# Exhaust Emissions Sampling 

# Dal-Italia, Muskogee, OK Six Emission Sources October 30- November 3, 2006**Ar~strong** 

# Environmental, Inc. Project W

..2516-06

Report Prepared For: Bob Hurt

Daltile 7834 C.F. Hawn Freeway Dallas, TX 7521 7

Report Prepared November 8, 2006 By: Armstrong**Environmental~** 

# Inc. 

# 1748 Hlavek Rd. Decatur, Texas 76234 (214) 631-0021

# I. Introduction II. Summary ID. Procedures IV. Appendices 

# TABLE OF CONTENTS

A. Calculation Summaries B. Continuous Emissions Monitor Summaries C. Analytical Summaries D. Field Data Sheets E. Equipment Calibrations F. Standard Gas Certifications Page 1 

# 2- 13 14-23

24-50 51- 139 140- 240 241 -273 274-294 295- 305

## SUMMARY OF EMISSIONS TEST DATA Table: 1 Plant : Dal-ltalia, Muskogee, OK Location : Glaze Line Baghouse (EPN 41) Operator : R. Taylor Test Date : 30-0ct-06 Repetition : 1 2 

## 3 STACK GAS Temperature, F 85.5 86.3 87.3 Velocity, fps 60.58 59.05 59.96 Volume Flow, acfm 21589.9 21045.3 21366.5 scfm 19996.5 19461.1 19818.3 seth 1199793 1167666 1189095 Moisture,% 2.39% 2.41% 1.94%



# - C02,% 0.00 0.00 0.00 02,% 21.00 21.00 21.00 

## SAMPLE Start Time, hrs:min 10:20 AM 11:40 AM 12:57 PM Finish Time, hrs:min 11:23 AM 12:43 PM 2:00PM Sample Volume, set 42.365 41.220 41.725 lsokinetic Ratio, % 101.1859 101.1609 100.5536 

## PARTICULATE Front Half Sample Weight, mg 10.01 7.16 7.61 Concentration, gr/scf 0.003646 0.00268 0.002814 Emissions, lbs/hr 0.625093 0.44723 0.478208 Back Half Sample Weight, mg 18.85 22.15 6.40 Concentration, gr /set 0.006866 0.008291 0.002367 Emissions, lbs/hr 1.177123 1.383538 0.402172 Total Particulate, lbs/hr 1.802215 1.830768 0.88038

## SUMMARY OF EMISSIONS TEST DATA Table: 2 Plant: Dal-ltalia, Muskogee, OK Location : Press Baghouse (EPN 40) Operator: T. Armstrong, G. Salinas Test Date: 30·0ct·06 Repetition : 1 2 3 STACK GAS Temperature, F 86.6 87.8 88.8 Velocity, fps 37.15 36.51 36.52 Volume Flow, acfm 18491.6 18172.4 18179.5 scfm 17152.9 16786.3 16659.7 seth 1029174 1007181 999579 Moisture,% 2.03% 2.22% 2.82% C02,% 0.00 0.00 0.00 02,% 21.00 21.00 21.00 SAMPLE Start Time, hrs:min 10:00 AM 11:25 AM 12:47 PM Finish Time, hrs:min 11:02 AM 12:27 PM 1:49PM Sample Volume, scf 42.600 41.539 41.400 lsokinetic Ratio, % 103.0065 102.6355 103.0697 PARTICULATE Front Half Sample Weight, mg 9.51 9.35 7.86 Concentration, gr/set 0.003445 0.003473 0.002929 Emissions, lbs/hr 0.506603 0.499881 0.418451 Back Half Sample Weight, mg 4.35 3.10 2.40 Concentration, gr/scf 0.001576 0.001152 0.000894 Emissions, lbs/hr 0.231727 0.165736 0.127771 Total Particulate, lbs/hr 0.738331 0.665617 0.546222

### SUMMARY OF EMISSIONS TEST DATA Table: 6 Plant : Dal-ltalia, Muskogee, OK Location : Phase II Scrubber Exhaust (EPN 29) Operator: R. Taylor, G. Salinas, T. Armstrong Test Date : 2·NOV·06 Repetition : 1 

### 2 3 

### STACK GAS Temperature, F 127.6 128.7 128.9 Velocity, tps 24.42 24.10 23.66 Volume Flow, acfm 42002.5 41458.6 40705.1 sctm 32589.9 31921.4 31479.1 seth 1955395 1915282 1888747 Moisture,% 14.32% 14.67% 14.42% C02,% 3.00 3.00 3.00 02,% 17.00 17.00 17.00 

### SAMPLE Start Time, hrs:min 9:15AM 10:40 AM 12:10 PM Finish Time, hrs:min 10:18 AM 11:43 AM 1:13PM Sample Volume, set 36.525 35.748 35.211 lsokinetic Ratio, % 100.4746 100.39"47 100.2762 

### CARBON MONOXIDE Concentration, ppm 89.57 132.24 126.6 Emissions, lbs/hr 12.73118 18.41058 17.38118 

### NITROGEN OXIDE AS N02 Concentration, ppm 22.02 22.75 23.02 Emissions, lbs/hr 5.141896 5.203383 5.19219 

### VOC AS Methane Concentration, ppm as CH4, WET 30.85 28.25 26.88 Concentration, ppm as CH4, DRY 36.00637 33.10801 31.4076 Emissions as CH4, lbs/hr 2.924472 2.633902 2.464008 Emissions as C3H8, lbs/hr 2.680864 2.414498 2.258756 Emissions as C, lbs/hr 2.193354 1.975426 1.848006 

### SULFUR DIOXIDE Concentration, ppm 0.116 0 0.123 Emissions, lbs/hr 0.037687 0 0.038599 

### HYDROGEN FLUORIDE Sample Weight, mg 0.00 0.00 0.00 Concentration, ppm 0 0 0 Emissions, lbs/hr 0 0 0 

### CHLORINE Sample Weight, mg 0.00 0.00 0.00 Concentration, ppm 0 0 0 Emissions, lbs/hr 0 0 0


### HYDROGEN CHLORIDE Sample Weight, mg 0.00 0.00 0.39 Concentration, ppm 0 0 0.254441 Emissions, lbs/hr 0 0 0.045537



# IO

## SUMMARY OF EMISSIONS TEST DATA Table: 7 Plant: Dal·ltalia, Muskogee, OK Location : Phase 

## II Scrubber Exhaust (EPN 29) Operator : R. 

## Taylor, 

## G. Salinas Test Date : 2-Nov-06 Repetition : 

## STACK GAS Temperature, F Velocity, fps Volume Flow, acfm
Moisture,% C02,% 02,% 

## SAMPLE scfm seth

Start Time, hrs:min Finish Time, hrs:min Sample Volume, scf lsokinetic Ratio, %**~** 

## ARTlCU LATE

## ~ Sample Weight, mg Concentration, gr/scf Emissions, lbs/hr Back Half Sample Weight, mg Concentration, gr /scf Emissions, lbs/hr Total Particulate, lbs/hr 

## 4

129.3 24.67 42426.7 31520.9 1891253

14.91% 3.00 17.00

1:40PM 2:43PM

34.773 99.15317

35.38 0.015699 4.242949

10.20 0.004526 1.223236 5.466185



# n 5

128.6 23.36 40187.1 31116.5 1866992

14.35% 3.00 17.00

3:05PM 4:08PM

34.339 99.18727

23.36 0.010497 2.800-:183

11.50 0.005167 1.378662 4.179145 6

129.5 23.93 41166.6 31996.8 1919807

13.89% 3.00 17.00

4:30PM 5:33PM

35.506 99.73715

29.93 0.013007 3.56?332

14.29 0.00621 1. 703691 5.272023

# III. PROCEDURES
The procedure for emissions sampling followed USEPA test methods as detailed in Title 

# 40: Code of Federal Regulations. The following methods were used: Method Title 1 

# 2

3 4 

## 5 6C



## 7E

10 

# 25A

26A



# 202 Sample and Velocity Traverses for Stationary Sources
Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S Pitot Tube)
Gas Analysis for the Determination of Dry Molecular Weight Determination ofMoisture Content in Stack Gas
Determination ofParticulate Emissions from Stationary Sources Determination of Sulfur Dioxide Emissions from Stationary Sources (Instrumental Allalyzer Procedure)
Determination ofNitrogen Oxides Emissions from Stationary Sources (Instrumental Analyzer Procedure) Determination of Carbon Monoxide Emissions from Stationary Sources Determination ofTotal Gaseous Organic Concentration using a Flame Ionization Analyzer
Determination of Hydrogen Halides and Halogens Emissions from Stationary Sources
Determination of Condensible Particulate Emissions from Stationary Sources 02 and C02 were determined using PyRite Analyzers.
PM. HF and HCI sampling was perfonned on each source according to the following:

EPN 40 20 3 60 

## minutes EPN 

## 36 24 2.5 60 

## minutes EPN 

## 29 24 2.5 60 

## minutes EPN 

## 35 8 7.5 60 

## minutes EPN 

## 30 8 

## 7.5 60 

## minutes



# 14

# Source geometry's are shown in Figures 1 - 6. The 

# HF, HCl, and CL2 sampling train was configures as follows: Glass Sampling Nozzle Heated Glass Lined Probe Heated teflon filter lmpinger #1

- 100 mls 0.1 N H2S04 Impinger #2

- 100 mls 0.1 N H2S04 Impinger#3 -lOOmis 0.1 NNaOH Impinger#4- 100 mls 0.1 N NaOH Impinger #5

- 

# 200 grams silica Gel Analysis was performed for HF and HCI on the solution from the 1st and 2nd impingers. Analysis for Cl2 was performed on the solution from the 3rd and 4th impingers. The PM sampling train was configured as follows: Stainless Sfeel Sampling Nozzle Heated Glass Lined Probe Heated Glass Fiber Filter Impinger #1- 100 mls H20 Impinger #2

- 100 mls H20 lmpinger #3

- 100 mls H20 lmpinger #4

- Empty Impinger #5 200 grams silica gel
PM analysis was performed on the probe wash, filter, impinger solutions, and the MeCI rinse and impinger extraction's. Continuous emissions were monitored for the Spray Dryer and Vertical Dryer as 

# follows:
Fuji 3300 CO analyzer 0- 100 EcoPhysics 70S Nox Analyzer 

# 0-60 0- 

# 100 ThermoEnvironmental 51 FID 

## 0- 

# 100 :. '·'· •'' 

## 49.9 ppm, 99.1 ppm CO 

## in N2 EPA Protocol 1 25 ppm, 51.0 ppm Nox in N2 EPA Protocol 1 49.8 ppm, 50.1 ppm, 100 ppm

802 in N2 EPA Protocol 1 19.9 ppm, 40.8 ppm, and 67.1 CH4 in Air 

## EPA Protocol I



# Continuous emissions were monitored for the Kiln Scrubber as follows:

# Fuji 3300 CO analyzer 0-200 EcoPhysics 70S Nox Analyzer 

# 0-60 0- 100 0- 100



# A schematic of CEM configuration is shown in Figure 6. 200 ppm, 99.1 ppm CO in N2 EPA Protocol 1 

## 25 ppm, 

## 51.0 ppm Nox in N2 EPA Protocol I 49.8 ppm, 100 ppm S02 in N2 EPA Protocol 1 19.9 ppm, 40.8 ppm, and 61.7 CH4 in Air EPA Protocol!

# Figure·1- Glaze Line Baghouse (EPN 41)

580 inches



# 0

126 inches stack Diameter
- 33 inches Point #1
- 1 inches Point #2
- 2.2 inches Point #3
- 3.4 inches Point #4
- 5.8 inches Point #5
- 8.25 inches Point #6 -11 .7 Inches Point #7
- 212 inches Point #8- 24.751nches Point #9
- 27.2 inches Point #1 0
- 29.1 inches Point #11
- 30.8 inches Point #12
- 32 inches

# Figure 2- Press Baghouse (EPN 40)

180 inches



# 0

204inches stack Diameter
- 39 inches Point 

### #1 - 1 .0 inches Point 

### #2

- 2.4 inches Point #3
- 5.7 inches Point 

### #4

- 8.8 inches Point 

### #5

- 13.3 inches Point 

### #5- 25.71nches Point 

### #7
- 

### 30.2 Inches Point 

### #8

- 33.3 inches Point 

### #9

- 35.8 inches Point 

### #1 

## o - 38 inches

# Figure 5 - Scrubber Exhaust (EPN 

# 29)

,,

' 88inches

·t43inches**~·--~--** 

### ----··-------- stack Daimeter
- 72.5 inches Point #1 - 1 .5 inches Point #2
- 4.9 inches Point #3
- 8.5 inches Point 

### #4

- 12.8 inches Point #5 -18.1 inches Point #6
- 25.8 inches Point #7- 46.7 inches Point #8- 54.4 inches Point #9- 59.7 inches Point #1 0
- 63.9 inches Point #11
- 67.6 inches Point #12- 71.inches1\) 1\) 

# Figure 6- Vertical Tile Dryer #7 (EPN 30)

46inches

150 inches

stack Diameter
- 

### 17 inches Point 

### #1 - 1 .1 inches Point 

### #2

- 4.25 inches Point 

### #3

- 12.75 inches Point #4
- 

### 15.9 inches\)

..N 

# Figure 7 - GEM Configuration

Instack Filter. Heated Probe
Heated Sample Line

Pump



### 8 ias Calibration Span Line FID Analyzer



## ' Heated 

### Manifold 

# I L-------.l
Sample 

### Processor ...... 1-- 

# co Analyzer**"-~-...**

r-**~** 

### NOx Analyzer**I-~-.**

......


### S02 Analyzer**~~-**



### Flowmeter 

### Cafibration Point



### Sample processor consists of two short stem impingers followed 

## by a 0.3 Pump 

### micron filter

# . -; .



## ..

# ·.

•I -1 0 ',**~,** 0 ::t;:

. I:,

. ,, ·-

1

......**~** i::. ; . '. 

### :< 

# ·c-:·-, J.·.**t.~** •
·.,·,

l'r•.'•



### , 

# .. •. t··

"-=. •• :,,
__ .··.• I. • 

# Appendix'·)\. .. . ', :.**~** 

### . 

### , '

:- :: 

# .**~·** : \ 

### .. · 

### ... : 

### ··--

·.·· 

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L.**~· ~-**  

### ....

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# .. '

## ..... .. ;.:-



### . • 

### ···.

### EMISSION TEST SUMMARY
PLANT: Dal-ltalia. MuskoRee. OK DATE: 30-0ct-06 PLACE: Glaze Line BaRhouse (EPN 41) RUN#: 1 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 22 NOZZLE DIAMETER {INCH.): 0.195 PARTICULATE WEIGHT (Front half mg): 10.01 METER COEFFICIENT (Y) : 0.972 PARTICULATE WEIGHT (Back half mg): 18.85 PI TOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): ·027 GAS METER VOL.(Cu.Ft.) : 45.194 PERCENT C02 0 BAROMETRIC PRESSURE 29.35 PERCENT 02 21 PERCENT CO 0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 33 STACK LENGTH(inchs): STACK AREA (SQ.Ft.) : 5.939574 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000207 STACK AREA (SQ. Ft.): 0 ENTER THE STACK AREA SHOWN ABOVE: 5.939574 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): 42.3647 VOLUME OF WATER VAPOR (STD. CU.FT.): 1.0355

FRACTIONAL MOISTURE CONTENT(%): 0.0239 DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 MOLECULAR WT. OF STACK GAS (WET BASE): 28.5814 STACK PRESSURE (inch Hg): 29.3301 STACK,GAS VELOCITY (ft/sec.): 60.5821 ACTUAL STACK GAS FLOW RATE (ACFM): 21589.9223 STANDARD STACK GAS FLOW RATE (SCFH): 1199792.54 PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0036 PARTICULATE CONCENTRATION (LBS/SCF): 5.21E·07 PARTICULATE EMISSION (LBS/HR): 0.6251 BACK HALF PARTICULATE CONCENTRATION (GR.ISCF): 0.0069 PARTICULATE CONCENTRATION (LBS/SCF): 9.81E·07 PARTICULATE EMISSION (LBS/HR): 1.1771 ISOKINETIC RATIO(%): 101.1859

POINTS STACK T. DELTA P SQUAR D.P DELTA H METERT. METER T. deg F INLET OUTLET 1 85 0.85 0.921954 1.10 70 70 2 85 0.86 0.927362 1.10 73 70 3 85 0.90 0.948683 1.20 75 71 4 85 0.85 0.921954 1.10 76 71 5 85 0.90 0.948683 1.20 78 71 6 85 0.95 0.974679 1.30 80 72 7 85 1.00 1 1.30 81 72 8 85 1.10 1.048809 1.40 83 73 9 85 1.30 1.140175 1.70 84 74 10 85 1.40 1.183216 1.90 85 74 ll 85 1.20 1.095445 1.60 85 74 12 85 l.lO 1.048809 1.50 85 74 13 86 1.40 1.183216 1.90 83 74 14 86 1.50 1.224745 2.00 85 75 15 86 1.50 1.224745 2.00 86 75 16 86 1.50 1.224745 2.00 87 76 17 86 1.30 1.140175 1.70 87 77 18 86 1.20 1.095445 1.60 87 77 19 86 0.93 0.964365 1.20 88 77 20 86 0.92 0.959166 1.20 88 77 21 86 0.97 0.984886 1.30 89 77 22 86 1.00 1 1.30 89 77 23 

### 86 1.00 1 1.30 88 77 METER T. 24 

### 86 0.88 0.938083 1.20 

### sa 78 AVERAGE 85.5 1.0458 1.4625 83.3333 74.2917 78.8125 

# ?4

### EMISSION TEST SUMMARY
PLANT: Dal·ltalia, Muskonee, OK DATE: 30·0Cf·06 PLACE: Glaze Line BaRhouse {EPN 41) RUN#: 2 TEST DURATION {MINUTES): 60 LIQUID COLLECTED (mls) : 21.6 NOZZLE DIAMETER (INCH.): 0.195 PARTICULATE WEIGHT (Front half mg): 7.16 METER COEFFICIENT (Y) : 0.972 PARTICULATE WEIGHT (Back half mg): 22.15 PilOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): ·0.21 GAS METER VOL.(Cu.Ft.) : 44.328 PERCENT C02 0 BAROMETRIC PRESSURE 29.35 PERCENT 02 21 PERCENT CO 0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 33 STACK LENGTH(inches): STACK AREA (Sq.Ft.) : 5.939574 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000207 STACK AREA (Sq.Ft.): 0 ENTER THE STACK AREA SHOWN ABOVE: 5.939574 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): 41.2202 VOLUME OF WATER VAPOR (STD. CU. FT.): 1.0167

FRACTIONAL MOISTURE CONTENT (%): 0.0241 DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 MOLECULARWT. OF STACK GAS (WET BASE): 28.5791 STACK PRESSURE Cinch Hg): 29.3346 STACK GAS VELOCITY (fVsec.): 59.0539 ACTUAL STACK GAS FLOW RATE (ACFM): 21045.3061 STANDARD STACK GAS FLOW RATE (SCFH): 1167665.96 PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR.ISCF): 0.0027 PARTICULATE CONCENTRATION (LBS/SCF): 3.83E·07 PARTICULATE EMISSION (LBS/HR): 0.4472 BACK HALF PARTICULATE CONCENTRATION (GR.ISCF): 0.0083 PARTICULATE CONCENTRATION (LBS/SCF): 1.18E·06 PARTICULATE EMISSION (LBS/HR): 1.3835 ISOKINETIC RATIO(%): 101.1609

POINTS STACK T. DELTA P SQUAR D.P DELTA H METERT. METERT. deg F INLET OUTLET
1 86 0.68 0.824621 0.90 76 76 2 86 0.77 0.877496 1.00 79 76 3 86 0.80 0.894427 1.10 83 76 4 86 0.80 0.894427 1.10 85 76 5 86 0.85 0.921954 1.10 86 76 6 86 0.87 0.932738 1.20 86 77 7 86 1.10 1.048809 1.50 87 77 8 86 1.10 1.048809 1.50 90 77 9 86 1.30 1.140175 1.70 90 78 10 86 1.40 1.183216 1.90 90 78 11 86 1.20 1.095445 1.60 91 78 12 86 1.20 1.095445 1.60 91 79 13 86 1.20 1.095445 1.60 81 79 14 86 1.40 1.183216 1.90 91 79 15 86 1.50 1.224745 2.00 91 79 16 86 1.40 1.183216 1.90 91 79 17 87 1.30 1.140175 1.70 90 79 18 87 1.20 1.095445 1.60 91 79 19 87 0.85 0.921954 1.10 91 80 20 87 0.82 0.905539 1.10 90 80 21 87 0.84 0.916515 1.10 90 80 22 87 0.90 0.948683 1.20 

### 90 80 23 87 0.91 0.953939 1.20 

### 90 80 METER T. 24 87 0.85 0.921954 1.10 90 80 AVERAGE
86.333333 1.0187 1.4042 87.9167 78.2500 83.0833

### f)~
..... uPLANT: DATE: PLACE: RUN#: 

### EMISSION TEST SUMMARY Dal·ltalia, Muskogee, OK 30·0CI·06 Glaze Line BaRhouse (EPN 41) 3 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : 0.195 PARTICULATE WEIGHT (Front half mg): 0.972 PARTICULATE WEIGHT (Back half mg):

0.84 STATIC PRESSURE (in. H20): 17.5 7.61 6.4 ·0.25 0 21

0 GAS METER VOL.(Cu.Ft.) : 44.89 PERCENT C02 BAROMETRIC PRESSURE 29.35 PERCENT 02 PERCENT CO FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA (Sq.Ft.) : NOZZLE AREA (teet): FOR RECTANGULAR STACK 33 STACK LENGTH(inchs): 5.939574 STACK WIDTH(inchs) : 0.000207 STACK AREA (Sq. ft.): ENTER THE STACK AREA SHOWN ABOVE: 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD. CU.FT.):

FRACTIONAL MOISTURE CONTENT(%): DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH): PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): BACK HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): ISOKINETIC RATIO(%): 5.939574

41.7247 0.8237 0.0194 79.0000 28.8400 28.6301 29.3316 59.9552 21366.4831 1189095.14

0.0028 4.02E·07

0.4782

0.0024 3.38E·07

0.4022 100.5536

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T.

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 deg F INLET 87 87 87 87 87 87 87 87 87 87 87 87 87 87 87 87 87 87 88 88 88 88 

### 88 88 87.25 0.81 0.9 0.85 0.921954 0.85 0.921954 0.86 0.927362 0.84 0.916515 0.92 0.959166 1.00 1 1.20 1.095445 1.40 1.183216 1.40 1.183216 1.30 1.140175 1.10 1.048809 1.40 1.183216 1.50 1.224745 1.50 1.224745 1.40 1.183216 1.30 1.140175 1.20 1.095445 0.87 0.932738 0.85 0.921954 0. 90 0. 948683 0.93 0.964365 0.87 0.932738 0. 76 0.87178 1.0342 

## po 1.10 1.10 1.20 1.10 1.20 1.30 1.60 1.90 1.90 1.70 1.50 1.90 2.00 2.00 1.90 1.70 1.60 1.20 1.10 1.20 1.20 1.20 1.00 1.4458 78 82 84 

### 86 87 87 88 

### 88 89 90 

### 90 90 

### BO 89 89 90 90 90 90 90 90 

### 90 90 

### 90 87.7917 METERT. OUTLET 78 78 78 

### 78 78 78 78 78 79 79 

### 79 79 

### 79 79 79 79 

### 79 80 80 80 80 80 0

80 METER T. 80 AVERAGE 78.9583 83.3750

### EMISSION TEST SUMMARY
PLANT: Dal·llaha, Muskogee. OK DATE: 30·0Ct·06 PLACE : Press BaRhouse (EPN 40) RUN#: 1 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : NOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : 0.2473 PARTICULATE WEIGHT (Front half mg): 0.994 PARTICULATE WEIGHT {Back hall mg): 0.84 STATIC PRESSURE {in. H20): GAS METER VOL.(Cu.Ft.) : 44.539 PERCENT C02 BAROMETRIC PRESSURE 29.35 PERCENT 02 PERCENT CO FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA (Sq.Ft.) : NOZZLE AREA (feet): FOR RECTANGULAR STACK 39 STACK LENGTH(inchs): 8.295768 STACK WIDTH(inchs) : 0.000334 STACK AREA (Sq.Ft.): ENTER THE STACK AREA SHOWN ABOVE: 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD. CU.FT.):

FRACTIONAL MOISTURE CONTENT (%): DRY BASE.: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ftlsec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH): PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR.ISCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): BACK HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): ISOKINE.TIC RATIO(%): 8 295768

42.6000 0.8849 0.0203 79.0000 28.8400 28.6194 29.3257 37.1507 18491.6348 1029174.15

0.0034 4.92E·07

0.5066

0.0016 2.25E·07

0.2317 103.0065

POINTS STACKT. DELTAP SQUARD.P DELTAH deg F METER T. INLET METER T. OUTLET
1 2 3 4 

### 5 6 7 8 

### 9 10 11 12 13 14 15 16 17 18 19 20 86 86 86 86 87 87 87 87 87 86 85 87 87 87 87 87 87 87 87 85 0.42 0.648074 0.43 0.655744 0.43 0.655744 0.45 0.67082 0.45 0.67082 0.46 0.678233 0.42 0.648074 0.40 0.632456 0.35 0.591608 0.33 0.574456 0.42 0.648074 0.50 0.707107 0.56 0.748331 0.60 0.774597 0.57 0.754983 0.44 0.663325 0.35 0.591608 0.29 0.538516 0.22 0.469042 0.25 0.5 1.40 1.40 1.40 1.50 1.50 1.50 1.40 1.30 1.20 1.10 1.40 1.70 1.90 2.00 1.90 1.50 1.20 0.96 0.72 0.82 74 77 

## so 82 83 84 84 85 84 85 82 85 86 87 87 87 86 86 86 86 74 74 74 73 74 75 75 76 76 76 76 77 77 77 77 78 78 78 78 78 18.8 9.51 4.35 ·0.33 0 21 

### 0

0

86.55 0.6411 1.3900 83.8000 76.0500 79.9250 

# 27

### EMISSION TEST SUMMARY
PLANT : Dal·ltalia. Muskogee. OK DATE: 30·0Ct·06 PLACE : Press Baghouse (EPN 40) RUN#: 

### 2 TEST DURATION (MINUTES): GO LIQUID COLLECTED (mls) : NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : 0.2473 PARTICULATE WEIGHT (Front half mg): 0.994 PARTICULATE WEIGHT (Back half mg):

0.84 STATIC PRESSURE (in. H20): GAS METER VOL.(Cu.Ft.) : 43.69 PERCENT C02 BAROMETRIC PRESSURE 29.35 PERCENT 02 PERCENT CO FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA (Sq. Ft.) : NOZZLE AREA (feet): FOR RECTANGULAR STACK 39 STACK LENGTH(inches) : 8.295768 STACK WIDTH(inches) : 0.000334 STACK AREA (Sq.Ft.): ENTER THE STACK AREA SHOWN ABOVE: 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD. CU.FT.):

FRACTIONAL MOISTURE CONTENT (%): DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE):

• STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ttlsec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH): PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): BACK HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): ISOKINETIC RATIO(%): 8.295768

POINTS STACK T. DELTA P SQUAR O.P DELTA H

1 2 3 4 5 6 7 8 

### 9 10 11 12 

### 13 14 15 16 17 18 19 20 deg F88 

### 88 87 88 

### 88 88 88 

### 88 87 87 87 

### 88 88 88 

### 88 88 88 

### 88 88 

### 88 0.44 0.663325 0.46 0.678233 0.55 0.74162 0.57 0.754983 0.57 0.754983 0.44 0.663325 0.36 0.6 0.29 0.538516 0.25 0.5 0.22 0.469042 0 36 0.6 0.39 0.6245 0.40 0.632456 0.40 0.632456 0.38 0.616441 0.42 0.648074 0.42 0.648074 0.40 0.632456 0.37 0.608276 0.33 0.574456 1.50 1.50 

### 1.80 1.90 1.90 1.50 1.20 0.96 

### 0.83 0.73 1.20 

### 1.30 1.30 1.30 1.30 

### 1.40 1.40 1.30 1.20 1.10 41.5395 0.9414 0.0222 79.0000 28.8400 28.5998 29.3243 36.5093 18172.3544 1007180.79

0.0035 4.96E·07

0.4999

0.0012 1.65E·07

0.1657 102.6355

METER T.

INLET 78 86 87 

### 88 89 89 

### 88 87 87 87 81 

### 88 89 88 89 89 89 89 89 88 METER T. OUTLET 77 77 77 78 

### 79 79 79 

### 79 79 79 

### 79 79 79 79 79 80 80 80 80 80 20 9.35

3.1 ·0.35 0 21 

### 0

0

87.8 0.6291 1.3310 87.2500 78.9000 83.0750 

# 28PLANT: DATE: PLACE: RUN#: 

### EMISSION TEST SUMMARY
Dal·ltalia. Muskogee. OK 30·0Ct·06 Press Baghouse (EPN 40) 3 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : 0.2473 PARTICULATE WEIGHT (Front hall mg): 0.994 PARTICULATE WEIGHT (Back half mg):

0.84 STATIC PRESSURE (in. H20): GAS METER VOL.(Cu.Ft.) : 43.617 PERCENT C02 BAROMETRIC PRESSURE 29.35 PERCENT 02 PERCENT CO FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA (Sq.Ft.) : FOR RECTANGULAR STACK 39 STACK LENGTH(inchs) : 8.295768 STACK WIDTH(inchs) : NOZZLE AREA (feet): O.OD0334 STACK AREA (Sq.Ft.): ENTER THE STACK AREA SHOWN ABOVE: 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): VOLUME OF WATER VAPOR (STD. CU.FT.):

FRACTIONAL MOISTURE CONTENT(%): DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH): PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): BACK HALF PARTICULATE CONCENTRATION (GR.ISCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): ISOKINETIC RATIO(%): 8.295768

41.4003 1.2003 0.0282 79.0000 28.8400 28.5346 29.3250 36.5236 18179.4977 999579.435

0.0029 4.19E·07

0.4185

0.0009 l.28E·07

0.1278 103.0697

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

1 2 

### 3 4 

### 5 6 7 

### 8 9 10 11 12 13 14 15 16 17 18 19 20 deg F
89 88 89 

### 89 89 89 

### 89 89 89 

### 88 87 89 

### 89 89 89 90 90 89 89 87 0.39 0.6245 0.37 0.608276 0.36 0.6 0.40 0.632456 0.38 0.616441 0.42 0.648074 0.43 0.655744 0.42 0.648074 0.39 0.6245 0.37 0.608276 0.41 0.640312 0.48 0.69282 0.50 0.707107 0.52 0.72111 0.54 0.734847 0.40 0.632456 0.37 0.608276 0.30 0.547723 0.27 0.519615 0.24 0.489898 1.30 1.20 1.20 1.30 1.30 1.40 1.40 1.40 1.30 1.20 1.40 1.60 1.70 1.70 1.80 1.30 1.20 1.00 0.90 0.80 INLET 79 86 87 87 88 88 89 

### 89 89 89 83 

### 89 89 

### 89 90 90 90 90 

### 89 89 OUTLET 79 79 79 79 79 79 80 80 80 80 80 80 80 80 81 81 81 81 81 81 25.5 7.86 2.4 ·0.34 0 21 0

0

88.8 0.6280 1.3200 87.9500 80.0000 83.9750 

# 29

### EMISSION TEST SUMMARY
PLANT: Dal-ltalia, Muskogee, OK DATE: 2-Nov-06 PLACE: Phase II Scrubber Exhaust (EPN 29) RUN#: 

### 1 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) 

### : 

### 129.7 NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg): 0 METER COEFFICIENT (Y) : 0.994 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 GAS METER VOL.(Cu.Ft.) : 35.432 PERCENT C02 3 BAROMETRIC PRESSURE 30.15 PERCENT 02 17 PERCENT CO 0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 72.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 28.6684 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.): 0 ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): 36.5254 VOLUME OF WATER VAPOR (STD. CU.FT.): 6.1050

FRACTIONAL MOISTURE CONTENT (%): 0.1432 DRY BASE: 

## so.oooo MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 MOLECULAR WT. 

### OF STACK GAS (WET BASE): 27.5618 STACK PRESSURE (inch Hg): 30.1529 STACK GAS VELOCITY (ft/sec.): 24.4186 ACTUAL STACK GAS FLOW RATE (ACFM): 42002.4699 STANDARD STACK GAS FLOW RATE (SCFH): 1955394.53 ISOKINETIC RATIO(%): 100.4746 POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. deg F INLET OUTLET 1 129 0.10 0.316228 0.54 44 44 2 129 

### 0.12 0.34641 0.64 46 45 3 127 0.13 0.360555 0.70 50 45 4 128 0.15 0.387298 0.80 51 45 5 128 0.15 0.387298 0.80 53 46 6 126 0.20 0.447214 1.10 56 46 7 126 0.20 0.447214 1.10 57 47 8 125 0.20 0.447214 

### 1.10 57 47 9 126 0.14 0.374166 0.76 58 47 10 128 0.14 0.374166 0.76 58 48 11 128 0.12 0.34641 0.65 59 48 12 129 0.11 0.331662 0.60 60 49 13 129 0.14 0.374166 0.76 58 50 14 129 0.16 0.4 0.87 61 51 15 128 0.18 0.424264 0.98 62 51 16 128 0.20 0.447214 1.10 63 51 17 128 0.22 0.469042 1.20 64 52 18 128 0.23 0.479583 1.25 64 52 19 127 0.22 0.469042 1.20 64 53 20 127 0.22 0.469042 1.20 64 53 21 127 0.20 0.447214 1.10 

### 64 53 22 127 

### 0.17 0.412311 0.93 64 54 23 127 0.15 0.387298 0.81 64 54 METER T. 24 

### 128 0.13 0.360555 0.71 64 54 AVERAGE 127.58333 0.4044 0.9025 58.5417 49.3750 53.9583 

# 39

### EMISSION TEST SUMMARY
PLANT: Dal·ltalia. Muskogee, OK DATE: 2·NOV·06 PLACE: Phase II Scrubber Exhaust (EPN 29) RUN#: 2 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mls) 

### : 130.6 NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg) : 

### 0 METER COEFFICIENT (Y) : 0.994 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 GAS METER VOL.(Cu.Ft.) : 35.462 PERCENT C02 3 BAROMETRIC PRESSURE 30.1 PERCENT 02 17 PERCENT CO 0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 72.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 28.6684 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0 ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): 35.7477 VOLUME OF WATER VAPOR (STD. CU.FT.): 6.1473

FRACTIONAL MOISTURE CONTENT (%): 0.1467 DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 MOLECULAR WT. OF STACK GAS (WET BASE): 27.5225 STACK PRESSURE (inch Hg): 30.1029 STACK GAS VELOCITY (ft/sec.): 24.1024 ACTUAL STACK GAS FLOW RATE (ACFM): 41458.6419 STANDARD STACK GAS FLOW RATE (SCFH): 1915282.49 ISOKINETIC RATIO(%): 100.3947 POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. deg F INLET OUTLET
1 129 0.13 0.360555 0.71 55 54 2 129 0.15 0.387298 0.82 60 

### 55 3 129 0.15 0.387298 0.82 63 55 4 129 0.20 0.447214 1.10 65 55 

### 5 128 0.20 0.447214 1.10 69 56 6 129 0.18 0.424264 

### 1.00 69 57 7 129 0.20 0.447214 1.10 70 57 8 129 0.21 0.458258 1.20 72 58 9 129 0.20 0.447214 1.10 72 59 10 129 0.18 0.424264 1.00 71 60 11 129 0.16 0.4 0.90 72 60 12 128 0.13 0.360555 0.73 72 60 13 129 0.10 0.316228 0.56 65 61 14 129 0.12 0.34641 0.67 69 61 15 129 0.13 0.360555 0.73 72 61 16 129 0.15 0.387298 0.84 72 62 17 129 0.15 0.387298 0.84 72 61 18 129 0.19 0.43589 1.10 73 61 19 128 0.21 0.458258 1.20 74 62 20 127 0.19 0.43589 1.10 75 62 21 128 0.16 0.4 0.90 75 62 22 128 0.14 0.374166 0.79 74 63 23 129 0.12 0.34641 0.67 74 63. METER T. 24 129 0.10 0.316228 0.56 73 63 AVERAGE
128.70833 0.3982 0.8975 69.9167 59.5000 64.7083 

# 40

### EMISSION TEST SUMMARY
PLANT: Dal·ltalia, Muskogee, OK DATE: 2-Nov-06 PLACE: Phase II Scrubber Exhaust (EPN 29) RUN#: 

### 3 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) 

### : 126 NOZZLE DIAMETER (INCH.): 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 0.994 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 GAS METER VOL.(Cu.Ft.} : 35.19 PERCENT C02 3 BAROMETRIC PRESSURE 30.15 PERCENT 02 17 PERCENT CO 0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 72.5 STACK LENGTH(inchs): STACK AREA (Sq.Ft.) : 28.6684 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.): 0 ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

### FLOWS SAMPLED VOLUME (STD. CU.FT.): 35.2108 VOLUME OF WATER VAPOR (STD. CU.FT.}: 5.9308

FRACTIONAL MOISTURE CONTENT(%): 0.1442 DRY BASE: • 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 MOLECULAR WT. OF STACK GAS (WET BASE): 27.5512 STACK PRESSURE (inch Hg): 30.1529 STACK GAS VELOCITY (ft/sec.): 23.6643 ACTUAL STACK GAS FLOW RATE (ACFM): 40705.1208 STANDARD STACK GAS FLOW RATE (SCFH}: 1888746.64 ISOKINETIC RATIO(%): 100.2762 POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. deg F INLET OUTLET 1 129 0.12 0.34641 0.67 62 62 2 129 0.14 0.374166 0.79 67 62 3 129 0.16 0.4 0.90 70 62 4 129 0.18 0.424264 1.00 72 62 5 129 0.21 0.458258 1.20 73 62 6 129 0.22 0.469042 1.20 

### 74. 63 

### 7 129 0.23 0.479583 1.30 75 63 

### 8 129 0.22 0.469042 1.30 75 63 9 129 0.20 0.447214 1.10 76 64 10 129 0.17 0.412311 0.97 76 64 

### 11 129 0.14 0.374166 0.80 76 65 12 128 0.11 0.331662 0.63 75 65 13 128 0.10 0.316228 0.57 68 65 14 129 0.11 0.331662 0.62 

### 73 65 15 129 0.12 0.34641 0.68 75 66 16 129 0.13 0.360555 0.71 76 66 17 129 0.15 0.387298 0.86 76 66 18 129 C.17 0.4123i 1 

### 0.97 77 66 19 129 0.20 0.447214 1.15 

### 78 67 20 129 0.18 0.424264 1.00 

### 79 67 21 130 0.15 0.387298 0.86 

### 78 67 22 129 0.12 0.34641 0.69 78 67 23 129 0.11 0.331662 0.63 

### 77 67 METER T. 24 127 0.10 0.316228 0.57 76 67 AVERAGE 128.875 0.3914 0.8821 74.2500 64.7083 69.4792 

# 41PLANT: DATE: PLACE: RUNt#: EMISSION TEST SUMMARY Dal·ltalla, Musk<'l·lC:e. OK 2·NOV·06 Phase II Scrubber Exhaust (EPN 29) 4 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : 0.3123 PARTICULATE WEIGHT (Front half mg): 0.992 PARTICULATE WEIGHT (Back half mg): 0.84 STATIC PRESSURE (in. H20): 129.4 35.38

10.2 0.04 3 GAS METER VOL.(Cu.Ft.) : 36.351 PERCENT C02 BAROMETRIC PRESSURE 29.15 PERCENT 02 PERCENT CO FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA (SQ.Ft.) : NOZZLE AREA (feet): FOR RECTANGULAR STACK 72.5 STACK LENGTH(inchs): 28.6684 STACK WIDTH(inchs) : 0.000532 STACK AREA (SQ.Ft.): ENTER THE STACK AREA SHOWN ABOVE: FLOWS SAMPLED VOLUME (STD. CU.fi.): VOLUME OF WATER VAPOR (STD. CU.fi.):

FRACTIONAL MOISTURE CONTENT (%): DRY BASE: MOLECULAR 

### WT. OF STACK GAS (DRY BASE): MOLECULAR 

### WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ftlsec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH): PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): BACK HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): ISOKINETIC RATIO(%): 28.6684

34.7735 6.0909 0.1491 80.0000 29.1600 27.4966 29.1529 24.6652 42426.7332 1891253.17

0.0157 2.24E·06

4.2429

0.0045 6.47E·07

1.2232 99.1532

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T.

1 2 3 4 

### 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 deg F INLET 129 129 128 128 128 128 128 129 130 130 130 130 129 129 129 129 129 130 130 130 130 130 130 130 129.25 0.13 0.360555 0.14 0.374166 0.15 0.387298 0.18 0.424264 0.22 0.469042 0.23 0.479583 0.22 0.469042 0.20 0.447214 0.18 0.424264 0.16 0.424264 0.14 0.374166 0.13 0.360555 0.10 0.316228 0.11 0.331662 0.14 0.374166 0.15 0.387298 0.19 0.43589 0.22 0.469042 0.21 0.458258 0.19 0.43589 0.15 0.387298 0.12 0.34641 0.11 0.331662 0.12 0.34641 0.4006 0.75 0.80 0.86 1.00 1.30 1.30 1.30 1.20 1.00 1.00 0.81 0.76 0.58 0.64 0.81 0.87 1.10 1.30 1.20 1.10 0.88 0.70 0.65 0.70 0.9421 66 70 72 76 79 79 80 81 81 81 80 80 73 78 81 82 83 85 85 

### 85 85 84 84 84 79.7500 METERT. OUTLET 66 

### 66 66 66 67 67 67 

### 68 69 69 69 69 69 70 70 70 71 71 71 72 72 72 17 0



### 0

72 METERT. 73 AVERAGE 69.2500 74.5000 

# 42

### EMISSION TEST SUMMARY
PLANT: Dal·ltalia. MuskORee, OK DATE: 2·NOv·06 PLACE: Prtase II Scrubber Exhaust (EPN 29) RUN#: 5 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 122.2 NOZZLE DIAMETER (INCH.): 0.3123 PARTICULATE WEIGHT (Front half mg): 23.36 METER COEFFICIENT (Y) : 0.992 PARTICULATE WEIGHT (Back half mg}: 11.5 PI TOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 GAS METER VOL.(Cu.Ft.) : 35.05 PERCENT C02 3 BAROMETRIC PRESSURE 30.15 PERCENT 02 17 PERCENT CO 0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 72.5 STACK LENGTH(Inches): STACK AREA (Sq.Ft.) : 28.6684 STACK WI DTH(inches) : NOZZLE AREA (feet): 0.000532 STACK AREA (Sq.Ft.): 0 ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

### FLOWS SAMPLED VOLUME (STD. CU. FT.): 34.3393 VOLUME OF WATER VAPOR (STD. CU.FT.): 5.7520

FRACTIONAL MOISTURE CONTENT (%): 0.1435 DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 MOLECULAR WT. OF STACK GAS (WET BASE): 27.5589 STACK PRESSURE (inch Hg): 30.1529 STACK GAS VELOCITY (ftlsec.): 23.3632 ACTUAL STACK GAS FLOW RATE (ACFM): 40187.0515 STANDARD STACK GAS FLOW RATE (SCFH): 1866991.87 PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR.ISCF): 0.0105 PARTICULATE CONCENTRATION (LBS/SCF): 1.50E·06 PARTICULATE EMISSION (LBS/HR): 2.8005 BACK HALF PARTICULATE CONCENTRATION (GR.ISCF): 0.0052 PARTICULATE CONCENTRATION (LBS/SCF): 7.38E·07 PARTICULATE EMISSION (LBSIHR): 1.3787 ISOKINETIC RATIO(%): 99.1873

POINTS STACK T. DELTA P SQUAR D.P DELTA H METERT. METER T. deg F INLET OUTLET 1 129 0.10 0.316228 0.59 71 71 2 129 0.11 0.331662 0.65 80 71 3 129 0.13 0.360555 0.76 82 71 4 129 0.16 0.4 0.94 84 72 5 129 0.18 0.424264 1.10 86 73 6 129 0.20 0.447214 1.20 87 74 7 129 0.22 0.469042 1.30 88 75 8 129 0.20 0.447214 1.20 89 75 9 129 0.18 0.424264 1.10 87 76 10 129 0.15 0.387298 0.89 88 76 11 129 0.12 0.34641 0.71 88 77 12 127 0.10 0.316228 0.60 88 77 13 128 0.10 0.316228 0.58 77 76 14 128 0.12 0.34641 0.71 83 76 15 129 0.14 0.374166 0.82 85 76 16 129 0.15 0.387298 0.89 

### 86 76 17 129 0.19 0.43589 1.10 86 76 18 129 0.20 0.447214 1.20 87 75 19 128 0.21 0.458258 1.20 86 75 20 129 0.20 0.447214 1.20 86 75 21 129 0.16 0.4 1.95 

### 86 75 22 128 0.12 0.34641 0.71 86 75 23 128 0.11 0.331662 0.65 85 75 METER T. 24 127 0.10 0.316228 0.59 85 74 AVERAGE 128.625 0.3866 0.9433 84.8333 74.6667 79.7500 

# 43

### EMISSION TEST SUMMARY
PLANT: Dal·llalia, MuskoRee. DK DATE: 2-Nov-06 PLACE: Phase II Scrubber Exhaust (EPN 29) RUN#: 6 TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : NOZZLE DIAMETER (INCH.): METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp} : 0.3123 PARTICULATE WEIGHT (Front half mg): 0.992 PARTICULATE WEIGHT (Back half mg}: 0.84 STATIC PRESSURE (in. H20): 121.7 29.93 14.29 0.04 3 17 0 GAS METER VOL.(Cu.Ft.) : 35.98 PERCENT C02 BAROMETRIC PRESSURE 30. 15 PERCENT 02 PERCENT CO FOR CIRCULAR STACK STACK DIAMETER (inch): STACK AREA (Sq.Ft.) : NOZZLE AREA (feet): FOR RECTANGULAR STACK 72.5 STACK LENGTH(inchs): 28.6684 STACK WIDTH(inchs) : 0.000532 STACK AREA {Sq. Ft.): ENTER THE STACK AREA SHOWN ABOVE: 

### FLOWS SAMPLED VOLUME (STD. CU.FT.):. VOLUME OF WATER VAPOR (STD. CU.FT.):

FRACTIONAL MOISTURE CONTENT (%): DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY {fVsec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH): PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): BACK HALF PARTICULATE CONCENTRATION (GR.ISCF): PARTICULATE CONCENTRATION (LBS/SCF): PARTICULATE EMISSION (LBS/HR): ISOKINETIC RATIO(%): 2B.6684

35.5065 5.7284 0.1389 80.0000 29.1600 27.6096 30.1529 23.9327 41166.6439 1919807.14

0.0130 1.86E·06

3.5683

0.0062 8.87E-07

1.7037 99.7372

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T.

1 2 3 4 

### 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 deg F INLET 129 

### 128 128 128 129 129 130 130 130 130 130 130 

### 129 130 130 130 130 130 130 130 130 130 129 

### 129
129.5 0.13 0.360555 0.14 0.374166 0.15 0.387298 0.18 0.424264 0.19 0.43589 0.21 0.458258 0.22 0.469042 0.22 0.469042 0.21 0.458258 0.20 0.447214 0.16 0.4 0.14 0.374166 0.10 0.316228 0.12 0.34641 0.13 0.360555 0.15 0.387298 0.16 0.4 0.18 0.424264 0.19 0.43589 0.17 0.412311 0.15 0.387298 0.13 0.360555 0.10 0.316228 0.09 0.3 0.3960 0.75 0.80 0.87 1.00 1.10 1.20 1.30 1.30 1.20 1.20 0.94 0.82 0.59 0.70 0.76 0.87 0.93 1.05 1.10 0.99 0.87 0.76 0.58 0.52 0.9250 71 78 81 82 82 83 

### 84 84 84 84 84 83 78 79 80 81 80 80 

### 81 80 79 78 77 77 80.4167 METER T. OUTLET 71 

### 71 71 72 72 72 73 73 73 73 73 73 72 72 71 

### 71 71 71 71 70 69 69 0

68 METER T. 68 AVERAGE
71.2500 75.8333 

# 44--.-.-**--~---;--- -~** **~:** .... -



## '·

•I

# App~ndlxB

l·ti .•

.. J.:.

## Sheet1
Summary of CO Analyzer Calibrations and Bias Plant: Dal-ltalia, Muskogee, OK Source: Phase II Scrubber Date: 11/2/2006 Analyzer Calibratrion Data Cylinder Analyzer Absolute % 

## Span Zero Gas Mid Range High Range Value Response Difference 0 1.33 1.33 99.1 99.18 0.08 200 196.65 -3.35
System Calibration Bias 

## and Drift Data 0.665 0.04 -1.675

Analyzer Initial Values Final Values Drift

Run #1

Run #2

Run #3 Calibration System System System System Respon·se Calibration Calibration Calibration Calibration Response Bias Response Bias Zero Gas Upscale 1.33 99.18 Average CO Concentration: Corrected CO Concentration: (Equation 6C-1) Zero Gas 1.33 Upscale 99.18 Average CO Concentration: Corrected CO Concentration: (Equation 6C-1)
Zero Gas 1.33 Upscale 99.18 Average CO Concentration: 1.1 94.7

2.2 96.58

0.33 94.38

Corrected CO Concentration: (Equation 6C-1) -0.115 -2.24

86.6 89.56852

0.435

-1.3 126.99 132.2438

-0.5 -2.4 118.98 126.6041

Page 1 2.2 96.58

0.33 94.38

-0.35 91.88 0.435 -1.3

-0.5 -2.4

-0.84 -3.65 0.55 0.94

-0.935 -1.1

-0.34 -1.25 Average Calibration Values

1.65 95.64

1.265 95.48

-0.01 93.13

### Sheet1
Summary of NOx Analyzer Calibrations and Bias Plant: Dal-ltalia, Muskogee. OK Source: Phase 

## II Scrubber Date: 10/31/2006

Run #1

Run#2

Run 

## #3 Analyzer Calibratrion Data Cylinder Analyzer Absolute % Span Value Response Difference Zero Gas Mid Range High Range 0 0 0 0 25 25.45 0.45 0. 75 51 50.78 -0.22 -0.36667
System Calibration Bias and Drift Data Analyzer Initial Values Final Values Calibration System System System System Response Calibration Calibration Calibration Calibration Response Bias Response Bias Zero Gas 

## 0 0.03 0.05 0.13 0.216667 Upscale 25.45 24.1 -2.25 25.08 -0.61667 Average NOx Concentration: 21.67 Corrected NOx Concentration: 22.02162 (Equation 6C-1) Zero Gas 0 0.13 0.216667 0.15 0.25 Upscale 25.45 25.08 -0.61667 24.45 -1.66667 Average NOx Concentration: 22.55 Corrected NOx Concentration: 22.75127 (Equation 6C-1) Zero Gas 0 0.15 0.25 0.25 0.416667 Upscale 25.45 24.45 -1.66667 24.98 -0.78333 Average NOx Concentration: 22.77 Corrected NOx Concentration: 23.01652 (Equation 6C-1)

Page 1 Drift Average Calibration Values

0.166667 0.08 1.633333 24.59

0.033333 0.14 -1.05 24.765

0.166667 0.2 0.883333 24.715



# 82

## Sheet1


## Summary of Sulfur Dioxide Analyzer Calibrations and Bias Plant: Source: Date:

Run #1

Run #2

Run #3 Dal-ltalia, Muskogee, OK Phase II Scrubber

11/2/2006 

## Analyzer Calibratrion Data Cylinder Analyzer Absolute % 

## Span Zero Gas Mid Range High Range Value Response Difference 0 -0.03 -0.03 49.8 49.3 -0.5

100 99.8 -0.2


## System Calibration Bias and Drift Data -0.03 -0.5 -0.2

Analyzer Initial Values Final Values Drift Calibration System System System System Response Calibration Calibration Calibration Calibration Response Bias Response Bias
Zero Gas Upscale -0.03 49.3 -0.08 47 Average S02 Concentration: Corrected S02 Concentration:

. (Equation 6C-1)
Zero Gas -0.03 -0.08 Upscale 49.3 47.08 Average S02 Concentration: Corrected S02 Concentration: (Equation 6C-1)
Zero Gas -0.03 -0.4 Upscale 49.3 46.48 Average 502 Concentration: Corrected S02 Concentration: (Equation 6C-1) -0.05 -2.3
0.03 0.116256

-0.05 -2.22
-0.44 -0.21182

-0.37 -2.82
-0.11 0.123413

Page 1 -0.08 47.08

-0.4 46.48

-0.05 45.88 -0.05 -2.22

-0.37 -2.82

-0.02 -3.42 

## 0 0.08

-0.32

-0.6

0.35 -0.6 Average Calibration Values

-0.08 47.04

-0.24 46.78

-0.225 46.18



# 83

## 11/2106 Nox Converter Check

Date/Time NOx mm/dd/yy hh:mm:ss ppm 11/02/06 07:34:04 

# 0.0163 Zero NOx 11/02106 07:35:04 0.040228 11/02/06 07:36:04 44.50978 11/02/06 07:37:04 

# 49.981 51 ppm NOx 11/02/06 07:38:04 12.04688 11/02/06 07:39:04 26.13428 Start Converter Check 11/02/06 07:40:04 27.84863 11/02/06 07:41:04 27.82276 11/02/06 07:42:04 27.87696 11/02/06 07:43:04 27.88623 11/02/06 07:44:04 27.89161 11/02106 07:45:04 27.89698 11/02/06 07:46:04 27.89844 11/02/06 07:47:04 27.8794 11/02/06 07:48:04 27.89747 11/02/06 07:49:04 27.87061 11/02/06 07:50:04 27.86622 11/02/06 07:51:04 27.85255 11/02/06 07:52:04 27.83887 11/02/06 07:53:04 27.83595 11/02/06 07:54:04 27.83106 11/02/06 07:55:04 27.82081 11/02/06 07:56:04 27.79054 11/02/06 07:57:04 27.75929 11/02/06 07:58:04 27.75636 11/02/06 07:59:04 27.72511 11/02/06 08:00:04 27.74366 11/02/06 08:01:04 27.72023 11/02/06 08:02:04 27.70314 11/02/06 08:03:04 27.69288 11/02/06 08:04:04 27.64454 11/02/06 08:05:04 27.64699 11/02/06 08:06:04 27.61622 11/02/06 08:07:04 27.6006 11/02/06 08:08:04 27.60352 Stop Converter Check 11/02/06 08:09:04 27.58936

Page 1 

# 8411/2/06 Calibrations

Date/Time 

## voc co NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm ppm 11/02/06 08:19:52 1.2 1.5 

### 0.0 7.1 11/02/06 08:20:02 1.6 1.7 

### 0.0 7.1 Zero NOx 11/02/06 08:20:12 1.9 1.7 

### 0.0 7.1 11/02/06 08:20:22 2.1 2.0 

### 0.0 7.1 11/02/06 08:20:32 2.5 2.1 0.1 7.2 11/02/06 08:20:42 2.6 1.7 20.7 7.2 11/02/06 08:20:52 2.8 1.5 24.4 7.2 11/02/06 08:21 :02 2.8 1.8 24.5 7.1 11/02/06 08:21:12 2.9 1.8 25.0 7.1 11/02106 08:21:22 3.0 1.8 25.5 7.3 11/02106 08:21:32 3.0 2.1 

### 25.4 7.2 11/02/06 08:21:42 3.1 2.2 

### 25.5 7.2 Zero NOx 11/02/06 08:21 :52 3.2 2.1 

### 25.5 7.2 11/02/06 08:22:02 3.2 2.3 

### 25.4 7.2 11/02/06 08:22:12 3.2 2.2 25.5 4.3 11/02106 08:22:22 3.2 2.1 25.4 0.0 11/02/06 08:22:32 3.3 2.4 13.1 -0.1 11/02/06 08:22:42 3.3 2.3 0.1 -0.1 11/02106 08:22:52 3.4 2.3 0.1 -0.2 11/02/06 08:23:02 3.4 2.1 0.0 -0.1 11/02/06 08:23:12 3.4 2.2 0.1 -0.1 11/02106 08:23:22 3.3 2.0 0.1 -0.1 11/02106 08:23:32 3.4 2.1 0.1 -0.1 11/02106 08:23:42 3.4 1.8 43.8 -0.1 11/02106 08:23:52 3.4 1.8 50.3 0.0 11/02/06 08:24:02 3.4 1.9 50.6 0.0 H/02106 08:24:12 3.4 2.0 

### 50.7 -0.1 11/02/06 08:24:22 3.4 2.2 

### 50.7 -0.2 51 ppm NOx 11/02/06 08:24:32 3.4 2.0 

### 50.7 -0.1 11/02106 08:24:42 3.4 1.9 

### 50.8 -0.1 11/02/06 08:24:52 3.4 2.1 32.0 -0.2 11/02/06 08:25:02 3.3 2.3 0.2 -0.1 11/02/06 08:25:12 3.3 2.1 0.1 0.0 11/02/06 08:25:22 3.3 1.8 0.1 0.0 11/02106 08:25:32 3.3 1.8 0.0 0.0 11/02106 08:25:42 3.3 1.8 0.1 0.0 11/02106 08:25:52 3.4 1.8 0.1 0.0 11/02106 08:26:02 3.4 16.6 0.0 0.0 11/02/06 08:26:12 3.4 85.0 0.0 0.0 11/02/06 08:26:22 3.4 97.3 0.0 -0.1 11/02106 08:26:32 3.3 98.5 0.0 -0.1 11/02/06 08:26:42 3.3 98.8 0.0 0.0 11/02/06 08:26:52 3.3 98.9 0.0 0.0 11/02/06 08:27:02 3.3 99.1 0.0 0.0 11/02106 08:27:12 3.3 

### 99.0 0.0 

### 0.0 11/02106 08:27:22 3.3 

### 99.3 0.0 

### -0.1 99.1 ppm CO 11/02/06 08:27:32 3.4 

### 99.2 0.0 

### 0.0 Zero S02 11/02/06 08:27:42 3.4 

### 99.2 0.0 

### 0.0 11/02106 08:27:52 3.4 68.9 0.0 -0.1 11/02/06 08:28:02 3.4 9.0 0.0 -0.1 11/02106 08:28:12 3.4 2.7 0.0 -0.1 11/02106 08:28:22 3.4 2.3 0.0 -0.1 11/02106 08:28:32 3.4 2.1 0.1 0.0 11/02106 08:28:42 3.4 2.0 0.0 -0.1 11/02/06 08:28:52 3.4 1.9 0.1 -0.1 11/02/06 08:29:02 3.4 5.0 0.1 0.0 11/02/06 08:29:12 3.4 130.5 0.0 0.0 11/02/06 08:29:22 3.4 190.4 0.0 0.0 11/02106 08:29:32 3.4 194.5 0.0 -0.1 11/02106 08:29:42 3.4 195.1 0.0 -0.1 11/02/06 08:29:52 3.4 195.3 0.0 -0.2 11/02/06 08:30:02 3.4 196.0 0.0 -0.2 11/02106 08:30:12 3.4 196.5 0.0 0.0 11/02/06 08:30:22 3.4 

### 196.6 0.0 0.0 11/02/06 08:30:32 3.3 

### 196.9 0.0 0.0 200 ppm NOx 11/02/06 08:30:42 3.3 

### 196.7 0.0 0.0 11/02/06 08:30:52 3.3 

### 196.4 0.0 0.0

Page 1 

# 851112/06 Calibrations

11/02/06 08:31 :02 3.3 165.8 0.0 -0.1 11/02/06 08:31 :12 3.3 27.8 0.0 -0.2 11102106 08:31 :22 3.3 4.2 0.0 -0.3 11/02/06 08:31 :32 3.4 2.4 0.1 -0.2 11/02/06 08:31:42 3.4 2.1 0.0 -0.2 11102/06 08:31:52 3.4 1.9 0.0 -02 11/02/06 08:32 :02 3.4 1.6 0.0 -0.2 11102/06 08:32:12 3.4 1.6 0.1 -0.1 11/02/06 08:32:22 3.4 1.6 0.1 0.8 11/02/06 08:32:32 3.4 1.1 0.1 17.5 11/02/06 08:32:42 3.4 1.1 0.1 37.2 11/02/06 08:32:52 3.4 0.9 0.1 44.9 11/02/06 08:33:02 3.4 0.9 0.1 47.2 11/02/06 08:33:12 3.4 0.9 0.1 47.8 11/02/06 08:33:22 3.4 0.9 0.1 47.9 11/02/06 08:33:32 3.4 0.9 0.1 47.9 11/02/06 08:33:42 3.4 1.0 0.1 47.7 11/02/06 08:33:52 3.4 1.1 0.1 47.7 11/02/06 08:34:02 3.4 0.9 0.1 47.7 11/02/06 08:34:12 3.4 1.0 0.1 49.1 11/02/06 08:34:22 3.4 1.2 0.1 49.2 11/02/06 08:34:32 3.4 

### 1.4 .0.1 

### 49.3 11/02/06 08:34:42 3.4 

### 1.3 0.0 

### 49.3 49.8 ppm S02 11102/06 08:34:52 3.4 

### 1.4 0.0 

### 49.3 Zero CO 11102/06 08:35:02 3.3 

### 1.2 0.0 

### 49.3 11/02/06 08:35:12 3.3 1.2 0.0 49.3 11/02/06 08:35:22 3.4 1.6 0.0 44.9 11/02/06 08:35:32 3.3 1.7 0.1 22.4 11/02106 08:35:42 3.4 1.8 0.0 6.6 11/02/06**08:35:~2** 3.4 1.6 0.1 1.3 11/02/06 08:36:02 3.4 1.7 0.0 0.0 11102/06 08:36:12 3.4 1.6 0.1 -0.2 11/02106 08:36:22 3.4 1.5 0.1 -0.2 11/02/06 08:36:32 3.4 1.7 0.1 -0.2 11/02/06 08:36:42 3.3 1.7 0.0 -0.3 11/02/06 08:36:52 3.3 1.6 0.0 -0.2 11/02/06 08:37:02 3.3 1.1 0.2 21.1 11/02/06 08:37:12 3.4 0.9 0.4 70.9 11/02/06 08:37:22 3.3 0.9 0.4 96.0 11/02/06 08:37:32 3.3 0.9 0.4 99.8 11/02/06 08:37:42 3.4 0.9 0.4 

### 99.8 11/02/06 08:37:52 3.4 0.9 0.4 

### 99.8 100 ppm S02 11/02/06 08:38:02 3.3 0.9 0.4 

### 99.8 11/02/06 08:38:12 3.4 0.9 0.4 

### 99.8 11/02/06 08:38:22 3.3 1.1 0.3 97.6 11/02/06 08:38:32 3.2 1.4 0.1 56.3 11/02/06 08:38:42 3.2 1.1 0.1 17.9 11/02/06 08:38:52 32 1.2 0.1 4.4 11/02/06 08:39:02 3.2 1.4 0.0 0.8 11/02/06 08:39:12 2.2 1.2 0.0 0.0 11/02106 08:39:22 0.6 1.0 0.7 0.0 11/02/06 08:39:32 0.5 1.2 8.4 0.0 11/02/06 08:39:42 0.4 1.0 14.4 0.0 11/02/06 08:39:52 0.3 1.0 18.0 -0.1 11/02/06 08:40:02 0.3 1.0 20.5 -0.1 11/02/06 08:40:12 0.2 0.9 22.0 -0.2 11/02/06 08:40:22 0.3 0.9 23.0 -0.3 11/02/06 08:40:32 0.3 0.9 23.4 -0.4 11/02/06 08:40:42 0.3 0.9 23.7 -0.3 11/02/06 08:40:52 0.2 1.2 23.9 -0.2 11/02/06 08:41:02 0.1 1.0 23.9 -0.2 11/02/06 08:41:12 0.1 0.9 24.0 -0.1 11/02/0S 08:41:22 

### 0.1 1.0 24.1 -0.1 11/02/06 08:41:32 

### 0.1 1.1 24.1 -0.2 25 ppm NOx Bias 11/02/06 08:41:42 

### 0.1 1.1 24.1 -02 Zero VOC. CO Bias 11/02/06 08:41 :52 

### 0.1 1.2 24.1 -0.2 11/02/06 08:42:02 0.1 1.2 24.2 -0.2 11/02/06 08:42:12 0.1 1.2 24.1 -0.1 11/02/06 08:42:22 0.7 1.2 24.0 -0.1 11/02/06 08:42:32 0.9 1.3 22.9 -0.1 11/02/06 08:42:42 1.3 5.4 17.5 -0.1

Page 2 

# 861112/06 Calibrations

11/02/06 08:42:52 2.2 15.0 9.2 -0.1 11/02106 08:43:02 1.5 14.6 4.5 -0.1 11/02/06 08:43:12 0.4 15.5 2.4 0.0 11/02/06 08:43:22 0.2 41.1 1.3 0.1 11/02106 08:43:32 0.2 61.9 0.8 0.0 11/02106 08:43:42 0.3 75.1 0.6 0.0 11/02106 08:43:52 0.1 83.4 0.6 0.0 11/02/06 08:44:02 0.1 87.3 0.7 0.0 '\1/02/06 08:44:12 0.1 89.3 0.6 

## o.o 11/02/06 08:44:22 0.1 90.9 0.3 0.0 11/02106 08:44:32 0.0 92.1 0.3 -0.2 11/02106 08:44:42 0.0 92.9 0.2 -0.2 11/02106 08:44:52 0.0 93.4 0.1 -02 11/02106 08:45:02 0.0 93.5 0.0 -0.2 11/02106 08:45:12 0.0 93.9 0.0 -0.1 11/02/06 08:45:22 0.0 94.2 0.0 

### -02 11/02106 08:45:32 0.0 94.4 0.0 -0.1 11/02106 08:45:42 0.1 94.5 0.0 -0.1 11/02/06 08:45:52 0.1 

### 94.9 0.0 

### -0.1 11/02/06 08:46:02 0.1 

### 94.6 0.0 

### 0.0 99.1 ppm CO Bias 11/02/06 08:46:12 0.1 

### 94.7 0.0 

### -0.1 Zero 502 11/02106 08:46:22 0.1 

### 94.6 0.0 

### -0.1 11/02/06 08:46:32 0.0 94.3 0.0 -0.1 11/02106 08:46:42 0.1 94.0 0.0 -0.1 '\ 1/02/06 08:46:52 0.0 84.2 0.0 0.0 11/02106 08:47:02 0.0 52.8 0.0 1.9 11/02106 08:47:12 0.0 27.5 0.0 7.6 11/02/06 08:47:22 0.1 15.3 0.0 14.9 11/02/06 08:47:32 0.1 9.7 0.0 21.4 11102/06 08:47:42 0.1 7.3 0.0 26.5 11102/06 08:47:52 0.0 5.6 0.0 

### 302 11/02106 08:48:02 0.1 4.3 0.0 33.0 11/02/06 08:48:12 0.1 3.6 0.0 35.2 11/02106 08:48:22 0.0 3.1 0.0 37.0 11102106 08:48:32 0.0 2.5 0.0 38.4 11/02106 08:48:42 0.0 2.3 0.0 39.5 11/02/06 08:48:52 0.0**~.0** 0.0 40.6 11/02106 08:49:02 0.1 1.4 0.0 41.6 11/02106 08:49:12 0.0 1.3 0.0 42.2 11/02106 08:49:22 0.1 1.3 0.0 42.8 11/02/06 08:49:32 0.1 1.2 0.0 43.4 11/02/06 08:49:42 0.0 1.2 0.0 44.0 11/02/06 08:49:52 0.0 1.1 0.0 44.6 11/02106 08:50:02 0.0 1.0 0.0 45.2 11/02/06 08:50:12 0.0 1.0 0.0 45.7 11/02106 08:50:22 0.0 1.0 0.0 46.1 11/02106 08:50:32 0.0 1.1 0.0 46.6 11/02/06 08:50:42 0.1 1.1 0.0 46.8 11/02/06 08:50:52 0.0 1.1 0.0 47.1 11/02/06 08:51:02 0.0 1.2 

### 0.0 47.0 11/02/06 08:51:12 0.1 1.3 

### 0.0 47.0 49.2 ppm 502 11/02/06 08:51:22 0.0 1.3 

### 0.0 47.0 ZeroNOx 11/02106 08:51:32 0.1 1.2 

### 0.0 47.0 11/02106 08:51:42 30.6 1.2 0.1 47.1 11/02106 08:51:52 39.9 1.3 0.1 46.5 11/02/06 08:52:02 39.9 1.4 0.0 44.4 11/02106 08:52:12 39.9 1.5 0.1 38.7 11/02106 08:52:22 40.2 1.3 0.0 27.9 11/02106 08:52:32 40.7 1.1 0.0 19.3 11/02/06 08:52:42 

### 40.8 1.0 0.1 13.6 11/02/06 08:52:52 

### 40.8 0.9 0.1 10.1 40.8 ppm CH4 11/02106 08:53:02 

### 40.8 0.9 0.1 7.8 11/02106 08:53:12 

### 40.8 1.0 0.1 6.4 11/02106 08:53:22 40.5 0.9 0.0 5.5 11/02/06 08:53:32 37.9 0.9 0.0 4.7 11/02/06 08:53:42 29.9 0.9 0.0 4.0 11/02/06 08:53:52 9.3 1.0 0.0 3.8 11/02/06 08:54:02 2.9 1.3 0.0 3.9 11/02/06 08:54:12 2.6 1.3 0.0 5.3 11/02/06 08:54:22 16.8 1.5 0.0 9.2 11/02/06 08:54:32 19.1 1.3 0.0 14.9 

# 87 Page31112/06 Calibrations

11/02106 08:54:42 

### 19.1 1.1 0.0 16.8 11/02/06 08:54:52 

### 19.1 0.9 0.0 13.6 19.9 ppm CH4 11/02/06 08:55:02 

### 19.1 0.6 0.0 9.2 11/02106 08:55:12 

### 19.1 0.5 0.0 5.9 11/02/06 08:55:22 19.1 0.4 0.0 3.9 11/02/06 08:55:32 

## 1s.s 0.6 0.0 2.8 11/02106 08:55:42 17.4 0.6 0.0 2.0 11/02106 08:55:52 12.1 0.5 0.0 1.7 11/02/06 08:56:02 3.2 0,7 0.0 

### 1.3 11/02/06 08:56:12 2.6

. 0.8 0.0 1.2 11/02/06 08:56:22 10.2 1.1 0.0 1.6 11102/06 08:56:32 61.2 

### 1.1 0.0 3.0 11/02/06 08:56:42 

### 62.7 1.2 0.0 4.9 11/02/06 08:56:52 

### 62.7 1.0 0.0 5.4 61.7ppm CH4 11/02/06 08:57:02 

### 62.7 0.9 0.0 4.3 11/02/06 08:57:12 

### 62.6 0.8 0.0 3.0 11/02/06 08:57:22 62.4 0.8 0.0 2.0

Page 4 

# 881112/06 Run #1

Oatemme 

## voc co NOx 502 mm/ddlyy hh:mm:ss ppm ppm ppm ppm 11/02/06 09:14:52 38.3 76.8 22.0 2.1 Stan Run#1 11/02106 09:15:02 39.0 80.8 22.0 2.0 11/02106 09:15:12 39.8 84.2 22.0 1.8 11/02106 09:15:22 39.8 86.9 22.1 1.7 11/02106 09:15:32 40.1 88.1 22.2 1.6 11/02/06 09:15:42 40.3 89.6 22.1 1.7 11/02/06 09:15:52 40.1 91.3 22.0 1.5 11/02/06 09:16:02 39.6 93.0 22.0 1.3 11102106 09:16:12 38.8 94.5 22.0 1.2 11/02/06 09:16:22 38.1 96.0 21.8 1.3 11/02/06 09:16:32 37.2 97.6 21.7 1.3 11/02/06 09:16:42 35.8 98.7 21.7 1.2 11/02106 09:16:52 34.9 99.3 21.7 1.1 11/02106 09:17:02 34.0 99.7 21.7 0.9 11/02106 09:17:12 32.6 99.8 21.7 0.9 11/02/06 09:17:22 31.8 99.8 21.6 0.8 11/02106 09:17:32 31.3 99.4 21.8 0.8 11/02/06 09:17:42 31.0 98.6 21.7 0.8 11/02106 09:17:52 30.4 98.4 21.6 0.7 11/02106 09:18:02 30.3 98.0 21.5 0.7 11/02106 09:18:12 31.0 97.9 21.5 0.7 11/02/06 09:18:22 31.9 97.8 21.4 0.6 11/02106 09:18:32 32.5 97.7 21.2 0.5 11/02106 09:18:42 33.1 97.6 21.2 0.5 11/02/06 09:18:52 33.7 97.4 21.2 0.6 11/02106 09:19:02 34.3 97.6 21.2 0.6 11/02106 09:19:12 34.8 97.6 21.2 • 0.5 11/02106 09:19:22 34.7 98.0 21.2 0.4 t 1/02106 09:19:32 34.4 98.1 21.2 0.5 11/02/06 09:19:42 34.4 98.2 21.1 0.6 11/02/06 09:19:52 34.2 98.4 21.2 0.5 11/02/06 09:20:02 34.2 98.4 21.1 0.4 11/02/06 09:20:12 33.9 98.6 21.2 0.4 11/02/06 09:20:22 33.3 98.7 21.3 0.4 11/02/06 09:20:32 32.9 98.6 21.3 0.4 11/02/06 09:20:42 32.3 98.6 21.3 0.2 11/02/06 09:20:52 31.8 98.7 21.4 0.2 1t/02106 09:21:02 31.8 98.4 21.4 0.1 11/02/06 09:21:12 31.7 98.0 21.6 0.1 11/02/06 09:21:22 31.6 97.5 21.6 0.1 11/02/06 09:21:32 31.8 97.2 21.7 0.3 11/02106 09:21:42 32.1 96.7 21.8 0.2 11/02106 09:21:52 32.4 96.3 21.8 0.2 11/02106 09:22:02 33.0 96.2 21.9 0.3 11/02/06 09:22:12 33.5 96.0 21.9 0.3 11/02/06 09:22:22 33.6 95.4 22.0 0.3 11/02/06 09:22:32 34.0 95.0 22.0 0.3 11/02106 09:22:42 34.1 94.8 21.9 0.2 11/02106 09:22:52 34.2 94.5 22.0 0.2 11/02106 09:23:02 34.0 94.1 21.9 0.3 11/02106 09:23:12 33.8 94.1 21.9 0.2 11/02/06 09:23:22 33.3 93.9 21.9 0.2 11/02106 09:23:32 32.6 93.7 21.9 0.2 11/02/06 09:23:42 31.9 93.4 21.8 0.1 11/02/06 09:23:52 32.1 93.3 21.7 0.1 11/02/06 09:24:02 31.6 93.4 21.5 0.2 11/02106 09:24:12 30.9 93.8 21.3 0.2 11/02/06 09:24:22 30.7 94.0 21.2 0.1 11/02/06 09:24:32 30.4 94.4 21.1 0.1 11/02/06 09:24:42 30.4 94.8 21.1 0.1 11/02/06 09:24:52 30.8 94.6 21.1 0.1 11/02/06 09:25:02 31.3 94.6 20.9 0.2 11/02/06 09:25:12 32.3 94.2 20.9 0.1 11/02/06 09:25:22 32.8 94.2 20.9 0.1 11/02106 09:25:32 33.0 93.1 20.9 0.1 11/02/06 09:25:42 33.2 91.1 20.9 0.1 11/02106 09:25:52 33.6 88.5 20.9 0.1 11/02106 09:26:02 33.7 87.0 21.0 0.1 11102106 09:26:12 34.2 85.3 21.0 0.1 11/02106 09:26:22 34.9 83.7 20.9 0.1

Page 1 

# 8911/2106 Run #1

11/02/06 09:26:32 34.3 81.0 20.8 0.1 11/02106 09:26:42 34.8 78.2 20.8 0.1 11/02106 09:26:52 33.9 75.8 20.8 0.1 11/02/06 09:27:02 32.9 74.4 20.9 0.1 11/02/06 09:27:12 32.1 72.9 20.9 0.1 11/02106 09:27:22 30.5 71.2 20.8 0.1 11/02106 09:27:32 29.7 70.1 20.7 0.1 11/02106 09:27:42 29.1 69.3 20.7 0.0 11/02106 09:27:52 28.7 68.5 20.6 0.0 11/02/06 09:28:02 28.2 67.8 20.6 0.1 11/02/06 09:28:12 28.0 66.8 20.7 0.1 11/02106 09:28:22 28.0 65.8 20.7 0.0 11/02106 09:28:32 28.0 65.3 20.7 0.1 11/02/06 09:28:42 28.1 64.8 20.6 0.1 11/02/06 09:28:52 28.4 64.8 20.5 0.1 11/02/06 09:29:02 28.8 65.3 20.2 0.1 11/02106 09:29:12 29.7 66.4 20.1 0.1 11/02106 09:29:22 30.9 67.8 20.0 0.0 11/02106 09:29:32 31.7 69.1 19.8 

## o.o 11/02/06 09:29:42 32.5 70.2 19.6 0.0 11/02/06 09:29:52 32.9 70.9 19.6 0.0 11/02/06 09:30:02 32.6 71.9 19.6 0.0 11/02106 09:30:12 32.3 n.5 19.6 0.0 11/02/06 09:30:22 32.1 72.5 19.7 0.0 11/02/06 09:30:32 31.7 72.7 19.8 0.0 11/02/06 09:30:42 31.2 72.8 19.8 0.0 11/02/06 09:30:52 30.7 73.8 19.9 0.0 11/02106 09:31:02 30.0 76.0 20.0 0.1 11/02/06 09:31:12 29.2 78.8 20.0 0.0 11/02/06 09:31 :22 28.4 82.1 20.1 0.1 11/02106 09:31:32 27.9 85.3 20.3 0.0 

# . 11/02106 09:31:42 27.7 87.9 20.4 0.0 11/02106 09:31:52 27.5 90.0 20.4 0.0 11/02/06 09:32:02 27.6 91.9 20.5 0.0 11/02/06 09:32:12 28.8 93.2 20.7 0.0 11/02/06 09:32:22 29.6 93.7 20.8 0.0 11/02106 09:32:32 29.9 94.0 20.9 0.0 11/02106 09:32:42 30.0 94.3 21.0 0.0 11/02/06 09:32:52 30.4 94.6 21.1 0.1 11/02106 09:33:02 30.5 94.5 21.2 0.0 11/02106 09:33:12 31.4 94.6 21.4 0.0 11/02/06 09:33:22 32.2 94.7 21.5 0.0 11102106 09:33:32 33.2 94.9 21.6 0.0 11/02106 09:33:42 33.6 95.2 21.8 0.0 11/02106 09:33:52 34.3 95.4 21.8 0.0 11/02106 09:34:02 35.1 95.2 21.8 0.0 11/02106 09:34:12 35.3 95.2 21.9 0.0 11/02/06 09:34:22 35.1 95.3 22.1 0.1 11/02/06 09:34:32 34.1 95.2 22.1 0.0 11/02106 09:34:42 33.3 95.7 22.2 0.0 11/02/06 09:34:52 32.8 95.7 22.2 0.0 11/02/06 09:35:02 32.3 96.0 22.3 0.0 11/02/06 09:35:12 31.7 96.0 22.5 0.0 11/02106 09:35:22 30.9 95.7 22.6 0.0 11/02/06 09:35:32 31.0 95.4 22.5 -0.1 11/02/06 09:35:42 30.8 94.5 22.4 -0.1 11/02106 09:35:52 31.1 93.8 22.5 -0.1 11/02/06 09:36:02 31.2 93.2 22.4 -0.1 11/02106 09:36:12 31.2 92.2 22.4 -0.1 11/02106 09:36:22 30.6 91.8 22.4 0.0 11/02/06 09:36:32 30.5 91.1 22.4 -0.1 11/02/06 09:36:42 30.7 90.8 22.4 -0.2 11/02/06 09:36:52 30.9 90.6 22.4 -0.1 11/02/06 09:37:02 31.0 90.7 22.4 -0.2 11/02106 09:37:12 31.4 90.9 22.4 -0.2 11/02106 09:37:22 31.5 90.9 22.5 -0.3 11/02106 09:37:32 31.9 90.9 22.5 -0.2 11/02/06 09:37:42 32.2 90.9 22.6 -0.1 11/02/06 09:37:52 32.3 90.8 22.7 -0.1 11/02/06 09:38:02 32.1 90.8 22.7 ·0.2 11/02/06 09:38:12 32.2 90.9 22.9 -0.2 11/02/06 09:38:22 32.5 90.9 23.0 -0.2 11/02106 09:38:32 32.7 90.9 23.0 0.0 11/02/06 09:38:42 32.5 90.8 23.1 0.0

Page 2 

# 901112/06 Run #1

11102/06 09:38:52 32.3 90.5 23.1 0.0 11/02/06 09:39:02 32.1 90.0 23.1 0.0 11/02/06 09:39:12 32.1 89.4 23.1 -0.1 11/02/06 09:39:22 31.7 88.8 23.1 -0.1 11102106 09:39:32 31.4 88.2 23.0 -0.1 11/02106 09:39:42 31.1 87.9 22.9 -0.1 11/02106 09:39:52 30.6 87.7 22.7 -0.2 11/02/06 09:40:02 30.3 87.9 22.6 -0.1 11/02/06 09:40:12 30.3 88.2 22.5 -0.1 11/02/06 09:40:22 30.3 89.0 22.4 -0.1 11/02/06 09:40:32 30.2 90.0 22.4 -0.1 11/02106 09:40:42 30.1 92.0 22.4 -0.1 11/02/06 09:40:52 30.5 94.0 22.4 -0.2 11/02/06 09:41:02 30.7 95.7 22.4 -0.2 11/02/06 09:41:12 31.0 97.1 22.5 -0.1 11/02106 09:41:22 31.5 98.0 22.6 0.0 11/02106 09:41:32 31.9 98.1 22.6 0.0 11/02/06 09:41:42 32.1 98.0 22.6 0.0 11/02106 09:41:52 32.1 97.7 22.7 0.0 11/02/06 09:42:02 32.1 96.9 22.7 0.0 11/02106 09:42:12 32.6 96.5 22.7 0.0 11/02106 09:42:22 32.9 95.8 22.8 0.0 11/02/06 09:42:32 332 95.5 22.9 0.0 11/02/06 09:42:42 33.1 952 22.8 0.0 11/02/06 09:42:52 32.7 94.8 22.8 0.1 11/02/06 09:43:02 32.1 94.7 22.8 0.1 11/02/06 09:43:12 31.9 94.4 22.8 0.0 11/02106 09:43:22 31.2 94.1 22.8 0.0 11/02/06 09:43:32 30.9 94.0 22.8 -0.1 11/02/06 09:43:42 30.4 93.4 22.8 -0.1

, 11/02106 09:43:52 29.9 93.4 22.9 0.0 11/02/06 09:44:02 29.8 93.5 22.8 0.0 11/02/06 09:44:12 29.6 93.5 22.8 0.0 11/02106 09:44:22 28.9 93.3 22.7 0.0 11/02106 09:44:32 28.4 93.0 22.8 0.0 11/02/06 09:44:42 28.2 92.7 22.8 0.0 11/02106 09:44:52 28.2 92.E,; 22.9 0.0 11/02/06 09:45:02 28.6 92.6 22.9 0.0 11/02106 09:45:12 29.0 92.9 22.9 0.0 .11/02106 09:45:22 29.4 93.3 22.9 -0.1 11102/06 09:45:32 29.9 93.9 22.9 -0.1 -11/02/06 09:45:42 30.7 94.3 22.9 -0.1 11/02106 09:45:52 31.5 94.8 22.9 -0.1 11/02106 09:46:02 32.2 95.1 23.0 0.0 11/02106 09:46:12 32.6 95.1 23.0 0.0 11/02/06 09:46:22 33.0 95.3 23.0 0.0 11/02106 09:46:32 33.3 95.2 23.0 0.0 11/02/06 09:46:42 33.6 95.3 23.0 0.0 11/02/06 09:46:52 33.7 95.4 22.9 0.0 11/02/06 09:47:02 34.1 94.9 22.8 0.0 11/02/06 09:47:12 33.6 94.7 22.8 0.0 11/02/06 09:47:22 33.6 94.7 22.8 0.1 11/02/06 09:47:32 33.7 94.8 22.9 0.1 11/02106 09:47:42 32.7 95.0 22.9 0.0 11/02106 09:47:52 32.1 95.1 22.9 -0.1 11/02106 09:48:02 31.2 95.3 22.9 -0.1 11/02/06 09:48:12 30.6 95.3 22.9 0.0 11/02/06 09:48:22 30.1 95.1 22.9 0.0 11/02/06 09:48:32 29.9 94.6 22.8 0.0 11/02/06 09:48:42 30.0 94.2 22.7 0.0 11/02106 09:48:52 29.6 93.9 22.7 0.0 11/02/06 09:49:02 29.7 93.8 22.7 0.0 11/02/06 09:49:12 29.8 93.5 22.6 0.0 11/02106 09:49:22 29.7 93.9 22.6 -0.1 11/02106 09:49:32 29.5 94.1 22.7 0.0 11/02106 09:49:42 28.8 94.0 22.7 0.0 11102/06 09:49:52 28.4 93.6 22.7 0.0 11/02106 09:50:02 28.4 93.1 22.7 -0.1 11102/06 09:50:12 28.8 92.4 22.7 -0.1 11/02/06 09:50:22 29.2 91.7 22.8 -0.1 11/02/06 09:50:32 29.8 91.2 22.8 -0.1 11/02/06 09:50:42 30.4 90.9 23.0 -0.1 11/02/06 09:50:52 312 90.7 23.1 -0.1 11/02/06 09:51:02 32.0 90.2 23.2 -0.2

Page 311/2/06 Run #1

11/02106 09:51 :12 32.2 90.2 23.2 -0.2 11/02/06 09:51 :22 32.4 90.3 23.2 -0.2 11/02/06 09:51:32 32.8 90.5 23.2 -0.2 11/02/06 09:51:42 32.6 91.1 23.3 -0.2 11/02/06 09:51 :52 33.1 91.4 23.4 -0.2 11/02106 09:52:02 32.8 91.5 23.5 -0.2 11/02106 09:52:12 32.7 91.6 23.5 -0.2 11/02/06 09:52:22 32.9 91.7 23.5 -0.2 11/02/06 09:52:32 33.1 92.0 23.5 

## -o.2 11/02/06 09:52:42 32.2 92.0 23.5 -0.2 11102/06 09:52:52 31.0 92.5 23.3 -0.1 11/02/06 09:53:02 29.7 92.9 23.3 -0.1 11/02/06 09:53:12 28.6 93.1 23.4 -0.2 11/02106 09:53:22 27.4 93.2 23.5 -0.1 11/02/06 09:53:32 27.0 92.8 23.3 0.0 11/02/06 09:53:42 26.7 92.0 23.3 -0.1 11/02/06 09:53:52 27.1 91.4 23.3 -0.1 11/02/06 09:54:02 27.1 91.1 23.3 -0.1 11/02/06 09:54:12 27.8 90.7 23.4 -0.1 11/02106 09:54:22 28.1 90.2 23.4 -0.1 11/02/06 09:54:32 28.9 89.8 23.4 -0.1 11/02/06 09:54:42 29.4 90.3 23.4 -0.1 11/02/06 09:54:52 30.0 90.4 23.4 -0.1 11/02/06 09:55:02 31.1 89.6 23.2 -0.1 11/02106 09:55:12 31.5 87.8 23.1 -0.1 11/02/06 09:55:22 32.8 85.6 23.0 -0.1 11/02106 09:55:32 33.2 83.3 22.9 0.0 11/02/06 09:55:42 33.6 82.1 22.6 -0.1 11/02/06 09:55:52 33.5 80.1 22.5 -0.2 11/02/06 09:56:02 33.1 76.8 22.3 -0.2 11/02106 09:66:12 32.6 73.9 22.2 0.0 11/02/06 09:56:22 31.5 71.7 22.1 0.0 11/02/06 09:56:32 30.3 71.0 22.0 0.0 11/02106 09:56:42 28.4 70.8 21.8 -0.1 11/02106 09:56:52 27.6 70.9 21.6 -0.1 11/02/06 09:57:02 26.9 71.2 21.6 -0.1 11/02/06 09:57:12 26.7 71.9 21.4 -0.1 11/02/06 09:57:22 26.7 72.9 21.4 -0.1 11/02/06 09:57:32 27.3 74.0 21.3 -0.2 11/02106 09:57:42 28.1 75.8 21.2 -0.1 11/02106 09:57:52 28.1 77.8 21.2 0.0 11/02/06 09:58:02 29.4 79.5 21.1 0.0 11/02/06 09:58:12 30.3 80.7 21.1 -0.1 11/02106 09:58:22 30.5 81.2 21.0 -0.1 11/02/06 09:58:32 31.4 81.5 21.1 -0.1 11/02/06 09:58:42 32.0 81.5 21.1 -0.1 11/02106 09:58:52 33.6 81.4 21.2 -0.1 11/02106 09:59:02 35.2 81.5 21.1 -0.1 11/02106 09:59:12 35.6 82.5 21.3 -0.1 11/02/06 09:59:22 35.0 83.9 21.4 -0.1 11/02106 09:59:32 34.7 85.5 21.5 -0.1 11102106 09:59:42 34.1 87.1 21.5 -0.1 11/02/06 09:59:52 33.0 88.0 21.6 -0.1 11/02/06 10:00:02 32.0 87.9 21.6 -0.2 11/0210610:00:12 30.7 86.3 21.6 -0.2 11/02/06 10:00:22 29.9 83.3 21.6 -0.2 11/02/06 10:00:32 29.7 80.8 21.5 -0.2 11/02/06 10:00:42 29.2 79.1 21.3 -0.3 11/02106 10:00:52 28.5 76.7 21.1 -0.2 11/02/06 10:01:02 27.9 73.6 21.0 -0.2 11/02/06 10:01:12 27.9 70.8 20.9 -0.3 11/02/06 10:01:22 27.6 69.5 20.7 -0.3 11/02106 10:01:32 27.8 68.2 20.6 0.0 11/02/06 10:01 :42 27.8 67.2 20.4 -0.1 11/02106 1 0:01 :52 27.8 66.8 20.4 -0.2 11/02106 10:02:02 28.0 67.3 20.4 -0.2 11/02/06 10:02:12 28.3 68.3 20.7 -0.1 11/02/06 10:02:22 29.6 69.5 20.6 -0.1 11/02/0610:02:32 30.3 69.9 20.4 -0.1 11/02/0610:02:42 30.7 70.2 20.3 -0.1 11/02106 10:02:52 30.8 70.2 20.2 0.0 11/02/06 10:03:02 30.4 70.3 20.0 -0.1 11/0210610:03:12 30.2 70.1 20.0 -0.1 11/02/06 10:03:22 29.9 69.9 20.0 -0.1

Page4 

# 9211/2/06 Run #1

11/02106 10:03:32 29.1 70.0 20.2 -0.1 11/02106 10:03:42 29.4 70.4 20.2 0.0 11/02106 10:03:52 29.6 71.2 20.4 0.0 11/02106 10:04:02 29.4 73.5 20.6 -0.1 11/02106 10:04:12 29.3 74.7 20.8 -0.2 11/02106 10:04:22 28.8 74.6 20.8 -0.2 11/02106 10:04:32 29.0 73.4 20.8 -0.2 11/02106 10:04:42 28.7 

### n.9 20.7 -0.1 11/02/0610:04:52 28.4 73.2 20.8 -0.1 11/02106 10:05:02 28.7 72.3 20.8 0.0 11/02106 10:05:12 29.3 70.5 20.7 -0.1 11/02/06 10:05:22 30.3 68.5 20.8 -0.1 11/02/06 10:05:32 30.3 66.9 20.7 -0.2 11/02/06 10:05:42 30.9 66.1 20.6 -0.2 11/02/06 10:05:52 30.8 64.7 20.7 -0.1 11/02106 10:06:02 30.4 63.3 20.8 -0.1 11102106 10:06:12 30.7 61.7 20.8 -0.2 11/02/06 10:06:22 29.8 60.7 20.8 -0.3 11/02106 10:06:32 29.8 60.4 20.8 -0.3 11/02106 10:06:42 29.8 59.7 20.7 -0.2 11/02106 10:06:52 29.6 59.0 20.8 -0.1 11/02/06 10:07:02 29.3 58.3 20.6 -0.1 11/02106 10:07:12 28.2 58.0 20.7 -0.1 11/02/06 10:07:22 27.2 57.8 20.6 -0.2 11/02/06 10:07:32 26.8 57.7 20.4 -0.2 11/02106 10:07:42 26.5 58.7 20.3 -0.3 11/02106 10:07:52 26.6 60.5 20.2 -0.3 11/02106 10:08:02 26.7 62.1 20.0 -0.1 11/02/06 10:08:12 27.0 63.7 19.9 -0.1 11/02106 10:08:22 27.5 65.0 19.8 -0.1 11/02106 10:08:32 

# . 27.4 66.6 19.8 -0.2 11/02106 10:08:42 27.4 67.9 19.9 -0.2 11/02106 1 0:08:52 27.2 68.4 20.2 -0.1 11/02106 10:09:02 27.1 68.6 20.5 -0.1 11/02/0610:09:12 27.6 68.9 20.7 -0.1 11/02106 10:09:22 27.9 70.0 20.7 -0.1 11/02/06 10:09:32 28.7 71.3 20.7 -0.2 11/02106 10:09:42 29.7 74.7 20.5 -0.4 11/02106 10:09:52 30.7 78.7 20.4 -0.5 11/02106 10:10:02 32.2 82.6 20.2 -0.4 11/02106 10:10:12 33.8 86.1 20.1 -0.3 11/02106 10:10:22 34.5 88.2 20.0 -0.3 1 1/02106 10:10:32 34.3 89.9 20.0 -0.2 11/02/06 10:10:42 33.3 91.1 20.0 -0.2 11/02/06 10:10:52 32.0 92.0 20.0 -0.2 11/0210610:11:02 30.5 92.8 20.1 0.0 11/02106 10:11:12 29.0 93.2 20.2 0.0 11/0210610:11:22 26.6 93.3 20.4 0.0 11/02106 10:11:32 26.1 93.1 20.6 0.0 11/02106 10:11:42 25.6 92.9 20.8 0.0 11/02/0610:11:52 25.5 92.5 20.9 0.0 11/02/06 10:12:02 25.5 92.3 20.9 0.0 11/02/06 10:12:12 26.0 91.7 21.0 0.0 11/02/06 10:12:22 26.1 91.0 21.0 0.0 11/02/06 10:12:32 25.7 90.0 21.0 -0.1 11/02/0610:12:42 25.5 89.0 21.1 0.0 11/02/0610:12:52 25.4 88.4 21.2 0.0 11/0210610:13:02 25.7 88.2 21.2 0.0 11/02/06 10:13:12 27.4 88.3 21.1 -0.1 11/02/0610:13:22 29.3 88.8 21.1 0.0 11/02/06 10:13:32 30.1 90.0 21.0 0.0 11/02/06 10:13:42 30.5 91.0 21.0 0.0 11/02/06 10:13:52 30.5 91.7 21.5 0.0 11/02/06 10:14:02 31.0 92.1 22.5 -0.1 11/02/06 10:14:12 31.2 92.7 23.0 -0.1 11/02106 10:14:22 30.8 93.3 23.2 -0.1 11/02106 10:14:32 30.2 94.0 23.3 -0.2 11/02/06 10:14:42 29.7 94.3 23.2 -0.2 11/02/06 10:14:52 29.1 94.5 22.8 -0.1 11/02106 10:15:02 28.4 94.0 22.4 -0.1 11/02/0610:15:12 26.9 92.7 22.0 -0.1 11/02/06 10:15:22 25.7 90.5 21.8 -0.1 11/02106 10:15:32 25.4 88.5 21.6 -0.1 11/0210610:15:42 25.2 85.8 21.5 0.0 

# 93 Page 511/2/06 Run #1

11/02/0610:15:52 25.6 82.4 21.4 0.0 11/02/06 10:16:02 26.0 79.9 21.1 0.0 11/02106 10:16:12 25.9 78.9 21.1 0.0 11/02/06 10:16:22 26.2 79.9 21.0 0.0 11/02106 10:16:32 26.2 83.1 21.2 -0.1 11/02106 10:16:42 26.8 88.1 21.3 -0.1 11/02106 10:16:52 27.5 93.2 21.4 -0.1 11/02/06 10:17:02 28.0 98.3 21.5 -0.1 11/02/0610:17:12 28.5 102.6 21.4 -0.1 11/02/06 10:17:22 29.4 105.7 21.3 -0.1 11/02/06 10:17:32 30.0 108.9 21.2 -0.1 11/02/06 10:17:42 30.3 112.2 21.0 -0.1 11/02/06 10:17:52 31.0 114.7 21.0 -0.1 Stop Run #1 30.85 86.60 21.67 0.03 11/02106 10:18:02 31.3 116.1 20.9 -0.1 11/02106 10:18:12 32.1 116.2 20.9 -0.1 11/0210610:18:22 14.4 116.3 20.7 -0.2 11/02106 10:18:32 4.4 101.2 19.5 0.0 11/02/06 10:18:42 4.8 59.9 13.1 0.0 11/02106 10:18:52 5.1 32.5 8.9 -0.1 11/02106 10:19:02 5.1 18.9 7.3 -0.1 11/02/06 10:19:12 5.1 11.4 6.7 -0.2 11/02106 10:19:22 5.1 6.2 6.3 -0.2 11/02/06 10:19:32 5.2 3.4 5.8 -0.3 11/02/0610:19:42 5.2 1.4 5.4 -0.3 11/02/06 10:19:52 5.9 0.4 5.0 -0.4 11/02/06 10:20:02 7.0 -0.2 8.3 -0.3 11/02106 10:20:12 7.8 0.0 15.4 -0.3 11/02/06 10:20:22 8.0 

# . 0.9 19.6 -0.4 11/02/06 10:20:32 7.6 0.3 22.2 -0.4 11/0210610:20:42 7.2 0.2 23.6 -0.3 11/02/06 10:20:52 7.0 -0.2 24.4 -0.3 11/02/06 10:21:02 6.4 -0.2 24.7 -0.1 11/02/06 10:21:12 4.9 -0.1. 

### 25.1 -0.1 11/02106 1 0:21 :22 3.8 -0.2 

### 25.1 -0.1 25 ppm NOx 11/02/06 10:21:32 3.0 1.5 

### 25.1 0.0 ZeroS02 11/02106 10:21:42 2.4
. 2.7 

### 25.0 -0.1 11/0210610:21:52 2.0 2.6 25.1 -0.1 11/02106 10:22:02 1.7 2.4 25.1 -0.1 11/02/0610:22:12 1.3 4.1 24.0 ·0.2 11/02/06 10:22:22 1.0 31.2 17.9 -0.2 11/02/06 10:22:32 0.9 61.7 9.7 -0.2 11/02/0610:22:42 0.8 78.7 5.6 -0.2 11/02106 10:22:52 0.8 87.2 3.5 -0.2 11/02/0610:23:02 0.8 90.5 2.5 -0.1 11/0210610:23:12 0.8 92.6 2.0 0.0 11/02/0610:23:22 0.7 94.0 1.7 -0.1 11/02/06 10:23:32 0.5 94.7 1.5 0.0 11/02106 10:23:42 0.5 95.4 1.3 -0.1 11102106 10:23:52 0.5 95.7 1.2 -0.1 11/02/06 10:24:02 0.5 96.0 1.1 -0.1 11/02/06 10:24:12 0.5 96.3 1.0 ·0.1 11/02106 10:24:22 0.5 96.4 0.9 -0.1 11102/06 10:24:32 0.5 

### 96.6 0.8 -0.2 11/0210610:24:42 0.5 

### 96.6 0.7 -0.1 99.1 ppm CO 11/02/06 10:24:52 0.5 

### 96.5 0.7 -0.1 11/02106 10:25:02 0.5 

### 96.6 0.6 -0.1 11/02/06 10:25:12 0.5 96.6 0.6 0.0 11/02/06 10:25:22 0.5 95.3 0.6 0.0 11/02106 10:25:32 0.5 79.5 0.6 ·0.1 11/02/06 10:25:42 0.5 46.9 0.6 0.1 11/02/06 10:25:52 0.5 25.9 0.6 1.2 11/02106 10:26:02 0.3 15.9 0.6 3.5 11/02/0610:26:12 0.3 10.9 0.6 7.0 11/02/06 10:26:22 0.5 8.2 0.5 10.8 11/02/06 10:26:32 0.3 6.4 0.5 14.9 11/02/06 10:26:42 0.3 5.4 0.5 18.7 11/02/06 10:26:52 0.3 4.6 0.5 22.3 11/02/0610:27:02 0.3 4.0 0.4 25.4 11/02/0610:27:12 0.3 3.6 0.4 28.0

Page 6 

# 94·1112/06 Run #1

11/02/06 10:27:22 0.3 3.4 0.4 30.2 11/02/06 10:27:32 0.3 3.2 0.4 32.0 11/02106 10:27:42 0.3 3.1 0.4 33.7 11/02106 10:27:52 0.3 2.8 0.3 35.1 11/02/0610:28:02 0.3 2.6 0.3 36.3 11/02/06 10:28:12 0.3 2.5 0.3 37.4 11/02/0610:28:22 0.3 2.6 0.3 38.3 11/0210610:28:32 0.3 2.2 0.3 38.8 11/02/06 10:28:42 0.2 1.8 0,3 39.4 11/02/06 10:28:52 0.2 2.0 0.3 40.1 11/02106 10:29:02 0.2 1.9 0.3 40.7 11/02/06 10:29:12 0.2 2.0 0.3 41.3 11/02106 10:29:22 0.2 1.9 0.3 41.6 11/02106 1 0:29:32 0.2 1.8 0.3 41.9 11/0210610:29:42 0.2 1.8 0.2 42.2 11/02106 10:29:52 0.2 1.8 0.2 42.5 11/02106 10:30:02 0.3 2.0 0.2 42.8 11/02/0610:30:12 0.3 2.1 0.2 43.1 11 /02/06 1 0:30:22 0.3 1.9 0.2 43.3 11/02/06 1 0:30:32 0.2 1.8 0.2 43.6 11/02/06 10:30:42 0.2 1.7 0.2 43.9 11/0210610:30:52 0.2 1.8 0.2 44.0 11/0210610:31:02 0.2 1.8 0.2 44.0 11/02/0610:31:12 0.2 1.9 0.2 44.0 11/02106 10:31:22 0.3 1.9 0.1 44.0 11/0210610:31:32 0.2 1.9 0.1 44.0 11/0210610:31:42 0.2 1.9 0.1 44.5 11/02/0610:31:52 0.2 2.0 0.1 45.5 11/02/0610:32:02 0.2 1.8 0.1 45.6 11/02/06 10:32:12 0.2 1.7 0.1 45.7 11/02106 10:32:22 0.2 1.9 • 0.2 46.0 11/02106 10:32:32 0.2 2.3 0.1 46.3 11/0210610:32:42 

## 0.2 2.4 0.1 46.4 11/02/0610:32:52 

### 0.3 2.4 0.1 46.5 ZeroVOC 11/02/06 10:33:02 

### 0.2 2.3 0.1 

### 46.8 11/02/0610:33:12 

### 0.2 2.2 0.1 47.1 49.8ppm 502 11/02/06 10:33:22 1.0 

### 2.2 0.1 47.4 Zero CO, NOx

. 11/0210610:33:32 37.6 

### 2.1 ·.0.2 47.0

11/02106 10:33:42 42.4 2.1 0.2 46.7 11/02/06 10:33:52 41.9 2.1

. 0.1 45.9 11/02/0610:34:02 

### 41.0 2.2 0.1 42.7 11/02/0610:34:12 

### 41.0 2.1 0.1 37.4 11/02/06 10:34:22 

### 41.0 2.1 0.1 31.7 11/02106 10:34:32 

### 41.1 2.0 0.1 26.5 11/02/06 10:34:42 41.2 2.1 0.1 22.2



# 95·
Page71112/06 Run #2

Date/Time 

### voc co NOx 502 mrnldcllyy hh:mm:ss ppm ppm ppm ppm 11/02106 10:39:52 24.2 125.8 21.9 0.5 Start Run #2. 11/02/06 10:40:02 24.4 126.6 22.2 0.4 11/02106 10:40:12 24.7 127.3 22.2 0.4 11/02/06 10:40:22 24.7 127.9 22.4 0.4 11/02/06 10:40:32 24.9 128.2 22.4 0.3 11/02/06 10:40:42 24.7 128.2 22.6 0.2 11/02/06 10:40:52 24.8 128.3 22.4 0.1 11/02/06 10:41:02 25.4 128.3 22.4 0.1 11102/06 10:41:12 25.7 128.5 22.3 0.2 11/02/0610:41:22 25.7 128.4 22.3 0.2 11/02106 10:41:32 26.2 128.5 22.3 0.1 11/0210610:41:42 26.3 128.7 22.2 0.1 11/02/06 10:41:52 26.5 129.1 22.2 0.0 11/02106 10:42:02 26.7 128.9 22.2 0.0 11/02106 10:42:12 27.0 128.8 22.3 0.0 11/02/06 1 0:42:22 27.4 128.7 22.5 0.0 11/02/06 10:42:32 27.6 128.4 22.7 0.0 11/02106 10:42:42 27.6 128.4 22.6 0.0 11/02106 10:42:52 27.1 128.2 22.5 0.0 11/02106 10:43:02 26.5 128.3 22.4 0.0 11102/06 10:43:12 26.1 128.4 22.2 0.1 11102106 10:43:22 25.8 128.6 22.0 0.0 11/02/06 10:43:32 26.0 129.2 21.7 -0.1 11/02106 10:43:42 25.8 130.1 21.5 -0.1 11/02/06 10:43:52 25.7 131.2 21.2 0.0 11/0210610:44:02 25.5 132.2 21.1 -0.1 11/02/06 10:44:12 25.3 132.9 21.1 0.0 11/02/06 10:44:22 24.8 133.0 21.2 -0.1 11/02/0610:44:32 24.6 132.4 21.1 -0.1 11/02/06 10:44:42 24.2 131.8 21.1 -0.2 11/02/06 10:44:52 24.3 130.8 21.0 -0.2 11/02106 10:45:02 24.6 130.5 21.0 -0.1 11/02106 10:45:12 24.9 129.9 20.9 0.0 11/02/06 10:45:22 25.9 129.6 20.9 -0.1 11/02106 10:45:32 26.4 129.7 20.9 -0.3 11/02106 10:45:42 26.8 129.6 20.9 -0.2 11/02/06 10:45:52 27.0 129.8 21.0 -0.2 11/02106 10:46:02 27.5 129.9 21.1 -0.-2 11/02/0610:46:12 27.9 130.1 21.0 -0.2 11/02/06 10:46:22 28.2 130.3 20.9 -0.2 11/02/06 10:46:32 28.6 130.9 20.9 -0.3 11/0210610:46:42 29.1 131.2 20.9 -0.3 11/02106 10:46:52 28.8 131.2 20.9 -0.3 11/02/06 10:47:02 28.4 131.1 20.9 -0.3 11/02106 10:47:12 28.4 130.6 20.9 -0.2 11/02/06 10:47:22 28.5 130.2 20.8 -0.2 11/02106 10:47:32 27.8 129.6 20.7 -0.3 11/02106 10:47:42 27.0 129.8 20.6 -0.2 11/02/06 10:47:52 26.3 130.6 20.6 -0.4 11/02/06 10:48:02 26.0 131.6 20.5 -0.4 11/0210610:48:12 25.6 131.7 20.6 -0.3 11/02/0610:48:22 25.7 131.8 20.7 -0.2 11/02106 10:48:32 25.7 132.1 20.8 -0.4 11/02/06 10:48:42 26.0 132.1 20.9 -0.3 11/02/06 10:48:52 26.7 132.1 21.0 -0.3 11/0210610:49:02 27.0 132.3 21.0 -0.3 11102/0610:49:12 27.1 132.2 21.1 -0.3 11/02/06 10:49:22 27.4 132.1 21.2 -0.3 11/02106 10:49:32 28.0 131.6 21.2 -0.3 11/02106 10:49:42 28.4 131.3 21.3 -0.4 11/02106 10:49:52 28.7 131.0 21.4 -0.3 11/02/06 10:50:02 29.8 130.5 21.4 -0.3 11/02/06 10:50:12 30.1 130.2 21.7 -0.4 11/02106 10:50:22 30.6 130.0 21.7 -0.4 11/02/06 10:50:32 31.4 130.1 21.7 -0.4 11102/06 10:50:42 31.8 130.7 21.7 -0.4 11/02/06 10:50:52 31.2 131.1 21.8 -0.4 11/02/06 10:51 :02 30.5 131.5 21.7 -0.5 11/02106 10:51:12 29.5 131.6 21.7 -0.4 11/02/06 10:51:22 28.9 131.6 21.6 -0.4

Page 1 

# 9611/2/06 Run #2

11/02/0610:51:32 28.4 132.0 21.7 -0.4 11/02/06 10:51:42 27.7 132.3 21.7 -0.4 11/02/0610:51:52 27.1 132.6 21.7 -0.4 11/02106 10:52:02 26.5 132.8 21.5 -0.5 11/02/06 10:52:12 26.4 132.1 21.5 -0.6 11102/06 10:52:22 26.3 131.7 21.4 -0.5 11/02/0610:52:32 26.2 131.4 21.3 -0.4 11/0210610:52:42 26.6 131.4 21.4 -0.3 11/02/0610:52:52 27.2 131.7 21.3 -0.3 11/02106 1 0:53:02 27.6 132.2 21.4 -0.3 11/02106 10:53:12 28.4 132.7 21.4 -0.3 11/02106 10:53:22 28.9 132.8 21.4 -0.3 11/02106 10:53:32 29.2 133.0 21.3 -0.4 11/0210610:53:42 29.8 133.2 21.3 -0.5 11/02106 10:53:52 30.4 133.9 21.4 -0.5 11/02106 10:54:02 31.2 134.5. 21.5 -0.4 11/02/06 10:54:12 31.6 135.5 21.6 -0.5 11/02/06 10:54:22 31.8 136.1 21.7 -0.4 11/02/06 10:54:32 31.7 136.6 21.8 -0.2 11/02/06 10:54:42 31.4 136.9 22.1 -0.1 11/02/06 10:54:52 30.9 137.4 22.1 0.0 11/02/06 10:55:02 30.2 138.3 22.0 0.0 11/02/06 10:55:12 29.7 138.1 22.0 -0.1 1 1/02106 10:55:22 29.5 136.6 21.9 0.0 11/0210610:55:32 29.1 134.7 21.8 0.0 11/02/0610:55:42 28.4 132.7 21.6 0.0 11/02/06 10:55:52 27.9 130.9 21.5 0.0 11102/06 10:56:02 27.1 128.9 21.4 -0.1 11/02/0610:56:12 26.6 127.3 21.5 -0.1 11/02/06 10:56:22 26.6 126.6 21.7 -0.1 11/02/06 10:56:32 26.4 126.7 21.8 -0.1 11/02/0610:56:42 26.3 127.7 21.8 -0.2 11/02106 10:56:52 26.6 129.0 21.6 -0.3 11/02/06 10:57:02 27.4 129.7 21.5 -0.2 11/02/0610:57:12 27.6 130.4 21.4 -0.1 11/02/06 10:57:22 27.7 131.2 21.3 -0.1 11/02/06 10:57:32 28.2 131.5 21.4 -0.1 11/02/06 10:57:42 28.4 131.9 21.5 0.0 11/02106 10:57:52 29.1 132.1 21.5 -0.1 11/0210610:58:02 29.9 132.1 21.6 -0.2 11/02/06 10:58:12 30.9 132.0 21.6 -0.2 11/0210610:58:22 31.4 132.0 21.5 .0.2 11/02/06 10:58:32 32.3 132.1 21.4 -0.1 11/02/0610:58:42 33.0 132.2 21.4 -0.1 11/02/06 10:58:52 32.7 132.7 21.4 -0.1 11/02/06 10:59:02 32.4 133.2 21.5 -0.1 11/02106 10:59:12 31.8 133.9 21.6 -0.1 11/02/06 10:59:22 31.0 134.5 21.5 -0.1 11/02106 10:59:32 30.4 134.7 21.6 .0.2 11/02/06 10:59:42 30.1 135.4 21.5 .0.2 11/02/06 10:59:52 29.8 136.0 21.4 0.0 11/02/06 11 :00:02 29.5 136.4 21.3 -0.1 11/02/06 11:00:12 29.5 136.2 21.3 -0.2 11/02/06 11:00:22 29.4 135.5 21.2 -0.2 11/02/06 11 :00:32 28.9 135.2 21.2 ·0.2 11/02/06 11:00:42 28.8 134.4 21.3 -0.2 11/02/06 11:00:52 28.3 133.9 21.3 -0.3 11/02106 11 :01 :02 28.4 133.7 21.3 -0.3 11/02/0611:01:12 28.4 133.2 21.5 -0.2

, 1/02/06 11 :01:22 29.0 133.1 21.5 -0.2 11/02/06 11 :01:32 29.4 133.0 21.6 -0.2 11/02/06 11 :01 :42 29.8 133.2 21.7 -0.2 11/02106 11 :01 :52 31.0 133.1 21.6 -0.2 11/02/06 11 :02:02 32.1 132.6 21.6 -0.1 11/02/0611:02:12 32.9 131.8 21.5 -0.1 11/02106 11 :02:22 34.0 130.7 21.5 -0.2 11/02/06 11 :02:32 34.4 129.7 21.5 ·0.2 11/02/06 11:02:42 34.5 129.3 21.5 -0.1 11/02/06 11:02:52 34.2 128.8 21.5 -0.1 11/02/06 11:03:02 34.0 128.7 21.4 -0.2 11/02/06 11 :03:12 33.7 128.9 21.4 -0.2 11/02/06 11:03:22 33.2 129.6 21.3 -0.2 11/02106 11 :03:32 33.1 130.3 21.2 -0.2 11/02/06 11:03:42 33.1 131.0 21.1 -0.1 

# 97 Page 21112/06 Run #2

11/02/06 11:03:52 32.8 131.4 21.1 0.0 11/02/06 11:04:02 32.1 131.4 21.1 0.0 11/0210611:04:12 31.3 131.2 21.1 -0.1 11/02/06 11:04:22 30.5 131.1 21.2 -0.2 11/02/06 11 :04:32 30.0 130.9 21.3 -0.2 11/02106 11:04:42 29.8 130.4 21.3 -0.3 11/02/06 11:04:52 29.7 129.9 21.2 -0.2 11/02/06 11 :05:02 30.2 129.7 21.2 -0.1 11/02/06 11:05:12 30.6 129.9 2'1.2 -0.'1 11/02/06 11:05:22 31.5 129.9 21.2 -0.1 11/02/06 11 :05:32 31.8 130.1 21.2 -0.1 11/02106 11 :05:42 32.6 130.2 21.2 -0.1 11/02106 11 :05:52 33.3 130.8 21.4 -0.1 11/02/06 11 :06:02 33.6 131.4 21.6 -0.2 11/02/06 11 :06:12 34.1 131.5 21.6 -0.2 11/02/06 11:06:22 34.3 131.5 21.7 -0.2 11/02106 11:06:32 34.4 131.7 21.7 -0.1 11/02/06 11:06:42 34.0 132.2 21.7 -0.1 11102106 11:06:52 33.6 132.6 21.6 -0.2 11/02/06 11 :07:02 32.9 133.1 21.6 -0.2 11/02/0611:07:12 32.1 133.1 21.5 -0.1 11/02/06 11:07:22 31.4 133.2 21.4 -0.1 11/02/06 11:07:32 30.5 132.8 21.4 -0.1 11/0210611:07:42 29.7 132.9 21.5 -0.1 11/02106 11 :07:52 29.7 132.9 21.7 -0.2 11/02/06 11 :08:02 29.7 132.9 21.7 -0.3 11/02/06 11:08:12 29.6 133.0 21.7 -0.2 11/02/06 11:08:22 29.8 132.8 21.7 -0.2 11/02106 11:08:32 30.3 132.7 21.7 -0.3 11/02106 11 :08:42 30.9 132.3 21.7 -0.3 11/02106 11:08:52 31.5 132.4 21.7 -0.3 11/02106 11:09:02 31.8 132.4 21.7 -0.3 11/02/06 11 :09:12 322 131.8 21.8 -0.4 11102/06 11 :09:22 32.5 131.6 21.9 -0.3 11/02/06 11:09:32 33.2 131.1 21.8 -0.3 11/02106 11 :09:42 33.6 131.0 21.8 -0.2 11/02106 11 :09:52 33.9 130.7 21.7 -0.2 11/02/06 11:10:02 34.7 131.2 21.6 -0.3 11/0210611:10:12 34.2 131.2 21.6 -0.3 11/02106 11:10:22 33.6 131.3 21.7 -0.3 11/02/0611:10:32 33.1 131.3 21.7 -0.3 11/02/06 11:10:42 32.2 131.8 21.7 -0.2 11/02/0611:10:52 31.6 132.2 21.8 -0.3 11/02/06 11:11:02 30.9 132.5 21.8 -0.3 11/02/0611:11:12 30.6 132.9 21.8 -0.2 11/02/06 11:11:22 29.9 133.0 21.9 -0.3 11/02/06 11:11:32 29.8 133.3 21.7 -0.2 11/02106 11:11:42 30.0 133.1 21.8 -0.2 11/02/0611:11:52 30.1 133.1 21.8 -0.3 11/02/0611:12:02 29.7 132.1 22.6 -0.3 11/02/06 11:12:12 29.0 130.4 24.0 -0.5 11/02/06 11:12:22 28.9 129.6 24.6 -0.5 11102/0611:12:32 28.9 129.4 24.5 -0.3 11/02/06 11:12:42 29.1 130.3 24.0 -0.3 11/02/06 11:12:52 29.5 131.2 23.4 -0.2 11/02/06 11:13:02 29.8 131.9 23.1 -0.3 11/02/0611:13:12 29.9 132.3 23.0 -0.3 11/0210611:13:22 30.1 132.1 22.9 -0.3 11102106 11 :13:32 30.2 132.0 23.0 -0.4 11/02/06 11:13:42 30.1 132.3 23.0 -0.4 11/02/0611:13:52 30.1 132.3 23.0 -0.3 11/02/06 11:14:02 29.7 132.2 23.0 -0.4 11/02/0611:14:12 29.3 132.3 22.9 -0.5 11/02/0611:14:22 29.1 132.6 22.8 -0.3 11/02/0611:14:32 28.7 132.4 22.7 -0.4 11/02/06 11 :14:42 28.1 132.2 22.5 -0.5 11/02106 11:14:52 28.1 131.6 22.5 -0.6 11/02/06 11:15:02 28.6 130.9 22.4 

## -o.s 11/02/06 11:15:12 29.0 130.3 22.3 -0.4 11/02/06 11:15:22 29.1 129.9 22.2 -0.4 11/02/06 11:15:32 29.6 129.0 22.2 -0.4 11/02/06 11:15:42 30.3 128.1 22.2 -0.4 11/02106 11 :15:52 30.9 127.6 22.1 -D.4 11/02/06 11:16:02 31.9 127.5 21.9 -0.3

Page 3 

# 9811/2106 Run #2

11/02/06 11:16:12 33.2 127.0 21.8 -0.4 11/02/06 11:16:22 33.9 126.7 21.6 -0.3 11/02/06 11:16:32 34.3 126.8 21.6 -0.4 11/02/06 11:16:42 34.1 127.1 21.8 -0.5 11102/06 11:16:52 33.1 127.2 22.6 -0.5 11102/0611:17:02 32.2 127.2 23.5 -0.5 11/02/0611:17:12 31.6 127.3 23.9 -0.4 11102/06 11:17:22 30.8 127.7 24.0 -0.4 11/02/0611:17:32 29.5 127.9 23.8 -0.5 11/02/06 11:17:42 28.7 127.6 23.6 -0.6 11/02/06 11:17:52 28.2 127.4 23.5 -0.6 11/02/06 11 :18:02 27.8 127.6 23.4 -0.5 11/02/06 11:18:12 27.2 128.0 23.3 -0.4 11/02/06 11 :18:22 27.2 128.1 23.3 -0.3 11/02/06 11:18:32 27.5 128.7 23.2 -0.4 11/02/06 11 :18:42 27.7 128.9 23.2 -0.4 11/02/06 11 :18:52 27.4 129.1 23.1 -0.5 11/02/06 11:19:02 27.4 1292 23.1 -0.5 11/02/0611:19:12 27.5 129.0 23.2 -0.4 11/02/06 11:19:22 27.9 129.0 23.3 -0.4 11/02/06 11:19:32 28.1 128.5 23.1 -0.5 11/02106 11:19:42 28.3 128.4 23.2 -0.5 11/02106 11:19:52 28.7 128.5 23.3 -0.5 11/02/0611:20:02 28.9 128.5 23.3 -0.6 11/02/0611:20:12 29.4 129.0 23.2 -0.5 11/02/06 11 :20:22 29.6 129.9 23.0 -0.6 11/02/06 11 :20:32 29.6 130.7 22.9 -0.5 11/02/06 11 :20:42 29.8 131.3 22.8 -0.6 11/02106 11 :20:52 30.1 131.6 22.8 -0.6 11/02/06 11:21:02 30.0 131.6 22.7 -0.5 11/02/0611:21:12- 28.7 131.4 22.6 -0.5 11/02/0611:21:22 28.2 130.9 22.6 -0.6 11/0210611:21:32 27.7 130.6 22.7 -0.7 11/02106 11:21:42 27.2 129.9 22.7 -0.6 11/0210611:21:52 26.3 128.7 23.2 -0.5 11/02106 11:22:02 25.7 127.7 23.5 -0.6 11/02106 11:22:12 25.3 127.5 23.7 -0.7 11/02/0611:22:22 25.3 127.6 23.6 -0.7 11/0210611:22:32 25.5 128.4 23.5 -0.6 11/0210611:22:42

. 25.9 128.9 23.5 -0.5 11/02/06 11 :22:52 26.4 129.5 23.4 -0.6 11/02/06 11:23:02

. 26.7 129.6 23.2 -0.7 11/0210611:23:12 27.4 129.4 23.2 -0.8 11/02/06 11 :23:22 27.6 129.2 23.2 -0.8 11/02106 11 :23:32 27.6 128.6 23.4 -0.7 11/02/06 11:23:42 27.4 127.7 23.7 -0.7 11/02106 11 :23:52 27.1 126.8 24.1 -0.7 11/02106 11:24:02 26.7 126.5 24.4 -0.7 11/02/0611:24:12 26.8 126.4 24.5 -0.8 11/02106 11:24:22 26.9 126.3 24.5 -0.8 11/02106 11:24:32 27.3 126.6 24.7 -0.8 11/02/0611:24:42 27.7 126.7 24.6 -0.9 11/02106 11 :24:52 28.0 127.1 24.4 -0.9 11/02/06 11:25:02 27.7 127.2 24.0 -0.9 11/0210611:25:12 27.6 127.1 23.7 -0.9 11/0210611:25:22 27.2 126.4 23.5 -0.9 11/02/06 11 :25:32 26.9 125.8 23.5 -0.8 11/02/06 11 :25:42 26.2 125.0 23.7 -0.8 11/02/06 11:25:52 25.6 124.3 23.9 -0.7 1 ,02106 11 :26:02 25.4 '\23.8 24.1 -0.8 11/02/06 11:26:12 25.3 123.6 24.2 -0.8 11/02/06 11:26:22 25.0 123.7 24.1 -0.9 11/02/06 11 :26:32 25.5 124.1 23.9 -0.9 11/02/06 11:26:42 25.5 124.7 23.5 -0.7 11/02106 11:26:52 26.0 125.7 23.2 -0.7 11/02/06 11:27:02 26.1 126.6 23.0 -0.7 11102106 11 :27:12 26.5 127.6 22.9 -0.7 11102/06 11 :27:22 26.6 128.4 23.0 -0.7 11/02/06 11 :27:32 26.7 128.9 23.2 -0.8 11/02/06 11:27:42 27.1 129.3 23.2. -0.8 11/02106 11:27:52 27.4 129.4 23.1 -0.7 11/02/06 11 :28:02 28.2 129.4 23.1 -0.8 11/02106 11 :28:12 29.3 129.3 23.1 -0.8 11/02/06 11:28:22 29.8 129.4 23.0 -0.8

Page 4 

# 9911/2/06 Run #2

11/02106 11:28:32 30.2 129.1 22.9 -0.9 11/02/06 11 :28:42 30.5 129.1 22.9 -0.8 11/02/06 11:28:52 30.2 129.0 22.9 -0.8 11/02/06 11:29:02 29.9 128.7 22.8 ..0.9 11/02/06 11 :29:12 29.7 128.3 22.8 -0.9 11/02106 11:29:22 28.9 128.1 22.7 ..0.8 11/02/06 11 :29:32 29.0 127.9 22.9 -0.9 11/02/06 11 :29:42 28.9 128.1 23.1 -0.9 11/02/06 11 :29:52 28.1 128.7 23.2 ...().8 11/02/06 11:30:02 27.7 128.9 23.4 -0.8 11/02/06 11:30:12 27.1 129.0 23.6 -0.8 11 /02/06 11 :30:22 26.5 128.7 23.6 -0.9 11/02/0611:30:32 25.8 128.2 23.4 -0.9 11/02106 11 :30:42 26.1 127.8 23.3 -0.9 11/02/06 11 :30:52 26.2 127.4 23.2 -0.8 11/02/06 11 :31:02 26.3 127.1 23.1 ..0.8 11/02/0611:31:12 25.6 127.1 23.0 ..0.8 11102/06 11:31:22 24.8 126.2 23.6 ..0.8 11/02/06 11:31:32 24.2 125.2 24.2 -0.9 11/02/06 11:31:42 23.6 124.5 24.5 -0.9 11/02/06 11:31 :52 23.5 124.1 24.8 -0.8 11/02106 11:32:02 23.8 124.0 25.3 ..0.8 11/02106 11:32:12 24.3 124.5 25.8 ..0.9 11/02/06 11 :32:22 24.4 125.1 25.5 -1.0 11/02/0611:32:32 25.1 125.6 24.6 -0.9 11/02/06 11:32:42 25.5 126.0 23.8 ..0.9 11/02/06 11 :32:52 25.4 125.7 23.5 -0.9 11/02/06 11:33:02 25.5 125.6 23.4 -0.9 11/02/06 11:33:12 26.1 125.3 23.3 -1.0 11/02/06 11 :33:22 26.3 125.1 23.3 -1.0 11/02/06 11:33:32 26.9 125.2 23.3 -1.1 11/02/06 11 :33:42 27.0 125.4 23.3 -1.1 11102/06 11 :33:52 26.7 125.1 23.1 -0.9 11/02/0611:34:02 26.1 124.7 22.7 -0.9 11/02/0611:34:12 24.7 124.3 22.7 -1.0 11/02/06 11 :34:22 23.5 123.4 23.2 -1.0 11/02/0611:34:32 22.5 122.3 23.7 -1.1 11/02/06 11 :34:42 21.6 121.1 24.2 -1.2 11/02/06 11 :34:52 21.2 120.1 24.6 -1.2 11/02/0611:35:02 21.f. 119.4 24.9 -1.2 11/02/0611:35:12 19.8 119.5 25.4 -1.2 11/02/06 11 :35:22 20.1 119.7 26.1 -1.1 11/02/06 11 :35:32 21.5 120.5 26.6 -1.0 11/02/06 11:35:42 22.4 121.5 25.7 -1.0 11/02/06 11 :35:52 23.3 122.7 24.5 -1.1 11/02/0611:36:02 24.1 123.4 23.8 -1.1 11/02/0611:36:12 25.5 125.2 23.5 -1.2 11/02/06 11:36:22 27.1 126.6 23.3 -1.1 11/02106 11 :36:32 28.9 127.0 23.3 -1.2 11/02/06 11:36:42 30.2 127.4 23.2 -1.1 11/02/06 11 :36:52 31.2 127.9 23.1 -1.2 11/02/06 11:37:02 31.5 128.5 22.8 -1.2 11/02/06 11:37:12 31.8 128.6 22.5 -1.2 11/02/06 11:37:22 32.1 127.9 22.4 -1.2 11/02/06 11:37:32 31.5 126.7 22.4 -1.1 11/02/06 11:37:42 31.4 125.5 22.3 -1.1 11/02/06 11 :37:52 30.4 124.0 22.4 -1.1 11/02/0611:38:02 29.8 122.4 22.4 -1.1 11/02/0611:38:12 29.5 119.0 22.4 -1.1 11/02/06 11:38:22 28.4 114.5 22.6 -1.2 11/02/06 11 :38:32 26.5 109.2 23.0 -1.2 11102/06 11 :38:42 25.5 104.7 23.8 -1.3 11/02/06 11 :38:52 25.3 100.1 24.4 -1.2 11/02/06 11 :39:02 25.4 95.6 24.7 ·1.3 11/02/06 11:39:12 25.5 92.0 24.9 -1.2 11/02/06 11 :39:22 25.7 88.9 25.0 -1.3 11/02/06 11 :39:32 26.0 87.3 24.9 -1.4 11/02/06 11:39:42 26.3 86.0 24.7 -1.4 11/02/06 11 :39:52 26.7 85.4 24.5 -1.1 11/02/06 11 :40:02 26.6 85.5 24.1 -0.9 11/02/0611:40:12 25.6 85.5 23.8 ·0.1 11/02/06 11 :40:22 24.4 84.6 24.2 ·0.2 11/02/06 11 :40:32 23.1 85.0 24.6 0.0 11/02/06 11:40:42 22.6 86.6 25.1 0.0

Page 5 

# 1001112/06 Run #2

11/02/06 11 :40:52 22.3 88.6 26.0 -0.1 11/02106 11 :41:02 22.2 91.4 26.5 -0.1 11/02106 11:41:12 21.8 93.9 27.0 -0.1 11/02106 11:41:22 21.7 95.2 27.7 -0.1 11/02/06 11:41:32 21.7 96.0 28.6 -0.2 11/02/0611:41:42 22.0 95.9 28.7 -0.3 11/02./0611:41:52 22.3 95.1 27.0 -0.1 11/02/0611:42:02 22.6 93.5 25.6 -0.1 11/0210611:42:12 23.7 91.8 24.9 -0.2 11/02/06 11 :42:22 25.1 91.5 24.4 -0.2 11/02/06 11 :42:32 25.7 93.1 24.1 -0.2 11/02106 11 :42:42 26.3 95.1 23.7 -0.1 11/02106 11:42:52 27.3 97.7 23.5 0.0 Stop Run #2 28.25 126.99 22.55 -0.44 11/02/06 11:43:02 27.9 100.5 23.2 0.0 11/02/0611:43:12 27.8 103.8 22.7 -0.1 11/02/06 11:43:22 26.8 105.9 22.6 -0.2 11/02/06 11:43:32 13.6 107.2 23.0 -0.3 11/02/06 11 :43:42 6.3 88.4 21.4 -0.3 11/02106 11:43:52 6.4 51.2 14.9 -0.2 11/02/0611:44:02 6.1 27.1 10.9 -0.4 11/02/06 11:44:12 6.0 14.7 9.0 -0.5 11/02/06 11:44:22 6.0 7.9 7.6 -0.5 11/0210611:44:32 6.0 4.7 6.7 -0.4 11/02/0611:44:42 6.0 2.8 6.4 -0.4 11/02/06 11 :44:52 6.2 1.6 6.3 -0.3 11/02/06 11 :45:02 7.6 7.7 6.5 -0.3 11/02/0611:45:12 7.0 41.6 5.7 -0.2 11/0210611:45:22 6.2 65.2- 4.6 -0.3 11/02/06 11:45:32 5.5 76.6 3.7 -0.3 11/02106 11:45:42 4.9 84.1 3.1 -0.3 11/02/06 11 :45:52 4.4 87.7 2.5 -0.3 11/0210611:46:02 3.9 89.5 2.3 -0.3 11/02/0611:46:12 3.4 91.0 2.1 -0.3 11/02/06 11:46:22 2.7 91.6 1.9 -0.3 11/02106 11:46:32 2.3 92.3 1.7 -0.3 11/02106 11:46:42 2.1 92.1 1.6 -0.4 11/02106 11 :46:52 2.0 93.3·· 1.6 -0.3 11/02/06 11:47:02 1.6 

### 94.5 1.5 

### -0.4 11/02106 11:47:12 1.4 

### 94.4' 1.5 

### -0.3 99.1 ppm CO 11/02/06 11:47:22 1.2 

### 94.4 1.4 

### -0.4 Zero S02 11/02/06 11:47:32 1.2 

### 94.2 1.4 

### -0.5 11/02/06 11 :47:42 1.2 92.2 1.4 -0.4 11/02/06 11 :47:52 1.2 90.6 1.4 -0.4 11/02106 11 :48:02 1.2 82.1 1.3 -0.5 11/02/0611:48:12 1.2 52.4 6.2 -0.6 11/02106 11 :48:22 1.0 25.6 15.3 -0.6 11/02/06 11:48:32 1.0 12.5 20.0 -0.5 11/02/06 11 :48:42 1.0 5.9 22.2 -0.5 11/02106 11:48:52 1.0 3.0 23.3 -0.5 11/02106 11:49:02 1.0 1.4 23.7 -0.5 11/02/06 11 :49:12 1.0 0.7 24.0 -0.5 11/02106 11 :49:22 1.0 0.3 24.1 -0.6 11/02106 11:49:32 1.0 0.2 24.3 -0.6 11/02/0611:49:42 1.0 -0.1 24.4 -0.7 11/02/06 11 :49:52 1.0 -0.2 24.4 -0.7

, 1/02/06 11:50:02 1.0 

### -0.3 

### 24.4 -0.6 11/02/0611:50:12 1.0 

### 0.3 24.4 -0.6 25 ppm NOx 11/02/06 11 :50:22 1.0 

### 0.7 24.5 -0.6 Zero CO 11/02/06 11 :50:32 1.0 

### 0.6 24.5 0.0 11/02106 11 :50:42 1.1 0.5 24.4 0.0 11/02106 11 :50:52 1.2 0.5 24.1 0.0 11/02106 11 :51:02 1.2 0.6 21.1 0.0 11/02/0611:51:12 2.4 0.5 17.9 0.0 11/02/06 11 :51 :22 3.1 0.7 15.1 0.0 11/02/06 11:51:32 2.1 0.9 8.8 0.0 11/02/06 11:51:42 1.0 0.8 4.3 0.0 11/02/06 11:51:52 1.0 0.8 2.4 0.1 11/02/06 11 :52:02 1.0 0.6 1.7 0.6 11/02/0611:52:12 1.0 0.5 1.6 2.0

PageS 

# 10'111/2/06 Run #2

11/02/06 11:52:22 1.0 0.4 1.4 4.0 11/02/06 11 :52:32 1.0 0.3 1.2 6.4 11/02/06 11 :52:42 1.0 0.4 1.1 9.0 11/02/06 11:52:52 1.0 0.3 1.0 11.6 11/02106 11:53:02 0.9 0.3 0.9 14.4 11/02/06 11:53:12 1.0 0.3 0.9 17.2 11/02/06 11:53:22 1.0 0.3 0.8 19.8 11/02/06 11:53:32 1.0 0.3 0.7 22.1 11/02/06 11:53:42 1.0 0.3 0.7 24.3 11/02/06 11:53:52 1.0 0.3 0.6 26.2 11102/06 11:54:02 1.0 0.3 0.6 27.9 11/02/06 11 :54:12 1.0 0.3 0.6 29.6 11102/06 11:54:22 1.0 0.3 0.5 31.2 11/02/06 11 :54:32 1.0 0.3 0.5 32.5 11/02/06 11 :54:42 1.0 0.3 0.5 33.8 11102/06 11:54:52 1.0 0.3 0.4 35.1 11/02/06 11:55:02 1.0 0.3 0.4 36.0 11/02/06 11 :55:12 1.0 0.3 0.4 37.1 11/02/06 11:55:22 1.0 0.3 0.4 38.0 11/02/06 11 :55:32 1.0 0.5 0.4 38.6 11/02/06 11 :55:42 1.0 0.5 0.3 39.0 11/02/06 11:55:52 1.0 0.5 0.4 39.2 11/02/06 11 :56:02 1.0 0.5 0.3 39.5 11/02106 11:56:12 1.0 0.5 0.3 40.1 11/02/06 11:56:22 1.0 0.5 0.3 40.5 11/02/06 11 :56:32 1.1 0.3 0.3 40.6 11/02/06 11 :56:42 1.2 0.3 0.3 41.2 11/02/06 11:56:52 1.1 0.3 0.3 41.6 11/02/06 11:57:02 1.0 0.2 0.3 42.1 11/02106 11:57:12 1.0 0.2 0.3 42.4 11/02/06 11:57:22 1.0 0.2 0.2 

# . 42.7 11/02/06 11:57:32 1.0 0.2 0.2 43.1 11/02/06 11:57:42 1.0 0.3 0.2 43.4 11/02/06 11 :57:52 1.0 0.3 0.2 43.6 11/02/06 11:58:02 1.0 0.3 0.2 43.9 11/02/0611:58:12 1.0 0.3 0.2 44.2 11/02/06 11 :58:22 1.0 0.3 0.2 44.4 11/02/06 11 :58:32 1.0 0.4 0.2 44.7 11/02/06 11 :58:42 1.0 0.4 0.2 44.9 11/02106 11 :58:52 1.0 0.3 0.1 45.2 11/02/06 11:59:02 1.0 0.3 0.2 45.4 11/02/06 11 :59:12 1.0 0.3 0.1 45.5 11/02106 11 :59:22 1.0 0.2 0.1 45.7 11/02106 11 :59:32 1.0 0.2 0.1 45.8 11102106 11 :59:42 1.0 0.2 0.1 45.9 11/02/06 11:59:52 1.0 0.2 0.1 46.0 11/02/06 12:00:02 

### 1.0 0.3 0.1 46.1 11/02/06 12:00:12 

### 1.0 0.3 0.1 46.2 ZeroVOC 11/02/06 12:00:22 

### 1.0 0.3 

### 0.2 46.4 11/02/06 12:00:32 

### 1.0 0.3 

### 0.1 46.4 49.8 ppm 502 11102/06 12:00:42 1.1 0.3 

### 0.1 46.5 Zero NOx 11/02/06 12:00:52 3.3 0.3 

### 0.2 46.6 11/02/06 12:01:02 39.6 0.3 0.2 46.4 11/02106 12:01:12 42.0 0.3 0.1 46.1 11/02/06 12:01:22 42.2 0.3 0.1 45.2 11/02/0612:01:32 

### 42.1 0.3 0.1 42.1 11/02/0612:01:42 

### 41.6 0.3 0.1 37.9 40.8 ppmCH4 11/02/06 12:01 :52 

### 41.5 0.2 0.0 33.6 11/02/06 12:02:02 

### 41.6 0.2 0.0 29.6 11/02/06 12:02:12 38.7 0.3 0.1 25.8

Page 7 

# 10211/2/06 Run #3

Date/Time 

## voc co NOx 502 mm/dd/yy hh:mm:ss ppm ppm ppm ppm 11/02/06 12:09:52 27.5 123.2 20.0 0.2 Stan Run #3 11/02106 12:10:02 26.8 123.4 19.8 0.2 11/02106 12:10:12 26.3 123.4 19.8 0.1 11/02/0612:10:22 25.5 123.4 19.7 0.0 11/02106 12:10:32 25.3 123.4 19.8 0.0 11/02/06 12:10:42 25.4 123.2 19.6 0.1 11/02/06 12:10:52 25.4 122.7 19.6 0.1 11/02/06 12:11:02 25.5 122.5 19.5 0.1 11/0210612:11:12 25.4 122.1 19.5 0.1 11/02/06 12:11:22 25.3 121.5 19.5 0.1 11/02/0612:11:32 24.9 121.1 19.5 0.0 11/02/06 12:11:42 24.9 121.1 19.6 0.0 11/02/06 12:11:52 25.3 120.8 19.6 -0.1 11/02/0612:12:02 25.8 121.0 19.7 -0.2 11/02106 12:12:12 26.2 120.6 19.8 -0.1 11/02/06 12:12:22 26.7 120.6 19.8 -0.1 11/02/06 12:12:32 27.3 113.1 20.0 -0.1 11/02/06 12:12:42 28.2 120.7 20.1 -0.2 11/02/06 12:12:52 29.2 120.8 20.1 -0.3 11/02/06 12:13:02 29.8 120.9 20.1 -0.3 11/02/0612:13:12 30.0 121.3 20.2 -0.2 "\1/02/0612:13:22 29.8 121.9 20.2 -0.1 11/02/06 12:13:32 29.6 122.0 20.3 -0.2 11/02/0612:13:42 29.4 122.5 20.2 -0.2 11/02/06 12:13:52 29.5 122.6 20.3 -0.3 11102/06 12:14:02 29.8 122.7 20.4 -0.2 11/02/06 12:14:12 29.1 122.8 20.5 -0.3 11/02/06 12:14:22 28.8 122.8 20.4 -0.4 11/02/0612:14:32 28.3 122.8 20.6 -0.5 11/02/0612:14:42 28.0 122.8 20.6 -0.5 11/0210612:14:52 27.8 122.5 20.7 -0.3 11/02106 12:15:02 27.6 122.3 20.7 -0.3 11/02/06 12:15:12 27.4 122.2 20.7 -0.3 11/02/06 12:15:22 27.0 122.0 20.7 -0.3 11/02/06 12:15:32 27.0 122.5 20.7 -0.5 11/02106 12:15:42 27.5 122.7 20.7 -0.5 11/02106 12:15:52 27.8 122.8 20.7 -0.5 11/02/06 12:16:02 28.0 123.0 20.7 -0.5 11/02106 12:16:12 28.0 122.9 20.6 -0.5 11/02106 12:16:22 28.0 122.7 20.6 -0.3 11/02/06 12:16:32 28.6 122.5 20.7 -0.3 11/02106 12:16:42 28.8 122.1 20.8 -0.5 11/02106 12:16:52 28.9 121.8 20.9 -0.5 11/02106 12:17:02 29.2 121.4 21.0 -0.5 11/02106 12:17:12 29.5 121.1 21.0 -0.5 11/02106 12:17:22 29.5 121.4 21.0 -0.5 11/02/06 12:17:32 29.1 121.5 20.9 -0.7 11/02/06 12:17:42 28.2 121.9 21.0 -0.7 11/02/06 12:17:52 27.8 122.2 21.0 -0.5 11/02106 12:18:02 28.2 122.3 21.1 -0.5 11/02106 12:18:12 28.9 122.2 21.2 0.0 11/02/06 12:18:22 29.4 122.1 21.3 0.0 11/02106 12:18:32 29.6 122.2 21.2 0.0 11/02/06 12:18:42 29.5 122.4 21.2 0.0 11/02106 12:18:52 30.3 122.4 21.1 0.0 11/02/0612:19:02 30.6 122.6 21.1 0.0 11/02106 12:19:12 30.4 122.9 21.1 0.0 11/02/06 12:19:22 30.7 123.0 21.0 0.0 11/02/06 12:19:32 31.4 122.9 20.9 -0.1 11/02/06 12:19:42 31.6 123.1 20.9 -0.1 11/02/0612:19:52 31.7 123.3 20.9 -0.2 11/02/06 12:20:02 32.0 1232 20.8 -0.1 11/02/06 12:20:12 32.1 123.0 20.8 0.0 11/02/06 12:20:22 32.5 123.3 20.8 0.0 11/02/06 12:20:32 32.4 123.3 20.7 -0.1 11/02106 12:20:42 31.6 123.4 20.7 -0.1 11/02106 12:20:52 30.7 123.4 20.6 0.0 11/0210612:21:02 29.9 123.4 20.7 -0.2 11/0210612:21:12 29.6 123.3 20.6 -0.1 11/02/06 12:21 :22 29.0 123.1 20.5 0.0

\ 

# 103 Page 11112/06 Run #3

11/02/06 12:21:32 28.7 123.0 20.7 0.0 11/02/06 12:21:42 28.4 122.9 20.7 0.0 11/02/0612:21:52 28.0 122.7 20.7 ·0.1 11/02/0612:22:02 27.8 122.4 20.7 -0.1 11/02/06 12:22:12 27.9 121.9 20.7 -0.1 11/02/06 12:22:22 27.9 121.7 20.8 0.0 11/02/06 12:22:32 28.2 121.3 20.9 -0.1 11/02/06 12:22:42 28.6 121.2 21.1 0.0 11/02/06 12:22:52 28.5 121.4 21.3 .0.1 11/02/06 12:23:02 29.3 121.6 21.5 -0.1 11/02/06 12:23:12 29.6 121.6 21.5 -0.1 11/02/06 12:23:22 30.0 121.6 21.6 -0.1 11/02/06 12:23:32 31.2 121.5 21.6 0.0 11/02/06 12:23:42 31.9 121.5 21.6 -0.1 11/02/06 12:23:52 32.4 121.9 21.5 -0.1 11/02/06 12:24:02 32.8 122.0 21.6 -0.1 11/02/06 12:24:12 32.8 122.2 21.6 -0.1 11/02/06 12:24:22 32.8 122.5 21.8 0.0 11/02/06 12:24:32 32.6 122.3 21.9 0.0 11/02/06 12:24:42 31.8 122.7 22.0 -0.1 11/02/06 12:24:52 31.0 123.0 22.0 -0.1 11/02/06 12:25:02 30.0 123.0 22.0 -0.1 11/02/06 12:25:12 28.9 122.7 21.9 -0.1 11/02/06 12:25:22 27.6 122.4 21.8 -0.1 11/02/06 12:25:32 26.6 121.5 22.0 -0.1 11/02/06 12:25:42 26.1 120.7 22.3 -0.2 11/02/06 12:25:52 26.0 119.8 22.4 -0.1 11/02/06 12:26:02 26.0 119.7 22.1 -0.1 11/02/06 12:26:12 25.8 119.9 21.8 -0.1 11/02/06 12:26:22 26.1 120.1 21.7 -0.1 11/02/06 12:26:32 26.4 120.4 21.7 -0.1 11/02/06 12:26:42 26.9 120.3 21.6 -0.1 11/02/06 12:26:52 28.1 120.7 21.6 -0.1 11/02/06 12:27:02 29.8 121.3 21.7 -0.1 11/02/06 12:27:12 30.4 121.8 21.8 

### -0.1 11/02/06 12:27:22 30.4 122.1 21.8 -0.1 11/02/06 12:27:32 31.1 122.2 21.9 -0.2 11/02/06 12:27:42 31.4 122.3 21.9 -0.2 11/02/06 12:27:52 31.1 122.3 22.0 -0.1 11/02/06 12:28:02 30.8 122.2 22.1 -0.1 11/02/06 12:28:12 30.2 121.9 22.2 -0.1 11102/06 12:28:22 29.6 121.4 22.2 -0.1 11/02/06 12:28:32 29.4 120.6 22.3 -0.1 11/02/06 12:28:42 29.2 120.1 22.3 -0.1 11/02/06 12:28:52 29.3 119.4 22.3 -0.1 11/02/06 12:29:02 28.5 119.6 22.2 -0.1 11/02/06 12:29:12 28.0 119.6 22.2 -0.2 11/02/06 12:29:22 27.6 120.1 22.0 ·0.2 11/02/06 12:29:32 27.3 120.4 22.0 ·0.1 11/02/06 12:29:42 27.1 120.6 22.0 -0.2 11/02/06 12:29:52 26.5 120.7 22.0 -0.2 11/02/06 12:30:02 26.1 120.7 22.4 -0.1 11/02/06 12:30:12 25.6 120.5 22.9 0.0 11/02/06 12:30:22 25.0 120.3 23.4 ·0.1 11/02/06 12:30:32 24.9 120.5 23.7 ·0.2 11/02/06 12:30:42 25.9 120.8 23.5 -0.1 11/02/06 12:30:52 27.0 121.1 23.0 ·0.1 11/02/0612:31:02 27.4 121.3 22.5 -0.2 11/02/0612:31:12 28.1 121.4 22.1 ..0.1 11/02/06 12:31 :22 29.7 121.5 21.9 -0.2 11/02/0612:31:32 30.5 121.4 21.8 -0.2 11/02/0612:31:42 30.6 121.9 21.7 -0.1 11/02/06 12:31:52 29.7 121.8 21.9 -0.2 11/02/06 12:32:02 29.3 120.8 22.6 -0.2 11/02/06 12:32:12 28.8 120.3 23.3 -0.3 11/02/0612:32:22 27.1 120.0 23.6 -0.3 11/02/06 12:32:32 26.1 120.0 23.8 -0.2 11/02106 12:32:42 26.2 120.1 23.7 -0.2 11/02/06 12:32:52 26.1 120.3 23.4 -0.1 11/02/0612:33:02 26.0 120.2 23.2 -0.2 11/02/06 12:33:12 25.7 120.1 23.0 -0.3 11/02/06 12:33:22 25.7 120.3 22.8 -0.3 11/02/06 12:33:32 26.0 121.2 22.6 -0.2 11102/06 12:33:42 26.0 121.4 22.6 -0.2

Page 2 

# 10411/2/06 Run #3

11/02/06 12:33:52 25.6 121.6 22.5 -0.2 11/02/06 12:34:02 24.9 121.6 22.5 -0.1 11/02/06 12:34:12 24.6 121.1 22.6 -0.2 11/02/06 12:34:22 24.4 120.6 22.6 -0.2 11/02106 12:34:32 24.1 119.6 22.6 -0.2 11/02106 12:34:42 24.4 119.1 22.8 -0.2 11/02106 12:34:52 24.8 118.7 22.8 -0.1 11/02/06 12:35:02 25.9 118.7 22.8 -0.1 11/02/0612:35:12 27.2 119.3 22.9 -0.1 11/02106 12:35:22 27.7 119.8 22.9 ·0.2 11/02106 12:35:32 27.8 120.1 22.7 ·0.3 11/02106 12:35:42 27.8 120.1 22.6 ·0.3 11/02/0612:35:52 27.6 120.1 22.6 ·0.3 11/02106 12:36:02 27.5 119.8 22.8 -0.2 11/02106 12:36:12 27;0 119.5 23.1 0.0 11/02106 12:36:22 27.1 119.8 23.3 -0.1 11/0210612:36:32 27.7 120.0 23.4 -0.1 11/02/06 12:36:42 27.9 119.9 23.3 -0.2 11/02106 12:36:52 26.2 118.2 23.1 -0.1 11/02/06 12:37:02 24.0 114.3 23.7 -0.2 11/02/06 12:37:12 22.4 108.5 25.5 -0.2 11/02/06 12:37:22 21.2 103.2 26.7 -0.2 11/02/06 12:37:32 20.4 97.8 27.0 -0.3 11/02106 12:37:42 19.8 94.0 27.2 -0.3 11/02106 12:37:52 19.8 91.4 27.5 -0.3 11/02/0612:38:02 19.8 91.1 27.9 -0.3 11/02/06 12:38:12 20.1 93.2 27.5 -0.2 11/02/06 12:38:22 20.6 96.7 26.1 -0.2 11/02/06 12:38:32 20.9 100.3 25.1 -0.2 11/02/06 12:38:42 21.7 103.6 24.5 -0.2 11/02/06 12:38:52. 22.3 105.5 24.2 -0.4 11/02/06 12:39:02 23.0 107.2 23.9 -0.4 11/02/06 12:39:12 24.6 109.3 23.6 -0.4 11/02106 12:39:22 25.9 111.2 23.4 ·0.3 11/02106 12:39:32 26.7 113.0 23.3 -0.4 11/0210612:39:42 26.9 114.8 23.2 -0.4 11/02/06 12:39:52 27.2 116.3 23.4 -0.3 11/02/06 12:40:02 27.9 117.0 23.4 -0.2 11/02/0612:40:12 28.6 117.8 23.3 -0.1 11/02106 12:40:22 ·. 28.1 118.6 23.2 -0.2 11/02/0612:40:32 27.9 119.2 23.4 -0.3 11/02106 12:40:42. 27.6 119.7 23.8 -0.3 1110210612:40:52 27.7 120.1 23.9 -0.3 11/02/0612:41:02 27.6 120.5 23.9 -0.4 11/02/0612:41:12 27.1 121.0 23.5 -0.2 11/02/06 12:41:22 27.1 121.3 23.1 -0.3 11/02/0612:41:32 27.2 121.7 22.9 -0.2 11/02106 12:41:42 26.5 122.4 22.8 -0.3 11/02/06 12:41:52 26.4 122.6 22.8 -0.3 11/02/0612:42:02 24.4 122.6 22.6 -0.1 11/02/0612:42:12 22.5 120.9 23.1 -0.1 11/02/06 12:42:22 21.6 118.1 24.4 0.0 11/02106 12:42:32 20.8 116.4 25.2 -0.1 11/02/06 12:42:42 20.5 116.1 25.7 -0.1 11/02106 12:42:52 20.5 117.0 26.1 -0.2 11/02/0612:43:02 21.1 118.8 26.6 -0.2 11/02/06 12:43:12 22.4 121.3 26.8 -0.1 11/02/06 12:43:22 23.3 123.1 25.5 ·0.1 11/02/06 12:43:32 24.3 124.0 24.4 0.0 11/02/06 12:43:42 25.3 124.4 24.0 -0.1 11/02106 12:43:52 25.9 124.2 23.7 -0.1 11/02106 12 :44:02 26.4 123.8 23.5 -0.1 11/02/0612.:44:12 27.2 123.4 23.2 0.0 11/02/06 12:44:22 28.7 123.0 23.0 -0.1 11/02/06 12:44:32 30.1 122.6 22.9 0.0 11/02/06 12:44:42 30.8 122.1 22.8 -0.1 11/02/0612:44:52 31.0 121.1 22.8 -0.1 11/02/06 12:45:02 29.5 119.7 22.9 -0.1 11/02/06 12:45:12 27.8 118.0 23.0 -0.1 11/02/06 12:45:22 26.8 116.5 23.3 -0.1 11/02/06 12:45:32 26.3 114.7 23.7 0.0 11/02/06 12:45:42 26.2 114.0 24.0 -0.1 11/02106 12:45:52 26.2 113.6 24.0 -0.1 11/02/0612:46:02 26.3 113.6 23.7 0.0 

# 105
Page311/2/06 Run #3

11/0210612:46:12 26.4 113.7 23.4 -0.1 11/02/06 12:46:22 26.4 114.2 23.2 -0.2 11/02/0612:46:32 26.9 114.4 23.2 -0.2 11/02106 12:46:42 27.2 114.3 23.1 -0.1 11/02106 12:46:52 27.3 114.2 23.1 -0.1 11/02106 12:47:02 24.8 113.8 23.1 -0.1 11/02106 12:47:12 23.1 111.5 24.1 -0.1 11/02/0612:47:22 22.0 109.0 25.2 -0.1 11/02/06 12:47:32 21.1 107.6 26.0 -0.2 11/02/06 12:47:42 20.7 106.7 26.3 -0.2 11/02/0612:47:52 20.6 106.4 26.6 -0.1 11/02/06 12:48:02 20.8 106.4 27.1 -0.1 11/02/06 12:48:12 21.6 106.9 26.7 -0.1 11/02/06 12:48:22 22.3 108.1 25.8 

### -0.1 11/02/06 12:48:32 23.1 108.8 25.1 -0.1 11/02/0612:48:42 23.9 108.9 24.6 -0.1 11/02/06 12:48:52 24.8 109.0 24.4 -0.2 11/02/06 12:49:02 25.5 109.2 24.0 -0.2 11/02/06 12:49:12 26.1 109.9 23.9 -0.3 11/02/06 12:49:22 26.5 110.6 23.7 -0.1 11/02/06 12:49:32 27.5 111.0 23.6 -0.1 11/02/06 12:49:42 28.3 111.3 23.5 0.0 11/02/06 12:49:52 29.0 111.4 23.4 -0.1 11/02/06 12 :50:02 29.7 111.5 23.3 -0.1 11/02/06 12:50:12 29.6 111.9 23.1 -0.1 11/02106 12:50:22 29.6 112.0 23.0 -0.1 11102/06 12:50:32 29.6 112.6 22.9 -0.1 11/02/06 12:50:42 29.4 113.1 23.0 -0.1 11/02/06 12 :50:52 29.7 113.6 22.9 -0.1 11/0210612:51:02 29.5 114.2 23.0 -0.1 11/02/0612:51:12 28.6 • 115.2 22.9 0.0 11/02/06 12:51:22 28.1 116.2 22.7 0.0 11/02/06 12:51:32 27.8 117.0 22.7 -0.1 11102/06 12:51 :42 27.1 118.2 22.6 0.0 11/02106 12:51:52 26.2 118.3 22.7 0.0 11/02/06 12:52:02 25.6 117.5 23.1 0.1 11/02/06 12:52:12 24.8 117.0 23.6 0.0 11/02/06 12:52:22 24.7 117.4 23.8 -0.1 11/02/06 12:52:32 25.2 117.9 23.9 

### -0.1 11/02106 12:52:42 25.4 118.2 23.7 -0.1 11/02/0612:52:52 25.6 118.3 23.4 -0.1 11/02/06 12:53:02 26.2 118.5 23.1 -0.1 11/02106 12:53:12 26.6 118.9 22.9 -0.1 11/02/06 12:53:22 25.1 119.0 22.8 -0.1 11/02/06 12:53:32 24.3 117.9 23.4 -0.1 11/02/06 12:53:42 24.1 116.6 24.4 0.0 11/02106 12:53:52 24.1 116.0 25.0 0.0 11/02/06 12:54:02 24.3 116.8 25.4 -0.1 11/02/06 12:54:12 24.4 118.2 25.4 0.0 11/02106 12:54:22 24.9 119.4 25.0 0.0 11/02106 12:54:32 25.7 120.6 24.5 0.0 11/02/06 12:54:42 26.6 121.3 23.9 -0.1 11/02/06 12:54:52 27.6 121.7 23.5 -0.1 11/02106 12:55:02 28.1 122.2 23.2 -0.2 11/02/06 12:55:12 28.7 122.4 23.1 -0.2 11/02/06 12:55:22 29.0 122.0 22.9 -0.2 11102106 12:55:32 27.0 121.4 22.9 -0.2 11/02/06 12:55:42 25.7 119.1 23.4 -0.2 11/0210612:55:52 24.6 116.4 24.1 -0.1 11/02/0612:56:02 24.0 115.5 24.5 0.0 11/02/06 12:56:12 23.6 115.5 24.7 -0.1 11/02/06 12:56:22 24.0 116.3 25.2 -0.1 11/02/06 12:56:32 24.6 117.8 25.5 -0.1 11/02/06 12:56:42 25.4 119.8 24.8 ·0.2 11/02106 12:56:52 26.0 

### 121.3 24.0 -0.2 11102/06 12:57:02 26.2 121.9 23.4 -0.1 11/02/06 12:57:12 26.6 122.2 22.9 -0.1 11/02/06 12:57:22 27.5 122.5 22.7 0.0 11/02/06 12:57:32 27.8 122.7 22.6 0.0 11/02/06 12:57:42 27.2 122.9 22.5 0.0 11/02/06 12:57:52 26.9 122.9 22.4 0.0 11/02/06 12:58:02 26.4 122.5 22.4 -o.1 11/02/06 12:58:12 26.0 122.1 22.4 -0.1 11/02/06 12:58:22 25.7 122.2 22.5 0.0 

# 106 Page41112/06 Run #3

11/02/06 12:58:32 25.7 122.3 22.6 0.0 11/02/06 12:58:42 26.1 122.4 22.6 0.0 11/02/06 12:58:52 26.2 122.4 22.6 0.0 11/02/06 12:59:02 27.0 122.4 22.6 0.0 11/02/06 12:59:12 27.7 122.5 22.8 0.0 11/02106 12:59:22 27.7 122.4 22.7 0.0 11/02106 12:59:32 28.1 121.8 22.8 0.1 11/02/0612:59:42 28.2 121.1 23.1 0.1 11/02/06 12:59:52 28.2 120.8 23.2 0.0 11/02106 13:00:02 28.4 120.5 23.2 0.0 11/02106 13:00:12 28.7 120.9 23.2 ·0.1 11/0210613:00:22 28.5 120.7 23.1 ·0.1 11/02106 13:00:32 28.0 120.7 22.9 0.1 11/02/06 13:00:42 27.7 120.4 22.8 0.1 11/02/06 13:00:52 27.6 119.8 22.7 0.0 11/02/0613:01:02 27.2 119.3 22.7 0.0 11/0210613:01:12 26.5 118.6 22.7 0.0 11/02/06 13:01 :22 25.0 118.1 22.7 0.0 11/02/06 13:01 :32 23.9 117.6 22.8 0.0 11/02/06 13:01 :42 23.0 117.2 23.4 0.0 11/02/06 13:01:52 22.6 117.4 23.8 0.0 11/02/06 13:02:02 22.8 118.1 24.1 0.0 11/02/06 13:02:12 23.5 118.9 23.9 0.0 11/02/06 13:02:22 24.4 119.6 23.5 0.1 11/02/06 13:02:32 25.6 119.8 23.2 0.0 11/02/0613:02:42 27.0 119.8 23.1 0.0 11/02/06 13:02:52 27.9 120.2 22.9 0.1 11/02106 13:03:02 28.6 120.5 22.8 0.0 11/02/06 13:03:12 29.2 120.4 22.9 0.0 11/02106 13:03:22 27.7 120.0 22.9 0.0 11/02106 13:03:32 26.4 118.8 • 23.1 0.0 11/02/06 13:03:42 26.1 117.8 23.9 0.0 11/02106 13:03:52 25.6 117.1 24.5 0.0 11/02106 13:04:02 25.5 117.2 25.1 0.0 11/02/06 13:04:12 25.4 117.5 25.6 ·0.1 11/02/06 13:04:22 26.2 118.0 25.4 0.0 11/02/06 13:04:32 26.7 118.5 24.6 0.0 11102/06 13:04:42 26.6 118.7 24.0 0.0 11/02/06 13:04:52 26.2 119.0 23.5 0.0 11/02/06 13:05:02 25.8 119.4 23.4 0.0 11/02/06 13:05:12 25.3 120.1 23.2 0.0 11/02106 13:05:22 24.9 120.6 23.2 0.1 11/02/06 13:05:32 23.8 121.2 23.2 0.0 11/02/06 13:05:42 22.7 121.5 23.2 0.0 11/02/06 13:05:52 22.1 120.8 23.6 0.0 11/02/06 13:06:02 21.5 120.2 24.2 0.0 11/02/06 13:06:12 22.3 119.7 24.7 0.0 11/02106 13:06:22 23.2 120.1 25.0 0.1 11/0210613:06:32 24.2 120.6 24.8 0.1 11/02/0613:06:42 25.4 120.7 24.5 0.0 11/02/06 13:06:52 26.2 121.2 24.2 0.0 11/02106 13:07:02 27.5 121.8 23.7 0.0 11/02/06 13:07:12 28.5 122.2 23.3 0.1 11/02/06 13:07:22 29.6 122.2 23.2 0.1 11/02/06 13:07:32 30.8 121.8 23.0 0.0 11/02/06 13:07:42 32.0 121.7 22.9 0.0 11/02/0613:07:52 32.9 121.4 22.9 0.0 11/02/06 13:08:02 32.3 121.3 22.8 0.0 11/02/0613:08:12 31.4 121.3 22.7 0.1 11/02/0613:08:22 30.1 121.2 22.7 0.0 11/02/06 13:08:32 29.3 121.8 22.7 0.0 11/02/06 13:08:42 28.4 122.4 22.7 0.0 11/02/06 13:08:52 27.7 122.8 22.9 0.1 11/02/06 13:09:02 26.9 122.8 23.1 0.1 11/02/06 13:09:12 26.2 122.6 23.1 0.1 11/02/06 13:09:22 26.0 122.3 23.2 0.1 11/0210613:09:32 25.5 121.4 23.1 0.1 11/02/06 13:09:42 25.0 120.9 23.1 0.1 11/02/06 13:09:52 24.7 120.5 23.1 0.0 11/02/0613:10:02 24.7 120.5 23.0 0.0 11/02/06 13:10:12 24.8 120.7 23.0 0.0 11/02/06 13:10:22 24.7 120.8 23.0 0.0 11/02/06 13:10:32 24.7 120.5 23.1 0.0 11/02/06 13:10:42 24.8 120.4 23.4 0.1 

# 107 Page 51112/06 Run #3

11/02/0613:10:52 25.6 120.8 23.6 0.1 11/02/0613:11:02 26.7 121.3 23.6 0.1 11/02106 13:11:12 27.3 121.7 23.4 0.1 11/02/06 13:11:22 27.9 121.3 23.1 0.1 11/0210613:11:32 29.0 120.1 23.1 0.0 11/0210613:11:42 29.7 119.2 23.0 0.1 11/0210613:11:52 30.0 118.3 23.0 0.0 11/02106 13:12:02 29.5 117.3 23.0 0.1 11/02/06 13:12:12 25.5 116.2 22.9 0.1 11/02/06 13:12:22 22.2 112.0 23.2 0.1 11/02/0613:12:32 20.7 106.8 23.7 0.1 11/02/0613:12:42 20.1 104.4 24.3 0.1 11/02/06 13:12:52 19.9 103.7 25.0 

### 0.1 Stop Run #3 26.88 118.98 22.77**~0.11** 11/02/0613:13:02 19.0 104.5 25.9 0.1 11/02/0613:13:12 18.6 105.4 27.0 0.0 11/02/0613:13:22 19.3 107.2 28.8**~.1** 11/02/06 13:13:32 7.7 107.9 29.0 -0.1 11/02/06 13:13:42 5.7 76.7 22.9 0.0 11/02106 13:13:52 6.0 37.9 13.7 0.0 11/0210613:14:02 5.7 18.1 9.1 0.0 11/0210613:14:12 5.5 9.6 7.2 0.0 11/0210613:14:22 5.2 5.6 6.4 0.0 11/02/06 13:14:32 5.1 3.3 5.8 0.1 11/02/06 13:14:42 5.3 4.1 5.5 0.0 11/02/06 13:14:52 4.9 33.4 5.1 0.0 11/02106 13:15:02 4.0 62.7 4.7 0.1 11/02106 13:15:12 3.5 77.0 4.1 

### 0.0 11/02/0613:15:22 3.0 84.4 3.5 • 0.1 11/02106 13:15:32 2.4 88.0 3.2' 0.1 11/02/06 13:15:42 1.7 89.5 2.9 0.0 11/0210613:15:52 1.4 90.5 2.7**~0.1** 11/0210613:16:02 1.2 90.8 2.5 0.0 1110210613:16:12 1.0 91.1 2.3 0.0 11/02106 13:16:22 1.0 91.1 2.2 0.0 11/02/06 13:16:32 1.0 91.3 2.1 0.0 11/02/06 13:16:42 1.0 91.4 2.0 0.0 11/02/0613:16:52 0.9 91.7 1.9
. 0.0 11/0210613:17:02 0.7 91.8 1.9 0.0 11/02106 13:17:12 0.7 

### 91.7 1.8 

# ·o.o 11/02/0613:17:22 0.7 

### 91.8 1.8 

### 0.0 99.1 ppm CO 11/02/06 13:17:32 0.8 

### 92.0 1.7 

### -0.1 Zero S02 11/02106 13:17:42 0.9 

### 92.0 1.6 

### -0.1 11/0210613:17:52 1.1 86.9 1.6 0.0 11/0210613:18:02 0.9 70.1 2.2 0.0 11/02/06 13:18:12 0.8 37.1 10.8 0.0 11/0210613:18:22 0.8 17.2 18.5 0.0 11/02106 13:18:32 0.8 8.2 22.0 0.0 11/02/0613:18:42 0.8 4.3 23.4 0.0 11/02/06 13:18:52 0.8 2.2 24.0**~0.1** 11/02/06 13:19:02 0.8 1.1 24.4 -0.2 11/02/06 13:19:12 0.8 0.5 24.6 -0.1 11/02/0613:19:22 0.8 0.3 24.7 0.0 11/02106 13:19:32 0.8 0.3 24.8 0.0 11/02/06 13:19:42 0.8 0.1 24.8 0.0 11/02106 13:19:52 0.8 

### -0.2 24.9 0.0 11/02/06 13:20:02 0.8 

### -0.3 24.9 -0.1 25 ppm NOx 11/02/0613:20:12 0.8 

### -0.4 24.9 0.0 Zero CO 11/02/06 13:20:22 0.9 

### -0.5 25.0 0.0 11/02106 13:20:32 1.1**~.4** 24.2 0.0 11/02106 13:20:42 1.3**~.5** 20.9 0.0 11/02/06 13:20:52 2.6 ·0.7 18.3 0.0 11102/06 13:21 :02 2.9**~.5** 13.5 0.0 11/02/0613:21:12 1.6 -0.4 6.7 0.0 11/02/06 13:21:22 0.9 ·0.4 3.7 0.0 11/02/06 13:21:32 0.8 -0.8 2.3 0.1 11102/06 13:21:42 0.8 -1.0 1.8 1.0 11/02/06 13:21:52 0.7 ·1.3 1.6 2.6 11/02/06 13:22:02 0.8 -1.0 1.7 4.6 11/02106 13:22:12 0.8 ·0.8 1.6 6.9

Page 6 

# 10811/2/06 Run #3

11/02/06 13:22:22 0.8 -0.9 1.4 9.4 11/02/06 13:22:32 0.8 -0.5 1.3 11.9 11/02/06 13:22:42 0.8 -0.7 1.2 14.4 11/02/06 13:22:52 0.8 -0.7 1.1 16.8 11/02106 13:23:02 0.8 -0.7 1.0 19.0 11/02/06 13:23:12 0.8 -0.7 0.9 21.3 11/02/06 13:23:22 0.8 -0.6 0.9 23.2 11/02/06 13:23:32 0.8 -1.0 0.8 25.0 11/02/06 13:23:42 0.8 -1.0 0.8 26.8 11/02/06 13:23:52 0.8 -1.1 0.8 28.1 11/02/06 13:24:02 0.6 -1.0 0.8 29.2 11/02/06 13:24:12 0.4 -1.1 0.7 30.3 11/02106 13:24:22 0.5 -1.0 0.7 31.2 11/02/06 13:24:32 0.7 -0.9 0.7 32.0 11/02/06 13:24:42 0.8 -1.0 0.7 32.9 11/02106 13:24:52 0.8 -1.0 0.6 33.7 11/02106 13:25:02 0.5 -0.8 0.7 34.6 11/02/06 13:25:12 0.5 -0.9 0.6 35.4 11/02/06 13:25:22 0.5 -0.9 0.6 36.1 11/02/06 13:25:32 0.5 -0.9 0.6 36.9 11/02/06 13:25:42 0.8 -0.7 0.5 37.5 11/02106 13:25:52 0.8 -0.9 0.5 38.2 11/02/06 13:26:02 0.7 -0.8 0.5 38.7 11/02106 13:26:12 0.8 -1.0 0.5 39.1 11/02/06 13:26:22 0.8 -0.9 0.5 39.5 11/0210613:26:32 0.8 -1.0 0.5 40.0 11/02/06 13:26:42 0.8 

### -1.1 0.5 40.7 11/02/06 13:26:52 0.8 

### -1.1 0.4 41.3 11/02/06 13:27:02 0.8 -1.1 0.4 41.7 11/02106 13:27:12 0.8 -1.1 0.4 42.1 11/02/06 13:27:22 0.8 -1.2 0.4 42.3 11/02/06 13:27:32 0.8 -1.3 0.4 42.5 11/02/06 13:27:42 0.8 -1.1 0.4 42.9 11/02/06 13:27:52 0.8 -0.9 0.4 43.2 11/02/06 13:28:02 0.8 -0.9 0.4 43.4 11/02/06 13:28:12 0.8 -1.0 0.3 43.7 11/02/06 13:28:22 0.8 -0.8 0.3 43.9 11/02/0613:28:32 0.8 -0.9 0.3 44.2 11/02/06 13:28:42 0.8 -1.0 0.4 44.6 11/02106 13:28:52 0.8 -0.9 0.4 44.9 11/02106 13:29:02 0.8 -0.8 0.3 45.0 11/02/0613:29:12 0.8 -0.9 0.3 45.2 11/02/0613:29:22 0.8 -D.9 0.3 45.4 11/02/06 13:29:32 

### 0.8 -0.9 0.3 45.5 11/02/0613:29:42 

### 0.8 -0.7 0.3 45.5 ZeroVOC 11/02/06 13:29:52 

### 0.8 -0.7 0.3 45.6 11/02106 13:30:02 

### 0.8 -0.7 0.3 45.7 11/0210613:30:12 0.8 -0.6 

### 0.3 45.9 11/02/06 13:30:22 1.0 -0.7 

### 0.3 45.9 49.8 ppm 502 11/0210613:30:32 26.3 -o.8 

### 0.2 45.8 Zero NOx 11/02/06 13:30:42 40.3 -o.s 

### 0.2 45.9 11/02/0613:30:52 40.4 -0.8 0.3 46.1 11/02/06 13:31:02 

### 40.5 -0.9 0.2 44.2 11/0210613:31:12 

### 40.4 -1.1 0.2 40.5 40.8 ppm CH4 11/02/06 13:31:22 

### 40.5 -0.9 0.2 36.1 11/02/0613:31:32 

### 40.6 -0.8 0.2 31.9 11102/0613:31:42 33.8 -0.8 0.2 28.3



# 109
Page 7

### .

## ~ I

# I



# Appen'dix C · ·.



# . .

·. ,' 

# .. , .. ,;

## FILTER ANALITICAL DATA

Company: Dal-ltalla, Muskogee, OK Date: 10/30/06 Location: Glaze Line Baghouse (EPN 41) Run 

## 1 Filter ID Number Date of Weighing Time Gross Filter Wt. Date of Weighing Time Gross Filter Wt. Ave. Gross Filter Wt. Date of Weighing Time Filter Tare Wt. Date of Weighing Time Filter Tare Wt. Ave. Filter Tare Wt. Wt. of PM on Filter (grams) Total Weight of Particulate (mg)

## \azG.\WH:n~Hn**jH1l1j~~uat.o~1** 

# ::::::m=:**1HlH11H~~/afQ$1 H1Hl~i~S1P:M1** 

## @HH1PUa9:5.S~ 

## 0.3655 :=:=:=:::.t:;;r;a1na=**:::;:::::~:yJ.~/~~;**

## HlH12l1~1P:Ml**1WiWin~®4a1**

## 1~m~~w1oroa1**lH11lS.~~~m~M~**

## HH~HP~4!4~ 

## 0.3645 0.0010 1.0 Run 2

## :~~Gfl~;f:1~1~lj\l~~**~~jH:J~f:~ip$.j**

## UfU1:i:W.~HAMi**?HHHQi~P.~tti**

## ,WHHi~1,~6i~6.1**:;Hn~r~a$H?:t.W 'i)iHHO;aa~i~i**  

## 0.3612

0.3610 0.0001 0.1 Run 3

## ·~~tt~:nnnun**:nn~n1l11$1Q.~:**

# ·l::::ili~::i HiWn1116100:i**HU~~~!4HP:MH 1\lHH~Hl$.~1**  

## 0.3633

## H~)~Q/.~1®.**YH2~20HRIYf** 

# HHHHO:Jaazt**~~iljbi:~PI:®~ HHH~H21:1ANf** **P1HHH10~a~9l:** 

## 0.3627 0.0006 0.6



# 140

### PARTICULATE ANALYTICAL DATA FORM 

## Company: Dal-ltalia, Muskogee, OK 

## Date: 10/30/06 Location: Glaze Line Baghouse (EPN 

## 41) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) 

# = Ca*Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight' Weight of Particulate in Rinse (mg). 

## j1{%LldJ1$$.f

# l:l:l~l~~~~f~~~ 0.0001

# :l;l:lll:l~;~;r:.~l**nnnl;~;tctJ2llail!**

# ·':'·\lj~!~i!!**~UHHl~o¥:51:061 ~=~H~Y1:!~0l~tVf** **~~UHlllO:i26~1.l** 

# l1 ll 

# !lHlll 

# b¥:$Xd6l

# l::;:mi~~~~~: 110.2739

0.0001 110.2647 9.01 Run 

### 2**~nnnnn~ot?:sshH** 

# lHHot(}di2tr3jl**nnHH~n:HHlit4~l** 

## 0.0001**~HHHt1i6i:Oe1 nnH:n~siAA~Ml** **n~nnJQ~ls~r.al**

## HHH(Ellt~i.<16.l**~;nlHn1a~07:l~Ml ~iHHJJ(}3;S~7:8~** 

### H?Hlltoi6i~6.l**:1n1~Hf1!2tANH** 

## .HnJJ)3iSZ01i 

# HHH1tl1:6i:{)e l**~nnnnl~~341P-Nt Y;llfG.3~S2QS.~**  

## 103.8278

0.0001 103.8206 7.06

ACETONE BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va*Pa) 

## = mg/g

# !iii\,··!:~~~~ HlHHH98.16l460: 

# nHHl:tiV:$/061

# ;;w~:~;:m~:.~: 98.646**~ H~** **1Hll~~~/.S1:0.6l**

# 1m::m;~~~:.~;:**~:l:~:l:l;~~g(~~~** /1l!H;**Sa.6~$11** 

## 98.64575

0.00025 0.00127
Note: In no case should a blank residue greater than 

## 0.01 mg/g or 

## 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 3

### Hl=lUUHd1t:$~f 

# ;H\tb.th27:stt**n~Hl~=WH=~=n~~~~:** 

## 0.0001 

# HHHI1t.el.m6l**lHl\l~l$l;MYf lliH1;~tj~j[;j~$.~**  

# HHlHf11.61:b6.1**Hnn~n~ta$H?:tW H:H10~ltt7~~** 

## ~HHH1c~l:b5:**n:<nl1~3~~tw nu10011:6s.~t::** 

## <tllllot.e~o6.:**l1~1Hl3~3~1P.t~f l<H~02J~53:**  

## 102.1725

0.0001 102.1654 7.01

## PARTICULATE ANALYTICAL DATA FORM

. Company: Dal-ltalia, Muskogee, OK Date: 10/30/06 Location: Glaze Line Baghouse (EPN 41) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (J/a) Average Beaker Tare Weight Weight of Particulate in Rinse (mg) 

# ;Hu;nHH1111ll$6i :Hifl2ls4itslot**:;~nnnn=H~HH~~S3i** 

### 0.0001 

# nHHlWIWi6i:G6l**HHniiHS~(l~1HMW iHHHWS.O:..:O:Of?~~** 

# lll:l:l!ll~~;.ri:**i~iii1~iH~~~!QS$il**

## l1HlHiO:l:t~Y:06i**HiliiUH?::i~ttU~Ml il~nnlH95.10059i** **=======~;oiid~a6=**

# '!::~.!::!~~§~~ 96.0062

0.0001 96.0058 0.35 Run 

### 2 

# +U1:1nHntaei**Hlin2Hi4if!~o1:i iHH~:n:HH~n~i~Si**  

### 0.0000 

# nHHHtli:61f()6l

# lllll:l~il1~~~**lHHHn~tl~i:6ic61**

## ~;~nnn:z~iO;P.~t**HHil~ili®tP~$$1 j)Jb/.~1&1061** **:::::!:::::Y:i:i=?==~M·: :·:·:i.:!•:I:,:..L:~·1'\.'**  0**:nnntosro~3~i**

## UHH1m~10:/<l6l**HiH~iiSip&iP.Mi ii~** **i~~ilt05l0i1i.30** 

### i
105.0435

0.0000 105.0431 0.35


## METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va«·Pa) = g/g

# llllil:l:l~[~~~~**~;!HH;ns~~!AMl iHHilit~~Jtill541** 

### HHHHitf~6xo6i**~n:p;iii~l~().;fW1~ nnnn1m~~W5.4l**  

### 103.1154

### HH1!ll10(:~0Y:~6!

## \!l!HH?:i;30!~Nl**UliHllS~l~lt53l liiUi~lOJ101:0:6l** 

# ::;l::::~~~~li~l 103.1153 1E·04 2.941E·07 Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 3 

## ;:lililililjliljlitl$&**HHH2t9~1£;bt :nnnnnn=Hiill2~::**  

### 0.0000

### HIH111.~1b.5: 

## HHHiliiS:.1>2iAMi**iHHlliQ~i~51:0:i**

### lHHH~H¥.6~a6U**iHiiiH2~~HlliP:M1 iHi;ttO!ai~69::**  

# YHtoi:iPib&**iliilliin1~tSlAM** 

## UlUUJ2lili56l 

# unnrol:io1.o&**}jn!ii3~$Zii?:M nn==J02A~559.**  

### 102.4570

0.0000 102.4561 0.85



# 14.2

## PARTICULATE ANALYTICAL DATA FORM Company: Dal·ltalia, Muskogee, OK Date: 

### 10/30/06 Location: Glaze Line Baghouse (EPN 

### 41) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) 

## = Ca*Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate in Rinse (mg)**~~nHlll:HH1nHlill**

# lllllllllll!llll~~~i 0.0003

# :l:l:l:::l~f~~r~~**lnH;HeS..~S5.3l**

# l!l!l:l:l:~~~rll UlH<99.ASG1i

# ::::·.l·.'~::ri:.**==l=l=====1ti~9.la6=**

# ;lili1j1j~~i521~~M1**HHHnS.~** 

## .. 461:5l 99.4863

0.0003 99.4675 1S.50 Run 2**\lll\U~nnllnllllmtl** 

# iHHHHHHilEh:06l**l;ljljljljljl;lll:i~{)IiJj** 

### 0.0003 

# :HHHHtii&J<>al**[UnllH4l~29.iflNf YH~HllQ3tBSUH** 

### !HHHntti;Y:~i~sl 

## :HlU!S:Ba1AM.i**Hln;t()3~$Biltl**

### H!HUt61:~i.(}6\ 

## nn;l;lH7:H)3lAMl lilUlll1().3lS$.9llii

## WiHHH~W:9=mai 

## UHHHigi50iP.til!l :l;>lll03l8$8Sl 103.8811

0.0003 103.8590 21.80



## H20 BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing · Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca=**Ma/(Va·~Pa)** 

## = g/g

# :lllllll!l~li~~=**i!HHHil.8i~1H~M; lHnHllO~l6~00:** 

## illil!ll!l1lE~6.1:d6;**lHnlll~i~SH~~t =innll10~~648.~l**  

### 106.64895**iiiiiiii!ilil¥.91:~61 nHnnnr?:!2~~AtW** 

### h%~lD~t64S9l 

## :unHHllti91:D.6l**liHHHlH3:~~l~Ml** 

## :=;1/t**0&.~6:485!** 

### 106.6487 0.00025 1E·06**No~e:** In no case should a blank residue greater than 

### 0.01 mg/g or 

### 0.001% of the blank we1 ht be subtracted from the sam le wei ht. Run 3


# HHHHHH11E!d&.i UlllllnHHlH\lSQct 0.0003

# ·ll:::1:1:m~:ri~l lllHHlbOl0.6$Zl

# lllllllll~~~;:~:**:nu~OOH)6S4il**

## lHUHip/.91-d~\**;;;l;(n:n()~l~rw HiHii~OOi~62&:** 

## HiHHi~lsKm&.l

## ~~~y~n~j9a~;F~: :::::::1(!aJ.:0.62a: 100.0683

0.0003 100.0625 5.55



## · .. 

# 143

## FILTER ANALITICAL DATA

Company: Dal-ltalia, Muskogee, OK Date: 

## 10/30/06 Location: Press Baghouse (EPN 40) 

## Run 1 Filter ID Number Date of Weighing Time Gross Filter Wt. Date of Weighing Time Gross Filter Wt. Ave. Gross Filter Wt. Date of Weighing Time Filter Tare Wt. Date of Weighing Time Filter Tare Wt. Ave. Filter Tare Wt.

. Wt. of PM on Filter (grams) Total Weight of Particulate (mg)

## i4.~s.n1nnnw1~1**:~nHH~~i.$roe1** 

# HUU7:it:$lAMl**l\HllHJ)~7.;1 $~** 

## Hn~!i~Jat.Qsl**nHHZl~$~P:Ml**

## 1HHHHP~arf7:l 

## 0.3718

## ~1HlH~~~wet.o6~ 

# lHHlZ!63.ll?:Ml**HHillHO~~tft**

## [i~~~~iohoroai**HHHS.~4Pl~M~ llHHHl~t~7tt**  

## 0.3711 0.0007 0.7 

## Run 

## 2**·4$~~~lj)llllll)lil)**

## /%t~t:$ioal**>W~i~it?.i~t\f nHHn~;~a$e,l** 

## t~lm~Hni1Y:6Joal**~HH121~$4:lP:Ml :H:HHO;~aaz;**  

## 0.3657

0.3648 0.0009 0.9 

## Run 3

## ~7~i!H)T/ 

# Hn(1:1ml®·**UiH!r:P~rtHANf** 

# HHH**(¥:HJ.$~3:**

## ~HUl1lrtJ~I:d~:**l11111~~$.311P:M1f HHH1J)J$a<)~l=**  

## 0.3803

## ~~Hdltit.~!:OO.l~**H1Hi2~~4HP:Nf HWiUHO~~~t~Sn** 

## nnJot1P~oo::**lHW~Hl4tA.MF fHHJta!l9$~'**  

## 0.3794 0.0008 0.8

### PARTICULATE ANALYTICAL DATA F'ORM Company: Dal·ltalia, Muskogee, OK Date: 10/30/06 Location: Press Baghouse (EPN 40) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate in Rinse (mg)**:u::j:HHili~S.tl u=:~:N:\:;:ii:~~i** **:.:::\fi.(\AI~:,:(:Y.T:•**

## llHlHll\l!l!iHllj~sz: 0.0002

# ;::lll~lll~T~~~~~ lHHH lH 

# !i{ijioaa ll

# lll!~;::llM~f;r~~**!lC~nl~~JGa~;** 

# HllHHlot:Eit:o6.**~H1HH1:illl~l.~#t ~lHHH196ll6J:~~~** 

## \llllnU!OI-~~0.61**;nnn~HrBii1l5W~.M: 1~HilH1~9.6!J61:4.tl!**  

### 96.6831

0.0002 96.6741 8.81 Run 2 

## YHUil(H?:$1$\jH

# lmm~m~~~[~~~ 0.0001 

# llHHlHltiii&J{)sl**n;HHUS.ill~lm.l** 

## 1il1lli11i0:7:tS(}i$1

# ~llllllll;~~&f:.~l**::H~lli().?.t~O.l$1** 

# 1;t1;;;;;**wor6li<l~l ;;r~l~li~1:HUl:AMl** **;nn?liCf1.~~9.2S;** 

# HH\iHlO.I:§{{}Sl**\1Hi=lgi4~l~Ml H>li0.7l29.2:6~**  

### 10i.3013

0.0001 107.2927 8.45


## ACETONE BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va*Pa) 

# = mg/g

# ll:l;l;/:liltij~~~l**iiliiliHlS!tll!l~Ml ~n=HH~~98J6400i**  

# !;HHlHXW6.i0.6i**~nnn~~i~t$§HP:Mi ~;H:J;iH~98J54.:Sf**  

### 98.646 

# i 11

# ii.'!'.il!i**nnHHHl0¥:91:GJ.6~**

# lllW:lll~~~~~l 98.64575

0.00025 0.00127 Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 3**n:H~H~djf:S$~~:**

# ;;l:m:~~~~~:~: 0.0002

# llllllll:l:.r~~l**1~1HHtt(l$lZ5~Z~**

# l;lllil:lit~r:.~:**~~wn~og;zs~~t**

### \l\lll\tla~V.el.o~t**>~Y~V.~i2~~tW H~U10~il41:lL**  

# HHHlliPV.eKo6:**/1nH3~4~1~Ml ~H1~~1l09.!241Cr**  

### 103.2543

0.0002 103.2471 7.06



# 145

### PARTICULATE ANALYTICAL DATA FORM Company: Dal-ltalia, Muskogee, OK Date: 10/30/06 Location: Press Baghouse (EPN 40) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Yaw) Residue in Rinse (Wa) = Ca*Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker**~are** 

### Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate in 'Rinse (mg)

### wnnn~wnn;ru;$1

### nm~2~9.4WeHO.i**l~nHHUHiHHHt~~l** 0.0000 

# n:HlHili t6.X061 nnnn=rstoSrAMl**:rrrrrr:1I?il1.!1:1~1**

# !'!!i'!!~W!f~!**:!!':!!~~~;:~ THHar~/1o~®1** **~lHlHH13i41:llP:Ml Y?t11~l1.r1:0.21**  

### 112.7709

0.0000 112.7704 0.50 Run 

### 2**HH1~UlHi1illi11U36l ~** **~** 

# 1**~;** 

# 121914**tilE~1 ~** **rUnil~lllilil;Hl~;~it** 

### 0.0000 

# nT:CU:t:6V661**H<YBi35l~Ml nr~lt~s;asial** 

### UHHHVtili:~JoS.l**:lllHi{a~il4lPMr ~%UU~:3lS$lS1** 

# !!·,!!!ill~,:~~~ 1Hljml:16i6S1**r=rHln~gi4~rP.M.r l~PlG3~95~5.l**  

### 103.9519

0.0000 103.9516 0.25



### METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va*Pa) = g/g

### :~HHHlH1HHW~ool**1H~~~iHlll~¥:$l:Q6l t:HHllS!l4Ql~N11** **~n~Hi03.Jl1541**

## HHHlHtt/.6~®1**~~ilH!lH3ig01llmil lHllHlfPg:~~l~6.4l**  

### 103.1154**il~HH~iO:.HD.XQ6l**

### H=lH1HH7~~Q1~till 

## i[1}1;tS3dlt5.Sl**lH1HialO/H!/:G.6~ rrliW~rs:ssn~tvt** 

### =rn;;:riog~lt~r 103.1153 lE-04 2.941E-07 Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 3

### ;u;n>;~;t~&:~**:lH2~W.1Eibt** 

## ;:;n;r:rH:l;r:il25\[ 0.0000 

# r)lHt1/61.b.ff**~:YY8i36.~A~ )UH:91::75$~:** 

### HH1!~Ha111.61:d&.:**lHlH3t:ts~P:tW :r;Y:;9~i7:5S$l**  

# \HHi.oi1P.I:b6H**lHlUH7:~01~tW rnnnH9ZJ7:5Stv.~** 

## nwnroi:1oV.o&.~**HhHl3~14$r~rw rrHn:~rtrsaa'**  

### 97.7589

0.0000 97.7584 0.45



# 146

## PARTICULATE ANALYTICAL DATA FORM Company: Dal·ltalia, Muskogee, 

### OK Date: 10/30/06 Location: Press Baghouse (EPN 

### 40) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate in Rinse (mg)

### ~nn:inlllHHtH:lHf 

## lHnlHHlHjiti0.6l**;i;:;i1:n;;;;;;Hl~~o;** 

### 0.0003**HH:lHi¢~6!1:@1**

# ;::;:::;~~l&~:**UlfHHi~o/.91:0.61**

# ll:m::~~~~:~: 104.0121

0.0003 104.0080 3.85 Run 2

### ;n~fHnHHlillHnUuH 

# HHHHUHHtili!ooS.l HnHiHHllHllilaO.Ol 0.0003 

# iHHHliii&Jo6l**YinlnztH~~P:NO lUHt~5t17:4i52l** 

### )/Hf1li:~J.b6.l 

## nHlHiSlZ$iAM.l**lnllnitOO)H1.~5tl** 

# ;;;llllljltol9io6.1

# m::::i&k~:a~: 1111 ;; ; 

# 11fild.i9:t:<>a;**i;i~Hl;H3~~~~M~ HUiW0.5t17:~~9.~**  

### 105.7452

0.0003 105.7420 2.85



## H20 BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va*Pa) = g/g

### Ul~lnHHHHH2ool

# ~w:l~U~M~rl:**n:~uo&.l64S.Ol**

## HUHnllfl~¥:0.61**)1Yi2i~ai~M~** 

## iiililiifQO:J64B.91 106.64895 

## l:ljl)!llltv.9.1:06l**<:lHH1:~20l~Ml**

### n~Hll**o$..~489; }HH~lt¥:9¥:G.6~**  

## lHnHnlS:1f-9nP:Ml )}l{Q$:J64$5l 106.6487 0.00025 1E·06 Note: 

### In no case should a blank residue greater than 

### 0.01 mg/g or 

### 0.001% of the blank wei ht be subtracted from the sample wei ht. Run 3

### :Hnl~lm~UlHnnlt

## HniHHHHnieHm~l**H~H~ ~=~l~HjH1~;3mg;**  

### 0.0003

# :l:lml;~~~r&~~**UU1HH~i$4~;li!** 

# Y\T1li.1:¥:d&.

# w::::i~i~~1~;1**~UH1Habi.91:d~'** 

## WHiHlm$nlliMW**UH~OllJ~40.4~;**

### fHTjtt~iavo.&.:**~;~~H ~!H?!sg;P.Ml:** **;=nn;aol~!B.4(jS:i** 

### 101.8426

0.0003 101.8404 1.95



# 147

## PARTICULATE ANALYTICAL DATA FORM Company: Dal-ltalia, Muskogee, OK Date: 

### 11/2/06 Location: Phase 

### II Scrubber Exhaust (EPN 

### 29) Run 1 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) 

## = Ca*Vaw·•Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate in Rinse (mg)

### ~~iHllilillitJlV.$~~~ 

# nnlolooiai3.1:1**inH;WHHHiHli~&S~** 0.0002 

# ilHHHHfii.S.t:OO.

# mm::~m:~:;

# lll:l:l;l:~~;r::**HHH406:J4.7:~ HWWH~ol:e/:001** **HiHHH~!l2$lA~l 11Willliil&.A6~.0l** 

## mmnH~dl:ef:tl6i**lHHHni~ta~~P::Ml Hkl\~Hl.6**  

## ..**=4~2ll** 

### 106.4744

0.0002 106.4621 12.18 Run 2 

# HHHHHbl1i:$5£**H10too12ia1~**

## ~Hl;i;lnn:Hlng4fu~ 0.0002 

# HHHHtii6iosl**nnnsi241AM~** 

## ;nn$®:QllliSl 

# WlUHittli:6J.oS.l**HiU!iH3~0:4=EMi ~ilni** **H11()()~~4.I** 

# s i

### HHWW~PI~i()ei 

# lHiiHil11:laEJi;4Ml**Hlii1110~Hl3.2Si**

### lHHHntGI:~J.QEii**~HilHigiS$lP.Mi ~~Hill!OOlO.a2UH**  

### 100.0415

.

0.0002 100.0322 9.06


## ACETONE BLANK ANALYTICAL DATA FORM
Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va«'Pa) 

### = mg/g

### HHHmHHil~lH2~1**iliHHllit~61:001 ~=lHHHl$~ltll!AM1** **i~lHill98:J6~001**

# ~~~~~~~l~~~~~:r:~**;~;;nn;;n;98iS4.=Ell** 

### 98.646**;lnnn~lHJ~91:06l**

# ::::;:::::~~i~~l 98.64575

0.00025 0.00127 Note: In no case should a blank residue greater than 

### 0.01 mg/g or 

### 0.001% of the blank wei ht be subtracted from the sam 

### le wei ht. Run 3

### UUYHd!i.S~f 

# lHtilo6.tztaz, HWli**Hii;l:!:i:i~6.5.~** 

### 0.0002 

# <HHHi.ill6ib.6H**:/HHiaiJ9.!AMi~ nHli()~i5.S~$.:** 

### HHHH!l!~~vo~1**~n;lnn~2t59.iP:r\f ~UH1Q2l~Z~'**  

# HHHii6i.61:btt**HHHl:H1.~i7:)~~t liHHl~O~i$2~~~** 

### nHHiHa~V.6ib.&~**nHlU3~3Zl~Mi ~<ll~02l5.24s:**  

### 102.5326

0.0002 102.5246 7.83



# 15.6

### PARTICULATE ANALYTICAL DATA FORM Company: Dal·ltalia, Muskogee, OK Date: 11/2/06 Location: Scrubber Exhaust (EPN 29) Run 

### 4 Density (Pa) Blank Concentration (Ca) Rinse Volume 

## 0faw) Residue in Rinse (Wa) 

### = Ca*Vaw.j(·Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time Beaker Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) ·.Average Beaker Tare Weight Weight of Particulate in Rinse (mg) 

## ;;m;1;H:n;Hnilla6l 

# 1H1H2l9W.telt}.7:l ;)j(lH::inHt2t 0.0000

# tl1l1l:::l~:~~r~~l**n:Hqos1~o.6:**

# \'!,!,'!~S~!:~**~ HHHil0/:1~1:6.61** **:U~HHH1.~lt$l~~l** 

## l::::;;lHHtOSOO:

# lllll:m~~~r~~~**:~n=Hllt!lS0089~** 

### 105.0606

0.0000 105.0590 1.60 Run 

### 5 [[j;:;j;**i~~** 

## lillliliU361**HH2194ia~1l** 

## :::;:::il:l:::;;:::li3Sl 0.0001

### :\HiHt~i:61:<>6i

## HY=H~ib.$l;t.\Ntl**l~:l:l:ltQ5l5~Sl**

# :;l:l;l:ll~i:~~~**:Hnnwm>~~Z3~l**

### lkjbl.u~oi¢6.1 

# nn:: :Hl1:! 1=61**~M:**

### HH1105~52ll1H

## ;nnnl6it~i:<>ei**lnn:;H:a~Sbl~r\JH** 

## ;::HdlO.SiSZHH
105.5233

0.0001 '105.5210 2.25



### METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM Blank Volume (Va)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va*Pa) = g/g 

# :HHHHli1HU2ool

# ~~~lllll~l~M:r:~1**i)jl~ll03.1ft5~**

## UHHHtt~6.ko6!**:HHllllltg!~~ji?:Ml Hiilj1jfm~~~t5.41**  

### 103.1154

# :~:;:::G~~m~~l**Ui!i!lSSlJ$$~1** 

## ljlHl:OI:Hll:G.61 

## ::::::::::s•a5::pM:

# ~11~;~~1~o&~it$$1 103.1153 lE-04 2.941E·07 Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 

### 6 

## HilU1<n=tit3&:**HH2~9~1e~mi: :n\::nn:n:::::J~~l**  

### 0.0001 

# @Hl1iii.6¥.Q&.\

# ::::mi:~~~~; HiHHHtlv.6V:m&:**wnnn\B~=taifrH~t** 

## H:nnH>biS03e/ 

# 1HiHtoiiPI.tti6.l**:Hl:lH7.~i1:l~Mr** 

## :::::;ll0bJS030::**~Hnilt0.1:1b~b&.~ mnnn3~~s:~ML**  

# n?::looiso-gG::
100.8036

0.0001 100.8030 0.54

;. 

# 157

## PARTICULATE ANALYTICAL DATA FORM Company: Dal·ltalia, Muskogee, OK Date: 11/2/06 Location: Scrubber Exhaust (EPN 29) Run 4 Density (Pa) Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca«Vaw*Pa Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight

Date of Weighing Time**~eaker** 

### Tare Weight Date of Weighing Time Beaker Tare Weight Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight Weight of Particulate in Rinse (mg)

### nwn;111n~1HWHi1J**~~HHH[i;IEiloo~ ~lmiHH~H~Hli$001**  0.0003 

# HWHHlii/.61:6.61**HiHi~W~iU~6.ii?:Ml nHHllt4~i~®l**  

# HHHnfOil:ool )::):S:lZAMl**~/UlJ4P~5®~** 

# HHHlljoV:s/:061**~lU~lHi7:~9~1AMl Hilin1t1ll!tJi~U121** 

## lWHHl~~~W~I:®l 

## l1ll)ll3i@SHP::-Ml**~~l~1Wfl4Ji4~()1** 

### 114.1500

0.0003 114.1411 8.60 Run 

### 5 

# H11H11Hlilnnnnn;ti

# l:l:t:l:~;l:i:m:~~ml 0.0003 

# HHHHili&J()61 HYil:iMliiHP:Ml**U}l®l~H~:gt** 

# HiH/tl/7io6l HiHU:B:l8iAMi 

## U\YiOOt€>5.911 

# HHHHHto/6!/(}61**~~~liH1ii1:i®~!AMi ~HlH~l00l65.03i** 

### ll1Hnn:o.~:61{)e;

## lUUiH~*t#;M;**i~HiUll00~65001** 

### 100.6597

0.0003. 100.6502.
9.25


## H20 BLANK ANALYTICAL DATA FORM
Blank Volume 0fa)

Date of Weighing Time Gross Weight Date of Weighing Time Gross Weight Average Gross Weight Date of Weighing Time Tare Weight Date of Weighing Time Tare Weight Average Tare Weight Weight of Blank (Ma) Ca= Ma/(Va·•Pa) == 

### g/g 

# :;HUHHWH2ool**YH\~;;ftV:S/:061 ~H~ill~J~~Ott~lAMl** **~>YtOS:J64SOl**

## CHHllllt~~ool**~lHlillH~lgeya?~Ml ~~n;~;llo.~:64B9l**  

### 106.64895**1HHHH1~~WS.1:~6l HHlHiH11:ii20lAfM~** 

### 1)1lllS~16~$9\**)l1H;ao.Y:9~~6l HHllllS:~~n~Ml** 

### nHlilll05~~85l

106.6487 0.00025 1E·06 Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank wei ht be subtracted from the sam le wei ht. Run 6



# · H)Hlni1HUf

nLH?;iElbK 1**~1111** 

# u Hi 

# 1

n 

# 11 n30.0.**~** 0.0003 

# WH111i61.o6H

# :::m:~~~~~~; H?il!ihi:d5.= ><d8-::2s:AM1 H:HlD1i068$:.**HUHHibl6¥:d~:** 

## 1inmllitciatArW**1i1HHa07:J05!4.~1**

# l~lilllll~~g~r&~l**<Hil0~10.54l'** 

### 107.0683

0.0003 107.0542 13.75



# 158

## FILTER ANALITICAL DATA

Company: Dal-ltalia, Muskogee, OK Date: 11/2/06 Location: Phase 

## II Scrubber Exhaust 

## (EPN 29)

Filter ID Number Date of Weighing Time Gross Filter Wt. Date of Weighing Time Gross Filter Wt. Ave. Gross Filter Wt. Date of Weighing Time Filter Tare 

## Wt. Date of Weighing Time Filter Tare Wt. Ave. Filter Tare Wt. Wt. of PM on Filter (grams) Total Weight of Particulate (mg) 

## Run 4 Run 5

## !$~$.1Hl)H!!Hi

# ::,::!~~~~=: HH\QU$$.131

# .!:!::~1~~6,~!**HHUHP~$f7:$1** 

## 0.3874**==::=:::;f~i· ··'Jn=;j=** **H:nn::·~~~-** 

## ·**~~~:** 

# HHH2l4QiP:M1**lHUlHO~~~l**

## Hi1jniot1!oto~1**iH1HS.~!41:1AMi**

## nnn:JK~6421 0.3642 0.0232 23.2

## $o~nHi~HUWj

# t!!:!!~~~Wl~!**~H1HOi3SS~H**

## nn~HH~11~6lma;**111Hl~4.~lP:M1 )1HUlO;~aSQl**  

## 0.3786**::::::::=;;1\=Jn:i~a···= ·~;:~:i~~:\Y.i:~~** **.~**

## HHl~a~lP.tW**:flHH!HOt~a~a; =;=;~~~oiH;oiaa~** 

# ;:;;;;~~5.=~M;

# :!i~ili~1lo\~~~~; 0.3643 0.0143 14.3 

## Run 6

## i$HlG.~iW~iUfH1iH**H~~\lllijl$1®:~ jHi1:~~~HAMU** **~H\(f:i~$1.01** 

# UHUMiHJsY:P6i1**f1H~~~()J?:MH**

## :HHHHlQlaar~n 

## 0.3871

## 1~~Wd~ot.$.f:O.~t 

# nHiatl3SHP:Mn**:JHU;o.~aa5t**

# ,:,:,~~~~~- :\lHHQ.4$$®l
0.3651 0.0221 22.1



# 159

## Sheet1
Summary of HF, HCI, and Cl2 Analysis Plant: Dal-ltalia, Muskogee, OK Date: 11/2/06 Location: Scrubber Exhaust (EPN 29) Run# Imp# Volume Dilution Fl-, ug/ml HF, mg Cl-, ug/ml HCI, mg 1 1 & 2 350 1 0 0 0 0 1 1 & 

## 2 

## 350 1 

## 0 0 0 0 

## Average 0 

## 0 1 1 & 2 350 1 0 0 0 0 1 1 & 2 350 1 0 0 0 0 Average 0 0 1 1 & 2 350 0 0 1.11 0.399378 1 1 & 

## 2 350 0 0 1.03 0.370594 Average 0 0.384986 Run# Imp# Volume Dilution Cl·, ug/ml Cl2, mg 13&4 250 1 0 0 1 3 &4 250 .1 0 0 0 13&4 250 1 0 0 13&4 250 1 0 0 

## 0 13&4 250 

## 1 0 0 13&4 250 1 0 0 

## 0



# 165 Page 1

# Conditions 2.53 

# ug/ml Fl- 

# in H2S04 : 2

.. 51 

# ug/ml Cl- 

# Ln H2S04 

# Date 11/08/2006 

# Time 

# 09:os:ss
256

.. 000mV 

# Component -25.600mV 

# Retention**·--·-·--·-·-~~**

## ........ ,_

# ....

# - ....:"""""--·--·---·

..

# ---·---·-·-·-..

# ···-·-···-··""'"""'""""""'--·-·-·-·"'"'-·--·----···-

........__ ,_.,.,,.,_,_,_,_,

# ... ,

# ___

# ..,_

## .......--:·-

## ..

Fl# ClFlCl- •I! 

# li

.. 

# ::55:·-

# ·~f:~· :'-•1



### I 

## 31""'""



# I 

# J

...-

..

5-·-·-·



# L

.................

# ~-- ..·--·-..·--..-········--·---·..·-·-·..··-..·-·-··-·-..

# ·--·-----·--·-·~:~...............................--·-·--·-·--·..···-··..··-···-···---.............-.. Component

2 

# Number Retention 1 2 

## 1

.. 016 1

.. 550 

# Area 163

.. 36 M 

# 144.40 M 

# External Units 1.49 

# ug/ml 2.25 

# ug/ml
3.74 

# Area External

163.36 M 1.49 

# 144.40 M 2.25



# 167

# Conditions 2.53 ug/ml Fl- in H2S04 : 2M51 

# ug/ml Cl- in H2S04 Date 11/08/2006 Time 09:20:35**-25~600mV** 

## 256.000mV 

# Component Retention Area External

Fl# ClFl# Cl

# 1,.---·-·-·::r-------------·----·----··--·----------·---·----·--··-------··-··-····---

.r/ 

## I. 

## 1·--·

# J~·M• 178.95 H. 

## 1.73

I• 

## 1 ,566**··;·~;::;::;~~:::::uonz:•** 

## 150.10 2• 35 

## 2·--"

3

......



## 4·--...



## 5 --·

6



# Component 

# Number Retention Area External Units

2 1 

## 2 

## 1.033 1.566 178.95 M 1.50.10
329

.. 

# 05 1.73 

# ug/ml 2.35 

# ug/ml
4

.. 08



# 168

# Conditions**5~06** 

# ug/ml Fl- in H2S04 : 5.06 

# ug/ml Cl- 

# in H2S04 Date 11/08/2006 Time 

# 09=29=19**-25~600mV 256~000mV**  

# Component 

# Retention**1'""'"''"'''''''"''"!1""'"'"'"""''"'"'"''"'"''"'""'"''""''"'"'"'"""""'""'"'"'"'''"''"'"'"'"'"''"'"'"''""''""'"'"""''"'""""'"''"'"""'"""''"'"'"'"'""'"''"''"'"''"''~'m'"'""'''''"'"''"''''"''"''""'"'"'""** 

# (unknown)Fl# ClI 

# i; 0.7831 ::....;::::::::::::•· Q 

## 1 I**••••••••••••••••••••u••••••••••••••••••·•••••••••••h••"·~Uit:ar:l;ld5:t1UI** rtE•ts•

t 

# f"""" ,.,)t"""""""'""""'""""'""""""'"'"'""'""' I ' 

## 1. 

# sool

....i.'""""""'-"""'"'"'•••r:nrunr.I:U:U' 

# I**:!·i:::::::::::::::~::::::::::::::**.................................................................................................- ................................................................................................................... 

# 2,

.........



# I 3'

........



## 4

........

5**··~·"''**

# 6~

I . .

. 

# . !

.......................: ..............................................................._ .......- ..............,_.,_............... _,_,_,., ......................................................................................... 

# Component 

# Number Retention External Units

# FlCl2 

## 1 2 

# 0.950 1.500 465.12 M 

# 301.07 M

766

.. 

# 19 5.78 

# ug/ml 4.65 

# ug/ml

-10**~43** 

# Area External

109.64 M 

## NIA 

# 465.12 M 5.78 301.07 M 4.65



# 169

## Conditions 

# Date Time 5.06 ug/ml Fl- in H2S04 5.06 ug/ml Cl- in H2S04 11/08/2006 09:32=01


## 256.000mV 

# Component -25.600mV 

# Retention



# FlClFlCl

# r····--·-
..·-:.-t-····--·-·······-·····--·--·-····

..--................................................................................................................. _

.......____....

.•J 

## ·'· ..;1 

### H: ri: 

## 1

• 1

.......

# ~**::::~~=:~~::::::::::.:::;:::::::::::::::::::::::::nr•mmr•** 1,.-· 

## 1.550 

# 2['"'" 

# r·· 4j

........

# "f;~·;:::;:::::::;:::::::::::::::nrt• :•1:1



# t- '

# 6~ i ·. ·. 1.

..................:........,_,_.,.,............................_____,_,.,........_______, _____.,___,_,_,__, __,,__,_,.....---··-···..--·-···-·-·..···-····-·· Component 

# Number Retention Area External Units

2 1 2 

## 1.016 1.550 453.47 M 304.60
758.07 5.66 

# ug/ml 4.70 

# ug/ml
10.35 

# Area External

453.47 H 5.66
304.60 4.70

# Conditions 7.58 

# u.e/ml Fl- in H2S04 : 7.52 

# ug/ml Cl- in H2S04 

# Date 11/08/2006 Time 09=41:01**-25~600mV 256~000mV**  

# Retention 

# r
..................-r····""'"'""'"'"""'""""'"'""""""''"""''"'"'"'-""'"'"''"'"""""'"""''''""'"'"''''"'"'"'"'""'"'""'""'"'"'"'"'""'''"""""""'""""''""'"""''""""'"''"'"-·-·

...................., 

# Component



# FlCl

# FlClI II I I**I~** ! 

# 1 . 11--·

# J:::~~==::.::::::::::::::::~:::::::::::>•........................... ;
1 5 3 1 I!"•,,,.,,,.,,.,,.,,,.,,.,,,,.,,,.,,,.,.,.,,.,.::::IIIIIIIIIIIIIHIU13nlllll' 

## ·' 8 ':.,

............................................... ·:



## 4·-····

......................

# ~................................................. :...................................................................................... _ ..., ...................................... _,_,__, ....................1 

## Component 

# Number Retention Area External Units

2 1 2 

## 1 .016 

## 1.583 694.10 M 

## 452.05 7.80 

# ug/ml 7.22 

## ug/ml 

# Area External

694.10 H 7.80 

# 452.05 7.22

# 17~

# Conditions



# Component Date Time



# Retention 7.58 

# ug/ml Fl- 

# in H2S04 

# 7.52 ug/ml Cl- in H2S04 11/08/2006**09:44~03** 

## -25

.. 600mV 256.000mV

1 ..**----···-·"·~~**......... _,__,_,...... --·-·····-··- ..···-···--· .. ·-- ....._ ..,_ ...**~--** ..··-··-·······-····--·· ................................................- ....- .. - ..·-·-···---·· 

# ·" 

# *· I·

# Fl

# Cl-·

Fl

# Cl- ,I_ 

## 1• 1·-··"

# ~:**:::~===~::::::::::::::::::::::::::::::um:~n~"""''"'"'"'"m::llr.lllr.:nm·•rr** ·'I'' 

# 1.550

3

.......... 

# I
4

.........

5

.......



## 6·-·-..



# Component

2

# ·1:r~.:.========·····=-·

Numbei Retention 1 2 

## 1

.. 033 

## 1.550 

# Area 666

.. 19 M 

## 458.05 M
1124

.. 24 

# External Units 7.48 

# ug/ml 7.31 

# ug/ml
14

.. 78 

# Area External

666.19 M 7.48 

## 458.05 H 7.31



# 172

## Conditions Date Time**10~11** 

## ug/ml Fl- in H2S04 10.02 ug/ml Cl- in H2S04 11/08/2006 09:53:33**256~000mV** 

# Component -25.600mV 

# Retention

Fl# ClFlCl-**~-·-··--··l:···········~·-···-·"'"'''"-··----····-····-···-··-·-·--··--·---···-·-··--···""""''"'"'"""''"'"'"''"'-·--·-······---·-·····~---··-···--··1** 

### II I 1:

. 

### I! 

### 1 • 1''"'""

# ~:··:~::::::::::::::::::::::::::::::::::~::::::::=::::::::::~:::::-.::::::::::::::::::::::::::::::::::a•tlllllll011111mlhlllt1Ctt.ll:tl1tlllliiUI1" li''

# ·(.t~r~===-~:==~=~~~~~~~~~~:::::::::::::

# _____·-·---··--·---·--·---·----·-----···---·· 1.583 2··-·-



## 3·--·



## 4·-·-

5
--..



# I

. '[-··

. 

## 6 :

····---··-.:--···--·-·-····............_•• ,.,____,_,_,__ ,_,____,_,__,..,...___,_,__, __,_,..,_,.,___, ...,••
__,_,__,_,__,_,••••••_,_,__,_,__. __, __,,_,__ .1 

## Component Number Retention 

# Area External Units

2 

## 1 2 

## 1

.. 033 1 .583 

## 1014.52 

# M 648.70 M 1663_22 11.36 

# ug/ml 10.71 

# ug/ml
22.07 

# Area External

1014.52 M 11.36
648·. 70 M 

## 10.71



# 173

# Conditions 10.11 ug/ml Fl- in H2S04 10.02 ug/ml Cl- in H2S04 Date 11/08/2006 Time : 09:56:01


## -25.600mV 256.000mV 

# Component Retention Area External 

# (unknown)

# Fl# Cl

# r-·---:r----··-------------------------·----..--·-·------------1

"If 

## 0.850 ::
.... · ..**·:::::::-~:....** 

## 114.72 M N/A 

## l, 1·--·**::,:~::::::::=::=::::::::::::::::=:::==:::::::::::::::::o~:::::::::::.-.:::::::::::::nnll"'l"ll~'"** 

## 979,88 M 10,97 I, 

## 1.550 

# f.?:==--=---·-- 674.60 H 11.14 

## 2--

5--- 

# I 6,

. 

# I



# l

____

# j_

__.,.,_____________________**~:**

# ______

# j

Component Number Retention Area External Units

# FlCl2 1 

## 2 

## 979.88 M 674 H60 

## 1"'1


# 1654.48 10.97 

# ug/ml 1:1..14 

## ug/m.l


# 22

.. 11

# Calibration file : Fl--cal

AMOUNT INJECTED 

# AREA 0.000 10.110 

# o . o o o**r:::::~**

# .........**~**

# ......_ ..............................................................- ....................................................1 

# I ··... ····........ 

## ··...............



# . , 

# ··...'·

## \ 

## ..•.



# . , 

# '···-'·'\·

## .•..
····•··•··•·

## ...··.··•····•···

### ....•.

## '··

.....•.,

## .,.,··

## ..

# . , .,\t



### ...

## '·

## ··.., ·,,

### '·,

## .,., 

## 9 9 7

. 2 0 0

_______,,.........--.....,...._,_,_,__, __,

__,_,__,.__,_,_,____,,,______,.,..**-~:t..** 

# Avg slope 

# of curve: 98.62 

# Y-axis intercept: 0.00 Coeff of lin regr: 0.79 No. 

# Area 0.000 

# 171 .155 457.175 680.145 

## 997.200**A~ount** 

# .0.000

2.530 

# 5.060 7.580 10.110 CF 

# 0.000 67.650 

# 90.351 89.729 98

.. 635 1

2



## 3

4



## 5

# Calibration file

Avg 

# slope of curve: 66.05 

# Y-axis intercept: 

# OMOO Coeff of lin regr: 0.80 Area

0.000 

# 147.250 302.835 455.050 661.650 

# Amount 0. 000.; 2.510 5.010 7.520 10.020 

# CF 0.000 

## 58

.. 665 

# 60.446 60.512 66

.. 033 1



## 2

3



## 4

5



# 176

# Conditions Dal-Italia, Muskogee, OK Scrubber Exhaust Run**~1** 

# Imps 1 

# & 2



# Component Date Time Volume 350 

# Dilution 1/1 

## 11/08/2006 10=40:22


## -25.600mV 256.000mV Rete n 

## t i 

# or--···..··-....**~·-···-····**

# ..................................- ......- ....................- ......................,_.., ....................................................-.,.._ ................._ .........---····- 1

# ~ fi II 

### I; 

## 1····- 

## ·if::::::· :r:ll·


## 2

.......

3-····



## 4···-·



# I 

# s!

...- .. 

# I 6

.......**I"~·** ·:;1.

.. 

## ;.t 

## : •:·::

### ........

## ._.-.............._,

### ....................................... .



# Component Number Retention Area 

# External Units

0 

## 0.00 0.00 

# Area External



# 183

# Conditions Dal-Italia, Muskogee, OK Scrubber Exhaust Run #1 Imps 1 

# & 2



# Component Date Time Volume 350 

# Dilution 1/1 11/08/2006 

# 10:44:14
-25.600mV 

# Retention 256.000mV



# , ......**·-·-·---··:.~·---···**....

# -·-·--·-·-·--·---·-·-·---·-··-·-··--·-----..

# ·-·-----·-··..

# -··-······..

# -··-·- .............._,

# __,,_.

# _____.. ,

### .....

# --··-·--··-··- : 

# .·,, • r;l,•

.. .!r 

## :**~** 

## 1-····· 

# l·:=··· :!:r •. I



### ... I 

# ':'t:"•:!• 2 ·-·

3--··



## 4--··

5 ·-·-

6

........

ol_,

.. , .......,,,..**_,_l_lloll-••--•-t•I---··--·~·---·-·---IO•t,t**

## ..ltooo-o•o

...otol---··-•-••to•--

..-·-· ..•tooto••
.. ••-o•ooMo-ooooooo

..

## -••-•--•-•-toiN•I-••oool

..---••o•--Po

.....• 

# Component Number Retention Area External Units

0 

## 0.00 0

.. 00 

# Area External



# .184

# Conditions Dal-Italia, Muskogee, OK Scrubber Exhaust Run #2 Imps 1 

# & 2



# Component Date 

# Time Volume 350 Dilution 1/1 11/08/2006 10:53:00


## -25.600mV 256.000mV 

# Retentio

# --:.~: ..•

# :--·-------------------------·-·--]

1·'""" .,**~~::·** 

## :f•' 'il..

.... 

## :'1 : ·:1. 

### 2

........ ' ·:,1 

# :if

:·1:...

___

# ,_~...------..·-····--· ..-·---·..- ..._,__,_,__, __,.,.....---·-·-··--·-....

# ~-·---···-·····---·..·-··-----..---·-"·•-···---· 

## 3

......



## 4

........ 

# I sl-·-··



# I 6

........

1

.........._ ..........:
....... _, ..__,......... --·-···-·..···-·-··"·'"'"•'-······-···-

.. ·-·-·--·····-·-- .. -· .............................. __,,__,_,,_,_,.,.••,_,.,................................. 

# Component 

# Number Retention Area External Units

0 

# 0

.. 00 

# Area External



# 185

# Conditions
Date Time



# L

4A""'"



## 5
UAOHI



## 6

......... 

# Dal-Italia, Muskogee, OK Scrubber Exhaust 

# Run #2 Imps 1 

# & 2 Volume 350 Dilution 1/1 11/08/2006 10=56:14



# . . .,,._._.. , ••,,,..,,.,..,...., .."

.. "'''u'""u"'"'"''"'""'''"""'"'"''"''

..''"'''''''•tloll._,,..,..,

...... .,.,.,,,.,..... ,....,,.,., ... .,..,...,.•-••••,.•••.,•••••••••n
..•••••"J•

....• ..••••••••""'''''''

.. "''-U"II'II'Itlll

..ltt•••-•«•MI«IMI••••"''"''"'•••"'

..u'-'"''•n• 

# Component Number Retention Area External Units

0 

## 0

.. 00 0.00



# 186 External 

# N/A

## Conditions**Dal-Italia~** 

## Muskogee, OK Scrubber Exhaust Run #3 Imps 1 

# & 2



# Component**(unkno~m)** 

## Date 

# Time Volume 350 Dilution 1/1 11/08/2006 11=06:54


## -25

.. 600mV 

# Retention · 256

.. 000mV 

# r .....................,r.............................._ .................................................................................__. __..........................................................................................____..._.'"

___......**~ !~**  

### 0 ,850 

## ,}::::::lr 

## 1........**~I** 

## 1''1

## ~::r

# ··ri:~:::~·

I



# . 61""'""

I 

# ; . L

....**---~-···----·--------·---···------·--·---··-·----------------** 

# ...........**_:~-·------------"-··-··-...1** Component Number Retention Area 

# External Units 

# Cl- 2 1

.. 616 64

.. 95 M 

## 1

.. 11 

# ug/ml

1 

## 64.95 1

.. 11 

# Area External

61.80 N/A



# 64.95 M 1.11



# 187

# Conditions**Dal-Italia~ Muskogee~**  

# OK Scrubber Exhaust Run #3 Imps 1 

# & 2



# Component (unknotvri) (**unkno~m)**

# ClVolume 350 Dilution 1/1 Date : ll/08/2006 

# Time 11:1.0:03
-25.600mV · 256.000mV 

# Retention 

# I

........................F.

...............................................................................................................................................................- ........................................................................ 

## 0 3001 !!.......

. I "!!r• • I •""' 

# , ...

. J1



## .**.~~::::::t·** 

### 0, 1""'"" •:11 

# f''

.....**1.~** 

# 1.61: ·--**:;~~:**

# .._, 3!

........

. I

4

.........

5

........

6

.......



# . '**IIIIIIIH'IIOfiiiiiOIIIIofi~:**.. III.IIOoti

.. IPIItiJIIIIIII.I

...I+tlllll

.. tiNI.IIJIII

.. It+IHIIII

... I

.. Itolll"l

...llll-llll-ll.llllftlllll

.... lloiiiMitUIIII

.... tl

... loolllltl•tlotl+tllllloiiUII

... IIIflllllltnll:l+tlttlll

..**l~ll4** ..llt.lflloii

.. IIIIII•IIO:I•IIOIIIIIOI

.. III

...II

.. I"I

... IIIIIIII 

# Component 

# Number Retention A1ea External Units 

# Cl- 2 

## 1.616 60

.. 45 M. 

## 1.03 

# ug/ml

1. 

## 60.45 

# 1.03 

# Area External 136.50 N/A 

# 74.35 N/A
60.45 M 1.03



# ·188

# Conditions 

# Date Time 5.01 

# ug.ml Cl- in NaOH 11/08/2006 

## 12:17=23
-25.600mV 256.000mV 

# Component Retention**r----·-l~-·-··--·---·-·--** 

# ..····--·------·-···--·----·----·-····-·--·--·--·--···--:-·-·----..--·-·-·--·-·-·----··--·····--·1 

# I**.~·** 0

# .83~**~:.::".·.:>:::=.::::;;==~·-~·**

# ..**=·~···~** (unknown)



# Cl- l • 7



## SO

.....n••:t••;:···::
...**:;~:::::::::::::::::::ti~IUtt\Uuuutuuu.nutumm•lmtummttuiiUnul•**



## 2""'"" 

# I:

# 5~

·-··--·--·-L

..................._____, _______............_____.....................

# ---·-------··---··--·--·----_j
Component Number Retention Area External Units Cl- 2 

## 1.750 

# 275

.. 40 M 4.44 

# ug/ml

1 

# 275.40 4.44 

# Area Externaj



## 1392.20 

# N/A

275.40 M 

# 4.44



# 197

# Conditions

.. 

# Date**Ii9ba~~o~t** 

# cl- in NaOH 12:22=18 

## Ti.me
-25w600mV 256ftOOOmY Component 

# Retenti

# o~---·---T·----------~---·----·------------··--------··-----·----··--·------·------

# 1 0.833**~** I 

## l -···· ,• 

# 1**,··::.;.~:~:::=~~:::=~~::::::;:~.::::;:::::::::::::-.:::::::::::::::'''~'"'"'"'r.llllltll=:.•o::t~~** j



## ::

## ..**~.::**

## ............. 

# : (unknown)



# Cl4

......

5

.........

6'""""

# ""''"'"'"'"''"''":"'"''"'m"'""'"'"""'"''"'"'"''"''""'"''"'"'"'*'"''""'"'"'"'-"""'"'"""'"""''~'"'"'"::,....,,.,_,.,,,,,,,,.,,.,• .,,.,,,..,,.,,.,,.,,,,,.,,.•.,., •

# .,,,.,.,.,.,~,,..,,.,.,,.,,,..,,.,_,,,,.,,.,,.,,,,,.,l Component 

# Number Retention 

# Area External Units C.l- 2 1.750. 

## 270.50 M 4.34 ug/ml
1 

## 270

.. 50 4.34 

# Area External

1056.60 

# N/A

270.50 M 

# 4.34



# 198.

# Conditions Date Time**7~52** 

# ug.mi Cl- 

# in NaOH .11/08/2006

12:26:01


## -25.600mV 256.000mV 

# Component Retention
(unknown)


# Cl

# f

...........- .......'j;

.................................................................................................. _,__.......................................................... _ .......................................................... ou........ 

## j 

# I II •**~** 

### . 

# o. a!

# tL_,..,t;.:::.=:=:..-:::::::===-=--

1 .733

# ~~=~~~;J:=~-"'=::=::::::::::::==::::,····~··~····"'""'' II,



## ... 

## 2

........ 1::**~!:**



## 4

....... .

5

.......

6

.........

1

.......................:
...........................................

## ~.................................................................................................. ;:
......................,_.................................................................... 

# Component Number Retention Area External. Units 

# Cl- 2 

## 1.733 397.90 M 6.73 

# ug/ml
1 

# 397

.. 90 6

.. 73 

# Area External

1170.90 

# N/A

397.90 M 

## 6.73



# 199.

# Conditions Da·te 

# Time**7~52** 

# ug.ml Cl- in NaOH 11/08/2006 12:32:00
-25.600mV 256.000mV 

# Component Retention

. 

# r
.........- .......

# r
...................-=-·············-··-·····-····---··-··-·····-·············....................-................................................................._.,,..........._,, .

# ~ 

# i 0.833**~~~** I



## 1.

# 76:

# ~2~[:::~~:=~,~~~=-~=~· I 

## 2

........ !i:: 

# (unknown)



# Cl

# I 3 -···



## 4

......



## 5

.......

6 -··· 

# I

# --·----~~___:,_________________. _________________..:.._
_______(.__j
Component Number Retention Area External Units 

# Cl- 2 

# 1.766 419

.. 95 M 7

.. 04 

# ug/ml

1 

## 419.95 

# 7.04 

# Area Externa

1163.10 

# N/A

419.95 f·l 

## 7.0·



# 200

# Conditions Date Time**10~02** 

# ug/ml Cl- in NaOH 11/0S/2006 i2:36:32


## -25.600mV 256.000mV Component Retention Area 

## Externa.

,...... ,_........... 'li'"""'"'"'"""'"'"'"''"""'"'"""'"''"''""'"''"'"''""'"'""'"'"'"''"'""."''""'"'"'"'""''"'"""'''""'"""'"''"""'"''"'"'"'"'"'"'"""'"'"""'"''-'"'"'"'"''""'""'""""'"'"'"'"'"'-"""'1 

# I ..J. 

### 0•

8 3



## 31 .• 1 ;!,,.,_,.,••,_•.,.,....,._,..,_,.,"'

..

### ""-'"'"'""""""""~'~"'"""tl''_,tllnll:tntrn• 

# I 1207•8 0 N /A 11••'""' •' I : , ..... •••"'"'-""""'"'""""''"'"'"'""'""'"-"""'"-'"''' 

## (**unkno~m)**

t •• •
....

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# ll~::::::::::::.....; ................-........................ , ..,;................. . . 1 7 50 , , . 1 .. :
.. ,•• ,..............................**~** •• ,.... ,.....**,,."''''''ut••••Etlltnnu•m~SUIUIMtul:ltt~UmuEinmmtnmEumnuln1UIIPilUUtlttU5:tutiUIUtnnu••n•** 

## 52 9,1 0 M 8 7. •
........ II, •. 

# 2 :

# Cl4

........

6•.•.•.

I ,: o

IIOIIOIHIIIUtofiMIIIIIolllllltiiiHII.I+IIIUI+IIt•ll•lllt9II•IIIII•II

.. I

.. IIOIIolll.lllllllllflllollt11111HifiiOOI11fiiU

... I

.. o ...IIOII•olooll111101oii

.. IIOIIIIIINI

.. Iltiiii11111011UIIIIIt•o•IIIMINIU

..IIIIIHI

.. III.IHIMIIIIII

.. IItloloof

.. t•oti04IOOfiOto

..IIOI

.. IIOIIIIIoiOioiiOOIO 

# Component Number Retention Area External Unl.ts 

# Cl- 2**1~750** 

## 529.10 M 8.71 

# ug/ml
1 8.71



# 20'1

# Conditions Date Time 10.02 

# ug/ml Cl- 

# ln NaOH 11/08/2006 12=41=32


## -25.600mV 256.000mV 

# Component Retention

. 

# ····:
..................**~r··**

# .............................................................................................................................................................................................;
...........................- .....................**~** . 

## ,, 

## 0' 8 3 

# f

"'""'' •'•' ,• 1

# :L::::::::::::::::::::::::::::::::::::~::~:::::::::::::::::::::::::::::;:::::::•=r.IIIWIIliiiiiUilll' ,·· , . .1"!•"'

..**·t~** 

## 1. 7 66

# ~c::.:::::~;::.:::-.:.:::::::======:==-::=."::.'=··~

2......... 

# I: (**unknot~n)**


# Cl3

.........

5

........ .



## 6

....... .



# I I

. 

# I . . J

llo41ootll'liilo4P41o"l""l:lll•tlliloll•ll

.. lll+llfoti+IIIIIIIII

.. IIII<IHIIIfiiPI+I'II.IItfiiiiMIII1IIHIMIOI

...IMIIoiiMIUitfiiiiiiiiHI

..::.,................... , ..............,UHIMI

.. IIII+tl+tllloiiiiiHIIIIOIII

...INIHIIIIIIO+It41Mitii

.. IIIUI+IIIotlllln

..III

.. IMIUnootiH11olllllllllllll 

## Component Number ·Retention 

# Area External Units 

# Cl- 2 

## 1.766 531 .60 1"1 

## 8.73 

# ug/ml

1 8.:73 

# Area External

1092.00 N/A

531.60 M 8.73



# 20·2

# Conditions Date Time 

## 2M51 

# ug/ml Cl-. in NaOH 11/08/2006 12:47=36


# -25.600mV**256~000mV** 

# Component Retention Area 

# Externa**J""""""'""'''"';!l''"'"""'''""''"''''""""'"'''""''"''"'"""'"'"''""'''"'"'"""''""'''''""'''"'.""''''""'""""'""'""'"''"'"''"''"''"''"''"'"'"''"""'"''"""'"'"~""'"'"'"'''''"'"'"'"''"'"'""'""'""'~"'"'""** I ·i' 

## 0•



## 831

# )~--·-----·-··-··-·-··------------ ............

# ~. 1382 • 20 N/A I

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# (unknown)



# Cl- 1. 7SO

........, ..::.•. r.
..

### "i::~:::::~:~:m:::::::::.............................. 

## 155.60 H 2.1 2t'""'" :



# I :

4

........



## Component 

# Area 

# External Units 

# Cl- 1.750 155.60 M 

## 2.13 ug/ml

1 

## 155.60 2

.. 13

( 0 

# 203

# Conditions Date Time 2.51 ug/ml Cl- 

# in NaOH 11/08/2006 

# 12:59:40
-25.600mV 256.000mV 

# Component Retention Area External

,..................... ::··········"·"'"''"'"'"'"""''"'-'""''-"'"'"""'"""'"'""""""'"'"'"'"'""'"'"'''""''"''"'"'"'""'"'"'"''"'""""''"''"'"''"'""""''''""'"''"'"'"''"'""'"''"'"'"'"''"'"'"'"''"'''"'"'"""1 

# J I 0. 833 :· .!

.........-·-···-····--·· 

## 1145 .1 0 M N/A l .:
..... •' •'. :
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## ·:.::
................

# ·:**1.733::~1'1"!!'!'"""•"";""'""1nii111U:UIIII'** 

## 147.30 M 2.73

.. '1•·:

........ 

# (unknown}
Cl2'"'"'" •



## 4

.........

5

........



## 6

.......



# . ,:

,..,'t''"'''''_'
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.. ""'
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....,,_,.,,.. , .. , .. , ........... ,,,.,.,., 1, 11 , 11111 "''"'" 

# Component Number. 

# Retention Area External Units Cl- 2 

## 1.733 147

.. 30 M 2.73 

# ug(ml

1 

## 147.30 2.73



# 204

# Calibration'file Cl-

.. cal

AMOUNT INJECTED AREA 0.000 10.020 0

.. 0 0 0**~·~:::·····"'"'"'"""''""""'"'"""'""'"''""'"'"'"'""'"'"''''''''"''""""''"""'"''"'"'"'''"'"""'"'"""'"'""''"''''""""1** 

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## 53 0 • 3 50

# -----·----·-----~------·------~----~--·-- ..

# -~~~~~~J . Avg slope of 

# curve: 52.92 Y-a>< is 

# intercept: 

# o.oo· Coeff· of lin regr: 0

.. 90 

# No. 

# Area 

# Amount CF



# o: 0.000 

# ·o. ooo 0.000 1 : 

## 147.300 2. 510'' 

## 58.685 2: 

# 272.950 5.010 

# 54.481 3: 

# 408.925 7.520 54.378 4: 

## 530.350 10.020 

## 52.929 1

2

4



## 5



# --

# Conditions Dal-Italia, Scrubber Exhaust Run #1 Imps 3 & 

# 4·



# Component (unknown)


# ("unknown) (unknown) Date Time Volume 250 

# Dilution 1/1 11/08/2006 13:38:31


# -25.600mV 256.000mV 

# Retention

.**·----·~·-~-. ·-------·---·----··--·-·-------·--·-~--·---·-----·----·--·**  

## I! 0.

# 83~ ·····- .

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0 

## 0.00 0 

# .oo. Area

573.20



## 100.50 226.50



# 212· External

N/A



# N/A N/A

# Conditions Dal-Italia, Scrubber Exhaust
· . Run #1 Imps 

# 3 

# & 4 Volume·250 Dilution 1/1



# Component (unknown)
(unknown) (unknown) Date 11/08/2006. Tim.e 13:40:57
-25.600mV · 256.000mV 

# Retention 

# r

......................i:;:·····-

.................................................................................................................................................................................................................. -....................... 1

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# I 0
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## 616i 

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## Component Number Retention 

# Area External Units

0 

## 0.00 0.00 

# Area

661.40



## 122.30 229.45.



# 213: External

N/A



# N/A N/A

# Conditions Dal-Italia 7 

# Scrubber Exhaust Run #2 Imps 3 

# & 4



# Component (unknown)
(unknown} (unknown) : Volume 250 Dilution 1/1 Date 11/08/2006 

# Time 13=49:17
-25.600mV 256.000mV 

# Retention 0

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# Component Number Retention Area 

# External Units

0 

## 0.00 

# Area 

# External

550.15 N/A



# 125.55 H N/A 210.85 N/A



# 214·

# Conditions Dal-Italia, Scrubber Exhaust Run #2 Imps 3 

# & 4



# Component
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# (unknown) (**unkno~m)** 

# Date Time vo.lume 250 

# Dilution 1/1 11/08/2006 

## 13:51=43
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# Retention

.**~rea** 

### 1 ......................**;~~"''''"''"''"'"'"""''"""''"''"''"'"''"''"""''""'"'"'""'""'"'"''""'"'"'"'''"'"'"'"''""'"'"'""'"'"'"''"'''""'""'"''"'"''"'"'"''"''"""''"""'''"""''""'"'"'"'"'"""'"'"'"'"'"''"'"'""1** 

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## Component 

# Number Retention Area External Units

0 

## 0.00 0.00



# 215 External



# N/A



# N/A**N/~**

# Conditions Dal-Italia, Scrubber Exhaust : Run #3 Imps 3 

# & 4 Volume 250 Dilution 1/1 Date 11/08/2006 Time 14:10=18
-25.600mV 256.000mV 

# Retention Component**I"''''''"'''''''''''''"~'''''""""""'"''""''"''"'"""'"'''""''"'"'""'"'"'"''"""''"'"""'"'"'""''""'""'""''"''""'"'"'W''""''"'"''"''"'"""''"''''"''"'"''"'"''"''''""""'"""'""''""'"'"'"''"'""''"""'"'"''"""I**

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OiotiiOio•II•II

... II

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.. OOooiiNiotoo-IIOIIoiiOOioOOOIIOOIIOIOOIIHIIIOOIIMIIIIIMIIOIIOOII'IO

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.. I

.. IO

.. I

.. IOIIHOotloo

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# Component 

# Number Retention Area External Units

0 

## 0.00 0.00 

# I 

# I I Area External

552.00 N/A



# 110.50 M N/A 211.40 N/A



# 216

# Conditions bal-Italia, Scrubber Exhaust Run #3 Imps 3 

# & 

# 4

Component
(unknown)

(unknown) (unknown) 

# Date Time 

# Volume 250 Dilution 1/1 11/08/2006 

## 14:12:56
-25.600mV 256.000mV 

# Retention

. Area**"''"'''''"''''"'''"''"jl::••••••••n••••••••••~••••"'''"""''"'"''"'"'""""''""""""'~'""''"'""'"''"'"''"''"'""'"""'"'"""'"'"'"'''"'"'"'"'"''"'"'""'"'"''"'"'"'"''"""'"'"''"''"''"''"'""''"""""'''"'"''"'..;""''"''""''"'"""''l .~~~**  

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## 0 833 1 ;,"""·;·-:u·,..

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## 634.60 

## 1**hll~oU~** : "o**.llltllt"'I"IIIUIO~oll** .. lhiUotUoUoUIU...IootnMUtn• u n 1 • UUU,tEU 

# :r·l

..... 

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......... : /::::::::::::::::::mmm:mu• 

## 114 , 15 2**~** 

## 21 :**:;::::;:;;;;:::::::::::::::::::::::::::::::~:::nn•** 

## 21 0,0 0

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# Units

0 

## 0.00



# 21.7 External

N/A

N/A N/A

### Document No. 034184-25

Dione x Corootallon :228 ·:-ilan Wat · 

### c. 607 3003**.~rnyvale.** CA**l~!ie-3503** •::CSl 737 ·0700 Dioncx U.S. Replonol Olllcus Sunn)'\'ale. CA (405) 737-0522 · Wr.strnrot. t {63G) 789·3650 Hoosioo. 1X (281) 847·5652 ld<n:t. Gl. {770) <U.SIOO

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### 20 May 1998

Dian ex International Subsidiaries Avslria(01)Gi65125 · ·G=rmanr(OG12!i)991-0**8!1pium(03)~3<294 111~(00)1j(j51**  5052 C.wd.l (005)**8~~-*50** J.!,?lil 105) 6885-1213**Ct.~7i!** (552j**2~28** 3282 I:Utl {2) 2ii53-25SO DtnmJ;J. ((5) :;s 36 

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## The· prep_aration and analyses of 

# the**Flu~)fide _S~andard**  was

# performe~ 

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# by DIONEX Corpora_tion Co'nsumables Manufacturing Department.

Document No. 034 183-1 8 1 3-Dec-02

1cnex Corporation 

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# J '} BAROMETRIC PRESSURE: 3o,( 

# C02 ASSUMED MOISTURE:

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# E ·ter Box & 10

·ial #: 30272

Ill! 

### APE Armstrong Environmental Inc. EPA Method 5 522 Series Meter Box Calibration

Pre·Test Orifice Method English Meter Box Units, English K' Factor
Date: 

## -----·-··--·····-> Barometric Pressure: 

## ·····---> Theoretical Critical Vacuum:-> 10104/06 29.43 (in. Hg) 13.88 (in. Hg)
,ORTAI\ For valid test results. the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. tQRTAI\ The Critical Orifice Coefficient, K', must be entered in English units, (ft)AJ•(deg R) 11 0.5/((in.Hg)•(min)). !!!!

···-·-·----- DRY GAS METER READINGS ··-···-····· -CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual
- Ambient Temperature
- dH Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial i20) (min) (cu fl) (cu fl) (cu fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F)

0.24 5.00 107.900 109.503 1.603 77.0 77.0 76.0 76.0 40 0.242 22.0 74.0 0.50 5.00 109.900 112.185 2.285 76.0 76.0 76.0 76.0 48 0.344 20.5 74.0 0.92 5.00 115.200 118.265 3.065 76.0 76.0 77.0 76.0 55 0.464 19.0 75.0 1.50 5.00 118.900 122.823 3.923 77.0 76.0 78.0 76.0 63 0.593 18.0 76.0 2.90 7.00 123.800 131.329 7.529 78.0 76.0 79.0 76.0 73 0.824 15.0 74.0

•••••••······································· RESULTS •••••••••••••••••••••••••••••••••
.. •••••••••••••••• ·RY GAS METER ·- UME VOLUME !RECT CORRECTED 'll(std) Vm(std) {cu fl) (tilers) 1.552 0.1 2.216 0.1 2.974 0.1 3.809 0.1 7.328 0.3 ·-···- ORIFICE

--- VOLUME VOLUME VOLUME CORRECT CORRECT NOMINAL

Vcr(std)· Vcr(std) Vcr (cu ft) (liters) (cu ft) 1.543 0.1 1.587 2.191 0.1 2.256 2.953 0.1 3.040 3.775 0.1 3.890 7.344 0.3 7.554 •• DRY GAS METER •• CALIBRATION FACTOR y Value Varialion (number) (number) 0.994 0.000 0.989 -0.005 0.993 -o.001 0.991 -0.003 1.002 0.008 ---.ORif.lCE

--- CALIBRATION FACTOR dH@ Value Variation (in H20) (in H20) 1.372 .().0474 1.419 -o.001 1.438 0.018 1.434 0.014 1.436 0.016 Final Average (deg F) (deg F)

74.0 74.0 75.0 74.5 74.0 74.5 74.0 75.0 74.0 74.0



## Average Y 

# ------> 0.994 1.420 <------Average dH@

For Calibration FactorY, the ratio or the reading or the calibration meter to the dry gas meier, •cceptable tolerance or individual values from the average is +-D.02.

I pressure in inches or H20 that equates to 0.75 crm or air individual values from the average Is +-0.2. Date: 

# /i:J /

# ~ 

# /6£ CONVERSION FACTORS 1 mm Hg • 0.13330 kPa 1 em 

## = 0.39370 inch 1 mm 

# = 0.03937 inch 1 cu fl 

## = 28.32 liters

•• Average Temperatures ••



### OGM OGM Ambient Outlet Overall Temp

(deg R) (deg R) (deg R)

536.5 536.5 534.0 536.0 536.0 534.5 536.0 536.3 534.5 536.0 536.8 535.0 536.0 537.3 534.0

## Temperature Meter Calibrations

Meter Box#: 10 Date: 10/04/06 Calibrated By: 

## RT Emtech 42312 

## Degrees F Calibrator Probe Stack Oven Exit Auxiliary Point 1 32 34 32 

## 33 32 32 Point 2 21'2 213 212 213 212 212 Point 3 752 753 752 753 752 752

Emtech 42312 

## Degrees R Calibrator Probe Stack Oven Exit Auxiliary

Point 1 492 494 492 .493 492 492**~** 

## Point 2 672 673 672 673 672 672 Point 3 1212 1213 1212 1213 1212 1212

Percent Difference Probe Stack Oven 

## Exit Auxiliary Point 1 0.404858 

## 0 0.20284 0 

## 0 Point 2 0.148588 0 0.148588 0 0 Point 3 0.08244 0 0.08244 0 0



# 275ter Box ll rial#:

!!!! 10 

### 30272 Armstrong Environmental Inc. EPA Method 5 511 Series Meter Box Calibration Post-Test Orifice Method English Meter Box Units, English K' Factor
Date: 

# --·----------> Barometric Pressure: 

# ·-····-> Theoretical Critical Vacuum:···> 11/06/06 29.35 

### (ln. Hg) 13.84 (in. Hg)

;,ORTAf\ For valid test results, the Actual Vacuum should be 

### 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above.**~RTAI\** The Critical Orifice Coefficient, K', must be entered in English units, (ft)"'3.(deg R)"''.S/(Qn.Hg)*(min)). 

### !Ill

-···--------- DRY GAS METER READINGS

- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:-> 13.84 (in. Hg) Volume Volume Volume Initial Temps. Final Temps. Orifice 

### K' Orifice Actual
- Ambient Temperature
- dH Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial H20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see abovo) (In Hg) (deg F) 0.91 5.00 460.600 463.630 3.030 67.0 66.0 69.0 67.0 55 0.464 18.0 69.0 0.91 5.00 464.000 467.023 3.023 68.0 67.0 69.0 68.0 55 0.464 19.0 70.0 0.91 5.00 467.600 470.637 3.037 69.0 68.0 68.0 68.0 55 0.464 19.0 71.0

••••••••••••••••••••••••••••••••••••••••••••••• RESULTS .,.. ...,..,. ............................................. . )RY GAS METER ••• -------ORIFICE------ LUME VOLUME VOLUME VOLUME VOLUME RRECTI CORRECTED COR RECTI COR RECTI NOMINAL /m(std) Vm(std) Vcr(std) Vcr(std) Vcr

(cu ft) {liters) (cu ft) (liters) (cu 

### ft) 2.982 0.1 2.960 0.1 3.024 2.971 0.1 2.956 0.1 3.029 2.983 0.1 2.954 0.1 3.030 -· DRY GAS METER
- CALIBRATION FACTOR y Value Variation (number) (number) 0.993 

### -0.000 0.995 0.002 0.990 ·0.002 ---ORIFICE·-- CALIBRATION FACTOR dH@ Value Variation (in H20) (in H20) 1.437 -0.0009 1.438 

### 0.000 1.438 

### 0.000 Final Average (deg F) (deg F)

69.0 69.0 71.0 70.5 71.0 71.0



# Average Y 

# -------> 0.993 .'·1.438 <-------Average dH@

!l: For Calibration FactorY. the ratio of the reading of the calibration meter to the dry gas meter, acceptable tolerance of individual values from the average is +·0.02. For Orifice Calibration Factor dH@, the orifice differential pressure in,i9ches of H20 that equates to 0.75 cfm of air 

### at 68 F and 29.92

## i~~~~~--~~~=-~**a;;~table--~er~f i~iduai:.V'Stf;"es**  from the average is +-0.2. SIGNED:

# '7J:;...--t..~·u;Z.·-·-:--f**~..;:-(~**

N -...] 

## CP

# ~ Dale:

# ///6:~/ DGM Outlet

(deg R)

526.5 527.5 528.0 CONVERSION FACTORS
1 mm Hg**~** 0.13330 kPa 

### 1 

### em = 0.39370 inch 

### 1 mm 

## = 0.03937 inch 1 cu ft 

# = 28.32 liters



### OGM Ambient Overall Temp (deg R) (deg R)

527.3 529.0 528.0 530.5 528.3 531.0

## Temperature Meter Calibrations

Meter Box#: 10 Date: 10/04/06 Calibrated By: RT Emtech 42312 

## Degrees F Calibrator Probe Stack Oven Exit Auxiliary

.

Point 1 32 32 32 33 32 32 Point 2 100 100 100 101 100 100 Point 3 250 250 250 251 250 250

Emtech 42312 

## Degrees R Calibrator Probe Stack Oven Exit Auxiliary

Point 1 492 492 492 493 492 492 Point 2 560 560 560 561 560 560 Point 3 710 710 710 711 710 710

Percent Difference Probe Stack Oven Exit :Auxiliary Point 1 0 0 0.20284 0 0 Point 2 0 0 0.178253 0 0 Point 3 0 0 0.140647 0 0



# 277!ler Box 

### t 11 rial#: ·10312

!!!!! Armstrong Environmental Inc. EPA Method 5 522 Series Meter Box Calibration

Pre-Test Orifice Method English Meter Box Units, English 

### K' Factor Date:----··------> Barometric Pressure: 

### -------> Theorelical Critical Vacuum:--> 10/04/06 29.46 (in. Hg) 13.90 (in. Hg)

:JORTAt-. For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Crillcal Vacuum shown above. :JORTAI\ The Critical Orifice Coefficient, 

### K', must be entered in English units, (ft) 11 3*(deg R) 11 0.5/((in.Hg)•(mln)). 

### !!!!!

--····--·-·--· DRY GAS METER READINGS -·-----·---··· -CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual
- Ambient Temperature
- dH Time Initial Final Total Inlet Oullet Inlet Outlet H20) (min) (cu fl) (curt) (cu fl) (deg F) (deg F) (deg F) (deg F) 0.25 7.00 697.600 699.867 2.267 75.0 75.0 75.0 75.0 0.51 5.00 700.200 702.529 2.329 75.0 75.0 75.0 75.0 0.94 7.00 702.900 707.282 4.382 75.0 75.0 75.0 75.0 1.55 7.00 707.700 713.324 5.624 75.0 75.0 76.0 75:0 3.00 5.00 724.500 730.037 5.537 76.0 75.0 77.0 75.0

·••
..··-··············"'·••••••••••••••••••••••• RESULTS

........................ ••••••••••••••••••••••••••••• DRY GAS METER

... -·----- ORIFICE

------- -- DRY GAS METER
- LUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR •RRECT CORRECTED CORRECT CORRECT NOMINAL 

### y llm(sld) Vrn(std) Vcr(std) Vcr(std) Vcr Value Variation

(cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 2.203 0.1 2.163 0.1 2.221 0.982 0.010 2.265 0.1 2.198 0.1 2.252 0.970 -0.002 4.266 0.2 4.144 0.2 4.250 0.971 -0.001 5.481 0.2 5.298 0.2 5.439 0.967 -0.006 5.411 0.2 5.256 0.2 5.391 0.971 -0.001 

# Average Y ----> 

# 0.972

e: For Calibration Factor Y, the ratio of the reading or the calibration meter to the dry gas meter, acceptable tolerance of individual values from the average is +-0.02. Serial# Coefficient Vacuum Initial Final Average (number) (see abOve) (in Hg) (deg F) (deg F) (deg F) 40 0.242 23.0 74.0 73.0 73.5 48 0.344 22.0 73.0 

# n.o 72.5 55 0.464 20.5 74.0 

# n.o 73.0 63 0.593 19.0 73.0 74.0 73.5 73 0.824 16.0 73.0 73.0 73.0

--ORIFICE-----

CALIBRATION FACTOR dH@ Value Variation (in H20) (in H20) 1.431 -0.0298 1.443 -0.018 1.466 0.006 1.479 0.018 1.484 0.023 

# 1.461 <---- 

# Average dH@ CONVERSION FACTORS 1 mm Hg: 0.13330 kPa 1 

### em 

### = 0.39370 inch 1 mm 

# = 0.03937 inch 1 cu 

# n

# = 28.32 liters

-Average Temperatures
-



### DGM DGM Ambient Outlet Overall Temp

(deg R) (deg R) (deg R)

535.0 535.0 533.5 535.0 535.0 532.5 535.0 535.0 533.0 535.0 535.3 533.5 535.0 535.8 533.0

## Temperature Meter Calibrations

Meter Box#: 

# 11 Date: 10/04/06 Calibrated 

## By: RT Emtech 42312 Degrees F Calibrator Probe Stack Oven Exit Auxiliary Point 1 32 32 32 32 32 32 Point 2 212 213 213 213 213 213 Point 3 752 753 753 753 753 753

Emtech 42312 Degrees R Calibrator Probe Stack Oven Exit Auxiliary

Point 1 492 492 492 492 492 492 Point 2 672 673 673 673 673 673 Point 3 1212 1213 1213 1213 1213 1213

Percent Difference Probe Stack Oven Exit Auxiliary Point 1 0 0 0 0 0 Point 2 0.148588 0.148588 0.148588 0.148588 0.148588 Point 3 0.08244 0.08244 0.08244 0.08244 0.08244



# 279er 

### Box# al#:



### Ill! 11 73 Armstrong Environmental Inc. EPA MethodS APEX INSTRUMENTS 511 Series Meter Box Calibration Post-Test Orifice Method English Meter Box Units, English K' Factor Date: 

# ------:> Barometric Pressure: 

# ----:> Theoretical Critical Vacuum:---> 11/06/06 29.35 (in. Hg) 13.84 (in. Hg)

ORTAI' For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. ORTAI' The Critical Orifice Coefficient, 

### K', must be entered in English units, (ft)"3.(deg R)"0.5/((ln.Hg)*(min)). 

### !!!!

-------------DRY GAS METER READINGS--------- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:--> 13.84 (in. Hg) Volume Volume Volume Initial Temps. Final Temps. Orifice**~** Orifice Actual
- Ambient Temperature
- dH 

### Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average i20) (min) (cu 

### ft) (cu 

### ft) (cu 

### ft) (deg F) (deg F) (deg F) (deg F) (number) (see above} (in Jig) (deg F) (deg F) (deg F)

0.94 5.00 770.800 773.869 3.069 64.0 64.0 66.0 64.0 0.94 6.00 775.400 779.092 3.692 66.0 65.0 68.0 66.0 0.94 5.00 779.300 782.380 3.080 67.0 66.0 68.0 67.0

•••••••••••••••••••••••••••••••••••••••••••••• RESULTS •••••••••-.••••••••••••••••••••••••••--•••••••••••••• >RY GAS METER
--- .UME VOLUME**~RECT** CORRECTED m(std) Vm(std) (cu ft) (liters) 3.037 0.1 3.641 0.1 3.033 0.1 -----ORIFICE--- VOLUME VOLUME VOLUME CORRECT CORRECT NOMINAL

Vcr(std) Vcr(std) Vcr (cu 

### ft) (liters) (cu ft) 2.963 0.1 3.021 3.552 0.1 3.629 2.957 0.1 3.027 

# Average Y 

# -------> - DRY GAS METERCALIBRATION FACTOR 

### y Value Variation (number) (number) 0.976 0.000 0.976 0.000 0.975 -0.000 

# 0.975

!: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, acceptable tolerance of individual values from the average is +-0.02.



### t\,j 

## 00··, 

# 0 55 55 55 0.464 18.0 0.464 18.0 0.464 18.0

--ORIFICE-- CALIBRATION FACTOR dH@ Value Variation (in H20) (In H20) 1.489 0.0010 1.487 -0.000 1.487 -0.000 68.0 68.0 68.0 68.0 70.0 69.0 70.0 70.0 70.0



# 1.488 <-------Average dH@ DGM Outlet

(deg R)

524.0 525.5 526.5 CONVERSION FACTORS

1 mm Hg: 0.13330 kPa 1 em 

# = 0.39370 inch 1 mm 

## = 0.03937 inch 1 cu 

### ft 

### = 28.32 liters

DGM Ambient Overall Temp (deg R) (deg R)

524.5 528.0 526.3 529.0 527.0 530.0

### Temperature Meter Calibrations

Meter Box#: 

# 11 Date: 11/06/06 Calibrated By: RT Emtech 42312 

## Degrees F Calibrator Probe Stack Oven Exit Auxiliary

Point 1 32 31 31 32 31 31 Point 2 100 98 98 99 98 98 Point 3 250 250 250 251 250 250

Emtech 42312 

## Degrees R Calibrator Probe Stack Oven Exit Auxiliary

Point 1 492 491 491 492 491 491 Point 2 560 558 558 559 558 558 Point 3 710 710 710 711 710 710

Percent Difference Probe Stack Oven Exit Auxiliary Point 1 0.203252 0.203252 0 0.203252 0.203252 Point 2 0.357143 0.357143 0.178571 0.357143 0.357143 Point 3 0 0 0.140647 0 0

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# yrzJ I



# Pi tot tube/probe number**.~** 

# 0 meets or exceeds 

# all specifications 

# I 

# I

f 

## I 

# l
I 

# I

r 

# I 

# I 

# I I

criteria and/or applicable design features* and is**hereby~assigned** 

# a pitot tube calibration factor of**0.~4. ~** **;f~**

# S1gnat"Ur~

· Date

# ;o/tt/o~ - /(Lf/Ot-

- ' j!f YSee 

## •o**CF~** 

### 60, 

### Vol. 42, Ho. 160, 

### Method Z. Verify**~he** 

### minimum 2 inch**se:~ack** of the**~he~c~up1e** 

### and**t~e ~ini~** **3/~ ~n:h** **separa~ion bet;~een**  the ;>i tot tube and :he 

### nc::h as 

### shovn a: the**t~~** of this page. 

# 284

# 285

# NOZZLE INSPECTION AND MEASURfMENT DATA SHEET Company Name

# -D~c:::::(.~/...:...k~/.;_( e;:.._
__ "

___ Da,te Sampled ·Nozzle Number
Presample Inspection I 

# hereby certify that the ,above referenced nozzl'e appears to be round,**sharp-edg~d,** 

# free of nicks and dehts and for us e· at t 

# hi's t i 

# me · , 

# /7 ) 1 .. 

## 1 

# 7 

# L{ i

. ( 

# 1 ( Last Previously Measured Nozz 1

# e Area 

# o. ooo z..o9: ft2 .signature r 

## Date 

# Measured 

# t.obo 

# J (56 

# date 

# ;o/:l_o/r;o

Postsample**M~asurement** 

# Measure three diameters as shown; me.asurement is in fnches; record bel ovt; .'perform cal cul at ions. • 1 •• 

# tcr<..f Ave 

# rage· 0 

## i amet 

# er , 

# I 

# 9 

# f.....- '.: 

# Are··a = n 

# o2 4 X 

## 144 

# = • orJbz._

..

# ocr
This**are~·** 

# sha-ll · 

# e used in 

# Aata

# ~---·- 

# •' ./**.r~/~**

# '~/~ Siirlature-9

. 

# .. 2 Tt 

# reduction.**~Maximum** 

### allowable difference 

## betHe-eri 

### hrgest diameter and smallest 

## diameter. is 0.004 inches


# 286

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET
Company Name

.....

# ~~-·**-..~f-..~'+~...,;,t_/_("** ____ "

___ 

## D

a,t e 

# Samp 1

# ed 1 11

# /J 1)./o t:. · · -Nozzle Number

.. 

# J.l{:7 

# .3

I 

# Presample Inspection

Date

# Measured(O/)o~.( date

Postsample**M~asurement** 

# Measure three diameters as shown; measurement is in 

# i"nches; record belo\'1; 

# ·perform calculat;.ons

. ., 1• • L. 

# (_! ::;- 1/g 2.

. l., "-{ 

## Average· 

# Diameter

. l- 

# <f73 J '.: (I _. - 

# r.rea 

# = " D2 4 X 

## 144 

# This reduction.

• Haxi mum all

# owe~i ;-·;ifference 

## te- 

# I t\:leeri largest diaiileter and 

### sme1lest 

## f d1ameter is 0.004**i~** 

# 287

# Company 

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET
Name 

# D" 

# (/J(_ Da,te 

# Sampled. 

# /0/J// o6 .-· 

# Nozzle Number
..

# JoL!J.
Presample Inspection I hereby certify that the ,above referenced nozzle appears to be round, sharp-ed·g'ed, 'free of nicks and dents and is· judged zccetable for use· at t h

# i s t 

# i me . . 

# 3 

# a-z. , 

# J tJ '2... , 

# a j , Last Previo.usly

# Mea~J.Ired · 

# V**~~** Nozzle Area 

# .oo 0 

# '1'7'6 

# ft2 

# ignature ' Date Measured

# t.o/>1/6~ date

# 11/.JI/a~

Postsample**M~asurement** 

# Measure three 

# diameters as shown;**measurem~nt** 

# is i 

# n i'n c

# he s ; r e 

# cord 

# be 1Ovl ; ·

# p e r form c a 1 c u 1at i 

# on s . • 

# 1.**~)oZ..** 

## 2. , 

# )oz.. Average· Diameter

.. }o**~** 

# :3**--~~=~----------** 

# P.re·a = iT 

# o2 4 X 

## 144**~a-re-a-** 

# shall be**us~? ~data** 

.

# ~_/"

.

## ~ / 

# /'**~~{** ... ··:,. 

# signature 

# tJ.

. aate 

# II/ 

# c/o 6 2 

# ft
reduction

.



# ....,.-'**~Maximum** 

## allowable difference bet1-1eeri 

### 1arges 

### t di cme ter 

### and sme 

### 11 est 

## diameter. is 0.004 

## inches


# 288

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET Company 

# Name

# D~ 

# /f,**~~** Da.te Samp 1ed 

# .J 0 

# /1/.

. , · Nozzle Number 

# .grJ36-

Presample Inspection I hereby certify that the above referenced no-zzre appears to be round, sharp-ed·ged, free of nicks and dents and is.· judgedzacceRtable 

# for use· at this time. , 

# zs-J

.**z..~~ ~z;t'?**  

# . Last Previ o.usly Measured**·~** 

## Nozzle Areq

..

# oa:>~ 

# ft2 ' .signature ' R' · 

# Date Measured 

# to/JO/o ( date 

# /CJ

# I~!Jidt

Postsample Measurement 

# Measure three diameters as 

# shown; measurement is i 

# n i n

# ch

# e s ; r e c o r d 

# be 1ov1 ; · 

## p

# e r form c a 1 c u 1at i 

# on s . • 1.

_ 

# z.rr 2•• 

# -z,.)6 Ave 

## rage 

# Diameter , 

# Z.J-.5-3**~~~=~----------**

# Are~ = iT 

## o2 = •

# ~."~(..)'t**~** f

.... 

# l2 4 X 

## 144**~~:.o~{;** 

### JJ J


## //'his

# a;;/sh~. be

# u~e.~)'f1 data reduction.

# ~~::,_; signature 

# /1'
date 

# !1·/ 

# 6/o 6 0 

## ·-·*" :**Ma~imum** 

## allowable difference 

## be-**L~een** 

## largest diameter and smallest d1ameter is 

## 0.004 inches 

# 289

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET Company Name 

# \J 

# t6./ .z:j,. //""' '

- Da.te Sampled

. / 

# o/ J 

# 1/ d 

## f · · 

# ·Nozzle Number ./ 

# f,{
Presample Inspection I hereby certify that the .above referenced nozzl'e appears to be round, sharp-ed·g·ed, 'free of nicks and dents**a~d** 

# is· judged acceJpt'able for use· at thi"s time. ( 

# ¥7 /C"( ;' 

## (8 

# f-:'**~·** i 

# 4/

·**~** , , I 0 /**~** /**·.------·/;~·** 

## Last Previ qusly Measured ·

# >-d.~·- / 

# L::jt:/, Nozzle Areqa,c.W/¥7 ft2 · .signature '

. Date Measured 

# ;o/3!)/d. tr 

# date / 

# Cj'"lyt}Jjc;,/

Postsample**M~asurement** 

# Measure three. diameters as shO\,.rn;**me.asurem~nt** 

# is in**i~ches;** 

# record below;**·~erform** 

# calculations. 

# 1 . p 

# I**~6** 2. • 

# I ?")- 3. 

# ,f

# K'l-- Average· Diameter 

# _.:;...,_,..(_.k..._6

____ _**Are-~** = 7T 

# D2 4 X 

## 144 

# = 0

.. 000 {

# ~**~** .. 2 rt · 

# reduct ion. :r. I '""'

# \~~:::~3 \**·~~2./** ' .·

# -~-- 

# . I

"/·la:dmum 

### a11ovn:ble difference be- 

# I tHe-eri 

### l::r;est diatileter and smallest .l· 

### diatileter is 0.004 inches

. 

# 290'

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET i)

.. 

# f .,. ; 1: 

## Company 

# Name**~** 

# ; 

# {"C'**,-,~.** 

# Da,te Sampled 

# ;{jt,·/Q C

.. · ·Nozzle Number ., 

# 3/ 

# Z.?. 6

Presample Inspection I 

# hereby certify that the ,above referenced nozzl"e appears. to be round,**.sharr-~dg~~'** 

# ·free of nicks and**den~s** 

# and .is·

.. j.·udged**ac~.**

## table 

# for use at Lhls Llme.

# ,JfJ**J(! .J!~~-**  .. •

# !~

# /,

Last Previously Measured ·

# ~**~/{n)** Nozzle Areq ,ocJOS"' 

# J} ft2**~** 

# gnatu 

# e r / · , 

# Date Measured 

# lljt/o6. date 

# ///I/o 6
I •



# Postsample Measurement Measure three di.ameters as sh0\-1n; measurement is 

# in i'nches; record belov1; 

# ·perform calculations." 1 •• 

# J 

# I "3> 

# 2. I 

# 313 3. I 

# J/"L, Average 0 i 

# ameter
. J ( Z., 

# 9-**--~~=-------------** 

# = 7T 

## o2 4 X 

## 144 

# = . ooo.)]

# J**ft~** ..;._ 

# _____ _ reduction.

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET Company

# Name~"'_/ A_.



# _(t

____ ... ___ Da,te Sampled. II 

# /J

# /o.(

... ·Nozzle Number

__ 

# L_I__:_?

__ Presample Inspection I 

# hereby certify .that the above referenced nozzle appears to be round,**sharp-edg~d,** 

# free of nicks and dehts and is judged acceptable for use· at thi's time. , 

# ,_1 11**~ z.-/~** **~** l,

# 0 (. 

# r7**·~·** Last**Pr~viqusly** 

# Measured Nozz 1 e 

# Areq<

. · ft2 

# Date Measured .// 

# /J/o

. ..f 

# date 

# 1(/;/o f**~** .



# Postsample Measurement Measure three. diameters as sho\·m;**me.asurem~nt** 

## is 

# in i'nches; record belovt; 

# ·perform calculations. • 2 • I 

# Z,/ 

# tf 3.**I~~~** 

# Average 

# Diameter " 

# Z/**~ -----~~:~-----------------**  

# P.rera = 7i 

## D2 

# 0 0 ;¥'\,? 

# "'Z-**~** 2 

# 4 

# x 144 

# = ,**~~o** 

# rt · reduction.

..,·"" "" l·laxi:num

## alio~1abie differenc; be- 

### J 

### t•
..teeri 

### 1:rgest dia;neter c:nd

### sma11~st 

# Jf diameter is 0.004 inches

_ 

# 292

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET Company Name D:::::::_G-_/_.-_T._fc._, I,_,



### I-_.

_____ 

# Da.te Sampled 

# !1./z/46

... ·Nozzle Number I.Jtl.,;.3.


# Presample Inspection I hereby certify that the ,above referenced nozzle appears to be round,**sharp-ed9~d,** 

# free of nicks and dehts and is 

# judged acceptable for use· at thi's time. , 

# Jl'- 1 , 

## J/L/ , 

# J/)

# ~**~**


# . /2/**~.** 

# ' Last Previo.usly Measured

# ""'f[?f.-/~'6~ Nozzle Area**,~orJ ~**  

# ft2 

# .signature"· / Date Measured

# !1/?-/0~ date 

# 1//zJ'

Postsample Msasurement Measure three. di 

# arneters as shO\·m; measurement is 

# in inches; record below; perform calculati6ns. ¥ 

## 1•. 

# J ( 3 2.**~Jfl-** 

## 3•

# ----'t......~J~/--=l..:;___ 

# Ave rage D i 

# amet e r . 

# 3 (1.. )**~~-----------** 

# Area = ;r 

# o2

_**~3** ?

_ 

# 2 4 x 

## 144
-**~_ooo** 

# __ J

__

### ~- ___ 

## r 

## t 

# reduction.

·. ·-·*" :**Ha~imum al!o~~ble**  

### difference 

## be-**~~een l~rgest**  

### Glameter and**sm~11est** 

### diameter is 

### 0.004 inches 

# 293

# NOZZLE INSPECTION AND MEASUREMENT DATA SHEET Company Name 

# Q..,/;{/t ' Da.ie Sampled

. .

# !/ J

. o(

.. · 

## Nozzle Number 

# ;2/7] .6-**~~----------------** 

# '
Presample Inspection I hereby certify ·that the .above referenced nozzl·e appears to be round,**sharp-edg~d,** 

# free of nicks and dehts and is 

# jUdged acceptable for use· at thi's**t~me.** 

# , 

# t-1 

# 1 1 

# Z.../1 1 

## L.l. o - ;/ 

## Last Previously Measured :;;:: .// 

# _Nv

. Nozzle Area o,cOCJ 

## Z 

## o?., 

# ft2 .signature 

# '7 Date Measured I)/ 

# .J/t1 1

. 

# date 

# /1/;J/oo

Postsample Measurement Measure three diameters as 

# sho\"'n; measurement is i 

# n i'n c h e s ; r e cord be 1Ovl ; 

## p

# e r form c ai 

# c u 1at i 

# on s . .. 1•**~** 

# Z...l -, 2.**~** 

# L/1 3

.. 

# z,z. 0 

# Averdge Diameter 6 

## "b(Cf3**--~,-,**

# ------------ " > 

# r.rea = 71' 

# o2 4 X 

## 144

/ 

# 2 

# ft

. data reduction.

date 

# 11//**~joe** * Haxirnum allowable difference betweeri largest diameter and 

## smell!st diameter is 0.004**i~ches** 

# 294

### . i

I

I**·~**


# App.en:dix F ·I**~** 'I 

### j 

# I

:,

# Specialty Gas Products

Date: 6/27/2005 Customer: Trigas Description: CO in N2- EPA Protocol Cylinder**No~** 

### EB0000701 

## Component Carbon Monoxide ' Nitrogen, Balance



## Reference Standard Description NTRM 

## Instrumentation Description Horiba Process Analyzer 31 06 Pasadena Freeway Pasadena,Texas77503 ·(713) 534-8217 Fax(713) 534-8133



## Requested Concentration 50 ppm



## Expiration date 5/29/2006


## Model# VIA-510-CO Project: 16017 Exp. Date: 6/27/2008 Cylinder Pressure: 1900psig 

## Certified Concentration·. 49.9 ppm



## Cylinder Number SX19190


## Date Last Clibrated 6/10/2005 

## Anaylsis Results: Z =zero gas, S =standard gas, X= 

## sample gas First Triad
- CO Z1= -0.90 S2= 204.80 Z3= -0.80 S1= 204.90 Z2= -0.80 X3= 198.60 Y=0.28607+0.250309*X Average= 49.94ppm



## nalyst: _/-'

-- ...- 

# .------=::::**~** X1= 198.70 .X2= 198.60 S3= 204.90 

## Second Triad
- CO Z1= -0.40 S2= 513.20 Z3= -0.40 S1= 513.30 Z2= -0.40 X3= 496.90 Y=0.031 031 +0.1 00163*X Average= 49.82ppm 

## Accuracy 1%



## Concentration 994.2 ppm CO 

## Principle NDIR

X1= 497.10 X2= 497.10 S3= 513.20

fHIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 1 

## 0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 295;..



# Specialty Gas Products**~,.**



### .Date: 6/2712005 Customer: Trigas Description: CO in N2- EPA Protocol Cylinder No: EB0000761 

## Component Carbon Monoxide Nitrogen. Balance



## Reference Standard DescriPtion NTRM 

## Instrumentation Description Horiba Process Analyzer 31**0~ p~sadena**  

### Freeway Pasadena.Texas77503 (713) 534-8217 Fax(713) 534-8133



## Requested Concentration 100 ppm



## Expiration date 5/29/2006


## Model# VIA-510-CO Project: 16018 Exp. Date: 6/27/2008 Cylinder Pressure: 1900psig 

## Certified

.Concentration 99.1 ppm



## Cylinder Number SX19190


## Date Last Clibrated 6/10/2005 

## Anaylsis Results: Z =zero gas, S = standard gas, X= 

## sample gas First Triad
- CO Z1 = -0.90 S2= 204.80 Z3= -0.80 S1= 204.90 Z2= -0.80 X3= 396.50 Y=0.28607+0.250309*X Average = 99.45ppm X1 = 396.60 X2= 396.60 S3= 204.90

/'·

- ----=:_

# Analys~-z?~-**~** Second Triad
- CO Z1= -0.40 S2= 513.20 Z3= -0.40 S1= 51"3.30 Z2= -0.40 X3= 985.20 Y=0.031031 +0.100163*X Average = 98.74ppm 

## Accuracy 1%



## Concentration 994.2 ppm 

# co Principle NDIR



### X1= 985.70 X2= 985.40 S3= 513.20

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 296

# Specialty 

# Gas Products

Date: 8/16/2004 Customer. Matheson- Trigas Description: CO, 02 in N2- EPA Protocol Cylinder No: CC187154 3106 Pasadena Freeway Pasadena,Texas77503 (713) 534-8217 Fax(713) 534-8133

Project: 1 0548 Exp. Date: 8/162007 Cylinder Pressure: 1900psig 

### Component Carbon Monoxide Nitrogen, Balance 

### Requested Concentration Certified 

### Concentration 200ppm 200ppm
Rete·rence Standard 

### Accuracy 1%



### Description Expiration date Cylinder Number CC177636 

### Concentration GMIS 

### 4/6/2096 Instrumentation 

### Description Model# Horiba Process Analyzer VIA-510-CO Anaylsis Results: Z = zero gas, S = standard gas, X = sample gas 

### First Triad
- CO Z1= -0.3 S2= 993.20 Z3= -0.30 51= 993.5 Z2= -0.30 X3= 199.90 Curve: Y=-0.6893+1.001139X Average =199.6ppm

Analyst: 

# L-- .-,**_,~' ~**  Ling Wen_...--- X1= 199.9 X2= 200.00 S3= 993.00 

### Date Last Clibrated 8/6/2004



### Second Triad
- CO Z1= -0.4 51= 995.5 S2= 995.80 Z2= -0.30 Z3= -0.30 X3= 200.60 Average= 199.8ppm Principle NDIR

X1= 200.6 X2= 200.60 S3= 995.60

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 297

# Specialty Gas Products

Date: 3/22/2005 Customer: Trigas 3106 Pasadena**Fr~way** 

### Pasadena, Texas 77503 (713) 534-8217 Fax(713} 534-8133

Project 14445 Description: Methane in Air- EPA Protocol Exp. Date: 3/22/2008 Cylinder Pressure: 1950psig Cylinder No: SX31814 Component Methane Air, Balance

Reference Standard Description SRM Instrumentation Description Horiba Process Analyzer Requested Concentration 20 ppm

Expiration date 6/1/2008
Model# FIA-510 Anaylsis Results: 

## Z =zero gas, 

## 5 =standard gas, X= sample gas 

## Fl,rst Triad
- Methane Z1 = 1.60 S1 = 492.30 S2= 492.70 Z2= -0.10 Z3= -0.70 · X3= 199.50 Curve: Y=-0.09706+0.099752*X Average = 19.87pm X1= 199.70 X2= 198.60 S3= 490.40 

# // /-' ,/ 

### tl.nalyst: 

# ;t'::;.:::

..

# ;;.~·-::;Z~~·/**~** 

### Certified Concentration 19.9 ppm

Cylinder Number FF23319
Date Last Clibrated 3/21/2005 Accuracy 1%

Concentration 49.22 ppm Methane Principle FIA

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

## )0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# 298

# MATHESON TRI•GAS ask

... The Gas 

### Professionals

..... 

# Certificate of Analysis

- EPA 

# Protocol Mixtures

Customer: MATHESON TRI-GAS- DALLAS ::ylinder Number: SX-32759 Cylinder pressure: l_ast Analysis date: ::xpiration Date: 2000 5/3/2005 5/3/08 Protocol: G1 Reference# 329498 1650 Enterprise Parkway Twinsburg, Ohio 44087 21 S-648-4000

Lot# 

### 109-56-43191



## REPLICATE RESPONSES 

## Date: Component : Methane Certified Cone: 40.8 PPM± 1% REL

3ALANCE GAS: Air

# ~EFERENCE STANDARDS

# "·>~; Component:

# Methane.::..;;~{ SRM #: 

## SRM-27so,i1 Cylinder#: SX-20007 Concentration: 48.80 pp.m

_ .... :.'<; ·-:.

### ..:.-·



## Measurement Principle: TC, FlO Last Calibration: 4/26/2005

Notes: :-.. ·

### .....

........ --":>.. ••-·· 

# :-**;~ii';~~~::~tili1~J>"**

- 

### ...... ·;· 

## 5/3/2005 40.8 PPM 40.8 PPM 40.7 PPM ·"

....... 

## Date:

This certification was performed according to EPA Traceability Protocol for Assay & 

## Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2

.

. nalyst

____ 

# f**A_:___,~y_·_D_._~--~-~---------** Date

## ----=-5/~4'-'-=/2,...0.....,.;0-=-5


# 299

# MATHESON TR&•GAS ask

... The Gas Professionals"• 

# Certificate of Analysis

.. EPA Protocol Mixtures

Customer: MATHESON TRI-GAS

- DALLAS Protocol: :ylinder Number: SX-34951 G1 Cylinder pressure: 2000 Last Analysis date: 5/3/2005 =xpiration Date: 5/3/08 Reference# 329498 1650 Enterprise Parkway 

### Twinsburg, Ohio 44087 21 5-648-4000

Lot# 109-56-43192



### REPLICATE RESPONSES


### Component : Methane Certified Cone: 61.7 PPM 

# ± 1

## °/o REL

IALANCE GAS: Air

!EFERENCE STANDARDS ,._ Component:

# MethaneL:'~J SRM #: SRM-2750 5 

### Cylinder 

## #: SX-20007 Concentration: 48.80 ppm**·~:~~·~**

# ERTIFICATI~::~~:::r~::~n;~:;J:~~T~~f Serial Number: LR-92489 .··**.~!~·:~** 

# .. : Measurement Principle: TC, FlO /)''

..,.p···· 

### Date:

Last Calibration: 4/26/2005 :' ):**-~~~** 

### .. -,**:--~ ~-:.~**  ......**~~-;1 -~** 

.

### ~ .... 

## ·
........... ·

### ·~~.. .

### ;~**~···~·** 

### Notes: 

### 5/3/2005 61.7 PPM 61.8 PPM .•:61.5 PPM
o-:• 

### Date:

rhis certification was performed according to EPA Traceability Protocol for Assay 

## & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.

alyst.

____

# .!.._/~_ ... 4 ·

# ;?~·_}>._._ ..

# ~---=-=-k- 

# ___________ _ Date

## ---~51--!.4~12~0~0~5


# 300'

# MATHESON TRI·GAS® ask

... The Gas Professionals 

## Certificate of Analysis
- EPA Protocol Mixtures

Customer: Protocol: Reference# Cylinder Number: G1 3106 Pasadena Freeway Pasadena, TX 77503 713-534-8217



## Lot# 25738-02 Cylinder Pressure: MTG-CALI SX39223 1900 PSIG 10/.16/2006 DO NOT -USE THIS CYLINDER WHEN THE PRESSURE FALLS BELOW. 

## Last Analysis Date: 

## · · · · · .**-~··.** 

## .**ts~ esf~.**  

# ···· · . . · ·.·

..... 1·:··,..

. •' 

## Expiration Date: 10/16/2008

.. 

## REPLICATE RESPONSES Component: Nitric Oxide Date: 10/9/2006 24.87 24.77 24.85 Mean Cone: 24.9 ppm 

## +/- 1% rei BALANCE GAS:
REFERENCE STANDARDS: CompGnent: Reference Standard: Cylinder#: Concentration: Nitrogen

Nitric Oxide GMIS ND22477 48.8 ppm Ex·p: ·Date: 2/15/2008 CERTIFICATION INSTRUMENTS Component: Make/Model: Serial Number: 1easurement Principle: Last Calibration:

Notes: Nitric Oxide Horiba CLA-51 OSS 42312910013 Chemiluminescence 9/29/2006 NOx: 25.0 

# ppm Date: 10/16/2006 24.84 24.95 24.95

This Certification was performed according to EPA Traceability Protocol for Assay 

## & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.

# Anal~st:**h~** 

# ....._ Date: ( 

# <:>/r 6

# /.z-...--ue;**~~ ~~~--~---------**  

## Manufactured 

## By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.

# Specialty Gas Products

Date: 6/27/2005 Customer: Matheson- Trigas Description: NO in N2- EPA Protocol Cylinder No: EB0001164 Component Nitric Oxide Nitrogen, Balance
Reference Standard Description GMIS 

## Instrumentation Description Horiba Process Analyzer Requested Concentration 50 ppm

Expiration date 11/22/2006
Model# CLA-510-NO 31 06 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713} 534-8133

Project: 16015 Exp. Date: 6/27/2007 Cylinder Pressure: 1900psig Certified Concentration 50.4 ppm
NOx: 51 ppm Cylinder Number ND22557
Date Last Clibrated 6/16/2005 Accuracy 1%



## Concentration 99.8 PPM no Principle CHEMI 

## Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas
First Triad
- NO 

## Z1= -1.20 S2= 994.10 Z3= -1.10 51=. 994.80 Z2= -1.30 X3= 499.80 Average= 50.3ppm Curve: Y 

# = 0.33645 + 0.099857*X X1= 498.30 X2= 498.40 53= 997.40 Second Triad
- NO Z1= -1.10 S2= 998.20 Z3= -0.80 51= 998.50 Z2= -0.70 X3= 500.80 Average= 50.53ppm X1= 502.80 X2= 502.40 S3= 994.20

# MATHESON TRI·GAS 0 

### 3106 Pasadena Freeway Pasadena, TX 77503 

### 713-534-8217 

### ask

... The Gas Professionals 

## Certificate of**~nalysis** 

## - EPA Protocol Mixtures

Customer: Cylinder Number: MTG-Cali Crossing CC176977. Cylinder Pressure: 1900 PSIG Last Analysis Date: 2/13/2006 Expiration Date: 2/13/2008
Component: Sulfur Dioxide Date: Mean Cone: 49.8 ppm 

## +/- 1% rei BALANCE GAS: Nitrogen
REFERENCE STANDARDS: Component: Sulfur**Dio~ide** 

## Reference Standard: GMIS Cylinder#: CC 177775 Concentration: 101.3 ppm Exp. Date: 9/4/2006

. CERTIFICATION INSTRUMENT$ Component: Make/Model: Serial Number: Measurement Principle: Last Calibration:
Notes: Sulfur Dioxide Horiba VIA-51 0 42321590023 NDIR 2/7/2006 Protocol: Reference# G1

REPLICATE RESPONSES
2/6/2006 49.44 49.65 49.78 Date: 2/13/2006 50.22 49.91 49.88 Lot# 20832

This Certification was performed according to EPA Traceability Protocol for Assay 

## & Certification of Gaseous Calibration Standards September 1997, using procedure G 1 and/or G2. Analyst:

# ~ ::::::.. Date: 

# ?:1!_9**1~0** 7'

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## Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 303

# MATHESON TRI·GAS® 3106 Pasadena Freeway**Pasadena~** 

### TX 77503 713-534-8217 

### ask

...The Gas Professionals 

## Certificate ofAnalysis -EPA Protocol Mixtures·

Customer: Cylinder Number: Cylinder Pressure: Last Analysis Date: Expiration Date: MTG-CALI CROSSING EB0000352 1900 PSIG 10/16/2006 1**0/16/2008'·~·**


## Component: Sulfur Dioxide Date: Mean Cone: 50.1 ppm +/- 

## 1% rei BALANCE GAS: Nitrogen
REFERENCE STANDARDS: Component: Sulfur Dioxide Reference Standard: GMIS Cylinder#: CC 177775

· Concentration: 99.6 ppm Exp. Date: 9/26/2008 CERTIFICATION INSTRUMENTS Component: Make/Model: Serial Number: Measurement Principle: Last Calibration:
Notes: Sulfur Dioxide Horiba VIA-510 42321590023 NDIR 9/26/2006 Protocol: Reference# 

## G1

.. !.·,·

... 

## REPliCATE RESPONSES
10/9/2006 50.07 50.10 50.18 Date: 10/16/2006 50.16 50.20 50.13 Lot# 25738-01

This Certification was performed according to EPA Traceability Protocol for Assay 

## & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.

# Analyst:.~ Date:

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 304

# MATHESON TRI·GAS® 3106 Pasadena Freeway Pasadena, TX 77503 713-534-8217 

## ask

... The Gas Professionals 

## Certificate of 

## Analysis -EPA Protocol Mixtures

Customer: Cylinder Number: Cylinder Pressure: Last Analysis Date: Expiration Date: MTG-Cali Crossing CC177031 1900 PSIG 2/13/2006 2/13/2008
Component: Sulfur Dioxide Date: Mean Cone: 100 ppm 

## +/- 1% rei BALANCE GAS: Nitrogen


## REFERENCE STANDARDS: Component: Sulfur Dioxide Reference Standard: GMIS Cylinder#: ND22558 Concentration: 502.1 ppm Exp. Date: 9/4/2006 

## CERTIFICATION INSTRUMENTS Component: Make/Model: Serial Number: Measurement Principle: Last Calibration:
Notes: Sulfur Dioxide Horiba VIA-510 42321590023 NDIR 1/16/2006 Protocol: Reference# G1



## REPLICATE RESPONSES
2/6/2006 100.60 100.30 100.30 Date: 2/13/2006 100.30 100.10 100.10 Lot# 20829

This Certification was performed according to EPA Traceability Protocol for Assay 

## & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2. 

## Analyst

# ~ ..., Date: 

# ?;/!.])?-:!:de

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 305