### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

891 Havana 6Fuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 891 Havana 6 As Received Higher Heating Value 

### 891 Havana 6 As Received % Moisture 

### 891 Havana 6 As Received % Ash 

### 891 Havana 6 As Received % Sulfur 

### 891 Havana 6 Dry basis Higher Heating Value 

### 891 Havana 6 Dry basis % Ash 

### 891 Havana 6 Dry basis % Sulfur 

### 891 Havana 6 Dry basis Antim ony 

### 891 Havana 6 Dry basis Arsenic 

### 891 Havana 6 Dry basis Beryllium 

### 891 Havana 6 Dry basis Cadmium 

### 891 Havana 6 Dry basis Chlorine 

### 891 Havana 6 Dry basis Chromium 

### 891 Havana 6 Dry basis Cobalt 

### 891 Havana 6 Dry basis Fluorine 

### 891 Havana 6 Dry basis Lead 

### 891 Havana 6 Dry basis Manganese 

### 891 Havana 6 Dry basis Mercury 

### 891 Havana 6 Dry basis Nickel 

### 891 Havana 6 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04)


### ASTM D5865 ASTM D5142 ASTM D5142 ASTM D4239 ASTM D5865 ASTM D5142 ASTM D5142 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D6722 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357EIA

Facility Code Facility

Name Boiler ID HAPs Test Group


### 891 Havana 6 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher

Heating Value (HHV) (as received) HHV Units % Moisture (as received) 

### RUN 1 4/21 4/21/2010 4/21/2010 27.56286 RUN 2 4/22 4/21/2010 4/21/2010 28.21493 RUN 3 4/23 4/21/2010 4/21/2010 30.39671 Fuel Testing Results% A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) 

### 11916 btu/dry lb 6.59 0.34 9 ppm 0.059 11900 btu/dry lb 6.28 0.33 11 ppm 0.062 12014 btu/dry lb 5.5 0.34 7 ppm 0.082Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units 

### μg/g 0.201 μg/g 1.04 μg/g 0.255 μg/g 0.167 μg/g μg/g 0.144141 μg/g 0.979041 μg/g 0.283728 μg/g 0.056373 μg/g μg/g 0.142619 μg/g 1.595567 μg/g 0.337855 μg/g 0.068463 μg/gChromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) 

### 4.46 μg/g 2.78 μg/g 13 μg/g 5.29 μg/g <1 4.329267 μg/g 2.651601 μg/g 12.31029 μg/g 5.106138 μg/g <1 4.278239 μg/g 3.003925 μg/g 9.31492 μg/g 5.695515 μg/g <1Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 

### μg/g 1.98 μg/g μg/g 2.424108 μg/g μg/g 2.579566 μg/gEIA

Facility Code Facility

Name Boiler ID HAPs Test Group


### 891 Havana 6 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units RUN 1 4/19 

### 4/19/2010 4/19/2010 RUN 1 4/20 4/20/2010 4/20/2010 RUN 2 4/20 4/20/2010 4/20/2010 RUN 3 4/20 4/20/2010 4/20/2010 Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 27.21435 11943 btu/dry lb 6.47 0.32 11 ppm 27.36593 11899 btu/dry lb 6.44 0.33 28.14371 11741 btu/dry lb 6.61 0.35 12 ppm 26.47095 11990 btu/dry lb 5.96 0.32 10 ppmMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 

### 73.8 ug/g

73.3 ug/g 59.9 ug/gEIA

Facility Code Facility

Name Boiler ID HAPs Test Group


### 891 Havana 6 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### RUN 1 4/21 4/21/2010 4/21/2010 RUN 2 4/22 4/21/2010 4/21/2010 RUN 3 4/23 4/21/2010 4/21/2010 Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 27.56286 11916 btu/dry lb 6.59 0.34 9 ppm 28.21493 11900 btu/dry lb 6.28 0.33 11 ppm 30.39671 12014 btu/dry lb 5.5 0.34 7 ppmMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 

### 0.059 μg/g 0.201 μg/g 1.04 μg/g 0.255 μg/g 0.167 0.062 μg/g 0.144141 μg/g 0.979041 μg/g 0.283728 μg/g 0.056373 0.082 μg/g 0.142619 μg/g 1.595567 μg/g 0.337855 μg/g 0.068463Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units 

### μg/g 4.46 μg/g 2.78 μg/g 13 μg/g 5.29 μg/g μg/g 4.329267 μg/g 2.651601 μg/g 12.31029 μg/g 5.106138 μg/g μg/g 4.278239 μg/g 3.003925 μg/g 9.31492 μg/g 5.695515 μg/gSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 

### <1 μg/g 1.98 μg/g <1 μg/g 2.424108 μg/g <1 μg/g 2.579566 μg/gEIA

Facility Code Facility

Name Boiler ID HAPs Test Group


### 891 Havana 6 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units RUN 1 4/19 

### 4/19/2010 4/19/2010 RUN 1 4/20 4/20/2010 4/20/2010 RUN 2 4/20 4/20/2010 4/20/2010 Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 27.21435 11943 btu/dry lb 6.47 0.32 11 ppm 27.36593 11899 btu/dry lb 6.44 0.33 28.14371 11741 btu/dry lb 6.61 0.35 12 ppmMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 

### 73.8 μg/g

73.3 μg/g