# Instructions The EPA secondary aluminum production test program requires emissions and other test data for several pollutants. EPA understands that you own one or more secondary aluminum production facilities. For at least one thermal chip dryer and at least one scrap dryer/delacquering kiln/decoating kiln that you own, you must perform a stack test for volatile and semi-volatile organic HAPs as specified in the letter and instructions accompanying this file. You should collect emissions samples for the identified pollutants downstream of the last relevant emissions control device (i.e., stack or other point representing the composition of the flue gases at the exit to the atmosphere), unless otherwise indicated. (Contact the EPA project lead for situations with multiple stacks or other complex emissions points for the unit.) Sample and analyze the particulate matter collected in the hopper from at least one bag house used to control particulate matter from each type of affected source subject to 40 CFR 63, subpart RRR at your secondary aluminum production facilities. Choose bag houses that are used to control particulate matter from each of the six different types of affected sources (i.e.group 1 furnaces, scrap shredders, chip dryers, scrap dryers/delacquering kilns/decoating kilns, dross only furnaces, and rotary dross coolers) if you have these controlled affected sources at your facilities. Where more than one bag house discharges solids to a common hopper, a single sample will be adequate. In cases where solids from different compartments of a single bag house are collected in multiple hoppers or multiple collection sacks, a single composite sample will be adequate. If you have a total of three or fewer bag houses at all of your facilities, sample and analyze particulate matter from all of them, even if they are controlling the same type of affected source. It is not necessary to conduct a stack test for multi-metals analysis.
Sample and analyze the lime used for injection to any of the lime-injected bag houses from which particulate matter samples were collected. If lime of the same type, obtained from the same supplier, is used for more than one lime injected bag house, a single sample will be adequate to represent the lime used in these bag houses.
You must report the results of these tests and chemical analyses in this Microsoft® Excel Emission Test Template. The Excel templates are specific to each type of pollutant. You must report the results of each test on the appropriately labeled worksheet corresponding to the specific tests and analyses conducted at your facilities. If more than one source was tested, you must make a copy of the worksheet and update the source ID in order to distinguish between each separate test of a chip dryer or scrap dryer/ delacquering kiln/decoating kiln at each facility and each different source of particulate matter. After completing the worksheet, you must also submit an electronic copy of the emission test report and the chemical analyses. (PDF format preferred). Please refer to the cover letter of this packet (CAA section 114 letter) for additional testing information. Please note that you do not have to submit a test plan to EPA for approval prior to testing; however, we recommend that you prepare a test plan for your own use to assist in the planning and to verify that you address all of the testing and reporting requirements. You must follow all of the procedures as specified in the test methods, including the quality assurance and quality control measures, and document the results in any test report provided to EPA.**Facility Name and Address Unit Description**  **Process Unit ID Control Device ID** 

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing Feed/Charge Rate Mg/hr Afterburner Operating Temperature degree F

Type of Charge:_______________________________________________________________________

**Compound Volatile Organic HAP**  **Emission Rate Sample 1**

**(kg/hr) Volatile Organic HAP**  **Emission Rate Sample 1 (kg/Mg of feed/charge)**  **Volatile Organic HAP Emission Rate Sample**  **2 (kg/hr) Volatile Organic HAP** 

**Emission Rate Sample 2 (kg/Mg of**  **feed/charge) Volatile Organic HAP** 

**Emission Rate Sample 3**

**(kg/hr) Volatile Organic HAP** 

**Emission Rate Sample 3 (kg/Mg of**  **feed/charge) Test Method**  **Used Detection Limit** 

**Information (BDL,DLL,ADL)**  **Other Supporting Information**  Acrylonitrile 107-13-1 Benzene 71-43-2 Bromodichloromethane 75-27-4 Carbon disulfide 75-15-0 Carbon tetrachloride 56-23-5 Chlorodibromomethane 124-48-1 Chloroform 67-66-3 Chloroprene 126-99-8 Dibromomethane 74-95-3 1,1-Dichloroethane 75-34-3 1,2-Dichloroethane 107-06-2 1,1-Dichloroethene 75-35-4 trans-1,2-Dichloroethene 156-60-5 1,2-Dichloropropane 78-87-5 1,3-Dichloropropene 542-75-6 Methylene chloride 75-09-2 Tetrachloroethene 127-18-4 Toluene 108-88-3 1,1,1-Trichloroethane 71-55-6 1,1,2-Trichloroethane 79-00-5 Trichloroethene 79-01-6 Trichlorofluoromethane 75-69-4 **Speciated Volatile Organic HAP Emission Data Facility Name and Address**  **Unit Description Process Unit ID**  **Control Device ID**

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing Feed/Charge Rate Mg/hr Afterburner Operating Temperature degree F

Type of Charge:_______________________________________________________________________

**Compound Semi-volatile Organic HAP**  **Emission Rate Sample 1**

**(kg/hr) Semi-volatile Organic HAP** 

**Emission Rate Sample 1 (kg/Mg of feed/charge)**  **Semi-volatile Organic HAP Emission Rate**  **Sample 2 (kg/hr) Semi-volatile Organic HAP**  **Emission Rate Sample 2 (kg/Mg of feed/charge)**  **Semi-volatile Organic HAP Emission Rate**  **Sample 3 (kg/hr) Semi-volatile Organic**  **HAP Emission Rate Sample 3 (kg/Mg of**  **feed/charge) Test Method Used**  **Detection Limit Information**  **(BDL,DLL,ADL) Other Supporting**  **Information** Acenaphthene 83-32-9 Acenaphthylene 208-96-8 Anthracene 120-12-7 Benz[a]anthracene 56-55-3 Benzo[a]pyrene 50-32-8 Benzo[b]fluoranthene 205-99-2 Benzo[g,h,i]perylene 191-24-2 Benzo[k]fluoranthene 207-08-9 Chrysene 218-01-9 Dibenz[a,h]anthracene 53-70-3 Fluoranthene 206-44-0 Fluorene 86-73-7 Indeno(1,2,3-cd)pyrene 193-39-5 Naphthalene 91-20-3 Phenanthrene 85-01-8 Pyrene 129-00-0 **Speciated Volatile Organic HAP Emission Data**

### Facility Name and A**ddress Unit Description**  **Process Unit ID Control Device ID** 

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing Feed/Charge Rate Mg/hr Afterburner Operating Temperature degree F Flow Rate 

## actual M 3

## /min Flow Rate 

## dry sM 3

## /min

**Emission Test Results Constituent**  **Composition Sample 1**  **(%) Composition** 

**Sample 2 (%)**  **Composition**

**Sample 3 (%)**  **Test Method Used**

**(ex. U.S. EPA**

**Method 3B) Other Supporting Information**  O 2 

### CO 2 

### H 2

### O

# Facility Name and A**ddress Unit Description** 



# Sample ID No._____________________ **Type of Sample (Lime or Particulate):_____________________________**
**Date Sampled Date(s) Analyzed** 

**HA P Metal**  **mg/kg** Antim ony Beryllium Chromium Hexavalent chromium Lead Mercury Selenium Arsenic Cadmium Cobalt Manganese Nickel

*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**

# Process Unit ID **Control Device ID***

*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**