Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

50976 Indiantown Cogeneration 1 bituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

50976 Indiantown Cogeneration 1 As Received Higher Heating Value

50976 Indiantown Cogeneration 1 As Received % Moisture

50976 Indiantown Cogeneration 1 As Received % Ash

50976 Indiantown Cogeneration 1 As Received % Sulfur

50976 Indiantown Cogeneration 1 Dry basis Higher Heating Value

50976 Indiantown Cogeneration 1 Dry basis % Ash

50976 Indiantown Cogeneration 1 Dry basis % Sulfur

50976 Indiantown Cogeneration 1 Dry basis Antimony

50976 Indiantown Cogeneration 1 Dry basis Arsenic

50976 Indiantown Cogeneration 1 Dry basis Beryllium

50976 Indiantown Cogeneration 1 Dry basis Cadmium

50976 Indiantown Cogeneration 1 Dry basis Chlorine

50976 Indiantown Cogeneration 1 Dry basis Chromium

50976 Indiantown Cogeneration 1 Dry basis Cobalt

50976 Indiantown Cogeneration 1 Dry basis Fluorine

50976 Indiantown Cogeneration 1 Dry basis Lead

50976 Indiantown Cogeneration 1 Dry basis Manganese

50976 Indiantown Cogeneration 1 Dry basis Mercury

50976 Indiantown Cogeneration 1 Dry basis Nickel

50976 Indiantown Cogeneration 1 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D3302

ASTM D3174

ASTM 

ASTM D5865

ASTM D3174

ASTM 

ASTM 

ASTM D3683 (Mod)

ASTM D3683 (Mod)

ASTM D3683 (Mod)

ASTM 

ASTM D3683 (Mod)

ASTM 

ASTM D3761

ASTM D3683 (Mod)

ASTM D3683 (Mod)

ASTM D6722

ASTM D3683 (Mod)

ASTM D3684 (Mod)
EIA Facility Code Facility Name Boiler ID HAPs Test Group

50976 Indiantown Cogeneration 1 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

2010-11189 12548.00 Btu/lb

2010-11197 12656.00 Btu/lb

2010-11196 12473.00 Btu/lb

2010-11195 12725.00 Btu/lb

2010-11194 12693.00 Btu/lb

2010-11193 12693.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

2.22 13.4 0.85 12832 Btu/lb 13.7 0.87

2.3 12.75 0.89 12954 Btu/lb 13.05 0.91

2.49 14.12 0.84 12792 Btu/lb 14.49 0.86

2.32 12.96 0.89 13027 Btu/lb 13.27 0.91

2.25 12.88 0.92 12986 Btu/lb 13.18 0.92

2.24 12.79 0.89 12984 Btu/lb 13.08 0.91


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

1598 ppm

1729 ppm

1485 ppm

1528 ppm

1552 ppm

1477 ppm


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

2.22

2.3

2.49

2.32

2.25

2.24

Proximate Analys


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

13.7 70.23 4.58 1.45 0.87

13.05 71.17 5.67 1.51 0.91

14.49 69.73 4.39 1.36 0.86

13.27 70.41 4.61 1.42 0.91

13.18 70.53 4.66 1.44 0.92

13.08 70.96 4.58 1.46 0.91

Proximate Analyses, % by wt Ultimate Analyses, % by wt


Oxygen

9.17

8.69

9.17

9.38

9.27

9.01


EIA Facility Code Facility Name Boiler ID HAPs Test Group

50976 Indiantown Cogeneration 1 Mercury and non-mercury metalic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

2010-11190 12526.00 Btu/lb

2010-11199 12604.00 Btu/lb

2010-11200 12669.00 Btu/lb

2010-11198 12690.00 Btu/lb

2010-11192 12757.00 Btu/lb

2010-11188 12671.00 Btu/lb

2010-11187 12612.00 Btu/lb

2010-11201 12546.00 Btu/lb

2010-11191 12661.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

2.07 13.7 0.88 12790 Btu/lb 13.99 0.9

2.1 13.72 0.87 12874 Btu/lb 14.02 0.89

2.1 13.4 0.87 12940 Btu/lb 13.69 0.89

2.19 13.09 0.89 12974 Btu/lb 13.38 0.89

2.08 12.77 0.9 13029 Btu/lb 13.04 0.92

2.18 13.05 0.89 12954 Btu/lb 13.34 0.91

2.13 13.38 0.88 12887 Btu/lb 13.67 0.9

2.2 13.86 0.85 12828 Btu/lb 14.17 0.87

2.1 13.4 0.88 12933 Btu/lb 13.69 0.9


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

1316 ppm 0.063 μg/g 0.37 μg/g 2.435 μg/g 2.197

1523 ppm 0.037 μg/g 0.404 μg/g 2.834 μg/g 2.229

1516 ppm 0.114 μg/g 0.278 μg/g 2.694 μg/g 2.236

1590 ppm 0.049 μg/g 0.274 μg/g 2.89 μg/g 2.201

1502 ppm 0.06 μg/g 0.984 μg/g 2.726 μg/g 2.169

1378 ppm 0.086 μg/g 0.319 μg/g 2.497 μg/g 2.158

1707 ppm 0.09 μg/g 0.314 μg/g 2.357 μg/g 2.203

1468 ppm 0.055 μg/g 0.959 μg/g 4.381 μg/g 2.24

1447 ppm 0.0489 μg/g 0.309 μg/g 2.544 μg/g 2.207


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

μg/g 0.063 μg/g 19.498 μg/g 8.68 μg/g 7.71 μg/g

μg/g 0.081 μg/g 20.006 μg/g 8.744 μg/g 7.635 μg/g

μg/g 0.099 μg/g 19.842 μg/g 8.828 μg/g 7.67 μg/g

μg/g 0.085 μg/g 19.708 μg/g 8.685 μg/g 7.22 μg/g

μg/g 0.081 μg/g 19.059 μg/g 8.297 μg/g 7 μg/g

μg/g 0.075 μg/g 19.023 μg/g 8.656 μg/g 7.289 μg/g

μg/g 0.134 μg/g 19.319 μg/g 8.73 μg/g 8.31 μg/g

μg/g 0.1 μg/g 26.46 μg/g 8.817 μg/g 7.067 μg/g

μg/g 0.083 μg/g 19.346 μg/g 8.564 μg/g 7.381 μg/g


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

16.552 μg/g 4.67 μg/g ND 9.09 μg/g

16.87 μg/g 4.03 μg/g ND 9.272 μg/g

17.048 μg/g 5.234 μg/g ND 9.393 μg/g

17.074 μg/g 4.847 μg/g ND 9.42 μg/g

16.699 μg/g 4.479 μg/g 10 ppm 9.319 μg/g

16.613 μg/g 4.407 μg/g ND 9.174 μg/g

16.856 μg/g 4.665 μg/g ND 9.264 μg/g

17.558 μg/g 4.552 μg/g ND 9.674 μg/g

16.64 μg/g 4.751 μg/g 10 ppm 9.257 μg/g


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

2.07 13.99 70.04 4.6 1.28 0.9

2.1 14.02 70.22 4.66 1.29 0.89

2.1 13.69 70.48 4.62 1.31 0.89

2.19 13.38 70.9 4.69 1.32 0.89

2.08 13.04 70.83 4.64 1.29 0.92

2.18 13.34 70.45 4.64 1.29 0.91

2.13 13.67 71 4.63 1.33 0.9

2.2 14.17 69.84 4.51 1.29 0.87

2.1 13.69 70.58 4.66 1.32 0.9

Proximate Analyses, % by wt Ultimate Analyses, % by wt


 basis (including ash).

Oxygen

9.19

8.92

9.01

8.82

9.28

9.37

8.47

9.32

8.85


EIA Facility Code Facility Name Boiler ID HAPs Test Group

50976 Indiantown Cogeneration 1 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

Proximate Analyses, 


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Proximate Analyses, % by wt Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

50976 Indiantown Cogeneration 1

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

Proximate Analys


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Proximate Analyses, % by wt Ultimate Analyses, % by wt


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm