P. 1



# OAR Box 1672 Prepped by Charmelle Mathews



### Document

Number: 

# >6)II-B-1 0 Docket Number: 

# A-98-1 3

Printed 9/30/200811:01:00AM

Sheet 16 of 132P. 2



### ESBJB 

# A-98-1 3

MEMORANDU

M

TO :

FROM : Project

Fil e Organi c Liquid s Distributio n NESHA P ES D Project

No
. 96/0 5 BemdHaneke <^ — Pacific Environmenta

l Services , Inc
. (PES ) DATE : Marc

h 2,199 9 SUBJECT : Sit

e Visit to Paktan k Corporation , Dee

r Park , Texa s I . Purpos e The purpos e of

thi s sit e visi t wa s to tour

th e Paktan

k facilit y in a n effor t to infor mEP A an d contractor

personnel concerning organi c liquid s distributio n (O.L.D. ) operation s andto collec t informatio n relate d t

o ai r emission s fromth e operations

. Thi s wor k i s in suppor

t ofth e developmen

t of nationa l emissio n standard s fo

r hazardou s ai

r pollutant s (NESHAP) fo

r th e organi c liquid s distributio n (non-gasoline ) sourc e category
. II . Locatio n an

d Dat e Paktan k Corporatio n Dee r Par k Termina l Sout h of Houston Shi

p Channel 275 9 Battlegroun d Roa

d Dee r Park , Texa s 7753 6 Octobe r 21,199 8 (9:00-11:3 0 am

) III . Participant

s Paktan k Corporatio n Mr
. Quirino Won

g - Manage

r of Environmenta

l Affair s Mr
. Davi d Carte

r - Environmenta

l Superviso

r Texa s Natura

l Resource s Conservatio n Commissio n (TNRCC ) Ms
. Caro l Harkin s Environmenta

l Protectio n Agency (EPA) Mr
. Stephe

n Shed d - Project Officer, OAQPS/ESD/WCPG Research Triangl e Park , N CSit e Visi t

Memo/Paktan k

Corporatio n Marc h 2,199 8 Pag e 2 Pacifi c Environmenta l Services

. Inc
. CPBS) Mr
. Greg LaFla

m- Researc h Triangl e Park , N C Mr
. Bem d Hanek e - Research Triangl e Park , N C IV
. Pre-Tou r

Discussio n Introductio n EPA Introduction Afte r th e participant s introduce dthemselves , Stev e Shedd , EPA , bega n th e meetin g b y discussin g th e background ofth e EPA' s regulatio n of hazardou s air

pollutan t (HAP ) emissions

. Prio r t o th e Clea

n Air Act Amendment s o f

1990 (CAAA) , regulation s were o n th e basi s o f individua l HA P an d alimite d numbe

r o f regulation s wer

e completed

. Th e CAA

A include d a HA P lis t and prescribe d tha

t rule s b e develope dfo

r categorie s o f

source s (industria

l types)

. Th e stringenc y ofth e Organi c Liquid s Distributio n (non-gasoline ) rul e (fo r existin g sources ) wil l b e base d o n "floor " level s o f

contro l representin g th e contro l achieve db y th e averag e ofth e to p 1 2 percent o f source s in thi s category
. Th e standard s ar e slate dt o b e propose di n 1999 , wit h promulgatio n o f

th e final rul e i n Novembe

r 2000

. Mr
. Shed d then wen

t o n t o describ e th e EPA' s procedure s fo r handlin g informatio n tha

t th e compan

y consider s to b e confidentia l busines s information (CBI)

. Th e compan y wil l hav e a n opportunit y t o revie w th e draf

t sit e visi t repor t prepare dby th e EP

A projec t team , an dt o commen t o n it s accuracy and t o identif y an y CBI

. The repor

t wit h an y CB I remove dwil l b e made apar

t ofth e publi c recor

d fo r thi s rulemaking

. Mr
. Won g andMr
. Carte

r wer e aske d t o identif y whethe r an y ofth e informatio n in th e conversation s wa s confidential

. N o informatio n presente d wa s claime d to b e confidentia l by th e Paktan

k officials

. Paktank Introduction Mr
. Won g bega n hi s introductio n b y statin g tha t th e Dee r Par k termina l i s th e larges t

for

hir e chemica l termina l i n Texas
. H e als o notedtha t th e Stat e of Texa s require s bes t

availabl e contro l technolog y (BACT) fo r th e facility

. Furthermore , he state dtha t h e ha s bee n involve d i n th e developmen

t of numerou s Ne w Sourc e Performanc e Standard s (NSPS ) whil e workin g fo r Regio n 6 ofth e EPA

. For

thes e reasons , he fel

t tha t ou r visi t to th e Paktan

k facilit y wa s agoo d choice

. H e provide d acopy of Paktank' s Texa s permit

(Attachmen

t 1)

. V
. Facility Processe s Paktan k Corporation' s Dee

r Par k termina l i s locate dnea

r th e Battlegroun dMemoria l o n

. th e Housto n Shi

p Channel

. I t

ha s 23 6 storag e tank s rangin g i n siz e from1,00 0 - 80,00 0 banel s 

# zP. 4

Sit e Visi tMemo/Paktank Corporatio n Marc h 2,199 8 Pag e 3 (42,00 0 - 3,360,00 0 gallons) , and ha s atotal storag e capacit y of 6,650,00 0 barrel s (279,300,00 0 gallons)

. Th e distributio n i s approximately 40 % fixed-roof tank s and60 % interna

l floatin g roo f tanks

. Th e Standar

d Industr y Classificatio n (SIC ) cod

e i s 422 6 (for-hir

e terminal s andspecialt

y warehousing)

. According to th e 199 7 Independen t Liqui dTerminal s Associatio n (ILTA ) Membe r Directory , th e primar

y commoditie s handle da

t th e facilit y are : primar

y organics , organi c intermediates , organi c end chemicals , andinorgani c chemicals

. Mr
. Won g als o state d tha t th e terminal handle s chemical s exclusively

. Paktan k compete s wit

h other for-hir e terminal s i n th e area , includin g Intercontinenta l Terminal s Company , Housto n Fue l Oi l Company , Baytank , and PetroUnite d Terminals

. Mr
. Wong indicate d tha

t th e facilit y wa s currentl

y operating o n aschedul e o f 2 4 hr/day , 7 days/week , and 5 2 weeks/yr

. H e als o state dtha t th e termina

l wa s operatin g a

t 10 0 percent capacity

. H e base d thi s figur e o n th e fact

tha t al l tank s wer

e presently occupied , an dtha t th e facilit y i s facing ashortag e o f

lan d fo r futur e expansions

. Paktank receive s liquid s b y al l modes , whic h include tanke r ships , barges , pipelines , tan k trucks , and railcars

. A s afor-hir e terminal , th e facilit

y doe s no t own an y ofth e organi c liquid s tha t it store s fo r it s customers
. Wastewater

Treatment Th e facilit y ha s tw o wastewate

r systems : astormwate

r syste man dacontaminate d wate r system
. Th e contaminate d wastewate r i s pipe dto asiste

r compan y adjacen t t o Paktank , calle d Empak

. Empa

k i s acommercia

l railca r cleanin g facilit

y tha t ha s wate r treatment capability

. Paktan k ha s aNationa

l Pollutio n Discharg e Eliminatio n System(NPDES ) permit fo r th e discharg e o f

stormwater
. Stormwate

r i s analyze do n sit

e b y EMPAK

fo r Paktan k andthe n discharge d t o th e Houston Shi p Channe l accordin g t o provision s ofth e Paktan k NPDE S stormwate r discharg e permit

. Semi-Aqueous Waste On e sourc e o

f semi-aqueou s waste identifiedfo r th e Paktan

k facilit y i s tank bottoms

. A t th e facility , semi-aqueou s wast e (o r sludge ) ma

y b e removedwhen cleanin g tanks ; i t the n ma y becom e par t ofth e wastewate

r stream , o r i t ma y b e packedinto drum s andreturne dt o customers
. Anothe r optio n that

Paktan k ha s i s to tur

n ove r th e semi-aqueou s wast

e t o Empa k fo r treatment
. Th e cleanin g of

tank s i s usually performe db y acontractor

who i s als o responsibl e fo

r removin g vapor s fromstorag e tank s (whic h ma y b e destroye dusin g aportabl e therma l oxidizer)

. 

# 3P. 5

Sit e Visi tMemo/Paktan k Corporation Marc h 2,199 8 Pag e 4 Emission Controls Paktan k ha s tw o flares fo

r surfac e vehicl e loading s (tan k truck s andrailcars) , on e marin e flare (tanke

r ship s an d barges) , and on e scrubbe r couple dwit

h acarbo n adsorptio n syste mt o contro l emission s fromth e storag e an dtransfe r of organi c liquids

. The marin e vapor contro l uni t and th e flares controllin g railca r and tank truc k loading s are manufacturedb y th e Joh n Zin k Company , and operate a

t approximatel

y 1,50 0 degree s Fahrenheit

. Th e unit s are firedwith natura l ga s to retai n th e idea

l operating temperature , anddatalogger s recor dvariou s parameters , includin g temperature , whic h ar e sen t t o th e company' s headquarter s i n Houston
. Th e scrubber , whic h i s couple dwit h tw o carbo n canisters , control s emission s fromtan k truc k and railca r loadin g operations

. Th e scrubbe r use s kerosene a s ascrubbin g mediu man d i s specifically designe d t o handl e chlorinate dhydrocarbons , afamil y o f product s tha

t Paktank doe s no t handl e i n larg e quantities

. Th e scrubbe r i s electrically controlle dandmonitore dwit h a systemdesigne d b y Teledyn e Analytica l Instruments
. Paktan k staf f wer e asked whethe

r they hadexperience dan

y hardwar e incompatibilit

y problem s o

r other issue s concerning vapor

recover y operation s wit

h tan k truck s or railcars

. The y indicate d that

ther e ha d been n o suc h problems

. Fugitive Emissions Paktan k calculate s it s fugitiv e emission s base dupo n SOCM I emissio n factors

. A s th e facilit y store s benzene , 4 0 CF

R6 1 subpar

t V (VHA P Equipmen

t Leaks ) applies

. Unde r

th e Federa l program , alea

k i s defined a s 50 0 ppmv , usin g EP A Metho d21

. Th e facilit

y ha s 5 day s fo r th e initial repair

attempt , an

d 1 5 day s t o complet

e an y equipmen

t lea k repairs

. Al l o f Paktank' s equipmen

t i s tagge dandnumbered

. According t o th e company' s O.L.D

. Sectio n 11 4 surve

y response , th e Dee

r Par k facilit y ha s atota

l of 7,25 9 valves , 14,59 3 compressors , and 15 7 pumps , al l o f whic h ar e monitore dquarterly

. Of

thes e piece s o f equipment , 1,83 5 valves , 3,69 4 flanges, and1 1 pump s ar e i n HA P service

. Th e Stat e o f Texa s als o require s Paktan k t o monitor

fugitive emissions

. Th e program cover s piping , valyes , flanges, pumps , andcompressor s i n VO C service

. Accordin g t o th e permi t issue d by th e TNRCC , th e fugitive emission s lea k detectio n an

drepair progra mapplie s t o equipmen t handlin g liquid s wit

h th e following parameters :

• VO C witi i an aggregat e partia l pressure o f

greate r than 0. 5 psi aa

t 2 0 degree s C , o r
• wher

e operatin g pressur

e i s a t leas t 0.72 5 psi aabov e ambien

t pressure . Mor e detaile d informatio n regardin g th e fugitiv e emissio n lea k detectio n andrepai r

programi s 

# 4 -P. 6

Sit e Visi tMemo/Paktank Corporatio n Marc h 2,199 8 Page 5 containe d i n th e facility' s Stat e permit (Attachment)

. V . Tou r o f

Facilit y A t approximately 10:00 a.m. , Paktan k staf f escorte dth e EP

A projec t tea mo n atou r

o f thei r facility

. Th e entourag e made it s first sto p a t atan k truc k loadin g rac k

(Statio n 1 ) tha

t had tw o loadin g spots
. Th e loadin g rac k wa s provisione dfo

r botto mloading , wit

h vapo r recover y line s tha t vente d t o aflare

. T o prevent a n accidenta

l overfilling o f

atank truck , th e facilit

y use s a Scull y overfil l protectio n device

. Thi s device , i n th e for mo f alance , i s inserte dinto th e tan k truc k and measure s liqui d level wit h afloat

. Followin g th e tan

k truc k rack , th e tea

mwa s ledto arailca

r loadin g rack

wit h tw o loadin g stations

. Railca

r loading s follo w aver

y tight schedule an

dnighttim e loadin g i s no t

unusual

. However , n o railcar s wer

e bein g loade ddurin g th e EP A sit e visit

. Nevertheless , genera l purpose-typ e car s dedicate d to MTB E transpor t wer e observedparke da

t th e rack

. The tea

m climbe d o n th e rac k

an d inspecte d th e 3-inc

h vapo r recover y line s andth e Scully overflo w protectio n device

. Depending upo n th e produc t being loaded , loadin g rate s var y between 40 0 an d 800 gallon s per

minut e (gpm)

. Adjacen t to th e railca

r loadin g rack , th e tea

mwa s escorte dto aJohn Zink therma l oxidize r whic h control s bot

h th e railca

r andtank truck loading racks

. A s wa s mentione dearlier i n thi s report , th e therma

l oxidizer' s temperatur

e i s maintaine da

t approximately 1,50

0 degree s F wit h natural gas . Parameter s that ar e recorde do n th e dat alogge r are th e maintenanc e activity , shutdowns , and report s o f

prope r operation/malfunctions

. Afte r viewin g th e therma

l oxidizer , th e projec t

tea mwen t t o se e th e marin e loadin g facility , whic h ha s tw o loadin g spot s fo r barge s only andon e spot

fo r ship s o r barges

. A barg e present a t th e dock wa s being loade d wit

h methanol

. Afte

r abrie f discussio n abou

t th e loadin g procedure s fo

r tan k ship s an d barges , th e projec t

tea mheadedto th e marin e vapor recover y uni t (MVRU)

. Th e MVR

U i s als o manufacturedby Joh n Zin k Company , andit s recorde dparameter s ar e simila r to thos e discusse d in th e previou s paragraph

. Thi s uni t wa s originally , installe di n 199 3 fo r th e purpos e of

controllin g benzen e emissions

. Th e facility' s scrubber/carbo n adsorptio n syste mwa s inspecte dnex

t b y th e EP A projec t team
. Th e scrubbe

r i s use d when loadin g chlorinate d hydrocarbons , andth e carbo n canister s serv e a s abackup shoul d th e scrubbe r malfunction

. Th

e carbon i s change di f

th e 10 0 pp m breakthroug h alar

msounds , but

i t ha s no t bee n changedsinc e i t

wa s first installe d in 1997

. Mr
. Wong note d that

th e us e o f chlorinate dhydrocarbon s i s decreasin g andtherefor e th e systemi s rarely used

. 

# 5P. 7

Site Visi tMemo/Paktank Corporatio n Marc h 2,199 8 Pag e 6 VI . Post-tou r Debriefing Followin g th e tour

ofth e facility , th e EP

A projec t tea mandth e Paktan

k staf f reconvene d i n th e facility' s conferenc e room . N o furthe r issue s wer

e discussed , andth e tou r

wa s concluded

. VII . Actio n Item s Th e EP A projec t tea minformedMr
. Won

g tha t h e wouldb e sen

t adraf t cop y ofth e tri p repor t fo r hi s revie w and comment
. N o furthe r actio n item s wer

e identified

.



## loP. 8

ATTACHMEN

T



# 9 -P. 9

Barr y R . McBee , Chairman R . B . "Ralph " Marquez , Commissioner Joh n M. Baker , Commissioner Da n Pearson . Executive Director

TEXA S NATURA

L RESOURC E CONSERVATIO N COMMISSIO N Protecting Texas by Reducing and Preventing Pollution Januar y 2 , 199 8

Mr
. Quirin o Q

. Won

g Manager , Environmenta

l Affairs Paktank Corporatio n 200 0 Wes t

Loo p South , Suit

e 220 0 Houston , Texa s 7702 7 Re : Permi t

Amendmen

t Permi t No
. 466 A Dee r Par k Termina l Bul k Chemica l Storag e Facilit

y Deer Park , Harri s Count

y Accoun t I D No
. HG-0629- I Dea r Mr
. Wong : Thi s i s i n respons e t

o you r lette r datedSeptembe

r 23 , 1997 an dpenni t

application , For mPI-1 , concerning th

e propose damendmen

t t o Permi t No
. 466A

. We understan dtha t yo u propos e t o stor e toluen e diisocyanat

e (TDI ) in Spherica

l Pressur e Tan k T-80 0 andtha

t al l TD I produc t shipment s will b e controlle deither b y avapor-balanc e operatio n o r b y routin g th e emission s generate dduring TD I loadin g t o aflare. Also , thi s will acknowledg e tha t you r applicatio n fo r th e above-reference dpermi t amendmen

t i s technicall

y complet e a s of December

8 , 1997

. Pursuant to 3 0 TA C Section 116.116(b) , Penni t No
. 466 A i s hereb y amended

. Thi s informatio n wil l b e incorporatedint

o th e existing permit

file. Enclose

dare revise dspecia

l condition s pages , ashort-ter

mmaximu

mallowabl e emissio n rate s tabl e (MAERT ) (Attachmen t A-l) , an da n Attachment

B- 3 tha t include s TD I to replac e thos e cunentl y attache dto you r permit

. Pleas e replac e thos e conditions , di e short-ter mMAERT , an

dthe Attachment

B- 3 currentl y attache dt o you r permi t wit h thos e enclosed

. Thi s amendmen

t wil l b e automaticall

y voi dupo n th

e occurrenc e o f

an y o f th e following , a s pe r §116.115(b)(1) : 1

. Failur e t

o begin constructio n of

th e change s authorize dby thi s amendmen t withi n 1 8 month s fro

mthe date o

f thi s audiorization

.

P.O . Bo x 1308 7 • Austin

. Texa s 78711-308 7 • 512/239-100 0 • Interne taddress : www.tr.rcc.s.ate.' x '!< ;P.1 0

Mr
. Quirin o Q

. Won

g Pag e 2 Januar y 2 , 199 8 Re : Permi t

No
. 466A
2

. Discontinuanc e o

f constructio n o

f th e change s authorize db y thi s amendmen t for aperio d o f 1 8 consecutiv e month s or more . 3

. No t completin g th e change s authorizedb y thi s amendmen t witiii n areasonabl e time

. We hav e enclose d tw o operation s certificatio n form s (FormPI-3 A an dFon n PI-3B)

. Sectio n 116.110(b ) require s yo u t o certif y tha t operation s addresse di n thi s permi t ar e i n conformanc e wit

h representation s in th e permi t amendment

application

. Pleas e fil e thes e certification s wit

h bot h th e Texa s Natura

l Resourc e Conservatio n Commissio n (TNRCC ) Ne w Sourc e Revie

w Permit s Division i

n Austi n an ddi e TNRC C Housto n Regiona l Offic e i n atimely manner . You r cooperatio n i

n thi s matte

r i s appreciated

. I f

you hav e furthe

r questions , pleas e contac t Mr
. Timoth y Frida

y of our Offic e o f Ai r Quality , New Sourc e Review Permit s Divisio n a t (512 ) 239-1568

. Sincerely ,

Pearso n A ^ cecutiv e Directo r

/ Texa s Natural Resourc e Conservatio n Commissio n DP/TF/r l Enclosure s
cc : Ms
. Orbi e Ratcliff

, Air Sectio n Manager , Housto n Mr
. Ro b Barrett , Director , Harri s Count y Pollutio n Contro l Department , Pasaden a



# °iP.1 1

SPECIA L CONDITION S Permit No
. 466 A
STORAG E AN D LOADIN G O F VOLATIL E ORGANI C COMPOUND S (VOC ) 1

. A

. A n interna l floating roo f

(IFR) o r equivalent

contro l shal l b e installe do n al l tank s (1 ) wher e th e VO C ha s a

n aggregat

e partial pressure greate

r tha n 0. 5 psi aat

th e maximu mexpecte d operatin g temperature o r (2 ) wher e a n IFRi s require d b y th e storag e an d loadin g scenario s o

f Attachment

B
. B
. A n open-to p tan k containin g afloating roo f

whic h use s doubl e sea

l o r secondar y sea l technolog y shal l b e an approve dcontro l alternativ e t o a n interna l floating roo f

tank provided di e primar

y sea l consists o

f eitiie r amechanica

l shoe sea l or aliquid-mounte d seal , an d di e secondar

y sea l i s rim-mounted

. A weathershiel di s no t approvabl e a s a secondar y sea l unles s specificall

y reviewe dan ddetermine dt o b e vapor-tight

. C

. Fo r an y tan k equipped wid

i afloatin g roof , di e integrit

y o f di e floating roo f

seal s shal l b e verifie d annuall y and record s maintaine dt o describ e dates , sea l integrity , an d correctiv e action s taken

. D
. Th e floating roo f

desig n shall incorporate sufficien t flotatio n to confor

mt o th e requirement s o f

AP I Code 650 , Appendix C an dAppendi x H o r a n equivalent

degre e o f flotation , except

tha t a n interna l floatin g cove r neednot b e designe

dt o meet rainfal l suppor t requirements

. E
. Uninsulate d tan

k exterio r surface s expose dt o th e su n shal l b e white

. F
. Fo r purpose s o

f assurin g compliance wit

h VO C emission limitations , th e holder o f thi s permit shal l maintain amonthl

y emission s recor

dwhich describe s calculate demission s o f VO C fro mall storag e tanks an

dloadin g operations

. Th e recor dshal l include tan k o r loadin g point

identificatio n number , contro l metho dused , shor e tan k capacit y i n gallon s o r barrels , name o f

th e material store do r

loaded , VOC molecula

r weight , *— > VO C monthl

y averag e temperatur

e i n degree s Fahrenheit , VO C vapo r pressure at

th e montiil y averag e materia

l temperatur

e i n psia , VO C throughpu

t fo r th e previou s mont

h and year-to-date i n gallon s o r barrels , andtotal ton s o f

emission s including control s fo r th e previou s mont

h an dyear-to-date

. G

. Emission s fo

r storag e tank s shall b e calculate dusing : (a ) th e most recen t editio n o f AP-4 2 "Compilatio n o f

Ai r Pollutant Emissio n Factors " and(b ) th e Texa s Natura l Resourc e Conservatio n Commissio n (TNRCC ) publicatio n title d"Technica l Guidanc e Packag e fo

r Chemica l Source s - Storag e Tanks. " Emission s fo r loading operation s shal l b e calculate d using : (a) the mos t recent editio n o f AP-4 2 an d(b ) di e TNRC C publicatio n title d "Technica l Guidanc e Packag e fo

r Chemica l Source s - Loadin g Operations. " The permit

holde r shal l hav e si x month s fromth e dat e o n whic h ane w editio n o r supplemen

t o f AP-4 2 i s publishe d t

o calculat e all termina

l storag e an d loadin g emission s accordin g to th e mos t recent AP-4 2 methodology

. 

# 1 0P.1 2

SPECIA L CONDITION S Permi t No
. 466 A Pag e 2

2

. An y IFR s dia

t are installe d in fixed-roof tank s shal l b e equippe dwit h either amechanica

l shoe , aliquid-mounted , o r

avapor-mounte

dprimar y seal

. I f avapor-mountedprimar

y seal i s used , th e tan

k mus t als o b e equippedwit

h arim-mounte dsecondar y seal

. 3

. Audio , olfactory , an

d visua l checks shal

l b e made of

quic k connec t joints , fittings , and hose s i n VO C servic e during all transfe r operations

. Repai

r o f di e leakin g componen

t shal l b e performe d immediatel y upo n detectio n o f

aleak

. Loadin g operation s shal l ceas e i f repair cannot b e accomplishe

d during operation

. Record s shal l b e kep t of al l leak s detecte d and subsequent

repair s performed

.
FUGITIV E EMISSIO N LEA K DETECTION AN

D REPAI RPROGRA

M 4

. Piping

. Valves

. Flanges

. Pumps , an dCompressor s in VO C Servic e - Intensiv e Directe d Maintenanc e (28MID ) Excep t a s ma y b e provide d fo

r i n th e specia l condition s o f

thi s permit , th e followin g requirement s apply t o th e above-referencedequipment

. A

. Thes e condition s shal

l no t appl y (1 ) wher e th e VOC hav

e a n aggregate partial pressur e o r vapo r pressure of

les s tha n 0.0 5 psi aa

t 20° C o r (2 ) operatin g pressure i s a t leas t 5 kilopascal s (0.72 5 psi ) belo w ambien t pressure . Equipmen

t exclude dfromthi s conditio n shal l b e identifiedi n alis t t o b e made availabl e upo n request
. B
. Constructio n o

f ne w an d reworke dpiping , valves , andpum p andcompresso r

system s shal l confor

mt o applicabl e ANSI , API , ASME , o r equivalent

codes

. C

. Ne w and reworked undergroundproces s pipeline s shall contai n n o burie dvalve s suc h tha t fugitiv e emissio n monitorin g i s rendere dimpractical

. D
. T o m e exten t dia t goo d engineerin

g practic e will pennit , ne

w an dreworke dvalve s an d pipin g connection s shal l b e s o locatedto b e reasonabl y accessibl e fo

r leak-checkin g durin g plan

t operation

. Non-accessibl e valve s shall b e identifie di n alis t t o b e mad e availabl e upo n request
. E
. Ne w an d reworke d pipin g connection s shal l b e weldedo r flanged. Screwe d connection s are permissibl e onl y o n pipin g smalle

r tha n two-inc h diameter

. N o later tha n di e nex t schedule d quarterly monitorin g afte r initia l installatio n o r

replacement , all new o r reworke d connection s shal l b e gas-teste do r

hydraulically-teste dat

n o les s dia n norma l operating pressur

e an dadjustment s mad

e as necessar

y to obtai n leak-fre e performance

. Flange s shal l b e inspectedb y visual , audible , and/o r olfactor y mean s a t leas t weekly b y operatin g personnel walk-through

.



# I IP.1 3

SPECIA L CONDITION S Permi t No
. 466 A Pag e 3

Each open-ende

d valv e o r lin e shal l b e equippe dwit h acap , blin dflange , plug , o r a secon d valve

. Excep t

durin g sampling , th e secon dvalv e shal l b e closed

. F
. Accessibl e valve s shal l b e monitore db y leak-checking fo r fugitive , emission s a t

leas t quarterl y using a

n approve dga s analyzer

wit h adirecte dmaintenanc e program . Sealless/leakles s valve s (including , but no t limite dto , bellow s an

ddiaphrag mvalves ) an d relie f valve s equippe dwiti i arupture dis c o r venting t o acontro l devic e ar e no t require d t o b e monitored

. Fo r

valve s equippe dwit

h ruptur e discs , apressure gaug e shal l b e installed betwee n th e relie f valv e an druptur e dis c to monitor

dis c integrity

. All leakin g disc s shall b e replace da

t di e earlies t

opportunit

y bu t n o later tha n th e nex t proces s shutdown

. A directe d maintenanc e progra mshal l consis t of the repai r

an dmaintenanc e o f components assisted simultaneousl y b y th e us e of a n approve dga s analyzer

suc h tha t aminimumconcentratio n o f leakin g VO C i s obtainedfo r eac h componen

t bein g maintained

. G

. Al l ne

w an d replacement

pump s an

dcompressor s shall b e equippe dwit h ashaf t sealin g syste

mtha t prevent s o r

detect s emission s of

VO C fromth e seal

. Thes e sea l system s nee d no t

b e monitore dandma

y include (bu t

are no t limite dto ) dual pump seal s witi i barrier

fluid a t highe r pressure tha

n proces s pressure , seal s degassin g t o ven t contro l systems kep t

i n goo dworking order , o r seal s equippe dwidi an automati c sea l failure detectio n an

dalarmsystem
. Submergedpump s o r sealles s pump s (including , bu

t no t limitedto , diaphragm , canned , o r magneti c drive n pumps ) ma y b e use d t o satisf

y di e requirement s o f

dii s conditio n an

dneedno t

b e monitored

. Al l other pum p and compresso r

seal s emittin g VO C shal l b e monitore d wit h a n approve d ga s analyze

r at leas t quarterly

. H
. Damage d o r

leakin g valves , flanges , compressor seals , an dpum p seal s foun

d t o b e emittin g VOC i

n exces s of

50 0 ppm v o r foun db y visua l inspectio n t o b e leakin g (e.g. , drippin g proces s fluids) shal l b e tagge dandreplace do r repaired

. Ever

y reasonabl e effor t shal l b e mad

e t o repai r

aleakin g component , a s specifiedi n dii s paragraph , within 1 5 day s afte

r th e lea k i s found

. I f

th e repair of acomponen

t would requir e a uni t shutdown , th e repai r

ma y b e delaye dunti l th e nex t schedule dshutdown

. A

U leakin g component s whic h canno t b e repaire dunti l aschedule dshutdow n shal l b e identifie d fo

r suc h repai r b y tagging

. Th e TNRC C Executiv e Director , a t hi s discretion , ma

y require earl y uni t

shutdow n o r

othe r appropriate actio n base d o n th e number an d severit y of tagge dleak s awaitin g shutdown

.P.1 4

SPECIAL CONDITION S Permi t No
. 466 A Pag e 4

I
. Th e result s o f

the require dfugitiv

e monitorin g an

dmaintenanc e programshal l b e mad e availabl e to th e TNRC C Executive Directo r o r hi s designate drepresentativ e upo n request
. Record s shal l indicat e appropriat

e dates , tes t

methods , instrument readings , repai r

results , an

dcorrectiv e action s taken

. Record s o f flange inspection s ar e no t require d unles s alea

k i s detected

. J
. Complianc e wit

h the requirement s o

f dii s conditio n doe s not

assure complianc e wit

h requirement s of

TNRC C 3 0 TA

C Chapte r 11 5 (Regulatio n V) , a n applicabl e Ne w Sourc e Performanc e Standard , o r a n applicabl e Nationa

l Emissio n Standard fo r Hazardou s Ai r

Pollutant s (NESHAPS ) an ddoe s not constitut e approval o f

alternativ e standard s fo r

thes e regulations

.
EMISSIO N LIMITATION S 5

. A

. Attachmen t

A- l reflect s short-ter

memissio n rate s fo

r all unit s covere d b y th e consolidate d permit

. Short-ter mstorag e tan

k emissio n rate s ar e base do n operatio n a s fixed-roof

tanks

. B
. Attachmen

t A- 2 reflects annua

l allowabl e emission s fo

r landan dmarin e operation s fo r al l unit s covere d by th e consolidate dpermit

.
FEDERAL PROGRA M APPLICABILITY 6
. Thes e facilitie s shal l comply wit h all requirement s o

f U.S

. Environmenta

l Protectio n Agenc y (EPA ) Regulation s o n Standard s o f Performanc e fo

r Ne w Stationar

y Source s promulgate d for

Storag e Tank s i n Titl e 4 0 Cod e o f Federa l Regulation s Par t

6 0 (4 0 CF R 60) , Subpart s A , K , Ka , andKb

. Th e permit holder shal l maintai n alis t

showin g th e applicabilit

y o f K , Ka , o r

Kb

. 7
. Thes e facilitie s shal l compl y wit h all requirement s o

f EP A Regulation s o n NESHAP S i n 4 0 CF R61 , Subpart s A , J , V , Y , an dBB
.
OPERATIONAL CONDITION S 8

. Thi s termina

l facilit y i s authorizedto stor

e an dloa dcompound s accordin g t o th e scenario s an d control s describe d i

n Attachmen

t B o f thi s permi t

entitle d"Paktan

k Corporatio n - Approve d Chemicals , Storage , an dLoadin g Scenarios. " Exemption s fromPermitting , 3 0 TA C Chapte r

106 , ma y b e usedt

o authoriz e achang e i

n the storag e an d loadin g scenario s of

Attachment

B provide dtha

t th e exemptio n clai mi s submitte dt o th e TNRC C New Sourc e Revie w Permit s Divisio n i n Austi n an dall loca l pollutio n contro l agencie s 

# 13P.1 5

SPECIA L CONDITION S Permi t No
. 466 A Pag e 5

simultaneousl

y wid i apenni t amendmen

t wit h th e penni t

review limite dt o tha t

particular chemical(s)

. Storag e and loadin g of chemical s which are not

include do n Attachmen t

B i s prohibite d without

amendmen

t to thi s permit

unles s al l of

th e followin g condition s ar e met : A

. Th e ne

w chemica l ha s a n equa l o r lowe r vapo r pressur e (a t 100'F) , a n equa l o r

lowe r vapo r molecula r weight , an

da n equa l o r higher publishe dEffect s Screenin g Leve l (ESL ) valu e tha

n achemica

l alread y approve dfo

r handlin g o n Attachmen t B
. Acceptabl e ES L value s fo

r ne w chemical s are limite dt

o tiiose specifie di n di e mos t curren t publishe d TNRC C Toxicology andRis k Assessmen

t (TARA ) ES L Lis t

o r approve d b y th e TNRC C TAR A group . B
. Th e ne w chemica l shal l no t b e (1 ) a n inorgani c compoun

dor (2) achemical containin g sulfu r o r halogen s unles s di

e product has avapor

pressur e les s tha n 0. 5 psi aat

100 * F an d doe s no t requir e loadin g control s unde

r an y scenari o o n Attachmen

t B
. Th e new chemica l mus t b e handledwit

h the sam

e filling, witiidrawal , an dpumpin g rat e limitation s and di e sam

e medio do

f storag e andloadin g control s a s require d fo r th e approve d chemica

l o n Attachmen

t B wid i whic h it i s compared

. C

. Notification shal

l b e mad e widii n 1 5 calenda

r day s afte r th e first occurrenc e o f

storag e o r loadin g of

eac h ne w chemica

l addedt o Attachment

B b y implementatio n o f paragraph s A and B above

. Th e notificatio n shal l include di e name o f th e ne w chemica l and di e correspondin g storag e andloadin g scenarios

. Th e notificatio n shal l b e submitte d i n writin g t o th e followin g offices : One cop y t o th e TNRC C Housto n Regiona l Office

. One cop y to di e Harri s Count y Pollutio n Contro l Department , Pasadena

. One cop y to th e TNRC C Austin Office o f Ai r Quality , New Sourc e Revie w Permit s Division

. D
. Th e ne

w chemica

l shal l b e identifiedi n th e next permi t amendmen

t o r renewal application fo

r review an

d incorporatio n withi n di e permit

. Air dispersio n modelin g i s no t require d to incorporat

e chemical s addedunder

the authorit

y o f thi s special conditio n int

o Attachmen

t B
. 9

. Any chemica

l currentl y authorize dfo

r storag e in afixed-roof

tan k ma y als o b e store d i n an y tan k equippe d wid i a n IFR
. An

y chemica l currentl y authorize dfo

r storag e i n an IF R tan k ma y als o b e store d i n ahig

h pressur e spherica l storag e tank

. An

y chemical ma

y b e store d i n tank s smalle

r tha n thos e grante di

n the permi t

scenario

. 

# /4 -P.1 6

SPECIAL CONDITION S Permi t No
. 466A Pag e 6

10

. Thi s permit

als o audiorize s th e storag e an dloading o f

an y material consistin g o f

amixtur e o f approved chemicals , amixtur e containin g chemical s addedunder

th e audiorit

y of Special Conditio n No
. 8 , o r

chemical s ma

t mee t al l applicable requirements unde r exemption s from permitting , 3 0 TA C Chapte r 106

. Mixtures , a

s authorizedhere , shal l b e manage dusin g di e scenari o o f th e componen

t tha t i s presen t i n die highes t

percentag e i n th e vapo r

phase

. Fo r mixture s tha

t contai n component s i

n equa l percent s i n th e vapo r

phas e bu t

diffe r i n requirement s fo

r storag e and loading , die mor e stringen t scenari o wil l apply

. I n th e situatio n dia t the differenc e in percentag e o f di e highest

an dsecon dhighes t compound s i s equal t o o r les s tha n 1 0 percent , the mixtur

e shal l be handle daccordin g to the compoundwit h th e lowes t ESL

. Record s shal l b e kep t o f th e vapo r phas e percentag e determination s fo r eac h mixtur e stored

. 11

. Thi s permit

als o authorize s th e storag e an dloading o

f an y materia l consistin g o f

amixtur e of approve d chemicals

. An

y compoun

dnam e ma t i s no t liste do n Attachment

B shal l b e authorize d fo

r storag e an d loadin

g i f it s chemica

l abstrac t number matche s tha

t o f a compound alread

y liste d i n Attachmen

t B
. Except

a s authorize dunde r

Special Conditio n No
. 8 , storag e of

odie r chemical s i s prohibite dunles s prio r approva l i s obtaine dfromdi e Executive Director

o f th e TNRCC

. It

wil l no t b e necessar

y t o obtai n approva

l for chemical s previousl y approve d fo

r storag e in aspecific tank

. A revise dTabl e 7 shal l b e sen t t o th e TNRC C Regiona

l Office witiii n te

n day s o f an y chang e i n servic e o f

thes e tanks

. 12

. Flare s shall b e designe d an doperatedin accordanc e wit h 4 0 CF R60.18 , includin g specification s of

minimumheatin

g value o f di e wast e gas , maximu mti p velocity , an d pilo t flam e monitoring

. I

f necessar y t o insur e adequat e combustion , sufficien

t fue l ga s shal l b e adde d t o mak

e th e gase s combustible

. A n infrared o r

ultraviole t

monito r i s considere d equivalen t t o athermocoupl e fo

r flame monitoring purposes . 13

. Issuanc e of

thi s permi t

doe s no t assur e complianc e wit

h o r constitute approval o f

marin e vapo r contro l system s pursuant to the requirement s o f

th e Unite dState s Coas t

Guard (USCG ) whic h ma y hav e jurisdictio n ove

r the desig n andoperatio n of suc h systems
. Th e holde r o f thi s permit

i s advise dt

o contac t di e USC G regarding dii s matter
. Withi n 6 0 day s o f obtaining certificatio n fromdi e USCG , di e applican

t shal l sen dacop y of dii s certificatio n t o th e TNRC C Housto n Regiona l Office

. 14

. Emission s fro

mbarg e loadin g operation s shal l b e minimizedby th

e us e o f avapo r collectio n syste mwhe n loading al l compound s whic h requir e vapo r contro l under

permitte dconditions

. Th e vapor

collectio n syste mshal

l be operatedan

dmaintaine dat

les s than atmospheri c condition s a

t th e facilit y vapor collectio n poin

t whe n authorize db y USC G Regulations , 4 6 CF R154.800ff

. Negativ e pressure s ar

e prohibitedb

y thi s regulatio n durin g th e loadin g 

# 15P.1 7

SPECIA L CONDITION S Penni t No
. 466 A Pag e 7

o f inerte d vessels

. Al

l inerted U.S

. fla

g vessel s shal l b e certifiedleak-tigh t prio r t o loadin g a s specifie d i

n 4 0 CF R6 1 (NESHAP

S Subpar t BB)

. I f negativ e pressur

e loading i s possibl e unde r USC G regulations , th

e syste mpressure shal l b e monitore dan drecorded

. A pressure/vacuu mgaug e shall be installe dto verif y anegativ e pressur

e of a t leas t aone-inc h water column

. I

f di e vacuu msyste mshoul dfail , th e operato r ha s on e hour

to correc t

th e proble man d restore the vacuum . Loading operation s shal l ceas e i f di e vacuu mi s no t restore d withi n one hou

r of failure

. 15

. Th e following compound s (storag e scenario s show n i n Attachmen t B-3 ) must b e maintaine d a t atemperature les s tha

n or equa l t o thos e liste dbelow

. CA S Numbe r 75-07- 0

106-99- 0

107-00- 6 503-17- 3 822-35- 3 75-61- 6 109-93- 3 75-04- 7 540-67- 0 109-92- 2 513-35- 9 78-78- 4 Chemica l Nam e Acetaldehyd

e Aviatio n Fue

l (10 0 Octane ) Aviatio n Gasoline 1,3-Butadien

e Butylen e 1-Butyn e 2-Butyn e Cyclobuten

e Dibroraodifluoromethane Divinyl Edie

r Ediylamin e Ethy l Methy

l Ether Ethy l Viny

l Ethe r Isoamylen e Isopentan e Isopren e Contro l

Temperature (°F ) 

### 60 8 5 8 5 4 8 5 7 0 7 4 2 5 6 3 5 5 5 5 4 0 8 5 8 8 7 7 4 0 Storag e Tan k

Typ e 

### IF R 

### IF R IF R IF R IF R Pressur e 

### IF R 

### IF R IF R IF R IF R EF R IF R IF R IF R IF R 

# lbP.1 8

SPECIA L CONDITION S Permit No
. 466A Pag e 8

CA

S Numbe r 75-31- 0 563-46- 2 563-45- 1

513-35- 9 107-31- 3

107-25- 5 591-93- 5 109-66- 0 627-20- 3
109-67- 1 75-56- 9 689-97- 4 Chemica l Nam e Isopropylamin e 2 Metiiy l 1 Buten

e 3 Methy l 1 Buten

e 3 Methy l 1 Butyn

e 2 Metiiy l 2 Buten

e Methy l Format

e Methy l Isopropy l Ethe

r Methy l Viny l Etiie

r 1,2-Pentadiene Pentan e 2-Penten e (trans ) Pentene s 1-Penten e Propylen e Oxid

e Viny l Acetylene Contro l Temperature (°F ) 5 5 8 0 5 6 7 4 8 8 7 5 7 8 6 7 6 6 8 8 5 0 5 5 5 5 8 0 3 3 Storag e Tan k

Typ e IF R IF R IF R IF R IF R IF R IF R Pressur e IF R IF R IF R IF R IF R IF R IF R
In di e even t

dia t aproduc t

i s delivere dto di e facilit y at atemperature exceedin g th e represented reduced temperamre , th e permi t holde r wil l hav e 7 2 hour s to lowe r th e produc t temperature
. A s long a s th e tan k i s unde r refrigeratio n durin g thi s 72-hour period , i t wil l b e considere d t

o b e in complianc e wid

i di e requirement s i n thi s paragraph

. Record s shal l be kep t o f product deliver y temperature s an

ddi e tim e take n t o reduc e th e temperatur

e t o th e require d level

. Whe n i n VO C servic e requirin g temperatur e control , daily temperature reading s shal l b e performed an

d recorde d fo r

al l applicabl e tanks

.


## I 1 

## *P.1 9

SPECIA L CONDITION S Permi t No
. 466A Pag e 9

HALOGENATED HYDROCARBO N LOADIN G CONTRO L REQUIREMENT S 16

. Durin g loadin

g o f railcar s an

d tank s truck s containin g compound s requirin g vapo r contro l b y th e carbo n adsorptio

n syste m(CAS ) a s designate do n Attachmen t B- 2 (compound s note d with CARBO

N a s the loading contro l device) , al l resultin g emission s shal l ven t throug h th e Station 2 0 lea

n oi l adsorption uni t

andCA S consistin g o f

a t leas t tw o activate d carbo n canister s tha

t ar e connected i

n serie s (Emissio n Poin t

No
. [EPN ] CA-1)

. A

. Th e CA S shall b e sampledan drecorde dever

y fiftee n minute s durin g loadin g o f al l halogenated compounds t

o determine breakthroug h of VOC

. Th e samplin g poin t shal l b e at th e outlet

of th e initia l canister bu t before th e inlet

t o th e secon do r

final polishin g canister

. Samplin g shal l b e don e durin g loadin g condition s reflectin g maximu memission s to di e CAS

. B
. Th e metho d o

f VOC samplin g andanalysi s shal l b e by anon-dispersiv e infrare d spectroscopy analyze

r o r aTNRCC-approve dequivalent

. O n eac h da y tha t samplin g i s required, di e analyze

r shal l b e calibrate dprio r

t o samplin g at

0 ppmv ±1 0 percen t and a t 100 ppm v ±1 0 percent

wid i acertifie dga s mixture o f th e specifi c compoun d dia t will b e transferred utilizing th e Station 2 0 lea n oi l adsorptio n uni t

andCA S a s th e emissio n contro l device

. I f tw o o r more different

product s wil l b e controlle d b y di e Statio n 2 0 lea

n oi l adsorptio n uni t

andCA S o n di e sam

e day , prio r

t o samplin g th e ne w compound di e analyze r shal l b e re-calibrate da

t 0 ppmv ±1 0 percent

and a t 10 0 ppm v ±1 0 percen

t using acertifie dga s mixture o f th e subsequent

compound(s)

. C

. Breakthroug

h shal l b e define da s ameasuredVO C concentratio n o f 10 0 ppmv . Whe n di e condition of

breakthrough o f

VO C fromth e initial saturatio n caniste r occurs , th e wast e ga s flow shal

l b e switche

dt o di e secondcaniste

r immediately

. Prio r

t o an y ne w loadin g event , afresh canister shal l b e place da s di e new fina l polishin g canister

. Sufficient ne w activated carbo n canister s shal l b e maintaine da t di e sit e t o replace spen t carbon canisters suc

h dia t replacement s can performe dprio r t o an y ne w loadin g event
. D
. Record s o

f di e CA S monitoring maintaine da t di e plant site shal l includ e (bu t

ar e no t limite d to ) di e following : (1 ) Sampl e tim

e an d date

. (2 ) Monitorin g result s (ppmv)

. (3 ) Correctiv e actio n take n includin g di e tim e an

ddate of that action

. (4 ) Th e compoun

d an d loading rate a

t th e time of

sampling

. (5 ) Analyze

r calibratio n records

.P.2 0

SPECIA L CONDITION S Permi t No
. 466A Pag e 1 0

17

. Th e CA S t

o b e installed i

n serie s wit

h the existin g Statio n 2 0 lea n oi l adsorptio n unit , including th e analyze

r specifie di n Specia

l Conditio n No
. 16B , shal l b e fully operationa l n o late r tha n Januar y 1 , 1998

. After

th e CA S i s operational , bu t n o late r tha n Januar y 1 , 1998 , Attachmen

t C i s voi dandall termina l operation s ar e limite d t o di e storag e an d loading scenario s o f

Attachmen t

B
. 18

. An y halogenate d compoundwith amarin e loadin g contro l requiremen t designate d i n Attachmen

t B- 2 a s "CONTROL " canno t b e handle dby barg e o r

shi p unti l engineerin g specification s fo

r amarine halogenate dvapo r contro l syste

mhav e bee n submitte d t o and approve d b y th e TNRCC

. Th e propose dcontro l technology mus t mee t o r excee d 9 8 percen t

contro l efficiency

. Th e marin e halogenate dvapor contro l syste mmus t

b e operationa l prio r to loadin g an

y halogenate dproduct s tha t require marin e vapo r

control s pe r Attachmen

t B-2

.
HEXAMETHYLEN

E DIAMIN

E (HMD ) LOADIN G CONTROL REQUIREMENT S 19

. Al l emission s resultin g fro mHM D loadin g operation s (landan dmarin e based ) shal l b e controlle d by th e SC-80 0 Water Scrubber

. Wate

r shall circulat

e throug h th e scrubbin g syste msuch tha

t all HM D loadin g emission s ar e controlle dwid i aminimu mo f 98. 3 percen

t efficiency

. 20

. The minimu

mSC-80 0 wate r circulatio n rat e tha

t wil l ensur

e a98. 3 percen t

HM D contro l efficienc y shal l b e establishe dan ddocumente ddurin g th e initia l stac k emissio n testin g performed in accordanc e wid i Special Conditio n No
. 23

. Th e SC-80 0 wate r circulatio n rate s shall b e monitored an drecorde ddurin g al l HM D loading operations

. 21

. Th e SC-80 0 scnibbin g wate r shal l b e change dou t

afte r ever y 120,00 0 barrel s o f

HM D loadin g throughput

. TOLUENE-2.4-DIISOCYANAT E (TD D CONTRO L REQUIREMENT S 22

. Th e TD I i s limite d t

o storag e i n Pressur e Tan k T-800

. All emission s fro mTan k T-80 0 depressurization s shal

l b e route dt o th e terminal' s Marin e Flare

. Pressure Tan k T-80 0 shal l not b e depressurize d durin g TD I loadin g operations

. (12/97 )

\<\P.2 1

SPECIAL CONDITION S Permi t No
. 466 A Pag e 1 1

INITIA L DETERMINATIO N O F COMPLIANC E 23

. Th e holde r

o f dii s permit

shal l perfor mstac k samplin g andodier

testin g a s requiredt o establis h th e actual patter n an dquantitie s o f

ai r contaminant s being emitte dint o th e atmospher e fromth e CA S (EP N CA-1 ) an

dth e HM D Wate

r Scrubbe r (EP N SC-800)

. Th e holde r o f thi s permi t

i s responsible for

providin g samplin g andtestin g facilitie s an d conductin g th e samplin g an d testing operation s at

hi s expense . A

. Th e TNRC C Houston Regiona l Offic e shal l b e contacte da s soo n a s testin g i s scheduled , bu t

no t les s dia n 4 5 day s prio r

t o samplin g t o schedul e apretes t meetin g o r meetings

. Th e notic e shal l include : (1 ) Date for

pretes t meeting(s)

. (2 ) Date(s ) sampling will occur . (3 ) Nam e of

firmconductin

g sampling

. (4 ) Typ e o f

sampling equipmen

t t o b e used

. (5 ) Medio d o r

procedur e to b e use di n sampling

. Th e purpos e of

di e pretes t

meeting(s ) i s t o revie w th e necessar y samplin g an

d testin g procedures , t o provide the proper dat aform s for

recordin g pertinent

data , an d t o revie w th e forma

t procedure s fo

r submittin g th e tes t

reports
. A writte n propose d description of an y deviatio n fro msamplin g procedure s specifie d i n permi t condition s or

TNRC C o r EP A samplin g procedure s shal l b e mad e availabl e t o di e TNRC C prio r

t o th e pretes t meeting

. Th e TNRC C Regiona l Manager o r th e Manager o f TNRC C Engineerin

g Service s Teamshal l approv e o r disapprov e o f

an y deviatio n fromspecifiedsampling procedures

. Request s t o waiv e testin

g fo r an y pollutant

specifie di n B o

f thi s conditio n shall b e submitted to di e TNRCC Offic e o f Ai r Quality , New Sourc e Revie w Permit s Division

. B
. Ai r contaminant s emittedfro mth e CA S t o b e teste dfo r include halogenate d hydrocarbons

. Th e SC-80

0 Wate r Scrubber shal l b e teste dfo

r HM D mas s emission s an d to demonstrat

e complianc

e wid i aminimu

m98. 3 percen

t HM D contro l efficiency

. C

. Sampling fo

r the CA S shal l occu r witiii n 6 0 day s afte

r initia l CAS start-up and a

t suc h odie r time s a s ma

y b e requiredb

y th e Executiv e Directo r

o f the TNRCC

. Samplin g fo r th e SC-80 0 Wate

r Scrubbe r shal l occur

witiii n 6 0 day s afte

r initia l start-up o f 

# aoP.2 2

SPECIA L CONDITION S Permi t No
. 466A Pag e 1 2

controlled HM

D loading operation s an

da t suc h othe r time s a s ma

y b e require d b y th e Executiv e Directo r o f the TNRCC

. Requests fo

r additiona l tim e t o perfor msamplin g shal l be submitte d t o th e TNRC C Housto n Regiona l Office

. D
. Loadin g shall occur

a t maximu moperating/emissio n rate s durin g stac k emissio n testing

. Primar

y operatin g parameter s tha t enabl e determinatio n of

th e maximu m loading/emissio

n rate s shal l b e monitore dandrecorde ddurin g di e stac k tests
. Thes e parameter s are t o b e determine da t di e pretes t

meeting(s)

. E
. Thre e copie s of

th e fina l sampling report s shal l b e forwardedt o th e TNRC C withi n 3 0 day s afte

r sampling i s completed

. Samplin g report s shal l compl

y wit h th e attache d provision s of

Chapter 1 4 o f the TNRC C Sampling Procedure s Manual

. Th e report s shal l b e distribute d a s follows : One cop y to th e TNRC C Houston Regiona l Office

. One cop y to th e Harri s Count

y Ai r Pollutio n Contro l Department , Pasadena

. On e cop y t o th e TNRC C Austi n Ai r Qualit y Enforcement , Engineerin g Service s Section

.
EMISSIO N CALCULATION AN D RECORDKEEPING REQUIREMENT S 24

. Daily an

d annua l storag e tan

k throughputs shall b e recorde dfo r ever y tan k affecte db y dii s permit

. Dail

y and annua

l truck , railcar , barge , an dshi p loadin g throughput s shal l b e recorded

. I n addition , an

y tan k filling , tan

k wididrawal , o r

loading operation s tha

t ar e performe d under reduce d hourl y rate s pe r

Attachmen

t B shal l b e recorde

da t di e tim e the y occur . Fo r truc k an d railca r loading , areduce drate i s tha t which i s permitte dbelo w 80 0 gallon s pe r minute

. Fo r

barg e and shi p loading , areduce drat e i s tha t which i s permitte d belo w 3,80 0 barrel s per

hour for chemical s storedi n 80,00 0 barre l tank s an d2,00 0 barrel s pe r hou r fo r chemical s store d i n smalle r tanks

. Thes e record s shall reflect th e dat e and th e actua l rat e o f th e filling, withdrawing , and/o r loading operatio n of

di e specifi c compound

. Also , m e record s shal l sho w ho

w the reducedrat

e was attained , i.e. , restrictiv e orifice , desig n capacit

y o f pump , etc
. 25

. Facility-wid

e land-base

d emissions'Shal

l b e calculate dmondily

. Thi s must includ e storag e tank emissions , al l land-base dloading emissions , flare emissions , an dfugitiv e emissions

. Total annua

l land-base d emission s must b e kep t o n acalenda

r yea r basis

. 

# a iSPECIAL CONDITION S

Permi t No
. 466 A Pag e 1 3

26

. Marin e loadin

g emission s shal

l b e calculate

dmondily

. Tota

l annua l marin e emission s mus t b e kep t o n acalenda

r yea r basis

. Record s shal l include material s loaded , throughputs , loadin g method , contro l method , VOC molecula r weight , VO C monthl

y averag e temperature , VO C vapo r

pressure a

t the monthl

y averag e material temperature , an d tota l ton s o f emissions

. 27

. Th e followin

g record s shall b e maintainedin accordanc e wit h th e requirements o f

General Conditio n No
. 7 o f

tiiis pennit : A

. Record s describin g di e date s o f inspection , sea

l integrity , an dan

y correctiv e action s take n fo r al l IF Rsea

l inspection s i

n accordanc e wit

h Specia l Conditio n No
. IC

. B
. A mondil y emission s recordi n accordanc e wit h Specia l Conditio n No
. IF
. C

. Record s o f

al l leak s detecte dduring transfe r operation s andth e subsequen t repair s performe d i n accordanc e wit h Specia l Conditio n No
. 3

. D
. Record s o f

th e fugitive emission lea

k detection an drepai r

progra mi n accordanc e with Specia l Conditio n No
. 41

. E
. Record s demonstratin g ho w eac h ne w chemica

l meet s al l o f

th e requirement s fo r additio n t o Attachment

B a s establishe di n paragraph s A andB o f Specia l Conditio n No
. 8

. Th e recor d shal l identif y the nam e o f th e ne w chemica

l andth e compariso n chemica l already approve dfo

r handling andshal l lis t

an dcompare th e value s o f di e vapor pressure (a

t 100 ' F) , vapor

molecula r weight , andES L o f

th e ne w chemica

l t o th e chemical already approve dfo r handlin g o n Attachmen

t B
. Th e record shal l includ e th e storag e an d loadin g scenarios , th e applicabl e Attachment (B-l , B-2 , o r B-3 ) fo r th e ne w chemical , an

ddi e dat e o n whic h di e new chemica l wa s first handle d a t di e terminal

. F
. Record s o f

al l vapo r

phas e percentag e determination s for al l mixture s store d i n accordanc e wit

h Specia l Conditio n No
. 10

. G

. Record s of

all shore-sid

e vacuu msyste mrepair s i n accordanc e wit h Specia l Conditio n No
. 14

. H
. Record s o f

di e produc t

deliver y temperature , th e time take n t o reduc e th e temperature t o th e require d level , andth e daily temperatur e reading s for

al l applicabl e tank s i n accordanc e wit

h Specia l Conditio n No
. 15

. 

# a aP.2 4

SPECIA L CONDITION S Penni t No
. 466 A Pag e 1 4

I
. Record s o

f the CA S i

n accordanc e wit

h Specia l Conditio n No
. 16D

. J
. Record s o

f th e SC-80 0 scrubbin g water circulatio n rate s durin g al l HM D loadin g operation s in accordanc e wit h Special Conditio n No
. 20

. K
. Record s showin

g die cumulative HM D loadin g throughpu

t an ddi e date s o f

al l SC-80 0 scrubbin g wate

r replacement s t o demonstrat e compliance wit

h Special Conditio n No
. 21

. L
. Record s o

f al l compounds handledb y shi p o r barge fo r whic h marin e loadin g control s ar e no t require d b y Attachment s B- 2 o r B-3 , but ar e require db y th e curren t

editio n o f 3 0 TA C Chapte

r 11 5 (Regulatio n V)

.

Date d 1-2-9 8



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d Cnamicali . Sloraga . on d Loadin g Scanario *

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pv..aof 2Parm l No . 468 A Allaelman l B-3 : Compound a Stora d k l Haala d an d Refrigerate d Insutala d Tank * Paklan k Corporatio n • Approve d Chemical* . Storage , an d Loadin g Scenario *

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" ' NONE " FLAI B NON E NON E NON E NONE" " NON E HON K RAI E HON E HONE" - "HOH B ' NONE" ' NON E NON E " ' NON E — ' " NON B " NON B " '
' HON E NON B HOH B HON E
' —NbN E "tfOH G NON E "
' HOHE ' HOHB" " HONE' ' FLAI B ' ' NON B "HON B ' " "HON B — "NON B —NON B — '

— FLAIE "
HON ! HON E NON B NON B NON E FLAI B HON B ' NON E NON E HON B NON E NbN E NbN E

' NON B NON E HON E NON E NON I PCAI E — HON E NON E PLAIE'" ' RAI E

.. .

SCIIIBIE I

— ~ .

HON ! HONE " —PtAlE ^ FCMS — HON E
" HOH E ' ' HON !
" FLAI R | ' FLAI E

Pag o I o( a

T J