00 PM 1min avg: 15.062 8.628 19.289 1.161 2.162

 2:51:00 PM 1min avg: 11.601 8.205 20.144 0.694 0.523

 2:52:00 PM 1min avg: 5.733 2.537 19.918 0.752 0.773

 2:53:00 PM 1min avg: 13.189 6.728 19.167 1.297 0.733

 2:54:00 PM 1min avg: 17.962 10.860 19.114 1.290 1.423

 2:55:00 PM 1min avg: 13.554 12.342 19.464 1.132 1.545

 2:56:00 PM 1min avg: 17.921 10.414 18.679 1.589 0.943

 2:57:00 PM 1min avg: 20.312 8.787 18.865 1.490 0.756

 2:58:00 PM 1min avg: 13.538 5.085 19.182 1.263 0.984

 2:58:01 PM Test Avgs: 13.522 6.904 19.456 1.092 1.062

94
Run P3L-3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P3L-3 

Start: 11/21/2013 3:06:01 PM

End: 11/21/2013 3:26:02 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 3:07:01 PM 1min avg: 7.268 1.236 20.319 0.476 0.893

 3:08:01 PM 1min avg: 6.267 1.954 19.427 1.075 1.002

 3:09:01 PM 1min avg: 9.833 3.247 19.315 1.079 0.977

 3:10:01 PM 1min avg: 15.586 5.372 18.801 1.446 1.227

 3:11:01 PM 1min avg: 16.881 8.334 18.108 1.908 0.866

 3:12:01 PM 1min avg: 15.196 3.765 18.825 1.418 1.043

 3:13:01 PM 1min avg: 15.151 6.758 18.249 1.843 1.311

 3:14:01 PM 1min avg: 10.233 5.358 19.449 1.033 1.370

 3:15:01 PM 1min avg: 12.032 8.922 18.989 1.329 1.413

 3:16:01 PM 1min avg: 13.794 9.376 18.221 1.794 1.588

 3:17:01 PM 1min avg: 13.388 10.646 18.989 1.344 1.037

 3:18:01 PM 1min avg: 10.148 5.731 19.114 1.282 1.523

 3:19:01 PM 1min avg: 10.194 6.222 19.527 1.004 0.919

 3:20:01 PM 1min avg: 13.576 4.979 19.011 1.334 1.432

 3:21:01 PM 1min avg: 9.540 6.572 19.171 1.238 1.466

 3:22:01 PM 1min avg: 14.092 5.642 19.048 1.270 2.256

 3:23:01 PM 1min avg: 19.058 16.557 17.893 2.065 1.250

 3:24:01 PM 1min avg: 19.162 7.481 18.382 1.729 0.915

 3:25:01 PM 1min avg: 13.790 4.859 19.081 1.288 1.628

 3:26:01 PM 1min avg: 16.451 8.210 18.824 1.475 1.249

 3:26:02 PM Test Avgs: 13.082 6.561 18.937 1.372 1.268

95
Run P3H-3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P3H-3 

Start: 11/21/2013 3:34:02 PM

End: 11/21/2013 3:54:02 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 3:35:01 PM 1min avg: 11.387 6.863 19.415 1.060 1.689

 3:36:01 PM 1min avg: 11.674 7.171 19.328 1.091 1.633

 3:37:01 PM 1min avg: 12.097 7.991 19.235 1.147 1.647

 3:38:01 PM 1min avg: 11.723 7.627 19.326 1.133 1.909

 3:39:01 PM 1min avg: 11.316 7.703 19.569 0.956 1.503

 3:40:01 PM 1min avg: 11.317 6.963 19.314 1.096 1.849

 3:41:01 PM 1min avg: 12.671 8.102 19.528 1.021 2.098

 3:42:01 PM 1min avg: 10.751 7.714 19.406 1.042 1.607

 3:43:01 PM 1min avg: 11.252 6.738 19.523 0.996 1.675

 3:44:01 PM 1min avg: 11.607 7.654 19.080 1.228 1.822

 3:45:01 PM 1min avg: 10.749 9.851 19.378 1.100 2.164

 3:46:01 PM 1min avg: 6.921 7.409 19.788 0.846 1.862

 3:47:01 PM 1min avg: 7.189 8.301 19.678 0.934 2.286

 3:48:01 PM 1min avg: 8.054 8.504 19.732 0.848 2.135

 3:49:01 PM 1min avg: 11.012 10.314 19.194 1.197 2.402

 3:50:01 PM 1min avg: 9.957 9.449 19.678 0.923 2.156

 3:51:01 PM 1min avg: 9.678 7.697 19.399 1.054 1.749

 3:52:01 PM 1min avg: 12.721 7.614 19.042 1.276 1.972

 3:53:01 PM 1min avg: 13.527 10.184 18.874 1.400 2.247

 3:54:01 PM 1min avg: 11.814 10.717 19.217 1.158 1.895

 3:54:02 PM Test Avgs: 10.871 8.228 19.385 1.075 1.916

96
Run P2H-3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P2H-3 

Start: 11/21/2013 4:01:59 PM

End: 11/21/2013 4:22:01 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 4:02:59 PM 1min avg: 14.030 5.408 19.199 1.252 1.061

 4:03:59 PM 1min avg: 13.723 5.490 19.165 1.278 0.997

 4:04:59 PM 1min avg: 12.308 4.811 19.596 1.016 1.166

 4:05:59 PM 1min avg: 14.175 5.979 19.414 1.083 1.141

 4:06:59 PM 1min avg: 12.079 5.279 19.471 1.074 1.067

 4:07:59 PM 1min avg: 12.538 5.488 19.281 1.215 0.969

 4:08:59 PM 1min avg: 17.069 5.547 19.193 1.274 1.023

 4:09:59 PM 1min avg: 11.362 4.645 19.655 0.981 1.068

 4:10:59 PM 1min avg: 12.474 6.257 19.599 0.980 1.196

 4:11:59 PM 1min avg: 11.067 5.010 20.013 0.777 0.934

 4:12:59 PM 1min avg: 10.764 4.017 19.903 0.812 0.946

 4:13:59 PM 1min avg: 11.253 4.952 19.537 1.046 1.019

 4:14:59 PM 1min avg: 11.936 5.580 19.556 1.021 1.019

 4:15:59 PM 1min avg: 12.249 4.834 19.670 0.967 0.875

 4:16:59 PM 1min avg: 11.557 3.296 19.320 1.176 0.927

 4:17:59 PM 1min avg: 15.324 5.206 19.698 1.006 0.893

 4:18:59 PM 1min avg: 11.476 4.747 19.424 1.094 0.921

 4:19:59 PM 1min avg: 12.274 4.725 19.378 1.154 0.781

 4:20:59 PM 1min avg: 10.799 3.528 20.178 0.684 0.678

 4:21:59 PM 1min avg: 2.337 0.818 20.683 0.332 0.649

 4:22:01 PM Test Avgs: 12.040 4.781 19.597 1.011 0.967

97
Run P1L-3 Datalog Records

Testing by TRC, Austin, Texas

199009 November 21 

Run P1L-3 

Start: 11/21/2013 4:32:02 PM

End: 11/21/2013 4:52:03 PM

 

Operator: JPB 

Plant: John Zink 

Location: Tulsa, OK 

Source ID: Dow Flare Test

 

 NOx CO O2 CO2 C3H8-Propy

 Time Entry ppm ppm % % ppm

 4:33:01 PM 1min avg: 10.135 1.493 19.226 1.336 0.436

 4:34:01 PM 1min avg: 8.216 1.176 19.335 1.356 0.446

 4:35:01 PM 1min avg: 6.073 0.754 19.841 0.900 0.470

 4:36:01 PM 1min avg: 6.743 1.150 19.956 0.875 0.498

 4:37:01 PM 1min avg: 7.500 0.698 19.793 0.968 0.503

 4:38:01 PM 1min avg: 3.797 0.430 20.754 0.332 0.521

 4:39:01 PM 1min avg: 3.714 1.055 19.915 0.880 0.492

 4:40:01 PM 1min avg: 3.966 0.602 20.572 0.461 0.491

 4:41:01 PM 1min avg: 1.060 0.267 20.845 0.237 0.483

 4:42:01 PM 1min avg: 3.307 0.876 20.392 0.561 0.410

 4:43:01 PM 1min avg: 6.514 1.249 19.294 1.308 0.437

 4:44:01 PM 1min avg: 7.698 1.761 19.765 1.066 0.476

 4:45:01 PM 1min avg: 4.311 1.775 19.576 1.091 0.504

 4:46:01 PM 1min avg: 6.745 1.584 19.970 0.909 0.481

 4:47:01 PM 1min avg: 6.754 0.866 20.082 0.767 0.418

 4:48:01 PM 1min avg: 8.462 1.296 19.656 1.097 0.456

 4:49:01 PM 1min avg: 3.406 0.886 20.551 0.480 0.514

 4:50:01 PM 1min avg: 5.451 0.884 19.764 0.965 0.443

 4:51:01 PM 1min avg: 6.056 1.034 19.931 0.892 0.482

 4:52:01 PM 1min avg: 7.264 1.373 19.883 0.919 0.391

 4:52:03 PM Test Avgs: 5.861 1.061 19.955 0.870 0.468

98
Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

Channel_A_02.ASC 11/18/2013 10:39:44 Methane 1.553 3343 Ethane 1.7 14292 Propylene 0 0

Channel_A_03.ASC 11/18/2013 10:45:03 Methane 1.546 1693 Ethane 1.693 6554 Propylene 0 0

Channel_A_04.ASC 11/18/2013 11:00:40 Methane 0 0 Ethane 0 0 Propylene 1.99 945152

Channel_A_05.ASC 11/18/2013 11:08:02 Methane 0 0 Ethane 0 0 Propylene 1.986 975455

Channel_A_06.ASC 11/18/2013 11:15:19 Methane 0 0 Ethane 0 0 Propylene 1.983 990708

Channel_A_07.ASC 11/18/2013 11:24:14 Methane 0 0 Ethane 0 0 Propylene 1.996 600029

Channel_A_08.ASC 11/18/2013 11:30:22 Methane 0 0 Ethane 0 0 Propylene 1.993 568286

Channel_A_09.ASC 11/18/2013 11:38:31 Methane 0 0 Ethane 0 0 Propylene 1.993 571236

Channel_A_10.ASC 11/18/2013 11:45:03 Methane 0 0 Ethane 0 0 Propylene 1.998 336432

Channel_A_11.ASC 11/18/2013 11:48:21 Methane 0 0 Ethane 0 0 Propylene 2.001 333042

Channel_A_12.ASC 11/18/2013 11:51:37 Methane 0 0 Ethane 0 0 Propylene 1.998 331664

Channel_A_13.ASC 11/18/2013 12:56:13 Methane 1.526 365922 Ethane 1.675 7955 Propylene 2.008 15086

Channel_A_14.ASC 11/18/2013 13:00:56 Methane 1.523 372545 Ethane 1.673 8130 Propylene 2.006 5352

Channel_A_15.ASC 11/18/2013 13:05:22 Methane 1.523 375843 Ethane 1.673 8241 Propylene 2.006 1988

Cal 50 C1 10 C2 A_16.ASC 11/18/2013 13:12:48 Methane 1.526 209749 Ethane 1.673 78550 Propylene 2.006 656

Cal 50 C1 10 C2 A_17.ASC 11/18/2013 13:17:23 Methane 1.525 205188 Ethane 1.671 80708 Propylene 0 0

Cal 50 C1 10 C2 A_18.ASC 11/18/2013 13:21:16 Methane 1.525 204191 Ethane 1.671 81667 Propylene 0 0

Cal 20 C1 20 C2 A_19.ASC 11/18/2013 13:27:58 Methane 1.526 83857 Ethane 1.67 162602 Propylene 0 0

Cal 20 C1 20 C2 A_20.ASC 11/18/2013 13:31:52 Methane 1.528 83836 Ethane 1.671 162688 Propylene 0 0

Cal 20 C1 20 C2 A_21.ASC 11/18/2013 13:34:46 Methane 1.528 84026 Ethane 1.671 163179 Propylene 0 0

Cal 5 C1 5 C2 A_22.ASC 11/18/2013 13:39:35 Methane 1.526 21445 Ethane 1.673 42137 Propylene 0 0

Cal 5 C1 5 C2 A_23.ASC 11/18/2013 13:42:08 Methane 1.528 21477 Ethane 1.673 42186 Propylene 0 0

Cal 5 C1 5 C2 A_24.ASC 11/18/2013 13:45:53 Methane 1.526 21547 Ethane 1.671 42174 Propylene 0 0

Channel_A_25.ASC 11/18/2013 15:35:45 Methane 1.53 22803 Ethane 1.675 44469 Propylene 2.006 1563

Cal 85.02 C3= A_26.ASC 11/19/2013 6:51:40 Methane 0 0 Ethane 0 0 Propylene 1.965 1097273

Cal 85.02 C3= A_27.ASC 11/19/2013 7:05:04 Methane 0 0 Ethane 0 0 Propylene 1.963 1144216

Cal 85.02 C3= A_28.ASC 11/19/2013 7:13:11 Methane 0 0 Ethane 0 0 Propylene 1.963 1138793

Cal 50 C3= A_29.ASC 11/19/2013 7:21:34 Methane 0 0 Ethane 0 0 Propylene 1.975 656152

Cal 50 C3= A_30.ASC 11/19/2013 7:25:38 Methane 0 0 Ethane 0 0 Propylene 1.975 647915

Cal 50 C3= A_31.ASC 11/19/2013 7:29:26 Methane 0 0 Ethane 0 0 Propylene 1.975 646843

Cal 30 C3= A_32.ASC 11/19/2013 7:35:37 Methane 0 0 Ethane 0 0 Propylene 1.983 394904

Cal 30 C3= A_33.ASC 11/19/2013 7:41:29 Methane 0 0 Ethane 0 0 Propylene 1.985 378900

Cal 30 C3= A_34.ASC 11/19/2013 7:46:46 Methane 0 0 Ethane 0 0 Propylene 1.985 377435

Channel_A_35.ASC 11/19/2013 7:56:09 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_A_36.ASC 11/19/2013 8:03:32 Methane 1.52 206661 Ethane 1.665 83279 Propylene 1.998 4493

Channel_A_37.ASC 11/19/2013 8:32:02 Methane 1.528 6542 Ethane 1.673 796 Propylene 2.005 813

Channel_A_38.ASC 11/19/2013 8:35:16 Methane 1.523 2167 Ethane 1.668 527 Propylene 1.97 780636

Channel_A_39.ASC 11/19/2013 8:39:03 Methane 1.525 744 Ethane 0 0 Propylene 1.97 843356

Channel_A_40.ASC 11/19/2013 8:42:28 Methane 1.521 12377 Ethane 1.666 3339 Propylene 1.97 757075

Channel_A_41.ASC 11/19/2013 8:47:46 Methane 0 0 Ethane 0 0 Propylene 1.975 676952

Channel_A_42.ASC 11/19/2013 9:00:52 Methane 1.523 1731 Ethane 0 0 Propylene 1.97 795008

S1 A_43.ASC 11/19/2013 9:08:14 Methane 0 0 Ethane 0 0 Propylene 1.976 641940

S1 A_44.ASC 11/19/2013 9:15:01 Methane 0 0 Ethane 0 0 Propylene 1.978 607371

S1 A_45.ASC 11/19/2013 9:20:01 Methane 0 0 Ethane 0 0 Propylene 1.975 636470

S1 A_46.ASC 11/19/2013 9:25:01 Methane 0 0 Ethane 0 0 Propylene 1.976 579908

S1 A_47.ASC 11/19/2013 9:30:01 Methane 0 0 Ethane 0 0 Propylene 1.975 637004

S2 A_48.ASC 11/19/2013 9:45:08 Methane 0 0 Ethane 0 0 Propylene 1.976 647849

S2 A_49.ASC 11/19/2013 9:50:08 Methane 0 0 Ethane 0 0 Propylene 1.976 629863

S2 A_50.ASC 11/19/2013 9:55:08 Methane 0 0 Ethane 0 0 Propylene 1.976 600996

S2 A_51.ASC 11/19/2013 10:00:08 Methane 0 0 Ethane 0 0 Propylene 1.975 616391

Channel_A_52.ASC 11/19/2013 10:09:28 Methane 0 0 Ethane 0 0 Propylene 2.001 11810

Channel_A_53.ASC 11/19/2013 10:13:32 Methane 0 0 Ethane 0 0 Propylene 1.998 17394

Channel_A_54.ASC 11/19/2013 10:20:27 Methane 0 0 Ethane 0 0 Propylene 2.003 20168

Channel_A_55.ASC 11/19/2013 10:24:56 Methane 0 0 Ethane 0 0 Propylene 2.003 20207

Channel_A_56.ASC 11/19/2013 10:42:24 Methane 0 0 Ethane 0 0 Propylene 1.988 347031

99
Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

Channel_A_57.ASC 11/19/2013 10:46:06 Methane 0 0 Ethane 0 0 Propylene 1.99 252965

Channel_A_58.ASC 11/19/2013 10:55:21 Methane 0 0 Ethane 0 0 Propylene 2 76618

Channel_A_59.ASC 11/19/2013 11:12:34 Methane 0 0 Ethane 0 0 Propylene 1.99 300631

Channel_A_60.ASC 11/19/2013 11:17:26 Methane 0 0 Ethane 0 0 Propylene 1.988 307103

S3 A_61.ASC 11/19/2013 11:29:01 Methane 0 0 Ethane 0 0 Propylene 1.988 336318

S3 A_62.ASC 11/19/2013 11:34:01 Methane 0 0 Ethane 0 0 Propylene 1.985 328695

Channel_A_63.ASC 11/19/2013 11:39:01 Methane 0 0 Ethane 0 0 Propylene 2.003 5236

S3 A_64.ASC 11/19/2013 11:44:01 Methane 0 0 Ethane 0 0 Propylene 1.986 362085

S3 A_65.ASC 11/19/2013 11:50:05 Methane 0 0 Ethane 0 0 Propylene 1.985 351404

Channel_A_66.ASC 11/19/2013 11:55:27 Methane 0 0 Ethane 0 0 Propylene 1.985 383370

Channel_A_67.ASC 11/19/2013 11:58:52 Methane 0 0 Ethane 0 0 Propylene 1.981 384498

Channel_A_68.ASC 11/19/2013 12:04:04 Methane 0 0 Ethane 0 0 Propylene 1.986 367968

Channel_A_69.ASC 11/19/2013 12:45:51 Methane 0 0 Ethane 0 0 Propylene 1.986 362478

Channel_A_70.ASC 11/19/2013 12:49:54 Methane 0 0 Ethane 0 0 Propylene 1.985 364459

Channel_A_71.ASC 11/19/2013 12:57:06 Methane 0 0 Ethane 0 0 Propylene 1.983 508555

S4 A_72.ASC 11/19/2013 13:36:06 Methane 0 0 Ethane 0 0 Propylene 1.985 422309

S4 A_73.ASC 11/19/2013 13:41:06 Methane 0 0 Ethane 0 0 Propylene 1.983 431030

S4 A_74.ASC 11/19/2013 13:46:06 Methane 0 0 Ethane 0 0 Propylene 1.983 434189

S4 A_75.ASC 11/19/2013 13:51:06 Methane 0 0 Ethane 0 0 Propylene 1.983 424148

S5 A_76.ASC 11/19/2013 14:18:51 Methane 0 0 Ethane 0 0 Propylene 1.986 374314

S5 A_77.ASC 11/19/2013 14:23:51 Methane 0 0 Ethane 0 0 Propylene 1.985 373703

S5 A_78.ASC 11/19/2013 14:28:51 Methane 0 0 Ethane 0 0 Propylene 1.983 389657

S5 A_79.ASC 11/19/2013 14:33:51 Methane 0 0 Ethane 0 0 Propylene 1.983 404682

S6 A_80.ASC 11/19/2013 14:56:04 Methane 0 0 Ethane 0 0 Propylene 1.955 1306487

S6 A_81.ASC 11/19/2013 15:01:04 Methane 0 0 Ethane 0 0 Propylene 1.956 1304866

S6 A_82.ASC 11/19/2013 15:06:04 Methane 0 0 Ethane 0 0 Propylene 1.956 1305717

S6 A_83.ASC 11/19/2013 15:11:04 Methane 0 0 Ethane 0 0 Propylene 1.955 1306852

Channel_A_84.ASC 11/19/2013 15:21:12 Methane 0 0 Ethane 0 0 Propylene 1.981 372255

Channel_A_85.ASC 11/19/2013 15:24:42 Methane 0 0 Ethane 0 0 Propylene 1.985 375799

Channel_A_86.ASC 11/19/2013 15:27:43 Methane 0 0 Ethane 0 0 Propylene 1.961 1072314

Channel_A_87.ASC 11/19/2013 15:31:02 Methane 0 0 Ethane 0 0 Propylene 1.961 1089138

Channel_A_88.ASC 11/19/2013 15:34:09 Methane 0 0 Ethane 0 0 Propylene 1.961 1092651

Channel_A_89.ASC 11/19/2013 15:38:14 Methane 0 0 Ethane 0 0 Propylene 1.975 637828

Channel_A_90.ASC 11/19/2013 15:41:12 Methane 0 0 Ethane 0 0 Propylene 1.973 631517

Channel_A_91.ASC 11/19/2013 15:45:08 Methane 0 0 Ethane 0 0 Propylene 0 0

P1H-1 A_92.ASC 11/19/2013 15:50:08 Methane 0 0 Ethane 0 0 Propylene 1.955 1317397

P1H-1 A_93.ASC 11/19/2013 15:55:08 Methane 0 0 Ethane 0 0 Propylene 1.956 1337434

P1H-1 A_94.ASC 11/19/2013 16:00:08 Methane 0 0 Ethane 0 0 Propylene 1.956 1325391

Channel_A_95.ASC 11/19/2013 16:10:57 Methane 0 0 Ethane 0 0 Propylene 1.956 1288955

Channel_A_96.ASC 11/19/2013 16:14:33 Methane 0 0 Ethane 0 0 Propylene 1.96 1029914

Channel_A_97.ASC 11/19/2013 16:20:07 Methane 0 0 Ethane 0 0 Propylene 1.971 745639

Cal 50 C3= A_98.ASC 11/19/2013 16:23:39 Methane 0 0 Ethane 0 0 Propylene 1.975 625401

Cal 50 C3= A_99.ASC 11/20/2013 10:59:25 Methane 0 0 Ethane 0 0 Propylene 1.976 602221

Cal 50 C3= _100.ASC 11/20/2013 11:04:12 Methane 0 0 Ethane 0 0 Propylene 1.973 608316

Cal 50 C1 10 C2 _101.ASC 11/20/2013 13:46:27 Methane 1.521 195417 Ethane 1.666 78720 Propylene 2 4269

P1H-2 _102.ASC 11/20/2013 14:09:11 Methane 1.523 2510 Ethane 1.668 823 Propylene 1.958 1260048

P1H-2 _103.ASC 11/20/2013 14:14:11 Methane 0 0 Ethane 0 0 Propylene 1.955 1295417

P1H-2 _104.ASC 11/20/2013 14:19:11 Methane 0 0 Ethane 0 0 Propylene 1.953 1304635

P1H-2 _105.ASC 11/20/2013 14:24:11 Methane 0 0 Ethane 0 0 Propylene 1.955 1317226

P1L-1 _106.ASC 11/20/2013 14:57:11 Methane 0 0 Ethane 0 0 Propylene 1.956 1306952

P1L-1 _107.ASC 11/20/2013 15:02:11 Methane 0 0 Ethane 0 0 Propylene 1.956 1303504

P1L-1 _108.ASC 11/20/2013 15:07:11 Methane 0 0 Ethane 0 0 Propylene 1.953 1303764

P1L-1 _109.ASC 11/20/2013 15:12:11 Methane 0 0 Ethane 0 0 Propylene 1.955 1303151

Channel_A_110.ASC 11/20/2013 15:21:30 Methane 0 0 Ethane 0 0 Propylene 1.953 1296992

Channel_A_112.ASC 11/20/2013 15:30:29 Methane 0 0 Ethane 0 0 Propylene 1.97 684422

100
Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

Channel_A_113.ASC 11/20/2013 15:34:17 Methane 0 0 Ethane 0 0 Propylene 1.996 48999

P2H-1 _114.ASC 11/20/2013 16:01:23 Methane 0 0 Ethane 0 0 Propylene 1.981 469186

P2H-1 _115.ASC 11/20/2013 16:06:23 Methane 0 0 Ethane 0 0 Propylene 1.978 442584

P2H-1b _116.ASC 11/20/2013 16:37:10 Methane 0 0 Ethane 0 0 Propylene 1.981 452209

P2H-1b _117.ASC 11/20/2013 16:42:10 Methane 0 0 Ethane 0 0 Propylene 1.978 471370

P2H-1b _118.ASC 11/20/2013 16:47:10 Methane 0 0 Ethane 0 0 Propylene 1.978 478287

P2H-1b _119.ASC 11/20/2013 16:52:10 Methane 0 0 Ethane 0 0 Propylene 1.976 484779

P2L-1 _120.ASC 11/20/2013 17:23:01 Methane 0 0 Ethane 0 0 Propylene 1.985 397546

Channel_A_121.ASC 11/20/2013 17:28:01 Methane 0 0 Ethane 0 0 Propylene 2.001 26727

Channel_A_122.ASC 11/20/2013 17:33:01 Methane 0 0 Ethane 0 0 Propylene 1.981 392530

P2L-1b _123.ASC 11/20/2013 17:38:01 Methane 0 0 Ethane 0 0 Propylene 1.98 426879

P2L-1b _124.ASC 11/20/2013 17:53:38 Methane 0 0 Ethane 0 0 Propylene 1.98 428086

Channel_A_125.ASC 11/20/2013 18:36:18 Methane 0 0 Ethane 0 0 Propylene 1.998 67721

Channel_A_126.ASC 11/20/2013 18:38:58 Methane 0 0 Ethane 0 0 Propylene 1.996 67860

Channel_A_127.ASC 11/20/2013 18:42:17 Methane 0 0 Ethane 0 0 Propylene 2 72491

Channel_A_128.ASC 11/20/2013 18:45:02 Methane 0 0 Ethane 0 0 Propylene 1.991 72509

Channel_A_129.ASC 11/20/2013 18:56:10 Methane 1.526 105040 Ethane 1.671 9734 Propylene 1.988 329807

P3H-1 _130.ASC 11/20/2013 19:18:09 Methane 1.52 95223 Ethane 1.666 8805 Propylene 1.983 303502

P3H-1 _131.ASC 11/20/2013 19:23:09 Methane 1.523 95020 Ethane 1.67 8884 Propylene 1.986 279466

P3H-1 _132.ASC 11/20/2013 19:28:09 Methane 1.523 94398 Ethane 1.67 8714 Propylene 1.986 287825

P3H-1 _133.ASC 11/20/2013 19:33:09 Methane 1.523 95747 Ethane 1.67 8620 Propylene 1.986 284975

Cal 50 C3= _134.ASC 11/20/2013 19:38:04 Methane 1.523 2963 Ethane 0 0 Propylene 1.973 609278

Cal 50 C3= _135.ASC 11/20/2013 19:44:33 Methane 1.523 1165 Ethane 0 0 Propylene 1.973 615466

Cal 50 C3= _136.ASC 11/20/2013 19:47:31 Methane 1.523 504 Ethane 0 0 Propylene 1.973 616195

Cal 50 C1 10 C2 _137.ASC 11/21/2013 6:51:41 Methane 1.525 197433 Ethane 1.67 79420 Propylene 2.003 909

Cal 50 C1 10 C2 _138.ASC 11/21/2013 6:59:48 Methane 1.523 201679 Ethane 1.668 81107 Propylene 0 0

Cal 50 C1 10 C2 _139.ASC 11/21/2013 7:10:29 Methane 1.523 203513 Ethane 1.668 81963 Propylene 0 0

Cal 50 C1 10 C2 _140.ASC 11/21/2013 7:31:01 Methane 1.523 202060 Ethane 1.668 81236 Propylene 2.001 10191

Cal 50 C3= _141.ASC 11/21/2013 7:50:04 Methane 1.525 4120 Ethane 1.67 1908 Propylene 1.975 609757

Cal 50 C3= _142.ASC 11/21/2013 7:58:59 Methane 1.525 1347 Ethane 1.67 819 Propylene 1.975 603811

Cal 50 C3= _143.ASC 11/21/2013 8:05:23 Methane 1.525 521 Ethane 0 0 Propylene 1.975 606974

Channel_A_144.ASC 11/21/2013 8:40:44 Methane 1.525 99176 Ethane 1.671 9245 Propylene 1.986 321258

P3L-1 _145.ASC 11/21/2013 8:54:04 Methane 1.523 90433 Ethane 1.668 7810 Propylene 1.986 273998

Channel_A_146.ASC 11/21/2013 8:59:04 Methane 1.523 53194 Ethane 1.668 4522 Propylene 1.978 499965

P3L-1b _147.ASC 11/21/2013 9:06:08 Methane 1.523 97802 Ethane 1.67 8285 Propylene 1.988 284379

P3L-1b _148.ASC 11/21/2013 9:11:08 Methane 1.525 97009 Ethane 1.67 8284 Propylene 1.986 282050

P3L-1b _149.ASC 11/21/2013 9:16:08 Methane 1.521 98492 Ethane 1.668 8608 Propylene 1.986 268555

P3L-1b _150.ASC 11/21/2013 9:21:08 Methane 1.523 98582 Ethane 1.668 8723 Propylene 1.986 263876

P1L-2 _151.ASC 11/21/2013 9:44:07 Methane 1.525 631 Ethane 0 0 Propylene 1.958 1305181

P1L-2 _152.ASC 11/21/2013 9:49:07 Methane 0 0 Ethane 0 0 Propylene 1.956 1306814

P1L-2 _153.ASC 11/21/2013 9:54:07 Methane 0 0 Ethane 0 0 Propylene 1.956 1310545

P1L-2 _154.ASC 11/21/2013 9:59:07 Methane 0 0 Ethane 0 0 Propylene 1.955 1295583

Channel_A_155.ASC 11/21/2013 10:08:03 Methane 0 0 Ethane 0 0 Propylene 1.958 1302294

Channel_A_156.ASC 11/21/2013 10:11:20 Methane 0 0 Ethane 0 0 Propylene 1.955 1268399

Channel_A_157.ASC 11/21/2013 10:14:55 Methane 0 0 Ethane 0 0 Propylene 1.961 1075557

Channel_A_158.ASC 11/21/2013 10:17:52 Methane 0 0 Ethane 0 0 Propylene 1.961 1012210

P2H-2 _159.ASC 11/21/2013 10:56:05 Methane 0 0 Ethane 0 0 Propylene 1.981 477967

P2H-2 _160.ASC 11/21/2013 11:13:55 Methane 0 0 Ethane 0 0 Propylene 1.981 485970

P2L-2 _161.ASC 11/21/2013 11:31:04 Methane 0 0 Ethane 0 0 Propylene 1.981 439275

P2L-2 _162.ASC 11/21/2013 11:36:04 Methane 0 0 Ethane 0 0 Propylene 1.981 439170

P2L-2 _163.ASC 11/21/2013 11:41:04 Methane 0 0 Ethane 0 0 Propylene 1.981 436590

P2L-2 _164.ASC 11/21/2013 11:46:04 Methane 0 0 Ethane 0 0 Propylene 1.98 437812

Channel_A_165.ASC 11/21/2013 12:31:52 Methane 0 0 Ethane 0 0 Propylene 2.003 15489

Channel_A_166.ASC 11/21/2013 12:34:28 Methane 0 0 Ethane 0 0 Propylene 2.001 16596

Channel_A_167.ASC 11/21/2013 12:37:09 Methane 0 0 Ethane 0 0 Propylene 0 0

101
Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

Channel_A_168.ASC 11/21/2013 12:40:17 Methane 1.525 100752 Ethane 1.67 9135 Propylene 1.983 383721

P3H-2 _169.ASC 11/21/2013 12:45:10 Methane 1.525 95453 Ethane 1.67 8555 Propylene 1.986 297094

P3H-2 _170.ASC 11/21/2013 12:50:10 Methane 1.523 95974 Ethane 1.668 8657 Propylene 1.986 279987

P3H-2 _171.ASC 11/21/2013 12:55:10 Methane 1.525 96925 Ethane 1.67 8720 Propylene 1.988 281531

P3H-2 _172.ASC 11/21/2013 13:00:10 Methane 1.52 96532 Ethane 1.666 8656 Propylene 1.983 283868

P3L-2 _173.ASC 11/21/2013 13:17:09 Methane 1.525 99061 Ethane 1.671 8784 Propylene 1.988 276091

P3L-2 _174.ASC 11/21/2013 13:22:09 Methane 1.525 96952 Ethane 1.67 8602 Propylene 1.988 285361

P3L-2 _175.ASC 11/21/2013 13:27:09 Methane 1.523 97440 Ethane 1.668 8698 Propylene 1.986 264834

P3L-2 _176.ASC 11/21/2013 13:32:09 Methane 1.525 96108 Ethane 1.67 8523 Propylene 1.988 286640

P1H-3 _177.ASC 11/21/2013 13:48:09 Methane 1.523 1690 Ethane 0 0 Propylene 1.958 1297699

P1H-3 _178.ASC 11/21/2013 13:53:09 Methane 0 0 Ethane 0 0 Propylene 1.956 1319434

P1H-3 _179.ASC 11/21/2013 13:58:09 Methane 0 0 Ethane 0 0 Propylene 1.956 1312146

P1H-3 _180.ASC 11/21/2013 14:03:09 Methane 0 0 Ethane 0 0 Propylene 1.956 1325167

Channel_A_181.ASC 11/21/2013 14:15:26 Methane 0 0 Ethane 0 0 Propylene 1.956 1269918

Channel_A_182.ASC 11/21/2013 14:17:59 Methane 0 0 Ethane 0 0 Propylene 1.958 1157644

Channel_A_183.ASC 11/21/2013 14:21:29 Methane 0 0 Ethane 0 0 Propylene 1.968 795263

Channel_A_184.ASC 11/21/2013 14:24:26 Methane 0 0 Ethane 0 0 Propylene 1.971 734415

P2L-3 _185.ASC 11/21/2013 14:38:09 Methane 0 0 Ethane 0 0 Propylene 1.981 455987

P2L-3 _186.ASC 11/21/2013 14:43:09 Methane 0 0 Ethane 0 0 Propylene 1.983 435496

P2L-3 _187.ASC 11/21/2013 14:48:09 Methane 0 0 Ethane 0 0 Propylene 1.981 431441

P2L-3 _188.ASC 11/21/2013 14:53:09 Methane 0 0 Ethane 0 0 Propylene 1.983 432839

P3L-3 _189.ASC 11/21/2013 15:06:08 Methane 1.526 96334 Ethane 1.671 8265 Propylene 1.988 297097

P3L-3 _190.ASC 11/21/2013 15:11:08 Methane 1.525 97601 Ethane 1.671 8431 Propylene 1.988 291414

P3L-3 _191.ASC 11/21/2013 15:16:08 Methane 1.525 97865 Ethane 1.67 8522 Propylene 1.988 291210

P3L-3 _192.ASC 11/21/2013 15:21:08 Methane 1.523 98078 Ethane 1.668 8415 Propylene 1.986 292218

P3H-3 _193.ASC 11/21/2013 15:34:14 Methane 1.525 98044 Ethane 1.671 8302 Propylene 1.988 298488

P3H-3 _194.ASC 11/21/2013 15:39:14 Methane 1.525 98008 Ethane 1.67 8369 Propylene 1.988 289776

P3H-3 _195.ASC 11/21/2013 15:44:14 Methane 1.523 97708 Ethane 1.668 8345 Propylene 1.986 287892

P3H-3 _196.ASC 11/21/2013 15:49:14 Methane 1.525 97792 Ethane 1.671 8258 Propylene 1.988 288208

P2H-3 _197.ASC 11/21/2013 16:02:04 Methane 1.526 3171 Ethane 0 0 Propylene 1.981 471065

P2H-3 _198.ASC 11/21/2013 16:07:04 Methane 1.525 688 Ethane 0 0 Propylene 1.98 470290

P2H-3 _199.ASC 11/21/2013 16:12:04 Methane 0 0 Ethane 0 0 Propylene 1.98 469491

P2H-3 _200.ASC 11/21/2013 16:17:04 Methane 0 0 Ethane 0 0 Propylene 1.981 471437

P1L-3 _201.ASC 11/21/2013 16:32:15 Methane 0 0 Ethane 0 0 Propylene 1.955 1298181

P1L-3 _202.ASC 11/21/2013 16:37:15 Methane 0 0 Ethane 0 0 Propylene 1.956 1306426

P1L-3 _203.ASC 11/21/2013 16:42:15 Methane 0 0 Ethane 0 0 Propylene 1.956 1311460

P1L-3 _204.ASC 11/21/2013 16:47:15 Methane 0 0 Ethane 0 0 Propylene 1.956 1298736

Channel_A_205.ASC 11/21/2013 16:55:46 Methane 0 0 Ethane 0 0 Propylene 1.956 1308056

Channel_A_206.ASC 11/21/2013 16:58:41 Methane 0 0 Ethane 0 0 Propylene 1.973 635118

Channel_A_207.ASC 11/21/2013 17:01:37 Methane 0 0 Ethane 0 0 Propylene 1.975 618627

Channel_A_208.ASC 11/21/2013 17:04:15 Methane 0 0 Ethane 0 0 Propylene 1.973 626028

Cal 50 C1 10 C2 _209.ASC 11/21/2013 17:08:32 Methane 1.523 194335 Ethane 1.668 78046 Propylene 0 0

Cal 50 C1 10 C2 _210.ASC 11/21/2013 17:11:35 Methane 1.521 200019 Ethane 1.668 80605 Propylene 2 11982

Cal 50 C1 10 C2 _211.ASC 11/21/2013 17:17:08 Methane 1.523 203009 Ethane 1.668 81775 Propylene 2.001 4638

Cal 20 C1 20 C2 _212.ASC 11/21/2013 17:20:40 Methane 1.525 84100 Ethane 1.666 161968 Propylene 0 0

Cal 50 C1 10 C2 _213.ASC 11/22/2013 7:32:45 Methane 1.521 201041 Ethane 1.666 80921 Propylene 1.998 682

Cal 50 C1 10 C2 _214.ASC 11/22/2013 7:41:37 Methane 1.52 206082 Ethane 1.665 82801 Propylene 0 0

Cal 50 C1 10 C2 _215.ASC 11/22/2013 7:47:30 Methane 1.518 207320 Ethane 1.661 83365 Propylene 0 0

Channel_A_216.ASC 11/22/2013 8:06:04 Methane 1.523 650 Ethane 0 0 Propylene 2.005 9703

Channel_A_217.ASC 11/22/2013 8:40:28 Methane 1.525 609 Ethane 0 0 Propylene 2.008 9488

Channel_A_218.ASC 11/22/2013 9:46:18 Methane 1.526 6509 Ethane 1.67 1825 Propylene 1.996 144200

Channel_A_219.ASC 11/22/2013 9:51:18 Methane 1.518 375332 Ethane 1.666 35840 Propylene 2.008 4764

Channel_A_220.ASC 11/22/2013 9:56:18 Methane 1.518 375344 Ethane 1.666 35976 Propylene 2.008 4733

Channel_A_221.ASC 11/22/2013 10:01:18 Methane 1.516 340053 Ethane 1.665 32400 Propylene 2.005 4144

Channel_A_222.ASC 11/22/2013 10:06:18 Methane 1.518 374102 Ethane 1.665 35978 Propylene 2.006 4415

102
Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

P4 _223.ASC 11/22/2013 10:09:07 Methane 1.52 53788 Ethane 1.665 5064 Propylene 2.006 685

P4 _224.ASC 11/22/2013 10:13:18 Methane 1.52 36092 Ethane 1.666 3430 Propylene 0 0

P4 _225.ASC 11/22/2013 10:17:20 Methane 1.52 34737 Ethane 1.665 3285 Propylene 0 0

P4 _226.ASC 11/22/2013 10:21:06 Methane 1.52 34398 Ethane 1.665 3217 Propylene 0 0

Channel_A_227.ASC 11/22/2013 10:26:06 Methane 1.515 374730 Ethane 1.663 35554 Propylene 2.005 4534

Channel_A_228.ASC 11/22/2013 11:52:28 Methane 0 0 Ethane 0 0 Propylene 1.99 249929

Channel_A_229.ASC 11/22/2013 11:56:14 Methane 0 0 Ethane 0 0 Propylene 1.988 240364

Channel_A_230.ASC 11/22/2013 12:01:01 Methane 0 0 Ethane 0 0 Propylene 1.988 247619

Channel_A_231.ASC 11/22/2013 12:05:54 Methane 0 0 Ethane 0 0 Propylene 1.986 258306

Channel_A_232.ASC 11/22/2013 12:12:48 Methane 0 0 Ethane 0 0 Propylene 1.983 278691

Channel_A_233.ASC 11/22/2013 12:16:17 Methane 0 0 Ethane 0 0 Propylene 1.985 268062

Channel_A_234.ASC 11/22/2013 12:24:41 Methane 0 0 Ethane 0 0 Propylene 1.983 292581

Channel_A_235.ASC 11/22/2013 12:29:41 Methane 0 0 Ethane 0 0 Propylene 1.985 291816

Channel_A_236.ASC 11/22/2013 12:34:41 Methane 0 0 Ethane 0 0 Propylene 1.986 297517

Channel_A_237.ASC 11/22/2013 12:39:41 Methane 1.523 798 Ethane 0 0 Propylene 1.983 286981

Channel_A_238.ASC 11/22/2013 12:44:41 Methane 1.525 942 Ethane 0 0 Propylene 1.985 295147

Channel_A_239.ASC 11/22/2013 13:26:13 Methane 0 0 Ethane 0 0 Propylene 2 35989

Channel_A_240.ASC 11/22/2013 13:30:47 Methane 0 0 Ethane 0 0 Propylene 1.98 324605

Cal 50 C3= _241.ASC 11/22/2013 13:42:31 Methane 0 0 Ethane 0 0 Propylene 1.971 623425

Cal 50 C3= _242.ASC 11/22/2013 13:45:58 Methane 0 0 Ethane 0 0 Propylene 1.971 625038

Cal 50 C3= _243.ASC 11/22/2013 13:49:10 Methane 0 0 Ethane 0 0 Propylene 1.971 624181

Cal 50 C1 10 C2 _244.ASC 11/22/2013 13:53:32 Methane 1.518 196740 Ethane 1.663 79316 Propylene 1.995 27512

Cal 50 C1 10 C2 _245.ASC 11/22/2013 13:58:16 Methane 1.52 202737 Ethane 1.665 81620 Propylene 1.998 10306

Cal 50 C1 10 C2 _246.ASC 11/22/2013 14:04:50 Methane 1.52 205193 Ethane 1.665 82645 Propylene 1.996 3796

Cal 20 C1 20 C2 _247.ASC 11/22/2013 14:08:24 Methane 1.521 84887 Ethane 1.663 163626 Propylene 0 0

Cal 20 C1 20 C2 _248.ASC 11/22/2013 14:10:49 Methane 1.521 84956 Ethane 1.663 164204 Propylene 0 0

Cal 20 C1 20 C2 _249.ASC 11/22/2013 14:13:38 Methane 1.521 84800 Ethane 1.663 164174 Propylene 0 0

103
Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

Channel_B_03.ASC 11/18/2013 10:45:03 Methane 1.395 25038 Ethane 1.513 41264 Propylene 0 0

Channel_B_04.ASC 11/18/2013 11:00:40 Methane 1.398 25356 Ethane 1.515 41002 Propylene 0 0

Channel_B_05.ASC 11/18/2013 11:08:02 Methane 1.4 25648 Ethane 1.516 41568 Propylene 0 0

Channel_B_06.ASC 11/18/2013 11:15:19 Methane 1.398 25926 Ethane 1.515 41748 Propylene 0 0

Channel_B_07.ASC 11/18/2013 11:24:14 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_08.ASC 11/18/2013 11:30:22 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_09.ASC 11/18/2013 11:38:31 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_10.ASC 11/18/2013 11:45:03 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_11.ASC 11/18/2013 11:48:21 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_12.ASC 11/18/2013 11:51:37 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_13.ASC 11/18/2013 12:56:13 Methane 1.425 2769 Ethane 0 0 Propylene 1.773 63146

Channel_B_14.ASC 11/18/2013 13:00:56 Methane 1.423 1612 Ethane 0 0 Propylene 1.771 62849

Channel_B_15.ASC 11/18/2013 13:05:22 Methane 1.423 1742 Ethane 0 0 Propylene 1.771 62897

Channel_B_16.ASC 11/18/2013 13:12:48 Methane 1.421 1409 Ethane 0 0 Propylene 1.771 37335

Channel_B_17.ASC 11/18/2013 13:17:23 Methane 1.421 1278 Ethane 0 0 Propylene 1.77 37098

Channel_B_18.ASC 11/18/2013 13:21:16 Methane 1.421 1226 Ethane 0 0 Propylene 1.771 37145

Channel_B_19.ASC 11/18/2013 13:27:58 Methane 0 0 Ethane 0 0 Propylene 1.773 22632

Channel_B_20.ASC 11/18/2013 13:31:52 Methane 0 0 Ethane 0 0 Propylene 1.773 22565

Channel_B_21.ASC 11/18/2013 13:34:46 Methane 0 0 Ethane 0 0 Propylene 1.773 22552

Channel_B_22.ASC 11/18/2013 13:39:35 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_23.ASC 11/18/2013 13:42:08 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_24.ASC 11/18/2013 13:45:53 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_25.ASC 11/18/2013 15:35:45 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_26.ASC 11/19/2013 6:51:40 Methane 1.405 26745 Ethane 1.523 42316 Propylene 0 0

Channel_B_27.ASC 11/19/2013 7:05:04 Methane 1.408 27077 Ethane 1.525 43254 Propylene 0 0

Channel_B_28.ASC 11/19/2013 7:13:11 Methane 1.406 26514 Ethane 1.523 42866 Propylene 0 0

Channel_B_29.ASC 11/19/2013 7:21:34 Methane 0 0 Ethane 1.568 110687 Propylene 1.77 36574

Channel_B_30.ASC 11/19/2013 7:25:38 Methane 0 0 Ethane 0 0 Propylene 1.771 37038

Channel_B_31.ASC 11/19/2013 7:29:26 Methane 0 0 Ethane 0 0 Propylene 1.773 37014

Channel_B_32.ASC 11/19/2013 7:35:37 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_33.ASC 11/19/2013 7:41:29 Methane 0 0 Ethane 0 0 Propylene 1.803 30232

Channel_B_34.ASC 11/19/2013 7:46:46 Methane 1.416 1299 Ethane 0 0 Propylene 0 0

Channel_B_35.ASC 11/19/2013 7:56:09 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_36.ASC 11/19/2013 8:03:32 Methane 1.421 1034 Ethane 0 0 Propylene 0 0

Channel_B_37.ASC 11/19/2013 8:32:02 Methane 1.433 1346 Ethane 0 0 Propylene 0 0

Channel_B_38.ASC 11/19/2013 8:35:16 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_39.ASC 11/19/2013 8:39:03 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_40.ASC 11/19/2013 8:42:28 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_41.ASC 11/19/2013 8:47:46 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_42.ASC 11/19/2013 9:00:52 Methane 0 0 Ethane 0 0 Propylene 1.793 1499

S1 B_43.ASC 11/19/2013 9:08:14 Methane 0 0 Ethane 0 0 Propylene 1.795 1635

S1 B_44.ASC 11/19/2013 9:15:01 Methane 0 0 Ethane 0 0 Propylene 1.795 1404

S1 B_45.ASC 11/19/2013 9:20:01 Methane 0 0 Ethane 0 0 Propylene 0 0

S1 B_46.ASC 11/19/2013 9:25:01 Methane 0 0 Ethane 0 0 Propylene 1.791 1626

S1 B_47.ASC 11/19/2013 9:30:01 Methane 0 0 Ethane 0 0 Propylene 0 0

S2 B_48.ASC 11/19/2013 9:45:08 Methane 1.428 904 Ethane 0 0 Propylene 1.796 3184

S2 B_49.ASC 11/19/2013 9:50:08 Methane 0 0 Ethane 0 0 Propylene 1.75 825

S2 B_50.ASC 11/19/2013 9:55:08 Methane 1.425 675 Ethane 0 0 Propylene 1.795 832

S2 B_51.ASC 11/19/2013 10:00:08 Methane 0 0 Ethane 0 0 Propylene 1.791 850

S1 Bag B_52.ASC 11/19/2013 10:09:28 Methane 1.426 585 Ethane 0 0 Propylene 1.79 3009

S1 Bag B_53.ASC 11/19/2013 10:13:32 Methane 0 0 Ethane 0 0 Propylene 1.778 2506

S2 Bag B_54.ASC 11/19/2013 10:20:27 Methane 1.425 618 Ethane 0 0 Propylene 0 0

104
Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

S2 Bag B_55.ASC 11/19/2013 10:24:56 Methane 1.421 495 Ethane 0 0 Propylene 1.761 513

Channel_B_56.ASC 11/19/2013 10:42:24 Methane 0 0 Ethane 1.586 251 Propylene 0 0

Channel_B_57.ASC 11/19/2013 10:46:06 Methane 1.423 705 Ethane 1.565 263 Ethane 1.593 208

Channel_B_58.ASC 11/19/2013 10:55:21 Methane 1.423 803 Ethane 0 0 Propylene 0 0

Channel_B_59.ASC 11/19/2013 11:12:34 Methane 1.416 337 Ethane 1.545 498 Propylene 1.791 372

Channel_B_60.ASC 11/19/2013 11:17:26 Methane 1.425 821 Ethane 1.498 632 Propylene 1.781 1149

S3 B_61.ASC 11/19/2013 11:29:01 Methane 1.423 1147 Ethane 0 0 Propylene 1.773 3481

S3 B_62.ASC 11/19/2013 11:34:01 Methane 1.413 268 Ethane 1.505 484 Propylene 1.773 9757

Channel_B_63.ASC 11/19/2013 11:39:01 Methane 1.416 829 Ethane 0 0 Propylene 1.755 778

S3 B_64.ASC 11/19/2013 11:44:01 Methane 1.405 550 Ethane 1.506 212 Propylene 1.735 1233

S3 B_65.ASC 11/19/2013 11:50:05 Methane 1.408 581 Ethane 0 0 Propylene 1.771 8218

Channel_B_66.ASC 11/19/2013 11:55:27 Methane 1.411 650 Ethane 1.5 893 Propylene 1.771 5663

Channel_B_67.ASC 11/19/2013 11:58:52 Methane 1.418 1079 Ethane 1.493 1143 Propylene 1.765 9366

Channel_B_68.ASC 11/19/2013 12:04:04 Methane 1.391 684 Ethane 1.548 214 Propylene 1.793 309

Channel_B_69.ASC 11/19/2013 12:45:51 Methane 0 0 Ethane 1.498 798 Propylene 1.78 217

Channel_B_70.ASC 11/19/2013 12:49:54 Methane 1.41 698 Ethane 0 0 Propylene 1.778 211

Channel_B_71.ASC 11/19/2013 12:57:06 Methane 1.411 1378 Ethane 0 0 Propylene 1.77 1467

S4 B_72.ASC 11/19/2013 13:36:06 Methane 1.415 627 Ethane 0 0 Propylene 1.765 6391

S4 B_73.ASC 11/19/2013 13:41:06 Methane 1.41 783 Ethane 0 0 Propylene 1.761 5240

S4 B_74.ASC 11/19/2013 13:46:06 Methane 1.41 918 Ethane 0 0 Propylene 0 0

S4 B_75.ASC 11/19/2013 13:51:06 Methane 1.413 790 Ethane 0 0 Propylene 1.763 7911

S5 B_76.ASC 11/19/2013 14:18:51 Methane 1.408 844 Ethane 1.491 787 Propylene 1.763 18023

S5 B_77.ASC 11/19/2013 14:23:51 Methane 1.403 225 Ethane 1.491 233 Propylene 1.756 1845

S5 B_78.ASC 11/19/2013 14:28:51 Methane 1.405 320 Ethane 1.491 364 Propylene 1.76 11516

S5 B_79.ASC 11/19/2013 14:33:51 Methane 1.413 681 Ethane 0 0 Propylene 1.761 10105

S6 B_80.ASC 11/19/2013 14:56:04 Methane 1.41 350 Ethane 0 0 Propylene 1.773 440

S6 B_81.ASC 11/19/2013 15:01:04 Methane 1.413 745 Ethane 0 0 Propylene 1.731 954

S6 B_82.ASC 11/19/2013 15:06:04 Methane 1.405 746 Ethane 0 0 Propylene 0 0

S6 B_83.ASC 11/19/2013 15:11:04 Methane 1.415 827 Ethane 0 0 Propylene 1.733 591

Channel_B_84.ASC 11/19/2013 15:21:12 Methane 1.406 678 Ethane 0 0 Propylene 1.788 1614

S3 Bag B_85.ASC 11/19/2013 15:24:42 Methane 1.411 789 Ethane 1.535 231 Propylene 1.766 15810

S3 Bag B_86.ASC 11/19/2013 15:27:43 Methane 1.416 911 Ethane 1.495 366 Propylene 1.765 16278

S4 Bag B_87.ASC 11/19/2013 15:31:02 Methane 1.416 1225 Ethane 0 0 Propylene 1.765 3538

S4 Bag B_88.ASC 11/19/2013 15:34:09 Methane 0 0 Ethane 0 0 Propylene 1.768 3408

S5 Bag B_89.ASC 11/19/2013 15:38:14 Methane 1.406 848 Ethane 1.498 1022 Propylene 1.766 23525

S5 Bag B_90.ASC 11/19/2013 15:41:12 Methane 1.41 681 Ethane 1.498 1390 Propylene 1.766 24178

Channel_B_91.ASC 11/19/2013 15:45:08 Methane 0 0 Ethane 0 0 Propylene 0 0

P1H-1 B_92.ASC 11/19/2013 15:50:08 Methane 1.42 564 Ethane 0 0 Propylene 1.78 2299

P1H-1 B_93.ASC 11/19/2013 15:55:08 Methane 1.418 482 Ethane 1.525 263 Propylene 1.745 2754

P1H-1 B_94.ASC 11/19/2013 16:00:08 Methane 1.418 732 Ethane 0 0 Propylene 1.781 2249

S6 Bag B_95.ASC 11/19/2013 16:10:57 Methane 0 0 Ethane 0 0 Propylene 1.783 4317

S6 Bag B_96.ASC 11/19/2013 16:14:33 Methane 1.416 586 Ethane 0 0 Propylene 1.771 1559

P1H-1 Bag B_97.ASC 11/19/2013 16:20:07 Methane 1.418 572 Ethane 0 0 Propylene 1.766 1625

Channel_B_98.ASC 11/19/2013 16:23:39 Methane 1.423 718 Ethane 0 0 Propylene 1.776 1339

Channel_B_99.ASC 11/20/2013 10:59:25 Methane 1.41 26014 Ethane 1.526 41137 Propylene 0 0

Channel_B_100.ASC 11/20/2013 11:04:12 Methane 1.41 25544 Ethane 1.526 41609 Propylene 0 0

Channel_B_101.ASC 11/20/2013 13:46:27 Methane 1.431 1387 Ethane 1.543 764 Propylene 1.781 22833

P1H-2 _102.ASC 11/20/2013 14:09:11 Methane 1.426 742 Ethane 0 0 Propylene 1.798 1955

P1H-2 _103.ASC 11/20/2013 14:14:11 Methane 1.43 413 Ethane 0 0 Propylene 0 0

P1H-2 _104.ASC 11/20/2013 14:19:11 Methane 1.435 590 Ethane 0 0 Propylene 1.798 2297

P1H-2 _105.ASC 11/20/2013 14:24:11 Methane 1.438 749 Ethane 0 0 Propylene 0 0

P1L-1 _106.ASC 11/20/2013 14:57:11 Methane 1.426 747 Ethane 0 0 Propylene 0 0

105
Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

P1L-1 _107.ASC 11/20/2013 15:02:11 Methane 1.433 674 Ethane 0 0 Propylene 0 0

P1L-1 _108.ASC 11/20/2013 15:07:11 Methane 1.436 625 Ethane 0 0 Propylene 1.756 432

P1L-1 _109.ASC 11/20/2013 15:12:11 Methane 1.43 792 Ethane 0 0 Propylene 1.763 611

P1H-2 Bag _110.ASC 11/20/2013 15:21:30 Methane 1.436 797 Ethane 0 0 Propylene 0 0

P1L-1 Bag _112.ASC 11/20/2013 15:30:29 Methane 1.438 790 Ethane 0 0 Propylene 0 0

P1L-1 Bag _113.ASC 11/20/2013 15:34:17 Methane 1.433 763 Ethane 0 0 Propylene 0 0

P2H-1 _114.ASC 11/20/2013 16:01:23 Methane 1.43 755 Ethane 0 0 Propylene 1.763 5925

P2H-1 _115.ASC 11/20/2013 16:06:23 Methane 1.431 1129 Ethane 0 0 Propylene 1.786 490944

P2H-1b _116.ASC 11/20/2013 16:37:10 Methane 1.43 404 Ethane 0 0 Propylene 1.761 1446

P2H-1b _117.ASC 11/20/2013 16:42:10 Methane 1.436 590 Ethane 0 0 Propylene 1.765 1155

P2H-1b _118.ASC 11/20/2013 16:47:10 Methane 1.436 592 Ethane 0 0 Propylene 1.803 928

P2H-1b _119.ASC 11/20/2013 16:52:10 Methane 1.433 881 Ethane 0 0 Propylene 1.758 1305

P2L-1 _120.ASC 11/20/2013 17:23:01 Methane 1.436 236 Ethane 1.511 602 Propylene 1.796 5478

Channel_B_121.ASC 11/20/2013 17:28:01 Methane 1.43 726 Ethane 0 0 Propylene 1.793 1212

Channel_B_122.ASC 11/20/2013 17:33:01 Methane 1.431 710 Ethane 0 0 Propylene 1.791 1567

P2L-1b _123.ASC 11/20/2013 17:38:01 Methane 1.428 679 Ethane 0 0 Propylene 1.791 882

P2L-1b _124.ASC 11/20/2013 17:53:38 Methane 1.428 656 Ethane 0 0 Propylene 1.8 702

P2H-1b Bag _125.ASC 11/20/2013 18:36:18 Methane 1.426 723 Ethane 0 0 Propylene 1.795 529

P2H-1b Bag _126.ASC 11/20/2013 18:38:58 Methane 1.428 722 Ethane 0 0 Propylene 1.788 279

P2L-1b Bag _127.ASC 11/20/2013 18:42:17 Methane 1.438 703 Ethane 0 0 Propylene 1.795 743

P2L-1b Bag _128.ASC 11/20/2013 18:45:02 Methane 1.425 655 Ethane 0 0 Propylene 1.781 894

Channel_B_129.ASC 11/20/2013 18:56:10 Methane 0 0 Ethane 0 0 Propylene 1.806 1188

P3H-1 _130.ASC 11/20/2013 19:18:09 Methane 1.436 2710 Ethane 1.52 249 Propylene 1.801 4932

P3H-1 _131.ASC 11/20/2013 19:23:09 Methane 0 0 Ethane 0 0 Propylene 1.805 666

P3H-1 _132.ASC 11/20/2013 19:28:09 Methane 1.436 1342 Ethane 0 0 Propylene 1.805 586

P3H-1 _133.ASC 11/20/2013 19:33:09 Methane 0 0 Ethane 0 0 Propylene 1.806 530

Channel_B_134.ASC 11/20/2013 19:38:04 Methane 1.42 24883 Ethane 1.535 40325 Propylene 1.74 304

P3H-1 Bag _135.ASC 11/20/2013 19:44:33 Methane 1.425 1952 Ethane 1.54 1748 Propylene 1.745 751

P3H-1 Bag _136.ASC 11/20/2013 19:47:31 Methane 1.421 1198 Ethane 1.541 564 Propylene 1.746 3795

Channel_B_137.ASC 11/21/2013 6:51:41 Methane 1.421 25919 Ethane 1.54 40864 Propylene 0 0

Channel_B_138.ASC 11/21/2013 6:59:48 Methane 1.423 26483 Ethane 1.541 41663 Propylene 0 0

Channel_B_139.ASC 11/21/2013 7:10:29 Methane 1.42 3483 Ethane 1.526 9600 Propylene 0 0

Channel_B_140.ASC 11/21/2013 7:31:01 Methane 0 0 Ethane 1.558 740 Propylene 1.803 2206333

Channel_B_141.ASC 11/21/2013 7:50:04 Methane 0 0 Ethane 0 0 Propylene 1.798 547181

Channel_B_142.ASC 11/21/2013 7:58:59 Methane 0 0 Ethane 1.615 555 Propylene 1.795 27199

Channel_B_143.ASC 11/21/2013 8:05:23 Methane 0 0 Ethane 0 0 Propylene 1.795 10751

Channel_B_144.ASC 11/21/2013 8:40:44 Methane 1.438 1360 Ethane 0 0 Propylene 1.803 3799

Channel_B_145.ASC 11/21/2013 8:54:04 Methane 1.431 1620 Ethane 0 0 Propylene 1.801 1809

Channel_B_146.ASC 11/21/2013 8:59:04 Methane 1.435 894 Ethane 0 0 Propylene 1.79 875

P3L-1b _147.ASC 11/21/2013 9:06:08 Methane 0 0 Ethane 0 0 Propylene 1.803 1117

P3L-1b _148.ASC 11/21/2013 9:11:08 Methane 0 0 Ethane 0 0 Propylene 1.803 1291

P3L-1b _149.ASC 11/21/2013 9:16:08 Methane 1.438 1113 Ethane 0 0 Propylene 1.793 221

P3L-1b _150.ASC 11/21/2013 9:21:08 Methane 0 0 Ethane 0 0 Propylene 1.8 532

P1L-2 _151.ASC 11/21/2013 9:44:07 Methane 0 0 Ethane 0 0 Propylene 1.756 2914

P1L-2 _152.ASC 11/21/2013 9:49:07 Methane 1.436 1070 Ethane 0 0 Propylene 1.751 1290

P1L-2 _153.ASC 11/21/2013 9:54:07 Methane 0 0 Ethane 0 0 Propylene 1.761 1308

P1L-2 _154.ASC 11/21/2013 9:59:07 Methane 1.435 334 Ethane 0 0 Propylene 1.753 1343

P3L-1b Bag _155.ASC 11/21/2013 10:08:03 Methane 1.43 454 Ethane 0 0 Propylene 1.746 2128

P3L-1b Bag _156.ASC 11/21/2013 10:11:20 Methane 1.431 1127 Ethane 0 0 Propylene 1.741 1347

P1L-2 Bag _157.ASC 11/21/2013 10:14:55 Methane 1.433 793 Ethane 0 0 Propylene 1.743 1284

P1L-2 Bag _158.ASC 11/21/2013 10:17:52 Methane 1.431 797 Ethane 0 0 Propylene 1.741 1153

P2H-2 _159.ASC 11/21/2013 10:56:05 Methane 1.438 570 Ethane 0 0 Propylene 1.81 5046

106
Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

P2H-2 _160.ASC 11/21/2013 11:13:55 Methane 1.435 1313 Ethane 0 0 Propylene 0 0

P2L-2 _161.ASC 11/21/2013 11:31:04 Methane 1.431 1001 Ethane 0 0 Propylene 1.808 1038

P2L-2 _162.ASC 11/21/2013 11:36:04 Methane 0 0 Ethane 0 0 Propylene 1.808 834

P2L-2 _163.ASC 11/21/2013 11:41:04 Methane 1.433 773 Ethane 1.521 267 Propylene 1.796 2010

P2L-2 _164.ASC 11/21/2013 11:46:04 Methane 1.431 691 Ethane 0 0 Propylene 1.803 254

P2H-2 Bag _165.ASC 11/21/2013 12:31:52 Methane 1.436 678 Ethane 0 0 Propylene 1.808 541

P2H-2 Bag _166.ASC 11/21/2013 12:34:28 Methane 1.436 697 Ethane 0 0 Propylene 1.79 382

P2L-2 Bag _167.ASC 11/21/2013 12:37:09 Methane 1.438 704 Ethane 0 0 Propylene 1.793 1446

P2L-2 Bag _168.ASC 11/21/2013 12:40:17 Methane 1.436 857 Ethane 0 0 Propylene 1.796 1437

P3H-2 _169.ASC 11/21/2013 12:45:10 Methane 0 0 Ethane 0 0 Propylene 1.808 422

P3H-2 _170.ASC 11/21/2013 12:50:10 Methane 0 0 Ethane 0 0 Propylene 1.805 1082

P3H-2 _171.ASC 11/21/2013 12:55:10 Methane 0 0 Ethane 0 0 Propylene 1.806 1085

P3H-2 _172.ASC 11/21/2013 13:00:10 Methane 0 0 Ethane 0 0 Propylene 1.805 860

P3L-2 _173.ASC 11/21/2013 13:17:09 Methane 0 0 Ethane 0 0 Propylene 1.81 1202

P3L-2 _174.ASC 11/21/2013 13:22:09 Methane 1.438 1007 Ethane 0 0 Propylene 0 0

P3L-2 _175.ASC 11/21/2013 13:27:09 Methane 1.433 930 Ethane 0 0 Propylene 1.803 207

P3L-2 _176.ASC 11/21/2013 13:32:09 Methane 1.435 916 Ethane 0 0 Propylene 1.765 245

P1H-3 _177.ASC 11/21/2013 13:48:09 Methane 1.436 1180 Ethane 0 0 Propylene 1.76 3382

P1H-3 _178.ASC 11/21/2013 13:53:09 Methane 1.43 972 Ethane 0 0 Propylene 1.808 2333

P1H-3 _179.ASC 11/21/2013 13:58:09 Methane 1.436 825 Ethane 0 0 Propylene 1.761 285

P1H-3 _180.ASC 11/21/2013 14:03:09 Methane 1.436 1520 Ethane 0 0 Propylene 1.758 2602

P3H-2 Bag _181.ASC 11/21/2013 14:15:26 Methane 1.435 832 Ethane 0 0 Propylene 1.751 2904

P3H-2 Bag _182.ASC 11/21/2013 14:17:59 Methane 1.431 913 Ethane 0 0 Propylene 1.745 1150

P3L-2 Bag _183.ASC 11/21/2013 14:21:29 Methane 1.433 780 Ethane 0 0 Propylene 1.75 263

P3L-2 Bag _184.ASC 11/21/2013 14:24:26 Methane 1.433 766 Ethane 0 0 Propylene 0 0

P2L-3 _185.ASC 11/21/2013 14:38:09 Methane 1.438 687 Ethane 0 0 Propylene 1.808 1337

P2L-3 _186.ASC 11/21/2013 14:43:09 Methane 0 0 Ethane 0 0 Propylene 1.806 253

P2L-3 _187.ASC 11/21/2013 14:48:09 Methane 1.438 886 Ethane 0 0 Propylene 1.806 208

P2L-3 _188.ASC 11/21/2013 14:53:09 Methane 0 0 Ethane 0 0 Propylene 1.803 1353

P3L-3 _189.ASC 11/21/2013 15:06:08 Methane 0 0 Ethane 0 0 Propylene 1.811 543

P3L-3 _190.ASC 11/21/2013 15:11:08 Methane 0 0 Ethane 0 0 Propylene 1.805 385

P3L-3 _191.ASC 11/21/2013 15:16:08 Methane 0 0 Ethane 0 0 Propylene 1.811 247

P3L-3 _192.ASC 11/21/2013 15:21:08 Methane 0 0 Ethane 1.53 227 Propylene 1.803 202

P3H-3 _193.ASC 11/21/2013 15:34:14 Methane 0 0 Ethane 0 0 Propylene 1.811 2088

P3H-3 _194.ASC 11/21/2013 15:39:14 Methane 0 0 Ethane 0 0 Propylene 1.813 584

P3H-3 _195.ASC 11/21/2013 15:44:14 Methane 1.438 1649 Ethane 1.525 243 Propylene 1.806 2097

P3H-3 _196.ASC 11/21/2013 15:49:14 Methane 0 0 Ethane 0 0 Propylene 1.806 1961

P2H-3 _197.ASC 11/21/2013 16:02:04 Methane 0 0 Ethane 0 0 Propylene 1.81 1971

P2H-3 _198.ASC 11/21/2013 16:07:04 Methane 1.438 618 Ethane 0 0 Propylene 1.808 1188

P2H-3 _199.ASC 11/21/2013 16:12:04 Methane 1.435 911 Ethane 0 0 Propylene 1.745 1777

P2H-3 _200.ASC 11/21/2013 16:17:04 Methane 0 0 Ethane 0 0 Propylene 1.81 2039

P1L-3 _201.ASC 11/21/2013 16:32:15 Methane 1.433 1000 Ethane 0 0 Propylene 1.806 2517

P1L-3 _202.ASC 11/21/2013 16:37:15 Methane 0 0 Ethane 0 0 Propylene 1.81 1099

P1L-3 _203.ASC 11/21/2013 16:42:15 Methane 0 0 Ethane 0 0 Propylene 1.811 1297

P1L-3 _204.ASC 11/21/2013 16:47:15 Methane 0 0 Ethane 0 0 Propylene 1.813 1282

P2L-3 Bag _205.ASC 11/21/2013 16:55:46 Methane 0 0 Ethane 0 0 Propylene 1.808 1738

P2L-3 Bag _206.ASC 11/21/2013 16:58:41 Methane 1.431 591 Ethane 0 0 Propylene 1.791 771

P3L-3 Bag _207.ASC 11/21/2013 17:01:37 Methane 1.436 826 Ethane 0 0 Propylene 1.758 272

P3L-3 Bag _208.ASC 11/21/2013 17:04:15 Methane 1.43 795 Ethane 0 0 Propylene 1.761 418

P3H-3 Bag _209.ASC 11/21/2013 17:08:32 Methane 1.433 1192 Ethane 0 0 Propylene 1.735 3398

P3H-3 Bag _210.ASC 11/21/2013 17:11:35 Methane 1.436 1259 Ethane 0 0 Propylene 1.751 236

P1L-3 Bag _211.ASC 11/21/2013 17:17:08 Methane 0 0 Ethane 0 0 Propylene 0 0

107
Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas

Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area

P1L-3 Bag _212.ASC 11/21/2013 17:20:40 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_213.ASC 11/22/2013 7:32:45 Methane 0 0 Ethane 0 0 Propylene 1.831 21872

Channel_B_214.ASC 11/22/2013 7:41:37 Methane 0 0 Ethane 1.596 290 Propylene 1.833 21674

Channel_B_215.ASC 11/22/2013 7:47:30 Methane 0 0 Ethane 0 0 Propylene 1.83 21252

Channel_B_216.ASC 11/22/2013 8:06:04 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_217.ASC 11/22/2013 8:40:28 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_218.ASC 11/22/2013 9:46:18 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_219.ASC 11/22/2013 9:51:18 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_220.ASC 11/22/2013 9:56:18 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_221.ASC 11/22/2013 10:01:18 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_222.ASC 11/22/2013 10:06:18 Methane 0 0 Ethane 0 0 Propylene 0 0

P4 _223.ASC 11/22/2013 10:09:07 Methane 0 0 Ethane 0 0 Propylene 0 0

P4 _224.ASC 11/22/2013 10:13:18 Methane 0 0 Ethane 0 0 Propylene 0 0

P4 _225.ASC 11/22/2013 10:17:20 Methane 0 0 Ethane 0 0 Propylene 0 0

P4 _226.ASC 11/22/2013 10:21:06 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_227.ASC 11/22/2013 10:26:06 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_228.ASC 11/22/2013 11:52:28 Methane 1.436 1064 Ethane 0 0 Propylene 1.795 7809

Channel_B_229.ASC 11/22/2013 11:56:14 Methane 1.43 1584 Ethane 1.528 750 Propylene 1.793 364914

Channel_B_230.ASC 11/22/2013 12:01:01 Methane 0 0 Ethane 0 0 Propylene 1.805 813

Channel_B_231.ASC 11/22/2013 12:05:54 Methane 1.428 952 Ethane 0 0 Propylene 1.806 601

Channel_B_232.ASC 11/22/2013 12:12:48 Methane 1.428 885 Ethane 0 0 Propylene 0 0

Channel_B_233.ASC 11/22/2013 12:16:17 Methane 1.43 437 Ethane 0 0 Propylene 0 0

Channel_B_234.ASC 11/22/2013 12:24:41 Methane 1.438 1161 Ethane 0 0 Propylene 1.791 3110

Channel_B_235.ASC 11/22/2013 12:29:41 Methane 1.431 812 Ethane 0 0 Propylene 1.798 888

Channel_B_236.ASC 11/22/2013 12:34:41 Methane 0 0 Ethane 1.521 1083 Propylene 1.795 26140

Channel_B_237.ASC 11/22/2013 12:39:41 Methane 1.435 747 Ethane 0 0 Propylene 1.803 269

Channel_B_238.ASC 11/22/2013 12:44:41 Methane 1.436 1039 Ethane 1.523 704 Propylene 1.793 9421

Channel_B_239.ASC 11/22/2013 13:26:13 Methane 0 0 Ethane 1.516 897 Propylene 1.733 17048

Channel_B_240.ASC 11/22/2013 13:30:47 Methane 1.428 1125 Ethane 0 0 Propylene 1.79 17344

Channel_B_241.ASC 11/22/2013 13:42:31 Methane 0 0 Ethane 0 0 Propylene 1.793 22494

Channel_B_242.ASC 11/22/2013 13:45:58 Methane 0 0 Ethane 0 0 Propylene 1.793 22082

Channel_B_243.ASC 11/22/2013 13:49:10 Methane 1.431 305 Ethane 0 0 Propylene 1.795 21915

Channel_B_244.ASC 11/22/2013 13:53:32 Methane 0 0 Ethane 0 0 Propylene 1.821 61188

Channel_B_245.ASC 11/22/2013 13:58:16 Methane 0 0 Ethane 1.558 267 Propylene 0 0

Channel_B_246.ASC 11/22/2013 14:04:50 Methane 0 0 Ethane 1.565 215 Propylene 0 0

Channel_B_247.ASC 11/22/2013 14:08:24 Methane 1.438 271 Ethane 0 0 Propylene 0 0

Channel_B_248.ASC 11/22/2013 14:10:49 Methane 0 0 Ethane 0 0 Propylene 0 0

Channel_B_249.ASC 11/22/2013 14:13:38 Methane 0 0 Ethane 0 0 Propylene 0 0

108
Method 18 Inlet Fuel Initial Calibration

7HVWLQJE\75&$XVWLQ7H[DV

Compound

Low Level 

Calibration 

Value (%)

Low Level 

Injection 1 

(Area 

Counts)

Low Level 

Injection 2 

(Area 

Counts)

Low Level 

Injection 3 

(Area 

Counts)

Low Level 

Average 

(Area 

Counts)

Precision 

(Percent of 

Average)

Precision 

within 5%?

GC Run Number

 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6

Compound

Mid Level 

Calibration 

Value (%)

Mid Level 

Injection 1 

(Area 

Counts)

Mid Level 

Injection 2 

(Area 

Counts)

Mid Level 

Injection 3 

(Area 

Counts)

Mid Level 

Average 

(Area 

Counts)

Precision 

(Percent of 

Average)

Precision 

within 5%?

GC Run Number

 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6

Compound

High Level 

Calibration 

Value (%)

High Level 

Injection 1 

(Area 

Counts)

High Level 

Injection 2 

(Area 

Counts)

High Level 

Injection 3 

(Area 

Counts)

High Level 

Average 

(Area 

Counts)

Precision 

(Percent of 

Average)

Precision 

within 5%?

GC Run Number

 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6

109
Method 18 Inlet Fuel Curves

Initial Calibration Curve Final Calibration Curve (Combination of all Calibrations)

Compound Slope (m) R2 Compound Slope (m) R2

1 Methane 0.000242 0.999956 1 Methane 0.000242 0.999956

2 Ethane 0.000123 0.999971 2 Ethane 0.000123 0.999971

3 Propylene 0.000076 0.999866 3 Propylene 0.000076 0.999866

4 4

5 Methane 0.000242 0.999956 5 Methane 0.000242 0.999956

6 Ethane 0.000123 0.999971 6 Ethane 0.000123 0.999971

7 Propylene 0.000076 0.999866 7 Propylene 0.000076 0.999866

8 8

9 Methane 0.000242 0.999956 9 Methane 0.000242 0.999956

10 Ethane 0.000123 0.999971 10 Ethane 0.000123 0.999971

11 Propylene 0.000076 0.999866 11 Propylene 0.000076 0.999866

12 12

13 Methane 0.000242 0.999956 13 Methane 0.000242 0.999956

14 Ethane 0.000123 0.999971 14 Ethane 0.000123 0.999971

15 Propylene 0.000076 0.999866 15 Propylene 0.000076 0.999866

0

10

20

30

40

50

60

70

80

90

0.0 200000.0 400000.0 600000.0 800000.0 1000000.0 1200000.0

Concentrations (ppmv)

Area Counts

Calibration Curves

Methane

Ethane

Propylene

Methane

Ethane

Propylene

Methane

Ethane

Propylene

Methane

Ethane

Propylene

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Linear ()

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Linear ()

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Linear ()

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Testing by TRC, Austin, Texas

110
Method 18 Inlet Fuel Test Run Data

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

6 (WKDQH

3URS\OHQH        ,1,7,$/

0HWKDQH

6 (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

6 (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

6 (WKDQH

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

6 (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

6 (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

3+ (WKDQH

3URS\OHQH      ,1,7,$/

0HWKDQH

3+ (WKDQH

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

3/ (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

3+ (WKDQH

3URS\OHQH     ,1,7,$/

0HWKDQH

3+E (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

3/ (WKDQH

3URS\OHQH    ,1,7,$/

111
Method 18 Inlet Fuel Test Run Data (2)

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

3/E (WKDQH

3URS\OHQH     ,1,7,$/

0HWKDQH       ,1,7,$/

3+ (WKDQH       ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/E (WKDQH       ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH

3/ (WKDQH

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

3+ (WKDQH

3URS\OHQH     ,1,7,$/

0HWKDQH

3/ (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3+ (WKDQH       ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH       ,1,7,$/

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

3+ (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

3/ (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH       ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3+ (WKDQH       ,1,7,$/

3URS\OHQH       ,1,7,$/

112
Method 18 Inlet Fuel Test Run Data (3)

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(%)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH

3+ (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH

3/ (WKDQH

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3 (WKDQH       ,1,7,$/

3URS\OHQH

0HWKDQH

(WKDQH

3URS\OHQH

113
Method 18 Outlet Initial Calibration

7HVWLQJE\75&$XVWLQ7H[DV

Compound

Low Level 

Calibration 

Value 

(ppmv)

Low Level 

Injection 1 

(Area 

Counts)

Low Level 

Injection 2 

(Area 

Counts)

Low Level 

Injection 3 

(Area 

Counts)

Low Level 

Average 

(Area 

Counts)

Precision 

(Percent of 

Average)

Precision 

within 5%?

GC Run Number

 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6

Compound

Mid Level 

Calibration 

Value 

(ppmv)

Mid Level 

Injection 1 

(Area 

Counts)

Mid Level 

Injection 2 

(Area 

Counts)

Mid Level 

Injection 3 

(Area 

Counts)

Mid Level 

Average 

(Area 

Counts)

Precision 

(Percent of 

Average)

Precision 

within 5%?

GC Run Number

 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6

Compound

High Level 

Calibration 

Value 

(ppmv)

High Level 

Injection 1 

(Area 

Counts)

High Level 

Injection 2 

(Area 

Counts)

High Level 

Injection 3 

(Area 

Counts)

High Level 

Average 

(Area 

Counts)

Precision 

(Percent of 

Average)

Precision 

within 5%?

GC Run Number

 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6

114
Method 18 Outlet Curves

Initial Calibration Curve Final Calibration Curve (Combination of all Calibrations)

Compound Slope (m) R2 Compound Slope (m) R2

1 Methane 0.003739 0.999365 1 Methane 0.003739 0.999365

2 Ethane 0.002299 0.999820 2 Ethane 0.002299 0.999820

3 Propylene 0.001349 0.999999 3 Propylene 0.001349 0.999999

4 4

5 Methane 0.003739 0.999365 5 Methane 0.003739 0.999365

6 Ethane 0.002299 0.999820 6 Ethane 0.002299 0.999820

7 Propylene 0.001349 0.999999 7 Propylene 0.001349 0.999999

8 8

9 Methane 0.003739 0.999365 9 Methane 0.003739 0.999365

10 Ethane 0.002299 0.999820 10 Ethane 0.002299 0.999820

11 Propylene 0.001349 0.999999 11 Propylene 0.001349 0.999999

12 12

13 Methane 0.003739 0.999365 13 Methane 0.003739 0.999365

14 Ethane 0.002299 0.999820 14 Ethane 0.002299 0.999820

15 Propylene 0.001349 0.999999 15 Propylene 0.001349 0.999999

0

20

40

60

80

100

120

0.0 10000.0 20000.0 30000.0 40000.0 50000.0 60000.0 70000.0

Concentrations (ppmv)

Area Counts

Calibration Curves

Methane

Ethane

Propylene

Methane

Ethane

Propylene

Methane

Ethane

Propylene

Methane

Ethane

Propylene

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Linear ()

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Linear ()

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Linear ()

Linear (Methane)

Linear (Ethane)

Linear (Propylene)

Testing by TRC, Austin, Texas

115
Method 18 Outlet Test Run Data Direct

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH       ,1,7,$/

6 (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

6 (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

6 (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

6 (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH       ,1,7,$/

6 (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

6 (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH      ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH      ,1,7,$/

0HWKDQH       ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH       ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH     ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH    ,1,7,$/

0HWKDQH       ,1,7,$/

3+E (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH    ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH    ,1,7,$/

116
Method 18 Outlet Test Run Data Direct (2)

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH     ,1,7,$/

3/E (WKDQH     ,1,7,$/

3URS\OHQH     ,1,7,$/

0HWKDQH       ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/E (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH     ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH     ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH    ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH       ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH    ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

117
Method 18 Outlet Test Run Data Direct (3)

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Injection 3 

(Area Counts)

Injection 4 

(Area Counts)

Injection 5 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH       ,1,7,$/

3+ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/

3/ (WKDQH    ,1,7,$/

3URS\OHQH       ,1,7,$/

0HWKDQH

(WKDQH

3URS\OHQH

0HWKDQH

(WKDQH

3URS\OHQH

118
Method 18 Outlet Test Run Data Bag

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH     ,1,7,$/

6 (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

6 (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

6 (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

6 (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH 848 681   ,1,7,$/

6 (WKDQH    ,1,7,$/

%DJ 3URS\OHQH 23525 24178   ,1,7,$/

0HWKDQH 0 586   ,1,7,$/

6 (WKDQH    ,1,7,$/

%DJ 3URS\OHQH 4317 1559   ,1,7,$/

0HWKDQH 572    ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH 1625    ,1,7,$/

0HWKDQH    ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH    ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH 790 763   ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH 1071 344   ,1,7,$/

0HWKDQH N/A

3+ (WKDQH 1$

%DJ 3URS\OHQH N/A

0HWKDQH 723    ,1,7,$/

3+E (WKDQH    ,1,7,$/

%DJ 3URS\OHQH 529    ,1,7,$/

0HWKDQH 1$

3/ (WKDQH 1$

%DJ 3URS\OHQH 1$

119
Method 18 Outlet Test Run Data Bag (2)

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH     ,1,7,$/

3/E (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3/E (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH     ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH    ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH    ,1,7,$/

0HWKDQH     ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/

3+ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

120
Method 18 Outlet Test Run Data Bag (3)

7HVWLQJE\75&$XVWLQ7H[DV

Test Run 

Number:

Injection 1 

(Area Counts)

Injection 2 

(Area Counts)

Average Area 

Counts

Concentration 

(ppmv)

Curve Used 

(Initial or Final)

GC Run Number

0HWKDQH     ,1,7,$/

3+ (WKDQH     ,1,7,$/

%DJ 3URS\OHQH     ,1,7,$/

0HWKDQH    ,1,7,$/

3/ (WKDQH    ,1,7,$/

%DJ 3URS\OHQH    ,1,7,$/

0HWKDQH

(WKDQH

3URS\OHQH

0HWKDQH

(WKDQH

3URS\OHQH

121
Appendix E: 

Sample Gas Extraction Diagram



 

122
123
Appendix F: 

Calibration Certificates 

124
Customer Service Center

Manufacturing Location

Shipping Location

2550 KYLE CROSSING

mtgKYLE@matheson-trigas.com

1700 SCEPTER ROAD

2550 KYLE CROSSING

KYLE, TX 78640

WAVERLY, TN 37185

KYLE, TX 78640

P 512-262-2129

F 512-262-4011

CYLINDER NUMBER(S)

Product:

Grade:

Cylinder Size:

MTG Part No: Contents:

Pressure:

Valve:

Net:

To:

MTG Customer No:

Sales Order No:

Purchase Order No:

Certificate No:

111933

619978

52186

G2684058

CERTIFIED

Multi-Component Mixture 1R

CGA 350 BR

TRC AIR MEASUREMENTS

9225 US HWY 183 S

AUSTIN, TX 78747

140 ft3; 3.96 m3

2000 psig @ 70°F; 13891 kPa @ 21°C

255153

Certificate of Mixture Analysis

SX050102

Analysis Method

Certified

Accuracy

Blend

Units Tolerance

Certified

Concentration

Requested

Concentration 

Methane 5 5.01 ppm ±20% ±5%

Ethane 5 5.85 ppm ±20% ±5%

Propane 5 5.45 ppm ±20% ±5%

Butane 5 5.05 ppm ±20% ±5%

Pentane 5 5.12 ppm ±20% ±5%

Hexane 5 5.12 ppm ±20% ±5%

Nitrogen Balance Balance

TRACEABILITY

COMMENTS

PO# 52186

Lot No:

Fill Date:

Expiration Date:

Analysis Date:

9302604235

01/07/2013

01/07/2015

01/07/2013

Unless otherwise indicated, Matheson Tri-Gas terms and conditions govern the product data contained herein. This document was 

issued electronically and data validated by electronic signature. For further information visit www.matheson-trigas.com.

WenWen Zhang - Analyst Date Date

01/07/2013

Jeff Medlock - QA Approval

02/01/2013

Page 1 of 1

125
Customer Service Center

Manufacturing Location

Shipping Location

2550 KYLE CROSSING

mtgKYLE@matheson-trigas.com

1700 SCEPTER ROAD

2550 KYLE CROSSING

KYLE, TX 78640

WAVERLY, TN 37185

KYLE, TX 78640

P 512-262-2129

F 512-262-4011

CYLINDER NUMBER(S)

Product:

Grade:

Cylinder Size:

MTG Part No: Contents:

Pressure:

Valve:

Net:

To:

MTG Customer No:

Sales Order No:

Purchase Order No:

Certificate No:

111933

619978

52186

G2684059

CERTIFIED

Multi-Component Mixture 1R

CGA 350 BR

TRC AIR MEASUREMENTS

9225 US HWY 183 S

AUSTIN, TX 78747

140 ft3; 3.96 m3

2000 psig @ 70°F; 13891 kPa @ 21°C

252871

Certificate of Mixture Analysis

*SX041078

Analysis Method

Certified

Accuracy

Blend

Units Tolerance

Certified

Concentration

Requested

Concentration 

Methane 50 50.06 ppm ±10% ±2%

Ethane 50 46.58 ppm ±10% ±2%

Propane 50 53.34 ppm ±10% ±2%

Butane 50 47.58 ppm ±10% ±2%

Pentane 50 47.77 ppm ±10% ±2%

Hexane 50 46.52 ppm ±10% ±2%

Nitrogen Balance Balance

TRACEABILITY

* Indicates the actual 

cylinder(s) analyzed.

COMMENTS

PO# 52186

Lot No:

Fill Date:

Expiration Date:

Analysis Date:

9302604236

01/03/2013

01/04/2015

01/04/2013

Unless otherwise indicated, Matheson Tri-Gas terms and conditions govern the product data contained herein. This document was 

issued electronically and data validated by electronic signature. For further information visit www.matheson-trigas.com.

WenWen Zhang - Analyst Date Date

01/04/2013

Paula Gentry - QA Approval

01/11/2013

Page 1 of 1

126
Customer Service Center

Manufacturing Location

Shipping Location

2550 KYLE CROSSING

mtgKYLE@matheson-trigas.com

1700 SCEPTER ROAD

2550 KYLE CROSSING

KYLE, TX 78640

WAVERLY, TN 37185

KYLE, TX 78640

P 512-262-2129

F 512-262-4011

CYLINDER NUMBER(S)

Product:

Grade:

Cylinder Size:

MTG Part No: Contents:

Pressure:

Valve:

Net:

To:

MTG Customer No:

Sales Order No:

Purchase Order No:

Certificate No:

111933

619978

52186

G2684060

CERTIFIED

Multi-Component Mixture 1R

CGA 350 BR

TRC AIR MEASUREMENTS

9225 US HWY 183 S

AUSTIN, TX 78747

140 ft3; 3.96 m3

2000 psig @ 70°F; 13891 kPa @ 21°C

252872

Certificate of Mixture Analysis

*SX030921

Analysis Method

Certified

Accuracy

Blend

Units Tolerance

Certified

Concentration

Requested

Concentration 

Methane 100 100.6 ppm ±10% ±2%

Ethane 100 98.52 ppm ±10% ±2%

Propane 100 100.4 ppm ±10% ±2%

Butane 100 100.6 ppm ±10% ±2%

Pentane 100 100.9 ppm ±10% ±2%

Hexane 100 100.9 ppm ±10% ±2%

Nitrogen Balance Balance

TRACEABILITY

* Indicates the actual 

cylinder(s) analyzed.

COMMENTS

PO#52186

Lot No:

Fill Date:

Expiration Date:

Analysis Date:

9302604237

01/02/2013

01/03/2015

01/03/2013

Unless otherwise indicated, Matheson Tri-Gas terms and conditions govern the product data contained herein. This document was 

issued electronically and data validated by electronic signature. For further information visit www.matheson-trigas.com.

Ashley Ellis - Analyst Date Date

01/03/2013

Paula Gentry - QA Approval

01/11/2013

Page 1 of 1

127
Certification Date:

Expiration Date:

Cylinder Pressure: MFG Facility:

COA # Lot Number:

20.0%

19.6%

Nitrogen Balance

Type Component Expiration 

GMIS Oxygen 4/28/2013

GMIS Carbon Dioxide 11/3/2013

Z -0.0410 S 94.995 C 69.8040 Z 0.0090 S 72.715 C 69.8130

S 95.1050 C 69.949 Z -0.051 S 72.8230 C 69.943 Z 0.009

C 69.866 Z -0.0220 S 95.101 C 69.87 Z 0.0090 S 72.652

Assay Laboratory: Red Ball TGS

555 Craig Kennedy Way

Shreveport, LA 71107 

800-551-8150

EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS

Cylinder Number: EB0045768 1/30/2013

Product ID Number: 124240 1/30/2017

1900 PSIG RBTGS-Shreveport-LA

GC1301031102-0 GC1301031102

Customer PO. NO.: Tracking Number: 065123346

Customer Previous Certification Dates:

This calibration standard has been certified per the 1997 EPA Traceability Protocol, Document EPA-600/97/121, using procedure G1. All values certified 

to be +/-1% NIST Traceable.

Do Not Use This Cylinder Below 150 psig (1.0 Megapascal).

Certified Concentration(s)

Component Concentration Analytical Principle Accuracy

Oxygen Magnetic Pressure Analysis +/- 1% NIST

EB0010703 NTRM 071001

Carbon Dioxide Non Dispersive Infrared Absorptiometry +/- 1% NIST

Analytical Information

Component Oxygen

Reference Standard(s)

Balance Gas Concentration Cylinder Number NIST Reference

Nitrogen 24.430%

Analysis Date: 1/30/2013

Conc. 19.9%

Conc. 20.0%

Conc. 20.0%

Z= Zero Gas S= Span Gas C= Candidate Gas 

Conc. 19.6%

Conc. 19.7%

Conc. 19.6%

Analysis Date:

800-551-8150

Fax (318-425-6309)

Red Ball Technical Gas Service

Information and Ordering

Fred Holt, CHMM

Quality Control

PGVP Vendor ID # G12012

1/30/2013

Nitrogen 18.4% EB0005577 PRM 3221755.02

Component Carbon Dioxide

128
CERTIFICATE OF ANALYSIS

Grade of Product: EPA Protocol

Customer: TRC PO: 45933,

STOCK BY

CONCENTRATION

Part Number: E04NI99E15A38H6 Reference Number: 54-124320914-19

Cylinder Number: CC403079 Cylinder Volume: 144.4 Cubic Feet

Laboratory: ASG - Chicago - IL Cylinder Pressure: 2015 PSIG

PGVP Number: B12012 Valve Outlet: 660

Gas Code: CO,NO,PPN,BALN Certification Date: Jun 08, 2012

Expiration Date: Jun 08, 2020

Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA

600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical

uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a

volume/volume basis unless otherwise noted.

Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.

ANALYTICAL RESULTS

Component Requested Actual Protocol Total Relative Assay

Concentration Concentration Method Uncertainty Dates

PROPANE 85.00 PPM 86.79 PPM G1 +/- 1% NIST Traceable 06/07/2012

CARBON MONOXIDE 100.0 PPM 100.1 PPM G1 +/- 1% NIST Traceable 06/07/2012, 06/08/2012

NITRIC OXIDE 100.0 PPM 100.1 PPM G1 +/- 1% NIST Traceable 06/07/2012, 06/08/2012

NITROGEN Balance

Total oxides of nitrogen 100.1 PPM For Reference Only

CALIBRATION STANDARDS

Type Lot ID Cylinder No Concentration Uncertainty Expiration Date

NTRM/C3H8 09061733 CC303833 97.82 PPM PROPANE/AIR +/- 0.5% Oct 02, 2013

NTRM/CO 09060516 CC280458 98.88 PPM CARBON MONOXIDE/ +/- 0.5% Feb 01, 2013

NTRM/CO 09060516 CC280693 98.88 PPM CARBON MONOXIDE/ +/- 0.5% Feb 11, 2013

NTRM/NO 11060518 CC331279 101.2 PPM NITRIC OXIDE/NITROGEN +/- 0.6% Feb 16, 2017

ANALYTICAL EQUIPMENT

Instrument/Make/Model Analytical Principle Last Multipoint Calibration

Nexus 470 AEP0000428 FTIR May 09, 2012

Nexus 470 AEP0000428 FTIR May 09, 2012

Nexus 470 AEP0000428 FTIR May 09, 2012

Triad Data Available Upon Request

Notes:TRC PO: 45933, STOCK BY 

CONCENTRATION

Signature on file

____________________________________

Approved for Release

Page 1 of 54-124320914-19

129
CERTIFICATE OF ANALYSIS

Grade of Product: EPA Protocol

Customer PO Number: 59415

Part Number: E03NI80E15AC2K9 Reference Number: 54-124385978-17

Cylinder Number: CC351249 Cylinder Volume: 150.9 Cubic Feet

Laboratory: ASG - Chicago - IL Cylinder Pressure: 2015 PSIG

PGVP Number: B12013 Valve Outlet: 590

Gas Code: CO2,O2,BALN Certification Date: Jul 26, 2013

Expiration Date: Jul 26, 2021

Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA

600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical

uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a

volume/volume basis unless otherwise noted.

Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.

ANALYTICAL RESULTS

Component Requested Actual Protocol Total Relative Assay

Concentration Concentration Method Uncertainty Dates

CARBON DIOXIDE 10.00 % 9.950 % G1 +/- 1.0% NIST Traceable 07/26/2013

OXYGEN 10.00 % 9.969 % G1 +/- 1.0% NIST Traceable 07/26/2013

NITROGEN Balance

CALIBRATION STANDARDS

Type Lot ID Cylinder No Concentration Uncertainty Expiration Date

CO2 97051015 SG9198991BAL 10.818 % CARBON DIOXIDE/NITROGEN +/- 0.5% Jun 28, 2018

NTRM/O2 98051016 SG9163074BAL 12.05 % OXYGEN/NITROGEN +/- 0.7% Dec 02, 2017

ANALYTICAL EQUIPMENT

Instrument/Make/Model Analytical Principle Last Multipoint Calibration

CO2-1 HORIBA VIA-510 V1E3H7P5 NDIR Jul 22, 2013

O2-1 HORIBA MPA-510 3VUYL9NR Paramagnetic Jul 18, 2013

Triad Data Available Upon Request

Permanent Notes:STOCK BY 

CONCENTRATION

Notes:TRC PO #59415 "STOCK BY 

CONCENTRATON"

Signature on file

____________________________________

Approved for Release

Page 1 of 54-124385978-17

130
CERTIFICATE OF ANALYSIS

Grade of Product: EPA Protocol

Part Number: E04NI99E15A3528 Reference Number: 54-124369425-2

Cylinder Number: CC335400 Cylinder Volume: 144.4 Cubic Feet

Laboratory: ASG - Chicago - IL Cylinder Pressure: 2015 PSIG

PGVP Number: B12013 Valve Outlet: 660

Gas Code: CO,NO,PPN,BALN Certification Date: Apr 16, 2013

Expiration Date: Apr 16, 2021

Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA

600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical

uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a

volume/volume basis unless otherwise noted.

Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals.

ANALYTICAL RESULTS

Component Requested Actual Protocol Total Relative Assay

Concentration Concentration Method Uncertainty Dates

NOX 50.00 PPM 51.01 PPM G1 +/- 1.1% NIST

Traceable

04/09/2013, 04/16/2013

PROPANE 45.00 PPM 45.57 PPM G1 +/- 1% NIST Traceable 04/09/2013

CARBON MONOXIDE 50.00 PPM 49.66 PPM G1 +/- 1% NIST Traceable 04/09/2013

NITRIC OXIDE 50.00 PPM 51.01 PPM G1 +/- 1.1% NIST

Traceable

04/09/2013, 04/16/2013

NITROGEN Balance

CALIBRATION STANDARDS

Type Lot ID Cylinder No Concentration Uncertainty Expiration Date

NTRM/C3H8 09061733 CC303833 97.82 PPM PROPANE/AIR +/- 0.5% Oct 02, 2013

CO 12060505 CC353897 49.53 PPM CARBON MONOXIDE/NITROGEN +/- 0.6% Dec 20, 2017

NO 12060806 CC280981 49.95 PPM NITRIC OXIDE/NITROGEN +/- 0.8% Dec 16, 2017

NO2 124206889130 CC323209 4.824 PPM NITROGEN DIOXIDE/NITROGEN +/- 2.0% Oct 25, 2015

ANALYTICAL EQUIPMENT

Instrument/Make/Model Analytical Principle Last Multipoint Calibration

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Triad Data Available Upon Request

Notes:TRC P.O. 55889 "STOCK BY 

CONCENTRATION"

Signature on file

____________________________________

Approved for Release

Page 1 of 54-124369425-2

131
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP

Part Number: X03NI60P15A25V2 Reference Number: 126-400243593-1

Cylinder

Number:

CC427628 Cylinder Volume: 160.0 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 1936 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243593-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

ETHANE 20.00 % 20.00 % +/- 1%

METHANE 20.00 % 20.00 % +/- 1%

NITROGEN Balance

Notes:.

PO # 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243593-1

132
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP

Part Number: X03NI90P15A51P0 Reference Number: 126-400243594-1

Cylinder

Number:

CC427627 Cylinder Volume: 148.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243594-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

ETHANE 5.000 % 4.995 % +/- 1%

METHANE 5.000 % 5.002 % +/- 1%

NITROGEN Balance

Notes:.

PO # 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243594-1

133
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX

Part Number: X03NI4P15A57J0 Reference Number: 126-400243591-1

Cylinder

Number:

CC427616 Cylinder Volume: 174.6 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243591-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

ETHANE 1.000 % 0.9998 % +/- 1%

METHANE 95.00 % 95.00 % +/- 1%

NITROGEN Balance

Notes:

TRC ENVIRONMENTAL CORP - BELTON , TX

TRC PO#: 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243591-1

134
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX

Part Number: X03NI40P15A4BC1 Reference Number: 126-400243592-1

Cylinder

Number:

CC427422 Cylinder Volume: 166.5 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243592-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

ETHANE 10.00 % 10.00 % +/- 1%

METHANE 50.00 % 50.00 % +/- 1%

NITROGEN Balance

Notes:

TRC ENVIRONMENTAL CORP - BELTON , TX

TRC PO#: 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243592-1

135
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP

Part Number: X02NI15P15A0PK1 Reference Number: 126-400243585-1

Cylinder

Number:

CC427195 Cylinder Volume: 9.8 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 109 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243585-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

PROPYLENE 85.00 % 85.02 % +/- 1%

NITROGEN Balance

Notes:.

PO # 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243585-1

136
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX

Part Number: X02NI99P15A3LE2 Reference Number: 126-400243589-1

Cylinder

Number:

CC427190 Cylinder Volume: 144.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG

Analysis Date:Aug 26, 2013 Valve Outlet: 350

Lot Number: 126-400243589-1

Expiration Date: Aug 26, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

PROPYLENE 50.00 PPM 50.20 PPM +/- 1%

NITROGEN Balance

Notes:

TRC ENVIRONMENTAL CORP/BELTON , TX

TRC PO#: 60350

"JIM BARUFALDI/ JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243589-1

137
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX

Part Number: X02NI99P15A51P7 Reference Number: 126-400243588-1

Cylinder

Number:

CC427187 Cylinder Volume: 144.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG

Analysis Date:Aug 26, 2013 Valve Outlet: 350

Lot Number: 126-400243588-1

Expiration Date: Aug 26, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

PROPYLENE 85.00 PPM 84.96 PPM +/- 1%

NITROGEN Balance

Notes:

TRC ENVIRONMENTAL CORP/BELTON , TX

TRC PO#: 60350

"JIM BARUFALDI/ JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243588-1

138
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP

Part Number: X02NI50P15A40F3 Reference Number: 126-400243586-1

Cylinder

Number:

CC427185 Cylinder Volume: 16.3 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 197 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243586-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

PROPYLENE 50.00 % 50.00 % +/- 1%

NITROGEN Balance

Notes:.

PO # 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243586-1

139
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP

Part Number: X02NI70P15A0PK1 Reference Number: 126-400243587-1

Cylinder

Number:

CC427181 Cylinder Volume: 26.8 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 338 PSIG

Analysis Date:Aug 22, 2013 Valve Outlet: 350

Lot Number: 126-400243587-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

PROPYLENE 30.00 % 30.01 % +/- 1%

NITROGEN Balance

Notes:.

PO # 60350

"JIM BARUFALDI / JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243587-1

140
CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX

Part Number: X02NI99P15A51P8 Reference Number: 126-400243590-1

Cylinder

Number:

CC427175 Cylinder Volume: 144.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG

Analysis Date:Aug 26, 2013 Valve Outlet: 350

Lot Number: 126-400243590-1

Expiration Date: Aug 26, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.

ANALYTICAL RESULTS

Component Requested Actual Concentration Analytical

Concentration (Mole %) Uncertainty

PROPYLENE 30.00 PPM 30.35 PPM +/- 1%

NITROGEN Balance

Notes:

TRC ENVIRONMENTAL CORP/BELTON , TX

TRC PO#: 60350

"JIM BARUFALDI/ JOHN ZINK"

Signature on file

____________________________________

Approved for Release

Page 1 of 126-400243590-1

141
142
This is to Certify that:

James P. Barufaldi 

Is a Qualified Individual as defined in Section 8.3 of ASTM D7036-04 for the following test methods: 

EPA Methods 18, 15, 16, 23 and 0023A 

The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04 and has successfully passed an internal comprehensive examination for the test methods designated above. This certification is effective until: 01-12-2016 

Edward J MacKinnon Air Measurements Practice Quality Coordinator 

143
This is to Certify that:

James Barufaldi 

Is a Qualified Individual as defined in Section 8.3 of ASTM D7036-04 for the following test methods: 

EPA Methods 3A, 6C, 7E, 10, 10B, 19, 20, 25A. 

CEM Performance Specifications PS2, PS3, PS4, PS4A, PS5, PS6, PS7, PS8, and PS15 

The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04 and has successfully passed a comprehensive examination for the test methods designated above. This certification is effective until: 02-21-2018 

Date of Issue: 03-25-2013 

Certificate Number: 00560

Edward J MacKinnon Air Measurements Practice Quality Director 

144
This is to Certify that:

James Barufaldi 

Is a Qualified Individual as defined in Section 8.3 of ASTM D7036-04 for the following test methods: 

EPA Methods 1, 2, 3, 4, 3B, 6, 6A, 6B, 7, 7C, 7D, 8, 11, 13A, 13B, 15A, 16A, 19, 26, 26A, and 202. 

The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04 and has successfully passed a comprehensive examination for the test methods designated above. This certification is effective until: 02-21-2018 

Date of Issue: 03-25-2013

Certificate Number: 00559

Edward J MacKinnon Air Measurements Practice Quality Director 

145
This is to Certify that:

James Barufaldi 

Is a Qualified Individual as defined in Section 8.3 of ASTM D7036-04 for the following test methods: 

EPA Methods 1, 1A, 2, 2A, 2C, 2D, 2F, 2G, 2H, 3, 3B, 4, 5, 5A, 5B, 5E, 5F, 5i, 17, 19, 201A, and 202. 

The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04 and has successfully passed a comprehensive examination for the test methods designated above. This certification is effective until: 02-21-2018 

Date of Issue: 03-25-2013

Certificate Number: 00558

Edward J MacKinnon Air Measurements Practice Quality Director 

146