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a

A

Section No. EMS _-2T

Revision No. 0
Date: Feoruary ise)
Page i oT C

II. QA TECHNICAL SERVICES AVAILABLE

A Standards Laboratory has seen established at CMSL/RTP. The
Standards Laboratory offers calibration, stanc

b
cation of client-owned sample material. . There
sarvica. where apolicabie, certifications

NBS Staneara Aeference Matarials.

ure at wnich caijoration is needed. tancarcizes ¢

tions are to de preferred.

the apeve

Static ana Filter Samples, Hi-Yoi, anc Organic Comoressea Gases
CONTACT:. Robert. L. | Lame;

: ~ Quality Assurance Division: (0-77

Environmental Monitoring Sys Laboratory

U. §. Environmental Protection Agency

Research Triangle Park, Ni
Telephone: TTS: ¢€29-4

5

77}



Seesion No. _=MSL oat?

Revision No. u

POON errs a c5-3 ee
Date: February .SéL
Po) By TA
Pace 2 oT 3

Tagie Rei (Continued)

Concentration Rance
pe hp

Vinyl Chlorice Several levels from 5 <5 40 oem SoA

i,2-Ditromo ethyiene Several

aervlonitrije

m 20 tc 100 poem 6t4

test samples


Section No. EMSL-C2
Revision ‘No. ]

Date: _ February i961
oT ta

. Pace 1

Priority Pollutant Catagcries for GC analyses - 12 categories
available. Priority Pollutants for GC/MS Analyses (as Volatile and

ang fazarcous

naj stancares



. Section Yo. _ EMSL-LY

- : Revision No.
Oate: —feariery “ez
Pace ss

—

Tabie L—t (Continued)



Section No. — EMSL-27?
i Revision No.
: Data: Feoruary 1Sé1
Page 2 oT j

——

Technic2] Services and Imerganic Compressed Gases

CONTACT: 8erne [. Bennett
Quality Assurance Division (MD-77)

Environmental Monitoring Systems Ladcratory
U. S. Environmental Protection Acenc
Research Triangle Park, NC 27711

Teleonone: FITS: 629-2266
lommerciai:

ray
ry
‘oO
on
tt
pan
&
a
OV
an

mation.



Section No.

. Revision ‘lo.
' : Date: “goruery izei a T
‘ Page . CF

computer data dase as part cf

Effects Research Laboratory -

Barta

toxic or nazardcus compouncs are
manufacturing and commercial uses are restricted, the Rencsitory nas

deen given the star7, eguicment and facilities nesced to dur

upgrade chemicals, and to perform complex chemical syntheses for



| Section No, — EMSL=aT!

: Revision No.

’ Date: Fenruary iSol
Pace } or 7

Mail Oreo 75

Tetangia Sark, Nerth

Di-eetor: Thomas &.

urate. awe verte
MESIA ANACYSTS



CT CS es ee poling ney oe oa

b t '
‘ 2 '
1 br 7 ' Aine
¢ z 4 2 to ane
1 a Avy
7 1 z { : piady
v € | 2 i ; qoney

7 t ‘ t eg

t é : ; , ‘ z ' 2 Squad
1 t + tReLAAOH

v C 2 1 1190

jou os. yu,


Section No. =MSLnLY
Revision No. Q
Data: Feoruar: iS6i

Page 12 or 20
Table L-5 (Continue)

Type Major Gamma Gamma
Isotope Emission Half-Life Peak (MeV) Abundance com/o*
Cane
26TH 2 1.4 _ _ 10,030

32,

3 _— —

2 4.5 _ _

2 Z.4 _— —_—

2— Liay _ ~—

3 422 v4 _ —



INTRODUCTICN

EMSL-CINCINNATI

CONTENTS

Pages Revision Dats
1 is) 2/82

14 ie) 2/81
29 0 2/82
10 a r/s2


Table Rei

MATERTALS AVAILABLE

Section No. EMSL-R7F
16 ——=—_—
Revision No. C
: NO
Date: February 126.

Page 2 oT i

AS COMPRESSED SAS CYLINCERS

TAR nee pew
ZC tam o:
pom CAM
2 pom methane with srovane ranging CAM
from 0.5 t2 6 oom :
Several, levels from 2 to 300 oem errs
feom 5 to 20,000 oom
Several levels from iC0CG <a 8000 som GCA
of metnane, anc 2CC ta 7CO sem of
ethane
tc 700 ‘pom. SCA
to 700 som SCA
to 70G poem GcA
zo 790 ppm 6CA



J]

2)

ai
79
oz

z

&
co
or
uw
Yar
o>
ow
oe

eoruarTM

vate

Page

a)
L
Q

a
3
fe]
tL
ww

a
2

ia

containiy

id

Fa
i

v

a

ataining

et

v

yearn

ter


Section No. _EMSL-C!

Revision No. GO
———

w Data: Fedruary 196!
Page Q cr i



action ‘No. EMSL-LY
vision 'o. “
te: feordary .s60

ce og OF

Gdn
wm 1D

ey

jm the lanoratory intercomparison stucie:

cm! ang ov un forms incigieg et tng ane ot th*s duu.
®
a cv

2 oS On. fee Tnetin iteturréns the 2scve ortiramt viv fe cl-
. agloactive otentarcs: :
e oren Themenan 702-7 S6-2147
FTS $$52i2
prey el atth ° 702-7 38-2874
FYS 3-257"
. 702 HF SE—_2i62
FYS $95-2142

- .  ieeercoapert



Section No. - EMSL-LY

Revision No. ie]
date: February isa.

Page 6 oT 29

3. Standard Monazite Ore

Principal radionuclides

and aporeximate activity -

4. Silutad Monazite Ore

Stlutad with loweactivity soils
5. Uranium Mit): Fatlines (ides. -

ana acoroximata activi : 287 sCi/¢
225n. . 342 C4/¢
“=“9n : 30C aCi/¢

5. Uranium Mil]

toy

A comcosite mixture from 1

Principal radionuclides’:

ang eccreximate activity - °°'Th : 3iL eci/¢
225 - ,
S“9n2 : SOL cCi/s

6
'
€

0

or

be

,

ab
ul

a)


Section No. EMSL-C!
Revision No. G
Date: __ February io
Page 5 oT z
Table C-2
LES FOR ORINKING WATER ANALYSES
crromium, lead, merc

AMPLES FOR PR

®
QUALITY CONTROL SAMP
®
®
t
e
QUALITY CONTROL S$
® CATESORIES (
e
haloethers (7)
Chlorinated Hycrocardens (9)
e " :
: Benzidi nes tay
Polynuclear Aromatics (16)
Pesticiaes/PC3s (25)
8
Purgeapies (26)
Trace Metais (15)
®

o
Q
oO

a Phenols (specif

» texaphene

wAttTy ont itawes
TORITY PCLLUTANTS,

moqunds/Categery)

Availabie bv i2/&

Acrolein, Ac

Nitrosamines



Revision No. _ G :
Date: Fepruary .ce.

Page a

Table C-i
FOR WATER QUALITY ANALYSES

QUALITY CONTROL SAMP

DEMAND ANALYSES ~ 80D, COD, TCC

MINERAL/PHYSICAL ANALYSES =~
ium, oH, $ te, chloride,

Sada,
city,

hardness, zctai dissaived so

er ee ee ae)
an, Orencoacss 3

> NO. 2 hi
ization analyses)

mo

rey

wo crucs oi]
s for characte

$
ia

Alper annayer
VOLATILE ORGANTO =


deo
We
YP pope
aE wy
7 ca]
t
+0
-ow
ow
—-
c
£ Oo
om
rue
peo wo
a>
yao
warm
a

@

a
&
rt

WOR ACA

ut
a



. Section No. _ EMSL-CT
H . Revision Ko. ‘ iy

| , Date: Fe = Tet

Page 7 le

Table Ct
REPOSITORY MATERIALS TO BE DISTRISUTED IN GANUARY 1981

Concantrations are 5,000 ug of OAS-pure compound oer mL of
methanol solvent uniess ot cnerwise noted.

COOL Acengortrene ECO4 genzene (10,0CC

““ EQO6 "Chiorebenzene (70,000 ng/mL) £007-1,2,4-Tricniorobenzene

£222 2-Chlerochencl £063 Shencl

Jaoxaphene. (GAT) oe _ .


Section No. _EMSL-LY
; Revision No. o
) Date: February 156i

Page ra oF 20

i¥. AQUEOUS CALIBRATED SAMPLES

The inventory of calibrated samples consists ©
trated recionuclide solutions (Table L-5). Except
avery effort is mace to maintain chis inventory so

snizped in 2 timely manner. Iodine-131 is prenarea bimontnly

ivigutes io requestors on recora. while cne tyes
>» every effort is mace ta

gies in tne inventory vary during tne year



»  600R81102 | assguzs

we

PPA QUALITY ASSURANCE OFFICER’S HANDBOOK

e
e
e
CAMS -OGE / 21
e . :
ssntal Protection Agency!
uibrary
 < th Dearborn Street
- aicago, Wunals 60604 - >
e o
Quality Assurance Management Staf+
Office of Monitoring Systems anc Quality Assuranca
U.S. Environmental ection Agency
e be AGL M Street,’ :
: Washington, 0.0. <
e


o ; Section Ne. EuSi-¢
. - Revision No.
Data: ao Er

) Page 10 v4

(vay

IV. PERFORMANCE EVALUATION STUDIE

Performance Evaiuation Stucies have tne primary purgcese of
e larly evaluating performance of laboratories as requireo oy SFA man-
aquest.

interest are sent

water,



No.
N

EMSL-CI
OQ. mo

ection
ision }

S
Rev

: rene)
w 4 i ct
= ow o mM oO
Or et -
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is Lue @ rm OD
a on ao a Gk we
N yogaiaigo w ai tw ce}
c COOKE. '-  ¥ ©
y wt owoo wv
NOvanoktoart red
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cl See Pr can an ed E Ww Qa
Bdot wan 6a P ca]
gene ye Pe Bb pevetoy
Tod wack o tot yo
10 1) CO cs mod On '
ou Ut - Jud ne
Kok



TOE

US. F...wenmental Protection Agency
~ ¥, Library

south Dearborn Street vag
Chicago, UMnols 60608 ..

Bp

fa _


Farere)
a7 000

oy th

» & 1

a n

o u

eros ral
i oR

Fay
are :



N Section No. 2MSEoLY

: Revision ‘Ne. o

. 4 ata: February .sa.
Page i or 28

A 7:1 dilution of the Climax sand tailines with loweactivity

wqliags
2 —OOWRG 2 2.4 somig
Towa 2 2.9 com/g
i
3



' i Section No. EMSL-C1
Revision No. ej
Date: February i196.
Page é oT

To establish qualitative identification and determine purity,
Repository cempounds are qualitatively and quantitatively measured by
at least two independent methodologies by the Repository staff and sub
sequently verified by at least two referee jaboratories, Significant

cifferences are resolvea before release of a campcuncd.

aoivenior

list cv the first Repository materials

S
pnenvis {PC3's) ana toxapnene, will te catagerized as CAR or CAT anc
fo u

x


‘ . Secticn No. EMSL-LY

a vg Revision No. t
' ’ : Date: February 1oe.
Page gor a
Taple Lt
RATIOS OF ACTIVITY MEASUREMENTS PERFORMED UNDER THE IDS
TRACEASILITY SRCGRAM WITH NGS, JANUARY 1974 TO JANUARY LSEO

EPA Value
Nuclide N

to the EMSL-LY

a
w
Oo
its)



eo

Type
Ambient Suifate-
Nitrata Sempies.

Sittion No. _=MSL-aT>

Re sion No. Cc

Da.a: Feoruary 156:
ee

Page 5 oT ic

Tabie RZ (Continued

from 0.02 72

Acueous potassium aitrate that similate 2
sourcs emissic¢n concentretion of i5C- ts

Dilute sulfuric acid that simulate 2

emissitn cancantration cf 200- tc 280C—m¢

a
a.
4
“nh
wo
4
0
I
ra)
o°
oO.
3
a
(o
5.
a
4
ft
°
3
a
w
o
o
oO
m7
Cc
a
aay
<t



7o

Sect ‘on No. — EMSL-RTP

Rev’ ion No. 0
Date.’ Feoruary Trét
Page § oT i0
Table R-3
PERFORMANCE AUDIT MATERTAL AVAILABLE AS FLOW MEASUREMENT DEVICE

Tyvoe : Sescriotion and Aucit Oursese

Antient A#i-vol Raterence consists of 4 set cf resistance niates

Flew Sevice sess as see :

: eye to simuiata various fitter loading conditions



Section “Yo.  EMSE-LY
Revisio: !No. vu

Cate: Fepruary iss.
Page i4 oT 29
Table Ld
CALIBRATED RAOIGNUCLIDE SAMPLES SUPPLIED AS NEEDED
Type Major Gemma Gamma
Isotcs Emission Haif-Livte Peak (Mey) Abundance com/c*

+ ttt 0.477
87,7 2.502 y 0.511
B-yy 22.20 ¢ 1.229
+ 27.704 ¢ 9.329
ws. a aan aeose en aan
a7 yy Teo Ss o.d4 39.875 2se,tCo
37 4 a 2.3L 9.45 230,ce°
a—,7 qd 1.0¢¢. 26.1 320,008
a 3 9.255 39.5 220, 5Cf
- a G.EkE $2.5 250,000
oy ary 167 ¢ 1.836 og .35 £56,000
as med asp +an
3-57 63.98 4 52.2 320,200
0. aqoce - ae
Y 33.35 <. cS .5 320,0CC
124 an er we
124s, bas7 60.20 ¢ $7.9 180,000
iis — 2 . a cael fat
“-"Ce + 127.85 4 30.5 180, 05C
oo" ea a~,y 32.50 4 4.0 220,060

a
fn
uy
rey
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in
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&
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oo

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mo Oo
©

3



. Section No. | -EMSL-Ci
Revision No. 0

Date: February 161
Pag 2 or TL
qT. QUALITY CONTROL SAMPLE PROGRAM

Quality Control (QC} samples are furnished without charge <9
interested governmental, imaustria], commercial, and private labor

a
‘

jity

tories for use ag secondary checks on their within-laboratory qué
control pregrams. The samples are intenced as independent measure

w
Q
an

tecnnicue and performance, mot as replacement for the standards, r

on. spike sampies

pecific metnocoiccy in tnese ©

there is no requirement for use of

Sampie Program now covers

analyses. Tne Quali

provice ‘the Priority Pollutants, Sut wii
con to cover ai] trace organics of interes= to tne Agency.
mole, ‘personnel ‘are being. acced to sugport cne Sroacer needs 6

Hedardous Wastes Program.

orann/mass spectrometry

organic comaounds wricn nave



: Section No. _EMSL-RTP
' Revision No. i]

‘ Date: february Sol
Page ic oT iis)

SOURC

tia
fan
to
oO
ry
3.
e
a
mt

»
ye
-t
a
my

SoG = fate t/a
Method ich.) 3/3L
3/84
Method § 30a 2/32
aecthed 7 Noy
ane
awit

A
—

Ri = G. Fuers

Quality Assuran ivision (M077)
Environmental * cring §



Section No. _ =MSL~c2

Revision No. 4

° “Date: february sel.
Page 13 oT 74

VI. ALTERNATE TEST PROCEDURES

In adaiticn to these services and matarials, ¢MSL-Cincinnati also
provides direct support by administering the Alternate Test Procedure
Program in botn the National Pollutant Oischarge Elimination System a
the National Interim Primary Orinking Water Regulations. Ail alternate
test orocedures intendea for limitec use apolications that are con-

sioered for approval at the state and regional jevel are forwarded to
ered pp " nes , <o

EMSL-Cincinnati for technical review and consistency witn orevious

actions.

in vne F

Larry Lobrin
Acting OA Of7i


ra a ow 4 Hong
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“ . wow ak
- 2 : Soe Loo M
: Soot Boag, Foe A
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Section No. eet
Revision No.

‘Date: Esoruary oo Feorgary Te 2o

Page 77s

EMSL = CINCINNAT?
26 W. St. Clair Street
Cincinnati, Ohio 45268

Director: Robert 1. 8cotn

WATER AND WASTEWATER ANALYSIS

ASL-Ci nrovides seven major cuaiity assurance sugocrt arograms:



Section No. EMS] WOT?

Revision No. 9
) Cate: Feoruary isél
Page 4 oT iT

Table RZ

PERFORMANCE AUDIT MATERIALS AVAILABLE AS STATIC AND FILTER SAMPLES

escriotion ana Audit Pursese

Loe

Ambient SO, Samoles Freeze-dried mixtures of sodium sulfite anc

potassium ‘<etracn}



_ Section No. EMSL ALY
Revision No. 0

Date: Feorvary iséi
Page 12 oT 29

Table L-5

CALIBRATED RACICNUCLICE SAMPLES KEPT IN INVENTORY

Type Major Gamna Gamma
rsotoce Emission dHalv—_ife Peak (Me¥) Abundance gom/o*

Su = 12.38 y ~_ ~ 16,006

ae §730 y —_ _ 10,005

~ 212.8 ¢ 3 $9.978 40,000

Y 276.3 3 25.8 3d, 3¢¢

a=, S.271 y 400 40,0C0

a+ $2 y _ _ 40,ces

: a7, 2aa.i ¢ Lilis 30.73 160,060

3+ _ ~_ 1sc.ccc

3-47 0.512 20.8 230,000

+ 9.088 B72 20.2 uCi/g

3—)7 280.2 ¢ 0.852 4,8 30,0C0

$-,7 2.77 ¢ 2.428 29.6 220,000

; a~.7 B.th¢ 0.256 61.2 20.4 uli/s

y 10.5 ¥ 0.286 2.2 180,000

“7"cs a~,y 2.062 y 6.608 37.6 40,000

“""es 3-47 30.27 ¢ 0.882 §3.0 20,006

itteg 8-57 284.3 0 0.134 16.3 320,c00

228R8 3 _ l8t0-y ~ 10,000

2238p a 5.78 y _ _ 30,069
220—. ->5 nt

i] ra 7.7 x 107 y _ — 10,C0¢


Section No. Introcuction

Revision Now
Date: _ February vol
Page oT

INTRODUCTION

This directory of services, materials, and performance evalua—
tions, available from the two Environmental Monitoring Systems Labore-
tories (&MSLs}, Iecateq in Las Yegas, Nevaca, anc Researcn Triangie
Park, North Carolina, and the one Environmental Monitoring and Support
Laboratory (also EMSL), located in Cincinnati, Chie, is offered Sy the
Quality Assurance Management Star? (QAMS) in response to many requests

from resianal and

Quality Assurance (QA Officers. lis
ver information resardine i i
ORD/EMSL Facilities.

Jaboratories free of

mough tner2 may be restricticns in some instances on hcw
s

ara used and how

mace throuan correspondence.
This compendium is providea in a jcose-iea? format sce that paaes

etec, cr otherw!_<

can sasiiy de replaced es information is ac

a
revised. Our intent jis to revise ‘tnis cccument
recuire. CAMS welcomes comments ana $s

utility of tnis pualication.


Sect jon No. EMSL-LY

Revision No. Cc

ae
Date: Feoruary 1961
Page on oT 2

g 2 20

+, J2llgn 37 daaiocnemistry Laporatories:

ICUS wastes:

t
fo
o
6
3
ray
7h
-
ta
is)
6
4
mH
&
3
@
wv
ard
at
fe
“&
'
my
3
a
é
oo
La
a
Q
€

Row Seediyeicai !

Jatiaation. and. &

asi wee a Lik ee

das emery 7%

ey Jlaporatories ana

i
: !
tens os someting tt drinking water or analyzing hazardous was
Qn

and assistance on raciaticn anda naz



Seezion No. =EMSL-2T? -
Revision No. :

Date: February ise.
Page 3 oT ig

Table Rot

tm

AMBIENT AiR 1981 AUDIT SCHEDUL
sanuary 5 - FS

February 2 - SCq NO

Maren 2 - co
“Maren 30 - S02 bubbler
Moe od - HiHYo?
vers Lb -~ We
- 39 = continuous
- %%
- sca = ww
- co
- § er

Novemter 2G = NOs dSuc6

CONTACT:

Robert L. Lampe
Quality Assuranca Division (40-77)
Environmental Monitoring Systems Laporaetsry ws
U. S. Environmental Oretection Agency
‘. Regearca Triangle Park,.NC. 27712
* Teleonone: 7S: $29-4521-

Commercial:



rm
N

Oo

<

Section No. EMS
Revision No. g

Date: February .S6.

Page 1s or

v. SPECTAL REFERENCE MATERIALS

a
@
4S
40
ny

Calibrated soil samples for use as reference materia
available. These samples have been cried, cround to pass 2 170—mash c
a 200—nesn screen, and carefully biended. Reports of caijbration

.:
actompany che samples. The samples are packaged in glass containers
a

wnicn contain acoreximately 10 grams et soil. Soi

934
= *F"U » 283 2Ct/¢

S12 aCilg
ia) 270 944. 226

Princisal daugnter srecucts - Cray Saha ooh y Seem
re aS
ewdny <h5q5 6H/ ons
woes, Ra, Ac, n,
Zita,

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Section No. EMSL-C?

> . \ Revision No.
Date: February
\ Date: Feb at ot
i Page i oT - i4

Table C-7

WATER SUPPLY STUDIES FOR GRINKING WATER CERIFICATION PROGRAM

Parameters - a1} MCL Parameters:

Trace Metais ~ Ag, As, 8a, Cd, Cr, Pb, Ho, Se
Nitrate/Fluoride
Lingane, Encrin, Metnexychnior, Toxapnena
2,40, 2,4.
( or

9

]

Semple Recuest Terics
eens aims
nSOCE i/3l -
4SOCS 7/8i =
wSCLO 1/82 -

WATER POLLUTION STUDIES

sieved

Minsr2ls - 9K,
Pot
Sui

Nutrients - Ammonia-N,
Tetai~

Demands - 80D, TOC, COD

Jrace Metais - Ai, As, Se, Cd,

Se, Zn, Sb, Ti,-.

Purgeables (11)

Chiordane, Cyanide

Study No. Semzie
‘WP.OO7 z/SL - 8/E2
WwPeOC8 9/81 - 2/82
weocs 3/S1 = 3/82
~~


Seczion No. EMS! UCT
_ Revision No.
Date: . February .961
i

Page is oT

]

VII. DEVELCPMENT OF MONITORING METHODS AND STANGARDS

Indirect suaport is also oproviced by developing stancardized
amalytical test orecedures to identify and measure pollutants and
quality characteristics, both cnemical and dicicgical, in drinking
water, ambient receiving waters, and effiuents. EMSL-Cincinnati also
develops cuality assurance manuais for use in water colluticn measure-

. ments.