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# S A M P L E I N F O R M A T I O N

Batch_or_Req_No N285/2 Sample Name: WB386-03 B/1083411 (P920-2) Sample Type: Date Acquired: Broad Unknown 01/12/05 16:55:09 Vial: Acq. Method Set: 5 AN054 1000A Date Processed: 02/12/05 11:12:18 Analyst JD Injection Volume: Processing Method: 40.00 ul AN054 1000A Run Time: Channel Name: 14.0 Minutes 410 Sample Set Name: Proc. Chnl. Descr.: n285 1000a AN054 1000A

Auto-Scaled ChromatogramMV

0.00 100.00 200.00 300.00 400.00 500.00

Minutes 2.00 4.00 6.00 8.00 10.00 12.00 14.0012898

1 Name MP Mw Mn Polydispersity %Poly < MWM 500 %Poly < MWM 1000 Broad 12898 12575 2556 4.919857 4.499 10.360 

### Peak Results

All reported molecular weight distributions are calculated using polystryrene standards. They will differ from absolute values depending on the structure and chemical differences between the test subtance and polystyrene.

### Printed 11:18:47 02/12/05 Page: 2 of 5 GPC Calibration PlotLog Mol Wt

1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50

Retention Time 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00

1 2 3 4 5 6 7 8 Mol Wt (Daltons) RT Calculated Weight (Daltons) 49170 19880 8450 1260 30330 12970 3370

925 6.248 6.248 6.248 6.248 6.542 6.542 6.542 6.542 44694 20331

8705 1258 30578 13676 3524

870 

### GPC Calibration Table For

Polystyrene Standards

### Printed 11:18:47 02/12/05 Page: 3 of 5 dwt/d(logM) Cumulative %dwt/d(logM)Cumulative %

0.00 0.20 0.40 0.60

0.00 20.00 40.00 60.00 80.00 100.00

Slice Log MW 2.50 3.00 3.50 4.00 4.50MP=12898Mn=2556Mw=12575Mz=26654Mz+1=37852

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 RT Mol Wt Cumulative % Outside Vo-Vt Slice MW 6.030 6.112 6.179 6.241 6.298 6.351 6.400 6.445 6.488 6.527 6.564 6.599 6.632 6.665 6.696 6.725 6.754 6.783 6.810 6.837 6.864 59134 53209 48817 45104 41883 39118 36724 34646 32814 31195 29744 28427 27230 26125 25103 24158 23273 22439 21657 20918 20215 1.000 2.000 3.000 4.000 5.000 6.000 7.000 8.000 9.000 10.000 11.000 12.000 13.000 14.000 15.000 16.000 17.000 18.000 19.000 20.000 21.000 No No No No No No No No No No No No No No No No No No No No No 59134 53209 48817 45104 41883 39118 36724 34646 32814 31195 29744 28427 27230 26125 25103 24158 23273 22439 21657 20918 20215 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 RT Mol Wt Cumulative % Outside Vo-Vt Slice MW 6.890 6.916 6.941 6.966 6.990 7.015 7.039 7.064 7.088 7.112 7.136 7.159 7.183 7.207 7.231 7.255 7.279 7.303 7.327 7.351 7.376 19547 18913 18309 17730 17174 16641 16127 15631 15153 14692 14247 13815 13396 12991 12599 12216 11844 11483 11133 10792 10459 22.000 23.000 24.000 25.000 26.000 27.000 28.000 29.000 30.000 31.000 32.000 33.000 34.000 35.000 36.000 37.000 38.000 39.000 40.000 41.000 42.000 No No No No No No No No No No No No No No No No No No No No No 19547 18913 18309 17730 17174 16641 16127 15631 15153 14692 14247 13815 13396 12991 12599 12216 11844 11483 11133 10792 10459 

### GPC Distribution Table Mp: 12898 Name: Broad

### Printed 11:18:47 02/12/05 Page: 4 of 5 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 RT Mol Wt Cumulative % Outside Vo-Vt Slice MW 7.400 7.425 7.450 7.475 7.500 7.525 7.551 7.577 7.603 7.629 7.656 7.684 7.711 7.739 7.767 7.796 7.826 7.856 7.886 7.917 7.949 7.981 8.014 8.048 8.082 8.118 8.154 8.191 8.230 8.269 8.310 8.351 8.394 8.438 8.484 8.532 10135 9819 9510 9208 8914 8627 8347 8073 7805 7543 7287 7036 6791 6551 6315 6085 5859 5638 5421 5209 5001 4797 4598 4402 4210 4023 3839 3659 3483 3310 3142 2978 2818 2662 2509 2361 43.000 44.000 45.000 46.000 47.000 48.000 49.000 50.000 51.000 52.000 53.000 54.000 55.000 56.000 57.000 58.000 59.000 60.000 61.000 62.000 63.000 64.000 65.000 66.000 67.000 68.000 69.000 70.000 71.000 72.000 73.000 74.000 75.000 76.000 77.000 78.000 No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No No 10135 9819 9510 9208 8914 8627 8347 8073 7805 7543 7287 7036 6791 6551 6315 6085 5859 5638 5421 5209 5001 4797 4598 4402 4210 4023 3839 3659 3483 3310 3142 2978 2818 2662 2509 2361 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 RT Mol Wt Cumulative % Outside Vo-Vt Slice MW 8.581 8.631 8.683 8.736 8.787 8.837 8.888 8.942 9.001 9.068 9.141 9.221 9.307 9.394 9.483 9.580 9.682 9.786 9.912 10.069 10.220 10.625 2217 2077 1942 1815 1699 1593 1492 1392 1289 1183 1077 971 870 778 693 612 536 469 399 326 269 159 79.000 80.000 81.000 82.000 83.000 84.000 85.000 86.000 87.000 88.000 89.000 90.000 91.000 92.000 93.000 94.000 95.000 96.000 97.000 98.000 99.000 100.000 No No No No No No No No No No No No No No No No No No No No No No 2217 2077 1942 1815 1699 1593 1492 1392 1289 1183 1077 971 870 778 693 612 536 469 399 326 269 159 

### GPC Distribution Table Mp: 12898 Name: Broad

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