Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

891 Havana 6
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

891 Havana 6 As Received Higher Heating Value

891 Havana 6 As Received % Moisture

891 Havana 6 As Received % Ash

891 Havana 6 As Received % Sulfur

891 Havana 6 Dry basis Higher Heating Value

891 Havana 6 Dry basis % Ash

891 Havana 6 Dry basis % Sulfur

891 Havana 6 Dry basis Antimony

891 Havana 6 Dry basis Arsenic

891 Havana 6 Dry basis Beryllium

891 Havana 6 Dry basis Cadmium

891 Havana 6 Dry basis Chlorine

891 Havana 6 Dry basis Chromium

891 Havana 6 Dry basis Cobalt

891 Havana 6 Dry basis Fluorine

891 Havana 6 Dry basis Lead

891 Havana 6 Dry basis Manganese

891 Havana 6 Dry basis Mercury

891 Havana 6 Dry basis Nickel

891 Havana 6 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D4239

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D6722

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357
EIA Facility Code Facility Name Boiler ID HAPs Test Group

891 Havana 6 Mercury and non-mercury metalic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

% Moisture

(as 

received)

RUN 1 4/21 4/21/2010 4/21/2010 27.56286

RUN 2 4/22 4/21/2010 4/21/2010 28.21493

RUN 3 4/23 4/21/2010 4/21/2010 30.39671

 Fuel Testing Results


% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

11916 btu/dry lb 6.59 0.34 9 ppm 0.059

11900 btu/dry lb 6.28 0.33 11 ppm 0.062

12014 btu/dry lb 5.5 0.34 7 ppm 0.082


Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

μg/g 0.201 μg/g 1.04 μg/g 0.255 μg/g 0.167 μg/g

μg/g 0.144141 μg/g 0.979041 μg/g 0.283728 μg/g 0.056373 μg/g

μg/g 0.142619 μg/g 1.595567 μg/g 0.337855 μg/g 0.068463 μg/g


Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

4.46 μg/g 2.78 μg/g 13 μg/g 5.29 μg/g <1

4.329267 μg/g 2.651601 μg/g 12.31029 μg/g 5.106138 μg/g <1

4.278239 μg/g 3.003925 μg/g 9.31492 μg/g 5.695515 μg/g <1


Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

μg/g 1.98 μg/g

μg/g 2.424108 μg/g

μg/g 2.579566 μg/g


EIA Facility Code Facility Name Boiler ID HAPs Test Group

891 Havana 6 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

RUN 1 4/19 4/19/2010 4/19/2010

RUN 1 4/20 4/20/2010 4/20/2010

RUN 2 4/20 4/20/2010 4/20/2010

RUN 3 4/20 4/20/2010 4/20/2010

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

27.21435 11943 btu/dry lb 6.47 0.32 11 ppm

27.36593 11899 btu/dry lb 6.44 0.33

28.14371 11741 btu/dry lb 6.61 0.35 12 ppm

26.47095 11990 btu/dry lb 5.96 0.32 10 ppm


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

73.8 ug/g

73.3 ug/g

59.9 ug/g


EIA Facility Code Facility Name Boiler ID HAPs Test Group

891 Havana 6 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

RUN 1 4/21 4/21/2010 4/21/2010

RUN 2 4/22 4/21/2010 4/21/2010

RUN 3 4/23 4/21/2010 4/21/2010

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

27.56286 11916 btu/dry lb 6.59 0.34 9 ppm

28.21493 11900 btu/dry lb 6.28 0.33 11 ppm

30.39671 12014 btu/dry lb 5.5 0.34 7 ppm


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.059 μg/g 0.201 μg/g 1.04 μg/g 0.255 μg/g 0.167

0.062 μg/g 0.144141 μg/g 0.979041 μg/g 0.283728 μg/g 0.056373

0.082 μg/g 0.142619 μg/g 1.595567 μg/g 0.337855 μg/g 0.068463


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

μg/g 4.46 μg/g 2.78 μg/g 13 μg/g 5.29 μg/g

μg/g 4.329267 μg/g 2.651601 μg/g 12.31029 μg/g 5.106138 μg/g

μg/g 4.278239 μg/g 3.003925 μg/g 9.31492 μg/g 5.695515 μg/g


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

<1 μg/g 1.98 μg/g

<1 μg/g 2.424108 μg/g

<1 μg/g 2.579566 μg/g


EIA Facility Code Facility Name Boiler ID HAPs Test Group

891 Havana 6 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

RUN 1 4/19 4/19/2010 4/19/2010

RUN 1 4/20 4/20/2010 4/20/2010

RUN 2 4/20 4/20/2010 4/20/2010

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

27.21435 11943 btu/dry lb 6.47 0.32 11 ppm

27.36593 11899 btu/dry lb 6.44 0.33

28.14371 11741 btu/dry lb 6.61 0.35 12 ppm


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

73.8 μg/g

73.3 μg/g