# Bioassays of 

# Florida Power Corporation Crystal River Citrus County NPDES #FL0036366 Sampled February 2, 2004

July 2004

Biology Section Bureau of Laboratories Division of Resource Asses sment and Management Quality Manual No. 870346G NELAC Certification No. E31780

## Florid a Powe r Co rpo r ation Crystal River, 15760 Po we r Line Road, Crystal River, Citrus Cou n ty, Florid a, NPDES #FL0036 3 66. Effluent sample s fo r thi s facility were colle cted on February 2, 2004.



# Introduction The Flo r ida P o we r Co rp ora t ion's Crystal River fa cility is an ele c tri c power ge ne ra ting plant. The facility con s ists of five generating u n its; howev er, onl y two units, Unit 4 and Unit 5, both fossil fuel-fire d , are under NPDE S permit FL0 0363 66. The s e two units h a ve a total nameplate ratin g of 1390 M W . Th e permitted di scharge rate for ea ch unit i s 44 million g a llon s per d a y (MGD). The averag e daily flow (ADF ), base d on the Disch a rg e M onitorin g Re p o rts fro m Nov e mbe r 200 2- De cemb er 2 0 03 from Unit 4 wa s 1.90 M G D (Outfall D-074 ). The A D F for Unit 5 wa s 1.86 MG D (Outfall D-075). The wastewater treatment process at the facility consi s ts of screening and chlo rinatio n o f the cooling

- towe r blo w do wn (a s ne ede d) and retenti on of wa stewater for solid s settling in the coal an d ash

- pile runoff co llection p ond s. In general, chlorin e is ap p lied on a daily basi s to one of the two co oling towers serving Un its 4 and 5. Treat ed effluent is discha rge d in to the Class III Marine Waters of the Gulf of Mexi co. The facility also has three power generating units. Unit s 1 and 2 are fossil fuel-fired u n its and Un it 3 is a nu clea r fuel-fired u n it. These three units are mon i tored un de r NPDES pe rm it FL00001 59 (facility information provid ed by Melissa Gunter, F D E P , Southwest Distri ct, Tam pa).

The bioa ssay sample wa s colle cted fro m Outfall D-0 75 (Unit 5) si nce the cooli ng-to we r blo w do wn from Unit 5 was chlori nate d durin g the morni ng of the sampli ng e v ent.



# Methods Sample s we re colle cted from the NPDE S samplin g p o int by Melissa Gunte r (F DEP, Southwest Distri ct, Tam pa) follo wing DEP-SOP-00 1/01 FS 2400 Waste w ate r Sampling. All DEP SOP’s a r e available on t he we b at: http://www.flo r id adep.o r g/lab s /qa/sop s .htm

. The toxicity and algal g r o w th potential tests di sc usse d in this repo rt were pe rform ed followi ng internal DEP SOP’s TA07_ 03,TA07_ 04, and TA08 _01 through TA0 8_06. All internal DEP SOP’s are availa ble on the we b at: http://www.fl orida dep.o r g/l abs/ c gi-bin/sop/bio s op.a s p

.



# Toxicit y Test Results Test s we re p e rform ed Fe b r ua ry 3 - 5, 2004.

Am ericam ysi s bahi a 48-hr acute scree n i ng bioa ssay – Not Toxic; LC 50 

## > 100%, 0% mortality in 100% sam p l e at 48 hours

Menidia b e ryl lina 48-hr a c u t e screeni ng bioa ssay – Not Toxic; LC 50 

## > 100%, 0% mortality in 100% sam p l e at 48 hours

See Table 1 f o r bioa ssay b ench sh eets.



# Algal Gro w t h Potent ial The effluent AGP was 4.5 1 mg dry wt/L of Dunali e lla tertiole cta. Nu trient data su gge sts that the effluent is nitrogen -limited, and there is n o evi den ce of growth in hibi tion. Rasch k e and Shultz found that Algal Gro w th P o tential (AGP ) val ues a bov e 10.0 mg dry weight/L re prese n t a “problem ” thresh old for ma rine receiving waters, implying nutrie n t enrichme n t (pe r so nal
comm uni cati on with Ron Ra schke US EPA Region 4 1987).



# 2

## See Table 2 f o r AGP re sult s.



# Chemistr y Results Total re sidu al chlori ne an d total ammoni a were not de tected in the bioa ssay sam p le in the laboratory. The total amm onia con c entration in t he sample p r e s erved for che m i c al an alysi s wa s 0.043 mg/L. Based o n the pH, salinity, and tempe r at ure of the effluent at the time of sampl e colle ction, the effluent unio n ize d ammo n i a con c e n trati on wa s 0.01 mg/L.
The effluent concentration of copper (3.97 μg /L) exceeded the Class III Marine Quality Criteri on (See Tabl e 3, 62-30 2.530 (24) F.A.C.).

Aluminum and iron were detected in the effluent sam p les at level s that complied with Class III Ma r i ne C r iter ia

.
See Table 3 f o r re sult s of analytes dete c ted in the effluent.
See Appen di x 1 for a com p lete list of ch emical a nalyses pe rform e d

.



# Conclusion Effluent samp les colle cted from this fa cility on F ebru a ry 2, 2004 did not sho w un a c ceptabl e acute toxicity to eith er test spe c ie s duri ng the 4 8 -ho u r bi oa ssay tests. The effluent AGP result wa s less than the "pro blem” thresho l d for marin e receiving waters. Th e effluent con c e n tra t ion of copp er (3.97 μg/L) exc eeded the Clas s III Marine Quality Criterion.



# Literature Cited Ra schke, R. L. and D. A. Schultz. 198 7. The use of the algal gro w th potential test for data
asse ssm ent. J. Wat. Poll. Cont. Fed. 5 9 (4 ): 222-2 2 7.



# 3Table 1.Facility:Florida PowerCorporationCrystal RiverNPDES #:FL0036366FacilityType:IndustrialAnalysts:Christa A.PieriniLocation:15760PowerLine Road,CrystalRiverContact/District:M.Gunter, T.Falkner/SouthwestPower PlantSarah PrichardJoshua AyresCounty:CitrusTest type:staticacutescreenScott AndreeJamesDanielsSampleCollection Date:2/2/2004Time:1205#tests:2ReceivingWater:GulfofMexicoMarshallFairclothTestBeginningDate:2/3/2004Time:1500ChlorinationType:chlorinatedClass III marineTest EndingDate:2/5/2004Time:1315FDEP SOP#:TA07_01/02Page1of1Reviewer:Julie EspyOrganism:AmericamysisbahiaLifestage:5 daysAFeeding:Artemia(mysid)Chambersize:1000 mlFood Batch #:0194025GJobnumber:Sample/DiluentSURVIVAL# AlivepHCTemperature (°C)Diss. Oxygen(mg/L)DConductivitysamplenumber:ConcentrationsVolume(mL)0hr24hr48hr0 hour24 hour48hour0hour24hour48hour0hour24hour48 hour0hour48hourControlA0/5005558.28.18.124.024.224.06.96.06.441.245.0ControlB0/5005558.28.18.124.024.324.26.75.75.843.745.6ControlC0/5005558.28.18.124.024.024.86.55.25.844.446.6ControlD0/5005558.28.18.124.024.524.06.45.65.944.545.0100%A500/05558.38.18.024.024.024.27.15.86.443.145.5Total Residual CL2mg/LMethod100%B500/05558.38.18.024.024.124.77.15.96.042.946.5Field:notmeasured-100%C500/05558.38.18.024.024.024.06.66.06.344.046.2Lab:<0.03Hach100%D500/05558.38.18.024.024.124.16.76.06.343.945.4Control water(NSW):<0.03HachAOrganismsfed priortotestand daily.AmmoniaTotal (mg/L)Unionized (mg/L)Organism:MenidiaberyllinaLifestage:13 daysBFeeding:ArtemiaControl water (NSW):<0.017<0.017(fish)Chambersize:1000 mLFood Batch #:0194025G100% Sample:<0.068<0.068Sample/DiluentSURVIVAL# AlivepHCTemperature (°C)Diss. Oxygen(mg/L)DConductivityConcentrationsVolume(mL)0hr24hr48hr0 hour24 hour48hour0hour24hour48hour0hour24hour48 hour0hour48hourAlk&HardnessAlkalinity(mg/L) Hardness(mg/L)ControlA0/5005558.38.28.124.125.125.66.85.96.343.346.2Control water (NSW):132-ControlB0/5005558.38.28.124.024.925.16.85.86.543.146.4100% Sample:158-ControlC0/5005558.38.28.124.224.924.46.85.96.444.045.9ControlD0/5005558.38.28.124.024.824.86.76.06.543.945.8Percent100%A500/05558.28.18.124.125.125.46.76.06.443.342.40%100%B500/05558.28.18.124.424.924.96.86.06.542.245.40%100 %C500/05558.28.18.124.024.824.26.86.06.543.945.40%100%D500/05558.28.18.124.224.324.46.76.06.544.445.30%BOrganismsfedprior totesting.CTemperatures ofroomand testincubatorwerecontinuouslyrecordedona stripchart recorder.pptDConductivityvalueis uncorrectedmmhos/cm.29.2RoomTemperaturerangeforthetestperiodwas 23.5-24.5°C.29.1Incubator#3temperature range forthetestperiodwas23.0 - 25.0°C.ESalinitybasedon temperatureandconductivity.LightIntensityduringthetestwas50-100footcandles.FNSW(Control water)wasdiluted withwellwaterfrom32 ppt to29.2Photoperiodduringthetestwas16hoursoflight: 8hoursofdark.Datarecorded duringthe 48-houracutescreeningbioassaysofa sampleofeffluent from theFloridaPowerCorporation CrystalRiverPower Plant,15760Power Line Road,CrystalRiver,CitrusCounty, Florida,NPDES# FL0036366,performed from 3 to5February2004.DataTranscriptionVerificationdate: 4/09/04by:CathyOaks/JamesDanielsTLH-2004-02-03-01731735100 %sample:FControlwater(NSW):LIMSMortalityESalinityControlwater(fish):Controlwater(mysid):100%(mysid):100 %(fish):4

### Ta bl e 2 . M eas ured al g al g row t h potenti a l ( AG P ) and rati os

of total s o l uble nitr o g en to ortho-phos phate and total nitr o g en to tot a l phos phate for the s a mple of effluent c o l l ec ted fr om F l orida Pow e r C o rporation C r y

s t

al R i v e r Pow e r Plant on F ebruary 2, 2004.

Lo catio n A G P (m easured) In o r g a nic N : P ratio T o t al N : P ratio

Ef f l uent Sam p l e s 4 .51 4 .69 7 .33



# 5

## Ta b l e 3

. E ffluent limits
, Clas s III Cr ite r ia and c hem ic al da ta fr om s a m p les c o l l ec ted fr om th e F l or

ida P o wer Cor por a t

ion Cr y

s t

al Riv e r

P o wer P

l ant s a mpled on F e b r uar y 2, 2004

.
Flo r id a Po w e r Co rp orat io n Cry s tal R i v e r P o w e r P l a n t Class III M a rin e St d s E ffl u e nt Li mi ts E f f l ue nt Samp les

Alu m inum ≤ 1500 - 1 1 1 Ar senic ≤ 50 - 2 9 U Cad m i u m ≤ 9.3 - 0. 25 U Ca l c i u m (m g / L ) - - 3 5 9 Chrom i um
- III - - 6 U Cop per ≤ 3.7 - 3

. 97 Ir on ≤ 300 - 1 4 0 Lea d ≤ 8.5 - 0

. 5 U Ma gnes ium ( m g/ L) - - 1 140 Ni ck el ≤ 8.3 - 6 2 U Sel enium ≤ 71 - 1 6 U Silv er ≤ 2.3 - 0

. 2 U Zi n c ≤ 86 - 2 7 U

T D S - - 27 300 T S S - - 8 I O r t ho- pho s phate - - 0. 013 T o t a l Phosphor u s - - 0. 072 Am m onia - - 0. 043 Uni oniz e d Am m o nia - - 0. 01 c Nitrate+Ni tr ite - - 0. 018 T o t a l Kj eld ahl Nit r ogen - - 0

. 51 O r g anic Nitr ogen - - 0. 47 c T o t a l Nitr o gen - - 0. 53 c T u rbidity - - 3 A

Diss olved O x y g e n ( m g/ L) ≥ 4.0 s - 7

. 4 pH ( S .U.) 6.5 - 8.5 s 6 .5 - 8.5 8 .2 Con duc tiv i ty ( u m hos /c m ) - - 45 345 T e m per atu r e ( C ) - - 2 9 .4 B O D (m g / L ) - - 0

. 5 9 A I B O D (m g / L ) - - 0

. 4 6 A I O il and G r eas e (m g/l) ≤ 5 - 0.9 2 IV Hardnes s ( m g/L) - - 559 0.9 c AGP ( m g Dr y W t/ L) - - 4. 51 A Chl o r i ne ( 1 00% sam p le lab) ≤ 0.01 - ≤ 0

. 03 U

Val ue ex ceeds th e Class III M a r i ne W a ter Quality Cr iter ia A - Value r epor te d is the m ean of tw o or m o r e dete r m i na tions I - V a lue r e por ted is bet w een t he labo r a tor y m e tho d detection lim it and the lab o r a tory pr ac t i c a l q uantita t ion lim it U - Mater i al anal y z ed f o r but n o t dete c ted; v a lue r e por ted is the m i nim u m det ec tion lim it V - Analy t e w a s d e tec t e d in bo th s a m p le an d m e th od blan k

s
- Single s a m p le G e neral P h y s ica l an d Ch emi cal Pa ramet e rs Me t a l s ( μ g /L u n less o t h e rw is e n o t e d )

Nutrients ( m g /L )



# 6

### A ppe ndi x 1

. C h e m i cal A n al y s es pe r f or me d on the e f fl ue nt fr om the F l o r i d a P o w e r Co r p o r atio n Cry s t a l Riv e r P o w e r P l ant sa mpled on Fe bruary 2, 20 04

.

DAT E SAMPLE D FI ELD ID ANAL Y S I S G R O U P C O M PO NEN T RE SULT UNI T S RE MAR K MD L P Q L 2 / 2 / 2 0 0 4 13 :15 D -0C0 B i o-B O D B i o ch em i c al Oxy g en De m and -5 Da y 1 .1 m g /L 2 / 2 / 2 0 0 4 13 :15 D -0C0 B i o-B O D B i o ch em i c al Oxy g en De m and -5 Da y , N-Inhi b 1 .3 m g /L 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Me ta ls

- W a t er C o p p e r 1

. 1 u g/ L I 1 4 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Nu tr ien t s
- Liq u i d Am m o ni a- N 0 .0 13 m g N/L I 0. 01 0

. 0 2 2 / 2 / 2 0 0 4 13 :15 D -0C0 Nutr i e nts- L i qu id NO 2 N O3

- N 0.00 4 m g N/L U 0

. 004 0.01 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Nu tr ien t s
- Liq u i d N_ KJ EL _T O T 0. 36 m g N/L 0

. 0 6 0 .2 2 / 2 / 2 0 0 4 13 :15 D -0C0 Nutr i e nts- L i qu id O

- P h o s ph ate-P 0 .00 4 m g P/L U 0

. 004 0.01 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Nu tr ien t s
- Liq u i d T D S 3 84 m g / L 15 60 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Nu tr ien t s
- Liq u i d T S S 1 3 m g/ L I 4 1 6 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Nu tr ien t s
- Liq u i d T o t a l- P 0 .0 23 m g P / L I 0. 02 0

. 0 6 2/ 2/ 20 04 1 3 :1 5 D

- 0 C0 Nu tr ien t s
- Liq u i d T u r b i d it y 5 .2 NT U 0

. 0 5 0 .0 5 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B i o -B O D B i och e m i cal Oxy g en De m and -5 Da y 0 .2 m g /L U 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B i o -B O D B i och e m i cal Oxy g en De m and -5 Da y , N-Inhi b 0 .2 m g /L U 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1, 2,4
, 5

- T e tr ac h l o r ob e n z e n e 0. 97 u g / L U 0

. 9 7 3 .9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 1,2,4

- T r i c h l orobe nz ene 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1
, 2

- Dic h lo r o be nz e n e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1, 3,5

- T r in itr o b e n z en e 3 .9 u g / L U 3 .9 16 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1
, 3

- Dic h lo r o be nz e n e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1
, 3- Din i tr ob en z e n e 1

. 9 u g/ L U 1

. 9 7 .8 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1
, 4

- Dic h lo r o be nz e n e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 1, 4- Nap h t ho qu in on e 1 9 u g/ L U 19 78 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 1-Nap h thy l am i n e 9 .7 ug /L UJ 9.7 3 9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 2
, 3
, 4,6-T e tr a c hl orop he no l 1 .9 ug /L U 1 .9 7.8 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 2,4,5-T r i c h l o r oph en ol 0

. 9 7 ug /L U 0 .9 7 3 .9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 2,4,6-T r i c h l o r oph en ol 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2
, 4

- Dic h lo r o ph en ol 0. 97 u g / L U 0

. 9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2, 4- D i m e thy l ph en ol 4 9 u g / L U 4 9 1 9 0 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2
, 4

- Din i tr op he no l 1 5 u g/ L U 15 58 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2
, 4

- Di nit r ot olu e n e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2
, 6

- Dic h lo r o ph en ol 0. 97 u g / L U 0

. 9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2
, 6

- Di nit r ot olu e n e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2

- Ac e t y l a m in of lu or en e 0

. 9 7 u g/ L U 0. 97 3

. 9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 2-Chl o ro nap htha l e n e 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2

- Ch lor o p h e n o l 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2

- M e thy l

- 4 ,6

- d init r o ph en ol 2

. 9 u g/ L U 2

. 9 1 2 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2- Me th y l n a p h t h a l e n e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2

- Na ph th y l a m ine 9 .7 u g / L U 9 .7 39 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2- Nitr oa ni lin e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2- Nitr op he no l 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 2

- Pi c o li ne 0. 97 u g / L U 0

. 9 7 3 .9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 3,3 '

- D i c hl o r o ben z i di n e 39 ug /L U 3 9 1 60 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 3,3'-Dim e t hy l ben z i di n e 19 ug /L UJ 1 9 7 8 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 3-Meth y l ch ol an th rene 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 3- Nitr oa ni lin e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 4, 4'

- D DD 1

. 5 u g/ L U 1

. 5 5 .8 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 4
, 4'

- DDE 1

. 5 u g/ L U 1

. 5 5 .8 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 4,4'-DDT 1.5 u g / L U 1.5 5 .8 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 4

- Am in o b ip he ny l 3 .9 u g / L U 3 .9 16 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 4

- Br om o p h e n y l ph en y l e t h e r 0

. 9 7 u g/ L U 0. 97 3

. 9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 4-Chl o ro-3-m eth y l p he nol 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B N A

- W a t er 4

- C h lo r o a n ilin e 0

. 9 7 u g/ L U 0. 97 3

. 9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r 4

- Chl o r o ph en y l ph en y l e t h e r 1 .9 ug /L U 1 .9 7.8 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 4- Nitr oa ni lin e 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 4- Nitr op he no l 1 5 u g/ L U 15 58 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 5

- N i tr o
- o
- t o lu id ine 0

. 9 7 u g/ L U 0. 97 3

. 9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er 7
, 12

- D im et hy l b e n z ( a ) a n t h r a c e ne 0. 97 u g / L U 0

. 9 7 3 .9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r A c en ap hthe ne 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er Ac en ap h t hy len e 0. 97 u g / L U 0

. 9 7 3 .9 2 / 2 / 2 0 0 4 11 :10 F IE LD BL A N K B NA

- W ate r A c etop he no ne 0

. 9 7 ug /L U 0 .9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er A l dr in 1

. 5 u g/ L U 1

. 5 5 .8 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er An ili ne 0. 97 u g / L U 0

. 9 7 3 .9 2/ 2/ 20 04 1 1 :1 0 F IEL D B L AN K B NA- W a t er An th r a c e n e 0. 97 u g / L U 0

. 9 7 3 .9



# 7

### 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er A z obe nz e n e / 1, 2-D i ph en y l h y dra z i n e 0 .9 7 u g/L U 0

. 97 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B e nz i d i n e 9 7 u g/L U 9 7 39 0 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B e nz o(a)a n t h ra cene 0.9 7 u g /L U 0 .97 3 .9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Be nz o ( a ) py re ne 0

. 97 ug / L U 0

. 9 7 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Be nz o ( b) f l u o r a n t he ne 0

. 97 ug / L U 0

. 9 7 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B e nz o(g,h
, i ) pery l en e 0 .9 7 u g/L U 0

. 97 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B e n z o(k ) f l uo ran t he ne 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B e n z y l al co ho l 0 .9 7 u g/L U 0

. 97 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Bis ( 2

- c h lor o et ho x y )m et h a n e 0

. 97 ug / L U 0

. 9 7 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B i s(2-c h l o roe t hy l ) eth e r 0 .9 7 u g/L U 0

. 97 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B i s ( 2-ch l o roi s o p ro py l ) e t he r 2 .9 u g /L U 2 .9 12 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er B i s ( 2-e t hy l h exy l )p hth a l a te 15 u g /L U 1 5 5 8 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Bu t y l be nz y l p h t h a l at e 4

. 9 ug / L U 4

. 9 1 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Chry se ne 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Di -n-b ut y l ph tha l at e 4 .9 u g /L U 4 .9 19 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r D i -n
- o c t y l p h t h alat e 0

. 9 7 u g / L U 0. 9 7 3. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Di be nz o(a,h ) a n th race ne 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Di be nz o f ura n 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Di el d r i n 1.5 u g/L U 1

. 5 5 .8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Di et hy l p h th al ate 0 .9 7 u g/L U 0

. 97 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Di m e t h y l p h th al ate 4 9 u g/L U 4 9 19 0 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r D i m e t h y l am i n oa z o be nz e n e 0

. 9 7 u g / L U 0. 9 7 3. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er D i no seb 3 .9 u g /L U 3 .9 16 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r D i ph en y l a m ine 2

. 9 ug / L U 2

. 9 1 2 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er E n do s u l f an I 3 .9 u g /L U 3 .9 16 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er E n do sul f an II 3.9 u g/L U 3

. 9 1 6 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r En do s u l f an s u lf a t e 1

. 5 ug / L U 1

. 5 5. 8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er E n d r i n 1.5 u g/L U 1

. 5 5 .8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er E n dri n a l d ehy d e 3.9 u g/L U J 3 .9 16 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er E t h y l m e th an esul f o na te 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er F l u o ra nt hen e 0 .9 7 u g/L U 0

. 97 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r F l u o r e ne 0

. 97 ug / L U 0

. 9 7 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er He pta c hl o r 1.5 u g/L U 1

. 5 5 .8 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r H e p t ac h l or ep ox id e 1

. 5 ug / L U 1

. 5 5. 8 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r H e x a c h lor o be nz e n e 0

. 9 7 u g / L U 0. 9 7 3. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r H e x a c h lo ro bu t a d i en e 2

. 9 ug / L U 2

. 9 1 2 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Hexach l o rocy cl op en tad i en e 2 .9 u g /L U 2 .9 12 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Hexach l o roe t ha ne 2.9 u g/L U 2

. 9 1 2 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r H e x a c h l o r o p r op en e 1

. 9 ug / L U 1

. 9 7. 8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er In de no(1,2
, 3

- cd)p y r en e 0 .9 7 u g/L U 0

. 97 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Is op ho ro n e 0

. 97 ug / L U 0

. 9 7 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r I s os a f r o l e 0

. 97 ug / L U 0

. 9 7 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er M e th ap y r i l e n e 3.9 u g/L U J 3 .9 16 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er M e th y l m e th an esul f o na te 0.9 7 u g /L UJ 0

. 97 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N

- N i tr o s od i- n- bu t y lam i ne 0

. 97 ug / L U 0

. 9 7 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er N-Ni trosod i

- n
- p r op y l am i n e 1 .9 u g /L U 1 .9 7

. 8 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N

- N i t r os od i e t h y l a m in e 0

. 9 7 u g / L U 0. 9 7 3. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N

- N i t r os od i m et h y lam i ne 1

. 9 u g / L U 1. 9 7

. 8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er N

- Ni trosod i p h e n y l a m i ne 2.9 u g/L U J 2 .9 12 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N

- N i t r os o m e t hy le t h y l a m in e 1

. 9 ug / L U 1

. 9 7. 8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er N-Ni trosom orph ol i n e 0 .9 7 u g/L U 0

. 97 3

. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N

- N i t r os o p ip er idin e 0

. 9 7 u g / L U 0. 9 7 3. 9 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N

- N i t r os op y r r o lidin e 1

. 9 ug / L U 1

. 9 7. 8 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r N a ph t h a l en e 0

. 9 7 u g / L U 0. 9 7 3. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Ni t r ob en z e n e 1.9 u g/L U 1

. 9 7 .8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er Ni t r oq ui n o l i ne -1-oxi d e 19 u g /L U 1 9 7 8 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P e nt achl oro b e n z e ne 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P e nta c hl o r o e th an e 4 9 u g/L U 4 9 19 0 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Pen t ac h l or on itr o be nz e n e 0

. 9 7 u g / L U 0. 9 7 3. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P e nta c hl o r op he no l 2 .9 u g /L U 2 .9 12 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P h en ace t i n 3.9 u g/L U 3

. 9 1 2 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P h en ant hre n e 0 .9 7 u g/L U 0

. 97 3

. 9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P h en ol 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P y re ne 0.9 7 u g /L U 0 .97 3 .9 2 / 2/2 0 0 4 11: 10 FIE L D B L A N K B NA -W a t er P y ri d i ne 3.9 u g/L U J 3 .9 16 2/ 2 / 20 04 1 1 : 1 0 F I EL D BL AN K B N A

- W at e r Sa f r ole 0

. 9 7 u g / L U 0. 9 7 3. 9



# 82 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er a l ph a-BHC 1 .5 ug /L U 1 .5 5.8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er b e ta

- B HC 1

. 5 u g / L U 1.5 5 .8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er d e l t a
- B H C 1 .5 ug /L U 1 .5 5.8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er ga m m a
- B H C 1 .5 ug /L U 1 .5 5.8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er m , p-Cr e s o l s 1 .9 ug /L U 1 .9 7.8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er o
- Cr e s ol 1

. 9 u g / L U 1.9 7 .8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K B NA

- W a t er o-T o l u i d i n e 0

. 9 7 u g / L U 0

. 9 7 3.9 2/ 2 / 2 0 0 4 1 1 : 1 0 F I E L D BL ANK G C- W a t e r A lac h lor 0 .5 9 u g/ L U 0. 59 2. 36 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r A m e try n 0.0 4 9 u g / L U 0

. 04 9 0 .19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r A t r a z i n e 0 .0 49 ug /L U 0 .04 9 0

. 19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r A z i n p h o s M e thy l 0.0 4 9 u g / L U 0

. 04 9 0 .19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r B r o m a c i l 0 .2 ug /L U 0 .2 0.8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r B ut y l at e 0 .2 ug /L U 0 .2 0.8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r C hl o r py r i f o s E t h y l 0 .0 49 ug /L U 0 .04 9 0

. 19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r C h l orpy ri f o s M e t h y l 0.0 9 8 u g / L U 0

. 09 8 0 .39 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r D i a z i n o n 0 .0 49 ug /L UJ 0

. 04 9 0 .19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r E thi o n 0 .0 49 ug /L U 0 .04 9 0

. 19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r E th op r o p 0 .0 98 ug /L U 0 .09 8 0

. 39 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r F en am i p ho s 0 .2 ug /L U 0 .2 0.8 2/ 2 / 2 0 0 4 1 1 : 1 0 F I E L D BL ANK G C- W a t e r F on of os 0

. 09 8 u g/ L U 0. 0 9 8 0

. 3 92 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r H exa z i n on e 0 .0 98 ug /L U 0 .09 8 0

. 39 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r M a l ath i on 0. 15 ug /L U 0 .1 5 0 .6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r M et al a x y l 0. 24 ug /L U 0 .2 4 0 .9 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r M eto l ach l or 0. 49 ug /L U 0 .4 9 1 .9 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r M e t ri bu z i n 0 .0 98 ug /L U 0 .09 8 0

. 39 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r M ev i n p h o s 0

. 2 u g / L U 0.2 0 .8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r N al e d 0. 78 ug /L U 0 .7 8 3 .1 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r N orf l u r a z on 0.0 9 8 u g / L U 0

. 09 8 0 .39 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r P a r a t h i on Et hy l 0

. 1 5 u g / L U J 0 .1 5 0 .6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r P a r at hi o n M e thy l 0.0 9 8 u g / L U 0

. 09 8 0 .39 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r P h o rate 0.0 4 9 u g / L U 0

. 04 9 0 .19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r P r o m e tr y n 0. 15 ug /L U 0 .1 5 0 .6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K G C- W a te r S i m az i n e 0 .0 49 ug /L U 0 .04 9 0

. 19 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r A l u m i n u m 7 ug /L U 7 28 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r A rs e n i c 6 u g / L U 6 2 4 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r C a d m i um 0.0 2 5 u g / L U 0

. 02 5 0 .1 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r C a l c i u m 0. 05 m g /L U 0 .0 5 0 .2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r C hrom i u m 3 ug /L U 3 12 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r C o p p e r 1 ug /L U 1 4 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r I r o n 1 7 u g / L I 15 60 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r L ea d 0

. 1 6 u g / L I 0

. 0 5 0.2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r M a g n e si um 0. 02 m g /L U 0 .0 2 0 .0 8 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r N i c k e l 3 ug /L U 3 12 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r S el e n i u m 1 ug /L U 1 4 2/ 2 / 2 0 0 4 1 1 : 1 0 F I E L D BL ANK M et a l s
- W a t e r S ilver 0 .0 2 u g/ L U 0. 02 0. 08 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K M e t al s-W a te r Z i n c 4 ug /L U 4 16 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d A m m on i a -N 0. 01 m g N/L U 0

. 0 1 0

. 0 2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d N O2 NO3

- N 0 .0 04 m g N/L U 0

. 00 4 0 .0 1 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d N _K J E L_ T O T 0

. 0 6 m g N/L U 0

. 0 6 0.2 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d O

- P ho s p ha te

- P 0.0 0 4 m g P / L U 0

. 00 4 0 .0 1 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d T S S 4 m g / L U 4 1 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d T ota l

- P 0. 02 m g P / L U 0

. 0 2 0

. 0 6 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K N ut r i e n ts-Li q ui d T u r bi d i ty 0. 05 NT U U 0

. 0 5 0

. 0 5 2 / 2/ 20 04 11 :1 0 F IE LD B L A N K O v e rf l o w O i l a n d Gr e a se 0. 88 m g /l I V 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B i o
- A GP/ L i m Nut A l g a l Grow t h P o t e n t i a l 4

. 5 1 m g Dr y W t

/ L A 0.1 0 .3 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B i o
- B OD B i oche m i ca l Oxy g e n De m a n d

- 5 Day 0

. 4 6 m g / L A I 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B i o
- B OD B i och e m i cal Oxy g en Dem a n d -5 Da y , N-Inh i b 0

. 5 9 m g / L A I 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B i o
- C hl

- a Chl o r o ph y l l

- A
, M o no c h r o m a ti c, W a te r 0

. 8 5 u g / L U 0

. 8 5 2.6 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B i o
- C hl

- a Ph ae op hy t i n-A, Mo no chrom a ti c, W a te r 0

. 8 5 u g / L U 0

. 8 5 2.6 2/ 2 / 2 0 0 4 1 2 : 0 5 O UT F A LL D- 0 7 5 B io- T ox ic olo g y B io as s a y
- Ac u t e- Sc r e en
- S W

- F i s h
, LC 50 10 0 L C5 0 L 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B i o
- T o x i c o l og y B i o ass a y
- Acu t e-Scr e en
- S W

- M y si d
, L C 5 0 1 0 0 L C50 L 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B NA

- W a t er 1
, 2
, 4, 5-T e t r a c h l orob en z ene 0. 95 ug /L U 0 .9 5 3 .8 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B NA

- W a t er 1
, 2
, 4-T r i c h l orob en z e n e 0. 95 ug /L U 0 .9 5 3 .8 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B NA

- W a t er 1
, 2

- Di chl o r o be nz en e 0

. 9 5 u g / L U 0

. 9 5 3.8 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B NA

- W a t er 1
, 3, 5-T r i n i t r o be nz e n e 3 .8 ug /L U 3 .8 15 2 / 2/ 20 04 12 :0 5 O UT FAL L D-07 5 B NA

- W a t er 1
, 3

- Di chl o r o be nz en e 0

. 9 5 u g / L U 0

. 9 5 3.8



# 92/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 1,3

- D i n i tr o b e n z en e 1 .9 ug /L U 1

. 9 7

. 6 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 1,4-D i ch lo rob enz e n e 0 .95 u g/L U 0

. 95 3.8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 1
, 4-Na ph th oq ui no ne 1 9 u g /L U 1 9 7 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 1

- Na ph th y l a m in e 9 .5 ug /L U 9

. 5 3 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2
, 3, 4,6

- T e tr ac hl or o p h e n o l 1 .9 ug /L U 1

. 9 7

. 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2, 4,5

- T r i c hl or o p h e n o l 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2, 4,6

- T r i c hl or o p h e n o l 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2, 4- D i c h lo r o ph en ol 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2,4

- D i m e thy l p h e n o l 48 ug /L U 4 8 1 9 0 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 2,4-D i n i trop he no l 1 4 u g/L U 1 4 57 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2, 4- D i n i t r oto l u e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2, 6- D i c h lo r o ph en ol 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2, 6- D i n i t r oto l u e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2

- Ac e t y l am in of l u o r en e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2

- C h lo r o na ph th ale n e 0 .9 5 u g / L U 0.9 5 3

. 8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 2

- Ch lo r o ph en ol 0.95 u g /L U 0 .95 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2- M e th y l

- 4 ,6

- d i n i t r o ph en ol 2.9 u g / L U 2. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2- Me th y l na ph tha l e n e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2

- Na ph th y l a m in e 9 .5 ug /L U 9

. 5 3 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2- N i t r oa ni li ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2- Ni tr op he n o l 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 2- Pic o li ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 3,3'-Di c hl oro b e n z i di ne 3 8 u g /L U 3 8 1 50 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 3
, 3'

- D i m eth y l b e n z i di ne 19 ug /L U 1 9 7 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 3

- Me th y l c h o l a n t h r e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 3- N i t r oa ni li ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4
, 4 '

- D DD 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4,4 '

- D DE 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4, 4'

- D D T 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4- Am i n o b i p h e n y l 3 .8 ug /L U 3

. 8 1 5 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 4-Bro m op he ny l p hen y l eth e r 0 .95 u g/L U 0

. 95 3.8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 4

- Ch lo ro-3-m e t hy lp he no l 0 .95 u g/L U 0

. 95 3.8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4- C h l o r o a n il in e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4- Ch lo r o p h e n y l p h e n y l eth e r 1 .9 ug /L U 1

. 9 7

. 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4- N i t r oa ni li ne 0

. 9 5 ug /L U J 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 4- Ni tr op he n o l 1 4 u g / L U 14 5 7 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r 5-N i tro-o

- to lu id in e 0 .95 u g/L U 0

. 95 3.8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er 7, 12

- D i m eth y l b e n z ( a) a n t h r a c e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ac en ap ht he ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ac en ap ht hy le ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ac et op he no ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ald r in 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ani lin e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er An th r a c e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r Az ob en z e n e /1,2

- D i phe ny l h y d raz i ne 0.95 u g /L U 0 .95 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ben z id in e 9 5 u g / L U 95 38 0 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Be nzo( a ) an th r a c e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ben z o( a ) p y r e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Be nz o ( b) f l uo r a nth e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ben z o( g , h
, i) p e r y le ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Be nz o ( k ) f l u o r a nt he ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Be nzy l al c o h o l 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Bis ( 2- c h lo r o eth o x y ) m e t h a n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Bis ( 2- c h lo r o e t h y l ) et he r 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Bis ( 2- c h lo r o i s o p r o py l) e t h e r 2 .9 ug /L U 2

. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Bi s ( 2

- et hy lhe x y l ) p hth a l at e 1 4 u g / L U 14 5 7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Bu ty l b e n z y l p h th al at e 4 .8 ug /L U 4

. 8 1 9 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er C h r y s e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r Di -n-b uty l ph th al ate 4 .8 u g /L U 4 .8 19 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er D i

- n
- o c t y l p h th al at e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Di be nz o ( a , h) an thr a c e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er D i b e n z of u r an 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er D i e l d r in 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er D i e t h y l ph th al ate 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Di m e th y l p h th al at e 4 8 u g / L U 48 19 0 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Di m e th y l am i n o a z o be nz e n e 0 .9 5 u g / L U 0.9 5 3

. 8



# 102/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er D i n o s e b 3 .8 ug /L U 3

. 8 1 5 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r D i phe ny l a m i ne 2

. 9 u g/L U 2

. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er En do s u l f a n I 3 .8 ug /L U 3

. 8 1 5 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er En do s u l f an II 3.8 u g / L U 3. 8 1 5 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er En do s u l f a n s u lf at e 1 .4 ug /L U 1

. 4 5

. 7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er En dr i n 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er En dr in al de hy de 3.8 u g / L U 3. 8 1 5 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ethy l m e th an es u l f o na te 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er F l u o r a nth e n e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er F l uo r e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er He pta c h l o r 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er H e p t a c hl or ep ox i d e 1 .4 ug /L U 1

. 4 5

. 7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er He x a c h l o r o be nz e n e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er H e x a c h lo r o bu tad i e n e 2 .9 ug /L U 2

. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er H e x a c h lo r o c y c l o p e n tad i e n e 2 .9 ug /L U 2

. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er H e x a c h lo r o e t h a n e 2.9 u g / L U 2. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er H e x a c h lo r o p r o p e n e 1 .9 ug /L U 1

. 9 7

. 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er In de no ( 1 ,2, 3

- c d ) p y r e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Is o p h o r o ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Is os a f r o l e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er M e t h a p y r il en e 3 .8 ug /L U J 3. 8 1 5 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Me th y l m e th an e s ul f o n a te 0

. 9 5 ug /L U J 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N- Ni tr os od in
- bu ty la m i ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N

- N i tr os o d i

- n- pr o p y l a m ine 1 .9 ug /L U 1

. 9 7

. 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N

- N i tr o s o d i e th y l am i n e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N

- Ni tr o s od im e t h y la m i n e 1.9 u g / L U 1. 9 7 .6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er NN i t r os o d i ph en y l am i n e 2 .9 ug /L U J 2. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N

- Ni tr o s om e t h y le th y l am in e 1 .9 ug /L U 1

. 9 7

. 6 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r N-Ni trosom o r ph ol in e 0 .95 u g/L U 0

. 95 3.8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N- Ni tr os op ip er i d i n e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N

- N i tr os o p y r r o lid in e 1 .9 ug /L U 1

. 9 7

. 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N a p h th al en e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ni tr o b e n z e ne 1.9 u g / L U 1. 9 7 .6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er N i tr oq uin o l i n e
- 1

- o x i d e 19 ug /L U 1 9 7 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Pe nta c h l o r ob en z e n e 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Pen t ac hlo r o e th an e 4 8 u g / L U 48 19 0 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Pe nta c h l or on itr o be nzen e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Pen t a c hl or o p h e n o l 2 .9 ug /L U 2

. 9 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Ph en ac eti n 3.8 u g / L U 3. 8 1 1 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Phe n a n t h r e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r Ph en ol 0.95 u g /L U 0 .95 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Py r e ne 0

. 9 5 ug /L U 0 .9 5 3 .8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Py r i d i n e 3.8 u g / L U 3. 8 1 5 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er Sa f r ol e 0 .9 5 u g / L U 0.9 5 3

. 8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 B N A -W ate r al ph a-BH C 1 .4 u g /L U 1 .4 5.7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er be ta

- B HC 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er de lta

- BHC 1 .4 ug /L U 1

. 4 5

. 7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er ga m m a
- B H C 1.4 u g / L U 1. 4 5 .7 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er m , p
- C r es o l s 1 .9 ug /L U 1

. 9 7

. 6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er o
- C r es ol 1.9 u g / L U 1. 9 7 .6 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 B NAW a t er oT o lu id in e 0 .9 5 u g / L U 0.9 5 3

. 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r A la c h l o r 0 .5 6 u g / L U 0.5 6 2. 24 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r A m e t r y n 0

. 04 7 u g / L U 0

. 0 4 7 0 .1 88 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r A tr azine 0 .04 7 ug /L U 0 .0 47 0.1 8 8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 G C

- W a ter A z i nph os Me th y l 0.0 4 7 u g/L U 0.04 7 0 .18 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r B r o m a c i l 0 .1 9 u g / L U 0.1 9 0. 76 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r B u t y l at e 0 .1 9 u g / L U 0.1 9 0. 76 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r C hl or p y r i f o s Et hy l 0 .04 7 ug /L U 0 .0 47 0.1 8 8 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 G C

- W a ter C h l orpy rifos Methy l 0.0 9 3 u g/L U 0.09 3 0 .37 2 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r D i a z i no n 0 .04 7 ug /L U J 0

. 0 4 7 0 .1 88 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r E th io n 0 .04 7 ug /L U 0 .0 47 0.1 8 8 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r E th op r o p 0 .09 3 ug /L U 0 .0 93 0.3 7 2 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r F e n a m ip ho s 0 .1 9 u g / L U 0.1 9 0. 76 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r F on of o s 0

. 09 3 u g / L U 0

. 0 9 3 0 .3 72 2/ 2/2 0 0 4 12 :0 5 O UT F A LL D- 07 5 G CW a te r H ex az in o n e 0 .09 3 ug /L U 0 .0 93 0.3 7 2 2 / 2 / 200 4 1 2 :05 O U T F A L L D

- 0 7 5 G C

- W a ter M al athi on 0.14 u g /L U 0 .14 0 .5 6



# 11

### 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater M e talax y l 0 .23 u g / L U 0.23 0.92 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater M e tolac h lor 0 .47 u g / L U 0.47 1.88 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater Metr ibuz in 0.093 ug /L U 0 .09 3 0.37 2 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater Mevin phos 0.19 ug /L U 0 .19 0 .76 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater N a led 0 .75 u g / L U 0.75 3 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater N o r f lur a z o n 0 .093 ug /L U 0 .09 3 0.37 2 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater Par a thion Ethy l 0 .14 u g / L U J 0 .14 0 .56 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater Par a thio n Meth y l 0.093 ug /L U 0 .09 3 0.37 2 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater P h o r ate 0 .047 ug /L U 0 .04 7 0.18 8 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater Pr om etr y n 0 .14 u g / L U 0.14 0.56 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 G C

- W ater Sim a z i ne 0.047 ug /L U 0 .04 7 0.18 8 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Alum in um 111 ug /L 14 5 6 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater A r sen i c 2 9 u g / L U 29 1 2 0 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Ca dm ium 0 .25 u g / L U 0.25 1 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater C a lc ium 359 m g /L 0.1 0 .4 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater C h r o m i um 6 u g / L U 6 2 4 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater C opper 3.97 ug /L 0.2 0 .8 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Ir on 140 ug /L 30 1 2 0 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Lead 0.5 u g / L U 0.5 2 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Magne sium 1

. 14E+ 0 3 m g / L 0 .5 2 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater N i c k el 62 ug /L U 6 2 2 50 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Selen i um 16 ug /L U 1 6 6 4 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Silver 0.2 u g / L U 0.2 0 .8 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 M e tals

- W ater Z i nc 27 ug /L U 2 7 1 10 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid A m m on ia- N 0.043 m g N / L 0 .01 0 .02 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid N O 2 N O 3- N 0 .018 m g N / L 0 .00 4 0.01 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid N

_ K J E L_T O T 0.51 m g N / L 0 .12 0 .4 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid O

- P hos phate

- P 0 .013 m g P / L 0 .00 4 0.01 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid T D S 2

. 73E+ 0 4 m g / L 1 5 6 0 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid T SS 8 m g / L I 4 1 6 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid T otal- P 0.072 m g P / L 0 .02 0 .06 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 N u tr ie nts

- Liquid T u r bidity 3 N T U A 0 .05 0 .05 2/2 / 2004 1 2 :05 O U T F A L L D

- 075 O v er f l ow O il a nd G r eas e 0 .92 m g/l I V



# 12T r an sacti on C o de N P D E S NU M B E R Y R /M O/D A I n sp T y p e I n spector F ac T y pe



### 1 N 2 5 3 F L 003 6 3 6 6 1 1 1 204 0 2 0 2 1 8 B 19 S 20 2

66

T r an sacti on C o de N P D E S NU M B E R Y R /M O/D A I n sp T y p e I n spector F ac T y pe



### 1 N 2 5 3 F L 003 6 3 6 6 1 1 1 204 0 2 0 2 1 8 X 19 S 20 2

66 Fill O u t This S e c t ion For A ll Surf ac e W a t e r Disc harger I n s pec t i o n s ( CE I
, CS I
, CBI
, P A I
, X S I

- RI Op t i onal)

Rem a rk s Rem a rk s 

# The Bioassay of the Fl ori d a Pow e r Cor por ati o n Cr y s tal Riv e r Pow e r Plant effluen t sa mpled on 2 February 2004, NPDES #FL 0036366.

Fill O u t This S e c t ion For A ll Surf ac e W a t e r Disc harger I n s pec t i o n s ( CE I
, CS I
, CBI
, P A I
, X S I

- RI Op t i onal)



# Th e Priority Pollutan ts A n al y s is fo r B i o ass ay o f th e F l o rid a Po w e r C o rp o r atio n C r y s ta l R i v e r Po w er Plan t effluen t sampled on 2 Februa ry 2004, N P DES #F L0036366.

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