Exhaust Emissions Sampling 

Dal-Italia, Muskogee, OK 

Six Emission Sources 

October 30- November 3, 2006 

Ar~strong Environmental, Inc. 

Project W .. 2516-06 

Report Prepared For: 

Bob Hurt 

Daltile 

7834 C.F. Hawn Freeway 

Dallas, TX 7 521 7 

Report Prepared November 8, 2006 By: 

Armstrong Environmental~ Inc. 

17 48 Hlavek Rd. 

Decatur, Texas 76234 

(214) 631-0021 
I. Introduction 

II. Summary 

ID. Procedures 

IV. Appendices 

TABLE OF CONTENTS 

A. Calculation Summaries 

B. Continuous Emissions Monitor Summaries 

C. Analytical Summaries 

D. Field Data Sheets 

E. Equipment Calibrations 

F. Standard Gas Certifications 

Page 

1 

2- 13 

14-23 

24-50 

51- 139 

140- 240 

241 -273 

274-294 

295- 305 
SUMMARY OF EMISSIONS TEST DATA 

Table: 1 

Plant : Dal-ltalia, Muskogee, OK 

Location : Glaze Line Baghouse (EPN 41) 

Operator : R. Taylor 

Test Date : 30-0ct-06 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 85.5 86.3 87.3 

Velocity, fps 60.58 59.05 59.96 

Volume Flow, acfm 21589.9 21045.3 21366.5 

scfm 19996.5 19461.1 19818.3 

seth 1199793 1167666 1189095 

Moisture,% 2.39% 2.41% 1.94% - C02,% 0.00 0.00 0.00 

02,% 21.00 21.00 21.00 

SAMPLE 

Start Time, hrs:min 10:20 AM 11:40 AM 12:57 PM 

Finish Time, hrs:min 11:23 AM 12:43 PM 2:00PM 

Sample Volume, set 42.365 41.220 41.725 

lsokinetic Ratio, % 101.1859 101.1609 100.5536 

PARTICULATE 

Front Half 

Sample Weight, mg 10.01 7.16 7.61 

Concentration, gr /scf 0.003646 0.00268 0.002814 

Emissions, lbs/hr 0.625093 0.44723 0.478208 

Back Half 

Sample Weight, mg 18.85 22.15 6.40 

Concentration, gr /set 0.006866 0.008291 0.002367 

Emissions, lbs/hr 1.177123 1.383538 0.402172 

Total Particulate, lbs/hr 1.802215 1.830768 0.88038 
SUMMARY OF EMISSIONS TEST DATA 

Table: 2 

Plant: Dal-ltalia, Muskogee, OK 

Location : Press Baghouse (EPN 40) 

Operator: T. Armstrong, G. Salinas 

Test Date: 30·0ct·06 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 86.6 87.8 88.8 

Velocity, fps 37.15 36.51 36.52 

Volume Flow, acfm 18491.6 18172.4 18179.5 

scfm 17152.9 16786.3 16659.7 

seth 1029174 1007181 999579 

Moisture,% 2.03% 2.22% 2.82% 

C02,% 0.00 0.00 0.00 

02,% 21.00 21.00 21.00 

SAMPLE 

Start Time, hrs:min 10:00 AM 11:25 AM 12:47 PM 

Finish Time, hrs:min 11:02 AM 12:27 PM 1:49PM 

Sample Volume, scf 42.600 41.539 41.400 

lsokinetic Ratio, % 103.0065 102.6355 103.0697 

PARTICULATE 

Front Half 

Sample Weight, mg 9.51 9.35 7.86 

Concentration, gr /set 0.003445 0.003473 0.002929 

Emissions, lbs/hr 0.506603 0.499881 0.418451 

Back Half 

Sample Weight, mg 4.35 3.10 2.40 

Concentration, gr/scf 0.001576 0.001152 0.000894 

Emissions, lbs/hr 0.231727 0.165736 0.127771 

Total Particulate, lbs/hr 0.738331 0.665617 0.546222 
SUMMARY OF EMISSIONS TEST DATA 

Table: 6 

Plant : Dal-ltalia, Muskogee, OK 

Location : Phase II Scrubber Exhaust (EPN 29) 

Operator: R. Taylor, G. Salinas, T. Armstrong 

Test Date : 2·NOV·06 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 127.6 128.7 128.9 

Velocity, tps 24.42 24.10 23.66 

Volume Flow, acfm 42002.5 41458.6 40705.1 

sctm 32589.9 31921.4 31479.1 

seth 1955395 1915282 1888747 

Moisture,% 14.32% 14.67% 14.42% 

C02,% 3.00 3.00 3.00 

02,% 17.00 17.00 17.00 

SAMPLE 

Start Time, hrs:min 9:15AM 10:40 AM 12:10 PM 

Finish Time, hrs:min 10:18 AM 11:43 AM 1:13PM 

Sample Volume, set 36.525 35.748 35.211 

lsokinetic Ratio, % 100.4746 100.39"47 100.2762 

CARBON MONOXIDE 

Concentration, ppm 89.57 132.24 126.6 

Emissions, lbs/hr 12.73118 18.41058 17.38118 

NITROGEN OXIDE AS N02 

Concentration, ppm 22.02 22.75 23.02 

Emissions, lbs/hr 5.141896 5.203383 5.19219 

VOC AS Methane 

Concentration, ppm as CH4, WET 30.85 28.25 26.88 

Concentration, ppm as CH4, DRY 36.00637 33.10801 31.4076 

Emissions as CH4, lbs/hr 2.924472 2.633902 2.464008 

Emissions as C3H8, lbs/hr 2.680864 2.414498 2.258756 

Emissions as C, lbs/hr 2.193354 1.975426 1.848006 

SULFUR DIOXIDE 

Concentration, ppm 0.116 0 0.123 

Emissions, lbs/hr 0.037687 0 0.038599 

HYDROGEN FLUORIDE 

Sample Weight, mg 0.00 0.00 0.00 

Concentration, ppm 0 0 0 

Emissions, lbs/hr 0 0 0 

CHLORINE 

Sample Weight, mg 0.00 0.00 0.00 

Concentration, ppm 0 0 0 

Emissions, lbs/hr 0 0 0 

HYDROGEN CHLORIDE 

Sample Weight, mg 0.00 0.00 0.39 

Concentration, ppm 0 0 0.254441 

Emissions, lbs/hr 0 0 0.045537 

IO 
SUMMARY OF EMISSIONS TEST DATA 

Table: 7 

Plant: Dal·ltalia, Muskogee, OK 

Location : Phase II Scrubber Exhaust (EPN 29) 

Operator : R. Taylor, G. Salinas 

Test Date : 2-Nov-06 

Repetition : 

STACK GAS 

Temperature, F 

Velocity, fps 

Volume Flow, acfm 

Moisture,% 

C02,% 

02,% 

SAMPLE 

scfm 

seth 

Start Time, hrs:min 

Finish Time, hrs:min 

Sample Volume, scf 

lsokinetic Ratio, % 

~ 

~ ARTlCU LATE 

Sample Weight, mg 

Concentration, gr/scf 

Emissions, lbs/hr 

Back Half 

Sample Weight, mg 

Concentration, gr /scf 

Emissions, lbs/hr 

Total Particulate, lbs/hr 

4 

129.3 

24.67 

42426.7 

31520.9 

1891253 

14.91% 

3.00 

17.00 

1:40PM 

2:43PM 

34.773 

99.15317 

35.38 

0.015699 

4.242949 

10.20 

0.004526 

1.223236 

5.466185 

n 

5 

128.6 

23.36 

40187.1 

31116.5 

1866992 

14.35% 

3.00 

17.00 

3:05PM 

4:08PM 

34.339 

99.18727 

23.36 

0.010497 

2.800-:183 

11.50 

0.005167 

1.378662 

4.179145 

6 

129.5 

23.93 

41166.6 

31996.8 

1919807 

13.89% 

3.00 

17.00 

4:30PM 

5:33PM 

35.506 

99.73715 

29.93 

0.013007 

3.56?332 

14.29 

0.00621 

1. 703691 

5.272023 
III. PROCEDURES 

The procedure for emissions sampling followed USEP A test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method Title 

1 

2 

3 

4 

5 

6C 

7E 

10 

25A 

26A 

202 

Sample and Velocity Traverses for Stationary Sources 

Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

Gas Analysis for the Determination of Dry Molecular Weight 

Determination of Moisture Content in Stack Gas 

Determination of Particulate Emissions from Stationary Sources 

Determination of Sulfur Dioxide Emissions from Stationary Sources 

(Instrumental Allalyzer Procedure) 

Determination of Nitrogen Oxides Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

Determination of Carbon Monoxide Emissions from Stationary Sources 

Determination of Total Gaseous Organic Concentration using a Flame 

Ionization Analyzer 

Determination of Hydrogen Halides and Halogens Emissions from 

Stationary Sources 

Determination of Condensible Particulate Emissions from Stationary 

Sources 

02 and C02 were determined using PyRite Analyzers. 

PM. HF and HCI sampling was perfonned on each source according to the following: 

EPN 40 20 3 60 minutes 

EPN 36 24 2.5 60 minutes 

EPN 29 24 2.5 60 minutes 

EPN 35 8 7.5 60 minutes 

EPN 30 8 7.5 60 minutes 

14 
Source geometry's are shown in Figures 1 - 6. 

The HF, HCl, and CL2 sampling train was configures as follows: 

Glass Sampling Nozzle 

Heated Glass Lined Probe 

Heated teflon filter 

lmpinger #1 - 100 mls 0.1 N H2S04 

Impinger #2 - 100 mls 0.1 N H2S04 

Impinger#3 -lOOmis 0.1 NNaOH 

Impinger#4- 100 mls 0.1 N NaOH 

Impinger #5 - 200 grams silica Gel 

Analysis was performed for HF and HCI on the solution from the 1st and 2nd impingers. 

Analysis for Cl2 was performed on the solution from the 3rd and 4th impingers. 

The PM sampling train was configured as follows: 

Stainless Sfeel Sampling Nozzle 

Heated Glass Lined Probe 

Heated Glass Fiber Filter 

Impinger #1- 100 mls H20 

Impinger #2 - 100 mls H20 

lmpinger #3 - 100 mls H20 

lmpinger #4 - Empty 

Impinger #5 200 grams silica gel 

PM analysis was performed on the probe wash, filter, impinger solutions, and the MeCI 

rinse and impinger extraction's. 

Continuous emissions were monitored for the Spray Dryer and Vertical Dryer as follows: 

Fuji 3300 CO analyzer 0- 100 

EcoPhysics 70S Nox Analyzer 0-60 

0- 100 

ThermoEnvironmental 51 FID 0- 100 

:. '·'· •'' 

49.9 ppm, 99.1 ppm CO in N2 

EPA Protocol 1 

25 ppm, 51.0 ppm Nox in N2 

EPA Protocol 1 

49.8 ppm, 50.1 ppm, 100 ppm 

802 in N2 EPA Protocol 1 

19.9 ppm, 40.8 ppm, and 67.1 

CH4 in Air EPA Protocol I 

Continuous emissions were monitored for the Kiln Scrubber as follows: 
Fuji 3300 CO analyzer 0-200 

EcoPhysics 70S Nox Analyzer 0-60 

0- 100 

0- 100 

A schematic of CEM configuration is shown in Figure 6. 

200 ppm, 99.1 ppm CO in N2 

EPA Protocol 1 

25 ppm, 51.0 ppm Nox in N2 

EPA Protocol I 

49.8 ppm, 100 ppm S02 in N2 

EPA Protocol 1 

19.9 ppm, 40.8 ppm, and 61.7 

CH4 in Air EPA Protocol! 
Figure·1- Glaze Line Baghouse (EPN 41) 

580 inches 

0 

126 inches 

stack Diameter - 33 inches 

Point #1 - 1 inches 

Point #2 - 2.2 inches 

Point #3 - 3.4 inches 

Point #4 - 5.8 inches 

Point #5 - 8.25 inches 

Point #6 -11 .7 Inches 

Point #7 - 212 inches 

Point #8- 24.751nches 

Point #9 - 27.2 inches 

Point #1 0 - 29.1 inches 

Point #11 - 30.8 inches 

Point #12 - 32 inches 
Figure 2- Press Baghouse (EPN 40) 

180 inches 

0 

204inches 

stack Diameter - 39 inches 

Point #1 - 1 .0 inches 

Point #2 - 2.4 inches 

Point #3 - 5.7 inches 

Point #4 - 8.8 inches 

Point #5 - 13.3 inches 

Point #5- 25.71nches 

Point #7 - 30.2 Inches 

Point #8 - 33.3 inches 

Point #9 - 35.8 inches 

Point #1 o - 38 inches 
Figure 5 - Scrubber Exhaust (EPN 29) 

,, 

' 

88inches 

·t43inches 

~·--~-- ----··--------

stack Daimeter - 72.5 inches 

Point #1 - 1 .5 inches 

Point #2 - 4.9 inches 

Point #3 - 8.5 inches 

Point #4 - 12.8 inches 

Point #5 -18.1 inches 

Point #6 - 25.8 inches 

Point #7- 46.7 inches 

Point #8- 54.4 inches 

Point #9- 59.7 inches 

Point #1 0 - 63.9 inches 

Point #11 - 67.6 inches 

Point #12- 71.inches 
1\) 

1\) 

Figure 6- Vertical Tile Dryer #7 (EPN 30) 

46inches 

150 inches 

stack Diameter - 17 inches 

Point #1 - 1 .1 inches 

Point #2 - 4.25 inches 

Point #3 - 12.75 inches 

Point #4 - 15.9 inches 
\) 

..N 

Figure 7 - GEM Configuration 

I nstack Filter. Heated Probe 

Heated 

Sample Line 

Pump 

8 ias Calibration Span Line 

FID Analyzer 

' 

Heated Manifold I L-------.l 

Sample 

Processor 

...... 1--

co Analyzer "-~-... 

r- ~ 

NOx Analyzer I-~-. 

...... 

S02 Analyzer ~~-

Flowmeter 

Cafibration Point 

Sample processor consists of two short stem impingers followed by a 0.3 

Pump micron filter 
. -; . 

.. ·. 

•I -1 0 ', ~, 0 

::t;: 

. I:, . ,, ·-

1 ...... 

~ i::. ; . '. :< 

·c-:·-, J.·. 

t.~ • 

·.,·, 

l'r•.'• 

, .. 

•. t·· 

"-=. •• :,, __ 

.··.• I. • 

Appendix'·)\. .. . ', :. ~ . , ' 

:- :: . ~· : \ .. · ... : ··--

·.·· .. _1 • 

,I •' 

.; .:;·: 

L. ~· ~- .... 

'·,.' 

. ·.'· ·;· .. ' ..... .. ;.:-

. • ···. 
EMISSION TEST SUMMARY 

PLANT: Dal-ltalia. MuskoRee. OK 

DATE: 30-0ct-06 

PLACE: Glaze Line BaRhouse (EPN 41) 

RUN#: 1 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 22 

NOZZLE DIAMETER {INCH.): 0.195 PARTICULATE WEIGHT (Front half mg): 10.01 

METER COEFFICIENT (Y) : 0.972 PARTICULATE WEIGHT (Back half mg): 18.85 

PI TOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): ·027 

GAS METER VOL.(Cu.Ft.) : 45.194 PERCENT C02 0 

BAROMETRIC PRESSURE 29.35 PERCENT 02 21 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 33 STACK LENGTH(inchs): 

STACK AREA (SQ.Ft.) : 5.939574 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000207 STACK AREA (SQ. Ft.): 0 

ENTER THE STACK AREA SHOWN ABOVE: 5.939574 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 42.3647 

VOLUME OF WATER VAPOR (STD. CU.FT.): 1.0355 

FRACTIONAL MOISTURE CONTENT(%): 0.0239 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.5814 

STACK PRESSURE (inch Hg): 29.3301 

STACK,GAS VELOCITY (ft/sec.): 60.5821 

ACTUAL STACK GAS FLOW RATE (ACFM): 21589.9223 

STANDARD STACK GAS FLOW RATE (SCFH): 1199792.54 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0036 

PARTICULATE CONCENTRATION (LBS/SCF): 5.21E·07 

PARTICULATE EMISSION (LBS/HR): 0.6251 

BACK HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 0.0069 

PARTICULATE CONCENTRATION (LBS/SCF): 9.81E·07 

PARTICULATE EMISSION (LBS/HR): 1.1771 

ISOKINETIC RATIO(%): 101.1859 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METERT. METER T. 

deg F INLET OUTLET 

1 85 0.85 0.921954 1.10 70 70 

2 85 0.86 0.927362 1.10 73 70 

3 85 0.90 0.948683 1.20 75 71 

4 85 0.85 0.921954 1.10 76 71 

5 85 0.90 0.948683 1.20 78 71 

6 85 0.95 0.974679 1.30 80 72 7 85 1.00 1 1.30 81 72 

8 85 1.10 1.048809 1.40 83 73 

9 85 1.30 1.140175 1.70 84 74 

10 85 1.40 1.183216 1.90 85 74 ll 85 1.20 1.095445 1.60 85 74 12 85 l.lO 1.048809 1.50 85 74 

13 86 1.40 1.183216 1.90 83 74 14 86 1.50 1.224745 2.00 85 75 15 86 1.50 1.224745 2.00 86 75 16 86 1.50 1.224745 2.00 87 76 17 86 1.30 1.140175 1.70 87 77 

18 86 1.20 1.095445 1.60 87 77 

19 86 0.93 0.964365 1.20 88 77 

20 86 0.92 0.959166 1.20 88 77 21 86 0.97 0.984886 1.30 89 77 22 86 1.00 1 1.30 89 77 

23 86 1.00 1 1.30 88 77 METER T. 24 86 0.88 0.938083 1.20 sa 78 AVERAGE 

85.5 1.0458 1.4625 83.3333 74.2917 78.8125 

?4 
EMISSION TEST SUMMARY 

PLANT: Dal·ltalia, Muskonee, OK 

DATE: 30·0Cf·06 

PLACE: Glaze Line BaRhouse {EPN 41) 

RUN#: 2 

TEST DURATION {MINUTES): 60 LIQUID COLLECTED (mls) : 21.6 

NOZZLE DIAMETER (INCH.): 0.195 PARTICULATE WEIGHT (Front half mg): 7.16 

METER COEFFICIENT (Y) : 0.972 PARTICULATE WEIGHT (Back half mg): 22.15 

PilOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): ·0.21 

GAS METER VOL.(Cu.Ft.) : 44.328 PERCENT C02 0 

BAROMETRIC PRESSURE 29.35 PERCENT 02 21 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 33 STACK LENGTH(inches): 

STACK AREA (Sq.Ft.) : 5.939574 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000207 STACK AREA (Sq.Ft.): 0 

ENTER THE STACK AREA SHOWN ABOVE: 5.939574 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 41.2202 

VOLUME OF WATER VAPOR (STD. CU. FT.): 1.0167 

FRACTIONAL MOISTURE CONTENT (%): 0.0241 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 

MOLECULARWT. OF STACK GAS (WET BASE): 28.5791 

STACK PRESSURE Cinch Hg): 29.3346 

STACK GAS VELOCITY (fVsec.): 59.0539 

ACTUAL STACK GAS FLOW RATE (ACFM): 21045.3061 

STANDARD STACK GAS FLOW RATE (SCFH): 1167665.96 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 0.0027 

PARTICULATE CONCENTRATION (LBS/SCF): 3.83E·07 

PARTICULATE EMISSION (LBS/HR): 0.4472 

BACK HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 0.0083 

PARTICULATE CONCENTRATION (LBS/SCF): 1.18E·06 

PARTICULATE EMISSION (LBS/HR): 1.3835 

ISOKINETIC RATIO(%): 101.1609 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METERT. METERT. 

deg F INLET OUTLET 

1 86 0.68 0.824621 0.90 76 76 

2 86 0.77 0.877496 1.00 79 76 

3 86 0.80 0.894427 1.10 83 76 

4 86 0.80 0.894427 1.10 85 76 

5 86 0.85 0.921954 1.10 86 76 

6 86 0.87 0.932738 1.20 86 77 

7 86 1.10 1.048809 1.50 87 77 

8 86 1.10 1.048809 1.50 90 77 

9 86 1.30 1.140175 1.70 90 78 

10 86 1.40 1.183216 1.90 90 78 

11 86 1.20 1.095445 1.60 91 78 

12 86 1.20 1.095445 1.60 91 79 

13 86 1.20 1.095445 1.60 81 79 

14 86 1.40 1.183216 1.90 91 79 

15 86 1.50 1.224745 2.00 91 79 

16 86 1.40 1.183216 1.90 91 79 

17 87 1.30 1.140175 1.70 90 79 

18 87 1.20 1.095445 1.60 91 79 

19 87 0.85 0.921954 1.10 91 80 

20 87 0.82 0.905539 1.10 90 80 

21 87 0.84 0.916515 1.10 90 80 

22 87 0.90 0.948683 1.20 90 80 

23 87 0.91 0.953939 1.20 90 80 METER T. 

24 87 0.85 0.921954 1.10 90 80 AVERAGE 

86.333333 1.0187 1.4042 87.9167 78.2500 83.0833 

f)~ ..... u 
PLANT: 

DATE: 

PLACE: 

RUN#: 

EMISSION TEST SUMMARY 

Dal·ltalia, Muskogee, OK 

30·0CI·06 

Glaze Line BaRhouse (EPN 41) 

3 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

0.195 PARTICULATE WEIGHT (Front half mg): 

0.972 PARTICULATE WEIGHT (Back half mg): 

0.84 STATIC PRESSURE (in. H20): 

17.5 

7.61 

6.4 

·0.25 

0 

21 

0 

GAS METER VOL.(Cu.Ft.) : 44.89 PERCENT C02 

BAROMETRIC PRESSURE 29.35 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA (Sq.Ft.) : 

NOZZLE AREA (teet): 

FOR RECTANGULAR STACK 

33 STACK LENGTH(inchs): 

5.939574 STACK WIDTH(inchs) : 

0.000207 STACK AREA (Sq. ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO(%): 

5.939574 

41.7247 

0.8237 

0.0194 

79.0000 

28.8400 

28.6301 

29.3316 

59.9552 

21366.4831 

1189095.14 

0.0028 

4.02E·07 

0.4782 

0.0024 

3.38E·07 

0.4022 

100.5536 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

17 

18 

19 

20 

21 

22 

23 

24 

deg F INLET 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

87 

88 

88 

88 

88 

88 

88 

87.25 

0.81 0.9 

0.85 0.921954 

0.85 0.921954 

0.86 0.927362 

0.84 0.916515 

0.92 0.959166 

1.00 1 

1.20 1.095445 

1.40 1.183216 

1.40 1.183216 

1.30 1.140175 

1.10 1.048809 

1.40 1.183216 

1.50 1.224745 

1.50 1.224745 

1.40 1.183216 

1.30 1.140175 

1.20 1.095445 

0.87 0.932738 

0.85 0.921954 

0. 90 0. 948683 

0.93 0.964365 

0.87 0.932738 

0. 76 0.87178 

1.0342 

po 

1.10 

1.10 

1.20 

1.10 

1.20 

1.30 

1.60 

1.90 

1.90 

1.70 

1.50 

1.90 

2.00 

2.00 

1.90 

1.70 

1.60 

1.20 

1.10 

1.20 

1.20 

1.20 

1.00 

1.4458 

78 

82 

84 

86 

87 

87 

88 

88 

89 

90 

90 

90 

BO 

89 

89 

90 

90 

90 

90 

90 

90 

90 

90 

90 

87.7917 

METERT. 

OUTLET 

78 

78 

78 

78 

78 

78 

78 

78 

79 

79 

79 

79 

79 

79 

79 

79 

79 

80 

80 

80 

80 

80 

0 

80 METER T. 

80 AVERAGE 

78.9583 83.3750 
EMISSION TEST SUMMARY 

PLANT: Dal·llaha, Muskogee. OK 

DATE: 30·0Ct·06 

PLACE : Press BaRhouse (EPN 40) 

RUN#: 1 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 

NOZZLE DIAMETER (INCH.) : 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

0.2473 PARTICULATE WEIGHT (Front half mg): 

0.994 PARTICULATE WEIGHT {Back hall mg): 

0.84 STATIC PRESSURE {in. H20): 

GAS METER VOL.(Cu.Ft.) : 44.539 PERCENT C02 

BAROMETRIC PRESSURE 29.35 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA (Sq.Ft.) : 

NOZZLE AREA (feet): 

FOR RECTANGULAR STACK 

39 STACK LENGTH(inchs): 

8.295768 STACK WIDTH(inchs) : 

0.000334 STACK AREA (Sq.Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE.: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ftlsec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINE.TIC RATIO(%): 

8 295768 

42.6000 

0.8849 

0.0203 

79.0000 

28.8400 

28.6194 

29.3257 

37.1507 

18491.6348 

1029174.15 

0.0034 

4.92E·07 

0.5066 

0.0016 

2.25E·07 

0.2317 

103.0065 

POINTS STACKT. DELTAP SQUARD.P DELTAH 

deg F 

METER T. 

INLET 

METER T. 

OUTLET 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

17 

18 

19 

20 

86 

86 

86 

86 

87 

87 

87 

87 

87 

86 

85 

87 

87 

87 

87 

87 

87 

87 

87 

85 

0.42 0.648074 

0.43 0.655744 

0.43 0.655744 

0.45 0.67082 

0.45 0.67082 

0.46 0.678233 

0.42 0.648074 

0.40 0.632456 

0.35 0.591608 

0.33 0.574456 

0.42 0.648074 

0.50 0.707107 

0.56 0.748331 

0.60 0.774597 

0.57 0.754983 

0.44 0.663325 

0.35 0.591608 

0.29 0.538516 

0.22 0.469042 

0.25 0.5 

1.40 

1.40 

1.40 

1.50 

1.50 

1.50 

1.40 

1.30 

1.20 

1.10 

1.40 

1.70 

1.90 

2.00 

1.90 

1.50 

1.20 

0.96 

0.72 

0.82 

74 

77 

so 

82 

83 

84 

84 

85 

84 

85 

82 

85 

86 

87 

87 

87 

86 

86 

86 

86 

74 

74 

74 

73 

74 

75 

75 

76 

76 

76 

76 

77 

77 

77 

77 

78 

78 

78 

78 

78 

18.8 

9.51 

4.35 

·0.33 

0 

21 

0 

0 

86.55 0.6411 1.3900 83.8000 76.0500 79.9250 

27 
EMISSION TEST SUMMARY 

PLANT : Dal·ltalia. Muskogee. OK 

DATE: 30·0Ct·06 

PLACE : Press Baghouse (EPN 40) 

RUN#: 2 

TEST DURATION (MINUTES): GO LIQUID COLLECTED (mls) : 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

0.2473 PARTICULATE WEIGHT (Front half mg): 

0.994 PARTICULATE WEIGHT (Back half mg): 

0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 43.69 PERCENT C02 

BAROMETRIC PRESSURE 29.35 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA (Sq. Ft.) : 

NOZZLE AREA (feet): 

FOR RECTANGULAR STACK 

39 STACK LENGTH(inches) : 

8.295768 STACK WIDTH(inches) : 

0.000334 STACK AREA (Sq.Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

• STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ttl sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO(%): 

8.295768 

POINTS STACK T. DELTA P SQUAR O.P DELTA H 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

17 

18 

19 

20 

deg F 

88 

88 

87 

88 

88 

88 

88 

88 

87 

87 

87 

88 

88 

88 

88 

88 

88 

88 

88 

88 

0.44 0.663325 

0.46 0.678233 

0.55 0.74162 

0.57 0.754983 

0.57 0.754983 

0.44 0.663325 

0.36 0.6 

0.29 0.538516 

0.25 0.5 

0.22 0.469042 

0 36 0.6 

0.39 0.6245 

0.40 0.632456 

0.40 0.632456 

0.38 0.616441 

0.42 0.648074 

0.42 0.648074 

0.40 0.632456 

0.37 0.608276 

0.33 0.574456 

1.50 

1.50 

1.80 

1.90 

1.90 

1.50 

1.20 

0.96 

0.83 

0.73 

1.20 

1.30 

1.30 

1.30 

1.30 

1.40 

1.40 

1.30 

1.20 

1.10 

41.5395 

0.9414 

0.0222 

79.0000 

28.8400 

28.5998 

29.3243 

36.5093 

18172.3544 

1007180.79 

0.0035 

4.96E·07 

0.4999 

0.0012 

1.65E·07 

0.1657 

102.6355 

METER T. 

INLET 

78 

86 

87 

88 

89 

89 

88 

87 

87 

87 

81 

88 

89 

88 

89 

89 

89 

89 

89 

88 

METER T. 

OUTLET 

77 

77 

77 

78 

79 

79 

79 

79 

79 

79 

79 

79 

79 

79 

79 

80 

80 

80 

80 

80 

20 

9.35 

3.1 

·0.35 

0 

21 

0 

0 

87.8 0.6291 1.3310 87.2500 78.9000 83.0750 

28 
PLANT: 

DATE: 

PLACE: 

RUN#: 

EMISSION TEST SUMMARY 

Dal·ltalia. Muskogee. OK 

30·0Ct·06 

Press Baghouse (EPN 40) 

3 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

0.2473 PARTICULATE WEIGHT (Front hall mg): 

0.994 PARTICULATE WEIGHT (Back half mg): 

0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 43.617 PERCENT C02 

BAROMETRIC PRESSURE 29.35 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA (Sq.Ft.) : 

FOR RECTANGULAR STACK 

39 STACK LENGTH(inchs) : 

8.295768 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): O.OD0334 STACK AREA (Sq.Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO(%): 

8.295768 

41.4003 

1.2003 

0.0282 

79.0000 

28.8400 

28.5346 

29.3250 

36.5236 

18179.4977 

999579.435 

0.0029 

4.19E·07 

0.4185 

0.0009 

l.28E·07 

0.1278 

103.0697 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

17 

18 

19 

20 

deg F 

89 

88 

89 

89 

89 

89 

89 

89 

89 

88 

87 

89 

89 

89 

89 

90 

90 

89 

89 

87 

0.39 0.6245 

0.37 0.608276 

0.36 0.6 

0.40 0.632456 

0.38 0.616441 

0.42 0.648074 

0.43 0.655744 

0.42 0.648074 

0.39 0.6245 

0.37 0.608276 

0.41 0.640312 

0.48 0.69282 

0.50 0.707107 

0.52 0.72111 

0.54 0.734847 

0.40 0.632456 

0.37 0.608276 

0.30 0.547723 

0.27 0.519615 

0.24 0.489898 

1.30 

1.20 

1.20 

1.30 

1.30 

1.40 

1.40 

1.40 

1.30 

1.20 

1.40 

1.60 

1.70 

1.70 

1.80 

1.30 

1.20 

1.00 

0.90 

0.80 

INLET 

79 

86 

87 

87 

88 

88 

89 

89 

89 

89 

83 

89 

89 

89 

90 

90 

90 

90 

89 

89 

OUTLET 

79 

79 

79 

79 

79 

79 

80 

80 

80 

80 

80 

80 

80 

80 

81 

81 

81 

81 

81 

81 

25.5 

7.86 

2.4 

·0.34 

0 

21 

0 

0 

88.8 0.6280 1.3200 87.9500 80.0000 83.9750 

29 
EMISSION TEST SUMMARY 

PLANT: Dal-ltalia, Muskogee, OK 

DATE: 2-Nov-06 

PLACE: Phase II Scrubber Exhaust (EPN 29) 

RUN#: 1 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 129.7 

NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg): 0 

METER COEFFICIENT (Y) : 0.994 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 

GAS METER VOL.(Cu.Ft.) : 35.432 PERCENT C02 3 

BAROMETRIC PRESSURE 30.15 PERCENT 02 17 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 72.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 28.6684 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.): 0 

ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 36.5254 

VOLUME OF WATER VAPOR (STD. CU.FT.): 6.1050 

FRACTIONAL MOISTURE CONTENT (%): 0.1432 

DRY BASE: so.oooo 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.5618 

STACK PRESSURE (inch Hg): 30.1529 

STACK GAS VELOCITY (ft/sec.): 24.4186 

ACTUAL STACK GAS FLOW RATE (ACFM): 42002.4699 

STANDARD STACK GAS FLOW RATE (SCFH): 1955394.53 

ISOKINETIC RATIO(%): 100.4746 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 129 0.10 0.316228 0.54 44 44 

2 129 0.12 0.34641 0.64 46 45 

3 127 0.13 0.360555 0.70 50 45 

4 128 0.15 0.387298 0.80 51 45 

5 128 0.15 0.387298 0.80 53 46 

6 126 0.20 0.447214 1.10 56 46 

7 126 0.20 0.447214 1.10 57 47 

8 125 0.20 0.447214 1.10 57 47 

9 126 0.14 0.374166 0.76 58 47 

10 128 0.14 0.374166 0.76 58 48 

11 128 0.12 0.34641 0.65 59 48 

12 129 0.11 0.331662 0.60 60 49 

13 129 0.14 0.374166 0.76 58 50 

14 129 0.16 0.4 0.87 61 51 

15 128 0.18 0.424264 0.98 62 51 

16 128 0.20 0.447214 1.10 63 51 

17 128 0.22 0.469042 1.20 64 52 

18 128 0.23 0.479583 1.25 64 52 

19 127 0.22 0.469042 1.20 64 53 

20 127 0.22 0.469042 1.20 64 53 

21 127 0.20 0.447214 1.10 64 53 

22 127 0.17 0.412311 0.93 64 54 

23 127 0.15 0.387298 0.81 64 54 METER T. 

24 128 0.13 0.360555 0.71 64 54 AVERAGE 

127.58333 0.4044 0.9025 58.5417 49.3750 53.9583 

39 
EMISSION TEST SUMMARY 

PLANT: Dal·ltalia. Muskogee, OK 

DATE: 2·NOV·06 

PLACE: Phase II Scrubber Exhaust (EPN 29) 

RUN#: 2 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mls) : 130.6 

NOZZLE DIAMETER (INCH.) : 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 

METER COEFFICIENT (Y) : 0.994 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 

GAS METER VOL.(Cu.Ft.) : 35.462 PERCENT C02 3 

BAROMETRIC PRESSURE 30.1 PERCENT 02 17 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 72.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 28.6684 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 35.7477 

VOLUME OF WATER VAPOR (STD. CU.FT.): 6.1473 

FRACTIONAL MOISTURE CONTENT (%): 0.1467 

DRY BASE: 80.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.5225 

STACK PRESSURE (inch Hg): 30.1029 

STACK GAS VELOCITY (ft/sec.): 24.1024 

ACTUAL STACK GAS FLOW RATE (ACFM): 41458.6419 

STANDARD STACK GAS FLOW RATE (SCFH): 1915282.49 

ISOKINETIC RATIO(%): 100.3947 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 129 0.13 0.360555 0.71 55 54 

2 129 0.15 0.387298 0.82 60 55 

3 129 0.15 0.387298 0.82 63 55 

4 129 0.20 0.447214 1.10 65 55 

5 128 0.20 0.447214 1.10 69 56 

6 129 0.18 0.424264 1.00 69 57 

7 129 0.20 0.447214 1.10 70 57 

8 129 0.21 0.458258 1.20 72 58 

9 129 0.20 0.447214 1.10 72 59 

10 129 0.18 0.424264 1.00 71 60 

11 129 0.16 0.4 0.90 72 60 

12 128 0.13 0.360555 0.73 72 60 

13 129 0.10 0.316228 0.56 65 61 

14 129 0.12 0.34641 0.67 69 61 

15 129 0.13 0.360555 0.73 72 61 

16 129 0.15 0.387298 0.84 72 62 

17 129 0.15 0.387298 0.84 72 61 

18 129 0.19 0.43589 1.10 73 61 

19 128 0.21 0.458258 1.20 74 62 

20 127 0.19 0.43589 1.10 75 62 

21 128 0.16 0.4 0.90 75 62 

22 128 0.14 0.374166 0.79 74 63 

23 129 0.12 0.34641 0.67 74 63. METER T. 

24 129 0.10 0.316228 0.56 73 63 AVERAGE 

128.70833 0.3982 0.8975 69.9167 59.5000 64.7083 

40 
EMISSION TEST SUMMARY 

PLANT: Dal·ltalia, Muskogee, OK 

DATE: 2-Nov-06 

PLACE: Phase II Scrubber Exhaust (EPN 29) 

RUN#: 3 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 126 

NOZZLE DIAMETER (INCH.): 0.3127 PARTICULATE WEIGHT (Front half mg) : 0 

METER COEFFICIENT (Y) : 0.994 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 

GAS METER VOL.(Cu.Ft.} : 35.19 PERCENT C02 3 

BAROMETRIC PRESSURE 30.15 PERCENT 02 17 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 72.5 STACK LENGTH(inchs): 

STACK AREA (Sq.Ft.) : 28.6684 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000533 STACK AREA (Sq.Ft.): 0 

ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 35.2108 

VOLUME OF WATER VAPOR (STD. CU.FT.}: 5.9308 

FRACTIONAL MOISTURE CONTENT(%): 0.1442 

DRY BASE: • 80.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.5512 

STACK PRESSURE (inch Hg): 30.1529 

STACK GAS VELOCITY (ft/sec.): 23.6643 

ACTUAL STACK GAS FLOW RATE (ACFM): 40705.1208 

STANDARD STACK GAS FLOW RATE (SCFH}: 1888746.64 

ISOKINETIC RATIO(%): 100.2762 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 129 0.12 0.34641 0.67 62 62 

2 129 0.14 0.374166 0.79 67 62 

3 129 0.16 0.4 0.90 70 62 

4 129 0.18 0.424264 1.00 72 62 

5 129 0.21 0.458258 1.20 73 62 

6 129 0.22 0.469042 1.20 74. 63 

7 129 0.23 0.479583 1.30 75 63 

8 129 0.22 0.469042 1.30 75 63 

9 129 0.20 0.447214 1.10 76 64 

10 129 0.17 0.412311 0.97 76 64 

11 129 0.14 0.374166 0.80 76 65 

12 128 0.11 0.331662 0.63 75 65 

13 128 0.10 0.316228 0.57 68 65 

14 129 0.11 0.331662 0.62 73 65 

15 129 0.12 0.34641 0.68 75 66 

16 129 0.13 0.360555 0.71 76 66 

17 129 0.15 0.387298 0.86 76 66 

18 129 C.17 0.4123i 1 0.97 77 66 

19 129 0.20 0.447214 1.15 78 67 

20 129 0.18 0.424264 1.00 79 67 

21 130 0.15 0.387298 0.86 78 67 

22 129 0.12 0.34641 0.69 78 67 

23 129 0.11 0.331662 0.63 77 67 METER T. 

24 127 0.10 0.316228 0.57 76 67 AVERAGE 

128.875 0.3914 0.8821 74.2500 64.7083 69.4792 

41 
PLANT: 

DATE: 

PLACE: 

RUNt#: 

EMISSION TEST SUMMARY 

Dal·ltalla, Musk<'l·lC:e. OK 

2·NOV·06 

Phase II Scrubber Exhaust (EPN 29) 

4 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

0.3123 PARTICULATE WEIGHT (Front half mg): 

0.992 PARTICULATE WEIGHT (Back half mg): 

0.84 STATIC PRESSURE (in. H20): 

129.4 

35.38 

10.2 

0.04 

GAS METER VOL.(Cu.Ft.) : 36.351 PERCENT C02 3 

BAROMETRIC PRESSURE 29.15 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA (SQ.Ft.) : 

NOZZLE AREA (feet): 

FOR RECTANGULAR STACK 

72.5 STACK LENGTH(inchs): 

28.6684 STACK WIDTH(inchs) : 

0.000532 STACK AREA (SQ.Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.fi.): 

VOLUME OF WATER VAPOR (STD. CU.fi.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ftlsec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO(%): 

28.6684 

34.7735 

6.0909 

0.1491 

80.0000 

29.1600 

27.4966 

29.1529 

24.6652 

42426.7332 

1891253.17 

0.0157 

2.24E·06 

4.2429 

0.0045 

6.47E·07 

1.2232 

99.1532 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

17 

18 

19 

20 

21 

22 

23 

24 

deg F INLET 

129 

129 

128 

128 

128 

128 

128 

129 

130 

130 

130 

130 

129 

129 

129 

129 

129 

130 

130 

130 

130 

130 

130 

130 

129.25 

0.13 0.360555 

0.14 0.374166 

0.15 0.387298 

0.18 0.424264 

0.22 0.469042 

0.23 0.479583 

0.22 0.469042 

0.20 0.447214 

0.18 0.424264 

0.16 0.424264 

0.14 0.374166 

0.13 0.360555 

0.10 0.316228 

0.11 0.331662 

0.14 0.374166 

0.15 0.387298 

0.19 0.43589 

0.22 0.469042 

0.21 0.458258 

0.19 0.43589 

0.15 0.387298 

0.12 0.34641 

0.11 0.331662 

0.12 0.34641 

0.4006 

0.75 

0.80 

0.86 

1.00 

1.30 

1.30 

1.30 

1.20 

1.00 

1.00 

0.81 

0.76 

0.58 

0.64 

0.81 

0.87 

1.10 

1.30 

1.20 

1.10 

0.88 

0.70 

0.65 

0.70 

0.9421 

66 

70 

72 

76 

79 

79 

80 

81 

81 

81 

80 

80 

73 

78 

81 

82 

83 

85 

85 

85 

85 

84 

84 

84 

79.7500 

METERT. 

OUTLET 

66 

66 

66 

66 

67 

67 

67 

68 

69 

69 

69 

69 

69 

70 

70 

70 

71 

71 

71 

72 

72 

72 

17 

0 

0 

72 METERT. 

73 AVERAGE 

69.2500 74.5000 

42 
EMISSION TEST SUMMARY 

PLANT: Dal·ltalia. MuskORee, OK 

DATE: 2·NOv·06 

PLACE: Prtase II Scrubber Exhaust (EPN 29) 

RUN#: 5 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 122.2 

NOZZLE DIAMETER (INCH.): 0.3123 PARTICULATE WEIGHT (Front half mg): 23.36 

METER COEFFICIENT (Y) : 0.992 PARTICULATE WEIGHT (Back half mg}: 11.5 

PI TOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 0.04 

GAS METER VOL.(Cu.Ft.) : 35.05 PERCENT C02 3 

BAROMETRIC PRESSURE 30.15 PERCENT 02 17 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 72.5 STACK LENGTH(Inches): 

STACK AREA (Sq.Ft.) : 28.6684 STACK WI DTH(inches) : 

NOZZLE AREA (feet): 0.000532 STACK AREA (Sq.Ft.): 0 

ENTER THE STACK AREA SHOWN ABOVE: 28.6684 

FLOWS 

SAMPLED VOLUME (STD. CU. FT.): 34.3393 

VOLUME OF WATER VAPOR (STD. CU.FT.): 5.7520 

FRACTIONAL MOISTURE CONTENT (%): 0.1435 

DRY BASE: 80.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.5589 

STACK PRESSURE (inch Hg): 30.1529 

STACK GAS VELOCITY (ftlsec.): 23.3632 

ACTUAL STACK GAS FLOW RATE (ACFM): 40187.0515 

STANDARD STACK GAS FLOW RATE (SCFH): 1866991.87 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 0.0105 

PARTICULATE CONCENTRATION (LBS/SCF): 1.50E·06 

PARTICULATE EMISSION (LBS/HR): 2.8005 

BACK HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 0.0052 

PARTICULATE CONCENTRATION (LBS/SCF): 7.38E·07 

PARTICULATE EMISSION (LBSIHR): 1.3787 

ISOKINETIC RATIO(%): 99.1873 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METERT. METER T. 

deg F INLET OUTLET 

1 129 0.10 0.316228 0.59 71 71 

2 129 0.11 0.331662 0.65 80 71 

3 129 0.13 0.360555 0.76 82 71 

4 129 0.16 0.4 0.94 84 72 

5 129 0.18 0.424264 1.10 86 73 

6 129 0.20 0.447214 1.20 87 74 

7 129 0.22 0.469042 1.30 88 75 

8 129 0.20 0.447214 1.20 89 75 

9 129 0.18 0.424264 1.10 87 76 

10 129 0.15 0.387298 0.89 88 76 

11 129 0.12 0.34641 0.71 88 77 12 127 0.10 0.316228 0.60 88 77 

13 128 0.10 0.316228 0.58 77 76 14 128 0.12 0.34641 0.71 83 76 

15 129 0.14 0.374166 0.82 85 76 

16 129 0.15 0.387298 0.89 86 76 17 129 0.19 0.43589 1.10 86 76 

18 129 0.20 0.447214 1.20 87 75 

19 128 0.21 0.458258 1.20 86 75 20 129 0.20 0.447214 1.20 86 75 21 129 0.16 0.4 1.95 86 75 22 128 0.12 0.34641 0.71 86 75 23 128 0.11 0.331662 0.65 85 75 METER T. 24 127 0.10 0.316228 0.59 85 74 AVERAGE 

128.625 0.3866 0.9433 84.8333 74.6667 79.7500 

43 
EMISSION TEST SUMMARY 

PLANT: Dal·llalia, MuskoRee. DK 

DATE: 2-Nov-06 

PLACE: Phase II Scrubber Exhaust (EPN 29) 

RUN#: 6 

TEST DURATION (MINUTES): 60 LIQUID COLLECTED (mls) : 

NOZZLE DIAMETER (INCH.): 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp} : 

0.3123 PARTICULATE WEIGHT (Front half mg): 

0.992 PARTICULATE WEIGHT (Back half mg}: 

0.84 STATIC PRESSURE (in. H20): 

121.7 

29.93 

14.29 

0.04 

3 

17 

0 

GAS METER VOL.(Cu.Ft.) : 35.98 PERCENT C02 

BAROMETRIC PRESSURE 30. 15 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 

STACK AREA (Sq.Ft.) : 

NOZZLE AREA (feet): 

FOR RECTANGULAR STACK 

72.5 STACK LENGTH(inchs): 

28.6684 STACK WIDTH(inchs) : 

0.000532 STACK AREA {Sq. Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.):. 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY {fVsec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

BACK HALF 

PARTICULATE CONCENTRATION (GR.ISCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO(%): 

2B.6684 

35.5065 

5.7284 

0.1389 

80.0000 

29.1600 

27.6096 

30.1529 

23.9327 

41166.6439 

1919807.14 

0.0130 

1.86E·06 

3.5683 

0.0062 

8.87E-07 

1.7037 

99.7372 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

12 

13 

14 

15 

16 

17 

18 

19 

20 

21 

22 

23 

24 

deg F INLET 

129 

128 

128 

128 

129 

129 

130 

130 

130 

130 

130 

130 

129 

130 

130 

130 

130 

130 

130 

130 

130 

130 

129 

129 

129.5 

0.13 0.360555 

0.14 0.374166 

0.15 0.387298 

0.18 0.424264 

0.19 0.43589 

0.21 0.458258 

0.22 0.469042 

0.22 0.469042 

0.21 0.458258 

0.20 0.447214 

0.16 0.4 

0.14 0.374166 

0.10 0.316228 

0.12 0.34641 

0.13 0.360555 

0.15 0.387298 

0.16 0.4 

0.18 0.424264 

0.19 0.43589 

0.17 0.412311 

0.15 0.387298 

0.13 0.360555 

0.10 0.316228 

0.09 0.3 

0.3960 

0.75 

0.80 

0.87 

1.00 

1.10 

1.20 

1.30 

1.30 

1.20 

1.20 

0.94 

0.82 

0.59 

0.70 

0.76 

0.87 

0.93 

1.05 

1.10 

0.99 

0.87 

0.76 

0.58 

0.52 

0.9250 

71 

78 

81 

82 

82 

83 

84 

84 

84 

84 

84 

83 

78 

79 

80 

81 

80 

80 

81 

80 

79 

78 

77 

77 

80.4167 

METER T. 

OUTLET 

71 

71 

71 

72 

72 

72 

73 

73 

73 

73 

73 

73 

72 

72 

71 

71 

71 

71 

71 

70 

69 

69 

0 

68 METER T. 

68 AVERAGE 

71.2500 75.8333 

44 
--.-.- --~---;--- -~ ~: .... -

'· 

•I 

App~ndlxB 

l·ti .• 

.. J.:. 
Sheet1 

Summary of CO Analyzer Calibrations and Bias 

Plant: Dal-ltalia, Muskogee, OK 

Source: Phase II Scrubber 

Date: 11/2/2006 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Zero Gas 

Mid Range 

High Range 

Value Response Difference 

0 1.33 1.33 

99.1 99.18 0.08 

200 196.65 -3.35 

System Calibration Bias and Drift Data 

0.665 

0.04 

-1.675 

Analyzer Initial Values Final Values Drift 

Run #1 

Run #2 

Run #3 

Calibration System System System System 

Respon·se Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 

Upscale 

1.33 

99.18 

Average CO Concentration: 

Corrected CO Concentration: 

(Equation 6C-1) 

Zero Gas 1.33 

Upscale 99.18 

Average CO Concentration: 

Corrected CO Concentration: 

(Equation 6C-1) 

Zero Gas 1.33 

Upscale 99.18 

Average CO Concentration: 

1.1 

94.7 

2.2 

96.58 

0.33 

94.38 

Corrected CO Concentration: 

(Equation 6C-1) 

-0.115 

-2.24 

86.6 

89.56852 

0.435 

-1.3 

126.99 

132.2438 

-0.5 

-2.4 

118.98 

126.6041 

Page 1 

2.2 

96.58 

0.33 

94.38 

-0.35 

91.88 

0.435 

-1.3 

-0.5 

-2.4 

-0.84 

-3.65 

0.55 

0.94 

-0.935 

-1.1 

-0.34 

-1.25 

Average 

Calibration 

Values 

1.65 

95.64 

1.265 

95.48 

-0.01 

93.13 
Sheet1 

Summary of NOx Analyzer Calibrations and Bias 

Plant: Dal-ltalia, Muskogee. OK 

Source: Phase II Scrubber 

Date: 10/31/2006 

Run #1 

Run#2 

Run #3 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 

Mid Range 

High Range 

0 0 0 0 

25 25.45 0.45 0. 75 

51 50.78 -0.22 -0.36667 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 0 0.03 0.05 0.13 0.216667 

Upscale 25.45 24.1 -2.25 25.08 -0.61667 

Average NOx Concentration: 21.67 

Corrected NOx Concentration: 22.02162 

(Equation 6C-1) 

Zero Gas 0 0.13 0.216667 0.15 0.25 

Upscale 25.45 25.08 -0.61667 24.45 -1.66667 

Average NOx Concentration: 22.55 

Corrected NOx Concentration: 22.75127 

(Equation 6C-1) 

Zero Gas 0 0.15 0.25 0.25 0.416667 

Upscale 25.45 24.45 -1.66667 24.98 -0.78333 

Average NOx Concentration: 22.77 

Corrected NOx Concentration: 23.01652 

(Equation 6C-1) 

Page 1 

Drift Average 

Calibration 

Values 

0.166667 0.08 

1.633333 24.59 

0.033333 0.14 

-1.05 24.765 

0.166667 0.2 

0.883333 24.715 

82 
Sheet1 

Summary of Sulfur Dioxide Analyzer Calibrations and Bias 

Plant: 

Source: 

Date: 

Run #1 

Run #2 

Run #3 

Dal-ltalia, Muskogee, OK 

Phase II Scrubber 

11/2/2006 

Analyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Zero Gas 

Mid Range 

High Range 

Value Response Difference 

0 -0.03 -0.03 

49.8 49.3 -0.5 

100 99.8 -0.2 

System Calibration Bias and Drift Data 

-0.03 

-0.5 

-0.2 

Analyzer Initial Values Final Values Drift 

Calibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Zero Gas 

Upscale 

-0.03 

49.3 

-0.08 

47 

Average S02 Concentration: 

Corrected S02 Concentration: . 

(Equation 6C-1) 

Zero Gas -0.03 -0.08 

Upscale 49.3 47.08 

Average S02 Concentration: 

Corrected S02 Concentration: 

(Equation 6C-1) 

Zero Gas -0.03 -0.4 

Upscale 49.3 46.48 

Average 502 Concentration: 

Corrected S02 Concentration: 

(Equation 6C-1) 

-0.05 

-2.3 

0.03 

0.116256 

-0.05 

-2.22 

-0.44 

-0.21182 

-0.37 

-2.82 

-0.11 

0.123413 

Page 1 

-0.08 

47.08 

-0.4 

46.48 

-0.05 

45.88 

-0.05 

-2.22 

-0.37 

-2.82 

-0.02 

-3.42 

0 

0.08 

-0.32 

-0.6 

0.35 

-0.6 

Average 

Calibration 

Values 

-0.08 

47.04 

-0.24 

46.78 

-0.225 

46.18 

83 
11/2106 Nox Converter Check 

Date/Time NOx 

mm/dd/yy hh:mm:ss ppm 

11/02/06 07:34:04 0.0163 Zero NOx 

11/02106 07:35:04 0.040228 

11/02/06 07:36:04 44.50978 

11/02/06 07:37:04 49.981 51 ppm NOx 

11/02/06 07:38:04 12.04688 

11/02/06 07:39:04 26.13428 Start Converter Check 

11/02/06 07:40:04 27.84863 

11/02/06 07:41:04 27.82276 

11/02/06 07:42:04 27.87696 

11/02/06 07:43:04 27.88623 

11/02/06 07:44:04 27.89161 

11/02106 07:45:04 27.89698 

11/02/06 07:46:04 27.89844 

11/02/06 07:47:04 27.8794 

11/02/06 07:48:04 27.89747 

11/02/06 07:49:04 27.87061 

11/02/06 07:50:04 27.86622 

11/02/06 07:51:04 27.85255 

11/02/06 07:52:04 27.83887 

11/02/06 07:53:04 27.83595 

11/02/06 07:54:04 27.83106 

11/02/06 07:55:04 27.82081 

11/02/06 07:56:04 27.79054 

11/02/06 07:57:04 27.75929 

11/02/06 07:58:04 27.75636 

11/02/06 07:59:04 27.72511 

11/02/06 08:00:04 27.74366 

11/02/06 08:01:04 27.72023 

11/02/06 08:02:04 27.70314 

11/02/06 08:03:04 27.69288 

11/02/06 08:04:04 27.64454 

11/02/06 08:05:04 27.64699 

11/02/06 08:06:04 27.61622 

11/02/06 08:07:04 27.6006 

11/02/06 08:08:04 27.60352 Stop Converter Check 

11/02/06 08:09:04 27.58936 

Page 1 84 
11/2/06 Calibrations 

Date/Time voc co NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

11/02/06 08:19:52 1.2 1.5 0.0 7.1 

11/02/06 08:20:02 1.6 1.7 0.0 7.1 Zero NOx 

11/02/06 08:20:12 1.9 1.7 0.0 7.1 

11/02/06 08:20:22 2.1 2.0 0.0 7.1 

11/02/06 08:20:32 2.5 2.1 0.1 7.2 

11/02/06 08:20:42 2.6 1.7 20.7 7.2 

11/02/06 08:20:52 2.8 1.5 24.4 7.2 

11/02/06 08:21 :02 2.8 1.8 24.5 7.1 

11/02/06 08:21:12 2.9 1.8 25.0 7.1 

11/02106 08:21:22 3.0 1.8 25.5 7.3 

11/02106 08:21:32 3.0 2.1 25.4 7.2 

11/02/06 08:21:42 3.1 2.2 25.5 7.2 Zero NOx 

11/02/06 08:21 :52 3.2 2.1 25.5 7.2 

11/02/06 08:22:02 3.2 2.3 25.4 7.2 

11/02/06 08:22:12 3.2 2.2 25.5 4.3 

11/02106 08:22:22 3.2 2.1 25.4 0.0 

11/02/06 08:22:32 3.3 2.4 13.1 -0.1 

11/02/06 08:22:42 3.3 2.3 0.1 -0.1 

11/02106 08:22:52 3.4 2.3 0.1 -0.2 

11/02/06 08:23:02 3.4 2.1 0.0 -0.1 

11/02/06 08:23:12 3.4 2.2 0.1 -0.1 

11/02106 08:23:22 3.3 2.0 0.1 -0.1 

11/02106 08:23:32 3.4 2.1 0.1 -0.1 

11/02106 08:23:42 3.4 1.8 43.8 -0.1 

11/02106 08:23:52 3.4 1.8 50.3 0.0 

11/02/06 08:24:02 3.4 1.9 50.6 0.0 

H/02106 08:24:12 3.4 2.0 50.7 -0.1 

11/02/06 08:24:22 3.4 2.2 50.7 -0.2 51 ppm NOx 

11/02/06 08:24:32 3.4 2.0 50.7 -0.1 

11/02106 08:24:42 3.4 1.9 50.8 -0.1 

11/02/06 08:24:52 3.4 2.1 32.0 -0.2 

11/02/06 08:25:02 3.3 2.3 0.2 -0.1 

11/02/06 08:25:12 3.3 2.1 0.1 0.0 

11/02/06 08:25:22 3.3 1.8 0.1 0.0 

11/02106 08:25:32 3.3 1.8 0.0 0.0 

11/02106 08:25:42 3.3 1.8 0.1 0.0 

11/02106 08:25:52 3.4 1.8 0.1 0.0 

11/02106 08:26:02 3.4 16.6 0.0 0.0 

11/02/06 08:26:12 3.4 85.0 0.0 0.0 

11/02/06 08:26:22 3.4 97.3 0.0 -0.1 

11/02106 08:26:32 3.3 98.5 0.0 -0.1 

11/02/06 08:26:42 3.3 98.8 0.0 0.0 

11/02/06 08:26:52 3.3 98.9 0.0 0.0 

11/02/06 08:27:02 3.3 99.1 0.0 0.0 

11/02106 08:27:12 3.3 99.0 0.0 0.0 

11/02106 08:27:22 3.3 99.3 0.0 -0.1 99.1 ppm CO 

11/02/06 08:27:32 3.4 99.2 0.0 0.0 Zero S02 

11/02/06 08:27:42 3.4 99.2 0.0 0.0 

11/02106 08:27:52 3.4 68.9 0.0 -0.1 

11/02/06 08:28:02 3.4 9.0 0.0 -0.1 

11/02106 08:28:12 3.4 2.7 0.0 -0.1 

11/02106 08:28:22 3.4 2.3 0.0 -0.1 

11/02106 08:28:32 3.4 2.1 0.1 0.0 

11/02106 08:28:42 3.4 2.0 0.0 -0.1 

11/02/06 08:28:52 3.4 1.9 0.1 -0.1 

11/02/06 08:29:02 3.4 5.0 0.1 0.0 

11/02/06 08:29:12 3.4 130.5 0.0 0.0 

11/02/06 08:29:22 3.4 190.4 0.0 0.0 

11/02106 08:29:32 3.4 194.5 0.0 -0.1 

11/02106 08:29:42 3.4 195.1 0.0 -0.1 

11/02/06 08:29:52 3.4 195.3 0.0 -0.2 

11/02/06 08:30:02 3.4 196.0 0.0 -0.2 

11/02106 08:30:12 3.4 196.5 0.0 0.0 

11/02/06 08:30:22 3.4 196.6 0.0 0.0 

11/02/06 08:30:32 3.3 196.9 0.0 0.0 200 ppm NOx 

11/02/06 08:30:42 3.3 196.7 0.0 0.0 

11/02/06 08:30:52 3.3 196.4 0.0 0.0 

Page 1 85 
1112/06 Calibrations 

11/02/06 08:31 :02 3.3 165.8 0.0 -0.1 

11/02/06 08:31 :12 3.3 27.8 0.0 -0.2 

11102106 08:31 :22 3.3 4.2 0.0 -0.3 

11/02/06 08:31 :32 3.4 2.4 0.1 -0.2 

11/02/06 08:31:42 3.4 2.1 0.0 -0.2 

11102/06 08:31:52 3.4 1.9 0.0 -02 

11/02/06 08:32 :02 3.4 1.6 0.0 -0.2 

11102/06 08:32:12 3.4 1.6 0.1 -0.1 

11/02/06 08:32:22 3.4 1.6 0.1 0.8 

11/02/06 08:32:32 3.4 1.1 0.1 17.5 

11/02/06 08:32:42 3.4 1.1 0.1 37.2 

11/02/06 08:32:52 3.4 0.9 0.1 44.9 

11/02/06 08:33:02 3.4 0.9 0.1 47.2 

11/02/06 08:33:12 3.4 0.9 0.1 47.8 

11/02/06 08:33:22 3.4 0.9 0.1 47.9 

11/02/06 08:33:32 3.4 0.9 0.1 47.9 

11/02/06 08:33:42 3.4 1.0 0.1 47.7 

11/02/06 08:33:52 3.4 1.1 0.1 47.7 

11/02/06 08:34:02 3.4 0.9 0.1 47.7 

11/02/06 08:34:12 3.4 1.0 0.1 49.1 

11/02/06 08:34:22 3.4 1.2 0.1 49.2 

11/02/06 08:34:32 3.4 1.4 .0.1 49.3 

11/02/06 08:34:42 3.4 1.3 0.0 49.3 49.8 ppm S02 

11102/06 08:34:52 3.4 1.4 0.0 49.3 Zero CO 

11102/06 08:35:02 3.3 1.2 0.0 49.3 

11/02/06 08:35:12 3.3 1.2 0.0 49.3 

11/02/06 08:35:22 3.4 1.6 0.0 44.9 

11/02/06 08:35:32 3.3 1.7 0.1 22.4 

11/02106 08:35:42 3.4 1.8 0.0 6.6 

11/02/06 08:35:~2 3.4 1.6 0.1 1.3 

11/02/06 08:36:02 3.4 1.7 0.0 0.0 

11102/06 08:36:12 3.4 1.6 0.1 -0.2 

11/02106 08:36:22 3.4 1.5 0.1 -0.2 

11/02/06 08:36:32 3.4 1.7 0.1 -0.2 

11/02/06 08:36:42 3.3 1.7 0.0 -0.3 

11/02/06 08:36:52 3.3 1.6 0.0 -0.2 

11/02/06 08:37:02 3.3 1.1 0.2 21.1 

11/02/06 08:37:12 3.4 0.9 0.4 70.9 

11/02/06 08:37:22 3.3 0.9 0.4 96.0 

11/02/06 08:37:32 3.3 0.9 0.4 99.8 

11/02/06 08:37:42 3.4 0.9 0.4 99.8 

11/02/06 08:37:52 3.4 0.9 0.4 99.8 100 ppm S02 

11/02/06 08:38:02 3.3 0.9 0.4 99.8 

11/02/06 08:38:12 3.4 0.9 0.4 99.8 

11/02/06 08:38:22 3.3 1.1 0.3 97.6 

11/02/06 08:38:32 3.2 1.4 0.1 56.3 

11/02/06 08:38:42 3.2 1.1 0.1 17.9 

11/02/06 08:38:52 32 1.2 0.1 4.4 

11/02/06 08:39:02 3.2 1.4 0.0 0.8 

11/02/06 08:39:12 2.2 1.2 0.0 0.0 

11/02106 08:39:22 0.6 1.0 0.7 0.0 

11/02/06 08:39:32 0.5 1.2 8.4 0.0 

11/02/06 08:39:42 0.4 1.0 14.4 0.0 

11/02/06 08:39:52 0.3 1.0 18.0 -0.1 

11/02/06 08:40:02 0.3 1.0 20.5 -0.1 

11/02/06 08:40:12 0.2 0.9 22.0 -0.2 

11/02/06 08:40:22 0.3 0.9 23.0 -0.3 

11/02/06 08:40:32 0.3 0.9 23.4 -0.4 

11/02/06 08:40:42 0.3 0.9 23.7 -0.3 

11/02/06 08:40:52 0.2 1.2 23.9 -0.2 

11/02/06 08:41:02 0.1 1.0 23.9 -0.2 

11/02/06 08:41:12 0.1 0.9 24.0 -0.1 

11/02/0S 08:41:22 0.1 1.0 24.1 -0.1 

11/02/06 08:41:32 0.1 1.1 24.1 -0.2 25 ppm NOx Bias 

11/02/06 08:41:42 0.1 1.1 24.1 -02 Zero VOC. CO Bias 

11/02/06 08:41 :52 0.1 1.2 24.1 -0.2 

11/02/06 08:42:02 0.1 1.2 24.2 -0.2 

11/02/06 08:42:12 0.1 1.2 24.1 -0.1 

11/02/06 08:42:22 0.7 1.2 24.0 -0.1 

11/02/06 08:42:32 0.9 1.3 22.9 -0.1 

11/02/06 08:42:42 1.3 5.4 17.5 -0.1 

Page 2 86 
1112/06 Calibrations 

11/02/06 08:42:52 2.2 15.0 9.2 -0.1 

11/02106 08:43:02 1.5 14.6 4.5 -0.1 

11/02/06 08:43:12 0.4 15.5 2.4 0.0 

11/02/06 08:43:22 0.2 41.1 1.3 0.1 

11/02106 08:43:32 0.2 61.9 0.8 0.0 

11/02106 08:43:42 0.3 75.1 0.6 0.0 

11/02106 08:43:52 0.1 83.4 0.6 0.0 

11/02/06 08:44:02 0.1 87.3 0.7 0.0 

'\1/02/06 08:44:12 0.1 89.3 0.6 o.o 

11/02/06 08:44:22 0.1 90.9 0.3 0.0 

11/02106 08:44:32 0.0 92.1 0.3 -0.2 

11/02106 08:44:42 0.0 92.9 0.2 -0.2 

11/02106 08:44:52 0.0 93.4 0.1 -02 

11/02106 08:45:02 0.0 93.5 0.0 -0.2 

11/02106 08:45:12 0.0 93.9 0.0 -0.1 

11/02/06 08:45:22 0.0 94.2 0.0 -02 

11/02106 08:45:32 0.0 94.4 0.0 -0.1 

11/02106 08:45:42 0.1 94.5 0.0 -0.1 

11/02/06 08:45:52 0.1 94.9 0.0 -0.1 

11/02/06 08:46:02 0.1 94.6 0.0 0.0 99.1 ppm CO Bias 

11/02/06 08:46:12 0.1 94.7 0.0 -0.1 Zero 502 

11/02106 08:46:22 0.1 94.6 0.0 -0.1 

11/02/06 08:46:32 0.0 94.3 0.0 -0.1 

11/02106 08:46:42 0.1 94.0 0.0 -0.1 

'\ 1/02/06 08:46:52 0.0 84.2 0.0 0.0 

11/02106 08:47:02 0.0 52.8 0.0 1.9 

11/02106 08:47:12 0.0 27.5 0.0 7.6 

11/02/06 08:47:22 0.1 15.3 0.0 14.9 

11/02/06 08:47:32 0.1 9.7 0.0 21.4 

11102/06 08:47:42 0.1 7.3 0.0 26.5 

11102/06 08:47:52 0.0 5.6 0.0 302 

11/02106 08:48:02 0.1 4.3 0.0 33.0 

11/02/06 08:48:12 0.1 3.6 0.0 35.2 

11/02106 08:48:22 0.0 3.1 0.0 37.0 

11102106 08:48:32 0.0 2.5 0.0 38.4 

11/02106 08:48:42 0.0 2.3 0.0 39.5 

11/02/06 08:48:52 0.0 ~.0 0.0 40.6 

11/02106 08:49:02 0.1 1.4 0.0 41.6 

11/02106 08:49:12 0.0 1.3 0.0 42.2 

11/02106 08:49:22 0.1 1.3 0.0 42.8 

11/02/06 08:49:32 0.1 1.2 0.0 43.4 

11/02/06 08:49:42 0.0 1.2 0.0 44.0 

11/02/06 08:49:52 0.0 1.1 0.0 44.6 

11/02106 08:50:02 0.0 1.0 0.0 45.2 

11/02/06 08:50:12 0.0 1.0 0.0 45.7 

11/02106 08:50:22 0.0 1.0 0.0 46.1 

11/02106 08:50:32 0.0 1.1 0.0 46.6 

11/02/06 08:50:42 0.1 1.1 0.0 46.8 

11/02/06 08:50:52 0.0 1.1 0.0 47.1 

11/02/06 08:51:02 0.0 1.2 0.0 47.0 

11/02/06 08:51:12 0.1 1.3 0.0 47.0 49.2 ppm 502 

11/02/06 08:51:22 0.0 1.3 0.0 47.0 ZeroNOx 

11/02106 08:51:32 0.1 1.2 0.0 47.0 

11/02106 08:51:42 30.6 1.2 0.1 47.1 

11/02106 08:51:52 39.9 1.3 0.1 46.5 

11/02/06 08:52:02 39.9 1.4 0.0 44.4 

11/02106 08:52:12 39.9 1.5 0.1 38.7 

11/02106 08:52:22 40.2 1.3 0.0 27.9 

11/02106 08:52:32 40.7 1.1 0.0 19.3 

11/02/06 08:52:42 40.8 1.0 0.1 13.6 

11/02/06 08:52:52 40.8 0.9 0.1 10.1 40.8 ppm CH4 

11/02106 08:53:02 40.8 0.9 0.1 7.8 

11/02106 08:53:12 40.8 1.0 0.1 6.4 

11/02106 08:53:22 40.5 0.9 0.0 5.5 

11/02/06 08:53:32 37.9 0.9 0.0 4.7 

11/02/06 08:53:42 29.9 0.9 0.0 4.0 

11/02/06 08:53:52 9.3 1.0 0.0 3.8 

11/02/06 08:54:02 2.9 1.3 0.0 3.9 

11/02/06 08:54:12 2.6 1.3 0.0 5.3 

11/02/06 08:54:22 16.8 1.5 0.0 9.2 

11/02/06 08:54:32 19.1 1.3 0.0 14.9 

87 

Page3 
1112/06 Calibrations 

11/02106 08:54:42 19.1 1.1 0.0 16.8 

11/02/06 08:54:52 19.1 0.9 0.0 13.6 19.9 ppm CH4 

11/02/06 08:55:02 19.1 0.6 0.0 9.2 

11/02106 08:55:12 19.1 0.5 0.0 5.9 

11/02/06 08:55:22 19.1 0.4 0.0 3.9 

11/02/06 08:55:32 1s.s 0.6 0.0 2.8 

11/02106 08:55:42 17.4 0.6 0.0 2.0 

11/02106 08:55:52 12.1 0.5 0.0 1.7 

11/02/06 08:56:02 3.2 0,7 0.0 1.3 

11/02/06 08:56:12 2.6 . 0.8 0.0 1.2 

11/02/06 08:56:22 10.2 1.1 0.0 1.6 

11102/06 08:56:32 61.2 1.1 0.0 3.0 

11/02/06 08:56:42 62.7 1.2 0.0 4.9 

11/02/06 08:56:52 62.7 1.0 0.0 5.4 61.7ppm CH4 

11/02/06 08:57:02 62.7 0.9 0.0 4.3 

11/02/06 08:57:12 62.6 0.8 0.0 3.0 

11/02/06 08:57:22 62.4 0.8 0.0 2.0 

Page 4 

88 
1112/06 Run #1 

Oatemme voc co NOx 502 

mm/ddlyy hh:mm:ss ppm ppm ppm ppm 

11/02/06 09:14:52 38.3 76.8 22.0 2.1 

Stan Run#1 

11/02106 09:15:02 39.0 80.8 22.0 2.0 

11/02106 09:15:12 39.8 84.2 22.0 1.8 

11/02106 09:15:22 39.8 86.9 22.1 1.7 

11/02106 09:15:32 40.1 88.1 22.2 1.6 

11/02/06 09:15:42 40.3 89.6 22.1 1.7 

11/02/06 09:15:52 40.1 91.3 22.0 1.5 

11/02/06 09:16:02 39.6 93.0 22.0 1.3 

11102106 09:16:12 38.8 94.5 22.0 1.2 

11/02/06 09:16:22 38.1 96.0 21.8 1.3 

11/02/06 09:16:32 37.2 97.6 21.7 1.3 

11/02/06 09:16:42 35.8 98.7 21.7 1.2 

11/02106 09:16:52 34.9 99.3 21.7 1.1 

11/02106 09:17:02 34.0 99.7 21.7 0.9 

11/02106 09:17:12 32.6 99.8 21.7 0.9 

11/02/06 09:17:22 31.8 99.8 21.6 0.8 

11/02106 09:17:32 31.3 99.4 21.8 0.8 

11/02/06 09:17:42 31.0 98.6 21.7 0.8 

11/02106 09:17:52 30.4 98.4 21.6 0.7 

11/02106 09:18:02 30.3 98.0 21.5 0.7 

11/02106 09:18:12 31.0 97.9 21.5 0.7 

11/02/06 09:18:22 31.9 97.8 21.4 0.6 

11/02106 09:18:32 32.5 97.7 21.2 0.5 

11/02106 09:18:42 33.1 97.6 21.2 0.5 

11/02/06 09:18:52 33.7 97.4 21.2 0.6 

11/02106 09:19:02 34.3 97.6 21.2 0.6 

11/02106 09:19:12 34.8 97.6 21.2 • 0.5 

11/02106 09:19:22 34.7 98.0 21.2 0.4 

t 1/02106 09:19:32 34.4 98.1 21.2 0.5 

11/02/06 09:19:42 34.4 98.2 21.1 0.6 

11/02/06 09:19:52 34.2 98.4 21.2 0.5 

11/02/06 09:20:02 34.2 98.4 21.1 0.4 

11/02/06 09:20:12 33.9 98.6 21.2 0.4 

11/02/06 09:20:22 33.3 98.7 21.3 0.4 

11/02/06 09:20:32 32.9 98.6 21.3 0.4 

11/02/06 09:20:42 32.3 98.6 21.3 0.2 

11/02/06 09:20:52 31.8 98.7 21.4 0.2 

1 t/02106 09:21:02 31.8 98.4 21.4 0.1 

11/02/06 09:21:12 31.7 98.0 21.6 0.1 

11/02/06 09:21:22 31.6 97.5 21.6 0.1 

11/02/06 09:21:32 31.8 97.2 21.7 0.3 

11/02106 09:21:42 32.1 96.7 21.8 0.2 

11/02106 09:21:52 32.4 96.3 21.8 0.2 

11/02106 09:22:02 33.0 96.2 21.9 0.3 

11/02/06 09:22:12 33.5 96.0 21.9 0.3 

11/02/06 09:22:22 33.6 95.4 22.0 0.3 

11/02/06 09:22:32 34.0 95.0 22.0 0.3 

11/02106 09:22:42 34.1 94.8 21.9 0.2 

11/02106 09:22:52 34.2 94.5 22.0 0.2 

11/02106 09:23:02 34.0 94.1 21.9 0.3 

11/02106 09:23:12 33.8 94.1 21.9 0.2 

11/02/06 09:23:22 33.3 93.9 21.9 0.2 

11/02106 09:23:32 32.6 93.7 21.9 0.2 

11/02/06 09:23:42 31.9 93.4 21.8 0.1 

11/02/06 09:23:52 32.1 93.3 21.7 0.1 

11/02/06 09:24:02 31.6 93.4 21.5 0.2 

11/02106 09:24:12 30.9 93.8 21.3 0.2 

11/02/06 09:24:22 30.7 94.0 21.2 0.1 

11/02/06 09:24:32 30.4 94.4 21.1 0.1 

11/02/06 09:24:42 30.4 94.8 21.1 0.1 

11/02/06 09:24:52 30.8 94.6 21.1 0.1 

11/02/06 09:25:02 31.3 94.6 20.9 0.2 

11/02/06 09:25:12 32.3 94.2 20.9 0.1 

11/02/06 09:25:22 32.8 94.2 20.9 0.1 

11/02106 09:25:32 33.0 93.1 20.9 0.1 

11/02/06 09:25:42 33.2 91.1 20.9 0.1 

11/02106 09:25:52 33.6 88.5 20.9 0.1 

11/02106 09:26:02 33.7 87.0 21.0 0.1 

11102106 09:26:12 34.2 85.3 21.0 0.1 

11/02106 09:26:22 34.9 83.7 20.9 0.1 

Page 1 89 
11/2106 Run #1 

11/02/06 09:26:32 34.3 81.0 20.8 0.1 

11/02106 09:26:42 34.8 78.2 20.8 0.1 

11/02106 09:26:52 33.9 75.8 20.8 0.1 

11/02/06 09:27:02 32.9 74.4 20.9 0.1 

11/02/06 09:27:12 32.1 72.9 20.9 0.1 

11/02106 09:27:22 30.5 71.2 20.8 0.1 

11/02106 09:27:32 29.7 70.1 20.7 0.1 

11/02106 09:27:42 29.1 69.3 20.7 0.0 

11/02106 09:27:52 28.7 68.5 20.6 0.0 

11/02/06 09:28:02 28.2 67.8 20.6 0.1 

11/02/06 09:28:12 28.0 66.8 20.7 0.1 

11/02106 09:28:22 28.0 65.8 20.7 0.0 

11/02106 09:28:32 28.0 65.3 20.7 0.1 

11/02/06 09:28:42 28.1 64.8 20.6 0.1 

11/02/06 09:28:52 28.4 64.8 20.5 0.1 

11/02/06 09:29:02 28.8 65.3 20.2 0.1 

11/02106 09:29:12 29.7 66.4 20.1 0.1 

11/02106 09:29:22 30.9 67.8 20.0 0.0 

11/02106 09:29:32 31.7 69.1 19.8 o.o 

11/02/06 09:29:42 32.5 70.2 19.6 0.0 

11/02/06 09:29:52 32.9 70.9 19.6 0.0 

11/02/06 09:30:02 32.6 71.9 19.6 0.0 

11/02106 09:30:12 32.3 n.5 19.6 0.0 

11/02/06 09:30:22 32.1 72.5 19.7 0.0 

11/02/06 09:30:32 31.7 72.7 19.8 0.0 

11/02/06 09:30:42 31.2 72.8 19.8 0.0 

11/02/06 09:30:52 30.7 73.8 19.9 0.0 

11/02106 09:31:02 30.0 76.0 20.0 0.1 

11/02/06 09:31:12 29.2 78.8 20.0 0.0 

11/02/06 09:31 :22 28.4 82.1 20.1 0.1 

11/02106 09:31:32 27.9 85.3 20.3 0.0 . 11/02106 09:31:42 27.7 87.9 20.4 0.0 

11/02106 09:31:52 27.5 90.0 20.4 0.0 

11/02/06 09:32:02 27.6 91.9 20.5 0.0 

11/02/06 09:32:12 28.8 93.2 20.7 0.0 

11/02/06 09:32:22 29.6 93.7 20.8 0.0 

11/02106 09:32:32 29.9 94.0 20.9 0.0 

11/02106 09:32:42 30.0 94.3 21.0 0.0 

11/02/06 09:32:52 30.4 94.6 21.1 0.1 

11/02106 09:33:02 30.5 94.5 21.2 0.0 

11/02106 09:33:12 31.4 94.6 21.4 0.0 

11/02/06 09:33:22 32.2 94.7 21.5 0.0 

11102106 09:33:32 33.2 94.9 21.6 0.0 

11/02106 09:33:42 33.6 95.2 21.8 0.0 

11/02106 09:33:52 34.3 95.4 21.8 0.0 

11/02106 09:34:02 35.1 95.2 21.8 0.0 

11/02106 09:34:12 35.3 95.2 21.9 0.0 

11/02/06 09:34:22 35.1 95.3 22.1 0.1 

11/02/06 09:34:32 34.1 95.2 22.1 0.0 

11/02106 09:34:42 33.3 95.7 22.2 0.0 

11/02/06 09:34:52 32.8 95.7 22.2 0.0 

11/02/06 09:35:02 32.3 96.0 22.3 0.0 

11/02/06 09:35:12 31.7 96.0 22.5 0.0 

11/02106 09:35:22 30.9 95.7 22.6 0.0 

11/02/06 09:35:32 31.0 95.4 22.5 -0.1 

11/02/06 09:35:42 30.8 94.5 22.4 -0.1 

11/02106 09:35:52 31.1 93.8 22.5 -0.1 

11/02/06 09:36:02 31.2 93.2 22.4 -0.1 

11/02106 09:36:12 31.2 92.2 22.4 -0.1 

11/02106 09:36:22 30.6 91.8 22.4 0.0 

11/02/06 09:36:32 30.5 91.1 22.4 -0.1 

11/02/06 09:36:42 30.7 90.8 22.4 -0.2 

11/02/06 09:36:52 30.9 90.6 22.4 -0.1 

11/02/06 09:37:02 31.0 90.7 22.4 -0.2 

11/02106 09:37:12 31.4 90.9 22.4 -0.2 

11/02106 09:37:22 31.5 90.9 22.5 -0.3 

11/02106 09:37:32 31.9 90.9 22.5 -0.2 

11/02/06 09:37:42 32.2 90.9 22.6 -0.1 

11/02/06 09:37:52 32.3 90.8 22.7 -0.1 

11/02/06 09:38:02 32.1 90.8 22.7 ·0.2 

11/02/06 09:38:12 32.2 90.9 22.9 -0.2 

11/02/06 09:38:22 32.5 90.9 23.0 -0.2 

11/02106 09:38:32 32.7 90.9 23.0 0.0 

11/02/06 09:38:42 32.5 90.8 23.1 0.0 

Page 2 90 
1112/06 Run #1 

11102/06 09:38:52 32.3 90.5 23.1 0.0 

11/02/06 09:39:02 32.1 90.0 23.1 0.0 

11/02/06 09:39:12 32.1 89.4 23.1 -0.1 

11/02/06 09:39:22 31.7 88.8 23.1 -0.1 

11102106 09:39:32 31.4 88.2 23.0 -0.1 

11/02106 09:39:42 31.1 87.9 22.9 -0.1 

11/02106 09:39:52 30.6 87.7 22.7 -0.2 

11/02/06 09:40:02 30.3 87.9 22.6 -0.1 

11/02/06 09:40:12 30.3 88.2 22.5 -0.1 

11/02/06 09:40:22 30.3 89.0 22.4 -0.1 

11/02/06 09:40:32 30.2 90.0 22.4 -0.1 

11/02106 09:40:42 30.1 92.0 22.4 -0.1 

11/02/06 09:40:52 30.5 94.0 22.4 -0.2 

11/02/06 09:41:02 30.7 95.7 22.4 -0.2 

11/02/06 09:41:12 31.0 97.1 22.5 -0.1 

11/02106 09:41:22 31.5 98.0 22.6 0.0 

11/02106 09:41:32 31.9 98.1 22.6 0.0 

11/02/06 09:41:42 32.1 98.0 22.6 0.0 

11/02106 09:41:52 32.1 97.7 22.7 0.0 

11/02/06 09:42:02 32.1 96.9 22.7 0.0 

11/02106 09:42:12 32.6 96.5 22.7 0.0 

11/02106 09:42:22 32.9 95.8 22.8 0.0 

11/02/06 09:42:32 332 95.5 22.9 0.0 

11/02/06 09:42:42 33.1 952 22.8 0.0 

11/02/06 09:42:52 32.7 94.8 22.8 0.1 

11/02/06 09:43:02 32.1 94.7 22.8 0.1 

11/02/06 09:43:12 31.9 94.4 22.8 0.0 

11/02106 09:43:22 31.2 94.1 22.8 0.0 

11/02/06 09:43:32 30.9 94.0 22.8 -0.1 

11/02/06 09:43:42 30.4 93.4 22.8 -0.1 , 11/02106 09:43:52 29.9 93.4 22.9 0.0 

11/02/06 09:44:02 29.8 93.5 22.8 0.0 

11/02/06 09:44:12 29.6 93.5 22.8 0.0 

11/02106 09:44:22 28.9 93.3 22.7 0.0 

11/02106 09:44:32 28.4 93.0 22.8 0.0 

11/02/06 09:44:42 28.2 92.7 22.8 0.0 

11/02106 09:44:52 28.2 92.E,; 22.9 0.0 

11/02/06 09:45:02 28.6 92.6 22.9 0.0 

11/02106 09:45:12 29.0 92.9 22.9 0.0 

.11/02106 09:45:22 29.4 93.3 22.9 -0.1 

11102/06 09:45:32 29.9 93.9 22.9 -0.1 

-11/02/06 09:45:42 30.7 94.3 22.9 -0.1 

11/02106 09:45:52 31.5 94.8 22.9 -0.1 

11/02106 09:46:02 32.2 95.1 23.0 0.0 

11/02106 09:46:12 32.6 95.1 23.0 0.0 

11/02/06 09:46:22 33.0 95.3 23.0 0.0 

11/02106 09:46:32 33.3 95.2 23.0 0.0 

11/02/06 09:46:42 33.6 95.3 23.0 0.0 

11/02/06 09:46:52 33.7 95.4 22.9 0.0 

11/02/06 09:47:02 34.1 94.9 22.8 0.0 

11/02/06 09:47:12 33.6 94.7 22.8 0.0 

11/02/06 09:47:22 33.6 94.7 22.8 0.1 

11/02/06 09:47:32 33.7 94.8 22.9 0.1 

11/02106 09:47:42 32.7 95.0 22.9 0.0 

11/02106 09:47:52 32.1 95.1 22.9 -0.1 

11/02106 09:48:02 31.2 95.3 22.9 -0.1 

11/02/06 09:48:12 30.6 95.3 22.9 0.0 

11/02/06 09:48:22 30.1 95.1 22.9 0.0 

11/02/06 09:48:32 29.9 94.6 22.8 0.0 

11/02/06 09:48:42 30.0 94.2 22.7 0.0 

11/02106 09:48:52 29.6 93.9 22.7 0.0 

11/02/06 09:49:02 29.7 93.8 22.7 0.0 

11/02/06 09:49:12 29.8 93.5 22.6 0.0 

11/02106 09:49:22 29.7 93.9 22.6 -0.1 

11/02106 09:49:32 29.5 94.1 22.7 0.0 

11/02106 09:49:42 28.8 94.0 22.7 0.0 

11102/06 09:49:52 28.4 93.6 22.7 0.0 

11/02106 09:50:02 28.4 93.1 22.7 -0.1 

11102/06 09:50:12 28.8 92.4 22.7 -0.1 

11/02/06 09:50:22 29.2 91.7 22.8 -0.1 

11/02/06 09:50:32 29.8 91.2 22.8 -0.1 

11/02/06 09:50:42 30.4 90.9 23.0 -0.1 

11/02/06 09:50:52 312 90.7 23.1 -0.1 

11/02/06 09:51:02 32.0 90.2 23.2 -0.2 

Page 3 
11/2/06 Run #1 

11/02106 09:51 :12 32.2 90.2 23.2 -0.2 

11/02/06 09:51 :22 32.4 90.3 23.2 -0.2 

11/02/06 09:51:32 32.8 90.5 23.2 -0.2 

11/02/06 09:51:42 32.6 91.1 23.3 -0.2 

11/02/06 09:51 :52 33.1 91.4 23.4 -0.2 

11/02106 09:52:02 32.8 91.5 23.5 -0.2 

11/02106 09:52:12 32.7 91.6 23.5 -0.2 

11/02/06 09:52:22 32.9 91.7 23.5 -0.2 

11/02/06 09:52:32 33.1 92.0 23.5 -o.2 

11/02/06 09:52:42 32.2 92.0 23.5 -0.2 

11102/06 09:52:52 31.0 92.5 23.3 -0.1 

11/02/06 09:53:02 29.7 92.9 23.3 -0.1 

11/02/06 09:53:12 28.6 93.1 23.4 -0.2 

11/02106 09:53:22 27.4 93.2 23.5 -0.1 

11/02/06 09:53:32 27.0 92.8 23.3 0.0 

11/02/06 09:53:42 26.7 92.0 23.3 -0.1 

11/02/06 09:53:52 27.1 91.4 23.3 -0.1 

11/02/06 09:54:02 27.1 91.1 23.3 -0.1 

11/02/06 09:54:12 27.8 90.7 23.4 -0.1 

11/02106 09:54:22 28.1 90.2 23.4 -0.1 

11/02/06 09:54:32 28.9 89.8 23.4 -0.1 

11/02/06 09:54:42 29.4 90.3 23.4 -0.1 

11/02/06 09:54:52 30.0 90.4 23.4 -0.1 

11/02/06 09:55:02 31.1 89.6 23.2 -0.1 

11/02106 09:55:12 31.5 87.8 23.1 -0.1 

11/02/06 09:55:22 32.8 85.6 23.0 -0.1 

11/02106 09:55:32 33.2 83.3 22.9 0.0 

11/02/06 09:55:42 33.6 82.1 22.6 -0.1 

11/02/06 09:55:52 33.5 80.1 22.5 -0.2 

11/02/06 09:56:02 33.1 76.8 22.3 -0.2 

11/02106 09:66:12 32.6 73.9 22.2 0.0 

11/02/06 09:56:22 31.5 71.7 22.1 0.0 

11/02/06 09:56:32 30.3 71.0 22.0 0.0 

11/02106 09:56:42 28.4 70.8 21.8 -0.1 

11/02106 09:56:52 27.6 70.9 21.6 -0.1 

11/02/06 09:57:02 26.9 71.2 21.6 -0.1 

11/02/06 09:57:12 26.7 71.9 21.4 -0.1 

11/02/06 09:57:22 26.7 72.9 21.4 -0.1 

11/02/06 09:57:32 27.3 74.0 21.3 -0.2 

11/02106 09:57:42 28.1 75.8 21.2 -0.1 

11/02106 09:57:52 28.1 77.8 21.2 0.0 

11/02/06 09:58:02 29.4 79.5 21.1 0.0 

11/02/06 09:58:12 30.3 80.7 21.1 -0.1 

11/02106 09:58:22 30.5 81.2 21.0 -0.1 

11/02/06 09:58:32 31.4 81.5 21.1 -0.1 

11/02/06 09:58:42 32.0 81.5 21.1 -0.1 

11/02106 09:58:52 33.6 81.4 21.2 -0.1 

11/02106 09:59:02 35.2 81.5 21.1 -0.1 

11/02106 09:59:12 35.6 82.5 21.3 -0.1 

11/02/06 09:59:22 35.0 83.9 21.4 -0.1 

11/02106 09:59:32 34.7 85.5 21.5 -0.1 

11102106 09:59:42 34.1 87.1 21.5 -0.1 

11/02/06 09:59:52 33.0 88.0 21.6 -0.1 

11/02/06 10:00:02 32.0 87.9 21.6 -0.2 

11/0210610:00:12 30.7 86.3 21.6 -0.2 

11/02/06 10:00:22 29.9 83.3 21.6 -0.2 

11/02/06 10:00:32 29.7 80.8 21.5 -0.2 

11/02/06 10:00:42 29.2 79.1 21.3 -0.3 

11/02106 10:00:52 28.5 76.7 21.1 -0.2 

11/02/06 10:01:02 27.9 73.6 21.0 -0.2 

11/02/06 10:01:12 27.9 70.8 20.9 -0.3 

11/02/06 10:01:22 27.6 69.5 20.7 -0.3 

11/02106 10:01:32 27.8 68.2 20.6 0.0 

11/02/06 10:01 :42 27.8 67.2 20.4 -0.1 

11/02106 1 0:01 :52 27.8 66.8 20.4 -0.2 

11/02106 10:02:02 28.0 67.3 20.4 -0.2 

11/02/06 10:02:12 28.3 68.3 20.7 -0.1 

11/02/06 10:02:22 29.6 69.5 20.6 -0.1 

11/02/0610:02:32 30.3 69.9 20.4 -0.1 

11/02/0610:02:42 30.7 70.2 20.3 -0.1 

11/02106 10:02:52 30.8 70.2 20.2 0.0 

11/02/06 10:03:02 30.4 70.3 20.0 -0.1 

11/0210610:03:12 30.2 70.1 20.0 -0.1 

11/02/06 10:03:22 29.9 69.9 20.0 -0.1 

Page4 92 
11/2/06 Run #1 

11/02106 10:03:32 29.1 70.0 20.2 -0.1 

11/02106 10:03:42 29.4 70.4 20.2 0.0 

11/02106 10:03:52 29.6 71.2 20.4 0.0 

11/02106 10:04:02 29.4 73.5 20.6 -0.1 

11/02106 10:04:12 29.3 74.7 20.8 -0.2 

11/02106 10:04:22 28.8 74.6 20.8 -0.2 

11/02106 10:04:32 29.0 73.4 20.8 -0.2 

11/02106 10:04:42 28.7 n.9 20.7 -0.1 

11/02/0610:04:52 28.4 73.2 20.8 -0.1 

11/02106 1 0:05:02 28.7 72.3 20.8 0.0 

11/02106 10:05:12 29.3 70.5 20.7 -0.1 

11/02/06 10:05:22 30.3 68.5 20.8 -0.1 

11/02/06 10:05:32 30.3 66.9 20.7 -0.2 

11/02/06 10:05:42 30.9 66.1 20.6 -0.2 

11/02/06 10:05:52 30.8 64.7 20.7 -0.1 

11/02106 10:06:02 30.4 63.3 20.8 -0.1 

11102106 10:06:12 30.7 61.7 20.8 -0.2 

11/02/06 10:06:22 29.8 60.7 20.8 -0.3 

11/02106 10:06:32 29.8 60.4 20.8 -0.3 

11/02106 10:06:42 29.8 59.7 20.7 -0.2 

11/02106 10:06:52 29.6 59.0 20.8 -0.1 

11/02/06 10:07:02 29.3 58.3 20.6 -0.1 

11/02106 10:07:12 28.2 58.0 20.7 -0.1 

11/02/06 10:07:22 27.2 57.8 20.6 -0.2 

11/02/06 10:07:32 26.8 57.7 20.4 -0.2 

11/02106 10:07:42 26.5 58.7 20.3 -0.3 

11/02106 10:07:52 26.6 60.5 20.2 -0.3 

11/02106 10:08:02 26.7 62.1 20.0 -0.1 

11/02/06 10:08:12 27.0 63.7 19.9 -0.1 

11/02106 10:08:22 27.5 65.0 19.8 -0.1 

11/02106 10:08:32 . 27.4 66.6 19.8 -0.2 

11/02106 10:08:42 27.4 67.9 19.9 -0.2 

11/02106 1 0:08:52 27.2 68.4 20.2 -0.1 

11/02106 10:09:02 27.1 68.6 20.5 -0.1 

11/02/0610:09:12 27.6 68.9 20.7 -0.1 

11/02106 10:09:22 27.9 70.0 20.7 -0.1 

11/02/06 10:09:32 28.7 71.3 20.7 -0.2 

11/02106 10:09:42 29.7 74.7 20.5 -0.4 

11/02106 10:09:52 30.7 78.7 20.4 -0.5 

11/02106 10:10:02 32.2 82.6 20.2 -0.4 

11/02106 10:10:12 33.8 86.1 20.1 -0.3 

11/02106 10:10:22 34.5 88.2 20.0 -0.3 

1 1/02106 10:10:32 34.3 89.9 20.0 -0.2 

11/02/06 10:10:42 33.3 91.1 20.0 -0.2 

11/02/06 10:10:52 32.0 92.0 20.0 -0.2 

11/0210610:11:02 30.5 92.8 20.1 0.0 

11/02106 10:11:12 29.0 93.2 20.2 0.0 

11/0210610:11:22 26.6 93.3 20.4 0.0 

11/02106 10:11:32 26.1 93.1 20.6 0.0 

11/02106 10:11:42 25.6 92.9 20.8 0.0 

11/02/0610:11:52 25.5 92.5 20.9 0.0 

11/02/06 10:12:02 25.5 92.3 20.9 0.0 

11/02/06 10:12:12 26.0 91.7 21.0 0.0 

11/02/06 10:12:22 26.1 91.0 21.0 0.0 

11/02/06 10:12:32 25.7 90.0 21.0 -0.1 

11/02/0610:12:42 25.5 89.0 21.1 0.0 

11/02/0610:12:52 25.4 88.4 21.2 0.0 

11/0210610:13:02 25.7 88.2 21.2 0.0 

11/02/06 10:13:12 27.4 88.3 21.1 -0.1 

11/02/0610:13:22 29.3 88.8 21.1 0.0 

11/02/06 10:13:32 30.1 90.0 21.0 0.0 

11/02/06 10:13:42 30.5 91.0 21.0 0.0 

11/02/06 10:13:52 30.5 91.7 21.5 0.0 

11/02/06 10:14:02 31.0 92.1 22.5 -0.1 

11/02/06 10:14:12 31.2 92.7 23.0 -0.1 

11/02106 10:14:22 30.8 93.3 23.2 -0.1 

11/02106 10:14:32 30.2 94.0 23.3 -0.2 

11/02/06 10:14:42 29.7 94.3 23.2 -0.2 

11/02/06 10:14:52 29.1 94.5 22.8 -0.1 

11/02106 10:15:02 28.4 94.0 22.4 -0.1 

11/02/0610:15:12 26.9 92.7 22.0 -0.1 

11/02/06 10:15:22 25.7 90.5 21.8 -0.1 

11/02106 10:15:32 25.4 88.5 21.6 -0.1 

11/0210610:15:42 25.2 85.8 21.5 0.0 

93 

Page 5 
11/2/06 Run #1 

11/02/0610:15:52 25.6 82.4 21.4 0.0 

11/02/06 10:16:02 26.0 79.9 21.1 0.0 

11/02106 10:16:12 25.9 78.9 21.1 0.0 

11/02/06 10:16:22 26.2 79.9 21.0 0.0 

11/02106 10:16:32 26.2 83.1 21.2 -0.1 

11/02106 10:16:42 26.8 88.1 21.3 -0.1 

11/02106 10:16:52 27.5 93.2 21.4 -0.1 

11/02/06 10:17:02 28.0 98.3 21.5 -0.1 

11/02/0610:17:12 28.5 102.6 21.4 -0.1 

11/02/06 10:17:22 29.4 105.7 21.3 -0.1 

11/02/06 10:17:32 30.0 108.9 21.2 -0.1 

11/02/06 10:17:42 30.3 112.2 21.0 -0.1 

11/02/06 10:17:52 31.0 114.7 21.0 -0.1 

Stop Run #1 30.85 86.60 21.67 0.03 

11/02106 10:18:02 31.3 116.1 20.9 -0.1 

11/02106 10:18:12 32.1 116.2 20.9 -0.1 

11/0210610:18:22 14.4 116.3 20.7 -0.2 

11/02106 10:18:32 4.4 101.2 19.5 0.0 

11/02/06 10:18:42 4.8 59.9 13.1 0.0 

11/02106 10:18:52 5.1 32.5 8.9 -0.1 

11/02106 10:19:02 5.1 18.9 7.3 -0.1 

11/02/06 10:19:12 5.1 11.4 6.7 -0.2 

11/02106 10:19:22 5.1 6.2 6.3 -0.2 

11/02/06 10:19:32 5.2 3.4 5.8 -0.3 

11/02/0610:19:42 5.2 1.4 5.4 -0.3 

11/02/06 10:19:52 5.9 0.4 5.0 -0.4 

11/02/06 10:20:02 7.0 -0.2 8.3 -0.3 

11/02106 10:20:12 7.8 0.0 15.4 -0.3 

11/02/06 10:20:22 8.0 . 0.9 19.6 -0.4 

11/02/06 10:20:32 7.6 0.3 22.2 -0.4 

11/0210610:20:42 7.2 0.2 23.6 -0.3 

11/02/06 10:20:52 7.0 -0.2 24.4 -0.3 

11/02/06 10:21:02 6.4 -0.2 24.7 -0.1 

11/02/06 10:21:12 4.9 -0.1. 25.1 -0.1 

11/02106 1 0:21 :22 3.8 -0.2 25.1 -0.1 25 ppm NOx 

11/02/06 10:21:32 3.0 1.5 25.1 0.0 ZeroS02 

11/02106 10:21:42 2.4 . 2.7 25.0 -0.1 

11/0210610:21:52 2.0 2.6 25.1 -0.1 

11/02106 10:22:02 1.7 2.4 25.1 -0.1 

11/02/0610:22:12 1.3 4.1 24.0 ·0.2 

11/02/06 10:22:22 1.0 31.2 17.9 -0.2 

11/02/06 10:22:32 0.9 61.7 9.7 -0.2 

11/02/0610:22:42 0.8 78.7 5.6 -0.2 

11/02106 10:22:52 0.8 87.2 3.5 -0.2 

11/02/0610:23:02 0.8 90.5 2.5 -0.1 

11/0210610:23:12 0.8 92.6 2.0 0.0 

11/02/0610:23:22 0.7 94.0 1.7 -0.1 

11/02/06 10:23:32 0.5 94.7 1.5 0.0 

11/02106 10:23:42 0.5 95.4 1.3 -0.1 

11102106 10:23:52 0.5 95.7 1.2 -0.1 

11/02/06 10:24:02 0.5 96.0 1.1 -0.1 

11/02/06 10:24:12 0.5 96.3 1.0 ·0.1 

11/02106 10:24:22 0.5 96.4 0.9 -0.1 

11102/06 10:24:32 0.5 96.6 0.8 -0.2 

11/0210610:24:42 0.5 96.6 0.7 -0.1 99.1 ppm CO 

11/02/06 10:24:52 0.5 96.5 0.7 -0.1 

11/02106 10:25:02 0.5 96.6 0.6 -0.1 

11/02/06 10:25:12 0.5 96.6 0.6 0.0 

11/02/06 10:25:22 0.5 95.3 0.6 0.0 

11/02106 10:25:32 0.5 79.5 0.6 ·0.1 

11/02/06 10:25:42 0.5 46.9 0.6 0.1 

11/02/06 10:25:52 0.5 25.9 0.6 1.2 

11/02106 10:26:02 0.3 15.9 0.6 3.5 

11/02/0610:26:12 0.3 10.9 0.6 7.0 

11/02/06 10:26:22 0.5 8.2 0.5 10.8 

11/02/06 10:26:32 0.3 6.4 0.5 14.9 

11/02/06 10:26:42 0.3 5.4 0.5 18.7 

11/02/06 10:26:52 0.3 4.6 0.5 22.3 

11/02/0610:27:02 0.3 4.0 0.4 25.4 

11/02/0610:27:12 0.3 3.6 0.4 28.0 

Page 6 94· 
1112/06 Run #1 

11/02/06 10:27:22 0.3 3.4 0.4 30.2 

11/02/06 10:27:32 0.3 3.2 0.4 32.0 

11/02106 10:27:42 0.3 3.1 0.4 33.7 

11/02106 10:27:52 0.3 2.8 0.3 35.1 

11/02/0610:28:02 0.3 2.6 0.3 36.3 

11/02/06 10:28:12 0.3 2.5 0.3 37.4 

11/02/0610:28:22 0.3 2.6 0.3 38.3 

11/0210610:28:32 0.3 2.2 0.3 38.8 

11/02/06 10:28:42 0.2 1.8 0,3 39.4 

11/02/06 10:28:52 0.2 2.0 0.3 40.1 

11/02106 10:29:02 0.2 1.9 0.3 40.7 

11/02/06 10:29:12 0.2 2.0 0.3 41.3 

11/02106 10:29:22 0.2 1.9 0.3 41.6 

11/02106 1 0:29:32 0.2 1.8 0.3 41.9 

11/0210610:29:42 0.2 1.8 0.2 42.2 

11/02106 10:29:52 0.2 1.8 0.2 42.5 

11/02106 10:30:02 0.3 2.0 0.2 42.8 

11/02/0610:30:12 0.3 2.1 0.2 43.1 

11 /02/06 1 0:30:22 0.3 1.9 0.2 43.3 

11/02/06 1 0:30:32 0.2 1.8 0.2 43.6 

11/02/06 10:30:42 0.2 1.7 0.2 43.9 

11/0210610:30:52 0.2 1.8 0.2 44.0 

11/0210610:31:02 0.2 1.8 0.2 44.0 

11/02/0610:31:12 0.2 1.9 0.2 44.0 

11/02106 10:31:22 0.3 1.9 0.1 44.0 

11/0210610:31:32 0.2 1.9 0.1 44.0 

11/0210610:31:42 0.2 1.9 0.1 44.5 

11/02/0610:31:52 0.2 2.0 0.1 45.5 

11/02/0610:32:02 0.2 1.8 0.1 45.6 

11/02/06 10:32:12 0.2 1.7 0.1 45.7 

11/02106 10:32:22 0.2 1.9 • 0.2 46.0 

11/02106 10:32:32 0.2 2.3 0.1 46.3 

11/0210610:32:42 0.2 2.4 0.1 46.4 

11/02/0610:32:52 0.3 2.4 0.1 46.5 ZeroVOC 

11/02/06 10:33:02 0.2 2.3 0.1 46.8 

11/02/0610:33:12 0.2 2.2 0.1 47.1 49.8ppm 502 

11/02/06 10:33:22 1.0 2.2 0.1 47.4 Zero CO, NOx 

. 11/0210610:33:32 37.6 2.1 ·.0.2 47.0 

11/02106 10:33:42 42.4 2.1 0.2 46.7 

11/02/06 10:33:52 41.9 2.1 . 0.1 45.9 

11/02/0610:34:02 41.0 2.2 0.1 42.7 

11/02/0610:34:12 41.0 2.1 0.1 37.4 

11/02/06 10:34:22 41.0 2.1 0.1 31.7 

11/02106 10:34:32 41.1 2.0 0.1 26.5 

11/02/06 10:34:42 41.2 2.1 0.1 22.2 

95· 

Page7 
1112/06 Run #2 

Date/Time voc co NOx 502 

mrnldcllyy hh:mm:ss ppm ppm ppm ppm 

11/02106 10:39:52 24.2 125.8 21.9 0.5 

Start Run #2. 

11/02/06 10:40:02 24.4 126.6 22.2 0.4 

11/02106 10:40:12 24.7 127.3 22.2 0.4 

11/02/06 10:40:22 24.7 127.9 22.4 0.4 

11/02/06 10:40:32 24.9 128.2 22.4 0.3 

11/02/06 10:40:42 24.7 128.2 22.6 0.2 

11/02/06 10:40:52 24.8 128.3 22.4 0.1 

11/02/06 10:41:02 25.4 128.3 22.4 0.1 

11102/06 10:41:12 25.7 128.5 22.3 0.2 

11/02/0610:41:22 25.7 128.4 22.3 0.2 

11/02106 10:41:32 26.2 128.5 22.3 0.1 

11/0210610:41:42 26.3 128.7 22.2 0.1 

11/02/06 10:41:52 26.5 129.1 22.2 0.0 

11/02106 10:42:02 26.7 128.9 22.2 0.0 

11/02106 10:42:12 27.0 128.8 22.3 0.0 

11/02/06 1 0:42:22 27.4 128.7 22.5 0.0 

11/02/06 10:42:32 27.6 128.4 22.7 0.0 

11/02106 10:42:42 27.6 128.4 22.6 0.0 

11/02106 10:42:52 27.1 128.2 22.5 0.0 

11/02106 10:43:02 26.5 128.3 22.4 0.0 

11102/06 10:43:12 26.1 128.4 22.2 0.1 

11102106 10:43:22 25.8 128.6 22.0 0.0 

11/02/06 10:43:32 26.0 129.2 21.7 -0.1 

11/02106 10:43:42 25.8 130.1 21.5 -0.1 

11/02/06 10:43:52 25.7 131.2 21.2 0.0 

11/0210610:44:02 25.5 132.2 21.1 -0.1 

11/02/06 10:44:12 25.3 132.9 21.1 0.0 

11/02/06 10:44:22 24.8 133.0 21.2 -0.1 

11/02/0610:44:32 24.6 132.4 21.1 -0.1 

11/02/06 10:44:42 24.2 131.8 21.1 -0.2 

11/02/06 10:44:52 24.3 130.8 21.0 -0.2 

11/02106 10:45:02 24.6 130.5 21.0 -0.1 

11/02106 10:45:12 24.9 129.9 20.9 0.0 

11/02/06 10:45:22 25.9 129.6 20.9 -0.1 

11/02106 10:45:32 26.4 129.7 20.9 -0.3 

11/02106 10:45:42 26.8 129.6 20.9 -0.2 

11/02/06 10:45:52 27.0 129.8 21.0 -0.2 

11/02106 10:46:02 27.5 129.9 21.1 -0.-2 

11/02/0610:46:12 27.9 130.1 21.0 -0.2 

11/02/06 10:46:22 28.2 130.3 20.9 -0.2 

11/02/06 10:46:32 28.6 130.9 20.9 -0.3 

11/0210610:46:42 29.1 131.2 20.9 -0.3 

11/02106 10:46:52 28.8 131.2 20.9 -0.3 

11/02/06 10:47:02 28.4 131.1 20.9 -0.3 

11/02106 10:47:12 28.4 130.6 20.9 -0.2 

11/02/06 10:47:22 28.5 130.2 20.8 -0.2 

11/02106 10:47:32 27.8 129.6 20.7 -0.3 

11/02106 10:47:42 27.0 129.8 20.6 -0.2 

11/02/06 10:47:52 26.3 130.6 20.6 -0.4 

11/02/06 10:48:02 26.0 131.6 20.5 -0.4 

11/0210610:48:12 25.6 131.7 20.6 -0.3 

11/02/0610:48:22 25.7 131.8 20.7 -0.2 

11/02106 10:48:32 25.7 132.1 20.8 -0.4 

11/02/06 10:48:42 26.0 132.1 20.9 -0.3 

11/02/06 10:48:52 26.7 132.1 21.0 -0.3 

11/0210610:49:02 27.0 132.3 21.0 -0.3 

11102/0610:49:12 27.1 132.2 21.1 -0.3 

11/02/06 10:49:22 27.4 132.1 21.2 -0.3 

11/02106 10:49:32 28.0 131.6 21.2 -0.3 

11/02106 10:49:42 28.4 131.3 21.3 -0.4 

11/02106 10:49:52 28.7 131.0 21.4 -0.3 

11/02/06 10:50:02 29.8 130.5 21.4 -0.3 

11/02/06 10:50:12 30.1 130.2 21.7 -0.4 

11/02106 10:50:22 30.6 130.0 21.7 -0.4 

11/02/06 10:50:32 31.4 130.1 21.7 -0.4 

11102/06 10:50:42 31.8 130.7 21.7 -0.4 

11/02/06 10:50:52 31.2 131.1 21.8 -0.4 

11/02/06 10:51 :02 30.5 131.5 21.7 -0.5 

11/02106 10:51:12 29.5 131.6 21.7 -0.4 

11/02/06 10:51:22 28.9 131.6 21.6 -0.4 

Page 1 96 
11/2/06 Run #2 

11/02/0610:51:32 28.4 132.0 21.7 -0.4 

11/02/06 10:51:42 27.7 132.3 21.7 -0.4 

11/02/0610:51:52 27.1 132.6 21.7 -0.4 

11/02106 10:52:02 26.5 132.8 21.5 -0.5 

11/02/06 10:52:12 26.4 132.1 21.5 -0.6 

11102/06 10:52:22 26.3 131.7 21.4 -0.5 

11/02/0610:52:32 26.2 131.4 21.3 -0.4 

11/0210610:52:42 26.6 131.4 21.4 -0.3 

11/02/0610:52:52 27.2 131.7 21.3 -0.3 

11/02106 1 0:53:02 27.6 132.2 21.4 -0.3 

11/02106 10:53:12 28.4 132.7 21.4 -0.3 

11/02106 10:53:22 28.9 132.8 21.4 -0.3 

11/02106 10:53:32 29.2 133.0 21.3 -0.4 

11/0210610:53:42 29.8 133.2 21.3 -0.5 

11/02106 10:53:52 30.4 133.9 21.4 -0.5 

11/02106 10:54:02 31.2 134.5. 21.5 -0.4 

11/02/06 10:54:12 31.6 135.5 21.6 -0.5 

11/02/06 10:54:22 31.8 136.1 21.7 -0.4 

11/02/06 10:54:32 31.7 136.6 21.8 -0.2 

11/02/06 10:54:42 31.4 136.9 22.1 -0.1 

11/02/06 10:54:52 30.9 137.4 22.1 0.0 

11/02/06 10:55:02 30.2 138.3 22.0 0.0 

11/02/06 10:55:12 29.7 138.1 22.0 -0.1 

1 1/02106 10:55:22 29.5 136.6 21.9 0.0 

11/0210610:55:32 29.1 134.7 21.8 0.0 

11/02/0610:55:42 28.4 132.7 21.6 0.0 

11/02/06 10:55:52 27.9 130.9 21.5 0.0 

11102/06 10:56:02 27.1 128.9 21.4 -0.1 

11/02/0610:56:12 26.6 127.3 21.5 -0.1 

11/02/06 10:56:22 26.6 126.6 21.7 -0.1 

11/02/06 1 0:56:32 26.4 126.7 21.8 -0.1 

11/02/0610:56:42 26.3 127.7 21.8 -0.2 

11/02106 1 0:56:52 26.6 129.0 21.6 -0.3 

11/02/06 10:57:02 27.4 129.7 21.5 -0.2 

11/02/0610:57:12 27.6 130.4 21.4 -0.1 

11/02/06 10:57:22 27.7 131.2 21.3 -0.1 

11/02/06 10:57:32 28.2 131.5 21.4 -0.1 

11/02/06 10:57:42 28.4 131.9 21.5 0.0 

11/02106 10:57:52 29.1 132.1 21.5 -0.1 

11/0210610:58:02 29.9 132.1 21.6 -0.2 

11/02/06 10:58:12 30.9 132.0 21.6 -0.2 

11/0210610:58:22 31.4 132.0 21.5 .0.2 

11/02/06 10:58:32 32.3 132.1 21.4 -0.1 

11/02/0610:58:42 33.0 132.2 21.4 -0.1 

11/02/06 10:58:52 32.7 132.7 21.4 -0.1 

11/02/06 10:59:02 32.4 133.2 21.5 -0.1 

11/02106 10:59:12 31.8 133.9 21.6 -0.1 

11/02/06 10:59:22 31.0 134.5 21.5 -0.1 

11/02106 1 0:59:32 30.4 134.7 21.6 .0.2 

11/02/06 1 0:59:42 30.1 135.4 21.5 .0.2 

11/02/06 10:59:52 29.8 136.0 21.4 0.0 

11/02/06 11 :00:02 29.5 136.4 21.3 -0.1 

11/02/06 11:00:12 29.5 136.2 21.3 -0.2 

11/02/06 11:00:22 29.4 135.5 21.2 -0.2 

11/02/06 11 :00:32 28.9 135.2 21.2 ·0.2 

11/02/06 11:00:42 28.8 134.4 21.3 -0.2 

11/02/06 11:00:52 28.3 133.9 21.3 -0.3 

11/02106 11 :01 :02 28.4 133.7 21.3 -0.3 

11/02/0611:01:12 28.4 133.2 21.5 -0.2 

, 1/02/06 11 :01:22 29.0 133.1 21.5 -0.2 

11/02/06 11 :01:32 29.4 133.0 21.6 -0.2 

11/02/06 11 :01 :42 29.8 133.2 21.7 -0.2 

11/02106 11 :01 :52 31.0 133.1 21.6 -0.2 

11/02/06 11 :02:02 32.1 132.6 21.6 -0.1 

11/02/0611:02:12 32.9 131.8 21.5 -0.1 

11/02106 11 :02:22 34.0 130.7 21.5 -0.2 

11/02/06 11 :02:32 34.4 129.7 21.5 ·0.2 

11/02/06 11:02:42 34.5 129.3 21.5 -0.1 

11/02/06 11:02:52 34.2 128.8 21.5 -0.1 

11/02/06 11:03:02 34.0 128.7 21.4 -0.2 

11/02/06 11 :03:12 33.7 128.9 21.4 -0.2 

11/02/06 11:03:22 33.2 129.6 21.3 -0.2 

11/02106 11 :03:32 33.1 130.3 21.2 -0.2 

11/02/06 11:03:42 33.1 131.0 21.1 -0.1 

97 

Page 2 
1112/06 Run #2 

11/02/06 11:03:52 32.8 131.4 21.1 0.0 

11/02/06 11:04:02 32.1 131.4 21.1 0.0 

11/0210611:04:12 31.3 131.2 21.1 -0.1 

11/02/06 11:04:22 30.5 131.1 21.2 -0.2 

11/02/06 11 :04:32 30.0 130.9 21.3 -0.2 

11/02106 11:04:42 29.8 130.4 21.3 -0.3 

11/02/06 11:04:52 29.7 129.9 21.2 -0.2 

11/02/06 11 :05:02 30.2 129.7 21.2 -0.1 

11/02/06 11:05:12 30.6 129.9 2'1.2 -0.'1 

11/02/06 11:05:22 31.5 129.9 21.2 -0.1 

11/02/06 11 :05:32 31.8 130.1 21.2 -0.1 

11/02106 11 :05:42 32.6 130.2 21.2 -0.1 

11/02106 11 :05:52 33.3 130.8 21.4 -0.1 

11/02/06 11 :06:02 33.6 131.4 21.6 -0.2 

11/02/06 11 :06:12 34.1 131.5 21.6 -0.2 

11/02/06 11:06:22 34.3 131.5 21.7 -0.2 

11/02106 11:06:32 34.4 131.7 21.7 -0.1 

11/02/06 11:06:42 34.0 132.2 21.7 -0.1 

11102106 11:06:52 33.6 132.6 21.6 -0.2 

11/02/06 11 :07:02 32.9 133.1 21.6 -0.2 

11/02/0611:07:12 32.1 133.1 21.5 -0.1 

11/02/06 11:07:22 31.4 133.2 21.4 -0.1 

11/02/06 11:07:32 30.5 132.8 21.4 -0.1 

11/0210611:07:42 29.7 132.9 21.5 -0.1 

11/02106 11 :07:52 29.7 132.9 21.7 -0.2 

11/02/06 11 :08:02 29.7 132.9 21.7 -0.3 

11/02/06 11:08:12 29.6 133.0 21.7 -0.2 

11/02/06 11:08:22 29.8 132.8 21.7 -0.2 

11/02106 11:08:32 30.3 132.7 21.7 -0.3 

11/02106 11 :08:42 30.9 132.3 21.7 -0.3 

11/02106 11:08:52 31.5 132.4 21.7 -0.3 

11/02106 11:09:02 31.8 132.4 21.7 -0.3 

11/02/06 11 :09:12 322 131.8 21.8 -0.4 

11102/06 11 :09:22 32.5 131.6 21.9 -0.3 

11/02/06 11:09:32 33.2 131.1 21.8 -0.3 

11/02106 11 :09:42 33.6 131.0 21.8 -0.2 

11/02106 11 :09:52 33.9 130.7 21.7 -0.2 

11/02/06 11:10:02 34.7 131.2 21.6 -0.3 

11/0210611:10:12 34.2 131.2 21.6 -0.3 

11/02106 11:10:22 33.6 131.3 21.7 -0.3 

11/02/0611:10:32 33.1 131.3 21.7 -0.3 

11/02/06 11:10:42 32.2 131.8 21.7 -0.2 

11/02/0611:10:52 31.6 132.2 21.8 -0.3 

11/02/06 11:11:02 30.9 132.5 21.8 -0.3 

11/02/0611:11:12 30.6 132.9 21.8 -0.2 

11/02/06 11:11:22 29.9 133.0 21.9 -0.3 

11/02/06 11:11:32 29.8 133.3 21.7 -0.2 

11/02106 11:11:42 30.0 133.1 21.8 -0.2 

11/02/0611:11:52 30.1 133.1 21.8 -0.3 

11/02/0611:12:02 29.7 132.1 22.6 -0.3 

11/02/06 11:12:12 29.0 130.4 24.0 -0.5 

11/02/06 11:12:22 28.9 129.6 24.6 -0.5 

11102/0611:12:32 28.9 129.4 24.5 -0.3 

11/02/06 11:12:42 29.1 130.3 24.0 -0.3 

11/02/06 11:12:52 29.5 131.2 23.4 -0.2 

11/02/06 11:13:02 29.8 131.9 23.1 -0.3 

11/02/0611:13:12 29.9 132.3 23.0 -0.3 

11/0210611:13:22 30.1 132.1 22.9 -0.3 

11102106 11 :13:32 30.2 132.0 23.0 -0.4 

11/02/06 11:13:42 30.1 132.3 23.0 -0.4 

11/02/0611:13:52 30.1 132.3 23.0 -0.3 

11/02/06 11:14:02 29.7 132.2 23.0 -0.4 

11/02/0611:14:12 29.3 132.3 22.9 -0.5 

11/02/0611:14:22 29.1 132.6 22.8 -0.3 

11/02/0611:14:32 28.7 132.4 22.7 -0.4 

11/02/06 11 :14:42 28.1 132.2 22.5 -0.5 

11/02106 11:14:52 28.1 131.6 22.5 -0.6 

11/02/06 11:15:02 28.6 130.9 22.4 -o.s 

11/02/06 11:15:12 29.0 130.3 22.3 -0.4 

11/02/06 11:15:22 29.1 129.9 22.2 -0.4 

11/02/06 11:15:32 29.6 129.0 22.2 -0.4 

11/02/06 11:15:42 30.3 128.1 22.2 -0.4 

11/02106 11 :15:52 30.9 127.6 22.1 -D.4 

11/02/06 11:16:02 31.9 127.5 21.9 -0.3 

Page 3 98 
11/2106 Run #2 

11/02/06 11:16:12 33.2 127.0 21.8 -0.4 

11/02/06 11:16:22 33.9 126.7 21.6 -0.3 

11/02/06 11:16:32 34.3 126.8 21.6 -0.4 

11/02/06 11:16:42 34.1 127.1 21.8 -0.5 

11102/06 11:16:52 33.1 127.2 22.6 -0.5 

11102/0611:17:02 32.2 127.2 23.5 -0.5 

11/02/0611:17:12 31.6 127.3 23.9 -0.4 

11102/06 11:17:22 30.8 127.7 24.0 -0.4 

11/02/0611:17:32 29.5 127.9 23.8 -0.5 

11/02/06 11:17:42 28.7 127.6 23.6 -0.6 

11/02/06 11:17:52 28.2 127.4 23.5 -0.6 

11/02/06 11 :18:02 27.8 127.6 23.4 -0.5 

11/02/06 11:18:12 27.2 128.0 23.3 -0.4 

11/02/06 11 :18:22 27.2 128.1 23.3 -0.3 

11/02/06 11:18:32 27.5 128.7 23.2 -0.4 

11/02/06 11 :18:42 27.7 128.9 23.2 -0.4 

11/02/06 11 :18:52 27.4 129.1 23.1 -0.5 

11/02/06 11:19:02 27.4 1292 23.1 -0.5 

11/02/0611:19:12 27.5 129.0 23.2 -0.4 

11/02/06 11:19:22 27.9 129.0 23.3 -0.4 

11/02/06 11:19:32 28.1 128.5 23.1 -0.5 

11/02106 11:19:42 28.3 128.4 23.2 -0.5 

11/02106 11:19:52 28.7 128.5 23.3 -0.5 

11/02/0611:20:02 28.9 128.5 23.3 -0.6 

11/02/0611:20:12 29.4 129.0 23.2 -0.5 

11/02/06 11 :20:22 29.6 129.9 23.0 -0.6 

11/02/06 11 :20:32 29.6 130.7 22.9 -0.5 

11/02/06 11 :20:42 29.8 131.3 22.8 -0.6 

11/02106 11 :20:52 30.1 131.6 22.8 -0.6 

11/02/06 11:21:02 30.0 131.6 22.7 -0.5 

11/02/0611:21:12- 28.7 131.4 22.6 -0.5 

11/02/0611:21:22 28.2 130.9 22.6 -0.6 

11/0210611:21:32 27.7 130.6 22.7 -0.7 

11/02106 11:21:42 27.2 129.9 22.7 -0.6 

11/0210611:21:52 26.3 128.7 23.2 -0.5 

11/02106 11:22:02 25.7 127.7 23.5 -0.6 

11/02106 11:22:12 25.3 127.5 23.7 -0.7 

11/02/0611:22:22 25.3 127.6 23.6 -0.7 

11/0210611:22:32 25.5 128.4 23.5 -0.6 

11/0210611:22:42 . 25.9 128.9 23.5 -0.5 

11/02/06 11 :22:52 26.4 129.5 23.4 -0.6 

11/02/06 11:23:02 . 26.7 129.6 23.2 -0.7 

11/0210611:23:12 27.4 129.4 23.2 -0.8 

11/02/06 11 :23:22 27.6 129.2 23.2 -0.8 

11/02106 11 :23:32 27.6 128.6 23.4 -0.7 

11/02/06 11:23:42 27.4 127.7 23.7 -0.7 

11/02106 11 :23:52 27.1 126.8 24.1 -0.7 

11/02106 11:24:02 26.7 126.5 24.4 -0.7 

11/02/0611:24:12 26.8 126.4 24.5 -0.8 

11/02106 11:24:22 26.9 126.3 24.5 -0.8 

11/02106 11:24:32 27.3 126.6 24.7 -0.8 

11/02/0611:24:42 27.7 126.7 24.6 -0.9 

11/02106 11 :24:52 28.0 127.1 24.4 -0.9 

11/02/06 11:25:02 27.7 127.2 24.0 -0.9 

11/0210611:25:12 27.6 127.1 23.7 -0.9 

11/0210611:25:22 27.2 126.4 23.5 -0.9 

11/02/06 11 :25:32 26.9 125.8 23.5 -0.8 

11/02/06 11 :25:42 26.2 125.0 23.7 -0.8 

11/02/06 11:25:52 25.6 124.3 23.9 -0.7 

1 ,02106 11 :26:02 25.4 '\23.8 24.1 -0.8 

11/02/06 11:26:12 25.3 123.6 24.2 -0.8 

11/02/06 11:26:22 25.0 123.7 24.1 -0.9 

11/02/06 11 :26:32 25.5 124.1 23.9 -0.9 

11/02/06 11:26:42 25.5 124.7 23.5 -0.7 

11/02106 11:26:52 26.0 125.7 23.2 -0.7 

11/02/06 11:27:02 26.1 126.6 23.0 -0.7 

11102106 11 :27:12 26.5 127.6 22.9 -0.7 

11102/06 11 :27:22 26.6 128.4 23.0 -0.7 

11/02/06 11 :27:32 26.7 128.9 23.2 -0.8 

11/02/06 11:27:42 27.1 129.3 23.2. -0.8 

11/02106 11:27:52 27.4 129.4 23.1 -0.7 

11/02/06 11 :28:02 28.2 129.4 23.1 -0.8 

11/02106 11 :28:12 29.3 129.3 23.1 -0.8 

11/02/06 11:28:22 29.8 129.4 23.0 -0.8 

Page 4 99 
11/2/06 Run #2 

11/02106 11:28:32 30.2 129.1 22.9 -0.9 

11/02/06 11 :28:42 30.5 129.1 22.9 -0.8 

11/02/06 11:28:52 30.2 129.0 22.9 -0.8 

11/02/06 11:29:02 29.9 128.7 22.8 ..0.9 

11/02/06 11 :29:12 29.7 128.3 22.8 -0.9 

11/02106 11:29:22 28.9 128.1 22.7 ..0.8 

11/02/06 11 :29:32 29.0 127.9 22.9 -0.9 

11/02/06 11 :29:42 28.9 128.1 23.1 -0.9 

11/02/06 11 :29:52 28.1 128.7 23.2 ...().8 

11/02/06 11:30:02 27.7 128.9 23.4 -0.8 

11/02/06 11:30:12 27.1 129.0 23.6 -0.8 

11 /02/06 11 :30:22 26.5 128.7 23.6 -0.9 

11/02/0611:30:32 25.8 128.2 23.4 -0.9 

11/02106 11 :30:42 26.1 127.8 23.3 -0.9 

11/02/06 11 :30:52 26.2 127.4 23.2 -0.8 

11/02/06 11 :31:02 26.3 127.1 23.1 ..0.8 

11/02/0611:31:12 25.6 127.1 23.0 ..0.8 

11102/06 11:31:22 24.8 126.2 23.6 ..0.8 

11/02/06 11:31:32 24.2 125.2 24.2 -0.9 

11/02/06 11:31:42 23.6 124.5 24.5 -0.9 

11/02/06 11:31 :52 23.5 124.1 24.8 -0.8 

11/02106 11:32:02 23.8 124.0 25.3 ..0.8 

11/02106 11:32:12 24.3 124.5 25.8 ..0.9 

11/02/06 11 :32:22 24.4 125.1 25.5 -1.0 

11/02/0611:32:32 25.1 125.6 24.6 -0.9 

11/02/06 11:32:42 25.5 126.0 23.8 ..0.9 

11/02/06 11 :32:52 25.4 125.7 23.5 -0.9 

11/02/06 11:33:02 25.5 125.6 23.4 -0.9 

11/02/06 11:33:12 26.1 125.3 23.3 -1.0 

11/02/06 11 :33:22 26.3 125.1 23.3 -1.0 

11/02/06 11:33:32 26.9 125.2 23.3 -1.1 

11/02/06 11 :33:42 27.0 125.4 23.3 -1.1 

11102/06 11 :33:52 26.7 125.1 23.1 -0.9 

11/02/0611:34:02 26.1 124.7 22.7 -0.9 

11/02/0611:34:12 24.7 124.3 22.7 -1.0 

11/02/06 11 :34:22 23.5 123.4 23.2 -1.0 

11/02/0611:34:32 22.5 122.3 23.7 -1.1 

11/02/06 11 :34:42 21.6 121.1 24.2 -1.2 

11/02/06 11 :34:52 21.2 120.1 24.6 -1.2 

11/02/0611:35:02 21.f. 119.4 24.9 -1.2 

11/02/0611:35:12 19.8 119.5 25.4 -1.2 

11/02/06 11 :35:22 20.1 119.7 26.1 -1.1 

11/02/06 11 :35:32 21.5 120.5 26.6 -1.0 

11/02/06 11:35:42 22.4 121.5 25.7 -1.0 

11/02/06 11 :35:52 23.3 122.7 24.5 -1.1 

11/02/0611:36:02 24.1 123.4 23.8 -1.1 

11/02/0611:36:12 25.5 125.2 23.5 -1.2 

11/02/06 11:36:22 27.1 126.6 23.3 -1.1 

11/02106 11 :36:32 28.9 127.0 23.3 -1.2 

11/02/06 11:36:42 30.2 127.4 23.2 -1.1 

11/02/06 11 :36:52 31.2 127.9 23.1 -1.2 

11/02/06 11:37:02 31.5 128.5 22.8 -1.2 

11/02/06 11:37:12 31.8 128.6 22.5 -1.2 

11/02/06 11:37:22 32.1 127.9 22.4 -1.2 

11/02/06 11:37:32 31.5 126.7 22.4 -1.1 

11/02/06 11:37:42 31.4 125.5 22.3 -1.1 

11/02/06 11 :3 7:52 30.4 124.0 22.4 -1.1 

11/02/0611:38:02 29.8 122.4 22.4 -1.1 

11/02/0611:38:12 29.5 119.0 22.4 -1.1 

11/02/06 11:38:22 28.4 114.5 22.6 -1.2 

11/02/06 11 :38:32 26.5 109.2 23.0 -1.2 

11102/06 11 :38:42 25.5 104.7 23.8 -1.3 

11/02/06 11 :38:52 25.3 100.1 24.4 -1.2 

11/02/06 11 :39:02 25.4 95.6 24.7 ·1.3 

11/02/06 11:39:12 25.5 92.0 24.9 -1.2 

11/02/06 11 :39:22 25.7 88.9 25.0 -1.3 

11/02/06 11 :39:32 26.0 87.3 24.9 -1.4 

11/02/06 11:39:42 26.3 86.0 24.7 -1.4 

11/02/06 11 :39:52 26.7 85.4 24.5 -1.1 

11/02/06 11 :40:02 26.6 85.5 24.1 -0.9 

11/02/0611:40:12 25.6 85.5 23.8 ·0.1 

11/02/06 11 :40:22 24.4 84.6 24.2 ·0.2 

11/02/06 11 :40:32 23.1 85.0 24.6 0.0 

11/02/06 11:40:42 22.6 86.6 25.1 0.0 

Page 5 100 
1112/06 Run #2 

11/02/06 11 :40:52 22.3 88.6 26.0 -0.1 

11/02106 11 :41:02 22.2 91.4 26.5 -0.1 

11/02106 11:41:12 21.8 93.9 27.0 -0.1 

11/02106 11:41:22 21.7 95.2 27.7 -0.1 

11/02/06 11:41:32 21.7 96.0 28.6 -0.2 

11/02/0611:41:42 22.0 95.9 28.7 -0.3 

11/02./0611:41:52 22.3 95.1 27.0 -0.1 

11/02/0611:42:02 22.6 93.5 25.6 -0.1 

11/0210611:42:12 23.7 91.8 24.9 -0.2 

11/02/06 11 :42:22 25.1 91.5 24.4 -0.2 

11/02/06 11 :42:32 25.7 93.1 24.1 -0.2 

11/02106 11 :42:42 26.3 95.1 23.7 -0.1 

11/02106 11:42:52 27.3 97.7 23.5 0.0 

Stop Run #2 28.25 126.99 22.55 -0.44 

11/02/06 11:43:02 27.9 100.5 23.2 0.0 

11/02/0611:43:12 27.8 103.8 22.7 -0.1 

11/02/06 11:43:22 26.8 105.9 22.6 -0.2 

11/02/06 11:43:32 13.6 107.2 23.0 -0.3 

11/02/06 11 :43:42 6.3 88.4 21.4 -0.3 

11/02106 11:43:52 6.4 51.2 14.9 -0.2 

11/02/0611:44:02 6.1 27.1 10.9 -0.4 

11/02/06 11:44:12 6.0 14.7 9.0 -0.5 

11/02/06 11:44:22 6.0 7.9 7.6 -0.5 

11/0210611:44:32 6.0 4.7 6.7 -0.4 

11/02/0611:44:42 6.0 2.8 6.4 -0.4 

11/02/06 11 :44:52 6.2 1.6 6.3 -0.3 

11/02/06 11 :45:02 7.6 7.7 6.5 -0.3 

11/02/0611:45:12 7.0 41.6 5.7 -0.2 

11/0210611:45:22 6.2 65.2- 4.6 -0.3 

11/02/06 11:45:32 5.5 76.6 3.7 -0.3 

11/02106 11:45:42 4.9 84.1 3.1 -0.3 

11/02/06 11 :45:52 4.4 87.7 2.5 -0.3 

11/0210611:46:02 3.9 89.5 2.3 -0.3 

11/02/0611:46:12 3.4 91.0 2.1 -0.3 

11/02/06 11:46:22 2.7 91.6 1.9 -0.3 

11/02106 11:46:32 2.3 92.3 1.7 -0.3 

11/02106 11:46:42 2.1 92.1 1.6 -0.4 

11/02106 11 :46:52 2.0 93.3·· 1.6 -0.3 

11/02/06 11:47:02 1.6 94.5 1.5 -0.4 

11/02106 11:47:12 1.4 94.4' 1.5 -0.3 99.1 ppm CO 

11/02/06 11:47:22 1.2 94.4 1.4 -0.4 Zero S02 

11/02/06 11:47:32 1.2 94.2 1.4 -0.5 

11/02/06 11 :47:42 1.2 92.2 1.4 -0.4 

11/02/06 11 :47:52 1.2 90.6 1.4 -0.4 

11/02106 11 :48:02 1.2 82.1 1.3 -0.5 

11/02/0611:48:12 1.2 52.4 6.2 -0.6 

11/02106 11 :48:22 1.0 25.6 15.3 -0.6 

11/02/06 11:48:32 1.0 12.5 20.0 -0.5 

11/02/06 11 :48:42 1.0 5.9 22.2 -0.5 

11/02106 11:48:52 1.0 3.0 23.3 -0.5 

11/02106 11:49:02 1.0 1.4 23.7 -0.5 

11/02/06 11 :49:12 1.0 0.7 24.0 -0.5 

11/02106 11 :49:22 1.0 0.3 24.1 -0.6 

11/02106 11:49:32 1.0 0.2 24.3 -0.6 

11/02/0611:49:42 1.0 -0.1 24.4 -0.7 

11/02/06 11 :49:52 1.0 -0.2 24.4 -0.7 

, 1/02/06 11:50:02 1.0 -0.3 24.4 -0.6 

11/02/0611:50:12 1.0 0.3 24.4 -0.6 25 ppm NOx 

11/02/06 11 :50:22 1.0 0.7 24.5 -0.6 Zero CO 

11/02/06 11 :50:32 1.0 0.6 24.5 0.0 

11/02106 11 :50:42 1.1 0.5 24.4 0.0 

11/02106 11 :50:52 1.2 0.5 24.1 0.0 

11/02106 11 :51:02 1.2 0.6 21.1 0.0 

11/02/0611:51:12 2.4 0.5 17.9 0.0 

11/02/06 11 :51 :22 3.1 0.7 15.1 0.0 

11/02/06 11:51:32 2.1 0.9 8.8 0.0 

11/02/06 11:51:42 1.0 0.8 4.3 0.0 

11/02/06 11:51:52 1.0 0.8 2.4 0.1 

11/02/06 11 :52:02 1.0 0.6 1.7 0.6 

11/02/0611:52:12 1.0 0.5 1.6 2.0 

PageS 10'1 
11/2/06 Run #2 

11/02/06 11:52:22 1.0 0.4 1.4 4.0 

11/02/06 11 :52:32 1.0 0.3 1.2 6.4 

11/02/06 11 :52:42 1.0 0.4 1.1 9.0 

11/02/06 11:52:52 1.0 0.3 1.0 11.6 

11/02106 11:53:02 0.9 0.3 0.9 14.4 

11/02/06 11:53:12 1.0 0.3 0.9 17.2 

11/02/06 11:53:22 1.0 0.3 0.8 19.8 

11/02/06 11:53:32 1.0 0.3 0.7 22.1 

11/02/06 11:53:42 1.0 0.3 0.7 24.3 

11/02/06 11:53:52 1.0 0.3 0.6 26.2 

11102/06 11:54:02 1.0 0.3 0.6 27.9 

11/02/06 11 :54:12 1.0 0.3 0.6 29.6 

11102/06 11:54:22 1.0 0.3 0.5 31.2 

11/02/06 11 :54:32 1.0 0.3 0.5 32.5 

11/02/06 11 :54:42 1.0 0.3 0.5 33.8 

11102/06 11:54:52 1.0 0.3 0.4 35.1 

11/02/06 11:55:02 1.0 0.3 0.4 36.0 

11/02/06 11 :55:12 1.0 0.3 0.4 37.1 

11/02/06 11:55:22 1.0 0.3 0.4 38.0 

11/02/06 11 :55:32 1.0 0.5 0.4 38.6 

11/02/06 11 :55:42 1.0 0.5 0.3 39.0 

11/02/06 11:55:52 1.0 0.5 0.4 39.2 

11/02/06 11 :56:02 1.0 0.5 0.3 39.5 

11/02106 11:56:12 1.0 0.5 0.3 40.1 

11/02/06 11:56:22 1.0 0.5 0.3 40.5 

11/02/06 11 :56:32 1.1 0.3 0.3 40.6 

11/02/06 11 :56:42 1.2 0.3 0.3 41.2 

11/02/06 11:56:52 1.1 0.3 0.3 41.6 

11/02/06 11:57:02 1.0 0.2 0.3 42.1 

11/02106 11:57:12 1.0 0.2 0.3 42.4 

11/02/06 11:57:22 1.0 0.2 0.2 . 42.7 

11/02/06 11:57:32 1.0 0.2 0.2 43.1 

11/02/06 11:57:42 1.0 0.3 0.2 43.4 

11/02/06 11 :57:52 1.0 0.3 0.2 43.6 

11/02/06 11:58:02 1.0 0.3 0.2 43.9 

11/02/0611:58:12 1.0 0.3 0.2 44.2 

11/02/06 11 :58:22 1.0 0.3 0.2 44.4 

11/02/06 11 :58:32 1.0 0.4 0.2 44.7 

11/02/06 11 :58:42 1.0 0.4 0.2 44.9 

11/02106 11 :58:52 1.0 0.3 0.1 45.2 

11/02/06 11:59:02 1.0 0.3 0.2 45.4 

11/02/06 11 :59:12 1.0 0.3 0.1 45.5 

11/02106 11 :59:22 1.0 0.2 0.1 45.7 

11/02106 11 :59:32 1.0 0.2 0.1 45.8 

11102106 11 :59:42 1.0 0.2 0.1 45.9 

11/02/06 11:59:52 1.0 0.2 0.1 46.0 

11/02/06 12:00:02 1.0 0.3 0.1 46.1 

11/02/06 12:00:12 1.0 0.3 0.1 46.2 ZeroVOC 

11/02/06 12:00:22 1.0 0.3 0.2 46.4 

11/02/06 12:00:32 1.0 0.3 0.1 46.4 49.8 ppm 502 

11102/06 12:00:42 1.1 0.3 0.1 46.5 Zero NOx 

11/02/06 12:00:52 3.3 0.3 0.2 46.6 

11/02/06 12:01:02 39.6 0.3 0.2 46.4 

11/02106 12:01:12 42.0 0.3 0.1 46.1 

11/02/06 12:01:22 42.2 0.3 0.1 45.2 

11/02/0612:01:32 42.1 0.3 0.1 42.1 

11/02/0612:01:42 41.6 0.3 0.1 37.9 40.8 ppmCH4 

11/02/06 12:01 :52 41.5 0.2 0.0 33.6 

11/02/06 12:02:02 41.6 0.2 0.0 29.6 

11/02/06 12:02:12 38.7 0.3 0.1 25.8 

Page 7 

102 
11/2/06 Run #3 

Date/Time voc co NOx 502 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

11/02/06 12:09:52 27.5 123.2 20.0 0.2 

Stan Run #3 

11/02106 12:10:02 26.8 123.4 19.8 0.2 

11/02106 12:10:12 26.3 123.4 19.8 0.1 

11/02/0612:10:22 25.5 123.4 19.7 0.0 

11/02106 12:10:32 25.3 123.4 19.8 0.0 

11/02/06 12:10:42 25.4 123.2 19.6 0.1 

11/02/06 12:10:52 25.4 122.7 19.6 0.1 

11/02/06 12:11:02 25.5 122.5 19.5 0.1 

11/0210612:11:12 25.4 122.1 19.5 0.1 

11/02/06 12:11:22 25.3 121.5 19.5 0.1 

11/02/0612:11:32 24.9 121.1 19.5 0.0 

11/02/06 12:11:42 24.9 121.1 19.6 0.0 

11/02/06 12:11:52 25.3 120.8 19.6 -0.1 

11/02/0612:12:02 25.8 121.0 19.7 -0.2 

11/02106 12:12:12 26.2 120.6 19.8 -0.1 

11/02/06 12:12:22 26.7 120.6 19.8 -0.1 

11/02/06 12:12:32 27.3 113.1 20.0 -0.1 

11/02/06 12:12:42 28.2 120.7 20.1 -0.2 

11/02/06 12:12:52 29.2 120.8 20.1 -0.3 

11/02/06 12:13:02 29.8 120.9 20.1 -0.3 

11/02/0612:13:12 30.0 121.3 20.2 -0.2 

"\1/02/0612:13:22 29.8 121.9 20.2 -0.1 

11/02/06 12:13:32 29.6 122.0 20.3 -0.2 

11/02/0612:13:42 29.4 122.5 20.2 -0.2 

11/02/06 12:13:52 29.5 122.6 20.3 -0.3 

11102/06 12:14:02 29.8 122.7 20.4 -0.2 

11/02/06 12:14:12 29.1 122.8 20.5 -0.3 

11/02/06 12:14:22 28.8 122.8 20.4 -0.4 

11/02/0612:14:32 28.3 122.8 20.6 -0.5 

11/02/0612:14:42 28.0 122.8 20.6 -0.5 

11/0210612:14:52 27.8 122.5 20.7 -0.3 

11/02106 12:15:02 27.6 122.3 20.7 -0.3 

11/02/06 12:15:12 27.4 122.2 20.7 -0.3 

11/02/06 12:15:22 27.0 122.0 20.7 -0.3 

11/02/06 12:15:32 27.0 122.5 20.7 -0.5 

11/02106 12:15:42 27.5 122.7 20.7 -0.5 

11/02106 12:15:52 27.8 122.8 20.7 -0.5 

11/02/06 12:16:02 28.0 123.0 20.7 -0.5 

11/02106 12:16:12 28.0 122.9 20.6 -0.5 

11/02106 12:16:22 28.0 122.7 20.6 -0.3 

11/02/06 12:16:32 28.6 122.5 20.7 -0.3 

11/02106 12:16:42 28.8 122.1 20.8 -0.5 

11/02106 12:16:52 28.9 121.8 20.9 -0.5 

11/02106 12:17:02 29.2 121.4 21.0 -0.5 

11/02106 12:17:12 29.5 121.1 21.0 -0.5 

11/02106 12:17:22 29.5 121.4 21.0 -0.5 

11/02/06 12:17:32 29.1 121.5 20.9 -0.7 

11/02/06 12:17:42 28.2 121.9 21.0 -0.7 

11/02/06 12:17:52 27.8 122.2 21.0 -0.5 

11/02106 12:18:02 28.2 122.3 21.1 -0.5 

11/02106 12:18:12 28.9 122.2 21.2 0.0 

11/02/06 12:18:22 29.4 122.1 21.3 0.0 

11/02106 12:18:32 29.6 122.2 21.2 0.0 

11/02/06 12:18:42 29.5 122.4 21.2 0.0 

11/02106 12:18:52 30.3 122.4 21.1 0.0 

11/02/0612:19:02 30.6 122.6 21.1 0.0 

11/02106 12:19:12 30.4 122.9 21.1 0.0 

11/02/06 12:19:22 30.7 123.0 21.0 0.0 

11/02/06 12:19:32 31.4 122.9 20.9 -0.1 

11/02/06 12:19:42 31.6 123.1 20.9 -0.1 

11/02/0612:19:52 31.7 123.3 20.9 -0.2 

11/02/06 12:20:02 32.0 1232 20.8 -0.1 

11/02/06 12:20:12 32.1 123.0 20.8 0.0 

11/02/06 12:20:22 32.5 123.3 20.8 0.0 

11/02/06 12:20:32 32.4 123.3 20.7 -0.1 

11/02106 12:20:42 31.6 123.4 20.7 -0.1 

11/02106 12:20:52 30.7 123.4 20.6 0.0 

11/0210612:21:02 29.9 123.4 20.7 -0.2 

11/0210612:21:12 29.6 123.3 20.6 -0.1 

11/02/06 12:21 :22 29.0 123.1 20.5 0.0 

\ 

103 

Page 1 
1112/06 Run #3 

11/02/06 12:21:32 28.7 123.0 20.7 0.0 

11/02/06 12:21:42 28.4 122.9 20.7 0.0 

11/02/0612:21:52 28.0 122.7 20.7 ·0.1 

11/02/0612:22:02 27.8 122.4 20.7 -0.1 

11/02/06 12:22:12 27.9 121.9 20.7 -0.1 

11/02/06 12:22:22 27.9 121.7 20.8 0.0 

11/02/06 12:22:32 28.2 121.3 20.9 -0.1 

11/02/06 12:22:42 28.6 121.2 21.1 0.0 

11/02/06 12:22:52 28.5 121.4 21.3 .0.1 

11/02/06 12:23:02 29.3 121.6 21.5 -0.1 

11/02/06 12:23:12 29.6 121.6 21.5 -0.1 

11/02/06 12:23:22 30.0 121.6 21.6 -0.1 

11/02/06 12:23:32 31.2 121.5 21.6 0.0 

11/02/06 12:23:42 31.9 121.5 21.6 -0.1 

11/02/06 12:23:52 32.4 121.9 21.5 -0.1 

11/02/06 12:24:02 32.8 122.0 21.6 -0.1 

11/02/06 12:24:12 32.8 122.2 21.6 -0.1 

11/02/06 12:24:22 32.8 122.5 21.8 0.0 

11/02/06 12:24:32 32.6 122.3 21.9 0.0 

11/02/06 12:24:42 31.8 122.7 22.0 -0.1 

11/02/06 12:24:52 31.0 123.0 22.0 -0.1 

11/02/06 12:25:02 30.0 123.0 22.0 -0.1 

11/02/06 12:25:12 28.9 122.7 21.9 -0.1 

11/02/06 12:25:22 27.6 122.4 21.8 -0.1 

11/02/06 12:25:32 26.6 121.5 22.0 -0.1 

11/02/06 12:25:42 26.1 120.7 22.3 -0.2 

11/02/06 12:25:52 26.0 119.8 22.4 -0.1 

11/02/06 12:26:02 26.0 119.7 22.1 -0.1 

11/02/06 12:26:12 25.8 119.9 21.8 -0.1 

11/02/06 12:26:22 26.1 120.1 21.7 -0.1 

11/02/06 12:26:32 26.4 120.4 21.7 -0.1 

11/02/06 12:26:42 26.9 120.3 21.6 -0.1 

11/02/06 12:26:52 28.1 120.7 21.6 -0.1 

11/02/06 12:27:02 29.8 121.3 21.7 -0.1 

11/02/06 12:27:12 30.4 121.8 21.8 -0.1 

11/02/06 12:27:22 30.4 122.1 21.8 -0.1 

11/02/06 12:27:32 31.1 122.2 21.9 -0.2 

11/02/06 12:27:42 31.4 122.3 21.9 -0.2 

11/02/06 12:27:52 31.1 122.3 22.0 -0.1 

11/02/06 12:28:02 30.8 122.2 22.1 -0.1 

11/02/06 12:28:12 30.2 121.9 22.2 -0.1 

11102/06 12:28:22 29.6 121.4 22.2 -0.1 

11/02/06 12:28:32 29.4 120.6 22.3 -0.1 

11/02/06 12:28:42 29.2 120.1 22.3 -0.1 

11/02/06 12:28:52 29.3 119.4 22.3 -0.1 

11/02/06 12:29:02 28.5 119.6 22.2 -0.1 

11/02/06 12:29:12 28.0 119.6 22.2 -0.2 

11/02/06 12:29:22 27.6 120.1 22.0 ·0.2 

11/02/06 12:29:32 27.3 120.4 22.0 ·0.1 

11/02/06 12:29:42 27.1 120.6 22.0 -0.2 

11/02/06 12:29:52 26.5 120.7 22.0 -0.2 

11/02/06 12:30:02 26.1 120.7 22.4 -0.1 

11/02/06 12:30:12 25.6 120.5 22.9 0.0 

11/02/06 12:30:22 25.0 120.3 23.4 ·0.1 

11/02/06 12:30:32 24.9 120.5 23.7 ·0.2 

11/02/06 12:30:42 25.9 120.8 23.5 -0.1 

11/02/06 12:30:52 27.0 121.1 23.0 ·0.1 

11/02/0612:31:02 27.4 121.3 22.5 -0.2 

11/02/0612:31:12 28.1 121.4 22.1 ..0.1 

11/02/06 12:31 :22 29.7 121.5 21.9 -0.2 

11/02/0612:31:32 30.5 121.4 21.8 -0.2 

11/02/0612:31:42 30.6 121.9 21.7 -0.1 

11/02/06 12:31:52 29.7 121.8 21.9 -0.2 

11/02/06 12:32:02 29.3 120.8 22.6 -0.2 

11/02/06 12:32:12 28.8 120.3 23.3 -0.3 

11/02/0612:32:22 27.1 120.0 23.6 -0.3 

11/02/06 12:32:32 26.1 120.0 23.8 -0.2 

11/02106 12:32:42 26.2 120.1 23.7 -0.2 

11/02/06 12:32:52 26.1 120.3 23.4 -0.1 

11/02/0612:33:02 26.0 120.2 23.2 -0.2 

11/02/06 12:33:12 25.7 120.1 23.0 -0.3 

11/02/06 12:33:22 25.7 120.3 22.8 -0.3 

11/02/06 12:33:32 26.0 121.2 22.6 -0.2 

11102/06 12:33:42 26.0 121.4 22.6 -0.2 

Page 2 

104 
11/2/06 Run #3 

11/02/06 12:33:52 25.6 121.6 22.5 -0.2 

11/02/06 12:34:02 24.9 121.6 22.5 -0.1 

11/02/06 12:34:12 24.6 121.1 22.6 -0.2 

11/02/06 12:34:22 24.4 120.6 22.6 -0.2 

11/02106 12:34:32 24.1 119.6 22.6 -0.2 

11/02106 12:34:42 24.4 119.1 22.8 -0.2 

11/02106 12:34:52 24.8 118.7 22.8 -0.1 

11/02/06 12:35:02 25.9 118.7 22.8 -0.1 

11/02/0612:35:12 27.2 119.3 22.9 -0.1 

11/02106 12:35:22 27.7 119.8 22.9 ·0.2 

11/02106 12:35:32 27.8 120.1 22.7 ·0.3 

11/02106 12:35:42 27.8 120.1 22.6 ·0.3 

11/02/0612:35:52 27.6 120.1 22.6 ·0.3 

11/02106 12:36:02 27.5 119.8 22.8 -0.2 

11/02106 12:36:12 27;0 119.5 23.1 0.0 

11/02106 12:36:22 27.1 119.8 23.3 -0.1 

11/0210612:36:32 27.7 120.0 23.4 -0.1 

11/02/06 12:36:42 27.9 119.9 23.3 -0.2 

11/02106 12:36:52 26.2 118.2 23.1 -0.1 

11/02/06 12:37:02 24.0 114.3 23.7 -0.2 

11/02/06 12:37:12 22.4 108.5 25.5 -0.2 

11/02/06 12:37:22 21.2 103.2 26.7 -0.2 

11/02/06 12:37:32 20.4 97.8 27.0 -0.3 

11/02106 12:37:42 19.8 94.0 27.2 -0.3 

11/02106 12:37:52 19.8 91.4 27.5 -0.3 

11/02/0612:38:02 19.8 91.1 27.9 -0.3 

11/02/06 12:38:12 20.1 93.2 27.5 -0.2 

11/02/06 12:38:22 20.6 96.7 26.1 -0.2 

11/02/06 12:38:32 20.9 100.3 25.1 -0.2 

11/02/06 12:38:42 21.7 103.6 24.5 -0.2 

11/02/06 12:38:52. 22.3 105.5 24.2 -0.4 

11/02/06 12:39:02 23.0 107.2 23.9 -0.4 

11/02/06 12:39:12 24.6 109.3 23.6 -0.4 

11/02106 12:39:22 25.9 111.2 23.4 ·0.3 

11/02106 12:39:32 26.7 113.0 23.3 -0.4 

11/0210612:39:42 26.9 114.8 23.2 -0.4 

11/02/06 12:39:52 27.2 116.3 23.4 -0.3 

11/02/06 12:40:02 27.9 117.0 23.4 -0.2 

11/02/0612:40:12 28.6 117.8 23.3 -0.1 

11/02106 12:40:22 ·. 28.1 118.6 23.2 -0.2 

11/02/0612:40:32 27.9 119.2 23.4 -0.3 

11/02106 12:40:42. 27.6 119.7 23.8 -0.3 

1110210612:40:52 27.7 120.1 23.9 -0.3 

11/02/0612:41:02 27.6 120.5 23.9 -0.4 

11/02/0612:41:12 27.1 121.0 23.5 -0.2 

11/02/06 12:41:22 27.1 121.3 23.1 -0.3 

11/02/0612:41:32 27.2 121.7 22.9 -0.2 

11/02106 12:41:42 26.5 122.4 22.8 -0.3 

11/02/06 12:41:52 26.4 122.6 22.8 -0.3 

11/02/0612:42:02 24.4 122.6 22.6 -0.1 

11/02/0612:42:12 22.5 120.9 23.1 -0.1 

11/02/06 12:42:22 21.6 118.1 24.4 0.0 

11/02106 12:42:32 20.8 116.4 25.2 -0.1 

11/02/06 12:42:42 20.5 116.1 25.7 -0.1 

11/02106 12:42:52 20.5 117.0 26.1 -0.2 

11/02/0612:43:02 21.1 118.8 26.6 -0.2 

11/02/06 12:43:12 22.4 121.3 26.8 -0.1 

11/02/06 12:43:22 23.3 123.1 25.5 ·0.1 

11/02/06 12:43:32 24.3 124.0 24.4 0.0 

11/02/06 12:43:42 25.3 124.4 24.0 -0.1 

11/02106 12:43:52 25.9 124.2 23.7 -0.1 

11/02106 12 :44:02 26.4 123.8 23.5 -0.1 

11/02/0612.:44:12 27.2 123.4 23.2 0.0 

11/02/06 12:44:22 28.7 123.0 23.0 -0.1 

11/02/06 12:44:32 30.1 122.6 22.9 0.0 

11/02/06 12:44:42 30.8 122.1 22.8 -0.1 

11/02/0612:44:52 31.0 121.1 22.8 -0.1 

11/02/06 12:45:02 29.5 119.7 22.9 -0.1 

11/02/06 12:45:12 27.8 118.0 23.0 -0.1 

11/02/06 12:45:22 26.8 116.5 23.3 -0.1 

11/02/06 12:45:32 26.3 114.7 23.7 0.0 

11/02/06 12:45:42 26.2 114.0 24.0 -0.1 

11/02106 12:45:52 26.2 113.6 24.0 -0.1 

11/02/0612:46:02 26.3 113.6 23.7 0.0 

105 

Page3 
11/2/06 Run #3 

11/0210612:46:12 26.4 113.7 23.4 -0.1 

11/02/06 12:46:22 26.4 114.2 23.2 -0.2 

11/02/0612:46:32 26.9 114.4 23.2 -0.2 

11/02106 12:46:42 27.2 114.3 23.1 -0.1 

11/02106 12:46:52 27.3 114.2 23.1 -0.1 

11/02106 12:47:02 24.8 113.8 23.1 -0.1 

11/02106 12:47:12 23.1 111.5 24.1 -0.1 

11/02/0612:47:22 22.0 109.0 25.2 -0.1 

11/02/06 12:47:32 21.1 107.6 26.0 -0.2 

11/02/06 12:47:42 20.7 106.7 26.3 -0.2 

11/02/0612:47:52 20.6 106.4 26.6 -0.1 

11/02/06 12:48:02 20.8 106.4 27.1 -0.1 

11/02/06 12:48:12 21.6 106.9 26.7 -0.1 

11/02/06 12:48:22 22.3 108.1 25.8 -0.1 

11/02/06 12:48:32 23.1 108.8 25.1 -0.1 

11/02/0612:48:42 23.9 108.9 24.6 -0.1 

11/02/06 12:48:52 24.8 109.0 24.4 -0.2 

11/02/06 12:49:02 25.5 109.2 24.0 -0.2 

11/02/06 12:49:12 26.1 109.9 23.9 -0.3 

11/02/06 12:49:22 26.5 110.6 23.7 -0.1 

11/02/06 12:49:32 27.5 111.0 23.6 -0.1 

11/02/06 12:49:42 28.3 111.3 23.5 0.0 

11/02/06 12:49:52 29.0 111.4 23.4 -0.1 

11/02/06 12 :50:02 29.7 111.5 23.3 -0.1 

11/02/06 12:50:12 29.6 111.9 23.1 -0.1 

11/02106 12:50:22 29.6 112.0 23.0 -0.1 

11102/06 12:50:32 29.6 112.6 22.9 -0.1 

11/02/06 12:50:42 29.4 113.1 23.0 -0.1 

11/02/06 12 :50:52 29.7 113.6 22.9 -0.1 

11/0210612:51:02 29.5 114.2 23.0 -0.1 

11/02/0612:51:12 28.6 • 115.2 22.9 0.0 

11/02/06 12:51:22 28.1 116.2 22.7 0.0 

11/02/06 12:51:32 27.8 117.0 22.7 -0.1 

11102/06 12:51 :42 27.1 118.2 22.6 0.0 

11/02106 12:51:52 26.2 118.3 22.7 0.0 

11/02/06 12:52:02 25.6 117.5 23.1 0.1 

11/02/06 12:52:12 24.8 117.0 23.6 0.0 

1 1/02/06 12:52:22 24.7 117.4 23.8 -0.1 

11/02/06 12:52:32 25.2 117.9 23.9 -0.1 

11/02106 12:52:42 25.4 118.2 23.7 -0.1 

11/02/0612:52:52 25.6 118.3 23.4 -0.1 

11/02/06 12:53:02 26.2 118.5 23.1 -0.1 

11/02106 12:53:12 26.6 118.9 22.9 -0.1 

11/02/06 12:53:22 25.1 119.0 22.8 -0.1 

11/02/06 12:53:32 24.3 117.9 23.4 -0.1 

11/02/06 12:53:42 24.1 116.6 24.4 0.0 

11/02106 12:53:52 24.1 116.0 25.0 0.0 

11/02/06 12:54:02 24.3 116.8 25.4 -0.1 

11/02/06 12:54:12 24.4 118.2 25.4 0.0 

11/02106 12:54:22 24.9 119.4 25.0 0.0 

11/02106 12:54:32 25.7 120.6 24.5 0.0 

11/02/06 12:54:42 26.6 121.3 23.9 -0.1 

11/02/06 12:54:52 27.6 121.7 23.5 -0.1 

11/02106 12:55:02 28.1 122.2 23.2 -0.2 

11/02/06 12:55:12 28.7 122.4 23.1 -0.2 

11/02/06 12:55:22 29.0 122.0 22.9 -0.2 

11102106 12:55:32 27.0 121.4 22.9 -0.2 

11/02/06 12:55:42 25.7 119.1 23.4 -0.2 

11/0210612:55:52 24.6 116.4 24.1 -0.1 

11/02/0612:56:02 24.0 115.5 24.5 0.0 

11/02/06 12:56:12 23.6 115.5 24.7 -0.1 

11/02/06 12:56:22 24.0 116.3 25.2 -0.1 

11/02/06 12:56:32 24.6 117.8 25.5 -0.1 

11/02/06 12:56:42 25.4 119.8 24.8 ·0.2 

11/02106 12:56:52 26.0 121.3 24.0 -0.2 

11102/06 12:57:02 26.2 121.9 23.4 -0.1 

11/02/06 12:57:12 26.6 122.2 22.9 -0.1 

11/02/06 12:57:22 27.5 122.5 22.7 0.0 

11/02/06 12:57:32 27.8 122.7 22.6 0.0 

11/02/06 12:57:42 27.2 122.9 22.5 0.0 

11/02/06 12:57:52 26.9 122.9 22.4 0.0 

11/02/06 12:58:02 26.4 122.5 22.4 -o.1 

11/02/06 12:58:12 26.0 122.1 22.4 -0.1 

11/02/06 12:58:22 25.7 122.2 22.5 0.0 

106 

Page4 
1112/06 Run #3 

11/02/06 12:58:32 25.7 122.3 22.6 0.0 

11/02/06 12:58:42 26.1 122.4 22.6 0.0 

11/02/06 12:58:52 26.2 122.4 22.6 0.0 

11/02/06 12:59:02 27.0 122.4 22.6 0.0 

11/02/06 12:59:12 27.7 122.5 22.8 0.0 

11/02106 12:59:22 27.7 122.4 22.7 0.0 

11/02106 12:59:32 28.1 121.8 22.8 0.1 

11/02/0612:59:42 28.2 121.1 23.1 0.1 

11/02/06 12:59:52 28.2 120.8 23.2 0.0 

11/02106 13:00:02 28.4 120.5 23.2 0.0 

11/02106 13:00:12 28.7 120.9 23.2 ·0.1 

11/0210613:00:22 28.5 120.7 23.1 ·0.1 

11/02106 13:00:32 28.0 120.7 22.9 0.1 

11/02/06 13:00:42 27.7 120.4 22.8 0.1 

11/02/06 13:00:52 27.6 119.8 22.7 0.0 

11/02/0613:01:02 27.2 119.3 22.7 0.0 

11/0210613:01:12 26.5 118.6 22.7 0.0 

11/02/06 13:01 :22 25.0 118.1 22.7 0.0 

11/02/06 13:01 :32 23.9 117.6 22.8 0.0 

11/02/06 13:01 :42 23.0 117.2 23.4 0.0 

11/02/06 13:01:52 22.6 117.4 23.8 0.0 

11/02/06 13:02:02 22.8 118.1 24.1 0.0 

11/02/06 13:02:12 23.5 118.9 23.9 0.0 

11/02/06 13:02:22 24.4 119.6 23.5 0.1 

11/02/06 13:02:32 25.6 119.8 23.2 0.0 

11/02/0613:02:42 27.0 119.8 23.1 0.0 

11/02/06 13:02:52 27.9 120.2 22.9 0.1 

11/02106 13:03:02 28.6 120.5 22.8 0.0 

11/02/06 13:03:12 29.2 120.4 22.9 0.0 

11/02106 13:03:22 27.7 120.0 22.9 0.0 

11/02106 13:03:32 26.4 118.8 • 23.1 0.0 

11/02/06 13:03:42 26.1 117.8 23.9 0.0 

11/02106 13:03:52 25.6 117.1 24.5 0.0 

11/02106 13:04:02 25.5 117.2 25.1 0.0 

11/02/06 13:04:12 25.4 117.5 25.6 ·0.1 

11/02/06 13:04:22 26.2 118.0 25.4 0.0 

11/02/06 13:04:32 26.7 118.5 24.6 0.0 

11102/06 13:04:42 26.6 118.7 24.0 0.0 

11/02/06 13:04:52 26.2 119.0 23.5 0.0 

11/02/06 13:05:02 25.8 119.4 23.4 0.0 

11/02/06 13:05:12 25.3 120.1 23.2 0.0 

11/02106 13:05:22 24.9 120.6 23.2 0.1 

11/02/06 13:05:32 23.8 121.2 23.2 0.0 

11/02/06 13:05:42 22.7 121.5 23.2 0.0 

11/02/06 13:05:52 22.1 120.8 23.6 0.0 

11/02/06 13:06:02 21.5 120.2 24.2 0.0 

11/02/06 13:06:12 22.3 119.7 24.7 0.0 

11/02106 13:06:22 23.2 120.1 25.0 0.1 

11/0210613:06:32 24.2 120.6 24.8 0.1 

11/02/0613:06:42 25.4 120.7 24.5 0.0 

11/02/06 13:06:52 26.2 121.2 24.2 0.0 

11/02106 13:07:02 27.5 121.8 23.7 0.0 

11/02/06 13:07:12 28.5 122.2 23.3 0.1 

11/02/06 13:07:22 29.6 122.2 23.2 0.1 

11/02/06 13:07:32 30.8 121.8 23.0 0.0 

11/02/06 13:07:42 32.0 121.7 22.9 0.0 

11/02/0613:07:52 32.9 121.4 22.9 0.0 

11/02/06 13:08:02 32.3 121.3 22.8 0.0 

11/02/0613:08:12 31.4 121.3 22.7 0.1 

11/02/0613:08:22 30.1 121.2 22.7 0.0 

11/02/06 13:08:32 29.3 121.8 22.7 0.0 

11/02/06 13:08:42 28.4 122.4 22.7 0.0 

11/02/06 13:08:52 27.7 122.8 22.9 0.1 

11/02/06 13:09:02 26.9 122.8 23.1 0.1 

11/02/06 13:09:12 26.2 122.6 23.1 0.1 

11/02/06 13:09:22 26.0 122.3 23.2 0.1 

11/0210613:09:32 25.5 121.4 23.1 0.1 

11/02/06 13:09:42 25.0 120.9 23.1 0.1 

11/02/06 13:09:52 24.7 120.5 23.1 0.0 

11/02/0613:10:02 24.7 120.5 23.0 0.0 

11/02/06 13:10:12 24.8 120.7 23.0 0.0 

11/02/06 13:10:22 24.7 120.8 23.0 0.0 

11/02/06 13:10:32 24.7 120.5 23.1 0.0 

11/02/06 13:10:42 24.8 120.4 23.4 0.1 

107 

Page 5 
1112/06 Run #3 

11/02/0613:10:52 25.6 120.8 23.6 0.1 

11/02/0613:11:02 26.7 121.3 23.6 0.1 

11/02106 13:11:12 27.3 121.7 23.4 0.1 

11/02/06 13:11:22 27.9 121.3 23.1 0.1 

11/0210613:11:32 29.0 120.1 23.1 0.0 

11/0210613:11:42 29.7 119.2 23.0 0.1 

11/0210613:11:52 30.0 118.3 23.0 0.0 

11/02106 13:12:02 29.5 117.3 23.0 0.1 

11/02/06 13:12:12 25.5 116.2 22.9 0.1 

11/02/06 13:12:22 22.2 112.0 23.2 0.1 

11/02/0613:12:32 20.7 106.8 23.7 0.1 

11/02/0613:12:42 20.1 104.4 24.3 0.1 

11/02/06 13:12:52 19.9 103.7 25.0 0.1 

Stop Run #3 26.88 118.98 22.77 ~0.11 

11/02/0613:13:02 19.0 104.5 25.9 0.1 

11/02/0613:13:12 18.6 105.4 27.0 0.0 

11/02/0613:13:22 19.3 107.2 28.8 ~.1 

11/02/06 13:13:32 7.7 107.9 29.0 -0.1 

11/02/06 13:13:42 5.7 76.7 22.9 0.0 

11/02106 13:13:52 6.0 37.9 13.7 0.0 

11/0210613:14:02 5.7 18.1 9.1 0.0 

11/0210613:14:12 5.5 9.6 7.2 0.0 

11/0210613:14:22 5.2 5.6 6.4 0.0 

11/02/06 13:14:32 5.1 3.3 5.8 0.1 

11/02/06 13:14:42 5.3 4.1 5.5 0.0 

11/02/06 13:14:52 4.9 33.4 5.1 0.0 

11/02106 13:15:02 4.0 62.7 4.7 0.1 

11/02106 13:15:12 3.5 77.0 4.1 0.0 

11/02/0613:15:22 3.0 84.4 3.5 • 0.1 

11/02106 13:15:32 2.4 88.0 3.2' 0.1 

11/02/06 13:15:42 1.7 89.5 2.9 0.0 

11/0210613:15:52 1.4 90.5 2.7 ~0.1 

11/0210613:16:02 1.2 90.8 2.5 0.0 

1110210613:16:12 1.0 91.1 2.3 0.0 

11/02106 13:16:22 1.0 91.1 2.2 0.0 

11/02/06 13:16:32 1.0 91.3 2.1 0.0 

11/02/06 13:16:42 1.0 91.4 2.0 0.0 

11/02/0613:16:52 0.9 91.7 1.9 . 0.0 

11/0210613:17:02 0.7 91.8 1.9 0.0 

11/02106 13:17:12 0.7 91.7 1.8 ·o.o 

11/02/0613:17:22 0.7 91.8 1.8 0.0 99.1 ppm CO 

11/02/06 13:17:32 0.8 92.0 1.7 -0.1 Zero S02 

11/02106 13:17:42 0.9 92.0 1.6 -0.1 

11/0210613:17:52 1.1 86.9 1.6 0.0 

11/0210613:18:02 0.9 70.1 2.2 0.0 

11/02/06 13:18:12 0.8 37.1 10.8 0.0 

11/0210613:18:22 0.8 17.2 18.5 0.0 

11/02106 13:18:32 0.8 8.2 22.0 0.0 

11/02/0613:18:42 0.8 4.3 23.4 0.0 

11/02/06 13:18:52 0.8 2.2 24.0 ~0.1 

11/02/06 13:19:02 0.8 1.1 24.4 -0.2 

11/02/06 13:19:12 0.8 0.5 24.6 -0.1 

11/02/0613:19:22 0.8 0.3 24.7 0.0 

11/02106 13:19:32 0.8 0.3 24.8 0.0 

11/02/06 13:19:42 0.8 0.1 24.8 0.0 

11/02106 13:19:52 0.8 -0.2 24.9 0.0 

11/02/06 13:20:02 0.8 -0.3 24.9 -0.1 25 ppm NOx 

11/02/0613:20:12 0.8 -0.4 24.9 0.0 Zero CO 

11/02/06 13:20:22 0.9 -0.5 25.0 0.0 

11/02106 13:20:32 1.1 ~.4 24.2 0.0 

11/02106 13:20:42 1.3 ~.5 20.9 0.0 

11/02/06 13:20:52 2.6 ·0.7 18.3 0.0 

11102/06 13:21 :02 2.9 ~.5 13.5 0.0 

11/02/0613:21:12 1.6 -0.4 6.7 0.0 

11/02/06 13:21:22 0.9 ·0.4 3.7 0.0 

11/02/06 13:21:32 0.8 -0.8 2.3 0.1 

11102/06 13:21:42 0.8 -1.0 1.8 1.0 

11/02/06 13:21:52 0.7 ·1.3 1.6 2.6 

11/02/06 13:22:02 0.8 -1.0 1.7 4.6 

11/02106 13:22:12 0.8 ·0.8 1.6 6.9 

Page 6 108 
11/2/06 Run #3 

11/02/06 13:22:22 0.8 -0.9 1.4 9.4 

11/02/06 13:22:32 0.8 -0.5 1.3 11.9 

11/02/06 13:22:42 0.8 -0.7 1.2 14.4 

11/02/06 13:22:52 0.8 -0.7 1.1 16.8 

11/02106 13:23:02 0.8 -0.7 1.0 19.0 

11/02/06 13:23:12 0.8 -0.7 0.9 21.3 

11/02/06 13:23:22 0.8 -0.6 0.9 23.2 

11/02/06 13:23:32 0.8 -1.0 0.8 25.0 

11/02/06 13:23:42 0.8 -1.0 0.8 26.8 

11/02/06 13:23:52 0.8 -1.1 0.8 28.1 

11/02/06 13:24:02 0.6 -1.0 0.8 29.2 

11/02/06 13:24:12 0.4 -1.1 0.7 30.3 

11/02106 13:24:22 0.5 -1.0 0.7 31.2 

11/02/06 13:24:32 0.7 -0.9 0.7 32.0 

11/02/06 13:24:42 0.8 -1.0 0.7 32.9 

11/02106 13:24:52 0.8 -1.0 0.6 33.7 

11/02106 13:25:02 0.5 -0.8 0.7 34.6 

11/02/06 13:25:12 0.5 -0.9 0.6 35.4 

11/02/06 13:25:22 0.5 -0.9 0.6 36.1 

11/02/06 13:25:32 0.5 -0.9 0.6 36.9 

11/02/06 13:25:42 0.8 -0.7 0.5 37.5 

11/02106 13:25:52 0.8 -0.9 0.5 38.2 

11/02/06 13:26:02 0.7 -0.8 0.5 38.7 

11/02106 13:26:12 0.8 -1.0 0.5 39.1 

11/02/06 13:26:22 0.8 -0.9 0.5 39.5 

11/0210613:26:32 0.8 -1.0 0.5 40.0 

11/02/06 13:26:42 0.8 -1.1 0.5 40.7 

11/02/06 13:26:52 0.8 -1.1 0.4 41.3 

11/02/06 13:27:02 0.8 -1.1 0.4 41.7 

11/02106 13:27:12 0.8 -1.1 0.4 42.1 

11/02/06 13:27:22 0.8 -1.2 0.4 42.3 

11/02/06 13:27:32 0.8 -1.3 0.4 42.5 

11/02/06 13:27:42 0.8 -1.1 0.4 42.9 

11/02/06 13:27:52 0.8 -0.9 0.4 43.2 

11/02/06 13:28:02 0.8 -0.9 0.4 43.4 

11/02/06 13:28:12 0.8 -1.0 0.3 43.7 

11/02/06 13:28:22 0.8 -0.8 0.3 43.9 

11/02/0613:28:32 0.8 -0.9 0.3 44.2 

11/02/06 13:28:42 0.8 -1.0 0.4 44.6 

11/02106 13:28:52 0.8 -0.9 0.4 44.9 

11/02106 13:29:02 0.8 -0.8 0.3 45.0 

11/02/0613:29:12 0.8 -0.9 0.3 45.2 

11/02/0613:29:22 0.8 -D.9 0.3 45.4 

11/02/06 13:29:32 0.8 -0.9 0.3 45.5 

11/02/0613:29:42 0.8 -0.7 0.3 45.5 ZeroVOC 

11/02/06 13:29:52 0.8 -0.7 0.3 45.6 

11/02106 13:30:02 0.8 -0.7 0.3 45.7 

11/0210613:30:12 0.8 -0.6 0.3 45.9 

11/02/06 13:30:22 1.0 -0.7 0.3 45.9 49.8 ppm 502 

11/0210613:30:32 26.3 -o.8 0.2 45.8 Zero NOx 

11/02/06 13:30:42 40.3 -o.s 0.2 45.9 

11/02/0613:30:52 40.4 -0.8 0.3 46.1 

11/02/06 13:31:02 40.5 -0.9 0.2 44.2 

11/0210613:31:12 40.4 -1.1 0.2 40.5 40.8 ppm CH4 

11/02/06 13:31:22 40.5 -0.9 0.2 36.1 

11/02/0613:31:32 40.6 -0.8 0.2 31.9 

11102/0613:31:42 33.8 -0.8 0.2 28.3 

109 

Page 7 
. ~ 

I 

I 

Appen'dix C · ·. . . 

·. ,' .. , .. ,; 
FILTER ANALITICAL DATA 

Company: Dal-ltalla, Muskogee, OK 

Date: 10/30/06 

Location: Glaze Line Baghouse (EPN 41) 

Run 1 

Filter ID Number 

Date of Weighing 

Time 

Gross Filter Wt. 

Date of Weighing 

Time 

Gross Filter Wt. 

Ave. Gross Filter Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Ave. Filter Tare Wt. 

Wt. of PM on Filter (grams) 

Total Weight of Particulate (mg) 

\azG.\WH:n~Hn 

jH1l1j~~uat.o~1 

::::::m=: 

1HlH11H~~/afQ$1 

H1Hl~i~S1P:M1 

@HH1PUa9:5.S~ 

0.3655 

:=:=:=:::.t:;;r;a1na= 

:::;:::::~:yJ.~/~~; 

HlH12l1~1P:Ml 

1WiWin~®4a1 

1~m~~w1oroa1 

lH11lS.~~~m~M~ 

HH~HP~4!4~ 

0.3645 

0.0010 

1.0 

Run 2 

:~~Gfl~;f:1~1~lj\l~~ 

~~jH:J~f:~ip$.j 

UfU1:i:W.~HAMi 

?HHHQi~P.~tti 

,WHHi~1,~6i~6.1 

:;Hn~r~a$H?:t.W 

'i)iHHO;aa~i~i 

0.3612 

0.3610 

0.0001 

0.1 

Run 3 

·~~tt~:nnnun 

:nn~n1l11$1Q.~: 

·l::::ili~::i 

HiWn1116100:i 

HU~~~!4HP:MH 

1\lHH~Hl$.~1 

0.3633 

H~)~Q/.~1®. 

YH2~20HRIYf 

HHHHO:Jaazt 

~~iljbi:~PI:®~ 

HHH~H21:1ANf 

P1HHH10~a~9l: 

0.3627 

0.0006 

0.6 

140 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal-ltalia, Muskogee, OK 

Date: 10/30/06 

Location: Glaze Line Baghouse (EPN 41) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight' 

Weight of Particulate in Rinse (mg). 

j1{%LldJ1$$.f 

l:l:l~l~~~~f~~~ 0.0001 

:l;l:lll:l~;~;r:.~l nnnl;~;tctJ2llail! 

·':'·\lj~!~i!! 

~UHHl~o¥:51:061 

~=~H~Y1:!~0l~tVf 

~~UHlllO:i26~1.l 

l1 ll !lHlll b¥:$Xd6l 

l::;:mi~~~~~: 

110.2739 

0.0001 

110.2647 

9.01 

Run 2 

~nnnnn~ot?:sshH 

lHHot(}di2tr3jl 

nnHH~n:HHlit4~l 

0.0001 

~HHHt1i6i:Oe1 

nnH:n~siAA~Ml 

n~nnJQ~ls~r.al 

HHH(Ellt~i.<16.l 

~;nlHn1a~07:l~Ml 

~iHHJJ(}3;S~7:8~ 

H?Hlltoi6i~6.l 

:1n1~Hf1!2tANH 

.HnJJ)3iSZ01i 

HHH1tl1:6i:{)e l ~nnnnl~~341P-Nt 

Y;llfG.3~S2QS.~ 

103.8278 

0.0001 

103.8206 

7.06 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) = mg/g 

!iii\,··!:~~~~ HlHHH98.16l460: 

nHHl:tiV:$/061 

;;w~:~;:m~:.~: 

98.646 

~ H~ 1Hll~~~/.S1:0.6l 

1m::m;~~~:.~;: 

~:l:~:l:l;~~g(~~~ /1l!H; Sa.6~$11 

98.64575 

0.00025 

0.00127 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

Hl=lUUHd1t:$~f 

;H\tb.th27:stt 

n~Hl~=WH=~=n~~~~: 

0.0001 

HHHI1t.el.m6l 

lHl\l~l$l;MYf 

lliH1;~tj~j[;j~$.~ 

HHlHf11.61:b6.1 

Hnn~n~ta$H?:tW 

H:H10~ltt7~~ 

~HHH1c~l:b5: 

n:<nl1~3~~tw 

nu10011:6s.~t:: 

<tllllot.e~o6.: 

l1~1Hl3~3~1P.t~f 

l<H~02J~53: 

102.1725 

0.0001 

102.1654 

7.01 
PARTICULATE ANALYTICAL DATA FORM 

. Company: Dal-ltalia, Muskogee, OK 

Date: 10/30/06 

Location: Glaze Line Baghouse (EPN 41) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (J/a) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

;Hu;nHH1111ll$6i 

:Hifl2ls4itslot 

:;~nnnn=H~HH~~S3i 

0.0001 

nHHlWIWi6i:G6l 

HHniiHS~(l~1HMW 

iHHHWS.O:..:O:Of?~~ 

lll:l:l!ll~~;.ri: i~iii1~iH~~~!QS$il 

l1HlHiO:l:t~Y:06i 

HiliiUH?::i~ttU~Ml 

il~nnlH95.10059i 

=======~;oiid~a6= 

'!::~.!::!~~§~~ 

96.0062 

0.0001 

96.0058 

0.35 

Run 2 

+U1:1nHntaei 

Hlin2Hi4if!~o1:i 

iHH~:n:HH~n~i~Si 

0.0000 

nHHHtli:61f()6l 

lllll:l~il1~~~ 

lHHHn~tl~i:6ic61 

~;~nnn:z~iO;P.~t 

HHil~ili®tP~$$1 

j)Jb/.~1&1061 

:::::!:::::Y:i:i=?==~M·: :·:·:i.:!•:I:,:..L:~·1'\.' 0 

:nnntosro~3~i 

UHH1m~10:/<l6l 

HiH~iiSip&iP.Mi 

ii~ i~~ilt05l0i1i.30 i 

105.0435 

0.0000 

105.0431 

0.35 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va«·Pa) = g/g 

llllil:l:l~[~~~~ ~;!HH;ns~~!AMl 

iHHilit~~Jtill541 

HHHHitf~6xo6i 

~n:p;iii~l~().;fW1~ 

nnnn1m~~W5.4l 

103.1154 

HH1!ll10(:~0Y:~6! 

\!l!HH?:i;30!~Nl 

UliHllS~l~lt53l 

liiUi~lOJ101:0:6l 

::;l::::~~~~li~l 

103.1153 

1E·04 

2.941E·07 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

;:lililililjliljlitl$& 

HHH2t9~1£;bt 

:nnnnnn=Hiill2~:: 

0.0000 

HIH111.~1b.5: 

HHHiliiS:.1>2iAMi 

iHHlliQ~i~51:0:i 

lHHH~H¥.6~a6U 

iHiiiH2~~HlliP:M1 

iHi;ttO!ai~69:: 

YHtoi:iPib& 

iliilliin1~tSlAM 

UlUUJ2lili56l 

unnrol:io1.o& 

}jn!ii3~$Zii?:M 

nn==J02A~559. 

102.4570 

0.0000 

102.4561 

0.85 

14.2 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal·ltalia, Muskogee, OK 

Date: 10/30/06 

Location: Glaze Line Baghouse (EPN 41) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

~~nHlll:HH1nHlill 

lllllllllll!llll~~~i 0.0003 

:l:l:l:::l~f~~r~~ lnH;HeS..~S5.3l 

l!l!l:l:l:~~~rll UlH<99.ASG1i 

::::·.l·.'~::ri:. ==l=l=====1ti~9.la6= 

;lili1j1j~~i521~~M1 

HHHnS.~ .. 461:5l 

99.4863 

0.0003 

99.4675 

1S.50 

Run 2 

\lll\U~nnllnllllmtl 

iHHHHHHilEh:06l 

l;ljljljljljl;lll:i~{)IiJj 

0.0003 

:HHHHtii&J<>al 

[UnllH4l~29.iflNf 

YH~HllQ3tBSUH 

!HHHntti;Y:~i~sl 

:HlU!S:Ba1AM.i 

Hln;t()3~$Biltl 

H!HUt61:~i.(}6\ 

nn;l;lH7:H)3lAMl 

lilUlll1().3lS$.9llii 

WiHHH~W:9=mai 

UHHHigi50iP.til!l 

:l;>lll03l8$8Sl 

103.8811 

0.0003 

103.8590 

21.80 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing · 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va·~Pa) = g/g 

:lllllll!l~li~~= i!HHHil.8i~1H~M; 

lHnHllO~l6~00: 

illil!ll!l1lE~6.1:d6; 

lHnlll~i~SH~~t 

=innll10~~648.~l 

106.64895 

iiiiiiii!ilil¥.91:~61 

nHnnnr?:!2~~AtW 

h%~lD~t64S9l 

:unHHllti91:D.6l 

liHHHlH3:~~l~Ml 

:=;1/t 0&.~6:485! 

106.6487 

0.00025 

1E·06 

No~e: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

we1 ht be subtracted from the sam le wei ht. 

Run 3 

HHHHHH11E!d&.i 

UlllllnHHlH\lSQct 

0.0003 

·ll:::1:1:m~:ri~l lllHHlbOl0.6$Zl 

lllllllll~~~;:~: :nu~OOH)6S4il 

lHUHip/.91-d~\ 

;;;l;(n:n()~l~rw 

HiHii~OOi~62&: 

HiHHi~lsKm&.l 

~~~y~n~j9a~;F~: :::::::1(!aJ.:0.62a: 

100.0683 

0.0003 

100.0625 

5.55 

· .. 

143 
FILTER ANALITICAL DATA 

Company: Dal-ltalia, Muskogee, OK 

Date: 1 0/30/06 

Location: Press Baghouse (EPN 40) 

Run 1 

Filter ID Number 

Date of Weighing 

Time 

Gross Filter Wt. 

Date of Weighing 

Time 

Gross Filter Wt. 

Ave. Gross Filter Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Ave. Filter Tare Wt. 

. Wt. of PM on Filter (grams) 

Total Weight of Particulate (mg) 

i4.~s.n1nnnw1~1 

:~nHH~~i.$roe1 

HUU7:it:$lAMl 

l\HllHJ)~7.;1 $~ 

Hn~!i~Jat.Qsl 

nHHZl~$~P:Ml 

1HHHHP~arf7:l 

0.3718 

~1HlH~~~wet.o6~ 

lHHlZ!63.ll?:Ml 

HHillHO~~tft 

[i~~~~iohoroai 

HHHS.~4Pl~M~ 

llHHHl~t~7tt 

0.3711 

0.0007 

0.7 

Run 2 

·4$~~~lj)llllll)lil) 

/%t~t:$ioal 

>W~i~it?.i~t\f 

nHHn~;~a$e,l 

t~lm~Hni1Y:6Joal 

~HH121~$4:lP:Ml 

:H:HHO;~aaz; 

0.3657 

0.3648 

0.0009 

0.9 

Run 3 

~7~i!H)T/ 

Hn(1:1ml®· 

UiH!r:P~rtHANf 

HHH (¥:HJ.$~3: 

~HUl1lrtJ~I:d~: 

l11111~~$.311P:M1f 

HHH1J)J$a<)~l= 

0.3803 

~~Hdltit.~!:OO.l~ 

H1Hi2~~4HP:Nf 

HWiUHO~~~t~Sn 

nnJot1P~oo:: 

lHW~Hl4tA.MF 

fHHJta!l9$~' 

0.3794 

0.0008 

0.8 
PARTICULATE ANALYTICAL DATA F'ORM 

Company: Dal·ltalia, Muskogee, OK 

Date: 10/30/06 

Location: Press Baghouse (EPN 40) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

:u::j:HHili~S.tl 

u=:~:N:\:;:ii:~~i :.:::\fi.(\AI~:,:(:Y.T:• 

llHlHll\l!l!iHllj~sz: 0.0002 

;::lll~lll~T~~~~~ lHHH lH !i{ijioaa ll 

lll!~;::llM~f;r~~ !lC~nl~~JGa~; 

HllHHlot:Eit:o6. 

~H1HH1:illl~l.~#t 

~lHHH196ll6J:~~~ 

\llllnU!OI-~~0.61 

;nnn~HrBii1l5W~.M: 

1~HilH1~9.6!J61:4.tl! 

96.6831 

0.0002 

96.6741 

8.81 

Run 2 

YHUil(H?:$1$\jH 

lmm~m~~~[~~~ 0.0001 

llHHlHltiii&J{)sl 

n;HHUS.ill~lm.l 

1il1lli11i0:7:tS(}i$1 

~llllllll;~~&f:.~l ::H~lli().?.t~O.l$1 

1;t 1;;; ;; wor6li<l~l 

;;r~l~li~1:HUl:AMl 

;nn?liCf1.~~9.2S; 

HH\iHlO.I:§{{}Sl 

\1Hi=lgi4~l~Ml 

H>li0.7l29.2:6~ 

10i.3013 

0.0001 

107.2927 

8.45 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) = mg/g 

ll:l;l;/:liltij~~~l iiliiliHlS!tll!l~Ml 

~n=HH~~98J6400i 

!;HHlHXW6.i0.6i 

~nnn~~i~t$§HP:Mi 

~;H:J;iH~98J54.:Sf 

98.646 

i

11ii.'!'.il!i 

nnHHHl0¥:91:GJ.6~ 

lllW:lll~~~~~l 

98.64575 

0.00025 

0.00127 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

n:H~H~djf:S$~~: 

;;l:m:~~~~~:~: 0.0002 

llllllll:l:.r~~l 1~1HHtt(l$lZ5~Z~ 

l;lllil:lit~r:.~: ~~wn~og;zs~~t 

\l\lll\tla~V.el.o~t 

>~Y~V.~i2~~tW 

H~U10~il41:lL 

HHHlliPV.eKo6: 

/1nH3~4~1~Ml 

~H1~~1l09.!241Cr 

103.2543 

0.0002 

103.2471 

7.06 

145 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal-ltalia, Muskogee, OK 

Date: 10/30/06 

Location: Press Baghouse (EPN 40) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Yaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker ~are Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in 'Rinse (mg) 

wnnn~wnn;ru;$1 

nm~2~9.4WeHO.i 

l~nHHUHiHHHt~~l 

0.0000 

n:HlHili t6.X061 

nnnn=rstoSrAMl 

:rrrrrr:1I?il1.!1:1~1 

!'!!i'!!~W!f~! 

:!!':!!~~~;:~ 

THHar~/1o~®1 

~lHlHH13i41:llP:Ml 

Y?t11~l1.r1:0.21 

112.7709 

0.0000 

112.7704 

0.50 

Run 2 

HH1~UlHi1illi11U36l 

~ ~ 1 ~; 121914 tilE~1 ~ 

rUnil~lllilil;Hl~;~it 

0.0000 

nT:CU:t:6V661 

H<YBi35l~Ml 

nr~lt~s;asial 

UHHHVtili:~JoS.l 

:lllHi{a~il4lPMr 

~%UU~:3lS$lS1 

!!·,!!!ill~,:~~~ 

1Hljml:16i6S1 

r=rHln~gi4~rP.M.r 

l~PlG3~95~5.l 

103.9519 

0.0000 

103.9516 

0.25 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) = g/g 

:~HHHlH1HHW~ool 

1H~~~iHlll~¥:$l:Q6l 

t:HHllS!l4Ql~N11 

~n~Hi03.Jl1541 

HHHlHtt/.6~®1 

~~ilH!lH3ig01llmil 

lHllHlfPg:~~l~6.4l 

103.1154 

il~HH~iO:.HD.XQ6l 

H=lH1HH7~~Q1~till 

i[1}1;tS3dlt5.Sl 

lH1HialO/H!/:G.6~ 

rrliW~rs:ssn~tvt 

=rn;;:riog~lt~r 

103.1153 

lE-04 

2.941E-07 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

;u;n>;~;t~&:~ 

:lH2~W.1Eibt 

;:;n;r:rH:l;r:il25\[ 

0.0000 

r)lHt1/61.b.ff 

~:YY8i36.~A~ 

)UH:91::75$~: 

HH1!~Ha111.61:d&.: 

lHlH3t:ts~P:tW 

:r;Y:;9~i7:5S$l 

\HHi.oi1P.I:b6H 

lHlUH7:~01~tW 

rnnnH9ZJ7:5Stv.~ 

nwnroi:1oV.o&.~ 

HhHl3~14$r~rw 

rrHn:~rtrsaa' 

97.7589 

0.0000 

97.7584 

0.45 

146 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal·ltalia, Muskogee, OK 

Date: 10/30/06 

Location: Press Baghouse (EPN 40) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

~nn:inlllHHtH:lHf 

lHnlHHlHjiti0.6l 

;i;:;i1:n;;;;;;Hl~~o; 

0.0003 

HH:lHi¢~6!1:@1 

;::;:::;~~l&~: 

UlfHHi~o/.91:0.61 

ll:m::~~~~:~: 

104.0121 

0.0003 

104.0080 

3.85 

Run 2 

;n~fHnHHlillHnUuH 

HHHHUHHtili!ooS.l 

HnHiHHllHllilaO.Ol 

0.0003 

iHHHliii&Jo6l 

YinlnztH~~P:NO 

lUHt~5t17:4i52l 

)/Hf1li:~J.b6.l 

nHlHiSlZ$iAM.l 

lnllnitOO)H1.~5tl 

;;;llllljltol9io6.1 

m::::i&k~:a~: 

1111 ;; ; 11fild.i9:t:<>a; i;i~Hl;H3~~~~M~ 

HUiW0.5t17:~~9.~ 

105.7452 

0.0003 

105.7420 

2.85 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) = g/g 

Ul~lnHHHHH2ool 

~w:l~U~M~rl: n:~uo&.l64S.Ol 

HUHnllfl~¥:0.61 

)1Yi2i~ai~M~ 

iiililiifQO:J64B.91 

106.64895 

l:ljl)!llltv.9.1:06l 

<:lHH1:~20l~Ml 

n~Hll o$..~489; 

}HH~lt¥:9¥:G.6~ 

lHnHnlS:1f-9nP:Ml 

)}l{Q$:J64$5l 

106.6487 

0.00025 

1E·06 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sample wei ht. 

Run 3 

:Hnl~lm~UlHnnlt 

HniHHHHnieHm~l 

H~H~ ~=~l~HjH1~;3mg; 

0.0003 

:l:lml;~~~r&~~ UU1HH~i$4~;li! 

Y\T1li.1:¥:d&. 

w::::i~i~~1~;1 

~UH1Habi.91:d~' 

WHiHlm$nlliMW 

UH~OllJ~40.4~; 

fHTjtt~iavo.&.: 

~;~~H ~!H?!sg;P.Ml: 

;=nn;aol~!B.4(jS:i 

101.8426 

0.0003 

101.8404 

1.95 

147 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal-ltalia, Muskogee, OK 

Date: 11/2/06 

Location: Phase II Scrubber Exhaust (EPN 29) 

Run 1 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw·•Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

~~iHllilillitJlV.$~~~ 

nnlolooiai3.1:1 

inH;WHHHiHli~&S~ 0.0002 

ilHHHHfii.S.t:OO. 

mm::~m:~:; 

lll:l:l;l:~~;r:: HHH406:J4.7:~ 

HWWH~ol:e/:001 

HiHHH~!l2$lA~l 

11Willliil&.A6~.0l 

mmnH~dl:ef:tl6i 

lHHHni~ta~~P::Ml 

Hkl\~Hl.6 .. =4~2ll 

106.4744 

0.0002 

106.4621 

12.18 

Run 2 

HHHHHbl1i:$5£ 

H10too12ia1~ 

~Hl;i;lnn:Hlng4fu~ 

0.0002 

HHHHtii6iosl 

nnnsi241AM~ 

;nn$®:QllliSl 

WlUHittli:6J.oS.l 

HiU!iH3~0:4=EMi 

~ilni H11()()~~4.I s i 

HHWW~PI~i()ei 

lHiiHil11:laEJi;4Ml 

Hlii1110~Hl3.2Si 

lHHHntGI:~J.QEii 

~HilHigiS$lP.Mi 

~~Hill!OOlO.a2UH 

100.0415 . 

0.0002 

100.0322 

9.06 

ACETONE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va«'Pa) = mg/g 

HHHmHHil~lH2~1 

iliHHllit~61:001 

~=lHHHl$~ltll!AM1 

i~lHill98:J6~001 

~~~~~~~l~~~~~:r:~ ;~;;nn;;n;98iS4.=Ell 

98.646 

;lnnn~lHJ~91:06l 

::::;:::::~~i~~l 

98.64575 

0.00025 

0.00127 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 3 

UUYHd!i.S~f 

lHtilo6.tztaz, 

HWli Hii;l:!:i:i~6.5.~ 

0.0002 

<HHHi.ill6ib.6H 

:/HHiaiJ9.!AMi~ 

nHli()~i5.S~$.: 

HHHH!l!~~vo~1 

~n;lnn~2t59.iP:r\f 

~UH1Q2l~Z~' 

HHHii6i.61:btt 

HHHl:H1.~i7:)~~t 

liHHl~O~i$2~~~ 

nHHiHa~V.6ib.&~ 

nHlU3~3Zl~Mi 

~<ll~02l5.24s: 

102.5326 

0.0002 

102.5246 

7.83 

15.6 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal·ltalia, Muskogee, OK 

Date: 11/2/06 

Location: Scrubber Exhaust (EPN 29) 

Run 4 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume 0faw) 

Residue in Rinse (Wa) = Ca*Vaw.j(·Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

·.Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

;;m;1;H:n;Hnilla6l 

1H1H2l9W.telt}.7:l 

;)j(lH::inHt2t 

0.0000 

tl1l1l:::l~:~~r~~l n:Hqos1~o.6: 

\'!,!,'!~S~!:~ 

~ HHHil0/:1~1:6.61 

:U~HHH1.~lt$l~~l 

l::::;;lHHtOSOO: 

lllll:m~~~r~~~ :~n=Hllt!lS0089~ 

105.0606 

0.0000 

105.0590 

1.60 

Run 5 

[[j;:;j; i~~ lillliliU361 

HH2194ia~1l 

:::;:::il:l:::;;:::li3Sl 

0.0001 

:\HiHt~i:61:<>6i 

HY=H~ib.$l;t.\Ntl 

l~:l:l:ltQ5l5~Sl 

:;l:l;l:ll~i:~~~ :Hnnwm>~~Z3~l 

lkjbl.u~oi¢6.1 

nn:: :Hl1:! 1=61 ~M: 

HH1105~52ll1H 

;nnnl6it~i:<>ei 

lnn:;H:a~Sbl~r\JH 

;::HdlO.SiSZHH 

105.5233 

0.0001 

'105.5210 

2.25 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va*Pa) = g/g 

:HHHHli1HU2ool 

~~~lllll~l~M:r:~1 i)jl~ll03.1ft5~ 

UHHHtt~6.ko6! 

:HHllllltg!~~ji?:Ml 

Hiilj1jfm~~~t5.41 

103.1154 

:~:;:::G~~m~~l Ui!i!lSSlJ$$~1 

ljlHl:OI:Hll:G.61 

::::::::::s•a5::pM: 

~11~;~~1~o&~it$$1 

103.1153 

lE-04 

2.941E·07 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 6 

HilU1<n=tit3&: 

HH2~9~1e~mi: 

:n\::nn:n:::::J~~l 

0.0001 

@Hl1iii.6¥.Q&.\ 

::::mi:~~~~; 

HiHHHtlv.6V:m&: 

wnnn\B~=taifrH~t 

H:nnH>biS03e/ 

1HiHtoiiPI.tti6.l 

:Hl:lH7.~i1:l~Mr 

:::::;ll0bJS030:: 

~Hnilt0.1:1b~b&.~ 

mnnn3~~s:~ML 

n?::looiso-gG:: 

100.8036 

0.0001 

100.8030 

0.54 

;. 

157 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal·ltalia, Muskogee, OK 

Date: 11/2/06 

Location: Scrubber Exhaust (EPN 29) 

Run 4 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca«Vaw*Pa 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

~eaker Tare Weight 

Date of Weighing 

Time 

Beaker Tare Weight 

Average Gross Weight 

Less Blank Residue (Wa) 

Average Beaker Tare Weight 

Weight of Particulate in Rinse (mg) 

nwn;111n~1HWHi1J 

~~HHH[i;IEiloo~ 

~lmiHH~H~Hli$001 

0.0003 

HWHHlii/.61:6.61 

HiHi~W~iU~6.ii?:Ml 

nHHllt4~i~®l 

HHHnfOil:ool 

)::):S:lZAMl 

~/UlJ4P~5®~ 

HHHlljoV:s/:061 

~lU~lHi7:~9~1AMl 

Hilin1t1ll!tJi~U121 

lWHHl~~~W~I:®l 

l1ll)ll3i@SHP::-Ml 

~~l~1Wfl4Ji4~()1 

114.1500 

0.0003 

114.1411 

8.60 

Run 5 

H11H11Hlilnnnnn;ti 

l:l:t:l:~;l:i:m:~~ml 0.0003 

HHHHili&J()61 

HYil:iMliiHP:Ml 

U}l®l~H~:gt 

HiH/tl/7io6l 

HiHU:B:l8iAMi 

U\YiOOt€>5.911 

HHHHHto/6!/(}61 

~~~liH1ii1:i®~!AMi 

~HlH~l00l65.03i 

ll1Hnn:o.~:61{)e; 

lUUiH~*t#;M; 

i~HiUll00~65001 

100.6597 

0.0003. 

100.6502. 

9.25 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume 0fa) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va·•Pa) == g/g 

:;HUHHWH2ool 

YH\~;;ftV:S/:061 

~H~ill~J~~Ott~lAMl 

~>YtOS:J64SOl 

CHHllllt~~ool 

~lHlillH~lgeya?~Ml 

~~n;~;llo.~:64B9l 

106.64895 

1HHHH1~~WS.1:~6l 

HHlHiH11:ii20lAfM~ 

1)1lllS~16~$9\ 

)l1H;ao.Y:9~~6l 

HHllllS:~~n~Ml 

nHlilll05~~85l 

106.6487 

0.00025 

1E·06 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

wei ht be subtracted from the sam le wei ht. 

Run 6 

· H)Hlni1HUf 

nLH?;iElbK 

1 ~1111 u Hi 1 n 11 n30.0. ~ 

0.0003 

WH111i61.o6H 

:::m:~~~~~~; 

H?il!ihi:d5.= 

><d8-::2s:AM1 

H:HlD1i068$:. 

HUHHibl6¥:d~: 

1inmllitciatArW 

1i1HHa07:J05!4.~1 

l~lilllll~~g~r&~l <Hil0~10.54l' 

107.0683 

0.0003 

107.0542 

13.75 

158 
FILTER ANALITICAL DATA 

Company: Dal-ltalia, Muskogee, OK 

Date: 11/2/06 

Location: Phase II Scrubber Exhaust (EPN 29) 

Filter ID Number 

Date of Weighing 

Time 

Gross Filter Wt. 

Date of Weighing 

Time 

Gross Filter Wt. 

Ave. Gross Filter Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Date of Weighing 

Time 

Filter Tare Wt. 

Ave. Filter Tare Wt. 

Wt. of PM on Filter (grams) 

Total Weight of Particulate (mg) 

Run 4 Run 5 

!$~$.1Hl)H!!Hi 

::,::!~~~~=: HH\QU$$.131 

.!:!::~1~~6,~! 

HHUHP~$f7:$1 

0.3874 

==::=:::;f~i· ··'Jn=;j= 

H:nn::·~~~- · ~~~: 

HHH2l4QiP:M1 

lHUlHO~~~l 

Hi1jniot1!oto~1 

iH1HS.~!41:1AMi 

nnn:JK~6421 

0.3642 

0.0232 

23.2 

$o~nHi~HUWj 

t!!:!!~~~Wl~! ~H1HOi3SS~H 

nn~HH~11~6lma; 

111Hl~4.~lP:M1 

)1HUlO;~aSQl 

0.3786 

::::::::=;;1\=Jn:i~a···= 

·~;:~:i~~:\Y.i:~~ .~ 

HHl~a~lP.tW 

:flHH!HOt~a~a; 

=;=;~~~oiH;oiaa~ 

;:;;;;~~5.=~M; 

:!i~ili~1lo\~~~~; 

0.3643 

0.0143 

14.3 

Run 6 

i$HlG.~iW~iUfH1iH 

H~~\lllijl$1®:~ 

jHi1:~~~HAMU 

~H\(f:i~$1.01 

UHUMiHJsY:P6i1 

f1H~~~()J?:MH 

:HHHHlQlaar~n 

0.3871 

1~~Wd~ot.$.f:O.~t 

nHiatl3SHP:Mn 

:JHU;o.~aa5t 

,:,:,~~~~~- :\lHHQ.4$$®l 

0.3651 

0.0221 

22.1 

159 
Sheet1 

Summary of HF, HCI, and Cl2 Analysis 

Plant: Dal-ltalia, Muskogee, OK 

Date: 11/2/06 

Location: Scrubber Exhaust (EPN 29) 

Run# Imp# Volume Dilution Fl-, ug/ml HF, mg Cl-, ug/ml HCI, mg 

1 1 & 2 350 1 0 0 0 0 

1 1 & 2 350 1 0 0 0 0 

Average 0 0 

1 1 & 2 350 1 0 0 0 0 

1 1 & 2 350 1 0 0 0 0 

Average 0 0 

1 1 & 2 350 0 0 1.11 0.399378 

1 1 & 2 350 0 0 1.03 0.370594 

Average 0 0.384986 

Run# Imp# Volume Dilution Cl·, ug/ml Cl2, mg 

13&4 250 1 0 0 

1 3 &4 250 .1 0 0 

0 

13&4 250 1 0 0 

13&4 250 1 0 0 

0 

13&4 250 1 0 0 

13&4 250 1 0 0 

0 

165 

Page 1 
Conditions 2.53 ug/ml Fl- in H2S04 

: 2 .. 51 ug/ml Cl- Ln H2S04 

Date 11/08/2006 

Time 09:os:ss 

256 .. 000mV 

Component 

-25.600mV 

Retention ·--·-·--·-·-~~ ........ ,_ .... -.... :"""""--·--·---· .. ---·---·-·-·-.. ···-·-···-··""'"""'""""""'--·-·-·-·"'"'-·--·----···-........ __ ,_.,.,,.,_,_,_,_, ... , ___ .. ,_ ....... --:·-.. 

FlClFlCl-

•I! li .. 

::55:·- ·~f:~· :'-•1 

I 

31""'"" 

I J ... -.. 

5 -·-·-· 

L ................. ~--.. ·--·-.. ·--.. -········--·---· .. ·-·-· .. ··-.. ·-·-··-·-.. ·--·-----·--·-·~:~ ............................... --·-·--·-·--· .. ···-·· .. ··-···-···---............. -.. 

Component 

2 

Number Retention 

1 

2 

1 .. 016 

1 .. 550 

Area 

163 .. 36 M 

144.40 M 

External Units 

1.49 ug/ml 

2.25 ug/ml 

3.74 

Area External 

163.36 M 1.49 

144.40 M 2.25 

167 
Conditions 2.53 ug/ml Fl- in H2S04 

: 2M51 ug/ml Cl- in H2S04 

Date 11/08/2006 

Time 09:20:35 

-25~600mV 256.000mV 

Component Retention Area External 

FlClFlCl1,.---·-·-·::r-------------·----·----··--·----------·---·----·--··-------··-··-····---

.r/ 

I. 1·--· J~·M• 178.95 H. 1.73 

I• 

1 , 566 ··;·~;::;::;~~:::::uonz:• 150.10 2 • 35 

2 ·--" 

3 ...... 

4 ·--... 

5 --· 

6 

Component Number Retention Area External Units 

2 

1 

2 

1.033 

1.566 

178.95 M 

1.50.10 

329 .. 05 

1.73 ug/ml 

2.35 ug/ml 

4 .. 08 

168 
Conditions 5~06 ug/ml Fl- in H2S04 

: 5.06 ug/ml Cl- in H2S04 

Date 11/08/2006 

Time 09=29=19 

-25~600mV 256~000mV 

Component Retention 1'""'"''"'''''''"''"!1""'"'"'"""''"'"'"''"'"''"'""'"''""''"'"'"'"""""'""'"'"'"'''"''"'"'"'"'"''"'"'"''""''""'"'"""''"'""""'"''"'"""'"""''"'"'"'"'""'"''"''"'"''"''~'m'"'""'''''"'"''"''''"''"''""'"'"'"" 

(unknown) 

FlClI i; 

0.7831 ::. ... ;::::::::::::•· Q 1 I ••••••••••••••••••••u••••••••••••••••••·•••••••••••h••"·~Uit:ar:l;ld5:t1UI rtE•ts• 

t f"""" ,.,)t"""""""'""""'""""'""""""'"'"'""'""' I ' 

1. sool .... i.'""""""'-"""'"'"'•••r:nrunr.I:U:U' I :!·i:::::::::::::::~:::::::::::::: ................................................................................................. -.................................................................................................................. . 

2, ......... 

I 3' ...... .. 

4 ........ 

5 ··~·"'' 

6~ 

I. . . . ! ....................... : ............................................................... _ ....... - .............. ,_.,_ ............... _,_,_,., ....................................................................................... .. 

Component Number Retention External Units 

FlCl2 

1 

2 

0.950 

1.500 

465.12 M 

301.07 M 

766 .. 19 

5.78 ug/ml 

4.65 ug/ml 

-10 ~43 

Area External 

109.64 M NIA 

465.12 M 5.78 

301.07 M 4.65 

169 
Conditions 

Date 

Time 

5.06 ug/ml Fl- in H2S04 

5.06 ug/ml Cl- in H2S04 

11/08/2006 

09:32=01 

256.000mV 

Component 

-25.600mV 

Retention 

FlClFlClr····--·-.. ·-:.-t-····--·-·······-·····--·--·-···· .. --................................................................................................................. _ ....... ____ ... . . •J ·'· ..;1 

H: 

ri: 

1 • 1 ....... ~ ::::~~=:~~::::::::::.:::;:::::::::::::::::::::::::nr•mmr• 1,.-· 

1.550 

2['"'" 

r·· 

4j ........ 

"f;~·;:::;:::::::;:::::::::::::::nrt• :•1:1 

t- ' 

6~ i ·. ·. 

1. ................ ..: ........ ,_,_.,.,. ........................... _____ ,_,., ........ _______ , _____ ., ___ ,_,_, __ , __ ,, __ ,_, ..... ---··-··· .. --·-···-·-· .. ···-····-·· 

Component Number Retention Area External Units 

2 

1 

2 

1.016 

1.550 

453.47 M 

304.60 

758.07 

5.66 ug/ml 

4.70 ug/ml 

10.35 

Area External 

453.47 H 5.66 

304.60 4.70 
Conditions 7.58 u.e/ml Fl- in H2S04 

: 7.52 ug/ml Cl- in H2S04 

Date 11/08/2006 

Time 09=41:01 

-25~600mV 256~000mV 

Retention r .................. -r····""'"'""'"'"""'""""'"'""""""''"""''"'"'"'-""'"'"''"'"""""'"""''''""'"'"''''"'"'"'"'""'"'""'""'"'"'"'"'""'''"""""""'""""''""'"""''""""'"''"'"-·-· .................... , Component 

FlClFlClI II I I I~ ! 

1 .11--· J:::~~==::.::::::::::::::::~:::::::::::>•........................... ; 

1 5 3

1 I!"•,,,.,,,.,,.,,.,,,.,,.,,,,.,,,.,,,.,.,.,,.,.::::IIIIIIIIIIIIIHIU13nlllll' ·' 8 ':., ............................................. .. ·: 

4 ·-···· 

...................... ~ ................................................. : ...................................................................................... _ ... , ...................................... _,_, __ , .................... 1 

Component Number Retention Area External Units 

2 

1 

2 

1 .016 

1.583 

694.10 M 

452.05 

7.80 ug/ml 

7.22 ug/ml 

Area External 

694.10 H 7.80 

452.05 7.22 

17~ 
Conditions 

Component 

Date 

Time 

Retention 

7.58 ug/ml Fl- in H2S04 

7.52 ug/ml Cl- in H2S04 

11/08/2006 

09:44~03 

-25 .. 600mV 256.000mV 

1 

.. ----···-·"·~~ ......... _, __ ,_, ...... --·-·····-··-.. ···-···--· .. ·--..... _ .. ,_ ... ~--.. ··-··-·······-····--·· ................................................ - .... - .. - .. ·-·-···---·· 

·" 

*· I· 

FlCl-· 

FlCl-

,I_ 

1 • 1 ·-··" ~: :::~===~::::::::::::::::::::::::::::::um:~n~"""''"'"'"'"m::llr.lllr.:nm·•rr ·'I'' 

1.550 

3 ........ .. 

I 

4 ......... 

5 ...... . 

6 ·-·-.. 

Component 

2 

·1:r~.:.========·····=-· 

Numbei Retention 

1 

2 

1 .. 033 

1.550 

Area 

666 .. 19 M 

458.05 M 

1124 .. 24 

External Units 

7.48 ug/ml 

7.31 ug/ml 

14 .. 78 

Area External 

666.19 M 7.48 

458.05 H 7.31 

172 
Conditions 

Date 

Time 

10~11 ug/ml Fl- in H2S04 

10.02 ug/ml Cl- in H2S04 

11/08/2006 

09:53:33 

256~000mV 

Component 

-25.600mV 

Retention 

FlClFlCl-

~-·-··--··l:···········~·-···-·"'"'''"-··----····-····-···-··-·-·--··--·---···-·-··--···""""''"'"'"""''"'"'"''"'-·--·-······---·-·····~---··-···--··1 

II I 

1: . 

I! 

1 • 1 ''"'"" ~:··:~::::::::::::::::::::::::::::::::::~::::::::=::::::::::~:::::-.::::::::::::::::::::::::::::::::::a•tlllllll011111mlhlllt1Ctt.ll:tl1tlllliiUI1" li'' 

·(.t~r~===-~:==~=~~~~~~~~~~::::::::::::: _____ ·-·---··--·---·--·---·----·-----···---·· 1.583 

2 ··-·-

3 ·--· 

4 ·-·-

5 --.. 

I . '[-·· . 6 : 

····---··-.:--···--·-·-···· ............ _ •• ,., ____ ,_,_, __ ,_, ____ ,_, __ , .. , ... ___ ,_, __ , __ ,_, .. ,_,., ___ , ... , •• __ ,_, __ ,_, __ ,_, •••••• _,_, __ ,_, __ . __ , __ ,,_, __ .1 

Component Number Retention Area External Units 

2 

1 

2 

1 .. 033 

1 .583 

1014.52 M 

648.70 M 

1663_22 

11.36 ug/ml 10.71 ug/ml 

22.07 

Area External 

1014.52 M 11.36 

648·. 70 M 10.71 

173 
Conditions 10.11 ug/ml Fl- in H2S04 

10.02 ug/ml Cl- in H2S04 

Date 11/08/2006 

Time : 09:56:01 

-25.600mV 256.000mV 

Component Retention Area External 

(unknown) 

FlClr-·---:r----··-------------------------·----.. --·-·------------1 "If 0.850 :: .... · .. ·:::::::-~:.... 114.72 M N/A 

l, 1·--· ::,:~::::::::=::=::::::::::::::::=:::==:::::::::::::::::o~:::::::::::.-.:::::::::::::nnll"'l"ll~'" 979,88 M 10,97 I, 

1.550 f.?:==--=---·-- 674.60 H 11.14 

2--

5---

I 

6, . I 

l ____ j_ __ .,., _____________________ ~: ______ j 

Component Number Retention Area External Units 

FlCl2 

1 

2 

979.88 M 

674 H60 1"'1 

1654.48 

10.97 ug/ml 

1:1..14 ug/m.l 

22 .. 11 
Calibration file : Fl--cal 

AMOUNT INJECTED 

AREA 0.000 10.110 o . o o o r:::::~ ......... ~ ...... _ .............................................................. -.................................................... 1 

I ·· ... 

···· ....... . 

·· .............. . 

. ,

·· ... '· 

\ ..•. . , 

'···-'· 

'\· .•.. 

····•··•··•· ... 

··. 

··•····•··· ....•. 

'·· ..... •., ., ., 

·· .. . , 

., 

\t 

... '· 

·· .. , 

·,, 

'·, ., ., 9 9 7 . 2 0 0 _______ ,, ......... --..... ,. ... _,_,_, __ , __ , __ ,_, __ ,. __ ,_,_, ____ ,,, ______ ,., .. -~:t.. 

Avg slope of curve: 98.62 

Y-axis intercept: 0.00 

Coeff of lin regr: 0.79 

No. Area 

0.000 

171 .155 

457.175 

680.145 

997.200 

A~ount 

.0.000 

2.530 

5.060 

7.580 

10.110 

CF 

0.000 

67.650 

90.351 

89.729 

98 .. 635 

1 

2 

3 

4 

5 
Calibration file 

Avg slope of curve: 66.05 

Y-axis intercept: OMOO 

Coeff of lin regr: 0.80 

Area 

0.000 

147.250 

302.835 

455.050 

661.650 

Amount 

0. 000.; 

2.510 

5.010 

7.520 

10.020 

CF 

0.000 

58 .. 665 

60.446 

60.512 

66 .. 033 

1 

2 

3 

4 

5 

176 
Conditions Dal-Italia, Muskogee, OK Scrubber Exhaust 

Run ~1 Imps 1 & 2 

Component 

Date 

Time 

Volume 350 Dilution 1/1 

11/08/2006 

10=40:22 

-25.600mV 256.000mV 

Rete n t i or--··· .. ··-.... ~·-···-···· .................................. -...... -.................... -...................... ,_ .. , .................................................... -., .. _ ................. _ ......... ---····- 1 ~ fi II I; 

1 ····- ·if::::::· 

:r:ll· 

2 ....... 

3 -···· 

4 ···-· 

I 

s! ... -.. 

I 

6 ...... . 

I"~· 

·:;1. .. 

;.t 

: •:·:: ........ ._.-.............. _, ....................................... . 

Component Number Retention Area External Units 

0 0.00 0.00 

Area External 

183 
Conditions Dal-Italia, Muskogee, OK Scrubber Exhaust 

Run #1 Imps 1 & 2 

Component 

Date 

Time 

Volume 350 Dilution 1/1 

11/08/2006 

10:44:14 

-25.600mV 

Retention 

256.000mV 

, ...... ·-·-·---··:.~·---··· .... -·-·--·-·-·--·---·-·-·---·-··-·-··--·-----.. ·-·-----·-·· .. -··-······ .. -··-·-.............. _, __ ,,_. _____ .. , ..... --··-·--··-··- : .·,, • r;l, • .. . !r 

: ~ 

1-····· l·:=··· 

:!:r 

•. I 

... I 

':'t:"•:!• 

2 ·-· 

3--·· 

4 --·· 

5 ·-·-

6 ........ 

ol_, .. , .... ...,,, .. _,_l_lloll-••--•-t•I---··--·~·---·-·---IO•t,t .. ltooo-o•o ... otol---··-•-••to•--.. -·-· .. •tooto•• .. ••-o•ooMo-ooooooo .. -••-•--•-•-toiN•I-••oool .. ---••o•--Po ..... • 

Component Number Retention Area External Units 

0 0.00 0 .. 00 

Area External 

.184 
Conditions Dal-Italia, Muskogee, OK Scrubber Exhaust 

Run #2 Imps 1 & 2 

Component 

Date 

Time 

Volume 350 Dilution 1/1 

11/08/2006 

10:53:00 

-25.600mV 256.000mV 

Retentio 

--:.~: ..• :--·-------------------------·-·--] 

1·'""" ., ~~::· 

:f•' 

'il.. .... 

:'1 

: ·:1. 2 ........ ' ·:,1 

:if 

: ·1:... ___ ,_~ ... ------.. ·-····--· .. -·---· .. -... _, __ ,_, __ , __ ,., ..... ---·-·-··--·-.... ~-·---···-·····---· .. ·-··-----.. ---·-"·•-···---· 

3 ...... 

4 ........ 

I 

sl-·-·· 

I 

6 ........ 

1 .......... _ .......... : ....... _, .. __ , ......... --·-···-· .. ···-·-··"·'"'"•'-······-···-.. ·-·-·--·····-·--.. -· .............................. __ ,, __ ,_,,_,_,., .•• ,_,., ............................... .. 

Component Number Retention Area External Units 

0 0 .. 00 

Area External 

185 
Conditions 

Date 

Time 

L 

4 A""'" 

5 UAOHI 

6 ......... 

Dal-Italia, Muskogee, OK Scrubber Exhaust 

Run #2 Imps 1 & 2 

Volume 350 Dilution 1/1 

11/08/2006 

10=56:14 

. . .,,._._ .. , •• ,,,..,,.,.., .... , .. " .. "'''u'""u"'"'"''"'""'''"""'"'"''"'' .. ''"'''''''•tloll._,,..,.., ...... .,.,.,,,., ..... , .... ,,.,., ... .,.., ... ,.•-••••,.•••.,•••••••••n .. •••••"J• .... • .. ••••••••""''''''' .. "''-U"II'II'Itlll .. ltt•••-•«•MI«IMI••••"''"''"'•••"' .. u'-'"''•n• 

Component Number Retention Area External Units 

0 0 .. 00 0.00 

186 

External 

N/A 
Conditions Dal-Italia~ Muskogee, OK Scrubber Exhaust 

Run #3 Imps 1 & 2 

Component 

(unkno~m) 

Date 

Time 

Volume 350 Dilution 1/1 

11/08/2006 

11=06:54 

-25 .. 600mV 

Retention · 256 .. 000mV 

r ..................... ,r .............................. _ ................................................................................. __ . __ .......................................................................................... ____ ... _.'" ___ ..... . 

~ 

!~ 

0 , 850 ,}::::::lr 1........ ~I 

1''1 

~::r 

··ri:~:::~· 

I 

. 61""'"" 

I 

; . L .... ---~-···----·--------·---···------·--·---··-·----------------........... _:~-·------------"-··-··-...1 

Component Number Retention Area External Units 

Cl- 2 1 .. 616 64 .. 95 M 1 .. 11 ug/ml 

1 64.95 1 .. 11 

Area External 

61.80 N/A 

64.95 M 1.11 

187 
Conditions Dal-Italia~ Muskogee~ OK Scrubber Exhaust 

Run #3 Imps 1 & 2 

Component 

( unknotvri) 

( unkno~m) 

ClVolume 350 Dilution 1/1 

Date : ll/08/2006 

Time 11:1.0:03 

-25.600mV · 256.000mV 

Retention I ........................ F. ............................................................................................................................................................... - ...................................................................... .. 

0 3001 

!!....... . I "!!r• • I •""' , ... 

. J1 

. .~~::::::t· 

0, 1""'"" •:11 

..... f'' 

1.~ 

1.61: ·-- :;~~: .. _, 

3! ........ . I 

4 ......... 

5 ........ 

6 ....... 

. ' IIIIIIIH'IIOfiiiiiOIIIIofi~: .. III.IIOoti .. IPIItiJIIIIIII.I ... I+tlllll .. tiNI.IIJIII .. It+IHIIII ... I .. Itolll"l ... llll-llll-ll.llllftlllll .... lloiiiMitUIIII .... tl ... loolllltl•tlotl+tllllloiiUII ... IIIflllllltnll:l+tlttlll .. l~ll4 .. llt.lflloii .. IIIIII•IIO:I•IIOIIIIIOI .. III ... II .. I"I ... IIIIIIII 

Component Number Retention A1ea External Units 

Cl- 2 1.616 60 .. 45 M. 1.03 ug/ml 

1. 60.45 1.03 

Area External 

136.50 N/A 

74.35 N/A 

60.45 M 1.03 

·188 
Conditions 

Date 

Time 

5.01 ug.ml Cl- in NaOH 

11/08/2006 

12:17=23 

-25.600mV 256.000mV 

Component Retention r----·-l~-·-··--·---·-·--.. ····--·------·-···--·----·----·-····-·--·--·--·--···--:-·-·----.. --·-·-·--·-·-·----··--·····--·1 

I .~· 

0 .83~ ~:.::".·.:>:::=.::::;;==~·-~· .. =·~···~ (unknown) 

Cl- l • 7 SO ..... n••:t••;:···:: ... :;~:::::::::::::::::::ti~IUtt\Uuuutuuu.nutumm•lmtummttuiiUnul• 

2 ""'"" I: 

5~ 

·-··--·--·-L ................... _____ , _______ ............ _____ ..................... ---·-------··---··--·--·----_j 

Component Number Retention Area External Units 

Cl- 2 1.750 275 .. 40 M 4.44 ug/ml 

1 275.40 4.44 

Area Externaj 

1392.20 N/A 

275.40 M 4.44 

197 
Conditions .. Date Ii9ba~~o~t cl- in NaOH 

Ti.me 12:22=18 

-25w600mV 256ftOOOmY 

Component Retenti o~---·---T·----------~---·----·------------··--------··-----·----··--·------·------

0.833 ~ 

1 I 

l -···· ,• 1 ,··::.;.~:~:::=~~:::=~~::::::;:~.::::;:::::::::::::-.:::::::::::::::'''~'"'"'"'r.llllltll=:.•o::t~~ j 

:: .. ~.:: ............. : 

(unknown) 

Cl4 ...... 

5 ......... 

6 '"""" 

""''"'"'"'"''"''":"'"''"'m"'""'"'"""'"''"'"'"''"''""'"''"'"'"'*'"''""'"'"'"'-"""'"'"""'"""''~'"'"'"::, .... ,,.,_,.,,,,,,,,.,,., • .,,.,,,..,,.,,.,,.,,,,,.,,. •. ,., • .,,,.,.,.,.,~,,..,,.,.,,.,,,..,,.,_,,,,.,,.,,.,,,,,.,l 

Component Number Retention Area External Units 

C.l- 2 1.750. 270.50 M 4.34 ug/ml 

1 270 .. 50 4.34 

Area External 

1056.60 N/A 

270.50 M 4.34 

198. 
Conditions 

Date 

Time 

7~52 ug.mi Cl- in NaOH 

.11/08/2006 

12:26:01 

-25.600mV 256.000mV 

Component Retention 

(unknown) 

Clf ........... -....... 'j; .................................................................................................. _, __ .......................................................... _ .......................................................... ou ........ j 

I II • 

~ . 

o. a! tL_,.., t;.:::.=:=:..-:::::::===-=--

1 . 733 ~~=~~~;J:=~-"'=::=::::::::::::==::::,····~··~····"'""'' II, 

... 2 ........ 1:: 

~!: 

4 ....... . 

5 ....... 

6 ......... 

1 ....................... : ........................................... ~ .................................................................................................. ;: ...................... ,_ ................................................................. ... 

Component Number Retention Area External. Units 

Cl- 2 1.733 397.90 M 6.73 ug/ml 

1 397 .. 90 6 .. 73 

Area External 

1170.90 N/A 

397.90 M 6.73 

199. 
Conditions 

Da·te 

Time 

7~52 ug.ml Cl- in NaOH 

11/08/2006 

12:32:00 

-25.600mV 256.000mV 

Component Retention . r ......... -....... r ................... -=-·············-··-·····-····---··-··-·····-············· .................... -................................................................. _.,, ........... _,, . 

~ i 

0.833 ~~~ I 

1. 76: ~2~[:::~~:=~,~~~=-~=~· I 

2 ........ !i:: 

(unknown) 

ClI 3 -··· 

4 ...... 

5 ...... . 

6 -··· I 

--·----~~___:,_ ________________ . _________________ ..:.._ _______ (.__j 

Component Number Retention Area External Units 

Cl- 2 1.766 419 .. 95 M 7 .. 04 ug/ml 

1 419.95 7.04 

Area Externa 

1163.10 N/A 

419.95 f·l 7 .0· 

200 
Conditions 

Date 

Time 

10~02 ug/ml Cl- in NaOH 

11/0S/2006 

i2:36:32 

-25.600mV 256.000mV 

Component Retention Area Externa. , ...... ,_ ........... 'li'"""'"'"'"""'"'"'"''"""'"'"""'"''"''""'"''"'"''""'"'""'"'"'"''"'""."''""'"'"'"'""''"'"""'''""'"""'"''"""'"''"'"'"'"'"'"'"""'"'"""'"''-'"'"'"'"''""'""'""""'"'"'"'"'"'-"""'1 

I ..J. 

0 • 8 3 31 .• 1 ;!,,.,_,., •• ,_ •. ,., ... .,._, .. ,_,.,"' .. ""-'"'"'""""""""~'~"'"""tl''_,tllnll:tntrn• I 120 7 • 8 0 N /A 11••'""' •' I : , ..... •••"'"'-""""'"'""""''"'"'"'""'""'"-"""'"-'"''' 

( unkno~m) 

t •• • .... ~ ... • 

•' ,I 

ll~:::::::::::: ..... ; ................ -........................ , .. ,;................. . . 1 7 50 , , . 

1 

.. : .. , •• , .............................. ~ •• , .... , ..... ,,."''''''ut••••Etlltnnu•m~SUIUIMtul:ltt~UmuEinmmtnmEumnuln1UIIPilUUtlttU5:tutiUIUtnnu••n• 52 9 ,1 0 M 8 7. • ........ II, •. 

2 : 

Cl4 ....... . 

6 •.•.•. 

I ,: o 

IIOIIOIHIIIUtofiMIIIIIolllllltiiiHII.I+IIIUI+IIt•ll•lllt9II•IIIII•II .. I .. IIOIIolll.lllllllllflllollt11111HifiiOOI11fiiU ... I .. o ... IIOII•olooll111101oii .. IIOIIIIIINI .. Iltiiii11111011UIIIIIt•o•IIIMINIU .. IIIIIHI .. III.IHIMIIIIII .. IItloloof .. t•oti04IOOfiOto .. IIOI .. IIOIIIIIoiOioiiOOIO 

Component Number Retention Area External Unl.ts 

Cl- 2 1~750 529.10 M 8.71 ug/ml 

1 8.71 

20'1 
Conditions 

Date 

Time 

10.02 ug/ml Cl- ln NaOH 

11/08/2006 

12=41=32 

-25.600mV 256.000mV 

Component Retention . ····: .................. ~r·· ............................................................................................................................................................................................. ; ........................... -..................... ~ . 

,, 

0 ' 8 3 f "'""'' •' •' ,• 

1 

:L::::::::::::::::::::::::::::::::::::~::~:::::::::::::::::::::::::::::;:::::::•=r.IIIWIIliiiiiUilll' 

,·· , . .1"!•"' .. ·t~ 

1. 7 66 ~c::.:::::~;::.:::-.:.:::::::======:==-::=."::.'=··~ 2......... I: 

( unknot~n) 

Cl3 ......... 

5 ........ . 

6 ....... . 

I I . 

I . . J llo41ootll'liilo4P41o"l""l:lll•tlliloll•ll .. lll+llfoti+IIIIIIIII .. IIII<IHIIIfiiPI+I'II.IItfiiiiMIII1IIHIMIOI ... IMIIoiiMIUitfiiiiiiiiHI .. ::.,. .................. , .............. ,UHIMI .. IIII+tl+tllloiiiiiHIIIIOIII ... INIHIIIIIIO+It41Mitii .. IIIUI+IIIotlllln .. III .. IMIUnootiH11olllllllllllll 

Component Number ·Retention Area External Units 

Cl- 2 1.766 531 .60 1"1 8.73 ug/ml 

1 8.:73 

Area External 

1092.00 N/A 

531.60 M 8.73 

20·2 
Conditions 

Date 

Time 

2M51 ug/ml Cl-. in NaOH 

11/08/2006 

12:47=36 

-25.600mV 256~000mV 

Component Retention Area Externa J""""""'""'''"';!l''"'"""'''""''"''''""""'"'''""''"''"'"""'"'"''""'''"'"'"""''""'''''""'''"'.""''''""'""""'""'""'"''"'"''"''"''"''"''"'"'"''"""'"''"""'"'"~""'"'"'"'''''"'"'"'"''"'"'""'""'""'~"'"'"" 

I ·i' 

0 • 831 )~--·-----·-··-··-·-··------------............ ~. 1382 • 20 N/ A 

I ;;~~~.)·-" .. ,.---·------.. ---·-·--·-·-·-··--- . 

(unknown) 

Cl- 1. 7SO ........ , .. :: .•. r. .. "i::~:::::~:~:m:::::::::.............................. 155.60 H 2.1 

2t'""'" : 

I : 

4 ....... . 

Component Area External Units 

Cl- 1.750 155.60 M 2.13 ug/ml 

1 155.60 2 .. 13 

( 0 

203 
Conditions 

Date 

Time 

2.51 ug/ml Cl- in NaOH 

11/08/2006 

12:59:40 

-25.600mV 256.000mV 

Component Retention Area External , ..................... ::··········"·"'"''"'"'"'"""''"'-'""''-"'"'"""'"""'"'""""""'"'"'"'"'""'"'"'''""''"''"'"'"'""'"'"'"''"'""""''"''"'"''"'""""''''""'"''"'"'"''"'""'"''"'"'"'"''"'"'"'"''"'''"'"'"""1 

J I 0. 833 :· .! ......... -·-···-····--·· 1145 .1 0 M N/A l .: ..... •' •'. : ................. -.... "'""""''-"''..:::::-.:::::::::::n•~~·••mn~mlm:t'!.,,r 

,• ,I 

·:.:: ................ ·: 1.733::~1'1"!!'!'"""•"";""'""1nii111U:UIIII' 147.30 M 2.73 .. '1•·: ........ 

(unknown} 

Cl2'"'"'" • 

4 ......... 

5 ........ 

6 ....... 

. ,: ,..,'t''"'''''_' .. ''''''''"'+t'"'" .. •'•'''"'' .. ' .. '''' 10' 11•••HoHoo+•nwoMoo•l•" .. 'lti'UIH•• .. u•"""'''''"'''' .. "'''"''*''''''''"'.,.'•"''"''"'''"""+'' .. ""' .. ""''ttu11,.1111, .. ,.,,,,, .. ,,,., .. ,,,,,"''''u1,. 1w1,..1 .... ,,_,.,, .. , .. , .. , ........... ,,,.,.,., 1, 11, 11111"''"'" 

Component Number. Retention Area External Units 

Cl- 2 1.733 147 .. 30 M 2.73 ug(ml 

1 147.30 2.73 

204 
Calibration'file Cl- .. cal 

AMOUNT INJECTED 

AREA 0.000 10.020 

0 .. 0 0 0 ~·~:::·····"'"'"'"""''""""'"'"""'""'"''""'"'"'"'""'"'"''''''''"''""""''"""'"''"'"'"'''"'"""'"'"""'"'""''"''''""""1 

I""··. . I I ··········... I 

I \.. I t •••• 

··,\.,· ... 

... 

······• .... 

'\ ...... \ 

\ ..•.••.. 

'· ·~ ...... 

·· .. ·,, 

\ ....•...•... 

'I 

'•. 

53 0 • 3 50 -----·----·-----~------·------~----~--·--.. -~~~~~~J . 

Avg slope of curve: 52.92 

Y-a>< is intercept: o.oo· 

Coeff· of lin regr: 0 .. 90 

No. Area Amount CF 

o: 0.000 ·o. ooo 0.000 

1 : 147.300 2. 510'' 58.685 

2: 272.950 5.010 54.481 

3: 408.925 7.520 54.378 

4: 530.350 10.020 52.929 

1 

2 

4 

5 

--
Conditions Dal-Italia, Scrubber Exhaust 

Run #1 Imps 3 & 4· 

Component 

(unknown) 

("unknown) (unknown) 

Date 

Time 

Volume 250 Dilution 1/1 

11/08/2006 

13:38:31 

-25.600mV 256.000mV 

Retention . ·----·~·-~-. ·-------·---·----··--·-·-------·--·-~--·---·-----·----·--· 

I! 

0. 83~ ·····- . l'-~:=~~::-.:::::::::::::=:::::::::::::::::=:::..--··"'"'""'"'"""" . ,,.. 

:n:l .·. 

: ::J. 

1: 85 ~ '"""" ~ ·f.i~;;=~~-.. ::•=muommu•l'~3' I 

4 ....... . 

I 

L ·I 

I 

6 ........ 

t'"''"'"""-•-~---·•-•-••-•-.:.~_,_,,, __ ,:.,,. ___ ,,_•••-••••-•·--'""'""-'"''"'"'"'"'-"'"''""'""''"""""'"""''"'"'"-'"'"'-------··--·•••"'"'"'"-'"'"'"'"'"'"~-..1 

Component Number Retention Area External Units 

0 0.00 0 .oo. 

Area 

573.20 

100.50 

226.50 

212· 

External 

N/A 

N/A 

N/A 
Conditions Dal-Italia, Scrubber Exhaust · . Run #1 Imps 3 & 4 

Volume·250 Dilution 1/1 

Component 

(unknown) 

(unknown) 

(unknown) 

Date 11/08/2006. 

Tim.e 13:40:57 

-25.600mV · 256.000mV 

Retention r ...................... i:;:·····-.................................................................................................................................................................................................................. -....................... 1 

I ,• 

I r; I 

0 o 616i t .. .,,~.,••-••oO•"--"'""''"'"-'"'"'_'_'"'"MoOo" 

11

1 ! ,., ... ••••• .. ,, ... ..,., .. ,..,••"'•"'"'""'" .. "'" .. ••"""'" .. ,.,ltUttl~!llt:EttiS:IntEt:nUiU' 

... u.... '• z··· ....... . , ... ... :·:j 

I ; ·:,. 

t83~·- :~. 

I 4 ........ 

6 ........ 

. .• Hl-lllllll--l·l-lll-lllf .. 60o .. _ .. II-·IOIIWI .. I_I .. I .. t""IIIIO•IIIII--·-··---···-····• .. toot--t-.. IIIMI-:...-... HI .. IOOIIMI-1Ht'IIIHI-IH .. HIHI-MIIH--II-1001-IOOI .. IIoot••-··-·"" .. •l---·--.. it .. t __ .. ol•l 

Component Number Retention Area External Units 

0 0.00 0.00 

Area 

661.40 

122.30 

229.45. 

213: 

External 

N/A 

N/A 

N/A 
Conditions Dal-Italia 7 Scrubber Exhaust 

Run #2 Imps 3 & 4 

Component 

(unknown) 

(unknown} 

(unknown) 

: Volume 250 Dilution 1/1 

Date 11/08/2006 

Time 13=49:17 

-25.600mV 256.000mV 

Retention 

0 .alrr~·---l===-=~----------·----·--------------------·-·1 

;'il'r 

~ lj 

·'I :·:·, 

~: 83~ -- : :1~;::::~:·--------···-

4 ·-..... 

L 

I 

1 ....................... : ............................................ ,_, ................................................ -: ......................................................................... : ...................................................................... . 

Component Number Retention Area External Units 

0 0.00 

Area External 

550.15 N/A 

125.55 H N/A 

210.85 N/A 

214· 
Conditions Dal-Italia, Scrubber Exhaust 

Run #2 Imps 3 & 4 

Component 

( unkno~m) 

(unknown) 

( unkno~m) 

Date 

Time 

vo.lume 250 Dilution 1/1 

11/08/2006 

13:51=43 

-2S.600mV 256wOOOmV 

Retention . ~rea 

1 

...................... ;~~"''''"''"''"'"'"""''"""''"''"''"'"''"''"""''""'"'"'""'""'"'"''""'"'"'"'''"'"'"'"''""'"'"'""'"'"'"''"'''""'""'"''"'"''"'"'"''"''"""''"""'''"""''""'"'"'"'"'"""'"'"'"'"'"''"'"'""1 

l!' I 'I . 

0 . 8161 lL .......................................................................... ~....... I 617 . 50 1 ........ :·~ ....................................................................................... r.JUIOIIIII'II::IIII' I I ;:i . 

• ·1. : ·::, I 

1 ' S16 : ::~:::::::::::~'!:IIIIIIICIICIIItiUIII' 12 6 ' 85 

2 • 21·--· ................................... ::,, II ,.,. I I : t::::::::=-.:.~:.. I 196 . 80 

3 ........ 

4j ........ 

s ......... 

6 

. .• ............. _._ .................... _ ........ -.................... _ ........................... _ ....... _. __ .. ,_ .................................... -........................... __ ._, ..... --.... _ ......... ____ ...... _ ... __ ... _ .... _ .... -..... . 

Component Number Retention Area External Units 

0 0.00 0.00 

215 

External 

N/A 

N/A 

N/~ 
Conditions Dal-Italia, Scrubber Exhaust 

: Run #3 Imps 3 & 4 

Volume 250 Dilution 1/1 

Date 11/08/2006 

Time 14:10=18 

-25.600mV 256.000mV 

Component Retention I"''''''"'''''''''''''"~'''''""""""'"''""''"''"'"""'"'''""''"'"'""'"'"'"''"""''"'"""'"'"'""''""'""'""''"''""'"'"'W''""''"'"''"''"'"""''"''''"''"'"''"'"''"''''""""'"""'""''""'"'"'"''"'""''"""'"'"''"""I 

1 . f · I 

(unknown) 

(unknown) 

(unknown) 

0 • 83 ~ -·-·- 1.:;.;:=~--=:;::::=====,==···""~'""' 

·'I ·'' 

i : \ 

~ : 8 6 ~I...... ~ ;~~~~~~~~~;;~~;;;;;;;;;~~;,:,,.,;. 

'3 ........ 

I 

I 

41""'"" 

5 ....... 

6 ........ . . 

. . ll .. l•tlo•IOOooo .. IIOOIII••I .. I•UOoii-OOOIO•IOooOO .. Oiolo .. IOoOI .. OiotiiOio•II•II ... II .. IIOOINIMOoolooOoo .. OOooiiNiotoo-IIOIIoiiOOioOOOIIOOIIOIOOIIHIIIOOIIMIIIIIMIIOIIOOII'IO .. OitootooloOOioOOIOUIIItloiiiiOOIIOIIOoltOIIOtloiiOOIOOINittiiOOMIOtO .. I .. IO .. I .. IOIIHOotloo .. OooOoot 

Component Number Retention Area External Units 

0 0.00 0.00 

I 

I 

I 

Area External 

552.00 N/A 

110.50 M N/A 

211.40 N/A 

216 
Conditions bal-Italia, Scrubber Exhaust 

Run #3 Imps 3 & 4 

Component 

(unknown) 

(unknown) 

(unknown) 

Date 

Time 

Volume 250 Dilution 1/1 

11/08/2006 

14:12:56 

-25.600mV 256.000mV 

Retention . Area "''"'''''"''''"'''"''"jl::••••••••n••••••••••~••••"'''"""''"'"''"'"'""""''""""""'~'""''"'""'"''"'"''"''"'""'"""'"'"""'"'"'"'''"'"'"'"'"''"'"'""'"'"''"'"'"'"''"""'"'"''"''"''"''"'""''"""""'''"'"''"'..;""''"''""''"'"""''l .~~~ ! il:;. . . I ;j:' . 

0 8331 ;,"""·;·-:u·,.. . • I • u ................................ , ........................ mll 11 nuu-u • • 634.60 1 hll~oU~ : "o .llltllt"'I"IIIUIO~oll .. lhiUotUoUoUIU ... IootnMUtn• u n 1 • UUU,tEU 

: r·l ..... 

I ~ ·;~!i: 1 • 8 6 6 ......... : /::::::::::::::::::mmm:mu• 114 , 15 

2 ~ 21 : :;::::;:;;;;:::::::::::::::::::::::::::::::~:::nn• 21 0 , 0 0 

3 ......... 

J_ ... I l 

j .. I s, ........ 

I 

6 ......... 

i 

i ........ ; ............. ~.: ....................................................................................................................................................................... '"'"'"''"""'"""'"''"''"'"""'"'"''': .................................... . 

Component Number Retention Area External Units 

0 0.00 

21.7 

External 

N/A 

N/A 

N/A 
Document No. 034184-25 

Dione x Corootallon 

:228 ·:-ilan Wat · 

c. 607 3003 

.~rnyvale. CA 

l~!ie-3503 

•::CSl 737 ·0700 

Dioncx U.S. Replonol Olllcus 

Sunn)'\'ale. CA (405) 737-0522 · 

Wr.strnrot. t {63G) 789·3650 

Hoosioo. 1X (281) 847·5652 

ld<n:t. Gl. {770) <U.SIOO 

., • .ar~oo.ll.! (856)593-00JO 

5.11• l2ke Ctt. UT 180il ~72-~:>92 

. ·.·. 

20 May 1998 

Dian ex International Subsidiaries 

Avslria(01)Gi65125 · ·G=rmanr(OG12!i)991-0 

8!1pium(03)~3<294 111~(00)1j(j51 5052 

C.wd.l (005) 8~~-*50 J.!,?lil 105) 6885-1213 

Ct.~7i! (552j 2~28 3282 I:Utl {2) 2ii53-25SO 

DtnmJ;J. ((5) :;s 36 ro ~ 1~ Htt.'lttWtas (0161) <3 .o 03 

Fra::a!Oil3; 300110 S~i'sltm'![)J212C5 ~ £0 

., ...... . : . 

.··· ·,;, 

·.· · .. · 

. - ~ -~- , .. : 

· .. • . . . · -· 

226 

. ~\one.t 

~'?.F .'~% 

~~:~;.H ... W~D 

lFN 03131e·0310M ~ 

0 l'00-1 01met Co:o:.r.l3· 
The· prep_aration and analyses of the Flu~)fide _S~andard was performe~ _wi.th extreme care by 

DIONEX Corpora_tion Co'nsumables Manufacturing Department. 

Document No. 034 1 83-1 8 1 3-Dec-02 

1cnex Corporation 

:l'a i nan I\ av 

j Box SGJ3. 

mny1'ale. CA 

OS6·3!l03 

~: 737·07~ 

Dicnu u.s. Regional Dlflces 

S~'MJ"Viile. CJ.. (4CS) i37-E52i 

\l.'tstrron:. ll (630) 7SS·3~60 

HM!on. TX (281)5<7·5652 

Al!an:a Gl. 1770)43Z·81CO 

Morllro. tlJ 1855) !i%-0500 c-"'"'w."""""· ,,. fM1\t\ .. ., n"Xl"' 

Dionex lnlematioaal Subsidiaries 

A~-stri.T(Ot) 516 51 ZS Gtvliol1Ji'(l)3i26) 991-V 

8elp!U171(C3)353429< 1!~1}'(05)6551 5-J52 

Canad8(9C!i) 644·9550 Japan (06) rees, 1213 

Chm.r(652) 2<28 3282 YM.t(2) 2653-2590 

Oe;lmzrf.(4!i) 35 3? 90 SO Tflef.Jt.'hlrlznds(Ot61) 43 4303 r,...,,.,.tn".,., ~n n1 11\ t\...:.-;v•·~Afl'\f.")t ?tv.~ r.::. 

227 

LPtiC31318·0310M 3/0-4 

\0 ?me Oim-t r.l'rr«;>!i'n 
i k\(l .._; l 11 0 ~\1 \._~ \:~~vI H 0 '" lVI E.l~·T A 1:-' l N-C : . . r. _! . • 

PHONE.NOP (214)'631~0021 

7715 Sovereign Row FAX NO. ( 214). 905.:-0~34 . . . 

DALLA-S, TX 7524·7··.··. ·cHAIN OF CUSTODY ~ECORD 

r Nar~1o of Unit oncJ A~dross: 

vt 

Sumplo Dnln Tlmo 

._ V1 

0 '- '- QJ 

QJ .s 

.0 "' E.c' 

Tay NumberS' no marks 

Hvmbor Snrnplod Spmplod Ooscriplion ol S<tmplos ::l Q 

zo 

·---•-. ----------·---.- --·- --··------

10(3,D ----.~.G-l_· ·~___:;_~~r·.__;_&t_,.r_l~::,_l_JE.._:__r __ ~_, __ , f_t_r;~_tJ._'f_l_· ·~-~·-· -·- __ .. __ , __ _ I 

10/?o .·~ t·l (l1- GP/J tt I t<. ---- --- 1--'----1--------·-·--·------------

3 lO{:O •r ((?J ~p,o 'I J j . ·--- -·---- ----------------1 

4 ~~~--~---•---~-~-~-·~A-~_~_A_L I olio ____ /_,~~~4{_~------ ~ ~-. r l0/3o 

-- _I_ f-~J"v ~~ Ci I _L_ __ : ___ __ __:_1_Uo_Le_· 4._.k----n=(/::..._;;;<-~_, 

fo ,o(?o ----

'7 fo(;o_ --~--

_t_,,__;__ ________ ,_. /L? ~,:) iftJ!.!_·£_ __ .---. - fJp ~~c_ 

·--·...:.....------...~~--~---.---- --· A.ei>.-e.f;U i _.·. "_. ~-- __ No u~-~--- ·~ Jo6o 

1 _!!/!!_o_ 

. 10' to/'-'D 

lJJ-() , . I .. {(1 j;ttA~ £/)j't( ~ /J1> ~k· e._ ---------·---·---- ----~---... . ---· ---- ·-· --- ·- (}-----

, __ , ____ ._1 ------. I. /l2- .1wtf? E.PJU'ft ~ ---· ·-·- IJo ~ c - .. I .. fl3 ~~·[fA; q( . r; /lJo ~~ 

- ··-. ---~ ------·--·--·------- -·---- -·· -·---·- --· ----- ·----· .:---

y: (~ius · uu · 1\ulinquishcd by: (Signt~turu) D«llo limo . Rocoivod by: (Siur turo) 

II 

O.ato limo 

n/q 8:0 

Datu · flolirlqui~ht:d by: (Siunaturo) . ()a lu limo 

.__n_ol....,..ih-qu-is-hO<_J_by_I_S_i 9._,a_'"'_o_) ___ L.__o_"_'o~~l-imo n.~ lor.t~b.;;;;;;;y;;;.~·,siu.l-. . n.:--r- 1:;;;;- . ·-n(-!(1-,a-,~~,-s ----------·-------··-------.-

Distribution: Oliuinall\ccompanics Shipnwnl 

Copy·lo ClionVProjcc;t Cooulin<1lor ·"···---------·· ............... _ .......... _ ...... _ ---"'-. ·--··- ...... -·--·--......... --·' 
~r~wl-,:; -~ r1 0 ~"~ ~1 \: a\t \1; H 0 '\11V1_ E.l\l·T A~~ l N-C ;o. 

7715 Sovereign How .... -··· ... 

DALLJtS, TX 7524·7··.··. ·cHAIN OF CU~TODY RECORD 

PHONE NO .. (214)'631--:0021. 

FAX NO- ( 214). 905.:-0f;}3-4 .. 

~~--------------------------------------------r-~-,1-----------------------r------- l Ha~10 of Unil nntl Add1oss: ...... 

S11mpto Dolo Timo 

1-iurnbor Somplod Sprnplod 

·--~-·---------------------------

Dos.crir;lion ol Samplos 

- Vl 0 .... ... (1) 

rp .s 

.0"' 

E '-• .c :J 0 

zu 

l ng Numbct s nomatks 

t 1 l

0 /3o 1-1-~o fl.z,l) f!J/&,~'~L _t_ ____ · .--- __ ·-·--~/J_o_~"-LJ_:f_ __ _ I -----1-----1-~------------------·----~~t-----1 

--~ ~- to~___ t1e.-C t (. 1 · <4 tht.{( t;JfAJlil_ L ___ ·-. ____ No ~k-'ci e. 

t3 /.1>~1() 

i£1 ,o·f?o -- t'5" lD/?JD 

ll ,~ 11~( ~ :!_!__ -~ ~- _ _ _ __ /Jo LeQ 14-r L ·---------·-------- . v 

I(._ ~3 MeLt EIJJ'-~~ 'r ______ , _ _,· (V~ ~ . ~rl.d~ e.. 

I I ,_.- 1AJed J~V\L ( ___ ~- _... _ _ M ~~'-{.L Jc_ 

Oolo 

Dalo limo 

Oisttihulion: Ori~Jinnl Accompanios Shipmcnl· 

Copy·lo Clionl/Projcd Coor din<tlor 

·-----------· -· -- flulint1uishod by·. (Signaluro) Dnlu Rocoivot.l by: (Sionnturo) 

· nulinqui!-11(:<.1 hy: (Siun~turo) _ 0:110 limo 

·--------··-------..--· 

--·--·--·------· .......... --·. --·· -· . -. -·-····----·--· .,. ______ ·---- ---- ----··--·---
7715 _ soverei~11 Row 

DALLAS, TX 7524·7°00•

0 CHAIN OF CUSTODY R~CORD 

PHONE NO~ {214)'631-0021° 

FAX NQ_ ( 214) 905.:......0634 

l Naino ollJnil om.l A9d•oss: ---.-----

Snmplo Onlo limo OoscriJ;lion of Sarnplos 

...... 0 "' ... ... Ql 

cv.S 

00 nJ r: ~· \::.C 

::l 0 zo 

lag Numbots llom<uks 

HurniJor Somploo S;unplod 

1---1·---------------~ -o ---- -~-------r" 

~ l 1~- --t---'---=G'---'-' f_~c.--'75_____.__f_; f?e_,_ .......... , c_J:_L fy...;._~v-0 -:t--' · _,··R-3 · {.f/ll LID . _'f-. ·-· ___________ 0 

-~~ t'b/!,o --l---t;-~>J.=a__;;....'~..A-o.....Z:..fl_\.e... ____ ~_: 1 -~ ILt Pw ~PIJ ~o_ £ 0 ______ _ !'J_tJ~i~_4.-_k-_~""-L ______ , 

7-3 Jo/3tO __ 1 ______ ,_' _______ ___ I __ P-1-_Pw _6p,u Ero _Y · ______ /\J~ Le~~.J~.4,c;bL __ _ 

______________ ,__:_ 1 __ I f2-~ Pw £PPJi.fo ----- Y -·-_,__:,_ IJ~ ____ l-~L4-J= 0....1J-_..__ 

~ ___ , 

]..;'{ JD/7D --- ' I 

, ____ _...;;1-=--f-~~=------ ._{_ /{/ ~fb_§P}.)_'t-o OK_ _0 

0 

_ ~~- ~ _ ftJo ~~ e._ 

l I 'l 

0 

flz, ~fY\{>5 EIIJ l'-o . )C /V 8 L~k 0 <-- 1--------~-------- --0 0---- ----·----- J-

'2,~ ~ u, Jo/io 

~-1--1--1-'-----''------. -· __:__. ~ Jrt(J:.> !l'N '-ID ~ _

0

: 0 ~- __ __ _ N/) Lec.;_f:_~ c.. -;,7 Jo/3v 

·~g to[3oo Me-C\ ______ ---·-' _ gt_He.c! ~A!-~.-~ _0 __ • 

0

- ____ ~ ___ W __~d=...., _ 

29! !_fJ_/3_o _0__ __ '

1 0 

'· P-02../vk{t GPAJCfo !:_, ____ 0 __ _ iJo Le~_L. __ 1 

?D 0 /o(~_ 11 . 12.3 ° Jl1eCi li{flJ '-ID 7° ~ L.Pa-)"cf-e_~;__-- nuooivod IJy: (Sionaluro) 

1-...,...-----o-o __ _ 

nocoivod by: (Siunaturu) 

nolihqoishod hy: (-S-ig-n;_,·~-J-,(~J)~~~~~.------l)~a-1-o~--- -_Tin-lO- llocoivcd IOI.I.oi;;;;-;;k,,~y: (S-ig) . --o;~-~[[;;,_-,0_-_~·-n(!_ll_lil-1!1.-s. ------------------------o-o------,.-· 

l\:) 

w 

0 

Oistrihulion: Oriuinal Accompnnios Shipment· 

Copy to ClionVProjecl Coordin<•lor 
7715 Sovereign Ho,.., ~ + • • • 

DALLA.S, TX 7524·7··.··. CHAIN OF CUSTODY RECORD 

I Namo ol Unit nnd A~d1~ss: ·-----·---. -·------·------- ·.:.,· 

Tng l-lumbcrs 

Srimplo Dolo Timo 

1

_U_,u_rnb_o_r _ 1 Snrnpl~ St~mplod OoscriJ;Iion of Samplos 

PHONE NO~ (214)'631-0021. 

FAX NO~ ( 214) 905.:.....0634 . 

Homarks 

·----------·-

'11 _lo_t?_.J> _____ c;;:_:_·.(_>c_~_G._e,_(_f -----..~.•--•(2.~~(! &P1Vjt:. . .C._. ______ , __ 2_· o_b_,_~:%rrttS 

_3_~ lv/3$ __ 1 f __ _I _,_P-3_~_6-_e-,---PN_.?b ____ _ >t-. ·-_____ , __ cz.bf, hdrn-,~ 

·_LjL!E_{p_{___ &/c..s5 P.lber 'P/fe~---···-~-· ~tf ~PN '$b _._._'1-_________ _ 

_ /lf ~·-__ , ____ ·'_1 ________ J?.S"f.,ff'J 3/o· ____ Y _____ , ____ .:---! 

'f~ to/3, '' t £b &PAJ 3" 'f 1----r---1---·----------·-------· ·-----·------------·--- -·-~--------

'tt, ~·•--•----=--~-4o_· _pl..e-......:...~------- __ £_· . {}:+Pw BPI{)3k __ ·-. __ ·-. ·- /Jo k._(cer~ . 

4:7 · to/3t , __ ,..;_ ___ -.-L_I ---~--1_.((5Pu6PtV3k --~------ Po Uc,JkJ-c:_ _ 

-1-~- to/"~ I __ ______ I I ______ : __ !__ __ P._· b!_~---~-~ ~----3 f=_ ___ . __ ·- _·- __ No-~-· <. 

,--.-->Lf-J..Cz_ 1J!k ____ Hl- 0 ___ · _

1 _ ~'t T""if> G/Pt;, .-______ ·- /!Jo ~ ~ 

·-·-:-~-D __ ,::::::;;oolo_{...::;3l 

11 

···· -,--~ ~· ~~-~fitJ?Jb- ·--,·,.~-10 -- --T,.,-,,-u. n/Ju~~~o·' by.· Lec.(S•'•J·n ..a{~,)cf ~ ·--\-,t---- 1l71;Cb. ;·;; •-~r:.__--~ . .,--. ..... -+-_,_- 11u:•_isl-•cd~-:;u•:•_o) ___ , ___ .. --·-· ___ ,_...,..... .... "_'~_" __ ,____ "Sf ___ _ 2to _ limo nulir\qui!;h(:d by: (Siun~l\llo) Datu limo nueoivod by: (SiomllllrcJ) 

Oislrihution: Oriuin<tl Ac:comp<tnios Shipmnnl 

Copy·lo Clioni/Projccl Coordinator 
I ow a·,) l K n U ~\\ \..l 1:: K~ Vi N 0 1\\ IVl E: l'!·T A 1:-' I l\I.C ,... .! . 

7715 Sovereig-n How "" . . .. .. ~ .. . . 

DALLA.S, TX 7524·7··.·. CHAIN OF .CUSTODY ~ECORD 

I Narno ol Unil ond /\~dross: 

Tag Numbors 

Somplo Onln Timu 

t~umoor Somploo S~mplod 

·--~-·-------------------------------

Doscrif)lion ol Samplos 

rlt!linquishcd by: (SigntJIUIO) 

Pl\ONE NO~ (214)'631~0021 

FAX NO. ( 214) 905.:......0634 . 

Hom,uks 

Datu limo . Rocoivod by: lSionahuo) 

·--~---~~;_-+_,__ __ -------·--------·--·--·--· --1-....,..-----· 

Ootu nulirtqui!>ht.'t.l hy: (Sign~luru) ();,lu . Tirno noeoivo<.l by: (Siunai\IICI) 

t.p,.;~---------·L..--0-a-lo_-_. limo . 11.;~<~-;;bo;;;<.,,y by: {Siy I - _ l)u~-~L- limo- _. flommks- ----------•---------·---·--·-·-r--· 

w 

w 

Oishibution: Oriuinal Accornpanios Shipment 

Copy·lo Clion\/Projccl Cooulino.1lor ....... -· ........ --~ .. ----- _____ ....; _____ --·----··-·---- ~- ··-· ··-·----
~ awa·'") l a aU v"' ~-i (;. M~ V H N 01\\ lVI E:.l\lT A 1:-, IN-C . ~ 

PHONE NO~ (214)'631-0021 

FAX NO. { 214) 905.:..-0634 . 77~~'? Soverei~n.o Ho\.f 

DALLA-S, TX 7524·7·0 •• 

0 CHAIN OF CUSTODY RECORD 

I Na~1o ol Unit on<.l A~<.lross: 

Snmplo Onlo Timo 

HtJmhor SnmploJ S\lmplod 1---.,.----

00~0 

Doscrir;lion of Samplos 

- 111 0 ... .... QJ 

IJl OS 

oO 1\l 

E oJ• 

oC 

::J 0 zu 

Ttlg Hurnbors llomarks 

~ f t~ {? t 4ce,-1ra r'- L· Rt i>v §PJJ ; s- '(- 0 /Jo {,~c_(CLg .e_ . I ------1-~---------0--~-1---1-·- -~·-o- --- 0- f;J 

·_6_, 2,_ ~ __ __ lt l 2. Pw GPtJ 3J- 1- 1.;{) u.c}...g <-

,_b '-r~ __ ,___ 

1

1 _____ R-~ Pv diru :C f -= = ~ = _/u_o __ ~_I<-4_(£L.L.-e_- '--;--b_~_, __ co{_;f 0

, __ ,

0 __ __::....{~_"2:-_ 0 o_·_____ t Rl_5~~ e/1J3 _..1:_ ______ 1 __ /J.-=--e_/.J?._·~-~--t;;~;iC-<-_-_ 

[g( to/31- 11 __ ,_· _(<23Pt{J58fN3~_Y: __ o ____ __._N....:,....oo.;;.___~_~-h---'1/:~··_c:.... __ , 

·-rz: _1o/'_' ·.~-=-~-·.--- tt ____ ,_-_ fL>rA>&[PN'% f -_ _ ___ _ _ No L12-a..l"a:~ 0 • 

b.7 to{3r _, __ ,...:.._ __ fvl_(:!__._a __ L_\ ______ _..:..__..---0 _.1_0 _.Rt ~ld.l (JPIJ 5~ '!_0

_

0

' . <-___ 0 __ _l}_~ ~ _._ 

bY to{3 f II-------·---·-- ~~~~-· ~2 1Aeto_,_el1_~~b_o _'f. 0 _ __ 0

- 0 _ __ /Jo L,e~--~----

_b_?_~o{_31 ________ ll _______ o_J_0

_

0

(2,3 Mt2-CI e.{JIJ3'f> otL--_______ 0

_ jJD ~l-.:C}e_ 

.-f,-~_{}_c~ .. __ G_'l!,,_( _ I {L\ 

0

* 6PN35 ° ~ 2o7 .. 4 _ _,_. 

Rucoivod uy: (Siunnluro) rlulinquishcd by: (Signilturu} Dalo 

----·----------------------0 ----t-~---·-·-0·----

Daln noeoivod by: (SiomtlliiO) 

---------1----

nulihq:Jishod by: (Signaturn) Oalo limo 

1'\:) ~,~~~----------------L-----~ 

~ Oistrihtrlion: Ori9in<tl Accompanios Shipment 

Copy to Clioni/Projcc;t Coordirwlor 

nofir\quislu.:d by: (Sign~turu) Oalu Tilllo 

-·-·--------·-·-· ··- ······ .... -····· ·-···-···------------------.. -- ______ _... .. - ----
LfKVI-31 Ki 0 ~\ll1 t. N \II R 0 N ME N·T A~' I N.C ·. . . ,'! :' . . : 

7715. soverei.~n Row 

PHONE NOP (214)'631-0021. 

FAX NO. ( 214 )· 905.:--063-4 -

. DALLA-S, TX 7524·7··.·. ·cHAIN OF CUSTODY RECORD 

I t·laino ol Unit ond Asfdr~ss: ·..:..· 

-......~---·-, 

Snmplo Dolo Timo 

Hvmbor Ooscription ol Samplos 

-~-----------·---------------

- VI 0 .... .... Ill 

-~ -~ ,: ·~· ~.;;;.c 

:i3 

T ng ~hunbcrs, 

Analy 

Somplod SiJmplod . , '__;,___;__,, _________________ , -. ---- __________ ,. __ -.-r-·- --. 

~I t0/11 

l 

. ~ z,., ID/31 

~~ Hf1-

7'7 ".,.,_ \ I 1. 

- I 

75' 11/t- I l 

.,/o ,, 2- It l .. -----------------------· I ., It (1- I 

~~ 11/l-

,.;......__ _____ ,__, __ __;_______,. __ , __ ,---·Ill Imf~¥1 e/IJ"; --(,'f. -- - - 0,/ tJ IJ&o\or+-

ll ---- ~~ It {-z.,. I I 

.=~o u/~ 't 

llomatks 

Ln_o~:~:~~-sl_'~-~-:-(S_~_"_~_"'_o_} __ ~:-O~n~to:_-:_T~~-_'o~~~~l~o-ro:i_v-c-U~I-o_r-._L~~~o-,_a~~~~Y~b~y:~(S~~~-l~---0-~---[-~_o_--_.-~-!,,-,a-,k-s·---------------~ .... _ 

:..u 

C.Jl 

Distribution: O•i9in;:1l Accompanies Shipment 
I a w a- '-..., l i n U v 'A ~~ t:. M ~ V i M 0 I~ 1\fl l:. 1\\· T A ~ , I N · C PHONE NOr (214)'63"1~002.1 

7715 SC?verei_~n FAX NO. ( 214) 905.:.....0634 . __ How 

DALLt\.S, TX 7524·7··.··. 

r. 

CHAIN OF CUSTODY RECORD 

~~-----------------------------------------------.----·------

1 Narno of Unit nncJ Asf_dross: 

Oos_crip\ion of Samplos S~mplo Dolo limo 

Numbor Snmplod Sprnplod 

'S I u{?_ S':/l /'. ,. • , ca~ c:re, 

·I ----- -gz_ 11/7_. 11 ---- ---

~J '''7~ II 

- Vl 0 '- .... Q) 

qJ .s 

.0"' 

E.c' 

::J Q zu 

lng Numbers 

~ ·-. --- -~-------,-- -

"{ -.. 

~I '5~ efAJ 2.G 'f 

"' --·----

r l {Lz_5{r- ~PM z.q 'f· --·-· -· --

Homarks 

----- --, __ 1_o_fc c7 J=rtl'\S 

-· - --- z; 2. b 2_111.s __ 

______ , _____ , ______ , ___ __ ;. 

_2-ll.n __J:_fM--=S::::...-__ , 

8 '{ 1t"( 1- &l Ct.~s-. f,'h,,. ... P lfe.r R,Lf ePA12.&; --r-- . __ , ___________ ....:_ ________________ --------------- ---1--------:...----1 

1/ 't { l!.b:_, __ , __ _ ~~ G"PIV z. '1 ---________ , __ ---·-- __,.- ----------

g~ n/-z- . , fl,b 6(JAJ ~, 'f , ____ , ___________ __;__ _________ --- --- ·--- - -1--------------1 

I (1.'1 fA.J .bPiV 2..'j -~. <- /Je l.ec.../c..:r L ___ ,..:..._ ____________ _.:...... ___ -· --- ----- --·--· - -- ·----- "(j-

. ' ) P-s- ftU e{>IJ 2-'1 'Y IJ 0 ~~, (!.__ 

---------------- ------· -----··-----..-----· ---· - -- ·-· - - ------·--fr 

, __ , _____ u________ · _

1 

_· ~ _tlb P"' [PAJ 2,q __ 1- __ __ __ __ No ~G.lc:.{i~ 

Jfz_.,D '· P.tt ~tf.} CPIJ 2.7 . )<' IJ'() ~~~C-. .----· ··---- -···-·· ---· ···--------·-·----- --·--·· --- <T-----'--

·-+1-----· /;;;~ ;~ ;,0 I--"'---J--~~ Dnlu limo Aocoivod lty: (Sionalur--o) __ _ 

Dolo rloeoivod by: (Siumlluro) 

floli\WfJishod by: {Signiii\JIO) DtJlO Tirno ~--·-----·--· ____ 

l ________ --· -------------------.. -· 

lloroivolllor. Labornlory bv: (~ig.) . Do~~ ---~~~ llnnrorks . · 

--------1:----~- --

Oislrihulion: Ori9innl Accornpimios Shiprnonl· 

Copy·to Clionl/Projec:t Coordinator -------·--·-·-··. - ......... -··· ....... ·----··--·------.. ··--------·-----·--·-···-----
-f~vt51 KiONG t.NVIRONMENTA~, ,IN-C,; PHONE NO .. (214)'631~002"\ 

7715 Sovereign Row FAX NO. ( 214 )- 905.:......0~3-4 .. 0 ·• • • •• •• 

... DALLt\.S, TX 7524·7··.··. ·cHAIN OF .CUST-ODY ~ECORD 

I t·la~Hl of Unit nnd J\~<.Jross: ·.~-

; 

Srimplo Onlo Timo 

- lf1 0 .... lag Numbers 

E.c' · 

Hom arks 

-~-~. - A 

Doscrir)tion of Sarnplos ;:, 0 · 

t---.----t---~~~~-1-----------------------------~l·~z __ o_ ---------------~ Humbor Snmplod S~mplod 

•! 

tit ti/?- . I -

·"92., u/~ ! 

/JD &4./Lif-e__ _ 

~'S'"f.' {fAJ2q 1__ __ --- _,___...!.A9_:_0=----·Le_· -~"_k..pc.~;:.__e. __ , :. 

1 

_____ H ________ , ....... _,_I :__~PJ; J:.r.f/7 iPN ':__ _f. -· ________ _ 

I 

<13 tt/z_ /J.'I Jl!1eLI t{jJJ~7 ~ _ _ __ _ __ /JtJ ~{L~ ~ ---1--------------------------------- Me,L( ,. 

'?I{ 11/1- . -

___ , __ ' ___ ._·

11 ______ ,_

1

_,fl<J lvld'l t.fAJl-7_ ;c - - ---- ~ ~e_ 

~{ u/"L. 1---·---__ , ___ , __ '' _______ ·-' - fl_b __ I1£L_._, ~_fN_?9- __ f ---·--- - _,__:..IJ-,-f) __ &.G_· ~--

... 1_~ JLL1-__ , ___ , ____________ G-r-1 _;..._ _________ ·--- __ Y. --.- -. - ___ UJ_~ 

7.7 

! 

11/?- 1--1..;__ ___ £_-1.------..:_-..---1--'--_. _fl..$"_~_i:r._~_P_IJ __ 'l,c_1 __ f.~---- _, ____ -u;_6_, 2:_~~-

t---:---t----'-~•---•---------'--' __________ ~~--- _flb __ ~ ___ 6_"P~~ •. _ ~ _ ___ __ _ -zo_ 7. ·7 ~rl'l15 

___ , ___ , ___ tJ_,I_IJ_I_~.z-S_ .. 6_.c..;_ .. ___ , __ · r_· _ flt ~ 1~--~~f'T; _ :t_ _ __ _ Mv __ Le~f,ye_._ 

01 11/'J-

?J.tJ tt(';J . ' 

too· "'" 

nolihc-y.Jishod hy: (Signai\Hn) 

,, .. I .(2:z_-t""'~fl2 ::;a . ·-!__ ____ ·-- /Ja f_p,_b_lf.L- ~-· -

/lh/oG ;~~&. ~---fi;;J;;;q;;i;t.",;;n;y:-~.,;;;- l)nlo Hmo . Aomivod by: (Siunalu<o} 

. -~)illo ~- Tirno )'focoivcd by: (Signalufo} i'l~fulqui~ht'<.l~hy:- (Sig~~luro) . --- --l-)at;-·-·-· Ti~l~-·-nu_,..eo-iv-od--by-: -(S~Jn~;.-,o) ___ _ 

Dalo Tirno 

Oislfibulion: Ori~Jinal Accompanies Shipment· 

Copy·to Clioni/Projcc;t Coordinator 
l n w a ,) l 1 n V v 'A ~1 1::0 K \t V i rl 0 I~ 1\11 £:. 1\1· T A ~ , I l\1. C :: 

7715 ~~ove.1:-eign Row 

DALLAS, TX 7524·7··.·. ·cHAIN OF CUSTODY RECORD 

~o of lJnit ond Ad-dro~s: 

,_ VI 

u ... '- IV 

cp .S 

----- .o ru ---.---- c.: -~· 

S~mplo Onto limo 

Hurnbor SnrnpltXl S;lmplod --.j -----·--

Ooscrir;tion ol Sllrnplos 

Datu Tirno 

~.:.c 

:.l 0 

Z0 

Oislrihulion: Ori~Jinnl Accompnnins Shiprnnnt· 

Copy to CliontJProjcc.l Coordinator 

lag l'lumbc1s 

p It 0 N E N 0 ~ ( 2 1 4) ' 6 :-l. -~ - 0 0 2 l 

FAX NO- ( 214} 905.:-0634 . 

nollltllkS 

-----· --·-~- Dalo Titt\O noeoivod by: (Sion;.Huru) 

---------···· ......... -........ ·- -·····------·-----..-·---------------·--
7715 Sovereign Row 

DALLt\.S, TX 7524·7·· CHAIN OF CUSTODY RECORD 

PHONE NO~ (214),631~0021 

FAX NO- ( 214) 905.:.-0~3-4 .. 

I Namo ollJnil nnd Asf<.lloss: -.--~--,------------·--.---------------r-·---------------- Annlysos r1oquirod 

no marks 

Sn mplo Onlo Timo 

Hur nl>or SnmphxJ Sam plod Doscrir~lion of Sarnplos --·-

.. ~;£ _______ _ 

L-1 tl/]:, t;~/>cc_. G~l' --, ------

z,-v 11/3 1. l 

------------1-----------------------·-·--- -~-- ---------1··---- -- -- - - -----·-----------

--------1---11-------------------------- ----------------- - --

-----1----1----------------------1---- ------------·--·--- ~ - ---.,.-----

------1---1---------------------- -------·----1-· ---- -- ·-- -------------

---:----l---1-----l-'----------------------.,..--l.----- --··-------- --·-------

---------1--------------------·-----

-----· ---- ----------------------.. -~- -----·-·--- . --- -- - --- --------------1 

limo noroivod by: (Sionaluro) 

nolin:hod hy: (SignahJ-1(-J)- __ L--0-n-lu __ .. --1-imo Jlo~cill;(;;bo~~;~::-.. IJa~--[~~~,~--··-n-n_n_Hl-rlo.-s. ----. _..__ __ ·-------------·---.·-··· 

~ 

0 Distribution: Ori9in;.tl 1\ccompanios Shipment 

Copy to Clioni/Projcct Coordinalor .. - .. -· . -... ---····---····-·· -'---·· ---......... -···-· ....... ·····-· _l 
I 

I~ 

~ I . 

: . 

I 

;,I 

.J. 
~ tJ J'l/J 1.1>~~ e.Jv 

PLANT: D 0 rn.te ''" u 

DATE: ;o 73(/ or 

REPETmON: r . . .JI I I l ( 

LOCATION (SOURCE#): EP IV l 

OPERATOR: (Ul 

SAMPLE TRAIN#: "f.. 

METER BOX#: tJ ,-

BAROMETRIC PRESSURE:l ~, J \ 

M1BIENT T.Elvfi>ERATURE: "7 b 

ASSUMED MOISTURE: ( 

PROBE LENGTH: :J ~ 

NOZZLED~TER:·~ /.'j~ .. /11/./7( 

STACK DIAMETER:;,)- ;

1(sf';.,,1

rlt) 

METERH: /. {j(/ 

C FACTOR:. gC{ 

METER CO-EFFICIENT: • 7 7i- ~1ER T ARE:0',.3.6' t{ S'(. # 1.U · 

PRE-TEST LEAK CHE~ 

Metero,o.o7Z-' cu. ft. 1 s-in. HG . 

FIELD DATA 

IMPINGERS 

! 

I 

' t qg'~ 1' 

I I I 

I 0 ~~T 

Initial 

#1 /oJ 

#2 tf!O 

#3 ( tP 

#4 'LdiJ}' 

#5 

#6 

C02· 

II {) 

J

P'' 

POS~-TE!~ LEAK CHE~ 

Me~er. c:>· 1/. cu.ft. @R·~ m .. HG 

Pitots: /./"' · 1 in. H20 ~~~~~~~~ Pitots: V r.. in. H20 

J .)Z 

: o3 

: tf6 

~ :! (3 

~ 

~ 6C 

ve. rt :-~-J- .••:- . 

ur ./7tl 

.3 

J 

) 

241 

z.z ' 

I.Lj 

~J·1·· 

~.~r 

,,, 1-

]., /. -z.., 

;. ~1r 

;J.1,; "1.... 

z.. ~-I 3 Cl., )' 

:J l,. "] 1 
PLANT: {)~ j~'k-< DATE:· JO/J 10 

,. REPETITION: t/ .. ~- J ~) LOCATION (SOURCE#): Gfcv OPERATOR:·~ 

SAl\.1PLE TRAIN #: $ 

METER BOX#: 11 ,--

BAROMETiuC PRESSURE: z._ 7. 'J} 

A1v.1BIENT TBvn>ERA TURE: 70 

ASSU11ED MOISTURE: I 

PROBE LENGTH:3l- ,-

NOZZLE DIAMETER: • /1S 

STACK DIAMETER:~ "l '' 

METERH: /, "(~l 

C FACTOR: , !' '-( 

METER CO-EFFICIENT: I 'i ?'-' 

FTI.,TER TARE: o,j(/~~ 

PRE-TEST LEAK CHECJr_... 

cu.ft. @ . in. HG 

in. H20 

FIELD DATA 

I I '"'1 G . 1.-f (, .tv 

rMPINGERS 

Initial 

#1 { oJ 

#2 ( tfJ 

#3(6> 

#4 ~PYrSt­

#5 u 

#6 

C02· 

0 

J I 

I 
... :· · · · · ···; .:~·~ :::':'-~\J'Tf{~~!'/{:tr·;;~;M:·~~~..,:~~::~~mft>~ij·~?r.x-.,·., .......... ·· · · 

;~~~~%':!!~ / . REPETITION: '3>. ( ( . . tJ ( 

LOCATION (S2QB9-E #): t:ft-1 -, 

OPERATOR: ~\ \ .. · . 

SAMPLE TRAIN#: .. r 

:METERBOX#: If ·,y · _ 

BAROMETRIC PRESSURE: L,1.i}) 

A?v1BIENT TEMPERATURE: 7v . ASSUMED MOISTURE: (. (' 

PROBE LENGTH: 3~'' 

NOZZLE DIAMETER:. /1S 

STACK DIAMETER: o'> 

METERH: /, 46/ 

C FACTOR: , gtw/ 

METER CO-EFFICIENT: , Cf1"2-

FIT..,'fER TARE:-, ~C ~ ~ . PRE-TEST LEAK f: 

Meter: t::J , o ()r eti.ft. · 

Pitots: Y 

.J 

~ 

~C)9-

t 

7 : ,~ 

' 

' . l:t 

I· 

~?_),-

~I 

2. 

.3 

~ 

) 

c 

7 L/) 

~ 

1 , )0 J 

, .. J 

')) ~ s-s-

-z_ 

.. -· . Ave: fC-f:tiCT : 

I/,· 

IMPINGERS 

Initial 

#1 (r.JJ 

#2 /,p; 

.u3 I .J" 

~ l;..""'Y sr 

#5 .' 

#6 

02 

L\ 

POST-TEST LEAK CHECK 

...... ··~ \.4 ·' 

in.HG 

. H2o 

s-

-~ 

:s-
. n 4 !.//le 1/u)lw,r:f PLANT. v /. /i I / 

DATE· /o //0/ CJ /, 

REPETITION: Cvduv-·~ c.A.e~AL "J;/ 

LOCATION (SOURCE#): e:ff'.J c.r I OPERATOR:~ 

SAMPLE TRAIN #: 

METERBOX#: 

BAROMETRIC PRESSURE: 

M181ENT TEMPERATURE: 

ASSUlv.1ED MOISTURE: 

PROBE LENGTH: 

NOZZLE DIAMETER: 

STACK DIAMETER: 

METERH: 

CFACTOR:., ~ 

METER CO-EFFICIENT: 

FILTER TARE: 

PRE-TEST LEAK CHECK 

cu.ft. @ in. HG 

in. H20 

6 

{( 

12_ 

... -. 

"\'C. 

FIELD DATA 

IMPINGERS 

#1 

#2 

#3 

#4 

#5 

#6 

Initial 

POST-TEST LEAK CHECK 

Final 

02 J,l 

cu.ft. @ in. HG 

==~=· in. H2G 
PLANT: Pc...l+t l e_ 

DATE: IS /?~e/e lp 

FIELD DATA 

REPETffiON: ( · 

LOCATION @_QURCE #):Pre-ss B~ko \!) '-e..,(_/3"fiJ Gfo) 

OPERATOR: I ~ I &S 

SAMPLE TRAIN#: t I . ME1ER BOX#; I () 

BAROMETRIC PRESSURE: 2-C, , .3 S 

AMBlENT TEMPERATURE: {:, s-: 

ASSUMED MOISTURE: 2-

PROBE LENGTII: .lff 

NOZZLE DIAMETER: ·, 2'-l73 

STACK DIAM:ETER: '3·CZ''t ( ~ ,$"'1./ AJ}pp( e) 

METERH: b ,q'l..O 

C FACTOR: ,~ 'i 

METER CO-EmCIENT:l) .qq'1 

FIL1ER.TARE: 

PRE-TEST LEAK CHEQ{ 

Meter:6'-DO~cu.ft. I~ in.HG 

v ,.,..,in.H20 

',.Q '}.,. 

I· ·I 

IMPINGERS 

Initial Final 

#1 {00 1/07" 

#2 lDO ro6 

#J tt>o leo 

#4 () \1 # 5 'l,;.&JZ) $o7,3 

#6 ~~,? 

C02· 02 

0 2./ 

POST-TEST LEAK CHECK 

Meter: ~ ·~cu. ft. ?;tO in: HG 

Pitots: ~ :£-in. H20 

1- I· /2451 
PLANT: 17ct (.f. .'l e_ 

DATE: to (?,fJ {c '=' 

FIELD DATA 

REPETITION: )- ( ). 

LOCATION (SOURCE #): p~,s Be..~ t.fo 

OPERATOR:77f, G- ~ S~LE TRAIN#: (J..,. 

~'fER BOX#: II 

BARO{\iETRIC PRESSURE:2..<7. s {" 

MmiENI_ TEMPERATURE: ?o ASSb:ME~MOISTURE: z.· 

PROBE LEN'Grn: ~9 NOZZLED~E~R:4zq73 

STACK DIAMETER'~- -37 .e, 

METERH: /.l!z,O ... C FACTOR: ,9'1 . '·- . 

METER CO-EFFICIENT: 0. r:JsFn.,TER TARE: 

PRE-TEST LEAK CHEC~ 

Meter: (} , C«;. cu.ft. @ IS in. HG 

Pitots: """ · H20 

~03 

I ~ 

,l.fv 

7 ~L~ 

8 : l·~ 

I ,. , ... 

IMPINGERS 

Initial Final 

#I lO~ roy, #2 roo ·Jo'h 

#3. / /00 to~ 

#4 S, , ..

#5 2-o() ,2c,,rf) 

#6 'l--01' 0 

· C02 02 

0 2..( 

!-- j~ /=·2461 
Ave. 

PLANT: rJ~J~·{.\e._ 0A1E: fo(~o o ((:, 

"2. 

FIELD DATA 

REPETITION: ~ ~ ( 

LOCATION (SOURCE#): Pre.-r.; · ... ~._,_r-Io) 

OPERATOR: 'f"A· J G-.5 

SAMPLE TRAIN#: II 

METERBOX#: tO 

BAROMETRIC PRESSURE: z:t. !iJ' 

AMBIENT TE~ERATURE~g ·· 

ASSUMED MOISTURE: /!!:! 

PROBE LENG1H: ltf . NOZZLE DIAMETER: "·VI 71} 

STACK DIAMETER: ~~ 

METER H: ( •

1

1(...0 

CFACTOR: .~c.,( 

METER CO-EFFICIENT: (;),~"\c..{ 

FILTER TARE: 

PRE-TEST LEAK CHECJ( 

Meter: t!>. C DOcu.ft. fb in. HG 

Pitots: ~ H20 

'1 ' 

( 772 .-c) 

774 I "2-

77fo,t..f 

778.7 

,a, 

IMPINGERS 

Initial 

#1 teo 

#2 {CO 

#3 l () 0 

#4 0 

#5 zoo 

#6 

·S2o 

go 

8C 

~0 

,. 

2}·/.b 

24./ 

2'/t; 

252 

2'-f( 

Final 

tCJ t.f 

I o cf> 

{00 

) 

Z-Jz...s-

~5) 

02 

2( 

247 
,1 

/ 

Ave. 

PLANT: D~t.+ ,< ( '€__ 

DATE: 

•.t' 

. : 

REPETITION: · . · 

LOCATION (SOURCE#)fre$~ ~-~aa$( OPERATOR: . tq 

SAN.1PLE TRAIN #: 

:ME1ER BOX #: 

BAROMETRIC PRESSURE: 

AlvffiiENT TE!v.1PERA TURE: 

ASSUlvffiD MOISTURE: 

PROBE LENGTH: 

NOZZLE DIAMETER:/lc.t7), ?..c.tb J. 2.tf{ 

STACKDIAMETER: (_. ZY"13) 

METERH: 

CFACTOR: 

METER CO-EmCIENT: 

FILTER TARE: 

PRE-TEST LEAK CHECK 

cu.ft. @ in. HG 

in. H20 

FIELD DATA ,, .,.,· 

Il\1P1NGERS 

#1 

#2 

#3 

#4 

#5 

#6 

Initial 

(. 6'&0 ~3 ~65") 

C02· 

Final 

POST-TEST LEAK CHECK 

cu.ft. @ . in. HG 

in. H2o 

tJtJ 

2,~ 

~.7 

g,l? 

r~, s 

2.)-,7 

• 

3c,2-

3~.3> 

3&:8 

38.() 
Ave. 

t

,, t1.fLAk.ate,~ FIELD DATA 

PLANT: Da / ll"tA I' J 

DA'IE: II~ REPETmON: I .J/t.y (/J 

LOCATION (SOURCE #):fJ,,_~(/t SL ., 1 

OPERATOR: r(T G-S , i 

SAMPLE TRAIN#: -=f. 

METER BOX#: JD 

BAROMETRIC PRESSURE:)O .. /5 

M1BIENT TElvfPERA TIJM: 

ASSUMED MOISTURE:/ 'I 

PROBE LENGTII: ~ 1 

NOZZLE DIAMETER: C.: 3lj • 31 t ·1' D • ~ IU 

STACK DIAMETER: 7i.SU~' l'l\y"f"c. 

METER H: I, t./ z., l 

c FACTOR: , ~q I 

~~~~~CJENT: .')"!</ (l 

PRE-TEST LEAK CHECK 

~eter:o e,t I cu. ft. @ I> ~n. HG 

P1tots: l In .. H20 

~ 

7 , I)' "t7 

"t 

i : $) 

(D 

: tf;D 

I 

~rl 

IIVIPINGERS 

Initial 

# 1 I ro I tft..)Cl{ 

#iJ.ro 

#3f tP.· ~ ('1().))\-f 

#4/(J::J 

#5 ;tw ct S 6-

#6 

Final 

;tO) 

It~ 

/~. f I 

~6,7 

/2-7,7 
I $1 J t. {1u~lc~J tAJ FIELD DATA 

PLANT: Ou .J ) v' \ 

DATE: . .J (7 L tJ b 

REPETiTI6N: ~ . k v {3"' 

LOCATION (SOURCE#): 5 C..V\u1 " 

OPERATOR: fL.\ 6--5 

SAMPLE TRAIN#: ~ 

:METER BOX #: I{) l 

BAROMETRIC PRESSURE:), () 1 

AMBIENT TE:MPERA:. TURfi iJ ( 

ASSUlvffiD MOISTURE: I 7 

PROBE LENGTH:·~ 1 

NOZZLE DIAMETER: ~3fl'fr STACK DIAMETER: 12·) 

METER H: I, y-1, 

C FACTOR: • ~· "'( . \. 

METER CO-EFFICIENT:~ c;c;· { 

FTI..TER TARE:-

PRE-TEST LEAK CHE<;l{ 

Meter: o .. 0 o Ck.ft. I~ in. HG 

Pitots: ~ ' in. H20 

'-I 

r 

/( :·({3 

\ 

7~{1/"'1 

IMPINGERS 

Initial Final 

#I I t.D 7 L-f.j ~!.! 

#2 l 0.0 

~ {0 #3 1 rrJ ) P-'IA "rf 

#4(cl0 ··2-J2.1b #51:-7~c.r #6 I :So. 6 

C02· 02 

3 !+· 
PLANT: ~ /f(( ( 

DATE:JtX!i': . REPETITION: ~ 

FIELD DATA 

LOCATION (SOURCE#):<;"" c..,..J~!~r 

OPERATOR: ~\G-.) 

SAMPLE TRAIN#:~ 

:METERBOX#:/0 . _ 

BAROMETRIC PRESSURE:3" I(_) 

MvfBIENT TEMPERATURE: s-~ 

ASSU11ED MOISTURE: fl.{,\ 

PROBE LENGTII: 3' 1 . 

NOZZLE DIAMETER: • )l'Z-CJSTACKDIAMETER: ?z.r 

METER H: /, ~l;, 

C FACTOR:,~'-{ 

METER CO-EFFICIENT: • '=1 i L! 

FILTER TARE: 

PRE-TEST LEAK CHECK.-

Meter:O·,OO 0 cu..ft. 5 in. HG 

.. Pitots: . 1, : H20 ~~~~~a=~~~ 

. J ~· 

IMPINGERS 

Initial 

#1 fP 

#i I rJ1) 

#3tuU 

#4l"(J) 

#5 t..O""os (j-

#6 

C02· 

3r: 

POST-TEST LEAK CHECK 

Final " 

l'fL 

1)-=t 

JoY . ( o·t; ··.::i :-~· 

z,t' I 0 

I ;z_,~ 

Meter: o. ooacu.ft. in. HG 

Pitots: v in. H2o 

3-S"", I { 
PLANT: Do.. II L(lf 

DATE: 1//l1-t j 

REPETITION:·...,( 1. y 

LOCATION. (SOURCE #):5 c...~t..l1 u 

OPERATOR: X/7 G S' 

SAMPLE TRAIN#: t( . 

METER BOX #: I o 

BAROMETRIC PRESSURE: 2,.,7, ( l 

AMBIENT TEMPERATURE: ~ 

ASSUMED MOISTURE: ;~, r 

FIELD DATA 

PROBE LENGTH: e- ' ( · 

NOZZLE DIAMETER: 1 ~/}.J .. 3/2 > • 3/2- "3t2-~) 

STACK DIAMETER: 7 "t .5 

METERH: f4"Z..-

C FACTOR: . i '-{ 

METER CO-EFFICIENT: I 91 l 

FILTER TARE:o .)61 L # _5{_) . 

PRE-TEST LEAK CHECK 

Meter: o . 6 °( cu.ft. 1/in. HG 

Pitots: ~ . ''-· in. H20 

., / 'ir I 

IMPINGERS 

Initial 

#.1 ;vv L ;.)1 Jh 0 

#2/ (/~ •..} 

#3 jf.j 

#4--

#5 l- 00(/ s ~ 

#6 0 

Final 

Lol 

I ~b 

te'i 

t ~1,q 

-t zr;. ~ 

02 lr 
Ave. 

PLANT: Q q 1-fd t 

DATE: tljvjo·( 

REPETITION: s-- . I 

LOCATION (SOURCE#): S<...rv~~ :./"" 

OPERATOR: (l--l 

SM-1PLE TRAIN #: I 4--

METER BOX#:/ o 

BAROMETRIC PRESSURE: 3v. f) 

AlvfBIENT TEMPERATURE: 6 o 

ASSU1v.1ED MOISTURE: rl/.) 

PROBE LENGTH: '5 1 

NOZZLE DIAMETER: , 31~3 . 

STACK DIAMETER: 7~· )' 

METERH: /,c{L 

C FACTOR:~ z~( 

METER CO-EFFICIENT: I 9l!L 

FILTERTARE: I 3(t/"L~.#>2>) 

PRE-TEST LEAK CHECK . 

Meter: o · o \ l cu.ft. )in. HG 

Pitots: v 

~ }0 

~, 

r (<;;" 

b 

: l_o 

'; :L) 

lb 

;3a 

lL 

FIELD DATA 

IMPINGERS 

Initial 

#1 I CJO 

#2 I (JO 

#3 ( ;jt) 

#4-

#5 Z. c•o:y S C-

#6 0 

02 

{.J_ 
PLANT: ~ j f/-.:./1 l"-

DATE: ll ;{/> 6 

REPETITION: 6 _ LOCATION (SOURCE#): Sc:. .... .,s~~r c. I,_ 

OPERATOR: )U G-5 

SAlvfPLE 1RAIN #: i \ . 

METER BOX#: [b 

BAROMETRIC PRESSURE: ?:fbo 1\ 

AlvffiiENT TEMPERATURE: 5r 

ASStJ1\.1ED MOIS~: 1'-f '} 

PROBE LENGTH: ~ 

NOZZLE DIAMETER: , 3 12.3·· 

STACK DIAMETER: 1LS ... METERH: /. t.j7..,o 

C FACTOR: . '8' e../ 

METER CO-EFFICIE!iJ':. 7tt'i 

FIL1ER TARE: t j()O:> * ;( . PRE-TEST LEAK CHECK 

Meter: 0 .. 0 ( l. cu.ft. I~ in. HG 

Pitots: "" • '!t in. H20 

/ 

•;;, 

,. 

FIELD DATA 

IMPINGERS 

Initial 

#1 i l.f"J 

#2 ftJv 

#3 f()O 

#4--- /: 

:~uaswFinal 

{<;7 

('{1.-

re ct 

I ~~7,.~7 

t 7-(' 7 

02 

(2 

POST-TEST LEAK CHECK 

=~~ 

in.HG 

in. H2o 

265 
FLOW DATA 

AVE. 

PLANT : f>lr<.~{ ,'l e . 

DATE: lr/1- o£ C/oW ~ RUN#: Cy •1M '- r . rC:.J.Jf--

LOCATION (SOURCE #):~c.-)ef <g~ . 

OPERATOR: tU G-S 

AMBIENT TEMPERATURE: J '} 

BAROMETRIC PRESSURE: 3o,( C02 

ASSUMED MOISTURE: /~ ro v ~ 3 

STACK DIAMETER: 7-Z.S//(/('),!;'fo/ 

C FACT<?R: ., ~t{ 

COMMENTS: 

l 

75~ 1/ 

L 

. J{b li 

f 

t· 

; 

266 
. ~:Append:j:x·· E · 
ter Box & 10 

·ial #: 30272 

Ill! 

APE Armstrong Environmental Inc. 

EPA Method 5 

522 Series Meter Box Calibration 

Pre· Test Orifice Method 

English Meter Box Units, English K' Factor 

Date: -----·-··--·····-> 

Barometric Pressure: ·····---> 

Theoretical Critical Vacuum:-> 

10104/06 

29.43 (in. Hg) 

13.88 (in. Hg) 

,ORTAI\ For valid test results. the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

tQRTAI\ The Critical Orifice Coefficient, K', must be entered in English units, (ft)AJ•(deg R)110.5/((in.Hg)•(min)). 

!!!! 

···-·-·----- DRY GAS METER READINGS ··-···-····· -CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual - Ambient Temperature -

dH Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial 

i20) (min) (cu fl) (cu fl) (cu fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) 

0.24 5.00 107.900 109.503 1.603 77.0 77.0 76.0 76.0 40 0.242 22.0 74.0 

0.50 5.00 109.900 112.185 2.285 76.0 76.0 76.0 76.0 48 0.344 20.5 74.0 

0.92 5.00 115.200 118.265 3.065 76.0 76.0 77.0 76.0 55 0.464 19.0 75.0 

1.50 5.00 118.900 122.823 3.923 77.0 76.0 78.0 76.0 63 0.593 18.0 76.0 

2.90 7.00 123.800 131.329 7.529 78.0 76.0 79.0 76.0 73 0.824 15.0 74.0 

•••••••······································· RESULTS ••••••••••••••••••••••••••••••••• .. •••••••••••••••• 

·RY GAS METER ·-

UME VOLUME 

!RECT CORRECTED 

'll(std) Vm(std) 

{cu fl) (tilers) 

1.552 0.1 

2.216 0.1 

2.974 0.1 

3.809 0.1 

7.328 0.3 

·-···- ORIFICE ---

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMINAL 

Vcr(std)· Vcr(std) Vcr 

(cu ft) (liters) (cu ft) 

1.543 0.1 1.587 

2.191 0.1 2.256 

2.953 0.1 3.040 

3.775 0.1 3.890 

7.344 0.3 7.554 

•• DRY GAS METER •• 

CALIBRATION FACTOR 

y 

Value Varialion 

(number) (number) 

0.994 0.000 

0.989 -0.005 

0.993 -o.001 

0.991 -0.003 

1.002 0.008 

---. ORif.lCE ---

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.372 .().0474 

1.419 -o.001 

1.438 0.018 

1.434 0.014 

1.436 0.016 

Final Average 

(deg F) (deg F) 

74.0 74.0 

75.0 74.5 

74.0 74.5 

74.0 75.0 

74.0 74.0 

Average Y ------> 0.994 1.420 <------Average dH@ 

For Calibration FactorY, the ratio or the reading or the calibration meter to the dry gas meier, 

•cceptable tolerance or individual values from the average is +-D.02. 

I pressure in inches or H20 that equates to 0.75 crm or air 

individual values from the average Is +-0.2. 

Date: /i:J / ~ /6£ 

CONVERSION FACTORS 

1 mm Hg • 0.13330 kPa 

1 em = 0.39370 inch 

1 mm = 0.03937 inch 

1 cu fl = 28.32 liters 

•• Average Temperatures •• 

OGM OGM Ambient 

Outlet Overall Temp 

(deg R) (deg R) (deg R) 

536.5 536.5 534.0 

536.0 536.0 534.5 

536.0 536.3 534.5 

536.0 536.8 535.0 

536.0 537.3 534.0 
Temperature Meter Calibrations 

Meter Box#: 10 

Date: 10/04/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 32 34 32 33 32 32 

Point 2 21'2 213 212 213 212 212 

Point 3 752 753 752 753 752 752 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 492 494 492 .493 492 492 ~ 

Point 2 672 673 672 673 672 672 

Point 3 1212 1213 1212 1213 1212 1212 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0.404858 0 0.20284 0 0 

Point 2 0.148588 0 0.148588 0 0 

Point 3 0.08244 0 0.08244 0 0 

275 
ter Box ll 

rial#: 

!!!! 

10 

30272 

Armstrong Environmental Inc. 

EPA Method 5 

511 Series Meter Box Calibration 

Post-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date: --·----------> 

Barometric Pressure: ·-····-> 

Theoretical Critical Vacuum:···> 

11/06/06 

29.35 (ln. Hg) 

13.84 (in. Hg) 

;,ORT Af\ For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

~RTAI\ The Critical Orifice Coefficient, K', must be entered in English units, (ft)"'3.(deg R)"''.S/(Qn.Hg)*(min)). 

!Ill 

-···--------- DRY GAS METER READINGS - -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:-> 13.84 (in. Hg) 

Volume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual - Ambient Temperature -

dH Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial 

H20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see abovo) (In Hg) (deg F) 

0.91 5.00 460.600 463.630 3.030 67.0 66.0 69.0 67.0 55 0.464 18.0 69.0 

0.91 5.00 464.000 467.023 3.023 68.0 67.0 69.0 68.0 55 0.464 19.0 70.0 

0.91 5.00 467.600 470.637 3.037 69.0 68.0 68.0 68.0 55 0.464 19.0 71.0 

••••••••••••••••••••••••••••••••••••••••••••••• RESULTS .,.. ... ,..,. ............................................. . 

)RY GAS METER ••• -------ORIFICE------

LUME VOLUME VOLUME VOLUME VOLUME 

RRECTI CORRECTED COR RECTI COR RECTI NOMINAL 

/m(std) Vm(std) Vcr(std) Vcr(std) Vcr 

(cu ft) {liters) (cu ft) (liters) (cu ft) 

2.982 0.1 2.960 0.1 3.024 

2.971 0.1 2.956 0.1 3.029 

2.983 0.1 2.954 0.1 3.030 

-· DRY GAS METER -

CALIBRATION FACTOR 

y 

Value Variation 

(number) (number) 

0.993 -0.000 

0.995 0.002 

0.990 ·0.002 

---ORIFICE·--

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.437 -0.0009 

1.438 0.000 

1.438 0.000 

Final Average 

(deg F) (deg F) 

69.0 69.0 

71.0 70.5 

71.0 71.0 

Average Y -------> 0.993 .'·1.438 <-------Average dH@ 

!l: For Calibration FactorY. the ratio of the reading of the calibration meter to the dry gas meter, 

acceptable tolerance of individual values from the average is +·0.02. 

For Orifice Calibration Factor dH@, the orifice differential pressure in,i9ches of H20 that equates to 0.75 cfm of air 

at 68 F and 29.92 i~~~~~--~~~=-~ a;;~table--~er~f i~iduai:.V'Stf;"es from the average is +-0.2. 

SIGNED: '7J:;...--t..~·u;Z.·-·-:--f ~..;:-(~ 

N 

-...] 

CP 

~ 

Dale: ///6:~/ 

DGM 

Outlet 

(deg R) 

526.5 

527.5 

528.0 

CONVERSION FACTORS 

1 mm Hg ~ 0.13330 kPa 

1 em = 0.39370 inch 

1 mm = 0.03937 inch 

1 cu ft = 28.32 liters 

OGM Ambient 

Overall Temp 

(deg R) (deg R) 

527.3 529.0 

528.0 530.5 

528.3 531.0 
Temperature Meter Calibrations 

Meter Box#: 10 

Date: 10/04/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxiliary . 

Point 1 32 32 32 33 32 32 

Point 2 100 100 100 101 100 100 

Point 3 250 250 250 251 250 250 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 492 492 492 493 492 492 

Point 2 560 560 560 561 560 560 

Point 3 710 710 710 711 710 710 

Percent Difference 

Probe Stack Oven Exit :Auxiliary 

Point 1 0 0 0.20284 0 0 

Point 2 0 0 0.178253 0 0 

Point 3 0 0 0.140647 0 0 

277 
!ler Box t 11 

rial#: ·10312 

!!!!! 

Armstrong Environmental Inc. 

EPA Method 5 

522 Series Meter Box Calibration 

Pre-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date:----··------> 

Barometric Pressure: -------> 

Theorelical Critical Vacuum:--> 

10/04/06 

29.46 (in. Hg) 

13.90 (in. Hg) 

:JORTAt-. For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Crillcal Vacuum shown above. 

:JORTAI\ The Critical Orifice Coefficient, K', must be entered in English units, (ft) 113*(deg R)110.5/((in.Hg)•(mln)). 

!!!!! 

--····--·-·--· DRY GAS METER READINGS -·-----·---··· -CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual - Ambient Temperature -

dH Time Initial Final Total Inlet Oullet Inlet Outlet 

H20) (min) (cu fl) (curt) (cu fl) (deg F) (deg F) (deg F) (deg F) 

0.25 7.00 697.600 699.867 2.267 75.0 75.0 75.0 75.0 

0.51 5.00 700.200 702.529 2.329 75.0 75.0 75.0 75.0 

0.94 7.00 702.900 707.282 4.382 75.0 75.0 75.0 75.0 

1.55 7.00 707.700 713.324 5.624 75.0 75.0 76.0 75:0 

3.00 5.00 724.500 730.037 5.537 76.0 75.0 77.0 75.0 

·•• .. ··-··············"'·••••••••••••••••••••••• RESULTS ........................ ••••••••••••••••••••••••••••• 

DRY GAS METER ... -·----- ORIFICE ------- -- DRY GAS METER -

LUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR 

•RRECT CORRECTED CORRECT CORRECT NOMINAL y 

llm(sld) Vrn(std) Vcr(std) Vcr(std) Vcr Value Variation 

(cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 

2.203 0.1 2.163 0.1 2.221 0.982 0.010 

2.265 0.1 2.198 0.1 2.252 0.970 -0.002 

4.266 0.2 4.144 0.2 4.250 0.971 -0.001 

5.481 0.2 5.298 0.2 5.439 0.967 -0.006 

5.411 0.2 5.256 0.2 5.391 0.971 -0.001 

Average Y ----> 0.972 

e: For Calibration Factor Y, the ratio of the reading or the calibration meter to the dry gas meter, 

acceptable tolerance of individual values from the average is +-0.02. 

Serial# Coefficient Vacuum Initial Final Average 

(number) (see abOve) (in Hg) (deg F) (deg F) (deg F) 

40 0.242 23.0 74.0 73.0 73.5 

48 0.344 22.0 73.0 n.o 72.5 

55 0.464 20.5 74.0 n.o 73.0 

63 0.593 19.0 73.0 74.0 73.5 

73 0.824 16.0 73.0 73.0 73.0 

--ORIFICE-----

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.431 -0.0298 

1.443 -0.018 

1.466 0.006 

1.479 0.018 

1.484 0.023 

1.461 <---- Average dH@ 

CONVERSION FACTORS 

1 mm Hg: 0.13330 kPa 

1 em = 0.39370 inch 

1 mm = 0.03937 inch 

1 cu n = 28.32 liters 

-Average Temperatures -

DGM DGM Ambient 

Outlet Overall Temp 

(deg R) (deg R) (deg R) 

535.0 535.0 533.5 

535.0 535.0 532.5 

535.0 535.0 533.0 

535.0 535.3 533.5 

535.0 535.8 533.0 
Temperature Meter Calibrations 

Meter Box#: 11 

Date: 10/04/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 32 32 32 32 32 32 

Point 2 212 213 213 213 213 213 

Point 3 752 753 753 753 753 753 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 492 492 492 492 492 492 

Point 2 672 673 673 673 673 673 

Point 3 1212 1213 1213 1213 1213 1213 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0 0 0 0 0 

Point 2 0.148588 0.148588 0.148588 0.148588 0.148588 

Point 3 0.08244 0.08244 0.08244 0.08244 0.08244 

279 
er Box# 

al#: 

Ill! 

11 

73 

Armstrong Environmental Inc. 

EPA MethodS 

APEX INSTRUMENTS 

511 Series Meter Box Calibration 

Post-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date: ------:> 

Barometric Pressure: ----:> 

Theoretical Critical Vacuum:---> 

11/06/06 

29.35 (in. Hg) 

13.84 (in. Hg) 

ORTAI' For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

ORTAI' The Critical Orifice Coefficient, K', must be entered in English units, (ft)"3.(deg R)"0.5/((ln.Hg)*(min)). 

!!!! 

-------------DRY GAS METER READINGS--------- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:--> 13.84 (in. Hg) 

Volume Volume Volume Initial Temps. Final Temps. Orifice ~ Orifice Actual - Ambient Temperature -

dH Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average 

i20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above} (in Jig) (deg F) (deg F) (deg F) 

0.94 5.00 770.800 773.869 3.069 64.0 64.0 66.0 64.0 

0.94 6.00 775.400 779.092 3.692 66.0 65.0 68.0 66.0 

0.94 5.00 779.300 782.380 3.080 67.0 66.0 68.0 67.0 

•••••••••••••••••••••••••••••••••••••••••••••• RESULTS •••••••••-.••••••••••••••••••••••••••--•••••••••••••• 

>RY GAS METER ---

.UME VOLUME 

~RECT CORRECTED 

m(std) Vm(std) 

(cu ft) (liters) 

3.037 0.1 

3.641 0.1 

3.033 0.1 

-----ORIFICE---

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMINAL 

Vcr(std) Vcr(std) Vcr 

(cu ft) (liters) (cu ft) 

2.963 0.1 3.021 

3.552 0.1 3.629 

2.957 0.1 3.027 

Average Y -------> 

- DRY GAS METERCALIBRATION FACTOR 

y 

Value Variation 

(number) (number) 

0.976 0.000 

0.976 0.000 

0.975 -0.000 

0.975 

!: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, 

acceptable tolerance of individual values from the average is +-0.02. 

t\,j 

00··, 

0 

55 

55 

55 

0.464 18.0 

0.464 18.0 

0.464 18.0 

--ORIFICE--

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (In H20) 

1.489 0.0010 

1.487 -0.000 

1.487 -0.000 

68.0 68.0 68.0 

68.0 70.0 69.0 

70.0 70.0 70.0 

1.488 <-------Average dH@ 

DGM 

Outlet 

(deg R) 

524.0 

525.5 

526.5 

CONVERSION FACTORS 

1 mm Hg: 0.13330 kPa 

1 em = 0.39370 inch 

1 mm = 0.03937 inch 

1 cu ft = 28.32 liters 

DGM Ambient 

Overall Temp 

(deg R) (deg R) 

524.5 528.0 

526.3 529.0 

527.0 530.0 
Temperature Meter Calibrations 

Meter Box#: 11 

Date: 11/06/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 32 31 31 32 31 31 

Point 2 100 98 98 99 98 98 

Point 3 250 250 250 251 250 250 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 492 491 491 492 491 491 

Point 2 560 558 558 559 558 558 

Point 3 710 710 710 711 710 710 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0.203252 0.203252 0 0.203252 0.203252 

Point 2 0.357143 0.357143 0.178571 0.357143 0.357143 

Point 3 0 0 0.140647 0 0 
PITOT TUBE INSPECTION DATA SHEET 

Compc.ny Name: Q ... 16/e 1(!1/!k'zc-~; Pre-se.mole 

., Date 7Li/o6 Post samplZ 

Date t/ } tf Cld y I 

11r1:1tr IIIOI(.JfiiOC; Lt'ftL ~OIIflllol 

K~tt lmiC&TIIfC Ltl'tL 

"'lliTIDol ·~ IICHIIOIOIOO: • 

JO& OUliiiiOIK; ,, :"'>oliO C£4tll\,.&l11C t. 

~rc:•U 1•01(.\TIC Lf~ 

ooJn '"" t~:~• :nro .. •••-c ., ..... a. 

• ~~·~/! 

j ~:;&~ :~ 

·-J.'• = . -!· . _--:-.:...-. --=-- -,-·~ 

Comments: 

. ....., .-· . -· --~··· ...... ~f ,IIIOtUTlC LML P:11tl010 

104 X"':tJIItll•u•lw;. '' .... &1 

·~ 

~·· 

I I 

! I 

0 

f 

I '0 

, tf70· 

level? 

obstructions? 

damaged? 

-10° < 

-1 oo < 

-so < 

.. 0 -::> < 

Cll 

02 

s1 

s2 

y 

e 

A 

< 

< 

< 

< 

+10° 

+10° 

+50 

• .-o -r:> 

~ 4 q t 1. OS Dt < Pa < 1. 5 

., .t.f tj t/ I 1 . OS Dt < P b < 1 . 5 D. 

,?7J"I 3/l6"~Dt~3/8" L 

f OJD A tan y < 0.125 11 

0 /A ta~ e < o. 03125 11 

yes I Pa = pb ± o.o63" 

I 

r 

I 

I 

. .:.; ~~~;· I ... .? 7s' __ , 

e o;s-r-1 

I 

ya.J J 

Pitot tube/probe number A tzY meets or exceeds all specnlca"Clons 

c~2ter2a and/o~ ap~~ica~le.desi~n featur-es*.and 2s he.r.eby0a .. s·~.)9ned a 

p1.ot .ube cal1bra.1on .ac.or o. 0.84. /? .. ~h.·~ .. -_. .. ...-. 

Signatu~~hf~ 

•See ~0 c~~ oO, Vc1. 42, No. 160. ~e~hod 2. Verify ~he ~inimu~ 

2 inch se":.bad:. of the -:hemoc:~up1 e and ~l'le minir::v::1 J/~ inch 

separa~ion b~:ween the·~~\.~': :u!::e and the nc:zie as shown a: 

:he top of :his ~age. 

... .,·I' 

Date 7 /ff.;b# 

282 
OC~•rr 1"'1(.-TI..C ~tYI~ •OUTIO. 

ro .. OCtt..,.t•tJt!. 'Ia :.-t• CAL:\1\..&1 uc :. ec:arc "'"'t ... T•.c LC'I'U ~ITIOoo IOol IIUU,t•l~ e 

I 

I 

f 

2-

"2.-

3 

[ 

{ . 

~ .)171 

Post Samole 

Date ·;1,/o JC;o f 

level? 

obstructions? /tJO 

damaged? 

( 

3 1 

y 

e 

A 

~ 1. as Dt < P a < 1 . s oJ , l 7 'I J :.. f 

~ .L9 I '1 . OS Dt < Pb < 1 . 5 o~ ; L 51 I 

I· 3/16" ~ Dt ~ 3/8" 

I. I 

j 

~n:•rr ••:,.c•Tr~~~; ~t...:L 

fOJ,Ittt- tol :C':'[••••t.C 

. z.~ 

• ~~-~'/! . i :::;::;:::;&2J ·o.o(2-

04 of.z,. :rrr==J 

a : . 

.. ....;.':.... ,.-~ . ·-· ·-·-· -

Comments: 

. ...,,. .-· -· __ .c.;,3. ••. ·-·· 

~...ot[ ,1100HATI..C U'ftL ~l:"SITIOOI 

10. x::t .... •••-.c; a: • .,.., •• 

•See 40 CF~ 60, Vol. 42, Nc. 15C, Me~~od 2. Verify ~he mini~~~ 

2 inch se:t.acl: of the -:her::'X:lcoupie .ana :he mir.i:::-w-m :l/< inch sep~:-t:lon !let:>~ee:~ the· ;>it::t t:.:be anc th~ !'l::::1e B sno..-n a: 

the t:? of this ~ase. 

. yes 

( 

I A tan y < 0. 1 2 5" 

~~ 

,o/Z- I 

I A ta~ e < o. 03125" .,o/1- I 

I P a = P b ± 0 • 06 3 " .._,jq} I 

/ 

283 
,~ P ITOT T~BE INSPECTION DATA SHEET 

Compcny Name: \Ck/.h/r f}fvtfCJ~t Post Samo1 e 7 Pre-sam! 

L- .... -l Date to]t[i6 Date {( /..{ fo 6 noc-..c:-• .,c ~ , 

C ~::H!I:&( (t) 

t :o~ =__........ .... . 21• '"· I rn..-.... ~m• I 

OftiU IIIOIVfiOoC; ~t'l't\. •o11TIOOt 

''' lftl.,.••••~ 1. :'>otll '""'-C\1\..1.1IOoC; 1. on:.arr •••cn•ooc uwn. "CCSITIDIO lOA l(fi ... IOIIIIC t 

Comrnents: 

or~:atr•o•IIICio11~ U'l'tl. 

~OJHIOII 10& ~ITf""""OOC 

....... ~. 

~~ .• .. •urooo: U'l't~ OV11Toooo 1001 ::l('n""•••oo: io - &o 

I 

I 

ya) level? 

fv6 obstructions? 

,JO damaged? 

I -10° < Cll < +10° 

I -10° < a2 < +10° 

1,- -so < 81 < +50 

I -so < 62 < +So 

1- y 

0 . e 

·~·1f~ A 

, 3SII 1. OS Dt < Pa < 1. 5 

,J 60 1.05 Dt.:< Pb < 1.5 

. 1) I 3/16" -~ Dt ~ 3/8" 

.o~~f 1Atany<0.125" 

(2) /A tan e < 0.03125" 

y{d) I Pa = Pb ± 0.063" 

I 

'\I rL} 

frJO 

tiJO 

1, ' 

I Ll 

7.-

0 

r 7 ~~ 

Dt I, 35"'&' 

Dt I JCO 

I ~r-· 

.. oLs-( 

0 

yrzJ 

I 

Pi tot tube/probe number .~ 0 meets or exceeds all specifications 

I 

I 

f 

I 

l 

I 

I 

r 

I 

I 

I 

I 

criteria and/or applicable design features* and is hereby~assigned a 

pitot tube calibration factor of 0.~4. ~ ;f~ 

S1gnat"Ur~ · Date ;o/tt/o~ - /( Lf/Ot- - ' j!f YSee •o CF~ 60, Vol. 42, Ho. 160, Method Z. Verify ~he minimum 

2 inch se:~ack of the ~he~c~up1e and t~e ~ini~ 3/~ ~n:h 

separa~ion bet;~een the ;>i tot tube and :he nc::h as shovn a: the t~~ of this page. 

284 
285 
NOZZLE INSPECTION AND MEASURfMENT DATA SHEET 

Company Name -D~c:::::(.~/...:...k~/.;_( e;:.._ __ " ___ Da,te Sampled ·Nozzle Number 

Presample Inspection 

I hereby certify that the ,above referenced nozzl'e appears to be 

round, sharp-edg~d, free of nicks and dehts and 

for us e· at t hi's t i me · , /7 ) 1 .. 1 7 L{ i . ( 1 ( 

Last Previously Measured 

Nozz 1 e Area o. ooo z..o9: ft2 .signature r 

Date Measured t.obo J (56 date ;o/:l_o/r;o 

Postsample M~asurement 

Measure three diameters as shown; me.asurement is 

in fnches; record bel ovt; .'perform cal cul at ions. • 

1 •• tcr<..f 

Ave rage· 0 i amet er , I 9 f.....-

'.: 

Are··a = n o2 

4 X 144 = • orJbz._ .. ocr 

This are~· sha-ll · e used in Aata ~---·- •' ./ .r~/~ 

'~/~ Siirlature-9 . 

.. 2 Tt 

reduction. 

~Maximum allowable difference betHe-eri hrgest diameter and smallest 

diameter. is 0.004 inches 

286 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Company Name ..... ~~-· -..~f-..~'+~...,;,t_/_(" ____ " ___ D a,t e Samp 1 ed 1 11 /J 1)./o t:. · · -Nozzle Number .. J.l{:7 .3 I 

Presample Inspection 

Date Measured(O/)o~.( date 

Postsample M~asurement 

Measure three diameters as shown; measurement is 

in i"nches; record belo\'1; ·perform calculat;.ons . ., 

1 • • L. (_! ::;- 1/g 2. . l., "-{ 

Average· Diameter . l- <f73 J 

'.: (I _. -

r.rea = " D2 

4 X 144 

This reduction. 

• Haxi mum all owe~ i ;-·;ifference te- I 

t\:leeri largest diaiileter and sme1lest f 

d1ameter is 0.004 i~ 

287 
Company 

NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Name D" (/J (_ Da,te Sampled. /0/J// o6 .-· Nozzle Number .. JoL!J. 

Presample Inspection 

I hereby certify that the ,above referenced nozzle appears to be 

round, sharp-ed·g'ed, 'free of nicks and dents and is· judged zcce table 

for use· at t h i s t i me . . 3 a -z. , J tJ '2... , a j , 

Nozzle 

Last Previo.usly 

Area .oo0 '1'7'6 

Mea~J.Ired ft2 · 

ignature 

V 

' 

~~ 

Date Measured t.o/>1/6~ date 11/.JI/a~ 

Postsample M~asurement 

Measure three diameters as shown; measurem~nt is 

i n i'n c he s ; r e c or d be 1 Ovl ; · p e r form c a 1 c u 1 at i on s . • 

1. ~)oZ.. 2. , )oz.. 

Average· Diameter .. }o ~ :3 --~~=~----------

P.re·a = iT o2 

4 X 144 

~a-re-a- shall be us~? ~data 

. ~_/" . ~ / /' ~~{ ... ··:,. 

signature tJ. . 

aate II/ c/o 6 

2 ft 

reduction . 

.. ..,.-' 

~Maximum allowable difference bet1-1eeri 1 arges t di cme ter and sme 11 est 

diameter. is 0.004 inches 

288 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Company Name D~ /f, ~~ Da.te Samp 1 ed .J 0 /1/. . , · Nozzle Number .grJ36-

Presample Inspection 

I hereby certify that the above referenced no-zzre appears to be 

round, sharp-ed·ged, free of nicks and dents and is.· judgedzacceRtable 

for use· at this time. , zs-J . z..~~ ~z;t'? . 

Last Previ o.usly Measured ·~ 

Nozzle Areq .. oa:>~ ft2 ' .signature ' R' · 

Date Measured to/JO/o ( date /CJ I~!Jidt 

Postsample Measurement 

Measure three diameters as shown; measurement is 

i n i n c h e s ; r e c o r d be 1 ov1 ; · p e r form c a 1 c u 1 at i on s . • 

1. _ z.rr 2 •• -z,.)6 

Ave rage Diameter , Z.J-.5-3 ~~~=~----------

Are~ = iT o2 = • ~."~(..)'t ~ f .... l2 4 X 144 ~~:.o~{; JJ J 

//'his a;;/sh~. be u~e.~)'f1 data reduction. 

~~::,_; signature /1' 

date !1·/ 6/o 6 

0 ·-·*" 

: Ma~imum allowable difference be- L~een largest diameter and smallest 

d1ameter is 0.004 inches 

289 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Company Name \J t6./ .z:j,. //""' ' - Da.te Sampled . / o/ J 1/ d f · · ·Nozzle Number ./ f,{ 

Presample Inspection 

I hereby certify that the .above referenced nozzl'e appears to be 

round, sharp-ed·g·ed, 'free of nicks and dents a~d is· judged acceJpt'able 

for use· at thi"s time. ( ¥7 /C"( ;' (8 f-:' ~· i 4/ · ~ , , I 0 / ~ / ·.------·/;~· 

Last Previ qusly Measured · >-d.~·- / L::jt:/, Nozzle Areqa,c.W/¥7 ft2 · .signature ' . 

Date Measured ;o/3!)/d. tr date / Cj'"lyt}Jjc;,/ 

Postsample M~asurement 

Measure three. diameters as shO\,.rn; me.asurem~nt is 

in i~ches; record below; ·~erform calculations. 

1 . p I ~6 2. • I ?")- 3. ,f K'l--

Average· Diameter _.:;...,_,..(_.k..._6 ____ _ 

Are-~ = 7T D2 

4 X 144 = 0 .. 000 { ~ ~ .. 2 rt · 

reduct ion. 

:r. I '""' 

\~~:::~3 \ ·~~2./ ' .· 

-~-- . I 

"/·la:dmum a11ovn:ble difference be- I 

tHe-eri l::r;est diatileter and smallest .l· 

diatileter is 0.004 inches . 

290' 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

i) .. f .,. ; 1: Company Name ~ ; {"C' ,-,~. Da,te Sampled ;{jt,·/Q C .. · ·Nozzle Number ., 3/ Z.?. 6 

Presample Inspection 

I hereby certify that the ,above referenced nozzl"e appears. to be 

round, .sharr-~dg~~' ·free of nicks and den~s and .is· .. j.·udged ac~. table 

for use at Lhls Llme. ,JfJ J(! .J!~~- .. • !~ /, 

Last Previously Measured · ~ ~/{n) Nozzle Areq ,ocJOS"' J} ft2 ~ gnatu e r / · , 

Date Measured ll jt/o6. date ///I/o 6 I • 

Postsample Measurement 

Measure three di.ameters as sh0\-1n; measurement is 

in i'nches; record belov1; ·perform calculations." 

1 •• J I "3> 2. I 313 3. I J/"L, 

Average 0 i ameter . J ( Z., 9- --~~=-------------

= 7T o2 

4 X 144 = ..;._ . ooo.)] _____ J _ ft~ 

reduction. 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Company Name~"'_/ A_. _(t ____ ...___ Da,te Sampled. II /J /o.( ... ·Nozzle Number __ L_I__:_? __ 

Presample Inspection 

I hereby certify .that the above referenced nozzle appears to be 

round, sharp-edg~d, free of nicks and dehts and is judged acceptable 

for use· at thi's time. , ,_1 11 ~ z.-/~ ~ l, 0 (. 

Last Pr~viqusly Measured r7 ·~· 

Nozz 1 e Areq< . · ft2 

Date Measured .// /J/o . ..f date 1(/;/o f 

~ . 

Postsample Measurement 

Measure three. diameters as sho\·m; me.asurem~nt is 

in i'nches; record belovt; ·perform calculations. • 

2 • I Z,/ tf 3. I~~~ 

Average Diameter " Z/ ~ -----~~:~-----------------

P.rera = 7i D2 0 0 ;¥'\,? "'Z- ~ 2 4 x 144 = , ~~o rt · 

reduction. 

..,·"" 

"" l·laxi:num alio~1abie differenc; be- J 

t• .. teeri 1:rgest dia;neter c:nd sma11~st Jf 

diameter is 0.004 inches _ 

292 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Company Name D:::::::_G-_/_.-_T._fc._, I,_, I-_. _____ Da.te Sampled !1./z/46 ... ·Nozzle Number I.Jtl.,;.3. 

Presample Inspection 

I hereby certify that the ,above referenced nozzle appears to be 

round, sharp-ed9~d, free of nicks and dehts and is judged acceptable 

for use· at thi's time. , Jl'- 1 . , J/L/ , /2/ J/) ~ ~. ~ ' 

Last Previo.usly Measured ""'f[?f.-/~'6~ Nozzle Area ,~orJ ~ ft2 .signature"· / 

Date Measured !1/?-/0~ date 1//zJ' 

Postsample Msasurement 

Measure three. di arneters as shO\·m; measurement is 

in inches; record below; perform calculati6ns. ¥ 

1 •. J ( 3 2. ~Jfl- 3 • ----'t......~J~/--=l..:;___ 

Ave rage D i a met e r . 3 (1.. ) ~~-----------

Area = ;r o2 _ ~3 ? _ 2 

4 x 144 - ~_ooo __ J __ ~-___ r t 

reduction. 

·. ·-·*" : Ha~imum al!o~~ble difference be- ~~een l~rgest Glameter and sm~11est 

diameter is 0.004 inches 

293 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

Company Name Q..,/;{/t ' Da.ie Sampled . . !/ J . o( .. · Nozzle Number ;2/7] .6- ~~---------------- ' 

Presample Inspection 

I hereby certify ·that the .above referenced nozzl·e appears to be 

round, sharp-edg~d, free of nicks and dehts and is jUdged acceptable 

for use· at thi's t~me. , t-1 1 1 Z.../1 1 L.l. o - ;/ 

Last Previously Measured :;;:: .// _Nv . Nozzle Area o,cOCJ Z o?., ft2 .signature '7 

Date Measured I)/ .J/t1 1

. date /1/;J/oo 

Postsample Measurement 

Measure three diameters as sho\"'n; measurement is 

i n i'n c h e s ; r e c or d be 1 Ovl ; p e r form c a i c u 1 at i on s . .. 

1 • ~ Z...l -, 2. ~ L/1 3 .. z,z. 0 

Averdge Diameter 6 "b(Cf3 --~,-, ------------

r.rea " > = 71' o2 

4 X 144 

/ 

2 ft . 

data reduction. 

date 11// ~joe * Haxirnum allowable difference betweeri largest diameter and smell!st 

diameter is 0.004 i~ches 

294 
. i 

I 

I 

·~ 

App.en:dix F 

:, 
Specialty Gas Products 

Date: 6/27/2005 

Customer: Trigas 

Description: CO in N2- EPA Protocol 

Cylinder No~ EB0000701 

Component 

Carbon Monoxide ' 

Nitrogen, Balance 

Reference Standard 

Description 

NTRM 

Instrumentation 

Description 

Horiba Process Analyzer 

31 06 Pasadena Freeway 

Pasadena,Texas77503 

·(713) 534-8217 Fax(713) 534-8133 

Requested 

Concentration 

50 ppm 

Expiration date 

5/29/2006 

Model# 

VIA-510-CO 

Project: 16017 

Exp. Date: 6/27/2008 

Cylinder Pressure: 1900psig 

Certified 

Concentration·. 

49.9 ppm 

Cylinder Number 

SX19190 

Date Last Clibrated 

6/10/2005 

Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

First Triad - CO 

Z1= -0.90 

S2= 204.80 

Z3= -0.80 

S1= 204.90 

Z2= -0.80 

X3= 198.60 

Y=0.28607+0.250309*X 

Average= 49.94ppm 

nalyst: _/-' -- ...- .------=:::: ~ 

X1= 198.70 

.X2= 198.60 

S3= 204.90 

Second Triad - CO 

Z1= -0.40 

S2= 513.20 

Z3= -0.40 

S1= 513.30 

Z2= -0.40 

X3= 496.90 

Y=0.031 031 +0.1 00163*X 

Average= 49.82ppm 

Accuracy 

1% 

Concentration 

994.2 ppm CO 

Principle 

NDIR 

X1= 497.10 

X2= 497.10 

S3= 513.20 

fHIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

1 0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

295 
; .. 

Specialty Gas Products 

~,. 

. Date: 6/2712005 

Customer: Trigas 

Description: CO in N2- EPA Protocol 

Cylinder No: EB0000761 

Component 

Carbon Monoxide 

Nitrogen. Balance 

Reference Standard 

DescriPtion 

NTRM 

Instrumentation 

Description 

Horiba Process Analyzer 

31 0~ p~sadena Freeway 

Pasadena.Texas77503 

(713) 534-8217 Fax(713) 534-8133 

Requested 

Concentration 

100 ppm 

Expiration date 

5/29/2006 

Model# 

VIA-510-CO 

Project: 16018 

Exp. Date: 6/27/2008 

Cylinder Pressure: 1900psig 

Certified 

. Concentration 

99.1 ppm 

Cylinder Number 

SX19190 

Date Last Clibrated 

6/10/2005 

Anaylsis Results: Z =zero gas, S = standard gas, X= sample gas 

First Triad - CO 

Z1 = -0.90 

S2= 204.80 

Z3= -0.80 

S1= 204.90 

Z2= -0.80 

X3= 396.50 

Y=0.28607+0.250309*X 

Average = 99.45ppm 

X1 = 396.60 

X2= 396.60 

S3= 204.90 

/'· - ----=:_ 

Analys~-z?~- ~ 

Second Triad - CO 

Z1= -0.40 

S2= 513.20 

Z3= -0.40 

S1= 51"3.30 

Z2= -0.40 

X3= 985.20 

Y=0.031031 +0.100163*X 

Average = 98.7 4ppm 

Accuracy 

1% 

Concentration 

994.2 ppm co 

Principle 

NDIR 

X1= 985.70 

X2= 985.40 

S3= 513.20 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

296 
Specialty Gas Products 

Date: 8/16/2004 

Customer. Matheson- Trigas 

Description: CO, 02 in N2- EPA Protocol 

Cylinder No: CC187154 

3106 Pasadena Freeway 

Pasadena,Texas77503 

(713) 534-8217 Fax(713) 534-8133 

Project: 1 0548 

Exp. Date: 8/162007 

Cylinder Pressure: 1900psig 

Component 

Carbon Monoxide 

Nitrogen, Balance 

Requested 

Concentration 

Certified 

Concentration 

200ppm 200ppm 

Rete·rence Standard 

Accuracy 

1% 

Description Expiration date Cylinder Number 

CC177636 

Concentration 

GMIS 4/6/2096 

Instrumentation 

Description Model# 

Horiba Process Analyzer VIA-510-CO 

Anaylsis Results: Z = zero gas, S = standard gas, X = sample gas 

First Triad - CO 

Z1= -0.3 

S2= 993.20 

Z3= -0.30 

51= 993.5 

Z2= -0.30 

X3= 199.90 

Curve: Y=-0.6893+1.001139X 

Average =199.6ppm 

Analyst: L-- .-, _,~' ~ Ling Wen_...---

X1= 199.9 

X2= 200.00 

S3= 993.00 

Date Last Clibrated 

8/6/2004 

Second Triad - CO 

Z1= -0.4 51= 995.5 

S2= 995.80 Z2= -0.30 

Z3= -0.30 X3= 200.60 

Average= 199.8ppm 

Principle 

NDIR 

X1= 200.6 

X2= 200.60 

S3= 995.60 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 297 
Specialty Gas Products 

Date: 3/22/2005 

Customer: Trigas 

3106 Pasadena Fr~way 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713} 534-8133 

Project 14445 

Description: Methane in Air- EPA Protocol Exp. Date: 3/22/2008 

Cylinder No: SX31814 Cylinder Pressure: 1950psig 

Component 

Methane 

Air, Balance 

Reference Standard 

Description 

SRM 

Instrumentation 

Description 

Horiba Process Analyzer 

Requested 

Concentration 

20 ppm 

Expiration date 

6/1/2008 

Model# 

FIA-510 

Anaylsis Results: Z =zero gas, 5 =standard gas, X= sample gas 

Fl,rst Triad - Methane 

Z1 = 1.60 S1 = 492.30 

S2= 492.70 Z2= -0.10 

Z3= -0.70 · X3= 199.50 

Curve: Y=-0.09706+0.099752*X 

Average = 19.87pm 

X1= 199.70 

X2= 198.60 

S3= 490.40 

// 

/-' ,/ 

tl.nalyst: ;t'::;.::: .. ;;.~·-::;Z~~·/ 

~ 

Certified 

Concentration 

19.9 ppm 

Cylinder Number 

FF23319 

Date Last Clibrated 

3/21/2005 

Accuracy 

1% 

Concentration 

49.22 ppm Methane 

Principle 

FIA 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

)0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

298 
MATHESON 

TRI•GAS 

ask ... The Gas Professionals ..... 

Certificate of Analysis - EPA Protocol Mixtures 

Customer: MATHESON TRI-GAS- DALLAS 

::ylinder Number: SX-32759 

Cylinder pressure: 

l_ast Analysis date: 

::xpiration Date: 

2000 

5/3/2005 

5/3/08 

Protocol: 

G1 

Reference# 

329498 

1650 Enterprise Parkway 

Twinsburg, Ohio 44087 

21 S-648-4000 

Lot# 

109-56-43191 

REPLICATE RESPONSES 

Date: 

Component : Methane 

Certified Cone: 40.8 PPM± 1% REL 

3ALANCE GAS: Air 

~EFERENCE STANDARDS "·>~; 

Component: Methane.::..;;~{ 

SRM #: SRM-27so,i1 

Cylinder#: SX-20007 

Concentration: 48.80 pp.m _ .... :.'<; 

·-:. .. :.-· 

Measurement Principle: TC, FlO 

Last Calibration: 4/26/2005 

Notes: 

:-.. · ..... 

........ --":>.. •• -·· 

:- ;~ii';~~~::~tili1~J>" 

- ...... ·;· 

5/3/2005 

40.8 PPM 

40.8 PPM 

40.7 PPM 

·" ....... 

Date: 

This certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2 . 

. nalyst ____ f A_:___,~y_·_D_._~--~-~--------- Date ----=-5/~4'-'-=/2,...0.....,.;0-=-5 

299 
MATHESON 

TR&•GAS 

ask ... The Gas Professionals"• 

Certificate of Analysis .. EPA Protocol Mixtures 

Customer: MATHESON TRI-GAS - DALLAS Protocol: 

:ylinder Number: SX-34951 G1 

Cylinder pressure: 2000 

Last Analysis date: 5/3/2005 

=xpiration Date: 5/3/08 

Reference# 

329498 

1650 Enterprise Parkway 

Twinsburg, Ohio 44087 

21 5-648-4000 

Lot# 

1 09-56-43192 

REPLICATE RESPONSES 

Component : Methane 

Certified Cone: 61.7 PPM ± 1 °/o REL 

IALANCE GAS: Air 

!EFERENCE STANDARDS ,._ 

Component: MethaneL:'~J 

SRM #: SRM-27505 

Cylinder #: SX-20007 

Concentration: 48.80 ppm 

·~:~~·~ 

ERTIFICATI~::~~:::r~::~n;~:;J:~~T~~f Serial Number: LR-92489 .·· .~!~·:~ .. : 

Measurement Principle: TC, FlO /)'' .. ,.p···· 

Date: 

Last Calibration: 4/26/2005 :' ): -~~~ .. -, 

:--~ ~-:.~ ...... ~~-;1 -~ 

. ~ .... · ........... · ·~~.. . ;~ ~···~· 

Notes: 

5/3/2005 

61.7 PPM 

61.8 PPM 

.•:61.5 PPM o-:• 

Date: 

rhis certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

alyst. ____ .!.._/~_ ... 

4

· ;?~·_}>._. _ .. ~---=-=-k- ___________ _ Date ---~51--!.4~12~0~0~5 

300' 
MATHESON 

TRI·GAS® 

ask ... The Gas Professionals Certificate of Analysis - EPA Protocol Mixtures 

Customer: Protocol: Reference# 

Cylinder Number: G1 

3106 Pasadena Freeway 

Pasadena, TX 77503 

713-534-8217 

Lot# 

25738-02 

Cylinder Pressure: 

MTG-CALI 

SX39223 

1900 PSIG 

10/.16/2006 

DO NOT -USE THIS CYLINDER WHEN THE PRESSURE FALLS BELOW. 

Last Analysis Date: · · · · · . -~··. . ts~ esf~. · · ·· · . . · ·.· ..... 1·:··,.. . •' 

Expiration Date: 10/16/2008 .. 

REPLICATE RESPONSES 

Component: Nitric Oxide Date: 10/9/2006 

24.87 

24.77 

24.85 

Mean Cone: 24.9 ppm +/- 1% rei 

BALANCE GAS: 

REFERENCE STANDARDS: 

CompGnent: 

Reference Standard: 

Cylinder#: 

Concentration: 

Nitrogen 

Nitric Oxide 

GMIS 

ND22477 

48.8 ppm 

Ex·p: ·Date: 2/15/2008 

CERTIFICATION INSTRUMENTS 

Component: 

Make/Model: 

Serial Number: 

1easurement Principle: 

Last Calibration: 

Notes: 

Nitric Oxide 

Horiba CLA-51 OSS 

42312910013 

Chemiluminescence 

9/29/2006 

NOx: 25.0 ppm 

Date: 10/16/2006 

24.84 

24.95 

24.95 

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

Anal~st: h~ ....._ Date: ( <:>/r 6 /.z-...--ue; ~~ ~~~--~---------

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 
Specialty Gas Products 

Date: 6/27/2005 

Customer: Matheson- Trigas 

Description: NO in N2- EPA Protocol 

Cylinder No: EB0001164 

Component 

Nitric Oxide 

Nitrogen, Balance 

Reference Standard 

Description 

GMIS 

Instrumentation 

Description 

Horiba Process Analyzer 

Requested 

Concentration 

50 ppm 

Expiration date 

11/22/2006 

Model# 

CLA-510-NO 

31 06 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713} 534-8133 

Project: 16015 

Exp. Date: 6/27/2007 

Cylinder Pressure: 1900psig 

Certified 

Concentration 

50.4 ppm 

NOx: 51 ppm 

Cylinder Number 

ND22557 

Date Last Clibrated 

6/16/2005 

Accuracy 

1% 

Concentration 

99.8 PPM no 

Principle 

CHEMI 

Anaylsis Results: Z =zero gas, S =standard gas, X= sample gas 

First Triad - NO 

Z1= -1.20 

S2= 994.10 

Z3= -1.10 

51=. 994.80 

Z2= -1.30 

X3= 499.80 

Average= 50.3ppm 

Curve: Y = 0.33645 + 0.099857*X 

X1= 498.30 

X2= 498.40 

53= 997.40 

Second Triad - NO 

Z1= -1.10 

S2= 998.20 

Z3= -0.80 

51= 998.50 

Z2= -0.70 

X3= 500.80 

Average= 50.53ppm 

X1= 502.80 

X2= 502.40 

S3= 994.20 
MATHESON 

TRI·GAS0 

3106 Pasadena Freeway 

Pasadena, TX 77503 

713-534-8217 

ask ... The Gas Professionals Certificate of ~nalysis - EPA Protocol Mixtures 

Customer: 

Cylinder Number: 

MTG-Cali Crossing 

CC176977. 

Cylinder Pressure: 1900 PSIG 

Last Analysis Date: 2/13/2006 

Expiration Date: 2/13/2008 

Component: Sulfur Dioxide Date: 

Mean Cone: 49.8 ppm +/- 1% rei 

BALANCE GAS: Nitrogen 

REFERENCE STANDARDS: 

Component: Sulfur Dio~ide 

Reference Standard: GMIS 

Cylinder#: CC 177775 

Concentration: 1 01.3 ppm 

Exp. Date: 9/4/2006 . 

CERTIFICATION INSTRUMENT$ 

Component: 

Make/Model: 

Serial Number: 

Measurement Principle: 

Last Calibration: 

Notes: 

Sulfur Dioxide 

Horiba VIA-51 0 

42321590023 

NDIR 

2/7/2006 

Protocol: Reference# 

G1 

REPLICATE RESPONSES 

2/6/2006 

49.44 

49.65 

49.78 

Date: 2/13/2006 

50.22 

49.91 

49.88 

Lot# 

20832 

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G 1 and/or G2. 

Analyst: ~ ::::::.. Date: ?:1!_9 1~0 7' c: 

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 

303 
MATHESON 

TRI·GAS® 

3106 Pasadena Freeway 

Pasadena~ TX 77503 

713-534-8217 

ask ... The Gas Professionals Certificate ofAnalysis -EPA Protocol Mixtures· 

Customer: 

Cylinder Number: 

Cylinder Pressure: 

Last Analysis Date: 

Expiration Date: 

MTG-CALI CROSSING 

EB0000352 

1900 PSIG 

10/16/2006 

1 0/16/2008'·~· 

Component: Sulfur Dioxide Date: 

Mean Cone: 50.1 ppm +/- 1% rei 

BALANCE GAS: Nitrogen 

REFERENCE STANDARDS: 

Component: Sulfur Dioxide 

Reference Standard: GMIS 

Cylinder#: CC 177775 

· Concentration: 99.6 ppm 

Exp. Date: 9/26/2008 

CERTIFICATION INSTRUMENTS 

Component: 

Make/Model: 

Serial Number: 

Measurement Principle: 

Last Calibration: 

Notes: 

Sulfur Dioxide 

Horiba VIA-510 

42321590023 

NDIR 

9/26/2006 

Protocol: Reference# 

G1 

.. !.·,· ... 

REPliCATE RESPONSES 

10/9/2006 

50.07 

50.10 

50.18 

Date: 10/16/2006 

50.16 

50.20 

50.13 

Lot# 

25738-01 

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

Analyst:.~ Date: 

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 

304 
MATHESON 

TRI·GAS® 

3106 Pasadena Freeway 

Pasadena, TX 77503 

713-534-8217 

ask ... The Gas Professionals Certificate of Analysis -EPA Protocol Mixtures 

Customer: 

Cylinder Number: 

Cylinder Pressure: 

Last Analysis Date: 

Expiration Date: 

MTG-Cali Crossing 

CC177031 

1900 PSIG 

2/13/2006 

2/13/2008 

Component: Sulfur Dioxide Date: 

Mean Cone: 1 00 ppm +/- 1% rei 

BALANCE GAS: Nitrogen 

REFERENCE STANDARDS: 

Component: Sulfur Dioxide 

Reference Standard: GMIS 

Cylinder#: ND22558 

Concentration: 502.1 ppm 

Exp. Date: 9/4/2006 

CERTIFICATION INSTRUMENTS 

Component: 

Make/Model: 

Serial Number: 

Measurement Principle: 

Last Calibration: 

Notes: 

Sulfur Dioxide 

Horiba VIA-510 

42321590023 

NDIR 

1/16/2006 

Protocol: Reference# 

G1 

REPLICATE RESPONSES 

2/6/2006 

100.60 

100.30 

100.30 

Date: 2/13/2006 

100.30 

100.10 

100.10 

Lot# 

20829 

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

Analyst ~ ..., Date: ?;/!.])?-:!:de 

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 

305