STAND & TECH

A -1.1107 glDjlQ

NBS SPECIAL

FUBLlCATiON

260-111

STANDARD REFERENCE HATERIALS:

CONPILATinN OF ELEflENTAL CONCENTRATION DATA FOR NRS

CLINICAL. BIOLOGICAL. GEOLOGICAL. AND ENVIRONNENTAL STANDARD

REFERENCE MATERIALS.

E. S. Gladney. R. T. O'Malley.

I. ROELANDTS. AND T- E* GlLLSmm

•.-

Research Information Center

iNalionai Bureau of Standards

Gaithersburg, Marylaad 20899

NBS SPECIAL PUBLICATION 260-1 1

1

U.S. DEPARTMENT OF COMMERCE/National Bureau of Standards

Standard Reference Materials:

Compilation of Elemental Concentration

Data for NBS Clinical, Biological,

Geological, and Environmental

Standard Reference Materials

E. S. Gladney, B. T. O'Malley, I. Roelandts, and T. E. Gills
m he National Bureau of Standards' was established by an act of Congress on March 3, 1901. The Bureau's overall

goal is to strengthen and advance the nation's science and technology and facilitate their effective appUcation for

pubUc benefit. To this end, the Bureau conducts research to assure international competitiveness and leadership of U.S.

industry, science arid technology. NBS work involves development and transfer of measurements, standards and related

science and technology, in support of continually improving U.S. productivity, product quality and reUability, innovation

and underlying science and engineering. The Bureau's technical work is performed by the National Measurement

Laboratory, the National Engineering Laboratory, the Institute for Computer Sciences and Technology, and the Institute

for Materials Science and Engineering.

The National Measurement Laboratory

Provides the national system of physical and chemical measurement;

coordinates the system with measurement systems of other nations and

ftimishes essentia services leading to accurate and uniform physical and

chemical measurement throughout the Nation's scientific community,

industry, and commerce; provides advisory and research services to other

Government agencies; conducts physical and chemical research; develops,

produces, and distributes Standard Reference Materials; provides

calibration services; and manages the National Standard Reference Data

System. The Laboratory consists of the following centers:

Basic Standards^

Radiation Research

Chemical Physics

Analytical Chemistry

The National Engineering Laboratory

Provides technology and technical services to the public and private sectors

to address national needs and to solve national problems; conducts research

in engineering and applied science in support of these efforts; builds and

maintains competence in the necessary disciplines required to carry out this research and technical service; develops engineering data and measurement

capabilities; provides engineering measurement traceability services;

develops test methods and proposes engineering standards and code

changes; develops and proposes new engineering practices; and develops

and improves mechanisms to transfer results of its research to the ultimate

user. TTie Laboratory consists of the following centers:

Applied Mathematics

Electronics and Electrical

Engineering^

Manufacturing Engineering

Building Technology

Fire Research

Chemical Engineering^

The Institute for Computer Sciences and Technology

Conducts research and provides scientific and technical services to aid

Federal agencies in the selection, acquisition, application, and use of

computer technology to improve effectiveness and economy in Government

operations in accordance with Public Law 89-306 (40 U.S.C. 759),

relevant Executive Orders, and other directives; carries out this mission by

managing the Federal Information Processing Standards Program,

developing Federal ADP standards guidelines, and managing Federal

participation in ADP voluntary standardization activities; provides scientific

and technological advisory services and assistance to Federal agencies; and

provides the technical foundation for computer-related policies of the

Federal Government. The Institute consists of the following divisions:

Information Systems Engineering

Systems and Software

Technology

Computer Security

System and Network

Architecture

Advanced Systems

The Institute for Materials Science and Engineering

Conducts research and provides measurements, data, standards, reference

materials, quantitative understanding and other technical information

fundamental to the processing, structure, properties and performance of

materials; addresses the scientific basis for new advanced materials

technologies; plans research around cross-cutting scientific themes such as nondestructive evaluation and phase diagram development; oversees Bureau-wide technical programs in nuclear reactor radiation research and

nondestructive evaluation; and broadly disseminates generic technical

information resulting firom its programs. The Institute consists of the

following Divisions:

Ceramics

Fracture and Deformation'

Polymers

Metallurgy

Reactor Radiation

'Headquarters and Laboratories at Gaithersburg, MD, unless otherwise noted; mailing address

Gaithersburg, MD 20899. ^Some divisions within the center are located at Boulder, CO 80303.

'Located at Boulder, CO, with some elements at Gaithersburg, MD
Standard Reference Materials:

Compilation of Elemental Concentration

Data for NBS Clinical, Biological,

Geological, and Environmental

Standard Reference Materials

E. S. Gladney\ B. T. 0'Malley\ I. Roelandts^ and T. E. Gills^

1 . Los Alamos National Laboratory

Los Alamos, NM 87545

2. Universite de Liege

Liege, Belgium

3. National Bureau of Standards

Gaithersburg, Maryland 20899

U.S. DEPARTMENT OF COMMERCE, C. William Verity, Secretary

NATIONAL BUREAU OF STANDARDS, Ernest Ambler, Director

Issued November 1987
Library of Congress Catalog Card Number: 87-619888

National Bureau of Standards Special Publication 260-1 1

Natl. Bur. Stand. (U.S.), Spec. Publ. 260-111, 547 pages (Nov. 1987)

CODEN:XNBSAV

U.S. GOVERNMENT PRINTING OFFICE

WASHINGTON: 1987

For sale by the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402-9325
PREFACE

Standard Reference Materials (SRMs) as defined by the National Bureau of Standards are "well-characterized

materials, produced in quantity, that calibrate a measurement system to assure compatabi I ity of measurement in

the Nation." SRMs are widely used as primary standards in many diverse fields of science, industry and

technology, both within the United States and throughout the world. For many of the Nation's scientists and

technologists it is of more than passing interest to know the measurements obtained and methods used by the

analytical community when analyzing SRMs. An NBS series of papers, of which this publication is a member, is called the "NBS Special Publication - 260 Series" is reserved for this purpose.

This 260 Series is dedicated to the dissemination of elemental concentration data for NBS clinical,

biological, geological, and environmental SRMs. More information will be found in this 260 than is generally

found in NBS Certificates of Analysis. This 260 enables the user of these SRMs to assess the validity of data

not available in the certificate of analysis. We hope that this 260 will provide sufficient additional

information so that new application of these SRMs may be sought and found.

Inquires concerning the technical content of this compilation should be directed to the authors. Other

questions concerned with the availability, delivery, or price of specific SRMs should be addressed to:

Office of Standard Reference Materials

National Bureau of Standards

Gaithersburg, MD 20899

Stanley D. Rasberry, Chief

Office of Standard Reference Materials

i i i
CONTENTS

Page

Preface i i i 1.. Introduction 1 2.. Data Cotnpilation 3

3.. Discussion 4

4.. Conclusion 5 5.. References 5 Table I: NBS Biological, Environmental, and Geological Standard Reference Materials 7

Table II: Literature Surveyed 11 Table III: Whole Material Concentration Sunmations of Major and Minor Elements for Selected SRMs . 13

Table IV: Analytical Method Codes for Individual Data Tables 14 Table V: COMMENT Codes for Individual Data Tables 15 Table VI: Factors used for Oxide to Element Conversions 16

Appendix: References for NBS SRM Collected Data R-1

List of SRM Data Tables (revised 3/1/86 unless otherwise indicated)

Table # Title Page

lA-1 Compiled Data for NBS SRM 1A Argillaceous Limestone 1A-1

1A-2 Individual Data for NBS SRM 1A lA-2

1B-1 Compiled Data for NBS SRM IB Argillaceous Limestone ......... . lB-1

1B-2 Individual Data for NBS SRM IB 1B-2

1C-1 Compiled Data for NBS SRM 1C Argillaceous Limestone 1C-1

1C-2 Individual Data for NBS SRM 1C 1C-2

27F-1 Compiled Data for NBS SRM 27F Sibley Iron Ore 27F-1

27F-2 Individual Data for NBS SRM 27F 27F-1

28-1 Compiled Data for NBS SRM 28 Norrie Iron Ore 27F-1

56-1 Compiled Data for NBS SRM 56 Phosphate Rock 56-1

56-2 Individual Data for NBS SRM 56 56-1

56B-1 Compiled Data for NBS SRM 56B Phosphate Rock 56-1

56B-2 Individual Data for NBS SRM 56B 56-1

69A-1 Compiled Data for NBS SRM 69A Bauxite Ore 69A-1

69A-2 Individual Data for NBS SRM 69A 69A-2

69B-1 Compiled Data for NBS SRM 69B Bauxite Ore 69B-1

70-1 Compiled Data for NBS SRM 70 Potash Feldspar 70-1

70-2 Individual Data for NBS SRM 70 70-2

70A-1 Compiled Data for NBS SRM 70A Potash Feldspar 70A-1

70A-2 Individual Data for NBS SRM 70A 70A-2

iv
List of SRM Data Tables (cont.)

Table # Title Page

76-1 Cotnpiled Data for NBS SRM 76 Burnt Refractory 76-1

76- 2 Individual Data for NBS SRM 76 76-2

77- 1 Compiled Data for NBS SRM 77 Burnt Refractory 76-1

77- 2 Individual Data for NBS SRM 77 76-2

78- 1 Compiled Data for NBS SRM 78 Burnt Refractory 76-1

78-2 Individual Data for NBS SRM 78 76-2

76A-1 Compiled Data for NBS SRMs 76A-78A Burnt Refractories 76A-1

79A-1 Compiled Data for NBS SRM 79A Fluorspar 76A-1

79A-2 Individual Data for NBS SRM 79A 76A-2

80-1 Compiled Data for NBS SRM 80 Soda-Lime Glass 76A-1

80-2 Individual Data for NBS SRM 80 76A-2

88-1 Compiled Data for NBS SRM 88 Dolomitic Limestone 88-1

88-2 Individual Data for NBS SRM 88 88-2

88A-1 Compiled Data for NBS SRM 88A Dolomitic Limestone 88A-1

88A-2 Individual Data for NBS SRM 88A , 88A-3

88B-1 Compiled Data for NBS SRM 88B Dolomitic Limestone 88-1

91-1 Compiled Data for NBS SRM 91 Opal Glass 91-1

91- 2 Individual Data for NBS SRM 91 91-2

92- 1 Compiled Data for NBS SRM 92 Soda-Lime Glass 92-1

92- 2 Individual Data for NBS SRM 92 92-2

93- 1 Compiled Data for NBS SRM 93 Borosilicate Glass 92-1

93-2 Individual Data for NBS SRM 93 92-2

93A-1 Compiled Data for NBS SRM 93A Borosilicate Glass 92-1

97-1 Compiled Data for NBS SRM 97 Flint Clay 97-1

97- 2 Individual Data for NBS SRM 97 97-2

97A-1 Compiled Data for NBS SRM 97A Flint Clay 97A-1

97A-2 Individual Data for NBS SRM 97A 97A-2

98- 1 Compiled Data for NBS SRM 98 Plastic Clay 98-1

98- 2 Individual Data for NBS SRM 98 98-3

98A-1 Compiled Data for NBS SRM 98A Plastic Clay 98A-1

98A-2 Individual Data for NBS SRM 98A 98A-2

99- 1 Compiled Data for NBS SRM 99 Soda Feldspar 99-1

99-2 Individual Data for NBS SRM 99 99-2

V
List of SRM Data Tables (cont.)

Table # Title Page

99A-1 Compiled Data for NBS SRM 99A Soda Feldspar 99A-1

99A-2 Individual Data for NBS SRM 99A 99A-2

120A-1 Compiled Data for NBS SRM 120A Phosphate Rock' 120A-1

120A-2 Individual Data for NBS SRM 120A 120A-1

120B-1 Compiled Data for NBS SRM 120B Phosphate Rock 120B-1

120B-2 Individual Data for NBS SRM 120B , 120B-3

181-1 Compiled Data for NBS SRM 181 Lithium Ore (Spodumene) 181-1

181- 2 Individual Data for NBS SRM 181 181-1

182- 1 Compiled Data for NBS SRM 182 Lithium Ore (Petalite) 181-1

183- 1 Compiled Data for NBS SRM 183 Lithium Ore (Lepidolite) 181-1

278-1 Compiled Data for NBS SRM 278 Obsidian Rock 278-1

278-2 Individual Data for NBS SRM 278 278-3

330- 1 Compiled Data for NBS SRM 330 Copper Ore, Mill Heads 330-1

331- 1 Compiled Data for NBS SRM 331 Copper Ore, Mill Tails 330-1

332- 1 Compiled Data for NBS SRM 332 Copper Concentrate 330-1

332- 2 Individual Data for NBS SRM 332 330-1

333- 1 Compiled Data for NBS SRM 333 Molybdenum Concentrate 330-1

610-1 Compiled Data for NBS SRM 610 Trace Elements in Glass 610-1

610-2 Individual Data for NBS SRM 610 610-2

612-1 Compiled Data for NBS SRM 612 Trace Elements in Glass 612-1

612-2 Individual Data for NBS SRM 612 612-2

614-1 Compiled Data for NBS SRM 614 Trace Elements in Glass 614-1

614-2 Individual Data for NBS SRM 614 614-2

616-1 Compiled Data for NBS SRM 616 Trace Elements in Glass 616-1

616-2 Individual Data for NBS SRM 616 616-2

633-1 Compiled Data for NBS SRM 633 Portland Cement: Red Cap 633-1

633- 2 Individual Data for NBS SRM 633 633-1

634- 1 Compiled Data for NBS SRM 634 Portland Cement: Gold Cap 634-1

634- 2 Individual Data for NBS SRM 634 634-1

635- 1 Compiled Data for NBS SRM 635 Portland Cement: Blue Cap 635-1

635- 2 Individual Data for NBS SRM 635 635-1

636- 1 Compiled Data for NBS SRM 636 Portland Cement: Yellow Cap 636-1

636-2 Individual Data for NBS SRM 636 636-1

vi
List of SRM Data Tables (cont.)

Table # Title Page

637-1 Compiled Data for MBS SRM 637 Portland Cement: Pink Cap 637-1

637- 2 Individual Data for NBS SRM 637 637-1

638- 1 Compiled Data for NBS SRN 636 Portland Cement: Green Cap 638-1

638- 2 Individual Data for NBS SRM 638 638-1

639- 1 Compiled Data for NBS SRM 639 Portland Cement: Clear Cap 639-1

639-2 Individual Data for NBS SRM 639 639-1

688-1 Conpiled Data for NBS SRM 688 Basalt 688-1

688-2 Individual Data for NBS SRM 688 688-3

694-1 Compiled Data for NBS SRM 694 Western Phosphate Rock 694-1

696-1 Compiled Data for NBS SRM 696 Bauxite: Surinam 696-1

696- 2 Individual Data for NBS SRM 696 696-2

697- 1 Compiled Data for NBS SRM 697 Bauxite: Dominician 694-1

698- 1 Compiled Data for NBS SRM 698 Bauxite: Jamaican , 698-1

698-2 Individual Data for NBS SRM 698 698-2

1083- 1 Compiled Data for NBS SRM 1083 Wear Metals in Lubricating Oil 1083-1

1084- 1 Compiled Data for NBS SRM 1084 Wear Metals in Lubricating Oil 1083-1

1084- 2 Individual Data for NBS SRM 1084 1083-2

1085- 1 Compiled Data for NBS SRM 1085 Wear Metals in Lubricating Oil 1085-1

1085-2 Individual Data for NBS SRM 1085 1085-2

1549-1 Compiled Data for NBS SRM 1549 Milk Powder 1549-1

1549-2 Individual Data for NBS SRM 1549 1549-2

1566-1 Compiled Data for NBS SRM 1566 Oyster Tissue 1566-1

1566- 2 Individual Data for NBS SRM 1566 1566-3

1567- 1 Compiled Data for NBS SRM 1567 Wheat Flour 1567-1

1567- 2 Individual Data for NBS SRM 1567 1567-3

1568- 1 Cod^Jiled Data for NBS SRM 1568 Rice Flour 1568-1

1568- 2 Individual Data for NBS SRM 1568 1568-3

1569- 1 Compiled Data for NBS SRM 1569 Brewer's Yeast 1569-1

1569- 2 Individual Data for NBS SRM 1569 1569-3

1570- 1 Compiled Data for NBS SRM 1570 Spinach 4 1570-1

1570- 2 Individual Data for NBS SRM 1570 1570-4

1571- 1 Compiled Data for NBS SRM 1571 Orchard Leaves 1571-1

1571-2 Individual Data for NBS SRM 1571 1571-4

vi i
List of SRM Data Tables (cont.)

Table # Title Page

1572-1 Compiled Data for NBS SRM 1572 Citrus Leaves 1572-1

1572- 2 Individual Data for NBS SRM 1572 1572-3

1573- 1 Compiled Data for NBS SRM 1573 Tomato Leaves 1573-1

1573-2 Individual Data for NBS SRM 1573 1573-4

1575-1 Compiled Data for NBS SRM 1575 Pine Needles 1575-1

1575-2 Individual Data for NBS SRM 1575 1575-3

1577-1 Compiled Data for NBS SRM 1577 Bovine Liver 1577-1

1577-2 Individual Data for NBS SRM 1577 1577-A

1577A-1 Compiled Data for NBS SRM 1577A Bovine Liver 1577A-1

1577A-2 Individual Data for NBS SRM 1577A 1577A-2

1580- 1 Compiled Data for NBS SRM 1580 Organics in Shale Oil 1580-1

1581- 1 Conpiled Data for NBS SRM 1581 Polychlorinated Biphenyls in Oils 1580-1

1582- 1 Compiled Data for NBS SRM 1582 Petroleum Crude Oil 1582-1

1582- 2 Individual Data for NBS SRM 1582 1582-1

1583- 1 Compiled Data for NBS SRM 1583 Chlorinated Pesticides in 2,2,4-Trimethylpentane 1580-1

^

1584- 1 Compiled Data for NBS SRM 1584 Priority Pollutant Phenols in Methanol 1584-1

1584- 2 Individual Data for NBS SRM 1584 , 1584-1

1585- 1 Compiled Data for NBS SRM 1585 Chlorinated Biphenyls in Isooctane 1585-1

1587-1 Conpiled Data for NBS SRM 1587 Nitrated Polycyclic Aromatic Hydrocarbons in Methanol 1585-1

1589- 1 Compiled Data for NBS SRM 1589 Polychlorinated Biphenyls in Human Serum 1585-1

1590- 1 Compiled Data for NBS SRM 1590 Stabilized Wine 1590-1

1590-2 Individual Data for NBS SRM 1590 1590-1

1614-1 Compiled Data for NBS SRM 1614 Dioxin in Isooctane 1590-1

1618- 1 Compiled Data for NBS SRM 1618 Vanadium and Nickel in Residual Fuel Oil 1618-1

1619- 1 Compiled Data for NBS SRM 1619 Sulfur in Residual Fuel Oil 1619-1

1619- 2 Individual Data for NBS SRM 1619 . 1619-2

1620- 1 Compiled Data for NBS SRM 1620 Sulfur in Residual Fuel Oil 1620-1

1620A-1 Compiled Data for NBS SRM 1620A Sulfur in Residual Fuel Oil 1620-1

1620A-2 Individual Data for NBS SRM 1620A 1620-2

W

1621- 1 Compiled Data for NBS SRM 1621 Sulfur in Residual Fuel Oil 1621-1

1621-2 Individual Data for NBS SRM 1621 1621-1

vi i i
List of SRM Data Tables (cont.)

Table # Title Page

1621A-1 Compiled Data for NBS SRM 1621A Sulfur in Residual Fuel Oil 1621-1

1621A-2 Individual Data for NBS SRM 1621A 1621-1

1621B-1 Compiled Data for NBS SRM 1621B Sulfur in Residual Fuel Oil 1621B-1

1621B-2 Individual Data for NBS SRM 1621B 16218-1

1622-1 Compiled Data for NBS SRM 1622 Sulfur in Residual Fuel Oil 1622-1

1622- 2 Individual Data for NBS SRM 1622 1622-1

1622A-1 Compiled Data for NBS SRM 1622A Sulfur in Residual Fgel Oil 1622-1

1622A-2 Individual Data for NBS SRM 1622A 1622-1

1622B-1 Compiled Data for NBS SRM 1622B Sulfur in Residual Fuel Oil , 1622B-1

1622B-2 Individual Data for NBS SRM 1622B 1622B-1

1622C-1 Compiled Data for NBS SRM 1622C Sulfur in Residual Fuel Oil 1622-1

1623- 1 Compiled Data for NBS SRM 1623 Sulfur in Residual Fuel Oil 1623-1

1623- 2 Individual Data for NBS SRM 1623 1623-2

1623A-1 Compiled Data for NBS SRM 1623A Sulfur in Residual Fuel Oil 1623-1

1623A-2 Individual Data for NBS SRM 1623A 1623-2

162A-1 Compiled Data for NBS SRM 1624 Sulfur in Distillate Oil 1624-1

1624- 2 Individual Data for NBS SRM 1624 1624-2

1624A-1 Compiled Data for NBS SRM 1624A Sulfur in Distillate Oil 1624-1

1624A-2 Individual Data for NBS SRM 1624A 1624-2

1630-1 Compiled Data for NBS SRM 1630 Mercury in Coal 1630-1

1630-2 Individual Data for NBS SRM 1630 1630-2

1631A-1 Compiled Data for NBS SRM 1631A Sulfur in Coal 1631-1

1631A-2 Individual Data for NBS SRM 1631A 1631-2

1631B-1 Compiled Data for NBS SRM 1631B Sulfur in Coal 1631-1

1631B-2 Individual Data for NBS SRM 1631B 1631-2

1631C-1 Compiled Data for NBS SRM 1631C Sulfur in Coal 1631-1

1631C-2 Individual Data for NBS SRM 1631C 1631-2

1632-1 Compiled Data for NBS SRM 1632 Trace Elements in Coal 1632-1

1632-2 Individual Data for NBS SRM 1632 1632-4

1632A-1 Compiled Data for NBS SRM 1632A Trace Elements in Coal 1632A-1

1632A-2 Individual Data for NBS SRM 1632A 1632A-3

1632B-1 Compiled Data for NBS SRM 1632B Trace Elements in Coal 1632B-1

ix
List of SRM Data Tables (cont.)

Tabl« # Title Page

1633-1 Compiled Data for NBS SRM 1633 Trace Elements in Coal Fly Ash 1633-1

1633- 2 Individual Data for NBS SRM 1633 1633-3

1633A-1 Compiled Data for NBS SRM 1633A Trace Elements in Coal Fly Ash 1633A-1

1653A-2 Individual Data for NBS SRM 1633A 1633A-A

1634- 1 Compiled Data for NBS SRM 1634 Trace Metals in Fuel Oil 1634-1

1634- 2 Individual Data for NBS SRM 1634 1634-2

1634A-1 Compiled Data for NBS SRM 1634A Trace Metals in Fuel Oil 1634A-1

1634A-2 Individual Data for NB^ SRM 1634A 1634A-2

1634B-1 Compiled Data for NBS SRM 1634B Trace Elements in Fuel Oil 1634B-1

1635- 1 Compiled Data for NBS SRM 1635 Trace Elements in Coal 1635-1

1635-2 Individual Data for NBS SRM 1635 1635-4

1639-1 Compiled Data for NBS SRM 1639 Halocarbons in Methanol 1590-1

1641-1 Compiled Data for NBS SRM 1641 Mercury in Water 1641-1

1641- 2 Individual Data for NBS SRM 1641 . 1641-1

1641A-1 Compiled Data for NBS SRM 1641A Mercury in Water 1641-1

1641B-1 Compiled Data for NBS SRM 1641B Mtrcury in Water 1641-1

1641B-2 Individual Data for NBS SRM 1641B 1641-1

1642- 1 Compiled Data for NBS SRM 1642 Mercury in Water 1642-1

1642A-1 Compiled Data for NBS SRM 1642A Mercury in Water 1642-1

1642A-2 Individual Data for NBS SRM 1642A 1642-1

1642B-1 Compiled Data for NBS SRM 1642B Mercury in Water 1642-1

1642B-2 Individual Data for NBS SRM 1642B 1642-1

1643- 1 Compiled Data for NBS SRM 1643 Trace Elements in Water 1643-1

1643-2 Individual Data for NBS SRM 1643 1643-2

1643A-1 Conpiled Data for NBS SRM 1643A Trace Elements in Water 1643A-1

1643A-2 Individual Data for NBS SRM 1643A 1643A-2

1643B-1 Compiled Data for NBS SRM 1643B Trace Elements in Water 1643B-1

1643B-2 Individual Data for NBS SRM 1643B 1643B-2

1645-1 Compiled Data for NBS SRM 1645 River Sediment 1645-1

1645- 2 Individual Data for NBS SRM 1645 1645-4

1646- 1 Compiled Data for NBS SRM 1646 Estuarine Sediment 1646-1

1646-2 Individual Data for NBS SRM 1646 1646-3

X
List of SRM Data Tables (cont.)

Table # Title Page

16A7-1 Compiled Data for NBS SRM 16A7 Priority Pollutant PNA Hydrocarbons (in Acetonitri le) 16A7-1

16A7-2 Individual Data for NBS SRM 1647 1647-1

1648-1 Compiled Data for NBS SRM 1648 Urban Particulate Matter 1648-1

1648- 2 Compiled Data for NBS SRM 1648 1648-4

1649- 1 Compiled Data for NBS SRM 1649 Urban Dust/ Organics 1649-1

1649-2 Individual Data for NBS SRM 1649 1649-3

1818- 1 Compiled Data for NBS SRM 1818 Chlorine in Lubricating Base Oil (revised 3/1/87) ... 1818-1

1819- 1 Compiled Data for NBS SRM 1819 Sulfur in Lubricating Base Oil (revised 3/1/87) 1818-1

1880-1 Compiled Data for NBS SRMs 1880-1883 Cements (revised 3/1/87) 1818-1

2661- 1 Compiled Data for NBS SRM 2661 Benzene on Charcoal 2661-1

2661A-1 Compiled Data for NBS SRM 2661A Benzene on Charcoal 2661-1

2661A-2 Individual Data for NBS SRM 2661A 2661-2

2662- 1 Compiled Data for NBS SRM 2662 m-Xylene on Charcoal 2661-1

2663- 1 Compiled Data for NBS SRM 2663 1,4-Dioxane on Charcoal 2661-1

2663- 2 Individual Data for NBS SRM 2663 2661-2

2664- 1 Compiled Data for NBS SRM 2664 Ethylene Chloride on Charcoal 2664-1

2664- 2 Individual Data for NBS SRM 2664 2664-2

2665- 1 Compiled Data for NBS SRM 2665 Chloroform on Charcoal 2664-1

2665- 2 Individual Data for NBS SRM 2665 2664-2

2666- 1 Compiled Data for NBS SRM 2666 Trichloroethylene on Charcoal 2664-1

2666- 2 Individual Data for NBS SRM 2666 2664-2

2667- 1 Compiled Data for NBS SRM 2667 Carbon Tetrachloride on Charcoal 2664-1

2667-2 Individual Data for NBS SRM 2667 2664-2

2670-1 Compiled Data for NBS SRM 2670 Trace Elements in Urine 2670-1

2670- 2 Individual Data for NBS SRM 2670 Entire Pool 2670-2

2670N-2 Individual Data for NBS SRM 2670 Normal Level 2670-2

2670E-2 Individual Data for NBS SRM 2670 Elevated Level 2670-2

2671- 1 Compiled Data for NBS SRM 2671 Fluoride in Urine 2671-1

2672- 1 Conpiled Data for NBS SRM 2672 Mercury in Urine 2671-1

2762-2 Individual Data for NBS SRM 2672 Entire Pool 2671-1

2674-1 Compiled Data for NBS SRM 2674 Lead on Filter Media 2674-1

xi
List of SRM Data Tables (cont.)

Table # Title Page

2675-1 Compiled Data for NBS SRM 2675 Beryllium on Filter Media 267^-1

2675- 2 Individual Data for NBS SRM 2675 2674-1

2676- 1 Compiled Data for NBS SRM 2676 Metals on Filter Media 2674-1

2676A-1 Compiled Data for NBS SRM 2676A Metals on Filter Media 2676A-1

2676A-2 Individual Data for NBS SRM 2676A 2676A-1

2676B-1 Conpiled Data for NBS SRM 2676B Metals on Filter Media 2676B-1

2677- 1 Compiled Data for NBS SRM 2677 Beryllium and Arsenic on Filter Media 2676B-1

2679-1 Conpiled Data for NBS SRM 2679 Quartz on Filter Media 2676B-1

2682-1 Compiled Data for NBS SRM 2682 Sulfur in Coal 2682-1

2682- 2 Individual Data for NBS SRM 2682 2682-2

2683- 1 Compiled Data for NBS SRM 2683 Sulfur in Coal 2683-1

2683- 2 Individual Data for NBS SRM 2683 2683-2

2684- 1 Compiled Data for NBS SRM 2684 Sulfur in Coal 2684-1

2684- 2 Individual Data for NBS SRM 2684 2684-2

2685- 1 Compiled Data for NBS SRM 2685 Sulfur in Coal 2685-1

2685-2 Individual Data for NBS SRM 2685 2685-2

2689-1 Compiled Data for NBS SRMs 2689-2691 Fly Ash (revised 3/1/87) 2689-1

2694-1 Compiled Data for NBS SRM 2694 Simulated Rainwater (revised 3/1/87) 2689-1

4350-1 Compiled Data for NBS SRM 4350 Environmental Radioactivity Standard, River Sediment 4350-1

4350- 2 Individual Data for NBS SRM 4350 4350-2

4350B-1 Compiled Data for NBS SRM 4350B Environmental Radioactivity, River Sediment 4350B-1

4350B-2 Individual Data for NBS SRM 4350B 4350B-2

4351- 1 Compiled Data for NBS SRMs 4351 and 4352 Environmental Radioactivity

(Human Lung and Human Liver) 4351-1

4353-1 Compiled Data for NBS SRM 4353 Environmental Radioactivity - Rocky Flats Soil #1 ... 4353-1

4353-2 Individual Data for NBS SRM 4353 4353-2

4355-1 Compiled Data for NBS SRM 4355 Environmental Radioactivity - Peruvian Soil 4355-1

4355-2 Individual Data for NBS SRM 4355 4355-3

xi i
List of SRM Data Tables (cont.)

Table # Title Page

8030- 1 Compiled Data for NBS RM 8030 Trace elements in an Aquatic Plant Lagarosiphon Major

Community Bureau of Reference BCR No. 60 (revised 8/1/87) 8030-1

8031- 1 Compiled Data for NBS RM 8031 Trace Elements in an Aquatic Moss Platihypnidium

Riparioides, Community Bureau of Reference BCR No. 61 (revised 8/1/87) 8031-1

8032- 1 Compiled Data for NBS RM 8032 Trace Elements in a Calcareous Loam Soil

Community Bureau of Reference BCR No. 141 (revised 8/1/87) 8032-1

8033- 1 Compiled Data for WBS RM 8033 Trace Elements in a Light Sandy Soil

Community Bureau of Reference BCR No. U2 (revised 8/1/87) 8033-1

803A-1 Compiled Data for NBS RM 8034 Trace Elements in a Sewage Sludge

Community Bureau of Reference BCR No. 144 (revised 8/1/87) 8034-1

8035- 1 Compiled Data for NBS RM 8035 Trace Elements in a Sewage Sludge of Mainly

Industrial Origin, Community Bureau of Reference BCR No. 146 (revised 8/1/87) ...... 8035-1

8036- 1 Compiled Data for NBS RM 8036 Trace Elements in a Spiked Skim Milk Powder

Community Bureau of Reference BCR No. 150 (revised 8/1/87) 8036-1

8412-1 Compiled Data for NBS RMs 8412 and 8413 Corn Stalk and Kernel (revised 3/1/87) 4355-3

8431-1 Compiled Data for NBS RM 8431 Mixed Diet (revised 3/1/87) . 8431-1

xiii
ff ( f
Compilation of Elemental Concentration Data for N8S Clinical, Biological, Geological, and Environmental

Standard Reference Materials

Concentration data on as many as 92 constituents in 166 NBS Standard Reference Materials have been collected

from over 1500 journal articles and technical reports. These data are summarized in consensus (mean) values

with uncertainties expressed as ± one standard deviation and compared with all available certification data

from NBS. Data are presented on the analytical procedures employed and all raw data are given in the tables.

This compilation is a successor to NBS Special Publication 260-88.

Keywords: Analytical methods, biological, certified, clinical, compilation, consensus values, environmental,

geological, informational values, literature values, mean values. Standard Reference Materials, SRM.

Certain commercial equipment, instruments, or materials are identified in this report to adequately specify the

procedure used for data compilation. Such identification does not imply recommendation or endorsement by the

National Bureau of Standards or the Department of Energy, nor does it imply that the materials or equipment

identified are necessarily the best available for the purpose.

Ernest S. Gladney and Bryan T. O'Malley

Health and Environmental Chemistry Group, MS K-484

Los Alamos National Laboratory

Los Alamos, New Mexico 87545

Iwan Roelandts

Geologie, Petrologie, et Geochimie

Universite de Liege

B-4000 Sart-Tilman par Liege 1 Belgium

Thomas E. Gills

Office of Standard Reference Materials

National Bureau of Standards

Gaithersburg, Maryland 20899

DISCLAIMER

1. Introduction CSRM's) for use in clinical, biological,

geological ,arKl environmental analytical chemistry.

The basic goal of the SRM program is to provide

homogeneous and stable materials of a variety of

natural matrices, for use in technique development

and in analytical quality assurance. The function

of SRM's in the latter role has been

well -documented in a series of publications by

Taylor (2-5). Standard Reference Materials carry

the full legal weight and authority of NBS and the

U.S. Department of Commerce, as they have been

specifically authorized by fecjeral legislation.

This compilation is a revised, updated, and

expanded version of the 1982 edition published as NBS Special Publication 260-88 in 1984 (1). It is

produced in a "living manual" format with the

intent that individual tables will be revised

whenever sufficient new data have appeared in the

literature. These revisions will be provided to

all known holders of the manual.

The National Bureau of Standards (NBS) has

produced nearly 200 Standard Reference Material^

1
The concentrations of as many as 44 constituents have been determined by NBS at one of two

confidence levels in each SRM: certified values

and non-certified or informational values. The

former is the present best estimate of the true

concentration of that constituent and is not

expected to deviate from that concentration by more than the stated uncertainty. These certified

concentrations are determined at NBS or with

cooperating laboratories using either a definitive

method, two or more independent methods, or refer- ence methods. These methods and other certification criteria have been carefully defined by

Uriano and Gravatt (6). Constituent

concentrations that are labeled as non-certified

or informational are those that NBS has not

measured by a defini- tive method, a reference

method, or two or more independent methods.

A limitation of many of these SRM's has been

the restricted number of constituents that NBS can

afford to certify in each material. Numerous

investigators outside NBS have published concen- tration data on constituents in these reference

materials. Although brief review articles on NBS

SRM's occasionally appear in the literature (7,8), we believe that the user should have access to both the summarized "consensus" value or mean concentration value and all the data on which they

were based. This philosophy has been the basis of

most of our previous compilation efforts (9-18).

Because abstracting services do not have a category "standard reference materials" and this label

is rarely used in keyword indices published with

articles, the widely scattered data in reports,

articles, books, and conference proceedings have

been collected only with difficulty.

Data conpilations also provide a mechanism

for quality assurance checks on agency or com- piler's "certified" values. Consistent disagreement between the user community and a certifying

agency should encourage the material's producer to carefully re-examine his certification measure- ments on the elefnent(s) that are in dispute.

There has been continuing controversy annong compilers concerning the determination and reporting of final compositional information on refer- ence materials. Flanagan (19) has used

"recommended", "average", and "magnitude" to characterize his "estimates" for major conponents

and trace elements in United States Geological

Survey materials. Abbey (20,21) has coined the

term "usable value" for some of his results and

pioneered the "select Laboratories" approach for

arriving at overall compositional information.

Gladney and Goode (13) elected to report only

"mean values" and associated standard deviations

without further attempt to assess the varying

quality of data determined by different analytical

techniques. For the French geostandards (CRPG,

ANRT) Roubault, et al. (22) have considered

"recommended", "preferred", and "proposed" values

depending upon the degree of confidence they felt

could be attached to the data. Steele, et al.(23), have reported "recommended" values in the

six NIMROC rock samples using some statistical

methods. Gladney, et al. (15), chose the term

"consensus values" to describe their mean values

calculated for USGS rocks after judgemental and

statistical eliminations of initial outliers.

Lister (24) has examined other "robust" estimators

which he believes provide better estimates of true

concentations than mean values. Flanagan (25) has

used two-way analysis of variance to produce "best

estimates of composition" on three recent USGS

reference rock samples. Abbey and Rousseau (26)

have debated the merits of "Pragmatism vs Rigour"

as approaches to the resolution of "disparate"

analytical data on four Canadian Iron- Format ion

reference samples. Lister (27) has used plotting

of "S-distribution curves" in an attempt to more closely examine analytical data included in

reference materials compilations. Abbey (28) has

also recently examined the use of "robust"

estimators and Flanagan (29) has recently reviewed

the entire spectrum of approaches to composition

determination in reference samples.

Approaches to value judgement of data quality

or even the advisability of compiling reference

materials data can be debated endlessly. The

responsibility for the informed end use of these

compi led data, regardless of who performed the

compilation, lies with individual investigators.

Each should read our methodology carefully and

critically so that he may decide for himself its

limitations. The values in the tables must not be

used uncritically. All data behind our mean "consensus values" are presented in the succeeding

table so that anyone may recalculate them to reflect his own experience whenever desired.

2
2. Data Conpilation

A listing of the 167 SRH's included in this

document is provided in Table 1, along with the

most recent certification date, the number of data

points included in the present compilation, and

the relative amount of this data which is new from

the previous compilation. All NBS certified and

informational values for these SRM's are reported

in the individual data tables for ease of comparison. Certified values have uncertainties stated,

while informational/uncertified values do not.

The 67 major journals in analytical

chemistry, geology, petrology, geochemistry, and

environmental science that have been surveyed

are shown in Table II. Less comprehensive

coverage of books and institutional reports for

1972-1985 has been achieved. More than 1500

different references containing original data on

NBS materials have been located. All tables

containing summarized data are numbered xxxx-1

while all individual data follow in the table

numbered xxxx-2, where xxxx is the NBS SRM number

of the material. These latter tables contain the

individual data, uncertainties (where provided),

references, and the analytical techniques used.

All individual data located were assembled

using a VAX 11/730 minicomputer with a VAX-VMS

(version 4.2) operating system, an RA-80 121 Mb

fixed-media disc drive, three RL-02 10 Mb

cartridge disc drives, the Common Data Dictionary

(version 3.2) and VAX Datatrieve (version 3.2)

software packages (all are registered trademarks

of the Digital Equipment Corporation, Manard,

Massachusetts). Datatrieve is an interactive data

storage and maintenance software system that provides facilities for selective data retrieval,

updating, sorting, formatting, and report generation with a minimum of programming overhead. Data

were hand-entered into the system via terminal

keyboard from copies of the original references.

Details of our Datatrieve based data management

system are published elsewhere (30).

Upon closing of the database for calculation

and publication of the compiled data, all individual records were inspected for typographical

errors in material name, element name, units,

analytical methods, etc. Those identified were corrected using simple user-generated Datatrieve

procedures. Data were then sorted by material.

then constituent, and finally units. This collection was inspected (via another user- generated

Datatrieve procedure) to identify constituents

within a given material that had two or more unit

types for the same element. These were then cor- rected to the same set of units for each conflicting set found using another Datatrieve procedure.

Data were resorted by material, constituent, and

in ascending order of concentration within each

constituent (this can be accomplished in a single

operation within Datatrieve). This year, to conserve space, we have chosen to eliminate all

reports of limit values (less-than and

greater-than) from materials and elements where

the data justify confidence in our ability to report a real consensus value. Some subjective

criteria, as described by Abbey (21) were used to eliminate data on either end of the reported con- centration spectrum that we judged to be clearly

beyond the limits of acceptability. Following

these eliminations (usually less than 1% of the

total data), an initial mean and standard deviation were computed using all remaining data for a given constituent in each SRM. All data points

now outside ± two standard deviations from the

initial mean were dropped and a revised mean and

standard deviation recomputed. These final means

and associated standard deviations are reported as our consensus values in Tables 1A-1 to 4355-1 for

up to 92 constituents. The number of literature

values used to calculate each final value is

indicated in the tables. Where sufficient data

exist, the median was also determined using all

data other than "less-than" values.

The compiled data were again resorted by

material, constituent, and groups of analytical

methods. An iterative mean and standard deviation

(using ± 2s for first round eliminations) were calculated for groups of analytical methods which

had sufficient data (i.e., instrumental thermal,

instrumental epithermal, radiochemical thermal,

radiochemical epithermal, general neutron activation, and delayed neutron methods were all com- bined into neutron activation; general,

wave-length dispersive, and energy dispersive

methods into X-ray fluorescence, etc.). These

analytical method means and associated standard

deviations are also included in the tables.

Mean values in the summary tables (xxxx-1

series) that are based upon less than three data

points do not include standard deviations. In a few cases the reported data had such a wide range

3
as to render the mean value calculation

meaningless. Such cases are reported as ranges

only (no standard deviation specified).

Additionally, there are a few elements where only

upper limit data exist, and these are given as only limit values in the tables.

3. Discussion

Our consensus values for major and minor

elements in some SRM's can be subjected to a test

commonly used by geochemists. "Whole material"

summations, similar to geochemists "whole rock"

summations, can be calculated from elemental data

when oxygen data are available, or the elements

can be converted to stoichiometric oxides and then

summed. The latter approach is inappropriate for

coals, oils, biologicals, and non-silicate rocks

where many elements are not present in oxide

forms. Because we still have not located any

reports of oxygen determination in any of the

biological SRM's, the "whole material" summation

test cannot yet be applied. There are sufficient

oxygen data on three coals and two fly ash

materials to attempt the "whole nnaterial" sunmation. It is important that all concentration data

used are either on a "dry-weight" basis or that

the hydrogen or bound and unbound water be

included as individual items in constituents

summed. For two silicate rock SRM's where insufficient oxygen data exist, major and minor

elements have been converted to stoichiometric

oxide forms and summed. In all cases, the uncer- tainties (where known) are propagated onto the

final sum using standard statistical techniques.

The results of these calculations are shown below

in Table III. Summations of 99 - 101 % are con- sidered a good indication that the major and minor

element data are reasonably accurate and internally consistent. The material summations for NBS

SRM's 278, 688, 1632A, 1633, 1633A, and 1635 meet

this quality criteria, although the propagated

uncertainty on the coals (1632A and 1635) are much

larger than one would prefer. The summation for

NBS SRM 1632 is over 2% lower than the previous

compilation, due to a drop in the consensus value

for oxygen. Since the two oxygen measurements

located differ by a factor of 1.5, the uncertainty

on this consensus value is quite high. In the

future it is hoped that good oxygen data will be

available so that this approach can be applied to

a larger number of materials.

The growth of the body of SRM data since the

last compilation is summarized in Table I. More

details about the changing patterns in reference

material measurements, their sources, the analytical techniques used, and the constituents

measured were recently described by Gladney and

Roelartdts (31).

The key to analytical method codes (METHOD)

is given in Table IV. The key to the COMMENT code

is given in Table V. All data reported as oxides

in the original references were converted to elemental form using the conversion factors shown in

Table VI. The individual data (CONC), their

uncertainties when provided (UNCER), analytical

technique used (METHOD), and the individual refer- ences are given in Tables numbered xxxx-2 for each

SRM. These tables were generated with

user-written Datatrieve "procedures," the VAX

Datatrieve report writing facilities and the DEC

Keypad editor. All tables were printed on a Hewlett-Packard LaserJet printer. Data that were reported as "greater- than" values have been

omitted entirely, and "less-than" values are shown

as «<" under CONC and "L" under COMMENT. As

mentioned above, less-than values that no longer

offer any useful perspective on elements with

well-established values have been dropped from the

database to conserve space. The data have been

sorted in ascending order based upon material,

constituent, and concentration using VAX

Datatrieve. All the references (CODE and NUM)

have been identified in Reference Appendix. The

CODE consists of the last two digits of the year

of publication plus the first three letters of the

first author's last name. The two digit numerical

suffix (NUM) is provided to enable handling of

multiple reports by the same first author in the same year. This particular reference coding

system was adopted in preference to a sequential

numbering system in 1980 to permit rapid searching

of the reference database using Datatrieve, and to permit easy random updating of both the reference

and concentration databases without the necessity

of renumbering the references. Since over 4000

references with data on various NBS, United States

Geological Survey (USGS), and Canadian Certified

Reference Materials Project (CCRMP) materials are

now in our system, these considerations are extremely important.

4
4. Conclusion ACKNOWLEDGEMENTS

Although we have endeavored to achieve as wide a coverage of the literature as possible, we

realize that this compilation is still incomplete.

We appreciate the efforts of those investigators

who have sent us their data directly, and we con- tinue to request that the users of this compilation call our attention to omissions and errors so that they may be corrected in subsequent editions.

Anyone with unpublished results or data published

in "technical reports" that may not be widely circulated, on any NBS, USGS, or CCRMP reference

materials are urged to send their data to the

first author of this compilation and it will be

placed in our database with appropriate reference

to the source.

We remain indebted to the compilers of refer- ence material data that have preceeded us. We

also thank William Goode (DEC) and Daniel Perrin

(Los Alamos County) who helped us establish our original data management framework. We also thank

June Gladney and Christy Gladney for their

assistance with editing and proofreading of this

manuscript.

CREDIT

. This work was performed under the auspices of

the U.S. Department of Energy and the U.S.

National Bureau of Standards.

REFERENCES

1. Gladney, E. S., C. E. Burns, D. R. Perrin, I. Roelandts, and T. E. Gills, "1982 Compilation of Elemental

Concentration Data for NBS Biological, Geological, and Environmental Standard Reference Materials," NBS

Special Publication 260-88, 221 pp., 1984.

2. Taylor, J. K., Anal. Chem., 53: 1588A-1596A (1981).

3. Taylor, J. K., "Reference Materials -- How They Are, or How They Should be Used," Presented at the ASTM

C-26 Committee Meeting, Knoxville, TN, 1982.

4. Taylor, J. K., Anal. Chem., 55: 600A-608A (1983).

5. Taylor, J. K., "Handbook for SRM Users," NBS Special Publication 260-100, 1985.

6. Uriano, G. A., and C. C. Gravatt, Crit. Rev. Anal. Chem., 6: 361-411 (1977).

7. Nadkarni, R. A. and G. H. Morrison, J. Radioanal. Chem, 43: 347-369 (1978).

8. Gladney, E. S., Anal. Chim. Acta, 118: 385-396 (1980).

9. Gladney, E. S., "Compilation of Elemental Concentration Data for NBS Biological and Environmental Standard

Reference Materials," Los Alamos Scientific Laboratory Report LA-8438-MS, Los Alamos, New Mexico,

119 pp., 1980.

10. Gladney, E. S., "Compilation of Elemental Concentration Data for United States Geological Survey's Eight

New Rock Standards," Los Alamos Scientific Laboratory Report LA-8265-MS, Los Alamos, New Mexico, 55 pp., 1980.

11. Gladney, E. S., "Compilation of Elemental Concentration Data for Fourteen Canadian Certified Reference

Materials Project Standards," Los Alamos Scientific Laboratory Report LA-8382-MS, Los Alamos, New Mexico,

28 pp., 1980.

5
12. Gladney, E. S., "Compilation of Elemental Concentration Data for the United States Geological Survey's

Six Geochemical Exploration Reference Materials," Los Alamos Scientific Laboratory Report LA-8473-MS, Los

Alamos, New Mexico, 18 pp., 1980.

13. Gladney, E. S. and U. E. Goode, Geostandards Newsletter, 5: 31-64 (1981).

14. Gladney, E. S., "Comparison of Methods for Calculation of Recomnended Elemental Concentrations for

Canadian Certified Reference Materials Project Rock Standards SY-2, SY-3, and MRG-1," Los Alamos

Scientific Laboratory Report LA-8770-MS, Los Alamos, New Mexico, A pp., 1981.

15. Gladney, E. S., C. E. Burns,

16. Gladney, E. S., C. E. Burns,

17. Gladney, E. S., C. E. Burns,

and I. Roelandts, Geostandards

and !. Roelandts, Geostandards

and I. Roelandts, Geostandards

Newsletter, 7: 3-226 (1983).

Newsletter, 8: 119-154 (1984)

Newsletter, 9: 35-68 (1985).

18. Abbey, S. and E. S. Gladney, Geostandards Newsletter, 10: 3-11 (1986).

19. Flanagan, F. J., Geochim. Cosmochim. Acta, 37: 1189-1200 (1973).

20. Abbey, S., Geostandards Newsletter, 2: 141-146 (1978).

21, Abbey, S., X-ray Spect., 7: 99-121 (1978).

22. Roubault, M., H. de la Roche, and K. Govindaraju, Sciences de la Terre, Nancy, IX: 105-121 (1966).

23. Steele, T. W., A. Wilson, R. Goudvis, P. J. Ellis, and A. J. Radford, "Analysis of the NIMROC Reference

Samples for Minor and Trace Elements," National Institute of Metallurgy report 1945, 222 pp.

24. Lister, B., Geostandards Newsletter, 8: 171-172 (1984).

25. Flanagan, F. J., "Three USGS Mafic Rock Reference Samples, W-2, DNC-1, and BIR-1," U.S. Geological Survey

Bulletin 1623, 54 pp., 1984.

26. Abbey, S. and R. M. Rosseau, Geostandards Newsletter, 9: 1-16 (1985).

27. Lister, B., Geostandards Newsletter, 9: 263-273 (1985).

28. Abbey, S., Geostandards Newsletter, 10: 159-168 (1986).

29. Flanagan, F. J., "Reference Samples in Geology and Geochemistry," U. S. Geological Survey Bulletin 1582,

72 pp., 1986.

30. Gladney, E. S., "Data Base Design and Management for Elemental Compositional Studies of Environmental and

Geological Reference Materials," Los Alamos National Laboratory report, in press, 1987.

31. Gladney, E. S. and I. Roelandts, "Distribution of NBS, USGS, and CCRMP Reference Material Data in the

Literature (1951-1985)," Geostandards Newsletter, 11: in press (1987).

6
TABLE I: NATIONAL BUREAU OF STANDARDS BIOLOGICAL, ENVIRONMENTAL, AND GEOLOGICAL STANDARD REFERENCE MATERIALS

SRM Number Name Certification Date # data % New

(1986) (1986)

1A Argillaceous Limestone 1931 98 19

lb Argillaceous Limestone 1966 77 32

1c Argillaceous Limestone 1978 37 100

27F Iron Ore (Sibley) 1977 1 100

56 Tennessee Phosphate Rock 1927 1 0

56B Phosphate Rock (Tennessee Brown) 1947 3 0 69A Bauxite 1951 81 44

69B Bauxite (Arkansas) 1979 0

--

70 Feldspar 1926 24 0

70a Feldspar 1981 64 22

76 Burnt Refractory 1955 10 0

76A Burnt Refractory 1985 0

--

77 Burnt Refractory 1955 12 0

77A Burnt Refractory 1985 0

--

78 Burnt Refractory 1955 2 0 78A Burnt Refractory 1985 0

--

79A Fluorspar 1971 1 100

80 Soda-Lime Glass 1927 2 0

81A Glass Sand 1978 0

--

88 Dolomite 1928 14 21 88A Dolomitic Limestone 1982 100 48

88B Dolomitic Limestone 1986 0

--

91 Opal Glass 1931 54 20

92 Soda-Lime Glass Powder 1982 3 100

93A Borosilicate Glass 1973 2 0 97 Flint Clay 1931 86 3

97A Flint Clay 1969 64 22

98 Plastic Clay 1931 134 0 98A Plastic Clay 1969 60 20

99 Soda Feldspar 1931 57 2 99A Feldspar 1981 42 12 120A Phosphate Rock (Florida) 1961 21 24

120B Phosphate Rock (Florida) 1979 188 43

181 Lithium Ore (Spodumene) 1981 1 100

182 Lithium Ore (Petalite) 1981 0

183 Lithiun Ore (Lepidolite) 1981 0

278 Obsidian Rock 1981 296 59

330 Copper Ore, Mill Heads 1977 0

331 Copper Ore, Mill Tails 1977 0

332 Copper Concentrate 1977 1 100

333 Molybdenum Concentrate 1977 0

470 Mineral Glasses for Microanalysis 1979 0

610 Trace Elements in Glass (500 ppm) 1972 126 72

612 Trace Elements in Glass (50 ppm) 1982 112 85

614 Trace Elements in Glass (1 ppm) 1982 81 84

616 Trace Elements in Glass (0.02 ppm) 1982 24 88

7
TABLE I: NATIONAL BUREAU OF STANDARDS BIOLOGICAL, ENVIRONMENTAL, AND GEOLOGICAL STANDARD REFERENCE MATERIALS

(cont.

)

SRM Number Name Certification Date M data % New

(1986) (1986)

633 Portland Cement 1974 11 100

634 Portland Cement 1974 3 100

635 Portland Cement 1974 10 100

636 Portland Cement 1974 11 100

637 Portland Cement 1974 '10 100

638 Portland Cement 1974 10 100

639 Portland Cement 1974 10 100

688 Basalt Rock 1981 255 76

694 Western Phosphate Rock 1984 0

--

696 Bauxite (Surinam) 1979 30 100

697 Bauxite (Dominican) 1979 0

--

698 Bauxite (Jamaican) 1979 33 100

909 Human Serum 1985 0

--

1083 Wear-Metals in Lubricating Oil 1985 0

--

1084 Wear-Metals in Lubridating Oil 1985 30 100

1085 Wear-Metals in Lubricating Oil 1985 27 100

1549 Non-Fat Milk Powder 1984 56 100

1566 Oyster Tissue 1983 425 77

1567 Wheat Flour 1978 317 55

1568 Rice Flour 1978 269 58

1569 Brewer's Yeast 1976 139 12

1570 Trace Elements in Spinach 1976 715 36

1571 Orchard Leaves 1977 3113 27

1572 Citrus Leaves 1982 139 89

1573 Tomato Leaves 1976 758 34

1575 Pine Needles 1976 664 34

1577 Bovine Liver 1977 2262 23

1577a Bovine Liver 1982 216 100

1581A PCBs in Oi

I

1982 0

1581B PCBs in Oi

I

1982 0

1581C PCBs in Oi

I

1982 0

1581D PCBs in Oi

I

1982 0

1582 Petroleum Crude Oil 1984 8 100

1584 Priority Pollutant Phenols 1984 10 100

1585 Chlorinated Biphenyls 1986 0

1587 Nitrated Polycyclic Aromatic Hydrocarbons 1985 0

1590 Stabi li Ized Wine 1985 4 100

1614 Dioxin 1985 0

8
TABLE I: NATIONAL BUREAU OF STANDARDS BIOLOGICAL, ENVIRONMENTAL, AND GEOLOGICAL STANDARD REFERENCE MATERIALS

(cont.

)

SRH Number Name Certification Date # data % New

(1986) (1986)

1618 Vanadium and Nickel in Residual Fuel Oil 1985 0

1619 Sulfur in Residua Fuel Oil 1981 18 100

1620 Sulfur in Residua Fuel Oil 1979 0

1620a Sulfur in Residual Fuel Oil 1981 19 100

1621 Sulfur in Residual Fuel Oil 1967 5 20

1621a Sulfur in Residual Fuel Oil 1980 7 14

1621b Sulfur in Residual Fuel Oil 1981 7 100

1622 Sulfur in Residual Fuel Oil 1967 2 100

1622a Sulfur in Residual Fuel Oil 1979 5 20

1622b Sulfur in Residual Fuel Oil 1981 7 100

1622c Sulfur in Residual Fuel Oil 1986 0

1623 Sulfur in Residual Fuel Oil 1971 4 0

1623a Sulfur in Residual Fuel Oil 1981 6 100

1624 Sulfur in Distillate Fuel Oil 1971 4 0

1624a Sulfur in Distillate (Diesel) Fuel Oil 1981 6 100

1630 Trace Mercury in Coal 1971 72 4 1631A Sulfur in Coal 1974 8 50

1631B Sulfur in Coal 1974 6 33

4 Z7 4 0* 1631C Sulfur in Coal 1974 7 43

1632 Trace Elements in Coal 1974 1810 16

1632A Trace Elements in Coal (Bituminous) 1983 952 51 1632B Trace Elements in Coal (Bituminous) 1985 0

1633 Trace Elements in Coal Fly Ash 1975 2057 4 7

13

1633A Trace Elements in Coal Fly Ash 1985 850 60

1634 Trace Elenients in Fuel Oil 1975 4 TO 138 4 T

17

1634A Trace Elements in Fuel Oil 4 not 1982 95 100

1634B Trace Elements in Fuel Oil 1986 0

1635 Trace Elements in Coal (Subbituminous) 1979 454 46

1639 Halocarbons for Water Analysis 1983 0

1641 Mercury in Water - Concentrate 1975 1 0

1641A Mercury in Water - ug/mL 1978 0

1641B Mercury in Water - ug/mL 1983 1 100

1642 Mercury in Water - Trace 1974 0

1642A Mercury in Water - ng/mL 1977 4 75

1642B Mercury in Water - ng/mL 1982 2 100

1643 Trace Elements in Water 1977 132 61

1643A Trace Element;s in Water 1980 313 88

1643B Trace Elements in Water 1984 29 100

1645 R i ver Sediment 1982 524 64

1646 Estuarine Sediment 1982 173 98

1647 Priority Pollutant Polynuclear Aromatic Hydrocarbons 1981 13 100

1648 Urban Particulate Matter 1982 371 33

1649 Urban Dust/Organics 1982 64 64

9
TABLE I: NATIONAL BUREAU OF STANDARDS BIOLOGICAL, ENVIRONMENTAL, AND GEOLOGICAL STANDARD REFERENCE MATERIALS

(cont.)

SRM Number Nanne Certification Date # data % New

(1986) (1986)

lis io Total Chlorine in Lubricating Base Oil i9oo U IBIy Sulfur in Lubricating Base Oil 0

IBJJO Portland Centent U loo 1 Portland Cement 4 Oct/ 0

Benzene on Charcoal lyf f 0

2661A Benzene on Charcoal 1978 2 100

Tl >£ m-Xylene on Charcoal 1977 0

p~Dioxane on Charcoal 1977 1 TOO

1 j2-Dichloroethane on Charcoal 1977 c

4 t\f\ lOO

Chloroform on Charcoal 1977 1

4 nn TOO

Trichloroethylene on Charcoal 197f 1 TOO

cool Carbon tetrachloride on Charcoal \yf7 m1 TOO

i£Of U Toxic Metals in Freeze-Dried Urine 4 00c 1 7 1 no lUU

do 11 Freeze Dried Urine Certified for Fluorine 190 u col£. Freeze-Dried Urine Certified for Mercury 10VC 7

1 UU

ox.7/. Lead on Filter Media 1 Q70 nu Beryllium on Filter Media 107C 19f 3 1

cOf O Meta iS on r 8 Iter ReQ 1

9

n

U

£Os Oh netSLS on riiter n6Qia 107A 0y inn 1 UU

£.Of OD rie ta I s on r i iter ncQ i a n

V

COI s otzt y I I B USII aiKJ nrSCM 1 C Un r 1 I t€l ricu 1 a n

uuariz on riirer neuia 107A u ^OOc oULTUr in KfOa I 10RX 7*; inn 1 UU

b-UlTUr in Loai A7Of 11 nnUU

suiTur in Losi lyoo A7Of 11 nnUU

2685 Sulfur in Coal 1983 67 100

2689 ' Coal Fly Ash 1986 0

2690 Coal Fly Ash 1986 0

2691 Coal Fly Ash 1986 0

2694 Simulated Rainwater 1986 0

4350 Environmental Radioactivity Standard: River Sediment 1975 12 67

4350B Environmental Radioactivity: River Sediment 1981 23 74

4351 Environmental Radioactivity: Human Lung 1982 0

4352 Environmental Radioactivity: Human Liver 1982 0

4353 Environmental Radioactivity: Rocky Flats Soil #1 1981 28 82

4355 Environmental Radioactivity: Peruvian Soil 1982 0

8412 Corn (Zea Mays) Stalk 1986 0

8413 Corn (Zea Mays) Kernel 1986 0

8419 Bovine Serum 1985 84 100

8431 Mixed Diet 1986 0

10
TABLE II: LITERATURE SURVEYED

I

Journal Vol. # data % total

Acta Chimica Hungarica 113 - 119 0

Acta Chimica Scandanavia 39A, :39B 0

American Laboratory 11 - 17 132 0.6

American Mineralogist 67 - 70 0

Ana I us is 1 - 13 128 0.6

Analyst 97 - 110 922 4.6

Analytica Chimica Acta 53 - 178 1115 5.5

Analytical Chemistry 44 - 57 3574 17.7

Analytical Instrumentation 13 - 14 0

Analytical Letters 1 - 18 97 0.5

Annales de la Societe Geologique de Belgique 91 - 108 0

Applied Spectroscopy 25 - 39 265 1.3

Atomic Absorption Newsletter 1 - 18 111 0.6

Atomic Spectrometry 1 - 6 169 0.8

Biological Trace Element Research 1 - 8 31 0.2

Bulletin des Societes Chimiques Beiges 80 - 94 3 <0.1

Bunseki Kagaku 24 - 34 966 4.8

Canadian Journal of Earth Sciences 9

- 22 20 0.1

Canadian Journal of Spectroscopy 20 - 30 59 0.3

Chemical Geology 13 - 53 108 0,5

Comptes-Rendus Hebdomadaires des Seances de I 'Academic

des Sciences (Paris) 272 - 301 1 <0.1

Conference Proceedings 1523 7.6

Contributions to Mineralogy and Petrology 36 - 91 10 <0.1

Earth and Planetary Science Letters 1

- 77 15 <0.1

Economic Geology 67 - 80 0

Environmental Geology 1

- 5 9 <0.1

Environmental Letters 1 - 10 13 <0.1

Environmental Pollution 29A - 39A 22 0.1

IB - 10B

Environmental Research 1

- 38 4 <0.1

Environmental Science and Technology 5

- 19 469 2.3

Fresenius Zeitschrift fur Analytische Chemie 244 - 322 589 2.9

Geochemistry International (trans, from Geokhimiya) 9

- 22 0

Geophysical Research Letters 1

- 7 25 0.1

Geochimica et Cosmochimica Acta 36 - 49 169 0.8

Geostandards Newsletter 1

- 9 1146 5.7

Geotechnical Testing Journal 1 - 7 0

Geochemical Journal 7

- 19 6 <0.1

International Journal of Applied Radiation and Isotopes 23 - 36 14 <0.1

International Journal of Environmental Analytical Chemistry 1

- 23 161 0.8

International Journal of Environmental Studies 1 - 25 9 <0.1

Journal of Analytical Chemistry of USSR (trans, of

Zhurnal Anal iticheskoi Khimii) 26 - 38 0

Journal of Environmental Quality 1 - 1^ 14 <0.1

Journal of Environmental Radioactivity 1

- 3 0

Journal of Environmental Science and Health 11 - 20 79 0.4

Journal of Geochemical Exploration 1

- 24 0

Journal of Petrology 12 - 26 0

11
TABLE II: LITERATURE SURVEYED (cont.)

Journal Vol. # data % total

Journal of Radioanalytical and Nuclear Chemistry 10 - 96 2436 12.1

Journal of Research of the USGS 1 - 6 25 0.1

Journal of the Association of Official Analytical Chemists 55 - 68 734 3.6

Journal of the Geological Society (London) 127 - 142 0 ...

Journal of the Soil Science Society of America 46 - 48 2 <0.1

Journal of the South African Chemical Institute 21 - 37 0

...

Journal of Volcanology and Geothermal Research 1 - 26 0

...

Lithos 4

- 18 0

...

Marine Geology 12 - 44 0

...

Mass Spectroscopy 31 - 32 0

...

Microchemical Journal 17 - 28 3 <0.1

Mikrochimica Acta (Wien) 1972 - 1984 98 0.5

Mineralogy Magazine 40 - 44 0 —

Nuclear Instruments and Methods 114 - 172 268 1.3

Precambrian Research 1

- 14 2 <0.1

CIO 1 A Radiochimica Acta 17 - 38 0

Radiochemical and Radioanalytical Letters 1

- 59 468 2.3

Reports and Books 2617 13.0

Sedimentology 16 - 28 0

Spectrochimica Acta 27B - 40B 423 2.1

Spectroscopy Letters 17 - 18 0

Talanta 19 - 32 238 1.2

X-ray Spectrometry 1

- 14 179 0.9

Misc. sources 364

Total 20113 100.0

12
TABLE III: WHOLE MATERIAL CONCENTRATION SUMMATIONS OF MAJOR AND MINOR ELEMENTS FOR SELECTED NBS SRMs (7o)

1633 1633A 1632 1632A 1635

ELE CONSENSUS CONSENSUS CONSENSUS CONSENSUS CONSENSUS

Mean ± SD Mean ± SD Mean ± SD Mean ± SD Mean ± SD

Al 12.6 ± 0.6 14.4 ± 0.7 1.73 ± 0.10 2.95 ± 0.10 U • C.7J — u . Ba 0.266 ± 0.016 0.142 ± 0.010

C 3.3 ± 0.2 70.6 ± 1.7 64.4 ± 3.9

Ca 4.65 ± 0.34 1.14 ± 0.06 0.418 ± 0.042 0.241 ± 0.017

Fe 6.16 ± 0.27 9.37 ± 0.23 0.851 ± 0.044 1.11 ± 0.03 0.229 ± 0..006

H 0.02 0.04 4.29 ± 0.22 4.1 ± 0.4 4.07

K 1.69 ± 0.09 1.88 ± 0.05 0.278 ± 0.017 0.411 ± 0.02

Mg 1.5 ± 0.3 0.457 ± 0.045 0.156 ± 0.041 0.115 ± 0.02 0.104 ± 0,.013

N 1.20 ± 0.14 1.25 ± 0.04 1.16 ± 0,.32 Na 0.3130 ± 0.02 0.173 ± 0.011 — 0.239 ± 0,.020

0 47.02 47.66 12.6 18.8 ± 0.8 30 ± 8

P 0.101 ± 0.018 0.169 ± 0.024

S 0.450 ± 0.050 0.190 ± 0.070 1.32 ± 0.08 1.55 ± 0.05

Si 22.0 ± 1.0 23.0 ± 0.9 3.08 ± 0.24 5.87 ± 0.22 0.590 ± 0..050

Sr 0.138 ± 0.010

Ti 0.710 ± 0.050 0.823 ± 0.039 0.163 ± 0.01

Other 0.33 0.39 0.33 0.27 u . u 1

Total 101.25 ± 1.3 99.83 ± 1.17 96.85 ± 1.74 101.23 ± 4.01 inn ? + R 1

. 1

278 688

OXIDE CONSENSUS CONSENSUS

Mean ± SD Mean ± SD -

Al 0 14.39 ± 0 .25 17.33 ± 0.30

2 3

BaO 0 .11 ± 0 .01

'°2 0 .18 0.05

CaO 1 .00 ± 0 .02 11.85 ± 0.50

'V3 0 .49 1.8

FeO 1 .38 7.645

"/

"2°

0

0

.30

.05

0.14

0.11

K 0 4 .07 ± 0 .12 0.19 ± 0.01

2 MgO 0 .25 8.72 ± 0.36

MnO 0 .05 ± 0 .01 0.16 ± 0.01 Na 0 4.72 ± 0.05 2.09 ± 0.11

2

P 0

Z 5 SiO

0 .03 0.16 ± 0.05

71 .52 ± 1 .28 48.22 ± 0.32

. 2 0 .24 ± 0 .01 1.18 ± 0.03

Other 0 .16 0.17

Total '98 .98 ± 1 .31 99.82 ± 0.77
Code

TABLE IV: ANALYTICAL METHOD CODES FOR INDIVIDUAL DATA TABLES

Specific Technique Code Specific Technique

14NAA 14 MeV Neutron Activation Analysis

AA General, Flame Atomic Absorption: Unspecified,

or Mixed Conditions

AAC Flame Atomic Absorption Preceeded by Chemical

Separation

ABS Absorption (69FLA 01)

AE+AF Atomic Emission + Atomic Fluorescence

AF Atomic Fluorescence

AS Alpha Spectrometry

ASV Anodic Stripping Voltammetry

CALC Calculated

CB Combustion: Elemental Analyzer

CB-GC Combustion + Gas Chromatography

CHEM Chemical (taken from several other compilers,

usually undefined)

CHEML Chemi luminescence, Cando luminescence

CHROM Chromatographic

COLOR Colorimetry, Photometry, Spectrophotometry

CONV Conventional (taken from several other

compilers, usual ly undefined)

COUL Coulometry

CPAA Charged Particle Activation Analysis

CPXRF Charged Particle Induced X-ray Fluorescence

CSV Cathodic Stripping Voltammetry

CVAA Cold Vapor Atomic Absorption

DCPES Direct Coupled Plasma Atomic Emission

Spectrometry

DNA Delayed Neutron Activation Analysis

ESCA Electron Spectroscopy for Chemical

Appl i cat ions

ESR Electron Spin Resonance

EXRF Energy Dispersive X-ray Fluorescence

FA Fire Assay

FA-AA Fire Assay-Atomic Absorption

FA-OS Fire Assay-Optical Emission Spectrometry

FAA Flameless Atomic Absorption (Electrothermal,

Carbon Rod)

FAAC Flameless Atomic Absorption Preceeded by

Chemical Separation

FAE Flameless Atomic Emission

FD Freeze Drying

FE Flame Emission, Flame Photometry, Atomic

Emission

FLUOR Fluorometry

GAMMA Direct Gamma-ray Counting (without activation)

GC Gas Chromatography

GC-AA Gas Chromatography-Atomic Absorption

Spectrometry

GC-MS Gas Chromatography-Mass Spectrometry

GCMES Gas Chromatography Microwave Emission

GE Gas Evolution (CO^ in rocks)

GRAV Gravimetry

HAA Hydride Evolution Atomic Absorption

I Infrared

IC Ion Chromatography

ICPAF Inductively Coupled Plasma Atomic Fluorescence

ICPES Inductively Coupled Plasma Atomic Emission

Spectrometry

ICPMS Inductively Coupled Plasma Mass Spectrometry

IDMS Isotope Dilution Mass Spectrometry

IE Ion Exchange (76FLA 04)

lENA Instrumental Epi thermal Neutron Activation

ISE Ion Selective Electrodes

ITNA Instrumental Thermal Neutron Activation

KF Karl Fischer Method for H 0

2 LC Liquid Chromatography (reversed or normal

phase)

MECA Molecular Emission Cavity Analysis

MOSS Mossbauer Spectroscopy

MPOES Microwave Plasma Optical Emission Spectrometry

MS General Mass Spectrometry

NAA Neutron Activation Analysis: General,

unspecified, or mixed conditons

NM Nuclear Methods (general)

NT Nuclear Track

OES General, DC Arc Optical Emission Spectrometry

PAA Photon Activation or X-ray Activation Analysis

PC Paper Chromatography

PEN Penfield Method (HO ) 2 POL Polarography

POT Potentiometry (69FLA 01, 69FLE 01) PM Petrographic Microscope

PROBE Ion or Electron Microprobe Mass Analyzer

PYHYD Pyrohydro lysis

RENA Radiochemical Epithermal Neutron Activation

RR Rapid rock

RTNA Radiochemical Thermal Neutron Activation

SIMS Secondary Ion Mass Spectrometry

SM Semi -micro (69FLE 01)

SSMS Spark-source Mass Spectrometry

TC Thermal Conductivity

TCGS Thermal Neutron Capture Prompt Gamma- ray

Spectrometry

TITR Titrimetry

TURB Turbidimetry

UU Unspec i f i ed

VOLT Voltammetry (76FLA 04)

VOLU Volumetry (76FLA 04)

W Various, Mixed Methods

WXRF Wavelength Dispersive X-ray Fluorescence \

XRF General or Unspecified X-ray Fluorescence

14
TABLE V: COMMENT Codes for Individual Data Tables

Code Definition

* Data eliminated from all mean value calculations.

D Same data reported in two or more references. Duplicate data are flagged and oldest reference used in mean calculations.

H Hydride generation

L Limit (less than) data. Not used in computations.

R Concentration range. Not used in computations.

1 Different nebulizers used for independent results.

2 V 0 catylist used in dissolution.

2 5 3 Different electrodes used for independent results.

4 Aqueous slurry of reground sample.

5 Different radioactive isotopes or irradiation conditions used for independent results.

6 Different methods of standardization used for independent results.

7 Different chemical separation methods used for independent results.

8 Isotope dilution methods combined with spark source mass spectrometry.

9 Gamma -gamma coincidence.

10 Different neutron filters used for independent results by epithermal neutron activation analysis.

11 Different dissolution or matrix destruction methods used for independent results.

12 Different methods of peak integration or dead time correction used for independent results.

13 Different detectors used for independent results.

14 Different furnace configurations used for independent results.

15 Different laboratories prepared fused beads used for independent results.

16 Different matrix correction methods used for independent results.

17 Different laboratories or analysts reporting independent results in same reference.

18 Different bottles of reference material used for independent results.

19 Duplicate entries from same reference from previous data compilation assembled by another compiler; reason for duplication unknown.

20 Different emission/absorption lines used for independent results.

21 Dichromate used for FEO determination (76FLA 04).

22 Vanadate used for FEO determination (76FLA 04).

+ 23 Modified Penfield method used for H 0 determination.

2 24 Different irradiation containers used for independent results.

25 Different colorimetric methods used for independent results.

26 CONC and UNCER should be multiplied by 10(-5).

28 CONC and UNCER should be multiplied by 10(-3).

30 Results were used by NBS to determine certified values.

31 Different chemical methods used for independent results.

32 Different background correction or excitation sources or crystals used for independent results by XRF. 33 Different pellet sizes used for independent results.

34 Reported on a dry weight basis.

35 Reported on an as-received basis.

36 OES pre-ignition at various temperatures for independent results.

37 Karl Fischer titration for H 0 . 38 CONC and UNCER are XI 0(9), A/G=atoms/gram

40 Different gamma- rays from the same isotope used for independent results.

41 Acid evolution method for CO determination.

44 Different conditions employed for independent results by Liquid Chromatography.

15
TABLE VI: Factors Used for Oxide to Element Conversions

Oxide Multipl ier Oxide Multipl ier

Al^03

BaO

BeO

CO

2

CaO

CdO

CoO

Cs 0

2

CuO

FeO to fe^O^

FeO

Fe^O^

Ga^O^

<^0

La^03

Li^O

MgO

MnO

0.529

0.311

0.896

0.360

0.273

0.715

0.875

0.786

0.684

0.943

0.799

1.112

0.777

0.699

0.592

0.830

0.853

0.465

0.603

0,774

""2°3

"V4

MoO_

Na^O

Nd^O^

NiO

''2°5

PbO

Rb 0

2

SiO.

SO.

^^2°3

SrO

TiO.

^2°3

ZnO

ZrO

0.696

0.720

0.667

0.742

0.857

0.786

0.436

0.928

0.914

0.467

0.400

0.652

0.846

0.599

0.848

0.560

0.787

0.803

0.740

16
TABLE 1A-1: COMPILED DATA FOR NBS SRM 1A ARGILLACEOUS LIMESTONE (revised 3/1/86)

ELE UNITS NBS CONSENSUS MEDIAN RANGE XRF OES OTHER METHODS

Mean Mean ± SD (n) Mean Mean t SD (n) Mpan ± SD Cn) Method

Al X

1 o"? _». n no c..c5 ± U.Uo ('

)

2.1 2.36 O 1

^: . To 2.18 (2) COLOR

A t Al V 2.36 (1) RR

AA 1

2.29 (1) TITR

A 1 A

/o 2.27 (1) DCPES

AoAS ug/g 1

1 .OA / 1 ^ 1 .6 (1) AA

Qb ug/g onyu 80 100 onyu

Ha ug/g ^ Ann <V Ann ouu Be ng/g Of U 670 (1) AA

D « B1 ng/g / 1 \ K 1 / 57 (1

)

AA

C" 1 A y. ij o n^ J. n on 1"^ \

V j; O 1

y. lo 8.82 9.17 9.05 ± 0.20 (3) COUL

ug/g o 1 uu ^Ann jOUU / 1 \ 5600 t1

)

CALC

C-T ^ 9.72 9.73 9.72 (1

)

COUL

T c

% 9.73 (1) CB

Ld oo A + n 1

V J/ ^yOO . oA 29.5 29.7 ^y.o 29.7 (1) DCPES

La 29.5 (1

)

RR

T/J Lu ng/g 32 (1

)

AA LO ug/g 7 O f 1 ^ 3.9 (1

)

NAA

cr ug/g OA C ^O. D 23 30 / 1 \ 23 (1

NAA

LU ug/g /In / 1 \

re 1 1/. 1 1 1 * n n7 1 11 . 1 1 .08 1 .15 1 nA 1 - uo \ 1 ) 1.1 (1

)

COLOR

re y 1 .08 (1) DCPES

re 1.15 (1) TITR

re n 1 .13 (1) RR ba ug/g H

^ 1 ^

/H / 1 ^

ng ng/g Jr.* A4 71 .4 57.7 (2) AA ug/g lonn JTUU Aonn / 1 \ 6900 (1) RR

La ug/g 1 nn 1

1 nnuu /IN

LUi . J J

'¥

1 DC 11 . 7AJjH 1

* nU . n^UD 1 7 1.29 1.39 1

1 . 7nJU /?N 1.39 (1) DCPES

Mn^g %n 1.37 (1) RR nn ug/g ^yu AAn hhu +z inn I uu jUU 320 500 LLt\ HH-U +Z inn lUU /^^

nu ug/g < 1 Mana ug/g coyu o^nn ^ouu It/ 2300 2700 2700 (1) DCPES

Na ug/g 2300 (1) RR

Nug/g 11 nu / 1 \ in1 U / 1 \ Dr ug/g A';n 1 n7^ 650 1500 /

\

1

\ )

\ mnn 1 ^UU / 1 ^ Ph ug/g ioIT. 7J +Z

1

1 .oA 10ly. 11 17.2 21 pn 19.1 ± 1.9 (3) AA

C ug/

g

OARn ^ojU +z lAn iou ^ouu OAnn 2620 3073 pAnn / 1 > 2840 ± 200 (5) CB

cd ug/g 3000 (1

)

TURB

ng/g o^U 630 f 1 i AA

aC ug/g To (1 )

1 1; /In

d 1 o. jy A An A n no o . OU ± U . Uo (3/ A 6.53 6.72 A / 1 N

1 1 / 6.63 (1) COLOR

d 1 6.58 (1

)

RR

a 1 6.72 (1) DCPES

Qnan ug/g 0 17 /On 1 .68 2.58 2.13 (2) AA

ar ug/g 1 yju ioin 1 y 1 U +± iAn IhU 10/ n ly^u 1700 2000 iAAn 1 OOU +Z iAn lOU \->) 2000 (1) NAA

T 1 1ug/g in /n OAn THU +Z "^n jU oAn you 900 1000 900 (1) DCPES

T i

1 1 ug/g 960 (1) NAA

1 1 iifi ug//ng 900 (1) RR

11 1ug/g m/n 1 JO 156 (1) ICPES

\lV

1ug/g tn /fi ^n /IN 7n3U / 1 \

Y ug/g lU r 1 \ (1) 10 / i \ (1

)

Zn ug/g 20.15 (2) 17 23.3 17 (1) 23.3 (1) NAA

Zr ug/g 60 (1) 60 (1)

1A-1
TABLE 1A-2: INDIVIDUAL DATA FOR NBS SRM 1A (revised 3/1/86)

Cone Uncer Com Method Reference 1 Cone Uncer Com Method Reference

A I (%) 1 Cd (ng/g)

2.1 OES 62 JOE 01 1 32 AA 84TER 01 2.17 0.01 1 1 COLOR 830HM 01 2.19 0.01 1 1 COLOR 830HM 01 I Co (ug/g)

2.23 OES 78KN0 01 2.27 DCPES 73KAR 01 1 * 10 L OES 63CLA 01 2.29 TITR 58WAT 01 1 3,9 1.4 RTNA 61TUR 01 2.36 RR U 1

1 Cr (ug/g)

As (;ug/g>

1 23 RTNA 61TUR 01

1 .6 HAA 84TER 04 1 30 OES 63CLA 01

B (ug/g) 1 Cu (ug/g)

80 3 OES 63CLA 01 1 3 OES 63CLA 01 100 3 OES 63CLA 01

1 Fe (%) Ba (ug/g)

1 0.855 OES 62J0E 01

< 800 L OES 63CLA 01 1 1.08 OES 78KN0 01

1 1.08 DCPES 73KAR 01 Be (ng/g) 1 1.1 COLOR 59COL 01

1 1.13 RR 73KAR 01 670 AA 82TER 02 1 1.15 TITR 69WIC 01 670 D AA 83TER 01

1 Ga (ug/g)

Bi (ng/g)

1 ^ OES 63CLA 01 57 D FAA 84TER 03

57 HAA 84TER 02 1 Hg (ng/g)

C-I (%) 1 44 FAA 75HEI 01

1 71.4 2.16 FAA 82FLA 01 8.8234 0.5651 41 COUL 85ENG 01 9.16 0.07 41 COUL 86CAH 01 1 K (ug/g)

9.1673 0.0273 41 COUL 85ENG 01

1 6900 RR 73KAR 01 C-0 (ug/g)

1 La (ug/g)

5600 1800 CALC 86CAH 01

1 100 OES 63CLA 01 C-T (%)

1 Mg (%)

9.72 0.17 COUL 86CAH 01 9.73 CB 78TER 01 1 1.29 OES 78KN0 01

1 1.3 OES 62J0E 01 Ca (7.) 1 1.37 RR 73KAR 01

1 1.39 DCPES 73KAR 01 28.6 OES 62J0E 01 29.5 RR 73KAR 01 29.6 XRF 78KN0 01 29.7 DCPES 73KAR 01

1A-2
TABLE 1A-2: INDIVIDUAL DATA FOR NBS SRM 1A (cont.)

Cone Uncer Com Method Reference 1 Cone Uneer Com Method Reference

Mn (uq/g) 1 Si (%)

320 OES 78KN0 01 1 6.53 XRF 78KN0 01 500 3 OES 63CLA 01 1 6.54 OES 62J0E Ol 500 3 OES 63CLA 01 1 6.58 RR 73KAR 01

1 6.63 COLOR 74SHA 01 Mo (ug/g) 1 6.72 DCPES 73KAR 01

<

4

1 L OES 63CLA 01 1 Sn (ug/g)

Na (uq/g) 1 1.68 AA 82TER 01

1 2.58 0.1 FAA 85TER 01 2300 RR 73KAR 01 2700 DOPES 73KAR 01 1 Sr (ug/g)

Ni (ug/g) 1 1700 OES 75TH0 01

1 1940 OES 58GRA 01 10 OES 63CLA 01 1 2000 3 OES 63CLA 01

1 2000 RTNA 61TUR 01

P <ug/g> 1 3000 3 OES 63CLA 01

650 WXRF 71 FAB 01 1 Ti (ug/g)

1500 OES 78KN0 01

1 900 RR 73KAR 01 Pb (ug/g) 1 900 DCPES 73KAR 01

1 960 61 RTNA 65UAH 01 17.2 FAA 75CAM 02 1 1000 OES 78KN0 01 19.1 AA 8ATER 01 1 1500 3 OES 63CLA 01 20 OES 63CLA 01 1 2500 3 OES 63CLA 01

21 FAA 79HEI 03

1 U (ug/g)

S (ug/q)

1 155.75 1.86 ICPES 83N0R 01 2620 CB 84LEC 02

2700 CB 55COL 01 1 V (ug/g)

CB 74RUN 01 2800 OES 78KN0 01 1 30 OES 63CLA 01 ^ouu 1 II

uu 72BOU 01 3000 TURB 73SHA 01 1 Y (ug/q)

3020 90 CB 77LAN 01 3073 CB 78TER 01 1 10 OES 63CLA 01

Sb (ng/g) 1 Zn (ug/g)

630 HAA 84TER 04 1 17 XRF 65BAL 01

1 23.3 RTNA 65BAL 01 Sc (uq/q)

1 Zr (ug/g)

15 OES 63CLA 01

1 60 OES 63CLA 01

1A-3
TABLE 1B-1: COMPILED DATA FOR NBS SRM IB ARGILLACEOUS LIMESTONE (revised 3/1/86)

ELE UNITS NBS CONSENSUS RANGE AA ICPES OES OTHER METHODS

Mean Mean ± SD (n) Mean (n) Mean (n) Mean <n) Mean (n) Method

-i^

Ag ug/g — < 5 ... < 5 ... ...

Al ug/g 5920 5730 (2) 5660 5800 — 5660 (1) 5800 (1) ...

As ug/g < 5

~ - - - < 5 — —

Au ug/g < 3

... < 3 — ...

Ba ug/g 86 (1) ... 86 (1) —

Be ng/g - • * 420 (1) * . — 420 (1) — ...

Bi ug/g < 25 - - - < 25 — . _ -

C-! % 11.0 ... ... ... — ...

Ca X 36.4 36.31 i 0.44 (3) 35.93 36.8 36.2 (1) 35.93 (1) 36.8 (1) ... Cd ng/g " 41 (2) 30 52 30 (1) ... 52 (1) IDMS

Ce ug/g ... 7.81 (1) ... ... 7.81 (1) — ...

CI ug/g - - . 70 (1) ... — 70 (1) XRF Co ug/g " ~ ~ 4.1 (1) . . - 4.1 (1) — ...

Cr ug/g ... 15.7 (1) A . . 15.7 (1) ... ...

Cu ug/g _ - - 5.5 (1) ... 5.5 (1) — . - - Oy ug/g 0.9 (1) ... 0.9 (1) — ...

Er ng/g 570 (1) ... 570 (1) — ...

Eu ng/g 240 (1) . . . ... 240 (1) — ...

F ug/g ... 1766 (1) — 1766 (1) XRF

Fe ug/g 5240 5320 ± 280 (3) 5000 5500 5500 (1) 5460 (1) 5000 (1) ...

Gd ug/g - - - 0.97 (1) 0.97 (1) — ...

H9 ng/g 15.7 (1) 15.7 (1) — ...

Ho n#/g 200 (1) 200 (1) — ...

K ug/g 2100 2100 (2) 2000 2200 2200 (1) 2000 (1) — ...

LOI % 41.1 — — ...

La ug/g ... 6.86 (1) ... 6.86 (1) — . . -

Li ug/g . - - < 2

... < 2 — . . -

Lu ng/g ... 80 (1) 80 (1) — , ...

Mg ug/g 2170 2150 ± 220 (3) 2000 2400 2000 (1> 2040 (1) 2400 (1) ... Nn ug/g 1550 1510 ± 85 (3) 1430 1600 1600 (1) 1510 (1) 1430 (1) ...

No ug/g ... < 3

... < 3 — ...

Na ug/g 300 330 (2) 260 400 400 (1) 260 (1) ... ...

Nd ug/g ... 4.88 (1) 4.88 (1) —

Nf ug/g 11 (1) ... 11 (1) ...

P ug/g 350 370 (1) 370 (1) ... ...

Pb ug/g ... 9.5 (2) 2 17 2 (1) 17 (1) - _ . ...

Pr

S

ug/g

ug/g

...

...

1.18

146

(1)

(2) 100

...

192

1.18 (1) . - -

... 192 (1) XRF

S ug/g . . - — ... ... 100 (1) CB

Sb ug/g . - - < 10 < 10 ...

Se u§/g ~ * "* < 30 ... < 30 ... ...

Si % 2.3 2.3 (2) 2.28 2.32 2.32 (1) 2.28 (1) COLOR

Sm ug/g - - - 0.89 (1) . . . 0.89 (1) — ...

Sn ug/g - - - < 3 < 3 — ...

Sr" ug/g 1180 1170 ± 60 (3) 1100 1208 1100 (1) 1208 (1) 1200 (1) ...

Th ug/9 ... < 25 25 — ...

Ti ug/g 280 296 (2) 292 300 292 (1) 300 (1) ... U ug/g - - - < 30 30 ... ...

V ug/g — 29.45 (2) 28.8 30.1 30.1 (1) 28.8 (1) ...

y ug/g ... 7 CD 7 (1) —

Yb ng/g 1325 (2) 550 2100 1325 (2)

Zn ug/g 40.7 (1) 40.7 (1) Zr ug/g 16 (1) 16 (1)

1B-1
TABLE 1B-2: INDIVIDUAL DATA FOR NBS SRM IB (revised 3/1/86)

Cone Uncer Com Method Reference

Ag (ug/g)

Al (ug/g)

5660

5800

As (ug/g)

200

Au (ug/g)

Ba (ug/g)

86

Be (ng/g)

420

Bi (ug/g)

1.7

50

Ca (%)

35.93

36.2

36.8

Cd (ng/g)

< 2000

30 80

52

Ce (U3/3?

7.81

CI (ug/g)

70

Co (ug/g)

4.1

15 L 0.48

< 5 L ICPES 81CHU 01

ICPES 81CHU 01 OES 73BES 01

< 5 L ICPES 81CHU 01

< 3 L ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

< 25 L ICPES 81CHU 01

1.19 ICPES 81CHU 01 AA 84SCH 01 OES 73BES 01

L ICPES 81CHU 01 AA 83G0G 01 IDMS 74R0S 02

ICPES 81CHU 01 ICPES 85JAR 02

WXRF 82LE0 03

ICPES 81CHU 01

Cone Uncer Com Method Reference

Cr (ug/g)

15.7

Cu (ug/g)

5.5

Dv (ug/g)

Er (ng/g)

570

Eu (ng/g)

240

1700

F (ug/g)

1766

Fe (ug/g)

5000

5460

5500

Gd (ug/g)

0.97

Hg (ng/g)

15.7

Ho (ng/g)

200

< (ug/g)

2000

2200

La (ug/g)

6.86

0.9 0.03

20

10

1200

140

5 L 0.05

0.9

10

50

5 L 0.35

ICPES 81CHU dl

ICPES 81CHU 01

ICPES 85JAR 02

ICPES 85 JAR 02

ICPES

ICPES

WXRF

OES

ICPES

AA

ICPES

ICPES

ICPES AA

ICPES

ICPES

85JAR 02

81CHU 01

82 LEO 03

73BES 01 81CHU 01 84SCH 01

81CHU 01 85JAR 02

FAA 82FLA 01

ICPES 85JAR 02

81CHU 01 84SCH 01

81CHU 01 85 JAR 02

1B-2
TABLE 1B-2: INDIVIDUAL DATA FOR NBS SRM IB (cont.)

Cone Uncer Com Method Reference 1 Cone Uncer Com Method Reference

Li (ug/g) 1 S (uq/Q)

< 2 L ICPES 81CHU 01 1 100 77LAN 01

1 192 UXRF 82LE0 03

Lu (ng/g)

1 Sb (ug/g)

80 10 ICPES 85 JAR 02

< 10 L ICPES 81CHU 01 Mq (uq/g)

1 Se (ug/g)

2000 AA 84SCH 01 2040 60 ICPES 81CHU 01 < 30 L ICPES 81CHU 01 2400 OES 73BES 01

1 Si (%)

Mn (ug/g)

1 2.28 0.05 COLOR 81F0N 01 1430 OES 73BES 01 1 2.32 dES 73BES 01 1510 45 ICPES 81CHU 01 1600 AA 84SCH 01 1 Sm ug/g)

Mo (ug/g) < 5 L ICPES 81CHU 01

1 0.89 0.04 ICPES 85 JAR 02

< 3 L ICPES 81CHU 01

1 Sn (ug/g)

Na (ug/g)

< 3 L ICPES 81CHU 01 260 15 ICPES 81CHU 01 400 AA 84SCH 01 1 Sr (ug/q)

Nd (ug/g) 1 1100 AA 84SCH 01

1 1200 OES 75THO 01

< 20 L ICPES 81CHU 01 1 1208 24 ICPES 81CHU 01 4.88 0.09 ICPES 85 JAR 02

1 Th (uq/q)

< 25 L ICPES 81CHU 01

11 1 ICPES 81CHU 01

1 Ti (ug/g)

P (uq/g)

1 292 6 ICPES 81CHU 01 370 9 ICPES 81CHU 01 1 300 OES 73BES 01

Pb (ug/g) 1 U (uq/q)

2 0.4 FAA 75CAM 02 < 30 L ICPES 81CHU 01 17 2 ICPES 81CHU 01

1 V (Ufl/q) Pr (ug/g)

1 28.8 OES 84PLS 01 1.18 0.03 ICPES 85JAR 02 1 30.1 1.4 ICPES 81CHU 01

1B-3
TABLE 1B-2: INDIVIDUAL DATA FOR NBS SRM IB (cont.)

Cone

Y (ug/g)

7

550

2100

Zn (ug/g)

A0.7

Zr (ug/g)

16

Uncer Com Method Reference

0.34

20

100

ICPES

ICPES

ICPES 85 JAR 02

85JAR 02

81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

lB-4
TABLE 1C-1: COMPILED DATA FOR NBS SRM 1C ARGILLACEOUS LIMESTONE (revised 3/1/86)

ELEMENT UNITS NBS

Mean t SD

CONSENSUS

Mean (n)

RANGE NAA

Mean (n)

ICPES

Mean (n)

OTHER METHODS

Mean (n) Method

AlBa

ug/g

ug/g

6880

-

160

84 <1) -- 84 (1) — —

Ca % 35.96 ± 0.21 — — — —

Cd ng/g 400 (1) — 400 (1) ...

Ce ug/g 7.14 (2) 6.87 - 7,4 7.4 (1) 6.87 (1) —

Co ug/g 1.15 (1) 1.15 (1) —

Cr ug/g .- 19 (1) 19 (1) — —

Cs ng/g 590 (1) 590 (1) — —

Dy ng/g - 640 (1) — 640 (1) —

Er ng/g - 410 (1) — 410 (1) —

Eu ng/g 165 (2) 160 - 170 170 (1) 160 (1) —

Fe ug/g 3840 + 210 3900 (1) 3900 (1) —

Gd ng/g 650 (1) — 650 (1) —

Hf ng/g 750 (1) 750 (1) — —

Ho ng/g - 140 (1) — 140 (1) —

K ug/g 2320 + 80 .... — — —

LOI % 39.9 + 0.1 — ... — —

La ug/g - 4.63 (2) 4 .,26 - 5 5 (1) 4.26 (1) —

Lu ng/g - 60 (2) -- 60 <1) 60 (1) —

Mg ug/g 2530 + 240 — -- — — —

Mn ug/g 190 40 — -- — — —

Na ug/g lb.0 ± 75 — -- ... — —

Nd ug/g - 3.72 (2) 3.7 - 3.73 3.7 (1) 3.73 (1) ...

P ug/g 175 ± 44 165 (2) 160 - 170 — 170 (1) 160 Pr ug/g -• 0.9 (1) -- — 0.9 (1) —

Rb ug/g -. 12.5 (1) 12.5 (1) — —

Sc ug/g 1.3 (1) 1.3 (1)

Si % 3.19 + 0.04

Sm ng/g 730 (2) 730 (1) 730 (1)

Sr ug/g 250 + 40

Ta ng/g 90 (1) 90 (1)

Tb ng/g 130 (1) 130 (1)

Th ug/g 1.02 (1) 1.02 (1)

Ti ug/g 420 ± 60

Tm ng/g 70 (1) 70 (1) U ug/g 1.5 (1) 1.5 (1)

Y ug/g 5.05 (1) 5.05 (1)

Yb ng/g 385 (2) 380 - 390 380 (1) 390 (1)

COLOR

1C-1
TABLE 1C-2: INDIVIDUAL DATA FOR NBS SRM 1C (revised 3/1/86)

Cone Uncer Com Method Reference

Ba (up/g)

84

Cd (ng/g?

400

Ce (ug/g)

6.87

7.4

Co (ug/g)

1.15

Cr (uq/g)

19

Cs <ng/g ?

590

Dv (ng/g)

640

Er tnq/g)

410

Eu (nq/g)

160

170

Pe (uq/q)

3900

Gd (ng/g)

650

Hf <ng/fl?

750

500

38

0.14

10

20

10

ITNA 85POT 02

FAA 83UCH 02

ICPES 83UCH 02

ICPES 85 JAR 02 ITNA 85POT 02

ITNA 85POT 02

ITNA 85POT 02

ITNA 85P0T 02

ICPES 85 JAR 02

ICPES 85 JAR 02

ICPES 85 JAR 02

ITNA 85P0T 02

ITNA 85POT 02

ICPES 85JAR 02

ITNA 85POT 02

Cone Uneer Com Method Reference

Ho (ng/g)

140

La (ug/g)

Nd (uq/g)

3.7

3.73

P_t%2

0.016

0.017

Pr (uq/g)

0.9

12.5

Sc (ug/g)

1.3

Sm (nq/g)

730

730

Ta (ng/g)

90

Tb (nq

130

Th (Ug/g)

1.02

10

4.26 0.1

5

60

60

0.05

0.0002

0.0001

20

ICPES 85JAR 02

ICPES

ITNA

ICPES

ITNA

ITNA ICPES

COLOR

ICPES

ITNA ICPES

85JAR 02

85POT 02

85JAR 02

85P0T 02

85POT 02

85JAR 02

83UCH 01 83UCH 01

0.02 ICPES 85JAR 02

ITNA 85POT 02

ITNA 85P0T 02

85P0T 02

85JAR 02

ITNA 85POT 02

ITNA 85P0T 02

ITNA 85POT 02

1C-2
TABLE 1C-2: INDIVIDUAL DATA FOR NBS SRM 1C (cont.)

Cone Uncer Com Method Reference |

I 70 ITNA 85POT 02 |

I

I 1.5 ITNA 85POT 02 |

I

i 5.05 0.02 ICPES 85JAR 02 |

I

I 380 ITNA 85POT 02 | 390 10 ICPES 85JAR 02 |

1C-3
TABLE 27F-1: COMPILED DATA FOR NBS SRM 27F SIBLEY IRON ORE

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

CONSENSUS

Mean

METHOD

Al ug/g 4340 160

Bi ng/g 150 (1) AA

Ca ug/g 280 ± 20

Fe X 65.97 ± 0.05

K ug/g 66 17

Mg ug/g 115 ± 25

Mn ug/g 85 15

Na ug/g 89 ± 22

P ug/g 410 i 10

S ug/g 50 ± 10

Si % 1.95 ± 0.02

Ti ug/g 110 ± 11

TABLE 27F-2: INDIVIDUAL DATA FOR NBS SRM 27F

(revised 3/1/86)

Cone Uncer Com Method Reference

Bi <ng/g)

150 FAA 84TER 03

TABLE 28-1: COMPILED DATA FOR NBS SRM 28 NORRIE IRON ORE

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean Mean

Mn ug/g 4400

27F-1
TABLE 56-1: COMPILED DATA FOR NBS SRM 56 PHOSPHATE ROCK

(revfsed 3/1/86)

ELEMENT UNITS

Al

Ca

Fe

P

S

%

%

%

7o%

NBS

Mean

1.62

32

2.31

13.66

CONSENSUS

Mean

METHOD

2.5 (1) TURB

TABLE 56-2: INDIVIDUAL DATA FOR NBS SRM 56

(revised 3/1/86)

Cone

S (%)

2.5

Uncer Com Method Reference

TURB 73SHA 01

TABLE 56B-1: COMPILED DATA FOR NBS SRM 56B PHOSPHATE ROCK

(revised 3/1/86)

ELEMENT UNITS

Ca

F

P

Si

%

%

%

%

NBS

Mean

31.5

3.4

13.76

4.72

CONSENSUS

Mean

METHOD

3.32 (2) ISE

4.8 (1) AA

TABLE 56B-2: INDIVIDUAL DATA FOR NBS SRM 56B

(revised 3/1/86)

Cone

F (%)

3.25

3.38

Uneer Com Method

11

11

ISE

ISE

Reference

71PET 01 71PET 01

Si (%)

4.8 0.05 AA 82KIS 01

56-1
TABLE 69A-1: COMPILED DATA FOR NBS SRH 69A BAUXITE ORE (revised 3/1/86)

ELE UNITS NBS CONSENSUS MEDIAN RANGE AA XRF OTHER METHODS

Mean Mean ± SD (n) Mean (n) Mean ± SD (n) Mean (n) Method

Al % 29.1 29.5 ± 0.4 (7) 29.2 29.17 - 30.20 29.2 (2) 29.68 ± 0.41 (4) 29.17 (1) TITR

As ug/g ... 12.4 (2) ... 12.2 - 12.7 12.7 (1) 12.2 (1) —

Ba ug/g 90 73 (1) ... ... ... 73 (1) —

Be ng/g ... 200 (1) ... ... 200 (1) ... —

Bi ng/g ... 668 (1) ... ... 668 (1) ... —

Ca ug/g 2100 1980 ± 80 (5) 1900 1900 - 2100 1900 (1) 2000 (1) 1900 (1) OES

Ca ug/g --- ... ... ... ... ... 2050 (2) TITR Cd ng/g ... 20 (1) ... ... 20 (1) ... —

Ce ug/g ... 94 (1) ... --- 94 (1) —

CI ug/g ... 117 (1) ... ... ... 117 (1) —

Co ug/g ... 3.5 (1) ... ... ... 3.5 (1) ...

Cr ug/g 340 270 (1) ... ... ... ... 270 (1) OES

Cu ug/g ... 9 (1) ... ... ... 9 (1) ...

Dy ug/g ... 4.5 (1) ... ... ... 4.5 (1) ...

F ug/g ... 1490 (1) ... ••- ... 1490 (1) —

Fe % 4.07 3.99 ± 0.12 (6) 3.9 3.82 - 4.12 3.96 (1) 3.93 ± 0.14 (3) 4.12 (1) OES

Fe % ... ... ... ... ... ... 4.07 (1) TITR

Ga ug/g ... 119 (1) ... ... ... 119 (1) —

Gd ug/g ... 3.2 (1) ... ... ... 3.2 (1) —

Hf ug/g ... 33 (1) ... ... ... 33 (1) ...

K ug/g < 80 75 (2) ... 70 - 80 ... 75 (2) —

LCI % 29.55 ... ... ... ... ... —

La ug/g ... 71 (1) ... ... ... 71 (1) ...

Mg ug/g 120 75 (2) ... 60 - 90 90 (1) ... 60 (1) OES

Hn ug/g < 80 23 (1) ... ... ... 23 (1) —

Na ug/g < 80 ... ... ... ... ... —

Nb ug/g ... 59 (1) ... — — 59 (1) ...

Nd ug/g ... 28 (1) ... — — 28 (1) ...

P ug/g 350 510 (2) ... 220 - 800 ... 220 (1) 800 (1) OES

Pb ug/g ... 34 (2) ... 31 - 37 30.8 (1) 37 (1) —

Pr ug/g ... 5.4 (1) ... ... ... 5.4 (1) —

S ug/g 160 300 ± 80 <4) 300 200 - 400 ... 358 (2) 200 (1) OES

S ug/g ... --- ... ... ... ... 300 (1) TURB

Sb ug/g ... 2.0 (2) ... 1.0 - 3.1 1.0 (1) 3.1 (1) ...

Sc ug/g ... 8.9 (1) ... ... ... 8.9 (1) —

Si % 2.81 2.82 ± 0.03 (5) 2.8 2.78 - 2.85 2.85 (2) 2.8 ± 0.02 (3) —

Stn ug/g ... 5.1 (1) ... ... ... 5.1 <1) —

Sn ug/g ... 8.2 (2) --- 8.0 - 8.5 8.51 (1) 8 (1)

Sr ug/g 49 (1) 49 (1)

Th ug/g 94 (1) 94 (1)

Ti % 1.66 1.62 ± 0.11 (7) 1.64 1.46 - 1.74 1.46 (2) 1.68 ± 0.04 (4) 1.7 (1) OES

U ug/g 6.2 (1) 6.2 (1)

V ug/g 170

Y ug/g 16 (1) 16 (1)

2n ug/g 11 (1) 11 (1) Zr ug/g 1330 1285 (1) 1285 (1)

69A-1
TABLE 69A-2: INDIVIDUAL DATA FOR NBS SRM 69A (revised 3/1/86)

Cone Method Reference 1 Cone Unccr Pmn Mf^thnH l\C 1 CI CI IL>C

Al (%) 1 Cr (ua/a)

29.17 TITR U 1

1 270 OES 78KN0 01 29.2 XRF 78KN0 01 29.2 1,04 AA 79BRE 02 1 Cu (uq/g)

29.2 1.04 AA 80LAB 03

29.64 XRF 79SCH 02 1 9 XRF 76LE0 02

29.68 0.07 XRF 80LAB 03

30.2 EXRF 80DAL 01 1 Dv (uq/q)

As (uq/q) 1

' XRF 76LE0 02

12.2 XRF 76LE0 02 1 F (ug/g)

12.7 HAA 84TER 04 1

1 1490 WXRF 82LE0 03

Ba (uq/q)

i Fe (%)

Jl XRF 76LE0 02

1 3.82 0.08 XRF 80LAB 03

Be (ng/g) 1 3.88 XRF 79SCH 02

1 3.96 0.03 AA 80LAB 03

200 AA 82TER 02 1 4.07 TITR 69WIC 01 200 D AA 83TER 01 1 4.09 EXRF 80DAL 01

1 4.12 OES 78KN0 01

Bi (ng/q)

1 Ga (ug/g)

668 HAA 84TER 02

668 D FAA 84TER 03 1 119 XRF 76LE0 02

Ca (uq/q) 1 Gd (ug/g)

1100 11 AA 79MEN 01 1 3.2 XRF 76LE0 02

1900 11 AA 79MEN 01 1900 OES 78KN0 01 1 Hf (ug/g)

2000 TITR 80HIT 02

2000 EXRF 80DAL 01 1 33 XRF 76LE0 02

2100 TITR 79MEN Ul

1 K (ug/g)

Cd (nq/q)

1 70 EXRF 80DAL 01 20 AA 84TER 01 1 80 XRF 78KN0 01

Ce (uq/q) I La (ug/g)

94 XRF f OLbU 1 XRF 76LE0 02

CI (ug/g) 1 Mg (ug/g)

117 UXRF 82LEO 03 1 60 OES 78KN0 01

1 90 AA 79MEN 01 Co (uq/q)

3.5 XRF 76LE0 02

69A-2
TABLE 69A-2: INDIVIDUAL DATA FOR NBS SRM 69A (cont.)

Cone Uncer Com Method Reference 1 Cone Uncer Com Method Reference

Mn (ug/g) 1 Sm (ug/g)

< 100 L OES 78KN0 01 1 5.1 XRF 76LE0 02

23 EXRF 80DAL 01

1 Sn (ug/g)

Nb (ug/g)

1 8 XRF 76LE0 02

59 XRF 76LE0 02 1 8.51 0.4 FAA 85TER 01

Nd (ug/g) 1 Sr (ug/g)

CO AKr rOLcU Kjc. 1 hV XKr 7A\ cn no fOLbU \jc

P (ug/g) 1 Th (ug/g)

EXKr oODAL 01 1 XRF 76LE0 02

Ubb loKnO l}\

1 Ti (%)

PD (ug/g)

\ 1 .32 0-11 COLOR 79BRE 01

A A AA Q/TCD ni ohIcR Ui 1 1 .HO n 1 / U- 1h AA 7Aone A

1

Z^VBRE 01

Of VDAK rr rOLcU KJc. 1 1 n 1 /. U . 1 H

A A AA oni AD ni

1

1 .OH u . \jc. VD C AKr pni AD nT

Pr (ug/g) 1 1 .06 XRF 79SCH 02

1 1 .66 0„01 XRF 79BRE 01 XKr fOLtO \Ji 1 1 7

1 ' ' OES 78KN0 01

1 1.74 EXRF 80DAL 01

S (ug/g)

1 U (ug/g)

200 OES 78KN0 01 ouu Tl IDD f JdflA U 1

1 A 7

1 O. c VD C AKr 7AI CO no rOLtU

717 J f 1 UVD C O^LtU

EXRF oODAL 01 1 Y (ug/g)

Sb (ug/g) 1 16 XRF 76LE0 02

1 HAA 84TER 04 1 Zn (ug/q)

3.1 XRF 76LE0 02

1 11 XRF 76LE0 02

Sc (ug/g)

8.9

Si (%)

XRF 76LE0 02 XRF 76LE0 02

2.44 EXRF 80DAL 01 2.78 XRF 78KN0 01 2.8 XRF 79SCH 02

2.82 0.04 XRF 80LAB 03

2.85 0.08 AA 80LAB 03

2.85 0.08 AA 79BRE 02

69A-3
TABLE 69B-1: COMPILED DATA FOR NBS SRM 69B BAUXITE ORE

(revised 3/1/86)

ELEMENT UNITS NBS

Mean t SD

Al % 25.8 ± 0.1 Ba ug/g 72

Ca ug/g .930 ± 140

Ce ug/g 240

Co ug/g 1 Cr ug/g 75 ± 14 Fe % 4.99 ± 0.08

Hf ug/g 63

K ug/g 560 ± 75

LOI % 27.2 ± 0.2

Mg ug/g 510 ± 50

Mn ug/g 850 ± 40

Na ug/g 180

P ug/g 514 ± 17

S ug/g 2500 i 80

Sc ug/g 8

Si % 6.27 ± 0.05

Ti % 1.14 ± 0.03

V ug/g 160 1 20

Zn ug/g 28 ± 4 Zr ug/g 2150 ± 520

69B-1
TABLE 70-1: COMPILED DATA FOR NBS SRM 70 POTASH FELDSPAR (revised 3/1/86)

ELEMENT UNITS NBS

Mean

CONSENSUS

Mean ± SD (n)

MEDIAN RANGE METHOD

Al % 9.54 " " ... ... ...

Ba ug/g 300 380 (1) ... ... NAA

Ca ug/g 500 ... ... ... ...

Ce ug/g < 4 NAA

Co ng/g 100 (1) NAA

Cr ug/g < 2 NAA

Cs ug/g 6.6 (1) NAA

Eu ng/g 400 (1) NAA

Fe ug/g 210 300 (1) NAA

Hf ng/g < 200 ... NAA

Hg ng/g 98 (1) AA

K % 10.44 - - - ... ...

LOI % 0.22 ... .... ...

La ug/g " ~ " < 3

... ... NAA

Lu ng/g ~ ~ ~ < 40 ... ... NAA

Mg ug/g 78 ... ... ...

Mn ug/g 7

... ... ...

Na % 1.76 ... ... ...

Nd ug/g ~ < 3

- - . ... NAA

P ug/g 52 ~ " ... ...

Rb ug/g ~ ~ " 470 (1) ... ... NAA

Sb ng/g " " " < 500 ... ... NAA

Sc ng/g 40 (1) ... ... NAA

Si % 31.13 ... ... ...

Sm ng/g < 500 NAA

Ta ng/g < 200 NAA

Tb ng/g < 200 NAA

Th ng/g < 400 NAA

Ti ug/g 12 Yb ng/g < 300 NAA

Zn ug/g 6.9 ± 0.8 (3) 7.3 6.0 - 7.5 NAA/XRF

Zr ug/g < 75 NAA

70-1
TABLE 70-2: INDIVIDUAL DATA FOR NBS SRM 70 (revised 3/1/86)

Cone Uncer Com Method Reference

Ba (uq/g)

380

Ce (ug/q)

Co (ng/g)

100

Cr (ug/g)

Cs (ug/g)

6.6

Eu (ng/g?

400

Fe (ug/g)

300

Hf (ng/ g ?

Hg (nq/g)

98

La (ug/g)

Lu (ng/g)

Nd (uq/q)

17

10

Rb (ug/g?

470 26

ITNA 77FLA 01

< 4 L ITNA 77FLA 01

ITNA 77FLA 01

< 2 L ITNA 77FLA 01

0.19 ITNA 77FLA 01

ITNA 77FLA 01

ITNA 77FLA 01

< 200 L ITNA 77FLA 01

5.95 FAA 82FLA 01

< 3 L ITNA 77FLA 01

< 40 L ITNA 77FLA 01

< 3 L ITNA 77FLA 01

ITNA 77FLA 01

Cone Uneer Com Method Reference

Sb (ng/q)

Sc (ng/g)

40

Sm (ng/g)

Ta (nq/g)

Tb (ng/g)

Th (ng/g)

Yb (ng/ g ?

Zn (ug/g)

< 500 L ITNA 77FLA 01

ITNA 77FLA 01

< 500 L ITNA 77FLA 01

< 200 L ITNA 77FLA 01

< 200 L ITNA 77FLA 01

< 400 L ITNA 77FLA 01

< 300 L ITNA 77FLA 01

6 0.71 ITNA 77FLA 01

7.3 RTNA 65BAL 01 7.5 XRF 65BAL 01

(ug/g)

< 75 L ITNA 77FLA 01

70-2
TABLE 70A-1: COMPILED DATA FOR NBS SRM 70A POTASH FELDSPAR (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE AA NAA OTHER METHODS

Mean Mean ± SD (n) Mean (n) Mean (n) Mean ± SD (n) Method

Al X 9.47

Ba ug/g 180 121 (2) ... 120 - 122 ... 120 (1) 121.9 (1) IDMS

B« ng/g ... 640 (1) ... 640 (1) ... ...

Bi ng/g T - - 68 (1) ... .. 68 (1) ... . . »

c ug/g ... 50 <1) ... ... ... 50 (1) CB

Ca ug/g 790 770 (2) . — - 640 - 900 770 (2) ...

Cd ng/g 8.7 (1) ... ... 8.7 (1) IDMS

Ce ug/g * . . < 4

... ... ... < 4

Co ng/g ... 200 (1) ... . — ... 200 (1) ...

Cr ug/9 . . - < 4

. — — . _ . < 4...

Cs ug/g ... 9.64 (2) ... 9.28 - 10 10 (1) 9.28 (1) ...

Eu ng/g ... 570 (1) - - - 570 (1) ...

Fe ug/g 520 600 ± 100 (3) 600 490 - 700 595 (2) 600 (1) ...

Hf ng/g ... < 300 ... < 300 ...

-

Ng ng/g ... 15 (1) - - . - - . 15 (1) ... ...

K % 9.79 9.76 ± 0.07 (4) 9.71 9.71 - 9.85 9.82 (2) 9.71 (1) ISE K X 9.71 (1) FE LOI X 0.4 ... ... ... ...

La ug/g ... < 2

... _ - - < 2 ...

Lu ng/g 8.0 (1) 8.0 (1) IDMS

Na X 1.87 1.86 ± 0.04 (5) 1.87 1.8 - 1.9 1.87 (2) 1.85 (1) XRF Na X

... 1.9 (1) FE Na X

... ... 1.8 (1) ISE Nd ug/g — < 3

... ... < 3

Rb ug/g 550 525 ± 9 (9) 524.2 507 - 540 540 (1) 530 (1) 519 (2) XRF Rb ug/9 ... ... - . - 524 ± 4 (4) IDMS

Rb ug/g ... 520.4 (1) MS

S ug/g ... 3.0 (1> 3.0 (1) CB

Sb ng/g < 400 ... < 400 . - .

Sc ng/g ... 110 (1) ... ... 110 (1)

Se ug/g 66.1 (1) 66.1 (1) XRF

Si % 31.3 ... Sm ng/g ... < 200 ... < 200 ...

Sn ug/g ... 0.75 (1) ... 0.75 (1) ... ...

Sr ug/g 64.7 ± 1.4 (6) 64.8 62.4 - 66.4 62.43 (1) XRF

Sr ug/g 64.8 (1) MS

Sr ug/g 65.2 ± 1.0 (4) IDMS

Sr-87/86 ratio 1.2002 ± 0.0024 (3) 1.2002 1.1978 - 1.2025 1.2002 (1) MS

Sr-87/86 ratio 1.2002 (2) IDMS Ta ng/g 150 (1) 150 (1)

Tb ng/g < 200 < 200

Th ng/g 300 (1) 300 (1)

Ti ug/g 60

Tl ug/g 2.81 <2) 2.72 - 2.91 2.81 (2) ASV

Yb ng/g < 500 < 500

2n ug/g < 5 < 5 Zr ug/g < 90 < 90

70A-1
TABLE 70A-2: INDIVIDUAL DATA FOR NBS SRM 70A (revised 3/1/86)

Cone KCI CI Ci ICC 1 ul KoCl

120 5 ITNA 77FLA 01 1 < 300 L ITNA 77FLA 01

121 .9 ' IDMS 69LAE 01 1

Vies be f r\n / n\ tng/g;

IS 1 0"?

640 AA 83TER 01 1

Bi (nq/q)

9.71 FE 75PUF 01 68 FAA 84TER 03 1 9.71 ISE 75PUF 01 9.79 AA 73RAM 01

j 9.85 AA 84SCH 01

PR

Ca (ug/g) < 2 L ITNA 77FLA 01

640 AA 73RAM Q1 1 Lu (ng/g)

900 AA R4SrH 01 1 100 77FI III LnA niV 1 ua ^ng/g; o

8.7 IDMS 74R0S 02 1 Na (%)

Ce (uq/q) [ 1.8 ISE 75PUF 01 1.85 WXRF 83BAL 01 < 4 L ITNA 77FLA 01 1 1.87 AA 84SCH 01 1.87 AA 73RAM 01 Co (ng/g) j 1.9 FE 75PUF 01

200 ITNA 77FLA 01 1 Nd fua/al

1 ITMA 77FLA 01

AH 1L T1 TUA 1 nn 77FI A ni 1 f r r LM u 1 1 KD tug/g;

sn7 4 83\/Al 01 S10 J IT 1 • I 9.28 0.15 I TNA 77FLA fir i.n 01w 1 1 520.4 MS 84ZIC 01

10 AA 72ALL 01 1 523.4 IDMS 70LAE 01 524.2 1.5 IDMS 74C0R 01 529 a 1 6 IDMS 69C0M 01 S29 9 1 XRF 69COM 01 101 w I TUA 1 nn 77ft A (11 ! 530 ITNA 77FLA 01 540 AA 72ALL 01

Fe (uq/q)

S (ug/g)

490 AA 73RAM 01 ! 600 ITNA 77FLA 01 1 3 CB 78TER 01 700 AA 84SCH 01 1

70A-2
TABLE 70A-2: INDIVIDUAL DATA FOR NBS SRM 70A (cont.)

Cone Uncer Com Method Reference

Sb (nq/g)

< 400 L ITNA 77FLA 01

Sc (na/g)

110

Se (ug/g)

66.1

Sm (ng/g)

ITNA 77FLA 01

0.2 XRF 69C0M 01

< 200 L ITNA 77FLA 01

Sn (ug/g)

0.75

Sr <ug/g?

AA 82TER 01

62.43 WXRF 83VAL 01 64 0.4 IDMS 74COR 01 64.8 MS 84ZIC 01 65.1 0.1 IDMS 69C0M 01

65.5 IDMS 82KRA 01 66.4 IDMS 70LAE 01

Sr-87/86 (ratio)

Cone Uncer Com Method Reference

Yb (ng/g)

< 500 L ITNA 77FLA 01

< 5 L ITNA 77FLA 01

2r (ug/g)

< 90 L ITNA 77FLA 01

1.1978 0,0033 IDMS 74C0R 01 1.2002 MS 84ZIC 01 1.2025 0.0012 IDMS 69C0M 01

Ta (ng/9)

150 8 ITNA 77FLA 01

Tb (ng/g)

200 L ITNA 77FLA 01

Th (ng/g?

300 ITNA 77FLA 01

2.715 0.217 7 ASV 82CAL 01 2.906 0.25 7 ASV 82CAL 01

70A-3
TABLE 76-1: COMPILED DATA FOR NBS SRM 76 BURNT REFRACTORY (revised 3/1/86)

CI FMPUT \jn I 1 o MBS i«un Odious

Al % 19.93 20 05 (1>

Ca 1930 1600 (1) Fe % 1 .66 1.53 (2) K % 1.28 1 29 ti)

LOI % 0.22

Li ua /a 510

Mg ua/a 3500 2800 ( 1

)

Mnni 1

1uy/y in /n

Na ua/a 1100

P ug/g 300

Si % 25.53 25.76 (1)

Sr ug/g 85 (1)

Ti % 1.32 1.34 (1)

V ug/g 120 Zr uo/a uy/ y 520

TABLE 77-1: COMPILED DATA FOR

ELEMENT UNITS NBS CONSENSUS

Wean M^an ri^cii 1 fn) \ 1 1 /

Al % 27.73 31.02 (2)

Ca ua/a 1860 1400 (1) Fe uq/a 6290 5450 (2)

K 1.75 1.79 (1)

LOI 0.21

Li ua/ay/ y 1630

Mq uq/q 3000 2200 ( 1

)

Mn uq/qy/ y 80 (1) Na 440

P ug/g 1960

Si % 15.12 15.32 (2)

Sr ug/g 1200 (1)

Ti % 1.76 1.82 (1)

V ug/g 180

Zr ua/a uy/ y 670

TABLE 78-1: COMPILED DATA FOR

ELEMENT UNITS NBS CONSENSUS

Mean Mean (n)

Al % 36.84 (1) Fe ug/g 5000 (1)

Li ug/g 930

Na ug/g 440

RANGE

1.47 - 1.59

XRF

Mean (n)

20.05 (1)

1600 (1)

1.59 (1)

1.29 (1)

OTHER METHODS

Mean (n) Method

1.47 (1) COlOft

2800

230

(1)

(1)

25.76 (1)

85 (1)

1.34 (1)

RANGt

30.63 - 31.4

5200 - 5700

XRF

Mean (n)

31.02 (2)

1400 (1)

5200 (1)

1.79 (1)

OTHER METHODS

Mean (n) Method

5700 (1) COLOR

2200

80

(1)

(1)

15.3 - 15.34 15.32 (2)

1200 (1)

1.82 (1)

RANGE XRF

Mean (n)

OTHER METHODS

Mean <n) Method

36.84 (1) TITR

5000 (1) COLOR

76-1
TABLE 76-2: INDIVIDUAL DATA FOR NBS SRH 76

(revised 3/1/86)

TABLE 77-2: INDIVIDUAL DATA FOR NBS SRM 77

(revised 3/1/86)

Cone

Al (%)

20.05

Ca (ug/g)

1600

Fe (%)

1.47

1.59

K (%)

1.29

Mg (ug/g)

2800

Hn (ug/g)

230

Si (%)

25.76

Sr (ug/g)

85

Ti (%)

1.34

Uncer Com Method Reference

0.01

UXRF

WXRF

COLOR

UXRF

UXRF

WXRF

UXRF

WXRF

UXRF

WXRF

67K0D 01

67K00 01

59C0L 01 67K00 01

67K0D 01

67K0D 01

67K0D 01

67K0D 01

67K0D 01

67K00 01

Cone

AL (%)

30.63

31.4

Ca (ug/g)

1400

Fe (ug/g)

5200

5700

Uncer Com Method Reference

100

1.79

Mg (ug/g)

2200

Mn (ug/g)

80

Si (%)

15.3

15.34

Sr (ug/g)

1200

Ti (%)

1.82

TABLE 78-2: INDIVIDUAL DATA FOR NBS SRM 78 (revised 3/1/86)

WXRF

XRF

WXRF

WXRF

COLOR

WXRF

UXRF

WXRF

XRF UXRF

UXRF

UXRF

67KO0 01 72ASH 01

67K0D 01

67K0D 01 59C0L 01

67K0D 01

67K0D 01

67K0D 01

72ASH 01 67K0D 01

67KO0 01

67K0D 01

Cone

AL (%)

36.84

Uncer Com Method Reference

TITR 58UAT 01

Fe (ug/g)

5000 100 COLOR 59COL 01

76-2
TABLE 76A-1: COMPILED DATA FOR NBS SRHs 76A-78A BURNT REFRACTORIES

(revised 3/1/86)

ELEMENT UNITS 76A 77A 78A

Al % 20.47 31.84 37.92

Ca ug/g 1570 360 790

Fe % 1.12 0.699 0.840

K % 1.10 0.075 1.01

LOI % 0.34 0.22 0.42

Li ug/g 200 120 560

Mg ug/g 3140 2290 4220

Na ug/g 520 275 580

P ug/g 520 400 5700

Si % 25.63 16.34 9.06

Sr ug/g 310 75 2120

Ti % 1.22 1.59 1.93

TABLE 79A-1: COMPILED DATA FOR NBS SRM 79A FLUORSPAR

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean t SD Mean

Ca

CaF2

F

Si

U

%

%

%

ug/g

ng/g

49.99 ± 0.03

97.39 ± 0.06

47.40 ± 0.03

3130

210 (1) NAA

TABLE 80-1: COMPILED DATA FOR NBS SRM 80 SODA-LIME GLASS

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean Mean

Al ug/g 1750

As ug/g 690

As(III) ug/g 230

As(V) ug/g 460

Ca % 3.32 3.2 (1) TITR

CI ug/g 470

Fe ug/g 450

K ug/g 330

LOI % 0.3

Mg % 1.95 1.93 (1) TITR

Mn ug/g 23

Na % 12.35

S ug/g 1640

Si % 34.6

Ti ug/g 120 Zr ug/g 22

76A-1
TABLE 79A-2: INDIVIDUAL DATA FOR NBS SRM 79A

(revised 3/1/86)

Cone Uncer Com Method Reference

U (nq/g)

210 30 DNA 86GAU 01

TABLE 80-2: INDIVIDUAL DATA FOR MBS SRM 80

(revised 3/1/86)

Cone Uneer Com Method Reference

Ca (%)

3.2 TITR 80HIT 02

Mq (%)

1.93 TITR 86hiT 02

76A-2
TABLE 88-1: COMPILED DATA FOR NBS SRM 88 DOLOMITIC LIMESTONE (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE OTHER METHODS

Mean Mean ± SD (n) Mean ± SD (n) method

Al ug/g 350

C-Inorg % 12.9 12.93 ± 0.06 (3) 12.90 12.90 - 13.00 12.93 ± 0.06 (3) COUL

C-Org ug/g 800

Ca % 21.8 21.81 (1) --- --- 21.81 (1) TITR

Co ug/g --- 0.7 (1) --- --- 0.7 (1) NAA

Cr ug/g --- 3.9 (1) --- --- 3.9 (1) NAA

Fe ug/g 590 580 (1) --- --- 580 (1) COLOR

H ug/g 80

K ug/g 250

LOI % 47.52

Mg % 12.95

Mn ug/g 50 — — — —

Na ug/g 590

p ug/g 13

S ug/g 130 287 ± 15 (3) 290 270 - 300 300 (1) TURB

S ug/g --- --- --- --- 280 (2) CB

Si ug/g 1450

Sr ug/g < 85 57.5 (2) --- 55 - 60 60 (1) NAA

Sr ug/g --- --- --- --- 55 (1) OES

Ti ug/g 30 182 (2) --- 24 - 340 24 (1) NAA

Ti ug/g --- --- --- --- 340 (1) COLOR

TABLE 88B-1: COMPILED DATA FOR NBS SRM 88B DOLOMITIC LIMESTONE

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

AL ug/g 1778 ± 69

C- Inorg % 12.66 ± 0.03

Ca % 21.53 ± 0.36

Fe ug/g 1937 ± 14

H20- % 0.24

K ug/g 855 ± 20

LOI % 46.98

Mg % 12.68 ± 0.04

Mn ug/g 124 ± 9

Na ug/g 215 ± 5

P ug/g 19 ± 1

Si ug/g 5282 ± 93

Sr ug/g 64 ± 3

Ti ug/g 96

88-1
TABLE 88-2: INDIVIDUAL DATA FOR NBS SRM 88 (revised 3/1/86)

Cone

C-Inorq (%)

12.9

12.9047

13.0003

Ca (%)

21.81

Co (ug/g)

0.7

Cr (ug/g)

3.9

Uncer Com Method Reference

0.42 41 0.0109 41 0.1556 41

0.03

0.6

COUL

COUL

COUL

TITR

RTNA

RTNA

86CAH 01 85ENG 01 85ENG 01

80HIT 02

61TUR 01

61TUR 01

Cone Uneer Com Method Reference

Fe (ug/g)

580

S (ug/g)

270

290

300

10 COLOR

CB

CB

TURB

59COL 01

55COL 01 77LAN 01 73SHA 01

Sr (ug/g)

55

60

OES

RTNA

58GRA 01 61TUR 01

Ti (ug/g)

24

340

RTNA

COLOR

65WAH 01 63K0R 01

88-2
"g

03O 3 cc

rg

ed

Uc

ocX

eo

c

3d an o <u >

t.

HI >^

3j

C

Q1—

c/>C

UJ (D z: z (U o

i—i_i GE o z Q <Of <CO

eozot

</> to z

CQ < Z o o: LU Ou.<1—<QUJ

—1 (/>

a

CI. V) (/> s: z o LU +1 u COz c o <D u (1) 2:

LE{

CO< </)

c

CDz (U M1—z

1-zlU£UI_l

o 00

tVJ

in• 00 1 1 o

O * 1 I 1 O fSI • • ^ 1 1 o O 1 i 1 1 o (NJ 1 1 tn fM 1 1 1 1 Oo

in ro fio in

»- 00 (M

VV TV

<0 ^0

0> CM ^ o

inoo in • eo

(M (M «- ^

in f\j o cvo

inooOCM

oo nO o

to

V

O00

vO

oo eo

to

00 in

oOo CO o ^ CVJ f\l (\j CM (M o

o rvj -J- to «- CJ to f\J to

o to in sO in (\l in

oo

o -Jo

o

o ro ro

o to

ro

tNJ

o (M

o (MofV

o

t^

CM

O<M

O

ino

ro «- to (M fNJ «- to «- to rj (M

ro

oin

toV

inV

00 in o (M

•H 00

V

CO

in in

oo r\i

o CM ro O O o o o 00 o o o CM

O

H t^ 00 +1o •H CO 00m

M to

V <f) vO CM in CM 00V

to to

oo CM

to CM

m

CM

o

CM

in

ooO vO

-J

OJ O) O) O) O) C7> u> O) o> o> c» cn tn tn

\\\

\

—\ •V.\\

\

\

\

\

\

\ o> CD cn O) cn o> O) cn cn cn tn 3 3 3 c 3 &S S< 3 3 3 3 3 3 c c c 3 3 3 c c c 3 3 3 c oc

tn

—' (0 < < < 3 (0 (L> < m CO

O

o

u (J

O I- 3 X (-) o o o M.

U

Z

o ^ -I

•'- 3

88A-1
"S

to SI 8 %

1 1» z c

I— <D O <U

CDU

<M

in

CO

UJo

UJo

u. C

QC (D »< <U

(/i U UJ

a. <a o o

o

COi

c u c 5z O

1

o

UJ CO

00 z«(

(A

C/) COz

Q z Ll_ <

< oUJ

UJ

_l

a. c u in

Z3

(/> (/> z 1 UJ -H < (/> ON an u UJ

—I

CQ<

m c

OQ <D Z

(/> 1—z

1—Z

UJzUJ

oin o o >—

• «— I rvi o00

o o o O >*O

o o 1 OJ «- 1 1 ro o00

<M V V to 1 1 V V (M

:8

oin ooro

o

o o o to in (NJ

rvj I— <

1^

oin oo

o

ro

oo

o00

o o o

ro in o

ro

<0 oCO

1 1 00 o

CM 1 C\J <>

f\J ^>

-o

in 1 o 00 1 (NJ 1

^

1 1 o 1 1

1 1 in 1 1

1 1 1

o ro

f\l o f\i

1

1

f\J -o

1 o

1 CO1

1 in

(NJ

or^

CNJ CM (\j ro «- to ro f\j roo 0> {M o ro ro ro ro ro in o o ro N- ro ro in in o o o o o o o o o ro o •O (\j 00 OJ fVJ -H o ro o o •H ro in o> tM o H

ro V V ro ro (\J (M ro in ro oin o

in

o

ro

(\j f\j Oo

>o

in

in

00 o

at O) O) cn at at at > O) D) > cn \ >^ — \ \ \ \ "V. \ D> O) O) O) o> at at at at at at at cn cn cn at D> at 3 3 3 3 3 3 c 3 3 3 c 3 3 c 3 3 c c c 3 c 3 3 c 3 3

c o z s: XI I- ^

a. a. a. oi {/)(/></)t/)(/)t/)t/)(— I— I— > >- >- rsi rsi

88A-2
TABLE 88A-2: INDIVIDUAL DATA FOR NBS SRM 88A (revised 3/1/86)

Cone

Ag (ug/g)

Uncer Com Method Reference

*s (uq/q)

Au (ug/g)

Ba (ug/g)

Be (ng/g?

180

Bi <ug/g?

12.75

12.83

Ca (%)

20.96

22.5

Cd <ug/g)

Ce (uq/g)

< 5 L ICPES 81CHU 01

< 3 L ICPES 81CHU 01

20 ICPES 81CHU 01

< 25 L ICPES 81CHU 01

0.02

0.69

CB

CB

ICPES

EXRF

ICPES

80ANO 01 78TER 01

81CHU 01 80DAL 01

81CHU 01

< 15 L ICPES 81CHU 01

2.A6 0.27 ICPES 85 JAR 02

2.7 ITNA 85P0T 02

A.

8

XRF 76LE0 02

< 3 L ICPES 81CHU 01 1 113 UXRF 82LE0 03

Al (Ufl/q) Co (u9/g)

300 EXRF 80DAL 01 1 0.5 ITNA 85POT 02

900 30 ICPES 81CHU 01 t 3 1 ICPES 81CHU 01 3.4 XRF 76LE0 02

13 0.26 ICPES 81CHU 01 1 14 ITNA 85POT 02 1 Dy (ng/g)

28 XRF 76LE0 02 1

Cone

ct (ug/g)

Uncer Com Method Reference

Cr (ug/g)

2.2

11.7

Cu (ug/g)

2.5

11.4

270

Er (nq/g)

180

Eu (ng/g)

10

10

F (ug/g)

500

Fe (ug/q)

Hf (ng/g)

180

ITNA ICPES

ICPES

XRF

ICPES

ICPES

WXRF

85POT 02

81CHU 01

81CHU 01 76LE0 02

85 JAR 02

85JAR 02

! 70 ITNA 85POT 02

C-Inorg (%) 1 70 10 ICPES 85 JAR 02

1 1200 600 ICPES 81CHU 01

82LE0 03

2030 ITNA 85P0T 02

2050 40 ICPES 81CHU 01 2200 EXRF 80DAL 01

Gd (ug/g)

0.32 0.02 ICPES 85JAR 02

3.4 0.35 ICPES 81CHU 01

ITNA 85POT 02

88A-3
TABLE 88A-2: INDIVIDUAL DATA FOR NBS SRM 88A (cont.)

Cone Uncer Com Method Reference

Hg (ng/g)

28.2 0.68 FAA 82FLA 01

Ho (ng/g?

60 10 ICPES 85JAR 02

tC (ug/g)

700 EXRF 80DAL 01 1000 25 ICPES 81CHU 01

< 5 L ICPES 81CHU 01 1.A4 0.16 ICPES 85 JAR 02

1.6 ITNA 85POT 02

2.2 XRF 76LE0 02

Li (ug/g)

< 2 L ICPES 81CHU 01

Lu <ng/g)

30 ITNA 85P0T 02

30 10 ICPES 85JAR 02

13 EXRF 80DAL 01 13.06 0.4 ICPES 81CHU 01

Mn (ug/g)

150 EXRF 80DAL 01 210 6.3 ICPES 81CHU 01

Mo (ug/g)

< 3 L ICPES 81CHU 01

Na (ug/g)

104 7 ICPES 81CHU 01 150 ITNA 85P0T 02

Nd (ug/g)

< 20 L ICPES 81CHU 01 1.26 0.11 ICPES 85JAR 02

1.4 ITNA 85P0T 02

Cone Uncer Com Method Reference

Hi <ug/g?

< 3 L ICPES 81CHU 01

P (ug/g)

70 4 ICPES 81CHU 01 220 EXRF 80DAL 01

Pb (ug/g)

3 XRF 76LE0 02

27 3 ICPES 81CHU 01

Pr (ng/g)

310 20 ICPES 85 JAR 02

("g/g>

2 ITNA 85P0T 02

S (ug/g?

4 CB 78TER 01

21 CB 77LAN 01 78 WXRF 82LE0 03

Sb (ug/g)

< 10 L ICPES 81CHU 01

Sc (ng/g)

300 ITNA 85P0T 02

Se (ug/g)

< 30 L ICPES 81CHU 01

Si (ug/g)

4100 EXRF 80DAL 01

Sm (ng/g)

280 10 ICPES 85 JAR 02

300 ITNA 85POT 02

Sn (ug/g?

< 3 L ICPES 81CHU 01 2.1 XRF 76LE0 02

88A-4
TABLE 88A- 2: INDIVIDUAL DATA FOR NBS SRH 88A (cont.

)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Sr (uq/g) U (nq/q)

41

4196

Ta <ng/g)

0.8

XRF

ICPES

OES

76LEO D2 1

fbTHp 01 1

< 300

V (UQ/q)

25000 L ICPES

ITNA

81CHU 01 85P0T 02

5ij I TNA O3P0T Ud 1

2.2

y

4

1

OES

ICPcS

84PLS 01 olCHU U1

Tb (nq/q) Y (uq/q)

50

Th (nq/q)

ITNA 85POT 02 1 2.16

2.3

0.06 ICPES

XRF

85JAR 02

76LE0 02

<

190

Ti (uq/q)

25000 L ICPES

ITNA

81CHU 01 1 85P0T 02 1

Yb (nq/q)

150

170

1200

10

40

ITNA

ICPES

85P0T 02

81CHU 01

66

180

2 ICPES EXRF

81CHU 01 1 80DAL 01 1Zn (uq/q)

2.8

4.1 1

XRF

ICPES

76LE0 02

81CHU 01

Zr (ug/g)

6.6

ICPES

XRF

81CHU 01 76LE0 02

88A-5
X v>

a: C

O 01

0£ W O

O O I— SOS MW Scrt o a. o o o — —i tj o I— u

/-\ *^

vO CJ «-

00

NO

o CO

• • • in lA in o o

O «VJ -4- in

(/></> CO O CD CD

CJ (_) CJ

S8 o

(M

rvj

5 COo CJ

rvi

c /-\ <»—

\

/-\ ^\

CM CM (V >^ \^ c

(0 I I 1 (\J >o « • 1 e O fVJ a 1 1 O o to N.

lU 1 1 1 o S- 1 ( ^— 1 1 T— 1 1 CO

I K) 9 1 s4- 1 1 1 t 'S^ D 1 1 1 XTk

^ c ?V c

(A <

< <U > z:

ICO

(0< c

V-/ C3 c

_i< O£

o

zor

COM C3

CQ z 2 <

OfOLk. <1—<

a 2

<

C3

LU oLU

a. z

o

/—V C

t

(/> Q UJ V> CO _I z CO 111 •H < CO 1— z c o

u

CO

in

00in

-J- in

f\l

COm

o

vO

oo

o

(\i ino

«M

S8

rvi S-

(M

rvj

0> (\l M (VJ N.

O fM

in •

1^ in

o

o

in

o

1 1 1 1 1 t ) o D I e 1 1 B 1

1 1 1 1 1 1 1 B t 1 t a 1 1 1 1

>^ ^—

in r\i ro I

ro o >o CM o O -*

rsj O f\j O o o CNJ On in N- in 1 1 f\J O • o fVi O H 1 1 M in M 00 +) in o PO i m •« (V J- o -J- CO O ^0 vO N.

in o ^ CM in in CM

CO CO o o I- f\j

fVJ o tv. ^ o

m

o in Oo o •J- N.

D) C3) o> Ut -V '

-•^ >^

O) cn O) C» u> O) 3 3 3 3 3 3 3 3 >« S« »S 3 3 3en en3 S< 3

C7> O) 3 3 S«

O) 0> O) O) G> CD O) 0> O) O) O) O) 3 3 C 3 3 3

PO in O OCM f\J m If) < < m

flj —

u u

3

(J

«> OJ (0

Li_ ?C Li_ CU ^ O Ol Q. (/> (/> C -

r) > N M

^91-1
TABLE 91-2: INDIVIDUAL DATA FOR NBS SRM 91 (revised 3/1/86}

Cone

MAM.

Uncer Com Method Reference

3.21 35 TCGS 78GLA 04 1 430 OES 64FIL 01 600 35 lENA 79GLA 03

(ug/g) 700 AA 84SCH 01 4000 35 TCGS 78GLA 04

302 OES 64FIL 01 1 5200 100 COLOR 59COL 01

Ba (ug/g)

79

Ca (%)

7.54

7.58

167

Co (ug/g)

4.5

Cr (ug/g)

26

26

cu <ug/g)

16

F (%)

25

35

OES

TCGS

AA

COLOR

OES

OES

72AVN 01

78GLA 04

84SCH 01

85UHI 01

72AVN 01

64FIL 01

OES 72AVN 01

Cone

Fe (ug/g>

Uneer Com Method Reference

12

K (%)

2.68

2.72

Mg (ug/g)

60

Mn (ug/g)

39

63

Na (%)

35

35

OES

TCGS

AA

TCGS

OES

OES

(ug/g)

0.79

6

35 lENA

OES

31.5

32.1

32.2

1.21

72AVN 01

78GLA 04

84SCH 01

78GLA 04

64FIL 01 72AVN 01

OES 72AVN 01 j 6.22 AA 84SCH 01 6.23 35 lENA 79GLA 03

6.32 35 TCGS 78GLA 04

79GLA 03

72AVN 01 4.9 0.1 IC 83KEN 04 1 5.1 IC 82UIL 02 1 0 (%)

5.16 35 lENA 79GLA 03 1 5.55 0.09 ISE 85UHI 01 1 49 0.6 14NAA 80NOR 01 5.6 0.16 11 ISE 77H0P 01 1 5.62 0.08 NAA 80NOR 01 1 Pb (ug/g)

5.68 0.15 ISE 77TR0 01 1 5.7 11 ISE 77H0P 01 1 17 OES 64FIL 01 5.7 0.07 CPAA 84HAN 01 1 1150 OES 72AVN 01 5.72 ISE 70ING 01 1 5.75 0.003 ISE 71PET 01 1 Si (%)

5.81 0.21 COLOR 83CHA 02 1

35

35

AA 82KIS 01! TCGS 78GLA 04

lENA 79GLA 03

91-2
TABLE 91-2: INDIVIDUAL DATA FOR NBS SRM 91 (cont.)

Cone

Sr (ug/g)

39

Ti (ug/g)

110

140

156

Uncer Com Method Reference

350 L35

OES

lENA

TCGS

OES

OES

72AVN 01

79GLA 03

78GLA OA

72AVN 01 64FIL 01

Cone Uncer Com Method Reference

U (ng/g)

540

710

V (ug/g)

43

Zn Cug/g)

700

Zr (ug/g)

60

DNA

DNA

OES

AA

66HAM 01 86GAU 01

72AVN 01

84SCH 01

47 OES 64FIL 01

91-3
TABLE 92-1: COMPILED DATA FOR NBS SRM 92 SODA-LIME GLASS

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

B ug/g 2180 ±90

Ca % 5.9 5.88 (1) MPOES

K ug/g 5000 4810 <1) MPOES

LOI % 0.42

Mg ug/g 600 — —

Na % 9.72 9.65 (1) MPOES

Si % 35

Zn ug/g 1600

TABLE 93-1: COMPILED DATA FOR NBS SRM 93 BOROSILICATE GLASS

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean Mean (n)

Fe ug/g --- 550 (1) COLOR

Si % --- 37.86 (1) AA

TABLE 93A-1: COMPILED DATA FOR NBS SRM 93A: Borosilicate Glass

(revised 3/1/86)

ELEMENT UNITS NBS

Mean

Al % 1.21

B % 3.9

Ca ug/g 70

CI ug/g 600

Fe ug/g 200

K ug/g 120

Mg ug/g 30

Na % 2.95

Si % 37.7

Ti ug/g 84

Zr ug/g 310

92-1
TABLE 92-2: INDIVIDUAL DATA FOR NBS SRH 92

(revised 3/1/86)

Cone Uncer Com Method Refereiice

Ca (%)

5.88

K (ug/g)

4810

Na (%)

9.65

MPOES 85ZHA 01

MPOES 85ZHA 01

MPOES 85ZHA 01

TABLE 93-2: INDIVIDUAL DATA FOR NBS SRM 93

(revised 3/1/86)

Cone Uncer Com Method Reference

550 10 COLOR 59C0L 01

Si (%)

37.86 0.84 AA 82KIS 01

92-2
TABLE 97-1: COMPILED DATA FOR NBS SRH 97 FLINT CLAY (revised 3/1/86)

ELE UNITS NBS

Mean

CONSENSUS

Mean ± SD (n)

MEDIAN RANGE NAA

Mean (n) Mean (n)

OTHER METHODS

Method Mean (n) Method

, ,

Al % 18.1 20.49 ± 0.02 (3) 20.5 9n ^1 C.\J.J 1 — 20.47 (1) LULUK (1) TITR

Al % — — — — — 5n ci (1) CHEM

B ug/g — 64 (2) — Of 71 7 — — it/ o (2) OES

Ba ug/g 130 170 ± 80 (3) 141 C.f\J 270 (1) 126 (2) ObS

Be ug/g — 1.3 (1) — — — 1 X 1.0 (1) OES

C ug/g — 3200 (1) — — — Tonn o^UU (1) CB

Ca ug/g 720 — — — —

Ce ug/g — 58.8 (2) — D f AnOU 7. I 57 (1) 60.7 (1) Utb

Co ug/g — 3.7 ± 0.6 (3) 3.46 L L 3.85 (2) 3.46 (1) uto

Cr ug/g 540 550 i 60 (6) 540 Ojt 578 (2) 486 (1) A70 DOT (1) AA

Cr ug/g --- — — — 500 (1) LULUK RAn (1) CHEM

Cs ug/g — 2.4 (1) — 2.4 (1) —

Cu ug/g 24 18 ± 5 (4) 18.5 1

1 1 C.C — 14.8 <2) 5n (1) CHEM

Cu ug/g — — — — — 55 (1) COLOR

Dy ug/g — 4.28 (1) — — — H . Co (1) OES

Eu ug/g — 1.4 (2) — 1 1 .30 1.24 (1) 1.56 (1) Fe ug/g 6850 6660 ± 130 (5) 6600 ojuu AQnn OoUU 6600 (1) 6800 (1) T 1 TD 1 L 1 K 055U (2) COLOR

Fe ug/g — — — — 6800 (1) Lntn

Ga ug/g — 45.1 (1) — — — AC 1 (1) OES

Hf ug/g — 39.5 (1) — 39.5 (1) —

Hg ng/g — 110 <2) — bo i CO 5 — 110 <2) A A AA

K ug/g 4500 — - — — —

LOI % 13.35 — — — —

La ug/g — 34 (1) — 34 (1) —

Li ug/g 1070 1074 (1) — — — 1 n7/ lUf H (1) OES

Lu ug/g — 0.96 (1) — 0.96 (1) —

Mg % 0.157 0.145 (2) — n IT n 1

— 0.16 (1) Lntn n 17 U. 10 (1) COLOR

Mn ug/g 15 50 ± 44 (3) 35 11 o OO 7 — 67 <2) 1A (1) CHEM

Mo ug/g 1.3 2.0 (1) — — — 5 n (1) CHEM

Na ug/g 520 — — — —

Nb ug/g — 35.6 (1) — — — V% A (1) OES

Nd ug/g — 19 (1) — — 19 (1) uto

Ni ug/g — 34.4 (2) — XAOO . Ro — 34.4 (2) uto

P ug/g 350 — — — —

Pb ug/g — 34.6 (2) — XL X — 34.3 (1) ncc Uto 03 (1) AA

Rb ug/g — 24 (1) — 24 (1) —

S ug/g 170 176 ± 22 (3) 170 1 JO — 200 (1) TI IDD 1 UKb 1 AA (2) CB

Sb ug/g — 1.4 (1) — 1.4 (1) —

Sc ug/g — 16.4 (2) — 17 1 1 c. . 1 5n 7 20.7 (1) 12.1 (1) ncc uco

Si % 20.02 20.0 (1) — — 20 (1) T t TD

Sm ug/g — 5.8 (1) — 5.8 (1) —

Sn ug/g — 8.6 (2) — f in 1 — 8.55 (2) ncc uto

Sr lig/g — 73 ± 38 (3) 88 xn ini 30 (1) 94.5 (2) ncc uto

Ta ug/g — 4.2 (1) — 4.2 (1) —

Tb ug/g — 1.27 (1) — 1.27 (1) —

Th ug/g — 37 (1) — 37 (1) —

Ti % 1.42 1.39 ± 0.08 (3) 1.43 1 X 1 LX — 1.3 (1) mlLULUKno 1 A7 (1) CHEM

Ti % — — — — 1.43 (1) T 1 TD

V ug/g 225 240 ± 90 (4) 205 148 362 — 255 (2) Oca (1) COLOR

V ug/g — — — — 234 (1) CHEM

Y ug/g — 35.3 (2) — 33 37.6 — 35.3 (2) OES

Yb ug/g 7.1 (2) 6.8 7.47 6.8 (1) 7.47 (1) OES

Zn ug/g 92 (2) 81 103 103 (1) 81 (1) XRF

Zr ug/g 1850 1390 (1) 1390 (1)

(ij

97-1
TABLE 97-2: INDIVIDUAL DATA FOR NBS SRM 97 (revised 3/1/86)

Cone

Al (%)

Uncer Com Method Reference

20.47 COLOR 57SHI 01 1 11 OES 64FIL 01 20.5 0.03 TITR 84DAS 01 1 18.5 OES 77FLA 01 20.51 CHEN 57SHI 01 1 20 CHEM 57SHI 01

B (ug/g)

57

71,3

Ba (ug/q)

1.3

c (ug/g)

3200

Ce (ug/g)

57

60.7

Co (ug/g)

Cr (ug/g)

29

OES

OES

6^FIL 01 77FLA 01

110 OES 77FLA 01 t 1.24 0.03 ITNA 77FLA 01 141 OES 58GRA 01 1 1.56 OES 77FLA 01 270 21 ITNA 77FLA 01

OES

CB

ITNA OES

77FLA 01

78TER 01

77FLA 01 77FLA 01

486 OES 77FLA 01 500 COLOR 57SHI 01 540 CHEM 57SHI 01 576 14.4 ITNA 77FLA 01 581 RTNA 61TUR 01 639 AA 80DON 01

Cs (ug/g)

2.4 0.08 ITNA 77FLA 01

Cone

Cu (ug/g)

Uncer Com Method Reference

22

Dv (ug/^)

4.28

Eu (ug/g)

(ug/g)

6500

6600

6600

6800

6800

Ga tug/g)

45.1

Hf !;ug/g?

39.5

100

100

600

1.19

159.2

La (ug/g)

34

Li (ug/g)

1074

Lu <ug/g?

0.96

COLOR

OES

COLOR

COLOR

ITNA CHEM

TITR

OES

ITNA

6.22

14.7 L 0.71

0.02

FAA

OES

ITNA

OES

ITNA

57SHI 01

77FLA 01

59COL 01 57SHI 01 77FLA 01 57SHI 01 84DAS 01

77FLA 01

77FLA 01

3.3 0.06 ITNA 77FLA 01 1 Hg (ng/g)

3.46 OES 77FLA 01 i 4.4 RTNA 61TUR 01 1 68 FAA 75HEI 01 82FLA 01

77FLA 01 77FLA 01

77FLA 01

77FLA 01

97-2
TABLE 97-2: INDIVIDUAL DATA FOR NBS SRM 97 (cont.)

Cone

0.13

0.16

Mn (ug/g)

Uncer Com Method Reference

Mo (ug/g)

Nb (ug/g)

Nd (ug/g)

19

Ni (ug/g?

32

36.8

Pb (ug/g)

34.

35

Rb (ug/g)

S (ug/g)

Sb (ug/g)

1.4.

Sc (ug/g)

12.1

20.7

0,11

COLOR

CHEM

57SHI 01 57SHI 01

16 CHEM 57SHI 01 35 OES 64FIL 01 99.7 OES 77FLA 01

CHEM 57SHI 01

30 RTNA 61TUR 01 35.6 OES 77FLA 01 1 88 OES 58GRA 01

101 OES 77FLA 01

ITNA

OES

OES

77FLA 01

64FIL 01 77FLA 01

OES 77FLA 01 FAA 79HEI 03

ITNA

0.17

OES

ITNA

77FLA 01

77FLA 01 77FLA 01

Cone

Si (%)

20

Sm (ug/g)

5.8

Sn (ug/g)

7

10.1

Sr (ug/g)

Uneer Com Method Reference

4.64 L 0.08

Ta (ug/g)

4.2

Tb (ug/g)

1.27

Th (ug/g)

37

Ti (%)

0,09

0.02

0.48

V (ug/g)

234

362

Y (ug/g?

33

37.6

TITR

OES

ITNA

OES

OES

ITNA

ITNA

ITNA

CHEM

OES

OES

OES

770HL 01

77FLA 01 77FLA 01

64FIL 01 77FLA 01

77FLA 01

77FLA 01

77FLA 01

1.3 COLOR 57SHI 01 24 1.6 ITNA 77FLA 01 1 1.43 CHEM 57SHI 01 1.43 0.03 TITR 84DAS 01

158 CB 78TER 01 1 170 CB 55COL 01 1 148 OES 64FIL 01 200 TURB 73SHA 01 1 205 COLOR 57SHI 01 57SHI 01 77FLA 01

64FIL 01 77FLA 01

97-3
TABLE 97-2: INDIVIDUAL DATA FOR NBS SRM 97 (cont.)

Cone Uncer Com Method Reference

Yb (ug/g)

6.8 0.17 ITNA 77FLA 01 7.47 OES 77FLA 01

Cug/g)

81 XRF 65BAL 01 103 3.15 ITNA 77FLA 01

1390 34.8 ITNA 77FLA 01

97-4
TABLE 97A-1: COMPILED DATA FOR NBS SRM 97A FLINT CLAY (revised 3/1/86)

ELE UNITS NBS CONSENSUS RANGE NAA OTHER METHODS

Mean Mean ± SD (n) Mean (n) Mean <n> Method Mean (n) Method

Al % 20.52 20.84 (1) ... 20.84 (1) ... ...

As ug/g --- 3.53 (1) — ... 3.53 (1) AA —

B ug/g ... 69.4 (1) — — 69.4 (1) OES —

Ba ug/g 670 660 (1) — 660 (1) — —

Be ug/g ... 3.4 (2) 3.2 - 3.55 — 3.55 (1) OES 3.2 (1) AA

Bi ng/g ... 733 (1) ... — — 733 (1) AA

C ug/g ... 600 (1) ... — — 600 (1) CB

Ca ug/g 790 — — — —

Cd ng/g ... 16 (1) — — — 16 (1) AA

Ce ug/g ... 160 (2) 124 - 203 203 (1) 124 (1) OES —

Co ug/g ... 4.4 (2) 4.1 - 4.64 4.1 (1) 4.64 (1) OES ...

Cr ug/g 200 190 (2) 180 - 203 180 (1) 203 (1) OES ...

Cs ug/g ... 1.6 (1) ... 1.6 (1) ... ...

Cu ug/g ... 24.9 (1) ... ... 24.9 (1) OES ...

Dy ug/g ... 8.89 (1) ... ... 8.89 (1) OES ...

Eu ug/g ... 3.74 (2) 3,66 - 3.81 3.81 (1) 3.66 (1) OES —

Fe ug/g 3140 3000 (1) ... 3000 (1) ... —

Ga ug/g ... 31.6 (1) ... ... 31.6 (1) OES ...

Hf ug/g — 13.4 (2) 11.3 - 15.4 13.35 (2) — —

Hg ng/g — 388 (1) ... — — 388 (1) AA

K ug/g 4150 ... — — — —

LOI % 13.32 ~ ~ ~ — — — —

La ug/g ... 73 (2) 43.7 - 103 103 (1) 43.7 (1) OES —

Li ug/g 510 439 (1) ... ... 439 (1) OES —

Lu ug/g ... 0.98 (1) — 0.98 (1) — —

Mg ug/g 900 ... ... — —

Mn ug/g ... 5.24 (1) ... ... 5.24 (1) OES —

Na ug/g 275 ... ... — —

Nb ug/g ... 39 (1) ... ... 39 (1) OES —

Nd ug/g ... 88 (1) ... 88 (1) — ---

Ni ug/g ... 81 (1) ... ... 81 (1) OES —

P ug/g 1570 845 ? (2) 160 - 1530 ... 160 (1) ICPES 1530 (1) COLOR

Pb ug/g — 40.15 (2) 38.6 - 41.7 ... 41.7 (1) OES 38.6 (1) AA

Rb ug/g — < 20 ... < 20 — —

S ug/g — 308 (1) — ... — 308 (1) CB

Sb ng/g ... 800 (2) 800 - 800 800 ( 1

)

... 800 (1) AA

Sc ug/g ... 26 (2) 21.3 - 31.3 31.3 (1) 21.3 (1) OES —

Si % 20.39 20.7 (1) ... 20.7 (1) ... ...

Sm ug/g ... 14 (2) 6.88 - 21.3 21,3 (1) 6.88 (1) OES ...

Sn ug/g ... 6.5 ± 0.4 (3) 6.16 - 6.9 ... 6.53 (1) OES 6.53 (2) AA

Sr ug/g 1500 860 (1) \ ... 860 (1) OES ...

Ta ug/g ... 3.21 (1)

\ 3.21 (1) ... ...

Tb ug/g ... 2.77 (1) ... 2.77 (1) ... —

Th ug/g ... 31.1 (1) ... 31.1 (1) ... —

Ti % 1.14 ... ... ... ...

U ug/g 6.58 (1) 6.58 (1)

V ug/g 362 (1) 362 (1) OES

Y ug/g 121 (1) 121 (1) OES

Yb ug/g 8.9 (2) 7.7 - 10.1 7.7 (1) 10.1 (1) OES

Zn ug/g < 20 < 20

Zr ug/g 470 522 (2) 465 - 580 522 (2)

97A-1
TABLE 97A-2: INDIVIDUAL DATA FOR NBS SRM 97A (revised 3/1/86)

Cone

AL (%)

20.84

As Cug/g)

3.53

69.4

Ba (uq/q)

Uncer Com Method Reference

Bi (nq/g)

733

733

c (uq/q)

600

Cd (ng/q)

16

Ce tuq/q)

124

203

Co (uq/q)

4.1

4.64

Cr (uq/g)

180

203

lENA

HAA

OES

84CEL 01

84TER 04

77FLA 01

660 20.6 ITNA 77FLA 01 1 3.66

3.81

OES

0.02 ITNA

77FLA

77FLA

01

01 Be (ug/g)

Fe <ug/3)

3.2 AA 82TER 02 1 3.2 D AA 83TER 01 1 3000 30 ITNA 77FLA 01 3.55 OES 77FLA 01 1

200

3.51

0.08

4.1

FAA HAA

CB

ICPES

AA

OES

ITNA

ITNA OES

ITNA OES

84TER 03

84TER 02

78TER 01

83UCH 02

84TER 01

77FLA 01 77FLA 01

77FLA 01 77FLA 01

77FLA 01 77FLA 01

Cone

Cs (ug/g)

1.6

CU (uq/q)

24.9

Dv (uq/g)

8.89

Eu (ug/g)

Uneer Com Method Reference

0.6

Ga (ug/g)

31.6

Hf (ug/g)

11.3

15.4

Hq (ng/g)

387.5

La (ug/g)

43.7

103

Li (ug/g)

439

Lu (ug/g)

0.98

Mn (ug/g)

5.24

0.39

22.5

1.83

0.04

ITNA

OES

OES

OES

ITNA RTNA

FAA

OES

ITNA

OES

ITNA

OES

77FLA 01

77FLA 01

77FLA 01

77FLA 01

77FLA 01 76GAN 01

82FLA 01

77FLA 01 77FLA 01

77FLA 01

77FLA 01

77FLA 01

97A-2
TABLE 97A-2: INDIVIDUAL DATA FOR NBS SRM 97A (cont.)

Cone

Nb (uq/g)

39

Nd (ug/g)

88

Ni" (ug/g)

81

Uncer Com Method Reference

0.016

0.153

Pb (ug/g)

38.6

41.7

Rb (ug/g)

S (ufl/ g?

308

Sb (ng/g)

800

800

Sc (ug/g)

21.3

31.3

Si (%)

20.7

Sm (ug/g)

6.88

21.3

3.7

0.0001

0.001

100

0.75

OES

OES

ICPES

COLOR

AA

OES

CB

HAA

ITNA

OES

ITNA

77FLA 01

ITNA 77FLA 01

77FLA 01

83UCH 01 83UCH 01

84TER 01 77FLA 01

20 L ITNA 77FLA 01

78TER 01

8ATER 04

77FLA 01

77FLA 01 77FLA 01

lENA 84CEL 01

0.69

OES

ITNA

77FLA 01 77FLA 01

Cone

Sn (ug/g?

6.16

6.53

6.9

Sr (ug/g)

860

Ta (ug/g)

3.21

Tb (ug/g)

2.77

Th (ug/g)

31.1

u (ug/g)

6.58

V (ug/g)

362

Y (ug/g)

121

Yb (ug/g)

7.7

10.1

Zn (ug/g)

Uneer Com Method Referenee

Zr (ug/g)

465

580

0.28

0.06

0.08

0.37

0.23

19

21

AA

OES

FAA

OES

OES

OES

ITNA OES

82TER 01 77FLA 01 85TER 01

77FLA 01

ITNA 77FLA 01

ITNA 77FLA 01

ITNA 77FLA 01

RTNA 76GAN 01

77FLA 01

77FLA 01

77FLA 01 77FLA 01

< 20 L ITNA 77FLA 01

RTNA 76GAN 01 ITNA 77FLA 01

97A-3
CO "8 8 £ 3: <u

lU

t—o

c

c

a>

ono

= o

oinin 00 M M

CJ I—

000

o >o in

a:o

O 3: 5

O K>

>dO Z _J LU O oc O O

O (M

o

O ac

CM <M O 00

5

-J0(/) CO CO v. UJ H 0 c

ro (aa> m

x:

(0 '>

a> c

L. \^ < c

>• z (0

u• I—<_l

0. UJ 00 z 0 <a: za:

</) COm

z

C>£ z

0 < u_< UJ <0

0tu

_l c

Q.

CO 0 CO Q z CO

UJ

«

CO •H

1 z

CO 0 C

(D0

UJ £ _l

GD<1—

C

CO (D CQ <U z Z

in

/—

\

^\ <^

<M ro ro f\J f\j >^0 0 CO ro

in 1 1 1 0 0 1 t 1 ro -J- 1 "H CO • "M +1 1 1 1 +1 • in 1 1 1 0 1 vO in 1 1 1 CM 1 1 1 «

1 0 10 in 0

ro

NO

/—

s

CJ

(M

1 0 1 1 in (\J 1 1 • 1 1 1 ' 2^

1 0 1 1 1 in f\J I 1 0 1 1 • 1 1 S- 1 in

1 1 1 1 1 1 1

sO 0 r^ to 0 0 in 0 0 0 0 in 0 «0 ro 1^ 0 0 in

f (VJ1 001 1 r—

1 1 1 00

1 1 1 1

1 t

1 00

1 1

1 00

1 1

1 0

t 1

1

1 01 CO1 1

i ro

1 1 1

1 1 1 CM

1 1 1

1 1

1 1 1

1 1 CM 0 1^in in ro in

ro CM m

in

to

in

• o CO o

in oCO

fO

t^o

o

•H roin

ro ro CM in CO CM CM ro

ro

in sr 0 0 00 0 00 >0 CM t^ 0 0 in 0 1 1 0 CM ro I 1 <t 0 H H 0 H CM H -H I 1 0 H • H in r^ 1 1 -H in 0 1 1 0 0 0 00 00 CM in

00 ro ro :S ro Oin in

o

in o CM

r^

to to CO

1 1 1 t CM 0 1 1 1 1 ^ 1 1 1 I CM

1- O) 0) C3) 0 cn o> O) O) o> cn cn \ — \ \ z O) cn O) at o> cn cn cn

ID >« »5 S< 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 >e s< 3 3 c »« »S 3

0 0) o>

< < <

flj 00 V o O CJ 000 «- (0 3 OJ 01 (D

li. u. C3 O <D - 3 V —I —I —I —I

98-1
M

0)

c

to

LU

(M «- o o o o

ro «-

a:O

O a: =

u o u

o o

O

Oo

o

cao

o

EO

Of

Oo

o

U. O I-

<o o o • in

• • «- (M

CM

o z X o

O z X O u u u u

«- rvi cj

o o o »- o >o K! !Q *" *" <h COoo

o c

(D c <1) o Z u

>-< c

_lu

C

u z <D

<U t- X

<

a.eoo

z: LU

Of u

M z

W

COz

Ou.<1— z

< <

oLU

LU X

PIL

COM

v>

1 Z3 eo </) o Z </>

LU LUCO +1 _l z CO o c < u 03 1— OX

o

<M

Oo

o

o

o

o

o

o

o

eo

eo

in

eo

o.

in

CO in o (Mm M >«•

c> o o ro in

o

oo

Oin

(M

O

(M

ro

^\ m rj w w

O oo <^

•H +1 O O 00

K»

PJ (M

(M in in

in (M K) • o • • «M <M <r- «-

ro o o ro ro

1 1 >*1 1 in o in o «M (M

o

(M oo o

2

^

o

eo o>

rj •

o eo

o

eofM

in o

«- ro

ro

s

o

to

ro

ro (\i (M «- ro W W

00 o

ro m

in

tM ro o

(M

ro\^ ro ro\^

o

>» o d

H •H +< m(M o<M

27.60

00

in >0 eo ro ro >^ r Si* o o o <M in in >o eo o> >o (M ro in

•« • • •H +< -H fM -ft fM o o o eo o eo ro (M ro

o>

c

(/> ni CO V o

ro

0> I o ro I ro oin

ro oeofM

^0

(M in

eo

oo

ro

(7> o> o> D> o> o> o> O) O) o> O) V. ««» *>. «^ •v

CD o> o> o> O) o> Ol o> 01) o> 3 D 3 3 3 3 3 3 3 3 3 3 3 3 »c a< 3 3 3 3 3 3 3 ? 5 5 3

> O) o> c X X X X(0 "D —

a. a. ot ^ u 0) •- - E c I. </>(/)(/>(/>(A(/>MM(/>M 18 ^ £ •— —

r- t- »- 1- I- > > >- >- C U

98-2
TABLE 98-2: INDIVIDUAL DATA FOR MBS SRM 98 (revised 3/1/86)

Cone Uncer Com Method Reference

At (%)

13.48 TITR 58WAT 01 13.5 CHEH 62J0E 01 13.5 OES 62J0E 01 13.51 CHEH 57SHI 01 13.65 COLOR 57SHI 01

B (ug/g)

68 OES 64FIL 01 78.5 OES 77FLA 01 150 3 OES 63CLA 01 250 3 OES 63CLA 01

Ba (ug/g)

570 OES 58GRA 01 670 10.8 ITNA 77FLA 01 800 OES 63CLA 01

Be (ug/g)

4.1 OES 77FLA 01

c (ug/g)

4000 CB 78TER Ql

1500 OES 62JOE 01 1500 CHEM 62J0E 01 1600 TITR 80HIT 02

Ce (ug/g)

119 OES 77FLA 01 135 1.32 ITMA 77FLA 01

Co (ug/g)

13.8 0.1 ITNA 77FLA 01 15 OES 63CLA 01 16.5 RTNA 61TUR 01 16.9 OES 77FLA 01 17 OES 64FIL 01

Cone Uncer Com Method Reference

Cr (ug/g)

113 2.33 ITNA 77FLA 01 119 OES 64FIL 01 130 RTNA 61TUR 01 136 OES 77FLA 01 143 AA 80DON 01 144 CHEM 57SHI 01 150 3 OES 63CLA 01 170 COLOR 57SHI 01 250 3 OES 63CLA 01 1400 CHEH 62J0E 01 1600 OES 62J0E 01

Cs (ug/g)

10.7 0.17 ITNA 77FLA 01

Cu (ufl/fl)

33,7 OES 77FLA 01 39 OES 64FIL 01 70 3 OES 63CLA 01 70 COLOR 57SHI 01 72 CHEM 57SHI 01 100 3 OES 63CLA 01

Pv (ug/g)

7.07 OES 77FLA 01

Eu (ug/g)

1.74 0.02 ITNA 77FLA 01 2.07 OES 77FLA 01

Fe (%)

1.12 CHEH 62J0E 01 1.17 OES 62J0E 01 1.38 0.01 COLOR 59COL 01 1.4 COLOR 57SHI 01 1.4 0.05 ITNA 77FLA 01 1.43 CHEH 57SHI 01

Ga (ug/g)

< 100 L OES 63CLA 01 24.1 OES 77FLA 01

80 3 OES 63CLA 01

98-3
TABLE 98-2: INDIVIDUAL DATA FOR NBS SRM 98 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Hf (uq/q)

1

P (ug/g)

7 0.42 ITNA 77FLA 01 1 350 COLOR 76WH I 0

1 111 \j I 390 11 COLOR 76WHI 01 Hg (ng/g)

Pb (uq/q)

462.6 12.1 FAA 82FLA 01 1

1 40 OES 63CLA 01

1 47.5 OES 77FLA 01

55.2 OES 77FLA 01 1 Rb (uq/g)

79 1.7 ITNA 77FLA 01 1 150 OES 63CLA 01 1 154 1.12 ITNA 77FLA 01

]

144 OES 77FLA

1 01 1 250 CB 78TER 01

1 270 CB 55COL 01 Lu (nq/q) 1 300 TURB 73SHA 01

650 ITNA 77FLA 01 1 Sb (uq/q)

1 1 .3 0.12 ITNA 77FLA 01

4100 TITR 80HIT

1 02 1 Sc (ua/a)

4200 OES 62JOE 01 1 4300 CHEM 62J0E 01 1 22.1 OES 77FLA 01 4300 CHEM 57SHI 01 1 22.9 0.06 ' ITNA 77FLA 01 4600 COLOR 57SHI 01 1 30 OES 63CLA 01

Mn (uq/q)

1

1 Se (uq/q)

39 OES 64FIL

1 01 1 1.04 0.08 FLUOR 74CRE 01 39 CHEM 57SHI 01 1 1.2 UU 74WAH 01 40 CHEM 62J0E 01 1 1.37 UU 65UEL 01 96.5 OES 77FLA 01 1 100 3 OF 9 63CLA 01 1 Si (%)

100 3 OES 63CLA 01 i

1 27.59 TITR 770HL 01 Mo (ug/g) 1 27.6 CHEM 62J0E 01

1 27.6 OES 62JOE 01

< 1 L OES 63CLA 01 1

1 CHEM 57SHI 01 1 Sm (ug/g)

Nd (uq/g)

1 6.3 OES 77FLA 01 10.3 0.42 ITNA 77FLA 01 49 0.58 ITNA 77FLA 01 1 Sn (uq/g)

Ni (ug/g)

6.47 OES 77FLA 01 39 OES 64FIL 01 1 40 OES 63CLA 01 1 52.8 OES 77FLA 01 1

98-4
TABLE 98-2: INDIVIDUAL DATA FOR NBS SRH 98 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Sr (ufl/g)

1

1 V (uq/q)

205 RTNA 61TUR

1 01 j 106 OES 64FIL 01 230 OES 58GRA 01 1 120 OES 62JOE 01 300 OES 63CLA 01 1 140 CHEM 62J0E 01 326 OES 77FLA 01 1 140 CHEM 57SHI 01 390 OES 75TH0 01 1 161 COLOR 57SHI 01

1 200 3 OES 63CLA 01 Ta (ufl/3) 1 300 3 OES 63CLA 01

1 310 OES 77FLA 01 2.22 0.03 ITNA 77FLA 01 1

1 Y (uq/q)

Tb (Uq/q) 1

1 28 OES 64FIL 01 1.35 0.02 ITNA 77FLA 01 1 40 OES 63CLA 01

1 46.7 OES 77FLA 01 Th (uq/Q) 1 Yb (uq/q)

19.5 0.21 ITNA 77FLA 01 1 4.9 0.1 ITNA 77FLA 01

Ti (ug/g) 1 6.8 OES 77FLA 01

1 21.2 OES 77FLA 01 8400 CHEM 62J0E 01 1 sm CHEH 57SHI 01 1 Zn (uq/g)

8690 OES 62J0E 01 1 9000 3 OES 63CLA 01 1 125 2.1 ITNA 77FLA 01 9300 COLOR 57SHI 01 1 10000 3 OES 63CLA 01 j Zr (ug/g>

190 OES 64FIL 01 270 OES 62JOE 01 300 OES 63CLA 01

300 CHEM 62J0E 01 340 19.6 ITNA 77FLA 01 377 OES 77FLA 01

98-5
TABLE 98A-1: COMPILED DATA FOR NBS SRH 98A PLASTIC CLAY (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS RANGE NAA OES OTHER METHODS

Mean Mean ± SO (n) Mean (n) Mean (n) Mean (n) Method

Al % 17.56 V.42 y 4 \ (1) 17.42 ^ 4 \ (1)

As ug/g 11 .4 r 4 \ (1) 4 4 / 1 1 .4 (1) AA

B ug/g 120 / 4 % (1) 120 (1) Ba ug/g 270 520 (2) 168 - / on 480 h80 / i \ (1) i Z.Q loo ^ 4 \ (1

Be ug/g 5.4 (2) 4.0 3.y3 D.y3 /IX (14,o ^ 4 \ (1) AA

Bi ng/g f yo / i \ (1) / 4 \ (1) AA

C ug/g 8100 X 4 \ (1

O 4 AA 8100 (1) CB

Ca ug/g 2200

Cd ng/g 47 (1) 47 (1) AA

Ce ug/g 200 (2) 180 - 2iy 219 / i \ (1) 4 OA loO / 4 \ (1)

Co ug/g 13 (2) 11.5 - i4.4 11.5 / i \ 14,

(1)

Cr ug/g 200 223 (2) 212 - 234 11 o 212 (1) 234 / 4 \ (1)

Cs ug/g 6.2 (1) 6.2 (1)

Cu ug/g 121 ^ 4 \ (1> 4 14 121 r 4 ^ (1)

Dy ug/g 4 ^ C 17.5 y 4 <k (1) 17.5 y 4 \ (1)

Eu ug/g 3.35 /Ox (2) 3.18 T CO 3.52 3.18 (1

T CO 3.52 /fx (1) Fe ug/g BoUU (1) oonn 8800 /IX (1

Ga ug/g 23.3 (1) 07 T 23.3 / 1 X (1

H r ug/g r .3 (1> ( .5 / 1 \ (1

Hg ng/g 3y .3 (1) TO T 3y .3 /IX (1AA

K ug/g oo5V

vA1 "5 /. /-

La ug/g 1 y 1 . f 1 A5 (1

01 7 y 1 . f / 1 ^

V 1

Li ug/g 5dD 2V1 / 1 \ (1 ) 001 2yi /IX (1)

LU ug/g 1.13 / 1 \ (1 ) 1.13 (1)

Mg ug/g OC Art

Mn ug/g Hi .H / i \ (1 ) Hi .H /IX (1

Na ug/g

ND ug/g 10 O jy.y / 1 \ TO O jy .y /IX (1

Nd ug/g / 1 \ (1 ) 98 /IX (1)

Nl ug/g 110£ 11 J n

r ug/

g

/ tin

pd ug/g oo (2; 00.8 - AO o oy .£ /IX (1

}

OO.O / 1 X

( 1

A A

Kb ug/g 33 (133 /IX (1

S ug/g 1300 y 4 \ (1

1 Tnn /IX (1

LD Sb ug/g 2.4 (2) 2.3 - 2.57 O T 2.3 ^ 4 V (1) O C7 2.5/ / i X (1

A A AA

Sc ug/g 32 (2) 2o-o - 34.8 t/ o 3h.8 / 1 \ (1) Ofl 0 28.8 /IX (1

Si A 22-2 / 4 \ (1) oo o 22.2 / i X (1

Sm ug/g 4 O12 (2) n 4 o 9.18 - 15 15 / 4 \ (1) y. IB /IX (1

Sn ug/g 5.3 ± 0.4 (3) 1 CO 5. 76 H.88 / 1 X CD c cn /Ox (2) A A AA

Sr ug/g 330 438 (1) /TO 438 / i X (1) Ta ug/g 2.46 (1) 2.46 (1)

Tb ug/g 2.92 (1) 2.92 (1)

Th ug/g 23.9 (1) 23.9 (1)

Ti % 0.964

Tl ng/g 351 (1) 351 <1) ASV V ug/g 554 (1) 554 (1) Y ug/g 176 (1) 176 (1)

Yb ug/g 9.8 (2) 9.3 - 10.3 9.3 (1) 10.3 (1) Zn ug/g < 23 < 23

Zr ug/g 740 (1) 740 (1)

98A-1
Cone

TABLE 98A-2: INDIVIDUAL DATA FOR NBS SRM 98A (revised 3/1/86)

Uncer Com Method Reference I Cone Uncer Com Method Reference

Al (%) I Cs (ug/g)

17.42 2.5 lENA 84CEL 01 | 6.2 0.06 ITNA 77FLA 01

As <ug/3) I Cu (ug/g)

11.4 HAA 84TER 04 | 121 OES 77FLA 01

120 OES 77FLA 01 | 17.5 OES 77FLA 01

Ba (ug/g? I Eu (ug/g)

168 OES 77FLA 01 | 3.18 0.02 ITNA 77FLA 01 480 20 ITNA 77FLA 01 | 3.52 OES 77FLA 01

Be (ug/g? | Fe (ug/g)

4.8 D AA 83TER 01 j 8800 30 ITNA 77FLA 01 4.8 AA 82TER 02 | 5.93 OES 77FLA 01 | 6a (ug/g)

Bi (ng/g) | 23.3 OES 77FLA 01

790 D FAA 84TER 03 | Hf (ug/g)

790 HAA 84TER 02 |

I 7.3 0.14 ITNA 77FLA 01

C (ug/g) I

I Hg (ng/g)

8100 CB 78TER 01 |

I 39.3 4.8 FAA 82FLA 01 cd (ng/a?

1

I La (ug/g)

47 AA 84TER 01 |

I 91.7 OES 77FLA 01 Ce (ug/g) | 162 2.99 ITNA 77FLA 01

180 OES 77FLA 01 | Li (ug/g)

219 0.29 ITNA 77FLA 01 |

I 291 OES 77FLA 01 Co (ug/g)

I

I Lu (ug/g)

11.5 0.06 ITNA 77FLA 01 | 14.4 OES 77FLA 01 | 1.15 0.06 ITNA 77FLA 01

Cr (ug/g) | Mn (ug/g)

212 4.8 ITNA 77FLA 01 | 41.4 OES 77FLA 01 234 OES 77FLA 01 I

98A- 2
TABLE 98A-2: INDIVIDUAL DATA FOR NBS SRH 98A

Cone Uncer Com Method Reference

Nb (ug/g?

39.9

.jjd (ug/g?_

98

162

Pb (ug/g)

66.8

69.2

Rb (ug/g)

35

S (ug/g)

1300

Sb (ug/g)

2.3

2.57

Sc (ug/g)

28.8

34.8

Si (%)

22.2

Sm (ug/g)

9.18

15

Sn (ug/g)

OES 77FLA 01

2.6 ITNA 77FLA 01

OES 77FLA 01

0.1

0.21

2.4

AA

OES

84TER 01 77FLA 01

2.3 ITNA 77FLA 01

CB 78TER 01

ITNA HAA

OES

ITNA

77FLA 01

84TER 04

77FLA 01 77FLA 01

1.2 lENA 84CEL 01

OES

ITNA

77FLA 01 77FLA 01

4.88 OES 77FLA 01 5.25 AA 82TER 01 5.76 0.3 FAA 85TER 01

Cone Uncer Com Method Reference

Sr (ug/g)

438

Ta (ug/g)

2.46

Tb (ug/g)

2.92

Th (ug/g)

23.9

Tl (ng/g)

351

554

Y (ug/g)

176

Yb (ug/g)

9.3

10.3

Zn (ug/g)

OES 77fU 01

0.03 tTNA 77FLA 01

0.06 ITNA 77FLA 01

0.11 ITNA 77FLA 01

40 7 ASV 82CAL 01

OES 77FLA 01

OES 77FLA 01

0.29 ITNA OES

77FLA 01

77FLA 01

< 23 L ITNA 77FLA 01

Zr (ug/g)

740 32 ITNA 77FLA 01

98A-3
TABLE 99-1: COMPILED DATA FOR NBS SRM 99 SODA FELDSPAR (revised 3/1/86)

Fl P UNITS NBS CONSENSUS MPD T AM RANGE NAA OTHEI

. Mean ± SD (n) Mean (n) Moan + Me3n 1

'

' '

Ai % i0.08 10.07 (1) _ _ _ _ _ _ 10 07

ua/a uy/ y 10 (1) _ _ _ _ _ 10 f 1 ^ Ba uy/ y 90 < 130 _ _ , < 130 < 800

Ca ua/a 2570

Ce 8 (1) 8 (1)

Co na/a 740 (2) 700 - 780 740 (2)

Cr uq/q 7.2 ± 5.1 (3) 8.51 3.3 - 13 4.3 (2) 13 (1)

Cs nq/q 700 (1) 700 (1)

Cu ug/g 21 (2) 20 - 22 21 (2)

Eu nq/q 350 (1) 350 (1) Fe uq/q A70 500 (1) 500 (1)

Ga uq/q 30 (1) 30 (1)

Hf nq/q 900 (1) 900 (1) K ua/qy/ y 3400 - - -

LOI 0,52 _ _ _

La ua/a < 8

_ _ , < 8 < 100 Lu na/a < 200 < 200

UQ/a 320

Mn UQ/a < 70 31 (2) 12 - 50 31 (2) Na % 7.96 7.94 (1) 7.94

Nd uq/q < 4 < 4

Ni uq/q «a/ a 15 (1) 15 (1

)

p uq/q 620 567 (1) 567 (1

)

Pb uq/q 106 (2) 62 - 150 106 (2)

Rb uq/q 23 (1) 23 (1)

Sb nq/q 500 (1) 500 (1)

Sc nq/q 830 (1) 830 (1)

Si % 32.06 32.05 (2) 32.05 - 32.05 32.05

Si

.

% 32.05

Sm uq/q < 2 < 2 Sr uq/q 220 ± 160 (3) 130 120 - 400 120 (1) 265 (2) Ta 1uy/in /aa 1.9 (1) 1.9 (1)

Tb ng/g 280 (1) 280 (1)

Th ug/g 1.6 (1) 1.6 (1)

Ti ug/g 100 240 ± 220 (4) 68 61 - 560 140 ± 70 (3) 560

U ug/g 1.09 (1) 1.09 (1)

V ug/g < 10 < 10 Y ug/g 10 (1) 10 (1)

Yb ug/g 1 (1) 1 (1)

Zn ug/g 15.9 ± 1.8 (3) 15 14.6 - 18 16.3 (2) Zr ug/g 26 (2) 11 - 40

99-1
TABLE 99-2: INDIVIDUAL DATA FOR NBS SRM 99 (revised 3/1/86)

Cone Uncer Com Method Reference

10.07

B (Ufl/3?

10

Ba (ug/g)

<

<

Ce (ug/g?

8

Co (ng/g)

TITR 58WAT 01

OES 63CLA 01

130

800

ITNA OES

Cr (ug/g)

3.3

5.3

13

Cs (ng/g)

700 100

Cu tug/g)

20

22

Eu (ng/g)

350

Fe (ug/g)

500

Ga (ug/g)

30

20 L 0.16

77FLA 01 63CLA 01

0.6 ITNA 77FLA 01

< 10000 L OES 63CLA 01 700 30 ITNA 77FLA 01 780 120 RTNA 61TUR 01

OES 63CLA 01

Cone Uncer Com Method Reference

Hf (nfl/g)

900 60

La (ug/g)

ITNA 77FLA 01

<

<

8

100

ITNA OES

77FLA 01 63CLA 01

Lu (na/n)

< 200 L ITNA 77FLA 01

Mn (ug/g)

12

^0

Na (%)

7.94

Nd (ug/g)

OES

OES

64FIL 01 63CLA 01

UXRF 83BAL 01

< 4 L ITNA 77FLA 01 OES 63CLA 01 1 ITNA 77FLA 01 1 Ni (ug/q)

RTNA 61TUR 01 1 OES 64FIL 01 1 15 OES 63CLA 01

P (ug/g)

ITNA 77FLA 01 1 567 OES 64FIL 01

Pb (ug/g)

OES 63CLA 01 1 62 OES 64F1L 01 OES 64FIL 01 1 150 OES 63CLA 01

Rb (ug/g)

ITNA 77FLA 01 1 23 1.6 ITNA 77FLA 01

Sb (ng/g)

ITNA 77FLA 01 1 500 60 ITNA 77FLA 01

Sc (ng/g)

< 10000

830 10

OES

ITNA

63CLA 01 77FLA 01

99-2
TABLE 99-2: INDIVIDUAL DATA FOR NBS SRM 99 (cont.)

Cone Uncer Com Method Reference

32.05 COLOR 82SAR 01 32.05 0.01 TITR 770HL 01

Sm (ug/q)

< 2 L ITNA 77FLA 01

Sr (uq/g)

120 RTNA 61TUR 01 130 OES 75TH0 01 400 OES 63CLA 01

Ta (ug/a)

1.9 0.02 ITNA 77FLA 01

Tb (ng/g)

280 6 ITNA 77FLA 01

Th (ug/g)

1.6 0.03 ITNA 77FLA 01

Ti (ug/g)

61 OES 64FIL 01 150 3 OES 63CLA 01 200 3 OES 63CLA 01 560 COLOR 63K0R 01

Cone Uncer Com Method Reference

1.09 DNA 66HAM 01

< 10 L OES 63CLA 01

Y (uq/q)

10 OES 63CLA 01

Yb (uq/q)

1 0.06 ITNA 77FLA 01

zn (uq/q)

14.6 RTNA 65BAL 01

15 XRF 65BAL 01 18 0.82 ITNA 77FLA 01

Zr (ug/g)

< 100 L ITNA 77FLA 01

11 OES 64FIL 01 40 OES 63CLA 01

99-3
TABLE 99A-1: COMPILED DATA FOR NBS SRM 99A SODA FELDSPAR (revised 3/1/86)

ELE UNITS NBS CONSENSUS MEDIAN RANGE AA NAA OTHER METHODS

Mean Mean ± SD (n) Mean (n) Mean (n) Mean (n) Method

Al % 10.8 — — — —

Ba ug/g 2330 2570 (1) — — 2570 (1) —

Be ug/g — 2.02 (1) — 2.02 (1) — —

Bi ng/g ... 3 (1) ... — 3 (1) — —

C ug/g — 300 (1) — — — 300 (1) CB

Ca % 1.53 1.51 (1) — 1.51 (1) — —

Cd ng/g — < 200 — — — —

Ce ug/g ... 5 (1) — — 5 (1) —

Co ng/g — 100 (1) — — 100 (1) —

Cr ug/g — < 3 — — < 3 —

Cs ug/g — 5 ? (2) 0.5 - 9 9 (1) 0.5 (1) —

Eu ng/g ... 820 (1) — — 820 (1) —

Fe ug/g 450 475 (2) 450 - 500 450 (1) 500 (1) —

Hf ng/g — 300 (1) — — 300 (1) —

Hg ng/g — 165 (1) — 165 (1) — —

K % 4.3 4.27 ± 0.12 (3) 4.2 4.2 - 4.4 4.4 (1) — 4.2 (1) FE K %

... ~ ~ ~ — — — — 4.2 (1) ISE

LOI % 0.26 ~ ~ ~ — — — — —

La ug/g — 22 (1) — — — 22 (1) —

Lu ng/g — < 100 — — — < 100 —

Mg ug/g 120 130 (1) — — 130 (1) — —

Na % 4.6 4.55 ± 0.09 (3) 4.6 4.45 - 4.6 4.45 (1) — 4.6 (1) ISE

Na % — — — — — 4.6 (1) FE

Nd ug/g — < 4 — — — < 4 —

P ug/g 87 55 (2) — 50 - 60 — — 60 (1) COLOR

Rb ug/g — 104 (2) — 100 - 109 100 (1) 109 (1) —

S ug/g — 19 (1) — — — — —

Sb ng/g — < 300 — — — < 300 —

Sc ng/g — 230 (1) — — — 230 (1) —

Si % 30.4 30.42 (1) — — 30.42 (1) — —

Sm ng/g 500 (1) 500 (1)

Sn ug/g 0.45 (1) Ta ng/g < 200 < 200

Tb ng/g < 200 < 200

Th ng/g 500 (1) 500 (1)

Ti ug/g 42

Yb ng/g < 300 < 300

Zn ug/g < 7 < 7

Zr ug/g 70 (1) 70 (1)

99A-1
TABLE 99A-2: INDIVIDUAL DATA FOR NBS SRM 99A (revised 3/1/86)

Cone Uncer Com Method Reference

Ba (ug/g)

2570 38.6 ITNA 77FLA 01

Be (ng/g)

2020

Bi (ng/g)

3

C (ug/g)

300

Ca (%)

1.51

Cd (ng/g)

< 200

Ce (ug/g)

Co (ng/g)

100

Cr (ug/g)

AA 83TER 01

FAA 84TER 03

CB 78TER 01

AA 73RAM 01

ICPES 83UCH 02

0.29 ITNA 77FLA 01

ITNA 77FLA 01

< 3 L ITNA 77FLA 01

Cs (ua/fl)

0.5

9

Eu (ng/g?

820

Fe (ug/g?

450

500

0.03 ITNA AA

77FLA 01 72ALL 01

ITNA 77FLA 01

AA

ITNA

73RAM 01 77FLA 01

Cone Uncer Com Method Reference

Lu (ng/g)

Mg (ug

130

Na (%)

4.45

4.6

4.6

Nd (ug/g)

P (%?

0.005

0.006

Rb ( ug/g)

100

109

s (ug/g)

19

Hf (ng/g?

300 30

Hg (ng/g)

164.6

< (%)

ITNA 77FLA 01

7.35 FAA 82FLA 01

0.13

FE

ISE AA

75PUF 01 75PUF 01 73RAM 014.2

4.2

4.4

La (ug/g)

22 1,9 ITNA 77FLA 01

< 100 L ITNA 77FLA 01

AA 73RAM 01

0.1

AA

FE

ISE

73RAM 01 75PUF 01 75PUF 01

< 4 L ITNA 77FLA 01

0.0001

0.0002

1.2

ICPES

COLOR

AA

ITNA

83UCH 01 83UCH 01

72ALL 01 77FLA 01

CB 78TER 01

99A-2
TABLE 99A-2: INDIVIDUAL DATA FOR NBS SRM 99A

Cone Uncer Com Method Reference

Sb (ng/g)

< 300 L ITNA 77FLA 01

Sc (ng/g)

230

Si (%)

30.42

Sm (ng/g)

500

Sn (ug/g)

0.45

ITNA 77FLA 01

0.4 AA 82KIS 01

70 ITNA 77FLA 01

AA 82TER 01

Cone Uncer Com Method Reference

Ta (ng/q)

< 200 L ITNA 77FLA 01

Tb (ng/g)

< 200 L ITNA 77FLA 01

Th (ng/g)

500

Yb (ng/g)

ITNA 77FLA 01

< 300 L ITNA 77FLA 01

Zn (ug/g)

< 7 L ITNA 77FLA 01

Zr (ug/g)

70 ITNA 77FLA 01

99A-3
TABLE 120A-1: COMPILED DATA ON NBS SRM 120A PHOSPHATE ROCK (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE ICPES OTHER METHODS

Mean Mean ± SD (n) Mean (n) Mean ± SD (n) Method

Al ug/g 5000 4500 (1) ... 4500 (1) —

Be ug/g 1 .88 (1) ... 1.88 (1) AA

C % 1 .04 (1) ... 1.04 (1) CB

C- inorg ug/g 8700 --- - - -

Ca % 36 36.06 (2) 36.02 - 36.1 36.1 (1) 36.02 (1) TITR Cd ug/g 1 1 .8 (1) — 11.8 (1) AA

F % 3.92 3.90 ± 0.10 (7) 3.88 3.8 - 4.04 3 .88 ± 0.09 (5) ISE

F % — 4.04 ( 1 ) CPAA

F % — 3.82 (1) COLOR

Fe ug/g 6990 7340 (1) — 7340 (1)

Hg ng/g 57.5 (1) — 57.5 (1) AA

K ug/g 830 —

Mg ug/g 1600 1400 (1) — 1400 (1)

Mn ug/g 150 160 (1) — 160 (1) ...

Na ug/g 3000 —

pr % 15

Pb ug/g 9.3 (1) 9.3 (1) AA

s 2900 (1) 2900 (1) CB

Ti ug/g 720 720 (1) 720 (1)

U ug/g 110 (1) 110 ( 1 ) COLOR

TABLE 120A-2: INDIVIDUAL DATA FOR NBS SRM 120A (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Al (uq/q) Fe (ug/g)

4500 ICPES 80BRE 01 1 7340 ICPES 80BRE 01 Be (uq/g) Hg (ng/g)

1.88 AA 83TER 01 1 57.5 3.6 FAA 82FLA 01

C (%) Mq (uq/q)

1.04 CB 78TER 01 1 1400 ICPES 80BRE 01 Ca (%) Mn (ug/g)

36.02 TITR 80HIT 02 1 160 ICPES 80BRE 01 36.1 ICPES 80BRE 01 1 Pb (uq/q)

Cd (uq/q)

9.3 AA 84TER 01 11.8 AA 84TER 01 1 S (ug/g)

F (%) 2900 CB 78TER 01

3.8 11 ISE 69EDM 01 1 Ti (ug/g)

3.8 0.1 ISE 77H0P 01 1 3.82 0.05 COLOR 83CHA 02 1 720 ICPES 80BRE 01 3.88 11 ISE 69EDM 01 1 3.93 11 ISE 71PET 01 1 U (uq/q)

4.01 11 ISE 71 PET 01 1 4.04 CPAA 85R0E 01 1 110 10 COLOR 810GU 01

120A-1
1g

8 «>

I- «0 o u

u

u

ooo

o

vtz

00

CO o

CO

(3u CO U I—

< to

LU U

O. C/) U O —• —. I—

o- o 00 oo

CO

o

w w Ui

a. M ^ c

to

o

PJ

<0 (NJ v-^ w \^ ^—^

o

«- (\J PO CM

(M m H CO (\J

ro

ro 00 r^ »-

•o ro oIDro

00

fVI o o> in •

oofMV

ro

M

">«

u

o

UI<

o.too

3 c Z (D

z:

5

O N. >0 o in

«- (M

o fVI in m in

00 O

CO

ro fNj ro rvi

ro

in 00 fO ro

in

ro

(M o

CO

CO

eaoIM

m

UJID<

o

oo

o PU

CO

fVI

00

to

• CO in in (M ro fvj «-

ro

ro -O

ro

^ O N. >0 ^ ^»

• o 'in • «— O «- (M CO

CO o fM

«- ro

vi- in 00

«- ro

or>~

O 00 in Nroo o • o vj- 00CO o• ro >0

CO

Q

o00

o«

in

o• (M 00 m <\i »-

0>

in CO ro ro o

O 00

I o

: 5 00

CQO(MCOM Q Z CO UJ

CO +) S c U (D z

«- CO rvi o to ro fVI ro IM ro in rvi to «- PM o

\^

o PJ o CO in •J- 00 ro ^

to o o >* «o in >o in 1 1 PJ

in 00 ro 1 x H +) CO &• in o 1 <> 1 o in V fM >* (M in in <y >o o o to in <M 00 in o -* to CO in to ro

to

o

o

c M (0 CO 0) Oo-oino to 00 in

to

I ^ i

I I to

o o

OI o> OI OI OI OI OI CD OI OI OI O) OI OI OI OI OI OI OI OI OI OI OI »v >>. \ >» >>. cn cn OI o> OI OI OI OI OI at OI OI OI OI OI OI OI OI OI O) OI 3 3 3 3 3 3 C S« X 3 X 3 3 3 3 3 3 3 3 X X X 3 3 3 3 3 3 3

17) —' U) < < <

3 <D V < OB oa CO u u

o 01 O C 3 > U U O U O

«) T3 Hu. u. C3 z — 3

120B-1
c

(0

v> </> LU

Q. +1

<_) c

(P

<u

4-' o

c o c Q (0

1 1

1

(/) Q3C

IX

CO AA 13

t—

1

(0

CNi

a:

CO

t«

caz

ai

0£O z U- <a: <1—<

O

lU

_l

CL <

o o

1 COoCM

LU c: _lm

<1— V) o z

lUw H

z

o c

CI z

oo

o

o z <s

C/) o 5

CJ <: o CO CJ (/> 3

* - rvj o 00

1 1 o o 1 1 1 1 1 1 t 1 , tc o 1 1 1 1

1 1 o o 1 1 1 ro 1 1 1 1 1 1 ^ in ro 1 1 1 1

1 1 CO o 1 1 1 f\J 1 1 1 O 1 1 1 f\J CM 00

/-^

rvj fM in ro fO CM ro o 00o o ro

f\J o in o in in «

tn LTV o 1 in 1 o o in 1 1 1 1 ro 1 in -H CJ 1 ro -H •H o • 1 ' 1 •H • f\I V >o 1 1 1 1 1 o 1 f\j (M V si- ro O ro (\J

o

O

CM (M fM

^ T- ^ f\J

03 fvj oO OJ o «-

CO

in

CO o

o ro O 1 1 ^ 1 1 ^ 1 I fM < 1 ^ r— 1 1 1 1 1 1 i 1 O 1 1 N- o O 1 1 1 1 • 1 1 ^0 ) ro ^ Dill 1 1 1 1 CO 1 1 O (M ro I 1 fM 1 1 OJ 1 1 1 1 1 1 1 1 1 1 1 fM 1 fM fM fM fM o

o o in o fM s- o o o co fM in fM o CO

fM fM fM ro

1 1 1 fM ro

1 o

1 o

1 o1 00

1 fM1 1 1

1

1 1 1 fM

1 1

1 CO o ro o nO O

>o fM ro ro in

<

fM fM

ino .o o o in ~* CO fM

<> <y fM

fM

1 o1 1 ro1 o1 N- o O 1^ f£ in

o o O 1 1 1 1 1 1 o ro 1^ • in 1 1 1 1 1 1 fM

h- fM <i in in fM 1 1 1 Ilia fM fM

in fM o O fM o in • <M o o O

ro

roro»-N-rofM«-»-fM«- o ro •>- 1- in »- ro >t fM «—

inV

o

fMosO o

in NCOo ro o -* o

-O -H •H o CO ro

ro ro fM

-4- fM in V o

in

o

H

fM ro

fM fM

«— in o

oO fM

(M

o o o fM o

+1 •H m+4 COfM

+) fM •H o o fM

ro oN- o

CO CO o

c o o o (D in

00 0) rs. fM z z rvi

o 00

fM

in

' o o 1 -H 1

128.4

1

cn CD O) D> O) o> O) > ) o> cn cn O) \ \ \ \ \ \ \ \ \ \ \ \ CD o u> O) O) o> O) tj) O) ) O) ) 3 3 3 3 3 3 3 S« »S 3 3 3 3 3 3 >e 3 3 3 c 3 3 3 3 3 3 3 3 3 3

> C O (Q (0 "D — 13

fM

fM

SI

V> to to CO Crt (/)</> to

(U ^ — E

00

ro

fM

I 3 >- C eisl ISI

120B-2
TABLE 120B-2: INDIVIDUAL DATA FOR NBS SRM 120B (revised 3/1/86}

Cone uncer Com Methoa Reference

Cone uncer Com neLnoa Reference |

1 Ca (%)

Ag (ug/g) 1

1 17 fi

1 fmO SIMS 78M0R 01

c3

T PDCC 81CHU 01 1 TLUS '70i-'i A n/ ^oGLA 04

1 TT cXKr oUDAL 01 Al <ug/g) 1 3^. to ICPES o^JEN 01

1 .70 U. f c

A A AA o^JcN 01

CI fin 1 nn { UU AA 82JEN 01 1 1 . 10 T PDCO 1 CrcS 0 1 r^ui 1 ni olCHU 01

¥ PDCC 1 Lrtb 82JEN 01 1 TC O/. 11 I PDCC ICPES O^HOr 01 C07A ILrto 81CHU 01 1 TC O/ 11 ICPcS D/ Lirnr ni ohHOF 01 coon 1

1

ILrtb 83H0F 01 1 TC / 1 U.UO 11 T fDCO 11 ICPcS OhHOF 01 Annn JJ 78GLA 04 1

I 1 1 Ur Co AXunc ni

ouuu 1

1

t

I PDCC lor Co 84H0F 01 1 oUUU HiSU 1

1

ICPtS 84H0F 01 1 Cd (ug/g)

oUUU i 1 T PDCC 83H0F 01 1 7*7Dn CVD C tXRF 80DAL 01 1 on 1 ^U. 1 A A AA O / TED D 4 o4TEK U1 oDUU Rcnn o 1 no 78M0R 01 1 Cc. in T

1 PDCC Lrco o 1 LnU U

1

1 A A AA 7A^D I n7

As (ug/g) 1

e: 1L 1 Co 81CHU 01 1 U A A HAA 84TER 04 1 inn lUU f TU A

1 1 NA QCDnT no o3rUI uc 118 ICPES 84MCA 01 Au (ug/g) 1 128 3 ICPES 85JAR 02

1 182 3.6 ICPES 81CHU 01

< 3 L ICPES 81CHU 01 1

1 Co (ug/g)

Ba (ug/q> 1

1 1 1 NM W 1 1 2 ICPPS I Wr KbO 81CHU 01 1 1 ICPES 81CHU 01

Be (ug/q)

1

j

cr (ug/g)

AA 82TER 02 1 CA T

1 TWA 1 Nn A*^D^T OJrUI f\y KJC 2.82 D AA 83TER 01 1 63.1 1.9 ICPES 81CHU 01 2.9 0.06 ICPES 81CHU 01 1

j

Cu (ug/g)

Bi (ng/q)

1

fi A O.O 1 T PDCC 1 Lrto Ripuii ni o iLnu u

1

< 25000 L ICPES 81CHU 01 j 11.3 AA 76KRI 03

197 HAA 84TER 02 1 197 D FAA 84TER 03 j Dy (ug/g)

c (%) 17 ICPES 84MCA 01 17.3 0.2 ICPES 85 JAR 02

0.983 CB 77TIL 01 1 1.8 SIMS 78M0R 01 1 Er (uq/q)

11-4 0.1 ICPES 85JAR 02

12 ICPES 84MCA 01

120B-3
TABLE 120B-2: INDIVIDUAL DATA FOR NBS SRH 120B (cont.)

Cone

Eu (ug/g)

Uncer Com Method Reference

3.5 ITNA 85POT 02

3.5 ICPES 84MCA 01

3.89 0.07 ICPES 85JAR 02

A.

8

1 ICPES 81CHU 01

3.78 0.07 NAA 80NOR 01 1 La (ug/g)

3.82 35 lENA 79GLA 03 1 3.89 0.21 IC 82JEN 01 1 79 ITNA 85POT

3.93 0.09 CPAA 84HAN 01 1 89 4 ICPES 81CHU

4.04 0.47 ISE 82JEN 01 1 90 ICPES 84MCA

92.8 1.6 ICPES 85 JAR

Fe (ug/g)

3200 SIMS 78M0R 01 6570 ITNA 85POT 02

6600 200 AA 82JEN 01 6990 11 ICPES 83H0F 01 7000 11 ICPES 84H0F 01 7200 800 ICPES 82JEN 01 7400 35 TCGS 78GLA 04

7500 300 11 ICPES 83H0F 01 7500 350 11 ICPES 84H0F 01 7700 35 lENA 79GLA 03

7827 AA 76KRI 03

7900 200 ICPES 81CHU 01 7970 EXRF 80DAL 01

Gd (ug/g)

17.8 0.3 ICPES 85JAR 02

18 ICPES 84MCA 01

21 0.6 ICPES 81CHU 01

Hf (ug/q)

Ho (ug/g)

3.8

4.03 0.04

ITNA

ICPES

ICPES

85POT 02

84MCA 01 85JAR 02

Cone

< (ug/g>

110

600

660

760

800

1170

Uncer Com Method Reference

35

200

100

25

TCGS

ICPES

EXRF

SIMS

AA

ICPES

L' (ug/g)

Lu (ug/g)

1.6

1.71

1.8

Mg (u3/g?

51 1600

1600

1700

1700

1700

1700

1870

2800

Mn (ug/g)

130

150

230

240

246

260

Ho (ug/g?

0.05

ICPES

ICPES

ICPES

ITNA

78GLA 04

82JEN 01 80DAL 01 78M0R 01 82JEN 01 81CHU 01

81CHU 01

84MCA 01 85JAR 02

85POT 02

35 TCGS 78GLA 04

100 ICPES 82JEN 01 100 AA 82JEN 01

11 ICPES 84H0F 01

11 ICPES 83H0F 01 60 11 ICPES 84H0F 01 100 11 ICPES 83H0F 01 60 ICPES 81CHU 01 SIMS 78M0R 01

SIMS 78M0R 01 EXRF 80DAL 01

15 ICPES 82JEN 01 20 AA 82JEN 01 AA 76KRI 03

7.8 ICPES 81CHU 01

5 L ICPES 81CHU 01

120B-4
TABLE 120B-2: INDIVIDUAL DATA FOR NBS SRM 120B (cont.)

Cone

Na (ug/g)

Uncer Com Method Reference

Nd (ug/g)

Ni (ug/g)

0 (%)

36

P (%)

2300 100 AA 82JEN 01 1 2200 EXRF 80DAL

2630 70 ICPES 81CHU 01 1 2800 35 TCGS 78GLA 04 1 Sb (ug/9)

2900 SIMS 78M0R 01 1

12 35 lENA 79GLA 03

15.4 1 ICPES 81CHU 01 i2.9 AA 76KRI 03

0.5 14NAA

Pr (ug/g)

17

17.9 0.2

Ra-226 (pCi/g)

43.3 0.6

ICPES

ICPES

GAMMA

80NOR 01

12.97 0.79 IC 82JEN 01 13.5 SIMS 78M0R 01 14.7 35 TCGS 78GLA 04

14.96 0.14 11 ICPES 84H0F 01 15.04 0.14 11 ICPES 83H0F 01 15.12 11 ICPES 84H0F 01 15.19 1.23 ICPES 82JEN 01 15.2 11 ICPES 83H0F 01 15.21 0.38 ICPES 81CHU 01 15.9 EXRF 80DAL 01

13.1 AA 84TER 01

25 5 ICPES 81CHU 01 32.7 AA 76KRI 03

84MCA 01 85JAR 02

83KIM 01

68 ITNA 85POT 02 1 Sc (ug/3)

77 ICPES 84MCA 01 1 79.5 0.9 ICPES 85JAR 02 1 6.4 ITNA 85P0T

127 25 ICPES 81CHU 01 1

Cone

S (ug/g)

Uncer Com Method Reference

1.62

10

HAA

ICPES

Se (ug/g)

Si (%)

2.01

2.12

2.12

2.19

2.21

2.23

2.23

2.32

2.32

2.41

Sm (ug/g)

15.8

16

38

Sn (ug/g)

0.41

Sr (ug/g)

705

Ta (ng/g)

200

Tb (ug/g)

30 ICPES

84TER 04

81CHU 01

81CHU 01

EXRF 80DAL 01 35 lENA 79GLA 03

0.19 ICPES 82JEN 01 35 TCGS 78GLA 04

0.01 AA 82KIS 01 0.03 11 ICPES 84H0F 01 0.03 11 ICPES 83H0F 01

11 , ICPES 84H0F 01

11 ICPES 83H0F 01 0.24 AA 82JEN 01

0.2 ICPES 85JAR 02

ICPES 84MCA 01 1.9 ICPES 81CHU 01

3 L ICPES 81CHU 01 0.05 FAA 85TER 01

14 ICPES 81CHU 01

ITNA 85P0T 02

ITNA 85P0T 02

120B-5
TABLE 120B-2: INDIVIDUAL DATA FOR NBS SRM 120B (cont.)

Cone Uhcer Com Method Reference | Cone Uncer Com Method Reference

Th (ug/g) U-238 (DCi/q)

< 25 L ICPES 01 1 42.8 0.8 GAMMA 83KIM 01

7.2 ITNA RSPOT 02 1 7.9 0.8 AS 01 1

1 9.05 0.4 AS 82TH0 02 1 103 3.1 ICPES 81CHU 01

Ti (uq/Q) 120

280

10

40

ICPES

AA

82JEN 01

82JEN 01 590 SIMS 78M0R 01 1 740 20 ICPES 81CHU 01 1 Y (uq/q)

780 35 lENA 79GLA 03 1 950 35 TCGS 78GLA 04 1 172 5 ICPES 85JAR 02

950 10 11 ICPES 83H0F 01 1 950 10 ICPES 84H0F 01 1

1 Yb (uq/g)

1200 EXRF 80DAL 01 1 10 ICPES 84MCA 01

Tm (ug/g) 10.2

10.8 0.2

ITNA ICPES85P0T 02

oe A n AO 85JAR 02

1 .1 ITNA 85POT 02 1 12.

7

D.H iCPcS BiCHU 01

U (uq/g) Zn (uq/Q)

125.7 0.6 DNA 86GAU 01 1 107 AA 76KRI 03

130 5 AS 82R0E 01 1 127 3.9 ICPES 81CHU 01

130.25 1.5 ICPES 83N0R 01 1 132 2 AS 82TH0 02 1 Zr (uq/q)

140 ITNA 85POT 02 1 12 1.2 ICPES 81CHU 01

120B-6
TABLE 181-1: COMPILED DATA FOR NBS SRM 181 LITHIUM ORE (SPODUMENE)

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

BiK

LiNa

ng/g

ug/g

%

ug/g

892 (1) AA 2500

2.97 ± 0.02

5900

TABLE 182-1: COMPILED DATA FOR NBS SRM 182 LITHIUM ORE (PETALITE)

(revised 3/1/86)

ELEMENT UNITS NBS

K

LiNa

Rb

ug/g

%

ug/g

ug/g

830

2.02 ± 0.02

3000

275

TABLE 183-1: COMPILED DATA FOR NBS SRM 183 LITHIUM ORE (LEPIDOLITE)

(revised 3/1/86)

ELEMENT UNITS NBS

Cs ug/g 2800

K % 6.6

Li % 1.92 ± 0.02

Na ug/g 1500

Rb % 3.2

TABLE 181-2: INDIVIDUAL DATA FOR NBS SRM 181 (revised 3/1/86)

Cone Uncer Com Method Reference

892 FAA 84TER 03

181-1
"8

JC 8 £c

ooH

o </) U UJ

1-

o

cn

aiO

H

in

(M

(/) (/I C9 u CO Ul O o o

t— 1—u1—^

ro to or— o -fl 00 •H (M O o

>o

0£

CO

U

O Q£

CJ

—I —I I—

CJ < O

—

1— CJ

O (-

O

CM in

to

V> CO O CJ

o «- «-

^0

COo

+1 3 8 o

fMo

ino

OfX

c

(1) in

oCOmV

in

c

CO ^

UJa.

c

00 ^ o 00 «-o

^d -*

t^

tvj (M vO 5

^\

rvj to to f\J in >* t^ tM to to to (\)

c >^ ^>

r\j to m rvi o »

o

o (A o (\l

omooo f\Jooo CM in 1 1 1 o 1 to 1 1 CM

+f +1 1 M 1 I in 1 -H +)

H -tl +1 1 +1 1 I -H 1^ fVJ 1 I 1 I (M 1 1 1 1 t 1 c o o in t^ o 00 o -3- to vO in !«. ID o %o in CO m CO

UJ

C3< 4

o

t^ in CM CM

00

to COo

1^

o

o 00 c> o»- CM CM

in

>0

CM

o

o in 00 CO

N- ^ -O oo 00

«- -J- in

o 1^ in CO rO in • to CM

CM 1^ in «0 00

o5 m in o>

00

~ 5 ;S

>o • t^ to

CMto

ooto

in

o8 in

oo'I I O CM

00

Q < o

O in in CM CM CM to

UJ ino 1 o 1 I O 1 o inO >* 1 1 ino 1 CO CM

_J

o 1 in 1 1 O 1 vd CM

O 1 in 1 1 UJ t^ in 1 CM o 1 CM 1 1 in in 1 t^ 1 1 in in 1 1 00

:oMP z

to CM in CM to t^ CM 00 <t in to CM 00 CM CM

O to to to

c

CM </> to CM 00 sr >o 3 CM o to CM to o o UJ (/> a o O in o _l z (/> o o CM CM o in O O o o CM o o to o CM o m o o CO Ul r~ 1 1 O in to to o < (/) H •H H +1 H +4 i 1 -H 00 •H +1 H +) H H -H *{ 1 •H H -t-i +1 z CM 1 1 V to o o o o c o in o CO O o CM >* in O o o CJ n> CM o 00 CM o t>. to

a>

o CM CM >d in >d CO in

X t^ r— ?I 00

CO

COCn

00 <M CM o CM o o o o CM CM o o o 1 • in O 1 1^ o 1 i in »- in 1 1 o o 1 1 to 1 •H 1 1 CM 1 1 CM o +1 CM 1 M I -4- o •H +1 1 1 B 1 1 B 1 1 »— 1 1 m ^ 1 in 1 • 00 in 1 1 in 1 00 O to

toO

m

to

—' U) < <

O) \

CJ)

\

C3) \at a> \at at at \

at at at

O) at at at at at at at at at 3 3 3 3 3 3 c 3 3 3 3 3 3 3 3 3 c 3

CD ca at

0)

c

CQ CO I 10 CJ CJ

u

<u

—< —

O CJo

O

C (A

U CJ CJ 3 l- 3

CJ £3 Ul UJ

»s »s ?s >«

tooCM

O

o> at at at at \ at at at CD 3 3 3 3 3 1 o ID •a CM CM H- O

C3 C3 3C z 3: IE

278-1
JC 8 £

uic

Uica«

(/> CA (/) CA

W CA tf) C9 U u C3 z: o C3 ID O U u U o o O I— h- t- 1— 1— 1— »—

#^ ^ ^\

N» ro rj <\l ro -o o

00

1^O

O

lO

fVl

NO

O

o e\j o o M -H ro CO • in

oo

CA

O3

in CM

(0

0)

coo

Of

cC

O (D 2 S (A Z 8e 3c

<u

CM OJ CM CM \^

r- in

o in 1 V* 1 1 o tA 1 lA 1 O 0 1 1 1 1 1 1 1 O 1 1 N- 1 1 CM 1 1 I 1 1 00 1 1 1 ro 1 1 t CM 1 t 1 in in 1 1 1 in ro 1 ro 1 (M 1 1 1 1 1 1 t 1 CM 1 o> ro CM

»^ ^\ /-^ ^\ ^\ ^ *— ^TM r— «^ «~

w \^ \^ N^ %^ «* >o CO 00 1 O O o eo 1 I 00 o 1 1 lO O o 1 o 1 lO tvi ro 00 1 • 1 >o 1 1 »— 00 o 1 CO CO o> 1 lO hi ro OJ <» 1 1 1 nO 1 1 vl- m 1 ro CM r-

<^ <^ *^ CM >* <\I •<t in lA

o CO CM CM

w \^

ro NO

«TM*

o CM >o

o • • o in o 00 \0 o o o o o o in

o h- • • 4 1 1 1 1 -4- 1 00 1 CM 1 00

•H 1 1 H

H 1 1 M +1 •H 1 •H lA +1 +1H 1 +1 +1 1 -t-i in o> 1 1 to I 1 1 1 1 in CM K1 o m o in CM >o 00 o N- o 00 in K> CO AJ ^ LA ro • CM m lA

(A

(A

COz

00 00

o >o

m

mo

R in in ro 00 ro r^ ro ro ro lO • eo 1 lA 1 o 1 o • 1 CM 1 1 1

«o

CM ro <o >*• CM • ro CM

ro ro

o >0 ro

N- eo • >* r- 00 «-

in

CM

•>o ro

CM

ro CMo ro CM • o ^ • • ro in

o o>

in 0> si- • O •* • r^

>* in in

CM

«*

o CM 00 •* o> >0 in CO ro 00 r^

oo 00 ro eo 00 in

CM

m SI- in CM CM ro

o CM in CO CO ro o ro ro CO rs." CM >d (M ro in CM ro to' I

in ro CM oo ce ro ro o 1 CM • 1 1 1 1 o «- oo o CM o o in CM r- vO ro CM • 00 ^ 1 1 1 1 ro • • ro CM CM ro • m

ro 00 • ro ro ro CM I I 1 1 1— «— in ro in ro vio

o>

(M I sCM

UJ

CD CACA

(AO

C

U CD

ro

CO 00 CM ro r^ CM CM CM CM CM >o in 00 vO >o ro

o ro ro eo

m

o ro >o ro o o in CM o s* CM <0 in o o «TM d >» <^ CM d CM >o o o o O ro o d o in o CO ro o fs. m CM o *\ >* M 00 H -M H •M 00 -H -H M 44 H •H H H H H -H M -fi -fi •fi -H to ro o O CM o ty ro CM 00 eo o OO o o ro in in in

ro ro CM On

m CM ro CM (M in >* inO • «0 ro ro in ro in CM ro CM ro ro ro

CM >* >o o o ro CM ro o ro

o

o in • ro

Oo CA o 1 1 • o o o 1 o 1 O o in o o CM o

o 1 1 in in I -M I : R o M -H 1 -H M -H • «- -H -H •fi H 1 1 in 1 1 st 1 1 in in 1 ^ c tn o » vO O m in -4- O o 00

CD >*

o

O r^ in

«> • >*• » ro nO CM >* in X ro ro «— (M >*

ro

«^

(A cn D> cn o> C3) cn cn o> cn cn cn cn cn cn cn cn cn tn C3> s^ Sv •V. •>> s^ v^ —.

o> o> at o> o> cr> o> cn cn cn Sn cn cn cn cn cn cn o> cn cn o> cn cn cn

c »c 3 c 3 3 3 »« 3 3 3 3 3 3 3 3 34 3 3 3 3 3 3 c

c 3 3 3 3

<D

M -I

— 3 O)

C <g i3 -O

— ^ t. Si Si

U •-

B a.CLa.aecACACACA ta Si ^ •'- —> Si

c L. 3 > >- >- CM CM

278-2
TABLE 278-2: INDIVIDUAL DATA FOR NBS SRM 278 (revised 3/1/86)

Cone

Al (%)

Uncer Com Method Reference

7.43 0.57 ITNA 82GRA 01 1 6000 1000 TCGS 82GRA

7.55 0.08 TCGS 83AND 01 1 7000 570 ITNA 85GLA

7.55 0.08 TCGS 85AND 01 1 7080 50 WXRF 856LA

7.56 0.06 WXRF 85GLA 01 1 7100 300 TCGS 85AND

7.62 0.11 ITNA 85GLA 01 1 7100 300 TCGS 83AND

7.78 0.08 ICPES 83CR0 01 1 7200 100 ICPES 83CR0

7.8 0.2 TCGS 82GRA 01 1 7300 300 TCGS 82V0G

7500 1200 ITNA 82GRA

As (ug/g)

4.68 0.13 ITNA 81AHM 01 1 5.06 1.29 ITNA 82GRA 01 1 180 60 TCGS 85AND

5.1 0.88 ITNA 82V0G 01 1 180 60 TCGS 83AND

Au (ng/g)

1.6

2.64

B (ug/g)

Be (ug/g)

1.4

2.4

Br (ug/g)

0.8

0.52

0.1

ITNA

ITNA

OES

ICPES

82GRA 01 82V0G 01

21 OES 83MIL 01 24.1 0.4 TCGS 83AND 01 24.9 0.5 TCGS 82V0G 01 25.2 0.4 TCGS 82GRA 01 26 3 TCGS 84GLA 01 27.9 0.4 TCGS 85AND 01

600 160 WXRF 85GLA 01 885 54 ITNA 81AHM 01 928 9 ICPES 83CR0 01 1050 40 ITNA 85GLA 01 1060 40 ITNA 82V0G 01 1080 58 ITNA 82GRA 01

83MIL 01 83CR0 01

2.61 0.62 ITNA 82GRA 01 2.65 0.2 ITNA 81AHM 01 2.99 1.01 ITNA 82V0G 01

Cone

Ca (ug/g)

Uneer Com Method Referenee

Cd (ng/g)

54.4

55.8

56.5

56.5

59.4

6166.5

68

90

CI (ug/g)

610

610

627

640

Co (ug/g)

1.85

1.89

22.04

2.08

2.6

2.7

Cr (ug/g)

2

56.34

6.42

6.79

7.5

2.2

0.3

1.9

2.9

6.8

19.3

1 30

7

7

14

90

0.18

0.31

10.22

0.1

2.7

0.2

7

0.5

0.93

0.28

0.44

1.2

ITNA RTNA

ITNA

ITNA

ITNA ICPES

ITNA

ITNA WXRF

TCGS

TCGS

ISE TCGS

ITNA ITNA ICPES

ITNA

ITNA WXRF

ITNA

WXRF

ICPES

ITNA

ITNA

ITNA

ITNA

840DD 01 8400D 01 81AHM 01 80AHM 01 82GRA 01 83CR0 01 82V0G 01 85GLA 01 85GLA 01

85AND 01 83AND 01 86ELS 01 82GRA 01

82GRA 01 82V0G 01 83CR0 01 81AHM 01 85GLA 01 85GLA 01 84GLA 11

85GLA 01 83CR0 01 82GRA 01 82V0G 01 81AHM 01 86GAU 01

278-3
TABLE 278-2: INDIVIDUAL DATA FOR NBS SRM 278 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Cs (ug/g)

1

j FED (%)

4.9 ITNA S6GAU

1 01 1 1.35 TITR 84G0L 01 4.91 0.14 ITNA 84GLA 11 1 1.42 0.1 COLOR 85GLA 01 4.92 0.34 ITNA 82GRA 01 j 5.12 0.44 ITNA 81ANM 01 1 Ga (ug/g)

5.3 0.25 ITNA 82V0G 01 1 5.3 0.7 ITNA 84GLA 02 I 10 3 ITNA 82GRA 01

5.46 0.07 ITNA 85GLA 01 1 12.47 2.53 ITNA 82VOG 01 22 4 ICPES 83CR0 01 Cu (ug/g) 1

1 Gd (ug/g)

< 5 ICPES 83CR0 01 !

1 4.5 ITNA 82GRA 01 Dy (ug/g) 1 4.96 0.08 TCGS 83AND 01

1 5.28 0.06 TCGS 82VOG 01 6.2 0.1 ITNA 840DD 01 1 5.34 0.08 TCGS 82GRA 01 6,51 0.2 RTNA 84GDD 01 1 5.5 0.5 4 TCGS 85GLA 05

6.8 0.4 ICPES 83CR0 01 1 5.65 0.07 ITNA 840DD 01

1 5.7 0.03 RTNA 840DD 01 Er (ug/Q) 1 5.9 0.5 4 TCGS 85GLA 05

5.95 0.08 TCGS 85AND 01 3.66 0.07 RTNA 84000 01 1 6.1 0.3 ICPES 83CR0 01 4.1 0.3 ICPES 83CR0 01 j 37.74 1.5 ITNA 80AHH 01

1 37.74 1.5 ITNA 81AHM 01 Eu (ng/g) 1

1 H (ug/g)

764 56 ITNA 82GRA 01 1 770 30 ICPES 83CR0 01 1 530 45 TCGS 83AND 01 780 20 RTNA B40DD 01 ! 550 50 TCGS 85AND 01 790 40 ITNA 85GLA 01 1 890 120 TCGS 82V0G 01 796 9 ITNA 82VOG 01 1 820 30 ITNA 80AHM 01 1 H20+ (%)

820 30 ITNA 81AHM 01 1

-

830 20 ITNA 840DD 01 1 0.3 0.02 COUL 85GLA 01

Fe (%)

1

1 H20- (%)

1.14 0.23 ITNA 81AHM

1 01 1 0.05 0.01 COUL 85GLA 01 1.32 0.17 TCGS 82GRA 01 1 1.39 0.05 TCGS 83AND 01 1 Hf (ug/g)

1.39 0.05 TCGS 85AND 01 1 1.45 0.02 WXRF 85GLA 01 1 6.41 0.24 ITNA 81AHM 01

1 .47 0.01 ICPES 83CR0 01 1 8.6 0.2 ITNA 85GLA 01 1.52 0.05 ITNA 82GRA 01 j 8.82 0.73 ITNA 82GRA 01 1.54 0.01 ITNA 82V0G 01 j 8.86 0.73 ITNA 82V0G 01

1.55 0.04 ITNA 85GLA 01 1 1.55 0.06 TCGS 82V0G 01 1 Ho (uq/g)

FE203 (%) 1.2 0.04 RTNA 8400D 01 1.23 0.06 ITNA 840DD 01 0.49 0.11 CALC 85GLA 01 1 1.5 0.1 ICPES 83CR0 01

278-4
TABLE 278-2: INDIVIDUAL DATA FOR NBS SRH 278 (cont.)

Cone

In (ng/g)

Uncer Com Method Reference

La (ug/q)

Cone Uncer Com Method Reference

3.73

3.73

0.52

0.52

43.6 2.7 ITNA 81AHM 01 1 367 15 ITNA 82V0G

370 15 ITNA 85GLA

(%) 373 3 ICPES 83CR0

1 380 50 TCGS 83AND

3.28 0.11 ITNA 85GLA 01 1 382 52 TCGS 85ANO

3.31 0.01 TCGS 83AND 01 1 395 40 UXRF 85GLA

3.31 0.01 TCGS 85AND 01 1 400 50 ITNA 82GRA

3.34 0.03 ICPES 83CR0 01 1 409 15 ITNA 81AHM

3.4 0.01 WXRF 85GLA 01 1 430 70 TCGS 82GRA

3.42 0.34 ITNA 82GRA 01 j 3.44 0.08 TCGS 82GRA 01 1 Mo (ug/g)

3.58 0.7 TCGS 82V0G 01 1 4.23 0.13 ITNA 81AHM 01 1 2 1 ICPES 83CR0

ITNA

ITNA

82V0G 01 82GRA 01

24 6 WXRF 85GLA 01 27.59 0.38 ITNA 81AHM 01 27.6 0.4 ITNA 80AHM 01

31 0.7 ICPES 83CRO 01 33 3 nm 85GLA 01 35.4 2.5 ITNA 82GRA 01 35.8 1.5 ITNA 82V0G 01 37.6 0.8 ITNA 84000 01 37.8 0.8 RTNA 840DD 01

Li (ug/g)

47

Lu Cng/g)

Mg (ug/g)

ICPES 83CR0 01

710 10 ICPES 83CR0 01 740 50 ITNA 80AHM 01 745 310 ITNA 81AHM 01 820 39 ITNA 82V0G 01 836 50 ITNA 82GRA 01 934 2 RTMA 840DD 01 947 2 ITNA 8400D 01

< 2400 ITNA 85GLA 01 1430 20 ICPES 83CR0 01 1540 30 UXRF 85GLA 01

Na (%)

2.6

3.3

3.44

3.46

3.49

3.51

3.51

3.56

3.56

3.9

Nb (ug/g)

12.7

18.4

Nd (ug/g)

26

28.2

28.6

29.5

30

30

33.5

4

19

0.2

0.4

0.02

0.26

0,01

0.05

0.05

0.02

0.03

0.23

0.9

1.5

4

10.9

0.3

5

50.02

250

TCGS 82GRA 01 ITNA 82V0G 01 ICPES 83CR0 01 ITNA 82GRA 01 ITNA 85GAU 04

TCGS 85AND 01 TCGS 83AND 01 UXRF 85GLA 01 ITNA 85GLA 01 ITNA 81AHM 01

ICPES 83CRO 01 UXRF 84KYL 01

ITNA 85GLA 01 ITNA 82GRA 01 ICPES 83CR0 01 ITNA 84(»D 01 TCGS 83AND 01 TCGS 85AND 01 RTNA 840DD 01

ICPES 83CR0 01 UXRF 85GLA 01

278-5
TABLE 278-2: INDIVIDUAL DATA FOR NBS SRM 278 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Referenee

P (uq/g)

1

1 Sm (ug/g)

110 20 UXRF 85GLA

1 01 1 5.45 0.03 TCGS 83AND 01 170 . 10 ICPES 83CR0 01 1 5.61 0.05 TCGS 82V0G 01 5.66 0.1 TCGS 82GRA 01 Pb (uq/q) j 5.69 0.62 ITNA 82GRA 01 5.7 0.7 ITNA 82V0G 01 16.22 0.037 IDMS 86FIS 01 1 5.8 0.03 RTNA 84(X>D 01 18 3 ICPES 83CR0 01 i 5.8 0.6 4 TCGS 85GLA 05

1 5.85 0.09 ITNA 8400D 01 Pr (ug/g) i 6 0.7 ITNA 85GLA 01

1 6.08 0.03 TCGS 85AND 01 7.48 0.08 RTNA 840DD 01 1 6.2 0.6 4 TCGS 85GLA 05

8.6 0.8 icPES 83CR0 01 1 6.8 0.6 ICPES 83CR0 01

Rb (ug/g) 1 Sr (ug/q)

128.4 1 WXRF 84KYL

1 01 1 58 lENA 85GAU 04

129 7 UXRF 85GLA 01 1 60 3 ICPES 83CR0 01

130 5 ITNA 85GLA 01 1 61.8 1 WXRF 84KYL 01

130 12 ITNA 82GRA 01 1 66 6 WXRF 85GLA 01 138 10 ITNA 82VOG 01 1 143.17 2.63 ITNA 81AHM 01 1 Ta (ug/g)

Sb (ug/g)

1

1 1.23 0.16 ITNA 82VOG 01

1 1.23 0.19 ITNA 82GRA 01 1.59 0.05 ITNA 82V0G 01 I 1.32 0.18 ITNA 81AHM 01

1.61 0.13 ITNA 82GRA 01 1 1.34 0.09 ITNA 85GLA 01 1.7 0.4 ITNA 81AHM 01 1 1.8 0.1 ITNA 85GLA 01 1 Tb (ug/q)

1.9 ITNA 84GLA 02 1

1 0.8 0.02 ITNA 85GLA 01

Sc (uq/q) 1 1.11 0.1 ITNA 840DD 01

1 1.12 0.22 ITNA 82V0G 01 4.16 0.21 ITNA 81AHM 01 1 1.14 0.1 ITNA 82GRA 01

5 0.03 ITNA 86GAU 01 1 1.23 0.03 ITNA 81AHM 01

5 0.1 ITNA 84GLA 02 1 1.23 0.08 ITNA 80AHM 01

5.1 0.07 ITNA 84GLA 11 1 1.81 0.03 RTNA 840DD 01 5.24 0.14 ITNA 82GRA 01 1 5.3 0.1 ITNA 85GLA 01 1 Th (uq/g)

5.31 0.05 ITNA 82V0G 01 1 6 0.5 ICPES 83CR0 01 1 12.27 0.77 ITNA 81AHM 01 12.27 0.77 ITNA 80CHA 02

Si (%) 12.7 0.4 ITNA 866AU 01 12.8 0.3 ITNA 82GRA 01

33.1 0.3 TCGS 85AND 01 1 13 3 ICPES 83CR0 01

33.1 0.3 TCGS 83AND 01 I 13.1 0.2 ITNA 82VOG 01

33.2 0.7 TCGS 82VOG 01 1 13.2 0.4 ITNA 85GLA 01

34.25 0.14 WXRF 85GLA 01 1 36.6 1.3 TCGS 82GRA 01 1

278-6
Cone

TABLE 278-2: INDIVIDUAL DATA FOR NBS SRM 278 (cont.)

Uncer Com Method Reference | Cone Uncer Com Method Reference

Ti (ug/g)

1330

1330

1420

1450

1480

1500

Tm (ng/g)

301

330

400

500

4.204

4.21

4.51

4.51

4.51

4.51

4.53

4.58

4.82

4.96

V (ug/g)

8

12

24

38.3

4144.5

Yb (ug/g)

3.58

3.58

4.54

4.68

4.79

4.8

5.04

5.09

60 TCGS 85AND

60 TCGS 83AND

30 WXRF 85GLA

90 TCGS 82GRA

10 ICPES 83CR0

40 TCGS 82V0G

20 ITNA 81AHM

30 RTNA 8400D

20 ITNA 840DD

100 ICPES 83CR0

01 I 47.8

01 I 54

01 I 57

01 I 57.4

01 I 01 I Zr (ug/g)

I 285

I 288.8

01 I 290

01 I 302

01 I 311

01 I

0.4 ICPES 83CR0 01

2.5 ITNA 82GRA 01

7 UXRF 8SGLA 01

3.6 ITNA 82V0G 01

16 ITNA 82GRA 01

2 UXRF 84KYL 01

2 ICPES 83CR0 01

9 WXRF 85GLA 01

50 ITNA 82V0G 01

0.284 ITNA 81AHM 01 0.12 FLUOR 86KAN 01 0.005 IDMS 86FIS 01 0.05 DNA 85GLA 04

0.08 DNA 85GLA 01 0.08 DNA 85GAU 04

0.12 DNA 86GAU 01 DNA 84GLA 02

0.35 ITNA 82GRA 01 0.33 ITNA 82VOG 01

1 ICPES 83CR0 01 4 ITNA 85GLA 01

4 UXRF 85GLA 01

4 ICPES 83CR0 01

2 UXRF 85GLA 01

1 UXRF 84KYL 01

0.25 ITNA 80AHH 01 0.25 ITNA 81AHM 01 0.86 ITNA 82GRA 01 0.05 ICPES 83CR0 01 0.04 ITNA 84000 01 0.2 ITNA 85GLA 01 0.08 RTNA 840DD 01 0.95 ITNA 82V0G 01

278-7
TABLE 330-1: COMPILED DATA ON NBS SRM 330 COPPER ORE, MILL HEADS (revised 3/1/86)

ELEMENT UNITS NBS

Ag ug/g 1.51

Au ng/g 93

Cu ug/g 8400 ± 100

Mo ug/g 180 ± 10

Re ng/g 300 i 60

TABLE 331-1: COMPILED DATA ON NBS SRM 331 COPPER ORE, MILL TAILS (revised 3/1/86)

ELEMENT UNITS NBS

'

Ag ng/g 243

Au ng/g 34

Cu ug/g 910 ± 10

Mo ug/g 22 ± 2 Re ng/g 40 ± 20

TABLE 332-1: COMPILED DATA ON NBS SRM 332 COPPER CONCENTRATE (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Ag ug/g 38.7

Au ug/g 2.14 --- —

Cu % 28.4 ± 0.1

Mo ug/g 6400 ± 100

Re ug/g 10.2 ± 0.2 10.2 (1) PROBE

TABLE 332-2: INDIVIDUAL DATA FOR NBS SRM 332 (revised 3/1/86)

Cone Uncer Com Method Reference

Re (ug/g)

10.2 1.8 PROBE 85HAS 01

TABLE 333-1: COMPILED DATA ON NBS SRM 333 MOLYBDENUM CONCENTRATE (revised 3/1/86)

ELEMENT UNITS NBS

Ag ug/g 25

Au ug/g 8.9

Cu % 1.038 ± 0.01

Mo % 55.3 ± 0.1

Re ug/g 870 ± 10

330-1
TABLE 610-1: COMPILED DATA FOR NBS SRM 610 TRACE ELEMENTS IN GLASS (revised 3/1/86)

ELEMENT UNITS NBS Mean t SO

CONSENSUS Mean ± SD (n)

Ag ug/g 254 ± 10 180 (1) As ug/g 305 (1) Au ug/g 25 20 (1)

B ug/g 351 357 t 9 (5)

B ug/g ...

B-10 atom X 19.827 (1) Ba ug/g 638 (1) Be ug/g 450 (1)

Bi ug/g 405 (1) Ca X 8.6 7.64 (1)

Cd ug/g 187 (1) Ce ug/g 318 <1) Co ug/g 390 389 t 22 (9) Co ug/g — —

Cr ug/g — 410 i 60 (9) Cr ug/g — —

Cu ug/g 444 t 4 380 1 100 (8) Fe ug/g 458 ± 9 460 (1) Ga ug/g — 481 (1) Ge ug/g — 496 (1)

Hf ug/g — 220 (1)

In ug/g ... 319 (1)

K ug/g 461 —

Li ug/g — 354 (1)

Hg ug/g — 472 (1) Mn ug/g 485 1 10 480 ± 50 (9) Mn ug/g ... —

Mo ug/g ... 307 (1)

Ni ug/g 458.7 ± 4 480 ± 50 (8)

Ni ug/g ... —

Ni ug/g ... —

Pb ug/g 426 t 1 418 t 17 (4)

Pb ug/g ... ...

Rb ug/g 425.7 t 0.8 425.7 (1)

Sb ug/g — 387 (1)

Sr U9/9 515.5 t 0.5 515.5 (1) Ta ug/g — 206 (1) Te ug/g — 259 (1) Th ug/g 457.2 ± 1.2 460 ± 7 (3) Th ug/g — —

Ti ug/g 437 490 t 70 (10)

Ti ug/g — —

Ti ug/g —

TI ug/g 61.8 ± 2.5 57 (2)

TI ug/g —

U ug/g 461.5 t 1.1 453 t 22 (7) U ug/g

U ug/g

U ug/g

U-234 atom X 0.0010 (1)

U-235 atom X 0.2376 0.2376 (2)

U- 235/238 ratio 0.0024 0.0025 ± 0.0001 (4)

U-236 atom X 0.0043 (1)

U-238 atom X 99.7571 (1)

V ug/g 490 ± 60 (8) Zn ug/g 433 500 ± 140 (6)

MEDIAN RANGE METHOD MEANS Mean ± SD (n) Method

— 180 (1) NAA — -- 305 (1) SSMS — — 20 (1) NAA 358 348 - 368 356 ± 8 (3) TCGS — -- 358 (2) ICPES — -- 19.827 (1) IDMS

... -- 638 (1) SSMS — -- 450 (1) CPAA — -- 405 (1) SSMS 7.64 (1) SSMS

;; 187 (1

)

SSMS

... -- 318 (1) SSMS 390 360 - 420 391 ± 23 (8) PROSE

375 (1) SSMS 380 340 - 510 420 t 60 (8) PROBE

... 371 (1) SSMS 360 230 - 510 380 ± 100 (8) PROBE

... 460 (1) POL

... 481 (1) SSMS

... 496 (1) SSMS

* • . " 220 (1) SSMS

... 319 (1) SSMS

...

354 (1) CPAA 472 (1) SSMS 490 391 - 550 495 t 40 (8) PROBE

391 (1) SSMS 307 (1) SSMS 470 431 - 550 490 ± 50 (6) PROBE 450 (1

)

POL

... 431 (1) SSMS 425.58 392 - 427 426.2 ± 0.7 (3) IDMS 392 (1) SSMS 425.7 (1) IDMS 387 (1) SSMS 515.5 (1

)

IDMS 206 (1) SSMS

... "" 259 (1) SSMS 457.23 455.4 - 469 456.3 (2) IDMS

... - 469 (1) SSMS 530 361 - 560 520 ± 50 (8) PROBE

... 434 (1) POL

... 361 (1) SSMS

52 - 61.8 52 (1) SSMS 61.8 (1) IDMS 461.5 413 - 471 457 ± 23 (3) NAA 461.4 (2) IDMS 413 (1) SSMS 462.8 (1) NT 0.0010 (1) IDMS 0.2376 - 0.2376 0.2376 (2) IDMS 0.0024 0.0023 - 0.0026 0.0025 ± 0.0001 (4) NAA 0.0043 (1) IDMS 99.7571 (1) IDMS 460 410 - 560 490 ± 60 (8) PROBE 500 320 - 650 500 ± 140 (6) PROBE

610-1
TABLE 610-2: INDIVIDUAL DATA FOR NBS SRM 610 (revised 3/1/86)

Cone Uncer Com Method Reference |

1

Cone Uneer Com Method Reference

Ag (ug/g)

1

1

1

Co (ug/q)

180 80 ITNA 73SHE 01 1 135 14 ITNA 73SHE 01

1 360 60 6 PROBE 71 HE I 02

As (ug/g) 1 360 90 6 PROBE 71HEI 02

1 375 12 SSMS 74BER 01 305 20 SSMS 74BER 01 1 390 90 6 PROBE 71 HE I 02

1 390 100 6 PROBE 71 HE I 02

Au (ug/g) 1 390 110 6 PROBE 71 HE I 02

1 400 130 6 PROBE 71 HE I 02

20 2 ITNA 73SHE 01 1 420 140 6 PROBE 71 HE I 02

1 420 180 6 PROBE 71 HE I 02

B (ug/g) 1

1 Cr (ug/g)

348 13.6 ICPES 85ZAC 01 1 348 20 6 TCGS 76GLA 01 1 340 40 6 PROBE 71 HE I 02

358 15 6 TCGS 76GLA 01 1 360 40 6 PROBE 71 HE I 02

363 17 6 TCGS 76GLA 01 I 370 100 6 PROBE 71 HE I 02

368 12 ICPES 820WE 01 1 371 15 SSMS 74BER 01

1 380 140 6 PROBE 71 HE I 02

B-10 (atom %) 1 440 40 6 PROBE 71 HE I 02

1 440 90 6 PROBE 71 HE I 02

19.827 IDMS 72CAR 01 I 500 120 6 PROBE 71 HE I 02

1 510 60 6 PROBE 71 HE I 02

Ba (ug/g) 1

1 Cu (ug/q)

638 24 SSMS 74BER 01 1

1 230 210 6 PROBE 71 HE I 02

Be (ug/q) 270 150 6 PROBE 71 HE! 02

350 200 6 PROBE 71 HE I 02

450 50 CPAA 82LAS 01 1 360 130 6 PROBE 71 HE! 02

420 200 6 PROBE 71 HE I 02

Bi (ug/g) 440 250 6 PROBE 71 HE I 02

500 100 6 PROBE 71 HE I 02

405 18 SSMS 74BER 01 1 510 110 6 PROBE 71 HE I 02

Ca (%) 1 Fe (ug/q)

7.64 0.002 SSMS 74BER 01 1 460 10 POL 73MAI 01

Cd (uq/g) 1 Ga (uq/q)

187 21 SSMS 74BER 01 1 481 10 SSMS 74BER 01

Ce (ug/q) Ge (uq/q)

318 14 SSMS 74BER 01 1 496 10 SSMS 74BER 01

Hf Cug/g)

220 14 SSMS 74BER 01

610-2
TABLE 610-2: INDIVIDUAL DATA FOR NBS SRM 610 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

In (uq/q) I Sb <ufl/3)

319 11 SSMS 74BER 01 1 387 18 SSMS 74BER 01

Li (uq/q) 1 Sr (uq/q)

354 27 CPAA 82LAS 01 1 515.5 0.3 IDMS 73MOO 01

Mg (uq/g)

1

1

1

Ta (ug/g)

472 22 SSMS 74BER 01 1 206 9 SSMS 74BER 01

Mn (uq/q)

1

1 Te (uq/q)

391 7 SSMS 74BER

1 01 1 259 21 SSMS 74BER 01 440 90 6 PROBE f 1 Hb 1 450 90 6 PROBE 71 HE I 02 1 Th (ug/g)

480 100 6 PROBE 71 HE I 02 1 490 40 6 PROBE 71 HE I 02 1 455.4 1.6 17 IDMS 73BAR 01 490 70 6 PROBE 71 HE I 02 1 457.23 0.52 17 IDMS 73BAR 01 530 70 6 PROBE 71 HE I 02 1 469 7 SSMS 74BER 01 530 80 6 PROBE 71 HE I 02 1 550 100 6 PROBE 71HEI 02 1 Ti (ug/g)

Mo (ug/g)

1

1 361 18 SSMS 74BER 01

1 430 50 6 PROBE 71 HE I 02

307 19 SSMS 74BER 01 1 434 10 POL 73MAI 01

1 440 30 6 PROBE 71 HE I 02

Ni (ug/g) 1 530 80 6 PROBE 71 HE I 02

1 540 70 6 PROBE 71 HE I 02

431 10 SSMS 74BER 01 1 540 80 6 PROBE 71HEI 02

440 50 6 PROBE 71HE1 02 1 550 70 6 PROBE 71HEI 02

450 7 POL 73MAI 01 1 550 100 6 PROBE 71 HE I 02

450 50 6 PROBE 71 HE I 02 1 560 110 6 PROBE 71 HE I 02

470 70 6 PROBE 71 HE I 02 1 480 80 6 PROBE 71 HE I 02 1 Tl (uq/q)

550 140 6 PROBE 71 HE I 02 1 550 180 6 PROBE 71HEI 02 1 52 35 SSMS 74BER 01 940 420 6 PROBE 71 HE I 02 1 61.8 1 IDMS 73BAR 01 950 220 6 PROBE 71 HE I 02 1

1 U (ug/g)

Pb (ug/q)

1

1 413 18 SSMS 748ER 01 392 11 SSMS 74BER 01 1 430 DNA 84GLA 02

425.58 0.4 17 IDMS 73BAR 01 1 461.3 1 17 IDMS 73BAR 01 426.15 0.41 17 IDMS 73BAR 01 1 461.3 1.7 D IDMS 72CAR 01 427 1 IDMS 83BR0 01 1 461.5 0.4 17 IDMS 73BAR 01 461.5 1.1 D IDMS 72CAR 01 Rb (ug/q) 462.8 13.8 NT 72CAR 01 470 90 17 DNA 82CON 01 425.7 0.7 IDMS 73MOO 01 1 471 28 17 DNA 82CON 01

610-3
TABLE 610-2: INDIVIDUAL DATA FOR NBS SRH 610 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

U-234 (atom %)

1

1

1

V (ug/q)

0.001 IDMS 73BAR 01 j 206 10 SSMS 74BER 01

1 410 70 6 PROBE 71 HE I 02

U-235 (atom %) 1 430 70 6 PROBE 71 HE I 02

1 450 100 6 PROBE 71 HE I 02

0.2376 IDMS 73BAR 01 1 460 40 6 PROBE 71 HE I 02

0.2376 0.0004 IDMS 72CAR 01 1 500 80 6 PROBE 71 HE I 02

1 530 70 6 PROBE 71 HE! 02

U- 235/238 (ratio) 1 550 70 6 PROBE 71 HE I 02

1 560 110 6 PROBE 71 HE I 02

0.0023 RTNA 86GAU 01 1 0.0024 0.0001 RTNA 856AU 04 1 Zn (uq/ci>

0.0025 0.0001 RTNA 84GLA 02 1 0.0026 0.0001 RTNA 84GLA 11 1 320 130 6 PROBE 71 HE I 02

320 150 6 PROBE 71HEI 02

U-236 (atom %) 500 140 6 PROBE 71 HE I 02

590 170 6 PROBE 71 HE I 02

0.0043 IDMS 73BAR 01 1 600 190 6 PROBE 71 HE I 02

650 140 6 PROBE 71 HE I 02

U-238 (atom %)

99.7571 IDMS 73BAR 01

610-4
TABLE 612-1: COMPILED DATA FOR NBS SRM 612 TRACE ELEMENTS IN GLASS (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE NAA OTHER METHODS Mean ± SO Mean ± SD (n) Mean ± SD (n) Mean ± SD (n) Method

U9/g 22 t 0.3 26 (2) 20 31 31 (1) 20 <1) AA

Al X 1.1 1.11 (1) 1.11 (1) As ua/Q 47 (2) 35.6 58.1 58.1 (1) 35.6 (1

)

PAA Au ua/a 5 5.09 t 0.16 (3) 5 5 5.27 5.09 ± 0. 16 (3)

B ua/a 32 33 ± 5 (4) 31 27.8 40 33.9 (2) ICPES

B 31 ( 1

)

TCGS

B 32.39 (1) NT B-10 atom % 19.827 (1) 19.827 (1) lOMS 8a 41 36.5 f 1) 36.5 (1

1

Be ua/a 31 (1) 31 f 1 1 CPAA

Br ua/a < 1.4 < 1 .4 Ca X 8.6 8.72 (2) 8.65 8.79 8.79 f 11 8.65 ( 1

1

PAA Ce ua/a 39 41 t 3 (4) 40.6 37 45.3 41.15 (2) 40.6 1 1

1

PAA Co ua/a 35.5 ± 1.2 35 ± 3 (5) 34.3 31 37.47 35 t 3 (4) 33.3 ( 1

)

PAA

Cr ug/g 110 (2) 65.9 155 110 (2) Cs ug/g ... 43 1 2 (3) 43 41.1 44.8 42.0 (2) 44.8 (1) PAA Cu ug/g 37.7 ± 0.9 37 (1) 37 (1)

Oy ug/g 35 37 (1) 37 (1) Er ug/g 39 ...

•

Eu ug/g 36 31 ± 5 (3) 32.86 26 35.3 31 ± 5 (3) Fe ug/g 51 t 2 56 (2) 51.3 60 60 (1) 51.3 (1

)

POL Gd ug/g 39 37 (2) 36 38 37 (2) TCGS

Hf ug/g 42 (2) 32.2 52.29 42.2 (2) K us/g 64 ...

La ug/g 36 38 (2) 35 40.2 37.6 (2)

Li ug/g 44 (1) .... 44 (1) CPAA

Lu ug/g ... 36.8 (1) ... 36.8 (1)

Mg ug/g . • - 341 (1) ... 341 <1) PAA Hn ug/g 39.6 ± 0.8 38.6 (2) ... 38.2 39 38.2 (1) 39 <1) PAA

Na X 10.4 10.6 (2) • . . 10.5 10.68 10.68 (1) 10.5 (1) PAA Nb ug/g ... 38.1 (1) ... 38.1 (1) PAA Nd ug/g 36 ... ... ...

Ni ug/g 38.8 ± 0.2 40.1 (1) ... ... 40.1 (1) PAA Pb ug/g 38.57 1 0.2 38.58 ± 0.16 (5) 38.56 38.37 38.83 ... 38.6 ± 0.2 (5) IDMS Pb ug/g - . - ... _ ... 36.3 (1) AA Rb ug/g 31.4 i 0.4 32 t 2 (5) 31.7 31.41 36 36 (1) 32 (1) PAA Rb ug/g ... ... 31.425 (2) IDMS Sb ug/g ... 39 t 6 (3) 39.4 32.2 45.2 38.7 (2) 39.4 (1) PAA

Sc ug/g ... 38 t 3 (3) 38.2 34 40.35 37.2 (2) 38.2 (1) PAA

Si X 33.6 34.04 (1) 34.04 (1)

Srn ug/g 39 35 t 4 (3) 32.8 32.7 39.6 39.6 (1) 32.75 <2) TCGS

Sr ug/g 78.4 t 0.2 77.6 t 1.0 (4) 77.3 76.3 78.38 77.3 (1) PAA

Sr ug/g — — ... ... 78.345 (2) IDMS Sr -87/86 ratio — 0.70907 (1) — 0.70907 (1) IDMS Ta ug/g- ... 44 (2) — 36.33 52.7 44.5 (2) ... Tb ug/g — 37 (2) — 22 52.96 37.5 (2) ...

Th ug/g 37.79 ± 0.08 36 t 3 (5) 37.55 31 38.43 35 t 4 (3) 37.67 (2) IDMS

Ti ug/g 50.1 t 0.8 53 (2) 50 55.2 ... 55.2 (1) PAA

Ti ug/g 50 (1) POL

Tl ug/g 15.7 t 0.3 15.7 (1) 15.68 (1) IDMS U ug/g 37.38 ±0.08 37.5 t 1.3 (9) 37.37 35.74 40 40 t 3 (4) 37.4 ± 0.1 (4) IDMS U ug/g 36.32 (2) NT U-235 atom X 0.2392 0.2392 (1) 0.2392 (1) IDMS U-235/238 ratio 0.0023 (1) 0.00229 (1) V ug/g 58.6 (1) 58.6 (1)

Y ug/g 37.9 (1) 37.9 (1) PAA Yb ug/g 42 48 (2) 40 55 47.5 (2) Zr ug/g 41.8 (1) 41.1 (1) PAA

612-1
TABLE 612-2: INDIVIDUAL DATA FOR NBS SRM 612 (revised 3/1/86)

Cone

Ag (ug/g)

Uncer Com Method Reference

1.1109

As (ug/g)

35.6

58.1

Au (ug/g)

B (ug/g)

B-10 (atom %)

19.827

Ba (ug/g)

36.5

Be (ug/g)

31

Br (ug/g)

<

Ca (%)

20 1 FAA 8AHEA 01 1 31 1 ITNA 73SHE 01

31 7 ITNA 73SHE 01 1 33.3 1 PAA 80KAN 01 34.3 2.9 ITNA 84KUL 01

(%) 37.1 2.3 6 ITNA 73KIM 01 37.47 4.1 6 ITNA 73KIM 01 0.0212

0.3

7.3

5.2

1.4

ITNA

PAA

ITNA

85PEN 01

80KAN 01 84KUL 01

5 0.2 ITNA 84KUL 01 1 43 2 ITNA 84KUL

5 1 ITNA 73SHE 01 1 44.8 1.2 PAA 80KAN

5.27 0.11 ITNA 73KIM 01 1

ITNA 84KUL 01

CPAA

ITNA

82LAS 01

84KUL 01

Cone Uncer Com Method Reference

Cr (ug/g)

65.9

155

Cs (ug/g)

41.1

3.7

8

6.6

ITNA

ITNA

ITNA

Cu (ug/g)

37 ITNA

(ug/g)

Fe (ug/g)

51.3

60

Gd (ug/g)

36

38

Hf (ug/g)

0.8

7

4

4

4

4

POL

ITNA

TCGS

TCGS

84KUL 01 73KIM 01

73KIM 01

84KUL 01 27.8 2.9 ICPES 85ZAC 01 1 31 3 TCGS 84GLA 01 1 Dy (ug/g)

32.39 1.04 NT 72CAR 01 1 40 4 ICPES 820WE 01 1 37 4 ITNA 84KUL

IDMS 72CAR 01 1 26 1 ITNA 73SHE 01 32.86 2.19 ITNA 73KIM 01 35.3 1.2 ITNA 84KUL 01

73MAI 01 84KUL 01

85GLA 05

85GLA 05

8.65 0.14 PAA 80KAN 01 1 32.2 1.6 ITNA 84KUL

8.79 0.72 ITNA 84KUL 01 1 52.29 3.11 ITNA 73KIM

(ug/g) La (ug/g)

37 2 ITNA 73SHE 01 1 35 15 ITNA 73SHE

40.6 0.2 PAA 80KAN 01 1 40.2 1.2 ITNA 84KUL

41.2 UU 77HAN 02 1 45.3 1.5 ITNA 84KUL 01 1

612-2
TABLE 612-2: INDIVIDUAL DATA FOR NBS SRM 612 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Li (ug/q) So (uq/g)

44 8 CPAA 82LAS 01 1 34 3 ITNA 84KUL 01 38.2 1.2 PAA 80KAN 01 Lu fug/a) 40.35 0.35 ITNA 73KIM 01

36.8 0.2 ITNA 84KUL 01 1 Si (%)

Mg (ug/q)

1

]

34.04 0.65 ITNA 85PEN 01

< 2412 ITNA 85PEN 01 1 Sm (ug/g)

341 16 PAA 80ICAN A 4 1 01 1 32.7 3 4 TCGS 85GLA 05

Mn (ug/g) 32.8 3 4 TCGS 85GLA 05

] 39.6 1.1 ITNA 84KUL 01 38.2 1.1 ITNA 84ICUL 01 1 39 2.6 PAA 80KAN 01 i

Na (X) ] 76.3 UU 77HAN 02

77.3 1.3 PAA 80KAN 01 10.5 0.15 PAA 80KAN 01 1 78.31 0.09 IDMS 83LIP 01 10.68 0.59 ITNA 84KUL 01 1 78.38 0.25 IDMS 73MOO 01

Nb (ug/g)

1

Sr-87/86 (ratio)

38.1 1 PAA ni 1 709.07 0.1 28 IDMS 83LIP 01

Mi (uq/q) Ta (ug/g)

40.1 1.1 PAA 80KAN ni 9 01 1 36.33 5.6 ITNA 73KIM 01 52.7 0.3 ITNA 84KUL 01 Pb (ug/g>

1 Tb (ug/g)

36.3 1.5 FAA oAHcA m 1 Ul 1 38.37 0.13 IDMS 86FIS 01 1 22 2 ITNA 84KUL 01 38.56 0.07 17 IDMS 73BAR A4 1 01 1 52.96 5.62 ITNA 73KIM 01 38.56 0.11 IDMS 7701)L A 4 1 01 1 38.57 0.09 17 IDMS 73BAR 01 1 Th (ug/g)

38.83 0.04 IDMS 83BR0 01 1 31 1 ITNA 73SHE 01 Rb fuq/q) 36 2 ITNA 84KUL 01 37.55 0.04 17 IDMS 73BAR 01 31.41 0.08 IDMS 83LIP 01 1 37.79 0.017 17 IDMS 73BAR 01 31.44 0.31 IDMS 73M00 A4 1 01 1 38.43 0.42 ITNA 73KIM 01 31.7 UU 77HAN 02 1 32 1.4 PAA BOKAN 01 1 Ti (ug/g)

36 4 ITNA 84KUL 01 1 50 0.3 POL 73MAI 01 Sb (uq/q) 55,2 8.3 PAA 80KAN 01

32.2 1.6 ITNA 84KUL 01 1 Tl (ug/g)

39.4 0.3 PAA 80KAN 01 1 45.2 6.74 ITNA 73KIM 01 1 15.68 0.1 IDMS 73BAR 01

612-3
TABLE 612-2: INDIVIDUAL DATA FOR NBS SRH 612 (cont.)

Cone Uncer Com Method Reference j Cone Uncer Com Method Reference

U <ug/g) U-235/238 (atom %)

35.74 NT 1 0.00229 0.00011 RTNA 84GLA 02

36.3 7.2 17 DNA R?rnM 01 ! 36.9 1.8 NT f bOnn ni 1 V (ug/a)

37.37 0.015 17 IDMS 01 1 37.37 0.064 IDMS 86FIS 01 1 58.6 6 ITNA 84iaJL 01 37.39 0.09 D IDHS 72CAR 01 j 37.41 0.09 17 IDMS 73BAR 01 1 Y (ug/g)

37.41 0.21 D IDMS 72CAR 01 1 37.66 0.08 IDMS 77n IS f r uUL U 1

1 37.9 1.4 PAA 80KAN 01 39 4.9 17 DNA 82C0N 01 1 40 DNA 84GLA 02 j Yb (ug/g)

43.6 1.6 ITNA 84KUL 01 1 40 3 ITNA 84KUL 01 U-235 (atom %) 55 7.15 ITNA 73KIM 01

0.2392 0.0004 IDMS 72CAR 01 1 Zr tug/Q)

41.8 1.1 PAA 80KAN 01

612-4
TABLE 614-1: COMPILED DATA FOR NBS SRM 614 TRACE ELEMENTS IN GLASS (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

CONSENSUS

Mean ± SD Cn)

Ag ug/g 0.42 1 0.04 0.52 (2)

Ag ug/g — —

Au ng/g 500 580 i 300 (4)

Au ug/g — ...

B ug/g 1 .3 ± 0.2 1.14 (2)

B ug/g ... ...

B-10 atom % — 19.827 (1) Br ug/g — < 1 Ca % 8.6 7.92 <1)

Cd ng/g 550 —

Ce ug/g — 1.24 (1)

Co ug/g 0.73 ± 0.02 1.2 ± 0.5 (4)

Cr ug/g — 1.81 (1)

Cs ng/g --- 720 (2)

Cu ug/g 1.37 ± 0.07 1.61 (1)

Dy ug/g — 1.4 <1)

Eu ug/g 0.99 ± 0.04 0.85 * 0.28 (3)

Fe ug/g 13.3 ± 1 13.8 ± 1.0 (3) Fe ug/g — —

Fe ug/g — —

Ga ug/g 1.3 —

Gd ug/g — 0.75 (2)

Hf ug/g — 0.88 (2)

K ug/g 30 ± 1 —

La ng/g 830 t 20 680 (1) Lu ng/g ... 630 (1)

Mn ug/g — < 3.8

Na % 10.4 10.39 (1)

Ni ug/g 0.95 0.95 (1)

Pb ug/g 2.32 ± 0.04 2.30 ± 0.06 (4)

Pb ug/g — —

Rb ug/g 0.855 ± 0.005 0.89 (2)

Rb ug/g — —

Sb ug/g 1.06 1.03 ± 0.10 (3)

Sc ng/g 590 ± 40 720 i 100 (3)

Sm ug/g — 0.75 ± 0.12 (3)

Sm ug/g — —

Sr ug/g 45.8 ± 0.1 45.82 (1) Ta ug/g — 0.97 (2)

Tb ng/g — 560 (2)

Th ng/g 748 ± 6 744 ± 9 (4)

Th ug/g — —

Ti ug/g 3.1 ± 0,3 3.1 (1)

Tl ng/g 269 ± 5 280 (2)

Tl ug/g — —

U ug/g 0.823 ± 0.002 0.82 1 0.04 (6) U ug/g — —

U ug/g

U-235 atom % 0.2792 0.2792 (1)

V ug/g < 13

Yb ug/g 1.06 (2)

MEDIAN RANGE METHOD MEANS

Mean ± SD (n> Method

" " " 0.471 0.57 0.57 (1) NAA

0.471 (1) AA 510 280 - 1000 690 ± 270 (3) NAA — - 280 (1) AA — 0.99 - 1.29 0.99 (1) TCGS

... - 1.29 (1) NT — - 19.827 (1) IDMS — - < 1 NAA ——

- 7.92 (1) NAA —

-

- —

1.24 (1) NAA 0.85 0.59 1.66 1.2 ± 0.5 (4) NAA

1 .81 (1) NAA

... 590 - 860 725 <2) NAA

~ ~ ~ 1.61 (1) AA

1 .4 (1) NAA

0.91 0.54 - 1.10 0.85 ± 0.28 (3) NAA

13.5 13 - 15 15 (1) NAA — - 13 (1) AA —

—

- 13.5 (1) POL — 0.70

-

- 0.80 —

0.75 (2) TCGS —

—

0.55 -

-

1.2 0.88 (2) NAA

... - —

680 (1) NAA

... - 630 (1) NAA

... - < 3.8 NAA

... - 10.39 (1) NAA

... - 0.95 (1) POL

2.32 2.22 - 2.35 2.33 ± 0.02 (3) IDMS

... * 2.22 (1) AA — 0.855 - 0.92 0.92 (1) NAA — - 0.855 (1) IDMS

1.08 0.91 - 1.10 1.03 ± 0.10 (3) NAA 680 640 - 840 720 ± 100 <3> NAA

0.69 0.68 - 0.89 0.89 (1) NAA — -• 0.68 (2) TCGS — - 45.82 (1) IDMS — 0.96 - 0.98 0.97 (2) NAA — 510 - 620 565 (2) NAA 746 730 - 750 740 (2) NAA

- - - 747.5 (2) IDMS

- - - - 3.1 (1) POL

269 290 290 (1) NAA 269 (1) IDMS

1.8230 0.74 0.87 0.87 (1) NAA

0.822 ± 0.005 (3) IDMS

0.7835 (2) NT 0.2792 (1) IDMS

< 13 NAA 0.74 1.38 1.06 (2) NAA

614-1
TABLE 614-2: INDIVIDUAL DATA FOR NBS SRM 6U (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Aq (uq/g) 1 Cu (ug/q) —

0.A71 0.06 FAA 82JEN 02 1 < 9 ITNA 84KUL 01

0.57 0.07 ITNA 73SHE ni 1 U1 1 1.61 0.32 FAA 82JEN 02

Au (ng/g)

]

Dv (uq/q)

280 140 FAA oZJEN no 1

1 1.4 0.3 ITNA 84KUL 01

510 20 ITNA O/ V\ II m 1 U 1

1 550 50 ITNA U 1

1

• Eu (uq/q)

1000 800 ITNA roSHE U1 1 0.54 0.05 ITNA 73KIM 01

B (ucj/g) 0.91 0.07 ITNA 84KUL 01

1.1 0.6 ITNA 73SHE 01

0.99 0.32 TOGS OHbLA U 1

1 1.29 0.05 NT ni \ U 1

1 Fe (uq/g)

2.5 1.7 6 TCGS 76GLA 01 1 2.6 1.5 6 TCGS 76GLA 01 1 13 FAA 84HEA 01

2.9 1.5 6 TCGS 76GLA 01 1 13.5 0.7 POL 73MAI 01

15 2 ITNA 84KUL 01

B-10 (atom %) ] Gd (uq/q)

19.827 IDMS 72CAR n 4 1 01 1 0.7 0.4 4 TCGS 85GLA 05

Br (ug/g) 0.8 0.2 4 TCGS 85GLA 05

< 1 ITNA UH^UL ni 1 Hf (uq/q)

Ca (%) I 0.55 0.06 ITNA 84KUL 01

1.2 0.18 ITNA 73KIM 01

7.92 0.78 ITNA 84KUL 01 1

1 La (nq/q)

Ce (uo/a)

< 2000 ITNA 73SHE 01

1.24 0.09 ITNA Q/ }^\ il u 1

1 680 120 ITNA 84iajL 01

Co (ug/g) Lu (nq/g)

0.59 0.1 ITNA ( Oont ni 1 630 80 ITNA 84KUL 01

0.85 0.09 ITNA 84KUL 01 1 1.63 0.09 ITNA 73k I

M

ni 1 01 1 Mn (uq/q)

1.66 0.17 ITNA 01 1

< 3.8 ITNA 84KUL 01

Cr (ug/g)

Na (%)

1.81 0.2 ITNA 73KIM 01 1 10.39 0.22 ITNA 84KUL 01

Cs (nq/g)

Ni (uq/g)

590 50 ITNA 73KIM 01 1 860 30 ITNA 84KUL 01 1 0.95 0.08 POL 73MAI 01

614-2
TABLE 614-2: INDIVIDUAL DATA FOR NBS SRM 614 (cont.)

Cone Uncer Com Method Reference

0.855

0.92

Sb (ug/g)

Sc (ng/g)

640

680

840

Sm (ug/g)

Sr (ug/g)

45.82

Ta (ug/g)

0.96

0.98

Tb (ng/g)

510

620

2.22 FAA 84HEA 01 2.32 0.016 17 IDMS 73BAR 01 2.33 0.006 17 IDMS 73BAR 01 2.35 0.005 IDMS 86FIS 01

0.005

0.11

IDMS

ITNA

73MOO 01 84KUL 01

20

230

10

ITNA 84KUL 01 ITNA 73SHE 01 ITNA 73KIM 01

0.09

0.05

0.04

40

60

IDMS

ITNA

ITNA

ITNA

ITNA

0.68 0.1 4 TCGS 85GLA 05

0.69 0.1 4 TOGS 85GLA 05

0.89 0.06 ITNA 84KUL 01

73M00 01

84KUL 01 73KIM 01

84KUL 01 73KIM 01

Cone

Th (ng/g)

580

730

746

749

750

Ti (ug/g)

3.1

(ng/g)

Uneer Com Method Reference

150

90

3

2

10

17

17

ITNA

ITNA

IDMS

IDMS ITNA

0.2 POL

u (ug/g?

73SHE 01 84KUL 01 73BAR 01 73BAR 01 73KIM 01

73MAI 01

0.91 0.01 ITNA 84KUL 01 1 269 1 IDMS 73BAR

1.08 0.11 ITNA 73KIM 01 1 290 50 RTNA 82C0H

1.1 0.1 ITNA 73SHE 01 1

0.74 NT 80V I

R

01 0.817 0.009 IDMS 86FIS 01 0.823 0.0007 17 IDMS 73BAR 01 0.823 0.002 D IDMS 72CAR 01 0.827 0.0025 17 IDMS 73BAR 01 0.827 0.007 NT 72CAR 01 0.828 0.05 D IDMS 72CAR 01 0.87 0.14 ITNA 84KUL 01

U-235 (atom %)

0.2792 0.0004 IDMS 72CAR 01

V (ug/g)

< 13 ITNA 84KUL 01

Yb (ug/g)

0.74 0.06 ITNA 84KUL 01 1.38 0.01 ITNA 73KIM 01

614-3
TABLE 616-1: COMPILED DATA FOR NBS SRM 616 TRACE ELEMENTS IN GLASS (revised 3/1/86)

ELEMENT UNITS NBS

Mean t SD

CONSENSUS

Mean ± SD (n)

MEDIAN RANGE METHOD MEANS

Mean (n) Method

AU ng/g 180 1 10 B ng/g 200 i 20 220 (2) B ng/g ... ...

B-10 atom % — 19.827 (1)

Cu ng/g 800 1 90 ...

Fe ug/g 11 i 2 12 (2)

Fe ug/g —

Ga ng/g 230 ± 20 ...

Gd ng/g < 10 K ug/g 29 ± 1 La ng/g 34 t 7

Pb ug/g 1.85 t 0.04 1.86 (2)

Rb ng/g 100 i 7 99.8 (1)

Sb ng/g 78 t 7 12 (1)

Sc ng/s 26 i 12 20 (1)

Sm ng/g < 10

Sr ug/g 41.72 t 0.05 41.72 (1)

Th na/g 25.2 t 0.7 23 ± 4 (3)

Th ng/g

Ti ug/g 2.5 t 0.7 2.5 (1)

Tl ng/g 8.2 t 0.5 8.2 (1)

U ng/g 72.1 t 1.3 72.3 ± 0.5 (3)

U ng/g

U-235 atom % 0.6160 0.616 (1)

203 - 230 230 (1) TCGS

203 (1) NT 19.827 (1) IDMS

... 11 - 14 11 (1) POL

_ _ _ _ _ 14 (1) CPAA

< 10 TCGS

1.85 - 1.88 1.865 (2) IDMS

99.8 (1) IDMS

12 (1) NAA

20 (1) NAA

< 10 TCGS

41.72 (1) IDMS

25.2 18 - 25.5 18 (1) NAA 25.35 (2) IDMS

2.5 (1) POL

8.2 (1) IDMS

72.5 71.7 - 72.6 72.15 (2) IDMS

72.5 (1) NT 0.616 (1) IDMS

616-1
TABLE 616-2: INDIVIDUAL DATA FOR NBS SRM 616 (revised 3/1/86)

Cone

B (ng/g)

203

230

B-10 (atom %)

19.827

1114

Gd (ug/g)

1.85

1.88

99.8

Sb (ng/g)

12

Uncer Com Method Reference

57

130

0.8

3

0.01

0.018 17

0.014 17

0.6

20

NTTCGS

IDMS

POL

CPAA

TCGS

IDMS

IDMS

IDMS

ITNA

72CAR 01 84GLA 01

72CAR 01

73MAI 01 74SWI 01

85GLA 05

73BAR 01 73BAR 01

73M00 01

73SHE 01

Cone Uncer Com Method Reference

Sc (ng/g)

20 ITNA 73SHE 01

Sm (ug/g)

0.01 4 TCGS 85GLA 05

Sr (ug/g)

41.72

Th (ng/g)

18

25.2

25.5

0.02

0.3 17

1.5 17

IDMS

ITNA

IDMS

IDMS

73M00 01

73SHE 01 73BAR 01 73BAR 01

Ti (ug/g)

2.5

TL (ng/g)

8.2

0.2

0.1

POL

IDMS

73MAI 01

73BAR 01

U (ng/g)

71.7

71.7

72.5

72.6

72.9

0.5

1.4

1.5

0.4

1.7

17

D

17

D

IDMS

IDMS

NTIDMS

IDMS

73BAR 01 72CAR 01 72CAR 01 73BAR 01 72CAR 01

U-235 (atom %)

0.616 0.001 IDMS 72CAR 01

616-2
TABLE 633-1: COMPILED DATA FOR NBS SRM 633 PORTLAND CEMENT (RED CAP)

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS RANGE METHOD

Mean Mean (n)

Al % 2.0 2.00 (2) 1.95 - 2.06 XRF

B ug/g < 100 — — —

Ca % 45.34 46.11 (2) 46.02 - 46.20 XRF

F ug/g 800 — — —

Fe % 2.94 2.92 (1) XRF

K ug/g 1400 1410 (1) XRF

LOI % 0.75

Mg ug/g 6300 5900 (1) XRF Mn ug/g 280

Na ug/g 4700

P ug/g 1050

S % 0.88 1.8 (2) 0.88 - 2.78 XRF

Si % 10.22 10.22 (2) 10.2 - 10.25 XRF

Sr ug/g 2600

Ti ug/g 1440

Zn ug/g < 80

TABLE 633-2: INDIVIDUAL DATA FOR NBS SRM 633 (revised 3/1/86)

Cone

AL (%)

1.95

2.06

Ca (%)

46.02

46.2

Fe (%)

2.92

K (ua/g)

1410

Uncer Com Method Reference

XRF

XRF

XRF

XRF

XRF

XRF

74AND 03

79FRE 01

79FRE 01 74AND 03

79FRE 01

79FRE 01

Cone

Hg (ug/g)

5900

S (%)

Uneer Com Method Reference

0.88

2.78

Si (%)

10.2

10.25

XRF

XRF

XRF

XRF

XRF

79FRE 01

79FRE 01 79FRE 01

74AND 03

79FRE 01

633-1
TABLE 634-1: COMPILED DATA FOR NBS SRM 634 PORTLAND CEMENT (GOLD CAP)

(revised 3/1/86)

ELEMENT UNITS NBS

Mean

CONSENSUS

Mean (n)

METHOD

Al % 2.76 2.7 (1) XRF

B ug/g < 100

Ca % 44.74 45 (1) XRF

F ug/g 700

Fe % 1.98

K ug/g 3500

LOI % 1.61

Mn ug/g 1950

Na ug/g 1100

P ug/g 440

S ug/g 8840

Si % 9.68 9.57 (1) XRF

Sr ug/g 1000

Ti ug/g 1800

Zn ug/g 160

TABLE 634-2: INDIVIDUAL DATA FOR NBS SRM 634

(revised 3/1/86)

Cone Uncer Com Method Reference

Al (%)

2.7 XRF 74AND 03

Ca (%)

45 XRF 74AND 03

Si (%)

9.57 XRF 74AND 03

634-1
TABLE 635-1: COMPILED DATA FOR MBS SRM )635 PORTLAND CEMENT (BLUE CAP)

(revised 3/1/86)

ELEMENT UNITS NBS

Mean

CONSENSUS

Mean (n)

RANGE METHOD

Al % 3.33 3.36 (2) 3.33 - 3.40 XRF

Ca % 42.06 42.82 (2) 42.8 - 42.84 XRF

F ug/g 300

Fe % 1.82 1.85 (1) XRF

K ug/g 3700 3800 (1) XRF

LCI % 3.25

Mg ug/g 7120 (1) XRF Mn ug/g 630

Na ug/g 500

P ug/g 740

S % 2.83 2.82 (1) CB

Si % 8.6 8.58 (2) 8.50 - 8.65 XRF

Sr ug/g 1780

Ti ug/g 1900

Zn ug/g 80

TABLE 635-2: INDIVIDUAL DATA FOR NBS SRM 635 (revised 3/1/86)

Cone

A I (%)

3.33

3.4

Ca (%)

42.8

42.84

Fe (%)

1.85

Uncer Com Method Reference

XRF

XRF

XRF

XRF

XRF

79FRE 01 74AND 03

74AND 03

79FRE 01

79FRE 01

Cone

K <ug/g)

3800

(ug/q)

7120

S (%)

Uncer Com Method Reference

2.82

Si (%)

XRF

XRF

CB

8.5

8.65

XRF

XRF

79FRE 01

79FRE 01

84LEC 02

74AND 03

79FRE 01

635-1
TABLE 636-1: COMPILED DATA FOR NBS SRM 636 PORTLAND CEMENT (YELLOW CAP)

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS RANGE METHOD

Mean Mean (n)

Al % 1.6 1.72 (2) 1.68 - 1.75 XRF

Ca % 45.43 45.46 (2) 45.43 - 45.5 XRF

F ug/g 500

Fe % 1.12 1.11 (1) XRF

K ug/g 4900 4650 (1) XRF

LOI % 1.16

Mg % 2.31 (1) XRF

Mn ug/g 840

Na ug/g 820

P ug/g 390

S % 0.924 0.94 (2) 0.925 - 0.964 CB,XRF

Si % 10.84 10.72 (2) 10.70 - 10.75 XRF

Sr ug/g 340

Ti ug/g 1000

Zn ug/g 240

TABLE 636-2: INDIVIDUAL DATA FOR NBS SRM 636 (revised 3/1/86)

Cone

A I (%)

1.68

1.75

Ca (%)

45.43

45.5

Fe (%)

1.11

Uncer Com Method Reference

XRF

XRF

XRF

XRF

XRF

79FRE 01 74AND 03

79FRE 01 74AND 03

79FRE 01

Cone

JLlmlaL

4650

Mg (%)

2.31

S (%)

Uncer Com Method Reference

0.925

0.964

Si (%)

10.7

10.75

XRF

XRF

CBXRF

XRF

XRF

79FRE 01

79FRE 01

84LEC 02

79FRE 01

74AND 03

79FRE 01

636-1
TABLE 637-1: COMPILED DATA FOR NBS SRM 637 PORTLAND CEMENT (PINK CAP)

(revised 3/1/86)

ELEMENT

\

UNITS NBS

Mean

CONSENSUS

Mean (n)

RANGE METHOD

Al % 1.74 1.76 (2) 1.75 - 1.76 XRF

Ca % 47.22 47.3 (2) 47.09 - 47,5 XRF

F ug/g 400 — ...

Fe % 1.26 1.22 (1) XRF

K ug/g 2100 2080- (1) XRF

LOI % 1.68 ... ...

Mg ug/g 3900 (1) XRF

Mn ug/g 420

Na ug/g 1100

P ug/g 1090

S % 0.952 0.964 (1) XRF

Si % 10.77 10.8 (2) 10.8 - 10.8 XRF

Sr ug/g 760

Ti ug/g 1260

Zn ug/g 80

TABLE 637-2: INDIVIDUAL DATA FOR NBS SRM 637 (revised 3/1/86)

Cone

A I (%)

1.75

1.76

Ca (%)

47.09

47.5

Fe (%)

1.22

K <ug/g)

2080

Uncer Com Method Reference

XRF

XRF

XRF

XRF

XRF

XRF

74AND 03

79FRE 01

79FRE 01

74AND 03

79FRE 01

79FRE 01

Cone

Mg (ug

3900

S (%)

0.964

Si (%)

10.8

10.8

Uncer Com Method Reference

KRF

XRF

79FRE 01

79FRE 01

XRF 79FRE 01 XRF 74AND 03

(

637-1
TABLE 638-1: COMPILED DATA FOR NBS SRM 638

(revised 3/1/86)

PORTLAND CEMENT (GREEN CAP)

ELEMENT UNITS NBS

Mean

CONSENSUS

Mean (n)

RANGE METHOD

Al % 2.35 2.41 (2) 2.40 - 2.42 XRF

B ug/g < 100 ... ...

Ca % 44.39 44.35 (2) 44.3 - 44.4 XRF

F ug/g 400 ... ...

Fe % 2.48 2.49 (1) ... XRF

K ug/g 4900 4900 (1) ... XRF

LOI % 0.95

Mg % 2.26 (1) XRF

Mn ug/g 350

Na ug/g 960

P ug/g 260

S % 0.936 0.984 (1) XRF

Si % 10.03 9.99 (2) 9.98 - 10.0 XRF

Sr ug/g 590

Ti ug/g 1500 Zn ug/g 720

TABLE 638-2: INDIVIDUAL DATA FOR NBS SRM 638 (revised 3/1/86)

Cone

Al (%)

2.4

2.42

Ca (%)

44.3

44.4

(%)

2.49

Uncer Com Method Reference

XRF

XRF

XRF

XRF

XRF

74AND 03

79FRE 01

74AND 03

79FRE 01

79FRE 01

Cone

K (ug/g)

4900

Mg (%)

2.26

S (%)

0.984

Si (%)

9.98

10

Uneer Com Method Reference

XRF

XRF

XRF

XRF

XRF

79FRE 01

79FRE 01

79FRE 01

79FRE 01 74AND 03

638-1
T&Di 1 mdlcr 1

Ojt I . COMPILED DATA FOR NBS SRM 639 PORTLAND CEMENT (CLEAR PAD \

(revised 3/1/86)

CICLCPiCN PMPUt1

1UNIMI1 1 o NBS CONSENSUS RANGE

Mean Mean (ri)

Al V 2.26 2.3 (2) 2.3 - 2.3 VPP

wB A 47.02 47.14 (2) 47.07 - 47.2 Ar\ r Er 200

re 1.68 1.65 (1) AKr

1ug/g In /n 500 500 (1) Anr A 1.0 > » «

Ma 7120 (1) XRF nn ug/g 560

Na ug/g 480

P ug/g 350

S % 0.992 0.98 (1) XRF

Si % 10.09 10.04 (2) 10.0 - 10.09 XRF

Sr ug/g 1270

Ti ug/g 1860

Zn ug/g 80

TABLE 639-2: INDIVIDUAL DATA FOR NBS SRM 639 (revised 3/1/86)

Cone

A I <%?

2.3

2.3

Ca (%)

47.07

47.2

Fe (%)

1.65

Uncer Com Method Reference

XRF

XRF

XRF

XRF

XRF

79FRE 01 74AND 03

79FRE 01 74AN0 03

79FRE 01

Cone

500

(ug/g)

7120

s (%)

Uncer Com Method Reference

0.98

Si (%)

10

10.09

XRF

XRF

XRF

XRF

XRF

79FRE 01

79FRE 01

79FRE 01

74AND 03

79FRE 01

(

639-1
28

13

(/) m C3 lU u LiJ (J C/) ^*

8 C CM

111 Z o OJ

(/> * Ml~* ^3 —

** CD

- n ft

1 o c

sX <> CO

c

X «] 1 1 o 1 1 , 1 • 1 1 1 o 1 1 1 1 £ o • 1 1 OJ 1 00 1 1 1

^\ c

(/> LU

Q. c O O 1 1 1 O CO 1 0) • ( 1 1 O 1 1 <^ • 1 1 rsj od 1 1

3 5

k5 oj

o o in fo

a:

CO u o (n: u —I —I I— u < o -•

I- o I—

</> M -J —

I

o u 3 3 o O o I- !- <J 3

Kl «- «- w w w ^

o oo >0 >0

in CM «- «-

eo o «- «- > o o

to

(M

N- O O OO

1^ Oo00

^ ^ ^ <\ ^ ^ ^ ^ (M

in

00 o

m

o

in

o

>c

c fVI (M in in in ro ro in ro CM ro

1- >^ \^ \^ >^

_l< in 00

(A ro ro O PJ o o o

< rvi in

OQ o oin

1^

1 1 rj 1 •*1 <M O o o 1 in I o 1 CO

• z

•H (M fVI H 1

1

1 •

I CO

•H I

1

1 +1

1 +1 •H H H +11

1 s-ro

D 1 1 +1

1 c <\J o O ro r^ in V

(Q 00 O m ro -* O in Z 4> fM ro ro ro Z CO si

COo

<

<

o (M 00 -* >* m CM

ro ^ro in o o CO o CO o ro >0 IS- o <0 o CM >o in in o r^ <\J ol ro CM 00 ro in ro >! ro CM r^ ro

1 1 CO o

1 ro1

<>>

1 1 CO1 o1 1 1 o1 O1 1 1 1 ro

1 1 in

1 1

1 o

t 1 11 o CO ro o ro ro o o o o (M o <\j ro ro CO

00 OJ o r^

o

1^

orom

a. o111

CO r>. m o» 00

1 C\J O CO in • 00 o >* CM o 1 1 1 1 ro 1 1 in o o 1 1 . O 1 1 ro S- CM • 1 1 g 1 • 1 1 Ov 1 1 »- tVJ 1 1 CO r\j ro (M ro IM N> I 1 1 1 fO • 1 T— 00 in

O

r^ (M ro in OJ ro ro >o ro >o 00 OJ OJ «— ro ro in

in ^o 00 r\j 00

ro >o o OJ o •* o OJ o in o O o O o o OJ fVI ro in O o o o in o o CO

in o O GO o

H +1 o H H H -H +1 +1 +1 r^ •H o -H +1

f\j OJ • O o r^ ro r^ ro o. 0> o o OJ in o V o ro -4- o in

ro ro (M ro ro CO in

ol 00 ro rJ r>I

EO

CO

c

CI

mo

CO oO

o

ro

ro

ro

ro

ro ro o o o o o r^ o o 1 1 1 1 1 1 ^ 1 1 o •M -Hill III • 1 1 -H OM 1 1 1 1 1 1 T— 1 1 ro * O IM <<) min nI

o> o> o> C7> O) at cn O) at cn »^ >^ >^

cn O) O) o> O) CD O) O) O) O) cn at cn cn c 3 3 c 3 »S 3 3 3 3 3 c 3 3 3 3 3 *S 5* >« S« 3 3 3 3^ >S 3 c c

at3

—< to < <

3<as CQ

o

c

1 nj 01 —' —

U <J O U CJ O i- CJ u

3

(J a

(. 3

UJ LU 8OJ

<D 01 CO T3

CD O

G O OJ OJ o t_ 3: •-•

688-1
in8 5

Ml Q

Z to

I- c O a>

0)

c

(0

0)

c

o

u

to<

a. c u m

o

q: % +1 to z

c

</> CO a> z

a:Ou.<

<Q lUo O z

LU < _l a:

O.o

o

<

LLI

</) (/) CD 5

CJ

J—

\^ >«

ro

fNJ o o sO

1 1 CM 1

I 1 H -M 1 1

1 1 in 1 1 ^3

in «—

^\

CM o 1 1 C\J O in o 1 * * * in *

>—

ro

ro o O O o >o o ro • O ro in (NJ * in

*

ro C\J O in o o o 00 o in 1 1 fVJ +1 +1 * +1 +1 in o lA m ro CNJ

O ro O o o o in u-i in

Ofo

oCJ

o

o (/) _J CJ CD o CJ

1—

CM

in

CM

>o o CM

CM H

CM

CM

tou

o

5

O

o o 00 ro

«- -O o

to

o-

(M

(M

M O

»- in CM

o

00 o o> in 00 ro o fvi ro ro CM NO «— • • »— in «- CO

ro

ro >o o in

CO CM «- o tNro -o

o >o •

• ro

ro >* ^

eo N. CM

T- 00 in

(M ro

CM

CMOro

CM

CM

oo

in

CM

«- CM «- CM W N—

in • ro o CM r- oNO

o o

CM ^

O 00 • CM o ro ^ On • nO CM «- CM

NO ro in ro CM in CM

CM

roCM o o o in O 00 CM o tN. o o CM O H s

+1 H +1 o NO •H +1 o C> o ro CM in o o o ^^ o CM NO t

o CM fo in ro ro

CM

o in NO O o> o o o On o o CO ro

fN- 00 00 nO

fC

<o <> CM ro in ro ro CM CM

1 On1 o nO1 CM o1 o1 o1 o1 in1 eo1 o -4- nO o in 00 ro CM ro o CM CM CM

CM •c

CM O CM

ro in

in ro On lO o in On ro O I o • ro O o o o CM CM 1 I CM nO • O CM CM o CM o nO * 1 >* ro CM CM IN. ro in ro o CM

xj- o in eo

nO »- ro »-

CM ro CM

-J- ro On nO

COin

NO CO O On

• N- O CM nO

< N r-N ^\ /-N c in r>. CO 00 CM ro ro CM ro 1^

to CM CO o N* CM o o o C/l to o o o o o

z O -* O NO o ro CM CM ro

LU o O >* >* nO

C/> H H H H •H -H H •H H -H H

z in V CM CM o c lO O nO O in nO CO O O 00 o in CM in in o O ro

in ro CM o^ ro z in

roV

ino

CM

in

CMCM

/-N CM ro m ro •o ro •J- •* ro

/-N N* m

N_^ CMO

o onJ- o00 oOn oNO CM CO CM

oCMO

O

o

•M •H H H +) •H H H •H +1 H +1 in

CM

CM o

ro OCM

in oNO

ro O

o

oOn

CM O

ro

CM

>*

CM

fN- ino

CM

NOoNO

CM in o O CM o o t/> o o o o CM O o o o On o fVJ nO

to 1 1 O T— I I o • 00

CD +> 1 1 N^ B H •H I I in •H H H CO -H • H -H •H z 1 1 ro in 1 ro CM >*• c o nO o ro nO CM O o m On 00 On ro o <u CM in ro CM <y ro o I. CM NO

*—

fNo oin

ro CM

OnO 00

• m CM

CD CJ) > CD at a) o> a> at at at CJ) at CJ) at CJ) CJ) CJ) CJ) O) CJ) \ \ \ \ N^ \ >v "N» «N» a> ay O) O) a) o> en at at at C]> cn at > o> at O) o> CJ) at 3 3 c s< s< 3 s< 3 3 3 3 3 3 3 c 3 3 X »« 3 3 c c c 3 c c 3 3 3 3 3

(D ^ T3 •— a.cLQ.ac(/)c/>(/>(/>c/>cA</> CO ^ x: - e XI > >- >- C (. . rsi rNi

688-2
TABLE 688-2: INDIVIDUAL DATA FOR NBS SRM 688 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Al (%)

1

1 Ce (ug/g)

8.54 0.39 ITNA 82GRA

1 01 1 10.1 3.9 ITNA 82GRA 01 8.89 0.11 ITNA 85GLA 01 1 11.3 0.4 ICPES 83CR0 01 9.04 0.05 ICPES 83CR0 01 1 12.87 0.2 ITNA 83B0Y 01

9.18 0.09 TOGS 85AND 01 1 13.4 0.6 ITNA 85GLA 01 9.18 0.09 TCGS 83AND 01 1 13.7 0.5 RTNA 85GAU 04

9.24 0.1 lENA 85GLA 02 1 16.7 1 RTNA 84GLA 11 9.3 0.2 TCGS 82GRA 01 1 25 25 WXRF 85GLA 01 9.34 0.08 UXRF 85GLA 01 1

As (ug/g)

2.33

2.68

Au (ng/g)

0.9

3.3

B (ug/g)

Ba (ug/g)

Be (ng/g)

200

1200

Ca (%)

0.05

0.54

0.4

0.1

50

ITNA

ITNA

ITNA

ITNA

83BOY 01 82GRA 01

82GRA 01 83B0Y 01

< 3 OES 83MIL 01 0.88 0.14 TCGS 82GRA 01 1.2 0.2 TCGS 84GLA 01 1.3 0.2 TCGS 83AND 01 1.5 0.2 TCGS 85AN0 01

178 2 ICPES 83CR0 01 197 33 ITNA 82GRA 01 200 30 ITNA 85GLA 01 200 60 WXRF 85GLA 01 210 30 ITNA 84GLA 02

ICPES

OES

83CR0 01 83MIL 01

7,9 0.2 TCGS 82GRA 01 1 Cu (ug/g)

8.2 0.6 ITNA 82GRA 01 1 8.2 0.6 ITNA 85GLA 01 1 90

8.7 0.09 TCGS 83AND 01 1 8.7 0.09 TCGS 85AND 01 1 8.75 0.02 WXRF 85GLA 01 1 8.82 0.02 ICPES 83CRO 01 1

31

35

35.8

Co (ug/g)

46.1

46.6

47

47.5

50

51.9

55.6

Cr (ug/g)

230

260

322

328

330

330

377

Cs (ng/g)

<

<

110

210

400

3

10.8

0.5

0.9

11.5

3

0.5

1.2

25

20

4

154

10

4

400

600

60

110

ISE TCGS

TCGS

ITNA ITNA

ICPES

ITNA WXRF

ITNA

ITNA

WXRF

ICPES

ITNA

ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ICPES

86ELS 01 85AND 01 83AND 01

85GLA 01 84GLA 11 83CR0 01 82GRA 01 85GLA 01 83B0y 01 84GLA 02

85GLA 01 83CR0 01 86GAU 01 82GRA 01 85GLA 01 84GLA 02

83B0Y 01

84GLA 11 83B0Y 01 85GLA 01 84GLA 02

86GAU 01

83CR0 01

688-3
TABLE 688-2: INDIVIDUAL DATA FOR NBS SRM 688 (cont.)

Cone

..DiLlyaZai.

Er (ug/g)

FE203

1.8

FEO

Ga (ug/g)

Uncer Com Method Reference

0.17

3.1 0,3 RTNA 85GAU 04 1 2.5 ITNA 82GRA 01 3.2 0.8 ITNA 83B0Y 01 j 2.82 0.08 TCGS 'i2GRA 01 3.4 O.U FAA 84GLA 11 1 2.8S 0.1 TCGS 83AKD 01 3.4 0.5 FAA 85GAU 04 1 3,3 0.5 4 TCGS 85GLA 05

3.53 0.17 RTNA 84GLA 11 j 3.46 0.1 TCGS 85AN0 01 3.8 0.2 ICPES 83CR0 01 1 3,6 0.3 ICPES 83CR0 01 3.7 0.4 4 TCGS 85GLA 05

1.9 0.1 ICPES 83CR0 01 1 2.2 0.4 FAA 85GAU 04 1 390 10 TCGS 83AND 01 2.22 0.08 FAA 84GLA 11 j 410 10 TCGS 85AND 01

CALC 85GLA 01

17 7 ICPES 83CR0 01 17.7 1.1 ITNA 83B0Y 01 57 10 ITNA 82GRA 01

0.919 0.048 ITNA 82GRA 01 1 0.14 0,01 COUL 85GLA

0.99 0.06 ITNA 85GLA 01 1 1.001 0.01 ITNA 83B0Y 01 1 H20- (%)

1.01 0.02 ICPES 83CR0 01 1 1.01 0.04 RTNA 85GAU 04 1 0,11 0,01 COUL 85GLA

1.01 0.05 ITNA 84GLA 02 1 1.04 0.04 RTNA 84GLA 11 1

7.03 0.1 TCGS 85AND 01 1 1.62 0

7,03 0.1 TCGS 83AND 01 1 7.1 0.06 ITNA 84GLA 02 1 Ho (nq/g)

7.19 0.02 UXRF 85GLA 01 1 7.19 0.17 ITNA 85GLA 01 1 800 50

7.23 0.17 TCGS 82GRA 01 1 810 60

7.23 0.19 ITNA 82GRA 01 1 820 20

7.34 0.03 ICPES 83CR0 01 1 7.82 0.08 ITNA 83B0Y 01 1 Ir (ng/g)

Cone

Gd (ug/g)

Uncer Com Method

H20t- (%)

1.46

1.58

0.13

0.14

K (ug/g)

1.8 ITNA

Reference

ITNA 84GLA 02 ITNA 82GRA 01 ITNA 85GLA 01

ICPES 83CR0 01 FAA 85GAU 04

FAA 84GLA 11

83B0Y 01

<%) 1530 60 TCGS 83AND 01 1530 60 TCGS 85AND 01 7.64 TITR 84G0L 01 1 1590 75 WXRF 85GLA 01 7.65 0.15 COLOR 85GLA 01 1 1620 30 ICPES 83CR0 01 1700 100 TCGS 826RA 01

(

688-4
TABLE 688-2: INDIVIDUAL DATA FOR NBS SRH 688 (cont.)

Cone

La (ug/g)

Uncer Com Method Reference

4.8 0.4 RTNA 84GLA 11 1 1.05 0.07 TCGS 82GRA

4.96 0.05 ITNA 83B0Y 01 1 1.39 0.12 ITNA 82GRA

5 2.5 UXRF 85GLA 01 1 1.48 0.02 ITNA 85GAU

5.3 0.1 ICPES 83CR0 01 1 1.51 0.08 ITNA 85GLA

5.3 0.3 RTNA 85GAU 04 1 1.57 0.02 WXRF 85GLA

5.9 0.2 ITNA 84GLA 02 1 1.61 0.01 ITNA 84GLA

5.9 0.6 ITNA 85GLA 01 1 1.61 0.06 TCGS 83AND

7.54 0.93 ITNA 82GRA 01 1 1.61 0.06 TCGS 85AND

1.63 0.05 ICPES 83CR0

JLLlug/ai.

l-u (ng/g)

Mg (%)

ICPES 83CR0 01

330 3 ITNA 83B0y 01 330 10 ICPES 83CR0 01 340 40 ITNA 84GLA 11 342 57 ITNA 82GRA 01 420 60 RTNA 84GLA 11

3.9 0.8 ITNA 82GRA 01

5 0.12 ITNA 85GLA 01 5.08 0.02 ICPES 83CR0 01 5.2 AA 85GAU 04

5.22 0.02 WXRF 85GLA 01 5.3 0.2 TCGS 83AND 01 5.31 0.18 TCGS 85AND 01 5.7 0.4 TCGS 82GRA 01 6.12 0.12 lENA 85GLA 02

Mn (ug/g)

1120 60 TCGS 82GRA 01 1140 30 ITNA 85GLA 01 1180 70 ITNA 82GRA 01 1220 40 WXRF 85GLA 01 1230 40 TCGS 83AND 01 1230 40 TCGS 85AND 01 1240 20 ICPES 83CR0 01 1290 60 ITNA 84GLA 02

Cone

Wa (%)

Uncer Com Method Reference

Nb (ug/g)

5

5

Nd (ug/g)

8.38

9.95

10.4

15

Wi (ug/g)

123

143

180

186

p (ug/g)

560

620

930

Pb (ug/g)

Pr (ug/g)

2.4

Rb (ug/g)

2.18

3

32.7

10

0.16

1.08

0.5

1

29

250

13

20

20

0.6

10

0.26

3

1

UXRF

ICPES

ITNA

ITNA

ITNA ICPES

RTNA

ITNA ICPES

WXRF

ITNA

ICPES

WXRF

COLOR

ICPES

ICPES

ITNA

ITNA WXRF

WXRF

84KYL 01 83CR0 01

85GLA 01 83B0Y 01 82GRA 01 83CR0 01 84GLA 1

82GRA 01 83CR0 01 85GLA 01 83B0Y 01

83CR0 01 85GLA 01 85GAU 04

83CR0 01

83CR0 01

85GLA 01 83B0Y 01 85GLA 01 84KYL 01

688-5
TABLE 6SS-2: INDIVIDUAL DATA FOR NBS SRH 68S (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Sb (ng/g)

1

la (ng/g)

< 200 ITNA 85GLA 01 1 246 58 ITNA 82GRA 01 87 3 ITNA 83BQY 01 1 310 Z. A60 ITNA 85GLA 01 420 ITNA 84GLA 02 1 ton 380 »A70 ITNA O / ^1 A AO 84GLA 02

466 207 ITNA 82GRA 01 1 Tb (ng/g)

Sc (ug/g)

1 462 25 ITNA 82GRA 01 35.2 0.4 ITNA 85GLA 01 1 512 10 ITNA 07nAV A

o3B0Y 01

U.I 1 1 NA 84GLA 11 1 Aft OU T TUA I 1 NA

36.0.9 ITNA 82GRA 01 1 535 24 RTNA ohGLA 11 36.3 0.5 ITNA 84GLA 02 1 COA 5oU CA T Til A

1 1 NA ocn A Ai

nU.HA 1 1 Nn 83B0Y 01 1 "zn o oo.y ft 5 T TU A 1 1 NA 86GAU 01 1 Tn (ng/g)

43.3 0.5 ICPES 83CR0 01 1 71 A 310 ^A60 T TLI A ITNA QCr^i A Ai 05GLA U1 Se (ug/g) 1 TOA 320 f Tkl A ITNA OC/^ AI 1 A/ 05GAU U4

1

/ ZA 460 47A 130 ITNA O/ f*l A AO o4GLA 02

< 3 ITMA 83B0Y 01 1 Ti (ug/g)

Si (%)

1 6900 100 TCGS 83AND 01

22.39 0.08 TCGS 85AN0 01 1 6910 100 TCGS 85AND 01 A no U.Uo TCGS 83AND 01 1 7AAA 1 1 NA OcuKA U

22.6 COLOR 85GAU 04 1 71 1A OAyu UVD C WXKr ORri A AI ODuLA U

U. 13 1 IVD C WXKr 85GLA 01 1 OcuKA U

u.o 1 Luo 82GRA 01 1 onyu 1 UrCd

Sm (ug/g)

1

Tm (ng/g)

^ Art 2.09 0.22 ITNA 82GRA 01 1 ^CA 250 ilA 6U C A A PAA fl^f^AII A/. oDuAU Uh

2.29 0.03 ITNA 83B0Y 01 1 264 15 FA A PAA ohGLA 11 2.3 0.3 ITNA 85GLA 01 1 7^A 360 36 T TLI A

1 1 NA ojoUT U1

2.31 A AO TCGS 82GRA 01 1 2.35 0,02 TCGS 83AND 01 1 U (nq/g)

2.4 0.2 4 TCGS 85GLA 05 1 n 1 / U. 1h K 1 NA 85GAU 04 1 UNA Q/ri A ftp

2.5 0.2 4 TCGS 85GLA 05 1 Oil) f\kl A qzaaii ni OOuAU U

2.54 0.07 ITNA 84GLA 02 1 / A f\U A UNA OJuLA ocAi A niU

2.62 A AO U.u2 TCGS 85AND 01 1 DW Rft 1 1 NA O^uKn U

2. OH A If} DTU A K 1 NA 84GLA 11 1 u. r

T PDCC i Lrts 83CR0 01 1

Sr (uQ/g) 235 25 ITNA 82GRA 01

235 40 UXRF 85GLA 01

170 10 ICPES 83CR0 01 1 248 1 ICPES 83CR0 01

170.3 1 WXRF 84KYL 01 1 248 5 RTNA 84GLA 1

171 10 UXRF 85GLA 01 1 179 14 lENA 84GLA 02 1

688-6
Cone

TABLE 688-2: INDIVIDUAL DATA FOR NBS SRM 688 (cont.)

Uncer Com Method Reference I

14.8

18

19.5

Yb (ug/g)

1.77

1.86

1.97

2.06

2.14

2.2

2.36

73

79

90

94

Zr (ug/g?

58.6

58.8

60.8

62

63

1 UXRF 84KYL 01

4 WXRF 85GLA 01

0.1 ICPES 83CR0 01

0.09 ITNA 84GLA 11 0.27 ITNA 82GRA 01 0.02 FAA 84GLA 11 0.05 ITNA 85GLA 01 0.02 ITNA 83B0Y 01 0.03 ICPES 83CR0 01 0.12 RTNA 84GLA 11

5 WXRF 85GLA 01

1 ICPES 83CR0 01 1.8 ITNA 83B0Y 01 AA 85GAU 04

8.7 ITNA 82GRA 01

1 UXRF 84KYL 01 0.3 ITNA 83BOY 01 2 WXRF 85GLA 01 4 ICPES 83CR0 01

688-7
TABLE 694-1: COMPILED DATA FOR NBS SRM 694 WESTERN PHOSPHATE ROCK

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

Al % 0.95 ± 0.05

Ca % 31.2 ± 0.3

Cd ug/g 131 ± 26

Or ug/g 6980

F % 3.2 ± 0.1 Fe ug/g 5520 ± 420

K ug/g 4230 ± 170

Mg ug/g 1990 ± 120

Mn ug/g 90 ± 9

Na ug/g 6380 ± 300

P % 13.17 ± 0.04

Si % 5.23 ± 0.19

Ti ug/g 660

U ug/g 141.4 ± 0.6

V ug/g 1740 ± 390

Zn ug/g 1520

TABLE 697-1: CCWPILED DATA FOR NBS SRf^ 697 BAUXITE (DWINICIAN)

(revised 3/1/86)

ELEMENT UNITS NBS

Mean i SD

Al % 24.2 ± 0.1

Ba ug/g 130

Ca ug/g 5100 ± 210

Ce ug/g 690

Co ug/g 13

Cr ug/g 684 ± 34

Fe % 14,0 ± 0.2

Hf ug/g 14

K ug/g 510 ± 60

LOI % 22.1

Mg ug/g 1100 ± 120

Mn ug/g 3200 ± 230

Na ug/g 270

P ug/g 4200 ± 260

S ug/g 520 ± 120

Sc ug/g 58

Si % 3.18 ± 0.03

Ti % 1.51 ± 0.03

V ug/g 350 ± 30

Zn ug/g 300 ± 25 Zr ug/g 480 ± 50

694-1
TABLE 696-1: COMPILED DATA FOR NBS SRM 696 BAUXITE (SUfilNAH)

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS RANGE METHOD

Mean ± SD Mean (n)

a 1 Al %

OQ O J. rt O Oft / It (2) ICPcS

Ba ug/g 5 I (2) ICPcS ca ug/g lOU 1 13 led (2) lie 113 I2y ICPcS ce ug/g Hi TO (1)

CO ug/g u.y

turn- er ug/g ^cU X (2) 1 ICPcS

Fe % 6.08 ± 0.07 6.04 (2) 6.01 6.07 ICPES

Hf ug/g 32 29 (2) 28 30 ICPES K ug/g 75 ± 25

LOI % 29.9 ± 0.2

Mg ug/g 72 ± 18 63.3 <2> 60.30 66.33 ICPES

Mn ug/g 31 ± 8 28.2 (2) 27.09 29.41 ICPES

Na ug/g 52

P ug/g 220 1 30 209 (2) 192 227 ICPES

S ug/g 840 ± 120

Sc ug/g 8 8 (2) 7 9 ICPES

Si % 1.77 ± 0.05 1.76 (2) 1.76 1.76 ICPES

Ti % 1.58 ± 0.03 1.56 (2) 1.55 1.58 ICPES

V ug/g 400 ± 30 398 (2) 398 398 ICPES

Zn ug/g 11 ± 6 12.8 (1) ICPES Zr ug/g 1040 t 150 1003 (2) 992 1014 ICPES

696-1
TABLE 696-2: INDIVIDUAL DATA FOR NBS SRM 696 (revised 3/1/86)

Cone

A I (%)

28.3015

28.566

Ba (ug/g)

30.46A

32.256

Ca (ug/g)

115

129

Ce (ug/g)

38

Cr (ug/g)

314.64

321.48

Fe (%)

Uncer Com Method Reference

6.0114

6.0743

Hf (ug/g)

28

30

Mg (ug/g)

60.3

66.33

0.4232 1 0.4232 1

1.792 1 2.688 1

1.4

2

6.84

6.84

0.0699 1 0.0629 1

2

2

6.03 1 1.206 1

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

Cone

Mn (ug/g)

27.09

29.412

P (ug/g)

191.84

226.72

Sc (ug/g)

7

9

Si (%)

1.7559

1.7559

1.5514

1.5754

397.6

397.6

Zn (ug/g)

12.848

Zr (ug/g)

992

1013.8

Uncer Com Method Reference

1.548

15.48

4.36

4.36

0.0234

0.028

0.024

0.03

5.6

5.6

0.803

15

22.2

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

696-2
TABLE 698-1: COMPILED DATA FOR NBS SRM 698 BAUXITE (JAMAICAN)

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SO

CONSENSUS

Mean (n)

RANGE METHOD

Al % 25.5 ± 0.2 25.10 (2) 25.02 25.18 ICPES

Ba ug/g 72 68 (2) 68 68 ICPES

Ca ug/g 4400 i 140 4400 (2) 4390 4404 ICPES

Ce ug/g 300 300 (2) 291 310 ICPES

Co ug/g 45 45 (2) 43 47 ICPES

Cr ug/g 550 ± 40 527 (2) 527 527 ICPES

Fe % 13.7 ± 0.1 13.6 (2) 13.35 13.91 ICPES

Hf ug/g 15 13 (1) K ug/g 83 ± 17

LOI % 27.3

Mg ug/g 350 ± 50 332 (2) 332 332 ICPES

Nn ug/g 2900 ± 230 2875 (2) 2872 2879 ICPES

Na ug/g 110

P ug/g 1600 ± 40 1585 (2) 1570 1600 ICPES

S ug/g 880 ± 120

Sc ug/g 51 48 (2) 46 50 ICPES

Si ug/g 3200 ± 140 3180 (2) 3129 3232 ICPES

Ti % 1.42 ± 0.04 1.40 (2) 1.39 1.40 ICPES

V ug/g 360 ± 10 347 (2) 342 353 ICPES

Zn ug/g 230 ± 20 221 (2) 217 225 ICPES

Zr ug/g 450 ± 70 429.6 (2) 429.2 429.9 ICPES

698-1
TABLE 698-2: INDIVIDUAL DATA FOR NBS SRM 698 (revised 3/1/86)

Cone

Al (%)

25.0217

25.1804

Ba (ug/ci)

68.096

68.096

Ca (uq/g)

4390.1

4404.4

Ce (ug/g)

291

310

Co (ug/g)

43

47

Cr (ug/g)

526.68

526.68

Fe (%)

13.3509

13.9101

13

Mg (ug/g)

331.65

331.65

Uncer Com Method Reference

0.3703 1 0.3703 1

2.688 1 3.584 1

57.2 1 64.35 1

510

2

3

6.84

6.84

0.2097 1 0.2796 1

6.03

30.15

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

Cone

Mn (ug/g)

2871.54

2379.28

1569.6

1600.12

Sc (ug/g)

46

50

Si (ug/g)

3128.9

3231.64

Ti (%)

1 .3897

1.4017

V (ug/g)

341.6

352.8

Zn (ug/g)

216.81

224.84

Zr (ug/g)

429.2

429.94

Uncer Com Method Reference

46.44

38.7

21.8

26.16

3

2

46.7

42.03

0.024

0.018

5.6

5.6

8.03

4.015

7.4

5.18

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

83BAR 02

698-2
TABLE 1083-1: COMPILED DATA FOR NBS SRM 1083 WEAR METALS IN LUBRICATING OIL (revised 3/1/86)

ELEMENT UNITS NBS

Mean

Ag ng/g < 50

Al ug/g < 0.5

Cd ng/g < 40

CI ug/g 1.7

Co ng/g < 10

Cr ng/g < 20

Cu ng/g < 500

Fe ug/g < 1 Mg ng/g < 100

Mn ng/g < 5 Mo ng/g < 10 Na ng/g < 60

Ni ng/g < 400

Pb ng/g < 40

S ug/g 980

Si ug/g < 1 Sn ng/g < 400

Ti ug/g < 5 V ng/g < 300

Zn ng/g < 80

TABLE 1084-1: COMPILED DATA FOR NBS SRM 1084 WEAR METALS IN LUBRICATING OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD

Mean ± SD Mean + SD (n)

Ag ug/g 101 95.7 + 1.5 (3) 96 94 - 97 ICPES

Al ug/g 98 ± 2 98 ± 6 (3) 100 92 - 103 ICPES

Cd ng/g < 40

CI ug/g 1.7

Co ng/g < 10

Cr ug/g 100 ± 3 101 + 1 (3) 101 100 - 102 ICPES

Cu ug/g 98 ± 4 99 ± 2 (3) 99 96 - 101 ICPES

Fe ug/g 100 ± 3 98.7 ± 0.6 (3) 99 98 - 99 ICPES

Mg ug/g 98 ± 4 95 ± 3 (3) 96 92 - 97 ICPES

Mn ng/g < 5 Mo ug/g 97 ± 5 97 i 2 (3) 97 94 - 99 ICPES

Na ng/g < 60

Ni ug/g 101 ± 4 97 + 4 (3) 98 93 - 101 ICPES

Pb ug/g 101 98 ± 2 (3) 97 96 - 100 ICPES

S ug/g 2237

Si ug/g 102

Sn ug/g 102 ± 6

Ti ug/g 99 ± 5 100 + 2 (3) 101 98 - 102 ICPES

V ng/g < 300

Zn ng/g < 80

1083-1
TABLE 1084-2: INDIVIDUAL DATA FOR NBS SRM 1084 (revised 3/1/86)

Cone Uncer Com Method Reference

1

I LKta OhBAK Uj

96 5 11 ICPES 84BAR 03

97 1 11 ICPES 8ABAR 03

(ug/q)

92 5 11 ICPES 84BAR 03

100 3 11 ICPES 8ABAR 03

103 7 11 ICPES 84BAR 03

(ug/g)

100 1 11 ICPES 84BAR 03

101 3 11 ICPES 84BAR 03

102 5 11 ICPES 84BAR 03

Cu (ug/g)

96 3 11 ICPES 84BAR 03

99 4 11 ICPES 84BAR 03

101 3 11 ICPES 84BAR 03

(ug/g)

98 4 11 ICPES 84BAR 03

99 2 11 ICPES 84 BAR 03

99 2 11 ICPES 84BAR 03

Cone Uncer Com Method Reference

Mg (ug/g)

92 2 11 ICPES 84BAR 03

96 2 11 ICPES 84BAR 03

97 2 11 ICPES 84BAR 03

(ug/g)

94 3 11 ICPES 84BAR 03

97 3 11 ICPES 84BAR 03

99 4 11 ICPES 84BAR 03

Ni (ug/g)

93 3 11 ICPES 84BAR 03

98 4 11 ICPES 84BAR 03

101 5 11 ICPES 84BAR 03

Pb (ug/g)

96 4 11 ICPES 84BAR 03

97 2 11 ICPES 84BAR 03

100 3 11 ICPES 84BAR 03

(ug/g)

98 2 11 ICPES 84BAR 03

101 7 11 ICPES 84BAR 03

102 2 11 ICPES 84BAR 03
TABLE 1085-1: COMPILED DATA FOR NBS SRM 1085 WEAR METALS IN LUBRICATING OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD

Mean ± SD Mean ± SD (n)

Ag ug/g 291 300 ± 6 (3) 303 293 - 305 ICPES

Al ug/g 296 ± 4 303 ± 6 (3) 303 297 - 309 ICPES

Cd ng/g < 40 — —

CI ug/g 1.7 --- - - . —

Co ng/g < 10 • - • — —

Cr ug/g 298 ± 5 302 ± 8 (3) 304 294 - 309 ICPES

Cu ug/g 295 ± 10 302 ± 2 (3) 302 299 - 304 ICPES

Fe ug/g 300 ± 4 303.3 + 1.5 (3) 303 302 - 305 ICPES

Mg ug/g 297 ± 3 300 ± 5 (3) 302 295 - 304 ICPES

Mn ng/g < 5 — —

Mo ug/g 292 ± 11 293 + 4 (3) 292 290 - 298 ICPES

Na ng/g < 60

Ni ug/g 303 ± 7 300 ± 10 (3) 303 288 - 308 ICPES

Pb ug/g 305 300.3 ± 1.2 (3) 301 299 - 301 ICPES

S ug/g 4806

Si ug/g 308

Sn ug/g 296 ± 12

Ti ug/g 300 ± 4

V ng/g < 300

Zn ng/g < 80

1085-1
TABLE 1085-2: INDIVIDUAL DATA FOR NBS SRM 1085 (revised 3/1/86)

Cone Uncer Com Method Reference

Ag (ug/g)

293 5 11 ICPES 84BAR 03

303 7 11 ICPES 84BAR 03

305 5 11 ICPES 84BAR 03

(ug/g)

297 7 11 ICPES 84BAR 03

303 7 11 ICPES 8ABAR 03

309 8 11 ICPES 84BAR 03

Cr (ug/g)

294 4 11 ICPES 84BAR 03

304 3 11 ICPES 84BAR 03

309 6 11 ICPES 84BAR 03

J (ug/ci)

299 5 11 ICPES 84BAR 03

302 6 11 ICPES 84BAR 03

304 7 11 ICPES 84BAR 03

Cone Uncer Com Method Reference

<ug/si?

302 5 11 ICPES 84BAR 03

303 5 11 ICPES 84BAR 03

305 10 11 ICPES 84BAR 03

1 (UQ/q)

295 8 11 ICPES 84BAR 03

302 10 11 ICPES 84BAR 03

304 8 11 ICPES 84BAR 03

Mo (ug/g)

290 10 11 ICPES 84BAR 03

292 4 11 ICPES 84BAR 03

298 7 11 ICPES 84BAR 03

(ug/g)

288 7 11 ICPES 84BAR 03

303 5 11 ICPES 84BAR 03

308 5 11 ICPES 84BAR 03

Pb (ug/g)

299 10 11 ICPES 84BAR 03

301 6 11 ICPES 84BAR 03

301 6 11 ICPES 84BAR 03

1085-2
TABLE 1549-1: COMPILED COMPOSITION DATA FOR NBS SRH 1549 MILK POWDER (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SO

CONSENSUS

Mean (n)

RANGE

Aa na/a < 0.3 < 0.3 -- - NAA

Al 2 < 3

-- - NAA

As ng/Q 1.9 1.77 (1) -- - NAA

Br ug/g •*a# a 12 11.85 (2) 11.6 - 12.1 NAA

Ca X 1.3 ± 0.05 1.263 (2) 1.2 - 1.326 NAA

Cd ng/g • 'a/ a 0.5 * 0.2 0.47 <1) NAA

CI % 1.09 t 0.02 1.085 (1) -- NAA

Co na/g 4.1 4.12 (1) .. NAA

Cr ng/g • »a/ a 2.6 ± 0,7 2.5 (1) .. NAA

Cs ng/g ' 'a' a 17.6 (1) ... NAA

Cu ng/g • 'a/ a 700 ± 100 628 <2) 606 - 650 NAA

F ng/g 'a/ a 200 ... ...

Fe ug/g **a' a 2.1 2.03 (2) 1.76 - 2.3 NAA

H20 % 3.6 (1) ...

Hg ng/g ' 'a/ a 0.3 ± 0.2 0.16 (1) ... NAA

I ug/g 3.38 ± 0.02 3.2 (1) .., NAA

K X 1.69 ± 0.03 1.735 (2) 1.69 - 1.78 NAA

Mg 1200 1 Www tlb 30«^ V 1190 <1) ... NAA

Mn na/a 260 1 60 281.5 (2) 233 - 330 MAA

Mo hq/q '3/ 99 340 332 (2) 322 - 342 NAA

N % 5.61 (1) ...

Na ug/g *"a' a 4970 ± 100 4890 (1) ... NAA

Ni ng/g • 'a* a 240 (1) ...

p % 1.05 ... ...

Pb ng/g 'a' a 19 ± 3 < 100 ...

Rb ug/g **a' a 11 12.75 (2) 12.4 - 13.1 NAA

s ug/g *»a/ a 3510 ± 50 3514 (1) ... IDHS

S-32/34 ratio 22.624 (1) ... IDMS

S-33/34 ratio 0.1779 (1) ... IDMS

Sb ng/g 0.27 0.25 (1) ... NAA

Sc ng/g 0.94 (1) NAA

Se ng/g 110 t 10 100 (2) 90 - 110 NAA

Si ug/g **a/ a < 50

Sn ng/g < 500 1.9 (1) NAA

Sr ug/g 3.69 (1)

U ng/g < 1 NAA

W ng/g 0.43 (1) NAA

Zn ug/g 46.1 ± 2.2 46.75 (2) 46.6 - 46.9 NAA

COMPOUND CAS #

Total Folates

Total Pantothenates

Thiamine

Protein

Lactose

l-Ascorbic acid

Niacin

Vitamin B6

Riboflavin

50817

59676

65236

83885

UNITS

ug/g

ug/g

ug/g

%

%

ug/g

ug/g

ug/g

ug/g

NBS

Mean

47

53

CONSENSUS

Mean (n)

0.64

45.2

4.5

35.8

43.4

9.8

4.8

15

<1)

(1)

(1)

(1)

(1)

(1)

(1)

(1)

1549-1
TABLE 1549-2: INDIVIDUAL DATA FOR NBS SRM 1549 (revised 3/1/86)

Cone Uncer Com Method Reference

Total Folates (ug/g)

0.64

Total Pantothenates (ug/g)

45.2

Thiamine (ug/g)

4.5

Protein (%)

35.8

I -Ascorbic acid (ug/g)

43.4

Niacin (ug/g)

9.8

Vitamin B6 (ug/g)

4.8

Riboflavin (ug/g)

15

Ag (ng/g)

< 0.3

Al (ug/g)

< 3

As (ng/g)

<

1.77

Br (ug/g)

11.6

12.1

50

0.1

0.04

0.2

W 85TAN 01

W 85TAN 01

W 85TAN 01

W 85TAN 01

W 85TAN 01

W 85TAN 01

VV 85TAN 01

W 85TAN 01

RTNA 86GRE 01

RTNA 86GRE 01

XRF

RTNA

ITNA XRF

86GIA 01 86GRE 01

86GRE 01 86GIA 01

Cone

Ca (%)

1.2

1.326

Cd (ng/g)

0.47

CI (%)

Uncer Com Method Reference

0.08

0.026

XRF

ITNA

Co (ng/g)

4.12 0.27

Cr (ng/g)

2.5

Cs (ng/g)

17.6

Cu (ng/g)

606

650

Fe (ug/g)

1.76

2.3

H20 (%)

3.6

HPi (ng/g)

0.16

i Cug/g)

3.2

600

0.6

0.7

10

40

0.13

0.16

100 L 0.015

0.3

XRF RTNA

RTNA

XRF

ITNA XRF

XRF RTNA

86GIA 01 86GRE 01

0.09 RTNA 86GRE 01

1.085 0.014 ITNA 86GRE 01

ITNA 86GRE 01

86GIA 01 86GRE 01

ITNA 86GRE 01

86GRE 01 86GIA 01

86GRE 01 86GIA 01

W 85TAN 01

86GIA 01 86GRE 01

ITNA 86GRE 01

1.69

1.78

0.03

0.2

ITNA XRF

86GRE 01 86GIA 01

1549-2
TABLE 15A9-2: INDIVIDUAL DATA FOR NBS SRM 1549 (cont.)

240

Pb (ng/g)

12.4

13.1

, S (ug/g>

3514

Cone

<ug/g>

1190

Hn (ng/g)

233

330

Mo (ng/g)

322

342

5.61

Wa (ug/g)

4890 60

Ni (ng/g)

Uncer Com Method Reference

30

13

120

17

10

60

0.4

0.2

29

RTNA

RTNA

ITNA XRF

ITNA 86GRE 01

ITNA 86GRE 01 XRF 86GIA 01

86GRE 01 84BYR 01

W 85TAM 01

ITNA 86GRE 01

XRF 86GIA 01

< 100 L XRF 86GIA 01

86GRE 01 86GIA 01

IDMS 84ICEL 01

Cone Uncer Com Method Reference

S-32/34 (ratio)

22.624

S-33/34 (ratio)

0.1779

Sb (ng/g)

0.25 0.03

Sc (ng/g)

0.94

Se (ng/g)

90

110

Sn (ng/g)

Sr (ug/g)

U (ng/g)

W (ng/g)

0.43

Zn (ug/g)

46.6

46.9

40

3

1.9 0.7

3.69 0.1

< 1

0.03

1.2

0.9

XRF

ITNA

ITNA XRF

IDMS 84KEL 01

IDMS 84KEL 01

RTNA 86GRE 01

ITNA 86GAU 01

86GIA 01 86GRE 01

RTNA 86GRE 01

XRF 86GIA 01

DNA 86GAU 01

RTNA 84BYR 01

86GRE 01 86GIA 01

1549-3
Q. >< O CO

CL </>

CO

CO

o> c 8 £ o

CO

N.

O

UJ 4>

C/J uo OfX CO

</) a. >

OfX

Ou -J o o •-< CJ

m

o u. a.

o 3c

«>

o in ^ 3 I ^>0 <

tn

«- fM vO • o in rj f\j MOO o • o>

%t ^ O 00 o> o

a.o

28

"8>

COM

Of

UJ

(—

</> >-o

z:

Of

CO

CO

00

oeO< - o

o OJ

\^

00 00

m

oO

oo Si

r:

O

oo • o ^ 

00o

oo <\l

o 1 1 1 1 1 1 1 1 1 1 1 1 D O

HH

t •M +1 1 1 1 -H 1 -H 1 1 1 1 1 H 1 1 1 +* 4-!

o +< •M 1 1 1 1 1 1 1 1 1 1 1 1 c N. o O T— CO o ro in 00 a

:8

vO

O <M o»

o> f\) in «-~ ro

o

X

o in

o

c DO NO oo -*m ro f\J ro lA

1^

o

o ro

oooo so f\J CO o o ro m O NO o m o lA m o in o o o ro CO 1 g o o o o o o o H M -H 0 •H 1 rvi +< H H O +< •H CO H (M +1 1 H +1 •H 1 1 1 o c in ro O O ro V V 00 V o O

<> in

m 8:

:S

•O

t

in

s 00 « (M (M ro X o o o >*

^> ^\ c oo fO <* (\J >-/ w \^ Q O </> o *

1TM in rvi

o 1 1 1 1 1 O 1 1 1 1 1 1 ro 1 O

o *l 00 +1 1 1 H 1 ( *>) 1 H 1 1 •M t in 1 1 1 1 OJ 1 00 CO Kl 1 1 1 1 1 1 1 1 1 1 1 1 ro OJ

t

c

o (Mm

o

o in

a

m

o

v • (M X <oc

in

in • ^ (M in

olOo

o

o

o in -o

in

sr fvj

o • »-

<Ni in (M

o

oo in

ro

o00

o in o «—

ro

in rin o fM o r^ o o <— o O o St oo o o in o o o ro -* o 1

ro

O >«• ro ro in

oo CO ro ro in ro * o ro «* t

o

o rvJ >*•

o

a.

(J

in

CO< <a111 X

ro CO

00 rj ro 1 <o

o in I 1 fM • o (M in >!• ro o

ooin

ro vO <M

in I nO

in

oCOo

o

ro

fVI

o

in in rs. ^ St (M ro fM fM

T

ro IM «M fM

c fM s^ fM s^

>-/ sv s^ s^

fM

IM

o

o =) CO ro fM

OO

Mo fM 00 vO T—

oo st 00 in fMo ro in

Z

ooO UJ •M H •H +1 h- +1 •H M fM 1 M +) o H fM +) -H CO in vt st in in z c St in O ro O ro O o ro V <s in o ID in m O vt ^. fs. in o O- u 0) (M lO st to X o ro o

ofM

ost

COo

stCo

H fM

-O

V

in

fM fM «- «— s-* s^

fs- ro o o

•H 00 ro

ofs- ro

fM

ro

fM fM sto o>

fM s^ S^ s^

>-/ s^

o>

O fM

oo

O fM

f— st fM fM

o

O •M +( +1

H +1

OO

o

O ro st in

o

ro

st

t

Oh

o

O

O CO O (/> GO +1 +1 •H z c o st

CO

«t ro X o

in

in

o sto in

rs. st in

IM

o

oo

fM ro 1 fM ro 1 00

+1 •H

o «- st

HH I1 1 • I in 1 1 -M 1 • fM

o inoO in ts.

o o> in

in ro -o ro

O O- fM o o O o r— o ro o 1 +1 1 I -M •H IM H •H 1 o> 1 O in V o ro vO CO o & fM rs! in z

O) o> o> O) O) D) o> o> o> O) O) O) O) O) o> cn O) O) \ sv •s. \ Ss s. s^ s^ ss. >^ s^ "«s o> O) Ui o> at O) O) cn CD O! o> a) CD cn 3 3 3 3 3 3 3 3 c s< c c c 3 3 c c 3 3 « c c c 3 S« c c c 3 3 c

0> O) D>

0> O) o> 3 3 3

(fl <(0

U 10 "D <U

—

00 CO CDUO

UU

oo 3 3 >. 3 O U O UJ . o 0> fM 10 •- 3 — V _J -1 -I XXX > C O

1566-1
8 8C

o *-l _l $ 01 o Ol. CO X o o o

1^c

rvj

c

(0

<uoo

o 00 1 1 ObN. 1 1 CO

Q CO o X u. > a. Ua: in o oc X < X zc *— CM t

c o 11 in 00 o

(D 1 o

(Uo ir>

X to >O C9

«— rvi

rvj CJ ><

a: </> 2 £ 8

(/)</)M

z:XX

OO CO

— <«

sOo

rj «- <o

CO toU CO —1 (/>

00

X

a.u5 c

<a

COc

(0

oo

:8

rvj

roo

w

w <^ %^

00

Os sr o o CM (M 1 1 t o O O 1 1 1 1 in 1 m I 1 -H 1 1 o o o 1 +( t 1 • 1 • 1 44 1 1 1 1 r- 1 1 1 1 V 1 <M I in CK lA

tn »

<^ *^

ru

mm fNJ fNJ fO \^ w

CVJ

o

o

o CO

om

o >o

CO • o

o 1 1 CsJ 1 t in in 1 «- o 1 t •H 1 1 o <*— in 1 in •H 1 1 V 1 1 m 1 V

in

fS

V

O (M

CNJ

COc

(/> z

LLI

</>

c

o lU U X

(Mo in -Jo

-* 00

o 5 c

(D

O

rvj oo

ro «-

in

o

00o

too

00

C71 CJI 0>

0> D> 0> 3 3 D *<

O) O) O)

O) O) C7) 3 3 3

UJ<a:aw

CO

d =5 CO MzLLI -H

(/> Z

C

o 10

o

IM

OO

O-*

in

O fV o o <r • >o o o> in o> sr 00 (Min

to

8:

vO

O

r— «

oo CO 00

o 00 fNJ in

ro f\j <o

o in

o in sr K> <> T— 00

od rij

O

oooo r\io 1 t o>

t 1 t 1 1 -o 1 1 o CO o in r>- • 1 1 1 1 1 1 • 1 1 in 1 >* fM 1 1 t 1 9 1 g 1 00

OO

N- in

o f\i 00 00 CM o

o in

oO <M N. (M

o

o

oO • • -*

in ro

o fM 00O ino fNJ OOo

O rvi (M O • in in fNJ in «- O -H +t •H +! +) +) o o •H «— in M in M V ^

o in V V o o in o o 00 V o 00 o a> O (M in

>0 N.

O CM 00

O.

u-i 1 1 1 1 ho ro CO < 1 1 1 1 ^ CM CO 1 1 1 1 ^ in lO in 00

0)

0>

4-> tac

0>oc

(0 a.—

B <u

(Q 9 4-> O

oo< >o1 c u CQ > c E c

a) 4-> i O (0 o u

L. a. z > a:

CM

oo CO osf o o

o

m +1

H +)

o z c 00 O in IS

<D 00 * 4) z

ino

CM

in

ro

o inV

O

o

•O fO

r— • «- CM

CM

in

00 3

o> O) a> O) o> CD O) o> O) o> O) o> a> o» O) O) CD s» Sn

o> *s *s V.

\ •ss »s >s •s. •V s^ •>s "s. -s •V, s^

a> O) at > O) O) O) O) cn O) o> o> O) O) a> O) c c 3 3 c c 3 3 3 c 3 c c c 3 c c 3 3 3 c 3 3 ^ "D J3

O. Q. Ol Q. oe ^ U

V <U •—

E (- (/>(/>(/></>(/>(/></>(/>

(0 ^ -C •—

—

3 > > 3

Si

>-

cc

IM tsl

1566-2
TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRM 1566 (revised 3/1/86J

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Total Folates (ug/g) As (ug/g) cont.

1.2 W 85TAN 01 1 12.1 1 HAA 85NAR 03

12.2 1.1 lENA 82GLA 02

Total Pantothenates (ug/g) 12.4 lENA a4Cl A 02

12.9 0.85 ICPES 01 10.2 W 85TAN 01 1 13 0.6 ITNA 01

13 1.2 ITNA 79K0B 03

Thiamine (ug/g) 13.1 0.3 HAA 83MAH 01

1 13.17 0.34 HAA 81UTH 01

5.1 W 85TAN 01 1 13.2 0.4 HAA 83MAH 04

13.4 0.3 HAA 84NAR 01 Protein (%) 13.9 0.52 AA 85SAK 01

14 3 ICPES 84NAD 01

41 .4 W 85TAN 01 1 15 3 NAA 85LEP 01 15.5 0.3 11 HAA 82JON 01 Nicotinic acid (ug/g)

]

15.87 3.5 ITNA 86CHI 01

101.6 W 85TAN 01 1 B (ug/g)

Vitamin B-6 (ug/g)

1

7 1 TCGS 82GLA 02

1.4 W 85 TAN 01 1 Ba fua/a)

Riboflavin (ug/g) < 4 NAA 85LEP 01 5.18 0.24 ICPES 84NA0 01

9.8 w 85TAN 01 1

.-

Br (uq/q)

Aq (uq/q) 1 45 1.4 ITNA 79K0B 03

0.86 0.09 lENA 86CHI 01 1 50.57 0.45 ITNA 86CHI 01 0.88 0.05 ITNA 84ALK 01 1 51.7 7.1 lENA 86CHI 01

0.89 0.02 FAA 850KA 02 1 52.9 3.3 lENA 86CHI 01

0.93 0.06 ITNA 86CHI 01 1 55 17 lENA 84GLA 11

1.14 0.13 ITNA 01 1 62.6 0.4 NAA 85LEP 01 3.6 0.3 ICPMS 85 PAR 01 1 180 EXRF 81 PAR 01

Al (ug/g) Ca fua/a)

231 9 FAA 86KRA 02 1 880 3370 R AA 80UCH 01

240 7 ITNA 8/^KRA 02 1 1200 400 CPXRF 85SIM 01

252 6 ITNA 86KRA 01 1 1200 400 NAA 85LEP 01 263 8 lENA 85GLA 02 1 1300 MPOES 85ZHA 01

291 24 ICPES 84NAD 01 1

1 ouu inn ICPES 84NAD 01 366 9 HPLC 85 BON 01 1 1300 200 ITNA 86KRA 01

1353 146 RTNA 01

As (ug/g) 1426 44 WXRr 84ALK 01

1499 6 ICPES 83CHA 01 9.2 0.6 ICPMS 85PAR 01 1 1500 100 ICPES 85UHI 02

9.7 ICPES 84MAR 01 1 1500 100 ICPES 84SUN 01

11.1 1.1 ICPES 830LI 01 1 1500 100 ICPES 84SUN 01

11.3 1 RTNA 85GAU 04 1 11.96 0.56 lENA 86CHI 01 1

1566-3
TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRM 1566 (cont.)

Cone Uncer Com Method Reference

Ca (ug/g) cont.

1510 20 11 ICPES 82 J ON 01 1530 30 11 ICPES 82J0N 01 1549 6 ICPES 83CHA 01 1738 153 ITNA 84ALK 01 4500 EXRF 81 PAR 01

:d (ug/g)

3.2 0.1 FAA 82SUZ 01 3.2 0.15 ICPES 84SUN 01 3.24 0.29 ASV 82SAT 02

3.25 0.05 6 ICPES 850KA 02

3.3 0.3 ASV 82GAJ 01 3.31 0.03 AA 850KA 02

3.4 14 FAA 80CHA 09

3.4 0.22 FAA 81CHA 01 3.43 0.07 6 ICPES 850ICA 02

3.49 0.01 IDMS 84BR0 03

3.5 0.5 AA 84ICAN 01 3.54 0.04 11 ICPES 82JON 01 3.6 14 FAA 80CHA 09

3.6 0.1 ICPES 84SUN 01 3.6 0.1 FAA 850KA 02

3.61 0.03 11 ICPES 82J0N 01 3.68 0.06 FAA 83DEL 01 4.7 1 ICPES 84NAD 01

:e (ng/g)

410 180 ITNA 86KRA 01 430 20 NAA 85LEP 01

CI (%)

0.827 0.007 NAA 85LEP 01 0.97 0.04 lENA 84GLA 11 0.98 0.02 ITNA 86KRA 01 1.011 0.05 ITNA 84ALK 01

Co (ng/g>

220 30 VOLT 84ADE 02

310 10 ITNA 84ALK 01 317 14 ITNA 86KRA 01 340 14 FAA 80CHA 09

340 14 FAA 80CHA 09

340 10 ITNA 86CHI 01 340 20 ITNA 79K0B 03

346 6 NAA 85LEP 01 370 10 FAA 850KA 02

Cone Uncer

I Co (ng/g) cont.

I 390 60

I 420 70

I 440 30

I 440 70

I 1200 100

I Cr <na/3)

I 340 90

I 540 310

I 550 60

I 600 100

I 600 200

I 620 30

I 650 50

I 680 20

I 700 200

I 720 70

I 750 100

I 750 120

I 750 120

I 1100 200

I 1450 310

I Cs (ng/g)

I 31 3

I 50 4

!

I CU (uq/q)

1

I 53

I 55

I 60 6

! 60 6.7

I 60.5 4.2

I 60.7 0,7

I 60.9 0.5

I 61

I 61 2.1

I 61.8 0.9

I 62.6 3.7

1 62.9 0.5

I 63

I 64 2.1

I 64.4 1

I 64.5 0.6

I 65

I 65

1 65.2 1.5

1566-4

Com Method Reference

lENA 86CHI 01 lENA 86CHI 01 SSMS 81BER 01 ITNA 86CHI 01 ICPES 81BER 01

11 ICPES 82 J ON 01

11 CPXRF 84SIM 01 ITNA 84ALK 01 SSMS 81BER 01

11 ICPES 82 J ON 01 NAA 85LEP 01 ICPES 84SUN 01 FAA 850KA 02 ITNA 79K0B 03

ILrtS Oh SUN Ul ITNA 86CHI 01

D CPXRF 84SIM 02

11 CPXRF 84SIM 01 ICPES 81BER 01

I Tilt OOK.KM U 1

NAA 85LEP 01 ITNA 84ALK 01

6 ICPES 83CHA 01 6 ICPES 83CHA 01 ICPES 84NAD 01 ITNA 84ALK 01

13 HPLC 85BON 01 6 ICPES 850KA 02

6 ICPES 850ICA 02 XRF 80SUZ 02

RTNA 82MUR 01

11 ICPES 82J0N 01 ICPES 84SUN 01

11 ICPES 82J0N 01 AA 80UCH 01 ICPMS 85PAR 01 AA 850KA 02

ICPES 81BER 01

14 FAA 80CHA 09

ICPES 84SUN 01

13 HPLC 85 BON 01
TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRH 1566 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

fua/a) cont

.

' "

1 H20- (X)

66 FAA 81BER 01 1 66 14 FAA 80CHA 09 1 2.6 GRAV 84NAR 01 67 2 SSHS 81BER 01 1 2.6 D GRAV 85NAR 03

69 14 ITNA 86KRA 01 1 7.3 W 85TAN 01 128 2 AA OlUCH nt 1 Ul 1 189 EXRF 81 PAR 01 1

' Cna/a)

1

I Hf (rig/g)

< 200 NAA 85LEP

1 01 1 80 8 NAA 85LEP 01

1 (nq/q)

1

1 Hg (ng/g)

13.9 0.7 NAA 85LEP

1 01 1 40 CVAA 84GLA 02

15 8 ITNA 86KRA 01 1 49 7 RTNA 84DRA 01 20 10 ITNA 79K0B 03 1 54 4 CVAA 86GAU 01

1 56 5 RTNA 84DEL 01

\"a/ at 1 58 6 7 RTNA 80GAL 02

1 60 ICPES 84MAR 01 4.9 0.5 ISE 83KNA 01 1 60 10 ICPES 84SUN 01 5.4 1.2 ISE 84GLA 02 1

1 Ho (nq/q)

1

1 < 200 NAA 85LEP 01

161 2.5 ICPES 84SUN 01 1 171 10 ICPES 84NAD 01 1 I (ug/g)

177 ICPES 84SUN 01 1 178 4 ITNA 79K0B 03 1 2.337 0.074 RTNA 80GVA 01

178 32 ITNA 86KRA 01 1 2.5 0.2 lENA 84 FAR 01

179 6 ICPES 83CHA 01 1 2.7 0.7 lENA 84GLA 11

180 6 ICPES 83CHA 01 1 2.79 NAA 79HEC 01 190.5 9 ITNA 84ALK 01 1 3.062 0.128 35 RTNA 81ALL 01

191 5 11 ICPES 82JON 01 1 3.209 0.134 RTNA 81STR 01

192 8 ICPES 81BER 01 1 3,209 0.134 34 RTNA 81ALL 01

193 4 SSMS 81BER 01 1 194 9 11 ICPES 82J0N 01 1 K (%)

196 6 11 ICPES 82J0N 01 1 198 14 FAA 80CHA 09 1 0.475 MPOES 85ZHA 01

200 4 13 HPLC 85B0N 01 1 0.8 0.15 ITNA 86ICRA 01

200 5 6 ICPES 850KA 02 1 0.82 0.07 ITNA 86CHI 01

201 3 6 ICPES 850ICA 02 1 0.86 0.03 lENA 86CHI 01

203 5 13 HPLC 85B0N 01 1 0.87 0.03 ITNA 79K0B 03

203 8 11 ICPES 82J0N 01 1 0.96 0.03 NAA 85LEP 01

204 2 AA 850KA 02 1 0.962 0.03 ITNA 84ALK 01

c\jy 9no AA 80UCH 01 1 u . yoj ICPES 85UHI 02

209 14 FAA 80CHA 09 1 0.9763 0.0301 WXRF 84ALK 01 210 4 NAA 85LEP 01 1 0.977 FE 80UCH 01

212.5 37 lENA 86CHI 01 1 0.98 0.02 11 ICPES 82J0N 01 218.9 9 ITNA 86CHI 01 1 0.98 0.04 11 ICPES 82J0N ,01 576 EXRF 81 PAR 01 1 1.01 0.06 ICPES 84NAD 01

1 1.89 EXRF 81 PAR 01

1566-5
TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRM 1566 (cont.)

Cone

La (ng/g)

Uncer Com Method Reference

330 110 ITNA 86KRA 01 /in U A A NAA DC 1 CD Ul

Li (ng/g)

323 6 AA 85EVA 01

(ng/g)

< 60 NAA 85LEP 01

Mg (ug/g)

980 30 ICPES 84NAD 01 1150 ICPES 84SUN 01 1200 100 ITNA 86KRA 01 1270 6 ICPES 83CHA 01 77 DTUik K 1 NA fiOUl ID OcnUK niU 1 1280 AA 80UCH 01 1310 20 ICPES 85WHI 02

1380 100 ICPES 84SUN 01 1410 20 11 ICPES 82JON 01 1430 6 ICPES 83CHA 01 1430 38 WXRF 84ALK 01 1430 40 11 ICPES 82J0N 01 1451 213 ITNA 84ALK 01

Mn (ug/g)

3 XRF 80SUZ 02

14 2 SSMS 81BER 01 14.5 FAA 81BER 01 15 1.2 ITNA 79K0B 03

15 2.4 ITNA 84ALK 01 15.3 0.15 ICPES 84SUN 01 16.1 1.1 ICPES 84NAD 01 16.57 0.97 lENA 86CHI 01 16.7 6 ICPES 83CHA 01 16.7 6 ICPES 83CHA 01 17 1 ITNA 86KRA 01 17.1 0.4 RTNA 82MUR 01 17.2 0.2 11 ICPES 82J0N 01 17.2 0.6 FAA 81CHA 01 17.3 0.3 6 ICPES 850KA 02

17.4 0.6 11 ICPES 82 J ON 01 17.4 0.6 6 ICPES 850KA 02

17.5 0.7 ICPES 81BER 01 17.8 0.9 11 ICPES 82J0N 01 17.9 0.42 ICPES 84SUN 01 17.9 1.3 ICPES 85WHI 02

Cone Uncer Com Method Reference

Mn (ug/g) cont.

18.6

19

19.3

2149

Mo (ng/g)

100

109

160

180

N (%)

6.62

(ug/g)

4200

4600

4700

4800

4800

4920

5030

5070

5082

5200

5300

9750

Ni (ug/g)

0.89

0.92

0.95

0.97

0.98

1.05

1.1

1.1 1.15

1.3

1.6

1.6

0.3

1.1 3

70

100

72

40

20

300

240

200

40

20

258

400

100

L

11

6

6

AA

AA

I CRMS

NAA

EXRF

ICPES

ICPES

COLOR

lENA FAA

W

lENA ITNA

ITNA ICPES

ICPES

FEITNA NAA

ITNA ICPES

ICPES

MPOES

850KA 02

80UCH 01 85PAR 01 85LEP 01

81 PAR 01

82J0N 01 82J0N 01 85EVA 02

86CHI 01 84G0H 01

85TAN 01

86CHI 01 79K0B 03

86CHI 01 83CHA 01 83CHA 01 80UCH 01 86KRA 01 85LEP 01 84ALK 01 84NAD 01 85WHI 02

85ZHA 01

POL 85UT0 01 0.04 11 ICPES 82 J ON 01 0.04 ICPES 84SUN 01 0.09 11 ICPES 82J0N 01 0.1 lENA 86CHI 01 0.02 VOLT 84ADE 02 FAA 81BER 01 0.17 ICPES 84SUN 01 0.02 FAA 850KA 02

0.1 SSMS 81BER 01 0.3 ICPES 81BER 01 0.5 NAA 85LEP 01

1566-6
TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRM 1566 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

' tufl/g) Rb (uq/g)

5600 200 ICPES 0*»NMU niU t1

1 3.8 0.5 ICPMS tJjrAK ni

6A20 150 11 COLOR A/ 1 f U

1 4.2 0.6 ITNA ookka U 1 6530 120 11 COLOR fi/. 1 f y ohL 1

N

ni 1

I 4.27 0.19 ITNA ooLnl ni

7000 100 ICPES O/ CI ly U 1 1 4.49 0.05 ITNA ni111 7057 231 WXRF OHnLK 1 4.6 0.1 NAA ni

7266 1144 lENA 1 5.04 0.1 lENA ooun 1 ni

7600 400 6 FAA 81 LAN 01 1 5.35 0.32 AA 85EVA 01 7700 100 ICPES 85WHI 02 1 20 EXRF 81 PAR 01 7700 400 14 FAA 84LIN 01 1 7800 100 CPAA OTUAC n? 1

1 S (ug/g)

7800 200 11 ICPES 1 7800 300 6 FAA R^O 1

1LMNAM

i 7977 248 WXRF AAA! ni

7800 500 14 FAA AAl OHL TM1 n ni 1 8700 200 WXRF 01

7900 100 11 ICPES ni 1

1 8700 200 CB AARnu 01

8100 900 14 FAA OhL 1 n 1 9600 200 ICPES A^UU o^wn T

1 8200 ICPES OHoUn o / CI ly

1 Sb (ng/g)

'b (09/g)

9.8 1.2 NAA niU 1 42® 20 14 FAA OHLUN 1 150 40 ITNA f TK.UD 444 40 FAA ni 1

1 400 300 ICPES 01

450 6 FAA o 1 n 1 n ni 1

1 450 6 FAA 01 1 Sc (ng/g)

460 50 14 FAA OHLUN 1 460 60 14 FAA OHLUN 15 2 ITNA 01

470 10 FAA O 1 LnM 1 69 ITNA AAni A 1

1

480 6 FAA OCKUl U B 1 71 3 ITNA 01

480 6 FAA O II n U nl U D 1 72 4 NAA ASl FP 01

480 10 FAA OcA 1 O

f\y Uc 1

1 79.5 ITNA AAHAII ni

480 20 FAA 1 89 6 ITNA f 7KWD

500 14 FAA 80CHA 09 1 508 20 ASV OtiGAJ ni 1 Ul 1 Se (ug/g)

508 200 11 ICPES 82JON 01 1 508 300 11 ICPES U1 1 1.6 0.4 NAA niU 1 518 14 FAA 80CHA 09 1 1.7 0.14 ICPES 84SUN 01 518 60 ASV 82SAT 02 1 1.7 0.2 ICPES 830LI 01 528 30 ICPES 84SUN 01 1 1.8 0.2 HAA 82MAY 01 548 10 ICPES 84SUN 01 1 1.94 0.07 ASV 84ADE 01 560 40 14 FAA ni 1 2 0.2 HAA 01

2600 200 ICPMS 85PAR 01 1 22.02

0.2

0.9

HAA

ITNA

85NAR

84ALK

03

01

>d (HQ/CJ) 2.04

2.05

0.04

0.05

lENA HAA86CHI

82JUL

01

01

< 2 RTNA 85BEM 01 1 2.07

2.1

2.18

2.21

2.22

0.03

0.2

0.25

0.08

0.03

11

11

FAA ITNA

GCITNA HAA

82JUL

84LAN

84SIU

86CHI

82J0N

01

01

01, 01

01

1566-7
TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRM 1566 (cont.)

Cone Uncer Com Method Reference

Se (ug/g) cont.

2.23 0.26 11 GC 84SIU 01 1 < 200 NAA 85LEP

2.26 0.24 CSV 83AHM 02 1 7.32 0.91 ICPES 84NAD

2.3 ICPES 84MAR 01 1 2.3 0.3 ITNA 86KRA 01 1 Tl (nq/q)

2.42 0.08 11 HAA 82JON 01 1 2.6 0.3 HAA 85CUT 01 1 < 5 ICPES 84SUN

Se(IV) (uq/q)

< 0.01

Se(VI) (uq/q)

< 0.01

Si (ug/g)

1100

Sm (nq/g)

63

76

Sr tuq/q)

100

157

HAA

HAA

ICPES

ITNA NAA

85CUT 01

85CUT 01

84NAD 01

86KRA 01 85LEP 01

8.58 0.42 ICPES 84NAD 01 9.87 0.35 6 ICPES 850KA 02

9.9 0.68 AA 85EVA 01 9.9 1.1 FAA 82SUZ 03

9.96 0.2 6 ICPES 850KA 02

10.5 0.3 AA 850KA 02

10.8 0.6 lENA 85GAU 04

10.99 0.76 lENA 86CHI 01 92 EXRF 81 PAR 01

Ta (nq/q)

5.5 0.6 NAA 85LEP 01

Tb (nq/q)

15 2 NAA 85LEP 01

Th (ng/fl>

52 2 NAA 85LEP 01

Cone

Ti (uq/q)

Uncer Com Method Reference

U <ng/g?„

112

117

126

129

1.64

2.316

2.44

2.5

2.67

2.7

2.8

2.9

3.1

Yb (ng/g)

Zn (ug/g)

716

730

746

750

805

805

822

824

843

848

848.5

850

18

0.05

0.006

0.06 11 0.2

0.4

0.3

0.4

0.6

500

30

10

2.2

7

36

4

9

12

5.7

4.5

14

6

6

11

IDMS

DNA

DNA

DNA

RTNA

IDMS

ICPES

ITNA COLOR

ICPES

SSMS

ICPMS

NAA

NAA

NAA

ICPES

NAA

ICPES XRF

ICPES

ITNA ICPES

ICPES

ICPES

ICPES

lENA

ITNA

83KEL 01 85GAU 04

84GLA 02

84GLA 1

1

82MUR 01 85 FAS 02

82J0N 01 86KRA 01 85EVA 02

81BER 01 81BER 01 85PAR 01 85LEP 01

85LEP 01

85LEP 01

84NAD 01 85LEP 01 84SUN 01 80SUZ 02

850KA 02

84ALK 01 850KA 02

85WHI 02

82J0N 01 84SUN 01

86CHI 01 86KRA 01

1566-8
1

TABLE 1566-2: INDIVIDUAL DATA FOR NBS SRM 1566 (cont.)

Cone Uncer Com Method Reference

Zn (uq/q) cont.

851 37 SSMS 81BER 01 851 43 ICPES 81BER 01 859 9 11 ICPES 82JON 01 860 AA 80UCH 01 860 6 AA 850KA 02

860 50 I CRMS 85PAR 01

869 8 11 ICPES 82JON 01 870 35 ITNA 79K0B 03

874 14 FAA 80CHA 09

878 15 11 ICPES 82J0N 01 880 14 FAA 80CHA 09

884.6 17 ITNA 86CHI 01 887.6 10 lENA 86CHI 01 2953 EXRF 81 PAR 01

I

1566-9
8lo c

ni

0)

uu 0£

u. > X <

in

vj- oo >* • o N- «* N- (M «- CM

z:o > u. UJ

</> a£ to < X —

CM «- ^ I X oCM «-

til

O fO 00 o

CM ro

in

c^XoCM

CM

o

cc

O

X

o

CM »- O 1^ N- O• lO

-O 00

a </> </)

tij a.o •«c

(0

0) 00 z

Xiw> o 01 (/>

-H z c

o <D

LUX3 c

in

ac

Of AA +1 M _ M (D COz

eeoiL<1—

111 u

o z

LU < _l Of

o.so z 1 «s >o

in 111 z

LEea<»-

c

M

=>

<A (/> z111

efl

M zo c u <a

<u z

CO

ro

in

^0

in

oroooV

00mro

omlO

00oo

o

OO

in

ooooH

/-X ^ ^

>J- ^ ^ ^

00 »- in

eo

>0o

CMo

+1

00

in

eo ^ ^\

«- CM ro

oro

CM

ro

CM

(y 00 • o 0> CM

ro

o

in in

eo »-

in

o «- ^ <0 o o CM

in

oo

ro COm

o

in

CM

CMo

CM

00o

in

^0

CMin

oo

-*

+1M

ro

o

in CM • <M

00o

o

ino

roo

ro

O- 0> CMor*. CMm oo in O

ro CO

CMo

CMoO

o

CM

O 1 o 1 1 00 1 CM

m

o 1 CM 1 • 1 d 1 CM CO 1 O 1 in

•H 11 1 -H 1 1 1 I o • roH CM ro+1 11 1 1 1 r— 1 1 -H 1 CK • 1 ro «- 1 1 -M 1 JCM N. ro CO in

in • CO ino 0C> in

ooCO

rooCM

oO ^- >!•o 00 CM CMO 00 «— CM \^ CM \^ O o

ro CM CM «— o O

oo

o

om CM 00o >o

o

o sf CM

o ro in ro CO in 1 » o o &• CO

+1 •« 'H -H CM -H -H I +1 CM

o +1 -M

MH

VV ro 1 t >* O o O vO 00

V 00OO •oo

o> ro o>

o

oo CM in CO in CM fO -* 00

o</>

00z c

o

o-

+1 CM

ro

o

+t o

CM

•H ro

00

00o

+1 o

oo

ro

mo

in

CO

o

-4-

tj) o> o> O) o> D) U) cn o> O) cn cn V, >^ "^

O) D) en D) O) O) O) a> O) O) U) at O) cn CD cn c 3 c c 3 3 C 3 c c c 3 3 3 c 3 3 c c c 3 c c 3 3 3 c

(A <u 1- (0 <a

D

o (_ cn 3 3 3 V 01 <u 1 oCM <0 O)

C

C

o < m 00 m u u U U (J u o o O U 11. 11. u. C3 -J _J Z Z Z z

1567-1
"8 8 «> 3: z I—

LUz c

3:

o

o

c

(0

0) < O a:

u- Q.

X > u-

!/> DC < X

m a: o X > I u-(/)u oc

O

OX >< oO Oi<J

X

T- in

oo

o 10 «- fM «-

o

00 «- «- o>

o

O • -H 00 O N- o o »-

00

COo

90

o

(Xl

^3

(/} </> LU

Cl. ^

4-> c0u

no

_i C/>

I— 2 H <LU

3:3mzOf

c

C/3 CO

COz c/> a:0u. c

(0 < 0

1—<00UJ

_l• Ol Ul

OM 0z 0 < 1 i>>. 010

UJ < _l 1—<

CQ< UJ I— z

CO3 O o c

01

(MOCO

oo

o

o

(\l

ino

to

to

00

ino

00 00

in

«-

o

00

in c^

o

COo

oo

in (M o>

Ok

«-

o

o «- «- 0 0 1^ 00 10 ro 0 in CO vO 0 0 0> CO 1 t\J 1 10 1 1 1 ro 1 1 0 1 0 0 11 9 ro 1 ro 1 1 in 1 1« 1 1 « 1 > 1 0 11 1

(\l 1 0- in 0 (\i CO 00

Kl

r

0 f\i

T

0! 0 0 0

-* >* ro r~ >o 1 in 0 1 0 0 1 1 0 1 1 1 0 1 1 0 N. 0 1 1 1 • 1 1 1 • • 1 1 0 1 *— ro 1 0 00 1 1 1 1 ro 1 1 ,—4

/~\ ^>

ro (M rj in >* ro (NJ ro \^ \^ \^

ro 00 CO 0 0 0 -0 >* 0 0

Kl 00 0 in 00 0 (M 0 in in C3

00 in 1 1 00 o> <M

+1 +) •H

H +1 +) 1 1 H 44 +1 On 0 1 1 0 0 0 in 0 ro 0

o« 0 ro 5 (M 0 0 0 <

3 C

CO

C

Z (D O 0) CJ Z

(M vt CvJ >0

ro «— in • • r»- in • • (M s# . • o ro r\J «- T- o o

oa

O) o> V. \ o> cn O) z 3 3 3 »< 3 3 3

-0 in 1 1 1 1 ro 00

to 1 1 1 1 ^ <\j CO < 1 1 1 1 in ro

(J in vO CO 8a.$u

COc

OJ CO

y

0) 4-*

u

*J 0 < vO

<a 1 C c u CD 0 V >

U- CL

cCEC <D

E

V 4->

E

(D (D (D 4-> 0 (0

4-' +J

u •*-> 0 0

1— (— a. z > c

(D01

o -H 00

00

oo

r\j o

o CMV

+1 d

o> O) ) o> a> O) cn cn \ \ \ O) o> cn u> at cn m cn cn o> cn 3 c c 3 3 3 3 3 c c 3 3 3 c 3 c c

i3 ^

o. o. cr: ^umwojEc-o)—

Mc/></)(/)(/>(/)c/>(/>(n I- 3 > c

IM

1567-2
TABLE 1567-2: INDIVIDUAL DATA FOR NBS SRM 1567 (revised 3/1/86)

Cone Uncer Com Method Reference

Total Folates (ug/g)

0.22

Total Pantothenates (ug/g)

3.1

Thiamine (ug/g)

2.5

Protein (%)

12.4

Nicotinic acid (ug/g)

14.7

Vitamin B-6 (ug/g)

0.72

Riboflavin (ug/g)

0.56

At (ug/g)

17

As (ng/g)

W

W

W

W

W

W

W

SIMS

85TAN 01

85TAN 01

85TAN 01

85TAN 01

85TAN 01

85TAN 01

85TAN 01

83RAM 01

< 30 L XRF 86GIA 01 5.4 0.5 RTNA 78GIL 01 5.4 0.5 7 RTNA 77GIL 03

5.4 0.5 7 RTNA 80GAL 02

5.6 1 7 RTNA 77GIL 03

5.6 1 7 RTNA 80GAL 02

5,6 1 RTNA 84DEL 01 5.7 RTNA 85TIA 01 6 0.3 HAA 85 YAM 01 6 1 H ICPES 82HAH 01 6.3 0.4 RTNA 84BYR 02

30 10 COLOR 77BUR 01

[ug/g)

1.5 TCGS 82GLA 02

Cone

Be (ng/g)

Bi (ng/g)

Br (ufl/g?

6.3

7.6

8.3

8.5

8.6

9.3

9.9

Ca (ug/g)

Uncer Com Method Reference

30

0.4

0.7

1.4

1.5

ICPES

ICPES

CPXRF

lENA

ITNA XRF

lENA

ITNA

ITNA

82KUE 01

82HAH 01

84BIS 01 84GLA 1

85GAU 04

86GIA 01 85GAU 04

86GAU 01 78GIL 01

1 in OHD 1 o U 1 i7n CM ojwn ocmlj I

1 n?

17X 1 ( J JO AA R1O i VAC T Mo U 1 ML1 f H 1 u Ai\ r OOU I M ni

179 38 AA 81 YAS 01

181 38 AA 81YAS 01 183 38 AA 81 YAS 01 193 ICPES 81W0L 01 194 6 11 ICPES 82 J ON 01 195 2 6 ICPES 82KUE 01 195 3 6 ICPES 82KUE 01 196 2 6 ICPES 82KUE 01 197 38 AA 81 YAS 01 198 5 1 ICPES 81U0L 02

199 38 AA 81 YAS 01 199 4 11 ICPES 82J0N 01 204 1 ICPES 81W0L 02

208 34 FAE 83MAR 04

217 9 12 FAA 85CAR 02

Cd (ng/g)

20 ASV 82GAJ 01 29 4 ASV 82SAT 02

30 1 7 RTNA 80GAL 02

30 10 FAA 80SCH 08

30 20 6 ICPES 82KUE 01 30 20 6 ICPES 82KUE 01 30 20 6 ICPES 82KUE 01 31.7 1 RTNA 84BYR 02

32 3 ICPES 83SCH 04

40 10 11 ICPES 82J0N 01 50 30 11 ICPES 82J0N 01

1567-3
TABLE 1567-2: INDIVIDUAL DATA FOR NBS SRM 1567 (cont.)

Cone

Ct (ug/g)

Uncer Com Method Reference

570 50 lENA 84GLA 11 580 30 ITNA 85GAU A/04

600 30 ITNA 84GLA 4 4 11 615 ITNA 86GAU A401

Co tng/g)

21 4 ITNA /^oGIL 01

1970 280 RTNA 84BYR 02

Cr (nq/g)

< 250 L ICPES 82iaJE 01 < OCA 250 L ICPES 82<UE 01 < 250 L ICPES 82KUE 01 < 300 L XRF 86GIA 01 225 100 FAA 85CAR 01

240 10 FAA 83CAR 02

300 4 AA 100 1 1 ICPES 82J ON A 4 01 400 OAA 200 1 1 ICPES 82J0N 01 760 160 P A E FAE OTZu A n HjMAk o/Oh

Cs (ng/g)

< OAA 200 L ITNA DOOl A OiiiGLA 0^

f Tfcl A ITNA cSoGAU 01

Cu (ug/g)

1 .6 A ? O.i IT A A FAA OC A D

0<c

1 .78 RTNA OC T T A BbTIA 01

1 .8 ASV 83H0L 01

1 .8 A 4 0.

1

CPXRF 84BIS A401

1 .8 A O 0.2 1 1 ICPES 82 J ON 01

1 .88 A 4 0.12 XRF 86GIA Ai01

1 .9 A O 0.2 11 ICPES 82J0N A 4 01

1 .95 A A1 0.02 RTNA 84BYR 02

2.00 0.01 6 ICPES 82KUE A401 2.0 0.1 ICPES 81KNA 01 2.0 0.2 7 RTNA 80GAL 02

2.0 0.2 RTNA 78GIL 01 2.0 0.2 2 FAA 84MIL 01 2.0 0.3 ICPES 80SCH 08

2.0 0.6 2 FAA 84MIL 01 2.02 0.08 1 ICPES 81W0L 02

2.035 0.007 IDMS 84BR0 03

2.04 ICPES 81W0L 01 2.06 0.03 6 ICPES 82iaJE 01 2.06 0.04 6 ICPES 82ICUE 01 2.08 1 ICPES 81U0L 02

Cone Uncer Com Method Reference

Cu (ug/g) cont.

2.2

2.6

2.6

F <ng/fl?

40

Fe (ug/g?

11.5

14.8

15.2

16.2

16.7

17

17.1

17.1

17.2

17.5

17.7

17.9

18

18.4

18.4

18.6

18.7

19.3

19.6

19.6

23.6

Ge (ng/g)

H20 (%)

9.8

H20- (%)

11.5

11.5

0.1

0.2

1

200

20

12

ICPES 83SCH 04

FAE 83MAR 04

FAA 85CAR 02

ISE

ISE

84GLA 02

83KNA 01

6.1 12 FAE 83MAR 04

1.2 2 FAA 84MIL 01 0.5 12 FAE 83MAR 04

0.5 2 FAA 84MIL 01 3.8 12 FAA 85CAR 02

1 11 ICPES 82JON 01 0.8 11 ICPES 82J0N 01 4.8 XRF 86GIA 01 0.6 ITNA 78GIL 01 1.2 CPXRF 84BIS 01 0.7 6 ICPES 82KUE 01 0.8 11 ICPES 82J0N 01

1 11 ICPES 82J0N 01 0.8 1 ICPES 81U0L 02

1 6 ICPES 82iaJE 01 1.2 ICPES 80SCH 08

2.1 6 ICPES 82)aJE 01

1.1 ICPES 81KNA 01

1 ICPES 81U0L 02

ICPES 81U0L 01 3.9 12 FAA 85CAR 02

20 L ICPES 82HAH 01

W 85TAN 01

GRAV 84NAR 01

D GRAV 85NAR 03

1567-4
TABLE 1567-2: INDIVIDUAL DATA FOR NBS SRM 1567 (cont.)

Cone

Hg (ng/g)

Uncer Com Method Reference

< 60 L XRF 86GIA 01

1 0.3 7 RTNA 80GAL 02

1 0.3 RTNA 78GIL 01 1.08 0.15 RTNA 84DEL 01 1.22 0.16 RTNA 84BYR 02

(ng/Q)

1.97 0.28 RTNA 84BYR 02

9 5 lENA 84GLA 11

K <ug/g)

100 20 FAE 83MAR 04

1061 114 12 FAA 85CAR 02

1130 190 ICPES 85UHI 02

1220 130 XRF 86GIA 01 1240 30 2 FAA 84MIL 01 1260 30 2 FAA 84MIL 01 1300 50 11 ICPES 82J0N 01 1310 40 11 ICPES 82J0N 01 1320 10 6 ICPES 82KUE 01 1320 10 6 ICPES 82KUE 01 1320 60 1 ICPES 81U0L 02

1330 20 6 ICPES 82iaJE 01 1392 37 ITNA 78GIL 01 1500 1 ICPES 81W0L 02

1583 34 CPXRF 84BIS 01

La <ng/g)

1.8

Li (ng/g)

41.4

(ug/g)

0.3 RTNA

AA

86TSU 01

85EVA 01

370 20 ICPES 85WHI 02

373 11 2 FAA 84MIL 01 378 8 2 FAA 84MIL 01 397 14 1 ICPES 81U0L 02

398 10 6 ICPES 82KUE 01 406 3 6 ICPES 82KUE 01 408 1 ICPES 81W0L 02

419 4 6 ICPES 82KUE 01 420 10 11 ICPES 82J0N 01 429 9 11 ICPES 82J0N 01 466 5 SIMS 83RAM 01

Cone

Mn (ug/g)

5.7

6.7

7.2

7.9

8

8.2

8.2

8.3

8.3

8.3

8.3

8.55

8.58

8.6

8.6

8.63

8.67

8.7

8.8

9.2

9.6

9.7

9.9

Mo (ng/g)

310

380

390

400

420

420

420

430

470

N (%)

2.2

Na (ug/g)

9

10.4

12

13

Uneer Com Method Reference

0.8 12 FAA 85 CAR no02

1.2 AE+AF 82G0L 01

1 ICPES OCl III T 85WHI 02

0.2 2 FAA 84MIL 01 0.4 11 ICPES 82JON 01 0.3 11 ICPES 82JON 1 1.8 XRF 86GIA 01 ICPES 81W0L 01 0.03 RTNA 84BYR 02

0.2 ICPES BOSCH OS

0.2 11 ICPES ocJOH U 1 0.15 6 ICPES o<:KUc Ul

0.16 6 ICPES 82KUE Ol ITNA 85GAU 04

0.4 ITNA 78GIL 01 0.38 1 ICPES 81U0L 02

0.12 6 ICPES 82KUE 01

1 ICPES 81U0L 02

0.5 ICPES 83SCH 04

1.4 CPXRF 84BIS 01 3.1 12 FAA 03CAK

0.4 2 FAA Of M T 1 U 1 0.5 ICPES O iK.roA U 1

RTNA 85TIA 01 30 6 ICPES 82KUE 01 90 11 ICPES 82JON 01 40 6 ICPES 82KUE 01 20 RTNA 84BYR 02

40 6 ICPES 82KUE 01 70 11 ICPES 82JON 01 63 COLOR 85EVA 02

70 RTNA no

W 85TAN 01

20 ICPES 85UHI 02

0.8 FAE 83MAR 04

2.5 ITNA 78GIL 01 ITNA 84GLA 11 3 ITNA 85GAU 04

1567-5
TABLE 1567-2: INDIVIDUAL DATA FOR NBS SRM 1567 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ni (ng/g) Sb (ng/g)

< 500 L ICPES 82KUE 01 1 < 2 L ICPES 82HAH 01

< 500 L ICPES 82iaJE 01 1 1.7 0.08 RTNA 84BYR 02

< 500 L ICPES 82KUE 01 1 38 1 RTNA 78GIL 01 no OU WD C XRF 86GIA 01 1 160 40 11 ICPES 82JON 01 1 Sc (ng/g)

175 FAA 85L0N 01 1 200 40 11 ICPES 82J0N 01 1 0.5 ITNA 84GLA 11 230 POL 83H0L 01 1 0.67 ITNA 86GAU 01 1500 100 CPXRF 84BIS 01 1 Se (ug/g)

P (ug/g?

0.7 FAA 81MEY 01 150 ICPES 85UHI 02 1 0.76 0.08 1

1

HAA 82J0N 01 1350 20 6 ICPES 82ICUE 01 1 0.82 0.08 ICPES 81W0L 01 1370 10 6 ICPES 82KUE 01 1 0.87 HAA 81 HAH 01 1370 50 11 ICPES 82J ON 01 1 0.87 0.06 H ICPES 82HAH 01 1390 50 1 ICPES 81W0L 02 1 0.901 0.051 HAA 80RAP 02

1400 10 6 ICPES 82KUE 01 1 0.91 0.03 11 HAA 82J0N 01 1420 30 11 ICPES 82 J ON 01 1 0.92 0.06 XRF 86GIA 01 1450 1 ICPES 81W0L 02 1 0.94

0.95

0.08

0.04

HAA GC-MS83K0L

81REA

0102

Pb (ug/g) 0.96

0.98

0.08

11

HAA

HAA

81MEY

85PIW

01

01 < 0.02 ASV 82GAJ 01 1 1 CSV 81 HAN 01 < 0.1 L ICPES 82J0N 01 1 1 0.1 HAA 85YAM 01

< 0.1 ICPES 82J0N 01 1 1 0.1 HAA 85NAR 03

< 3.8 L ICPES 82KUE 01 1 1 0.1 HAA 80V IJ 01

< 3.8 ICPES 82KUE 01 1 1 0.1 11 XRF 80RAP 01 < 3.8 ICPES 82KUE 01 1 1 0.2 HAA 85NAR 01

< 100 XRF 01 1

1 1 0.2 HAA 81REA 01 0.018 0.003 ASV 82SAT 02 1 1.03

1 .04

0.04

0.01

HAA

EXRF

81 HAN 80RAP0103

Rb (ug/g) 1.05

1 .05

0.09

0.09

7

7

RTNA

RTNA

77GIL

80GAL

03

02

0.93 0.13 AA 85EVA 01 1 1 .05 0.09 7 RTNA 77GIL 03

0.94 0.06 XRF 86GIA 01 1 1 .07 11 HAA 85PIU 01 0.99 0.16 ITNA 01 1

1 1 .08

1 .09 0.11 7

ICPES

RTNA

84MIA

80GAL

0102

S (ug/g) 1.1

1.1

0.02

0.02

11 XRF

XRF

80RAP

81KNA

01

01

1623 32 CB 1 1.1 0.09 ICPES 85NAK 01

1780 60 WXRF 86B0W 01 1 1.1 0.1 HAA 84NAR 01

1790 D CB 85JAC 01 1 1.11 0.05 RTNA 78GIL 01

1790 100 6 CB 84JAC 01 1 1.12 0.01 7 RTNA 77GIL 03

1810 D CB 85 J AC 01 1 1.12 0.01 ITNA 80GAL 02

1810 70 6 CB 84JAC 01 1 1.12 0.01 ITNA 78GIL 01

1830 140 CB 86B0W 01 1 1.17 0.15 RTNA 84DEL or

1860 50 ICPES 85UHI 02 1 1.17 0.18 7 RTNA 80GAL 02

1980 210 CB 84GLA 11 1 1.17 0.18 7 RTNA 77GIL 03

1567-6
TABLE 1567-2: INDIVIDUAL DATA FOR NBS SRM 1567 (cont.)

Cone

Sm (ng/g)

0.82

Sn (ng/g)

•«

Sr (ug/g)

0.82

0.97

1.02

1.08

Tt (ng/g)

2

3

3

u <ng/g)

< 0.95

V (ng/g)

0.05

20

0.04

0.2

0.06 1

10.24

Reference | \t\Jt Iw LI i\c 1 CI cri iwc

_____ ____

1

1 (ug/q; —

!\ 1 NH 86TSU

1 01 1 Oy. 1

1 DTUA OHDTK fi/DVp n?

1 O 0 KfmJ r HM aamti ni

1 in n 1 a V^r Co o^vfn I yjc.

1 in 7 I rPFC oiuni ni

L ICPPS 82HAH 01 1 10 3 0 L XRF Ai\ r uuu in u

1 0 7 1

1 I l.r kO o 1 nuL

1 10 5 0 7 1

ICPES 8? JON 01

1 10.6 0.4 ICPES 83SCH 04

XRF 86GIA 01 1 10.6 0.4 11 ICPES a?JON 01 AA 85EVA 01 1 10.6 0 5 11 ICPES a?JON fli

1 ICPES 81W0L 02 1 10 6 0 7 111 1 ICPES a?JON 01

1 ICPES 81W0L 02 1 10 a 1

1 1 C^O Aluni n?

10.88 0.56 ITNA 78GIL 01 10.9 0.1 6 ICPES 82KUE 01

10 ? Ao 1 Ur C O ft7i^iiF ni

11 ASV O/ lie ni 1 Ul 1 11 0.4 ICPES 80SCH 08

11 ASV 84LIE 01 1 11.1 0.4 6 ICPES 82KUE 01

11 ASV 84LIE 01 1 11.3 1.1 ICPES 81KNA 01

11 ASV 84LIE 01 1 12.6 1.3 2 FAA 84MIL 01 13.8 1.8 CPXRF 84BIS 01 14.8 4.2 12 FAA 85CAR 02

DNA 86GAU 01 1 35 DNA 80GLA 04 1

< 50 L ICPES 82J0N 01 11.2 1.2 RTNA 84BYR 02

11.3 COLOR 85EVA 02

1567-7
X

a:

LXJ U- < ae

X

OfX 8 cC o eo

u-t

o

to (M

in

>0

"8cHc

<D

<l> X >s. ro

"8

0)

c

'>

t_

Q</>

(/) UJ

Q. +1 3 O _i c

0) lUo

oe00

c

inz o OfMM •H CO X c

(0 o: <u o<1—<OOlU—1

UJo *—< z

a. ««: s

a£z s < in »—< o

lU

UJ —J

ca<1—

w

Z3

U)

Q

Z (O LU

C/i Z -H o c

(0

0)

o

u- UJ OS < < X II. < > 3 s

UJ z: -J o Q. < ac

UJ UJ

I/) < 5 ><u

UJ z 2 3 CO 5

LU u. < Q£

uX

(M

M rg cj »- »-

M «- >4-

K

LTl t

-4- OoHOoo

to

in «—m• o fvj to

(NJ

00

>0

00V00

otoo

«—

o

o

rvj

mo to

00 >o

m

o

O N-

-H fM -H in o o o o

o

•O 00

rvi oo

eoo

CO

V* 00 lO

o

ooo

o

OO

OoH

oin

min

eoo

<^ 4^

CM >! in CM f\J w \^ o tvi >*

o to

inoo in

oo CNj « « o 1 00 1 1 in I H CM H 1 1 B 1 1 -H H

rj

D 3 00 * 1 0 CO V <^ in rj CO lO o fV

(M

in «— eo T- +1 «- V V 5

CM rvj CO

o -4-o 00 in 1^ 35o

o to

o fM fM fMO CO lO 0 fM 1 fM 1 (> 1 1 <d m fM 1

f*J i m

a O 1 o 1 oo

a O 11 1 1 1 1 1 o 1 1 d 1 1 1 o> 1 o 1 o 1 ^1 o 11 1 vO 1 o

O to (M oo 00o in in in

fM >0 in in

o

o >*• (>

O r— o O CO 00 CO o 1 CO 1 1 o

o -O 1 o >* OJ to o 0 1 1 1 00 O CM fM 1 fM 1 1 1 1 o in fM 1

to N- to to CO fM >s- fM in in

o in in

•i

!^

v~

O fM

oo CO lO CO o o fM

o CO «

fM z—

OoO

oo o> fOo

O

t 1 O 1 fM «- LA

HH t-l +1 "V-f fMH 1 • o -H 1 +1 •HM

H +)H +1 +1 1 1 V 1

eo h- 00

o

oV COO to (\J

O in to »

too in O-

(\J fM COo

o

v>

CD

COc

(0

oinMO

ofMO fM

OfM

toO

fM

CM

OH

CO

oMO

ofMOfM

OOfM

HO

^0'

O

CJ) cn en u> cn CD 1 O) CJ) CJ) O) CD O) CJ) CJ> CJ) D) CJ) CJ) CJ) O) o> cn cn cn cn cn cn

t—

\ •V.

\\\\ >^ V.\\

\ 1—«

en o> CJ) P) u> cn cn CJ) CJ) CJ) CJ) CJ) CJ) CJ) CJ) cn cn cn O) CJ) cn cn O) cn UN 3 c 3 c 3 3 3 c c 3 c c c 3 3 3 c 3 3 c c c 3 3 3 3 3 3 c

LE

CO L. (0 CO T3

o L. (A 3 3 3 ID 1 ofM O) cnC

o (0 UJ S < CO m CO o o O O O o CJ O U O U 11. u. u. C3 3: 3: 2: s: 31 Z Z z

1568-1
X

u 8 c

(D«)

O

ooo

V

1,

UJ 9> o 2C

<D < X

Of

<M (M -*o M 00 Oin

o

-o~

olA

Xo >

(MV

O-J

cwo

OCO

u.

mo in

UJ CMo LU Q. H 1 1 o 1 1 o 1 1 1 t 1 1 o •H I (M 1 1 1 1 +1 >^ c 1 1 >«• 1 ( 1 1 1 1 1 o O V « roov~

ro inz c

(A eM fSJ 00 fM\^

CO

IBQ z (/)

O

d: inO CM

o

H 1 1 (\j 1 >3- 1 1 1 1 00 (NJo u. z 1 1 A •H 1 1 t 1 • r>j c 1 1 t 1^ o 1 1 1 1 o NO < (D O 1- 0) < X aoUJ

_j

oom to

Q.o f\jO in GO

UJ roo (M

uo 1 1 1 1 1 1 z 1 1 1 1 1 1 1 1 1 1 1 1 1 < 1 1 1 1 1 1 o o in o N- o in CO >o ru OJ 00

N-'

o «— tn

r—

UJ z _l < 00 m o (\l o 1 1 O 1 1 1 1 1 1 < o >o 1 1 00 t 1 1 1 1 1 UJ <o 00 ro 1 1 fO I I 1 1 1 1

V)

z>

(/>

o

Z (/> UJ

(/> Z -H oo c

<D

•O (Vi CO V*- ^\ ^ ^ ^ >o

N-'

W ^ oHO

<\j lO

o

o

o

00

oin

to

in o>o

oin

o

oOn

ooo

ro

V

0>

00

o

Z3

C

(/) ^

UJM

C z m O «> U 3C

c/> 00

»vi eo Nj- o ro «- 00

IS. in

ro

«-

o

0)0 0) o> O) O) 3 3 30)0)0)

O) O) O) 3 3 3

rS

in

o in to 00

(\i 00 in to >0 00 8a.

CO

0)

"o

(DO

tocc

a. < I COc E

ni —

o

<D 4-»

E

M

P (D ^

I— I— I— a. z > Of

o

CDz c

ID

01

H

Oo

fVI V

0)0)0)0)0)0)0)0)0)0)0)0)0)0)0)0)

0>0)0)0)0)0)0)0)0)0)0)0)0)0)0)0> 3 3 CCCCCCCC3

a. a. o£ </)(/>(/>(A(/>(/>(/)h- 1- 3 > c

c

IM rsi

1568-2
TABLE 1568-2: INDIVIDUAL DATA FOR NBS SRM 1568 (revised 3/1/86)

Cone Uncer Com Method Reference 1 Cone uncer Com Method Reference

Total Folates (ug/g) 1 As (ng/g) cont -

0.21 W 85TAN 01 ! /in 1 H lu HAA 84IKE 01

1 /.in

1 H lU on 7 RTNA 80GAL 02

Total Pantothenates (ug/g) 1 /.in

1 H lU on 11 HAA 81 RAP 01

1 /in

1 HlU 7n 11 HAA 81 RAP 01 3.8 W 85TAN 01 1 /in

1 hIU 7nf U HAA 81KNA 01

1 / on

1 'tdv on HAA 84NAR 01 Thiamine (ug/g) 1 ' / on onyu XRF 86GIA 01

lO HAA 82TAM 01 1.4 85TAW 01 HAA 83KUM 01

1 //n H ICPES 82HAH 01 Protein (%) ou HAA 85NAR 03

1 452 70 ICPES 81U0L 01 8.4 w 85TAM 01 1 460 70 lENA 82GLA 02

1 HOf 1

1

1 1 RTNA 84BYR 02

Nicotinic acid (ug/g)

15.7 w 85TAN 01

1 ^ 1 L TCGS 82GLA 02

Vitamin B-6 (ug/g)

\ Bi (ng/g)

1.4 w 85TAN 01

1 ^ oO L ICPES 82HAH 01 Riboflavin (ug/g)

1 or lua/g^

0.33 w 85TAN 01

1 n 07 1 U B TC lENA 84GLA 11

Al (ug/g) 1 1 10 nU 171 f XRF 86GIA 01 n DR ITNA 78GIL 01

115 SIMS 83RAM 01

1 ca (ug/g)

As (ng/g)

1 Qi;

1 / CPXRF 84BIS 01

41 2 RTNA 84DEL 01 s ion Tn ICPES 85UHI 02

90 10 COLOR 77BUR 01 1 I'ZC

1 '''^ / FAE 83MAR 04

320 40 11 HAA 82J0N 01 1 loo c3 12 FAA 85CAR 02

370 ICPES 84MIA 01 1 ' I/O

1 Ihc z ICPES 81U0L 01 380 20 7 RTNA 77GIL 03 1 1/A 38 AA 81YAS 01 387 RTNA 85TIA 01 D 1/C 38 AA 81YAS 01 390 30 HAA 85YAM 01 1 1 / X 38 AA 81YAS 01 390 70 7 RTNA 77GIL 03 1 1AA 38 AA 81YAS 01 390 80 7 RTNA 77GIL 03 1 148 3 11 ICPES 82J0N 01

400 10 RTNA 78GIL 01 1 148 5 11 ICPES 82J0N 01 400 10 FAA 84XIA 01 1 1A9 38 AA 81YAS 01 400 10 7 RTNA 80GAL 02 1 151 38 AA 81YAS 01

400 10 11 HAA 81 RAP 01 1 158 14 XRF 86GIA 01

1 160 10 ICPES 85LY0 01

1 162 10 12 FAA 85CAR 02

1568-3
TABLE 1568-2: INDIVIDUAL DATA FOR NBS SRM 1568 (cont.)

Cone

Cd (ng/g)

Uncer Com Method Reference

20 ASV 82GAJ 01 25 2 ASV 82SAT 02

27 2 IDMS 84BR0 03

28 2 ICPES 83SCH 04

29 9 7 RTNA 80GAL 02

29.8 1.4 RTNA 84BYR 02

30 10 FAA 80SCH 08

40 20 11 ICPES 82J0N 01 60 30 11 ICPES 82J0N 01

CI (ug/g)

220 ITNA 86GAU 01 238 ITNA 84GLA 11 246 11 lENA 84GLA 11 248 ITNA 85GAU 04

Co (ng/g)

16.8 3.8 FAA 84B0R 01 18 2 ITNA 78GIL 01

21 10 RTNA 84BYR 02

Cr (ng/g)

< 400 L XRF 86GIA 01 80 80 11 ICPES 82JON 01 200 200 11 ICPES 82J0N 01 430 70 FAE 83MAR 04

Cs (ng/g)

< 200 L ITNA 82GLA 02

Cu (ug/g)

1.76 0.1 CPXRF 84BIS 01 1.86 0.03 RTNA 84BYR 02

1.87 0.11 11 HPLC 85ICH 01 1-9 0.2 12 FAA 85CAR 02

1.9 0.2 11 ICPES 82J0N 01 1.9 0.2 11 ICPES 82J0N 01 1.95 0.09 11 HPLC 85ICH 01 2.01 0.01 ICPES 81U0L 01 2.1 RTNA 85TIA 01 2.1 0.1 ICPES 81KNA 01 2.1 0.2 ICPES 80SCH 08

2.13 0.06 IDMS 84BR0 03

2.2 0.13 7 RTNA 80GAL 02

2.2 0.13 RTNA 78GIL 01

Cone Uncer Com Method Reference

Cu (ug/g) cont.

2.2

2.2

2.21

2.3

2.4

2.8

F (ng/g)

180

200

Fe (ug/g)

5.6

6.4

7

7.1

7.3

7.6

7.8

8

8.85

9.06

9.1

9.1

9.4

9.7

11.2

Ge (ng/g)

H20 (%)

9.9

H20- (%)

12

12

Hg (ng/g)

5.6

6.4

6.4

6.4

6.8

0.2 2 FAA 84MIL 01 0.3 ICPES 83SCH 04

0.22 XRF 86GIA 01 0.2 FAE 83MAR 04

0.1 2 FAA 84MIL 01 0.3 12 FAA 85 CAR 02

T CP ODKTin U 1

1 CP OhuLM

0.9 2 FAA 01 0 6 12 FAF 83MAR 04

0 3 2 FAA WHPl 1 1. 01

0 4 1

1

1 1 Trppc i V«r CO 01

0 4 1

1

irppc 01

n A 1 1 1 l«r CO 01

1 1 1 CO Rp inw 01

1 ICPES 80SCH 08

0.94 ITNA 78GIL 01

1 ICPES 81W0L 01 0.9 ICPES 85LYO 01 1.2 XRF 86GIA 01 0.3 ICPES 81KNA 01 2.7 12 FAE 83MAR 04

0.7 CPXRF 84BIS 01

20

80

0.5

0.5

1

11.05

ICPES

W

GRAV

GRAV

XRF CVAA

RTNA

RTNA

RTNA

RTNA

82HAH 01

85TAN 01

85NAR 03

84NAR 01

86GIA 01 81KNA 01 84DEL 01 78GIL 01 80GAL 02

84BYR 02

1568-4
Cone

I (ng/g)

TABLE 1568-2: INDIVIDUAL DATA FOR NBS SRH 1568 (cont.)

Uncer Com Method Reference

lU.y \.c. DTU A K 1 NA fl/. DVD

1

1

1 K 1 NA OTA 1 1 U1

1 1 o

T ERil A IcNA O/ f^l A o<»GLA 1

1

n = 1 »

1 03 nTki A kTNA 0 1 A 1 R BIALL u \

4

1 DTU A Kl NA Di A 1 Q Ul

K (ug/g)

900 100 FAE 83MAR 04

965 11 ICPES 81W0L 01

Vf u ICPES OCI lu t

995 48 cr A A FAA DC^ A n

lOoO C A A FAA o/ u r 1 ci^MI L 01 nuo r A A FAA Q/ U T 1 OhMI L Ul

1125 16 ITNA 78GIL 01 1140 30 11 ICPES 82JON 01 1150 80 11 ICPES 82J0N 01 1239 28 CPXRF 84BIS 01

1lOU An ART OOuiA niU 1

T TDCTC 1 LrCd Ojmn \ n?

LQt\ ni

3 1 u in1 u 1 1

U 1 ni

I? y u 7n 1 1 ni

O

070 AU ni

Mn (ug/g)

io 1 It. B nu.yo 1

1

1 1 ft? insj niU 1

It. J 1 c. C A A ft/ Mf 1 niU 1

It . f n A T PDCC 1 Lrto nA

It .O 1.3 1 Lrtd ftRi vn niU 1 19.9 0.4 ICPES 81U0L 01 19.95 0.69 ITNA 78GIL 01 20 3 ICPES 80SCH 08

20.1 0.3 11 ICPES 82J0N 01 20.2 0.5 11 ICPES 82J0N 01 20.7 1.4 ICPES 85WHI 02

20.8 0.4 12 FAA 85CAR 02

21 0.4 12 FAA 85CAR 02

21.4 1.4 ICPES 81KNA 01 22.1 0.7 RTNA 84BYR 02

22.1 2.8 XRF 86GIA 01 22.4 0.9 2 FAA 84MIL 01 25.8 1.1 CPXRF 84BIS 01

Cone

Mo (ug/g)

1.59

1.59

1.6

1.61

1.68

1.5

Ma Cug/g)

6

6.4

6.9

10

Ni (ng/g ?

Uncer Com Method Reference

0.07

0.09

0.13

0.18

11

11

ICPES 82J0N 01 ICPES 82J0N 01 ICPES 81U0L 01 RTNA 85TIA 01 RTNA 84M0K 02

w

20

1.6

0.4

85TAN 01

ICPES 85UHI 02

FAE 83MAR 04 ITNA 84GLA 11 ITNA 78GIL 01 ITNA 85GAU 04

150 20 11 ICPES 82JON 01 160 30 11 ICPES 82J0N 01 165 FAA 85LON 01 180 60 XRF 86GIA 01 2000 100 CPXRF 84BIS 01

P (ug/g)

1420 2 ICPES 84PRI 01 1600 60 11 ICPES 82JON 01 1600 100 ICPES 85LYO 01 1630 30 11 ICPES 82JON 01 1680 40 ICPES 85UHI 02

Pb (ng/g)

< 100 L ICPES 82JON 01

< 100 L ICPES 82J0N 01 30 ASV 82GAJ 01 35 4 ASV 82SAT 02

100 90 XRF 86GIA 01

Rb (ug/g)

7.27 0.21 ITNA 78GIL 01 8.2 0.8 CPXRF 84BIS 01 8.4 0.9 XRF 86GIA 01

1568-5
TABLE 1568-2: INDIVIDUAL DATA FOR NBS SRH 1568 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

S (UQ/q)

1

1 Se (ng/g) cont

1059 5 ICPES 84PRI

1 01 1 420 30 ITNA 78GIL 01 1256 58 CB 86GAU 01 1 420 30 7 RTNA 77GIL 03

1320 30 UXRF 86B0U 01 1 430 40 RTNA 84DEL 01 1360 50 CB 86B0W 01 1 450 30 RTNA 78GIL 01 1380 D CB 85JAC 01 1 460 80 7 RTNA 77GIL 03

1380 60 6 CB 84JAC 01 1 460 80 7 RTNA 80GAL 02

1400 ICPES 85UHI 02 1 480 70 7 RTNA 80GAL 02

1400 D CB 85JAC 01 1 480 70 HAA 82TAM 01 1400 30 6 CB 84JAC 01 1 1520 70 CB 84GLA 11 1 Sn (ng/g)

Sb (ng/q) 1 < 20 L ICPES 82HAH 01

< 2 L ICPES 82HAH

1 01 1 Sr (ng/g)

5 1 RTNA 78GIL 01 j 9.9 0.3 RTNA 84BYR 02 1 190 40 XRF 86GIA 01

Sc (ng/q) 1 Tl (ng/g)

0.13 0.17 UNA 86GAU

1 01 1 < 2 11 ASV 84LIE 01 0.25 ITNA 84GLA 11 1 < 2 11 ASV 84LIE 01

1 < 2 11 ASV 84LIE 01 Se <ng/gj 1 < 2 11 FAA 84LIE 01

280 30 11 HAA 82JON

1 01 1 U (ng/g)

280 55 FAA 81MEY 01 1 300 11 HAA 85PIW 01 1 < 1 DNA 86GAU 01 315 14 HAA 81HAH 01 1 0.89 0.22 35 DMA 80GLA 04

320 40 11 HAA 82J0N 01 1 320 50 HAA 81MEY 01 1 V (ng/g)

331 29 ICPES 81U0L 01 1 338 3 7 RTNA 77GIL 03 1 < 50 L ICPES 82JON 01 350 11 HAA 85PIU 01 1 6.2 0.8 RTNA 84BYR 02

370 30 HAA 80RAP 02 1 370 60 H ICPES 82HAH 01 1 380 ICPES 84MIA 01 1 380 10 HAA 81 HAN 01 1 17.3 7.2 12 FAA 85CAR 02

380 20 HAA 83K0L 01 1 18.7 4.6 2 FAA 84MIL 01 380 40 HAA 84NAR 01 1 19.1 0.4 RTNA 84BYR 02

380 40 XRF 86GIA 01 1 19.1 2.4 ICPES 85LY0 01 380 40 HAA 85YAM 01 1 19.3 0.7 11 ICPES 82JON 01 380 50 HAA 80VIJ 01 1 19.4 0.4 ICPES 81U0L 01 390 20 GC-HS 81REA 02 1 19.5 0.5 11 HPLC 85ICH 01 390 70 HAA 81REA 01 1 19.5 0.6 11 HPLC 85ICH 01 400 8 EXRF 80RAP 03 1 19.6 0.4 ICPES 80SCH 08

400 20 11 XRF 80RAP 01 1 19.8 0.8 11 ICPES 82J0N 01 400 20 XRF 81KNA 01 1 19.9 0.4 ICPES 83SCH 04

400 100 HAA 85NAR 03 1 19.9 1.4 2 FAA 84MIL 01 400 100 11 XRF 80RAP 01 1 19.97 0.69 ITNA 78GIL 01 420 30 ITNA 80GAL 02 1 20 1 11 ICPES 82JON 01

1568-6
Cone Uncer

TABLE 1568-2: INDIVIDUAL DATA FOR NBS SRM 1568 (cont.)

Com Method Reference I

2n (ug/g) cont.

20.2 0.8 11 ICPES 82JON 01 20.4 0.9 ICPES 85WHI 02

21.3 1,3 ICPES 81KNA 01 21.9 1.8 XRF 86GIA 01 26.3 3.1 CPXRF 84BIS 01

1568-7
"8

8

I- C

en o UJ Vt O -Hc

4)

t— u.

<M «- «-

in ro CM

5 S

O 00o •H • <M

eg

in

C\J

tvj

a

</>

)S o 00 c

(D z

ro

(0V c

1_

1

(/> <Ui

>- +4

(/) (D 0£ OJ UJ Z 3lU

ee. COaoinz UJu

(/> z

< (/> COou.<1— z

< <: o

o Q 111 LU z

i—

o.s

1 c o>o (/) in m

UJ z (/> _i UJ

c/> z

< o 1- u c

<0

<u

o

(M

O O O N.

fVJ

o o

o o O Kl o in

(\J

o

in

o o

T- f\l (M «-

N—/ T

ro Ln o • CO CO

fVI fM mo

(M

in

o

o

fVl (M

O

CJO00 O

o «-

o (M

><• o o • 0> (M

to fVJ ^

eoo

00

o

(\j o(M

o

I 00 «- o

: 3 n: 2

CO in o

-t o «- in

I o

0 v3

00o

1^ o

in

<M to to f\J <NJ in (M

\^ \^ \^ ^^

<o O o (M o o o O to O O ro in in O

in (\j <M to in o 1 o o o H H •H +t eo eo H 1 1 (M « f\j +) ro •H

<\j f\J -J- (M t 1 1— O O o O V >o o f\l o t^ o m

in fO to •

m

c

4>

O) cn CI O) cn cn ) cn cn cn \ >«. \ > o> O) o> cn o> cn cn O) cn cn cn >

3 c 3 c 3 3 c 3 3 c 3 3 3 c 3 c 3 3 3 c c c

—•HI <u < < ca 00

I- 10 TJ « —• o u

CO (_] o u o o o

{. <- (fl 3 3 U U (J O UJ lA. U. O

1569-1
"8

to 0) 8a: ^

I- C

tu ^

111 </> O -HC

«)

o

X

o

m

u

(/> (/> o o

«* o

a.u t c

•JJ (0 C 4) o z u

<UJ

>- c

(/>

UJ3UJ

ae, < H

09 z

c O CO -O <1> ir» z

z

(/J

(/> m

a: LU O O u. <

<I—<

oLLI _l

Q.i

<

oUJz

1 o>om

LECD c <I— o

w

UJ H

oo c

<* <*

CD

<1>

O

«- o

o

o

o o> CO

o> o

o «-

o o

00

nJ- tM

>^ >^ CO

CO Kl

o >o

o

o

o

oin

«— (M m «-

O

o (M o t 1 ^0 * 1 »M o> CO

*" O H ( 1 1 • in M o •

1 1 1 } r— O ro o fGO

o« o

M o«—

ro in

CO o o o o o O O (NJ O in fVI >«• -4-

-o o a • • o Nj- «- f\J

o CO o

o

o

o

oCO s

V*

o in

in m >* -* CO (M

>^

o o O o o o O o o o (M o in o O rsi CO 12 t\j H +1 +1 H +) -H in in o -H O •H

-4- to >t O o >o O O O in

in O CO o o CO o <) m >* o

CO c

«)

UJ

cn O) CD cn cn cn cn m cn >^ V. >^ *j >»

o» o> o> o> cn cn cn cn cn cn (0 cn C 3 3 3 3 3 >S c 3 3 3 c c 3 3 3 3 c (- 3 3

cn c o z z z<D— ja XI SI <j <o t- zza.Q.ae:(/>Mcq(/s(/>(A

CO(M

in

(M

I 3 >

CM

1569-2
TABLE 1569-2: INDIVIDUAL DATA FOR NBS SRM 1569 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Al (UQ/g) Cr (ug/g)

2000 56 11 ICPES 82J0N 01 1 0.078 0.026 FAA 74WOL 01 2300 10 ITNA 78BER 01 1 0.7 0.1 11 ICPES 82 J ON 01 0.87 FAA 80CHA 01 As (ng/g) 1 1 .04 0.04 7 FAA 80CHA 01

4 4 1 1.12 A AO 0.08 RTNA 78G0E 01 530 80 11 HAA 82J ON 01 1 1.2 0.6 11 ICPES 82JON 01 560 30 11 HAA 82JON 01 1 1 .558 0.015 11 RTNA 78MCC 01 670 70 lENA 82GLA 02 1 2.00 0.02 NM 80SHI 01 2.02 0.1 FAA 83CAR 02

B (ug/g) 2.043 11 NAA 79VER 01

1 2.074 0.012 11 RTNA 78MCC 01 6.2 TCGS 82GLA 02 1 2.08 0.09 IDMS 79VEI 01 2.082 0.013 24 ITNA 78MCC 01 Be (ng/g) 1 2.094 11 NAA 79VER 01

1 2.096 A AO 0.02 24 ITNA 78MCC 01 22 6 FAAC 86GAU 01 1 2.1 0.5 ITNA 79K0B 03

1 2.119 0.025 24 ITNA 78MCC 01 Br (ug/g) 1 c. 1^ T TilA 78BER 01

1 rt 1 o f r A A rAA 80CHA 01 0.65 0.03 ITNA 78BER 01 1 2.13 0.13 RTNA 79TJI 01 3.4 lENA 84GLA 11 1 2.17 0.11 ITNA 82GLA 02

6.7 0.4 ITNA 79K0B 03 1 Cs (ng/g)

Ca <ug/g>

1 < OAA 200 L ITNA 82GLA 02

2270 70 1 1 ICPES 82J0N 01 1 TO •1 i ICPES 82 J ON 01 1 Cu (ug/g)

2h2U 40 ICPES 82JON 01 1 30 4 4 1 1 ICPES 82J0N 01 1 11 2 ITNA 78BER 01

4

1 1

1

ICPcS 82J0N 01 Cd (ng/g) 1

4 *7 "7 If.f A "5 0.2 1

1

ICPES 82 J ON 01

1

4 O 4 18.1 A "7 0.7 4 t 1

1

ICPES 82 J ON 01 OU 1 1 iLrtd 82J0N 01 1 IS/. u.o 1

1

1 1 1 Lrto 82 J ON 01

rU 11 ICPcS 82J0N 01 1 160 70 4 4 11 ICPES 82J0N 01 1 Eu (nq/g) onA 290 60 11 ICPES 82J0N 01 1 20 10 ITNA 79K0B 03

Ce (ug/g) 1

1 F (ug/g)

2.3 0.1 ITNA 78BER 01 1 14 2 I SB 83KNA 01

CI (ug/g) 1

4 P15 2 ISE 84GLA 02

/ XA ITNA 78BER

1

01 1 Fe (ug/g)

3 lU ITNA 84GLA 11 1 onn 1 CNA 84GLA 11 1 1/. Oh 1

1

I PDCC 1 Lrto 82J0N 01 499 15 11 ICPES 82J0N 01 Co (ng/g) 590 24 ITNA 79K0B 03

660 15 11 ICPES 82JON 01 260 20 ITNA 78BER 01 1 693 25 11 ICPES 82JON 01 300 60 ITNA 79K0B 03 1 707 16 ITNA 78BER 01 1569-3
TABLE 1569-2: INDIVIDUAL DATA FOR NBS SRH 1569 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ga (ug/g)

1 Na (ug/g)

f . 1 u.b UNA 78BER

1 01 1 310 50 UNA 78BER 01

1 660 UNA 84GLA 11 Hf (ng/g) 1 670 42 UNA 79K0B 03

130 10 UNA 78BER

1 01 1 Ni (uq/g)

Hg (ng/g)

1

1 4.6 0.3 11 ICPES 82JON 01

1 4.8 0.1 11 ICPES 82J0N 01

22 CVAA 82GLA 02 1 5.9 0.2 11 ICPES 82JON 01

1 6 0.2 11 ICPES 82J0N 01

I (ng/g) 1

1 p m

32 lENA 84GLA 11 1 60 20 lENA 82SAT 01 1 1 0.04 11 ICPES 82J0N 01

1 1.02 0.03 11 ICPES 82JON 01

K (%) ! 1.04 0.05 11 ICPES 82J0N 01

1 1.08 0.04 11 ICPES 82J0N 01 1.4 0.1 11 ICPES 82JOM 01 j 1.45 0.007 11 ICPES 82 J ON 01 1 Pb (ng/g)

1.45 0.05 11 ICPES 82J0N 01 1 1.55 0.05 UNA 78BER 01 1 200 200 11 ICPES 82J0N 01 1.59 0.04 11 ICPES 82J0N 01 j 500 500 11 ICPES 82J0N 01

1.71 0.12 UNA 79K0B 03 1

1 Rb (ug/g)

Li (ng/g) 1

1 16 1 UNA 78BER 01 440 20 AAC 85GAU 04 1

1 Mg (ug/g) 1 4100 90 CB 86B0U 01 1730 70 11 ICPES 82J0N 01 1 4140 120 WXRF 86B0W 01 1780 100 UNA 78BER 01 1 4170 120 CB 84GLA 11

lO? u

1

1

1

1

1 LrtS 82J0N 01 1 1900 60 11 ICPES 82JON 01 1 Sb (ng/g)

1980 60 11 ICPES 82J0N 01 1

1 75 5 UNA 78BER 01 Mn (ug/g) 1 230 50 UNA 79K0B 03

7 0.8 UNA 78BER

1 01 1 Sc (ng/g)

9.1 0.6 11 ICPES 82 J ON 01 1 9.6 0.6 11 ICPES 82JON 01 1 170 9 UNA 86GAU 01

10 1.5 UNA 79K0B 03 1 170 14 UNA 84GLA 11 10.4 0.8 11 ICPES 82J0N 01 1 180 10 UNA 78BER 01 10.9 0.7 11 ICPES 82J0N 01 1 196 UNA 85GAU 04

220 30 UNA 79K0B 03

Mo (ug/g)

Se (ug/g)

3.3 0.3 11 ICPES 82J0N 01 1 3.4 0.1 11 ICPES 82J0N 01 1 0.92 0.09 UNA 78BER 01 3.8 0.2 11 ICPES 82J0N 01 ! 0.98 0.05 11 HAA 82J0N 01 3.9 0.2 11 ICPES 82J0N 01 1 1.01 0.06 11 HAA 82J0N 01

1569-4
TABLE 1569-2: INDIVIDUAL DATA FOR NBS SRM 1569 (cont.)

Cone

Sr (ug/g)

10.3

Th (ug/g)

3-7

38

Uncer Com Method Reference

0.2

lENA

ITNA

ITNA

85GAU 04

78BER 01

78BER 01

Cone Uncer Com Method Reference

U-235/238 (ratio)

7,26

V (ug/g)

1.46

4.1

4.4

Zn (ug/g)

0.07 28

0.05

0.1

0.1

11

11

IDMS

ICPES

ITNA ICPES

82CUR 01

82J0N 01 78BER 01 82JON 01

U (ng/g) 30 4.3 ITNA 79K0B 03

59 6 11 ICPES 82J0N 01 441 4 IDMS 82CUR 01 1 63 2 11 ICPES 82 J ON 01 460 20 35 DNA 81GLA 03 1 64 4 11 ICPES 82J0N 01 470 20 DNA 84GLA 02 1 64 5 11 ICPES 82J0N 01 470 20 DNA 82GLA 02 1 65 2 11 ICPES 82J0N 01 470 20 35 DNA 80GLA 04 1 65 2 11 ICPES 82J0N 01 470 50 35 DNA 81GLA 04 1 66 2 11 ICPES 82J0N 01 490 20 ITNA 78BER 01 1 70 2 ITNA 78BER 01 490 30 DNA 84GLA 11 1 70 4 11 ICPES 82J0N 01

1569-5
"8

-Cc

ena> z: 8? "S

LU f

a: -M

01

o ^c

ra

ft)

00

-^ lu

a.

4.) "S c

(0<u > X

L.

c

u

«tz 0 CL 00

COo +1 in c

<00 X X

ae

(/>

(0

CQz c

oeO 0 << < +1 a c d (0 LU 0) _J X &u

lU *

oz o <

in

LE z < < 0 CO (/> LU (/) _1 X CL X 0 u CO X (/> CJ < 0 0 t— 0 z </) CL.

^—^

r—\

n

— «

^

' > ' '—

% ' in 0 00 > 1 1 •0 N. fM 1 1 1 1 • • • 1 1 1 0 1 >j- < U- > u_ •H —1 u.

or: UJ 0 Oi

X < X < 0.

X

ILI V> a. X O CO

CO

(NJ *—

in

Oo

O—I 111 o < U u.

Q£

X

X

Z

in I

CD

CJ

y^ ^-^

(NJ 1^ (M OJ >—

\—/ V—

•—

>o0 00 » 0 0 00 in •J- -J- • ro 0 fVJ 0 • 1 1 00 1 in M 0 • *— 0 (M «— 1 1 M < in in m «— T— 1 in 1 in in •0 ro

rvj in

00 >- oin o o

O

CJ

00

in «—

o

ro

inoo

ro

COo ^ vO (NJ in (NJ

fM

in 00 N.

<0 fO M fM >» 0 0 in fVJ 0 •H +4 ro 11 1 +1 I M in

•0 CO in •J- -* in 00

f\J

o «- in

~»

o

o 00

fvi in

o>o

+) +t

«~ ^ CO ro rvin «— ^ S8 o

fVl o

CO

lA

in

o

in 00

eo r^

f\j «-

fM

ro 80 o>

ino in -J- «—

>- -0

in

oo

O S- fM o »- m

o

fM

fM

in

o ~j

•O

O r- . fM

>o ro

•J- fN. o- r\j

o

<MO • (M

v» >J «-

O <-

Nj- «- ro

ro

ro

(NJ

00 fM

J-

<r

o (NJ in

CO «-

^^ ro (M 1-

>3-

o in in «- o

ro

CO

fM

in

inmin

r^

fM

o • o (NJ vO

ro 00 «—

Jin

ofM

o

in

o

fM

(M < z

rvj

OJ 1 1 ro 1 1 ro

U00 CXL X X

ro

00 hO 1 0 ' 1

0000 1 1 +1 '

fO

<r (M CO in

S—

fM

''• 0 LA 0 in

*' *'

m in 0 ro in

K»

ro

in' 1 11 0

+1 1 1 I

inro

in

ro 1

ro 1 0 0 ro

ro

ro

^— 0in 0

in 1 ro ro

o

to /—\

y^ ^—1 fM ro 00 (NJ in ro fM 0 fM •0 fM in -J- in ro fM 0 (M >0 fM in

c fM 10 fM \^ ro

V—

> ' fM * ' >^ «^

CO fM fM in

CO 0 0 in 0 0 1

in r—

CO 0 0 0 0 CO fM 0 fM -*

rS 0 0 sj- 0 0 0- 0 in ro ~» 0 in 0 >3- z m (NJ •0 00 <o 1 to 0 in 0 (NJ LU ( >0 +( •H H H +1 •H in +) •H +< H +) +t 1 fM 0 -J +1 +1 +1 +1 CO V 1 m z c 0 ro rs. o- 00 ro ro 0 >o ro 00 in 0 V 0 0 0 0 CO in -* ro 0 in t

to (M in

u 0; 00 •J- in

10' ro

X fM

ro to

a 0 ro 0

CO 0 0 0 m in 0 0 fM in 0

CO 1 1 0 1 va- 1 in 1 in 1 1 1 1 0 1 1 0

COK I •H ro 1 in 1 M 1 I M 1 1 +)

t fM 1 •« +1 1 +4 z 1 1 1 »— 1 I 1 1 1 1 1 to c 0 0 m fM 0 0

(S lA ro in ro in « CO * in X to

to

I— Ol O) CJ) cn O) O) O) O) O) 0 D) cn O) cn cn cn cn at cn cn cn cn cn cn cn cn >v \ \ \ v. \ \ '

\ — — z 01 D) O) O) o> O) O) O) cn O) cn en cn O) cn tn tn cn cn cn cn 01 cn cn cn c 3 c C 3 c c 3 >« 3 c 3 3 ? 3 c 3 3 3 3 c 3 3 3 c c s< c c 3 c c

Ul 0

_l

D (D 4)

D (0 ft> 0 u (_ (/) 3 3 3 3 3 <U (U T3 (NJ H- cn c

LU < < < m CQ CD CD

m 0 U

U CJ

U (_J (J CJ 0 (J LU u_ C3 0 3r 3: 3:

CO

<>

1570-1
c

CO

a> 8^

"8

LU ^ X 0)

tc o ~-- c

01

U- c/> LU

g +4 Q_ _J LU C_) o (_) < t— ^

»^

o NO 00 o vt«— s o mu

«— I in ^ ^] 5 O O Q. O. > Uo

o ^ • in «— -o in in

Xo

in 3a.

_iou

in

in < a. oo o

o

ino

CJU

K1

CJ

OO

00ooCJ

</) UJ

a.(Jom

o< O O

00

4-) UJ

a.

cu

ou

c«

ac

X

uz

a.co

m cn z z +* CO c

(0 CO 0) m X z

a:Ou.

c

<t

t-<o

o(/>

aUJ AA •H a. c

<s

s 0) (J X 1 s UJ

(9Z

UJ < _im<1— <3 CO COz

UJ +1 COZ C O (0

OJ

o

(M

m

m

«- fNj omo

•*

*i o

OOo

(MOooo

«— ^ o» oOin

ICo

<^

ro

>^ \^

\^

o

O

O r^

o 1 o roo

OO 1 in

o in

ro

o in m

OO >^ o•

>»

o vO 1 ( •H o H 1 1

f\J 1

*—

nj fO

W

fvj

o

oo f\j

O in 11 1 44 +1 in OPJ>*

in

(NJ

ro

oo

O

in

o

o

om

mo fM (M

>« -O ^ in

o

O <r- o ro o

ro

o00

o

O vO oro in

o CO

(\J ro

«* in

o

ro 1 m

o • in ro

in

r^ «* -* r^ W nj (VJ o in o (\j o o o O » o •H •H +1 ro ovj- in PJm

oo

o

(NJ . r^

ro

».

/-^ ro

^•.^

o 1 ^

-*<M

•flH +H +1

o 2CO

Om

in

ro

ro

o

N.

O -4- (vj in PJ

h- ro

o00

ro

ro

ro • PJ

roCO

o

o CO ro

mOO

OO

PJ

PJto

om eo

T- PJ o o ^ CO

in

r^

ro ^ r^o

in

00

PJ CO ^ POo

in PJ

•J-

^o r^ r^ o- •- ro »- «— (NJ ro «—

in in

(NJ +(

ro

o PJ vO

(NJ PJom

ro

-J-

(yo -4- •Jo

o -*o PJ

m ro ro

o in

o

o PJoo

*i *iH +)oo

M • +1 ro • 00 ro o «-H ro +f +1 (NJ

V in

oo 1 o PJ -Oo 00o

oo

inm 00 >» PJ in

t~ lO

>j

CO

03

a

COc

(D«)

m

m

cn oi o) O) CD

Ui Ui Ut Oi C 3 3 3 C cX

O

o

PJ

o

o PJ ro

o (M 1 1 1 1 o o o 1 1 H 1 +1 1 1 +4 >J- 1 1 +H 1 +1 ro +1 +1 1 1 o 1 PJ 1 1 1 1 1 1 o -o O o OO PJ in in PO

in

Ol Ol D> Ol Ol Ol O) Ol Ol Ol Ol Ol O) Ol O) O) Ol Ol D) O) O) Ol Ol Ol \ \ \ —

Ol D) Ol Ol Ol O) Ol Ol Ol Ol 1 Ol CJ) Ol CJl O) D) Ol O) CJl Ol O) »« c 3 3 3 3 3 3 c c 3 3 ? c c 3 c 3 3 3 c c 3 C c 3 c c 3

to TJ jD i3 x> L. S3

E

C L. Si

C z z Z Z a. a a. Cl. CL a to (O CO CO to C/l t/l CO »— I— 1— 1— 3) > 3 >- rj

Ol3

1570-2
c UJ c (\I s o </> nj u z <u 00 o x: in in ro vj- o

<

z

Cl. (/> 1 1 1 1 1 (/) CO 1 1 1 1 1 1 z 1 1 1 1 1 osin

<:

Q£ V) O) ) CD CO t— ~-. \ D> cn

(/> z 3 3 3 3 3 3 m 3 z

a:OLI- < % vO vO in

1— 1 1 1 1 1^ ro CO < 1 1 1 1 vO OJ 00 o < 1 1 1 1 o in ro

CJ in -o 00 Q

LU

1 U) a. 0) M

(D o C

o TJ z U) ^ 0) u

1 +J o < vO o a. (D 4-' 1 c

h- c o CO in o "o (0 d) > U LL. Q. C c E c (a lU E M E

_i (D (D 4-* o (D o

CO M 4-» o u 4-" < O O 1- 1— 1— 1— 1— a. z > or

1570-3
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Total Folates (ug/g)

1

1

1 As (ng/g)

5.3 W 85TAN 01 1

1 62 13 7 FAA 82H0E 02

Total Pantothenates (ug/g) 1 114 HAA 771 HN 01

1 120 10 7 RTNA 80GAL 02

14.3 W 85TAN 01 1 120 70 ITNA 85NDI 01

1 140 10 AA 83RAP 01 Thiamine (ug/g) 1 146 RTNA 85TIA 01

1 147 1 RTNA 79H0E 01 5.6 W 85TAN 01 1 149 25 RTNA 85GAU 04

1 150 10 11 HAA 82 J ON 01 Protein (%) 1 150 13 7 FAA 82H0E 02

1 152 5 7 FAA 82H0E 02

33.2 VV 85TAN 01 1 160 FAA 78CAP 01

1 160 10 11 HAA 82 J ON 01 Nicotinic acid (ug/g) 1 170 10 H ICPES 82HAH 01

1 170 10 COLOR 77BUR 01 42.4 W 85TAN 01 1 170 20 FAA 80DUP 01 170 40 RTNA 80SLO 01 Vitamin B-6 (ug/g) 1 180 20 HAA 80TAM 01

1

•1 OA 180 70 lENA 82GLA 02

12.1 W 85TAN 01 1

1 Au (ng/g)

Riboflavin (ug/g) 1

1 0.4 RTNA 80SLO 01 17.6 W 85TAN 01 1 2 0.0004 ITNA 79REN 03

Ag (ng/g)

1

1 B (ug/g)

65 10 RTNA 80SLO 01 1 65 40 AA 80JAC 01 1 20.9 0.3 ICPES 79HER 01

1 27 3.5 ICPES 84PRI 01 Al (Uq/q) 1 27.2 0.8 11 ICPES 81MUN 01 366 48 11 ICPES 81MUN 01 1 27.6 1.3 11 ICPES 81MUN 01 402.6 23.2 6 COLOR 85BAR 01 1 28 0.4 TCGS 82GLA 02

412.7 24.8 6 COLOR 85BAR 01 1 28.5 ICPES 81 GOO 01 482 ICPES 78CAP 01 1 536 ICPES 81 GOO 01 1 Ba (ug/g)

609 16 11 ICPES 81MUN 01 1 620 36 ICPES 83SCH 03 1 < 45 L ITNA 78CAP 01 782 31 11 ICPES 82 J ON 01 1 13.1 1.8 ITNA 77NAD 02

819 30 ICPES 84ABD 01 1 13.9 0.7 ICPES 85WHI 02

820 25 ITNA 84GLA 02 1 17.8 2 ICPES 84NAD 01 824 10 ITNA 80SLO 01 1 87 29 ITNA 79REN 03

829 23 ITNA 77NAD 02 1 854 25 ICPES 83SCH 04 1 Be (nq/q)

861 30 AA 83RAP 01 1 865 47 ICPES 84NAD 01 1 < 30 L ICPES 82KUE 01 870 ITNA 84GLA 11 1 < 30 L ICPES 82KUE 01 881 ITNA 78CAP 01 1 < 30 L ICPES 82KUE 01 909 11 lENA 85GLA 02 1 < 60 L ICPES 78CAP 01 1190 35 ITNA 81GLA 03 1 < 80 ICPES 84W0L 02

1 16 6 ICPES 83SCH 03

1570-4
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ng/g) Ca (%) eont. —

< 8 L ICPES OcnRn m 1 U 1

1 1.49

1.54

0.1

0.01

ITNA ICPES

77NAD

79HER

02

(uq/g) 1.62

1.78 0.25

ICPES ITNA

f oLAP

/yREN

0105

42.4 2.4 5 ITNA oUnUt u 1

1 2.45 EXRF Q 1 n A 0 01 PAR Ul 43.6 2.3 5 lENA f TULA no 1 Uc 1 45 ITNA Q/ PI A 1 1 1

1 1

1 Cd (ug/g> 1

45 3.3 ITNA OUSLU U I |! 45.1 0.3 5 lENA /vGLA n'y 1 U£ 1 1.2 FAA 80PRE 01 46 2 5 ITNA 80HOE 01 1 1.2 0.05 FAA 84KUR 01 47 4 ITNA O/ PI A oAGLA Uii

1 1.2 0.15 ASV 82GAJ 01 47.2 0.5 ITNA 77NAD 02 1 1.23 0.16 ASV 82SAT 02

48 ITNA TOP A O m 1 Ul 1 1.3 FAA 82PRE niU 1 48 9.4 ITNA 79REN 03 1 1.3 0.05 AA 83RAP 01 51.1 2.5 CPXRF Ul 1 1.3 0.2 11 ICPES 0 1 Ul 111 0 IMUN 01 52 4.8 ITNA U«>

1 1.32 ASV 7Qf* A n

f oLAr Ul 54 3 35 NAA 81GLA 03 1 1.38 0.08 RTNA 80SLO 01 55.3 3.8 5 ITNA OU 1 UU Ul 1 1.39 0.11 ICPES Ul 138 EXRF 81 PAR 01 1 1.4

1.4

0,08

0.1

11 ICPES

ICPES

82J0N

tSoSCH

01

n/

m 1.4

1.4

0.1

0.14

ICPES

AA

Q/ A nrv o4AbD

odtvf\

ni

ul 40.7 1 CB f f WA 1 00 1 \)c

\ 1.4 0.2 ICPES n*2

40.82 0.81 CB aoicr*ij OUbLH no 1 XJC

1 1.41

1.42

0.03

0.03

6

6

ICPES

ICPES

niU 1

U 1

<%> 1.45

1.46

0.07

0.02

6 ICPES

NAA

OCKut. 7An CD

niu 1

u 1 0.82 0.11 ITNA OUoLU u 1

j 1.46 0.04 FAA ftfll cr OULCu u 1 0.85 0.01 CPXRF ft/. OhoD T C1 3 1 1.47 0.12 FAA ft'^nci OOUuL u 1 0.99 0.05 ICPES ft/. A on ni 1 u 1

1 1.48 RTNA ftS\T T A niu 1 1.19 0.09 6 EXRF 70UAT ni 1 Ul 1 1 .49 0.08 11 ICPES ftp inij niu 1

1.21 35 AA Q1 n A O 1 uLA f\L 1 uh I 1.5 0.3 AA ftA^AU niu 1 1.22 0.02 ICPES ft/.ijni n5 1 1.52 0.07 RTNA 77nCD f fUCK niu 1 1.24 0.08 11 ICPES ni 1 Ul 1 1.6 0.2 FAA ft 1 ^kl A u 1 1.25 0.01 11 ICPES O^JUN ni 1 U 1 1 1.67 0.29 SSMS 77DAI

1

/ f KAU niu 1 1.29 0.03 6 ICPES ocKut Ul 1 1.7 0.1 RTNA 7Ar Al niu 1 1.29 0.04 11 ICPES 01MUN ni 1 Ul 1 1.7 0.2 D FAA ftflCPLI uo

1.3 ICPES 01GOO ni i U1 1 1.7 0.2 AA oUoLn n^Uj

1.34 0.07 ICPES 85WHI no 1 02 1 1.7 0.3 11 ICPES Q 1 Ul III 0 IMUN niui

1.34 0.23 ICPES B4NAD ni 1 01 1 2 0.1 AA 7Ar At niu 1 1.347 0.014 NM 01 YUZ ni 1 01 1 2.1 0.2 ICPES 70UCD /VntK u 1 1.35 0.025 6 ICPES DO1^1 IC OcKUc ni 1 Ul 1 2.2 1 11 ICPES 0^ JUN niu 1 1.35 0.06 11 ICPES 0 InUN mU 1

1 1 2.8 0.1 11 ICPES ftp inw U 1 1.36 0.04 11 ICPES 82JON 01 1 1.37 0.07 5 ITNA 80TCXJ 01 1 Ce (ng/g)

1.38 0.014 6 ICPES 82KUE 01 1 1.39 0.03 11 ICPES 82J0N 01 1 240 30 RTNA 8OSLO 01

1.4 0.04 6 EXRF 79MAT 01 1 671 162 RTNA 83TJI 01 1.44 0.035 ICPES 83SCH 03 1 1.46 ITNA 78CAP 01 1 1570-5
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference

6000 35 ITNA 81GLA 04

6290 ITNA 78CAP 01 6500 300 CPXRF 79REN 02

6800 100 ITNA 80SLO 01 7000 ITNA 84GLA 11 7000 120 ITNA 84GLA 02

10000 1000 ITNA 77NAD 02

Co (uq/q)

0.9 0.1 PAA 80YAM 01 1.41 ITNA 78CAP 01 1.42 0.1 AA 83RAP 01 1.47 0,1 AA 80JAC 01 1.49 0.05 RTNA 80SLO 01 1.5 0.1 ITNA 79K0B 03

1 .5 0.2 ITNA 79REN 03

1.5 0.4 ICPES 84ABD 01

1 .6 0.1 5 ITNA 80TOU 01

1 .65 FAA 82H0E 01

1 .68 0.03 RTNA 77MEL 01 1.7 0.1 ITNA 76GAL 01

1 .76 0.01 ITNA 77NA0 02

3.2 0.2 AA 76GAL 01

Cr (uq/g)

1 .9 0.3 1 1 ICPES 81MUN A<l 01 2.U ICPES 81 GOO A 4 01 3.06 0.3 AA 80JAC A 4 01 3.33 0.74 ICPES 84NAD 01 3.5 0.3 6 ICPES 82KUE 01 3-54 0.3 6 ICPES 82KUE 01 3.6 0.5 11 ICPES 82JON 01 3.7 1 .2 11 ICPES 81MUN 01

3. 75 1

1

AA 79H0E 02

3.9 POL 83H0L 01 4.0 0.34 ITNA 85N0I 01 4.2 0.7 ICPES 83SCH 03

4.3 0.5 ITNA 77NAD 02

4.3 0.7 6 ICPES 82KUE 01 4.4 11 AA 79H0E 02

4.4 FAA 82H0E 01 4.4 0.2 ICPES 84ABD 01 4.47 0.4 FAA 83CAR 02

4.5 0.2 RTNA 76GAL 01 4.5 0.3 ITNA 79K0B 03

4.51 11 AA 79H0E 02

4.6 0.2 11 ICPES 82J0N 01 4.7 0.15 AA 83RAP 01

1570-6

Cone Uncer Com Method Reference

Cr (ug/g) cont.

4.7 0.3 DCPES 79REE 01 4.7 0.3 D DCPES 81REE 01 4.7 0.4 ITNA 82GLA 02

4.8 ITNA 78CAP 01 5.2 0.5 ITNA 76GAL 01 5.2 1.5 AE+AF 82G0L 01 5.8 0.2 AA 76GAL 01 6 0.7 PAA 80YAM 01 6.2 0.1 ICPES 79HER 01 7.5 1.6 ITNA 79REN 03

20.5 2.8 11 RTNA 76STE 01

21 2 RTNA 77MEL 01

21 .3 2.6 11 RTNA 76STE 01

21 .8 1.5 11 RTNA 76STE 01 23.9 0.9 1

1

RTNA 76STE 01 24.5 1.2 11 RTNA 76STE 01 24.8 2.8 ITNA 76STE 01

(nq/q)

<

AA 200 L ITNA 82GLA 02

48 5 ITNA 77NAD 02

63 3 ITNA 84GLA 11 64 2 ITNA 84GLA 02

68 8 ITNA 85GAU 04

J 70 / A40 RTNA 77MEL 01

>20 / A40 ITNA 79REN A?03

< 20 ITNA 84GLA 11 5.3 4 "7 1 .3 ITNA 85NDI 01 9.1 0.4 AA 76GAL 01 9.5 ICPES 81 GOO 01

4 A O 10.2 4

1 ICPES 82EVA 01

4 A C 10.5 A TP 0.3 1

1

ICPES 81MUN 01

4 A Z 10.6 A A 0.9 CPXRF SAB IS 01 10.7 0.5 ICPES 83SCH 03

10.8 ASV 83HOL 01 10.9 0.3 11 ICPES 82J0N 01 10.9 0.6 RTNA 80SLO 01 11.0 0.2 7 RTNA 80GAL 02

11.0 0.2 AA 83RAP 01

11.1 0.2 11 ICPES 82JON 01 11.1 0.5 11 ICPES 82 J ON 01

11.1 0.5 11 ICPES 81MUN 01 11.2 0.4 11 ICPES 82JON 01 11.4 0.5 RTNA 79K0B 01 11.5 0.4 FAE 76EPS 01 11.5 0.5 SSMS 77PAU 01
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Cu Cuq/q) cont.

1

1

1

Fe (uq/ci)

11.6 0.3 ICPES 84U0L 02 1 178 2 DCPES 81REE 01 11.6 0.7 ITNA 79K0B 03 1 384 79 11 ICPES 81MUN 01 11.6 0.7 RTNA 78K0B 01 1 470 50 6 ICPES 82KUE 01 11.8 0.3 RTMA 7TDER 01 1 478 ICPES 78CAP 01 11.8 0.3 6 ICPES 82KUE 01 1 491 20 11 ICPES 82JON 01 11.8 2.5 W 80SCH 05 1 494 FAA 78CAP 01 12.0 RTNA 85TIA 01 1 500 26 6 FAA 84FUD 02

12.0 0.2 IDMS 84BR0 03 1 506 34 CPXRF 84BIS 01 12.0 0.3 6 ICPES 82KUE 01 1 508 14 ICPES 83SCH 03

12.0 0.5 ICPES 80SCH 08 1 510 ITNA 78CAP 01

12 1 2 FAA 84MIL 01 1 511 7 ICPES 79HER 01

12 1 2 FAA 84MIL 01 1 516 36 ICPES 84NAD 01 12.06 0.03 COLOR 77BUR 01 1 518 8 11 ICPES 82J0N 01

12.1 AA 80EVA 01 1 522 14 11 COLOR 82SCH 03

12.1 0.1 COLOR 76EPS 01 1 525 11 6 EXRF 79MAT 01

12.1 0.2 ICPES 79HER 01 1 527 30 ICPES 84ABD 01

12.1 0.4 AA 82EVA 01 1 530 11 6 ICPES 82iaJE 01 12.14 0.61 RTNA 85DYB 01 1 540 10 6 ICPES 82iaJE 01 12.2 0.1 6 ICPES 82KUE 01 1 540 18 D ICPES 80SCH 08

12.2 0.3 AA 85KOJ 01 1 540 18 ICPES 80SCH 05

12.3 ICPES 78CAP 01 1 540 23 ITNA 79K0B 03

12.3 11 AA 79H0E 02 1 541 15 11 ICPES 82JON 01 12.6 FAA 78CAP 01 1 545 AA 80EVA 01 12.6 0.2 ICPES 83SCH 04 1 548 9 NH 80SUZ 01 12.6 1.4 6 EXRF 79MAT 01 1 551 11 AA 79H0E 02

12.7 0.4 AA 76EPS 01 1 552 10 6 FAA 84FUD 02

13 0.4 ICPES 84ABD 01 1 556 ICPES 81G00 01

13 1 D DCPES 81REE 01 1 556 11 11 COLOR 82SCH 03

13 1 DCPES 79REE 1 556 15 2 FAA 84MIL 01 13.2 11 AA 79H0E 02 1 557 8 ITNA 79DAS 01

18 3 ICPES 84NAD 01 1 557 8 RTNA 80SLO 01

1 557 19 11 ICPES 82J0N 01 Eu (nq/g) 1 558 12 2 FAA 84MIL 01

1 562 25 AA 83RAP 01

< 200 L ITNA 78CAP 01 1 566 18 ITNA 77NAD 02

11 1 RTNA 83TJI 01 1 570 11 AA 79H0E 02

14 1 ITNA 79K0B 03 1 576 18 11 ICPES 81MUN 01 20 1 ITNA 77NAD 02 1 597 6 6 EXRF 79MAT 01 600 90 35 ITNA 816LA 03

F (ug/g) 601 12 ICPES 84U0L 02

660 300 ITNA 79REN 03

4.3 0.4 ISE 83KNA 01 1 763 34 RTNA 77MEL 01 4.4 0.3 ISE 84GLA 02 1 1200 EXRF 81PAR 01

Gd (ng/g)

60 21 RTNA 83TJI 01

1570-7
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone

Ge (nq/g)

H (%?

Uncer Com Method Reference

5.54

5.6

H20 (%)

Hf (ng/g)

20

0.08

0.1 35

ICPES

CB

TCGS

W

82HAH 01

BOSCH 02

79GLA 04

85TAN 01

40 20 RTNA 80SLO 01

(ng/g)

25 1 1 CVAA 79H0E 02

26 8 RTNA 80SLO 01 29 CVAA 83MAR 05

30 5 CVAA 82GLA 02

33 16 CVAA 82DOO 01 34 3 ITNA 77NAD 02

110 20 RTNA 77MEL 01

1.08 0.04 MS 85SCH 01 1.08 0.16 lENA 82SAT 01

1.1 0.2 PAA 77WIL 01 1.267 0.054 35 RTNA 81ALL 01 1.325 0.055 RTNA 81STR 01 1.325 0.055 34 RTNA 81ALL 01

In (nq/q)

1.2 0.1 RTNA 78K0B 01 1.3 0.2 RTNA 79K0B 01

K (%>

2.58 0.09 11 ICPES 81MUN 01 3.09 0.54 ICPES 84NAD 01 3.26 0.23 ITNA 79REN 03

3.29 0.09 2 FAA 84MIL 01 3.29 0.18 ICPES 79HER 01 3.43 0.11 ITNA 77NAD 02

3.44 0.2 11 ICPES 81MUN 01 3.46 ITNA 84GLA 11 3.52 0.1 6 ICPES 82KUE 01

Cone

K (%) eont.

3.53

3.54

3.56

3.57

3.57

3.58

3.59

3.6

3.6

3.6

3.61

3.61

3.65

3.7

3.7

3.73

3.74

3.9

4.02

4.04

4.85

7.95

La (ng/g)

260

315

320

350

350

361

400

Li (ug/g)

1.93

2.04

Lu (ng/g)

Uneer Com Method Reference

0.032 6 ICPES 82KUE 01 ITNA 80EDD 01

1 AA 78SZY 01 0.04 6 ICPES 82KUE 01 0.29 2 FAA 84MIL 01 0.06 ICPES 84ABD 01 ICPES 79C00 01 0.06 ICPES 85WHI 02

0.09 ITNA 79K0B 03

0.2 11 ICPES 82 J ON 01

1 AA 78SZY 01 0.35 ITNA 82EHM 01 0.21 ICPES 84U0L 02

0.04 11 ICPES 82J0N 01

0.1 11 ICPES 82J0N 01 ITNA 78CAP 01 0.07 ITNA 80SLO 01

0.1 11 ICPES 82 J ON 01 0.08 CPXRF 84BIS 01 0.06 6 EXRF 79MAT 01 0.05 6 EXRF 79MAT 01 EXRF 81PAR 01

50

30

10

60

89

50

0.06

0.01

RTNA

NMITNA

NMITNA RTNA

ITNA

ICPES AA

RTNA

RTNA

80SLO 01 83KAT 01 77NAD 02

85KAT 02

79REN 03

83TJI 01 85KAT 02

84NAD 01 85EVA 01

80SLO 01 83TJI 01

1570-8
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Mg (ug/g)

1

1 Mn Cug/g) cont.

6990 ICPES 81 GOO

1 01 1 165 3 6 EXRF 79MAT 01 7000 ICPES 78CAP 01 1 165 8 2 FAA 84MIL 01 7300 500 ITNA 80SLO 01 1 165 10 ICPES 85UHI 02

7800 200 ICPES 84ABD 01 1 166 1 ICPES 79HER 01 8300 800 ICPES 84NAD 01 1 166 5 11 ICPES 82JON 01 8340 130 ICPES 84W0L 02 1 167 5 ICPES 83SCH 03

8400 FAA 78CAP 01 1 167 6 11 ICPES 82J0N 01

8500 120 11 ICPES 81MUN 01 1 167 7 ICPES 82EVA 01 8550 65 6 ICPES 82KUE 01 1 168 3 D ICPES 80SCH 08

8600 230 6 ICPES 82)(UE 01 1 168 3 W 80SCH 05

8600 400 11 ICPES 82JON 01 1 168 4 AA 83RAP 01 8600 500 ICPES 85WHI 02 1 168 6 ICPES 83SCH 04

8700 100 ICPES 79HER 01 1 169 4 ITNA 80SLO 01 8700 500 2 FAA 84MIL 01 1 170 AA 80EVA 01 8790 150 6 ICPES 82KUE 01 1 170 4 AA 82EVA 01 8800 100 11 ICPES 82JON 01 1 171 ITNA 78CAP 01 8800 270 ICPES 83SCH 03 1 171 1 6 ICPES 82KUE 01 8833 299 11 ICPES 81MUN 01 1 172 5 6 ICPES 82KUE 01 8900 300 11 ICPES 82J0N 01 1 173 3 ICPES 84NAD 01 9000 200 11 ICPES 82J0N 01 1 176 2 11 ICPES 81MUN 01 9000 600 ITNA 78CAP 01 1 178 2 DCPES 79REE 01 9200 300 2 FAA 84MIL 01 1 184 10 6 EXRF 79MAT 01 9800 ITNA 77NAD 02 1

1

185

187.9 18.9

ICPES

PAA

81G00 01 80YAM 01 Mn (uq/g) 1

1

200

684

ITNA EXRF

79REN 03

81PAR 01

1.3 0.1 DCPES 81REE 01 1 49 2 11 ICPES 82JON 01 1 Mo (ng/g)

102 3 AA 76GAL 01 1 118 3 ITNA 76GAL 01 1 200 100 11 ICPES 82J0N 01

146 32 AE+AF 82G0L 01 1 200 100 11 ICPES 82JON 01

155 FAA 78CAP 01 1 300 41 COLOR 85EVA 02

156 11 AA 79H0E 02 1 300 100 11 ICPES 82J0N 01

156 4 ICPES 84ABD 01 1 300 100 RTNA 80SLO 01 156 5 ITNA 79K0B 03 1 400 200 11 ICPES 82J0N 01 157 ICPES 78CAP 01 1 420 RTNA 85TIA 01 157 5 6 FAA 84FUD 02 1 157 13 11 ICPES 81MUN 01 1 N (%)

158 7 11 ICPES 82J0N 01 1 158 13 2 FAA 84MIL 01 1 5.31 W 85TAN 01

159 11 AA 79H0E 02 1 5.62 0.11 CB 80SCH 02

160 35 ITNA 81GLA 04 1 6 0.4 35 TCGS 79GLA 04

160 3 11 ICPES 82J0N 01 1 160 3 ICPES 84W0L 02 1 161 6 ITNA 77NAD 02 1 162 4 6 FAA 84FUD 02 1 162 7 CPXRF 84BIS 01 1 162 9 ITNA 84GLA 02 1 164 ITNA 84GLA 11 1 165 3 6 ICPES 82KUE 01 1

1570-9
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference

Na (%)

1.13 0.02 ITNA 80SLO 01 1.24 0.21 ICPES 84NAD 01 1.28 0.1 ITNA 82SCH 05

1.29 0.11 11 ICPES 81MUN 01

1.31 0.07 ITNA 77NAD 02

1.33 0.03 11 ICPES 81MUN 01 1.33 0.05 ITNA 79K0B 03

I.HI 81 GOO 01

1.42 0.02 ICPES 84U0L 02

1.43 ITNA 84GLA 02

1.43 0.03 ICPES 84ABD 01 1.44 ITNA 78CAP 01 1.48 35 ITNA 81GLA 04

1.5 ITNA 84GLA 11 1.54 0.14 ITNA 79REN 03

1.547 0.021 ICPES 85WHI 02

1.55 1 AA 78SZY 01 1.56 1 AA 78SZY 01

Nd (ng/g)

306 73 RTNA 83TJI 01

Ni (ug/g)

1.3 0.1 DCPES 79REE 01 2.3 0.5 RTNA 80SLO 01 4.1 0.5 ITNA 77NAD 02

4.8 0.7 ICPES 82EVA 01 4.9 0.2 11 ICPES 82J0N 01

5 7 ICPES 84W0L 02

5.1 0.1 11 ICPES 82J0N 01 5.1 0.4 11 ICPES 81MUN 01 5.12 VOLT 81PIH 01 5.2 0.3 CPXRF 84BIS 01 5.4 0.1 11 ICPES 82J0N 01 5.4 0.1 11 ICPES 82 J ON 01 5.4 1 6 EXRF 79MAT 01 5.5 0.5 ICPES 83SCH 03

5.51 0.32 6 ICPES 82KUE 01 5.6 0.3 AA 83RAP 01 5.7 0.3 11 ICPES 81MUN 01 5.8 0.2 AA 82EVA 01 6.03 0.52 6 ICPES 82KUE 01 6.1 0.2 PAA 80YAM 01 6.17 0.72 6 ICPES 82KUE 01 6.4 POL 83HOL 01 6.5 0.2 RTNA 78K0B 01 6.5 0.3 RTNA 79K0B 01 6.7 0.8 ICPES 84ABD 01 7.5 0.5 RTNA 77MEL 01 8.1 FAA 82H0E 01 8.1 0.2 ICPES 79HER 01

Cone Uneer Com Method Reference

4100 200 ICPES 84NAD 01 4500 ICPES 78CAP 01 4530 120 11 COLOR 84LIN 01 4600 100 ICPES 84ABD 01 4814 300 ICPES 84PRI 01 4865 ICPES 81 GOO 01 5082 192 11 ICPES 81MUN 01 5100 FAA 79EDI 01 5100 120 ICPES 84U0L 02

5100 200 CPAA 83MAS 02

5120 60 11 ICPES 81MUN 01 5200 200 11 ICPES 82 J ON 01 5240 70 6 ICPES 82KUE 01 5300 70 6 ICPES 82KUE 01 5300 100 11 ICPES 82J0N 01 5300 300 ICPES 85WHI 02

5350 45 6 ICPES 82KUE 01 5360 270 ICPES 81 OWE 01 5400 ICPES 79EDI 01 5500 200 11 ICPES 82J0N 01 5500 300 14 FAA 84LIN 01 5500 500 14 AA 84LIN 01 5600 100 11 COLOR 84LIN 01 5600 300 14 FAA 84LIN 01 5600 400 7 NM 81SHI 01 5700 200 11 ICPES 82J0N 01 6000 100 ICPES 79HER 01

»b (ug/g)

0.8 0.1 11 ICPES 82JON 01 0.8 0.3 11 ICPES 82 J ON 01 1.0 0.1 FAA 80LEG 01 1.0 0.8 ICPES 79HER 01 1.02 FAA 82H0E 01 1.03 0.15 ASV 82GAJ 01 1.04 0.09 ASV 80SZY 01 1.09 0.06 FAA 79DAB 02

1.1 11 FAA 79H0E 02

1.1 0.06 AA 82EVA 01

1.1 0.08 ASV 82SAT 02

1.1 0.1 AA 80SCH 05

1.1 0.1 D FAA 80SCH 08

1.1 0.2 FAA 81KNA 01 1.12 0.03 SSMS 77PAU 01 1.16 0.08 FAA 82RAI 01 1.18 0.12 AA 84ST0 01 1.2 FAA 80PRE 01 1.25 ASV 78CAP 01 1.25 0.2 AA 83RAP 01

1570-10
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference

Pb (ug/g) cont.

1.3 FAA 82PRE 01 1.3 6 FAA 81HIN 01 1.3 6 FAA 82K0I 01 1.3 0.4 HAA 82UEI 01 1.4 6 FAA 82K0I 01 1.4 6 FAA 81HIN 01

1.75 1.33 ICPES 82EVA 01 2.0 1.4 PAA 80YAM 01 2.2 0.6 ICPES 83SCH 03

2.5 0.4 ICPES 84ABD 01

3.1 1.6 11 ICPES 81 HUN 01 3.4 0.6 AA 84KAN 01 4.4 3.1 11 ICPES 81MUN 01

Pd (ng/g)

Pr (ng/g)

Rb (ug/g)

60

RTNA

RTNA

81BYR 01

80SLO 01

10 ITNA 78CAP 01

11 1 35 ITNA 81GLA 03

11.32 3.1 ITNA 79REN 03

11.6 0.3 ITNA 77NAD 02

12.2 0.7 FAA 83GR0 02

12.7 0.47 AA 85EVA 01 17 3 RTNA 77MEL 01 39 EXRF 81 PAR 01

S <ug/g)

2400 600 CPXRF 79REN 02

3600 500 CB 84GLA 11 3834 58 ICPES 84PRI 01 4400 400 CB 86B0U 01 4440 D CB 85JAC 01 4440 60 6 CB 84JAC 01 4500 270 WXRF 86B0U 01 4800 200 ICPES 85UHI 02

4860 D CB 85JAC 01 4860 160 6 CB 84JAC 01

Cone

Sb (ng/g)

14

27

31

38

40

44

50

50

690

Sc (ng/g)

150

153

159

160

170

170

170

180

180

470

Se (ng/g)

24

25

33

33

37

40

42.9

60

66

360

400

510

Si (ug/g)

2900

Sm (ng/g)

33

54

80

200

Uncer Com Method Reference

3

6

13

10

2

20

150

30

6

12

4

20

10

20

40

10

3

3

10

20

9

20

110

80

900

4

2120

140

11

11

ICPES 82HAH 01 ITNA 77NAD 02

RTNA 80KOS 02

RTNA 79H0E 01 RTNA 80GAL 02 ITNA 79K0B 03 ITNA 78CAP 01 RTNA 80SLO 01 ITNA 79REN 03

ITNA 80TOU 01 ITNA 86GAU 01 ITNA 84GLA 11 ITNA 78CAP 01 ITNA 80EDD 01 ITNA 77NAD 02

RTNA 80SLO 01 ITNA 79K0B 03

RTNA 77MEL 01 ITNA 79REN 03

ITNA 80WAN 01 FAA 78CAP 01 GC 81UCH 02

GC 81UCH 02

FLUOR 79WAT 02

RTNA 80KNA 01 HAA 771 HN 01 RTNA 80SLO 01 ITNA 77NAD 02 FAA 82JUL 01 HAA 82JUL 01 RTNA 82P0L 01

ICPES 84NAD 01

ITNA 80TOU 01 RTNA 83TJI 01 RTNA 80SLO 01 ITNA 79REN 03

1570-11
TABLE 1570 -2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.

)

Cone Uncer Com Method Reference | Cone Uneer Com Method Referenee

sn lug/g;

1

1 V (ug/g;

nu . vc 82HAH

1 01 1 u . yco n nni3 1

1

DTMA 82HEY 02

7 1 1

1 rPFC UrCd 78CAP 01 1 nU . 171 fT TWA 77NAD 02

1 1 Oft 1 . UO nU . n7U f U 81REE 01

i>r lug/g; 1 1 Oft 1 . UO nU . 07U f 79REE 01

1

1 • UTJ U . UOJ f TMA 82HEY 02

r ^ J 84BIS 01 1 U . U 1 PTMA 78BYR 01

f J 11 84NAD 01 1 1 13 U . U 1 o 1

1

PTUA 82HEY 02

70 1 I rPF^ 79HER 01 1 11 o ?C U . UO T TMA 76GAL 01

1 D . o 82G0L 01 1 1 ?n7 U . UUJ> 1 1

1

DTMA K 1 NM 82HEY 02

OJ m LH 85GAU 04 1 nU • n7U f 1

1

T PDFC 82J0N 01 83.7 0.7 AA 85GAU 04 1 1 34 0.06 1

1

I CPES 82 J ON 01 87 8 AA 85EVA 01 1 1 44 COLOR 85EVA 02

CAn r 81 PAR 01 i

I

1 PDPC L>r Co 83SCH 03

1 1 7 T

1 TMA 1 NM 78CAP 01 Ta fua/a) 1 U (na/a)

0 23 0 08 ITKIA 79REN 03 1

1 140 PTMA 80SLO 01 Tb <ng/g) 1

1 Yb <n<3/g)

8 1 RTNA 83TJI 01 1

1

1 PTMA i\ 1 NM 80SLO 01

in (ng/a) 1 CO oc PTMA K 1 NM 83TJI 01

110 10 ITMA 77NAD

1 02 1 (ug/g)

150 40 RTMA 80SLO 01 I

1 He PTMA 80SLO 01

1 43 1 At 82EVA 01

1 ^ . o PTMA n 1 Wn 77DER 01 8.9 1 .4 ICPES 83SCH 03 1 46 1 1

1

82JON 01 16.5 ICPES 78CAP 01 1 46 2 1

1

82JON 01 28 2 84NAD 01 1 U B O 1 1 1 1 T rPF^ 82JON 01

1 7 11 11 nnAA 79H0E 02

Tl tna/a)

1 LI n Aft Ti TMA 1 nn 79REN 03

1 L7H r 1 a C T PPF^ 84W0L 02

31 77PAU 01 1 L7H f c FAA rMM 84MIL 01

1 L7 c . ?

T rPFC 83SCH 03

1 L7 H T

1 PPFC LrCo 84ABD 01

1 HO T

1 PPFQ UrCo 78CAP 01 42 DNA 84GLA 02 1 HO T1 TMA 1 nn 78CAP 01 45 0.8 35 DMA 80GLA 04 1 HO 11 1

1

1 1 1 rpF^ Ur C O 82J0N 01 47 5 DNA 86GAU 01 1 Aft HO 1

1

1 1 1 Or C O 82J0N 01 48 2 DNA 85GAU 04 1 LRHO iJ 1

1

1 1 1 l«r CO 82J0N 01 69 120 R DNA 81GLA 03 1 Aft HO nu

f

1 rpFC Lrr CO 80SCH 08

Aft HO T T

i rPFQ Ltr Co 80SCH 05

48.9 4.6 11 ICPES 81MUN 01 49.2 0.1 PAA 80YAM 01 49.5 0.7 SSMS 77PAU 01 49.8 1.3 6 ICPES 82KUE 01

1570-12
TABLE 1570-2: INDIVIDUAL DATA FOR NBS SRM 1570 (cont.)

Cone Uncer Com Method Reference I

Zn (ug/g? cont.

50 ICPES 81 GOO 01 50 1 ITNA 77NAD 02

50 3 ICPES 85UHI 02

50.6 1.3 6 ICPES 82KUE 01 50.8 AA 80EVA 01 50.8 1.9 AA 82EVA 01

51 2 ICPES 84NAD 01 51.2 0.6 6 ICPES 82KUE 01 52 1 DCPES 79REE 01 52 1 D DCPES 81REE 01 52 2.2 ITNA 79K0B 03

52 3 AA 83RAP 01 52.6 2.5 11 ICPES 81MUN 01 52.9 2.2 6 EXRF 79MAT 01 53 11 AA 79H0E 02

53 3 11 ICPES 82J0N 01 54 1 ICPES 79HER 01 54 3 ICPES 83SCH 04

55 2 2 FAA 84MIL 01 57 8 RTNA 77MEL 01 59.7 FAA 78CAP 01 60.1 2 6 EXRF 79MAT 01 66.8 8 CPXRF 84BIS 01 72.5 1.6 RTNA 76GAL 01 72.8 1.3 AA 76GAL 01

19 EXRF 81 PAR 01

1570-13
< 3: a. O u a.

(M r\j <M rg fNj »- ro

00 fNJ

. I o trt w- T- , r- oj Kl in I rCM t\l r- K\X r-

. T- nO O O 00

-O ' . . O o N# f\J <M

f\j ^ (\j

ir> CD >0 c\i I •—

fNJ (\J ro

5 5 to 3 g -J < <o n z o a. uj -J lo O (J O U. CO

i>o cn (/>

oj «- •J' fO N» LH *~ Kl (M ^ m —

o o «- o «- +1 CO

o u-i

*- (M vj-

• 'J- ro in

o «- o +1 -M CO lA

ro o Kl (NJ

B 5 5 U O.

^ ^ in »- *- >o »- If- u-i Kl I- CO

O CO fNj in o -o

•H -M +1

f\J *o

Kl -4- (M

*0 O O K» O O T- (M - «-

•vj in K>

w w fM

in o

(M TO *— >o o r\j -o

. »- fM

in in ro o

ino +) *1 NO o in

o o

<i in »- CO ro *- Kl PO

in o -o K1 CO O (M m (M oj

T- O ^ fV

f\l +1 ' +1 PO

T- m »- o •

• CO -J' o o

ro "4- o in

-J

fM t— o

f\j -sj c

o> Q) o cn oi o) — — ^ ^

0> ^ ^ ^

0> O) CT> CT* CTi W CTi CI Ol 0> O) O) ^ "v.

CT» d O O

C71 O)

oi D) o>

0> — —' (/I I/) I/; i/i "C X3 "D OJ —

1571-1
a. {_) LO u uj I- 5£

rvj rj rsj

O U Nj (/) I O u-

«— r<j rg f\j ir>

+4 T- I N- ir»

a, u_ a (_J (X <

5 ^

a. CL

^ Kl t> Kl

l/^ fO fV O rj O *-

ir» -o o -^r OJ O O CO

»— in

O +1 <~ +4 o ^o in o • o in »—

in o c^ o

o- • in rM «-

^ *o *— in >— >o w w ^ w w 00

CO

o> ^ o o

•H -iH in -ft S S oS

<f in o +4

«— o m o • in 'CO o rvj H -M +* -H N- o o

Dl CT) CT) CTt Ol ^ ^ ^ —

D> cn oi CT) Cn (_) cn CT)

CT) tTi CTi CTi 0>

cr at

cr cn CT> cn

Di cn o> cn ^ ^

D) 0> CT>

CT> CTI CT> cn ^ ^

m Qt w cn

o o o

f\j H- cn CD D cn cn

1571-2
Ui vt Z X

»- rg ^ »- f\i »-

i/i tr»

• o o o in fM o nj ro

fM ^ fj

W vj- (rt

t/) t/l X o O (rt u LJ*/)*— t/J_IO</>t— CJ

t/> m </}

fM K) «- ^N-rof\J»-T-»-o»-'— r\j*— K»«— CO (NJ T- CO

O fO N. O

O- O O (M

>0 rj f\j T- « CO O ^

< > »- _j

«t t/i O O

Q. < Q. Q. 8 3

in N. »- >0 »— ro -J- <- (\J f^J

o o o ** O to >Q M

-J- o eo

f\J «— •- O

rvj in +1

K» O • in

«- o

Ki CO ?o ro ^ O

OJ ^ ^ ^o CO oO r- (\1

3 S

O Kl OD CO Kl

s. ^ ^ ro •-

in f\j

CM f\J o o in

in in

*- ro o p>j in o

O 00

O O O nO

CO »- o- ro ^

^ r\j r>n CO -J- r^n

o ru o

^0 ^- "-J (\J nO »- f\J fM m in f-^ K) Ki ro

o ^ o >0

in •— O' Kl

in »- rg cOKl cOOON-OOO mm t- innjfO rvjOKi rgnj

01 Ol O) O)

"»v ^ "v. o) a> D1

D) D) Dt >v ^ D) Dl CT) CT)

CTi tJi CT* CD Di CP cn 0> CT)

XI ^ ^ J3 "D

rs) ts( rsj fsj

1571-3
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (revised 3/1/86)

Cone Uncer Com Method Reference

Ag (nq/q)

< 20 L ITNA 74RAN 02

< 100 OES 75B0L 02

13 5 RTNA 80SLO 01 620 60 RTNA 74CAR 03

14000 1000 ITNA 84GIB 01

Al (uq/q)

99 OES 75J0N 02

103 22 6 ITNA 74H0F 01 110 140 R AA 75MAN 01 123 11 11 ICPES 81MUN 01 128 OES 75J0N 11 137.2 16.3 6 COLOR 85 BAR 01 140 8 ICPES 81BLA 02

146 20 ICPES 79ABE 01 151.6 8.9 6 COLOR 85BAR 01 157 ICPES 78CAP 01 165 OES 75J0N 07

187 27 ICPES 84ABD 01 196 OES 75J0N 06

201 OES 75JON 01 223 OES 75 JON 09

231 OES 75J0N 04

241 7 11 ICPES 81MUN 01 243 OES 75J0N 08

251 ICPES 81 GOO 01 255 OES 75J0N 05

278 OES 75J0N 10

296 30 ITNA 77ZIK 01 322 18 11 ICPES 82J0N 01 322 22 14NAA 81UIL 01 330 NAA 77LAU 01 333 ITNA 76BAT 01 337 ICPES 84NAD 01 343 460 RD ITNA 79 1 MA 03

343 460 R ITNA 79 1 MA 01 347 7.5 POL 72MAI 01 347 7.5 POL 77MAI 01 349.7 6.1 ITNA 77G00 01 350 ITNA 78LAU 02

359 4 lENA 79J0N 01 372 20 lENA 85GLA 02

377 21 ICPES 79MCQ 01 377 62 ICPES 85LIE 02

378 13 ITNA 75RIC 01 380 ITNA 84GLA 02

380 100 14NAA 81WIL 02

383 ITNA 78CAP 01 390 50 AA 79MCQ 01

Cone Uncer Com Method Reference

Al (uq/g) cont.

398 24 ITNA 82EHM 01 40b 11 SSMS 85V0S 01 407 11 6 ITNA 74HOF 01 420 58 ITNA 77HAM 01 430 CPAA 80HAN 01 430 40 ITNA 74RAN 02

RTNA 72M0R 03

460 7 W 81N0N 01 460 33 ITNA 79K0B 03

470 35 ITNA 81GLA 03

472 20 ITNA 84NDI 01 488 CPXRF 84ICAU 01 500 ITNA 80CRE 01 520 180 FAA 77FUJ 01 824 50 ITNA 80SLO 01

. (ug/g)

1.1 ITNA 78KEL 02

3.5 1.6 CPXRF 80KIR 01 7.5 SSMS 81VER 02

8 1 PAA 80SEG 01 8.5 0.3 HAA 74 LOO 01 8.66 1.25 ITNA 79REN 03

8.7 0.2 RTNA 73HEY 01 8.8 0.4 ICPES 80HAA 01 8.9 2.2 ICPES 81 NAD 01 9 RTNA 75ABU 01 9 0.4 H ICPES 79R0B 01

9.1 1 lENA 79KUC 01 9.2 ITNA 79KUC 01 9.25 0.44 ITNA 84NDI 01 9.27 HAA 77IHN 01 9.3 35 HAA 77TAM 01 9.4 0.5 HAA 84NAR 01 9.4 1 HAA 76V IJ 02

9.5 HAA 85 IKE 01 9.5 HAA 81INU 01 9.5 AA 83ELA 01 9.5 0.2 RTNA 83DAN 01 9.5 0.3 11 HAA 81 RAP 01 9.5 0.5 HAA 85NAR 01 9.5 0.5 RTNA 80SLO 01 9.5 0.76 RTNA 79HEI 04

9.5 0.8 RTNA 79R0S 02

9.58 2.25 ITNA 85MAD 01 9.6 FAA 82HEI 01 9.6 0.3 11 HAA 81 RAP 01 9.6 0.4 HAA 85YAM 01 9.6 0.5 AA 83RAP 01

1571-4
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(uq/g) cont.

1

1 As (ug/g) cont.

9.68 O.U NAA 74HEY

1 01 1 10.14 ASV 780AV 01 9.7 11 HAA 82CR0 03 1 10.2 35 XRF 77TAM 01 9.7 0.12 RTNA 72BYR 01 1 10.2 HAA 80HON 01 9.7 0.2 RTNA 73DAM 01 1 10.2 0.2 RTNA 85TIA 01 9.7 0.2 HAA 83MAH 01 1 10.2 0.2 HAA 77SMI 01 9.7 0.3 RTNA 79ICAN 02 1 10.2 0.2 COLOR 77BUR 01 9.7 0.3 HAA 83MAH 04 1 10.2 0.5 7 RTNA 80GAL 02

9.7 0.4 7 RTNA 80GAL 02 1 10.2 1 PAA 74CHA 01 9.7 0.4 7 RTNA 77GIL 03 1 10.2 1 NAA 77JER 01 9.7 0.4 RTNA 78GAL 01 1 10.3 HAA 81ARA 01 9.7 0.4 ITNA 75RIC 01 1 10.3 FAA 82PER 02

9.76 0.17 RTNA 79H0E 01 1 10.3 0.2 HAA 80AGE 02

9.8 HAA 84IKE 01 1 10.3 0.2 34 HAA 78FLA 01 9.8 0.1 HAA 81KNA 01 1 10.3 0.4 7 RTNA 77GIL 03

9.8 0.1 11 HAA 81 RAP 01 1 10.3 0.4 7 RTNA 80GAL 02

9.8 0.3 RTNA 82COR 01 1 10.3 0.9 ITNA 81K0S 01 9.8 0.4 H ICPES 81PIC 01 1 10.3 1.6 RTNA 79REN 01 9.8 0.9 COLOR 76VIJ 02 1 10.4 0.4 ITNA 78LAU 02

9.8 0.9 ESCA 78CAR 01 1 10.43 0.22 HAA 81UTH 01 9.8 3.2 XRF 78STA 02 1 10.5 ITNA 82AKA 01 9.85 HAA 84YAM 01 1 10.5 1 lENA 79KUC 01 9.9 FAA 83X1

A

01 1 10.5 HAA 83KUM 01 9.9 0.1 lENA 78WAN 01 1 10.5 0.6 HAA 85NAR 03

9.9 1.3 RTNA 85GAU 04 1 10.5 1 PAA 76ICAT 04

9.9 1.6 ICPES 85LIE 02 1 10.6 ASV 81LEE 01 9.93 0.13 ITNA 73DAM 01 1 10.6 0.3 14NAA 81WIL 01 9.98 0.31 HAA 80TAM 01 1 10.6 0.5 14NAA 81WIL 02

10 RTNA 798YR 01 1 10.6 0.6 6 HAA 81KAH 01 10 11 HAA 82CRO 03 1 10.6 0.8 EXRF 73GIA 01 10 HAA 79PEA 01 1 10.6 0.8 RTNA 740RV 01 10 RTNA 72M0R 03 1 10.7 0.4 FAA 78HAY 01 10.0 0.1 6 HAA 81KAH 01 1 10.7 1 6 ITNA 74BEC 01 10.0 0.1 W 81N0N 01 1 10.8 6 NAA 78GAN 01 10.0 0.1 ICPES 84LIV 01 1 10.8 FAA 78CAP 01 10.0 0.1 FAA 79PET 01 1 10.8 HAA 81BR0 01 10.0 0.4 RTNA 78GIL 01 1 10.8 lENA 84GLA 02

10 1 6 ICPES 85ABD 01 1 10.8 0.5 lENA 82GLA 02

10 1 EXRF 80DYC 01 1 10.8 0.9 RTNA 76MEL 01 10 2 COLOR 79MCQ 01 1 10.82 0.25 HAA 77YAS 02

10 2 MPOES 83SAR 01 1 11 ICPES 79MCQ 01 10 2 ITNA 77MIN 01 1 11 ICPES 79MCQ 02

10 14 RD ITNA 79 1 MA 03 1 11 ICPMS 83D0U 02

10 14 R ITNA 79 1 MA 01 1 11.0 0.6 PAA 78HIS 01 10.1 ITNA 80CRE 01 1 11 1 PAA 76KAT 02

10.1 0.2 19 ITNA 74RAN 02 1 11 1 HAA 76FI0 01 10.1 0.3 7 RTNA 77GIL 03 1 11.0 1.5 7 RTNA 80GAL 02

10.1 0.3 RTNA 78WEE 01 1 11 2 RTNA 77KUS 01 10.1 0.3 ITNA 80GAL 02 1 11 2 ITNA 85WAH 01 10.1 0.4 lENA 81K0S 01 1 11.0 2.9 ITNA 84TU 01 10.1 0.8 EXRF 79GIA 01 1 11 3 ITNA 77ZIK 01

1571-5
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

:onc Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/g) cont.

1

1 As (ug/g) cont

11.5 11 SSMS 85VOS

1 01 1 14.1 1.5 SSMS 84V0S 01 11.5 0.3 GCMES 75TAL 01 1 14.3 XRF 78CAM 02

11.5 0.47 HAA 81YAN 01 1 14.3 0.4 EXRF 77NIE 01 11.5 0.5 HAA 81YAN 01 1 14.7 2 ITNA 83AHM 01 11.5 1.5 RTNA 73GOE 01 1 15 0.1 RTNA 77BAN 03

11.5 1.5 D RTNA 74G0E 01 1 15.3 0.5 EXRF 73SPA 01 11.6 HAA 77SIE 01 1 15.3 1.6 SSMS 84V0S 01 11.6 0.27 H HAA 76SIE 01 1 15.3 2 ITNA 79AHM 01 11.6 1.3 ITNA 74NAD 02 1 15.4 0.2 19 ITNA 74RAN 02

11.6 1.8 RTNA 79NIC 01 1 15.7 5 CPXRF 85CLA 01 11.7 NM 83MAR 03 1 16 AA 79HIL 01 11.8 0.8 SSMS 77D0N 01 1 16 2 CPXRF 77CAM 01 11.9 H FAE 79FEL 01 1 17 CPXRF 76ZEI 01 11.9 0.1 FAA 80DUP 01 1 17 CPAA 78MCG 01 11.9 0.2 ITNA 81HAB 01 1 19 6 ICPES 85ABD 01 11.9 0.6 ICPES 830LI 01 1 26 AF 85NAR 02

11.98 0.08 H ICPES 81 PAH 01 1 38 EXRF 81 PAR 01

12 ICPES 84MAR 01 1 12 RTNA 74ERD 01 1 AS(III) (uq/q)

12 0.38 HAA 82TAM 01 1 12 0.6 AE+AF 82MAT 01 1 4.9 HAA 76AGG 01

12 0.6 11 HAA 82JON 01 1 12 1 ITNA 76KUC 01 1 Au (ng/g)

12 1.5 RTNA 83BRA 01 1 12 2 HAA 79ST0 01 1 0.72 0.25 RTNA 84TJI 01

12 2.5 ITNA 77HAM 01 1 0.78 0.15 ITNA 79REN 03

12 2.6 EXRF 75REU 01 1 0.97 0.09 RTNA 77NAD 01

12 3 ITNA 81KUL 01 1 1 RTNA 72M0R 03

12.15 0.43 NAA 76GUZ 01 1 1 0.5 ITNA 82QUR 01 12.2 0.3 AA 84MAT 01 1 1.2 1 lENA 79KUC 01 12.3 0.2 ITNA 79K0B 03 1 1.4 ITNA 81KUL 01 12.3 0.4 RTNA 73TJI 01 1 1.4 0.3 ITNA 85MAD 01 12.4 1 ITNA 85NDI 01 1 1.4 0.5 lENA 81K0S 01 12.5 11 SSMS 85V0S 01 1 1.43 0.08 RTNA 82ZEI 01 12.7 0.7 ITNA 79JER 01 1 1.5 ITNA 79KUC 01 12.7 2 ITNA 82QUR 01 1

f 0.5 RTNA 77KUS 01 12.9 0.4 11 HAA 82J0N 01 1 1.5 4 R* RTNA 80SLO 01 12.9 2.3 SSMS 84V0S 01 1 1.6 0.2 RTNA 83SIR 01

13 0.1 ITNA 75B0L 01 1 1.64 0.1 ITNA 77MIN 01

13 1 H ICPES 82HAH 01 1 1.8 1 lENA 79KUC 01

13 2.4 SSMS 84V0S 01 1 1.8 0.3 ITNA 81HAB 01

13 3 CPAA 77ZIK 01 1 2 0.8 ITNA 81K0S 01 13.2 CPXRF 75CAM 01 1 3.5 0.6 RTNA 74CAR 03

13.3 ICPES 85NAR 02 1 4.2 FAA 85BRO 01 13.3 0.4 HAA 76WAU 01 1 13.4 0.93 COLOR 73LEB 01 1 13.5 HAA 76AGG 01 (

1 13.7 CPXRF 84KAU 01 1 14 1 ITNA 78FUR 01 1 14.1 6 NAA 78GAN 01 1

1571-6
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

B <ug/g)

16 12 ITNA 82SCH 05

22.55 6 AE+AF 74DAU 01 23 OES 75 JON 10

24 2 ICPES 79HER 01 25.15 6 AE+AF 74DAU 01 27 OES 75 JON 05

27 OES 75JOM 02

30 OES 75JON 01

31 3 ICPES 84PRI 01 31.2 2.8 NM 79YAN 01 31.5 ICPES 81 GOO 01 31.7 TCGS 84HIG 01 31.9 4.7 14 FAA 79SZY 01 32 OES 75 JON 04

32 OES 75J0N 09

32 4 ICPES 79ABE 01 32.2 0.4 TCGS 79AND 01 32.5 0.5 COLOR 79YAN 01 32.8 2.3 6 TCGS 76GLA 01 33 OES 75J0N 07

33 OES 75J0N 06

33 2 11 ICPES 79MIZ 01 33 4 CPAA 80HAN 01 33.2 0.1 TCGS 79FAI 01 33.3 11 COLOR 85SHI 02

33.3 2.3 6 TCGS 76GLA 01 33.4 11 COLOR 85SHI 02

33.4 0.7 ICPES 81KNA 01 33.5 2.8 11 ICPES 81MUN 01 34 1 11 ICPES 79MIZ 01 34.8 0.9 11 ICPES 81MUN 01 35.1 9.9 14 FAA 79SZY 01 36 CPAA 81SAS 02

36 OES 75JON 03

36 3 CPAA 81SAS 01 36 5 CPAA 75MCG 01 37 3 ICPES 84 SOB 01 38 OES 75J0M 11 38 OES 75 JON 08

40 1 11 ICPES 79MIZ 01

(uq/q)

0.3 0.1 CPXRF 77RIN 01 14.7 SSMS 81VER 02

25.9 6.8 ITNA 81HAB 01 28 ITNA 80CRE 01 30 NAA 74BEL 01 35 11 SSMS 85V0S 01 35.9 7 CPXRF 85CLA 01

Cone Uncer Com Method Reference

Ba ( ug/g ) cont.

37 6 ICPES 83BRA 02

37 11 5 ITNA 80TOU 01 37.7 6 ICPES 83BRA 02

37.9 6 ICPES 83BRA 02

37.9 1 lENA 79KUC 01 38 OES 75 JON 05

38 4.7 CPXRF 80KIR 01 39.4 ITNA 79KUC 01 40 11 SSMS 85VOS 01 40 OES 75 JON 03

40 NAA 77LAU 01 40 3 9 ITNA 78LAU 02

41 1.3 RTNA 77GUI 03

41 4 ITNA 79SAT 01 42 2 ICPES 79MCQ 02

42 2 ICPES 79MCQ 01 42 6 ITNA 78LAU 02

43 OES 75 J ON 11 43 3 ITNA 85WAH 01 43 5.7 ITNA 77HAM 01 43.9 1 lENA 79KUC 01 44 5 SSMS 84V0S 01 44 57 R AA 75MAN 01 44.3 AA 74BUS 02

44.8 2.5 lENA 81K0S 01 45 ITNA 78CAP 01 45 OES 75J0N 04

45 1 ICPES 85LIE 02

45 6 W 81N0N 01 45 7 SSMS 84V0S 01 45.3 2.7 ITNA 81K0S 01 45.6 2.43 ITNA 85MAD 01 45.7 ICPES 84NAD 01 46 6 ICPES 83CHA 01 46 6 ITNA 74RAN 02

47 3 ITNA 81KUL 01 47.3 2.7 ITNA 84TU 01 48 6 ICPES 83CHA 01 48 8 SSMS 84V0S 01 50 14 FAA 86GAU 01

51 RTNA 72M0R 03

51.3 4.5 PAA 74CHA 01 51.9 ICPES 78DAH 01 52 OES 75J0N 01 52 8 SSMS 84V0S 01 59.54 1.81 ITNA 79REN 03

62 21 ITNA 77ZIK 01 80 22 14NAA 81WIL 02

1571 -7
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Be (ng/g) Br (uq/g) cont.

13.7 1.8 6 ICPES 1 9.2 ITNA 80CRE 01 U.8 1.6 6 ICPES 82SCH 01 1 9.2 0,2 ITNA 74RAN 02

19 4 ICPES OJ Lie 9.3 0,6 EXRF 73GIA 01 26 1 FLUOR 77WIC 01 1 9.3 1,4 RTNA 78WEE 01 26 3 FAA 01 1

1 9.4 ITNA 79KUC 01 30 4 VV 01 1

1 9.5 1 lENA 79KUC 01 36 4 11 FAA 75OWE 01 1 9.5 1 lENA 79KUC 01 67 7 11 FAA 75OWE 01 1 9.5 XRF 78CAM 02

110 10 GC f jo^.n 01 1

1 9.5

9.5

0,8

1

RTNA

EXRF

76MEL 03

77NIE 01

Bi (nq/g) 9,6

9.6

1 .2 2,8

6 NAA

ITNA

78GAN 01 77HAM 01

4 1 H ICPES A1P&H o 1 rMn ni 1

1 9.7 1,1 ITNA 78GIL 01 30 FAA 77RPI1 ni 1

1 9.8 0,78 ITNA 77STE 02

39 FAA 791 NU 01 1 9.8 0.8 RTNA 79CR0 01 64 FAA o^nc 1 ni 1

1 9.8 1.1 CPXRF 85CLA 01 100 11 SSMS 85VOS 01 1 9.9 0.2 lENA 81K0S 01 100 10 HAA ni 1

1 10 1 ITNA 76KUC 01 110 20 POL 1 CvlfK 1 ni 1

1 10 2.1 W 81N0N 01

110 20 POL TVMfl I f 1 rin 1 01\J 1

1 10 2,2 XRF 78STA 02

110 100 POL 7AM&! 01 1

1 10.1 0,8 ITNA 77GUI 02

160 AF 85NAR 0? 1 10.2

10.5

10,6ITNA

ITNA

81KUL 01 81K0S 01

Br (up/g) 10,5

10,6

1 ,4

1 ,5

ITNA

ITNA

79CR0 01 84TU 01

5 5 ITNA 777 T If 01 1 10.8 0,4 35 NAA 81GLA 03

6.3 2 EXRF 77FL0 01 1 10,8 0,9 6 NAA

Mufti ^ A 78GAN 01 6.6 0.4 EXRF 73SPA 01 1 10.9 ITNA 80SAT 01 6.6 0.4 5 lENA 79GLA 02 1 11 ITNA 78CAP 01

7.1 EXRF 81BIS 01 ! 11 0.7 5 ITNA 80TOU 01 7,3 3.2 CPXRF 80KIR 01 1 11 1 .2 ITNA 79K0B 03

7.3 9.3 R ITNA 79 1 MA 01 1 11.5 1 .5 ITNA 85WAH 01 7.3 9.3 RD ITNA 79 1 MA 03 1 12 1 .3 ITNA 79AHM 01 7.4 0.2 ITNA 01 1

1 12 3 ITNA 77ZIK 01 7.8 0.3 EXRF WW I Irf 01 11 12.1 1,3 ITNA 83AHM 01 8.2 RTNA 03 1 12.5 ITNA 82AKA 01 8.2 0.6 ITNA 01\J 1 1 I 34 EXRF 81 PAR 01 8.3 0.5 5 ITNA fin HDP 01 1

t 8.48 0.07 5 ITNA 01 1 C (%)

8.5 0.5 6 ITNA 74BEC 01 I 8.6 ITNA 85MIS 01 1 45.6 1 .2 COUL 86CAH 01 8.7 ITNA 0? 1

1 45.76 0.51 CB 82GLA 02

8.8 0.6 5 lENA 1 45,8 1 .3 35 CB 79GLA 04

8.8 1 .6 EXRF 75REU 01 1 46 2 TCGS 79FAI 01 8.87 CPXRF 84KAU 01 1 46,35 0.31 CB 80SCH 02

9.0 0.5 EXRF 79GIA 01 1 47 5 35 TCGS 79GLA 04

9.0 0.5 ITNA 78LAU 02 1 52 5 TCGS 79AND 0^

9.0 0.62 ITNA 84NDI 01 1 9.1 0.5 ITNA 78WEE 01 1 9.19 1.39 ITNA 79REN 03 1

1571-8
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ca (% ) Ca (%) cont.

0.9 11 SSMS 85VOS 01 1 2.04 OES 75JON 03

1 ,58 35 AA 81GLA 04 1 2.04 AA 80URE 01

1 .6 2.26 R ITNA 79 1 MA 01 1 2.04 0.02 11 AA 78GAI 01

1 .6 2.26 RD ITNA 79 1 MA 03 1 2.05 6 ICPES 83CHA 01

1 .63 OES 75 JON 07 1 2.05 0.9 XRF 78STA 02

1 .69 AF 85DAV 01 1 2.06 COLOR 77HAM 04

1.69 0.05 CPXRF 85CLA 01 1 2.07 0.06 lENA 79JON 01 1.74 CPXRF 84KAU 01 1 2.07 0.06 11 ICPES 81MUN 01

1 .74 OES 75 JON 05 i 2.08 OES 75J0N 11

1 .8 NAA 77LAU 01 ! 2.08 OES 75JON 09

1 .8 OES 75JON 02 1 2.08 0.01 PAA 74CHA 01

1.81 ITNA 82AKA 01 1 2.08 0.02 11 AA 78GAI 01

1.8'! 0.24 5 ITNA 80TOU 01 i 2.08 0.04 ITNA 79K0B 03

1.83 0.07 CPXRF 80KIR 01 j 2.08 0.06 ICPES 79ABE 01

1 .86 0.1 14NAA 77VAN 01 1 2.09 0.04 11 ICPES 81HUN 01

1 .89 6 ICPES 83BRA 02 1 2.1 ICPES 81 GOO 01 1.90 0.11 ITNA 79REN 03 1 2.1 ICPES 83KEI 01 1.91 AA 77BRU 01 1 2.1 RTNA 72M0R 03

1.91 OES 75JON 10 r 2.1 0.05 ITNA 81K0S 01 1.92 EXRF 81BIS 01 1 2.1 0.08 6 EXRF 79MAT 01 1.93 0.07 EXRF 79KUE 01 1 2.1 0.2 14NAA 80FAA 01 1.93 0.09 ITNA 77ZIK 01 I 2.1 0.2 ITNA 78LAU 02

1.94 OES 75 JON 04 1 2.11 ICPES 81WEI 01 1.96 0.002 11 AA 75ISA 01 1 2.11 AA 79HIL 01 1.96 0.06 FE 78K0R 01 1 2.11 0,08 6 EXRF 79MAT 01 1.97 6 ICPES 83BRA 02 ! 2.12 0.07 lENA 81K0S 01 1.97 0.03 11 ICPES 82 J ON 01 1 2.13 SSMS 81VER 02

1.97 0.05 PAA 76KAT 02 1 2.13 ITNA 76BAT 01 1.97 0.055 PAA 76KAT 04 1 2.13 0.09 ITNA 75RIC 01 1.97 0.08 TCGS 79AN0 01 1 2.13 0.11 TCGS 79FAI 01 1.97 0.15 14NAA 81WIL 02 1 2.14 6 ICPES 83CHA 01 1.98 0.02 ICPES 85LIE 02 i 2.14 0.02 ITNA 78FUR 01 1.98 0.04 11 ICPES 82 J ON 01 1 2.14 0.11 ITNA 84TU 01 1.98 0.05 ICPES 79MCQ 02 1 2.145 0.017 CPXRF 81 ROB 02

1.98 0.07 ICPES 79MCQ 01 1 2.15 COLOR 80LAU 01 1.98 0.08 EXRF 75REU 01 1 2.15 ITNA 78CAP 01 1.99 XRF 78CAM 02 1 2.17 OES 75 JON 08

1.99 0.06 EXRF 77NIE 2.17 0,03 EXRF 80DYC 01 2.00 1 J L On £ . 1 o AA niU 1 2.00 0.08 ITNA 80SLO 01 1 2.2 EXRF 810HT 01 2.00 0.19 ICPES 85LY0 01 j 2,2 0.02 ICPES 79HER 01 2.01 0.02 AA 79MCQ 01 1 2.2 0.05 PAA 78HIS 01 2.01 0.18 RTNA 80CAN 01 1 2.2 0.1 ITNA 81KUL 01 2.02 0.002 11 AA 75 ISA 01 ! 2.21 0.15 ITNA 77HAM 01 2.02 0.11 EXRF 82DAK 01 ! 2.23 0.12 ITNA 83AHM 01 2.03 COLOR 840GU 01 1 2.26 0.58 ICPES 84ABD 01 2.03 ICPES 780AH 01 1 2.28 CPAA 80HAN 01 2.03 0.02 11 ICPES 82J0N 01 ! 2.29 OES 75JON 06

2.03 0.04 11 ICPES 82J0N 01 1 2.29 0.04 W 81N0N 01 2.04 0.06 CPAA 77ZIK 01 I 2.41 OES 75JON 01

1571-9
TABLE 1571-2: iNDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ca (%) cont. Cd (ng/g) cont

2.46 0.09 5 ITNA 80TOU

1 01 1 116 10 FAA 84GLA 02

2.6 ICPES 84NAD 01 1 116 13 RTNA 80GRE 01 2.63 ICPES 78CAP 01 1 120 RTNA 85TIA 01 3.04 11 SSMS 85VOS 01 1 120 AA 84SAT 02

5.01 EXRF 81 PAR 01 1

1

120

120

11 FAA RTNA79H0E 02

74R00 01 Cd (ng/g) 1

1

120

120

7

10 11

AA

ASV

83FAG 01

84L0C 01 70 RTNA 80SLO 01 1 120 10 11 ASV 84L0C 01 70 FAA 75LO0 01 1 120 10 lENA 81K0S 01 72 14 FAA 81ZAU 01 1 120 10 ASV 84L0C 01 90 6 AF 84NAR 02 1 120 10 RTNA 83BRA 01 90 AA 79HIL 01 1 120 10 RTNA 740RV 01 90 10 FAA 80LEG 01 1 120 14 NAA 76GUZ 01 92 18 RTNA 73TJI 01 1 120 20 11 FAA 78SMI 01 95 11 FAA 79H0E 02 1 120 20 11 FAA 78SMI 01 100 AA 79NAR 01 j 120 30 AA 86GAU 01 100 FAA 80PRE 01 1 120 40 6 AA 84KAN 01 100 11 SSMS 85V0S 01 1 120 50 AA 82R00 03

100 6 AF 84NAR 02 1 120 80 11 ICPES 82JON 01 100 AA 73L00 01 1 130 ICPES 84MAR 01 100 4 ASV 82SAT 02 1 130 ICPES 840HL 01 100 10 ASV 85ADE 01 1 130 FAA 82HEI 01 100 10 POL 74MAI 01 1 130 ICPES 85NAR 02

100 20 AA 83RAP 01 j 130 5 FAA 74TAL 01 100 40 HAA 82UEI 01 1 130 5 7 AA 73TAL 01 105 FAA 82 HOE 01 1 130 7 FAA 74TAL 01 105 5 FAA 79ST0 01 1 130 7 7 AA 73TAL 01

105 10 FAA 84ROS 01 j 130 10 ICPES 85KUM 01 106 9 FAA 74RAI 02 1 130 20 ITNA 81K0S 01 108 8 AE+AF 74RAI 02 1 130 160 11 ICPES 81MUN 01 109 2 FAA 790AB 02 1 135 FAA 840HL 01 110 AF 85NAR 02 1 140 AA 83ELA 01 110 FAA 82PRE 01 1 140 40 FAA 82UEI 01 110 FAA 82AKA 01 1 150 50 AA 80AGE 01 110 RTNA 79BYR 01 1 150 50 AA 76GAL 01 110 6 AA 80SCH 05 1 150 60 TCGS 79AND 01 110 10 D FAA 80SCH 08 1 160 10 ICPES 79HER 01 110 10 AA 82RIT 01 1 160 16 FAA 76URE 01 110 10 FAA 81KNA 01 1 160 50 RTNA 80VAL 01 110 10 ICPES 83SCH 04 1 160 70 11 ICPES 82J0N 01 110 10 NAA 77JER 01 1 170 AF 78URE 02

110 10 PAA 74CHA 01 1 170 70 11 ICPES 82JON 01 110 10 AA 78RIT 01 1 180 16 AA 79AB0 01 110 10 AF 75EPS 01 1 190 40 FAA 77BRU 01 110 10 AA 75EPS 01 1 200 80 RTNA 76GAL 01 114 18 FAA 84GLA 11 1 200 100 11 ICPES 82JON 01 115 8 AA 84ST0 01 1 230 20 FAA 73SEG 01 116 8 7 RTNA 80GAL 02 1 230 60 ITNA 74RAN 02

116 8 RTNA 78GAL 01 1 260 70 6 AA 84KAN 01

1571-10
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method

Cd (ng/q) cont. CI (uq/g) cont.

260 200 ICPES 85LIE

1 02 1 720 15 W

350 20 ICPES 84ABD 01 1 720 25 ITNA 370 10 6 ICPES 85ABD 01 1 720 140 PAA 580 16 AA 79AB0 01 1 730 26 NAA

660 340 AA 79M0N 01 1 730 30 TCGS

2000 AE+AF 79ULL 01 1

1

730

732

60

29

ITNA

ITNA Ce (Ufl/q) 1 732 29 NAA

1 739 ITNA 0.75 0.067 ITNA 77HAM 01 1 740 30 TCGS

0.82 11 SSMS 85V0S 01 1 740 58 ITNA 0.8A 0.04 ITNA 81K0S 01 1 750 ITNA 0.866 0.059 RTNA 83TJI 01 1 750 19 ITNA 0.9 D RTNA 82LAU 01 1 750 35 ITNA 0.9 RTNA 77LAU 02 1 755 ITNA

0.91 0.06 RTNA 80SLO 01 1 760 ITNA 0.92 0.14 ITNA 77NAD 02 1 770 XRF 0.949 0.076 RTNA 86TSU 01 1 770 150 CPXRF

0.97 ITNA 79KUC 01 1 770 240 EXRF 0.98 0.05 ITNA 78LAU 02 1 773 108 ITNA 0.98 0.07 W 81N0N 01 1 790 RTNA

1 RTNA 72M0R 03 1 800 40 lENA

1 NAA 77LAU 01 1 810 150 EXRF

1.03 0.07 ITNA 84TU 01 1 838 ITNA

1.05 0.33 RTNA 83SIR 01 1 950 70 14NAA

1.1 SSMS 78URE 01 1 1.2 0.2 ITNA 81KUL 01 1 Co <ng/g)

1.25 0.41 ITNA 840DD A 4 1 01 1 1.28 0.18 RTNA 840DD 01 1 100 RTNA

1.38 0.23 ITNA 85MA0 A 4 1 01 1 105

107

2

3

ASV

VOLT

CI (ug/q) - 110

112

20

17

6 NAA NAA

53 SSMS 81VER 02 1 120 50 AA

400 770 RD ITNA 79 1 MA 03 1 130 ITNA 400 770 R ITNA 79 1 MA 01 1 130 NAA 510 35 ITNA 81GLA 03 1 130 ITNA 580 27 FAA 78TSLI 01 1 130 ITNA 630 24 AA 78TSU 01 1 130 10 D RTNA

632 80 ITNA 77ZIK 01 1 130 10 ITNA 638 27 ISE 81 NAD 01 1 130 10 RTNA

675 ITNA 78CAP 01 1 130 20 6 ITNA 685 32 PAA 74CHA 01 1 130 20 RTNA

687 32 ITNA 83LI 01 1 130 20 RTNA

690 NAA 76GUZ 01 1 138 10 ITNA 700 60 35 ITNA 81GLA 04 1 140 NAA

706 26 ITNA 78FUR 01 1 140 10 ITNA

715 CPXRF 84KAU 01 1 140 30 6 NAA

717 193 PAA 76KAT 04 1 142 7 FAA 719.5 ITNA 82AKA 01 1 145 ITNA

Reference

81N0N 01 85UAH 01 76KAT 02

78GAN 01 79FAI 01 80SLO 01 77GUI 02

76MIL 02

76BAT 01 79AND 01 77HAM 01 74RAN 02

75RIC 01 77STE 02

80CRE 01 84GLA 02

78CAM 02

79REN 02

77NIE 01 84NDI 01 72M0R 03

79JON 01 80DYC 01 86GAU 01 81WIL 02

72M0R 03

85ADE 01 84ADE 02

78GAN 01 76GUZ 01 76GAL 01 78CAP 01 77LAU 01 80CRE 01 79KUC 01 74G0E 01 78LAU 02

73G0E 01 74BEC 01 77KUS 01 83SIR 01 74RAN 02

74BEL 01 78GIL 01 78GAN 01 75HAG 01 82AKA 01

1571-11
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com MetnoQ Reference | Cone Uncer Com Metnoa Reference

Co (ng/g) cont

.

-

1

1 cr (ug/g) cont

.

1 K(\ 1 3U 1 1 NA 80SAT

1 01 1 3 n c. • u

vAAA A 7Qurf\ f\ 1

1

1 3U 1

1 IcNA 79KUC 01 1 9£.Un

1 jV 1

1

r/W 80FUD 01 1 9c . nU n ix fir ~ Ah 7ALmi ft 1r OWUL U

1

1 1 1 NA 76KUC 01 1 9 ft nUmC9 Ao T1 TMA 1 NM T/Dcr ftl

lOU in i 1 NA 82C0R 01 1 9 n"; 1

1

AAA A

1 Ad 3n K 1 NA 80SLO 01 1 9 9 n 9 flA CHD ft

1

i7n in 1 1 NA 79K0B 03 1 9 9 n X K 1 NA 77un ftl

1 f u in TTUA 1 1 NA 79SAT 01 1 9 9 n A VV Qiui^U ftl O 1 NUN U

1

1 7n inlU TTUA 1 1 NA 84TU 01 1 9 9 C.C 1

1 PDVD C ftftb^lD ftl

1 fin T TUA I 1 NA 85MIS 01 1 9 9 c.V nKA A AA TIhIIAU ftl

1 An 1

1

1

1

85V0S 01 1 9C,CC99 n 9 u . c DArAAA 7A r U A ftl mn 5n DTUA K 1 NA 77MEL 01 1 9 9X zo

y A A NAA^ Tftf^AU ftl

r OuAN U

1

loU CO TTUA 1 1 NA 77HAM 01 1 9 9t; 1

1

1 1 A A AA 70unc no mnloU tnou T TUA 1 1 NA 81KUL 01 1 9 9A 1

1

1 1 CCMC nR\/nc ftl ion c3

1

1

1

1

CAA rAA 80FUD 01 ! 9 XX LrAKr

ion IVU L.n hU \A/ VV 81N0N 01 1 9 X7 nU.Urn7 70UAC ftl ion lyu inn 1 uu 85LIE 02 1 9 A DTUA K 1 NA 7Cadii ftl 10A ITO A1O 1 TTUA 1 1 NA 85MAD 01 j 9 A T TUA 1 1 NA 70b'l ir ftl 5nn AAAA 8ASAT 02 1 9 A A A AA OTci A ftl

51 n 9n TTUA 1 1 NA 81K0S 01 1 9 A n 1 U. 1 T TUA 1 1 NA oDWAn QCMAU ftl U

1

01 n O

T TUA 1 1 NA 74BEC 01 1 9 A n 1 U. 1 1 1 T PDCC oo mu ftl

51 n T TUA 1 1 NA 85UAH 01 1 9 A n 1 U. 1 y

T TUA 1 i NA 7fti Ai 1 no xn T TUA 1 1 NA 82QUR 01 1 9 A n 1 U . 1 DTUA K 1 NA TAMP 1 07

55n An TTUA 1 1 NA 78FUR 01 1 9 A n 1 U . 1 LnCrlL 7Al T ni

9xn xn TTUA 1 1 NA 79AHM 01 1 9 A n X T1 TMA 1 NM 7ftl AI 1 ftp xn TTUA 1 1 NA 83AHM 01 1 9 L ftu . XAoo TTMA k 1 nM 77HAM ft1

1 Cnn 81K0S 01 1 0w . AO

fiiDiA no

CO\J i?n cJ i 1 tin 80TOU 01 1 9 L 1 1 wr A(\ r ASPI A ft1 ?on inn TTMA 77ZIK 01 1 9 AA 0 095 RTMA

ty f rni HP 82KIR 01 1 9£ . AAX HOJ 0 09 1

1

1 1 PTMA

300 FAA 82H0E 01 1 2.47 0.14 FAA 75CAR 02

?nn An TTMA 1 1 NA 76GAL 01 1 9e. . AOS HTJ ftU . niA U 1

H

1

1

PTMA

320 11 SSMS 85VOS 01 1 2.5 RTNA 72M0R 03

Apn A7n T TUA 1 1 NA 75RIC 01 1 9 >; Cm J T

I TMA 1 NM AAn inn 1 uu T TUA 1 1 NA 79REN 03 1 9 <; c . 9

1

1

1

1

Q^x/nc fti Ann An T PDCC 84ABD 01 1 9C.J nU.HA T

I TUA 1 NM 7A^iir ni

oUU Ann Ann OUU VDC 78STA 02 1 9c . 9

9 i^A ^ . 9o

1 A

nil U. 1 1

CAKr

CAA rAA

TXHTA ftl r IM u 1 A'^rAD ft5

cr \ug/gj 1 9 S7A nU.Uni1 T1 TMA 1 NM 7Qurr ftl

1 c • 9o n nA TTMA 1 1 NM fti^nQ ftl

1 n7 n IX U. \J o

UA A NAA 78GAN 01 1 C9 . SO97 nU is . 1 9 7 PAA rMM QftruA ftl

1 1 n 5 u . ^

1

1

1 1 I PDCC 1 Lrtd 81MUN 01 1 9C.OA 1

1

1 1 MMAA 70Hnp no

1 c

1 • J

A A AA 73L00 03 1 9 A n 1 T1 TMA 1 NM 70^nB ft7

n 9 u . ^ o 1 Lrto 85ABD 01 1 9 A n 1 XR rFAAMM ftiRi A nx

1.9 POL 83H0L 01 1 2.6 0.2 NM 80SHI 01 1.9 0.3 11 ICPES 81MUN 01 1 2.6 0.2 6 ITNA 74BEC 01 1.9 0.3 ICPES 85LIE 02 1 2.6 0.3 11 ICPES 82JON 01 1.97 0.A4 NAA 76GUZ 01 1 2.6 0.4 ITNA 78FUR 01 2.0 NAA 74BEL 01 1 2.64 0.2 ITNA 85NDI 01 2.0 ICPES 79MCQ 01 1 2.65 0.16 7 FAA 80CHA 01

1571-12
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Cr (ug/g) cont.

2.67 0.15 7 RTNA 80GAL 02

2.67 0.15 RTNA 78GAL 01 2.7 ITNA 78CAP 01 2.7 AA 81ARA 01 2.7 FAA 82H0E 01 2.7 0.1 ITNA 84TU 01 2.7 0.17 AA 80AGE 01 2.7 0.2 AA 83RAP 01 2.7 0.2 ITNA 79SAT 01 2.7 0.2 DCPES 79REE 01 2.7 0.2 D DCPES 81REE 01 2.7 0.3 ITNA 82C0R 01 2.72 0.15 ITNA 84GIB 01 2.8 SSMS 81VER 02

2.8 NAA 77LAU 01 2.8 0.2 ITNA 75RIC 01 2.8 0.2 ITNA 79AHM 01 2.8 0.2 ICPES 81KNA 01 2.8 0.2 ITNA 82QUR 01 2.8 0.2 ITNA 83AHM 01 2.8 0.4 ICPES 84ABD 01 2.8 0.4 ITNA 74RAN 02

2.8 0.6 FAA 74W0L 01 2.82 7 FAA 80CHA 01 2.9 RTNA 79TJI 01 2.9 RTNA 78G0E 01 2.9 0.3 D RTNA 74G0E 01 2.9 0.3 RTNA 73G0E 01 2.9 0.4 EXRF 80DYC 01 2.9 0.4 SSMS 84V0S 01 2.92 0.28 ITNA 85MAD 01 3.0 ICPES 81 GOO 01 3.0 0.2 AA 76GAL 01 3.0 0.3 SSMS 84V0S 01 3.0 1 ITNA 77ZIK 01 3.1 6 ICPMS 83D0U 01 3.14 0.4 ITNA 81HAB 01 3.2 0.3 SSMS 84V0S 01 3.2 0.3 ITNA 81KUL 01 3.2 0.3 RTNA 76GAL 01 3.3 ITNA 80CRE 01 3.4 6 ICPMS 83D0U 01 3.4 0.5 SSMS 84V0S 01 3.4 0.5 ITNA 76GAL 01 3.67 0.01 ICPES 79HER 01 3.9 15 XRF 78STA 02

5.5 2.2 PAA 80YAM 01 5.81 0.84 ITNA 79REN 03

Cone Uncer Com Method Reference

Cs (ng/g)

20 NAA 77LAU 01 24 3 9 ITNA 78LAU 02

28 5 ITNA 78LAU 02

28 5 ITNA 81ICUL 01 29 2 ITNA 74RAN 02

32 8 ITNA 84TU 01 36 6 ITNA 84GLA 11 37 2 ITNA 84GLA 02

37.4 11 NAA 76GUZ 01 38 7 6 ITNA 74BEC 01 40 11 SSMS 85V0S 01 40 9 W 81N0N 01 40 10 ITNA 79SAT 01 42 ITNA 80CRE 01 42 1 lENA 81K0S 01 44 2 ITNA 85GAU 04

48 4 ITNA 81K0S 01 49 9 ITNA 85MAD 01 50 6 ITNA 83AHM 01 50 10 ITNA 85UAH 01 80 10 RTNA 77MEL 01 50 60 ITNA 79REN 03

!00 50 7 RTNA 80GAL 02

(ug/g)

3.6 1 .3 6 ITNA 74H0F 01 8 EXRF 82KEE 01 8.1 2 EXRF 77FL0 01 8.4 0.8 ITNA 78 FUR 01 8.9 1.7 FAA 77FUJ 01 9.4 EXRF 81BIS 01 9.5 ICPES 81 GOO 01 9.6 0.8 XRF 85AVA 01 9.6 1.7 EXRF 73SPA 01 9.7 11 SSMS 85V0S 01 9.76 0.61 9 ITNA 77GAN 03

9.8 0.6 6 NAA 78GAN 01 9.8 0.6 6 NAA 78GAN 01 10 RTNA 72MOR 03

10 0.7 AA 78LIN 01

10 1 XRF 78LIN 01 10 2 CPXRF 77CAM 01 10 2 AA 82HAR 01 10.1 1.2 RTNA 83DAN 01 10.3 AA 76KRI 03

10.3 0.5 FAA 82JEN 02

10.3 0.6 AA 76GAL 01 10.4 2.4 EXRF 75REU 01 10.4 13.3 RD ITNA 79IMA 03

1571-13
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

:onc Uncer Com Method Reference | Cone Uncer Com Method Reference

(uq/q) cont. Cu (uq/q) cont.

10.4 13.3 R ITNA 791 MA 01 1 11 .8 0.4 RTNA 85TIA 01 10.5 1 RTNA 80SLO 01 1 11 .8 0.7 ITNA 79K0B 03

10.6 8 SSMS 01 1

1 11 .9 11 SSMS 85VOS 01 10.7 0.3 11 ICPES R1MIIU o 1 nun 01 1 11 .9 0.6 HPLC 83ICH 01 10.7 0.9 ITNA OJ'nL/ 1 ni 1 11 .9 1.4 FAA 82GR0 01 10.8 6 NAA f CO 1 n ni 1 11.9 1.6 ASV 79BRI 02

10.8 0.8 SSMS OH vUo 1 12

,

AA 73LOO 03

11 AA OHon i 1 12 AA 76FUK 01

11 ICPES O 1 WC 1

1 12 XRF 78CAM 02

11 FAA OOn 1 o 1 12 FAA 73SEG 01

11 AE+AF 701 II 1 ni 11 12 AA 79HIL 01

11 1 AA 77FPY 1 12 CPAA 78MCG 01

11 OES 10 1 12 OES 75 JON 02

11 0.1 ICPES 83SCH 04 1 12 CPXRF 76ZEI 01

11 0.8 7 RTNA 80GAL 02 1 12 AA 81ARA 01

11 1 ICPES 01 11 12 ASV 83H0L 01

11 1 FAA 01 1

1 12 0.2 11 ICPES 82J0N 01

11 1 ICPES 02 1 12 0.3 6 ICPES 85ABD 01

11 1 RTNA 01 1 12 0.4 ICPES 80SCH 08

11 1.5 AA ni 1

t 12 0.4 11 ICPES 82JON 01

11 15 R AA niU I

1 1 12 0.5 AA 73TAL 01

11.1 1 RTNA U 1 1 12 0.8 11 ICPES 82JON 01 11.2 W O 1 nUn 1 12 AA 79MCQ 01 11.2 6 ICPES OTDp A OJDKM n? 1

1 12 ICPES 79MCQ 01 11.2 0.18 AA uUnUC 1 12 AA 77^AN 01 11.2 1 6 POL 7?SIIJ f i n 01 1 12 AA 78RIT 01 11.2 1 .3 ITNA 7L01M 02 1 12 RTNA 73G0E 01

11 .3 16 AA 79AB0 01 1 12 D RTNA 74G0E 01 11.3 ICPMS 85 SCI 01 1 12 1.4 EXRF 77NIE 01

11 .3 1 SSMS 84V0S 01 1 12 2 FAA 77L0R 01 11.3 2.3 XRF 02 1 12 2 RTNA 74CAR 03

11.4 ICPES 7RrAP 01 1 12.1 16 AA 79AB0 01

11 .43 0.2 RTNA 01 1

1 12.1 6 ICPES 83BRA 02

11.5 0.5 RTNA 7^T 1

1

U 1 1 12.1 0.2 ICPES 81KNA 01 11.5 0.6 FAA AAn A n? 1

1 12.1 0.7 SSMS 84V0S 01 11.5 1 POL 7/ MA I ni 1

1 12.1 0.9 ITNA 79SAT 01 11.5 1 EXRF 70f: 1 A ni 1

1 12.1 1.3 PAA 76WIL 01 11.6 FAA f OUMr ni 1

1 12.2 1.1 ICPES 79ABE 01 11.6 0.2 AA 7<tARI 1 ni 1

1 12.3 0.4 ICPES 85LIE 02

11.6 0.4 RTNA 7RRAI ni 1

1 12.3 0.9 RTNA 76MEL 03

11.6 0.4 ICPES A1RI A n? 1 12.3 1.4 W 80SCH 05

11.6 0.4 7 RTNA 80GAL 02 1 12.4 1.4 CPXRF 85CLA 01 11.6 0.6 11 ICPES 81MUN 01 1 12.4 1 .4 11 ASV 84L0C 01 11.7 0.2 11 ICPES 82 J ON 01 1 12.4 1 .6 RTNA 80VAL 01 11.7 0.4 AA 83RAP 01 1 12.4 1.9 RTNA 83SIR 01 11.7 1.7 CPXRF 81 ROB 02 1 12.5 11 AA 79H0E 02

11.8 6 ICPMS 83D0U 01 1 12.5 0.5 11 ASV 84L0C 01 11.8 RTNA 79BYR 01 1 12.5 0.7 FAA 74W0L 01 11.8 0.3 RTNA 78GIL 01 1 12.5 0.8 W 79ST0 01 11.8 0.3 7 RTNA 80GAL 02 1 12.5 1.5 FAA 84R0S 01

1571 -14
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Cu (ug/g) cont.

12.6 6 ICPMS 8300U 01 12.6 0.6 EXRF 73GIA 01 12.6 0.7 ASV 84L0C 01 12.62 0.85 NAA 76GUZ 01 12.7 6 POL 72SIN 01 12.9 6 AA 72SIN 01

13 OES 75J0N 07

13 11 AA 79H0E 02

13 1 AA 77FRY 01

13 ICPES 78DAH 01

13 AA 83ELA 01

13 0.1 EXRF 85COE 02

13 0.47 11 AA 75ISA 01

13 1 35 RTNA 77GLA 01

13 1.7 AA SAKAN 01

13 4.2 CPXRF 80KIR 01 13.1 6 ICPMS 83D0U 01 13.1 0.4 ASV 85ADE 01

13.1 0.6 AA 73TH0 01 13.2 0.5 SSMS 72MAG 01 13.3 0.1 ICPES 79HER 01 13.4 6 ICPES 83BRA 02

13.4 0.5 7 RTNA 84 FAR 02

13.5 0.6 7 RTNA 84FAR 02

13.5 1.5 ITNA 82QUR 01 13.5 1.5 ITNA 79AHM 01 13.6 0.5 7 RTNA 84 FAR 02

13.7 1.3 6 EXRF 79MAT 01 13.8 1.4 XRF 74REU 01 14 OES 75JON 03

14 OES 75J0N 04

14 OES 75J0N 11 14 CPXRF 84KAU 01 14 6 ICPES 85ABD 01 14 0.13 11 AA 75ISA 01 14 1 EXRF 80DYC 01 14 2 ITNA 77ZIK 01

14 4.5 6 ITNA 74H0F 01 14.5 1 FAA 82KRI 01 14.5 4.7 ITNA 77HAM 01

15 OES 75 JON 05

15 OES 75ISA 01 15.5 ITNA 82AKA 01 15.5 SSMS 81VER 02

16 ICPES 84NAD 01 16 OES 75J0N 09

16 OES 75J0N 01 16 1 ICPES 84ABD 01 17 OES 75 JON 06

18 4 ICPES 82AZI 02

I 1571-15

Cone Uncer Com Method Reference

Cu (ug/g> cont.

18^1 CPXRF 75 CAM 01 18.3

1 6.9 XRF 77SMI 04

19 ITNA 78KEL 02

20 OES 75 JON 08

21 1

1

CPAA 77ZIK 01 27 OES 75BOL 02

30 XRF 80SUZ 02

35 EXRF 81 PAR 01

Dy (ng/g)

< 100 L NAA 77LAU 01 JJ oo

Y T U A

1 1 NA 77NAD 02

80 7 RTNA 840DD 01 86 3 RTNA 86TSU 01 110 SSMS 78URE 01

Er (ng/g)

< 100 RTNA 77LAU 02

< 100 D RTNA 82LAU 01 28 3 RTNA 86TSU 01 30 SSMS 78URE 01 31 4 RTNA 840DD 01

Eu (ng/g)

20 ITNA 80CRE 01 20 SSMS 78URE 01 20 2 ITNA 78LAU 02

21 RTNA 77LAU 02

21 D RTNA 82LAU 01

21 1 ITNA 74RAN 02

22 3 ITNA 79K0B 03

22 8 RTNA 80SLO 01 22.6 2.9 ITNA 85MAD 01 23 1 RTNA 83TJI 01 24 4 ITNA 77NAD 02

25 3 ITNA 83AHM 01 26 NAA 77LAU 01 26 1 lENA 81K0S 01 26 5 ITNA 84TU 01 27 3 ITNA 81K0S 01 27 6 ITNA 81KUL 01 28 1 RTNA 86TSU 01 28 6.3 ITNA 77HAM 01 30 10 RTNA 83SIR 01

31 4 6 ITNA 74BEC 01 35 ITNA 85MIS 01

91 5 RTNA 840DD 01 120 20 RTNA 77KUS 01 300 RTNA 72MOR 03
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

<ug/g)

3.12 COLOR 790AB 01 3.6 AA 77TSU 01 3.69 COLOR 790AB 01 3.7 DISE 83ESA 01 3.8 0.32 ISE 79DAB 01 3.88 ISE 79DAB 01

4 0.3 ISE 82GLA 02

4.2 0.4 ISE 84GLA 02

4.4 0.3 ISE 83KNA 01 4.8 1 MS 77STE 02

10 CPAA 80HAN 01

'..(yg/a)..

121 CPXRF 76ZEI 01

121 CPAA 78MCG 01 145 4 11 AA 78GAI 01

151 OES 75J0N 09

174 OES 75J0N 06

183 22 11 ICPES 81MUN 01 190 OES 75J0N 02

190 OES 75J0N 11 205 37 ITNA 81HAB 01 213 6 ICPES 83BRA 02

213 OES 75J0N 03

220 6 11 AA 78GAI 01 225 58 XRF 77SMI 04

229 OES 75 J ON 08

229 22 XRF 78LIN 01 232 OES 75 J ON 04

235 AA 76FUK 01 235 ICPES 78CAP 01 237 13 CHEML 72SEI 01 238 AA 76KRI 03

239 OES 75 ISA 01 240 24 SSMS 84VOS 01 240 330 R AA 75MAN 01 245 35 ICPES 79A3E 01 246 FAA 78CAP 01 250 AA 73L00 03

250 11 SSMS 85V0S 01 250 30 RTNA 7/ PAD Uj

250 42.5 11 AA 75ISA 01 253 ITNA 80SAT 01 254 9 EXRF 80DYC 01 255 5 11 COLOR 82SCH 03

256 1 AA 78LIM 01 256 11 11 ICPES 82J0N 01 258 ICPES 84NAD 01 259 ITNA 78CAP 01

Cone Uneer Com Method Reference

Fe (ug/g) cont.

260 20 ITNA 78GIL 01 260 20 SSMS 84V0S 01 261 SSMS 81VER 02

261 39.1 11 AA 75ISA 01 262 5 ICPES 79HER 01 265 54 RTNA 83SIR 01 266 21 CPXRF 85CLA 01 267 ICPES 780AH 01 267 2.9 CPXRF 81 ROB 02

267 6 ICPES 79MCQ 02

270 OES 75BOL 02

270 11 SSMS 85VOS 01 270 ITNA 80CRE 01 270 50 35 ITNA 81GLA 03

271 6 11 COLOR 82SCH 03

271 7 RTNA 77MEL 01 272 16 AA 73TH0 01 273 6 ICPES 79MCQ 01 274 19 EXRF 79GIA 01 276 OES 75 JON 05

276 8 EXRF 73GIA 01 277 4 ICPES 85LIE 02

278 1

1

AA 79MCQ 01 279 79 RTNA 77KUS 01

280 NAA 77LAU 01 280 AA 83ELA 01 280 10 ITNA 78LAU 02

280 26 ITNA 77HAM 01 280 37 ICPES 84ABD 01 282 COLOR 72SEI 01 282 21 14NAA 81UIL 02

282.3 9.4 11 ASV 84L0C 01 283 3 11 ICPES 82J0N 01 283 23 ITNA 75RIC 01 284 AA 82WIL 04

285 5 RTNA 80SLO 01 285 5 ITNA 790AS 01 285 9 11 COLOR 82SCH 03

287 AA 79HIL 01 288 20 ICPES 80SCH 05

288 20 D ICPES 80SCH 08

288.1 7.2 11 ASV 84L0C 01 290 FAA 73SEG 01 290 RTNA 72MOR 03

290 2 AA 84SAT 02

290 6 11 ICPES 82J0N 01 290 12 PAA 74CHA 01 290 15 7 RTNA 80GAL 02

290 25 6 NAA 78GAN 01 290 30 CPAA 77ZIK 01

1571 -16
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Fe (ug/g) cont.

290 30 ITNA 81iaJL 01 290 30 ITNA 81K0S 01 290 35 lENA 81K0S 01 290 58 SSMS 84V0S 01

291 19 EXRF 85C0E 02

291 24 W 81N0N 01 292 6 ICPES 83BRA 02

292 10 AA 83RAP 01 293 6 ICPES 85ABD 01 293 11 AA 79H0E 02

293 14 EXRF 77FL0 01 293 18 EXRF 79ICUE 01 294 OES 75 JON 10

295 11 AA 79H0E 02

295 14 11 ICPES 81 HUN 01 295.7 20.1 ITNA 82C0R 01 296 ICPES 83KEI 01 296 8 ITNA 82QUR 01 296 8 ITNA 79AHM 01 296 12 ICPES 81BLA 02

297 AA 81ARA 01 297 6 ITNA 85WAH 01 297 10 FAA 82JEN 02

298 8 ITNA 83AHM 01 298 30 ICPES 85LYO 01 298.9 8.1 ASV 84L0C 01 299 1 ITNA 79K0B 03

300 NAA 74BEL 01 300 EXRF 81BIS 01 300 14 COLOR 82M0R 01 300 17 11 ICPES 82J0N 01 300 23 ITNA 84TU 01 300 40 ITNA 76KUC 01 300 45 ITNA 74RAN 02

300 50 14NAA 80FAA 01 301 2.5 EXRF 73SPA 01 301 8 ICPES 84 SOB 01 303 32 ITNA 79SAT 01 304 30 ITNA 78FUR 01 306 ITNA 79KUC 01 306 6 EXRF 77NIE 01 309 17 ITNA 85MAD 01 310 ITNA 85MIS 01 310 XRF 78CAM 02

310 31 SSMS 84V0S 0: 310 54 FAA 77FUJ 01 311.1 10.4 NAA 76GUZ 01 312 11 POL 74MAI 01 312 11.4 POL 72MAI 01 312 11.4 POL 77MAI 01

Cone Uncer Com Method Reference

Fe (ug/g) cont.

313

313

314 40

315 25

315 25

316

316

317 25

318.4 26.9

319 32

320 25

325

326

326 30

331.5 118

332 84

335

335 14

335 40

338 16

340 28

343 6

348 10

367

370 45

422

450 70

500

884

Ga (ng/g)

<

<

78

86

89.3

100

Gd (ng/g)

1.64

12

81 100

100

100

111

160

500

25

3.6

10

0.24

1

10

6

6

38

ICPES

ICPES EXRF RTNA

RTNA

OES

CPXRF

ICPES

ITNA XRF NAA

ICPES EXRF

ITNA PAA

PAA

EXRF

EXRF

ITNA EXRF

AA

SSMS

14NAA

OES

CPXRF

CPXRF

ITNA AE+AF

EXRF

lENA EXRF NAA

RTNA

RTNA

RTNA

ITNA RTNA

RTNA

RTNA

RTNA

SSMS

RTNA

81WEI 01 83BRA 02

75REU 01 73G0E 01 74G0E 01 75J0N 01 84KAU 01 81KNA 01 74BEC 01 74REU 01 78GAN 01 81G0O 01 82KEE 01 77ZIK 01 76KAT 04

76KAT 02

810HT 01 79MAT 01 S4NDI 01 79MAT 01 82HAR 01 72MAG 01 81WIL 01 75 JON 07

77CAM 01 75CAM 01 79REN 03

79ULL 01

81 PAR 01

78WAN 01 79GIA 01 76GUZ 01 72MOR 03

80STU 01 77KUS 01

77NAD 02

840DD 01 86TSU 01 82LAU 01 77LAU 02

78URE 01 83TJI 01

1571-17
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Ge (np/ci) Hg (ng/g> cont •

< 400 L EXRF f yuiA ni 1 Ul 1 146 12 RTNA 82LO 01 150 H ICPES OcHAM ni 1 U 1

1 U6 17 NAA 76GUZ 01 148 10 7 RTNA 72HEI 01

H (%) 148 16 CVAA 82SUL 01 150 AA 83ELA 01 5.54 0.08 TCGS f VrAl 1 150 CVAA 81NAR 01 5.6 0.1 TCGS f VANU m 1 150 5 FAA 72LYO 01 5.91 0.3 CB O^uLA no 1 150 5.1 AA 84ST0 01 6.05 0.07 CB ououn n? 1 150 10 RTNA 838RA 01 6.1 0.1 35 TCGS f TuLA nL 1 150 10 FAA 83YAN 01 150 17 CVAA 74FIT 01 H20- (%) 150 18 ITNA 82LIN 01 150 40 RTNA 83SIR 01 11.4 D GRAV ODNAK fVZ 1 151 7 RTNA 84DRA 01 11.4 GRAV Q/.UhD OhNAK ni 1 U E

1 152 5 2 CVAA 79KNE 01 152 6 RTNA 76MEL 01

Hf (ng/q) 152 6 CVAA 80TON 01 153 8 CVAA 80KOR 01

13 RTMA OUoLU niU !1

J 153 14 FAA 75KOI 01 23 NAA 771 All 01 1 154 5 RTNA 740RV 01 27 ITNA ni 1 154 13 FAA 7600G 01 28 2 ITNA niU 1

1 1 154 13 CVAA 7800G 01

31 4 ITNA 7AI Al 1 CO 1 154 16 5 RTNA 80GRE 01 34 ITNA Ojri i o (11 U 1

1 1 154 20 7 RTNA 80GAL 02

37 5 ITNA 7/. D A U f hKAN 154 20 RTNA 78GIL 01 46 12 ITNA ODrlAU ni i 154 28 FAA 74CHU 03

155 3 RTNA 72RAI 01

Hg <ng/c|) 155 5.6 RTNA 72ROO 02

155 6 RTNA 72ROO 01 110 30 RTNA ( f dAN n'? 1 155 6 11 CVAA 77TAG 01 120 10 D RTNA r HuUC ni 1

1 155 13 5 RTNA 80GRE 01

120 10 RTNA 77fine ni 1

1 155 15 RTNA 73TJI 01 120 10 CVAA AARAD np 1

1 157 1 AF 81EBD 01 120 20 RTNA OUoLU ni 1

1 157 20 CVAA 82GLA 02

122 11 CVAA f ynuc n? 1 158 ITNA 80SAT 01 122 28 ITNA A/. TI II OH 1 U

ni 1 U 1

1 158 CVAA 84LAU 01

125 AA 7/. DIP ni 1 U 1

1 158 RTNA 74RIC 01

125 IDMS 7/. D T

f hK 1

L

ni 1 U 1

1 158 5 RTNA 72LY0 01 130 CVAA oUNAU ni i u 1

1 158 10 FAA 77GLA 03

130 CVAA Q7U A D nc 1 \}j

1 158 16 RTNA 82LIN 01 138 2 11 CVAA 77T AT A / 1 Ab U 1 1 159 21 CVAA 78MAT 01 140 ICPES Q/ U A D ni 1 U 1

1 160 RTNA 790ES 01 140 10 NAA 77JER 01 i 160 6 CVAA 72RAI 01 140 10 PAA 74CHA 01 I 160 10 ITNA 83AHM 01 140 10 ITNA 74FRI 01 1 160 12 FAA 74SIE 02

140 20 IDMS 72RAI 01 1 160 12 FAA 72R00 01

141 9 SSMS 74ALV 01 1 160 20 FAA 79ST0 01 142 27 CVAA 82DOO 01 1 160 20 CVAA 82CHA 01 146 UU 74FEL 01 1 160 20 FAA 82JEN 02

146 6 FAE 76CAV 01 1 160 30 RTNA 80VAL 01

1571-18
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Hg (ng/g) cont.

160 40 6 POT 82JAG 01 160 70 ITNA 81KUL 01

161 13 RTNA 75LIT 01

162 10 7 RTNA 72HEI 01

163 6 17 CVAA 77TAG 01

163 12 RTNA 82GRI 01

165 5 35 CVAA 81GLA 04

165 25 ITNA 85WAH 01 167 ITNA 74RIC 01 168 10 ITNA 79AHM 01 168 10 ITNA 82QUR 01 170 12 CVAA 82LIN 01 175 5 17 CVAA 77TAG 01 180 10 ITNA 78FUR 01

180 20 ITNA 74RAN 02

180 30 RTNA 77MEL 01 180 40 6 POT 82JAG 01 190 ITNA 75RIC 01 190 10 NAA 78GAN 01 190 30 6 ITNA 74BEC 01 190 40 CVAA 77AND 01 on 1 1 NA Ul 200 30 PAA 80SEG 01 200 30 ITNA 81HAB 01 200 80 ITNA 74GUI 01 203 11 17 CVAA 77TAG 01 210 50 ITNA 77ZIK 01

I ( CVAA 1 / TAG Ul

305 70 ITNA 75LIT 01

Ho (ng/q)

11 1 RTNA 86TSU 01 13 D RTNA 82LAU 01

13 RTNA 77LAU 02

20 SSMS 78URE 01 22 2 RTNA 840DD 01

I (ng/g)

100 50 PAA 78HIS 01 100 50 PAA 77WIL 01 160 20 lENA 82SAT 01 167 10 RTNA 77ROO 01 173.2 4.4 RTNA 80GVA 01 183 6 17 NAA 79HEC 01 188 26 NAA 79BRA 01 190 70 lENA 84 FAR 01 192 10 RTNA 83TAK 02

200 70 RTNA 77STE 02

220 17 NAA 79HEC 01

Cone

1-129 (fCi/g)

0.006

1.23

1.6

1.8

2

Ir (ng/g)

15

Uncer Com Method Reference

K (%)

1.05

1.05

1.11

1.19

1.2

1.229

1.25

1.26

1.28

1.3

1.33

1.35

1.35

1.36

1.37

1.37

1.37

1.37

1.374

1.38

1.38

1.39

1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.4

1.41

1.41

1.41

1.41

1.42

0.0028

0.11

0.1

0.8

0.2

1.406 RD

1.41 R

0.018

0.2

0.01

0.01 11

0.06

0.06

0.14

0.04

0.01 11 0.06

0.098 6

0.2 35

0.03

0.09

RTNA

RTNA

RTNA

RTNA

ITNA

RTNA

ITNA ITMA OES

OES

ICPES

CPXRF

ICPES

OES

OES

14NAA

ICPES

AA

OES

AA

ITNA

ITNA

ITNA

lENA

AA

OES

ITNA CPAA

ITNA ICPES

ICPES

OES

AA

ITNA NAA

ITNA OES

AATCGS

CPXRF

EXRF

79BRA 01

74RAV 01 78K0B 01 77KUS 01 85WAH 01

74CAR 03

79 I MA 03

79IMA 01 75J0N 05

75J0N 09

83BRA 02

81 ROB 02

83BRA 02

75JON 03

75 JON 11 77SEG 01 84ABD 01 78SZY 01 75 JON 04

78GAI 01 80CRE 01 74RAN 02

84NDI 01 79J0N 01 78SZY 01 75ISA 01 75RIC 01 80HAN 01 82AKA 01 84NAD 01 85ABD 01 75J0N 02

78GAI 01 78LAU 02

78GAN 01 81GLA 04

75J0N 07

77BRU 01 79AND 01 85CLA 01 81BIS 01

1571-19
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

K (%) cont.

1 .42 ITNA 78CAP 01

1 .42 0.04 ITNA 81K0S 01

1 .42 0.09 ITNA 76KUC 01

1 .42 0.23 ITNA 84TU 01

1 .43 6 ICPES 83BRA 02

1.43 0.04 EXRF 79KUE 01 1.43 0.06 FE 78K0R 01 1.43 0.07 11 ICPES 82J0N 01 1.4375 0.0794 NAA 76GUZ 01 1.44 0.0004 11 AA 75ISA 01

1 .44 0.04 RTNA 76MEL 03

1.445 0.11 PAA 76KAT 04

1 .45 ITNA 79KUC 01

1 .45 ICPES 79C00 01

1 .45 OES 75J0N 01

1 .45 0.0003 11 AA 75ISA 01

1 .45 0.02 AA 82HAR 01

1 .45 0.03 11 ICPES 81MUN 01

1 .45 0.08 PAA 76KAT 02

1 .46 0.02 ITNA 85WAH 01

1 .46 0.07 ITNA 83AHM 01

1 .46 0.07 ITNA 79AHM 01

1 .46 0.11 EXRF 82DAK 01

1 .46 0.14 14NAA 80FAA 01

1 .46 0.2 14NAA 81WIL 02

1 .47 NAA 77LAU 01

1 .47 0.02 1

ICPES 82 J ON A 4 01

1 .47 0.07 1

ICPES 82 J ON A 4 01

1 .47 A 4 0.1 ITNA 79REN A703

1 .47 0.12 ITNA 79K0B AT03

t /a

1 .48 AA 79HIL 01

1 .48 ICPES 81 WEI 01

1 .49 1 lENA 79KUC 01

1 .49 0.03 ITNA 78GIL 01

1 .49 0.04 TOGS 79FAI 01

1 .49 0.194 ITNA 77HAM 01

1 .496 0.043 ITNA 78FUR 01 1.5 ITNA 78KEL 02

1.5 RTNA 72M0R 03

1.5 ITNA 76BAT 01 1.5 0.05 11 ICPES 81MUN 01 1.5 0.08 W 81N0N 01 1.51 CPXRF 84KAU 01 1.51 XRF 78CAM 02

1.51 0.06 CPXRF 80ICIR 01 1.51 0.06 EXRF 77NIE 01 1.54 OES 75J0M 08

1.54 0.03 ITNA 80SLO 01 1.55 0.8 XRF 78STA 02

1.56 0.05 11 ICPES 82J0N 01

Cone Uncer Com Method Reference

K (%) cont.

1 .57 0.08 EXRF 75REU 01 1.57 0.25 14NAA 81UIL 01 1.58 0.08 6 NAA 78GAN 01 1.59 OES 75J0N 10

1.62 OES 75 JON 06

1 .65 ITNA 84TU 03

1 .66 0.8 6 EXRF 79MAT 01 1.67 0.03 6 ICPES 85ABD 01

1 .7 0.07 ICPES 79HER 01 1.74 0.04 EXRF 80DYC 01 1.81 0.08 6 EXRF 79MAT 01 3.89 EXRF 81 PAR 01

:uq/q)

0.7 0.1 ITNA 77ZIK 01 0.8 0.05 RTNA 80SLO 01 0.88 0.07 RTNA 83SIR 01 0.89 1 .25 R ITNA 79 1 MA 01 0.89 1.25 RD ITNA 79 1 MA 03

0.95 ITNA 79KUC 01 0.98 ITNA 80CRE 01 0.99 0.08 6 ITNA 74BEC 01 1.0 RTNA 77LAU 02

1.0 NAA 77LAU 01 1.0 NAA 74BEL 01 1.0 D RTNA 82LAU 01

1.1 4 41SSMS 85VOS A 4 01

1 .

A H 0.1 ITNA 78LAU 02

1 . 145 0.058 RTNA 86TSU A 4 01

1 . 15 0.1 lENA 81K0S A 4 01 1.17 0.15 ITNA 84TU 01

1 .18 0.09 ITNA 81K0S 01

1 .2 RTNA 72M0R 03

1.2 ITNA 78CAP 01 1.2 SSMS 78URE 01 1.2 0.1 RTNA 76MEL 03

1.2 0.1 ITNA 81KUL 01 1.2 0.165 ITNA 77HAM 01 1.2 0.3 ITNA 83AHM 01 1.209 0.039 RTNA 83TJI 01 1.22 0.02 W 81N0N 01 1.23 0.02 NM 85KAT 02

1.23 0.05 ITNA 84NDI 01 1.24 0.08 ITNA 79REN 03

1.24 0.18 ITNA 85MAD 01 1.26 0„2 ITNA 85ICAT 02

1.27 ITNA 85MIS 01 1.27 0.33 ITNA 840DD 01 1.3 0.1 ITNA 74RAN 02

1571 -20
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

La (ug/g) cont.

1.4 NM 83KAT 01 1.44 0.2 RTNA 8400D 01 1.7 0.6 RTNA 77iajs 01 1.96 0.02 ITNA 77NAD 02

Li (nq/q)

< 900 L CPAA 81SAS 01 500 80 AA 84GLA 11 510 660 R AA 75MAN 01 570 70 AA 84GLA 02

770 30 ITNA 77HEY 01 800 200 CPAA 80HAN 01 830 AA 85GAU 04

13700 1500 NT 74CAR 02

14000 1000 RTNA 85YAN 01

Lu (ng/g)

0.61 0.09 ITNA 77NAD 02

0.9 0.1 ITNA 81K0S 01 2.9 0.2 RTNA 83TJI 01 2.9 0.8 RTNA 86TSU 01 3.3 D RTNA 82LAU 01 3.3 RTNA 77LAU 02

4 2 RTNA 83SIR 01 6 RTNA 80SLO 01 8.4 0.7 RTNA 840DD 01 8.5 1.3 ITNA 83AHM 01 10 SSMS 78URE 01

Mg (ug/g)

4000 6250 R ITNA 79 1 MA 01 4000 6250 RD ITNA 79 1 MA 03

4900 ICPES 78CAP 01 4900 6 ICPES 833RA 02

4915 ICPES 81 GOO 01 5140 190 W 81N0N 01 5300 FAA 78CAP 01 5400 NAA 77LAU 01 5400 100 ICPES 85LIE 02

5500 AA 80URE 01 5500 6 ICPES 85ABD 01 5500 300 ICPES 79ABE 01 5500 300 lENA 79J0N 01 5600 AA 77BRU 01 5600 ITNA 84TU 03

5600 6 ICPES 83BRA 02

5600 100 AA 79MCQ 01

Cone Uncer Com Method Reference

Mg (ug/g) cont.

5640 420 AA 86GAU 01 5700 OES 75 JON 05

5700 60 ICPES 79MCQ 02

5700 80 ICPES 79MCQ 01 5800 100 11 AA 78GAI 01 5800 300 ICPES 85LY0 01 5800 730 ITNA 77HAM 01 5900 ICPES 84NAD 01 5900 1 11 AA 75ISA 01 5900 300 AA 84GLA 11 5922 172 11 ICPES 81MUN 01 5960 CPXRF S4iCAU 01 5980 70 11 ICPES 82 J ON 01 6000 RTNA 72M0R 03

6000 OES 75JON 09

6000 OES 75 JON 07

6000 2 11 AA 75ISA 01 6000 100 11 AA 78GAI 01 6000 200 11 ICPES 82 J ON 01 6000 500 14NAA 80 FAA 01 6000 500 ITNA 78LAU 02

6000 500 CPXRF 80KIR 01 6100 OES 75 J ON 10

6100 AA 79HIL 01 6100 ICPES 83KEI A401 6100 100 PAA 74CHA A401 6100 "iA A 200 PAA 78HIS A 4 01

£. A AA 6100 AAA 200 1

1

ICPES 82 J ON 01

£. >l AA 6100 400 ITNA 80SLO 01

Z 4 AA 6100 4 4 AA

1 100 14NAA 81WIL A' 1 0^

Z 4 Cf A 6150 ICPES 780AH 01 6150 70 PAA 76KAT 02

6150 100 PAA 76KAT 04

6173.8 179 NAA 76GUZ 01 6174 173 ITNA 75PIE 01 6200 OES 75JON 02

6200 OES 75JOM 08

6200 6 ICPES 83BRA 02

6200 100 1

1

ICPES 82JON 01 6200 200 6 ICPES 85ABD 01 6200 400 ICPES 84ABD 01 6221 153 11 ICPES 81MUN 01 6258 315 ITNA 77ZIK 01 6300 ITNA 78CAP 01 6300 130 ITNA 78FUR 01 6300 700 TCGS 79FAI 01 6400 OES 75 ISA 01 6400 ICPES 81 WE I 01 6500 OES 75JON 06

6500 100 COLOR 74SLE 01

1571 21
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Mg (ug/g) cont

.

1 Mn (ug/g) cont

.

ODUU 1 (\(\

\ uu AA 82HAR 01 1 Q/.U*fr UA A NAA 771 All ni

I f LAU Ul

1 1 NA 79K0B 03 1

fl/. OH 11 1

1 LrtS 00 lf\U Ai B^JON U1 ooUU 75J0N 11 1 0/OH H

T TU A

1 1 NA 701 All AO fBLAU Ux

oooU A C Ar 85DAV 01 1 OR T TU A

I 1 NA 70/* An Ai

CPAA 80HAN 01 1 QCo!> i. 1 11 1 ICPcS BxJON 01 6700 i AA 100 ICPES 79HER 01 1 o!>

/ EXRF 0AAV A 4

6800 OES 75J0N 03 1 ocOD 1 A10 z EXRF fyfAR] 01 6800 OES 75 JON 04 1 83.6 2.8 z6 ITNA 74H0F 01 6800 1 AAA 1 UUU 1 / kl A A 77SEG 01 1 00 A A AA 7X CI 1^ A

1

f6FUK 01 7000 ITNA 76BAT 01 1 oz86 ASV OAoiin All 80CHR 01 7030 1 7A 170 14NAA 81WIL 01 1 86 RTNA fZnOR 03

"7-1 / 100 OES 75J0N 01 1 Oil 00 T Tkl A ITNA Q/ nt A no 8hGLA 0^

T Tkl A

I TNA 75RIC 01 1 ox00 z0 1 Lrbo o3LnA Ul ox00 1 I CPcS f ynCQ uc. Mn (ug/g) 1 ox00 1 Urto fyriLu Ul

1 ox00 £. 1 Lrto o^oLn Uh

/ / 0

r Tiki A

1 1 NA 74HOF 01 1 ox00 1 1 T PDCC 00 inu rti OC.JUN U

1

To tXKr 77FL0 01 1 ox ^ /. 0 H .T rvD c tAKr rVulA U

1

CO OcS 75J0N 07 i ox 0 00.0 X 7 i Lrto OCl A

4

oDLTU Ul 5h 1

1

bans 84V0S 01 j ox It 00.0 1

1

1 1 i Lrto OinUN Ul

K

T Ti) A ITNA 79 1 MA 01 1 07Of 1

1

1 1 CCMC oono oDVUo U

1

yu op* RD T TLI AI TNA 79 1 MA 03 1 Q701 1

1

1 1 A A AA f VnUt Ut

a.i. XRF 77SMI 04 j Q701 C A A rAA rooku Ul

71 .8 6 ICPES 83BRA 02 j 87.

1

i X

1 .6 RTNA r^3HET Ul

72 OES 75 JON 06 1 OT 1

Of .0 0 0 B.B ICPtS qoa^t ai o^AZI Ul

72 1 1

1

AA 78GAI 01 I Of .8 c 0 D .y

DTLI A R f NA 7/ D A\; AI /^hRAV Ul

73.!) ITNA 82AKA 01 1 0000 Uto 7c mu AO

76 1 A10 ICPES 82AZI 02 1 0000 uto 7c inu A/. fDJUN Uh

-7-7 f / SSMS 81VER 02 1 00 i

1 AAA A ft/. OhoACAT AO 1 \JC 70 D Tkl A K 1 NA 76MEL 03 1 Ofl 5o c AAA A OchAK OOUAD AIU

1

oU A A AA 73L0O 03 1 0000 7 K 1 NA OHtMK Ut

on ICPES 78CAP 01 j OR00 XJ

7 DTU A K 1 NA OHrAK U^ ou on c 75 J ON 11 j fiO 00 fH 1 Lrto ODLlt Uc on OES 75 ISA 01 1 QO00 A A H.H 1 1

1 1 A A AA 7c T CA AI r D 1 oA U 1 OA80 3 XRF 78LIN 01 1 QO 0 00. <: 7 / J.H DA A rAA 7/ ru A AI fHLHA Ul 80.6 2.9 CPXRF 81 ROB 02 1 00 X 80.6 C.d cXKr A T A A

1

r3GIA Ul 80.7 3.3 ITNA 81HAB 01 1 00 0 08.0 1 i

1

1

A A AA 70lJrtC AO f ynOc Ut

0 -f 81 4 RTNA 77KUS 01 1 89 A X 0.6 ICPES 70UCB AI fyntR Ul

81 .3 FAA 78CAP 01 1 0089 4

1

1

1

I CPcS 00 lAkl A 4 o^JON Ul

81 -9 6 ICPES 83BRA 02 1 00By 0 XT 1

1

A A AA TCfCA AI fDloA Ul

1

1

SSMS 85VOS 01 1 DOay 0

r\V 1 Lrto QACPU Aft oUoLH Uo

0*5 EXRF 82KEE 01 1 QOBy •rJ vv OACPU AC OUoLH \jj 0^ 3 lENA 79J0N 01 1 00By AH

T TU A

i 1 NA 7/ DAU AO / hKAN XJc.

/ 0 H . C

A A AA 78LIN 01 1 so AH

A A 70Mm n 1

82 7 EXRF 79KUE 01 1 89 4.4 ITNA 79K0B 03

82 99 R AA 75MAN 01 j 89 5 ITNA 78GIL 01 82.7 ICPES 84NAD 01 1 89 5 FAA 84R0S 01 82.9 5.1 RTNA 83DAN 01 1 89 7 EXRF 85COE 02

83.3 ICPES 780AH 01 1 89.4 1.4 11 ASV 84L0C 01 83.4 FAA 77SHE 02 1 89.9 ITNA 76BAT 01

1571-22
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Mn (ug/g) cont.

90 ITNA 80CRE 01 90 6 ICPES 83BRA 02

90 0.9 11 AA 78GAI 01 90 1 ITNA 80SLO 01 90 3 ICPES 79ABE 01 90 4 7 RTNA 84FAR 02

90 6 ITNA 76KUC 01 90 7 ITNA 77HAM 01 90 12 CPXRF 77CAM 01 90 16 SSMS 84V0S 01 90.9 4.7 ASV 84L0C 01

91 EXRF 81BIS 01

91 0.8 11 ASV 84L0C 01

91 2 ITNA 85WAH 01

91 2 6 NAA 78GAN 01

91 4 FAA 79WES 01

91 4 ICPES 84ABD 01 91.1 10.9 ITNA 85MAD 01 91.1 18 EXRF 75REU 01 91.5 AA 83 FAG 01 91.6 1.08 NAA 76GUZ 01 92 AA 76<RI 03

92 6 ICPES 83CHA 01 92 1 D DCPES 81REE 01 92 1 DCPES 79REE 01 92 3 ITNA 78 FUR 01 92 3 ITNA 75RIC 01 92 3 AA 83RAP 01 92 4 35 ITNA 81GLA 04

92 17 SSMS 84V0S 01 92.4 0.8 ICPES 81KNA 01 92.8 4 ITNA 83AHM 01 93 AA 83ELA 01 93 ITNA 80SAT 01 93 XRF 78CAM 02

93 OES 75 JON 05

93 6 EXRF 77NIE 01 93 8 XRF 78STA 02

93.8 17.2 PAA 80YAM 01 94 3.5 6 NAA 78GAN 01 94.5 5 PAA 76KAT 04

94.8 4 ITNA 79AHM 01 94.8 4 ITNA 82QUR 01 95 6 ICPES 85ABD 01 95 AE+AF 79ULL 01 95 4 PAA 76KAT 02

95 7.3 CPXRF 80KIR 01 95 12 ITNA 79SAT 01 95.4 2.1 ITNA 76GAL 01 95.7 2 11 ICPES 81MUN 01

1571-23

Cone Uneer Com Method Reference

Mn (ug/g) cont.

96 ICPES 81WEI 01 96 ICPES 81 GOG 01 96 OES 75 JON 03

96 5 PAA 78HIS 01 96.2 4.8 AA 76GAL 01 96.8 3.6 AA 73TH0 01 97 OES 75J0N 10

97 CPXRF 84KAU 01 97 10 ITNA 77ZIK 01 97.4 CPXRF 75CAM 01 98 XRF 80SUZ 02

98 20 TCGS 79FAI 01 98.9 11 CPXRF 85CLA 01 99 12 SSMS 84V0S 01 100 ITNA 78KEL 02

101 OES 75 JON 01

101 5 ICPES 84S0B 01

101 10 XRF 74REU 01 103 5 W 81N0N 01 104 9 ITNA 84NDI 01 106 3 6 ICPES 85ABD 01 107 ITNA 84TU 03

107 3 SSMS 72MAG 01 110 ITNA 79REN 03

110 9 6 - EXRF 79MAT 01

131 OES 75J0N 08

144 OES 75 J ON 09

242 EXRF 81 PAR 01

D (ng/g)

110 80 11 ICPES 82J0N 01 200 11 SSMS 85VOS 01 200 FAA 79BEN 01 200 100 11 ICPES 82J0N 01 200 100 11 ICPES 82J0N 01 200 200 11 ICPES 82JON 01 230 20 COLOR 83MAT 02

240 20 RTNA 78NAD 01 240 21 RTNA 82HAD 01 250 1 lENA 79KUC 01 260 20 FAA 84G0H 01 270 9 RTNA 85TIA 01 280 20 ICPES 82LY0 01 280 30 RTNA 83DAN 01 300 30 D RTNA 74G0E 01 300 30 RTNA 73G0E 01 300 60 RTNA 77DIK 01 320 1 lENA 79KUC 01 320 60 RTNA 80SLO 01
TABLE 1571-2: INDIVIDUAL DATA FOR HBS SRH 1571 (cont.)

Cone Uncer Com Method Reference

Ho (ng/g) cont.

320 80 RTNA 84M0K 02

327 70 NAA 76GUZ 01 390 40 FAA 81NEU 01 Ann K 1 Nn U 1 400 100 PAA 80SEG 01 410 83B0U 01 410 AA 8380U 01

2260 210 PAA 74CHA 01

2300 OES 75J0N 10

3300 OES 75J0N 11 4000 2000 CPAA 77ZIK 01 4600 OES 75J0N 03

6200 OES 75J0N 01 10500 OES 75J0N 07

15200 OES 75J0N 02

N (%)

2.59 0.11 CB 82GLA 02

2.61 0.05 14KAA 80 FAA 01 2.62 0.03 CB 80SCH 02

2.7 0.01 11 TITR 82LIA 01 2.7 0.09 13 NT 74CAR 01 2.7 0.09 TCGS 79FAI 01 2,7 0.4 35 TCGS 79GLA 04

2.7 0.4 14NAA 77SEG 01 2.71 0.01 TITR 80GIN 01 2.72 11 TITR 82LIA 01 2.74 0.01 11 TITR 82LIA 01 2.74 0.01 COLOR 80GIN 01 2.74 0.02 11 TITR 82LIA 01 2.75 0.03 11 TITR 82LIA 01 2.755 0.038 GRAV 74CAR 01 2.76 0.09 13 NT 74CAR 01 2.81 0.15 TCGS 79AND 01

N-15 (atom %)

0.367 0.002 MS 73CAR 01

Cone Uncer Com Method Reference

Na (ug/g)

40 OES 75 JON 03

45.8 6 11 ICPES 81MUN 01 50.5 1 11 ICPES 81MUN 01 66 6 ICPES 85LIE 02

74 OES 75J0N 06

75 NAA 77LAU 01 76 NAA 74BEL 01 76 34 6 ICPES 85ABD 01 77 RTNA 72M0R 03

77 4 RTNA 76MEL 03

77 6 ITNA 80SLO 01 78 3 ITNA 74RAN 02

78 5 ITNA 76KUC 01 79.2 1.8 ITNA 84NDI 01 79.3 5 PAA 74CHA 01 80 ITNA 78LAU 02

80 ITNA 84TU 03

80 2 FE 81MI2 01 80 3 ITNA 85WAH 01 80.6 1.3 FE 78K0R 01

81 ICPES 81 GOO 01

81 ITNA 79KUC 01

81 17 ITNA 78FUR 01 81.5 3 ITNA 79AHM 01 81.6 3 ITNA 83AHM 01 81.8 1.83 NAA 76GUZ 01 82 1 lENA 79KUC 01 83 5 ITNA 75RIC 01 83 8.5 ITNA 77HAM 01 84 4 ITNA 78GIL 01 84.4 ITNA 76BAT 01 86 1 W 81N0N 01 86 5 ITNA 77ZIK 01 87 CPAA 80HAN 01 87 11 PAA 76KAT 02

87 16 PAA 76KAT 04

88 6.8 ITNA 79K0B 03

88 142 R ITNA 79 1 HA 01 88 142 RD ITNA 79 1 MA 03

89 17 AA 82HAR 01 90 8 ITNA 81K0S 01 92 ITNA 80CRE 01 92 35 ITNA 81GLA 04

93 14 ICPES 84ABD 01 99.8 6.7 ITNA 85HAD 01

100 OES 75 JON 01

100 OES 75 JON 05

101 6 ICPES 85ABD 01

103.5 ITNA 82AKA 01

110 35 ITNA 81GLA 03

1571-24
TABLE 1571-2: INDIVIDUAL DATA FOR MBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Na (ug/g) cont

1

1 Ni (uq/g) cont.

114 2 NAA 78GAN

1 01 1 1.2 0.4 FAA 82GR0 01 120 40 ITNA 79REN 03 1 1.2 0.5 EXRF 79GIA 01 123 ICPES 84NAD 01 1 1.2 1 EXRF 77NIE 01 130 11 SSMS 85VOS 01 1 1.2 1 EXRF 85C0E 02

140 12 ICPES 79A8E 01 j 1.24 0.07 11 ICPES 82J0M 01 150 OES 75J0N 04 1 1.264 0.052 FAA 846RE 01 154 OES 75 JON 09 1 1.27 0.08 11 ICPES 82JON 01 155 ITMA 78CAP 01 1 1.27 0.08 PAA 74CHA 01 162 1 AA 78SZY 01 1 1.28 0.16 NAA 76GUZ 01 170 30 lENA 79J0N 01 1 1.3 AA 73L00 03

200 AA 77BRU 01 1 1.3 0.07 VOLT 81PIH 01 206 21 ICPES 84S0B 01 1 1.3 0.1 AA 84SAT 02

244 1 AA 78SZY 01 1 1.3 0.1 HPLC 83ICH 01 400 OES 75J0N 11 1 1.3 0.1 RTNA 75ABU 01 524 OES 75J0N 08 1

1

1.3

1.3

0.2

0.4

9 UNA

EXRF

78LAU 02

73GIA 01 Nb (uq/g) 1

1

1.3

1.3

0.5

0.6

11 ICPES

ICPES

81MUN 01 84S0B 01 < 0.3 L PAA 78HIS 01 1

1

1.31

1.31

0.11

0.17

UNA

FAA

75PIE 01 80DOR 01 Nd (nq/q) 1

1

1.32

1.33

0.02

0.07

ASV

VOLT

85ADE 01 84ADE 02

320 90 UNA 77NAD 02 1 1.36 0.11 FAA 86GAIJ 01 407 20 UNA 8400D 01 1 1.37 0.03 COLOR 77BUR 01 420 90 RTNA 83SIR 01 1 1.38 POL 85UTO 01 423 9 RTNA 840DD 01 1 1.4 FAA 82H0E 01 480 SSMS 78URE 01 1 1.4 FAA 73SEG 01 570 RTNA 77LAU 02 1 1.4 1 lENA 79KUC 01 570 D RTNA 82LAU 01 1 1.4 0.1 POL 72MA1 01 582 48 RTNA 86TSU 01 1 1.4 0.1 POL 74MAI 01 600 11 SSMS 85V0S 01 1 1.4 0.1 POL 77MAI 01 765 51 RTNA 83TJI 01 j

1

1.4

1.4

0.3

0.4

RTNA

XRF

77MEL 01 78STA 02

1

1

1.4

1.5

0.6

0.2

UNA

PAA

74RAN 02

80SEG 01 0.7 CPXRF 75CAM 01 1 1.5 0.3 EXRF 80DYC 01 0.95 11 SSMS 85V0S 01 1 1.5 0.3 PAA 80YAM 01

1 1 lENA 79KUC 01 1 1.5 0.3 RTNA 80SLO 01 1.1 16 AA 79AB0 01 1 1.5 0.7 CPXRF 85CLA 01 1.1 AA 83ELA 01 1 1.6 11 SSMS 85V0S 01 1.1 0.1 6 ICPES 85ABD 01 1 1.6 0.4 AA 78RIT 01 1.1 0.5 AA 83RAP 01 1 1.7 0.1 DCPES 79REE 01 1.14 0.08 FAA 79ST0 01 1 1.7 0.1 0 DCPES 81REE 01 1.15 0.07 11 ICPES 82J0N 01 1 1.8 CPXRF 84KAU 01 1.15 0.09 11 ICPES 82J0N 01 1 1.8 POL 83H0L 01 1.18 0.08 AA 80AGE 01 1 1.8 0.2 ICPES 79ABE 01 1.2 XRF 78CAM 02 1 2 NAA 77LAU 01 1.2 FAA 85L0N 01 1 2.1 0.02 ICPES 79HER 01 1.2 0.063 6 COLOR 78FUD 01 1 2.2 0.7 14NAA 81WIL 01 1.2 0.07 6 COLOR 78FUD 01 1 2.6 1 CPXRF 80KIR 01

1571-25
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

i (ug/g) cont.

2.9 1 CPXRF 77CAM 01

4 AE+AF 79ULL 01

4 1 .3 AA 79H0N 01 4.3 16 AA 79AB0 01 6 0.9 ICPES 84ABD 01

1400 OES 75J0N 04

1500 OES 75J0N 05

1500 11 SSMS 85V0S 01 1560 ICPES 78CAP 01 1600 ICPES 84NAD 01 1760 CPXRF 84KAU 01 1770 90 ICPES 81 OWE 01 1800 6 ICPES 83CHA 01 1800 OES 75J0N 07

1800 OES 75 JON 11 1800 100 COLOR 79MCQ 01 1845 ICPES 81 GOO 01 1883 100 ICPES 84PRI 01 1900 6 ICPES 83CHA 01 1900 OES 75J0N 10

1900 OES 75 JON 06

1900 40 ICPES 79MCQ 02

1900 40 ICPES 84ABD 01 1900 100 ICPES 85LIE 02

1900 100 ICPES 79MCQ 01 1900 200 6 FAA 81LAN 01

1901 61 1

1

ICPES 81MUN 01 1920 1000 EXRF 77NIE 01 1930 COLOR 77HAM 04

1958 69 1

1

ICPES 81MUN 01 1970 70 11 ICPES 82JON 01 1980 40 1

1

ICPES 82 J ON 01 2000 6 ICPES 83BRA 02

2000 COLOR 79HIL 01 2000 CPAA 80HAN 01 2000 ICPES 79EDI 01 2000 100 6 FAA 81 LAN 01 2000 100 6 FAA 81 LAN 01 2000 100 14NAA O 1 Ml L niU 1 2000 200 14NAA 81WIL 02

2000 400 CPXRF 80KIR 01 2000 500 ICPES 79ABE 01 2060 40 11 ICPES 82JON 01 2070 70 7 NM 81SHI 01 2070 100 lENA 79J0N 01 2090 60 11 ICPES 82J0N 01 2096.7 70.14 NAA 76GUZ 01

1571-

Conc Uncer Com Method Reference

P (ug/g) cont.

2100 OES 75 JON 02

2100 FAA 79EDI 01 2100 OES 75 JON 09

2100 6 ICPES 83BRA 02

2100 80 12 FAA 78EDI 01

2100 100 14NAA 80 FAA 01 2100 130 7 NM 81SHI 01 2110 110 7 NM 81SHI 01 2130 20 ICPES 79HER 01 2160 50 12 FAA 78EDI 01 2190 110 7 NM 81 SHI 01 2200 EXRF 810HT 01 2300 OES 75J0N 08

2380 180 EXRF 75REU 01 2400 OES 75J0N 03

2400 100 6 ICPES 85AB0 01 2400 200 ICPES 85LY0 01 2500 400 14NAA 77SEG 01 2600 6 ICPES 83BRA 02

2600 6 ICPES 85ABD 01 3100 OES 75J0N 01

'b (ug/g

J

15 5. 1 CPXRF 80ICIR 01 17.6 SSMS 81VER 02

24 7 SSMS 84V0S 01 26 AA 76FUK Af01 26 7 SSMS 84V0S 01 28.5 3. 6 FAA 77FUJ 01

31 2 ICPES 81 NAD A 4 01 33.6 1

.

5 FAA 77BRU A 4 01 34 7 SSMS 84V0S A 4 01 37 AA 73L00 A*y 03

37 8 SSMS 84V0S A 4 01 37.3 7 XRF 78STA AO02

38 3 FAA 77L0R A401 39 1 ASV 85ADE A401 40 AA 83ELA 01 40 11 SSMS 85VOS 01 40 2 EXRF 73SPA 01 40 3 AA 82R0D 03

40 4 PAA 78HIS 01 40.2 11 HAA 84KUM 01 40.7 3 EXRF 79GIA 01

41 ICPES 780AH 01

41 0. 6 ICPES 84ABD 01

41 1 ICPES 79HER 01

41 2 ICPES 85LIE 02

41 2 AA 84GLA 02
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Pb (ug/g) cont.

/ 1 TO MM OHon 1 (12

/.I R O^NMK QCUAP n2

/. 1 Q 1 1 HDi r U 1 He o U 1 Ht 84MAR 01

Ht FAA 82H0E 01 Ht 11 SSMS 85V0S 01 FAA 78URE 02

42 1 ICPES 79MCQ 02

42 1 .7 AA 80AGE 01 42 3 ICPES 79MCQ 01 42 4 ITNA 77GUI 02

42 4 NAA 76MI

L

02

42 9 14NAA 81WI

L

02

42HC 11 1

1

HAA 84KUM 01 HC b 1

1

FAA 7ounF 02

42HC a aU J > 1 1

1

MOV A^U 01 42 9 1

1

I 1 FAA 7QunF n?

43HJ FAA RnpRF ni\j \ 43 SSMS 1U\ IIT 01 43 EXRF 84PIN 01 43 2 POT 84PIN 01 43.2 5.1 FAA 82JEN 02

43.3 AA 76KRI 03

43.4 6 POL 72SIN 01 43.7 0.9 HAA 76V I

J

01 44 FAA 79HEI 03

44 FAA 73SEG 01 44 2 NAA 77J ER 01 44 2 FAA 80LEG 01 44 2 AA 7SAR1I 01 44 2 1

1

ICPES R2 inu 01 44 A pni r r ^o 1 n U 1 44 4 FAA r MM mifUA U 1 44 5 FAA f MM uHnuo U 1 44 FAA 1

1

44.1 3.1 11 ICPES u 1 nun 01 44.1 4 AA 01 LL 2 5 1 rAA Ul 44.3 FAA 79YAS 01 44.5 1.7 POL 74MAI 01 44.5 6.2 XRF 77SMI 04

44.6 1.7 POL 72MAI 01 44.6 1.7 POL 77MAI 01 44.67 1.53 ASV 77K0N 01 44.7 0.8 6 FAA 84FUD 01 44.9 ICPES 78CAP 01 44.9 1 ASV 82SAT 02

45 6 ICPMS 83D0U 01 45 POL 74LUT 01

Cone Uncer Com Method Reference

Pb (ug/g) cont.

\j FAA r MM R1O 1 JMU lAr 01

\J m J AA 73TAI r J \ ML 01 AS PAA r MM 7AI 1 IT 01 ASHJ 3 6 AA 79M0N 01U 1 AS 1 CPXRF 84KAU 01

45.1 2.5 AA 84ST0 01 45.3 CPXRF 75 CAM 01 45.3 0.7 FAA 79DAB 02

45.3 0.9 FAA 81KIT 01 45.3 1 . 13 FAA 82VAN 01 45,4 2 EXRF 73GIA 01 45.5 0.4 6 FAA 84FUD 01 45.5 0.7 6 FAA 84FUD 01 45.5 1 RTNA 72GIB 01 45.7 1 .3 ASV 84L0C 01 45.8 5 DCPES 84SNE 01 45.9 0.14 FAA 79ST0 01 45.9 1 .2 1

1

ASV 84L0C 01 46 5 DCPES 84SNE 01 46 FAA 82PRE 01 46 1 1

1

ICPES 82J0N 01 46 2 AA 77YAN 01 46 2 FAA 79KRA 01 46 2 AA 80SCH 05

46 2 D FAA 80SCH \tJ \^ WWII 08

46 52 R AA 75MAN 01 46.1 7 CPXRF 85CLA 01 46.2 3.5 11 ICPES 81MUN 01 46.4 AA 74B0P 01 46.5 16 AA 79AB0 01 46.5 1 .3 XRF 85AVA 01 46.8 5.6 HAA 82WEI 01 47 MMAA 79m I 01 47 ICPES 81WEI 01 47 5 FAA 81JAC 01 47 0.5 IDMS 83BR0 01 47 2.5 ASV 79BRI 02

47 4 ICPES 79ABE 01

/ -J c3

A CI/ ASV tSlDOG Ul

1*7 6 EXRF 79KUE 01 47.1 4.7 XRF 74REU 01 47.3 5.6 FAA 82UEI 01 48 5 AA 82RIT 01 48 5 AA 78RIT 01 48.6 3.8 EXRF 75REU 01 49 DCPES 78NAK 01 49 2 PAA 80SEG 01 49 5 EXRF 77NIE 01 49.3 16 AA 79AB0 01 49.3 1.5 PAA 80YAM 01

1571 -27
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Pb (ug/g) cent.

Cone Uneer Com Method Reference

Rb (ug/g) cont.

49.7 1.4 6 FAA 84FUD 01 1 10 ITNA 80CRE 01 50 AE+AF 79ULL 01 1 10 0.9 ITNA 79AHM 01 50 FAA 74BRA 03 1 10 1 14NAA 81UIL 02

50 AA 76FUK 01 1 10 1 EXRF 79ICUE 01 50 5 EXRF 77FL0 01 1 10 1.5 CPXRF 80KIR 01 50 11 AA 79MCQ 01 1 10.3 1 lENA 79KUC 01

51 3 EXRF 80DYC 01 1 10.3 0.6 ITNA 74RAN 02

52.6 FAA 78CAP 01 1 10.3 0.7 ITNA 75RIC 01 54 10 CPXRF 77CAM 01 1 10.5 ITNA 79KUC 01 54.5 7.2 ICPES 82AZI 01 1 10.5 ITNA 78CAP 01 56 1 6 ICPES 85ABD 01 1 10.6 1 lENA 79KUC 01 57 12 14NAA 81WIL 01 1 10.8 0.4 ITNA 79SAT 01 57 17 CPAA 77ZIK 01 1 10.8 2 SSMS 84V0S 01 58 6 ICPES 85ABD 01 1 10.95 0.08 ITNA 81K0S 01 67.5 6 DCPES 84SNE 01 1 11 RTNA 72M0R 03

76.1 AF 85NAR 02 1 11 0.8 EXRF 73GIA 01 85 OES 75B0L 02 1 11 1 ITNA 77Z1K 01

115 EXRF 81 PAR 01 1 11 1 EXRF 80DYC 01

1 11 1 ITNA 78LAU 02

Pd (ng/g) 1 11 2 RTNA 77MEL 01

1 11 2 CPXRF 77CAM 01 ( < 1 L RTNA 81BYR 01 1 11 16 R AA 75MAN 01

1 11.2 0.3 lENA 81K0S 01 Pr (ng/g) 1 11.2 0.4 EXRF 73SPA 01

1 11.2 0.9 ITNA 83AHM 01 60 SSMS 78URE 01 1 11.2 1.5 ITNA 81HAB 01

65 3 RTNA 840DD 01 1 11.28 0.42 NAA 76GUZ 01

103 15 RTNA 86TSU 01 1 11.3 2.9 5 ITNA 80TOU 01

110 RTNA 80SLO 01 1 11.3 5.2 EXRF 75REU 01 230 RTNA 77LAU 02 1 11.4 EXRF 81BIS 01 230 D RTNA 82LAU 01 1 11.5 XRF 78CAM 02

270 11 SSMS 85VOS 01 1 11.5 0.6 EXRF 79GIA 01

1 11.5 0.9 FAA 83GR0 02

Pt (ng/g) 1 11.5 1 EXRF 77NIE 01

1 11.6 1 ITNA 85HAD 01

< 1 RTNA 84TJI 01 1 11,6 3.4 SSMS 84V0S 01

0.2 RTNA 82ZEI 01 1 11.7 0.1 ITNA 78GIL 01 89.2 15.4 RTNA 77NAD 01 1 11.8 ITNA 80SAT 01

1200 300 RTNA 74CAR 03 1 11.8 1.2 35 ITNA 81GLA 03

11.9 0.8 NAA 78GAN 01 Rb (ug/g) 12 NAA 74BEL 01

12 0.04 ITNA 78FUR 01

5 2 EXRF 77FL0 01 1 12 0.7 ITNA 82C0R 01 8.5 0.6 EXRF 85COE 02 1 12 1.1 6 ITNA 74BEC 01 9.8 11 SSMS 85VOS 01 1 12 1.5 ITNA 77HAM 01 9.8 1.3 XRF 77SMI 04 1 12 2 ITNA 76KUC 01. 9.9 2.6 SSMS 84V0S 01 1 12.1 1 9 ITNA 78LAU 02^

10 CPXRF 84KAU 01 1 12.5 ITNA 85MIS 01

10 11 SSMS 85VOS 01 1 12.5 0.6 PAA 78HIS 01

10 NAA 77LAU 01 1 12.5 1 PAA 76KAT 04

1571-28
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Rb (ug/g) cont.

12.6 2.1 XRF 78STA 02

12.8 0.6 14NAA 81UIL 01

12.8 0.7 CPXRF 85CLA 01

13 0.9 W 81N0N 01

13 1 PAA 76KAT 02

13 2 ITNA 81KUL 01

13 3.5 CPXRF 81 ROB 02

13.1 2.5 SSMS 84V0S 01

14 1 ITNA 84TU 01

14 2 ITNA 85WAH 01 14.8 CPXRF 75CAM 01

15.61 3.01 ITNA 79REN 03

19.9 SSMS 81VER 02

28 EXRF 81 PAR 01 30 CPAA 78MCG 01 30 CPXRF 76ZEI 01

S Cug/g)

1200 CB 72J0N 03

1400 200 17 W 72J0N 03

1400 600 CPXRF 79REN 02

1660 220 TCGS 79AND 01 1690 5 TITR 80SMI 01 1700 200 TCGS 79FAI 01 1760 790 7 NM 83LI 01 1830 CPXRF 84KAU 01 1850 30 XRF 83GUN 01 1860 90 ICPES 84M0R 01 1860 180 COLOR 82BAR 01 1890 100 ICPES 84PRI 01 1900 34 CB 84HER 01 1920 20 CB 84LEC 02

1920 90 CB 86B0U 01 1943 23 CB 86GAU 01 1950 200 XRF 82BAR 01 1960 D CB 85JAC 01 1960 40 6 CB 84JAC 01 2000 300 IC 83HER 01 2020 180 CB 84GLA 11 2028 21 ICPES 85LIE 02

2040 D CB 85 J AC 01 2040 60 6 CB 84JAC 01 2120 XRF 78CAM 02

2120 50 EXRF 77NIE 01 2140 60 WXRF 86B0U 01 2150 200 CB 77LAN 01 2150 380 EXRF 75REU 01 2200 103 CPXRF 80KIR 01 2200 1100 7 NM 83LI 01

Cone Uncer Com Method Reference

S (ug/g) cont.

2300 200 TCGS 77JUR 01 2400 TURB 79B0G 01 2400 FE 79B0G 01 2600 400 CPAA 84R0U 01 2600 400 CPAA 85FRI 01 2700 400 XRF 81 NAD 01 7020 2620 EXRF 77NIE 01

Sb (ug/g)

1 . 1 0.2 ITNA 777 IK 01 0.2 HAA 74L00 Q 1 2.3 SSMS 85V0S 01 i.5 U.2o RTNA 83s I

R

01

•3 1 Z.5 O.o H ICPES 79R0B Ct 4 01 £.3 I TNA 78CAP Ul

•5 C i.b R ITNA 79 1 MA 01 2.3 i.o Ru I TNA 70 f u A AVIMA m\}5

2.33 i 1 1 1 C A A FAA ^ VHOE 02

2.33 i 1 FAA 79H0E 02

2.3f 0. 19 ITNA 79REN 03

O CO 2.30 (\ 17 f Tkl A ITNA OCu A n 03MAD 01 2.62 £o

U A A NAA ^oGAN Al01 i.l ITNA oUCRE 01

2. 1 4

1 T Ckl A

/ VKUC 01

2. f

kl A A NAA 771 Al 1 1 / LAU U 1 O 7 2. f U. 1

T Tkl A

1 INA 70I Al 1 02

O 7 2. f U.2 nU

DTkl A K 1 NA 71 f*nc Ul 2.7 0.2 RTNA 73G0E 01 2.7 0.2 ITNA 85UAH 01 2.7 0.3 ITNA 74RAN 02

2.7 0.3 6 ITNA 74BEC 01 2.7 0.4 14NAA 81WIL 02

2.7 0.4 6 ITNA 74BEC 01 2.72 0.01 ITNA 79AHM 01 2.72 0.01 ITNA 83AHM 01 2.72 0.2 ITNA 82QUR 01 2.77 0.02 H ICPES 81 PAH 01 2.8 HAA 80HON 01 2.8 ITNA 79KUC 01 2.8 1 lENA 79KUC 01 2.8 11 HAA 82KUE 03

2.8 ITNA 85MIS 01 2.8 0.1 7 RTNA 77GIL 03

2.8 0.1 RTNA 78GAL 01 2.8 0.1 H ICPES 82HAH 01 2.8 0.1 7 RTNA 80GAL 02

2.8 0.2 ITNA 81K0S 01 2.8 0.2 ICPES 830LI 01 2.85 0.06 RTNA 80SLO 01

1571 -29
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Sb (ug/g) cont.

c. • OO u . uo PTMA 7Ar;i 1 r Ou I L U 1 n ns 1 1 nn Anr^Ai OUunU (19

C - OO n ns 7 9 IMr; n3

£ > 7 1

1

03

9 0 n no 79HnF 01

C a 7 n 1 01 9£ > 07 n 9 ITMA 1 1 nn U 1 9 0 0U a 3J ITMA I 1 nn RATH oaf 1 U 01

? 9 0.5 RTNA 79REN 01

0 08 7 1 wn 02

? 92 0 08 7 RTNA 77GIL 03

V a AA 83RAP 01

9C. 0977 0 05 01

? 99 0.45 RTNA 02

•J 79RYR 01 I PTMA

•I•7 1

1

HAA K?V\ IF n 1 HAA ni

0 9 FAA ni

0 9 7f n?

3 02 0.26 HAA 70VI.I 01 3 1 1

1

HAA R?rRO 03

5# 11 0 03 W u 1 nun 01 3J a 11 0 1 ITMA 79^AT 01

J a 1 0.7 ITNA 77HAM 01 3J a 14It 0.13 RTNA 72BYR 01

3J a ISI J 0.26 PAA 01 3 ^f^ 0 ?f> MAA 77 IFR 01 3 ? 0 ? 7STAI 01 3 9S PAA "nn

» T J a 1

1

HAA i\nn 03

T »

J a J I TMA \ fin n3

3a3 0.2 5 ITNA 80T(X) 01 3a3 0.2 PAA 76KAT 02

3a3 0.3 ITNA 81KUL 01 3a3 0.6 RTNA 77KUS 01 3.31 0.15 ITNA 84NDI 01 3.5 ICPES 85NAR 02

3.5 AF 85NAR 02

3.5 0.2 PAA 78HIS 01 3.5 0.3 FAA 78HAY 01 3.78 0.02 ITNA 81HAB 01 3.8 0.2 RTNA 73TJI 01 3.8 0.6 6 NAA 78GAN 01 5.1 1.1 UNAA 81UIL 01

1571-30

Cone Uneer Com Method Reference

Sc (ng/g>

*»u D IIAA nMA r OunN U 1

Aft T D I

1 TMA 1 nn U 1 10 Ao MAA nnn f ouAn niU 1 41 W o 1 nun U 1 44 ITMA 1 1 nn 7APAU » Ti\Mn n9

SO 10 RTMA i\ 1 nn ni 52 XmJ ITMA I 1 nn n4

S4' L•r RTMA R 1 nn U 1 57 A I TNA 60 1 ITNA 7Al All 02

62 NAA ni 62 2 ITNA n"? 62 J ITMA i 1 nn OH 1 U ni 62 4.5 ITNA ni 63 Aw ITMA i 1 nn 01 6S MAA nnn 771 All 01 6S T I TMA 1 nn 7SPTr niU 1 66 I1 TMA 1 nn ASHAII OaJUniJ OO I TMA 1 nn AAni A 1 1 66OO A 1ITMA 1 nn 70CAT 1 TOM 1 ni ITMA I 1 nn 7ArAP ni 67 s ITMA 1 1 nn A1HAR 01

70.1 4 ITNA 83AHM 01 73 ITNA 80CRE 01 75 5 5 ITNA 80TOU 01 75 7 ITNA 85WAH 01 80 ITNA 79KUC 01 o ITMA I i nn 70RFM 03

fil 9 ITMA i 1 nn A4RIR 0*tU i D 01

I TMA 1 nn asmi^ 01 on 90 ITMA i 1 nn All^lll 01 iin 7AIIRF f OUI\u 01 i7n 1 r U sn RTMA n 1 nn 77MFI ni ?nn RTMA i\ 1 nn 79MnR r ^noi\ n*^ 9pn 1 u PAA r nn 74rHA ni

ing/g;

24 6.7 FAA 81MEY 01 53 FLUOR 79TAM 01

55 9 HAA 76FI0 01 56 20 RTNA 79R0S 02

57 6.3 ITNA 77HAM 01 58 14 RTNA 73TJI 01 60 20 D RTNA 74G0E 01 60 20 RTNA 73G0E oy

60 20 ICPES 830LI 01 64 7 ICPES 84MIA 01

65 14 9 ITNA 80UAN 01 68 FAA 82HEI 01
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Se. (ng/g) cont.

70f\j ni

IK) 1

1

1

1

UAHAmA u 1

7C\ fU AHUAA ni

7r» (U in u

n 1 Lrto o^nAn DOu AU niu 1 ynf\j Oft UAA dc \ An niu 1

/ U 5nn nK DTU A A1 CA A nx

70I c. oo r LUUK ni

( *f

f

1 TUA 1 Nn A1MPY ni

f H T1 TUA 1 NM A1O 1 UAU nnn ni

r J c 7 AHCAI TO

7^ c 7 77^^ 1

1

r r U 1 L 7Sf J AA A'^PAP OJl\Mr ni

7fs 1 o HAA riMM A1 HAM 01u 1

7f\ I 1

1

1 1 AIIIPH o 1 ui^n n?

7Ar D in T TMA 7QAHM ni

77 1

7

1 r PI imp 7/ Aun ni 77 c 1

1

1 1 Uw Alt irH n?

77 c PIPLUUK 1 inp r OLnM n?

77 o PA A f yVUD ni 7A UAA 77t f f 1 uuUN ni

7A 7 T

1 rPFQ UrCo AAMf A ni

7Rr O H MO V AAAHP ni

7ft / PTMA f\ 1 WM 7Arnn f owuu ni

78 4 TTMA 1 1 HM 77RI 1

T

f 1 Uw 1 78 5 GC 77POO 01 78 7 34 HAA 78FLA 01 78 7.2 HAA 81MEY 01 78 10 ITNA 83AHM 01 78 10 ITNA 85UAH 01 78 11 RTNA 82POL 01 79 12 RTNA

79 12 RTNA

79.8 ftu MAA PIMM 7Ani 17 ni

80 171 f PI iinp 7/ AMn ni

80 MAA PIMM 7AnAM ni

80 PTMA 77Mnp f cnuK cn\jj 80 7 AAMT A ni 80 1

1 PAA rMM OUNC V ni 80 4 pr

1Luui\ 1 inp AOi^nH ouKun ni uU 1ft RTNA oUKNA 1

80 10 9 ITNA 79V0B 01 80 10 9 ITNA 79PAV 02

80 10 RTNA 75ABU 01 80 10 RTNA 740RV 01 80 10 ITNA 84GIB 01 80 20 HAA 80AGE 02

80 20 SSMS 77RO0 02

80 30 ITNA 81K0S 01 80.4 4.6 RTNA 78G0E 03

81 9 HAA 83KOL 01

Cone Uncer Com Method Reference

Se (ng/g) cont.

A? Cv IPMA 1 cnn ni APoc OL UAA 7AI / 01 UMnn n?

A7 /H UUr Co A1 TAR n?

1.H 7ATAI / H 1 ML n?

A"^ / V V A10 1 MDIJ nun ni

A*^ 1? 0 ni AAOH ft PTMA ni AS 4 TTMA 1 1 nn f Ton 1 ni AA 10 TI TMA 1 nn f OU 1 u ni 87 171 f 7^AND f *Tnniy 01•J 1 87 AW FLUOR 01 87 FLUOR 74LEI 01 87 7 HAA 75s IE 01 87 10 7 RTNA n 1 nn 77RI

1

03UJ 87 10 7 RTNA i\ 1 nn 80GAL 02

88 7 RTNA i\ 1 nn 73HFY 01 88 111 7^1 1 1 1 HMn n 0?

88 1A1

0

nw¥ A^V r onnu ni 89 Fl unR 01 89 17 ITNA 1 1 nn 01 90 HAA nnn ounun ni

90 11 HAA nnn 85PIW 01 90 4 HAA 85YAM 01 90 10 7 RTNA 80GAL 02

90 10 7 ' RTNA 77GIL 03

90 10 RTNA 77BAN 03

90 10 RTNA 78GAL 01 90 10 ITNA 82QUR 01 90 20 ITNA 79PAV 02

90 30 ITNA 78LAU 02

100 ITNA 80CRE 01 100 ITNA 1 1 nn f T VUD 01

100 20 7f RTNA i\ 1 nn 80GAL 02

100 70 0T ITNA I 1 nn 7fti f OLnuAll Vic 100 •iA 20 6 ITNA 74BEC A 4 01 100 40 NAA 74LEI 01 110 20 RTNA 80SLO 01 110 30 AA 79PAV 02

118 79 HAA 77IHN 03

130 40 RTNA 77MEL 01 140 20 ITNA 74RAN 02

140 90 RTNA 83SIR 01 160 ICPES 84MAR 01 200 ITNA 78CAP 01 1100 170 HAA 74CHU 01

1571 31
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Si (ug/g)

ATS R 1? NAA nnn 01 A75.8 12. 3 ITNA 75PIE 01 480 14 CPXRF 80KIR 01 500 200 14NM 80FAA 01 600 VV 81N0N 01 750 NAA 78GAN 01 1000 160 14NAA 77SEG 01 2080 CPXRF 84KAU 01 2340 60 lENA 79J0N 01 2400 11 SSMS 85VOS 01

5m (ng/g)

16 3 lENA 81K0S 01

19 4 ITNA 81K0S 01 88 8 5 ITNA 80TOU 01 90 SSMS 78URE 01 90 140 R ITNA 79 1 MA 01 92 2 RTNA 86TSU 01 100 ITNA 79KUC 01 100 RTNA 77LAU 02

100 1 lENA 79KUC 01 100 D RTNA 82LAU 01 100 NAA 77LAU 01 100 30 ITNA 77NA0 02

105 4 RTNA 80SLO 01 110 ITNA 80CRE 01 110 10 ITNA 78LAU 02

110 10 RTNA 83SIR 01

110 30 TCGS 79FAI 01 113 7 RTNA 83TJI 01 114 1 RTNA 840DD 01 130 40 ITNA 77HAM 01

140 1 lENA 79KUC 01 140 RTNA 72M0R 03

140 40 ITNA 74RAN 02

150 20 W 81N0N 01 150 33 ITNA 85MAD 01 170 30 TCGS 79AND 01 320 120 ITNA 79RE^f 03

Cone Uncer Com Method Reference

Sn (ng/g)

180 10 H ICPES 82HAH 01 230 11 SSMS 85VOS 01 284 4 5 RTNA 748YR 01 290 25 RTNA 77BYR 01 304 15 5 RTNA 74BYR 01 340 90 ICPES 80HAA 01 375 25 COLOR 820MA 01 1750 AF 85NAR 02

4100 RTNA 72B0W 01

r (ug/g)

14.5 2.5 FAA 77FUJ 01

18.1 SSMS 81VER 02

23 OES 75J0N 03

26 2 EXRF 85COE 02

28 0.6 PAA 78HIS 01 28 28.3 R AA 75MAN 01 29.7 CPXRF 84KAU 01 30 6 SSMS 84V0S 01 30.4 6 ICPES 83BRA 02

31 11 SSMS 85V0S 01

31 3.3 CPXRF 80ICIR 01 31.3 4.1 XRF 77SMI 04

31.7 4.8 14NAA 77VAN 01 33 11 SSMS 85V0S 01 33 4 SSMS 84V0S 01 33 6 SSMS 84V0S 01

33.1 EXRF 81BIS 01 33.6 6 ICPES 83BRA 02

34 1 FAA 82SUZ 03

34.3 0.5 EXRF 73SPA 01

35 OES 75 JON 04

35 NAA 77LAU 01

35 2 EXRF 80DYC 01

35 3 9 ITNA 78LAU 02

35 3 ICPES 79ABE 01

35 5 SSMS 84V0S 01 35.2 ICPES 780AH 01 35.2 4.9 ITNA 84TU 01 36 6 ICPMS 83D0U 01 36 CPXRF 76ZEI 01 36 CPAA 78MCG 01 36 1 ICPES 85LIE 02

36 6 ITNA 78LAU 02

36.2 2 PAA 74CHA 01 36.3 1.3 EXRF 79GIA 0\

36.3 1.8 CPXRF 85CLA 01 36.5 0.3 ICPES 79HER 01 36.5 1 PAA 76KAT 04

1571 -32
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Sr (ug/g) cont.

1

1 Te (ng/g)

36.5 2 EXRF 77FL0

1 01 1 10 3 HAA 85YAM 01 36.5 4 EXRF 75REU 01 1 11 3 35 RTNA 75GLA 01 36.6 1.2 EXRF 73GIA 01 1 36.7 6 XRF 78STA 02 j Th (ng/g)

37 1 ITNA 79SAT 01 1 37 1 PAA 76ICAT 02 1 6.6 0.3 lENA 81K0S 01 37 1 ICPES 79MCQ 02 1 6.8 0.4 ITNA 81K0S 01 37 2 ICPES 79MCQ 01 1 40 10 RTNA 83SIR 01 37.2 0.2 lENA 81K0S 01 1 44 ITNA 79KUC 01 37.4 8.3 CPXRF 81 ROB 02 1 44 1 lENA 79KUC 01 37.8 6 ICPES 83BRA 02 1 50 10 RTNA 80SLO 01 37.8 0.1 lENA 85GAU 04 1 52 4 ITNA 78LAU 02

38 5 NAA 78GAN 01 1 59 13 ITNA 81KUL 01 38.7 1.5 ITNA 81K0S 01 1 59 20 ITNA 74RAN 02

39 2 14NAA 81UIL 02 1 60 ITNA 80CRE 01 39 3 ICPES 84S0B 01 1 60 NAA 77LAU 01 40 RTNA 72M0R 03 1 63 23 ITNA 85MAD 01

41 3 RTNA 77KUS 01 1 69 1 lENA 79KUC 01 42.2 4.2 XRF 74REU 01 1 69.8 8.1 RTNA 85JAI 01 44.2 2.85 NAA 76GUZ 01 1 85 ITNA 85MIS 01 45 OES 75J0N 01 1 90 50 W 81N0N 01 45 EXRF 810HT 01 1 45 2 ITNA 74RAN 02 1 Ti (ug/g)

45 15 CPAA 77ZIK 01 1 53 4 14NAA 81UIL 01 1 2.4 0.4 CPAA 77ZIK 01 118 EXRF 81 PAR 01 1 6.6 0.5 ICPES 79ABE 01 160 6 I CPUS 83D0U 01 1 7.6

10.5 0.8

ICPES

ICPES

78CAP 01 85LIE 02

Ta ^ng/g) 1

1

14.2

17.2 0.3

SSMS

COLOR

81VER 02

82KIR 02

5 NAA 77LAU 01 1 17.7 2 SSMS 84V0S 01 7 2 ITNA 78LAU 02 1 18 8.5 EXRF 79GIA 01

10 ITNA 80CRE 01 1 19.1 1 1 SSMS 85VOS 01

10 3 ITNA 74RAN 02 1

1

19.3

21.9 3

1 1 SSMS

CPXRF

85V0S 01 85CLA 01 Tb (ng/g) 1

1

22

22

23

SSMS

SSMS

84V0S 01 84V0S 01 1.23 0.12 ITNA 77NAD 02 1 23 2.3 SSMS 84V0S 01 9 1 RTNA 80SLO 01 1 24 5 FAA 86GAU 01 9 2 RTNA 86TSU 01 1 26 SSMS 78URE 01 10 7 RTNA 83SIR 01 1 26 3 14NAA 81WIL 01 12 2 ITNA 78LAU 02 1 28.6 CPXRF 84KAU 01 13 D RTNA 82LAU 01 1 30 4 14NAA 81WIL 02

13 RTNA 77LAU 02 1 40 ITNA 78LAU 02

14 ITNA 80CRE 01 1 60 NAA 77LAU 01 15 NAA 77LAU 01 1 96 12 PAA 78HIS 01

15 2 RTNA 83TJI 01 1 191 33 ITNA 81HAB 01 18 1 ITNA 74RAN 02 1 72 6 RTNA 840DD 01 1 80 SSMS 78URE 01 1

1571 -33
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

(

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Tl (nq/q) V (nq/g)

32 11 ASV 84LIE 01 1 140 30 6 ITNA 74H0F 01 34 11 ASV 84LIE 01 1 248 10 11 RTNA 82HEY 02

36 11 FAA 84LIE 01 1 300 35 ITNA 81GLA 03

40 20 FAA 77BRU 01 1 340 20 11 RTNA 72LEV 01 74 FAA 82HEI All 1 01 1 361 90 UU 75WEL 02

200 40 PAA oOSEG 01 1 370 11 FAA 77MYR 01 300 100 PAA 78HIS 01 1 377; 10 RTNA 80HEY 01 390 980 RD ITNA 79IHA 03

Tm (ng/g) 390 980 R ITNA 79IMA 01 400 100 ITNA 77ZIK 01 < 10 RTNA 77LAU 02 1 401 16 RTNA 79C0R 01

< 10 D RTNA 82LAU 01 1 401 16 RTNA 81 COR 02

3.72 0.23 ITNA 77NAD 02 1 408 16 RTNA 80HEY 01 7 5.5 RTNA 840DD 01 1 408 16 11 RTNA 82HEY 02

10 SSMS 78URE 01 1 409 41 RTNA 72DAM 01 410 15 RTNA 80HEY 01

U (ng/q) 410 15 11 RTNA 82HEY 02

435 20 RTNA 80HEY 01

18 3 lENA 79FAA A 4 1 01 1 440 40 RTNA 79BL0 01 25 4 35 RTNA 75GLA A 4 1 01 1 440 200 ICPES 85LIE 02

25 5 PAA 80SEG A 4 1 01 1 471 14 11 RTNA 78BYR 01 25.2 1 RTNA 780ER A 4 1 01 1 480 28 COLOR 82KIR 01 26 3 RTNA 72BEC A7 1 03 1 500 150 RTNA 77GUI 03

27 8 ITNA 81ICUL A4 1 01 1 530 50 11 ICPES 82JON 01 27 10 ITNA 85UAH A4 1 01 1 535 NAA 80KOS 02

28 2 NT 72BEC A7 1 03 1 535 30 11 RTNA 78BYR 01 28 3 5 RTNA 80AUG A 4 1 01 1 540 20 11 ICPES 82JON 01 28 3 lENA SiKOS A 4 1 01 1 570 110 ITNA 81HAB 01 29 3 5 RTNA 80AUG A 4 1 01 1 570 140 6 ITNA 74H0F 01 30 35 DNA 81GLA 04 1 580 ITNA 76BAT 01 30 1 IDMS 72BEC 03 1 580 70 ITNA 75RIC 01 30 4 13 PAA 81SEG 01 1 580 130 ITNA 77HAM 01 30 6 13 PAA 81SEG 01 1 598 32 ITNA 80HEY 01 30.6 0.6 35 DNA 80GLA 04 1 600 20 RTNA 79BL0 01

31 7 DNA 84GLA I i 1

I I

1 600 200 ITNA 78LAU 02

32 5 ITNA 81K0S 01 1 610 23 ITNA 73PIE 01 32 9 ITNA 74UEA 01 1 622 23 11 RTNA 72LEV 01 33 2 DNA 84GLA 02 1 640 310 UU 75GUI 01 33.6 0.6 DNA 85GAU 04 1 643 129 RTNA 76GUI 01 34.3 0.6 DNA 86GAU 01 1 660 11 SSMS 85VOS 01 56 9 35 DNA 81GLA 03 1 680 11 SSMS 85VOS 01 700 100 ITNA 79K0B 03

750 110 W 81N0N 01 800 ITNA 78CAP oi

900 20 ITNA 76GAL 01 2200 100 ICPES 79ABE 01

1571-34
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Referenee

W (ng/g) Zn (ug/g) eont

.

< 2000 L RTNA 72M0R

1 03 1 22 AA 83ELA 01

16 4 RTNA 80SLO 01 1 22 1 EXRF 80DYC 01

20 7 RTNA 77KUS 01 1 22 3.1 CPXRF 80KIR 01 50 10 RTNA 83SIR 01 1 22.5

23

0.8 AA

AA

76GAL 01 73L00 03

Y (ng/g)

1

23

23

AA

AE+AF

84SAT 02

79ULL 01

< 1000 L EXRF 79GIA 01 1 23 OES 75JON 02

< 1100 L 14NAA 81UIL 01 1 23 EXRF 818IS 01

< 1100 L 14NAA 81WIL 02 1 23 ITNA 78CAP 01 480 SSMS 78URE 01 1

1

23

23 1

11 SSMS

RTNA

85V0S 01 76MEL 03

Yb (ng/g) 1

1

23

23

11.5

RTNA

EXRF

77MEL 01 85COE 02

11 RTNA 80SLO 01 1 23 2 7 RTNA 80GAL 02

20 SSMS 78URE 01 1 23 2.1 XRF 78LIN 01 20 2 RTNA 86TSU 01 1 23 5 SSMS 84V0S 01 20 20 RTNA 83SIR 01 1 23.1 ICPES 78CAP 01

21 1 ITNA 77NAD 02 1 23.1 0.8 RTNA 83DAN 01

21 2 RTNA 83TJI 01 1 23.2 2.2 AA 77BRU 01

25 RTNA 77LAU 02 1 23.3 2.7 RTNA 74RAV 01 25 D RTNA 82LAU 01 1 23.4 1.4 11 ASV 84L0C 01 27 5 RTNA 840DD 01 1 23.5 0.9 11 ICPES 82JON 01 29 3 ITNA 81K0S 01 1 23.5 1.8 AA 73TH0 01

31 1 lENA 81K0S 01 1 23.7 0.8 EXRF 73GIA 01 34 3 ITNA 85UAH 01 1 23.75 ITNA 82AKA 01 40 NAA 77LAU 01 1

1

23.9

23.9

1.5

3.2

ASV

PAA

84L0C 01 80YAM 01 Zn (ug/g) 1

1

24

24

FAA AA73SEG 01 81ARA 01

12 EXRF 82KEE 01 1 24 FAA 83ATS 01

13 OES 75B0L 02 1 24 6 ICPES 83CHA 01

15 3 CPXRF 77CAM 01 1 24 1 AA 77FRY 01 17 AA 76KRI 03 1 24 0.4 W 81N0N 01 17.1 2 EXRF 77FL0 01 1 24 1 7 RTNA 84FAR 02

18 OES 75JON 09 1 24 1 RTNA 740RV 01 18 1 ICPES 85LIE 02 1 24 1 7 RTNA 84FAR 02

19 FAA 83ATS 01 1 24 1 11 AA 78GAI 01 19 4 ICPES 79HER 01 1 24 1 AA 84GLA 02

19.8 6 ICPES 83BRA 02 1 24 1.5 FAA 84R0S 01 20 3 ITNA 81KUL 01 1 24 2 11 AA 78GAI 01 20 4 ICPES 82AZI 02 1 24 2 7 RTNA 84 FAR 02

20 6 CPAA 77ZIK 01 1 24 2 ITNA 85WAH 01 20.3 11 SSMS 85V0S 01 1 24 3 AA 77YAN 01 21 1 ICPES 79ABE 01 1 24 28 R AA 75MAN 01 21 2 ITNA 75RIC 01 1 24.2 1.5 NAA 77JER 01 21 7 SSMS 84V0S 01 1 24.2 1.5 PAA 74CHA 01 21.5 1.8 ICPES 82AZI 01 1 24.2 2 AA 83RAP 01 21.7 2.8 ITNA 81HAB 01 1 24.3 0.3 11 ICPES 82JON 01 22 ITNA 79KUC 01 1 24.4 0.9 CPXRF 85CLA 01

1571-35
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference

Zn (ug/g) cent.

Cone Uneer Com Method Reference

Zn (utj/g) cont.

24.5 CPXRF 84KAU 01 1 26 1 ICPES 79MCQ 02

24.5 XRF 78CAM 02 j 26 1 ICPES 79MCQ 01 24.5 0.6 RTNA 80SLO 01 1 26 1.3 11 AA 75 ISA 01 24.5 0.8 RTNA 838 1

01 1 26 2 11 ICPES 82J0N 01 24.5 3 EXRF 77NIE 01 1 26 2.1 AA 78LIN 01 24.6 RTNA 79BYR 01 j 26 3 ICPES 80SCH 05

24.6 0.9 SSMS 72MAG 01 ! 26 3 D ICPES 80SCH 08

24.6 2.2 11 ICPES 81MUN 01 1 26 3 RTNA 74CAR 03

24.7 AA 83 FAG 01 1 26 3 EXRF 79KUE 01 24.7 1.5 ITNA 84TU 01 1 26 3.4 ITNA 77HAM 01 24.7 2.2 EXRF 79MAT 01 1 26 4 ITNA 76KUC 01 24.8 1.1 ITNA 78GIL 01 1 26 4 ICPES 84ABD 01 24.8 1 .9 ITNA 79SAT 01 1 26 5 AA 75ABU 01 25 ITNA 80CRE 01 1 26 14 AA 82HAR 01 25 ITNA 80SAT 01 1 26.1 2.2 ITNA 82COR 01 25 OES 75J0N 03 1 26.3 5 XRF 78STA 02

25 RTNA 72M0R 03 j 26.4 1 .8 ICPES 83SCH 04

25 6 ICPES 83CHA 01 j 26.7 4.6 6 ITNA 74BEC 01 25 ICPES 81WEI 01 1 26.8 1.2 ITNA 81K0S 01 25 ICPES 84 SOB 01 ! 26.9 1.1 11 ASV 84L0C 01 25 11 ICPES 82JOM 01 j 26.9 1.2 RTNA 73TJI 01^

25 6 ICPES 85ABD 01 1 27 6 ICPES 85ABD 01 25 11 ICPES 82JON 01 1 27 OES 75 JON 06

25 AA 78RIT 01 j 27 AA 79HIL 01 25 1.6 EXRF 73SPA 01 ! 27 1 AA 77FRY 01 25 2 9 ITNA 78LAU 02 1 27 ICPES 78DAH 01

25 3 FAA 82JEN 02 1 27 NAA 77LAU 01

25 3 ITNA 78LAU 02 1 27 1 11 ICPES 82JON 01

25 4 SSMS 84V0S 01 1 27 2 RTNA 77KUS 01 25.07 0.76 NAA 76GUZ 01 1 27 2 RTNA 73G0E 01 25.1 0.7 AF 75EPS 01 1 27 2 D RTNA 74G0E 01 25.1 0.8 AA 75EPS 01 1 27 2 ITNA 83AHM 01 25.3 SSMS 81VER 02 1 27 2 FAA 74TAL 01 25.3 0.5 AA 80AGE 01 1 27 2 7 AA 73TAL 01 25.3 2.1 EXRF 79GIA 01 1 27 3 PAA 76KAT 02

25.3 2.5 5 EXRF 79MAT 01 1 27 4 PAA 76KAT 04

25.5 1AA 79H0E 02 1 27 5 SSMS 84V0S 01

CJ .J o I CrcS Q7DD A 02 1 07£r f 1 1 NA f f ClK U 1 25.5 1.1 6 ITNA 74BEC 01 1 27.2 2.4 ITNA 74RAN 02

25.6 3.4 EXRF 75REU 01 ! 27.3 ICPES 85NAR 02

25.6 7.64 AA 79M0N 01 1 27.3 2.1 ITNA 82QUR 01 25.9 FAA 78CAP 01 1 27.3 2.1 ITNA 79AHM 01 26 OES 75 JON 10 j 27.4 2.7 XRF 74REU 01 26 OES 75 JON 11 1 27.5 11 AA 79H0E 02

26 OES 75J0N 05 1 27.6 1.3 CPXRF 81 ROB 02

26 NAA 74BEL 01 I 28 OES 75ISA

26 6 AF 84NAR 02 1 28 ITNA 85MIS Om

26 6 AF 84NAR 02 j 28 1 D DCPES 81REE 01 26 1 11 ICPES 82JON 01 1 28 1 DCPES 79REE 01 26 1 11 ICPES 82J0N 01 j 28 3 FAE 74TAL 01

1571-36
TABLE 1571-2: INDIVIDUAL DATA FOR NBS SRM 1571 (cont.)

Cone Uncer Com Method Reference Cone Uncer Com Method Reference

Zn (ug/g) cont. Zr (ug/g)

28 3 7 AE+AF 73TAL 01 28 5 FAA 77L0R 01 28.1 CPXRF ^CAM 01 28.3 0.8 ITNA 79K0B 03

28.3 2.6 6 POL 72SIN 01 28.5 6 ICPES 83BRA 02

28.5 0.8 ICPES 81ICNA 01 28.6 2.5 11 ICPES 81MUN 01 28.7 AF 85NAR 02

29 0.87 11 AA 75ISA 01 29 1 FAA 79KRA 01 29 2 ITNA 74GUI 01 29 5 NAA 78GAN 01 29 32 RD ITNA 79IMA 03

29 32 R ITNA 79IMA 01 29.1 3.7 ICPES 85LY0 01 29.3 2.5 PAA 76WIL 01 29.5 6 AA 72SIN 01 29.6 16 AA 79AB0 01 29.6 16 AA 79AB0 01 29.63 1.8 ITNA 79REH 03

29.8 6 POL 72SIN 01 30 EXRF SIGHT 01 30 ICPES 81 GOO 01 30 2 5 ITNA 80TOU 01 30 2 AA 79MCQ 01 30 3 PAA 80SEG 01 30 4 ITNA 78FUR 01 30.5 1.2 RTNA 76GAL 01 31 OES 75JON 04

32 OES 75 JON 07

34 3 PAA 78HIS 01 35.6 11.4 XRF 77SMI 04

36.4 7 ITNA 85MAD 01 37 ICPES 84NAD 01 38 6 FAA 77FUJ 01 41 OES 75JON 08

45 XRF 80SUZ 02

56 CPXRF 76ZEI 01 56 CPAA 78MCG 01 77 EXRF 81 PAR 01 81 OES 75JON 01

0.4

1.3

1.6

1.7

2.1

3

3.8

210

3 L EXRF 79GIA 01

5 L 14NAA 81WIL 01

11 SSMS 85VOS 01 0.3 PAA 78HIS 01 0.2 9 ITNA 78LAU 02

0.44 PAA 84SAT 01 NAA 77LAU 01

1 14NAA 81UIL 02

CPAA 77ZIK 01 20 PAA 74CHA 01

1571-37
"8

Qo ^—I

:c

c

1—

LU

CO

LUC

f1 t—O c

<U

00

co 8M

+1 ">

0)

c

I- (D

z:

t/> Ul „>

Ill _l

c

CO

ZD

oe. CO

-I— o +1C

(D in <1J ' zOf

(/>

(/) m LU z U

Of <

FO<1—<oQLU

Z 1 <

Q.

o s: LU ou

^-1 t\i NC

in

LU

oCO

CO < z ,1— LU +1

c/> z c o mOX

(/I m

c

0)

CO (/I Ul (/> Ul Q. U Q. O O CJ 5

a.o

CO

C3o

LU

U a. —I

CJ Ooi: (/> O LU

-I Q. o o

CJ

—

CO

CJ

wUl (/> Q. C3 CJ O

CJ5 3

OJ '

f ooM

lA

T- Vl- »- O

in

o 1^ +1 o

fVI «- »-

in • «- in

rj «- CM

f«1 CO

M in

in

(M ro

0>

ro

o00 COCO

ro

00

in

N.

NNO

f-5

in

in

o

(M CMO

tM

O ^

1^

O o> m in O 1 m 1 a a «— 1 ro 1 1I a 1 1 1

f\i

aaaaa

a ro

aaaaa

a (M

a in

rvio

o 00

00

o in

00 in 00 . 2S

o

a.o

o

o

in i a ^ 00

O

>o

o

aa

a • in •H Ln i a ^ «

O

in

in

in

in

oinOin.

oo -O OO O o in

^— fO evj in

t o 1 00

a

(VJ

a Oa O in O

in

inom

(\l -* ro CM ro vO CM ro «- CM in CM ro CM in

ro COo

o

o ino

O in o in o >o in >o o ro o in 1^ o • • fO vO Kl ro CM O Ch 00 m

<> +1 ro +1 -S-l -4- inoM •H CM ro ro +) 00 +1 o«H +1 ^

o f\j 00 >j- in

o ro

o ro

oO 0> O 00 00 ro O ro >d CM -Om o ro -O

ro CMoooo in O o o o lO o O CM o o ro a a 1 o o a a o a a 1 a a a +1 +1 a a +1 0 (M H OO H a a a M a 1 H i -H H a a H a a 1 fHI o a a a a a 1 a a .1 OO in O o CM o O CM 'io 00 CO OO o

ro

O 00 «

in

COO t3> o> O) O) o> o>

OO t3> en O)

1—

\\\

\

\ v.\ '\

\\\

\\\\\ o> cn Ul C35 cn Ol o> D) > ) cn o C7> a> cn cn cn z 3 3 a 3 3 3 c C 3 c c 3 c 3 C 3 3 c c c 3 3 c s« C c 3 s« c c c 3 —' en < < 3< m 0) CQ CO CO CO

<u i- CQ CO(D T3 d)

—' O

OO CJO CJ

I- cn 3 3 >K

CJ CJ CJ

o

o LL. U. C3

(D

—

— !a<: _l _J

1572-1
ofi

LU

</> LU ^ . C C o >^

CO

LU> 5 H <

-J (D0)

</)

X

Q£1—

tA

T—y^

(/> 0) z

rvQ< III Q < oUJ

-J

CLsu z<

151

Q111

m

UJ

_i

flD <1—

Cw

CO

O 3 (/) </] z

UJ

(/)

H z C o nj u

w (/) </) (/> Ul v> UJ o UJ u UJ CO (/) (/> (/I a. u o a. _i o. _l a. z 3E z u u o u a. o a. u CD u 1— I— z z u v~

(AU a.

a

O —I

o

UJu

a. -I u o.

<\j

<\J

<M

(\J

(VJ

O

CO

OfSJ (\J (M00 5 oo o H O oooT- eo

to

(\J

o

8: 2

f\J N-

(\j «

f\J <\J

rvi to

in

to

o

oo

ou-1 to

ro «- «- <NJ

+1 to • »-

(\J «o »-

o4-

oo to

o <NJ

(NJ

ino

(\j NO

o oo

to f\j

O to

o in

in in to to to to CM

o in

(\j >*• 00 >* 1 III 111 1 in 1 1 1 oo

m 1 1 o i

rvj 1CvJ 1 o 1 o 1 i1 CO 1 1 1 1 1 1 III f\J 1 1 1 1 1 III 1 o 1 1 1 1 1 11 o 1 1 1 1 in 1 CO 1 00

CM

O

ooo (\I to ro rsi >o to to 00

too

to

to5o•4-

o

o

^\

CM to CM CM to CM «- to CM in CM to CM CM

o

w

—

w

>*

O in

o 00

o CM CM 5 o On to CM

(M

mo 1 1 to

O CM

O +( in •H •H to vO -H I 1 >o «— to « in +4 CM •H >»•

M r- to to 1 t o CO CO

o> toO

o CMo 00O o>

O oo CO

o >*

CM to

oo CM CO

to

C/> CO -ft c

CO

NO

oo >*•o

Oo

oo

o CM On NO

00

CO to CM CM

o

o 1 1 1 1 o

o in CMo

CO 1 o

oO I CO 1 H +1 CO

•H +1

H +1H -H 1 1 1 1 1 1 ^ 1 1 CM in >*CO+< 11 1 CO 1 in 1 r— 1 1 44 1 to o o o O to

>*•

OoV On

CO NO

oNOO

to to

N-O>»o

V CM

O) (7> CD O) N^ \ ) 3 3 C X 3 c c 3 3

D> O) 0> O) D) O)

OO

.,_ o>

s

a. a. a. 3

to to

CO to to to (/>(/>(/> f/> (/> (/> X)

CO

cc a<

O) O) cn O) CD o> O) O) \ \ \ \ -V NV

cn O) O) o> o> at D) o> a>

cc 3 3 cc 3 cccCc 3 3

CO t/5

c SiV

— —'

I- 3 > 3 >-

cc

tMN

1572-2
TABLE 1572-2: INDIVIDUAL DATA FOR NBS SRM 1572 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Corn Method Reference

Al (uq/q) Ce (nq/q)

75 2 lENA 85GLA 02 1 392 53 RTNA 83TJI 01 78 12 ICPES 85ISS n 4 1 01 1 514 79 RTNA 86TSU 01

As (ug/g)

]

CI (uq/q)

2.7 0.3 RTNA 85GAU 04 1 391 6 TCGS 83AND 01 2.77 0.2 RTNA 86GAU 01 1 417 ITNA 86GAU 01 3.2 0.06 RTNA 84GLA 11 1 3.38 0.05 RTNA 848YR 02 1 Co (na/q)

Au (dq/q)

1

1 16 1 RTNA 84BYR 02

110 8 RTNA 82ZEI 01 1 Cr (uq/q)

B (uq/q)

1

1 1 0.5 FAA 85GAU 04

64.3 0.6 TCGS 83AND

1 01 1 Cs (nq/q)

69 0.3 ICPES 84PRI 01 1

1 83 ITNA 86GAU 01 Ba (uq/q) 1 85 6 ITNA 84GLA 11

j 111 25 ITNA 85GAU 04

23 6 FAA 86GAU 01 j 24 1 ICPES 85WHI 02 1 Cu (uq/q)

Be (ng/g)

1

1 14.6 0.3 RTNA 84BYR 02

1 15 1.8 ICPES 85ISS 01 6 0.4 FAA 86GAU 01 1 15.9 0.2 HPLC 85ICH 01 7.2 FAAC 86GAU 01 1 16 0.56 11 AA 75 ISA 01 7.6 1.6 FAAC 85GAU 04 1 17 0.14 11 AA 75 ISA 01

1 17 4 AA 86GAU 01 Br (uq/q) 1

1 Dv (nq/q)

8.36 ITNA 866AU 01 1

1 43 7 RTNA 86TSU 01 Ca (%) 1 Er (na/o)

3.07 0.0055 11 AA 75ISA 01 1 3.12 0.25 ICPES 85ISS 01 1 22 3 RTNA 86TSU 01 3.14 0.0053 11 AA 75 ISA 01 1 3.15 0.29 ICPES 85LY0 01 1 EU (nq/q)

3.19 0.03 ICPES 85WHI 02 1 3.47 0.05 TCGS 83AND 01 1 12 0.2 RTNA 83TJI 01

15 1 RTNA 86TSU 01 Cd (nq/q)

, C

F (uq/q)

37 3 RTNA 84BYR 02 1 55 3 AA 86GAU 01 1 4 COLOR 83JAC 01

1572-3
TABLE 1572-2: INDIVIDUAL DATA FOR NBS SRM 1572 (cont.)

Cone Uncer Com Method Reference Cone Uncer Com Method Reference

Fe (ug/g)

95 7.6 11 AA 75ISA 01 j 5180 270 AA 86GAU

96 8.6 11 AA 75ISA 01 1 5500 300 ICPES 85LY0

102.8 10.5 ICPES 85LY0 01 ! 5600 1.7 11 AA 75 ISA 109 8 ICPES 85ISS 01 1 5600 100 ICPES 85UHI

1 5600 600 ICPES 85ISS

Gd (ng/g) 1 5700 3 11 AA 75ISA

39

H <%>

Ho (ng/g)

8

1.29

1.62

La tng/g)

192

203

Li (ng/g)

0.01

RTNA

TCGS

0.05

0.08

RTNA

lENA

RTNA

86TSU 01

83AND 01

77 3 RTNA 84DEL 01 83 2 RTNA 84BYR 02

83 3 CVAA 86GAU 01

86TSU 01

84FAR 01 84BYR 02

2122

22

23

23.3

24.1

25

Mo Cng/g)

150

153

N (%)

3.62

Ma {u^/B)

162

163

13

6

0.12

0.7

1.9

0.5

15

16

0.04

11

11

28

16

RTNA

RTNA

86TSU 01 83TJI 01

432

(ng/g)

600

830

P (ug/g)

73

50

190

ICPES

ICPES

TCGS

AA

RTNA

ICPES

AA

RTNA

RTNA

TCGS

ICPES

ITNA

RTNA

FAA HPLC

85UHI 02

85ISS 01 83AND 01 75ISA 01 84BYR 02

85LY0 01 75ISA 01

84BYR 02

84BYR 01

83AND 01

85ISS 01 86GAU 01 1.78 0.0004 11 AA 75ISA 01 j 164 13 ICPES 85WHI

1.8 0.0011 11 AA 75 ISA 01 1 1.84 0.03 ICPES 85WHI 02 1 (ng/g)

1.84 0.11 ICPES 85ISS 01 1 1.889 0.007 TCGS 83AND 01 1 202 28 RTNA 86TSU

83TJI 01

86GAU 01 85ICH 01

150 20 AAC 85GAU 04 1 190 10 AA 86GAU 01 1 1300 ICPES 85WHI 02

350 50 AA 85GAU 04 1 1300 100 ICPES 85ISS 01

1 1332 11 ICPES 84PRI 01 Lu (ng/g)

1 1800 100 ICPES 85LY0 01

1.1 0.1 RTNA 83TJI

1 01 1 2 0.4 RTNA 86TSU 01 1 1572-4
TABLE 1572-2: INDIVIDUAL DATA FOR NBS SRM 1572 (cont.)

Cone Uncer Com Hethod Reference

Pb (ug/g)

13.2 0.5 HPLC 85ICH 01 13.6 1.1 FAA 85GAU 04

Pt (tjg/g)

60 30 RTNA 82ZEI 01

S (ug/g)

3600 TURB 84JAC 01 3822 58 ICPES 01 3990 90 CB 86B0U 01 4000 300 CB OHoLA 1 1

1 1 4066 22 IDMS 84KEL 01 4140 D CB 01 4140 100 6 CB 84JAC 01 4160 D CB 01

4160 70 6 CB 84JAC 01 4400 200 TCGS 83AND 01 4590 70 ICPES 85WHI 02

S-32/34 (ratio)

22.631 IDMS 84KEL 01

S-33/34 (ratio)

0.1781 IDMS 84KEL 01

Sb <ng/g)

34 1 RTNA 84BYR 02

Sc (ng/g)

10 3 ITNA 86GAU 01 10.2 1.1 ITNA 84GLA 11

11 ITNA 85GAU 04

Si (%)

0.19

Sm <ng/g?

49

52

0.06

4

8

TCGS

RTNA

RTNA

83AND 01

83TJI 01 86TSU 01

Cone

Sr (ug/g)

93

97

99.3

100.6

102

Tb (ng/g)

9

9

Ti (ug/g)

22

u (ng/g)

37

41

41

V (ng/g)

235

245

W (ng/g)

8.1

Yb (ng/g)

8

15

Zn (ug/g)

28

29

29.7

30

3131.8

Uncer Com Method Reference

5

13.5

2.6

1

14

5

0.5

13

14

0.5

1.5

0.62

4.1

11

11

lENA 85GAU 04

AA 85GAU 04

CPAA 85MAS 01 IDNAA 85YAG 01 AA 86GAU 01

RTNA 86TSU 01 RTNA 83TJI 01

FAA 86GAU 01

DNA 85GAU 04

DNA 84GLA 02

DNA 86GAU 01

RTNA 84BYR 02

IDMS 85 FAS 02

RTNA 84BYR 01

RTNA 83TJI 01 RTNA 86TSU 01

ICPES 85UHI 02

ICPES 85ISS 01 HPLC 85ICH 01 AA 75ISA 01 AA 75ISA 01 ICPES 85LYO 01

1572-5
"8

0)

8(0

a: q: o o o o

oa.

uo

rvi »- «-

ho

o f\J h-

>! <M PJ

o5

00

U. > _1

a: (/>

o

X < Q.

c> in

(M

sO in

OfX

oo(_)

ro <M PJ

vO OO o o

"8

I- 0) O X.a

CO>

(/) ^

UJ z > C

(Q ljOs1—1^

S-

(/)

n •M m c

</) 0) CQ z: z

Q£Ou.<

LU

C3Z < < oUJ

_l

a.zo

Z<

ME ID

UJ

_Jm< c

v>3in C/1 UJ

Vt

H zo C u (0

OJ

Q. a. o o o o Oin

OO

«-

M 00 O

OCO

M

(NJ tofVJ

•H

Oin

tvj CO

-O

(M

oo

o«-

OOO rvi <0 »- o o

a. <A a. a. O UJ u u „ o — —

in «- fM <-

Q£ COuu

Xo

—• —

o^ o 

in

•H lO

ro ro

•o

fM

O

CO

00o

O fVJ o

+) 

00

in

ooO

O Q.

a. (_)

»- (\J

00o

COo - ^\

ro

o to •4 in in\^

ro

PJo in O vO f\J o o o vO o 00 ro ^0 M •H •H • +) -H +1 H H 1 +1 I : S lA +1 (M 1 1 fO PJ 1^ ro 00 t

<\i fM o ro in fM

fVJ in ro

^—\

ro ro pj

o ro ro

00 o>

oo rvi

o 1 1 1 O I 1 1 1 H +1 1 •H H 1 1 1 1 1 1 1 1 1 1 +1 I 1 1 1 1 in OO ro 1 >o 1 1 pj in

<\J

PJ

CO

in

PJ

O CO

ro

in

PJ

COPJ

O

o in To ^ ^ 3 o«4-

CO

in

•OO 00

PJ «- >0 ro

ro

o

o in

roo

1^

PJ

00 00m I «— • 00 in • PJ • • 1 ro PJ PJ00m »- PJ o o o >o CO • »— - in • «- «- in ro o

o OOo PJ ro CO -J- r^

o 1^

PM ro PJ %^ in w »—

>^

PJ ro ro

o PJ PJ PJo in

o -o >o

ro ro O- PJ

ooooo >*o CO PJ

o CO PJ

00H • •H •H roHHHMHH -HHHH

o

o ro ro OO ro in ro ino

o in ro in PJ COo PJ in

o PJ PJ in PJ

in

PJ

«— «— in

COO in

PJPJ

CO

COCD -Hc

oin

oO

M

PJ

«-

o

PJ

PJ

rooo

oo

ino

in

o

O) o> O) O) at cn o> O) cno 1— \ \ \ O) O) O) > o> z c 3 c c c 3 3 3 c 3 »< X 3 3 3 X C 3 C 3 3 3 3 c c

c

O)

—

< <

(0 U> 3 < < <(0 a> CO 00 CD

t- (0"OT3fl>—'OU OOOUUCJCJUOO U) 3 3 3 3 O O O O CJ

O

1573-1
"8

c

o

o

>

111

to c Sat

I—

111 :ii at j=

ac «-•

c

C

4)

Q(A

C

(0

in

CO

CO

O

<

UJ

c

(0

X

C/) (/) C3

u. U. 31 U- O

< »— 0£ < H- X

CNI (VI

Ov O 1 1 II II 1 1 lA 1 1 lA 00 in 1 I 1 I lA 1 1 11 1 1 ro •

* 1 II SI t 1 1 1 r\j •4-

o <r t— (—

Lu a. < ^ -J

</9 u o a. o o — — o <_) > >

o in 00 o in «— • in o 00

•H -H -M S- v}- in

>0 m «-

r>- o (M

" (NJ o in >o tn

CO (/> (/> (A (/> CO

LU UJ lU UJ LU UJ

Q. 0. a. Ll_ a. a. a.

EQ o CJ CJ a: CJ CO o CJ U a. s—

<

X U

AN A% AN AN

CM o <M CM in N^ VA o U-l o o o CM

00 fM o GO to o «— O 1 1^1 1 1 O 1 1 1 II B 1 1 1 O 1 +( • 1 +1 •M fl H •H 1 H

1 1 m 1 1 1 1 1 t 1 o o CO O ro ?J

OJ CM

fM >* o

CM «- <M «- in vO M (M O CM in ro

vO

eo

CM

eo

00 in

00

in

in o CM o o N. CM CM O o O K> m o CM

in O ro H M H in +1 • •H H • (\j <D

:8 o >!• O m in O CM CM

<> CM in O

AN AN A> AN

V* NI- NA O O o ro O 1 1 1 1 1 1 1 1

1 ^ 1 B 1 •H 1 1 •M +1 B •H 1 1

e 1 B 1 o( 1 O <r

1 o

1 1 in CM N»- N* 2

CM

CO o «0 O o CM o o o a. o s CM o- o CM in in o < fN. 00 m ro CO CM O >* <0

a B 1 1 1 u B e t 1 s 0 0 Q B 1 B B B 1 1 B B 1 i 1 1 1 in

1 O1 1 1 O

1 1 o o

1 lA o o nS- <> vO

>*• o o SO CO r^ o o- CM CM vO o * ro in m ro in

T— z UJ < _l 1 1 1 I 1 0 1 «— 1 O 1 sr o in o o CM

03 a O 1 1 1 1 1 1 1 1 o 1 C> o CM o CO < in iX O < t a D I m 8 1 ro 1 CM o m in z

AN N* K) CM ro eo ro in ro ro ro c >* CM nJ- NA NA NA w NA NA NA NA

00 N* o ro 3 o -a- o o CM in O o o o CM

CO f/) CM 00 ro ro o

z o m o CM in o O c\3 ro o o O UJ 1 O 00 o ro o CO •H •H -H I in •H in +1 «— •H •M +) +1 •H *t H H +< •M z t • in CM o

o c m O eo ro ro nS- o ro o N* ro ro O o ro o (D eo o o CM N* in CM in fN. CM

«> in in «

ro f3 <> «2 CM N* O Nt

COOQ

a

c

to Z

roo in

CM

B B 1 B B B B 1 O B o 1 o o 1 1 +1 S B fl B

B B B B

B B 1 1 O I

B B 1 1 T— B

1 *l

1 o

o> o +) 1 B in O o CO 0 nI- ro -o

Nt CM

CO u> O) at O) O) O) D> CD CJ> o> I— •N> Nn •»N N. •Nn •V, Nn N^ N. »v V, 'N. >N, >N. >N

or> o> o> a> > O) o> o> O) > U) o> at UN 3 3 3 3 3 3 c c c c c c c c c 3 3 3 3 3 c 3

111 NA

t—

<

NA

_i <U «i <U «> (Q o H- o c CD 3 C» C C O CO D 111 u. 11. u. u. C3 u Z z _1 _l Z Z Z z z z z z

1573-2
:S - 5 a. ac a. u X u 2

at - 5 o

5a. o o a.

»- ^ «- f\j

c<> C

8 10

4)

o o fQ CO

i~t • • • ^ m >o Ki o

<ooin

eo OCO

in O

t/) M

lU LU </> O. O. Z > O O Q «/>

M

HI

u. a.

a: o CO X —• (J

a. o o C3 «

M < UJ

a. z

u Q

Q. >

— <

a.o

Q.

oCO

c

(00) X

(M in <\J CM ro o

O O oo

<M «— o •* o> o 1 • 1 o vO • 1 1 • <M ( 1 o-

•« -N +< I

I 2

*i 1 in o in i 1 (\j -H 1 I M in +1

1 1 o >* I 1 ^ t t O CO in o in

ro 1*1 <l

>* >d m

vj- o. pg «- M fVJ «- O in

5

c

(D

0)

O <M N.

CO V

CO (M in «-

<0 in

0>

otoino 3 H

in

(Mo

+1 o

fO

vO

(\l

5 c

0)

o «*

•- O

M M

O O in • fo in

lO

in

(M

UJu

Of

o

ro CO o oo fM O (M >0 o

O (M «-

•4- (M >0 in o m <M (M 0> «* ro «- (\i 00 CM vO «- o «-

00 ooCO

>o o

• in m m

o oo

ro (O •sf 00 • in

vj- O -O O fM S- fM 0> fM • 00 m «- (\j o «- in o

QLU

COr- -O ro

ro

in

• o -o -o «- o>in

vt o o

ro r>- in o8 ro

I (M I CO •

fx. O (M ro «-

CO3 O CO M

o c

0)

00 (M N. 00 in o- lO fM ro fM ro fM 00 ro in

fMO 00 in o fM

(M o o <o •o

fM o fM >* fM >o in in ro o O 1 1 f\j o o in fM M -H > CO •H +t *t » •H o +1 +1 ro o M fM +) +1 •H •H

1 1 V o fM V O ro o >* ro fM fM O fM ro o ro in o in in <0 ro in r-. fM

avt

CO

CO c

3C

o ro ofM o

+) +1 o ro

sf vO

ro

o

+1 in

o

ro

roo

+)

>

oroo

om

ro

+1 fM

0)0>0>C7>0)Cr>0)0)0)0>0)0>0>D>0)D)C3)0>0>0>0)0)0>^0>0)0)0)

0> O) 3 3 0)O>0)CD0)0)0)0>C7>0)0)0)n)0>O)O)O)0)0)0)C7)0)O)0)0)O) 33CC3DDCCC3C33CCC3CCDC:C333

JQ ^ ^ -O L. JQ

o. a. a. a. a. a. ae (/>(/></> CO (/> E t. i. CO CO CO W) m S3 jz — —• 3 > 3 >- C C c

1573-3
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Mg ing/g; —

1

1

1 ou SO DTMA n 1 nn 80SLO

1 01 1

1

in

PO

1

1

1

1

1

1

HAA nnn

HAA nnn

R?ocjun inM niu

1

op inu ni

1 310 10

FAA rnn HAARnniiP ni

80TAM 01 OuO 75J0N 02 1 ?o IFMA I unn RPfii OCULMA npUC ceo 75JON 11 1 cou oc o 75J0N 07 1 AuAll fing/g; nn /n\

cow 75JON 08 1 C70 OES 75 JON 06 1 0.8 0.1 RTNA Rn<;i n ni

JC 1 ?7 1

1

I L*r to 81MUN 01 1 OES 75J0N 03 1 o \ UH/ g

;

75J0N 04 1 jy 1 75J0N 09 1 75 5 1 1 irPF<; 70HFD ni

H 1 f H O J \j 85BAR 01 1 76bO o 7S inM 1 n

fJO J 11 S rni np 85BAR 01 1 7fl CO \JC o

7"? IDM n?

75J0N 05 1 79C7 np^ 7"; inu n7

uco 81 GOO 01 1 30 OES 7S.inM n^

21 83SCH 03 1 37 OPS wc o 75 J ON n'?

661 18 11 ICPES 81MUN 01 1 32 OES 75JON 01 835 OES 75J0N 01 1 32 OES 75 J ON 06

1160 ICPES 84NAD 01 1 32 3 35 TCGS 81GLA 04

1170 60 1

1

ICPES 82J0N 01 1 34 2.8 1

1

ICPES 81MUN 01

1225 239 ITNA 77NAD 02 1 35 OES 75 J ON 09

1250 200 AA 83RAP 01 1 35 4 TCGS 84GLA 11

1 280 ITNA 82GLA 02 1 35.5 ICPES 81\J 1 GOO Uwv 01\J I loOU on80 ITNA 80SLO 01 1

1

5o

36.

1

1 .5 1

1

TCGS

ICPES

OcGLA \jc 81MUN 01 Ac t r\n In \

1

1

37

37

OES

OES

75 .ION 08

75JON 05

lis 1 1 o in 7 FAA 82H0E 02 1 •JO 0 1 1 y^r c o R^pRi ni 170 in 7f FAA 82H0E 02 1 42 OPS 75 JON 11 180 40 I1 TUA 1 nn 85NDI 01 1 POO 40 RTMA l\ 1 nn 80SLO 01 1 RTMA i\ 1 nn 79H0E 01 1 7r DTMA i\ 1 nn 80GAL 02 1 OES

1 1 1 1 UAA Finn 81 RAP 01 1 L7 OF^ uco 7S lOM n4

240 IFKIA i c nn 84GLA 02 1 OES 75 JON 11

240 25 RTMA i\ 1 nn 85GAU 04 1 56 5 11 .24 NAA 76GUZ 01 £4d cb 7 FAA 82H0E 02 j 58 OES

?S0 HAA nnn 81KNA 01 1 OFS 7Sjnw 01

1

1

1 1 HAA nnn 81RAP 01 1 ITMA 1 1 nn 77MAn n? HAA nnn 81ARA 01 1 I CPES 84NAD 01

260 30 1ITNA 1 nn 77NAD 02 1 66 3 ICPES 85WHI 02

260 30 11 HAA 81 RAP 01 1 69 14 ITNA 79REN 03

260 80 HAA 81YAN 01 1 270 H ICPES 81PIC 01 1 Be (nq/g)

270 40 RTNA 86GAU 01 1 270 50 MPOES 83SAR 01 1 26 10 ICPES 83SCH 03

290 10 AA 83RAP 01 1 38 4 FAAC 85GAU 04

290 10 COLOR 77BUR 01 1

1573-4
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference

Br (ug/g>

19 1 .5 5 ITNA 80HOE 01 19.8 0.6 5 lENA 79GLA 02

20.1 1.2 5 ITNA 80HOE 01 20.3 1.1 CPXRF 84BIS 01 20.8 2.4 ITNA 80SLO 01

21 1.2 5 lENA 79GLA 02

21 3 ITNA 79REN 03

21.9 0.2 ITNA 77NAD 02

22.5 ITNA 85GAU 04

24.

ITNA 86GAU 01 25.31 1 ITNA 77STE 02

29 2 35 NAA 81GLA 03

54 EXRF 81 PAR 01

;%)

37.67 0.45 CB 82GLA 02

37.8 0.9 CB 77WAT 02

37.92 0.26 CB 80SCH 02

(,%)

c.cc O.Oo ITNA 80SLO A 4 01 OES 75J0N A/04

0.07 ITNA 79REN 03

o / o OES 75J0N 07

O / T 2.43 OES 75JON A703

2.!>D OES 75 JON 02

2.62 OES 75 JON 08

2.64 OES 75JON 10

2.63 0.07 6 EXRF 79MAT 01

2. r 0.02 CPXRF 84BIS 01 2.70 0.21 NAA 76GUZ 01 2.75 0.005 11 AA 75 ISA 01 2.8 OES 75JON 11 2.85 ICPES 81 GOO 01 2.86 0.05 1

AA 84SUZ 03

0.005 1

AA 75 ISA 01 2.88 0.27 ICPES 85LYO 01 2.9 0.05 11 AA 84SUZ 03

2.91 OES 75J0N 05

2.91 0.08 ICPES 85WHI 02

2.92 OES 75 JON 09

2.92 0.08 6 EXRF 79MAT 01 2.92 0.12 11 ICPES 81MUN 01 2.93 0.045 ICPES 83SCH 03

2.99 0.05 11 ICPES 82JON 01 2.99 0.12 11 ICPES 81HUN 01 3.04 0.05 11 ICPES 82J0N 01 3.08 0.05 11 ICPES 82J0N 01

1573-5

Cone Uncer Com Method Reference

Ca (%) cont.

3.1 ITNA 82GLA 02

3.1 0.03 11 ICPES 82 J ON 01 3.19 OES 75 JON 06

3.28 OES 75J0N 01 3.41 0.09 ICPES 79HER 01 3.49 0.12 ITNA 77NAD 02

3.55 ICPES 84NAD 01 5.82 EXRF 81 PAR 01

(ug/q)

1 .6 4 4 11 FAA 80PRE 01

2.1 6 POL 72SIN 01 2.2 11 FAA 80PRE 01 2.3 11 FAA 80PRE 01 2.3 FAA 80PRE 01 2.3 11 FAA 80PRE 01 2.3 ICPES 84NAD 01 2.3 11 FAA 80PRE 01 2.3 0.1 FAA 80LEG 01 2.4 0.01 11 ICPES 82J0N 01 2.4 0.22 6 POL 72s IN A 4 01 2.5 FAA 82PRE 01 2.5 ASV 82GAJ A 4 01 2.5 A 4 0.1 ICPES 83SCH A^03

2.55 A Aft 0.09 4 4 11 ICPES 82 J ON 01 2.56 A AZ 0.06 4 4

1ICPES 82 J ON A 4 01 2.6 A 4 0,

4 4 11 ICPES 82J0N 01 2.6 A O 0.2 FAA 84GLA 11 2.6 0.3 11 ICPES 81MUN 01 2.66 0.1 FAA 83DEL 01 2.7 ASV 74COP 01 2.7 0.4 RTNA 80SLO 01 2.7 0.5 11 ICPES 81MUN 01 2.74 0.2 ASV 82SAT 02

2.8 0.2 AA 80SCH 05

2.8 0.2 FAA 84GLA 02

2.8 0.2 D FAA 80SCH 08

2.9 0.1 FAA 81KNA 01 2.94 0.15 AA 83RAP 01 3 0.16 ICPES 83SCH 04

3.3 0.2 ICPES 79HER 01

(uq/g)

1 0.1 RTNA 80SLO 01 1.28 0.18 ITNA 86<RA 01 1.3 0.36 RTNA 83TJI 01 1.559 0.114 RTNA 86TSU 01
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference

CI (%)

1 f)L n n? 1 1 nn ftn^i n ni

U U r CJ T1 TMA 1 M« 775TF f r d 1 C n?

n i?ni MAA 7/ini 17 ni

1.1 0.07 ITNA 77NAD 02

> (nq/q)

inn 1 uo NMM 7Ar:) 17 r OuU^ ni

'Of I1 TM/1 1 nM ni AOS r nn OcnUC ni sn7 9n 1 1 Kn ni Rin in 1

1

FAA OUrUU ni

SAn xn DTBJ A K I nn OUdLU ni

in 11 ni

n xn T TUA n?

Awn I TUA

1.5 0.2 1

1

ICPES 81MUN 01 2.28 0.06 1

1

ICPES 82 J ON 01 2.5 0.2 1

1

ICPES 81 MUM 01 3 ICPES 81 GOO 01 3.1 11 AA 79HOE 02

3.107 1 .08 NAA 76GUZ 01 3.7 0.3 ITNA 02

3.8 0.2 1

•) ICPES fl?JOM 01 3.8 0.3 35 FAA 81RI A 03

01 3.9 0 3 1 TMA 77NAn

9 y • i 1

1

rpypc OHO i n U 1 3.94 11 AA 79HOE 02

4.3 FAA 82H0E 01 4.3 AA 81ARA 01 4.3 0.2 AA 83RAP 01 4.3 0.5 ICPES 83SCH 03

4.4 0.2 11 CPXRF 84SIM 01 4.4 0.2 D CPXRF 84SIH 02

4.5 1.6 ITNA 79REN 03

4.53 ICPES 84NAD 01 4.6 11 AA 79H0E 02

4.6 0.7 FAA 85GAU 04

5.15 0.29 ITNA 86KRA 01 5.9 0.2 ICPES 79HER 01

Cone Uneer Com Method Referenee

Cs (nq/g)

A"? c

1

1 TUA 1 NH 77UAn f /NAU uc

L** I TklA 1 1 NH AAn A Uc

1 1 NA OOuAU niU 1 Ao T

1 TUA 1 nn 77fil 17 U 1 jO * T

1 TUA 1 NA AAri A 1

1

1 1 OH ?1 I

i TUA 1 NA AA^D A OOIS.KA ni

7C\ f U o

1 TUA 1 1 NA ODuAU n/.

1 AH ^n 1 TUA 1 1 NA f VKtN n7

vug/g;

AAAA A1 ADA O 1 AKA niU 1 A 1 O. 1 1 1 T TUA 1 1 NA niU 1 AO.TO n 7 PDVD C Q / Die OhdI o

ni

n 7 AKr OjAVA niU 1 7e , 71 o DDI rUL 7PC 1

U

r Col

N

ni 7f 7r n s o pni f CO 1 n ni

ao I CO ni

ft ? 1

1

oc wijn ni

ft 7 11 • 9T AA 01 9 02vC

9 4 A MAA PIMM f Co 1 n ni 9 4 1

1

T rPF^ 01 9T.J5 1

1

irPF^ I Or CO ucuvn 01 9T.JS 11 11 I CO u 1 nun 01 9T • 7f

I\ PPF^CO ujo^n 03

9 ft 0 3 1 CO ft'^^PH uJOL*n 04

0T*0A n 4 1 1 1 1 1 PPFC A7Oc JUn inu ni

in nFC UCo 7*5 inu n'^

in 1 n 4 PTUA 7ApAW f •RnV ni

in 4 T PPFC 70UFP ni

in L 1 1 T

1 PPF^ L«r Co OCQOJUN inu ni

in A n A VV ououn n";

in > n ft DTUA K 1 NA OUoLU ni

in A n 1 1 UPlo AArpo OHDKU n'?

inlU.OA n AAAA AXD 0->KArAD ni

in 7 n L T

1 rocc UrCo AHcru nft uo 10.8 0.1 COLOR 76ZAN 02

10.81 0.02 COLOR 77BUR 01 10.9 0.1 D AA 76ZAN 02

10.9 0.1 AA 76ZAN 01

11 FAA 83ATS 01

11 OES 75J0N 04

11 1 11 AA 84SUZ 03

11 1 6 AF 83MCC 02

11 2 6 AF 83MCC 02

11 2.4 CPAA 85CAN 01

11.1 0.2 7 RTNA 80GAL 02

11.2 11 AA 79H0E 02

11.2 0.2 AA 85K0J 01

1573-6
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Cu (ug/g) cont.

1

1 Fe (ug/g)

1 55 OES 75JON 01

11.5 0.2 AA 76EPS 02 1 162 OES 75J0N 09

12 11 AA 79H0E 02 1 207 6.3 11 AA 84SUZ 03

12 0.14 11 AA 75ISA 01 1 220 AA 81ARA 01

12 0.17 11 AA 75ISA 01 1 266 OES 75J0N 06

12.2 1.3 6 EXRF 79MAT 01 1 267 OES 75J0N 03

13 OES 75J0N 10 1 340 OES 75J0N 02

13 0.7 11 AA 84SUZ 03 1 342 OES 75J0N 04

13.5 0.4 AA 77GUZ 01 1 350 OES 75 JON 11

14.1 1.3 ITNA 77GUZ 01 j 361 50 11 ICPES 81MUN 01

14.1 5.64 NAA 76GUZ 01 1 379 OES 75J0N 08

15 OES 75J0M 09 1 442 115 11 AA 75ISA 01

15 OES 75 JON 01 1 450 17 11 AA 84SUZ 03

15 OES 75 JON 11 1 463 157 11 AA 75ISA 01

15 OES 75J0N 06 1 469.25 118.3 NAA 76GUZ 01

15 3 AA 86GAU 01 1 478 OES 75 JON 05

17 OES 75 JON 05 1 507.6 14.3 ITNA 77GUZ 01

17 OES 75J0N 08 1 531 14 11 ICPES 82J0N 01

20 OES 75JON 07 1 534 OES 75 JON 10

25 EXRF 81 PAR 01 1 546 19 ICPES 83SCH 03

1 550 36 CPXRF 84BIS 01 Dy (ng/g) 1 552 OES 75 JON 07

1 568 3 ICPES 79HER 01 68 4 RTNA 86TSU 01 1 575 10 11 COLOR 82SCH 03

1 597 11 COLOR 82SCH 03

Er (ng/g) 1 602 28 6 FAA 84FUD 02

1 604 11 11 COLOR 82SCH 03

51 3 RTNA 86TSU 01 I 614 14 6 AF 83MCC 02

1 623 10 6 EXRF 79MAT 01 Eu (ng/g) 1 625 14 11 ICPES 82J0N 01

1 632 ICPES 81GC0 01

15 2 ITNA 77GUZ 01 1 636 65 ICPES 85LY0 01

16 3 RTNA 83TJI 01 1 642 17 11 ICPES 82J0N 01

25 5 ITNA 77NAD 02 1 657 ICPES 84NAD 01 26 1 RTNA 86TSU 01 1 658 18 11 ICPES 82J0N 01 27 7 ITNA 86KRA 01 1 661 14 ITNA 77NAD 02

55 8 RTNA 80SLO 01 j 665 11 AA 79H0E 02

1 668 25 11 ICPES 81MUN 01

F (ug/g) 1 670 50 35 ITNA 81GLA 03

1 672 11 AA 79H0E 02

5 1 MS 77STE 02 j 674 97 ITNA 86KRA 01 5.4 1.3 ISE 85GAU 04 j 675.8 18.9 CPAA 85CAN 01 5.7 0.2 ISE 83KNA 01 1 684 9 6 FAA 84FUD 02

6 0.7 ISE 84GLA 02 ! 685 20 D ICPES 80SCH 08

9 COLOR 83JAC 01 1 685 20 ICPES 80SCH 05

1 685 50 6 AF 83MCC 02

1 698 VOLT 81SZY 01 705 30 AA 83RAP 01 706 12 ITNA 790AS 01 706 12 RTNA 80SLO 01 730 90 ITNA 79REN 03

831 10 6 EXRF 79MAT 01 1170 EXRF 81PAR 01

1573-7
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference

FeCIl) (uq/g)

540

Fed II) (ug/g)

158

Ga (ng/g)

250

Hg (ng/g)

Ho (ng/g)

13

I (ng/g)

In (ng/g)

0.96

VOLT

VOLT

20 ITNA

RTNA

0.08 RTNA

81SZY 01

81SZY 01

69.3 67 NAA 76GUZ 01 83 FAA 85X1

A

01

Gd (ng/g)

74 15 RTNA 83TJI 01 76 5 RTNA 86TSU 01

H <%>

5 0.1 35 TCGS 79GLA 04

5.1 0.2 CB 82GLA 02

5.14 0.07 CB 80SCH 02

86KRA 01

90 8 ITNA 77NAD 02

91 11 CVAA 82GLA 02

128 118 NAA 76GUZ 01

86TSU 01

280 30 lENA 82SAT 01 300 100 PAA 77WIL 01 390 120 RTNA 77STE 02

74RAV 01

Cone Uneer Com Method Reference

La (ng/g)

346

630

640

677

766

770

800

2.68 0.26 11 ICPES 81MUN 01 2.9 ICPES 84NAD 01 3 0.29 ICPES 79HER 01 3.8 OES 75JON 02

3.81 OES 75JON 10

3.85 OES 75J0N 07

4.055 1 AA 78SZY 01 4.15 0.08 ITNA 79REN 03

4.17 1 AA 78SZY 01 4.18 0.4 ITNA 86KRA 01 4.25 OES 75 JON 04

4.3 0.2 11 ICPES 82J0N 01 4.33 OES 75J0N 08

4.34 0.18 ICPES 85UHI 02

4.34 0.23 11 ICPES 81MUN 01 4.39 0.09 CPXRF 84BIS 01 4.4 0.1 11 ICPES 82 J ON 01 4.4 0.2 11 ICPES 82J0N 01 4.4272 0.2816 NAA 76GUZ 01 4.47 0.15 ITNA 80SLO 01 4.47 0.24 ITNA 77NAD 02

4.49 ICPES 79C00 01 4.51 OES 75 JON 09

4.58 OES 75JON 03

4.58 0.0046 11 AA 75ISA 01 4.6 OES 75J0N 06

4.6 0.0083 11 AA 75ISA 01 4.6 0.2 11 ICPES 82J0N 01 4.73 0.14 11 AA 84SUZ 03

4.74 OES 75J0N 05

4.79 0.06 6 EXRF 79MAT 01 4.8 OES 75J0N 11 4.81 0.09 11 AA 84SUZ 03

5.16 0.06 6 EXRF 79MAT 01 5.72 OES 75J0N 01 9.24 EXRF 81 PAR 01

79

90

40

13

199

110

200

NAA 76GUZ 01 ITNA 86KRA 01 ITNA 77NAD 02

RTNA 86TSU 01 RTNA 83TJI 01 RTNA 80SLO 01 ITNA 79REN 03

1573-8
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Lu (na/a) 1 Mn (ug/g) cont

.

1 215 27 FAA 84KUR 01 7 1 RTNA 83TJI 01 1 216 17 11 AA 75 ISA 01 9 1 RTNA 86TSU 01 I 217 11 AA 79H0E 02

12 2 RTNA 80SLO 01 1 217 5 11 ICPES 82J0N 01

1 217 16 11 ICPES 81MUN 01 Ma (uq/q) 1 218 13 11 AA 75ISA 01

1 219 7 ICPES 85WHI 02

5365 ICPES 81 GOO 01 1 221 5 11 ICPES 82J0N 01 6000 OES 75J0N 08 1 222 5 11 ICPES 82J0N 01 6000 600 ITNA 80SLO 01 1 223 11 AA 79H0E 02

6100 600 ICPES 79HER 01 1 223 7 6 EXRF 79MAT 01 6300 OES 75J0N 09 1 224 2.6 11 AA 84SUZ 03

6400 400 ICPES 85LY0 01 1 225.6 17 ICPES 85LY0 01 6500 300 ICPES 85WHI 02 1 227 OES 75JON 05

6600 OES 75 JON 07 ! 227 7 6 AF 83MCC 02

6672 186 11 ICPES 81MUN 01 j 230 OES 75 JON 03

6700 3 11 AA 75ISA 01 1 230 5 11 ICPES 82JON 01 6700 3 11 AA 75ISA 01 ! 230 9 6 AF 83MCC 02

6700 200 11 ICPES 82J0H 01 1 231 3.6 11 AA 84SUZ 03

6784 206 11 ICPES 81MUN 01 j 231 8 11 ICPES 81MUN 01 6800 ICPES 84NAD 01 j 231 10 ITNA 80SLO 01 6800 OES TSJON 10 1 232 ICPES 84NAD 01 6800 90 ICPES 83SCH 03 I 233 13 ICPES 83SCH 03

6900 OES 75JON 04 1 234 5 W 80SCH 05

6900 200 11 ICPES 82J0N 01 j 234 5 0 ICPES 80SCH 08

6900 200 11 ICPES 82J0N 01 j 235 2 m 84SUZ 01 7000 OES 75J0N 03 j 235 4 6 FAA 84FUD 02

7000 100 11 AA 84SUZ 03 ! 235 5 ICPES 79HER 01 7000 200 11 AA 84SU2 03 j 236 5 6 FAA 84FUD 02

7000 200 11 ICPES 82JON 01 ! 238 17 ITNA 77NAD 02

7100 OES 75 JON 02 1 240 4 ICPES 83SCH 04

7300 100 ITNA 1 J NAD 02 j 241 OES 75 JON 08

7400 OES 75J0N 05 1 241 12 AA 83RAP 01 7400 OES 75J0N 06 i 251 OES 75J0N 01 7400 OES 75J0N 11 1 252 ICPES 81G00 01 7800 OES 75J0N 01 i 266 ITNA 82GLA 02

1 266 8 6 EXRF 79MAT 01 Mn (ug/g) 1 414 EXRF 81PAR 01

138 OES 75J0N

1 07 i Mo (ug/g)

189 OES 75J0N 10 1 0.4 0.2 11 ICPES 82JON 01 189 OES 75J0N 04 i 0.5 0.1 11 ICPES 82J0N 01 197 OES 75J0N 09 i 0.5 0.1 11 ICPES 82JON 01 198 OES 75 JON 06 { 0.5 0.3 11 ICPES 82 JON 01 200 ITNA 79REN 03 1 0.62 0.04 ITNA 77NA0 02

200 9 CPXRF 84BIS 01 1 0.65 0.1 RTNA 80SLO 01 209.18 9.93 NAA 76GUZ 01 1 OES 7SJ0M 10

209.2 11.9 ITNA 77GUZ 01 1 4.2 OES 75 JON 11 210 OES 75 JON 02 1 4.5 OES 75J0N 03

211.1 2.1 AA 77GUZ 01 1 11.7 OES 75J0N 01 215 OES 75 JON 11 1 14.6 OES 75J0N 07

1 17.9 OES 75J0N 02

1573-9
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Cotn Method Reference

N (%) 1 P (uq/q)

4.9 0.2 35 TCGS 79GLA

1 04 1 2400 OES 75J0N 04

4.94 0.11 CB 80SCH 02 1 2700 ICPES 84NAD 01 4.95 0.08 CB 82GLA 02 1

1

2800

3030

OES

ICPES

75J0N

81 GOO

10

01 Na (uq/q) 1

1

3100

3200

OES

OES

75 JON

75 JON

07

05

326 18 11 ICPES 81MUN 01 1 3200 200 6 FAA 81 LAN 01 332 4.9 11 AA 84SUZ 03 1 3263 130 11 ICPES 81MUN 01 337 13 11 ICPES 81MUN 01 1 3300 OES 75J0N 09

337 23 11 AA 84SUZ 03 1 3300 OES 75JON 08

350 OES 75 JON 04 1 3300 OES 75JON 11 369 16 ICPES 85UHI 02 1 3300 OES 75J0N 06

388 OES 75J0N 02 1 3300 200 6 FAA 81 LAN 01 459 46.1 NAA 76GUZ 01 1 3300 200 ICPES 85WHI 02

475 25 ITNA 80SLO 01 1 3318 106 11 ICPES 81MUN 01 488 1 AA 78SZY 01 1 3320 160 ICPES 81 OWE 01 500 200 ITNA 79REN 03 1 3400 OES 75J0N 03

520 ICPES 81 GOO 01 1 3400 FAA 79EDI 01 522 13 ITNA 77NAD 02 1 3400 ICPES 79EDI 01

531 OES 75J0N 08 1 3400 100 11 ICPES 82J0N 01 568 ICPES 84NAD 01 1 3400 200 CPAA 83MAS 02

602 1 AA 78SZY 01 1 3420 89.5 NAA 76GUZ 01 610 OES 75JON 06 1 3459 8 ICPES 84PRI 01 618 18 ITNA 86KRA 01 1 3500 100 11 ICPES 82JON 01 650 OES 75J0N 03 j 3500 100 11 ICPES 82J0N 01 800 OES 75J0N 01 1 3500 100 11 ICPES 82J0N 01 820 OES 75J0N 09 1 3500 200 6 FAA 81 LAN 01 950 OES 75J0N 05 1 3700 100 ICPES 79HER 01 1090 70 ITNA 82SCH 05 1 3800 OES 75JON 02

1600 OES 75 JON 11 1 3900

5000

200 ICPES

OES

85LY0

75JON

01

01 Nd (nq/g) 1

1 Pb (uq/q)

566 59 RTNA 86TSU 01 1 580 140 RTNA 83TJI 01 1 3.2 6 POL 72SIN 01 700 100 RTNA 80SLO 01 1

1

4

4.3 0.2 11

ASV

ICPES

74C0P

82J0N

01

01

Ni (ua/a) 1

1

4.5

4.9

0.1 6

11

POL

FAA

72SIN

80PRE

01

01

< 1.5 11 ICPES 81MUN 01 1 5.0 0.2 11 ICPES 82JON 01 0.3 0.2 RTNA 80SLO 01 1 5.2 0.8 AA 84KAN 01

1.1 0.08 11 ICPES 82J0N 01 1 5.4 6 FAA 81JAC 01 1.12 0.06 11 ICPES 82J0N 01 1 5.5 11 FAA 79H0E 02

1.12 0.08 11 ICPES 82J0N 01 1 5.5 0.4 FAA 80LEG 01 1.2 0.3 ITNA 77NAD 02 1 5.6 6 FAA 81JAC 01 1.3 0.2 11 ICPES 82J0N 01 1 5.6 0.2 ASV 82SAT 02

1.5 0.8 11 ICPES 81MUN 01 1 5.7 11 FAA 79H0E 02

1.7 0.4 ICPES 83SCH 03 1 5.8 6 FAA 81HIN 01 5.9 0.6 ICPES 79HER 01 1 5.8

5.8

6

6

FAA

FAA

82K0I

81HIN

01

01

1573-10
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Pb (ug/g) cont

1

1

1

S (ug/g)

5.8 6 FAA 82K0I 01 1 5500 300 CB 84GLA 1

1

5.8 0.8 HAA 82UEI 01 1 5848 58 ICPES 84PRI 01 5.9 11 FAA 80PRE 01 1 5860 270 CB 86B0U 01 5.9 0.5 XRF 85AVA 01 1 5960 150 UXRF 86B0U 01 5.95 0.06 FAA 79DAB 02 1 6260 D CB 85JAC 01

6 FAA 82H0E 01 j 6260 100 6 CB 84JAC 01 6 11 FAA 80PRE 01 j 6360 190 CB 86GAU 01 6 ASV 82GAJ 01 I 6550 D CB 85JAC 01 6.0 0.5 FAA 84GLA 11 j 6550 90 6 CB 84JAC 01 6.03 0.15 IDMS 83BR0 All 1 01 1 6900 300 ICPES 85WHI 02

6.1 FAA 83 HOE 01 1 6.1 11 FAA 79H0E 02 1 Sb (ng/g)

6.1 0.3 AA 80SCH 05 ! 6.1 0.3 D FAA 80SCH 08 1 30 1 RTNA 79H0E 01 6.2 FAA 80PRE 01 1 30 2 RTNA 80KOS 02

6.2 0.3 FAA 81KNA 01 1 34 HAA 82KUE 03

6.23 0.97 CPAA 85CAN 01 1 40 2 ITNA 77NAD 02

6.3 11 FAA 80PRE 01 1 46 20 ITNA 86KRA 01 6.3 0.5 ICPES 83SCH 03 1 120 30 7 RTNA 80GAL 02

6.4 0.1 AA 83RAP 01 j 120 50 ITNA 79REN 03

6.4 0.3 FAA 82ATS 02 1 6.55 0.22 ASV 80SZY 01 i Sc (ng/g)

6.6 FAA 82PRE 01 f 7.1 0.9 FAA 82WEI 01 1 138 7 ITNA 77GUZ 01 7.5 11 FAA 80PRE 01 j 151 4 ITNA 84GLA 1

1

7.6 3.1 FAA 85GAU 04 1 160 30 ITNA 79REN 03

8.1 1.8 11 ICPES 81MUN 01 1 164 16 ITNA 86GAU 01 8.3 1.1 ICPES 79HER 01 1 170 3 ITNA 77NAD 02

9.1 2.9 11 ICPES 81MUN 01 1 175 1 ITNA 85GAU 04

15 EXRF 81 PAR 01 j 175 4 ITNA 86KRA 01

1 208 89 NAA 76GUZ 01 Pd (ng/g) 220 30 RTNA 80SLO 01

< 2 RTNA 85BEH 01 j Se (ng/g)

1 49 5 ITNA 77NAD 02

50 20 RTNA 80KNA 01 ISA 11 RTNA 86TSU 01 1 57 3 11 GC 81UCH 02

190 40 RTNA 80SLO 01 1 61 2 11 GC 81UCH 02

1 84 15 9 ITNA SOMAN 01 Rb (ug/q) 1

1 Si (Uq/Q)

15.16 1.35 NAA 76GUZ 01 1 15.21 2.3 ITNA 79REN 03 1 3000 ICPES 84NAD 01 16.4 0.5 ITNA 77GUZ 01 1 16.5 0.7 ITNA 77NAD 02 1 Sm (ng/g)

16.8 0.9 ITNA 86KRA 01 1 19.2 1.8 CPXRF 84BIS 01 1 81 3 RTNA S6TSU 01 22 3 35 ITNA 81GLA 03 1 86 27 RTNA S3TJI 01 40 EXRF 81 PAR 01 1 110 15 RTNA 80SLO 01 200 90 ITNA 79REN 03

1573-11
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Sr (ug/g>

1

1

1

V (ug/g)

35.6 1.4 lENA 85GAU 04 1 0.31 0.045 11 RTNA 82HEY 02

36 0.6 ICPES 79HER 01 1 0.87 0.013 11 RTNA 82HEY 02

38 OES 75J0N 04 1 0.888 0.013 11 RTNA 82HEY 02

38 OES 75 JON 03 1 1.19 0.01 11 ICPES 82J0N 01 42.

2

0.8 AA 86GAU 01 1 1.27 0.035 RTNA 78BYR 01 42.9 0.5 CPAA 85CAN 01 1 1.297 0.112 ITNA 82HEY 02

43.7 0.2 AA 85GAU 04 1 1.3 0.2 ITNA 77NAD 02

44 2 CPXRF 84BIS 01 1 l!.42 0.08 11 ICPES 82JON 01 44.8 0.5 CPAA 85MAS 01 1 1.5 0.2 ICPES 83SCH 03

45 1 ITNA 77NAD 02 1 45.3 0.4 IDNAA 85YAG 01 j W (ng/g)

54 OES 75J0N 01 1 65.5 5.84 NAA 76GUZ 01 1 < 40 L RTNA 80SLO 01 102 EXRF 81 PAR 01 1

1 Yb (ng/q)

Ta (ng/g) 1

1 47 10 RTNA 83TJI 01 430 300 ITNA 79REN 03 1 63 4 RTNA 86TSU 01

1 80 20 RTNA 80SLO 01 Tb (na/g) 1 Zn (ug/g)

4 1 RTNA 80SLO 01 1 12 2 RTNA 86TSU 01 j 26 OES 75J0N 09

12 4 RTNA 83TJI 01 j 29 ASV 74C0P 01

1 48 OES 75J0N 10

Th Cng/g) 1 50 OES 75 JON 03

1 52 1 11 ICPES 82J0N 01 190 20 ITNA 77NA0 02 1 53 FAA 83ATS 01 220 30 RTNA 80SLO 01 1 54 4 RTNA 80SLO 01

1 55 3 XRF 85AVA 01

Ti (ug/g) 1 56 2 11 ICPES 82J0N 01

1 56.8 7.3 ICPES 85LY0 01 12.6 1 ICPES 83SCH 03 1 57 2 11 ICPES 82J0N 01 68 9 ITNA 77NAD 02 1 58 OES 75JON 01 89 8 COLOR 84GLA 11 1 58 OES 75J0N 06

1 58 1.5 11 AA 84SUZ 03

Tl (ng/q) 1 58 4 6 AF 83MCC 02

1 58.03 3.33 NAA 76GUZ 01 20 11 ASV 84LIE 01 i 58.9 11 AA 79H0E 02

24 11 ASV 84LIE 01 1 59 ICPES 81 GOO 01

1 59 OES 75JON 11

U (nq/g) 59 2 11 ICPES 82JON 01 59 3 11 ICPES 82J0N 01 20 20 RTNA 80SLO 01 1 59 3 AA 83RAP 01 50.2 2.3 RTNA 780ER 01 1 59.5 2.2 ICPES 83SCH 03

54 DNA 84GLA 02 1 60 OES 75 JON 02

60 120 R* DNA 81GLA 03 1 60 2 6 AF 83MCC 02

63 3 35 DNA 80GLA 04 1 60 3 11 ICPES 82J0N 01 63 4 DNA 86GAU 01 1 61 6 AA 72SIN 01 63 6 DNA 85GAU 04 1 61 3 ICPES 85WHI 02

1573-12
TABLE 1573-2: INDIVIDUAL DATA FOR NBS SRM 1573 (cont.)

Cone Uncer Com Method Reference I

Zn (ug/g) cont.

62 ICPES 82J ON 01 62 4 ITNA 77NAD AO02

62 4.6 ITNA f vRcN 1)5 62.5 AA 81ARA 01 62.3 1 .2 CPAA 85CAN f\ 4 01 62.9 6 POL 72SIN r> 4

62. y

i

"7

1 . f 6 POL Too T kl f 2S1N Ul

2.3 4 41 1 AA 75 ISA 01 6J. 3 1 .3 1 1 ICPcS oiMUN n401

o*f 1 1 ICPcS 82 J ON n 4 01 03 OJON 0/ AKOj 7C I/Ml /3J0N 03

J . c3 1 1

1 1 AA -TC 1 OA r31dA U 1 65 7 ICPES 80SCH 05

65 7 D ICPES 80SCH 08

66 2.2 11 AA 84SUZ 03

66.4 8 CPXRF 84BIS 01 66.6 4.6 11 ICPES 81MUN 01 68 11 AA 79H0E 02

68 FAA 83ATS 01 68.5 1.7 ITNA 86KRA 01

71 2 ICPES 83SCH 04

72.8 2 6 EXRF 79MAT 01 73 3 ICPES 79HER 01 75 OES 75J0N 08

78 2.1 6 EXRF 79MAT 01 86 OES 75J0N 04

124 EXRF 81 PAR 01

1573-13
Si

*-> c•—

3 a

3: 01

UJooo

ooo

UJOoo

IM

a.uo

CO rvi

o—J LU C/) O </) LU U- (J — O <

«- r\j 0>

S.

o >< o

CO

o

COo

CO

"8

JZ

OX

CO

c

xKl

"O

0) 0

UJ

Q. > u *i

L_

C

(0

CO

UJ

_lUJ

J—.

UI

c z

UJ

00

Q. < Ln «c

iO

<ll z:

a;

(A ^

ea

C

3C

Of0 0 < < +< <0 c QUJ

—I

o.

5:0u UJ< 1 in

in

UJ

—JCO a: < <

83

u^ CNJ

CO QC

o

M sj- roM ro

»~

w

ww

CO

in COo -*

o (M in

>t

o o> lO om

ino

COm

u.

—I (/> a: O yj X <J 0 o rjO (M O O fVJ

Oo

ro

M CM

r\j ^

0> CO

in

-o"

o

CO fx fM

X^ 0 fO 0 0 Kl 0 ro 0 so (M in f\J N- 0 0 CM CM

>» 0 t ) 1 1 1 1 •H 0 H •M H M 1 t 1 1 1 • 41 1 1 41 1 1 1 1 1 1 1 1 i 1 0 sO in (x

*— to CO

in »—

M rj ro •C » Kl

*^ >^ 0 0 <\J 0 -t ro ro -0 s» •0 CM CM CM si- in "—

X^ x^ ^

in

CO 0 >!• 0 0 0 CO m f1 0 0 0 0 CO PvJ in 0 m (M 0 0 IX

sO <> (NJ 1 1 1 CO 1 0 in

M •H •H 41 « 'M +< +1 41 41 I 1 44t 1 41 i CM 41 0 1 1 1 0 (M 0 0 0 0 CO tx O; in 0 0 0- 0 IX rvj in 0 0 0 -0 tM T— rvi (M m CM

rvj J-

*^

0- Kl

•.^ ^> ' '

PJ fO

vO CM

rj 0 0 1 1 0 0 1 1 1 1 1 1 1 1 1 0 +* M 1 1 1 +1 44 44 1 1 +1 • 1 t 41 1 1 1 1 1 1 1 1 t 1 CO in 0 in Kl >o in 0 »- m rj <M oCM

8: 0 0 0 0 00

m 0 •0 inm IX in 0 0 0 0 0 0 0 in 0 -J- CM in -0 in

nj 0 CM 00 CO

mm CM ro K> 1 <> CM 1 1 Kl in CM 0 -0 IX 1 0 0 0 lO 0 CM 1 1 11 CM t CM 1 t1 CO 1 1 1 1 0 0 0 0

CO 0 »»

m 0 Kl CM 0 K) 0 m >o CM CM s. 0 • CM 0 c 0 0 m -J 1 u^ S : r in I 1 |x CM 0 IX 0 CO 0 ' CO • 0 Kl 1 •^i in CM -o in »— CM ' CM «- 1 r\j 1 >o f o -

CM CM 00 CM Kl CO 0 Kl in sO >0 >o •* Kl 4- ^0 Kl CM in CM 0 in Kl

c X/ IM INJ CM CM x/ Kl x< x^ Kl X' '—

x^ x^ CM x^

x^ X'w v_« X*

t/5 CO 00 3 00 0 0 CM -J- Kl ^. 0 vO

in t/) 0 CO •0 0 0 0

3E •Q 0 0 0 Kl vO

m Kl 0 0 0 CM 0 Kl -J- 0

UJ 0 0 1 1 CO Kl in 0

</> 41 in 44 41 +1 41 44 41 41 44 41 44 41 44 41 44 1 41 41 41 CM 41 CM 44 sT 41 44 sT +1 0 1 St Kl 0 C IX CM o> 0 0 CM >o 0 m 00 in 00 «* 0 0 a: >» 0 CM CO CM CO St rx <l

01 in CM (X >o CM CM CM CM CM 4— K> in CM 0 -4- Kl

in 0 0 CM Kl 0

</> 0 0 0 0 0

Kl xr CM 0 0 m CM

(/) 1 0 0

CD 44 44 44 «>• 41 41 44 >o 44 +H 44 z m CM c in 0 0 >0 0 0 0 0

HI 0 V 0 m 0

OJ in CM CM Kl CM IX

-» Kl

h- cn O) o> 01 a> CJ) O) 01 o> 01 O) O) 01 01 O) C3) 01 O) o> 01 01 O) Ol 01 01 O) C31 01 CD X, X, x^ X. *x *x x^ — x^ X, "x x '

X, X,

X

XX X,XX *x X,

X *xXX

Z O) 131 CD 01 O) D) D) 01 O) 01 01 o> C71 cn o> O) 01 tJ> 01 O) 01 o> 01 O) 01 o> 01 01 D) O) D> 3 c C c 3 »< c c c 3 c 3 3 3 c 3 3 3 3 c J* C c C 3 C c C

UJ 6 —1

13 IS

u <D 0 D 01 0 1- (ft 3 3 3 3 01 01D CM 01 <0 3

UJ < < < CO CO CO CO CJ CJ CJ CJ 0 0 0 <->

u CJ 0 LU u_ u. 0 x;

1575-1
"8

c

8 n>

I- I

ai jz o X

c

a

• *-» c c o

u o to

LU UJ

_1 a. a +4 UJ c z <oa> LU z: z

CLin c

in o 3e: (/) a: < (o <

H

C/) CO c z <s

0) Q£ s: O

<t

c <

o

o LU w

-J <<

§ c u Id

m

in

LUO

UJ z

_i <

cs<

CO T— rO

O

o

:8

Oo CO

o om

t/) UJ

CJ a. CO s: CJ u y 1

O

Irt ro 1 1 <o o

I ^'

I 1 C>J Q

CO tn u. u. m UJ ce o O X

c '"^ o m

o in 1 « 1 1 •H 1— CVJ ' «— 1 fO o >o in

f\J CO

^\ *—

in o

in CO o o to

K. o

o Kl o

+1 -N *i

1

1 44

1

1 M

O o

1 O>

>*• N.

r— o f\J *

o

8

o

O

U(9

CO

UJ

a.

»— in (\j rj

•O 3

w fM

o ro I m I

CD

(NJ O

in o o

(M K>

00 CO (M

T— CM

1— (V ooo

o

ro

Oro

oo

r^ CO

^ CM

4- ^

ao o o • O CO IM o rj ru. > ec ov

3< «c

CO

CO

»- CM ro

o

«- o o • O O CO

ro in fsi ro ro ro

«- *— CM tn m

o o

•O u^

CO CO in ^ «-

(M

O

nO o ^

oCO

oCM

o T- o Npo rj

ro 00

(M >-

f\j CO

o

CM IM . »-

03o

o o o •- u> 00 ro

CM O in o CM

ro

: :8

=> Q cn on z

UJ

CO -M z

o c U ID O O CM in

CM O

in ro ^- CM ro

u^ o o CM m

CM >OOr\J^mc\JfON- v-CMro*— inNOoo^-fMro

ro o in o o N. *

o

o o CM OCO in CM O o

ro TCM ro s- o

M *t +1 V+t +1 •H CO

•M H t— ro -H ro M H *i in

ITi o V o CO o O o £> •o o

o CM O CM CM orsj o ro in ro

<o

oo

CO ro

»— CJ> CB (Jl CJ) O) Ol O) CJ) CJ) CJ) CJ) CJl CJ) CJ) C7) CJl CD CJ) CJl CD CJ) CJl Ol CD Ol CJl O) CJl Ol CJl C71 \ \ — \ \ '

\ \ "-^ —

z CJl cn CJ) CJl CJ) CJ) tJI CJ) CJ) CJ) Ol CJl O) CJl CJ) CJ) C7) CJ) CJl CJl CJl CJl CJl Ol CJl CP CJl Ol Dl Ol CJl D c D 3 3 c c 3 3 c c c 3 c 3 3 c c c 3 c c c c c 3 3

C c o (D •a t- J3 u CI l_ (- m XI c C

UJ Z X X z z z z z CL a. a CL CL a. 00 CO cn C/> (/) C/l CO Z) > 3 >- fsl

1575-2
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

1 (ng/g) As (nq/g) cont.

150 50 RTNA 1 210 10 COLOR 77BUR 01 210 20 HAA 84NAR 01 (ug/g) 215 6 HAA 81UTH 01 220 20 7 RTNA 80GAL 02

255 OES 1 1 1 220 40 lENA 82GLA 02

287 OES 7^ IHM 220 60 HAA 85NAR 03

399 ICPES 230 HAA 81ARA 01 405 OES OA 1 230 20 FAA 80DUP 01 439 18 11 ICPES 81MUN 01 1 240 20 7 RTNA 77GIL 03

443.9 20.4 6 COLOR n't RAD 01 1

1 240 20 7 RTNA 80GAL 02

449 OES 07 1

461 .5 16.6 6 COLOR 1 Au (ng/g)

465 OES f P JUN 473 OES r J JUn OA 1 0.3 0.08 ITNA 79REN 03

483 OES OA 1 0.9 0.1 RTNA 80SLO 01 495 ICPES 1 498 15 11 ICPES o inuN 1 B (ug/g)

521 OES 1 526 17 11 ICPES ni 1 13 OES 75J0N 08

529 6 ITNA 1 1 1

1 13 OES 75J0N 09

532 20 AA 01U 1

1 13.3 0.7 ICPES 79HER 01 553 12 ITNA 02 1 15 OES 75J0N 02

558 FAA 02 1 15 OES 75JON 05

560 10 ICPES 04 1 16 4 ITNA 82SCH 05

565 44 ITNA 77m An 16.1 0.1 TCGS 82GLA 02

575.1 1 ICPES OH rKJ\3 17 OES 75JON 01 582 47 CPXRF 80KIR 01 1 17 1 35 TCGS 81GLA 04

585 AA fil ADA 01 1

1 17.2 1.4 11 ICPES 81MUN 01 590 50 ITNA QLUH 1

1 17.6 0.7 11 ICPES 81MUN 01 620 35 ITNA 81GLA 03 1 18 ICPES 81 GOO 01 734 CPXRF AA^AI 1 01 11 18 OES 75 JON 07

750 200 ITNA niU 1

1 j 19 OES 75JON 06

243 OES 7S inu ni 1 19 1 TCGS 84GLA 11 20 OES 75J0N 04

> (ng/g) 20 OES 75 JON 03

20 OES 75 JON 11

150 50 RTNA ni 1

154 5 7 FAA n? 1

1 Ba (uq/g)

180 15 7 FAA n? 1

181 3 RTNA 01 1 3 OES 75 JON 03

187 6 7 FAA 0? 11 6 OES 75J0N 05

190 10 11 HAA R7 inu ni 1

1 6.1 0,4 ITNA 77NAD 02

190 30 11 HAA 82J0I>$ 01 1 7 OES 75 JON 11

193 ICPES 84MIA 01 1 7 OES 75 JON 04

200 FAA 84XIA 01 j 7.1 ICPES 84NAD 01 200 20 7 RTNA 80GAL 02 1 7.8 4 ICPES 85WHI 02

200 20 7 RTNA 77GIL 03 1 8 OES 75JON 01|

200 30 ITNA 77NAD 02 1 8.4 2.5 ITNA 85GAU 04

200 50 AA 83RAP 01 1 205 22 ITNA 85GAU 04 1 1575-3
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (cont.)

Cone

Br (ug/q)

Uncer Com Method Reference

1 . c CPXRF 80KIR 01

6.1 0 .09 ITNA 79REN 03

6.25 0 .2 ITNA 80HOE 01 6.4 0 .8 5 lENA 79GLA 02

6.43 0 .08 ITNA 77NAD 02

6.8 0 .5 5 lENA 79GLA 02

6.9 0 .2 ITNA 85GAU 04

7.08 CPXRF 84KAU 01 7.4 0 .3 ITNA 77STE 02

7.6 ITNA 86GAU 01

8 ITNA 84GLA 02

8.6 ITNA 84GLA 11 30 EXRF 81 PAR 01

50.37 0 .16 CB 80SCH 02

50.4 1 .5 35 CB 79GLA 04

50.7 0 .9 CB 82GLA 02

54 2 35 TCGS 79GLA 04

Ca (uq/q)

3100 200 ITNA 80SLO 01 3300 OES 75 JON 07

3600 ICPES 84NAD 01 3700 500 CPXRF 80KIR 01 3800 OES 75 JON 02

3800 OES 75JON 11 3800 OES 75J0N 05

3830 CPXRF 84KAU 01 3900 OES 75J0N 09

4000 OES 75J0N 06

4000 30 ICPES 84F0G 01 4000 100 11 ICPES 82 J ON 01 4070 120 ITNA 85GALI 04

4090 20 11 ICPES 82 J ON 01 4100 30 11 ICPES 82J ON 01 41 10 1

1 Lrto Oil J UN U 1 4182 67 11 ICPES 81MUN 01 4200 100 ICPES 85WHI 02

4290 40 NM 81YUZ 01 4290 60 ICPES 79HER 01 4300 ITNA 84GLA 11 4300 600 ITNA 79REN 03

4316 157 11 ICPES 81MUN 01 4500 400 ICPES 85LYO 01 4500 400 ITNA 77NAD 02

4600 OES 75J0N 03

4660 AA 84GLA 02

Cone Uneer Com Method Reference

Ca (ug/g) cont.

4800

4900

5000

5300

13100

Cd (ng/g)

140

150

160

180

180

185

193

193

200

200

206

210

220

250

260

300

300

300

300

310

340

Ce (ng/g)

150

220

258

243

260

280

300

305

510

551

OES 75 J ON 04

OES 75 JON 01 ICPES 81G00 01 OES 75 J ON 08

EXRF 81 PAR 01

70 11 ICPES 82 J ON 01 20 ICPES 84 FOG 01 90 11 ICPES 82J0N 01 30 RTNA 80SLO 01 90 11 ICPES 82J0N 01 17 FAA 84GLA 11

10 7 RTNA 80GAL 02

30 AA 86GAU 01 FAA 80PRE 01 20 ICPES 83SCH 04

10 RTNA 77DER 01 FAA 82PRE 01 30 FAA 84GLA 02

10 FAA 80LEG 01

10 ICPES 79HER 01 40 D FAA 80SCH 08

40 AA 80SCH 05

100 11 ICPES 82 J ON 01 200 11 ICPES 81MUN 01 30 FAA 81KNA 01 30 AA 83RAP 01

30 RTNA 80SLO 01 ^nj\j T TklA i 1 NA 27 RTNA 83TJI 01

20 ITNA 77NAD 02 ITNA 84GLA 11 30 ITNA 80SLO 01 20 ITNA 85GAU 04

CPXRF 84KAU 01 120 CPXRF 79REN 02

37 ITNA 77STE 02

1575-4
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (cont.)

\*UI IK* Pnm MAfhruH Reference |

1

1

1

Pij (iia/a\

110 FAA 82HOE 01 1 0.7 OES 75J0N 09

110 RTNA 80SLO 01 j 2 ICPES 81G00 01 110 20 ICPES 84FOG 01 1 2 OES 75J0N 02

130 20 ITNA 77NAD 02 1 2.3 FAA 83ATS 01

134 6 ITNA 77GUZ 01 1 2,3 0.7 11 ICPES 81MUN 01 140 20 ITNA 85GAU 04 1 2.41 0.09 RTNA 77DER 01 340 180 ITNA 79REN 03 1 2.5 0.3 11 ICPES

1 2 7 0.2 1

1

ICPES 87.inN 01

1 7 S 0 1 MMAA A3RAP ni

1 2 8 0 3 FAFMt 76FPS 01

0 2 11 irPFS 82JON 01 1 2 8 Q 5 1

1

IPPFS u 1 nun \j 1 1.5 0.3 11II ICPFS 1 to 81MUN 01 1 2 9 0 1 COLOR 762AN 02

1 .8 ICPES 84NA0 01 1 2.9 0.1 COLOR 76EPS 01 2.2 0.5 11 ICPES 81MUN 01 1 2.9 0.2 ICPES 83SCH W*^ WWII 04V^ 2.25 11 AA 79H0E 02 1 2.9 0.2 1

1

ICPES 82JON 01 2.25 11 AA 79H0E 02 1 2.94 0.01 COLOR 77BUR 01 2.39 11 AA 79H0E 02 j 2.98 0.16 7 RTNA 80GAL 02

Oil ITMA 77NAD 02 1 0.1 ICPES aOSCH 08

81 GOO 01 1 X 0 15 u 1 ^nn V

1

n 1 AA 83RAP 01 1 0 3 MMAA 762 f UbnnAN Ol( V It

C a JO 84KAU 01 1 mJ 0 3 AA 76ZAN 02

? A MMAA 82UIL 04 1 J 0 3 V V ftO^PH OS

? A nU 1 D 1 82GLA 02 1 n 3 ycF Ai\ r

£ . o 81KNA 01 1 J 0 5 1

1

IPPFS R? inM 01

2.62 0.2 ICPES 84 FOG 01 1 3 0.52 CPXRF 80KIR 01

? 7 TTMA 1 D nM 85GAU 04 1 3.01 0.5 ICPES 84F0G 01 2.8 FAA 82H0E 01 1 3.04 0.16 7 RTNA 80GAL 02

2.9 0.2 11 ICPES 82J0N 01 1 3.17 CPXRF 84KAU 01

3.1 0.6 ICPES 79HER 01 1 3.2 0.2 DCPES 79REE 01 3.93 0.05 ITNA 79REN 03 1 3.2 0.2 D DCPES 81REE 01 4.48 0. 19 FAA 83CAR 02 1 3.2 0.4 AA 76EPS 02

1 3.2 0.4 AA 84KAN 01 pe { no /fl ^

1 3 2 0.4 AA 76EPS 01

1 3 77 0 ns RTNA l\ 1 RM 8QSL0 01

lU 1 J

T

1 TMA 1 tin 77NAD 02 ! 3 1

1

MMAA 70HnF OP

71 1 1 NA 84GLA 11 1

1 1

1

MMAA yOunp 0?

r f TU A 1 1 NA 84GLA 02 1 "K A n 3 FAA rMM AP^PT 01

luy J

f Ty A

1 1 NA 86GAU 01 j XJ.I7 MMAA flC^n 1 01 lie f 1 1 NA 77GUZ 01 1 / 7** inu OA

1 ft T TUA 1 1 NA 85GAU 04 I L 1 n ft I PPFQ 7Qupp ni lAn A 1 NA 79REN 03 1 OFS 75 JON 07

5 OES 75J0N 06

6 OES 75 JON 08

8 OES 75JON 1

1

8 OES 75J0N 0^

8 OES 75JON Oi> 8 OES 75 JON 03

11 AA 81ARA 01

53 XRF 80SUZ 02

1575-5
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRH 1575 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

U (nq/q)

__

Fe (ug/g) cont.

4 1 RTNA HIT 1 r ool Jl Ul 1 209 AA 82UIL 04

6 2.6 ITNA 1 214.5 21.9 ICPES 85LY0 01 6.5 0.8 ITNA 77kl An Mc.

1 217 8 11 ICPES 81MUN 01 11.3 1.6 ITNA O^uAU riA 1 254 OES 75J0N 05

260 OES 75J0N 04

(ug/g) 280 50 ITNA 79REN 03

595 AA 81ARA 01

2 COLOR oOJML 1 790 EXRF 81 PAR 01 2.5 0.3 ISE AT^UA

1 2.9 0.8 ISE oHuLA 1 Gd Cng/Q)

3.7 0.8 MS T7CTC 1 28 7 RTNA 83TJI 01

e (ug/g)

H (%)

47 OES JUN no 1 Uv 1 100 10 11 ICPES olHUN U1 1 6.39 0.07 CB 80SCH 02

106 OES f D JUn UO 1

1 6.5 0.1 35 TCGS 79GLA 04

118 OES 7C milf 3J0N no 1

1 6.54 0.08 CB 82GLA 02

120 OES fVZ 1

1 142 OES r 3 JUN 1 1

1 H20- (%)

152 ICPES D/ ki Ar\ ohNAU U1 1 152 ICPES A1 nnn 01 1

1 4.4 D GRAV 85NAR 03

156 OES ni 1 U 1

1 4.4 GRAV 84NAR 01 170 10 ITNA 70ri AC ni 1

1 170 10 RTNA ni 1

i Hf (nq/g)

174 0.9 11 COLOR

174 6 11 COLOR 10 RTNA 80SLO 01 175 7 11 ICPES A7 mu 01 1

t 36 17 ITNA 85GAU 04

177 4 11 ICPES A9 \r\u 01 1

1 182 OES r J JUn OAUO 1

1 Hg (ng/g)

183 3 ICPES 70LICD 01 1

185 11 AA f ynut no 1 Uc 1 121 6 ITNA 77NAD 02

185 11 AA 70unc f ynut no 1 yjc.

1 133 11 CVAA 79H0E 02

188 9 XRF 03AVA ni 1 U1 1 147 8 CVAA 82GLA 02

188 17 CPXRF OUKlK ni 1 U1 1 157 18 CVAA 80DUM 01 193 OES OJON f\7 \ \jf

\ 160 20 RTNA 80SLO 01 194 4 11 ICPES o<:JON n 1 1 U1 1 194 6 11 COLOR DOcr*u m 1

1 I (nq/q)

194 10 ICPES n^ 1 UD 1 195 CPXRF fi/ ^Al 1 OHikAU ni 1 Ul 1 < 200 L PAA 77WIL 01 195 10 11 ICPES oo mil O£J0N ni 1 Ul 1 140 20 lENA 82SAT 01 195 10 D ICPES OAUO t

1 150 50 RTNA 77STE 02

195.7 5.4 ITNA 77GUZ 01 1 196 7 ITNA 77NAD 02 1 196 13 XRF 83PEL 01 1 198 8 AF 81H0R 01 1 204 10 ITNA 85GAU 04 1 204 12 ICPES 81KNA 01 1 207 0.8 ICPES 84F0G 01 1 207 12 AA 83RAP 01 1

1575-6
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (cont.)

Cone uncer Codi

-

Reference | Cone Uncer Com netnoa Reference

< (ug/g) 1

1

Mg (U3/3?.

ciQlJ OcS 75J0N 05 1 yuu OcS 7C 1 mi AA /DJON 09

3UUU ICPcS 84NAD 01 1 1UUU ICPcS O/ kl Ar\ A1 OhNAD 01 3200 OES 75 JON 09 1 1025 ICPES O <1 ^AM All 81G00 01 3300 ICPES 79HER 01 1 lOf U CPXRF O/I/AII Al 84KAU 01 ZUO 1

1

ICPcS 82J0N 01 11 lUU 1 nn ICPcS ryHtK 01 DUU LrAKr 80KIR 01 1

1 1 / o ly 11 ILrcb O A Ul ILI At 0IHUN 01 OU 1

1

ILrtb 82J0N 01 1 1 A fin1 IQU TO 1 1 T CDCC ILrto 00 mu ni O^JUN 01 OOUU T PDCC ILrto 79COO 01 i 1 ion 1 lyu on 1

1

1 Lrtd 00 mu ni O^JUN 01

1

1 nnuu T TU A 1 1 NM 77NAD 02 1 1 101 Xft 1

1

OO 1 1 T PDCC 0 inuN u

1

*f u 82JON 01 1 i?nn Tcr jJUN inu OAUO

ft? 1 1 1 1 I rpcc 81MUN 01 1 i?nn r 3 JUN U

1

75J0N 03 1 i?nn r^JUn Ur ^uu 7 TM A 1 \ WA 79REN 03 1 i5nn 7c inu no rDJUn U^

X7Q/. l/.T! IhO 1 1

1 1 1 Lrto 81MUN 01 ! 1

1 cUU 5nn 5n 1

1

cU 1 1 I PDCC 00 lou ni Oc JUN U

1

OOUU 75 JON 04 ! 1 5nn JU 1 1 1 PDCC 1 Lrto 00 lou ni 0^ JUN U

1

oU 1 1

1 CPcS 82J0N 01 1 IcUU ILrcd cSdLTU Ul oVUU zuu ILrtb 85UHI 02 1

1 onn inn luu ILrta ficuuT no oDWnl Uc

CPXRr 84KAU 01 ! I TNA 0Act A A i oUSLO Ul 4000 OES 75J0N 01 1 1300 OES 75J0N 03

4000 100 ITMA 80SLO 01 1 1330 UNA 84GLA 11 4400 OES 75 JON 02 i 1400 OES 75J0N 08

5100 OES 75J0N 06 1 1500 OES 75 JON 11

D 1 uu T TU A 1 I nA 84GLA 11 ! 1 DUU 7nn f

1 TUA 1 NM 77UAn 1 rnMU nou£

75 JON 11 1 1lOUU Ann HFC Tc mu n^

OjUU nrc 75J0M 07 1 i7nn 1 f uu HFC Tc inu

y 1 uu CAKr 81 PAR 01 1 ccUU Ann rpYPF OA^Tp n^ OUK, IK u 1

La (ng/g) 1

j

Mn (ug/g)

<iO RTNA 80SLO 01 I

t 7/ 1 1 PDCC oipnn ni 0 i uUU U

1

140 i n10 I TNA 77NAD 02 1 Uto 7c mij no adjun uy

i / i DTII A K INA 83TJI 01 1 / / Q 7c inu ni ion lyu T TU A

1 1 NA 85GAU 04 1 DOf 7"^ inu nA r jJUn UO

210 ^0 T Tkt A

1 TNA 79REN 03 1 Uto 7^ inu no fDJUN Uc

3oU uto 7c inu nA

Li (ng/g) 1 Uto 7c inu f OJUN UO

1 Ano ouc IO 1

1

I PDCC fiiMiiu 0 ni 1 nun u

1

340 40 AA 85GAU 04 1

ill n 61

U

ILrto Q/. u A A n 1 ohNAU U I

ood. i / 11 T PDCC ILrtd 00 inu ni o^JUN U

1

Lu (ng/g) tod. 1 C 11 15 T PDCe iLrtb flo inu m

1 o!>4 AA 77PI 1*7 ni f (\j\JL Ul

1 .2 0.2 RTNA 83TJI 01 1 zee 655 17 1 1 13 11 I CPcS O^JUN 00 lAii mU1

1 .3 A T 0.3 RTNA 80SLO 01 1 65/^ 7 11

f

T PDCC 1 Lrto O^JUN Ul 2.2 0.5 I TNA 85GAU 04 1 660 28 I TNA 77NAD 02

668 OES 75J0N 05

668 20 AA 83RAP 0|

669 48 XRF 83PEL 01 670 6 ICPES 79HER 01

671 2 ICPES 83SCH 04

673 10 DCPES 79REE 01

1575-7
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (cont.)

Cone Uncer Com Method Reference

Mn (ug/g) cont.

673 10 D DCPES 81REE 01 676 0.7 ICPES 84 FOG 01 677 12 W 80SCH 05

677 12 D ICPES 80SCH 08

678 7 ICPES 81KNA 01 685 15 ITNA 80SLO 01 686 CPXRF 84KAU 01 686 53 ICPES 85LY0 01 688 11 AA 79H0E 02

690 20 ITNA 85GAU 04

693 6 ICPES 85UHI 02

698 11 AA 79H0E 02

700 100 ITNA 79REN 03

719 13 11 ICPES 81MUN 01 727 XRF 80SUZ 02

738 OES 75 J ON 08

885 OES 75J0N 07

2200 EXRF 81 PAR 01

lo (ug/g)

0.1 RTNA 80SLO 01 0.1 0.1 11 ICPES 82J0N 01 0.13 0.06 11 ICPES 82J0M 01 O.C 0. 1 4 4

1ICPES 82J ON 01

f\ O v.c U. 1 1 1 ICPES 82 J ON n 4 01 1.5 OES 75JON 11 1.7 OES 75J0N 01 2.5 OES 75J0N 07

3.6 OES 75J0N 03

18.5 OES 75 JON 02

<%)

•1 4 4 1.11 0.01 CB 8QSCH 02

1 .2 0.14 CB 82GLA 02

1 .3 0.2 35 TCGS 79GLA 04

a (ug/g)

18 OES 75J0N 06

18 4 11 ICPES 81MUN 01 20 OES 75J0N 03

23 ICPES 84NAD 01 26 ICPES 81 GOO 01 26 4 ITNA 77NAD 02

26 9 ICPES 85WHI 02

30 OES 75J0N 09

37 4 ITNA 85GAU 04

40 ITNA 79REN 03

1575-8

Cone Uneer Com Method Reference

Na (ug/g) cont.

56 ITNA 84GLA 11 70 OES 75 JON 11

71 ITNA 84GLA 02

78 OES 75J0N 08

100 OES 75J0N 01 100 OES 75J0N 05

105 16 11 ICPES 81MUN 01 190 OES 75J0N 04

Nd Cng/g)

128 53 RTNA 83TJI 01 200 100 RTNA 80SLO 01

2.07 0.07 11 ICPES 82JON 01 2.2 0.1 11 ICPES 82JON 01 2.2 0.2 ITNA 77NAD 02

2.24 0.06 11 ICPES 82J0N 01 2.3 ICPES 85J0N 01 2.3 0.2 ICPES 79HER 01 2.3 0,2 RTNA 80SLO 01 2.31 CPXRF 84KAU 01 2.39 0.09 11 ICPES 82JON 01 2.4 0.5 11 ICPES 81MUN 01 2.63 VOLT 81PIH 01 2.7 1.1 CPXRF 80KIR 01 2.9 0.1 DCPES 79REE 01 2.9 0.1 D DCPES 81REE 01 3.3 0.07 AA 83RAP 01 3.7 0.2 ICPES 84F0G 01 4 FAA 82H0E 01

P (ug/g)

900 ICPES 84NAD 01 1000 OES 75 JON 04

1000 300 CPXRF 80KIR 01 1100 ICPES 79EDI 01 1100 OES 75 JON 09

1100 ICPES 81 GOO 01 1100 FAA 79E0I 01 1100 50 ICPES 84F0G 01 1100 100 CPAA 83MAS 02

1146 120 11 ICPES 81MUN 01 1155 41 11 ICPES 81MUN 01 1170 40 11 ICPES 82 JON 01 1170 50 ICPES 810WE 01 1180 10 ICPES 79HER 01
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (cont.)

Prim ncr LDIUU Reference |

1

Cone 1 In/^op 1*16 LMoa Reference

/ 1 in / /*/^r>t" lug/g; cont

1

1 DrI t nn /n \

1 ion 50 1 1

1 1 T1 PDCC Lrto 82 J ON 01 1

1 ion ^0 1

1

1 1 1TTDCQ Ur Co 82 J ON 01 1

1L DTUA K 1 Nn 81BYR 01

1 ?nn 75JON 05 1 c DTUA 85BEM 01 100 1 UU 85UHI 02 1 ?0£U 1 1 1 do 82 J ON 01 1 upon rpvpp Wr/M\ r 84KAU 01 ! 75J0N 06 i 70 1 RTUA 80SLO 01

o 75JON 08 1 ion 1 vU 1 V«r G.O 85LYO 01 ! Ku ^ug/g;

1400 OES 75 JON 07 ! 1400 75J0N 11 1 10-8 CPXRF 84KAU 01 1410 80 FAA 84KUB 01 1 10-8 0.5 ITNA 85GAU 04

1 \J\J\J 75JON 02 ! 11 0 2 ITNA 77NAD 02

1800 OES 75 JON 03 1 12.22 0.85 ITNA 77GUZ 01

C. 1 uu wed 75 JON 01 1

1

IP S

1"? 1

9

£ . o

I TMA

l#r AKr

79REN

80KIR

03

01 W / 1 in /rt\

I CAKr 81 PAR 01

1 ''i rpvop 80K« 01 i o 1 Ani r 85AVA 01 j y • D fi i 1 I t rppc 82 J ON 01 j 0 A rMM 80PRE 01 1 5fin 140 79REN 02

7 a \J 0 ? U a 1 1 82J0N 01 i 1200 250 CB 84GLA 11

lU B si, 84FUD 01 j 1??0 70 CB 86GAU 01 84KAU 01 1 1240 CB 85JAC 01 10.4 82GAJ 01 1 1240 30 5 CB 84JAC 01 10 4 FAA 82PRE 01 j 1250 40 CB 86B0U 01

10 5 A FAA 82K0I 01 1 1290 CPXRF 84KAU 01 10.5 6 81HIN 01 1 1290 D CB 85JAC 01 10,6 (, FAA 84FUD 01 1 1290 50 6 CB 84JAC 01 in A 0 ^ AA 83RAP 01 1 1400 100 ICPES 85WHI 02

in1 U B AO 0 "2; U o J> 83BR0 01 1 1490 40 UXRF 86B0W 01 in 7 MMAA 84KAN 01 1 1500 300 CPXRF 80KIR 01 in A FAA 83H0E 01 j in R MMAA 82WIL 04 ! oD ing/g;

in R 0 ^ I Ur Eld 84 FOG 01 1 in ft 1 u o FAA inn 80LEG 01 j 180 10 ITNA 77NAD 02

in 0 U a FAA 81KNA 01 ! 180 14 HAA 79V I

J

01 in 0"^ 0 01 ACV 80SZY 01 j 185 2 RTNA 79H0E 01 FAA 82KOI 01 j 185 60 AA 83RAP 01

o FAA 81HIN 01 1 1fi7 7 HAA 78KUB 02

1

1

rMM 79H0E 02 j 1AQ 1 OT 17 ITNA 85GAU 04

0 A 79DAB 02 j 100 101 u RTNA 80SLO OT

1 79HER 01 j 198 3 RTNA 80KOS 02

11 1 0 X MMAA 80SCH 05 1 220 10 7 RTNA 77GIL 03

11 1 0 n FAA 80SCH 08 I 220 10 7 RTNA 80GAL 02

1

1

FAA 79H0E 02 1 220 20 7 RTNA 77GIL 03

11.2 FAA 82H0E 01 ! 71 DTUA K 1 NA 80GAL 02

11.2 1.1 HAA 82UEI 01 j 1140 440 ITNA 79REN

11.9 1.1 11 ICPES 81MUN 01 1 13.9 1.2 FAA 82WEI 01 1 14.6 3.4 11 ICPES 81MUN 01 1 33 EXRF 81 PAR 01 !

1575-9
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRH 1575 (cont.)

Cone

Sc (ng/q)

Uncer Com Method Reference

27 4 ITNA 77GUZ 01 38.7 0.6 ITNA 86GAU 01 39 2 ITNA 84GLA 11 42 2 ITNA 77NAD 02

45 6 ITNA 85GAU 04

53 8 ITNA 79REN 03

130 RTNA 80SLO 01

Se (nq/q)

43 1 11 GC 81UCH 02

43 1 11 GC 81UCH 02

44 8 ITNA 77NAD 02

50 10 RTNA 80KNA 01 53 10 9 ITNA 80WAN 01 96 16 RTNA 82P0L 01

Si (ug/g?

248

1380

Sm (ng/g)

Sr (us/g)

Ta (ng/g)

13

1740

Tb (ng/g)

2

60

36

4

270

1

10

CPXRF

CPXRF

ITNA

ITNA

RTNA

RTNA

80KIR 01 84KAU 01

18 1 RTNA 83TJI 01 20 2 RTNA 80SLO 01

21 2 ITNA 85GAU 04

130 120 ITNA 79REN 03

4.45 CPXRF 84KAU 01 4.7 0.2 AF 81H0R 01 4.75 0.1 ICPES 84 FOG 01 4.9 0.1 ICPES 79HER 01

5 OES 75 JON 03

5.4 lENA 85GAU 04

5.5 0.57 CPXRF 80KIR 01 10 OES 75J0N 04

20 OES 75J0N 01

85GAU 04

79REN 03

83TJI 01 80SLO 01

Cone

Th (ng/g)

34

35

50

Ti (ug/g)

13.7

Tt (ng/g)

27

28

29

30

31

U (ng/g)

13

15

15

18

18

20

20

V (ng/q)

99

248

346

347

370

410

450

453

470

M tng/g)

50

Yb (ng/g)

9

26

Uncer Com Method Reference

1 ITNA 77NAD 02

5 RTNA 80SLO 01 12 ITNA 85GAU 04

CPXRF 84KAU 01

ASV 84LIE 01

II ASV 84LIE 01

11 FAA 84LIE 01

11 ASV 84LIE 01

11 ASV 84LIE 01

2 RTNA 80SLO 01 DNA 84GLA 02

0.5 RTNA 780ER 01 2 DNA 86GAU 01 6 35 DNA 80GLA 04

4 DNA 85GAU 04

48 R DNA 81GLA 03

14 11 RTNA 82HEY 02

6 11 RTNA 82HEY 02

18 RTNA 78BYR 01 27 11 RTNA 82HEY 02

90 11 ICPES 82J0N 01 60 11 ICPES 82J0N 01 ITNA 85GAU 04

61 ITNA 82HEY 02

80 ITNA 77NAD 02

10 RTNA 80SLO 01

1 RTNA 83TJI 01 8 ITNA 85GAU 04

1575-10
TABLE 1575-2: INDIVIDUAL DATA FOR NBS SRM 1575 (cont.)

Cone Uncer Com Method Reference

Zn (uq/g)

5 OES 75JON 09

51 9 CPXRF 79REN 02

52 1 ITNA 77NAD 02

53.5 2 RTNA 80SLO 01 56 ICPES d4NAD 01 57 OES 75JON 11 59.2 CPXRF 84KAU 01 60 3 11 ICPES 82JON 01 60.3 1.3 RTNA 77DER 01

61 4 11 ICPES 82JON 01 63 3 11 ICPES 82JON 01 64 4 11 ICPES 82J0N 01 64 7 ICPES 79HER 01 65 AA 81ARA 01 65 4 11 ICPES 82J0N 01 65 4.6 XRF 83PEL 01 65 6 ITNA 79REN 03

66 OES 75J0N 06

67 XRF 80SUZ 02

68 OES 75J0N 08

68 5 11 ICPES 82J0N 01 69 8.8 ICPES 85LYO 01

71 1 DCPES 79REE 01

71 1 D DCPES 81REE 01

71 10 11 ICPES 82JON 01 72 i' OES 75 JON 02

72 13 ICPES 85UHI 02

74 OES 75J0N 03

74 9 11 ICPES 82J0N 01 76 2 ICPES 83SCH 04

78 ICPES 81 GOO 01 82 OES 75 JON 05

85 OES 75JON 07

86 21 11 ICPES 81MUN 01 87 OES 75J0N 01 99 10 D ICPES 80SCH 08

99 10 ICPES 80SCH 05

110 12 CPXRF 80KIR 01

111 39 11 ICPES 81MUN 01

141 OES 75 JON 04

1575-11
(A UJ (/>(/) < c/> X S </>

tJ I ^ u

(J U trt CJ ^ U (J7 u

f\j <M f\i ^ f\; (M fVJ f\J 1— •" rg f\j

i/> o ir> (M ro

fSJ f\J f\)

fM CO ITN O oD O 00

f\j rsj fu !-o r\j

V) u. O u

< LU (-1 W > Q. -J

LU U Ou

p*j »- »- o ro (M fNJ »- ^ T- in (\j

GO 00

fM O « « O fNj fNJ r\j r\j

ru »- u-i

S 2:

O «— u-i sO CO

4H -H

f\l o

^^ rvj in rsj Ki

in 'O Kl CO

• o o o mom

2 3

O CO ^ o-

. -J- r~ m <z> r- o <M o

CO O ^

«M no O c\i

• f\J CO

o •-

o> Oi W Oi

"-^ ^ ^

0> W CTt C

0< CT* Oi CT* CT^ O* 0» tJ*

(D -O T T T5

1577-1
r\t r- ^ rg (Ni f>j

Ki K> . fo O IT* *— O

fsj rg

CJ O < >

o

rvj*4 oo<rgi 'Ow*-

rg in

r\j w ^

in o pn o

in

g 2

nj o f\j o

OD •— S- nj

>0 njo rg

SI

o o in o KJ 1^ o o

<0 (M

*- o

o «0

( rg o

o

+1 N. W

rg >J

O) O) o> 0> Ql Ql O) Dl o> oi o> o o) tji ni o> o> oi DDCCCJv'CCCCCCLi

^ J3 ^ i3 t1577-2

TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Aq (nfl/g)

1

1 Al (uq/q) cont.

< 130 L RTNA 76GAU

1 01 1 34.4 1.4 RTNA 80WOI 01

5 17 UU 74MAS 01 1 34.6 ICPES 84NAD 01 40 8 RTNA 79WAR 02 1 37 6 ITNA 77ZIK 01 49 16 lENA 86CHI 01 1 42 13 ITNA 77HAM 01

51 11 RTNA 77LIE 01 1 45.6 ITNA 73NAD 01

5,1 11 RTNA 75LIE 01 1 65 ITNA 78CAP 01 53 17 ITNA 86CHI 01 1 58 3 ITNA 86GRE 01 1 As (ng/q)

60 ITNA 770SB 01 1 60 1 FAA 75PIC 01 1 23 12 HAA 82TAM 01 65 5 RTNA 80SLO 01 1 30 15 lENA 78WAN 01 65 10 SSMS 77PAU 01 1 40 10 RTNA 75ABU 01 66 21 ITNA 79CHA 04 1 40 10 RTNA 80SLO 01 68 6 ITNA 78BEH 01 1 41 HAA 79EVA 01 72 13 AA 80JAC 01 1 43.3 HAA 771 HN 01 80 6 ITNA 79CHA 02 1 46 2 RTNA 79H0E 01

91 26 ITNA 73C0R 01 1 47 5 HAA 82SUB 01 100 10 ITNA 84ALK 01 1 49 6 HAA 76FI0 01 100 30 ITNA 80MIC 01 1 50 HAA 78WEL 01 194 17 UU 74MAS 01 1 50 ICPES 84MIA 01 300 100 34 CPXRF 78J0L 01 1 50 3 ITNA 86GRE 01 400 OES 75B0L 02 1 50 10 HAA 80AGE 02

2000 600 RTNA 74SCH 03 1

1

50

52

10

3 34

HAA HAA74LOO Ol( 78FLA 01

Al (ug/fl) 1

1

52

52

3

7

AA

ITNA

79FLA 02

79CHA 02

< 3 ITNA 86GRE 01 1 52.9 1.9 H RTNA 790RV 01 < 15 L ICPES 78CAP 01 1 53 2 7 RTNA 80GAL 02

< 50 CPXRF 84KAU 01 1 53 2 7 RTNA 81KUC 01

< 80 L 14NAA 81UIL 01 1 53 2 RTNA 84SCH 04

< 80 L 14NAA 81WIL 02 1 54 RTNA 85TIA 01 0.7 0.2 lENA 85GLA 02 1 54 H FAE 79FEL 01 1.44 0.1 HPLC 85BON 01 1 54 2 RTNA 79WAR 02

1.8 0.2 ITNA 77G00 01 1 54 2 6 HAA 81KAH 01 2.21 0.15 ITNA 82EHM 01 1 54 4 7 RTNA 80GAL 02

3.6 11 SSMS 85V0S 01 1 54 4 RTNA 82BYR 01

5 ICPES 79MCQ 01 1 54 4 RTNA 78GAL 01 6 2 ICPES 79ABE 01 1 54 5 RTNA 79MAY 01 6 3 ITNA 84GLA 02 1 54 5 RTNA 74HEN 01

6.1 ITNA 84GLA 11 1 55 1 RTNA 80BYR 01 7 17 UU 74MAS 01 1 55 3 7 RTNA 80GAL 02

8 0.6 11 ICPES 81BLA 02 1 55 3 RTNA 77GIL 03

8.2 0.8 11 ICPES 81BLA 02 1 55 3 NAA 77GIL 01 11.3 2.9 6 ITNA 74H0F 01 1 56 3 6 HAA 81KAH 01 15.3 1.1 ITNA 80SLO 01 1 56 3 HAA 81UTH 01 20.4 2.9 6 ITNA 74H0F 01 1 56 4 RTNA 77LIE 01 20.8 0.7 RTNA 77BU0 01 1 56 4 RTNA 75LIE 01 23.4 0.6 RTNA 79WAR 02 1 56.6 1.2 RTNA 73DAM Olj

23.6 2 ITNA 79CHA 02 1 56.6 1-2 NAA 74HEY 01 30 65 RD ITNA 79IMA 03 1 57 ASV 78DAV 01 30 65 R ITNA 79 1 MA 01 1 58 3 RTNA 79HEI 04

1577-4
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

As (ng/g) cont.

58

58.5

59

59

59

60

63

63

64

66

66

69

70

80

100

100

150

200

280

290

500

600

Au (ng/g)

0.058

0.083

0.23

1.7

4.9

6

7

29.2

B (ug/g)

2.24

2.34

3.2

4

Ba (ug/g)

<

< 0.12

0.13

0.15

0.22

1.24

1.8

2.92

3

9

9

6

4

5

23

10

30

10

300

100

110

500

0.5

0.013

0.021

0.16

0.4

0.8

10.8

2.1

0.02

0.39

17

17

6

34

6

6

0.2

1

20 L 30 L 0.13

11

Cone

Be <nc}/g)

Uneer Com Method Reference

RTNA 79R0S 02 1 < 3 L ICPES 82SCH 01 NAA 76GUZ 01 1 < 60 L ICPES 78CAP 01 RTNA 75STE 02 1 3 1 6 ICPES 82SCH 01 RTNA 81iaJC 01 1 5 3 FAA 750WE 01 AA 83RAP 01 1 17 4 FLUOR 77WIC 01 RTNA 83DAN 01 1 RTNA 740RV 01 1 Bi (ng/g)

RTNA 85GAU 04 1 UU 74MAS 01 1 150 AF 85NAR 02

ASV 81 LEE 01 1 RTNA 74SCH 03 1 Br (ug/g)

UU 74MAS 01 1 RTNA 83BRA 01 1 4.3 17 UU 74MAS 01 RTNA 77TJI 01 1 4.7 0.8 CPXRF 77RIN 01 ITNA 770SB 01 1 6.1 0.6 CPXRF 77WIL 02

GCMES 75TAL 01 1 7.35 17 UU 74MAS 01 ICPES 80HAA 01 1 7.4 0.5 EXRF 80DYC 01 CPXRF 77UIL 03 1 7.7 0.5 5 ITNA 80HOE 01 CPXRF 78J0L 01 1 7.8 0.1 5 lENA 79GLA 02

ICPES 80HAA 01 1 8.0 0.1 5 lENA 79GLA 02

FAA 78CAP 01 1 8.0 0.5 RTNA 76GAU 01 CPXRF 77WIL 03 1 8 1 RTNA 77TJI 01

1 8.22 0.4 RTNA 79WAR 02

1 8.23 0.45 lENA 86CHI 01

1 8.4 0.6 ITNA 84GLA 02

RTNA 80SLO 01 1 8.5 1 ITNA 79CHA 02

RTNA 82ZEI 01 1 8.5 1.3 lENA 84GLA 11 RTNA 84TJI 01 1 8.5 9.9 R ITNA 79 1 MA 01 RTNA 77TJI 01 1 8.5 9.9 RD ITNA 79 1 MA 03

RTNA 77KUS 01 1 8.56 CPXRF 84KAU 01 RTNA 74SCH 03 1 8.6 0.4 NAA 78GAN 01 ITNA 79CHA 02 1 8.8 0.3 ITNA 84GLA 11 RTNA 79WAR 02 1 8.8 0.3 5 ITNA 80HOE 01 RTNA 77NAD 01 1 8.8 0.4 EXRF 79GIA 01

1 8.8 1.4 EXRF 77NIE 01

1 8.9 2.1 ITNA 77HAM 01 AE+AF 74DAU 01 1 9 lENA 85GAU 04

AE+AF 74DAU 01 1 9.0 0.6 ITNA 77JUR 02

TCGS 79FAI 01 1 9.0 0.6 ITNA 78BEH 01 ICPES 79ABE 01 1 9.0 0.9 ITNA 86GRE 01

1 9 1 CPXRF 78V IS 01

1 9.3 1 lENA 79KUC 01 14NAA 81UIL 02 1 9.3 0.8 ITNA 80MAE 01 ITNA 78CAP 01 1 9.3 3 CPXRF 79REN 02

RTNA 76GAU 01 1 9.34 0.82 ITNA 74D0N 01 ICPES 780AH 01 1 9.37 ITNA 73NAD 01 SSMS 85V0S 01 1 9.4 0.4 XRF 77SMY 01 RTNA 79WAR 02 1 9.5 ITNA 80CRE 01 ICPES 84NAD 01 1 9.5 1 6 CPXRF 77W1L 03

RTNA 77GUI 03 1 9.6 0.7 CPXRF 85CLA 01 ITNA 73NAD 01 1 9.7 1 lENA 79KUC 01

1577-5
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone UncGr COfTl Method Reference | Cone Uncer Coni Methcid Referenc^

V ug/ y

1

1 cont

9 7 0.5 CPXRF 84BIS

1 01 1 119 2 1 AA 77UCH 02

9 8 ITNA 79KUC 01 1 120 1

SSMS 85VOS 01 9.8 0.3 RTNA 80WOI 01 1 120 2 11 ICPES 82 JON 01 10 0.7 CPXRF 82R0E 02 1 121 3 11 ICPES 82J0N 01 10 1 CPXRF 80MAE 01 1 122 ICPES 80HAA 01 10.4 ITNA 82AKA 01 1 122 7 ICPES 79MCQ 01

11 ITNA 78CAP 01 1 123 5 FAA 8AHAR 02

11 1 5 ITNA 80TOU 01 1 123 17 AA 79MCQ 01

11 2.3 CPXRF 80KIR 01 1 124 10 ITNA 79CHA 02

11.1 1 .6 RTNA 74SCH 03 1 1 24 . 67 8.48 NAA 76GUZ 01

12 4 ITNA 77ZIK 01 1 125 8 ITNA 75PIE 01 13 4 17 UU 74MAS 01 1 125 13 RTNA 79WAR 02

10 ITNA 77ZIK 01 1 127

127

s7

AAAA75HIN

80UCK

01

01

]

1

127

128

12

2

ICPES

FAE

79MCQ

83MAR

02

04

49.6 1.5 35 CB 79GLA 04 1 129 12 12 FAA 85CAR 02

49.87 0.07 CB 80SCH 02 1 130 10 ITNA 77ZIK 01

51 2 35 TCGS 79GLA 04 1 130 12 ITNA 84ALK 01 52 2 TCGS 79FAI 01 1

1

130

131

30 ITNA RTNA

84GLA

75STE

02

02

1

1

131

131

58

WXRF

CPXRF

84ALK

78V IS

0^

01 30 AE-fAF 79ULL 01 j 131 9 CPXRF 80KIR 01 68 AA 82HAR 01 j 133 ICPES 84NAD 01

71 23 EXRF 77NIE 01 1 134 18 ICPES 79ABE 01 80 30 ITNA 74WES 01 1 134 21 12 FAA 85CAR 02

87 13 ICPES 85UHI 02 1 135 11 SSMS 85V0S 01 90 13 CPXRF 80MAE 01 1 135 ICPES 78DAH 01 94 112 AA 79MAN 01 1 137.5 18 PAA 76KAT 04

100 CPXRF 77WIL 02 1 140 ICPES 78CAP 01

100 20 RTNA 76GAU 01 1 140 7 CPXRF 84BIS 01 100 26 ITNA 78FUR 01 1 143 19 CPXRF 85CLA 01

101 AA 79L0C 01 1 143 42 ICPES 846LA 01

103 12 CPXRF 79MAN 01 1 150 ITNA 84GLA 11

104 17 UU 74MAS 01 1 151 7.4 CPXRF 81 ROB 02

3Jab2 AA 74WES 01 1 158 15 EXRF 80DYC 01 107 1 \i 1 i 1 nn 82AKA 01 1 210 CPXRF 84ICAU 01 107 I TMA 79 1 MA 03 1 309 ITNA 78CAP 01 107 p ITMA I 1 nn 79 1 MA 01 1 108 9 rPAA \frnn 77ZIK 01 1 110 1 ICPES 85WOL 01 1 110 ITMA 1 1 nn 86GRE 01 1 200 11 SSMS 85V0S 01

114 2 1 ICPES 78SUD 01 1 210 20 11 ASV 84ADE 03

115 12 RTNA 80CAN 01 1 210 42 ASV 79ST0 01

116 2 AA 801 ID 01 1 230 11 FAA 75BL0 01

116 2 1 AA 77UCH 02 1 240 17 UU 74MAS OH

116 3.4 6 DCPES 83FRA 01 1 240 10 FAA 82SUZ 01

118 4.9 6 DCPES 83FRA 01 1 246 56 NAA 766UZ 01

118 9 1 ICPES 78SUD 01 1 250 11 FAA 75BL0 01

1577-6
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Cd (ng/g) cont.

250 AA 78EVA 01 250 FAA 83ATS 01 250 10 11 ASV 84ADE 03

250 20 11 ASV 84ADE 03

250 20 RTNA 83BRA 01 250 20 AF 75EPS 01 250 25 AA 82EVA 01 250 30 w 79CHA 02

253 24 AE-i-AF 74RAI 02

253 24 FAA 82ATS 01 260 11 ASV 81DAN 01 260 FAA 82AKA 01 260 FAA 75SLA 01 260 10 RTNA 740RV 01 260 10 FAA 84RAB 01 260 20 FAA 84R0S 01 260 20 11 ASV 84ADE 03

260 20 AA 74ULL 01 260 20 FAA 790AB 02

260 30 RTNA 74SCH 03

260 30 FAA 78PIE 01 260 30 RTNA 80SLO 01 266 20 FAA 74RAI 02

266 27 RTNA 79MAY 01 269 13 RTNA 74R00 01 270 AA 77FRI 01 270 17 UU 74MAS 01 270 17 uu 74MAS 01 270 17 UU 74MAS 01 270 2 FAA 83STE 05

270 10 ICPES 83SCH 04

270 10 11 AA 81BLA 03

270 20 11 ASV 84ADE 03

270 20 AA 85ADE 02

270 20 AA 79WAR 01 270 20 AA 75EPS 01 270 30 AA 79LAK 01 270 50 FAA 81KNA 01 270 60 TCGS 79FAI 01 270 80 FAA 74GR0 01 275 5 FAA 78HUD 01 280 ASV 74C0P 01 280 FAA 82H0E 01 280 AA 84KAN 01 280 RTNA 85TIA 01 280 20 SSMS 77PAU 01 280 30 AA BOSCH 05

280 30 D FAA 80SCH 08

280 50 11 AA 81BLA 03

280 50 ICPES 84MIA 01

Cone Uncer Com Method Reference

Cd (ng/g) cont.

280 70 AA 83RAP 01 280 70 CPAA 85 CAN 01 283 RTNA 75 HAL 01 283 17 UU 74MAS 01 283 50 FAA 79ST0 01 288 26 FAA 81ZAU 01 288 29 RTNA 80GRE 01 288 35 RTNA 75LIE 01 288 35 RTNA 77LIE 01 290 17 UU 74MAS 01 290 17 UU 74MAS 01 290 14 FAA 80CHA 08

290 14 FAA 80CHA 08

290 11 ASV 81 DAN 01 290 FAA 80JAR 01 290 10 FAA 80LEG 01 290 10 AA 84 HUD 01 290 10 D AA 84 HUD 03

290 10 RTNA 77BAJ 02

290 13 7 AA 73TAL 01 290 20 NAA 76DER 01 290 20 AA 79FLA 02

290 30 RTNA 74HEN 01 290 30 RTNA 79DER 01 290 30 FAA 79WAR 01 290 30 FAA 84GLA 02

290 30 ICPES 84BLA 01 293 9 ITNA 86GRE 01 300 ASV 82GAJ 01 300 ICPES 80HAA 01 300 18 7 AA 73TAL 01 300 18 FAA 74TAL 01 300 20 RTNA 78GAL 01 300 20 RTNA 77TJI 01 300 20 7 RTNA 80GAL 02

300 20 VOLT 840ST 01 300 23 AF 75UOR 01 300 25 FAA 74TAL 01 300 25 7 AA 73TAL 01 300 30 RTNA 76GAU 01 300 40 7 RTNA 81iaJC 01 300 50 AA 75HIN 01 300 70 AA 80AGE 01 300 700 AA 76LAN 01 300 800 6 FAA 76LAN 01 310 RTNA 75STE 02

310 7 RTNA 81iaJC 01 310 11 FAA 81DAN 01 310 ICPES 85NAR 02

310 AF 85NAR 02

1577-7
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Cd (ng/q) cent.

310 20 FAA 78GR0 A401

310 40 ICPES 82AZI AH01

310 C A50 FAA BOPOL A401

320 FAA 83ATS 01

320 11 FAA 81DAN 01

320 40 11 AA 81BLA 03

320 130 6 FAA 76LAN 01

CCi DO RTNA /VPLA 01 Ten (to

1

1

IT tf*ACe

I CPcS ocJOH

ooU do ICPcS o^cVA U 1 380 6 DCPES 83FRA A4

390 1

1

T f*ACC* ICPES OCJOH A4

/ nA" 4UU / A 6 DCPcS OTCO A OJrKA U 1 550 450 AA 79M0N 01 560 130 34 CPXRF 78J0L 01

J (np/q)

13 17 UU 74MAS 01 18 4 RTNA 80SLO 01 21.5 RTNA 77LAU 02

22 RTNA 82LAU 01 25 3 RTHA 83TJI 01 46 14 RTNA 76GAU 01 74 28 RTNA 86TSU 01

1880 17 UU 74MAS 01

2155 170 34 CPXRF 78J0L 01

2410 600 EXRF 77NIE 01 2460 35 ITNA 81GLA 04

2480 17 UU 74MAS 01 2500 130 35 ITNA 81GLA 03

2530 ITNA 78CAP 01 2542 300 ITNA 77ZIK 01 2550 100 ITNA 74WES 01 2570 3110 R ITNA 79 1 MA 01 2570 3110 RD ITNA 79 1 MA 03

2590 17 UU 74MAS 01 2610 17 UU 74MAS 01 2610 200 ITNA 79CHA 02

2615 192 RTNA 74SCH 03

2632 67 ITNA 77GUI 02

2632 67 NAA 76MIL 02

2650 100 ITNA 80SLO 01 2680 80 RTNA 79WAR 02

2685 165 PAA 76KAT 04

2690 170 EXRF 80DYC 01 2700 70 ITNA 84GLA 02

Cone Uncer Com Method Reference

Cl (ug/g) cont.

2700 300 ITNA 84GLA 11 2715 151 ITNA 84ALK 01 2740 CPXRF 84KAU 01

ft 2750 ITNA 73NAD 01 2750 110 ITNA 78FUR 01 2760 ITNA 82AICA 01 2770 40 ITNA 86GRE 01 2793 294.4 NAA 76GUZ 01 2800

' 4 CA 150 lENA 84GLA 11 do30 200 HA A NAA 78GAN ft 4 01

•3AAA 2900 ITNA 80CRE ft 4 01 T AAA 3000 4 AA 100 TOGS 79FAI 01 ^ AAA 3000 4 AA 190 ITNA 77HAM ft 4 01 3200 OAA 800 CPXRF 79REN ftO 02

*ZC AA 3300 OAA 200 14NAA 81WIL ftO 02

1 1663 17 UU 74HAS ft 4 01

Co (ng/g)

1 "yn ICU 1 1

1 II

1

UU 7/ UA r4MAS A401 loU i A10 A C\f ASV OC Anc A4

1 iCO AA osncT AOU2

1 fU 1 1 NA 77u An A1

1 f\J lU U A A NAA 7QA A U roiiAN Ul

1 f U 1 1 NA 70AUA f VLHA Uc

1 7/ 1 71 f UU 7/.IJAC Ul

1 70 1 r O1/ rAA OULHA Uo

1 70 1 fO RTNA 701 lA D no

loU lU DTU A RTNA 77e* f i A1U3

in LI A A NAA 77f* T 1 A1Ul

t on i<50 Tn^0 T TU A

I TNA 70H IAD rVWAR A1Ul

loZ 14 FAA OAAU A oOCHA AOUo

loo 27 LI A A NAA 7£.M n A401

IVU 4 IcNA 7fWt lA A4Ul IVO OA20 6

T Tkl A ITNA 71 DCA A4Ul 190 OA20 A A AA D/ I^A Lt A1Ul

•iftft 200 4 4 1 1 SSMS O3V0S A4Ul

200 4 Z16 FAA 74WES A401 200 40 ITNA 80LAK 01 203 RTNA 75STE 02

210 ITNA 79KUC 01 210 10 ITNA 86CHI 01 210 20 ITNA 74WES 01 210 30 AA 79FLA 02

210 40 FAA 79WAR 0^ 217 13 ITNA 81KRI 01 220 RTNA 75ABU 01 223 11 RTNA 75LIE 01 223 11 RTNA 77LIE 01 225 17 UU 74MAS 01

1577-8
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Co (ng/q) cont.

225 7 COLOR 82KIR 01 230 20 RTNA 80SLO 01 230 20 6 ITNA 74BEC 01 230 100 ITNA 77ZIK 01 233 5 RTNA 790ER 01 236 9 ITNA 80MIC 01 240 CHEML 79MIL 01 240 ITNA 80CRE 01 240 10 ITNA 73C0R 01 240 10 ITNA 84ALK 01 240 14 lENA 75HAZ 01 240 20 RTNA 74HEN 01 240 30 ITNA 78BEH 01 240 37 ITNA 77HAM 01 245 7 RTNA 81KUC 01 246 14 RTNA 77TJI 01 247 31 ITNA 81M0L 01 248 25 ITNA 79ZEI 01 250 ITNA 82AKA 01 250 30 CHEML 81MAR 01 252 8 ITNA 86GRE 01 257 2 ITNA 74LIN 01 260 17 UU 74MAS 01 260 7 7 RTNA 81)(UC 01 260 10 ITNA 79SAT 01 260 21 RTNA 76GAU 01 265 AA 79ABU 01 269 30 AA 80JAC 01 275 FAA 82H0E 01 280 NAA 79MIL 01 290 ITNA 78CAP 01 300 ICPES 80HAA 01 300 ITNA 770SB 01 300 11 SSMS 85V0S 01 300 70 lENA 86CHI 01 310 60 RTNA 74SCH 03

310 120 14NAA 81UIL 02

310 120 14NAA 81UIL 01 340 17 UU 74MAS 01 360 60 ITNA 78FUR 01 370 60 RTNA 77MEL 01 390 17 UU 74MAS 01 400 FAA 75SLA 01 410 120 RTNA 77KUS 01

I

1577

Cone Uncer Com Method Reference

Cr (ng/q)

22 10 ICPES 81BLA 01 35 3 GC 81BLA 01 35 4 11 FAA 80KUM 01 44.9 5 11 RTNA 76PIE 01

51 17 UU 74MAS 01 53 9 FAA 74W0L 01 60 12 AA 80JAC 01 60 30 RTNA 74SCH 03

61 3 11 FAA 80KUH 01 72 8 11 ICPES 81BLA 02

72 13 ITNA 86GRE 01 74 5 RTNA 77LIE 01 78.9 11 NAA 79VER 01 80.6 11 NAA 79VER 01 85 9 RTNA 78GAL 01 85 9 7 RTNA 80GAL 02

88 7 RTNA 81KUC 01 88 8 11 FAA 80KUM 01 92 9 11 ICPES 81BLA 02

92 10 7 RTNA 81KUC 01 94 8 7 FAA 80CHA 01 94.8 19.5 11 RTNA 76PIE 01 96 8 RTNA 79TJI 01 98 5 RTNA 75LIE 01 115 42 RTNA 79PLA 01 120

j 120

40 ' AA 79FLA 02

70 ITNA 78BEH 01 123 6 RTNA 77LIE 01 130 17 UU 74MAS 01 130 ITNA 80CRE 01 130 30 RTNA 78G0E 01 130 50 RTNA 77TJI 01 133 12 ITNA 80MIC 01 140 17 UU 74MAS 01 144 23 7 FAA 80CHA 01 150 17 UU 74HAS 01 150 10 NAA 78GAN 01 150 30 ITNA 74D0N 01 160 5 11 RTNA 78MCC 01 160 60 RTNA 76GAU 01 163 10 RTNA 74MCC 01 180 100 CPXRF 78V IS 01 190 10 FAA 79WAR 01 200 20 DCPES 79REE 01 200 20 D DCPES 81REE 01 210 2 11 RTNA 78MCC 01 210 30 ITNA 78MCC 01 210 31 ITNA 748CC 01 210 40 ITNA 79WAR 01 210 70 RTNA 79WAR 02

280 200 ITNA 79SAT 01
TABLE 1577- 2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com —Method Reference

cont. 1 Cu (uq/q)

400 500 11 ICPES 82J ON 01 1 87 11 SSMS 85V0S 01 400 500 11 ICPES 82J0N 01 1 93 12 6 ITNA 74H0F 01 490 17 UU 74MAS 01 1 124 11 XRF 83PEL 01 500 3500 R ITNA 73NAD 01 1 138 18.8 FAA 74GR0 01 540 17 UU 74MAS 01 1 146 40 ITNA 77ZIK 01 600 ITNA 79KUC 01 1 148 19 FAA 77FUJ 01 870 60 CHEML 74LI 01 1 151 191 RD ITNA 79 1 MA 03

1000 400 FAE 83MAR 04 1 151 191 R ITNA 79IMA 01 1000 600 11 RTNA 76STE 01 1 153 CPXRF 78UEM 01 1160 600 ITNA 76STE 01 1 154 7 ICPES 85 FAS 01 1300 17 UU 74MAS 01 1 154 43 CPAA 77ZIK 01 1400 800 11 RTNA 76STE 01 1 161 12 RTNA 77KUS 01 1570 17 UU 74MAS 01 1 167 17 UU 74MAS 01 1600 11 SSMS 85V0S 01 1 167 XRF 80SUZ 02

1600 800 11 RTNA 76STE 01 1 168 8 1 ICPES 78SUD 01 1700 900 11 RTNA 76STE 01 1 169 7 12 FAA 85 CAR 02

1900 1000 11 RTNA 76STE 01 1 170 8 RTNA 80SLO 01 2000 11 SSMS 85V0S 01 1 173 17 UU 74MAS 01 2400 700 CPXRF 77WIL 02 1 173.5 13.9 34 CPXRF 78J0L 01 2700 FAA 83ATS 01 1 173.6 18.5 RTNA 83DAN 01 174 2 EXRF 80DYC 01 Cs (na/g) 1 175 17 UU 74MAS 01

1 176 9 6 ITNA 74H0F 01 9 4 ITNA 86GRE 01 1 177 1 AA 79MCQ 01 10 2 ITNA 80MIC 01 1 177 7 RTNA 77TJI 01 11.5 1 ITNA 81KRI 01 1 177 19 5 ITNA 80TOU 01 12 ITNA 81M0L 01 1 179 19 ICPES O / ni A A<l 84BLA 01

13 1 ITNA 77JUR 02 1 180 17 UU 74MAS 01

13 1 ITNA 78BEH 01 1 180 3 AA 73TAL 01

14 2 RTNA 75LIE 01 1 180 8 11 ICPES 81BLA 02

14.9 2.2 RTNA 77LIE 01 1 180 15 CPXRF 84BIS 01

15 17 UU 74MAS 01 1 181 11 SSMS 85V0S 01

15 2 RTNA 79UAR 02 1 181 17 UU 74MAS 01 16 3 ITNA 79SAT 01 1 181 124 ITNA 82KIM 01

16 4 RTNA 76GAU 01 1 182 6 1 ICPES Al lA A it 78SUD 01

18 9 ITNA 73C0R 01 1 182 8 7 RTNA 81KUC 01 19.2 17 UU 74MAS 01 1 182 13 CPXRF 81SAI 01 20 5 ITNA 86CHI 01 1 183 ICPES 84NAD 01 23 8 lENA 86CHI 01 1 183 2 7 RTNA A / r A A AA 84 FAR 02

24 ITNA 80CRE 01 1 183 8 35 RTNA 77GLA 01 30 6 ITNA 84ALK 01 1 183 8 PAA 76WIL 01 35 ITNA 73NAD 01 1 183 19 CPXRF 79MAN 01 40 11 SSMS 85VOS 01 1 184 5 SSMS 77PAU 01 44 17 UU 7/|JAC

f HnMa ni 1 U 1

1 184 6 12 FAA 85CAR 02

130 30 RTNA 77MEL 01 1 185 FAA 78CAP 01 180 10 7 RTNA 80GAL 02 1 185 3 7 RTNA 84FAR 02

185 3.3 6 DCPES 83FRA 01 185 6.8 11 RTNA 74UES 01 185 7 RTNA 78GAL 01

185 7 7 RTNA 80GAL 02

1 185 8 FAE 83MAR 04

1577-10
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Cu (ug/g) cont.

185 9 11 ICPES 82J0N 01 185 U AA 83RAP 01 186 ITNA 84GLA 11 186 2 ICPES 79MCQ 02

186 5.2 D AA 84 HUD 03

186 5.2 AA 84 HUD 01 186 5,5 11 FAA 74WES 01 186 5.5 6 CPXRF 77WIL 03

186 16 EXRF 77NIE 01 187 CPXRF 84KAU 01 187 7 RTNA 81KUC 01 187 2 2 FAA 84MIL 01 187 2.3 AA 80AGE 01 187 4 11 ICPES 81BLA 02

187 6 ITNA 78FUR 01 187 8 RTNA 75LIE 01 187 8 RTNA 77LIE 01 187 13 ITNA 74D0N 01 187.4 15.5 AA 79M0N 01 188 11 XRF 83PEL 01 188 1 ICPES 79MCQ 01

4 OA 188 3 RTNA 74HEN 01 188 6 AA 79FLA 02

188 6 HPLC 85SAI 01 188 9 AA 75HIN 01 188 n o 9.8 4 4

1

1

FAA 74UES n 4 01

4 OO 188 4 r\ 10 RTNA 79WAR 02

4 OO 188 4 n

10 ITNA 79UAR 01

4 on 189 ITNA 82AKA 01

4 on 189 1 1 XRF 83PEL 01

4 on 189 2 1 AA 77UCH 02

4 on 189 2 1 AA 77UCH 02

4 on 189 2 AA 801 ID 01

4 on 189 3.4 6 DCPES 83FRA 01 189 4

4 4

1 1 ICPES 82J0N 01

•1 OA 189 4 CPXRF 81 ROB 02

4 on 189 6 FAA 81CLE 01

4 on 189 7 ICPES 78JAC 01

4 on 189 4 O12 CPXRF 80KIR 01

4 on 189 20 EXRF 84KNA 01

4 nn 190 4 4 11 AA 81M0H 01 190 1 RTNA 80UOI 01 190 2 FAA 84HAR 02

190 3 FAA 79WAR 01 190 8 W 80SCH 05

190 10 ICPES 79ABE 01 190 14 ITNA 84ALK 01 190 15 ASV 81 DOG 01 190 24 ITNA 77HAM 01 191 6 NAA 72SIN 01 191 14 FAA 80CHA 08

1577-

Conc Uncer Com Method Reference

Cu (ug/q) cont.

191 11 FAA 81DAN 01

191 11 XRF 83PEL 01

191 6.2 11 RTNA 74WES 01

191 9 CPXRF 85CLA 01

191 10.5 NAA 76GUZ 01

191 34 XRF 77SMI 04

192 4 EXRF 79GIA 01 192 4 FAA 81CLE 02

192 6 ITNA 86GRE 01 192 8 ICPES 80SCH 08

192 9 6 FAA 76LAN 01 192 26 ICPES 84ZER 01 193 11 FAA 810AN 01 193 1 ICPES 85UOL 01 193 10 FAA 80LON 01 193 14 RTNA 77GIL 03

193 14 NAA 77GIL 01 193 14 7 RTNA 80GAL 02

194 17 UU 74MAS 01 194 17 UU 74MAS 01

4 n/ 194 FAA 75SLA 01

4 n/ 194 1 AA 75ABU A 4 01

4 n/ 194 3 ASV 85ADE A401 194 4 AA 82HAR A 4 01 194 6 ICPES 82EVA A 4 01

4 n/ 194 4 7

13 6 CPXRF TTWIL ATT 03

4 n/ 194 7 4 31 AA 79LAK A 4 01 195 6 POL 72SIN A 4 01 195 AE+AF 7ni II 1 79ULL A 4 01

4 nc 195 3 AA 79WAR 01 195 4 AA 80UCH 01

4 nc 195 5 RTNA 76GAU 01 195 4 A10 ICPES 81KNA 01

4 nz 196 ASV 83H0L A 4 01 196 4 / 14 FAA 80CHA AOOo

4196 RTNA 85TIA A 4 01 196 Z6 6 FAA 76LAN A 4 01 196 8 CPXRF 77UIL 02

4 nz 196 9 FAA ?'5SME A 4 01

4 nz 196 9 AA 81KRI 01 196 4 / ^

14.7 RTNA 79PLA A 4 01 196 28 RTNA 82KIM 01 197 NAA 78GAN 01 197 4 ITNA 79SAT 01 197 11 2 FAA 84MIL 01 197 13 6 POL 72SIN 01 197 16 CPXRF 80MAE 01 198 AA 80EVA 01 198 7 AA 82EVA 01 198 9 ITNA 79CHA 02

199 6 ITNA 80MAE 01
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Cu (ug/g) cont.

100 1

5

T TUA 1 1 NA ft/n OHuLAA onn 1 1

1 1 AM 0 inun u 1 DTUA TOnPD U 1 A oooun 71 r AM AADHC u 1

1 f ouMn ni

cu 1 1 7f DTUA K 1 NA 0/ CAD OHrAK n5

1 / 10 UDi r OObUN niu 1

1 . r f .y DTUA K 1 NA r r bUU niu 1 H

IT HrLL oDduN Ul

cw 1 Lrto OUHAA U1 0y

PDVD C LrXKr 7QV/ 1 C f OVl aniUl

cU<f 0y A A AA ft/. PI ID niu 1 0 AAA A 700 T U f ^ol N niu 1

3 DTUA K 1 NA 7/ PAW f hKAv ni

1

1

MoV ACV/ 0 1 UAN niu 1

1

1

1 1 MMAA 7AI r OLANAU niU 1 37 DTUA K 1 NA

T

1 rPFC l^r Co niU 1 210 12.5 FAA 75PIC 01 213 17 UU 74MAS 01 216 11 ASV 81DAN 01 216 22 32 CPXRF 77CR0 01

31 113

241 45 CPAA 78MCG 01

241 54 32 CPXRF 77CR0 01 241 65 CPXRF 76ZEI 01 270 90 14NAA 81UIL 02

tf?77f 1AIH MM 70MAT f tHA I n3

T AMAA ft1t IPU ni

' Cng/q)

nu . A0 PTUA 7AnAi 1 r OuAU ni

fi 1 u. 1 DTUA K 1 MM 00 1 oU ni

ing/gj

u . 3

1L K 1 NA fi?l Al 1 niu 1 u . 3

1L DTUA K 1 NA 7APAI

1

r OuAU niu 1 0.5 RTNA 77LAU 02

1 (ng/g)

0.235 0.024 RTNA 76GAU 01 0.3 0.04 RTNA 86TSU 01 0.35 RTNA 82LAU 01 0.35 RTNA 77LAU 02

0.4 0.1 RTNA 83TJI 01

3 ITNA 78CAP 01 140 ITNA 80CRE 01 310 ITNA 73NAD 01

1577-12

Cone uncer Com Method Reference

(ng/q)

40 20 fISc 83KNA 01 ISc 84GLA 02

e (ug/g)

3

A A AA 75HIN 01

1 ti 1 UU 74HAS 01

1 17 c3 IhNAA 81WIL 01

i«»y 1

1

XRr 83PEL 01 130 1

1

VD C XKr 83PEL 01 133 / QhV 1

1

1 A A AA 78G0R 01 100 5f A A AA 79HAN 01 Tor on80 12 E A C FAE 83MAR 04 one £03 CPXRF 78UEH 01 209 CO 1

1

ICPES 82J0N 01 220 16 RTNA 77MEL 01

1 1 UU 74HAS 01 22y 4 71 f

1 H 1 UU 74HAS 01 2jU Of CA A rAA 77FUJ 01 0

C A A rAA 84HAR 02

c3 DTUA K 1 NA 75LIE 01

c3 - DTUA K 1 NA 77LIE 01 3XO c^y 84NAD 01 3An 1 1 VDr AKr 83PEL 01 3An 1 1

1 11

1

UU 74HAS 01

3/ n 1 CVD C tXKr 80DYC 01

3/ n 1 312 K 1 NA 77TJI 01

3/ 1 Q 4

1 ICPcS 78SUD 01

3/ 3 2<»2

4 71 /

1 II 1 UU 74MAS 01

•5/ T 2<>3 , 14 C A A FAA 81 CLE 02

2h«» 2 iCPcS 79MCQ 02

3/ / z0 ILrba 79MCQ 01

3/ / i n10 A A AA 79MCQ 01

3/ 7 "7 CHf .3 A A AA 79LOC 01

2<»o 10 UrXRr 80MAE 01

3/ 0 2'»y DTUA K 1 NA 75STE 02

230 < 312 CPXRF 78V IS 01 230 3322 f TU A

1 1 NA 77HAM 01 OCT 232 f TUA I TNA 79KUC 01 232 oc23 ICPES 81BLA 01 253 FAA 78CAP 01 254 ICPES 78CAP 01 254 ( 2

C A A FAA 84MIL 01 255 08

T Tkl A

I TNA 79SAT 01 233 13 r TU A

1 INA 79ZEI 01 255 30 ITNA 78FUR 01 256 OES 75BOL 02

256 3 AA 801 ID 01 256 3 1 AA 77UCH 02

256 32 CPXRF 79MAN 01 257 ITNA 78CAP 01
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Fe (ug/g) cont.

257 11 XRF 83PEL 01 257 14 FAA 80CHA 08

257 30 32 CPXRF 77CR0 01 258 7 RTNA 81KUC 01 258 10 11 ICPES 82JON 01 259 12 11 ICPES 81BLA 02

260 CPXRF 84KAU 01 260.9 12.89 NAA 76GUZ 01

261 8 ITNA 86GRE 01

261 15 ICPES 85 FAS 01 262 ITNA 73NAD 01 262 7 ICPES 78JAC 01 262 7.7 6 DCPES 83FRA 01 262 10 FAA 81CLE 01 262 13 ICPES 79ABE 01 262 18 CPXRF 81SAI 01 263 12 ITNA 84ALK 01 263 12 CPXRF 81 ROB 02

264 3 11 ICPES 82J0N 01 264 4 2 FAA 84MIL 01 264 6 11 ICPES 82J0N 01 264 29 ITNA 78BEH 01 264 44 ITNA 86CHI 01 265 5 GC 81BLA 01 265 11 RTNA 79WAR 02

265 16 ITNA 74UES 01 265 19 ITNA 81KRI 01 265 25 NAA 78GAN 01 265 30 ITNA 79CHA 02

266 5 11 ICPES 81BLA 02

266 9 D ICPES 80SCH 08

266 9 ICPES 80SCH 05

266 10 11 AA 74WES 01 266 10 11 AA 78G0R 01 267 14 FAA 80CHA 08

267 5 EXRF 79GIA 01 268 8 FAA SOLON 01 268 24 EXRF 77NIE 01 268 25 1 ICPES 78SUD 01 268 38 W 79LAK 01 269 9 CPXRF 85CLA 01 269 10 ICPES 81KNA 01 269 12 ITNA 80LAK 01 270 ICPES 780AH 01 270 11 SSMS 85V0S 01 270 4.2 6 DCPES 83FRA 01 270 12 ITNA 73C0R 01 270 12 COLOR 78GOR 01 270 18 CPXRF 84BIS 01 270 20 7 RTNA 80GAL 02

270 20 NAA 77GIL 01 1577-1

Cone Uncer Com Method Reference

Fe (ug/g) cont.

270 47 ITNA 74D0N 01 271 6 ITNA 80MIC 01

271 27 ITNA 81M0L 01 271.5 11.5 34 CPXRF 78J0L 01 272 3 AA 82TIN 01 272 9.5 11 AA 74WES 01 272 15 7 RTNA 81KUC 01 272 27 RTNA 76GAU 01 272 71 XRF 77SMI 04

273 5 ITNA 8QMAE 01 273 8.5 6 CPXRF 77WIL 03

273 9 FAA 81CHA 01 273 10 AA 84CUB 01 274 5 AA 80UCH 01 274.5 28 PAA 76ICAT 04

275 4 13 HPLC 85BON 01 275 6 13 HPLC 85B0N 01 275 12 AA 83RAP 01 276 FAA 75SLA 01 276 2 1 AA 77UCH 02

277 2 ITNA 74LIN 01 277.9 16.7 6 ITNA 74BEC 01 278 AA 80EVA 01 278 14 CPAA 77ZIIC 01 279 20 RTNA 77GIL 03

280 AA 82UIL 04

280 11 SSMS 85V0S 01 280 30 ITNA 77ZIIC 01

281 2 ICPES 85WOL 01 282 ICPES 80HAA 01 282 26 ICPES 84ZER 01 283 60 CPAA 78MCG 01 283 68 CPXRF 76ZEI 01 285 17 UU 74MAS 01 287 17 CPXRF 77WIL 02

287 81 lENA 36CHI 01 289 52 32 CPXRF 77CR0 01 290 ITNA 80CRE 01 293 17 UU 74MAS 01 293 8 RTNA 80SLO 01 29i 8 ITNA 790AS 01 293 21 6 CPXRF 77WIL 03

300 31 12 FAA 85CAR 02

305 33 ICPES 84BLA 01 310 28 RTNA 74SCH 03

310 33 12 FAA 85CAR 02

315 ITNA 770SB 01 331 17 UU 74MAS 01 334 10 14NAA 81UIL 02

343 19 AA 82HAR 01 345 7 12 FAE 83MAR 04
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Fe (ug/g) cont.

1

1 Hg (ng/g) cont

350 64 RTNA 77KUS

1 01 1 16 1.2 FAA 72ROO 01 364 17 UU 74MAS 01 1 16 1.6 RTNA 79MAY 01 1395 AE+AF 79ULL 01 1 16 2 FAA 77GLA 03

U33 17 UU 74MAS 01 1 16 2 RTNA 77TJI 01

1 16 2 AA 79FLA 02

Ga (ng/g) 1 16 3 CVAA 80TON 01

1 16 3 7 RTNA 81KUC 01 < 240 L lENA 78UAN 01 1 16 5 CVAA 80KOR 01

< 500 L EXRF 79GIA 01 1 16.1 0.4 ITNA 86GRE 01

< 20000 L 14NAA 81UIL 02 1 16.2 0.08 RTNA 84DRA 01 4 RTNA 74HEN 01 1 16.2 3 14 FAA 74CHU 03

1100 700 CPXRF 77WIL 02 1 16.4 0.4 RTNA 74HEN 01

1 16.4 4.3 NAA 76GUZ 01 Gd (ng/g) 1 16.5 0.8 CVAA 72RA1 01

1 16.8 1.8 5 RTNA 80GRE 01 < 1.4 L RTNA 76GAU 01 1 17 2 RTNA 740RV 01 1.8 RTNA 82LAU 01 1 17 2 RTNA 79WAR 02

2.4 RTNA 77LAU 02 1 17 2 CVAA 82SUL 01

1 17 4 2 CVAA 79KNE 01 Ge (ng/g) 1 17.3 2.8 5 RTNA 80GRE 01

1 17.4 2 RTNA 82GRI 01 < 400 L EXRF 79GIA 01 1 18 2 RTNA 79CHA 02

1 18 3 RTNA 75LIT 01

H (%) 1 18 40 R* AA 83YAN 01

1 20 UU 74FEL 01 6.8 0.3 TCGS 79FAI 01 1 20 17 UU 74MAS 01 7 0.1 35 TCGS 79GLA 04 1 20 2 CVAA 77AND 01 7.12 0.1 CB 80SCH 02 1 20 5 CVAA 84BAR 02

22 1 RTNA 75LIE 01

Hf (ng/g) 1 22.1 6.3 14 FAA 74CHU 03

1 22.3 1.3 RTNA 77LIE 01

1 RTNA 80SLO 01 1 30 10 FAA 78EGA 01 7.3 ITNA 80CRE 01 1 41 17 UU 74MAS 01

i 47 4 RTNA 77MEL 01

Hg (ng/g) 1 200 21 ITNA 75LIT 01

13.7 1.4 14 FAA 74CHU

1 01 1 Ho (ng/g)

14 2 FAA 79ST0 01 1 14 2 CVAA 78MAT 01 1 < 0.94 L RTNA 76GAU 01

14.5 1.7 RTNA 72RAI 01 1 0.2 RTNA 82LAU 01

14.5 3.4 RTNA 72R0O 01 j 0.25 RTNA 77LAU 02

14.5 3.4 RTNA 72ROO 02 1 0.3 0.1 RTNA 86TSU 01 14.7 RTNA 75STE 02 1 15 2 MPOES 81 TAN 01 1 15 4 RTNA 74SCH 03 1 15.8 5.1 14 FAA 74CHU 03 1 16 7 RTNA 81KUC 01 1 16 CVAA 79TAG 01 1 16 CVAA 82GLA 02 1 T6 0.3 RTNA 83GRE 02 1 16 1 RTNA 74BYR 03 1 1577-14
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ng/g)

1

1 K (%) cont.

180 12 RTNA 77R00

1 01 1 0.95 0.05 CPXRF 80KIR 01

190 ITNA 84GLA 11 1 0.96 ITNA 79KUC 01

200 10 RTNA 79WAR 02 1 0.96 ITNA 73NAD 01

210 60 lENA 84FAR 01 1 0.96 0.06 AA 74WES 01

220 30 ITNA 79CHA 02 1 0.961 CPXRF 84KAU 01 221.8 14.8 RTNA 80GVA 01 1 0.964 CPXRF 76ZEI 01 230 40 lENA 84GLA 11 1 0.964 0.0244 ITNA 84ALK 01 237 lENA 85GAU 04 1 0.9645 0.0045 CPAA 78MCG 01 246 11 35 RTNA 81ALL 01 1 0.969 0.022 FE 80UCH 01 249 12 34 RTNA 81ALL 01 1 0.969 0.09 ITNA 79CHA 02

249 12 RTNA 81STR 01 1 0.969 0.091 PAA 76KAT 04

251 16 RTNA 83ALL 01 1 0.9695 0.0785 ITNA 74D0N 01 270 30 lENA 82SAT 01 1 0.97 0.05 11 ICPES 82JON 01 280 NAA 79HEC 01 1 0.979 0.024 12 FAA 85CAR 02

280 10 MS 85SCH 01 1 0.979

0.98

0.028

17

WXRF

UU

84ALK

74MAS

01

01

1 (nq/q) 0.98

0.98

0.008

0.026

FAA ITNA

84HAR

86GRE

02

01

< 1000 L RTNA 76GAU 01 1 0.98 0.1 ITNA 82EHM 01 0.05 RTNA 74RAV 01 1 0.9875 17 UU 74MAS 01 0.09 0.01 RTNA 78K0B 01 1

1

0.99

0.99

0.02

0.02 11

ITNA ICPES80MIC

82J0N

01

01 m 1

1

0.99

0.992

0.03

0.022

CPXRF

AA

84BIS

75HIN

01

01 0.5 0.07 CPXRF 80MAE 01 1 0.9984 0.0648 NAA 76GUZ 01 0.63 0.11 14NAA 81WIL 01 1 1.00 ITNA 770SB 01 0.6674 0.0662 RTNA 74SCH 03 1 1.00 0.01 2 FAA 84MIL 01 0.7 CPXRF 78UEM 01 1 1.00 0.03 TCGS 79FAI 01 0.7 11 SSMS 85VOS 01 1 1.006 1 AA 78SZY 01 0.725 0.789 RD ITNA 79 1 MA 03 1 1.01 0.18 ITNA 77HAM 01 0.725 0.7898 R ITNA 79 1 MA 01 1 1.015 1 AA 78SZY 01 0.742 ITNA 78CAP 01 1 1.02 0.01 RTNA 80UOI 01 0.7537 17 UU 74MAS 01 1 1.02 0.012 ITNA 78FUR 01 0.76 11 SSMS 85VOS 01 1 1.02 0.03 AA 82HAR 01 0.821 17 UU 74MAS 01 1 1.021 0.048 34 CPXRF 78J0L 01 0.84 0.13 32 CPXRF 77CR0 01 1 1.0323 0.0258 RTNA 77LIE 01 0.85 0.02 CPXRF 85CLA 01 1 1.0323 0.0258 RTNA 75LIE 01 0.87 0.13 ITNA 84GLA 02 1 1.04 0.03 ITNA 74WES 01 0.875 ITNA 80CRE 01 1 1.05 0.01 ICPES 85U0L 01 0.904 17 UU 74MAS 01 1 1.05 0.02 ICPES 85WHI 02

0.91 ICPES 84NAD 01 1 1.06 35 ITNA 81GLA 04

0.91 0.08 RTNA 79WAR 02 1 1.06 0.08 NAA 78GAN 01 0.92 1 lENA 79KUC 01 1 1.087 0.124 CPXRF 79MAN 01 0.92 0.01 2 FAA 84MIL 01 1 1.12 0.02 ITNA 80SLO 01 0.92 0.028 CPXRF 81 ROB 02 1 1.13 0.04 EXRF 80DYC 01 0.93 0.05 CPXRF 77WIL 02 1 1.15 0.06 ICPES 84BLA 01 0.93 0.11 EXRF 77NIE 01 1 1.18 0.1 14NAA 81WIL 02

0.935 ITNA 82AKA 01 1 1.2 0.22 FAE 83MAR 04

0.94 0.05 ITNA 80MAE 01 1 0.948 17 UU 74MAS 01 1 0.948 17 UU 74MAS 01 1 1577-15
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

1 (ng/g)

10 1 RTNA 74HEN 01

12 9 RTNA 74SCH 03

14 5 RTNA 80SLO 01 17 RTNA 75LIE 01 17 RTNA 82LAU 01 17 RTNA 77LAU 02

17 2 RTNA 83TJI 01 17.3 0.4 RTNA 77LIE 01 20 ITNA 73NAD 01 24.5 1 .2 RTNA 76GAU 01

31 1 RTNA 86TSU 01 62 5 ITNA 79CHA 02

70 ITNA 78CAP 01 72 ITNA 80CRE 01

164 26 AA 85EVA 01

1 (ng/q)

< 0.02 RTNA 83TJI 01

< 0.1 L RTNA 76GAU 01 0.039 RTNA 77LAU 02

0.039 RTNA 82LAU 01

(ug/g)

290 40 14NAA 81WIL 01 332 541 R ITNA 79 1 MA 01 332 541 RD ITNA 79 1 MA 03

450 11 SSMS 85V0S 01 516 17 UU 74MAS 01 517 17 UU 74MAS 01 555 12 2 FAA 84MIL 01 555 21 1 ICPES 78SUD 01 558 11 ITNA 84ALK 01 566 FAA 78CAP 01 566 10 AA 79MCQ 01 567 AA 79L0C 01 573 4 ICPES 79MCQ 02

573 17 ICPES 79MCQ 01 580 20 CPXRF 80KIR 01 588 ICPES 84NAD 01 590 40 ICPES 79ABE 01 593 10 AA 801 ID 01 593 10 1 AA 77UCH 02

593 49 AA 82HAR 01 594 13 2 FAA 84MIL 01 595 6 6 AA 76H0W 01 596.5 13.5 PAA 76KAT 04

1577-

Conc Uncer Com Method Reference

Mg (ug/g) cont.

597 10 AA 75HIN 01 598 14 ITNA 75PIE 01 598 50 ITNA 77ZIK 01 600 9 1 AA 77UCH 02

601 5 ICPES 85UOL 01 601 6 6 AA 76H0W 01 602. 11 AA 80UCH 01 604.6 26.84 NAA 76GUZ 01 605 32 AA 74WES 01 608 6 RTNA 79UAR 02

608 6 ITNA 79WAR 01 609 AE+AF 79ULL 01 610 15 FAA 79WAR 01 613 ICPES 78CAP 01 616 19 ICPES 85WHI 02

618 10 RTNA 80UOI 01 620 20 ITNA 79CHA 02

629 6.7 6 DCPES 83FRA 01 629 12.3 6 DCPES 83FRA 01 636 ICPES 780AH 01 638 34 UXRF 84ALK 01 650 60 ITNA 86GRE 01 657 9 11 ICPES 82J0N 01 658 48 ICPES 84BLA 01 659 82 ITNA 74WES 01 660 20 1 J ICPES 82JON 01 668 42 AA 79LAK 01

Of H

1 7 1 II

1

UU 7/.IIAC niUl 684 110 ITNA 78FUR 01 700 20 14NAA 81WIL 02

700 130 ITNA 77HAM 01 712 98 1 ICPES 78SUD 01 720 ITNA 84GLA 11 949 ITNA 78CAP 01 1040 ITNA 73NAD 01

In (ug/g)

5.3 0.72 6 ITNA 74HOF 01 7.7 FAA 83ATS 01

8 1 CPXRF 80MAE 01 8.4 2.1 CPXRF 80KIR 01 8.5 2.6 ICPES 82AZI 02

8.73 FAA 77SHE 02

9.00 0.37 FAA 74GR0 01 9.0 0.7 W 80SCH 05

9.0 0.7 D ICPES 80SCH 08

9.0 2.2 6 CPXRF 77WIL 03

9.12 17 UU 74MAS 01 9.14 ITNA 73NAD 01 9.2 11 SSMS 85VOS 01
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/q) cont. Mn (ug/g) cont.

9.2 0.7 AA 79FLA 02 1

4 A 4 10.1 1 .

1

ITNA Trtr* AT A 4 /VSAT 01 9.2 0.9 1

1

ICPES 81BLA 02 [ 10.1 1 .2 CPXRF 81 ROB 02

9.2 1.1 12 FAA 85CAR 02 1

4 A 4 10. J 7 £. 3.6 EXRF 77m f c A1

1 IHlC 01 9.2 1 .8 6 CPXRF 77WIL 03 1

4 A 4 C 10.15 •> 1 c 2- 15 nA A PAA 7^I^AT A/ foKAT 04

9.26 0.85 RTNA 79PLA 01 1

4 A 4 7

10.17 A0.69 M A A NAA /oGUZ 01 9.3 ITNA 82AKA 01 1 10.2 1 7 UU 7/ b4 A O A

1

01 9.3 A C 0.5 CPXRF 84BIS 01 1 in o 10.2 1 7 UU 7/ U A C A

1

^4MAS 01 9.4 A <t 0.1 7 RTNA 84 FAR 02 1

4 A •> 10.2 ASV Oft ft Lin ftl oOCMR 01 9.4 A 7 0.3 RTNA 83DAN 01 1

4 A T 10.2 A 4 0.1 Am oOI on T TIDA m01 9.4 1.1 EXRF 79GIA 01 1

1 A O 10.2 A0.2 AA 7C U T III A 4 fbnlH 01 9.42 17 UU 74MAS 01 1

4 A ^ 10.2 A / 0.4 ICPES 82EvA 01 9.44 1 . 16 FAA 84HAR 02 1 10.2 0.45 1 1 RTNA r4WES 01 A C 9.5 17 UU 74MAS 01 1

4 A 1 10.2 1 1 AA 7AJCH 02

9.5 A C 0.5 ITNA 82KIM 01 1

4 A 17 10.23 A / 7 0-45 RTNA "7/ n n\i A4 <'4RAV 01 9.5 ft 7 0.7 4 4

1

1

ICPES 81BLA 02 1

4 A 7 10.3 A "5 0.2 ITNA o2EHM 01 9.5 4 /

1 .4 CPXRF 77WIL 02 1

4 A 7 10.3 A "5 0.2 ICPES ODWOL 01 9.6 A / 0.4 RTNA 74HEN 01 1

4 A 7 10.3 A 1 0.2 AA OCl/n 1 ft 1 odKOJ 01 y.6 0.5 RTNA 77KUS 01 1

4 A 7 10.3 ft 7 0.3 FAA o2CLE 01 y.6 A ^ 0.6 1

1

IT A A FAA 74WES 01 1 10.3 A 7 U.3 r A A FAA Q 1 ft 1 c AO o1CLc 02

y. 1 ICPES 78CAP 01 1 in 7 10.3 A 7iC U.3o 1 1 f A A FAA 7/ I lr"c» A

1

f4WES 01 O 7 V.f 1 1 ccuc bans 85V0S 01 1 1U.3 A 77 I TNA 77LIAU A1 f f HAM 01 O "7 A T CPXRr 85CLA 01 1 in T 10.3 A Q RTNA 7^ ft A II A

1

^oGAU 01 9.7 A 7 0.3 1 ICPES 78SUD 01 1

4 A 7 10.3 1 FAA OAt A4 oOLON 01

ft T 9.7 ft O O.B 1

1

ICPES 82 J ON 01 1

4 A / 10.4 FAA TOf^A A A 4 78CAP 01

1 .^6 ICPES 82AZI 01 1

4 A / 10.4 M o2CLE 01 V.lf A 70 0.79 ITNA 74DON 01 1

4 A / 10.4 ft I 0.2 FAA o2Ci.E 01 y .o 1 .

1

C A A FAA 82GR0 01 1 in / 10.4 A A A rAA 7Cft T ft A i OPIC 01 y.y ICPES 780AH 01 1 in / 10.4 A 7 0.3 1 AA 771 Iftu ftO

! AJCK 02

y.y i 7 UU 74MAS 01 1 in / 10.4 ft / 0.4 RTNA 77DI lA n 4 7fBU0 01 y.y A 7 COLOR 84HIR 02 1 in / 10.4 A / 0.4 1 1 ICPES o2uOn 01 y.y A / 7 0.4r ITNA 74WES 01 1

4 A / 10.4 A £. 0.6 1 1

1 1 FAA OSME 01 y.y A Q u.y ICPcS 85UHI 02 1 in / 10.4 1 . 1 RTNA 7/ eft LI A7 f4SCH 03

y .ys A OO ITNA 86GRE 01 1

4 A C 10.5 1 1 XRF OTnc 1 A 4 83PEL 01 lU ITNA 81GLA 04 1

4 A C 10.5 ft 1 U. 1 1 RTNA O / E A n AO o4FAR 02

1 n1U C A A FAA 75SLA 01 1 in c 10.5 A 1 U. 1 7( RTNA O/ TAD ftO o»»FAR 02

1 n1U 1

1

A A AA 81M0K 01 1 in c 10.5 A RTNA OAl lA F A 4 oOv/Oi 01

i A A 1U.U A C 0.5 NAA 78GAN 01 1

4 A C 10.5 ft 7 0.3 1 1 ICPES OO mhi A4 o2J0N 01

i A A A £ 0.6 6 ITNA 74H0F 01 1

4 A ET 10.5 ft z 0.6 AA 07n A A A 4 o3RAP 01

1 A A A 7 0. 1 ITNA 79WAR 01 1

4 A C 10.5 ft £. 0.6 ITNA O / ^ 1 A AO 54GLA 02

1 A A 1U.U A 7 0. r RTNA 79WAR 02 1

4 A C 10.5 1 . 1 ITNA f9CHA 02

1 A fl1 ICPES 79MCQ 01 1

4 A C 10.5 16 6 FAA 7Z n A bi A 4 76LAN 01

i A10 1 ICPES 79MCQ 02 1

4 A ^ 10.6 A 4 4 o.n 6 DCPES 0*3 p n A A 4 83FRA 01

i A A 10.0 « 7 1 .3 ICPES 79ABE 01 1

4 A Z 10.6 A 4 A 0.19 D AA 84 HUD 03

i AlU £ EXRF 80DYC 01 1 10.6 ft -1 ft 0.19 AA O/ IJI it\ A 4 o4HUU 01

i AlU AA 7M AM 01 1

1 10.6 ft '5 0.2 ICPES 07eftU ft/ o3SCH 04

1 A 1 CPXRF 84KAU 01 1 10.6 A 7 A A FAA 0 1 ft 1 ft i mCLE 01 10.1 ITNA 84GLA 11 1 10.6 1.1 ITNA 78FUR 01

10.1 0.1 AA 82CLE 01 1 10.7 0.3 ITNA 80MAE 01 10.1 0.2 ITNA 80SLO 01 1 10.8 0.15 6 DCPES 83FRA 01 10.1 0.5 11 RTNA 74WES 01 1 10.8 0.2 2 FAA 84MIL 01 10.1 0.6 2 FAA 84MIL 01 1 10.8 0.3 RTNA 82KIM 01

1577-17
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

1 (uq/g) cont.

1

1 Mo (ug/g) cont.

1 2.97 17 UU 74MAS 01 10.8 0.8 FAA 79WAR 01 1 3 ITNA 73NAD 01 10.8 20 6 FAA 76LAN 01 1 3.0 0.2 RTNA 830AN 01 10.9 1.2 CPXRF 79MAN 01 1 3.0 0.3 RTNA 77GIL 03

10.9 1.5 34 CPXRF 78J0L 01 1 3.0 0.3 NAA 77GIL 01 10.9 2 XRF 77SMI 04 1 3.0 0.3 7 RTNA 80GAL 02

11 AA 80EVA 01 1 3.04 0.18 lENA 75MAZ 01

11 17 UU 74MAS 01 1 3.06 0.7 34 CPXRF 78J0L 01

11 11 AA 81M0H 01 1 3.1 FAA 79BEN 01

11 ICPES 84NAD 01 1 3.1 1 lENA 79KUC 01 11.0 0.4 FAA 81CHA 01 1 3.1 0.03 RTNA 80KUL 01 11.0 0.4 AA 82EVA 01 1 3.1 0.5 11 ICPES 82J0N 01 11.0 0.7 ICPES 84ZER 01 1 3.12 0.26 RTNA 78NAD 01

11.1 1.6 AA 82HAR 01 1 3.19 0.14 RTNA 77LIE 01 11.1 2.1 ICPES 85 FAS 01 1 3.19 0.14 RTNA 75LIE 01 11.2 0.5 RTNA 77LIE 01 1 3.2 ITNA 79KUC 01 11.2 0.5 RTNA 75LIE 01 1 3.2 0.1 RTNA 77DIK 01 11.2 0.7 FAA 84R0S 01 1 3.2 0.11 ITNA 86GRE 01 11.2 1.4 1 ICPES 78SUD 01 1 3.23 0.09 SSMS 77PAU 01 11.4 0.8 11 FAA 75SME 01 1 3.3 0.2 RTNA 79WAR 02

11.4 3.7 12 FAA 85CAR 02 1 3.3 0.3 11 RTNA 74UES 01 11.5 17 UU 74MAS 01 1 3.31 0.09 COLOR 85EVA 02

11.5 ITNA 78CAP 01 1 3.33 RTNA 75STE 02

11.5 13.7 RD ITNA 79 1 MA 03 1 3.39 0.24 POL 84NAG 01 11.5 13.7 R ITNA 79 1 MA 01 1 3.4 1 lENA 79KUC 01 11.7 0.7 FAA 79WES 01 1 3.4 0.1 11 ICPES 82JON 01 12 2.6 ITNA 84ALK 01 j 3.4 0.15 FAA 74WES 01 12.5 2 DCPES 79REE 01 1 3.4 0.2 RTNA 80SLO 01 12.5 2 D DCPES 81REE 01 1 3.4 0.2 7 RTNA SIKUC 01

13 AE+AF 79ULL 01 1 3.4 0.36 RTNA 82BYR 01

13 3 ITNA 77ZIK 01 1 3.4 0.7 5 ITNA 80TOU 01

13 6 TCGS 79FAI 01 1 3.42 0.11 RTNA 80VER 01

14 1 AA 79MCQ 01 1 3.42 0.11 11 RTNA 81C0R 01 14.2 1.8 FAA 77FUJ 01 1 3.42 0.2 COLOR 83MAT 02

19 XRF 80SUZ 02 1 3.5 RTNA 84BYR 01 19 9 CPXRF 78V IS 01 1

1

3.5

3.5

0.2

0.6

11 RTNA

CPXRF

74UES 01 77RIN 01 (Uq/q) 1

1

3.5

3.6

1.5 CPXRF

RTNA

77WIL 02

85TIA 01

1.81 0.07 FAA 84G0H 01 1 3.6 0.14 11 RTNA 81 COR 01

2 ICPES 79MCQ 02 1 3.6 0.7 RTNA 74SCH 03

2 1 CPAA 77ZIIC 01 1 3.6 0.9 CPXRF 80MAE 01 2.2 0.9 CPXRF 80KIR 01 1 3.7 0.4 14NAA 81UIL 02

2.3 11 SSMS 85VOS 01 1 3.71 0.25 RTNA 77TJI 01 2.5 17 UU 74MAS 01 1 3.78 0.356 NAA 76GUZ 01 2.5 0.1 ITNA 78FUR 01 1 3.8 ICPES 80HAA 01 2.6 0.4 14NAA 81UIL 01 1 3.8 7 RTNA 81KUC 01 2.8 17 UU 74MAS 01 1 3.9 0.42 RTNA 84M0K 02

2.8 ICPES 84MIA 01 1 4.1 0.4 CPXRF 78VIS 01 2.89 0.45 lENA 86CHI 01 1 4.3 1.2 ITNA 79ZEI 01

2.91 0.14 ITNA 80MIC 01 1 4.9 17 UU 74MAS 01

2.95 0.27 RTNA 76GAU 01 1 5.8 0.3 AA 79FLA 02

1577-18
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

N (X)

1

1 Na (uq/g) cont

.

in 7c lU. j3 U. O 1 Lud 79FAI

1 01 1

1 TUA 1 1 NA 78CAP 01 n A JJ 1 Luo 79GLA 04 1 1 An DTUA K 1 NA 79WAR 02

10.42 0.11 CB 80SCH 02 1 2454 135 ITNA 84ALK 01 in so n c\L Urmv 74CAR 01 1 2ASS 11 MM 78SZY 01 10.59 0.04 D GRAV 74CAR 05 1 2462 502 12 FAA 85CAR 02

in fti n 2A V UTN 1 74CAR 05 1 7An c

!^ A A 84MIL 01 in 09 n OL UTN

1

74CAR 01 1 9"jf»n

1 ^n

f TUA 1 1 NA

U A A NAA

80MIC

78GAN

01

01 Na (ug/g) 1

1

1 A A Am

T TUA 1 1 NA

78SZY

81GLA

0104

1 uiy 1 II

1

74MAS 01 1 ^D>U ion lyu T TU A

I 1 NA 78BEH 01

1 \JC. 1 ioly o

T TkIA

1 1 NA 74H0F 01 1 1 T CU A IcNA 79KUC 01

1 Ann inn lUU 1 AUAA 81UIL 01 1 171 /

1 II

1

74MAS 01

j\j f TilA 1 1 NA 80SLO 01 1 CD f\J ft7n or U

CA A PAA 84HIL 01 iOAn 1 you An 1 1 NA 78FUR 01 1 9Ano UA A NAA 76GUZ 01 isn i/UA A IHNAM 81UIL 02 1 20 DTUA K 1 NA 75LIE 01 ?nnn snn roypp l*r ak r 80KIR 01 1 9A"? 5 30 DTUA K 1 NA 77LIE 01

T TUA 80CRE ()1 1 579n ion lyu 85UHI 02

C 1 r O 77 o T1 TUA 1 nn 74H0F 01 1

T TUA 1 1 NA 84GLA 11 p??n 17 1 II

1

UU 74MAS 01 1 57AA 1 c;a DTUA K 1 NA 74SCH 03

?nn T TUA 1 1 NA 77ZIK 01 1

1 u 1 LrCs 84BLA 01 ?in T TUA 1 1 NA 77HAM 01 1 71 nn r TU A I 1 NA 770SB 01 17 1UUH 1 74MAS 01 1 71J 1 nnUU Ann 79FAI 01 ?5^n T TUA 1 1 NA 84GLA 02 1 X7n 1 TUA 1 1 NA 77JUR 02 1 NO (nq/Q}

55An 1 1

T PUA CNA 79KUC 01 1 ??An ?nn T

I TUA 1 Nn 82SCH 05 1 oy DTUA K 1 NA 82LAU 01 2300 ICPES 84NAD 01 1 14,5 RTNA 77LAU 02

C.OJKJ KU 1 TUA 1 Nn 79 1 MA 03 1 1

A

1

0

/H DTUA K 1 NA 83TJI 01 2300 2RS0 p TTMA 1 1 Tin 79 1 MA 01 1 i7n 1 r U L(\ DTUA K 1 WM 76GAU 01 2310 TX TUA 1 nn 79KUC 01 1 2320 40 nnAA 75HIN 01 1 U 1 f nn / A

\

2320 300 I CO 79ABE 01 1 2330 60 TTMA 1 1 nn 74UES 01 1 An 1L 82JON 01 2340 171 f nil UU 74MAS 01 1 Anou MMAA 82EVA 01 2340 2S0 MAAA 82HAR 01 1 Anou 1L 1 Urco 82J0N 01 121 c FAA rAA 85CAR 02 1 i2n 1 cu T TU A 1 1 NA 80MIC 01

T

1 TUA 1 NA 82AKA 01 1 Rnn T TUA 1 1 NA 75PIE 01

T TUA 1 1 NA 86GRE 01 1 ^nn jUU 1 PDCC 79ABE 01 277n 17 1 II

1

UU 74MAS 01 1 < jUU L

fcl A A NAA 76GUZ 01 An DAKAAA 76KAT 04 1 inn jUU 1L t AKr 77NIE 01 2300 20 1 UrCo 85UOL 01 1 ^on PDVD C LrAKr 84KAU 01 TC T

1 TUA 1 NA 81GLA 03 1 7nn f UU L DTUA K 1 NA 76GAU 01 2400 TTMA 1 1 Nn 73NAD 01 1 7?n t DTUA K 1 NM 81KUC 01 2400 200 MMAA 74WES 01 1 ouu JL CAKr 79GIA 01 2400 350 FAr iMC 83MAR 04 1 innn 1 uuu PTUA K 1 NM 77MEL 01

1 U in DTkl A K 1 NA 74HEN 01 1 < yuuu

1L

1 / kl A A ihNAA 81UIL 01 2420 50 FE 80UCH 01 1 50 AA 78EVA 01 2425 17 UU 74MAS 01 1 50 50 ICPES 82EVA 01 2426 130 ITNA 74D0N 01 1 62 18 lENA 75MAZ 01 2430 150 ITNA 79CHA 02 1 70 30 AA 79FLA 02

1577-19
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Ni (ng/g) cont.

155 19 FAA 80DOR 01 180 20 PAA 79CHA 02

195 GC 85MEY 02

200 10 ASV 85ADE 01 200 30 RTNA 79WAR 02

210 ITNA 73NAD 01

227 VOLT 81PIH 01 270 120 RTNA 77TJI 01 470 7 RTNA 81ICUC 01 520 150 lENA 86CHI 01 600 400 CPXRF 78V IS 01 700 500 CPXRF 77UIL 02

1000 500 RTNA 80SLO 01 1000 690 AA 79M0N 01 1200 100 EXRF 80DYC 01 1300 200 CPXRF 79REN 02

(%)

0.31 0.1 CPXRF 79REM 02

0.64 0.06 14NAA 81UIL 01 0.816 0.64 EXRF 77NIE 01 0.905 NAA 78GAN 01 0.93 ICPES 84NAD 01 0.98 ICPES 78CAP 01 0.9891 0.0465 1 ICPES 78SLI0 01 1.0009 0.026 1 ICPES 78SUD 01 1.04 0.06 6 FAA 81 LAN 01

1.1 0.006 COLOR 79MCQ 01

1.1 0.02 6 FAA 81 LAN 01

1.1 0.15 14NAA 81UIL 02

1.13 0.03 ICPES 79MCQ 01 1.14 CPXRF 84KAU 01 1.152 0.004 ICPES 84PRI 01 1.16 0.01 ICPES 85WOL 01 1.16 0.03 ICPES 79ABE 01 1.18 0.03 11 ICPES 82J0N 01 1.18 0.05 ICPES 84BLA 01 1.2056 0.065 WXRF 84ALK 01

1.21 0.01 11 ICPES 82J0N 01 1.235 0.241 lENA 84ALK 01 1.24 0.02 ICPES 85UHI 02

1.3 0.1 CPXRF 80)CIR 01 1.3498 0.029 NAA 76GUZ 01

1577-20

Cone Uncer Com Method Reference

Pb (ng/g)

200 11 SSMS 85VOS 01 240 80 FAA 77FUJ 01 250 AA 78EVA 01 250 40 AA 82EVA 01 262 17 UU 74MAS 01 270 20 11 ASV 84ADE 03

280 40 AA 80AGE 01 290 20 11 ASV 84ADE 03

300 FAA 79YAS 01 300 20 11 ASV 84ADE 03

300 40 FAA 78GR0 01 300 100 CPXRF 78V IS 01 300 300 11 ICPES 82JON 01 310 20 VOLT 840ST 01 320 14 FAA 80CHA 08

320 13 FAA 75PIC 01 320 30 11 ASV 84ADE 03

320 60 FAA 79WAR 01 328 16 11 IDMS 74CH0 02

330 AA 77FRI 01 330 9 FAA 83STE 05

330 10 FAA 80P0L 01 330 10 FAA 790AB 02

330 20 AA 83RAP 01 330 700 AA 76LAN 01 333 67 11 IDMS 74CH0 02

340 11 FAA 81 DAN 01 340 20 AA 79FLA 02

340 20 AA 85ADE 02

340 20 11 ASV 84ADE 03

340 40 FAA 76HAD 01 343 23 FAA 76K0I 01 343 23 AA 76ZAN 02

350 AA 84KAN 01 350 15 FAA 81CHA 01 350 20 FAA 82ATS 02

350 22 6 FAA 76LAN 01 350 40 AA 79UAR 01 350 50 FAA 75BEH 01 350 50 D FAA 80SCH 08

350 50 FAA 81KNA 01 350 50 AA 80SCH 05

360 11 FAA 81DAN 01 360 12 6 FAA 76LAN 01 360 25 6 POL 72SIN 01 360 30 FAA 79ST0 01 360 30 SSMS 77PAU 01 370 AA 82UIL 04

370 ASV 82GAJ 01 380 FAA 83ATS 01 380 ICPES 80HAA 01
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Pb (ng/g) cont.

1

1

1

Rb (ug/g) cont

380 FAA 82H0E 01 1 10. 1 LPXKr 81 ROB 02

380 FAA 80CHA 08 1 lo.o 1

f ETU A IcNA 79KUC 01 380 FAA 82VAN 01 1 16.

o

1 O 1 .y 6 CPXRF 77WIL 03

380 ASV 74C0P 01 1 16.

y

ITNA 79KUC 01 380 76 ASV 79ST0 01 1 17 0.7 ITNA 80MIC 01 390 6 POL 72SIN 01 1 If

m

1 cwn c cXRF 80DYC 01 390 n A CI/ ASV 810AN 01 1 If ts 1 TNA 77ZIK 01 390 1

1

ASV 81DAN 01 1 1 r .H 1 o 1 .B kl A A NAA 78GAN 01 390 40 C A A FAA 84R0S 01 1 1 f . le.

1 n 1 .B f TU A

I TNA 81M0L 01 400 30 o ULrto 83FRA 01 1

1 r .o f TU A1 1 NA 78CAP 01 400 50 DA A PAA 79CHA 02 1

1 7 07 1 f .y( ft / o T TU A

1 TNA 86CHI 01 400 100 DA A PAA 74LUT 01 1 17 07 u.o DTUA K 1 NA 75LIE 01 400 300 1

1

1 I PDCC 1 Urtb 82J0N 01 1 17 07 u.o DTUA K 1 NA 77LIE 01 420 140 LrAKr 78J0L 01 1 in T TU A I 1 NA 770SB 01 430 130 1 PDCC 1 LrCO 82EVA 01 1 lo U.J DTUA K 1 NA 79UAR 02

450 30 CA A rAA 80LEG 01 1 IBlo n fl u.o T TU A 1 1 NA 79SAT 01 460 130 r A A rAA 74GR0 01 1 Ifi IB 1

1 f*DVD C LPXKr 77WIL 02

480 50 O OCPcS 83FRA 01 1 10 1 IB. 1 U.6 i / U A A IhNAA 81WIL 01 490 zO

C A A rAA 82KOI 01 1 lO /. ft / U.H CVD C tXKr 79GIA 01 490 o

C A A rAA 81HIN 01 1 Ifi / 1B.H ft 7 U. ff TU A

1 1 NA 86GRE 01 500 75B0L 02 1 lo.H C

T TU A

I 1 NA 81KRI 01 500 o

C A A rAA 82KOI 01 1 Ifi C IB.

3

ft / T Tkl A

1 TNA 74LIN 01 500 zO

C A A rAA 81HIN 01 1 1 n i/i ftu.ya U A A NAA 76GUZ 01 520 17 1 II

1

74MAS 01 1 1ft LJ ft cfi f CU A IcNA 86CHI 01 530 T PDCC 85NAR 02 1 Ifl lo. 71

1

7

1 /

1 II

1

UU 74MAS 01 3900 1000 UrAK r 77WIL 02 1 1ft lO. 7r nU.C7 f TUA 80LAIC 01 5000 81UIL 01 1 1ft lo. 7f Urn J

1 TUA 1 1 NA 78FUR 01 43000 4000 rMM 79WES 01 1 1ft lo. 7r nu.yo c T TUA 1 1 NA 80TOU 01

lo. r 11 f

1 TUA 1 NA 73C0R 01 Pr (ng/q) 1 Ifl lo. 7r 1 « 1 . J

T TkIA 1 1 NA 79CHA 02

1 Ifl lo. 7r CAKr 77NIE 01 < 3

1L DTUA K 1 NA 82LAU 01 1 Ifl 1o.ofl nu.oftRJ

T TUA 1 1 NA 84ALK 01 4 DTUA K 1 NA 77LAU 02 1 Ifl fl lO.O 1 T 1 .o DTUA K 1 NA 76GAU 01 4 2 K 1 NA 86TSU 01 1 Ifl fl lO.O 1 /. 1 .«f

r TUA 1 f NA 79LAK 01 4.6 0.3 DTM A K 1 NA 76GAU 01 1 10 fi 1B.B 1 Q 1 .y LPXKr 84BIS 01

Ifi o lo.y ft fi u.o C A A rAA 83GR0 02

Pt (pq/q) 1 fi oc 10. ya 1 .03 DA A PAA 76KAT 04

i

1 ioly f TUA 1 1 NA 80CRE 01 < 3000 DTUA K 1 NA 84TJI 01 1 ioly 1

1 DTUA K 1 NA 77MEL 01 70 33 DTUA K 1 NA 82ZEI 01 1 ioly 1 X 1.0 T TUA I 1 NA 78BEH 01 IOly 1 ^ 1 .o I TUA 1 1 NA 77JUR 02

Rb (uq/q) IOly f TUA 1 1 NA 77HAM 01

1 IO 1 ly. 1 nu.on LPXKr 85CLA 01 9.9 1.6 UPAKr 80MAE 01 1 IO 9 iy.£ 1 A 1 .H T TUA I 1 NA 80MAE 01 13.2 1

1

i 1 CCMC 85V0S 01 1 IO T ly. J

5 fl f*DVD LPXKrC 79MAN 01 15 2

1 /. U A A IhNAA 81UIL 02 1 IO c iy.3 o 1 £.1 f TUA I 1 NA 79ZEI 01 15 2.5 J** l*r AKT 78J0L 01 1 IO ft ly .o 11 .HA o f

1 TUA 1 NA 74BEC 01 15.1 4.4 XRF 77SMI 04 1 19.9 17 UU 74HAS 01

16.5 1.2 5 ITNA 80TOU 01 1 20 11 SSMS 85V0S 01 16.6 2.8 RTNA 74SCH 03 1 20 2.4 CPXRF 80KIR 01 16.7 CPXRF 84KAU 01 1 20 3 CPXRF 78VIS 01

1577-21
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Rb (uq/q) cont.

1

1 Sb (ng/g) cont

20.1 ITNA 73NAD

1 01 1 50 ITNA 79ICUC 01 20.9 2.5 6 CPXRF 77WIL 03 1 55 9 6 ITNA 74BEC 01 21.2 0.55 AA 85EVA 01 1 69 24 6 ITNA 74BEC 01 23.3 17 UU 74MAS 01 1 70 1 lENA 79KUC 01 23.4 17 uu 74MAS 01 1 130 170 RD ITNA 79 1 MA 03

28 CPXRF 76ZEI 01 1 130 170 R ITNA 79 1 MA 01 28 17 UU 74MAS 01 1 300 200 ICPES 830LI 01 29 4 CPAA 78MCG 01 1

1 Sc (ng/g)

S (ug/g) 1

1 < 0.5 L RTNA 75LIE 01 3300 1000 CPXRF 79REN 02 1 < 0.5 L RTNA 77LIE 01 6300 2100 m 83L1 01 1 < 1 L RTNA 80SLO 01 7200 200 TCGS 79FAI 01 1 < 1 RTNA 75STE 02

7200 400 TCGS 77JUR 01 j < 1 L NAA 78GAN 01 7353 81 ICPES 84PRI 01 1 < 4 L ITNA 78CAP 01 7410 110 ICPES 84M0R 01 1 < 800 L 14NAA 81WIL 02

7440 CPXRF 84KAU 01 1 0.4 17 UU 74MAS 01 8150 80 CB 86B0U 01 1 0.6 0.1 RTNA 74HEN 01 8550 150 WXRF 86B0U 01 1 1 ITNA 73NAD 01 8800 273 WXRF 84ALK 01 1 1 0.9 RTNA 76GAU 01 9300 100 ICPES 85WHI 02 1 1.1 ITNA 84GLA 11 9500 700 CPXRF 80KIR 01 1 1.1 0.1 RTNA 79WAR 02

16200 2000 ITNA 79CHA 02 1 1.1 0.3 ITNA 78BEH 01

1 1.2 0.2 ITNA 80MIC 01 Sb (ng/q) 1 20 6 RTNA 77MEL 01

4 RTNA 79MAY

1 01 j Se (ug/g)

4 RTNA 75LIE 01 1 4 1 RTNA 80SLO 01 1 0.228 0.011 FLUOR 74IHN 02

4.8 0.5 RTNA 77LIE 01 1 0.4 0.27 FAA 81MEY 01 4.8 1.2 RTNA 79R0S 02 1 0.69 0.06 NAA 78GAN 01

5 HAA 79EVA 01 1 0.75 FAA 74IHN 01

5 2 RTNA 79H0E 01 1 0.76 7 ICPES 84MIA 01 5.7 0.5 ITNA 86GRE 01 1 0.774 HAA 771 HN 01 7 5 ITNA 78BEH 01 1 0.8 CPXRF 84KAU 01 9 3 RTNA 74HEN 01 1 0.9 11 FAA 82VER 03

10 2 RTNA 78GAL 01 1 0.91 FLUOR 78EGA 01

10 3 ITNA 80MIC 01 1 0.92 0.04 HAA 82SUB 01

11 9 RTNA 74SCH 03 1 0.92 0.18 6 ITNA 74BEC 01

12 ITNA 80CRE 01 1 0.95 0.03 HAA 78EGA 01

12 2 7 RTNA 80GAL 02 1 0.97 0.03 ICPES 80HAA 01

14 5 NAA 78GAN 01 j 0.972 FLUOR 79TAM 01

14 10 ITNA 77ZIK 01 1 0.98 0.01 HAA 76FI0 01

15 4 RTNA 77TJI 01 1 0.98 0.03 DCPES 81 CAR 02

16 2 ITNA 79CHA 02 1 0.98 0.03 GCMES 74TAL 02

16 7 ITNA 73C0R 01 1 0.98 0.05 ITNA 76DIK 01

18 17 UU 74MAS 01 1 0.98 0.06 AA 79PAV 02

22.9 17 UU 74MAS 01 1 0.98 0.15 34 CPXRF 78J0L 01

26 1 RTNA 79WAR 02 1 1.00 HAA 78WEL 01

34 ITNA 73NAD 01 1 1.00 11 FAA 82VER 03

1577-22
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Se (ug/g) cont.

Cone Uncer Com Method Reference

Se (ug/g) cont.

1.00 17 UU 74MAS 01 1 1 .07 0.11 ITNA 78HIR 01

1.00 0.01 ITNA 79SAT 01 1 1 .07 0.18 RTNA 79PLA 01

1.00 0.02 FAA 761 HN 02 1 1 .07 0.19 RTNA 79R0S 02

1.0C 0.04 FAA 761 HN 01 1 1 .08 0.01 CSV 83ADE 01

1.00 0.1 RTNA 75ABU 01 1 1 .08 0.01 ITNA 74LIN 01

1.00 0.1 11 AA 85BYE 01 1 1 .08 0.015 FAA 80MEV 01

1.00 0.1 11 HAA 82J0N 01 1 1 .08 0.05 ASV 76AND 01 1.00 0.1 ICPES 830LI 01 1 1 .08 0.08 AA 84MAT 01 1.00 0.2 CPXRF 80MAE 01 1 1 .08 0.12 ITNA 77GUI 02

1.00 0.4 CPXRF 78VIS 01 1 1 .08 0.13 6 ITNA 74BEC 01

1.01 0.04 ITNA 79CHA 04 1 1 .08 0.2 FAA 79RAI 01

1.01 0.06 ITNA 84ALK 01 1 1 .09 0.01 ASV 83ADE 01

1.02 11 HAA 85PIW 01 1 1 .09 0.02 AA 79FLA 02

1.02 ITNA 81 HAN 01 1 1 .09 0.02 34 HAA 78FLA 01 1.02 7 ICPES 84HIA 01 { 1 .09 0.04 ITNA 86GRE 01 1.02 17 UU 74MAS 01 1 1 .09 0.05 RTNA 740RV 01 1.02 ITNA 81MEY 01 1 1 .09 0.06 HAA 81 HAN 01 1.02 0.03 RTNA 77LIE 01 1 1 .09 0.08 RTNA 79WAR 02

1.02 0.03 RTNA 75LIE 01 1 1 1 FAA 77YAS 01 1.02 0.03 9 ITNA 81SUZ 01 j 1 ITNA 80CRE 01 1.02 0.04 HAA 80AGE 02 1 1 ITNA 770SB 01 1.02 0.06 lENA 86CHI 01 1 1 ITNA 78CAP 01 1.02 0.438 5 RTNA 82TIN 01 1 1 11 FAA 82VER 03

1.03 6 FAA 77SHU 01 1 1 0.02 XRF 81KNA 01 1.03 0.03 RTNA 77RA! 01 1 1 0.05 11 GC 81UCH 02

1.03 0.03 ITNA 79RAI 01 1 1 0.06 11 GC 81UCH 02

1.03 0.04 11 HAA 82J0N 01 1 1 0.06 FLUOR 30KOH 01 1.03 0.05 ITNA 80MIC 01 1 1 0.1 GC 77P00 01 1.03 0.09 ITNA 81M0L 01 1 1 0.1 9 ITNA 80UAN 01 1.04 FLUOR 74IHN 01 1 1 1 0.13 11 RTNA 82P0L 01 1.04 0.03 ITNA 86CHI 01 1 1 0.17 9 ITNA 77V0B 01 1.04 0.07 ITNA 74WES 01 1 1 0.17 9 ITNA 79PAV 02

1.04 0.1 RTNA 80KNA 01 1 1 0.17 9 ITNA 77V03 01 1.045 0,04 ITNA 77EGA 01 1 1 0.2 EXRF 79GIA 01 1.05 6 FAA 77SHU 01 1 1 0.2 HAA 82MAY 01 1.05 7 ICPES 84MIA 01 1 1 0.3 ITNA 79ZEI 01 1.05 0.05 HAA 80V IJ 01 1 1 0.4 5 ITNA 80TOU 01 1.05 0.12 RTNA 80SLO 01 1 1 107 0.15 NAA 76GUZ 01 1.05 0.19 ITNA 79LAK 01 1 1 "I "I 0.02 SSMS 77PAU 01 1.053 0.051 COLOR 79SZY 02 1 1 11 0.03 FAA 82JUL 01 1.06 FAA 78CAP 01 1 1 11 0.04 SSMS 77R00 02

1.06 0.06 RTNA 78GAL 01 1 1 ^1 0.05 RTNA 74BYR 03

1.06 0.06 7 RTNA 80GAL 02 1 1 0.06 HAA 761 HN 02

1.06 0.1 RTNA 77TJI 01 1 1 0.08 13 ITNA 73BL0 02

1.06 0.11 11 RTNA 82P0L 01 1 1 0.09 12 FAA 84RIN 01 1.069 0.016 ITNA 82DAM 01 ] 1 0.1 ITNA 79CHA 02

1.07 RTNA 75STE 02 1 1 12 0.02 FLUOR 84ALF 01 1.07 0.02 AA 83RAP 01 1 1 12 0.03 ASV 75AND 01 1.07 0.04 GC-MS 81REA 02 1 1 12 0.075 HAA 81MEY 01 1.07 0.06 5 ITNA 81SUZ 01 1 1 12 0.08 11 RTNA 82P0L 01 1.07 0.1 RTNA 79MAY 01 1 1 12 0.08 RTNA 72R00 03

1577-23
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Com Method Reference

Se (ug/g) cont.

1 1? PTMA Uc.

1 1? n no 7 PTMA K 1 fin O IKUI# ni

1 1? nU.I1 noV O 1 rU9 niU 1

1 1? (119 o Fl imp 1 JUL9 ni

1 17 171 1

1 U 1 7AIIAC U 1

1 1'^

1 . \J n n7 1

1

A^V RAADF OHnUC ni

1 17 ft m AA ftCAnC OjnUC n?

1 17 nU . UJ OCUA^ O^nnK ni

1 17 n no T TMA ni

1 177 n 1?? 1 1 nn nouns n?uc

1 ^L 0 04 TTMA 1 1 nn 01U 1

1 1^ 0 OS TTMA AflMAF ounnii 01U 1

1 1^ Q 09 HAA nnn 01U 1

1 1i U a UT 1 HAA nnn 0£ 1 nn niU B

1 1i U a 1 1 TTMA 1 1 nn 77 II ID n?u£

1 1A U a e 1 TTMA A 1 nn 70PA\/ I Trn V n?

1 1i nil U a t 1 TTMA 1 1 nn ni

1 1A n 1

1

U a 1 1 T

1 TMA 1 Nn ni

1 1^ n%f a n?Ub Fl 1 inp ni

1 1 ^ U a T

i TMA 1 Nn AAl ni

0W a OAUO 1

1

1 1 n3V A^V A^ADF niU 1

1 1& rev A1UAM o 1 nnn niU 1

11 • 16I! U 0V . 08UU FAA rnn AARAII niU 1

1 .16 0.09 12 FAA rnn 1 n 01 1.17 0.06 6 75QI S 01 1.17 0 18 HAA 82JUL 01

1 .18 1

1

HAA 85PIU 01

1 .18 0.14 RIKA 74HEN 01

1 .19 0.11 13 ITNA T^BLO 02

1 2 1

1 IFNA f 7^U^ 01

1 2 79ifiir f T^Ul. 01

1lab2 FAA 77YAS f f 1 no 01

1lab2 finHAA uunnn 01

1lab2 7 i\ 1 Pin Rlifiir W 1 KUW 01U 1

1 2 0Hal1 I 1 nn ouHnn niU 1

1lab2 0 1 R 1 nn 77MFI niU 1

1lab2 fl 1 7 n 1 nn An^AI OUunL n?

1labP n 1 1 1 nn AI^PI niU 1

1lab2 0 1 MAA nnn 77RI

1

niU 1

1 2 0U.I1 PTMA i\ 1 nn 77RII n7UJ>

1 2 0U.I1 rpvDC 77UI

1

02uc

1 .Z 0.11 RTNA 770MI n 4 01 1.2 0.155 ITNA 77HAM 01 1.2 0.16 HAA 81REA 01 1.2 0.2 11 AA 85BYE 01 1.2 0.2 HAA 81 COX 01 1.204 0.124 HAA 771 HN 03

1.22 0.04 COLOR 81 TOE 01 1.23 17 UU 74MAS 01 1.24 0.04 GC 81 TOE 01 1.24 0.3 CPXRF 85CLA 01

Cone Uncer Com Method Reference

Se (ug/g) cont.

1.26

1.26 0.15

1.28 0.24

1.3 0.4

1.4

1.4 0.1

• 1.4 0.5

1.7

1.7 0.1

2.7

7.65 0.277

13.376 0.926

Se(VI) (ug/g)

0.3 0.07

0.31 0.11

16.7 0.67

16.79 1.84

19

246

Sm (ng/g)

1 0.2

1.3 0.4

1.5 0.2

1.6

1.6

1.9 0.2

2 0.2

2.8

35

Sn (ng/g)

<

<

<

<

10

20

20

21 220

24

240

600

600

1500

3

6

3

180

17

5

11

UU 74MAS 01 FLUOR 81SUZ 01 CSV 83AHH 02

RTNA 74SCH 03 FAA 82INU 01 EXRF 80DYC 01 CPXRF 77WIL 03 ITNA 73NAD 01 ITNA 78FUR 01 ICPES 85NAR 02

RTNA 82TIN 01 RTNA 82TIN 01

GC 81 TOE 01 COLOR 81 TOE 01

ITNA 75PIE 01 NAA 76GUZ 01 SSMS 85VOS 01 CPXRF 84KAU 01

RTNA 74HEN 01 RTNA 80SLO 01 RTNA 83TJI 01 RTNA 82LAU 01 RTNA 77LAU 02

RTNA 76GAU 01 RTNA 86TSU 01 ITNA 80CRE 01 RTNA 74SCH 03

RTNA 81KUC 01 RTNA 75LIE 01 RTNA 77LIE 01 ICPES 78CAP 01 HAA 79EVA 01 RTNA 83GRE 02 ITNA 86GRE 01 RTNA 77BYR 01 ICPES 80HAA 01

1577-24
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone

Sr (ng/g)

Uncer Com Method Reference

100 11 SSMS 85V0S 01

150 20 RTNA 76GAU 01 160 ICPES 780AH 01 160 20 FAA 82SUZ 03

300 60 ICPES 79ABE 01 500 180 34 CPXRF 78J0L 01 550 440 AA 85EVA 01 2000 800 14NAA 81WIL 02

Ta (ng/3?

Tb (ng/g?

Te (ng/g)

90

Th (ng/g?

Ti (ug/g)

ITNA

15 RTNA

80CRE 01

< 0.2 RTNA 83TJI 01

< 1.6 L RTNA 76GAU 01 0.17 RTNA 82LAU 01 0.18 RTNA 77LAU 02

2 ITNA 80CRE 01

77DIK 01

< 1000 L EXRF 79GIA 01 3 6 R* RTNA 80SLO 01 6.8 ITNA 80CRE 01

< 0.15 L ICPES 78CAP 01

< 3.3 CPXRF 84KAU 01

< 4 L 14NAA 81WIL 02

< 11 L EXRF 79GIA 01 0.7 0.2 COLOR 82KIR 02

1.7 0.2 ICPES 79ABE 01 2 1 CPAA 77ZIK 01 3.2 1 14NAA 81UIL 01 3.8 11 SSMS 85VOS 01 4.7 11 SSMS 85VOS 01

(ng/g)

< 2 11 ASV 84LIE 01

< 2 11 ASV 84LIE 01 2 11 ASV 84LIE 01 48 3 SSMS 77PAU 01

Cone

Tm (ng/g)

0.1

0.15

U (ng/g?

Uncer Com Method Reference

0.99

1 20

V (ng/g)

1533

55

56

56

58.6

59

60

60

60

61.5

61.5

65

66.2

90

320

370

400

460

500

600

W (ng/g)

3.8

5

5

12

1530

700

0.3 RTNA

RTNA

RTNA

76GAU 01 82LAU 01 77LAU 02

< 1 DNA 86GAU 01 < 20 L ITNA 74WEA 01 < 100 L RTNA 76GAU 01 < 2000 L EXRF 79GIA 01 0.25 35 DNA 80GLA 04

1 .6 DNA 84GLA 02

48 R DNA 81GLA 03

< 20 L RTNA 77BU0 01 < 20 L ITNA 74H0F 01 < 40 L ITNA 74H0F 01

5 COLOR 82KIR 01 3 RTNA 79WAR 02

1 FAA 77MYR 01 17 UU 74MAS 01 7 UU 73STE 01 1.6 RTNA 78BYR 01 NAA 80KOS 02

ICPES 80HAA 01

2 RTNA 80UOI 01

5 RTNA 79CHA 02

2 RTNA 79C0R 01 2 RTNA 81 COR 02

2 RTNA S2BYR 01 4.9 RTNA 78ALL 04

60 11 ICPES 82 J ON 01 80 RTNA 77GU1 03

11 SSMS 85V0S 01

11 SSMS 85V0S 01 ITNA 78CAP 01 100 ITNA 77ZIK 01 100 ICPES 79ABE 01

RTNA 84BYR 01 17 UU 74MAS 01 3 RTNA 74SCH 03

RTNA 76GAU 01 RTNA 75STE 02

17 UU 74MAS 01 100 RTNA 80SLO 01

1577-25

1
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Coni Method Reference | Cone Uncer Com Method Reference

f

Y (uq/g) Zn (ug/g) cont.

< 1 L EXRF 70RI

A

123.8 1.2 FAA ni

< 14 L 14NAA 81WIL 01 1 124

124

17

6

UU

POL

74MAS

7?^IM 1 CO 1 n

01

01 Yb (ng/g) 1 124

124 7 7

ITNA AA78CAP

73TAL

01

01

< 0,1 RTNA fi'^T J

I

01 1

1 124 7 FAA 7ATAI ni

0.28 RTNA KPl AM 01 1 124 7.3 11 RTNA 74WES 01

0.285 RTNA 771 All n? 1

1 124 10 D ICPES Rn<;rH 08

0.48 0.09 RTNA 7ARAII 01 1

1 124 10 ICPES 05

830 UUk 01w 1

1 124

124.4

14 CPXRF

RTNA

79MAN

7SHAI

01

ni

Zn (ug/g) 125

125

ITNA RTNA 75STE

ni

02

13.17 17.59 R AA 01 1

1 125 2 AA 79FLA 02

32 ASV 01\J 1 1 1 125 5 7 RTNA 80GAL 02

65 15 FAA 77IFII 1 01 1

1 125 5 RTNA 77GIL 03

78 25 14NAA 01 1 125 5 NAA 77GIL 01 93 17 12 FAA 0? 1

1 125 6 AA 83RAP 01 98 122 RD ITNA 79 1 MA O'? 1 \J-J 1 125 16 ITNA 77HAM 01 98 122 R ITNA 70 1 MA 01 1 125.7 10.6 34 CPXRF 78J0L 01

101 17 UU 7^MA^ 01 1 126 FAA 75SLA 01

102 FAA RXAT? OJn 1 O ni 1

1 126 2 ITNA RnMAF 01

104 CPXRF 7fl| ipu ni 1

1 126 4 7 AA T^TAI 01

106 31 12 FAA \JC 1 126 4 FAA 74TAI 01

112 XRF n? 1 126 4 SSMS 77PAU 01

112 15 ICPES A1RI A ni 1 126 5 ITNA 81M0L 01 112.6 1.1 FAA 81 CLE 02 1 126 8 FAA 79WAR 01

113 5 FAA 84R0S 01 1 126 9 RTNA 740RV 01

116 ITNA 01 1 126 71 ITNA 82ICIM 01

116 18 CPXRF RDMAF 01 1 127 11 FAA 81DAN 01 117 13 AA 70mAM 01\f 1

D 127 1 lENA 79KUC 01 117.2 10 RTNA 83DAN 01 1 127 1 RTNA 80SLO 01

118 11 ASV RlDfiW 01 1 127 4 AA 80UCH 01

118 4 6 POL 7?<;iij 1 CO m 01 1 127 8 11 RTNA 74WES 01

118 21 RTNA 871^ I

M

01U 1

1 P 127 9 ITNA 81KRI 01 118.2 7.8 lENA 7SMA7 r Jrln^ 1 127.9 9.1 6 ITNA 74BEC 01 119 6 POL 7?Q I M ni 1 128 DCPES 78NAK 01

120 17 UU ni 1

1 128 7 RTNA 81ICUC 01

120 6 11 ICPES ft1RI O 1 oL.nA n? 1 128 3 FAA 81CLE 01

120 12 FAA RAMAD n? 1 128 3.6 11 AA 74WES 01

121 10 7 RTNA RAFAP n? 1 128 5 ITNA 79SAT 01

121 13 ICPES OJ rno ni 1 128 6 AA 75HIN 01 121.9 RTNA 74RAV n 1 1 01 1 128 7 RTNA 70nCD U 1

122 11 FAA 81DAN 01 1 128 10 CPXRF 80KIR 01

122 3 NAA 78GAN 01 1 128 12 ITNA 79CHA 02

122 3 EXRF 80DYC 01 1 128 14 EXRF 77NIE 01

122 9 ITNA 79LAK 01 1 128 14 CPAA 77ZIK 01

123 5 ITNA 74UES 01 1 128 26 ICPES 82AZI 02

123 8 7 RTNA 84FAR 02 1 128.6 AA 79L0C 01

123 25 ITNA 78FUR 01 1 128.6 0.7 ITNA 82DAM 01

123 26 ICPES 84BLA 01 1 129 ICPES 80HAA 01 1577-26
TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Cone Uncer Cora Method Reference

Zn (ug/g) cont.

129 ICPES 84NAD 01 129 1 lENA 79KUC 01 129 ITNA 80CRE 01 129 1.5 ITNA 86CHI 01 129 3 ITNA 74D0N 01 129 4 RTNA 79WAR 02

129 4 ITNA 79WAR 01 129 8 ITNA 80LAK 01 129 16 32 CPXRF 77CR0 01 129.2 6 ITNA 84ALK 01 130 OES 75B0L 02

130 11 AA 81M0H 01 130 4 11 ICPES 81BLA 02

130 4.5 AA 84 HUD 01 130 4.5 D AA 84 HUD 03

130 5 1 ICPES 78SUD 01 130 7 CPXRF 78V IS 01 130 13 FAA 80LON 01 130 22 AA 82HAR 01

131 AF 85NAR 02

131 14 FAA 80CHA 08

131 17 UU 74MAS 01

131 1 AA 75ABU 01

131 1 AA 75EPS 01

131 1 ICPES 79MCQ 02

131 1.4 AA 80AGE 01

131 2 ICPES 79MCQ 01 131 4 ITNA 80MIC 01

131 13.5 PAA 76KAT 04

131 37 EXRF 84KNA 01 131.8 6.5 ITNA 73C0R 01 132 1 AF 75EPS 01 132 3 GC 81BLA 01 132 3.3 6 CPXRF 77WIL 03

132 5 AA 79MCQ 01 132 6 7 RTNA 81KUC 01 132 7 1 AA 77UCH 02

132 7 AA 801 ID 01 132 10

' CPXRF 81SAI 01 132 15 ICPES 83SCH 04

133 11 ASV 81DAN 01 133 CPXRF 84KAU 01 133 14 FAA 80CHA 08

133 4 7 RTNA 84FAR 02

133 6 ICPES 78JAC 01 133 7 ITNA 77JUR 02

133 7 ITNA 78BEH 01 133.9 6.8 ITNA 79ZEI 01 134 ICPES 85NAR 02

134 17 UU 74MAS 01 134 2 RTNA 77MEL 01 1577-27

Cone Uneer Com Method Reference

Zn (ug/g) cont.

134 2 EXRF 79GIA 01 134 3 AA 79WAR 01 134 4 1 AA 771ICH 02

134 5 7 AE+AF 73TAL 01 134 5 FAE 74TAL 01 134 5 RTNA 77TJI 01 134 6 11 ICPES 82J0N 01 134 7 11 ICPES 82J0N 01 134 7.2 RTNA 79PLA 01 134 10 7 AE+AF 73TAL 01 134 10 FAE 74TAL 01 135 17 UU 74MAS 01 135 AE+AF 79ULL 01 135 ICPES 78CAP 01 135 1 ITNA 74LIN 01 135 2 11 ICPES 82J0N 01

135 2 ICPES 85WOL 01

135 4 11 ICPES 82J0N 01 135 5 CPXRF 85CLA 01 135 5 RTNA 75LIE 01 135 5 RTNA 77LIE 01 135 6 lENA 86CHI 01 135 7 AA 84CUB 01 136 11 XRF 83PEL 01 136 17 UU 74MAS 01 136 1.8 6 DCPES 83FRA 01 136 3 HPLC 85SAI 01 136 6 RTNA 76GAU 01 136 9 RTNA 74HEN 01 137 2 ASV 85ADE 01 137 4 ITNA 74GUI 01 137 9 5 ITNA 80TOU 01 137.2 5.75 NAA 76GUZ 01 138 3 ITNA 86GRE 01 139 17 UU 74MAS 01 139 11 SSMS 85VOS 01 139 5 ICPES 82EVA 01 140 ITNA 770SB 01 140 11 AA 81M0H 01 140 ICPES 78DAH 01 140 2.4 6 DCPES 83FRA 01 140 16 RTNA 77KUS 01 140 29 XRF 77SMI 04

141 2 D DCPES 81REE 01

141 2 DCPES 79REE 01

141 16 5 RTNA 74SCH 03

141.7 5.3 6 ITNA 74BEC 01 142 AA 80EVA 01 142 4 AA 82EVA 01 142 11 ITNA 77ZIK 01 143 19 ICPES 79ABE 01
Cone

TABLE 1577-2: INDIVIDUAL DATA FOR NBS SRM 1577 (cont.)

Uncer Com Method Reference I

Zn (ug/g) cont.

144 12 6 CPXRF 77WIL 03

144 17 CPXRF 84SIS 01

145 FAA 78CAP 01

145 11 SSMS 85V0S 01

145 5 CPXRF 77WIL 02

145.5 HNA 82AKA 01 146 12 ICPES 82AZI 01 147 7.3 11 AA 74UES 01 148 15 CPAA 78!'1CG 01 148 74 CPXRF 76ZEI 01 150 10 PAA 76WIL 01 153 2 ICPES 85WHI 02

156 6.2 CPXRF 81 ROB 02

157 20 1 ICPES 78SUD 01 159 8 5 RTNA 74SCH 03

160 17 UU 74MAS 01 160 17 UU 74MAS 01 162 31 32 CPXRF 77CR0 01 200 40 14NAA 81UIL 02

Zr Cug/g)

< 0.5 L 14NAA 81UIL 02

< 3 L 14NAA 81WIL 01

< 3 L EXRF 79GIA 01 0.09 0.08 PAA 84SAT 01 1.6 11 SSMS 85V0S 01 3.4 0.4 PAA 79CHA 02

4 3 CPAA 77ZIK 01

1577-28

/
8 2

LU O

Z to

3: C

O «

in

«/) <A cn (/) </) to to </> X z z z ac LU to z t« (n

a. a. a. a. Q. a. O. x: a. z z

o o u u O u O o CD o o

o o

CO O I 1 O J- 1 o 1 00 CM • 1 1 1^

1 1 o

O o« 1 CM O

in oo

in o in

in m in • 00 (M

z z

O COo o

u. C

q: (0 X 0)

c

00

</>

"H03 AA H

c

>

C- z

Q£

LU>

c

LU o > (/) oCD

;*

AA H

c

(D in 41 Z

z

</> to

a>z

lU O 13

Ll_ Z

< <t—<

a

aUl

_i z Q. <aUJz

<

c

in

UJ to a _j to

00 CO < z

LU +) COz c o <D

0)

fM m 1 N- 1 t 1 1 in 1 1 1 1 in 1 1 1 1 t

1 1 1 1 1 1 >* ro 1 1 1 1 1 1 1 1 1

1 1 1 1 1 O 1 1 1 o 1 1 1 1 1 «—

>3- ro f\i <M ro (M

CM o <0 IM

in in in o CNJ

1 o o o to o lA * 1 > (M H 1 J- •M •H CO O H • OJ 1 I f\J to in 1 >t (\j ro in 1 1 o in t^ (\j in

<>

o

in «-

o

O ro

«t in

-*o

M oin

o

o o

>o »- (M 1^ CO in

in t- T- >a- csi (M

I o in to o o >* ^ • • >!

CO «- -J- in (\J

-4-

in CO 1^ o to o o CO o >o

to to (NJ

1

(\J

1

*—

1 to o1 * 1 1 1 o1 o -J- O m -o" 00 m to

OJ o

o

00

in

to O 1 1 • t • Ch CO > 1 o O o <\J in t to in 1 (M • 1 t in in o nO ' I in in

«—

I o nO Ov 1 e vj- o (V

t^

«- «- rj

«- 00 in

ro • CO o <3

in

CO

oo

oCO

in

o

^ -o t^ V

in

(M

rvj (M

r»- o 00 ro

to >* -o CM fM o in CM CM to ro CM to m CM 1^

to

(M O

>^ to CM

Nto

to

-*

v^oCM o

o in

> ' o

w CM

CO in m o ro o to CM 00 CM CM in in t^ CM vl- >!• in o o ro 1 in N- 00 1 1 o

to

+) •H H in

>«• •H CM H -H to CM

+) +< •H • ro

•H M CM 4H •

1

1 •

1 CM

to o

•M 1

1

1

1 • o +1 CO o O in o CM O o CM O o o CM

-*

Ch <M ONin o «

otoCM 00

COm -Hc

o

o

-O t^ O

o Oin t^ oCM CM O

o

m«—

OOOino h- oto O

o

in o

o

«

1 1 ofs. ro o

o CO 00

•H CM •H *i i •H M M M •H •H +4 +1 o +1 H H H

1 1 M 1 1 1 1 to H +1 to +1 +1 +1 O>* oCM o

•J- o

00

CM

o

CM

CO

in

^

-J- o>

-O O O;

<>

inro

«— o

ro

si- CM

inroin

CM

1 1 Oo

1 1 O«

CO

to

«

sio

o mCM

O) O) O) o CD cn O) \ \ \ s^ — \ 4-* M \ \ \ cn cn cn O) cn (7) CD <D cn cn O) c 3 c 3 3 c 3 c 3 3 3 c c 3 3 3 *< 3 frS c 3 3 3 3 t_ 1. c c c c c c c 3

D) —• </) < «: <

(0 "0 —

•

o u u

o t. 3 <U O) c z z a.

to to

<M to

to to ^ U <U I- C/>C/)(/)tO(/>CO(/>tO h- 3 >

c

rsi

1577A-1
TABLE 1577A-2: INDIVIDUAL DATA FOR NBS SRM 1577A (revised 3/1/86)

Cone

AL (ug/q)

3.4

As (ng/q)

Uncer Com Method Reference

Br (ug/q)

0.8 ITNA 84GLA 1

1

40 10 HAA 85SAL 01 49 4 RTNA 85GAU 04

56 3 RTNA 84BYR 02

8.5 1 lENA 84GLA 11 9 0.9 ITNA 84GLA 11 9.7 ITNA 85GAU 04

11.2 lENA 85GAU 04

Ca (uq/q)

25 1.1 1 1 AA 84IMA 02

26.1 1.4 1 1 AA 84IMA 02

111.3 1 AA 84IMA 02

112.9 1 AA 84IMA 02

113.2 2.6 1 1 AA 84IMA 02

113.5 1 AA 84IMA 02

115.7 3.5 1 1 AA 84IMA 02

116.2 1 AA 84IMA 02

117.3 10.3 1 1 AA 84IMA 02

117.6 1 AA 84IHA 02

117.7 27.9 1 1 AA 84IMA 02

118.6 1 AA 84IMA 02

120.7 1 AA 84IMA 02

121.3 1 AA 84IMA 02

122.2 3.3 1 1 AA 84IMA 02

123 1 AA 84IMA 02

124.1 8.4 1 1 AA 84IMA 02

124.1 9.1 1 1 AA 84IMA 02

124.1 9.2 1 1 AA 84 1 MA 02

124.7 1 AA 84IMA 02

124.9 1 AA 84IMA 02

125 0.2 1 1 AA 84IMA 02

126.5 9.1 1 1 AA 84 IMA 02

126.5 9.1 1 1 AA 84IMA 02

127 9 CPXRF 85SIM 01 127.6 12 1 1 AA 84IMA 02

129.3 1.4 1 1 AA 84IMA 02

129.7 13.2 1 1 AA 84IMA 02

145 3 I CRMS 86SCI 01 160 60 ITNA 84GLA 11

Cone

Cd (nq/q)

440

470

CI (uq/q)

2570

2650

2780

2800

Co (nq/q)

244

254

Cr (uq/q)

Cu (ug/g)

62.3

73.7

100.5

108.9

114.2

126

129.2

129.4

131 136.1

136.6

137.2

141 142.9

149.1

149.9

151.4

153.6

153.6

154.8

156

157.6

159

159

159.1

159.1

160

160.4

160.7

Uncer Com Method Ref erenc^

10 RTNA 84BYR 02

10 FAA 85SAL 01

ITNA 85GAU 04

soo lENA 84GLA 11 50 ITNA 84GLA 11 00 ITNA 86KRA 01

12 ITNA 86KRA 01

21 RTNA 84BYR 02

0.3 ITNA 86KRA 01

11

11

AA

AA

84IMA

84 1 MA <02

2.4 11 AA 84 1 MA 02

11 AA 84IMA 02

11 AA 84IMA 02

0.5 11 AA 84 1 MA 02

2.7 11 AA 84 1 MA 02

7.2 11 AA 84 1 MA 02

11 XRF 83PEL 01 4.1 11 AA 84 1 MA 02

2.2 11 AA 84IMA 02

11 AA 84IMA 02

5 RTNA 84BYR 02

11 AA 84IMA 02

4.9 11 AA 84 1 MA 02

4.2 11 AA 84IMA 02

12.7 11 AA 84IMA 02

11 AA 84 1 MA 02

8.3 11 AA 84 1 MA 02

11 AA 84 1 MA 02

4 AA 85SAL 01 1.2 11 AA 84 1 MA 02

11 XRF 83PEL 01 6 ITNA 84GLA 11

11 AA 84IMA 02

5.5 11 AA 84 1 MA 02

0.6 I CRMS 86SCI oi^

11 AA 84IMA 02 . 9.3 11 AA 84IMA 02

1577A-2
TABLE 1577A-2: INDIVIDUAL DATA FOR NBS SRM 1577A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

J (ug/g) cont.

1 K C%)

162.7 6.5 11 AA 84IMA 02 1 0.894 0.03 ICPMS 86SCI 01 162.7 6.5 11 AA 84IMA 02 1 0.95 0.02 ITNA 84GLA 11

163.1 3.2 11 AA 84IMA 02 1 1.15 0.17 ITNA 86KRA 01 163.6 11 AA 84IMA 02 1 164 10 ITNA 86ICRA 01 1 Mg (ug/g)

i <ug/g)

1

1 571 57 ITNA 86ICRA 01

1 624 2 ICPMS 86SCI 01 67.2 9.2 11 AA 84IMA 02 1 640 30 ITNA 84GLA 1

82.1 3.8 AA 84IMA 02 1 95.8 AA 84IMA 02 1 Mn (uq/g)

105.9 AA 84IMA 02 1 116.1 AA 84IMA 02 1 8.4 11 AA 84IMA 02

119.8 1.6 AA 84IMA 02 1 9.1 11 AA 84IMA 02

135.1 AA 84IMA 02 1 9.1 0.08 ICPMS 86SCI 01 136.9 8.6 11 AA 84IMA 02 1 9.1 0.4 RTNA 84BYR 02

140 11 AA 84IMA 02 1 9.1 0.8 11 AA 84IMA 02

147 1^ AA 84IMA 02 1 9.4 11 AA 84IMA 02

147.8 7.4 AA 84IMA 02 1 9.5 11 AA 84IMA 02

148.3 3.5 AA 84IMA 02 1 9.5 0.6 11 AA 84IMA 02

149 XRF 83PEL 01 1 9.5 0.6 11 AA 84IMA 02

149.7 10.8 AA 84 IMA 02 1 9.58 0.38 6 FAA 85D0U 01 155.8 AA 84IMA 02 1 9.7 11 AA 84IMA 02

155.9 5.4 11 AA 84IMA 02 1 9.7 0.2 11 AA 84IMA 02

156.2 5.7 11 AA 84IMA 02 1 9.7 0.3 11 AA 84IMA 02

156.7 5.4 11 AA 84IMA 02 1 9.8 11 AA 84IMA 02

160.2 9.4 11 AA 84IMA 02 1 9.8 11 AA 84IMA 02

162.6 11 AA 84IMA 02 1 9.8 11 AA 84IMA 02

164.1 6.7 11 AA 84 IMA 02 1 9.8 11 AA 84IMA 02

168.2 11 AA 84IMA 02 1 9.8 0.4 ITNA 86KRA 01 168.3 4.4 11 AA 84IMA 02 1 9.8 0.4 11 AA 84IMA 02

170.9 11 AA 84IMA 02 1 9.9 0.3 11 AA S4IMA 02

170.9 9.8 11 AA 84IMA 02 1 9.9 0.3 11 AA 84IMA 02

170.9 9.8 11 AA 84IMA 02 1 9.9 0.4 11 AA 84IMA 02

172.4 11 AA 84IMA 02 1 10.1 0.1 11 AA 84IMA 02

178 11 XRF 83PEL 01 1 10.1 0.3 11 AA 84IMA 02

181 28 ITNA 86KRA 01 1 10.1 0.7 11 AA 84IMA 02

202 2 I CRMS 86SCI 01 1 10.2 0.1 11 AA 84IMA 02

204.1 49 11 AA 84IMA 02 1 10.2 0.7 6 FAA 85D0U 01

1 10.3 11 AA 84IMA 02

(ng/g) 10.3 0.5 ITNA 84GLA 11 10.3 1 6 FAA 85D0U 01 < 10 CVAA 85SAL 01 1 10.4 0.6 11 AA 84IMA 02

3 0.2 RTNA 84DEL 01 1 10.5 11 XRF 83PEL 01 3.3 0.5 RTNA 84BYR 02 1 10.5 11 AA 84IMA 02

10.7 0.2 11 AA 84IMA 02

(nq/q) 10.8 0.4 11 AA 84IMA 02

< 400 ITNA 84GLA 11 1 240 30 lENA 84GLA 11 1 246 11 RTNA 84BYR 02 1 1577A-3
TABLE 1577A-2: INDIVIDUAL DATA FOR NBS SRM 1577A (cont.)

Cone

Mo (uq/q)

3.4

3.47

Wa (ug/g)

Uncer Com Method Reference

1.18

Pb (ng/g)

Rb (ug/g)

12.2

s (ug/g?

1.2

0.01

ITNA RTNA86KRA 01 84BYR 02

2170 70 ICPHS 86SCI 01 1 2450 30 ITNA 86KRA 01 1 U Cnq/q)

2600 200 ITNA 84GLA 11 1

0.005 I CRMS

0.7 ITNA

86SCI 01

150 6 DCPES 84SNE 01 150 10 FAA 85SAL 01 160 6 DCPES 84SNE 01 210 6 DCPES 84SNE 01

86KRA 01

7845 46 IDHS 84KEL 01

7900 200 ICPMS 86SCI 01 8550 70 CB 86B0W 01 8860 170 WXRF 86B0U 01

S-32/34 (ratio)

22.555 IDMS 84KEL 01

S-33/34 (ratio)

0.1776 IDMS 84KEL 01

Sb <ng/g>

31 1 RTNA 84BYR 02

Sc (nq/g)

0.8 ITNA 84GLA 11

Cone

Se (ng/q)

580

650

779

790

1100

Uneer Com Method Reference

0.704

96

98.7

Zn (uq/q)

109.6

109.6

111.6

115.4

116.4

117

117.9

118

119

120

120.9

122

122.8

122.8

122.8

122.9

123.9

124.1

124.5

125.3

125.5

126

126.1

126.4

126.8

126.9

127

127.5

130.1

90

40

34

180

100

10.012

4

1.6

8.1

4.4

3.3

5.2

2

6

6

10.9

1.3

1.7

2.3

2.2

3,5

2.6

1.5

9.7

3

2.1

RTNA 84BYR 02

HAA 85SAL 01 CPXRF 84BUS 01 ITNA 86KRA 01 HAA 85CUT 01

DNA 86GAU 01 IDMS 83KEL 01

RTNA 84BYR 02

IDMS 85 FAS 02

AA 84 1 MA 02

AA 84IMA 02

AA

AA 84IMA 02

AA o4IMA 02

AA 84IMA 02

AA 84 1 MA 02

AA 84IMA 02

AA 84IMA A*> 02

AA 84IMA 02

AA 84IMA A*) 02

AA 85SAL A 4 01 AA 84IMA AO02

AA 84IMA AO02

AA 84IMA 02

AA 84IMA 02

AA 84IMA 02

AA 84IMA 02

AA 84IMA 02

AA 84IMA 02

AA 84IMA 02 XRF 83PEL 01 AA 84IMA 02

AA 84IMA 02

AA 84IMA 02

AA 84IMA 02 ITNA 86KRA 01 AA 84IMA 02

AA 84IMA 02

1577A-4
TABLE 1580-1: COMPILED DATA FOR NBS SRM 1580 ORGANICS IN SHALE OIL (revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean ± SD

Benzo [a] pyrene 50328 ug/g 21 ± 6

Benzo [e] pyrene 192972 ug/g 18 ± 8

Benzo[f]quinol ine 85029 ug/g 16 ± 4

m-Cresol 108394 ug/g 330

o-Cresol 95487 ug/g 385 ± 50

p-Cresol 106445 ug/g 270

2,4-Dimethylphenol 105679 ug/g 380

2 , 5 - D i methyI pheno

95874 ug/g 320

2,6-Dimethylphenol 576261 ug/g 175 ± 30

Fluoranthene 206440 ug/g 54 ± 10

Perylene 198550 ug/g 3.4 ± 2.2

Phenanthridine 229878 ug/g 45

Phenol 108952 ug/g 407 ± 50

Pyrene 129000 ug/g 104 ± 18

2,5,6-Trimethylphenol 2416946 ug/g 360

2,4,6-Triinethylphenol 527606 ug/g 120

TABLE 1581-1: COMPILED DATA FOR NBS SRM 1581 POLYCHLORINATED BIPHENYLS IN OILS

(revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean ± SD

Aroclor 1242 in Motor Oil

Aroclor 1260 in Motor Oil

Aroclor 1242 in Transformer Oil

Aroclor 1260 in Transformer Oil

53469219 ug/g 100 ± 1 11096825 ug/g 100 ± 2 53469219 ug/g 100 ± 1 11096825 ug/g 100 ± 3

TABLE 1583-1: COMPILED DATA FOR NBS SRM 1583 CHLORINATED PESTICIDES IN 2.2,4-TRIMETHYLPENTANE

(revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean t SD

gaiima-BHC 58899 ug/g 1.11 ± 0.01

delta-BHC 319868 ug/g 0.76 ± 0.01

Aldrin 309002 ug/g 0.86 ± 0.01

p.p'-DDE 72559 ug/g 1.23 ± 0.03

p,p'-DDT 50293 ug/g 1.90 ± 0.10

Heptachlor Epoxide 1024573 ug/g 1.0

1580-1
TABLE 1582-1: COMPILED DATA FOR NBS SRM 1582 PETROLEUM CRUDE OIL (revised 3/1/86)

COMPOUND CAS # UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean (n) Metho<

Benz [a] anthracene 56553 uq/q 3.0 ± 0.3

Benzo [gh i ] pery I ene 191242 uq/q 1.7 (1) 1.7 (1) GC-MS

192242 uq/q 1.7

Benzo [a] pyrene 50328 ug/g 1.1 ± 0.3 1,08 ± 0.12 (3) 1.1 0.95 - 1.2 1.2 (1) HPLC

50328 ug/g 1.02 (2) GC-MS

Benzo [e] pyrene 192972 ug/g 3.5

Carbazole 86748 ug/g 3.4

o-Cresol 95487 ng/g 500 ... ...

u 1 DcnzoLn 1 upnene ug/g JJ z c Fluoranthene 206440 ug/g 2.5 ± 0.3

I ndeno [ 1, 2 , 3 - cd] pyrene 193395 ng/g 170 170 (1) --- 170 (1) GC-MS

Perylene 198550 ug/g 31 ± 3 30.9 ± 1,4 (3) 30.2 30 - 32.6 30.1 (2) GC-MS

198550 ug/g 32.6 (1) HPLC

Phenanthrene 85018 ug/g 101 ± 5 Phenol 108952 ng/g 300

Pyrene 129000 ug/g 7

1

TABLE 1582-2: INDIVIDUAL DATA FOR NBS SRM 1582

Cone

(revised 3/1/86)

Uncer Com Method Reference

Benzo [ghi] perylene (ug/g)

1.7 0.1

Benzo [a] pyrene (ug/g)

GC-MS 84HIL 01

0.95 0.05 GC-MS 84HIL 01

1.1 0.23 GC-MS 84HIL 01

1.2 0.1 HPLC 84HIL 01

Indenoll .2.3- cd] pyrene (ng/g)

170 40 GC-MS

Perylene (ug/g)

84HIL 01

30 1.1 GC-MS 84HIL 01 30.2 1.7 GC-MS 84HIL 01 32.6 1.2 HPLC 84HIL 01 (

1582-1
TABLE 158A-1: COMPILED DATA FOR NBS SRM 1584 PRIORITY POLLUTANT PHENOLS IN METHANOL

(revised 3/1/86)

COMPOUND CAS # UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

f V 111 \rl COW^ 59507 ug/mL 27.4 ± 0.4

C7 - PK 1 nmr^^nfx 1 i«lllUI U^ICIIVi 95578 ug/mL 64.4 ± 1 .4 A— PnacAl 1 08594 1 in /ml CP

l/l^llivll (jpVICI l\J I 120832 ug/mL 35.6 ± 1 .3 ? T -Hu i n^^K\/l n}i Ann 1

1 iiic Lii y i piici lu

526750 < 1 GC

9 A - n 1 im^K\/ 1 r^onn 1 CfH u 1 hr; Lii y L

f.fli«?i lu

105679 tin /ml 51 6 ± 0 2 48 6 f 1 i GC

9 A» n Y n^^Kul Ann

£ f o u 1 niciny i pncno i J r uCO

1 in /ml < 1 RP

3,4-Diniethylphenol 95658 ug/mL < 1 GC

4,6-Dim"tro-o-cresol 534521 ug/mL 20.1 ± 0.9

2,4-Dinitrophenol 51285 ug/mL 22 .4 m-Ethylphenol 620177 ug/mL < 1 GC

o-Ethylphenol 90006 ug/mL < 1 GC

p-Ethylphenol 1230709 ug/mL < 1 GC

2-Methylphenol 95487 ug/mL < 1 GC

2-Nitrophenol 88755 ug/mL 25.2 ± 0.7

4-Nitrophenol 100027 ug/mL 20.7 ± 0.7

Pent ach I oropheno

87865 ug/mL 15.4 ± 1.1 Phenol 108952 ug/mL 29,7 ± 0.9 27.2 (1) GC

2,4,6-Trichlorphenol 88062 ug/mL 20.4 ± 1.9

TABLE 1584-2: INDIVIDUAL DATA FOR NBS SRM 1584 (revised 3/1/86)

Cone Uncer Com Method Reference

o-Cresol (ug/mL)

< 1

2.3-Diniethylphenol (ug/mL)

< 1

2.4-Dimethylphenol (ug/mL)

48.6

2.6-Diniethylphenol (ug/mL)

< 1

3.4-Dimethylphenol (ug/mL)

< 1

GC 85GAU 04

GC 85GAU 04

GC 85GAU 04

GC 85GAU 04

GC 85GAU 04

Cone Uneer Com Method Reference

m-Ethylphenol (ug/mL)

< 1

o-Ethylphenol (ug/mL)

< 1

p-Ethylphenol (ug/mL)

< 1

2-Methylphenol (ug/mL)

< 1

Phenol (uq/mL)

27.2

GC 85GAU 04

GC 85GAU 04

GC 85GAU 04

GC 85GAU 04

GC 85GAU 04

1584-1
TABLE 1585-1: COMPILED DATA FOR NBS SRM 1585 CHLORINATED BIPHENYLS IN ISOOCTANE

(revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean ± SD

4 - Ch I orobi pheny

I

2051629 ug/g 43.3 ± 1.0

4 , 4 ' - D i ch I orobi phenyl 2050682 ug/g 9.53 ± 0.08

2,4,4' -Trichlorobiphenyl 7012375 ug/g 3.70 t 0.02

2,2',5,5'-Tetrachlorobiphenyl 35693993 ug/g 7.72 t 0.06

3,3' ,4,4' -Tetrachlorobiphenyl 32598133 ug/g 6.62 t 0.05

2.2',4,5,5'-Pentachlorobiphenyl 37680732 ug/g 5.24 t 0.02

2,2',3,4,4',5'-Hexachlorobiphenyl 35065282 ug/g 2.37 ± 0.02

2,2',4,4',5,5'-Hexachlorobiphenyl 35065271 ug/g 3.06 ± 0.02

TABLE 1587-1: COMPILED DATA FOR NBS SRM 1587 NITRATED POLYCYCLIC AROMATIC HYDROCARBONS IN METHANOL

(revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean ± SD

2- Nitrof luorene

9- N i t roanth racene

3 - N i t r of I uoranthene

1-Nitropyrene

7-Ni trobenz [a] anthracene

6-Nitrochrysene

6- N i t r obenzo [a] pyr ene

607578

602608

829217

5522430

20268513

7496028

63041907

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

9.67 ± 0.39

5.01 ± 0.11

9.24 ± 0.06

8.95 ± 0.28

9.27 ± 0.23

8.13 ± 0.11

6.1

TABLE 1589-1: COMPILED DATA FOR NBS SRM 1589 POLYCHLORINATED BIPHENYLS IN HUMAN SERUM

(revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean + SD

Aroclor 1260

1,2,3,4-Tetrachlorodibenzo-p-dioxin

2,3,7,8-Tetrachlorodibenzo-p-dioxin

11096825 ng/g 106.0 ± 1.3

30746588 ng/g 0.153

1746016 ng/g 0.081

1585-1
TABLE 1590-1: COMPILED DATA FOR NBS SRM 1590 STABILIZED WINE (revised 3/1/86)

ELEMENT

As

CU

Fe

KMn

Na

Zn

UNITS

ug/L

ug/L

mg/L

mg/L

ug/L

mg/L

ug/L

Volatile Acidy g/L

Ethanol %

NBS

Mean ± SD

300

6

320

95

0.24

18.51 ± 0.16

CONSENSUS METHOD

Mean (n)

5.8 (1)

270 (1)

423 (1)

197 (1)

NAA

NAA

NAA

NAA

TABLE 1590-2: INDIVIDUAL DATA FOR NBS SRM 1590 (revised 3/1/86)

Cone

As (ug/L ?

5.8

Cu (ug/L)

270

Uncer Com Method Reference

14

RTNA

RTNA

84BYR 02

84BYR 02

Cone

Mn (ug/L)

423

2n (ug/L)

197

Uncer Com Method Reference

11

14

RTNA

RTNA

84BYR 02

84BYR 02

TABLE 1614-1: COMPILED DATA FOR NBS SRM 1614 DIOXIN IN ISOOCTANE (revised 3/1/86)

COMP(XJND CAS # UNITS NBS

Mean

2,3,7,8-Tetrachlorodiben2o-p-dioxin 1746016 ng/g

2,3,7,8-Tetrachlorodiben2o-p-dioxin, C-13 76523405 ng/g

98.3

95.6

TABLE 1639-1: COMPILED DATA FOR NBS SRM 1639 HALOCARBONS IN METHANOL (revised 3/1/86)

COMPOUND CAS # UNITS NBS

Mean

Chloroform 67663 ng/uL 6235

Chlorodibromomethane 124481 ng/uL 124.6

Bromodi ch I oromethane 74975 ng/uL 389.9

Bromoform 75252 ng/uL 86.5

Carbon Tetrachloride 56235 ng/uL 157.0

Trichloroethylene 79016 ng/uL 85.8

Tet rach I oroethyI ene 127184 ng/uL 40.6

1590-1
TABLE 1618-1: COMPILED DATA FOR NBS SRM 1618 VANADIUM AND NICKEL IN RESIDUAL FUEL OIL

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

ASH % 0.083

Ni ug/g 75.2 ± 0.4

S % 4.3

V ug/g 423.1 ± 3.4

1618-1
TABLE 1619-1: COMPILED DATA FOR NBS SRM 1619 SULFUR IN RESIDUAL FUEL OIL

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean ± SD

Al ug/g A.

Al ug/mL 4 —

As ng/g — 94 (1) NAA

B ug/g < 1.1 — —

B ug/mL < 1 — —

Br ng/g — 700 (1) NAA

Ca ug/g 10.6 — —

Ca ug/mL 10 — —

CI ug/g — 20 (1) NAA

Co ng/g — 350 (1) NAA

Cr ng/g < 1100 380 (1) NAA

Cr ug/mL < 1 — —

Cu ug/g < 1.1 — —

Cu ug/mL < 1 — —

Density g/cmS 0.939 — —

Eu ug/g — 10.2 (1) NAA

Fe ug/g < 5.3 23 (1) NAA

Fe ug/mL < 5 — —

La ng/g — 37 (1) NAA

Mg ug/g 1.1 ... —

Mg ug/mL 1 ... —

Mn ug/g < 1.1 — —

Mn ug/mL < 1 ... ...

Mo ug/g < 1.1 ... ...

Mo ug/mL < 1 ... —

Na ug/g 18 27 (1) NAA

Na ug/mL 17 — —

Ni ug/g 9.6 12 (1) NAA

Ni ug/mL 9 — —

S ug/g 7190 ± 70 7215 (2) NM

Sb ng/g 30 (1) NAA

Sc ug/g 1.39 (1) NAA

Se ng/g 95 (1) NAA

Si ug/g 2.2

Si ug/mL 2

Sm ug/g 2.45 (1) NAA

Sn ug/g < 1.1 Sn ug/mL < 1

Ti ug/g < 1.1

Ti ug/mL < 1 V ug/g 37 42.6 (1) NAA V ug/mL 35 Zn ug/g 4.3 1.27 (1) NAA

Zn ug/mL 4

1619-1
Cone

As (ng/g)

94

Br (ng/g)

700

CI (ug/g)

20

Co (ng/g)

350

Cr (ng/g)

380

Eu (ug/g)

10.2

23

La Cng/g)

37

Na (ug/g)

27

TABLE 1619-2: INDIVIDUAL DATA FOR NBS SRH 1619 (revised 3/1/86)

Uncer Com Method Reference

10

900

40

110

16

ITNA 85FIL 02

ITNA 85FIL 02

1.8 ITNA 83LI 01

ITNA 85FIL 02

ITNA 85FIL 02

2.4 ITNA 85FIL 02

ITNA 85FIL 02

ITNA 85FIL 02

Cone Uncer Com Method Reference

Ni Cug/g)

12

S (ug/g)

7130

7300

Sb (ng/g)

30 20

Sc (ug/g)

1.1 ITNA 85FIL 02

110

180

7

7

NM

NM

83LI 01 83LI 01

ITNA 85FIL 02

1.39 0.67 ITNA 85FIL 02

Se (ng/g)

95 27

Sm (ug/g)

2.45

V Cug/g)

42.6

Zn (ug/g)

1,27 0.35 ITNA 85FIL 02

ITNA 85FIL 02

0.47 ITNA 85FIL 02

4.7 ITNA 85FIL 02

6 ITNA 85FIL 02

1619-2
TABLE 1620-1: COMPILED DATA FOR NBS SRM 1620 SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SO

S % 4.A8 ± 0.02

TABLE 1620A- 1 • COMPILED DATA FOR NBS SRM 1620A SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

M^rin -t- SD Mean ± SD (n) Mean (n) Method

Al ug/g 18 — _ _ _

A

I

ug/mL 20 — ~ _ _ _

As ng/g 40 (1) 40 (1) NAA

B ug/g < 0.9 ~ " ~

B ug/mL < 1 ... ...

Br ng/g 600 (1) 600 (1) NAA

Ca ug/g 8.2 ...

Ca ug/mL 9

...

CI ug/g 11.8 (1) 11.8 (1) NAA

Co ng/g 80 (1) 80 (1) NAA

Cr ng/g < 900 200 (1) 200 (1) NAA

Cr ug/mL < 1 ~ ~ ...

Cu ug/g < 0.9 ... ...

Cu ug/mL < 1 ... - . -

Density g/cm3 1.096 ... ...

Eu ng/g 10 (1) 10 (1) NAA

Fe ug/g < 4.6 11 (1) 11 (1) NAA

Fe ug/mL < 5 ... ...

Flash Pt. deg. C 70 ... ...

La ng/g 500 (1) 500 (1) NAA

Mg ug/g < 0.9 . _ — ...

Mg ug/mL < 1 ... _ _ _

Hn ug/g < 0.9 . - _ . * -

Mn ug/mL < 1 . . - ...

Mo ug/g < 0.9 - - . ...

Mo ug/mL < 1 ... ...

Na ug/g 28 9.4 (1) 9.4 (1) NAA

Na ug/mL 31 ~

Ni ug/g < 0.9 < 2 < 2 NAA

Nt ug/mL < 1

S % 4 504 ± 0 010 4.48 ± 0.02 (3) 4.49 4.46 - 4.49 4.49 (1) ICPES

S % - - . 4.48 (2) NM Sb ng/g 100 (1) 100 (1) NAA

Sc ug/g 2 (1) 2 (1) NAA

Se ng/g 80 (1) 80 (1) NAA

Si ug/g 12 ...

Si ug/mL 13

Sm ug/g 9 (1) 9 (1) MAA Sn ug/g < 0.9

Sn ug/mL < 1

Ti ug/g < 0.9

Ti ug/mL < 1 V ng/g < 900 < 200 < 200 NAA

V ug/mL < 1 Zn ug/g 21 0.7 (1) 0.7 (1) NAA

Zn ug/mL 23

1620-1
TABLE 1620A-2: INDIVIDUAL DATA FOR NBS SRH 1620A (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

As (nq/q) I Ni (uq/q)

40 10 ITNA 85FIL 02 | < 2 ITNA 85FIL 02

Br (nq/q) I S (%)

600 600 ITNA 85FIL 02 | 4.46 0.13 7 NM 83LI 01

I 4.49 0.03 ICPES 85FAB 01

CI (ug/g) I 4.49 0.12 7 NM 83LI 01

11.8 1 ITNA 83LI 01 | Sb (ng/g)

Co (ng/q) | 100 140 ITNA 85FIL 02

80 60 ITNA 85FIL 02 | Se (ug/g)

Cr (ng/q) j 2 0.6 ITNA 85FIL 02

200 70 ITNA 85FIL 02 | Se (ng/g)

Eu (ng/g) | 80 20 ITNA 85FIL 02

10 3 ITNA 85FIL 02 | Sm (ug/g)

Fe (ug/g) | 9 5 ITNA 85FIL 02

11 7 ITNA 85FIL 02 | V (ng/g)

La (ng/g) | < 200 ITNA 85FIL 02

500 300 ITNA 85FIL 02 | Zn (ug/g)

Na (uq/q) I 0.7 0.5 ITNA 85FIL 02

9.4 2.9 ITNA 85FIL 02

1620-2
TABLE 1621-1: COMPILED DATA FOR NBS SRM 1621 SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS

Mean i SD

CONSENSUS

Mean ± SD (n)

MEDIAN RANGE METHOD MEANS

Mean (n) Method

S

S

s

s

s

%

%

%

%

%

1.05 ± 0.02 1.01 ± 0.05 (5) 1.05 0.9 - 1.06 1.06 (1) XRF 0.99 (1) IC 0.9 (1) MECA

1.05 (1) TITR

1.05 (1) CB

TABLE 1621-2: INDIVIDUAL DATA FOR NBS SRM 1621 (revised 3/1/86)

Cone Uncer Com Method Reference

s m

0.9

0.99

1.05

1.05

1.06

0.1

0.03

0.01

0.03

MECA

ICCB

TITR

XRF

80MCC 01 80MCC 01 84LEC 02

80MCC 01 80MCC 01

TABLE 1621A-1: COMPILED DATA FOR NBS SRM 1621A SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean (n) Method

S % 0.94 ± 0.01 0.94 ± 0.03 (7) 0.94 0.89 - 0.973 0.9715 (2) XRF

S % --- --- --- --- 0.935 (2) ICPES

S % --- --- --- "- 0.89 (1) POL

S % --- --- --- --- 0.945 (1) TITR

S % --- --- --- --- 0.931 (1) IC

TABLE 1621A-2: INDIVIDUAL DATA FOR NBS SRM 1621A (revised 3/1/86)

Cone Uncer Com Method Reference

S (%)

0.89 0.07 POL 81REL 01 0.93 0.02 ICPES 81 UAL 02

0.931 0.01 IC 82V IS 01 0.94 0.02 ICPES 84BAR 03

0.945 0.014 TITR 82V IS 01 0.97 0.009 6 EXRF 81CHR 01 0.973 0.008 6 EXRF 81CHR 01

1621-1
TABLE 1621B-1: COMPILED DATA FOR NBS SRH 1621B SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean i SD Mean ± SD (n) Mean t SD (n) Method

Al ug/g 6.5

Al ug/mL 6 — — — —

B ug/g < 1.1

B ug/mL < 1 — — — —

Ca ug/g 9.7

Ca ug/mL 9 — — — —

Cr ug/g 3.2

Cr ug/mL 3 — — — —

Cu ug/g <1.1 — — — —

Cu ug/mL < 1 — — ' — —

Density g/cm3 0.929

Fe ug/g <5.4 — — — —

Fe ug/mL <5 — — — ---

Flash Pt. deg. C 111 Mg ug/g < 1.1

Mg ug/mL < 1 — — — —

Mn ug/g 1.1 — — — —

Mn ug/mL 1 --- — — —

Mo ug/g <1.1 — — — —

Mo ug/mL <1 — — — —

Na ug/g 8.6

Na ug/mL 8 — — — —

Ni ug/g 6.5 — — —

Ni ug/mL 6 — — — —

S % 0.95 ± 0.005 0.948 ± 0.014 (7) 0.944 0.935 - 0.975 0.954 ± 0.015 (4) XRF

S % .-- --- ... --- 0.953 (1) ICPES

S % --- --- --- 0.935 (2) COUL

Si ug/g 6.5

Si ug/mL 6 — — —

Sn ug/g <1.1

Sn ug/mL <1 — — — —

Ti ug/g <1.1 — — — —

Ti ug/mL <1 — — — —

V ug/g 16

V ug/mL 15 Zn ug/g 16 — — — —

Zn ug/mL 15

TABLE 1621B-2: INDIVIDUAL DATA FOR NBS SRM 1621B (revised 3/1/86)

Cone Uncer Com Method Reference

S (%)

0.935 COUL 84TAK 01 0.935 COUL 83TAK 01 0.944 XRF 83TAK 01 0.944 XRF 84TAK 01 0.953 0.003 ICPES 85 FAB 01 0.953 0.031 32 EXRF 83SAN 02

0.975 0.031 32 EXRF 83SAN 02

1621B-1
TABLE 1622-1: COMPILED DATA FOR NBS SRM 1622 SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS

%

%

NBS

Mean ± SD

2.U ± 0.01

CONSENSUS

Mean ± SD (n)

2.16 (2)

MEDIAN RANGE

2.15 - 2.16

METHOD MEANS

Mean (n) Method

2.16

2.15

(1) ICPES

(1) CB

TABLE 1622-2: INDIVIDUAL DATA FOR NBS SRM 1622 (revised 3/1/86)

Cone Uncer Com Method Reference

2.15

2.16

0.03

0.02

CB

ICPES

84LEC 02

85FAB 01

TABLE 1622A-1: COMPILED DATA FOR NBS SRM 1622A SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS

%

%

NBS

Mean i SD

1.96 ± 0.04

CONSENSUS MEDIAN

Mean ± SD (n)

2.00 ± 0.03 (4) 2.01

RANGE

1.948 - 2.02

METHOD MEANS

Mean (n) Method

1.98 (2) XRF 2.02 (2) ICPES

TABLE 1622A-2: INDIVIDUAL DATA FOR NBS SRM 1622A (revised 3/1/86)

Cone

S (%)

Uncer Com Method Reference

1.6 0.1 POL 81REL 01 1.948 0.018 6 EXRF 81CHR 01 2.01 0.02 ICPES 84BAR 03

2.011 0.015 6 EXRF 81CHR 01 2.02 0.02 ICPES 81WAL 02

TABLE 1622C-1: COMPILED DATA FOR NBS SRM 1622C SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

2.012 ± 0.025

1622-1
TABLE 1622B-1: COMPILED DATA FOR NBS SRM 1622B SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean i SD (n) Method

Al ug/g 8.1

Al ug/mL 8

B ug/g <1 — — — —

B ug/mL < 1 Ca ug/g 24.4 — — — —

Ca ug/mL 24 — — — —

Or ug/g 1 """

Cr ug/mL 1 Cu ug/g < 1 Cu ug/mL < 1 — — — —

Density g/cm3 0.984

Fe ug/g < 5,1 --- --- ---

Fe ug/mL < 5 — — — —

Flash Pt. deg. C 65

Mg ug/g 2

Mg ug/mL 2 — — — —

Mn ug/g 1 --- — — —

Mn ug/mL 1 --- — — —

Mo ug/g <1 — --- — —

Mo ug/mL <1 — — — —

Na ug/g 25.4

Na ug/mL 25 — — — —

Nt ug/g 15.2

Ni ug/mL 15 S % 1.982 ± 0.018 1.98 ± 0.01 (6) 1.979 1.971 - 2.01 2.00 ± 0.04 (4) XRF

S % --- --- --- --- 2.01 (1) ICPES

S % --- --- --- --- 1.98 (2) COUL

Si ug/g 13.2 — — — —

Si ug/mL 13 — — — —

Sn ug/g < 1 Sn ug/mL <1 — — — —

Ti ug/g <1 — — — —

Ti ug/mL < 1 V ug/g 51

V ug/mL 50

2n ug/g 11.2 — — — —

Zn ug/mL 11 — — — —

TABLE 1622B-2: INDIVIDUAL DATA FOR NBS SRM 1622B (revised 3/1/86)

Cone Uncer Com Method Reference

S (%)

1.971 0.031 32 EXRF 83SAN 02

1.977 COUL 83TAK 01 1.977 COUL 84TAK 01 1.979 XRF 84TAK 01 1.979 XRF 83TAK 01

2.01 0.02 ICPES 85FAB 01 2.06 0.07 32 EXRF 83SAN 02

1622B-1
TABLE 1623-1: COMPILED DATA FOR NBS SRM 1623 SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean (n) Method

S ug/g 2680 ± 40 2710 ± 130 (4) 2650 2600 - 2900 2700 (1) XRF

S ug/g --- --- --- --- 2600 (1) MECA

S ug/g --- --- --- --- 2900 (1) TITR

S ug/g --- --- —•' 2650 (1) IC

TABLE 1623A-1: COMPILED DATA FOR NBS SRM 1623A SULFUR IN RESIDUAL FUEL OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean ± SD (n) Method

Al ug/g 5.4 — — — —

Al ug/mL 5 — — — —

B ug/g < 1.1

B ug/mL <1 --- — --- —

Ca ug/g 9.8

Ca ug/mL 9 — — — —

Cr ug/g 1.1 Cr ug/mL 1 — — — —

Cu ug/g < 1.1 --- ---

Cu ug/mL <1 — - - - — —

Density g/cm3 0.918 --- --- --- ---

Fe ug/g < 5.4

Fe ug/mL <5 — — — —

Flash Pt. deg. C 140

Mg ug/g < 1.1 Mg ug/mL <1 — --- --- —

Mn ug/g <1.1 --- — --- —

Mn ug/mL <1 — — — —

Ho ug/g < 1.1 Mo ug/mL <1 — --- --- —

Na ug/g 9.8

Na ug/mL 9 — — —

Ni ug/g 1.1 --- --- --- ...

Ni ug/mL 1 --- --- --- —

S ug/g 2400 ± 30 2340 ± 50 (6) 2310 2300 - 2400 2370 ± 40 (4) XRF

S ug/g --- --- --- --- 2300 (2) COUL

Si ug/g < 1.1

Si ug/mL <1 --- --- — —

Sn ug/g < 1.1 Sn ug/mL < 1 — — — —

Ti ug/g < 1.1

Ti ug/mL <1 --- — — —

V ug/g 3,3

V ug/mL 3

Zn ug/g 16.3

Zn ug/mL 15

1623-1
TABLE 1623-2: INDIVIDUAL DATA FOR NBS SRM 1623

(revised 3/1/86)

Cone Uncer Com Method Reference

S (ug/g)

2600

2650

2700

2900

200

40

500

MECA

IC XRF TITR

80MCC 01 80MCC 01

80MCC 01 80MCC 01

TABLE 1623A-2: INDIVIDUAL DATA FOR NBS SRM 1623A

(revised 3/1/S6)

Cone Uneer Com Method Reference

s (ug/g)

2300 COUL 84TAIC 01 2300 COUL 83TAK 01 2310 240 32 EXRF 83SAN 02

2380 XRF 84TAK 01 2380 XRF 83TAt( 01 2400 50 32 EXRF 83SAN 02

1623-2
TABLE 1624-1: COMPILED DATA FOR NBS SRM 1624 SULFUR IN DISTILLATE OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SO Mean ± SD (n) Mean (n) Method

S ug/g 2110 ± 40 2050 ± 120 (4)

S ug/g

S ug/g

S ug/g

TABLE 1624A-1: COMPILED DATA FOR NBS SRM 1624A SULFUR IN DISTILLATE OIL (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean ± SD (n) Method

2030 1900 - 2200 1900 (1) ICPES

2200 (1) POL

2030 (1) TITR 2080 (1) IC

Al ug/g 1.2 ... ... ...

Al ug/mL 1

B ug/g < 1 .2

B ug/mL < 1 Ca ug/g 8.2

Ca ug/mL 7

Or ug/g < 1.2

Cr ug/mL < 1 Cu ug/g < 1.2

Cu ug/mL < 1 Density g/cm3 0.848 ... ... ...

Fe ug/g < 5.9

Fe ug/mL < 5 Mg ug/g < 1.2

Mg ug/mL < 1 Mn ug/g < 1.2

Mn ug/mL < 1 Mo ug/g < 1.2

Mo ug/mL < 1 Na ug/g < 1.2 Na ug/mL < 1

Ni ug/g < 1.2

Ni ug/mL < 1

S ug/g 1410 t 20 1420 ± 20 (5) 1420 1400 - 1450 1440 ± 20

S ug/g 1400

Si ug/g < 1.2

Si ug/mL < 1 Sn ug/g < 1.2

Sn ug/mL < 1

Ti ug/g < 1.2

< Ti ug/mL < 1 V ug/g < 1.2

V ug/mL < 1 Zn ug/g < 1.2

Zn ug/mL < 1

1624-1
TABLE 1624-2: INDIVIDUAL DATA FOR NBS SRM 1624

(revised 3/1/86)

Cone Uncer Com Method Reference

S (ug/g>

1900 100 ICPES 81UAL 02

2030 50 TITR 82VIS 01 2080 210 IC 82VIS 01 2200 200 POL 81REL 01

TABLE 1624A-2: INDIVIDUAL DATA FOR NBS SRM 1624A

(revised 3/1/86)

Cone Uncer Com Method Reference

S Cug/g)

1400 COUL 84TAK 01 1400 COUL 83TAK 01 1420 90 32 EXRF 83SAN 02

1450 XRF 83TAK 01 1450 XRF 84TAK 01 1540 280 32 EXRF 83SAN 02

1624-2
TABLE 1630-1: COMPILED DATA FOR NBS SRM 1630 MERCURY IN COAL (revised 3/1/86)

ELEMENT UNITS NBS

Mean t SO

CONSENSUS

Mean ± SD (n)

ASH % — 2.2 (1)

Al ug/g — 5300 (1)

As ug/g — 19 (1) B ug/g — 5 (1)

Be ug/g — 1 <1) Br ug/g — 33 (2)

Ca ug/g — 700 (1)

Cd ng/g — < 200

CI ug/g — 1725 (2)

Co ug/g — 4.8 (2)

Cr ug/g — 7.55 (2)

Cu ug/g — 16 (1)

F ug/g — 25 (1) Fe % — 0.77 (2)

Ga ug/g — 1.08 (2)

Ge ug/g — 1 (1)

H20- % — 0.4 (1)

Hg ng/g 130 ± 10 126 t 13 (20)

Hg ng/g — —

Hg ng/g — —

Hg ng/g — —

K ug/g ... 800 (1) La ug/g — 4.4 (1)

Mg ug/g — 200 (1)

Mn ug/g — 6 (1)

Ho ug/g — 2 (1)

Na ug/g — 405 (2)

Ni ug/g — 10 (1) P ug/g — 17 (1)

Pb ug/g — 4 (1)

S % — 1.14 ± 0.20 (3)

S % — —

S % ... —

Sb ug/g — 1.15 (2)

Sc ug/g — 1.4 (1)

Se ug/g

' 2.1 2.2 ± 0.2 (6)

Se ug/g

Si ug/g 7200 (1)

Sn ug/g 6 (1)

Ti ug/g 500 (1)

V ug/g 24 (1)

Zn ug/g 6 (1) Zr ug/g 21 (1)

MEDIAN RANGE METHOD MEANS

Mean t SD (n) Method

—

~ ~ "

--

2.2

...

(1) CB

... —

—

--

29 -

--

37

...

37 —

(1) NAA —

... 1230 - 2220 —

1230 (1) IC 3.6 - 6 3.6 (1

)

NAA

...

7.1 - 8 7.1 (1) NAA

0.51 - 1.04 0.51 (1) NAA

... 1.07 - 1.1 1.07 (1) NAA

0.4 (1) GRAV

127 104 - 150 122 ± 13 (9) NAA

135 (1) OES

... 118 (1) FAE

...

...

130 ± 14 (8) AA —

——

—

4.4 —

—

(1) NAA

320 • 490 490 (1) NAA

1.07 0.99 - 1.37 1.37 (1) XRF 0.99 (1) IC 1.07 (1) CB

0.6 - 1.7 1.7 (1) NAA

1.4 (1) NAA

2.11 2.0 - 2.6 2.23 ± 0.25 (4) NAA

2.12 (1) ICPES

1630-1
TABLE 1630-2: INDIVIDUAL DATA FOR NBS SRM 1630 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Al (ug/g)

1

1 F (ug/g)

5300 W 77GLU 01 1 25 W 77GLU 01

As (ug/g)

1

1 Fe (%)

19 w ^^/^ III A 4 1 77GLU 01 1

t\ If 4 0.51 0.0204 ITNA 74TAM 01 1.04 W 77GLU 01 ASH (%)

Ga (ug/g)

i.c Co ( f GLU Ul 1 1.07 0.04 RTNA 72SAN 01

B (ug/g) 4 4 1.1 W 77GLU 01

5 W III 4 1 77GLU 01 1 Ge (ug/g)

Be (ug/q) 1 1 W 77GLU 01

1 VV

1 77GLU 01 1 H20- (%)

Br (uq/q)

1

1 0.4 GRAV 77GLU 01

29 w

1 77GLU 01 1 Hq (nq/q)

37 ITNA 74TAM 01 1

1 104 6 CVAA 80NAD 01 Ca (uq/q) 1 105 RTNA 74RIC 01

1 105 30 RTNA 72LY0 01 700 W 77GLU 01 1 106 ITNA 74RIC 01

1 118 11 FAE 76CAV 01 Cd (ug/q) 1 120 10 CVAA 73L0 01

1 124 11 CVAA 82D00 01 < 0.2 L W 77GLU 01 1 125 10 CVAA 75WIM 01

1 127 5 RTNA 740RV 01

CI (ug/q) 1 127 6 RTNA 72RAI 01

1 127 12 RTNA 72ROO 01 1230 40 IC 85GEN 01 1 130 10 RTNA 75LIT 01 2220 W 77GLU 01 1 130 10 ITNA 74TAM 01

1 135 OES 75PEC 01 Co (ug/g) 1 136 7 FAA 82UCH 02

139 7 CVAA 72RAI 01 j.o 0. 18 ITNA 74TAM Ul 1 Toy \£. C A A FAA (cVxfj Ul 6 W 77GLU 01 1 140 RTNA 75FR0 01 140 W 77 III n 1 f f bLU U1 Cr (ug/g) 150 CVAA 75MUR 01

1 486 60 ITNA 75LIT 01

7.1 0.35 ITNA 74TAM 01 1 8 W 77GLU 01 1 K (uq/q)

Cu (uq/q) 800 W 77GLU 01

16 VV 77GLU 01 1 La (ug/g)

4.4 ITNA 74TAM 01

1630-2
TABLE 1630-2: INDIVIDUAL DATA FOR NBS SRM 1630 (cont.)

Cone

Mg (uq/q)

200

(ug/g?

6

Ho <ug/g?

2

Na (ug/g)

320

490

Hi (ug/g?

10

17

Pb (ug/g ?

4

S (%)

Uncer Com Method Reference

0.99

1.07

1.37

0.05

W

W

W

W

ITNA

W

W

W

ICCBXRF

77GLU 01

77GLU 01

77GLU 01

77GLU 01 74TAM 01

77GLU 01

77GLU 01

77GLU 01

85GEN 01 77GLU 01 77GLU 01

Cone

Sb (ug/g)

0.6

1.7

Sc (ug/q)

1.4

Se (uq/q)

2

2.09

2.11

2.11

2.12

2.6

Si (ug/g)

7200

Sn (uq/g)

Ti (ug/q)

500

V (ug/g)

24

zn (ug/g?

6

Zr (ug/q)

21

Uncer Cora Method Reference

0.51

0.06

0.06

0.09

0.09

0.09

0.21

W

ITNA

ITNA

W

RTNA

RTNA

RTNA

ICPES

ITNA

W

W

W

W

W

W

77GLU 01 74TAM 01

74TAM 01

77GLU 01 740RV 01 72R00 03

77R00 02

80HAA 01 74TAM 01

77GLU 01

77GLU 01

77GLU 01

77GLU 01

77GLU 01

77GLU 01

1630-3
TABLE 1631A-1: COMPILED DATA FOR NBS SRM 1631A SULFUR IN COAL

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean + SD (n) Mean ± SD (n) Method

ASH % 5.00 ± 0.02

H20 % 0.84 ~ ~ ~ ~ ~ ~ —

Hg na/a 73

Pb ug/g 5.44 --- ... ...

S ug/g 5460 ± 30 5570 ± 250 (8) 5460 5260 - 5990 5900 (1) TCGS

S ug/g 5375 (2) TITR

S ug/g ~ *" ... 5460 (1) IC s ug/g ... 5610 ± 260 (4) CB

TABLE 1631B-1: COMPILED DATA FOR NBS SRM 163 IB SULFUR IN COAL

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean ± SO (n) Method

ASH % 14.59 ± 0.09

H20 % 0.69 ... ...

Hg ng/g 41 Pb ug/g 5.97 ... ... ...

S % 2.016 ± 0,014 2.01 ± 0.08 (6) 1.97 1.92 - 2.14 2.02 ( 1 ) TCGS

S % 1.98 (2) TITR

S % •r m m — *• — 1.97 (1) IC

S % — — 2.045 (2) CB

TABLE 1631C-1: COMPILED DATA FOR NBS SRM 1631C SULFUR IN COAL

(revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS MEDIAN RANGE METHOD MEANS

Mean ± SD Mean ± SD (n) Mean t SD (n) Method

ASH % 6.17 ± 0.02

H20 % 0.47

S % 3.02 ± 0.008 3.03 ± 0.06 (7) 3.00 2.97 - 3.117 2.98 (1) TCGS

S % 3.05 (2) TITR

S % 3.09 (1) IC

S % 3.00 ± 0.04 (3) CB

1631-1
TABLE 1631A-2: INDIVIDUAL DATA FOR NBS SRM 1631A

(revised 3/1/86)

Cone Uncer Com Method Reference

s (ug/g)

5260 350 TITR 80ARO 01 5420 60 CB 86GAU 01 5450 80 CB 8ALEC 02

5460 IC 77SMI 05

5490 TITR 74HIC 01 5590 50 CB 84GLA 11 5900 400 TCGS 77JUR 01 5990 20 CB 85GLA 03

TABLE 16313-2: INDIVIDUAL DATA FOR NBS SRM 1631B

(revised 3/1/86)

Cone Uncer Com Method Reference

S (%)

1.92

1.95 0.07

1.97

2.02 0.05

2.042 0.067

2.14 0.09

TITR 74HIC 01 CB 85GLA 03

IC 77SMI 05

TCGS 77JUR 01 TITR 80ARO 01 CB 86GAU 01

TABLE 1631C-2: INDIVIDUAL DATA FOR NBS SRM 1631C

(revised 3/1/86)

Cone Uncer Com Method Reference

S (%)

2.97

2.98 0.02

2.99

3 0.05

3.04 0.03

3.09

3.117 0.097

CB 82AN0 01 TCGS 77JUR 01 TITR 74HIC 01 CB 85GLA 03

CB 86GAU 01

IC 77SMI 05

TITR 80ARO 01

1631-2
g

So < UJ O u> O

UJ CA C/l " lU UJ O O

«- ca

-O lA •OOOOOO •INJfM

i/\ rsj

8

"8

UJ 0) OD S U S O U (A I- O. U

(9 < W < U 4 LU S a. o a. >— CLa.c/>a.o.»-a.a.

M

a. (A

C/> LU

UJ (/> o —

lU C

»—O

rg •o fM «- *- •->0»-fM»-rsl»-f\Jf\J "-M

g 58

in «- fNJ O 44 O

o o o o in i/> o o f\J »— o • o fvj O 00 in f\j

fNJ ro •-co

+4 I CO

g

Kl

r\j M

COo ru

>0

r- w IM

o. o o

00 o CO in in

rvj

f\J ^ s. o o

<>• +1 +H 1 +1 • 1 +1 +1 fi +1 +1 o o o CO 1^ CO ro

K>

OJ in o rg o CO in C> in

'J- OsJ

«- (M lA

o

°

CO ' *i

CO Nj- o o

Kl O

ro oCO

8:

ro o

o o

in o m

< O CO

«- in

«— in

«- o o

CM +4 -H +t

ro -J- O O 'J- OO o O ' o o fNl

1 o 1 o 00 N-'

fNJ . fNJ ' 1 fNJ CO in

ro ro uS o >0 ro ro fNJ PO ro fNJ fNJ ro r\j ro o CO o o o in fNJ fNJ (M nj O

Ki o in -4- (M O o o fNJ O o +1 H +1 > •H H +(

>o rg o O O O O O o <f ro

fNJ CO o o' in fNJ o rj o CO in

>* r\j

cji m o> CTi

CTl —(/)(/) (/) < < CD CQ (_J LJ LJ

1632-1
</)</) (J (/) o

o o 2 S •sj K)

ITv 00 COO

5 S

a. t- »- o

< t3

(_> — Q.

f\J »- (M «— (M «- in r\j «- m fvj ^

>6 o o «- -vj fM >j- f\J I »- o «-O O

o o rvj in

fVJ o

in I r- ^ ro t »-

T- tin *-

^ X

CO

in

00

O o in

CO in s» rvj rg

I I I in

I 1 I ! I I 1 00 I +4 ** 1 <r « +1 rg ' ' &> o CO •4- rg

N*

OJ m"

rg

in ro o c in ro o o in in rg rg OJ rg rg *^ o 00 in t— o o o rg o o o in ro rg

f\i

; ; *t +1 H H ; ! H H ; H ; ; M ! *i Z

in rj 00 o IM in CO o <r o 00 CO o o in in ro ro ro

in rg rg oo o ro ro (y o rg

£

oo r*- o

in

-J- PO o o -3 in o o

H m rg o H 00 CO

rvj in nJ 00 rg oJN- in ro o in s. o ro

in <o in o o in o o CO PO O

00 o 00 in ^0 ro o

00 ro 'J- (M ro ro rg rg in >j

in rj rg r\j o O o CO o o o 00 in o CO s rg o CO ro o o rg

rg >d t> PO

d- o rg rg OJ ro

oo <i CO CO in N- (M o O fO o in o in o o rg 1 o in

in K) o o rg ro o CO in r«j (NJ o rg Kl ro CO ro ro o"

rg

00 o O rg in OJ N- PO O ro in -o o o o O

rg rg ro ro rg in ro

fVJ o o ru •vj- sO o r«- in o O CO •o ro o O o o rg O rg o o OJ og o o OJ rg

o m O O

rvi CO 00 rg rg in 00 o nO O O o CO o O o in o m ro CO rg OJ N. m rg rsi rg rg N. o tn in ro o OJ rg "Jorg PO

44 o o in

(NJ

cn o o> O) t7) cn CTi cn Ol Ol Ol O) u> CD \ \ "-^ •v.

IT> OJ O) D> O) E31 ? Ol Ol o> O) J* a*

Ol Ol CJl 3 c c 3 c c 3 3 3 3 3 3 3 3 3 3 3 3

"D 0; 6

r>j H- o c 3 Ol C c O (D J3 T3 z z -J X Z z z z Z Z z Z

rg

«— V

1632-2
I/) CO g 5

w w

ro f\j «-

fM ro -o fO fO

c8 oS N. irt

rvj fvj ro fNj

5d 5 3C O < (/) U Q. CO u en S S 3 »~ U CL O. O. > I < <n (A < < (/> a. ass >- a a. a. u o. I- 5 5

CO (/) «t

UJ UJ < O O Q. S

rj Nj- ro fvj in »- (M *- u-» »- rj ro »- in ro -O f\i «-

rvj ro o

ro o o ro ro

ro ut o

o o o o

V I ro 'O <-

in o n* t ir> ro Kl I

ro o in o o

o

ro >*

CO

COro -M ro I +1 oro

o

o

in +4 >0

»- ro ro ro in

ro CO

+4 CO o>

ro f\J

4 ro +i I »— o o o

Nj- CO <-

ro ro ro

o

ro ro

ro o

w ro

CO o o

nO o o

ro iTt o «-

8:

ro «- <-

ro *o

ro O in

+1 f\j O CO CO roro

COro

ro O o >t

r\j ro

ro o o ro

ro ro

+1 +1 +4

IT* o o CO

•J- ro ro

ro

CO

o

CO

ro o sO

+1 o H

nj

>* >* ro ro »-«-«- o in o o o o ro ^ o *- o» in o o ro

ro roo 00

ro -st ro

ro ro ro ro

ro in o» o o o P*- 5> rs- ro in oj o o m ro »— o o o o o m ro

2 . s o o o o o ro o o ro o • in ro o o ro stf' • o- ro

N- r^

ro o «- »- CO ^ f\l

+4 ro *4

•O ro >* o o o

ro CO o o o 00 > ro ro N- ro o »-

>0 ro o o o o o • • m in CO

«- ro ro Nin o

o o r»- in o ro

o o in • ro o o

N- N.

ro «-

o

41 ^ ro o

D) O) Cn Q)

""v U> Oi U> 3 3 3

m uy m ot o> Oi CT) cr oi

3 D

>v

C7> O) )

C 3 3

o. a. o.

1632-3
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Aq (nq/q)

1

1 A I \A) eoni

< lUU 1 1 NA 75RUC

1 01 1 1

1 .TOOR n 1 U. 1 VDC 70DDA ni

< 1 An 1 1 NM 77MAE 01 1 ? 1 1 n'i 7AUFU ni

< 76WEW 01 1 1 1 NA f r uLU U 1

< 1 TU A 1 1 NA 77CAH 01 1

•XJ

n 1 U. 1 < 81CHU 01 1 < CCVl f TklA 1 1 NA 82SUZ 02 1 AS cug/gj

< L(\n hUU DAA KAA 76CHA 01 1 45 c3 DTUA K 1 NA 77NAD 02 1 TJ c r JorA U

60 30 ITNA 750ND 01 1 4.5 0.4 ITNA 75RIC 01 60 ou f

i TUA 1 NA 73ABE 01 1 H .O U.J TTMA i 1 NA f ONAU VC

70 34 SSMS 77PAU 01 1 4.61 0.32 ITNA 75NAD 02

80 MM 76UEU 01 1 L 7 TTMA 1 1 nn 7ftMAr ni

1050 1 uu DAA rAA 74CHA 01 1

1

L 7

c

1

1 nu.oA un

CVPC CAK r Uco7Qfl 1 A n 1

f yu 1 A u 1 flnn A ni

Al (%) 1

1

C 1 J m 1 «J mJ71I

TTMA 1 1 NA

1 Lrto

7A^i IP n 1

AlkiAn O ni 1 NAU U

1.51 u uo UANMAA 76HAN 01 1 n 1 T CklA 1 CNA 7ALiAki ni f OWAN U

1.57 /•* MAAA 79REI 01 1 nu.o7 EAP rAC Ann CI ni

1.57 f TklA 1 1 NM 73SHE 01 1 > L rr\i LULUKno 77ADII ni fAKU U

1.59 U.C T TklA 1 1 NM 76RAG 01 1 c c J mJ TTUA 1>I NA 7CL'i p ni

1.6 1 UrCd 80NAD 01 1 ^ ^R n 77 PAA rAA A^DPki ni

1.6 Ti; T1 IMA 1 NM 81GLA 03 1 ^ • o PAA rMM 7Ani IT n 1 f OuU 1 w

1.62 Ill u TTMA 78MAC 01 1 fiu . ?c TTMA i 1 nn 77APII ni

1.64 80NAD 01 1 iJ »oA n 7A PAA rnn 77APII 1 1 MRU niU

1.66 80NAD 01 1 S 7 TTMA 1 1 nn 77RI (1 ni

1.66 n OR 84NAD 01 1 QJ m 71 FAA rMn TSPni ni

1.67 0 01 1

Trppc I CO 85HAR 01 1 S 7 TTMA 1 1 nn 7AUFA f owcn niu

1.68 0 01 TTMA 83NDI 01 1 S 7 n 17 RTMA i\ 1 nn tspiip ni

1.68 nu 1 Uuo 80AND 01 1 J m f n ? un PAFMC 70FPI ni

1.68 1 Uuo 79FAI 01 1 c 7 nU . 7c PAA "MM 7AUAY f oriM 1 niu 1 1.69 1

1 1 85HAR 01 1 c 7 1

T TMA 1 NM 70CDII ni f yrKu u

1.71 T TklA 1 1 NM 77MAE 01 1 c 7 nU mJ TTMA 1 1 NA 77Anp ni r OADC U

1.71 T1 TMA 1 NM 78LAU 02 1 s 7*; n 77 PAA rMM 7/puA ni

1.72 n no T1 TUA 1 NM 75RIC 01 1 > R n 7 PAA rMM 7APHA f OL>nM niU 1 1.73 T1 TklA 1 NM 76BL0 01 1 S R nU.J7 T

1 TMA 1 NM 7APAn f OKMu niU

1.74 f1 TklA 1 NM 77R0W 03 1 t^ B RO flu.o7 TTMA 1 1 NM 77MAP ni

1.74 nu klAA NMM 79STE 01 1 i^ > Ro nu.o7 PAA rMM 77IPP ni

1.74 0-4 ITkIA 76STE 05 1 S R PTMA r\ 1 nn 1.76 ITMA 1 1 NM 78NAD 02 1 ^ • Ro u . ^ iTTMA 1 NM 7ARI f ODLUn niU

1.76 I TklA 75NAD 02 1 S 0 0u.o7 ITMA 1 1 Nn 70fiPF r Tunc niU

1.78 0 OR TTMA I 1 NM 73ABE 01 1 J • 0T U « f TTMA i 1 NM A1UAM O 1 WMN niU

1.8 TTMA 84CLE 01 1 S 0 TTMA 1 1 Nn TTcup r jonc niU

1.8 0 18 TTMA I 1 nn 76UEU 01 1 Ao • nu nu.o7 1TTMA 1 nn 7AI All n?

1.82 0 06 I wr CO 81CHU 01 1 AO.I1 0u.o7 nrMF^ ui^nco 7*iTAI r J 1 nu ni\j 1 1.85 ITMA I 1 nn 78WEA 01 1 AO.I1 0 4 TTMA 1 1 nn 77Rnu / f nun n^UH 1.85 0 08 TTMA I 1 nn 79GRE 01 1 ftO . 11 nV m sJ ypF 70FRII ni

1.85 0.13 ITNA 750ND 01 1 6.1 0.55 ITNA 77JER 01 1.85 0.13 FAA 77PIL 01 1 6.1 1.4 ITNA 750ND 01 1.86 ICPES 80NAD 01 1 6.2 0.8 6 PAA 82SEG 01 1.9 ITNA 75KLE 01 1 6.2 1.3 ITNA 77CAH 01 1.9 0.19 ITNA 81 WAN 01 1 6.27 0.89 RTNA 77JER 01 1632-4
TABLE 1632-2: INDIVIDUAL DATA

Cone Uncer Com Method Reference I

As (ug/g) cont.

6.3 0.2 lENA 77R0U 04

6.3 0.2 D NAA 79STE 01 6.3 0.3 ITNA 85FIL 01 6.3 1 6 PAA 82SEG 01 6.3 1 PAA 80SEG 01 6.4 0.2 lENA 77R0W 03

6.5 0.3 NAA 76HAN 01 6.5 0.5 ICPES 80HAA 01 6.5 1.2 lENA 76STE 05

6.5 1.4 D NAA 740ND 01 6.6 34 UXRF 82MIL 01 6.6 1.3 ITNA 76WEU 01 7 AA 76WEU 01 8 2 PAA 750ND 01 8.9 0.2 ITNA 82SUZ 02

8.9 0.5 ITNA 75RUC 01

ASH (%)

12.17 CB 79PRA 01 13.2 34 CB 82MIL 01

Au (ng/g)

< 1 L ITNA 77CAH 01 < 20 ITNA 75RUC 01 < 30 L ITNA 73ABE 01

< 300 L ICPES 81CHU 01 0.85 0.03 RTNA 77NAD 02

0.99 0.16 RTNA 77NAD 01 146 48 ITNA 73SHE 01 200 ITNA 78WEA 01

<ug/g>

29 ICPES 81 NAD 01 30 1.1 OES 76UEU 01 42,1 0.7 TCGS 79FAI 01 42.1 0.7 D TCGS 80AND 01 43 W 77GLU 01 47 1.6 6 TCGS 76GLA 01 47.7 1.6 6 TCGS 76GLA 01 47.7 1.8 6 TCGS 76GLA 01 118 ITNA 77GLU 01

NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

Ba (ug/g)

87 5 9 ITNA 82SUZ 02

104 5 9 ITNA 82SUZ 02

152 37 ICPES 84NAD 01 183 ICPES 80NA0 01 256 ICPES 80NAD 01 274 31 ITNA 76STE 05

280 ITNA 75MIL 01

300 60 ITNA 78LAU 02

301 34 WXRF 82MIL 01 302 8 ITNA 76RAG 01 306 20 lENA 77R0W 04

306 20 D NAA 79STE 01 309 24 ITNA 77R0W 04

310 11 ICPES 85HAR 01 310 35 ITNA 81GLA 03

310 10 11 ICPES 85HAR 01 310 30 ITNA 78MAC 01 311 25 ITNA 75NAD

31

1

25 ITNA 78NAD

314 20 PAA 74CHA 01 314 43 ITNA 81UAN 01 315 20 PAA 76CHA 01 320 20 NAA 76HAN A401 320 77 ITNA 85FIL A401 322 20 lENA 77R0W 03

337 42 ITNA 73SHE 01 338 13.8 lENA 76STE 05

338 14 D NAA 79STE 01 345 70 ITNA 76UEW 01 350 ITNA 78WEA 01 350 20 ITNA 77MAE 01 350 30 ITNA 79GRE 01 352 30 ITNA 750ND 01 354 84 ITNA 79R0S 03

360 20 9 ITNA 78LAU 02

366 34 ITNA 75RUC 01 385 40 ITNA 77CAH 01

390 20 ITNA 73ABE 01 390 40 ITNA 79FRU 01

405 ITNA 75KLE 01 410 82 OES 76UEW 01 c

1632-5
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/q)

1

1

1

Br (ug/g) cont.

1.1 0.47 ICPES 84NAD 01 1 19 4 ITNA 75RIC 01 1.2 0.07 OES 76UEW 01 1 19.2 0.6 ITNA 77R0W 04

1.24 FAA 75P0L 01 1 19.2 1.2 ITNA 77MAE 01 1.49 0.03 FLUOR 77WIC 01 1 19.3 ITNA 78UEA 01 1.5 AA 76WEW 01 1 19.3 1.9 ITNA 750ND 01

1.5 0.1 FAA 750WE 01 1 19.5 0.3 lENA 76STE 05

1.52 0.11 6 FAA 77GLA 02 1 19.6 0.4 D NAA 79STE 01 1.56 0.07 11 AA 82LIN 03 1 19.6 0.4 D lENA 77R0W 04

1.57 0.12 6 FAA 77GLA 02 1 19.6 0.4 lENA 77R0W 03

1.63 0.05 11 AA 82LIN 03 1 20 ITNA 77GLU 01 1.69 0.07 11 AA 82LIN 03 1 20 2 ITNA 79GRE 01 1.7 4 AA 79REI 01 1 20 3 ITNA 73SHE 01 1.7 ITNA 77GLU 01 1 23.7 3.2 EXRF 73SPA 01 1.7 0.03 ICPES 81CHU 01 1 38 1 ITNA 82SUZ 02

1.7 0.4 35 FAA 76GLA 02 1 1.77 ICPES 80NAD 01 1 C (%)

1.85 ICPES 80NAD 01 1

1 68.93 0.11 CB 80SCH 02

(ug/g) 69.6 2.1 35 CB 79GLA 04

70 5 D TCGS 80AND 01 < 1 L WXRF 82MIL 01 1 70 5 TCGS 79FAI 01 < 1 L PAA 76CHA 01 1 71 .7 CB 79PRA 01 < 1 L AA 76WEU 01 1 73 3 35 TCGS 79GLA 04

< 1.5 L OES 76UEU 01 1 1.05 PAA 74CHA 01 1 Ca (ug/g)

(ug/g)

1

1 2400 600 ITNA 82SUZ 02

1 2840 80 GAMMA 750N0 01 7.8 5.8 ITNA 81UAN 01 1 3300 500 D TCGS 80AND 01

14 2 ITNA 76STE 05 1 3300 500 TCGS 79FAI 01 14.2 ITNA 75KLE 01 1 3500 300 D NAA 79STE 01

15 1 ITNA 78MAC 01 1 3500 300 ITNA 76STE 05

15.2 1.4 ITNA 75NAD 02 1 3500 2800 ITNA 77R0W 03

15.2 1.4 ITNA 78NAD 02 1 3600 ITNA 84CLE 01 15.6 0.4 ITNA 85GAU 04 1 3700 400 NAA 76HAN 01 16.2 1 5 lENA 79GLA 02 1 3890 40 11 ICPES 85HAR 01 16.6 0.6 NAA 76HAN 01 1 3940 11 ICPES 85HAR 01 17 1 , ITNA 78LAU 02 1 4000 ICPES 80NAD 01 17 2 ITNA 79FRU 01 1 4030 480 14NAA 77VAN 01 17 2 ITNA 73ABE 01 1 4070 560 ITNA 73SHE 01 17 2 XRF 79FRU 01 1 4100 400 ITNA 79GRE 01. 17.2 ITNA 76RAG 01 1 4100 500 ITNA 81WAN 01 17.4 1.1 lENA 84GLA 02 1 4140 140 ICPES 81CHU 01 17.5 0.3 EXRF 79GIA 01 1 4200 ICPES 80NAD 01 17.9 0.3 5 lENA 79GLA 02 1 4200 300 ITNA 77MAE 01

18 34 WXRF 82HIL 01 1 4200 400 PAA 76CHA 01 18 2 ITNA 76KUC 01 1 4200 500 XRF 79FRU 01 18.2 2.3 ITNA 75RUC 01 1 4200 500 ITNA 750ND 01 18.8 0.9 ITNA 83NDI 01 1 4200 600 ITNA 76RAG 01 18.8 2.4 ITNA 77CAH 01 1 4300 200 ITNA 78NAD 02

19 1 XRF 79PRA 01 1 4300 200 ITNA 75NAD 02

1632-6
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

Ca (ug/g) cont.

4400 ITNA 75ICLE 01 4400 100 ICPES 84NAD 01 4400 900 ITNA 76WEW 01 4420 120 XRF 79PRA 01 4500 ICPES 80NAD 01 4700 600 PAA 750ND 01 4950 4 AA 79REI 01 5000 ICPES 80NAD 01 5100 1000 OES 76UEW 01 5300 35 ITNA 81GLA 03

7000 ITNA 77GLU 01

:d (ng/g)

170 6 7 FAA 85FUD 01 170 36 SSMS 77PAU 01 180 10 AF 75EPS 01 180 14 AF 74RAI 01 180 20 D TCGS 80AND 01 180 20 TCGS 79FAI 01 180 40 6 PAA 82SE6 01 190 POL 74MAI 01 190 2 7 FAA 85FUD 01 199 20 PAA 74CHA 01 200 20 RTNA 77JER 01 200 20 PAA 77JER 01 200 20 PAA 76CHA 01 200 50 6 TCGS 76GLA 01 200 100 6 PAA 82SEG 01 210 10 FAA 77GLU 01 210 20 FAA 74RAI 01 230 10 7 AA 73TAL 01 230 10 FAA 74TAL 01 230 20 RTNA 740RV 01 230 20 RTNA 84DEL 01

C 1 no fll

240 30 FAA 74TAL 01 240 30 7 AA 73TAL 01 250 FAA 78GUI 01 250 FAA 75P0L 01 250 70 PAA 80SEG 01 310 IDMS 75KLE 01 310 AA 76UEW 01 400 200 SSMS 77D0N 01 700 350 OES 76WEU 01

Cone Uncer Com Method Reference

Ce (ug/g)

17.34 0.089 ITNA 73SHE 01 18.5 ITNA 75KLE 01 18.8 1 ITNA 76RAG 01 19 0.7 ITNA 85FIL 01 19 1 ITNA 78LAU 02

19.5 0.7 D ITNA 77R0W 04

19.5 0.7 ITNA 77R0W 03

19.5 0.7 ITNA 77XAE 01 19.5 0.7 D NAA 79STE 01 19.5 1 ITNA 750ND 01 19.7 0.2 ITNA 76UEU 01 19.7 0.56 ITNA 75NAD 02

19.7 0.6 ITNA 78NAD 02

20 ITNA 75MIL 01 20 1.2 PAA 76c HA 01 20.1 3.7 ITNA 77CAH 01 20.4 0.3 ITNA 840DD 01 20.6 0.2 RTNA 840DD 01

21 1 ITNA 79GRE 01

21 .2 3.5 ITNA 81 WAN 01

21 ,5 1.7 NAA 76HAN 01 21.5 1.8 ITNA 83NDI 01 22.6 2.2 lENA 77R0W 04

22.8 0.5 ICPES 81CHU 01 23 OES 82GUP 02

23.3 2.7 ITNA 75RUC 01 24 34 WXRF 82MIL 01 26 5 ITNA 78MAC 01 29 1 12 ITNA 82SUZ 02

29 1 12 ITNA 82SUZ 02

30 15 OES 76UEW 01

80 20 ITNA 73ABE 01 750 75 ITNA 73SHE 01 760 35 ITNA 81GLA 03

800 50 ITNA 78MAC 01 810 34 WXRF 82MIL 01 810 30 ITNA 82SUZ 02

811 5 XRF 79PRA 01 o 1 r OAyo I1 TMA 1 nn A1UAM 01

828 22 ITNA 76RAG 01 844 37 ITNA 77R0W 03

844 37 ITNA 76STE 05

844 37 D NAA 79STE 01 846 44 ITNA 75RUC 01 850 40 IC 85GEN 01 850 150 ITNA 79FRU 01 860 54 ITNA 77CAH 01 866 40 ITNA 75RIC 01 1632-7
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

Cl (ufl/g) cont.

880 UNA 84GLA 02

890 ITNA 78UEA 01 890 50 ITNA 79GRE 01 890 100 PAA 76CHA 01 890 125 ITNA 750ND 01 895 15 D TCGS 80AND 01 895 15 TCGS 79FAI 01 915 ISE 81 NAD 01 915 IC 83NAD 01 NAA rOHAN U 1 930 ISE 83NAD 01 HO rnn f Hi#nn 01

945 35 ITNA 75NAD 02

945 35 ITNA 78NAD 02

990 20 ITNA 77MAE 01 1000 ITNA 77GLU 01 1000 ITNA 75KLE 01 1177 ISE 80NAD 01

:o (ug/g)

3.9 0.2 ICPES 81CHU 01 4.3 11 ICPES 85HAR 01 4.7 0.32 OES 76UEU 01 4.8 0.3 ITNA 76BL0 01 4.9 ICPES 80NAD 01 5.0 34 UXRF 82MIL 01 5.1 0.6 ITNA 78NAD 02

5.13 0.57 ITNA 75NAD 02

5.2 0.1 ITNA 79FRU 01 5.2 0.4 ITNA 73ABE 01 5.3 0.4 ITNA 76KUC 01 5.31 0.41 ITNA 83NDI 01 5.4 4 AA 79REI 01 5.46 0.2 ITNA 79R0S 03

5.48 0.15 ITNA 73SHE 01 5.5 0.3 ITNA 77CAH 01 5.5 0.4 PAA 74CHA 01 5.5 0.6 ICPES 84NAD 01 5.51 0.6 ITNA 76RAG 01 5.58 0.21 ITNA 75RUC 01 5.6 0.4 PAA 76CHA 01 5.7 ITNA 78WEA 01 5.7 0.1 ITNA 78LAU 02

5.7 0.12 ITNA 77R0W 03

5.7 0.12 D NAA 79STE 01 5.7 0.12 lENA 77R0W 04

5.7 0.3 11 ICPES 85HAR 01 5.7 0.4 ITNA 750ND 01 5.78 ICPES 80NAD 01 5.8 0.6 ITNA 76UEW 01

1632-

Conc Uncer Com Method Reference

Co (ug/g) cont.

5.8 0.6 ITNA 85FIL 01 5.9 ITNA 75KLE 01 5.9 0.5 AA 79R0S 03

6 0.02 ITNA 78MAC 01 6 0.2 ITNA 796RE 01 6.01 0.16 ITNA 77R0U 04

6.1 0.1 ITNA 77MAE 01

1 1 NA r Dm L U1 6.39 0.74 ITNA 81 WAN 01

I

1 TUA 1 Nn 6.57 0.47 NAA 76HAN 01 6.6 ITNA 84CLE 01 6.9 35 ITNA 81GLA 03

7 AA 76WEW 01 8.5 4.2 EXRF 79GrA 01

11 ITNA 77GLU 01

(ug/g)

8 EXRF 82KEE 01 9 2 XRF 79PRA 01

14.1 3.2 ICPES 84NAD 01

15 ICPES 80NAD 01 16 11 ICPES 85HAR 01 16 1.2 OES 76WEU 01 17 1 ITNA 75RIC 01 17 1 11 ICPES 85HAR 01 17.6 1 ITNA 76RAG 01 17.8 2 ITNA 77CAH 01 18 ICPES 80NAD 01 18 2 XRF 79FRU 01 18.3 1.8 ITNA 85FIL 01 18.5 1.7 ITNA 78MAC 01 18.8 1.1 ITNA 76BL0 01 18.9 2.2 ITNA 75NAD 02

18.9 2.2 ITNA 78NAD 02

19 AA 76WEU 01 19 0.8 ITNA 73SHE 01 19 2 ITNA 79FRU 01 19 2 ITNA 73ABE 01 19 2.8 ITNA 79R0S 03

19 3 SSMS 77D0N 01 19.4 FAA 75POL 01 19.4 1.3 11 AA 82LIN 03

19.5 0.8 PAA 76CHA 01 19.6 0.5 ITNA 77MAE 01 19.6 0.6 AA 79R0S 03

19.7 0.9 0 NAA 740ND 01 19.7 0.9 ITNA 750ND 01 19.8 FAA 78GUI 01 20 AA 78GUI 01
TABLE 1632-2: INDIVIDUAL DATA

Cone Uncer Com Method Reference I

Cr (ug/g) cont.

20 ITNA 84CLE 01

20 1 9 ITNA 78LAU 02

20 3 ITNA 78LAU 02

20.17 0.76 RTNA 74MCC 01

20.2 0.4 AA 74RAI 01 20.3 1.4 11 AA 82LIN 03

20.3 2.9 ITNA 75RUC 01 20.5 0.6 ITNA 79GRE 01

20.6 ITNA 75MIL 01 20.6 2.3 lENA 77R0W 04

20.8 0.6 ICPES 81CHU 01 20.8 0.8 ITNA 77R0W 03

20.8 0.8 D NAA 79STE 01 20,8 0.8 D ITNA 77R0W 04

21 2 ITNA 75KLE 01 21.5 ITNA 78UEA 01 21.5 1 NAA 76HAN 01 21.6 2 ITNA 76WEU 01 21.6 2.1 PAA 74CHA 01 22 ITNA 77GLU 01 22 8 EXRF 79GIA 01 23 4 AA 79REI 01 24 3 ITNA 76iaJC 01 25.2 3.8 ITNA 81 WAN 01 32.3 0.9 12 ITNA 82SUZ 02

34.9 0.9 12 ITNA 82SUZ 02

(ug/g)

0.35 0.04 PAA 74CHA 01

1.3 0.1 PAA 76CHA 01

1.3 0.2 ITNA 78LAU 02

1.32 0.11 ITNA 78NAD 02

1.32 0.11 ITNA 75NAD 02

1.36 0.1 lENA 76STE 05

1.4 ITNA 75KLE 01 1.4 34 WXRF 82MIL 01 1.4 ITNA 73UEA 01 1.4 0.08 ITNA 76RAG 01 1.4 0.1 ITNA 73ABE 01 1.4 0.1 9 ITNA 78LAU 02

1.4 0.1 ITNA 750ND 01

1 L ITMA 1 1 PIM r OMCM U 1 1.46 0.11 lENA 77R0U 03

1.49 0.22 ITNA 77R0W 04

1.52 0.11 lENA 77R0W 04

1.52 0.11 D NAA 79STE 01 1.6 0.1 ITNA 85FIL 01 1.6 0.2 ITMA 79GRE 01 1.71 0.04 ITNA 77MAE 01 1.73 0.09 ITNA 79R0S 03

1632-

NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

Cs (ug/g) cont.^

1 ft 1 1 NA 0 luLA \ii 1.8 0.1 NAA 76HAN 01 1.8 0.3 ITNA 75RUC 01 1.8 0.3 ITNA 77CAH 01 1.9 0.2 ITNA 81 WAN 01 2.3 0.1 ITNA 82SUZ 02

2.55 0.06 ITNA 73SHE 01 2.6 ITNA 75MIL 01 3.5 1.3 ITNA 78HAC 01

13 EXRF 82KEE 01 14.1 0.9 ITNA 73SHE 01

15 1.2 ITNA 77R0W 03

15 1.2 D NAA 79STE 01

15 1.2 ITNA 76STE 05

15 2 XRF 79FRU 01

15 3 SSMS 77D0N 01 15.1 0.7 11 ICPES 85HAR 01 15.7 2.7 ITNA 81 WAN 01 16.3 FAA 78GUI 01 16.8 AA 78GUI 01 16.8 1 8 SSMS 80KOP OW

17 0.3 AA 73TAL 01 17 1 35 RTNA 77GLA 01 17 4 EXRF 81KIN 01 17 7.5 OES 76UEW 01

17.1 0.2 11 AA 82LIN 03

17 2 0 5 ICPES 81CHU 01 17.4 11 ICPES 85HAR 01 17.7 1.5 EXRF 79GIA 01 17.9 0.2 AA 74RAI 01

18 ICPES 80NAD 01

18 XRF 75ICLE 01

18 34 WXRF 82MIL 01

18.1 0.8 NAA 76HAN 01 18.4 0.3 11 AA 82LIN 03

18.4 1.1 SSMS 77PAU 01

19 ICPES 80NAD 01

19 3 ICPES 84NA0 01

19.4 1.9 FAA 74RAI 01 20 4 AA 79REI 01

21 AA 76UEU 01 22.6 3 EXRF 73SPA 01

23 ITNA 77GLU 01

24 3 XRF 79PRA 01

24 3 6 PAA 82SEG 01 30 10 6 PAA 82SEG

30 10 PAA 80SEG

1
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Dy (uq/q)

1

1 Eu (ng/g) cont.

0.57 0.04 NAA 76HAN

1 01 1 410 60 OES 76WEW 01 0.85 0.06 ITNA 73SHE 01 1 420 10 ITNA 77MAE 01

1 0.1 ITNA 78MAC 01 1 420 20 ICPES 81CHU 01

1.1 0.1 RTNA 8400D 01 1 480 90 ITNA 81UAN 01 1.12 0.06 D NAA 79STE 01 1 500 60 ITNA 82SUZ 02

1.12 0.06 ITNA 76STE 05 1 1.12 0.06 ITNA 77R0W 03 1 F (ug/g)

1.2 0.2 ITNA 8400D 01 1 1.3 AA 82GUP 02 1 51 ITNA 77GLU 01 1.3 0.5 ITNA 75RUC 01 1 65 ISE 83KNA 01 1.38 0.09 ITNA 75NAD 02 1 71 IC 83NAD 01 1.4 ITNA 75MIL 01 1 71 ISE 81 NAD 01 1.4 0.1 ITNA 78NAD 02 1 80 4 ISE 74TH0 01 1.59 0.16 ITNA 77CAH 01 1 81 W 77GLU 01 2.4 0.2 ITNA 82SUZ 02 1 87

90

ISE

ISE

74TH0 01 83NAD 01 Er (ug/g) 1 91 100

5 ISE AA

83BET 02

76UEU 01

< 3 L WXRF 82MIL 01 1 < 15 L OES 76UEW 01 1 Fe (ug/g)

0.7 AA 82GUP 02 1 9.3 0.2 RTNA 8400D 01 1

1

6500

7000

1300

400

OES

ITNA

76UEW 01 76BL0 01 Eu (ng/g) 1

1

7150

7200

800 EXRF EXRF

73SPA 01 82KEE 01 210 ITNA 75KLE 01 1 7517 119 ITNA 73SHE 01 270 20 ITNA 76RAG 01 1 7600 100 ICPES 84NAD 01 280 10 ITNA 73ABE 01 1 7790 360 EXRF 79GIA 01 299 33 ITNA 76STE 05 1 7800 200 ITNA 75RIC 01 300 100 ITNA 78MAC 01 1 7800 350 XRF 79FRU 01 312 37 ITNA 73SHE 01 1 7900 ITNA 84CLE 01 330 ITNA 78UEA 01 1 8000 ICPES 80NAD 01 330 40 ITNA 750ND 01 1 8100 500 ITNA 79FRU 01 340 10 NAA 76HAN 01 1 8100 700 ITNA 73ABE 01 340 14 ITNA 83NDI 01 1 8200 ICPES 80NAD 01 340 20 ITNA 78LAU 02 1 8230 80 11 ICPES 85HAR 01 340 40 ITNA 77R0W 03 1 8300 ICPES 80NAD 01 340 50 ITNA 840DD 01 1 8300 600 ITNA 85FIL 01 344 15 ITNA 79R0S 03 1 8300 700 ITNA 76KUC 01 350 30 RTNA 840DD 01 1 8350 120 AA 79R0S 03

360 30 ITNA 77CAH 01 1 8380 405 ITNA 83NDI 01 370 20 ITNA 78NAD 02 1 8400 ITNA 75KLE 01 370 20 ITNA 75NA0 02 1 8400 200 D TCGS 80AND 01 370 40 ITNA 76UEW 01 1 8400 200 ITNA 78LAU 02

380 40 D NAA 79STE 01 1 8400 200 ITNA 76RAG 01 380 40 ITNA 77R0W 04 1 8400 400 ITNA 750ND 01 380 40 ITNA 79GRE 01 1 8400 400 D NAA 740ND 01 390 40 ITNA 85FIL 01 1 8410 250 lENA 77R0W 04

400 AA 82GUP 02 1 8420 240 TCGS 79FAI 01 400 ITNA 75MIL 01 1 8440 11 ICPES 85HAR 01 410 30 ITNA 75RUC 01 1 8500 60 ITNA 75NAD 02

1632-10
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Fe (uq/g) cont. Gd (ufl/g)

8500 600 ITNA f ONnU n? 1

1 1.-2 AA QOf^i in ocuUP 02

8527 AA 1 OuU 1 ni 1

1 \.2 0.06 ICPES 0 1 PUI 1 U 1 8600 POL 7/M4I

1 1.43 0.05 TCGS 70C A T

f yrAX

8600 ITNA r OMCn ni 1

1 2.2 0.08 TCGS OUANU Ul 8630 266 EXRF R1lf TM ni 1 2.5 ITNA 7<sMT 1 ni 8690 410 PAA 7/ru* ni 1

1 3 34 WXRF A?y 1

1

mUl 8700 35 ITNA 05 1

1 3 0.9 ITNA niU 1 8700 200 ITNA 70RDF ni 1

1 3.1 0.2 RTNA OhUUU Ul 8700 400 PAA 7ArUA ni 1

1 3.6 0.4 ITNA 7nu An U£

8730 AA r OWtW ni 1 3.62 0.35 ITNA ONAD no

8800 ICPES oUNAU ni t

1 8800 200 ITNA TTMAr ni 1

1 Ge (uq/g)

8810 210 ICPES o 1 unu niU 11

1 8900 240 XRF ni 1 2 ITNA r r uLU niU 1 8900 300 ITNA 7AMAr ni 1

1 2.3 0.1 ICPES OHNAU no

9000 200 D NAA 70CTF r 1 C ni i

1 2.4 UU 7ftQ!M niU 1 9010 150 ITNA 1 2.7 0.22 OES f DWCM niU 1 9010 190 D ITNA n^ 1 2.9 0.2 EXRF f TU 1

M

niU 1 9030 ITNA 7SMr 1 ni 1

1 3 34 WXRF ni

9130 560 ITNA 70pnc n'^ 1

1 5 1 XRF 7QPPA niU 1 9200 4 AA 70PF

I

ni 1

1 14.9 FAA f jrKJL ni

9200 300 NAA ! OfIMN ni 1

1 70 5 ITNA 77CUP f OdnC ni

9200 700 ITNA AIUAU ni 1

1 9300 800 ITNA 75RUC 01 1 H (%) k

9300 800 ITNA ni 1

1 9800 1000 ITNA 76UEW 01 1 4.02 0.05 TCGS 79FAI 01 11100 ITNA 01 1 4.02 0.05 D TCGS 8QAND 01 11100 300 12 ITNA n? 1 4.28 0.03 CB 02

11300 500 12 ITNA n? 1 4.3

4.57

0.1 35 TCGS

CB

7QRI A

1 Tr Rft

04

01

Ga Cug/q>

H20-T (%)

4.5 ITNA f r uLU ni 1

4.5 0.5 RTNA r Jt\\j\^ ni 1

1 2.6 FD 02

4.8 0.2 lENA you f OnnnAM ni 1

1 5 1 ITNA 7ftMAr t OHML. ni 1

1 Hf (uq/q)

5.15 0.3 ITNA 7K0\ IP ni 1

5.3 0.5 ITNA f f LAH ni 1 0.72 0.071 ITNA f 7KUd

5.4 0.8 ITNA 7TCUC U 1 1 0.81 0.1 ITNA 7AI Al 1 r OLnU n?

5.5 0.7 ITNA O IWAN ni t U 1 1 0.83 0.06 lENA

5.8 34 WXRF ni 1 0.83 0.06 D lENA f rKLFM (XL

5.8 0.4 lENA f rKUW n7 1 0.83 0.06 D NAA 70CTP ( 7d 1 C 01

5.8 0.4 D NAA 70CTC TO 1 C ni 1 0.89 0.02 ITNA 02

5.8 0.4 5 lENA 7AQTF n^; 1

1 0.89 0.02 ITNA 02Wfc 5.8 0.5 ITNA O^r I L ni 1

1 0.91 0.11 ITNA 04

6.1 0.3 EXRF f yy 1 ft ni 1

1 0.91 0.15 ITNA 85FIL 01

6.1 0.6 5 lENA 76STE AC 1 05 1 0.92 0.05 ITNA 77CLJC niU 1 6.2 0.3 OES 76WEW 01 1 0.95 ITNA 75ICLE 01 7.7 1.4 ITNA 82SUZ 02 1 0.96 ITNA 78WEA

8 1 XRF 79PRA 01 1 0.96 0.05 ITNA 750ND

8.5 XRF 75KLE 01 1 0.96 0.06 ITNA 79GRE 01 9 2 NAA 76HAN 01 1

1632-11

1
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/g) cont. I (ug/g)

0.97 0.09 ITNA 79FRU 01 1 2.68 0.2 RTNA 77ROO n 1 01 0.97 0.1 ITNA f5Mt 01 1 2.78 0.38 ITNA OSHE ni01 1.00 0.07 ITNA roRAG U1 1 2.8 ITNA 7QI IC A n 1 Ul 1.02 0.03 ITNA f fnAt ni 1 01 1 2.8 0.4 ITNA 7COI If* ni01

1.1 ITNA OMIL ni 1 Ul 1 2.9 0.3 D NAA ni01

1.1 0.07 NAA 76HAN 01 1 2.9 0.3 ITNA 76STE 05

1.1 0.15 ITNA 75RUC 01 1 3 34 WXRF OOU 1 1 ni01

1.1 0.2 ITNA 77CAH 01 1 3.3 0.3 PAA 77WIL 01

1.1 0.4 ITNA 81 WAN 01 1 3.3 0.3 PAA /on IS ni01 1.15 0.12 ITNA 7^1 Id f 01 1 3.3 0.4 ITNA f rCAH ni01 1.4 0.09 9 ITNA odSUZ 3.3 0.5 ITNA 7*7UA C niUl 1.53 0.5 9 ITNA B^SUZ AO 1

1 3.7

4

0.5

1

lENA

ITNA

Q/ ^1 A OHuLA no0£

niUl (ng/q) 6.2 1.9 ITNA olWAN ni01 6.63 1.2 ITNA no02

70 5 CVAA O/ DAD Mc.

\ 88 5 CVAA TK^l C ijKLt U 1

1 In (ng/g)

100 PAA f hLHA U 1

1 100 PAA 7^r^u A ni 1 Ul 1 16.9 1.2 lENA 0^

100 PAA 1 1 JcR ni 1 01 1 16.9 1.7 5 lENA roSTE nc03

110 ITNA 78WEA ni t 01 1 17 1 D NAA rVSTE ni01 110 10 RTNA 84DEL 01 1 17.8 1 5 lENA roSTE ncOb

110 10 RTNA 740RV 01 1 30 20 ITNA 76RAG 01 110 10 RTNA 75RUC ni 1 01 1 40 10 ITNA 73SHE 01 110 16 RTNA / / ICO ni 1 U1 1 56 9 ITNA noU2

110 50 ITNA f y ICO

I f JcR ni 1 U1 1 70 ITNA niUl

111 10 FAA f r uLA 180 20 ITNA f rLAH niU 1 117 13 FAA ni 1 200 120 ITNA niU 1 120 CVAA 0£NAU ni 1 u 1 1 220 20 ITNA 7CDI IP niU 1 120 CVAA DiUAn O iNAU ni 1 Ul 1 230 20 PAA f hLHA niU 1 120 20 ITNA f VrKU ni 1 Ul 1 230 30 PAA 7APU A niUl 122 29 CVAA fiAni 111 ni 1 U 1 1 126 6 CVAA 7/ DAT ni 1 Ul 1 Ir (nq/g)

136 9 FAA Q^l l/^u no 1 \}i

\ 160 40 ITNA o<:SUZ no 1 \3c

\ 2.48 0.27 ITNA ni01 160 80 ITNA 76UEW 01 1 2.5 ITNA 78WEA 01 180 ITNA 77GLU 01 1 3.53 0.52 RTNA ( f NAD no02

230 20 - ITNA 78NAD 02 1 230 20 ITNA 75NAD 02 1 IC (uq/q)

230 50 ITNA 76BL0 01 1 510 170 ITNA 75RIC ni 1 01 1 2410 70 XRF niUl

950 90 ITNA 77cun ni 1 01 1 2500

2500 200 11

ICPES

ICPES

oUNAU

QCUAD

Ul

niU 1

) (nq/g) 2500 200 ICPES o/ u An o*fNAU niU 1 2570 4 AA / TKt 1 ni

240 30 lENA 77R0W 03 1 2600 11 ICPES 85HAR 01 240 30 lENA 76STE 05 1 2600 200 ITNA 76KUC 01 240 30 D NAA 79STE 01 1 2650 190 ITNA 76BL0 01 250 FAA 82GUP 02 1 2660 20 ITNA 75RIC 01 260 30 ITNA 840DD 01 1 2700 ICPES 80NAD 01 270 40 RTNA 84CX)D 01 1 2700 ICPES 80NAD 01

1632-12
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

K (ug/q) cont

2700 100 PAA 76CHA 01 2700 200 ITNA 79FRU 01 2700 200 ITNA 76RAG 01 2700 300 NAA 76HAN 01 2750 100 D TCGS 80AND 01 2750 100 TCGS 79FAI 01 2780 230 ITNA 75NAD 02

2800 ITNA 78UEA 01 2800 100 ITNA 73ABE 01 2800 200 ITNA 77MAE 01 2800 200 ITNA 79GRE 01 2800 200 ITNA 78NAD 02

2800 200 ITNA 78LAU 02

2800 300 ITNA 750ND 01 2800 300 ITNA 77CAH 01 2800 500 ITNA 76UEW 01 2840 80 GAMHA 73ABE 01 2900 ITNA 75MIL 01 2900 ITNA 75KLE 01 2900 ICPES 80NAD 01 2900 200 ITNA 75RUC 01 2930 120 ITNA 83NDI 01 2980 200 ITNA 76STE 05

2980 240 ITNA 77R0W 03

3000 75 ICPES 81CHU 01 3000 200 D NAA 79STE 01 3000 200 ITNA 78MAC 01 3040 230 ITNA 85FIL 01 3100 500 ITNA 81UAN 01 3100 600 OES 76UEU 01 3300 ITNA 77GLU 01 3500 360 ITNA 73SHE 01 4000 200 ITNA 82SUZ 02

La (uq/q)

6 0.17 OES 76UEW 01 7.89 0.15 ITNA 75NAD 02

7.9 0.2 ITNA 78NAD 02

8.3 0.2 ITNA 78MAC 01

9.1 0.4 ITNA 76BL0 01 9.3 0.3 ICPES 81CHU 01 9.3 0.5 ITNA 78LAU 02

9.5 0.2 ITNA 76RAG 01 9.76 0.45 NAA 76HAN 01

10 34 UXRF 82MIL 01

10 FAA 82GUP 02

10.3 0.5 ITNA 77R0W 03

10.3 0.5 D ITNA 77R0W 04

10.3 0.5 D NAA 79STE 01 10.3 1.1 ITNA 76STE 05

Cone Uncer Com Method Reference

La (uq/g) cont.

10.5

10.5

10.5

10.5

10.6

10.7

10.7

10.7

10.7

10.8

10.8

11

11

11,

11,

11,

11,

11,

11.4

11.4

11.4

11.5

12.7

Li (ug/g)

24

25

28.7

Lu (ng/g)

100

100

109

109

109

120

120

130

130

130

140

140

140

140

140

150

150

210

416

ITNA 75KLE 01 0.2 ITNA 79FRU 01 0.5 ITNA 73ABE 01 0.9 ITNA 81 WAN 01 0.4 ITNA 77CAH 01 ITNA 78WEA 01 0.3 ITNA 77MAE 01 0.4 ITNA 82SUZ 02

1.2 ITNA 750ND 01 0.3 RTNA 840DD 01 0.8 lENA 77R0W 04

OES 82GUP 02

1 ITNA 85FIL 01 0.3 ITNA 83NDI 01 ITNA 75MIL 01 0.4 ITNA 75RUC 01 3.3 ITNA 73SHE 01 0.3 11 ICPES 85HAR 01 0.4 ITNA 84000 01 0.5 lENA 77R0W 03

0.5 lENA 76STE 05

0.7 ITNA 79GRE 01

11 ICPES 85HAR

1.1

0.6

11

11

11

5

10

520

30

10

20

20

30

70

10

20

20

17

OES 76WEW 01 AA 76WEW 01 ICPES 81CHU 01

ITNA 75MIL 01 FAA 82GUP 02 ITNA 77R0W 04

NAA 79STE 01 ITNA 77R0W 03 ITNA 75NAD 02

ITNA 78NAD 02 ITNA 77MAE 01 ITNA 84OD0 01 ITNA 77CAH 01 ITNA 750ND 01 ITNA 78LAU 02

NAA 76HAN 01 RTNA 8400D 01

ITNA 81 WAN 01

ITNA 75RUC 01

ITNA 76WEU *

ITNA 82SUZ 02

ITNA 73SHE 01

1632-13

V
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Cora Method Reference

Hg (ug/g)

980 250 ITNA 73SHE 01

1000 100 ICPES 84NAD 01 1100 ITNA 77GLU 01 1100 300 ITNA 77MAE 01 1150 40 11 ICPES 85HAR 01 1190 11 ICPES 85HAR 01 1200 ICPES 80NAD 01 1200 ICPES 80NAD 01 1340 270 ITNA 82SUZ 02

1370 40 ICPES 81CHU 01 1400 ICPES 80NAD 01 1500 300 ITNA 75NAD 02

1500 300 ITNA 78NAD 02

1600 ICPES 80NAD 01 1600 150 PAA 74CHA 01 1600 200 PAA 76CHA 01 1600 300 OES 76UEU 01 1700 200 ITNA 79GRE 01

1700 300 ITNA 76STE 05

1700 300 D NAA 79STE 01 1700 300 ITNA 77R0W 03

1900 400 NAA 76HAN 01 2000 400 ITNA 76UEU 01 2000 500 ITNA 750ND 01 2300 400 ITNA 81 MAN 01 2300 700 ITNA 73ABE 01 2480 ITNA 75KLE 01 2500 800 ITNA 76RAG 01 4000 2000 ITNA 78LAU 02

8200 2000 ITNA 78MAC 01

in (ug/Q)

27.5 2.4 ITNA 82SUZ 02

36 1.8 OES 76WEU 01 36.8 FAA 78GUI 01 37 EXRF 82KEE 01 37 2 EXRF 81KIN 01 37 4

- XRF 79PRA 01 38 4 AA 79REI 01 38 2.6 ITNA 73SHE 01 38 8 35 ITNA 81GLA 03

38.3 0.8 11 ICPES 85HAR 01 38.5 AA 78GUI 01 39 34 UXRF 82MIL 01 39 ITNA 84CLE 01 39 ITNA 77GLU 01 39 2 ICPES 84NAD 01 39 3 EXRF 79GIA 01 39.5 0.7 ITNA 76RAG 01 40 AA 76UEW 01

Cone Uncer Com Method Reference

Mn (ug/g) cont.

40 4 ITNA 76UEU 01 40 7 ITNA 78NA0 02

40.3 6.9 ITNA 75MAD 02

41 ITNA 78WEA 01

41 1 ITNA 75RIC 01

41 2 NAA 76HAN 01

41 4 D NAA 79STE 01

41 6 ITNA 80BUA 01

41 6 ITNA 73ABE 01 41.1 3.6 ITNA 76STE 05

41.1 3.6 ITNA 77R0W 03

41.2 11 ICPES 85HAR 01 41.7 0.5 AA 79R0S 03

42 ICPES 80NAD 01 42 1 ITNA 79GRE 01 42 6 ITNA 79FRU 01 42.5 5.8 ITNA 81WAN 01 42.8 1.9 ITNA 83NDI 01 42.8 2.4 ITNA 77CAH 01 43 1 ITNA 78MAC 01 43 3 PAA 76CHA 01 43 4 D NAA 740ND 01 43 4 ITNA 750ND 01 *3 6 ITNA 76BL0 01 43.5 2.4 TCGS 79FAI 01 43.5 2.4 D TCGS 80AND 01 43.7 1.8 ITNA 75RUC 01 44 0.9 11 AA 82LIN 03

44 2 ITNA 78LAU 02

44.5 0.9 ITNA 77MAE 01 44.6 0.4 11 AA 82LIN 03

45 ICPES 80NAD 01 45 1.4 ICPES 81CHU 01 45 3 ITNA 76iajc 01 46 ITNA 75MIL 01 46 3 ITNA 75KLE 01 47.1 4.1 PAA 74CHA 01

(ug/g)

0.2 0.02 PAA 74CHA 01 0.2 0.04 PAA 76CHA 01 0.3 0.1 PAA 80SEG 01 0.3 0.1 6 PAA 82SEG 01 0.3 0.1 6 PAA 82SEG 01 0.41 0.1 ITNA 82SUZ 02

3.08 0.12 lENA 77R0W 03

3.08 0.12 D lENA 77R0W 04

3.1 0.1 D NAA 79STE 01 3.14 0.28 RTNA 78NAD 01 3.2 0.4 ITNA 77CAH 01

1632-14
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Mo (uq/g) cont.

1

1 Na (ug/g) eont.

3.3 ICPES 80NAD

1 01 1 406 7 ITNA 83NDI 01 3.4 ITNA 75KLE 01 1 409 ICPES 80NAD 01 3.6 0.16 OES 76WEW 01 1 410 ITNA 75MIL 01 A 34 WXRF 82MIL 01 1 414 ITNA 78WEA 01 4.7 ICPES 80NAD 01 1 414 20 ITNA 750ND 01

5 ITNA 78WEA 01 1 415 42 ITNA 76WEW 01 5 ITNA 77GLU 01 1

1

420

420

20

30

ITNA

ITNA

79FRU 01 73ABE 01

N (%) 1 439

480

42

4

ICPES

AA

84NAD 01 79REI 01 1.01 IC 83NAD 01 1 840 30 ITNA 82SUZ 02

1.2 0.2 35 TCGS 79GLA 04 1 1200 240 OES 76WEW 01 1.3 0,02 CB 80SCH 02 1 1.3 0.2 D TCGS 80AND 01 1 Nb (ug/g)

1.3 0.2 TCGS 79FAI 01 ! 1.98 CB 79PRA 01 i

1 5

< 15

54

OES

WXRF

76WEW 01 82MIL 01 Na (ug/g) 1

1 Nd (ug/g)

325 6 ITNA 75RIC 01 j 330 11 ICPES 85HAR 01 ! 6.4 1.5 ITNA 73SHE 01 330 20 11 ICPES 85HAR 01 1 7 34 WXRF 82MIL 01 335 ICPES 80NAD 01 1 8 AA 82GUP 0^

340 10 ITNA 78LAU 02 1 8.7 1 D NAA 79STE 01 347 32 ITNA 75NAD 02 1 8.7 1 D ITNA 77R0W 04

350 20 PAA 76CHA 01 1 8.7 1 ITNA 77R0W 03

350 30 ITNA 78NAD 02 j 9.5 1.9 ICPES 81CHU 01

351 30 PAA 74CHA 01 j 9.7 0.4 ITNA 840DD 01 352 34 ITNA 77CAH 01 1 9.9 0.6 RTNA 840DD 01 353 21 ITNA 76KUC 01 j 10.7 ITNA 75MIL 01 360 10 ITNA 79GRE 01 j 11.3 2 TCGS 79FAI 01 360 20 NAA 76HAN 01 1 11.3 2 D TCGS 80AND 01 368 9 ITNA 77MAE 01 j 16.9 1.4 12 ITNA 82SUZ 02

370 ICPES 80NAD 01 1 17.8 3.7 12 ITNA 82SUZ 02

370 33 ITNA 73SHE 01 1 380 ICPES 80NAD 01 i Ni (ug/g)

380 3 ITNA 78MAC 01 j 380 12 ITNA 76RAG 01 1 10 EXRF 82KEE 01 380 25 ITNA 76STE 05 j 11 lENA 77R0W 03

380 25 ITNA 77R0W 03 1 11.5 11 ICPES 85HAR 01 380 25 D NAA 79STE 01 1 12 0.7 ITNA 78NAD 02

383 14 ITNA 75RUC 01 1 12.1 0.7 ITNA 75NAD 02

387 42 ITNA 81 WAN 01^ 1 12.5 0.1 11 AA 82LIN 03

390 ITNA 75KLE 01 1 13 3 9 ITNA 78LAU 02

390 ITNA 77GLU 01 1 13.5 1.2 PAA 74CHA 01 390 34 WXRF 82MIL 01 1 13.8 0.4 11 ICPES 85HAR 01

395 ITNA 86GAU 01 1 14 4 AA 79REI 01 400 ITNA 84CLE 01 j 14 1 PAA 80SEG or 400 7 ICPES 81CHU 01 ! 14 1 6 PAA 82SEG of

400 30 ITNA 76BL0 01 j 14 2 6 PAA 82SEG 01 400 900 R ITNA 81GLA 03 1 14 2 XRF 79FRU 01

1632-15
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRN 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

<ug/g) cont P (uq/g)

14 2 PAA 76CHA A 4 1 01 1 71 AA 76UEU 01

14.3 AA 78GUI 01 1 92 ICPES 80NAD 01 14.5 XRF 75KLE 01 1 104 ICPES 80NAD 01 14.5 0.6 11 AA 82LIN 03 1 117 4 11 ICPES 85HAR 01 14.5 1.2 EXRF 79GIA 01 1 120 W 77GLU 01 14.7 0.6 6 IDHS 74M00 A 4 1 01 1 121 11 ICPES 85HAR 01 14.7 0.6 6 IDMS 74M00 A -I t 01 1 137 14 ICPES 84NAD 01 14.8 POL 74MAI A 4 1 01 1 138 34 WXRF 82MIL 01 14.8 0.7 6 IDMS 74MOO A 4 1 01 1 150 9 ICPES 81CHU 01

15 AA 76WEW 01 1 156 ICPES 81NAD 01

15 34 WXRF 82MI

L

01 1 250 COLOR 80NAD 01

15 1.1 OES 76WEW 01 1 270 COLOR 80NAD 01

15 3 SSMS 77D0N A 4 1 01 [ 1200 100 XRF 79PRA 01 15.2 0.5 ICPES 81CHU 01 1 15.5 1.1 8 SSMS 80KOP A 4 1 01 1 Pb (ug/Q)

16 D NAA 79STE A 4 1 01 1 12 120 R OES 76UEU 01 16 ICPES 80NAD A 4 1 01 1 13.6 6.5 EXRF 79GIA 01 16 2 ICPES 84NAD A 4 1 01 1 15 ICPES SONAD 01 16 2 ITNA 79FRU A 4 1 01 1 19.1 ICPES 81 NAD 01 16 4 ITNA 73ABE A 4 1 01 1 20 ICPES 80NAD 01 16 5 ITNA 77CAH 01 1 20 2 XRF 79PRA 01 16.4 lENA 77R0W A / 1 04 1 23 W 77GLU 01

17.1 FAA 78GUI A4 1 01 1 23 0.9 EXRF 73SPA 01 17.5 1 EXRF SUKIN A4 1 01 1 24 4 AA 79REI 01 18 4 ITNA 750ND A1 1 01 1 24 4 11 ICPES 85HAR 01 18 4 D NAA f 40ND 01 1 25.5 4.2 11 AA 82LIN 03

18 5 NAA /onAN 01 1 26 6 FAA 76BL0 01 18.4 2.1 ITNA *7Cdi in

f DRUG AI 1 01 1 26.1 AA 78GUI 01 18.9 0.8 12 ITNA odSUZ AO 1 \JC.

\ 27.9 2.5 8 SSMS 80KOP 01 19 ICPES 80NAD Ai 1 01 1 28 1 6 PAA 82SEG 01 20 ITNA I r GLU AI 1 01 1 28 2 PAA 80SEG 01 20 11 ITNA o5FIL A 4 1 01 1 28 2 6 PAA 82SEG 01 20.4 1 12 ITNA 82SUZ A*^ 1 02 1 28 3.6 SSMS 77PAU 01 83 7 XRF 79PRA A 4 1 01 1 28 4 IDMS 78CAR 02

28 5 FAA 75BL0 02

(%) 28.4 POL 74MAI 01 28.5 1.5 ICPES 81CHU 01 10.08 CALC 79PRA A 4 1 01 1 28.6 FAA 78GUI 01 15.05 o.ir 34 14NAA 80KHA AI 1 02 1 29 0.5 AA 73TAL 01 29 2 PAA 77JER 01 (ug/g) 29.4 IDMS 75KLE 01 30 AA 76UEU 01 < 1 RTNA 77NAD 30.8 FAA 75POL 01

31 3 EXRF 81KIN 01 32 34 WXRF 82MIL 01 32 2 PAA 76CHA 01 32 2 PAA 77JER 01 32.1 1.8 PAA 74CHA 01 33 2 AA 79R0S 03

33 3 SSMS 77D0N 01 33.8 0.1 11 AA 82LIN 03

f 36 11 ICPES 85HAR 01 1632-16
TABLE 1632-2: INDIVIDUAL DATA FOR MBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Referenee

Pd fna/a)

1

1 —

RTMA 77NAD

1 02 1 AP\r 75KLE 01

1 ITMA 75MIL 01 Dp 1 1 in In

\

1 CH mi 1 ITUA 79R0S 03

1 2& 1 1 b ITUA i 1 nn 82SUZ 02

2 L FAA 82GUP 02 1 CAnr 73SPA 01 < 15 L OES 76UEU 01 1 30 1 12 ITNA 82SUZ 02

2 34 UXRF 82HIL 01 1 3.6 0.4 12 ITNA 82SUZ 02 1 Rh (ug/g)

4.6 0.5 12 ITNA 82SUZ 02 1 4.9 0.5 RTNA 840DD 01 1 OES WbW 76UEU 01

r\ ing/g;

1

1

1

PiKu1 (^ng/g; nn i n\

< 15000 L OES 76UEU 01 1 < 5000 L OES 76UEW 01 1S6 1 WW 2 3 RTNA 77NAD 01 1 18 1 PTMA K 1 nn 77NAD 02

270 20 RTNA 77NAD 02 1

1 S 1%^

1

1 0.17 ICPES 80NA0 01 10 3 ITNA 81 WAN 01 1 0.17 CB 80NAD 01

11 1 XRF 79PRA 01 1 0.9 CB 80NAO 01

15 35 ITNA 81GLA 03 1 0.9 ICPES 80NA0 01 16.3 3.7 ITNA 75NAD 02 1 1 .22 IC 83NAD 01 16 3 3.7 ITNA 78NAD 02 1 1 25 XRF 77GLU 01 181 U 34 UXRF 82MIL 01 j 1 29 0 03 TCGS 80AND 01 18 1 XRF 79FRU 01 1 1 29 0 03 TCGS 79FAI 01 18.3 1 .1 lENA 77R0W 04 1 1.3 0.02 IC 85GEN 01 18.3 1 .6 lENA 77R0W 03 1 1 .32 XRF 82NAD 01 18.3 1 .6 D NAA 79STE 01 1 1 .32 XRF 81 NAD 01

19 1.5 ITNA 76RAG 01 1 1 32 0 01 CB 86GAU 01

19 1 .9 ITNA 73SHE 01 1 1 32 0 03 CB 85GLA 03

19 2 ITNA 79FRU 01 1 1 32 0 07 TCGS 77JUR 01

19 2 ITNA 73ABE 01 j 1 34 0 08 CB 84GLA 11

19 6 ITNA 76WEW 01 1 1.52 0.05 XRF 79PRA 01 19.4 2.3 ITNA 77R0W 04 1 1 .99 CB 77LAD 01 19.5 IT MA 75KLE 01 1 2.02 TITR 77LAD 01 20 2 PAA 76CHA 01 1 20 2 PAA 750ND 01 1 Sb fua/a)

20 2 ITNA 79GRE 01 1 20 2 9 ITNA 78LAU 02 1 0 61 0 05 ITNA 82SUZ 02

20 4 78LAU 02 1 18 0 9 FAA 77ARU 01 20 1 0 6 79GIA 01 1 2 2 ITNA 75MIL 01

21 78WEA 01 1 2 3 5 8 R* COLOR 77ARU 01

21 7 750ND 01 j 2b • 6W 2b ITNA 77ARU 01 22 2 9 76WEW 01 1 2 6 3 6 ITNA 85FIL 01 22.5 0 7 ITMA 77MAE 01 1 2bar7 5 ITNA 77R0U 04

22.5 3Jot7 ITMA i 1 nn 75RUC 01 1 2.8 5 lENA 77R0W 04

22.8 4.8 ITNA 77CAH 01 1 2.8 0.7 ITNA 81 WAN 01

23 3 NAA 76HAN 01 1

. 3.0 34 UXRF 82MIL 01

23 4 ITNA 85FIL 01 1 3.0 5 ITNA 77R0W 04

23 7 ITNA 76KUC 01 1 3.0 lENA 77R0W 03

1632-17
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

Sb (ug/q) cent.

3.0 RTNA 75RUC 01 3.0 D NAA 79STE 01 3.0 UNA 77GLU 01 3.06 1.4 ITNA 75NAD 02

3.09 0.26 PAA 74CHA 01 3.1 1.4 ITNA 78NAD 02

3.2 5 lENA 77R0W 04

3.2 35 ITNA 81GLA 03

3.4 0.1 ITNA 76RAG 01 3.4 0.8 ITNA 75RUC 01 3.6 0.8 ITNA 77CAH 01 3.6 1.2 ITNA 77MAE 01 3.62 FAA 75POL 01 3.7 0.3 ITNA 79FRU 01 3.7 2 ITNA 73ABE 01 3.8 ITNA 84CLE 01 3.8 0.2 ITNA 78MAC 01 3.8 0.4 NAA 76HAN 01 3.82 0.1 ITNA 78LAU 02

3.9 ITNA 78UEA 01 3.9 0.24 ITNA 77JER 01 3.9 0.3 PAA 76CHA 01 3.9 0.3 PAA 77JER 01 3.9 1.3 ITNA 750ND 01 4.1 1.2 ITNA 76WEW 01 4.3 0.3 ITNA 79GRE 01 4.4 0.3 FAA 78HAY 01 4.45 ITNA 75KLE 01 6.4 1.6 ITNA 73SHE 01

(ug/g)

3.4 0.3 ITNA 77CAH 01 3.4 0.3 ITNA 73ABE 01 3.47 ITNA 84GLA 11 3.5 0.08 ITNA 75NAD 02

3.5 0.1 ITNA 78NAD 02

3.58 0.35 PAA 74CHA 01 3.6 0.08

- OES 76WEW 01 3.6 0.3 ITNA 83NDI 01 3.6 0.3 PAA 76CHA 01 3.68 0.08 ITNA 76RAG 01 3.69 0.05 ITNA 78LAU 02

3.7 ITNA 78WEA 01 3.7 0.1 ITNA 75RIC 01 3.7 0.3 ITNA 750ND 01 3.75 0.24 ITNA 79R0S 03

3.8 11 ICPES 85HAR 01 3.8 0.05 D NAA 79STE 01 3.8 0.05 ITNA 77R0W 03

3.8 0.05 D ITNA 77R0W 04

1632-

Conc Uncer Com Method Reference

Sc (ug/g) cont.

3.8 0.1 11 ICPES 85HAR 01 3.8 0.4 ITNA 76UEU 01 3.81 0.47 ITNA 75RUC 01 3.88 0.15 NAA 76HAN 01 3.9 0.2 ITNA 76KUC 01 3.95 0.06 lENA 77R0W 04

3.98 0.04 ITNA 78MAC 01 4 0.2 ITNA 79GRE 01 4.1 34 WXRF 82MIL 01 4.1 ITNA 75MIL 01 4.1 0.2 ITNA 81UAN 01 4.1 0.4 ITNA 85FIL 01 4.2 0.1 ITNA 77MAE 01 4.5 ITNA 75KLE 01 5.4 0.1 ITNA 82SUZ 02

(ug/g)

1.1 0.08 CPXRF 80KIR 01

2 HAA 74BYR 02

2.3 0.2 9 ITNA 82SUZ 02

2.4 0.1 ITNA 78NAD 02

2.44 0.08 ITNA 75NAD 02

2.5 0.2 ITNA 80WAN 01 2.51 0.13 8 SSMS 80KOP 01 2.6 0.1 9 ITNA 82SUZ 02

2.6 0.16 FAA 77ARU 01 2.6 0.3 9 ITNA 80WAN 01 2.7 0.2 RTNA 740RV 01 2.8 ITNA 77GLU 01 2.8 0.11 RTNA 75RUC 01 2.86 0.13 DOPES 81 CAR 02

2.86 0.13 GCHES 75KLE 01 2.86 0.13 GCMES 74TAL 02

2.9 0.1 ICPES 80HAA 01 2.9 0.2 ITNA 79GRE 01 2.9 0.2 XRF 77ARU 01 2.9 0.4 ITNA 76RAG 01 2.99 0.07 SSMS 77PAU 01 3 34 WXRF 82MIL 01 3.0 0.3 PAA 76CHA 01 3.0 0.3 H OES 80CLA 01 3.0 0.3 D NAA 79STE 01 3.0 0.3 D lENA 77R0W 04

3.0 0.3 lENA 77R0W 03

3.0 0.4 RTNA 80KNA 01 3.0 0.4 6 PAA 82SEG 01 3 1 6 PAA 82SEG 01 3 1 PAA 80SEG 01 3.03 0.28 PAA 74CHA 01 3.05 ITNA 75KLE 01
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

^onc Unccr Com netnoa Reference | Cone uncer Com Hetnoa KeTerence

(ug/g) cont! •

1

1 dn /im/n\

\> m HO noV 76AND

1 01 1 fTMA t 1 nn

3 1 T TMA 78WEA 01 1 0V a 2^

3 1 0.2 EXRF 79GIA 01 1 1 38 0.09 ITNA 1 1 nn 77R0IJ 04

1 0 3 TTMA 85FIL 01 1 1 IkPk 1 • JO 0 1 IPMA I cnn 7ASTF r OO 1 C OSU

D 1 > 1 n A A(\ r 79FRU 01 1 1\ aHL PAA r nn

O 1 • 1 nU s Ao 7 TMA 78MAC 01 1 1 L nUa 11 T1 PUA CNM f r KUW U3

1 1il AO T TUA 76WEU 01 1 1\ aHL nU 1 . 1 T

X TMA 1 Nn 1 OTIMU U 1

U •3 t1 TUA 1 Nn 75RIC 01 11 • H 1 nU a HAUO nu MAA Nn#\ 70CTP ni

T TUA 76BL0 01 1 1I.HIL\ n fiA TPMA 1 CNn 1 f KUW UH

Qy

T TUA 1 1 NA 78LAU 02 1

1 . 33 u a yjc Tr^^C (yrni ul U B 3

T TUA 79FRU 01 1

1 c 33 n HP nu TPnC 1 Uuo AOAun OUnnU niU

n L T

1 TUA 1 Nn 73ABE 01 1 11 a 33 nU a n7Uf MAA NnM 7AUAU f OnnN niU

U a O f1 TMA 1 Nn 78LAU 02 1 1i aOA TTMA 7SMTI ni

1

f TMA 1 Nn 750ND 01 1 11 . Ao n 5 I1 TMA 1 Nn 77rAH r 1 Unn niU

n MAA NMn 740ND 01 1 11 aOOAA nV . 1Ato TTMA 1 1 nn TSMAn n?

3 • 7 U • 3 Ti TMA 1 Nn 77MAE 01 1 11 a 7f TTMA I 1 Nn 7AUPA r OWCn niU

3 a O T1 TMA 1 nn 75RUC 01 1 11 a 7f u c TTMA I 1 nn 7AMAn f onnv n?u& 3.7 ITNA 84CLE 01 1 1.7 0.2 ITNA 750ND 01 7 n 7 I

1 TMA 1 nM 77R0W 04 1 1 7 W.J TTMA 1 1 nn 3.8 0.51 ITNA 73SHE 01 1 1.7 0.3 ITNA 840DD 01 X ft n 7 T TUA 77CAH 01 1 1 7? n nft I1 TMA 1 nn 76RAG 01

I TMA 81 WAN 01 1 11 . 74f H 0 02 ITNA 78LAIJ 02

U 7 COLOR 74BYR 02 1 1 .8 0.07 ITNA 85FIL 01

5 5 0 5 EXRF 73SPA 01 1 1 .8 0.1 RTNA 840DD 01 Aw 1 AR r 79PRA 01 1

1

1 .8

1 83

0.1

0w . 08vO

ITNA

I1 TMA 1 nn

75RUC 01 83NDI ojnV 1 01VI

1

1

1 9

11 a 93TJ 0 14

ITNA 1 1 nn

1ITNA 1 nn

79GRE 01 77MAE 01

C . 1 U a He. 76WEW 01 1 2 9 0U a 2b ITNA 82SUZ 02

£ . o

LH AA 79REI 01 1 ? Aft 84NAD 01 1 oil vuy/yy

U a UO 79FAI 01 1 nu > HAuo n 80AND 01 1 10 p 76WEW 01 n L PAA rnn 76CHA 01 1 H 0 2 ICPES 80HAA 01

n <7 U . 3 r I

1 TMA 1 nn 83NDI 01 1 3 34JH nAi\ r 82HIL 01

3.14 ICPES 80NAD 01 1 8 ICPES 80NAD 01

3 • 171 f 80NAD 01 1 0y a 7f 80NAD 01 3.19 ICPES 80NAD 01 1 10 ITNA 77GLU 01 3.19 0.1 XRF 79PRA 01 1 10 1 PAA 76CHA 01 3.2 AA 76WEW 01 1 10 1 PAA 80SEG 01

3.21 ICPES 80NAD 01 1 10 1 6 PAA 82SEG 01

3.5 0.8 UNAA 76BL0 01 1 10a2 1 PAA 74CHA 01 3.92 W 77GLU 01 1 11 125

0.4

20

6 PAA

ITNA

82SEG 01

73SHE 01

1632-19
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference

Sr (ug/g)

1.02 0.05 ITNA 75NAD 02

1.33 0.1 PAA 74CHA 01

91 9 12 ITNA 82SUZ 02

93 7 12 ITNA 82SUZ 02

93 9.2 ITNA 73SHE 01 99 4 AA 79REI 01 112 26 ITNA 76RAG 01 120 20 NAA 76HAN 01 123 ITNA 75KLE 01 125 26 ITNA 78NAD 02

128 3 XRF 79PRA 01 129 ITNA 75MIL 01

131 23 ITNA 76STE 05

136 2 11 ICPES 85HAR 01 140 2.8 ICPES 81CHU 01 140 15 PAA 76CHA 01 140 40 ITNA 78LAU 02

142 11 ICPES 85HAR 01 144 XRF 75KLE 01 145 9 ITNA 75RUC 01 150 20 XRF 79FRU 01

151 34 WXRF 82MIL 01

151 4 EXRF 79GIA 01 155 6 ITNA 77CAH 01 155 15 EXRF 73SPA 01 159 14 lENA 77R0W 04

160 10 lENA 77R0W 03

161 9 D NAA 79STE 01

161 9 5 lENA 76STE 05

161 16 ITNA 750ND 01 164 14 ITNA 77MAE 01 164 25 ITNA 81 WAN 01 165 21 5 lENA 76STE 05

170 10 ITNA 73ABE 01 170 17 ITNA 76WEU 01 170 20 ITNA 78MAC 01 170 20 9 ITNA 78LAU 02

170 20 ITNA 79FRU 01 171 22 ITNA 85FIL 01 190 ITNA 77R0W 04

280 56 OES 76WEU 01

Cone Uneer Com Method Referenee

Ta (ng/g)

170 ITNA 75KLE 01 210 35 ITNA 81GLA 03

210 20 ITNA 77CAH 01 210 20 ITNA 75RUC 01 230 20 ITNA 76RAG 01 240 ITNA 78WEA 01 240 10 ITNA 75NAD 02

240 10 ITNA 78NAD 02

240 25 ITNA 85FIL 01 240 40 ITNA 750ND 01 250 10 ITNA 77MAE 01 250 30 NAA 76HAN 01 270 20 ITNA 79R0S 03

273 6 lENA 77R0W 03

273 6 D NAA 79STE 01 273 9 D lENA 77R0W 04

290 50 ITNA 78LAU 02

300 ITNA 77R0W 04

300 ITNA 75MIL 01 350 20 ITNA 82SUZ 02

360 28 ITNA 73SHE 01 460 50 ITNA 73ABE 01

rb (ng/g)

30 ITNA 73SHE 01 200 20 ITNA 76RAG 01 200 40 ITNA 76UEU 01 230 10 ITNA 78LAU 02

230 50 ITNA 750ND 01 230 60 ITNA 73ABE 01 260 20 ITNA 82SUZ 02

270 10 D NAA 79STE 01 274 12 lENA 77R0W 03

274 12 D lENA 77R0W 04

290 80 ITNA 85FIL 01 310 40 ITNA 840DD 01 340 20 RTNA &40DD 01 400 20 ITNA 78NAD 02

400 20 ITNA 75NAD 02

500 ITNA 75MIL 01

re (ng/g)

< 600 L UXRF 82MIL 01

< 690 L ITNA 82SUZ 02

< 1000 L PAA 76CHA 01 500 FAA 77GLU 01 600 40 35 RTNA 75GLA 01 1020 PAA 74CHA 01

1632-20
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone

Th (ug/g)

Uncer Com Method Reference

1.28 0.06 ITNA 75NAD 02

1.3 0.1 ITNA 78NAD 02

2.4 0.2 ITNA 76BL0 01 2.7 0.7 EXRF 79GIA 01 2.87 0.09 ITNA 77R0W 04

2.87 0.24 ITNA 79R0S 03

2.9 0.1 ITNA 76RAG 01 2.9 0.2 ITNA 85FIL 01 3 34 WXRF 82MIL 01 3 ITNA 75KLE 01 3 0.2 ITNA 78LAU 02

3.1 0.2 ITNA 750ND 01 3.1 0.2 ITNA 73SHE 01 3.12 0.1 D lENA 77R0W 04

3.12 0.1 lENA 77R0W 03

3.12 0.1 D NAA 79STE 01 3.2 35 ITNA 81GLA 03

3.2 ITNA 75MIL 01 3.2 0.1 ITNA 77MAE 01 3.2 0.2 ITNA 79GRE 01 3.2 0.3 ITNA 76WEW 01 3.2 0.5 NAA 76HAN 01 3.3 0.6 ITNA 81WAN 01

3.4 0.3 ITNA 79FRU 01 3.4 0.6 ITNA 73ABE 01 3.45 0.1 GAMMA 73ABE 01 3.45 0.1 GAMMA 750ND 01 3.5 0.6 ITNA 77CAH 01 3.65 0.49 ITNA 75RUC 01 4.1 0.1 12 ITNA 82SUZ 02

4.6 0.1 12 ITNA 82SUZ 02

4.7 DNA 75MIL 01

(ug/g)

425 25 ICPES 84NAD 01 680 EXRF 82KEE 01 690 4 AA 79REI 01 790 POL 74MAI 01 800 AA 76UEU 01 800 ITNA 78UEA 01 810 20 11 ICPES 85HAR 01 839 172 ITNA 75NAD 02

840 200 ITNA 78NAD 02

860 11 ICPES 85HAR 01 885 150 ITNA 76BL0 01 890 35 D TCGS 80AND 01 890 35 TCGS 79FA1 01 890 50 D NAA 79STE 01 890 50 ITNA 76STE 05

890 50 ITNA 77R0W 03

Cone Uncer Com Method Reference

Ti (ug/g) cont.

890

900

900

920

930

930

930

946

951

960

960

972

973

980

995

1000

1028

1060

1075

1100

1100

1100

1100

1100

1160

1200

1300

1312

1550

Tl (ng/g)

500

500

512

520

590

600

600

610

Tm (ng/g)

110

300

300

300

300

200 PAA 750ND 01 100 PAA 76CHA 01 180 OES 76WEU 01

50 NAA 76HAN 01

34 WXRF 82MIL 01 ICPES 80NAD 01 ITNA 75KLE 01 24 ICPES 81CHU 01

53 EXRF 79GIA 01 ICPES 80NAD 01

ICPES 80NAD 01 ICPES 80NAD 01 50 PAA 74CHA 01 60 ITNA 79GRE 01 100 ITNA 78MAC 01 260 ITNA 76RAG 01 30 AA 79R0S 03

35 NAA 81GLA 03

100 ITNA 750ND 01 ITNA 77GLU 01

100 ITNA 81UAN 01 110 ITNA 76WEW 01 200 ITNA 79FRU 01 200 ITNA 73ABE 01 50 XRF 79PRA 01 200 ITNA 78LAU 02

200 XRF 79FRU 01 150 ITNA 73SHE 01 130 ITNA 82SUZ 02

inn PAA rnn U 1 100 6 PAA 82SEG 01 60 PAA 74CHA 01 60 PAA 76CHA 01 60 SSMS 77PAU 01 100 6 PAA 82SEG 01 200 SSMS 77D0N 01 37 8 SSMS 80KOP 01

FAA 82GUP 02 ITNA 75MIL 01 ITNA 77GLU 01 20 RTNA 840DD 01 40 ITNA 840DD 01

1632-21
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

U (ug/q) V (ua/fl) cont.

0.98 0.078 ITNA 73SHE 01 1 32.9 1.7 ITNA 83N0I 01

1.1 0.08 35 RTNA 75GLA 01 1 33 ICPES SONAD 01 1.19 DNA 85GAU 04 1 33 1 ITNA 76BL0 01 1.2 0.05 IDMS 78CAR 02 1 33 3 ITNA 78NAD 02

1.2 0.1 ITNA 7RMAD 1 33 3 ITNA 78MAC 01 1.2 0.1 ITNA 07 1 33 4 ITNA 73ABE 01

1.21 IDMS ni 1 33 6 ITNA 80BUA 01 1.24 0.05 ITNA r OKnu ni 1

1 33.6 AA 78GU! 01 1.25 0.06 ITNA ftoei 17

1 33.9 11 ICPES 85HAR 01 1.26 ITNA f JKLC m 1

1 33.9 3 PAA 74CHA 01 1.3 0.1 6 PAA 01 1

1 34 ITNA 84CLE 01 1.3 0.1 PAA 80SEG 01 1 34 ICPES 80NAD 01 1.33 0.05 DNA 84GLA 02 1 34 3 PAA 76CHA 01 1.3A 0.5 ITNA 78MAC 01 1 35 ITNA 78UEA 01 1.35 ITNA 78WEA 01 1 35 2.9 ITNA 76STE 05

1 .37 0.08 ITNA 74WEA 01 1 35 2.9 D NAA 79STE 01 1.4 ITNA 81 WAN 01 1 35 2.9 ITNA 77R0W 03

1.4 0.1 6 PAA 82SEG 01 1 35 4 ITNA 79FRU 01 1.4 0.4 ITNA 01 1

1 35.2 1 .5 AA 79R0S 03

1.41 0.07 GAMMA 01 1

1 35.8 3.4 ITNA 81WAN 01 1.41 0.07 GAMMA 750ND 01 1

1 35.9 0.8 11 AA 82LIN 03

1.41 0.07 D NAA 740ND 01 1

1 36 AA 76UEW 01 1.43 DNA 75MIL 01 1 36 2 ITNA 79GRE 01 1.45 0.04 D NAA 79STE 01 1 36 3 ITNA 750ND 01

1 .45 0.04 lENA 77R0W 04 1 36 3 D NAA 740ND 01

1 .46 0.02 lENA 76sTE 05 1 36 4 ITNA 76UEU 01

1 .46 0.02 D NAA 79sTE 01 1 36 4 ITNA 73SHE 01

1 .46 0.04 lENA 77R0W 03 1 36.2 FAA 78GUI 01

1 .46 0.35 ITNA 75RUC 01 1 37 3 ITNA 75RIC 01

1 .49 35 DNA 81GLA 03 1 37.6 1 .4 ITNA 77MAE 01 1.5 ITNA 75MIL 01 1 37.9 1 .7 11 AA 82LIN 03

1.5 0.1 13 PAA 81SEG 01 1 38 1 .2 ICPES 81CHU 01

1 .52 0.11 ITNA 76STE 05 1 38 4 XRF 79FRU 01 1.6 0.2 13 PAA 81SEG 01 1 40 3 ITNA 75KLE 01 1.6 0.2 NAA 76HAN 01 1 41 10 ITNA 76RAG 01 1.6 0.2 ITNA 79FR1J 01 1

1 42 2 ITNA 82SUZ 02

2 34 UXRF fl7MI o^n 1 i u 01 1

1 43 4 AA 79REI 01 6 AA 7AUFU 01 1 50

50 10

ITNA XRF77GLU 01 79PRA 01 V (ug/g)

U (ng/q)

24 8 EXRF 79GIA 01 1

' 30 6 35 ITNA 81GLA 03 1 450 90 ITNA 81 WAN 01 31 4 ICPES 84NA0 01 1 630 60 ITNA 77MAE 01 V4 C 31 .5 2.6 11 AA 82LIN 03 1 650 150 ITNA 76RAG 01 32 34 UXRF 82MIL 01 1 710 70 D NAA 79STE 01

3C. 1 .3 OES 76UEU 01 1 ^4 n 710 70 lENA 77R0W 04

32 4 ITNA 78LAU 02 1 710 80 ITNA 82SUZ 02

32.5 1.5 NAA 76HAN 01 1 740 300 ITNA 75RUC 01 32.7 0.6 11 ICPES 85HAR 01 1 32.7 3.4 ITNA 75NAD 02 1 1632-22
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRH 1632 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

W (ng/g) cont • Zn (uq/q)

750 ITNA 78UEA 01 1 21 11 ICPES 85HAR 01 750 100 lENA 77R0U 03 1 30 10 ITNA 750ND 01 750 170 ITNA OOND U1 1 30 10 D NAA 740ND 01 780 80 ITNA 79GRE 01 1 32 3 ITNA 75NAD 02

790 170 lENA 76STE AC 1 05 1 32 3 XRF 79FRU 01 870 200 ITNA 77CAH 01 1 32 3 ITNA 78NAD 02

1900 800 ITNA 73SHE 01 1 32 8 SSMS 77D0N 01 33 3 9 ITNA 78LAU 02

Y (ug/g) 34 XRF 75KLE 01 34 4 AA 79REI 01 6.6 11 ICPES &5HAR 01 1 34 ITNA 78UEA 01 7 AA 82GUP 02 1 34 1 EXRF 81KIN 01 7 1 XRF 79PRA 01 1 34 9 ITNA 77CAH 01 7.4 34 UXRF 82MIL 01 j 34 17 ITNA 76UEU 01 7.6 0.81 OES 76WEW 01 1 34.9 1.6 11 AA 82LIN 03

7.9 0.6 EXRF 79GIA 01 1 35 2 12 ITNA 82SUZ 02

8 OES 82GLIP 02 1 35 5 ITNA 77JER 01 8.3 0.2 11 ICPES 85HAR 01 1 35.7 9.9 EXRF 79GIA 01 36 ICPES 80NAD 01 Yb (ng/q) 36 0.6 RTNA 740RV 01 36 7 6 PAA 82SEG 01 550 40 ITNA 73SHE 01 1 36.6 1.4 EXRF 73SPA 01 550 80 ITNA 76UEU 01 1 36.9 1.1 11 AA 82LIN 03

670 20 ICPES 81CHU 01 1 37 AA 76UEW 01 690 40 ITNA 78NAD 02 1 37 3 PAA 76CHA 01 690 40 ITNA 75NAD 02 1 37 3 PAA 77JER 01 700 AA 82GUP 02 1 37 3 XRF 79PRA 01 700 100 ITNA 78LAU 02 1 37 3 ITNA 79FRU 01 700 100 ITNA 750ND 01 1 37 6 lENA 77R0W 04

740 90 ITNA 77CAH 01 1 37 10 NAA 76HAN 01 760 30 ITNA 76RAG 01 1 37.2 17.4 ITNA 75RUC 01 780 70 ITNA 75RUC 01 1 37.5 2.8 PAA 74CHA 01 790 20 RTNA 840DD 01 1 38 34 UXRF 82MIL 01 800 ITNA 75HIL 01 1 38 5 SSMS 77PAU 01 810 20 ITNA 77MAE 01 1 38.1 0.8 AF 75EPS 01

810 40 ITNA 8400D 01 1 38.1 1.4 RTNA 77JER 01 840 70 D NAA 79STE 01 1 38.4 0.9 AA 74RAI 01 840 70 5 ITNA 77R0U 04 1 38.4 1 AA 75EPS 01 840 70 ITNA 77R0U 03 1 38.5 AA 78GUI 01 880 90 5 ITNA 77R0W 04 1 39 ICPES 80NAD 01 910 70 OES 76UEU 01 1 39 EXRF 82KEE 01 950 50 lENA 77R0W 04 1 39 1 FAA 74TAL 01 1000 200 NAA 76HAN 01 1 39 1 7 AA 73TAL 01 1000 200 ITNA 78MAC 01 1 39 2 11 ICPES 85HAR 01 1030 80 ITNA 82SUZ 02 1 39 2 12 ITNA 82SUZ 02

1200 200 ITNA 81 WAN 01 1 39 3 6 PAA 82SEG 01 39 3 PAA 80SEG 01 39 6 ITNA 77R0W 03

39 6 D NAA 79STE 01 39 6 D ITNA 77R0W 04

1 40 1.2 ICPES 81CHU 01 1632-23
TABLE 1632-2: INDIVIDUAL DATA FOR NBS SRM 1632 (cont.)

Cone Uncer Com Method Reference I

Zn (ug/g) cont.

40 2 ICPES 84NAD 01 40.8 4 ITNA 81UAN 01 42 ITNA 77GLU 01 43 2 ITNA 76RAG 01 45 17 OES 76UEU 01 50 10 ITNA 78LAU 02

52 4 ITNA 78MAC 01 58 7 ITNA 77MAE 01

(ug/g)

1.56 0. 14 PAA 74CHA 01 16 2 PAA 76CHA 01 25 0. 75 ICPES 81CHU 01 25 3 OES 76UEU 01 28 24 ITNA 76RAG 01 33 4 EXRF 79GIA 01 38 34 UXRF 82MIL 01 40 4 9 ITNA 78LAU 02

41 ITNA 75MIL 01 45 ITNA 75ICLE 01 46 AA 76WEW 01 85 9 12 ITNA 82SUZ 02

90 10 12 ITNA 82SUZ 02

1632-24
i5 2

2 S

cn t/) UJ X u (AMU — (/»»- CD & O LL.

in *- M ^ ^

S „- o w

4* : a

»- ro «- <- INJ

t OJ *- Kt rsj

CM CO -sj »- f- *~ in ^ Kl <- ^ ^

(\j m »- r- ^ <Nj N. m fvj «- o- ^ tn o

O M\

in CO o o o

M M \r\ *\ o <trg

in o O

in

o fO o oin nj

N. oj

^o m 00

N»«- IM

inO sj-

** *i to Kl

CO O CO

in

<NJ »-

>0 * ** M m

o— o «- nj

-st cj «— (\J o o

•O nj

in

CO k!

in >0 0> O o O • nj

. CO • o in O N- S

in

lO O O o o in . tnro <M o» o "J- »- -4- -O K) p^ in o ^ • Kl PO K fSJ O CO

rg O

BO ^ »- <M o >o

in *— o >*

»- 00 nj

-in in in o o •— orvj 00 «-

• • o o o o o m d o

»- o

no o. pg o ?o «- . in n5

o 00 o o ^ N. ni ^O O

in o o «- fM

• CO rg rg o CO o tn o- o o O- e0Ki»- .-KiN-inrg

Ol Q) ^ O) 01 0> O ^ ^ -V *v. Q> O) cr> C7I C) 9> o> OIO)?>0>Q>0>90tO) ^ ^ ^ ^

0> O) 5* 3 3 C 3 3 1

01 Ot O) O)

"N.

O (_) O (J

4) (0 "P 41 u. u. u- O O C3

r> on c c

1632A-1
«— «— ro

o

-* r- 6 SO

5 mm a.

*~ rNj (M r- T- (M

«~ o • a -0 O w- win o

CM u-\ rvj ^ tA «S o o o

Nt O ^ N»

OD O O

IT* (M in rsr

<M

CO 03 CO O u~i

o

ao ro

»- (\J g a- »- f\J 00 ^ -O Kt ^ (NJ «0 NT ^ rn ir>

in Ki 2 in t> o -v*

in fsj in nO ^ CO

o> Q K> c>> K(

ro CO • • • >f 00 o

»- t CO O fVJ «- I >o

in K> o o • M O »-

fNj rg CO sT ro

s» o lA T- "in ^ • . r^. in

S- »- <M

«- (\j »~ ^0f^0>0»^K>OC0O'--'0«- nO O

3 g

(J V

f\J »-

fS( f\J K>

«— o O' fVJ rvj in >*

•sj -4^

*- in o o o 2

_ 00 CO rvj ^ rj ^ f\J -J- o « o o o -J- O (Nl

O ^ lA 4 -H 44 00 ry fo O • in

' N.

in ^ c ;

C7>

« 1 1

o o

rj rg

CO O fM fM PO »0

fM fSJ (M a 0) ^ ^ jc x:

in 00 M K> K>

(M fM rg 3 3 3 > 3

1632A-2
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRM 1632A (revised 3/1/86)

Cone Uncer Com Method Reference Cone Uneer Com Method Referenee

Aq (ng/g)

1

1 As (ug/q) cont t.

< 1500 ITNA 86GLA

1 01 1 9.21 0.15 ITNA 86GLA 01 < 3000 L UXRF 82MIL 01 1 9.27 AF 82WIL 01 300 ITNA 79CAH 01 1

1

9.34

9.4 1.3

FAA ITNA82UIL

830BR

01

01 Al (%) 1 9.4 1.3 ITNA 79CAH 01

1 9.5 11 HAA 82CR0 03

2.74 34 AA 83BET 01 1 9.54 0.64 HAA 82NAD 01 2.8 0.27 CPXRF 80KIR 01 1 9.6 11 FAA 82EBD 02

2.81 0.02 34 AA 83BET 01 1 9.7 0.3 ITNA 85GAU 04

2.82 0.13 ITNA 83JER 01 1 9.8 11 FAA 82EBD 02

2.86 0.03 ICPES 85HAR 01 1 9.8 11 HAA 82CR0 03

2.9 0.05 TCGS 79AND 01 1 9.9 0.5 PAA SOGER 01 2.9 0.12 ITNA 82JER 01 1 10.2 0.4 ITNA 81JIN 01 2.9 0.3 ITNA SOGER 01 1 11 2 ITNA SOGER 01 2.91 0.05 ITNA 86GLA 01 1 11.1 1 .3 ITNA S5SUN 01 2.93 0.03 AA 82NAD 02 1 2.95 0.04 XRF 79CAH 01 1 ASH (%)

2.96 0.14 ITNA 85SUN 01 1 2.97 0.04 lENA 85GLA 02 1 21.7 UU S5SHI 01 2.99 0.06 ITNA 830BR 01 1 21 .7 UU 82EBD 02

2.99 0.14 ITNA 84GLA 02 1 21 .8 34 CB 82MIL 01 3 0.01 ICPES 84NAD 01 1 22 11 AA 84NAIC 01 3 0.05 ICPES 82NAD 02 1 22 CB S2KAM 01 3 0.1 AA 83RAP 01 1 3.01 0. 13 TCGS 79FAI 01 1 Au (ng/g)

0. ID D TCGS 80GER 01 1 3.01 0.13 D TCGS 80AND 01 1 < 8 ITNA 86GLA 01 3.0576 0.0106 ICPES 85PEA 01 1 < 50 L ITNA 79CAH All 01 3.06 0.08 ITNA 85AICA 01 1 3 1 ITNA 80KOS 01 3.07 0.13 ITNA 80GAR 01 1 3.1 ITNA 84CLE 01 1 B (ug/q)

3.1 0.06 AA 82KAM 01 1 3.33 CPAA 83BIR 01 1 22 3 ICPES 81 NAD 01 9.47 EXRF 82EBD 02 1 50.9

52

0.5

19

TCGS

ITNA

79AND

82SCH

0105

As (ug/g) 52.7 1.8 TCGS 79FAI 01 53 2 TCGS 80AND 01 6.4 2.

1

CPXRF 80KIR 01 1 53 2 D TCGS SOGER 01 7.6 11 FAA 82EBD 02 1 54 TCGS 85GAU 04

8.3 1 ITNA 83JER 01 1 55 OES 83HIL 01 8.4 11 FAA 82EBD 02 1 55 4 35 TCGS SIGLA 04

8.7 0.2 ITNA 82JER 01 j 8.7 0.3 HAA 85LIN 02 1 Ba (Uq/q)

8.88 1 .22 ICPES 81 NAD 01 1 9 11 FAA 82EBD 02 1 97 7 ITNA 84TU 01 9 0.4 ITNA 80KOS 01 1 100 13 ITNA 81JIN 01 9 0.4 ITNA 81KUL 01 1 102 1 ICPES 84NAD 01 9 0.9 ITNA 84CHA 02 1 102 6 ITNA 84SUZ 02

9.2 34 WXRF 82MIL 01 1 112 3 ICPES S5HAR 01 9.2 0.5 AA 83RAP 01 1 116 7 5 ITNA SOTOU 01 9.2 1.2 ITNA 84TU 01 1 119 27 ITNA 85SUN 01 1632A-3
Cone Uncer Com

TABLE 1632AMethod

2: INDIVIDUAL DATA

Reference |

FOR NBS SRM 1632A

Cone

(cont.)

Uncer Com Method Reference

1 (ug/q) cont 1

1

C- Fixed (%)

120 10 ICPES 82NAD 02 1 43 11 AA 84NAK 01

122 11 ITNA 80GER 01 1 125 34 UXRF 82MIL 01 1 Ca (uq/g)

126 11 ITNA 82JER 01 1 132 7 ITNA 85AKA 01 1 2100 100 PAA 80GER 01

136 16 ITNA 03GAU t\i 1 Uh I 2160 130 ITNA U1 138 20 ITNA 79CAH 01 1 2200 300 ITNA 84GLA 02

150 26 ITNA 80GAR 01 1 2240 30 ICPES 85HAR 01 170 15 ITNA 84CHA 02 1 2300 30 AA 82NAD 02

2300 100 XRF 79CAH 01 (ug/g) 2300 200 AA 82KAH 01 2340 270 ITNA 85SUN 01 1.48 0.08 11 AA 82LIN 03 1 2400 30 ICPES 82NAD 02

1.53 0.04 11 AA 84NAK 01 1 2400 100 34 AA 83BET 01 1.63 0.1 11 AA 82LIN 03 1 2400 200 D TCGS 80AND 01 1.7 OES 83MIL 01 1 2400 200 D TCGS 79AND 01 1.73 0.15 11 AA 82LIN 03 1 2400 200 D TCGS 80GER 01 2400 200 ITNA 80GER 01 (ug/g) 2400 200 TCGS 79FAI 01 2450 140 ITNA 830BR 01

< 1 L UXRF 82MIL 01 1 2600 34 AA 83BET 01 2600 ITNA 84CLE 01 (ug/q) 2600 100 ICPES 84NAD 01 2600 200 ITNA 85AKA 01 38 2 ITNA 83JER 01 1 2652.65 ICPES 85PEA 01 38.3 4.9 ITNA 84CHA 02 1 2700 175 ITNA 80&AR 01 39 3 ITNA 84SUZ 02 1 46500 EXRF 82EBD 02

39.6 1.9 ITNA 830BR 01 1 40 2 ITNA 84GLA 02 1 Cd (ng/g)

40 2.3 ITNA 82JER 01 1 41 4 ITNA SOGER 01 1 150 30 TCGS 79AND A 4 01 42 34 UXRF 82MIL A 4 1 01 1 160 34 FAA 83BET A 4 01 42 1 ITNA 86GLA 01 1 170 60 34 FAA 83BET A 4 01 43 ISE 81 NAD 01 1 180 40 AA 83RAP A4

43 0.6 ITNA 81 JIN A 1 1 01 1 200 50 ITNA OUKOS 01 43 7 ITNA 79CAH 01 1 210 30 TCGS 79FAI A 4 01 43.1 1.1 ITNA 85 SUN 01 1 210 30 D TCGS 80GER A401 44.5 2.7 5 lENA 79GLA 02 1 210 30 D TCGS 80AND A401 44.9 0.9 5 lENA 79GLA 02 1 50 4- 5 ITNA 80TOU 01 1 Ce <ug/g)

60 ISE 83NAD 01 1 25.7 7.2 CPXRF 80KIR 01

<%) 26 1.7 ITNA 79CAH A401 26 3 ITNA 85AI(A A401 61.3 14 CB 85NAD 01 1 27 4 ITNA 81KUL A 4 01 62.08 0.1 14 CB 27 4 ITNA (J 1 62.7 0.06 CB 80SCH 02 1 28 2 ITNA 84SUZ 02

65 4 TCGS 79AND 01 1 28.5 0.3 ITNA 81JIN 01

71 4 D TCGS 80AND 01 1 28.5 0.4 ICPES 82CR0 01

71 4 TCGS 79FAI 01 1 29.7 0.9 ICPES 83MAH 05

71 4 D TCGS SOGER 01 1 30 ITNA 85GRE 02

1632A-4
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRM 1632A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ce (ug/g) cont.

1

1 Co (ug/g) cont.

30.2 1.2 UNA 85SUN

1 01 1 7.3 1.3 11 AA 84NAK 01 30.8 0.5 UNA 84TU 01 1 7.5 UNA 84CLE 01 31.1 3.4 UNA 80GAR 01 1 7.5 0.4 UNA 79CAH 01 31.8 1.5 UNA 85GAU 04 1 8.5 1 UNA 83JER 01 32 34 UXRF 82MIL 01 1 32 4 UNA 80GER 01 1 Cr (ug/g)

CI (ug/g?

1

1

1

3.4

12.8

0.2

2

AA

ICPES

83RAP 01 84NAD 01 700 10 IC 85GEN 01 1 26 2 11 AA 84NAK 01 700 100 XRF 79CAH 01 1 26 3 UNA 81KUL 01 704 42 UNA 85SUN 01 1 26 6 UNA SOKOS 01 743 46 IC 83NAD 01 1 30 2 ICPES 85HAR 01 750 15 UNA 86GLA 01 1 30.9 0.6 UNA S4TU 01 750 60 UNA 84GLA 02 1 31 DCPES 85MCC 02

760 34 UXRF 82MIL 01 1 31.2 3.7 UNA 84CHA 02

766 30 TCGS 79AND 01 I 31.8 3.7 11 AA 82LIN 03

770 ISE 83NAD 01 1 32 1.9 AA S2ICAM 01 770 24 UNA 82JER 01 1 33 3 UNA 85AKA 01 770 48 ISE 81 NAD 01 1 33.3 ICPES 81MER 03

776 20 UNA 83JER 01 1 33.3 1.6 UNA 81JIN 01 776 36 UNA 830BR 01 1 33.4 1.5 UNA 85SUN 01 784 17 TCGS 79FAI 01 1 33.8 34 FAA 83BET 01 784 17 D TCGS SOGER 01 1 33.8 2 UNA 83JER 01 784 17 D TCGS 80AND 01 1 34 2 UNA 80GER 01 800 70 UNA 80GER 01 1 34 3.6 UNA 82JER 01 897 23 UNA 806AR 01 1

1

34

34.4

4

2.4

XRF

UNA

85HAR 01 84SUZ 02

Co (ug/g) 1

1

34.7

34.8

2

6 34

UNA

FAA

86GLA 01 83BET 01 4.4 0.3 ICPES 85HAR 01 1 35 UNA 84CLE 01 5.86 0.21 UNA 81JIN 01 i 35.6 1 UNA 85GAU 04

6 34 UXRF B2MIL 01 1 36 2 UNA 79CAH 01

6.1 0.1 UNA 84TU 01 1 36 3.5 CPXRF 80KIR 01

6.1 0.4 UNA 84SUZ 02 1 36 6 UNA 80GAR 01 6.3 1.3 34 FAA 83BET 01 1 36.9 1 11 AA 84NAK 01 6.4 0.6 AA 83RAP 01 1 36.9 3.3 11 AA 82LIN 03

6.5 ICPES 81MER 03 1 39 8.8 AE+AF 82GOL 01 6.5 0.2 UNA SOGER 01 1 40 34 UXRF 82MIL 01 6.5 0.5 UNA 81KUL 01 1 6.56 0.22 UNA S5GAU 04 1 Cs (ug/g)

6.6 0.3 UNA 86GLA 01 1 6.6 0.5 5 UNA 80TOU 01 1 1.9 0.6 UNA 79CAH 01 6.6 1.1 UNA 80GAR 01 1 2 0.3 UNA 80GER 01 6.7 0.1 ICPES 83MAH 05 1 2 0.32 UNA 84CHA 02

6.7 0.9 11 AA 84NAK 01 1 2.12 0.13 UNA 84GIB 01 6.71 0.11 UNA 85SUN 01 1 2.2 0.1 UNA 85AKA 01 6.8 0.3 UNA SOKOS 01 1 2.27 0.15 ITNA 85GAU 04

7 0.4 UNA S5AKA 01 1 2.3 0.11 UNA 81JIN 01

7.1 0.5 UNA 84CHA 02 1 2.33 0.07 ITNA 85SUN 01 7.3 34 FAA 83BET 01 1 2.4 0.2 ITNA 81KUL 01

1632A-5
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRH 1632A (cont.)

Cone Unccr Coni Method Reference | Cone Uncer Com MGthod Reference

Cs fua/a) cont Eu fna/a>

2.4 0.8 ITNA 80GAR 01 1 410 50 ITNA 85AKA 01 2.47 0.12 ITNA 84TU 01 1 460 20 ITNA 830BR 01 2.5 34 UXRF 82HIL 01 1 490 10 ICPES 82CR0 01 2.5 0.2 lENA 80KOS 01 1 490 50 ITNA 84CHA 02

2.9 1.4 ITNA 84SUZ 02 1

1

500

510

40

30

ITNA

ITNA

84SUZ 02

81JIN 01 Cu (ua/a) 1

1

510

510

70

82

ITNA

ITNA

86GLA 01 80GAR 01 14 DCPES 85MCC 02 1 540 40 ITNA 85GAU 04

14.5 0.5 XRF 85HAR 01 1 540 80 ITNA 80KOS 01

15 0.45 AA 82KAH 01 1 540 80 ITNA 81KUL 01 15.3 0.9 11 AA 84NAK 01 1 550 30 ITNA 79CAK 01 15.4 1.9 ITNA 84SUZ 02 1 550 30 ITNA 80GER 01 15.5 0.7 ICPES 85HAR 01 1 600 ITNA 85GRE 02

15.7 1.6 11 AA 84NAK 01 1 610 30 ITNA 85SUN 01 15.8 0.6 11 AA 82LIN 03 1 15.9 0.4 AA 79CAH 01 1 F (ug/g)

16 2.1 CPXRF 80KIR 01 1 16.1 0.6 AA 83RAP 01 1 84 8 ISE 81 NAD 01 16.3 34 FAA 83BET 01 1 95 ISE 83KNA 01 16.3 0.2 ICPES 83MAH 05 1 164 CPAA 83BIR 01 16.4 ICPES 81MER 03 1 176 14 CPAA 85CLA 02

16.6 0.6 11 AA 82LIN 03 1 177 ISE 82MCG 01 16.7 2 34 FAA 83BET 01 1 178 SSHS 85CLA 02

17 34 WXRF 82MIL 01 1 200 ISE 83NAD 01 17.2 3 FAA SOLAN 01 1 210 10 IC 83NAD 01 19.8 1.5 ICPES 84NAD 01 1

< 2.5

1.83 0.11

1.98 0.53

2 0.1

2.1 0.1

2.11 0.11

2.13 0.15

2.2 .0.1

2.2 0.1

2.2 0.3

2.56 0.26

(ug/q)

0.91

3

0.05

UXRF

ITNA

ITNA

ITNA ICPES ITNA

ITNA

ITNA ITNA

ITNA

ITNA

UXRF

ICPES

82MIL 01 830BR 01 80TOU 01 82JER 01 82CRO 01 86GLA 01 85SUN 01 79CAH 01 84SUZ 02

SOGER 01 SOGAR 01

82HIL 01 82CR0 01

Fe (%)

I 1632A-6

0.89

1.00

1.03

1.07

1.07

1.08

1.08

1.09

1.10

1.10

1.10

1.10

1.10

1.10

1.104

1.1

1.1

1.1

1.1

1.1

1.12

1.12

14

0.03

0.14

0.01

0.03

0.02

0.08

0.08

0.02

0.02

0.06

0.1

0.3

0.01

0.02

0.06

0.06

0.06

0.028

0.01

0.01

34

34

ICPES

ITNA

ITNA ICPES

XRF

ITNA AA

ITNA AA

ITNA ICPES

ITNA ITNA

ITNA

ITNA AA

TCGS

TCGS

TCGS

ICPES

ICPES

ITNA

84NAD 01 84CLE 01 84CHA 02

85HAR 01 79CAH 01 83JER 01 83BET 01 84SUZ 02

83BET 01 81JIN 01 S3HAH 05

81KUL 01 85AKA 01 82JER 01 84TU 01 82NAD 02

80AND 01 79FAI 01 SOGER 01 85PEA 01 82NAD 02

80KOS 01
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRM 1632A (cont.)

Cone

Fe (%) cont.

Uncer Com Method Reference

1.12 0.09 ITNA 80GAR 01 1.125 ICPES 81MER 03

I 1 nn U 1 1.14 0.01 AA 79CAH 01

1 .14 0.04 ITNA 85GAU 04

1.14 0.05 ITNA 86GLA 01 1.16 0.03 ITNA 80GER 01 1.16 0.37 ITNA 79CAH 01 1.17 0.04 AA 83RAP 01

1.17 0.04 TCGS 79AND 01 1.2 0.02 AA 82KAN 01 AD . 7Rr O P¥DP tAKr occou n?yjc

7.2 2.5 CPXRF 80KIR 01 7.84 0.6 ITNA aSOBR 01 8 0.8 ITNA SOGER 01 8.2 FAA 85X1

A

01 8.4 34 UXRF 82MIL 01 8.5 0.8 ITNA 79CAH 01

Gd (ug/g)

1.9 0.2 TCGS 79AND 01

1 05 n 01

1.95 0.03 TCGS 79FAI 01 2.4 0.2 ICPES 82CRO 01 3 34 WXRF 82MIL 01 3 0.05 TCGS 80AND 01 3.4 0.3 ITNA 84SUZ 02

Ge (ug/g>

UVDP WAKr r 1 OCri k L U 1

H (%)

3.68 0.07 TCGS 79AND 01 3.7 0.1 TCGS 79FAI 01 3.7 0.1 D TCGS 80AND 01 3.7 0.1 D TCGS 80GER 01 4.17 14 CB 85NAD 01 4.17 0.01 CB 80SCH 02

4.59 0.07 14 CB 85NAD 01

H20- (%)

1.6 GRAV 85LIN 02

1.62 FD 80KHA 02

2.6 0.1 GRAV 85HAN 01 2.6 0.1 2 MPOES 85HAN 01 2.6 0.1 2 MPOES 85HAN 01

Cone

Hf Cug/g)

1.43

1.44

1,46

1.55

1.55

1.65

1.68

1.7

1.7

1.8

1.9

Hg (ng/g)

90

118

120

122

129

129

134.1

134.1

135

169

170

210

Ho Cng/g)

340

380

I Cug/g)

0.9

1.63

1.77

1.8

2

In (ng/g?

36

36

40

40.5

Uncer Com Method Reference

0.05

0.09

0.07

0.08

0.11

0.15

0.06

0.1

0.2

0.3

0.3

15

14

50

6

10

20

3.1

18

65

20

90

0.2

0.3

3

4

10

5

ITNA 84TU 01 ITNA 81JIN 01 ITNA 85 SUN 01 ITNA 80GER 01 ITNA 84SUZ 02

ITNA 85GAU 04 ITNA 86GLA 01 ITNA 79CAH 01 ITNA 85AICA 01 ITNA 80GAR 01 ITNA 80TOU 01

ITNA 84CHA 02

CVAA 80NAD 01 ITNA 80KOS 01 CVAA 85DUM 02

RTNA 84DRA 01 RTNA 84DEL 01 AF 82UIL 01 CVAA 82EBD 01 CVAA 82DCO 01 ITNA 84SUZ 02

CVAA 81 NAD 01 ITNA 81iCUL 01

< 2000 L UXRF 82MIL 01 110 ITNA 84SUZ 02

50 ICPES 82CR0 01

34 UXRF 82MIL 01 ITNA 85SUN 01 lENA 84GLA 02 ITNA 80GER 01 ITNA 84SUZ 02

ITNA 8308R 01 ITNA 80GER 01 ITNA 79CAH 01 ITNA 84CHA 02

1632A-7
TABLE 1632A- 2: INDIVIDUAL DATA FOR NBS SRM 1632A (cont.

)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

K (uq/g)

1

1

1

Li (ug/g)

3A00 100 ITNA 83JER 01 1 35 OES 83MIL 01 3700 XRF 79CAH 01 1 36.2 0.1 AA 79CAH 01 3800 50 ITNA 830BR 01 1 37 1 ICPES 84NAD 01 3900 100 ICPES 84NAD 01 '

1 47 CPAA 83BIR 01 4000 200 ITNA 81JIN 01 j 4000 900 ITNA 84CHA 02 1 Lu (ng/g)

4100 80 AA 82KAM 01 1 4100 100 TCGS 79AND 01 1 134 13 ITNA 80KOS 01 4100 200 ICPES 82NAD 02 1 150 10 ICPES 82CRO 01 4100 500 ITNA 86GLA 01 1 163 10 ITNA 84CHA 02

4120 50 ITNA 85SUN 01 1 170 20 ITNA S5SUN 01 4200 34 AA 83BET 01 1 170 30 ITNA S5AKA 01 4200 150 AA 82NAD 02 1 173 12 ITNA 86GLA 01 4200 200 D TCGS 80GER 01 1 174 24 ITNA 84SUZ 02

4200 200 TCGS 79FAI 01 1 177 10 ITNA 85GAU 04

4200 200 D TCGS 80AND 01 ! 180 ITNA 85GRE 02

4200 200 ITNA 79CAH 01 1 180 30 ITNA SOGER 01 4200 200 ITNA SOGER 01 1 ISO 70 ITNA 80GAR 01 4200 400 34 AA 83BET 01 1 190 20 ITNA 81JIN 01 4300 645 ITNA 80GAR 01 1 220 40 ITNA 79CAH 01 4400 300 ITNA 85AKA 01 1 4523.5 166 ICPES 85PEA 01 1 Mg <ug/g)

4700 300 ICPES 85HAR 01 1 14900 EXRF 82EBD 02 1 600 300 XRF 79CAH 01

1 870 10 ICPES 84NAD 01 K-40 (pCi/g) 1 910 DCPES 85MCC 02

1 980 40 ICPES 85KAR 01 2.7 0.2 GAMMA 84R0S 03 1 990 30 AA 82KAM 01

1 990 40 AA 82NAD 02

La (ug/g) 1 1020 10 ICPES 82NAD 02

1 1052 ICPES 85PEA 01 8.88 0.74 ITNA 84CHA 02 1 1100 100 34 AA 83BET 01 10.9 0.5 ITNA 80KOS 01 j 1300 34 AA 83BET 01 11.4 0.6 ITNA 84SUZ 02 1 1300 300 ITNA SOGER 01 12.8 0.5 ITNA 830BR 01 1 1400 100 lENA 85GLA 02

13.03 0.3 ITNA 81JIN 01 1 1400 220 ITNA SOGAR 01 14.2 0.1 ITNA 86GLA 01 1 1600 700 ITNA 85AKA 01 14.5 0.2 ICPES 82CRO 01 1 1714 CPAA 83BIR 01

15 ITNA 85GRE 02 1 19900 EXRF 82EBD 02

15 2.6 ITNA 80GAR 01 1 15.1 1.2 ITNA 79CAH 01 1 Mn (ug/g)

15.2 0.8 ICPES 83MAH 05 1 15.4 0.6 ITNA 85SUN 01 1 20 4.3 CPXRF 8QKIR 01 15.6 0.4 ICPES 85HAR 01 1 23 ITNA 84CLE 01 15.9 0.6 ITNA 85GAU 04 1 26 2 34 FAA 83BET 01 17 1 ITNA 85AKA 01 1 26 6 AE+AF S2G0L 01 18 2 ITNA SOGER 01 1 27 2 ITNA 83JER 01 19 34 WXRF 82MIL 01 1 27.1 0.4 ICPES 83MAH 05

19 2 ITNA 83JER 01 1 27.3 1.4 ITNA S2JER 01

21 1 ITNA 82JER 01 1 27.4 2.5 ITNA 84CHA 02

28 ESR 85SHI 01

1632A-8
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRM 1632A (cont.)

Cone

S (%>

0. 09

1.19

1.37

1. A8

1.48

1.48

1.5

1.5

1.57

1.58

1.59

1.59

1.59

1.59

1.59

1.6

1.6

1.62

Sb (ng/g)

410

460

520

530

530

560

580

600

600

600

600

620

620

620

630

640

650

690

800

1000

Sc (ug/g)

5.3

5,7

5.9

6

6.06

6.1

6.14

0.01

0.01

0.003

0.07

0.7

0.7

0.01

0.02

0.02

0.02

0.02

0.03

0.09

0.02

0.07

150

30

50

50

40

40

90

20

50

80

60

150

90

50

50

1.2

0.2

0.2

0.3

0.11

0.4

0.2

11

11

5

34

Method Reference | Cone Uncer Com Method Reference

Se (ug/g) cont •

ICPES 85PEA 01 1 6.2 34 UXRF 82MIL 01 XRF 79cAH 01 1 6.2 0.2 ITNA 79CAH 01 IC 83NAD 01 1 6.2 0.3 ITNA 86GLA 01 XRF 83NAD 01 1 6.3 0.1 ITNA 80KOS 01 IC 03GcN ni 1 01 1 6.3 0.2 5 ITNA 80TOU 01 XRF 0INAD Ul 1 6.4 0.2 ITNA 83JER A401 UNA 82JER 01 1 6.42 0.25 ITNA 84CHA 02

NAA 111 un u 1 HU n9 1 Uc 1 6.56 0.23 ITNA on/* A D BOGAR ni01 CB oOuAU ni 1 u 1 1 6.7 0.05 ITNA Q 1 ITU 01 JIN ni01 CB ojuLA HT 1

1 6.8 0.6 ITNA oOGcR ni01 TCGS uUnnU 1 6.9 0.9 5 ITNA onT^M 1 oOTUU ni01 TCGS oUbbK 1 TCGS "TOOL 1

f VrAI ni 1 Ul 1 Se (ug/g)

CPAA Q/ 1 A U ohLAN no 1 U<:

1 TCGS 7nA kir\ f VAND ni 1 U1 1 1.9 0.5 ITNA 86GLA 01 XRF 84UEB 01 1 2.4 34 UXRF 82MIL 01 CPXRF 80KIR 01 1 2.4 0.2 AA 83RAP Al01 UU odcoD no 1 Vd 1 2.4 0.3 RTNA 80KNA A101 2.54 0.45 ITNA ohCHA 0^

2.55 0.29 FAAC OCI uv\ ObUOO 01 2.57 0.05 lENA BOKOS A 4 01 HAA OOkl Af\ i5<:NAD ni 1 01 1 2.58 FAA 001 It 1 B<:UIL 01 ITNA o4GIB ni 1 01 1 2.59 AF 001 1 f 1 B^UI L 0^

ITNA 0*5 1 CD ni 1 01 1 2.6 0.3 ITNA BOGcR ni01 ITNA 0 i ^1 II OIKUL ni 1 01 1 2.65 0.02 7 HAA 0/ T UA Oh IMA niUl ITNA OUKOS ni 1 01 1 2.65 0.1 D HAA D/ T UA BhIHA n*z Uj

AA D7D A n ooKAP m 1 01 1 2.69 0.4 RTNA 0/ nc 1 niUl ITNA O^^l A OOGLA ni 1 01 1 2.7 0.3 HAA QC 1 T U niUl HAA O^CRU Oo 1 2.7 0,3 HAA OCl f U BsLIN no

ITNA 0/ r*i c ni 1 01 1 2.7 0.4 ITNA 0 / CI 17 noU^

HAA ni 1 Uo 1 2.9 0.2 ITNA fil^A^A OjIKkR niUl ITNA SOGER 01 1 3 0,1 ITNA 79CAH 01 ITNA OT 1 CD ni 1 01 1 3 0,4 ITNA fl/ Tl 1 OHiU niUl ITNA 0/ Tl 1 o4TU ni 1 01 1 3.1 ITNA 0/ f*l c BhCLc ni01 ITNA 81JIN ni 1 01 1 3.12 0,17 HAA OOu An B^NAD ni01 ITNA o4CnA no 1 vc 1 3.62 0,52 ITNA QCCI ILI niUl ITNA 85 SUN ni t 01 1 ITNA OC/^ Al 1 n/ 1 Oh I Si (%) ITNA OUTUU ni 1 01 1 ITNA 79CAH 01 1 3.1 0.14 CPXRF OfW T D BOKIR ni01 UXRF 82MIL n 1 1 01 1 5.5 0.4 34 AA B3BcT ni01 5.68 0.01 ICPES Q/ LI An BhNAD niUl

5.7 34 AA Book 1 niUl

5.8 0.1 D TCGS on A ftm BOAND ni01 CPXRF oOKIR 01 1 5.8 0.1 TCGS 70C A f Ul

ICPES 85HAR 01 1 5.8 0.1 D TCGS 80GER 01 ITNA 82JER 01 1 5.9122 0.0187 ICPES 85PEA 01 ITNA 81KUL 01 1 5.92 0.01 XRF 79CAH

ITNA 85SUN 01 f 1 6.05 0.2 TCGS 79AND 0\ ITNA 85AKA 01 1 6.09 0,07 ICPES 82NAD 02

ITNA 85GAU 04 1 6.21 0,08 AA 82NAD 02

1 1632A-11

27.79 EXRF 82EBD 02
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRM 1632A (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

1 (ug/q) Tb (nsi/g)

1.1 0.1 UNA 80KOS 01 1 290 30 ITNA 81 JIN A401

1.9 0.1 5 UNA 80TOU 01 1 290 60 ITNA 86GLA 01

2 34 WXRF 82MIL 01 1 300 ITNA 85GRE AO02

2.1 0.05 TCGS 79AND 01 1 300 100 ICPES 82CRO A 4 01

2.1 0.07 TOGS Tor A r 7VFAI 01 1 310 30 ITNA 84SUZ 02

2.1 0.07 D TCGS DAAUn f)1 1 U1 1 320 50 ITNA OOGcR 01

2.1 0.07 D TCGS 80GER 01 1 330 40 ITNA 79CAH A

1

01 2.2 0.1 ITNA 85AKA 01 1 330 40 ITNA 85 SUN 01 2.28 0.08 ITNA B3GAU Oh 1 330 120 ITNA S4CHA AO02

2.4 ITNA 85GRE Od \ 2.4 0.05 ITNA 03SUN 01 1 Te Cng/q)

2.5 0.4 ITNA OUbAK ni 1 U1 1 2.57 0.09 ITNA oUD i 1 t u

IN U1 1 < 600 L WXRF OOU t 1 OcMIL A101 2.6 0.1 ITNA 79CAH 01 1 < 830 ITNA 84SUZ 02

2.6 0.1 ICPES o^CRO 01 1 500 50 HAA 82NAD A101 2.62 0.13 ITNA 830BR 01 1 2.7 2 ITNA 83JER 01 1 Th (ug/g>

2.8 0.3 ITNA 80GER 01 1 3.1 0.3 ITNA 84SUZ 02 1 3.1

3.77

0.5

0.38

CPXRF

ITNA

80KIR

84CHA

01AO02

(uq/q) 1 4.2

4.2

0.2

0.3

5 ITNA

ITNA

80TOU

79cAH

01

A101

1 34 WXRF 82MIL 01 1 4.3 ITNA 82JER 01 2.3 FAA ohLON 01 1 4.3 0.3 ITNA oOKOS Ai

8.08 1.02 HAA 01 1 4.3 0.9 ITNA OiKUL Al01 84.2 2.6 ITNA 03SUN 01 1 4.4

4.4

0.1

0.5

ICPES

ITNA D/ CI 17 BhSUZ

(ug/g) 4.48

4.5

0.04

0.02

ITNA

lENA

81JIN

85BEL

At01

Af01 60 1 ICPES 84NAD 01 1 4.5 0.3 ITNA 85AKA A401 76.4 12.8 ITNA 85SUN 01 1 4.6 0.2 ITNA 86GLA A<l 01 79 9 ITNA 82JER 01 1 4.63 0.07 ITNA 85 SUN A401 80 11 ITNA O/ Tl 1 84TU 01 1 4.8 0.2 ITNA SOGER Af01 83.6 7.8 ITNA 830BR 01 1 4.8 0.6 ITNA SOGAR 01 84 2 ICPES DC U A D 01 1 4.81 0.17 ITNA DC/* Al 1 BsGAU A/Oh

84 9 ITNA SOGER 01 1 5 34 WXRF S2MIL 01 90 34 WXRF 82MIL 01 1 91 18 ITNA 79CAH 01 1 Th-228 (pCi/g)

95.5 11.8 ITNA 81JIN 01 1 0.499 0.011 D NM 81 CAS 01 (ng/q) 0.499 0.011 NM SOCAS 01

290 50 ITNA S4CHA 02 1 Th-230 (pCi/g)

360 10 ITNA S4SUZ 02 1 390 50 ITNA 85GAU 04 1 0.452 0.017 NM SOCAS 01 390 50 ITNA 79CAH 01 1 0.452 0.017 D NM 81 CAS 01 400 30 ITNA SOGER 01 1 450 40 ITNA S5SUN 01 1 Th-232 (DCi/g)

450 50 ITNA 81JIN 01 1 460 30 ITNA S4TU 01 1 0.40 0.07 GAMMA 84R0S 03

460 90 ITNA 85AKA 01 1 0,484 0.018 NM SOCAS 01 0.484 0.01S D NM 81 CAS 01 1632A-12
TABLE 1632A- 2: INDIVIDUAL DATA FOR NBS SRM 1632A (cont.

)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

i

Ti (ua/g) U (ug/g) cont •

592 30 I OPES 84NAD 01 1 1.29 0.04 DNA 85GAU 04

1310 20 ICPES 85HAR 01 1 1.29 0.07 DNA 86GLA 01 1437.6 119.8 ICPES 85PEA 01 1 1.3 0.02 ICPES 83MAH 05

1480 30 TCGS 79AND 01 1 1.3 0.1 35 DNA 81GLA 04

1550 40 D TCGS 80GER 01 1 1.3 0.11 ITNA 830BR 01 1550 40 D TCGS 80AND 01 j 1.3 0.12 ITNA 85SUN 01 1550 40 TCGS TyPAI 01 1 1.31 0.09 ITNA 82JER 01 1560 70 ITNA 83JER 01 1 1.33 0.04 DNA 86GAU 01 1570 100 ITNA 86GLA 01 1 1.4 DNA 84GLA 11 1580 80 ITNA ni 1 U1 1 1.45 0.05 35 DNA 81GLA 03

1600 34 UXRF o^nl L U1 1 1.5 0.13 ITNA 04CHA 02

1600 40 ICPES O^NAU no 1

1620 45 ITNA ojUoK Ul 1 U-234 (DCi/q)

1630 ICPES oinbR Uo j 1630 70 ITNA oUGER U1 1 0.448 0.012 D NM 81 CAS 01 1700 50 ICPES 83MAH 05 1 0.448 0.012 NN 80CAS 01 1700 300 CPXRF 80KIR ni 1 01 1 1720 170 ITNA 80GAR 01 1 U-235 (fCi/g)

1756 128 ITNA 85SUN 01 1 1760 AA 82NAD no 1 UC \ 22.8 1.9 D NM 81 CAS 01 1800 100 XRF TOPAU f VLAH U 1

1 22.8 1.9 NM OULAo niU 1 1800 300 34 COLOR O^DC 1

1 1900 34 COLOR 03BET U1 1 U-238 (pCi/g)

2230 WXRF ojGAR ni 1 Ul 1 5990 EXRF odcou 0.444 0.016 NM oULAb niU 1 0.444 0.016 D NM D1 C 01 CAS Ul

Tl (uq/g)

V (ug/g)

< 1 L WXRF 82MI

n 1 1 01 1 37.4 3.1 11 AA 82LIN 03

Tm (nq/ci) 39 2 ITNA Q7 ICQ Ul

40.5 0.9 ICPES 85HAR n 4 01

< 1000 L WXRF 82MIL 01 1 41 2.05 AA 82KAM 01 380 40 ITNA 84SUZ 02 1 41.6 2.2 ITNA 85 SUN ni01 400 100 ICPES 82CR0 01 1 42 2 ICPES S3MAH nc

42 2.4 11 AA 82LIN 03

U (ug/g) 42 4.2 FAA 80LAN 01 43 34 UXRF OOu t 1 oZMiL 01

1 34 WXRF 82MIL 01 1 43 1 ITNA oo tco ni

1.1 0.2 ITNA 79CAH A 1 1 01 1 43 4 AA OlD An A1U 1 1.12 0.4 ITNA 81KUL 01 1 43.4 1.8 ITNA ooOBR 01 1.14 0.07 ITNA 84SUZ m 1

1 44 ITNA niU 1 1.16 0.11 ITNA 81JIN A 4 1 01 1 44 3 ITNA OUGcR U1

1.2 0.1 5 ITNA 80TOU A 4 1 01 1 44 7 11 AA O/ U A^ ohNAK Ul

1.21 0.1 ITNA 80GER A4 1 01 1 44.3 ICPES D1 UCQ olMcK U3

1.22 0.1 ITNA 83JER 01 1 45 2 ITNA 84GLA 02

1.24 0.04 lENA 80KOS 01 1 45.5 1.6 11 AA 84NAK 01 1.24 0.1 lENA 81KUL 02 1 46 34 FAA 83BET

1.26 0.08 DNA 84GLA 02 1 46 6 AE+AF 82G0L f01 1.28 0.02 lENA 85BEL 01 1 46 2 ITNA 86GLA 01

1.28 0.08 DNA 80GAR 01 1 46 8 34 FAA 83BET 01

1632A-13
TABLE 1632A-2: INDIVIDUAL DATA FOR NBS SRH 1632A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

V (uci/g) cont

1

1

1

Zn (ug/g)

46 8.2 CPXRF 80KIR 01 1 19 4 ITNA 86GLA 01 46.9 2.5 ITNA 80GAR 01 1 24.3 4 AA 79CAH 01 48 7 6 AE-t-AF 82G0L 01 1 25 2 ITNA 84CHA 02

49 ITNA 85GAU 04 1 25 3 34 FAA 83BET 01 49.6 1.7 11 AA 82LIN 03 1 26 0.7S AA 82KAM 01 67 3 ICPES 84NAD 01 1 26 1 XRF S5HAR 01

1 26.6 0.1 11 AA 82LIN 03

U (ng/g) 1 27 6 ITNA 79CAH 01

1 27.1 ICPES 81MER 03

600 200 ITNA SOGER 01 1 27.5 3 AA S3RAP 01 780 230 ITNA 830BR 01 1 27.6 1.8 11 AA S4NAK 01 790 20 ITNA &4SUZ 02 1 27.6 2.4 11 AA 84NAK 01 890 150 ITNA 81JIN 01 1 27.7 1.4 11 AA S2LIN 03

920 150 ITNA 85SUN 01 1 28 34 WXRF 82MIL 01 1000 300 ITNA Ton A U Ul 1 28 0.4 ICPES S3MAH 05

28 1 ICPES 85HAR 01 Y (ug/q) 1 28 2 ITNA 83JER 01

1 28 3.7 CPXRF SOKIR 01 5.8 0.5 PAA SOGER 01 1 29 34 FAA S3BET 01 8.3 0.5 ICPES 82CR0 01 1 30 3 ITNA SOKOS 01 9.5 34 UXRF S2MIL 01 1 31 6 ITNA SOGER 01 9.7 0.4 ICPES 85HAR 01 1 39 8 ICPES 84NAD 01

Yb (ug/q)

1

1 Zr (ug/g>

0.9 0.01 ICPES S2CR0

1 01 1 < 140 ITNA S6GLA 01 0.98 0.07 ITNA S1JIN 01 1 47 6 ITNA SOGER 01 0.98 0.08 ITNA SOGER 01 1 55 34 UXRF 82MIL 01 1.04 0.17 ITNA 85SUN 01 1 57 5 PAA SOGER 01 1.09 0.06 ITNA 85GAU 04 1 1.1 ITNA 85GRE 02 1 1.1 0.1 5 ITNA SOTOU 01 1 1.13 0.07 ITNA 86GLA 01 1 1.14 0.2 ITNA 84CHA 02 1 1.19 0.06 ITNA 84SUZ 02 1 1.2 ' 0.1 ITNA 79CAH 01 1

1632A-14
TABLE 1632B-1: COHPILED DATA FOR NBS SRM 1632B TRACE ELEMENTS IN COAL

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

ASH % 6.79 ± 0.16

Al ug/g 8550 ± 190

As ug/g 3.72 ± 0.09

Ba ug/g 67.5 ± 2.1 Br ug/g 17

C-Total X 78.11 ± 0.37

Ca ug/g 2040 ± 60

Cd ng/g 57.3 ± 2.7

Ce ug/g 9

CI ug/g 1260

Co ug/g 2.29 ± 0.17

Cr ug/g 11 Cs ng/g 440

Cu ug/g 6.28 ± 0.30

Eu ng/g 170

Fe ug/g 7590 ± 450

H % 5.07 ± 0.06

Heat BTU/lb 14005 ± 35

Hf ng/g 430

K ug/g 748 ± 28

La ug/g 5.1

Li ug/g 10

Mg ug/g 383 ± 8

Mn ug/g 12.4 ± 1 Mo ug/g 0.9

N % 1.56 ± 0.07

Na ug/g 515 ± 11

Ni ug/g 6.10 ± 0.27

Pb ug/g 3.67 ± 0.26

Rb ug/g 5.05 ± 0.11

S % 1.89 ± 0.06

Sb ng/g 240

Sc ug/g 1.9

Se ug/g 1.29 ± 0.11

Si % 1.4

Sm ug/g 0.87

Sr ug/g 102

Th ug/g 1.342 ± 0.036

Ti ug/g 454 ± 17

U ng/g 436 i 12

V ug/g 14

Volatile % 35,4 ± 1.1 W ug/g 480

Zn ug/g 11.89 t 0.78

1632B-1
5

*^ ^ ^ ^ r- t/t &. U. — r- l/> «i Hi

8 S

ac

S 5

f • <^ t/t N

•- ro ru

S kr\ o- s o in

tn O Kl O (M S t/s o- o rsj CO o • *4 ' M • *- >» W < S ^ .X

ru §f>i 2o ° IS

t>4 w w8 rsl o

8 : S

<0 lA

Kt <M -#

a

3 - S ; ^ : O K> Kt <0

4* r4 ** -H to M ~ 5 S S

s c s

o o

I M

•- CD

--

O CO OO >0 o d $ *-* o o o »- -o

• fSJ f\» N. • • '

O O

-M «4

0--•— in oo o i/> in

LA ro CO tn-sfo- tn^'C eo-O -Q o-^-nj-'" Ki---*«-Min--

to 'O Lno o»-Kcoinf>j<M

•- (M nj Ki Kt

«0 -J ^ (D fM (M OOOJO'iiCDO'OfMOmKl^m • tn rvKiin ^ v_ f\; rom

O • ITi >0 • .... un O ^ <NI IMnJOOO

o^^ fvi-«* in^rg-*K>inN. o • o • -o < • • • -o KiiM in>* -ocNJ to r<% • '

CO

. o M rj -o in-orijfOKitnO>«-m OJ • O • • » ^ rg ro

o o J o ^ d ^

•- oo o. o nj -o rg

rtj o 'O o •

• • rg « oo »- K) Kt M «- o ^- o ^

O. Kl »- in M

• ooo ^ •in 'Oaon-o-f

•o • ^ m •

K ^ ^ »M ^ ; 8

o m <D

rg •- m « tn in >n ^ in

-O »- fg

• « • o *- o -o o o o »- — O O (M tn

-J- fO rg

<o ^ O « O «

fM fw fw K

R S

'

Ql O) O

. T «

o o w <<<«<<(0(Dma)CDcaui.JUOuo(_)U(_>c-)uuaujiuu->*-u.O(.30xxzx

^ f\J M — aoico xoo

1633-1
St

1 S

»- f

° I

rg

8: S

3C3CXXZX3CX

*rt V> C/> S S 5 (/>»(/) — rs» r*i

S » <t

5 8 2 S I J

i\j fM m tvj

s s <» ? ^ 5

K» rg

5010 8.3

22.7

1

0.

18.5 5.7

ii if

i i i § S H IS ^ X X X o v> v> H. S 1 S »-

M CA </> t/> < </» I/) S S UJ S S C/) (A < </> <A

f>J fM ^

O O

^ o (M rsi

fM O O « O ^ >» g

O- in K Ki 1^ ^. S -

o Fi. o

C\t CM M (M m

t ° g

<V in O •O • O M o a rg «

iM w- w~ r>i

^ 2 ; 3

m oi m SO

O CO o* tn fM o • rvi 41 fM »-

Kt fM m

fM fM fM <M (\J O

m in

• m ro •

5 « O O

CO o r<-

'O ty o p o

fM 5>

3 o o

CO eo

tsi • O

fM (NJ *-

fM m

o m eo m fM • • fl6 in «- «- m 00 o o o • rj fM o rO »M fM O o m po o>

. • S

" -

. o ^- in

. m -

m '« fM CM fM

fM 'O • CM ^ -O fM

«j- >» m '- CO oU 1)

fM %0 O

a 3 §

o CO o in o • M *< fM o m 00 o to o omooo*— lACOoo

. o • • g Ki ^ m m o o

fM -J- s s

o 00 tn

(M M fM o o m CO O • PO • sc oo -* m fM • « I", fM >» -O fM

cn O^ 9) o o)

0> Q>

O) tn oi 0)0)QlO>0)0)01V> Q) 0> O) ^ O) Ol O) O) CT> O^ O) Ot O) 0» O) Ol SI O) D> O) 0> V

z O O tl. o.

O

3 (rt (/> (/)

1633-2
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

3 (nfl/g)

1

1 Al (%) cont.

< 100 L ITNA 77CHA

1 01 1 12.99 0.47 ICPES 81CHU 01 < 100 D ITNA 78RYA 01 1 13 0.2 TCGS 79AND 01

< 300 L ICPES 81CHU 01 1 13 2.6 OES 76WEW 01

< 400 D PAA 77CHA 01 1 13.6 0.5 14NAA 81WIL 01

< 400 L PAA 76CHA 01 1 14 OES 78SUG 01

< 500 L UU 80HEN 01 1 14 1 AA 80STO 02

< 600 L lENA 80GLA 03 1 14.1 2.8 ITNA 81UAN 01

< 1000 L OES 76WEU 01 1 14.3 1.1 ITNA 78NAD 02

258 20 RTNA 77NAD 02 1 14.3 1.1 ITNA 75NAD 02

300 SSMS 83UEI 02 1 350 AA 76UEU 01 1 As (uq/g)

320 130 PAA 74CHA 01 1

1 46 ITNA 78KEL 02

(%) 1

1

49

50

5 6

ITNA SSMS76KUC 01 78GUI 01 10.4 0.6 ITNA 78MAC 01 1 54 ITNA 75KLE 01 10.96 0.402 ITNA 73SHE 01 1 54 1 lENA 78UAN 01

11.1 0.6 ICPES 85HAR 01 1 54 3 ITNA 78MAC 01 11.6 ICPES 80NAD 01 1 55 FAA 78GUI 01 11.7 2 XRF 79SMI 01 1 55 10 ICPES 81CHU 01 11.8 0.8 ITNA 76BL0 01 1 55.8 1.4 H AE+AF 77FEL 01 11.9 ICPES 84CLE 01 1 56 ICPES 80FLO 01

12 1 ITNA 760ND 01 1 56 1 H FAE 79FEL 01

12.1 0.5 ITNA 76RAG 01 1 56.6 3.6 ITNA 81UAN 01 12.2 0.3 ITNA 77MAE 01 j 57 ICPES 82NYG 01 12.2 0.5 14NAA 81WIL 02 1 57 3 35 NAA 81GLA 03

12.3 35 TCGS 78GLA 04 1 57 4 ITNA 750ND 01 12.3 0.5 ITNA 76WEW 01 1 58 13 ICPES 84B0T 01 12.3 0.6 D ITNA 78RYA 01 1 58 1 ITNA 76BL0 01 12.3 0.6 ITNA 77CHA 01 1 58 1 35 RTNA 78GLA 02

12.35 0.25 ITNA 76STE 05 1 58 2 lENA 76STE 05

12.35 0.25 ITNA 77R0W 03 1 58 4 D NAA 740ND 01 12.4 0.3 D NAA 79STE 01 1 58 4 FAA 78HAY 01 12.4 0.7 35 ITNA 81GLA 03 1 58.1 1.6 RTNA 81GAL 01 12.5 ITNA 75KLE 01 1 58.1 1.6 D RTNA 81 GAL 02

12.5 0.3 ICPES 80NAD 01 1 59 ITNA 78WEA 01 12.6 0.1 35 ITNA 81GLA 02 1 59 2 35 W 81GLA 04

12.6 0.2 ICPES 84B0T 01 1 59 3.5 HAA 77SMI 01 12.6 0.2 TCGS 79FAI 01 1 59 4 ITNA 77CHA 01 12.6 - 0.2 D TCGS 80AND 01 1 59 4 D ITNA 78RYA 01 12.6 0.4 ITNA 73ABE 01 1 59.1 4.8 lENA 77R0W 04

12.6 0.7 AA 760ND 01 1 59.8 2 lENA 77R0W 03

12.7 UU 80HEN 01 1 60 UU 80HEN 01 12.7 OES 80WAL 01 1 60 2.6 D PAA 77CHA 01 12.7 ITNA 78WEA 01 1 60 2.6 PAA 76CHA 01 12.7 AA 70c T 1 ni 1

1 60 2.6 NAA 77JER 01 12.7 0.05 FAA 77PIL 01 1 60 3 GCMES 75TAL 01 12.7 0.5 ITNA 750ND 01 1 60.4 0.8 35 lENA 80GLA 03

12.7 0.5 ICPES 84NAD 01 1 60.7 2.6 PAA 74CHA 01 12.8 ICPES 80FLO 01 1 61 SSMS 83WEI 02

12.8 0.3 ITNA 78LAU 02 ' 61 3 RTNA 740RV 01 1633-3
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

As (ug/g) cont.

61 4 ITNA 760ND 01

61 5 ITNA 73ABE 01

61 6 ITNA 84SIL 01 61.2 FAA 75P0L 01 61.5 2.4 D NAA 79STE 01 61.5 2.4 ITNA 77R0W 04

61.5 3 PAA 750ND 01 62 XRF 78CAM 02

63 4 6 PAA 82SEG 01 63 4 PAA 80SEG 01 63 4 FAE 80DSI 01 63 4 ITNA 85FIL 01 63 4 6 PAA 82SEG 01 63 7 EXRF 77GIA 01 63.7 3.6 HAA 82NAD 01 6A FAA 84SIL 01 64 1 PAA 76KAT 03

64 2 ITNA 78LAU 02

64 4 ITNA 76RAG 01 65 1 PAA 76ICAT 02

OO 1 AK r 70cm I U 1 66.3 10.1 FAA 82BEN 01 67 6 0 6 ITMA i 1 nn 75NAD 02

68 6 ITNA 78NAD 02

68 12 14NAA 81UIL 02

68 12 14NAA 81WIL 01 68 15 ITNA 76UEW 01 69.5 7.6 ITNA 73SHE 01 72 6 SSMS 78GUI 01 74 13 ICPES 84B0T 01

(ng/g)

< 300 L ICPES 81CHU 01 < 500 L UU 80HEN 01 2.75 0.2 RTNA 77NAD 02

4.84 0.13 RTNA 77NAD 01 8 2 D ITNA 78RYA 01 8 2 ITNA 77CHA 01 700 ITNA 78WEA 01

1633-

Cone Uncer Com Method Reference

100 UU 80HEN 01 320 COLOR 790AL 01 340 OES 79DAL 01 407 ICPES 80NAD 01 433 4 D TCGS 80AND 01

433 4 TCGS 79FAI 01 443 5 TCGS 79AND 01 450 20 ICPES 820UE 01 49Q 14 6 TCGS ^6GLA 01 492 13 6 TCGS 76GLA 01 O 1 Liib f DuLA U

1

500 29 OES 76UEW 01 600 SSMS 83WEI 02

a (ug/g)

1800 XRF 76WEW 01 2100 100 14NAA 81UIL 01 2100 200 ICPES 84NAD 01 2300 100 AA 76ON0 01 2370 ICPES 80NAD 01 2490 ITNA 75MIL 01 2500 UU 80HEN 01 2500 250 ITNA 81 WAN 01 2500 300 ITNA 76UEU 01 2510 50 lENA 77R0W 04

2510 160 ITNA 76RAG 01 2510 200 ITNA 760ND 01 2520 AA 79SIL 01 2540 ICPES 84CLE 01 2540 XRF 78CAM 02

2540 50 lENA 77R0W 03

2540 50 D NAA 79STE 01 2540 51 lENA 76STE 05

2550 30 ITNA 77R0W 04

2550 30 D NAA 79STE 01 2550 110 14NAA 81WIL 02

2580 170 ITNA 76STE 05

2600 160 D PAA 77CHA 01 2600 160 PAA 76CHA 01 2600 170 5 lENA 80GLA 03

2600 300 ITNA 78LAU 02

2610 210 PAA 74CHA 01 2630 20 XRF 79SMI 01 2660 150 ITNA 84GLA 02

2670 85 EXRF 77GIA 01 2700 ITNA 78UEA 01 2700 200 ITNA 78NAD 02|

2700 200 ITNA 750ND 01 2700 200 ITNA 75NAD 02

2710 190 D ITNA 78RYA 01

f
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

Ba (ug/g) cont.

2710 190 ITNA 77CHA 01 2720 80 5 lENA 80GLA A703

2734 167 ITNA 73SHE Ai01 2750 140 5 lENA 80GLA 03

2780 ITNA 75KLE A 4

2800 ICPES 80 FLO A 4 0

2800 ^ A60 ITNA OC r r 1 85FIL niU1 2800 4 AA 100 35 ITNA 81GLA 03

2800 100 9 ITNA 78LAU A102

2800 200 ICPES 85HAR A 4 01 2800 200 35 ITNA 81GLA 02

2840 180 35 NAA 81GLA 04

2860 70 ICPES 84B0T 01 2880 100 ITNA 77MAE 01 2900 4 '>A 120 FAA 760WE A 4 01 OAAA 2900 AA 200 5 lENA 80GLA 03

7AAA 3000 SSMS 83UEI m02

3000 OUU OES 76WEW U1 3^00 / nn UVQ I TNA /oMAC niU1 3hU0 I TNA / I ADC Ul

Je (ug/g)

c3

III 1 UU 80HEN 01 FAA 75P0L 01

lU. 1 o

C A A FAA 79GEL 01 lu.y ICPES 80NAD 01

i i

1

ICPtS 80 FLO 01

i 4

1

ucS 78SUG ni

i i o ft 1 U.o ICPES 84B0T n i 01

1

A A AA 79SIL n i 01 ic A A AA 76WEW n i 01 19 n Q U.o C A A FAA 75OWE n i 01 13 1

1 C A A

f OGLA no0<: 15 1 ZO

C A A FAA 79GEL n i 01 12.3 0.3 FAA 760WE 01 12.4 0.31 AA 74RAI 01 12.6 6 FAA 79GEL 01 12.6 0.25 ICPES 81CHU 01 12.6 0.5 AA 760ND 01 13.2 6 FAA 79GEL 01 13.5 6 FAA 79GEL 01 14 0.95 OES 76WEU 01 15 ICPES 84CLE 01 18.7 0.5 ICPES 84NA0 01

I 1633-5

Cone Uncer Com Method Reference

Bi (ug/g)

< 1 L PAA 76CHA A 4 01 < 1 D PAA 77CHA A 4 01 <

4 A10 L OES 76WEW A401 0.7 UU 80HEN n i 01

i no

1 .08 PAA 74CHA n i 01 4.5 SSMS 83UEI 02

(ug/g)

3.8 0.8 35 lENA 79GLA AO02

6 ITNA TsKLE A 4 01 6

i

1 ITNA 78MAC A 4 01 6 2 EXRF 77GIA 01 6.4 A0.2 35 ITNA 81GLA AT03

6.5 A 1 0.2 5 lENA 80GLA 03

6.7 A ^ 0.6 ITNA 76RAG 01 o.y n 7 0.3 35 NAA 81GLA A/04

i

1 ITNA 78LAU AO02

n c 0.3 ITNA 78NAD 02

7 Q9 ft /it 1 TU A

1 TNA 7Ckl AfN

r 3NAD no02

f .1 1 c 1.3 lENA /^OSTE nc03

1 .D T CLI A lENA 77R0W 03

y .£ ft Ji u.o ITNA 7'7ROW 04

9.2 0.6 D NAA 79STE 01 9.2 0.8 lENA 77R0W 04

9.5 XRF 78CAM 02

10 UU 80HEN 01

11 . i 7 C D ITNA 78RYA A 4

i 1 1 1 .<: ITNA 77CHA A 4 01 12 ITNA 78WEA 01 12 4 ITNA 750ND 01 12 4 ITNA 73ABE 01 12.1 1.5 ITNA 73SHE 01

3.U!> ft ftC 0.03 CB 79s I

A 4

3.3 UU SOMEN A 4 01 3.4D ft fto 0.02 GRAV 79s I

n i 01

1.15 0.02 AA 82HAR 01 3.5 XRF 76UEU 01 3.8 35 TCGS 78GLA 04

3.92 0.28 PAA 74CHA 01 4.1 0.36 ITNA 73SHE 01 4.2 UU 80HEN 01 4.2 0.2 ITNA 76RAG 01 4.21 0.09 ITNA 75NAD 02

4.21 0.09 ITNA 78NAD 02
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Utx;er Com Method Reference

Ca (%) cont.

4.3 AA 79SIL 01 4.3 0.2 AA 760ND 01 4.3 0.3 35 ITNA 81GLA 02

4.34 ITNA 75KLE 01 4.4 0.18 14NAA 81UIL 02

4.4 0.4 D PAA 77CHA 01 4.4 0.4 ITNA 750ND 01 4.4 0.4 PAA 76CHA 01 4.5 ICPES 80FL0 01 4.5 0.05 ICPES 85HAR 01 4.5 0.5 D ITNA 78RYA 01

4.5 0.5 ITNA 77CHA 01 4.5 0.6 35 lENA 80GLA 03

4.54 0.06 ICPES 84B0T 01 4.6 EXRF 78WEG 01

4.6 0.5 ITNA 78LAU 02

4.62 0.06 ICPES 80NAD 01 4.62 0.15 EXRF 78PEL 01 4.65 0.15 ICPES 81CHU 01 4.69 0.14 D NAA 79STE 01 4.69 0.14 ITNA 77R0W 03

4.69 0.14 ITNA 76STE 05

4.7 OES 80WAL 01 4.7 0.3 ITNA 77MAE 01 4.73 0.42 ITNA 81 WAN 01 4.75 0.08 D TCGS 80AND 01 4.75 0.08 TCGS 79FAI 01 4.8 ICPES 80NAD 01 4.8 0.96 OES 76WEW 01 4.81 ICPES 84CLE 01 4.9 0.2 AA 80STO 02

4.9 0.2 TCGS 79AND 01

5 1.1 ITNA 760ND 01 5.04 XRF 78CAM 02

5.09 0.56 14NAA 77VAN 01

5.1 0.03 PAA 76ICAT 02

5.1 0.05 PAA 76KAT 03

5.1 0.6 ITNA 76WEW 01

5.11 0.13 XRF 79SMI 01

5.21 0.2 ICPES 84NAD 01 5.3 0.1 EXRF 77NIE 01 5.3 0.5 PAA 750ND 01

Cone Uncer Com Method ReferencCi

Cd (ug/g)

0.93 POT 82CHR 01

1 ITNA 76UEU 01 1.2 0.04 7 AA 73TAL 01 1.2 0.04 FAA 74TAL 01 1.2 0.1 6 PAA 82SEG 01 1.2 0.2 6 PAA 82SEG 01 1.2 0.2 PAA 80SEG 01 1.3 0.25 FAA 760UE 01 1.38 0.14 FAA 79G00 01 1.4 0.16 TCGS 79AND 01 1.43 FAA 78GUI 01 1.43 0.04 RTNA 740RV 01 1.43 0.07 D RTNA 81 GAL 02

1.43 0.07 RTNA 81GAL 01 1.45 FAA 75POL 01

1.45 0.04 AA 75EPS 01 1.45 0.06 RTNA 84DEL 01 1.46 AE+AF 77FEL 01 1.46 0.05 AA 74RAI 01

1.5 POL 74MAI 01

1.5 0.07 TCGS 79FAI 01

1.5 0.07 D TCGS 80AND ol

1.5 0.09 7 AA 73TAL 01

1.5 0.09 FAA 74TAL 01

1.5 0.1 NAA 77JER 01

1.5 0.1 D PAA 77CHA 01

1.5 0.1 PAA 76CHA 01 1.5 0.15 FAA 74RAI 01

1.5 0.5 ICPES 81CHU 01 1.52 0.07 PAA 74CHA 01 1.52 0.08 AF 75EPS 01 1.53 AA 76UEU 01 1.55 FAA 79SIL 01 1.6 0.15 7 AE+AF 73TAL 01 1.6 0.15 FAE 74TAL 01

1.6 0.2 6 TCGS 76GLA 01 1.6 0.5 ICPES 80EPS 03

1.63 0.07 8 SSMS 80KOP 01 1.69 AA 78GEL 01 1.7 0.2 AA 760ND 01

1.85 IDMS 75ICLE 01

2.2 0.6 13 ICPES 84B0T 01 9.5 13 ICPES 84B0T 01

15 UU 80HEN 01

1633-6
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

125 UU 80HEN 01 129 10 ITNA 73SHE 01 136 5 UNAA 81WIL 01 136 8 14NAA 81UIL 02

140 ICPES 80FLO 01 140 10 D ITNA 78RYA 01 140 10 ITNA 77CHA 01

141 7 ITNA 81WAN 01 145 5 ITNA 78LAU 02

145 6 ITNA 76UEU 01 146 ITNA 82GLA 02

146 15 ITNA 750ND 01 146 17 ITNA 760ND 01 148 6 ITNA 76RAG 01 148 7 35 ITNA 81GLA 02

149 4 XRF 79SMI 01 149 7 35 NAA 81GLA 04

149.6 2 ITNA 77R0W 03

149.6 2 D ITNA 77R0W 04

150 2 D NAA 79STE 01 150.6 3.3 lENA 77R0W 04

152 10 D PAA 77CHA 01 152 10 PAA 76CHA 01 152 15 ITNA 85FIL 01 153 1 PAA 76KAT 02

153 2 PAA 76KAT 03

153 3 35 ITNA 81GLA 03

153 4 ITNA 840DD 01 153 6 RTNA 840DD 01 154 XRF 78CAM 02

154 8 35 lENA 80GLA 03

157 3.2 ICPES 81CHU 01 160 23 EXRF 77GIA 01 161 35 ITNA 78NAD 02

161 35 ITNA 75NAD 02

169 ITNA 75MIL 01 176 4 ITNA 78MAC 01 200 100 OES 76UEU 01 210 SSMS 83WEI 02

210 34 SSMS 78SUG 02

I 1633-7

Cone Uncer Com Method Reference

19.6 0.1 PAA 74CHA 01 20 2 ITNA 78NAD 02

20 2 ITNA 75NAD 02

25 7 PAA 76CHA 01 25 7 D PAA 77CHA 01 32 10 ITNA 77CHA 01 32 10 D ITNA 78RYA 01 40 8 ITNA 78MAC 01 40.6 14.4 ITNA 83LI 01 42 SSMS 83UEI 02

42 ITNA 78WEA 01 42 10 ITNA 750ND 01 50 UU 80HEN 01 52 15 ITNA 81 WAN 01 56 35 ITNA 81GLA 03

58 9 ITNA 77MAE 01

185 44 ITNA 73SHE 01

(ug/g)

25 3 ICPES 34NAD 01 26 ICPES 80NAD 01 32 1 ICPES 84B0T 01 32 2 AA 77MIT 01 35 2 ITNA 76KUC 01 35.4 2.8 PAA 74CHA 01 36.2 1.1 ITNA 76BL0 01 36.7 3.9 ITNA 75NAD 02

37 4 ITNA 78NAD 02

38 ITNA 78UEA 01 38 SSMS 83WEI 02

38 0.96 OES 76UEU 01 38 1 ITNA 85FIL 01 38 2 35 lENA 80GLA 03

38 2 ITNA 78MAC 01 38.6 3.7 ITNA 73SHE 01 39 AA 76WEW 01 39 2 ICPES 85HAR 01 39.4 1.2 ITNA 76RAG 01 39.8 0.9 ITNA 81UAN 01 40 2 35 NAA 81GLA 04

40 2 PAA 76CHA 01 40 2 ITNA 760ND 01 40 2 ITNA 73ABE 01 40 2 D PAA 77CHA 01 40 4 PAA 760WE 01 40.1 0.6 ITNA 84GLA 02

40.3 0.4 ITNA 77R0W 03

40.3 0.4 D NAA 79STE 01 40.3 0.4 D ITNA 77R0W 04

41 ICPES 80FLO 01
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

) (ug/g) cont.

41 0.6 lENA 77R0W 04

41 1 ITNA 78LAU 02

41 1 35 ITNA 81GLA 02

41 1.2 ICPES 81CHU 01

41 2 35 ITNA 81GLA 03

41 3 ITNA 76WEW 01 41.5 1.2 ITNA 750ND 01 42 FAA 79SIL 01 42 ITNA 75MIL 01 42 1.6 ITNA 77CHA 01 42 1.6 D ITNA 78RYA 01 42 3 PAA 76KAT 02

42 5 PAA 76ICAT 03

42 6 AA 760ND 01 45 16 14NAA 81WIL 01 45 16 14NAA 81WIL 02

46 ITNA 75KLE 01 46 10 AA 82HAR 01 48 I TNA 84CLE 01 50 UU 80HEN 01 54 ICPES 84CLE 01

• (ug/g)

96 ICPES 84S03 01 103 10 AA 82KAR 01 104 4 ICPES 84NAD 01 110 ICPES 84CLE 01 112 XRF 78CAM 02

113 FAA 78GUI 01

113 1.5 ITNA 75NAD 02

113 2 ITNA 78NAD 02

114 ICPES 80NAD 01 117 6 SSMS 78GUI 01 117 7 ITNA 76RAG 01 118 6 ITNA 760ND 01 118 8 ITNA 76UEU 01 120 OES 78SUG 01 120 4 AA 760ND 01

120 5 ITNA 78MAC 01 120 6 ICPES 85HAR 01 122 12 ITNA 73SHE 01 123 ICPES 80FLO 01 124 9 ITNA 85FIL 01 124 14 XRF 79SMI 01

125 9 ICPES 84B0T 01 126 11 ITNA 76BL0 01 127 6 D NAA 740ND 01 127 6 ITNA 750ND 01 128 ITNA 78WEA 01 128 AA 79SIL 01 1633-

Conc Uncer Com Method Reference*

Cr (ug/g) cont.

128 5 35 ITNA 81GLA 02

128 5 35 ITNA 81GLA 04

128.5 8.5 AA 77MIT 01 129 3 D NAA 79STE 01 129 3.9 ICPES 81CHU 01 129.2 2.7 ITNA 77R0W 03

129.2 2.7 D ITNA 77R0W 04

130 AA 76UEU 01 130 SSMS 83UEI 02

130 UU 80HEN 01 130 4 ITNA 84GLA 02

130 5 9 ITNA 78LAU 02

131 EXRF 78WEG 01

131 6 PAA 76CHA 01

131 6 D PAA 77CHA 01

131 6.1 PAA 74CHA 01

131 8 ITNA 73ABE 01

131 8 EXRF 78PEL 01

131 9 ITNA 76KUC 01 131.7 4.6 RTNA 81 GAL 01 131.7 4.6 D RTNA 81 GAL 02

132 3.3 AA 74RAI OL

132 10 FAA 760WE ol

132.3 0.35 RTNA 74MCC 01

134 9 35 ITNA 81GLA 03

135 ITNA 84CLE 01

135 AA 78GUI 01

135 AA 78WEG 01

135 6 D ITNA 78RYA 01

135 6 ITNA 77CHA 01

135 14 lENA 77R0W 04

137 16 ITNA 81 WAN 01

138 ITNA 75KLE 01

140 15 ITNA 78LAU 02

142 9 PAA 76KAT 02

142 13 PAA 76KAT 03

150 13 OES 76WEW 01 159 115 EXRF 77GIA 01

175 6 SSMS 78GUI 01

180 ITNA 75MIL 01

181 FAA 75P0L 01
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

Cs (ug/g)

0.63 0.06 PAA 74CHA 01 5.8 1.4 ITNA 78NAD 02

5.81 1.4 ITNA 75NAD 02

7.3 1 ITNA 78LAU 02

7.7 1.3 ITNA 76UEW 01 8 1 PAA 76CHA 01 8 1 D PAA 77CHA 01

8.1 0.5 9 ITNA 78LAU 02

8.2 0.4 ITNA 84GLA 02

8.2 0.5 ITNA 760ND 01 8.2 0.9 lENA 76STE 05

8.3 0.4 35 ITNA 81GLA 02

8.3 0.7 ITNA 85FIL 01 8.3 0.9 lENA 77R0W 03

8.3 1 D ITNA 78RYA 01 8.3 1 ITNA 77CHA 01 8.4 0.2 D NAA 79STE 01 8.4 0.5 ITNA 77R0W 04

8.42 0.22 lENA 77R0W 04

8.5 0.5 ITNA 78MAC 01 8.6 ITNA 78WEA 01 8.6 SSMS 83UEI 02

8.6 0.8 ITNA 76RAG 01 8.6 1.1 ITNA 750ND 01 8.7 0.3 35 lENA 80GLA 03

8.7 0.7 35 NAA 81GLA 04

8.8 0.4 35 ITNA 81GLA 03

8.9 0.8 ITNA 81 WAN 01 9.4 ITNA 75MIL 01 9.9 0.8 ITNA 73ABE 01 10 UU 80HEN 01 10 1 14NAA 81WIL 02

13,8 1.4 ITNA 73SHE 01

1 (ug/g)

70.2 1.8 AA 77MIT 01 110 11 OES 76WEW 01 115 8 ITNA 77R0U 03

115 8 ITNA 76STE 05

115 8 D NAA 79STE 01 119 5 AA 760ND 01 120 ICPES 80FLO 01 120 UU 80HEN 01 121 AA 79SIL 01 123 EXRF 78WEG 01 124 XRF 78CAM 02

124 ICPES 84S0B 01 124 19 FAA 760WE 01 125 AA 78GUI 01 125 10 D ITNA 78RYA 01 1633-

Conc Uncer Com Method Reference

Cu (ug/g) cont.

D^

125 10 ITNA 77CHA 01 125 13 EXRF 78PEL 01 126 2 AA 82HAR 01 127 AA 78GEL 01 128 3.9 ICPES 81CHU 01 128 6 ICPES 84B0T 01 129 AA 76UEU 01 129 AA 78UEG 01 129 4 ICPES 85HAR 01 129 5 8 SSMS 80KOP 01 130 2.2 AA 74RAI 01 130 5 AA 80STO 02

131 6 SSMS 78GUI 01

131 FAA 78GUI 01

131 AE+AF 77FEL 01 132 ICPES 84CLE 01 133 XRF 75KLE 01 133 4 EXRF 77GIA 01 134 11 6 PAA 82SEG 01 135 3 XRF 79SMI 01 136 ICPES 80NAD 01 136 6 35 RTNA 77GLA 01 137 7 ITNA 76BL0 01 140 10 XRF 81C0H 02

140 20 6 PAA 82SEG 01 140 20 PAA 80SEG 01 142 9 ITNA 73SHE 01 142 37 ICPES 84NAD 01

145 6 SSMS 78GUI 01 198 61 ITNA 81 WAN 01

(ug/g)

7.6 2.4 ITNA 73SHE 01 9 0.1 RTNA 8400D 01 9 2 ITNA 78MAC 01 9.1 0.1 ITNA 840DD 01 9.4 0.5 ITNA 76STE 05

9„4 0.5 ITNA 77R0W 03

9.4 0.5 D NAA 79STE 01 10.2 ITNA 75MIL 01 10.2 35 ITNA 81GLA 04

10.3 0.4 35 ITNA 81GLA 02

10.9 ITNA 78NAD 02

10.9 ITNA 75NAD 02

12 SSMS 83UEI 02

12.1 0.6 ITNA 760ND 01

19 3 SSMS 78SUG 02
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone UncGr Com Method Reference | Cone Uncer Com Method

1

1

1

Fe (X)

< 100 [_ OES 76UEU 01 1 4.23 0.3 PAA 76ICAT 03

< 300 L OES 76UEU 01 1 4.24 0.19 PAA 76KAT 02

2.1 SSMS 83UEI 02 1 4.4 AA 78GLII 01

11 2 SSMS 78SUG 02 1 5.278 0.56 ITNA 73SHE 01

89 3 RTNA 840DD 01 1 5.53 0.12 ICPES 84NAD 01

1 5.6 0.2 ITNA 76WEU 01

1 5.6 2.8 OES 76UEU 01

1 5.7 0.3 ITNA 76KUC 01

1 .9 0.2 ITNA 760ND 01 1 5.8 OES 78SUG 01 2 ICPES 80 FLO 01 1 5.8 AA 78UEG 01

2 2 35 lENA 80GLA 03 1 5.8 ITNA 84CLE 01 2.3 0.1 ITNA 73ABE 01 ! 5.8 0.3 5 lENA 80GLA 03

2.39 0.11 ITNA 76RAG 01 1 5.9 0.2 5 lENA 80&LA 03

2.42 0.16 ITNA 73SHE 01 1 5.91 0.16 lENA 77R0U 04

2.44 0.19 ITNA 76STE 05 1 5.93 0.04 ICPES 85HAR 01 2.49 0.15 35 ITNA 81GLA 02 1 5.94 XRF 78CAM 02

2.5 ITNA 78UEA 01 1 5.96 0.16 XRF 79SMI 01 2.5 0.16 35 ITNA 81GLA 04 1 6 XRF 76UEU 01 2.5 0.4 ITNA 750ND 01 1 6 ICPES 80FLO 01 2.56 0.07 ITNA 84GLA 02 1 6 0.2 ICPES 80EPS 03

2.57 0.19 ITNA 77R0W 03 1 6 0.3 ITNA 760ND 01 2.6 0.2 ITNA 76UEW 01 1 6 0.4 AA 79WEG 01 2.6 0.2 ITNA 85FIL 01 1 6.03 0.16 ITNA 81 WAN 01 2.6 0.2 ITNA 81 WAN 01 1 6.08 0.52 PAA 74CHA 01 2.62 0.05 ITNA 75NAD 02 1 6.09 0.03 ITNA 84GLA 02

2.62 0.05 ITNA 78NAD 02 j 6.1 0.1 TCGS 79FAI 01 2.69 0.09 ITNA 77R0W 04 1 6.1 0.1 D TCGS 80AND 01 2.69 0.09 D NAA 79STE 01 1 6.1 0.2 D PAA 77CHA 01 2.7 0.1 ITNA 78LAU 02 1 6.1 0.2 PAA 76CHA 01 2.72 0.07 ITNA 840DD 01 1 6.1 0.3 35 NAA 81GLA 04

2.79 ITNA 82GLA 02 1 6.14 0.07 ICPES 84B0T 01 2.8 0.13 OES 76UEW 01 1 6.16 0.3 EXRF 78PEL 01

2.8 0.3 RTNA 840DD 01 1 6.17 0.41 ITNA 78NAD 02

2.86 ITNA 75KLE 01 1 6.17 0.41 ITNA 75NAD 02

2.9 0.2 35 ITNA 81GLA 03 1 6.2 EXRF 78UEG 01

3 0.15 ICPES 81CHU 01 j 6.2 OES 80WAL 01

3.1 ITNA 75MIL 01 1 6.2 0.04 ICPES 80NAD 01 s SSMS 83UEI 02 1 6.2 0.05 ITNA 77R0W 03

5 3 11 2Cm SSMS 78SUG 02 1 6.2 0.05 D ITNA 77R0W 04

1 6.2 0.05 D NAA 79STE 01

1 6.2 0.1 EXRF 77NIE 01

1 6.2 0.1 AA 760ND 01

10 80HEN 01 1 6.2 0.1 AA 77MIT 01 20 AA 76WEW 01 1 6.2 0.2 FAF 80EPS 04

20 2 83BET 02 1 6.2 0.3 D NAA 740ND 01

O. ^ u.o ITUA 1 1 fin ( J\Jnu sf 1 6.2 0.4 D ITNA 78RYA 01 6.2 0.4 ITNA 77CHA 01 6.2 0.6 XRF 81C0H 02

6.22 0.08 TCGS 79AND 01

1 6.22 0.48 EXRF 77GIA 01

1633-10
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(%) cont.

1

6.23 0.1 ITNA 78LAU no 1 Od 1 1.9 SSMS 83UEI 02

6.23 0.14 35 ITNA olGLA no 1 11 ITNA 75MIL 01 6.3 0.1 ITNA U1 1 11.4 0.2 TCGS 79FAI 01 6.3 0.15 AA OcHAK m 1 U 1

1 11.6 0.1 RTNA 8400D 01 6.3 0.4 35 ITNA Q i /^l A O IGLA m 1 Uo 1 11.7 0.4 TCGS 79AND 01 6.32 ICPES OAU An oUNAD ni t U1 1 11.9 0.2 ITNA 840DD 01 6.35 ITNA TOl IC A roUEA ni 1 Ul 1 12.1 0.36 ICPES 81CHU 01 6.35 0.12 ITNA obrlL ni 1 Ul 1 17.5 0.3 TCGS 80AND 01 6.37 ITNA OKLE ni 1 U1 1 23 4 SSMS 78SUG 02

6.4 AA 79SIL n 1 1 01 1 6.4 0.15 14NAA 81WIL no 1 Od 1 Ge (ug/g)

6.46 ICPES 84CLE n 1 1 01 1 6.46 0.14 ICPES 81CHU n 1 1 01 1 19 1 XRF 79SMI 01 6.5 UU tSUHEN ni 1 Ul 1 20 UU 80HEN 01 6.51 0.31 ITNA 7T ADC m 1 U1 1 24 UU 78SIM 01 6.69 ITNA 7SMI 1 01 1

1 25 1.4 OES 76UEW 01 6.7 35 TCGS 7flRI A \JH 1 25.9 0.7 COLOR 84SHI 01 6.8 0.03 ITNA fOKAb ni 1 u 1

1 26 5 EXRF 77GIA 01 6.8 0.2 AA oUa 1

U

Ud 1 26.8 2.6 ICPES 84NAD 02

6.95 0.15 14NAA o IWI

L

ni 1 U1 1 36 SSMS 83WEI 02

7 AA ni 1 U1 1 131 FAA 75P0L 01 476 166 ITNA 73SHE 01 (ug/g)

H (ug/g)

34.3 1.9 ITNA 81 WAN n 4 1 01 1 37 2 lENA 78UAN n 1 1 01 1 1000 UU 80HEN 01 38.3 6.3 ITNA OSHE ni 1 01 1 1200 400 TCGS 79AND 01 40 1 XRF 79SMI n 1 1 01 1 40.3 2 5 lENA fOSTE nc 1 03 1 H20- (%)

40.7 1.2 D NAA 70eTC m 1 U1 1 40.7 1.2 lENA 1 r KOW Uj I 0.03 UU 80HEN 01 40.7 1.2 5 lENA nc 1

41 1 35 lENA O 1 uLA n/. 1 Uh I H20-T (%)

41 7 EXRF 77r I A f ruXA ni 1

1 43 1 35 lENA OUGLA U3 1 0.17 FD 80KHA 02

43 1 35 lENA tSIGLA nT 1 Uo 1 45 7 ITNA f OUNU ni 1 U1 1 H2S04 (ug/g)

45 . 8 ITNA o3r I

L

ni 1 Ul 1 48 6 COLOR fVLIK ni 1 01 1 < 1000 L UU 80HEN 01 49 XRF OKLE ni 1 Ul 1 50 UU OUntN ni 1 Ul 1 Hf (ug/g)

58 10 FAA roUWt ni 1 U 1

1 68 14 OES r OWkW ni 1 Ul 1 4 SSMS 83WEI 02

72 ICPES 80FLO 01 1 6.5 0.7 ITNA 76UEU 01 6.7 0.3 lENA 77R0U 03

6.7 0.3 D lENA 77R0W 04

6.7 0.3 D NAA 79STE 01 7 0.4 ITNA 77R0W 04

7.2 0.6 ITNA 76RAG 01 7.4 0.5 ITNA 78LAU 02

1 7.5 ITNA 78NAD 02

1633-11
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Hf (ug/fl) cont.

1

1 Ho (ug/g)

7.5 0.4 ITNA 78MAC

1 01 1 0.82 SSMS 83UEI 02

7.5 0.4 ITNA 85FIL 01 1 1.94 0.13 lENA 77R0W 03

7.5 0.5 ITNA 77CHA 01 1 1.94 0.13 D NAA 79STE 01 7.5 0.5 D ITNA 78RYA 01 1 1.94 0.13 lENA 76STE 05

7.52 0.02 ITNA 75NAD 02 1 1.98 0.01 RTNA 840DD 01 7.6 0.2 ITNA 84GLA 02 1 1.99 0.07 ITNA 840DD 01 7.62 0.56 ITNA 73SHE 01 1 3.6 0.8 SSMS 78SUG 02

7.7 0.1 ITNA 81 WAN 01 1 7.9 ITNA 78UEA 01 1 I (ug/g)

7.9 0.4 ITNA 750ND 01 1 8 0.4 35 ITNA 81GLA 02 1 < 0.5 L UU 80HEN 01 8 0.4 35 NAA 81GLA 04 1 < 6 L EXRF 77GIA 01 8.1 0.1 35 lENA 80GLA 03 1 2 1 .2 ITNA 77MAE 01 8.2 ITNA 75MIL 01 1 2.8 1 PAA 77CHA 01 O.d n o

I TNA 73ABE 01 1 o o d.y ITNA 70UC A A

1

8.2 0.8 ITNA 760ND 01 1 2,9 1.2 PAA 750ND 01

10 UU 80HEN 01 1 3 1 ITNA 77CHA 01

10 2 35 ITNA 81GLA 03 1 3 1 D ITNA 78RYA 01 10.8 ITNA 75KLE 01 1 3.4 SSMS 83UEI 02

Hg (ng/g)

1

1 In (ng/g)

100 UU 80HEN

1 01 1 118 4 5 lENA 76STE 05

119 2 CVAA 80NAD 01 1 128 8 5 lENA 76STE 05

120 15 CVAA 82SUL 01 1 128 8 D NAA 79STE 01 127 3 CVAA 75KLE 01 1 128 8 lENA 77R0W 03

130 30 PAA 76CHA 01 1 156 35 ITNA 73SHE 01

130 30 NAA 77JER 01 1 160 20 ITNA 81 WAN 01

130 30 D PAA 77CHA 01 1 270 140 ITNA 76RAG 01

134 4 CVAA 74RAI 01 1 280 30 PAA 74CHA 01

135 10 PAA 74CHA 01 1 290 60 PAA 76CHA 01 137 15 D RTNA 81 GAL 02 1 290 60 D PAA 77CHA 01 137 15 RTNA 81 GAL 01 1 320 80 D ITNA 78RYA 01

141 12 FAA 77GLA 03 1 320 80 ITNA 77CHA 01

145 ITNA 78WEA 01 1 320 100 ITNA 750ND 01

145 6 RTNA 740RV 01 1 3000 2000 EXRF 77GIA 01

145 6 RTNA 84DEL 01 1 160 40 ITNA 77CHA 01 1 Ir (ng/g)

160 40 D ITNA 78RYA 01 1 170 20 6 PAA 82SEG 01 1 < 200 L UU 80HEN 01 200 20 PAA 80SEG 01 1 15.6 2.4 RTNA 77NAD 02

200 100 6 PAA 82SEG 01 1 18.6 ITNA 78UEA 01 550 XRF 76UEU 01 1 18.6 3.3 ITNA 73SHE 01 3700 1100 ITNA 73SHE 01 1 250 80 ITNA 77CHA 01 11000 XRF 78CAM 02 1 250 80 D ITNA 78RYA 01

1633-12
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRH 1633 (cont.)

Cone Uncer Com Method Reference

1.29 0.09 ITNA 76KUC 01

1.51 ICPES 80NAD 01

1.51 0.05 ITNA 78MAC 01 1.54 0.04 ITNA 76BL0 01 1.56 ICPES 84CLE 01 1.58 0.15 ITNA 750ND 01 1.59 0.05 PAA 76ICAT 02

1.59 0.05 PAA 76KAT 03

1.6 OES 80WAL 01 1.6 0.04 ICPES 81CHU 01 1.6 0.06 PAA 76CHA 01 1.6 0.06 0 PAA 77CHA 01 1.6 0.12 AA 80STO 02

1.61 ITNA 78UEA 01 1.63 XRF 78CAM 02

1.63 0.06 ITNA 77MAE 01 1.64 0.01 AA 82HAR 01 1.65 0.09 ITNA 78LAU 02

1.66 0.04 XRF 79SMI 01 1.67 0.06 EXRF 78PEL 01 1.67 0.07 ICPES 84B0T 01 1.68 AA 79SIL 01 1.69 35 TCGS 78GLA 04

1.69 0.13 D ITNA 78RYA 01 1.69 0.13 ITNA 77CHA 01 1.7 ITNA 78KEL 02

1.7 0.2 ITNA 760ND 01 1.71 0.03 GAMMA 750ND 01 1.71 0.03 GAMMA 73ABE 01 1.71 0.04 AA 760ND 01 1.71 0.1 ICPES 84NAD 01 1.72 0.09 ICPES 80NAD 01 1.73 0.18 ITNA 81 WAN 01 1.74 0.07 EXRF 77NIE 01 1.75 UU 80HEN 01 1.75 0.1 TCGS 79AND 01 1.75 0.18 ITNA 76RAG 01 1.76 0.05 D TCGS 80AND 01 1.76 . 0.05 TCGS 79FAI 01 1.76 0.19 ITNA 85FIL 01 1.77 ITNA 75MIL 01 1.78 0.23 ITNA 75NAD 02

1.78 0.24 ITNA 78NAD 02

1.8 ITNA 75KLE 01 1.8 0.1 ICPES 85HAR 01 1.8 0.13 ITNA 77R0W 03

1.8 0.13 D NAA 79STE 01 1.8 0.13 ITNA 76STE 05

1.8 0.3 14NAA 81UIL 02

1.81 0.15 35 ITNA 81GLA 03

1.83 0.05 35 lENA 80GLA 03

1633-1

Cone Uncer Com Method Reference

(%) cont.

1.9 0.5 14NAA 81UIL 01

1 .97 35 ITNA 81GLA 04

2.18 0.24 ITNA 73SHE 01 3.3 0.66 OES 76WEW 01

1 (uq/q)

45 4.5 OES 76WEU 01 64 2 ITNA 78NAD 02

64.1 1.6 ITNA 75NAD 02

68 2 ITNA 78MAC 01 68 5 ICPES 85HAR 01 70 UU 80HEN 01 71.9 ITNA 84GLA 02

72 6 XRF 79SMI A401 74 4 ITNA 78LAU A^02

74.8 ITNA 82GLA 02

75 4 35 ITNA 81GLA A903

76 14 ITNA 760ND A A 01 76.4 4.5 ITNA 81UAN A 4 01 77 8 ITNA 73SHE 01 78 XRF 78CAM 02

78 ICPES 80 FLO 01 79 1.6 ICPES 81CHU 01 79 6 35 lENA 80GLA A703

80 ITNA 75MIL A 4

81 2 ITNA 76RAG A 4 01

81 3 D NAA /ySTE 01 81.2 3.2 lENA f OSTc 0!> 81.2 3.3 lENA I / KOW 03

82 ITNA roWcA 01 82 ITNA oKLE 01 82 2 ITNA 750ND A 4 01 82 4 ITNA 73ABE A 4 01 82 20 EXRF 77GIA A401 83 0.9 ITNA 85FIL 01 84 2 RTNA 840DD 01 84 3.6 lENA 77R0W 04

84 3.6 ITNA 77R0W 03

85 3 ITNA 8400D 01 85 4 D ITNA 78RYA 01 85 4 ITNA 77CHA 01 85.3 3.8 ITNA 77R0W 04

86 2 ITNA 76UEU 01

91 7 ITNA 76STE 05

110 20 SSMS 78SUG 02

120 SSMS 83UEI 02
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRH 1633 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/g) Mg (%) eont.

1.7 0.3 ICPES 81CHU 01 1 1.5 0.15 PAA 76CHA 01 80 AA 76UEU 01 1

4 C 1.5 0.2 TCGS 79FAI 01 140 9 OES 76WEU 01 1 1.5 AO r\ 0.2 D TCGS 80AND 01

161 4 / 14 ICPES 84B0T 01 1

4 C 1.5 0.3 ITNA 76WEU 01 186 ICPES 84CLE 01 1 1.5 1 .3 14NAA 81WIL 01 300 UU 80HEN 01 1 1 .52 0.06 ITNA 75NAD 02

1 .52 0.06 ITNA 78NAD 02

1 (uq/g) 1 .597 0.806 ITNA 73SHE 01

1 .6 0.32 OES 76UEU 01 0.78 SSMS 83UEI 02 1 1 .68 0.21 ITNA 77CHA 01 0.87 ITNA 82GLA 02 1 1 .68 0.21 D ITNA 78RYA 01 0.9 0.3 ITNA 81 WAN 01 1 1 .78 0.2 ITNA 76STE 05

0.94 0.09 D ITNA 77R0W 04 1 1 .78 0.2 ITNA 77R0W 03

0.94 0.09 ITNA 77R0W 03 j 1 .78 0.2 D NAA 79STE 01 0.94 0.09 D NAA 79sTE 01 1 1 .8 ICPES AA^I M All 80FLO 01

1 0.1 ITNA 750ND 01 1 1 .8 OES 80WAL 01

1 0.2 ITNA 76UEW 01 1 1 .8 ITNA 78UEA 01

1 .01 0.02 ITNA 78NAD 02 1 1 .8 0.4 ITNA 750ND 01

1 .01 0.02 ITNA 75NAD 02 1 2 UU OAil^kl A4 80HEN 01

1-1 35 ITNA 81GLA 03 1 2

A / 0.4 ITNA 7Z n A A A 4 76RAG 01

4 4 1.1 0.15 D ITNA 78RYA 01 1 2.08 A / T T Til A ITNA 7^ ABE A 4

4 4 1.1 0.15 ITNA 77CHA 01 1 2.1 i / kl A A 14NAA Oil If 1 f\'i 0IUIL 0^

1.11 0.22 ITNA 84GLA 11 1 2.19 A0.35 ITNA 04llAkl A4 81WAN 01

1 .2 ITNA 75MIL 01 1 2.4 35 TCGS *70AI a a/ 78GLA 04

1 .56 0.01 RTNA 84ODD 01 1 6.3 0.3 ITNA

^VAftJ A A A 4 78MAC 01

1 .68 0.06 ITNA 84ODD 01 1

1 .7 0.4 SSMS 78SUG 02 1 Mn (uq/q)

2 0.05 ITNA 78LAU 02 1 3.8 0.5 ITNA 73SHE 01 1 351 6 SSMS ^OAl 1 Y A 4 78GUI 01 4 J ITNA 78MAC 01 1 388 ICPES 0 / AAA A 4 84S0B 01 420 ITNA ^OlXEl AO 78KEL 02

422.4 3.9 AA 77MIT 01 440 AA 70l IP A A 4 78UEG 01 0.84 0.05 AA 82HAR 01 1 460 ITNA 75KLE 01

1 .01 ICPES 80NAD 01 1 460 26 OES 76wEU 01

1 .2 0.1 AA 01 1 464 1 ITNA ^Oliaa AO 78nAD 02

1.22 AA 79s I

L

01 1 464 1 .4 ITNA A A AO 75 NAD 02

1.25 0.06 ICPES 85HAR 01 1 464 46 ITNA

^9£ lA A 4 76ICUC 01 1.29 0.02 ICPES 01 1 465 ICPES 0/ Al r* A4 84CLE 01 1.29 0.03 ICPES 84B0T 01 1 466 31 ITNA ^'Vaiip A4 73SHE 01

1.3 0.04 ICPES 84NAD 01 1 470 20 ICPES OPilftA A4 85HAR 01 1.32 0.04 ICPES 81CHU 01 1 477 5 AA 7^AilA A4 760ND 01

1 .34 ICPES 84CLE 01 1 478 FAA roGUI 01

4 / 1 .4 OES 70C1 \(i ni 1

1

/ OA 480 10 t Tkl A ITNA roBLO U1

4 / 1 .4 0.4 ITNA 78LAU 02 1/ OA 480 25 D TCGS OAAlin Al oUAND U1

1.4 0.4 ITNA 77MAE 01 1 480 25 TCGS 79FAI 01 1.44 0.02 PAA 76KAT 03 1 482 ICPES 80NAD 01

1.45 0.05 AA 80STO 02 1 483 12 ICPES 84NAD 01 1.48 0.01 PAA 74CHA 01 1 483 21 XRF 79SMI 01

1.5 0.01 PAA 76KAT 02 1 485 AA 79SIL 01

1.5 0.15 D PAA 77CHA 01 1 488 14 ITNA 77R0W 03

1633-14
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

Mn (ug/g) cont.

488 14 D NAA 79STE 01 488 14 ITNA 76STE 05

488 50 ITNA 81 WAN 01 489 11 ITNA 73ABE 01 490 SSMS 83UEI 02

490 14 ICPES 84B0T 01 ^91 10 PAA 76KAT 02

491 18 PAA 76KAT 03

492 AA 78GUI 01 492 7 AA 82HAR 01 493 4.1 AA 74RAI 01 495 ITNA 78WEA 01 495 15 PAA 76CHA 01 495 15 D PAA 77CHA 01 495 25 PAA 74CHA 01 496 OES 80UAL 01 496 19 D NAA 740ND 01 496 19 ITNA 750ND 01 498 11 35 ITNA 81GLA 03

499 22 6 FAA 79GEL 01 499 25 ITNA 760ND 01 500 OES 78SUG 01 500 EXRF 78UEG 01 500 UU 80HEN 01 500 15 ITNA 77CHA 01 500 15 D ITNA 78RYA 01 500 17 EXRF 78PEL 01 503 15 ITNA 77MAE 01 504 25 ITNA 76WEW 01 505 9 35 ITNA 81GLA 02

505 14 ITNA 76RAG 01 506 AA 76WEW 01 508 XRF 78CAM 02

510 ICPES 80FLO 01 510 10 ITNA 78LAU 02

510 70 XRF 81C0H 02

513 15 35 lENA 80GLA 03

516 16 ICPES 81CHU 01 520 . 6 FAA 760WE 01 520 20 ITNA 78MAC 01 528 6 SSMS 78GUI 01 528 104 EXRF 77GIA 01 530 30 AA 80STO 02

531 14 EXRF 77NIE 01 540 ITNA 75MIL 01 570 24 6 FAA 79GEL 01

Cone Uncer Com Method Reference

Mo (U3/a>

0.5 0.08 D PAA 77CHA 01 0.5 0.08 PAA 76CHA 01 1.52 0.15 PAA 74CHA 01 20 ITNA 78UEA 01 20 UU 80HEN 01 22.3 1.6 14NAA 81WIL 02

25 5 EXRF 77GIA 01 25.3 1.6 D NAA 79STE 01 25.3 1.6 lENA 77R0W 03

25.3 1.6 D lENA 77R0W 04

do OJWt 1 26 2 ICPES 84B0T 01 CO t VPF AKP 70CUI f Ton i 28 1 35 lENA 80GLA 03

onCO 1 1 CNA o 1 uLA

28 1.3 14NAA 81W1L 01 TOoc OUNML/ U 1 36 3 35 RTNA 78GLA 02

36 5 FAA 760WE 01 37 1.3 OES 76WEU 01

1 (ug/q)

< 1000 L UU 80HEN 01

la (ug/g)

2603 156 ITNA 76KUC 01 2658 129 ITNA 73SHE 01 2800 300 ITNA 76BL0 01 2820 50 ITNA 78MAC 01 2830 136 ITNA 76STE 05

2830 140 D NAA 79STE 01 2830 140 ITNA 77R0W 03

2900 ICPES 80NAD 01 2900 OES 78SUG 01 3000 AA 79SIL 01 3000 OES 80UAL 01 3000 UU 80HEN 01 3000 70 ICPES 81CHU 01 3000 100 ITNA 78LAU 02

3000 200 TCGS 79FAI 01 3000 200 D TCGS 80AND 01 3000 200 ICPES 84NAD 01 3052 264 ITNA 81WAN 01 3070 80 ITNA 77MAE 01 3100 200 ICPES 80NAD 01 3100 300 ITNA 760ND 01 3130 ITNA 84GLA 02

3150 110 14NAA 81UIL 01 3200 SSMS 83WEI 02

1633-15
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

Na (ug/g) cont.

3200 ITNA 78WEA 01 3200 200 AA 760ND 01 3200 200 AA 82HAR 01 3200 200 ICPES 84B0T 01 3200 300 D ITNA 78RYA 01 3200 300 ITNA 77CHA 01 3200 400 ITNA 750ND 01 3220 50 35 ITNA 81GLA 03

3230 ICPES 84CLE 01 32A0 100 ITNA 76RAG 01 3290 110 AA 80STO 02

3300 100 35 ITNA 81GLA 02

3300 100 ICPES 85HAR 01 3300 150 PAA 76CHA 01 3300 150 D PAA 77CHA 01 3300 200 ITNA 78NAD 02

3300 200 ITNA 75NAD 02

3330 170 14NAA 81WIL 02

T/ Aft 3A00 ITNA 75MIL ft i

3400 300 ITNA 76WEW 01 3400 300 PAA 74CHA 01 3600 35 TCGS 78GLA 04

3700 200 ITNA 73ABE 01 3850 210 PAA 76KAT 03

3860 130 PAA 76KAT 02

9700 1900 OES 76UEW 01

lb (ug/g)

< 100 L OES 76UEU 01

7. UU 80HEN 01 26 1 XRF 79SMI 01 28 2 EXRF 77GIA 01 56 SSMS 83UEI 02

id (ug/g)

57.8 1.6 D ITNA 77R0W 04

57.8 1.6 ITNA 77R0W 03

58 2 D NAA 79STE 01 58 10 ITNA 81 WAN 01 60 35 lENA 81GLA 04

60 SSMS 83WEI 02

60 2 35 lENA 80GLA 03

60.5 1.5 ITNA 75NAD 02

61 2 ITNA 78NAD 02

62 2 TCGS 80AND 01 62.1 2.4 TCGS 79FAI 01 66 7 ITNA 760ND 01 67 2 RTNA 8400D 01 69 4 ITNA 840DD 01 1633-16

Cone Uncer Com Method Reference

1 (ug/g) cont

69 7 ITNA 77CHA 01 69 7 D ITNA 78RYA 01

81 ITNA 75MIL 01 90 13 SSMS 78SUG 02

94 19 ICPES 81CHU 01

4 (ug/g)

< 100 L UU 80HEN 01

(ug/g)

69 7 lENA 77R0W 03

78 AA 76UEW 01 84 2 35 lENA 81GLA 04

84 6 35 lENA 80GLA 03

85 AA 78GUI 01 88 2 ICPES 84B0T 01 92 6 PAA 750ND 01 92 9 6 PAA 82SEG 01 93 EXRF 78UEG 01 93 5 8 SSMS 80KOP 01 94 XRF 78CAM 02

94 ICPES 80FLO 01 95 9 D ITNA 78RYA 01 95 9 ITNA 77CHA 01 95 20 EXRF 78PEL 01 96 3 PAA 76KAT 02

96 5 XRF 79SMI 01 96 5 PAA 76ICAT 03

96 5 ICPES 85HAR 01 96.4 1.2 6 I QMS 74M00 01 96.4 1.2 6 IDMS 74M00 01 96.6 1 6 IDMS 74M00 01 96.8 3.2 PAA 74CHA 01 97 5 PAA 76CHA 01 97 5 D PAA 77CHA 01 98 POL 74MAI 01 98 FAA 80UAL 01 98 9 D NAA 740N0 01 98.5 9.5 lENA 77R0W 04

99 AA 79SIL 01 99 4 AF 80EPS 02

99 9 D NAA 79STE 01 99.7 3.3 AA 77MIT 01

100 UU 80HEN 01

100 ICPES 84CLE 01

100 3 ICPES 81CHU 01

100 5 ITNA 75NAD 02

100 5 ITNA 78NAD 02

100 7 6 PAA 82SEG 01
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ni (ug/g) cont. 1

1

Pb (ug/g)

100 7 AA 760ND 01 1 40 6 SSMS 78GUI 01 100 20 ITNA 760ND 01 1 46 13 ICPES 84B0T 01

101 3.3 AA 74RAI 01 1 55 FAA 75 POL 01

101 7 EXRF 77GIA 01 1 62 AA 78GUI 01 105 3 14NAA 81UIL 01 1 62.8 FAA 78GUI 01

105 13 ITNA 750ND 01 1 64 13 ICPES 81CHU 01 106 FAA 78GUI 01 1 65 EXRF 78UEG 01 106 12 14NAA 81UIL 02 1 66 6 XRF 79SMI 01 109 XRF 75KLE 01 1 66 12 EXRF 78PEL 01 110 SSMS 83UEI 02 1 67 POL 74MAI 01 110 7 PAA 80SEG 01 1 68 4 PAA 80SEG 01 110 10 9 ITNA 78LAU 02 1 68 4 6 PAA 82SEG 01 120 OES 78SUG 01 1 68 5 13 ICPES 84B0T 01 120 7.5 OES 76UEU 01 1 68 6 8 SSMS 80KOP 01

121 21 ITNA 85FIL 01 1 68.8 POT 82CHR 01 128 ICPES 80NAD 01 1 69 4 6 PAA 82SEG 01 330 ICPES 84S0B 01 1 70 . AA 79SIL 01 70 AA 78GEL 01 N02 (uq/q) 70 6 SSMS 78GUI 01 70.5 FAA 78SIE 01 < 100 L UU 80HEN 01 1 70.7 2.6 PAA 74CHA 01

1 71 3 NAA 77JER 01 N03 (UQ/q) 71 3 PAA 76CHA 01

1 71 3 0 PAA 77CHA 01 < 100 L UU 80HEN 01 1 72 5 EXRF 77GIA 01

1 74 4 FAA 76BL0 01 0 (%) 1 74 4 FAA 75BL0 02

1 74 9 OES 76WEW 01 47.02 0.08 34 14NAA SOKHA 02 1 75 OES 80WAL 01 75 5 PAA 750ND 01 OS (nq/q) 75 5 D NAA 740ND 01 76 AE+AF 77FEL 01

< 400 L UU 80HEN 01 1 77 ICPES 80NAD 01

< 4000 RTNA 77NAD 02 1 77 6 AA 80STO 02

78 2 IDMS 78CAR 02

P (ug/g) 78 2 AA 760ND 01

1 78 4 IDMS 75KLE 01 750 50 ICPES 85HAR 01 1 79.6 9.7 HAA 82NAD 01 880 . AA 76WEW 01 1 80 UU 80HEN 01 898 ICPES 80NAD 01 1 80 10 ICPES 85HAR 01 910 30 ICPES u t

1 81 ICPES 80FLO 01 1040 70 ICPES 84NAD 01 1 81 AA 78WEG 01 1090 26 ICPES 81CHU 01 1 82 AA 76WEW 01 1200 UU 80HEN 01 1 82 6 FAA 760WE 01 1300 SSMS 83UEI 02 1 100 25 14NAA 81UIL 02

1900 100 COLOR 80NAD 01 1 110 SSMS 83UEI 02

3000 35 TCGS 78GLA 04 1 Pb-21 (pCi/g)

I 3.37 0.13 D NM 81CAS 01

" 3.37 0.13 NM 80CAS 01 1633-17
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

< 2 RTNA 77NAD 02

innn 1L1 II 1 ouncN U 1 < 4000 L EXRF 77GIA 01

<u«l/3>

< 100 L OES 76UEU 01 24 ICPES 80FLO 01

CO o

40 SSMS 83UEI 02

92 RTNA 84ODD 01

(ug/g)

< 90 L OES 76UEW 01 0.4 UU 80HEN 01 0.451 0. Oil RTNA 77NAD 01 1.38 0. 28 RTNA 77NAD 02

(ug/fl)

70 30 ITNA 81UAN 01 95 1 PAA 76KAT 02

96 2 PAA 76KAT 03

100 10 9 ITNA 78LAU 02

102 5 14NAA 81UIL 02

105 10 ITNA 76RAG 01 108 4 D NAA 79STE 01 108 4 EXRF 77GIA 01 108.4 3. 7 lENA 77R0W 03

108.4 3. 7 D lENA 77R0U 04

110 2 XRF 79SMI 01 110 9 ITNA 77R0W 04

110 22 OES 76UEW 01

111 7 ITNA 84GLA 02

111 13. 5 ITNA 75NAD 02

111 14 ITNA 78NAD 02

112 20 ITNA 76WEW 01 114 XRF 78CAM 02

115 10 ITNA 78LAU 02

115 15 ITNA 73SHE 01 116 10 ITNA 77CHA 01 116 10 D ITNA 78RYA 01 117 6 35 lENA 80GLA 03

118 7 35 NAA 81GLA 04

119 7 35 ITNA 81GLA 02

120 XRF 75KLE 01 120 SSMS 83UE1 02

120 10 PAA 76CHA 01 120 10 D PAA 77CHA 01 123 9 35 ITNA 81GLA 03

1633-18

Cone Uncer Com Method Reference

Rb (ug/g) cont.

124 10 ITNA 73ABE 01 125 ITNA 78UEA 01 125 4 EXRF 77NIE 01

125 10 ITNA 750ND 01

126 10 PAA 750ND 01 130 30 ITNA 760ND 01 136 6 ITNA 85FIL 01 137 . 4 14NAA 81UIL 01 150 UU 80HEN 01

Re (ng/g)

< 200 L UU 80HEN 01

(ug/g)

< 0.5 L UU 80HEN 01 < 4 L EXRF 77GIA 01 < 30 L OES 76UEU 01

< 0.5 L UU 80HEN 01

< 30 L OES 76WEW 01 0.258 0.02 RTNA 77NAD 02

3 2 EXRF 77GIA 01

s (ug/g)

2000 XRF 81C0H 02

3900 400 TCGS 79FAI 01 3900 400 D TCGS 80AND 01 4000 400 TCGS 79AND 01 4400 100 TCGS 77JUR 01 4930 490 7 NM 83LI 01 5090 530 7 NM 83LI 01 7800 XRF 78CAM 02

9000 500 XRF 79SMI 01

;b (ug/q)

4 3 EXRF 77GIA 01

5 ICPES 82NYG 01 5.9 0.3 ITNA 81UAN 01 5.9 0.5 5 lENA 77R0W 04

5.9 0.5 5 ITNA 77R0U 04

5.96 0.61 HAA 82NAD 01 6 0.2 lENA 77R0W 03

6 0.2 D NAA 79STE 01 6.03 0.23 5 lENA 77R0W 04

6.1 0.4 5 ITNA 77R0W 04
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

Sb (ug/g) cont.

6.2 35 ITNA 81GLA 03

6.4 0.2 ITNA 78LAU 02

6.5 0.2 35 RTNA 78GLA 02

6.6 0.3 ITNA 85FIL 01 6.72 0.35 ITNA 75NAD 02

6.72 0.35 ITNA 78NAD 02

6.9 ITNA 78WEA 01 6.9 SSMS 83WEI 02

6.9 0.3 ITNA 760ND 01 6.9 0.5 D ITNA 78RYA 01 6.9 0.5 ITNA 77CHA 01 6.9 0.6 ITNA 76RAG 01 6.9 0.6 ITNA 750ND 01 7 UU 80HEN 01 7 1.1 PAA 750ND 01 7 1.2 PAA 76KAT 03

7.1 0.5 D PAA 77CHA 01

7.1 0.5 PAA 76CHA 01

7.1 0.5 NAA 77JER 01

7.1 0.7 PAA 76KAT 02

7.14 0.56 PAA 74CHA 01 7.2 0.3 35 ITNA 81GLA 02

7.2 0.3 35 NAA 81GLA 04

7.2 0.8 ITNA 73ABE 01 7.3 0.3 FAA 78HAY 01 7 L n t u

f TilA

1 1 NA f oMAL Ul 7.7 0.5 35 lENA 80GLA 03

7 R I1 TU& 1 Nn U 1 7.9 ITNA 84CLE 01 8.3 1.8 14NAA 81WIL 02

8.4 3 13 ICPES 84B0T 01 9.8 2.1 ITNA 76WEW 01 12.08 0.86 ITNA 73SHE 01 17.4 FAA 75P0L 01 54 13 ICPES 84B0T 01

tUQ/g)

20 ICPES 80FLO 01 20 UU 80HEN 01 20.7 2.1 PAA 74CHA 01 23 0.4 ITNA 76BL0 01 23 2.3 OES 76UEU 01 24 1 ITNA 76WEW 01 24 2 ICPES 85HAR 01 25.1 0.5 ITNA 75NAD 02

25.1 0.5 ITNA 78NAD 02

25.5 2 D ITNA 78RYA 01 25.5 2 ITNA 77CHA 01 25.6 0.5 lENA 77R0W 04

26 2 35 lENA 80GLA 03

1633-19

Cone Uncer Com Method Reference

Sc (ug/g) cont.

26.5 0.2 ITNA 84GLA 02

26.7 0.2 D ITNA 77R0W 04

26.7 0.2 ITNA 77R0W 03

26.7 0.7 D NAA 79STE 01 26.8 0.2 ITNA 78MAC 01 26.9 0.3 ITNA 81UAN 01 26.9 1.4 ITNA 760ND 01 27 ITNA 78WEA 01 27 0.5 ITNA 78LAU 02

27 0.6 ITNA 76RAG 01 27 1 ITNA 750ND 01 27 1 ITNA 73ABE 01 27 2 D PAA 77CHA 01 27 2 PAA 76CHA 01

dm** 1 1 NA Ul

28 1 35 ITNA 81GLA 02

CO . J n 7 ftl ni A riA u*+ 29 3 14NAA 81UIL 02

29.1 ITNA 75MIL 01 30 1 35 ITNA 81GLA 03

30 2 ITNA 85FIL 01 32 ITNA 75KLE 01

41 5 14NAA 81UIL 01 45 SSMS 83UEI 02

(ug/g)

3.2 HAA 74BYR 02

4.5 0.7 ASV 76AND 01 5.5 3.4 ITNA 81UAN 01 8.7 1.8 ITNA 78MAC 01 8.76 0.48 HAA 82NAD 01 8.8 XRF 78CAM 02

8.8 0.7 9 ITNA 80UAN 01 8.8 1.2 ITNA 73ABE 01 8.9 0.6 ITNA 80UAN 01 8.9 1.2 XRF 79SMI 01 9 ICPES 82NYG 01 9 1.4 ITNA 76RAG 01 9 2 35 lENA 80GLA 03

9.1 0.2 ITNA 78NAD 02

9.1 0.2 ITNA 75NAD 02

9.1 0.2 ITNA 81 CAR 02

9.1 0.3 35 NAA 81GLA 04

9.1 1 RTNA 740RV 01 9.2 2.6 ICPES 84B0T 01 9.35 0.03 GCMES 75KLE 01 9.35 0.03 GCMES 74TAL 02

9.35 0.03 DCPES 81 CAR 02

9.4 SSMS 83WEI 02

9.48 0.8 PAA 74CHA 01
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

Se (ug/g) cont.

9.5 0.8 PAA 76CHA 01 9.5 0.8 D PAA 77CHA 01 9.6 3.1 UNA 76BL0 01 9.7 COLOR 74BYR 02

9.8 ITNA 78WEA 01 9.8 0.5 6 PAA 82SEG 01 9.8 1 ITNA 77CHA 01 9.8 1 D ITNA 78RYA 01 10 UU 80HEN 01

10 0.5 9 ITNA 78LAU 02

10 0.5 8 SSMS 80KOP 01 10 0.6 RTNA 80KNA 01 10 0.9 PAA 80SEG 01

10 0.9 6 PAA 82SEG 01

10 2 ITNA 760ND 01

10.1 2.2 ITNA 76WEW 01 10.2 HAA 80WAL 01 10.2 1.4 ITNA 750ND 01 10.2 1.4 D NAA 740ND 01 10.3 0.7 D RTNA 81GAL 02

10.3 0.7 RTNA 81 GAL 01 10.6 1 ITNA 78LAU 02

10.6 1.3 ITNA 77R0W 04

10 7 0 4 I TMA sjj r I u 01

10.8 0.8 D NAA 79STE 01 10.8 0.8 lENA 77R0W 04

10.8 0.8 lENA 77R0W 03

11 1 EXRF 77GIA 01

11 3 ITNA 76KUC 01 12.7 1.8 ITNA 73SHE 01 13.3 ITNA 84CLE 01 35 13 14NAA 81WIL 02

35 13 14NAA 81UIL 01

(%)

16 OES 78SUG 01 17 3.4 OES 76WEW 01 17.7 35 TCGS 78GLA 04

20 1.6 PAA 76CHA 01 20 1.6 D PAA 77CHA 01 20.4 ICPES 80NAD 01 20.9 UU 80HEN 01

21 2 PAA 750ND 01 21.5 1.4 XRF 79SMI 01 21.8 0.3 TCGS 80AND 01 21.8 0.3 TCGS r79FAI 01 21.9 XRF 78CAM 02

22 1 35 AA 81GLA 03

22.4 0.3 ICPES 80NAD 01 22.4 1.6 14NAA 81UIL 02

1633-

Conc Uncer Com Method Reference

Si (%) cont.

22.6 AA 79SIL 01 22.7 0.05 ICPES 84NAD 01 22.8 0.8 14NAA 81UIL 01 23 1 EXRF 77NIE 01 23 6 14NAA 76BL0 01 23.5 0.5 35 lENA 80GLA 03

24.5 1.1 TCGS 79AND 01

(ug/g)

10.05 0.58 ITNA 73SHE 01 10.4 0.9 lENA 77R0W 04

11 1 ITNA 78MAC 01 11.4 1.6 lENA 76STE 05

11.8 1.6 lENA 77R0W 03

12.1 0.4 TCGS 79FAI 01 12.1 0.4 D TCGS 80AND 01

12.1 1 D ITNA 78RYA 01

12.1 1 ITNA 77CHA 01

12.1 1.4 D NAA 79STE 01 12.1 1.4 ITNA 77R0W 04

12.3 0.6 RTNA 840DD 01 12.4 ITNA 78UEA 01 12.4 0.5 ITNA 73ABE 01 12.4 0.9 ITNA 750ND 01 12.8 0.6 ITNA 76UEU 01 12.9 0.3 ITNA 840DD 01 13 ITNA 84GLA 02

13 0.3 TCGS 79AND 01

13 0.7 ITNA 76RAG 01

13 1.3 ITNA 85FIL 01 13.2 ITNA 82GLA 02

13.4 0.7 ITNA 760ND 01 13.5 0.5 ITNA 78LAU 02

13.6 0.88 ITNA 75NAD 02

13.6 0.9 ITNA 78NAD 02

14.9 1 35 ITNA 81GLA 03

15 ITNA 75KLE 01 15.8 0.3 ICPES 81CHU 01 17 SSMS 83UEI 02

20 3 SSMS 78SUG 02
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference 1 Cone Uncer Com Method Reference —

cont

.

K 84CLE 01 1 1410 400 14NAA 77VAN 01 9 ft 83WEI 02 1 1450 30 ypF 79SMI 01 T lUI 80HEN 01 1 1430 60 IFMA I tnn 76STE 05

c

3 C CAnr 77GIA 01 1 1450 AO NAA nnn 79STE 01

C3 7r MM 81INU 01 1 1460 bOU ITMA 1 1 nn 85FIL 01

A0« 7r 1 L ypF Al\ r 79SMI 01 1 14ft0 ITMA 1 1 nn 77MAE 01

1 M s 76UEW 01 1 141 HOWAO 60 IFMA I c nn 77R0W 03

1 U • b 1 L ITM* 77CHA 01 1 1480 60 ITMA I 1 nn 77R0W 04

10 P 1 L n1/ ITMA 78RYA 01 1 1500 UUuu 80HEN 01

12 1 PAA 76CHA 01 1 1500 180 D ITNA 78RYA 01 121 b

1

1 n PAA 77CHA 01 1 1500 180 ITNA 77CHA 01 12.5 1.2 PAA 74CHA 01 1 1500 200 ITNA 78LAU 02

12 7 0 82 HAA 82NAD 01 1 1510 60 5 lENA 80GLA 03

740 210 ITNA 73SHE 01 1 1520

1 1541

35

188 1 WW

lENA

ITNA

77R0W

81 WAN

04

01 S04 (%) 1 1600

1 1620

100 9 ITNA

I rPFS

78LAU

80FLO

02

01 n OA III 80HEN 01 1 1700 1 f Uv

1 1900

^oo

200

I1 TMA 1 nn

ITMA 1 1 nn

750ND

73ABE

01

01

11 ?500 bJUU

1 8000

1 inn nF?

XRF

76UEW

76WEW

01

01 FXRF 78UEG 01 869 ITMA I 1 nn 73SHE 01 1 la ^uy/Hj

1200 300 ITNA 76STE 05

1240 30 ICPES 84B0T 01 1 1 .6 ITNA 75KLE 01 1244 PAA 76KAT 02 1 1 .74 0.1 35 ITNA 81GLA 02

1244 9 PAA 76KAT 03 1 1 .74 0.12 35 NAA 81GLA 04

1250 230 ITNA 76RAG 01 1 1 .8 ITNA 78UEA 01 1256 37 EXRF 78PEL 01 1 1 .8 0.2 35 lENA 80GLA 03

1260 35 lENA 81GLA 03 1 11 8w 0 3 ITNA 760ND 01 1260 30 J IFMA 1 unn 80GLA 03 1

1 11 • 8W 0 3 ITNA 1 1 nn 750ND 01 1300 35 IFMA 81GLA 04 11 11 aW811 0 08 ITNA I 1 nn 84GLA 02

1300 200 ITMA i 1 nn 760ND 01 1 1 84 0U • 09U7 ITMA I 1 nn 85FIL 01 1301 XRF 75KLE 01 1 19 0 1 ITNA 78LAU 02

1310 50 14NAA 81WIL 01 1 1 9 0V • 2b 35 ITMA I 1 nn 81GLA 03

1310 60 14NAA 81UIL 02 1 19 0.25 ITNA 78RYA 01 1340 AA 79SIL 01 1 191*7 0 25 ITMA I 1 nn 77CHA 01 1340 70 ICPES 85HAR 01 1 2b 0W UU 80HEN 01 1340 100 ITNA 78MAC 01 1 , 2 00 0\J m 06WSJ IFMA I cnn 77R0W 03

1342 20 EXRF 77GIA 01 1 2 00 0.06 Q NAA 79STE 01 1360 110 5 lENA 76STE 05 1 2 . 00 0.06 Q lENA 77R0U 04

1370 120 PAA 77CHA 01 1 2b • 00wU 0.1 ITNA 78MAC 01 1370 120 PAA 76CHA 01 1 2.00 0.2 ITNA 76RAG 01 1373 95 PAA 74CHA 01 1 2b • 01V 1 0. 14 ITNA 77R0W 04

1375 28 ICPES 81CHU 01 1 . 2 04 0.03 ITNA 78NAD 02

1380 ICPES 84CLE 01 1 ^ 2 . 04 0,03 ITNA 75NAD 02

1390 ITNA 75MIL 01 1 'i- 2.1 0.2 ITNA 81 WAN 01 1390 XRF 78CAM 02 1 2.2 ITNA 75MIL 01 1400 SSMS 83UEI 02 1 2.74 0.25 ITNA 73SHE 01 1406 80 ITNA 75NAD 02 1 3.5 0.3 ITNA 73ABE 01 1406 80 ITNA 78NAD 02

1633-21
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRH 1633 (cont.)

:onc Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/g) Th (ug/g) cont.

0.22 0.04 ITNA 73SHE 01 1 24 2 35 RTNA 78GLA 02

1 .2 0.2 ITNA 78MAC 01 1 24 2 ITNA 760ND 01

1 .5 A V 0.3 ITNA 81 WAN 01 1 24.4 2.2 ITNA 750ND 01 1.5 A / 0.4 ITNA 760ND 01 1 24.5 0.4 ITNA 84GLA 02

1 .53 A 4 4 0.11 ITNA 84GLA 02 1 25 0.9 35 NAA 81GLA 04

1.7 A A 0.8 ITNA 85FI

L

01 1 25 1 35 ITNA 81GLA 02

1 .8 ITNA 75MI

L

01 1 25 2 ITNA 73SHE 01 1.87 0.15 ITNA 76RAG 01 1 26 ITNA 75MIL 01

1 .9 SSMS 83UEI 02 1 26 ITNA 75KLE 01

1 .9 0.1 ITNA 78LAU 02 1 26 DNA 75MIL 01

1 .9 0.3 ITNA 750ND 01 1 26.2 1,3 GAMMA 73ABE 01

1 .99 0.16 ITMA 77R0W 04 1 26.2 1.3 GAMMA 750ND 01

2 0.

1

35 NAA 81GLA 04 1 28 SSMS 83WEI 02

2 0.1 35 lENA 80GLA 03 1 28 2 ITNA 73ABE 01

2 0.25 D ITNA 78RYA 01 1 32.2 0.2 ITNA 78NAD 02

2 0.25 ITNA 77CHA 01 1 32.2 0.2 ITNA 75NAD 02

2 0.3 ITNA 73ABE 01 1 2.01 0.06 D lENA 77R0W 04 1 Th-228 (pCi/g)

2.01 rt AZ 0.06 lENA 77R0W 03 1 2.01 0.06 D NAA 79STE 01 1 2.23 0.05 NM 80CAS 01 2.4 A 1 0.1 I TNA 84C»D 01 1 2.23 0.05 A NM 81 CAS 01

^ . J n 1 U. 1 K 1 NA 840DD 01 1 A AO U.U2 f TbI A

I TNA 75NAD 02 1 Th-23 (DCi/g)

3.12 0.02 ITNA 78NAD 02 1 3.3 0.5 SSMS 78SUG 02 1 3.74

3.74

0.17

0.17

D NMNM81 CAS

80CAS

01

01

1 Th-232 (DCi/Q)

< A P 0.5 L UU 80HEN 01 1 < 5 L EXRF 77GIA 01 1 2.45 0.08 D NM 81 CAS 01 0.92 0.05 HAA 82NAD 01 1 2,45 0.08 NM 80CAS 01 2.3 0.3 PAA 76CHA 01 1 2.3 0.3 D PAA 77CHA 01 1 Ti (ug/g)

2.32 0.2 PAA 74CHA 01 1 9.9 1.1 35 RTNA 75GLA 01 1 3000

6000

XRF

UU

76UEU

80HEN

01

01 6000

6100

400 ITNA OES

78MAC

78SUG

01

01 20 UU 80HEN 01 1 6100 200 ITNA 78NAD 02

21 3 EXRF 77GIA 01 1 6100 200 ITNA 75 NAD 02

22.8 0.5 ITNA 76BL0 01 1 6300 200 ICPES 84B0T 01

23 2 ITNA 85FIL 01 1 6420 ITNA 75KLE 01 23.6 A O 0.8 ITNA 76RAG 01 1 6600 300 ICPcS 85HAR 01 23.8 A / 0.4 ITNA 77R0W 04 1 6800 A A AA 79SIL 01 24 A C 0.5 lENA 77R0W 03 1 6800 200 ICPtS 84NAD 01 24 A C 0.5 D lENA 77R0W 04 1 6800 1100 T TLI

A

1 1 NA 760ND 01

24 0.5 D NAA 79STE 01 1 6960 35 TCGS 78GLA 04

24 0.8 ITNA 81 WAN 01 1 7000 100 35 lENA 80GLA 03

24 1 35 ITNA 81GLA 03 1 7000 300 ITNA 77R0W 03

24 1 ITNA 78LAU 02 1 7000 300 ITNA 76STE 05

24 1 35 lENA 80GLA 03 1 7000 300 D NAA 79STE 01

1633-22
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference

)

Ti <ug/a? cont.

7000 700 ITNA 76WEU 01 7070 180 ICPES 81CHU 01 7100 100 ICPES 80NAD 01 7150 1200 ITNA 76RAG 01 7200 200 35 NAA 81GLA 03

7200 200 TOGS 79FAI 01 7200 200 D TCGS 80AND 01 7200 1400 OES 76UEW 01 7210 95 TCGS 79AND 01 7230 400 PAA 74CHA 01 7250 360 D PAA 77CHA 01 7250 360 PAA 76CHA 01 7300 XRF 78CAM 02

7300 150 14NAA 81WIL 01 7300 280 ITNA 77CHA 01 7300 280 D ITNA 78RYA 01 7300 400 PAA 750ND 01 7330 ICPES 80FLO 01 7360 344 EXRF 78PEL 01 7400 ITNA 78UEA 01 7400 300 ITNA 750ND 01 7400 500 ITNA 78LAU 02

7400 800 AA 760ND 01 7500 EXRF 78WEG 01 7500 ICPES 80NAD 01 7500 500 35 ITNA 81GLA 02

7600 200 14NAA 81WIL 02

7600 800 ITNA 73ABE 01 7660 70 PAA 76KAT 02

7660 100 PAA 76KAT 03

7700 300 XRF 79SMI 01 8140 ICPES 84CLE 01 8200 1100 ITNA 81 WAN 01 8600 1100 EXRF 77GIA 01 8700 AA 76WEW 01 8900 752 ITNA 73SHE 01

I (uq/g)

2 UU 80HEN 01 3.5 0.5 PAA 80SEG 01 3.5 0.5 6 PAA 82SEG 01 3.64 0.34 PAA 74CHA 01

3.7 0.4 PAA 76CHA 01 3.7 0.4 D PAA 77CHA 01 3.8 0.27 8 SSMS 80tCOP 01 3.8 0.5 6 PAA 82SEG 01

5 AA 76UEU 01 5.3 POT 82CHR 01 18 6 14NAA 81WIL 01 18 6 14NAA 81WIL 02

1633

Cone Uncer Com Method Reference

0.45 SSMS 83UEI 02

1.3 ITNA 75MIL 01 1.3 0.3 SSMS 78SUG 02

1.36 0.02 RTNA 840DD 01 1.43 0.04 ITNA 840DD 01

(ug/g)

8.4 0.56 ITNA 73SHE 01 8.6 1 35 FLUOR 78GLA 01 9 6 EXRF 77GIA 01 10.5 1 ITNA 76RAG 01 10.6 ITNA 81UAN 01 10.6 0.6 35 lENA 78GLA 01

11 0.4 6 PAA 82SEG 01

11.1 1.7 ITNA 760ND 01 11.3 0.3 ITNA 75NAD 02

11.3 0.3 ITNA 78NAD 02

11.3 0.3 35 DNA 78GLA 01 11.5 0.5 35 lENA 80GLA 03

11.5 0.5 35 DNA 81GLA 03

11.7 DNA 75MIL 01 11.7 2 IDMS 78CAR 02

11.8 IDMS 75KLE 01 11.9 0.4 6 PAA 82SEG 01 11.9 0.6 PAA 80SEG 01

12 ITNA 78WEA 01 12 0.5 GAMMA 750ND 01

12 0.5 GAMMA 73ABE 01 12 0.5 D NAA 740ND 01

12.1 0.8 13 PAA 81SEG 01

12.1 2 35 RTNA 75GLA 01 12.2 0.5 D NAA 79STE 01 12.2 0.6 lENA 77^0U 04

12.2 1 13 PAA 81SEG 01 12.4 0.6 lENA 77R0W 03

12.7 0.5 D NAA 79STE 01 12.7 0.5 lENA 76STE 05

12.8 ITNA 80EDD 01

13 SSMS 83WEI 02

13.5 1.2 ITNA 76STE 05

13.8 ITNA 75MIL 01

15 UU 80HEN 01

234 (DCi/g)

4.07 0.12 D NM 81 CAS 01 4.07 0.12 NM 80CAS 01
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

U-235 (pCi/q) 1 V (uq/q) eont.

0.179 0.012 NM 80CAS 01 1 237 9 ITNA 77MAE 01 0.179 0.012 D NM 81 CAS 01 1

1

237

237

20

20

D NAA

ITNA

79STE 01 76STE 05

U-238 (pCi/g) 1

1

237

240

20 ITNA

ITNA

77R0W 03

75KLE 01 4.01 0.04 D NM 81 CAS 01 1 270 60 ITNA 760ND 01 4.01 0.04 NM 80CAS 01 1

1

271

290 80

6 SSMS

ITNA

78GUI 01 76RAG 01 V (ug/g) 1 295 156 EXRF 77GIA 01

1 410 AA 76WEU 01

151 6 SSMS 78GUI 01 1 174 55 XRF 79SMI 01 1 W (ug/q)

182 XRF 78GAM 02 1 190 50 TCGS 79FAI 01 1 3.8 0.7 ITNA 81UAN 01 190 50 D TCGS 80AND 01 1 3.9 0.4 D NAA 79STE 01 196 10 ITNA 78MAC 01 1 3.9 0.4 lENA 77R0W 04

200 UU 80HEN 01 1 4 0.4 lENA 77R0W 03

200 34 EXRF 78PEL 01 1 4.2 0.4 lENA 76STE 05

201 6 FAA 760WE 01 1 4.5 1 D ITNA 78RYA 01 204 15 ITNA 76BL0 01 1 4.5 1 ITNA 77CHA 01 208 12 PAA 74CHA 01 1 4.6 ITNA 78WEA 01 210 OES 78SUG 01 1 4.6 SSMS 83WEI 02

210 SSMS 83UEI 02 1 4.6 1.6 ITNA 750ND 01 210 12 D PAA 77CHA 01 1 4.8 1.5 ITNA 760ND 01 210 12 PAA 76CHA 01 1 4.9 0.7 35 RENA 81GLA 03

214 12 ICPES 84NAD 01 1 5 UU 80HEN 01 216 AA 78GUI 01 1 5 1 35 LENA 80GLA 03

216 EXRF 78WEG 01 1 5.2 0.3 35 RTNA 78GLA 02

219 ICPES 80NAD 01 1 5.5 1.5 ITNA 76RAG 01 220 15 D ITNA 78RYA 01 1 5.8 0.3 35 NAA 81GLA 04

220 15 ITNA 73ABE 01 1 6 1 ITNA 78MAC 01 220 15 ITNA 77CHA 01 1 12.7 1.1 ITNA 73SHE 01 220 20 35 ITNA 81GLA 03 1 221 ITNA 78WEA 01 1 Y (ug/g)

222 3 ICPES 84B0T 01 1 223 9.9 ITNA 75NAD 02 1 30 UU 80HEN 01

223 10 ITNA 78NAD 02 1 44 4.2 OES 76UEW 01 224 6.7 ICPES 81CHU 01 1 56 SSMS 83WEI 02

225 9 ICPES 85HAR 01 1 60 5 EXRF 77GIA 01

225 20 ITNA 76WEW 01 I 60 8 PAA 77CHA 01 226 FAA 78GUI 01 1 62 4 ICPES 85HAR 01

230 10 ITNA 78LAU 02 1 62 10 PAA 750ND 01

230 10 35 ITNA 81GLA 02 1 65 ICPES 80FLO 01

230 10.6 ITNA 73SHE 01 1 66 XRF 78CAM 02

230 12 OES 76UEU 01 1 66 2 PAA 76KAT 03

230 30 35 lENA 80GLA 03 1 67 1 PAA 76KAT 02

233 ICPES 80 FLO 01 1 68 1 XRF 79SMI 01

234 34 ITNA 81UAN 01 1 68 16 SSMS 78SUG 02

235 13 D NAA 740ND 01 1 150 7 14NAA 81UIL 01

235 15 ITNA 750ND 01 1 150 15 14NAA 81WIL 02

236 ICPES 84CLE 01 1 1633-24
TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRH 1633 (cont.)

Cone Uncer Com Method Reference

4.7 0.4 ITNA 78MAC 01 0.6 ITNA 76UEW 01

5 5 0.3 ITNA 78LAU 02

KJ m 5J 1 .4 ITNA 78NAD 02

5 53 0.14 ITNA 75 NAD 02

5.7 0.56 OES 76WEW 01 5.7 0.6 ITNA 760ND 01 5.9 0.3 ITNA 76RAG 01 5.9 0.3 lENA 77R0W 04

5.9 0.4 ITNA 84GLA 11

6.1 0.18 ICPES 81CHU 01 6.2 0.2 5 ITNA 77R0W 04

6.2 3.4 ITNA 73SHE 01 6.6 0.4 D ITNA 77R0W 04

6.6 0.4 D NAA 79STE 01 6.6 0.4 ITNA 77R0W 03

6.77 0.06 RTNA 840DD 01 6.8 ITNA 75MIL 01 6.8 0.1 ITNA 840DD 01 7 ICPES 80FLO 01 7 3 ITNA 750ND 01 7.2 2.1 D ITNA 78RYA 01 7.2 2.1 ITNA 77CHA 01 8 SSMS 83UEI 02

8 0.5 35 ITNA 81GLA 03

8.4 0.6 ITNA 81 WAN 01 8.9 0.9 ITNA 73ABE 01 9 1.4 SSMS 78SUG 02

1 (ug/g)

180.7 4 AA 74GAL 01 195 23 RTNA 740RV 01 197 7 ICPES 84NAD 01 198 AA 78GUI 01 199 7 ICPES 84B0T 01 200 UU 80HEN 01 200 EXRF 78UEG 01 200 8 lENA 77R0W 04

200 10 9 ITNA 78LAU 02

200 10 EXRF 78PEL 01 200 20 ITNA 77CHA 01 200 20 ITNA 78LAU 02

200 20 D ITNA 78RYA 01 200.5 4 RTNA 74GAL 01 201 AE+AF 77FEL 01 201 6 D ITNA 77R0W 04

201 6 D NAA 79STE 01 201 6 ITNA 77R0W 03

201 8 AA 760ND 01 202 XRF 78CAM 02

1633-25

Cone Uncer Com Method Reference

Zn (ug/g) cont.

204 12 35 FAA 81GLA 03

204 13 5 lENA 80GLA 03

205 10 6 PAA 82SEG 01 205 20 PAA 80SEG 01 206 ICPES 84CLE 01 206 7.3 ITNA 81 WAN 01 207 ITNA 78WEA 01 208 XRF 75KLE 01 208 9.5 AA 80STO 02

208.1 24 ITNA 74GAL 01 208.2 3.6 AA 77MIT 01 210 SSMS 83WEI 02

210 OES 78SUG 01 210 ICPES 80NAD 01 210 36 OES 76WEW 01 211 ICPES 80EPS 03

212 ICPES 80FLO 01 212 7 XRF 79SMI 01 212 14 ITNA 75 NAD 02

212 14 ITNA 78NAD 02

212 20 FAA 760WE 01 213 ICPES 84 SOB 01 213.5 1 XRF 74GAL 01 214 AA 78GEL 01 214 2 AA 75EPS 01 214 2 AF 75EPS 01 214 16 PAA 74CHA 01 215 20 PAA 76CHA 01 215 20 D PAA 77CHA 01 215 20 NAA 77JER 01 216 FAA 80WAL 01 216 2.4 AA 74RAI 01 216 14 EXRF 77GIA 01 216 25 D NAA 740ND 01 216 25 PAA 750ND 01 218 33 AA 82HAR 01 219 4 ICPES 79EPS 01 220 5 ITNA 760ND 01 220 10 PAA 82SEG 01 220 130 ITNA 76BL0 01

221 AA 79SIL 01

221 16 5 lENA 80GLA 03

221 16 35 NAA 81GLA 04

228 6.9 ICPES 81CHU 01 230 40 ITNA 76RAG 01 232 9 ICPES 85HAR 01 234 AA 78WEG 01 250 AA 76WEW 01
Cone Uncer

TABLE 1633-2: INDIVIDUAL DATA FOR NBS SRM 1633 (cont.)

Com Nethod Reference |

Zn (ug/g) cont.

o ssns roGUI Ul

dfi) ITNA ronAC ni01 do5 o ssns 7DOI 1 T roGUI 01

ID T TU A

I TNA 7^1 Id 1 Ul

T TU A ITNA 01

(ug/g)

lOU 34 OcS 7^1 Id 1 01

fO t TUA ITNA 7^D A

f ORAG ni01 ^UU onucu ni01

O. f Q i OUI 1 Ul

£00 o 03 f CU A IcNA Q 1 Ol A OIGLA t\i Uh

£00 T once OUrLO Ul

/ cXRr 770 T Af f GI A Ul

c3

f CU A IcNA oUGLA Uo ooo o

DA A PAA n^U^

in DA A PAA 7iLVA T

rOlkA 1 Uo

5neU U

DA A rAA 77011

A

Ul DA A rAA 7i^OU A

f OLnA niUl oUI on DA A PAA r 3UNU niUl

oU I DA A PAA 7/ PU

A

niUl

VDC 700 AM no

J 1

U

1 1 NA TTOUA f f LnA niu 1 310 20 D ITNA 78RYA 01 310 20 9 ITNA 78LAU 02

310 70 lENA 77R0W 03

310 70 D lENA 77R0W 04

310 70 D NAA 79STE 01 311 8 XRF 79SMI 01 340 50 5 lENA 80GLA 03

380 20 14NAA 81UIL 02

400 SSMS 83WEI 02

410 ITNA 77R0W 04

410 20 14NAA 81UIL 01 500 ITNA 75MIL 01 640 140 ITNA 73SHE 01

1633-26

/
(/) 8 zco o c

s: </> a. (j>

u- to

<£

X Irt I CL —I </) <J

UJ CJ

O LU

U < — Q. O I- »— 1— r\ji— »— t— t— ir\ <— »— »

00 in ^ ^ 00 00 ^ vt ro

(/I «/>

(/) 3: (/) (/)

X

u CL z (J a. U O O u- U (-1 I- — — < I- —

fS] >— »- fO (NJ ^

CO^ > ro • I • 1 ^ o

oo

oo

-I a. o CJ—•

COz

«- 1 f\J 5 Cl

o

OJ >- (M o r«. T- -o o • • «- o> o>

</>

o

O

O t- o H

CO

in

o

O

OO

****

ro

o

ES

a.

<L) t- z _< co

00

g(J

4<

0) z

lUu

o(/) < <<

roc

>o eg

ft) z z

CO

U)

CDZ UJ O < u.<<oa z

111 < _j

a.EuUJz c 1 <

>o CO

oCO

CO

UJ z —t

UJ

00 (/> < z c o IS u 0) z8

CD

C

(D

O

Oo

in

in

vivo

in

oeo

o

o CO

o.oo

o

o

r-- ^ oooo oo I ^ I o

(MO

»- CM <—

(Nl

«- rg

K) »- vO «-

OvO

o

vt fM in

•-

o

(NJ (NJ ^ o

in ro

in +1o

o

CO

>4-

00roos

00o in

o CO

<M (NJ in

r\i <> vO INI ro

roo

o (N) in ro r^ in ro in ro

o ro ro in ^- o o ro 00 ^

00 in

00 (NJ

o <> in ro »o ro ro CO ro o

•* f\i (NJ N- in 00 1 1 in 1 I O ro 1 o 1 1 1 >» (M o 1 in h~ ro r^ 1 »» o* 1 -* 1 1 1 1 r^ 1 •«» o> o (NJ 00 1 m ro 1 1 ro 1 -* 1 1 1 1 ro in

/—\

1^ f~\ *^ >^ ^-^ *^ *^

<o ro (NJ (NJ r--o ro CO ro >!o in

(NJ ro (NJ (NJ (NJ f\j 1— ro ^> »—• > '

vO ro

N.

oo r<- (NJ (NJ (NJ (NJ

oo

oo <o vOoo rv- ro r«- (DO (NJo roO

o 1 1 1 1 (Nl ro 1 1 1 1 o 1 1 Kl +1 1 1 1 +4 +H •H 1 1 1 1 « +« +4 •H 1 M M M

MH +1 1 1 1 1 (NJ 1 1 1 V >» o ro O 00 ^ (NJ V ro m O -o r^ -4 •o O

-J- (Nl * o (NJ

o rom

o (NJo in ro ro

o>' ro

mo

oO •

in

(3 CD >o roo I 1 1 1 1 o (NJ 1 1 I 1 1 O 1 o 1 CO 1 +< 1 1 M 1 1 o r— 1 1 M t •M CO 1 H 1 1 *i in 1 1 1 1 1 t in 1 1 ( 1 1 1 1 1 1 1 1 1 ro m O 00 o •* 1

o o •*

O) o> O) o> Ol O) Ol O) Ol Ol Ol Ol Ol Ol Ol Ol CJl Ol Ol Ol

\ -V •V.

\

—

—\

\ ~v

—.

v.

\\—

O) O) O) O) ) O) Ol CD O) Ol Ol Ol Ol Ol Ol >e

Ol Ol O)

c

K 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3

(S (11 <u

c (0 (0 XI TJ T3 (U

O Iti 3 3 >- 3 (0

s

01 < < < < < < < CD 00 m CD CD CD CD o o o (-> o CJ LJ o o (J u O a UJ 11- u- o C3

1633A-1
o

c

ID

<U

O ^ m 0> O CO • O >- o ro

»- (M

oo J- o >* CO

S o:

o o>o -o o >o

«- (VJ

00• >» CO

in (M Kt ^ «—

00 >»

sj Ko • CO N. K) Kl lO

X

ca

a> X

00o

00

fsi 00

eo

V>

UJ

CL

*-*

U

c

c

o

a

u 01 X

c/>

c

>-1 u.1 < </) o < 44 z ca

U) &> f— X z

UJXUJ

_J

tuc

UJu< o QC (/) < < +4 <

Klc

<0

01 X

XQC

cnm

00z UJu

ae z O < u-<<o z UI < 1

Cl

o

u

UJX

c 1 <

>o </> CO

to

UJ z _l

CD c/> < z c O (0 o CI X

o

oo

>0 in o

os

oOo

OO Kl

o

O

V N-in

CO

•-

oo

o o>

(\Jo «-

o

»-

o

o

o J5J Kl

oOO

<o

o

ro »— I O (M

»- fSJ

o

»— in 5

to in

CO

o

o • •- o-a

oKl

(NJ s

o

(M

Orooro

o o.

Kl CO «-

>0ro

C^ in

po S.

ooro

o

Kl

Kl

CO

CO

N.'

ro

K>

Kl K) -»Ki CO r- CO ro m Kl O • ^ m o ro in in o

KlO

o

<y 00 in

00

<—

o • in in o sj- ^

ro

m >0

o OK) ^ «- <0 ro >f I I <x)

m 3 in (S' s

»- PO «-

CO

Kl

oCO

c/t COz o3

Ol Ol Ol o> \ z Ol Ol Ol Ol Ol 3 c 3 3 c

LE i

»*- Ol

Oc

UI z z o — — V

ooo ro

Ol Ol Ol O) Ol Ol Ol Ol Ol Ol Dl Ol Ol Ol Ol \ •V \ \ \ \ Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol Ol cn 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 — — 3 Ol Ol C 13 T)

Ol Ol Ol Ol oioicroi^^^^oi^oi ^ ^ •- — — >^ •- ^ S'333^^^3^3 000

ro ro ro

roro ^ ^ n ^

a. a. a. a. a.
v>8

c

o co

CO (/> </) <n cn UUOOOU. U-IJUOUU-U — (- — — — < — l-< —

oo^KmooifMpj ^eoco >o<ooe0'0 ••- •©> ir>o • •! .»-^ .t)^ Kir-«M • ~o I ^ rsj rsi to

r- (vj (V o rsi fO

<0

rsi

• o o lO • o CM CM m g m CO o

—I u u u

I • • « ^ Q • I •

I O O • CM ^ I • •

• ^ ^ K> ro rn t • •

s li. U

< —

ro »-

CM o

(M

c

SI

DCX

c

0)

COUi

4-* (_) c c 5 <D u 01 X

Z(A<

>- w _l

u.

_J O

< v> Ou

H z z

c

CO CO 0) »— X z

111 Xm-J

lU c

Ulo

< oCO <

ro c

(0«l X Xoe

(/>

CO

IBZ Ulo ec z

O < u.<

<

oo z

lU < -J oUl

IMOC X

c

1 3A

ro

>0r— us g;

(O Ul z —

Ul •M m CO < z c

r— o o u 41 X

o

o

CM

o

CMO

CM

oo

o

00

r^

CMCM

^>

>o

(SI o

T~

1 M H

1

1

' 001

fSJ ^•^

O in

1 • O

• O 4<

I

! 00

1 m

ro

00 ro

m tn o

+1 H 41 ro H

ro o in m in o

<<~\ ro ro ro

>>^

ino in ro o 1 ro

I H •

I • >o

ro ro

^» o

ro in

00 fO ro -J- o CO <^ ro ro

1 ro1 1 in •c

ro ro o

ro

s o ro oro

• ro ro

^\

oo m

\^

m in o ro o <o

•H <H O o O O

ro o ro

rsj

K ^ To

o

2

CM

O

o

oo

CM

«- CM

in

00

CO

oCM

CMCM

r- r- CO

CM ro o o

o in

CM CM

m o

ro M

V o

o

o

CM

00

o o ro

eo CM o >— >-

>» r^ N. • CM

m O

O CM O- CM ^

00

CM

CMCM

O

o

oo

00

• • o J- 1 CM I «—

00

00 in w CM

<Mo in «— o

o o

00 CM

JCM oro

CM

00

in CM

roo

CMO

in T—

r>. in

too

row w CM

00O

CM

roo

CM

CM

00

CM

CM

O to to

• a • o >0 00 CO (M

>t CMo CO

vj- <M in sO

• 00 -CM

in r>- CM

r^www>r oo CMCM

r^o

r-. in

o

CM >o CO CM

r». CM

CM

O CO o o in

•H H H H +< o> r^ >t O o CO >» r^ CM in (M ro

o

oCM

CM

o

oCO

o

oo o

CO

00 O

ro CM o o 1 1 to

1 1 t o 1 O

O o

*i +4 t 1

1 1 11+11 1 1 1 1 o *^ ro 00 oro

r^ CO t^ CM o CM oo •J- in o CM CMr^

<>

CM oCM

CM

at ^ (0 Ol 1. 3

ro to

CM to

to to

(/> CO (/> CO

3

-Jut m Ui Ui

Ul Ui 3 3 M

(/>(/)(/>

01

</) (/>

O)3

CTl CD tjl 3 3 3

E C

eo CO

3330.3333

CM

ro

CM a ^ 0)£j: — •— — E

0)0)^ 0)0)0)0)00)0)0)

S'f^33?^?^35

00

ro

CM 3 O i > > 3 >- c

rsj C crsi isi

1633A-3
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (revised 3/1/86)

Cone Uncer Com Method Reference

<ug/g)

< 0„3 ITNA 85GALI 04

< 0.6 L lENA 80GLA 03

< 1.1 L ITNA 82SUZ 02

(%)

13 0.41 ICPES 84NAD 01 13.8 0.2 ICPMS 86SCI 02

13.8 0.32 ITNA 830BR 01 13.93 0.32 lENA 85GLA 02

l^ Q.2 TCGS 79FAI 01

D TCGS 80AND 01

14 0.3 T Til A

I TNA 85VOG 01

1A. 1 O.c I CPES 84B0T 01

1A. 1 A O O.o ITNA 85SUN 01

14.

0.3 ITNA 80GAR 01 14.2 0.3 35 ITNA 81GLA 02

14.2 A / 0.4 TIC 35 ITNA 81GLA 04

14.2 A C 0.5 4 4 11 ICPES 85SAT 01 14.3 A 4 0.1 TCGS 85V0G 01 14.4 A 4 0.1 ICPES 85HAR 01 14.4 A O 0.2 1 1 ICPES 85SAT 01

4 / f 14.5 A 4 O 0.12 AA 82NAD 02

4 / T 0.7 ITNA 82SUZ 02

0.^ To EXRr 82PEL 01

4 / 7Z 14.76 0.3 16 EXRF 82PEL 01

i / o i ft o I trcb 82NAD 02

14-y/^Uf ft ftCOO ICPES 85PEA 01

4 C15 CPAA 83BIR 01

4 C15 0.43 CPXRF 80KIR 01 15.3 1.1 CPXRF 84AHL 01 15.4 0.2 16 EXRF 82PEL 01 16.5 1.5 ITNA 85FIL 01 17.4 6 EXRF 84JEN 01 17.5 6 EXRF 84JEN 01

(ug/g)

52.3 iCPES 85NAR 02

66 AF 85NAR 02

96 4 T13 ICPES 84NAn 01 97 4 O18 CPXRF 80KIR 01

135 1

isAA 82CRO 03

•lie 135 cD HAA 85YAM 01 138.4 8.8 POL 83ELK 01

4 / A 140 1 ICPES 84LIV 01

141 8 AE-AF 82MAT 01

142 ITNA 81SL0 01 143 RTNA 81SL0 01 143 8 FAA 84SIL 01

144 12 13 .CPES 84B0T 01 1633A

Cone Uncer Com Method Reference

( As (ug/g) cont.

145 11 FAA 83X1

01 145 HAA 84YAM 01 145 6 ITNA 82SUZ 02

145 8 CPXRF 84AHL 01 145 8 35 W 81GLA 04

4 / C 145 4 4 11 lENA 82GLA 02

145 15 ITNA 84SIL A 4 01 145.3 O. 1 ITNA 830BR A401 146 L ITNA 85V0G ft4 01 147 HAA 84TER 04

147 15 ITNA 85FIL 01 148 3 35 lENA 80GLA 03

148 5 ICPMS 86SCI 02

4 / n

149 3 ITNA 85 SUN A 4 01

4 C A 150 4 4 11 HAA 82CR0 AT03

4 CI 151 6 EXRF 84JEN A401

4 C ^ 152 6 EXRF 84JEN 01

4 C9 153 4 4 11 FAA 83X1A 4 01 157 1 1 13 ICPES 84B0T A401

(ug/g)

37.9 1.7 TCGS 85V0G 01 39 1 ICPES 820UE 01 39 3 33 TCGS O 4 A OIGLA A/U4

39.2 A 7 0.7 D TCGS 80AND A101 39.2 A 7 0.7 TCGS c A T fyFAI A101

/ 4 41 TCGS 84HIG Al01 42 4 TCGS 84GLA A401 44 OES 83MIL A 4 01

a (ug/g)

1060 ITNA 82GLA AO02

1100 100 9 ITNA 82SUZ A102

1210 PA50 9 ITNA 82SUZ 02

4 O / A 1240 200 5t ELI A lENA Oft/^l A oUGLA Uj

1300 90 ITNA o4SUZ

4 7 AA 1300 100 CPXRF 0/ A Ul o4AHL A1Ul

1333 4 ftft 100 4 717 ITNA o4KTL ftl 01 1339 4177 ITNA 03SUN ftl 01 1400 20 5 lENA 80GLA 03

1400 100 ICPES 84NAD 01

1400 360 ITNA 85FIL 01

1430 25 11 ICPES 85SAT 01 1440 36 ITNA 830BR 01

1450 110 35 NAA 81GLA 04

1471 70 17 ITNA 84KYL 01 1480 30 ICPES 85 MAR 0^

1490 80 ITNA 84GLA 02

1500 90 ITNA 80GAR 01
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Cone Uncer Com Method Reference

Ba (ug/g) cont.

1500 100 UNA 85V0G 01 1500 100 CPXRF 80KIR 01

1500 200 35 ITNA 81GLA 02

1520 20 5 lENA 80GLA 03

1540 30 ICPES 84B0T 01 1600 ICPES 82NAD 02

1760 300 5 lENA 80GLA 03

2350 6 EXRF 84JEN 01 2370 6 EXRF 84JEN 01

Be <ug/g)

12 OES 83MIL 01 12.16 6 ICPES 85P0U 01 12.2 0.3 11 ICPES 85SAT 01 12.36 6 ICPES 85POU 01 12,5 0.8 FAA 85POU 01

13 0.2 ICPES 84B0T 01

13 2 ICPMS 86SCI 02

13.3 0.5 11 ICPES 85SAT 01 13.4 6 ICPES 85P0U 01 13.5 0,8 6 ICPES 85POU 01 13.6 D AA 83TER 01 13.6 AA 82TER 02

Bi (uQ/g)

1.11 D FAA 84TER 03

1.11 HAA 84TER 02

1.42 AF 85NAR 02

Br <ug/g)

< 4.4 ITNA 84SUZ 02

< 10 L lENA 80GLA 03

2.2 0.3 ITNA 82SUZ 02

2.4 0.1 5 lENA 80GLA 03

Ca (%)

0.025 0.002 AA 82HAR 01 0.99 0.09 ICPES 84NAD 01 1.05 0.16 35 ITNA 81GLA 02

1.08 0.02 ICPES 84B0T 01 1.08 0,06 CPXRF 84AHL 01 1.09 0,01 AA 82NAD 02

1.09 0,02 ICPES 85HAR 01 1.1 0,08 ICPMS 86SCI 02

1.1 0.1 35 ITNA 81GLA 04

1.1 0.3 35 lENA 80GLA 03

1.11 0.03 ICPES 82NAD 02

Cone

Ca (%) cont.

1.11

1.12

1.12

1.12

1.12

1.13

1.13

1.14

1.14

1.14

1.16

1.2

1.2

1.2155

1.23

1.27

1.27

1.29

1.29

1.29

Cd (ug/g)

0.901

0.95

0.96

1.01

1.07

1.07

1.2

1.28

1.31

1.36

3.1

7,4

Ce (ug/g)

163

167

170

170

172.1

173.1

174

175

180

180

183

185

186

230

Uncer Com Method Reference

0.076 ITNA 830BR 01 0.01 11 ICPES 85SAT 01 0.01 11 ICPES 85SAT 01 0.07 ITNA 85VOG 01 0.08 ITNA 80GAR 01 0.02 16 EXRF 82PEL 01 0.12 ITNA 85SUN 01 0.02 16 EXRF 82PEL 01 0.02 16 EXRF 82PEL 01 0.04 AA 82GLA 02

0.21 ITNA 82SUZ 02

0.08 CPXRF 80KIR 01 0,2 TCGS 85VOG 01 ICPES 85PEA 01 0.16 ITNA 85FIL 01 6 EXRF 84JEN 01 6 EXRF 84JEN 01

T T A 85GAU 04

0,11 D TCGS 80AND 01 0.11 TCGS 79FAI 01

AA 84TER 01 0.05 IDMS 84BR0 03

0.06 ICPMS 86SCI 02

0.13 TCGS 85VOG 01 0.05 D TCGS 80AND 01 0.05 TCGS 79FAI 01 0.6 13 ICPES 84B0T 01 6 AF 84NAR 02

AF 85NAR 02

6 AF 84NAR 02

ICPES 85NAR 02

3,3 13 ICPES 84B0T 01

6 ITNA 82GLA 02

8 12 ITNA 82SUZ 02

6 ITNA 84SUZ 02

6 35 ITNA 81GLA 02

1 17 ITNA 84KYL 01 3,2 17 ITNA 84KYL 01

5 12 ITNA 82SUZ 02

4 ITNA 85 SUN 01

5 35 NAA 81GLA 04

20 ITNA 85FIL 01 19 ITNA 80GAR 01

5 ITNA 85VOG 01 4 35 lENA 80GLA 03

45 CPXRF 80KIR 01

1633A-5
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

1

1

1

Cs (uq/q)

(

< 69 L ITNA 82SUZ 02 1 9.3 0.5 ITNA 82GLA 02

1 9.6 0 6 171 f 84ICYL 01

( 1 ia /a ^

1 9 7 0u 6o 35 I TMA 81GLA 02

I CPES 85HAR 01 1 9 9 0u 6o I TUA 84GLA 11 37 ICPES 84B0T 01 1 9.9 0.9 ITNA 84GLA 02

37 3 35 lENA 80GLA 03 1 10.1 0.2 35 lENA 80GLA 03

38 13 CPXRF 80KIR 01 1 10.2 0.2 ITNA 82SUZ 02

39 2 ITNA 85FIL 01 1 10.5 0.3 35 NAA 81GLA 04

40 ITNA 82GLA 02 1 10.6 1.1 ITNA 80GAR 01 42.8 0.8 17 ITNA 84KYL 01 1 10.7 0.6 17 ITNA 84KYL 01 43.3 1 17 ITNA 84KYL 01 1 10.8 0.3 ITNA 86GAU 01 43.5 1 .6 ITNA 84GLA 11 1 11 1 .

ITNA 85FIL 01 43.9 0.55 COLOR 85KAT 01 1 11.1 1 .2 ITNA 85GAU 04

44 1 35 ITNA 81GLA 02 1 11.2 0.5 ITNA 85V0G 01 44 1 ITNA 82SUZ 02 1 11 .3 0.5 ITNA 85SUN 01 44.2 1 .55 AA 85KAT 01 1 11 .8 3.2 ITNA 84SUZ 02

44.8 0.8 ITNA 84GLA 02 1 44 a 1

1 121 C COLOR 83KAT 02 1 45 2 ITNA 84SUZ 02 1 45 9 0 7 I1 TMA 1 ran 85V0G 01 1 96 7 CPXRF 84AHL 01 HO 1 "^A 1 a JO 1?1 C 83KAT 02 1 96TV m 6O 10 7 AA 84KAN 01

1 5 I TNA 85SUN 01 1 115 1 11 ICPES 85SAT 01 46.2 T.8 ITNA 80GAR 01 1 116 4 AA 82HAR

47 L 35 NAA 81GLA 04 1 116 7 ICPES 84NAD 01 47 AA 82HAR 01 1 116.1 0.8 IDMS 84BR0 03

1 120 11 ICPES 85SAT 01

1 120. 2 ICPES 85HAR 01 129 2 ICPES 84NAD 01 1 120 4 ICPES 84B0T 01

145 44 CPXRF 84AHL 01 1 120 5.2 CPXRF 80KIR 01

185 7 12 ITNA 82SUZ 02 1 123 4 ICPMS 86SCI 02

186 6 ICPES 85HAR 01 1 124 33 ITNA 84SUZ 02

186 8 35 ITNA 81GLA 02 1 128 4 UXRF 84KYL 01 187 ft ICPES 84B0T 01 1 186 EXRF 84JEN 01 189 1

ICPES 85SAT 01 1 188 EXRF 84JEN 01

190 1 5 1

AA 84KAM 01 I 190 5 ITNA 85SUN 01 1 190 8w ITNA 85FIL 01 1 191 131 J ITNA 82GLA 02 1 14.3 0.2 35 ITNA 81GLA 02

192 ICPES 81UAL 01 1 14.5 35 ITNA 81GLA 04

193 14 ITNA 84SUZ 02 1 15 0.9 ITNA 85SUN 01

194 12 ITNA 82SUZ 02 1 15 3.3 ITNA 830BR 01

195 7 ITNA 84GLA 02 1 16.6 1 .3 ITNA 80GAR 01

196 8 11 AA 84KAM 01 1 16.8 0.3 ITNA 82SUZ 02

197 13 ITNA 80GAR 01 1 17.4 0.5 ITNA 84SUZ 02

197 18 35 ITNA 81GLA 04 1 198 1 ITNA 85VOG 01 1 200 11 CPXRF SOKIR 01 1

C\}C. lo A A AM 82HAR 01 1 210 11 ICPES 85SAT 01 1 (

210 8 ICPMS 86SCI 02 1 482 6 EXRF 84JEN 01 1 486 6 EXRF 84JEN 01 I 1633A-6
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRH 1633A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

i (ug/g)

1

1 Fe (%) cont.

2 2 35 lENA 80GLA

1 03 1 9.51 0.61 AA 82HAR 01

2.98 0.33 ITNA 80GAR 01 1 9.52 0.34 TCGS 85V0G 01 3.19 0.08 35 ITNA 81GLA 02 1 9.53 0.08 11 ICPES 85SAT 01 3.6 0.1 ITNA 84GLA 02 1 9.58 0.22 ITNA 85SUN 01 3.62 0.04 17 ITNA 84KYL 01 1 9.62 0.1 ITNA 85GAU 04

3.64 0.25 ITNA 830BR 01 1 9.7 0.2 5 lENA 80GLA 03

3.7 0.2 35 ITNA 81GLA 04 1 9.7 0.2 D TCGS 80AND 01 3.7 0.2 ITNA 82GLA 02 1 9.7 0.2 TCGS 79FAI 01 3.7 0.3 ITNA 82SUZ 02 1 9.7 0.3 ITNA 84SUZ 02

3.7 0.6 ITNA 85FIL 01 1 3.72 0.08 17 ITNA 84KYL 01 1 Ga (uQ/g)

3.9 0.3 ITNA 84SUZ 02 1 4 0.2 ITNA 85V0G 01 1 33 6 EXRF 84JEN 01 4.06 0.14 ITNA 85SUN 01 1

1

34

45 5

6 EXRF

ITNA

84JEN

85FIL

01

01

5154

54

ITNA CPXRF82SUZ

84AHL

02

01

23 2 ISE 83BET 02 1 55 4.6 CPXRF 80KIR 01

70 UU 85RIC 01 1 55.7 4.5 ITNA 830BR 01

87 CPAA 83BIR 01 1 56 35 lENA 81GLA 04

107 SSMS 85CLA 02 1 57.5 FAA 85X1

01 114 13 CPAA 85CLA 02 1

1

59

62.5

1

1

35 lENA

WXRF

80GLA

84KYL

03

01 W 1

1 Gd (uq/g)

6.7 0.3 CPXRF 84AHL 01 1 8.4 0.1 ITNA 85FIL 01 1 15.3 0.2 TCGS 79FAI 01 8.54 6 EXRF 84JEN 01 1 16.3 0.8 TCGS 85V0G 01 8.6 6 EXRF 84JEN 01 1 17 2 4 TCGS 85GLA 05

8.83 0.43 ICPES 84NAD 01 1 18 2 4 TCGS 85GLA 05

8.84 AA 82GLA 02 1 23.5 0.3 TCGS 80AND 01 8.88 0.07 AA 82NAD 02 1 25 2 ITNA 84SUZ 02

9.16 0.01 ICPMS 86SCI 02 1 9.21 0.1 ICPES 82NAD 02 1 Ge (ug/g)

9.23 0.09 35 ITNA 81GLA 02 1 9.24 0.13 17 ITNA 84KYL 01 1 33.5 0.7 COLOR 84SHI 01 9.26 0.02 16 EXRF 82PEL 01 1 33.8 3.4 ICPES 84NAD 02

9.2967 0.2097 ICPES 85PEA 01 1 34 6 EXRF 84JEN 01 9.3 0.02 16 EXRF 82PEL 01 1 34 6 EXRF 84JEN 01 9.3 0.1 ICPES 85HAR 01 1 34 2 CPXRF 84AHL 01

9.36 0.02 11 ICPES 85SAT 01 1 9.36 0.49 35 NAA 81GLA 04 1 H20-T (%)

9.38 0.07 ICPES 84B0T 01 1 9.4 0.1 5 lENA 80GLA 03 1 0.35 FD 80KHA 02

9.4 0.3 12 ITNA 82SUZ 02 1 9.43 0.17 17 ITNA 84KYL 01 1 9.48 0.02 16 EXRF 82PEL 01 1 9.49 0.1 ITNA 84GLA 02 1 9.5 0.15 ITNA 85VOG 01 1 9.5 0.3 ITNA 80GAR 01 1 9.5 0.3 12 ITNA 82SUZ 02 1 1633A-7
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Hf (ug/q) K (%) cont.

6.3 0.7 9 ITNA 82SUZ 02 1 1 .88 0.04 ICPES 82NA0 02

6.6 ITNA 82GLA 02 1

1 OO

1 .88 A 4 0.1 35 ITNA 81GLA 04

7 0.2 17 ITNA 84KYL 01 1 1 .89 A AO 0.02 4 Z16 EXRF 82PEL 01

7 0.6 ITNA 85FIL 01 1 1 .9 A AO 0.02 16 EXRF 82PEL 01

7.2 0.3 35 ITNA 81GLA 02 1 1 .909 A A07 0.083 ICPES 85PEA 01 7.2 A O 0.8 9 ITNA 82SUZ 02 1 1 .92 A A/ 0.04 ITNA 85VOG 01

7.31 0.37 ITNA 85SUN 01 1 1 .93 A A7 0.03 AA 82NAD 02

7.4 0.4 ITNA 84GLA 02 1

•4 f\l 1 .94 A 4 4 0.11 TOGS 85VOG 01 7.5 0.4 17 ITNA 84KYL 01 1

4

1 .96 A AO 0.02 AA 82GLA 02

7.6 0.2 35 NAA 81GLA 04 1 1 .97 0.04 TCGS 79FAI 01 7.6 0.2 ITNA 85VOG 01 1 1 .97 0.04 D TCGS 80AND 01

f .6 U. J

f TU A

1 1 NA 84SUZ 02 1\ .yy U.Uj 7ej5 ItNA 80GLA 03

I . to I TNA 80GAR 01 1 o no U.UO ILrbS 85HAR 01 7.8 0.2 35 lENA 80GLA 03 1 2.29 6 EXRF 84JEN 01

O 7 4 2.31 6 EXRF 84JEN 01

Hq (ng/g) 1

1 LVAA 82GLA 02 1 151 12 CVAA 82D00 01 1 13.9 0.4 GAMMA 84R0S 03

192 8 ICPMS 86SCI 02 1 La (ug/g)

Ho (uq/q)

62 2 ITNA 82SUZ 02

2.9 0.4 ITNA 84SUZ 02 1 66 2 ITNA 84SUZ 02

79 ITNA 84GLA 02

I (uq/g) 1 79.4 4 7

1 .3 4 ^17 ITNA 84KYL 01 ry.y

4 71 f

f Til A

1 INA 84KYL 01

< 4.5 ITNA 84SUZ 02 1 81 4

1 ITNA 82GLA 02

< 5 L ITNA 82SUZ 02 1 83 4 ^5 t TU A ITNA 81GLA 04

83.8 41

ff TUA ITNA 85SUN 01

In (ng/g) 1 o/84 c

t TUA ITNA 82GRA 01 84 6 35 lENA 80GLA 03

151 16 ITNA 82SUZ 02 1 87.9 7 ITNA 830BR 01

160 10 FAA 85X1

A

02 1 89 5 ITNA 85FIL 01

160 30 ITNA 830BR 01 1 on o 90.2 o.y fUNA TUA 85VOG 01 93 2 ICPES 85HAR 01

K (%) 100 23 ITNA 80GAR 01

1.7 0.06 ICPES 84NAD 01 1 Li (uq/q)

1 .71 0.09 CPXRF 84AHL 01 1

1 .77 0.23 ITNA 85FIL 01 1 100 OES 83MIL 01

1 .8 0.07 CPXRF 80KIR 01 1 151 4 C15 ICrcS 84B0T 01

1 .82 ITNA 84GLA 02 1

4 07 lor o ICrcS 84NAD 01

1 .84 0.14 ITNA 80GAR 01 1 f^DA A LrAA 83BIR 01

1 .85 0.02 ICPMS 86SCI 02 1 t oc

1 .85 0.02 AA 82HAR 01 1

1 .85 0.05 ITNA 85SUN 01 1 1.86 0.06 ICPES 84B0T 01 1 1.86 0.089 ITNA 830BR 01 1 1.86 0.12 ITNA 82SUZ 02 1 1.87 0.02 16 EXRF 82PEL 01 1

1633A-8
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Referenee

Lu (ug/g)

1

1 Mn (uq/q) eont.

0.93 0. 09 ITNA 80GAR

1 01 1 230 ICPES 82NAD 02

0.97 0. 25 ITNA 82GLA 02 1 260 20 35 lENA 80GLA 03

0.99 0. 02 17 ITNA 84KYL 01 1 277 7 ITNA 84GLA 02

1.04 0. 07 ITNA 85SUN 01 1 1000 6 EXRF 84JEN 01 1.06 0. 13 ITNA 84GLA 11 1 1010 6 EXRF 84JEN 01 1.17 0. 03 17 ITNA 84KYL 01 1 1.33 0. 1 ITNA 84SUZ 02 1 Mo (uq/q)

1.44 0. 12 ITNA 82SUZ 02 1

1

•

26 3 CPXRF 84AHL 01 Mg (uq/g) 1

1

27

28.8

6

2.3

ITNA RTNA82SUZ

84M0K

02

02

1400 200 AA 82HAR 01 1 29.2 0.6 ICPMS 86SCI 02

3800 700 CPXRF 80KIR 01 1 30 4.2 CPXRF 80KIR 01 3900 200 ICPES 84NAD 01 1 31.3 3.6 ITNA 85V0G 01 4200 AA 82GLA 02 1 32 2 ICPES 84B0T 01 4440 40 I CRMS 86SCI 02 1 36 1 35 lENA 80GLA 03

4500 500 ITNA 80GAR 01 1 4520 80 ICPES 84B0T 01 1 Na (ug/g)

4590 30 AA 82NAD 02 1 4600 70 ICPES 82NAD 02 1 1484 ICPES 85PEA 01 4660 50 ICPES 85HAR 01 1 1560 70 AA 82NAD 02

4710 80 11 ICPES 85 SAT 01 1 1600 100 AA 82HAR 01 4760 200 11 ICPES 85SAT 01 1 1670 20 ICPMS 86SCI 02

4800 CPAA 83BIR 01 1 1680 90 ITNA 830BR 01 4824 ICPES 85PEA 01 1 1700 70 ICPES 82NAD 02

5700 ITNA 85GAU 04 1 1720 50 ITNA 80GAR 01 6200 500 lENA 85GLA 02 1 1730 10 ITNA 84GLA 02

8000 1300 ITNA 82SUZ 02 1

1

1740

1740

70

100 35

ITNA ITNA85VOG

81GLA

0104

Mn (ug/g> 1

1

1750

1760

50 ITNA

ITNA

82SUZ

82GLA

02

02

167 7 ITNA 85FIL 01 1 1760 60 ICPES 85HAR 01 167 9 AA 82HAR 01 1 1760 80 ICPES 84B0T 01 170 24 ITNA 82SUZ 02 1 1769 CPAA 83BIR 01 173 5 ICPES 85HAR 01 1 1770 50 ITNA 85SUN 01 180 11 ICPES 85SAT 01 1 1770 80 ITNA 85GAU 04

181 9 ITNA 85SUN 01 1 1800 100 ICPES 84NAD 01 182 ITNA 85GAU 04 1 1800 100 35 ITNA 81GLA 02

182 3 35 ITNA 81GLA 02 1 1900 70 17 ITNA 84ICYL 01 184 7 ICPES 84NAD 01 1 2020 400 ITNA 82SCH 05

185 11 ITNA 830BR 01 1 2100 600 TCGS 79FAI 01 188 1 11 ICPES 85SAT 01 1 2100 600 D TCGS 80AND 01 189 2 ITNA 85VOG 01 I 2200 600 CPXRF 80KIR 01 189 5 ICPES 84B0T 01 1 190 15 D TCGS 80AND 01 1 Nb (uq/g)

190 15 TCGS 79FAI 01 1 191 4 ITNA 80GAR 01 1 24 3 CPXRF 84AHL 01 195 15 CPXRF 80KIR 01 1 31.5 2 UXRF 84KYL 01 200 56 CPXRF 84AHL 01 1 206 7 ICPMS 86SCI 02 1 210 50 35 ITNA 81GLA 04 1

1633A-9
TABLE 1633A-2: INblVtDUAL DATA FOR NBS SRM 1633A (coHt.)

Cone Uncer Coth Method Reference Cone Com Method Reference

Nd (ufl/g) Pb (Ufl/El) coht

65.6 HA tCdS 79Mt 01 n 6 EXhF 84JEN 01

66 5 TCGS 80AHD 01 H i POT 84PIN 01

fi 3 35 lENA 80GLA 03 AA 84TER 01 77.3 ITNA 85 SUN 01 fi 6 EXRF 84JEN 01 ITNA 84SU2 02 n

it h 11 ICPES 84B0T 01 lis 7 12 ITNA 82SUZ 02 n

fs.i

CPXRF 84AHL 01

13 12 iTNA 82SUZ 02 1 UXRF 84KYL 01 75.8 EXhl= 84PIN 01

Hi (ua/fl) 75.9 ICPES 85NAR 02

92 8 CPXRF 84ANL 01 Pb-210 (DCi/a)

97 36 ITNA 85FIL 01

IciS 6 EXRF 84JEN 01 3.4 0.6 GAMMA B4R0S 03

106 6 01 3.9 0.6 84R0S 03

11^ 4.8 mm 01

117 6 35 lENA 80GLA 03 Po-210 (pCi/g)

119 ICPES 84B0T 01 124 VOLT 84Bt;A 01 3uH 0.15 RA§ 84R0S 03

1Z7 1 ICPES 85HAt% 01 128 12 ITNA 82SUZ 02 PI- (ua/q)

132 i I CRMS d6SCl 02

133 COLOR 01 17.9 1.7 12 ITNA 82SUZ 02

133 A 11 ict»^s 8SSAT 01 18.9 1.1 12 ITNA 82SUZ 02

134 OJ AA d4kAt 01 138 UXRF 64kYL 01 Ra-226 (DCi/fl)

139 7 12 tTNA 82SiUZ 02

140 11 ICPES 85SAT 01 0.2 GAMMA 84R0S 03

0 (%) Rb (ug/g)

47.66 0.!^ 34 14NAA 80I(HA 02 121 f CPXRF 84AHL 01 124 11 tftlA 82SUZ 02

130 U ItMA 80GAR 01 134 1 itMA 84GLA 0^

m 10 teNg tMi 01 134 16 !9 MAA 81GLA 04

1320 30 tCPES 84B0T 01 135 & 84JEN 01 1400 40 ICPE8 84NAD 01 136 84JEN 01 1700 81 tun 01 136 i itNA 82SU2 oi

1744 iepES 01 140 tt^A 85SUN 01

1800 300 ICPES 82NAD 02 140.7 2 Mi^ 84kYL 01 1840 120 tCPMS 86SCt 02 147 6 m ifNA BiGLA 02

2000 82MAD 02 150 IS* BOklR 01

163 tiNA 80GLA 03

170 iTNA eSFIL 01

51 12 11 ICPES 84B0T 01 S (Ufl/Q)

60 10 tCPES 85HAR 01 1200 ICPES 85PEA 01

64 13 ICPES 84HAD Ol 1350 ICPMS 86SCI 02

65 S«7 CPXRF dOKIft 01 2300 m CPXRF 84AHL 0,

70.4 1.1 iCPHS 865CI 02 2700 teos 80AND 01 71.8 bill iDMS 83B»iO 01 g700 m im 79FAI 01

1633A-10
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Cohe Jncer Com Method Reference Cone Uncer Com Method Reference

S-32/34 Cratio) Se (ug/g) cont

22.6A1 I DNS 84KEL 01 9.4 0.3 35 RTNA sIgla 01 9.4 0.5 RTNA 81SL0 01 S-33/34 (ratio) 9.5 1.2 CPXRF 84AHL 01 9.8 0.5 HAA 85YAM 01 0.1781 tDMS 84KEL 01 10 2 35 IENA 80GLA 03

10.2 0.6 9 ITNA 82SUZ 02

Sb (Ua/9) 10.4 5.4 ICPES 84B0T 01 10.6 tCPES 85NAft 02

4.a 11 HAA 82CRO 03 10.62 0.09 HAA 85CHA 01 AF 85NAI) 02 10.7 0.8 35 NAA 81GLA 04

6J 8.8 ITNA 82SUZ 02 10.8 0.3 D HAA 84IMA 03

6.3 8iS 17 ItNA 84KYL 01 10.8 0.3 7 HAA 84IMA 01 6.4 8.4 17 ITNA 84KYL 01 12 5 ICPMS 86SCI 02

11 HAA 82CR0 03 12.7 1.3 itNA 84SUZ 02

H 0.4 HAA 85YAH 01 13 3 itNA 85FIL 01 6iA ITNA 82GLA 02

A.SS 0.28 tei»M8 86SCI 02 g{ (X)

6.9 e.s ITNA 85VOQ 01 6t9 ITNA 85FIL 01 18 0.93 CPXRF 80KIR 01

6.9!) O.gg 35 ITNA 81GLA 02 18.5 1.1 ICPES 84NAD 01 fJ 0.2 RTNA 81SL0 01 20.4 1.1 CPXRF 84AHL 01 0.39 ITNA 85SUN 01 81 8 tt^OS 85V0G 01 0.5 35 lENA 80GLA 03 22.16 0.29 ICPMS 86SCI 02

^8 1.9 ITNA 80GAR 01 22.2 0.4 TCGS 79FAI 01 6.96 HAA 84TER 04 22.2 0.4 D TCGS 80AND Ol

10.1 Sti 13 ict>es 84B0T 01 22.4 6 EXRF 84JEN 01 22.5 6 IXRIi 84JEN 01 22.9764 0.0934 ICPES 85PEA 01

34

23 0.2 16 EXRF 82PEL Ol

1 ttMA 82SUZ 02 23.13 0.2 16 EXRF 82PEL 01 14 4.8 8okii; 01 23.16 0.2 16 EXRF 82PEL 01 16 ITNA 82GLA 02 23.37 0.23 ICPES 82NAD 02

If 8 ITNA 8SFIL 01 23.5 0.2 11 ICPES 85SAT 01 38.6 8if 17 itNA 84KYL 01 23.9 0.5 AA 82GLA 02

38.9 8.8 ifMA 85SUN 01 23.9 0.5 35 IENA SOGLA 03

19 8 ITNA 8AGLA 02 84 0.3 11 ICPES 85SAT 01 39.8 0;8 17 itNA 84KYL 01 24.2 0.8 AA 82NAD 02

40 1 3S ItMA 81gLA 02

40.3 85HAR 01 Sm (ucj/fl)

40.3 8J ttiilA 85VOQ 01 48.6 itNA eOGAti 01 14.5 1.3 35 ITNA 81GLA 04

41 8 IS itNA 81GLA 04 IS 1 ItNA 85FIL Ol 43 1 35 IENA SOGLA 03 16 0.2 tCdS 79FAI 01 18 0.2 D TCGS 80AND 01

16.1 1.5 4 TCGS SSQLA 0^

16.2 1.5 4 TCGS 85GLA OS AF i§ 16.3 0.5 itNA 85SUN 01

r 6 EXRF B4JEN 01 16.4 0.1 itNA 82GLA 02

f 6 EX^F 84JEN 01 16.6 0.3 itNA 85VOG 01 7.8 L\ 80KiR 81 16.7 itNA 84GLA 02

8.8 8.4 9 ItNA 8ZSU2 0!> 16.9 0.5 teas 85VOG Ol

1633a- 11
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Sm (ug/g) cont.

1

1 Tb (ug/g)

17 0.3 17 ITNA 84KYL 01 1 2.1 0.1 ITNA 82SUZ 02

17.1 0.2 17 ITNA 84KYL 01 1 2.1 0.2 ITNA 84GLA 02

18.8 0.6 ITNA 830BR 01 1 2.2 0.1 ITNA 84SUZ 02

19.4 0.7 ITNA 82SUZ 02 1 2.3 0.7 ITNA 80GAR 01 20 4.4 ITNA 80GAR 01 1 2,5 0.1 17 ITNA 84KYL 01

21 1 ITNA 84SUZ 02 1

1

2.6

2.75

0.1

0.18

17 ITNA

ITNA

84KYL

85SUN

01

01 Sn (ug/g)

1

2.8

2.9

0.5

0.1

35

35

NAA

lENA

81GLA

80GLA

04

03

3.96 0.12 I CRMS 86SCI 02 1 4.7 1.7 ITNA 85FIL 01 6.3 0.2 FAA 84L0N 01 1 6.36 0.15 FAA 85TER 01 1 Te (ug/g)

14.8 AF 85NAR 02 1 18.5 ICPES 85NAR 02 1

1

<

<

3.5

6.6 L

ITNA

ITNA

84SUZ

82SUZ

02

02

Sr (ug/g) 1

1 Th (uq/g)

717 26 ICPES 84NAD 01 1 740 20 5 lENA 80GLA 03 1 11 6 EXRF 84JEN 01 742 23 ITNA 85SUN 01 1 11 6 EXRF 84JEN 01 750 40 CPXRF 84AHL 01 1 18 3 CPXRF 84AHL 01 770 35 lENA 81GLA 04 1 22.4 ITNA 82GLA 02

790 30 ICPES 84B0T 01 1 23.2 0.8 ICPMS 86SCI 02

790 79 ITNA 85FIL 01 1 24 2 ITNA 85FIL 01 813 70 ITNA 830BR 01 1 24.3 3.8 12 ITNA 82SUZ 02

815 7 lENA 84GLA 02 1 24.6 0.9 35 NAA 81GLA 04

815 10 11 ICPES 85SAT 01 1 24.6 1.1 35 ITNA 81GLA 02

819 54 ITNA 80GAR 01 1 24.7 1.2 ITNA 85VOG 01 825 40 CPXRF 80KIR 01 1 24.7 1.4 17 ITNA 84KYL 01 829 22 lENA 84GLA 11 1 24.8 0.5 ITNA 84GLA 02

834.5 2 WXRF 84KYL 01 1 24.8 1.6 ITNA 80GAR 01 840 10 ICPES 85HAR 01 1 25 0.7 ITNA 84SUZ 02

840 30 5 lENA 80GLA 03 1 25 1 35 lENA 80GLA 03

840 40 12 ITNA 82SUZ 02 1 25.6 1 17 ITNA 84KYL 01 850 70 12 ITNA 82SUZ 02 1 25.6 2.8 ITNA 86GAU 01 882 6 EXRF 84JEN 01 1 26 0.4 ITNA 85SUN 01 890 6 EXRF 84JEN 01 1

1

26

27.9

1.3

1

12 ITNA WXRF

82SUZ

84KYL

02

01

Ta (ug/g) 1 28 8.3 CPXRF 80KIR 01

1.71 0.05 ITNA 82SUZ 02 1 1.8 0.07 ITNA 84SUZ 02 1 Th-232 (pCi/g)

1.8 0.1 ITNA 84GLA 02 1 1.8 0.12 35 ITNA 81GLA 02 1 2.4 0.2 GAMMA 84R0S 03

1.8 0.2 35 NAA 81GLA 04 1 1.94 ITNA 82GLA 02 1 2.0 0.1 17 ITNA 84KYL 01 1 2.0 0.5 ITNA 80GAR 01 1 2.1 0.2 35 lENA 80GLA 03 1 2.11 0.16 ITNA 85SUN 01 1 2.3 0.1 17 ITNA 84KYL 01 1 2.3 0.2 ITNA 85FIL 01 1

1633A-12
TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

i

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ti Cuq/q)

1

1 U (uq/q) cont.

6660 6 EXRF 84JEN

1 01 1 10.3 0.4 ITNA 82SUZ 02

6700 200 ICPES 84NAD 01 1 10.3 0.4 DNA 84GLA 11 6710 6 EXRF 84JEN 01 1 10.4 0.1 DNA 85GLA 04

7400 200 16 EXRF 82PEL 01 1 10.4 0.3 17 DNA 82C0N 01 7700 300 ICPES 84B0T 01 1 10.4 0.5 ITNA 85VOG 01 7800 300 ITNA 82SUZ 02 1 10.4 0.8 DNA 8^>GLA 02

7880 540 ITNA 830BR 01 1 10.47 0.09 35 DNA 80GLA 01 7940 90 11 ICPES 85SAT 01 1 10.47 0.15 DNA 86GAU 01 8000 40 ICPHS 86SCI 02 1 10.6 0.4 35 NAA 81GLA 04

8000 600 35 NAA 81GLA 04 1 10.7 0.3 17 DNA 82CON 01 8000 800 CPXRF 80KIR 01 1 11 2.7 CPXRF 80KIR 01 8060 370 ITNA 80GAR 01 1 8100 100 ICPES 85HAR 01 1 U-238 (pCi/q)

8200 700 35 ITNA 81GLA 02 1 8300 ITNA 84GLA 02 1 3.6 0.3 GAMMA 84R0S 03

8300 500 CPXRF 84AHL 01 1 8320 70 ITNA 85V0G 01 1 V (ug/q)

8386 ICPES 85PEA 01 1 8400 60 ICPES 82NAD 02 1 206 56 CPXRF 84AHL 01 8400 100 35 lENA 80GLA 03 1 271 14 ITNA 85 SUN 01 8400 100 D TCGS 80AND 01 1 277 5 11 ICPES 85SAT 01 8400 100 16 EXRF 82PEL 01 1 279 8 ICPES 84NAD 01 8400 100 16 EXRF 82PEL 01 1 280 ICPES 81 UAL 01 8400 100 TCGS 79FAI 01 1 280 18 CPXRF 80KIR 01 8600 500 TCGS 85V0G 01 1 288 20 ITNA 830BR 01 8855 830 ITNA 85SUN 01 1 289 3 ITNA 85VOG 01 9000 AA 82NAD 02 1 290 20 ITNA 82SUZ 02

9000 1440 ITNA 85FIL 01 1 290 20 35 lENA 80GLA 03

\ 1 292 16 35 ITNA 81GLA 02

Tl (uq/q) 294

295

28

5

35 ITNA ICPES81GLA

85HAR

04

01 4.4 1.3 CPXRF 80KIR 01 1 301 8 ITNA 80GAR 01 5.7 0.2 ICPMS 86SC! 02 1 304 5 11 ICPES 85 SAT 01 5.7 0.7 lENA 85RUC 01 1 305

324

516

ICPES

ICPMS

84B0T

OOSCl

01

Tm (uq/q)

1

344

360

30

40

ITNA TCGS

85FIL

79FAI

01

01 2.4 0.1 ITNA 84SUZ 02 1 360 40 D TCGS 80AND 01

U (ug/g)

1

1 U (uq/g)

8.9 0.7 ITNA 85FIL

j 01 1 4.71 0.37 ITNA 85SUN 01 9.66 0.25 ITNA 85SUN 01 1 5.4 0.4 35 lENA 80GLA 03

9.7 0.8 ITNA 84SUZ 02 1 5.4 0.4 D NAA 81GLA 04

9.83 0.9 lENA 830BR 01 1 5,4 0.8 ITNA 830BR 01 10.2 0.02 ICPMS 8A'^CI 02 1 5.9 0.4 ITNA 82SUZ 02

10.2 0.1 35 lENA 80GLA 03 1 6.4 0.6 ITNA 84SUZ 02

10.2 0.2 DNA 80GAR 01 1 6.9 1.2 RENA 82GLA 02

10.2 0.3 DNA 82GLA 02 j 10.2 0.8 FLUOR 86KAN 01 1 10.3 0.2 DNA 85GAU 04 1

1633A-13
Cone

TABLE 1633A-2: INDIVIDUAL DATA FOR NBS SRM 1633A (cont.)

Uncer Com Method Reference I

Y <ug/g?

74

81

82

89

101,4

Yb <U9/g)

6.02

6.9

7.2

7.5

7.5

7.5

8.2

8.3

10

zn (ug/g)

189

191

191

196

201

218

220

220

222

225

226

230

230

233

235

237

243

245

250

250

256

263

zr (ug/g)

220

262.1

300

370

400

410

5 CPXRF 84AHL 01 6 EXRF 84JEN 01 6 EXRF 84JEN 01 4 ICPES 85HAR 01

1 WXRF 84KYL 01

0.26 ITNA 85SUN 01 0.3 ITNA 82SUZ 02

0.3 ITNA 84GLA 11 0.2 17 ITNA 84KYL 01 0.3 17 ITNA 84KYL 01 0.5 ITNA 82GLA 02

35 ITNA 81GLA 04

0.7 ITNA 8ASUZ 02

1.8 ITNA 80GAR 01

6 AF 84NAR 02

ICPES 85NAR 02

6 AF 84NAR 02

AF 85NAR 02

11 CPXRF 84AHL 01 18 CPXRF 80KIR 01

10 ICPES SABOT 01 50 ITNA 80GAR 01 7 5 lENA 80GLA 03

32 AA 82HAR 01

19 ICPES 84 NAD 01 AA 82GLA 02

8 ICPMS 86SCI 02

3 11 ICPES 85SAT 01 6 EXRF 84JEN 01 6 EXRF 84JEN 01

10 11 ICPES 85SAT 01

3 ICPES 85HAR 01 20 12 ITNA 82SUZ 02

30 12 ITNA 82SUZ 02

12 5 lENA 80GLA 03

2 WXRF 84KYL 01

13 CPXRF 84AHL 01

1.5 WXRF 84ICYL 01 30 5 lENA 80GLA 03

50 5 lENA 80GLA 03

50 12 ITNA 82SUZ 02

40 12 ITNA 82SUZ 02

1633A-14
c

CO8

I— toc

0)

oc

O « (M<

-Joc

o < 0£

_J -J uO (— O O or: UJ —

a. Q.

X I to

fM

+1

00to

in ^

to -Jo T- O

O

m

o »-

<\j rj (M f\i

X

o

o

to

o

(J oo '—

c

(DVX ton8

(A

c > o(/> -Jo H

_J z c

UJ3u- z: z»^

CA

C

_l<»—

UJc

X «) UJ z u<

t—

to

UJ z o

oc z

(/> <

vt

CDz

oeou. z < < <a UJ£ oUl

_i

QLc

:oM

</>

o(J) (/> z

to UJ •H

(/> z c o UJ u 0) _i z CO<

too

+1

in

to

O<M

toH

to

in to

r

(M in «

>«•

CO

ino in

o

m in ^0

O to • m o to in o

+4 +1 • M

HM

n

M N.H *\ CO 00 to to

o

o

o t^ oO

o r-.

o

o to

too

to

oo tvj 00 t\j e\j ot^ 8:

fM 1 t 1 1 1 1 1 1 1 • 1 1 1 1 1 1 1 o 1 1 1 1 1 1 >o 1 1 i 1 LO 1 1 1 1 g 1 1 1 1 t in 1 1 t 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 ?o 1 1 > 1 1 1 1 1 to

to in

o to

o to

oO LO o O f\j in o o O 1 1 CO -3- 1 1 f\J fO 1 ro 1 in 1 1 1 1 CNJ to 1 >o 1I 1 t1 11 CO o 1 o 1 11 1 OO 1

to 1 1 o 11 1 OJ 1 11 1 1 1 1 11 CNJ 1 1 1 o 11 1 00 1 to

in in 00 to CO

s.' <Mo rvj OJ

OJ in

ro 1 1 1 to 1 1 1 1 o

a 1 1 1 ^ 1 1 o 1 o ^0 1 1 1 CO o o 1 1 1 o in 1 1 1 • 1 1 r— 1 1 1 1 to 1 1 1 ro < • 1 CM 1 1 1 to

^\ ^\ ^\

•<t to <o N. (M in

oO ro in t>-

rvj r—

o to in in o in o vO

in

oo in rj

o CVJ in

O OO (\J • o to in o 1 1 o ro

"H in in

H +1H •H 1 in •H 1 1 -H +1

H

(NJ (\J ro CO 1 1 1 O CO o t^ O fSJ ro

o <M

o

o t^

<> oo" to in to

too

+1

00o

too

•H

W

GO

c

(0

01

in

o0>

in

to

to(M

OCM

to

inH

fMoo

•H

o(Mto

moo

•H to

fM

D) O) O) D) ) O) ) O) o> O) o>

t—

\

\

\ •V,

\ ~v\ »^

\ o> O) CD CD O) O) O) O) o> z—

c c c c 3 c 3 c C c C 3 3 c 3 C c 3 3 3 3 c

D) U)O O) O) 0>

»s »s

O) o>OO O)

C 3 C 3 3 m_lUJ

u> 3 < <

<U I- (0 X)

—

m CD u u o

O t_ 3 u u u 3 <U 4) CJ>

co .„ ^ z z z a. t/t (A vt VI U> vt

W > > c

1634-1
TABLE 1634-2: INDIVIDUAL DATA FOR NBS SRM 1634 (revised 3/1/86)

Cone uncer LOfn ncinoa Reference | Cone uncer LOm necnou Reference

As (ng/q)

1

1 Cu (na/Q)

56 ITNA 77flL 01 1 < 800 L EXRF 79GIA 01 62 13 ITNA 85FIL 02 1 220 20 ITNA 73SHE 01 63 3 ITNA 78BER 02 1 70 ITNA 78UEA 01 1 Eu (ng/g)

yj K 1 NM 740RV 01 1 120 ITNA 81SHA 01 1 11 4 ITNA 85FIL 02

Au (ng/q)

1

1 Fe (ua/q)

24.5 0,7 ITNA 73SHE

1 01 1 10.8 3.3 32 EXRF 78ICUB 01

1 12.3 POL 74MAI 01 Br (ng/g) 1 12.4 1.6 ITNA 73SHE 01

1 12.5 2.2 UU 77PAC 01 39 ITNA 77FIL 01 1 12.7 3 EXRF 80SCH 07

39.1 5.3 UU 77PAC 01 1 13 ICPES 79MER 01 40 ITNA 78WEA 01 1 13.4 0.2 ICPES 83BR0 02

41 4 ITNA 78BER 02 1 13.5 1.2 ITNA 81SHA 01 240 70 ITNA 73SHE 01 1 14 1.5 EXRF 79GIA 01 330 90 ITNA 85FIL 02 1 14.1 0.6 AA 74RAI 01

1 14.2 1.5 ITNA 78BER 02

Ca (uq/g) 1 14.4 1.7 32 EXRF 78KUB 01

15.1 2.4 32 EXRF 78KUB 01

15 2 ITNA 73SHE 01 1 16.2 2.8 32 EXRF 78KU8 01 16.9 2.5 32 EXRF 78KUB 01 ca (ng/g) 5(1 1 1 NA f A r I L Ul

1 20 2 ICPES 84BAR 03

in1 u

1L DTUA K 1 nn 740RV 01 1 I

1 TUA 1 nn 7ftuPA r OWCM ni\J i

5 FAA 74RAI 01 1 27.5 6.5 ITNA 85FIL 02

CI (uq/q)

1

1 Hq (nq/q)

7.8 0.5 UU 77PAC

1 01 1 < 10 L ITNA 81SHA 01 8 ITNA 78UEA 01 1 < 10 ITNA 77FIL 01 8.4 0.5 ITNA 78BER 02 1 2.3 0.2 RTNA 84DEL 01

18 0.7 ITNA 73SHE 01 1 2.3 0.2 RTNA 740RV 01

1 22 15 ITNA 73SHE 01 Co (nq/g) 1

1 K (ug/g)

250 .10 ITNA 73SHE 01 1 301 ITNA 77FIL 01 1 315 ITNA 77FIL 01

301 14 UU 77PAC 01 1 310 15 ITNA 78BER 02 1 Mn (ng/q)

330 60 ITNA 85FIL 02 1 400 ITNA 78WEA 01 1 110 10 ITNA 78BER 02

1 190 ITNA 73SHE 01 Cr (nq/q) 1 200 ITNA 81SHA 01 320 ITNA 78WEA 01 80 ITNA 81SHA 01 1 93 ITNA 77FIL 01 1 Mo (nq/q)

100 ITNA 78WEA 01 1 116 35 ITNA 73SHE 01 1 870 80 ITNA 78BER 02

220 60 ITNA 85FIL 02 '

1634-2
TABLE 1634-2: INDIVIDUAL DATA FOR NBS SRM 1634 (cont.)

Cone UncGP Cofn Reference | Unccr Cofn Lnou Reference

1

1

1

Sb (na/a)

11 ? ITMA 1 1 nn 77FIL 01 1 in 1 1 NM 77FIL 01

11 y n 7 1 II

1

77PAC 01 1 in 1 1 nH 78WEA 01 1? ITNA 78UEA 01 1 14 fI TMA 1 nn 73SHE 01 17 ? 1 1 nn 78BER 02 1 on 1 in I

1 TUA 1 NH 85FIL 02

1 0 1 1 Nn 85FIL 02 1

1 (ug/q) 1

1 1 n 7A T TUA 1 1 NA 85FIL 02

"71 1 9 1 nnAA 74RAI 01 1

11 PXPF 78KUB 01 1 se \ng/g;

32 1 -6 EXRF 79GIA 01 1 2 32 FXPF 78KUB 01 1 138 AO PTMA 740RV 01

1 32 cAi\ r 78KUB 01 1 151 T

i TMA 1 nn 85FIL 02

33 2 3 ITNA 85FIL 02 1 170 TTMA 1 1 nn 77FIL 01 35 0 3 ICPES 83BR0 02 1 190 30 TTMA i D nn 73SHE 01 35 2 84BAR 03 1 200 1TTMA 1 nn 78WEA 01 2c FVDF 78KUB 01 1 35 2 PDI 74MAI 01 1 V (ug/g;

1

1 FVDF CAi\ r 78KUB 01 1

m f 79MER 01 1 1AlO 1 1 Nn 73SHE 01 36.9 2 7 tAi\ r 80SCH 07 1 283 121 b bAnr 79GIA 01 37 2 ITMA 78BER 02 1 300 ITMA 1 1 Nn 81SHA 01 37.4 ITNA 77FIL 01 1 301 15 TTMA 1 1 nn 85FIL 02

37.4 1.5 uu 77PAC 01 1 303 18 32Jb bAi%r 78ICUB 01 38,1 IDMS 74M00 01 1 306 24 bAi\r 80SCH 07

38.1 6 IDMS 74MOO 01 1 310 UNA 78UEA 01 38.2 6 IDMS 74M00 01 1 310 S 32Jb EXRF 78KUB 01 39.5 2.26 ITNA 73SHE 01 1 311 7 32 EXRF 78ICUB 01 312 1A L Mil 77PAC 01 (ng/g) ] 314 ICPES 79MER 01

1 317 6 GC 81DIL 01 < 500 ICPES 79MER 01 1 318 ICPES 84BAR 03

< 1500 1 FypF cAi\ r 79G1A 01 1 J 1 o 1 J ITUA 1 1 nn 78BER 02

41 pni 74MAI 01 1 /H I rPFC 83BR0 02

50 FAA inn 74RAI 01 1 X2X oy Jb CAKr 78iaJB 01

1

1 1 Jb FYDF CAKr 78KUB 01

(%")

1 o • o AA 74RAI 01

2 0.1 TITR 80MCC

1 01 1 7n f t in In \ Lr\ lug/g;

2 0.2 MECA 80HCC 01 1 2.04 0.39 ITNA 73SHE 01 1 < 0.6 ICPES 79MER 01 2.05 0.4 UU 77PAC 01 1 < 0.6 L EXRF 79GIA 01 2.15 0.02 ICPES 84BAR 03 1 < 1 L ITNA 81SHA 01 2.154 0.009 IC 80MCC 01 1 0.17 0.02 RTNA 740RV 01 2.17 XRF 80MCC 01 1 0.3 ITNA 78WEA 01 2.24 0.05 ITNA 81 SNA 01 1 0.48 0.12 ITNA 73SHE 01 2.24 0.05 ICPES 81UAL 02 1 1.0 0.4 ITNA 85FIL 02

2.3 0.3 ITNA 78BER 02 1

1634-3
in ^

8 5

!

I I

* t I

I

I

I

I

(M ru- C

X 01

in o

•

V V

CO

rv

K) O 28

I I

IN M

» (>4

3

9S

-1 c

I IM O

1 K S

O

I?

ma

00o

CO •- o -4- • I n

I O

^— <V «~

in (\J O 00 (M in o f\< K <v <o o

T- >0 I

I I

I (M I

r» *»

ff?

t— O

s ;3 §

1 Kl

1 5 s

i in

I

s

Ul

1^1

I >0

O OO o • so o

o o CO > r>j o

o

p

IN

«

I

n

I

00

CP •

2(

I If) «V

o

Z3

PJ >

V

m <M CO C D

CO

r— M s «

CO -o m •* G

1 o o o ^ S

r- o » o ?I 00 o iC O nj »> t

r'

» sO «* •* H o t> o •« «— in o * o V «- <— o P*J i

V V m *" 'I V $

V V V

Csl W

*

15

inm o

PJ •O «- PJ O N I I O • 1

1 K> O I

I

1 r; I PJ I

; ! y I i

tf

I?! ra

I

I I

I

i +( +1 «5

to O) o> O) Cl Ol Ol Ol Ol Ol Ol Ol O) Ol Ol

1— \ \ V.

Ol D) m on cn Ol O)

ae c 3 c 3 3 C c 3 c 3 c 5 §• ? 3 3

O)

C K

Ol O) O)

Ol3 1

OIOIDIOIOIDIDIOIOI

1

VI in 01 I- < cQ m CO u u

01—<oi-tA33aiiii UUUCJUUUJM-Cl a: V -) aX

(0 T3 .r- JQ ^

a; z a: Q- 0- (A C/> (/) V)S CO ^ w ;^ 1^

1634A-1
TABLE 1634A-2i INDIVIDUAL DATA FOR NBS SRH 1634A (revised 2/1/86)

Cone Com Reference Para Reference

As (n3/a) Cu (ua/a)

< 650 32 EXRF 83SAN 02 i IB EXRF 83SAN 02

< 650 32 EXRF 83SAN 02 T la EXRp 83SAN 02

HI 17 ITNA 85FIL 02

it,"' # 1 MM 85FIL 02

5 98 1 77 UNA 85FIL 02

Fe (ua/a)

Br (ua/a)

26 4 ICPES 84BAR 03

Q 5 32 EXRF 83SAN 02 30 4 1 1 32 bAn r 83SAN 02

0.5 32 EXRF 83SAN 02 30.8 0.4 ICPES 83MAH 05

0.88 0.19 ITNA 85FIL 02 30,8 1 1 32 EXRF aSSAN 02

k\~ 1 7.2 ITNA 85FIL 02

Ca (ua/a)

42 32 EXRF 83SAN 02

16 1

1 ICPES 84BAR 03 < 450 Won EXRF 83SAN 02

17.5 2.2 32 EXRF 83SAN 02 ?i 83SAN 02

m \m 85FIL 02

Ce (na/a)

H (u / ) 757 64 ITNA 85FIL 02

1-9 32 EXRF 83SAN 02

% 1.9 32 EXRF 83SAN 02

< 68 32 EXRF 83SAN 02 K (ug/g)

< 350 32 EXRF 83SAN 02

35 ITNA 86GAU 01 4 5 32 EXRF 83SAN 02

49.9 ITNA 83LI 01 66 32 EXRF 83SAN 02

Co (na/a) La (ua/a)

< 1400 32 EXRF 83SAN 02 2.04 0.18 ITNA 85FIL 02

< 1400 32 EXRF 83SAN 02

280 60 ICPES 83MAH 05

600 370 ITNA 85FIL 02

< 2600 32 EXRF 83SAN 02

Cr fua/a) < 2600 32 EXRF 83SAN 02

180 ICPES 83MAH 05

4.8 32 EXRF 83SAN 02 210 ICPES 85NG 01 < 4.8 32 EXRF 83SAN 02

0.6 ICPES 85NG 01 Mo ^ng/g)

0.82 0.11 ITNA 85FIL 02

110 ICPES 83MAH 05

Cs (ng/a)

N 22 9 ITNA 85FIL 02

1.23 0.02 16 83NAD 01

1634A-2
TABLE 1634A-2: INDIVIDUAL DATA FOR NBS SRH 1634A (cont.)

Cone

Na (ug/g)

Uncer Com Method Reference

P (ug/g)

1090

Pb (ug/g)

Rb (ng/g)

102 16 ITNA 85FIL 02

Nd Cug/g>

0.9 0.26 ITNA 85FIL 02

Ni (ug/g)

26 AA 85 FAB 01 26.3 2.5 ITNA 85FIL 02

27 ICPES 85NG 01 27 2 ICPES 84BAR 03

27.3 0.4 ICPES 85 FAB 01 28.4 1.3 32 EXRF 83SAN 02

28.5 1.3 32 EXRF 83SAN 02

29.2 0.5 ICPES 83HAH 05

1500

53

32

32

EXRF

EXRF

83SAN 02

83SAN 02

Cone

Sc (ug/g)

2.3

Se (ng/g)

<

<

190

Si (ug/g)

<

<

Sm (ug/g)

43

Sr (ug/g)

<

Ti (ug/g)

Uneer Com Method Referenee

1.6 ITNA

540

540

50

270

3000

32

32

32

32

3.8

4.3

4.3

32

32

EXRF

EXRF

ITNA

EXRF

EXRF

85FIL 02

EXRF 83SAN 02

EXRF 83SAN 02 ITNA 85FIL 02

83SAN 02

83SAN 02

85FIL 02

83SAN 02

83SAN 02

2.13 0.87 32 EXRF 83SAN 02 1 < 11 32 EXRF 83SAN

2.13 0.87 32 EXRF 83SAN 02 1 < 11 32 EXRF 83SAN

2.68 0.03 ICPES 83MAH 05 1

54 AA 85 FAB 01

< 610 32 EXRF 83SAN 02 1 54 4 32 EXRF 83SAN 02

< 610 32 EXRF 83SAN 02 1 54 4 32 EXRF 83SAN 02

55.5 ICPES 85NG 01 m 55.5 1 ICPES 83MAH 05

56.7 0.7 ICPES 85 FAB 01 2.12 0.01 IC 83NAD 01 1 57 2 ICPES 84BAR 03

2.82 0.1 7 NM 83LI 01 1 58.5 5 ITNA 85FIL 02

2.84 0.08 7 NM 83LI 01 1 2.848 0.09 32 EXRF 83SAN 02 1 Zn (ug/g)

2.87 0.02 ICPES 85 FAB 01 1 2.881 0.027 32 EXRF 83SAN 02 1 2.54 0.03 ICPES 83MAH 05

2.91 0.02 ICPES 84BAR 03 1 2.8 0.3 ICPES 84BAR 03

2.89 0.92 ITNA 85FIL 02

) <ng/g> 2.9 0.5 32 EXRF 83SAN 02

3 0.5 32 EXRF 83SAN 02

34 31 ITNA 85FIL 02 1

1634A-3
TABLE 16346-1: COMPILED DATA FOR NBS SRM 1634B TRACE ELEMENTS IN FUEL OIL

(revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SO

ASH ug/g 700

Al ug/g 16 As ng/g 120 ± 20

Ba ug/g 1.3

Ca ug/g 15 Co ng/g 320 ± 40

Cr ug/g 0.7

Fe ug/g 31.6 ± 2.0

HEAT BTU/lb 18100

Hg ng/g < 1 Mn ng/g 230 + 30

Na ug/g 90

Ni ug/g 28 ± 2 Pb ug/g 2.8

S % 2.80 ± 0.05

Se ng/g 180 ± 40

V ug/g 55.4 ± 1.1 Zn ug/g 3.0 ± 0.2

1634B-1
gM

">us

UJ

UJu< X

V)8 " z C

I— (0 UJ 01

Of

UJi

"8

«)c

V)c 2 5 c

4>

uU u.

I- < o o

u. a.

OQ OCU

O

X

—

00o

o • Oin o.

C\J (M

CO

o

o

Ho

(\J

>0

o

in

o

(\Jo

+)

ino

CO

CO (/i C3 ID U (J

O

CO

(O

u

in

X

oo

in

UJ

a.u

CO

CJ

«- <M

(NJ

O

>*

in

o 0£ —' X

00o fVl

XXoor\j

o

V)

UJ CO > Q. u. (J U. < u (J Of u a: cQ a:

•— •—

X I—X

O C3 ^ ^ <^ w s..^ w w

00

f\J

00 00

o in «- On • • O PJ O vj- «-

"O >o <o (NJ CO PO Pvl r-^

o >^ ^z

•*

oin

o

o ro

o

o in CJ

o •o ro ro

in 1 On in

o

o > i in

H 1 +1

H (MH •HH ro •H +4 -* 1 1 +1 1 ro ro 1 fVJ -* o O fO ro OJ o fSJ fM in CO s PvJ (M OJ CM

in CM

^\

ro rvj CNJ

PJo

00

o

•oin

o5

r^o

r>. PJ

ino

PJ

o

PvJ <oUJ

UJa

O.su

QUl

o

O

o

ro

PJ

oo

o 00 CO CO o o in o ro nO o O o 00 o r—

O ro (O

:8

CO 00 ino > in

:§ r^ ro nO vj- in «* to in CO o in ro PJ >0 PJ >o ro ro PJ •J- -4- ro ro

inoo

o CO

>0 PJ

PJo

o vO(M

N. vO

vO -4- O in PJ >J- o«- o

o

PJ

PJ

Onin

ooCO

N*oovj- in

PJ nO

PJ ro

o nO >0o On >! in «-

in «- ro

ro

00

vi- sO

o ^ ro nO • PJ PJ -in

ro nO PJ ro

0>

oo

in PJ CO

«- ro

o >0 vo roCM

O

ro

PJom

nO

o On «- «*CM

ro

oOnPJ

4 in

c (M ro ro NO PJ On PJ ro >0 PJ ro ro PJ PJ >0 PJ

K«o

ww

CM in

Ul (/>

a

oooo roo in

_j CO rS

-* OnoOo ro

ca (O

m PJmoo rooooo ro ro >o r- ro < z vO 00 >0 On o o in o

O On

1— UJ

CO

•H -*

ro

HH

V

-H

V

PJ

nO

H PJ •H +1

HM 44 ro

ro

oPJ

•H •H +4

o •N* in +4 PJ z c V O m 00 o O CO ro ro O PJ ro o O o (0 in O in PJ in vO V in On u Me On

PJ

•4-

o

ro

in ro

no' OJ

>0 PJ

ro

PJ

PJ ro CM

ao ro ro

CO in

o

oo CO 1 I o 1 1 1 1 1 1 I 1 o OB +1 1 1 O •H 1 1 1 1 1 1 1 +1 in +1 +4 z 1 r PJ 1 1 1 1 1 1 1 1 fO >0 c ro O o in O (0 PJ ro

0) PJ ro

oo

oin

mo +4 • o

roPJ

oOnOJ

I— Ul CD Ul cn Ul CD Ul Ul Ul D> CD Ul Ul \ \ \ V. V. v. «» >>. z at CD C3) CJ) C31 ai Ul Ul Ul Ul Ul Ul CD Ul CD Ul Ul 3 X c 3 C C 3 3 3 3 3 X 3 c 3 3 c 3 c 3 C c C 3 3

Ul

Ul3 »i

a

Ul Ui Ul Ul Ul c c

UJ

UJ—I

lU

00 CD

—• OJ 3 < < < < <

4)..-U C0TJ4)—'O moQOQUULJUOU 1- W) 3 t- 3 U U U O UJ UJ

4) (0 "D 4) u. u C3 C9

oPJ *- Ul 3:

1635-1
Q(ft

</) 8z c

ID Ui 4)

COuo

a:

V)

(Ao a:XofM

vj- •H vO

8:o

Of

m

Q

O

in

o

-Jz: z

CIQ

O00

-O 00

in SCJ o

cm

01 z ow c

-Jg

o

3E 5

toZ 1—

c

UJV

3L

III UJ

III f % <

HCO in

KJ>o

c

E «) oe 4J M Z

to

GDZ

ocou. UJo < z 1— < <oaUJ

_i z

«t

a.

QUIz «

1 in

C

KJ<o

UJ CO

(/>

m CO < z

UI

(Az c o <D u z

«- «- rvi o in o m o >0 «-

CO CO CO CO </> CO

UI UI UJ (/) UI CO UI UJ c/> a. u_ a. a. u_ C3 a. cs Li_ O. u. u. CL 13 u q: o CJ (J u CQ o CJ oe. u a: CJ O O X X t— CJ t— X X X X 1— ^ ^ ^\

T— fM m— IT" M in (M CO 1 1 o> in O o 1 O

ooo rg 1 <

fM fM 1 ooo <o • o

o

O 1 CD 1 o r^.

V 1 (M

V : S ro fM

fM fM fM

^-^

rvi NO h~ fM (M\^

ro

o

O

o

o

T

O 1 eo 1 1 eo

to

oo ro 1 1 • o

H •H +\ 1 (M 1 1 +1 1 1 1 1 1 t w— 1 1 1 1 i 1 H

00 eo

fM

ooo

>t

oinV in00

o*—of\l rofM

o

o

o

o +1 «- 00oo

<>fM

oro

00

fMo

fMCO

o

o fMooo

o in

o

oo in

o >* fM

O

o ro 00 ro 1 1 fM ro fM 1 1 fM <

1 fM ro fM 1 o 1 ro 1 1 1 11 1 1 1 1 CO 11 1 in 1 o 1 11 o 1 1 1 in 1 o 1 1 1 in in 1 1 o i 00 11 1 1 o 1 1 1 t 11 ro O ro •o 00

o>

o oo

o fMoo fM

fM

ro eo ro 1 O 1 s- o 1 i o O 1 1 00 ro 1 O- 1 1 00

O 1 1 1 1 1 o> 1 fM o 1 • O 1 1 ro 1 1 ] O 1 1 1 1 1 1 o N I 1 ^ 1 1 1 1 1 o ro 1 1 1 1 fM ro

>o ro «- ro fM (Mo ro fM -o ro 00 \^ s_/ fM o ro o in ro O fM -* in -o ro o NO CO o ro o- o fM 00 o 00 in o 8: o (M

o CO 1 o «- ro •o 1 1 in o in *t •H H H -H I H H H H o H +< I o 1 fM V «- V 1 1 fM

-O CO COo nOO COo

o

o ino fMo f\l >t O ro CO >o

t

o ro ro fM fM o ro

aM

CO

OOM z c

(D41

H

OO

fM

fMOOOOo

Si > O) O) a> O) o> o> at at CD \ \ \ \ \ \ \ \ \ z O) O) O) D) at ut at at 3 c c 3 3 3 c 3 3 3 C »« »S 3 3 3 3 3 >« 3 3

at at at at at \ \ D) O) 0> 3 3 3

CJ at at at at at <o Q. 3 3 3 3 3 <-

c

—

—• — 3 o>

c ni z<a XI T3

o

a. a. a. a. on

rofM ro ro ro

CO CO to (/) CO

1635-2
*j

a> Xc 1 

»- (0 UJ 4)

UJI ^x:c

0) z cQ c g 5 CO z 1— c

2?

UJ z

UJ

UJ

*~

o(/) in«

AA

Hc

X (S a£ 4) M z

vi

COo UJo < z I— < <ooUJ

_J < CLo

UJz 1 in

c

UJ to

o —1 (/> m m < z

UJ •H COz c ou Vz < «-

X

o>

o• o >oin

Crt CO

UJ (/> (/> UJ u. a. u o u. ol Qc u u u a: o X I- »- X —

U. C3 X t- O S I fM 1 O O O «- in (\j O in o o o in >o 0> V

u- o.

Qc z z z u

o oe

XZ

Z

Z » U

Xo

o 00 in o> • *j >o ^ «~ • o

o

o I >o S- >o

oo «— 1 O O O fM fM

V ...V

ooo zz o o

o

ooo

o

-*

o ^ >0 o-4-

CO>^oIf— o

inoo

^\

(M ^—

oO NO in oo 1 1 +4 M •M (M fM M 1 +1 O in 00 V 1 o 1 N- O CM O OJ in fM

>*

inoinoin

<M

U- u. u. u.

0£ Of ee

X.X

XX

^\ ^ ^% 1 <> 1 >o 1 1 in 1 1 in

in >*•

too (NJ <M 1 +1 O 1 44 +1 +1 «~ 1 in in 00 »^

o

fM >0 o

vO

in

o

00

o

ooo

oOooo 00

oO in >t COo fM

fM fO 1 -J- in 1 1 fM 1 1 1 ro 1 1 1 fM 1 1 o o 1 1 o 1 o 11 o in 11 o 1 11 11 1 11 o t 1 1 1 1 o 11 11 11 1 in 1 11 1 o 1 fM 1 in

fM -oo in

o ~*o

oR >* • m (\l f\j in CM ro «

o in

NO o o> o o 1 1^ in 1 1 o 1 1 1 O I 1 1 o 1 1 1 in 1 1 o •*

-*

o fM 1 1 1 1 1 O 1 1 1 * 1 1 1 1 in

oo fM 1 1 >o 1 1 1 fM 1 1 1 fM 1 1 1 «* 1 1 in

o in in fM t^

o in

o nj in o> *

o-o

o fM

o

ooO

o

o CO ino

o

o vO

to

m

o in >!OO f8o •*

o fM

o fM o> :SO K» nI

oo

H +<HHH •H fM •M

Ooo *) 1 O -O

H

o

o

o -HO +) +1 +1 1 o o -* o O V CO V o o o o fM o o o o in in CO

in

o

o o~O

V in

Oo fM in fM fM >* in

o in >*

(/> CO -H Z c

(S

o

o

to

tooo

o<M

o

fM

ofMO

fM

ino

fM

in

ino

o> o> O) o> o> o> O) o> \ \ \

\ O) o> o> a> tn at (3)

cc 3 3 3 cc 3 cccc

o> cn o> O) O) O)

J3oo

— •-

e

c L. (/>(/)</>(/)(/)l/>IA</>

00O f\J fM to to

fM fM fM t I I (D^ 01 ^ ^ ^ ^ •— •— —>

E ^ in 00

to to fO

fM fM fM I I I 3 3 3 3 > 3

Si > >-

C 1- rM M

1635-3
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 1635 (revised 3/1/86)

Cone

(ng/q)

<

<

<

2600

2600

2700

2800

2900

2960

3000

3000

3100

3352

3400

3400

3400

As (ng/g)

Uncer Com Method Reference

ASH (%)

4.5

4.8

Au (ng/g)

B (ug/g)

38

500

2500

100

500

200

170

300

300

100

25

400

400

400

34

34

ITNA 82SUZ 02 ITNA 86GLA 01 WXRF 82MIL 01

ITNA 84CLE 01 ICPES 84NAD 01 AA 83BET 01 AA 83BET 01 ITNA 86GLA 01 ITNA 85GAU 04 ITNA 82SUZ 02 ITNA SOGER 01 ITNA 82HAH 01 ICPES 85PEA 01 TCGS 80GER 01 TCGS 80AND 01 TCGS 79FAI 01

34

UU

CB

ITNA

85SHI 01 82HIL 01

86GLA 01

104.5 2.6 TCGS 79FAI 01 105 3 D TCGS 80GER 01 105 3 TCGS 80AND 01 135 11 ITNA 82SCH 05

Cone

Ba (ug/q)

47

67

69

70

72

74

77

81

Be (ug/g)

0.46

0.49

0.49

Bi (ug/g)

Br (ug/g)

Uncer Com Method Reference

220

6

9

17

18

24 9

34

ICPES

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA WXRF

UXRF

I 1635-4

66.23

Ca Cug/g)

4800

4900

5090

5100

5300

5400

5400

5400

5500

5500

5700

5700

5834.4

0.06

500

30

500

250

200

200

200

400

900

700

D34

34

CB

ITNA ITNA ICPES

ITNA

ITNA TCGS

TCGS

TCGS

AA

ITNA AA

ITNA ICPES

84NAD 01 82SUZ 02

85GAU 04

8PGER 01 80TOU 01 84SUZ 02

82SUZ 02

82MIL 01

0.04 11 AA 82LIN

0.01 11 AA 82LIN

0.05 11 AA 82LIN

82MIL 01

< 1 ITNA 86GLA

280 20 HAA 82NAD 01 1 0.84 0.14 ITNA 85GAU

320 FAA 82WIL 01 1 1.07 0.17 ITNA 82SUZ

330 AF 82UIL 01 1 1.22 0.24 ITNA 84SUZ

400 11 HAA 82CRO 03 1 1.5 0.07 ITNA 82HAM

400 11 HAA 82CR0 03 1 1.6 0.3 ITNA SOGER

400 50 ITNA 82SUZ 02 1 1.9 0.2 5 ITNA 80TOU

400 100 HAA 85LIN 02 1 3 34 UXRF 82MIL

430 40 RTNA 84DEL 01 1 440 50 RTNA 78GAL 01 1 C (,%) 510 40 ITNA 85GAU 04 1 530 50 ITNA 82HAM 01 1 59 3 TCGS 79FAI

700 34 UXRF 82MIL 01 1 59 3 D TCGS SOGER

700 400 ITNA 80GER 01 1 59 3 D TCGS 80AND

80SCH 02

84CLE 01 82HAM 01 84NAD 01 86GLA 01

85GAU OA

80AND 01 79FAI 01

SOGER 01 83BET 01 82SUZ 02

83BET 01 SOGER 01 SSPEA 01
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 1635 (cont.)

Uncer Com Method Reference

Cd (ng/g?

< 380 L ITNA B2SUZ 02

< 4SQ ITNA 8ASUZ 02

< 3000 L UXRF 82HIL 01 29 3 RTNA 78GAL 01

Ce (ug/g?

3.2 6.1 ITNA 84SUZ 02

3,3 12 ITNA 82SUZ 02

3.4 1? ITNA 82SUZ 02

3.4 ITNA 85GAU 04

3.5 0,5 ITNA SOGER 01 3.6 ITNA 82HAM 01

6 34 UXRF 82MIL 01

CI <ug/g)

Co <ng/g)

590 60 ITNA SOGER 01 600 150 34 FAA 83BET 01 610 180 ITNA 84SUZ 02

620 34 FAA 83BET 01 620 60 ITNA 82SUZ 02

630 40 ITNA 85GAU 04

630 50 ITNA 86GLA 01 640 ITNA 84CLE 01 650 70 ITNA 82HAM 01 700 34 WXRF 82MIL 01

Cr (ug/g?

ITNA 84CLE 01

0,? 11 AA 82LIN 03

34 UXRF 82MIL 01 ITNA 82HAM 01

Q.i ITNA SOGER 01

?'4 0.1 ITNA S4SUZ 02

0.08 RTNA 78GAL 01

6*11 12 ITNA 82SUZ 02

Cone Uncer Com Method Reference

Cr (ug/g) cont.

2.5S

2.6

2.6

2.9

3.9

4

Cs (ng/g)

0.17 ITNA B5GAU 04

34 FAA 83BET PI 0.3 12 ITNA 82SUZ 02

0.6 34 FAA 83BET 01 0.9 11 AA 82LIN 03

1 ITNA 86GLA 01

II

Cu (ug/g)

SOQ

2100

10

UXRF 82HIL 01 ITNA 84SUZ 02 ITNA SOGER 01 ITNA 82SUZ 02

ITNA 85GAU 04

26 D TCGS SOGER 01 1 3 34 UXRF 82MIL 01 26 i P TCGS SOAND 01 1 hU 0.18 RTNA 7SGAL 01 26 g TCGS 79FAI 01 1 hM 0.18 RTNA &4DEL 01 ITNA SOGER 01 1 3.6 34 FAA 83BET 01 ITNA 85GAU 04 1 3.6 0.2 11 AA 82LIN 03

28 i

IC S3NAD 01

1 3.6 1 34 FAA 83BET 01 36 34 UXRF S2MIL 01 1 h7 0.1 11 AA 82LiN 03

14 3 ICPES 84NAD 01

Dy (ng/9?

< 310

3§0

tng/g)

Eu (ng/g)

59

«1

IP

m

740

2000

40

40

2000

1QQ

7

6

ITNA 86GLA 01 ITNA 82SUZ 02

UXRF 82HIL 01 ITNA SOGER 01 ITNA 84SUZ 02

UXRF S2MIL 01

ITNA &6CLA 01 ITNA 82SUZ 02 ITNA 84SUZ Q2

ITNA SOGER 01 ITNA SSqAU 04

in 83i(NA 01 m 83BET 02

1 (6 83NAP 01

1635-5
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 163S (cont.)

0

Cone Uncer Com Method Reference Oone Uncer Com Method Reference

(ug/g) —

Hf <nfl/9) —

1340 90 ICPES 84NAD 01 «40 i A A

9 ITNA 82SUZ 02

1900 ITNA 84CLE 01 270 AO ITNA 80GER 01 2180 170 ITNA 84SIJZ 02 OAA 290 80 9 ITNA 82SUZ OlS 2200 100 TCGS 79FAI 01 290 10 ITN^

AF ^ A A M 85GAU 04

2200 100 0 TCGS 80AND 01 TAA WW ITNA

0/ 01 11 A*t B4SUZ 0«

2200 100 D TCGS 80GER 01 V / A 340 A A ITNA 86GLA 01 2200 200 ITNA 82HAH 01 2300 34 AA 83BET 01 Ha (na/aJ,-

2300 ITNA 86GLA 01 2300 200 ITNA 80GER 01 1 Wil A ITNA

0/ f1 1^ A4 B4SUZ 02

2300 ^AA 600 34 AA 83BET 01 < 90 1L

ff Til A ITNA oZSUZ 02

2320 TA70 ITNA 85GAU 04 < 13UU 1L WXRr

O^U f 1 A if 82MIL 01 2330 240 12 ITNA 82SUZ 02 5 1^ PVAA 82DOO 01 2340 140 ITNA 82SUZ 02

11 IP ITNA 82SUZ 02

2380 ICPES 85fEA 01 Ho (ng/g)

(MS/a)

<

1u UVD C WXRr

< 8 I ITNA 82SUZ 02 4* OA

ITNA 84SUZ 02

< 7

1 Til A ITNA 86GLA 01

1 c 1 H^MIL 01 I tna/a\

ITNA I94SUZ 02

m h ITNA S2SUZ 02

< 1500 L WXRF a2MIL 01 4 VAA 1300 I WKRF

OOU ff 1 A A 82MIL 01 230 10 TCGS 79FAI 01 z.nA ff Tkl A Hi OAACB AI

PPp||| Q1

350 SO TCGS 80AND 01 440 w ITNA 84SUZ 02 In (ng/g)

qe (ug/g) < 31 I ITNA 82SUZ 02

<

4 AAA 1000 L WXRp

A OftA ff 1 A A 82MIL 01 QtB 34 WXRF 82HIL 01 e9 1 ITNA OAmeb AA

^ / 1 m //I \

3 • TO nU.Ujnx f\u 1 LbS 80AND 01 w

1 PDCC Q^NAD HI

3 • 70 U . Uj U Tree 80GER 01 I 1 NA S.yo A m TCGS 79FAI 01 AM

9f 0 Tfifi? Q n A A SOGER 01 4.18 0.14 CB 80SCH 02 97 w. TCQS 79FAI 01 97 TRfiS 80ANO 0^ H20- (f) 100 AA 83BET 01 IPO 80 }^ AA 83BET 01 14 FD 80KHA 02 120 10 ITNA 80GER 01 16.8 GRAV 85LIN 02 199.2 39.84 !CPP8 85PEA 01

1635-6
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 1635 (cont.)

Cone UncGr Coni Method Reference | Cone Uncer Com Method Reference

1

1

1 .38 0.07 ITNA 82SUZ

1 02 1 < 1000 L UXRF 82HIL 01 0 08 ITNA 84SUZ 02 1 < 5000 ITNA 86GLA 01

1 .78 0.09 ITNA 86GLA 01 1 270 100 ITNA 82SUZ 02

1 .93 0.08 ITNA 85GAU 04 1 2 34 UXRF 82HIL 01 1 N f%)

2 0.25 ITNA 82HAH 01 1 2.1 0.3 ITNA 80GER 01 1 0.95 0.01 IC 83NAD 01

1 0.1 D TCGS SOGER 01

Li (uq/g) 1 1 0.1 D TCGS SOAND 01

1 1 0.1 TCGS 79FAI 01 0 28 ICPES 84NAD 01 1 1 .52 0.02 CB SOSCH 02

III f nn /n ^

1

1 Mand (\\qIq\ vuy/y;

ITMA 1 1 nn 86GLA

1 01 1 2070 30 ICPES 84NAD 01

15 3 ITNA 85GAU 04 1 2200 160 ITNA 82SCH 05

27 A ITNA 80GER 01 1 2279 424 ICPES 85PEA 01 33 14 ITNA 84SUZ 02 1 2300 70 ITNA 86GLA 01 36 7 ITNA 82SUZ 02 1 2320 ITNA 84CLE 01

1 2400 70 ITNA S2HAM 01 Ma (ua/a^ 1 2400 200 ITNA SOGER 01

1 2400 200 ITNA 82SUZ 02

600 ICPES 84NAD 01 1 2410 50 ITNA S5GAU 04

940 190 ITNA 82SUZ 02 1 2420 34 WXRF S2MIL 01

1000 34 AA 83BET 01 1 2700 50 D TCGS SOAND 01

1000 100 34 AA 83BET 01 1 2700 50 D TCGS SOGER 01 1000 200 ITNA 80GER 01 1 2700 50 TCGS 79FAI 01 1013.04 ICPES 85PEA 01 1 2800 34 AA S3BET 01

1300 200 ITNA 82HAM 01 1 3000 300 34 AA 83BET 01

nil Kua/yj

1

1 Nb Cua/a)

1S1 ^ . 7r n R 1 V.r c o 84NAD

1 01 1 < J L WXRF 82MIL 01 19 I1 TMA 1 nn 84CLE 01 1 19 1 2 ITMA 82SUZ 02 1 Ndnu (ua/a'i yuy/y;

20 2 0 3 ITNA 86GLA 01 1 20.4 1.5 ITNA 85GAU 04 1 < 1 L WXRF 82MIL 01 20.8 2.1 34 FAA 83BET 01 1 < 1.6 12 ITNA S2SUZ 02

21 4 ESR 85SHI 01 1 < 1 .8 12 ITNA S2SUZ 02

21 R ? 1 1 1 nn 82HAM 01 1 1 .35 0.15 ITNA S4SUZ 02

2P T I\ TMA 1 nn 80GER 01 1 1 4 0.2 ITNA SOGER 01 72 1 ^4 rnn 83BET 01 1 22 2 0 1

1

1

1 1 nnAA 82LIN 03 1 Mi fua/a)

22 n ft 1

1

1 1 nnAA 82LIN 03 1 WAR r 82MIL 01 1 1 .5 0.1 11 AA 82LIN 03

I D TCGS SOGER 01 1

1 . r ^ n 72 12 T

1 TUA 1 nn S2SUZ 02

24 7 D TCGS 80AND 01 1 1.78 34 FAA S3BET 01

24 7 TCGS 79FAI 01 1 1.8 0.5 34 FAA 83BET 01

345.6 ICPES 85PEA 01 1 1.83 0.23 12 ITNA 82SUZ 02

2.2 0.2 11 AA 82LIN 03

3 34 WXRF 82MIL 01 1635-7
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 1635 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

0 (%) 1

1

S-32/34 (ratio)

20.79 0.19 34 14NAA 80KHA 02 1 22.546 IDNS 84KEL 01 33 1.6 14NAA 80NAD 01 1 34.99 0.32 35 14NAA 80KHA 02 1 S-33/34 (ratio)

P (ufl/g) 1 0.1778 IDHS 84KEL 01

60 9 ICPES 84NAD

1 01 1 Sb (ng/3)

63 34 WXRF 82MIL 01 1 251 21 ICPES 85PEA 01 1 < 200 ITNA 86GLA 01

1 < 1000 L WXRF 82MIL 01 Pb (ug/g) 1 120 10 RTNA 78GAL 01 130 ITNA 84CLE 01 1.48 0.21 HAA 82NAD 01 1 130 10 HAA 82NA0 01 1.8 0.1 11 AA 82LIN 03 1 140 10 ITNA SOGER 01 1.9 0.3 11 AA 82LIN 03 1 140 10 ITNA 82HAH 01 1.9 0.6 34 FAA 83BET 01 1 147 21 ITNA 85GAU 04

2 34 FAA 83BET 01 1 160 30 ITNA 82SUZ 02

2.6 34 WXRF 82MIL 01 1 170 40 5 ITNA 80TOU 01 200 11 HAA 82CR0 03

Pb-210 (pCi/g) 200 11 HAA 82CR0 03

0.0699 0.0013 NM 80CAS 01 1 Sc (ng/g)

0.07 0.001 D NM 81 CAS 01 j < 1200 L ITNA 80T(XJ 01 Pr (ug/g) 1 560 50 ITNA 82SUZ 02

610 14 ITNA 85GAU 04

< 1 L WXRF 82MIL 01 1 610 20 ITNA 82HAM 01 < 4.3 12 ITNA 82SUZ 02 1 610 40 ITNA 86GLA 01 < 4.4 12 ITNA 82SUZ 02 1 690 70 ITNA 80GER 01 700 30 5 ITNA 80T0U 01 Rb (ug/g) 900 34 WXRF 82HIL 01

< 0.3 L WXRF 82MIL 01 1 Se (ug/9)

0.76 0.09 12 ITNA 82SUZ 02 1 0.83 0.08 12 ITNA 82SUZ 02 1 0.79 0.07 HAA 82NAD 01 0.95 0.37 ITNA 85GAU 04 1 0.8 0.2 RTNA 80KNA 01 0.82 0.04 RTNA 78GAL 01

S (ug/g) 0.9 AF 82UIL 01

1 0.9 FAA 82WIL 01 2880 40 ICPES 85PEA 01 1 0.93 0.07 7 HAA 84IMA 01 3200 100 D TCGS 80AND 01 1 0.93 0.07 D HAA 84IHA 03

3200 100 D TCGS 80GER 01 1 0.94 0.11 9 ITNA 82SUZ 02

3200 100 TCGS 79FAI 01 1 0.97 0.03 ITNA 84SUZ 02

3280 90 CB 85GLA 03 1 0.98 0.09 ITNA 80GER 01 3300 100 IC 83NAD 01 1 0,99 0.11 9 ITNA 82SUZ 02

3470 60 CB 86GAU 01 1 1.0 ITNA 84CLE 01 3540 40 XRF 84UEB 01 1 1.0 0.1 HAA 85LIN 01 3540 140 IDHS 84KEL 01 1 1.0 0.1 HAA 85LIN 02

3640 50 CB 84GLA 11 1 1.1 0.1 RTNA 84DEL 01 1.2 34 WXRF 82HIL 01

1635-8
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 1635 (cont.)

Cone Uncer Com Method Reference

5200 200 TCGS 79FAI 01 5200 200 D TCGS 80AND 01 5200 200 D TCGS SOGER 01 5600 700 14NAA SOGER 01 6000 1000 34 AA 83BET 01 6200 34 AA 83BET 01 6500 600 ICPES 84NAD 01 7600 22 ICPES 85PEA 01

Sm (ng/g)

250 10 D TCGS SOGER 01 250 10 D TCGS SOAND 01 250 10 TCGS 79FAI 01 260 10 ITNA 85GAU 04

260 20 ITNA 82HAM 01 270 10 5 ITNA 80TOU 01 300 40 ITNA SOGER 01 330 60 ITNA S4SUZ 02

340 30 ITNA S2SUZ 02

Sn (ug/g)

Sr (uq/g)

0.6 WXRF S2MIL 01

90 1 ICPES 84NAD 01 118 8 12 ITNA S2SUZ 02

127 24 12 ITNA 82SUZ 02

129 14 ITNA SOGER 01 140 34 UXRF S2MIL 01

< 300 ITHA 86GLA 01

< 1000 L WXRF S2MIL 01 44 6 ITNA 82SUZ 02

45 9 ITNA S4SUZ 02

46 9 ITNA SOGER 01 48 9 ITNA S5GAU 04

(ng/9)

< 100 ITNA 86GLA 01

< 2000 L WXRF S2HIL 01 35 3 ITNA 82SUZ 02

50 4 ITNA S4SUZ 02

290

360

600

Cone

Te (ng/g)

<

<

<

Th (ng/g)

560 30

580 40

610 70

630 25

630 60

640 50

640 60

Th-228 (fCi/g)

Uneer Com Method Reference

64.8

64.8

Th-23 (fCi/g)

76.5

76.5

Th-232 (fCi/g)

61.9

61.9

Ti (ug/g)

124

190

190

190

200

200

200

200

201

207

210

210

4.1

4.1

7.9

7.9

7.7

7.7

Tm (ng/g)

63

1000

10

L

34

12

12

ITNA S2SUZ 02 ITNA 84SUZ 02

WXRF 82MIL A 4 01

ITNA S4SUZ 02 ITNA 82SUZ 02 ITNA 82SUZ 02 ITNA 85GAU 04 ITNA 86GLA 01 ITNA 80TOU 01 ITNA SOGER 01

NM

NM

NM

NM

NH

NM

WXRF

ITNA

80CAS 01

81 CAS 01

80CAS 01

81 CAS 01

81CAS 01 SOCAS 01

2 ICPES S4NAD 01 20 D TCGS SOGER 01 20 D TCGS SOAND 01 20 TCGS 79FAI 01 34 COLOR 83BET 01 34 WXRF 82HIL 01 20 34 COLOR 83BET 01 40 ITNA 82HAM 01 ICPES 85PEA 01 WXRF 83GAR 01 20 ITNA SOGER 01 50 ITNA 82SUZ 02

1 L WXRF S2MIL 01

82MIL 01 84SUZ 02

1635-9
TABLE 1635-2: INDIVIDUAL DATA FOR NBS SRM 1635 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

U (nq/q) 1

1

Yb (ng/g)

200 SO ITNA SOGER 01 1 140 20 ITNA SOGER 01 220 20 ITNA 84SUZ 02 1 159 3 ITNA 85GAU 04

240 30 ITNA 82SUZ 02 1 170 60 5 ITNA aOTOJ 01 250 10 DNA 86GLA 01 j 175 12 ITNA 82SUZ 02

320 40 5 ITNA 80TOU 01 1 179 16 ITNA 84SUZ 02

U-234 (fCi/q)

1

1

1

(ug/g>

71.9 4.4 NH 80CAS 01 1 4.2 1 34 FAA S3BET 01 71.9 4.4 D NM 81 CAS 01 1 4.9 34 FAA 83BET 01

5 0.1 11 AA 82LIN 03

U-235 (fCi/g) 1 5 0.4 11 AA 82LIN 03

1 5.4 0. 76 ITNA 82HAM 01 4.9 0.3 D NM 81 CAS 01 1 5.6 34 UXRF 82MIL 01 4.9 0.3 NM 80CAS 01 1 6.6 1.4 12 ITNA 82SUZ 02

1 7.5 2.2 ITNA SOGER 01 U-238 (pCi/q) 1 7.8 1.2 12 ITNA 82SUZ 02

r 18 3 ICPES 84NAD 01 0.0731 0.0046 NM 80CAS 01 1 0.0731 0.0046 D NM 81 CAS 01 1 (<JS/a)

V (uq/q)

1

1 < 60 ITNA 86GLA 01

1 15 34 UXRF 82MIL 01 3.5 0.3 11 AA 82LIN 03 1 15.7 4.3 12 ITNA 82SUZ 02

4 34 WXRF 82HIL 01 1 16 3 ITNA SOGER 01 4.1 ITNA 84CLE 01 1 19.4 3.3 12 ITNA 82SUZ 02

4.3 0.2 ITNA 82HAM 01 1 0.3 ITNA 82SUZ 02 1 4.5 0.05 ITNA 80GER 01 1 L 7 0.3 f Tkl A 1 1 NA 85GAU 04 1 5 2 ITNA 86GLA 01 1 5.4 34 FAA 83BET 01 1 5.4 0.5 34 FAA 83BET 01 1 6.7 0.1 11 AA 82LIN 03 1 fmC 0.1 11 AA 82LIN 03 1

w (ng/g)

< 900 ITNA 86GLA 01 1 < 1000 L UXRF 82MIL 01 1 173 51 ITNA 82SUZ 02 1 210 50 ITNA 84SUZ 02 1

Y (uq/q)

1.9 34 WXRF 82MIL 01 1

1635-10
TABLE 1641-1: COMPILED DATA FOR NBS SRN 1641 MERCURY IN WATER

(revised 3/1/86)

ELE UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

Hg ug/mL 1.A9 ± 0.05 1.47 (1) AA

TABLE 1641-2: INDIVIDUAL DATA FOR NBS SRM 1641 (revised 3/1/86)

Cone Uncer Com Method ' Reference

Hg (nw/L)

1.47 0.17 CVAA 82GLA 02

TABLE 1641A-1: COMPILED DATA FOR NBS SRM 1641A MERCURY IN WATER

(revised 3/1/86)

ELE UNITS NBS

Mean ± SD

Hg ug/mL 1.1 i 0.05

TABLE 1641B-1: COMPILED DATA FOR NBS SRM 1641B MERCURY IN WATER

(revised 3/1/86)

ELE UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

Hg ug/mL 1.52 ± 0.04 1.52 (1) NAA

TABLE 1641B-2: INDIVIDUAL DATA FOR NBS SRM 1641B (revised 3/1/86)

Cone Uncer Com Method Reference

Hg (ug/g)

1.52 0.05 RTNA 85FEN 01

1641-1
TABLE 1642-1: COMPILED DATA FOR NBS SRM 1642 MERCURY IN WATER

(revised 3/1/86)

ELE UNITS NBS

Mean ± SD

Hg ng/mL 1.18 ± 0.05

TABLE 1642A-1: COMPILED DATA FOR NBS SRM 1642A MERCURY IN WATER

(revised 3/1/86)

ELE UNITS NBS CONSENSUS MEDIAN RANGE METHOD

Mean ± SD Mean ± SD (n)

Hg ng/mL 1.1 ±0.06 1.22 ±0.07 (4) 1.19 1.14-1.30 AA

TABLE 1642A-2: INDIVIDUAL DATA FOR NBS SRM 1642A (revised 3/1/86)

Cone Uncer Com Method Reference

H g <ug/L?

CVAA 85GAU 04

CVAA 81KAH 01 CVAA 84GLA 1

CVAA 82GLA 02

1.14 0.05

1.19 0.02

1.24

1.30

TABLE 1642B-1: COMPILED DATA FOR NBS SRM 1642B MERCURY IN WATER

(revised 3/1/86)

ELE UNITS NBS CONSENSUS RANGE METHOD

Mean ± SO Mean (n)

Hg ng/mL 1.49 ± 0.06 1.46 (2) 1.45 - 1.48 AA

TABLE 1642B-2: INDIVIDUAL DATA FOR NBS SRM 1642B (revised 3/1/86)

Cone Uneer Com Method Reference

Hg (ug/L)

1.45 0.13 CVAA 86GAU 01 1.48 0.06 CVAA 85GAU 04

1642-1 ^
cn

a.u It! S

to

UJ

CLU

O

»0 S. eo

CM

U UJ a u.

oin

Q. a. u u

o o

o Tx: 8 £

DC

f > UJ (A < <

< < ^

!^ !^ 1 S X

u. d, I g £ g !^

u. T u.

DC UJ « X < X

CM T- T- CM »M CM »- <^r-(M«-«-«-rM<-rM

in M o«

00 •- ro 0> «-

»- CM CM CM 2a to 00V

h> «o > o> o eo

• CM m CM »- • m ro »- eo K ^ IQ

in O CM

UJ

IUJ c

UJ 5

"

z

*- CM

CM >0 <- CM «- «- eo

K) in in <o m

•-^ eo

-H CO

•

t>~. eo eo CM o

H •M M -H +1 o>

eo *eo

17.6 in

(ijl

CM

eo

(M «- 1-

Or\j <o

eo

-Oo

eo

m• CMin in

44 44 P CM

in >o

</) CO

00

in

CM CM

tn eoed

CM K>

r- (M O N- CM >- CM

CO

^0 O

eo

CVJ in

S.CM

eo o

in o<

in o

o tn ^ in

< o ^o eo

0> CM •- ^ K CM o

oin CM «- oin

UJ

CD

C/l z

UJ 44

O in

44

tc

«cM«-inoo»00>o

44 (M

eo

eo N (SI o

41 44 44 44 41 in OCM 17.3 15.7

eoV in

41

eo

eo

CM

44 s 44 44 44 eo in CM C\| o CM+1 44 00 CM

CO

ce

OJ

3

»- «- »- Kl e- sf o 00 N. « 1 t o 1 41 44 CM 44 41 44 44 44 1 CM CM 44 1 1 44 ir— 44 41 1

1 4< 44 41

fc fS o eo In

fC

1 1 1 m 5 e OJ tsl e»

tr- CM o CM »^ in

CM

0> 0) at Ol 0) Ol Ol 01 Ol Ol 01 Ol Ol Ol Dl Dl Ol Ol Dl 01 0) 0) Dl 0) Ol 01

>>. v. •V V, "v. O) cn Ol Ol Dl Dl 01 1

01 Ol Ol Ol Dl c c c c C c C c c C c c c C c

m a "O L

a

V 01 01 c c n c i m u u 5 U u. X X z z i 2 z a. CO w w >

'mi^^'i'-'^':--'^^ 1643-1
TABLE 1643-2: INDIVIDUAL DATA FOR NBS SRM 1643 (revised 3/1/86)

Al Cng/g)

Uheer Com Method Refereheft

50 ITNA 81HAB 01 1 1^ u t^AA 84HAR 01 69 s ICPES 85FLO 01 1 18 i u FAA 84HAR 01 n 8 fkk 84HAR 02 1 18 i 14 FAA 84HAR 01 nA 5.7 AE-AP 78EPS 01 1 n XRF SOBER 02

82.1 1.4 FAA 78EPS 01 1 s t'AA 84HAR 02

83 FAA 84SLA 02 1 s u MA 84HAR 01 83 1 D DCPES 81REE 01 1 ICPES 85 FLO 01 83 f DCPES 79REE 01 1 a EXRF 84KNA 01

As (hg/g)

tia (mm

17.3 1.8 AE-AF 79EPS 03

18 14 FAA 79EPS 03

18 FAA 78BEA 01 18.7 0.7 FAA 78EPS 01 19./ 1 AE-AF 78EPS 01 21.5 1.2 14 FAA 79EPS 03

42 1 ICPES 85FLO 01

6e (ng/g)

18.8

21.3

Ca (ug/g)

23.9

Cd (ng/g)

M

r.s

9

ISM

0.4 FAA AE-AF

ITNA

78EPS 01 78EPS 01

81HAB 01

13

13

FAA 84SLA 02 FAA 84SLA 02 EKRF 84KNA 01

FE 82JEN 05 FAA 82JEN 05

torit

Co (ng/9)

Uncer Com Method Reference

Cr (na/a)

71 ICPES 82NYG 01 1 16 1 ICPES 85FLO 01 73 1 ICPES 83PRU 01 1 u FAA 84HAR 01 7S.7 1.3 HAA 80YAN 01 1 1i 1 u FAA 84HAR 01 78 13 ASV 82LEU 01 1 if g u PAA 84HAR 01 79 13 ASV 82LEU 01 1 10 s MA 84HAR 01 id s m 84HAR 02

14

IS

IIi&

16

11

16

16.2

\f

i4

N mm

n

n

n

n

ft

n

n

n

81

Hg (ng/d)

0.3 I^AA 78EPS 01

1 ^AA 84HAR 02

s 14 MA 84HAR 01

1 14 FAA 84HAR 01

14 FAA 84HAR 01

i 14 84HAR 01 3 EXRF 84KNA 01 1.8 AE-AF 78EPS 01

1 80BER 02

1 85 FLO 01

1 14 84HAR 01 1 14 m 84HAR 01 g b 81REE 01 DCPES 79REE 01 f FAA 84HAR 02

m 80EPS 04

s U m 84HAR 01

s 14 ^AA 84HAR 01 8 ICPES 85FLO 01 1 m 80BER 02

i ^XRF 84KNA 01

8 80BER 02

1643-2
TABLE 1643-2: INDIVIDUAL DATA FOR NBS SRM 1643 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

j Pb (ng/g)

5.7 ITNA 81HAB

1 01 1

1

18

21 7

FAA FAA

84SLA 02

84HAR 02

Mn (ng/q) 1

1

23

27

2

9

XRF

EXRF

80BER 02

84KNA 01 20 ITNA 81HAB 01 1 25 FAA 84SLA 02 1 Se (ng/a)

26 3 XRF 80BER 02 1 27.5 0.7 FAA 78EPS 01 1 10 ICPES 82NYG 01 28 2 14 FAA 84HAR 01 1 11.6 0.3 ICPES 83PRU 01 28 2.5 AE-AF 78EPS 01 1 12 1 HAA 81 COX 01 29 3 DCPES 79REE 01 1 29 3 D DCPES 81REE 01 1 Sn (ng/g)

29 7 14 FAA 84HAR 01 1 30 1 ICPES 85FLO 01 1 < 20 L XRF 80BER 02

30 5 14 FAA 84HAR 01 1 31 2 FAA 84HAR 02 1 Sr (ng/g)

51 2 14 FAA 84HAR 01 1 34 1 FAA 82JEN 05 1 203 16 ICPES 85 FLO 01 35 1 FE 82JEN 05 1 36 1 FE 82JEN 05 1 V (ng/g)

39 1 FAA 82JEN 05 1

1 40 ITNA 81HAB 01 Mo (ng/g) 1

1

41

50

15

2 D

FAA DCPES

84HAR 02

81REE 01 93 4 ICPES 85FLO 01 1 50 2 DCPES 79REE 01 95 17 14 FAA 84HAR 01 1 50 7 14 FAA 84HAR 01

10^ 18 14 FAA 84HAR 01 1 51 7 14 FAA 84HAR 01 104 3 FAA 78EPS 01 1 52 7 14 FAA 84HAR 01

105 27 FAA 84HAR 02 1 55 6 14 FAA 84HAR 01

110 5 AE-AF 78EPS 01 1 113 18 14 FAA 84HAR 01 1 Zn (ng/g)

118 25 14 FAA 84HAR 01 1

1 55 7 14 FAA 84HAR 01 Na (ug/g) 1 61 1 D DCPES 81REE 01 8.8 ITNA 81HAB 01 1

1

61

61

1 12 14

DCPES

FAA

79REE 01 84HAR 01

Ni (ng/g) 1 61 17 EXRF 84KNA 01 44 5 14 FAA 84HAR 01 1 62 5 14 FAA 84HAR 01

45 4 FAA 82JEN 05 1 62 7 14 FAA 84HAR 01 48 3 ICPES 85 FLO 01 1 63 3 XRF 80BER 02

48 4 D DCPES 81REE 01 1 67 3 ICPES 85FL0 01 4d 4 DCPES 79REE 01 1 69 12 FAA 84HAR 02

48 14 FAA 84HAR 02 1 49.8 0.8 FAA 78EPS 01 1 50 3 FE 82JEN 05 1 50 3 XRF SOBER 02 1 50 5 14 FAA 84HAR 01 1 51 3 14 FAA 84HAR 01 1 51.3 4.2 AE-AF 78EPS 01 1 52 6 14 FAA 84HAR 01 1 56 2 EXRF 84KNA 01 1 1643-3
"8

5

u

5

a.oa.oClua. a. u u

o(A

C

CD

0)

OO COo

oin

CO oin -M

x:

4-* V

z

c

c

(0

0)

CO

s:

a.o 5

CLO

in ui z z: O. CL o o 5 5 5 S 5 3 5 £5

a.o

z o s: s «f<cuj o..uo.<a.a.<<< u o. < a. a. <<OT o>fo<uu<<<

«

ro tn >* ro *— «— (M ro >* ro

CM >* in in 00 CM fM O rvj O o o o o o O ro in -* Kl fM o o 1 1 o o • o

•H rvi +1 H o M H +1 •H 1 I -M •H H • CO H H -H

1 1 O m CM fM o

>o CO fO V o CO CvJ o o 00 in

~* V

<y (M in

C

CD

01

«- CM «— «— <t- nO

lO

in -o

in

• m

fM ts- o

O o CM fM

1 1 • H H 1 I -H H -H

1 1 *

<^ ro OO 00

rg

CO o C> fM

«- «- <0 in

CO

~* >o

o

-H

CO •<-

ro -o fM

in T— oo

CO

H •H nO I CM 1

>o

1

1 +1 +1 •H

10.4 in

in

1 1 <^

ro

CM 52.0 3

c in >o OO in fM •r— ro o> in -* OO CO in

>o 00 o in in CO o CM ro O CO o >*• fM o >o CO o in o CM o o •o H +) M +4

1 +1 11

• -H

1 -H I1 H H H H •H •H +)1 •H1 ro •H

1 1 t 1 1 fM c in r^ o o fM CM in o CO •J- in fM

CD OO c^ in

0> ro CO CO fM 1^ z CM T

fM ro fM in

fM

fM

OCOO1^

-* CO ro fM o in fM fM .

1 fM1 CM

1 fM

g

1 1 O

1 in1 1

1 -*

1 1

1 ro

1 1

1

1 0

1 in

00 >o od CO in

(M

o «-

• «- fM o

CO

fM

COO fM

od

o

ro

r^ ^

CM

JfMOofM

in r^ oin m

O in . 1 1 o • 1 1 CO 00 fM fM in i ^ CM CM

• in in O 1 I fM 1^ 1 1 '— CO • • ro o m fM 1 1 T- ro in

ro 1^ -4- ^ t 1 ^ 1 1 Tr«. o 1 1 fM

lA a Z3 V>

Z C O <D U 01

0> CM «-

4-O mfM

ro

ro

00 in r^ fM ro -* «— ro CO in 00 <s- in o> ro ro

CM fM fM CM o

\^ >^ \^

in CM ro >*• -4- CM O •4 -4- m 00

-o

>« fM o 1 o

O

o

in

fM o O >* o

O >*

1 o o

CM o

•H -H •H M 1

1

I o 1 ro

•H +< >* •H H O•H r>~ H H + H •H M •

1 1 o

+1 H

o ro 1^ o ro r>w r>- O o ro •J- ro CM r>^ ro

CM fM OV oCM

CO

00

r—

OO

ro o

<>

in

CM

fM

fM V in

C

CD

0)

roo

H

r^

in CMM

fM

-H fM

1 M I

CM

1

I -H

CM

) •M 1

fM

• M

4-

+H

fMO fM

CM

00 -H H

ro r—

1 •H

^»

1

1 -H

in ro

•H 00CM

r8

vO

>* O

1 O1 o1 r^1 CO

S3 V inO

in

in

1 CM1 roCM

ro

in

CM

c c c

0> —' (fl < < <

CD o> o> CJ) cn O) O) cn o> cn cn cn cn CJ) cn cn cn cn cn cn cn cn cn cn cn cn \ \ \ '

\ ~^ "V. \ \ \ \ cn O) O) cn CJ) D) cn cn cn cn o> cn cn cn cn cn cn cn cn cn

ng

O) c c c 3 c c c c c c c c c C c c 3 c 3 c c 3 3 c c c c c c c

CO o

T3 TJ O l_) T3 -> » >

c

CJ 3CJ

0) cn

u. z ^

cn c o o Z Z Z Z

•- ^ XI XI 0) t- z a. a. cr (/> c/> c 3 > IM

1643A-1
TABLE 16A3A-2: INDIVIDUAL DATA FOR NBS SRM 16A3A (revised 3/1/86)

Cone

Ag (ng/g)

(ng/g )

As (ng/g)

70

7172

74

74

75.1

76

77

78

79

80

Au (ng/g)

15

Ba (ng/ g )

4145

45

45.7

46

48

49

54

Uncer Com Method Reference

70

4

5 62

3

0.8

7

28

6

4

6

10

13

3

6

2.7 FAA 82GLA 02

2.8 0.1 FAA 84GLA 02

2.8 0.4 FAA 85GAU 04

3.4 0.5 ICPES 82DEM 01 3.5 ICPMS 85DAT 01 3.5 1 6 ICPMS 83D0U 01 3.6 1.1 FAA 84GLA 11 3.8 0.4 FAA 83JEN 01 3.9 1 6 ICPMS 8300U 01

57 6 FAA 82JEN 02

121 8 UU 83LIN 01 129 10 RTNA 83&RE 01

Cone

Be (ng/g)

18.6

19

19

"19

24

Ca (ug/g)

26.5

26.9

27

27.4

27.5

27.6

28

30

Cd (ng/g)

Uneer Com Method

10.4

1

1

11

11

0.5

0.8

0.5

1.4

0.7

14

11

11

Referenee

ICPES 82DEM 01 ICPES 85HEE 01 ICPES 85NIS 01 ICPES 85NIS 01 ICPMS 85DAT 01

ICPES 85NIS 01 AA 84GLA 02

ICPES 85NIS 01 AA 84GLA 11 AA 85GAU 04

ICPES 85LAN 02

ICPES 85HEE 01 FAA 82GLA 02

ICPES 85LAN 02 1 FAA 84GLA 02 1 . 5 1 FAA 82JEN

FAA 84GLA 11 1 8.4 0.8 FAA 85BRE

ICPES 85KIM 01 I 9 1.4 ICPES 85KIM

ICPMS 85DAT 01 1 9.3 0.9 FAA 85GAU

HAA 81KAH 01 ! 9.4 1 RTNA 84BEM

NAA 84FEN 01 1 9.8 1.7 NAA 84FEN

FAA 82GLA 02 1 10 2 6 ICPMS 83D0U

ICPES 85HEE 01 1 10.1 0.5 RTNA 83GRE

FAA 85GAU 04 1 10.1 0.8 FAAC 85GAU

FAA 84SLA 02 1 10.4 0.5 ICPES 82DEM

ITNA 83JER 01 1 10.6 AAC 86GAU

10.6 0.2 11 FAA 85 SUB

11 ICPMS 85DAT

11 0.4 ICPES 85HEE

ICPES 85HEE 01 1 11 1 11 ICPES 85NIS

11 1 11 ICPES 85NIS

11 2 FAA 84GLA

11.4 2.9 11 FAA 85SUB

ICPMS 83DOU 01 1 12 FAA 82GLA

FAA 84GLA 02 1 12.2 1.6 ICPES 85LAN

AA 84GLA 11 1 12.5 0.3 FAA 83JEN

ICPMS 85DAT 01 j 12.5 1.3 FAA 83JER

ICPES 85HEE 01 1 13 2 6 ICPMS 83D0U

FAA 82GLA 02 1 FAA 85GAU 04 1 CI (ng/g)

ICPMS 83D0U 01 1 < 300 ITNA 84GLA

02^

01

0104

01

01

01

0104

01

01

01

01

01

01

0102

0102

02

01

01

01

1643A-2
TABLE 1643A-2: INDIVIDUAL DATA FOR NBS SRH 1643A (cont.)

Cone Uncer Com Method Reference

Co (ng/g)

18.3 1.4 NAA 84FEN 01

18.5 1.8 ICPES 82DEM 01 19 1 RTNA 83GRE 01

19 1 RTNA 82GRE 03

19.5 0.6 RTNA 84BEM 01 20 FAA 84SLA 02

20 2 11 ICPES 85NIS 01 20 2 11 ICPES 85NIS 01

21 3 14 FAA 84HAR 01

21 3 14 FAA 84HAR 01 21.5 2 ICPES 85LAN 02

22 3 14 FAA 84HAR 01 22 3 14 FAA 84HAR 01 24 4 ICPES 85HEE 01

(ng/q)

14.2 3.4 ICPES 85LAN 02

16 2 RTNA 83GRE 01 16 2 RTNA 82GRE 03

16 2 14 FAA 84HAR 01 16.2 1.5 D CPXRF 84SIM 02

16.2 1 .5 11 CPXRF 84SIM 01 16.4 3.1 11 FAA 85SUB 01 16.6 0.7 RTNA 84BEM 01 17 1 6 I CPUS 83D0U 01 17 1 11 ICPES 85NIS 01 17 1 ICPES 85HEE 01 17.4 2.2 11 CPXRF 84SIM 01 17.4 2.2 D CPXRF 84SIM 02

17.5 0.3 FAA 84GLA 02

17.6 0.9 FAA 85GAU 04

18 1 11 ICPES 85NIS 01 18 2 14 FAA 84HAR 01 18 3 FAA 84GLA 11 18 4 6 ICPMS 83D0U 01 18.1 2.9 11 FAA 85SUB 01 19 2 14 FAA 84HAR 01 19.8 5.6 11 CPXRF 84SIM 01 20 FAA 82GLA 02

20 2 14 FAA 84HAR 01 20 2.5 ICPES 82DEM 01 20 3 FAA 83JEN 01 20 4.2 ICPES 85KIM 01 32 6 ICPMS 83D0U 01

Cr(III? <nfl/fl)

14.9 2.1 ICPES 85COX 01

Cone Uncer

Cr(VI) (ng/g)

1.96 0.32

Cu (ng/g)

10 1 15.5 1.8

16

17

17 1 17 2

17 2.6

17.1 3.8

18 1 18 2

18 2

18 3

18 3

18.8 2.4

19 1 19 2

19.1 0.6

19.1 0.6

19.2 2 19.3 3.1

19.5 1 .3 19.5 3.2

21 3

21 10

31 10

45

Fe (ng/g)

23 5 78 9

80 8

82 4

83 6

84.5 1 .8

85 2

86 2

86 7

87

88 2.5

88 7

88 7

88 16

88 16

90

90 5 92 6

100

1643A-3

Com Method Reference

ICPES 01

FAA 02

FAA 01

FAA 82GLA 02

AA 84GLA 11

14 FAA 84HAR 01 FAA 83JER 01 FAA 85GAU 04

11 FAA 85SUB 01

11 ICPES 85NIS 01

14 FAA 84HAR 01

14 FAA 84HAR 01 ICPES 85HEE 01

14 FAA 84HAR 01 NAA 84FEN 01 FAA 84GLA 02

11 ICPES 85NIS 01 RTNA 83GRE 01 RTNA 82GRE 03

RTNA 84BEM 01 ICPES 85LAN 02

ICPES 82DEM 01

11 FAA 85SUB 01 6 ICPMS 83D0U 01 ICPES 85KIM 01 6 ICPMS 83D0U 01 6 ICPMS 83D0U 01

FAA 82JEN 02

14 FAA 84HAR 01 FAA 83JER 01 ICPES 85HEE 01

14 FAA 84HAR 01 ICPES 85LAN 02 FAA 83JEN 01 FAA 86GAU 01

14 FAA 84HAR 01 FAA 84SLA 02

ICPES 82DEM 01

14 FAA 84HAR 01 FAA OhuLA n?

RTNA 83GRE 01 RTNA 82GRE 03 FAA 84GLA 11

11 ICPES 85NIS 01

11 ICPES 85NIS 01 FAA 82GLA 02
TABLE 1643A-2: INDIVIDUAL DATA FOR NBS SRM 1643A (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Hq (nq/q) Mo (ng/g)

< 4 ICPES OSHEE ni 1 Ul 1 94 16 14 FAA 84HAR 01 0.2 I CRMS 85DAT Mi 1 01 1 95 9 14 FAA 84HAR 01 95.6 3.1 ICPES 85 LAN 02 K (un/q) 97 6 FAA 84M0K 01 97 6 RTNA 83GRE 01 1.5 FAA BdGLA 02 1 97 6 RTNA 82GRE fit 03

1.62 0.04 AA 84GLA 02 1 97 8 11 ICPES 85NIS 01 1.7 0.3 ICPES 85HEE 01 1 98 12 14 FAA 84HAR 01 1.82 AA 85GAU 04 1 100 10 11 ICPES 85NIS 01 2.1 0.2 11 ICPES 85NIS 01 1 102 4 RTNA 84M0K 01 103 4.5 NAA Q/ ecu Ul

Li (nq/q) 106 5 ICPES oc ucc A1Ul

106 24 14 FAA O/ U A D A1Ul

7 ICPMS OCn A T OOURl U1 1 108 ICPMS DCn A T B3DAT A1Ul

Mg (ug/g) Na (uq/g)

2.1 0.3 11 ICPES oc LI f ^ obNiS Ul 1 8.9 0.4 AA OC^ Al 1 03GAU 04

7.7 0.23 AA 85GAU 04 1 9 0.2 AA 84GLA 02

7.8 AA 84GLA 11 1 9 0.2 FAA 82GLA 02

7.8 0.13 ICPES ni 1 Ul 1 9.2 0.5 11 ICPES U 1 7.8 0.2 11 ICPES 03NIS Ul 1 9.6 AA ohGLA i i

1

1

7.8 0.4 AA ohGLA no 1 [}d

1 10 0.6 11 ICPES QCu r c AiU 1 7.8 0.4 11 ICPES QCU f C Ul 1 12 0.8 ICPES fiQUCC AiUl 7.9 0.3 FAA 0£uLA (15 1

9 0.2 ICPES QC D AU 03LAN no 1 Ud 1 Ni (nq/q)

Mn (ng/g) 31 3 6 ICPMS o«>UUU niU 1 47 3 6 ICPMS niU 1

10 1 FAA no 1 vc \ 47 4 FAA fix icy niU 1

24 2.5 ITNA ooJcK ni 1 Ul 1 47 10 ICPES ODntb niU 1 28 2.4 ICPES DCf f U ni 1 Ul 1 50.4 6.3 ICPES ODLAN (V) yjc 30 2 11 ICPES 85NIS Ul 1 51 8 14 FAA O/ LI A D niUl

30 2 14 FAA 84HAR Ul 1 52 FAA OC/^ Al 1 03GAU A/Uh

30.9 0.6 RTNA 83GRE Ul 1 52 6 14 FAA O/ UAD AiUl 30.9 0.6 RTNA 82GRE A1 1 05 1 54 5 FAA AiUl

31 3 FAA 83JEN Ul 1 54 7 14 FAA O/ UAD AiUl

31 ,3 0.8 ICPES ocDcn ni 1 Ul 1 55 FAA O/pi A OhuLA 1

1

1 1 31.5 2 RTNA ni 1 Ul 1 55 5 11 ICPES niU 1 32 FAA D/ A ohGLA 1 1 1 1 1

1 55 7 14 FAA nZoHnAK UAD niU 1 32 0.7 ICPES oc 1 A U 03LAN no 1 iJc.

1 56 6 ICPMS ni

32 2 14 FAA D/ U A D ni 1 Ul 1 56 1.5 ICPES niU 1 32 3 14 FAA 84HAR 01 1 56 8 RTNA 83GRE 01 32 3 FAA 84GLA 02 1 56 8 RTNA 82GRE 03

32.5 3.3 FAA 83JER 01 1 57 FAA 82GLA 02

33 1 ICPES 85HEE 01 1 60 3 11 ICPES 85NIS 01 33 1 11 ICPES 85NIS 01 1 62 18 ICPES 85KIM 01

33.5 FAA 85GAU 04 1 34 6 14 FAA 84HAR 01 1

1643A-4
TABLE 16A3A-2: INDIVIDUAL DATA FOR NBS SRM 1643A (cont.)

Cone

W03 (ug/g)

Uncer Com Method Reference Cone

V Cng/g)

Uncer Com Method Reference

1 ISE 84GLA 02 1 44 6 ICPMS 83D0U 01

1 50 1 ICPES 85HEE 01

3 (ng/g) 1 50 1.3 NAA 84FEN 01

1 51.1 4.8 ICPES 85 LAN 02

< 50 ICPES 85 LAN 02 1 52 1 RTNA 83GRE 01 22 5 ICPES 85HEE 01 1 52 1 RTNA 82GRE 03

24.1 0.8 11 FAA 85SUB 01 1 52 14 FAA 84HAR 01 25.2 FAAC 86GAU 01 1 53 1 ITNA 83JER 01 26 2 FAA 82GLA 02 1 53 1 11 ICPES 85NIS 01 26.8 FAA 86GAU 01 1 54 1 11 ICPES 85NIS 01 27 1 FAA 83JEN 01 1 54 8 14 FAA 84HAR 01 27 2 FAA 85GAU 04 1 55 10 14 FAA 84HAR 01 27 3 FAAC 85GAU 04 1 56 5 6 ICPMS 83D0U 01 27.4 AAC 86GAU 01 1 56 9 14 FAA 84HAR 01 27.6 ICPMS 85DAT 01 1 71 12 6 ICPMS 83D0U 01 28 2 FAA 84GLA 02 1 28 2 FAA 84GLA 11 1 Zn (ng/g)

28 3 FAA 83JER 01 1 28.9 9.1 11 FAA 85SU8 01 1 21 6 ICPMS 83D(XJ 01 29 2 ICPMS 83D0U 02 1 57 6 FAA 82JEN 02

30 38 ICPES 85KIM 01 1 58 9 14 FAA 84HAR 01

41 5 FAA 82JEN 02 1 60 7 6 ICPMS 83D0U 01

1 61 4.2 ICPES 85KIM 01

' (ng/g) 1 62 16 14 FAA 84HAR 01

1 63 FAA 85GAU 04

< 40 ICPES 85HEE 01 1 65 2 AA 84GLA 11

10 1 FAA 84GLA 02 1 65.1 0.3 FAA 83JEN 01

11 FAA 84GLA 11 1 66 2 FAA 84GLA 02

11 FAA 84SLA 02 1 68 1 ICPES 85HEE 01 11.5 0.5 HAA 81KAH 01 1 68 5 RTNA 82GRE 03

12 ICPMS 85DAT 01 1 68 5 RTNA 83GRE 01 12 0.8 FAA 85GAU 04 1 69.7 2.4 ICPES 85LAN 02

35 40 ICPES 85KIM 01 1 70 5 11 ICPES 85NIS 01

]

70 5 11 ICPES 85NIS 01 70 7 FAA 01

70 11 6 ICPMS 83D0U 01 200 6 ICPMS 83D0U 01 1 70 12 14 FAA 84HAR 01 206 50 6 ICPMS 83D(XJ 01 1 70.2 0.6 ICPES 82DEM 01 220 ICPMS 85DAT 01 1 72.5 2 RTNA 84BEM 01 225 32 6 ICPMS 83D(XJ 01 1 76 FAA 82GLA 02

232 5 11 ICPES 85NIS 01 1 77 3 6 ICPMS 83D(XJ 01 236 FAA 84GLA 02 1 77 7 14 FAA 84HAR 01 239 5 11 ICPES 85NIS 01 1 240 2.5 ICPES 82DEM 01 1 246 6 ICPES 85HEE 01 1

(ng/g)

< 0.01 RTNA 84BEM 01 1

1643A-5
i

TABLE 1643B-1: COMPILED DATA FOR NBS SRM 1643B TRACE ELEMENTS IN WATER (revised 3/1/86)

ELE UNITS NBS CONSENSUS MEDIAN RANGE AA OTHER METHODS

Mean ± SD Mean i SD (n) Mean ± SD (n) Mean (n) Method

Ag ng/g o n y.o A n n 10.6 (1) — — 10.6 (1) —

As ng/g AO 50 (2) — 46-54 50 (2) ...

B ng/g OA — ... — ...

Ba ng/g /./. Z C 42 (2) — 41 - 43 42 (2)

Be ng/g 10IT 4. 5 — ... — —

Bi ng/g 1

1

1 ... — — —

Ca ug/g 50 33 (2) — 31 - 35 35 (1) 31 (1) TITR Cd ng/g ± 1 20.0 ± 1. 2 (4) 19.4 18.8 - 21.7 19.7 (2) 18.8 <1) AAC

Cd ng/g ~ ~ ~ — — — 21.7 (1) FAAC

Co ng/g do z 1 " " " — — — ...

Cr ng/g 1R A * n A 18.4 (2) — 17.6 - 19.2 18.4 (2)

Cu ng/g 51 0 ^ 1 .7 * n A ± U.'f 21.7 <2) — 19.4 - 24 21.7 (2) Fe ng/g W A. fi X 0 98.4 (2) — 97.7 - 99.2 97.7 (1) 99.2 (1) IDMS K ug/g 3

... — — — —

Mg ug/g 15 ~ ~ ~ — — — —

Mn ng/g 28 1 2 26.7 ± 1. 6 (3) 27.2 25 - 28 26.7 ± 1 .6 (3)

Ho ng/g 85 ± 3 — — —

Na ug/g 8 — — —

Ni ng/g 49 t 3 69 (1) 69 (1)

Pb ng/g 23.7 ± 0.7 24 ± 3 (4) 22 21 - 27 25.8 (2) 21 (1) AAC

Pb ng/g 22 (1) FAAC

Se ng/g 9.7 t 0.5 9.1 (2) 9 - 9.2 9.1 (2)

Sr ng/g 227 t 6

Tl ng/g 8.0 t 0.2

V ng/g 45.2 ± 0.4

Zn ng/g 66 i 2 68.2 (2) 66 - 70.5 68.2 (2)

t

1643B-1
TABLE 1643B-2: INDIVIDUAL DATA FOR NBS SRM 1643B (revised 3/1/86)

Cone

Ag tnq/g)

10.6

As (ng/g)

46

54

Ba (ng/g)

4143

Ca (ug/g)

3135

Cd (ng/g)

18.8

19.4

20

21.7

Cr (ng/g)

17.6

19.2

Cu Cng/g)

19.4

24

Uncer Com Method Reference

1.1

16

5

0.6

1.1

1.8

1.5

8

Cone

(ng/g)

Uncer Com Method Reference

FAA 86GAU 01 1 97.7 6.4 FAA 86GAU

1 99.2 2.5 IONS 84 FAS

1

1 Mn (nq/g)

FAA 86GAU 01 1 FAA 85GAU 04 1 25 2 FAA 85GAU

1 27.2 AA 86GAU

1 28 3.5 FAA 86GAU

FAA 86GAU

1 01 1 Ni (ng/g)

FAA 85GAU 04 1 69 FAA 85GAU

1

1 Pb (nq/g) TITR 85GAU 04 1 AA 85GAU 04 1 21 AAC 86GAU

22 FAAC 86GAU

24.5 1.2 FAA 86GAU

1 27 3 FAA 85GAU

AAC 86GAU 01 1 FAA 86GAU 01 1 Se (ng/g)

FAA 85GAU 04 1 FAAC 86GAU 01 1 9 1.1 FAA 86GAU

9.2 1.4 FAA 85GAU

Zn (ng/g)

FAA 86GAU 01 1 FAA 85GAU 04 1 66 3 FAA 85GAU

70.5 2.1 AA 86GAU

AA 86GAU 01 1 FAA 85GAU 04 1

(J

1643B-2
"8

vt8 c

ID X

CO I/)

(/> UJ LU (/) X a. < o. u o o u < u u. < u — o a. Q < u- tS

SS

X 111

O- CLU CL

O

X < > a. a. < < (A u u o o. < o o

CO

LU UJ < a. CO < o — Q. Q

«-

M ro »- »— (M ^ fVI

N. • m «- • 00 vO K>

o

rsi o

»- CM ^ ^ O <M fM

O >C ^ (VJ • O O O O ^ »- «-

CO in m o

ca

0)

oo

00

-JO

ClU

"8o111 to

in

CD<I—<ao

a.5 o <

=3

CO

01

in -o o to

in

nj

o

in

^0

mCOoooo

fM •-

OO

roo

<MO

R

fM

toOo

fM

COo

<o

o

fM

•o

in

fMoo

o(M

r—O

M 11 M 11 fM 1 1 • • fM

N-m

O

m

oo 1 44 •M CO 1 CO

00 fM

fM in

00o 1 1 H 11 fM

fM

CO fMm K»

fM 1 ro K» 1 1 t fM

to

fM fMO in > CO 1 • fM • fM o O to

K»

«—

K» in O o

o •H •H

H

o ro 00 V

fM

fM

•- to

00o

fMo

00

fM

COooto

COo

t-o

H

fMO

too

o

COo

oo ot^ sj- • N. fM o «- <-

>— vo

to to • to r>- o «- o

«- fM fM <0 ^ w w fM

to

O To m o • +1 fM o in«- fM

vtm

c

IS«>

ofM

fM

fMO

o

o

oo

UJ

—I

UJ 3 3

CT

—• tf> (/) ^ ^ ^

0)

— 8 m CO u

0> TO 0> D* O) 0> ^ 3

•o 3 5 ^O

T3 T3 T3

OO ^ Of)

to

CJ t_) (_) 3

CJ

Ol3 « >«

1645-1

I.
"8

i c X o

c

«

0)

Ui

UJ (/) CL CS O (J 5 I o 5 3 o o a. a. o

lii a. UJ UJ

a. a. <,

^ <j o < a. o. o a a. 3 5

CL < o a

< CO > 1 I (/> LU O

< < —

T- ^ ^ ^ ^ ru »- T—

K> in

«- o

in

. o o 4 in o •J- o in •

ooNo o

hi

--f 00 O cNj ro o r- <o h~ r-. ^

o

8

(A

UJ

O. 44 U— c

«>

CO

00

ino

o> a

• >* o in

in

o

> +1 o

m

oinN- mo

c

ono CO w

1 Z

UJ c X 10

4) o X UJ

(/>

UJ c >

a: o m CO 1 •H X c

ee m

(/> 01 X COm

zgU. UJ < u *—< < a oc aUI—J

a.s z

< u

oUIX 1 in

UI c

—J

CD<1— </)

</>

X

</) CD c

<D4>

hO- O

o

in

o o

o rvi O

O

2 ro

ro o

o

oin

o

o

IM

O« o in ro o CO o in ro o in o o. >o s

ro s

o^^rsi o

o o

o o

ro

00 1 1 1 o 1 1 r-. 1 1 o ro

1 <> 11 1

1 1

(

1

1

t 1

1 ro t I1 oro o o in

/—

(Nl CO <NJ CO <M o ro CO rvj

v.* r—w

in CO rj (NJ o o ro -* Oro o o o vO

1 >*

C3 ro

1 CO1 vO H 44 1 •M 1 (M 44 41 1 44 44

1 1 1 1 1 V IM (M (M >t o

^. o IC

lO o

o o in

in 00 (M m o r\j O o r>. CO

I o t o o O o> •*1

1 1

•

1 44

1

1 44

1

1 44 o> 44 44

1 1

1

1 44 44 1

1 1 > 1 1 M in

1 1 r^ o1

f\J N. CO o r^ >» O o in

»—

o>

UI Ol O) O) o> Ol Ol Ol Ol Ol Ol Ol \ ~v \ \ — \ \ Ol o> o> Ol Ol Ol Ol Ol CD cn Ol a Ol Ol 3 3 3 3 c X »< 3 3 3 3 3 3 T3 3 3

«> o

IS o M- CD tjl c o o C c C O o m

cs C3 Z z _l —J X X X X X X z z

inin

in

O•4-

rsi

in

o

(Nl

O. Tr\i ro

rsi m in o

w Rj

o oo o

• o o «-

00

CNJ ^ o «*

r^ «- T-

• m r>-

Ol Ol Ol Ol Ol Ol Ol Ol CD Ql 333333X33333C

XIz - n n s> Si -a o a. a. a. a. a. a.

1645-2
"8

4) 8 -

8

c O <0

c

a

0)

« < u a. 5a.

o

C)

CO

UJ </) O U

Q »-

to

5a. 5 5 3

a. < < a. o. «

u < < u u ^ 5

Q.

V) </> UJ UJ

o. < o. O < CJ o a. o

(M «— Kl »- fM

00

o

-Jeo o o-

• kS o>0

in • in

o

o

I

o

LTl

(/>

Q. « O— C

(D

00

O

O(M o

00 ^ ^ o>

o

o

c

4^

on o uw

h- 5

z z

UJ c X (0

01 a X

UJ

(/> <^

UJ c >

oto < H < X c

oc SI

</> «) X (/> COzsu.

UJ < u

z

< < o

a

UJ

-Js

z

< u

oUJX 1

UJ c

_j w

OD<

t- US 8

</) z

UJ +4 U 01

00 ro ro o

NKI v~

• O N- O I 1 O 1 1 1 ^ 1 1 o in •H 1 1 • <\J 1 1 1 (M 1

1 f\J 1 1 1 I I 3 OJ

/-> <-»> /-> vt «— f\J in

ij— O o OJ 03 CO CO

1 1 O O • O ) 1 I O 1 1

1 •H 1 K» 1 o • 1 1 41

1 O O K» 1 1 • in

fO o

S8

(NJ (NJ O • O • 1^ • o in m sff fo ^ 00 CO N. fO

60 fO ^ • o ro (Ni rvj

fO fO

ro

rvj

rvi

ro

ro

POo

o

00 in

«- tsi

m 1—

0> 00

»- o

fM

00

oo

min

•o in «

in rg ro oo to o t^ to (M »

to mro N. o <

O o o -* in >o o ro oo ro ~» m O in o •* fO o o o fM o -o fM O ' 1 H H H -M * (M •M +4 +4 m I 44 o (M o o fVJ -* ro S

*^

: t ro o o oo o in >0 o -J- ro ro >o o fM o ro ro § in

CM «—

COm

c

CD

OJ

o in

• in • •

m O o (> O o

4 44 44 s» in

«» »— to

«— fM

o

ofM

CO cn cn cn cn o> (71 cn cn O) 9 O) O) t— \ \ — ^ — -"^ O) O) 1 K

cn cn o> z 3 3 3 3 3 3 3 3 3 c 3 3 3

fM

fM

I(0 .QoaioO'-ECt- </)</)C/>C/>VIC/)CO(/)(/)C/> 3 > :» .a c c c c t- c >->-rsirsiisirs(rslrsi

1645-3

I
TABLE 16A5-2: INDIVIDUAL DATA FOR NBS SRM 1645 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

1 (ug/g)

1

1 Ba (uq/q)

1.75 IDMS 83L0S

1 01 1

1

178

340

15

50 35

PAA

ITNA

SOKAT

81GLA

0102

(%) 370

385

36

42

11

11

ICPES

ICPES

84NAD

84NAD

01

01 0.5 ICPES 84SUN 01 1 400 ICPES 80 FLO 01 0.66 ICPES 84SUN 01 1 0.9 11 ICPES 84UOL 01 1 Be (uq/q)

1.4 0.1 DCPES 81 CAN 01 1 1.68 6 EXRF 84JEN 01 1 1 ICPES 80 FLO 01 2.09 0.32 11 ICPES 84NAD 01 1 2.11 6 EXRF 84JEN 01 1 Bi (nq/q)

2.14 ICPES 84SUN 01 1 2.18 0.028 ICPES 84HIR 01 1 < 100 FAA 82MAT 02

2.23 0.11 11 ICPES 84NAD 01 1 600 AF S5NAR 02

2.37 0.04 35 ITNA 81GLA 02 1 2.42 0.12 AA 81 FAR 01 1 Ca (%)

2.5392 0.1587 ITNA 85 PEN 01 1 3.9 ICPES 80FLO 01 j 2 11 ICPES 84W0L 01 6.9 11 ICPES 84U0L 01 [ 2.3 ICPES 84SUN 01 23.8 11 ICPES 84UOL 01 1

1

2.3

2.33

0.1

6

AA

XRF

83CAR

78TAK

01

01 (uq/q) 1

1

2.39

2.6

0.06 11

11

ICPES

ICPES

84NAD

84U0L

01

01 47 AF S5NAR 02 1 2.62 0.06 11 ICPES 84NAD 01 62.6 2.1 RTNA 82ELS 02 1 2.73 0.15 35 ITNA 81GLA 02

63 ICPES 35NAR 02 1 2.8 ICPES 84SUN 01 64 3.6 FAA 85 FAN 01 1 2.9 0.13 AA 81 FAR 01 65 11 FAA 83X1

A

01 1 2.93 0.01 PAA SOKAT 01 65 1 ICPES 84LIV 01 1 3 ICPES 84SUN 01 65 1 FAE SODS I 01 1 3.1 EXRF 83MAH 03

66 HAA 80AGE 03 1 3.106 6 XRF 78TAK 01 66 11 FAA 83X1

A

01 1 4.1 11 ICPES 84W0L 01 66 5 lENA 82GLA 02 1 4.2 ICPES 80 FLO 01 66 13 11 ICPES 84NAD 01 1 4.59 6 EXRF 84JEN 01 66.4 ICPES 81G0U 01 j 6.55 6 EXRF 84JEN 01 66.6 4.3 FAA 83L0V 01 1 67 ICPES 82NYG 01 1 Cd (uq/q)

68 lENA 84GLA 02 1 68.7 4.1 FAA 83CAR 01 1 7,2 0.4 11 FAA 83CAR 01

71 ICPES 80 FLO 01 1 7.6 0.4 AA 83CAR 01 71.3 1.3 DCPES 84URA 01 1 8.9 0.4 RTNA SOVAL 01 72 ITNA 81SL0 01 1 8.9 0.8 ICPES S4MAR 01 75 WXRF 84ZS0 01 1 9 ICPES 84SUN 01 87 PAA SOBER 01 1 9.1 0.3 IDMS SOROS 01 95 6 EXRF 84JEN 01 1 9.2 0.5 FAA 81 FAR 01 172 6 EXRF S4JEN 01 j 9.3

9.4

0.1 11

11

AA

FAA

S2SAK

S3CAR

01

01 (uq/q) 9.5

9.55 0.22 11

ICPES

AA

84SUN

82SAK

01

01 31 3 TCGS 84GLA 01 1 9.8 11 AA 84W0L 01 1645-4
TABLE 1645-2: INDIVIDUAL DATA FOR NBS SRM 1645 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Cd (uq/g) cont

1

1 Cr (%)

10 11 AA 84U0L

1 01 1 1.88 0.27 11 ICPES 84NAD 01 10 ICPES 84SUN 01 1 1.98 0.24 11 ICPES 84NAD 01

10 I OPES 80FLO 01 1 2 ICPES 84SUN 01

10.1 6 AF 84NAR 02 1 2.1 0.2 DCPES 81 CAN 01 10.1 0.6 11 AA 83HSU 01 1 2.29 0.08 PAA 80KAT 01 10,2 0.4 RTNA 79DER 01 1 2.5 0.4 RTNA 77MEL 01 10.25 AF 85NAR 02 1 2.66 EXRF 83MAH 03

10.3 11 AA 84U0L 01 1 2.67 0.03 ICPES 84HIR 01

. 10.5 6 AF 84NAR 02 1 2.7 11 ICPES 84W0L 01 10.5 0.4 11 AA 83HSU 01 1 2.7 0.2 FAA 83CAR 01 10.8 ICPES 85NAR 02 1 2.8 ICPES 84SUN 01 10.8 2 ICPES 82SCH 04 j 2.8 0.17 AA 83CAR 01

11 PAA 80BER 01 j 2.85 ICPES 84SUN 01 11.2 6 ICPES 83CHA 01 1 2.88 6 ICPES 83CHA 01 11.4 4.3 AE-AF 82G0L 01 1 2.9 11 ICPES 84U0L 01 11.98 6 ICPES 83CHA 01 1 2.91 0.01 11 AA 82SAK 01

1 2.91 0.24 ICPES 82SCH 04

Ce (ug/g) 1 2.93 6 ICPES 83CHA 01

1 2.97 0.125 11 RTNA 76STE 01 20 0.6 PAA 80KAT 01 1 2.98 PAA 80BER 01 28 PAA 80BER 01 1 2.99 0.13 35 ITNA 81GLA 02

120 10 DCPES 81 CAN 01 1 3 11 ICPES 84U0L 01

1 3 0.27 11 AA S2SAK 01 Co <ug/g) 1 3.02 ICPES 80 FLO 01

1 3.15 0.147 11 RTNA 76STE 01 6.7 0.5 11 FAA 83CAR 01 [ 3.16 0.152 11 RTNA 76STE 01 7.2 11 FAA 83CAR 01 1 3.18 0.08 AA 81 FAR 01

8 0.2 35 ITNA 81GLA 02 1 3.19 0.038 6 XRF 80IUA 01 8.4 0.7 RTNA 77MEL 01 1 3.25 0.049 6 XRF 80IUA 01 8.5 0.3 PAA 80KAT 01 1 3.25 0.152 11 RTNA 76STE 01 n 1? RTMA 790ER 01 1 3 2706 0.155 ITNA 76STE 01 10.4 ICPES 84SUN 01 1 3.4 0.148 11 RTNA 76STE 01 10.8 ICPES 84SUN 01 i 3.52 6 XRF 78TAK 01

11 ICPES 80 FLO 01 1 4.17 6 EXRF 84JEN 01 12.8 ICPES 84SUN 01 1 6.28 6 EXRF 84JEN 01 15.6 0.6 ICPES 84HIR 01 1 SOBER 01 1

Co-60 (pCi/g) 2.32 0.13 35 ITNA 81GLA 02

2.69 0.14 ITNA 84GLA 11

< 0.06 uu 84MEL 01 1 3.3 0.2 RTNA 77MEL 01

< 0.06 GAMMA 84KR! 01 1 Cs-137 (DCi/g)

< 0.05 GAMMA 84KRI 01

< 0.05 UU 84MEL 01

1645-5
TABLE 1645-2: INDIVIDUAL DATA FOR NBS SRM 1645 (cont.)

Cone Uncer Com Method Reference

Cu (ug/g)

D^

78 6 XRF 78TAIC 01 84 6 ICPES 83CHA 01 90 6 ICPES 83CHA Ai01 90.9 11.2 AA 84KAN A 4

96 14 ASV 81 DOG 01 98 4 4

1 1 W 84W0L 01 100 OA20 AA 77YAN 01

101

4 4

1 1 W O / 1 vw 01

4 A4 101 4.2 ICPES O/ u T n o<fHIR Ai01

4 At 102 oB DCPES O 4 ^ A U olCAN 01

4 A7 103 o8C A A FAA o3CAR 01

105 T f*DCC ILrbb O/ CI lU OHSUN 01

105 14 ICPES o<:SCn Oh

1Uo rAA oUbcK 01 10o ZO XRF 7OT A V roi AK 01 108 4 4

1 1 W 84W0L 01

i no 1uo 5

i 1

1 1 ICPES 0/ ki An <5hNAD 01

lUo 4 41 1 ICPES cShSud 01 luy o

A A AA OjLAK A1Ul 111 n 1 C3

A Ctf AoV ojnAl; ni01 111 »

f rAA SI1 CAD 0 1 rAK ni0 1

1 1 c I Lrto 0/ CI ty niU 1 112 ICPES 84SUN 01 113 6 XRF 78TAK 01 115 7 11 ICPES 84NAD 01 119 ICPES 80FLO 01

123 6 RTNA 790ER 01 124 4 11 AA 82SAK 01 125 3 11 AA 82SAK 01 125.2 8.2 RTNA 80VAL 01

1ICO WXRF 0/oAZSO ni01 190 66 EXRF 83MAH 03

213 6 EXRF 84JEN 01 379 6 EXRF 84JEN 01

' (uq/g)

2 0.2 DCPES 81 CAN 01

(ug/g)

0.31 0.03 35 ITNA 81GLA 02

0.7 ICPES 80FLO 01

Cone Uncer Com Method Reference

Fe (%)

I.I ICPES 84SUN A 4 01 7.9 n / 0.4 DCPES 81 CAN A 4 01 XRF 70T A V

f oTAK ni01

0 c 0.5 n c 0.5 RTNA 77MEL A101

0 0 8.8 4 4 11 ICPES 84W0L A 4 01 0 nc y.05 n 10 0.19 1 1

1 1 ICPES 84NAD ni01 9.25 n 11 U. 1

1

1 1

1 1 ICPES 0/ ki A n OHNAD ni01 y.5 1 !

1 1 ICPES 84U0L A 4 01 9.7 n c 0.5 AA 83CAR A 4 01 9.74 n 40 0. 12 ICPES 84HIR A 4 01 0 00 XRF 70T A V f oTAK ni01 in T ICPcS 0/ CI lU ohSUN ni01 in / VD C XRr 7QT A V rol AK ni01 in / ILrtS 0/ CI lU OhSUN ni0 1 in c 1U.5 n 1 U.J T Til A

1 INA 01^1 A OlbLA noOd

10.51 0.18 PAA 80KAT 01 10.6 0.3 AA 81 imR 01

11 6 ICPES 83CHA 01 11.2 EXRF 83MAH 03

11 5 11.^ n A 1

1

AA OCdAK niUl

4 •!

1 .J 1 LrCd UH

f PDCC our LU ni

11.5 6 ICPES 83CHA 01 11.8 0.2 11 AA 82SAK 01 12.3 6 EXRF 84JEN 01 12.9 11 ICPES 84W0L 01 5n 1 CVDC cAKr fi/. icy 04 JcN niu 1

(uq/q)

14 •1 DCPES 81 CAN 01 38 ICPES 80FLO 01 40 6 EXRF 84JEN 01

71 6 EXRF 84JEN 01

(uq/g)

0.96 0.14 4 TCGS 85GLA 05

1.16 0.15 4 TCGS 85GLA 05

(uq/q)

1.39 0.07 35 ITNA 81GLA 02

F (uq/g)

1336 97 ISE 83BET 02

1740 60 ISE 83KNA 01

1645-6
TABLE 1645-2: INDIVIDUAL DATA FOR NBS SRM 1645 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

vuij/ ay Ma fX) cont

0,4 AF 84NAR 02 1 0.75 0.02 AA 81 FAR 01 0.67 0.07 FAA 83CAR 01 1 0.78 ICPES 84SUN 01 0.7 6 AF 84NAR 02 1 0.82 ICPES 84SUN 01 0.83 0.05 ICPES 84MAR 01 1 0.84 ICPES 84SUN 01 0.85 0.036 CVAA 80NAD 01 1 0.8426 11 ICPES 84U0L 01 0.937 0.36 RTNA 84DEL 01 1 2.1 0.1 AA 83CAR 01 0.949 0.055 RTNA 84DRA 01 1 2.3 XRF 83CAR 01 1.05 0.19 CVAA 81KAH 01 1 4.1 ICPES 80FLO 01

1.1 0.04 CVAA 83CAR 01 1 1.1 0.1 RTNA 77MEL 01 1 Mnlit Cua/Q) ^ iif n f 1.11 0.26 CVAA 80UHI 01 1 700 EXRF 83MAH 03

1.3 PAA 80BER 01 1 707 7.2 ICPES 84HIR 01 1.3 0.2 RTNA 80VAL 01 1 710 40 11 ICPES 84NAD 01 716 110 11 AA 82SAK 01

f na/al 721 11 W 84W0L 01 723 77 11 AA 82SAK 01 < 790 RTNA 83BER 01 1 735 11 W 84U0L 01 746 130 AE-AF 82G0L 01

1 750 ICPES 80 FLO 01

1 750 11 W 84U0L 01 0.04 ICPES 84SUN 01 1 750 18 PAA 80KAT 01 0.09 0,002 AA 83CAR 01 1 756 15 AA 83CAR 01 0.15 ICPES 84SUN 01 1 760 30 11 ICPES 84NAD 01 0.608 6 EXRF 84JEN 01 1 762 9 35 ITNA 81GLA 02

0.857 6 EXRF 84JEN 01 1 768 85 ICPES 82SCH 04

0.87 0.12 11 ICPES 84NAD 01 1 770 30 DCPES 81 CAN 01 0.893 6 XRF 78TAK 01 1 780 90 AA 81 FAR 01

1 .06 0.13 11 ICPES 84NAD 01 1 793 52 ICPES 84S0B 01

1 .22 ICPES 84SUN 01 1 798 ICPES 84SUN 01 1.24 6 XRF 78TAK 01 1 838 ICPES 84SUN 01 1.4 EXRF 83MAH 03 1 870 ICPES 84SUN 01 1460 6 XRF 78TAK 01

-111 40 (OCWq) I / My 1 3321 6 XRF 78TAK 01

11.36 UU 84MEL 01 1 Mo (ug/q)

11.36 GAMMA 84KRI 01 1 25 PAA 80BER 01 37 1,9 ICPES 84HIR 01

1

1

40 2 DCPES 81 CAN 01

15 ICPES 80FLO 01 1 Na fua/a)

33 3 DCPES 81 CAN 01 1 1600 ICPES 84SUN 01 2050 ICPES 84SUN 01

1 (%) 3200 100 AA 83CAR 01 4100 500 11 ICPES 84NAD 01 0.603 0,1809 ITNA 85PEN 01 1 4700 XRF 83CAR 01 0.62 0,16 11 ICPES 84NAD 01 1 4700 400 11 ICPES 84NAD 01 0.65 0,02 11 ICPES 84NAD 01 1 5200 ICPES 84SUN 01 0.67 0.0092 84HIR 01 1 5450 110 PAA 80KAT 01 0.6823 11 ICPES 84W0L 01 1 5600 6 ICPES 83CHA 01 0.684 0.01 PAA 80KAT 01 1 5600 6 ICPES 83CHA 01 0.7095 11 ICPES 84U0L 01 1 5600 200 35 ITNA 81GLA 02

1645-7
TABLE 1645-2: INDIVIDUAL DATA FOR NBS SRM 1645 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

5 (ug/g)

1

Pb (ug/Q) cont.

1.4 0.07 PAA 80KAT 01 1 684 35 FAA 83CAR 01

30 3 DCPES 81 CAN 01 1 685 11 AA 84UOL 01 685 10 11 AA 82SAK 01 693 ICPES 85NAR 02

695 45 ASV 81 DOG 01 28 6 XRF 78TAK 01 1 701 6 ICPES 83CHA 01 30 6 XRF 78TAK 01 1 704 6 ICPES 83CHA 01 33 6 XRF 78TAK 01 1 705 11 AA 84U0L A401

37.6 6.4 AE-AF 82G0L 01 1 705 6 EXRF 84JEN A 4 01

39.8 11 FAA 83CAR 01 1 705 35 AA 83CAR A 4 01

41 2 11 AA 82SAK A 4 1 01 1 717 6 XRF 78TAK A401 42 4 11 AA 82SAK 01 1 718 28 11 AA 83HSU 01 43 11 W 84W0L 01 1 719 6 XRF 78TAK 01 44 6 ICPES 83CHA 01 1 721 20 ICPES 82SCH 04

44.7 2.7 AA 83CAR 01 1 721 26 11 AA 83HSU 01 44.9 11 W 84U0L 01 1 722 18 ASV 83MAD 01 45 11 W 84W0L 01 1 724 PAA 80BER A401

45 ICPES 80 FLO 01 1 724 43 11 AA 82SAK 01

45.8 2.8 11 FAA 83CAR 01 1 725 ICPES 80FLO 01 46 4 DCPES 81 CAN 01 1 725 11 AA 84U0L A401 46.1 2.5 ICPES 82SCH 04 1 732 ICPES 84SUN A401

46.6 4.6 PAA 78MAS 01 1 740 EXRF 83MAH fit 03

47 ICPES 84SUN 01 1 745 ICPES 84SUN 01 47 3 PAA oUKAT 01 1 768 ICPES O/ CI lU QhSUN 01 48 PAA 80BER 01 1 771 231 AE-AF 82GOL A 4 01 48 6 EXRF 84JEN A4 1 01 1 1019 6 XRF 78TAK 01 48 PAA 78ICAT A 4 1 01 1 1270 6 EXRF 84JEN 01 48 UXRF o4ZS0 01 1 50 6 ICPES 83CHA A 1 1 01 1 Pd (ng/g)

52 ICPES 84SUN 01 1 53 ICPES 84SUN 01 1 1 IDMS 83L0S 01 55 2.4 ICPES 84HIR 01 1 55 3 RTNA 77MEL 01 1 Pr (ug/g)

57.8 7.7 ICPES 84SOB A 4 1 01 1 85 6 EXRF 84JEN A 4 1 01 1 14 ICPES 80FLO A401

<ug/g) ] Ra-226 (DCi/g)

429 9 11 ICPES 84NAD A 4 1 01 1 0.86 UU B4MEL 01 452 27 ICPES 84HIR 01 1 0.86 GAMMA 84KRI A401 459 31 11 ICPES 84NAD 01 1 526.9 6.4 DCPES 84URA 01 1 Rb (ug/g)

) (ug/g)

1 38 6 XRF 78TAK A401 39 6 EXRF 84JEN 01 538 39 11 ICPES 84NAD 01 1 39 6 XRF f oTAK Hi

597 40 11 ICPES 84NAD 01 1 40 2 PAA 80KAT 01 631 AF 85NAR 02 1 41.4 0.5 RTNA 77MEL 01 670 22 ICPES 84MAR 01 1 50 7 35 ITNA 81GLA 02

680 20 AA 77YAN 01 1 70 6 EXRF 84JEN 01 683 29 FAA 81 FAR 01 1

1645-8
TABLE 1645-2: INDIVIDUAL DATA FOR NBS SRM 1645 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

S (%)

1

1 Si (X)

3.68 6 EXRF 84JEN

1 01 1 15.4 6 EXRF 84JEN 01 5.02 6 EXRF 84JEN 01 1 19.7 6 EXRF 84JEN 01

1 22.2 1.1 11 ICPES 84NAD 01 Sb (ug/g) 1 23.6 AA 83FAR 01

1 23.7 1.9 DCPES 81 CAN 01 5.9 AF 85NAR 02 1 27.2728 2.1949 ITNA 85PEN 01 21.7 RTNA 81NIS 01 1 22.6 RTNA 81KIB 01 1 Sm (ug/g)

25 HAA 81YAH 01 1 28.3 1.2 FAA 82MAT 02 1 1.22 0.14 4 TCGS 85GLA 05

31 4 ITNA 81 HAH 01 1 1.26 0.14 4 TCGS 85GLA 05

32.2 3.2 11 FAA 83CAR 01 1 33.2 RTNA 81SL0 01 1 Sn (ug/g)

33.6 2.2 RTNA 82ELS 02 1

f TUA 1 1 NA 81SL0 01 1 O Ar 85NAR 02

38 ICPES 82NYG 01 1 313 9 FAA 82MAT 02

40 5 35 ITNA 81GLA 02 1 366 FAA 84L0N 01 47.2 11 FAA 83CAR 01 1 416 15 RTNA 83BER 01 52 PAA 80BER 01 1 66 ICPES 85NAR 02 1 Sr (ug/g)

Sc (ug/g)

1

1 747 38 11 ICPES 84NAD 01

1 814 43 11 ICPES 84NAD 01 < 2 DCPES 81 CAN 01 1 851 13 PAA 80KAT 01 2.13 0.07 35 ITNA 81GLA 02 1 862 PAA SOBER 01 3.1 0,5 RTNA 77MEL 01 1 870 6 XRF 78TAK 01

1 910 EXRF 83MAH 03

Se (ug/g) 1 960 6 EXRF 84JEN 01

1 1033 6 XRF 78TAK 01 0.85 RTNA 81SL0 01 1 1200 ICPES 80FLO 01

1 ICPES 81G(XJ 01 1 1750 6 EXRF 84JEN 01 1.3 0.2 RTNA 77MEL 01 1 1.5 0.1 35 RTNA 81GLA 01 1 Ta (ng/g)

1.7 0.3 HAA 85CUT 01 1 5 ICPES 80FLO 01 1 220 20 35 ITNA 81GLA 02

8 ICPES 82NYG 01 1 9.8 ICPES 85NAR 02 1 Te (ug/g)

24 AF 85NAR 02 1 4.6 IDMS 83L0S 01 Se(IV) (Uq/q)

Th (ug/g)

0.02 0.01 HAA 85CUT 01 1 1.8 PAA 80BER 01 Se(VI) (uq/q) 19 6 EXRF 84JEN 01 34 6 EXRF 84JEN 01 0.08 0.03 HAA 85CUT 01

1645-9
TABLE 16A5-2: INDIVIDUAL DATA FOR NBS SRM 16A5 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

(ug/g)

1

1

1

Y (ug/g)

184 11 ICPES 84U0L 01 1 < 7 DCPES 81CAN 01 245 11 ICPES 84W0L 01 1 7 ICPES 80FLO 01 258 6 XRF 78TAK 01 1 7.4 0.3 PAA 80KAT 01 370 11 ICPES 84NAD 01 1 490 6 XRF 78TAK 01 1 Yb (ng/g)

491 14 ICPES 84HIR 01 1

-

590 11 ICPES 84NAD 01 1 < 2000 DCPES S1CAN 01 597 11 ICPES 84W0L 01 1 600 ICPES SOFLO 01 600 100 DCPES 81 CAN 01 1 642 13 PAA 80KAT 01 1 Zn (ug/g)

700 AA 82MAT 04 1 825 PAA SOBER 01 1 1254 EXRF 83MAH 03

1 1392 10 ICPES 84HIR 01 (ug/g) 1 1414 84 RTNA 77MEL 01

1 1480 6 XRF 78TAK 01 < 10 DCPES 81 CAN 01 1 1500 100 DCPES 81CAN 01 1.9 PAA SOBER 01 1 1540 67 PAA 80KAT 01 5.4 0.5 FAA 83CAR 01 1 1570 57 11 ICPES 84NAD 01

1 1587 ICPES SOFLO 01 (ug/g) 1 1610 40 AA 77YAN 01

1 1640 6 XRF 7STAIC 01 0.8 0.02 RTNA 780ER 01 1 1640 40 AA 81 FAR 01 1.11 0.03 DNA 85GAU 04 1 1660 11 W 84WOL 01 1.11 0.05 DNA 86GAU 01 1 1695 UXRF 84ZS0 01 1.16 DNA 84GLA 02 1 1700 ICPES 84SUN 01 1.17 0.01 DNA 85GLA 04 1 1713 145 ICPES 82SCH 04

1.3 DNA S4GLA 11 1 1720 361 AE-AF 82GOL 01 1.4 PAA SOBER 01 1 1726 11 W 84W0L 01

1 1730 PAA SOBER 01 (ug/g) 1 1735 37 11 ICPES 84NAD 01

1 1737 6 AF S4NAR 02

17.9 11 FAA 83CAR 01 1 1750 6 AF 84NAR 02

21.6 1.5 11 FAA 83CAR 01 1 1750 19 11 AA 82SAK 01 22 ICPES S4SUN 01 1 1767 177 AA 83CAR 01 24 ICPES 84SUN 01 1 1768 158 ICPES S4S0B 01 24.1 6.5 ICPES S2SCH 04 1 1785 ICPES 85NAR 02

25 ICPES 80FLO 01 1 1794 AF 85NAR 02

26 WXRF 84ZS0 01 1 1794 6 XRF 78TAK 01 27 ICPES 84SUN 01 1 1795 25 11 AA 82SAK 01 29 6 35 ITNA O 1 uLn 1 1800 ICPES 84SUN 01 29.6 11 ICPES 84W0L 01 1 1800 ICPES 84SUN 01 30.8 11 ICPES ni 1 1806 37 RTNA 79DER 01 31 0.8 ICPES 84HIR 01 1 1810 6 EXRF S4JEN 01 34 3 DCPES 81 CAN 01 1 1878 11 W 84U0L 01 39.6 11 ICPES 84U0L 01 1 3240 6 EXRF 84JEN 01

(ug/g)

1 Zr (ug/g)

54 9 DCPES 81 CAN 01 1 < 55 EXRF S3MAH 03

55 3 PAA SOKAT 01 57 6 DCPES 81 CAN 01

1 71 PAA SOBER 01 1645-10
01

c

C

mo

</> CO c/> (/> </> to Ui UJ (/> UJ UJ UJ UJ CO

a. a. u z a. X > o a. Q. a. o o o o u o u O u u o o t— Q < o Q o »—

CU <\J <\i (M CM

lA 00 SO ro in in

• 1 1 o o o in I ' f • OO 1 o> o r\i I 1 PJ o >o in I to • 1 1 in OO I 1 ro ro I 1 CO 1 1 «M

5

S ^-

CO

UJ 3

c

COUJ c

Q. (D

OJ o5 y

"V,

Kt

T3s

(0 c

> OCO

+1 z UI c z (D

0) a z UJ

COS•-^ <3v~

(/> UJ UJ

C3 >o z

zoe

CO

COz

oe z

o <£

u. o

< UJ

t— X

<

UJ

-J

CLs

c

CO a 1 z> CO

EN H

COz c

UJ o (S _J o CO z <

OOo

in

Oo o

re

00

o 00 3 5

o fM sO O

00 fO

(\J

t\i ino

r- • 00 o o o fM O<M

00

in

in

ro

r2

00 rj

lo 00

00

St

o

o

00

in

00

00 W «-

OO fM

• r^

f\j

g •

: 1^ 00

o ro ro ro

ro «-

o

<0 f\i ro o

ro

«- fM ro

00 00

in I «—

r^o

o

+)

00 (M (M O in

in «—

00fM

o

ro

• fM

O (M

ro o

sr •-

o

o

o

in

ro

(M <M

fM ro 0>

00

«* . OO

ro ofM ^ .00

ro fM ro

in ro r^

• ^ fM • in

ofMro

1^. o

r>^

St

o

fM

Ofs. ro

vOo

rs.

S8

^s y—^s ^s ^s ^s ^s

in ro CM fM fVJ ro s* in in ro ro ro fM «— fM fM ro ro

fM o >0 00

st vO -O fM r>. o o o o in st 00 St o fM o O o (M fM ro fM o in Is. o 0 1 ro 1 st o • OO H M fM o H 1 I -H H H H I 1 -H +1 •H +) t s* H >* 00 >* 1 1 1 1 fM O ro

in o o» ro •* fM m fs. in fM OO rS st fM ro

ro • >* s* ro

in ro ro

o

ors.

o fM ro o CO o o O ro rs.

(/) 1 1 1 in m •M 1 » +1 1 1 H H

z 1 1 1 ^

c in -o o o (0 (M o <o

4) ro ro z -O «

CO

oCO

ro

(s- ro

1 1 1 I in o 1 1 s* t • st

•H +) ro H 1 1

1 1

1 1

1 1 «— H I1

1 •

1 «—

•H 1

1

1 •

1 rin o 00 in ro

fs. ro

COo

o

•H o

ro

o> cn o> o> ) O) cn cn cn cn at o> O) cn cn en o> ~s s> s^ \ s^ s^ \ \ "s. *s. ~s s^ >s ~s. cn o> o> o> O) D) cn cn at O) > at > cn cn D) o> cn en C X 3 3 3 3 3 3 C c c 3 »« 3 3 3 3 3 3 3 3 3 a« 3 3 3 3 c 3 3

O) D> O) >» ^ o> O) o

a« 3 3 c a<

0> —' (0 (0 9>

<3; <C CO CD CO i_<0'D"D"Da)—'Ocuj OOUOCJUCJCJOCJU 3 3 o o 3>.t-30)lD-Oa)M- U0UJUJU.0C30Z cn o <0 — 3

•—I ^ _l —I —

1

cn z

1646-1
8 «

UJ ^

X c Z C

»- <D O «>

(/> </> CO </> UJ 111 UJ UJ

o. o. a. Ol

CJ o o O

a a o^

(\J w

O lA

a.o

o

>

CO O

in o 00

(M rvj fvj

o

(/> UJ (A

a. o

3 5 5 S

O o o in

-J- fO

a. O- o o

o o

(/></>(/>(/>

UJ UJ UJ UJ

a. Ol a. o. u o o o

a a a a

in

UJ

Ck.

<\l •t- O vO o «-

^- (M un O O 00 • fM fO

rM «- «- (\i

to

UJ C

Q. CD U «

CO in

00

: § I in o

ro

O (M

in «—

00 O o CO »-

«-> s c

u

t—zUJ CM X

o i

UJ

CO zC

<D UJz X

<

ES

UJ

cs X z

a: < c/>

(/> CDz

oeOLL- <

z

< <

o a UJ

UJ X —1

a.o

cw

1 v> Q</) UJ CO

_J z CO UJ •M < (/> 1— z c o (0

«j X

^% >^

fM rj K> in nj in <\j (M ^^ v** <^ O «* o in >Q o fO fNJ o (M O in o O <o 00

• 1 1 1 III 1 • 1 in o o O o O. 1 I O

M %o * * 1 1 I 1 N- M •H I I 1 1 <\i • H H fM • 1 1 O

K> * > * ' 1 I CO 1 1 00

f 1 >o o o OO fM 1 O

O O in

« o o (M ro

in

00

CO

00CO

CO

00 o CO

K1

fM O

5

vO

in

• O r- O. «— in o• 00 o

N.o00o

1^o

fM

CO

in ooo «- oo to VIco ro in ro o ro o o fM -J- fM fM o o ro N- CO N- o 00 ro ro OO • ro o o o fM •* o o fM CO fM ro fM ro o o ro «) CO

rv. 00

CO o

5

N.

• o O 00 «— in

fM

roo

o

IC

ro

o in

CO

CO

CJ oro

fM ro «- ro >*• CO ro

0> o> fM

«o

V* o o ro o +) H m +1 H 00 H

o -* -o N. *

OO

ro o ro

ro «—

CO ro CO

to vO «- «- fM -d- »- CO fM inin«-ininfM-*^

in

00

r^

00

o ro o o vO o o vt o o o in o 00 o to o •H •H »- o o H oCO o • H H M CO +1 H

in

to o 00 O ro CO o to o

ro

in

>* O

o

OoCO

8:

vO

CO

fM

o

CO

caz

c

(D«>

OCOM

00 ro m

H •fi H

fM o CO

ro •*in 00

fM

r^ (^ o 00 oo o o o «-

in o in

«- o in

•H CO

ro

CO o> O) o> D) o> o> O) O) 0) o> O) t— \ v^ \ \ \ \ \ \ >^ > O) O) O) o> O) > > O) O) O) O) (7) CD (7! O) z!3 3 3 34 3 3 3 3 3 3 3 3 3 3 >S c 3 c C C c s« 3 3 3 3 C 3 3 3 3 3 3 3 3 3

O)3

CXO (D ^ 73 — ^ c ^ 0.0.0.0.0:

> — — >

.Qoajooflj— Ei-

(/>(0(/>(/>(/>(/>(/>(/l(/9(/>

fO .Q «».£•-—• .a c c t. 3 > >- >• isl tsl tM

1646-2
TABLE 1646-2: INDIVIDUAL DATA FOR NBS SRH 1646 (revised 3/1/86)

Cone Uncer Com Method Reference [ Cone Uncer Com Method Reference

Aq (na/Q)

1

1 Cl (%)

88 a FAA 83BL0

1 01 1 1.383 0.054 ITNA 85SUN 01

Al (%)

1

1 Co (ug/g)

5.12 0.17 ICPES 84HIR 01 1 7.8 0.3 ICPES 84HIR 01 5.2 0.12 DCPES 81 CAN 01 1 8 2 ITNA 85HOL 01 5.4 0.2 DCPES 82SIN 01 1 8 • 2

5.93 0.3 ITNA 85SUN 01 1 10.6 0.6 ITNA 85SUN 01

6.03 0.2 ITNA 85HOL 01 1 11 1 ITNA 84GLA 11 17 3 DCPES 81 CAN 01 As (ug/g) 1 19 3 DCPES 82SIN 01

io.5 0,9 ITNA 85HOL

1 01 1 Cr (uq/g)

11.1 0.6 DCPES 84URA 01 1 11.7 2.5 lENA 85HOL 01 1 72 0.3 ICPES 84HIR 01

1 72 1 DCPES 82SIN 01

B (ug/g) 1 74 1 DCPES 81 CAN 01 75 1 ITNA 85HOL 01

81 3 TCGS 85GAU 04 1 78.4 3 ITNA 85SUN 01 84 8 TCGS 84GLA 01 1 80 ITNA 84GLA 11

1 84 5 ITNA 86GAU 01 Ba (ug/g)

Cs (ug/g)

370 ITNA 84GLA 11 j 448 50 ITNA 85SUN 01 1 3.6 0.2 ITNA 84GLA 1

1

1 3.6 0.4 ITNA 84GLA 02

Be (uq/q) 3.7 ITNA 86GAU 01

1 3.7 0.6 ITNA 85H0L 01 1.5 0.14 ICPES 86GAU 01 1 3.85 0.15 ITNA 85SUN 01

Br (ug/g)

1

1 Cu (ug/g)

112 1 ITNA 85SUN 01 1 13.3 0.6 AAC 85GAU 04

122 2 lENA 85H0L 01 1 16.8 ASV 83MAD 01

1 17.8 0.4 IDHS 84BR0 03

Ca (ug/g) 19 0.6 ICPES 84HIR 01

1 31 2.8 DCPES 81 CAN 01 8120 AA 85GAU 04 1 8760 620 ITNA 85SUN 01 1 Dv (ug/q)

Cd (ng/g) 1 2.8 0.21 DCPES 81 CAN 01 260 AAC 85GAU 04 1 4.04 0.07 ICPES 85JAR 02

355 40 FAA 86GAU 01 1 5.98 0,23 ITNA 85SUN 01 360 10 IDMS 84BR0 03 1 Er (ug/g)

Ce (uq/g) 2.41 0.04 ICPES 85JAR 02

76 0.9 ICPES 85JAR 02 1 77.2 1.6 ITNA 85SUN 01 1 Eu (ug/g)

82 ITNA 84GLA 11 1 1.34 ITNA 84GLA 11 84 8 ITNA 85HOL 01 1 1.36 ICPES 85 JAR 02

110 4.1 DCPES 81 CAN 01 ' 1.62 0,17 ITNA 85SUN 01

c

1646-3
TABLE 1646-2: INDIVIDUAL DATA FOR NBS SRM ^6A6 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Fe (%)

1

1 Hg (%)

r

'

2.9 0.05 DCPES Q i A U 01LAN Ul 1 0.9 0.08 lENA 85HOL 01

3 0.15 DCPES 82SIN 01 1 0.969 0.015 ICPES 8AHIR 01 3.02 0.04 ICPES 84HIR 01 1 0.97 AA 85GAU 04

3.38 ITNA 84GLA 11 1 0.97 0.09 ITNA a^SUN pi

3.49 0.1 UNA 85SUN 01 1 3.52 0.11 ITNA 85H0L 01 1 Mn (ug/g)

Ga (ug/g)

1

1 270 15 DCPES 82SIN 01

1 280 5 DCPES 81CAN 01

19 1.6 DCPES 81 CAN 01 1 328 3 ICPES 84HIR 01

1 356 17 lENA 85HOL 01 Gd (uq/g) 1 362 8 ITNA 85HOL 01

385 20 ITNA 85 SUN 01

3.7 0.4 4 TCGS 85GLA 05 1 4.6 0.8 4 TCGS 85GLA 05 1 Mo (ug/g)

5.09 0.13 ICPES 85 JAR 02 1

1 9 0.3 ICPES 84HiR 01 Hf (ug/g) 1 19 2.5 DCPES 81CAN 01

11.1 0.7 ITNA 85SUN

1 01 1 Na (%)

11.2 ITNA 84GLA 11 1

1 1.82 0.01 lENA 85HOL 01 Ho (ug/g) 1 2.1 0.2 ITNA 85HOL 01 2.19 0.02 ITNA 85SUN 01

0.84 0.03 ICPES OC 1 Jl D

o!> JAK Nb (ug/g)

I (ug/q) 1

1 53 4 DCPES 81CAN 01 32.5 2.9 ITNA 85SUN 01 1 36 2 lENA 85H0L 01 1 Nd (ug/g)

K (%)

1

1 32.6 9.7 ITNA 35SUN 01

1 34.7 0.6 ICPES 85JAR 02

1.43 0.17 lENA 85HOL 01 1 40 ITNA 84GLA 11 2.23 0.25 ITNA 85SUN 01 1 Ni (ug/g)

La (ug/g) 1 31 1.5 DCPES 81CAN 01

35.7 0.5 ICPES 85 JAR 02 1 31 5 DCPES 82SIN 01

36 0.63 DCPES 81 CAN 01 1 32 0.3 ICPES 84HIR 01 38.9 1.3 ITNA 85SUN 01 1 32.8 1.7 AAC 856AU 04

Li (ug/g)

1

1 P (ug/g)

46 AA 85GAU

1 04 1 433 1 ICPES 84HIR 01

529.6 3.9 DCPES 84^RA 01

Lu (ng/g)

Pb (ug/q)

320 ICPES 85JAR 02 1 26.5 ASV 83MA0 Q1

370 ITNA 84GLA 11 1 28 4 FAA 86GAU Ot 444 18 ITNA 85SUN 01 1 29 1 AAC 85GAU 04

1646-4
TABLE 1646-2: INDIVIDUAL DATA FOR NBS SRM 1646 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Pr (uq/q>

1

1

1

la (ug/g)

fto . DO U- It T TDCC 85 JAR 02 1 U .TH T Tk] A 1 1 NA 84GLA 11

1 A7 1 .07 0.16 ITNA 85 SUN 01 Rb Cug/g) 1

1 Tb (ug/g)

TTMA 1 1 nM 84GLA 11 1

f1 TMA 1 Nn 85SUN 01 1 T TUA 84GLA 11 nu.yoOft n 1

U. lo T TU A1 1 NA 85SUN 01 SD (ng/g) 1

1 Th (ug/g)

fln 1 cNA 85HOL 01 1 o 1 u 1 1 NA 84GLA 11 1 n A T CU A 1 CNA 85HOL 01

T TUA 1 1 NA 84GLA 02 1 Oy .oA f Ty A 1 1 NA 84GLA 11 yiu T TUA 1 TNA 85SUN 01 1 in 1 n / U.H I TNA 85SUN 01 in / f Tkl A

I TNA 86GAU 01 sc (ug/g) in1 U . 7r

f TUA 1 1 NA 85GAU 04

1 n 7 T Tkl A

I TNA 85H0L 01 n /. I TNA 84GLA 11 1 in / lU.H n o T TLI A

1 1 NA 84GLA 02 1 Ti (ug/g)

1U. f n X f Ckl A IcNA 85HOL 01 1 in o lu.y n /. T Tkl A

1 1 NA 85HOL 01 1 1 AA lUU DCrcS 81 CAN 01

11 0.2 UNA 85SUN 01 1 3600 360 DCPES 82SIN 01 11.56 0.06 I TNA 86GAU 01 1 3750 150 ICPES 84HIR 01

f TkIA 1 1 NA 85HOL 01 Se (ng/g) COO"? T TUA 1 1 NA 85SUN 01

430 20 HAA 85CUT 01 1 Tl (ug/g)

580 50 GC 83SIU 01 1 590 60 ICPES 83SIU 01 1 16 2.7 DCPES 81 CAN 01

SedV) (ng/g) 1

1 U.O U A A HAA 85CUT

1 01 1 o o c.y nuA UNA 84GLA 11 2.96 0.09 DNA 85GAU 04

Se(VI) (ng/g) 3 DNA 84GLA 02

1 3.01 0.1 DNA 86GAU 01 40 20 HAA 85CUT 01 1 3.07 0.48 ITNA 85SUN 01

SI (X) 1

1

V (ug/g)

n C5 ULrcb 81 CAN 01 1 Od X f TkIA

1 1 NA 85SUN 01

"zn

1 .e DCPcS 82SIN 01 1 fl7 c T TUA 1 1 NA 85HOL 01 moc T PDCC 84HIR 01 Sm (ug/g) 1 OT £. J ULrto 81 CAN 01

1 ooOT y 82SIN 01 o.e 0.6 4 TCGS 85GLA 05 1 o. c 1 A IT iLrts 85JAR 02 1 Y (ug/g)

U . 1

1 TkIA 1 1 Nn 85SUN 01 1 A ft AU.O / TCbS 85GLA 05 1 1 f

1 /. UUrCb 81 CAN 01 19.9 0.4 ICPES 85JAR 02

Sr (ug/g)

220 73 ITNA 85SUN 01 1

1646-5
TABLE 1646-2: INDIVIDUAL DATA FOR NBS SRM 1646 (cont.)

Cone Uncer Com Method Reference I

Yb (ug/q)

2.12 0.02

2.2 0.08

2.56 0.13

3.4

ICPES 85 JAR 02

DCPES 81 CAN 01 ITNA 85SUN 01 ITNA 84GLA 11

Zn (ug/g)

107

120

130

139

3

8

1

ICPES

DCPES

DCPES

AA

84HIR 01 82SIN 01

81 CAN 01 85GAU 04

270 12 DCPES 81CAN 01 400 ITNA 84GLA 11

1646-6
TABLE 1647-1: COMPILED DATA FOR NBS SRM 16A7 PRIORITY POLLUTANT POLYNUCLEAR AROMATIC HYDROCARBONS (IN ACETONITRILE)

LUnrUUNU LAo IF

1 ly T TC UN I 1 o NBS

Mean ± SO nean ± su Cn)

ncU 1 AN RANGb METHOl

Acensphthene mrt /I mg/L 21.0 ± 0.4

Acenapntny I ene cuoyoo mnmg/L/I 19.1 ± 0.2

Anthracene 1 5(11 57 ing/L 3.29 ± 0.10

Benz [a] anthracene jOjjj rMmg/L/I 5.03 ± 0.10 senzo LDJ T luorantnene /I tng/L 5.11 ± 0.10

5nQ005 ug/g (3) O T/. £. O T/. - o C . OH C

HPLC

Bcnzo [k] f luoranthene mg/L 5.02 ± 0.10

cu 1 uoy ug/g 7 A * n 7 \.o) 17 UDi r

Dt^n^u Lyii 1 J yjGi y i cnt? 1 T

nvi /I ing/ L 4.01 ± 0.10 oenzo Laj pyrene mg/L 5.3 ± 0.1

Chrysene c lou ly mg/L 4.68 ± 0.10

Dibenz [a,h] anthracene nn /I mg/L 3.68 ± 0.10

Fluoranthene 206A40 mg/L 10.1 ± 0.2

Fluorene 86737 mg/L 4.92 + 0.10

I ndeno [1,2,3- cd] pyr ene 193395 mg/L 4.06 ± 0.10

Naphthalene 91203 mg/L 22.5 ± 0.2

Perylene 198550 ug/g < 0.1 HPLC

Phenanthrene 85018 mg/L 5.06 ± 0.10

Pyrene 129000 mg/L 9.84 i 0.10

TABLE 1647-2: INDIVIDUAL DATA FOR NBS SRM 1647

Cone Uncer Com Method Reference

Benzo[b3 fluoranthene (ug/g)

1.04 12 HPLC 850TT 01 2.34 12 HPLC 850TT 01 2.34 12 HPLC 850TT 01 2.39 12 HPLC 850Ti 01 2.47 12 HPLC 850TT 01 2.65 12 HPLC 850TT 01

Benzo[k] fluoranthene (ug/g)

1.22 12 HPLC 850TT 01 2.04 12 HPLC 850TT 01 2.42 12 HPLC 850TT 01 2.42 12 HPLC 850TT 01 2.86 12 HPLC 850TT 01 3.17 12 HPLC 850TT 01

Perylene (ug/g)

< 0.1 HPLC 850TT 01

1647-1
CO 4-> 8 ^

m (A O **c

(0

a:

I- X

o

-O

CO

oc CD oc oe. X u X X

N. «- o

in «- >0

OfX

o

X

o

o

3

v»

U- o oe 00 X t- o

ro

\—

>*o

o

+t • oo• >*

X —

-O

OfX

o

X X

in Na</) </> UJU— c

0)

5

to

(M ro «* ro ro

-* o o

00 ro o (M ro in

;* o o>

1 • -H 1 H o H +) H

I M 1 in ro o vO 00 o

t2 <M ro

«* in ro to 1"1 ro ro f

^- <\1 (M

O O 00 o

3

-

«— m >*»—«— in «—

ro o fM o ro o o in rvj o CM o in O

o

H •H M +) +t H •H H •H H

o 00 ro ro 00 ro o N. in

(M o in o

>d in in si >*• ro

ro

o

f2

in

CO

ro

CO

ino o M (M

>o

o

oCOo roo

rvi

•H ro o

in

in o -H ro

CO ro

CA

c

(00)

pvi ro

CO CO ro

•H

vo' ro

ro N- ro COm o o f\I (VI rj in o

•M

1 -H I I m +1 M +1

1 CO rvi 55 ht^ o- m ro in ro

sr 00 w ^-^ o

roro -J- o o CO CO

<

LU

O (MO in o- o o o o • ro

• «- O V*

•>0 ro «- >0 00 11)11

CO m (M CO o • o «- in

in . »- «- r>- ro

ro in

oO . - _ (Min L/^ o o «— •>0 »--oF-vOst(M^ro>o

jO

CO (M

^*• in

r*- o • ro (M in

or^-*or\joino vO >o m o »- CO

-J- in in ro

fM ro o - CO

r^ in O SCO «- ro

>4-

o o in

ro ors. ro

>* ro in o ro

>* >o 0>

<y m in o ro

CO ro

(M o in (M

(M

(M

CO «- fM

<0 in O ro

o o

oo o o eg «- O 00 (M o o ^

(M N.

t^

o o h- ro «- NO 00

r

C in CO fM m ro (M CO ro ro o ro r>- ro in fM (M ro ro (\j m

ro ro in o fM ro o CO fM fM in O o cn (/> (>• o in >» ro C" m m

z o o ro >! o (M 00 o fM fM o fM o O ro o fM in <3 ro vO

SE O o> O >*• fM 1 o >*• H H •H H O •M +1 •H •H +1 H •M •H M -H •H +1 *t M +1 s

•M +) ro H H

z o ro (M 1 o o c fM ro o >o vO ro fM in o r--. in o in fM >o 00 ro o« O fM fM u ea fM o 00 r^ m o o CO o *— o ro ro fM

vO (M in ro ro •o 00 CO X ro in o ro «

o a o vt o fM r«- o (M o o in •o

r- 1 o 1 1 in o 00 00 1 1 1 •* o 1 o (M 1 o O 1 CD M H +1 1 1 o 1 1 in o H ro M H 1 1 fM 1 1 o •H >* 1 o 1 z 1 in t 1 in o 1 1 1 1 1 o 1 o 1 c rvj in ro <y in CO m •J- r— IC o o o «> -* vO z ro ro

(/> Ol O) o> Dl CD O) o> O) o> cn Ui 1

u> at at at

I— \ \ >^ \ >» >>. o> > o> D) O) O) o> at o> ••-> O) at O) o>

UN 3 3 a 3 >« 3 3 3 3 3 3 3 3 3 3 »« 3 <o c 3 c 3

ofM

LU

_1 M (Q « E- (9 TJ V O t_ (A 3 3 « (D T> H- c 10 3 at c o

UJ < < CD CD 00 CD (J U O o u u U U o Ul Lt_ O (3 _l _l z z

16A8-1
"8

JZ 8 £

tx

a

to

CDO

in

Ckf o:

O Of

X >: > X

«- rj «- ro

Vn' Vrf*

t\j «—

<M

O 00

o

to

0£

U. 11.

O u. u- a£ QC u oe Of X X I- X X

a:X

«— ^ »- (\j

in

o

o • o -4- 1- rsjoo

X

X

Oo00

oCO UJ

a. •H

4-* c Ll o <D o QJ \^ 2Z Oc

lU

1—f— ^-x < C z

lU

O < CO _l

<c

o

»—

_

a:< «> o. SI z<ma£

=3CO

3C

Of

_

(/>

(/> 3E mz

Ofo

UJ < o t—< "I

oe

a

>ILE S z u <o 1 x: CO

;s«—

UJ

_i

C <

</> =>

O</} z

LU

+1 zo c u

in

O

•J- Oooo

o

(M

<M

00

Kl -*

v-^

<M

O>»

O

oo

o -M

M

>* CO

OfVJ

^\

<~ >*• K> sf Kl «— Kl (M Kl in >* \^ v> No/ ^>

o (\1 (M

o N-

•o • o

o CM K) rj o CM O CO O in o <o O in 1 1 1 1 Kl o o ) H ^ 1 • *i I +4 •H «— M f\l +< H H H H 1 1 1 1 1 1 o >* in m fVl <o O in f\l OJ o Kl in o

(M >*

o in •*

oCO

«-

o 00 (M

COo

CIJ

oKlo

ino

ooooKl

in

00

in

CM

in

K>

in

1^

03 • 00 vO CM «- ^

«-

O V* • CM

^0

O

OCM

CMOo IS

00

o o>

o in • Kl

V* in «- >!•

00

•O in o»- Kl

CM

O vO CM • ^ • M nO ^ «-

CM

CM

tno -J- . • «-

in «-

ofx.

CMO

ooo00

in

X*

X*

X* in X* in X* xO in Kl CM Kl xt CO Kl w w

CM

J—

O Kl

X-' ^> x^

CM

\^o Klx^ CM

o

O <l in

o

O

o IM in CM

O

o «— 00

O CMO 00O CM V

CM CM »

<y

Oo CM o CM H H +1 44 +) X* +4 •H •M 41 41 41 4) « CM H n H • •o in CM

oo' in xCf

O X*O x* 1^ >oO in CMO

O (Mo in X* CMO S- CM

K) CO CM K» X* CM

O in xd- f£

CM

m X* x* X*-

xjO in

9:

oCO

c/> CO 4< z c

(0

00 »- o o

o

O CM Kl 00 CM in

o CMo X* in x*

M 41 4< in xl- 41 CM

A250

(M

00

6550

in in

CM

xt

X*

O• o

x»-

CO

ir\

o • x* in »-o

rS

xt

>«»«»< > a> o> O) o> D) o> Dl O) o> O) O) O) > O) o> O) x^ *«x Xx *Xx "Xx Xx ~xx >Xx \ Xx ~x. "v. -X «^

o> C7> a> o> O) a> Ol O) O) O) ) Ol Ul Ol o> 3 3 3 3 3 3 3 3 « 3 3 3 3 3 3 3 3 3 3 3 3 3

xt Kl

3=

O CO •—

X a. a. o£ J3

c t- > 3 >- >- tM fM

1648-2
g

SIJ

3CC

CA (D Z 0) < z LU8

Ul +-» X 01 X

4-* c

c

ou

c

(D oe V m X

1ATT

TE»<

UJ

uuz 1— < QL<z<CO

a:3 z< 00

EOX

Xoc

v>

vt

c

caz

Ofo (/>

o(/> 00 < z 1— Ul •H < (/> z c o <0 a o V

UJ

X —1

a.o

</) CD 1 z

00

;s

LEm (/> < 1—

</> X

(J 1 ou —I 13 _j

T—

o ID

ro rg in

c/>

XX 1 o o 1 u 1 o

^\

rvi

oo 00 *—

to

o

(A (/> to U U O

OU

O (9 C3 -J

—

>o

o ^ in sf r>^ X z

C3O

o 00 in "O

to

00

o

o f\J 00 vt 1^ 00o 00

>o o>

to to ro to eo vt

o vt 1 o in 1 1 1 to -o 1 vt 1 •o o 1 O

to

m <M to

o vt in vt

OO

iv!

CO to • *1 • Noin00

rsi to 1 vt

O

to (M to to to to (M lO

to vt

o

O

o ino ino

o o>o in CO ro >o tv. to •H •M •H H +1 «

to •o to vt o O o 00

to OO •o

at o> cn o> o> v^ \ \

at o> O) > O)

c 3 3 3 3 3 3 3 3 c 3 2

(M <M o> c>

o in

oo CO to vt 00 00 T

vt

O in oo

o in fVl f\j O- o o to in o

o in ro rvi rv. 00 to 00

o

o (M o «^ o o & O in CJ

in in t\i fSJ 00

t

8a.s c c —

<U >v o2 S.

0)cu

(0c< cNc

(U CO

0)cc

(0o

I- 3

a< ra <u ^ c c «C

OJuao

o» to cO CO

4)c

ID

0) *-> r- c ~

«) - _

cfl

c

C

—> <<9 >^ O « " C v^ C •»-• (0 o a> c 3 "E

0) - c

>v

C 0)

L. 01 i0> £ >.

a. a. a.

1648-3
TABLE 1648-2: COMPILED DATA FOR NBS SRH 1648 (revised 3/1/86)

Cone Uncer Coin netnou Reference | Cone Uncer Com Method Reference

Anthracene (ng/g) j Phenanthrene (ug/g)

310 GC-MS 84SIM 03 1 4.6 0.3 LC 84MAY 01 360 10 1 r 84MAY 01 1 4.8 84SIM 03

1 .2-Benzanthracene (ug/g) 1 Pyrene <ug/<3)

2.7 GC-HS 84SIM 03 1 6.1 GC-MS 84SIM 03

2.8 0.1 44 LC 84MAY 01 1 6.8 0.2 44 LC 34MAY 01 3.2 0.1 44 LC 84MAY 01 1 7.4 0.2 44 LC 84MAY 01

Benzo(g,h,i)Derylene (ug/g)

1

1

5.5 0.8 LC 84MAY 01 1 5.8 0.9 lENA 84GLA 07

6.8 GC-MS 84SIM 03 1 6 1 D XRF 79GIA 03

1 6 1 VD C XKr 77GIA 02

Benzo-a-pvrene (ug/g) 1 6.18 FAA 83BL0 01

1 6.2 NAA 83BL0 01 2.6 0.2 44 LC 84MAY 01 1 6.4 0.5 ITNA 79GRE 01 3.3 GC-MS 84SIM 03 j 3.4 0.2 44 LC 84MAY 01 1 Al (%)

Benzo-e-pyrene (ug/g) ] 3.05 0.03 AA 81FRA 01

1 3.05 0.17 ICPES 84JEN 02

6.8 84SIM 03 1 3.1 0.1 T1 TMA 1 fin 84GLA 07

3.12 0.2 35 ITNA 81GLA 03

Benzo-k-f luoranthene (ug/g) 1 3.3 ICPES 80FLO 01

1 3.3 ITNA 84TU 03

3.3 0.1 44 LC 84MAY 01 1 3.3 0.45 AA 81 FAR 01 3.4 0.05 44 LC 84MAY 01 1 3.5 0.1 ITNA 79GRE 01

Chrysene (ug/g)

1

1 As (ug/g)

6.6 0.1 44 LC 84MAY

1 01 1 104 10 ICPES 84JEN 02

6.6 0.2 44 LC 84MAY 01 1 112 ICPES 80FLO 01

1 112 2 AA 83BYR 01

F luoranthene (ug/g) 1 113 12 FAA 83L0V 01

1 117 ICPES 82NYG 01 7.4 GC-MS 84SIM 03 1 117 HAA 84YAM 01 7.9 0.6 44 LC 84MAY 01 j 117 5 ITNA 79GRE 01 8.7 0.4 44 LC 84MAY 01 1 117 5 ITNA 84GLA 07

1 117 6 1 1 1 1 84SCH 03

Indenod .2,3-cd)Dyrene (ug/g) 1 119 35 NAA 81GLA 03

1 119 2 lENA 84GLA 07

4.6 GC-MS 84SIM 03 1 119 2 11 ICPES 84SCH 03

4.7 0.2 44 LC 84MAY 01 1 4.8 0.2 44 LC 84MAY 01 1 B (uq/g)

Perylene (ng/g) 158 15 TCGS 84GLA 01 6000 170 UU 81FRA 01 520 GC-MS 84SIM 63 1 650 20 44 LC 84MAY 01 1 690 20 44 LC 84MAY 01 1

1648-4
TABLE 16A8-2: COMPILED DATA FOR NBS SRM 1648 (cont.)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ba (ug/g) Cd (ug/g) cont

740 60 ITNA 79GRE 01 1 72 11 AA 82YAM 01 757 35 D XRF 79GIA 03 1 72 1 11 ICPES 84SCH 03

757 35 XRF 77GIA 02 1 73 ICPES 80FLO 01

77i* ICPES 80 FLO 01 1 74 2 AA 838YR 01 800 10 5 ITNA 84GLA 07 1 75 7 AA 84GLA 07

840 40 lENA 84GLA 07 1 75 8 ICPES 84JEN 02

980 100 5 ITNA 84GLA 07 1 105 9 AA 81FRA 01

Be (ug/g)

2.3 0.2 11 ICPES 84SCH 03 1 52 5 lENA 84GLA 07

2.5 0.2 11 ICPES 84SCH 03 1 53 2 ITNA 84GLA 07

3 ICPES 80 FLO 01 1 54 3 ITNA 79GRE 01

Br (ug/g)

61

CI (ug/g)

ICPES 80FLO 01

460 15 5 lENA 84GLA 07 1 500 30 ITNA 79GRE 01 1 500 60 35 ITNA 81GLA 03

504 14 5 lENA 84GLA 07 1 4500 200 ITNA 79GRE 01 517 14 XRF 79GIA 03 1 4890 80 I TNA 84GLA 07

517 14 XRF 77GIA 02 1 4900 ITMA 03

526 24 35 ITNA 81GLA 03 1 526 25 ITNA 84GLA 07 1

15 3 ICPES 84JEN 02

15 2 0 9 AA 81 FRA 01 ^L 7 PR

1

. 171 f 7£ u o T1 TMA 1 nn fKLCX OHULMA

15.27 0.15 uu 81FRA 01 1 17.6 0.5 ITNA 79GRE 01 18 1 lENA 84GLA 07

Ca (%) 19 2 11 ICPES 84SCH 03

20 3 11 ICPES 84SCH 03

5.4 0.3 lENA 84GLA 07 1 28 ICPES 80FLO 01 5.5 0.4 AA 82GLA 02 1 42 7 35 ITNA 81GLA 03

5.6 0.4 AA 84GLA 07 1 5.77 0.38 ICPES 84JEN 02 1 Cr (ug/g)

5.8 0.5 ITNA 79GRE 01 1 6.1 0.04 EXRF 78PEL 01 1 173 27 FAA 81 FAR 01 6.18 0.23 AA 81 FAR 01 1 380 21 ICPES 84JEN 02

6.3 0.3 ITNA 84GLA 07 1 380 40 AA 84GLA 07

383 AA 82GLA 02

Cd (ug/q) 396 6 11 ICPES 84SCH 03

398 ICPES 80 FLO 01 64 7 AA 82GLA 02 1 402 10 ITNA 79GRE 01 69 4 FAA 81 FAR 01 1 410 8 ITNA 84GLA 07

70 2 XRF 77GIA 02 1 410 50 35 ITNA 81GLA 03

70 2 D XRF 79GIA 03 1 417 16 AA 81 FRA 01 70 6 ITNA 79GRE 01 1 440 10 EXRF 78PEL 01

71 2 11 ICPES 84SCH 03 1 560 11 UU 81 FRA 01 72 11 AA 82YAM 01 1 580 50 UU 81 FRA 01 72 11 AA 82YAM 01 1 72 11 AA 82YAM 01 1

1648-5
TABLE 1648-2: COMPILED DATA FOR NBS SRM 1648 (cont.)

nc LllvAJ Reference | uuiii nci.nou Referenc^

1

1

1 T T f

1 PMA CNH 84GLA 07 1 ROn "KJ U . H T1 FUA CNM 84GLA 07

f TMA 79GRE 01 1 7? T rDF<i 80 FLO 01 J • f w TTMA 84GLA 07 1 ua (ug/g^

II 1 1 in / n\

1 S7n ^ f u AA UN 81FRA 01 1 T 1 J.I A TPR^ 85GLA 05

JO 1 lO Al\ r 77GIA 02 1 T 7 n L A TPHQ 85GLA 05

Sfl'> 11 11 AA 82YAM 01 1 JOO 1

1

1 1 AA 83BYR 01 1 H f

cc PAA rMM 81 FAR 01 1

1 £ MMAA 81FRA 01 1 7 7% WD 84GLA 07

1

1

1 1 MMAA 82YAM 01 1

1

1

1 1 MMAA 82YAM 01 1 nr ^ug/g;

111 1 MMAA 82YAM 01 1 MMAA 82GLA 02 1 TTMA I 1 nM 79GRE 01 iOA JTO 80FLO 01 1 U > U r TTMA 1 1 nM 84GLA 07

Ann MMAA 84GLA 07 1 n A TFMA I cnM 84GLA 07

f

1

1

1 Lrco 84SCH 03 1 609 29 11 ICPES 84SCH 03 1 I (ug/g)

610 18 UU 81FRA 01 1 640 60 EXRF 81KIN 01 1 16 2 XRF 77GIA 02

OOT T TIJA 1 1 NM 84TU 03 1 1A 79GIA

TCO? 84JEN 02 1 10\y mC? n I^F 85COE 01 700 100 EXRF 78PEL 01 1 20 5 ITNA 79GRE 01

1

1 1-129 (ATOM/G)

ft 77 ft ft'? T1 TMA 1 nM 84GLA 07 1 nU« 70f 7 n nR TTMA 1 1 nM 79GRE 01 1 38 UU 83BPN 01

1

1 1

1 rpF^ Ur Cd 80 FLO 01 1 1 ft 0 6 "^R PTNA 83LUT 01

e I*;

1

1

Tinn tvny/y/ nn i f\\

X^ • nu 1

1

1 1 Mm 82YAM 01 1 7 n't 1

1

1 1 MmAA 82YAM 01 1 OAn 70 TTMA I 1 nM 79GRE 01 n n<; MMAA 81FRA 01 1 7 7 A A MM 82GLA 02 1

•IOaf7 n ?^ 84JEN 02 1

ftU.J TC f

1 TMA 1 NM 81GLA 03 1 nU OATO 0 1? TTMA 1 1 nM 84GLA 07

n nR TTMA 1 1 nM 79GRE 01 1 0.11 ITNA 79GRE 01 0 06 TTMA I 1 nM 84GLA 07 1 1 01 ITNA 84TU 03

Jay 1

1

1 1 MMAA 82YAH 01 1 0 02 FXRF 1^ Ai\ r 78PEL 01 TJaTO 1

1

1 1 MMAA 82YAM 01 1 1 n7 I PMA 84GLA 07

ft 1 T1 PMA CNM 84GLA 07 1 1 11 Q 08 '^S I TMA 81GLA 03

Y OA n n'^7 FVDP CAK r 78PEL 01 1 A ft n 1 U. 1 CAKr 81KIN 01 1 laLa ft(ug/g; tn /n\

ft 1 Art 77GIA 02 1 n 1 Ai\ r 79GIA 03 1 ICPES 80FLO 01

4.1 ICPES 80FLO 01 1 38 3 35 ITNA 81GLA

4.2 0.4 AA 84GLA 07 1 40 2 ITNA 84GLA

4.5 0.23 AA 81 FAR 01 1 42 2 ITNA 79GRE 01

5.45 0.32 UU 81FRA 01 1 42 5 lENA 84GLA 07

5.65 0.14 UU 81FRA 01 1 1648-6
TABLE 1648-2: COMPILED DATA FOR NBS SRM 1648 (cont.)

Cone

Lu (ng/g)

34

Mg (ug/g)

5500

7200

7500

7600

8000

8300

9000

Hn (ug/g)

740

747

770

770

790

790

805

810

810

830

840

850

851

852

860

870

877

880

880

961

961

Mo (ug/g)

17

17

18

21

N (%)

3.25

Ha (ug/g)

4000

4100

4220

4600

5500

600

400

400

130

800

30

10

20

80

4

40

60

40

85

20

30

19

80

34

34

0.04

11

11

35

11

11

11

11

200

120

200

1500

5

535

Method Reference | Cone Uncer Com Method Reference

1 Nb (ug/g)

ITNA oAGLA n7 1 [Jf

1 22 3 XRF 77GIA 02

Ni (ug/g)

ITNA O/ Tl 1 54TU AT 1 Oi 1 62 6 11 ICPES 84SCH 03

AA 82GLA 02 1 72 15 AA 82GLA 02

AA n7 1 Of 1 74 5 ICPES 84JEN 02

AA ol FAR U 1

1 74.2 11 AA 82YAM 01 AA Ol PKA 1 Ul 1 75 11 AA 82YAM 01 ITNA TO/* DC ni 1 U 1

1 75 4 lENA 84GLA 07

ICPES on CI n oUrLU ni 1 U 1

1 77 1 11 ICPES 84SCH 03

79.5 11 AA 82YAM 01 80.5 11 AA 82YAM 01 83 4 EXRF 78PEL 01 lENA OHULM (17 1

1 84 VOLT 84BRA 01 ITNA D/ f*l A OHbLA f\7 1 Uf 1 85 ICPES 80FLO 01 AA QOV AU O^YAM Ul 1 99 13 XRF 77GIA 02

AA OOV AU U1 1 100 7 UU 81FRA 01 ITNA ryGRc m 1 Ul 1 105 21 AA 81FRA 01 AA 84GLA fl7 1 Of 1 AA o1 rRA A1 1 U 1

1 Pb <ug/gj

ITNA Ol bLA 1 Uj I AA Qi CAD O 1 rAK 1 6100 200 AA 82GLA 02

ICPES OH Jtn (13 1 6200 810 UU 81FRA 01 UU ftl PDA ni 1

1 6210 85 FAA 81 FAR 01 AA OOVAU ocTAn ni 1 6300 100 XRF 77GIA 02

ICPES Ann our LUn ni 1

1 6300 300 AA 84GLA 07

AA OcTAW ni 1

1 6400 45 AA 81FRA 01 EXRF o N ni 1 6510 11 AA 82YAM 01 EXRF TfiDCI f OrtL ni 1 U 1

1 6530 AA 82YAM 01 ITNA ft/ Tl 1 OH lU ni 1 Uj I 6530 120 ICPES 84SCH 03

UU Oi EDA o 1 rKA ni 1 Ul 1 6550 AA 82YAM 01 AA no 1 Uc 1 6550 190 11 ICPES 84SCH 03

XRF "77^ f A

f rbIA no 1 6560 100 AA 83BYR 01 XRF 79GIA 03 1 6630 11 AA 82YAM 01 6760 70 ICPES 84JEN 02

6780 60 EXRF 78PEL 01 XRF 6900 200 EXRF 81KIN 01 ICPES 84SCH 03 1 7000 ICPES 80FLO 01 ICPES 84SCH 03 1 lENA ft/. OhULA PI A n7 1 Ur 1 Pr (ug/g)

8 ICPES 80FLO 01 CB OhuLA AAri A

Rb (ug/g)

ITNA 79GRE 01 1 52 9 ITNA 79GRE 01 ITNA 84TU 03 1 53 5 ITNA 84GLA 07

ITNA 84GLA 07 1 55 6 35 ITNA 81GLA 03 ITNA 84GLA 07 1 58 2 lENA 84GLA 07

ITNA 81GLA 03 1 1648-7
TABLE 1648-2: COMPILED DATA FOR NBS SRH 1648 (cont.)

Cone

s (%)

Sb (ug/g)

Sc (ug/g)

Si . W

Uncer Com Method Reference

0.06 UU 81FRA 01 1 190 10 EXRF 78PEL 01 211 6 XRF 77GIA 02

220 10 lENA 84GLA 07

450 ICPES 80FL0 01

41 ICPES 82NYG 01 1 44 3 XRF 77GIA 02 1 Ta (ug/g)

44 3 D XRF 79GIA 03 1 44 6 ITMA 84GLA 02 1 6.76 0.17 ITNA 84GLA 07

45 3 ITNA 79GRE 01 1 7.2 0.4 lENA 84GLA 07

47 2 ITNA 84GLA 07 1

6i6 0.2 ITNA 79GRE 01 1 7.5 0.5 ITNA 84GLA 07

6.6 0.6 ITNA 84GLA 02 1 7.8 0.4 lENA 84GLA 07

6i8 35 ITNA 81GLA 03 1 La 0.3 ITNA 84GLA 07 1 Ti (ug/g)

Cone

Sr (ug/g)

Uncer Com Method Reference ^

Th (ug/g)

7.4 0.3 ITNA

U <ug/g)

79GRE 01

(ug/g) 3300

3800 200

ITNA EXRF84TU

81KIN

03

01 4 ICPES 80FLO 01 1 3900 800 AA 81FRA 01 20 6 ICPES 84JEN 02 1 4000 ICPES 80FLO 01 23.1 0.2 35 RTNA 81GLA 01 1 4000 200 ITNA 79GRE 01 24.22 0.25 RTNA 84DEL 01 1 4000 200 ITNA 84GLA 07

25 4 XRF 77GIA 02 1 4100 300 AA 84GLA 07

25 4 D XRF 79GIA 03 1 4100 400 AA 82GLA 02

26 ICPES 82NYG 01 1 4260 30 EXRF 78PEL 01 27 2 ITNA 79GRE 01 1 4500

9700

400 lENA

35 NAA

84GLA

81GLA

07

03

11.5 2 AA 82GLA 02 1 12.63 0.47 AA 81FRA 01 1 5.2 0.6 DNA 85GAU 04

13 1.1 lENA 84GLA 07 1 5.42 0.2 DNA 84GLA 07

13 2 AA 84GLA 07 1 5.6 0.05 lENA 84GLA 07

13.3 1.1 AA 83 FAR 01 1 5.9 DNA 84GLA 02

14.7 0.3 EXRF 78PEL 01 1 V (ug/g)

Sm (ug/q)

106 ICPES 80FLO 01

4 0.4 ITNA 79GRE 01 1 116 4 ITNA 84GLA 07

4.2 0.4 35 ITNA 81GLA 03 1 116 19 35 ITNA 81GLA 03

4.4 0.3 ITNA 84GLA 07 1 119 9 11 ICPES 84SCH 03

i.4 0.4 4 TCGS 85GLA 05 1 123 12 lENA 84GLA 07

4.8 0.4 4 TCGS 85GLA 05 1 127 ITNA 84TU 03

130 2 11 ICPES 84SCH 03

Sn (ug/q) 130 7 ITNA 79GRE 01 #

147 4 XRF 77GIA 02 1

1648-8
Cone

TABLE 16A8-2: COMPILED DATA

Uncer Com Method Reference

FOR NBS SRM 16A8 (cont.)

3.5 35 RENA 81GLA 03

4.4 2.8 lENA 84GLA 07

4.8 0.6 ITNA 79GRE 01

Y /iin/n\

c ADPi our LUn V 1

ID (ug/g;

c Ann n U 1

7n 1 1 tn i n\

nil A1O 1 FDA rKn U 1 HHWU ov Mil A1 PDA U 1 nn ft1 FAR niU 1 4650 11 AA R7YAM u^ 1 nn 01 4650 150 7RPFI 01 4670 35 ICPES 84JEN 02

4670 70 AA A'^RYR 01 4700 11 nnAA A7YAM 01U 1 4700 11 AA ijc 1 nn 01 4700 ICPES 80 FLO 01U i 4700 200 ITNA I 1 nn 01 4740 30 AA 80EPS 01 4740 130 lENA 84GLA 07

4750 11 AA 82YAM 01 4750 50 ITNA 84GLA 07

4760 70 11 ICPES 84SCH 03

H f OU 1 lU 1

ohSCH niU3

4800 AA 82GLA 02

4800 60 AA 81FRA 01 4800 100 EXRF 81KIN 01 4800 300 AA 84GLA 07

4850 240 35 ITNA 81GLA 03

4890 130 D XRF 79GIA 03

4890 130 XRF 77GIA 02

Zr (Uq/Q)

169 8 XRF 77GIA 02

1648-9
X) CO (/) (/) c/> (/) i/i i/i 5

-C 1 1 TT 3E

«-> u o o U o u

1 o o o O o1 CJ CJ CJ1 CJ o CJ CJ o

1 O o o

1 o o o

1 CJ CJ CJ CJ CJ1 u o CJ

0) —1 —1 —1 o o _l _l o u o u -J (3 _l o _l U _l —1 o C3 _i C3 o _J U C3 o _i —J

s:

(/> z c «

ro <\J (V ro 1rvi fO rvi f\J M fM fM ro ro fM ro fM fM (M fM ro < V LU

z: <M fM in (M in

fM o N.

Vi 8 o in o o O in O in CD o tc m o IE o o N. in o ro o 00 >o O ro ro in o <o 00 f\J o 1— •H o +1 +1 •H H +4 H H H H

LU \r\ rvj >d vt -4- fM ro ro to ro ro •4- >! in

IE c ro N- r>- O (D o in m O 0) >* • 2: (\i fM fO ro

ro f\J o o> o o ro o o o rvi m • 111 •O in J- r^ -* U

z

1

1 1

1

i

1

1 1 1

1

1 1

1

1

1

1 1 1

1

1 1 1

1

1

1

1 1

1

1 1

1

1

1

1 1

1

1 1

1

1

1

1

1

1

1 sr1 1 o o ot 1 (M

1 1 1 in1 o <o1 1 ro1 1 o1 1 in1 CO

1 1

(M <o (\j fVi 5 ro m in

<

(M ofM ro o

ro o o

</> QCO

C/5

OCJ c

(0

o

in

roo

rfM

fM ro <o W *^ o in o o

• -H -H ro >0 o

fM

vO

roo

fM

o

in

ro

ro

-O

fM o

c> oro

COo

in

(Mo

+) (M

in

OfM

O

te

COo

(M

m

o

fM

oCO

c

(0

0)

roo

M

o

fM

fM

in

ino

(M

ro

ro ro o5

m

o

ino oro

c>M

in

fM O f\J f\J fM fM o o> o O o in in in o O o fM ro ro ro

8:

co >* 00 00 00 1^ r^ ro 0> O. o> in in in CO CO

(/> in in in o fM fM fM fM fM fM O o o o o o ro ro ro in in in < O in in m in ro ro ro fM fM fM 00 CO CO r>~ :S ro ro ro 00 CO CO o o

o tM >o <5 >0 o o 5^ o o o o O o ro o o o o> 0> a- 0» in in

in in in fM fM in in m TfM fM rvj in fM rg fM «00 CO

o o o

o

o •*o o in

<\J »-

r- CM

3a.

0)c c

<t> c

c 0)

(U c c

u (0 <D >^ 0) V

(0 £- c c

L. o o V «> 3 3 c

1—

f

c c H- H-

<u to 1—

)

f—

1

u r—

1

> "(0 «>

to to 1—

1

1—

1

t- • • o o o o o

N N N

c c c c c c

c (1) o 0) < CD CO CO CQ CO CD

c

(A

cu

c

to 01 -• c f 0) - £ CO t-) '-' c

N (0 C I.o

3

a

c

%.a.

•au

I PO

f\j

o

c

«>

c

0)u

0) a.

0)c

011_

c

(0c

0)c

0)c

>.

a.

o>c

wc

0> ^.

1649-1
TABLE 1649-1: COMPILED DATA FOR NBS SRM 1649 URBAN DUST/ ORGANICS (cont.)

(revised 3/1/86)

ELEMENT UNITS NBS

Ag ug/g 3.5

As ug/g 67

Ba ug/g 570

Br ug/g 1190

Cd ug/g 18

Ce ug/g 51.6

CI ug/g 2820

Co ug/g 16.4

Cr ug/g 211

Cs ug/g 2.85

Eu ug/g 0.87

Fe % 3.00

Hf ug/g 4.41

ELEMENT UNITS NBS

La ug/g 33.3

Mo ug/g 14

Rb ug/g 47

S % 3.27

Sb ug/g 29.9

Sc ug/g 8.73

Se ug/g 25.6

Sm ug/g 4.71

Sn ug/g 56

Th ug/g 6.63

U ug/g 2.65

U ug/g 3.8

Zn ug/g 1670

1649-2 I
TABLE 1649-2: INDIVIDUAL DATA FOR NBS SRM 1649 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Anthracene Di benz [a. h] anthracene (ng/g)

500 GC-HS OHd 1 n 1 410 70 LC AXMA OHnMTV Ul

450 40 LC AAMAV OhFIAT niU 1 Benz [a] anthracene (ug/g)

2.4 0.1 44 LC 01 1

1 Fluoranthene (ug/g)

2.4 0.1 GC 01 1

1 2.7 0.1 44 LC 84MAY 01 1 6.8 0.4 44 LC 84MAY 01 2.8 0.2 44 LC 84MAY 01 1 7 GC-MS 84SIM 03

2.8 1.1 GC-MS 85GRE 01 1 7 0.5 44 LC aamay ni 3.3 GC-MS 7.1 0.5 44 LC OHMAT niU 1 7.3 0.2 GC OhMAT ni

Benzo[b] f luoranthene (ug/g) 7.3 2.7 GC-MS A<?f^DC ni

6 0.3 44 LC 1 Indeno[1 ,2,3-cdlDryene (ug/g)

6.2 0.3 44 LC U 1

1 3.3 0.3 GC 84MAY 01 BenzoCk] f luoranthene (ug/g) 3.4 GC-MS 84SIM 03

[ 3.4 0.1 44 LC 84MAY 01 2 0.1 44 LC 84MAY 01 1 3.4 0.4 44 LC 84MAY 01

2 0.1 44 LC 0**rlM 1 U 1 1 3.6 0.2 LL LL OHPIM 1 ni

2.1 0.1 44 LC AAMAY ni 1 4 9 GC-MS O^UKC ni

BenzoCghilpervlene (ug/g) Perylene (ng/g)

3.9 0.8 44 LC 84MAY 01 1 570 GC-MS 84SIM 03

4.1 0.1 44 LC 84MAY 01 1 650 20 i / LC 84MAY 01 4.4 GC-MS 84SIM 03 1 740 50 / / LC 84MAY 01 4.7 0.2 GC 84MAY 01 1 800 40 44 LC 84MAY 01

5 9 GC-MS ni 1

1 840 90 GC OHrlMT ni

5.2 0.6 44 LC RAMAY 900 100 GC-MS ni

Benzo [a] pyrene (ug/g) Phenanthrene (ug/g)

2.2 1.4 GC-MS 85GRE 01 1 4.5 0.3 44 LC 84MAY 01 2.4 0.2 44 LC 84MAY 01 1 4.7 0.1 44 LC 84MAY 01 2.6 0.1 44 LC 84HAY 01 1 4.8 GC-MS 84SIM 03

2.6 0.4 44 LC fll 1 4.9 1.3 GC-MS 01 2.8 GC-MS OHO 1 n n7 1

1 3 0.3 GC AAMAV U 1 1 Pyrene (ug/g)

Benzo [e] pyrene (ug/g) 5.8 GC-MS OHd i n 3.1 1.8 GC-MS 01 1 6 0.2 44 LC 84MAY 01 3.3 0.2 GC AAM&Y OHPIM 1 01 1

1 6 2.1 GC-MS 85fiRf 01 3.6 GC-MS AAC OHO IM1 PI 6.2 0.2 44 LC niU 1 3.9 0.3 LC OHPIn I ni 1 6.3 0.4 44 LC R4MAy 01

7.2 0.2 GC 84MAY 01 Chrysene (ug/g)

3.5 0.1 44 LC 84MAY 01 1 Triphenylene (ug/g)

3.5 0.1 44 LC 84MAY 01 1 3.7 0.2 44 LC 84MAY 01 1 1.7 0.1 LC 84MAY 01 3.8 1.1 GC-MS 85GRE 01 1 4.6 0.2 GC 84MAY 01 1

1649-3
TABLE 1818-1: COMPILED DATA FOR NBS SRM 1818 CHLORINE IN LUBRICATING BASE OIL (revised 3/1/87)

ELEMENT UNITS NBS

Mean ± SD

Cl-I ug/g 29 ± 5 Cl-II ug/g 63 ± 4

Cl-III ug/g 78 ± 4

Cl-IV ug/g 231 ± 6

Cl-V ug/g 558 ± 11

TABLE 1819-1: COMPILED DATA FOR NBS SRM 1819 SULFUR IN LUBRICATING BASE OIL (revised 3/1/87)

ELEMENT UNITS NBS

Mean ± SD

S-I ug/g 299 ± 8

S-II ug/g 1070 ± 40

S-I 1 1 ug/g 2865 ± 70

S-IV ug/g 6030 ± 130

S-V % 1.055 i 0.026

TABLE 1880-1: COMPILED DATA FOR NBS SRMs 1880-1883 CEMENTS (revised 3/1/87)

ELEMENT UNITS SRM

1880 1881 1882 1883

NBS NBS NBS NBS

Al % 2.66 2.22 20.4 37.7

B ug/g < 100 < 100 Ba ug/g < 100 < 100

Ca % 45.14 41.96 26.9 19.9

CI ug/g 200 < 100

Cr ug/g < 100 < 100

F ug/g 1000 900

Fe % 2.03 3.27 11.0 0.056

K ug/g 7600 9710 1000 80

LOI % 1.38 2.01 1.58 0.42

Mg % 1.62 1.58 0.75 0.17

Mn ug/g 560 1800

Na ug/g 2100 300 440 2400

P ug/g 1260 390

S % 1.35 1.46

Si % 9.26 10.39 1.59 0.16

Sr ug/g 510 930

Ti ug/g 1400 1400 11000 60

Zn ug/g 80 80

Zr ug/g < 100 < 100

I 1818-1
TABLE 2661-1: COMPILED DATA FOR NBS SRM 2661 BENZENE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean ± SO Mean (n)

I ug/tube H ± 1

II ug/tube 66 ± 3

III ug/tube 258 ± 13 IV ug/tube 994 i 30

TABLE 2661A-1: COMPILED DATA FOR NBS SRM 2661A BENZENE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

I ug/tube 16 ± 1

II ug/tube 30 ± 2 31 (1) GC

III ug/tube 54 ± 2 57.9 (1) GC

TABLE 2662-1: COMPILED DATA FOR NBS SRM 2662 M-XYLENE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

I ug/tube 40 ± 2

II ug/tube 293 ± 15

III mg/tube 1.79 ± 0.09

IV mg/tube 8.38 ± 0.38

TABLE 2663-1: COMPILED DATA FOR NBS SRM 2663 1,4-DIOXANE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

I ug/tube 16 ± 1

II ug/tube 112 ± 6

III mg/tube 0.996 ± 0,050 0.94 (1) GC

IV mg/tube 6.49 ± 0.20

2661-1
TABLE 2661A-2: INDIVIDUAL DATA FOR NBS SRH 2661A (revised 3/1/86)

Cone Uncer Com Method Reference

Benzene- II (ug/tube)

31 GC 86GAU 01

Benzene-Ill (ug/tube)

57.9 GC 85GAU 04

TABLE 2663-2: INDIVIDUAL DATA FOR NBS SRH 2663 (revised 3/1/86)

Cone Uncer Com Method Reference

1.4-Dioxane-III (tng/tube)

0.9A 0.07 GC 86GAU 01

2661-2
TABLE 2664-1: COMPILED DATA FOR NBS SRH 2664 ETHYLENE CHLORIDE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean t SD Mean (n)

I ug/tube 98 t 5 100 (1) GO

II ug/tube 381 ± 19

III mg/tube 1.56 ± 0.08 1.6 (1) GC

IV mg/tube 5.8 ± 0.17

TABLE 2665-1: COMPILED DATA FOR NBS SRM 2665 CHLOROFORM ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean i SD Mean (n)

I ug/tube 147 ± 7

II ug/tube 516 ±26 510 (1) GC

III mg/tube 2.14 ± 0.1 IV mg/tube 6.87 ± 0.21

TABLE 2666-1: COMPILED DATA FOR NBS SRM 2666 TRICHLOROETHYLENE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

I ug/tube 286 ± 14

II mg/tube 1.03 ± 0.05

III mg/tube 4.09 ± 0.20 5.3 (1) GC

IV mg/tube 15.4 ± 0.5

TABLE 2667-1: COMPILED DATA FOR NBS SRM 2667 CARBON TETRACHLORIDE ON CHARCOAL (revised 3/1/86)

LEVEL UNITS NBS CONSENSUS METHOD

Mean ± SD ' Mean (n)

I ug/tube 33 ± 3

II ug/tube 114 ± 6

III ug/tube 414 ±21 580 (1) GC

IV mg/tube 1.58 ± 0.05

2664-1
TABLE 2664-2: INDIVIDUAL DATA FOR NBS SRM 2664 (revised 3/1/86)

Cone Uncer Com Method Reference

Ethylene Chloride- I (ug/tube)

100 GC 86GAU 01

Ethylene Chloride- 11 1 (mg/tube)

1.6 GC 86GAU 01

TABLE 2665-2: INDIVIDUAL DATA FOR NBS SRM 2665 (revised 3/1/86)

Cone Uncer Com Method Reference

Chloroform-II (ug/tube)

510 GC 86GAU 01

TABLE 2666-2: INDIVIDUAL DATA FOR NBS SRM 2666 (revised 3/1/86)

Cone Uncer Com Method Reference

Triehloroethylene-III (mg/tube)

5.3 GC 86GAU 01

TABLE 2667-2: INDIVIDUAL DATA FOR NBS SRM 2667 (revised 3/1/86)

Cone Uncer Com Method Reference

Carbon tetrachloride- III (ug/tube)

580 GC 86GAU 01

2664-2
TABLE 2670-1: COMPILED DATA OM MBS SRM 2670 TRACE ELEMENTS IN URINE (revised 3/1/86)

SAMPLE

Entire pool

Normal

Elevated

ELEMENT UNITS NBS

Mean ± SD

CONSENSUS

Mean (n)

METHOD

n 1 mpthvl 1 f 1 He* ua/L 2.73 (1) GC

Dimethyl tin ug/L ... 1 .04 (1) GC

Butyl tin ug/L — 0.03 (1) GC

Ca mg/L 105 ± 5 —

CI g/L A.

4

—

K g/L 1.5 ...

Mg mg/L 63 ± 3

...

Na g/L 2,62 ± 0.14 —

S04 g/L 1.3 —

Al ug/L 180 —

As ug/L 15 62 (1) ICPES

Be ug/L < 0.5

Cd ua/L 0.4

Cr ug/L 13 10 (1) ICPES

Cu ug/L 130 ± 20 135 (1) ICPES

Hg ug/L 20 —

Mn ug/L 30 24 (1

)

ICPES

Ni ug/L 70 61 ( 1

)

ICPES

Pb ug/L 10 —

Pt ug/L < 10 —

Se ug/L 30 ± 8 5f (1

)

ICPES

Al ug/L 180 —

As ug/L 480 ± 100 504 (1) ICPES

Be ug/L 33 —

Cd ug/L 88 ± 3 85 (1) ICPES

Cr ug/L 85 ± 6 75 (1) ICPES

Cu ug/L 370 ± 30 359 (1) ICPES

Hg ug/L 105 ± 8

Hn ug/L 330 310 (1) ICPES

Ni ug/L 300 257 (1) ICPES

Pb ug/L 109 ± 4 94 (1) ICPES

Pt ug/L 110

Se ug/L 460 ± 30 475 (1) ICPES

2670-1
TABLE 2670-2: INDIVIDUAL DATA FOR NBS SRM 2670 Entire Pool (revised 3/1/86)

Cotk: Uncer Com Method Reference

(He)2S2 (ug/L)

2.73 GC 830LS 02

(Me)2Sn (ug/L)

1.04 GC 830LS 02

BuSn (ug/L)

0.03 GC 830LS 02

TABLE 2670N-2: INDIVIDUAL DATA FOR NBS SRM 2670 Normal Level (revised 3/1/86)

Cone Uncer Com Method Reference

36

As (ug/L)

62

Cr (ug/L)

10

Cu (ug/L)

135 12

ICPES 85KIM 01

3.3 ICPES 85KIM 01

ICPES 85KIM 01

Cone Uncer Com Method Reference

Hn (ug/L)

24

Mi (ug/L)

61

Se (ug/L)

37 31

2.8 ICPES 85KIM 01

13 ICPES 85KIM 01

ICPES 85KIM 01

TABLE 2670E-2: INDIVIDUAL DATA FOR NBS SRM 2670 Elevated Level (revised 3/1/86)

Cone Uncer Com Method Reference

As (ug/L)

504

Cd (ug/L>

85

Cr (ug/L)

75

^ Cu (ug/L)

63 ICPES 85KIM 01

3.8 ICPES 85KIM 01

3.2 ICPES 85ICIM 01

359 12 ICPES 85KIM 01

Cone Uncer Com Method Reference

Mn (ug/L)

310 6

Ni (ug/L)

257 25

Pb (ug/L)

94 20

Se (ug/L)

475 36

ICPES 85KIM 01

ICPES 85KIM 01

ICPES 85KIM 01

ICPES 85KIM 01

2670-2
TABLE 2671-1: COMPILED DATA ON NBS SRM 2671 FLUORIDE IN URINE (revised 3/1/86)

SAMPLE ELEMENT UNITS NBS

Mean ± SD

Normal

Elevated F

mg/L 0.835 ± 0,082

mg/L 7.14 ± 0.48

TABLE 2672-1: COMPILED DATA ON NBS SRM 2672 MERCURY IN URINE (revised 3/1/86)

SAMPLE

Entire pool

Normal

Elevated

ELEMENT UNITS

Butyltin ug/L

Methyl tin ug/L

Sn ug/L

Hg

Hg

ug/L

ug/L

NBS

Mean ± SD

49.8 ± 4.2

294 £ 24

CONSENSUS

Mean (n)

1.5 (1)

1.0 (1)

28.1 (1)

METHOD

GC

GC

GC

TABLE 2762-2: INDIVIDUAL DATA FOR NBS SRM 2672 Entire Pool (revised 3/1/86)

Cone

BuSn (ug/L)

1.5

MeSn (ug/L)

1

Sn (ug/L)

Uncer Com Method Reference

GC

GC

830LS 02

830LS 02

28.1 GC 830LS 02

2671-1
TABLE 2674-1: COMPILED DATA FOR NBS SRM 2674 LEAD ON FILTER MEDIA (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

Pb-Blank ug/f 1.4 ± 0»7

Pb-I ug/f 100 ± 3

Pb-II ug/f 303 ± 9

Pb-I II mg/f 1.505 ± 0.028

TABLE 2675-1: COMPILED DATA FOR NBS SRM 2675 BERYLLIUM ON FILTER MEDIA (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

Be-I ng/f 52 ± 7 Be-II ug/f 0.25 ± 0.03 0.35 (1) AA

Be-III ug/f 1.0 ± 0.1

TABLE 2675-2: INDIVIDUAL DATA FOR NBS SRM 2675 (revised 3/1/86)

Cone Uncer Com Method Reference

Be-II ( ug/f i Iter)

0.35 AA 85GAU 04

TABLE 2676-1: COMPILED DATA FOR NBS SRM 2676 METALS ON FILTER MEDIA (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

Cd-I ng/f 500 ± 40

Cd-II ug/f 2.48 ± 0.14

Cd-I II ug/f 10.1 ± 0.4

Mn-I ug/f 1.93 ± 0.29

Mn-II ug/f 10.3 ± 1.5 Mn-I 1

1

ug/f 20.6 ± 1.0

Pb-I ug/f 6.8 ± 1.1

Pb-II ug/f 29 ± 2.6

Pb-I 1

1

ug/f 102 ± 6

Zn-I ug/f 1.02 ± 0.06

Zn-II ug/f 5.1 ± 0.26

Zn-I 1

1

ug/f 10.1 ± 1.1

2674-1
TABLE 2676A-1: COMPILED DATA FOR NBS SRM 2676A METALS ON FILTER MEDIA (revised 3/1/86)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean t SD Mean (n)

Cd-Blanlc ug/f 0.03 ^ 4 X (1) AA

Cd-I ug/f 1.02 t 0.03

Cd-II ug/f 2.5 ± 0.02 2.47 (1) AA

Cd-III ug/f 10.18 t 0.10 9.8 (1) AA

Mn-I ug/f 1.97 ± 0.06

Mn-II ug/f 9.89 ± 0.1 Mn- 1 1

1

ug/f 19.7 1 0.3

Pb- Blank ug/f 0.17 (1) AA

Pb-I u9/f 6.96 t 0.2

Pb-II ug/f 15.23 ± 0.15 15.6 (1) AA

Pb-Ill ug/f 29.64 ± 0.2 28.7 (1) AA

Zn- Blank ug/f 8.1 (1) AA

Zn-I ug/f 9.86 ± 0.28

Zn-II ug/f 49.52 1 0.48 47.6 (1) AA

Zn- 1 1

1

ug/f 99.22 ± 0.99 95 (1) AA

TABLE 2676A-2: INDIVIDUAL DATA FOR NBS SRM 2676A (revised 3/1/86)

Cone Uncer Com Method Reference

Cd- blank ( ug/f i Iter)

0.03

Cd-II ( ug/f i Iter)

2.47

Cd-III (ug/f i Iter)

9.8

Pb-blank (ug/f i Iter)

0.17

Pty-II (ug/filter)

15.6

AA 85GAU 04

AA 85GAU 04

AA 85GAU 04

AA 85GAU 04

AA 85GAU 04

Cone Uncer Com Method Reference

Pb-I 1 1 (ug/filter)

28.7

Zn-blank (ug/filter)

8.1

Zn-II (ug/filter)

47.6

Zn-I 1 1 (ug/filter)

95

AA 85GAU 04

AA 85GAU 04

AA 85GAU 04

AA 85GAU 04

2676A-1
TABLE 2676B-1: COMPILED DATA FOR NBS SRM 2676B HETALS ON FILTER MEDIA (revised 3/1/86)

cLtntN

1

1 lU f TC UNI 1 a UDC

nean z dU

r*/4. D 1 anl^ Lu'D lanK Hit /4 ug/T

f*j4~ f Uu" 1 ug/t u.yy n oo 4. n n? ± u.uc

CA- T T Lu 1

1

ug/T 5 AO * n nA

La" 111 ug/T lU.lH ± U.l£ nn D lariK 1 in ug/T ^ U.U 1 Un. Hn f

1 ug/T 11 • ftA oo X

« n nx u • u

J

nn 1

1

ug/T oy*HA1 « n I't 1 X u« 10

ftlm- TIT Hn" 111 ug/T

ug/f ^ U • U*f PD- 1 ug/t ± U.1

Pb-II ug/f U.9 t 0.2

Pb-III ug/f 30.4 t 0.4

Zn- Blank ug/f 0.4 ± 0.1

Zn-I ug/f 10.01 ± 0.14

Zn-II ug/f 49.7 ± 0.7

Zn-III ug/f 99.5 ± 1.2

TABLE 2677-1: COMPILED DATA FOR NBS SRM 2677 BERYLLIUM AND ARSENIC ON FILTER MEDIA (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

As-Blank ng/f < 2

As1ng/f 103 ± 5 As- 1

1

ug/f 1.07 ± 0.05

As-III ug/f 10.5 ± 0.5

Be-Blank ng/f < 1 Be1

ng/f 52 1 3

Be- 1

1

ng/f 256 i 13

Be-III ug/f 1.03 ± 0.05

TABLE 2679-1: COMPILED DATA FOR NBS SRM 2679 QUARTZ ON FILTER MEDIA (revised 3/1/86)

MATERIAL UNITS NBS

Mean i SD

Clay-A ug/f 400

Clay-B ug/f 370

Clay-C ug/f 320

Clay-D ug/f 200

Quartz-A ug/f 3.8 t 0.5

Quartz-B ug/f 29.9 ± 3.6

Quartz-C ug/f 76.1 * 9.1

Quartz-D ug/f 193.2 ± 23.2

2676B-1
TABLE 2682-1: COMPILED DATA FOR NBS SRH 2682 SULFUR IN COAL (revised 3/1/86)

PI FMPMT UN i 1 d Moan * Cn ncaii z Ok/

A A 17 4 n 1A

Ag ng/g ^ mnn

A 1 Al ug/g HOUU H^yu ± tvu /*7\ (o)

AS ug/g 1

1 U . Or z u . 1

AUAl 1 ng/g ^ O

DD ug/g 70 f 1 ^

Da ug/g JO 1 Rror 1 in In us/g •J • f ^ s + n

r\0 7^ r 9 ri ^ X 1 1

1 1 CI >

V 1 /

1ug/g in /n in1 u 0 R7

r 1 ug/g T7 K 1 / ug/g 1 7 11 > Rn^u It J LP ug/g 1 J It J PoLS ng/g * 1 nn

Dy ug/g n A rl ^

Pi I ng/g i7n 1 jo

r e ug/

g

7Ann CbOU ??An

ua ug/g < A

Un X ^ 7 U 7 f 1 ^ V 1 / X 1 O

htii/ 1 h 11 Ann ?A0

n T ng/

g

Ann SAS

ug/g 1

1 nnuu 117 f^^\

La 1ug/g m / n AH ^H 4-Z nU • AO

1 II ng/g < "^n Mn ug/g pnnn £UUU

Mnpii 1

1ug/in /ay 26 22.2 (2'i Mn 1ug/g in /n

y n nu • Ao nu • Ao K 1 J Na ug/g 11 nnn uuu AOR Ot3

KU ug/g ^ Cm cd ug/g A7nn H f UU +Z xnn ^UU A7nn HrUU Z+ iAn lOU ed ug/g

c ug/g

rdt 1cc AOOoyy

O JJ/ OH rdt 1

nu 17A'^ . 1 r oJ ng/g ion 1 TU 1A0 loy ri ^

ug/

g

11 ^J 1 HIAl

Ca ug/g nu oiy 1 nu oiy 1 /i ^

Olll nnng/g/n 7Rn 7nA

Ta1 d nnng/gin

Th1 1^ nnng/g/n < 100

Th1 1

1ug/in in

g

1 L"^

1 1 ug/g V 1

U ng/g 520 490 ± 35 (3)

V ug/g 15 13.45 (2) u ug/g 1.8 1.46 (2)

Yb ng/g < 300

Zn ug/g 8.6 8.6 (1) Zr ug/g < 100

MEDIAN RANGE METHOD MEANS

Mean i SD (n) Method

< 1000

4140 4100 4620 4290 ± 290 (3) NAA

0.96 0.7 -1 0.89 ± 0.16 (3) NAA

< O

70 \ 1 / TPPC

TA? 7A1 klA NAAA

J .OH 'K 1 O f f 7 ^ « n '7 \Ji klA NnAA

... 76 (1) TCGS

1 n'? ^ 1 "» yANAMA ... ... 9.87 (1) NAA

T7 ^ 1 ^ NAM

1 "K"^ 1 AA 1 sn \C.t MAA NnA

1 J

...

I"; p UAA NAA

... 0.6 (1) NAA

IAn 17? 1S6 1 JO t'>\ \C} MAA

^?inn 1 uu cMCyj tcOU ??An klAA NAA

< 6

...

... 4.7 —

(1) TCGS

Ann S6S JOJ \C} UAA

1 17 UAA

L "iO 'K "iA 17 AH AH X+ nU a AO UAA

^ JU

7^ A >oA tt . t I7\ MAA

n A \ 1 1 1 Uuo

Ain o 1 u OA1 TO 1 AOA oyo NAM UAA

AA7n HOf U AA7n HH f U Hynu AAon + 1 1

HOTU X 1 1

PR AOAn / 1 ^ inMC

AA7n ^ 1 ^ 1 laild tc . AOO oyy / 1 \

n 17A'? \ 1 1

11 AOoy \ 1 1 UAA Nnn

1 7 1 *>PA 11 . AlH 1 UAA nnn

0.91 # 4 X (1) NAA

633 776 704 (2) NAA

< 400

< 100

1.33 1.532 1.43 (2) NAA

540 (1) NAA

500 448 519 490 ± 35 (3) NAA

13 13.9 13.45 (2) NAA

1.1 1.81 1.46 (2) NAA

< 300

8.6 (1) NAA

< 100

2682-1
TABLE 2682-2: INDIVIDUAL DATA FOR NBS SRM 2682 (revised 3/1/86)

Cone

Ag (ng/g)

Uncer Com Method Reference

< 1000

Al (ug/g)

As (ug/g)

B (ug/g)

39

340

382

C (%)

76

Ca (%)

1.03

Ce (ug/g)

9.87

Ct (ug/g)

37

1.3

20

5

3.8

0.1

0,08

40

4

ITNA 86GLA 01

4100 200 ITNA 86GLA 01 1 4140 120 ITNA 85GAU 04 1 15 0.8 ITNA 86GLA 01 4620 20 ITNA 83LIN 02 1 15.4 0.3 ITNA 83LIN 02

TCGS

ITNA

ITNA

83LIN 02

86GLA 01 83LIN 02

TCGS

ITNA

ITNA

ITNA

ITNA

83LIN 02

86GLA 01

83LIN 02

86GLA 01 85GAU 04

0.7 0.3 ITNA 86GLA 01 1 0.6 0.2 ITNA 86GLA 01 0.96 0.06 ITNA 85GAU 04 1

1 0.02 ITNA 83LIN 02 1 Eu (ng/g)

(ng/g) 140 40 ITNA 86GLA 01 172 5 ITNA 83LIN 02

< 6 ITNA 86GLA 01 1

3.1 0.3 ITNA 86GLA 01 1 3.64 0.19 ITNA 85GAU 04 1 Hf (ng/g)

3.74 0.18 ITNA 83LIN 02 i

Cone

Co (ug/g)

1.33

1.66

Cr (ug/g)

Uncer Com Method Reference

0.15

0.03

Fe (ug/g)

2100

2420

Ga (ug/g)

H (%)

200

30

4.7

530

600

K (ug/g)

117

La (ug/g)

3.56

4.59

5.17

Lu (ng/g)

0.13

40

20

700

14

0.13

0.14

0.03

30

ITNA

ITNA

ITNA ITNA

ITNA

TCGS

ITNA ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

86GLA 01 83LIN 02

86GLA 01 83LIN 02

86GLA 01

83LIN 02

86GLA 01 83LIN 02

86GLA 01 83LIN 02

86GLA 01 85GAU 04

83LIN 02

86GLA 01

2682-2
TABLE 2682-2: INDIVIDUAL DATA FOR NBS SRM 2682 (cont.)

Cone

Mn (ug/g)

21.8

22.6

Mo (ug/g)

0.8

Na (ug/g)

810

981

S (ug/g)

4470

4600

4670

4810

4940

Uncer Cora Method Reference

0.1

0.8

0.3

30

12

130

200

60

50

110

S-32/34 (ratio)

22.699

S-33/34 (ratio)

0.1783

Sb (ng/g)

<

189

Sc (ug/g)

150

9

1.3

1.524

Se (ug/g)

0.91

Sm (ng/g)

633

776

0.1

0.005

10.1

16

4

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

86GLA 01 85GAU 04

ITNA 86GLA 01

TCGS 83LIN 02

IDMS 84KEL 01

IDMS 84KEL 01

86GLA 01 83LIN 02

86GLA 01 83LIN 02

86GLA 01 83LIN 02

ITNA 85GAU 04 ITNA 83LIN 02

ITNA 86GLA 01 1 540 200 ITNA 86GLA

ITNA 85GAU 04 1 U (ng/g)

448 23 DNA 86GLA

TCGS 83LIN 02 1 500 DNA 86GAU

CB 84GLA 11 1 519 15 ITNA 83LIN

CB 86GAU 01 1 CB 85GLA 03 1 V (ug/g)

IDMS 84KEL 01 1

Cone

Ta (ng/g)

Uncer Com Method Reference

< 400

Tb (ng/g)

< 100

Th (ug/g)

1.33

1.532

Ti (ug/g)

0.06

0.014

13

13.9

W (ug/g)

1.1

1.81

Yb (ng/g)

10.7

0.3

0.03

< 300

Zn (ug/g)

8.6

Zr (ug/g)

10

0.9

< 100

ITNA

ITNA

ITNA ITNA

ITNA ITNA

ITNA

ITNA

ITNA 86GLA 01

ITNA 86GLA 01

86GLA 01 83LIN 02

86GLA 01 85GAU 04

86GLA 01 83LIN 02

ITNA 86GLA 01

86GLA 01 83LIN 02

ITNA 86GLA 01

2682-3
TABLE 2683-1: COMPILED DATA FOR NBS SRM 2683 SULFUR IN COAL (revised 3/1/86)

ELEHENl UNITS NBS nean x ou Uaom nean ^ CR x ou

ASH VA O.OJ 1 U.U£

Ag ng/g ^< onn yuu

ug/g oouu ftcon ojyu f'>\

AS ug/g O.O

AU ng/g

D ug/g Or or r 1 ^

Dtt DO ug/g 71r 1 71r 1 or ug/g 1 f 171 r .JT VA TOIT 70f y K 1 ) ca ug/g <^ 5nnn cUUU

ug/g 0y 0y. 1Alo \ 1 /

CI ug/g 1 mn / 1 \

CO ug/g

cr ug/g 1 1 11 1

cs ug/g U.H n / /. CD

Dy ng/g < f UU

cU ng/g loU 17ft 1 r o

re ug/g r ouu 77An r rOU

Caua ug/g

u

n A

c

J R n \ I /

ULU/ Kfii/II h

U

FIT ng/g Ano Huy

ug/g Ann ouu 7^n \i) La ug/g J.I H.O L A \C)

LU ng/g - AnOU / 1 ^ Mang ug/g son Mnnn ug/g 11 ft

1 1 .o / 1 ^

no ug/g

IIN V 1 A 11 .oA V 1 ) Ua ug/g snn JUU inn jUU \ 1 ) QhKw ug/g c »

c %A 1 AS 4' n DA 1 fto + n ns

s X

c

1 a L 1 u ?? 7AA f^\ 1

1

) S-3'?/3d nu . 17A0 1 r oy ^ 1 ^

ng/g ?fln KC.) ug/g 1 o 1

1 .voOA \,C)

ug/g 1 5 /7\

ug/g U.oO nU.oORA

Ta ng/g < jUU

Tb nnng/g/n ^< 7nn jUU

Th1 II 1ug/g in /n 1 A1 yc.)

1

1

1ug/g in /n Ann •uu AAn hhU ^ 1 ^ U ng/g 443 lit

±

M 22m (3)

V ug/g 14 15.7 (1) u ng/g A80 480 (1)

Yb ng/g 370 (1)

Zn ug/g 9.5 9.5 (1)

Zr ug/g < 90

MEDIAN RANGE METHOD MEANS

Mean ± SD (n) Method ——

-

- —

< 900 NAA — 8580 - 8600 8590 (2) NAA — 3.64 - 4 3.82 (2) NAA — - < 5 NAA — • - 67 (1) TCGS — - 71 (1) NAA — 16.85 - 17.8 17.3 (2) NAA — - 79 (1) TCGS — - < 2000 NAA — - 9.18 (1) NAA — - 1100 (1) NAA

2.22 2.26 2.24 (2) NAA — 11.02 - 11.5 11.26 (2) NAA

0.44 (1) NAA — - < 700 NAA — 177 - 180 178.5 (2) NAA

--- 7620 - 7900 7760 (2) NAA

< 5 NAA

... — -

5.0 —

(1) TCGS —

... 400

-

- 418 —

409 (2) NAA

750 (1) NAA

... 4.2 5.05 4.62 (2) NAA —

...

- 60 (1) NAA

...

-

- —

11.8 (1) NAA

... - < 3 NAA

... - 1.6 (1) TCGS

... - 500 (1) NAA

...

1.90 1.82

-

- 1.95

...

1.91 ± 0.04 (3) CB

... - 1.90 (1) IDMS

... - 1.82 (1) TCGS

... - 22.364 (1) IDMS

... - 0.1769 (1) IDMS — 220 - 279 250 (2) NAA — 1.94 - 1.99 1.97 (2) NAA — 1.2 - 1.23 1.22 (2) NAA — - 0.86 (1) NAA

... - < 300 NAA

... < 300 NAA

1.36 1.45 1.41 (2) NAA

440 (1) NAA

450 418 460 443 ± 22 (3) NAA 15.7 (1) NAA 480 (1) NAA

370 (1) NAA

9.5 (1) NAA

< 90 NAA

2683-1
TABLE 2683-2: INDIVIDUAL DATA FOR NBS SRH 2683 (revised 3/1/86)

Cone

Ag (ng/g)

Uncer Com Hethod Reference

< 900

Al (ug/g)

8580

8600

As (ug/g)

3.64

4

Au (ng/g)

B (ug/g)

67

Ba (ug/g)

71

Br (ug/g)

16.85

17.8

C (%)

79

Ca (ug/g)

50

200

0.13

0.1

60

3

0.04

0.6

< 2000

Ce (ug/g)

9.18

CI (ug/g)

1100

Co (ug/g)

2.22

2.26

0.08

100

0.09

0.04

ITNA 86GLA 01

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

83LIN 02

86GLA 01

83LIN 02

86GLA 01

ITNA 86GLA 01

TCGS 83LIN 02

86GLA 01 83LIN 02

83LIN 02

86GLA 01

TCGS 83LIN 02

ITNA 86GLA 01

ITNA 83LIN 02

ITNA 86GLA 01

83LIN 02

86GLA 01

Cone

Cr <ug/g?

11.02

11.5

Cs (ug/g)

0.44

Uncer Com Method Reference

Dy (ng/g)

Eu (ng/g)

177

180

Fe (ug/g)

7620

7900

Ga (ug/g)

H (%)

Hf (ng/g)

400

418

K (ug/g)

750

La (ug/g)

4.2

5.05

Lu (ng/g)

60

Mn (ug/g)

11.8

0.18

0.4

0.02

< 700

6

12

190

200

0.1

70

4

450

10

0.2

0.04

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

83LIN 02

86GLA 01

ITNA 83LIN 02

ITNA 86GLA 01

83LIN 02

86GLA 01

83LIN 02

86GLA 01

ITNA 86GLA 01

TCGS 83LIN 02

86GLA 01

83LIN 02

86GLA 01 83LIN 02

86GLA 01 83LIN 02

0.2

ITNA 86GLA 01

ITNA 86GLA 01

2683-2
TABLE 2683-2: INDIVIDUAL DATA FOR NBS SRM 2683 (cont.)

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Mo (ug/g) j Sm (ug/g)

< 3 ITNA 86GLA 01 1 0.859 0.005 ITNA 83LIN 02

N (%) Ta (ng/g)

1.6 0.9 TCGS

1 83LIN 02 1 < 300 ITNA 86GLA 01

Na (ug/g)

1

1

1

Tb (ng/g)

500 30 ITNA 86GLA 01 1 < 300 ITNA 86GLA 01

S (%)

1

1 Th (ug/Q)

1.82 0.05 TCGS

1 83LIN 02 1 1.363 0.011 ITNA 83LIN 02

1.87 0.03 CB 84GLA 11 1 1.45 0.06 ITNA 86GLA 01 1.896 0.037 IDMS 84KEL 01 1 1.91 0.03 CB 86GAU 01 1 Ti (ug/g)

1,95 0.04 CB 85GLA 03 1

1 440 90 ITNA 86GLA 01 S-32/34 (ratio) 1

1 U (ng/g)

22.364 IDMS 84KEL 01 1 418 11 ITNA 83LIM 02

S-33/34 (ratio) 1 450 DNA 86GAU 01

1 460 40 DNA 86GLA 01 0.1769 IDMS 84KEL 01 1 V (ug/g)

Sb (ng/g)

15.7 0.9 ITMA 86GLA 01 220 20 ITNA 86GLA 01 1 279 8 ITNA 83LIN 02 1 W (ng/g)

Sc (Ufl/g)

1

1 < 600 ITNA 86GLA 01 480 30 ITNA 83LIM 02

1.941 0.008 ITNA 83LIN 02 1 1.99 0.06 ITNA 86GLA 01 1 Yb <ng/g>

Se (ug/g) 370 60 ITNA 86GLA 01

1.2 0.2 ITNA 86GLA 01 1 Zn (ug/g)

1.23 0.09 ITNA 83LIN 02 1 < 10 ITNA 86GLA 01 9.5 0.6 ITNA 83LIN 02

Zr (ug/g)

< 90 ITNA 86GLA 01

2683-3
TABLE 2684-1: COMPILED DATA FOR NBS SRM 2684 SULFUR IN COAL (revised 3/1/86)

ELEMENT UNITS NBS

Mean ± SD

CONSENSUS

Mean ± SD (n)

ASH % 11.09 ± 0.18 —

Ag ng/g — < 1200

Al % 1.1 1.10 (2)

As ug/g 3.9 3.92 (2)

Au ng/g — < 5 B ug/g 114 114 (1)

Ba ug/g 41 41.4 (1) Br ug/g 11 10.4 (2)

C % 68 68 (1)

Ca ug/g 4400 4800 (1)

Ce ug/g 12 11.5 (1)

CI ug/g 1050 (1)

Co ug/g 3.9 3.72 (2)

Cr ug/g 17 16.6 (2)

Cs ug/g 1.2 1.15 (1)

Dy ug/g — 0.96 (1)

Eu ng/g 230 226 (2) Fe % 1.5 0.96 (2)

Ga ug/g — < 5

H % 4.8 4.8 (1)

H20- % 3.6 —

HEAT btu/lb 12760 ± 200 —

Hf ng/g 570 568 (2) K ug/g 2000 1850 (2) La ug/g 6.7 5.98 (2)

Lu ng/g — 74 (1)

Mg ug/g 800

Nn ug/g 36 32 (1)

Mo ug/g — < 4

N % 1.6 1.6 (1)

Na ug/g 300 240 (1)

Rb ug/g 15 14.6 (1)

S % 3.00 ± 0.13 2.99 ± 0.06 (4)

S X — —

S % ... —

S-32/34 ratio — 22.726 (1)

S- 33/34 ratio — 0.1782 (1)

Sb ng/g 350 372 (2)

Sc ug/g 2.7 2.64 <2)

Se ug/g 1.9 1.82 (2)

Sm ug/g 1.1 1.11 (1)

Ta ng/g — < 300

Tb ng/g — < 200

Th ug/g 2 1.98 (2)

Ti ug/g 600 580 (1)

U ug/g 0.9 0.88 ± 0.02 (3)

V ug/g 22 22 (1)

W ng/g 560 562 (1)

Yb ng/g 510 (1)

Zn ug/g 110 110 (2) Zr ug/g < 120

MEDIAN RANGE METHOD MEANS

Mean ± SD (n) Method

< 1200

1.10 - 1.103 1.10 (2) NAA

3.87 - 3.96 3.92 (2) NAA

- < 5 NAA - 114 (1) TCGS

- 41.4 (1) NAA

10.2 - 10.6 10.4 (2) NAA

- 68 (1) TCGS

4800 (1) NAA

- 11.5 (1) NAA

1050 (1) NAA

3.6 - 3.85 3.72 (2) NAA

16.4 - 16.8 16.6 (2) NAA

- 1.15 (1) NAA

0.96 (1) NAA

226 _ 226 226 (2) NAA

0.45 - 1.46 0.96 (2) NAA

- < 5 NAA

-

-

4.8 —

(1) TCGS

565

-

- 570 —

568 (2) NAA

1730 - 1969 1850 (2) NAA

5.3 - 6.65 5.98 (2) NAA

- 74 (1) NAA

-

-

...

32 (1) NAA

- < 4 NAA

- 1.6 (1) TCGS

- 240 (1) NAA

- 14.6 (1) NAA

2.94 - 3.08 2.94 (1) TCGS

- 2.96 (2) CB

- 3.08 (1) IDMS

- 22.726 (1) IDMS

• 0.1782 (1) IDMS

354 - 390 372 (2) NAA

2.62 - 2.66 2.64 (2) NAA

1.77 1.87 1.82 (2) NAA

1.11 (1) NAA

< 300 NAA

< 200 NAA

1.96 2.00 1.98 (2) NAA

580 (1) NAA

0.87 0.90 0.88 ± 0.02 (3) NAA

22 (1) NAA

562 (1) NAA

510 (1) NAA

110 110 110 (2) NAA

< 120 NAA

2684-1
TABLE 2684-2: INDIVIDUAL DATA FOR NBS SRH 2684 (revised 3/1/86)

Cone

(ng/g)

Uncer Com Method Reference

< 1200

At (X)

1.1

1.103

As (ug/g)

3.87

3.96

Au (ng/g)

<

114

Ba (ug/g)

41.4

Br (ug/g)

10.2

10.6

C (%)

68

4800

Ce (ug/q)

11.5

CI (ug/g)

1050

Co (ug/g)

3.6

3.85

0.04

0.006

0.14

0.14

80

2.6

0.2

0.5

400

0.2

100

0.2

0.05

ITNA 86GLA 01

ITNA

ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

86GLA 01 83LIN 02

83LIN 02

86GLA 01

ITNA 86GLA 01

TCGS 83LIN 02

86GLA 01 83LIN 02

86GLA 01 83LIN 02

TCGS 83LIN 02

ITNA 86GLA 01

ITNA 83LIN 02

ITNA 86GLA 01

86GLA 01 83LIN 02

Cone

Cr (ug/g)

16.4

16.8

Cs (ug/g)

1.15

Pv (ug/g)

0.96

Uncer Com Method Reference

Eu (ng/g)

226

226

Fe (%)

0.454

1.46

Ga (ug/g)

H (X)

4.8

Hf (ng/g)

565

570

< (ug/g)

1730

1969

La (ug/g)

5.3

6.65

Lu (ng/g)

74

Mn (ug/g)

32

0.9

0.3

0.05

0.06

9

20

0.026

0.04

0.1

12

7

140

16

0.13

0.1

ITNA

ITNA

ITNA ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

86GLA 01 83LIN 02

ITNA 83LIN 02

ITNA 86GLA 01

83LIN 02

86GLA 01

83LIN 02

86GLA 01

ITNA 86GLA 01

TCGS 83LIN 02

83LIN 02

86GLA 01

86GLA 01 83LIN 02

86GLA 01 83LIN 02

0.2

ITNA 86GLA 01

ITNA 86GLA 01

2684-2
TARI 1 nDL.CP 7fJ<A C\i%J^ IMDIVIDIIAI DATA FOR MR^ ^DM 7fiIUt. \ \*\n 1 L . /

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Mo (uq/g)

1

1

Tb (ng/g)

< 4 ITNA 86GLA 01 1 < 200 ITNA 86GLA 01

N (%) Th (ug/g)

1.6 0.4 TCGS

1 83LIN 02 1 1.955 0.016 ITNA 83LIN 02

1 2 0.08 ITNA 86GLA 01 Na (ug/g)

1 Ti (ug/g)

240 20 ITNA 86GLA 01 1

1 580 60 ITNA 86GLA 01 Rb (ug/g) 1

1 U (ug/g)

14.6 1.1 ITNA 83LIN 02 1 0.87 0.02 DNA 86GLA 01

S (%) 0,88 DNA 86GAU 01

1 0.901 0.01 ITNA 83LIN 02

2.94 0,07 TCGS 83LIN 02 1 2.95 0.03 CB 86GAU 01 1 V (ug/g)

2.98 0.08 CB 85GLA 03 1 3.076 0.09 IDMS 84KEL 01 1 22 4 ITNA 86GLA 01

S-32/34 (ratio) W (ng/g)

22.726 IDMS

1 84KEL 01 1 < 700 ITNA 86GLA 01

1 562 22 ITNA 83LIN 02

S-33/34 (ratio) 1

1 Yb (ng/g)

0.1782 IDMS 84KEL 01 1

1 510 50 ITNA 86GLA 01 Sb (nq/g) 1

Zn (ug/g)

354 8 ITNA 83LIN 02 1 390 50 ITNA 86GLA 01 1 110 11 ITNA 86GLA 01

1 110 12 ITNA 83LIN 02

Sc (uq/q) 1 Zr (uq/q)

2.62 0.1 ITNA 86GLA 01 1 2.665 0.02 ITNA 83LIN 02 1 < 120 ITNA 86GLA 01

Se (uq/q) 1

1,77 0.13 ITNA 86GLA 01 1 1,87 0.16 ITNA 83LIN 02 1

Sm (ug/g)

1 1.109 0.012 ITNA 83LIN 02 1

Ta (ng/g)

< 300 ITNA 86GLA 01 1

2684-3
TABLE 2685-1: COMPILED DATA FOR NBS SRH 2685 SULFUR IN COAL (revised 3/1/86)

CI CUCbll cLcMENT 1 lU T TC UN 1 1 o Mean ± ou nean x bu

ASH % i6-D3 ± U.lD

Ag ng/g < IDuO

Al % 1 .7 1 .66 (2)

As ug/g 1 0 A / O \ (2)

Au ng/g A

B ug/g 1 uy 1 no luy / 1 \ (1) Ba ug/g 1

! U3 1 rt^ / 1 \

Br ug/g 3 .O JmO't

L X OO AA IWV 1

La ug/g 30UU (

}

Ce ug/g 1 Q 17 o 1 f .y / 1 \

CI ug/g i*on / 1 \

CO ug/g H .O /. ^fl H . JO /0\ (a;

Cr ug/g OO / / o \ (a)

Cs ug/g 1 .J 1 71 1.31 / 1 \ (1

)

Dy ug/g 1 7C / 1 \ CD

CU ng/g *7An 1/ L /o> (a) re %

O / C /0\ (a) ua ug/g ^ 7

H wA

/. A /. A / 1 \

ntU" 1 .O

UC AT DIU/ ID i5inn * iRn

MT ug/g n oi n OT \^) K ug/g oAnr» ^ouu 0/. oi CMC. 1 /o\ (A)

La ug/g in o /. /0^ ia;

1 1

Lu ng/g 1

1 1AIO ^ 1 ^

C 1 J ug/g mnn

tin ug/g H 1 JO /In

no ug/g < J yN

1 1

1 .

1 1

1 . 1 / 1 \

( 1

)

Na ug/g oUU 7QC / 1 \ ( 1

)

Ph ug/g 17 1lO.O A R / 1 \

1 1

c VA / AR J. n HA H.OO z U.UO

c9

c

^ OC./ rat 1

0

OO ^/A AC. 340 / 1 \

rat 1

0

nU. 1Mil 777 /IN

ng/g 7An 7A7 OOO /?\ (A)

ug/g J r 7J ml75c. /On

ug/g 11 .yO 1 OI 1 .y 1 /IN

dill ug/g 1 7 1 77 /IN Ta1 a ng/g A<»U /IN

Th1 u ng/g

Th1 n ug/g O AA A.OO /ON (a)

ug/g 900 910 <1) U ug/g 0.95 0.957 ± 0.012 (3)

V ug/g 31 31 (1) u ug/g 1.2 1.18 (1)

Yb ng/g 660 (1)

Zn ug/g 17 17.1 (1) Zr ug/g < 150

2685-1

MEDIAN RANGE METHOD MEANS

Mean ± SD (n) Method

_ < 1500 NAA

1.64 1.67 1.65 (2) NAA

12.3 12.9 12.6 (2) NAA

- < 6 NAA

109 (1) TCGS

105 (1) NAA 5.57 6.1 5.84 (2) NAA

- 66 (1) TCGS

- 5600 (1) NAA — - 17,9 (1) NAA

520 (1) NAA — 4.57 - 4.6 4.58 (2) NAA

22.3 22.6 22.4 (2) NAA

1.31 (1) NAA

1.35 (1) NAA

... 330 - 357 344 (2) NAA

2.40 2.51 2.45 (2) NAA

< 7 NAA

_

- ")

4.6 —

(1) TCGS — 0.913

-

0.94 —0.93 (2) NAA — 2250 2592 2421 (2) NAA

8.6 10.2 9.4 (2) NAA —

—

- 116 —

(1) NAA

- 38 (1) NAA — - < 5 NAA

... - 1.1 (1) TCGS

755 (1) NAA

- 16.8 (1) NAA

4.64 4.62 - 4.76 4.66 (2) CB

... - 4.64 (1) TCGS — - 4.76 (1) IDMS — - 22.546 (1) IDMS — - 0.1777 (1) IDMS — 357 370 363 (2) NAA — 3.7 - 3.73 3.72 (2) NAA — - 1.91 (1) NAA — 1.73 (1) NAA

... _ 240 (1) NAA

< 200 NAA

2.65 2.66 2.66 (2) NAA

910 (1) NAA

0.952 0.948 0.97 0.957 t 0.012 (3) NAA

31 (1) NAA

1.18 (1) NAA 660 (1) NAA

17.1 <1) NAA

< 150 NAA
TABLE 2685-2: INDIVIDUAL DATA FOR NBS SRM 2685 (revised 3/1/86)

Cone Uncer Com Method Reference

< 1500

Al (%)

1.64

1.669

As (ug/g)

12.28

12.9

Au (ng/g)

B (ug/g)

109

Ba (ug/g)

105

Br (ug/g)

5.57

6.1

C (%>

66

Ca (ug/g)

5600

Ce (ug/g)

17.88

CI (ug/g)

520

Co (ug/g)

4.57

4.6

0.04

0.007

0.38

0.6

80

6

0.07

0.5

600

0.18

40

0.06

0.2

ITNA 86GLA 01

ITNA ITNA

ITNA ITNA

ITNA ITNA

ITNA

ITNA

ITNA ITNA

86GLA 01 83LIN 02

83LIN 02

S6GLA 01

ITNA 86GLA 01

TCGS 83LIN 02

86GLA 01 83LIN 02

83LIN 02

86GLA 01

TCGS 83LIN 02

ITNA 86GLA 01

ITNA 83LIN 02

ITNA 86GLA 01

83LIN 02

86GLA 01

Cone

Cr (ug/g)

22.3

22.6

Cs (ug/g )

1.31

Dv (ug/g)

1.35

Uncer Com Method Reference

Eu (na/g>

330

357

Fe (%)

2.396

2.51

Ga (ug/g)

H (%)

4.6

Hf Cug/g)

0.913

0.94

K (ug/g)

2250

2592

La tug/g)

8.6

10.19

Lu (ng/g)

116

Mn (ug/g)

38

0.4

0.8

0.07

0.11

40

4

0.065

0.16

0.2

0.011

0.005

200

45

0.4

0.11

30

ITNA

ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

83LIN 02

86GLA 01

ITNA 83LIN 02

ITNA 86GLA 01

86GLA 01 83LIN 02

83LIN 02

86GLA 01

ITNA 86GLA 01

TCGS 83LIN 02

83LIN 02

86GLA 01

86GLA 01 83LIN 02

86GLA 01 83LIN 02

ITNA 86GLA 01

ITNA 86GLA 01

2685-2
TABLE 2685-2: INDIVIDUAL DATA FOR NBS SRH 2685 (cont.)

Cone

Mo (ug/g)

N (X)

1.1

Wa (ug/g)

755

Rb (ug/g)

16.8

S (%)

Uncer Com Method Reference

0.3

50

1.3

S-32/34 (ratio)

22.546

S-33/3A (ratio)

0.1777

Sb (ng/g?

357

370

Sc tug/g)

3.7

3.73

Se (ug/g)

<

1.91

Sm (ug/g)

1.729

12

30

0.019

0.13

3

0.16

0.007

Ta (ng/g)

240 70

ITNA 86GLA 01

TCGS 83LIN 02

ITNA 86GLA 01

ITNA 83LIN 02

4.62 0.07 CB 85GLA 03 1 4.64 0.19 TCGS 83LIN 02 1 V (ug/g)

4.7 0.02 CB 86GAU 01 1 4.76 0.19 IDMS 84KEL 01 1 31 1 ITNA 86GLA

IDHS

IDMS

84KEL 01

84KEL 01

ITNA 83LIN 02 ITNA 86GLA 01

ITNA ITNA

ITNA

ITNA

83LIN 02

86GLA 01

86GLA 01 83LIN 02

ITNA 83LIN 02

ITNA 86GLA 01

Cone

Tb (ng/g)

Uncer Com Method Reference

< 200

Th (ug/g?

2.65

2.66

Ti (ug/g)

910

u (ug/g?

0.948

0.952

0.97

0.1

0.03

80

0.013

0.005

W (ug/g)

1.18

Yb (ng/g)

660

Zn (ug/g)

17.1

Zr (ug/g)

1.5

0.06

120

10

1.1

< 150

ITNA

ITNA

ITNA DNA

DNA

ITNA

ITNA

ITNA

ITNA

ITNA 86GLA 01

86GLA 01 83LIN 02

ITNA 86GLA 01

83LIN 02

86GLA 01 86GAU 01

86GLA 01 83LIN 02

ITNA 86GLA 01

86GLA 01 83LIN 02

ITNA 86GLA 01

2685-3
TABLE 2689-1: COMPILED DATA FOR NBS SRMs 2689-2691 FLY ASH (revised 3/1/87)

LIMITS

2689 2690 2691

Mesn

Al % 12.94 lb* 7 O 1 BaDa ua/a 800 6500 6600

X 2 18 5 71 18 45

Fe X 9.32 3J 57^ f 4 42

0 12

trV X 2 14 1 00 0 33

1 nf 1 7A U Mg % 0.61 1.53 3.12

Mn ug/g 300 300 200

Na % 0.25 0.24 1.09

P ug/g 1000 5200 5100

S ug/g 1500 8300

Si X 24.06 25.85 16.83

Sr ug/g 700 2000 2700

Ti ug/g 7500 5200 9000

TABLE 2694-1: COMPILED DATA FOR NBS SRM 2694 SIMULATED RAINWATER (revised 3/1/87)

PARAMETER UNITS NBS

I II Mean ± SD Mean ± SD

Acidity meq/L 0.050 ± 0.002 0.284 ± 0.005

Ca ug/L 14 ± 3 49 ± 11

CI mg/L 0.24 1.0

Conductivity uS/cm 26 ± 2 130 ± 2

F ug/L 54 ± 2 98 ± 7

K ug/L 52 ± 7 106 ± 8

Mg ug/L 24 ± 2 51 ± 3

Na ug/L 205 ± 9 419 ± 15

NH4-N mg/L 1.0

N03-N mg/L 7.06 ± 0.15

PH units 4.27 ± 0.03 3.59 ± 0.02

S04 mg/L 2.75 ± 0.05 10.9 ± 0.2

2689-1
TABLE 4350-1: COMPILED DATA FOR NBS SRM 4350 ENVIRONMENTAL RADIOACTIVITY STANDARD, RIVER SEDIMENT (revised 3/1/86)

(Activities shown as of 1 January 1975)

NUCLIDE UNITS NBS CONSENSUS MEDIAN RANGE METHOD

Mean ± SD Mean t SD (n)

Ac-228 pCi/g 0.92 ± 0,18 — — —

Ac -228 mBq/g 34 ± 6.5 — — —

Am- 241 pCi/g 0.0084 < 0.007 — GAMMA

Am- 241 mBq/g 0.314 — — — —

Bi-212 mBq/g 50 — — — —

Bi-212 pCi/g 1.4 — — — —

Bi-214 mBq/g 34 — — — —

Bi-214 pCi/g 0.92 — — — —

Cm- 244 mBq/g 0.0015 — — — —

Co-60 pCi/g 4.00 ± 0.22 — — — —

Co-60 mBq/g 148 ± 8 — - - - — —

Cs-137 pCi/g 2.7 ± 0.12 2.83 ± 0.30 (4) 2.7 2.5 - 3.18 GAMMA

Cs-137 mBq/g 100 ± 4.5 — — — —

Eu-152 pCi/g 6.5 ± 0.38 7.11 (1) — GAMMA

Eu-152 mBq/g 240 ± 14 — — — —

Eu-154 pCi/g 1.4 ± 0.1 1.17 (1) — GAMMA

Eu-154 mBq/g 52 ± 4 — — — —

Eu-155 pCi/g 0.38 — — — —

Eu-155 mBq/g 14 — — — —

Fe-55 pCi/g 43 — — — —

Fe-55 mBq/g 1600 — — — —

I ng/g — 5400 (1) — NAA

1-129 FCI/G — 0.032 (1) — NAA

K-40 pCi/g 14.6 ± 1.3 15.2 (1) — GAMMA

K-40 mBq/g 540 ± 50 — — — —

Mn-54 pCi/g 0.057 ± 0.007 — — —

Mn-54 mBq/g 2.1 ± 0.2 — — — —

Pa-231 pCi/g 0.047 ... — — —

Pa-231 mBq/g 1.75 — — — —

Pb-212 pCi/g 1.6 — — — —

Pb-212 mBq/g 60 — — — —

Pb-214 pCi/g 1-1 — — — —

Pb-214 mBq/g 41 — — — —

Pu-238 pCi/g 0.002 — ... — —

Pu-238 mBq/g 0.067 — — —

Pu-239 pCi/g 0.038 ± 0.003 0.033 (1) — AS

Pu-239 mBq/g 1.4 ± 0.12 — — — —

Ra-226 pCi/g 0.84 — — — —

Ra-226 mBq/g 31 — — — —

Sb-125 pCi/g 0.095 — — — —

Sb-125 mBq/g 3.5 — — — —

Sr-90 pCi/g 0.278 ± 0.042

Sr-90 mBq/g 10.3 ± 1.6

Th-228 pCi/g 1.07

Th-228 mBq/g 39.5

Th-230 pCi/g 0.988

Th-230 mBq/g 36.6

4350-1
TABLE 4350-1: COMPILED DATA FOR NBS SRM 4350 ENVIRONMENTAL RADIOACTIVITY STANDARD, RIVER SEDIMENT (cont.)

NUCLIDE UNITS NBS

Mean i SD

Th-232 pCi/g 0.84

Th-232 mBq/g 34.4

Tl-208 pCi/g 0.38

Tl-208 mBq/g 14

U ug/g

U-234 pCi/g 1.34

U-234 mBq/g 49.6

U-235 pCi/g 0.05

U-235 mBq/g 1.85

U-238 pCi/g 1.14

U-238 mBq/g 42.2

Zn-65 pCi/g 0.35 ± 0.047

Zn-65 mBq/g 13 ± 1.8

CONSENSUS MEDIAN

Mean ± SD (n)

RANGE METHOD

0.9 (1) NAA

TABLE 4350-2: INDIVIDUAL DATA FOR NBS SRM 4350 (revised 3/1/86)

Cone Uncer Ccxn Method Reference

Ani-241 (pCi/g)

Cs-137 (pCi/g)

2.5

2.7

2.95

3.18

Eu-152 (pCi/g)

7.11

Eu-154 (PCi/g)

1.17

0.007

0.35

0.2

0.18

GAMMA 84GLA 11

Cone

I (ng/g)

Uneer Com Method Referenee

U (ug/g)

0.9

GAMMA 86GAU 01 1 5400 5000 RTNA 79BRA

1-129 (fCi/g)

GAMMA 84GLA 02 1 0.032 0.037 RTNA 79BRA

GAMMA 86GAU 01 1 GAMMA 85GAU 04 1 K-40 (DCi/g)

GAMMA 84GLA 11 1 15.2 GAMMA 86GAU

Pu-239 (DCi/g)

GAMMA 84GLA 11 1 0.033 0.001 AS 81 CAR

DNA 84GLA 11

4350-2
TABLE 4350B-1: COMPILED DATA FOR NBS SRM 4350B ENVIRONMENTAL RADIOACTIVITY, RIVER SEDIMENT (revised 3/1/86)

(Activity as of 9 Septetnber 1981)

NUCLIDE UNITS NBS CONSENSUS MEDIAN RANGE METHOD

Mean ± SD Mean ± SD (n)

AC ccO nTi la 1lab2 V 1 1 HAMMA

Am- OL 1 Am cM 1 rkP pci/g \ In ^^\ AC

Am- 9A

Am tH 1 mDq/ y V a I J Z U UJ LO-OU pci/g U • 1 ^3 I Urn UUO n 1? \c.l U « 1 1 uAPIMA UO OU mBc|/g H • OH X U • cJ pci/g nU 7fn f OJ +X nVI • nio VfHT 0 AA? + 0 070 n Ai n 70 - HAMMA

To- 1*^7 nAn /n ?9 0 -f 1 8

C||_ ICO rtPi In UaOCt X \J»\JJJ 1 1/^ 1 • ID uMrirlrt

niRi*i/n 30 5 * 1 2

CU 1 rr\ la 0 10? + 0 01S < 0 3 HAMMA

3 78 ± 0 57

re J J nTi /a

Fe-55 17

rV* i In 1S 13 (^^^ HAMMA UHPlrlM K HU mRrtIn iiR>q/ g Pu-23a r U baJW FPI /G 0 35 -t^ 0 06 0 2 f 1 ^ V

1 AC

rU £JO rrUn nnq/1 n

g n nix + n nn?

Pu-250 nTi pi< i/g/a 0 0137 + 0 onoa 0 0133 0 0116 - 0 0150 AC

r U C mRn noq//ng

lV*i la n 0A7 + n no7 1 00 / 1 ^ uMrlriM Ra-226 mSq/g 35.8 ± 3.6

Sr-90 pCi/g 0.14

Sr-90 mBq/g 5.3

Th-228 pCi/g 0.904 1.03 (1) AS

Th-228 mBq/g 33.5

Th-230 pCi/g 0.796 0.735 (2) 0.67 - 0.8 AS

Th-230 mBq/g 29.5

Th-232 pCi/g 0.896 1.07 (1) AS

Th-232 mBq/g 33.2

U ug/g 2.43 (1) NAA U-234 pCi/g 0.896

U-234 mBq/g 33.2

U-235 pCi/g 0.046

U-235 mBq/g 1.7

U-238 pCi/g 0.832

U-238 mBq/g 30.8

4350B-1
TABLE 4350B-2: INDIVIDUAL DATA FOR NBS SRH 4350B (revised 3/1/86)

Eu-152 (pCi/q)

1.16 0.12

Eu-154 (pCi/g)

< 0.3

IC-40 (pCi/q)

15.13 0.63

GAMMA

GAMMA

84GLA 11

84GLA 1

1

Cone Uncer Com Method Reference | Cone Uneer Com Method Reference

Ac-228 (pCi/g) Pu-238 (fCi/Q)

——_—

1.2 0.43 GAMMA 83KIM 01 j < 10 RAS 86GAU 01 0.2 0.8 AS 84GLA 02

Am-241 (DCi/g)

Pu-239 (pCi/a)

< 0.006 GAMMA 86GAU 01 1 0,005 AS ohGLA no 1 0.0116 0.0025 AS 84GLA 02

0.015 RAS 86GAU 01 Co-60 (DCi/(3)

Ra-226 (pCi/g)

0.11 0.03 GAMMA ni 1

1 0.13 0 = 01 GAMMA 82JEN 03 1 1.99 0.21 GAMMA 84KRI 01

Cs-137 (DCi/fl) Th-228 (DCi/g)

0.79 0.08 GAMMA 86GAU 01 1 1.03 0.03 AS 85JOS 01 0.8 0.1 GAMMA 85GAU 04 1 0.81 0.01 GAMMA 84KRI 01 1 Th-230 (DCi/q)

0.85 0.08 GAMMA 84GLA 02 1 0.96 0.12 GAMMA 84GLA 11 1 0.67 0.05 AS 85J0S 01

GAMMA 84KRI 01

0.8

Th-232 (pCi/g)

1.07 0.06

U (ug/g)

2.43 0.05

AS

AS

DNA

84GLA 02

85J0S 01

85GAU 04

4350B-2
TABLE 4351-1: COMPILED DATA FOR NBS SRMs 4351 and 4352 ENVIRONMENTAL RADIOACTIVITY

(Human Lung and Human Liver)

ELEMENT UNITS NBS

4351 (lung) 4352 (liver)

Mean ± SD Mean t SD

Am- 241 mBq/g 0.11 0.15 ± 0.06

Am- 241 pci/g 0.003 0.0040 ± 0.0015

Pu-238 mSq/g — 0.055 ± 0.024

Pu-238 pCi/g ... 0.0015 ± 0.0006

Pu- 238/239 ratio 0,0150 ± 0.0030 ---

Pu-239 mBq/g 1.1 ± 1.2 2.06 ± 0.39

Pu-239 pCi/g 0.0030 ± 0.0003 0.0556 ± 0.0106

Th-228 mBq/g 0.22 0.51

Th-228 pCi/g 0.0059 0.014

Th-230 mBq/g 0.2 0.2

Th-230 pCi/g 0.0054 0.0054

Th-232 mBq/g 0,21 ± 0.03 0.058

Th-232 pCi/g 0.0057 ± 0.0007 0.0016

U-234 mBq/g 0.10 ± 0.025 0.1

U-234 pCi/g 0.0027 ± 0.0007 0.0027

U-235 mBq/g 0.009

U-235 pCi/g 0.0002

U-238 mBq/g 0.100 ± 0.011 0.088

U-238 pCi/g 0.0027 ± 0.0003 0.0024

4351-1
"8

COz c

8

o

m

<0£

>-

t— O

> 00 z

o < 1—o o

< UJ o u z:

a> o o

«t in < c

o z

Lli (Am z m o

o

V)z

> > UJ +1 Z (/) UJ z c

o O (0 ro < o (L> in z

tnzOf

CO

v>

CD o</> ou. (/> CO H

< z 1- c < (0 o 4) z

oUJ

_l

a.so

(/) 1—

f rom => >*

UJ

_j 1—

OB z

< UJ

< < < < <

z z z z

z z z z X < <

o

(/> <; < < CO < t/i (/) < < < 13 < «( CD < < < z

fO «- t^ T— CNJ *~ \^ w

00 CO o CO o o o

C3 *^

CM 1 1 I in to O 1 O o O 1 1 1 1 -H O I +1 I (M O •H • 1 1 • • • 1 1 1 1 (M • 1 1 1 O ^ 1 1 ^ Kl 1 1 1 1 «— o o 10 • *

ro S- o r~ o in CM

in • o o o

o

(M «*

^3 O o (NJ <NJ

• • •

1 o 1 o 1 1 1 1 o O 1 1 1 1 1 1 1 1 1 1 1

1

0

1 1

1

1 1 1

1 1 00

1 1

1 1

1 in1 (M1 1

1 1

1 1

1 1

1 1

1

1 1 1

1 1 1

1 1 1

1 1 1 «M ro O O o (NJ *

• o • o O a O o

o f\j (NJ

1 in 1 ( in 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

1 1 • 1 1 1 1 <NI 1 1 1 1 1 1 1 1 1 1 1

t O I 1 O 1 1 1 1 • 1 1 1 1 1 1 1 1 1 1 1 O o

/TM\ /-\ /-\

•J- (M (NJ r—

CO 00 o CO o o o

CO o o CO o m "4- in

>*•

«

1 1 1 > in O I 1 ^ O o O I 1 I 1 ^ +< I -M • rvi O •H 1 1 • a • 1 1 1 1 • Cvl 1 1 1 1 o 1 ^ 1 1 r—

in sO

(O in o o <NJ o o o

vO ^

K> O

H +1 CO 00

• CO NO To

in

f\j o

o

•M COo

00o

H

fMO

CO

ino O «- CO CO (M o

o

o

o

«M

o o •o O 00 o r~- o >o o in

to o in o o o o o o O (M o o o to o

fM o to o o »

fM o H H +1 •H H H H +< +i •H H +1 M H H o H • ino H +1 in 1

in K) N- O -O to CO «TM O >o o o lO o to t^ o o> in

<> o (M ro <M O fM 00 o o o CO <> 00 o O o •* to to

0)D>0>0>0)0)0)CnO>00)0>C7>0)0)l7)0)0>0)0)0>0>0>0)0> D) O) O) D) C7) O)

CO 00 1^ 1^ 00 00 o o> •o O 00 00 O o fM fM

fM fM to to in in to to to ro fM fM o O fM fM ro ro to ro >* in in

<M

1 fM1 fM fM fM1 1 1 m1 in1 o>* o•-* fM1 fM

g fM

1 fM1 fMt fM1 o1 On1 fM

1 CM1 CM1 CM1 fM1 CM1 ro

fM

ro

fM

ro

fM

to

fM O U E k E (A U) <u 0) 1 1 3 3 3 <a (0 L. L. JC JZ 1 1 1 < < < < < O CJ u. u. a. a. a. CL ec oe (/> </) 3 3 3 3 3 3 3

4353-1
TABLE 4353-2: INDIVIDUAL DATA FOR NBS SRM 4353 (revised 3/1/86)

Cone Uncer Com Method Reference | Cone Uncer Com Method Reference

Ac-228 (pCi/g)

1 Pu-239 (pCi/g)

2.48 0.57 GAMHA 83KIM 01 1 0.169 0.014 11 AS 85YAM 02

0.202 0.039 AS 84GLA 02

Am- 241 (pCi/g) 0.207 0.014 11 AS 85YAM 02

0.212 0.011 11 AS 85YAM 02

0.024 GAMMA 86GAD 01 1 0.218 0.014 11 AS 85YAM 02

0.035 0.004 RAS Uh I 0.22 0.02 RAS oObAU U 1 0.04 0.004 RAS 1 1 1 1 1 1 0.22 0.02 RAS 1

1

0.042 0.008 AS 84GLA 02 1 0.221 0.017 11 AS 85YAM AO02

Cs-137 (DCi/g) [ Ra-226 (DCi/g)

0.48 0.04 GAMMA ooGAU U1 1 1.03 0.16 GAMMA 83KIM 01 0.52 0.06 GAMMA 84GLA 02 1 0.56 0.05 GAMMA 85GAU 04 1 Th-228 (DCi/g)

0.67 0.1 GAMMA 84GLA 11 1 1.97 0.04 AS 85J0S 01 K-40 (DCi/g)

1 Th-230 (DCi/g)

25 GAMMA 86GAU 01 1 0.88 0.05 AS 85 JOS 01 Pu-238 (DCi/g) 1 1.2 AS 84GLA 02

< 0.01 RAS 86GAU 01 1 Th-232 (DCi/g)

0.0035 0.0019 AS 84GLA 02 1 0.004 0.002 RAS 84GLA 11 1 1.93 0.08 AS 85 JOS 01

U (ug/g)

3.04 0.07 DNA 85GAU 04

U-238 (DCi/g)

1.45 0.49 GAMMA 83KIM 01

4353-2
TABLE 4355-1: COMPILED DATA FOR NBS SRM 4355 ENVIRONMENTAL RADIOACTIVITY - PERUVIAN SOIL (revised 3/1/86)

(Activity as of 1 June 1982)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean i SD Mean (n)

Ag ug/g 1.9

Al % 8.19 ± 0.28

Am- 241 mBq/g 0.004 ± 0.001

Am- 241 pCi/g 0.0001

As ug/g 93.9 ± 7.5

B ug/g 63

Ba ug/g 561 ± 53

Be ug/g 1.77 1 0.27

Bi ug/g 12

Bi-214 mBq/g 40

Bi-214 pCi/g 1.2

Br ug/g 5.4 ± 1.0

Ca % 2.2

Cd ug/g 1.5

Ce ug/g 59.3 ± 3.0

Co ug/g 14.8 ± 0.76

Co- 60 mBq/g < 0.016

Co-60 pCi/g < 0.0004

Cr ug/g 28.9 ± 2.8

Cs ug/g 56.7 ± 3.3

Cs-137 mSq/g 0.33 ± 0.04

Cs-137 pCi/g 0.0090 ± 0.0011

Cu ug/g 77.1 ± 4.7

Dy ug/g 4 ± 1 Eu ug/g 1.18 ± 0.08

Eu-152 mBq/g < 0.23

Eu-152 pCi/g < 0.0063

Eu-154 mBq/g < 0.2

Eu-154 pCi/g < 0.006

Eu-155 mBq/g < 0.2

Eu-155 pCi/g < 0.006

F ug/g 682

Fe % 4.45 ± 0.19

Fe-55 mBq/g 2.0

Fe-55 pCi/g 0.05

Ga ug/g 18.4 ± 1.6

Gd ug/g 35

Hf ug/g 6.3 ± 0.3

Hg ug/g 0.79

Ho ug/g 0.82

K % 1.86 t 0.15

IC-40 mBq/g 585

K-40 pCi/g 16 La ug/g 28.1 ± 1.5

Li ug/g 52 ± 33

Lu ng/g 336 ± 44

4355-1
TABLE 4355-1: COMPILED DATA FOR NBS SRM 4355 ENVIRONMENTAL RADIOACTIVITY - PERUVIAN SOIL (cont.)

ELEMENT UNITS NBS CONSENSUS METHOD

Mean ± SD Mean (n)

Mg % 1.5

Mg ug/g 852 ± 37 ... ...

Mo ug/g 1,7 ... " *

.Na % 1.92 ± 0.11 ...

Nb ug/g 9

Nd ug/g 29.9 ± 1.6

Ni ug/g 13 P ug/g 1100

Pb ug/g 129 ± 26

Pr ug/g 5 Pu-238 niBq/g 0.003

Pu-238 pCtVg < 0.0001

Pu-239 nnBq/g 0.0076 ± 0.0021

Pu-239 pCi/g 0.0002 ± 0.0001

Rb ug/g 138 ± 7.4

Sb ug/g 14.3 i 2.2

Sb-125 nfiq/g < 0.14

Sb-125 pCi/g ^ < 0.0038

Sc ug/g 14.8 ± 0.66

Se ug/g 1.4

Si % 33

Sm ug/g 5.42 ± 0.39

Sr ug/g 330

Sr-90 mBq/g 0.22

Sr-90 pCi/g 0.006

Ta ng/g 764 ± 56

Tb ng/g 665 ± 75

Th ug/g 11 .3 ± 0.73

Th-228 mBq/g 42.2 ± 2.1

Tn-228 pCi/g 1.15 ± 0.06 1.17 (1) AS

Th-230 mBq/g 39.7 ± 2 Th-230 pCi/g 1.08 t 0.06 0.99 (1) AS

Th-232 pCi/g 1.17 ± 0.06 1.21 (1) AS

Ti ug/g 4700

Tl-208 mBq/g 12

Tl-208 pCi/g 0.33

Tm ng/g 420

U ug/g 3.04 ± 0.51 2.82 (2) NAA

V ug/g 151 u ug/g 5.1 Y ug/g 21 Yb ug/g 2.24 ± 0.2

Zn ug/g 368 ± 8.2

Zr ug/g 221

'/

4355-2
TABLE 4355-2: INDIVIDUAL DATA FOR NBS SRM 4355 (revised 3/1/86)

Cone Uncer Com Method Reference

Th-228 (pCi/q)

1.17 0.03

Th-230 (pCi/g)

0.99 0.05

AS

AS

85J0S 01

85J0S 01

Cone Uneer Com Method Reference

Th-232 (pCi/fl) 1.21 0.06

U Cug/g)

2.75

2.88

0.09

0.05

AS

DNA

DNA

85J0S 01

85GAU 04

85GLA 04

TABLE 8412-1: COMPILED DATA FOR NBS RMs 8412 and 8413 CORN STALK AND KERNEL (revised 3/1/87)

ELEMENT UNITS NBS

8412 8413

Mean < SD Mean ± SD

Al ug/g 4 ± 2

Ca ug/g 2160 ± 80 42 ± 5

CI ug/g 2440 ± 140 450 ± 120

Cu ug/g 8 ± 1 3.0 ± 0.6

F ng/g 650 ± 130 240 ± 20

Fe ug/g 139 ± 15 23 ± 5 K % 1.735 ± 0.047 3570 ± 370

Mg ug/g 1600 ± 70 990 ± 82

Mn ug/g 15 i 2 4.0 i 0.3

N % 0.697 ± 0.032 1.375 ± 0.043

Na ug/g 28 ± 8

Se ng/g 16 ± 8 4 ± 2 Sr ug/g 12 ± 2 Zn ug/g 32 ± 3 15.7 ± 1.4

4355-3
TABLE 8030-1: COMPILED DATA FOR NBS RM 8030 TRACE ELEMENTS IN AN AQUATIC PLANT LAGAROSIPHON MAJOR (revised 8/1/87)

Conmunity Bureau of Reference BCR No. 60

Element Units NBS

Mean ± SD

Ag ng/g 200

Al ug/g 6140

As ug/g 8

Au ng/g 20

B ug/g 25 Br ug/g 20

Ca % 3.10

Cd ug/g 2.20 ± 0.10

Ce ug/g 4

CI % 1.0

Co ug/g 4

Cr ug/g 26

Cs ng/g 400

Cu ug/g 51.2 ± 1.9

Eu ng/g 170

F ug/g 24

Fe ug/g 2380

Hg ng/g 340 ± 40

K % 1.14

La ug/g 2 Mg ug/g 6030

Mn ug/g 1759 ± 51 Mo ug/g 2

N % 4.12

Na ug/g 6700

Ni ug/g 40

P ug/g 5140

Pb ug/g 63.8 ± 3.2

Rb ug/g 23

S ug/g 5200

Sb ng/g 400

Sc ng/g 500

Se ng/g 700

Si % 2.85

Sn ug/g 6

Ta ng/g 100

Tb ng/g 100

Ti ug/g 240

Tl ng/g 240

U ng/g 300

V ug/g 6

U ug/g 20

Zn ug/g 313 ± 8

8030-1
TABLE 8031-1: COMPILED DATA FOR NBS RM 8031 TRACE ELEMENTS IN AN AQUATIC MOSS PLATIHYPNIDIUM RIPARIOIDES

(revised 8/1/87)

Conmunity Bureau of Reference BCR No. 61

Element Units NBS

Mean t SD

Ag ug/g 2

Al % 1 .71 As ug/g 7

Au ng/g 220

B ug/g 77

Br ug/g 22

Ca % 1 .70

Cd ug/g 1.07 ± 0.08

Ce ug/g 12

Cl ug/g 2300

Co ug/g 43

Cr ug/g 532

Cs ng/g 600

Cu ug/g 720 ± 31

Eu ng/g 200

F ug/g 60

Fe % 0.93

Hg ng/g 230 ± 20

K % 1 .24

La ug/g 5 Mg ug/g 3900

Mn ug/g 3771 ± 78

Mo ug/g 11

N % 3.35

Na ug/g 3000

Ni ug/g 420

P % 0.92

Pb ug/g 64.4 ± 3.5

Rb ug/g 32

S ug/g 2300

Sb ug/g 1

Sc ug/g 1 Se ug/g 1

Si % 7.52

Sn ug/g 13 Ta ng/g 500

Tb ng/g 200

Ti ug/g 780

Tl ng/g 130

U ng/g 260

V ug/g 6

W ug/g 239

Zn ug/g 566 ± 13

(1>

8031-1
TABLE 8032-1: COMPILED DATA FOR NBS RM 8032 TRACE ELEMENTS IN A CALCAREOUS LOAM SOIL (revised 8/1/87)

Community Bureau of Reference BCR No. 141

Element Units NBS

Mean ± SD

Al % 5.59

As ug/g 8

Ba ug/g 243

Br ug/g 3.5

Ca % 12.86

Cd ng/g 360 i 100

Ce ug/g 81

Cu ug/g 32.6 ± 1.4

Eu ug/g 0.9

Fe % 2.61

Ga ug/g 14

Hf ug/g 3.7

Hg ng/g 56.8 ± 4.3

K % 1.29

La ug/g 27

LOI % 20.65

Mg ugAg 7180

Na ug/g 3200

Nb ug/g 10

P ug/g 700

Pb ug/g 29.4 i 2.6

Rb ug/g 95

Sb ng/g 600

Sc ug/g 8.4

Si % 19.88

Sm ug/g 6.3

Sn ug/g 4.0

Sr ng/g 460

Th ug/g 10.3

Ti ug/g 2800

U ug/g 1.4 Y ug/g 24

Yb ug/g 2.1 Zn ug/g 81.3 ± 3.7

Zr ug/g 120

8032-1
TABLE 8033-1: COMPILED DATA FOR NBS RM 8033 TRACE ELEMENTS IN A LIGHT SANDY SOIL (revised 8/1/87)

Community Bureau of Reference BCR No. 142

'V

E I cment Units NBS

Mean ± SD

a 1 Al % 5.01

As ug/g 16 Ba ug/g 450

Br ug/g o

ca

(yA Cd ng/g ^bU ± VU

Ce ug/g 80

Cu ug/g zr.D ± 0.6

Dy ug/g 5 . ID Er ug/g

Eu ug/g 1 .0

Fe % 1 .96

Ga ug/g 1

1

Gd ug/g 5.7

Hf ug/g 12

Hg ng/g 1 ft/ . i 1 "7 104 ± K % <:.00 La ug/g TO

LU ng/g / 1

«t lU Mg ug/g 65^0

Na ug/g

ND ug/g 1/.

Nd ug/g Oft zo

N1 ug/g

t\r ug/g you

rD ug/g .0 ± 1 .y RD ug/g 1 UD SD ug/g

SC ug/g o.£

Si % 31 .86

Sm ug/g 6.8

Sn ug/g 4

Sr ug/g 164

Th ug/g 11.9

Ti ug/g 3700

W ug/g 1.2

Y ug/g 30.4

Yb ug/g 2.77

Zn ug/g 92.4 ± 4.4

Zr ug/g 390

8033-1
TABLE 8034-1: COMPILED DATA FOR NBS RM 8034 TRACE ELEMENTS IN A SEWAGE SLUDGE (revised 8/1/87)

Community Bureau of Reference BCR No. 144

P 1 Ampnt' Uni ts NBS

Aa uq/q 13

Al % 2.42

As 6.7

ijn/n ua/ a 1

B uo/a 61

Be na/a ' 'y/ y 660

Bi *jy/ y 16 Br ua/a "y/ y 9

Ca 4.06

Cd ua/a 3 41 ± 0 25

Ce ua/a 14 Co ua/a ^jy/ y 9 06 + 0 60

Cu ua/ '-*y/ ay 713 ± 26

% 4.43

Ga ua/a 5 Ha uy/ y 1 49 ± 0 22

K ua/a 'y/ y 6500

Ma ua/a *jy/ y 5500

Mn ua/a 449 ± 13

Mo ug/g 4 Na ug/g 3400

Nb ug/g 3

Ni ug/g 942 ± 22

P % 2.21

Pb uq/q 495 ± 19

Rb ua/a uy/ y 14

Sc ug/g 1.5

Si % 6.37

Sn ug/g 98

Ti ug/g 1140

Tl ng/g 490

V ug/g 14

U ug/g 7

Y ug/g 5 Zn ug/g 3143 ± 103 Zr ug/g 56

8034-1
TABLE 8035-1: COMPILED DATA FOR NBS RM 8035 TRACE ELEMENTS IN A SEWAGE SLUDGE OF MAINLY INDUSTRIAL ORIGIN

(revised 8/1/87)

Community Bureau of Reference BCR No. 146

Element Units NBS

Mean t SO

Ag ug/g 203

Al % 4.76

As ug/g 5.1

Au ug/g 3.6

B ug/g 50

Be ug/g 5.4

Br ug/g 6

Ca % 10.2

Cd ug/g 77.7 ± 2.6

Ce ug/g 100

Co ug/g 11.8 ± 0.7

Cu ug/g 934 ± 24

Fe % 1.85

Ga ug/g 6

Hg ug/g 9.49 ± 0.76

K ug/g 4800

La ug/g 14

LOI % 37.7

Mg % 2.0

Mn ug/g 588 ± 24

Mo ug/g 10

Na ug/g 2200

Nb ug/g 15

Ni ug/g 280 ± 18

P % 2.57

Pb ug/g 1270 ± 28

Rb ug/g 27

Sc ug/g 2.4

Si % 10,6

Ti % 1.74

Tl ug/g 1.2

V ug/9 35

W ug/g 6

Zn ug/g 4059 ± 90

Zr ug/g 9

8035-1
TABLE 8036-1: COMPILED DATA FOR NBS RM 8036 TRACE ELEMENTS IN A SPIKED SKIM MILK POWDER (revised 8/1/87)

ComnHjnity Bureau of Reference BCR No. 150

Element Units NBS

Mean ± SD

Cd ng/g 21.8 ± 1.4

Co ng/g 6.4

Cu ug/g 2.23 ± 0.08

Fe ug/g 11.8 ± 0.6

Hg ng/g 9.4 ± 1.7

I ug/g 1.29 t 0.09

Mn ng/g 236

Ni ng/g 61.5

Pb ug/g 1.00 ± 0.04

Se ng/g 127

Tl ng/g 1.0

Zn ug/g 49.4

8036-1
TABLE 8A31-1: COMPILED DATA FOR NBS RM 8A31 MIXED DIET (revised 3/1/87)

ELEMENT UNITS NBS

Mean ± SD

Al ua/a 4.39 ± 1 07

As 0 92 ± 0 34

Ca uy/ y 1940 ± 140

Cd no/a iiy/ y 42 ± 11 Co no /a 38 ± 8

Cr 1 ly/ y 102 ± 6

Cu ua/o uy/ y 3 36 ± 0 33

Fe ug/g 37.0 ± 2.6

K ug/g 7900 ± 4200

Ma uy/ y 650 ± 40

Hn ua/a uy/ y a 12 ± 0 31

Mo na/a '3/ y 288 ± 29

Na ua/a uy/ y 3120 ± 160

Ni na/a iiy/ y 644 ± 151

p ua/a 3320 ±310

Se na/a iiy/ y 242 ± 30

Zn uq/q 17.0 ± 0.6

ASH % 3 00 ± 0 09

Calorie Cal/100 a 436

Fat % 9.5 ± 0.92

r ructose A

^ R

Glucose % 6.5

Lactose % 3.7

Maltose % 1.8

Phytate mg/g 2.10

Protein % 19.1 ± 0.6

Starch % 24.6 ± 5.0

Sucrose % 11.1

Total Sugar % 28.3 ± 1.7

Total Fiber % 5.3

8431-1
Appendix

References for NBS SRM Collected Data

^COOE N REFERENCE CODE N REFERENCE

55COL 01 N. E. CoLler and R. K. Leininflcr (1955 ) 69C0M 01 U. Compston, B. Chappell, P. Arriens, and H. Vernon (1969) Determination of Total Sulfur Content of Sedimentary Rocks On the Feasibility of NBS 70A K-Feldspar as a Rb-Sr Age

by a Combustion Method, Analytical Chemistry, 27: 949-951. Reference Sample, Geochimica et Cosmochimica Acta, 33: 753.

57SHI 01 N. F. Shimp, J. Connor, A. Prince, and F. Bear (1957) Spectrochemical Analysis of Soils and Biological Materials,

Soil Science, 83: 51-54.

58GRA 01 R. J. Grabowski and R. C. Unice (1958) Quantitative Spectrochemical Determination of Barium and

Strontiun, Analytical Chemistry, 30: 1374-1379.

58WAT 01 H. L. Watts (1958) Volunetric Determination of Aluitiniim in the Presence of

Iron, Titaniun, Calciun, Silicon, and other Impurities,

Analytical Chemistry, 30: 967-970.

59C0L 01 P. F. Collins, H. Diehl, and G. F. Smith (1959) Determination of Iron in Limestone, Silicates, and Refractories, Analytical Chemistry, 31: 1862-1867.

6nuR 01 K. K. Turekian and M. H. Carr (1961) Chromiun, Cobalt, and Strontium in some Bureau of Standards

Rock Reference Samples, Geochimica et Cosmochimica Acta,

24: 1-9.

62J0E 01 0. I. Joensuu and N. H. Suhr (1962) Spectrochemical Analysis of Rocks, Minerals, and Related

Materials, Applied Spectroscopy, 16: 101-104.

63CLA 01 M. C. Clark and D. J. Syaine (1963) Trace Element Contents of the National Bureau of Standards

Reference Samples Numbers 1A, 98, and 99, Geochimica et Cosmochimica Acta, 27: 1139-1142.

63KOR 01 J. Korkisch, G. Arrhenius, and D. P. Kharkar (1963) Spectrophotometric Determination of Titaniun After

Separation by Anion Exchange, Analytica Chimica Acta,

28: 270-277.

64FIL 01 R. K. Filby (1964) The Contents of Several Trace Elements in Some Standard Rock

Sampies, Geochimica et Cosmochimica Acta, 28: 265-269.

65BAL 01 T. K. Ball and R. H. Filby (1965) The Zinc Contents of Some Geochemical Standards by Neutron Activation and X-ray Fluorescence Analysis, Geochimica et Cosmochimica Acta, 29: 737-740.

65MTA 01 Proceedings of the 1965 Internationl Conference on Modern

Trends in Activation Analysis, College Station, Texas.

65WAH 01 W. H. Wahl, V. J. Molinski, and H. Arino (1965) Rapid Radiochemical Separation Procedures for Activation

Analysis Indicators, in 65MTA 01, pp. 44-47.

65WEL 01 N. Wells (1965)

SeleniLin Content of Soil-Forming Rocks, New Zealand Journal

of Geology and Geophysics, 10: 198-208; taken from 74CRE 01.

66HAM 01 E. I. Hamilton (1966) The Uraniim Content of Some International Standards,

Earth and Planetary Science Letters, 1: 317-318.

67KO0 01 H. Kodama, J. E. Brydon, and B. C. Stone (1967)

. X-ray Spectrochemical Analysis of Silicates using Synthetic

Standards with a Correction of Interelemental Effects by a Computer Method, Geochimica et Cosmochimica Acta,

31: 649-659.

69EDM 01 C. R. Ectnond (1969) Direct Determination of Fluoride in Phosphate Rock Samples,

Using the Specific Ion Electrode, Analytical Chemistry,

41: 1327-1328.

69LAE 01 J. R. de Laeter, I. D. Aberchrombie, and R. Date (1969) Mass Spectrometric Isotope Dilution Analyses of BariLui in Standard Rocks, Earth and Planetary Science Letters, 7: 64.

69THI 01 G. Thielicke (1969) Titrimetrische Bestiimung des Aluniniins in Si licatgesteinen

mit Potent iometrischer Indikation, Fresenius Zeitschrift fur Analytische Chemie, 246: 118-122.

69UIC 01 R. Uickbold (1969) Extraktion des Eisens mit Methyl isobuty I keton und seine Titration im Extrakt mit ADTA, Fresenius Zeitschrift fur Analytische Chemie, 244: 372-375.

70ING 01 B. L. Ingram (1970) Determination of Fluoride in Silicate Rocks Without Separation of Alijniniim using a Specific Ion Electrode, Analytical Chemistry, 42: 1825-1827.

70LAE 01 J. R. de Laeter and I. D. Aberchrombie (1970) Mass SpectronKtric Isotope Dilution Analyses of Rubidium and Strontium in Standard Rocks, Earth and Planetary Science

Letters, 9: 327-330.

71FAB 01 B. P. Fabbi (1971) Rapid X-ray Fluorescence Determination of Phosphorus in Geological Seniles, Applied Spectroscopy, 25: 41-43.

71HE1 02 R. H. Heidel (1971) Precision and Detection Limits of Certain Minor and Trace Elements in Silicates by Electron Microprobe Analysis,

Analytical Chemistry, 43: 1907-1908.

71PET 01 M. A. Peters and D. M. Ladd (1971) Determination of Fluoride in Oxides with the Fluoride- ion Activity Electrode, Talanta, 18: 655-664.

72ALL 01 W. J. F. Allen (1972) The Determination of Rubidiim and Caesiim in Geological Materials by Atomic Emission Spectrophotometry with a Nitrous Oxide-Acetylene Flame, Analytics Chimica Acta,

59: 111-117.

72ARU 01 P. J. Aruscavage and H. T. Millard (1972)

A Neutron Activation Procedure for the Determination of

Uranium, Thoriun, and Potassiun in Geological Samples,

Journal of Radioanalytieal Chemistry, 11: 67-84.

72ASH 01 D. G. Ashley and K. W. Andrews (1972) Analysis of Aluninosi I icate Materials by X-ray Fluorescence

Spectrometry, Analyst, 97: 841-845.

72AVN 01 R. Avni, A. Harel, and I. B. Brenner (1972)

A New Approach to the Spectrochemical Analysis of Silicate

Rocks and Minerals, Applied Spectroscopy, 26: 641-545.

72BEC 03 D. A. Becker and P. D. LaFleur (1972) Determination of Trace Quantities of Uraniun in Biological

Materials by Neutron Activation Analysis using a Rapid

Radiochemical Separation, Analytical Chemistry, 44: 1508.

R-1
CODE N REFERENCE CXE N REFERENCE

72B0U 01 J. L. Stxjvier, J. G. Sen Gupta, and S. Abbey (1972) Title Unknown, Geological Survey of Canada paper 72-31,

p. 22; taken from 77LAN 01.

72R00 01 H. L. Rook, P. D. LaFleur, and T. E. Gills (1972) Mercury in Coal: A New Standard Reference Material, Envirormental Letters, 2: 195-204.

72BOW 01 H. J. M. Bowen (1972)

The Determination of Tin in Biological Material by using Neutron Activation Analysis, Analyst, 97: 1003-1005.

72BYR 01 A. R. Byrne (1972) The Toluene Extraction of Some Elements as Iodides from Sulfuric Ac id- Potassium Iodide Media: Application to Neutron Activation Analysis, Analytica Chimica Acta, 59: 91-99.

72CAR 01 B. S. Carpenter (1972) Determination of Trace Concentration of Boron and Uraniun

in Glass by Nuclear Track Technique, Analytical Chemistry,

44: 600-602.

72DAM 01 0. Damsgaard, K. Heydorn, and B. Rietz (1972) Determination of Vsnadiun in Biological Materials by Neutron Activation Analysis, in 72IAE 01, pp. 119-130.

72R00 02 H. L. Rook, T. E. Gills, and P. D. LaFleur (1972) Method for Determination of Mercury in Biological Materials by Neutron Activation Analysis, Analytical Chemistry,

44: 1114-1117.

72ROO 03 H. L. Rook (1972)

Rapid, Quantitative Separation for the Determination of Seleniim using Neutron Activation, Analytical Chemistry,

44: 1276-1278.

72R0S 02 J. N. Rosholt (1972) Private Conmunication; taken from 72ARU 01.

72SAN 01 P. M. Santoliquido and R. R. Ruch (1972) Rapid Radiochemical Separation and Determination of GalliLin

in Coal Ash, Radiochemical and Redioanalytical Letters,

12: 71-76.

72GIB 01 D. Gibbons, M. Perkins, and T. U. Sanders (1972) Determination of Lead in Biological Materials by Neutron Activation Analysis, in 72IAE 01, pp. 131-138.

72HEI 01 M. U. Heitzman and R. E. Siirpson (1972) Neutron Activation Analysis of Mercury in Fish, Flour, and Standard Reference Orchard Leaves by Electrodeposition

Radiochemistry, Journal of the Association of Official Analytical Chemists, 55: 960-965.

72IAE 01 International Atomic Energy Agency (1972) Nuclear Activation Techniques in the Life Sciences,

Proceedings of a Symposiim held in Bled, Yugoslavia, STI/PUB/310.

72JON 03 J. B. Jones and R. A. Issac (1972) Determination of Sulfur in Plant Material using a LECO Sulfur Analyzer, Journal of Agricultural and Food Chemistry,

20: 1292-1294.

72SEI 01 U. R. Seitz and D. M. Hercules (1972) Determination of Trace Amounts of Iron(II) using

Chemi luninescence Analysis, Analytical Chemistry,

44: 2143-2148.

72SIN 01 I. Sinko and L. Kosta (1972) Determination of Lead, Cadniun, Copper, and Zinc in Biological Materials by Anodic Stripping Polarography, International Journal of Environmental Analytical Chemistry,

2: 167-173.

73ABE 01 K. H. Abel and L. A. Rancitelti (1973) Major, Minor, and Trace Element Composition of Coal and Fly

Ash, as Determined by Instrumental Neutron Activation

Analysis, in 73BAB 01, pp. 118-138.

73BAB 01 S. P. Babu, editor (1973) Trace Elements in Fuel, Advances in Chemistry Series 141, American Chemical Society, Washington, 0. C.

72LEV 01 M. Levstek, L. kosta, M. Dermelj, and A. R. Byrne (1972) Vanadiun Determination in Biological Materials by the use of Preconcentratton, in 72IAE 01, pp. 111-116.

72LY0 01 W. S. Lyon, L. C. Bate, and J. F. Emery (1972) Environmental Pollution: Use of Neutron Activation Analysis

to Determine the Fate of Trace Elements from Fossil Fuel Combustion in the Ecological Cycle, in 72IAE 01, pp. 253-261.

72MAG 01 C. U. Magee, 0. L. Oonohur, and U. U. Harrison (1972) Advantages of Dual Electrode Mounts in Spark Source Mass

Spectrometry usir^g Electrical Detection, Analytical

Chemistry, 44: 2413-2415.

72MAI 01 E. J. Maienthal (1972) Analysis of Botanical Standard Reference Materials by

Cathode Ray Polarography, Journal of the Association of

Official Analytical Chemists, 55: 1109-1113.

72M0R 03 G. H. Morrison and N. M. Potter (1972) Multielement Neutron Activation Analysis of Biological

Materiel using Chemical Group Separations and High

Resolution Gamna-ray Spectrometry, Analytical Chemistry,

44: 839- S42.

72RAI 01 T. C. Rains and 0. Menis (1972) Determination of Subroicrogram Amounts of Mercury in Standard

Reference Materials by Flameless Atomic Absorption

Spectrometry, Journal of the Association of Official

Analytical Chemists, 55: 1339-1344.

73BAR 01 I. L. Barnes, E. Garner, J. Gramlich, L. Moore, T. Murphy,

L. Machlan, U. Shields, M. Tatstmoto, and R. Knight (1973), Determination of Lead, Uranium, Thorium, and Thalliun in Silicate Glass Standard Materials by Isotope Dilution Mass Spectrometry, Analytical Chemistry, 45: 880-S85.

73BES 01 Y. Besnus and R. Rouault (1973) Une Methode D' Analyse des Roches au Spectrometre D'Arc a

Lecture Directe par un Dispositif D'Electrode Rotative,

Analusis, 2: 111-116.

73BLA 01 M. S. Black and R. E. Sievers (1973) Environmental Analysis Problems Created by Unexpected Volatile Beryl liun Compounds in Various Samples, Analytical

Chemistry, 45: 1773-1775.

73BL0 02 A. J. Blotcky, L. J. Arsenault, and E. P. Rack (1973) Optimun Procedure for the Determination of Selenium in

Biological Specimens using Se-77m Neutron Activation,

Analytical Chemistry, 45: 1056-1060.

73CAR 01 J. A. Carter, D. Matthews, R. Walker, and J. Walton (1973)

Measurement of Nitrogen and Nitrogen Isotopic Ratios using

Reduction Pyrolysis Coupled with Mass Spectrometry,

Analytical Letters, 6: 951-960.

73C0R 01 R. Cornelis, A. Speecke, and J. Hoste (1973)

A Multielement Serun Standard for Neutron Activation

Analysis, Analytica Chimica Acta, 68: 1-10.

R-2
CODE N REFERENCE

73DAM 01 E. Damsgaard and K. Heydorn (1973) Arsenic in Standard Reference Material 1571 (Orchard Leaves) Presented at the Third Symposiun on the Recent Developments

in Neutron Activation, Cantjridge; also in Danish Atomic Energy Conmission report RISO-M-1633.

73GIA 01 R. D. Giauque, F. Goulding, J. Jaklovic, and R. Pehl (1973) Trace Element Determination with Semiconductor Detector

X-ray Spectrometers, Analytical Chemistry, 45: 671-581.

73C0E 01 J. de Goeij, V. Guinn, D. Young, and A. Mearns (1973) Activation Analysis Trace Element Studies of Dover Sole

Liver and Marine Sediments, IRI report 133-73-09 (Delft).

73HEM 01 D. D. Hemphill, editor (1973) Proceedings of the Seventh Annual Conference on Trace Substances in Environmental Health, University of Missouri,

Columbia, Missouri.

CODE N REFERENCE

73RAM 01 E. R. Rambaldi (1973) Variation in the Coirposition of Plegioclase and Epidote in some Metamorphic Rocks near Bancroft, Ontario, Canadian

Journal of Earth Sciences, 10: 852-868.

73SEG 01 D. A. Segar and J. L. Gilio (1973)

The Determination of Trace Transition Elements in Biological Tissues using Flameless Atom Reservoir Atomic Absorption,

International Journal of Environmental Analytical Chemistry,

2: 291-301.

73SHA 01 L. Shapiro (1973) Rapid Determination of Sulfur in Rocks, Journal of Research

of the U. S. Geological Survey, 1: 81-84.

73SHE 01 D. W. Sheibley (1973) Trace Elements in Instrumental Neutron Activation Analysis

for Pollution Monitoring, in 73BAB 01, pp. 98-117.

73HEY 01 K. Heydorn and E. Damsgaard (1973) Simultaneous Determination of Arsenic, Manganese, and Seleniun in Biological Materials by Neutron Activation

Analysis, Talanta, 20: 1-11.

73MR 01 S. S. Karacki and F. L. Corcoran (1973)

Coal Ash Analysis with an Argon Plasma Emission Excitation

Source, Applied Spectroscopy, 27: 41-42.

73KIM 01 J. I. Kim and H.-J. Born (1973) Monostandard Activation Analysis and its Applications:

Analyses of Kale Powder and NBS Standard Glass Samples,

Journal of Radioanetytical Chemistry, 13: 427.

73SPA 01 C. J. Sparks, 0. Cavin, L. Harris, and J. Ogle (1973) Simple, Quantitative X-ray Fluorescent Analysis for Trace Elements, in 73HEM 01, pp. 361-358.

73STE 01 E. Steinnes (1973) Title unknown, in Trace Elements in Relation to Cardiovascular Diseases, IAEA Technical Report 157, p. 149; taken from 78BYR 01

73TAL 01 Y. Talni and R. Crosmun (1973) Applicability of the RF-Furnace Technique for AA and AE Analysis of Trace Elements in Environmental Sanples, -

in 73HEM 01, pp. 379-383.

73LEB 01 P. J. LeBlanc and A. L. Jackson (1973) Dry Ashing Technique for the Determination of Arsenic in Marine Fish, Journal of the Association of Official Analytical Chemists, 56: 383-386.

73L0 01 F.-C. Lo and 8. Bush (1973) Modified Procedure for Determining Mercury in Coal by Cold

Vapor Atomic Absorption Spectrophotometry, Journal of the Association of Official Analytical Chemists, 56: 1509-1510.

73L0C 01 ,1. C. van Loon, J. Lichwa, and D. Ruttan (1973)

A Study of the Determination and Distribution of Cattniim in Samples Collected in a Heavily I ndust ra I i zed and Urbanized

Region (Metropolitan Toronto), International Journal of Environmental Analytical Chemistry, 3: 147-150.

73LOO 03 J. C. van Loon and J. Lichwa (1973)

A Study of the Atomic Absorption Determination of Some

Important Heavy Metals in Fertilizers and Domestic Sewage

Plant Sludges, Environmental Letters, 4: 1-8.

73TH0 01 A. D. Thomas and L. E. Smythe (1973) Rapid Destruction of Plant Material with Concentrated Nitric Acid Vapor (Vapor Phase Oxidation), Talanta, 20: 459-475.

73TJI 01 P. S. Tjioe, J. de Goeij, and J. Houtman (1973) Automated Chemical Separations in Routine Activation

Analysis, Journal of Radioanalytical Chemistry, 16: 153-164.

74ALV 01 R. Alvarez (1974) Sub-microgram per gram Concentrations of Mercury in Orchard

Leaves Determined by Isotope Dilution and Spark-source Mass

Spectrometry, Analytica Chimica Acta, 73: 33-38.

74AND 01 L. U. Anderson and L. Acs (1974) Seleniun in North American Paper Pulps, Environmental Science and Technology, 8: 462-464.

74AND 03 C. H. Anderson, J. E. Mander, and J. W. Leitner (1974)

Advar»ces in X-ray Analysis, Plenon, New York, Vol. 17,

p. 214; taken from 82TER 03.

73MAI 01 E. J. Maienthal (1973) Determination of Trace Elements in Silicate Matrices by Differential Cathode Ray Polarography, Analytical Chemistry,

45: 644-648.

74BEC 01 R. R. Becker, A. Veglia, and E. R. Schmid (1974) Instrumental Neutron Activation Analysis of Standard

Biological Materials, Radiochemical and Radioanalytical

Letters, 19: 343-354.

73M00 01 L. J. Moore, J. Moody, I. Barnes, J. Gramtich, T. Murphy,

P. Paulsen, and W. Shields (1973), Trace Determination of Rubidium and Strontiun in Silicate Glass Standard Reference

Materials, Analytical Chemistry, 45: 2384-2387.

73NAD 01 R. A. Nadkarni and G. H. Morrison (1973) Multielement InstrLmental Neutron Activation Analysis of Biological Materials, Analytical Chemistry, 45: 19S7 i960.

73PIE 01 J. Pierce, A. Abu-Samra, D. Fehlauer, T. Clevenge' and

J. Vogt (1973), Title unknown, in Trace Elements in Relation

to Cardiovascular Diseases, IAEA, Vienna, p. 103; taken from 80HEY 01.

74BEL 01 Y. Belot and T. Merini (1974) Analyse par Activation Neutronique des PoUuants

Atmospheriques Sol ides Avec unc Technique de Standard

Interne, Journal of Radioanalytical Chemistry, 19: 319-327.

74BER 01 J. Bergholz, J. Luck, P. Moller, and W. Szacki (1974)

Funkenquel len-Massenspektrometrische Analyse des NBS-SRM

610 (3(iin) Standards, Fresenius Zeitschrift fur Analytische

Chemie, 269: 121,

R-3
CODE N REFERENCE CODE N REFERENCE

74B0P 01 B. Boppel (1974) Bleigehalte von Lebensmi tteln. zur Analytik der

B lei best i timing in Lebensmi tteln, Fresenius Zeitschrift

fur Analytische Chemie, 268: 114-119.

74CRE 01 G. L. Crenshaw and H. U. Lakin (1974)

A Sensitive and Rapid Method for the Determination of Trace Amounts of Selenitm in Geoloflical Materials, Journal of Research of the U. S. Geological Survey, 2: 483-487.

74BRA 03 D. V. Brady, J. Montalvo, J. Jung, and R. Curran (1974) Direct Determination of Lead in Plant Leaves via Graphite

Furnace Atomic Absorption, Atomic Absorption Newsletter,

13: 118-119.

74BUS 02 K. W. Busch, N. G. Howell, and G. H. Morrison (1974) Elimination of Interferences in Flame Spectrometry using

Spectral Stripping, Analytical Chemistry, 46: 2074-2079.

74BYR 01 A. R. Byrne (1974) Neutron Activation Analysis of Tin in Biological Materials

and their Ash using Sn-123 and Sn-125, Journal of Radioanalyticat Chemistry, 20: 627-637.

74BYR 02 F. P. Byrne (1974) The Analyst and Accuracy, in 74LAF 01, pp. 123-125.

74BYR 03 A. R. Byrne and L. Kosta (1974) Simultaneous Neutron Activation Determination of Selenium

and Mercury in Biological Samples by Volatilization,

Talanta, 21: 1083-1090.

74CAR 01 B. S. Carpenter and P. D. LaFleur (1974) Nitrogen Determination in Biological Materials by the Nuclear Track Technique, Analytical Chemistry, 46: 1112.

74CAR 02 B. S. Carpenter (1974) Lithiun Determinations by the Nuclear Track Technique,

Journal of Radioanalytical Chemistry, 19: 233-234.

74CAR 03 V. Caramel laCrespi , U. Pisani, M. T. Ganzerl i -Valent ini

,

S. Meloni, and V. Maxia (1974), Determination of Some Noble Metals and Copper by Destructive Neutron Activation Analysis

of Different Matrices, Journal of Radioanalytical Chemistry,

23: 23-31.

74CAR 05 B. S. Carpenter and G. M. Reimer (1974) Homogeneity Considerations in Trace Analysis using the Nuclear Track Technique, in 74LAF 01, pp. 457-459.

74CHA 01 A. Chattopadhyay and R. E. Jervis (1974) Multielement Determination in Market-Garden Soils by Instrimental Photon Activation Analysis, Analytical

Chemistry, 46: 1630-1639.

74DAU 01 E. H. Daughtrey and U. U. Harrison (1974) Analysis for Trace Levels of Boron by Ion-exchange Hollow Cathode Emission, Analytica Chimica Acta, 72: 225-230.

74D0N 01 I. Y. Donev and L. M. Marichkova (1974) Determination of Elements in Standard Material (Bovine Liver

SRM 1577), In 74LAF 01, pp. 1293-1303.

74ERD 01 G. Erdtmann and 0. Abouluafa (1974) Selective Chemical Separation Procedures for Activation

Analysis: II. Separation of Arsenic by ColLim Extraction

with TindDEthylxanthate. Determination in Titaniim Dioxide

of High Antimony Content and in Biological Material, Fresenius Zeitschrift fur Analytische Chemie, 272: 105-114.

74FEL 01 C. Felcinan (1974) Perchloric Acid Procedure for Wet-ashing Organics for the Determination of Mercury (and Other Metals), Analytical

Chemistry, 46: 1606-1609.

74FIT 01 U. F. Fitzgerald, W. B. Lyons, and C. D. Hunt (1974) Cold-trap Preconcentration Method for the Determination of Mercury in Sea Water and in Other Natural Materials,

Analytical Chemistry, 46: 1882-1885.

74FL0 01 T. M. Florence, Y. J. Farrar, L. Dale, and G. Batley (1974)

Beryl I inn Content of NBS Standard Reference Orchard Leaves, Analytical Chemistry, 46: 1874-1876.

74FRI 01 M. H. Friedman, E. Miller, and J. T. Tanner (1974) Instrunental Neutron Activation Analysis for Mercucy in Dogs Adninistered Methylmercury Chloride: Use of a Low Energy

Photon Detector, Analytical Chemistry, 46: 236-239.

74GAL 01 H. Gallorini and E. Orvini (1974) Determination of Zinc in Environmental Matrices: A Comparison of Results Obtained by Independent Methods,

In 74LAF 01, pp. 239-245.

74G0E 01 J. J. M. de Gocij, V. Guinn, D. Young, and A. Mearns (1974) Neutron Activation Analysis Trace Element Studies of Dover

Sole Liver and Marine Sediments, In Comparative Studies of Food and Environmental Contamination, Proceedirtg Series, International Atomic Energy Agency, Vienna, pp. 193-196.

74CH0 02 T. J. Chow, C. C. Patterson, and D. Settle (1974) Occurrence of Lead in Tuna, Nature, 251: 159-161.

74CHU 01 M. R. Church and W. H. Robinson (1974)

A Rapid, Routine Atomic Absorption Spectrometry Method for the Determination of Seteniun at Sub-microgram Levels in Animal Tissue, International Journal of Environmental Analytical Chemistry, 3: 323-331.

74CHU 03 D. A. Church, T. Hadeishi, L. Leong, R. D. McLaughlin, and

B. Zak (1974), Two-chamber Furnace for Flameless Atomic Absorption Spectrometry, Analytical Chemistry, 46: 1352-1355

74C0P 01 T. R. Copeland, R. A. Oysteryoung, and R. Skogerboe (1974) Elimination of Copper-Zinc Intermetal I ic Interferences in Anodic Stripping Vol tairmetry. Analytical Chemistry,

46: 2093-2097.

74C0R 01 R. F. Cormier (1974) Radiometric Age of the keppoch Formation, Browns Mountain

Group, Northern Mainland of Nova Scotia, Canadian Journal

of Earth Sciences, 11: 1325-1329.

74GR0 01 S. B. Gross and E. S. Parkinson (1974) Analysis of Metals in Hunan Tissues using Base (TMAH) Digests and Graphite Furnace Atomic Absorption

Spectrophotometry, Atomic Absorption Newsletter, 13:107-108.

74GUI 01 V. P. Guinn and R. Kishore (1974) Results from Multi -trace-element Neutron Activation Analyses

of Marine Biological Specimens, Journal of Radioanalytical

Chemistry, 19: 367-371.

74HEM 01 D. 0. Hemphill, editor (1974) Proceedings of the Eighth Annual Conference on Trace

Substances in Environmental Health, University of Missouri,

Colurfcia, Missouri.

74HEN 01 T. E. Henzler, R. J. Korda, P. A. Helmke, M. R. Anderson,

H. M. Jimenez, and L. A. Haskin (1974), An Accurate

Procedure for Multielement Neutron Activation Analysis of

Trace Elements in Biological Materials, Journal of

Radioanalytical Chemistry, 20: 649-663.

R-4
CODE N REFERENCE CODE N REFERENCE

74HEY 01 K. Heydorn (1974) Detection of Systematic Errors by the Analysis of Precision,

In 74LAF 01, pp. 127-134.

74HIC 01 J. E. Hicks, J. E. Fleenor, and H. Smith (1974)

The Rapid Determination of Sulfur in Coal, Analytica Chimica

Acta, 6B: 480-483.

74H0F 01 G. L. Hoffman, P. R. Walsh, and H. P. Doyle (1974) Determination of a Geometry and Dead Time Correction Factor

for Neutron Activation Analysis, Analytical Chemistry,

46: 492-496.

74IHN 01 M. Ihnat and R. J. Westerby (1974) Application of Flaroeless Atomization to the Atomic Absorption Determination of Seleniun in Biological Samples,

Analytical Letters, 7: 257-265.

74IHN 02 M. Ihnat (1974) Collaborative Study of a Fluorimetric Method for Determining Selenium in Foods, Journal of the Association of Official Analytical Chemists, 57: 373-378.

74LAF 01 P. D. LaFleur, editor (1974) Accuracy in Trace Analysis: Sampling, Sample Handling, and

Analysis, Proceedings of the Seventh IMR Symposiun, National Bureau of Standards Special Publication 422.

74LEI 01 0. W. Leisure and 0. E. Olson (1974) Use of the AOAC Fluorometric Method for Seleniun in Plants

for the Analysis of Papers and Tobaccos, Journal of the Association of Official Analytical Chemists, 57: 658-661.

74LI 01 R. T. Li and D. M. Hercules (1974) Determination of Chromium in Biological Sanples using

Chemi luninescence. Analytical Chemistry, 46: 916-919.

74NAD 02 R. A. Nadkarni (1974) Re-evaluation of Arsenic Concentration in the Biological

Standards, Radiochemical and Radioanalytical Letters,

19: 127-134.

740ND 01 J. M. Ondov, W. Zoller, I. Olmez, N. Aras, G. Gordon,

L. Rancitelli, K. Abel, R. Filby, K. Shah, and R. Ragaini

(1974), Four -Laboratory Comparative Instrunental Nuclear Analysis of the NBS Coal and Fly Ash Standard Reference

Materials, in 74LAF 01, pp. 211-218.

740RV 01 E. Orvini, T. E. Gills, and P. D. LaFleur (1974) Method for Determination of Selenitm, Arsenic, Zinc, Cadmiun, and Mercury in Environmental Matrices by Neutron Activation Analysis, Analytical Chemistry, 46: 1294-1297.

74RAI 01 T. C. Rains and 0. Menis (1974) An Intercomporison of Flame and Nonflame Systems in Atomic Absorption Spectrometry, in 74LAF 01, pp. 1045-1051.

74RAI 02 T. C. Rains, M. S. Epstein, and 0. Menis (1974) Automatic Correction System for Light Scatter in Atomic Fluorescence Spectrometry, Analytical Chemistry, 46: 207.

. 74RAN 02 L. A. Rancitelli, J. Cooper, and R. Perkins (1974) Multielement Characterization of Atmospheric Aerosols by Neutron Activation end Direct Gamma-ray Analysis, and X-ray Fluorescence Analysis, in Comparative Studies of Food and Environmental Contamination, Proceedings Series, International Atomic Energy Agency, Vienna, pp. 440-444.

74RAV 01 V. Ravnik, M. Dermelj, and L. Kosta (1974)

A Highly Selective Diethyldithiocarbamate Extraction System

in Activation Analysis of Copper, Indium, Manganese, and

Zinc: Application to the Analysis of Standard Reference Materials, Journal of Radioanalytical Chemistry, 20: 443.

74LIN 01 R. van der Linden, F. de Corte, and J. Hoste (1974) Activation Analysis of Biological Material with Rutheniun

as a Multi - isotopic Comparator, Analytica Chimica Acta,

71: 263-275.

74LOO 01 J. C. van Loon and E. J. Brooker (1974)

A Sirrplified Method for Determining Arsenic and Antimony by

the Hydride Evolution-Atomic Absorption Method, Analytical

Letters, 7: 505-513.

74LUT 01 G. J. Lutz (1974) The Analysis of Biological and Environmental Samples for Lead by Photon Activation, Journal of Radioanalytical

Chemistry, 19: 239-244.

74REU 01 F. U. Reuter and U. L. Reynolds (1974) Title UnkrK)wn, in Protein-Metal Interactions, M. Freicinan editor. Plenum Press. New York, p. 621; taken from 780AH 01.

74RIC 01 E. Ricci, T. Handley, and F. Dyer (1974) Analysis of Traces at ORNL's New High-flux Neutron Activation Laboratory, Journal of Radioanalytical

Chemistry, 19: 141-148.

74R00 01 H. L. Rook, P. D. LaFleur and J. E. Suddueth (1974) Trace Element Determination using a High Yield Electromag- netic Isotope Separator and Neutron Activation: The Determination of Cactniuti, Nuclear Instrunnents and Methods,

116: 579-586.

74MAI 01 E. J. Maienthal (1974) The Application of Linear Sweep Voltammetry to the Determination of Trace Elements in Biological and Envirormental Materials, In 74HEM 01, pp. 243-246.

74MAS 01 R. Masironi (1974) Trace Elements in Relation to Cardiovascular Diseases, Uorld

Health Organization Status Report, WHO Offset Publication

Nuit>er 5.

74MCC 01 L. T. McClendon (1974) Selective Determination of Chromiun in Biological and Environmental Matrices, in 74HEM 01, pp. 255-257.

74M0O 01 L. J. Moore, L. Machian, W. Shields, and E. Garner (1974)

Internal Normalization Techniques for High Accuracy Isotope Dilution Analyses - Application to Molybdenum and Nickel in Standard Reference Materials, Analytical Chemistry, 46: 1082

74R0S 02 K. J. R. Rosman and J. R. de Laeter (1974) Mass Spectrometric Isotope Dilution Analyses of Cadmiun in Standard Rocks, Chemical Geology, 13: 69-74.

74RUN 01 L. M. Rundle (1974) A Coirixistion Method for the Determination of Total Sulphur

in Limestones, Analyst, 99: 163-165.

74SCH 03 R. Schelenz and J.-F. Diehl (1974) A Study into the Accuracy of a Remote-controlled System for Multielement Determination in Foodstuffs using NAA,

in 74LAF 01, pp. 1173-1180.

74SHA 01 L. Shapiro (1974) Spectrophotometric Determination of Siica at High Concentrations using Fluoride as a Depolymerizer, Journal

of Research of the U. S. Geological Survey, 2: 357.

R-5
CODE N REFERENCE CODE N REFERENCE

74SIE 02 D. Siemer and R. Woodriff (1974) Application of the Carbon Rod Atomizer to the Determination

of Mercury in the Gaseous Products of Oxygen Combustion of Solid Samples, Analytical Chemistry, 46: 597-598.

75BLO 01 E. R. Blood and G. C. Grant (1975) Determination of CachiiLin in fish Tissue by Flameless Atomic Absorption with a Tantalun Ribbon, Analytical Chemistry,

47: 1438-1441.

74SLE 01 G. Siegers and A. Claeys (1974) Spectrophotometric Determination of Magnesium in Tobacco

Leaves with Eriochrome Black B, Analyst, 99: 471-475.

74SWI 01 D. L. Swindle, L. R. Novak, and E. A. Schweikert (1974) Determination of Iron in Glass and Cobalt via Charged Particle Activation Analysis, Analytical Chemistry,

46: 655-658.

74TAL 01 Y. Talmi (1974) Determination of Zinc and Cactnium in Environmentally Based Samples by the Radiof requency Spectrometric Source, Analytical Chemistry, 46: 1005-1010.

75BL0 02 C. Block (1975) Determination of Lead in Coal and Coal Ashes by Flameless Atomic Absorption Spectrometry, Analytica Chimica Acta,

80: 369-373.

75B0L 01 B. A. Bolton and P. K. Hopke (1975) The Use of Instrunental Neutron Activation Analysis for the Determination of Arsenic Concentrations in Poultry,

Journal of Radioanalytical Chemistry, 25: 299-302.

75BOL 02 H. J. BoUingberg (1975) Geochemical Prospecting using Seaweed, Shellfish and Fish, Geochimica et Cosmochimica Acta, 39: 1567-1570.

74TAL 02 Y. Talmi and A. U. Andren (1974) Determination of SeleniLm in Environmental Samples Using Gas Chromatography with a Microwave Emission Spectrometric Detection System, Analytical Chemistry, 46: 2122-2126.

75CAM 01 J. L. Campbell, B. H. Orr, A. U. Herman, L. A. McNelles,

J. A. Thompson, and W. B. Cook (1975), Trace Element Analysis of Fluids by Proton- induced X-ray Fluorescence

Spectrometry, Arwlytical Chemistry, 47: 1542-1553.

74TAM 01 N. Tamura (1974) Accuracy in the Nondestructive Neutron Activation Analysis

of Coal and Beryllitm for Minor and Trace Elements using Cobalt as a Flux Determinant, Radiochemical and Radioanalytical Letters, 18: 135-142.

74TH0 01 J. Thomas and H. J. Gluskoter (1974) Determination of Fluoride in Coal with the Fluoride Ion-selective Electrode, Analytical Chemistry, 46: 1321.

75CAM 02 W. C. Campbell and J. M. Ottaway (1975) Determination of Lead in Carbonate Rocks by Carbon- furnace

Atomic Absorption Spectrometry after Dissolution in Nitric

Acid, Talents, 22: 729-732.

75CAR 02 E. E. Cary and 0. E. Olson (1975) Atomic Absorption Spectrophotometric Determination of Chromiim in Plants, Journal of the Association of Official

Analytical Chemists, 58: 433-435.

74ULL 01 P. A. Ullucci and J. Y. Hwang (1974) Determination of Caei:iiL«n in Biological Materials by Atomic Absorption, Talanta, 21: 745-750.

74WAH 01 J. S. Wahlberg (1974) Unpublished data; quoted in 74CRE 01.

74WEA 01 J. N. Weaver (1974)

Rapid, Instrimental Neutron Activation Analysis for the Determination of Uraniim in Environmental Matrices,

Analytical Chemistry, 46: 1292-1294.

74WES 01 H. Wesch and A. Bindl (1974) Analysis of 11 Elements in Biological Material: Comparison

of Neutron Activation Analysis and Atomic Absorption

Analysis, in 74LAF 01, pp. 231-235.

74WOL 01 W. R. Wolf and F. E. Greene (1974) Preparation of Biological Materials for Chromium Analysis,

in 74LAF 01, pp. 605-610.

75ABU 01 A. Abu-saina J. S. Morris, and S. R. Koirtyohann (1975)

Wet Ashing of some Biological Samples in a Microwave Oven, Analytical Chemistry, 47: 1475-1477.

75AND 01 R. W. Andrews and D. C. Johnson (1975) Voltammetric Deposition and Stripping of SeleniimdV) at a

Rotating Gold-disk Electrode in 0.1 M Perchloric Acid, Analytical Chemistry, 47: 294-299.

75BAB 01 S. P. Babu, editor (1975) Trace Elements in Fuel, Advances in Chemistry Series 141,

American Chemical Society, Washington, D.C.

75EPS 01 M. S. Epstein, T. C. Rains, and 0. Menis (1975) Determination of Cadmiun and Zinc in Standard Reference

Materials by Atomic Fluorescence Spectrometry with Automatic

Scatter Correction, Canadian Journal of Spectroscopy,

20: 22-26.

75FR0 01 J. Frost, P. Santol iquido, L. Camp, and R. Ruch (1975) Trace Elements in Coal by Neutron Activation Analysis with Radiochemical Separations, in 75BAB 01.

75GLA 01 E. S. Gladney and H. L. Rook (1975) Simultaneous Determination of Telluriim and Uranium by Neutron Activation Analysis, Analytical Chemistry,; 47: 1554.

75GUI 01 V. P. Guinn, M. A. Purcell, and W. W. Wacinan (1975) International Symposiim on Development of Nuclear Based Techniques for Measurement, Detection, and Control of Environmental Pollutants, Vienna, IAEA-SM-206, Paper 30.

75HAG 01 L. Hageman, L. Torma, ar<d B. Ginther (1975) Analysis of Feed Grains and Forages for Traces of Cobalt by Flameless Atomic Absorption Spectroscopy, Journal of the Association of Official Analytical Chemists, 58: 990-994.

75HAL 01 C. Halvorsen and E. Steinnes (1975)

Sirtple and Precise Determination of Zn and Cd in Human Liver

by Neutron Activation Analysis, Fresenius Zeitschrift fur

Analytische Chemie, 274: 199-202.

75HEI 01 H. Heinrichs (1975) Determination of Mercury in Water, Rocks, Coal, and

Petroleum with Flameless Atomic Absorption Spectrophotometry

Fresenius Zeitschrift fur Analytische Chemie, 273: 197-201.

75BEH 01 D. Behne, P. Bratter, and W. Wolters (1975) Bestimnung von Blei in Biologischen Materialien mit Hilfe

der f lamnenlosen Atomabsorpt ionsspektrometrie, Fresenius

Zeitschrift fur Analytische Chemie, 277: 355-358.

75HIN 01 T. A. Hinners (1975) Atomic Absorption Analysis of Liver without Ashing,

Fresenius Zeitschrift fur Analytische Chemie, 277: 377-378.

R-6
CODE N REFERENCE CODE H REFERENCE

75 ISA 01 R. A. Isaoc and W. C. Johnson (1975) CoHaborstive Study of Wet and Dry Ashing Techniques for the Elemental Analysis of Plant Tissue by Atomic Absorption

Spectrophotometry, Journal of the Association of Official Analytical Chemists, 58: 436-AAO.

75J0N 01 J. B. Jones <1975) Collaborative Study of the Elemental Analysis of Plant Tissue by Direct Reading Emission Spectroscopy, Journal of the Association of Official Analytical Chemists, 58: 764.

75JON 01 Ibid., Laboratory 1.

75J0N 02 Ibid., Laboratory 2.

75J0N 03 Ibid., Laboratory 3.

75JON 04 Ibid., Laboratory 4.

75J0N 05 Ibid., Laboratory 5.

75J0N 06 Ibid., Laboratory 6.

75JON 07 Ibid., Laboratory 7.

75J0N 08 Ibid./ Laboratory 8.

75J0N 09 Ibid., Laboratory 9.

75J0N 11 Ibid., Laboratory 11.

75J0N 10 Ibid., Laboratory 10.

75KLE 01 D. H. Klein, A. Andren, J. Carter, J. Emery, C. Feldnan,

U. Futekerson, U. Lyon, J. Ogle, Y. Talmi, R. van Hook, and

N. Bolton (1975), Pathways of 37 Trace Elements through a Coal Fired Pouer Plant, Environmental Science and Technology

9: 973-978.

75K0I 01 H. Koizuna and K. Yasuda (1975) New Zeeman Method for Atomic Absorption Spectrophotometry,

Analytical Chemistry, 47: 1679-1682.

75LIE 01 P. Lievens, R. Cornel is, and J. Hoste (1975)

A Separation Scheme for the Determination of Trace Elements

in Biological Materials by Neutron Activation Analysis,

Analytica Chimica Acta, 80: 97-108.

75LIT 01 R. Litman, H. L. Finston, and E. T. Williams (1975) Evaluation of Sairple Pretreatments for Mercury Determination

Analytical Chemistry, 47: 2364-2369.

75MAN 01 0. C. Manning (1975) Aspirating Small Volune Samples in Flame Atomic Absorption

Spectroscopy, Atomic Absorption Newsletter, 14: 99-102.

75MAZ 01 B. Maziere, J. Gros, and D. Comer (1975) Possibilities et Limites de I'Analyse d'Echanti I Ions Biologiques par Activation Neutronique derriere Ecran de

Cadniun, Journal of Radioanalytical Chemistry, 24: 279-293.

75MCG 01 J. R. McCinley and E. A. Schweikert (1975) Determination of Lithiun, Boron, and Carbon by Quasi -prompt Charged Particle Activation Analysis, Analytical Chemistry,

47: 24032407.

75MIL 01 H. T. Millard and V. W. Swanson (1975) Neutron Activation Analysis of Coals using Instrunental Techniques, Transactions of the American Nuclear Society,

21: 108-109.

75MUR 01 J. Murphy (1975) Determination of Mercury in Coals by Peroxide Digestion and

Cold Vapor Atomic Absorption Spectrophotometry, Atomic Absorption Newsletter, 14: 151-152.

75NAD 02 R. A. Nadkarni (1975) Multielement Analysis of Coal and Coal Fly Ash Standards by

Instrumental Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 21: 161-176.

750LS 01 0. E. Olson, I. S. Palmer, and E. E. Cary (1975) Modification of the Official Fluorometric Method for Seleniun in Plants, Journal of the Association of Official Analytical Chemists, 58: 117-121.

750ND 01 J. M. Ondov, W. ZoUer, I. Olmez, N. Aras, G. Gordon,

L. Rancitelli, K. Abel, R. Filby, K. Shah, and R. R^gaini

(1975), Elemental Concentrations in the National Bureau of Standards Environmental Coal and Fly Ash Standard Reference

Materials, Analytical Chemistry, 47: 1102-1109.

750WE 01 J. U. Owens and E. S. Gladney (1975) Determination of Berylliun in Environmental Materials by Flameless Atomic Absorption Spectroscopy, Atomic Absorption

Newsletter, 14: 76-77.

75PEC 01 E. S. Peck (1975) Spectrogrephic Determination of Mercury in Rocks and Coal, Analytica Chimica Acta, 80: 75-83.

75PIC 01 C. J. Pickford and G. Rossi (1975) Determination of Some Trace Elements in NBS (SRM-1577) Bovine Liver using Ftemeless Atomic Absorption and S«lid

Sampling, Atomic Absorption Newsletter, 14: 78-80.

75PIE 01 R. Pietra, E. Sabbioni, and F. Girardi (1975) Determination of Ca, Mg, Ni, and Si in Biological Materials

by Neutron Activation and Cerenkov Counting, Radiochemical

and Radioanalytical Letters, 22: 243-250.

75P0L 01 E. N. Pollock (1975) Trace Impurities in Coal by Wet Chemical Methods,

in 75BAB 01.

75PUF 01 J. H. Puffer and R. S. Cohen (1975) Field Determination of Sodium and Potassium in Feldspars by Ion-selective Electrodes, Chemical Geology, 15: 217-222.

75REU 01 F. W. Reuter (1975) Numerical Matrix Correction Technique for the Measurement of Trace Elements in Plant Materials by X-ray Fluorescence

Spectrometry, Analytical Chemistry, 47: 1763-1766.

75RIC 01 E. Ricci (1975) Methodology for High-flux Absolute Multielement Neutron Activation Analysis: Environmental Baselines by Analysis

of Tree Rings, Analytica Chimica Acta, 79: 109-124.

75RUC 01 R. R. Ruch, R. Cahill, and J. Frost (1975) Trace Elements in Coals of the United States Determined by Activation Analysis and Other Techniques, Transactions of

the American Nuclear Society, 21: 107-108.

75SIE 01 D. D. Siemer and L. Hagemann (1975)

An Inproved Hydride Generation- Atomic Absorption Apparatus

for Seleniun Determination, Analytical Letters, 8: 323-337.

75SLA 01 S. Slavin, G. E. Peterson, and P. C. Lindahl (1975) Determination of Heavy Metals in Meats by Atomic Absorption

Spectroscopy, Atomic Absorption Newsletter, 14: 57-59.

R-7
CODE N REFERENCE CODE N REFERENCE

75SME 01 J. Smeyers-Vebede, C. Segebarth, and D. L. Massart (1975) The Determination of Cu and Hn in Small Biological Samples

with Graphite Furnace Atomic Absorption Spectrometry, Atomic Absorption Newsletter, 14: 153-154.

75STE 02 E. Steinnes (1975)

A Two-group Separation Scheme for the Determination of 11 Trace Elements in Biological Material by Neutron Activation

Analysis, Analytica Chimica Acta, 78: 307-315.

75TAL 01 Y. Talmi and V. E. Norvell (1975) Determination of Arsenic and Antimony in Environmental Samples using Gas Chromatography with a Microwave Emission Spectrometric System, Analytical Chemistry, 47: 1510-1516.

75TH0 01 C. P. Thomas (1975) An Integrated Intensity Method for Emission Spectrographic

Computer Analysis, Journal of Research of the United States

Geological Survey, 3: 181-185.

75WEL 02 R. H. Welch and E. E. Cary (1975) Title unknown, in Journal of Agricultural and Food Chemistry, 23: 479; taken from 78BYR 01.

75UIM 01 J. U. Wimberley (1975) The Determination of Total Mercury at the Part- Per-Bi 1 1 ion Level in Soils, Ores, and Organic Materials, Analytica

Chimica Acta, 76: 337-343.

75WCR 01 G. J. Worrell, T. J. Vickers, and F. D. Williams (1975)

A Solvent Extraction-Atomic Fluorescence System for the Determination of Cadmiuni in Complex Tamples, Analytica

Chimica Acta, 75: 453-456.

76AGG 01 J. Aggett and A. C. Aspell (1976) The Determination of ArsenicdII) and Total Arsenic by

Atomic Absorption Spectroscopy, Analyst, 101: 341-347.

76AND 01 R. W. Andrews and D. C. Johnson (1976) Determination of SeleniumdV) by Anodic Stripping

Voltammetry in Flow System with Ion Exchange Separation,

Analytical Chemistry, 48: 1056-1060.

76BAT 01 L. C. Bate, S. E. Lindberg, and A. W. Andren (1976) Elemental Analysis of Water and Air Solids by Neutron Activation Analysis, Journal of Radioanalytical Chemistry,

32: 125-135.

76BL0 01 C. Block, R. Dams, and J. Hoste (1976) Chemical Composition of Coal and Fly Ash, in 76IAE 01,

pp. 101-110.

76CAV 01 P. Cavalli and G. Rossi (1976) Determination of Submicrogram Amounts of Mercury in Various Matrices by Flaroeless Atomic Fluorescence Spectrometry, Analyst, 101: 272-277.

76CHA 01 A. Chattopadhyay (1976) Multielement Instrunental Photon Activation Analysis of Digested Sewage Sludges, in 76IAE 01, pp. 383-403.

76CHA 02 C. C. Y. Chan (1976) Improvement in the Fluorometric Determination of Seleniuti in

Plant Materials with 2,3-Diaminonaphthalene, Analytica

Chimica Acta, 82: 213-315.

760ER 01 M. Dermelj, V. Ravnik, and L. Kosta (1976)

A Fast Isolation and Determination of Cd in Some Fungi,

Other Biological Materials, Soil, and Zn Metal by NAA,

Radiochemical and Radioanalytical Letters, 24: 91-102.

7601K 01 M. Diksic and M. 0. McCrad>- (1976)

Fast Determination of Selenium in Biological Materials by Instrunental Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 26: 89-94.

76D0G 01 S. Dogan and U. Haerdi (1976) Some Applications of Rapid Separation of Mercury on Metallic

Copper to Environmental Samples with Determination by Flameless Atomic Absorption Spectrometry, Analytica Chimica

Acta, 84: 89-96.

76EPS 01 M. S. Epstein, T. C. Rains, and T. C. O'Haver (1976) Wavelength Modulation for Background Correction in Graphite

Furnace Atomic Emission Spectrometry, Applied Spectroscopy,

30: 324-329.

76EPS 02 H. S. Epstein (1976) Private Communication, National Bureau of Standards; taken

from 76ZAN 01.

76FI0 01 J. A. Fiorino, J. W. Jones, and S. G. Capar (1976) Sequential Determination of Arsenic, Seleniim, Antimony, and Tellurium in Foods via Rapid Hydride Evolution and Atomic Absorption Spectrometry, Analytical Chemistry, 48: 120-125.

76FUK 01 H. Fukami, S. Toda, and K. Fuwa (1976) Development of a New Type Low Temperature Asher for Small Amounts of Biological Sample, Bunseki Kagaku, 25: 282-284.

76GAL 01 M. Gallorini, M. diCasa, R. Stella, N. Geneva, and E. Orvini

(1976), Multielement Trace Analysis by Atomic Absorption

Spectrometry and Neutron Activation Analysis in Biological

Matrices, Journal of Radioanalytical Chemistry, 32: 17-23.

76GAN 01 R. Ganapathy, G. M. Papia, and L. Grossman (1976) The Abundances of Zirconiun and Hafnium in the Solar System, Earth and Planetary Science Letters, 29: 302-308.

76GAU 01 A. Gaudry, B. Haziere, D. Comar, and D. Nau (1976) Multielement Analysis of Biological Samples after Intense Neutron Irradiation and Fast Chemical Separation, Journal

of Radioanalytical Chemistry, 29: 77-87.

76GLA 01 E. S. Gladney, E. T. Jurney, and D. B. Curtis (1976) Nondestructive Determination of Boron and Cadmiim in Environmental Materials by Thermal Neutron-Prompt Gamma-ray

Spectrometry, Analytical Chemistry, 48: 2139-2142.

76GLA 02 E. S. Gladney and J. W. Owens (1976) Berylliun Emission from a Coal-fired Power Plant,

Journal of Environmental Science end Health, A11: 297-311.

76GUI 01 V. P. Guinn, M. A. Purcell, and W. W. Wactnan (1976) Measurement of Vanadiun in Oceanographic/Envi ronmental

Samples by Neutron Activation Analysis with Pre-irradiation

Separation, in 761AE 01, pp. 407-412.

76GUZ 01 G. Guzzi, R. Pietra, and E. Sabbioni (1976) Determination of 25 Elements in Biological Standard

Reference Materials by Neutron Activation Analysis, Journal

of Radioanalytical Chemistry, 34: 35-57.

76HAD 01 T. Hadeishi and R. D. McLaughlin (1976)

Zeeman Atomic Absorption Determination of Lead with a Dual

Chamber Furnace, Analytical Chemistry, 48: 1009-1011.

76HAN 01 R. G. V. Hancock (1976) Low Flux Multielement InstrLmental Neutron Activation

Analysis in Archaeometry, Analytical Chemistry, 48: 1443.

R-8
CODE N REFERENCE CODE N REFERENCE

76H0W 01 N. G. Howell, J. D. Ganjei, and G. H. Morrison (1976)

Internal Standard! lat ion in Flame Analyses using a Vidicon

Spectrometer, Analytical Chemistry, 48; 319-326.

76IAE 01 International Atomic Energy Agency (1976) Proceedings of an International Synposiun on the Development

of Nuclear-based Techniques for the Measurement, Detection,

and Control of Environmental Pollutants, Vienna.

76IHN 01 H. Ihnat (1976) Atomic Absorption Spectrometric Determination of Seleniim

with Carbon Furnace Atomization, Analytica Chimica Acta,

82: 293-309.

76IHN 02 H. Ihnat (1976) Seleniin in Foods: Evaluation of Atomic Absorption

Spectrometric Techniques involving Hydrogen Selenide Generation and Carbon Furnace Atomization, Journal of the Association of Off icial Analytical Chemists, 59: 911-922.

76ICAT 02 T. Kato, M. Masunoto, N. Sato, and N. Suzuki (1976)

The Yields of Photonuclear Reactions for Multielement

Photon Activation Analysis, Journal of Radioanalytical

Chemistry, 32: 51-70.

76KAT 03 T. Kato, N. Sato, and N. Suzuki (1976) Nondestructive Multielement Photoactivation Analysis of Environmental Materials, Talanta, 23: 517-524.

76HEL 03 S. Meloni, V. Caramel la-Crespi , and G. Fassi (1976) Determination of Some Bioelements in Rice Grains by Neutron Activation Analysis, Journal of Radioanalytical Chemistry,

34: 113-119.

76MIL 02 D. A. Miller and V. P. Guinn (1976) Precision High-speed Neutron Activation Analysis via Very Short-Lived Activities, Journal of Radioanalytical Chemistry

32: 179-188:

760ND 01 J. M. Ondov, R. Ragaini, R. Heft, G. Fisher, D. Silberman, and B. Prentice (1976), Inter laboratory Comparison of Neutron Activation and Atomic Absorption Analysis of Size Classified Stack Fly Ash, in Methods and Standards for Environmental Measurement, Proceedings of the Eighth IMR Symposium, Gaithersburg, Maryland, National Bureau of Standards Special Publication 464, pp. 565-569.

760WE 01 J. W. Owens and E. S. Gladney (1976) Lithium Metaborate Fusion and the Determination of Trace

Metals in Fly Ash by Flameless Atomic Absorption,' Atomic Absorption Newsletter, 15: 95-97.

76PIE 01 J. 0. Pierce, F. Lichte, C. Vogt, A. Abu-Sarma, T. Ryan,

S. Koirtyohann, and J. Vogt (1976), Comparison of Chromiim

Determinations in Environmental and Biological Sanples by Neutron Activation Analysis, Atomic Absorption, end Gas Chromatography, in 76IAE 01, pp. 357-368.

76»CAT 04 T. Kato, N. Sato, and N. Suzuki (1976) Multielement Photon Activation Analysis of Biological

Materials, Analytica Chimica Acta, 81: 337-347.

76K0I 01 H. Koizumi and K. Yusuda (1976) Determination of Lead, Cadmium, and Zinc using the Zeeman Effect in Atomic Absorption Spectrometry, Analytical Chemistry, 48: 1178-1182.

76RAG 01 R. C. Ragaini, R. E. Heft, end D. Garvis (1976) Neutron Activation Analysis at the Livermore Pool-Type Reactor for the Environmental Research Program, Lawrence Livermore Laboratory report UCRL- 52092.

76SIE 01 D. D. Siemer, P. Koteel, and V. Jariwala (1976) Optimization of Arsine Generation in Atomic Absorption Arsenic Determinations, Analytical Chemistry, 48: 836-840.

76KRI 03 K. V. Krishnamurty, E. Shprit, and M. M. Reddy (1976) Trace Metal Extraction of Soils and Sediments by Nitric Acid-Hydrogen Peroxide, Atomic Absorption Newsletter,

15: 68-70.

76KUC 01 E. T. Kucera and R. R. Heinrich (1976) Multielement Trace Analysis of Coals, Ashes, and Related Materials from Coal -Treatment Facilities by Instrutiental Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 32: 137-150.

76LAN 01 F. J. Langmyhr and J. Aamodt (1976) Atomic Absorption Spectrometric Determination of Some Trace

Metals in Fish Meal and Bovine Liver by the Solid Sampling

Technique, Analytica Chimica Acta, 87: 483-486.

76STE 01 R. Stella, N. Genova, H. di Casa, H. Gal lorini .and E. Orvini

(1976), Comparative Investigation of Different Radiochemical Methods for Chromium Determination in Biological and Environmental Matrices, Journal of Radioanalytical Chemistry

34: 59-63.

76STE 05 E. Steinnes (1976) Instrumental Activation Analysis of Coal and Fly Ash with Thermal and Epithermal Neutrons and Short-Lived Nuclides,

Analytica Chimica Acta, 87: 451-462.

76URE 01 A. M. Ure and M. C. Mitchell (1976) The Determination of Cadmium in Plant Material and Soil Extracts by Solvent Extraction and Atomic Absorption with a Carbon-rod Atomizer, Analytica Chimica Acta, 87: 283-290.

76LE0 02 L. Leoni and M. Saitta (1976) X-ray Fluorescence Analysis of 29 Trace Elements in Rock and

Mineral Standards, Rendiconti Soc. Italiana di Mineralogia e Petrologia, 32: 497-510.

76MCC 03 M. T. McCulloch, J. R. de Laeter, and K. j. R. Rosman (1976)

The Isotopic Composition and Elemental Abundance of Lutetium

in Meteorites and Terrestrial Samples and the Lu-176 Cosmochronometer, Earth and Planetary Science Letters,

28: 308-322.

76MEL 01 S. Meloni, V. Caramel la-Crespi , M. T. Ganzer I

i -Valentin!

,

and P. Borroni (1976), Accurate Determination of Arsenic and Mercury in Reference Materials by Destructive Neutron

Activation Analysis, Radiochemical and Radioanalytical

Letters, 25: 117-128.

76VIJ 01 P. N. Vijan and G. R. Wood (1976)

Semi -automated Determination of Lead by Hydride Generation

and Atomic Absorption Spectrophotometry, Analyst, 101: 966.

76VIJ 02 P. N. Vijan, A. C. Rayner, D. Sturgis, and G. R. Uood (1976)

A Semi -automated Method for the Determination of Arsenic in

Soil and Vegetation by Gas-phase Sampling and Atomic Absorption Spectrophotometry, Analytica Chimica Acta, 82:329

76WAU 01 R. D. Wauchope (1976) Atomic Absorption Determination of Trace Quantities of

Arsenic: Application of a Rapid Arsine Generation Technique

to Soil, Water, and Plant Samples, Atomic Absorption

Newsletter, 15: 64-67.

R-9
CODE N REFERENCE CODE N REFERENCE

76UEW 01 E. U. Wewerka <1976) Trace Element Characterization and Remove I /Recovery from

Coal and Coal Wastes, Los Alamos Scientific Laboratory

report LA-6498-PR.

76WHI 01 D. Whitehead and S. A. Malik (1976) Automated Colorimetric Determination of Phosphorus in Silicate Rocks in the Presence of Silicon, Analyst,

101: 485-490.

76UIL 01 D. R. Williams and J. S. Hislop (1976) Determination of Copper and Zinc in Bone Ash using Accelerator Produced Gamma Photons, Proceedings of the Analytical Division of the Chemical Society (London), 13:202.

76W0L 01 U. R. Wolf (1976) Coupled Gas Chromatography Atomic Absorption Spectrometry

for the Nanogram Determination of Chromiuii, Analytical

Chemistry, 48: 1717-1720.

76ZAN 01 A. T. Zander, T. C. O'Haver, and P. N. Keliher (1976) Continuum Source Atomic Absorption Spectrometry with High Resolution and Wavelength Modulation, Analytical Chemistry,

48: 1166-1175.

76ZAN 02 A. T. Zander and T. C. O'Haver (1976) Improved Accuracy in Background Corrected Atomic Absorption

Spectrometry, in Methods and Standards for Environmental

Measurement, Proceedings of the Eight IMR Symposium,

Gaithersburg, Maryland, National Bureau of Standards Special Publication 464, pp. 53-59.

76ZEI 01 R. Zeisler, J. B. Cross, and E. A. Schweikert (1976) Trace Elemental Analysis by Heavy Ion Induced X-ray Emission

Analytical Chemistry, 48: 2124-2129.

77AND 01 W. L. Anderson and K. E. Smith (1977) Dynamics of Mercury at Coal-Fired Power Plant and Adjacent

Cooling Lake, Environmental Science and Technology, 11: 75.

77ARU 01 P. Aruscavage (1977) Determination of Arsenic, Antimony, ar>d Selenium in Coal by Atomic Absorption Spectrometry with a Graphite Tube Atomizer

Journal of Research of the U. S. Geological Survey, 5: 405.

77BAJ 02 S. Bajo and A. Wyttenbach (1977) Liquid-Liquid Extraction of Cadniim with Diethyldithio- carbamic Acid, Analytical Chemistry, 49: 158-161.

77BAN 03 S. Bando and T. Imahashi (1977) Determination of Arsenic, Mercury, and Selenium in

Biological Standard Reference Materials by Neutron Activation Analysis, Bunseki Kagaku, 26: 138-140.

77BRU 01 H. J. Brjnsack (1977) Potential Metal Pollution in Grass and Soil Samples around

Brickworks, Environmental Geology, 2: 33-41.

77BU0 01 J. A. Buono, J. C. Buono, and J. L. Fasching (1977)

Simultaneous Determination of Al, V, Mn, and Cu from

Neutron- Activated Saline Matrices by Precipitation with

Poly-5-vinyl -8-hydroxyquinol ine. Journal of Radioanalytical

Chemistry, 36: 353-358.

77BUR 01 W. R. Burke and B. I. Diamondstone (1977) Procedures for the Determination of Arsenic, Copper, and

Nickel by Molecular Absorption Spectrometry, in 77MAV 01,

pp. 73-84.

r7BYR 01 A. R. Byrne (1977) Activation Analysis of Tin at Nanogram Levels by Liquid Scintillation Counting of Sn-121, Journal of Radioanalytical

Chemistry, 37: 591-597.

77CAH 01 R. A. Cahill (1977) Title Unknown, taken from 77GLU 01.

77CAM 01 J. L. Campbell (1977) Specimen Preparation in PIXE Analysis, Nuclear Instruments and Methods, 142: 263-273.

77CHA 01 A. Chattopedhyay (1977) Optimal use of Instrunental Neutron and Photon Activation

Analysis for Multielement Determinations in Sewage Sludges,

Journal of Radioanalytical Chemistry, 37: 785-799.

77CR0 01 J. B. Cross, R. Zeisler, and E. A. Schweikert (1977) High Energy Heavy-Ion Induced X-ray Emission Analysis, Nuclear Instrunents and Methods, 142: 111-119.

TTDER 01 H. Dermelj, V. Ravnik, and L. Kosta (1977) Simultaneous Determination of Trace Elements Cd, Cu, and Zn

in Different Environmental Samples by Neutron Activation

Analysis, Radiochemical and Radioanalytical Letters, 28: 231

77DIK 01 M. Diksic and T. F. Cole (1977)

Fast Determination of Molybdenim and Telluriun by Neutron Activation Analysis, Analytica Chimica Acta, 93: 261-266.

77D0N 01 0. L. Donohue, J. A. Carter, and J. C. Franklin (1977) Separated Isotopes as Internal Standards in Spark Source Mass Spectrometry, Analytical Letters, 10: 371-379.

77EGA 01 A. Egan, S. A. Kerr, and M. J. Minski (1977) Determination of Seleniun in Biological Materials using Se-77m and Cyclic Activation Analysis, Radiochemical and Radioanalytical Letters, 28: 369-378.

77FEL 01 C. Felchian (1977) Determination of Traces of Arsenic in Siliceous Materials,

Analytical Chemistry, 49: 825-828.

77FIL 01 R. H. Filby, k. R. Shah, and C. A. Sautter (1977)

A Study of Trace Element Distribution in the Solvent Refined

Coal Process using Neutron Activation Analysis, Journal

of Radioanalytical Chemistry, 37: 693-704.

77FLA 01 F. J. Flanagan, L. Schwartz, J. Rowe, and A. Dorrzapf (1977) Available Clay and Feldspar Reference Samples as Standards

for Archaeological Pottery Studies, Geostandards Newsletter,

1: 61-66.

77FL0 01 T. Florkowski, T. Kuc, and S. Piorek (1977)

Determination of Trace Elements in Plants by the X-ray

Fluorescence Analysis of Environmental Pollution

Investigations, International Journal of Applied Radiation

end Isotopes, 28: 679-686.

77FRI 01 M. T. Friend, C. A. Smith, and D. Wishart (1977)

Ashing and Wet Oxidation Procedures for the Determination of

Some Volatile Trace Metals in Foodstuffs and Biological

Materials by AAS, Atomic Absorption Newsletter, 16: 46-49.

77FRY 01 R. C. Fry and M. B. Denton (1977)

High Solids Sample Introduction for Flame Atomic Absorption

Analysis, Analytical Chemistry, 49: 1413-1417.

77FUJ 01 <. Fujiwara, Y. Umezawa, U. Nunata, and K. Fuwa (1977)

Carbon Rod Atomic Absorption for Intact Cell Systems and

Biological Tissues, Bunseki Kagaku, 26: 735-737.

R-10
CODE N REFERENCE CODE N REFERENCE

77GAN 03 S. Gangadharon, M. S. Das, and S. Yegnasubramani an (1977) Measurement of Annihilation Radiation in Activation Analysis Enhancement of Specificity through Triple Coincidence,

Journal of Radioanalytical Chemistry, 37: 181-187.

77G1A 01 R. D. Giauque, R. B. Garrett, and L. Y. Goda (1977) Determination of Forty Elements in Geochemical Samples and

Coal Fly Ash by X-ray Fluorescence Spectrometry, Analytical

Chemistry, 49: 1012-1017.

77GIA 02 R. D. Giauque (1977) Private Comunication, Lawrence Berkeley Laboratory.

77GIL 01 T. E. Gills and L. T. McClendon (1977) Role of Neutron Activation Analysis in the Evaluation of

Sampling, Storage, and Analysis of Samples for the National

Envi rormental Banking System, Journal of Radioanalytical

Chemistry, 39: 285-291.

77GIL 03 T. E. Gills, M. Gallorini, and R. R. Greenberg (1977)

The Determination of Selected Toxic Elements in Biological Matrices using Radiochemical Activation Analysis,

in 77V0G 01, pp. 597-609.

77GLA 01 E. S. Gladney (1977) Copper Determination in Standard Materials by Neutron Activation and Srafion NHRR Anion- Exchange Resin,

AnalyticB Chimica Acta, 91: 353-356.

77GLA 02 E. S. Gladney (1977) Direct Determination of Beryllium in NBS SRM 1632 Coal by

Flameless Atomic Absorption, Atomic Absorption Newsletter,

16: 42-43.

77GLA 03 E. S. Gladney and J. W. Owens (1977) Determination of Mercury by Carrier-Free Combustion

Separation and Flameless Atomic Absorption Spectrometry, AnalyticB Chimica Acta, 90: 271-274.

77GLU 01 H. J. Gluskoter, R. Ruch, W. Miller, R. Cahill, G. Dreher, and J. Kuhn (1977), Trace Elements in Coal: Occurrence and

Distribution, Illinois State Geological Survey circular 499.

77G0O 01 G. C. Goode, J. Herrington, and P. C. Goddard (1977) Neutron Activation Analysis for Aluninium in Bone and Tissue

Samples, Radiochemical and Radioanalytical Letters,

31: 87-94.

77GU! 02 V. P. Guinn and D. A. Miller (1977) Recent Instrunental Neutron Activation Analysis Studies Utilizing Very Short-lived Activities, Journal of Radioanalytical Chemistry, 37: 313-324.

77GUI 03 V. P. Guinn, E. R. Christensen, and K. de Lancey (1977) Neutron Activation Analysis Trace Element Studies in Connection with the Offshore Drilling for Oil, in 77V0G 01,

pp. 303-311.

77GUL 01 B. L. Gulson (1977) Isotopic and Geochemical Studies on Crustal Effects in the Genesis of the Woodlaun Pb-Zn-Cu Deposit, Contributions to Mineralogy and Petrology, 65: 227-242.

77GUZ 01 G. Guzzi, A. Colombo, F. Girardi, R. Pietra, G. Rossi, and

N. Toussaint (1977), Comparison of Various Analytical

Techniques for Homogeneity Test of Candidate Standard Reference Materials, Journal of Radioanalytical Chemistry,

39: 263-275.

77HAM 01 H. Namaguchi, Y. Nunata, S. Iwata, M. Koyama, K. Sasajima,

Y. Katayama, T. Takeuchi, M. Shinogi, T. Mamuro, Y. kusaka,

H. Tsuji, T. Tamari, T. Sagawa, S. Ohmori, S. Nagatsuka,

Y. Tanizaki, T. Susuki, K. Tomurs, Y. Hashimoto, S. Bando, and T. Imahashi (1977), Precision of Neutron Activation

Analysis for Envi rormental Biological Materials, Bunseki Kagaku, 26: T23-T28.

77HAM 04 L. G. Hambleton (1977) Semiautomated Method for Simultaneous Determination of Phosphorus, Calciun, and Crude Protein in Animal Feeds, Journal of the Association of Official Analytical Chemists,

60: 845-852.

77HAN 02 M. A. Haney (1977) Title Unknown, Journal of Forensic Science, 22: 534; taken from 80KAN 01.

77HEY 01 K. Heydorn, Z. Z. Skanborg, R. Gowzdz, J. 0. Schmidt, and

M. E. Uacks (1977), Determination of Lithiun by Instrumental Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 37: 155-158.

77H0P 01 D. M. Hopkins (1977) An Improved Ion Selective Electrode Method for the Rapid Determination of Fluorine in Rocks and Soils, Journal of Research of the U.S. Geological Survey, 5: 589-593.

77IHN 01 M. Ihnat and H. J. Miller (1977) Acid Digestion, Hydride Evolution Atomic Absorption

Spectrophotometric Method for Determining Arsenic and Seleniun in Foods: Collaborative Study, Part I, Journal of the Association of Official Analytical Chemists,

50: 1414-1433.

77IHN 03 M. Ihnat and H. J. Miller (1977) Analysis of Foods for Arsenic and Seleniun by Acid Digestion

Hydride Evolution Atomic Absorption Spectrophotometry,

Journal of the Association of Official Analytical Chemists,

60: 813-825.

77JER 01 R. E. Jervis, B. Tiefenbach, and A. Chattopadhyay (1977) Scalp Hair as a Monitor of Population Exposure to Environmental Pollutants, Journal of Radioanalytical

Chemistry, 37: 751-760.

77JUR 01 E. T. Jurney, D. B. Curtis, and E. S. Gladney (1977) Determination of Sulfur in Environmental Materials by

Thermal Neutron Capture Prompt Ganrna-ray Spectrometry, Analytical Chemistry, 49: 1741-1743.

77JUR 02 H. Jurgensen and D. Behne (1977) Variations in Trace Element Concentrations in Hunan Blood

Serum in the Normal State Investigated by Instrimental Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 37: 375-382.

77KON 01 N. K. Konanur and G. W. van Loon (1977) Determination of Lead and Antimony in Firearm Discharge

Residues on Hands by Anodic Stripping Voltammetry, Talanta,

24: 184-187.

77KUS 01 Y. Kusaka, H. Tsuji, Y. Tamari, T. Sagawa, S. Ohmori,

S. Imai, and T. Ozaki (1977), Neutron Activation Analysis of

Biologically Essential Trace Elements in Environmental

Specimens using Pyrrol idinedithiocarbamate Extraction,

Journal of Radioanalytical Chemistry, 37: 917-925.

R-11
CODE N REFERENCE CODE N REFERENCE

77LAD 01 W. Ladrach and J. D. van der Laarse ^^977^) The Determination of Total Sulphur in Coal by a Semi -micro

Tube Combustion Method, Analytica Chimica Acta, 94: 213-216.

77LAN 01 J. Lange and H.-J. Brumsack (1977)

Total Sulphur Analysis in Geological and Biological Material

by Coulometric Titration Following Combustion, Fresenius Zeitschrift fur Analytische Chemie, 286: 361-366.

77LAU 01 J. C. Laul and L. A. Rancitelli (1977) Multielement Analysis by Sequential Instrumental and Radiochemical Neutron Activation, Journal of Radioanalytical

Chemistry, 38: 461-475.

77N1E 01 K. K. Nielson (1977) Matrix Corrections for Energy Dispersive X-ray Fluorescence Analysis of Environmental Samples with Coherent/Incoherent Scattered X-rays, Analytical Chemistry, 49: 641-648.

770HL 01 0. A. Ohlweiler and J. 0. Meditsch (1977) Determination of Silica in Silicates by Formation of 12-Molyljdosi I ieic Acid and Redox Titration of Molyixlenumdll), Talanta, 24: 652-654.

770MI 01 J. Omi and Y. Hashimoto (1977)

Post- Irradiation Chemistry of Seleniun in Neutron Activation

Analysis, Bunseki Kagaku, 26: 419-421.

77LAU 02 J. C. Laul, K. K. Nielson, and N. A. Wogman (1977) Trace Rare Earth Analysis by Neutron Activation and

Ganina- ray/X-ray Spectrometry, in 77V0G 01, pp. 198-209.

770SB 01 T. W. Osborn and W. B. Broering (1977) Neutron Activation Analysis in an Industrial Laboratory

using an Off-site Nuclear Reactor, in 77V0G 01, pp. 185-197.

77LIE 01 P. Lievens, J. Versieck, R. Cornelis, and J. Hoste (1977) The Distribution of Trace Elements in Normal Human Liver Determined by Semi -automated Radiochemical Neutron Activation Analysis, Journal of Radioanalytical Chemistry,

37: 483-496.

77L0R 01 D. A. Lord, J. W. McLaren, and R. C. Wheeler (1977) Determination of Trace Metals in Fresh Water Mussels by Atomic Absorption Spectrometry with Direct Solid Sample

Injection, Analytical Chemistry, 49: 257-261.

77HAE 01 U. Maenhaut and W. H. Zoller (1977) Determination of the Chemical Composition of the South Pole Aerosol by Instrtinental Neutron Activation Analysis, Journal

of Radioanalytical Chemistry, 37: 637-650.

77MAI 01 E. J. Mainethal (1977) Analysis of Botanical Standard Reference Materials by Cathode Ray Polarography, in 77MAV 01, pp. 91-105.

77MAV 01 R. Mavrodineanu, editor (1977) Procedures used at the National Bureau of Standards to Determine Selected Trace Elements in Biological and

Botanical Materials, NBS Special Publication 492.

77MEL 01 S. Meloni and M. T. Ganzerl i -Valentini (1977) New Improved Chemical Procedures in the Neutron Activation Analysis of Environmental Samples, in 77VOG 01, pp. 161-169.

77MIN 01 M. J. Hinski, C. A. Girling, and P. J. Peterson (1977) Determination of Gold and Arsenic in Plant Materials by

Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 30: 179-186.

77MIT 01 J. U. Mitchell, L. D. Blitzer, T. Y. Kometani, T. Gilts, and

L. Clark (1977), Homogeneously Doped Silica Matrices for

Trace Element Standards in Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 39: 335-342.

77MYR 01 D. R. Myron, S. H. Givartfi, and F. H. Nielsen (1977) VanadiLm Content of Selected Foods as Determined by

Flameless Atomic Absorption Spectroscopy, Journal of

Agricultural and Food Chemistry, 25: 297-300.

77NAD 01 R. A. Nadkarni and G. H. Morrison (1977) Neutron Activation Determination of Noble Metals using a

Selective Group Separation Scheme, Journal of Radioanalytical Chemistry, 38: 435-449.

77NAD 02 R. A. Nadkerni (1977) Multielement Analysis of Biological Standards by Neutron

Activation Analysis, Radiochemical and Radioanalytical

Letters, 30: 329-340.

77PAC 01 Petrol. Assoc. Conserv. Can. Envir. (1977) Title Unknown, PACE report no. 77-5; taken from 78BER 02.

77PAU 01 P. J. Paulsen (1977)

SF>ark Source Mass Spectrometric Isotope Dilution Determination of Cd, Cu, Fe, Pb, Hg, Mo, Ni, Se, Ag, Te,

Tl, and 2n, in 77MAV 01, pp. 33-48.

77PIL 01 A. Pilate, P. Geladi, and F. Adams (1977) Determination of AlLfniniun in Aerosols by Flameless Atomic Absorption Spectrometry, Talanta, 24: 512-514.

77P00 01 C. F. Poole, N. J. Evans, and D. G. Wibberley (1977) Determination of Seleniun in Biological Samples by

Gas-liquid Chromatography with Electron Capture Detection,

Journal of Chromatography, 136: 73-83.

77RAI 01 R. M. Raie and H. Smith (1977) The Determination of Selenium in Biological Material by

Thermal Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 28: 215-220.

77RIN 01 H. A. van Rinsvelt, R. D. Lear, and U. R. Adams (1977) Human Diseases and Trace Elements: Investigations by Proton

Induced X-ray Emission, Nuclear Instrunents and Methods,

142: 171-180.

77R00 01 H. L. Rook (1977)

The Determination of Iodine in Biological and Environmental Standard Reference Materials, Journal of Radioanalytical

Chemistry, 39: 351-358.

77R00 02 H. L. Rook (1977)

Rapid, Quantitative Separation for the Determination of Seleniun using Neutron Activation Analysis, in 77MAV 01,

pp. 26-32.

77R0W 03 J. J. Rowe and E. Steinnes (1977) Instrunental Activation Analysis of Coal and Fly Ash with

Thermal and Epithermal Neutrons, Journal of Radioanalytical

Chemistry, 37: 849-856.

77R0W 04 J. J. Rowe and E. Steinnes (1977) Determination of 30 Elements in Coal and Fly Ash by Thermal

and Epithermal Neutron Activation Analysis, Talanta, 24: 433

77SEG 01 C. Segebade (1977) Simultane Bestirmung von N, Mg, Si, P, und K in

Pf lanzenmaterial durch 14 MeV-Neutronenaktivierungs analyse

Fresenius Zeitschrift fur Analytische Chemie, 284: 23-29.

R-12
CODE N REFERENCE CODE N REFERENCE

77SHE 02 D. A. Shearer and R. 0. CLoutier (1977) Chelate Extraction and Flame Atomic Absorption Spectroinetric Determination of Nanogram Amounts of Manganese in Blood and

Animal Tissue, Journal of the Association of Official Analytical Chemists, 60: 155-159.

77SHU 01 G. T. C. Shum, H. C. Freeman, and J. F. Uthe (1977) Flameless Atomic Absorption Spectrophotometry of Selenium

in Fish and food Products, Journal of the Association of Official Analytical Chemists, 60: 1010-10U.

77SIE 01 0. 0. Siemer, R. K. Viteic, P. ICoteel, and W. Houser (1977) Determination of Arsenic in Beverages and Foods by Hydride Generation Atomic Absorption Spectrometry, Analytical

Letters, 10: 357-369.

77SMI 01 R. G. Smith, J. van Loon, J. Knechtel, J. Fraser, A. Pitts, and A. Hodges (1977), A Simple and Rapid Hydride Generation

Atomic Absorption Method for the Determination of Arsenic in Biological, Environmental, and Geological Samples, Analytica

Chimica Acta, 93: 61-67.

77SMI 04 J. Smits and R. van Grieken (1977) Optimization of a Simple Spotting Procedure for X-ray

Fluorescence Analysis of Waters, Analytica Chimica Acta,

88: 97-107.

77SMI 05 F. Smith, A. McMurtrie, and H. Galbraith (1977)

Ion Chromatographic Determination of Sulfur and Chlorine

using Milligram and Submilligram Sample Weights, Microchemical Journal, 22: 45-49.

77SMY 01 W. R. Smythe (1977) Private Communication, University of Colorado; taken from

77RIN 01.

77STE 02 R. Stella, N. Genova, and M. di Casa (1977) Halogen Determination in Vegetable NBS Standard Reference

Materials: Fluorine by Isotope Dilution; Chlorine, Bromine

and Iodine by Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 30: 65-74.

77TAG 01 M. Taguchi, K. Yasuda, Y. Dokiya, and M. Shimizu (1977) Mercury Determination in Fish Samples by Flameless Atomic Absorption Spectrometry: Sampling and Wet Digestion,

Bunseki Kagaku, 26: 438-441.

77TAM 01 K. H. Tam and H. B. S. Conacher (1977)

The Suitability of the Dry Ashing Procedure for Determination of Arsenic in Marine Samples, Journal of Environmental Science and Health, B12: 213-227.

77TIL 01 J. H. Tillman (1977)

A Combustimetric Method for Determining the Total Carbon

Content of Geological Materials, Journal of Research of the

U.S. Geological Survey, 5: 583-587.

77TJI 01 P. S. Tjioe, J. J. M. de Goeij, and J. P. W. Houtman (1977) Extended Automated Separation Techniques in Destructive

Neutron Activation Analysis: Application to Various

Biological Materials, Including Hunan Tissues and Blood,

Journal of Radioanalytical Chemistry, 37: 511-522.

77TR0 01 G. Troll, A. Farzaneh, and K. Canmann (1977) Rapid Determination of Fluoride in Mineral and Rock Samples

using an Ion Selective Electrode, Chemical Geology, 20: 295.

77TSU 01 K. Tsunoda, K. Fujiwara, and K. Fuwa (1977) Subnanogram Fluorine Determination by Aluminim Monofluoride

Molecular Absorption Spectrometry, Analytical Chemistry,

49: 2035-2039.

77UCH 02 T. Uchida, I. Kojima, and C. lida (1977) "One-drop Method" in Flame Atomic Absorption Spectrometry,

Bunseki Kegaku, 26: T44-T47.

77VAN 01 C. VandecBSteele, R. Kieffer, and J. Hoste (1977) Activation Analysis with Cyclotron-Produced Fast Neutrons Application to Instrumental Multielement Analysis and to the Padiochemical Determination of Fluorine, Journal of Radioanalytical Chemistry, 37: 25S-265.

77V0B 01 M. Vobeczky, L. Pavlik, and J. Benes (1977) Nondestructive Neutron Activation Assay of Submicrogram

Quantities of Selenium, Radiochemical and Radioanalytical

Letters, 29: 159-164.

77V0G 01 J. R. Vogt, editor (1977) Proceedings of the Third International Conference on Nuclear

Methods in Environmental and Energy Research, Columbia,

Missouri, CONF-771072.

77VAT 02 G. R. Waterbgry (1977) Written Conuiunication, Group CMB-1, Los Alamos Scientific

Laboratory, Los Alamos, New Mexico.

77WIC 01 U. A. Wicks and R. W. Burke (1977) Determination of Beryllium by Fluorescence Spectrometry,

in 77WAV 01, pp. 85-89.

77WIL 01 D. R. Williams and J. S. Hislop (1977) The Nondestructive Determination of Iodine in Soils and Biological Materials by High Energy Gamma-Photon Activation,

Journal of Radioanalytical Chemistry, 39: 359-373.

77WIL 02 R. D. Willis end R. L. Halter (1977) Computer Analysis of Proton Induced X-ray Emission Spectra, Nuclear Instrunents and Methods, 142: 231-242.

77WIL 03 R. D. Willis, R. Walter, R. Shaw, and U. Gutknecht (1977) Proton- Induced X-ray Emission Analysis of Thick and Thin

Targets, Nuclear Instrunents and Methods, 142: 67-77.

77YAN 01 Y. Yano, N. Odaka, S. Takei , and K. Nagashima (1977) Determination of Trace Heavy Metals in Environmental Samples

with Special Reference to Lead in Plants, Bunseki Kagaku,

26: T25-T29.

77YAS 01 K. Yasuda, M. Taguchi, S. Tamura, and S. Toda (1977) Determination of Selenium in Biological Ssnples by Solvent Extraction-Graphite Furnace Atomic Absorption Spectrometry,

Bunseki Kagaku, 26: 442-445.

77YAS 02 A. Yasui and C. Tsutsumi (1977) Adaptability of Wet Decomposition Method to Food Samples

for the Determination of Arsenic by Arsine Generation-Atomic Absorption Spectrophotometry, Bunseki Kagaku, 26: 809-814.

77ZIK 01 I. Zikovsky end E. A. Schweikert (1977) Comparison of Nondestructive Proton and Neutron Activation:

The Case of Biological Samples, Journal of Radioanalytical

Chemistry, 37: 571-580.

78ALL 04 R. 0. Allen and E. Steinnes (1978) Determination of Vanadiun in Biological Materials by Radiochemical Neutron Activation Analysis, Analytical

Chemistry, 50: 1553-1555.

78BEA 01 R. D. Beaty and M. M. Cooksey (1978)

The Influence of Furnace Conditions on Matrix Effects in

Graphite Furnace Atomic Absorption, Atomic Absorption

Newsletter, 17: 53-58.

R-13
CODE N REFERENCE CODL N REFERENCE

78BEH 01 D. Behne end H. Jurgensen (1978) Oetermination of Trace Elements in Hunan 6lood Serum and in the Standard Reference Material "Bovine Liver" by

Instrunental Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 42: 447-453.

78BER 01 C. Bergerioux and L. Zilcovsky (1978) Instrumental Neutron Activation Analysis of Brewer's Yeast, Journal of Radioanalytical Chemistry, 47: 173-179.

78EGA 01 E. Egaas and K. Julshatm (1978)

A Method for the Determination of Seleniun and Mercury in Fish Products using the Same Digestion Procedure, Atomic Absorption Newsletter, 17: 135-138.

78EPS 01 M. S. Epstein, T. C. Rains, T. J. Brady, J. R. Moore, and

I. L. Barnes (1978), Determination of Several Trace Metals

in Simulated Fresh Water by Graphite Furnace Atomic Emission

Spectrometry, Analytical Chemistry, 50: 874-880.

78BER 02 C. Bergerioux and L. Zikovsky (1978) Determination of 18 Trace Elements in Petroleun and its Derivatives by Neutron Activation with a Small Nuclear

Reactor, Journal of Radioanalytical Chemistry, 46: 277-284.

78EVA 01 W. H. Evans, J. I. Read, and B. E. Lucas (1978) Evaluation of a Method for the Determination of Total

Cd, Pb, and Ni in Foodstuffs using Measurement by Flame Atomic Absorption Spectrophotometry, Analyst, 103: 580-591.

78BYR 01 A. R. Byrne and L. Kosta (1978) Determination of Vanadiun in Biological Materials at Nanogram Level by Neutron Activation Analysts, Journal of Radioanalytical Chemistry, 44: 247-264.78FLA 01 J. Flanjak (1978) Atomic Absorption Spectrometric Determination of Arsenic and Seleniun in Offal and Fish by Hydride Generation, Journal of the Association of Official Analytical Chemists, 61: 1299.

78CAM 02 J. A. Campbell, J. Laul, K. Nielson, and R. Smith (1978) Separation and Chemical Characterization of Finely-sized

Flyash Particles, Analytical Chemistry, 50: 1032-1040.

78CAP 01 S. G. Capar, J. Tanner, M. Frie<*iian, and K. Boyer (1978) Multielement Analysis of Animal Feed, Animal Wastes, and Sewage Sludge, Environmental Science and Technology,

12: 785-790.

78FUD 01 N. Fudagaua and A. Kawase (1978) Determination of Nickel by Graphite Tiiie Furnace Atomic Absorption Spectrometry: Application to Nickel Determination

in Plant Materials, Bunseki Kagaku, 27: 37-42.

78FUR 01 A. K. Furr, B. A. Roscoe, and T. F. Parkinson (1978) VAT-69: A Software System for Ganma Spectrometry,

in 78CAR 03, pp. 352-366.

78CAR 01 M. B. Carvalho and D. M. Hercules (1978) Trace Arsenic Determination by Volatilization and X-ray Photoelectron Spectroscopy, Analytical Chemistry, 50: 2030.

78CAR 02 J. A. Carter, D. Donahue, J. Franklin, and R. Walker (1978) Trace Impurities in Coal and Fly Ash by Isotope Dilution

Mass Spectrometry, in 78KAR 01, pp. 403-420.

78CAR 03 B. S. Carpenter, D. D'Agostino, and H. Yule, editors (1978) Computers in Activation Analysis and Ganma- ray Spectroscopy,

Proceedings of the American Nuclear Society, Mayaguez, Puerto Rico, CONF-780421.

78C0O 01 K. A. Cook and E. R. Grahma (1978) Title Unknown, Soil Science Society of America Journal,

42: 57; taken from 80KOS 02.

780AH 01 R. L. Dahlquist and J. W. Knoll (1978) Inductively Coupled Plasma Atomic Emission Spectrometry:

Analysis of Biological Materials and Soils for Major, Trace,

and Ultra-trace Elements, Applied Spectroscopy, 32: 1-29.

78DAV 01 P. H. Davis, G. R. Dulude, R. M. Griffin, W. R. Matson, and

E. W. Zink (1978), Determination of Total Arsenic at the Nanogram Level by High-speed Anodic Stripping Voltanmetry,

Analytical Chemistry, 50: 137-143.

780ER 01 M. Dermelj, J. Novak, V. Ravnik, and L. <osta (1978) Rapid Determination of Uraniun at the Nanogram Level in

Geological and Biological Materials, Journal of Radioanalytical Chemistry, 44: 271-277.

7800G 01 S. Dogan and W. Haerdi (1978) Preconcentration on Silver Wool of Volatile Organo- mercury

Compounds in Natural Waters and Air and the Determination of

Mercury, International Journal of Environmental Analytical

Chemistry, 5: 157.

78EDI 01 R. D. Ediger, A. Knott, G. Peterson, and R. Beaty (1978)

The Determination of Phosphours by Atomic Absorption using

the Graphite Furnace, Atomic Absorption Newsletter, 17: 28.

78GAI 01 T. P. Gaines and G. A. Mitchell (1978) Sample Preparation by Colimn Elution for Elemental Analysis

of Plant Tissue, Journal of the Association of Official Analytical Chemists, 61: 1179-1181.

78GAL 01 M. Gallorini, R. R. Greenberg, and T. E. Gills (1978) Simultaneous Oetermination of As, Sb, Cd, Cr, Cu, and Se

in Environmental Materials by Radiochemical Neutron Activation Analysis, Analytical Chemistry, 50: 1479-1481.

78GAN 01 S. Gangadharan and S. Yegnasubramanian (1978) Elemental Characterization through Instrumental Neutron

Activation, Journal of Radioanalytical Chemistry, 42: 455.

78GEL 01 R. Geladi and F. Adams (1978) The Determination of Cadniun, Copper, Iron, Lead, ana Zinc

in Aerosols by Atomic Absorption Spectrometry, Analytica

Chimica Acta, 96: 229-241.

78GIL 01 T. E. Gills, H. Gallorini, and H. L. Rook (1978)

The Determination of Trace Elements in New Food Grain SRM's using Neutron Activation Analysis, Journal of

Radioanalytical Chemistry, 46: 21-25.

78GLA 01 E. S. Gladney, W. K. Hensley, and H. M. Minor (1978)

Comparison of Three Techniques for the Measurement of Depleted Uranium in Soils, Analytical Chemistry, 50: 652.

78GLA 02 E. S. Gladney (1978) Determination of Arsenic, Antimony, Molybdemm, Thoriun, and

Tungsten in Silicates by Thermal Neutron Activation and

Inorganic Ion Exchange, Analytical Letters, All: 429-435.

78GLA 04 E. S. Gladney, D. B. Curtis, and E. T. Jurney (1978)

Multielement Analysis of Major and Minor Elements by

Thermal Neutron Induced Capture Gamma- ray Spectrometry,

Journal of Radioanalytical Chemistry, 46: 299-308.

R-14
CODE N REFERENCE CODE N REFERENCE

78G0E CI J. J. M. de Goeij, K. Volkers, P. Tjioe, and J. Kroon (1978)

NBS SRM 1569 Brewer's Yeast: Is it an Adequate Standard

Reference Material for Testing a Chromiuni Determination in Biological Materials?, Radiochemical and Radioanalytical

Letters, 35: 139-U6.

78K0B 01 K. Kobayashi and K. Kudo (1978) Determination of In, Cu, and Ni in Glassmaking Materials

and NBS Standard Reference Materials by Substoichiometric Radioactivation Analysis, Journal of Radioanalytical

Chemistry, 46: 265-276.

78G0E 03 J. J. M. de Goeij and C. Zegers (1978) Determination of Seleniun in BCR Single Cell Protein via Destructive Neutron Activation Analysis, Interuni versi tai

r

Reactor Instituut report 133-78-11 (Delft).

78G0R 01 D. T. Gordon (1978) Atomic Absorption Spectrometric and Colorimetric Determination of Iron in Seafoods, Journal of the Association of Official Analytical Chemists, 61: 715-719.

78GR0 01 Z. Grobenski, M. Melcher, and B. Welz (1978) Richtigkeit bei der Bestiiimung von Spurenelementen in Lebensmitteln mit der Graphitrohrtechnik AAS, Fresenius Zeitschrift fur Analytische Chemie, 290: U't-145.

78GU1 01 R. J. Guidoboni (1978) Spark-source Mass Spectrometry and Atomic Absorption

Spectrometry for the Determination of Trace Elements

in Coal, in 78KAR 01, pp. 421-434.

78HAY 01 B. W. Haynes (1978) Electothermal Atomic Absorption Determination of Arsenic

and Antimony in Combustable Municipal Solid Waste, Atomic Absorption Newsletter, 17: 49-52.

78HIR 01 S. Hirai, S. Suzuki, and M. Okamoto (1978) Determination of Seleniim in Biological Materials by Neutron Activation Analysis using Se-77m, Bunseki Kagaku, 27: 435.

78K0R 01 G. A. Korbe and E. S. Yeung (1978) Application of Fabry-perot Interferometry in Multielement

Flame Emission Analysis, Analytica Chimica Acta, 99: 209-216

78KUB 01 H. Kubo, R. Bernthal, and T. R. Wi Ideman (1978) Energy Dispersive X-ray Fluorescence Spectrometric Determination of Trace Elements in Oil Samples, Analytical

Chemistry, 50: 899-903.

78KUB 02 T. Kubota and T. Ueda (1978) Atomic Absorption Spectrophotometric Determination of Antimony with use of Borohydride Solution as Reductant,

Bunseki Kagaku, 27: 692-696.

78LAU 02 J. C. Laul, C. L. Wilkerson, and V. L. Crow (1978) Computer Methodology and its Applications to Geological and Environmental Matrices, in 78CAR 03, pp. 840-856.

78LIN 01 H. R. Linder, H. D. Seltner, and B. Schreiber (1978) Use of Dibenzyldithiocarbamate as Coprecipi tant in the Routine Determination of 12 Heavy Metals in Pharmaceuticals

by X-ray Fluorescence Spectroscopy, Analytical Chemistry,

50: 896-899.

78MAC 01 K. W. MacHurdo and W. W. Bowman (1978) Automated Absolute Activation Analysis with Cal iforniLiii-252 Sources, Report DP- 1457, Savannah River Laboratory, E. I. Dupont de Nemours and Company.

78HIS 01 J. S. Hislop (1978) Gamma Activation Analysis: An Appraisal, Proceedings of the Analytical Division of the Chemical Society (London),

15: 193-205.

78HUD 01 V. Hudnik, S. Gomiscek, and M. Katie (1978) Title Unknown, Vestn. Slov. Kem. Durs., 25: 391; Taken from

80KOS 02.

78JAC 01 C. J. Jackson, D. Porter, A. Dennis, and P. Stockwell (1978) Automated Digestion and Extraction Apparatus for use in the Determination of Trace Metals in Foodstuffs, Analyst,

103: 317-331.

78J0L 01 R. K. Jolly, J. Kane, D. Buckle, G. Randers-Pehrson, W. Teoh and H. Aceto (1978), A Target Chamber for PIXE Analysis

using Micorampere Beams of 4 MeV Protons, Nuclear

Instrunents and Methods, 151: 183-188.

78KAR 01 C. Karr, editor (1978) Analytical Methods for Coal and Coal Products, Vol. 1, Academic Press, New York.

78KAT 01 K. Kato (1978) Unpublished Data; Quoted in 78MAS 01.

78KEL 02 M. T. Kelly, J. E. Riley, and G. Gleason (1978) NAALSQ: A Program for Neutron Activation Analysis with Least Squares Deconvolution of the Gamma Spectra on a Minicomputer

in 78CAR 03, pp. 456-464.

78KN0 01 A. C. Knott, J. C. Mills, and C. B. Belcher (1978) Synthetic Calibration Standards for Optical Emission and X-ray Spectrometry, Canadian Journal of Spectroscopy,

23: 105-111.

7eMAS 01 K. Masimoto and N. Suzuki (1978) Selective Coincidence Spectrometry in the Nondestructive Determination of Nickel in Geological Materials with

High Energy Photon Activation Analysis, Journal of Radioanalytical Chemistry, 46: 121-135.

78MAT 01 M. Matthes, R. Flucht, and M. Stoeppter (1978) Beitrage zur Automat isierten Spurenanalyse, Fresenius Zeitschrift fur Analytische Chemic, 291: 20-26.

78MCC 01 L. T. McClendon (1978) Determination of Chromiun in Biological Matrices by Neutron

Activation: Application to Standard Reference Materials,

Journal of Radioanalytical Chemistry, 42: 85-91.

78MCG 01 J. R. McGinley, C. J. Stock, E. A. Schweikert, J. B. Cross,

R. Zeisler, and L. Zikovsky (1978), Nuclear and Atomic Activation with Heavy Ion Beams, Journal of Radioanalytical

Chemistry, 43: 559-573.

78MCK 01 D. M. McKown and J. S. Morris (1978) Rapid Measurement of Selenitm in Biological Samples using

InstrLmental Neutron Activation Analysis, Journal of

Radioanalytical Chemistry, 43: 411-420.

78M0R 01 A. E. Morgan and H. W. Werner (1978) Semiquantitative Analyses by Secondary Ion Mass Spectrometry

using One Fitting Parameter, Mikrochimica Acta (Wien),

1978 II: 31-50.

78NAD 01 R. A. Nadkarni and G. H. Morrison (1978) Determination of MolybdenLm by Neutron Activation and

Srafion NMRR Ion Exchange Resin Separation, Analytical

Chemistry, 50: 294-296.

R-15
REFERENCE CODE N REFERENCE

78NA0 02 R. A. Nadkarni and G. H. Morrison (1978) Use of Standard Reference Materials as Multielement

Irradiation Standards in Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 43: 347-369.

78TER 01 S. Terashima (1978) Rapid Determination of Total Carbon and Sulfur in Geological Materials by Combustion and Infrared Absorption Photometry,

Analytica Chimica Acta, 101: 25-31.

78NA< 01 R. Nakashima (1978) UHF-Plasma Torch Emission Spectrometry for Catiniim, Lead, and Zinc by Vaporization Introduction, Bunseki Kagaku,

27: 199-203.

78TSU 01 K. Tsunoda, K. Fujiwara, and K. Fuwa (1978) Determination of Chlorine and Bromine by Molecular Absorption of Aluninium Monohalides at High Temperature, Analytical Chemistry, 50: 861-865.

78PEL 01 P. A. Pel la, K. E. Lorber, and K. F. J. Heinrich (1978) Energy-Dispersive X-ray Spectrometric Analysis of Environmental Samples after Borate Fusion, Analytical

Chemistry, 50: 1268-1271.

78UEM 01 Y. J. Uemura, Y. Kuno, H. Koyama, and T. Yamazaki (1978)

A New Way of Determining Concentrations in PIXE Trace Element Analysis, Nuclear Instrunents and Methods,

153: 573-579.

78PIE 01 Z. Pietrzak-Fi Is, G. L. Rehnberg, M. J. Favor, D. F. Cahill

arxi J. W. Laskey (1978), Chronic Ingestion of Cadmiun and/or

Tritiijn in Rats: I. Accumulation and Distribution of Catinium

in Two Generations, Environmental Research, 16: 9-17.

78RIT 01 C. Ritter, S. Bergman, C. Cothern, and E. Zamierowski (1978) Comparison of Sample Preparation Techniques for Atomic Absorption Analysis of Sewage Sludge and Soil, Atomic Absorption Newsletter, 17: 70-72.

78RYA 01 D. E. Ryan, D. C. Stuart, and A. Chattopadhyay (1978) Rapid Multielement Neutron Activation Analysis with a SLOWPOKE Reactor, Analytica Chimica Acta, 100: 87-93.

78SIE 01 D. D. Siemer and H. Hei (1978) Determination of Lead in Rocks and Glasses by Temperature Controlled Graphite Cup Atomic Absorption Spectrometry,

Analytical Chemistry, 50: 147-151.

78SIM 01 P. C. Sims (1978) Preprint, Purdue University Accelerator Laboratory; taken from 84NAD 02.

78SMI 01 R. G. Smith (1978) Sources of Copper and Cadniun Contamination in Small Biological Samples, Talanta, 25: 173-175.

78STA 02 P. Standzenieks, A. Rindby, and E. Selin (1978) Development of Low Power Monoenergetic X-ray Tube for Trace

Element Analysis, Nuclear Instruments and Methods, 153: 269.

78SUD 01 R. F. Suddendorf and K. W. Boyer (1978) Nebulizer for Analysis of High Salt Content Samples with Inductively Coupled Plasma Emission Spectrometry, Analytical

Chemistry, 50: 1769-1771.

78SUG 01 A. Sugimae and R. K. Skogerboe (1978) Dual Approach to the Emission Spectrograph ic Determination

of Elements in Airborne Particulate Matter, Analytica

Chimica Acta, 97: 1-11.

78URE 01 A. M. Ure and J. R. Bacon (1978)

Scandiuti, Yttriun, and Rare Earth Content of Water Lily, Geochimica et Cosmochimica Acta, 42: 651-652.

78URE 02 A. M. Ure, M. P. Hernandez-Artiga, and M. C. Mitchell (1978)

A Carbon-rod Atomizer for the Determination of Cadmiun and Lead in Plant Materials and Soil Extracts, Analytica Chimica

Acta, 96: 37-43.

78VAL 01 I. Valente, M. J. Minski, and H. J. M. Bowen (1978) Rapid Determination of Sb in Biological ar>d Environmental Samples using instrunental Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 45: 417-421.

78VIS 01 R. D. Vis, K. J. Wiederspahn, and H. Verheul (1978) The Determination of the Elemental Composition of Glasses

for Forensic Application using a Combination of Proton

Induced X-ray Emission and Inelastic Proton Scattering,

Journal of Radioanalytical Chemistry, 45: 407-416.

78WAN 01 L. E. Wangen and E. S. Gladney (1978) Determination of Arsenic and Galliim in Standard Materials by Instrunental Epithermal Neutron Activation Analysis,

Analytica Chimica Acta, 96: 271-277.

78WEA 01 J. N. Weaver (1978) Neutron Activation Analysis of Trace Elements in Coal, Fly Ash, and Fuel Oils, in 78KAR 01, pp. 377-401.

78WEE 01 C. A. Weers, K. Hoede, and H. A. Das (1978) Application of Selective Evaporation in the Determination of

As and Br in Dry Biological Material by Thermal Neutron Activation Analysis, Journal of Radioanalytical Chemistry,

42: 113-119.

78WEG 01 U. Wegscheider, K. E. Lorber, and K. MuUer (1978) Quantitative Intermethod Comparison of Energy Dispersive

, X-ray Fluorescence and Atomic Absorption Spectrometry for

the Analysis of Urban Dusts and Fly Ash, International

Journal of Environmental Analytical Chemistry, 5: 171-187.

78SUG 02 A. Sugimae (1978) Determination of Trace Amounts of Rare Earth Elements in Various Environmental Sarrples by Spark Source Mass Spectrography, Bunseki Kagaku, 27: 169-174.

78SZY 01 F. J. SzydloHski (1978) Use of Branch Capillary for Ionization Buffer Addition in

Flame Atomic Absorption Spectrometric Determination of Sodiim and Potassium in Food Products, Atomic Absorption

Newsletter, 17: 65-69.

78TAK 01 T. Takamatsu (1978) Multielement Analysis of Rock and Sediment Samples by

Nondispersive X-ray Fluorescence, Bunseki Kagaku,

27: 193-198.

78WEL 01 B. Welz and M. Melcher (1978)

Bestirtinung von Arsen und Selen in Korperf lussigkeiten und

Geweben mit der Hydrid-methode, Fresenius Zeitschrift fur

Analytische Chemie, 290: 106-107.

79ABE 01 F. N. Abercrombie, M. 0. Silvester, and R. B. Cruz (1979) Simultaneous Multielement Analysis of Biologically Related

Samples with RF-ICP, in 79RIS 01, pp. 10-25.

79AB0 01 M. 0. K. Abo-Rady (1979) Schwermetal Ibestimmung in zwei Biologischen und zwei

Geologischen Standards mit Hilfe der Atom- Absorptions

Spectroskopie, Fresenius Zeitschrift fur Analytische Chemie,

296: 380-382.

R-16
CODE N REFERENCE CODE N REFERENCE

7VABU 01 J. Abukawa, H. Higuchi, K. Sato, and S. Bando (1979)

A Comparison of Various Methods for Determination of Cobalt

in Marine Biological Materials, Bunseki Kagaku, 28: S06-508.

7VAHM 01 S. Ahmed, M. S. Chaudhry, and I. H. Oureshi (1979) Determination of Toxic Elements in Tobacco Products by

Instrunentel Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 54: 331-341.

79AND 01 D. L. Anderson, M. failey, W. ZoUer, and G. Gordon (1979) Neutron Capture Prompt Gamna-rey Activation Analysis: Multielement Measurements on Various Materials, in 79CHR 01,

pp. 546-548.

79BAR 03 R. M. Barnes, editor (1979) Applications of Plasma Emission Spectrochemistry, Heyden,

Phi ladelphia.

79BEN 01 G. E. Bentley, L. Markowitz, and R. Meglen (1979) Analysis of Molybdenun in Biological Materials, in 79RIS 01,

pp. 35-39.

79BL0 01 A. J. Blotcky, C. Falcone, V. A. Medina, E. P. Rack, and

D. W. Hobson (1979), Determination of Trace Level Vanadium

in Marine Biological Samples by Chemical Neutron Activation

Analysis, Analytical Chemistry, 51: 178-182.

79B0G 01 S. Bogdanski, I. Shakir, W. Stephen, and A. Townshend (1979) Determination of Trace Amounts of Sulphate by Molecular

Emission Cavity Analysis using a Vaporization System, Analyst, 104: 886-890.

79BRA 01 F. P. Brauer and R. S. Strebin (1979) Title Unknown, in Nuclear Activation Techniques in the Life

Sciences, IAEA, Vienna, p. 27; Taken from 80GVA 01.

79BRE 01 J. J. la Brecque (1979) Interferences in the Determination of Titanium in Silicate

Rocks and Venezuelan Laterites by Atomic Absorption

Spectroscopy, Applied Spectroscopy, 33: 389-393.

79BRE 02 J. J. la Brecque (1979) Decomposition and Determination of Aliminium and Silicon in Venezuelan Laterites by Atomic Absorption Spectroscopy,

Chemical Geology, 26: 321-329.

79BRI 02 C. Brihaye (1979) Analyse dc Traces par la Methode Electrochimique Utilisant

une Electrode Disque-Anneau, Doctoral Thesis, University of Liege, Belgium (1979-1980).

79BYR 01 A. R. Byrne (1979) Extraction of Some Trace Elements as Iodides with

Methyl isobutyl Ketone and its Applications in Neutron Activation Analysis, Radiochemical and Radioanalytical

Letters, 40: 1-16.

79CAH 01 R. A. Cahill (1979) Private Conmunication, Illinois State Geological Survey.

79CHA 02 A. Chattopadhyay, K. M. Ellis, and K. N. de Silva (1979) Title Unknown, in Nuclear Activation Techniques in the Life

Sciences, IAEA, Vienna, pp. 667-682; Taken from 79IAE 01.

79CHA 04 A. Chattopadhyay and K. N. de Silva (1979) Pseudo-Cyclic Neutron Activation Analysis of Ag, F, Rb, Sc, and Se in Biological Samples, Transactions of the American

Nuclear Society, 32: 185-186.

79CHR 01 R. E. Chrien and U. R. Kane, editors (1979) Neutron Capture Gamma- ray Spectroscopy, Plenun Press, New York.

79C00 01 M. Cooksey and U. B. Barnett (1979) Sequential Multielement Atomic Absorption Analysis of Agricultural Samples, Atomic Absorption Newsletter, 18: 1-4.

79C0R 01 R. Cornelis, L. Mees, J. Hoste, J. Ryckenbusch, J. Versieck,

and F. Barbier (1979), Title Unknown, in Nuclear Techniques

in the Life Sciences 1978, IAEA, Vienna, p. 165; Taken from 80HEY 01.

79CR0 01 J. D. Cross and H. Smith (1979) The Determination of Bromine in Biological (Material by

Thermal Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 48: 191-196.

79DAB 01 R. U. Dabeka, A. D. McKenzie, and H. Conacher (1979) Microdiffusion and Fluoride Specific Electrode Determination

of Fluoride in Foods, Journal of the Association of Official Analytical Chemists, 62: 1065-1068.

790AB 02 R. W. Dabeka (1979) Graphite Furnace Atomic Absorption Spectrometric Determination of Lead and Cadmium in Foods after Solvent Extraction and Stripping, Analytical Chemistry, 51: 902-907.

79DAL 01 L. S. Dale (1979) The Emission Spectrograph ic Determination of Boron in Silicate Materials, Applied Spectroscopy, 33: 404-406.

790AS 01 H. A. Das, A. Faanhof, end H. A. van der Sloot (1979) Errors in Instrunental Neutron Activation Analysis:

I. Determination of the Peak Area, Journal of Radioanalytical Chemistry, 54: 289-301.

790ER 01 M. Dermelj, A. Vakselj, V. Ravnik, and B. Smodis (1979) Applicability of Carbamate Extraction to Radiochemical Separation and Determination of Cd, Co, Cu, and 2n in Various Biosphere Samples, Radiocnemical and Radioanalytical

Letters, 41: 149-160.

790ES 01 H. B. Desai, R. K. Iyer, and S. R. Kayasth (1979) Precipitation of Mercury as Zinc Mercuro-thiocyonate,

Application to Activation Analysis, Radiochemical and Radioanalytical Letters, 41: 299-306.

79EDI 01 R. D. Ediger and D. L. Wilson (1979) The Performance of an Inductively Coupled Plasma on the Model 5000 Atomic Absorption Spectrophotometer, Atomic Absorption Newsletter, 18: 41-45.

79EPS 01 M. Epstein, S. Nikdel, N. Omenetto, R. Reeves, J. Bradshaw, and J. Winefordner (1979), Inductively Coupled Argon Plasma

as an Excitation Source for Flame Atomic Fluorescence Spectrometry, Analytical Chemistry, 51: 2071-2077.

79EPS 03 M. S. Epstein and A. T. Zander (1979) Direct Determination of Bariun in Sea and Estuarine Water by

Graphite Furnace Atomic Spectrometry, Analytical Chemistry,

51: 915-918.

79EVA 01 W. H. Evans, F. J. Jackson, and D. Dellar (1979) Evaluation of a Method for Determination of Total Antimony,

Arsenic, and Tin in Foodstuffs using Measurement by Atomic

Absorption Spectrophotometry with Atomization in a Silica

Tube using the Hydride Generation Technique, Analyst,

104: 16-30.

R-17
CODE N REFERENCE CODE N REFERENCE

79FAA 01 A. Faanhof and H. A. Das (1979) Analysis of Tobacco by Instrumental Epithermal Neutron Activation Analysis, Radiochemical and Radioanalytical

Letters, 41: 367-374.

79FAI 01 M. P. Failey, 0. Anderson, W. Zoller, G. Gordon, and

R. Lindstrom (1979), Neutron-capture Prompt Gamma-ray Activation Analysis for Multielement Determination in Complex Samples, Analytical Chemistry, 51: 2209-2221.

79FEL 01 C. Feldman (1979) Improvements in the Arsine Accumulation-Hel iun Glow detector Procedure for Determining Traces of Arsenic,

Analytical Chemistry, 51: 564-669.

79FLA 0^ J. Flanjak and H. Y. Lee (1979) Trace Metal Content of Livers and Kidneys of Cattle, Journal

of Agricultural Science and Food Chemistry, 30: 503-507.

'/9FRE 01 G. Frechette, J. Hebert, T. Thinh, R. Rousseau, and

F. Claisse (1979), X-ray Fluorescence Analysis of Cements, Analytical Chemistry, 51: 957-961.

79FRU 01 J. S. Fruchter and M. R. Petersen (1979) Environmental Characterization of Products and Effluents

from Coal Conversion Processes, in 79ICAR 01, pp. 247-275.

79GEL 01 P. Geladi and F. Adams (1979) The Determination of Beryllitm end Manganese in Aerosols by

Atomic Absorption Spectrometry with Electrothermal

Atomization, Analytica Chimica Acta, 105: 219-231.

79GIA 01 R. D. Giauque, R. B. Garrett, and L. Y. Goda (1979) Determination of Trace Elements in Light Element Matrices

by X-ray Fluorescence Spectrometry with Incoherent Scattered Radiation as an Internal Standard, Analytical Chemistry,

51: 511-516.

79GIA 03 R. 0. Giauque (1979) Private Communication, Lawrence Berkeley Laboratory.

79GLA 02 E. S. Gladney and D. R. Perrin (1979) Determination of Bromine in Biological, Soil, and Geoloflical Standard Reference Materials by Instrumental Epithermal Neutron Activation, Analytical Chemistry, 51: 2015-2018.

79GLA 03 E. S. Gladney and D. R. Perrin (1979) Quantitative Analysis of Silicates by Instrumental Epithermal Neutron Activation using (n,p) Reactions,

Analytical Chemistry, 51: 2297-2300.

79GLA 04 E. S. Gladney, D. B. Curtis, and E. T. Jurney (1979) Simultaneous Determination of Nitrogen, Carbon, and Hydrogen

by Thermal Neutron Prompt Ganma-ray Spectrometry, Analytica

Chimica Acta, 110: 339-343.

79G0D 01 W. C. Godbeer and D. J. Swaine (1979) Cadmium in Coal and Fly Ash, in Trace Substances in Envirormental Health-XIII, D. D. Hem^jhill (editor),

University of Missouri, ColLinbis.

79GRE 01 R. R. Greenberg (1979) Trace Element Characterization of the NBS Urban Particulate

Matter Standard Reference Material by Instrumental Neutron Activation Analysis, Analytical Chemistry, 51: 2004-2006.

79HEC 01 M. H. Heckman (1979) Analysis of Foods for Iodine: Interlaboratory Study, Journal

of the Association of Official Analytical Chemists, 62: 1045

79HEI 03 H. Heinrichs (1979) Determination of Lead in Geological and Biologicat Materials

by Graphite Furnace Atomic Absorption Spectrometry, Fresenius Zeitschrift fur Anslytische Chemie, 295: 355-361.

79HEI 04 J. Heinonen (1979) Assurance and Control of Quality in Trace Element Analysis,

in 79IAE 01, pp. 7-25.

79HER 01 J. L. Hern (1979) Elemental Analysis in Agriculture using IrKkictively Coupled

F>lasma Atomic Emission Spectroscopy, in 79BAR 03.

79HIL 01 E. P. Milliard and J. D. Smith (1979) Minimun Sample Preparation for the Determination of Ten Elements in Pig Faeces and Feeds by Atomic Absorption

Spectrophotometry and A Spectrophotometric Procedure for Total Phosphorus, Analyst, 104: 313-322.

79H0E 01 D. Hoede and H. A. van der Sloot (1979) Application of Hydride Generation for the Determination of Antimony and Arsenic in Biological Material by Neutron Activation Analysis, Analytica Chimica Acta, 111: 321-325.

79H0E 02 M. Hoenig, P. van Hoeyweghen, and J. Liboton (1979) Evaluation a I 'aide d'etalons Internationaux de Deux Hethodes de Mineralisation des Vegetaux, Analusis, 7: 104.

79IAE 01 International Atomic Energy Agency (1979) Proceedings of an International Symposiim on Nuclear Activation Techniques in the Life Sciences held by the IAEA in Vienna, Hay 1978, STI/PUB/492, ISBN 92-0-010079-1.

79IMA 01 A. Imahori, I. Fukushima, S. Shiobara, Y. Yanagida, and

K. Tomure (1979), Multielement Neutron Activation Analysis

of Human Scalp Hair: A Local Population Survey in the Tokyo

Metropolitan Area, Journal of Radioanalytical Chemistry,

52: 167-180.

79IMA 03 A. Imahori, I. Fukushima, S. Shiobara, K. Tomura, M. Suzuki,

M. Yukawa, and M. Terai (1979), A Study of Trace Element Concentrations in Hunan Hair of Some Local Populations in Japan, in 791AE 01, pp. 563-571.

79INU 01 T. Inui, N. Fudagawa, and A. Kawase (1979) Extraction and Atomic Absorption Spectrometric Determination

of Bismuth with Electrothermal Atomization, Fresenius Zeitschrift fur Analytische Chemie, 299: 190-193.

79JER 01 R. E. Jervis and B. Tiefenbach (1979) Arsenic Accunulation in People Working Uith and Living Near

a Gold Smelter, in 79IAE 01, pp. 627-642.

79J0N 01 J. D. Jones, P. B. Kaufman, and U. L. Rigot (1979) Method for Determination of Silicon in Plant Materials by Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 50: 261-275.

79KAN 02 Y. Kanda and N. Suzuki (1979) Redox Substoichiometric Determination of Arsenic in

Biological Materials by Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 54: 7-14.

79KAR 01 C. Karr (1979) Analytical Method for Coal and Coal Products, Academic Press

New York, Vol. III.

79KNE 01 J. R. Knechtel and J. L. Fraser (1979)

Uet Digestion Method for the Determination of Mercury in

Biological and Environmental Samples, Analytical Chemistry,

51: 315-317.

R-18
CODE N REFERENCE COOE N REFERENCE

79IC0B 01 K. Koboysshi and K. Kudo <1979) Rapid Determination of In, Ni, and Cu in NBS Standard Reference Material by Substoichiometric Radioactivetion

Analysis, Journal of Radioanalytical Chemistry, 54: 49-58.

79MC0 02 N. R. McQuaker, D. F. Brown, and P. D. Kluckner (1979) Digestion of Environmental Materials for Analysis by

Inductively Coupled Plasma Atomic Emission Spectrometry, Analytical Chemistry, 51: 10821084.

79K0B 03 K. Kobayashi and K. Kudo (1979) Determination of Multielement in ojjtical Waveguide and Standard Reference Materials by Instrumental Neutron Activation Analysis, Journal of Radioanalytical Chemistry,

53: 233-246.

79HEN 01 E. Meridelovici, J. J. LaBrecque, and R. E. Villelba (1979) Calciim and Magnesiun Determirwtion in Silicates end Venezuelan Laterites by Atomic Absorption Spectroscopy: Interference Studies in the Fluoboric - Boric Acid Matrix, Chemical Geology, 24: 199-209.

79KRA 01 J. A. Krasowski and T. R. Copeland (1979) Matrix Interferences in Furnace Atomic Absorption

Spectrometry, Analytical Chemistry, 51: 1843-1849.

79KUC 01 J. Kucera (1979) Epithermal Neutron Activation Analysis of Trace Elements in Biological Materials, Radiochemical and Radioanalytical

Letters, 38: 229-246.

79KUE 01 E. C. Kuehner and P. A. Pella (1979) Energy-Dispersive X-ray Spectrometric Analysis of NBS Standard Reference Material 1571 Orchard Leaves after Oxidation and Borate Fusion, Applied Spectroscopy, 33: 632.

79LAK 01 E. L. Lakomaa and P. Eklund (1979) Trace Element Analysis of Hunan Cataractous Lenses by Neutron Activation Analysis and Atomic Absorption

Spectrometry, in 79IAE 01, pp. 333-343.

79LIK 01 W. Likussar (1979) Untersuchungen uber das Morpholin-N-dtthio-carbonsaure

Morphotiniim (MDCM) als Reagens in der Quantitativen

Analytik.X, Mikrochimica Acta (Wien), 197911: 43-52.

79L0C 01 J. Locke (1979) The Determination of Eight Elements in Hunan Liver Tissue by

Flame Atomic Absorption Spectrometry in Sulphuric Acid

Solution, Analytica Chimica Acta, 104: 225-231.

79LP1 01 Lunar and Planetary Institute (1979) Proceedings of the Tenth Lunar and Planetary Science

Conference, Houston, Texas; Geochimica et Cosmochimica

Acta Supplement 11.

79MAN 01 N. F. Mangelson, M. Hill, K. Neilson, D. Eatough, R. Izatt,

J. Christensen, and D. Richards (1979), Proton Induced X-ray

Emission Analysis of Pima Indian Autopsy Tissues, Analytical

Chemistry, 51: 1187-1194.

79MAT 01 K. Matsunoto and K. Fuwa (1979) Major and Trace Element Determination in Geological and Biological Satiples by Energy-Dispersive X-ray Fluorescence

Spectrometry, Analytical Chemistry, 51: 2355-2358.

79MAT 02 T. D. Mathews, J. Boyne, R. Davis, and D. Simnons (1979) The Distribution of Copper and Iron in South Carolina

Oysters, Journal of Environmental Science and Health,

A14: 683-694.

79MAT 01 S. May and D. Piccot (1979) Dosages de Traces D'Elements Toxiques (As, Cd, Hg, Sb, Se) dans les Proteines Synthetiques, par Radioactivetion

Neutronique, Analusis, 7: 133-137.

79MER 01 R. N. Merryfield and R. C. Loyd (1979) Simultaneous Determination of Metals in Oil by Inductively

Coupled Plasma Emission Spectrometry, Analytical Chemistry,

51: 1965-1968.

79MIL 01 R. J. Miller and D. J. Ingle (1979) Unpublished Data; Taken from 81MAR 01.

79MIZ 01 A. Mizuike and A. lino (1979) Coating of Borosilicate Glass Containers for Preventing Contamination in Trace Element Analysis, Analytica Chimica

Acta, 111: 251-256.

79M0N 01 J. R. Montgomery and M. T. Price (1979) Release of Trace Metals by Sewage Sludge and the Subsequent

Uptake by Members of a Turtle Grass Mangrove Ecosystem, Environmental Science and Technology, 13: 546-549.

79NAR 01 H. Narasaki (1979) ^

Determination of Cadmiun in Polished Rice by Low- temperature

Ashing and Atomic Absorption Spectrometry, Anaytica Chimica

Acta, 104: 393-395.

79NIC 01 L. W. Nicholson and K. Rengen (1979) Determination of Arsenic in Some Lake Michigan Fish using Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 54: 355-360.

790RV 01 E. Orvini and R. Delfanti (1979) Determination of Arsenic at Nanogram Level in Biological Tissues by Radiochemical Activation Analysis, Radiochemical

and Radioanalytical Letters, 37: 199-206.

79PAV 02 L. Pavlik, J. Kalouskova, M. Vobecky, J. Dedina, J. Benes, and J. Parizek (1979), Seleniun Levels in the Kidneys of Male and Female Rats, in 79IAE 01, pp. 213-223.

79PEA 01 S. Peats (1979) Determination of Arsenic in Seaweed and Related Products by Atomic Absorption Spectrophotometry using the MHS-10 Hydride Generation System, Atomic Absorption Newsletter, 18: 118-120

79PET 01 P. Peterson, C. Girling, D. Klumpp, and M. Minski (1979) Title Unknown, in Nuclear Activation Techniques in the Life

Sciences, IAEA, Vienna, p. 103; Taken from 80K0S 02.

79PLA 01 L.-O. Plantin (1979) Trace Elements in Cardiovascular Diseases, in 79IAE 01,

pp. 321-330.

79PRA 01 J. W. Prather, J. A. Guin, and A. R. Tarrer (1979)

X-ray Fluorescence Analysis of Trace Elements in Coal and

Solvent Refined Coal, in 79KAR 01, pp. 357-369.

79MCQ 01 N. R. McQuaker, P. D. Kluckner, and G. N. Chang (1979) Calibration of an Inductively Coupled Plasma Atomic Emission Spectrometer for the Analysis of Environmental

Materials, Analytical Chemistry, 51: 888-895.

79RAI 01 R. H. Raie and H. Smith (1979)

The Determination of Seleniun in Biological Materials by

Thermal Neutron Activation Analysis end Atomic Absorption

Spectrometry, Journal of Radioanalytical Chemistry,

48: 185-190.

R-19
CODE N REFERENCE CODE N REFERENCE

79REE 01 J. Reednick (1979)

A Unique Approach to Atomic Spectroscopy: High Energy Plasma Excitation and High Resolution Spectrometry, American

Laboratory, 11: 53-62.

79REI 01 J. E. O'Reilly and D. G. Hicks (1979) Slurry-Injection Atomic Absorption Spectrometry for Analysis

of Whole Coal, Analytical Chemistry, 51: 1905-1915.

79REN 01 K. Rengan, J. P. Haushalter, and J. D. Jones (1979) Simultaneous Determination of Arsenic and Antimony in Environmental Samples by Radiochemical Neutron Activation

Analysis, Journal of Radioanalytical Chemistry, 54: 347-353.

79REN 02 H. J. Renan (1979) The Determination of Elements Not Previously Certified in International Biological Reference Materials, Radiochemical and Radioanalytical Letters, 40: 87-102.

79REN 03 M. J. Renan, B. Drennan, R. Keddy, and J. Sellschop (1979) Oesophageal Cancer in the Transkei: Determination of Trace Element Concentrations in Selected Plant Material by INAA,

in 79IAE 01, pp. 479-494.

79RIS 01 T. H. Risby, editor (1979) Ultratrace Metal Analysis in Biological Sciences and Environment, Advances in Chemistry Series, American Chemical Society, Washington, D. C.

79R0B 01 W. B. Robbins, J. A. Caruso, and F. L. Fricke (1979) Determination of Ge, As, Se, Sn, and Sb in Complex Samples

by Hydride Generation - Microwave- induced Plasma Atomic Emission Spectrometry, Analyst, 104: 34-40.

79R0S 02 R. J. Rosenberg (1979) Radiochemical Activation Analysis of Arsenic, Seleniun, and Antimony in Biological Sairples, Journal of Radioanalytical

Chemistry, 50: 109-114.

79R0S 03 G. Rossi and A. Colombo (1979) Reference Materials for Chemical Analysis: Highlights on the Activity of JRC-ISPRA Laboratories, Fresenius Zeitschrift

fur Analytische Chemie, 297: 13-17.

79SAT 01 T. Sato and T. Kato (1979) Determination of Trace Elements in Various Organs of Rats by Thermal Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 53: 181-190.

79SCH 02 H. Schorin (1979) Quantitative Determination of Si, Al, Ti, and Fe in Laterite

and Bauxites by X-ray Fluorescence using a Computer for Correction of Interelement Effects, Applied Spectroscopy,

33: 634-637.

79SIL 01 D. Silberman and G. L. Fisher (1979)

Room- Temperature Dissolution of Coal Fly Ash for Trace Metal Analysis by Atomic Absorption, Analytica Chimica Acta,

106: 299-307.

79SMI 01 R. D. Smith, J. A. Campbell, and K. K. Nielsen (1979) Concentration Dependence upon Particle Size of Volatilized

Elements in Fly Ash, Environmental Science and Technology,

13: 553-560.

79STE 01 E. Steinnes (1979) Instrumental Activation Analysis of Coal and Coal Ash with

Thermal and Epi thermal Neutrons, in 79KAR 01, pp. 279-302.

R79ST0 01 M. Stoeppler, P. Valenta, and H. W. Nurnberg (1979) Application of Independent Methods and Standard Materials: An Effective Approach to Reliable Trace and Ultratrace

Analysis of Metals and Metalloids in Environmental and Biological Matrices, Fresenius Zeitschrift fur Analytische

Chemie, 297: 22-34.

79SZy 01 F. J. Szydlowski (1979) Boron in Natural Waters by Atomic Absorption Spectrometry

with Electrothermal Atomization, Analytica Chimica Acta,

106: 121-125.

79SZY 02 F. J. Szydlowski and D. L. Dunmire (1979) Semi-automatic Digestion and Automatic Analysis for Selenium

in Animal Feeds, Analytica Chimica Acta, 105: 445-449.

79TAG 01 M. Taguchi, K. Yasuda, M. Hashimoto, and S. Toda (1979) Some Inprovements for Mercury Determination in Marine Organisms by Atomic Absorption Spectrometry, Bunseki Kagaku,

28: T33-T38.

79TAM 01 Y. Tamari, K. Hiraki, and Y. Nishikawa (1979) Fluorometric Determination of Seleniun in Sediments with 2,3-Diaminonaphthalene, Bunseki Kagaku, 28: 164-169.

79TJI 01 P. Tjioe, J. de Goeij, and K. Volkers (1979)

A Routine Chromium Determination in Biological Materials: Application to Various Reference Materials and Standard Reference Materials, Interuniversitair Reactor Instituut report 133-79-02 (Delft).

79ULL 01 A. H. Ullman, B. Pollard, G. Boutillier, R. Bateh, P. Hanley

and J. Wincfordner (1979), Conputer-Control led Multielement Atomic Emission/Fluorescence Spectrometer System, Analytical

Chemistry, 51: 2382-2387.

79UNR 01 D. M. Unruh, R. Hutchison, and M. Tatsumoto (1979) U-Th-Pb Age of the Barwell Condrite: Anatomy of a "Discordant" Meteorite, in 79LPI 01, pp. 1011-1030.

79VEI 01 C. Veillon, W. R. Wolf, and B. E. Guthrie (1979) Determination of Chromitm in Biological Materials by Stable

Isotope Oi lution, Analytical Chemistry, 51: 1022-1024.

79VER 01 J. Versieck, J. Hoste, J. de Rudder, F. Barbier, and

L. Vanbal lent>erghe (1979), Determination of Chromium in Bowen's Kale, NBS Bovine Liver, and Brewers Yeast, Before

and After Dry Ashing, Analytical Letters, 12: 555-562.

79VIJ 01 P. N. Vijan (1979) Determination of Antimony Jn Environmental Samples by AA, American Laboratory, 11: 32-43.

79V0B 01 M. Vobecky, J. Dedina, L. Pavlik, and J. Valasek (1979) Gamma-ray Interferences in the Determination of Seleniun by

the INAA Method, Radiochemical and Radioanalytical Letters,

38: 197-204.

79WAR 01 N. 1. Ward, R. Stephens, and D. E. Ryan (1979) Comparison of Three Analytical Methods for the Determination

of Trace Elements in Whole Blood, Analytica Chimica Acta,

110: 9-19.

79WAR 02 N. I. Ward and D. E. Ryan (1979) Multielement Analysis of Blood for Trace Metals by Neutron

Activation Analysis, Analytica Chimica Acta, 105: 185-197.

79WAT 02 J. H. Watkinson (1979)

Semi -automated Fluorometric Determination of Nanogram

Quantities of Selenium in Biological Material, Analytica

Chimica Acta, 105: 319-325.
CODE REFERENCE REFERENCE

79WEG 0) W. Wegscheider, G. Kn»pp, and H. Spitzy (1979)

Sequential Testinj as an Efficient Screening Method for

Interferences in Routine Analysis as Applied to Atomic

Absorption Spectrometry with Flame and Graphite Furnace

Atomization, Talanta, 26: 25-31.

80BER 02 C. Berserioux and W. Haerdi (1980) Coprecipi tation of Dissolved Trace Elements with Coufcint-d Organic Precipitating Reagents for use in X-ray Fluorescence

Analysis: I. 1 , 10-Phenanthrol in and Tetraphenyl Boron, Analusis, 8: 169-173.

79WES 01 M. H. Uest. J. F. Molina, C. L. Yuan, and D. G. Davis (1979) Determination of Metals in Uaters and Organic Materials by

Flameless Atcnic Absorption Spectrometry with a Wire Loop

Atomizer, Analtyical Chemistry, 51: 2370-2375.

80BRA 01 P. Bratter and P. Schremel, editors (1980) Trace Element Analytical Chemistry in Medicine arxJ Biology,

Proceedings of the First International Workshop, Neuherberg,

Federal Republic of Germany, W. de Gruyter, Berlin.

79YAN 01 M. H. rang, C. L. Tseng, and G. Tolg (1979) Determination of Small Amounts of Boron by Radiation Decomposition of Chloroacetic Acid Solution, Talanta,

26: 705-711.

80BRE 01 I. Brenner, A. Watson, G. Russell, and M. Goncalves (1980) A New Approach to the Determination of the Major and Minor Constituents in Silicate and Phosphate Roclcs, Chemical

Geology, 28: 321-330.

79YAS 01 K. Yasuda, S. Toda, C. Igarashi, and S. Tamura (1979) Extraction System for Solvent Extraction-Graphite furnace Atomic Absorption Spectrometry, Analytical Chemistry,

51: 161-163.

79ZE! 01 R. Zeisler, F. Lux, and H. Seidenberger (1979) Studies on the Distribution of Platinun in Tunor-Bearing

Rats after the Administration of Pt Coordination Complexes used in Cancer Chemotherapy, in 79IAE 01, pp. 467-476.

80AGE 01 H. Agemian, D. P. Sturtevant, and K. D. Austen (1980) Simultaneous Acid Extraction of Six Trace Metals from Fish Tissue by Hot-Block Digestion and Determination by Atomic Absorption Spectrometry, Analyst, 105: 125-130.

80AGE 02 H. Agemian and R. Thompson (1980) Simple Semi -automated Atomic Absorption Spectrometric

Method for the Determination of Arsenic and Selenium in

Fish Tissue, Analyst, 105: 902-907.

80AGE 03 H. Agemian and E. Bedek (1980)

A Semi -automated Method for the Determination of Total Arsenic and Selenium in Soils and Sediments, Analytica

Chimica Acta, 119: 323-330.

80AHM 01 S. Ahmad, M. S. Chaudhary, and I. H. Qureshi (1980) Determination of Rare Earths in Low Grade Uraniun Ores and

SRM Rock by Instrunental Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 57: 185-193.

80AN0 01 D. L. Anderson, M. Fai ley, G. Gordon, and W. Zoller (1980) Instrumental Prompt Gaimia Activation Analysis of Energy Related Samples and Standards, Fourth International Conference on Nuclear Methods in Environmental and Energy

Research, University of Missouri, preprint.

80ANO 01 Anonymous (1980) LECO CR-12 Carbon Determinator, LEGO Corporation, St. Joseph

Michigan.

80ARO 01 H. S. Arora, C. Pugh, L. Hossner, and J. Dixon (1980)

Forms of Sulfur in East Texas Lignitic Coal, Journal of Environmental Quality, 9: 383-386.

80AUG 01 J. H. Augustson, J. W. Haynes, and T. W. Sanders (1980) The Determination of Uranium in Biological Materials by Neutron Activation Analysis using the Fission Product 1-134,

Journal of Radioanalytical Chemistry, 60: 373-383.

SOBER 01 C. Berthelot, G. Carraro, and V. Verdingh (1980) Non-destructive Multielement Photon Activation Analysis of

River Sediments, Journal of Radioanalytical Chemistry,

60: 443-451.

80BUA 01 P. Buat-Menard, C. Lambert, M. Arnold, and R. Chesselet

(1980), Multielement Neutron Activation Analysis Towards the Geochemistry of Particulate Matter Exchange Between

Continent-Atmosphere-Ocean, Journal of Radioanalytical

Chemistry, 55: 445-452.

80BYR 01 A. R. Byrne (1980) Unpublished Data; taken from 80XOS 02.

80CAN 01 C. E. Cann and S. G. Prussin (1980) Radiochemical Determination of Short-Lived Radionuclides in Neutron Activated Biological Samples, International Journal

of Applied Radiation and Isotopes, 31: 446-447.

80CAS 01 V. R. Casella, C. Bishop, A. Glosby, and C. Phillips (1980) Radiochemical Determination of Uraniun, Thoriun, and Pb-210

in Coal and Coal Ash: Redioelement Analysis: Progress and

Problems, Proceedings of the Twenty- third Conference on Analytical Chemistry in Energy Technology, W. S. Lyon (ed.), Ann Arbor Science Publishers, Ann Arbor, Michigan, p. 271.

80CHA 01 S. S. Chao and E. E. Pickett (1980) Trace Chroroiun Determination by Furnace Atomic Absorption

Spectrometry Following Enrichment by Extraction, Analytical

Chemistry, 52: 335-339.

80CHA 02 M. S. Chaudhary, S. Ahmad, and I. H. Qureshi (1980) Simultaneous Determination of Thorium and Uraniun in Ores and SRMS by Instrumental Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 57: 137-146.

80CHA 08 C. L. Chakrabarti, C. C. Wan, and W. C. Li (1960) Direct Determination of Traces of Copper, Zinc, Lead, Cobalt

Iron, and Cadmiim in Bovine Liver by Graphite Furnace Atomic Absorption Spectrometry using the Solid Sampling and the Platform Techniques, Spectrochimica Acta, 35B: 93-105.

80CHA 09 C. L. Chakrabarti, C. C. Wan, and W. C. Li (1980) Atomic Absorption Spectrometric Determination of Cd, Pb, 2n,

Cu, Co, and Fe in Oyster Tissue by Direct Atomization from

the Solid State using the Graphite Furnacs Platform Spectrochimica Acta, 35B: 547-560.

80CHR 01 J. D. Christensen and L. Kryger (1980) Reductive Potentiometric Stripping Analysis, Analytica

Chimica Acta, 118: 53-64.

80CLA 01 P. J. Clark, R. Zingaro, K. Irgolic, and A. McGinley (1980)

Arsenic and Selenium in Texas Lignite, International Journal

of Environmental Analytical Chemistry, 7: 295-314.

80CRE 01 E. A. Crecelius, E. A. Lepf^l , J. C. Laul, L. A. Rancitelli,

ar>d R. L. McKeever (1980), Background Air Particulate

Chemistry near Colstrip, Montana, Environmental Science and

Technology, 14: 422-428.

R-21
CODE N REFERENCE CODE N REFERENCE

80DAL 01 P. Dolheim (1980) Application of the Fundamental Parameter Model to Energy Dispersive X-ray Fluorescence Analysis of Complex Silicates, Advances in X-ray Analysis, New York, Plemm Press, 23: 71.

80DON 01 E. H. Donaldson (1980) Determination of Chroitiiun in Ores, Rocks, and Related

Materials, Iron, Steel, and Nonferrous Alloys by Atomic Absorption Spectrophotometry after Separation by

Tribenzylamine-Chloroform Extraction, Talenta, 27: 779-786.

80DOR 01 A. Dornemann and H. Kleist (1980) Bestiimung von Nanospuren Nickel in Biologischem Matrix, Fresenius Zeitschrift fur Analytische Chemie, 300: 197-199.

80DSI 01 A. P. D'Silva, G. U. Rice, and V. A. Fassel (1980) Atmospheric Pressure Active Nitrogen (APAN) - A New Source

for Analytical Spectroscopy, Applied Spectroscopy, 3A: 578.

80DUM 01 R. Dunarey, R. Heindryckx, and R. Dams (1980) Determination of Mercury in Environmental Standard Reference Materials by Pyrolysis, Analytics Chimica Acta, 118: 381-383

80FUD 01 N. Fudagawa and A. Kawase (1980) Determination of Cobalt in Plant Materials by Graphite

Furnace Atomic Absorption Spectrometry after Solvent Extraction, Bunseki Kagaku, 29: 6-11.

80GAL 02 M. Gallorini and E. Orvini (1980) The Role of Radiochemical Neutron Activation Analysis in Certifying Selected Trace Element Contents in Biological Related Matrices, in 80BRA 01, pp. 675-699.

80GAR 01 S. Garcia, U. Hensley, M. Minor, M. Denton, and M. Fuka

(1980), An Automated Multidetector System for Instrumental Neutron Activation Analysis of Geological and Environmental

Materials, Presented at the American Nuclear Society Meeting Puerto Rico.

SOGER 01 M. Germani, I. Gokmen, A. Sigleo, G. Kowalczyk, I. Olmez,

A. Small, D. Anderson, M. Failey, M. Gulovali, C. Choquette,

E. Lepel, G. Gordon, and U. Zoller (1980), Concentrations of Elements in the National Bureau of Standards' Bitiminous and Subbituninous Coal Standard Reference Materials, Analytical

Chemistry, 52: 240-245.

80DUP 01 S. Dupire and M. Hoenig (1980) Influence des Matrices Complexes sur la Determination des Elements en Trace, Analusis, 8: 153-158.

80DYC 01 P. M. van Dyck and R. W. van Grieken (1980) Absorption Correction via Scattered Radiation in Energy Dispersive X-ray Fluorescence Analysis for Samples of Variable Composition and Thickness, Analytical Chemistry,

52: 1859-1864.

80EDO 01 B. T. Eddy, J. I. W. Watterson, and C. S. Erasmus (1980) Preparation of Synthetic Standards for use in Instrimental Neutron Activation Analysis, Geostandards Newsletter, 4: 229

80EPS 01 M. S. Epstein and J. D. Winefordner (1980) Precision and Linearity of Determinations at High Concentrations in Atomic Absorption Spectrometry with Horizontal Rotation of the Burner, Talanta, 27: 177-180.

80EPS 02 M. S. Epstein, J. Bradshaw, S. Bayer, J. Bower, E. Voigtman, and J. D. Winefordner (1980), Application of Laser-Excited

Atomic Fluorescence Spectrometry to the Determination of Nickel and Tin, Applied Spectroscopy, 34: 372-376.

80EP$ 03 M. S. Epstein, N. Omenetto, S. Nikdel, J. Bradshaw, and

J. D. Winefordner (1980), Inductively Coupled Plasma as an Excitation Source for Flame Atomic Fluorescence Spectrometry

Analytical Chemistry, 52: 284-287.

80EPS 04 M. S. Epstein, S. Bayer, J. Bradshaw, E. Voigtman, and

J. Winefordner (1980), Application of Laser-excited Atomic Fluorescence Spectrometry to the Determination of Iron, Spectrochimica Acta, 35B: 233-237.

80EVA 01 W. Evans, D. Dellar, B. Lucas, F. Jackson, and J. Read (1980) Observations on the Determination of Total Copper, Iron, Manganese, and Zinc in Foodstuffs by Flame Atomic Absorption

Spectrophotometry, Analyst, 105: 529-543.

80FAA 01 A. Faanhof, H. A. Das, and J. Zonderhuis (1980) Possibilities of the Elemental Analysis of Dry Biological

Material by Fast Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 56: 173-184.

80FLO 01 M. A. Floyd, V. A. Fassel, and A. P. D'Silva (1980) Computer-Controlled Scanning Monochrometer of the Determination of 50 Elements in Geochemical and Environmental Samples by Inductively Coupled Plasma-Atomic

Emission Spectrometry, Analytical Chemistry, 52: 21682173.

80GIN 01 J. H. van Ginkel and J. Sinnaeve (1980) Determination of Total Nitrogen in Plant Material with Nessler's Reagent by Continuous -Flow Analysis, Analyst,

105: 1199-1203.

80GLA 01 E. Gladney, D. Perrin, W. Hensley, and M. Bunker (1980) Uranium Content of 25 Silicate Reference Materials, Geostandards Newsletter, 4: 243-246.

80GLA 03 E. S. Gladney, D. Perrin, J. Balagna, and C. Warner (1980) Evaluation of a Boron-Fi Itered Epithermal Neutron Irradiation Facility, Analytical Chemistry, 52: 2128-2132.

80GLA 04 E. S. Gladney, D. R. Perrin, and W. K. Hensley (1980) Determination of Uraniun in NBS Biological Standard Reference Materials by Delayed Neutron Assay, Journal of Radioanalytical Chemistry, 59: 249-251.

80GRE 01 R. R. Greenberg (1980) Simultaneous Determination of Mercury and Cadnium in Biological Materials by Radiochemical Neutron Activation

Analysis, Analytical Chemistry, 52: 676-679.

80GVA 01 I. Gvardjancic, L. Kosta, and H. Dermelj (1980) Determination of Iodine in Reference Materials by Activation

Analysis, Journal of Radioanalytical Chemistry, 58: 359-365.

80HAA 01 W. J. Haas and V. A. Fassel (1980) Inductively Coupled Plasma Atomic Emission Spectroscopy, Elemental Analysis of Biological Materials, IAEA Technical Report series no. 197, pp. 167-199.

80HAN 01 R. Hanninen, J. Raisanen, and A. Anttila (1980) Elemental Analysis of Li and B with Proton Induced Gamma-ray Reactions, Radiochemical and Radioanalytical

Letters, 44: 201-206.

80HEN 01 W. M. Henry and K. T. Knapp (1980) Compound Forms of Fossil Fuel Fly Ash Emissions,

Envirormentel Science and Technology, 14: 450-456.

80HEY 01 K. Heydorn, E. Damsgaard, and B. Reitz (1980)

Systematic Differences in the Determination of Vanadiun in

Standard Reference Material 1571 Orchard Leaves, Analytical

Chemistry, 52: 1045-1049.

R-22
CODE N REFERENCE CODE N REFERENCE

80HIT 02 A. Hitchen and G. ZechanoMi tsch (1980) CheUtomctric Determination of Calcium aixi HagnesiLm in

Iron Ores, Slags, Anorthosite, Limestone, Cu-Ni -Pb-Zn Ores,

and Divers Materials, Talanta, 27: 269-275.

80H0E 01 D. Hoede, J. Zonderhuis, and H. A. Das (1980)

The Determination of Bromine in Dry Biological Material by

Instrumental Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 56: 199-202.

80HON 01 P. K. Hon, W. W. Lau, H. C. Cheung, and M. C. Wong (1980) Atomic Absorption Spectrometric Determination of As, Bi, Pb,

Sb, Se, and Sn with a Flame-Heated Silica T-Tube after Hydride Generation, Analytica Chimica Acta, 115: 355-359.

801 ID 01 C. lida, T. Uchida, and Decomposition of Bovine Determination of Metals

Analytica Chimica Acta,

I . Kojima (1980) Liver in a Sealed Teflon Vessel for by Atomic Absorption Spectrometry,

113: 365-368.

80IWA 01 Y. Iwata, K. Matsimoto, and K. Fuua (1980) Determination of Chroroiun in Rocics and Sediments by Energy

Dispersive X-ray fluorescence Spectrometry: Evaluation of the Effectiveness of Internal Standards and Briquetting

Samples, Bunseki Kagalcu, 29: 640-644.

80JAC 01 F. J. Jackson, J. I. Read, and B. E. Lucas (1980) Determination of Total Chromiun, Cobalt, and Silver in Foodstuffs by Flame Atomic Absorption Spectrophotometry,

Analyst, 105: 359-370.

80JAR 01 J. 0. Jarvisalo, J. Kilpio, and N.-E. L. Saris (1930) Toxicity of Cactnium to Renal Mitochondria when Administered

in Vivo and in Vitro, Environmental Research, 22: 217-223.

SOKAN 01 Y. Kanda, T. Oikaua, and T. Niwaguchi (1980) Multi -element Determination of Trace Elements in Glass by

Instrumental Photon Activation Analysis, Analytica Chimica

Acta, 121: 157-163.

80KAT 01 T. Kato and M. Kato (1980) Multielement Determination in Floor Sediments of the Japan

Sea by Nondestructive Photon Activation Analysis, Journal

of Radioanalytical Chemistry, 57: 105-112. '

80KHA 02 S. R. Khalil, D. U. Koppenaal, and W. D. Ehmann (1980) Oxygen Concentrations in Coal and Fly Ash StarxJards, Analytical Letters, 13: 1063-1071.

80K1R 01 S. J. Kirchner, H. Oona, S. Perron, Q. Fernando, J. Lee, and

H. Zeitlin (1980), Proton- Induced X-ray Emission Analysis of

Deep-sea Ferromanganese Nodules, Analytical Chemistry,

52: 2195-2201.

80KNA 01 D. Knab and E. S. Gladney (1980) Determination of Seleniun in Environmental Materials by Neutron Activation and Inorganic Ion Exchange, Analytical

Chemistry, 52: 825-828.

80ICOH 01 T.-S. Koh (1980) Microwave Drying of Biological Tissues for Trace Determination, Analytical Chemistry, 52: 1978-1979.

SOtCOP 01 0. W. Koppennal, R. Lett, F. Brown, and S. Manahan (1980) Determination of Ni, Cu, Se, Cd, Tl, and Pb in Coal Gassif ication Products by Isotope Dilution Spark Source Mass

Spectrometry, Analytical Chemistry, 52: 44-49.

80KOR 01 V. korunova and J. Dedina (1980) Determination of Trace Concentrations of Hg in Biological Materials after Digestion under Pressure in Nitric Acid Catalysed by Vanadiun Pentoxide, Analyst, 105: 48-51.

SOKOS 01 K. N. Kostadinov and R. G. Djingova (1980) Trace Element Investigation of Coal Samples by Thermal and Epithermal Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 45: 297-304.

80KOS 02 L. Kosta (1980) Reference Samples for Trace Elements in Biological Materials

and Associated Analytical Problems, Elemental Analysis of Biological Materials: Current Problems and Techniques with Special Reference to Trace Elements, IAEA Technical Report series no. 197, Vienna, pp. 317-345.

80I(UL 01 A. I. Kulathilake and A. Chatt (1980) Determination of MolybdenLm in Sea and Estuarine Water with Beta-Naphthoin Oxime and Neutron Activation, Analytical

Chemistry, 52: 828-833.

SOIOJM 01 J. Kuipulainen (1980) Determination of Chromium in Hunan Milk and Urine by

Graphite Furnace Atomic Absorption Spectrometry, Analytica Chimica Acta, 113: 355-359.

80LAB 03 J. J. Labrecque and H. Schorin (1980) Analysis of the Major Constituents in Venezuelan Laterites:

A Con^^arison of Atomic Absorption, X-ray Fluorescence, and

Classical Methods, Applied Spectroscopy, 34: 39-43.

80LAK 01 E. L. Lakomaa (1980) Use of Neutron Activation Analysis in the Determination of Elements in Hunan Cerebrospinal Fluid, in 80BRA 01, p. 97.

80LAN 01 F. J. Langmyhr and U. Aadalen (1980) Direct Atomic Absorption Determination of Copper, Nickel, and Vanadium in Coal and Petroleim Coke, Analytica Chimica

Acta, 115: 365-368.

80LAU 01 0. W. Lau and S. F. Cham (1980) Spectrophotometric Determination of CalciLm with Chlorindazon C, Mikrochimica Acta (Wien), 19801: 465-474.

80LEG 01 P. A. Legotte, W. C. Rosa, and D. C. Sutton (1980) Determination of Cadniim and Lead in Urine and Other Biological Samples by Graphite Furnace Atomic Absorption

Spectrometry, Talanta, 27: 39-44.

80LON 01 B. Lonnerdal, M. Clegg, C. Keen, and L. Hurley (1980)

Effects of Wet Ashing Techniques on the Determination of

Trace Element Concentrations in Biological Samples,

in 80BRA 01, pp. 619-629.

80MAE 01 W. Maenhaut, L. de Reu, H. van Rinsvelt, J. Cafmeyer, and

P. van Espen (1980), Particle Induced X-ray Emission (PIXE) Analysis of Biological Materials: Precision, Accuracy, and Application to Cancer Tissues, Nuclear Instriments and

Methods, 168: 557-562.

80MCC 01 J. Mccormick (1980) Determination of Total Sulfur in Fuel Oils by Ion

Chromatography, Analytica Chimica Acta, 121: 233-238.

80MIC 01 R. Michel, J. Hofmann, and J. Zilkens (1980) Trace Element Behaviour of Hunan and Mammalian Tissues

During Excessive Supply of Metals, in 80BRA 01, p. 137.

R-23
CODE N REFERENCE CODE REFERENCE

80NAD 01 R. A. Nadkarni (1980)

Multi technique Multielement Analysis of Coal and Fly Ash, Analytical Chemistry, 52: 929-935.

80NAK 01 S. Nakainura, N. Fudagawa, and A. Kauase (19B0) Determination of Antimony in Plant Haterials by Zeeman

Atomic Absorption Spectrometry after Coprecipitation with Manganese Dioxide, Bunseki Kagaku, 29: 477-482.

80NEV 01 J. Neve, M. Hanocq, and L. Nolle (1980) Critical Study of Some Wet Digestion Methods for Deconposition of Biological Materials for the Determination of Total

Se and Se(VI), Mikrochimica Acta (Uien), 19801: 259-269.

80SCH 07 H. Schuenke and J. Knoth (1980) High-Sensitivity Multielement Trace Analysis using EDXRF Spectrometry with Multiple Total Reflection of the Exciting

Beam, in 80BRA 01, pp. 307-317.

80SCH 08 P. Schramel, A. Wolf, and B. J. Klose (1980) Analytical Pretreatment of Biological Material by

Wet Ashing Methods, in 80BRA 01, pp. 610-617.

80SEG 01 C. Segebade, H.-U. Fusban, and H.-P. Ueise (1980) Analysis of some Toxic Components of Environmental Samples

by High Energy Photon Activation, Journal of Radioanalytical

Chemistry, 59: 399-405.

80NOR 01 L. de Norre, J. op de Beeck, and J. Hoste (1980) Determination of Fluorine in Zinc Ores using an Isotope Neutron Source Based Automated Neutron Activation Analysis

System, Journal of Radioanalytical Chemistry, 59: 453-466.

80POL 01 J. E. Poldoski (1980) Determination of Pb and Cd in Fish and Clam Tissue by Atomic Absorption Spectrometry with a Mo and La Treated Pyrolytic

Graphite Atomizer, Analytical Chemistry, 52: 1147-1151.

80PRE 01 J. R. Preer, H. Sekhon, B. Stephens, and M. Collins (1980) Factors Affecting Heavy Metal Content of Garden Vegetables, Environmental Pollution, 1: 95-104.

80RAP 01 S. E. Raptis, W. Uegscheider, G. Knspp, and G. Tolg (1980) X-ray Fluorescence Determination of Trace Seleniun in Organic and Biological Matrices, Analytical Chemistry,

52: 1292-1296.

80RAP 02 S. Raptis, G. Knapp, A. Meyer, and G. Tolfl (1980)

. Systematische Fehler bei der Selenbcstimnung in NG/G-8ere1ch

in Biologischen Matrices nach dem Hydrid-AAS-Verfahren, Fresenius Zeitschrift fur Analytische Chemie, 300: 18-21.

80RAP 03 S. Raptis, W. Wegscheider, G. Knapp, and G. Tolg (1980) X-ray Fluorescence Determination of Traces of Selenius in Organic and Biological Matrices, Fresenius Zeitschrift fur Analytische Chemie, 301: 103.

80RIL 01 G. H. Riley and M. J. Korsch (1980) Natural Reactor Studies, in Proceedings of the International UraniLm Syirposium on the Pine Creek Geosyncline, IAEA, Vienna, pp. 407-416.

eOROS 01 K. J. R. Rosman and J. R. de Laeter (1980) Mass Spectrometric Isotope Dilution Determination of Cadniun in Geochemical Reference Samples, Geostandards

Newsletter, 4: 1-3.

80SAT 01 T. Sato end T. Kato (1980) Determination of Trace Elements in Subcellular Fractions Of

liver and Kidney from Monkey by Thermal Neutron Activation

Analysis, Radiochemical and Radioanalytical Letters,

42: 227-234.

80SCH 02 T. Schofield, E. Gladney, F. Miera, and P. Trujillo (1980) Comparative Determination of C, N, and H in Environmental Standard Reference Materials by Instrunental Conbustion

Analysis and Thermal Neutron Capture Gamma-ray Spectrometry

Analytical Letters, 13: 75-83.

BOSCH 05 P. Schramel, A. Wolf, R. Seif, and B.-J. Klose (1980)

Eine neue Apparatur zur Druckveraschung von Biologischem

Material, Fresenius Zeitschrift fur Analytische Chemie,

302: 62-64.

80SHI 01 T. Shigematsu and K. Kudo (1980) Substiochiometric Extraction of Chromium, Journal of Radioanalytical Chemistry, 59: 63-73.

80SL0 01 H. A. van der Sloot, G. Wals, C. Weers, and H. Das (1980) Simultaneous Elimination of Na-24, K-42, Br-82, and P-32 in the Determination of Trace Elements in Biological Materials

by Neutron Activation Analysis, Analytical Chemistry, 52:112

80SMI 01 G. R. Smith (1980) Rapid Determination of Total Sulfur in Plants and Soils by Combustion Sulfur Analysis, Analytical Letters, A13: 465-471

30ST0 02 T. R. Stolzenburg and A. W. Andren (1980)

A Simple Acid Digestion Method for the Determination of Ten Elements in Ambient Aerosols by Flame Atomic Absorption

Spectrometry, Analytica Chimica Acta, 118: 377-380.

80STU 01 0. Stulzaft, B. Haziere, and S. Ly (1980) Gatliun Determination in Biological Samples, Journal

of Radioanalytical Chemistry, 55: 291-295.

80SUZ 01 N. Suzuki, S. Nakamura, and H. Imura (1980) Substoichiometric Isotope Dilution Analysis of Iron in Biological Materials by the 8-Quinolinol Extraction, Journal

of Radioanalytical Chemistry, 57: 37-46.

80SUZ 02 M. Suzuki, Y. Dokiya, S. Yamazaki, and S. Toda (1980)

A New Type of Biological Reference Material for Multielement

Analysis: The Fungus Penicilliim Ochro-Chloron ATCC 36741, Analyst, 105: 944-949.

80SZY 01 F. J. Szydlowski, K. Monti, S. Michalak, and D. Dunmire

(1980), A Practical Voltanmetric Method for the Analysis of

Lead in Cereal and Feed Products using a Tubular Hg Thin

Film Electrode, Analytical Letters, A13: 529-542.

80TAM 01 G. K. H. Tam and G. LaCroix (1980) Determination of Arsenic in Urine and Feces by Dry Ashing,

Atomic Absorption Spectrometry, International Journal of

Environmental Analytical Chemistry, 8: 283-290.

80TON 01 S. L. Tong and W.-K. Leow (1980) Stationary Cold-Vapor Atomic Absorption Spectrometric

Attachment for Determination of Total Mercury in Undigested

Fish Samples, Analytical Chemistry, 52: 581-583.

80TOU 01 R. E. Tout and A. Chatt (1980)

A Critical Evaluation of Short-Lived and Long-Lived Neutron

Activation Products for Trace Element Determinations,

Analytica Chimica Acta, 118: 341-358.

80UCH 01 T. Uchida, I. Kojima, and C. lida (1980) Determination of Metals in Small Samples by Atomic

Absorption and Emission Spectrometry with Discrete

Nebulization, Analytica Chimica Acta, 116: 205-210.

R-24
CODE N REFERENCE CODE N REFERENCE

BOURE 01 A. H. Ure, G. J. Ewen, and M. C. Hitchell (1980)

A Three-channel Flame Atomic Absorption/Emission

Spectrometer for the Rapid, Routine Determination of Major

Cations in Soil Extracts and Plant Ash Solutions, Analytics

Chinica Acta, 118: 1-9.

80VAL 01 H. T. G. Valentini, N. Genova, and ft. Stella (1980) Determination of Cd, Cu, and Hg in Environmental Matrices by Destructive Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, M: 359-368.

80VER 01 J. Versieck, L. Vanbal lenberghe, G. Lemey, F. Barbier,

R. Cornells, and J. de Rudder (1980), Determination of Molybdenun in Serim, in 80BRA 01, pp. 273-282.

80V1J 01 P. N. Vijan and D. Leung (1980) Reduction of Chemical Interference and Speciation Studies

in the Hydride Generation-Atomic Absorption Method for Selenitn, Analytics Chimica Acta, 120: H1-146.

80V1R 01 H. S. Virk (1980) Intercalibration of Glass Dosimeters for Neutron Fluence Determination, International Jourrwl of Applied Radiation

and Isotopes, 31: 649-651.

80WAL 01 W. J. Walker and R. H. Dowdy (1980) Elemental Conposition of Barley and Ryegrass Grown on Acid

Soils Amended with Scrubber Sludge, Journal of Enviromientat

Quality, 9: 27-30.

80UAN 01 L. E. Wangen, E. S. Gladney, and U. K. Hensley (1980) Determination of Seleniim in Environmental Standard

Reference Materials by a Ganina-Ganina Coincidence Method

using Ge(Li) Detectors, Analytical Chemistry, 52: 765-767.

80WHI 01 L. E. White and M. H. Carter (1980) Determination of Mercury in Rocks, Sediments, and Soils by Flameless Atomic Absorption, Oak Ridge Y-12 Plant report

Y/DI(-254, Oak Ridge, Tennessee.

80WOI 01 J. R. W. Woittiez and H. A. Das (1980) Multielement Analysis by Neutron Activation to Short-Lived

Radionuclides with Previous Removal of Sodiim: Application

to Dry Biological Standard Materials, in 80BRA 01.

SOYAM 01 M. Yamashita and N. Suzuki (1980) Photon Activation Analysis of Trace Metals in Biological Materials via Collection of Metal Tropolone-5-Sulfonate

Complexes onto Ani on-Exchange Resin, Journal of Radioanalytical Chemistry, 60: 73-85.

80YAN 01 K. Yanagf (1980)

A New Procedure for Determining Arsenic in Natural Waters

by means of Atomic Absorption Spectrophotometry combined

with the Techniques of Arsine Evolution by Sodiim

Borohydride and of its Collection in a Trap of Liquid

Nitrogen, Bunseki Kagaku, 29: 194-198.

81AHM 01 S. Ahmad, M. S. Chaudhary, and 1. H. Qureshi (1981) Instrumental Neutron Activation Analysis of Obsidian Rock, Journal of Radioanalytical Chemistry, 67: 119-125.

81ALL 01 M. Allegini, K. W. Boyer, and J. T. Tanner (1981) Neutron Activation of Total Diet Food Composites for Iodine, Journal of the Association of Official Analytical

Chemists, 64: 1111-1115.

81ARA 01 N. M. Arafat and W. A. Glooschenko (1981) Method for the Simultaneous Determination of As, Al, Fe, Zn, Cr, and Cu in Plant Tissue Without the Use of Perchloric

Acid, Analyst, 106: 1174-1178.

81BAR 02 R. M. Barnes, editor (1981) Developments in Atomic Plasma Spectrochemical Aralysia,

Proceedings of the International Winter Conference, San Juan, Puerto Rico, Heyden, London.

81BER 01 S. S. Berman, J. W. McLaren, and 0. S. Russel (1981) Application of the Inductively Coupled Plasma to the Analysis of Marine Samples, in 81BAR 02, pp. 586-600.

81BIS 01 K. M. Bisgard, J. Laursen, and B. S. Nielsen (1981) Energy-Dispersive XRF Spectrometry using Secondary Radiation in a Cartesian Geometry, K-ray Spectrometry,

10: 17-19.

81BLA 01 H. S. Black and R. F. Browner (1981) Volatile Metal -Chelate Sanple Introduction for Inductively

Coupled Plasma-Atomic Emission Spectrometry, Analytical

Chemistry, 53: 249-253.

81BLA 02 M. S. Black, M. B. Thomas, and R. F. Browner (1981) Determination of Metal Chelates by Inductively Coupled Plasma Atomic Emission Spectrometry and Applications to Biological Materials, Analytical Chemistry, 53: 2224-2228.

81BLA 03 M. Blanusa and D. Breski (1981) Comparison of Dry and Wet Ashing Procedures for Cachiiun and

Iron Determination in Biological Material by Atomic Absorption Spectrophotometry, Talenta, 28: 681-684.

81BR0 01 P. J. Brooke and W. H. Evans (1981) Determination of Total Inorganic Arsenic in Fish, Shellfish, and Fish Products, Analyst, 106: 514-520.

81BYR 01 A. R. Byrne (1981) Determination of Patladiim in Biological Samples by Neutron Activation Analysis, Mikrochimica Acta (Wien),

19811: 323-329.

81CAN 01 A. Y. Cantillo (1981) Trace Element Deposition Histories in the Chesapeake Bay, Ph.D. Dissertation, University of Maryland, pp. 216-238.

81CAR 01 R. Carpenter and T. M. Beasley (1981) Plutonium and Americiim in Anoxic Marine Sediments: Evidence

Against Remobi I i ration, Geochimica et Cosmochimica Acta,

45: 1917-1930.

81CAR 02 J. W. Carnahan, K. J. Mulligan, and J. A. Caruso (1981) Element -Selective Detection for Chromatography by Plasma Emission Spectrometry, Analytics Chimica Acta, 130: 227.

81CAS 01 V. Casella, C. Bishop, A. Glosby, and C. Phillips (1981) Anion Exchange Method for the Sequential Determination of Uranium, Thoriun, and Lead-210 in Cosl and Coal Ash, Journal of Radioanalytical Chemistry, 62: 257-266.

81CHA 01 C. L. Chakrabarti, C. Wan, H. Hamed, and P. Bertels (1981) Matrix Interferences in Graphite Furnace Atomic Absorption

Spectrometry by Capacitive Discharge Heating, Analytical

Chemistry, 53: 444-450.

81CHE 01 J. H. Chen and G. J. Wasserburg (1981)

The Isotopic Conposition of Uraniim and Lead in Allende

Inclusions and Meteoritic Phosphates, Earth and Planetary

Science Letters, 52: 1-15.

81CHE 02 J. H. Chen and G. J. Wasserburg (1981) Isotopic Determination of Uraniim in Picomole and

Subpicomole Quantities, Analytical Chemistry, 53: 2060-2067.

R-25
CODE N REFERENCE CWE N REFERENCE

81CHR 01 L. H. Christensen and A. Agerbo (1981) Determination of Sulfur and Heavy Metals in Crude Oil and

PetroleLin Products by Energy-dispersive X-ray Fluorescence Spectrometry and Fundamental Parameter Approach, Analytical

Chemistry, 53: 1788-1792.

81CHU 01 S. E. Church (1981) Multielement Analysis of Fifty-four Geochemical Reference

Samples using Inductively Coupled Plasma Atomic Emission

Spectrometry, Geostandards Newsletter, 5: 133-160.

81CLE 01 M. S. Clegg, C. Keen, B. Lonnderat, and L. Hurley (1931) Influence of Ashing Techniques on the Analysis of Trace Elements in Animal Tissue: I. Wet Ashing, Biological Trace Element Research, 3: 107-115.

81CLE 02 M. S. Clegg, C. Keen, B. Lonnderal, and L. Hurley (1981) Influence of Ashing Techniques on the Analysis of Trace Elements in Biological Samples: II. Dry Ashing, Biological Trace Element Research, 3: 237-244.

81C0H 02 S. Cohen, S.-G. Chang, S. Markowitz, and T. Novakov (1981) Role of Fly Ash in Catalytic Oxidation of S(iV) Slurries, Environmental Science and Technology, 15: 1498-1502.

81FRA 01 G. Fraueruieser (1961) Private Conmunication, Technical University of Vienna, Austria.

81GAL 01 M. Gallorini, E. Orvini, A. Rolla, and M. Burdisso (1981) Destructive Neutron Activation Analysis of Toxic Elements

in Suspended Materials Released from Refuse Incinerators,

Analyst, 106: 328-334.

81GAL 02 M. Gallorini, E. Orvini, A. Rolla, and M. Burdisso (1981) Radiochemical Neutron Activation Analysis of Trace Elements

in Suspended Materials Released from Refuse Incinerators,

Analytical Proceedings Published by the Royal Society of Chemistry (London), 18: 199-201.

81GLA 01 E. S. Gladney and D. Knab (1981) Determination of Seleniun in Twenty Geological Reference

Materials by Neutron Activation and Inorganic Ion Exchange, Geostandards Newsletter, 5: 67-69.

81GLA 02 E. S. Gladney and 0. R. Perrin (1981) Instrunental Thermal Neutron Activation Determination of 20 Elements in Nineteen Silicate Reference Materials, Geostandards Newsletter, 5: 113-124.

81C0R 01 R. Cornelis, J. Versieck, A. Desmet, L. Meer, and

L. Vanbal lenberghe (1981), Neutron Activation Analysis of the Trace Element Molybdenun in Urine of Healthy Persons, Bulletin des Societes Chimiques Beiges, 90: 289-295.

81GLA 03 E. S. Gladney, J. Owens, T. Gunderson, and W. Goode (1981) Quality Assurance for Environmental Analytical Chemistry:

1976-1979, Los Alamos Scientific Laboratory report LA-8730-MS, pp. 113-118.

81C0R 02 R. Cornelis, J. Versieck, L. Meers, J. Hoate, and r. Garbier

(1981), The Ultratrace Element Vanadiun in Hunan Serun, Biological Trace Element Research, 3: 257-263.

81C0X 01 D. H. Cox and A. E. Bibb (1981) Hydrogen Selenide Evolution-Electrothermal Atomic Absorption Method for Determining Nanogram Levels of Toral Se, Journal

of the Association of Official Analytical Chemists, 64: 265.

81DAN 01 L.-G. Danielsson, D. Jagner, M. Josefson, and S. Westerlund

(1981), Computerized Potent iometric Stri|sping Analysis for the Determination of CadmiLm, Lead, Copper, and Zinc 'ii Biological Materials, Analytica Chimica Acta, 127: 147-156.

81DIL 01 S. Dilli (1981) Determination of Vanadium in Petroleum CiLides and Furl Oils

by Gas Chromatography, Analytica Chimica Acta, 128: f?vH9.

81D0G 01 S. Dogan, G. Nembrini, and W. Haerdi (1931)

A Novel Approach for Determination of Sn.. Pb, and Cu in Biological Samples and Sediments by Alternsting Current Anodic Stripping Voltammetry, Analytica Chimica Acta,

130: 385-390.

81GLA 04 E. S. Gladney, W. Goode, D. Perrin, and C. Burns (1981) Quality Assurance for Environmental Analytical Chemistry:

1980, Los Alamos National Laboratory report LA-8966-MS,

(| pp. 108-114.

81G0O 01 R. T. Goodpasture, R. J. HcElhaney, and R. Morrow (1981) Analysis of Botanical Samples for 25 Elements using an Automated Inductively Coupled Plasma Spectrometer,

in 81 BAR 02, pp. 697-705.

81G0U 01 P. D. Goulden, D. H. J. Anthony, end K. D. Austen (1981) Determination of Arsenic ar<d Seleniun in Water, Fish, and Sediments by Inductively Coupled Argon Plasma Emission Spectrometry, Analytical Chemistry, 53: 2027-2029.

81HAB 01 S. Habib and M. J. Minski (1981) Neutron Activation Technique for the Analysis of the Soluble and Particle Fractions of River Water, Journal

of Radioanalytical Chemistry, 63: 379-395.

81HAH 01 M. H. Haha, R. Kuennen, J. Caruso, and F. Ficke (1981) Title Unknown, Journal of Agricultural and Food Chemistry,

preprint.

81EBD 01 L. Ebdon, J. R. Wilkinson, and K. W. Jackson (1981) Determination of Sub- nanogram Amounts of Mercury by Cold Vapor Atomic Fluorescence Spectrometry with an Improved Gas-sheathed Atom Cell, Analytica Chimics ^cta, 128: 45-55.

81FAR 01 J. G. Farmer and M. J. Gibson (1981) Direct Determination of Cadmiui), Chromium, Copptr, and Lead

in Siliceous Standard Reference Materials from a Fluoboric Acid Matrix by Graphite Furnace Atomic Absorprion

Spectrometry, Atomic Spectroscopy, 2: 176-173.

81F0N 01 H. A. Foner and I. Gal (1981) Accurate Spectrophotometric Method for the Dots-.Tibat'on

of Silica in Rocks, Minerals, and Related K&tR-iaU, MnB'yv-.

106: 521-528.

81HAM 01 H. Hamaguchi (1981) Private Communication, taken from 81YAM 01.

81HAN 01 H.-B. Han, G. Kaiser, and G. Tolg (1981) Decomposition of Biological Materials, Rocks, and Soils in

Pure Oxygen under Dynamic Conditions for the Determination

of Se at Trace Levels, Analytica Chimica Acta, 128: 9-21.

81HIN 01 E. J. Hinderberger, M. Kaiser, and S. Koirtyohann (1981)

Furnace Atomic Absorption Analysis of Biological Samples

using the L'Vov Platform and Matrix Modification, Atomic

Spectroscopy, 2: 1-7.

81H0 02 R. Ho (1981) Title Unknown, M.S. Thesis, University of Toronto; taken

from 84LAN 02.

R-26
CODE N REFERENCE CODE N REFERENCE

81M0R 01 J. J. Horvath, J. D. Bradshaw, J. N. Bower, H. S. Epstein, and J. D. Winefordner (1981), Comparison of Nebulizer- Burner Systems for Laser-Excited Atomic Fluorescence Flame Spectrometry, Analytical Chemistry, 53: 6-9.

811MU 01 H. imura and N. Suzuki (1981) Substoichiometric Isotope Dilution Analysis for Tin with

Sal icyl ideneamino-2-Thiophenol Complexation in Non-aqueous

Medium, Talanta, 28: 73-79.

81INU 01 T. Inui, S. Tereda, and H. Tamura (1981) Determination of As by Arsine Generation with Reducing Tube Followed by Graphite Furnace Atomic Absorption Spectrometry, Fresenius Zeitschrift fur Analytische Chemie, 305: 189-192.

81JAC 01 K. W. Jacicson, L. Ebdon, D. C. Webb, and A. G. Cox (1981) Determination of Lead in Vegetation by a Rapid Microsampling

Cup Atomic Absorption Procedure with Solid Sample

Introduction, Analytica Chimica Acta, 128: 67-74.

81JIN 01 S. Jingxin, T. Shude, U. Yuqi, C. Bingru, Q. Oinfang, and

Z. Shen (1981), Determination of 28 Trace Elements in Soils

from Mount Qomolangma Region by INAA, taken from 81MTA 01.

81ICAH 01 H. L. Kahn, L. Cristiano, G. Dulude, and J. Sotera (1981) Automated Hydride Analysis, American Laboratory, 13(11): 136-U4.

81KIB 01 T. Kiba (1981) Private Comnunication, in 81YAM 01.

81KIN 01 H. Kingston and P. A. Pel la (1981) Preconcentration of Trace Metals in Environmental and

Biological Samples by Cation Exchange Resin Filters for X-ray Spectrometry, Analytical Chemistry, 53: 223-227.

81KIT 01 K. Kitagawa, T. Nanya, and S. Tsuge (1981) Application of the Atomic Faraday Effect to the Trace Determination of Lead, Spectrochimica Acta, 36B: 9-20.

81KNA 01 G. Knapp, S. Raptis, G. Kaiser, G. Tolg, P. Schramel, end

B. Schreiber (1981), A Partially Mechanized System for the Combustion of Organic Samples in a Stream of Oxygen with Quantitative Recovery of the Trace Elements, Fresenius Zeitschrift fur Analytische Chemie, 308: 97-103.

81K0S 01 K. Kostadinov and R. Djingova (1981) Trace Element Analysis of Biological Materials by Thermal and Epithermal Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 63: 5-12.

81KRI 01 V. Krivan, H. Geiger, and H. E. Franz (1981) Bestiimung von Fe, Co, Cu, Zn, Se, Rb, und Cs in NBSOchsenLeber Blutplasma und Erythrocyten durch INAA und AAS, Fresenius Zeitschrift fur Analytische Chemie, 305: 399-404.

81KUC 01 J. Kucera and J. J. M. de Goeij (1981)

A Comparison of Two Separation Techniques using NaKTl) and

Ge(Li) Spectrometry for Trace Element Determination in Biological Materials by Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 63: 23-40.

81KUL 01 I. Kuleff, R. Djingova, K. Kostadinov, and D. Todorovsky

(1981), Instrumental Neutron Activation Analysis of Trace

Elements in Quartz, Journal of Radioanalytif^al Chemistry,

62: 187-194.

81KUL 02 I. Kuleff and K. Kostadinov (1981) Epithermal Neutron Activation Analysis of Uraniun by

Neptuniaii-239 using High Resolution Gamma Spectrometry,

Journal of Radioanalytical Chemistry, 63: 397-404.

81LAN 01 F. J. Langmyhr and I. M. Dahl (1981) Atomic Absorption Spectrometric Determination of Phosphorus

in Biological Materials, Analytica Chimica Acta, 131: 303.

81LEE 01 S. W. Lee and J. C. Meranger (1981) Determination of Total Arsenic Species by Anodic Stripping

Voltammetry, Analytical Chemistry, 53: 130-131.

81MAR 01 D. F. Marino and J. D. Ingle (1981)

Ion Exchange Separation of Cobalt from Alkaline Earth and Selected Transition Metals with Lophine Chemi liminescence Detection, Analytical Chemistry, 53: 292-294.

81MER 03 R. N. Merefield and J. H. Runnels (1981) The Inductively Coupled Plasma: An Important and Versatile Analytical Tool for the Petroleun Industry, in 81BAR 02,

pp. 396-403.

81HEY 01 A. Meyer, C. Hofer, G. Knapp, and G. Tolg (1981) Selenbestimnung in UG/G and NG/G Bereich im Anorganischen

und Organischen Matrices nach Verdampf ungsalanyse in Dynamischen System durch AAS, Frenesius Zeitschrift fur Analytische Chemie, 305: 1-10.

81MIZ 01 A. Mizuike and A. lino (1981) Surface Treatment of Borosilicate Glass Beakers for Prevention of Sodium Contamination, Analytica Chimica Acta,

124: 427-430.

81M0H 01 N. Mohamed and R. C. Fry (1981) Slurry Atomization Direct Atomic Spectrochemical Analysis of Animal Tissue, Analytical Chemistry, 53: 450-455.

81M0L 01 A. Molokhia and A. Dyer (1981) Simultaneous Determination of Eight Trace Elements in Hunan Skin by Instrumental Neutron Activation Analysis, Analyst,

106: 1168-1173.

81MTA 01 Modern Trends in Activation Analysis (1981)

At)stracts, Sixth International Conference, University of Toronto, Canada.

81MUN 01 R. C. Munter end R. A. Grande (1981) Plant Tissue and Soil Extract Analysis by ICP-Atomic Emission Spectrometry, in 81BAR 02, pp. 653-672.

81NAD 01 R. A. Nadkarni (1981) Determination of Volatile Elements in Coal and Other Organic Materials by Oxygen Bomb Coirtxistion, American Laboratory,

13(8): 22-29.

81NAR 01 H. Narasaki (1981) Determination of Trace Hg in Milk Products and Plastics by

Combustion in an Oxygen Bomb and Cold-vapor Atomic Absorption Spectrometry, Analytica Chimica Acta, 125: 187-191.

81NEU 01 D. R. Neunan and F. F. Munshower (1981) Rapid Determination of Molybdenun in Botanical Material by

Electrothermal Atomic Absorption Spectrometry, Analytica

Chimica Acta, 123: 325-328.

81NIS 01 Y. Nishikawa (1981) Private Communication, in 81YAM 01.

81N0N 01 N. Nonaka, H. Higuchi, H. Haroaguchi, and K. Tomura (1981)

Losses of the Elements during Dry Ashing of Plant Materials,

Bunseki Kagaku, 30: 599-604.

R-27
CODE N REFERENCE CODE N REFERENCE

810GU 01 K. Oguma and R. Kuroda (1981) Dry-column Chromatography of Uranium: Application to Chemical Analysis of Monazite and Phosphate Rock for Uranium Mikrochimica Acta (Wien), 1981II: 57-67.

310HT 01 A. Ohta, T. Matsubayashi , and M. Itoman (1981) Energy-Dispersive XRF Spectrometric Determination of Phosphorus, Calciuti, Iron, Zinc, and Strontiun in Htman

Bones, Advances in X-ray Chemical Analysis in Japan, 12: 73.

810WE 01 J. W. Owens (1981) Private Comunication, Environmental Surveillance Group,

Los Alamos National Laboratory, Los Alamos, New Mexico.

81PAH 01 B. Pahlananpour, M. Thompson, and L. Thorne (1981) Simultaneous Determination of Trace Amounts of As, Sb, and

Bi in Herbage by Hydride Generation and ICP Atomic Emission

Spectrometry, Analyst, 106: 467-471.

81PAR 01 P. P. Parekh (1981) Energy- dispersive X-ray Fluorescence Analysis of Organic- rich Soils and Sediments, Radiochemical and Radioanalytical Letters, 50: 1-14.

81P1C 01 C. J. Pickford (1981) Determination of Arsenic by Emission Spectrometry using an Inductively Coupled Plasma Source and the Syringe Hydride

Technique, Analyst, 106: 464-467.

81P1H 01 B. Pihlar, P. Valenta, and H. W. Nurnberg (1981) New High -Performance Analytical Procedure for the Voltaimstric Determination of Nickel in Routine Analysis of Waters, Biological Materials, and Food, Fresenius Zeitschrift fur Analytische Chemie, 307: 337-346.

81SAI 01 S. 0. Saied, D. Crumpton, and P. E. Francios (1981) The Validation of a PIXE System for Trace Element Analysis

of Biological Samples, Nuclear Instrunents and Methods,

181: 53-57.

81SAS 01 C. S. Sastri, R. Caletka, and V. Krivan (1981) Simultaneous Determination of Boron and Lithitm by Charged

Particle Activation Analysis, Analytical Chemistry, 53: 765.

81SAS 02 C. S. Sastri, R. Caletka, and V. Krivan (1981) Analysis of Refractory Metals for LithiLn, Boron, and Nitrogen by Charged Particle Activation Yielding Be-7 as the Indicator Radionuclide, taken from 81MTA 01.

81SEG 01 C. Segebade and H.-U. Fusban (1981)

Uraniiin Analysis by Activation with 30 MeV Bremsstrahlung, Radiochemical and Radioanalytical Letters, 48: 311-328.

81SHA 01 P. G. Shaw, D. McKown, arvd S. E. Manahan (1981) Trace Element Determinations in Shale Oil Products by Neutron Activation, Anelytica Chimica Acta, 123: 65-74.

81SHI 01 T. Shigematsu and K. Kudo (1981) SubEtoichiometric Determination of Phosphorus, Journal of Radioanalytical Chemistry, 67: 307-319.

81SL0 01 H. van der Sloot, K. Hoede, T. Klinkers, and H. Das (1981) The Determination of Arsenic, Seleniun, and Antimony in Rocks, Sediments, Fly Ash, and Slag, in 81MTA 01.

eiSTR 01 W. B. Stroube, W. C. Cunningham, and M. Allegrini (1981) Activation Analysis Program of the USFDA at the NBSR, in NBS Reactor: Simmsry of Activities July 1979 to June 1980, NBS Technical Note 1142, pp. 186-188.

81P0S 01 R. S. Posey and R. W. Andrews (1981) Determination of Se(lV) by Anodic Stripping Volteimietry with an In-situ Gold-Plated Rotating Glassy Carbon Disk Electrode, Anelytica Chimica Acta, 124: 107-112.

81SUZ 01 S. Suzuki, S. Hirai, and tC. Noda (1981) Determination of Seleniufn in Herb Plants by Neutron Activation Analysis using a Coincidence Counting Method,

Bunseki Kagaku, 31: 67-71.

81RAP 01 S. E. Raptis, H. Wegscheider, srKl G. Knapp (1981) The Determination of Arsenic at NG/G and PPM Levels in Organic and Biological Matrices, Mikrochimica Acta (Wien), 19811: 93-97.

81REA 01 D. C. Reamer and C. Veil Ion (1981) Preparation of Biological Materials for Determination of Seleniun by Hydride Generation-Atomic Absorption

Spectrometry, Analytical Chemistry, 53: 1192-1195.

81REA 02 0. C. Reamer and C. Veillon (1981) Determination of Selenium in Biological Materials by Stable

Isotope Dilution Gas Chromatography - Mass Spectrometry, Analytical Chemistry, 53: 2166-2169.

81REE 01 J. Reednick (1981) Spectroscopi e Atomique: Excitation d'un Plasma de Haute Energie et Spectrometrie de Resolution Elevee, Analusis,

9: 14-20.

81SZY 01 F. Siydlowski, D. Dunmire, E. Peck, R. Eggers, and W. Matson

(1981), Simultaneous Determination of Fe(II), Fe(III), and

Total Iron in Sphagnun Moss Peat by Programnable Voltammetry

on a Graphite TutMilar Electrode, Analytical Chemistry,

53: 193-196.

81TAN 01 K. Tanabe, K. Chiba, H. Haraguchi, and K. Fuwa (1981) Determination of Mercury at the Ultratrace Level by

Atmospheric Pressure Helium Microwave- Induced Plasma Emission Spectrometry, Analytical Chemistry, 53: 1450-1453.

81T0E 01 K. Toei and Y. Shimoishi (1981) Determination of Ultramicro Amounts of Seleniun by Gas Chromatography with Electron-Capture Detection, Talanta,

28: 967-972.

81TUR 01 K. E. Turner (1931) Private Ccnmunication, Bhp. Central Research Laboratories,

Shortland, Australia.

81REL 01 R. E. Relm and D. D. Hawn (1981) Determination of Total Sulfur in Hydrocarbons by Reductive

Pyrolysis with Polarograptiic Detection, Analytical Chemistry

53: 1088-1093.

81R0B 02 G. Rotaye, G. Weber, J. Delbrouck, I. Roelandts, P. Bartsch,

and A. Collignon (1981), Attempts to Improve PIXE Quantitative Trace Element Analysis of Biomedical Materials,

Nuclear Instruments and Methods, 181: 59-62.

81UCH 01 T. Uchida, I. Kojiroa, and C. lida (1981) Application of an Automatically Triggered Digital Integrator

to Flame Atomic Absorption Spectrometry of Copper using a

Discrete Nebulisation Technique, Analyst, 106: 206-212.

81UCH 02 H. Uchida, Y. Shimoishi, and K. Toei (1981) Rapid Determination of Trace Amounts of Seleniun in

Biological Samples by Gas Chromatography with Electron

Capture Detection, Analyst, 106: 757-762.

R-28
CODE N REFERENCE CODE N REFERENCE

81UTH 01 E. Uthus, M. Codings, W. Cornatzer, and F. Nielsen (1981) Determination of Total Arsenic in Biological San^les by Arsine Generation and Atomic Absorption Spectrometry, Analytical Chemistry, 53: 2221-2224.

81VER 02 A. Verbueken, E. Michiels, and R. van Grieken (1981)

Total Analysis of Plant Material and Biological Tissue by

Spark Source Mass Spectrometry, Fresenius Zeitschrift fur Analytische Chemie, 309: 300-304.

81UAL 01 G. F. Wallace (1981) Application of a Sequential Scanning ICP to the Analysis of Geological Materials, Atomic Spectrometry, 2: 87-90.

81UAL 02 G. F. Wallace and R. D. Ediger (1981) Optimization of ICP Operating Conditions for the Determination of Sulfur in Oils, Atomic Spectrometry,

2: 169-172.

81WAN 01 L. E. Wangen (1981) Relationships Between the Elemental Conf>osition and Particle

Sizes of Aerosols With and Without Iii?)act from a Coal-fired

Power Plant, Los Alamos Scientific Laboratory report LA-8759-HS.

81WEI 01 A. D. Weiss, R. N. Savage, and G. H. Hieftje (1981) Development and Characterization of a 9-nm Inductively

Coupled Argon Plasma Source for Atomic Emission Spectrometry

Analytica Chimica Acta, 124: 245-258.

81ZAU 01 G.-P. Zaukc (1981) Cadmium in Ganmeridae (Amphipoda:Crustacea) of the Rivers

Werra and Weser: Geographical Variation and Correlation to Cadmium in Sediments, Environmental Pollution, 2: 465-474.

82AICA 01 J. Akashi, I. Fukushima, A. Imahori, and S. Shiobara (1982) Multielement Analysis of the Hair of Mining Industry Workers

Journal of Radioanalytical Chemistry, 68: 59-65.

82AN0 01 Anonymous (1982) Elemental Analysis: Model 240C Elemental Analyzer, Perkin-Elmer Corporation, Norwalk, Conn.

82ATS 01 I. Atsuya and K. Itoh (1982) Direct Determination of Caciniuiri in the NBS Bovine Liver by Zeeman Atomic Absorption Spectrometry using the Graphite

Miniature-cup, Bunseki kagaku, 31: 713-717.

82ATS 02 I. Atsuya and tC. Itoh (1982) Direct Determination of Lead in the NBS Bovine Liver by Zeeman Atomic Absorption Spectrometry using the Graphite

Miniature-cup, Bunseki Kagaku, 31: 708-712.

82AZI 01 A. Aziz, J. A. C. Broekaert, and F. Leis (1982) Analysis of Microamounts of Biological Samples by

Evaporation in a Graphite Furnace and Inductively Coupled Plasma Atomic Emission Spectroscopy, Spectrochimica Acta, 37B: 369-379.

81WIL 01 R. E. Williams, P. K. Hopke, and R. A. Meyer (1981) Trace Multielement Analysis using High-flux Fast-neutron

Activation, Journal of Radioanalytical Chemistry, 63: 187.

81WIL 02 R. E. Williams (1981) Gamma-ray Spectrometry Following High-flux 14-MeV Neutron

Activation, Ph.D. Thesis, University of Illinois, and Lawrence Livermore Laboratory report UCRL -53208.

81W0L 01 K. Wolnik, F. Fricke, M. Hahn, and J. Caruso (1981) Sample Introduction System for Simultaneous Determination of Volatile Elemental Hydrides and other Elements in Foods by

Inductively Coupled Argon Plasma Emission Spectrometry,

Analytical Chemistry, 53: 1030-1035.

81W0L 02 K. A. Wolnik, R. W. Kuennen, and F. L. Fricke (1981) Determination of Toxic and Nutritional Elements in Raw Agricultural Crops using ICAP Spectroscopy, in 81BAR 02,

pp. 685-696.

81YAM 01 M. Yamamoto, T. Shohjii, T. KamLmaru, and Y. Yamamoto (1981) Masking Effect of KI on the Interferences in the Atomic

Absorption Spectrometric Determination of Sb utilizing

Stibine Generation by Sodiun Borohydride Tablet Reduction,

Fresenius Zeitschrift fur Analytische Chemie, 305: 11-14.

81YAN 01 K. Yanagi and H. Airtbe (1981) Determination of Arsenic in Biological, Environmental, and

Geological Materials by Arsine Evolution Flameless Atomic Absorption Spectrophotometry, Bunseki kagaku, 30: 209-214.

81YAS 01 A. Yasui, H. Koizimi, and C. Tsutsumi (1981) Determination of Calcium in Food Samples: Application of Adding Interference Suppressing Reagent-Atomic Absorption

Spectrophotometric Metho.-J, Bunseki Kagaku, 30: 165-T71.

82AZI 02 A. Aziz, J. A. C. Broekaert, and F. Leis (1982) A Contribution to the Analysis of Microamounts of Biological

Samples using a Conbination of Graphite Furnace and Microwave Induced Plasma Atomic Emission Spectroscopy, Spectrochimica Acta, 37B: 381-389.

82BAR 01 U. Bartels and T. T. Pham (1982) Spectrophotometric Determination of Sulphur in Plants using

Schoniger Conbustion and Dimethylsulphonazo III, Fresenius Zeitschrift fur Analytische Chemie, 310: 13-15.

82BEN 01 H. Benard and M. Pinta (1982) Determination of Arsenic in Atmospheric Aerosols by Atomic Absorption with Electrothermal Atomization, Atomic Spectroscopy, 3: 8-12.

82BYR 01 A. R. Byrne (1982) Simultaneous Radiochemical Neutron Activation Analysis of Vanadiim, Molybdenum, and Arsenic in Biological Samples, Radiochemical and Radioanalytical Letters, 52: 99-110.

82CAL 01 G. Calderoni and T. Ferri (1982) Determination of Tl at Subtrace Level in Rocks and Minerals

by Coupling Differential Pulse Anodic Stripping Voltamnetry

with Suitable Enrichment Methods, Talanta, 29: 371-375.

82CHA 01 J. F. Chapman and L. S. Dale (1982) The Use of Alkaline Permanganate in the Preparation of

Biological Materials for the Determination of Hg by Atomic Absorption Spectrometry, Analytica Chimica Acta, 134: 379.

82CHR 01 J. K. Christensen, L. Kryger, and N. ^'nd (1982) The Determination of Traces of Cactnium, Lead, and thallium

in Fly Ash by Potentiometric Stripping Analysis, '"alytica Chimica Acta, 141: 131-146.

81YUZ 01 H. Yuzawa and N. Suzuki (1981) Substoichiometric Isotope Dilution Analysis of Calciun in Biological Material, Journal of Radioanalytical Chemistry,

62: 115-124.

82CLE 01 M. S. Clegg, C. Keen, B. Lonnerdal, and L. Hurley (1982) Analysis of Trace Elements in Animal Tissue: Determination

of Manganese by Graphite Furnace Atomic Absorption Spectrophotometry, Biological Trace Element Research, 4: 145-156.

R-29
CODE N REFERENCE CODE N REFERENCE

82C0H 01 I. M. Cohen, S. H. Rcsniiky, and G, B. Baro (1982) Activation Analysis of Thalliim by Tt -ZOSCn.Zn)!! -202 Reaction in Nuclear Reactors, Journal of Radioanalytical

Chemistry, 72: 451-461.

82CON 01 C. P. Conrad, M. W. Rowe, and E. S. Gladncy (1982) Comparative Determination of Uraniim in Silicates by Delayed Neutron Activation Analysis, Geostandards Newsletter, 6: 1-4.

82FLA 01 F. J. Flanagan, R. Moore, and P. J. Aruscavage (1982) Mercury in Geological Sanples, Geostandards Newsletter,

6: 25-46.

8?GAJ 01 R. J. Gajan, S. Capar, C. Subjoc, and M. Sanders (1982) Determination of Lead and Cadniun in Foods by Anodic Stripping Voltaitmetry: I. Development of Method, Journal of the Association of Official Analytical Chemists, 65: 970.

82C0R 01 E. Cortes, N. Gras, L. Munoz, and V. Cassorla (1982)

A Study of Some Trace Elements in Infant Foods, Journal

of Radioanalytical Chemistry, 69: 401-415.

82GLA 02 E. S. Gladney, D. Perrin, C. Burns, and R. Robinson (1982) Quality Assurance for Environmental Analytical Chemistry:

1981, Los Alamos National Laboratory report LA-9579-MS.

82CR0 01 J. G. Crock and F. E. Lichte (1982) Determination of Rare Earth Elements in Geological Materials

by Inductively Coupled Argon Plasma/Atomic Emission

Spectrometry, Analytical Chemistry, 54: 1329-1332.

82GOL 01 J. Goldberg and R. Sacks (1982) Direct Determination of Metallic Elements in Solid, Powder Sanples with Electrically Vaporized Thin Film Atomic Emission Spectrometry, Analytical Chemistry, 54: 2179-2186.

82CR0 03 J. G. Crock and F. E. Lichte (1982) An Improved Method for the Determination of Trace Levels of Arsenic and Antimony in Geological Materials by Automated

Hydride Generation Atomic Absorption Spectroscopy, Analytica Chimica Acta, 144: 223-233.

82CUR 01 0. B. Curtis (1982) Private Communication, Group INC-7, Los Alamos National Laboratory, New Mexico.

82GRA 01 C. Graham, M. Glascock, J. Carni, J. Vogt, and T. Spalding

(1982), Determination of Elements in National Bureau of Standards' Geological Standard Reference Materials by Neutron Activation Analysis, Analytical Chemistry, 54: 1623.

82GRE 03 R. R. Greenberg and H. M. Kingston (1982) Simultaneous Determination of Twelve Trace Elements in Estuarine and Ses Water using Pre- irradiation Chromatography, Journal of Radioanalytical Chemistry, 71: 147-167.

82DAK 01 T. Dakabu and M. D. Swaine (1982) Calciun and Potassium Levels in Leaves Measured by X-ray

Fluorescence Analysis, International Journal of Applied

Radiation and Isotopes, 33: 193-196.

82GRI 01 A. P. Grimanis and G. D. Kanias (1982) Rapid Determination of Mercury in Biological Materials by

Radiochemical Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 72: 587-595.

82DAM 01 E. Damsgaard, K. Ostergaard, end K. Heydorn (1982) Concentrations of Seleniim and Zinc in Hunan Kidneys,

Journal of Radioanalytical Chemistry, 70: 67-76.

82DEM 01 D. R. Demers, D. A. Busch, and C. D. Allemand (1982)

ICP Atomic Fluorescence Spectroscopy, American Laboratory,

14 (3): 167.

82DCK) 01 K. J. Doolan (1982) The Determination of Traces of Mercury in Solid Fuels by

High Temperature Combustion and Cold-vapor Atomic Absorption

Spectrometry, Analytica Chimica Acta, 140: 187-195.

82EBD 01 L. Ebdon, J. R. Wilkinson, and K. W. Jackson (1982) Determination of Mercury in Coal by Non-oxidative Pyrolysis

and Cold Vapor Atomic- Fluorescence Spectrometry, Analyst,

107: 269-275.

82EBD 02 L. Ebdon ..ind W. C. Pearce (1982) Direct Determination of Arsenic in Coal by Atomic Absorption

Spectroscopy using Solid Sampling and Electrothermal Atomization, Analyst, 107: 942-950.

82EHM 01 W. D. Ehmann, U. R. Markesbery, and T. M. Hossain (1982) Trace Elements in Human Brain Tissue by INAA, Journal of Radioanalytical Chemistry, 70: 57-65.

82ELS 02 C. H. Elson, J. Mi I ley, and A. Chatt (1982) Determination of Arsenic and Antimony in Geological Material

ar»d Natural Waters by Coprecipitation with Selenium and Neutron Activation-Gamma Spectrometry, Analytica Chimica

Acta, 142: 269-275.

82EVA 01 U. H. Evans and D. Dellar (1982) Evaluation of an Inductively Coupled Plasma Emission

Direct -Reading Spectrometer for Multiple Trace Element

Analysis of Foodstuffs, Analyst. 107: 977-992.

82GRO 01 Z. Grobenski, R. Lehmann, R. Taim, and B. Welz (1982) Improvements in Graphite Furnace Atomic Absorption

Microanalysis with Solid Sanpling, Mikrochimica Acta (Wien),

19821: 115-125.

82GUP 02 J. G. Sen Gupta (1982) Flame and Graphite Furnace Atomic Absorption and Optical Emission Spectroscopic Determination of Yttriun and the Rare Earth Contents of Sixteen International Reference

Samples of Rocks and Coal, Geostandards Newsletter, 6: 241.

82HAD 01 I. Hadzistelios and C. Papadopoulou (1982) Radiochemical Determination of Molybdenun in Biological Tissues by Ion Exchange, Journal of Radioanalytical

Chemistry, 72: 597-607.

82HAH 01 M. H. Hahn, K. Wolnik, F. Fricke, and J. Caruso (1982) Hydride Generation/Condensation System with an Inductively

Coupled Argon Plasma Polychromator for Determination of Arsenic, Bismuth, Germaniim, Antimony, Seleniim, and Tin

in Foods, Analytical Chemistry, 54: 1048-1052.

82HAM 01 E. P. Hamilton and A. Chatt (1982) Determination of Trace Elements in Atmospheric Wet Precipitation by Instrumental Neutron Activation Analysis,

Journal of Radioanalytical Chemistry, 71: 29-45.

82HAR 01 J. H. Harnly, J. S. Kane, and N. J. Miller-Ihli (1982)

Effects of Air-Acetylene Flame Parameters on Simultaneous

Multielement Atomic Absorption Spectrometry, Applied

Spectroscopy, 36: 637-643.

82HEI 01 H. Heinrichs and H. Keltsch (1982) Determination of Arsenic, Bismuth, Cadmiim, Seleniun, and

Thalliun by Atomic Absorption with a Volatilization

Technique, Analytical Chemistry, 54: 1211-1214.

R-30
COOE N REFERENCE COOE N REFERENCE

82HEY 02 K. Heydorn and E. Damsgaard (1982) Evaluation of Botanical Reference Materials for the Determination of Vanadiun in Biological Sanples,

Journal of Radioanalytical Chemistry, 69: 131-K6.

82K1M 01 T. Kimura, T. Ishimori, and T. Hamada (1982) Removal of Na-24 by a Chromatographic Extraction with a Kieselguhr Colunn and a Crown Ether Solution, Analytical

Chemistry, 54: 1129-1131.

82H0E 01 M. Hoenig, C. Lima, and S. Dupire (1982) Validite des Determinations par Spectrometrie D'Absorption

Atomique avec Atomisation Electrpthermique du CactniLir,

Cobalt, Chrome, Nickel et Plomb, Analusis, 10: 132-139.

82KIR 01 T. Kiriyama and R. Kuroda (1982)

Combir>ed Ion Exchange-Spectrophotometric Method for the Simultaneous Determination of Vanadiun and Cobalt in Biological Materials, Analyst, 107: 505-510.

82H0E 02 M. Hoenig and P. van Hoeyweghen (1982) Application de la SAA Electrothermique a L'Analyse des Matrices Complexes: Cas de L'Arsenic dans les Vegetaux

Spectrochimica Acta, 37B: 817-828.

82KIR 02 T. Kiriyama and R. Kuroda (1982) Ion-Exchange Separation and Spectrophotometric Determination

of Titaniim in Biological Materials, Fresenius Zeitschrift

fur Analytische Chemie, 313: 328-330.

82INU 01 T. Inui, S. Terada, H. Tamura, and N. Ichinose (1982) Determination of Se by Hydride Generation with Reducing Tube

Followed by Graphite Furnace Atomic Absorption Spectrometry,

Fresenius Zeitschrift fur Analytische Chemie, 311: 492-495.

82JAG 01 D. Jagner and K. Aren (1982) Flow Potent iometric Stripping Analysis for Mercury(II) in

Urine, Sediment, and Acid Digest of Biological Material,

Analytica Chimica Acta, 141: 157-162.

82JEN 01 D. ft. Jenke and F. E. Diebold (1982) Characterization of Phosphorite Ores, Analytical Chemistry,

54: 1008-1011.

82KIS 01 E. Kiss (1982) Determination of Silica in Geological Materials by Atomic Absorption Spectrometry, Analytica Chimica Acta, 140: 197.

82KOI 01 S. R. Koirtyohann, M. Kaiser, and E. Hinderberger (1982) Food Analysis for Lead using Furnace Atomic Absorption and

a L'Vov Platform, Journal of the Association of Official Analytical Chemists, 65: 999-1003.

82KRA 01 M. Kralik (1982) Rb-Sr Age Determinations of Precambrian Carbonate Rocks of the Carpentarian McArthur Basin, Northern Territories,

Australia, Precambrian Research, 18: 157-170.

62JEN 02 D. R. Jenke and R. Uoodriff (1982) Application of the Woodriff Constant Temperature Graphite

Furnace Atomizer to Atomic Spectroscopy, American Laboratory

14(8): 14-26.

82JEN 03 C. D. Jennings and T. M. Beasley (1982) Radiochemical Determination of Co-60 in Environmental

Samples, Talanta, 29: 871-873.

82JEN 05 D. R. Jenke and R. Woodriff (1982) Simultaneous Emission/Absorption Analysis in Constant Temperature Furnace Atomic Spectroscopy, Applied

Spectroscopy, 36: 686-689.

82JER 01 R. E. Jervis, K.-L. Ho, and B. Tiefenbach (1982) Trace Impurities in Canadian Oil-Sands, Coals, and Petroleun

Products and Their Fate during Extraction, Up-Grading, and

Combustion, Journal of Radioanalytical Chemistry, 71: 225.

82J0N 01 J. W. Jones, S. G. Capar, and T. C. O'Haver (1982) Critical Evaluation of a Multielement Scheme using Plasma Emission and Hydride Evolution Atomic Absorption

Spectrometry for the An<ilysis of Plant and Animal Tissues,

Analyst, 107: 353-377.

82JUL 01 K. Julshamn, 0. Ringdal, K. SI inning, and 0. Braekkan (1982) Optimization of the Determination of Seleniun in Marine

Samples by Atomic Absorption Spectrometry: Comparison of a Flameless Graphite Furnace Absorption System with a Hydride Generation Atomic Absorption System, Spectrochimica Acta,

37B: 473-482.

82KAM 01 E. Kamata, R. Nakashima, K. Goto, and S. Shibata (1982) Determination of Twelve Elements Including Major and Trace

Elements in Coal with Flame Atomic Absorption Spectrometry,

Bunseki Kagaku, 31: 551-556.

82KEE 01 J. A. Keenan and D. Holmes (1982) Quantitative Trace Analysis by X-ray Fluorescence using the Computer Program NRLXRF, Applied Spectroscopy, 36: 19-22.

B2KRI 01 V. Krivan and M. Lang (1982) Radiotraceruntersuchungen zur Direkten Bestirmung von Kupfer

in Biologischen Matrices durch Flammenlose AAS, Fresenius Zeitschrift fur Analytische Chemie, 312: 324-330.

82KUE 01 R. W. Kuennen, D. A. Wolnik, F. Fricke, and J. Caruso (1982) Pressure Dissolution and Real Sample Matrix Calibration for Multielement Analysis of Raw Agricultural Crops by

Inductively Coupled Plasma Atomic Emission Spectrometry, Analytical Chemistry, 54: 2146-2150.

82KUE 03 R. W. Kuennen, M. Hahn, F. Fricke, and K. Wolnik (1982) Hydride Generation and Condensation Flame Atomic Absorption

Spectroscopic Determination of Antimony in Raw Coffee Beans and Processed Coffee, Journal of the Association of Official Analytical Chemists, 65: 1146-1148.

82LAS 01 B. 0. Lass, N. G. Roche, and A. 0. Sanni (1982) Heavy Ion Activation Analysis, Journal of Radioanalytical

Chemistry, 70: 251-272.

82LAU 01 J. C. Laul, E. A. Lepel, W. C. Weimer, and N. Wogman (1982) Precise Trace Rare Earth Analysis by Radiochemical Neutron

Activation, Journal of Radioanalytical Chemistry, 69: 181.

82LE0 03 L. Leoni , M. Minichini, and M. Saitta (1982) Determination of Sulfur, Chlorine, and Fluorine in Silicate

Rocks by X-ray Fluorescence Analysis, X-ray Spectrometry,

11: 156-158.

82LEU 01 P. C. Leung, K. S. Subramanian, and J. Meranger (1982) Determination of Arsenic in Polluted Waters by Differential

Pulse Anodic Stripping Voltamnetry, Talanta, 29: 515-518.

82L1A 01 C. Liao (1982) Tellurian as Catalyst in Semimicro Kjeldahl Method for Total

Nitrogen Determination, Journal of the Association of

Official Analytical Chemists, 65: 786-790.

R-31
CODE N REFERENCE CODE N REFERENCE

82LIN 01 S. M. Lin, C. H. ChiBng, C. L. Tseng, and M. H. Yang (1982) Determination of Mercury Contents in Head Hair of Dentists

by Instrinental Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 56: 261-272.

82NAD 02 R. A. Nadkerni , R. I. Botto, and S. E. Smith (1982) Con^rison of Two Atomic Spectroscopic Methods for Elemental Analysis of Geological Materials, Atomic Spectroscopy,

3: 180-18A.

82LIN 03 P. C. Lindalh and A. M. Bishop (1982) Determination of Trace Elements in Coal by an Oxygen Bomb Combusiton/Atomic Absorption Spectrophotometric

Method, Fuel, 61: 658-562.

82L0 01 J. M. Lo, J. C. Wei, H. H. Yang, and S. J. Yeh (1982) Preconcentration of Hg nith Lead Diethyldithiocarbamate for Neutron Activation Analysis of Biological and Environmental

Samples, Journal of Radioanalytical Chemistry, 72: 571-585.

82NYG 01 D. D. Nygaard and J. H. Lowry (1982) Sample Digestion Procedures for Simultaneous Determination

of As, Sb, and Se by Inductively Coupled Argon Plasma Emission Spectrometry with Hydride Generation, Analytical

Chemistry, 54: 803-807. %

820MA 01 M. Omar and H. J. M. Bowen (1982) Pre-concentration of Environmental Tin and its Determination

using Catechol Violet, Analyst, 107: 654-658.

82LY0 01 D. J. Lyons and R. L. Roofayel (1982) Determination of Molybdemjn in Plant Material using

Inductively Coi^jled Plasma Emission Spectroscopy, Analyst,

107: 331-334.

820UE 01 J. U. Owens, E. S. Gladney, and D. Knab (1982) Determination of Boron in Geological Materials by

Inductively Coupled Plasma Emission Spectrometry, Analytiea Chimica Acta, 135: 169-172.

82MAT 01 K. Matsunoto and K. Fuwa (1982) Molecular Emission Spectrometry with Hydride Generation for Determination of Subnanogram Amounts of Arsenic, Analytical

Chemistry, 54: 2012-2015.

82MAT 02 K. Matsunoto, M. Nishio, Y. Misaki, and K. Terada (1982) Decomposition of Tin(IV) Oxide, Antimony(III) Oxide, and Bismuth(III) Oxide by Fusion with Ammoniin Iodide and its Application for Analysis of Environmental Samples, Bunseki

(Cagaku, 31: 141-145.

82MAT 04 K. Matsunoto, Y. Misaki, K. Hayashi, and K. Terada (1982) Decomposition of Titaniim Dioxide and Zirconitm Dioxide by Fusion with Ammonium Hydrogen Sulfate, Fresenius Zeitschrift

fur Analytische Chemie, 312: 542-543.

82MAY 01 T. U. May (1982) Recovery of Endogenous Selenitm from Fish Tissue by Open System Dry Ashing, Journal of the Association of Official Analytical Chemists, 65: 1040-1145.

82MCG 01 J. A. McGynn and T. D. Rice (1982) Proceedings of a Symposiun on Characteristics of Australian

Coals and their Consequences for Utilization, CSIRO Division

of Fossil Fuels, Sydney; taken from 85CLA 02.

82MIL 01 J. C. Mills, K. Turner, P. Roller, and C. Belcher (1982) Direct Determination of Trace Elements in Coal: Wavelength

Dispersive X-ray Spectrometry with Matrix Correction using

Ccmpton Scattered Radiation, X-ray Spectrometry, 10: 131-137

82PEL 01 P. A. Pel la and J. R. Sieber (1982) Intercomparison of Selected Semi-etrpirical and Fundamental Parameter Interelement Correction Methods in x-ray Spectrometry, X-ray Spectrometry, 11: 167-169.

82PER 02 G. Pershagen, 8. Lind, end N.-E. Bjorklund (1982) Lmg Retention and Toxicity of Some Inorganic Arsenic

Compoinds, Environmental Research, 29: 425-434.

82P0L 01 H. Polkowska-Motrenko, M. Dermelj, and A. R. Byrne (1982) Radiochemical Neutron Activation Analysis of Seleniun using Carbamate Extraction, Radiochemical and Radioanalytical

Letters, 53: 319-328.

82PRE 01 J. R. Preer, B. R. Stephens, and C. W. Bland (1982) Sample Preparation in Determination of Lead in Garden Vegetables by Flame Atomic Absorption Spectrophotometry,

Journal of the Association of Official Analytical Chemists,

65: 1010-1014.

82aUR 01 I. H. Oureshi, M. S. Chaudhary, and S. Ahmad (1982) Trace Element Concentration in Head Hair of the Inhabitants

of the Rawalpindi - Islamabad Area, Journal of Radioanalytical

Chemistry, 68: 209-218.

82RAI 01 T. C. Rains, T. A. Rush, and T. A. Butler (1982) Innovations in Atomic Absorption Spectrophotometry with Electrothermal Atomization for Determining Lead in Foods, Journal of the Association of Official Analytical Chemists,

65: 994-999.

82H0R 01 J. Mortatti, F. Krug, L. Pessenda, and E. Zagatto (1982) Determination of Iron in Natural Waters and Plant Material

with 1,10-phenanthrolinc by Flow Injection Analysis, Analyst

107: 659-663.

82MOR 02 J. S. Morris, H. F. Smith, and R. E. Morrow (1982)

INAA Determination of Seleniim via Se-77m in Plasma, Semen,

and Hair Samples from Beef and Dairy Bulls, Journal of Radioanalytical Chemistry, 69: 473-494.

82MUR 01 R. S. S. Murthy and D. E. Ryan (1982) Rapid Neutron Activation Analysis of Biological Samples

after Removal of Sodiun on Kryptofix 221B Polymer, Analytiea

Chimica Acta, 144: 107-114.

82NAD 01 R. A. Nadkarni (1982) Applications of Hydride Generation-Atomic Absorption

Spectrometry to Coal Analysis, Analytics Chimica Acta,

135: 363-368.

82RIT 01 C. J. Ritter (1982) The Dry-ashing Method of Preparing Sewage Sludge for Cd and Pb Determinations by AAS, American Laboratory, 14(8): 72-73.

82RCD 03 H. Rodriguez-Flores and E. Rodriguez-Castel Ion (1982)

Lead and CaAiiixn Levels in Soil and Plants near Highways and

Their Correlation with Traffic Density, Environmental Pollution, 4B: 281-290.

82ROE 01 K. K. Roe, W. Burnett, K. Kim, and H. Beers (1982)

Excess Protect ini in in Phosphate Nodules from a Coastal

Upwelling Zone, Earth and Planetary Science Letters,

60: 39-46.

82R0E 02 I. Roelandts, G. Robaye, G. Weber, and J. Delbrouck (1982)

Non-destructive Determination of Bromine in Blood Serijn

Sanples using Proton Induced X-ray Emission Spectrometry,

Radiochemical and Radioanalytical Letters, 50: 319-332.

R-32
CODE N REFERENCE CODE N REFERENCE

82SAK 01 M. Sflkata and 0. Shimoda (1982) Atomic Absorption Determination of Heavy Metals in Sediment

by Digestion Method using Teflon- Lined Bont>, Bunseki Kagaku,

31: T81-T86.

82SAR 01 R. C. Sarkar and M. S. Das (1982) Differential Spectrophotometric Determination of Silica in Rocks as ALpha-MoLytxjosi I icic Acid in Presence of Phosphate

and Other Interferences, Analytica Chimica Acta, 134: 401.

82SAT 01 T. Sato and T. Kato (1982) Estimates of Iodine in Biological Materials by Epithermsl Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 68: 175-180.

82SAT 02 R. D. Satzger, C. Clow, E. Bonnin, and F. Fricke (1982) Determination of Background Levels of Lead and Cadnium in Raw Agricultural Crops by using Differential Pulse Anodic

Stripping Voltanmetry, Journal of the Association of Official Analytical Chemists, 65: 987-991.

82SCH 01 P. Schramel and X. Li-Qiang (1982) Determination of Be in the PPB Range in Three Standard

Reference Materials by Inductively Coupled Plasma Atomic Emission Spectrometry, Analytical Chemistry, 54: 1333-1336.

82SCH 03 A. A. Schilt and M. R. di Tusa (1982) Spectrophotometric Determination of Iron and Reducing Agents

with PPTS, A New Uater-soluble Ferroin-type Chromogen of Superior Sensitivity, Talanta, 29: 129-132.

82SCH 04 P. Schramel, X. Li-Ouiang, A. Wolf, and S. Hasse (1982) ICP-Emissionspektroskopie: Ein Analytisches Verfahren zur Klarschlanm und Bodenuberwachung in der Routine, Fresenius Zeitsehrift fur Analytische Chemie, 313: 213-216.

B2SCH 05 J. 0. Schmidt, L. Palgaard, and J. Uestermann (1982) Determination of Boron by Fast Instrimental Neutron Activation Analysis, Journal of Radioanalytical Chemistry,

72: 425-436.

82SEG 01 C. Segebade, M. Kuhl, B. Schmitt, and R. Neider (1982) Some Remarks on the State of Photon Activation Analysis and

the Use of Internal Standards, Journal of Radioanalytical

Chemistry, 72: 665-696.

82SIN 01 S. A. Sinex and G. R. Helz (1982) Entrapment of Zinc and Other Trace Elements in a Rapidly

Flushed Industrialized Harbor, Envi rormental Science and

Technology, 16: 820-825.

82SMI 01 D. H. Smith, J. Walton, H. McKown, and R. Walker (1982)

A Mobile Mass Spectrometry Laboratory for Isctopic Ratio

Measurements of Uranimi and Plutonitm, Analytica Chimica

Acta, 142: 355-359.

82SUB 01 K. S. Subramanian and J. C. Meranger (1982) Rapid Hydride Evolution-Electrothermal Atomisation Atomic

Absorption Spectrophotometric Method for Determining Arsenic

and Seleniun in Hunan Kidney and Liver, Analyst, 107: 157.

82SUL 01 J. R. Sullivan and J. J. Delfino (1982) Determination of Mercury in Fish, Journal of Environmental

Science and Health, A17: 265-275.

82SUZ 01 M. Suzuki and K. Ohta (1982) Reduction of Interferences with Thiourea in the Determination of CactniLiti by Electrothermal Atomic Absorption

Spectrophotometry, Analytical Chemistry, 54: 1686-1689.

82SUZ 02 S. Suzuki and S. Hirai (1982) Determination of Trace Elements in Coal and Fly Ash by Neutron Activation Analysis, Bunseki Kagaku, 31: 443-449.

82SUZ 03 H. Suzuki and K. Ohta (1982) Determination of Strontiun in Biological Samples by Atomic Emission Spectrometry with Electrothermal Atomizetion, fresenius Zeitsehrift fur Analytische Chemie, 313: 34-37.

82TAM 01 G. Tam and G. LaCroix (1982) Dry Ashing, Hydride Generation Atomic Absorption Spectro- metric Determination of As and Se in Foods, Journal of the Association of Official Analytical Chemists, 65: 647-651.

82TER 01 S. Terashima (1982) Determination of Trace Amounts of Tin in Seventy-Three

Geochemical Reference Samples by Atomic Absorption

Spectrometry, Geostandards Newsletter, 6: 77-81.

82TER 02 S. Terashima (1982) Determi rut i on of Trace Amounts of Beryllium fn Geological

Samples by Solvent Extraction and Atomic Absorption

Spectrometry, Bunseki Kagaku, 31: 727-729.

82TER 03 R. Tertian and F. Clsisse (1982) Principles of Quantitative X-ray Fluorescence Analysis,

Heyden, London.

82TH0 02 J. Thomson (1982)

A Total Dissolution Method for Determination of the Alpha

Emitting Isotopes of Uranium and Thoriun in Deep-sea

Sediments, Analytica Chimica Acta, 142: 259-268.

82T1N 01 B. Ting, J. Pagounes, and M. Janghorbani (1982) Radiochemical Neutron Activation Analysis of Stable Isotopes

in Relation to Htinan Mineral Nutrition, Journal of Radioanalytical Chemistry, 70: 133-144.

82UCH 02 H. Uchikawa, R. Furuta, and Y. Mihara (1982) The Determirwtion of Trace Mercury in Solid Fuel by Atomic Absorption Spectrometry, Bunseki Kagaku, 31: 367-372.

82VAN 01 C. Vanoeteren, R. Cornelis, J. Versieck, and J. Hoste (1982) Trace Element Patterns in Hunan Lung Tissues, Journal of Radioanalytical Chemistry, 70: 219-238.

82VER 03 M. Verlinden (1982) On the Acid Decomposition of Human Blood and Plasma for the Determination of Seleniun, Talanta, 29: 875-882.

82VIS 01 P. ViswanatBiam, D. Smick, f. Pisney, and W. Oilworth (1982)

Comparison of Ion Chromatography and Titrimetry for Determination of Sulfur in Fuel Oils, Analytical Chemistry,

54: 2431-2433.

S2V0G 01 J. R. Vogt, C. Graham, M. Glascock, and R. Cobean (1982)

A Study of Mesoamerican Ottsidian Sources using Activation

Analysis, Journal of Radioanalytical Chemistry, 69: 271-289.

82WEI 01 A. Weitz, G. Fuchs, and K. Bachmann (1982) AAS-Bestimnung von Caciniun und Blei in Biologischen Proben

und Bodenproben nach Abtrennung durch Verf luchtigung, fresenius Zeitsehrift fur Analytische Chemie, 313: 38-42.

82WIL 01 J. R. Wilkinson, L. Ebdon, and K. W. Jackson (1982) Determination of Volatile Trace Metals in Ccal by Analytical

Atomic Spectroscopy, Analytical Proceedings of the Royal

Society of Chemistry (London), 19: 305-307.

R-33
CODE N REFERENCE CODE N REFERENCE

82WIL 02 S. A. Wilson and C. A. Gent (1982) The Determination of Fluoride in Geologic Samples by Ion Chromatography, Analytical Letters, 15: 851-864.

82W1L 04 E. V. Williams (1982) Low-temperature Oxygen- Fluorine Radiof reqoency Ashing of Biological Haterals in Teflon Dishes prior to the Determin- ation of Sn, Fe, Pb, and Cr by AAS, Analyst, 107: 1006-1013.

83BET 02 M. Bettinelli (1983) Determination of Fluorine in Environmental Standard Reference Materials with a Fluoride Ion-selective Electrode,

Analyst, 108: 404-407.

83BIR 01 J. R. Bird and E. Clayton (1983) The PIGME Method for Fluorine Determination, Nuclear Instruments and Methods in Physics Research, 218: 525-528.

82YAM 01 T. Yamashige, H. Ida, M. Yamamoto, Y. Shigetomi, and

Y. Yamamoto (1982), Comparison of Acid Digestion Methods

with and without Hydrofluoric Acid for the Determination of

re, Mn, Zn, Pb, Cd, and Ni in Ambient Particulates by Atomic Absorption Spectrometry, Bunseki Kagaku, 32: 169-173.

82ZEI 01 R. Zeisler and R. R. Greenberg (1982) Ultratrace Determination of Platinum in Biological Materials

Via Neutron Activation and Radiochemical Separation, Journal

of Radioanalytical Chemistry, 75: 27-37.

83ADE 01 S. Adeloju, A. Bond, M. Briggs, and H. Hughes (1983) Stripping Voltammetric Determination of Selenium in Biological Materials by Direct Calibration, Analytical

Chemistry, 55: 2076-2082.

83AHM 01 S. Ahmad, M. Chaudhary, A. Mannan, and I. Qureshi (1983) Determination of Toxic Elements in Tea Leaves by Instrumental Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 78: 375-383.

83AHM 02 R. bin Ahmad, J. 0. Hill, and R. J. Magee (1983) Direct Determination of Selenium(IV) in Biological Samples

by Cathodic Stripping Voltanmetry, Analyst, 108: S35-839.

83ALL 01 M. AUegrini, R. Delfanti, M. di Cassa, and E. Orvini (1983) Determination of Iodine in Biological Matrices using a Fast Radiochemical Separation, Radiochemical and Radioanalytical

Letters, 59: 163-170.

83AND 01 D. L. Anderson, G. E. Gordon, W. B. Walters, W. H. Zoller, and R. M. Lindstrom (1983), Neutron- capture Prompt Gamna-ray Activation Analysis, in 83SH0 01, pp. 159-164.

83BLO 01 N. Bloom (1983) Determination of Silver in Marine Sediments by Zeeman .Corrected Graphite Furnace Atomic Absorption Spectroscopy, Atomic Spectroscopy, 4: 204-207.

83BOU 01 P. Bourbon, J. Esclassan, and J. Vandaele (1983) Determination de Traces de Molytxiene par Polarographie

Impulsionncl le du Complexe Hydroxyquinoleine-Molybdene,

Analusis, 11: 341-344.

83B0Y 01 W. V. Boynton and D. H. Hill (1983) Composition of Bulk Samples and a Possible Pristine Clast from Allan Hills A81005, Geophysical Research Letters,

10: 837-840.

83BPN 01 Battelle Pacific Northwest Laboratories (1983) Private Communication, taken from 83LUT 01.

83BRA 01 A. Brandone, P. A. Borroni, and N. Geneva (1983) Determination of Arsenic, CactniKn, and Mercury in Biological

Samples by Neutron Activation Analysis, Radiochemical and Radioanalytical Letters, 57: 83-94.

83BRA 02 P. Bratter, K. P. Berthold, and P. E. Gardiner (1983) The Use of Reference Materials as Standards in the Simultaneous Multielement Analysis of Biological Materials

using Inductively Coupled Plasma Spectrometry, Spectrochimica Acta, 38B: 221-228.

83BR0 01 A. Broekman and J. G. van Raaphorst (1983) Stable Isotope Dilution Analysis by Thermal Ionization Mass

Spectrometry, Fresenius Zeitschrift fur Analytische Chemie,

315: 30-33.

83AND 02 J. R. Anderson (1983) Petrology of a Portion of the Eastern Penninsular Ranges Mylonite Zone, Southern California, Contributions to Mineralogy and Petrology, 84: 253-271.83BR0 02 R. J. Brown (1983) Determination of Trace Metals in Petroleun and Petroleun

Products using an Inductively Coupled Plasma Optical Emission Spectrometer, Spectrochimica Acta, 38B: 283-289.

83ATS 01 I. Atsuya and K. Itoh (1983) The Use of an Inner Miniature Cup for Direct Determination

of Powdered Biological Samples by Atomic Absorption

Spectrometry, Spectrochimica Acta, 38B: 1259-1264.

83BAL 01 A. H. E. Balaes and J. J. Jacobs (1983) The Installation and Coimissioning of a Siemens SRS200

Sequential X-ray Fluorescence Spectrometer, Mintek report

no. M80.

83BAR 02 R. M. Barnes and H. S. Mahanti (1983) Analysis of Bauxite by Inductively Coupled Plasma Atomic

Emission Spectroscopy, Spectrochimica Acta, 38B: 193-197.

83BER 01 C. Berthelot, H. Eschbach, V. Verdingh, and F. Verheyen

(1983), The Homogeneity Control of Reference Materials by

Photon Activation, International Journal of Environmental

Analytical Chemistry, 16: 227-236.

83BET 01 M. Bettinelli (1983) Fusion Procedure for the Trace Metal Analysis of Coal by

Atomic Absorption, Atomic Spectrometry, 4: 5-9.

83BYR 01 R. E. Byrne (1983)

A Rapid Method for the Determination of Arsenic, Cadniun,

Copper, Lead, and Zinc in Airborne Particulates by Flame Atomic Absorption Spectrometry, Analytica Chimica Acta,

151: 187-194.

83CAR 01 G. Carvajal, D. Mahan, D. Goforth, and D. Leyden (1983) Evaluation of Methods based on Acid Extraction and Atomic Absorption Spectrometry for Multielement Determinations in

River Sediments, Analytica Chimica Acta, 147: 133-150.

83CAR 02 E. E. Gary and M. Rutzke (1983) Electrothermal Atomic Absorption Spectroscopic Determination

of Chromiuti in Plant Tissues, Journal of the Association of

Official Analytical Chemists, 66: 850-852.

83CHA 01 D. Chase (1983) Written Communication of Background Information from an

American Laboratory Article, Instrunentation Laboratory,

Andover, Massachusetts.

R-34
CODE N REFERENCE

83CHA 02 C. Chan (198J) Semiautomated Determination of Fluoride in Rocks, American

Laboratory, 15(10): 32-41.

CODE N REFERENCE

83GAR 01 H. F. Garbauskas and J. Wong (1983)

XRF Analysis of Trace Titaniun in Coal Using Fundamental

Parameters, X-ray Spectrometry, 12: 118-120.

83CLA 01 R. N. Clayton and T. K. Hayede (1983) « Oxygen Isotopes in Eucrites, Shgrgottites, Nakhlites, and Chassignites, Earth and Planetary Science Letters, 62: 1-6.

83CRO 01 J. G. Crock, F. E. Lichte, and P. H. Briggs (1983) Determination of Elements in NBS' Geological Reference

Materials SRM 278 and SRM 688 by Inductively Coupled Argon

Plasma Atomic Emission Spectrometry, Geostandards Newsletter

7: 335-340.

83DAN 01 H. S. Dang, H. Desai, D. Jaisual, S. Kayasth, and

S. Somasundaram (1983), A Sequential Multielement Separation

Scheme for Determination of As, Mn, Mo, Cu, and Zn in Human Milk by Neutron Activation Analysis, Journal of Radioanalytical Chemistry, 77: 65-70.

83DEL 01 D. Dellar (1983) Evaluation of the Determination of High Levels of Total

Ca<±iiiiJii in Foodstuffs using Flame Atomic Absorption

Spectrophotometric Measurement, Analyst, 108: ^9-763.

8300U 01 0. J. Douglas, E. S. Ouan, and R. G. Smith (1983) Elemental Analysis with an Atmospheric Pressure Plasma

(MIP, ICP)/Ouadrupole Mass Spectrometer System, Spectrochimica Acta, 38B: 39-48.

83D0U 02 D. Douglas, G. Rosenblatt, and E. Ouan (1983) Inductively Coupled Plasma/Mass Spectrometry -- A New Technique for Trace Element Analysis, Trace Substances in Environmental Health, 17: 385-390.

83ELA 01 A. El-Ahraf, W. V. Willis, and F. Moses (1983) Determination of the Concentration of Metals in Animal

Feeds: Cd, Cr, Cu, Fe, Mg, Ni, Pb, and Zn in Dairy Cattle

Feed, Manure, and Processed Manure, Biological Trace Element

Research, 5: 129-137.

83ELK 01 E. A. Elkhatib, 0. L. Bennet, and R. J. Wright (1983) Determination of Total Arsenic in Soil by Differrential Pulse Polarography, Soil Science Society of America

Journal, 47: 836-838.

83G0G 01 R. Gogucl (1983) Improved Background Correction in the Analysis of Cadmium by

Flame Atomic Absorption, Geostandards Newsletter, 7: 341-344

83GRE 01 R. R. Greenberg and H. H. Kingston (1983) Trace Element Analysis of Natural Water Samples by Neutron Activation Analysis with Chelating Resin, Analytical

Chemistry, 55: 1160-1165.

83GRE 02 R. R. Greenberg (1983) Improved Radiochemical Procedures for High Sensitivity Measursments of Ultratrace Concentrations of Tin and Mercury

in 83SH0 01, pp. 140-141.

83GR0 02 Z. Grobenski, D. Weber, 3. Welz, and J. Wolff (1983) Determination of Cesiun and Rubidiim by Flame and Furnace Atomic Absorption Spectrometry, Analyst, 108: 925-932.

83GUN 01 M. F. Guns (1983)

La Determination du Soufre Total Dans les Vegeteux par Fluorescence des Rayons X, Analusis, 11: 295-298.

83HER 01 J. A. Hern, G. K. Rutherford, and G. W. van Loon (1983) Determination of Chloride, Nitrate, Sulfate, and Total Sulfur in Environmental Samples by Single-colimn Ion Chromatography, Tolanta, 30 : 677-M2.

83HOE 01 H. Hoenig and P. van Hoeyweghen (1983) Effect de L'Acide Ascorbique sur la Determination du Plomb

dans des Matrices Vegetales par ETA-AAS, Spectrochimica Acta 38B: 1179-1182.

83H0F 01 D. Hoffer, I. B. Brenner, and L. Halicz (1983) Application of a Low Power Ar I CP for the Analysis of Major and Minor Elements in Phosphate Rocks, Geological Survey of Israel, Geochemistry Division (Jerusalem), Report No. 12.

83H0L 01 W. Holak (1983) Determination of Copper, Nickel, and Chromium in Foods, Journal of the Association of Official Analytical Chemists,

66: 620-622.

83EPS 01 M. S. Epstein (1983) Determination of Ultratrace Levels of Lead in Reference

Fuels by Graphite Furnace Atomic Absorption, Atomic

Spectrometry, 4: 62-63.

eSESA 01 S. Esala, E. Vuori, and L. Niinisto (1983) Determination of Nanogram Amounts of Fluorine in Breast Milk by Ashing-dif fusion Method and the Fluoride Electrode, Mikrochimica Acta tWien] , 19831: 155-165.

83FAG 01 F. Fagioli and S. Landi (1983) Evaluation of a New Method for the Determination of Elements

in Vegetable Foods and Feeds by Atomic Absorption

Spectroscopy with Sampling of Carbonaceous Slurry,

Analytical Letters, 16: 1435-1447.

83FAR 01 J. G. Farmer and M. J. Gibson (1983) Erratun to Direct Determination of Cadniim, Chromiun,

Copper, and Lead in Siliceous Standard Reference Materials, Atomic Spectrometry, 4: 112.

83FRA 01 A. Frank and L. R. Petersson (1983) Selection of Operating Conditions and Analytical Procedure

in Multi -metal Analysis of Animal Tissues by D.C. Plasma

Atomic Emission Spectroscopy, Spectrochimica Acta, 38B: 207.

83HSU 01 C.-G. Hsu and D. C. Locke (1983) Digestion Methods for Determination of Cednium and Lead

in Organic and Silica-rich Sediments, Analytica Chimica

Acta, 153: 313-318.

83ICH 01 S. Ichinoki, M. Yamazaki, and T. Morita (1983) Simultaneous Determination of Lead, Nickel, and Copper in Orchard Leaves by High Performance Liquid Chromatography

Followed by Solvent Extraction, Bunseki Kagaku, 32: 285-287.

83JAC 01 J. S. Jacobson (1983) Written Comnunication, Boyce Thompson Institute for Plant

Research, Cornell University, Ithaca, New York.

83JEK 01 D. R. Jenke and R. Woodriff (1983) Continued Development of Direct Aerosol Introduction in Constant Teirperature Furnace Atomic Absorption Spectroscopy, Applied Spectroscopy, 37: 470-472.

83JER 01 R. E. Jervis, S. Landsberger, S. Aufreiter, J. van Loon,

R. Lecomte, and S. Monaro (1983), Trace Elements in Wet Atmospheric Deposition: Application and Conparison of PIXE,

INAA, and Graph i te- Furnace AAS Techniques, International

Journal of Environmental Analytical Chsnistry, 15: 89-106.

R-35
CODE N REFERENCE CODE N REFERENCE

83KAT 01 M. Katoh and K. Kudo (1983) Substoichiometric Determination of Lanthanum by using EDTA

and SHydroxyquinol ine, Journal of Radioanalytical Chemistry

79: 23-34.

83<AT 02 T. Katami, T. Hayakawa, M. Furukawa, and S. Shibata (1983) Extraction and Spectrophotometric Determination of Cobalt in

Coal Fly Ash using 2- [2- <3,5-Dibro(nopyridyl )azo] -5-dimethyl •

aminobenzoic Acid, Analyst, 108: 864-869.

83<EI 01 J. P. Keilsohn, R. D. Oeutsch, and G. M. Hieftje (1983) The Use of a Microarc Atomizer for Sample Introduction into an Inductively Coupled Plasma, Applied Spectroscopy, 37: 101

83L0S 01 R. D. Loss, K. J. R. Rosman, and J. R. de Laeter (1983)

Ag, Te, and Pd in 17 Geochemical Reference Materials by Mass Spectrometric Isotope Oi lution Analysis, Geostandards

Newsletter, 7: 321-324.

83L0V 01 M. A. Lovell and J. G. Farmer (1983) The Determination of Arsenic in Soil and Sediment Digests by

Graphite Furnace Atomic Absorption Spectrometry,

International Journal of Environmental Analytical Chemistry,

14: 181-192.

83LUT 01 G. J. Lutz (1983) 1-129 Analysis, in 83SH0 01, pp. 142-143.

83KEL 01 W. R. Kelley and J. D. Fassett (1983) Determination of Picogram Quantities of Uraniun in Biological Tissues by Isotope Dilution Thermal Ionization Mass Spectrometry with Ion Counting Detection, Analytical

Chemistry, 55: 1040-1044.

83KEN 04 W. T. Kennedy, W. B. Hubbard, and J. C. Tarter (1983) Rapid Analysis of Fluorine in Geological Samples with

Ion Chromatographic Detection, Analytical Letters,

16: 1133-1148.

83KIM 01 K. H. Kim and U. C. Burnett (1983)

Gatnna-ray Spectrometric Determination of Uranicm-series

Nuclides in Marine Phosphorites, Analytical Chemistry,

55: 1796-1800.

83KNA 01 D. Knab (1983) Written Communication, Los Alamos National Laboratory, New Mexico.

83KOH 01 T.-S. Koh and T. H. Benson (1983) Metals and Other Elements: Critical Re-appraisal of Fluorometric Method for Determination of Seleniun in Biological Materials, Journal of the Association of Official Analytical Chemists, 66: 918-925.

83K0L 01 H. W. Kolroer and S. E. Raptis (1983)

SeleniLTi Content of Geochemical Reference Samples Determined

by a Simple Method at the ng/g Level, Geostandards

Newsletter, 7: 315-318.

83KUM 01 T. Kiiramaru, H. Matsuo, and M. Ikeda (1983) Effect of Continuous Prereduction by Heating with Potassiun

Iodide and Hydrochloric Acid for Determining Arsenic (III,

V) by the Continuous Hydride Generation- Atomic Absorp-on

Spectrometry using Sodiun Tetrahydroborate Reduction,

Bunseki Kagaku, 32: 357-361.

83LI 01 M. Li and R. H. Filby (1983) Determination of Sulfur in Fly Ash and Fuel Oil Standard Reference Materials by Radiochemical Neutron Activation Analysis and Liquid Scintillation Counting, Analytical

Chemistry, 55: 2336-2340.

83LIN 01 R. H. Lindstrom (1983) Internal NBS Comnunication, taken from 83GRE 01.

83MAD 01 P. P. Madsen, I. Drabaek, and J. Sorensen (1983) The Determination of Copper and Lead in Sediments by Potentiometric Stripping Analysis, Analytica Chimica Acta,

151: 479-482.

83MAH 01 U. A. Maher (1983)

A Decomposition Procedure for the Determination of Arsenic

in Marine Samples, Talanta, 30: 534-536.

83MAH 03 K. 1. Mahan and D. E. Leyden (1983) Simultaneous Determination of Sixteen Major and Minor

Elements in River Sediments by Energy-dispersive X-ray

Fluorescence Spectrometry after Fusion in Lithiim

Tetraborate Glass, Analytica Chimica Acta, 147: 123-131.

83MAH 04 U. A. Maher (1983) Spectrophotometric Determination of Arsenic in Biological

Tissues and Sediments after Digestion with Nitric, Sulfuric, and Perchloric Acids and Pre-concentration by Zinc Colimn

Arsine Generation and Trapping, Analyst, 108: 939-943.

83MAH 05 H. S. Mahanti and R. M. Barnes (1983) Determination of Trace Elements in Coal and Other Energy Related Materials by Inductively Coupled Plasma Emission Spectrometry after Collection on a Poly(dithiocarbamate)

Resin, Analytica Chimica Acta, 149: 395-400.

83MAR 03 Y. Maruyama and Y. Nagaoka (1983) Determination of Arsenic in Biological Materials using

Amnoniuii Molybdate Labeled with Mo-99, Journal of Radioanalytical Chemistry, 76: 81-85.

83MAR 04 J. Marshall, D. Littlejohn, J. Ottaway, J. Harnly,

N. Miller-Ihli, and T. C. O'Haver (1983), Simultaneous Multielement Analysis by Carbon Furnace Atomic

Emission Spectrometry, Analyst, 108: 178-188.

83MAR 05 R. W. Marts and J. J. Blahe (1983) Mixed Acid Solubilization Procedure for Determination of

Total Mercury in Food Samples, Journal of the Association

of Official Analytical Chemists, 66: 1421-1423.

83HAS 02 K. Masunoto and M. Yagi (1983) Charged Particle Activation Analysis of Phosphorus in

Biological Materials, Journal of Radioanalytical Chemistry,

78: 233-239.

83L1N 02 R. M. LindstroiTi, R. R. Greenberg, and R. F. Flenming (1983) Multielement Analysis of Coal Standard Reference Materials,

in 83SH0 01, pp. 147-148.

83LIP 01 H. J. Lippolt, H. Schleicher, and I. Raczek (1983)

Rb-Sr Systematics of Permian Volcanites in the Schwarzwald

(SW-Germany): Part I. Space of Tiirie Between Plutonism and

Late Orogenic Volcanism, Contributions to Mineralogy and

Petrology, 84: 272-280.

B3MAT 02 I. MatSLtara (1983) Determination of Trace of Holybdenuti in Biological Materials

by a Confcined Ion Exchange-Spectrophotometric Method,

Bunseki Kagaku, 32: T97-T99.

83MCC 02 J. T. McCaffrey, M.-L. W. Uu, and R. G. Michel (1983)

Discrimination Against Atomic-emission Spectral

Interferences in Wavelength-modulated Continuim Source

Excited Flame Atomic-fluorescence Spectrometry, Analyst,

108: 1195-1208.

R-36
CODE N REFERENCE CODE N REFERENCE

83MIL 01 J. C. Hi Us (1983) Determination of Boron, Berylliun, and LUhiun in Coal Ash and Geological Materials by Spark Optical Emission

Spectrometry, Analytica Chimica Acta, ISA: 227-234.

83NAD 01 R. A. Nadkarni and D. M. Pond (1983) Applications of Ion Chromatography for Determination of Selected Elements in Coal and Oil Shale, Analytica Chimica

Acta, U6: 261-266.

83ND1 01 C. L. Ndiokwere, V. P. Guinn, and D. Burtner (1983) Trace Elemental Composition of Nigerial Coals Measured by Neutron Activation Analysis, Journal of Radioanalytical

Chemistry, 79: 123-128.

83N0R 01 J. D. Norman, L. Stimpe, J. Triitn, and F. Johnson (1983) Argon Plasma Emission Spectrometry of Uraniim in Phosphatic

Materials, Journal of the Association of Official Analytical

Chemists, 66: 949-951.

830BR 01 I. Obrusnik and S. Posta (1983) Instrumental Neutron Activation Analysis of NBS 1633A Fly

Ash and 1632A Bitiminous Coal Reference Samples with the use

of Short Irradiations, Geostandards Newsletter, 7: 291-293.

830HM 01 T. Ohmori (1983) Spectrophotometric Determination of a Small Amount of Aliminiun with Stilbazo and Zephiramine in Alkaline

Solution; Determination of Aluninium in Standard Rocks and

Cement, Bunseki Kagaku, 32: 485-487.

830LI 01 E. de Oliveira, J. W. McLaren, and S. S. Berman (1983) Simultaneous Determination of Arsenic, Antimony, «nd

Seleniuit in Marine Samples by Inductively toupied Plasma

Atomic Emission Spectrometry, Analytical Chemistry, 55:2047.

830LS 02 G. J. Olson, F. E. Brinckman, and J. A. Jackson (1983) Purge and Trap Flame Photometric Gas Chromatography

Technique for the Speciation of Trace Organotin and Organosulfur Compounds in Hunan Urine Standard Reference

Material, International Journal of Environmental Analytical

Chemistry, 15: 249-261.

83PEL 01 P. A. Pel la, H. Kingston, J. Sleber, and L.-Y. Feng (1983) Effect of Sample Dissolution Procedures on X-ray Spectrometric Analysis of Biological Materials, Analytical

Chemistry, 55: 1193-1194.

83PRU 01 E. Prusikowska, P. Barrett, R. Ediger, and G. Wallace (1983) Determination of Arsenic and Seleniun using Hydride System Combined with ICP, Atomic Spectroscopy, 4: 94-97.

83RAM 01 G. 0. Ramseyer and G. H. Morrison (1983) Relative Sensitivity Factors in Quantitative Secondary Ion

Mass Spectrometry Analysis of Biological Reference Materials

Analytical Chemistry, 55: 1963-1970.

83RAP 01 S. E. Raptis, G. Knapp, and A. P. Schalk (1983)

Novel Method for the Decompostion of Organic and Biological Materials in an Oxygen Plasma Excited at High Frequency for

Elemental Analysis, Fresenius Zeitschrift fur Analytische

Chemie, 316: 482-487.

83SAN 02 R. W. Sanders, K. Olsen, W. Weimer, and <. Nielson (1983) Multielement Analysis of Unweighed Oil Samples by X-ray

Fluorescence Spectrometry with Two Excitation Sources, Analytical Chemistry, 55: 1911-1914.

83SAR 01 B. Sarx and K. Sachmann (1983) Speciation von As-Verbindungen durch Verf luchtigung bus Festproben, Fresenius Zeitschrift fur Analytische Chemie,

316: 621-626.

83SCH 03 P. Schramel and X. Li-Qiang (1983) Determination of 14 Elements in Biological Samples by Simultaneous Inductively Coupled Plasma Atomic Emission Spectrometry using Standard Reference Materials as Multielement Standards, Fresenius Zeitschrift fur Analytische Chemie, 314: 671-677.

83SCH 04 P. Schramel (1983) Consideration of Inductively Coupled Plasma Spectrometry for Trace Element Analysis in the Bio-medical and Environmental

Fields, Spectrochimica Acta, 38B: 199-206.

83SH0 01 F. J. Shorten, editor (1983) NBS Reactor: Suimary of Activities July 1981 through

June 1982, NBS Technical Note.

83SIR 01 C.-I. Siripone, G. D. Wals, and H. A. Das (1983) Neutron Activation Analysis of Dry Biological Materials

using Mineralization with a Saturated Mg(N03)2 Solution and Scavenging by Activated Carbon, Journal of Radioanalytical

Chemistry, 79: 35-41.

eSSIU 01 K. U. M. Siu and S. S. Berman (1983) Determination of Seleniun in Marine Sediments by Gas Chromatography with Electron Capture Detection, Analytical

Chemistry, 55: 1603-1605.

83STE 05 J. U. Steiner and H. L. Kramer (1983) In-situ Gaseous Pre- treatment of Liver Extracts in a Modified Carbon Rod Atomizer During the Determination of Cadmiun and Lead, Analyst, 108: 1051-1059.

83TAK 01 Y. Takahashi and M. Rey (1983) A Dedicated XRF Analyzer for Sulfur in Oils, American

Laboratory, 15(11): 27-42.

83TAK 02 H. Takagi, T. Kimura, K. Iwashima, and N. Yamagata (1983) A Simple and Rapid Method for the Determination of Iodine

in Rice Samples by Radiochemical Neutron Activation

Analysis, Bunseki Kagaku, 32: 513-515.

83TER 01 S. Terashima (1983) Determination of Berylliun in Eighty Geological Reference

Samples by Atomic Absorption Spectrometry, Geostandards

Newsletter, 7: 295-299.

83TJI 01 P. S. Tjioe, K. Volkers, J. Kroon, and J. de Goeij (1983) Distribution Patterns of Rare-earth Elements in Biological Materials Evaluated by Radiochemical Neutron Activation

Analysis, Journal of Radioanalytical Chemistry, 80: 129-139.

83UCH 01 H. Uchikawa, R. Furuta, and Y. Mihara (1983) Determination of Phosphorus in Ceramic Materials and

Ceramic Products by Inductively Coupled Plasma Atomic

Emission Spectroscopy, Bunseki Kagaku, 32: 291-297.

83UCH 02 H. Uchikawa, R. Furuta, and Y. Mihara (1983)

Determination of Cadniun in Ceramic Materials and Ceramic

Products by Inductively Coupled Plasma-Atomic Emission

Spectroscopy, Bunseki Kagaku, 32: 675-677.

83VAL 01 G. Valentine (1983) Procedures for Analysis of Silicate Rocks and Minerals at

Los Alamos National Laboratory by X-ray Fluorescence,

Los Alamos National Laboratory report LA-9663-MS.

R-37
CODE M REFERENCE CODE N REFERENCE

83WEI 02 S. H. Ueissman, R. L. Carpenter, and G. J. Newton (1983) Respirable Aerosols from Fluidized Bed Coal Cotnbustion. 3: Elemental Compositon of Fly Ash, Environmental Science and Technology, 17: 65-70.

83XIA 01 S. Xiao-quan, N. Zhe-ming, and Z. Li (1983) Determination of Arsenic in Soil, Coal Fly Ash, and Biological Samples by Electrothermal Atomic Absorption with Matrix Modification, Analytica Chimica Acta, 151: 179-185.

83YAN 01 M. Yanagisawa, H. Suzuki, K. Kitagaua, and S. Tsuge (1983) Separative Column Atomizer (SCA) for Direct Analysis by Atomic Absorption Spectrometry: GC Separtion Characteristics

Spec trochi mica Acta, 38B: 1U3-11A9.

84AB0 01 M. Abdullah, IC. Fuwa, and H. Haraguchi (1984) Simultaneous Multielement Analysis of Microliter Volumes of Solution Samples by Inductively Coupled Plasma Atomic Emission Spectrometry Utilizing a Graphite Cup Direct Insertion Technique, Spectrochimica Acta, 39B: 1129-1139.

84ADE 01 S. B. Adelouju, A. M. Bond, and M. H. Briggs (1984) Critical Evaluation of Some Wet Digestion Methods for the Stripping Voltamnetric Determination of Seleniun in Biological Materials, Analytical Chemistry, 56: 2397-2401.

84ADE 02 S. B. Adeloju, A. M. Bond, and M. H. Briggs (1984) Assessment of Differential -pulse Adsorption Voltammetry for the Simultaneous Determination of Nickel and Cobalt in Biological Materials, Analytica Chimica Acta, 164: 181-194.

84ADE 03 S. B. Adeloju, A. M. Bond, and M. L. Noble (1984) Evaluation of Some Dry Ashing Methods for Anodic Stripping Voltamnetric Determination of CadmiLin and Lead in Biological Materials, Analytica Chimica Acta, 161: 303-314.

84AHL 01 H. S. Ahlberg, I. Fangmark, and L. E. Carlsson (1984) Elemental Particle Size Distribution in Coal Fly Ash Determined by PIXE Analysis of Thick Samples, Nuclear

Instrunents and Methods in Physical Research, 231: 511-515.

84ALF 01 G. Alfthan (1984)

A Micromethod for the Determination of Seleniuti in Tissues

and Biological Fluids by Single- test- tube Fluorimetry,

Analytica Chimica Acta, 165: 187-194.

84BLA 01 W. M. Blakemore, P. H. Casey, and U. R. Collie (1984) Simultaneous Determination of 10 Elements in Wastewater,

Plasma, and Bovine Liver by Inductively Coupled Plasma Emission Spectrometry with Electrothermal Atomiiation,

Analytical Chemistry, 56: 1376-1379.

84B0R 01 T. Bornhorst, U. Rose, and S. Wolfe (1984) Gold Content of Eleven French Goechemical Reference Sanples, Geostandards Newsletter, 8: 1-2.

84B0T 01 R. I. Botto (19S4) Quality Assurance in Operating a Multielement ICP Emission Spectrometer, Spectrochimica Acta, 39B: 95-113.

84BRA 01 N. Braun and M. Metzger (1984) Umweltanalytische Nickel -Bestimmung durch Adsorptions Voltammetrie mit der Queksi Iberf i Imelektrodc, Fresenius Zeitschrift fur Anatytische Chemie, 318: 321-326.

84BRA 02 P. Bratter and P. Schramel, editors (1984) Trace Element Analytical Chemistry in Medicine and Biology,

Proceedings of the Third International Workshop, Neuherberg,

Federal Republic of Germany, Walter de Gruyter & Company,

Berlin, Vol. 3.

84BR0 03 A. Broekman and J. G. van Raaphorst (1984) Stable Isotope Dilution Analysis by Thermal Ionization

Mass Spectrometry (II): The Determination of Cd and Cu, Fresenius Zeitschrift fur Analytische Chemie, 318: 398-401.

S4BUS 01 G. Buso, P. Colautti, G. Moschini, H. Xusheng, and

B. Stievano (1984), High Sensitivity PIXE Determination of Seleniun in Biological Samples using a Preconcentration

Technique, Nuclear Instrunents and Methods, 231: 177-180.

84BYR 01 A. R. Byrne (1984) A Simple Radiochemical Procedure for Analysis of Molybdernjm and Tungsten in Biological Materials by Radiochemical Activation Analysis, in 84BRA 02, pp. 505-511.

84BYR 02 A. R. Byrne, M. Dermelj, L. Kosta, and M. Tusek-Znidaric

(1984), Radiochemical Neutron Activation Analysis in the Standardization of Trace Elements in Biological Reference Materials at the Nanogram Level. Mikrochimica Acta [Wien],

19841: 119-126.

84ALk 01 A. Al-Kinai, D. Watt, B. East, and I. Harris (1984) Minor and Trace Analysis of Gallstones, Analyst, 109: 365.

84BAR 02 R. T. Barber, P. J. Whaling, and D. M. Cohen (1984) Mercury in Recent and Century-old Deep-sea Fish, Environmental Science and Technology, 18: 552-555.

84BAR 03 P. Barrett and E. Purszkowska (1984) Use of Organic Solvents for Inductively Coupled Plasma

Analyses, Analytical Chemistry, 56: 1927-1930.

84BAU 01 J. Bauslaugh, B. Radziuk, K. Saeed, and Y. Thomassen (1984)

Reduction of Effects of Structured Non-specific Absorption

in the Determination of Arsenic and Seleniun by Electrothermal Atomic Absorption Spectrometry, Analytica

Chimica Acta, 165: 149-157.

84BEH 01 H. Bem and D. E. Ryan (1984) Determination of Seven Trace Elements in Natural Waters by

Neutron Activation Analysis after Preconcentration with

1-(2-Pyridylazo)-2-naphthol, Analytica Chimica Acta, 166:189

84BIS 01 S. Biswas, M. Khal iquezzaman, H. Islam, and A. tCahn (1984)

The Use of a Single Multielement Standard for Trace Analysis

in Biological Materials by External Beam PIXE, Nuclear

Instrunents and Methods in Physical Research, 231: 337-342.

84CEL 01 I. Celenk and F. Ozek (1984) Simultaneous Neutron Activation Determination of Alunina

and Silica in Geological Samples using a 5 Ci Pu-Be Source,

Journal of Radioanalytical and Nuclear Chemistry, 85: 83-90.

84CHA 02 M. S. Chaudhary, S. Ahmad, A. Mannan, and I. Qureshi (1984)

INAA of Toxic Elements in Coal and Their Transfer into Environments, Journal of Radioanalytical and Nuclear

Chemistry, 83: 387-396.

84CLE 01 B. E. Cleveriger, E. Hinderbcrger, D. Yates, and W, James

(1984), Analysis for Trace Elements in Magnetohydrodynamic

(MHD) Pilot Power Plant Effluents, Environmental Science arid

Technology, 18: 253-257.

84CUB 01 M. J. S. Cubells, M. G. Cuiogeda, and L. A. Querada (1984)

Rapid Determination of Copper, Iron, and Zinc in Liver

Biopsies, Atomic Spectroscopy, 5: 217-221.

84DAS 01 S. Dasgupta, B. Sinha, and N. S. Rawat (1984)

Direct Coirplexometric Determination of Aluninium and

Moderate to Low Amounts of Titaniun and Iron using Tartaric

Acid as a De-masking Agent, Analyst, 109: 39-41.

R-38
CODE N REFERENCE REFERENCE

S^OEL 01 R. Oelfanti, M. OiCasa, M. Gallorini, and E. Orvini (198«)

Five Years Activity in Determining Trace Elements for the Certification of Standard Reference Materials by Neutron

Activation Analysis, Mikrochimica Acta [Wien}, 19841: 239.

84G0H 01 S. Gohda, H. Yamazaki, and H. Kataoka (1984) Determination of Molytxienum in Environmental Materials by Polarized Zeeman Atomic Absorption Spectrophotometry with Graphite Furnace, Bunseki Kagaku, 33: 410-412.

840RA 01 I. Drabaek and V. Carlsen (1984) Conparison of Different Analytical Techniques for the Determination of Organic Mercury, International Journal of Environmental Analytical Chemistry, 17: 231-239.

84FAR 01 J. J. Fardy and G. D. HcOrist (1984) Determination of Iodine in Milk Products and Biological Standard Reference Materials by Epithermal Neutron Activation Analysis, Journal of Radioanalytical and Nuclear

Chemistry, 87: 239-246.

84FAR 02 J. J. Fardy, G. D. McOrist, and T. M. Florence (1984) Rapid Radiochemical Separation in Neutron Activation

Analysis, Part 1: The Use of C-18 Borxied Silica Gel and Selective Complexation for Determination of Manganese,

Copper, and Zinc in Biological Materials, Analytica Chimica

Acta, 159: 199-209.

84FAS 01 J. D. Fassett, L. J. Powell, and L. J. Moore (1984) Determination of Iron in Serum and Water by Resonance

Ionization Isotope Dilution Mass Spectrometry,

Analytical Chemistry, 56: 2228-2233.

54FEN 01 X. Feng and D. E. Ryan (1984) Combination Collectors in Adsorption Colloid Flotation for Multielement Determination in Waters by Neutron Activation,

Analytica Chimica Acta, 162: 47-55.

84F0G 01 T. R. Fogg and R. C. Seeley (1984) ICP-OES Analysis of Atmospheric Aerosol Patricles, American Laboratory, 16 (12): 36-39.

84FUD 01 N. Fudagawa (1984) Determination of Lead by Atomic Absorption Spectrometry

with Tungsten Ribbon Atomizer, Bunseki Kagaku, 33: 301.

&4FLID 02 N. Fudagawa and A. Kawase (1984) Elimination of Nitric Acid Interference in Tungsten Ribbon

Atomic Absorption, Bunseki Kagaku, 33: 331.

84G0L 01 S. S. Goldich (1984) Determination of Ferrous Iron in Silicate Rocks, Chemical Geology, 42: 343-347.

84GRE 01 R. J. Green and C. J. Asher (1984) Measurement of Sub-microgram Amounts of Nickel in Plant Material by Electrothermal Atomic Absorption Spectroscopy,

Analyst, 109: 503-505.

84HAN 01 A. L. Hanson, H. W. Kraner, R. E. Shroy, and K. Jones (1984) Measurement of the Fluorine Content of Three NBS Standard

Reference Materials by use of the F- 19(P,P'gamma)F - 19 Reaction, Nuclear Instrunents and Methods in Physical Research, 232: 401-403.

84HAR 01 J. M. Harnly and J. S. Kane (1984) Optimization of Electrothermal Atomization Parameters for Simultaneous Multielement Atomic Absorption Spectrometry,

Anaytical Chemistry, 56: 48-54.

84HAR 02 J. M. Harnly, N. Miller-Ihli, end T. O'Haver (1984) Simultaneous Multielement Atomic Absorption Spectrometry

with Graphite Furnace Atomization, Spectrochimica Acta,

39B: 305-320.

84HEA 01 J. B. Headridge and I. M. Riddington (1984) Determination of Silver, Lead, and Bismuth in Glasses by Atomic Absorption Spectrometry with Introduction of Solid Samples into Furnaces, Analyst, 109: 113-118.

84HER 01 J. L. Hern (1984) Determination of Total Sulfur in Plant Materials using an Automated Sulfur Analyzer, Communications in Soil Science

and Plant Analysis, 15: 99-107.

84HIG 01 M. D. Higgins (1984) Abundance of Boron in International Geochemical Standards

by Prompt -gamma Neutron Activation Analysis, Geostandards

Newsletter, 8: 31-34.

84GIB 01 R. S. Gibson and C. A. Scythes (1984) Chromiun, Seleniun, and Other Trace Element Intakes of a Selected Sample of Canadian Premenopausal Women, Biological

Trace Element Research, 6: 105-116.

84HIL 01 L. R. Hilpert, G. D. Bryd, and C. R. Vogt (1984) Selectivity of Negative Ion Chemical Ionization Mass Spectrometry for Benzo[a]pyrene, Analytical Chemistry,

56: 1842-1846.

84GLA 01 E. S. Gladney, D. B. Curtis, end D. R. Perrin (1984) Determination of Boron in 35 International Geochemical Reference Materials by Thermal Neutron Capture Prompt Garma-ray Spectrometry, Geostandards Newsletter, 8: 43-46.

84GLA 02 E. S. Gladney, C. Burns, D. Perrin, R. Robinson, and D. Knab

(1984), Quality Assurance for Environmental Analytical

Chemistry: 1982, Los Alamos National Laboratory report

LA-9950-HS.

84HIR 01 S. Hirata (1984) Simultaneous Determination of Multielement in Standard Silicate Rocks and Sediments by Inductively Coupled Plasma Atomic Emission Spectrometry, Bunseki Kagaku, 33: T66-T68.

84HIR 02 K. Hirayama and N. Unohara (1984)

A New Sensitive Catalytic Method for Determination of Ultratrace Mang8nese( 1 1 ) based on Oxidation of N,N Diethyl* Aniline by Potassiim Periodate, Bunseki Kagaku, 33: E517.

84GLA 07 E. S. Gladney, D. Perrin, R. Robinson, and P. Truj i I lo{ 1984)

Multitechnique Determination of Elemental Concentrations

in NBS Urban Air Particulate SRM 1648 and Evaluation of its

use for Quality Assurance, Journal of Radioanalytical

Chemistry, 83: 379-386.

84GLA 11 E. S. Gladney, C. E. Burns, D. R. Perrin, R. D. Robinson, and N. Raybold (1984), Quality Assurance for Environmental

Analytical Chemistry: 1983, Los Alamos National Laboratory

report LA-10115-MS.

84H0F 01 D. Hoffer, I. B. Brenner, and L. Halicz (1984) Application of an Argon ICP for the Analysis of the Major

and Minor Elements in Phosphate Rocks and Related Minerals,

ICP Information Newsletter, 9: 494-509.

84HU0 01 V. Hudnik, M. Marol t -Gomi seek, and S. Gomiscek (1984)

The Determination of Trace Metals in Hunan Fluids and

Tissues: Part 1, Estimation of "Normal Values" for Copper,

Zinc, Cadmium, and Manganese in Blood Serun and Liver

Tissue, Analytica Chimica Acta, 157: 143-150.

R-39
CODE (J REFERENCE REFERENCE

84HUD 03 V. Hudnik, H. Marol t -Gomi seek, and S. Gomiscek (1984) The Determination of Trace Metals in Human Fluids and Tissues: Part 2, The Homogeneity of Liver Tissue for Sampling, Analytica Chimica Acta, 157: 183-186.

84IKE 01 M. Ikeda, F. Nekata, H. Matsuo, and T. Kunamaru (1984) Suction-flow Hydride Generation-Heated Quartz Cell Atomic Absorption Spectrometry of Arsenic (III, V) by Utilizing

Sensitivity Enhancement Effect of Air Introduction, Bunseki Kagaku, 33: 417-420.

84KRI 01 K. V. Krishnamurty and M. M. Kellogg (1984) Interlaboratory Comparison of Alfalfa as a Vegetation

Standard in Chemical and Radiochemical Analysis, Proceeding

of the 30th Annual Conference on Bioassay, Analytical and Environmental Chemistry, Cincinnati, Ohio.

84KUB 01 T. Kubota, T. Ueda, and T. Okutani (1984) Determination of Phosphorus by Atomic Absorption

Spectrometry using a Zirconiun Treated Graphite Tube," Bunseki Kagaku, 33: 637.

84IMA 01 N. Imai, S. Terashima, and A. Ando (1984) Determination of Seleniim in Twenty-eight Geological Reference Materials by Atomic Absorption Spectrometry, Geostandards Newsletter, 8: 39-41.

84KUL 01 I. Kuleff, R. Djingova, and I. Penev (1984) Analysis of Ancient and Medieval Glasses by INAA, Journal of Radioanalytical and Nuclear Chemistry,

83: 333-343.

84IMA 02 K. Imaeda, Y. Kuwagaki, K. Ohsawa, M. Sano, T. Yokoyama,

T. Tsutsumi, Y. Ohtani , K. Temura, and A. Yokota (1984) Determination of Zinc, Copper, Iron, Calciim, and Manganese

in Human Placenta by Acid Extraction-Atomic Absorption

Spectrometry, Bunseki Kagaku, 33: T103-T107.

841MA 03 N. Imai, S. Terashima, and A. Ando (1984) Determination of Selenium in Geological Materials by Automated Hydride Generation and Electrothermal Atomic Absorption Spectrometry, Bunseki Kagaku, 33: 290.

84JAC 01 L. L. Jackson, E. E. Engleman, and J. L. Peard (1984) Determination of Total Sulfur in Lichens by Combustion- Infrared Analysis, U. S. Geological Survey Open-File Report 84-656.

84JEN 01 B. B. Jensen, J. N. Marcussen, and N. Pind (1984) Software Package for Quantitative Analysis of Solid Materials by Energy-dispersive X-ray Fluorescence Spectrometry Without Alssolute Calibration, Analytica Chimica

Acta, 161: 175-16/.

84JEN 02 D. R. Jenke (1984) Analytical and Sampling Methodology used for Determining

the Impact of a MHD Test Facility, Analytical Letters,

17: 735-755.

84KAM 01 E. Kamata, R. Nakashima, and S. Shibata (1984) Determination of Chromiun in Coal Ash by Atomic Absorption

Spectrometry after Uet Digestion, Bunseki Kagaku, 33: 177.

84KAN 01 R. Kanipayor, D. Narajit, B. Radziuk, and J. C. van Loon

(1984), Direct Analysis of Solids for Trace Elements by Combined Electrothermal Furnace/Quartz T-tube/Flame Atomic Absorption Spectrometry, Analytica Chimica Acta, 166: 39-49.

84KAT 01 T. Katami, T. Hayakawa, M. Furukawa, and S. Shibata (1984) Extraction and Spectrophotometric Determination of Nickel in

Coal Fly Ashes and Stack Gas using 2- [2- (3,5-dibropyridyl

)

azol -5-dimethylaminobenzoic Acid, Analyst, 109: 731-733.

84KAU 01 H. C. Kaufmann and J. Steenblik (1984) Thick Target Elemental Analysis of Organic and Inorganic Materials by PIXE using Thin Film Standards, Nuclear

Instrunents and Methods in Physics Research, 231: 198-202.

84KEL 01 W. R. Kelly and P. J. Paulsen (1984) Precise and Accurate Determination of High Concentrations

of Sulphur by Isotope-dilution Thermal - i oni zat i on Mass

Spectrometry, Talanta, 31: 1063-1068.

84KNA 01 G. Knapp (1984) Der Ueg zu leistungsfahigen Mathoden der

E lementspurenanalyse in Umweltproben, Fresenius Zeitschrift fur Analytische Chemie, 317: 213-219.

84KUM 01 T. Kunamaru, F. Nakata, S. Hara, H. Matsuo, and M. Kiboku

(1984), Atomic Absorption Spectrometry of Lead by Suction

Flow Hydride Generation- Heated Quartz Cell Atomization,

Bunseki Kagaku, 33: 626.

84KUR 01 U. Kurfurst, H. H. Grobecker, and M. Stoeppler (1984) Homogeneity Studies in Biological Reference and Control Materials with Solid Sampling and Direct Zeeman-AAS,

in 84BRA 02, pp. 591-601.

84KYL 01 P. Kyle (1984) Written Communication, Department of Geoscience, New Mexico

Institute of Mining and Technology, Socorro, New Mexico.

84LAN 01 S. Landsberger and E. Hoffman (1984) Rapid Determination of Selenium in Various Marine Species by Instrumental Neutron Activation Analysis, Journal of Radioanalytical and Nuclear Chemistry, 87: 41-50.

84LAN 02 S. Landsberger, A. Giovagnoli, J.-L. Debrun, and P. Albert

(1984), Sulphur Determination in Coal by Proton Activation

Analysis, International Journal of Environmental Analytical

Chemistry, 16: 295-303.

84LAU 01 O.-W. Lau, P.-K. Hon, C.-Y. Cheung, and M.-C. Wong (1984) Uses of Silica Celts for the Static Cold Vapour Atomic Absorption Determination of Mercury Without Background

Correction, Analyst, 109: 1175-1178.

84LEC 02 LECO Corporation (1984) The LECO SC-32, SC-132, and SC-232 Determine Sulfur in Applications Note 5M-SPQ- 10/84- 12MTD.

84LEW 01 S. A. Lewis, T. C. O'Haver, and J. M. Harnly (1984) Analysis of Blood Serun for Essential Metals by Simultaneous Multielement Atomic Absorption Spectrometry

with Flame Atomization, Analytical Chemistry, 56: 1066.

84LIE 01 I. Liem, G. Kaiser, and M. Sager (1984) The Determination of Thalliun in Rocks and Biological Materials with ng/g Levels by Differential-Pulse Anodic Stripping Voltammetry and Electrothermal Atomic Absorption

Spectrometry, Analytica Chimica Acta, 158: 179-197.

84LIN 01 S.-W. Lin and K. Julshamn (1984)

A Comparative Study of the Determination of Phosphorus by

Electrothermal Atomic Absorption Spectrometry and Solution

Spectrophotometry, Analytica Chimica Acta, 158: 199.

84L1V 01 R. R. Liversage, J. C. van Loon, and J. C. De Andrade (1984)

A Flow Injection • Hydride Generation System of the

Determination of Arsenic by Inductively Coupled Plasma

Atomic Emission Spectrometry, Analytica Chimica Acta,

161: 275-283.

R-40
CCX>E N REFERENCE CODE N REFERENCE

WLOC 01 C. Locatelli, F. Fagioli, C. Bighi, and L. Scenavini (1984)

Simultaneous Determination of Trace Metals in Vegetable

Materials by Alternating Current Anodic Stripping

Voltamnetry and Atomic Absorption Spectroscopy, in 84BRA 02,

pp. 529-535.

WLOK 01 J. Long-2hu (1984) Determination of Trace Tin in River Sediment and Coal Fly

Ash by Graphite Furnace Atomic Absorption Spectrometry

using a Mixture of Ascorbic Acid and Iron as a Matrix

Modifier, Atomic Spectroscopy, 5: 91-95.

84LUN 01 E. Lundberg, U. Freeh, and I. Lindberg (1984)

Determination of Lead in Biological Materials by Constant

Tenperature Electrothermal Atomic Absorption Spectrometry,

Analytica Chimica Acta, 160: 205-215.

84MAR 01 D. B. Martin and W. A. Hartnian (1984)

Arsenic, Cadmiun, Lead, Mercury, and Selenium in Sediments

of Riverine and Pothole Uet lands of the North Central US,

Journal of the Association of Official Analytical Chemists,

67: 1141-1144.

84MAT 01 K. Matsumoto, T. Ishiwatari, and K. Fuwa (1984) Hydride Generation and Atomic Emission Spectrometry with Heliim Glow Discharge for Analysis of Biological Samples,

Analytical Chemistry, 56: 1545-1548.

84MAY 01 U. E. May and S. A. Wise (1984) Liquid Chromatographic Determination of Polycyclic Aromatic

Hydrocarbons in Air Particulate Extracts, Analytical

Chemistry, 56: 225-232.

84MCA 01 J. M. McArthur and J. N. Walsh (1984) Rare-Earth Geochemistry of Phosphorites, Chemical Geology,

47: 191-220.

84MEL 01 R. A. Mel lor (1984) Private Comnunication; quoted in 84KRI 01.

84MIA 01 Z. Hianzhi and R. M. Barnes (1984) Determination of Trace Elements in Serum using Inductively

Coupled Plasma Atomic Spectroscopy with Hydride Generation

end Chelating Resin Preeoncentration, Applied Spectroscopy,

38: 635-639.

84HIL 01 N. J. Miller-Ihli, T. C. O'Haver, and J. M. Harnly (1984) Staircase Modulation Wave Form for Continuun Source Atomic Absorption Spectrometry, Analytical Chemistry, 56: 176-181.

84H0K 01 W. M. Hok and C. M. Wai (1984) Preeoncentration with Dithiocarbamate Extraction for Determination of Molybdenum in Sea Water by Neutron Activation Analysis, Analytical Chemistry, 56: 27-29.

84M0K 02 W. H. Mok, H. Wilmes, and C. M. Wai (1984) Solvent Extraction of Molytxlenun from Biological Samples and

from Coal Fly Ash for Neutron Activation Analysis, Analytical

Chemistry, 56: 2623-2624.

84M0R 01 M. Morita, T. Uehiro, and K. Fuwa (1984) Determination of Sulfur in Biological Samples by Vacuum

Ultraviolet Inductively Coupled Plasma Atomic Emission

Spectrometry, Analytica Chimica Acta, 166: 283-288.

84NAD 01 R. A. Nadkarni (1984) Applications of Microwave Oven Sample Dissolution in Analysis, Analytical Chemistry, 56: 2233-2237.

84NAD 02 R. A. Nadkarni and R. I. Botto (1984) Determination of Germaniun in Coal Ashes by Inductively

Coupled Plasma Atomic Emission Spectrometry, Applied

Spectrometry, 38: 595-598.

84HAG 01 Y. Nagaosa and K. Kobayshi (1984) Differential Pulse Polarographic Determination of Molybdenun after Separation by 8-Hydroxyquinol ine Extraction

into Dichloromethane, Talanta, 31: 593-596.

84NAK 01 R. Makashima, E. Kamata, and S. Shibata (1984) Atomic Absorption Spectrometric Determination of Trace Elements in Coal by using an Acid Digestion in Sealed

Polytetraf luoroethylene Vessel, Bunseki ICagaku, S3: E343.

84NAR 01 H. Nerasaki and H. Ikeda (1984) Automated Determination of Arsenic and Seleniun by Atomic Absorption Spectrometry with Hydride Generation,

Analytical Chemistry, 56: 2059-2063.

84NAR 02 D. A. Naranjit, B. Radziuk, and J. C. Van Loon (1984) A Zeeman-ef feet Based Scatter Correction System for Non-dispersive Atomic Fluorescence Spectrometry,

Spec trochi mica Acta, 39B: 969-977.

84NDI 01 L. Ndiokwere (1984) Determination of Constituent Elements in some Nigerial Medicinal Plants by Thermal Neutron Activation Analysis,

Journal of Radioanalytical end Nuclear Chemistry, 85: 325.

-S400D 01 M. Oddone, S. Meloni, and N. Genova (1984) Neutron Activation Analysis: A Powerful Tool for Assay of Rare-earth Elements in Terrestrial Materials, Inorganica Chimica Acta, 94: 283-290.

840GU 01 K. OgiJna, S. Ishino, and R. Kuroda (1984) Spectrophotometric Determination of CalciLm in Silicate

Rocks, Bunseki Kagaku, 33: 284.

840HL 01 K. Ohls (1984) Die Bestimnung kleiner Cactniun-Antei le in versch i adenen

Material ien durch Festprobeneinsatz bei ICP-und flammenloser Atomabsorptionsspcktrometrie, Spectrochimica Acta, 398:1105.

840ST 01 P. Ostapezuk, M. Goedde, M. Stoeppler, and K. Nurnberg

(1984), Kontroll-und Routinebestimmung von 2n, Cd, Pb, Cu,

Ni, und Co mit Dif f erentiel ler Pulsvoltaitmetrie in Material ien des Deutschen Unweltprobenbank, Fresenius Zeitschrift fur Analytische Chemie, 317: 252-256.

84PIN 01 N. Pind (1984) Standard- addition Procedure for the Determination of Traces

of Lead in Solid Satuples by X-ray Fluorescence Spectrometry,

Talanta, 31: 1118-1120.

84PLS 01 E. Plsko and J. Kubova (1984) Ein Korrektur-Verf ahren zur Spektrographischen Bestimmung

von Vanadin in Karbonatgesteinen, Spectrochimica Acta,

39B: 1483-1485.

84PRI 01 M. W. Pritchard and J. Lee (1984) Simultaneous Determination of Boron, Phosphorus, and Sulfur

in some Biological and Soil Materials by Inductively

Coupled Plasma Emission Spectrometry, Analytica Chimica

Acta, 157: 313-326.

84RAB 01 M. Rabinowitz and H. Finch (1984) Cadmiim Content of Umbilical Cord Blood, Environmental

Research, 34: 120-122.

R-41
CODE N REFERENCE CODE H REFERENCE

84RIC 01 T. D. Rice, V. Sweeney, R. Semitekolos, and G. Rhyder (1984) Standard-addition Determination of Nitrogen in Coal with an Ammonia-sensitive Electrode, Talanta, 31: 607-610.

84RIN 01 0. Ringdal, K. Julshamn, K. Andersen, and E. Svendsen (1984) Determination of Selenitm in Hunan Tissue Samples using

Graphite Furnace Atomic Absorption Spectrometry based on Zeeman Effect Background Correction, &4BRA 02, pp. 189-199.

84R0S 01 A. Rosopulo, K. H. Grobecker, and U. Kurfurst (1984) Unterschungen uber die Schwermetal lanalyse in Feststoffen

mit der direkten Zeeman-Atom-Absorptionspektroskopie

Fresenius Zeitschrift fur Analytische Chemie, 319: 540-546.

84R0S 03 G. Rosner, K. Bunzl, H. Hotzl, and R. Winkler (1984)

Low Level Measurements of Natural Radionuclides in Soil

Saitples around a Coal-fired Power Plant, Nuclear Instruments and Methods in Physics Research, 223: 585-589.

84R0U 01 M. Rousseau, C. Friedli, and P. Lerch (1984) Trace Determination of Sulfur by Heavy Ion Activation

Analysis, Analytical Chemistry, 56: 2854-2856.

84SAT 01 T. Sato (1984) The Determination of Zircontun in Biological Materials by Photon Activation Analysis, Journal of Radioanalytical and Nuclear Chemistry, 86: 141-150.

84SAT 02 C. Sato and M. Taga (1984) Separation and Concentration of Trace Heavy Metals in Foods with Chelating Resin, Bunseki Kagaku, 33: 500-503.

84SCH 01 H. Schinkel (1984) Bestinmung von Calcium, Hagnesiim, Strontiun, Kaliun,

Natrium, Lithium, Eisen, Mangan, Chrom, Nickel, Kupfer,

Cobalt, Zink und Cadmiun. Eine Universalvorschrif t zur Untersuchung von Wassern, Kohlen, Aschen, Schlacken, Erzen, Gesteinen, Baustoffen, Metal len, und ahnlichen Proben, Fresenius Zeitschrift fur Analytische Chemie, 317: 10-26.

84SCH 03 F. Schlieckmann and F. Umland (1984) Ein Neuartiges Effizientes Aufschlussverfahren fur die Multielementbestirmiung von Schwermetal len in Luftstauben, Fresenius Zeitschrift fur Analytische Chemie, 318: 495-497.

84SCH 04 H. Schelhorn and M. Geisler (1984) Zun Einstaz von Radiotracern zur Ausbeutebestiiimung in der Neutronenaktivierungsanalyze, Journal of Radioanalytical

and Nuclear Chemistry, 83: 5-11.

84SHI 01 J. Shida, Y. Takahashi, and K. Ojima (1984) Flotation-spectrophotometric Determination of Germaniun with

Phenyl fluorone in Coal Fly Ash, Bunseki Kagaku, 33: E143.

84SIL 01 D. Silberman and W. R. Harris (1984) Determination of Arsenic(IIl) and Arsenic(V) in Coal and Oil

Fly Ashes, International Journal of Environmental Analytical

Chemistry, 17: 73-83.

84SIH 01 M. Simonoff, Y. Llabador, C. Hamon, and G. Simonoff (1984)

Extraction Procedure for the Determination of Trace Chromium

in Plasma by Proton- induced X-ray Emission Spectrometry,

Analytical Chemistry, 56: 454-457.

84SIM 02 M. Simonoff, Y. Llabador, G. Simonoff, P. Besse, and

C. Conri (1984), Cineangiographical ly Determined Coronary

Artery Disease and Plasma Chromium Levels for 150 Subjects,

Nuclear Instruments and Methods, 231: 368-372.

84SIM 03 W. J. Simonsick and R. A. Hites (1984) Analysis of Isomeric Polycyclic Aromatic Hydrocarbons in Charge-Exchange Chemical Ionization Mass Spectrometry, Analytical Chemistry, 56: 2749-2754.

84SIU 01 K. U. M. Siu and S. S. Berman (1984) Comparison of Two Digestion Methods used in the Determination of Seleniun in Marine Biological Tissues by

Gas Chromatography with Electron-capture Detection, Talanta,

31: 1010-1012.

84SLA 02 U. Slavin end G. R. Carnrick (1984) The Possibility of Standardless Furnace Atomic Absorption

Spectroscopy, Spectrochimica Acta, 39B: 271-282.

84SNE 01 J. Sneddon and V. A. Fuavao (1984) Observations on a Matrix Interference in the Measurement of Lead by D. C. Argon Plasma Emission Spectroscopy, Atomic

Spectroscopy, 5: 108.

84S0B 01 C. B. Sobel (1984) Automatic Simultaneous Multielement Analysis of Microvolune

Samples with an Inductively Coupled Plasma Source, Applied Spectroscopy, 38: 444-447.

84ST0 01 H. Stoeppler (1984) Bedeutung von Lknweltprobenbanken-Anorganisch-Analytische Aufhabenstel lungen und erste Ergebnisse des Deutschen

Umweltprobenbankprogramms, Fresenius Zeitschrift fur Analytische Chemie, 317: 228-235.

84SUN 01 J. F. C. Sung, A. E. Nevtssi, and F. B. Dewalle (1984) Simple Sample Digestion of Sewage and Sludge for Multielement Analysis, Journal of Environmental Science and Health, A19: 959-972.

84SUZ 01 N. Suzuki, S. Nakamura, and H. Imura (1984) Substoichiometric Determination of Manganese in a Synergistic Extraction System and its Application to the Analysis of Biological Materials, Journal of Radioanalytical

and Nuclear Chemistry, 81: 37-48.

84SUZ 02 S. Suzuki and S. Hirei (1984) Activation Analysis of Trace Elements in Coal and Fly Ash

by Low Energy Photon Spectrometry, Bunseki Kagaku, 33: 197.

84SUZ 03 H. Suzuki, H. Minami, K. Abe, H. Hiraiwa, and T. Uchida

(1984), Comparison of Sample Decomposition Methods for Atomic Absorption Spectrometry of Eight Elements in Chinese Cabbage, Bunseki Kagaku, 33: T-9.

84TAK 01 Y. Takahasmi and M. Rey (1984)

A Dedicated XRF Analyzer for Sulfur in Oils, International Laboratory, 14 (1): 84-93.

84TER 01 S. Terashiroa (1984) Determi ration of Cadmiun and Lead in Seventy- seven

Geological Reference Samples by Atomic Absorption

Spectrometry, Geostandards Newsletter, 8: 13-16.

84TER 02 S. Terashima (1984) Determination of Bismuth in Geological Materials by Automated Hydride Generation and Electrothermal Atomic Absorption Spectrometry, Analytica Chimica Acta, 156: 301.

84TER 03 S. Terashima (1984) Determination of Bismuth in Eighty-three Geochemical

Reference Sanples by Atomic Absorption Spectrometry,

Geostandards Newsletter, 8: 155-158.

R-42
CODE N REFERENCE CODE N REFERENCE

84TER 04 S. Terashimo (1984) Determination of Arsenic and Antimony in Geological Materials by Automated Hydride Generation and Electrothermal

Atomic Absorption Spectrometry, Bunseki Kagaku, 33: 561-563.

84TJI 01 P. S. Tjioe, K. Volkers, J. Kroon, J. de Goeij, and S. The

(1984), Determination of Gold and Plstinim Traces in

Biological Materials as a Part of a Multielement Radiochemical Activation Analysis System, International Journal of Environmental Analytical Chemistry, 17: 13-24.

84TIJ 01 S.-D. Tu and K. H. Lieser (1984) Multielement Analysis of Chinese Biological Standard

Reference Material by Monostandard Instrunental Neutron

Activation Analysis, Journal of Rsdioanalytical and Nuclear

Chemistry, 81: 345-352.

84TU 03 S.-O. Tu, U. Hanf, and K. H. Lieser (1984) Monostandard Instrunental Neutron Activation Analysis of Chinese Biological Standard Reference Material Using

Short-lived Radionuclides, Journal of Radioanalytical and Nuclear Chemistry, 83: 283-290.

84URA 01 I. T. Urasa (1984) Determination of Arsenic, Boron, Carbon, Phosphorus,

Seleniun, and Silicon in Natural Waters by Direct Current Plasma Atomic Emission Spectrometry, Analytical Chemistry,

56: 904-908.

84ZS0 01 I. M. Zsolnay, J. M. Brauer, and S. A. Sojka (1984) X-ray Fluorescence Determination of Trace Elements in Soil, Analytica Chimica Acta, 162: 423-426.

85ABD 01 M. Abdullah and H. Haraguchi (1985) Computer control led Graphite Cup Direct Insertion Device for Direct Analysis of Plant Sanples by Inductively Coupled Plasma Atomic Emission Spectrometry, Analytical Chemistry,

57: 2059.

85ADE 01 S. B. Adeloju, A. H. Bond, and M. H. Briggs (1985) Multielement Determination in Biological Materials by Differential Pulse Voltammetry, Analytical Chefnistry,

57: 1386-1390.

85ADE 02 S. B. Adeloju and A. M. Bond (1985) Influence of Laboratory Environment on the Precision and Accuracy of Trace Element Analysis, Analytical Chemistry,

57: 1728-1733.

85AKA 01 M. S. Akanni and V. 0. Ogugbuaja (1985) Multielement Analysis of Nigerian Traditional (Black) Soaps

Journal of Radioanalytical and Nuclear Chemistry, 91: 395.

85AND 01 D. L. Anderson, V. Sun, M. Failey, and W. ZoUer (1985) Neutron-capture Prompt Gamma-ray Multielement Analysis of Twenty-two Geochemical Reference Standards, Geostandards

Newsletter, 9: 219-228.

84V0S 01 L. Vos and R. van Grieken (1984) Preparation of Conducting Electrodes from Biological Samples

for Multielement Trace Analysis by Spark-source Mass Spectrometry or Emission Spectrometry, Analytica Chimica

Acta, 164: 83-90.

84WEB 01 H. T. Weber, J. van Willigen, and W. van der Linden (1984) Determination of Total Sulfur in Coal by X-ray Fluorescence

Spectrometry, Analytica Chimica Acta, 160: 271-2?^.

84W0L 01 A. Wolf, P. Schramel, G. Lill, and H. Hohn (1984)

Bestitmiung von Spurenelementen in Moos-und Bodenproben

2ur Untersuchung der Eignung als Indicatoren fur Umweltbelastungen, Fresenius Zeitschrift fur Analytische

Chemie, 317: 512-519.

85AVA 01 L. Avaldi, C. Bui, and M. Milazzo (1985)

The Problem of Irradiation and Detection Angles in Quantitative XRF Analysis, X-ray Spectrometry, 14: 159-163.

85BAR 01 U. Bartels (1985) Uber die Anwendung von Ascorbinsaure und Thioglykolsaure

lur Beseitigung der Storungen durch dreiwertiges Eisen bei der photometrischen Bestimnung von Aluninium mit Aliminon

in Pflenzen, Fresenius Zeitschrift fur Analytische Chemie,

320: 56-57.

85BEL 01 L. F. Bellido and B. de C. Arezzo (1985) Uraniim and ThoriLm Determination in Brazilian Coals by

Epithermal Neutron Activation Analysis, Journal of Radio- analytical and Nuclear Chemistry, 92: 151-158.

84U0L 02 K. A. Wolnik, F. Fricke and C. M. Gaston (1984) Quality Assurance in the Elemental Analysis of Foods by

Inductively Coupled Plasma Spectroscopy, Spectrochimica

Acta, 39B: 649-655.

85BEM 01 H. Bem and 0. E. Ryan (1985) Determination of Palladitm in Different Samples by Meutron Activation after Selective Preconcentretion with Alphabenzi Idioxime, Analytica Chimica Acta, 169: 79-85

84XIA 01 S. Xiao-quan, N. Zhe-ming, and Z. Li (1984) Use of Arsenic Resonance Line of 197.2 nm and Matrix Modification for Determination of Arsenic in Environmental

Samples by Graphite Furnace Atomic Absorption Spectrometry

using Palladitm as a Matrix Modifier, Atomic Spectroscopy,

5: 1-4.

85B0N 01 A. M. Bond and Y. Nagaosa (1985) Determination of Aluniniun, Copper, Iron, and Manganese in

Biological and Other Samples as 8-0uinolirK)l Complexes by

High-performance Liquid Chromatography with Electrochemical

and Spectrophotometric Detection, Analytica Chimica Acta,

178: 197-208.

84YAM 01 M. Yamamoto, Y. Yamamoto, and T. Yamashige (1984) Elimination of Metal Interferences in the Hydride Generation

Atomic Absorption Spectrometry of Arsenic using Sodiun Tetrahydroboratedll) Solution, Analyst, 109: 1461-1463.

84ZER 01 M. Zerezghi, K. C. Ng, and J. A. Caruso (1984) Simultaneous Multielement Determination by Inductively

Coupled Plasma-Rapid Scanning Atomic Emission Spectrometry,

Analyst, 109: 589-592.

34ZIC 01 Z. Zichao, M. Guogan, and L. Huaquin (1984) The Chronometric Age of the Sinian Cambrian Boundary in the Yangtze Platform, China, Geological Magazine, 121: 175-178.

85BRE 01 S. W. Brewer and R. D. Sacks (1985) Preconcentration of Cadmium from Highly Acidic Saline

Solutions and Direct Determination of Bismuth, Cadmium,

Mercury, Antimony, Tin, and Thallium in Highly Acidic

Solutions with Electrically Vaporized Thin Gold Film Atocmc

Emission Spectrometry, Analytical Chemistry, 57: 724-729.

85BR0 01 R. R. Brooks and S. D. Naidu (1985)

The Determination of Gold in Vegetation by Electrothermal

Atomic Absorption Spectrometry, Analytica Chimica Acta,

170: 325-329.

R-43
CODE H REFERENCE CODE N REFERENCE

85BYE 01 R. Bye and W. Lund (1985) Determination of Seleniim in Biological Samples by Electrothermal Preconcentration and Atomic Absorption

Spectrometry, Fresenius Zeitschrift fur Anelytische Chemie,

321: 483-484.

85CAN 01 M. C. Centone, N. Molho, and L. Pirola (1985) Cadmium and Titanium in Human Serun Determined by Proton

Nuclear Activation, Journal of Radioanalytical and Nuclear

Chemistry, 91: 197-203.

85CAR 01 E. E. Cary (1985) Electrothermal Atomic Absorption Spectroscopic Determination

of Chromiun in Plant Tissues: Interlaboratory Study, Journal

of the Association of Official Analytical Chemists, 68: 495.

85CAR 02 J. Carroll, H. HiUer-Ihli, J. Harnley, D. Littlejohn,

J. OttBway, and T. O'Haver (1985), Simultaneous Multielement Analysis by Continutjn Source Atomic Absorption Spectrometry

with Graphite Probe Electrothermal Atomisation, Analyst,

110: 1153-1158.

85CHA 01 C. C. Y. Chen (1985) Semiautomated Method for Determination of Selenium in Geological Materials using a Flow Injection Analysis

Technique, Analytical Chemistry, 57: 1482-1485.

85CLA 01 E. Clayton and tC. K. Woller (1985) Sample Preparation and System Calibration for Proton- Induced X-ray Emission Analysts of Hair from Occupational ly Exposed

Workers, Analytical Chemistry, 57: 1075-1079.

85CLA 02 E. Clayton and L. S. Dale (1985) Determination of Fluorine in NBS Coal and Coal Fly Ash by Proton Induced Garima Ray Emission end Sparli Source Mess Spectrometry, Analytical Letters, 18: 1533-1538.

85C0E 01 U. Coerdt and E. Mainka (1985) Versuche zur Goldbestimnung in Boden-und Staubf i I terproben, Fresenius Zeitschrift fur Anelytische Chemie, 320: 656.

85COE 02 P. P. Coetzee and K. H. Lieser (1985) Multielement Analysis by Energy- dispersive X-ray

Fluorescence using a Single Calibration Procedure, Requiring

One or Two Standards, Fresenius Zeitschrift fur Analytische

Chemie, 322: 386-390.

85COX 01 A. G. Cox, I. G. Cook, and C. W. Mcleod (1985) Rapid Sequential Determination of Chromiun (III) - Chromium

(VI) by Flow Injection Analysis - Ir>ductively Coupled Plasma

Atomic Emission Spectrometry, Analyst, 110: 331-333.

85CUT 01 G. A. Cutter (1985) Determination of Selenium Speciation in Biogenic Particles

and Sediments, Analytical Chemistry, 57: 2951-2955.

85DAT 01 A. R. Date end A. L, Gray (1985) Determination of Trace Elements in Geological Samples by

Inductively Coupled PlasiTB Source Mass Spectrometry, Spectrochimica Acta, 40B: 115-122.

85DAV 01 L. A. Davis, R. J. Krupa, and J. D. Winefordner (1985)

A Simple, Inexpensive Computer-controlled Slew-scan Atomic Fluorescence Flairie Spectrometer for Multielement

Determinations, Analytics Chimica Acta, 173: 51-62.

85DOU 01 J. P. Dougherty, R. G. Michel, and W. Slavin (1985) Precision Considerations in the Determination of Manganese

in Mouse Brains by Furnace Atomic Absorption with Zeeman

BBckgrour>d Correction, Analytical Letters, 18: 1231-1244.

85DUM 02 R. Dunarey, p. Verbiest, and R. Dams (1985) Optimization of a Wet Digestion Method for the Determination

of Mercury in Coal Saijples by Cold Vapor Atomic Absorption, Bulletin des Societes Chimiques Beiges, 94: 351-357.

85DYB 01 R. Dybczynski, H. Maleszewska, and M. Wasek (1985) An Accurate Method for the Determination of Copper in Biological Materials by Neutron Activation Analysis and Extraction Chromatography, Journal of Radioanalytical and Nuclear Chemistry, 96: 187-200.

85ENG 01 E. E. Engleman, L. L. Jackson, and D. R. Norton (1985) Determination of Carbonate Carbon in Geological Materials by Coulometric Titration, Chemical Geology, 53: 125-128.

85EVA 01 W. H. Evans and J. I. Read (1985) Determination of Lithium, Rubidium, and Strontiun in Foodstuffs, Analyst, 110: 619-623.

85EVA 02 W. K. Evans and D. Caughlin (1985) Evaluation of Methods for the Determination of Total Molybdenim and Vanadiun in Foodstuffs Using Spectrophoto- metric Measurements, Analyst, 110: 681-687.

85FAB 01 J. L. Fabec and M. L. Ruschek (1985) Determination of Nickel, Vanadiim, and Sulfur in Crudes and Heavy Crude Fractions by Inductively Coupled Argon Plasma

Atomic Emission Spectrometry and Flame Atomic Absorption

Spectrometry, Analytical Chemistry, 57: 1853-1863.

B5FAN 01 Y. Fang, G. Wuer, and U. Fushen (1985) Zeeman Effect Electrothermal Atomic Absorption of Arsenic

with Platinon as a Matrix Modifier, Analytical Letters,

18: 1245-1250.

85FAS 01 A. J. Faske, K. Snable, A. Boorn, and R. Browner (1985) Microliter Sanple Introduction for ICP-AES, Applied

Spectroscopy, 39: 542-545.

85FAS 02 J. D. Fassett and H. M. Kingston (1985) Determination of Nanogram Quantities of Vanadiun in Biological Material by Isotope Dilution Thermal Ionization Mass Spectrometry with Ion Counting Detection, Analytical

Chemistry, 57: 2474-2478.

85FEH 01 X. Feng end 0. E. Ryan (1985) Neutron Activation Determination of Mercury in Waters after Preconcentration by Flotation of Dithizone-Mercury Complexes

International Journal of Environmental Analytical Chemistry,

19: 272-280.

85FIL 01 R. H. Filby, S. Nguyen, C. Grimm, G. Markowski, V. Ekambaram

T. Tanaka, and I Grossman (1985), Evaluation of Geochemical Standard Reference Materials for Microanalysis, Analytical

Chemistry, 57: 551-555.

85FIL 02 R. H. Filby, G. van Bcrkel, A. Bragg, A. Joubert,

W. Robinson, and C. Grimm (1985), Evaluation of Residual

Fuel Oil Standard Reference Materials as Trace Element

Standards, Journal of Radioanalytical and Nuclear Chemistry,

91: 361-368.

85FL0 01 M. A. Floyd, A. Haloima, R. Morrow, and R. Farrar (1985)

Rapid Multielement Analysis of Water Samples by Sequential

ICP-AES, American Laboratory, 17(3): 84-92.

85FRI 01 C. Friedli, M. Rousseau, T. Diaco, and P. Lerch (1985)

Dosage de traces de soufre et de berylliun par activation

dans un faisceau d'oxygene- 18, Analusis, 13: 176-180.

R-44
CODE N REFERENCE CODE N REFERENCE

85FU0 01 N. Fudogawa and A. Kawase C1985) Determination of Ca<*niun in Coal by Metal Furnace Atomic

Absorption Spectrooietry, Bunseki Kagaku, 34: 233.

85GAU M M. A. Gautier, E. S. Gladney, and 0. R. Perrin (1985)

Quality Assurance for Health and Environmental Chemistry

1984, Los Alanxjs National Laboratory report LA-10508-MS.

85GEN 01 C. A. Gent and S. A. Wilson (1985)

The Determination of Sulfur end Chlorine in Coiils and Oil Shales using Ion Chromatography, Analytical Letters,

18: 729-7k0.

85GLA 01 E. S. Gladney and M. W. Bower (1985) Determination of Elemental Composition of NBS 278 and

NBS 688 via Neutron Activation and X-ray Fluorescence, Geostandards Newsletter, 9: 261-252.

85CLA 02 M. D. Glascock, W. Z. Tian, and W. D. Ehmann (1985) Utilization of a Boron Irradiation Vessel for NAA of Short Lived Radionuclides in Biological and Geological Materials,

Journal of Radioanalytical and Nuclear Chemistry, 92: 379.

85GLA 03 E. S. Gladney, R. Raymond, and M. W. Bower (1985) Evaluation of the LECO SC-132 Sulfur Analyzer for the Determination of Sulfur in Coals and Peats, American Laboratory, 17(7): 34-33.

85GLA 04 E. S. Gladney (1985) Determination of Uranium in GSJ, CRPC, and CCRMP Reference

Samples by Delayed Neutron Assay, Geostandards Newsletter,

9: 275-276.

85GLA 05 E. S. Gladney, D. B. Curtis, and D. R. Perrin (1985) Determination of Selected Rare Earth Elements in 37

International Geochemical Reference Materials by

Instrunental Thermal Neutron Capture Prompt Gama-ray

Spectrometry, Geostandards Newsletter, 9: 25-30.

85GRE 01 R. C. Greaves, R. M. Barkley, and R. E. Sievers (1985) Rapid Sampling ar>d Analysis of Volatile Constituents of Airborne Particulate Matter, Analytical Chemistry, 57: 2807.

85GRE 02 J. D. Greenough, S. R. McCutcheon, and V. S. Papezik (1985) Petrology and Geochemistry of Cambrian Volcanic Rocks from

the Avalon Zone in New Brunswick, Canadian Journal of Earth

Sciences, 22: 881-892.

85HAN 01 S. Hanamura, B. Kirsch, and J. 0. Winefordner (1985) Determination of Trace Levels of Water in Solid Samples by Evolved Gas Analysis/Heliun Microwave Plasma Emission

Spectrometry, Analytical Chemistry, 57: 9-13.

85HAR 01 H. Haraguchi, M. Kurosawa, and Y. Iwata (1985) Simultaneous Multielement Analysis of Coals and Fly Ashes

by Inductively Coupled Plasma Atomic Emission Spectrometry,

Bunseki Kagaku, 34: 257.

85HAS 01 R. J. Haskell and J. C. Wright (1985) Determination of Rheniun at Ultratrace Levels by Selective

Laser Excitation of Precipitates, Analytical Chemistry,

57: 332-336.

85HEE 01 S. S. Q. Hee, T. J. Macdonald, and J. R. Boyle (1985) Effects of Acid Type and Concentration on the Determination

of 34 Elements by Simultaneous Inductively Coupled Plasma

Atomic Emission Spectrometry, Analytical Chemistry, 57:1242

85H0L 01 J. Holzbecher, A. Chatt, D. E. Ryan (1985) SLOWPOKE Epi-cadmiun Neutron Flux in Activation Analysis of Trace Elements, Canadian Journal of Spectroscopy, 30: 67-72.

85ICH 01 S. Ichinoki and M. Yamazeki (1985) Simultaneous Oetermirwtion of Nickel, Lead, Zinc, and Copper

in Citrus Leaves and Rice Flour by Liquid Chromatography

with Hexamethylenedithiocarbemate Extraction, Analytical

Chemistry, 57: 2219-2222.

85IKE 01 M. Ikeda (1985) Determination of Arsenic at the Picogram Level by Atomic Absorption Spectrophotometry with Miniaturized Suction-flow Hydride Gareration, Analytics Chimico Acta, 167: 239-297.

85ISS 01 R. A. Jssac and W. C. Johnson (198^;) Elemental Analysis of Plant Tissue by Plasma Emission Spectroscopy: Collaborative Study, Journal of the Association of Official Analytical Chemists, 68: 499-504.

85JAC 01 L. L. Jackson, E. E. Engleman, and J. L. Peard (1985) Determination of Total Sulfur in Lichens and Plants by

Contiustion- Infrared Analysis, Environmental Science and Technology, 19: 437-441.

85JAI 01 D. D. Jaiswal, H. Dang, and C. Sunta (1985) Distribution of Thoriun in Human Tissues, Journal of Radioanalytical arvd Nuclear Chemistry, 88: 225-229.

85JAR 02 I. Jarvis and K. E. Jarvis (1985) Rare-earth Element Geochemistry of Standard Sediments: A Study using Inductively Coupled Plasma Spectrometry,

Chemical Geology, 53: 335-344.

85JON 01 J. W. Jones and T. C. O'Haver (1985) Effects of pH and Digestion Conditions on Chelex 100 Separation of Trace Elements from Tissue Digests Prior to ICP-AES Determination, Spectrochimica Acta, 40B: 263-277.

85JOS 01 S. R. Joshi (1985) Determination of Th-228, Th-230, and Th-232 in Sediments by Anion Exchange and Nuclear Spectrometry, Analytical

Chemistry, 57: 1023-1026.

85KAT 01 T. Katami, T. Hayakawa, H. Furukawa, and S. Shibata (1985) Spectrophotometric Determination of Cobalt in Pepperbush

Leaves ar>d Coal Fly Ashes Using 2-(2-Benzothiazolylazo)-5-

dimethylaminobcnzoic Acid, Analyst, 110: 399-401.

85KAT 02 M. Katoh and K. Kudo (1985) Study on the Comparator Method using Substoichiometry,

I. Principle, Journal of Radioanalytical and Nuclear Chemistry, 95: 55-62.

85KIM 01 M. M. Kimberly and D. C. Paschal (1985) Screening for Selected Toxic Elements in Urine by Sequential

, Scanning Inductively-coupled Plasma Emission Spectrometry,

Analytica Chimica Acta, 174: 203-210.

85KOJ 01 I. Kojima, T. Uchida, C. lida, and K. Goto (1985) Determination of the Absolute Mass of an Analyte by Flame

Atomic Absorption Spectrometry with Discrete Nebul isation.

Analyst, 110: 1161-1163.

85KUM 01 T. Kuroamaru, Y. Nitta, F. Nakata, and H. Matsuo (1985)

Determination of Cadmiun by Suction-flow Liquid- I iquid

Extraction Contiined with Inductively Coupled Plasma Atomic

Emission Spectrometry, Analytica Chimica Acta, 174: 183-189.

85LAN 02 S. Landsberger, R. E. Jervis, and A. Balicki (1985)

The Determination of Sulphur and Heavy Metals in Snow by

Inductively Coupled Plasma Atomic Emission Spectrometry,

International Journal of Environmental Analytical Chemistry,

19: 219-225.

R-45
CODE N REFERENCE CODE N REFERENCE

85LEP 01 E. A. Lepel and J. C. Laul (1985) Neutron Activation Analysis of NBS Oyster Tissue and IAEA Animal Bone, Proceedings of the 5th International Conference

on Nuclear Methods in Environmental and Energy Research, Mayaguez, Puerto Rico.

85LIE 02 T. Liese (1985)

Zur Bestinmung von Elementen in Pflanzen-und Bodenproben

miltels ICP-AES, Fresenius Zeitschrift fur Analytische

Chemie, 321: 37-44.

85LIN 01 P. C. Lindshl (1985) Electrically Heated Ouartz Cell and Holder for an Atomic Absorption Hydride Generation System, Atomic Spectrometry,

6: 123-124.

85NAR 01 K. Narasaki (1985)

Detertnination of Traces of Arsenic and Seleniim by Hydride Generation - Atomic Absorption Spectrometry, Frasenius Zeitschrift fur Analytische Chemie, 321: 464-466.

85NAR 02 D. A. Naranjit, B. Radziuic, J. Rylaarsdam, P. Larkins, and

J. van Loon (1985), A Microconputer-controUed Simultaneous Multielement Noodispersive Atomic Fluorescence Spectrometer, Applied Spectroscopy, 39: 128-136.

85NAR P3 H. Naraseki (1985) Determination of Arsenic and Setenitm in Fat MaterUls and Petroleum Products by Oxygen Bomb Combustion and Autoioated Atomic Absorption Spectrometry with Hydride Generation,

Analytical CheiHistry, 57: 2481-2486.

85LIN 02 P. C. Lindahl (1985) Determination of Arsenic and Seleniun in Coal by Hydride

Generation/Atomic Absorption Spectrophotometry -- An Inter- laboratory Evaluation of a Proposed Standard Test Method, Argonne National Laboratory report ANL/ACL-85-3.

85L0N 01 J. Long-zhu and N. Zhe-ming (1985) Determination of Nickel in Urine and Other Biological

Samples by Graphite Furnace Atomic Absorption Spectrometry,

Fresenius Zeitschrift fur Analytische Chemie, 321: 72-76.

85LYO 01 D. J. Lyons, K. P. Spann, and R. L. Roofayel (1985) Determination of Total Calcium, Zinc, Manganese, Iron, Magnesium, and Phosphorus in Animal Feeds and Plant Material Using Inductively Coupled Plasma Emission Spectrometry,

Analyst. 110: 955-957

85HAD 01 H. Madaro and A. Moaura (1985) Instrimental Neutron Activation Analysis Results in an Intercomparison Campaign on Lake and River Sediments,

Journal of Radioenalytical and Nuclear Chemistry, 90:129-136

85MAS 01 K. Masumoto and M. Vagi (1985) Determination of Strontiuti in Biological Materials by

Charged-Particle Activation Analysis using the Stable

Isotope Dilution Method, Journal of Radioanalytical and

Nuclear Chemistry, 91: 369-378.

85MCC 02 D. L. McCurdy, M. D. Wichman, and R. C. Fry (1985) Rapid Coal Analysis. Part 11: Slurry Atomization DCP

Emission Analysis of NBS Coal, Applied Spectroscopy,

39: 984-988.

85MEY 02 A. Meyer and R. Neeb (1985) Bestimmung von Cobalt und Nickel in einigen biologischen

Matrices - Vergleich Chelat Gas - Chromatographie und Adsorptions-Voltammetrie, Fresenius Zeitschrift fur Analytische Chemie, 321: 235-241.

85MIS 01 U. C. Mishra and G. N. Shaikh (1985) Determination of Trace Elements in Total Particulate Matter

of Cigarette Smoke by Instrumental Neutron Activation

Analysis, Journal of Radioanalytical and Nuclear Chemistry,

89: 545-552.

85NAD 01 R. A. Nadkarni , R. B. Cornett, and R. L. Bredeweg (1985) Evaluation of an Elemental Analyzer, American Laboratory,

17(2): 69-77.

85NAK 01 T. Nakahara and N. Kikui (1985)

Determination of Trace Concentrations of Seleniun by

Continuous Hydride Generation- Inductively Coupled Plasma

Atomic Emission Spectrometry, Spectrochimica Acta, 40B: 21.

eSNDI 01 C. L. Ndiokwere (1985) The Dispersal of Arsenic, Chromium, and Copper from a Wood

Treatment Factory, and Their Effect on Soil, Vegetation, and

Crops, Int. Journal of Environmental Studies, 24: 231-234.

8SNG 01 R. C. Ng, H. Kaiser, and B. Meddings (1985) Low Power Torches for Organic Solvents in Inductively

Coupled Plasma Emission Spectrometry, Spectrochimica Acta,

40B: 63-72.

85NIS 01 M. Nishikawa, Y. Anbe, and T. Hizoguchi (1985) Evaporation Preconcentration of Trace Elements in Rainwater

for Inductively Coupled Plasma Emission Spectrometry,

Bunseki Kagaku, 34: 664.

850KA 02 K. Okamoto and K. Fuwa (1985) Mussel Tissue Powder, A Certified Reference Material,

Analyst, 110: 785-788.

850TT 01 M. Otto, W. Wegscheider, and E. P. Lankmayr (1985) Single- and Multi -channel Detection for Generalized Quantitative Analysis in Cases of Unresolved Chromatographic

Peaks, Analytica Chimica Acta, 171: 13-31.

85PAR 01 C. J. Park (1985)

A Feasibility Study of an ETV/ICP/MS System, Ph.D. Thesis,

University of Toronto.

85PEA 01 U. C. Pearch, 0. Thornewill, and J. H. Harston (1985) Multielement Analysis of Solutions of Coal Ash using

Inductively Coupled Plasma Optical-emission Spectrometry,

Analyst, 110: 625-629.

85PEN 01 I. Penev, I. Kuleff, and R. Djingova (1985)

Simultaneous Activation Determination of Aliminiun,

Magnesicm, and Silicon in Rocks, Glasses, and Pottery,

. Journal of Radioanalytical and Nuclear Chemistry, 96: 219.

85PIU 01 J. Piwonka, G. Kaiser, and G. Tolg (1985)

Determination of Seleniun at ng/g end pg/g Levels by Hydride

Generation Atomic Absorption Spectrometry, in Biotic

Materials, Fresenius Zeitschrift fur Analytische Chemie,

321: 225-234.

B5P0T 02 P. J. Potts, 0. Thorpe, M. Isaacs, and N. Rodgers (1985)

Instrunental Neutron Activation Analysis of Fourteen

Carbonate Reference Materials from the NBS and George

Frederic Smith and Eleven Industrial Geological Samples from

the Bureau of Analyzed Samples, Geostandards Newsletter,

9: 173-179.

85P(XJ 01 M. Pougnet, M. Orren, and L. Haraldsen (1985)

Determination of Berylliun and Lithiim in Coal Ash by

Inductively Coupled Plasma Atomic Emission Spectroscopy,

Int. Journal of Environmental Analytical Chemistry, 21: 213.

R-46
CODE N REFERENCE CODE REFERENCE

85RIC 01 T. D. Rice (1985) Private Conmunication; taken from 85CLA 02.

85ROE 01 I. Roelandts, G. Robaye, G. Ueber, and J. Delbrouck (1985) Determination of Fluorine in Eighty International

Geochemical Reference Samples by Proton Induced G&ma Ray

Emission Spectrometry, Geostandards Newsletter, 9: 191-197.

85RUC 01 A. de Ruck and R. Dams (1985) Determination of Thallium in Environmental Samples by Activation Analysis with Fast Reactor Neutrons, Journal of Radioanalytical and Nuclear Chemistry, 94: 87-94.

85SAI 01 K. Saitoh and N. Suzuki (1985)

High -Performance Liquid Chromatographic Determination of Nickel, Copper, and Zinc as their Tetraphcnylporphine

Chelates, Analytica Chimica Acta, 178: 169-177.

85SA»; 01 T. Sakai, S. Hanamura, and J. D. Winefordner (1985) •

Evolved-gas Zeeman Flame Atomic Absorption Spectrometry for

the Determination of Arsenic Compounds, Analytica Chimica

Acta, 170: 237-243.

85SAL 01 C. D. Salisbury and W. Chan (1985) Simple Automated Wet Digestion of Animal Tissues for Determination of Seven Elements by Atomic Absorption

Spectroscopy, Journal of the Association of Official Analytical Chemists, 68: 218-219.

85SAT 01 K. Sato and H. Sakata (1985) Multielement Determination of Coal Ash by Inductively

Coupled Plasma Atomic Emission Spectrometry, Bunseki Kagaku,

34: 275.

85SCH 01 W. Schindlmeier and K. Neumann (1985) lodspurenbestimnung in Lebensmi ttelproben durch massenspektrometrische Isotopenverdunnungsanalyse, Fresenius Zeitschrift fur Analytische Chemie, 320: 745-748.

85SC! 01 Sciex Corporation (1985) Multielement Isotope Dilution Using the ELAN ICP/MS Elemental Analyzer, Sciex Application Note 00384E.

85SHI 01 J. Shida, M. Itoh, T. Ogata, and H. Kamada (1985) Characterization of Manganese in Coal by Electron Spin

Resonance, Bunseki Kagaku, 34: 247.

85TAN 01 J. T. Tanner, J. Smith, G. Angyal, P. Defibaugh, M. Bueno, and M. Villalobos (1985), National Bureau of Standards Reference Materials as Organic Nutrient Standards: A Preliminary Study, Journal of the Association of Official Analytical Chemists, 68: 1084-1086.

85TER 01 S. Terashima (1985) Determination of Tin in Geological Materials by Atomic Absorption Spectrometry, Bulletin of the Geological Survey

of Japan, 36: 375-383.

85TIA 01 W. Tian and W. D. Ehmann (1985) Radiochemical Neutron Activation Analysis for Arsenic,

Cadmium, Copper, and Molytxienum in Biological Matrices,

Journal of Radioanalytical and Nuclear Chemistry, 89: 109.

85UT0 01 M. Uto, Y. Itoh, and M. Sugawara (1985) Differential Pulse Polarographi c Determination of NickeUlI)

as Water-soluble Dithiocarbamate, Fresenius Zeitschrift fur Analytische Chemie, 321: 68-71.

85VEI 01 C. Veitlion, S. Lewis, K. Patterson, W. Wolf, J. Harnly,

J. Versieck, L. Vanballenberghe, R. Cornells, and T. O'Haver

(1985), Characterization of a Bovine Serum Reference Material for Major, Minor, and Trace Elements, Analytical

Chemistry, 57: 2106-2109.

85V0G 01 J. R. Vogt and S. C. Schlegel (1985) Elemental Determinations in NBS 1633A Fly Ash Standard Reference Material using INAA and PGNAA, Journal of Radioanalytical and Nuclear Chemistry, 88: 379-387.

85V0S 01 L. Vos and R. Van Greiken (1985) Matrix Effects and Analysis of Biological Materials by Spark Source Mass Spectrometry, Fresenius Zeitschrift fur Analytische Chemie, 321: 32-36.

85WAH 01 S. Waheed, I. Fatima, A. Merman, H. Chaudhary, and

I. Oureshi (1985), Trace Element Concentration in Egg-yolk and Egg-white of Farm and Domestic Chicken Eggs,

Int. J. Environmental Analytical Chemistry, 21: 333-344.

85WHI 01 D. Whitehead and J. E. Thomas (1985) Use of a Nebulizer in Pyrohydrolic Decomposition of Silicate

Materials for Determination of Fluorine and Chlorine,

Analytical Chemistry, 57: 2421-2423.

85SHI 02 J. Shida, H. Suzuki, and S. Abe (1985) Spectrophotometric Determination of Boron in Plants after

Separaton as Trimethyl Borate by Microdiffusion, Analytica

Chimica Acta, 169: 349-353.

85SIM 01 M. Simonoff, Y. Llabador, G. Simonoff, M. Boisseau, and

M. Roudaut (1985), PIXE Determination of Calciim in Red

Blood Cells, Journal of Radioanalytical and Nuclear

Chemistry, 94: 297-310.

85SUB 01 K. Subramanian, J. Meranger, C. Wan, and A. Corsini (1985)

Preconcentration of Cadmiun, Chromiun, Copper, and Lead in

Drinking Water on the Polyacrylic Ester Resin, XAD-7,

Int. J. Environmental Analytical Chemistry, 19: 261-272.

85SUN 01 J. X. Sun and R. E. Jervis (1985) Neutron Activation Analysis of 35 Elements in Chinese

Standard Rocks (GSR) and Soils (GSS) Using the Slowpoke

Reactor, Journal of Radioanalytical and Nuclear Chemistry,

89: 553-560.

85WHI 02 R. T. White and G. E. Douthit (1985) Use of Microwave Oven and Nitric Acid-Hydrogen Peroxide

Digestion to Prepare Botanical Materials for Elemental

Analysis by Inductively Coupled Argon Plasma Emission

Spectrometry, Journal of the Association of Official

. Analytical Chemists, 68: 766-769.

85WOL 01 K. A. Wolnik, J. Rader, C. Gaston, and F. Fricke (1985)

Development of Laboratory Control Samples for the ICP-ES

Determination of Nutrient Elements in Rat Tissues,

Spectrochimica Acta, 40B: 245-251.

85WOO 01 I. H. Woo, H. Nishiyama, Y. Hashimoto, and Y. K. Lee (1985)

Determination of Seleniun in Coal Using Graphite Furnace

Atomic Absorption Spectrometry after Chemical Separation,

Bunseki Kagaku, 34: 599.

85XIA 01 S. Xiao-quan, Y. Zhi-neng, and N. Zhe-ming (1985)

Determination of Galliun in Sediment, Coal, Coal Fly Ash,

and Botanical Sanples by Graphite Furnace Atomic

Absorption Spectrometry using Nickel Matrix Modification,

Analytical Chemistry, 57: 857-861.

R-47
CODE N REFERENCE CODE N REFERENCE

85XIA 02 S. Xiao-quan, N. Zhe-ming, and Y. Zhi-ncng (1985) Determination of Indiun in Minerals, River Sediments, and

Coal Fly Ash by Electrothermal Atomic Absorption

Spectrometry with Palladium as e Matrix Modifier,

AnalyticB Chimica Acta, 171: 269-277.

85YAG 01 M. Yagi and K. Masumoto (1985) Stable- Isotope Dilution Activation Analysis for Special

Samples in which the Self -shielding Effect is Negligible,

Journal of Radioanalytical and Nuclear Chemistry, 90: 91-103

86GLA 01 E. S. Gladney, S. R. Garcia, and J. S. Newlin (1986) Determination of Elemental Composition of NBS SRM Coals via Automated Neutron Activation Analysis, Geostandards

Newsletter, 10: 77-80.

86GRE 01 R. R. Greenberg (1986) Elemental Characterization of the National Bureau of Standards Milk Powder Standard Reference Material by Instrunental and Radiochemical Neutron Activation Analysis,

Analytical Chemistry, in press.

85YAM 01 M. Yamamoto, M. Yasuda, and Y. Yamamoto (1985) Hydride -Generation Atomic Absorption Spectrometry Coupled

with Flow Injection Analysis, Analytical Chemistry,

57: 1382-1385.

86KAN 01 Y. Kanai, N. Imai, and S. Terashima (1986) Determination of UraniLm in Thirty-six Geological Reference

Samples by Fluorimetry and Extractive Spectrophotometry, Geostandards Newsletter, 10: 73.

85yAM 02 H. Yamamoto (1985) Rapid Dissolution of Plutoniun in Soil by Fusion with Aimonium Hydrogen Sulfate followed by Plutonium Determination by Ion Exchange arxJ Alpha Spectrometry,

Journal of Radioanalytical and Nuclear Chemistry,

90: 401-408.

85YAN 01 J. Y. Yang, C. L. Tseng, J. M. Lo, and M. H. Yang (1985) Determination of Traces of Lithiun in Biological,

Environmental, and Metal Samples by Neutron Activation

Analysis, Fresenius Zeitschrift fur Analytische Chemie,

321: 141-145.

85ZAC 01 D. Zachmann (1985) Geochemistry of Boron in Concentrations and Host Rock of Emsian Age in the Rheinische Schief ergebi rge. Federal Republic of Germany, Chemical Geology, 48: 213-229.

85ZHA 01 Y. K. Zhang, S. Hanamura, and J. D. Winefordner (1985) Evaluation of Microwave- induced Air-plasma as an Excitation

Source, Applied Spectroscopy, 39: 226-230.

86B0H 01 N. W. Bower, E. S. Gladney, and R. W. Ferenbaugh (1986)

A Critical Comparison of the X-ray Fluorescence and

Combustion- Infrared Methods for the Determination of Sulfuf

in Biological Matrices, Analyst, 111: 105-106.

86CAH 01 R. A. Cahill and A. D. Autrey (1986) Organic Carbon Measurements of Biological Materials from

a Large River Ecosystem: A Major Iitprovement over Indirect Estimates of Carbon Flow, in preparation.

86CHI 01 F. Chisela, D. Gawlik, and P. Bratter (1986) Instrunental Determination of some Trace Elements in Biological Materials by Epithermal and Thermal Neutron Activation Analysis, Analyst, 111: 405-410.

86ELS 01 H. N. Elsheimer (1986) Application of an Ion Selective Electrode Method to the Determination of Chloride in 41 International Geochemical Reference Materials, Geostandards Newsletter, In Press.

86F1S 01 I. B. Fischer (1986) Microwave Dissolution of Geologic Material: Application to

Isotope Dilution Analysis, Analytical Chemistry, 58: 261-263

86GAU 01 M. A. Gautier, E. S. Gladney, and B. O'Malley (1986) Quality Assurance for Health and Environmental Chemistry:

1985, Los Alamos National Laboratory report, LA-10813-MS.

86G1A 01 R. D. Giauque, J. M. Jaklevic, and A. C. Thompson (1986)

Trace Element Determination using Synchrotron Radiation,

Analytical Chemistry, 58: 940-944.

86KRA 01 B. Kratochvil, M. Duke, and 0. Ng (1986) Evaluation of Homogeneity of a Certified Reference Material by Instrimental Neutron Activation Analysis, Analytical

Chemistry, 58: 102-108.

86KRA 02 B. Kratochvil, N. Motkosky, M. Duke, and D. Ng (1986) Comparison of Instrunental Neutron Activation Analysis and Graphite Furnace Atomic At)sorption Spectroscopy for the Determination of Trace Aluninium Concentration and Homogeneity in the Biological Reference Material TORT-1, Analytical Chemistry, submitted.

86SCI 01 Sciex Corporation (1986) Analysis of NBS SRM 1577a: Bovine Liver, Sciex Application

Note 13586A.

86SCI 02 Sciex Corporation (1986) ICP/MS Analysis of NBS SRM 1633a: Coal Fly Ash, Sciex Application Note 13086A.

86TSU 01 M. Tsukada, K. Yamashita, K. Endo, and H. Nakahara (1986) Use of an Activatable Tracer for the Determination of Lanthanoid Elements in Biological and Environmental Standard Reference Material by Neutron Activation Analysis,

Analytical Chemistry, in press.

R-48
NBS-n4A (REV. 2-ac)

U.S. DEPT. OF COMM.

BIBLIOGRAPHIC DATA

SHEET (See instructions)

1. PUBLICATION OR

REPORT NO.

NBS/S P-260/111

2. Performing Organ. Report No 3. Publication Date

November 19 8 7

4. TITLE AND SUBTITLE

Compilation of Elemental Concentration Data for NBS Clinical, Biological,

Geological, and Environmental Standard Reference Materials

5. AUTHOR(S)

E. S. Gladney, B. T. O'Malley, I. Roelandts, T. E. Gills

6. PERFORMING ORGANIZATION (If joint or other than NBS. see instructions) 7. Contract/Grant No.

NATIONAL BUREAU OF STANDARDS

DEPARTMENT OF COMMERCE 8. Type of Report & Period Covere

yWAttlNGTON, D.C. 20234

1982-1986

9. SPONSORING ORGANIZATION NAME AND COMPLETE ADDRESS (Street, City. State, ZIP)

Same as No. 6

10. SUPPLEMENTARY NOTES

Library of Congress Catalog Card Number 87-619888

I I Document describes a computer program; SF-185, FlPS Software Summary, is attached.

li. ABSTRACT (A 200-word or less factual summary of most significant information. If document includes a si gnificant

bibliography or literature survey, mention it here)

Concentration data on as many as 92 constituents in 166 NBS Standard Reference

Materials have been collected from over 1500 journal articles and technical

reports. These data are summarized in consensus (mean) values with uncertainties

expressed as ± one standard deviation and compared with all available certification data from NBS. Data are presented on the analytical procedures employed

and all raw data are given in the tables. This compilation is a successor to

NBS Special Publication 260-88.

12. KEY WORDS (S/x to twelve entries; alphabeti cal order; capitalize only proper names; and separate key words by semicolons)

analytical methods; biological; certified; clinical; compilation; consensus values;

environmental; geological; informational values; literature values; mean values;

Standard Reference Materials; SRM

13. AVAILABILITY

[Unlimited

I I For Official Distribution. Do Not Release to NTIS

pO^Order From Superintendent of Documents, U.S. Government Printing Office, Washington, D.C.

20402.

Order From National Technical Information Service (NTIS), Springfield, VA. 22161

14. NO. OF

PRINTED PAGES

547

15. Price

^U.S. GOVERNMENT rRINTING OFFICE: 1 9 8 7 / 2 6 5-M / 6 01 8

2

USCOMM-DC 6043-PI

I

Technical Pubttcations

Periodical

Journal of Research—The Journal of Research of the National Bureau of Standards reports NBS research

and development in those disciplines of the physical and engineering sciences in which the Bureau is active.

These include physics, chemistry, engineering, mathematics, and computer sciences. Papers cover a broad

range of subjects, with major emphasis on measurement methodology and the basic technology underlying

standardization. Also included from time to time are survey articles on topics closely related to the Bureau's

technical and scientific programs. Issued six times a year.

Nonperiodicals

Monographs—Major contributions to the technical literature on various subjects related to the Bureau's scientific and technical activities. Handbooks—Recommended codes of engineering and industrial practice (including safety codes) developed in cooperation with interested industries, professional organizations, and regulatory bodies.

Special Publications—Include proceedings of conferences sponsored by NBS, NBS annual reports, and other

special publications appropriate to this grouping such as wall charts, pocket cards, and bibliographies.

Applied Mathematics Series—Mathematical tables, manuals, and studies of special interest to physicists,

engineers, chemists, biologists, mathematicians, computer programmers, and others engaged in scientific and

technical work.

National Standard Reference Data Series—Provides quantitative data on the physical and chemical properties

of materials, compiled from the world's literature and critically evaluated. Developed under a worldvwde program coordinated by NBS under the authority of the National Standard Data Act (Public Law 90-396).

NOTE: The Journal of Physical and Chemical Reference Data (JPCRD) is published quarterly for NBS by

the American Chemical Society (ACS) and the American Institute of Physics (AIP). Subscriptions, reprints,

and supplements are available from ACS, 1155 Sixteenth St., NW, Washington, DC 20056.

Building Science Series—Disseminates technical information developed at the Bureau on building materials,

components, systems, and whole structures. The series presents research results, test methods, and perfor- mance criteria related to the structural and environmental functions and the durability and safety

characteristics of building elements and systems.

Technical Notes—Studies or reports which are complete in themselves but restrictive in their treatment of a

subject. Analogous to monographs but not so comprehensive in scope or definitive in treatment of the subject

area. Often serve as a vehicle for final reports of work performed at NBS under the sponsorship of other

government agencies.

Voluntary Product Standards—Developed under procedures published by the Department of Commerce in Part 10, Title 15, of the Code of Federal Regulations. The standards establish nationally recognized re- quirements for products, and provide all concerned interests with a basis for common understanding of the

characteristics of the products. NBS administers this program as a supplement to the activities of the private

sector standardizing organizations.

Consumer Information Series—Practical information, based on NBS research and experience, covering areas of interest to the consumer. Easily understandable language and illustrations provide useful background

knowledge for shopping in today's technological marketplace.

Order the above NBS publications from: Superintendent of Documents, Government Printing Office,

Washington, DC 20402.

Order the following NBS publications—FIPS and NBSIR 's—from the National Technical Information Service, Springfield, VA 22161.

Federal Information Processing Standards Publications (FIPS PUB)—Publications in this series collectively

constitute the Federal Information Processing Standards Register. The Register serves as the official source of

information in the Federal Government regarding standards issued by NBS pursuant to the Federal Property

and Administrative Services Act of 1949 as amended, Public Law 89-306 (79 Stat. 1127), and as implemented

by Executive Order 11717 (38 FR 12315, dated May 11, 1973) and Part 6 of Title 15 CFR (Code of Federal

Regulations).

NBS Interagency Reports (NBSIR)—A special series of interim or final reports on work performed by NBS

for outside sponsors (both government and non-government). In general, initial distribution is handled by the

sponsor; public distribution is by the National Technical Information Service, Springfield, VA 22161, in paper

copy or microfiche form.
U.S. Department of Commerce

National Bureau of Standards

Gaithersburg, MD 20899

Official Business

Penalty for Private Use $300