Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

50976 Indiantown Cogeneration 1 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

50976 Indiantown Cogeneration 1 As Received Higher Heating Value 50976 Indiantown Cogeneration 1 As Received % Moisture 50976 Indiantown Cogeneration 1 As Received % Ash 50976 Indiantown Cogeneration 1 As Received % Sulfur 50976 Indiantown Cogeneration 1 Dry basis Higher Heating Value 50976 Indiantown Cogeneration 1 Dry basis % Ash 50976 Indiantown Cogeneration 1 Dry basis % Sulfur 50976 Indiantown Cogeneration 1 Dry basis Antim ony 50976 Indiantown Cogeneration 1 Dry basis Arsenic 50976 Indiantown Cogeneration 1 Dry basis Beryllium 50976 Indiantown Cogeneration 1 Dry basis Cadmium 50976 Indiantown Cogeneration 1 Dry basis Chlorine 50976 Indiantown Cogeneration 1 Dry basis Chromium 50976 Indiantown Cogeneration 1 Dry basis Cobalt 50976 Indiantown Cogeneration 1 Dry basis Fluorine 50976 Indiantown Cogeneration 1 Dry basis Lead 50976 Indiantown Cogeneration 1 Dry basis Manganese 50976 Indiantown Cogeneration 1 Dry basis Mercury 50976 Indiantown Cogeneration 1 Dry basis Nickel 50976 Indiantown Cogeneration 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D3174 ASTM ASTM D5865 ASTM D3174 ASTM ASTM ASTM D3683 (Mod) ASTM D3683 (Mod) ASTM D3683 (Mod) ASTM ASTM D3683 (Mod) ASTM ASTM D3761 ASTM D3683 (Mod) ASTM D3683 (Mod) ASTM D6722 ASTM D3683 (Mod) ASTM D3684 (Mod)EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50976 Indiantown Cogeneration 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 2010-11189 12548.00 Btu/lb 2010-11197 12656.00 Btu/lb 2010-11196 12473.00 Btu/lb 2010-11195 12725.00 Btu/lb 2010-11194 12693.00 Btu/lb 2010-11193 12693.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 2.22 13.4 0.85 12832 Btu/lb 13.7 0.87 2.3 12.75 0.89 12954 Btu/lb 13.05 0.91 2.49 14.12 0.84 12792 Btu/lb 14.49 0.86 2.32 12.96 0.89 13027 Btu/lb 13.27 0.91 2.25 12.88 0.92 12986 Btu/lb 13.18 0.92 2.24 12.79 0.89 12984 Btu/lb 13.08 0.91Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 1598 ppm 1729 ppm 1485 ppm 1528 ppm 1552 ppm 1477 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 2.22 2.3 2.49 2.32 2.25 2.24 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

13.7 70.23 4.58 1.45 0.87 13.05 71.17 5.67 1.51 0.91 14.49 69.73 4.39 1.36 0.86 13.27 70.41 4.61 1.42 0.91 13.18 70.53 4.66 1.44 0.92 13.08 70.96 4.58 1.46 0.91 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

9.17 8.69 9.17 9.38 9.27 9.01EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50976 Indiantown Cogeneration 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 2010-11190 12526.00 Btu/lb 2010-11199 12604.00 Btu/lb 2010-11200 12669.00 Btu/lb 2010-11198 12690.00 Btu/lb 2010-11192 12757.00 Btu/lb 2010-11188 12671.00 Btu/lb 2010-11187 12612.00 Btu/lb 2010-11201 12546.00 Btu/lb 2010-11191 12661.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 2.07 13.7 0.88 12790 Btu/lb 13.99 0.9 2.1 13.72 0.87 12874 Btu/lb 14.02 0.89 2.1 13.4 0.87 12940 Btu/lb 13.69 0.89 2.19 13.09 0.89 12974 Btu/lb 13.38 0.89 2.08 12.77 0.9 13029 Btu/lb 13.04 0.92 2.18 13.05 0.89 12954 Btu/lb 13.34 0.91 2.13 13.38 0.88 12887 Btu/lb 13.67 0.9 2.2 13.86 0.85 12828 Btu/lb 14.17 0.87 2.1 13.4 0.88 12933 Btu/lb 13.69 0.9Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 1316 ppm 0.063 μg/g 0.37 μg/g 2.435 μg/g 2.197 1523 ppm 0.037 μg/g 0.404 μg/g 2.834 μg/g 2.229 1516 ppm 0.114 μg/g 0.278 μg/g 2.694 μg/g 2.236 1590 ppm 0.049 μg/g 0.274 μg/g 2.89 μg/g 2.201 1502 ppm 0.06 μg/g 0.984 μg/g 2.726 μg/g 2.169 1378 ppm 0.086 μg/g 0.319 μg/g 2.497 μg/g 2.158 1707 ppm 0.09 μg/g 0.314 μg/g 2.357 μg/g 2.203 1468 ppm 0.055 μg/g 0.959 μg/g 4.381 μg/g 2.24 1447 ppm 0.0489 μg/g 0.309 μg/g 2.544 μg/g 2.207Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g 0.063 μg/g 19.498 μg/g 8.68 μg/g 7.71 μg/g μg/g 0.081 μg/g 20.006 μg/g 8.744 μg/g 7.635 μg/g μg/g 0.099 μg/g 19.842 μg/g 8.828 μg/g 7.67 μg/g μg/g 0.085 μg/g 19.708 μg/g 8.685 μg/g 7.22 μg/g μg/g 0.081 μg/g 19.059 μg/g 8.297 μg/g 7 μg/g μg/g 0.075 μg/g 19.023 μg/g 8.656 μg/g 7.289 μg/g μg/g 0.134 μg/g 19.319 μg/g 8.73 μg/g 8.31 μg/g μg/g 0.1 μg/g 26.46 μg/g 8.817 μg/g 7.067 μg/g μg/g 0.083 μg/g 19.346 μg/g 8.564 μg/g 7.381 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 16.552 μg/g 4.67 μg/g ND 9.09 μg/g 16.87 μg/g 4.03 μg/g ND 9.272 μg/g 17.048 μg/g 5.234 μg/g ND 9.393 μg/g 17.074 μg/g 4.847 μg/g ND 9.42 μg/g 16.699 μg/g 4.479 μg/g 10 ppm 9.319 μg/g 16.613 μg/g 4.407 μg/g ND 9.174 μg/g 16.856 μg/g 4.665 μg/g ND 9.264 μg/g 17.558 μg/g 4.552 μg/g ND 9.674 μg/g 16.64 μg/g 4.751 μg/g 10 ppm 9.257 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

2.07 13.99 70.04 4.6 1.28 0.9 2.1 14.02 70.22 4.66 1.29 0.89 2.1 13.69 70.48 4.62 1.31 0.89 2.19 13.38 70.9 4.69 1.32 0.89 2.08 13.04 70.83 4.64 1.29 0.92 2.18 13.34 70.45 4.64 1.29 0.91 2.13 13.67 71 4.63 1.33 0.9 2.2 14.17 69.84 4.51 1.29 0.87 2.1 13.69 70.58 4.66 1.32 0.9 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 9.19 8.92 9.01 8.82 9.28 9.37 8.47 9.32 8.85EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50976 Indiantown Cogeneration 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 50976 Indiantown Cogeneration 1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm