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# Table of Contents

I NTRODUCTION 

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  A NALYTICAL 

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## A SSURANCE 

## A CTIVITIES 

## 

 A PPENDICES 

## A Detailed Summary of Results B Discussion of Errors and Example Calculations C Instrumental Quality Assurance D Datalog Records and Chromatograms E Sample Gas Extraction Diagram F Calibration Certificates





#  

# Introduction

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## 

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 Determination of the Inlet Flare Gas Composition and Mass Rate

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#   

# TABLE 

# 1
Background Information 

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7HVWLQJE\75&$XVWLQ7H[DV TABLE2:STEAMASSISTEDFLARESUMMARY OFRESULTSRunS1 S2 S3 S4 S5 S6Date11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013SteamRate(lbs/hr)582.00.0124.2 130.1 304.3 643.1HeatingValue(Btu/scf)101510205647006312136HeatRate(MMBtu/hr)121.27 121.17 10.89 34.44 13.85 38.59MassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)28.54 27.45 0.845.121.324.11CO(lbs/hr)10.73 2.252.412.167.522.65THC(lbs/hr)3.520.623.371.377.850.57Propylene(lbs/hr)Direct3.563.962.773.585.140.56Propylene(lbs/hr)Bag8.410.717.842.54 11.833.30NOx(lbs/MMBTU)0.235 0.227 0.077 0.149 0.095 0.106CO(lbs/MMBTU)0.088 0.019 0.221 0.063 0.543 0.069THC(lbs/MMBTU)0.029 0.005 0.310 0.040 0.567 0.015Propylene(lbs/MMBTU)Direct0.029 0.033 0.255 0.104 0.371 0.014Propylene(lbs/MMBTU)Bag0.069 0.006 0.720 0.074 0.854 0.086MassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)27.13 28.96 0.835.281.354.39CO(lbs/hr)10.20 2.382.382.237.672.83THC(lbs/hr)3.350.653.321.418.000.61Propylene(lbs/hr)Direct3.384.182.733.695.250.60Propylene(lbs/hr)Bag7.990.757.732.62 12.063.52NOx(lbs/MMBTU)0.224 0.239 0.076 0.153 0.097 0.114CO(lbs/MMBTU)0.084 0.020 0.218 0.065 0.554 0.073THC(lbs/MMBTU)0.028 0.005 0.305 0.041 0.578 0.016Propylene(lbs/MMBTU)Direct0.028 0.034 0.251 0.107 0.379 0.015Propylene(lbs/MMBTU)Bag0.066 0.006 0.710 0.076 0.871 0.091Efficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)99.94% 99.99% 99.39% 99.92% 98.96% 99.97%PropyleneDEDirect(%)99.94% 99.94% 99.50% 99.80% 99.32% 99.97%PropyleneDEBag(%)99.86% 99.99% 98.58% 99.86% 98.44% 99.83%Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)99.95% 99.99% 99.40% 99.92% 98.94% 99.97%PropyleneDEDirect(%)99.94% 99.93% 99.50% 99.80% 99.31% 99.97%PropyleneDEBag(%)99.87% 99.99% 98.60% 99.85% 98.41% 99.82%CombustionEfficeincy(%)99.90% 99.98% 99.59% 99.91% 99.08% 99.92%7HVWLQJE\75&$XVWLQ7H[DV TABLE3:PRESSUREASSISTEDFLARESUMMARY OFRESULTSRunP1HAverage P1LAverage P2HAverage P2LAverage P3HAverage P3LAverage P4Date11/19‐11/21 11/20‐11/21 11/20‐11/21 11/20‐11/21 11/20‐11/21 11/21/2013 11/22/2013HeatingValue(Btu/scf)2145 2133776711698690327HeatRate(MMBtu/hr)163.25 106.17 71.45 41.03 71.21 43.17 37.84MassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)21.46 11.40 14.73 7.91 11.48 6.30N/ACO(lbs/hr)2.541.692.493.544.361.89N/ATHC(lbs/hr)1.800.780.631.161.560.47N/APropylene(lbs/hr)Direct7.552.542.780.851.800.37N/APropylene(lbs/hr)Bag6.811.220.861.132.690.49N/ANOx(lbs/MMBTU)0.131 0.107 0.206 0.193 0.161 0.146 N/ACO(lbs/MMBTU)0.016 0.016 0.035 0.086 0.061 0.044 N/ATHC(lbs/MMBTU)0.011 0.007 0.009 0.028 0.022 0.011 N/APropylene(lbs/MMBTU)Direct0.046 0.024 0.039 0.021 0.025 0.008 N/APropylene(lbs/MMBTU)Bag0.042 0.012 0.012 0.027 0.038 0.011 N/AMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)23.01 12.18 15.60 8.15 11.76 6.43N/ACO(lbs/hr)2.771.802.643.654.491.93N/ATHC(lbs/hr)1.970.840.671.201.600.48N/APropylene(lbs/hr)Direct8.122.662.950.881.850.37N/APropylene(lbs/hr)Bag7.341.310.911.162.760.50N/ANOx(lbs/MMBTU)0.140 0.115 0.218 0.199 0.165 0.149 N/ACO(lbs/MMBTU)0.017 0.017 0.037 0.089 0.063 0.045 N/ATHC(lbs/MMBTU)0.012 0.008 0.009 0.029 0.022 0.011 N/APropylene(lbs/MMBTU)Direct0.049 0.025 0.041 0.021 0.026 0.009 N/APropylene(lbs/MMBTU)Bag0.045 0.013 0.013 0.028 0.039 0.012 N/AEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)99.98% 99.99% 99.98% 99.95% 99.96% 99.98% N/APropyleneDEDirect(%)99.91% 99.95% 99.93% 99.96% 99.95% 99.98% N/APropyleneDEBag(%)99.92% 99.98% 99.98% 99.95% 99.93% 99.98% N/AEfficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)99.98% 99.98% 99.98% 99.95% 99.96% 99.98% N/APropyleneDEDirect(%)99.90% 99.95% 99.92% 99.96% 99.95% 99.98% N/APropyleneDEBag(%)99.91% 99.98% 99.98% 99.95% 99.92% 99.98% N/ACombustionEfficeincy(%)99.98% 99.98% 99.96% 99.89% 99.92% 99.95% N/A

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# Figure 1. Test Arrangement

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#  

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# Appendix A: Detailed Summary of Results



 DetailedSummaryofResultsRunS1 S2 S3 S4 S5 S6Date11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013StartTime9:199:4511:2913:3614:1814:56EndTime9:3910:0511:5613:5614:4815:16FlareFeedpaused41‐48paused28‐38PropyleneFlowrate(lbs/hr)6122.8 6109.1 551.2 1802.3 757.8 1969.4NitrogenFlowrate(lbs/hr)4635.3 4595.5 1040.8 2366.6 1076.50.0NaturalGasFlowrate(lbs/hr)0.00.00.00.00.00.0TotalFuelFlowRate(lbs/hr)10758.1 10704.8 1592.0 4168.8 1834.3 1969.4SteamRate(lbs/hr)582.00.0124.2130.1304.3643.1HeatingValue(Btu/lb)11272 1132068408262755019593HeatingValue(Btu/scf)101510205647006312136HeatRate(MMBtu/hr)121.27 121.17 10.8934.4413.8538.59O2F‐Factor9837983110644 10291 104519304CO2F‐Factor139813981398139813981397ExhaustFlowRate(DSCFH)O2F‐factor20,740,514 18,933,793 3,323,103 4,978,617 3,372,093 7,641,384ExhaustFlowRate(DSCFH@0%O2)1,192,828 1,191,289115,911 354,458 144,726 359,035ExhaustFlowRate(DSCFH)CO2F‐factor19,713,348 19,977,101 3,275,139 5,134,872 3,439,597 8,157,100EmissionsNOx(ppmv)11.527 12.142 2.1138.6103.2794.503CO(ppmv)7.1191.6389.9865.983 30.694 4.779THC(ppmv)1.5580.3009.3052.526 21.347 0.689O2(%)19.698 19.585 20.171 19.412 20.003 19.918CO2(%)0.8600.8480.4650.9380.5630.661DirectM18methane(ppmv)1.4081.4742.3772.9111.9322.491DirectM18ethane(ppmv)0.0000.0000.0000.0000.0000.000DirectM18propylene(ppmv)1.5731.9197.6526.590 13.992 0.669BagM18methane(ppmv)1.0922.0783.1742.2872.8551.094BagM18ethane(ppmv)0.0000.0000.0000.0000.0000.000BagM18propylene(ppmv)3.7200.346 21.643 4.685 32.175 3.963NOx(ppmv@0%O2)200.428 192.979 60.578 120.933 76.400 95.838CO(ppmv@0%O2)123.783 26.034 286.293 84.035 715.167 101.712THC(ppmv@0%O2)27.0904.768 266.769 35.479 497.383 14.664TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunS1 S2 S3 S4 S5 S6Date11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013 11/19/2013StartTime9:199:4511:2913:3614:1814:56EndTime9:3910:0511:5613:5614:4815:16MassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)28.5427.450.845.121.324.11CO(lbs/hr)10.732.252.412.167.522.65THC(lbs/hr)3.520.623.371.377.850.57Propylene(lbs/hr)Direct3.563.962.773.585.140.56Propylene(lbs/hr)Bag8.410.717.842.5411.833.30NOx(lbs/MMBTU)0.2350.2270.0770.1490.0950.106CO(lbs/MMBTU)0.0880.0190.2210.0630.5430.069THC(lbs/MMBTU)0.0290.0050.3100.0400.5670.015Propylene(lbs/MMBTU)Direct0.0290.0330.2550.1040.3710.014Propylene(lbs/MMBTU)Bag0.0690.0060.7200.0740.8540.086MassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)27.1328.960.835.281.354.39CO(lbs/hr)10.202.382.382.237.672.83THC(lbs/hr)3.350.653.321.418.000.61Propylene(lbs/hr)Direct3.384.182.733.695.250.60Propylene(lbs/hr)Bag7.990.757.732.6212.063.52NOx(lbs/MMBTU)0.2240.2390.0760.1530.0970.114CO(lbs/MMBTU)0.0840.0200.2180.0650.5540.073THC(lbs/MMBTU)0.0280.0050.3050.0410.5780.016Propylene(lbs/MMBTU)Direct0.0280.0340.2510.1070.3790.015Propylene(lbs/MMBTU)Bag0.0660.0060.7100.0760.8710.091Efficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)99.94% 99.99% 99.39% 99.92% 98.96% 99.97%PropyleneDEDirect(%)99.94% 99.94% 99.50% 99.80% 99.32% 99.97%PropyleneDEBag(%)99.86% 99.99% 98.58% 99.86% 98.44% 99.83%Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)99.95% 99.99% 99.40% 99.92% 98.94% 99.97%PropyleneDEDirect(%)99.94% 99.93% 99.50% 99.80% 99.31% 99.97%PropyleneDEBag(%)99.87% 99.99% 98.60% 99.85% 98.41% 99.82%CombustionEfficeincy(%)99.90% 99.98% 99.59% 99.91% 99.08% 99.92%TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P1H‐1 P1H‐2 P1H‐3 P1HAverage11/19/2013 11/20/2013 11/21/2013 11/19‐11/2115:4514:0913:4816:0514:2914:088575.4 8200.9 8145.9 8307.40.00.00.00.00.00.00.00.08575.4 8200.9 8145.9 8307.40.00.00.00.019800 19476 19670 196492170211721492145169.80 159.72 160.23 163.259297930993029302139713971397139729,222,469 43,705,437 16,937,928 29,955,2781,578,573 1,486,821 1,490,376 1,518,59031,013,562 49,050,915 17,698,423 32,587,6347.5033.286 10.412 7.0671.0171.1821.3971.1990.0110.7940.8510.55219.771 20.189 19.061 19.6740.7650.4551.2650.8282.2132.3284.1982.9130.0000.0000.0000.0003.2831.4342.9012.5392.4082.9765.6763.6870.0000.0000.0000.0001.9991.5903.5102.367138.895 96.593 118.331 117.94018.827 34.745 15.877 23.1500.204 23.340 9.672 11.072TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P1H‐1 P1H‐2 P1H‐3 P1HAverage11/19/2013 11/20/2013 11/21/2013 11/19‐11/2115:4514:0913:4816:0514:2914:0826.1817.1521.0521.462.163.751.722.540.043.781.571.8010.466.835.367.556.377.586.486.810.1540.1070.1310.1310.0130.0240.0110.0160.0000.0240.0100.0110.0620.0430.0330.0460.0380.0470.0400.04227.7819.2422.0023.012.294.211.802.770.044.251.641.9711.107.675.608.126.768.506.777.340.1640.1200.1370.1400.0130.0260.0110.0170.0000.0270.0100.0120.0650.0480.0350.0490.0400.0530.0420.045100.00% 99.95% 99.98% 99.98%99.88% 99.92% 99.93% 99.91%99.93% 99.91% 99.92% 99.92%100.00% 99.95% 99.98% 99.98%99.87% 99.91% 99.93% 99.90%99.92% 99.90% 99.92% 99.91%99.99% 99.96% 99.98% 99.98%TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P1L‐1 P1L‐2 P1L‐3 P1LAverage11/20/2013 11/21/2013 11/21/2013 11/20‐11/2114:579:4416:3215:1710:0416:525240.5 5394.0 5632.7 5422.40.00.00.00.00.00.00.00.05240.6 5397.3 5632.7 5423.50.00.00.00.019577 19579 19570 195752133213421322133102.59 105.67 110.23 106.179305930593059305139713971397139715,809,862 11,193,125 18,370,446 15,124,478954,643 983,281 1,025,757 987,89417,741,972 11,644,847 19,181,822 16,189,5475.8038.6415.3406.5951.1572.0081.5821.5820.5430.3860.4680.46619.638 19.064 19.733 19.4780.8081.2680.8030.9602.6491.3110.9341.6310.0000.0000.0000.0000.3522.3122.0891.5842.8992.9690.0001.9560.0000.0000.0000.0000.9541.6440.0000.86696.104 98.364 95.635 96.70119.161 22.858 28.332 23.4508.9934.3948.3817.256TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P1L‐1 P1L‐2 P1L‐3 P1LAverage11/20/2013 11/21/2013 11/21/2013 11/20‐11/2114:579:4416:3215:1710:0416:5210.9511.5511.7111.401.331.632.111.690.940.470.940.780.612.824.182.541.642.010.001.220.1070.1090.1060.1070.0130.0150.0190.0160.0090.0040.0090.0070.0060.0270.0380.0240.0160.0190.0000.01212.2912.0112.2312.181.491.702.211.801.050.490.980.840.682.934.372.661.852.090.001.310.1200.1140.1110.1150.0150.0160.0200.0170.0100.0050.0090.0080.0070.0280.0400.0250.0180.0200.0000.01399.98% 99.99% 99.98% 99.99%99.99% 99.95% 99.93% 99.95%99.97% 99.96% 100.00% 99.98%99.98% 99.99% 99.98% 99.98%99.99% 99.95% 99.92% 99.95%99.96% 99.96% 100.00% 99.98%99.98% 99.98% 99.97% 99.98%TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P2H‐1* P2H‐1b P2H‐2 P2H‐3 P2HAverage11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/2114:0116:3710:5616:0214:0616:5711:1616:221638.8 3820.9 3786.7 3755.0 3787.50.54144.2 4130.3 4103.5 4126.00.00.00.00.00.01638.9 7965.1 7917.0 7859.3 7913.80.00.00.00.00.08723897991458961902874677178877077614.3071.5272.4070.4371.4510201 10155 10127 10158 10147139813981398139813981,886,027 8,213,579 11,608,173 10,008,135 9,943,296145,829 726,253 733,148 715,414 724,9381,979,139 8,650,402 12,360,155 10,611,690 10,540,74915.508 16.526 10.243 11.546 12.7721.7101.7702.9975.3253.3640.4220.3760.3900.9670.57819.284 19.052 19.580 19.406 19.3461.0101.1560.8190.9280.9683.5172.3033.5161.4272.4150.0000.0000.0000.0000.0007.9931.6303.4032.3522.462N/A2.6982.5671.7012.322N/A0.0000.0000.0000.000N/A0.5450.6231.1990.789200.568 186.901 162.181 161.520 170.20122.116 20.018 47.453 74.493 47.3215.4584.2526.175 13.528 7.985*Only5minutesofdata.NotincludedinaverageTestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P2H‐1* P2H‐1b P2H‐2 P2H‐3 P2HAverage11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/2114:0116:3710:5616:0214:0616:5711:1616:223.4916.2114.2013.8014.730.231.062.533.872.490.090.340.491.050.631.641.464.312.572.78N/A0.490.791.310.860.2440.2270.1960.1960.2060.0160.0150.0350.0550.0350.0060.0050.0070.0150.0090.1150.0200.0590.0360.039N/A0.0070.0110.0190.0123.6617.0715.1214.6315.600.251.112.694.112.640.090.350.531.120.671.721.544.592.722.95N/A0.510.841.390.910.2560.2390.2090.2080.2180.0170.0160.0370.0580.0370.0060.0050.0070.0160.0090.1210.0210.0630.0390.041N/A0.0070.0120.0200.01399.99% 99.99% 99.99% 99.97% 99.98%99.90% 99.96% 99.89% 99.93% 99.93%N/A99.99% 99.98% 99.97% 99.98%99.99% 99.99% 99.99% 99.97% 99.98%99.89% 99.96% 99.88% 99.93% 99.92%N/A99.99% 99.98% 99.96% 99.98%99.98% 99.98% 99.96% 99.93% 99.96%*Only5minutesofdata.NotincludedinaverageTestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P2L‐1* P2L‐1b P2L‐2 P2L‐3 P2LAverage11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/2117:2317:3911:3114:3817:2617:5911:5114:581984.9 2217.4 2175.5 2112.5 2168.52852.4 2738.0 2746.4 2705.7 2730.00.00.00.00.00.04837.3 4955.4 4921.9 4818.2 4898.50.00.00.00.00.07753825584338445837865069971771871137.5040.9141.5140.6941.0310402 10292 10256 10254 10267139813981398139813987,523,997 7,017,078 7,286,650 5,372,700 6,558,810390,120 421,025 425,694 417,220 421,3136,411,214 7,268,371 7,498,419 5,513,134 6,759,9759.2169.2089.015 12.757 10.32716.066 7.5057.3727.3967.4245.6311.8331.8371.0621.57719.816 19.646 19.679 19.277 19.5340.8180.7870.7741.0320.8640.8812.4922.3011.4682.0870.0000.0000.0000.0000.0007.3901.0681.3951.0631.175N/A2.5352.9141.1032.184N/A0.0000.0000.0000.000N/A1.1041.9451.6921.580177.737 153.467 154.311 164.277 157.351309.861 125.083 126.187 95.241 115.504108.608 30.550 31.444 13.676 25.223*Only3minutesofdata.NotincludedinaverageTestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P2L‐1* P2L‐1b P2L‐2 P2L‐3 P2LAverage11/20/2013 11/20/2013 11/21/2013 11/21/2013 11/20‐11/2117:2317:3911:3114:3817:2617:5911:5114:588.287.717.848.187.918.783.833.902.893.544.621.401.460.621.166.060.821.110.620.85N/A0.841.540.991.130.2210.1890.1890.2010.1930.2340.0940.0940.0710.0860.1230.0340.0350.0150.0280.1620.0200.0270.0150.021N/A0.0210.0370.0240.0277.057.998.078.408.157.493.964.022.963.653.941.451.500.641.205.160.851.140.640.88N/A0.871.591.021.160.1880.1950.1940.2060.1990.2000.0970.0970.0730.0890.1050.0360.0360.0160.0290.1380.0210.0270.0160.021N/A0.0210.0380.0250.02899.77% 99.94% 99.93% 99.97% 99.95%99.69% 99.96% 99.95% 99.97% 99.96%N/A99.96% 99.93% 99.95% 99.95%99.80% 99.93% 99.93% 99.97% 99.95%99.74% 99.96% 99.95% 99.97% 99.96%N/A99.96% 99.93% 99.95% 99.95%99.74% 99.88% 99.88% 99.92% 99.89%*Only3minutesofdata.NotincludedinaverageTestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P3H‐1 P3H‐2 P3H‐3 P3HAverage11/20/2013 11/21/2013 11/21/2013 11/20‐11/2119:1812:4515:3419:3813:0515:542598.8 2523.9 2512.4 2545.03882.5 3871.0 3824.3 3859.31103.2 1107.9 1113.5 1108.27584.4 7502.7 7450.2 7512.40.00.00.00.0944094199578947969769370569871.6070.6771.3671.2110176 10181 10156 1017113121310131013117,069,322 11,072,9339,042,647 9,061,634728,580 719,476 724,710 724,2557,076,371 11,305,4909,531,890 9,304,58415.005 7.951 10.441 11.1328.3613.7368.7956.9641.7251.2041.9161.61518.746 19.542 19.225 19.1711.3270.8190.9811.0423.7830.0001.5391.7740.0000.0000.0000.0002.2641.1632.2701.8995.8813.2584.5764.5720.0000.0000.0000.0003.0662.7342.4512.751145.592 122.368 130.279 132.74681.126 57.498 109.741 82.78816.737 18.530 23.907 19.725TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P3H‐1 P3H‐2 P3H‐3 P3HAverage11/20/2013 11/21/2013 11/21/2013 11/20‐11/2119:1812:4515:3419:3813:0515:5412.6610.5111.2711.484.303.015.784.361.331.451.891.561.741.402.241.802.363.302.422.690.1770.1490.1580.1610.0600.0430.0810.0610.0190.0210.0260.0220.0240.0200.0310.0250.0330.0470.0340.03812.6810.7311.8811.764.303.076.094.491.331.481.991.601.751.432.361.852.373.372.552.760.1770.1520.1670.1650.0600.0430.0850.0630.0190.0210.0280.0220.0240.0200.0330.0260.0330.0480.0360.03999.96% 99.96% 99.95% 99.96%99.95% 99.96% 99.94% 99.95%99.94% 99.91% 99.93% 99.93%99.96% 99.96% 99.95% 99.96%99.95% 99.96% 99.93% 99.95%99.94% 99.91% 99.93% 99.92%99.92% 99.94% 99.89% 99.92%TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P3L‐1b P3L‐2 P3L‐3 P3LAverage11/21/2013 11/21/2013 11/21/2013 11/21/20139:0613:1715:069:2613:3715:261539.3 1533.2 1579.6 1550.72393.7 2386.8 2354.6 2378.3665.7656.8666.6663.04598.6 4576.8 4600.8 4592.10.00.00.00.0927893279599940167968470869042.6742.6944.1643.1710207 10198 10152 1018613071308131113094,386,722 5,934,951 4,436,776 4,919,483435,524 435,324 448,348 439,7324,489,683 6,081,884 4,498,741 5,023,43612.018 8.562 12.356 10.9795.3153.8967.0985.4360.1601.0951.2680.84118.825 19.367 18.788 18.9931.2420.9181.2871.1491.0392.6630.0001.2340.0000.0000.0000.0001.0660.5580.4640.6962.9522.8863.0262.9550.0000.0000.0000.0002.3440.1770.4650.996121.049 116.729 122.273 120.01753.534 53.116 70.241 58.9641.612 14.929 12.548 9.696TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P3L‐1b P3L‐2 P3L‐3 P3LAverage11/21/2013 11/21/2013 11/21/2013 11/21/20139:0613:1715:069:2613:3715:266.296.076.546.301.691.682.291.890.080.710.610.470.510.360.220.371.120.110.230.490.1480.1420.1480.1460.0400.0390.0520.0440.0020.0170.0140.0110.0120.0080.0050.0080.0260.0030.0050.0116.446.226.646.431.731.722.321.930.080.730.620.480.520.370.230.371.150.120.230.500.1510.1460.1500.1490.0410.0400.0530.0450.0020.0170.0140.0110.0120.0090.0050.0090.0270.0030.0050.012100.00% 99.97% 99.97% 99.98%99.98% 99.98% 99.99% 99.98%99.95% 99.99% 99.99% 99.98%100.00% 99.97% 99.97% 99.98%99.98% 99.98% 99.99% 99.98%99.95% 99.99% 99.99% 99.98%99.96% 99.95% 99.94% 99.95%TestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeFlareFeedPropyleneFlowrate(lbs/hr)NitrogenFlowrate(lbs/hr)NaturalGasFlowrate(lbs/hr)TotalFuelFlowRate(lbs/hr)SteamRate(lbs/hr)HeatingValue(Btu/lb)HeatingValue(Btu/scf)HeatRate(MMBtu/hr)O2F‐FactorCO2F‐FactorExhaustFlowRate(DSCFH)O2F‐factorExhaustFlowRate(DSCFH@0%O2)ExhaustFlowRate(DSCFH)CO2F‐factorEmissionsNOx(ppmv)CO(ppmv)THC(ppmv)O2(%)CO2(%)DirectM18methane(ppmv)DirectM18ethane(ppmv)DirectM18propylene(ppmv)BagM18methane(ppmv)BagM18ethane(ppmv)BagM18propylene(ppmv)NOx(ppmv@0%O2)CO(ppmv@0%O2)THC(ppmv@0%O2)P411/22/201310:0910:230.00.01227.02703†0.0N/A32737.84N/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/A†TotalflowrateincludeshydrogenTestingbyTRC,Austin,TexasDetailedSummaryofResultsRunDateStartTimeEndTimeMassEmissionRates(BasedonO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagMassEmissionRates(BasedonCO2F‐Factor)NOx(lbs/hr)CO(lbs/hr)THC(lbs/hr)Propylene(lbs/hr)DirectPropylene(lbs/hr)BagNOx(lbs/MMBTU)CO(lbs/MMBTU)THC(lbs/MMBTU)Propylene(lbs/MMBTU)DirectPropylene(lbs/MMBTU)BagEfficiencies(BasedonO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)Efficiencies(BasedonCO2F‐Factor)DestructionEfficiency(%)PropyleneDEDirect(%)PropyleneDEBag(%)CombustionEfficeincy(%)P411/22/201310:0910:23N/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/AN/A†TotalflowrateincludeshydrogenTestingbyTRC,Austin,Texas

### 99.88% 99.89% 99.90% 99.91% 99.92% 99.93% 99.94% 99.95% 99.96% 99.97% 99.98% 99.99% 100.00%

P1H Average P1L Average P2H Average P2L Average P3H Average P3L Average Destruction Efficiency (%) (O2 F-Factor)
Propylene DE Direct (%) (O2 F-Factor)
Propylene DE Bag (%) (O2 F-Factor)
Destruction Efficiency (%) (CO2 F-Factor)
Propylene DE Direct (%) (CO2 F-Factor)
Propylene DE Bag (%) (CO2 F-Factor)
Combustion Efficeincy (%)

### Fuel Analysis

Page 1 Component Volume O2 F Factor (dry) 9836.53 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
S1 Nitrogen 52.8377 O2 F Factor (wet) 11237.52 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.99 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.47 volume % water in flue gas @ 0% excess air Propylene 47.1623 CO2 F Factor 1398.05 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 47.1623 Heating Value 11272.02 Net Heating Value Btu/lb Heating Value 1014.93 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9831.29 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
S2 Nitrogen 52.5917 O2 F Factor (wet) 11232.27 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.98 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.47 volume % water in flue gas @ 0% excess air Propylene 47.4083 CO2 F Factor 1398.05 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 47.4083 Heating Value 11319.54 Net Heating Value Btu/lb Heating Value 1020.23 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10643.60 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
S3 Nitrogen 73.8077 O2 F Factor (wet) 12044.99 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.38 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 11.63 volume % water in flue gas @ 0% excess air Propylene 26.1923 CO2 F Factor 1398.45 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 26.1923 Heating Value 6840.45 Net Heating Value Btu/lb Heating Value 563.66 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10290.57 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
S4 Nitrogen 67.4772 O2 F Factor (wet) 11691.83 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.26 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 11.98 volume % water in flue gas @ 0% excess air Propylene 32.5228 CO2 F Factor 1398.32 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 32.5228 Heating Value 8262.50 Net Heating Value Btu/lb Heating Value 699.89 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10450.96 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
S5 Nitrogen 70.6944 O2 F Factor (wet) 11852.28 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.32 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 11.82 volume % water in flue gas @ 0% excess air Propylene 29.3056 CO2 F Factor 1398.38 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 29.3056 Heating Value 7549.62 Net Heating Value Btu/lb Heating Value 630.66 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9304.47 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
S6 Nitrogen 0.7426 O2 F Factor (wet) 10704.71 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air Propylene 99.2574 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 99.2574 Heating Value 19593.28 Net Heating Value Btu/lb Heating Value 2136.02 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9296.89 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1H-1 Nitrogen -0.8353 O2 F Factor (wet) 10697.11 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.22 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.09 volume % water in flue gas @ 0% excess air Propylene 100.8353 CO2 F Factor 1397.29 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 100.8353 Heating Value 19800.34 Net Heating Value Btu/lb Heating Value 2169.97 Net Heating Value Btu/SCF

### Fuel Analysis

Page 2 Component Volume O2 F Factor (dry) 9308.83 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P1H-2 Nitrogen 1.6279 O2 F Factor (wet) 10709.09 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.25 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air Propylene 98.3721 CO2 F Factor 1397.32 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 98.3721 Heating Value 19476.13 Net Heating Value Btu/lb Heating Value 2116.97 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9305.08 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air

P1L-1 Nitrogen 0.8670 O2 F Factor (wet) 10705.32 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air Propylene 99.1330 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 99.1330 Heating Value 19576.85 Net Heating Value Btu/lb Heating Value 2133.34 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10200.92 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2H-1 Nitrogen 65.3517 O2 F Factor (wet) 11602.13 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.22 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.08 volume % water in flue gas @ 0% excess air Propylene 34.6483 CO2 F Factor 1398.28 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 34.6483 Heating Value 8722.75 Net Heating Value Btu/lb Heating Value 745.63 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10155.02 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2H-1b Nitrogen 64.1527 O2 F Factor (wet) 11556.21 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.19 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.13 volume % water in flue gas @ 0% excess air Propylene 35.8473 CO2 F Factor 1398.26 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 35.8473 Heating Value 8978.72 Net Heating Value Btu/lb Heating Value 771.43 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10402.20 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2L-1 Nitrogen 69.7856 O2 F Factor (wet) 11803.50 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.30 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 11.87 volume % water in flue gas @ 0% excess air Propylene 30.2144 CO2 F Factor 1398.37 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 30.2144 Heating Value 7753.01 Net Heating Value Btu/lb Heating Value 650.21 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10292.07 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2L-1b Nitrogen 67.5104 O2 F Factor (wet) 11693.32 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.26 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 11.98 volume % water in flue gas @ 0% excess air Propylene 32.4896 CO2 F Factor 1398.32 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 32.4896 Heating Value 8255.25 Net Heating Value Btu/lb Heating Value 699.18 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10176.28 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P3H-1 Nitrogen 53.9824 O2 F Factor (wet) 11838.18 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane 22.9790 Moisture F Factor 1661.90 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane 1.0784 Combust. Moisture 14.04 volume % water in flue gas @ 0% excess air Propylene 21.9602 CO2 F Factor 1311.58 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 46.0176 Heating Value 9439.90 Net Heating Value Btu/lb Heating Value 696.54 Net Heating Value Btu/SCF

### Fuel Analysis

Page 3 Component Volume O2 F Factor (dry) 10207.32 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P3L-1b Nitrogen 54.4037 O2 F Factor (wet) 11883.31 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane 23.6735 Moisture F Factor 1675.99 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane 1.0438 Combust. Moisture 14.10 volume % water in flue gas @ 0% excess air Propylene 20.8790 CO2 F Factor 1306.88 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 45.5963 Heating Value 9278.49 Net Heating Value Btu/lb Heating Value 678.95 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9305.01 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P1L-2 Nitrogen 0.8528 O2 F Factor (wet) 10705.25 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air Propylene 99.1472 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 99.1472 Heating Value 19578.74 Net Heating Value Btu/lb Heating Value 2133.65 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10126.65 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2H-2 Nitrogen 63.3693 O2 F Factor (wet) 11527.83 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.18 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.15 volume % water in flue gas @ 0% excess air Propylene 36.6307 CO2 F Factor 1398.24 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 36.6307 Heating Value 9144.56 Net Heating Value Btu/lb Heating Value 788.29 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10256.25 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2L-2 Nitrogen 66.6949 O2 F Factor (wet) 11657.49 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.02 volume % water in flue gas @ 0% excess air Propylene 33.3051 CO2 F Factor 1398.30 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 33.3051 Heating Value 8432.87 Net Heating Value Btu/lb Heating Value 716.73 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10181.05 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P3H-2 Nitrogen 53.9767 O2 F Factor (wet) 11846.96 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane 23.2506 Moisture F Factor 1665.91 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane 1.0650 Combust. Moisture 14.06 volume % water in flue gas @ 0% excess air Propylene 21.7078 CO2 F Factor 1310.24 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 46.0233 Heating Value 9419.03 Net Heating Value Btu/lb Heating Value 693.33 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10198.35 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P3L-2 Nitrogen 54.2551 O2 F Factor (wet) 11871.08 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane 23.5331 Moisture F Factor 1672.74 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane 1.0656 Combust. Moisture 14.09 volume % water in flue gas @ 0% excess air Propylene 21.1462 CO2 F Factor 1307.97 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 45.7449 Heating Value 9326.51 Net Heating Value Btu/lb Heating Value 683.79 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9301.66 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P1H-3 Nitrogen 0.1626 O2 F Factor (wet) 10701.89 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.23 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air Propylene 99.8374 CO2 F Factor 1397.30 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 99.8374 Heating Value 19669.64 Net Heating Value Btu/lb Heating Value 2148.50 Net Heating Value Btu/SCF

### Fuel Analysis

Page 4 Component Volume O2 F Factor (dry) 10253.88 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2L-3 Nitrogen 66.6395 O2 F Factor (wet) 11655.12 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.02 volume % water in flue gas @ 0% excess air Propylene 33.3605 CO2 F Factor 1398.30 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 33.3605 Heating Value 8444.89 Net Heating Value Btu/lb Heating Value 717.92 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10152.20 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P3L-3 Nitrogen 53.1446 O2 F Factor (wet) 11815.66 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane 23.5523 Moisture F Factor 1663.46 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane 1.0356 Combust. Moisture 14.08 volume % water in flue gas @ 0% excess air Propylene 22.2675 CO2 F Factor 1311.04 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 46.8554 Heating Value 9598.95 Net Heating Value Btu/lb Heating Value 707.61 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10156.09 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P3H-3 Nitrogen 53.1985 O2 F Factor (wet) 11821.40 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane 23.6534 Moisture F Factor 1665.30 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane 1.0245 Combust. Moisture 14.09 volume % water in flue gas @ 0% excess air Propylene 22.1236 CO2 F Factor 1310.42 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 46.8015 Heating Value 9577.82 Net Heating Value Btu/lb Heating Value 705.24 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 10158.09 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P2H-3 Nitrogen 64.2356 O2 F Factor (wet) 11559.29 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1401.19 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 12.12 volume % water in flue gas @ 0% excess air Propylene 35.7644 CO2 F Factor 1398.26 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 35.7644 Heating Value 8961.11 Net Heating Value Btu/lb Heating Value 769.65 Net Heating Value Btu/SCF Component Volume O2 F Factor (dry) 9305.32 DSCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
P1L-3 Nitrogen 0.9158 O2 F Factor (wet) 10705.56 SCF of Exhaust/MM Btu of Fuel Burned @ 0% excess air
Methane Moisture F Factor 1400.24 SCF of Water/MM Btu of Fuel Burned @ 0% excess air
Ethane Combust. Moisture 13.08 volume % water in flue gas @ 0% excess air Propylene 99.0842 CO2 F Factor 1397.31 DSCF of CO2/MM Btu of Fuel Burned @ 0% excess air
HC total 99.0842 Heating Value 19570.41 Net Heating Value Btu/lb Heating Value 2132.29 Net Heating Value Btu/SCF

#  

# 















 

# Appendix B: Discussion of Errors and Example Calculations







 

### Discussion of E rrors 7

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## Example Calculations for Run S1 Calculation of Heat Input

QF = flare waste gas flow, lbs/hr = 10758.1 GHV = lower heating value, Btu/lb = 11272 IHF = heat input, MMBtu/hr

= (QF x GHV)/ 1000000 IH = 121.27 MMBtu/HR

Calculation of Flare Exhaust Flow Rate via EPA Method 19

IH = heat input, MMBtu/hr = 121.27 F O2 

## = O2 F-Factor, DSCF exhaust/MMBtu = 9837 C O2 

## = exhaust O2 concentration, % = 19.70 QS = dry stack flow rate, standard conditions, DSCF/hr 20.9 20.9 - C O2 

## QS = 2.07E+07 DSCFH = IH X F O2 

## X

## Example Calculations for Run S1 Mass Emission Rates using EPA Method 19, lbs/hr

C CO 

## = exhaust CO concentration, ppmv = 7.12 C THC 

## = exhaust THC concentration, ppmv = 1.56 C propyl 

## = exhaust propylene concentration (direct), ppmv = 1.57 QSd = stack flow rate, DSCF/hr = 2.07E+07 MWCO = molecular weight of CO = 28 MWTHC = molecular weight of THC as C3H6 = 42 MWpropyl = molecular weight of propylene = 42 K = gas constant, SCF/lb-mole at EPA STP = 385.3

E"X" = mass emssion rate of "X", lbs/hour

ECO = 10.73 lbs/hr ETHC = 3.52 lbs/hr Epropyl = 3.56 lbs/hr (direct)

Propylene Destruction Rate Efficiency Calculation

MPI = Mass of propylene to flare, lbs/hr = 6122.8 MPO = Mass of propylene in exhaust, lbs/hr = 3.56

MPI - MPO MPI

DRE % = 99.94%

Combustion Efficiency

C CO 

## = exhaust CO concentration, ppmv = 7.12 C CO2 

## = exhaust CO2 concentration, ppmv = 8600 C THC 

## = exhaust THC concentration, ppmv = 1.56

C CO2 

## C CO2 

## + C CO 

## +C THC



## CE % = 99.90% x 100 =

DRE % = C"X" * QS * 10 -6 

## * MW"X" / K

CE % = x 100

#  

# 















 

# Appendix C: Instrumental Quality Assurance







 

### Initial Cal Error Instrumantal QA

Testing by TRC, Austin, Texas 199009 November 19
Initial Calibration Error Test Date/Time: 11/19/2013 7:33:51 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Zero ID: Low ID: Mid ID: High ID:
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 CC427175 X02NI99P15A3LE2 X02NI99P15A51P7

Calibration Error Results
Channel: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200 200 25 25 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Zero Ref: 0.000 0.000 0.000 0.000 0 Zero Cal: -0.043 0.124 0.044 -0.024 -0.001
Zero Error: 0.000 0.001 0.002 -0.001 0.00%

Low Ref: 30.35 Low Cal: 30.416
Low Error: 0.20%

Mid Ref: 51.010 49.660 9.969 9.950 50.2 Mid Cal: 51.798 50.545 10.059 9.989 49.709 Mid Error: 0.008 0.009 0.004 0.002 -1.00%

High Ref: 100.100 100.100 20.000 19.600 84.96 High Cal: 99.994 101.116 20.039 19.750 85.063 High Error: -0.10% 1.00% 0.20% 0.80% 0.10%

Cal Result: PASSED PASSED PASSED PASSED PASSED

### Initial System Bias Instrumantal QA

Testing by TRC, Austin, Texas 199009 November 19 Initial System Bias Check Date/Time: 11/19/2013 7:43:45 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: 0.750 0.058 0.107 0.117 0.055
Low Bias: 0.008 -0.001 0.003 0.007

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 51.294 50.560 9.904 9.941 50.081 Upscale Bias -0.50% 0.00% -0.80% -0.20%

Bias Result: PASSED PASSED PASSED PASSED PASSED

### Run S1 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 1
Run S1 Final Bias and Drift Check Date/Time: 11/19/2013 9:43:31 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: 0.844 -0.295 0.098 0.074 -0.91
Low Bias: 0.009 -0.004 0.003 0.005

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 51.901 50.622 10.071 9.894 49.147 Upscale Bias 0.001 0.001 0.001 -0.005

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.001 -0.004 0.000 -0.002 -1.00% Mid Drift: 0.006 0.001 0.008 -0.002 -0.90% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 1 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.750 0.058 0.107 0.117 Low final: 0.844 -0.295 0.098 0.074 Mid Init: 51.294 50.560 9.904 9.941 Mid Final: 51.901 50.622 10.071 9.894 Run Avg: 12.277 7.151 19.634 0.944 1.558
Co: 0.797 -0.119 0.103 0.095
Cm: 51.598 50.591 9.987 9.918
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 11.527 7.119 19.698 0.86

### Run S2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 2
Run S2 Final Bias and Drift Check Date/Time: 11/19/2013 10:12:51 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: 0.174 -0.378 0.102 0.057 -0.187
Low Bias: 0.002 -0.005 0.003 0.004

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 51.089 50.295 10.053 9.910 50.362 Upscale Bias -0.007 -0.002 0.000 -0.004

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.007 -0.001 0.000 -0.001 0.70% Mid Drift: -0.008 -0.003 -0.001 0.001 1.20% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 2 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.844 -0.295 0.098 0.074 Low final: 0.174 -0.378 0.102 0.057 Mid Init: 51.901 50.622 10.071 9.894 Mid Final: 51.089 50.295 10.053 9.910 Run Avg: 12.645 1.338 19.671 0.904 0.3
Co: 0.509 -0.337 0.100 0.065
Cm: 51.495 50.459 10.062 9.902
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 12.142 1.638 19.585 0.848

### Run S3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 3
Run S3 Final Bias and Drift Check Date/Time: 11/19/2013 12:07:02 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: -0.023 -0.549 0.082 0.052 -0.671
Low Bias: 0.000 -0.007 0.002 0.004

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 50.177 50.041 10.015 9.879 49.079 Upscale Bias -0.016 -0.005 -0.002 -0.006

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.002 -0.002 -0.001 0.000 -0.50% Mid Drift: -0.009 -0.003 -0.002 -0.002 -1.30% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 3 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.174 -0.378 0.102 0.057 Low final: -0.023 -0.549 0.082 0.052 Mid Init: 51.089 50.295 10.053 9.910 Mid Final: 50.177 50.041 10.015 9.879 Run Avg: 2.169 9.718 20.209 0.514 9.305
Co: 0.075 -0.464 0.092 0.055
Cm: 50.633 50.168 10.034 9.894
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 2.113 9.986 20.171 0.465

### Run S4 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 4
Run S4 Final Bias and Drift Check Date/Time: 11/19/2013 2:01:42 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: 0.290 -0.529 0.092 0.061 -0.482
Low Bias: 0.003 -0.007 0.002 0.004

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 50.858 50.107 10.013 9.856 49.694 Upscale Bias -0.009 -0.004 -0.002 -0.007

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.003 0.000 0.000 0.000 0.20% Mid Drift: 0.007 0.001 0.000 -0.001 0.60% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 4 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: -0.023 -0.549 0.082 0.052 Low final: 0.290 -0.529 0.092 0.061 Mid Init: 50.177 50.041 10.015 9.879 Mid Final: 50.858 50.107 10.013 9.856 Run Avg: 8.638 5.559 19.419 0.981 2.526
Co: 0.133 -0.539 0.087 0.057
Cm: 50.518 50.074 10.014 9.867
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 8.61 5.983 19.412 0.938

### Run S5 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 5
Run S5 Final Bias and Drift Check Date/Time: 11/19/2013 2:53:17 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: -0.071 -0.551 0.090 0.073 -0.475
Low Bias: 0.000 -0.007 0.002 0.005

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 50.105 49.883 9.989 9.830 50.509 Upscale Bias -0.017 -0.007 -0.003 -0.008

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.004 0.000 0.000 0.001 0.00% Mid Drift: -0.008 -0.002 -0.001 -0.001 0.80% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 5 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.290 -0.529 0.092 0.061 Low final: -0.071 -0.551 0.090 0.073 Mid Init: 50.858 50.107 10.013 9.856 Mid Final: 50.105 49.883 9.989 9.830 Run Avg: 3.347 30.694 19.976 0.620 21.347
Co: 0.109 -0.540 0.091 0.067
Cm: 50.482 49.995 10.001 9.843
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 3.279 30.694 20.003 0.563

### Run S6 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 6
Run S6 Final Bias and Drift Check Date/Time: 11/19/2013 3:20:35 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: 0.167 -0.545 0.071 0.045 -0.456
Low Bias: 0.002 -0.007 0.001 0.004

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 51.404 49.925 10.015 9.806 50.39 Upscale Bias -0.004 -0.006 -0.002 -0.009

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.002 0.000 -0.001 -0.001 0.00% Mid Drift: 0.013 0.000 0.001 -0.001 -0.10% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 6 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: -0.071 -0.551 0.090 0.073 Low final: 0.167 -0.545 0.071 0.045 Mid Init: 50.105 49.883 9.989 9.830 Mid Final: 51.404 49.925 10.015 9.806 Run Avg: 4.524 4.307 19.904 0.707 0.689
Co: 0.048 -0.548 0.080 0.059
Cm: 50.754 49.904 10.002 9.818
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 4.503 4.779 19.918 0.661

### Run P1H-1 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 19 Run 7
Run P1H-1 Final Bias and Drift Check Date/Time: 11/19/2013 4:09:40 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: -0.043 0.124 0.044 -0.024 Low Sys: 0.314 -0.532 0.107 0.044 -0.406
Low Bias: 0.004 -0.007 0.003 0.003

Upscale Cal: 51.798 50.545 10.059 9.989 Upscale Sys: 50.889 50.157 10.018 9.812 50.705 Upscale Bias -0.009 -0.004 -0.002 -0.009

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.001 0.000 0.002 0.000 0.10% Mid Drift: -0.005 0.002 0.000 0.000 0.30% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 7 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.167 -0.545 0.071 0.045 Low final: 0.314 -0.532 0.107 0.044 Mid Init: 51.404 49.925 10.015 9.806 Mid Final: 50.889 50.157 10.018 9.812 Run Avg: 7.728 0.498 19.778 0.795 0.011
Co: 0.241 -0.538 0.089 0.045
Cm: 51.147 50.041 10.016 9.809
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 7.503 1.017 19.771 0.765

### Initial Cal Error Instrumantal QA

Testing by TRC, Austin, Texas 199009 November 20
Initial Calibration Error Test Date/Time: 11/20/2013 11:57:34 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Zero ID: Low ID: Mid ID: High ID:
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 CC427175 X02NI99P15A3LE2 X02NI99P15A51P7

Calibration Error Results
Channel: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200 200 25 25 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Zero Ref: 0.000 0.000 0.000 0.000 0 Zero Cal: 0.045 0.058 0.064 -0.001 -0.666
Zero Error: 0.000 0.001 0.003 0.000 -0.70%

Low Ref: 30.35 Low Cal: 30.7
Low Error: 1.20%

Mid Ref: 51.010 49.660 9.969 9.950 50.2 Mid Cal: 51.991 50.105 9.963 10.131 49.707 Mid Error: 0.010 0.004 0.000 0.009 -1.00%

High Ref: 100.100 100.100 20.000 19.600 84.96 High Cal: 100.868 99.663 19.812 19.525 85.157 High Error: 0.80% -0.40% -0.90% -0.40% 0.20%

Cal Result: PASSED PASSED PASSED PASSED PASSED

### Initial System Bias Instrumantal QA

Testing by TRC, Austin, Texas 199009 November 20 Initial System Bias Check Date/Time: 11/20/2013 12:04:42 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 0.932 -0.466 0.073 0.063 -0.737
Low Bias: 0.009 -0.005 0.000 0.003

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 50.157 49.787 9.944 10.084 50.303 Upscale Bias -1.80% -0.30% -0.10% -0.20%

Bias Result: PASSED PASSED PASSED PASSED PASSED

### Run P1H-2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 20 Run 1
Run P1H-2 Final Bias and Drift Check Date/Time: 11/20/2013 2:33:25 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 0.823 0.027 0.112 0.048 0.07
Low Bias: 0.008 0.000 0.002 0.003

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 50.940 52.697 9.981 9.922 52.986 Upscale Bias -0.011 0.026 0.001 -0.011

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.001 0.005 0.002 -0.001 0.80% Mid Drift: 0.008 0.029 0.002 -0.008 2.70% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 1 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.932 -0.466 0.073 0.063 Low final: 0.823 0.027 0.112 0.048 Mid Init: 50.157 49.787 9.944 10.084 Mid Final: 50.940 52.697 9.981 9.922 Run Avg: 4.077 1.006 20.081 0.510 0.794
Co: 0.877 -0.219 0.093 0.055
Cm: 50.548 51.242 9.963 10.003
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 3.286 1.182 20.189 0.455

### Run P1L-1 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 20 Run 2
Run P1L-1 Final Bias and Drift Check Date/Time: 11/20/2013 3:23:03 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 1.175 0.132 0.077 0.045 -0.022
Low Bias: 0.011 0.001 0.001 0.002

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 51.367 50.173 10.076 10.020 50.364 Upscale Bias -0.006 0.001 0.006 -0.006

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.004 0.001 -0.002 0.000 -0.10% Mid Drift: 0.004 -0.025 0.005 0.005 -2.60% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 2 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.823 0.027 0.112 0.048 Low final: 1.175 0.132 0.077 0.045 Mid Init: 50.940 52.697 9.981 9.922 Mid Final: 51.367 50.173 10.076 10.020 Run Avg: 6.705 1.276 19.664 0.853 0.543
Co: 0.999 0.080 0.094 0.047
Cm: 51.153 51.435 10.028 9.971
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 5.803 1.157 19.638 0.808

### Run P2H-1 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 20 Run 3
Run P2H-1 Final Bias and Drift Check Date/Time: 11/20/2013 4:13:29 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 0.540 0.126 0.112 0.068 -0.328
Low Bias: 0.005 0.001 0.002 0.003

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 50.670 49.958 10.086 10.004 49.157 Upscale Bias -0.013 -0.001 0.006 -0.006

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.006 0.000 0.002 0.001 -0.30% Mid Drift: -0.007 -0.002 0.000 -0.001 -1.20% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 3 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 1.175 0.132 0.077 0.045 Low final: 0.540 0.126 0.112 0.068 Mid Init: 51.367 50.173 10.076 10.020 Mid Final: 50.670 49.958 10.086 10.004 Run Avg: 16.107 1.849 19.412 1.067 0.422
Co: 0.858 0.129 0.095 0.056
Cm: 51.018 50.065 10.081 10.012
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 15.508 1.71 19.284 1.01

### Run P2H-1b Instrumental QA

Testing by TRC, Austin, Texas 199009 November 20 Run 4 Run P2H-1b Final Bias and Drift Check Date/Time: 11/20/2013 5:01:37 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 1.022 0.117 0.101 0.076 -0.083
Low Bias: 0.010 0.001 0.002 0.004

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 50.659 50.010 10.084 10.030 50.058 Upscale Bias -0.013 -0.001 0.006 -0.005

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.005 0.000 -0.001 0.000 0.20% Mid Drift: 0.000 0.001 0.000 0.001 0.90% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 4 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.540 0.126 0.112 0.068 Low final: 1.022 0.117 0.101 0.076 Mid Init: 50.670 49.958 10.086 10.004 Mid Final: 50.659 50.010 10.084 10.030 Run Avg: 16.942 1.898 19.177 1.227 0.376
Co: 0.781 0.121 0.107 0.072
Cm: 50.664 49.984 10.085 10.017
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 16.526 1.77 19.052 1.156

### Run P2L-1(b) Instrumental QA

Testing by TRC, Austin, Texas 199009 November 20 Run 5 Run P2L-1(b) Final Bias and Drift Check Date/Time: 11/20/2013 6:01:44 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 1.029 0.058 0.093 0.071 -0.153
Low Bias: 0.010 0.000 0.001 0.004

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 51.137 49.791 10.065 10.034 50.098 Upscale Bias -0.009 -0.003 0.005 -0.005

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.000 -0.001 0.000 0.000 -0.10% Mid Drift: 0.005 -0.002 -0.001 0.000 0.00% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 5 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 1.022 0.117 0.101 0.076 Low final: 1.029 0.058 0.093 0.071 Mid Init: 50.659 50.010 10.084 10.030 Mid Final: 51.137 49.791 10.065 10.034 Run Avg: 10.106 7.615 19.760 0.861 1.833
Co: 1.025 0.087 0.097 0.073
Cm: 50.898 49.901 10.075 10.032
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 9.288 7.505 19.646 0.787

### Run P3H-1 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 20 Run 6
Run P3H-1 Final Bias and Drift Check Date/Time: 11/20/2013 7:42:28 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A3LE2

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.045 0.058 0.064 -0.001 Low Sys: 0.750 0.010 0.076 0.063 0.282
Low Bias: 0.007 0.000 0.001 0.003

Upscale Cal: 51.991 50.105 9.963 10.131 Upscale Sys: 51.468 49.719 10.067 10.034 51.606 Upscale Bias -0.005 -0.004 0.005 -0.005

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.003 0.000 -0.001 0.000 0.40% Mid Drift: 0.003 -0.001 0.000 0.000 1.50% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 6 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 1.029 0.058 0.093 0.071 Low final: 0.750 0.010 0.076 0.063 Mid Init: 51.137 49.791 10.065 10.034 Mid Final: 51.468 49.719 10.067 10.034 Run Avg: 15.719 8.405 18.854 1.397 1.725
Co: 0.889 0.034 0.084 0.067
Cm: 51.302 49.755 10.066 10.034
Coa: 0.000 0.000 0.000 0.000
Cma: 51.010 49.660 9.969 9.950 Corrected: 15.005 8.361 18.746 1.327

### Initial Cal Error Instrumantal QA

Testing by TRC, Austin, Texas 199009 November 21
Initial Calibration Error Test Date/Time: 11/21/2013 6:59:13 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Zero ID: Low ID: Mid ID: High ID:
NOx CC351249 CC335400 CC403079
CO CC351249 CC335400 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 CC427175 X02NI99P15A3LE2 X02NI99P15A51P7

Calibration Error Results
Channel: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200 200 25 25 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Zero Ref: 0.000 0.000 0.000 0.000 0 Zero Cal: 0.106 0.086 0.056 0.016 -0.144
Zero Error: 0.001 0.001 0.003 0.001 -0.10%

Low Ref: 30.35 Low Cal: 30.438
Low Error: 0.30%

Mid Ref: 51.010 49.660 9.969 9.950 50.2 Mid Cal: 50.635 50.431 10.088 10.169 50.354 Mid Error: -0.004 0.008 0.006 0.011 0.30%

High Ref: 100.100 100.100 20.000 19.600 84.96 High Cal: 100.349 99.970 20.074 19.586 85.09 High Error: 0.20% -0.10% 0.40% -0.10% 0.20%

Cal Result: PASSED PASSED PASSED PASSED PASSED

### Initial System Bias Instrumantal QA

Testing by TRC, Austin, Texas 199009 November 21 Initial System Bias Check Date/Time: 11/21/2013 7:07:08 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 1.140 -0.608 0.088 0.066 -0.005
Low Bias: 0.010 -0.007 0.002 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 101.043 100.756 10.068 10.116 84.656 Upscale Bias 0.70% 0.80% -0.10% -0.30%

Bias Result: PASSED PASSED PASSED PASSED PASSED

### Run P3L-1b Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 1 Run P3L-1b Final Bias and Drift Check Date/Time: 11/21/2013 9:30:36 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 1.026 -0.470 0.091 0.081 -0.61
Low Bias: 0.009 -0.006 0.002 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.211 99.810 10.096 10.102 86.282 Upscale Bias -0.001 -0.002 0.000 -0.003

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.001 0.001 0.000 0.001 -0.60% Mid Drift: -0.008 -0.009 0.001 -0.001 1.60% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 1 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 1.140 -0.608 0.088 0.066 Low final: 1.026 -0.470 0.091 0.081 Mid Init: 101.043 100.756 10.068 10.116 Mid Final: 100.211 99.810 10.096 10.102 Run Avg: 13.035 4.814 18.959 1.327 0.16
Co: 1.083 -0.539 0.090 0.074
Cm: 100.627 100.283 10.082 10.109
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 12.018 5.315 18.825 1.242

### Run P1L-2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 2
Run P1L-2 Final Bias and Drift Check Date/Time: 11/21/2013 10:08:32 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.553 -0.523 0.074 0.074 -0.222
Low Bias: 0.004 -0.006 0.001 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 99.814 100.406 10.084 10.118 86.165 Upscale Bias -0.005 0.004 0.000 -0.003

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.005 -0.001 -0.001 0.000 0.40% Mid Drift: -0.004 0.006 -0.001 0.001 -0.10% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 2 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 1.026 -0.470 0.091 0.081 Low final: 0.553 -0.523 0.074 0.074 Mid Init: 100.211 99.810 10.096 10.102 Mid Final: 99.814 100.406 10.084 10.118 Run Avg: 9.355 1.522 19.220 1.356 -0.386
Co: 0.790 -0.497 0.082 0.078
Cm: 100.012 100.108 10.090 10.110
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 8.641 2.008 19.064 1.268

### Run P2H-2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 3
Run P2H-2 Final Bias and Drift Check Date/Time: 11/21/2013 11:20:51 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.485 -0.529 0.085 0.061 0.456
Low Bias: 0.004 -0.006 0.001 0.002

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.993 99.770 10.107 10.104 86.528 Upscale Bias 0.006 -0.002 0.001 -0.003

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.001 0.000 0.001 -0.001 0.70% Mid Drift: 0.012 -0.006 0.001 -0.001 0.40% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 3 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.553 -0.523 0.074 0.074 Low final: 0.485 -0.529 0.085 0.061 Mid Init: 99.814 100.406 10.084 10.118 Mid Final: 100.993 99.770 10.107 10.104 Run Avg: 10.740 2.486 19.752 0.894 0.39
Co: 0.519 -0.526 0.079 0.067
Cm: 100.403 100.088 10.096 10.111
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 10.243 2.997 19.58 0.819

### Run P2L-2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 4
Run P2L-2 Final Bias and Drift Check Date/Time: 11/21/2013 11:55:51 AM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.463 -0.475 0.097 0.065 0.448
Low Bias: 0.004 -0.006 0.002 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.833 99.943 10.094 10.098 85.22 Upscale Bias 0.005 0.000 0.000 -0.004

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.000 0.001 0.001 0.000 0.00% Mid Drift: -0.002 0.002 -0.001 0.000 -1.30% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 4 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.485 -0.529 0.085 0.061 Low final: 0.463 -0.475 0.097 0.065 Mid Init: 100.993 99.770 10.107 10.104 Mid Final: 100.833 99.943 10.094 10.098 Run Avg: 9.520 6.889 19.850 0.843 1.837
Co: 0.474 -0.502 0.091 0.063
Cm: 100.913 99.857 10.100 10.101
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 9.015 7.372 19.679 0.774

### Run P3H-2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 5
Run P3H-2 Final Bias and Drift Check Date/Time: 11/21/2013 1:10:18 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.463 -0.527 0.089 0.053 -0.091
Low Bias: 0.004 -0.006 0.002 0.002

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 101.146 99.696 10.094 10.070 85.004 Upscale Bias 0.008 -0.003 0.000 -0.005

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.000 -0.001 0.000 -0.001 -0.50% Mid Drift: 0.003 -0.002 0.000 -0.001 -0.20% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 5 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.463 -0.475 0.097 0.065 Low final: 0.463 -0.527 0.089 0.053 Mid Init: 100.833 99.943 10.094 10.098 Mid Final: 101.146 99.696 10.094 10.070 Run Avg: 8.448 3.244 19.697 0.884 1.204
Co: 0.463 -0.501 0.093 0.059
Cm: 100.990 99.819 10.094 10.084
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 7.951 3.736 19.542 0.819

### Run P3L-2 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 6
Run P3L-2 Final Bias and Drift Check Date/Time: 11/21/2013 1:41:26 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.647 -0.529 0.088 0.082 0.613
Low Bias: 0.005 -0.006 0.002 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.208 99.924 10.090 10.109 85.391 Upscale Bias -0.001 0.000 0.000 -0.003

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.002 0.000 0.000 0.001 0.70% Mid Drift: -0.009 0.002 0.000 0.002 0.40% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 6 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.463 -0.527 0.089 0.053 Low final: 0.647 -0.529 0.088 0.082 Mid Init: 101.146 99.696 10.094 10.070 Mid Final: 100.208 99.924 10.090 10.109 Run Avg: 9.119 3.377 19.523 0.992 1.095
Co: 0.555 -0.528 0.088 0.067
Cm: 100.677 99.810 10.092 10.089
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 8.562 3.896 19.367 0.918

### Run P1H-3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 7
Run P1H-3 Final Bias and Drift Check Date/Time: 11/21/2013 2:19:06 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.492 -0.519 0.054 0.029 0.187
Low Bias: 0.004 -0.006 0.000 0.001

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 101.280 100.119 10.104 10.104 84.584 Upscale Bias 0.009 0.001 0.001 -0.003

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.002 0.000 -0.002 -0.003 -0.40% Mid Drift: 0.011 0.002 0.001 0.000 -0.80% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 7 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.647 -0.529 0.088 0.082 Low final: 0.492 -0.519 0.054 0.029 Mid Init: 100.208 99.924 10.090 10.109 Mid Final: 101.280 100.119 10.104 10.104 Run Avg: 10.989 0.879 19.242 1.333 0.851
Co: 0.569 -0.524 0.071 0.055
Cm: 100.744 100.021 10.097 10.106
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 10.412 1.397 19.061 1.265

### Run P2L-3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 8
Run P2L-3 Final Bias and Drift Check Date/Time: 11/21/2013 3:03:59 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.987 -0.525 0.080 0.069 -0.253
Low Bias: 0.009 -0.006 0.001 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.804 99.840 10.084 10.122 84.352 Upscale Bias 0.005 -0.001 0.000 -0.002

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.005 0.000 0.001 0.002 -0.40% Mid Drift: -0.005 -0.003 -0.001 0.001 -0.20% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 8 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.492 -0.519 0.054 0.029 Low final: 0.987 -0.525 0.080 0.069 Mid Init: 101.280 100.119 10.104 10.104 Mid Final: 100.804 99.840 10.084 10.122 Run Avg: 13.522 6.904 19.456 1.092 1.062
Co: 0.739 -0.522 0.067 0.049
Cm: 101.042 99.979 10.094 10.113
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 12.757 7.396 19.277 1.032

### Run P3L-3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 9
Run P3L-3 Final Bias and Drift Check Date/Time: 11/21/2013 3:31:16 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.483 -0.586 0.083 0.072 0.224
Low Bias: 0.004 -0.007 0.001 0.003

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.721 99.779 10.089 10.142 85.034 Upscale Bias 0.004 -0.002 0.000 -0.001

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.005 -0.001 0.000 0.000 0.50% Mid Drift: -0.001 -0.001 0.000 0.001 0.70% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 9 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.987 -0.525 0.080 0.069 Low final: 0.483 -0.586 0.083 0.072 Mid Init: 100.804 99.840 10.084 10.122 Mid Final: 100.721 99.779 10.089 10.142 Run Avg: 13.082 6.561 18.937 1.372 1.268
Co: 0.735 -0.556 0.081 0.070
Cm: 100.763 99.810 10.086 10.132
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 12.356 7.098 18.788 1.287

### Run P3H-3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 10
Run P3H-3 Final Bias and Drift Check Date/Time: 11/21/2013 3:59:39 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.400 -0.540 0.090 0.092 0.127
Low Bias: 0.003 -0.006 0.002 0.004

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 100.154 99.211 10.098 10.164 85.315 Upscale Bias -0.002 -0.008 0.001 0.000

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.001 0.000 0.000 0.001 -0.10% Mid Drift: -0.006 -0.006 0.000 0.001 0.30% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 10 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.483 -0.586 0.083 0.072 Low final: 0.400 -0.540 0.090 0.092 Mid Init: 100.721 99.779 10.089 10.142 Mid Final: 100.154 99.211 10.098 10.164 Run Avg: 10.871 8.228 19.385 1.075 1.916
Co: 0.441 -0.563 0.087 0.082
Cm: 100.437 99.495 10.094 10.153
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 10.441 8.795 19.225 0.981

### Run P2H-3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 11
Run P2H-3 Final Bias and Drift Check Date/Time: 11/21/2013 4:27:25 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.555 -0.525 0.079 0.048 0.047
Low Bias: 0.004 -0.006 0.001 0.002

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 101.282 99.498 10.118 10.147 84.357 Upscale Bias 0.009 -0.005 0.002 -0.001

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: 0.002 0.000 -0.001 -0.002 -0.10% Mid Drift: 0.011 0.003 0.001 -0.001 -1.00% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 11 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.400 -0.540 0.090 0.092 Low final: 0.555 -0.525 0.079 0.048 Mid Init: 100.154 99.211 10.098 10.164 Mid Final: 101.282 99.498 10.118 10.147 Run Avg: 12.040 4.781 19.597 1.011 0.967
Co: 0.477 -0.533 0.085 0.070
Cm: 100.718 99.355 10.108 10.155
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 11.546 5.325 19.406 0.928

### Run P1L-3 Instrumental QA

Testing by TRC, Austin, Texas 199009 November 21 Run 12
Run P1L-3 Final Bias and Drift Check Date/Time: 11/21/2013 4:57:14 PM Result: PASS

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

Reference Cylinder IDs
Low ID Upscale ID Span ID
NOx CC351249 CC403079 CC403079
CO CC351249 CC403079 CC403079
O2 CC335400 CC351249 EB0045768
CO2 CC335400 CC351249 EB0045768 C3H8-Propyl CC351249 X02NI99P15A51P7

System Bias Check Results Analyte: NOx CO O2 CO2 C3H8-Propyl
Units: ppm ppm % % ppm Span: 100.100 100.100 20.000 19.600 100 Range: 200.000 200.000 25.000 25.000 100 Method: EPA 7E EPA 7E EPA 7E EPA 7E EPA 25A

Low Cal: 0.106 0.086 0.056 0.016 Low Sys: 0.395 -0.519 0.078 0.061 -0.279
Low Bias: 0.003 -0.006 0.001 0.002

Upscale Cal: 100.349 99.970 10.088 10.169 Upscale Sys: 101.589 99.777 10.122 10.152 84.487 Upscale Bias 0.012 -0.002 0.002 -0.001

Bias Result: PASSED PASSED PASSED PASSED PASSED

System Bias Drift Results
Low Drift: -0.002 0.000 0.000 0.001 -0.30% Mid Drift: 0.003 0.003 0.000 0.000 0.10% Drift Result: PASSED PASSED PASSED PASSED PASSED

Cal Result: OK OK OK OK OK

Test Run 12 Bias Correction Calculations:
NOx CO O2 CO2 C3H8-Propyl
Low init: 0.555 -0.525 0.079 0.048 Low final: 0.395 -0.519 0.078 0.061 Mid Init: 101.282 99.498 10.118 10.147 Mid Final: 101.589 99.777 10.122 10.152 Run Avg: 5.861 1.061 19.955 0.870 0.468
Co: 0.475 -0.522 0.078 0.055
Cm: 101.436 99.638 10.120 10.149
Coa: 0.000 0.000 0.000 0.000
Cma: 100.100 100.100 9.969 9.950 Corrected: 5.34 1.582 19.733 0.803

#  

# 















 

# Appendix D: Datalog Records and Chromatograms 





 

### Run S1 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run S1
Start: 11/19/2013 9:18:55 AM End: 11/19/2013 9:38:55 AM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 9:19:55 AM 1min avg: 10.154 7.485 19.520 1.024 0.376
9:20:55 AM 1min avg: 10.148 5.376 19.722 0.890 1.486
9:21:55 AM 1min avg: 14.289 8.979 18.929 1.439 2.440
9:22:55 AM 1min avg: 14.182 9.542 19.025 1.337 2.099
9:23:55 AM 1min avg: 17.549 9.870 19.286 1.152 1.753
9:24:55 AM 1min avg: 12.625 5.722 20.119 0.654 0.769
9:25:55 AM 1min avg: 9.961 5.574 19.605 0.941 0.286
9:26:55 AM 1min avg: 7.076 2.774 20.434 0.429 1.633
9:27:55 AM 1min avg: 13.429 9.586 18.936 1.383 2.692
9:28:55 AM 1min avg: 12.671 6.940 19.875 0.806 -0.052
9:29:55 AM 1min avg: 10.035 4.296 19.773 0.834 2.045
9:30:55 AM 1min avg: 13.290 7.056 20.046 0.712 1.191
9:31:55 AM 1min avg: 10.219 7.134 19.369 1.120 2.429
9:32:55 AM 1min avg: 13.386 10.491 19.298 1.118 1.953
9:33:55 AM 1min avg: 13.523 7.678 19.748 0.889 1.466
9:34:55 AM 1min avg: 10.092 5.554 20.211 0.571 -0.165
9:35:55 AM 1min avg: 4.708 1.734 20.445 0.403 0.704
9:36:55 AM 1min avg: 14.929 6.846 19.566 0.994 2.750
9:37:55 AM 1min avg: 16.336 10.424 19.190 1.200 3.312
9:38:55 AM 1min avg: 16.933 9.954 19.576 0.977 2.001
9:38:55 AM Test Avgs: 12.277 7.151 19.634 0.944 1.558

### Run S2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run S2
Start: 11/19/2013 9:45:00 AM End: 11/19/2013 10:05:01 AM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 9:46:00 AM 1min avg: 12.228 1.070 19.635 0.908 -0.464
9:47:00 AM 1min avg: 15.192 1.336 19.575 0.967 -0.397
9:48:00 AM 1min avg: 12.773 1.333 19.927 0.733 -0.448
9:49:00 AM 1min avg: 13.123 1.490 19.229 1.177 -0.098
9:50:00 AM 1min avg: 16.778 1.831 19.211 1.199 0.419
9:51:00 AM 1min avg: 16.299 1.578 19.402 1.073 0.368
9:52:00 AM 1min avg: 9.547 0.947 20.247 0.543 0.397
9:53:00 AM 1min avg: 8.067 0.826 20.133 0.635 0.337
9:54:00 AM 1min avg: 4.705 0.606 20.478 0.368 0.560
9:55:00 AM 1min avg: 14.435 1.643 19.208 1.185 0.577
9:56:00 AM 1min avg: 15.722 1.765 19.214 1.196 0.337
9:57:00 AM 1min avg: 14.990 1.760 19.242 1.181 0.358
9:58:00 AM 1min avg: 11.582 1.051 19.881 0.803 0.261
9:59:00 AM 1min avg: 15.895 1.262 19.375 1.092 0.584
10:00:00 AM 1min avg: 16.953 1.782 19.352 1.092 1.134
10:01:00 AM 1min avg: 18.801 2.017 19.665 0.976 0.613
10:02:00 AM 1min avg: 7.888 1.253 19.815 0.828 0.341
10:03:00 AM 1min avg: 6.233 0.591 20.796 0.178 0.304
10:04:00 AM 1min avg: 7.019 0.994 19.571 0.929 0.392
10:05:00 AM 1min avg: 14.670 1.633 19.465 1.014 0.434
10:05:01 AM Test Avgs: 12.645 1.338 19.671 0.904 0.300

### Run S3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run S3
Start: 11/19/2013 11:29:00 AM End: 11/19/2013 12:01:01 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 11:30:00 AM 1min avg: 1.710 9.653 20.131 0.571 10.631
11:31:00 AM 1min avg: 2.178 14.209 19.820 0.743 10.925
11:32:00 AM 1min avg: 3.143 11.245 20.184 0.543 7.587
11:33:00 AM 1min avg: 2.489 12.785 19.887 0.710 8.342
11:34:00 AM 1min avg: 2.967 12.430 20.123 0.586 9.248
11:35:00 AM 1min avg: 2.465 12.952 20.189 0.558 6.162
11:36:00 AM 1min avg: 1.602 7.412 20.328 0.462 14.189
11:37:00 AM 1min avg: 1.039 5.490 20.723 0.195 30.427
11:38:00 AM 1min avg: 0.012 0.108 20.861 0.082 8.899
11:39:00 AM 1min avg: -0.049 0.109 20.883 0.081 0.918
11:40:00 AM 1min avg: -0.230 0.147 20.899 0.080 1.337
11:41:00 AM 1min avg: -0.254 0.164 20.864 0.079 29.781
11:42:00 AM 1min avg: -0.042 2.115 20.443 0.336 12.701
11:43:00 AM 1min avg: 4.063 18.388 19.432 0.998 7.310
11:44:00 AM 1min avg: 2.719 9.453 20.357 0.449 7.815
11:45:00 AM 1min avg: 1.567 9.563 20.417 0.409 2.884
11:46:00 AM 1min avg: 1.237 7.115 20.261 0.471 8.785
11:47:00 AM 1min avg: 2.748 14.666 19.972 0.683 6.467
11:48:00 AM 1min avg: 2.964 11.790 19.868 0.700 10.056
11:49:00 AM 1min avg: 2.797 17.313 19.904 0.683 10.660
11:50:00 AM 1min avg: 4.269 14.043 19.911 0.700 10.853
11:51:00 AM 1min avg: 2.392 10.854 20.393 0.423 3.741
11:52:00 AM 1min avg: 0.318 1.955 20.819 0.144 0.532
11:53:00 AM 1min avg: 1.332 7.363 19.912 0.646 11.505
11:54:00 AM 1min avg: 4.159 15.437 19.844 0.750 6.309
11:55:00 AM 1min avg: 2.319 9.361 20.558 0.324 7.087
11:56:00 AM 1min avg: 1.558 5.620 20.353 0.415 6.406
11:57:00 AM 1min avg: 4.695 14.037 19.849 0.757 9.277
11:58:00 AM 1min avg: 3.158 11.280 19.945 0.664 10.534
11:59:00 AM 1min avg: 3.375 15.043 19.930 0.699 8.772
12:00:00 PM 1min avg: 3.853 15.785 19.652 0.852 9.261
12:01:00 PM 1min avg: 2.861 13.074 19.972 0.668 8.359
12:01:01 PM Test Avgs: 2.169 9.718 20.209 0.514 9.305

### Run S4 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run S4
Start: 11/19/2013 1:36:01 PM End: 11/19/2013 1:56:01 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 1:37:01 PM 1min avg: 8.805 5.067 19.180 1.127 1.449
1:38:01 PM 1min avg: 11.953 6.503 19.216 1.134 2.700
1:39:01 PM 1min avg: 5.701 5.044 19.677 0.796 0.709
1:40:01 PM 1min avg: 7.205 3.509 19.784 0.760 0.657
1:41:01 PM 1min avg: 9.858 4.192 18.824 1.335 1.857
1:42:01 PM 1min avg: 12.111 7.185 19.619 0.905 1.646
1:43:01 PM 1min avg: 5.211 3.282 20.399 0.389 6.705
1:44:01 PM 1min avg: 8.398 4.763 19.312 1.051 1.185
1:45:01 PM 1min avg: 7.336 4.739 19.774 0.755 1.702
1:46:01 PM 1min avg: 6.911 5.568 19.118 1.167 0.805
1:47:01 PM 1min avg: 7.842 5.041 19.700 0.799 1.699
1:48:01 PM 1min avg: 9.549 6.076 19.611 0.867 4.180
1:49:01 PM 1min avg: 6.711 4.897 19.434 0.951 2.410
1:50:01 PM 1min avg: 10.829 7.753 18.963 1.266 1.865
1:51:01 PM 1min avg: 9.169 5.814 19.181 1.126 2.784
1:52:01 PM 1min avg: 6.335 5.476 19.775 0.725 4.978
1:53:01 PM 1min avg: 12.173 6.640 18.864 1.366 3.967
1:54:01 PM 1min avg: 6.928 6.890 19.339 1.002 2.951
1:55:01 PM 1min avg: 10.475 7.800 18.948 1.262 1.463
1:56:01 PM 1min avg: 9.263 4.931 19.652 0.842 4.814
1:56:01 PM Test Avgs: 8.638 5.559 19.419 0.981 2.526

### Run S5 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run S5
Start: 11/19/2013 2:18:47 PM End: 11/19/2013 2:47:38 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 2:19:47 PM 1min avg: 4.034 38.593 19.971 0.619 26.935
2:20:47 PM 1min avg: 3.662 35.488 19.625 0.824 31.287
2:21:47 PM 1min avg: 4.449 36.253 20.024 0.601 15.380
2:22:47 PM 1min avg: 4.959 32.585 19.708 0.757 23.552
2:23:47 PM 1min avg: 4.277 36.981 19.800 0.733 16.466
2:24:47 PM 1min avg: 3.777 22.371 20.007 0.588 21.033
2:25:47 PM 1min avg: 3.426 31.400 20.046 0.597 22.274
2:26:47 PM 1min avg: 2.950 36.226 19.787 0.729 29.157
2:27:47 PM 1min avg: 3.266 46.902 19.744 0.759 31.510
2:28:47 PM 1min avg: 2.545 31.814 20.216 0.482 25.990
2:38:37 PM 1min avg: 2.615 28.017 20.356 0.391 18.111
2:39:37 PM 1min avg: 2.241 24.726 19.980 0.614 17.302
2:40:37 PM 1min avg: 2.870 22.330 20.131 0.542 20.472
2:41:37 PM 1min avg: 3.091 33.476 19.801 0.726 16.267
2:42:37 PM 1min avg: 2.727 25.737 20.108 0.554 18.716
2:43:37 PM 1min avg: 2.360 21.238 20.476 0.326 6.886
2:44:37 PM 1min avg: 1.318 10.848 20.382 0.371 16.551
2:45:37 PM 1min avg: 2.941 23.932 20.092 0.549 24.981
2:46:37 PM 1min avg: 4.387 38.881 19.656 0.811 24.471
2:47:37 PM 1min avg: 4.998 36.064 19.602 0.839 19.889
2:47:38 PM Test Avgs: 3.347 30.694 19.976 0.620 21.347

### Run S6 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run S6
Start: 11/19/2013 2:56:01 PM End: 11/19/2013 3:16:02 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 2:57:01 PM 1min avg: 5.548 3.160 19.927 0.722 0.232
2:58:01 PM 1min avg: 3.889 3.690 19.750 0.812 1.034
2:59:01 PM 1min avg: 3.625 5.331 20.030 0.596 1.281
3:00:01 PM 1min avg: 3.742 4.025 20.041 0.623 0.628
3:01:01 PM 1min avg: 5.710 5.788 19.338 1.078 0.231
3:02:01 PM 1min avg: 5.311 3.045 20.132 0.565 0.184
3:03:01 PM 1min avg: 2.712 3.038 19.777 0.764 0.937
3:04:01 PM 1min avg: 4.541 5.217 20.135 0.566 0.278
3:05:01 PM 1min avg: 1.967 1.180 20.412 0.366 0.216
3:06:01 PM 1min avg: 1.904 1.562 20.190 0.481 0.196
3:07:01 PM 1min avg: 5.758 2.063 19.690 0.847 0.669
3:08:01 PM 1min avg: 5.503 7.153 19.988 0.674 0.669
3:09:01 PM 1min avg: 3.624 3.802 19.775 0.787 0.726
3:10:01 PM 1min avg: 4.369 5.671 19.809 0.751 0.985
3:11:01 PM 1min avg: 5.726 4.810 19.922 0.713 0.627
3:12:01 PM 1min avg: 5.894 4.838 19.459 0.986 0.228
3:13:01 PM 1min avg: 7.322 4.557 19.804 0.795 0.882
3:14:01 PM 1min avg: 4.744 6.454 19.545 0.957 2.303
3:15:01 PM 1min avg: 3.975 6.386 20.301 0.437 0.862
3:16:01 PM 1min avg: 4.668 4.389 20.050 0.618 0.608
3:16:02 PM Test Avgs: 4.524 4.307 19.904 0.707 0.689

### Run P1H-1 Datalog Records

Testing by TRC, Austin, Texas 199009 November 19
Run P1H-1
Start: 11/19/2013 3:45:01 PM End: 11/19/2013 4:05:02 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 3:46:01 PM 1min avg: 6.452 0.394 20.235 0.514 0.081
3:47:01 PM 1min avg: 3.951 0.271 20.138 0.529 -0.019
3:48:01 PM 1min avg: 8.024 0.730 19.801 0.762 0.037
3:49:01 PM 1min avg: 8.813 0.476 19.432 1.056 0.032
3:50:01 PM 1min avg: 4.153 0.384 20.260 0.466 -0.025
3:51:01 PM 1min avg: 6.138 0.415 19.995 0.624 0.053
3:52:01 PM 1min avg: 10.556 0.609 19.310 1.132 -0.048
3:53:01 PM 1min avg: 11.904 0.650 19.231 1.133 -0.020
3:54:01 PM 1min avg: 13.203 0.637 18.908 1.379 -0.002
3:55:01 PM 1min avg: 10.557 0.688 19.470 1.026 -0.043
3:56:01 PM 1min avg: 10.010 0.650 19.568 0.933 0.006
3:57:01 PM 1min avg: 10.284 0.649 19.401 1.049 0.026
3:58:01 PM 1min avg: 8.648 0.711 19.955 0.690 0.059
3:59:01 PM 1min avg: 6.018 0.227 20.459 0.353 0.062
4:00:01 PM 1min avg: 1.489 0.279 20.312 0.424 0.044
4:01:01 PM 1min avg: 4.499 0.301 20.383 0.409 0.081
4:02:01 PM 1min avg: 3.947 0.320 19.790 0.772 0.003
4:03:01 PM 1min avg: 9.213 0.669 19.748 0.816 -0.007
4:04:01 PM 1min avg: 9.104 0.519 19.800 0.776 -0.043
4:05:01 PM 1min avg: 7.439 0.381 19.386 1.049 -0.048
4:05:02 PM Test Avgs: 7.728 0.498 19.778 0.795 0.011

### Run P1H-2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 20
Run P1H-2
Start: 11/20/2013 2:09:01 PM End: 11/20/2013 2:29:01 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 2:10:01 PM 1min avg: 7.003 1.370 19.754 0.763 0.920
2:11:01 PM 1min avg: 2.142 1.037 20.277 0.366 0.855
2:12:01 PM 1min avg: 5.958 1.124 19.775 0.728 0.900
2:13:01 PM 1min avg: 3.297 1.033 20.297 0.373 0.839
2:14:01 PM 1min avg: 4.694 1.082 19.930 0.589 0.806
2:15:01 PM 1min avg: 7.290 1.365 19.552 0.865 0.795
2:16:01 PM 1min avg: 9.990 1.314 19.389 0.960 0.787
2:17:01 PM 1min avg: 8.142 1.226 19.573 0.895 0.833
2:18:01 PM 1min avg: 7.952 1.152 19.592 0.828 0.833
2:19:01 PM 1min avg: 2.527 0.884 20.208 0.462 0.833
2:20:01 PM 1min avg: 1.953 0.796 20.487 0.230 0.810
2:21:01 PM 1min avg: 0.678 0.725 20.663 0.089 0.821
2:22:01 PM 1min avg: 0.594 0.717 20.604 0.132 0.831
2:23:01 PM 1min avg: 1.458 0.785 20.410 0.270 0.782
2:24:01 PM 1min avg: 1.932 0.799 20.461 0.230 0.766
2:25:01 PM 1min avg: 4.194 0.944 19.919 0.649 0.714
2:26:01 PM 1min avg: 3.909 0.951 20.009 0.558 0.691
2:27:01 PM 1min avg: 3.586 1.046 20.243 0.426 0.713
2:28:01 PM 1min avg: 2.334 0.884 20.230 0.398 0.700
2:29:01 PM 1min avg: 1.912 0.876 20.246 0.395 0.641
2:29:01 PM Test Avgs: 4.077 1.006 20.081 0.510 0.794

### Run P1L-1 Datalog Records

Testing by TRC, Austin, Texas 199009 November 20
Run P1L-1
Start: 11/20/2013 2:57:01 PM End: 11/20/2013 3:17:01 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 2:58:01 PM 1min avg: 2.837 1.005 20.434 0.281 0.693
2:59:01 PM 1min avg: 1.506 0.894 20.527 0.190 0.594
3:00:01 PM 1min avg: 4.030 1.092 20.056 0.520 0.666
3:01:01 PM 1min avg: 4.024 1.178 20.014 0.568 0.625
3:02:01 PM 1min avg: 4.801 1.419 19.748 0.737 0.573
3:03:01 PM 1min avg: 5.163 1.159 19.977 0.576 0.570
3:04:01 PM 1min avg: 2.852 0.964 20.164 0.432 0.566
3:05:01 PM 1min avg: 9.534 1.637 18.610 1.567 0.480
3:06:01 PM 1min avg: 9.564 1.508 19.166 1.134 0.499
3:07:01 PM 1min avg: 9.788 1.551 18.916 1.307 0.514
3:08:01 PM 1min avg: 8.467 1.335 19.435 0.978 0.589
3:09:01 PM 1min avg: 8.313 1.300 19.744 0.747 0.515
3:10:01 PM 1min avg: 7.526 1.378 19.084 1.169 0.546
3:11:01 PM 1min avg: 6.674 1.284 19.572 0.918 0.440
3:12:01 PM 1min avg: 8.656 1.336 19.089 1.251 0.473
3:13:01 PM 1min avg: 12.364 1.537 19.438 1.195 0.540
3:14:01 PM 1min avg: 5.075 0.949 20.502 0.407 0.544
3:15:01 PM 1min avg: 7.726 1.286 19.103 1.364 0.514
3:16:01 PM 1min avg: 8.163 1.411 19.583 1.030 0.469
3:17:01 PM 1min avg: 7.033 1.291 20.109 0.688 0.443
3:17:01 PM Test Avgs: 6.705 1.276 19.664 0.853 0.543

### Run P2H-1 Datalog Records

Testing by TRC, Austin, Texas 199009 November 20
Run P2H-1
Start: 11/20/2013 4:01:12 PM End: 11/20/2013 4:09:16 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 4:02:12 PM 1min avg: 14.857 1.708 19.574 0.961 0.442
4:03:12 PM 1min avg: 17.259 1.781 19.203 1.188 0.451
4:04:12 PM 1min avg: 16.293 1.815 19.346 1.109 0.398
4:05:12 PM 1min avg: 14.149 2.250 19.323 1.136 0.430
4:09:16 PM Test Avgs: 16.107 1.849 19.412 1.067 0.422

### Run P2H-1b Datalog Records

Testing by TRC, Austin, Texas 199009 November 20
Run P2H-1b
Start: 11/20/2013 4:37:01 PM End: 11/20/2013 4:56:57 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 4:38:01 PM 1min avg: 14.238 1.576 18.991 1.370 0.357
4:39:01 PM 1min avg: 11.018 1.382 19.411 1.098 0.372
4:40:01 PM 1min avg: 11.701 1.502 19.402 1.076 0.326
4:41:01 PM 1min avg: 12.839 1.298 19.500 0.998 0.369
4:42:01 PM 1min avg: 12.285 1.608 19.720 0.883 0.340
4:43:01 PM 1min avg: 14.748 1.997 19.434 1.049 0.426
4:44:01 PM 1min avg: 13.354 2.001 19.466 1.041 0.399
4:45:01 PM 1min avg: 15.468 2.193 19.104 1.237 0.326
4:46:01 PM 1min avg: 22.783 2.028 18.638 1.588 0.418
4:47:01 PM 1min avg: 22.836 2.185 19.185 1.263 0.458
4:48:01 PM 1min avg: 12.534 1.203 19.259 1.164 0.351
4:49:01 PM 1min avg: 20.398 2.014 18.851 1.470 0.383
4:50:01 PM 1min avg: 17.094 2.161 19.201 1.203 0.331
4:51:01 PM 1min avg: 18.661 1.485 19.270 1.160 0.417
4:52:01 PM 1min avg: 18.111 2.089 18.985 1.335 0.321
4:53:01 PM 1min avg: 19.363 2.346 18.770 1.495 0.401
4:54:01 PM 1min avg: 22.847 2.205 18.929 1.408 0.439
4:55:01 PM 1min avg: 19.383 2.591 19.094 1.263 0.365
4:56:01 PM 1min avg: 19.243 1.660 19.111 1.239 0.324
4:56:57 PM Test Avgs: 16.942 1.898 19.177 1.227 0.376

### Run P2L-1(b) Datalog Records

Testing by TRC, Austin, Texas 199009 November 20 Run P2L-1(b)
Start: 11/20/2013 5:23:05 PM End: 11/20/2013 5:55:52 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 5:24:04 PM 1min avg: 10.066 19.477 19.815 0.841 3.509
5:25:04 PM 1min avg: 5.963 11.275 20.215 0.561 5.483
5:26:04 PM 1min avg: 11.024 17.447 19.419 1.052 7.902
5:39:51 PM 1min avg: 10.903 9.986 19.284 1.186 0.991
5:40:51 PM 1min avg: 8.773 4.534 20.410 0.461 0.679
5:41:51 PM 1min avg: 2.988 1.501 20.822 0.171 0.909
5:42:51 PM 1min avg: 6.249 3.929 20.223 0.563 0.724
5:43:51 PM 1min avg: 5.100 2.999 20.405 0.464 0.838
5:44:51 PM 1min avg: 3.675 2.783 20.466 0.390 1.037
5:45:51 PM 1min avg: 7.811 5.107 19.756 0.879 0.974
5:46:51 PM 1min avg: 17.235 8.730 18.770 1.473 1.592
5:47:51 PM 1min avg: 16.675 7.523 19.515 1.061 0.993
5:48:51 PM 1min avg: 9.529 5.025 19.815 0.819 1.481
5:49:51 PM 1min avg: 9.220 8.458 19.560 1.002 0.945
5:50:51 PM 1min avg: 8.784 4.719 19.629 0.937 1.391
5:51:51 PM 1min avg: 13.241 7.892 19.267 1.158 1.444
5:52:51 PM 1min avg: 21.098 9.005 18.978 1.353 1.745
5:53:51 PM 1min avg: 10.591 8.670 19.640 0.932 1.530
5:54:51 PM 1min avg: 13.435 7.167 19.493 1.055 0.942
5:55:51 PM 1min avg: 9.733 6.050 19.738 0.847 1.569
5:55:52 PM Test Avgs: 10.106 7.615 19.760 0.861 1.833

### Run P3H-1 Datalog Records

Testing by TRC, Austin, Texas 199009 November 20
Run P3H-1
Start: 11/20/2013 7:18:05 PM End: 11/20/2013 7:38:05 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 7:19:04 PM 1min avg: 19.182 12.605 18.317 1.761 1.943
7:20:04 PM 1min avg: 14.636 8.022 19.596 0.930 1.236
7:21:04 PM 1min avg: 8.795 3.669 19.556 0.934 1.800
7:22:04 PM 1min avg: 17.506 11.669 18.152 1.841 2.859
7:23:04 PM 1min avg: 22.318 13.812 18.669 1.522 1.592
7:24:04 PM 1min avg: 8.836 4.966 19.761 0.858 1.426
7:25:04 PM 1min avg: 7.938 5.849 19.403 1.022 1.524
7:26:04 PM 1min avg: 14.067 4.040 19.577 0.940 1.646
7:27:04 PM 1min avg: 14.252 8.160 18.501 1.603 2.017
7:28:04 PM 1min avg: 19.888 8.417 18.609 1.518 1.809
7:29:04 PM 1min avg: 16.740 9.877 18.476 1.638 1.514
7:30:04 PM 1min avg: 15.866 6.504 18.894 1.423 1.325
7:31:04 PM 1min avg: 12.329 7.285 18.888 1.356 2.175
7:32:04 PM 1min avg: 19.602 11.307 18.309 1.752 1.424
7:33:04 PM 1min avg: 15.049 8.460 18.696 1.478 2.327
7:34:04 PM 1min avg: 17.341 9.091 19.159 1.215 1.333
7:35:04 PM 1min avg: 16.352 8.684 18.444 1.656 1.778
7:36:04 PM 1min avg: 12.335 6.749 18.873 1.364 1.928
7:37:04 PM 1min avg: 20.670 12.322 18.504 1.657 1.581
7:38:04 PM 1min avg: 20.689 6.668 18.695 1.466 1.276
7:38:05 PM Test Avgs: 15.719 8.405 18.854 1.397 1.725

### Run P3L-1b Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P3L-1b
Start: 11/21/2013 8:54:00 AM End: 11/21/2013 9:25:34 AM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 9:06:33 AM 1min avg: 12.902 4.475 19.426 1.082 0.356
9:07:33 AM 1min avg: 11.889 3.823 19.030 1.290 0.230
9:08:33 AM 1min avg: 12.375 5.129 18.720 1.469 0.151
9:09:33 AM 1min avg: 13.655 4.330 19.021 1.278 0.065
9:10:33 AM 1min avg: 15.460 5.542 18.697 1.519 0.093
9:11:33 AM 1min avg: 9.998 3.877 19.272 1.110 0.032
9:12:33 AM 1min avg: 10.066 3.587 19.410 1.027 0.036
9:13:33 AM 1min avg: 11.001 3.290 19.396 1.045 0.097
9:14:33 AM 1min avg: 10.136 3.732 19.405 1.030 0.144
9:15:33 AM 1min avg: 11.647 4.127 19.106 1.196 0.074
9:16:33 AM 1min avg: 11.126 4.492 19.040 1.262 0.101
9:17:33 AM 1min avg: 12.875 4.502 19.202 1.167 0.131
9:18:33 AM 1min avg: 11.329 4.749 18.996 1.290 0.141
9:19:33 AM 1min avg: 15.443 5.421 18.457 1.636 0.203
9:20:33 AM 1min avg: 18.514 6.593 18.410 1.701 0.117
9:21:33 AM 1min avg: 12.625 4.489 19.333 1.087 0.026
9:22:33 AM 1min avg: 11.950 4.663 18.701 1.494 0.274
9:23:33 AM 1min avg: 13.590 5.213 18.779 1.448 0.067
9:24:33 AM 1min avg: 17.403 5.822 18.495 1.620 0.611
9:25:33 AM 1min avg: 16.621 8.381 18.288 1.787 0.246
9:25:34 AM Test Avgs: 13.035 4.814 18.959 1.327 0.160

### Run P1L-2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P1L-2
Start: 11/21/2013 9:44:00 AM End: 11/21/2013 10:04:01 AM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 9:45:00 AM 1min avg: 10.088 1.853 19.370 1.276 -0.235
9:46:00 AM 1min avg: 6.870 1.490 19.011 1.474 -0.264
9:47:00 AM 1min avg: 8.103 1.619 19.558 1.098 -0.212
9:48:00 AM 1min avg: 8.860 1.369 19.648 1.042 -0.214
9:49:00 AM 1min avg: 4.134 0.794 20.279 0.607 -0.185
9:50:00 AM 1min avg: 3.405 0.581 20.342 0.569 -0.266
9:51:00 AM 1min avg: 4.986 0.717 20.003 0.797 -0.245
9:52:00 AM 1min avg: 6.457 0.857 20.208 0.664 -0.285
9:53:00 AM 1min avg: 2.166 0.343 20.635 0.354 -0.305
9:54:00 AM 1min avg: 5.375 1.128 19.460 1.129 -0.426
9:55:00 AM 1min avg: 9.259 1.576 19.285 1.296 -0.398
9:56:00 AM 1min avg: 11.910 1.594 19.102 1.415 -0.440
9:57:00 AM 1min avg: 13.263 2.269 18.439 1.946 -0.462
9:58:00 AM 1min avg: 11.216 1.851 18.485 1.855 -0.523
9:59:00 AM 1min avg: 12.355 2.007 18.862 1.636 -0.510
10:00:00 AM 1min avg: 10.855 1.718 18.681 1.744 -0.499
10:01:00 AM 1min avg: 15.099 2.022 18.242 2.099 -0.550
10:02:00 AM 1min avg: 13.069 2.196 18.675 1.735 -0.617
10:03:00 AM 1min avg: 15.007 2.121 18.358 1.988 -0.521
10:04:00 AM 1min avg: 14.630 2.322 17.759 2.393 -0.557
10:04:01 AM Test Avgs: 9.355 1.522 19.220 1.356 -0.386

### Run P2H-2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P2H-2
Start: 11/21/2013 10:56:00 AM End: 11/21/2013 11:16:00 AM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 10:57:00 AM 1min avg: 7.539 2.260 19.774 0.849 0.257
10:58:00 AM 1min avg: 11.631 2.000 19.634 0.917 0.204
10:59:00 AM 1min avg: 11.981 1.842 19.489 1.002 0.294
11:00:00 AM 1min avg: 9.945 2.041 19.546 0.976 0.225
11:01:00 AM 1min avg: 13.263 2.345 19.299 1.180 0.193
11:02:00 AM 1min avg: 9.138 1.099 20.118 0.681 0.241
11:03:00 AM 1min avg: 15.092 1.440 19.519 1.042 0.257
11:04:00 AM 1min avg: 10.703 1.465 19.799 0.871 0.279
11:05:00 AM 1min avg: 11.612 1.566 19.790 0.889 0.282
11:06:00 AM 1min avg: 8.880 1.979 19.849 0.837 0.196
11:07:00 AM 1min avg: 11.352 0.771 19.894 0.827 0.192
11:08:00 AM 1min avg: 12.638 1.331 19.619 1.018 0.311
11:09:00 AM 1min avg: 5.917 0.454 20.774 0.272 0.382
11:10:00 AM 1min avg: 11.658 4.025 19.550 1.015 0.516
11:11:00 AM 1min avg: 11.626 4.701 19.721 0.919 0.476
11:12:00 AM 1min avg: 12.309 6.286 19.459 1.070 0.498
11:13:00 AM 1min avg: 10.282 3.353 19.950 0.783 0.420
11:14:00 AM 1min avg: 10.166 4.339 19.722 0.919 0.912
11:15:00 AM 1min avg: 11.169 3.621 19.901 0.833 0.884
11:16:00 AM 1min avg: 7.897 2.799 19.638 0.988 0.784
11:16:00 AM Test Avgs: 10.740 2.486 19.752 0.894 0.390

### Run P2L-2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P2L-2
Start: 11/21/2013 11:31:03 AM End: 11/21/2013 11:51:03 AM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 11:32:03 AM 1min avg: 3.203 2.600 20.805 0.244 1.203
11:33:03 AM 1min avg: 1.247 0.605 20.803 0.235 1.218
11:34:03 AM 1min avg: 1.567 1.025 20.732 0.276 1.269
11:35:03 AM 1min avg: 5.304 3.088 20.153 0.636 1.398
11:36:03 AM 1min avg: 7.177 6.341 19.965 0.744 1.477
11:37:03 AM 1min avg: 5.384 3.919 20.384 0.515 1.105
11:38:03 AM 1min avg: 8.789 4.639 19.398 1.118 1.200
11:39:03 AM 1min avg: 13.575 5.667 19.979 0.780 2.846
11:40:03 AM 1min avg: 10.448 11.449 19.175 1.262 2.234
11:41:03 AM 1min avg: 15.761 10.361 19.390 1.128 2.809
11:42:03 AM 1min avg: 16.209 11.235 19.324 1.199 1.941
11:43:03 AM 1min avg: 15.921 4.683 20.055 0.729 1.218
11:44:03 AM 1min avg: 7.163 4.558 19.332 1.169 1.389
11:45:03 AM 1min avg: 16.654 10.027 19.352 1.172 2.049
11:46:03 AM 1min avg: 11.194 9.708 19.929 0.809 1.163
11:47:03 AM 1min avg: 6.317 6.150 20.013 0.724 1.819
11:48:03 AM 1min avg: 9.274 8.629 19.807 0.863 1.497
11:49:03 AM 1min avg: 14.876 8.474 19.221 1.240 3.319
11:50:03 AM 1min avg: 9.241 12.055 19.641 0.957 2.436
11:51:03 AM 1min avg: 11.091 12.569 19.533 1.063 3.149
11:51:03 AM Test Avgs: 9.520 6.889 19.850 0.843 1.837

### Run P3H-2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P3H-2
Start: 11/21/2013 12:45:01 PM End: 11/21/2013 1:05:02 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 12:46:01 PM 1min avg: 7.354 2.896 19.828 0.789 1.171
12:47:01 PM 1min avg: 6.795 2.571 20.061 0.667 1.051
12:48:01 PM 1min avg: 8.850 3.062 19.446 1.003 1.090
12:49:01 PM 1min avg: 10.528 3.874 19.356 1.094 1.076
12:50:01 PM 1min avg: 6.764 3.255 19.997 0.710 1.126
12:51:01 PM 1min avg: 5.668 3.376 20.134 0.650 1.156
12:52:01 PM 1min avg: 5.768 2.909 19.630 0.894 1.205
12:53:01 PM 1min avg: 12.075 4.100 19.123 1.214 1.205
12:54:01 PM 1min avg: 8.029 3.832 19.673 0.897 1.199
12:55:01 PM 1min avg: 8.697 3.780 19.575 0.939 1.173
12:56:01 PM 1min avg: 11.629 4.045 18.860 1.412 1.103
12:57:01 PM 1min avg: 14.725 4.086 19.608 0.966 1.147
12:58:01 PM 1min avg: 6.188 2.219 19.617 0.937 1.214
12:59:01 PM 1min avg: 10.179 3.036 20.230 0.566 1.177
1:00:01 PM 1min avg: 5.245 2.437 19.992 0.706 1.385
1:01:01 PM 1min avg: 4.580 2.644 20.252 0.541 1.288
1:02:01 PM 1min avg: 6.246 2.999 19.997 0.730 1.377
1:03:01 PM 1min avg: 9.647 2.711 19.860 0.783 1.242
1:04:01 PM 1min avg: 6.564 3.012 19.436 0.988 1.342
1:05:01 PM 1min avg: 13.439 4.026 19.273 1.190 1.364
1:05:02 PM Test Avgs: 8.448 3.244 19.697 0.884 1.204

### Run P3L-2 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P3L-2
Start: 11/21/2013 1:16:57 PM End: 11/21/2013 1:36:57 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 1:17:56 PM 1min avg: 10.370 3.872 19.183 1.173 0.858
1:18:56 PM 1min avg: 9.858 3.216 19.827 0.810 0.932
1:19:56 PM 1min avg: 4.198 1.504 20.151 0.593 0.896
1:20:56 PM 1min avg: 7.434 2.423 19.424 1.008 0.870
1:21:56 PM 1min avg: 8.350 1.730 20.295 0.541 0.924
1:22:56 PM 1min avg: 1.126 0.236 20.948 0.118 0.905
1:23:56 PM 1min avg: 3.097 0.466 20.363 0.484 0.952
1:24:56 PM 1min avg: 7.367 1.738 19.551 0.948 1.108
1:25:56 PM 1min avg: 14.838 5.761 18.108 1.861 1.458
1:26:56 PM 1min avg: 20.400 9.881 18.034 1.946 1.614
1:27:56 PM 1min avg: 14.176 7.813 18.737 1.465 1.238
1:28:56 PM 1min avg: 12.187 6.405 19.143 1.205 1.324
1:29:56 PM 1min avg: 5.358 2.182 20.672 0.316 1.004
1:30:56 PM 1min avg: 3.869 1.549 20.008 0.674 1.148
1:31:56 PM 1min avg: 4.889 2.147 20.660 0.322 1.045
1:32:56 PM 1min avg: 0.680 0.299 20.863 0.180 1.106
1:33:56 PM 1min avg: 5.720 1.593 19.168 1.184 0.971
1:34:56 PM 1min avg: 11.352 2.525 19.558 0.965 1.111
1:35:56 PM 1min avg: 14.846 4.118 18.079 1.884 1.268
1:36:56 PM 1min avg: 22.108 8.037 17.697 2.164 1.161
1:36:57 PM Test Avgs: 9.119 3.377 19.523 0.992 1.095

### Run P1H-3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P1H-3
Start: 11/21/2013 1:48:07 PM End: 11/21/2013 2:08:08 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 1:49:07 PM 1min avg: 8.015 0.963 18.737 1.659 0.900
1:50:07 PM 1min avg: 17.713 1.575 17.867 2.338 0.913
1:51:07 PM 1min avg: 18.562 1.322 18.405 1.910 0.881
1:52:07 PM 1min avg: 16.961 1.373 18.600 1.815 0.963
1:53:07 PM 1min avg: 15.375 1.165 17.738 2.403 0.915
1:54:07 PM 1min avg: 11.775 0.780 19.975 0.818 0.925
1:55:07 PM 1min avg: 14.869 1.205 18.133 2.142 0.819
1:56:07 PM 1min avg: 9.490 0.674 20.199 0.684 0.923
1:57:07 PM 1min avg: 4.513 0.345 20.285 0.546 0.759
1:58:07 PM 1min avg: 12.799 0.853 18.777 1.616 0.780
1:59:07 PM 1min avg: 15.837 1.074 18.340 2.023 0.752
2:00:07 PM 1min avg: 13.487 0.917 19.078 1.446 0.814
2:01:07 PM 1min avg: 12.060 0.948 19.116 1.444 0.909
2:02:07 PM 1min avg: 4.976 0.341 20.600 0.371 0.896
2:03:07 PM 1min avg: 6.441 0.559 20.200 0.659 0.992
2:04:07 PM 1min avg: 0.905 0.145 20.920 0.156 0.985
2:05:07 PM 1min avg: 2.067 0.329 20.398 0.523 0.839
2:06:07 PM 1min avg: 7.410 0.611 19.728 0.957 0.718
2:07:07 PM 1min avg: 9.396 0.876 19.099 1.380 0.637
2:08:07 PM 1min avg: 17.000 1.520 18.647 1.775 0.708
2:08:08 PM Test Avgs: 10.989 0.879 19.242 1.333 0.851

### Run P2L-3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P2L-3
Start: 11/21/2013 2:38:00 PM End: 11/21/2013 2:58:01 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 2:39:00 PM 1min avg: 18.320 6.338 19.585 1.074 0.511
2:40:00 PM 1min avg: 9.637 2.385 19.783 0.875 0.751
2:41:00 PM 1min avg: 12.875 4.824 19.032 1.336 0.845
2:42:00 PM 1min avg: 17.104 8.382 18.984 1.389 1.802
2:43:00 PM 1min avg: 18.278 11.824 19.195 1.240 1.317
2:44:00 PM 1min avg: 9.694 4.652 19.986 0.766 0.762
2:45:00 PM 1min avg: 8.866 3.823 19.927 0.775 1.490
2:46:00 PM 1min avg: 13.800 8.692 19.256 1.201 1.255
2:47:00 PM 1min avg: 15.343 6.672 19.879 0.822 0.882
2:48:00 PM 1min avg: 7.167 2.475 20.016 0.720 0.640
2:49:00 PM 1min avg: 10.474 4.447 19.667 0.959 1.119
2:50:00 PM 1min avg: 15.062 8.628 19.289 1.161 2.162
2:51:00 PM 1min avg: 11.601 8.205 20.144 0.694 0.523
2:52:00 PM 1min avg: 5.733 2.537 19.918 0.752 0.773
2:53:00 PM 1min avg: 13.189 6.728 19.167 1.297 0.733
2:54:00 PM 1min avg: 17.962 10.860 19.114 1.290 1.423
2:55:00 PM 1min avg: 13.554 12.342 19.464 1.132 1.545
2:56:00 PM 1min avg: 17.921 10.414 18.679 1.589 0.943
2:57:00 PM 1min avg: 20.312 8.787 18.865 1.490 0.756
2:58:00 PM 1min avg: 13.538 5.085 19.182 1.263 0.984
2:58:01 PM Test Avgs: 13.522 6.904 19.456 1.092 1.062

### Run P3L-3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P3L-3
Start: 11/21/2013 3:06:01 PM End: 11/21/2013 3:26:02 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 3:07:01 PM 1min avg: 7.268 1.236 20.319 0.476 0.893
3:08:01 PM 1min avg: 6.267 1.954 19.427 1.075 1.002
3:09:01 PM 1min avg: 9.833 3.247 19.315 1.079 0.977
3:10:01 PM 1min avg: 15.586 5.372 18.801 1.446 1.227
3:11:01 PM 1min avg: 16.881 8.334 18.108 1.908 0.866
3:12:01 PM 1min avg: 15.196 3.765 18.825 1.418 1.043
3:13:01 PM 1min avg: 15.151 6.758 18.249 1.843 1.311
3:14:01 PM 1min avg: 10.233 5.358 19.449 1.033 1.370
3:15:01 PM 1min avg: 12.032 8.922 18.989 1.329 1.413
3:16:01 PM 1min avg: 13.794 9.376 18.221 1.794 1.588
3:17:01 PM 1min avg: 13.388 10.646 18.989 1.344 1.037
3:18:01 PM 1min avg: 10.148 5.731 19.114 1.282 1.523
3:19:01 PM 1min avg: 10.194 6.222 19.527 1.004 0.919
3:20:01 PM 1min avg: 13.576 4.979 19.011 1.334 1.432
3:21:01 PM 1min avg: 9.540 6.572 19.171 1.238 1.466
3:22:01 PM 1min avg: 14.092 5.642 19.048 1.270 2.256
3:23:01 PM 1min avg: 19.058 16.557 17.893 2.065 1.250
3:24:01 PM 1min avg: 19.162 7.481 18.382 1.729 0.915
3:25:01 PM 1min avg: 13.790 4.859 19.081 1.288 1.628
3:26:01 PM 1min avg: 16.451 8.210 18.824 1.475 1.249
3:26:02 PM Test Avgs: 13.082 6.561 18.937 1.372 1.268

### Run P3H-3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P3H-3
Start: 11/21/2013 3:34:02 PM End: 11/21/2013 3:54:02 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 3:35:01 PM 1min avg: 11.387 6.863 19.415 1.060 1.689
3:36:01 PM 1min avg: 11.674 7.171 19.328 1.091 1.633
3:37:01 PM 1min avg: 12.097 7.991 19.235 1.147 1.647
3:38:01 PM 1min avg: 11.723 7.627 19.326 1.133 1.909
3:39:01 PM 1min avg: 11.316 7.703 19.569 0.956 1.503
3:40:01 PM 1min avg: 11.317 6.963 19.314 1.096 1.849
3:41:01 PM 1min avg: 12.671 8.102 19.528 1.021 2.098
3:42:01 PM 1min avg: 10.751 7.714 19.406 1.042 1.607
3:43:01 PM 1min avg: 11.252 6.738 19.523 0.996 1.675
3:44:01 PM 1min avg: 11.607 7.654 19.080 1.228 1.822
3:45:01 PM 1min avg: 10.749 9.851 19.378 1.100 2.164
3:46:01 PM 1min avg: 6.921 7.409 19.788 0.846 1.862
3:47:01 PM 1min avg: 7.189 8.301 19.678 0.934 2.286
3:48:01 PM 1min avg: 8.054 8.504 19.732 0.848 2.135
3:49:01 PM 1min avg: 11.012 10.314 19.194 1.197 2.402
3:50:01 PM 1min avg: 9.957 9.449 19.678 0.923 2.156
3:51:01 PM 1min avg: 9.678 7.697 19.399 1.054 1.749
3:52:01 PM 1min avg: 12.721 7.614 19.042 1.276 1.972
3:53:01 PM 1min avg: 13.527 10.184 18.874 1.400 2.247
3:54:01 PM 1min avg: 11.814 10.717 19.217 1.158 1.895
3:54:02 PM Test Avgs: 10.871 8.228 19.385 1.075 1.916

### Run P2H-3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P2H-3
Start: 11/21/2013 4:01:59 PM End: 11/21/2013 4:22:01 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 4:02:59 PM 1min avg: 14.030 5.408 19.199 1.252 1.061
4:03:59 PM 1min avg: 13.723 5.490 19.165 1.278 0.997
4:04:59 PM 1min avg: 12.308 4.811 19.596 1.016 1.166
4:05:59 PM 1min avg: 14.175 5.979 19.414 1.083 1.141
4:06:59 PM 1min avg: 12.079 5.279 19.471 1.074 1.067
4:07:59 PM 1min avg: 12.538 5.488 19.281 1.215 0.969
4:08:59 PM 1min avg: 17.069 5.547 19.193 1.274 1.023
4:09:59 PM 1min avg: 11.362 4.645 19.655 0.981 1.068
4:10:59 PM 1min avg: 12.474 6.257 19.599 0.980 1.196
4:11:59 PM 1min avg: 11.067 5.010 20.013 0.777 0.934
4:12:59 PM 1min avg: 10.764 4.017 19.903 0.812 0.946
4:13:59 PM 1min avg: 11.253 4.952 19.537 1.046 1.019
4:14:59 PM 1min avg: 11.936 5.580 19.556 1.021 1.019
4:15:59 PM 1min avg: 12.249 4.834 19.670 0.967 0.875
4:16:59 PM 1min avg: 11.557 3.296 19.320 1.176 0.927
4:17:59 PM 1min avg: 15.324 5.206 19.698 1.006 0.893
4:18:59 PM 1min avg: 11.476 4.747 19.424 1.094 0.921
4:19:59 PM 1min avg: 12.274 4.725 19.378 1.154 0.781
4:20:59 PM 1min avg: 10.799 3.528 20.178 0.684 0.678
4:21:59 PM 1min avg: 2.337 0.818 20.683 0.332 0.649
4:22:01 PM Test Avgs: 12.040 4.781 19.597 1.011 0.967

### Run P1L-3 Datalog Records

Testing by TRC, Austin, Texas 199009 November 21
Run P1L-3
Start: 11/21/2013 4:32:02 PM End: 11/21/2013 4:52:03 PM

Operator: JPB Plant: John Zink
Location: Tulsa, OK
Source ID: Dow Flare Test

NOx CO O2 CO2 C3H8-Propy
Time Entry ppm ppm % % ppm 4:33:01 PM 1min avg: 10.135 1.493 19.226 1.336 0.436
4:34:01 PM 1min avg: 8.216 1.176 19.335 1.356 0.446
4:35:01 PM 1min avg: 6.073 0.754 19.841 0.900 0.470
4:36:01 PM 1min avg: 6.743 1.150 19.956 0.875 0.498
4:37:01 PM 1min avg: 7.500 0.698 19.793 0.968 0.503
4:38:01 PM 1min avg: 3.797 0.430 20.754 0.332 0.521
4:39:01 PM 1min avg: 3.714 1.055 19.915 0.880 0.492
4:40:01 PM 1min avg: 3.966 0.602 20.572 0.461 0.491
4:41:01 PM 1min avg: 1.060 0.267 20.845 0.237 0.483
4:42:01 PM 1min avg: 3.307 0.876 20.392 0.561 0.410
4:43:01 PM 1min avg: 6.514 1.249 19.294 1.308 0.437
4:44:01 PM 1min avg: 7.698 1.761 19.765 1.066 0.476
4:45:01 PM 1min avg: 4.311 1.775 19.576 1.091 0.504
4:46:01 PM 1min avg: 6.745 1.584 19.970 0.909 0.481
4:47:01 PM 1min avg: 6.754 0.866 20.082 0.767 0.418
4:48:01 PM 1min avg: 8.462 1.296 19.656 1.097 0.456
4:49:01 PM 1min avg: 3.406 0.886 20.551 0.480 0.514
4:50:01 PM 1min avg: 5.451 0.884 19.764 0.965 0.443
4:51:01 PM 1min avg: 6.056 1.034 19.931 0.892 0.482
4:52:01 PM 1min avg: 7.264 1.373 19.883 0.919 0.391
4:52:03 PM Test Avgs: 5.861 1.061 19.955 0.870 0.468

# Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area Channel_A_02.ASC 11/18/2013 10:39:44 Methane 1.553 3343 Ethane 1.7 14292 Propylene 0 0 Channel_A_03.ASC 11/18/2013 10:45:03 Methane 1.546 1693 Ethane 1.693 6554 Propylene 0 0 Channel_A_04.ASC 11/18/2013 11:00:40 Methane 0 0 Ethane 0 0 Propylene 1.99 945152 Channel_A_05.ASC 11/18/2013 11:08:02 Methane 0 0 Ethane 0 0 Propylene 1.986 975455 Channel_A_06.ASC 11/18/2013 11:15:19 Methane 0 0 Ethane 0 0 Propylene 1.983 990708 Channel_A_07.ASC 11/18/2013 11:24:14 Methane 0 0 Ethane 0 0 Propylene 1.996 600029 Channel_A_08.ASC 11/18/2013 11:30:22 Methane 0 0 Ethane 0 0 Propylene 1.993 568286 Channel_A_09.ASC 11/18/2013 11:38:31 Methane 0 0 Ethane 0 0 Propylene 1.993 571236 Channel_A_10.ASC 11/18/2013 11:45:03 Methane 0 0 Ethane 0 0 Propylene 1.998 336432 Channel_A_11.ASC 11/18/2013 11:48:21 Methane 0 0 Ethane 0 0 Propylene 2.001 333042 Channel_A_12.ASC 11/18/2013 11:51:37 Methane 0 0 Ethane 0 0 Propylene 1.998 331664 Channel_A_13.ASC 11/18/2013 12:56:13 Methane 1.526 365922 Ethane 1.675 7955 Propylene 2.008 15086 Channel_A_14.ASC 11/18/2013 13:00:56 Methane 1.523 372545 Ethane 1.673 8130 Propylene 2.006 5352 Channel_A_15.ASC 11/18/2013 13:05:22 Methane 1.523 375843 Ethane 1.673 8241 Propylene 2.006 1988 Cal 50 C1 10 C2 A_16.ASC 11/18/2013 13:12:48 Methane 1.526 209749 Ethane 1.673 78550 Propylene 2.006 656 Cal 50 C1 10 C2 A_17.ASC 11/18/2013 13:17:23 Methane 1.525 205188 Ethane 1.671 80708 Propylene 0 0 Cal 50 C1 10 C2 A_18.ASC 11/18/2013 13:21:16 Methane 1.525 204191 Ethane 1.671 81667 Propylene 0 0 Cal 20 C1 20 C2 A_19.ASC 11/18/2013 13:27:58 Methane 1.526 83857 Ethane 1.67 162602 Propylene 0 0 Cal 20 C1 20 C2 A_20.ASC 11/18/2013 13:31:52 Methane 1.528 83836 Ethane 1.671 162688 Propylene 0 0 Cal 20 C1 20 C2 A_21.ASC 11/18/2013 13:34:46 Methane 1.528 84026 Ethane 1.671 163179 Propylene 0 0 Cal 5 C1 5 C2 A_22.ASC 11/18/2013 13:39:35 Methane 1.526 21445 Ethane 1.673 42137 Propylene 0 0 Cal 5 C1 5 C2 A_23.ASC 11/18/2013 13:42:08 Methane 1.528 21477 Ethane 1.673 42186 Propylene 0 0 Cal 5 C1 5 C2 A_24.ASC 11/18/2013 13:45:53 Methane 1.526 21547 Ethane 1.671 42174 Propylene 0 0 Channel_A_25.ASC 11/18/2013 15:35:45 Methane 1.53 22803 Ethane 1.675 44469 Propylene 2.006 1563 Cal 85.02 C3= A_26.ASC 11/19/2013 6:51:40 Methane 0 0 Ethane 0 0 Propylene 1.965 1097273 Cal 85.02 C3= A_27.ASC 11/19/2013 7:05:04 Methane 0 0 Ethane 0 0 Propylene 1.963 1144216 Cal 85.02 C3= A_28.ASC 11/19/2013 7:13:11 Methane 0 0 Ethane 0 0 Propylene 1.963 1138793 Cal 50 C3= A_29.ASC 11/19/2013 7:21:34 Methane 0 0 Ethane 0 0 Propylene 1.975 656152 Cal 50 C3= A_30.ASC 11/19/2013 7:25:38 Methane 0 0 Ethane 0 0 Propylene 1.975 647915 Cal 50 C3= A_31.ASC 11/19/2013 7:29:26 Methane 0 0 Ethane 0 0 Propylene 1.975 646843 Cal 30 C3= A_32.ASC 11/19/2013 7:35:37 Methane 0 0 Ethane 0 0 Propylene 1.983 394904 Cal 30 C3= A_33.ASC 11/19/2013 7:41:29 Methane 0 0 Ethane 0 0 Propylene 1.985 378900 Cal 30 C3= A_34.ASC 11/19/2013 7:46:46 Methane 0 0 Ethane 0 0 Propylene 1.985 377435 Channel_A_35.ASC 11/19/2013 7:56:09 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_A_36.ASC 11/19/2013 8:03:32 Methane 1.52 206661 Ethane 1.665 83279 Propylene 1.998 4493 Channel_A_37.ASC 11/19/2013 8:32:02 Methane 1.528 6542 Ethane 1.673 796 Propylene 2.005 813 Channel_A_38.ASC 11/19/2013 8:35:16 Methane 1.523 2167 Ethane 1.668 527 Propylene 1.97 780636 Channel_A_39.ASC 11/19/2013 8:39:03 Methane 1.525 744 Ethane 0 0 Propylene 1.97 843356 Channel_A_40.ASC 11/19/2013 8:42:28 Methane 1.521 12377 Ethane 1.666 3339 Propylene 1.97 757075 Channel_A_41.ASC 11/19/2013 8:47:46 Methane 0 0 Ethane 0 0 Propylene 1.975 676952 Channel_A_42.ASC 11/19/2013 9:00:52 Methane 1.523 1731 Ethane 0 0 Propylene 1.97 795008
S1 A_43.ASC 11/19/2013 9:08:14 Methane 0 0 Ethane 0 0 Propylene 1.976 641940
S1 A_44.ASC 11/19/2013 9:15:01 Methane 0 0 Ethane 0 0 Propylene 1.978 607371
S1 A_45.ASC 11/19/2013 9:20:01 Methane 0 0 Ethane 0 0 Propylene 1.975 636470
S1 A_46.ASC 11/19/2013 9:25:01 Methane 0 0 Ethane 0 0 Propylene 1.976 579908
S1 A_47.ASC 11/19/2013 9:30:01 Methane 0 0 Ethane 0 0 Propylene 1.975 637004
S2 A_48.ASC 11/19/2013 9:45:08 Methane 0 0 Ethane 0 0 Propylene 1.976 647849
S2 A_49.ASC 11/19/2013 9:50:08 Methane 0 0 Ethane 0 0 Propylene 1.976 629863
S2 A_50.ASC 11/19/2013 9:55:08 Methane 0 0 Ethane 0 0 Propylene 1.976 600996
S2 A_51.ASC 11/19/2013 10:00:08 Methane 0 0 Ethane 0 0 Propylene 1.975 616391 Channel_A_52.ASC 11/19/2013 10:09:28 Methane 0 0 Ethane 0 0 Propylene 2.001 11810 Channel_A_53.ASC 11/19/2013 10:13:32 Methane 0 0 Ethane 0 0 Propylene 1.998 17394 Channel_A_54.ASC 11/19/2013 10:20:27 Methane 0 0 Ethane 0 0 Propylene 2.003 20168 Channel_A_55.ASC 11/19/2013 10:24:56 Methane 0 0 Ethane 0 0 Propylene 2.003 20207 Channel_A_56.ASC 11/19/2013 10:42:24 Methane 0 0 Ethane 0 0 Propylene 1.988 347031

# Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area Channel_A_57.ASC 11/19/2013 10:46:06 Methane 0 0 Ethane 0 0 Propylene 1.99 252965 Channel_A_58.ASC 11/19/2013 10:55:21 Methane 0 0 Ethane 0 0 Propylene 2 76618 Channel_A_59.ASC 11/19/2013 11:12:34 Methane 0 0 Ethane 0 0 Propylene 1.99 300631 Channel_A_60.ASC 11/19/2013 11:17:26 Methane 0 0 Ethane 0 0 Propylene 1.988 307103
S3 A_61.ASC 11/19/2013 11:29:01 Methane 0 0 Ethane 0 0 Propylene 1.988 336318
S3 A_62.ASC 11/19/2013 11:34:01 Methane 0 0 Ethane 0 0 Propylene 1.985 328695 Channel_A_63.ASC 11/19/2013 11:39:01 Methane 0 0 Ethane 0 0 Propylene 2.003 5236
S3 A_64.ASC 11/19/2013 11:44:01 Methane 0 0 Ethane 0 0 Propylene 1.986 362085
S3 A_65.ASC 11/19/2013 11:50:05 Methane 0 0 Ethane 0 0 Propylene 1.985 351404 Channel_A_66.ASC 11/19/2013 11:55:27 Methane 0 0 Ethane 0 0 Propylene 1.985 383370 Channel_A_67.ASC 11/19/2013 11:58:52 Methane 0 0 Ethane 0 0 Propylene 1.981 384498 Channel_A_68.ASC 11/19/2013 12:04:04 Methane 0 0 Ethane 0 0 Propylene 1.986 367968 Channel_A_69.ASC 11/19/2013 12:45:51 Methane 0 0 Ethane 0 0 Propylene 1.986 362478 Channel_A_70.ASC 11/19/2013 12:49:54 Methane 0 0 Ethane 0 0 Propylene 1.985 364459 Channel_A_71.ASC 11/19/2013 12:57:06 Methane 0 0 Ethane 0 0 Propylene 1.983 508555
S4 A_72.ASC 11/19/2013 13:36:06 Methane 0 0 Ethane 0 0 Propylene 1.985 422309
S4 A_73.ASC 11/19/2013 13:41:06 Methane 0 0 Ethane 0 0 Propylene 1.983 431030
S4 A_74.ASC 11/19/2013 13:46:06 Methane 0 0 Ethane 0 0 Propylene 1.983 434189
S4 A_75.ASC 11/19/2013 13:51:06 Methane 0 0 Ethane 0 0 Propylene 1.983 424148
S5 A_76.ASC 11/19/2013 14:18:51 Methane 0 0 Ethane 0 0 Propylene 1.986 374314
S5 A_77.ASC 11/19/2013 14:23:51 Methane 0 0 Ethane 0 0 Propylene 1.985 373703
S5 A_78.ASC 11/19/2013 14:28:51 Methane 0 0 Ethane 0 0 Propylene 1.983 389657
S5 A_79.ASC 11/19/2013 14:33:51 Methane 0 0 Ethane 0 0 Propylene 1.983 404682
S6 A_80.ASC 11/19/2013 14:56:04 Methane 0 0 Ethane 0 0 Propylene 1.955 1306487
S6 A_81.ASC 11/19/2013 15:01:04 Methane 0 0 Ethane 0 0 Propylene 1.956 1304866
S6 A_82.ASC 11/19/2013 15:06:04 Methane 0 0 Ethane 0 0 Propylene 1.956 1305717
S6 A_83.ASC 11/19/2013 15:11:04 Methane 0 0 Ethane 0 0 Propylene 1.955 1306852 Channel_A_84.ASC 11/19/2013 15:21:12 Methane 0 0 Ethane 0 0 Propylene 1.981 372255 Channel_A_85.ASC 11/19/2013 15:24:42 Methane 0 0 Ethane 0 0 Propylene 1.985 375799 Channel_A_86.ASC 11/19/2013 15:27:43 Methane 0 0 Ethane 0 0 Propylene 1.961 1072314 Channel_A_87.ASC 11/19/2013 15:31:02 Methane 0 0 Ethane 0 0 Propylene 1.961 1089138 Channel_A_88.ASC 11/19/2013 15:34:09 Methane 0 0 Ethane 0 0 Propylene 1.961 1092651 Channel_A_89.ASC 11/19/2013 15:38:14 Methane 0 0 Ethane 0 0 Propylene 1.975 637828 Channel_A_90.ASC 11/19/2013 15:41:12 Methane 0 0 Ethane 0 0 Propylene 1.973 631517 Channel_A_91.ASC 11/19/2013 15:45:08 Methane 0 0 Ethane 0 0 Propylene 0 0
P1H-1 A_92.ASC 11/19/2013 15:50:08 Methane 0 0 Ethane 0 0 Propylene 1.955 1317397
P1H-1 A_93.ASC 11/19/2013 15:55:08 Methane 0 0 Ethane 0 0 Propylene 1.956 1337434
P1H-1 A_94.ASC 11/19/2013 16:00:08 Methane 0 0 Ethane 0 0 Propylene 1.956 1325391 Channel_A_95.ASC 11/19/2013 16:10:57 Methane 0 0 Ethane 0 0 Propylene 1.956 1288955 Channel_A_96.ASC 11/19/2013 16:14:33 Methane 0 0 Ethane 0 0 Propylene 1.96 1029914 Channel_A_97.ASC 11/19/2013 16:20:07 Methane 0 0 Ethane 0 0 Propylene 1.971 745639 Cal 50 C3= A_98.ASC 11/19/2013 16:23:39 Methane 0 0 Ethane 0 0 Propylene 1.975 625401 Cal 50 C3= A_99.ASC 11/20/2013 10:59:25 Methane 0 0 Ethane 0 0 Propylene 1.976 602221 Cal 50 C3= _100.ASC 11/20/2013 11:04:12 Methane 0 0 Ethane 0 0 Propylene 1.973 608316 Cal 50 C1 10 C2 _101.ASC 11/20/2013 13:46:27 Methane 1.521 195417 Ethane 1.666 78720 Propylene 2 4269
P1H-2 _102.ASC 11/20/2013 14:09:11 Methane 1.523 2510 Ethane 1.668 823 Propylene 1.958 1260048
P1H-2 _103.ASC 11/20/2013 14:14:11 Methane 0 0 Ethane 0 0 Propylene 1.955 1295417
P1H-2 _104.ASC 11/20/2013 14:19:11 Methane 0 0 Ethane 0 0 Propylene 1.953 1304635
P1H-2 _105.ASC 11/20/2013 14:24:11 Methane 0 0 Ethane 0 0 Propylene 1.955 1317226
P1L-1 _106.ASC 11/20/2013 14:57:11 Methane 0 0 Ethane 0 0 Propylene 1.956 1306952
P1L-1 _107.ASC 11/20/2013 15:02:11 Methane 0 0 Ethane 0 0 Propylene 1.956 1303504
P1L-1 _108.ASC 11/20/2013 15:07:11 Methane 0 0 Ethane 0 0 Propylene 1.953 1303764
P1L-1 _109.ASC 11/20/2013 15:12:11 Methane 0 0 Ethane 0 0 Propylene 1.955 1303151 Channel_A_110.ASC 11/20/2013 15:21:30 Methane 0 0 Ethane 0 0 Propylene 1.953 1296992 Channel_A_112.ASC 11/20/2013 15:30:29 Methane 0 0 Ethane 0 0 Propylene 1.97 684422

# Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area Channel_A_113.ASC 11/20/2013 15:34:17 Methane 0 0 Ethane 0 0 Propylene 1.996 48999
P2H-1 _114.ASC 11/20/2013 16:01:23 Methane 0 0 Ethane 0 0 Propylene 1.981 469186
P2H-1 _115.ASC 11/20/2013 16:06:23 Methane 0 0 Ethane 0 0 Propylene 1.978 442584 P2H-1b _116.ASC 11/20/2013 16:37:10 Methane 0 0 Ethane 0 0 Propylene 1.981 452209 P2H-1b _117.ASC 11/20/2013 16:42:10 Methane 0 0 Ethane 0 0 Propylene 1.978 471370 P2H-1b _118.ASC 11/20/2013 16:47:10 Methane 0 0 Ethane 0 0 Propylene 1.978 478287 P2H-1b _119.ASC 11/20/2013 16:52:10 Methane 0 0 Ethane 0 0 Propylene 1.976 484779
P2L-1 _120.ASC 11/20/2013 17:23:01 Methane 0 0 Ethane 0 0 Propylene 1.985 397546 Channel_A_121.ASC 11/20/2013 17:28:01 Methane 0 0 Ethane 0 0 Propylene 2.001 26727 Channel_A_122.ASC 11/20/2013 17:33:01 Methane 0 0 Ethane 0 0 Propylene 1.981 392530 P2L-1b _123.ASC 11/20/2013 17:38:01 Methane 0 0 Ethane 0 0 Propylene 1.98 426879 P2L-1b _124.ASC 11/20/2013 17:53:38 Methane 0 0 Ethane 0 0 Propylene 1.98 428086 Channel_A_125.ASC 11/20/2013 18:36:18 Methane 0 0 Ethane 0 0 Propylene 1.998 67721 Channel_A_126.ASC 11/20/2013 18:38:58 Methane 0 0 Ethane 0 0 Propylene 1.996 67860 Channel_A_127.ASC 11/20/2013 18:42:17 Methane 0 0 Ethane 0 0 Propylene 2 72491 Channel_A_128.ASC 11/20/2013 18:45:02 Methane 0 0 Ethane 0 0 Propylene 1.991 72509 Channel_A_129.ASC 11/20/2013 18:56:10 Methane 1.526 105040 Ethane 1.671 9734 Propylene 1.988 329807
P3H-1 _130.ASC 11/20/2013 19:18:09 Methane 1.52 95223 Ethane 1.666 8805 Propylene 1.983 303502
P3H-1 _131.ASC 11/20/2013 19:23:09 Methane 1.523 95020 Ethane 1.67 8884 Propylene 1.986 279466
P3H-1 _132.ASC 11/20/2013 19:28:09 Methane 1.523 94398 Ethane 1.67 8714 Propylene 1.986 287825
P3H-1 _133.ASC 11/20/2013 19:33:09 Methane 1.523 95747 Ethane 1.67 8620 Propylene 1.986 284975 Cal 50 C3= _134.ASC 11/20/2013 19:38:04 Methane 1.523 2963 Ethane 0 0 Propylene 1.973 609278 Cal 50 C3= _135.ASC 11/20/2013 19:44:33 Methane 1.523 1165 Ethane 0 0 Propylene 1.973 615466 Cal 50 C3= _136.ASC 11/20/2013 19:47:31 Methane 1.523 504 Ethane 0 0 Propylene 1.973 616195 Cal 50 C1 10 C2 _137.ASC 11/21/2013 6:51:41 Methane 1.525 197433 Ethane 1.67 79420 Propylene 2.003 909 Cal 50 C1 10 C2 _138.ASC 11/21/2013 6:59:48 Methane 1.523 201679 Ethane 1.668 81107 Propylene 0 0 Cal 50 C1 10 C2 _139.ASC 11/21/2013 7:10:29 Methane 1.523 203513 Ethane 1.668 81963 Propylene 0 0 Cal 50 C1 10 C2 _140.ASC 11/21/2013 7:31:01 Methane 1.523 202060 Ethane 1.668 81236 Propylene 2.001 10191 Cal 50 C3= _141.ASC 11/21/2013 7:50:04 Methane 1.525 4120 Ethane 1.67 1908 Propylene 1.975 609757 Cal 50 C3= _142.ASC 11/21/2013 7:58:59 Methane 1.525 1347 Ethane 1.67 819 Propylene 1.975 603811 Cal 50 C3= _143.ASC 11/21/2013 8:05:23 Methane 1.525 521 Ethane 0 0 Propylene 1.975 606974 Channel_A_144.ASC 11/21/2013 8:40:44 Methane 1.525 99176 Ethane 1.671 9245 Propylene 1.986 321258
P3L-1 _145.ASC 11/21/2013 8:54:04 Methane 1.523 90433 Ethane 1.668 7810 Propylene 1.986 273998 Channel_A_146.ASC 11/21/2013 8:59:04 Methane 1.523 53194 Ethane 1.668 4522 Propylene 1.978 499965 P3L-1b _147.ASC 11/21/2013 9:06:08 Methane 1.523 97802 Ethane 1.67 8285 Propylene 1.988 284379 P3L-1b _148.ASC 11/21/2013 9:11:08 Methane 1.525 97009 Ethane 1.67 8284 Propylene 1.986 282050 P3L-1b _149.ASC 11/21/2013 9:16:08 Methane 1.521 98492 Ethane 1.668 8608 Propylene 1.986 268555 P3L-1b _150.ASC 11/21/2013 9:21:08 Methane 1.523 98582 Ethane 1.668 8723 Propylene 1.986 263876
P1L-2 _151.ASC 11/21/2013 9:44:07 Methane 1.525 631 Ethane 0 0 Propylene 1.958 1305181
P1L-2 _152.ASC 11/21/2013 9:49:07 Methane 0 0 Ethane 0 0 Propylene 1.956 1306814
P1L-2 _153.ASC 11/21/2013 9:54:07 Methane 0 0 Ethane 0 0 Propylene 1.956 1310545
P1L-2 _154.ASC 11/21/2013 9:59:07 Methane 0 0 Ethane 0 0 Propylene 1.955 1295583 Channel_A_155.ASC 11/21/2013 10:08:03 Methane 0 0 Ethane 0 0 Propylene 1.958 1302294 Channel_A_156.ASC 11/21/2013 10:11:20 Methane 0 0 Ethane 0 0 Propylene 1.955 1268399 Channel_A_157.ASC 11/21/2013 10:14:55 Methane 0 0 Ethane 0 0 Propylene 1.961 1075557 Channel_A_158.ASC 11/21/2013 10:17:52 Methane 0 0 Ethane 0 0 Propylene 1.961 1012210
P2H-2 _159.ASC 11/21/2013 10:56:05 Methane 0 0 Ethane 0 0 Propylene 1.981 477967
P2H-2 _160.ASC 11/21/2013 11:13:55 Methane 0 0 Ethane 0 0 Propylene 1.981 485970
P2L-2 _161.ASC 11/21/2013 11:31:04 Methane 0 0 Ethane 0 0 Propylene 1.981 439275
P2L-2 _162.ASC 11/21/2013 11:36:04 Methane 0 0 Ethane 0 0 Propylene 1.981 439170
P2L-2 _163.ASC 11/21/2013 11:41:04 Methane 0 0 Ethane 0 0 Propylene 1.981 436590
P2L-2 _164.ASC 11/21/2013 11:46:04 Methane 0 0 Ethane 0 0 Propylene 1.98 437812 Channel_A_165.ASC 11/21/2013 12:31:52 Methane 0 0 Ethane 0 0 Propylene 2.003 15489 Channel_A_166.ASC 11/21/2013 12:34:28 Methane 0 0 Ethane 0 0 Propylene 2.001 16596 Channel_A_167.ASC 11/21/2013 12:37:09 Methane 0 0 Ethane 0 0 Propylene 0 0

# Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area Channel_A_168.ASC 11/21/2013 12:40:17 Methane 1.525 100752 Ethane 1.67 9135 Propylene 1.983 383721
P3H-2 _169.ASC 11/21/2013 12:45:10 Methane 1.525 95453 Ethane 1.67 8555 Propylene 1.986 297094
P3H-2 _170.ASC 11/21/2013 12:50:10 Methane 1.523 95974 Ethane 1.668 8657 Propylene 1.986 279987
P3H-2 _171.ASC 11/21/2013 12:55:10 Methane 1.525 96925 Ethane 1.67 8720 Propylene 1.988 281531
P3H-2 _172.ASC 11/21/2013 13:00:10 Methane 1.52 96532 Ethane 1.666 8656 Propylene 1.983 283868
P3L-2 _173.ASC 11/21/2013 13:17:09 Methane 1.525 99061 Ethane 1.671 8784 Propylene 1.988 276091
P3L-2 _174.ASC 11/21/2013 13:22:09 Methane 1.525 96952 Ethane 1.67 8602 Propylene 1.988 285361
P3L-2 _175.ASC 11/21/2013 13:27:09 Methane 1.523 97440 Ethane 1.668 8698 Propylene 1.986 264834
P3L-2 _176.ASC 11/21/2013 13:32:09 Methane 1.525 96108 Ethane 1.67 8523 Propylene 1.988 286640
P1H-3 _177.ASC 11/21/2013 13:48:09 Methane 1.523 1690 Ethane 0 0 Propylene 1.958 1297699
P1H-3 _178.ASC 11/21/2013 13:53:09 Methane 0 0 Ethane 0 0 Propylene 1.956 1319434
P1H-3 _179.ASC 11/21/2013 13:58:09 Methane 0 0 Ethane 0 0 Propylene 1.956 1312146
P1H-3 _180.ASC 11/21/2013 14:03:09 Methane 0 0 Ethane 0 0 Propylene 1.956 1325167 Channel_A_181.ASC 11/21/2013 14:15:26 Methane 0 0 Ethane 0 0 Propylene 1.956 1269918 Channel_A_182.ASC 11/21/2013 14:17:59 Methane 0 0 Ethane 0 0 Propylene 1.958 1157644 Channel_A_183.ASC 11/21/2013 14:21:29 Methane 0 0 Ethane 0 0 Propylene 1.968 795263 Channel_A_184.ASC 11/21/2013 14:24:26 Methane 0 0 Ethane 0 0 Propylene 1.971 734415
P2L-3 _185.ASC 11/21/2013 14:38:09 Methane 0 0 Ethane 0 0 Propylene 1.981 455987
P2L-3 _186.ASC 11/21/2013 14:43:09 Methane 0 0 Ethane 0 0 Propylene 1.983 435496
P2L-3 _187.ASC 11/21/2013 14:48:09 Methane 0 0 Ethane 0 0 Propylene 1.981 431441
P2L-3 _188.ASC 11/21/2013 14:53:09 Methane 0 0 Ethane 0 0 Propylene 1.983 432839
P3L-3 _189.ASC 11/21/2013 15:06:08 Methane 1.526 96334 Ethane 1.671 8265 Propylene 1.988 297097
P3L-3 _190.ASC 11/21/2013 15:11:08 Methane 1.525 97601 Ethane 1.671 8431 Propylene 1.988 291414
P3L-3 _191.ASC 11/21/2013 15:16:08 Methane 1.525 97865 Ethane 1.67 8522 Propylene 1.988 291210
P3L-3 _192.ASC 11/21/2013 15:21:08 Methane 1.523 98078 Ethane 1.668 8415 Propylene 1.986 292218
P3H-3 _193.ASC 11/21/2013 15:34:14 Methane 1.525 98044 Ethane 1.671 8302 Propylene 1.988 298488
P3H-3 _194.ASC 11/21/2013 15:39:14 Methane 1.525 98008 Ethane 1.67 8369 Propylene 1.988 289776
P3H-3 _195.ASC 11/21/2013 15:44:14 Methane 1.523 97708 Ethane 1.668 8345 Propylene 1.986 287892
P3H-3 _196.ASC 11/21/2013 15:49:14 Methane 1.525 97792 Ethane 1.671 8258 Propylene 1.988 288208
P2H-3 _197.ASC 11/21/2013 16:02:04 Methane 1.526 3171 Ethane 0 0 Propylene 1.981 471065
P2H-3 _198.ASC 11/21/2013 16:07:04 Methane 1.525 688 Ethane 0 0 Propylene 1.98 470290
P2H-3 _199.ASC 11/21/2013 16:12:04 Methane 0 0 Ethane 0 0 Propylene 1.98 469491
P2H-3 _200.ASC 11/21/2013 16:17:04 Methane 0 0 Ethane 0 0 Propylene 1.981 471437
P1L-3 _201.ASC 11/21/2013 16:32:15 Methane 0 0 Ethane 0 0 Propylene 1.955 1298181
P1L-3 _202.ASC 11/21/2013 16:37:15 Methane 0 0 Ethane 0 0 Propylene 1.956 1306426
P1L-3 _203.ASC 11/21/2013 16:42:15 Methane 0 0 Ethane 0 0 Propylene 1.956 1311460
P1L-3 _204.ASC 11/21/2013 16:47:15 Methane 0 0 Ethane 0 0 Propylene 1.956 1298736 Channel_A_205.ASC 11/21/2013 16:55:46 Methane 0 0 Ethane 0 0 Propylene 1.956 1308056 Channel_A_206.ASC 11/21/2013 16:58:41 Methane 0 0 Ethane 0 0 Propylene 1.973 635118 Channel_A_207.ASC 11/21/2013 17:01:37 Methane 0 0 Ethane 0 0 Propylene 1.975 618627 Channel_A_208.ASC 11/21/2013 17:04:15 Methane 0 0 Ethane 0 0 Propylene 1.973 626028 Cal 50 C1 10 C2 _209.ASC 11/21/2013 17:08:32 Methane 1.523 194335 Ethane 1.668 78046 Propylene 0 0 Cal 50 C1 10 C2 _210.ASC 11/21/2013 17:11:35 Methane 1.521 200019 Ethane 1.668 80605 Propylene 2 11982 Cal 50 C1 10 C2 _211.ASC 11/21/2013 17:17:08 Methane 1.523 203009 Ethane 1.668 81775 Propylene 2.001 4638 Cal 20 C1 20 C2 _212.ASC 11/21/2013 17:20:40 Methane 1.525 84100 Ethane 1.666 161968 Propylene 0 0 Cal 50 C1 10 C2 _213.ASC 11/22/2013 7:32:45 Methane 1.521 201041 Ethane 1.666 80921 Propylene 1.998 682 Cal 50 C1 10 C2 _214.ASC 11/22/2013 7:41:37 Methane 1.52 206082 Ethane 1.665 82801 Propylene 0 0 Cal 50 C1 10 C2 _215.ASC 11/22/2013 7:47:30 Methane 1.518 207320 Ethane 1.661 83365 Propylene 0 0 Channel_A_216.ASC 11/22/2013 8:06:04 Methane 1.523 650 Ethane 0 0 Propylene 2.005 9703 Channel_A_217.ASC 11/22/2013 8:40:28 Methane 1.525 609 Ethane 0 0 Propylene 2.008 9488 Channel_A_218.ASC 11/22/2013 9:46:18 Methane 1.526 6509 Ethane 1.67 1825 Propylene 1.996 144200 Channel_A_219.ASC 11/22/2013 9:51:18 Methane 1.518 375332 Ethane 1.666 35840 Propylene 2.008 4764 Channel_A_220.ASC 11/22/2013 9:56:18 Methane 1.518 375344 Ethane 1.666 35976 Propylene 2.008 4733 Channel_A_221.ASC 11/22/2013 10:01:18 Methane 1.516 340053 Ethane 1.665 32400 Propylene 2.005 4144 Channel_A_222.ASC 11/22/2013 10:06:18 Methane 1.518 374102 Ethane 1.665 35978 Propylene 2.006 4415

# Gas Chromatograph Log Inlet Fuel

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area
P4 _223.ASC 11/22/2013 10:09:07 Methane 1.52 53788 Ethane 1.665 5064 Propylene 2.006 685
P4 _224.ASC 11/22/2013 10:13:18 Methane 1.52 36092 Ethane 1.666 3430 Propylene 0 0
P4 _225.ASC 11/22/2013 10:17:20 Methane 1.52 34737 Ethane 1.665 3285 Propylene 0 0
P4 _226.ASC 11/22/2013 10:21:06 Methane 1.52 34398 Ethane 1.665 3217 Propylene 0 0 Channel_A_227.ASC 11/22/2013 10:26:06 Methane 1.515 374730 Ethane 1.663 35554 Propylene 2.005 4534 Channel_A_228.ASC 11/22/2013 11:52:28 Methane 0 0 Ethane 0 0 Propylene 1.99 249929 Channel_A_229.ASC 11/22/2013 11:56:14 Methane 0 0 Ethane 0 0 Propylene 1.988 240364 Channel_A_230.ASC 11/22/2013 12:01:01 Methane 0 0 Ethane 0 0 Propylene 1.988 247619 Channel_A_231.ASC 11/22/2013 12:05:54 Methane 0 0 Ethane 0 0 Propylene 1.986 258306 Channel_A_232.ASC 11/22/2013 12:12:48 Methane 0 0 Ethane 0 0 Propylene 1.983 278691 Channel_A_233.ASC 11/22/2013 12:16:17 Methane 0 0 Ethane 0 0 Propylene 1.985 268062 Channel_A_234.ASC 11/22/2013 12:24:41 Methane 0 0 Ethane 0 0 Propylene 1.983 292581 Channel_A_235.ASC 11/22/2013 12:29:41 Methane 0 0 Ethane 0 0 Propylene 1.985 291816 Channel_A_236.ASC 11/22/2013 12:34:41 Methane 0 0 Ethane 0 0 Propylene 1.986 297517 Channel_A_237.ASC 11/22/2013 12:39:41 Methane 1.523 798 Ethane 0 0 Propylene 1.983 286981 Channel_A_238.ASC 11/22/2013 12:44:41 Methane 1.525 942 Ethane 0 0 Propylene 1.985 295147 Channel_A_239.ASC 11/22/2013 13:26:13 Methane 0 0 Ethane 0 0 Propylene 2 35989 Channel_A_240.ASC 11/22/2013 13:30:47 Methane 0 0 Ethane 0 0 Propylene 1.98 324605 Cal 50 C3= _241.ASC 11/22/2013 13:42:31 Methane 0 0 Ethane 0 0 Propylene 1.971 623425 Cal 50 C3= _242.ASC 11/22/2013 13:45:58 Methane 0 0 Ethane 0 0 Propylene 1.971 625038 Cal 50 C3= _243.ASC 11/22/2013 13:49:10 Methane 0 0 Ethane 0 0 Propylene 1.971 624181 Cal 50 C1 10 C2 _244.ASC 11/22/2013 13:53:32 Methane 1.518 196740 Ethane 1.663 79316 Propylene 1.995 27512 Cal 50 C1 10 C2 _245.ASC 11/22/2013 13:58:16 Methane 1.52 202737 Ethane 1.665 81620 Propylene 1.998 10306 Cal 50 C1 10 C2 _246.ASC 11/22/2013 14:04:50 Methane 1.52 205193 Ethane 1.665 82645 Propylene 1.996 3796 Cal 20 C1 20 C2 _247.ASC 11/22/2013 14:08:24 Methane 1.521 84887 Ethane 1.663 163626 Propylene 0 0 Cal 20 C1 20 C2 _248.ASC 11/22/2013 14:10:49 Methane 1.521 84956 Ethane 1.663 164204 Propylene 0 0 Cal 20 C1 20 C2 _249.ASC 11/22/2013 14:13:38 Methane 1.521 84800 Ethane 1.663 164174 Propylene 0 0

# Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area Channel_B_03.ASC 11/18/2013 10:45:03 Methane 1.395 25038 Ethane 1.513 41264 Propylene 0 0 Channel_B_04.ASC 11/18/2013 11:00:40 Methane 1.398 25356 Ethane 1.515 41002 Propylene 0 0 Channel_B_05.ASC 11/18/2013 11:08:02 Methane 1.4 25648 Ethane 1.516 41568 Propylene 0 0 Channel_B_06.ASC 11/18/2013 11:15:19 Methane 1.398 25926 Ethane 1.515 41748 Propylene 0 0 Channel_B_07.ASC 11/18/2013 11:24:14 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_08.ASC 11/18/2013 11:30:22 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_09.ASC 11/18/2013 11:38:31 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_10.ASC 11/18/2013 11:45:03 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_11.ASC 11/18/2013 11:48:21 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_12.ASC 11/18/2013 11:51:37 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_13.ASC 11/18/2013 12:56:13 Methane 1.425 2769 Ethane 0 0 Propylene 1.773 63146 Channel_B_14.ASC 11/18/2013 13:00:56 Methane 1.423 1612 Ethane 0 0 Propylene 1.771 62849 Channel_B_15.ASC 11/18/2013 13:05:22 Methane 1.423 1742 Ethane 0 0 Propylene 1.771 62897 Channel_B_16.ASC 11/18/2013 13:12:48 Methane 1.421 1409 Ethane 0 0 Propylene 1.771 37335 Channel_B_17.ASC 11/18/2013 13:17:23 Methane 1.421 1278 Ethane 0 0 Propylene 1.77 37098 Channel_B_18.ASC 11/18/2013 13:21:16 Methane 1.421 1226 Ethane 0 0 Propylene 1.771 37145 Channel_B_19.ASC 11/18/2013 13:27:58 Methane 0 0 Ethane 0 0 Propylene 1.773 22632 Channel_B_20.ASC 11/18/2013 13:31:52 Methane 0 0 Ethane 0 0 Propylene 1.773 22565 Channel_B_21.ASC 11/18/2013 13:34:46 Methane 0 0 Ethane 0 0 Propylene 1.773 22552 Channel_B_22.ASC 11/18/2013 13:39:35 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_23.ASC 11/18/2013 13:42:08 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_24.ASC 11/18/2013 13:45:53 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_25.ASC 11/18/2013 15:35:45 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_26.ASC 11/19/2013 6:51:40 Methane 1.405 26745 Ethane 1.523 42316 Propylene 0 0 Channel_B_27.ASC 11/19/2013 7:05:04 Methane 1.408 27077 Ethane 1.525 43254 Propylene 0 0 Channel_B_28.ASC 11/19/2013 7:13:11 Methane 1.406 26514 Ethane 1.523 42866 Propylene 0 0 Channel_B_29.ASC 11/19/2013 7:21:34 Methane 0 0 Ethane 1.568 110687 Propylene 1.77 36574 Channel_B_30.ASC 11/19/2013 7:25:38 Methane 0 0 Ethane 0 0 Propylene 1.771 37038 Channel_B_31.ASC 11/19/2013 7:29:26 Methane 0 0 Ethane 0 0 Propylene 1.773 37014 Channel_B_32.ASC 11/19/2013 7:35:37 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_33.ASC 11/19/2013 7:41:29 Methane 0 0 Ethane 0 0 Propylene 1.803 30232 Channel_B_34.ASC 11/19/2013 7:46:46 Methane 1.416 1299 Ethane 0 0 Propylene 0 0 Channel_B_35.ASC 11/19/2013 7:56:09 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_36.ASC 11/19/2013 8:03:32 Methane 1.421 1034 Ethane 0 0 Propylene 0 0 Channel_B_37.ASC 11/19/2013 8:32:02 Methane 1.433 1346 Ethane 0 0 Propylene 0 0 Channel_B_38.ASC 11/19/2013 8:35:16 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_39.ASC 11/19/2013 8:39:03 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_40.ASC 11/19/2013 8:42:28 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_41.ASC 11/19/2013 8:47:46 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_42.ASC 11/19/2013 9:00:52 Methane 0 0 Ethane 0 0 Propylene 1.793 1499
S1 B_43.ASC 11/19/2013 9:08:14 Methane 0 0 Ethane 0 0 Propylene 1.795 1635
S1 B_44.ASC 11/19/2013 9:15:01 Methane 0 0 Ethane 0 0 Propylene 1.795 1404
S1 B_45.ASC 11/19/2013 9:20:01 Methane 0 0 Ethane 0 0 Propylene 0 0
S1 B_46.ASC 11/19/2013 9:25:01 Methane 0 0 Ethane 0 0 Propylene 1.791 1626
S1 B_47.ASC 11/19/2013 9:30:01 Methane 0 0 Ethane 0 0 Propylene 0 0
S2 B_48.ASC 11/19/2013 9:45:08 Methane 1.428 904 Ethane 0 0 Propylene 1.796 3184
S2 B_49.ASC 11/19/2013 9:50:08 Methane 0 0 Ethane 0 0 Propylene 1.75 825
S2 B_50.ASC 11/19/2013 9:55:08 Methane 1.425 675 Ethane 0 0 Propylene 1.795 832
S2 B_51.ASC 11/19/2013 10:00:08 Methane 0 0 Ethane 0 0 Propylene 1.791 850 S1 Bag B_52.ASC 11/19/2013 10:09:28 Methane 1.426 585 Ethane 0 0 Propylene 1.79 3009 S1 Bag B_53.ASC 11/19/2013 10:13:32 Methane 0 0 Ethane 0 0 Propylene 1.778 2506 S2 Bag B_54.ASC 11/19/2013 10:20:27 Methane 1.425 618 Ethane 0 0 Propylene 0 0

# Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area S2 Bag B_55.ASC 11/19/2013 10:24:56 Methane 1.421 495 Ethane 0 0 Propylene 1.761 513 Channel_B_56.ASC 11/19/2013 10:42:24 Methane 0 0 Ethane 1.586 251 Propylene 0 0 Channel_B_57.ASC 11/19/2013 10:46:06 Methane 1.423 705 Ethane 1.565 263 Ethane 1.593 208 Channel_B_58.ASC 11/19/2013 10:55:21 Methane 1.423 803 Ethane 0 0 Propylene 0 0 Channel_B_59.ASC 11/19/2013 11:12:34 Methane 1.416 337 Ethane 1.545 498 Propylene 1.791 372 Channel_B_60.ASC 11/19/2013 11:17:26 Methane 1.425 821 Ethane 1.498 632 Propylene 1.781 1149
S3 B_61.ASC 11/19/2013 11:29:01 Methane 1.423 1147 Ethane 0 0 Propylene 1.773 3481
S3 B_62.ASC 11/19/2013 11:34:01 Methane 1.413 268 Ethane 1.505 484 Propylene 1.773 9757 Channel_B_63.ASC 11/19/2013 11:39:01 Methane 1.416 829 Ethane 0 0 Propylene 1.755 778
S3 B_64.ASC 11/19/2013 11:44:01 Methane 1.405 550 Ethane 1.506 212 Propylene 1.735 1233
S3 B_65.ASC 11/19/2013 11:50:05 Methane 1.408 581 Ethane 0 0 Propylene 1.771 8218 Channel_B_66.ASC 11/19/2013 11:55:27 Methane 1.411 650 Ethane 1.5 893 Propylene 1.771 5663 Channel_B_67.ASC 11/19/2013 11:58:52 Methane 1.418 1079 Ethane 1.493 1143 Propylene 1.765 9366 Channel_B_68.ASC 11/19/2013 12:04:04 Methane 1.391 684 Ethane 1.548 214 Propylene 1.793 309 Channel_B_69.ASC 11/19/2013 12:45:51 Methane 0 0 Ethane 1.498 798 Propylene 1.78 217 Channel_B_70.ASC 11/19/2013 12:49:54 Methane 1.41 698 Ethane 0 0 Propylene 1.778 211 Channel_B_71.ASC 11/19/2013 12:57:06 Methane 1.411 1378 Ethane 0 0 Propylene 1.77 1467
S4 B_72.ASC 11/19/2013 13:36:06 Methane 1.415 627 Ethane 0 0 Propylene 1.765 6391
S4 B_73.ASC 11/19/2013 13:41:06 Methane 1.41 783 Ethane 0 0 Propylene 1.761 5240
S4 B_74.ASC 11/19/2013 13:46:06 Methane 1.41 918 Ethane 0 0 Propylene 0 0
S4 B_75.ASC 11/19/2013 13:51:06 Methane 1.413 790 Ethane 0 0 Propylene 1.763 7911
S5 B_76.ASC 11/19/2013 14:18:51 Methane 1.408 844 Ethane 1.491 787 Propylene 1.763 18023
S5 B_77.ASC 11/19/2013 14:23:51 Methane 1.403 225 Ethane 1.491 233 Propylene 1.756 1845
S5 B_78.ASC 11/19/2013 14:28:51 Methane 1.405 320 Ethane 1.491 364 Propylene 1.76 11516
S5 B_79.ASC 11/19/2013 14:33:51 Methane 1.413 681 Ethane 0 0 Propylene 1.761 10105
S6 B_80.ASC 11/19/2013 14:56:04 Methane 1.41 350 Ethane 0 0 Propylene 1.773 440
S6 B_81.ASC 11/19/2013 15:01:04 Methane 1.413 745 Ethane 0 0 Propylene 1.731 954
S6 B_82.ASC 11/19/2013 15:06:04 Methane 1.405 746 Ethane 0 0 Propylene 0 0
S6 B_83.ASC 11/19/2013 15:11:04 Methane 1.415 827 Ethane 0 0 Propylene 1.733 591 Channel_B_84.ASC 11/19/2013 15:21:12 Methane 1.406 678 Ethane 0 0 Propylene 1.788 1614 S3 Bag B_85.ASC 11/19/2013 15:24:42 Methane 1.411 789 Ethane 1.535 231 Propylene 1.766 15810 S3 Bag B_86.ASC 11/19/2013 15:27:43 Methane 1.416 911 Ethane 1.495 366 Propylene 1.765 16278 S4 Bag B_87.ASC 11/19/2013 15:31:02 Methane 1.416 1225 Ethane 0 0 Propylene 1.765 3538 S4 Bag B_88.ASC 11/19/2013 15:34:09 Methane 0 0 Ethane 0 0 Propylene 1.768 3408 S5 Bag B_89.ASC 11/19/2013 15:38:14 Methane 1.406 848 Ethane 1.498 1022 Propylene 1.766 23525 S5 Bag B_90.ASC 11/19/2013 15:41:12 Methane 1.41 681 Ethane 1.498 1390 Propylene 1.766 24178 Channel_B_91.ASC 11/19/2013 15:45:08 Methane 0 0 Ethane 0 0 Propylene 0 0
P1H-1 B_92.ASC 11/19/2013 15:50:08 Methane 1.42 564 Ethane 0 0 Propylene 1.78 2299
P1H-1 B_93.ASC 11/19/2013 15:55:08 Methane 1.418 482 Ethane 1.525 263 Propylene 1.745 2754
P1H-1 B_94.ASC 11/19/2013 16:00:08 Methane 1.418 732 Ethane 0 0 Propylene 1.781 2249 S6 Bag B_95.ASC 11/19/2013 16:10:57 Methane 0 0 Ethane 0 0 Propylene 1.783 4317 S6 Bag B_96.ASC 11/19/2013 16:14:33 Methane 1.416 586 Ethane 0 0 Propylene 1.771 1559 P1H-1 Bag B_97.ASC 11/19/2013 16:20:07 Methane 1.418 572 Ethane 0 0 Propylene 1.766 1625 Channel_B_98.ASC 11/19/2013 16:23:39 Methane 1.423 718 Ethane 0 0 Propylene 1.776 1339 Channel_B_99.ASC 11/20/2013 10:59:25 Methane 1.41 26014 Ethane 1.526 41137 Propylene 0 0 Channel_B_100.ASC 11/20/2013 11:04:12 Methane 1.41 25544 Ethane 1.526 41609 Propylene 0 0 Channel_B_101.ASC 11/20/2013 13:46:27 Methane 1.431 1387 Ethane 1.543 764 Propylene 1.781 22833
P1H-2 _102.ASC 11/20/2013 14:09:11 Methane 1.426 742 Ethane 0 0 Propylene 1.798 1955
P1H-2 _103.ASC 11/20/2013 14:14:11 Methane 1.43 413 Ethane 0 0 Propylene 0 0
P1H-2 _104.ASC 11/20/2013 14:19:11 Methane 1.435 590 Ethane 0 0 Propylene 1.798 2297
P1H-2 _105.ASC 11/20/2013 14:24:11 Methane 1.438 749 Ethane 0 0 Propylene 0 0
P1L-1 _106.ASC 11/20/2013 14:57:11 Methane 1.426 747 Ethane 0 0 Propylene 0 0

# Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area
P1L-1 _107.ASC 11/20/2013 15:02:11 Methane 1.433 674 Ethane 0 0 Propylene 0 0
P1L-1 _108.ASC 11/20/2013 15:07:11 Methane 1.436 625 Ethane 0 0 Propylene 1.756 432
P1L-1 _109.ASC 11/20/2013 15:12:11 Methane 1.43 792 Ethane 0 0 Propylene 1.763 611 P1H-2 Bag _110.ASC 11/20/2013 15:21:30 Methane 1.436 797 Ethane 0 0 Propylene 0 0 P1L-1 Bag _112.ASC 11/20/2013 15:30:29 Methane 1.438 790 Ethane 0 0 Propylene 0 0 P1L-1 Bag _113.ASC 11/20/2013 15:34:17 Methane 1.433 763 Ethane 0 0 Propylene 0 0
P2H-1 _114.ASC 11/20/2013 16:01:23 Methane 1.43 755 Ethane 0 0 Propylene 1.763 5925
P2H-1 _115.ASC 11/20/2013 16:06:23 Methane 1.431 1129 Ethane 0 0 Propylene 1.786 490944 P2H-1b _116.ASC 11/20/2013 16:37:10 Methane 1.43 404 Ethane 0 0 Propylene 1.761 1446 P2H-1b _117.ASC 11/20/2013 16:42:10 Methane 1.436 590 Ethane 0 0 Propylene 1.765 1155 P2H-1b _118.ASC 11/20/2013 16:47:10 Methane 1.436 592 Ethane 0 0 Propylene 1.803 928 P2H-1b _119.ASC 11/20/2013 16:52:10 Methane 1.433 881 Ethane 0 0 Propylene 1.758 1305
P2L-1 _120.ASC 11/20/2013 17:23:01 Methane 1.436 236 Ethane 1.511 602 Propylene 1.796 5478 Channel_B_121.ASC 11/20/2013 17:28:01 Methane 1.43 726 Ethane 0 0 Propylene 1.793 1212 Channel_B_122.ASC 11/20/2013 17:33:01 Methane 1.431 710 Ethane 0 0 Propylene 1.791 1567 P2L-1b _123.ASC 11/20/2013 17:38:01 Methane 1.428 679 Ethane 0 0 Propylene 1.791 882 P2L-1b _124.ASC 11/20/2013 17:53:38 Methane 1.428 656 Ethane 0 0 Propylene 1.8 702 P2H-1b Bag _125.ASC 11/20/2013 18:36:18 Methane 1.426 723 Ethane 0 0 Propylene 1.795 529 P2H-1b Bag _126.ASC 11/20/2013 18:38:58 Methane 1.428 722 Ethane 0 0 Propylene 1.788 279 P2L-1b Bag _127.ASC 11/20/2013 18:42:17 Methane 1.438 703 Ethane 0 0 Propylene 1.795 743 P2L-1b Bag _128.ASC 11/20/2013 18:45:02 Methane 1.425 655 Ethane 0 0 Propylene 1.781 894 Channel_B_129.ASC 11/20/2013 18:56:10 Methane 0 0 Ethane 0 0 Propylene 1.806 1188
P3H-1 _130.ASC 11/20/2013 19:18:09 Methane 1.436 2710 Ethane 1.52 249 Propylene 1.801 4932
P3H-1 _131.ASC 11/20/2013 19:23:09 Methane 0 0 Ethane 0 0 Propylene 1.805 666
P3H-1 _132.ASC 11/20/2013 19:28:09 Methane 1.436 1342 Ethane 0 0 Propylene 1.805 586
P3H-1 _133.ASC 11/20/2013 19:33:09 Methane 0 0 Ethane 0 0 Propylene 1.806 530 Channel_B_134.ASC 11/20/2013 19:38:04 Methane 1.42 24883 Ethane 1.535 40325 Propylene 1.74 304 P3H-1 Bag _135.ASC 11/20/2013 19:44:33 Methane 1.425 1952 Ethane 1.54 1748 Propylene 1.745 751 P3H-1 Bag _136.ASC 11/20/2013 19:47:31 Methane 1.421 1198 Ethane 1.541 564 Propylene 1.746 3795 Channel_B_137.ASC 11/21/2013 6:51:41 Methane 1.421 25919 Ethane 1.54 40864 Propylene 0 0 Channel_B_138.ASC 11/21/2013 6:59:48 Methane 1.423 26483 Ethane 1.541 41663 Propylene 0 0 Channel_B_139.ASC 11/21/2013 7:10:29 Methane 1.42 3483 Ethane 1.526 9600 Propylene 0 0 Channel_B_140.ASC 11/21/2013 7:31:01 Methane 0 0 Ethane 1.558 740 Propylene 1.803 2206333 Channel_B_141.ASC 11/21/2013 7:50:04 Methane 0 0 Ethane 0 0 Propylene 1.798 547181 Channel_B_142.ASC 11/21/2013 7:58:59 Methane 0 0 Ethane 1.615 555 Propylene 1.795 27199 Channel_B_143.ASC 11/21/2013 8:05:23 Methane 0 0 Ethane 0 0 Propylene 1.795 10751 Channel_B_144.ASC 11/21/2013 8:40:44 Methane 1.438 1360 Ethane 0 0 Propylene 1.803 3799 Channel_B_145.ASC 11/21/2013 8:54:04 Methane 1.431 1620 Ethane 0 0 Propylene 1.801 1809 Channel_B_146.ASC 11/21/2013 8:59:04 Methane 1.435 894 Ethane 0 0 Propylene 1.79 875 P3L-1b _147.ASC 11/21/2013 9:06:08 Methane 0 0 Ethane 0 0 Propylene 1.803 1117 P3L-1b _148.ASC 11/21/2013 9:11:08 Methane 0 0 Ethane 0 0 Propylene 1.803 1291 P3L-1b _149.ASC 11/21/2013 9:16:08 Methane 1.438 1113 Ethane 0 0 Propylene 1.793 221 P3L-1b _150.ASC 11/21/2013 9:21:08 Methane 0 0 Ethane 0 0 Propylene 1.8 532
P1L-2 _151.ASC 11/21/2013 9:44:07 Methane 0 0 Ethane 0 0 Propylene 1.756 2914
P1L-2 _152.ASC 11/21/2013 9:49:07 Methane 1.436 1070 Ethane 0 0 Propylene 1.751 1290
P1L-2 _153.ASC 11/21/2013 9:54:07 Methane 0 0 Ethane 0 0 Propylene 1.761 1308
P1L-2 _154.ASC 11/21/2013 9:59:07 Methane 1.435 334 Ethane 0 0 Propylene 1.753 1343 P3L-1b Bag _155.ASC 11/21/2013 10:08:03 Methane 1.43 454 Ethane 0 0 Propylene 1.746 2128 P3L-1b Bag _156.ASC 11/21/2013 10:11:20 Methane 1.431 1127 Ethane 0 0 Propylene 1.741 1347 P1L-2 Bag _157.ASC 11/21/2013 10:14:55 Methane 1.433 793 Ethane 0 0 Propylene 1.743 1284 P1L-2 Bag _158.ASC 11/21/2013 10:17:52 Methane 1.431 797 Ethane 0 0 Propylene 1.741 1153
P2H-2 _159.ASC 11/21/2013 10:56:05 Methane 1.438 570 Ethane 0 0 Propylene 1.81 5046

# Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area
P2H-2 _160.ASC 11/21/2013 11:13:55 Methane 1.435 1313 Ethane 0 0 Propylene 0 0
P2L-2 _161.ASC 11/21/2013 11:31:04 Methane 1.431 1001 Ethane 0 0 Propylene 1.808 1038
P2L-2 _162.ASC 11/21/2013 11:36:04 Methane 0 0 Ethane 0 0 Propylene 1.808 834
P2L-2 _163.ASC 11/21/2013 11:41:04 Methane 1.433 773 Ethane 1.521 267 Propylene 1.796 2010
P2L-2 _164.ASC 11/21/2013 11:46:04 Methane 1.431 691 Ethane 0 0 Propylene 1.803 254 P2H-2 Bag _165.ASC 11/21/2013 12:31:52 Methane 1.436 678 Ethane 0 0 Propylene 1.808 541 P2H-2 Bag _166.ASC 11/21/2013 12:34:28 Methane 1.436 697 Ethane 0 0 Propylene 1.79 382 P2L-2 Bag _167.ASC 11/21/2013 12:37:09 Methane 1.438 704 Ethane 0 0 Propylene 1.793 1446 P2L-2 Bag _168.ASC 11/21/2013 12:40:17 Methane 1.436 857 Ethane 0 0 Propylene 1.796 1437
P3H-2 _169.ASC 11/21/2013 12:45:10 Methane 0 0 Ethane 0 0 Propylene 1.808 422
P3H-2 _170.ASC 11/21/2013 12:50:10 Methane 0 0 Ethane 0 0 Propylene 1.805 1082
P3H-2 _171.ASC 11/21/2013 12:55:10 Methane 0 0 Ethane 0 0 Propylene 1.806 1085
P3H-2 _172.ASC 11/21/2013 13:00:10 Methane 0 0 Ethane 0 0 Propylene 1.805 860
P3L-2 _173.ASC 11/21/2013 13:17:09 Methane 0 0 Ethane 0 0 Propylene 1.81 1202
P3L-2 _174.ASC 11/21/2013 13:22:09 Methane 1.438 1007 Ethane 0 0 Propylene 0 0
P3L-2 _175.ASC 11/21/2013 13:27:09 Methane 1.433 930 Ethane 0 0 Propylene 1.803 207
P3L-2 _176.ASC 11/21/2013 13:32:09 Methane 1.435 916 Ethane 0 0 Propylene 1.765 245
P1H-3 _177.ASC 11/21/2013 13:48:09 Methane 1.436 1180 Ethane 0 0 Propylene 1.76 3382
P1H-3 _178.ASC 11/21/2013 13:53:09 Methane 1.43 972 Ethane 0 0 Propylene 1.808 2333
P1H-3 _179.ASC 11/21/2013 13:58:09 Methane 1.436 825 Ethane 0 0 Propylene 1.761 285
P1H-3 _180.ASC 11/21/2013 14:03:09 Methane 1.436 1520 Ethane 0 0 Propylene 1.758 2602 P3H-2 Bag _181.ASC 11/21/2013 14:15:26 Methane 1.435 832 Ethane 0 0 Propylene 1.751 2904 P3H-2 Bag _182.ASC 11/21/2013 14:17:59 Methane 1.431 913 Ethane 0 0 Propylene 1.745 1150 P3L-2 Bag _183.ASC 11/21/2013 14:21:29 Methane 1.433 780 Ethane 0 0 Propylene 1.75 263 P3L-2 Bag _184.ASC 11/21/2013 14:24:26 Methane 1.433 766 Ethane 0 0 Propylene 0 0
P2L-3 _185.ASC 11/21/2013 14:38:09 Methane 1.438 687 Ethane 0 0 Propylene 1.808 1337
P2L-3 _186.ASC 11/21/2013 14:43:09 Methane 0 0 Ethane 0 0 Propylene 1.806 253
P2L-3 _187.ASC 11/21/2013 14:48:09 Methane 1.438 886 Ethane 0 0 Propylene 1.806 208
P2L-3 _188.ASC 11/21/2013 14:53:09 Methane 0 0 Ethane 0 0 Propylene 1.803 1353
P3L-3 _189.ASC 11/21/2013 15:06:08 Methane 0 0 Ethane 0 0 Propylene 1.811 543
P3L-3 _190.ASC 11/21/2013 15:11:08 Methane 0 0 Ethane 0 0 Propylene 1.805 385
P3L-3 _191.ASC 11/21/2013 15:16:08 Methane 0 0 Ethane 0 0 Propylene 1.811 247
P3L-3 _192.ASC 11/21/2013 15:21:08 Methane 0 0 Ethane 1.53 227 Propylene 1.803 202
P3H-3 _193.ASC 11/21/2013 15:34:14 Methane 0 0 Ethane 0 0 Propylene 1.811 2088
P3H-3 _194.ASC 11/21/2013 15:39:14 Methane 0 0 Ethane 0 0 Propylene 1.813 584
P3H-3 _195.ASC 11/21/2013 15:44:14 Methane 1.438 1649 Ethane 1.525 243 Propylene 1.806 2097
P3H-3 _196.ASC 11/21/2013 15:49:14 Methane 0 0 Ethane 0 0 Propylene 1.806 1961
P2H-3 _197.ASC 11/21/2013 16:02:04 Methane 0 0 Ethane 0 0 Propylene 1.81 1971
P2H-3 _198.ASC 11/21/2013 16:07:04 Methane 1.438 618 Ethane 0 0 Propylene 1.808 1188
P2H-3 _199.ASC 11/21/2013 16:12:04 Methane 1.435 911 Ethane 0 0 Propylene 1.745 1777
P2H-3 _200.ASC 11/21/2013 16:17:04 Methane 0 0 Ethane 0 0 Propylene 1.81 2039
P1L-3 _201.ASC 11/21/2013 16:32:15 Methane 1.433 1000 Ethane 0 0 Propylene 1.806 2517
P1L-3 _202.ASC 11/21/2013 16:37:15 Methane 0 0 Ethane 0 0 Propylene 1.81 1099
P1L-3 _203.ASC 11/21/2013 16:42:15 Methane 0 0 Ethane 0 0 Propylene 1.811 1297
P1L-3 _204.ASC 11/21/2013 16:47:15 Methane 0 0 Ethane 0 0 Propylene 1.813 1282 P2L-3 Bag _205.ASC 11/21/2013 16:55:46 Methane 0 0 Ethane 0 0 Propylene 1.808 1738 P2L-3 Bag _206.ASC 11/21/2013 16:58:41 Methane 1.431 591 Ethane 0 0 Propylene 1.791 771 P3L-3 Bag _207.ASC 11/21/2013 17:01:37 Methane 1.436 826 Ethane 0 0 Propylene 1.758 272 P3L-3 Bag _208.ASC 11/21/2013 17:04:15 Methane 1.43 795 Ethane 0 0 Propylene 1.761 418 P3H-3 Bag _209.ASC 11/21/2013 17:08:32 Methane 1.433 1192 Ethane 0 0 Propylene 1.735 3398 P3H-3 Bag _210.ASC 11/21/2013 17:11:35 Methane 1.436 1259 Ethane 0 0 Propylene 1.751 236 P1L-3 Bag _211.ASC 11/21/2013 17:17:08 Methane 0 0 Ethane 0 0 Propylene 0 0

# Gas Chromatograph Outlet Log

Testing by TRC, Austin, Texas Run File Date Time Methane RT Area Ethane RT Area Propylene RT Area P1L-3 Bag _212.ASC 11/21/2013 17:20:40 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_213.ASC 11/22/2013 7:32:45 Methane 0 0 Ethane 0 0 Propylene 1.831 21872 Channel_B_214.ASC 11/22/2013 7:41:37 Methane 0 0 Ethane 1.596 290 Propylene 1.833 21674 Channel_B_215.ASC 11/22/2013 7:47:30 Methane 0 0 Ethane 0 0 Propylene 1.83 21252 Channel_B_216.ASC 11/22/2013 8:06:04 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_217.ASC 11/22/2013 8:40:28 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_218.ASC 11/22/2013 9:46:18 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_219.ASC 11/22/2013 9:51:18 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_220.ASC 11/22/2013 9:56:18 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_221.ASC 11/22/2013 10:01:18 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_222.ASC 11/22/2013 10:06:18 Methane 0 0 Ethane 0 0 Propylene 0 0
P4 _223.ASC 11/22/2013 10:09:07 Methane 0 0 Ethane 0 0 Propylene 0 0
P4 _224.ASC 11/22/2013 10:13:18 Methane 0 0 Ethane 0 0 Propylene 0 0
P4 _225.ASC 11/22/2013 10:17:20 Methane 0 0 Ethane 0 0 Propylene 0 0
P4 _226.ASC 11/22/2013 10:21:06 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_227.ASC 11/22/2013 10:26:06 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_228.ASC 11/22/2013 11:52:28 Methane 1.436 1064 Ethane 0 0 Propylene 1.795 7809 Channel_B_229.ASC 11/22/2013 11:56:14 Methane 1.43 1584 Ethane 1.528 750 Propylene 1.793 364914 Channel_B_230.ASC 11/22/2013 12:01:01 Methane 0 0 Ethane 0 0 Propylene 1.805 813 Channel_B_231.ASC 11/22/2013 12:05:54 Methane 1.428 952 Ethane 0 0 Propylene 1.806 601 Channel_B_232.ASC 11/22/2013 12:12:48 Methane 1.428 885 Ethane 0 0 Propylene 0 0 Channel_B_233.ASC 11/22/2013 12:16:17 Methane 1.43 437 Ethane 0 0 Propylene 0 0 Channel_B_234.ASC 11/22/2013 12:24:41 Methane 1.438 1161 Ethane 0 0 Propylene 1.791 3110 Channel_B_235.ASC 11/22/2013 12:29:41 Methane 1.431 812 Ethane 0 0 Propylene 1.798 888 Channel_B_236.ASC 11/22/2013 12:34:41 Methane 0 0 Ethane 1.521 1083 Propylene 1.795 26140 Channel_B_237.ASC 11/22/2013 12:39:41 Methane 1.435 747 Ethane 0 0 Propylene 1.803 269 Channel_B_238.ASC 11/22/2013 12:44:41 Methane 1.436 1039 Ethane 1.523 704 Propylene 1.793 9421 Channel_B_239.ASC 11/22/2013 13:26:13 Methane 0 0 Ethane 1.516 897 Propylene 1.733 17048 Channel_B_240.ASC 11/22/2013 13:30:47 Methane 1.428 1125 Ethane 0 0 Propylene 1.79 17344 Channel_B_241.ASC 11/22/2013 13:42:31 Methane 0 0 Ethane 0 0 Propylene 1.793 22494 Channel_B_242.ASC 11/22/2013 13:45:58 Methane 0 0 Ethane 0 0 Propylene 1.793 22082 Channel_B_243.ASC 11/22/2013 13:49:10 Methane 1.431 305 Ethane 0 0 Propylene 1.795 21915 Channel_B_244.ASC 11/22/2013 13:53:32 Methane 0 0 Ethane 0 0 Propylene 1.821 61188 Channel_B_245.ASC 11/22/2013 13:58:16 Methane 0 0 Ethane 1.558 267 Propylene 0 0 Channel_B_246.ASC 11/22/2013 14:04:50 Methane 0 0 Ethane 1.565 215 Propylene 0 0 Channel_B_247.ASC 11/22/2013 14:08:24 Methane 1.438 271 Ethane 0 0 Propylene 0 0 Channel_B_248.ASC 11/22/2013 14:10:49 Methane 0 0 Ethane 0 0 Propylene 0 0 Channel_B_249.ASC 11/22/2013 14:13:38 Methane 0 0 Ethane 0 0 Propylene 0 0

# Method 18 Inlet Fuel Initial Calibration

7HVWLQJE\75&$XVWLQ7H[DV Compound Low Level Calibration Value (%) Low Level Injection 1 (Area Counts) Low Level Injection 2 (Area Counts) Low Level Injection 3 (Area Counts) Low Level Average

(Area Counts) Precision (Percent of Average) Precision within 5%? GC Run Number  0HWKDQH       <(6
 (WKDQH       <(6

 3URS\OHQH       <(6   0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6   0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6

Compound Mid Level Calibration Value (%) Mid Level Injection 1 (Area Counts) Mid Level Injection 2 (Area Counts) Mid Level Injection 3 (Area Counts) Mid Level Average

(Area Counts) Precision (Percent of Average) Precision within 5%? GC Run Number  0HWKDQH       <(6
 (WKDQH       <(6

 3URS\OHQH       <(6   0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6   0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6

Compound High Level Calibration Value (%) High Level Injection 1 (Area Counts) High Level Injection 2 (Area Counts) High Level Injection 3 (Area Counts) High Level Average

(Area Counts) Precision (Percent of Average) Precision within 5%? GC Run Number  0HWKDQH       <(6
 (WKDQH       <(6

 3URS\OHQH       <(6   0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6   0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6

# Method 18 Inlet Fuel Curves

Initial Calibration Curve Final Calibration Curve (Combination of all Calibrations ) Compound Slope (m) R 2 Compound Slope (m) R 2
1 Methane 0.000242 0.999956 1 Methane 0.000242 0.999956 2 Ethane 0.000123 0.999971 2 Ethane 0.000123 0.999971 3 Propylene 0.000076 0.999866 3 Propylene 0.000076 0.999866
4 4 5 Methane 0.000242 0.999956 5 Methane 0.000242 0.999956 6 Ethane 0.000123 0.999971 6 Ethane 0.000123 0.999971 7 Propylene 0.000076 0.999866 7 Propylene 0.000076 0.999866 8 8 9 Methane 0.000242 0.999956 9 Methane 0.000242 0.999956 10 Ethane 0.000123 0.999971 10 Ethane 0.000123 0.999971 11 Propylene 0.000076 0.999866 11 Propylene 0.000076 0.999866 12 12 13 Methane 0.000242 0.999956 13 Methane 0.000242 0.999956 14 Ethane 0.000123 0.999971 14 Ethane 0.000123 0.999971 15 Propylene 0.000076 0.999866 15 Propylene 0.000076 0.999866 0 10 20 30 40 50 60 70 80 90

0.0 200000.0 400000.0 600000.0 800000.0 1000000.0 1200000.0Concentrations (ppmv)

Area Counts Calibration Curves

Methane

Ethane Propylene

Methane

Ethane Propylene

Methane

Ethane Propylene

Methane

Ethane Propylene Linear (Methane) Linear (Ethane) Linear (Propylene) Linear () Linear (Methane) Linear (Ethane) Linear (Propylene) Linear () Linear (Methane) Linear (Ethane) Linear (Propylene) Linear () Linear (Methane) Linear (Ethane) Linear (Propylene)



### Testing by TRC, Austin, Texas

# Method 18 Inlet Fuel Test Run Data

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 6 (WKDQH 3URS\OHQH        ,1,7,$/

0HWKDQH 6 (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 6 (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 6 (WKDQH 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 6 (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 6 (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 3+ (WKDQH 3URS\OHQH      ,1,7,$/

0HWKDQH 3+ (WKDQH 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 3/ (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 3+ (WKDQH 3URS\OHQH     ,1,7,$/

0HWKDQH 3+E (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 3/ (WKDQH 3URS\OHQH    ,1,7,$/

# Method 18 Inlet Fuel Test Run Data (2)

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 3/E (WKDQH 3URS\OHQH     ,1,7,$/

0HWKDQH       ,1,7,$/ 3+ (WKDQH       ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/E (WKDQH       ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH 3/ (WKDQH 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 3+ (WKDQH 3URS\OHQH     ,1,7,$/

0HWKDQH 3/ (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3+ (WKDQH       ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH       ,1,7,$/ 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 3+ (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 3/ (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH       ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3+ (WKDQH       ,1,7,$/ 3URS\OHQH       ,1,7,$/

# Method 18 Inlet Fuel Test Run Data (3)

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (%) Curve Used (Initial or Final) GC Run Number 0HWKDQH 3+ (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH 3/ (WKDQH 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3 (WKDQH       ,1,7,$/ 3URS\OHQH

0HWKDQH (WKDQH 3URS\OHQH

## Method 18 Outlet 

# Initial Calibration

7HVWLQJE\75&$XVWLQ7H[DV Compound Low Level Calibration

Value (ppmv) Low Level Injection 1 (Area Counts) Low Level Injection 2 (Area Counts) Low Level Injection 3 (Area Counts) Low Level Average

(Area Counts) Precision (Percent of Average) Precision within 5%? GC Run Number  0HWKDQH       <(6
 (WKDQH       <(6

 3URS\OHQH       <(6   0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6   0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6

Compound Mid Level Calibration

Value (ppmv) Mid Level Injection 1 (Area Counts) Mid Level Injection 2 (Area Counts) Mid Level Injection 3 (Area Counts) Mid Level Average

(Area Counts) Precision (Percent of Average) Precision within 5%? GC Run Number  0HWKDQH       <(6
 (WKDQH       <(6

 3URS\OHQH       <(6   0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6   0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6

Compound High Level Calibration

Value (ppmv) High Level Injection 1 (Area Counts) High Level Injection 2 (Area Counts) High Level Injection 3 (Area Counts) High Level Average

(Area Counts) Precision (Percent of Average) Precision within 5%? GC Run Number  0HWKDQH       <(6
 (WKDQH       <(6

 3URS\OHQH       <(6   0HWKDQH       <(6

 (WKDQH       <(6

 3URS\OHQH       <(6



 0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6   0HWKDQH       <(6  (WKDQH       <(6  3URS\OHQH       <(6

## Method 18 Outlet 

# Curves

Initial Calibration Curve Final Calibration Curve (Combination of all Calibrations ) Compound Slope (m) R 2 Compound Slope (m) R 2
1 Methane 0.003739 0.999365 1 Methane 0.003739 0.999365 2 Ethane 0.002299 0.999820 2 Ethane 0.002299 0.999820 3 Propylene 0.001349 0.999999 3 Propylene 0.001349 0.999999
4 4 5 Methane 0.003739 0.999365 5 Methane 0.003739 0.999365 6 Ethane 0.002299 0.999820 6 Ethane 0.002299 0.999820 7 Propylene 0.001349 0.999999 7 Propylene 0.001349 0.999999 8 8 9 Methane 0.003739 0.999365 9 Methane 0.003739 0.999365 10 Ethane 0.002299 0.999820 10 Ethane 0.002299 0.999820 11 Propylene 0.001349 0.999999 11 Propylene 0.001349 0.999999 12 12 13 Methane 0.003739 0.999365 13 Methane 0.003739 0.999365 14 Ethane 0.002299 0.999820 14 Ethane 0.002299 0.999820 15 Propylene 0.001349 0.999999 15 Propylene 0.001349 0.999999 0 20 40 60 80 100 120

0.0 10000.0 20000.0 30000.0 40000.0 50000.0 60000.0 70000.0Concentrations (ppmv)

Area Counts Calibration Curves

Methane

Ethane Propylene

Methane

Ethane Propylene

Methane

Ethane Propylene

Methane

Ethane Propylene Linear (Methane) Linear (Ethane) Linear (Propylene) Linear () Linear (Methane) Linear (Ethane) Linear (Propylene) Linear () Linear (Methane) Linear (Ethane) Linear (Propylene) Linear () Linear (Methane) Linear (Ethane) Linear (Propylene)



### Testing by TRC, Austin, Texas

## Method 18 Outlet 

# Test Run Data Direct

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH       ,1,7,$/ 6 (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 6 (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 6 (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 6 (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH       ,1,7,$/ 6 (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 6 (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH      ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH      ,1,7,$/

0HWKDQH       ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH       ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH     ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH    ,1,7,$/

0HWKDQH       ,1,7,$/ 3+E (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH    ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH    ,1,7,$/

## Method 18 Outlet 

# Test Run Data Direct (2)

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH     ,1,7,$/ 3/E (WKDQH     ,1,7,$/ 3URS\OHQH     ,1,7,$/

0HWKDQH       ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/E (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH     ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH     ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH    ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH       ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH    ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

## Method 18 Outlet 

# Test Run Data Direct (3)

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Injection 3 (Area Counts) Injection 4 (Area Counts) Injection 5 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH       ,1,7,$/ 3+ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH       ,1,7,$/ 3/ (WKDQH    ,1,7,$/ 3URS\OHQH       ,1,7,$/

0HWKDQH (WKDQH 3URS\OHQH

0HWKDQH (WKDQH 3URS\OHQH

## Method 18 Outlet 

# Test Run Data Bag

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH     ,1,7,$/ 6 (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 6 (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 6 (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 6 (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH 848 681   ,1,7,$/ 6 (WKDQH    ,1,7,$/ %DJ 3URS\OHQH 23525 24178   ,1,7,$/

0HWKDQH 0 586   ,1,7,$/ 6 (WKDQH    ,1,7,$/ %DJ 3URS\OHQH 4317 1559   ,1,7,$/

0HWKDQH 572    ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH 1625    ,1,7,$/

0HWKDQH    ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH    ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH 790 763   ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH 1071 344   ,1,7,$/

0HWKDQH N/A
3+ (WKDQH 1$ %DJ 3URS\OHQH N/A

0HWKDQH 723    ,1,7,$/ 3+E (WKDQH    ,1,7,$/ %DJ 3URS\OHQH 529    ,1,7,$/

0HWKDQH 1$ 3/ (WKDQH 1$ %DJ 3URS\OHQH 1$

## Method 18 Outlet 

# Test Run Data Bag (2)

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH     ,1,7,$/ 3/E (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3/E (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH     ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH    ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH    ,1,7,$/

0HWKDQH     ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH     ,1,7,$/ 3+ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

## Method 18 Outlet 

# Test Run Data Bag (3)

7HVWLQJE\75&$XVWLQ7H[DV Test Run Number: Injection 1 (Area Counts) Injection 2 (Area Counts) Average Area Counts Concentration (ppmv) Curve Used (Initial or Final) GC Run Number 0HWKDQH     ,1,7,$/ 3+ (WKDQH     ,1,7,$/ %DJ 3URS\OHQH     ,1,7,$/

0HWKDQH    ,1,7,$/ 3/ (WKDQH    ,1,7,$/ %DJ 3URS\OHQH    ,1,7,$/

0HWKDQH (WKDQH 3URS\OHQH

0HWKDQH (WKDQH 3URS\OHQH

#  

# 















 

# Appendix E: Sample Gas Extraction Diagram 



 

#  

# 















 

# Appendix F: Calibration Certificates

Customer Service Center

Manufacturing Location

Shipping Location 2550 KYLE CROSSING

mtgKYLE@matheson-trigas.com

1700 SCEPTER ROAD

2550 KYLE CROSSING KYLE, TX 78640

WAVERLY, TN 37185

KYLE, TX 78640 P 512-262-2129
F 512-262-4011

CYLINDER NUMBER(S) Product:

Grade: Cylinder Size:

MTG Part No: Contents:

Pressure: Valve:

Net: To: MTG Customer No: Sales Order No: Purchase Order No: Certificate No: 111933 619978 52186

G2684058 CERTIFIED Multi-Component Mixture 1R
CGA 350 BR TRC AIR MEASUREMENTS 9225 US HWY 183 S AUSTIN, TX 78747

140 ft3; 3.96 m3

2000 psig @ 70°F; 13891 kPa @ 21°C 255153 

# Certificate of Mixture Analysis

SX050102 Analysis Method Certified Accuracy Blend
Tolerance Units Certified Concentration Requested Concentration

Methane 5 5.01 ppm ±20% ±5%

Ethane 5 5.85 ppm ±20% ±5%
Propane 5 5.45 ppm ±20% ±5%

Butane 5 5.05 ppm ±20% ±5%

Pentane 5 5.12 ppm ±20% ±5%

Hexane 5 5.12 ppm ±20% ±5%
Nitrogen Balance Balance

TRACEABILITY

COMMENTS

PO# 52186 Lot No:

Fill Date: Expiration Date:

Analysis Date : 9302604235 01/07/2013
01/07/2015

01/07/2013

Unless otherwise indicated, Matheson Tri-Gas terms and conditions govern the product data contained herein. This document was issued electronically and data validated by electronic signature. For further information visit www.matheson-trigas.com.

Date Date WenWen Zhang - Analyst 01/07/2013

Jeff Medlock - QA Approval 02/01/2013

Page 1 of 1Customer Service Center

Manufacturing Location

Shipping Location 2550 KYLE CROSSING

mtgKYLE@matheson-trigas.com

1700 SCEPTER ROAD

2550 KYLE CROSSING KYLE, TX 78640

WAVERLY, TN 37185

KYLE, TX 78640 P 512-262-2129
F 512-262-4011

CYLINDER NUMBER(S) Product:

Grade: Cylinder Size:

MTG Part No: Contents:

Pressure: Valve:

Net: To: MTG Customer No: Sales Order No: Purchase Order No: Certificate No: 111933 619978 52186

G2684059 CERTIFIED Multi-Component Mixture 1R
CGA 350 BR TRC AIR MEASUREMENTS 9225 US HWY 183 S AUSTIN, TX 78747

140 ft3; 3.96 m3

2000 psig @ 70°F; 13891 kPa @ 21°C 252871 

# Certificate of Mixture Analysis

SX041078 * Analysis Method Certified Accuracy Blend
Tolerance Units Certified Concentration Requested Concentration

Methane 50 50.06 ppm ±10% ±2%

Ethane 50 46.58 ppm ±10% ±2%
Propane 50 53.34 ppm ±10% ±2%

Butane 50 47.58 ppm ±10% ±2%

Pentane 50 47.77 ppm ±10% ±2%

Hexane 50 46.52 ppm ±10% ±2%
Nitrogen Balance Balance

TRACEABILITY * Indicates the actual cylinder(s) analyzed.

COMMENTS

PO# 52186 Lot No:

Fill Date: Expiration Date:

Analysis Date : 9302604236 01/03/2013
01/04/2015

01/04/2013

Unless otherwise indicated, Matheson Tri-Gas terms and conditions govern the product data contained herein. This document was issued electronically and data validated by electronic signature. For further information visit www.matheson-trigas.com.

Date Date WenWen Zhang - Analyst 01/04/2013

Paula Gentry - QA Approval 01/11/2013

Page 1 of 1Customer Service Center

Manufacturing Location

Shipping Location 2550 KYLE CROSSING

mtgKYLE@matheson-trigas.com

1700 SCEPTER ROAD

2550 KYLE CROSSING KYLE, TX 78640

WAVERLY, TN 37185

KYLE, TX 78640 P 512-262-2129
F 512-262-4011

CYLINDER NUMBER(S) Product:

Grade: Cylinder Size:

MTG Part No: Contents:

Pressure: Valve:

Net: To: MTG Customer No: Sales Order No: Purchase Order No: Certificate No: 111933 619978 52186

G2684060 CERTIFIED Multi-Component Mixture 1R
CGA 350 BR TRC AIR MEASUREMENTS 9225 US HWY 183 S AUSTIN, TX 78747

140 ft3; 3.96 m3

2000 psig @ 70°F; 13891 kPa @ 21°C 252872 

# Certificate of Mixture Analysis

SX030921 * Analysis Method Certified Accuracy Blend
Tolerance Units Certified Concentration Requested Concentration

Methane 100 100.6 ppm ±10% ±2%

Ethane 100 98.52 ppm ±10% ±2%
Propane 100 100.4 ppm ±10% ±2%

Butane 100 100.6 ppm ±10% ±2%

Pentane 100 100.9 ppm ±10% ±2%

Hexane 100 100.9 ppm ±10% ±2%
Nitrogen Balance Balance

TRACEABILITY * Indicates the actual cylinder(s) analyzed.

COMMENTS

PO#52186 Lot No:

Fill Date: Expiration Date:

Analysis Date : 9302604237 01/02/2013
01/03/2015

01/03/2013

Unless otherwise indicated, Matheson Tri-Gas terms and conditions govern the product data contained herein. This document was issued electronically and data validated by electronic signature. For further information visit www.matheson-trigas.com.

Date Date Ashley Ellis - Analyst 01/03/2013

Paula Gentry - QA Approval 01/11/2013

Page 1 of 1Certification Date : Expiration Date: Cylinder Pressure: MFG Facility: COA # Lot Number:



### 20.0% 19.6% Nitrogen Balance

Type Component Expiration
GMIS Oxygen 4/28/2013 GMIS Carbon Dioxide 11/3/2013

Z -0.0410 S 94.995 C 69.8040 Z 0.0090 S 72.715 C 69.8130 S 95.1050 C 69.949 Z -0.051 S 72.8230 C 69.943 Z 0.009 C 69.866 Z -0.0220 S 95.101 C 69.87 Z 0.0090 S 72.652 Assay Laboratory: Red Ball TGS 555 Craig Kennedy Way Shreveport, LA 71107 800-551-8150



# EPA PROTOCOL GAS CERTIFICATE OF ANALYSIS

Cylinder Number: EB0045768 1/30/2013 Product ID Number: 124240 1/30/2017 1900 PSIG RBTGS-Shreveport-LA GC1301031102 GC1301031102-0 Customer PO. NO.: Tracking Number: 065123346 Customer Previous Certification Dates:

This calibration standard has been certified per the 1997 EPA Traceability Protocol, Document EPA-600/97/121, using procedure G1. All values certified to be +/-1% NIST Traceable.

Do Not Use This Cylinder Below 150 psig (1.0 Megapascal).

Certified Concentration(s) Component Concentration Analytical Principle Accuracy 

### Oxygen Magnetic Pressure Analysis +/- 1% NIST

EB0010703 NTRM 071001 

### Carbon Dioxide +/- 1% NIST Non Dispersive Infrared Absorptiometry

Analytical Information Component Oxygen Reference Standard(s)

Balance Gas Concentration Cylinder Number NIST Reference Nitrogen 24.430%

Analysis Date: 1/30/2013 Conc. 19.9% Conc. 20.0% Conc. 20.0%

Z= Zero Gas S= Span Gas C= Candidate Gas Conc. 19.6% Conc. 19.7% Conc. 19.6% Analysis Date:

800-551-8150 Fax (318-425-6309) Red Ball Technical Gas Service

Information and Ordering Fred Holt, CHMM Quality Control

PGVP Vendor ID # G12012 1/30/2013

Nitrogen 18.4% EB0005577 PRM 3221755.02

Component Carbon Dioxide

# CERTIFICATE OF ANALYSIS

Grade of Product: EPA Protocol

Customer: TRC PO: 45933,

STOCK BY CONCENTRATION Part Number: E04NI99E15A38H6 Reference Number: 54-124320914-19 Cylinder Number: CC403079 Cylinder Volume: 144.4 Cubic Feet Laboratory: ASG - Chicago - IL Cylinder Pressure: 2015 PSIG PGVP Number: B12012 Valve Outlet: 660 Gas Code: CO,NO,PPN,BALN Certification Date: Jun 08, 2012 Expiration Date: Jun 08, 2020

Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a volume/volume basis unless otherwise noted.
Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. 

### ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates

PROPANE 85.00 PPM 86.79 PPM G1 +/- 1% NIST Traceable 06/07/2012

CARBON MONOXIDE 100.0 PPM 100.1 PPM G1 +/- 1% NIST Traceable 06/07/2012, 06/08/2012

NITRIC OXIDE 100.0 PPM 100.1 PPM G1 +/- 1% NIST Traceable 06/07/2012, 06/08/2012

NITROGEN Balance

Total oxides of nitrogen 100.1 PPM For Reference Only



### CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date

NTRM/C3H8 09061733 CC303833 97.82 PPM PROPANE/AIR +/- 0.5% Oct 02, 2013

NTRM/CO 09060516 CC280458 98.88 PPM CARBON MONOXIDE/ +/- 0.5% Feb 01, 2013

NTRM/CO 09060516 CC280693 98.88 PPM CARBON MONOXIDE/ +/- 0.5% Feb 11, 2013

NTRM/NO 11060518 CC331279 101.2 PPM NITRIC OXIDE/NITROGEN +/- 0.6% Feb 16, 2017 

### ANALYTICAL EQUIPMENT

Instrument/Make/Model Analytical Principle Last Multipoint Calibration

Nexus 470 AEP0000428 FTIR May 09, 2012

Nexus 470 AEP0000428 FTIR May 09, 2012

Nexus 470 AEP0000428 FTIR May 09, 2012

Triad Data Available Upon Request
Notes:TRC PO: 45933, STOCK BY CONCENTRATION Signature on file

____________________________________ 

### Approved for Release

Page 1 of 54-124320914-19

# CERTIFICATE OF ANALYSIS

Grade of Product: EPA Protocol

Customer PO Number: 59415 Part Number: E03NI80E15AC2K9 Reference Number: 54-124385978-17 Cylinder Number: CC351249 Cylinder Volume: 150.9 Cubic Feet Laboratory: ASG - Chicago - IL Cylinder Pressure: 2015 PSIG PGVP Number: B12013 Valve Outlet: 590 Gas Code: CO2,O2,BALN Certification Date: Jul 26, 2013 Expiration Date: Jul 26, 2021

Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a volume/volume basis unless otherwise noted.
Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. 

### ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates

CARBON DIOXIDE 10.00 % 9.950 % G1 +/- 1.0% NIST Traceable 07/26/2013

OXYGEN 10.00 % 9.969 % G1 +/- 1.0% NIST Traceable 07/26/2013

NITROGEN Balance



### CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date

CO2 97051015 SG9198991BAL 10.818 % CARBON DIOXIDE/NITROGEN +/- 0.5% Jun 28, 2018

NTRM/O2 98051016 SG9163074BAL 12.05 % OXYGEN/NITROGEN +/- 0.7% Dec 02, 2017 

### ANALYTICAL EQUIPMENT

Instrument/Make/Model Analytical Principle Last Multipoint Calibration

CO2-1 HORIBA VIA-510 V1E3H7P5 NDIR Jul 22, 2013

O2-1 HORIBA MPA-510 3VUYL9NR Paramagnetic Jul 18, 2013

Triad Data Available Upon Request

Permanent Notes:STOCK BY CONCENTRATION

Notes:TRC PO #59415 "STOCK BY CONCENTRATON" Signature on file

____________________________________ 

### Approved for Release

Page 1 of 54-124385978-17

# CERTIFICATE OF ANALYSIS

Grade of Product: EPA Protocol

Part Number: E04NI99E15A3528 Reference Number: 54-124369425-2 Cylinder Number: CC335400 Cylinder Volume: 144.4 Cubic Feet Laboratory: ASG - Chicago - IL Cylinder Pressure: 2015 PSIG PGVP Number: B12013 Valve Outlet: 660 Gas Code: CO,NO,PPN,BALN Certification Date: Apr 16, 2013 Expiration Date: Apr 16, 2021

Certification performed in accordance with “EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards (May 2012)” document EPA 600/R-12/531, using the assay procedures listed. Analytical Methodology does not require correction for analytical interference. This cylinder has a total analytical uncertainty as stated below with a confidence level of 95%. There are no significant impurities which affect the use of this calibration mixture. All concentrations are on a volume/volume basis unless otherwise noted.
Do Not Use This Cylinder below 100 psig, i.e. 0.7 megapascals. 

### ANALYTICAL RESULTS Component Requested Actual Protocol Total Relative Assay Concentration Concentration Method Uncertainty Dates

NOX 50.00 PPM 51.01 PPM G1 +/- 1.1% NIST Traceable 04/09/2013, 04/16/2013

PROPANE 45.00 PPM 45.57 PPM G1 +/- 1% NIST Traceable 04/09/2013

CARBON MONOXIDE 50.00 PPM 49.66 PPM G1 +/- 1% NIST Traceable 04/09/2013

NITRIC OXIDE 50.00 PPM 51.01 PPM G1 +/- 1.1% NIST Traceable 04/09/2013, 04/16/2013

NITROGEN Balance



### CALIBRATION STANDARDS Type Lot ID Cylinder No Concentration Uncertainty Expiration Date

NTRM/C3H8 09061733 CC303833 97.82 PPM PROPANE/AIR +/- 0.5% Oct 02, 2013

CO 12060505 CC353897 49.53 PPM CARBON MONOXIDE/NITROGEN +/- 0.6% Dec 20, 2017

NO 12060806 CC280981 49.95 PPM NITRIC OXIDE/NITROGEN +/- 0.8% Dec 16, 2017

NO2 124206889130 CC323209 4.824 PPM NITROGEN DIOXIDE/NITROGEN +/- 2.0% Oct 25, 2015 

### ANALYTICAL EQUIPMENT

Instrument/Make/Model Analytical Principle Last Multipoint Calibration

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Nexus 470 AEP0000428 FTIR Apr 04, 2013

Triad Data Available Upon Request

Notes:TRC P.O. 55889 "STOCK BY CONCENTRATION" Signature on file

____________________________________ 

### Approved for Release

Page 1 of 54-124369425-2

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP
Part Number: X03NI60P15A25V2 Reference Number: 126-400243593-1 Cylinder Number: CC427628 Cylinder Volume: 160.0 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 1936 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243593-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

ETHANE 20.00 % 20.00 % +/- 1%

METHANE 20.00 % 20.00 % +/- 1%

NITROGEN Balance



### Notes:

. PO # 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243593-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP
Part Number: X03NI90P15A51P0 Reference Number: 126-400243594-1 Cylinder Number: CC427627 Cylinder Volume: 148.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243594-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

ETHANE 5.000 % 4.995 % +/- 1%

METHANE 5.000 % 5.002 % +/- 1%

NITROGEN Balance



### Notes:

. PO # 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243594-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX
Part Number: X03NI4P15A57J0 Reference Number: 126-400243591-1 Cylinder Number: CC427616 Cylinder Volume: 174.6 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243591-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

ETHANE 1.000 % 0.9998 % +/- 1%

METHANE 95.00 % 95.00 % +/- 1%

NITROGEN Balance



### Notes: TRC ENVIRONMENTAL CORP - BELTON , TX TRC PO#: 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243591-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX
Part Number: X03NI40P15A4BC1 Reference Number: 126-400243592-1 Cylinder Number: CC427422 Cylinder Volume: 166.5 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243592-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

ETHANE 10.00 % 10.00 % +/- 1%

METHANE 50.00 % 50.00 % +/- 1%

NITROGEN Balance



### Notes: TRC ENVIRONMENTAL CORP - BELTON , TX TRC PO#: 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243592-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP
Part Number: X02NI15P15A0PK1 Reference Number: 126-400243585-1 Cylinder Number: CC427195 Cylinder Volume: 9.8 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 109 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243585-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

PROPYLENE 85.00 % 85.02 % +/- 1%

NITROGEN Balance



### Notes:

. PO # 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243585-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX
Part Number: X02NI99P15A3LE2 Reference Number: 126-400243589-1 Cylinder Number: CC427190 Cylinder Volume: 144.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG Analysis Date: Aug 26, 2013 Valve Outlet: 350
Lot Number: 126-400243589-1

Expiration Date: Aug 26, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

PROPYLENE 50.00 PPM 50.20 PPM +/- 1%

NITROGEN Balance



### Notes: TRC ENVIRONMENTAL CORP/BELTON , TX TRC PO#: 60350 "JIM BARUFALDI/ JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243589-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX
Part Number: X02NI99P15A51P7 Reference Number: 126-400243588-1 Cylinder Number: CC427187 Cylinder Volume: 144.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG Analysis Date: Aug 26, 2013 Valve Outlet: 350
Lot Number: 126-400243588-1

Expiration Date: Aug 26, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

PROPYLENE 85.00 PPM 84.96 PPM +/- 1%

NITROGEN Balance



### Notes: TRC ENVIRONMENTAL CORP/BELTON , TX TRC PO#: 60350 "JIM BARUFALDI/ JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243588-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP
Part Number: X02NI50P15A40F3 Reference Number: 126-400243586-1 Cylinder Number: CC427185 Cylinder Volume: 16.3 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 197 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243586-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

PROPYLENE 50.00 % 50.00 % +/- 1%

NITROGEN Balance



### Notes:

. PO # 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243586-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: BELTON , TX - TRC ENVIRONMENTAL CORP
Part Number: X02NI70P15A0PK1 Reference Number: 126-400243587-1 Cylinder Number: CC427181 Cylinder Volume: 26.8 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 338 PSIG Analysis Date: Aug 22, 2013 Valve Outlet: 350
Lot Number: 126-400243587-1

Expiration Date: Aug 22, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

PROPYLENE 30.00 % 30.01 % +/- 1%

NITROGEN Balance



### Notes:

. PO # 60350 "JIM BARUFALDI / JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243587-1

# CERTIFICATE OF ANALYSIS

Grade of Product: PRIMARY STANDARD

Customer: TRC ENVIRONMENTAL CORP - BELTON , TX
Part Number: X02NI99P15A51P8 Reference Number: 126-400243590-1 Cylinder Number: CC427175 Cylinder Volume: 144.4 CF

Laboratory: SWS - LaPorte Mix (SAP) - TX Cylinder Pressure: 2015 PSIG Analysis Date: Aug 26, 2013 Valve Outlet: 350
Lot Number: 126-400243590-1

Expiration Date: Aug 26, 2016

Primary Standard Gas Mixtures are traceable to N.I.S.T. weights and/or N.I.S.T. Gas Mixture reference materials.



# ANALYTICAL RESULTS Component Requested Actual Concentration Analytical
Concentration (Mole %) 

### Uncertainty

PROPYLENE 30.00 PPM 30.35 PPM +/- 1%

NITROGEN Balance



### Notes: TRC ENVIRONMENTAL CORP/BELTON , TX TRC PO#: 60350 "JIM BARUFALDI/ JOHN ZINK"

Signature on file



## ____________________________________ Approved for Release

Page 1 of 126-400243590-1**This is to Certify that:**James P. BarufaldiIs a Qualified Individual as defined in Section 8.3 of ASTM D7036-04 for the following test methods:EPA Methods 18, 15, 16, 23 and 0023AThe individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04and has successfully passed an internal comprehensive examination for the test methods designated above.This certification is effective until:01-12-2016Edward J MacKinnonAir Measurements Practice Quality CoordinatorThis is to Certify that:James BarufaldiIs a Qualified Individual as defined in Section 8.3of ASTM D7036-04 for the following test methods:EPA Methods 3A, 6C, 7E, 10, 10B, 19, 20, 25A.CEM Performance Specifications PS2, PS3, PS4, PS4A, PS5, PS6, PS7, PS8, and PS15The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04and has successfully passed a comprehensive examination for the test methods designated above.This certification is effective until:02-21-2018Date of Issue: 03-25-2013Certificate Number: 00560Edward J MacKinnonAir Measurements Practice Quality DirectorThis is to Certify that:James BarufaldiIs a Qualified Individual as defined in Section 8.3of ASTM D7036-04 for the following test methods:EPA Methods 1, 2, 3, 4, 3B, 6, 6A, 6B, 7, 7C,7D, 8, 11, 13A, 13B, 15A, 16A, 19, 26, 26A, and 202.The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04and has successfully passed a comprehensive examination for the test methods designated above.This certification is effective until:02-21-2018Date of Issue: 03-25-2013Certificate Number: 00559Edward J MacKinnonAir Measurements Practice Quality DirectorThis is to Certify that:James BarufaldiIs a Qualified Individual as defined in Section 8.3of ASTM D7036-04 for the following test methods:EPA Methods 1, 1A, 2, 2A, 2C, 2D, 2F, 2G, 2H,3, 3B, 4, 5, 5A, 5B, 5E, 5F, 5i, 17, 19, 201A, and 202.The individual has met the minimum experience requirements defined in Section 8.3.4.2 of ASTM D7036-04and has successfully passed a comprehensive examination for the test methods designated above.This certification is effective until:02-21-2018Date of Issue: 03-25-2013Certificate Number: 00558Edward J MacKinnonAir Measurements Practice Quality Director