### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

### Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

56068 Elm Road Generating Station 1 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 56068 Elm Road Generating Station 1 As Received Higher Heating Value 

### 56068 Elm Road Generating Station 1 As Received % Moisture 

### 56068 Elm Road Generating Station 1 As Received % Ash 

### 56068 Elm Road Generating Station 1 As Received % Sulfur 

### 56068 Elm Road Generating Station 1 Dry basis Higher Heating Value 

### 56068 Elm Road Generating Station 1 Dry basis % Ash 

### 56068 Elm Road Generating Station 1 Dry basis % Sulfur 

### 56068 Elm Road Generating Station 1 Dry basis Antim ony 

### 56068 Elm Road Generating Station 1 Dry basis Arsenic 

### 56068 Elm Road Generating Station 1 Dry basis Beryllium 

### 56068 Elm Road Generating Station 1 Dry basis Cadmium 

### 56068 Elm Road Generating Station 1 Dry basis Chlorine 

### 56068 Elm Road Generating Station 1 Dry basis Chromium 

### 56068 Elm Road Generating Station 1 Dry basis Cobalt 

### 56068 Elm Road Generating Station 1 Dry basis Fluorine 

### 56068 Elm Road Generating Station 1 Dry basis Lead 

### 56068 Elm Road Generating Station 1 Dry basis Manganese 

### 56068 Elm Road Generating Station 1 Dry basis Mercury 

### 56068 Elm Road Generating Station 1 Dry basis Nickel 

### 56068 Elm Road Generating Station 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 Method B ASTM D5865 ASTM D5142 ASTM D4239 ASTM D3683-94 ASTM D3683-94 ASTM D3683-94 ASTM D3683-94 EPA 5050/9056 ASTM D3683-94 ASTM D3683-94 EPA 5050/9056 ASTM D3683-94 ASTM D3683-94 EPA 7473 ASTM D3683-94 ASTM D3683-94EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 56068 Elm Road Generating Station 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) AD35023 

### 11/8/2010 11/8/2010 12723.00 Btu/lb 7.48 7.3 AD35024 

### 11/9/2010 11/9/2010 12590.00 Btu/lb 7.7 7.71 AD35025 

### 11/9/2010 11/9/2010 12771.00 Btu/lb 7.53 7.31 Fuel Testing Results% Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### 1.739376 13752 Btu/lb 7.89 2.03 1400 mg/kg 0.12 mg/kg 1.62448 13640 Btu/lb 8.36 1.9 1400 mg/Kg 0.13 mg/Kg 1.562743 13810 Btu/lb 7.91 1.83 1500 mg/Kg 0.11 mg/KgAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### 0.47 mg/kg 7.1 mg/kg 1 mg/kg 0.11 mg/kg 14 0.46 mg/Kg 9 mg/Kg 1 mg/Kg 0.11 mg/Kg 14 0.44 mg/Kg 8.4 mg/Kg 1 mg/Kg 0.12 mg/Kg 14Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### mg/kg 4.2 mg/kg 13 mg/kg 12 mg/kg 1.6 mg/kg mg/Kg 4.6 mg/Kg 16 mg/Kg 12 mg/Kg 1.6 mg/Kg mg/Kg 4.4 mg/Kg 13 mg/Kg 12 mg/Kg 1.6 mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 50 mg/kg 3.3 mg/kg 7.48 38.36 7.89 53.75 59 mg/Kg 3.6 mg/Kg 7.7 37.77 8.36 53.87 53 mg/Kg 3.2 mg/Kg 7.53 38.01 7.91 54.08 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen



### 76.32 4.97 1.53 2.03 7.26 76.25 4.93 1.67 1.9 6.89 76.89 4.87 1.6 1.83 6.9 Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 56068 Elm Road Generating Station 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) AD30520 

### 11/4/2010 11/4/2010 12769.00 Btu/lb AD30521 

### 11/4/2010 11/4/2010 12762.00 Btu/lb AD30522 

### 11/5/2010 11/5/2010 12654.00 Btu/lb Fuel Testing Results% Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### 13770 Btu/lb 1.82 1200 mg/kg mg/kg 13727 Btu/lb 1.79 1300 mg/Kg mg/Kg 13705 Btu/lb 1.76 1300 mg/Kg mg/KgAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### mg/kg mg/kg mg/kg mg/kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgChromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### mg/kg mg/kg mg/kg mg/kg mg/kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 46 mg/kg mg/kg 7.27 37.76 7.98 54.26 49 mg/Kg mg/Kg 7.03 37.8 8.28 53.98 57 mg/Kg mg/Kg 7.66 37.93 8.09 53.98 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 76.56 4.97 1.56 1.82 7.11 76.34 5 1.57 1.79 7.02 76.2 4.98 1.54 1.76 7.43

Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 56068 Elm Road Generating Station 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A

sh (as received) AD30517 

### 11/3/2010 11/3/2010 12772.00 Btu/lb AD30518 

### 11/3/2010 11/3/2010 12628.00 Btu/lb AD30519 

### 11/3/2010 11/3/2010 12649.00 Btu/lb Fuel Testing Results% Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### 13796 Btu/lb mg/kg mg/kg 13738 Btu/lb mg/Kg mg/Kg 13684 Btu/lb mg/Kg mg/KgAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### mg/kg mg/kg mg/kg mg/kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgChromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### mg/kg mg/kg mg/kg mg/kg mg/kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### mg/kg mg/kg 7.43 37.53 7.75 54.72 mg/Kg mg/Kg 8.08 37.88 7.77 54.35 mg/Kg mg/Kg 7.56 37.53 8.08 54.39 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 76.54 4.93 1.57 1.81 7.4 76.37 4.87 1.55 1.73 7.71 76.11 4.96 1.54 1.8 7.51

Ultimate Analy

ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm