### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date

2277 Sheldon Station 1Fuel Type 1 (5/05/2010) Fuel Type 2 (5/06/2010) Fuel Type 3 (5/07/2010)

subbituminous subbituminous subbituminousOther Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

2277 Sheldon Station 1 As Received Higher Heating Value 2277 Sheldon Station 1 As Received % Moisture 2277 Sheldon Station 1 As Received % Ash 2277 Sheldon Station 1 As Received % Sulfur 2277 Sheldon Station 1 Dry basis Higher Heating Value 2277 Sheldon Station 1 Dry basis % Moisture 2277 Sheldon Station 1 Dry basis % Ash 2277 Sheldon Station 1 Dry basis % Sulfur 2277 Sheldon Station 1 Dry basis Antim ony 2277 Sheldon Station 1 Dry basis Arsenic 2277 Sheldon Station 1 Dry basis Bery llium 2277 Sheldon Station 1 Dry basis Cadmium 2277 Sheldon Station 1 Dry basis Chlorine 2277 Sheldon Station 1 Dry basis Chromium 2277 Sheldon Station 1 Dry basis Cobalt 2277 Sheldon Station 1 Dry basis Fluorine 2277 Sheldon Station 1 Dry basis Lead 2277 Sheldon Station 1 Dry basis Manganese 2277 Sheldon Station 1 Dry basis Mercury 2277 Sheldon Station 1 Dry basis Nickel 2277 Sheldon Station 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 METHOD B ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 METHOD B ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6721 ASTM D6357 ASTM D6357 ASTM D3761 ASTM 6357 ASTM 6357 ASTM D6722 ASTM D6357 SW -846-7740EIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M30B, M2 6A, M0031 with SW846 M6260B) 2277 Sheldon Station 1 M5/29, OTM-27/OTM-28

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Sam ple 019 5/5/2010 8428.00 Btu/lb 29.97 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 3.99 0.2 12034 Btu/lb 5.7 0.29Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 23 ppm 0.07 μg/g <1 μg/g 0.2 μg/g 0.2Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units μg/g 4 μg/g <2 μg/g 21 μg/g 3 μg/gSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units <1 μg/g 54 ppm <1 μg/gEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M30B, M2 6A, M0031 with SW846 M6260B) 2277 Sheldon Station 1 M5/29, OTM-27/OTM-28

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Sam ple 022 5/6/2010 8547.00 Btu/lb 28.72 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 4.26 0.21 11990 Btu/lb 5.97 0.29Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 18 ppm 0.06 μg/g <1 μg/g 0.2 μg/g 0.2Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units μg/g 3 μg/g <2 μg/g 20 μg/g 3 μg/gSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units <1 μg/g 57 ppm <1 μg/gEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M30B, M2 6A, M0031 with SW846 M6260B) 2277 Sheldon Station 1 M5/29, OTM-27/OTM-28

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Sam ple 025 5/7/2010 8381.00 Btu/lb 29.16 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 4.79 0.17 11830 Btu/lb 6.76 0.24Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 37 ppm 0.06 μg/g <1 μg/g 0.2 μg/g 0.2Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units μg/g 4 μg/g <2 μg/g 23 μg/g 3 μg/gSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units <1 μg/g 46 ppm <1 μg/gEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6 260B) 2277 Sheldon Station 1

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm