P.1 

OAR Box 1672 

Prepped by Charmelle Mathews 

Document Number: 

>6)II-B-10 

Docket Number: 

A-98-13 

Printed 9/30/2008 11:01:00 AM Sheet 16 of 132 
P.2 

ESBJB 

A-98-13 

MEMORANDUM 

TO: 

FROM: 

Project File 

Organic Liquids Distribution NESHAP 

ESD Project No. 96/05 

BemdHaneke <^ — 

Pacific Environmental Services, Inc. (PES) 

DATE: March 2,1999 

SUBJECT: Site Visit to Paktank Corporation, Deer Park, Texas 

I. Purpose 

The purpose of this site visit was to tour the Paktank facility in an effort to inform EPA 

and contractor personnel concerning organic liquids distribution (O.L.D.) operations and to 

collect information related to air emissions from the operations. This work is in support ofthe 

development of national emission standards for hazardous air pollutants (NESHAP) for the 

organic liquids distribution (non-gasoline) source category. 

II. Location and Date 

Paktank Corporation 

Deer Park Terminal 

South of Houston Ship Channel 

2759 Battleground Road 

Deer Park, Texas 77536 

October 21,1998 (9:00-11:30 am) 

III. Participants 

Paktank Corporation 

Mr. Quirino Wong - Manager of Environmental Affairs 

Mr. David Carter - Environmental Supervisor 

Texas Natural Resources Conservation Commission (TNRCC) 

Ms. Carol Harkins 

Environmental Protection Agency (EPA) 

Mr. Stephen Shedd - Project Officer, OAQPS/ESD/WCPG 

Research Triangle Park, NC 
Site Visit Memo/Paktank Corporation 

March 2,1998 

Page 2 

Pacific Environmental Services. Inc. CPBS) 

Mr. Greg LaFlam - Research Triangle Park, NC 

Mr. Bemd Haneke - Research Triangle Park, NC 

IV. Pre-Tour Discussion 

Introduction 

EPA Introduction 

After the participants introduced themselves, Steve Shedd, EPA, began the meeting by 

discussing the background ofthe EPA's regulation of hazardous air pollutant (HAP) emissions. 

Prior to the Clean Air Act Amendments of 1990 (CAAA), regulations were on the basis of 

individual HAP and a limited number of regulations were completed. The CAAA included a 

HAP list and prescribed that rules be developed for categories of sources (industrial types). The 

stringency ofthe Organic Liquids Distribution (non-gasoline) rule (for existing sources) will be 

based on "floor" levels of control representing the control achieved by the average ofthe top 12 

percent of sources in this category. The standards are slated to be proposed in 1999, with 

promulgation of the final rule in November 2000. 

Mr. Shedd then went on to describe the EPA's procedures for handling information that 

the company considers to be confidential business information (CBI). The company will have an 

opportunity to review the draft site visit report prepared by the EPA project team, and to 

comment on its accuracy and to identify any CBI. The report with any CBI removed will be 

made a part ofthe public record for this rulemaking. Mr. Wong and Mr. Carter were asked to 

identify whether any ofthe information in the conversations was confidential. No information 

presented was claimed to be confidential by the Paktank officials. 

Paktank Introduction 

Mr. Wong began his introduction by stating that the Deer Park terminal is the largest forhire chemical terminal in Texas. He also noted that the State of Texas requires best available 

control technology (BACT) for the facility. Furthermore, he stated that he has been involved in 

the development of numerous New Source Performance Standards (NSPS) while working for 

Region 6 ofthe EPA. For these reasons, he felt that our visit to the Paktank facility was a good 

choice. He provided a copy of Paktank's Texas permit (Attachment 1). 

V. Facility Processes 

Paktank Corporation's Deer Park terminal is located near the Battleground Memorial on 

. the Houston Ship Channel. It has 236 storage tanks ranging in size from 1,000 - 80,000 banels 

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P.4 

Site Visit Memo/Paktank Corporation 

March 2,1998 

Page 3 

(42,000 - 3,360,000 gallons), and has a total storage capacity of 6,650,000 barrels (279,300,000 

gallons). The distribution is approximately 40% fixed-roof tanks and 60% internal floating roof 

tanks. The Standard Industry Classification (SIC) code is 4226 (for-hire terminals and specialty 

warehousing). According to the 1997 Independent Liquid Terminals Association (ILTA) 

Member Directory, the primary commodities handled at the facility are: primary organics, 

organic intermediates, organic end chemicals, and inorganic chemicals. Mr. Wong also stated 

that the terminal handles chemicals exclusively. Paktank competes with other for-hire terminals 

in the area, including Intercontinental Terminals Company, Houston Fuel Oil Company, 

Baytank, and PetroUnited Terminals. 

Mr. Wong indicated that the facility was currently operating on a schedule of 24 hr/day, 7 

days/week, and 52 weeks/yr. He also stated that the terminal was operating at 100 percent 

capacity. He based this figure on the fact that all tanks were presently occupied, and that the 

facility is facing a shortage of land for future expansions. 

Paktank receives liquids by all modes, which include tanker ships, barges, pipelines, tank 

trucks, and railcars. As a for-hire terminal, the facility does not own any ofthe organic liquids 

that it stores for its customers. 

Wastewater Treatment 

The facility has two wastewater systems: a stormwater system and a contaminated water 

system. The contaminated wastewater is piped to a sister company adjacent to Paktank, called 

Empak. Empak is a commercial railcar cleaning facility that has water treatment capability. 

Paktank has a National Pollution Discharge Elimination System (NPDES) permit for the 

discharge of stormwater. Stormwater is analyzed on site by EMPAK for Paktank and then 

discharged to the Houston Ship Channel according to provisions ofthe Paktank NPDES 

stormwater discharge permit. 

Semi-Aqueous Waste 

One source of semi-aqueous waste identified for the Paktank facility is tank bottoms. At 

the facility, semi-aqueous waste (or sludge) may be removed when cleaning tanks; it then may 

become part ofthe wastewater stream, or it may be packed into drums and returned to customers. 

Another option that Paktank has is to turn over the semi-aqueous waste to Empak for treatment. 

The cleaning of tanks is usually performed by a contractor who is also responsible for removing 

vapors from storage tanks (which may be destroyed using a portable thermal oxidizer). 

3 
P.5 

Site Visit Memo/Paktank Corporation 

March 2,1998 

Page 4 

Emission Controls 

Paktank has two flares for surface vehicle loadings (tank trucks and railcars), one marine 

flare (tanker ships and barges), and one scrubber coupled with a carbon adsorption system to 

control emissions from the storage and transfer of organic liquids. The marine vapor control unit 

and the flares controlling railcar and tank truck loadings are manufactured by the John Zink 

Company, and operate at approximately 1,500 degrees Fahrenheit. The units are fired with 

natural gas to retain the ideal operating temperature, and data loggers record various parameters, 

including temperature, which are sent to the company's headquarters in Houston. 

The scrubber, which is coupled with two carbon canisters, controls emissions from tank 

truck and railcar loading operations. The scrubber uses kerosene as a scrubbing medium and is 

specifically designed to handle chlorinated hydrocarbons, a family of products that Paktank does 

not handle in large quantities. The scrubber is electrically controlled and monitored with a 

system designed by Teledyne Analytical Instruments. 

Paktank staff were asked whether they had experienced any hardware incompatibility 

problems or other issues concerning vapor recovery operations with tank trucks or railcars. They 

indicated that there had been no such problems. 

Fugitive Emissions 

Paktank calculates its fugitive emissions based upon SOCMI emission factors. As the 

facility stores benzene, 40 CFR 61 subpart V (VHAP Equipment Leaks) applies. Under the 

Federal program, a leak is defined as 500 ppmv, using EPA Method 21. The facility has 5 days 

for the initial repair attempt, and 15 days to complete any equipment leak repairs. 

All of Paktank's equipment is tagged and numbered. According to the company's O.L.D. 

Section 114 survey response, the Deer Park facility has a total of 7,259 valves, 14,593 

compressors, and 157 pumps, all of which are monitored quarterly. Of these pieces of 

equipment, 1,835 valves, 3,694 flanges, and 11 pumps are in HAP service. 

The State of Texas also requires Paktank to monitor fugitive emissions. The program 

covers piping, valyes, flanges, pumps, and compressors in VOC service. According to the permit 

issued by the TNRCC, the fugitive emissions leak detection and repair program applies to 

equipment handling liquids with the following parameters: 

• VOC witii an aggregate partial pressure of greater than 0.5 psia at 20 degrees C, or 

• where operating pressure is at least 0.725 psia above ambient pressure. 

More detailed information regarding the fugitive emission leak detection and repair program is 

4-
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Site Visit Memo/Paktank Corporation 

March 2,1998 

Page 5 

contained in the facility's State permit (Attachment). 

V. Tour of Facility 

At approximately 10:00 a.m., Paktank staff escorted the EPA project team on a tour of 

their facility. The entourage made its first stop at a tank truck loading rack (Station 1) that had 

two loading spots. The loading rack was provisioned for bottom loading, with vapor recovery 

lines that vented to a flare. To prevent an accidental overfilling of a tank truck, the facility uses a 

Scully overfill protection device. This device, in the form of a lance, is inserted into the tank 

truck and measures liquid level with a float. 

Following the tank truck rack, the team was led to a railcar loading rack with two loading 

stations. Railcar loadings follow a very tight schedule and nighttime loading is not unusual. 

However, no railcars were being loaded during the EPA site visit. Nevertheless, general 

purpose-type cars dedicated to MTBE transport were observed parked at the rack. The team 

climbed on the rack and inspected the 3-inch vapor recovery lines and the Scully overflow 

protection device. Depending upon the product being loaded, loading rates vary between 400 

and 800 gallons per minute (gpm). 

Adjacent to the railcar loading rack, the team was escorted to a John Zink thermal 

oxidizer which controls both the railcar and tank truck loading racks. As was mentioned earlier in 

this report, the thermal oxidizer's temperature is maintained at approximately 1,500 degrees F 

with natural gas. Parameters that are recorded on the data logger are the maintenance activity, 

shutdowns, and reports of proper operation/malfunctions. 

After viewing the thermal oxidizer, the project team went to see the marine loading 

facility, which has two loading spots for barges only and one spot for ships or barges. A barge 

present at the dock was being loaded with methanol. After a brief discussion about the loading 

procedures for tank ships and barges, the project team headed to the marine vapor recovery unit 

(MVRU). The MVRU is also manufactured by John Zink Company, and its recorded parameters 

are similar to those discussed in the previous paragraph. This unit was originally, installed in 

1993 for the purpose of controlling benzene emissions. 

The facility's scrubber/carbon adsorption system was inspected next by the EPA project 

team. The scrubber is used when loading chlorinated hydrocarbons, and the carbon canisters 

serve as a backup should the scrubber malfunction. The carbon is changed if the 100 ppm 

breakthrough alarm sounds, but it has not been changed since it was first installed in 1997. Mr. 

Wong noted that the use of chlorinated hydrocarbons is decreasing and therefore the system is 

rarely used. 

5 
P.7 

Site Visit Memo/Paktank Corporation 

March 2,1998 

Page 6 

VI. Post-tour Debriefing 

Following the tour ofthe facility, the EPA project team and the Paktank staff reconvened 

in the facility's conference room. No further issues were discussed, and the tour was concluded. 

VII. Action Items 

The EPA project team informed Mr. Wong that he would be sent a draft copy ofthe trip 

report for his review and comment. No further action items were identified. 

lo 
P.8 

ATTACHMENT 

9-
P.9 

Barry R. McBee, Chairman 

R. B. "Ralph" Marquez, Commissioner 

John M. Baker, Commissioner 

Dan Pearson. Executive Director 

TEXAS NATURAL RESOURCE CONSERVATION COMMISSION 

Protecting Texas by Reducing and Preventing Pollution 

January 2, 1998 

Mr. Quirino Q. Wong 

Manager, Environmental Affairs 

Paktank Corporation 

2000 West Loop South, Suite 2200 

Houston, Texas 77027 

Re: Permit Amendment 

Permit No. 466A 

Deer Park Terminal 

Bulk Chemical Storage Facility 

Deer Park, Harris County 

Account ID No. HG-0629-I 

Dear Mr. Wong: 

This is in response to your letter dated September 23, 1997 and pennit application, Form PI-1, 

concerning the proposed amendment to Permit No. 466A. We understand that you propose to 

store toluene diisocyanate (TDI) in Spherical Pressure Tank T-800 and that all TDI product 

shipments will be controlled either by a vapor-balance operation or by routing the emissions 

generated during TDI loading to a flare. Also, this will acknowledge that your application for 

the above-referenced permit amendment is technically complete as of December 8, 1997. 

Pursuant to 30 TAC Section 116.116(b), Pennit No. 466A is hereby amended. This information 

will be incorporated into the existing permit file. Enclosed are revised special conditions pages, 

a short-term maximum allowable emission rates table (MAERT) (Attachment A-l), and an 

Attachment B-3 that includes TDI to replace those cunently attached to your permit. Please 

replace those conditions, die short-term MAERT, and the Attachment B-3 currently attached to 

your permit with those enclosed. 

This amendment will be automatically void upon the occurrence of any of the following, as per 

§116.115(b)(1): 

1. Failure to begin construction of the changes authorized by this amendment within 

18 months from the date of this audiorization. 

P.O. Box 13087 • Austin. Texas 78711-3087 • 512/239-1000 • Internet address: www.tr.rcc.s.ate.'x '!<; 
P.10 

Mr. Quirino Q. Wong 

Page 2 

January 2, 1998 

Re: Permit No. 466A 

2. Discontinuance of construction of the changes authorized by this amendment for a period 

of 18 consecutive months or more. 

3. Not completing the changes authorized by this amendment witiiin a reasonable time. 

We have enclosed two operations certification forms (Form PI-3A and Fonn PI-3B). 

Section 116.110(b) requires you to certify that operations addressed in this permit are in 

conformance with representations in the permit amendment application. Please file these 

certifications with both the Texas Natural Resource Conservation Commission (TNRCC) New 

Source Review Permits Division in Austin and die TNRCC Houston Regional Office in a timely 

manner. 

Your cooperation in this matter is appreciated. If you have further questions, please contact 

Mr. Timothy Friday of our Office of Air Quality, New Source Review Permits Division at 

(512) 239-1568. 

Sincerely, 

Pearson A ^ 

cecutive Director / 

Texas Natural Resource Conservation Commission 

DP/TF/rl 

Enclosures 

cc: Ms. Orbie Ratcliff, Air Section Manager, Houston 

Mr. Rob Barrett, Director, Harris County Pollution Control Department, Pasadena 

°i 
P.11 

SPECIAL CONDITIONS 

Permit No. 466A 

STORAGE AND LOADING OF VOLATILE ORGANIC COMPOUNDS (VOC) 

1. A. An internal floating roof (IFR) or equivalent control shall be installed on all tanks 

(1) where the VOC has an aggregate partial pressure greater than 0.5 psia at the 

maximum expected operating temperature or (2) where an IFR is required by the 

storage and loading scenarios of Attachment B. 

B. An open-top tank containing a floating roof which uses double seal or secondary seal 

technology shall be an approved control alternative to an internal floating roof tank 

provided die primary seal consists of eitiier a mechanical shoe seal or a liquid-mounted 

seal, and die secondary seal is rim-mounted. A weathershield is not approvable as a 

secondary seal unless specifically reviewed and determined to be vapor-tight. 

C. For any tank equipped widi a floating roof, die integrity of die floating roof seals shall 

be verified annually and records maintained to describe dates, seal integrity, and 

corrective actions taken. 

D. The floating roof design shall incorporate sufficient flotation to conform to the 

requirements of API Code 650, Appendix C and Appendix H or an equivalent degree 

of flotation, except that an internal floating cover need not be designed to meet rainfall 

support requirements. 

E. Uninsulated tank exterior surfaces exposed to the sun shall be white. 

F. For purposes of assuring compliance with VOC emission limitations, the holder of this 

permit shall maintain a monthly emissions record which describes calculated emissions 

of VOC from all storage tanks and loading operations. The record shall include tank 

or loading point identification number, control method used, shore tank capacity in 

gallons or barrels, name of the material stored or loaded, VOC molecular weight, 

*—> VOC monthly average temperature in degrees Fahrenheit, VOC vapor pressure at the 

montiily average material temperature in psia, VOC throughput for the previous month 

and year-to-date in gallons or barrels, and total tons of emissions including controls 

for the previous month and year-to-date. 

G. Emissions for storage tanks shall be calculated using: (a) the most recent edition of 

AP-42 "Compilation of Air Pollutant Emission Factors" and (b) the Texas Natural 

Resource Conservation Commission (TNRCC) publication titled "Technical Guidance 

Package for Chemical Sources - Storage Tanks." Emissions for loading operations 

shall be calculated using: (a) the most recent edition of AP-42 and (b) die TNRCC 

publication titled "Technical Guidance Package for Chemical Sources - Loading 

Operations." The permit holder shall have six months from the date on which a new 

edition or supplement of AP-42 is published to calculate all terminal storage and 

loading emissions according to the most recent AP-42 methodology. 

10 
P.12 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 2 

2. Any IFRs diat are installed in fixed-roof tanks shall be equipped with either a mechanical 

shoe, a liquid-mounted, or a vapor-mounted primary seal. If a vapor-mounted primary seal 

is used, the tank must also be equipped with a rim-mounted secondary seal. 

3. Audio, olfactory, and visual checks shall be made of quick connect joints, fittings, and 

hoses in VOC service during all transfer operations. Repair of die leaking component shall 

be performed immediately upon detection of a leak. Loading operations shall cease if 

repair cannot be accomplished during operation. Records shall be kept of all leaks detected 

and subsequent repairs performed. 

FUGITIVE EMISSION LEAK DETECTION AND REPAIR PROGRAM 

4. Piping. Valves. Flanges. Pumps, and Compressors in VOC Service - Intensive Directed 

Maintenance (28MID) 

Except as may be provided for in the special conditions of this permit, the following 

requirements apply to the above-referenced equipment. 

A. These conditions shall not apply (1) where the VOC have an aggregate partial pressure 

or vapor pressure of less than 0.05 psia at 20°C or (2) operating pressure is at least 

5 kilopascals (0.725 psi) below ambient pressure. Equipment excluded from this 

condition shall be identified in a list to be made available upon request. 

B. Construction of new and reworked piping, valves, and pump and compressor systems 

shall conform to applicable ANSI, API, ASME, or equivalent codes. 

C. New and reworked underground process pipelines shall contain no buried valves such 

that fugitive emission monitoring is rendered impractical. 

D. To me extent diat good engineering practice will pennit, new and reworked valves and 

piping connections shall be so located to be reasonably accessible for leak-checking 

during plant operation. Non-accessible valves shall be identified in a list to be made 

available upon request. 

E. New and reworked piping connections shall be welded or flanged. Screwed 

connections are permissible only on piping smaller than two-inch diameter. No later 

than die next scheduled quarterly monitoring after initial installation or replacement, 

all new or reworked connections shall be gas-tested or hydraulically-tested at no less 

dian normal operating pressure and adjustments made as necessary to obtain leak-free 

performance. Flanges shall be inspected by visual, audible, and/or olfactory means 

at least weekly by operating personnel walk-through. 

II 
P.13 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 3 

Each open-ended valve or line shall be equipped with a cap, blind flange, plug, or a 

second valve. Except during sampling, the second valve shall be closed. 

F. Accessible valves shall be monitored by leak-checking for fugitive, emissions at least 

quarterly using an approved gas analyzer with a directed maintenance program. 

Sealless/leakless valves (including, but not limited to, bellows and diaphragm valves) 

and relief valves equipped witii a rupture disc or venting to a control device are not 

required to be monitored. For valves equipped with rupture discs, a pressure gauge 

shall be installed between the relief valve and rupture disc to monitor disc integrity. 

All leaking discs shall be replaced at die earliest opportunity but no later than the next 

process shutdown. 

A directed maintenance program shall consist of the repair and maintenance of 

components assisted simultaneously by the use of an approved gas analyzer such that 

a minimum concentration of leaking VOC is obtained for each component being 

maintained. 

G. All new and replacement pumps and compressors shall be equipped with a shaft 

sealing system that prevents or detects emissions of VOC from the seal. These seal 

systems need not be monitored and may include (but are not limited to) dual pump 

seals witii barrier fluid at higher pressure than process pressure, seals degassing to 

vent control systems kept in good working order, or seals equipped widi an automatic 

seal failure detection and alarm system. Submerged pumps or sealless pumps 

(including, but not limited to, diaphragm, canned, or magnetic driven pumps) may be 

used to satisfy die requirements of diis condition and need not be monitored. 

All other pump and compressor seals emitting VOC shall be monitored with an 

approved gas analyzer at least quarterly. 

H. Damaged or leaking valves, flanges, compressor seals, and pump seals found to be 

emitting VOC in excess of 500 ppmv or found by visual inspection to be leaking (e.g., 

dripping process fluids) shall be tagged and replaced or repaired. Every reasonable 

effort shall be made to repair a leaking component, as specified in diis paragraph, 

within 15 days after the leak is found. If the repair of a component would require a 

unit shutdown, the repair may be delayed until the next scheduled shutdown. AU 

leaking components which cannot be repaired until a scheduled shutdown shall be 

identified for such repair by tagging. The TNRCC Executive Director, at his 

discretion, may require early unit shutdown or other appropriate action based on the 

number and severity of tagged leaks awaiting shutdown. 
P.14 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 4 

I. The results of the required fugitive monitoring and maintenance program shall be 

made available to the TNRCC Executive Director or his designated representative 

upon request. Records shall indicate appropriate dates, test methods, instrument 

readings, repair results, and corrective actions taken. Records of flange inspections 

are not required unless a leak is detected. 

J. Compliance with the requirements of diis condition does not assure compliance with 

requirements of TNRCC 30 TAC Chapter 115 (Regulation V), an applicable New 

Source Performance Standard, or an applicable National Emission Standard for 

Hazardous Air Pollutants (NESHAPS) and does not constitute approval of alternative 

standards for these regulations. 

EMISSION LIMITATIONS 

5. A. Attachment A-l reflects short-term emission rates for all units covered by the 

consolidated permit. Short-term storage tank emission rates are based on operation 

as fixed-roof tanks. 

B. Attachment A-2 reflects annual allowable emissions for land and marine operations for 

all units covered by the consolidated permit. 

FEDERAL PROGRAM APPLICABILITY 

6. These facilities shall comply with all requirements of U.S. Environmental Protection 

Agency (EPA) Regulations on Standards of Performance for New Stationary Sources 

promulgated for Storage Tanks in Title 40 Code of Federal Regulations Part 60 (40 CFR 

60), Subparts A, K, Ka, and Kb. The permit holder shall maintain a list showing the 

applicability of K, Ka, or Kb. 

7. These facilities shall comply with all requirements of EPA Regulations on NESHAPS in 

40 CFR 61, Subparts A, J, V, Y, and BB. 

OPERATIONAL CONDITIONS 

8. This terminal facility is authorized to store and load compounds according to the scenarios 

and controls described in Attachment B of this permit entitled "Paktank Corporation -

Approved Chemicals, Storage, and Loading Scenarios." Exemptions from Permitting, 

30 TAC Chapter 106, may be used to authorize a change in the storage and loading 

scenarios of Attachment B provided that the exemption claim is submitted to the TNRCC 

New Source Review Permits Division in Austin and all local pollution control agencies 

13 
P.15 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 5 

simultaneously widi a pennit amendment with the pennit review limited to that particular 

chemical(s). Storage and loading of chemicals which are not included on Attachment B 

is prohibited without amendment to this permit unless all of the following conditions are 

met: 

A. The new chemical has an equal or lower vapor pressure (at 100'F), an equal or lower 

vapor molecular weight, and an equal or higher published Effects Screening Level 

(ESL) value than a chemical already approved for handling on Attachment B. 

Acceptable ESL values for new chemicals are limited to tiiose specified in die most 

current published TNRCC Toxicology and Risk Assessment (TARA) ESL List or 

approved by the TNRCC TARA group. 

B. The new chemical shall not be (1) an inorganic compound or (2) a chemical containing 

sulfur or halogens unless die product has a vapor pressure less than 0.5 psia at 100 *F 

and does not require loading controls under any scenario on Attachment B. The new 

chemical must be handled with the same filling, witiidrawal, and pumping rate 

limitations and die same mediod of storage and loading controls as required for the 

approved chemical on Attachment B widi which it is compared. 

C. Notification shall be made widiin 15 calendar days after the first occurrence of storage 

or loading of each new chemical added to Attachment B by implementation of 

paragraphs A and B above. The notification shall include die name of the new 

chemical and die corresponding storage and loading scenarios. The notification shall 

be submitted in writing to the following offices: 

One copy to the TNRCC Houston Regional Office. 

One copy to die Harris County Pollution Control Department, Pasadena. 

One copy to the TNRCC Austin Office of Air Quality, New Source Review 

Permits Division. 

D. The new chemical shall be identified in the next permit amendment or renewal 

application for review and incorporation within die permit. Air dispersion modeling 

is not required to incorporate chemicals added under the authority of this special 

condition into Attachment B. 

9. Any chemical currently authorized for storage in a fixed-roof tank may also be stored in 

any tank equipped widi an IFR. Any chemical currently authorized for storage in an IFR 

tank may also be stored in a high pressure spherical storage tank. Any chemical may be 

stored in tanks smaller than those granted in the permit scenario. 

/4-
P.16 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 6 

10. This permit also audiorizes the storage and loading of any material consisting of a mixture 

of approved chemicals, a mixture containing chemicals added under the audiority of Special 

Condition No. 8, or chemicals mat meet all applicable requirements under exemptions from 

permitting, 30 TAC Chapter 106. Mixtures, as authorized here, shall be managed using die 

scenario of the component that is present in die highest percentage in the vapor phase. For 

mixtures that contain components in equal percents in the vapor phase but differ in 

requirements for storage and loading, die more stringent scenario will apply. In the situation 

diat the difference in percentage of die highest and second highest compounds is equal to or 

less than 10 percent, the mixture shall be handled according to the compound with the lowest 

ESL. Records shall be kept of the vapor phase percentage determinations for each mixture 

stored. 

11. This permit also authorizes the storage and loading of any material consisting of a mixture 

of approved chemicals. Any compound name mat is not listed on Attachment B shall be 

authorized for storage and loading if its chemical abstract number matches that of a 

compound already listed in Attachment B. Except as authorized under Special Condition 

No. 8, storage of odier chemicals is prohibited unless prior approval is obtained from die 

Executive Director of the TNRCC. It will not be necessary to obtain approval for chemicals 

previously approved for storage in a specific tank. A revised Table 7 shall be sent to the 

TNRCC Regional Office witiiin ten days of any change in service of these tanks. 

12. Flares shall be designed and operated in accordance with 40 CFR 60.18, including 

specifications of minimum heating value of die waste gas, maximum tip velocity, and pilot 

flame monitoring. If necessary to insure adequate combustion, sufficient fuel gas shall be 

added to make the gases combustible. An infrared or ultraviolet monitor is considered 

equivalent to a thermocouple for flame monitoring purposes. 

13. Issuance of this permit does not assure compliance with or constitute approval of marine 

vapor control systems pursuant to the requirements of the United States Coast Guard 

(USCG) which may have jurisdiction over the design and operation of such systems. The 

holder of this permit is advised to contact die USCG regarding diis matter. Within 60 days 

of obtaining certification from die USCG, die applicant shall send a copy of diis certification 

to the TNRCC Houston Regional Office. 

14. Emissions from barge loading operations shall be minimized by the use of a vapor collection 

system when loading all compounds which require vapor control under permitted conditions. 

The vapor collection system shall be operated and maintained at less than atmospheric 

conditions at the facility vapor collection point when authorized by USCG Regulations, 

46 CFR 154.800ff. Negative pressures are prohibited by this regulation during the loading 

15 
P.17 

SPECIAL CONDITIONS 

Pennit No. 466A 

Page 7 

of inerted vessels. All inerted U.S. flag vessels shall be certified leak-tight prior to loading 

as specified in 40 CFR 61 (NESHAPS Subpart BB). If negative pressure loading is possible 

under USCG regulations, the system pressure shall be monitored and recorded. A 

pressure/vacuum gauge shall be installed to verify a negative pressure of at least a one-inch 

water column. If die vacuum system should fail, the operator has one hour to correct the 

problem and restore the vacuum. Loading operations shall cease if die vacuum is not 

restored within one hour of failure. 

15. The following compounds (storage scenarios shown in Attachment B-3) must be maintained 

at a temperature less than or equal to those listed below. 

CAS 

Number 

75-07-0 

106-99-0 

107-00-6 

503-17-3 

822-35-3 

75-61-6 

109-93-3 

75-04-7 

540-67-0 

109-92-2 

513-35-9 

78-78-4 

Chemical Name 

Acetaldehyde 

Aviation Fuel (100 Octane) 

Aviation Gasoline 

1,3-Butadiene 

Butylene 

1-Butyne 

2-Butyne 

Cyclobutene 

Dibroraodifluoromethane 

Divinyl Edier 

Ediylamine 

Ethyl Methyl Ether 

Ethyl Vinyl Ether 

Isoamylene 

Isopentane 

Isoprene 

Control 

Temperature (°F) 

60 

85 

85 

48 

5 

70 

74 

25 

63 

55 

55 

40 

85 

88 

77 

40 

Storage Tank 

Type 

IFR 

IFR 

IFR 

IFR 

IFR 

Pressure 

IFR 

IFR 

IFR 

IFR 

IFR 

EFR 

IFR 

IFR 

IFR 

IFR 

lb 
P.18 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 8 

CAS 

Number 

75-31-0 

563-46-2 

563-45-1 

513-35-9 

107-31-3 

107-25-5 

591-93-5 

109-66-0 

627-20-3 

109-67-1 

75-56-9 

689-97-4 

Chemical Name 

Isopropylamine 

2 Metiiyl 1 Butene 

3 Methyl 1 Butene 

3 Methyl 1 Butyne 

2 Metiiyl 2 Butene 

Methyl Formate 

Methyl Isopropyl Ether 

Methyl Vinyl Etiier 

1,2-Pentadiene 

Pentane 

2-Pentene (trans) 

Pentenes 

1-Pentene 

Propylene Oxide 

Vinyl Acetylene 

Control 

Temperature (°F) 

55 

80 

56 

74 

88 

75 

78 

67 

66 

88 

50 

55 

55 

80 

33 

Storage Tank 

Type 

IFR 

IFR 

IFR 

IFR 

IFR 

IFR 

IFR 

Pressure 

IFR 

IFR 

IFR 

IFR 

IFR 

IFR 

IFR 

In die event diat a product is delivered to die facility at a temperature exceeding the 

represented reduced temperamre, the permit holder will have 72 hours to lower the product 

temperature. As long as the tank is under refrigeration during this 72-hour period, it will 

be considered to be in compliance widi die requirements in this paragraph. Records shall 

be kept of product delivery temperatures and die time taken to reduce the temperature to the 

required level. 

When in VOC service requiring temperature control, daily temperature readings shall be 

performed and recorded for all applicable tanks. 

I

1

* 
P.19 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 9 

HALOGENATED HYDROCARBON LOADING CONTROL REQUIREMENTS 

16. During loading of railcars and tanks trucks containing compounds requiring vapor control 

by the carbon adsorption system (CAS) as designated on Attachment B-2 (compounds noted 

with CARBON as the loading control device), all resulting emissions shall vent through 

the Station 20 lean oil adsorption unit and CAS consisting of at least two activated carbon 

canisters that are connected in series (Emission Point No. [EPN] CA-1). 

A. The CAS shall be sampled and recorded every fifteen minutes during loading of all 

halogenated compounds to determine breakthrough of VOC. The sampling point shall 

be at the outlet of the initial canister but before the inlet to the second or final 

polishing canister. Sampling shall be done during loading conditions reflecting 

maximum emissions to die CAS. 

B. The method of VOC sampling and analysis shall be by a non-dispersive infrared 

spectroscopy analyzer or a TNRCC-approved equivalent. On each day that sampling 

is required, die analyzer shall be calibrated prior to sampling at 0 ppmv ±10 percent 

and at 100 ppmv ±10 percent widi a certified gas mixture of the specific compound 

diat will be transferred utilizing the Station 20 lean oil adsorption unit and CAS as the 

emission control device. If two or more different products will be controlled by die 

Station 20 lean oil adsorption unit and CAS on die same day, prior to sampling the 

new compound die analyzer shall be re-calibrated at 0 ppmv ±10 percent and at 

100 ppmv ±10 percent using a certified gas mixture of the subsequent compound(s). 

C. Breakthrough shall be defined as a measured VOC concentration of 100 ppmv. When 

die condition of breakthrough of VOC from the initial saturation canister occurs, the 

waste gas flow shall be switched to die second canister immediately. Prior to any new 

loading event, a fresh canister shall be placed as die new final polishing canister. 

Sufficient new activated carbon canisters shall be maintained at die site to replace 

spent carbon canisters such diat replacements can performed prior to any new loading 

event. 

D. Records of die CAS monitoring maintained at die plant site shall include (but are not 

limited to) die following: 

(1) Sample time and date. 

(2) Monitoring results (ppmv). 

(3) Corrective action taken including die time and date of that action. 

(4) The compound and loading rate at the time of sampling. 

(5) Analyzer calibration records. 
P.20 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 10 

17. The CAS to be installed in series with the existing Station 20 lean oil adsorption unit, 

including the analyzer specified in Special Condition No. 16B, shall be fully operational 

no later than January 1, 1998. After the CAS is operational, but no later than 

January 1, 1998, Attachment C is void and all terminal operations are limited to die 

storage and loading scenarios of Attachment B. 

18. Any halogenated compound with a marine loading control requirement designated in 

Attachment B-2 as "CONTROL" cannot be handled by barge or ship until engineering 

specifications for a marine halogenated vapor control system have been submitted to and 

approved by the TNRCC. The proposed control technology must meet or exceed 

98 percent control efficiency. The marine halogenated vapor control system must be 

operational prior to loading any halogenated products that require marine vapor controls 

per Attachment B-2. 

HEXAMETHYLENE DIAMINE (HMD) LOADING CONTROL REQUIREMENTS 

19. All emissions resulting from HMD loading operations (land and marine based) shall be 

controlled by the SC-800 Water Scrubber. Water shall circulate through the scrubbing 

system such that all HMD loading emissions are controlled widi a minimum of 

98.3 percent efficiency. 

20. The minimum SC-800 water circulation rate that will ensure a 98.3 percent HMD control 

efficiency shall be established and documented during the initial stack emission testing 

performed in accordance widi Special Condition No. 23. The SC-800 water circulation 

rates shall be monitored and recorded during all HMD loading operations. 

21. The SC-800 scnibbing water shall be changed out after every 120,000 barrels of HMD 

loading throughput. 

TOLUENE-2.4-DIISOCYANATE (TDD CONTROL REQUIREMENTS 

22. The TDI is limited to storage in Pressure Tank T-800. All emissions from Tank T-800 

depressurizations shall be routed to the terminal's Marine Flare. Pressure Tank T-800 

shall not be depressurized during TDI loading operations. (12/97) 

\<\ 
P.21 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 11 

INITIAL DETERMINATION OF COMPLIANCE 

23. The holder of diis permit shall perform stack sampling and odier testing as required to 

establish the actual pattern and quantities of air contaminants being emitted into the 

atmosphere from the CAS (EPN CA-1) and the HMD Water Scrubber (EPN SC-800). The 

holder of this permit is responsible for providing sampling and testing facilities and 

conducting the sampling and testing operations at his expense. 

A. The TNRCC Houston Regional Office shall be contacted as soon as testing is 

scheduled, but not less dian 45 days prior to sampling to schedule a pretest meeting 

or meetings. 

The notice shall include: 

(1) Date for pretest meeting(s). 

(2) Date(s) sampling will occur. 

(3) Name of firm conducting sampling. 

(4) Type of sampling equipment to be used. 

(5) Mediod or procedure to be used in sampling. 

The purpose of die pretest meeting(s) is to review the necessary sampling and testing 

procedures, to provide the proper data forms for recording pertinent data, and to 

review the format procedures for submitting the test reports. 

A written proposed description of any deviation from sampling procedures specified 

in permit conditions or TNRCC or EPA sampling procedures shall be made available 

to die TNRCC prior to the pretest meeting. The TNRCC Regional Manager or the 

Manager of TNRCC Engineering Services Team shall approve or disapprove of any 

deviation from specified sampling procedures. 

Requests to waive testing for any pollutant specified in B of this condition shall be 

submitted to die TNRCC Office of Air Quality, New Source Review Permits Division. 

B. Air contaminants emitted from the CAS to be tested for include halogenated 

hydrocarbons. The SC-800 Water Scrubber shall be tested for HMD mass emissions 

and to demonstrate compliance widi a minimum 98.3 percent HMD control efficiency. 

C. Sampling for the CAS shall occur witiiin 60 days after initial CAS start-up and at such 

odier times as may be required by the Executive Director of the TNRCC. Sampling 

for the SC-800 Water Scrubber shall occur witiiin 60 days after initial start-up of 

ao 
P.22 

SPECIAL CONDITIONS 

Permit No. 466A 

Page 12 

controlled HMD loading operations and at such other times as may be required by the 

Executive Director of the TNRCC. Requests for additional time to perform sampling 

shall be submitted to the TNRCC Houston Regional Office. 

D. Loading shall occur at maximum operating/emission rates during stack emission 

testing. Primary operating parameters that enable determination of the maximum 

loading/emission rates shall be monitored and recorded during die stack tests. These 

parameters are to be determined at die pretest meeting(s). 

E. Three copies of the final sampling reports shall be forwarded to the TNRCC within 

30 days after sampling is completed. Sampling reports shall comply with the attached 

provisions of Chapter 14 of the TNRCC Sampling Procedures Manual. The reports 

shall be distributed as follows: 

One copy to the TNRCC Houston Regional Office. 

One copy to the Harris County Air Pollution Control Department, Pasadena. 

One copy to the TNRCC Austin Air Quality Enforcement, Engineering Services 

Section. 

EMISSION CALCULATION AND RECORDKEEPING REQUIREMENTS 

24. Daily and annual storage tank throughputs shall be recorded for every tank affected by diis 

permit. Daily and annual truck, railcar, barge, and ship loading throughputs shall be 

recorded. 

In addition, any tank filling, tank wididrawal, or loading operations that are performed 

under reduced hourly rates per Attachment B shall be recorded at die time they occur. For 

truck and railcar loading, a reduced rate is that which is permitted below 800 gallons per 

minute. For barge and ship loading, a reduced rate is that which is permitted below 

3,800 barrels per hour for chemicals stored in 80,000 barrel tanks and 2,000 barrels per 

hour for chemicals stored in smaller tanks. These records shall reflect the date and the 

actual rate of the filling, withdrawing, and/or loading operation of die specific compound. 

Also, me records shall show how the reduced rate was attained, i.e., restrictive orifice, 

design capacity of pump, etc. 

25. Facility-wide land-based emissions'Shall be calculated mondily. This must include storage 

tank emissions, all land-based loading emissions, flare emissions, and fugitive emissions. 

Total annual land-based emissions must be kept on a calendar year basis. 

ai 
SPECIAL CONDITIONS 

Permit No. 466A 

Page 13 

26. Marine loading emissions shall be calculated mondily. Total annual marine emissions must 

be kept on a calendar year basis. Records shall include materials loaded, throughputs, 

loading method, control method, VOC molecular weight, VOC monthly average 

temperature, VOC vapor pressure at the monthly average material temperature, and total 

tons of emissions. 

27. The following records shall be maintained in accordance with the requirements of General 

Condition No. 7 of tiiis pennit: 

A. Records describing die dates of inspection, seal integrity, and any corrective actions 

taken for all IFR seal inspections in accordance with Special Condition No. IC. 

B. A mondily emissions record in accordance with Special Condition No. IF. 

C. Records of all leaks detected during transfer operations and the subsequent repairs 

performed in accordance with Special Condition No. 3. 

D. Records of the fugitive emission leak detection and repair program in accordance with 

Special Condition No. 41. 

E. Records demonstrating how each new chemical meets all of the requirements for 

addition to Attachment B as established in paragraphs A and B of Special Condition 

No. 8. The record shall identify the name of the new chemical and the comparison 

chemical already approved for handling and shall list and compare the values of die 

vapor pressure (at 100' F), vapor molecular weight, and ESL of the new chemical to 

the chemical already approved for handling on Attachment B. The record shall 

include the storage and loading scenarios, the applicable Attachment (B-l, B-2, or 

B-3) for the new chemical, and die date on which die new chemical was first handled 

at die terminal. 

F. Records of all vapor phase percentage determinations for all mixtures stored in 

accordance with Special Condition No. 10. 

G. Records of all shore-side vacuum system repairs in accordance with Special Condition 

No. 14. 

H. Records of die product delivery temperature, the time taken to reduce the temperature 

to the required level, and the daily temperature readings for all applicable tanks in 

accordance with Special Condition No. 15. 

aa 
P.24 

SPECIAL CONDITIONS 

Pennit No. 466A 

Page 14 

I. Records of the CAS in accordance with Special Condition No. 16D. 

J. Records of the SC-800 scrubbing water circulation rates during all HMD loading 

operations in accordance with Special Condition No. 20. 

K. Records showing die cumulative HMD loading throughput and die dates of all SC-800 

scrubbing water replacements to demonstrate compliance with Special Condition 

No. 21. 

L. Records of all compounds handled by ship or barge for which marine loading controls 

are not required by Attachments B-2 or B-3, but are required by the current edition 

of 30 TAC Chapter 115 (Regulation V). 

Dated 1-2-98 

21 
Farm* No 486 M AAacflmanl B-1 Compound* Approved tor Storago n Faiod Roof Tar** Paftlar* Corporation. Approved ChomfcaK. Sloraga. *nd Loadng tcanarna 

STORAGE SCENARIO 

CHEMICAL 

ABSTRACT 

M4.I0-1 

lo»_.« 

m-l.-i 

1144.* 

H U M 

Ill-It-. 

SO 

AsirnCACio '"• " 

ACETAI.0OXIME 

A.fcTAMW* 

AI1:TANII.II>I. 

ACOTOR • / ACOREW BLEND 

ACONEWItR 

AC* ••KETONE 

ACTt£NE>4* 

ACM.ICACIO — 

AOIKMnULe 

ADMADI4AMME 

ADOGEMimi '" " 

AIOFIIYM. nxwE SOLUTION 

ALFfN. la 

ALFOLI 

ALfONK III4GC-10 

ALKANE l« 

ALKVL8EMENE 

ALKVL FOLYOLYCOSIDE SURFACTANT 

AUVL XYLENE 

ALKYLATE 14 

ALKYLATE teo 

ALKYLATE V 

ALKYLATE li t 

ALKYLATE loo 

AIJCYLATEJI 

ALKYLATE I I 

Al KYOTE M 

AIXYLATB t 

ALKVLATKH-IM. 

Al.riUM.MMriO.14 

AMINOCTUVL miANOLAMiNe 

AMMONIUM NITRATE' 

AMMONIUM SULFATE 

AMSCOSOLVIIUI 

AMYL ACETATE (ISO-) 

AMYL ALCOHOL<N) 

AMYl FHENOC*: 

ANETMOU " 

ANTHRACENE 

ANTHRAQUINONE- ' 

AMnOXIDAMTH 

AKHMA GLYCOSIDE ' 

ARCOIIfOLYOU 

ARCOSOLVFM ACETATE 

ARUMFFMATE ' ' 

ASPHALT 

AUTOMATMlUtr ~ " " 

" flM*. A2EUICACI0

 ,r " 

IBABASSUOLL 

BASE STOCK FALEOO. Il l (SEE 4M0)' 

BENZOFLEX MS FUSTIClZER ' 

BENZOWTIUU 

•CNZYLACtTATE " 

BKN m ALCOHOL 

DETA MCOUNEISEE toto FfCOUNE 

BICYCLOUBXYL 

•itd-miYuarYLimniAUTE OOF 

RiwrYANonim i rnir» 

•AROI SMF 

MAXIMUM MAXIMUM 

LOAMNO TANK nUtt C RAO. CAR 

RATI RATE L0ADINO LOAOfNO 

cammx 

•AROI 

LOAOfNO lAAOMO 

ca_n__-i cxuxiflU 

IIMI- I 

«4I4.S>.| 

niMa-t 

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" 1441-1 

"UST-4V-4 

— IM-I W 

W I M 

IIO-4I-* 

I1HW-* 

Vl-ll-l 

M7-4I-J 

i<* 14 
ParmiNo 4G6M Anacftmara 8-». Compound* Appro.art tor gioraga in Fwad Roof TanM P*lar* Corporation .Apprmad Chamcaaj. Storage and Loadng Soanarwa 

CHEMICAL 

ABSTRACT 

STORAGE SCENARIO 

TANK TANK SIZE IN M MLS 

FILL " ~ ' ' 

8 

lMl.10-1 

IO0|.J»-J' 

IIIM M 

Ml-44-0 

47M-.0-) 

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IM-44-* 

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111-444 

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I0II1-J 

mso-ii-t 

I4I-II-A 

• !-«*-» 

CORK OIL 

COTTONSEED OIL " 

CRCSYLATE SFENT CAUSTIC SOLUTION 

CRESYUCACID * 

CROTONOIL 

CROTONIC ACID (CIS) 

CROTONrtlULE (TRANS) " ~ 

CRUDE UOHT OIL 

CRUDE UMOMENE 

CRUDE MDI POLYMERIC 

CRUDE SULFATE TURPENTINE 

CUTTER STOCK 

CXI4M - LUBE OIL ADDITIVE ' 

CYCLE OIL 

CYCLOOOnECATRICNE. I.S.*. 

CYCUMIEXYL BENZENE 

CYCLOIIEXYL FEROXIOE 

CYCLOOCTADIENE (I.J) 

CYCLOOCTANE 

CYCLOOCTATETRAENM 1.1.9.?-) 

CYCLOFENTANOL 

CYCLOFENTANONE "~ ~ 

CYCLOFENT.LPEWTANE. I- " " " 

CYLESST1C ISM 

D LIMONENE 

DCI-4A - COR ROSIOM INHIBITOR NO «A 

DCPD-104 

DECAHYDRONAPMTHAlCNG(CIS) ' 

DECAHVDRONAPHTHALENE (TRANS)" ' " 

DECANAL, IDECANE 

DECANONE.1- " 

DECYL AlCOl ML (N) 

DECYL BENZENE 

DECYL NAPHTHALENE. I* 

DECYNE.IDETEROENT RANOI ALCOHOL - NEODOL 

DIISONOWVLAOI.ATE ••— 

MISCROCTYCADIPATC 

DIACETONE ALCOHOL "" 

DUUCYl DISULFIDES

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DUUCYLTHTHAUTE

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MALLVL MAI.EATE 

DIAMINOCYCI.OHSXANE (I.i-) 

MBASICESTERS 

DIBENZYl ETHER 

D«UTYi:rARarror r -

OWinYLMAL-UTE 

DUUTYL PHTHALATE 

DninviinACATr 

MCHCDROBOUENEM' — 

DiOILOROBENZENEl*-) 

OICMLOROETHYL ETHER, (l.i-1 

DtCVANOItUTENEfCIS) 

DICYCLMIEXYIAMINE 

DIESEL 

DIETHYL ADIPATE 

DIETHYL ANILINE 

Pagalo.}* 

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ParmiNo ««_-. AOacnmanl B-1. Compound* A«ipro»ad tor Sloraga «. Faad Root TarSt* Pafclar* Corporation • Approved Chanucato. Storag*. and Loaong 

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ABSTRACT 

1)1114* 

11140-1 

II1-4IJ 

lll-OI-l 

111-51-0 

50 

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DODECYLMERCAFTAN 

DOP 

OOWFROTH 

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01-11 (LT IX PARAFFIN A *•% WATER) 

DUTREX 111 - PROCESS/EXTENDER OIL 

DF. 100 

DF )UO0 

DF 100 

ECA I0I1IM 

ECA 10111 

ECA 10*17 

ECA 10*4* 

ECAISM1 

ECA 10477 » 

ECA MIM 

ECA 11*14 

ECA 11447 " • " 

ECAI1S04 

ECAllMS 

ECA DIM 

ECA "11710 M 

ECA I1MOC 

CCA 11741 " " ' • - "" 

ECA 11710 " 

ECA lilt * 

ECA tin t 

ECA 11104 (FUR. ADDITIVE) 

ECA 11*14 

ECA Illl * 

ECA 11710 

ECA 11711 LUBE ADDITIVE 

ECA 14101 

ECAI4SI4P 

ECAIJI7I 

ECA44-2 

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AtUdmanl 8-1. Compound* Approvad tar SloraganFmad Root Tank* Paktarti Corporation - Aeprovad Chan-Cato, Staraga. and L-a_an0 ioanarlDa 

CHEMICAL 

ABSTRACT 

NIIHHf . 

101-10-1 ' 

io7T:i4-i " 

II M M 

IIM5-4 ' 

""lfW«"" 

•*"ioHra~ 

U1M4-THEXONE 

HEXVLBENZENE 

IIEXYL CARBITOL 

HEXYL CELLOSOLVE 

HEXVUMME " 

KEXYLEWE GLYCOL 

KEXYLENE GLYCOL OUCETATE— 

so 

oO 

» i 

•"JWI.I 

IIMS.lt-1' 

—"—*— 

iron.*-

HMMM " 

- mn'' 

~H-n4' 

"•MM 

•r- • -..••- • 

. . . - _ 

ISOBUTVUC'ACID " " 

ISOOECYL ALCOHOL 

ISOMEfTVTAICOHOt 

ISOMONVTUCOHOC "" 

I-OOC7YTMCOHOL -

uoMwra w 

ISOMOrAMOtAMlNf "" 

ISO. R0m' 4 UETWYl BENZENE. 1-

ISOMWVUIVIIROXVUMM-: *•"" 

ttOMorvi>N-Mot<r.»" 

MYO-XOftV 

IET A 

IM 

KERO-IET FUEL GRADE 414 

STOAAOC SCENARIO 

TANK TANK SIZCINMBSU 

nu. 

RATE 

(BOLUIU U J 12 SB 11 

1.-00 

1.100 

l.MO 

1,100 

"Tt-»'~ 

J.--0"" 

ANNUAL 

TANK STORAOI 

THROUGHPUT TANK SfECIAL 

sue nuau 

IB 

10 

10 

to' 

"1" 

"Iff" 

lo10"! 

10 

» 

10 

T~ 

TB" 

10" 

-*' 1 

10 

1* 

« 

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'«'" 

Vi ' 

IB 

10 

4 

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"MOB-" 

l.MO*" 

"1,-dS"" 

l.MO 

T.-00 

l.MO 

1.M0" 

1 

I 

1" 

IS 

"IS 

IS" 

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Pago* of 14 
Parma No 466A AOaenmanl B-l. Compound* Approvad tor Storao* n Fbad Root Tank* PaMar* CorporaUon • Approved Cnanuoal*. Storaga. and Uadng 

STORAGE SCENARIO 

TANK SIZE IN MBBLS 

tllEMICAI. 

AllSlRAtT 

^ 

-£ 

nmillAI KAMI; 

LUBRIZOL 111 4* 

LUBRIZOI. Il l M 

LUBRIZOL 111 I*(ZINC DrTIIIOPMOSNUTEl 

LUBRIZOL 111 11 

LUBRIZOL 111 M' " " "" 

LUBRIZOL 111 •* 

LUBRIZOL III.*! 

LUBRIZOL 111 OO 

LUIR120C UI M " — 

LUBUZOClllTI 

LUBUZOCrill4 

LUBRIZOL II I ( I 

LUBRIZOL 111 •* 

LUBRIZOL 111 90 

LUBRIZOL II I t l 

LUBRIZOL 111»« 

LUBRIZOL 1115 

LUBRIZOL ll*S 

LUBRIZOL 11*10 

LUBRIZOL I It III 

LUBRIZOL lit lo 

LUBRIZOL 111 10 

LUBRIZOL 111 M 

I.IIRRIZm. It'll In 

LUBRIZOL Ill w 

LUBRIZOL III IS 

LUBRIZOL 111 It 

LUBRIZOL ITS I I " 

LUBRIZOL ITJ 10 

LUBRIZOL i n is --• 

LUBRIZOL 111 14 

LUBRIZOL II I 41 ' 

LUBRIZOL II I «* 

LUBRIZOL I M (SUCMIC ANHYDRIDE.""" 

LUBRJZO-IMOT 

LUBRIZOL IM-I " 

LUBRIZOL 1*1 IS ' 

LUBRIZOL Ill l ' 

LUBRIZOL 1114 " 

LUBRIZOL 1411N 

LUBRIZOL Miff " 

LUBRIZOL ISM" ' 

LUBRIZOL Ill l 

LUBRIZOL 1511 

LUBRIZOI un 

LUBRIZOL isno 

LUBRIZOL 11WC 

LUBRIZOL HIO 

LUBW20LUI-.' " 

LUBRIZOL HUB 

LUBUZaUM*" 

LUIUZOLHltW 

LUBRIZOL 1*40 

LUBRIZOL )*40A 

L0BUZ0L'I*4-C ' 

LUBRIZOL 1*1 

LU1R1Z0L 1*1 ' 

LUBRIZOL 4-0 

LU_M-0L'4MPogollefM 

co 

o 
Parma No 4«-s Attactimanl B-l: Campouvl* Approved tor Sloraga n Foiad Roof Tank* PaHar-i Carpcr-a_ow.Appro»adCl»amical». Slorap*. andLooang B<__naioa 

CHEMICAL 

ABSTRACT 

Miiuwr* 

STORAOE SCENARIO 

TANK TANK SIZE IN MBBLS 

fILL 

""""•" "*"" 

UV 

MAXIMUM 

LOA0040 tOAMNO TANK TRUCK KAIL CAR 

RATI RATE LOAMMO LOAOINO 

at_____u au_-___u oo-ccuu cottnaj. 

BAROf SMP 

LOAOINO LOAOP-O 

"•"M " rntfrinii 

LUBRIZOL 4»7oR 

LUBRIZOL 4*110 

lilBRIZOL 4WMA 

LUBRIZOL Uol 

LUBRIZOL HS " 

LUBRIZOL 1*1* 

LUBRIZOL (111 

LUBRIZOL til l 

LUBRIZOL U IB ' 

LUBRIZOL 4410" 

LUBRIZOI. -44* 

I.UBRIZM. 444IA 

LUBRIZOL alio 

LUBRIZOL *470i 

LUBRIZOL *414M 

LUBRIZOL 4414V 

LUBRIZOL -41! 

LUBRIZOL *411 

LUBRIZOL *4IIA 

LUBRIZOLAM " 

LUBRIZOL t4*M_T' 

LUBRIZOL U' 

LUBRIZOL ttllA ' 

LUBRIZOL M l 

LUBRIZOL tlUID 

LUBRIZOL tllO 

LUBRIZOL til l 

LUBRIZOL MM 

LUBRIZOL O-OD 

LUBRIZOL T1M0 "* 

LUBUZOL'TMSl— 

LUIRIZOLTMMLUBR1Z0LT1BITLUBRiZOLTSlS* 

LUBRIZOL 71715" 

LUBRIZOL 7S7IO 

LUBRIZOL'THIS " 

LUBRIZOL Tint 

LUBRIZOL 74" 

LUBRIZOI 7451* " 

LUBRIZOL 74711 " 

LUBRIZOL 74711" 

LUBRIZOL MTU 

LUBRIZOL 14IIB 

LUBRIZOL 74111 

LUBRIZOL 74110 

LUBRIZOL T4H»" 

LUBiuzornttoLUBUZ0L74NI ' 

LUBRUOCMX 

LUBRO0CT1HILUSR1Z0C.MJTM 

LUBRIZOL TASA" 

LUBRIZOL 7USC 

LUBRIZOL TSI4 

LUBRIZOL 7S74B " 

LUBRIZOI 11140 

LUBRIZOL 7SI4II 

LUBRIZOI. 71741 ' 

P*0*l3cf24 

"• 

co 
Parm* No 464A AtlaciwianlB-t: Compound* /^provad tar Sioraga *i Fbad Roof Tank* Paktank Corporation . Approvad Chamlea*-. J-oraga. and Lcad-V Seananoa 

STORAGE SCENARIO 

TANK SIZE IN MBBIJ 

CHEMICAL 

ABSTRACT 

ruruiCAi NAUF 

w 

LUBRIZOL Mil 

LUBRIZOL 1114 

LUBRIZOL Illl ' 

LUBRIZOL HUB 

LUBRIZOL 1HIC 

LUBRIZOL IIIIN 

LUBRIZOL TIIIS 

LUBRIZOL 111*1 

LUBRIZOL TWO 

LUBRIZOL 7*01 

LUBRIZOL Will 

LUBRIZOL liwl 

LUBRIZOL IIVIC 

LUBRIZOL I1WC 

UBRIZOI. II1S 

I.IIORIZOI. IMl* 

LURRIZOL IIUIC 

LUBRIZOI IIOIF 

LUBRIZOL HOT 

LUBRIZOI. IM7A 

LUBRIZOL II IB 

LUBRIZOL IISSK 

LUBRIZOL 1*441' 

LUBRIZOL 1157 

LUBRIZOL MIS 

LUBRIZOL 1170 

LUBRIZOL II10A 

LUBRIZOL Mil 

LUBRIZOL II7IA 

UBRIZOI. HUB 

LUBRIZOL I M 

LUBRIZOL 11101 

LUBRIZOL Ill l ' 

LUBRIZOI. IIIIA 

LUBRIZOL IIIIC 

LUBRIZOL" HlID 

LUBRIZOL Mill ' 

LUBRIZOL MHZ 

LUBRIZOL IW1 

LUBRIZOL IM 

LUBRIZOL -»S1 

LUBRIZOL W1IY 

LUBRIZOL IMO 

LUBRIZOL IMOA 

LUBRIZOL* 10 

LUBRIZOL •» » " 

LUBUZ0L..U -

LOMUZOLt)}!" 

LUBUZOL'MMT 

LUBRIZOL Al> ~ 

-U>MZ£0--4 ) 

LUBBJZOTASMM 

anmacasu • 

IVtUZOCAUMt 

UIBR-HMTA-OM 

LUiRlZOLlM"" ' 

(

LUBRIZOL BBS. " ' 

LUBRIZOL BBE4 

LUBRIZOL IHHVY AUCYt BENZENE) 

Pagal.of.4 

co 

ro 
Parma No: 4MA ARactMianl B-l: Compound* Approvad tar Sloraga n Fu d Root Tar** Paktar* Corporation -Approval CfarMcaa. SMraga. and Loadnt leananaa 

STORAOI SCENARIO 

TANK •_-_ IN M aai J 

CHEMICAL 

ABSTRACT 

"lllt-ll-l 

lilt-14-4 

o-ira 

TOMf-l 

llt-M-l 

'ITI-tl-S 

nifMiroi my. 

-tETHVTOCTANE. V " 

METHYL OCTANE. 4. " — ' 

METHYL P ENTAMETWYUNE DIAMINE (M 

METHVL~»ENTANOIC ACO-T*-"" 

wnwimiDmE.v 

-441)11-0 

141-41-1 

•l-io-l 

IIIU-U-I 

TM4-1 

10*-01-] 

""IIWI 

METHYL SALICYLATE 

METHYL SULFOLANE 

METHYLNITROBENZENE |>.) 

METHYUITERJDINE..1) 

METHYU1-M-ETHYLANIUNE 

MET01ACHLOR TECHNICAL. HERBICIDE' 

MINERAL SPIRITS 

MONOCTHANOIAMINE 

MPOKX-OLYCOL 

MM QUICK CURE-KERMTI 

NISainrOROflNISH 

NAPHTHALENE 

NAPHTHA. COAL TAR (DOT) 

NAPHTHA. MINERAL SPIRITS 

NAPHTHA SOLVENT 

NAPHTHENIC'ACIO 

NAPTHENIC LUBE OIL 

NAPTHEN1C VL * <ML 

NECT0N1I 

NECTON7I ..... . 

NEOCENE 1014 

NEOCENE 14/14/11 "DtEHHS— 

NEOD_NE(R>IOIl ALPHAOLEFIN" "'" 

NE00ENEfll)llll1NTCWIA["0_enN 

NEOOENE(R| 11/1114OLEFIN

 -

NE0D0L '"""' *"-

NEOO0C1l7fl 

NEODOCtr ~ 

NE000L~4i-1T 

"" NEOMLft)li'(-HEU.) 

NEOML'(t> I M J MOO-TR 

NEOFUX* ~'"' 

NEOfENTANOICAnO 

NEO-PEMTYL GLYCOL SUJUY 

NEUTRAL LUBE OIL IM 

NEUTRAL OIL SOO 

NEUTRAL 00 , 100 

NUITMIYOL'11-14" — 

NITRO I.I XYLENE. 4-

NTTROmiANI 

NmOOENEIRmiZEf - • 

NITROGEN SOLUTION 

NmoPROfANE(l) 

NmonwANiR.)" 

Nm-DTDOlDfZV 

•"IM-IW 

'"iri'44-r 

ui-M-r 

•vr-ux- w-urmYrFvuoaooNrNorowr 

NONANI 

MONANDq-f 

171I4-M-I"" NONDiri' =Jt USC K 

mOWONirSURFACTANT LZ-M ""' 

lOir-Tn-TNONVt'RDJZENE 

llll41M"fN0NVl'H<EN0l 

1NONVNE.I. -

Pag* 17 of 24 

co 

co 
Parmt No. Altacnmant B-l Compound* Approvod lor Storag* •» Ftaad Roof Tank* Paktank CarparaHon • Approvad Cnamica-t. Starao*. and laaang 

BTORAOI SCENARIO 

TANK IIZR IN M II U 

MIEMK'AL 

ABSTRACT 

1II4-.II.4 

IIW-K.I 

411-M4 

ISt-41-4 

1-4-17-0 

PAWOWNYl'mENOf 

•/ PARANOX IS. ZOOP O R INHIB. LOA 

PARANOX14 ••• . 

* FAtAKOXIM '. 

_ *MANDril-- 0 * - •-.— ~ 

' "PA-APOD II (STOCK I4H); 

| MWOC7JJ 0

 u 

"fPARAPOTIMO 

PARAQUAT 

IPAJWT O 1100 ' 

(TffMIIAI NAME 

OLEFINS C.II.14 

OLEFINS CU-ii" 

OLEFINS CZO-M ' 

OLEFINS C:j4-tf-

-L-FTNSC-10 

OLEFINS C-t-ll BLEND 

OLEFINS C* 7 

"M__F1NIC*T— 

OLEFINS C-4-I-I0" 

outrmrc-M"— 

OLEFINS C l 

OLEFINS CMO 

OLEFINS C-l-14 

OLEFINS C-i-* 

OLOA-.lt 

OLOA-11* 

ORfllEX T«t 

OXIOIZEO ASPHALT CUTUACK 

OXO ALCOHOL 

f METHYL BRNZCNI 

*0IISOPROPYL BENZENE 

* ETHYL TOLUENE 

rPtlENETIOINE 

f TOLUALOENYOE 

PALE OIL 1400 

PALI OIL IIS (1100) 

PALE OIL C. TEXACO Ian 

PALI OIL C. TEXACO 110 

PAL* ofL'flvrrto) IOIMMO••— 

PAU0ICMM"" 

PALM KERNEL OIL ~ " 

PALM OH " 

PALM STEARINE (PAG)" 

PAM - ' " " ' 

PA04"~ 

PARADYNE all - IN HVY AROMATIC SOLVENT 

PARAFFIN E' 

PARAFFINF(HEAVY) "" 

PARAFFIN (NTTRM-DIATEl STREAM 

PARAFFIN WAX 

PARAFFINS. CIO-11 

PARAFFINSTCRUDE CIA-It 

PARAFFINS. NORMAL. CUM I 

[PARAFFINS. NORMAL. ClO-lo 

PARAFFINS, NORMAL. CI1I4 .'"•' 

PARAFFINS. NORMAL. CI4.IP 

PARAFFIN-. NORMAL. CIA-IB 

FARAHIN ' 

nsxaoa 

P«0*IBotZ4 

co 
PamuINo 466-. AtlacPmanl B-1: Compound* Approvad tor Storapa in Farad Roof Tanka Pak-ank Carpenj-on - Approved Chamlcal*. Sloraga. and Uackng loananoa 

niEMICAL 

ABSIRAIT 

STORAOE SCENARIO 

TANK TANK SIZE IN M BBU 

FILL -*«—• — 

7|.«M 

Ill-M-t 

2 111)11-1 

llllll l 

ni_,MIIAI flAME 

REFORMER P-ED 

REFRIGERATION OIL • PENNZOIL 

RERUN M POLYMERS 

RERUN *0 POLYMERS " 

RESIDUAL FUEL OIL 

RESIDUAL'FUEL'OILtM 

__3rouALruELTJn.nl 

RESOrOIL - MISCELLANEOUS 

KESMOIL'-O 

ROIMUUI0 " 

RO WO FLUID ' ~ " 

SAFFLOWER OIL " 

SAYTEX 101.101E FUME RETARDANT 

BUTYL ALCOHOL 

BUTYL BENZENE 

SECONOARV BUTYL "ALCOHOL" 

SHELL SOL 

SIIF • 1001 (MOBIL) 

SHF-41 ' 

SHF-41. LURE "00."" 

Sllf-ll. LUBE BASE STOCK ' 

SODIUM ALUMfNATE ' 

SOOfUM'CARMNATf 

SODIUM CR-toxlDES"- PHEOXIDES 

SODIUM CRBSYLATE SOLUTION 

SODIUM HYOROXIOI (LIQUID) 

SODIUM UONOSULPONAT1 

S4NNUM SULFIDE SOLUTION 

SOOIUM SULFIDE WASTT 

SOMUM THIOCYANATE (>SW| IN WATER 

SOPTANOL-1* 

SOLVENT lot 

SOLVENT JJ ~ 

SOLV-MTUf 

-OtVEHTJIf" 

IOLVESSO "" 

SOLVE-SO IW 

SOBJITDL' 

TANK TRUCK 

MAXIMUM 

LOAOINO 

RATH 

tfiU-l 

l.fOO 

" I.t-tf 

i.too 

'" i.too 

~XK»~ 

—rw*- -

SOVBEXNTlir 

JPINDLS 0)1-MISCELLANEOUS 

-TANCffHMT 

sTW-rnaoc-DOAsoii" 

«4J-4M JnUBENE(di) 

ISTOCK 10] 

STOCK I0S-LUBE OIL 

"TU44M' 

•wwr 

" WM H 

TM44M 

sracri rt VLUIB OILIASI jmcr -

rncrs-*runf IASVSTOCK 

STOCK ilt. LUW RASE ITOCK" 

SULFONIC AtKYUTt 

SULFURIC ACID 

SULFURIC ACES M U (UZK). 

sucFuurAemttAMK 

suLFUucACtor 

SULFURIC ACID «!« ' 

SULFURIC ACID H S " 

(

SULFURIC ACID, SPENT 

SUNTHENIHI 

SURSOIIW 

SUB SOI IM 

Pag* }1 of 24 

co 

in 
Parmt No. 46b. Anaotmant B-l: Compound* Approved tar Storaga m Ftaad Root Tank* Paktank Corporatkin . Approvad Chamroaai. SHraga. and Loartng 

CHEMICAL 

ABSTRACT 

STORAGE SCENARIO 

TANK TANK SIZE IN MBBLS 

flU.

 J "• 

lil 

•SSM 

4-0-11-1 

I04-15-1 

101-11* 

IMM-I*.* 

ttt-so-s 

mr-st-r 

111-14-1 

imnu 

Jit-iu 

M-41-4 " 

rH-MH"AI NAMF 

TLA 1*0) - -

TLA 1101 

TLA 1101 

TLA-IWI 

TLA-1400 

TLA-1S0O 

TLA1404A 

TU-1MTA " 

KA-U1A " " 

TLA-414 -• " 

TLA.J1S 

TIA-HS" 

T1A-454A 

TLA-tSt.CllII 

TLA 411 

TtA-47* 

n_A-ttl'.C74ll ' 

TLA4IIA ' 

T_A4llC 

TLA4M 

TLA-IMS 

TLA-TTvO 

T0LUIDMC.O-. 

TOI.UNITRIL-. 1-

TOPPED POLYMER St 

M M I PHENYL PROPENAL" " 

TRANSFORMER OIL • MISCELLANEOUS 

TRIARYT PHOSPHATE 

TRIBinYlAMINB 

nuOKCANAI., ITRIDECANE 

TRIDECANOL(I-) 

TRJOeCENE. ITRimUNOLAMINE LOW FREEZING' 

TRIETHYL PHOSPHATE " ' 

TRIETHYLENEGYLCOL 

TwrrHYLENrrrnuwrnr " 

TRlUNOIEUICID-)' 

TR1METHYLT.1 PENTAN-DKmT13.V^"" 

mM-THYl BENZENE. OW " 

TRIMETHYL lENZOfCO.Tl-r 

TRAIETHYriENZLNI. ll,l » 

RAROC SMF 

MAXIMUM MAXIMUM 

LOAMNO LOAOINO TANK TRUCK RAILCAR 

RATI RATE LOAOINO LOAOINO 

Canaan cmrRnu 

•ARC* 

LOAOINO 

SMF 

LOAOMO 

' III-44-T 

H1M M 

I741-S4-7 

TRIMSTWVlTOBCAHI^nTr 

TUMEIHYL HEXANE."(l.l.r>'" 

TUMETHYl HEXANE. (Z.J.J-J' 

TWMETHYlHEXANlttT;*-)-

TlUMETWLH-XAN-raiin'" " 

TWMBTWlHO-ANVfl.TC. 

lUM-TmrHEXANCTDTI 

TUFROFVUNIOLYCOC 

TUFP1044I 

TURFOfTMr 

TXIB 

UCANI ALKYLATE 

UlTRKWIIOt P0TXI(_rC0UUONT~' 

UNDECANAV !• 

UNDECANI 

UND-CYl BEMZfNT 

UREA-AMMONIUM MTRATt SOLUTION 

Papa 7 ) of >4 

Tl 

CO 
Parma No 466A Aftacfananl B-2. Compound* Apr WStorapan mtarnal Floawig Root Tark* Pakiar-i Corporation * Appronad CftamcaJ go. and LoaoVig Soo 

CHEMICAL 

ABSTRACT 

STORAGE SCENARIO 

TANK TANK SIZE IN MBBLS 

WITHDRAWAL 

£ 

lOS-SLT 

I0H4-7 

'4744-1 

" -TS-lt-S 

" " IU-J44 

— I0J.IT-I 

1*7.114 ' 

'S7-04.T' 

414-114 

~l*04«> 

MI7 1 

100-51-7 

II-41-I 

M-II4 

I40-44-7 

IM-**4' 

74-»7.J 

T4-4J.J 

lll-U-4" 

"in-14-l 

I41-*t-l 

41I-II-* 

1*1-14-7 

" M1I4-7 

"-|0MJ.ff 

. IM-TM 

' 104-744 

" IM40-1 

*474I4}4 

54-11.1 

"lll-U".-

107.1*4 

" IMSO-T 

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~ST40 — 

—IIMM — 

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ACETAL 

ACETIC ANYHDRIDE" 

ACETONE • — 

ACETONE CYANOHYDIUN"' 

ACETYLACETONE 

AaYlONITUU 

ALKENYUUCCINIC ANHYDUDT 

ALKYLATE 

ALLYL ALCOHOL ' 

ALLVUSOTMOCYANATE 

AMYL ACETATE, (as) ' " 

AMsotr — 

ARALDITIGZ4MN4* 

ARCONOL 

AROMATIC loo (EXXON) 

BENZAL CHLORIDE 

BENZALOEHYDE 

BENZENE 

BENZOYL CHLORIDE 

BENZYL CHLORIDE 

BETA HCOLINE (SEE 4070 PICOUNE) 

BEOMOCHLOROMETHANE 

BUTANONE.1: "• 

BUTYL ACETATE. 

BUTYL'ACETATE. 1-"

 _ 

BUTYLCARBTTOL " 

BUTYL ETHER ' - ' " 

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