# TSCA N0N-C0NFIDENTIAL BUSIIIESS 

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Consent Order, Consent Order

### for Contract Manufacfuter and



### Determinations Supporting Consent Order


### "

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## -..: 

# rI. Ilrr.rr4ary 

### of lr':.irr's

### ofthe Order 

# i itt. Cl.ruteirts

# ofP[41'l '


# ,, IV., EP-A'sAssessmentofExBosqxdaulRis! 

# , ,; .' . :

# .' , 

# , ' 

## :,, ,',,', 

# VL rinforrnition Required 

### to Evaluate Human 

### Health and 

### Envirorunental 

### Effec$ t. . ,. 

## :'

-

# ' I, 

# . Scope

### of

### Applicability and Exemptions

, .t:-:,,. : .. , : 

## '' ' ;'.. ,. -,-

## '':''' '

, 

# ll. TdoAs 

### of 

### Manufaiture (includes importation)r Processiirg, 

### Distrbution in Commerce, Use,



# . : . . and Dispssal.Pending. Submissiqn aad 

### Evaluatigu of

### t4formatiga 

## :. ,: 

# ' U. ReoodkPePing 

# .IV. Requests for 

### Pre-Inspectiou 

### lnfonnation 

# V, Successor

### Liability Upon Transfer of Consent Order



# . VL Modification aird 

### Revocation 

### of Consent Order
: 

# VII. Effect

### of Consent Order:i.



# . : : n.il$,M*qlE}{ I

. 

## .: , : ,,. '1. .i ,l:tr.. ':,..i: ._.ri



## .

# ' ZOO4(")),tme 

### Enyiionmental Prgtebtion Agenqy ('.IEPA" q11'161 

## 4geiic/) ispues 

### the 

### ahachd :.,,.,':.i,..',." t:.,,..,.,' .. :-" ':l "' i 

## r,'::'.. _... Orde4 

### regar{irrg preinanufacti,re notice 

### ("PMNI) P.-] 1;226 

### for tlrq che'mical substance , i',. "' 

# , I

## ft} q

### Compart''), to tak€

### gfftct 'upoq 

### exp{atioa of the PIVIN 

### rwiew 

## ,.,,,' 

# I p#citl. fhe Compdn/ subrnitto{ 

### tle PMNto EpApursuant to $ 5(a)(1) 

### of 

### TSSA an440 CFR 

### Part' 

# : 720, 

# , , ,,., .

# '.' .,, ;.,, ,,,:' : l',. ..i

Under $

# lI of TSCA, 

### it isunlawfrrl for ariy:perooi to

### Ail or refirse 6o

### comply

### witli

# any : ,: ,,1,, 

### p ovi5iO4 of '$,5

### ol anV order issued 

### uir{er $.J1

### Vj{at<irc may,'be 

### zubj;ct 

### lo variBus 

### penaltiei add 

### te 

# , bofli 

### crii[inqt and

### civil liabilitypursuanl to $ 16, a,nd

### to spgcifiq enfprcertrenl and seiaure pur-suant 

### to $ 

### 17. In addition, chemii:al substp4ogs subject tO 

### !O Order issued 

### under $ 5 

### of TSCA. such aS ',. this one, are subject

### to

# t! $ 12(b).9np-ort notice 

### requird-enl



# II. SUMMARY OF 

### TERMS OX'THE 

### ORDER .The Consent Order for this 

### PMN zubstanpe requires the Company 

### to: (a)

### submit to EP^A" certaiq tiered 

### toxicity testing before manrrfacturing the 

### followirigr:specified

. ,,i..i.tn 

### ;lii,r!ir{ta:5ir:r ..4.r'141-' 

### ". . 

### :. . - ...-!.i ";.-i"!.1:ii:11l-:i. , i'i'*i-:: ':"' production volume 

### limits of the 

### PMN substatrce:'.i':ir:r' 

### Itr'I'cstin;;: ' I 1.' ;,i
],i.iil-,,1 r,-[i.;.1

## ;i ',r'i',t;' j1i. ,'1;r,:iLi:; 

## i' ii:: '

## '::3'li],'j -13) ,t j.i.til -ir.in ci- i r: n i i

### i i;l; s e,r.', t z-;i.+ i

### t"I i; ri i-icr :t : i'trl

,,iu ii{ip;ii:i-i r joj-.Y (

## I PX'l'.i g'i i).620 0} li.r:clenl cr;il" dami:trant 

### lctirai assay 

### ({ji'}oTS 8?S'5450). 

## }i-, ;;r;sitivr:, an oral rodeni;ilerita.'lrlo tra:'siceation test (CPPTS b lO,S+e O)

### will'be requirerl asthe fciit>w up

### tegl.,

# '. I 1,-yel:t 

### oral carcinogeni*ily test 

### (CPif t'S B'i0.4200) 

### in rats arid '; , :1fl.(l ,-',., !,J^J '!



### Iaboratory and 

### ,(b):prov-'ideitswoikerspersbnalpfo.tective'equipmenttopIeventd9rqa1'exposr1fe;...
I ' = : ; ,j I L

. 

### (c) provjde respirafors to 

### itsworkcrs to prevent 

### inhalation exposure; 

### (d) as an altemativ-e to using re,3-pirators,.maintain woikpJaeeairborne copcentrations,of thePJvIN ' l' ,.:: substanco at or 

### below a

### specifipil 

### l{ew Chemical E*pou.ore.Limit 

### ('NCllL") o10,03 4qg/m 

# , , 

### verified by gctual 

### exposuremonitoring data (to pursue

### this option, 

### asampling and analytical .'.. method mrrrt 

### pe dweloped by

### the Companf, verified by arrindependent thircl'party 

### lat submitted,to 

### EPA);

r: woxker 

### training 

### in accordanre

# *itt the 

### provisions of the Hazard. Couqrnunication Prggraru sec{ion; i 

### (f) distribute the

### pMN substance 

### only

### to a person 

### who agrees to

### follow the saffIe restrictions rts) and 

### to not further diskibute the 

### PMN substance 

### until it has been 

### completely polymerized; (g) dispose

### of the 

### pMN substance 

### only by incineration (deshuction and removal 

### efficiency

### of gg.gg%).orunderground iry'ection 

### control (class 1

### well, deep 

### well injection forhazardous waste); 

### (i) maintain cerlain records.',,., ,':-),;.,j

### ., ', 1li:,j',:;,,1 .i,i i'i 'i'.r ri

agtenr ij:at 

### all:rnftnnaiion ireroin 

### ili# ii; clai.ri.,::r1 em

### cotrfidehtial 

### bythe Con;;';Li.ny:s 

### cortectly identi fierl 

### witliin brackets and tha.Lany iurbr:rnaticn 

### that is 

### not l-rracketod is 

### nat elajrned as confir-isntiai. 

### To rnak6;tiris r]ocuriicnf a"lailable

### jnr pui;lic vievrin,g, 111)1\

### tvill rr:::novr; orrly the

, 

# ,,,. eB,qf,denlialEuqi+eryh]Qrqatigqgbl+s-Gr4 

# l : Submitter

, 

### identity, chemical identity, 

### production v.olume, use 

### infonaation, and process 

### infbirnation. 

### Specific: 

# [ -]. : 

### Generic: N-(2-hydroxyethyl) alkenamicle. Use:

: 

### Specific: I Generic: 

### A component 

### of adhesives and cosmetics. 

### Mauiryum 1

### 2-Mgnth Productictn 

### Vqlume; Test Data Submittq-d 

### with 

### PMN: 

# - SaLnonella 

### assay-negative 

### with and

### without activation E. coli reverse 

### mutation

### assay-negative

### with and

### without activation Rat acute 

### oral (gavage)

# : LD50 > 2.0 glkg. Rat subchronic 28D 

### oral (gavage) 

# : NOEL 50 

### mglkg, 

### with neurotoxic and male reproductive system

# effects. i,,.; ,r ,:r-:ii..:,iRrt.A}Utedermal 

## * LD50>200,0mg4(8,'--i'.: 11.i,.1r

## ' i. .'rr.-',;,'.i;,..' . ,-. 

### Minimal eye 

### irritation in male 

### rabbits at99oh ai. 

### Not adennal imitation 

### in m*le rabbits 'at99Yo ai. 

## il t)'...



### i\ii! I-. i'i;i' ;;rc;-tali't5r ls 

### !i;"' i i n;.,1 i.,. '|T*XJ.ottr z.:.i.i1al stti:.I;r

## * ilc:j'i i:; 30. 14

## mflL



# , 'w. EPA:I;ASSESSilMNTOFEXPOSUREANDRISK

.The 

### following me 

### EPA's predr6ions regarding the p .robable humari and enviradmental 

### toxicity, humari exppsure arid 

### envirblmental re.lease 

### of the 

### PMN substance, based on

### the information currenfly available 

### to the

### Agency. Human Health 

### Effects Summarv: 

### Absorption: Absorption of the 

### PMN is good all routes based on imalog data, 

### Toxicologieal Endpoin-ts 

### of 

### Conctrnl EPA 

### beliwes that the 

### PMN substqgce may cause carcinogenicity, heritable mutagenicity, 

### reproductive and 

### dwelolmental toxicity, and neuroJoxicity based on data

### fo: a riumber 

### of low molectrlar 

### weight acrylamides 

### in

### worked exposgd
See lvww.eba; 

### goy/opotinh/rtewcheins/oubs/cherrcat.htn Envircinmeptal 

### Efects Stmmarv: 

## -----------.-:-



# . tsased on the submitted aquatic 

### toxicity data on the 

### PMN substance the 

### concentation 

### of concern 

### (COC) was established at 1000 parts per 

### billion.Ur;.,,:

Dermal Exposuro 

### (*CrIuV) 1.8

### to 1$00 1.8 In-halation Exposure 

### Negligib[e



## ') -, 0;0016,to,0,01 

### Dtinltjng Water 

# , r 

### B*porure (mg/day) n Release 

### to w4teq 

### (kddoy) 0 0



## ,,,,,,.. .,,:. 'l ,l 

## Ri$ktocet€ralPubliii : 

## --::r.-l .----: 

# r"

# =x : 

# i ft fCAi Co,og'"is 

# p*ra a. Sufu 

### O,tirti"-g lV'ater

### Aq[ This law re-quir.e$'EPA to 

### detq+inp ths 

# ' ; levcl of clldta4i1ants in drinkipg weter atwhigh'rro adverse health 

### eftct5 are 

### likFly to ogqur. 

## ,; Basbd solely 

### onpossibie health 

### risk trud 

### e;rposire

### oyerl metimg widh an adequate

### iargin 

## of 

## : -. safety, the

### aaximum contaminant 

### level ggat 

### (MCIG) for.acrylamidc is 

### ziiro. Some people who 

# ' drink water containing 

### high levels 

### of acrylamide over a Iorig period 

### oftime coultl have nervous

. system or 

### blood e{fects and may have au increase 

### risk ofi:ancer'ET\I\{I 

### RONME 

### NTAL .E_EEECT E Tggger,gd

# t$tilg. The

### brder prohibits the Company from, exceeding aspecified Company submits the 

### information described 

### in the Testing section 

## of this Order 

### in accordance 

### withthe conditions specif,ed 

### in theTesting

# section. r 

### VI.

## CONSENE CR.DER

r

## " sc o PBI o

### tr A.F FL xCAB ILfl 

## rEAtip- xiEEMETno- 

### ryg *d;@,^**. 

### (a) Segpg.The requirements 

### ofthis Order apply 

### to all commercial rnanufacturing, processing, distrio-ution 

### in comrnel'ce, use and disposal 

### of the chemical substance [1



### .l (P-1 

### l-226)("the 

### PMN substance") 

### in the United States 

### by [. 

### | ("the Company''), except

### to the extent that those 

### activities are exempted by 

### para$aph (b). 

### (b) Exemptions, Manufacfuring, processing, 

### distribution in commerce, use and disposal of the 

### pMNi substance is exemptfrom the requirements of

### this Order (except the requirements 

### in the Recordkeeping and Successor 

### Liability Upon Transfer 

### Of Consent Order sections) only to the extent that (1) these

### activities are conducted 

### in fuII compliance

### with all applicable requirements

### of the

### following exernptions, and 

### (2) such cornpliance is documented 

### by appropriate recordkeeping as required 

### in the Recordkeeping section 

### of this Order.

lntemet Address (UHL)

### " http:/A,vww.spa.gov Reeyelod/Hecyclablo n Prlnted urlth Vagetable Oil Based lnks on Recycled Paper $/lnirnurn 25% Postconsumei)dis",.ji;'*,Iion irr 

### (:)rflnotcc 

### bf {.hc

### }.}dN :;ubrlatrn sclr.:.I'yfu:: c;rport 

### ir. accoidance 

### u'ith 

### TIICA



### gg12.(a)4d12@),40cFR720.3(s)md40criiP?"it'107. Ilovrever,oncethecompanybeginsto manufacture

### tte Pldlrl substancc 

### lirr uqe in the 

### United Statr,s, 

### ito

### firiher activityty 

### tle Compary
,. 

### inyolving the 

### PMN substance is ci.e,,qlpt as 

### "solely 

### for expotf' eved 

### if soISQamoirnt 

### of the 

### PMN substa[qeislate-r.exportcd.AithatPomt:',thelequ1rem9!tsoftIiqor{erapp!yioatl.ae!iyi]ies

,associatedvdth the 

### PMN substance whil-e in the

### tenitory of the 

### United StateS. 

### Prior tq 

### leaving U.S.

### ter-dtary even tho99 quantiti€s

### of batches 

### dfthe PMN substance

### that are destined 

### fol export are subject to teryts 

### of qhe

### order, and @unt,towards a4y 

### Foduction volumetest triggers 

### in the Testing 

### sectioi of this Order. 

### tZ) Rpig+ch 

## b pqvelopme,nt

### f:R&,p':t. The requiremenb 

## of this Order do 

### not 

### appl! 

### to manufactrfring, proobssing, 

### dishitutiori iu commerce, usc and disposal 

### of the 

### PMN substance 

### in small guantities sol.qlyfor r. search and devglgpurent 

### in aQco:dauce 

### with TSCA 

### $56X3), 40 

### qFR 

## ,.. 720.3(w),and. ?tOCFR 

### 720.36. The 

### rcquii.mentl qf thiq

# ffiq also db 

### not ap-ply to mariufiicturin-g, niDerce, use and -disposal 

### of the 

### PMN sribstairce when 

### manufrqhred ' 

### solely

### fornon-co-inercial researcli and 

### dwelopment per 

### TSCA $5(i) and a0 CFR 

### 720'30(i)'



# . (3) Byoroducts. The 

### requirments of-this Order do not apply to the 

### PMN substance when 

### it is produced, 

### without separate 

### commercial intimt, 

### only as a

### "blryroduc!' as definrcd at

### 40

### cFR 720.3(d) and 

### in compliance 

### with 40 CFR 720.30(9). 

### (4) No Separate Commercial 

### Pumose. The requirernents 

### of this Order do 

### not apply to the 

### !l\p,.I substance wheir 

### it is $anufac,h.red, pursuant 

### to any of the e:ennptions 

### in'40'CER?J0.fl0{fi},r'*1.u..,, wi{h no mmmercial purpose separate

### from the substance, 

### mixturg or article of which 

### it is apart.

### c t:t- .'

### D.o.z|.ib)

### (r).

(6) .11_o:Ugle&blj,tcAetgd 

### Gui1d). I'he re4uirements of this Orcler do 

### nci aErply 

### to qua&titics



# . of the 

### PMN substance after they have been completcly polyra 

### eized. 

### (c) Automatic Sunset. 

### If the Comptmy has obtained 

### fot tho 

### PMN stbstai.rce aTest 

### Market 

## Exmptioi ('TME') under

### TSCA 

### $s(hxl) and 40 CFR 720.38 or a

### Low Volume Exernption : 

## ('LVE ) or 

### Low Release and Exposure 

### Exemption 

### (i'LoREX') under 

### TSCA $5(h)(a) and 40

## CF( 72350(c)(l) and (2) respectively, any suc.h 

### exerrption is automatically iendered 

### null and

### void as 

### of the 

### effective date

### of this Conse,nt Order.



## rr. TERMS OF 

### MAI{UFACTU.RE" PROCE$SII{G,



## - DISTRIBUTTOhI 

### IN COMMEBCIX. USB. 

### AND DISPOSAr, PENDING SUBIVIISSION 

### ANI} 

### EVALUATION
The Company is 

### prohibited from niauiufacturing processing, 

### distributing in commerce,'

# {

. 

### using, or disposing 

### of the 

### PMN substancd 

### itr the 

### United States, 

### for auy 

### nonorempt commercial 

### purposg pe,nding the 

### dwelopment of information necessary

### for a reasoned evaluation 

### of the human 

### health effects 

### ofttre substancg and the completion of 

### EPA's review of, and regulatory action baqed

### op.thpt.infr,unationliex@r.i.ridcleordance with the conditions 

### descrihed,in.lhisfuen:sii*:iii i;:"r.r':'t''''iit-

### ': ']' "-'-i

. \ -'./ :j--'-: .' ..:-:.--::-.i--\...:,/--:--:. r:-:'-:-.r ::.-: {: - erivircnnrent srrcl r,vfuicfr is reclr,L"art1.' i;i: r'opoiter-1 

### undei't-S{)h se*ti*n 3(e) shel,.L r';ii:rerri;e tirt: nppl.CIpriate I.MJ.I 

### irie4tiitcaticl 

### nullr ':i.ibr tJris substar:.*e 

### ai:ii *ontain astatornent

### thalthe 

# ,'. sul;stance 

### is su.bjcr;t-to ikris Cc.n,;err:i (,,.

### r,kr- Aclrlitional infbriiiiri-ion -rega-rr]ing uectiorl S(e) 

### repcrfing ,requirerhents ca:r be fbiuncl,at

# lvww.eytt.gov/oppt/tsca$e,' ; , , --| j

, .j

,#:1r.+r,..1;tre):dGooit Laboratorv Practice Jlanalards4ir.rililtcs@.mt(r6rtlsii'-Eachsqdy*tel.f,Qryeil 

### to addfegs-ih.e-..:.':+iii#*rltrI 

### tisks identified 

### in this Order must be conducted according to

### TSCA Good 

### Laboiatory Practice

## .,,.

i-,orrriucteci usjng ui:r:rcri. iled pr-rblishedtest 

### guidelinos). Fro'uo*<;istnust be sn-bmiiterl as ii sui:'porl clocrr,nent i,br

### ihilrilvN, usirrgthe ,urocedures sef ar]-t

## it 40 

### CFlt 72.0,40,, H:llA i,vili.respoirrl to 

### *re t.-1n:pany r,vitir in zl. .,vecJisof ree

### eiving the n 

### ritten

### plotc';ols. l:,PA 

### I'tview af a 1.es I p:iotocol docs not'mean pre-.acceptance of test results.



## ,' ,],. 

### (ri) Irisgq{e.- 

### ierilirirlteqrliie+eqtg 'Ihe Company is prohiliitecl 

### from manufact+ryS the 

### PMlrl

.: I i r' .t .,,., ,. i su'bstanr:e 

### beyoniltlrc foilowing agglegate volurnes ('itheprqcluction lir:r:its"), unl*gs fhe Company 

# ', conrlucts the fotlo r^ring studies

### on the 

### PMN substanie and su'omits 

### all 

### final reports and underlying data:in accordance 

### with the conclitions spqcified 

### inthis Tesfiag

# sectipn'. , ,

## i Production 

### Volume 

### Limit ',: i' 

## {. .' 

### Tier 

### I Testing:



## , ,. ,.'


### Tier 

### II Testing: 

### mlce 'i .;. rl 'IaxicitV.'I-estms 

### 90.day oral

### toxicity in rodents (OPPTS- 870,3 100) 

### witt,functional observational 

### battery and neuropathology (OPPTS 870.6200) Rodent 

### oral dominant iettial assay (OPPTS 870.5450)'

# If positive, an oral rodent heritable translocation test 

## [OfffS 870,5460) 

### will be required asthe

### follow up test. Z-year 

### oral carcinogenicity test (OPPTS 870.4200) 

### in rats andlr .. i; .. :



### IlpA prior 

### tc oxcceiling the 

### applicirti+ pror:lrcfion

## limit, The 

### final report anr! da1'n 

### l1ust'on i. I :. suli1rr itt:e6 as 'a sr-ry;1:ort dEroumeat fo:r 

### .te FirAl,l, r rsi ng1thr: pro ce rlnres set otrt in 

### rl0 CIJR 72A 4'0
. The 

### linal r-qport,iirail 

### containthe contentsspccified 

### in a0 Ch-lt"

### 792]85, Lr:rderlyingduta qhall lie
-,: submittea 

### to 

### nFA 

### in accordincewrththe applicable *Reporting,t? "Data'and 

### Reportirg,",and "TePt F-eport,, subparagraphs 

### in the applicable test 

### [Liidelines. I{owever,

### for purposes 

### ofthis Consent

1 Order, the

### worrl "s1ou1rl" 

### inthose zut:paragraphs 

### shall br: intcrpreted to nlean 

### "shall" to lnake clear

. that ,the u.1rt

## *isricn of such 

### infbrnration'is 

### *orr,lotory. 

## nef will reQlire the submission 

### of raw 

### datasuchass1idesandlaboratoryflotebookson1yifEPAiinds.on{hetrasisofprofeqsiona1 l 

# ,,, jurlgment, that an adequate evaluation 

### of the study 

### iannot take p1ac9 

### in tne absence 

### of these:iterns, 

## (f) iesting Waivers. The Company is 

### not required 

### to conduct astudy specified in paragraph (d)

### of this Testing section 

### if notified 

### inwriting by EPA 

### that 

### it is unnecessary to conductthat stirdy-

.

### (g) Eqirivocal 

### Data, 

### If EPA fin(ls.that the data generated 

### by a shidy are 

### scientifically equivocat the Compaay 

### may continue to manufacture the 

### PM.[ substancd beyond th e applicable 

### production 

### limit. To seek 

### relief from any other 

### restrictions of

### this Order, tho Company may make a secorid attempt

### to obtain 

### unequivo cal 

### dalaby 

### teanducting the study untler the conditigns specified 

### in pma.graphs 

### (b.h(c);.aa4@),(elcept.thaf.theeudy.4aybe submittgdafter,rryeh,

### iagflaapFli.edble{i}qrtii,i.i:?':i:ii production 

### limit). The testing requirements may be 

### modificd, as necessary to 

### permit a reasoned(1) 'Il;rr;ept ;ir; c[+sr; i'ucrl i-n sr.rlri:ali'ip,rLLI]J1 (h)(:Z),

# i[ ',riihiri {r 'wrreks of ]l,.t:oA'r; it;t;i.:ii:t ot" a

tcs;'u Lepor"t 

### ald fial:a,the Cc,rupany tsceives 

### wriften notice lJra.t .Etr)A 

### ilrlds 

### tlial the t-lr*ttgcno-ra;ted 

### by



### ltiIically irirr;ilii:I, lhe Cornliany is pr:ohibiteLi frq-rn

### lirrfhar manufaci;l:re

### of the,Phnl-l a sh iriy a.resclc sul: stanee b ey orr.d il re app li cah-].c p ro ci uet ir:t: 1i"mit' 

### (2) The 

### Companymay coplinue to 

### manuf cture 

### thePMN substance beyonrl the 

### lpplicabie

: pro_tJuction 

### limit onlSr

### if so

### notified, in

### writing, by EPA in response to the 

### Company's compliance 

### with eiilrer 

### ofthe .firllowing subparagraphs 

### (hXZXi) 

### ot'{h)(z)(ii), ,'.|]-fi ^i*{ :f itt\.,t 1, 

## (i) 

## if there is 

### sufficient tirne to reconrluct the study 

### in cornpliancr: with ptlragi'?phs 

### p;), (o), and (e) 

### before exceeding the 

### prorluction 

### lirnit specified 

### in paragraph (d), the Company may reconduct the 

### shrdyi 

### If there 

### is insufficient tirne to reconduct the study 

### in compliance 

### with

: ' - .i paragraphs (b), (c), and (e) before exceeding the procluction 

### limit specified 

### in paragraph (d), the

., Corllpany-may exceed the

### production 

### limit, but mlrst bthelwise 

### comply

### with paragraphs (b), 

### (t), and (e), and shall submit the 

### report and data

### to EPA:withln a reasonable 

### period of time, aItr as ; specified 

### by EpA in the notice described 

### in subparagraph 

## (hxl). EPA 

### will respond to the 

### c'mpanv' in

# TTlffi H

# #;:::;:ffi1J:T. n.,ice describ ed 

### in subparagraph 

## (hxl), submit 

### to EPA a

### written report refuting 

### EPA's

### finding. EPA

### will respond 

### to the Company, 

### in

### writing, within 4weeks

### of receiving the Company's report.i'

## i j.lilr:..:i',i,.1'.r'.:'-;,,j:.. !'t',;,;i'1','... i'',.r- ii:-i:'i. tll':i'' i 't-'i:tt i'ti'"

ali,-t (r:),

### thi; C,;r*pany renrain.s 

### prohibilietl 'jionr 

### firrther ma.ilulhcture

### of'tho PMN substi::tce bcyouri _I_---,i4",t.- thr; applicaUle 

### productio;: 

### limit. 

## @ The 

### Compariy tilay 

### submit to BPA, 

### within 2 weeks 

### of 

### lirst i:ecomin 

### g awar* 

### of such cireumstarces" a

### written statemert 

### explainingwhy circumstances 

### clearlybeyond the 

### control of the

, ,., ++,... Company or 

### laboratory

### will cause or hav$ carrsed development 

### of scientifically 

### iflvalid data' EPA 

### rvill 

### notiff the Company 

### of its respcnse, 

### in

### writing, within 4weeks

### of receiving the Company's 

### reporf. EPA's written response 

### may 

### effierl



## (i) allow the Company 

### to continue to manufacture the 

### PMN sribstance beyond the applicable 

### production 

### limit, or he Company 

### to continue 

### to conduct, or to reconduct,the study 

### in compliance 

### with paragraphs 

### (b), (c), and (e),

## if there 

### is sufficient timeto conduct or reconduct the study andsubmit the 

### report and data 

### to EPA before exceeding the production 

### limit specified 

### in fficient tims for the Company 

### to comply with paragraphs 

## ft), (c), paragraph 

### (d). If there is 

### insufticient time tor the 

### uompany 

### to compry wILr' and (e) 

### before exceeding the 

### production 

### limit specified 

### in paragraph (d), the Company 

### may exceed the 

### production 

### limit, but must otherwise 

### comply

### with pffagraphs 

### (b), (c), and (e), and shall submit the 

### report and data 

### to EpA 

### within a reasonable 

### period of time, 

### all as specified 

### by EPA 

### in the notice described 

### in subparagraph

## (ixz). EpA

### will respond to the 

### comp ilny, 

### inwriting, 

### within 6weeks 

### of ::,receivingrthe Company's repo

## rt and drta,as to ryhetherthe Compalry.niay*continuerto tnanufacture beyond the applicable 

### prcduction 

### limit'

### .i:

, _!

.i

!. niarr.ifactlr':c, ploccssin;1, 

### rlistlrbrition, nsc iinri/,;r 

### rlislrola[ rif t]re 

### Pl\4]i su.bstanr;;;'to 

### mitigatc 

# .: oxilosLlres tr: ,rrlto tr-ret:L.;r

### charar:tcrizitl:e i.islcs l,rresentcil l:y rhc 

### PI/lt{ subsfanct,:. 

### Withip 2 v,rr-:cks- '

## frp* repeipt,of such a no{ice, Lhe Cgmpan,ymust ceaseall manufacfure,

## pioe**ilg, diStribution,

, 

### .,,'+anddisposa1ofthePM{.substange,un1esseither;':i.l



### (1) i,vithin?- vtoeks 

### from receipt 

### of the EPA notice, 

### the Compan-y complies 

### wittr 

## suchrequirer,nentsastltc,.roticespcci1iqS;of:,, ..t , l, 

# ., :, 

# : (2) 'within 4weeks 

### frorn'receipt of the 

### EPA uotice, the Cpmpany submits to EPA a



### (k) 

## Othf Requirements. Regardless 

### ofthe satisfaction 

### ofany other 

### gonditions in this Testing


## , ..segdoiq:the@. pm.luixirsficodi[.uqi-taobey all the

### ter4s pf

### thisGoosent&derrurtiimt&ufise**ts'sjiL *...- 

### notified inwriting by 

### EPA. The Coinpany. may,.based.upon submitted test data or other relevanting, pracgssing, an'l use of tha 

### PMN 

### $ulstirtce 

# r fal

# Lcl+L@4_st Dunn8manufactur ,

# , , : .

# i,

... ,



## .t' at r,nv site controllcd 

### by the Cornpany (incJudr'rrg 

### iny associate<1 paokaging arrd stqragq and during ' ..,'
. i r., 

### , 

### . ,. ] any cleanirig 

## ir maintbnalcb of equipment associatod

### with the PMT',I substance)' the CQmpany



# . .

# ",,.. 

# ,l... --:--.

# ----:-.

. 

# , 

# ." .l .. ,., , 

# '. 

# '' ; .. :

. 't ; , : .' , , , ,. . , .: ': , , ': I "": I ,l'l ,.i:,.r ,' i"i '' ! 

# - (1) Geperal Derm.al 

### Pi;te4ionj Eaoh pcrson

### who is,reasonabl.y 

### likely to be

### dermally : :.1','I ' " .: ,:l :expose{ in 

### $e work areatd ttre 

### plr4N substancc ttrrough direct handling 

### ofthe subsfaiuc 

### or 

# I': :""'".'.. . .., .'.',. tlrough contacf with.eqUipme,nt on 

### which the sqbstartce may exist, or because the subslancg '1 ' 

## . , .::. , . . ._ .. ided 

### with' and is 

# ' becomps 

### airtqme iq a

### frirm listed in ssbp,ara-q4pli 

### (aX2)(i) of this sectro4 is prov, 

### 1eirilr".l to wear, personal protec..tivs eguipment that 

### proviiles a

### birrier to p.reve,nt.d.

# fl*4 ."-{potrnp tq the substanpe 

### in the qppcifiq

### work area where 

### it is selected 

### for use, Each such item of

# pcrsonal : 

### protective gquipment must b1 sl.lected and uSed 

### in 

### lcoi.dancewith OccupatiQnat Safety 

### anjl



### :' 

## rraoean;nttratios f,osiflA?) denrlalprpteclrotrrcquir,emeds 

### at29 

### CFRi910.132'll9l0.1Ei :



### . .,t ,. ,.',..,"i. anrl 1910.138. 

# , (2) specific 

### Derind 

### Prctedv,g ..q.u.lilPen1, The dermal protecti-ve equiprr.eart required 

### by subparagr-aph (a)(1) 

### of this section must iaclirde, brrt is 

### not limited to, the 

### fellowing items: 

### 1i; Gloves, The

### following gltves have already b-eentested resulting in no breakthrough



# . an6 no permeation 

### by the 

### PMN cheinical: North Silver Shield Gloves; Ansell Barrier Gloves, 

### r.-

# -. Norfh 

### Butyl Gloves,-Aqseltr@t 

### lti+rA:6]res'.*uselli1{popreqe Gloves, 

### Apsell So1,.V.6ac'a4idr'{:4jr5."Bei"ai1*:t:r.'* 

### Alsell Canners.Frcyant (iss-riai expo$Er; 

### duling oarmal anC cxpected du,:itlicu nnd r:or'riif;ons 

### of exl.:rsure 

### within

u1eworK alea Dy any oBC or a 

### ,:rrnbination of the 

### fbllowing: '



## (i) E€rmCdiol1-1:c_$ine. T'estiag the material use.dto rnake the chemical 

### proteciive 

### 'clothingandtheconSEuotionoftIeilot!ingtoestab1ishthatt1reprotective9lothingwil1be



## ,,.,, ,'.: impervious for'the.eXpectcd cluration 4qd couditions 

### of exposule. 

### tho tes'ting 

### must subject 

### thc
' ;''.' : .. .,..,. .I ' ::''r:r "' I "'i' combinations 

### of 

### ch&iqal substances to

### which the 

### clgthing may beexposecl 

### in the 

### work area' :, 

### peimeatioli te$ting 

### shallbe condu-cted according tp

### the American 

### Soqi*), for'.Xesti+g imd M-aterials 

## ,,,,,,, 

# . (;ASTiWl F'Zg9 "Standard Test lvtethoa 

### for ferrneation of Liquids and Gases

### tlrougft Proiective ' \:.":--'- !.':'. --:-.--. :

. .. .'.'..' . .,t
. " I 

### Clothing Materials undpr C-oqditions 

### of Continuqus Cortact,?? Results 

### $al[ bb reported as

### tlte



# .;-1-..,.1----.,..:.-'.;.,...-,]:
,, imolutirr" poreAioniate as a

### firnctlon 

### oftime,qnd shall bq docuri:ente{ rn 3ecgrdaage

### with .,...::;.'.;..,..'.:::1'\,..l'',.,.].:':':] 

### AsTIvr F739 rising the 

### fbrniat specified 

### in ASTM 

### Fl 194-99('010) "standard 

### Guidefor

'_l 

### Do-tupe,fin the 

### Rlxu]ts of Chemiiml 

### Pirineation Testirrg of M4terials Used 

### in Protective Clgrhing 

### Mdterialsi' gloves may npt be used 

### for atirng Period'lone€f ttrao they are 4ctuallytested anrl must be ieplpced at

### tle end 

### of eapb

### Wo* shift during which they are exposed to the 

### PMN substahce. 

## (ii) Manufacturtr's Sobcifioatipns, Evaluating the 

### specific4tionsfrom the manufaoturer or supplier 

### of the cheniical protectivrc cloth.

### rlg, or 

### of the 

### material used 

### in construction 

### of the

### clorl ng, 

### to establish that 

### the chemical protective 

### clorhing

### will be impervious to

stancs alone 

### an{ 

### in likeJ,y,eombinationrwit}rofher,.chr*nioal:substances 

### in the wor"k-t .,:l

s$otion is 1:rtivii:lecl

### with iii.il is r:oquircd 

### io ,.,-,oal', at a ininimuln). a lrln'ii.cnai ir,stif:Eie ,i,tt" 

### ()+cupatiolal Safctf anci

### [{calih ('Nl0SlJ").-certifictl respii'atoi' r,vitiran A^pplied Pr'.:tectit:n }.a.r:.tut:

: (6rAr,Lr,') 

### of i.il{}g,

### fiorrr the respirators listerl 

### in subirai:agra'.i:h 

### (uX6lof. this si:c'tioh, a;rcl th-e

,: respirator is uscd 

### in accr;rdanr)o rn

### ith OSHi\ and 

### NIOSII respira.iory protection requiiemerrts at?*9 I 

## ,: CFR 191 

### 0.134 and

### 42 CFR Part 

## 84. A11 respirators must he issued, used, and'maintaineil

, accorcling 

### to an appropriate respiratory protection program under the OSHA requirements 

### in29



## ':

, 

### cFR.1910.134. 

### (S) El$UgALEIate€. 

### The fr:llowing physical states of,air.hor:re chernical sLrbstances are 

### listed

### for subparagraphs (a)(1) and (4) 

### ofthis section:

,,



## (i) Particulate 

### (including solids 

### o:

## liqlid droplets), 

## (ii) Gas/vapor (aII substances 

### in the gas

### fonn), or 

## (iii) Com-bination Gas/Vapor and Particulate (gas and liq-uid/solid physical states {.i are 

### both present; agood example is 

### paint spray 

### mist,which contains both 

### liquid droplets and 

### vapor). Authorized 

### Reslirators. The

### following NlosH-certified respirators meet the



### minimum requirements 

### for subparagraph (a)(a) 

### of this seetion: (6)." 1.j



### (i) Any iilii5f{.r;r:ri.i.i,ioil ipoin,errerf, a;l.t 

### ptlnrfyiiirl Iir1lfac'-:piece respirr;*o.r equipp,rcl 

### with appropria-ie gas/vapor (acid gal;, ot'g;:.'nic -^rapor,

### or subslani;r: specific) *a

### iirirl gcs " 

### (II) Any I-ffOSiT osrtifie,J 

### p'*werert a,i.i-pwrifi'l**= respil'aior eqillppcrl ''n':fit- ;t 

### hoodorhe1metanrlapprcpriategas/vapcr(ac]ctgaS,0Ig:}11icvapor;.oI'. substanco

### specifir) cu*riOg es

### with evidence demorustrating 

### prlotection level

## of 1,000or.greater.l 

# ' ,

### _' (III) Any 

### Nlc}sFl-certified continuous 

### flow supplied-air respirator equipperl 

### with a

### fuil facepiece. 

### (IV) Any 

### Nlg5H-cor,rified L:ontinuous 

### florv smpplted-.flir 

### respitator equipped 

## *ittt a

### hio,l or helmeLw'ith evidence demonstrating 

### protection level 

### of 1,000 or greater. 

### (VI) Any 

### Nl0sH-certified 

### pressnre-1-*:lf or other 

### positive pressure mode 

### supplied*ain respirator equipped 

### with a

### fu}l facepiece, 

## If

## Ni Cqrlridge S-ervice Li:fb Tesfing has bgefl.Qqndrycied; 

### (I) 

### Any 

### NlosH-certified continuous 

### flow supplied.aii respirator equipped 

### with a

### full facepiece. 

### (II)Anv 

### Nlg$H-certified continuous 

### flow supplied-air respirator equipped 

## *iin ahood or 

### helmet

### with evidence demonstrating 

### protection level 

### of 1,000 or 

### greater. 

### (III) Any 

### Nl0sH-certified pressure-demand or other 

### positive pressure mode
s

### upplied-air respirator equipp ed

### wit!-q'[u!] ece. osHA has assigned ApFs of 1000 for certain types of hoods and helmets with powered air purifiTing respirators (PAPRS) or supplied air respirators (sARs) where the manui'acturer can demonstrate adequate air flows to maintain positive pressure inside the hood or helmet i, 

### rd*rf working conclitions. Flowever, the employer rnust have evidence provided by the respirator manufacturer that the testing of these respirators demorstrates perfi:nnance at_alcvel -oflrotection of 1,000^olg:ut*tj| receive anAPF of 1,000' 'This Facroi (s\yp,) study

### #A[i;#,Ji#d,i:tW*'n*-t-;roiifriii^ ti,at rterr.onsrares a Ieveltr pi'otu"iioii'^ofr1;0s0roi'gre-itei;aii'PAPR' ' ''. ;i and SARs with helmets/hoods are to be treaterl as loose-fifting faeepiecc respirators, and reccive an APF of 25'.. i.n.
.. - ,:.,i'
i
-,' ./ :.'... --:---:., ::-":'Y.*'i-Y -jj.:..:-.::::,.. 1;::--:.'-. 

## /1/) ';i ':''- ;l.r;.rluli.-illoPI-'.4T"7 .i:.:t.tC,g;qCr:C',. 1.0 pei'Ctrtl'l;y Wr;iprjrl l:,'',ri)j;,'.ile l-i'

## j :;r):it';l:;-;ti:y

### t'r*r, iilt--)7'il/'
'i: 

## ,: Pro.qrar,isecti.;noftlrisL.rrile:).'Ihis..lx,lrrtpi:irlnisntlta.railaI,*Ieift1reComprxryhasreasonito: belie 

### 'e h,tt,rirrring itrtenrlefl acfiviticr;, 'll!,c i-t1,41{ Su-ir.ii;1.1Ce 

### in thetitixbu.re .may be reconcentratqd

' : _ ' '''"'t '''"' '- ::_' ' _' ' " i I ' l 

### abovethe10oi0.1percent1eve1,w}riehev*r'rppii*s.Ift}risordetcontains'NewChexqieal, Exposure 

### Limits provisions or Release toWater provisions that, 

### respectively, specify a

### NCEL I

, a /1 concentr 

### ailan[*'TwA,') or 

### in-skearn concentrotmo 

### ("N") less tha_n the de

### minimis concentfption



# ,\, ] ry:ecilie6 hes-,,then tlris'cJe

### urinirnis -+xernption does 

### noi apillSi to fitosn :provisions.

I

I (a) 

### ',. 

### ,,.''. :]:: ' 

# , (l) EPA rem{rmencls and elr,courpg, estheusg 

### o|pollution pr.evelrtion, sguce 

### redggtion, engi4eering.conhols aod wo.rk practices, rather tlian respirators, uis. a me9p5 

### of

### coltrollia! inhalation exposures w}renev. er practicable- 

### (2) Whenwer a

### pemor is reasonably.likely to be exposed

### to the 

### PMN substance 

### by inhalation, as an

### alteriative 

### to compliailce 

### with the respirator requireurenfs 

### in the Protection 

### in ttrq



# . \{orkplace section 

### of this 

### Ordo, the Company may oomply 

### with the requirernents of ihis 

### New thc Co,ptpany 

### may deviate

### from the 

### respiratgl

, requirements itr the Protection 

### in the V/orkplace seetion 

### ofthis Order,the Company utust: 

### NtrW 

### CIItrMI CA.L EXP-O SUBE 

### -L-IIAIT-+.i+-ffi-T-:Tr:-T:--r# ,:

l'b) Exuosure 

### Limit. 

# ,' (1) Ge+erai, The

### followirrg new chemical exposurp 

### limit (T\.ICEL')fo{ the 

### PMN substance 

### is an 

### interim level determined 

### by EPA based on the 

### limited informatiou availabletothe 

# ._-,., Agency at the 

### time of development 

### of this 

### Order. The 

### NCEL for the 

### PMN substance is asfollows:



## (i) Tinlp-Weigfuted 

### Aveiase 

### ("TWA']) 

### Limit, The Company shal1 ensure that no person 

### is exposed

### to an airborne concenh'ation 

### of the 

### PMN substauce 

### in excess

### of 0.03

## m#m' (thg
'i ,'

### '.NdEI-) as an, B=hour

### time-weighted 

### avardgl,wi$grrt using a

### i**pioifo, ih: aqxordan:e a r,vith subsection (e) 

### of this Ner,v

### chemical Exposure 

### Limit section.

## . i5,



## \/

-I 

### lU.4 ,r)/t.5f, o,i,.or*tt --=tlti: n;ti':iile.i-'5f 

### ;i:;ll;s 

### i;r ihe a.cl.r.::-i '.vort<-rhift. 

## (c)Bdqqlasseq+ei4&Jgeliace+d"&eJ@ga]$-e$9a, 

# : 

# . ; 

# irl'app:"+tlitr l*iilioitia uryqtopilient antl valiclatio:r 

### of tlre q4lirpling and

# *ilttitul rnethpd for rtrc 

### PMN Substance, 

### alI

### tte rcquirerapn+s 

### 9f

### t{i1 lbsection. (c) 

### apPly. )i9r 

### subletucn! elpqsure 

### mopitoriirg 

### "ouaortd p.

### qslant io subsecti= (d) of this 

## Nwl Chemical Exposure 

### Lrmit section, onty the

# follffi requirernents apply. 

## (c(l)(i)- (4xii), (4iGv)Oil; faXv)GO, 

### (a)i and (9D -----,- .a:.:,, : .,.,-, ,, ..i.: ,:. ".,. , . 

## {4y deviltiori 

### frop-tle 

## re+rirlertlof.this subsltion 

## (:j

# -"tt te

## *1ofe0 ln

### witine 

## !v E?A' ,1,,.,,.- 

### (Z) Su.tmlssion.of 

### V.erifiqidMethpd an4 

### qertif,.cation 

### Stalg&qgll 'fhe Comfauy shall submit to 

### EpA acopy 

### of a

### validatedsampling and 

### analytical method 

### for ttr9 PMIri' substarice 

### which i: satisfies the criteria speoifled r+

### this zubsection 

### (c). ilhe method description shall exp:essly state

. :.-1: .. . ... ... 

### how the rnetho.d compares w.ith each quantitative 

### requrgment specified in this zubsectio-n 

### (3), The suimissign must inclurle 

### a'written stateuie,n! sigped 

### by authorized 

### bf6cials of both the 

### eompany 

## ,- corducted'pursuant 

### tq subso16Oa 

### (c)(3). To assist 

### EFd iri identiSing'the docum-en, q 

### it shall

# state ' 

## ir a consprcuous, underlined subject-line at the top 

### of the

### first 

### page: 

## ItEELS@iSC.and Anatrtipal {,Iethpd 

### foi 

### pMN.' after 

### which the co .rrect 

### PMN number 

### for thic ohemical substance shall be stated.

r 

### !:;it{,r.rr:i21ir:+:{it:i46iii[l!BLti@r*Ibm$p4pany shall havq

# anindrpep4eetle ' --.....{b9,ffi1r,;3gl;tia*"r"*-- 

### (l,Laboratory',)

### verifi the

### validity of the analytical 

### method for the 

### PMN Substance, 

### in accordance 

### (3) Verifi.. !/ -

rzith i:i:r rr'1,:, 

### ,',q'rirr,rl.,.":I t'ir 

### i.',:i :tib'J:,"ii.i: 

### ). in)(3 )

## . ,.1i'; i1tr,

### t)i :i1;:"-"7'r 

### '--c "1':: 

### ':iiit-7to r'ire lt"-: 'i,,ti,. ihe i.,al.,,:,'.':()i7 co1',:,r.,iie,s \i'Ji

# il ail i:iii; :tc'rin:iremen+:; 

### ;peci|e4 irtlJ:.|s r'':i'l':''Jrlori (r:')i3)'



## (ii) ifi.1leperd-q1-ti.-cfue,ts!-i.abalats5,t The inrlependent
.Dfercn ? lairoratory must be zisepmate anil rlis'rirrct person (z:s

### deliueil at

### 40 CFR 720.3(x)) 

### liom 1fur:,{lontparry aud 

### liom any oth.er perst-rn tvho t:trLi.yhave develr:ped the rnr:lhod 

### forthe Coinl:any, government or 

### pdvatc laboratgry accredi{ation prograrn 

### foi chemical tgsting andlor aOaly.sis, ' '.1, t j l I 

### (iv) Good Laborato.fv 

### Practice Strin4arq$. The Laboratory verificziti'oq 

### ofttre 

## \ . -::- ,,. 

### analytical method 

### ior the 

### Pilm{sulqtaiice must 

### comnfr.ivrth 

### TscA Good I,aboraiory Praptice Stardaxds (,.GLp:,) at40 CFR P?rrt 

### 792. (Cedah proviiions of.the 

### TSCA GLP apPlicablc 

### to 

### toxicity testing 

### in laboratory animals, such as

### 40 CFn 792,43 

### ('Test sysleq carc 

### facilities"), 

## ,-., 792.45 

### ('Test systeq supply 

### faoilities') 

## a$ 792.90 

### ('l$nimal and other test s.yste'to gate'i), are 

### clemly inapplicableto the 

### NCEI- 

### ruiuirenrents) However, conrpliance 

### with TSCA GLP iS 

### not requir.grt 

### under'tbisNew Cheqical 

# n.n"r*; f:fr"rt seciilol whero the anatyti"ut method O

# :,* by a 

### laboraiory accredited 

## !y either; 

### (a) Oie 

### American IAdustrial Hygiene Association 

### ('Atr-LAr') 

### prograu approveil 

### in advance in 

### writing by 

### EPA'



### (v) Analysiq 

### of 

### Dlplicate Sapoles. The Company shall 

### collect six duplicate

, samples (a totat 

### of 12) at thc

# iwA conccntation. The samples shall be taken either fro-m a 

### controlled eirvironment (e.g., asealed chamber or 

### "glove 

## bo/) which closely rese,lnbles the actual 

### workplace condiiions or, 

### for solids anfl 

### liquids with very 

### low vapor 

### presstrg by injecting'the 

### PMN substance onto 

### asamptr&solpdiofl4iddi1g3&Ig.dpptrieate samples shall be collecte-il.o&ridedtical&$r:illi1Y*trl.jlis 

### collection media, atthe same

### timo, and under the

### sa-e condifions. One set 

### of six samples shalli-,ai:;.rrilciy uo.il;; i.i.tt 't:,.,'o,].t:,4 dt,: r:11;i.lr:.i:. i,:, 

### I 

### i ,"?;::'lh+ Cc;rrl:'rr:.iI 

### (vi) ,iasrpig-,.jq-li:ge-gtrd.n 

### If the 

### iosults oi't.he analysis 

### of

### duplic*e samples pursuant to paragraph 

### (oX3Xv) r1c

### not satir;fy the requileuror,.is in paragraph 

### (c)(3)(vii), the



# . Compa:ry must 

### perfoml a

### sauple iitorage r:tudy as

# follows:

.. 

### (D Tdeiisu-t€.$ggrpte.s. The Company shall 

### qollccl six 

### triplieate saurples (a 

### total 

### of 18) at the 

### 'I'WA concenlration. Tire samples shall be taken ei*ier:

### fron a controlled 

# - etrvir6fi-nelnt (e.g., asealed char-rber oq 

### "glove box") which clopelylgsunbles the acttral workplaee conditions or, 

### for soliils and 

### liquidr with vsry 

### low vapol pressure, 

### by injecling the 

### PMI{ subsltince onto asatriple 

### collection 

### devicc. The 

### triplicate samples shall be collbcted on identical 

### cqllection media, at the same 

### time, and 

### under the s;uae

### conditiqns, One set 

### of six samples 

### sliall immediately be analyzed by the Company.



## (II) Analfisis 

## Atq Sampk Storege. 

### r\ samplo storage 

### waluation.shall be perforrreil with tho 

### two remaining sets'of six 

### samples, Ore set

### ofslx saniples shall be aa

### alyvedby the Laboratory using the 

### methotl dweloped by or 

### for the Compaoy, and the other shall be.arialyze<l 

### by the Company onthe same day as the Labqratbry anal5zes 

### its six samples. Specializ:ed storage conditions for tho samples 

### including extraction conditions, time

## tom sarnpling

### to o<traction, 

### time



# . from collection or 

### exnaction 

### (if applicable) to

## *ulyri, 

# *d ,tooge conditions must be specifietl 

### in the 

### metlod description.



## (vii) Comoarison 

### of 

### Rixults. 

### Ihe differe,nce between the results 

### of the 

### two sets

### of six samples analyzed 

### by thelaboratory and the Company as required 

### in either pmagraph (o)(3)(v) :," ig.;::"-1r:trli(rr).@.)(uiXll) shall be evaluated usinggrt.w6:sryple..t.tpptrv.ifh,ua8q1ialivaliaaces, and the

### two- . .arru,+ 

### riiii,i]r

sides 

### ofthe critical regions shall 

### not 

### exceda5% significance 

### level. (See 

### r\ttachment C 

### -

### wilhi:l i0% of {lre {:tLcvahie, therr iLr; sanr:'.;Ll stolaS,..c iirne hoiurcerr 

### or;ilecli+li aad a-neiysis 

### mmt be 

# ' reduced unti.i tiro 4ve,rLrge ol'oach 

### sctof six 

### lirmpl s is

## lritlir 1.0%

### pftlle truc value"



### .

# I g) an o*n

# l The sampling.and ar,,rl5rtical riretlrod urusl ciearly dernonstratc 

### the 

### :' I .:r :-: ., .r '. "



# , (D Qe11srd- The sarupling anrl- anal;,lical merhgd, and qlf cxpgsule 

### nionitgnng data : .' : .' : ,'. 1. ., .,. -i. : ,::rri"r-: .:..i.-'i ,, .';r , : :.:... - 

### felied on 

### by tlie Ccimpany, shall

### te ac.curatqtq wilb

## n +25% 

## rt a95% confidence leYel

### for

# . ' 

# ...:'. . r. :.:' '" r'-,''" t -r'::r:':':i'-''''','.1 :.. :. ', 

### concenhationsofthePMNs9bstan,cerarigir,rsftom1eIraIfth;NCEL9twicethiNc,rr' lr,:'l ..,:i-;''(, 

## Iii) NCEL Ouantitation 

### Limits,"Ihe analvtical rhcthofl shq,uld be capa$le 

## of 

# '-:

# - ---:-l --

# 'll - .,.,, , , 

### reliably qridntif-ying

### tle PIvIITI .ob-.stanee ucrossthe ful.I raage of'reasonably likcl.1, cxposrrrps. 

### At q



## .

# . -ir,i*o^, the anafu4ical method musqbe 

### capatlq

# ofieiiffi rying

### fiom a

### tower quantitation 

## '.-,.',^:,,.


# . ri'*i (

# iQr') of;o1e 

### b.al{theNcP.l ,3

# il yoyantiu.{1ir timit

# ('UQriir at teasl

### twi11

# tte

, 

### NCEL. If the Company obtains an expOsure 

### monilothlesrmple thatjs marc than 1-0ilo above the 

## , .. , , ... ,,,: .},' , 

### actia UQr 

## oftte analytical mottiod" the

### pompmluxst

# ood

# wi$n*@ tel(4x0, ' 

## :, 

# , ' , ($i) f,o,lwrQrl+tilAt'oq Lig.rit 

### $ietrA+o-Noise 

### naiio, The. analytical 

### metl0d shall , 

# ' , becapableofquantiff,in-gthePlMlVtoaconcentoationofqnghalftheNCELrviihasignalthatisat least 

### fivp 

### tiues the baseline 

### nois! 

### fevel Easeline npise must be 

### arnplifieil to a measurable lov.el 

## *teo possible, 

### wen 

### if the required 

### amplification is beyond that used in 

### roufine imalysis

# of

. . 

### samples. 

### (If baseline noise

### camot:e obtainett, another reference must be 

### selectetL This may be a peak cgnsideredto be noise causedby the reagent 

### matrix.) The sampling preparation method must ,'' ..-.iri,{.i,ii.{iscspdeige*,and;meeae6doa"timit 

### for ttie analytical 

### proqpdurexru.ssi+ifud444sa}q+J:isru,',. ". 

### injection 

### for cliromatographic tecbniques.i l''

## j i.i:=., r.1 I :ililili.l -'=Ltl "i:' tJ'-G I r'.. lt .; .,',{-'^i..:',' i''t' '': iri-:-::l:i'-f :"i'':::" '! \'':' I i r;a1ibi'aitioil slalldarrilswitJi n lini';a.t'oor1etatiol 

### of 0.95 ",'i-lrcr:t' i-ive 

### (ii) caiiL:raJion st:mr-larrls i:riust I consiuL 

### of onc standard at each o

### Ithe foilowing c{riicontratici';i: crlo haiJ:the

### }ICEL (0'5 x ITT(JFI); 

### betwc*ri o:re 

### half and one 

### iimes i:iie irlCEI-, (>1i.5 x

# ]'Iijiil,( 1x

### ):'lCfiIJ; Qnetimes the 

### I{CI-{' (1

### x ':, 1-,r:, 

### IrfCEl); between one ancl rrro

### tirn*s thq 

### NCEL (>1 ;r

### NCEI ii 1?-

### x 

### NCEL), arrdtwice the 

### H{-EL Q

'I r'. 

### x NCLiL).

, 

### develoBgrent/valiclatiol anil suhserluent

### **po.rrre monitq:fini],,.thc 

### Compary shall conduetboth an 

### jnitiai instrument 

### calibration and'a c'on'iinuihg 

# calibr r. i'he-Company shall 

### perfonu at least one ,l 

## ij '. : ", ' '' ': ' " ' ; '' - ' additionalcalibration, confinurng 

### caribiation sample at the 

### NCEI, concenti#ion, and

### alleast olle
. . ,$arnple per 

### eyer, t p

### samples analyzgd, T'he continurng calibration 1amnle shall

### falIwithin 1-.2570

.. I I 

### of the 

### initial calibration value. 

### If not,

### thet the 

### initiai calibralion must be repeated, and any samples 

# :,' associated 

### with that 

### outlying calibration check must be

# rg-analyzed, '

.

# , ,



## (I) Initial Calirilation. For method deveJopment andvalidation, the Company must calculate the percent 

### of the 

### PMN substance recoYered 

### by the analytical method 

### from asarnple 

### containing a

### known quantity 

### of the PIvIN substance. The s4mple shaIl be taken 

### either

### from a

### controlled environment (*.g., a sealed cfiamber or 

### "glove 

### box")which closely resembles

### the actualworkplace conditions or,

### for solids and 

### liquids 

### with very Iow vapor pressure, 

### ,,matrix spike,,). The calculaJed percent rscovery 

### for each m.atrix spike sha1l be greater than or:

## i ilt:';,-'hl'i i;,-ii; lr..ll n+

### * it :.rlt;t i; r;



## (vi) Sa1gitfll-g ne:feSi1Cagl-1:r-i-11, 

### I :;o capacity

### of l1rr; r;arnpling device niust be \ / .------i- --& 

## ' .' ,: 

### 'jtestedarrdr.esu1tsreportedtoshow.rrndera1*'M.andwe1ldefinedsetofconditions.that.the.

.l.],,,.-,...n':,.'.,.::t,,],:'' : - i,.i- , ...':. .r,r I ,, . . , _. l 

### clwice is capabfe 

### of coll*bting the

# ".* ln**i"*t in 

### iglid,,liquid or vapor phase 

### with minimal loss. 

### jlhe sampllng devir:e's ca-pacity (air vr-rlumo aird collectet{ analy[e mass) must be

### specified.'Fq, l , , . , . . I

. , ,' . t. .. ' . . . 

### inethor1sthatuseu,15g1b.ent:tubesastiiecoilectioil,i,ileciuJn;evic[enceoftlrecapa.;ityrtrrjstb,e provided 

### in the 

### form of breakttnough

### testing. This testing rnust be rlone at aconcenttation 

### twice .r.i a ;', a the 

### NCEL and uncler conclition-s similar 

### to those pxpected 

### inthe 

### workplace. Bt'eaktlrrough is, 

# ,,. definecl to have occurred 

### w}er the concentratioU 

### of the 

### PMN substance 

### in the.effluent stream 

### is 

### "qo*l 

## io 5Voofthe concentration 

### of thE 

### ionrrent sffeam,

### orwhen Z}t!/oofthe 

### PMN substance

# is ' detected 

### in the backup section 

### of the sampler.



## (vii) Sampli 

### tion efficieney must be evaluated 

### for the 

### air sampling 

### dwice. A mimmum of six air samples spiked 

### with the 

### PMN substance at least the 

### NCEL concentration must be 

### prepared. 

### A recovery

### of at least 75o/o must be obtained 

### for each 

### of the 

### six samples. 

### (5) precision. The estimate of the 

### coefficient of variation

### of each set 

### of six sarnples 

### from ::;?-.l,Es.ii=,srithec.ontrolledatmosphere*t paragfaphs,(c)(3)(v)or(vi))lpust"he.Jg6qxtriei,'-*iif,':eii#-i':

than 0.105, 

### including allowance

### of 0.05

### for error due 

### to sampling.

# ili l"'l' ,. ;: r, ; l : m i;. .ix,. :':ii'.:': ';t";o.t' : 

### ;' i5 .lr:;; 1L;:ir 

### 'l:,oi 

### ,:tt'':tztf

## t '

### .:tr':"t:'t i:..t':' l')'5'/'t

o1i:irc estr'mated

### precisiot ir; ,1r'eah;rthao 0.105, #.:en the Compaily must re.preparc t"ile ,1!zrtii.x spike, 

### re-sa$plq arrd re-arLaLyze. a1.1,sarnples alsociaterl 

### witii;ruchmaftix spikc or 

### Lipii:ale siuaples.



## ,, recovely is 

### requirgd, Cone?t 

### for reco,very 

### first by <tividing the observsd auoU+t by ihe 

### proportion

. - .' i . . : " l recoyered before 

### detemining 

### if mezisurerients

### fall belqw the 

### NCEL. For eramplg 

### if the observed : :l ' I'.:J ' ':'''' " :' 

### level is 30 

### rng/ml 

### iud the percent recovery 

### is 75%, use the value 30 mg/m3/(0.75) = 40 

### mglpj ;l

## l'-' 't'" ' when d.eterqIaidg 

### wheper'the feyels are bglow the,expgsure

# limit

. 

### (7) ReDreseiltativ*es... A11 iamrrle conditions usedto develop the inethodqlqgy shall 

## \ , -._--.......-... 

### mimic thb aetual

### workplace envir.glpen!'e. Xpected to b9 

### monitored. Conditions such asthq



## .,,, te6pe-r4ture,

### fugidi51 lig[r1ing, afld presenoe of othcr chetnicalq, etc. must 

### mi4jc.the co.nditiori-s 

### in

: i '-, i.
. .. : r.' the

### workl ace to be 

### monitoreil. 

# ' (8) Ctanses 

### Affectins 

### Validitv. If the workplape 

### envirorment changesfrom the 

### initial conditions desc,ribid 

### in ftrc

### verified qampling and analytical method 

### in away reasonabiy 

### likeiy to 

### invalidite the accuracy 

### of ttre 

### method then ihe Company m.ust comply 

### with the respirator requirc@erits in the 

### Protection 

### in ihe 

### Workplacq section 

### of this Order, rmless the Compiriry 

### revalidates the method 

### to cotrfirm that the requir.ements 

### for accurAcy and precision in paragraphs 

### (c)(4) and (S).are 

### met. Examples 

### ofpossible changei iriclude but are 

### not 

### lipited 

### to: introducfion of a 

### new chemical.substance 

### to the workplace 

### which may interfere 

### with the analysis of

### tte new 

### :,srn,:r+.,iqgffifoea};*:lm.ducioqoflight to

### the.workplace*rhich,may.inteiffiffiiadighrensitive PI-vII{(,1) 

### Mppjlorine&lqdialExp[su] q=



### (l

# ) Generai. 

# \/_.

. (i) 

## &li*LlCyqL The 

### ,'action 

### level" is defined as anairbome concentration 

### of the 

### -weightcd average, ec1ua1 

### to one 

### half the

## NflEL'MA PMN substance, calculatecl as an B-hour

### time

i, specified 

### in subparagraph 

# pxl). For 

### nofl-8-holr wolk shifts, the action 

### level is equal 

### to one

### half the 

### NCELn. (The 

### NCpLn is described 

### in subparagrap-h 

## (b)(lxii).) The Company 

### may exceed the action 

### level

### withoutpenalty. The puqpose

### of the action level is solely 

### to determine the requisite 

### monitoring ftequency.



## (ii) Representative Exposure 

### Groups. Whenever exposure 

### monitoring is required by

### this New Chemical Exposure 

### Limit section, 

### the Company shall take representative samples 

### of what the 

### potential exposure 

### of each person

### who is reasonably 

### likely to be exposed 

### to airbome

. T AY , concentrations 

### of the 

### pMN substaflce 

### would be 

### if respirators were not

### wom. The Company shall 

### *p.air-of at least one person,that,rc,lrresents;,'gnrl-does*noli;.i.'-i':fi.Ii1*ilr# 

### ;i. . - unrlerest imate,the 

### potential exposure 

### of every person 

### perfonning the sarno or substantially 

### similar..?.4
.

i:;:r 11':.iliocrii'e 

### ff:o:lp") .jrh,,.o ;11:ha.iaiio 

### e:'ip:rr.i+tc 

### ite P

# ll] ir.r!,litani.i1 i1;flt23c1iabl-7 iihel;r 

### io ocor-i, 

### Iho expor;rue 

### of i:i.ch pcmon reerJ.nof 

### b,jilsclf rlirr:ctly sauplcct 

## i. :hat exposure is 

# ,;: ,"pr.l,unf"r1 

### lly sarupling ilre L;".pur;ufe

### oiar;o[hoi per:sort 

### iu I'.D saf ie 

### gxpoijurj 

### gtorp. 

# ':| (iii) Gqod

### ti{prator11fraqtlq D-.

### $lmfuIds-, Determir:ations 

### ofpotential 

### i4lalation

# ' 

# ' l 

# , _____-_.__:. 

# ': ' r.,.'l. r:.,r, ' 'l .y'. .,... ":

# -. .,,.


## . flcpi sure shall be made 

### dici:rding lo 

### 'ISCA Good Labor.atory Practice Standardp a! 40 CFR

# Part '

.

. : I ...':1 .a 

### 792,lil1the3irrhplingantlanaIytii,,l,lrnet1rod,]cve,loqcrl1:irisrraotto.subsection(c)oft}ri9}.{ew ',:'' i ', ---. ' : 

### .'CheEiea1ExposureL.jmi{s9ction,(celqaihpIqvi.sionsoftheTSCA,Gtr?anr|ic,.at}9to,,toxi9itv
itapplir;ablr: +o the.ItrCEI. 

### requircui,xls.) I{cwever; conrpli;i:rcb

### wit]f I'SCt\- GLP is riot requirbd where'e.rposLire 

### monitoring s4mplcs or* un{lyredrby a laboratory accreditert 

### by either: 

### (A) the ,+r 

## ,. : . '. 

## : ,, 

### AII-IA II{LAP; or (B),another comparable program approved 

### in advanie 

### inwriting by EPA.

.\.4ffi-. r : iI-'"'/l c6ncentrations shall be determined o:r lhe Qasis

### of samples representing the

### fuIl shift exposure 

### for ,t ' l' i i ' a. each exposure 

# group,

, 

### (2) Initial 

### Moniteri{s. Befqre the Company may 

### dwilte from

### tte respirator requifements 

## ,] of the 

### ?mtection in the

### Workplace section, the Compauy shail conduot 

### initial qrposure 

### monitoring 

### to acc*ately detenliine tho

## airbo-" "oo"*tuution of the 

### PMN substarce 

### for each expo$ure group 

### in which persons are reasonably 

### likely to be exposed to the 

### PMN substaoce. ' 

## rii..r,r* :..
.:.:r,tllr*ri*I.}srx.E${5+dnq+i&H-"sttifui}}ry4iD'.;rrl," ..-

## . , .+cuxr}:z!3tt*ii3ir:$,}$:&g-{..i1*EiirBxl":i:r.r

. ,1,r; -. 

## ': ',tt'i'iiii,,'' lri';',i){-;ijlii ;.

' '"''J- ' --.t- - 

### 7i)' f cri tr r' I iaticir o t-t'1i',:;1iJq -.iil il, \ _ / -i:j:-:-::-,...--

## {i) If r:e,prcseirtalivr: siunples ta]tr;il rJ;: iing the

### inilial t::lpi;sitre ntoititorfurg 

### ievi;al a-n '1 '

### :n below 

### the action 

### lwel, tl-rp Ccnrpany may discontinue n"lonitoring for that 

### allbo]llccodcentratonbelowlne.acuonleYct,ulE\-U]llP.'rrytltaJulor^Jllllrr4vl|(,1 oxposuie group, except 

### whei additidnal exposr.irc rT

### oritoiing is 

### requiiqrl by paragraph 

### (dxo 

## qf 

# i * ,

# ^.t - , 

# . , . ....

# .. , , r



## :^r___-l.-l-:1._.'..
. .. ,,.,,,.,,:..i,,,-., 

## ,. .. ,. .. . ,.. : , ,

',,,,,- , , ,, , ,r,i.'


### . ,' .

### :

## _ . . '. 

## ' " I '" ;'1:1 

## ''r ' : "'"' t "' - ' I " oirborir" 

### *rcentution,:is iod 

### icaleaay

## xteii'n Ajsqculive miasureriiairs tlke.n aI 

### leait 7 day$ ' ; i:,:, ,i .'-lt,..
. .., '
. . apar.fi aIe below the actiori 

### iet'el, the Co.,fiIpany 

### fnaydiscglli1ge the 

### monitoring 

### tbt that exposure ,'1i 

# I ' group, 

## 'r""pi

# *t* ,aaitio"ul moqittiniog rs reqrtiqaa 

### t1n*agraqh (d)(5) of

### t{is Nex Chernicat Exposure 1-imlt 

### section, 1gfiere the 

## Pml substance is rlanufachir-edi procqssed, or used irr 

### latahes 

## l.'r I ., , . 'ir',:,,,.. .': .

## . .., ,, -.. :.'

. 

## .. : 

### of duratioil less th a4 7 .days,. the

### 2 consecutive me4st[einen-ts may be

### takei at le,ast ?A 

### hour! apatt, 

## ",-*:*--.,=-..:.: :-"'r.- . .; _ ,.;;.:,..,,,.r.., 

## ,. , , .. ,. ', ,,.. provided ibat the measur-@reots.

### accurateliiieflegt th,

### I higqF$ peak gxpqsur-es.and vanabili:ty 

## ia

. ' : :.;- : l exDostrre.

, 

## ',.-. (5) Addifonal Monitoliqs.



## (i) For a pre-v-iously 

### monilord oxposUre group, the Company shall, 

### v.ithin 7 days 

### of 

### anybf the 

### wents listerl 

### below 

### in this paragraph 

### (d)(5)(i), conduct the 

### initial e,(posure 

### monitoring followe6 by any 

### periodio or 

### additiolal orpoSure 

### monitoriag reqrrired by srbsection (d) of this 

### New Cherdcal Expos-ure 

### Limit section: ss.@)sghange-in the prgduction yolumee proeessirrisntfol 

### eErippra{"plr-sonaet or 

### work practices that may reasonably caise new or additional expostues to thc 

### PMN substamce;'].'t

- 

### +. 

### f

## i) l:.'ill ', 

### ...,"tt", 'j".""t''"';

### "

## ' c,r'r:r Lr 

### ''i'rfuil,itl; t;coui if i' l:

### s 'i-''l ::ci:'::!-\i 

## ':'li! 

## \.' ..,..:,l,'1.j:,:,'.rcrlr.Iriii,lrr::+l]}:i]0lji!,r..::,,t1]l,l:.1',ii.l,;ililst;l,.ll;ac...i 

## 1rI) wlelorcr elso fhe Cornpany has any i'easoq to sun^pe{'t a cha$ge

## tiat may reasonably result in 

### ncw r,:.tCtiiticnLrl exposures 

### to tlic FlVllrl 

### substalcc'



## (ii) In no eve,rt i1 t11c aclditioae{ e.<posure 

### monitorial requ1el.CIrt in 

### paras4ph 

### (d)$)(i) intended 

### to delay 

### implcm:ntation pf any necessiry cleanup 

### or othe,r remediai action. 

### Duringanyg1eanuporr9medialop9tationsth{,ma1occuq'boibrecommenqingadditionalex1.1ostr1e monitoring, the Company shall ensure that 

### potentiallV exfosed 

### lersons u-se at least

### tle r3sfi"i

## tW p.rateorron 

### spelfied in sqqsgctionJ:)ft" 

# f.:"T::f*-

# *j:t: *::""I*n? or more pTorective ,'. ,,."'.,.,'.1, ]"' ..': 

### respir4lory equipmeirt rleemed appropriate 

### by the best profqssional judgm.ent 

### of a qualifiecl oxpert

.,, ,,:i' 

# (6)'Notifi9?

# o

. <r1

# Wim 15

### workiqg {ays after reeerpt 

### of the lesults 

### of any expQsure 

### monitoring requiied by 

### this Order, 

### tlie Qompany qh411

### notifi eacl person wh6se exposure is represented 

### by

: that 

### pqonitorirg. Th9 nofice shall 

### fdentiS the 

### NCEL; ttre exposure. m.oni{oring results, trind

### any

t " , '.

. co-nespqrdrng respiratory protection reguired 

### by supqectipn'(e)' 

### Afected persons 

### shal be

### sotfqd in

### writing either 

### individually or 

### by posting the 

### information in anappropriate 

### md acceqsible 

### location,

# , (il) Whenever 

### flie NCEL 

### is eiceeded, the written 

### notification required by the preceding paragraph shall desctibe the action 

### being taken 

### by the Company 

### to reduce 

### inhalation exposure 

### to or 

### below the 

### NCEL, oi shall r.efer 

### to a document 

### aviilable to ttre person 

### which states the actions to be taken to reduco exposure.



# . - .

### ,(i),Exerrmtion"basedjbr.Objsoti'iesata,*,Ufhere the 

### Companyhasdqgumm{9ft-tigd, igrulqi.sE$,' ,r,+}i+ 

### reliable objective data 

### dernonstating that,

## wet under worst-case conditions, employee exposure to

### (d)(lXii)), tneo that exposir-re group is cxempt

### frcni 

### iiis lrIcr.r-Chr:r:riczrl 

### l}'.posurc 

### Iirait section

(except 1:aragraph (d)(5) 

### 'liriititional i.1 

### rnitorurg" a"rvl su

### bsectiol (f) '"i

## i(;iil, Rei:ordlieeping") aird the respirator requiroments in the Protoction in tfie

### $or$la':o sectiou

### of ihis 

### orr]er'. 

### Any such 

## ', objectu'', e data r4ust acounrlely charactedze actrlal eli?plcyee exposures to 'rfte PMI'T substanqe and must be obtained under conditionq closely tosembling 

### lte types 

### of rhatuizrlsrproccssqs, 

### go

# trol 

# - " methods. work Dracuces. and enviroaqt€o.talconditions 

### in the 

### Company's current workplace edata that may be useil 

### to d€rnoqstrate operations

### with the 

### PMN substance. Exarnples

### ofobjectiv that employee exposure 

### will npt exceeal the action 

### level, gven under worst.case contlitiony, inolude 

### information on tlie physicat and chernicai prrcperties 

### pt'the 

### IMN substance; 

### industry-wide shrfies, and/or laboratory test results, 

### (1) Gerleml. Whenever 

### tlte Compa[y has ooitlducteal 

### eripo$re monito.ring at aworkp.lace and the measured 

### iri accordence 

### with subsection 

### (d)'of this 

### New Chemical Exposure 

### Limit section airbome concenfration of the 

### PMIri substance 

### fbr any person who is reasonably 

### tikely to be exposed to the 

### PMN substance 

### by intalation exceeds the 

### NCEL, the Company shall provide those penlgns the respirators specified 

### in this subsection (e) (rather ttran ttre 

### respiratods) identified in

## the ' 

### pmtection in the Workplac.e 

### sectionof this Order), and shall ensure that the resPirators are used 

### (including training, 

### fit testing, and maintearrmce) 

### in accordance 

### with 

### OSIIA and 

### MOSH respiratory :3prre.";1,;lprotection 

### requirqents at

### 2S-($i.&-{.9-riQd$eidi.4?gE&fg$;&*+tJl[hen the Companyhas 

### notgg@;-$*"3,$*;14



# . measured the airborne conbentration.of the 

### PMN substance at a

### workplace 

### in accordance 

### with thisi: , ,-r ,-,,r,-...,.,-. -.. ..I.r,: i ..r,.,,r- r'-;t..-. :_.. :.r i,:,,r:-:i ..'

secticn, i.he Cq:lrrpatryshall qelect, 1;.'lvid.r:, rind ensuLr: ihat ilffl'sol]s -.r'ho 

### illi) 1't)asiiri#ly 

### lftely i;':-bc ,.'.]..'...,..'.'.l,I:, 

## ' ':,, ] / correspgnds 

### in llle

### following table 

### tc tire rne.r,Srrred

### airi;r:ina concenlratiola (*,r itl:r1oie 1'roleqtive 

### respiiator r,vhich conespon<ls,to aconcentration highet'than 

# measured). i - , '

,, f-,-f
. .-- :.-". , ..*
, ''"'":-i: .].in.l.,.',,..],i rl t1 , :r:.' 

# , cffiv{}}rNerrrolhr

## x,A}rrirCu{,#ilt ANB.fr,S-ff.SF*Q-IiSS,SF-$liiAHle-B,I*aP-&lU 

### Comcen'trat[CIu,

- 'of 

### Fl\fiN Substance 

# * NCEI, 

## .'' 

# : l0 x 

### NCEL

i : ' i.'.

.



### (I) AnyNlQSH-certified pbwered 

### air-punfiiUg re.spuator

### with ahood 

### pr 

# i[f**i und

### with applopriite gas/v-apor laqiO gus, organic vapor? or'substatrce specific) cartridges 

### in corypin{iotr mth HEPA filters. 

### (II) AnV 

### M0sH-certifi ed'continuous 

### flow supplied-air 

### respirator equipped 

### with a loose 

### fitting faeepiece, hood, or helmelm Contducted: 

### (I) Any 

### niiOSff-certified continuous 

### flow supptied-air respirator equipped 

# *itt aloose 

### fitting facepiece, 

### hood, or helmet

### hyEEL;

## :]-

')'"'' : '' -'-i' iriosu lir.ling far:epi+:r; ivi'lh ap[ii'u1.,,:i*tq p;as/vr:ritr 

### (acl.ll3o, 

## Sanic viwar, cir srihstance 

### spr;cifii) cartriclges 

### it: .combiiuttio-Lr'with 

### I{EPA filters, ' 

# .,, (III)Aly}IIOSI'I-.certifiecl contin,lous 

### flow su;p"ptleat-alr respirator equipped

: 

# '. ({vJ 

### rtniNllt::,:tr cerriij::f *:loi"L,qris florvsrapplicc:aii-

# iespiratr:r , , 

# ruelurtitdf*erytq,,WWt Ei 

## :, (I)

### tury'NIO SH;c ertin eo

# co olis

### ftgrl s urp p

### lied'air respirator equipped 

### '.'r,vith.a1oosefittingfuccpiece,ho.ot1,or.he1mct..,., I (II) 

## nry UI0SI{=ceititie'd nefal]ve pr*ss ulrcr (demancl) 

### supplierf,*air 

### i*tpitatol equipped 

### with a

### full

# facepicce. '

' 

## tf\qls 

## 9

# .P qc&fuTe-ttitt*-W.b4 

## * 50

### x NCEfl,

t:. .:..

,, 1 .i r' .i | ,- 

## (DAoy'}JIoSH-cer-tineoni,ryurffingfu11facepiec-,-*n,Iljl;;:;r#lj 

## #itt appropriate gas/vaBor (acid'ges, organic

### vapol o1 sub *urtriOges 

### in combination

### withNl00 (if 

### oil u*tqto]: 

### *:u3t), R109, or P100 

# filt or an,appropriate 

### canisterircorporating 

### N|00 

## (ifojl aerosols abseuO; 

### (U)A"V NIO SH-certifi ed powcryed ai1-p

### urift'q g'respirator 

### with atigh!- 

### fittirg fulI facepi*** *qrippea 

### wittr appiopriate gaq/vap0r (acid gas, organic vapor, or substa4ce specific) cartridges 

### in combination

### with HEPA filters. 

### (III)Axy NIO SH- certifi ed negative pressure (demand) s

### upplied-air respirator equrpped

### with a

### full facepiece. (IV)A-ny 

### NIO SH-certifi ed 

### cortinuous 

### flow supplied-air respitator equipp ed 

### with a

### tighrfifirqg tuIl fbcePiece. 

### supplied-air respirator" equl:pped 

### with a

### tight-fittrng 

### fulI facepiece.(II)A.n;,t'UOStI..certilic+t c;ontinuoliri flov,r sr'i6iijplied'min respi::ator equipped r,r,itha iilqhi..flti.ing Juli

# r'irr;;pior;e.
, .1 (irI)/nyhT1osI-I"c.i.l,i.iitict.i1;re:;sure.r]c;na.ltdor.oLherpr:sit.ivcpreSSL1remci-lc 

### ..''.,"..i,,t,pliert-aifrespirato'e,1i'ippedrruithdtight-flttingfu1i.facepi*'*. f !a _ :r.
. r

. l .;.r .. , ,. : . : i l, , .,. . , 

### :i:,(IV)A11yNIoSH.certi{iednegativi..p.rQssure(denrand)s9lf-contairref..

''':'''"-'i

. : :.e.. r-...:,",".f r..:1,... -j--_. ,,, ";.,:. , 

# =roo0,qNipt' -lrpqbSq44c,?&twr"iirg;iEtW', 

# Asv-'"lryeWl ' 

## '- : *,.' , ...1,,

(I)A:ry 

### NloSH-cert!fierl powered air 

### purifying

## ftll facepiece 

### respirator 

# ' equipped 

### with'au appropriatq gas/vanor (acid g4s, organig vapor, 

### or

subJdirce gpecifig) car,hidee'inl 

### comlinatiorr with HEPA

### filters' 

# iit g-l"la ".tplnet trpi is

### Auipp"d

# ;'itt a ufo1op"ut1gas{yapo1 

### (qcid 

### gx, organic vqpqr, or 

### duistmce s?egific) 9ar,qi4ce 

### in

## gomlq{i9i^wio greater, i: 

### (III)Any NIOSH-c€rtifi ed continuous flow 

### supplied-air lespirator equrpppd



# . ([1/)Any 

### NloSH-certified continuous 

### flow supplied-air 

### respirator rqulpped 

### with ahood or 

### helmet With evidence demonstrating 

### protection e level of 1,000 or greater. 

### (V1a"V 

### NfOSff-certified pressure-{emaual or other positive pressure mode 

### iuiUiLd-air 1espirator equipped 

### witli a

### firll facepiece. 

### IfNo Cartri&e Serviae 

### Life 

### iesling has been

### QpnaueAd;

### > 10(}0

### x 

### NCtrL

(ruax. 1SrS00

### x (it)Auy l..lTOSiJ-r;i;,:iifir# co;:iii rr.i,rr.ti; .ilc.v,r sitia;li-it:;.l"rrir .r'i:s1'-:ii'ato:r r.i1u-i'.pi;eel r,vitli a

### hti,,ii r:r 

### hcl iaat tuitii r:riiie;:crt ie tncrnirr.tiin,t4' .;;t'oter:tir:tt le:;cl

### of l,A{i0 ,', ', 1y1'75; , .,, :.'

a 

### (III)fury l.{I0SlI-crrrtifir-:r1 Jilesrjuro-clornanil or othcr 

### positivrl tr)l"nssttirc mocle surppliJm*gir 1i:)s1lil'ator eqi-ripped .,vith a

## ttll fireepiccr::. fprorr ldes eye/far;e

'FOSI{A h;rs assiE,rccl ,\PFs of 1000 j:'of certairr tyires of hoof"3yl.hr:imets,lvith fow-qr1d ail pLrriiyilrg; respira.Lr:r i; (PAP.I{s) or strpplied.air relP_irators (SAlts) rvliete lhe lanufq?hlrer canrlqrnonrt.ate ar1*quate air llor.vs to rraintajrr positive prosstre insidc the hoo{ Srlelnt*t in normalworkin[ conditions. i{o-wever, t}1eemploye.r must have evidence Plov-ided b1_!e respirator: :rrraulfactur:cr that thc tesfing of thesE respirators demonstratcs peqfuryance at a

. 1eveIofpiotectionof1,0006rgieatertoreceive*lAIq:jt..090.Thisleve1of, pe.forrrince,'can best tre clemonstrated by'periormiog uWorkplace Protection Factor (\YPF) 

## 'ir Simulared Wor(place Protectioh Faeto{(SWfEl study -o11luivalent teqting'Without tesiimg rtnta that *emnonstratcs alevei olflote.gtiou o"f.l:000" or great'er', all P,AFEs arld ,$Alds-with trrefunets/hoods ar"efo be treatCId aSioos+fitt-ftrg facetrrie*e respirators, and

I .. 

### Any 

### 1li$SH-ccrtified pressure-demancl or oflrer positive pressure mode (*. gl, oper:/closed 

### circuit) self-comtaimed 

### hraatfui4g 

### allparafus (SCBA) ,' 

## (:) Redfrctipqi 

### irl:+elpiratlT prqtectipl. After appropriate 

### respiratoryprotection has' been selected based on the results 

### of actual exposure 

### monitoring conducted at aworkplace 

### in 'tF accordance 

### with subsection (d) 

### of this New Chemical Exposure 

### Limit section, the Company shall 

### tion 

### in the'WorkPlace 

### not, atthat worlqplace, use the 

### respiratory protection requifed by the Protec section 

### of this Order (unless 

### it is the same as required 

### bythis New Chemisal 

### ExposureLimit section). Before the 

### Company rnay make any 

### reduction 

### in any respiratory 

### protection selected pursuant to this 

### New Chemical 

### trxposure 

### Limit section,the Comp?ny must 

### veriff, by 2 appropriate 

### in accordance 

### with palagraph 

### (e)(2). \Yhere the 

### PMN substance is manufactured,,)rl ' r I -.



### (1) Sirggj aLE1} +pJ.i-g1r,,, .. 

## (i) MgaUfqUfejliq_Qg1t5C_qllue4ili[rgglgniis, When a rrirluc ler+s t]iair

### the LQI,

## cf aph 

### (cX4xiil) t:i ineasu.i'et1, i,'rc Comirany sha1l the aria.lytic*l rnnl-hori (as describe.J iri pa.ragri estimate 

### potcntial expos Llrc rrsin;;gcriorally cstal-:lishecl ancl a,'cepterlstati.stical t rlethor-ls. 

## If the

l Company obtains an exposur* or.onitoring sarnplethat is mote than 10% abovethe aptual 

### IJQL

### of the analytical method, the Compan5r must ellsure that its workers 

### weaf at least a

### NlOSH-cer[if,ed supplied-air respirator operated 

### in pressure den'rand or othcr 

### positive pressure mode anrl eqi-rii:ped 

### with a

### tighf.fitting

### fgll fbcepiec.e. Arry re<lnctions in this respiratory prr:tection musf cornply 

### with pTagraph 

### (e)(3). The Company may 

### submil im lrnprovecl analytical method provicled that

## it complies 

### fuily with subsection 

### (c) of this 

### New Chemical Exposure 

### Lirnit seotion, 

### including th-e j. .. /-\/-\ 

### verification required 

### by subsection (c)(3).



## (ii) Clbdntrp and 

### Remedial*Actiqqs, During any special oleanup 

### or other remedial ,actionsthat may occur befor€oommencing 

### additional exposure 

### mbnitoring (asdiscussed 

### in paragraph 

### (d1sxii)), the Company shall exsure that 

### potentially exBosed persons use at least the respiratory 

### protection specified above 

### in this subsection (e) 

### for the measured airborne concentration, or more protective respiratory equipment deemed appropriate 

### bythe best professional 

### judgment of a

### qualified expert.
.,,.r,..,..].r.1 .:r'l;a-i:+ri''--tli,ill'i-i';'':'*'::i.-*r,;a':'.':;1'.3'-E:.1":.rt't'..'.,,-.

... .1, .l .i t, t'I I i;t 11.--. :,-i. ,' i. .-q -;; :'.1-':.'I:i',+j !'ii : 'r r-'I :-'r, ii,,,-... ..,!..-......".---- i-.,' .i I- .t, ,';, i..,i:r.-ii,ri .:, ,.,, ii: ;i ! .,li:

C.r-clei', ihe Cornprxry shail fiii,iirf-ain i.hc

### ii>llowing rccurit1s 

### itntil 30 yoerl:i ai'i.er ihe tlatethey ;iro
.i'i:' creiit(;cl, anrJ sha-ll mi.,kc therr., 

### r"rttlltir:le

### fi:r inspection iinrl cupyir'.g by 

### i.iliA in accoi''.lance ',vith



### verific;d.ion results obtainecl by 

### both laboratorles;

,:,..:.' r . .' . : . ' ': : .1, 'i '.'
' : ' " t i J I '''l

- .r '..'i

. ,l : , l:r' .,'^, 1 ,,. . ,.,, ,- ,,. requircr{nenls:of subsection 

### (cX3), incl*rtin,g, 

### iopies of the pignecl'certilicalion 

### ititetnent and the

t: t .. 

## (iii) Records 

### documenting either compliance

### withthe Good Lhboratory. Pr:actice 

## :.., ::_,

## : .

## . :...:

. .'.r'... 

### Standardsat40CFItPart,7g2,oi,*,*ofalabofat0,ryaccr:edi1edbytheAIIfAoranother
: 1 coqlparaore program approved 

### in advance 

### in

### writing by 

### EPA Where the Cornpany plEcts to not 'i: t (' cornpty 

### with TSCA GLP, such

### ricoids'*hull include the

### wriuen accreditation frorn the

### AIHA or l

; 

### (lv) Records 

### documentihg all'exposurO 

### monitoring dates, duration, and iesults

## of i

I each'sample

# taken; ,' 

# ; (") Recordq 

### docurnentinl the name, addrgss, 

### work shift, 

### job classification, 

### urd 

### work arzaof the person 

### monitored and 

### of all other persons whose expo.sures the 

### monitoring is intended 

### to represent;


# , :

# , ,

# , (oi), r{ny,conditions,thatmiglrf-;have affected the 

### monitoriag resuJlsir .:,*ii.i, .,..tirirtui,.'r,(i



## (vii) Notification of exposure 

### mpnitoring results required 

### by paragraph (c1)(6);.. -) ,i



### RISI( 

### NOTIFICATION



# - ,:]



# . .

### (ix) Reoords clocunrci.'tiag any s,pills, ieaku, rup{':rres q:i othel 

### breakdollq tha't 

### may 

## ,, ,: : 

# causenqworaridiri3nalexp9$uIP;......;,,.',',.,. t' 

# ' t*f
.

## rtc type

## ofreslirurvr,rytbi!'J a"'ioes 

### rvtim"by,pelolitmed personlif ?oy': 

## .:r: i -,.' '.,t;.1

## :'.;t.,,.:'....,.' ,'. ' .' .'. ' .::,'''.' ,i

# !.

. ' (xi)r Recorrls'tlocume$tlrg ?ny 

### abtiols taken to 

### mitigate gxposures to t1i9 P...l,v$ 

### '


# .. .

, :,' : l ] ., ,' :,:, suUstanoe;

# ' ': ;' 

# ' ' :"''"' ; . r '

# '

. .' .' ...', 

# .:'., i
: .1',:..' 

## (xii) Records clocunienting 

### lpliaiice on

### tle objective data dxemption in paragraph 

### : (dX7), 

### in;luding: (A) ths sourae ofthe. data, (B) 

### prgtocolg zind rcsu'lts 

### of any relevanl testiog 

### or 

### .-,"'i.';.. ." ' ,....i . ".,;1.. '' .'. , ... " '1.. : ' 

## 4ualjsis,(C)adesbriptionb[ 

# , 

# . i: ,i .: 

## ' : ...,

## .-. .:. ' -. .. :. expqsures

### wifl not exceed t]re actibn 

### level; @J other data 

### relwant to (h6 operatigns, 

### halerials

## and ' 

## ' ' '.,
. 't.: ,., : 

## . i. . , .l

## i .. :. 

## '. I

. - 

## I : , t r.

## ' :. ..,1 

### ., :1 

## . .. 

## q-plgy"qixposurps,rollplrbvE."i*rX"o. 

# ,, 

# ,., , . . ,.,.r,

# i, ., l,

: r ,t ) - ----- - ^izL!- ,^l-l ^- +L^ /anmrqo?i-r l-er. 

### (a) 

### If as aresult 

### of ihe test data 

### requiiei under theterms of this 

### orde1,the Company becomes awarethat the 

### pMN' substance may present a

### risk of injury to 

### health (or is so

### notified by EPA), the against such 

### risk, 

### into a

### Material bafetyData Sheet 

### ('MSDS'), as described 

### in 40 CFR ssction 721.7!Z{c),

### within 90 days

### fr-o* the time the Cornpany becom.es awaro 

### of the new 

### infbnnation' 

# If

### (b) The Compatly !+ust ensrrethat persong wf,o wi1l r+):eive tlie 

### PI@{ ntrlistaur:e 

### l}9m the



# . date the compar.y lecomes 

## u**e nf 

### th"

## o"* intoqlalio" ux"tibert in palaglaph (a) of

### this section, are provided an MSDS 

### containing flre 

### infornation .requiled,updu paragiaph (a)

### within 90 

# : -::-'--, 

# ---,I-- 

# --.',,.,.,-



# .. . ,i.: ..,-, ,,

## :

# . .. ...: . -:

. davs 

### froin the time

## the,Co;p*,

# O"*-i u*#lof tt 

### " 

### nq* 

## infoo'utiop' 

# ' ' : ,*FJY*Y.9:i:l:*:.:::.:.{-i.i:--_-:::'-1.i:,:.].,...r.,.i,:
i, 

### RA}d 

# :: , r HffilI-C:WIs-UH[0Str:QHrY;ffiH"-*:=:: (u)

# UatrcsJlaraa ,!ie;t"-4*''v,tnu['a"v"top.aq4i-!leqen;a 

# . : '

. 1,. .:r.. 1;--., i.,..:..,: ir I .- 

# . writtenhlT{d

# *ryTitrq Pfrgraur for 

### the.rMlri subgtancl. ineaoh -w-o,ll la:P:: The 

### Entten



# . , :progparn

### willjat a

### mininumrde.scrile ho,w the leguiremer.rF 

### of this section 

### for l1bels, 

### MSD!+

# and 

# . ; i :'. :; .' .',". . ..,'., ':' r_: '':1i: ' 'l : 11 '',' '' l'l i t l-. .:'' .,.. , r: ..r ', communicatiou 

### progran available, upon reques! 

### to all empioyeesl 

### cqnhctor employ'e$s, and

### their 

# desrgnatedr****.*";G;ayrervonanJ,*r**a"ffi;:'

- 

### prograq, including an exiqting pr-ogram esfablishtd under 

### tle OSIIA Hazard

# Cornmunication

. 

### Sl4ndad (29 

### CFR 1910.1200), 

### to oomply'with this paragraph 

### povided thpt thd existing hazanl 

### com4uSica6on 

### prograo satisfies the 

### reqpireurqts of

### tfis section, The

### witten program 

### sha[ 

# ' include the

# following: ' '



# (l) A list of chemical substanc€s

### known to be prestrrt in the

### wqrk area

### which are subject to :.;r;,.liilir':ia..1rs-GA&riotiqa.5{ie.}@onsent order.sigrred 

### byJ&psornpany;qq.to.eflS@&ispr$oEfi@X4 SNUR 

## al 

# . .- .

# - t.-+ 

### 40 C1F-part72l, subpart 

# E The 

### list 

### mult be maintained in each 

### work area where the 

### PMN

## (A) A statement 

### of the 

### health hazards(s) and precautionary measure(s), 

# if

any, 

### identified either 

### in paragraph 

### (f) of this section or 

### by the Company, 

### for the 

### PMN substance.



### (B) The 

### identity by which the 

### PMN substance may be 

### commonlyi i'. l CD)

### A staternent ol'exposut1 

### anl firccaltionary measurc(s)' 

### if any'



### itlentifietl either in paragraph 

### (f) of this sectiQn; 

### or by 

### &e Cornpany,

### for the 

### PMN substaflce'



## G, Th,: Company m.ay use

### sips, placmds, pror.:tlss shects, batch 

### tickels, opcrati'ng procedures, or other 

### slch writt<n 

## ,utoialr lo 1i"u 

### of

### affilrng labols

### to r.flclMdua] statiorratyprocess co.ntriiners, as lotrg asthe alternative metnOa ldenUn"s th6 conlarners to ,which 

### it is applicable and conveys 

### irifoiiriation specified 

### by subparugap.h 

### (b)1rxi) of;this section" 

### Any

### writtar mateiials must be 

### readily accessible to the employees 

### in thqii 

### wolk 4reas 

### thrwghorlt cach 

### work 

### shift'

(iii)- The Company-need 

### no! labcl Uortable.containers 

### inlo which the 

### PMN iliate zubstancC is hansfened from labeled 

### coiitaintrs, antlwhiqh ale intended 

### only 

### for the 

### imme
use 'of the employee who 

### perforfiis the transfer',



### (,v)TheCompanyshallnorremoveordefaceariexistirigla.beloncontainersqft}e pMN substnce. obtaine6 

## toq per .sons outside the'Company unles's 

### the 

### cofiainer is 

### imme6iately 

### relabeled with rhe 

### information specified 

### in subnaragtaph 

### (b)(lXi) 

## oithi. 

## .*tioo. rll e,nsure that each container of the substance 

### leaving its

### workplace 

### (2) The CoinPanY shi 

### for distributioa 

### in commerce 

### is labeled 

### in acconilance 

### with this subparagraph 

### (bx2),



### '(i)Thelabelshall,ataminimum,containthefoilowinginforrnation: (A)Theinformationprescribedinsubparagraph(b)(l)(i)ofthissection, 

### (B) The name and address 

### of the 

### manufactuer or a responsible party 

### who can 

### provide.additional 

### inforruition onihe,substanre.for,hazarcl evaluation and any,approPriategixrn,*r1 {ii':!:.'-'r!;; ernergency procedures.,1--



### {:i) 'lhe labct; 

### cr aitcuurtivc Fcmrs 

### of warriing, si all be 

### legiblc and 

### plomincnily dispiayed. 

## ,.,. . ... ,..:.., .-.ll i; ,.' ,t. ,..,. 

# :
. informt,iion may be rr:peqt,;d 

### jn othei'

## .ringuages.. ., ' 

## ,; ,,, 

### ,,. 

## . . ,t , ,t :., , .. 

# ." (5) 

### Ifthc label or ultornative 

### iorm oe.waming 

### is

### tqbe applied 

### to a

### miilu're oontaininl; 

### the 

### ,i .'., :..''j., ,, .,, ,'., :' .-::i 

### .. 1 

# : I '

# , PiVDtr substanco 

### in conibinaiion w-itfi any gther substance that iS cither subject 

### to another

### TSCA

# ' . .

, ....1.. 1. . .' ..,:-...', i 

# :; sectio.n 5(e) 

### Orderapplicable tq th9 Compaliy, 

### oisutje"t to u

### TSCA sbotion 5(a)(2) SNUR at

## 40

# - -.l ' 1--- ' ll :; '' :j-:i 

### ..:af.RPart72l,ryb,partIIordefinodas,a.h,4zaidotrs.clii:riiica1',unde[ttisoSHA'IJaz;id.',.'.



# 'il' ..., ,, ,,,.ta 1

# ,', .,.,

# ,, 

# : .. .,- 

# ., 

# . . 

# . :'.

. 

# '

# j cornr,il*icrrtiori standaxd (29

## cFtl lr00Jr001.the cqmopanymbypiesqibeoutrr'e lairel,.M$l)-s, 

## ,',..'.,'..,.:..,., 

# * ult"-ative forrir of warning, the mi)asures 

### tg contrpl.Wor.ker'exposure or -e.nvirqnmental 

## reieAse

. 

## : . . ,. .. :..:. ' '-: 1 tr: ..,'i..,,''-' .,.;'., ..'.:.1l"'1 ,' r"'-'1 ."'



## . .

# .. ryhich.the Company determi-nes pro'iride tlie 

### geatest degree 

### oiprotection. I{owever, 

### sliould

# thgq

. . 

## ,':



# . conhblmeasures 

### differ $om the applic.abtre 4geasrlres

### ryquird un{er 

### tlis Order, 

### $e Company

# m}!t ' 

## - seek a

### d*erriiiation of equivalenry 

### fot gucfl alternafive 

### co:rtolmeasures 

## pGtdt to 40

# CFR '

# . ] 

## ';-. i..'r: .,.,. : ,', ',i,.,.-,n.,'...

, 

### '.

## T2l..30beforepiescribingtheilunderdrissubpriragraph0)(r, 

# . . 

## ,', -- ,- ,-.



# . hazards 

### of the 

### PMN substange 

### or ways to protect against the hazards, this new 

### information must 

### be 

### I .: added

### to the tabel

## witlin'l montlis frbm ttr9

### tipe thi: Company becomes 

### awarsof the ne-w

# I j : 

### information. 

### If the 

### PMN s.pbstance is trot being man-ufactured, processed, 01 rised in lhe ' 

## ,. Company's

### workplacq the Company mirst add'the new inf<irmation 

### to the label before the 

### PMN ';r+:..,,r1",-isubsfaixse,isreintroduced 

### into thc Wor&ilaBecae4.111f';.1i'5'14:'ri''i1i;;1;1'r:*t$@;*+s,-- 

# ' - -'', r"i*ir*$rrIti:-\ :"r "



### of this section,

:

# . (v) Sigus and

### symptosli 

### of expouur', an{ any 

### medical conditions whigh are ,.',.r :, i l


# . .' Sectea to be 

### aggaval.d ty,",.lp",..pre 

### P

## ai,f.pq +rti{fa"e krrovm to the 

### Comlranv

# : ' ' 

## ': fY-iil 

### pren+irqa.y 

## lh*at*o to,<nnnolwprter srtposure aatUor

### env'ronmrxrtat

, tl release required by this Cirder, 

### or

## at+atye co"tol'measures which EPA !1as detemritred under 40 

## .-,,.', CFR 721.30 

### provide substairtialllthe sarne deer.oe

### olprotiection asthe 

### idixrtiEed 

### contol mqisures.



### (uiii.) Any generally applicabie prectrutions 

### for safe 

### hrindling and use 

### of the 

### PMN substance 

### which are 

### lnowi to the Company, 

### ;lslu6ingbppropriate hygieiric prirctices, 

### protective tsirirj;ru.;.-,ime?sdres:ifuiingpcpdifiagfl,.maialeoance 

### of contaminate4pq+lpwgatrdvrtroriedlIp-$$qilsspcnsg--. ,**,i



### to

### spills and leakssuch;:,; aiipropiil;tr: e,ngin+crihg rn'-rtrois, 

## ; :tk p:Li:c'icli, 

### ci 1;crscrral i:'':':iectivr; c*iuip;igr^t' 

### (x) Lrrergcncy 

### firl:t aid proicdure*s 

### knov'n to'dro 

### Conpany' 

## (xi) lho tlate of preparatioir 

### qf the 

### MSDS or rrf its- ]ast 

### rcvision'

, 

## (xii) lhp nane, address, and lelephone mrmber 

### of the ComP4nl 

### ol

# ano*o

, :

# . iesporisibli 

### parlyvho can

### provide additional 

### iuformation on the 

### rhenical substarroc and,any ,: ,appropriate emorgefl oy' procedirres. 

# : 6):ffnoret". 

# i* iofor-utiori is founri 

### or'}nown for any grven ca-tegory

## oi the MSDS, the ': . .'_. - ,. : :' ,,' ' - , . 't, ' i' : -.,.!': ''"., ,: : :,,,,. 

# , "orrydrt-*ttteMspstoi"iiralettitaoaee:icablehforh"tio"wifoild" 

# ,, ,, 

# ,, ' 

# ' (r,"; Ae 

### "n"nisA 

## irgrqdi*tt

# *" ".S*tiaf ry

### t4"

## yne b.ut

### tlq 

### sPecifio mpoiifo"

# v*igg'l* 

# . .



# . mixtue to 

### mixture) and similar hazardsi,th g

### cbmpanymay prepare one MSD-S 

### tq apply

### to all

## qf
i


## , :l ''. .:' I :, .,,1 ,.:

## .,".... .l

, - .'t :. . , .' . ,, ,,.t .'. ::., :-.- ..,, r,,,..: i. hriaards 

### of thp P.

### MN zubstance 

### or ways tp 

### protect agarnsfjhe hazardi, this nevv 

### rnfonn+fon 

### mrrslle



## .:'.. aililed 

### to the 

### MSDS

### wiihin 3 

### monthsftom thb timg the Company become,s awaiE of the 

### new '

l-:'':-- ''-:-.i -:--- --': '' ':"'



## .,..'



# . iinforination. 

### Ifthe PIrdN Substance is not be+Ug 

## -iiuf*toi,ud, prccessedr or used 

### ih the 

### company's wortcplace, ttre 

### comphy mirst adtl the new 

### infonlation to ttre MSDS before th9 

### PMN I substance is reintroduced 

### intothewor[plabe: 

### (6) The Comparry must ensure ttrat pers0ns receiv'rng the 

### PMN substance 

### from the Cgmpany are 

### provided an appropriate 

### MSDS

### with their 

### initial shipment and 

### with the 

### fimt shipme,nt. after

# an,,MgQsrisrerjgo&ifri provide theMSD.S.uaifhrthclsHPpad+$EiBd'x!tuEc-ryiaiaa.sr confairr srs 61 5eral 

### it to the person 

### prior to or at

### tlo time of shipment.^'ire lv.!$,";;'i ii-r itc 

### ''r';ii;plaie, anrl 

### mu;t er:er'r:



## (i') 'i'he Co:npa:iy 

## l i")t me'i'flJ; r'

## t Ji'::

## ! rri' i:i 

### ir t,c:.k r'ieai,. itrat 

### it is readily acses5ible d':'tirrg sach

### vrqli( 

## iidji 'i

# ) t1' nlt i 

### !$tts 

### 'i'licl i'iey ;ue 

### in t- 

### (3)TheMSDISm*y,t,.,kr.rtinanyftrrrn,inclurli;rgal;operatirrgpioceclrires,andmaybe .tlesigredtocovergroupsof.substarrcgsinawor.kareawh,*oitmaybemgrealFroPri4te!oaddress



## .: tlppotoo'lazard;ofaplocesqrathertlranindividual,substalces' I]oyever,1.n.allca1r.thg



# " muqt 

### bcirrovicted for the 

### PMN sub$ta iice anrl must bc 'rcadily accessible 

### requred.uuormalron : .,'' 

### durins each

### work shift. 

### to er-nployeeq 

### when ttrey are in 

### theirwork areas' : r."r ' '. j;, ,. , '.'. ':r'r; 

### (9) Xhe MSDS must be 

### printed in 

### Elelilbhowever, thq 

### inforthation 

### pay be i:epeated 

### in

,,, : ' ..-.. t--- 

## tal

# pgBlqvsq 3nt1 

### ---rrabEq The Coupany must eniure 

### thal employees are 

### provided 1.' 

### with,infprm4tigrr and trarrririg oa the 

### PMN substaq.cgl' 

### This informafioq 

### artl qaining must 

### be provirled at the

### tiue of gach eimplbyeels 

## inltia assignqent to 4wgrk 

## 1:"

# *1|"*.t ":

# l.^

.i

### first tiniq. 

### (1) Tlie informatiqn provitled to ernployees under this 

### pragraph shall 

### inclqde: 

# : (i) Therequng@gtrEofthis slqqqon 

### (iii)ThelocritionandavailabilitvofthewdJtenhazardcommrmicatiotrprogam,' required 

### untlerparagrap! (a) 

### of this sectio:r, 

### iricluding the list of substanrces required

### by subparagraph (a)(1) 

### ofthis section and MSDSs required 

### by.paragaph (c) of

### this section' ' 

### (2) The 

### taining providedto ernployees shall inolude: 

### ,.{i$e,=,rrrr.iii*.\,*-(i)Methodsagd&}EBc$Pti{in8ffiatniay;be+sed'+pdetectthepresenceg{releassio&Efilio;1'E*"t$-3i

the 

### pMN substance 

### in or 

### from an employeg's 

### work area (such as exposure 

### monitoring conducted

## (ij) T'.he 

### i:ofilntiai hn:i,; air. iroalth Jia::ar+is ,',ftirr; l]h4r-i'i sr-ll;sLance EIjsi,ccilierJ in

pa{irriraph (D

### oi'this sc;ction.



## (iii) Tlle measrrres emplcyees ca.n take lr; prr:'iecl tltt-':r'i:r;e;]ves anit the envirot]-'ilrent
i, Ji'orrr i.ire 

### PMN substancc, 

### incl,ldlng s:1'rccific procc,Jures iltctlo;trJiilny hi;r; 

### iiriplorncirit:d to 

### protect employee,s and fhe eir.rirorrmeilf -l'ro;n e,tp,rsurc to ilre P]'.4fi sribstrmr;t:, .inclurlin;5 a.tr'i1.,r;priiiteworlc ; practices, emergency procedures, personal protective eclu.iprtcnt, engineering controls, and oth.er measures 

### to control 

### worker exposure and/or en+rironmeiital release required under 

### this Order, 

### or alteinative con,trol measures

### which EPA has delennined unrl,:r/10

### CltR 12L30 provide the same iiepgee 

### of i:rrott:ction asthe speci,fted contral rneasllres.

)i 

## (i") The requirernentS of the hazard communication program developeel by

### the

., Company under this section, 

### inclnding an explanation 

### ofthe labeling system andthe 

### MSDS ' required 

### bythis section and guidance on obtaining and using appropri atehazard 

### information. 

### (e) De 

### Minimis Cciirceritrations.

### fne require*.mts o1 qls Hazard 

### Coitmunicatioq section do 

### not appiy 

### tq qua[tities of the 

### PMN substance 

### ftat are (1) preserit in the

### work area 

### only as a

### mixture 

# ' rmil 

### (2) at a 

### concentation not

### to exceed 1.0 percearl 

### byweight or

### volume (0.1 perce,lrt 

### by weight or 

### volume 

### if the 

### PMN subsiance is 

### identified as a

### poteirtial carcinogen 

### in paragraph 

### (f) of the Hazard 

### Communication 

### Progrim section 

### of

## tlis Order),

### This exemption is 

### not available 

### if the 

### Company has reason to believe that, 

### during intended 

### actiiities, ttre 

### PMN substance 

### in the 

### mixture may 

### be ;smerris:r,ftcslidsitralp&abp. re.ihe 1.0 or O.1

### percentJeudl:erlirheilea'4pJies*@his&dercontains (1) 

### New Che,lnical Exposure 

### Limits provisions that

### speciff a

### NCEL concentration less than the 

### dc

## ,,, 

# I .(0 llunranHeAth, 

# linqroarqcrllalX aUgO ls.

## Tle

# . . ,



# . followiug hunian 

### iicalih 

### ani envjronmcntal hazar:.l 

### and,ptellutionary stalcrhcdts shall appear ';r.r

. ': :' ' "'"::t: ' ' : ' 'rl . .. . 

### Ieachlabeiasspecifiedpparagraph(t)an<ltheMSI)Sa,.p*cifi.di,,p*agraph(c)Oftlrissr:ction: ' 

### j,:,(1).Humanhealthhazardstatements.Thirsubstaflce,inayfduse: J..,,:','j.;.'',,',,..''.ll '. ,. : -.. ....-.;. .. li

. 

# : li) skin

# irritation. r.. 'i.

### ""

# '.':.' ; 

### . \? "-r*- 

### l+.+Yl*-t. 1 ,. .,.,,., l 

### '.,.:' I ,.:.,., ,: 

# , . ', lii)9entrAnervqus.system."tr"..,]",tl 

# ,,,,., 

# : . .t i,
. ', , . :



## (i) avoid skin 

### costact. ,

, 

# ' (iii) avoid 

### breathjng the

# substance. : 

# I b.lo* u, 8-hour rim e-.werghted averarge 

### 9f 0'03 mglrri3' 

### ,...,ar*,r.,-,4S,),mr*.amqi6lurrdd+.rem,utio:rary statema.ents. No.ticejo,'.rrer.s$:;st'nrei"FtlE?4Ei-tt!iil,.!E#dl+!E:f,J+e-'--



### (i) disposal 

### restrictions aPPlY.

## :i '. r ,.. . '. :.

## '.:.. I ..:'.,,,, .., , .. :. 

# ' (S) 

### Exi;iins l{azdril Cor,U&mica.1iolt rrig{.U[",:The Corr,Farty.ngccl not take adfl{!'oUal actions

# if

;:,..., .-".- .--=l i --'t;,.'..,. ".,'; ,i:r.,....:. ."... ,'' .-' t 

### ,

### oirtiog p.grarns and procedures 

### sitisff-ttrfi feq,$rementi of thiS

### sec.Soli

# ' i'
. ,,^ r, i
'

### ' ',.1

### :... , . 

# ,:'. ' . ' ' '.1' :'':',.:'. . li ' ,. "' . ..'.' 

# ,:PMNsubstancebyauyot1ierpq#oni]::,..:

, ' ,,,,,, ,:i:'. 

# . (Z) Sirnsetlollowing 

### i.Ng,R- 

### S"bp*rc.4ph.(r)(1)'+rq efiiire 75 clqys,

### afterpromulgation 

# . .'



## _ j '-.::,,;"i'.,.,:....

..

## 1 ,, ,-' .' ll ,, .ofafinalsigiffcantnewuserule(:SNUR':)ggverningnhePMNsubstluceundersection5(a)(2) 

# : of

## f SCa udess the 

### Compt y

## i. ootil"d on or beiore 

### thal day

### of an action 

### ir. a F

### erlerl

# Court
, ' " . :. - ' , ' : . I 1

. . ,: :'.: :,^ .l 

### ,sgekingjudi{alreviewoftheSNUR.Ifft9Compau,4is,sonotified,subpragra,ph(a)(1)shaltqot .,j,.,'',.,.....,,,,1 SNUR have been resolved aadthe

### validity of the 

### SNUR affirmed' '-l : ; 

# :ill Notec 

# ,tSlUn. When EPA promulgates a

### final 

### SNiIR for the PIVIN substance and \, _--:r' gubparagaph 

### (a)Q) oxpires 

### in accordanc6rvrtl subparag€.ph (aX2), 

### fte Company shall 

### notify eac person 

### whom 

### it causes, encouragds 

### er sugge$ts to 

### marufacfure the 

### PMN5ubstance of the existence

i

## :-

'I



### (1) Noti4, in

### writing ary

# Pers;-r : .:,: l

. 1.. :. ' a ,' .r': issuance 

### of this consent 

### orderunder secrlon 5(e)

## orrsce,lhe P,MI-I 

### *"bstance is 

### sublectto the export 

### notification requirements 

### of

## rsc$ section 12(b) and 40 c-FR Part 

### 707 subpaTt 

## D' such notice 

### shall contain, 

### in the 

### fo1u-fo which 

### it appears 

### in this consbnt 

### ordet, the 

### following
,. 

### information:,(1) the ph,g*{ nurnber, and 

### (2) either 

### (A) the specific 

### chemical identity of the 

### PMN 'l substance, or 

### (B)

### if the specific c-hemical 

### identity is confidential, the generic chemical 

### identity'

of further 

### distribute'th* PMIN substance 

### to any other person, other than 

### for disposal,

1 

# '.*: ' tpletelYPolYrrrgrizerl' 

### until afr.erthe 

### PMI'{ substance has been corn

..11::: ir::i.;,:,i, r ,

### (3) ,

### campry 

### with trre.. same recpiiremenls a rrd :tesfrictions; if,zury,r'recluirerl 

### of the c0mpar'-y 

### in fhe Protection in tJre Worlqplace'

lnternet Address (URL) . http.//www.epa.gov

Recycled/Recyclable - Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper; UNITED STATES eTVIRONMENTAL PROTECTION AGENCY



### , OFFICE OF CHEMICAL SAFETY 

### (,:) ll-girti.rrf-.,.fy-lrarrE:<:1'li r'.rrd.$loli1::c." }'ic it'viriml:Llri ir

### ilj l;aialJraph 

### (b)' ihr: iJotr4ial$PFrf|LurroN PREVENrroN iiisiii!;utt> tlu: 

### PMII subst'i;;luc out'j lr'lctlro (

### 'ompix'ty li'"' tOr;]pt)raty tl

### anq;';if ar'il stola-[l{'' 

### in s!'LIcq

.. ' : .1 .., ', ' li "' ,rrltiiliito.rs 

### provitlcrt L\c

### f'ritrt"itrli tl'icc l'dir'l"lil'io:1'; I'il)'rt'14"t: 

# (t) Subscqualnt,!o auy srrr:ir cxcr:t.tt tr...:"111;t;1..r 7 ,:rnl} 5P0It

### 9t stoJ:.l8:: ()f :,;:)aJCi.i i.;nti.,iljc,.s, 

### ilrc 

### -:. ' ,, . . .1 :' PN)IN 

### subsiatr;emaybe dislrib'uied 

### only qq

### t[e ComF.,+Y or aPcrsorr 

### who hzis gi-ven

### theCltnf aaV



### .. the

### writterl agreernent reqriirctl UV 

### patugf'pfr 

# G)' , ' I '. i 

### containersandrcmovingorwasbipg.outthePMNsubstancenrayoccuronl,ywhileflrePi.Vlll substance is in the possesSiOn and 

### conhol 

### oftho Company or a person who has giveri tlre Company 

### (3),ftesealedcontainersmustbelabeledinaccordancewithpmagraph(bX2)ofthe Hazard Communication Program section 

### of this 

### Order' 

### (d) Recipient 

### Non-Copoliance. 

### If, at any tirrie afte,r corrmencing 

### disdributiol iri coumerce'of th€ 

### pm..{substancqtheCompanyobtaiuskrtowledge,thatarecipieotofthesu,bstancehasfailedto 

## *r"ely with any 

### of the coaditions specified 

### in paraepph (b) 

### of this 

### Distribution section

## or,Jer 

# ' new use 

### of fire pM.N substanoe (as 

### ilefined in 

### 40 CFR Part 721, Subpart E) 

### without submitting a ..,....-.r,,:iri.:sipifioantino;w,'usearotice,tq,nP"A, .the Company 

### sha1l'cr:asesupplyinljittetuitbistaficsifo{hatr:;"'" '- ' ' '



### recipient, unless the Company 

### is able

### to <looument each 

### of the

### following:

lnternet Address (URL)' http://wwwepa.gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled PaperijiSl.rji:rrii(.ji1 t,;t{li.iCn, Cr !r-ir.ll r,,;:,:i(;i.ii 

### iil ii r;i;r,liil'r:ii;:1: -'ri:'''r ':''r)

snbri-iil.{.iitil a l;i;31ifir:a,itf- flfi'',;Y Li:;{i r--tiii.icu 

### i+ [i,l].'i-" 

# ,'.. .,',..'.: or is awal.f, 

### of the tenn:; of the 

### signiticax; fir;r,vusil 

### ruli; [i;L tltr: 

### riMN substance and

### wi]l not engage 

### in asigrrificant now use

### without sr.rb,rriiliilg 

### asigrifir;ant nr,w use 

### noticoto l"lPA; 

### (3) If, a-ftu l,:cccivirrg a :;Ldi:r:wrertl 

### of ar r'jilr a-ace 1-raln arcciprent nn*Jcr

## -:OrT'::lrh (dX21 

### ol.flris 

### llistrjbutiorr scctiou, thr: Conrpany oLrtains l<no'"rleclg,: ihat tlie 

### recipicnt has failed 

### tc comply 

### with a*y of the conc{itions specifierl in palagraph 

### (ir)ofthis 

### ilistribuiion section, or kras engaged 

### in

j a

### significant new use 

### of the 

### pMN substance wi'rhout sr-rbrrrittirrg asignif icunt new nse noticel'ttl

i 

### EpA, the Cornpany 

### shall cease 

### supplying the 

### PMN substancc

### to that 

### recipien[ shall 

### notifii EPA 

### of the

### failure to comply, aird shall resume 

### supplying the PhrIN substance

### to that 

### recipient only upon 

### written notifipation from the

### Agency' 

### (e) Sunset 

### Following SNUR. 

## (1) Subparagraph 

### (b)(2) of

### tlis Distribution section

### shdl expire 75 

### inal SNUR 

### for the PIMI$ substance under section 5(a)(2) 

### of

## TSC'\ days after 

### promulgation of a

# f unless the 

### company is 

### notified on or beforq 

### thaf day 

### of an action 

### in a Federal 

### court seeiking 

### juilicial roview 

### ofthe SNUR. 

### Ifthe Company 

### is so 

### notified, subparagraph 

### (b)(2) 

### ofthis Dislribution sectiro^rqs4utoeEaFiseffiItilsnAl4otifies t'he companyin.waiting;thal'aHj&6tlffii1sr'na::I*:Etsiixi3r*ii1 

### court actions 

### ihvolving the 

### sNUR have been resolved and the

### validity of the sNUR 

### affitmed'

lnternet Address (URL)' http:i/www,epa,gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 1000/o Postconsumer, Process Chlorine Free Recycled Paper 

### ' .i .,' ',ii.i':"l,ll 

### l,li iii) ,., i : ;

. 'J_l I ; Ilt: l'i ;[.] l;tti-lS'i,ltcr)i] (rr'l.l'rr-")LlI OFFICE OF CHEMICAL SAFETY AN9 POLLUTTON'PREVENTIONOFFICE OF.GHEMICAL SAFETY .

must be 

### i* rvi:iting 

### mrl mi,st sp*oiJiic,;ily 

### include 

### ;iii

### jiri:triio :i;tj;ltiriteil ilr.llLe $j'lMURPSrlQrThumevEHrpr 

# :.. ,,i"fi:,.ii6sSignifigairtnr:wpses,tanrl-;rhir:hr'v,iulil 

### itrv;ik"rridniiiclrit::,.Xrileiloti.fl:at:l] 

# ':rit+ .,',.,,,,':,.,

' " ' ,. : .. ,' ,. : . . '. ." ..:. ... _' ' ' I 

# n*-ffioo.t+ $\tin ana'ex?irationbll:;'ibpaiat-rap^,!trxz)' such noticr:.rnav 

### lubstitulq

## h'rthe

# '
, 

### . .,,I... ' . '.- : ' -' 

# *r;tt* igrrooent rpquired fut 

### ihe introductory'clause of paragaph 

### (b)i sothat' 

### ifthe 

## Company

. '.,...., ,. --. , , 1] , ,,



### . 

### gorides S,"rch notice

### tu the

### pcrsolis 

### io:who;, 

### it disTibr.iict fJrc 

### ilMI'{ substanct:, 

### tltxr ttre

# (-ompirny

. is notrcquifecir to.obtqiu 

### froh such 

### perqols ltrc 

### rvrilten.agrqerrrurt.spccltiul 

## 4 pdaglapfi 

## , . ':,'',,'',..:.'-..',.':'.j.,,l'.' ': " :: ' ': ''i ' :. " ':"



## ,''.,,, :.. . .t. 1 

### 'Th" Compa,p., 

### shalldisiiose of

### th" e,Nr-N'tut;tqqct, dud, any waste

### sti:ani cortai+ins the,Plvfl{ ' ':: l- ." : . :
. substance 

### only as

### fplloWs, This 

### provision dOes

### not supersed3 

### o'

# p"'-pt *y 4ppticable 

### fedaal'

. ,-,.. ' , , t l, ,- . .- -. 

### state,mtl.locailaws.andre,gulationsiftlro,selawsarerriorestringentthantherequiibme'lrtsbelorry. ,:j 

### (1) [he PMN substance 

### must be disposed 

### of only by: 

## ,.'-



# . "i ' G) 

### incinuation (destruction anil

## t"*oua em"iet'cy

## oi 9i9'99y4,

## or 

# ' ' : '



## (iq uniergound rqiection con@! (cl+ss 1

### woll, derp

### we[ injebtion for hazardous

, -' i irfacture nrust 

### be rlisposcd 

### of only by: 

### {'2) Waste streams

### fiom 

### mail ivir.l: cfficiencY.ofl 

### gg -q9%); o'; 

## (i) inci neratiow (rtesfnr eiitj nlarrd:remi

. lnternet Address (URL)' http://www.epa,gov Recycled/Recyclable ' Printed with Vegetable Oil Based lnks on 1000/o Postcon=,irn*r, Process Chlorine Free Recycled Paper

# g.-'H\'? uNrrED 

### 'TATES eruvrnoruMENTAL 

### pRorEcroN AGENcy 

## ,{ OFFICE OF CHEMICAL'SAFETY

'.r.., l-i' '\ yi i,iti L-,;, i r. - --..,,.1. 1,r',irc.r r,.,u.ti r..tit;;;;,:7 fi' " (ri.) WaStC SftC;;:rUl; ir'{}f-{I l-ilit ii-tt;rii r;i' Li}ir.r-l'''r\'t' i/.' ' '' "',

, 

## /'i ''-

## ""' "' t{clestructic'r 4ni1r't,iticlvai i"[[ie;ir:iicy 

### of 99'9970); 

### cr 

## \- fii) unde;rgrountl injectiorr' con



## ,]
'.; 

## '|
: 

### BE-J#ffiE-Tg-V"["2-[fi18

. , ..1:.. .._: .: . r,,

' , 1' -, ":: . - 

## f'hisprovisiondoesnotsupers 

# , : ,,: :-,i ,: 

# , i 

# 'r ' r any

## prrairt*t* or 

### pulposeful release of the 

### PMN fegulations, The Company is 

### prohibited fron ; r --. 

### ,tuting, piocessing and use

### cpntaining the Ph4N substance? or any waste stream 

### from manufa( 

## ,] .:'



### G)

## fesrldg The Company shall maintain the

### following records 

### until 5years after the date 

### they *:.r,i,1.tte+are.tleateduridshall,make 

### tlreo a.vailable fonrir.xspggtionarrd.nopyingfuiBBAiiin.uoooddrce la.ith

section 

### 1l ofTSCA:
lnternet Address (URL)' http:i/www.epa.gov

Recycled/Recyclable . Printed with Vegetable OilBased lnks on 100% Postconsumer, Process Chlorine Free Recycled Paperlnternet Address (URL)' http://www.epa.gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumet Process Chlorine Free Recycled Paper

# g''-X\a uNrrED 

### srArE$ ENuRb'r.iMENrAL 

### pRorEcroN AGENcy 

# L%:-1:.,:::.::,j:L:.: ,,11;i,:r, 

### , 

## ,,.,1o"11|3'o"l ,P9 3o1u''o-

## '

# ''"; ''1;"" f"rt"; "r ' : ''
,:r,orbrr rrf

# tlii Orilci; (6)Iier:olrltCocr.rmeritingiir'r:'cietcrininatir;lsrrirrriiirr;rii:yLhljltoteetionirlt#,uifu{uf@aneverrtoN sccti'n ct'{liis CrCer llir-t 

### r:ltmiicli iri.otgctjvc r:1c''tin2-is 

### i':'i;erv 

## lc s

### t'; thc 

### ?}'4N rubst?llDo; 

# :' . r 

# I ": l:ial 

## of (7) 

## r ,.;645 re,ruircrl 

### hy1,;,: r15aJ;ir 

### (i). 

### cf';:c trl':',v 

### il:lll:3-],::1"11111: 

## t-i|l{.|s)l 

## ,.,, 

# '" 1,itj 

## :or*ra!.to*o*ong *qta..blisrLruTliurrl 

### impr'erncntxion 

### of tliehazard 

## golfl]cation' prngram requirdd

## tv *re 

## rt-ard foto*onieotion r'ogram section 

### ofthiq 

### or'l'er; 

### (9) Copies 

### of labels 

### reqyircd;rndar 

### lne lazarcl 

### Cgrnnrrlrication Progr-am sectioa

# ofthis

. 

# O:der; ,. : '. , l.::-i'.,... i, , t,

' :-

# - . ': :' '

# ' r:'ld 

### by the 

### Ilazard

# Corrmuqication ' ' Program section 

### oflliis

# Orcler; '.

. i. ..: Lr. .1, :.. t ., 

## 01) 'Records 

### documartinc 

## "oml.1il 3wlS.anr annlicable 

### maaufactur[g p-rocessrt$' 

### usq arul distribudop rpstrictiol.nslin tfr" 

### l,ra".rfa"t"r:rrg and 

### Disuibutiqnsegtons qf this

# OdE['
. ' 

### iricluding dist-ibutee.s' 

### writtei dgreemen,

### tto 

### conolY.]$th the 

### Distibut'ott section

# oft$ ordari 

### (12)Recordstlo***tiog*i'pliancewithzuryapplicabledisposalrequire'mentsqrder the Disposal section 

### ofthis ortler, inclutling method 

### ofdisposal, location of disposal sites, 'dates of,



# ' fitl ,obut'oce 

### dittosed' 'Where the estimated disposal volirnie is 

### not disposal, and volume 

### ofP



# . lnown to the 

### company and is 

### not reasonably ascertaihable by the 

### company, the company 

### must 

### maintainotherrecordswhichdernonstrateestablishmentan{implemgrrtationofaprograpthat
;

## ii..,..-. ensllres complieuree;rui:tli;any'applJeabl*;Cllposa'Li"equi.':{:illr)tlts;

'lnternet Address (URL) 'http://www.epa gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper'' ,,-i - UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

OFFICE OF CHEMICAL SAFETY i-..iii 1i :, :i

### i tiry',11,, ;1S ircrlrl ri&t.lP nqllUflflJyP R EVE Nr Io N



### ftr) appliggbdity, Theprovisiorrs 

### cf this itocordkeeping section are nFplicable 

### onl;rto a'ctivities rct h,Ianu{"aciLtrt}}.", it'ai:p1ica-*1':, iuLt[ ni-'f i'nli:cfivities;

### cf Llrr: 

### ci'tfie Cornpitny anr"[ ils {]i-rntr ?t"- " Company' s ctlstomel 5; -

rtrl 

## (*) ph4B. 

### Cqqtrol_l,lur&e,., IJnder the pap'erwolk-Iterluction 

### Act i-lntl its rr:gulations at5

### CljltPart
i 

### 73[,0,particularly 5 C.FR 1320.5(b), the 

### company is 

### notrequired to Iespond to

### this 

### "collcclion

### of rmthe 

### Office 

## of infonnation unless

### this Order displays a

### cuffentlyva,lid control numbet frc-^^*:^-

### -'-1--- - Management and Budget 

### (,,oMB,,),

# *d EpA so 

### infon:rs the

### company. The 

### "collection

### of



# ' pSCA $5(e) Consent Order has been approved under currently 

### valid 

### jnformation" required 

### inthis 

### ONIB 

### Control Number 2070-0012'

lnternet Address (URL) . http:/iwww.epa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

# g'*Xho- uNrrED 

### srArEs euvnoiit'deumL pRorEcnoN AGENcy 

# e"Voc i,, .,

# ,.., **'Tli,"l,:1,',9, 

# irfl ,1,,,,.r,,i : 

## !r. i(Y -../"_ -.

### . ) :. :
_.: . '
. .
_ _.

### . . "

### . . ,. -
. ... .'- . 

### 'Zt 

## padlu -i " '' 

## f..;

. r;. .''.- ;;.i.'.::r ;;;. j.i::...1i., i..1., -:-.'.... - - . may u;;carrionally 

### co:t'jtict r:'n ';ii:e 

### r;i:ll1i;':iicc ilispr:ctio'':':

# li Conip:rny 

### :'1i:''"t'*'t 

# n"t'#:::';:'J:;:r 

# *r.- 

# ,;i$ild assocrrriet{'w.ili ';ire i,'lv: rI 

### s*1"taa.e: 

### Jlj lat'ilj tate 

### $i"lt' ttoi''""i''oi1g -I'i?'\ Lrx s;rnrrol' 

### rllYlhl#,Itffi rtrlueHrrou 

# ' " ' : rt

## inl.i:rlaliol ;i:;'tiiieqt 8-' 1l:r-'s;:ircdull:;g tu'tt1

## urfl'l1iqt'ut1'fi


# . .: Cornp,-rriy 

### iir advaneo i:l; rcqtlui 

# ;;r;, iu"t".r"*,r.t,ii!'**o".."t',' L'ttt't;'.'*o'Jliri:i:irrrti'rtrrl"'ln':A'n'rr,';+"e"t '


## ,,,, .. I .,iil .r,r,'...', 

## : , '.. ',.,..

## '. ' .-. inciiltle,br! aronotliulile{i1o1+l}.E 

## 'o4qYrol8i, 

# ;: ; , . , ,:l 

### ,.

# .,,,:: '.,1, 

## ...i,iExpccterl.1aresantti*",*#it'cPL[,h[substanc"witib,,inrriiductiqnwithi4ttlq:,, ..:',. ',':',t -- ,..:... r'':" ''-I ..",...: r":.. -:. : ... .'' 

## Su1DIjCq[uenf12rnonth:i;'|..

gonducting an inspection,for that'i1u1prc se' 'rhe

### l]lllN u,rbrtunce aur:|.

## *ry r*r,,sonaLrly bc exposed io the Ph'{iN, Sullstzuir:e; 

### (3)Cunerrtjobtit[csorcatcgoneqrorworkerswho.

,

# , ' , (4) Existing exposrrg 

### monitoring daia

### foi workus who are 

### invollgd in

# activities

,, '' 'l''t :: "' t r associated

### with the 

### pMN substancg 

## u"a**J

# r* ubry be expo$ed 

### to the 

### P$,N sublance;



# : '' ' rliance 

### with this Order

### oi (6)Anyotherinformationreasona!lvre1atedtodetenrriningcomtr


## I 

## Ol gs44uybB9spq,.g' The Company shalf 

### resnon{ to such r-equgsts 

### wthiir a redsoflable 

### periodoftime,butinnoeventlaterthan3Qdaysafterrecei'vingEPArsrequesl}-Y!enreqrrested ".,1in,'writingby-EP.,A;th.,op*puoy:u.r",poos*,hull.beirrwriting.'To$hhiorlentth+inibenprt.iopjs','. 

### lnown to or reasonably ascertaiuable 

### by the 

### company atthe

### time of the 

### reques! the 

### compaoy's

InterRet Address (URL) ' http://www epa.gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled PaperUNITED STATES ENVIRONITTIEruTru PRoTECTIoN AGENCY



# .''.,' , oFrce or cseirllreeL serery 

## I ,. ....alrDRoLlrl]:JTi.EREVENTloN
c

# u.p*f."*riltu to

### )ii'Apn1iuart 11

## f'I:riopt' (b) 

### rlr'Jl ti': 

### protle'q1;n 

### 'rcurrcl+oulnh.$tt1]: 

# : '



## v" s.u.-#cjis$*]l4l,lrl'nlt,I,{Y.^{'.El:ir}I{:rlirlilris,ttliB*s'J 

### C*(}-}LS*EHT:SE-uH}B

# ' '
,
1 Ll ' .rJ vv y q'. "'a-. :. \--l ::.y-.."*:--. :

. rrjrder

### thir

## or4*r*o, be trans{''crri;rJwhcn 

### tlic company transru:s 

### iis lnte-rcsts 

### in the }-M}T

,:.',, .,.,.,I , :

,, . ,

# . , : 

### s*bstancq 

### inctu{ing t}re 

### right to 

### rnanufacti;n: the'PMN substztrtce, 

### to attr:ther person tlutside the


### fu) Relation 

### of 

### encemeni'f"Nosl 

# .":

# .t1l lfdt'aTfertqtuthlcomnrmrtothut":t*ul,l"Itili-:u*""' before EPA recewbs a notice ofcorrimenCement 

### of,manufadre (T-{OC")for the 

### PMJ! subgtqnce

.i. 

## ,, fromt1ieCompanypursuanato40CIR720'102,theSuccess1rrnIhterostmustzubmitanewPMN to 

### EFA and com,

### ply 

### fully with Section 

### 5(a)(1) of TSCA imrl40 

### CFRpartT20 before 

### co4r4encing manufacfure of the Ph4N

# substance' i 

### (2) 

### Aeg-liOC. $the transfer from the Companl' to thq Successor ur

## Intaltis 

# :T*': after EP.,,-{,receiyes,a;@@hqrsauressor'fJrdn{erest shall compiy

### withtle'tamspf'&isofder'':adih'11''i"!:'i'.c''t:i't} shall not be requitcd 

### to submit a

### new 

### PMN to EPA'

lnternet Address (URL) . http.//www.epa.gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer. Process Chlorine Free Recycled Paper:.\SEo sr4D$-



## g'' 

# Il'o'rn 

# r#j .

### :;li UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

WASHINGTON, D.C. 20460 r..1 I .r-:i,l' .: '1i,.: ljl-1,.i;.,'ii:':.i,it,':":,'.,"'''i '-'' I''": :'' 

### (1) !'l:r;ccessorjnl:ntctest"ric;utsapet:iolrotttsilt':ril':(l'rl:'ii;'':"7n'hli'e;ac1,:j;^e-lr': OFFICE OF CHEMICAI SAFFTY 

## ''
, i o lt r': ;o r,r

### l.rrttl'cturc'ti:c iil'vii''[ 'r:''br;

### ari""' incil 'iin g aAi'roPi]0Q$$b{pnevelrtox 

### (lrrinoai:y's fttl.l irrlctcst rntnc 1*.,-

## " ', rights tu,.rl 1er,1;1 1i.;$irities,

### thiough a 

### rlrursj'l 

### ior''-ir"nt 

## I 4'1e'J Liy.tlt* il'.,r1p4::v, a'; t'rat's:tr'ror' ancl 

## .-. ,.,. '.,:.
.... 't ,', ''.' r,1,," 

## ''' '

' t.trcfi*c,-,rrsor ir:t 

### Intt-rcrtl as trzu..i".[eica, ti'1',,:

### tr-rit xc,1.li'ii,; pc:si;rtr; 

### v",io licqitire l';s$ tli rq ''he

# flil 

# 'r .-r ...

# '' , I,ir4],l ,iu.bstarr.il 

### suili n,; n. iir;ens'r.e ,,'1i1ii l,:+" a'.1'rci:1u .+ 1il

# lild,, :

. 

# ri.*i. *o 

### m" putenl

# f manufacruring 

### rights msoqiatqri witJr thd 

### PMN

# t'lou-:", A

## lu*1ltot

# *

. 

# #;i-,5i.t" iircorrporatea,ucensed'oldoinq 

### bylinessin rihe!lnit"a;St"t"s ittuc",91'{alce

# with : 

## ,:,!:::Y,**::-.,_.j.,..l.i;',..1,';l:,1l.....,.1.-.,...-,..

'

# . | , (?,\,rt 

## *rfu, no.u*e.tit means the lggaf 

### in.tr,rm"n4.) uscd 

### to corwey thc irltcrests in the



## . : : .... : r : ',

. 

## prurN.rtrt^j", iqsluding 

### therightto 

## mt'tif;"tuq*jpM1 tutttooge' 

### toln tlie Companyto th9 

## --: ,. .: . .: . l ': ' Suciessor 

### in Literest.



## .. 

## . ,' ' '
. . 

# (ON '::',. 

# ..,, '., ,:,: ,,

# .'.,.,

# :'.,' , , . . , Company shall 

### prolide to tho S.uccassor irr Interest' 

### by registoed 

### mail' a copy

### of the Conse'nt , ...': . l]

. , , 

### or{er and the 

### .Notice ofTransfer" 

### doculent w,lich is 

### incorpollted by 

### r€f:rTc,e as

# Aqgq*t'

, 

### !othis Order. 

### (2)NoticetoEPA'Witirill0busiless'claysoftheeffectivedateofthehansfer'the Company 

### 3ha[ by registoetl 

### mail, submit the

### finlv executed Notibe

# "t",*:ii.:]::t^'O'

.. ..-,.....u;i.+ 

### ir..u.s."Environmental plotectiooag€Bqjrr*ldilii,r$foEf-rieu1s$lanagerBatBranch (7405);1200r*$'rr*{*:*i*+!i:"}df':'d
Pennsylvania Ave,nug 

### N'W', Wash 

### nglon'D'C' 2'0460'

lnternet Address (URL). http://www.epa gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 1007o Postcon*,lmer, Process Chlorine Free Recycled Paper 

### (1) Notice tq SucqqsPor 

### iq

### ' etn'';rle av ai irr'Li'c forj inr;p''x;::ior''

rnarrrrl'aoturcri. Copir.s 

### of ihc 

### i';;rnsl';i i)r:*:i"lrrx't mus1

### 4

## ""::'-''"'." -

. OFFIPE,OF CHEMICAL SAFETY 

### pLnsuanitoS<:r:tion11cf1,9f'lA,rr:'rlrtstt'oiirr:nft-co1i";,'r'll"c';ftrr::i"it''t'nilmustfimrdlliurloNPREVENrloN
or

### r;viiions v'i'j,:l.r cxprtjsr;l.y l.ri.)

### rlsfi:i 

### i::tLiiil

## / iiir' iiic

### f i/:l'l irlri'ilan':'r 

### r';iiler ihe 

### lcrns of 1'hi:i { .r'r'iat


### ft:) Liabilitv, \."1 :_;_._+ 

### ''' 

# ,r, The

### co,u,p*v shaiuic lia],rre 

### fbr complianee 

### with the reqLliremerts 

### ofthis 

### ordcr r'rtrtil 

### ilrr,-t-:ffq'ctiverla1eot{Jrct-ransti:rr1+sr;ri[tic1.ai;cv;..i,.,

: : .r:' 'n 

### order effective as

### of th.e rJ.ate oJ:

### traflsfr:r. I Ja :)iionshail be conitrued. La'1,r:olribit the

### Agency 

### fiorn taking ' enfrircement action against the 

### cornpany aftcr

## theleffe e date 

### of the transfe: 

### for actigns taken' or omissions made, during the

### time in

### which the

### comp*y **.rfactured, n'ott*led, used'alstrihutea 

### in eommerce, or disposed of the 

### pMN substance pursuant to theterms 

### of this consent 

### order

lnternetAddress (URL) . http://www.epa.gov Recycled/Recyclable . Printed with Vegetable Oil Based lnks on '100% Postconsumer, Process Chlorine Free Recycled Paper

# g'--Hh,- uNrrED 'TATES eruu,*o,uMENTAL 

### pRorEcTroN AGENC' 

# tffii ASHNGToN,DC zo4oo



### ,*t rr,,rrr,,r, to 

### mt;riii7 or.i';r'i:l:L: 

### slllrrit'prl'vc i;'ro'visi't'trs cf

### 'li il; O:::'lcr

# ' i'hc, cx1:r;srltr;s ?nd

# risks

' ttrl ih'o iltlcu:natiorr 

### EPA dcle-'mined 

### io iilentitic.il by 

### liFA riuring i';s : ,":r'iow 

### of l'i':;: 

### i)l'4lT :*tbrrtail';e

# " , ,

, 1';v-pr'1;;r;1'r;5

# ilii ::iirrl r,.,, ii'1,i ", ;.ji':rl i-tttltr: 

### i'r':a';:tblc

### ttl ltris O;'cirr' 

# g'o**"" in detennining whet-her 

### to anien(l or rcvoke

### $is Order' 

### EPA

### will consider all 

### rilcvant erminatiog' 

### iqcluding' u'here 

### information available at tho tirne the 

### Ageucymakes tlrat det t

### of th.; tr)st {latn or

### otilu m:c:.'iril:ron that supports 

### the li+dings inthis 'approPriatc, artY rcassessmen 

### otcl.er,arrexaminationofnewtest'dataor+therinf,or.rratiolqramalysis,andimyotherr.clev.rnt informatiPn. 

### .ificatiotorrwocaiionifepAdeterrninesthatthe;ctivitiesproposed BPA

### will issue amodi 

### ttr€reitrwilltrotplesentanuffea,sonableriskofinjurytohealthortheenvironrrierrtaridwillnot resultinsipificantorsubstmtialhuuanexpoSureorsutstantiale,nviroirme,lrtalreleaseinthe f the health 

### or eirvironmental offects 

## of absence 

### of data sufEcient to 

### pbrmit a reasoned evaluation o the 

### PMN substaoce. 

### In addition, the Company may 

### petition EPA at any time to make other 

### modifications to the Ianguage 

### ofthis Oriler' .EPA 

### will issue such a

### modification 

### if EPA tletermines fhat the ,'modi.ficatio:o.is'rrsefrrlTappropriatg.and'consistentwifh,thostrrrotulo:tu,li1:intmtiof,lthiiiaorde-Eas.:u:,i*..alr*,,,,.-

Internet Address (URL) . http:/iwww.epa.gov Recycled/Recyclable - Printed with Vegetable Oil Based lnks on 100% Postconsumer,.Process Chlorine Free Recycled Paper issued.

### ouat'*aho 

# g ft 'o- 

# r#j . tr'



### UN|TEDSTATEsENVlRoNMENTALPRoTEcTloNAGENcY

WASHINGTON. D.C. 20460

. i -.'-':'- -. -. ..t -...,t ..,, , .' ,,.,.i.' ,,. , ,'i '



## .. ,: '
: i -: , t'

. trjis

# ; " uier; a*d llcrCIby: agrccs 

### that ali 

### inJ'hrniatiln,hetr:in tiiat is clair-rred- ari r:on,f { rrntial i:y rilr: '' !,.' . :

. 

### con parry (pcr seorion 14

### of 

### llscA, 40

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# rt Date OFFICE OF CHEM



### OfficeofPollution PrevEntion andToxics


## Title: I- n .o..sto tratto 

# g Il -ro- 

# "Mj UNTTED STATE$ ENVIF9NMENTAL' PROTECilON AGENGY WASHINGTON, D

## C 20460

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### C. 20460

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## ty ihe COmpany ielevzint to

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### at al}

## crR Yart"' 

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### prior r:r 'subscqEent 

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### 3. cout-rclenJial Business Infonrra.tio_g, The successor 

### in Intuest hcreby: reasserts,



## . 

# --- relinquishes, 

### or
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### all Confidential Businqss 

### Inform{ion

# ('*!{-) claims 

### 1u$-by the Company' pursuant 

### to Section 

### 14ofTscA and

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### to

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# ffi*I* "modifies" is indicated, such

### molificatio, ,nun be explained 

### in detail 

### in an attachment tothis 

### Notice 

### of Transfer. Information which has been previously.disclosed to the 

### publi* 

### (*.{', ?

## *h:}yal identity 

### thatwas not claiured as

## cBI"-tth* orifiinat submitter) 

### wouldnot subsequentlybe 

### eligibk: 

### firr confidential freatment under this 

### Notice of

## Trlsfcl ,:.-., ,

## ', ,. :.,',, ,,.

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# rmj UNITED STATES ENVIRONMENTAL PROTECTION AGENCY



# FIilC e

### ofAutho,naed Officja1 

## fitt* of Authorized 

### Official Addlesq 

### City, State, ZJP Code OFFICE OF CHEMICAL SAFETY AND POLLUTION PREVENTION

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# rmj UNITED STATES ENVIRONMENTAL PROTECTION AGENCY WASHINGTON, D.C. 20460

OFFICE OF CHEMICAL SAFETY AND POLLUTION PREVENTION

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# n..Hon 

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,,I ii* UNITED STATES ENVIRONMENTAL PROTECTION AGENCY WASHINGTON, 

### D.C 20460 ' . 'i'.,' '


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# --"*,ffi'"=ji:)i ,,.i UNITED STATES ENVIRQNIUIENTAL PROTECTION AGENCY

\iVASHINGTON, D,C. 20460

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