Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

September 2009 

Prepared by: 

TEC Inc. 

1001 Bishop St. Suite 1400 

American Savings Bank Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 6

1.1 Project Objective .............................................................................................................. 6

1.2 Previous Reports .............................................................................................................. 6

1.3 Background ...................................................................................................................... 7

1.3.1 Site Description ......................................................................................................... 7

1.3.2 Facility Information .................................................................................................. 7

1.3.3 UST Information ....................................................................................................... 7

1.4 Previous Environmental Investigations ............................................................................ 7

1.5 Regulatory Updates ........................................................................................................ 10

1.6 RHMW05 Installation .................................................................................................... 10

2.0 Sample Collection and Analyses ........................................................................................ 10

2.1 Monitoring Well Purging ............................................................................................... 11

2.2 Groundwater Sample Collection .................................................................................... 11

2.3 Groundwater Sample Analyses ...................................................................................... 11

3.1 July 2009 Sample Analytical Results ............................................................................. 15

3.2 Groundwater Contaminant Trend ................................................................................... 16

3.3 Results of Oil/Water Interface Measurements ............................................................... 17

3.4 Groundwater Status ........................................................................................................ 18

4.0 Summary and Conclusions ................................................................................................. 21

5.0 References .......................................................................................................................... 25

List of Tables 

Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ..13 

Table 2 MADEP Analytical Results .........................................................................................14 

Table 3 Oil/Water Interface Measurements ..............................................................................18 

Table 4 Action Levels for Compounds of Concern ..................................................................18 

Table 5 Results Categories and Responses to Groundwater Monitoring Results .....................19 

List of Figures 

Figure 1 MADEP VPH/EPH Analyses ......................................................................................12 

Figure 2 TPH Trends in Groundwater, Round 16 (July 15, 2009) .............................................23 

Figure 3 PAH Trends in Groundwater, Round 16 (July 15, 2009) ............................................24 

List of Appendices 

Appendix A – Laboratory Analytical Reports 
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Red Hill Fuel Storage Facility September 2009 

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Executive Summary 

This quarterly groundwater monitoring report presents the results of groundwater sampling 

conducted on July 15, 2009 at the United States (US) Navy Bulk Fuel Storage Facility at Red 

Hill, Oahu, Hawaii (the Facility). The sampling and reporting was conducted by TEC Inc. (TEC) 

for the Fleet and Industrial Supply Center (FISC) at Pearl Harbor, Hawaii. This report is part of 

a series of quarterly groundwater monitoring reports provided by the US Navy to the State of 

Hawaii Department of Health (HDOH) in accordance with HDOH’s release response 

requirements. Currently, there are 18 active and 2 inactive, 12.5 million gallon, field-constructed 

underground storage tanks (USTs) located at the Facility. 

Background 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from the 

Facility USTs and provides approximately 24 % of the potable water to the Pearl Harbor Water 

System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system, a background groundwater 

monitoring well (RHMW04) up-gradient from the Facility adjacent to the US Navy Firing Range, 

and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery 

(RHMW2254-01). 

All five wells were sampled twice as part of a comprehensive environmental investigation and 

risk assessment (TEC, 2006). For this investigation, groundwater samples were analyzed for 

petroleum constituents and compared against HDOH Drinking Water Environmental Action 

Levels (EALs) (HDOH, July 2005). In addition, a three-dimensional (3-D) groundwater model 

was developed to produce site-specific risk-based levels (SSRBLs) for compounds of concern. 

The results of this modeling effort indicated that Jet Propulsion (JP)–5 fuel presented the biggest 

risk to the US Navy water supply, due to its mobility and toxicity. Finally, the model 

determined that a non-aqueous plume (free product) of JP-5 would need to migrate to within 

1,100 feet of the US Navy Well 2254-01 infiltration gallery for HDOH EALs to be exceeded 

within the gallery. Based on this, free-product must be observed at RHMW01 for EALs to be 

exceeded at the US Navy Well 2254-01. 

In April 2009, another groundwater monitoring well (RHMW05) was installed down-gradient 

from the Facility, within the lower access tunnel between RHMW01 and RHMW2254-01. It 

was installed to identify the extent of contaminant migration down-gradient before it reaches the 

infiltration gallery at RHMW2254-01 (see Figure 2). 

 
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During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The HDOH Drinking Water 

toxicity EAL for these compounds was 240 g/L. This concentration assumed that 

methylnaphthalenes were not human carcinogens. Once evidence emerged and was accepted by 

the US Environmental Protection Agency (USEPA) that methylnaphthalenes are carcinogenic to 

humans, HDOH adopted more rigorous EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L 

for 2-methylnaphthalene (HDOH, 2008). 

The HDOH Drinking Water EAL for naphthalene was also updated during this process. 

Previously, HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation 

Goal (USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. In 

deference to the California Department of Public Health’s Drinking Water Notification Levels, 

(HDOH, 2008) HDOH updated their naphthalene drinking water EAL to 17 g/L. 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the Groundwater Gross Contamination EAL for TPH-DRO remains 100 g/L. 

Groundwater Protection Plan 

In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater 

Protection Plan (TEC, 2008), which specified SSRBLs and various required actions based on the 

category status (i.e., categories 1 through 4) of each groundwater monitoring well. The main 

objective of the Plan is to protect the groundwater quality of US Navy Well 2254-01, which 

provides potable water to the PHWS. This is accomplished by comparing petroleum 

concentrations in the Facility wells to established SSRBLs and taking appropriate action. A 

secondary, but important objective of the Plan is to identify leaking USTs by evaluating 

increasing concentration trends, or the presence of free product in one or more groundwater 

monitoring wells. This quarterly report compares observed water quality to these established 

categories and associated actions. 

Current Results 

On July 15, 2009, five groundwater samples (i.e., RHMW01, RHMW02, RHMW03, RHMW05 

and RHMW2254-01), along with the required quality control samples (duplicate, matrix spike, 

spike duplicate, and trip blank) were collected for analysis. Samples were analyzed for Total 

Petroleum Hydrocarbons (TPH) quantified as Diesel-Range Organics (DRO) and Gasoline 

Range Organics (GRO), Volatile Organic Compounds (VOCs), Polynuclear Aromatic 

Hydrocarbons (PAHs), and dissolved lead. 

In addition, groundwater samples from RHMW01, RHMW02, and RHMW03 were analyzed by 

the Massachusetts Department of Environmental Protection (MADEP) method (see Figure 1) for 

Extractable Petroleum Hydrocarbons (EPH) and Volatile Petroleum Hydrocarbons (VPH). 

 

TPH-DRO

TPH-DRO was detected at 248 micrograms per liter (μg/L) in RHMW01, 1,375 μg/L (i.e., the 

average of normal and duplicate samples) in RHMW02, and at 491 μg/L in RHMW05 (i.e., the 

recently installed monitoring well). TPH-DRO was not detected above the laboratory method 
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detection limit (MDL) at RHMW03 and RHMW2254-01. The HDOH Drinking Water EAL and 

SSRBL for TPH-DRO are 210 μg/L and 4,500 μg/L, respectively. 

TPH-GRO

For TPH-GRO the HDOH Drinking Water EAL is 100 μg/L. In samples RHMW01, RHMW02, 

RHMW02D (i.e., the duplicate sample collected), RHMW03, RHMW05, and RHMW2254-01 

TPH-GRO was not observed above the laboratory MDL (i.e., 30 μg/L). 

Other Parameters above HDOH Drinking Water EALs

At RHMW01, the concentration for 1-methylnaphthalene was 9.44 μg/L. At RHMW02, the 

average concentration between the normal and duplicate sample of 1-methylnaphthalene was 

11.9 μg/L. Both these results are above the HDOH Drinking Water EAL for 1-

methylnaphthalene of 4.7 μg/L. 

MADEP-EPH and MADEP-VPH Results

EPH and VPH constituents were only detected above the laboratory MDL at RHMW02. At 

RHMW02, the average of the normal and duplicate samples for EPH C11 - C22 aromatics 

averaged 275 μg/L. For EPH C9 - C18 aliphatics, at RHMW02 the average of the normal and 

duplicate samples was 270 μg/L. The average concentration of the normal and duplicate samples 

at RHMW02 for total EPH was 545 μg/L. 

Also at RHMW02, VPH C9 - C10 aromatics averaged a concentration of 455 μg/L. Total VPH 

was also detected at RHMW02 with an average concentration of 455 μg/L at RHMW02. A 

separate memorandum that discusses these EPH and VPH results relative to the companion TPHDRO and TPH-GRO will be issued. 

Trend Analysis 

The following is a discussion of compounds that exceeded HDOH Drinking Water EALs during 

two or more recent consecutive sampling events, thus establishing a trend: 

 

RHMW01

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005, but less than 25 percent of the SSRBL of 4,500 g/L. In July 2009, 

the result of 248 μg/L TPH-DRO was lower in concentration than any previous round since 

September 2005. TPH-DRO at RHMW01 is exhibiting a decreasing trend. 

RHMW02

At RHMW02, from September 2005 through February 2009, TPH-DRO exceeded the HDOH 

Drinking Water EAL and was greater than 50 percent of the SSRBL (estimated solubility limit of 

4,500 g/L). However, in May and July 2009, the average TPH-DRO concentrations (1,810 

g/L and 1,375 μg/L respectively) exceeded the HDOH Drinking Water EAL, but were below 

50 percent of the SSRBL. 

The July 2009 average TPH-DRO concentration represents the lowest concentration observed 

since September 2005. TPH-DRO is exhibiting a decreasing trend by having significantly 
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decreased over the last three sampling events (i.e., February, May, and July 2009). By way of 

comparison, in October 2008, the SSRBL for TPH-DRO of 4,500 g/L was exceeded. 

For other parameters, although the 1-methylnaphthalene average concentration (i.e., 11.9 g/L) 

exceeded the HDOH Drinking Water EAL of 4.7 g/L, there is a decreasing trend associated 

with 1-methylnaphthalene. The average concentrations of 1-methylnaphthalene observed during 

the October 2008, February 2009, May 2009, and July 2009 sampling events has respectively 

been 67.25 g/L, 22 g/L, 21.25 g/L, and 11.9 g/L. 

RHMW03

At RHMW03, historically, concentrations of TPH-DRO have fluctuated around the HDOH 

Drinking Water EAL, but have been significantly lower than corresponding values observed at 

RHMW01 and RHMW02. However, during the last two sampling events (i.e., May and July 

2009), TPH-DRO was not detected above the MDL. These results represent a continuing 

decreasing trend for TPH-DRO that has existed since October 2008. 

RHMW05

At RHMW05 there is an increasing trend for TPH-DRO. The July concentration of TPH-DRO 

of 491 μg/L exhibited an increase as compared with the May 2009 concentration of 200 μg/L, the 

first sampling event for RHMW05. However, the July 2009 concentration is less than 25 percent 

of the SSRBL for TPH-DRO. 

US Navy Well 2254-01

At US Navy Well 2254-01, trace concentrations of TPH-GRO and 2-methylnaphthalene that 

were observed in the February and May 2009 sampling events were not observed in July 2009. 

In addition, all other parameters were not detected as well. 

Current Groundwater Status 

To date, there is no observation of a trend (i.e., two or more consecutive events) of fuel presence 

on groundwater at any of the Facility monitoring wells. 

US Navy Well 2254-01(measured at RHMW2254-01)

Based upon the July 2009 sampling event, the US Navy Well 2254-01 has been removed from 

the provisional category 1 status since no compounds were detected above the laboratory MDLs. 

RHMW03

RHMW03 is no longer in Category 1 status because no compounds were detected above the 

laboratory MDL. 

Category 1 Status Locations

There are no Category 1 status locations. 
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Category 2 Status Locations

RHMW01 

The July 2009 sampling event indicates that RHMW01 should remain in Category 2 status. This 

is because the TPH-DRO concentration of 248 g/L is greater than the HDOH Drinking Water 

EAL (210 g/L), but less than half the SSRBL of 4,500 g/L (estimated solubility limit of JP-5) 

and the 1-methylnaphthalene concentration (i.e., 9.44 g/L) exceeded the HDOH Drinking 

Water EAL of 4.7 g/L. 

RHMW02 

The July 2009 sampling event results in RHMW02 remaining in Category 2 status since TPHDRO [1,450 g/L and 1,300 g/L (duplicate)] is greater than the HDOH Drinking Water EAL 

(210 g/L), but is less than half the established SSRBL value of 4,500 g/L and the 1-

methylnaphthalene average concentration (i.e., 11.9 μg/L) exceeded the HDOH Drinking Water 

EAL of 4.7 g/L. 

RHMW05

Based upon the July 2009 sampling event, the second event for this newly installed well, 

RHMW05 now holds a Category 2 status. TPH-DRO at RHMW05 (i.e., 491μg/L) is above the 

drinking water EAL of 210 μg/L and has been showing an increasing trend over the last two 

rounds (i.e., 200 μg/L in May 2009 and 491μg/L in July 2009). 

 

Category 2 for RHMW01, RHMW02, and RHMW05 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 or 4 Status Locations

There are no Category 3 or 4 status locations. 

Conclusions and Recommendations 

There is no indication of an immediate threat of disruption to drinking water resources of the US 

Navy Well 2254-01 as a result in the July 2009 data. Based upon the July 2009 data, the US 

Navy Well 2254-01 has been removed from the provisional Category 1 status that was 

established following the May 2009 sampling event. 

With the exception of RHMW05, compound concentrations for all the other monitoring wells 

(i.e., RHMW01, -02, -03, and RHMW2254-01) are exhibiting decreasing contaminant trends and 

thus have improved in groundwater quality as compared to results from recent sampling events. 

In fact, the July 2009 event has resulted in RHMW03 being removed from Category 1 status. 

Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead 

will continue at the Facility until such time that data indicates that a different monitoring plan is 

warranted. It is recommended that future quarterly analytical results be closely assessed at 

RHMW05, since this is currently the only well exhibiting an increasing contaminant trend (i.e., 

200 μg/L in May 2009 and 491μg/L in July 2009 for TPH-DRO). 
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1.0 Introduction

This report presents the results of the 16th groundwater sampling event, conducted in July 2009 

at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). The 

Facility consists of 18 active and 2 inactive underground storage tanks (USTs) operated by the 

Fleet and Industrial Supply Center (FISC), Pearl Harbor. The groundwater sampling and 

analysis event is part of a groundwater monitoring program for the UST site in response to past 

UST releases, previous environmental investigations, and recommendations from the State of 

Hawaii Department of Health (HDOH). 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater underlying the Facility. The project was conducted to ensure 

the Navy remains in compliance with HDOH UST release response requirements as described in 

Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release Response Action. The 

groundwater sampling program followed the procedures described in Red Hill Bulk Fuel Storage 

Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008], also referred to as “the Plan”. 

This groundwater sampling event was conducted by TEC under United States (US) Navy 

Contract Number N47408-04-D-8514, Task Order No. 54. 

1.2 Previous Reports 

The following groundwater monitoring reports were previously submitted to the HDOH: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); 

14. Groundwater Monitoring Results, February 2009 (submitted May 2009); and 
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15. Groundwater Monitoring Results, May 2009 (submitted July 2009) 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the 

Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south 

and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east 

of the Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet hydraulically down-gradient from the Facility (Dawson, 2006). The US Navy Well 

2254-01 is located approximately 3,000 feet down-gradient (west) of the Facility and provides 

approximately 24% of the potable water to the Pearl Harbor Water System, which serves 

approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel). Previously, several tanks stored 

Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Previous Environmental Investigations 

1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess 

potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy 

installed a one-inch diameter RHMW01 (previously known as MW-V1D) to monitor for 

contamination of the basal aquifer underlying the Facility. The well was installed and completed 

at approximately 100 feet below grade within the lower access tunnel. At the time of well 

completion, depth to water in RHMW01 was measured at 86 feet below grade (Dawson, 2006). 

In February 2001, groundwater samples collected from RHMW01 contained total petroleum 

hydrocarbons (TPH) concentrations ranging from 883 micrograms per liter (g/L) to 1,050 g/L 

and total lead ranging from 10.4 g/L to 15 g/L. The maximum total lead concentration in the 

samples was equal to the primary drinking water standard of 15 g/L for lead and exceeded the 

HDOH Tier 1 groundwater action level of 5.6 g/L (Dawson, 2006). 
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2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing 

monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 

and the Red Hill Navy Pump Station (US Navy Well 2254-01) in February, June, September, and 

December 2005. 

Samples collected in February and June 2005 were not filtered in the field prior to analysis for 

lead. Analytical results for samples collected from RHMW01 indicated concentrations of total 

lead were above the HDOH Tier 1 action level of 5.6 g/L. The results were not considered 

appropriate for risk assessment since the sample had not been filtered. In addition, lead was not 

a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility 

construction material (TEC, 2007). 

Samples were filtered in September and December 2005, and dissolved lead concentrations were 

below the HDOH Tier 1 action level. Concentrations of all other contaminants of potential 

concern were below HDOH Tier 1 action levels. 

2005 – Site Investigation: As part of a site investigation, TEC installed three groundwater 

monitoring wells at the Facility between June and September 2005. Well RHMW02 was 

installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the 

lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically 

upgradient of the USTs to provide geochemistry for water moving through the basal aquifer 

beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of 

approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of 

approximately 300 feet below ground surface outside the tunnel. Groundwater samples were 

collected from the three newly installed wells and two existing wells (RHMW01 and US Navy 

Well 2254-01) in September 2005. 

Naphthalene and trichloroethylene were detected in samples collected from RHMW02 at 

concentrations greater than the HDOH Tier 1 action levels. Lead was detected in the sample 

collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; 

however, the sample was not filtered in the field prior to analysis. Analytical results for filtered 

samples obtained by Dawson during the same period indicated concentrations of dissolved lead 

were below the HDOH Tier 1 action level. 

2006 – Site Investigation: Dedicated sampling pumps were installed in five wells (RHMW01, 

RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater 

samples from the wells in July 2006. The groundwater samples were analyzed for petroleum 

constituents. Naphthalene was detected in samples collected from RHMW02 at concentrations 

above the HDOH Tier 1 action level. 

In September 2005, with concurrence from the HDOH, the Navy decided to use the newer 

HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk 

Assessment project. The EALs are current and provide action levels for more chemicals, and are 

much more useful for conducting screening risk assessments. Since the HDOH (HDOH May 

2005) Policy Letter stated that the two sets of action levels should not be mixed, the Tier 1 
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screening levels presented in HAR Section 11-281-78 would no longer be used to evaluate 

environmental impact at the Facility. 

2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. 

Analytical results indicated the following: 

 No chemicals were detected in groundwater from US Navy Well 2254-01 or RHMW03; 

 TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH 

Drinking Water EALs in RHMW01; and 

 TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected 

in groundwater above the HDOH Drinking Water EALs in RHMW02. 

2007 – Groundwater Sampling: Groundwater samples were collected in March, June, and 

September 2007. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three 

sampling events; 

 TPH-GRO exceeded HDOH Drinking Water EALs at RHMW02 in March; 

 TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during 

all three sampling events; 

 1-methylnaphthalene and 2-methylnaphthalene exceeded the HDOH Groundwater Gross 

Contamination EAL at RHMW02 during all three sampling events; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in June. 

2008 – Groundwater Sampling: Groundwater samples were collected in January, April, July, 

and October 2008. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace detections of 1-methylnaphthalene and naphthalene prompted a resample event in 

December at US Navy Well 2254-01, no chemicals were detected above the MDL; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all four sampling 

events; 

 TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 

 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 during all four sampling 

events. 

2009 – Groundwater Sampling: Groundwater samples were collected in February, May, and 

July 2009. Analytical results indicated the following: 

 No chemicals have been detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace TPH-GRO at US Navy Well 2254-01 was detected above the laboratory MDL and 

significantly below the laboratory reporting limit and HDOH EAL, but has most recently 

not been detected; 
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 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01; 

 TPH-GRO has not exceed HDOH Drinking Water EALs at RHMW02; 

 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02, however most recently only TPH-DRO and 

1-methylnaphthalene exceeded the HDOH Drinking Water EALs; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in February, but not in 

May or July; and 

 TPH-DRO exceeded HDOH Drinking Water EAL at RHMW05 during the July 2009 

sampling event. 

1.5 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

The drinking water EAL for naphthalene has also been updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels, a Hazard Index of 2.7 

(HDOH, 2008). 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 100 

g/L. 

1.6 RHMW05 Installation 

In April 2009, a new groundwater monitoring well, RHMW05, was installed by TEC under US 

Navy Contract Number N47408-04-D-8514, Task Order No. 54. RHMW05 is located downgradient from the Facility, within the lower access tunnel between RHMW01 and RHMW2254-

01(located at the US Navy Well 2254-01). It was installed to identify the extent of contaminant 

migration down-gradient prior to contaminants reaching the infiltration gallery at the US Navy 

Well 2254-01. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on July 15, 2009. 

Groundwater samples were collected from four monitoring wells located inside the Facility 

lower access tunnel and one monitoring well located at the Red Hill Navy Pump Station. 

Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility 

Groundwater Protection Plan (TEC, 2009). A total of eight samples were collected as follows: 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

11 

 one environmental sample from RHMW2254-01 (i.e., located at the US Navy Well 

2254-01), RHMW01, RHMW02, RHMW03, and RHMW05; 

 one duplicate sample from RHMW02 (sampled as RHMWA01 and reported as 

RHMW02D); and 

 one matrix spike and matrix spike duplicate from RHMW2254-01. 

2.1 Monitoring Well Purging

All monitoring wells were purged prior to sampling. In general, well purging was considered 

complete when no less than three successive water quality parameter measurements had 

stabilized within approximately 10 percent. Field parameters were measured at regular intervals 

during well purging and included pH, temperature, specific conductivity, dissolved oxygen, and 

turbidity. At RHMW02 due to technical difficulties, in lieu of collecting field parameters, the 

well was sampled once the historically highest purge water volume was exceeded by over 20 

percent. Purge water was collected and disposed in the Facility oil/water separator system. 

2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. All wells were sampled 

directly from their dedicated bladder pump system, except for RHMW02 and RHMW05. 

RHMW02 and RHMW05 were sampled using disposable bailers. Samples were placed into 

sampling containers with appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile 

organic analysis, nitric acid (HNO3) for dissolved lead]. Dissolved lead samples were filtered in 

the field and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by 

EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. In addition, groundwater 

samples from RHMW01, RHMW02, and RHMW03 were analyzed by Test America in 

Westfield, Massachusetts for EPH and VPH by the MADEP method. 

Figure 1 depicts the analytical relationship between samples analyzed for TPH-GRO/TPH-DRO 

and MADEP VPH/EPH. As seen in Figure 1, if the concentrations of the three EPH fractions 

and target PAH analytes were added together, it would be equal to a traditional “TPH” value. 

Similarly, if the three VPH fractions and BTEX/MtBE & naphthalene concentrations were added 

together, it would equal a GRO value. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

12 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

four monitoring wells located in the lower access tunnel of the Facility and one monitoring well 

located at the Red Hill Navy Pump Station. Duplicate sample results from monitoring well 

RHMW02 are reported in this document as RHMW02D. A summary of groundwater analytical 

results for TPH-DRO and TPH-GRO, VOCs, PAHs, and dissolved lead is included in Table 1. 

A summary of groundwater analytical results for the MADEP-EPH and MADEP-VPH is 

included in Table 2. Complete analytical laboratory reports are provided in Appendix A. 

Figure 1. MADEP VPH/EPH Analyses 

Source: Massachusetts Department of Environmental Protection, Implementation of the MADEP VPH/EPH Approach, 

Final Policy, October 31, 2002 
Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (July 15, 2009)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result 

TPH as DIESEL RANGE ORGANICS 210 100 248 F 161 430 1450 150 400 1300 150 400 ND 

TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100 ND U 30 100 ND U 30 100 ND 1-METHYLNAPHTHALENE 4.7 10 9.44 0.158 0.526 13.2 0.156 0.521 10.6 0.165 0.549 ND 

2-METHYLNAPHTHALENE 24 10 3.07 0.158 0.526 3.66 0.156 0.521 2.58 0.0165 0.0549 ND ACENAPHTHENE 370 20 0.18 0.0158 0.0526 0.235 0.0156 0.0521 0.213 0.0165 0.0549 ND ACENAPHTHYLENE 240 2000 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND ANTHRACENE 1800 22 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND 

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND 

BENZO(a)PYRENE 0.2 0.81 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND 

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND 

BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND 

CHRYSENE 9.2 1 0.0159 F 0.0158 0.0526 0.0162 F 0.0156 0.0521 ND U 0.0165 0.0549 ND 

DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND 

Chemical

RHMW01

UG/L

RHMW02

UG/L

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

July 15, 2009 July 15, 2009 July 15, 2009 

RHMW02D

UG/L

8015B (Petroleum)

8270C SIM 

(PAHs)

Method

( )

FLUORANTHENE 1500 130 0.0263 F 0.0158 0.0526 0.0247 F 0.0156 0.0521 0.0199 F 0.0165 0.0549 ND 

FLUORENE 240 950 0.0952 0.0158 0.0526 0.115 0.0156 0.0521 0.108 0.0165 0.0549 ND INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.0158 0.0526 ND U 0.0156 0.0521 ND U 0.0165 0.0549 ND NAPHTHALENE 17 21 5.61 0.326 1.05 8.37 0.323 1.04 6.71 0.341 1.1 ND 

PHENANTHRENE 240 410 0.0349 F 0.0158 0.0526 0.0304 F 0.0156 0.0521 0.0291 F 0.0165 0.0549 ND PYRENE 180 68 0.027 F 0.0158 0.0526 0.0272 F 0.0156 0.0521 0.0189 F 0.0165 0.0549 ND 1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND 1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND 1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND NAPHTHALENE 17 21 ND U 0.62 2 10.1 0.62 2 11.2 0.62 2 ND STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TOLUENE 1000 40 ND U 0 31 1 ND U 0 31 1 ND U 0 31 1 ND 

8260B 

(VOCs)

TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND 

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method dete

U - Indicates that the compound was analyzed for but not detected at or above the stated limit

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

12

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater , HDOH, 2009

200

Page 1 of 1
Table 2. MADEP Analytical Results for Quarterly Groundwater Monitoring Release Response Report (July 15, 2009)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Resu

2-METHYLNAPHTHALENE 24 10 ND U 10 10 ND U 10 10 ND ACENAPHTHENE 370 20 ND U 10 10 ND U 10 10 ND ACENAPHTHYLENE 240 2000 ND U 10 10 ND U 10 10 ND ANTHRACENE 1800 22 ND U 10 10 ND U 10 10 ND BENZO(a)ANTHRACENE 0.092 4.7 ND U 10 10 ND U 10 10 ND BENZO(a)PYRENE 0.2 0.81 ND U 10 10 ND U 10 10 ND BENZO(b)FLUORANTHENE 0.092 0.75 ND U 10 10 ND U 10 10 ND BENZO(g,h,i)PERYLENE 1500 0.13 ND U 10 10 ND U 10 10 ND BENZO(k)FLUORANTHENE 0.92 0.4 ND U 10 10 ND U 10 10 ND TOTAL EXTRACTABLE PETROLEUM HYDROCARBONS NS NS ND U 100 100 540 100 100 550 CHRYSENE 9.2 1 ND U 10 10 ND U 10 10 ND EXTRACTABLE PETROLEUM HYDROCARBONS C11-C22 AROMATIC NS NS ND U 100 100 270 100 100 280 EXTRACTABLE PETROLEUM HYDROCARBONS C19-C36 ALIPHATIC NS NS ND U 100 100 ND U 100 100 ND EXTRACTABLE PETROLEUM HYDROCARBONS C9-C18 ALIPHATIC NS NS ND U 100 100 270 100 100 270 FLUORANTHENE 1500 130 ND U 10 10 ND U 10 10 ND FLUORENE 240 950 ND U 10 10 ND U 10 10 ND INDENO(1,2,3-cd)PYRENE+DIBENZ(a,h)ANTHRACENE NS NS ND U 10 10 ND U 10 10 ND NAPHTHALENE 17 21 ND U 10 10 ND U 10 10 ND PHENANTHRENE 240 410 ND U 10 10 ND U 10 10 ND PYRENE 180 68 ND U 10 10 ND U 10 10 ND BENZENE 5 170 ND U 5 5 ND U 5 5 ND ETHYLBENZENE 700 30 ND U 5 5 ND U 5 5 ND M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 10 10 ND U 10 10 ND NAPHTHALENE 17 21 ND U 10 10 ND U 10 10 ND O-XYLENE (1,2-DIMETHYLBENZENE) NS NS ND U 5 5 ND U 5 5 ND tert-BUTYL METHYL ETHER NS NS ND U 5 5 ND U 5 5 ND TOLUENE 1000 40 ND U 5 5 ND U 5 5 ND TOTAL VOLATILE PETROLEUM HYDROCARBONS NS NS ND U 100 100 420 100 100 490 VOLATILE PETROLEUM HYDROCARBONS C5-C8 ALIPHATIC NS NS ND U 100 100 ND U 100 100 ND VOLATILE PETROLEUM HYDROCARBONS C9-C10 AROMATIC NS NS ND U 100 100 420 100 100 490 VOLATILE PETROLEUM HYDROCARBONS C9-C12 ALIPHATIC NS NS ND U 100 100 ND U 100 100 ND 

MADEP EPH - Massachusetts Department of Environmental Protection Extractable Petroleum Hydrocarbons MDL - Method detection limitMADEP VPH - Massachusetts Department of Environmental Protection Volatile Petroleum Hydrocarbons RL - Reporting limit

UG/L - Micrograms per Liter ND -

Q - Data qualifier

U - Indicates that the compound was analyzed for but not detected at or above the stated limit NS- Indicates that the EAL for the 

12

Method

HDOH Drinking 

Water EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Chemical

RHMW01

UG/L

July 15, 2009 July 15, 2009 Ju

RHMW02

UG/L

R

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, HDOH, 2009Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with Contaminated Soil and Groundwater, HDOH, 2009

MADEP EPHMADEP VPH

Indicates that the compound stated method detection limit

Page 1 of 1
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

15 

3.1 July 2009 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. In addition, groundwater samples from RHMW01, RHMW02, and RHMW03 were 

analyzed by the Massachusetts Department of Environmental Protection (MADEP) method for 

Extractable Petroleum Hydrocarbons (EPH) and Volatile Petroleum Hydrocarbons (VPH). 

The trip blank sample (i.e., a blank sample provided by the lab and transported with the sample 

bottles to detect the potential incursion of contaminants from outside sources) was analyzed for 

TPH-GRO, VOCs, and MADEP-VPH. The results for each groundwater monitoring well are 

discussed below. 

RHMW01

TPH-DRO at 248 μg/L, and 1-methylnaphthalene at 9.44 μg/L exceeded the HDOH Drinking 

Water EALs of 210 μg/L and 4.7 μg/L, respectively. Trace concentrations of 2-

methylnaphthalene, acenaphthene, chrysene, fluoranthene, fluorene, naphthalene, phenanthrene, 

and pyrene were detected below HDOH EALs (Table 1). All other constituents were not 

detected. 

RHMW02

TPH-DRO, 1-methylnaphthalene, 2-methylnaphthalene, acenaphthene, chrysene, fluoranthene, 

fluorene, naphthalene, phenanthrene, and pyrene were detected at RHMW02. TPH-DRO was 

detected at RHMW02 in the normal and duplicate samples, at 1,450 μg/L and 1,300 μg/L, 

respectively. This result exceeded the HDOH EAL of 210 μg/L, but not the site-specific risk 

based level (SSRBL) of 4,500 μg/L. TPH-GRO was not detected above the laboratory MDL of 

30 μg/L. 

Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. USEPA 

Method 8260B produced the highest naphthalene concentrations, which averaged 10.65 μg/L 

from the normal and duplicate sample (HDOH Drinking Water EAL is 17 μg/L). In addition, 

1-methylnaphthalene and 2-methylnapthalene were detected by USEPA Method 8270C SIM in 

the normal and duplicate samples. The average result for 1-methylnaphthalene was 11.9 μg/L, 

exceeding the HDOH toxicity EAL of 4.7 μg/L. The average result for 2-methylnaphthalene 

was 3.12 μg/L, less than the HDOH Drinking Water EAL of 24 μg/L. All other petroleum 

constituents, including trace concentrations of acenaphthene, chrysene, fluoranthene, fluorene, 

naphthalene, phenanthrene, and pyrene were well below HDOH Drinking Water EALs at 

RHMW02 (Table 1). 

Regarding MADEP analyses, RHMW02 was the only sample location that had EPH and VPH 

chemicals of concern above the laboratory MDL. At RHMW02, the average of the normal and 

duplicate samples for EPH C11 - C22 aromatics was 275 μg/L. For EPH C9 - C18 aliphatics, at 

RHMW02 the average of the normal and duplicate samples was 270 μg/L. The average 

concentration of the normal and duplicate samples at RHMW02 for total EPH was 545 μg/L 

(Table 2). 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

16 

Also at RHMW02, VPH C9 - C10 aromatics averaged a concentration of 455 μg/L. Total VPH 

was also detected at RHMW02 with an average concentration of 455 μg/L at RHMW02. A 

separate memorandum that discusses these EPH and VPH results relative to the companion TPHDRO and TPH-GRO will be issued (Table 2). 

RHMW03

No parameters were detected above the laboratory MDLs at RHMW03 (Table 1). 

RHMW05

TPH-DRO was detected at a concentration of 491 μg/L. This concentration exceeds the HDOH 

Drinking Water EAL of 210 μg/L and the HDOH Groundwater Gross Contamination EAL of 

100 μg/L. All other parameters were not detected (Table 1). 

US Navy Well 2254-01

No parameters were detected above the laboratory MDLs at the US Navy Well 2254-01 (Table 

1). 

3.2 Groundwater Contaminant Trend 

Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 2 

shows TPH trends in groundwater at the Facility. Figure 3 shows PAH trends in groundwater at 

the Facility. In these figures, open icons (without data) represent locations where the compounds 

being analyzed were not detected. 

The following is a discussion of compounds that exceeded HDOH Drinking Water EALs during 

two or more recent consecutive sampling events, thus establishing a trend: 

 

RHMW01

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005, but less than 25 percent of the SSRBL of 4,500 g/L. In July 2009, 

the result of 248 μg/L TPH-DRO was lower in concentration than any previous round since 

September 2005. TPH-DRO at RHMW01 is exhibiting a decreasing trend. 

RHMW02

At RHMW02, from September 2005 through February 2009, TPH-DRO exceeded the HDOH 

Drinking Water EAL and was greater than 50 percent of the SSRBL (estimated solubility limit of 

4,500 g/L). Specifically, the concentration of TPH-DRO was relatively stable at RHMW02 

until July 2008, ranging from 2,250 to 2,995 μg/L. However, during the July and October 2008 

sampling events, these average concentrations increased. The July 2008 average concentration 

was 4,055 μg/L and the October 2008 average concentration was 5,420 μg/L. Both of these 

values were significantly above the HDOH Drinking Water EAL of 210 μg/L, with the October 

2008 average also exceeding the SSRBL of 4,500 μg/L. 

However, TPH-DRO at RHMW02 has shown a decreasing trend since October 2008. Most 

recently, the May 2009 average TPH-DRO concentration (i.e., 1,810 g/L) and the July 2009 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

17 

TPH-DRO average concentration (i.e., 1,375 μg/L) exceeded the HDOH Drinking Water EAL, 

but were below 50 percent of the SSRBL of 4,500 μg/L. 

The July 2009 average TPH-DRO concentration represents the lowest concentration observed at 

RHMW02 since September 2005. TPH-DRO concentrations have significantly decreased over 

the last three sampling events (i.e., February, May, and July 2009). 

For other parameters, although the 1-methylnaphthalene average concentration (i.e., 11.9 g/L) 

exceeded the HDOH Drinking Water EAL of 4.7 g/L, there is a decreasing trend associated 

with 1-methylnaphthalene. The average concentrations of 1-methylnaphthalene observed during 

the October 2008, February 2009, May 2009, and July 2009 sampling events has respectively 

been 67.25 g/L, 22 g/L, 21.25 g/L, and 11.9 g/L. 

RHMW03

At RHMW03, historically, concentrations of TPH-DRO have fluctuated around the HDOH 

Drinking Water EAL, but have been significantly lower than corresponding values observed at 

RHMW01 and RHMW02. However, during the last two sampling events (i.e., May and July 

2009), TPH-DRO was not detected above the MDL. These results represent a continuing 

decreasing trend for TPH-DRO that has existed since October 2008. 

RHMW05

At RHMW05 there is an increasing trend for TPH-DRO. The July concentration of TPH-DRO 

of 491 μg/L exhibited an increase as compared with the May 2009 concentration of 200 μg/L, the 

first sampling event for RHMW05. However, the July 2009 concentration is less than 25 percent of 

the SSRBL for TPH-DRO. 

US Navy Well 2254-01

At US Navy Well 2254-01, trace concentrations of TPH-GRO and 2-methylnaphthalene that 

were observed in the February and May 2009 sampling events were not observed in July 2009. 

In addition, all other parameters were not detected as well. 

3.3 Results of Oil/Water Interface Measurements 

The presence and thickness of light-non aqueous phased liquids (LNAPL), otherwise known as 

free product, released from the USTs is monitored at the Facility (see Table 3). Static water 

levels and fuel thickness is measured to a precision of ± 0.01 feet. 

In January 2008, fuel was measured in monitoring wells RHMW01 and RHMW02 at a thickness 

of < 0.01 ft, but has not been observed in other monitoring wells. Measurements to determine 

the presence and thickness of fuel were conducted at RHMW01, RHMW02, RHMW03, and 

RHMW05 prior to the July 2009 sampling round. On August 21, a subsequent round of 

oil/water interface measurements was conducted. During the last two rounds of measurements, 

no free product was observed in any of these wells. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

18 

Table 3. Oil/Water Interface Measurements 

            

Date 

RHMW01 RHMW02 RHMW03 RHMW05 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

 January 2008 17.74 < 0.01 18.78 < 0.01 NT1 NT1 ---- ---- 

 July 2008 19.04 0.00 18.91 0.00 18.86 0.00 ---- ---- 

October 2008 18.61 0.00 18.56 0.00 18.82 0.00 ---- ---- 

November 2008 18.50 0.00 18.45 0.00 18.51 0.00 ---- ---- 

January 2009 19.28 0.00 19.22 0.00 19.27 0.00 ---- ---- 

February 2009 NT2 NT2 18.66 0.00 18.75 0.00 ---- ---- 

March 2009 18.59 0.00 18.57 0.00 18.67 0.00 ---- ---- 

May 20093 18.69 0.00 18.64 0.00 18.72 0.00 NT5 NT5

May 2009 18.91 0.00 18.86 0.00 18.90 0.00 NT5 NT5

July 20094 18.66 0.00 18.59 0.00 18.64 0.00 17.91 0.00 

August 2009 18.37 0.00 18.30 0.00 18.47 0.00 17.49 0.00 

SWL - Static water level, elevation above mean sea level (for RHMW05 this is estimated until the top well casing elevation has been determined) 

LNAPL - Light Non-Aqueous Phased Liquid, fuel product on groundwater attributed to the Facility 

ft - Feet 

NT - Not Taken 1

 - The January 2008 measurement at RHMW03 was not taken due to equipment malfunction 2 - During the February 2009 measurements, RHMW01 was inaccessible due to extensive work being conducted at Tank 02 3

 - The measurements scheduled for April 2009 were postponed until May 6, 2009 due to RHMW05 drilling activities 4

 – The June 2009 measurements were skipped due to the installation of dedicated oil/water interface probes 5 - Oil/water interface measurements were not taken at RHMW05 until the installation of the oil/water interface probe was completed 

---- - Time period prior to the installation of RHMW05 

Oil/water interface measurements were not taken during in April 2008 

3.4 Groundwater Status 

Constituents of concern are defined as petroleum-related chemicals that have been observed in 

the groundwater samples above the HDOH EALs. In accordance with the Red Hill Bulk Fuel 

Storage Facility Final Groundwater Protection Plan (TEC, 2008), Table 4 defines the 

constituents of concern in groundwater at the Facility and the SSRBLs and updated EALs for 

each (HDOH 2008). 

Table 4. Action Levels for Constituents of Concern 

Chemical EAL (μg/L) SSRBL (μg/L) 

Petroleum Mixtures 

TPH-DRO 210 4,500 

TPH-GRO 100 4,500 

Semi-Volatile Compounds 

1-Methylnaphthalene 4.7 NA 

2-Methylnaphthalene 24 NA 

Naphthalene 17 NA 

NA – Not applicable or not determined 

SSRBLs are applicable at RHMW01, RHMW02, RHMW03, and RHMW05 

EALs are applicable at US Navy Well 2254-01 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

19 

In addition, the Plan defines four results categories of groundwater status for the Facility, based 

on concentrations of constituents of concern in RHMW01, RHMW02, RHMW03 and the US 

Navy Well 2254-01, and requires specific responses when these categories are observed during 

quarterly groundwater sampling. Table 5 describes each of the four results categories and 

identifies response actions to be taken in accordance with the Plan. 

 Table 5. Results Categories and Response Actions to Changes in Groundwater Status 

Results Category RHMW02 

RHMW03 or 

RHMW05* 

RHMW01 US Navy Pumping 

Well 2254-01 

Results Category 1: Result above 

detection limit but below drinking 

water EAL and trend for all 

compounds stable or decreasing 

A A A,D,M,E 

Results Category 2: Trend for any 

compound increasing or drinking 

water EAL exceeded 

A, B A, B A,B,C,D,E,F,G,K, 

L,O 

Results Category 3: Result 

Between 1/10X SSRBL and 

SSRBL for benzene, or between 

1/2X SSRBL and SSRBL for TPH 

A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J,

K,L,O 

Results Category 4: Result 

Exceeding any SSRBL or 

petroleum product observed 

A,C,D,E,F,I,J, 

K,M,N 

A,C,D,E,F,I, 

J,K,M,N,O 

A,C,D,E,F,G,I,J,K,

L,O 

*RHMW05 was installed in April 2009 and has been subsequently been added to this Table. 

Specific Responses: 

A. Send quarterly reports to HDOH 

B. Begin program to determine the source of leak 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report (see box below) to HDOH 

F. Send Type 2 Report (see box below) to HDOH 

G. Increase monitoring frequency to once per month (if concentrations increasing) 

H. Notify HDOH verbally within 7 days and follow with written notification in 30 days 

I. Remove sampling pumps, measure product in pertinent wells with interface probe, re-install 

pumps if product is not detected. 

J. Immediately determine leaking tank 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01 

L. Provide alternative water source at 2254-01 

M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

O. Install additional monitoring well downgradient 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

20 

Report Types 

HDOH Type 1 Report 

 Re-evaluate Tier 3 Risk Assessment/groundwater model results 

 Proposal to HDOH on a course of action 

HDOH Type 2 Report 

 Proposal for groundwater treatment 

Free Product Measurements

In response to the previous Category 3 status at RHMW02, free product measurements have 

been collected at the Facility monitoring wells (Table 3). To date, there is no trend (i.e., two or 

more consecutive events) of fuel presence on groundwater at any of these wells. 

US Navy Well 2254-01(measured at RHMW2254-01)

Based upon the July 2009 sampling event, the US Navy Well 2254-01 has been removed from 

the provisional category 1 status since no compounds were detected above the laboratory MDLs. 

RHMW03

RHMW03 is no longer in Category 1 status because no compounds were detected above the 

laboratory MDL. 

Category 1 Status Locations

There are no Category 1 status locations. 

Category 2 Status Locations

RHMW01 

The July 2009 sampling event indicates that RHMW01 should remain in Category 2 status. This 

is because the TPH-DRO concentration of 248 g/L is greater than the HDOH Drinking Water 

EAL (210 g/L), but less than half the SSRBL of 4,500 g/L (estimated solubility limit of JP-5) 

and the 1-methylnaphthalene concentration (i.e., 9.44 g/L) exceeded the HDOH Drinking 

Water EAL of 4.7 g/L. 

RHMW02 

The July 2009 sampling event results in RHMW02 remaining in Category 2 status since TPHDRO [1,450 g/L and 1,300 g/L (duplicate)] is greater than the HDOH Drinking Water EAL 

(210 g/L), but is less than half the established SSRBL value of 4,500 g/L and the 1-

methylnaphthalene average concentration (i.e., 11.9 μg/L) exceeded the HDOH Drinking Water 

EAL of 4.7 g/L. 

RHMW05

Based upon the July 2009 sampling event, the second event for this newly installed well, 

RHMW05 now holds a Category 2 status. TPH-DRO at RHMW05 (i.e., 491μg/L) is above the 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

21 

drinking water EAL of 210 μg/L and has been showing an increasing trend over the last two 

rounds (i.e., 200 μg/L in May 2009 and 491μg/L in July 2009). 

 

Category 2 for RHMW01, RHMW02, and RHMW05 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 or 4 Status Locations

There are no Category 3 or 4 status locations. 

4.0 Summary and Conclusions 

Summary

There is no indication of an immediate threat of disruption to drinking water resources of the US 

Navy Well 2254-01 as a result in the July 2009 data. As a result of the July 2009 sampling event, 

the US Navy Well 2254-01 has been removed from the provisional Category 1 status that was 

established following the May 2009 sampling event. 

With the exception of RHMW05, compound concentrations for all other Facility monitoring 

wells (i.e., RHMW01, -02, -03, and RHMW2254-01) are exhibiting decreasing contaminant 

trends and thus have improved in groundwater quality relative to recent sampling events. In fact, 

the July 2009 event has resulted in RHMW03 being removed from Category 1 status. Currently, 

RHMW01, RHMW02, and RHMW05 are the only Facility wells with a Category status (i.e., 

Category 2 status). 

Conclusions/Recommendations

 To date, there is no trend (i.e., two or more consecutive events) of fuel presence on 

groundwater at the Facility wells (Table 3). In fact, fuel on the groundwater has been 

observed only once (i.e., in January 2008 in RHMW01 and RHMW02 at < 0.01 ft.). It is 

recommended that the Facility continue regular monitoring of Facility wells for the 

presence of fuel on groundwater. 

 The concentration of TPH-DRO measured at the new monitoring well, RHMW05, in July 

2009 (i.e., 491 g/L) exceeded the HDOH Drinking Water EAL, but was less than half of 

the SSRBL. RHMW05 is located between RHMW01 and the US Navy Well 2254-01. It 

is recommended that future quarterly analytical results be closely assessed at RHMW05 

since this is currently the only well exhibiting an increasing contaminant trend (i.e., 200 

μg/L in May 2009 and 491μg/L in July 2009 for TPH-DRO). 

 RHMW01, -02, -03, and RHMW2254-01 are exhibiting decreasing contaminant trends 

and thus have improved in groundwater quality relative to recent sampling events. It is 

recommended that quarterly monitoring of the Facility wells continue so that overall 

groundwater quality trends may be established/observed and proactive action taken if the 

groundwater quality begins to show evidence of deterioration. 

 The US Navy Well 2254-01 is not imminently threatened at this time; however, 

monitoring should continue to evaluate the extent of contaminant migration from upgradient locations. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

22 

 The following activities are planned to monitor and/or clarify the groundwater 

contamination situation at the Facility: 

1. Re-evaluate risk assessment and groundwater model (TEC, 2007) to ensure both 

are valid and protective of human health and the environment under the existing 

conditions; 

2. Continue monthly free product measurements at RHMW01, RHMW02, and 

RHMW03, and RHMW05; 

3. Collect samples from nearby Halawa Deep Monitoring Well (2253-03), OWDF 

MW01, and RHMW04 to assess regional groundwater trends; 

4. Prepare for alternative water source at US Navy Well 2254-01, if appropriate. 

5. Continue quarterly groundwater monitoring of Facility wells for TPH-DRO, TPHGRO, VOCs, PAHs, and lead until such time that new data indicates that a 

different monitoring program is warranted. 
Figure 

TPH Trends in Groundwater

Round 16 (July 15, 2009)

Red Hill Fuel Storage Facility

Oahu, Hawaii

The HDOH toxicity EALs were updated in Fall, 2008. •TPH-DRO Residential Tap Water EAL is 210 ug/L; and •TPH-GRO Residential Tap Water EAL is 100 ug/L;

(HDOH, 2008).
Figure 

PAH Trends in Groundwater

Round 16 (July 15, 2009)

Red Hill Fuel Storage Facility

Oahu, Hawaii

The HDOH toxicity EALs were updated in Fall, 2008. 

• Naphthalene Residential Tap Water EAL is 17 ug/L;

• 1-methylnaphthalene Residential Tap Water EAL is 4.7 ug/L; and

• 2- methylnaphthalene Residential Tap Water EAL is 24 ug/L

(HDOH, 2008).
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility September 2009 

 ____________________________________________________________________________________________ 

25 

5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

Massachusetts Department of Environmental Protection (MADEP). Implementation of the 

MADEP VPH/EPH Approach. Final Policy, October 2002 

The Environmental Company, Inc. and AMEC. Red Hill Bulk Fuel Storage Facility Work Plan, 

Pearl Harbor, Hawaii. June 2005. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, Hawaii. 

August 2007. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

Red Hill BFSF

The Environmental Company, Inc. (TEC)

1093515

1 of 87
Case Narrative

THEENVC The Environmental Company, Inc. (TEC)

1093515 Red Hill BFSF

Customer:

Project:

NPDL WO:

SGS North America Inc.

Refer to the sample receipt form for information on sample condition.

1093515004 PS RHMW05-WG16

8015C - DRO - Unknown hydrocarbon with several peaks is present.

1093515007 PS RHMW02-WG16

8015C - DRO - The pattern is consistent with a weathered middle distillate.

1093515008 PS RHMWA01-WG16

8015C - DRO - The pattern is consistent with a weathered middle distillate.

1093515002 BMS RHMW2254-WG16 MS

8015C - GRO - BMS recovery does not meet QC criteria (biased high). Refer to LCS for accuraccy.

2 of 87
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1093515

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street, Suite 1400

Honolulu, HI 96813

Attn: Rick Adkisson

T: (808)528-1445 F:(808)528-0768

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

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Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343. All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm) 

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike (Duplicate)

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 8/3/2009

Notes: All DRO/RRO analyses are integrated per SOP.

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SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: Red Hill BFSF

Workorder No.: 1093515

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015B (W) SW8015C

GRO (W) SW8015C

Print Date: 8/3/2009 4:39 pm

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1093515001 RHMW2254-WG16

1093515002 RHMW2254-WG16 MS

1093515003 RHMW2254-WG16 MSD

1093515004 RHMW05-WG16

1093515005 RHMW01-WG16

1093515006 RHMW03-WG16

1093515007 RHMW02-WG16

1093515008 RHMWA01-WG16

1093515009 TB01-WG16

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The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW2254-WG16

SGS Ref. #: 1093515001 Collection Date/Time: 07/15/09 09:00

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5997 MXX21958

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5997

Analytical Method: SW6020

Analysis Date/Time: 07/28/09 13:41

Prep Batch: MXX21958

Prep Method: SW3010A

Prep Date/Time: 07/27/09 19:20 Container ID:1093515001-G

Dilution Factor: 5 Analyst: NRB

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The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW2254-WG16

SGS Ref. #: 1093515001 Collection Date/Time: 07/15/09 09:00

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9556 VXX19707

4-Bromofluorobenzene <surr> 91.2 50-150 % 1 VFC9556 VXX19707

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9556

Analytical Method: SW8015C

Analysis Date/Time: 07/23/09 12:25

Prep Batch: VXX19707

Prep Method: SW5030B

Prep Date/Time: 07/23/09 08:25 Container ID:1093515001-A

Dilution Factor: 1 Analyst: KPW

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The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW2254-WG16

SGS Ref. #: 1093515001 Collection Date/Time: 07/15/09 09:00

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.435 0.163 mg/L 1 XFC8727 XXX21224

5a Androstane <surr> 93.1 50-150 % 1 XFC8727 XXX21224

Batch Information

Initial Prep Wt./Vol.: 920 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8727

Analytical Method: SW8015C

Analysis Date/Time: 07/30/09 02:25

Prep Batch: XXX21224

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:15 Container ID:1093515001-H

Dilution Factor: 1 Analyst: KDC

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The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW2254-WG16

SGS Ref. #: 1093515001 Collection Date/Time: 07/15/09 09:00

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

Toluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Styrene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Acetone ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10654 VXX19686

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

Chloroform ND 1.00 0.300 ug/L 1 VMS10654 VXX19686

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromomethane ND 3.00 0.940 ug/L 1 VMS10654 VXX19686

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

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The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW2254-WG16

SGS Ref. #: 1093515001 Collection Date/Time: 07/15/09 09:00

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10654 VXX19686

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Naphthalene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

o-Xylene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromoform ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane-D4 <surr> 108 73-120 % 1 VMS10654 VXX19686

Toluene-d8 <surr> 99 80-120 % 1 VMS10654 VXX19686

4-Bromofluorobenzene <surr> 104 76-120 % 1 VMS10654 VXX19686

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10654

Analytical Method: SW8260B

Analysis Date/Time: 07/20/09 18:57

Prep Batch: VXX19686

Prep Method: SW5030B

Prep Date/Time: 07/20/09 12:19 Container ID:1093515001-D

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

10 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW2254-WG16

SGS Ref. #: 1093515001 Collection Date/Time: 07/15/09 09:00

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Acenaphthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Fluorene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Phenanthrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo(a)Anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Chrysene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[b]Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[k]fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[a]pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Indeno[1,2,3-c,d] pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Dibenzo[a,h]anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[g,h,i]perylene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Naphthalene ND 0.110 0.0341 ug/L 1 XMS4994 XXX21226

1-Methylnaphthalene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

2-Methylnaphthalene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Terphenyl-d14 <surr> 96.7 50-135 % 1 XMS4994 XXX21226

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4994

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 04:48

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515001-J

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

11 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW05-WG16

SGS Ref. #: 1093515004 Collection Date/Time: 07/15/09 07:35

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5997 MXX21958

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5997

Analytical Method: SW6020

Analysis Date/Time: 07/28/09 14:07

Prep Batch: MXX21958

Prep Method: SW3010A

Prep Date/Time: 07/27/09 19:20 Container ID:1093515004-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

12 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW05-WG16

SGS Ref. #: 1093515004 Collection Date/Time: 07/15/09 07:35

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9556 VXX19707

4-Bromofluorobenzene <surr> 99.8 50-150 % 1 VFC9556 VXX19707

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9556

Analytical Method: SW8015C

Analysis Date/Time: 07/23/09 10:50

Prep Batch: VXX19707

Prep Method: SW5030B

Prep Date/Time: 07/23/09 08:25 Container ID:1093515004-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

13 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW05-WG16

SGS Ref. #: 1093515004 Collection Date/Time: 07/15/09 07:35

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.491 0.421 0.158 mg/L 1 XFC8727 XXX21224

5a Androstane <surr> 83.1 50-150 % 1 XFC8727 XXX21224

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8727

Analytical Method: SW8015C

Analysis Date/Time: 07/30/09 02:52

Prep Batch: XXX21224

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:15 Container ID:1093515004-H

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

14 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW05-WG16

SGS Ref. #: 1093515004 Collection Date/Time: 07/15/09 07:35

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

Toluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Styrene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Acetone 65.0 10.0 3.10 ug/L 1 VMS10654 VXX19686

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10654 VXX19686

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

Chloroform ND 1.00 0.300 ug/L 1 VMS10654 VXX19686

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromomethane ND 3.00 0.940 ug/L 1 VMS10654 VXX19686

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

15 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW05-WG16

SGS Ref. #: 1093515004 Collection Date/Time: 07/15/09 07:35

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10654 VXX19686

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Naphthalene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

o-Xylene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromoform ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane-D4 <surr> 113 73-120 % 1 VMS10654 VXX19686

Toluene-d8 <surr> 99.9 80-120 % 1 VMS10654 VXX19686

4-Bromofluorobenzene <surr> 106 76-120 % 1 VMS10654 VXX19686

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10654

Analytical Method: SW8260B

Analysis Date/Time: 07/20/09 20:36

Prep Batch: VXX19686

Prep Method: SW5030B

Prep Date/Time: 07/20/09 12:19 Container ID:1093515004-D

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

16 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW05-WG16

SGS Ref. #: 1093515004 Collection Date/Time: 07/15/09 07:35

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Acenaphthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Fluorene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Phenanthrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo(a)Anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Chrysene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[b]Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[k]fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[a]pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Indeno[1,2,3-c,d] pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Dibenzo[a,h]anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[g,h,i]perylene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Naphthalene ND 0.110 0.0341 ug/L 1 XMS4994 XXX21226

1-Methylnaphthalene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

2-Methylnaphthalene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Terphenyl-d14 <surr> 83.7 50-135 % 1 XMS4994 XXX21226

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4994

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 09:02

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515004-J

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

17 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW01-WG16

SGS Ref. #: 1093515005 Collection Date/Time: 07/15/09 15:15

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5997 MXX21958

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5997

Analytical Method: SW6020

Analysis Date/Time: 07/28/09 14:09

Prep Batch: MXX21958

Prep Method: SW3010A

Prep Date/Time: 07/27/09 19:20 Container ID:1093515005-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

18 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW01-WG16

SGS Ref. #: 1093515005 Collection Date/Time: 07/15/09 15:15

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9556 VXX19707

4-Bromofluorobenzene <surr> 95.8 50-150 % 1 VFC9556 VXX19707

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9556

Analytical Method: SW8015C

Analysis Date/Time: 07/23/09 11:09

Prep Batch: VXX19707

Prep Method: SW5030B

Prep Date/Time: 07/23/09 08:25 Container ID:1093515005-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

19 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW01-WG16

SGS Ref. #: 1093515005 Collection Date/Time: 07/15/09 15:15

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.248 J 0.430 0.161 mg/L 1 XFC8727 XXX21224

5a Androstane <surr> 82.6 50-150 % 1 XFC8727 XXX21224

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8727

Analytical Method: SW8015C

Analysis Date/Time: 07/30/09 03:20

Prep Batch: XXX21224

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:15 Container ID:1093515005-H

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

20 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW01-WG16

SGS Ref. #: 1093515005 Collection Date/Time: 07/15/09 15:15

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

Toluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Styrene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Acetone ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10654 VXX19686

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

Chloroform ND 1.00 0.300 ug/L 1 VMS10654 VXX19686

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromomethane ND 3.00 0.940 ug/L 1 VMS10654 VXX19686

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

21 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW01-WG16

SGS Ref. #: 1093515005 Collection Date/Time: 07/15/09 15:15

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10654 VXX19686

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Naphthalene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

o-Xylene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromoform ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane-D4 <surr> 111 73-120 % 1 VMS10654 VXX19686

Toluene-d8 <surr> 98.9 80-120 % 1 VMS10654 VXX19686

4-Bromofluorobenzene <surr> 106 76-120 % 1 VMS10654 VXX19686

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10654

Analytical Method: SW8260B

Analysis Date/Time: 07/20/09 21:07

Prep Batch: VXX19686

Prep Method: SW5030B

Prep Date/Time: 07/20/09 12:19 Container ID:1093515005-D

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

22 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW01-WG16

SGS Ref. #: 1093515005 Collection Date/Time: 07/15/09 15:15

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Acenaphthene 0.180 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Fluorene 0.0952 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Phenanthrene 0.0349 J 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Anthracene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Fluoranthene 0.0263 J 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Pyrene 0.0270 J 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo(a)Anthracene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Chrysene 0.0159 J 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[b]Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[k]fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[a]pyrene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Indeno[1,2,3-c,d] pyrene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Dibenzo[a,h]anthracene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[g,h,i]perylene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Naphthalene 5.61 1.05 0.326 ug/L 10 XMS4996 XXX21226

1-Methylnaphthalene 9.44 0.526 0.158 ug/L 10 XMS4996 XXX21226

2-Methylnaphthalene 3.07 0.526 0.158 ug/L 10 XMS4996 XXX21226

Terphenyl-d14 <surr> 84.1 50-135 % 1 XMS4994 XXX21226

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4994

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 09:36

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515005-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4996

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 18:29

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515005-J

Dilution Factor: 10 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

23 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW03-WG16

SGS Ref. #: 1093515006 Collection Date/Time: 07/15/09 10:55

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5997 MXX21958

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5997

Analytical Method: SW6020

Analysis Date/Time: 07/28/09 14:11

Prep Batch: MXX21958

Prep Method: SW3010A

Prep Date/Time: 07/27/09 19:20 Container ID:1093515006-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

24 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW03-WG16

SGS Ref. #: 1093515006 Collection Date/Time: 07/15/09 10:55

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9556 VXX19707

4-Bromofluorobenzene <surr> 97.2 50-150 % 1 VFC9556 VXX19707

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9556

Analytical Method: SW8015C

Analysis Date/Time: 07/23/09 11:27

Prep Batch: VXX19707

Prep Method: SW5030B

Prep Date/Time: 07/23/09 08:25 Container ID:1093515006-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

25 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW03-WG16

SGS Ref. #: 1093515006 Collection Date/Time: 07/15/09 10:55

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.400 0.150 mg/L 1 XFC8727 XXX21224

5a Androstane <surr> 88.3 50-150 % 1 XFC8727 XXX21224

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8727

Analytical Method: SW8015C

Analysis Date/Time: 07/30/09 03:30

Prep Batch: XXX21224

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:15 Container ID:1093515006-H

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

26 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW03-WG16

SGS Ref. #: 1093515006 Collection Date/Time: 07/15/09 10:55

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

Toluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Styrene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Acetone ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10654 VXX19686

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

Chloroform ND 1.00 0.300 ug/L 1 VMS10654 VXX19686

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromomethane ND 3.00 0.940 ug/L 1 VMS10654 VXX19686

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

27 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW03-WG16

SGS Ref. #: 1093515006 Collection Date/Time: 07/15/09 10:55

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10654 VXX19686

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Naphthalene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

o-Xylene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromoform ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane-D4 <surr> 115 73-120 % 1 VMS10654 VXX19686

Toluene-d8 <surr> 99.9 80-120 % 1 VMS10654 VXX19686

4-Bromofluorobenzene <surr> 106 76-120 % 1 VMS10654 VXX19686

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10654

Analytical Method: SW8260B

Analysis Date/Time: 07/20/09 21:38

Prep Batch: VXX19686

Prep Method: SW5030B

Prep Date/Time: 07/20/09 12:19 Container ID:1093515006-D

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

28 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW03-WG16

SGS Ref. #: 1093515006 Collection Date/Time: 07/15/09 10:55

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Acenaphthene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Fluorene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Phenanthrene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Anthracene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Pyrene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo(a)Anthracene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Chrysene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[b]Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[k]fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[a]pyrene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Indeno[1,2,3-c,d] pyrene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Dibenzo[a,h]anthracene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Benzo[g,h,i]perylene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Naphthalene ND 0.105 0.0326 ug/L 1 XMS4994 XXX21226

1-Methylnaphthalene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

2-Methylnaphthalene ND 0.0526 0.0158 ug/L 1 XMS4994 XXX21226

Terphenyl-d14 <surr> 97.1 50-135 % 1 XMS4994 XXX21226

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4994

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 10:09

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515006-J

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

29 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW02-WG16

SGS Ref. #: 1093515007 Collection Date/Time: 07/15/09 13:20

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5997 MXX21958

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5997

Analytical Method: SW6020

Analysis Date/Time: 07/28/09 14:13

Prep Batch: MXX21958

Prep Method: SW3010A

Prep Date/Time: 07/27/09 19:20 Container ID:1093515007-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

30 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW02-WG16

SGS Ref. #: 1093515007 Collection Date/Time: 07/15/09 13:20

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9556 VXX19707

4-Bromofluorobenzene <surr> 96.8 50-150 % 1 VFC9556 VXX19707

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9556

Analytical Method: SW8015C

Analysis Date/Time: 07/23/09 11:46

Prep Batch: VXX19707

Prep Method: SW5030B

Prep Date/Time: 07/23/09 08:25 Container ID:1093515007-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

31 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW02-WG16

SGS Ref. #: 1093515007 Collection Date/Time: 07/15/09 13:20

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 1.45 0.400 0.150 mg/L 1 XFC8727 XXX21224

5a Androstane <surr> 78.9 50-150 % 1 XFC8727 XXX21224

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8727

Analytical Method: SW8015C

Analysis Date/Time: 07/30/09 03:39

Prep Batch: XXX21224

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:15 Container ID:1093515007-H

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

32 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW02-WG16

SGS Ref. #: 1093515007 Collection Date/Time: 07/15/09 13:20

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

Toluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

n-Butylbenzene 1.51 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

n-Propylbenzene 2.49 1.00 0.310 ug/L 1 VMS10654 VXX19686

Styrene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Acetone ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10654 VXX19686

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

Chloroform ND 1.00 0.300 ug/L 1 VMS10654 VXX19686

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromomethane ND 3.00 0.940 ug/L 1 VMS10654 VXX19686

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

33 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW02-WG16

SGS Ref. #: 1093515007 Collection Date/Time: 07/15/09 13:20

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

sec-Butylbenzene 3.48 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10654 VXX19686

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Naphthalene 10.1 2.00 0.620 ug/L 1 VMS10654 VXX19686

o-Xylene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromoform ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

tert-Butylbenzene 0.610 J 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Isopropylbenzene (Cumene) 2.58 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane-D4 <surr> 115 73-120 % 1 VMS10654 VXX19686

Toluene-d8 <surr> 99.5 80-120 % 1 VMS10654 VXX19686

4-Bromofluorobenzene <surr> 107 76-120 % 1 VMS10654 VXX19686

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10654

Analytical Method: SW8260B

Analysis Date/Time: 07/20/09 22:09

Prep Batch: VXX19686

Prep Method: SW5030B

Prep Date/Time: 07/20/09 12:19 Container ID:1093515007-D

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

34 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMW02-WG16

SGS Ref. #: 1093515007 Collection Date/Time: 07/15/09 13:20

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Acenaphthene 0.235 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Fluorene 0.115 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Phenanthrene 0.0304 J 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Anthracene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Fluoranthene 0.0247 J 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Pyrene 0.0272 J 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Benzo(a)Anthracene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Chrysene 0.0162 J 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Benzo[b]Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Benzo[k]fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Benzo[a]pyrene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Indeno[1,2,3-c,d] pyrene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Dibenzo[a,h]anthracene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Benzo[g,h,i]perylene ND 0.0521 0.0156 ug/L 1 XMS4994 XXX21226

Naphthalene 8.37 1.04 0.323 ug/L 10 XMS4996 XXX21226

1-Methylnaphthalene 13.2 0.521 0.156 ug/L 10 XMS4996 XXX21226

2-Methylnaphthalene 3.66 0.521 0.156 ug/L 10 XMS4996 XXX21226

Terphenyl-d14 <surr> 84.9 50-135 % 1 XMS4994 XXX21226

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4994

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 10:43

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515007-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4996

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 19:03

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515007-J

Dilution Factor: 10 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

35 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMWA01-WG16

SGS Ref. #: 1093515008 Collection Date/Time: 07/15/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5997 MXX21958

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5997

Analytical Method: SW6020

Analysis Date/Time: 07/28/09 14:15

Prep Batch: MXX21958

Prep Method: SW3010A

Prep Date/Time: 07/27/09 19:20 Container ID:1093515008-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

36 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMWA01-WG16

SGS Ref. #: 1093515008 Collection Date/Time: 07/15/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9556 VXX19707

4-Bromofluorobenzene <surr> 103 50-150 % 1 VFC9556 VXX19707

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9556

Analytical Method: SW8015C

Analysis Date/Time: 07/23/09 12:05

Prep Batch: VXX19707

Prep Method: SW5030B

Prep Date/Time: 07/23/09 08:25 Container ID:1093515008-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

37 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMWA01-WG16

SGS Ref. #: 1093515008 Collection Date/Time: 07/15/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 1.30 0.400 0.150 mg/L 1 XFC8727 XXX21224

5a Androstane <surr> 76.5 50-150 % 1 XFC8727 XXX21224

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8727

Analytical Method: SW8015C

Analysis Date/Time: 07/30/09 03:48

Prep Batch: XXX21224

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:15 Container ID:1093515008-H

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

38 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMWA01-WG16

SGS Ref. #: 1093515008 Collection Date/Time: 07/15/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

Toluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

n-Butylbenzene 1.59 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

n-Propylbenzene 2.33 1.00 0.310 ug/L 1 VMS10654 VXX19686

Styrene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Acetone ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10654 VXX19686

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10654 VXX19686

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

Chloroform ND 1.00 0.300 ug/L 1 VMS10654 VXX19686

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Chloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromomethane ND 3.00 0.940 ug/L 1 VMS10654 VXX19686

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

39 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMWA01-WG16

SGS Ref. #: 1093515008 Collection Date/Time: 07/15/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

sec-Butylbenzene 3.23 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10654 VXX19686

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10654 VXX19686

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10654 VXX19686

Naphthalene 11.2 2.00 0.620 ug/L 1 VMS10654 VXX19686

o-Xylene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Bromoform ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

tert-Butylbenzene 0.560 J 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

Isopropylbenzene (Cumene) 2.36 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10654 VXX19686

1,2-Dichloroethane-D4 <surr> 111 73-120 % 1 VMS10654 VXX19686

Toluene-d8 <surr> 99.8 80-120 % 1 VMS10654 VXX19686

4-Bromofluorobenzene <surr> 105 76-120 % 1 VMS10654 VXX19686

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10654

Analytical Method: SW8260B

Analysis Date/Time: 07/20/09 22:40

Prep Batch: VXX19686

Prep Method: SW5030B

Prep Date/Time: 07/20/09 12:19 Container ID:1093515008-D

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

40 of 87
The Environmental Company, Inc. (TEC) Print Date: 8/3/2009 4:39 pm

Client Sample ID: RHMWA01-WG16

SGS Ref. #: 1093515008 Collection Date/Time: 07/15/09 12:05

Project ID: Red Hill BFSF Receipt Date/Time: 07/17/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Acenaphthene 0.213 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Fluorene 0.108 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Phenanthrene 0.0291 J 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Fluoranthene 0.0199 J 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Pyrene 0.0189 J 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo(a)Anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Chrysene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[b]Fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[k]fluoranthene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[a]pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Indeno[1,2,3-c,d] pyrene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Dibenzo[a,h]anthracene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Benzo[g,h,i]perylene ND 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Naphthalene 6.71 1.10 0.341 ug/L 10 XMS4996 XXX21226

1-Methylnaphthalene 10.6 0.549 0.165 ug/L 10 XMS4996 XXX21226

2-Methylnaphthalene 2.58 0.0549 0.0165 ug/L 1 XMS4994 XXX21226

Terphenyl-d14 <surr> 94.2 50-135 % 1 XMS4994 XXX21226

Batch Information

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4994

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 11:17

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515008-J

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 910 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4996

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/22/09 19:36

Prep Batch: XXX21226

Prep Method: SW3520C

Prep Date/Time: 07/21/09 10:40 Container ID:1093515008-J

Dilution Factor: 10 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

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