Printed 11:18:47 02/12/05 Page: 1 of 5

S A M P L E I N F O R M A T I O N

Sample Name: WB386-03 B/1083411 (P920-2) Batch_or_Req_No N285/2 

Sample Type: Broad Unknown Date Acquired: 01/12/05 16:55:09 

Vial: 5 Acq. Method Set: AN054 1000A 

Analyst JD Date Processed: 02/12/05 11:12:18 

Injection Volume: 40.00 ul Processing Method: AN054 1000A 

Run Time: 14.0 Minutes Channel Name: 410 

Sample Set Name: n285 1000a Proc. Chnl. Descr.: AN054 1000A 

Auto-Scaled Chromatogram

MV

0.00

100.00

200.00

300.00

400.00

500.00

Minutes

2.00 4.00 6.00 8.00 10.00 12.00 14.00 12898

1

Name MP Mw Mn Polydispersity %Poly < MWM 500 %Poly < MWM 1000

Broad 12898 12575 2556 4.919857 4.499 10.360

Peak Results

All reported molecular weight distributions are calculated using polystryrene standards.

They will differ from absolute values depending on the structure and chemical differences between the test subtance and polystyrene.
Printed 11:18:47 02/12/05 Page: 2 of 5

GPC Calibration Plot

Log Mol Wt

1.50

2.00

2.50

3.00

3.50

4.00

4.50

5.00

5.50

Retention Time

5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00

1

2

3

4

5

6

7

8

Mol Wt

(Daltons) RT

Calculated 

Weight

(Daltons)

49170

19880

8450

1260

30330

12970

3370

925

6.248

6.248

6.248

6.248

6.542

6.542

6.542

6.542

44694

20331

8705

1258

30578

13676

3524

870

GPC Calibration Table For

Polystyrene Standards
Printed 11:18:47 02/12/05 Page: 3 of 5

dwt/d(logM)

Cumulative %

dwt/d(logM)

Cumulative %

0.00

0.20

0.40

0.60

0.00

20.00

40.00

60.00

80.00

100.00

Slice Log MW

4.50 4.00 3.50 3.00 2.50 MP=12898 Mn=2556 Mw=12575 Mz=26654 Mz+1=37852

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

20

21

RT Mol Wt Cumulative % Outside Vo-Vt Slice MW

6.030

6.112

6.179

6.241

6.298

6.351

6.400

6.445

6.488

6.527

6.564

6.599

6.632

6.665

6.696

6.725

6.754

6.783

6.810

6.837

6.864

59134

53209

48817

45104

41883

39118

36724

34646

32814

31195

29744

28427

27230

26125

25103

24158

23273

22439

21657

20918

20215

1.000

2.000

3.000

4.000

5.000

6.000

7.000

8.000

9.000

10.000

11.000

12.000

13.000

14.000

15.000

16.000

17.000

18.000

19.000

20.000

21.000

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

59134

53209

48817

45104

41883

39118

36724

34646

32814

31195

29744

28427

27230

26125

25103

24158

23273

22439

21657

20918

20215

22

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

40

41

42

RT Mol Wt Cumulative % Outside Vo-Vt Slice MW

6.890

6.916

6.941

6.966

6.990

7.015

7.039

7.064

7.088

7.112

7.136

7.159

7.183

7.207

7.231

7.255

7.279

7.303

7.327

7.351

7.376

19547

18913

18309

17730

17174

16641

16127

15631

15153

14692

14247

13815

13396

12991

12599

12216

11844

11483

11133

10792

10459

22.000

23.000

24.000

25.000

26.000

27.000

28.000

29.000

30.000

31.000

32.000

33.000

34.000

35.000

36.000

37.000

38.000

39.000

40.000

41.000

42.000

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

19547

18913

18309

17730

17174

16641

16127

15631

15153

14692

14247

13815

13396

12991

12599

12216

11844

11483

11133

10792

10459

GPC Distribution Table

Mp: 12898 Name: Broad
Printed 11:18:47 02/12/05 Page: 4 of 5

43

44

45

46

47

48

49

50

51

52

53

54

55

56

57

58

59

60

61

62

63

64

65

66

67

68

69

70

71

72

73

74

75

76

77

78

RT Mol Wt Cumulative % Outside Vo-Vt Slice MW

7.400

7.425

7.450

7.475

7.500

7.525

7.551

7.577

7.603

7.629

7.656

7.684

7.711

7.739

7.767

7.796

7.826

7.856

7.886

7.917

7.949

7.981

8.014

8.048

8.082

8.118

8.154

8.191

8.230

8.269

8.310

8.351

8.394

8.438

8.484

8.532

10135

9819

9510

9208

8914

8627

8347

8073

7805

7543

7287

7036

6791

6551

6315

6085

5859

5638

5421

5209

5001

4797

4598

4402

4210

4023

3839

3659

3483

3310

3142

2978

2818

2662

2509

2361

43.000

44.000

45.000

46.000

47.000

48.000

49.000

50.000

51.000

52.000

53.000

54.000

55.000

56.000

57.000

58.000

59.000

60.000

61.000

62.000

63.000

64.000

65.000

66.000

67.000

68.000

69.000

70.000

71.000

72.000

73.000

74.000

75.000

76.000

77.000

78.000

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

10135

9819

9510

9208

8914

8627

8347

8073

7805

7543

7287

7036

6791

6551

6315

6085

5859

5638

5421

5209

5001

4797

4598

4402

4210

4023

3839

3659

3483

3310

3142

2978

2818

2662

2509

2361

79

80

81

82

83

84

85

86

87

88

89

90

91

92

93

94

95

96

97

98

99

100

RT Mol Wt Cumulative % Outside Vo-Vt Slice MW

8.581

8.631

8.683

8.736

8.787

8.837

8.888

8.942

9.001

9.068

9.141

9.221

9.307

9.394

9.483

9.580

9.682

9.786

9.912

10.069

10.220

10.625

2217

2077

1942

1815

1699

1593

1492

1392

1289

1183

1077

971

870

778

693

612

536

469

399

326

269

159

79.000

80.000

81.000

82.000

83.000

84.000

85.000

86.000

87.000

88.000

89.000

90.000

91.000

92.000

93.000

94.000

95.000

96.000

97.000

98.000

99.000

100.000

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

No

2217

2077

1942

1815

1699

1593

1492

1392

1289

1183

1077

971

870

778

693

612

536

469

399

326

269

159

GPC Distribution Table

Mp: 12898 Name: Broad
Printed 11:18:47 02/12/05 Page: 5 of 5