H0H060471 Analytical Report .............................................. 1

Sample Receipt Documentation .......................................... 31

TestAmerica North Canton................................................... 42

General Chemistry Data...................................................... 43

Sample Data ....................................................................... 44

Supportive Raw Data .......................................................... 69

Sample Receipt Documentation .......................................... 87

Total Number of Pages ......................................................... 97
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GENERAL CHEMISTRY DATA

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SAMPLE DATA

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AECOM, Inc

Client Sample ID: U1,2-CTM0033-OUT-IMP12-R1

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-001 Work Order #...: Work Order #...: L47TM Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/05/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide Hydrogen Cyanide 58.7 42.4 ug SW846 9012A SW846 9012A 08/12/10 08/12/10 0224395 0224395

Dilution Factor: 4238.06 MDL............: 21

45
AECOM, Inc

Client Sample ID: U1,2-CTM0033-OUT-IMP12-R2

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-002 Work Order #...: Work Order #...: L47TR Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/05/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide Hydrogen Cyanide 44.9 40.0 ug SW846 9012A SW846 9012A 08/12/10 08/12/10 0224395 0224395

Dilution Factor: 3999.15 MDL............: 20

46
AECOM, Inc

Client Sample ID: U1,2-CTM0033-OUT-IMP12-R3

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-003 Work Order #...: Work Order #...: L47TT Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/05/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide Hydrogen Cyanide 44.0 41.3 ug SW846 9012A SW846 9012A 08/12/10 08/12/10 0224395 0224395

Dilution Factor: 4134.18 MDL............: 21

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AECOM, Inc

Client Sample ID: U1,2-CTM0033-OUT-IMP34-R1

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-004 Work Order #...: Work Order #...: L47T0 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/05/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 19.2 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1921.67 MDL............: 9.6

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AECOM, Inc

Client Sample ID: U1,2-CTM0033-OUT-IMP34-R2

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-005 Work Order #...: Work Order #...: L47VP Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/05/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 18.7 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1869.73 MDL............: 9.3

49
AECOM, Inc

Client Sample ID: U1,2-CTM0033-OUT-IMP34-R3

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-006 Work Order #...: Work Order #...: L47VT Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/05/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 18.5 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1848.96 MDL............: 9.2

50
AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP12-R1

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-007 Work Order #...: Work Order #...: L47V0 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 37.4 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 3739.46 MDL............: 19

51
AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP12-R2

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-008 Work Order #...: Work Order #...: L47V3 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 41.3 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 4134.18 MDL............: 21

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AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP12-R3

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-009 Work Order #...: Work Order #...: L47V6 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 40.8 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 4082.24 MDL............: 20

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AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP34-R1

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-010 Work Order #...: Work Order #...: L47V9 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 19.2 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1921.67 MDL............: 9.6

54
AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP34-R2

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-011 Work Order #...: Work Order #...: L47WA Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 18.4 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1838.57 MDL............: 9.2

55
AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP34-R3

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-012 Work Order #...: Work Order #...: L47WD Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 17.4 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1745.08 MDL............: 8.7

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AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP12-FB

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-013 Work Order #...: Work Order #...: L47WE Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 27.8 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 2783.82 MDL............: 14

57
AECOM, Inc

Client Sample ID: U3-CTM0033-OUT-IMP34-FB

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-014 Work Order #...: Work Order #...: L47WG Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/03/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 16.1 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1610.05 MDL............: 8.1

58
AECOM, Inc

Client Sample ID: U4-CTM0033-OUT-IMP12-R1

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-018 Work Order #...: Work Order #...: L47WT Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/04/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 41.0 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 4103.02 MDL............: 21

59
AECOM, Inc

Client Sample ID: U4-CTM0033-OUT-IMP12-R2

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-019 Work Order #...: Work Order #...: L47W0 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/04/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 43.1 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 4310.77 MDL............: 22

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AECOM, Inc

Client Sample ID: U4-CTM0033-OUT-IMP34-R1

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-021 Work Order #...: Work Order #...: L47W5 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/04/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 19.2 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1921.67 MDL............: 9.6

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AECOM, Inc

Client Sample ID: U4-CTM0033-OUT-IMP34-R2

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-022 Work Order #...: Work Order #...: L47W6 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/04/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 18.2 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1817.79 MDL............: 9.1

62
AECOM, Inc

Client Sample ID: U4-CTM0033-OUT-IMP34-R3

General Chemistry

Lot-Sample #...: Lot-Sample #...: H0H060471-023 Work Order #...: Work Order #...: L47XA Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 08/04/10 Date Received..: Date Received..: 08/06/10

PREPARATION- PREP

PARAMETER ____________________ RESULT __________ RL_______ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide ND 17.1 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 1713.92 MDL............: 8.6

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METHOD BLANK REPORT

General Chemistry

Client Lot #...: Client Lot #...: H0H060471 Matrix.........: Matrix.........: AIR

REPORTING PREPARATION- PREP

PARAMETER __________________ RESULT __________ LIMIT _________ UNITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide Work Order #: L5HX61AA MB Lot-Sample #: A0H120000-395

ND 1.04 ug SW846 9012A 08/12/10 0224395

Dilution Factor: 103.8

Hydrogen Cyanide Work Order #: L5J131AA MB Lot-Sample #: A0H130000-378

ND 1.04 ug SW846 9012A 08/13/10 0225378

Dilution Factor: 103.8

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

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LABORATORY CONTROL SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: H0H060471 Matrix.........: Matrix.........: AIR

PERCENT RECOVERY PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide Work Order #: L5HX61AC LCS Lot-Sample#: A0H120000-395

103 (69 - 118) SW846 9012A 08/12/10 0224395

Dilution Factor: 1038.

Hydrogen Cyanide Work Order #: L5J131AC LCS Lot-Sample#: A0H130000-378

96 (69 - 118) SW846 9012A 08/13/10 0225378

Dilution Factor: 1038.

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

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LABORATORY CONTROL SAMPLE DATA REPORT

General Chemistry

Client Lot #...: Client Lot #...: H0H060471 Matrix.........: Matrix.........: AIR

SPIKE MEASURED PERCNT PREPARATION- PREP

PARAMETER ____________ AMOUNT _______ AMOUNT ________ UNITS __________ RECVRY ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide Work Order #: L5HX61AC LCS Lot-Sample#: A0H120000-395

40.0 41.2 ug 103 SW846 9012A 08/12/10 0224395

Dilution Factor: 1038.

Hydrogen Cyanide Work Order #: L5J131AC LCS Lot-Sample#: A0H130000-378

40.0 38.4 ug 96 SW846 9012A 08/13/10 0225378

Dilution Factor: 1038.

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

66
MATRIX SPIKE SAMPLE EVALUATION REPORT

General Chemistry

Client Lot #...: Client Lot #...: H0H060471 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 07/13/10 Date Received..: Date Received..: 07/18/10

PERCENT RECOVERY RPD PREPARATION- PREP

PARAMETER ___________ RECOVERY ________ LIMITS __________ RPD ____ LIMITS ______ METHOD _________________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide WO#: L4D181AC-MS/L4D181AD-MSD MS Lot-Sample #: H0G200402-001

88 (42 - 140) SW846 9012A 08/12/10 0224395

95 (42 - 140) 7.8 (0-20) SW846 9012A 08/12/10 0224395

Dilution Factor: 4715.

Hydrogen Cyanide WO#: L47T01AC-MS/L47T01AD-MSD MS Lot-Sample #: H0H060471-004

95 (42 - 140) SW846 9012A 08/13/10 0225378

113 (42 - 140) 17 (0-20) SW846 9012A 08/13/10 0225378

Dilution Factor: 1921.

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

67
MATRIX SPIKE SAMPLE DATA REPORT

General Chemistry

Client Lot #...: Client Lot #...: H0H060471 Matrix.........: Matrix.........: AIR

Date Sampled...: Date Sampled...: 07/13/10 Date Received..: Date Received..: 07/18/10

SAMPLE SPIKE MEASRD PERCNT PREPARATION- PREP

PARAMETER __________ AMOUNT ______ AMT _______ AMOUNT _______ UNITS __________ RECVRY ______ RPD ____ METHOD _____________ ANALYSIS DATE ______________ BATCH # _______

Hydrogen Cyanide WO#: L4D181AC-MS/L4D181AD-MSD MS Lot-Sample #: H0G200402-001

ND 189 166 ug 88 SW846 9012A 08/12/10 0224395

ND 189 180 ug 95 7.8 SW846 9012A 08/12/10 0224395

Dilution Factor: 4715.

Hydrogen Cyanide WO#: L47T01AC-MS/L47T01AD-MSD MS Lot-Sample #: H0H060471-004

ND 76.9 73.4 ug 95 SW846 9012A 08/13/10 0225378

ND 76.9 87.2 ug 113 17 SW846 9012A 08/13/10 0225378

Dilution Factor: 1921.

NOTE(S): ____________________________________________________________________________________________

Calculations are performed before rounding to avoid round-off errors in calculated results.

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SUPPORTIVE RAW DATA

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Lot Number Sample Suffix Lab ID Test Prep Date Prepared by Analysis Date Analyzed by

TestAmerica North Canton

Sample Control Chain of Custody for General Chemistry

H0H060471 1 L47TM1AA Cyanide, Total (9012A, Automated) 08/12/10 Ben Rohr 08/12/10 Ben RohrH0H060471 2 L47TR1AA Cyanide, Total (9012A, Automated) 08/12/10 Ben Rohr 08/12/10 Ben RohrH0H060471 3 L47TT1AA Cyanide, Total (9012A, Automated) 08/12/10 Ben Rohr 08/12/10 Ben RohrH0H060471 4 L47T01AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 4 S L47T01AC Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 4 D L47T01AD Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 5 L47VP1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 6 L47VT1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 7 L47V01AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 8 L47V31AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 9 L47V61AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 10 L47V91AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 11 L47WA1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 12 L47WD1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 13 L47WE1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 14 L47WG1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 18 L47WT1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 19 L47W01AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 21 L47W51AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 22 L47W61AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben RohrH0H060471 23 L47XA1AA Cyanide, Total (9012A, Automated) 08/13/10 Ben Rohr 08/13/10 Ben Rohr

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