TSCA N0N-C0NFIDENTIAL BUSIIIESS lilI0nt',mlt:

OOEUI'ITIIT D E T ETII ?I OII O O E UI,ITIIT EOllTilEI. HUHIII DI?T ITEEIUTD

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EPA SANITIZED Page 1 of 77
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Consent Order, Consent Order for Contract Manufacfuter and

Determinations Supporting Consent Order

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rI. Ilrr.rr4ary of lr':.irr's of the Order

i itt. Cl.ruteirts ofP[41'l '

,, IV., EP-A'sAssessmentofExBosqxdaulRis! , ,; .' . : .' , , '

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VL rinforrnition Required to Evaluate Human Health and Envirorunental Effec$

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ll. TdoAs of Manufaiture (includes importation)r Processiirg, Distrbution in Commerce, Use,

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.IV. Requests for Pre-Inspectiou lnfonnation

V, Successor Liability Upon Transfer of Consent Order

. VL Modification aird Revocation of Consent Order

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VII. Effect of Consent Order

EPA SANITIZED Page 3 of 77
:i.

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. ' ZOO4(")),tme Enyiionmental Prgtebtion Agenqy ('.IEPA" q11'161 4geiic/) ispues the ahachd

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Orde4 regar{irrg preinanufacti,re notice ("PMNI) P.-] 1;226 for tlrq che'mical substance ,

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, I ft} q Compart''), to tak€ gfftct 'upoq exp{atioa of the PIVIN rwiew

,.,,,' I p#citl. fhe Compdn/ subrnitto{ tle PMNto EpApursuant to $ 5(a)(1) of TSSA an440 CFR Part'

: 720, 

, 

, 

,,., . '.' .,, 

;.,, ,,,:' : l',. ..i

Under $ lI of TSCA, it isunlawfrrl for ariy:perooi to Ail or refirse 6o comply witli any :

,: ,,1,,

p ovi5iO4 of '$,5 ol anV order issued uir{er $.J1 Vj{at<irc may, 'be zubj;ct lo 

variBus penaltiei add te

, bofli crii[inqt and civil liabilitypursuanl to $ 16, a,nd to spgcifiq enfprcertrenl and seiaure pur-suant

to $ 17. In addition, chemii:al substp4ogs subject tO !O Order issued under $ 5 of TSCA. such aS

',.

this one, are subject to t! $ 12(b).9np-ort notice requird-enl

II. SUMMARY OF TERMS OX'THE ORDER

.The Consent Order for this PMN zubstanpe requires the Company to:

(a) submit to EP^A" certaiq tiered toxicity testing before manrrfacturing the followirigr:specified

. ,,i..i.tn ;lii,r!ir{ta:5ir:r ..4.r'141-' ". . :. . 

- ...-!.i ";.-i"!.1:ii:11l-:i. , 

i'i'*i-:: ':"'

production volume limits of the PMN substatrce:

EPA SANITIZED Page 4 of 77
'.i':ir:r' Itr'I'cstin;;:

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;,i

],i.iil-,,1 r,-[i.;.1 ;i ',r'i',t;' j1i. ,'1;r,:iLi:; i' ii:: ' '::3'li],'j -13)

,t j. i.til -ir.in ci- i r: n i i i i;l; s e,r.', t z-;i.+ i t"I i; ri i-i cr : t : i't rl

,, i u ii{ip;ii:i-i r j 

o j-.Y ( I PX'l'.i g'i i). 620 0}

li.r:clenl cr;il" dami:trant lctirai assay ({ji'}oTS 8?S'5450). }i-,

;;r;sitivr:, an oral rodeni;ilerita.'lrlo tra: 'siceation test (CPPTS

b lO,S+e O) will'be requirerl as the fciit>w up tegl., '. I

1,-yel:t oral carcinogeni*ily test (CPif t'S B'i0.4200) in rats arid

'; , :1 fl.(l ,-',., !,J^J

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Iaboratory and

,(b):prov-'ideitswoikerspersbnalpfo.tective'equipmenttopIeventd9rqa1'exposr1fe;...

I ' 

= : ; ,j I L .

(c) provjde respirafors to its workcrs to prevent inhalation exposure;

(d) as an altemativ-e to using re,3-pirators,.maintain woikpJaee airborne copcentrations, of thePJvIN

' l' ,.::

substanco at or below a specifipil l{ew Chemical E*pou.ore.Limit ('NCllL") o1 0,03 4qg/m , ,

verified by gctual exposuremonitoring data (to pursue this option, asampling and analytical

.'..

method mrrrt pe dweloped by the Companf, verified by arr independent thircl'party lat

submitted,to EPA);

r:

woxker training in accordanre *itt the provisions of the Hazard. Couqrnunication Prggraru sec{ion;

i

(f) distribute the pMN substance only to a person who agrees to follow the saffIe restrictions

rts) and to not further diskibute the PMN substance until it has been

completely polymerized;

(g) dispose of the pMN substance only by incineration (deshuction and removal efficiency of

gg.gg%).orunderground iry'ection control (class 1 well, deep well injection forhazardous waste);

(i) maintain cerlain records.

EPA SANITIZED Page 5 of 77
' 

,, ., ,':-),; .,j ., ', 1li:,j',:;,,1 . i,i i'i 

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ri

agtenr ij:at all:rnftnnaiion ireroin ili# ii; clai.ri.,::r1 em cotrfidehtial bythe Con;;';Li.ny:s cortectly

identi fierl witliin brackets and tha.L any iurbr:rnaticn that is not l-rracketod is nat elajrned as

confir-isntiai. To rnak6; tiris r]ocuriicnf a"lailable jnr pui;lic vievrin,g, 111)1\ tvill rr:::novr; orrly the

,

,,,.

eB,qf,denlialEuqi+eryh]Qrqatigqgbl+s-Gr4 l : Submitter

,

identity, chemical identity, production v.olume, use infonaation, and process infbirnation.

Specific: [ -]. :

Generic: N-(2-hydroxyethyl) alkenamicle.

Use:

Specific: :

I

Generic: A component of adhesives and cosmetics.

Mauiryum 1 2-Mgnth Productictn Vqlume;

Test Data Submittq-d with PMN:

- SaLnonella assay-negative with and without activation

E. coli reverse mutation assay-negative with and without activation

Rat acute oral (gavage) : LD50 > 2.0 glkg.

Rat subchronic 28D oral (gavage) : NOEL 50 mglkg, with neurotoxic and male

reproductive system effects. i,,.; ,r

,:r-:ii..:,iRrt.A}Utedermal * LD50>200,0mg4(8,'--i'.: 11.i,.1r ' i. .'rr.-',;,'.i;,..' . ,-.

Minimal eye irritation in male rabbits at99oh ai.

Not a dennal imitation in m*le rabbits 'at99Yo ai.

ilt)'

EPA SANITIZED Page 6 of 77
...

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i'i;i' ;;rc;-tali't5r ls !i;"' i i n;.,1 i.,.

'|T*XJ.ottr z.:.i.i1al stti:.I;r * ilc:j'i i:; 3 0. 14 mflL

, 

'w. EPA:I;ASSESSilMNTOFEXPOSUREANDRISK

. The following me EPA's predr6ions regarding the p .robable humari and enviradmental

toxicity, humari exppsure arid envirblmental re.lease of the PMN substance, based on the

information currenfly available to the Agency.

Human Health Effects Summarv:

Absorption: Absorption of the PMN is good all routes based on imalog data,

Toxicologieal Endpoin-ts of Conctrnl EPA beliwes that the PMN substqgce may cause

carcinogenicity, heritable mutagenicity, reproductive and dwelolmental toxicity, and

neuroJoxicity based on data fo: a riumber of low molectrlar weight acrylamides in worked exposgd

See lvww.eba; goy/opotinh/rtewcheins/oubs/cherrcat.htn

Envircinmeptal Efects Stmmarv: -----------.-:-

. tsased on the submitted aquatic toxicity data on the PMN substance the concentation of concern

(COC) was established at 1000 parts per billion.

EPA SANITIZED Page 7 of 77
Ur;.,,:

Dermal Exposuro

(*CrIuV)

1.8 to 1$00 1.8

In-halation Exposure Negligib[e

') -,

0;0016,to,0,01

Dtinltjng Water , r

B*porure (mg/day)

n

Release to w4teq

(kddoy)

0 0

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--::r.-l Ri$ktocet€ralPubliii :

.----: r" =x :

i ft fCAi Co,og'"is p*ra a. Sufu O,tirti"-g lV'ater Aq[ This law re-quir. e$'EPA to detq+inp ths

' ; levcl of clldta4i1ants in drinkipg weter at whigh'rro adverse health eftct5 are likFly to ogqur.

,;

Basbd solely onpossibie health risk trud e;rposire oyerl metimg widh an adequate iargin of

: -.

safety, the aaximum contaminant level ggat (MCIG) for.acrylamidc is ziiro. Some people who

' 

drink water containing high levels of acrylamide over a Iorig period oftime coultl have nervous .

system or blood e{fects and may have au increase risk ofi:ancer'

EPA SANITIZED Page 8 of 77
ET\I\{I RONME NTAL .E_EEECT E

Tggger,gd t$tilg. The brder prohibits the Company from, exceeding a specified

Company submits the information described in the Testing section of

this Order in accordance with the conditions specif,ed in the Testing section. r

VI.

EPA SANITIZED Page 9 of 77
CONSENE CR.DER

r " s c o PBI o tr A.F FL x CAB ILfl 

*d;@,^**. rEAtip- xiEEMETno- ryg

(a) Segpg. The requirements of this Order apply to all commercial rnanufacturing, processing,

distrio-ution in comrnel'ce, use and disposal of the chemical substance [1

.l (P-1 l-226)("the PMN substance") in the United States by [.

| ("the Company''), except to the extent that those

activities are exempted by para$aph (b).

(b) Exemptions, Manufacfuring, processing, distribution in commerce, use and disposal of the

pMNi substance is exempt from the requirements of this Order (except the requirements in the

Recordkeeping and Successor Liability Upon Transfer Of Consent Order sections) only to the

extent that (1) these activities are conducted in fuII compliance with all applicable requirements of

the following exernptions, and (2) such cornpliance is documented by appropriate recordkeeping as

required in the Recordkeeping section of this Order.

lntemet Address (UHL) " http:/A,vww.spa.gov

Reeyelod/Hecyclablo n Prlnted urlth Vagetable Oil Based lnks on Recycled Paper $/lnirnurn 25% Postconsumei)

EPA SANITIZED Page 10 of 77
dis",. ji;'*,Iion irr (:)rflnotcc bf {.hc }.}dN :;ubrlatrn sclr.:.I'y fu:: c;rport ir. accoidance u'ith TIICA

gg12.(a)4d12@),40cFR720.3(s)md40criiP?"it'107. Ilovrever,oncethecompanybeginsto

manufacture tte Pldlrl substancc lirr uqe in the United Statr,s, ito firiher activityty tle Compary

,.

inyolving the PMN substance is ci.e,,qlpt as "solely for expotf' eved if soISQ amoirnt of the PMN

substa[qeislate-r.exportcd.AithatPomt:',thelequ1rem9!tsoftIiqor{erapp!yioatl.ae!iyi]ies

, associated vdth the PMN substance whil-e in the tenitory of the United StateS. Prior tq leaving

U.S. ter-dtary even tho99 quantiti€s of batches dfthe PMN substance that are destined fol export

are subject to teryts of qhe order, and @unt,towards a4y Foduction volumetest triggers in the

Testing sectioi of this Order.

tZ) Rpig+ch b pqvelopme,nt f:R&,p':t. The requiremenb of this Order do not appl! to

manufactrfring, proobssing, dishitutiori iu commerce, usc and disposal of the PMN substance in

small guantities sol.qly for r. search and devglgpurent in aQco:dauce with TSCA $56X3), 40 qFR

,..

720.3(w),and. ?tO CFR 720.36. The rcquii.mentl qf thiq ffiq also db not ap-ply to mariufiicturin-g,

niDerce, use and -disposal of the PMN sribstairce when manufrqhred '

solely fornon-co-inercial researcli and dwelopment per TSCA $5(i) and a0 CFR 720'30(i)'

. (3) Byoroducts. The requirments of-this Order do not apply to the PMN substance when

it is produced, without separate commercial intimt, only as a "blryroduc!' as definrcd at 40 cFR

720.3(d) and in compliance with 40 CFR 720.30(9).

(4) No Separate Commercial Pumose. The requirernents of this Order do not apply to the

!l\p,.I substance wheir it is $anufac,h.red, pursuant to any of the e:ennptions in'40'CER?J0.fl0{fi},r'*1.u..,,

wi{h no mmmercial purpose separate from the substance, mixturg or article of which it is a part.

EPA SANITIZED Page 11 of 77
c t: t- .' D.o.z|.ib) (r).

(6) .11_o:Ugle&bl j,t cAetgd Gui1d). I'he re4uirements of this Orcler do nci aErply to qua&titics

. of the PMN substance after they have been completcly polyra eized.

(c) Automatic Sunset. If the Comptmy has obtained fot tho PMN stbstai.rce a Test Market

Exmptioi ('TME') under TSCA $s(hxl) and 40 CFR 720.38 or a Low Volume Exernption

:

('LVE ) or Low Release and Exposure Exemption (i'LoREX') under TSCA $5(h)(a) and 40 CF(

72350(c)(l) and (2) respectively, any suc.h exerrption is automatically iendered null and void as

of the effective date of this Conse,nt Order.

rr. TERMS OF MAI{UFACTU.RE" PROCE$SII{G,

-

DISTRIBUTTOhI IN COMMEBCIX. USB. AND DISPOSAr,

PENDING SUBIVIISSION ANI} EVALUATION

The Company is prohibited from niauiufacturing processing, distributing in commerce,' { .

using, or disposing of the PMN substancd itr the United States, for auy nonorempt commercial

purposg pe,nding the dwelopment of information necessary for a reasoned evaluation of the

human health effects ofttre substancg and the completion of EPA's review of, and regulatory

action baqed op.thpt.infr,unationliex@r.i.ridcleordance with the conditions descrihed,in.lhisfuen:sii*:iii i;:"r.r':

EPA SANITIZED Page 12 of 77
't'''' iit- ': ']' "- '-i

.

\ -'./ :j--'-: .' ..:-:.--::-.i--\...:,/--:--:. r:-:'-:-.r ::.-: {: -

erivircnnrent srrcl r,vfuicfr is reclr,L"art1.' i;i: r'opoiter-1 undei't-S{)h se*ti*n 3(e) shel,.L r';ii:rerri;e tirt:

nppl.CIpriate I.MJ.I irie4tiitcaticl nullr ':i.ibr tJris substar:.*e ai:ii *ontain a statornent thalthe

,'.

sul;stance is su.bjcr;t-to ikris Cc.n,;err:i (,,. r,kr- Aclrlitional infbriiiiri-ion -rega-rr]ing uectiorl S(e) repcrfing

,requirerhents ca:r be fbiuncl,at lvww.eytt.gov/oppt/tsca$e,' ;

, 

, 

--| j 

,

.j

,#:1r.+r,..1;tre):dGooit Laboratorv Practice Jlanalards4ir.rililtcs@.mt(r6rtlsii'-Eachsqdy*tel.f,Qryeil to addfegs-ih.e-..:.':+iii#*rltrI

tisks identified in this Order must be conducted according to TSCA Good Laboiatory Practice

EPA SANITIZED Page 13 of 77
.,,.

i-,orrriucteci usjng ui:r:rcri. iled pr-rblished test guidelinos). Fro'uo*<;is tnust be sn-bmiiterl as ii sui:'porl

clocrr,nent i,br ihilrilvN, usirrg the ,urocedures sef ar]-t it 40 CFlt 72.0,40,, H:llA i,vili.respoirrl to *re

t.-1n:pany r,vitir in zl. .,vecJis of ree eiving the n ritten plotc';ols. l:,PA I'tview af a 1.es I p:iotocol docs

not'mean pre-.acceptance of test results. ,' ,],.

(ri) Irisgq{e.- ierilirirlteqrliie+eqtg 'Ihe Company is prohiliitecl from manufact+ryS the PMlrl

.: I i r' .t .,,., 

,. i

su'bstanr:e beyonil tlrc foilowing agglegate volurnes ('itheprqcluction lir:r:its"), unl*gs fhe Company

',

conrlucts the fotlo r^ring studies on the PMN substanie and su'omits all final reports and underlying

data:in accordance with the conclitions spqcified in this Tesfiag sectipn'. , , 

i

Production Volume Limit

',: i' {. .'

Tier I Testing:

, 

,. 

,.'

Tier II Testing:

mlce

'i .;. rl 'IaxicitV.'I-estms

90.day oral toxicity in rodents (OPPTS- 870,3 100)

witt, functional observational battery and

neuropathology (OPPTS 870.6200)

Rodent oral dominant iettial assay (OPPTS 870.5450)' If

positive, an oral rodent heritable translocation test

[OfffS 870,5460) will be required as the follow up test.

Z-year oral carcinogenicity test (OPPTS 870.4200) in rats and

EPA SANITIZED Page 14 of 77
lr

.. i; ..

:

IlpA prior tc oxcceiling the applicirti+ pror:lrcfion limit, The final report anr! da1'n l1ust'on

i. I :.

suli1rr itt:e6 as 'a sr-ry;1:ort dEroumeat fo:r .te FirAl,l, r rsi ng1 thr: pro ce rlnres set otrt in rl0 CIJR 7 2A 4'0 .

The linal r-qport,iirail containthe contents spccified in a0 Ch-lt" 792]85, Lr:rderlyingduta qhall lie

-,:

submittea to nFA in accordince wrth the applicable *Reporting,t? "Data'and Reportirg,",and "TePt

F-eport,, subparagraphs in the applicable test [Liidelines. I{owever, for purposes ofthis Consent

1

Order, the worrl "s1ou1rl" in those zut:paragraphs shall br: intcrpreted to nlean "shall" to lnake clear

.

that ,the 

u.1rt *isricn of such infbrnration'is *orr,lotory. nef will reQlire the submission of raw

datasuchass1idesandlaboratoryflotebookson1yifEPAiinds.on{hetrasisofprofeqsiona1 l

,,,

jurlgment, that an adequate evaluation of the study iannot take p1ac9 in tne absence of these:iterns,

(f) iesting Waivers. The Company is not required to conduct a study specified in paragraph (d) of

this Testing section if notified in writing by EPA that it is unnecessary to conduct that stirdy-

. (g) Eqirivocal Data, If EPA fin(ls.that the data generated by a shidy are scientifically equivocat

the Compaay may continue to manufacture the PM.[ substancd beyond th e applicable production

limit. To seek relief from any other restrictions of this Order, tho Company may make a secorid

attempt to obtain unequivo cal dalaby teanducting the study untler the conditigns specified in

pma.graphs (b.h(c);.aa4@),(elcept.thaf.theeudy.4aybe submittgdafter,rryeh, iagflaapFli.edble{i}qrtii,i.i:?':i:ii

production limit). The testing requirements may be modificd, as necessary to permit a reasoned

EPA SANITIZED Page 15 of 77
(1) 

'Il;rr;ept 

;ir; c[+sr; i'ucrl i-n sr.rlri:ali'ip,rLLI]J1 (h)(:Z), i[ ',riihiri {r 'wrreks of ]l,.t:oA'r; it;t;i.:ii:t ot" a

tcs;'u Lepor"t ald fial:a,the Cc,rupany tsceives wriften notice lJra.t .Etr)A ilrlds tlial the t-lr*ttgcno-ra;ted by

ltiIically irirr;ilii:I, lhe Cornliany is pr:ohibiteLi frq-rn lirrfhar manufaci;l:re of the,Phnl-l a sh iriy a.re sclc

sul: stanee b ey orr.d il r e app li cah-].c p ro ci u et ir :t: 1i"mit'

(2) The Companymay coplinue to manuf cture thePMN substance beyonrl the lpplicabie

:

pro_tJuction limit onlSr if so notified, in writing, by EPA in response to the Company's compliance

with eiilrer of the .firllowing subparagraphs (hXZXi) ot'{h)(z)(ii),

,'.|]-fi ^i*{ : f itt\.,t 1, (i) if there is sufficient tirne to reconrluct the study in cornpliancr: with ptlragi'?phs

p;), (o), and (e) before exceeding the prorluction lirnit specified in paragraph (d), the Company

may reconduct the shrdyi If there is insufficient tirne to reconduct the study in compliance with

: 

' 

- 

.i

paragraphs (b), (c), and (e) before exceeding the procluction limit specified in paragraph (d), the

.,

Corllpany-may exceed the production limit, but mlrst bthelwise comply with paragraphs (b), (t),

and (e), and shall submit the report and data to EPA:withln a reasonable period of time, aItr as

;

specified by EpA in the notice described in subparagraph (hxl). EPA will respond to the

c'mpanv' in 

TTlffi H #;:::;:ffi1J:T. n.,ice d escrib ed

in subparagraph (hxl), submit to EPA a written report refuting EPA's finding. EPA will respond

to the Company, in writing, within 4 weeks of receiving the Company's report.

EPA SANITIZED Page 16 of 77
i' i j.lilr:..:i',i,.1'.r'.:'-;,,j:.. !'t',;,;i'1','... i'',.r- ii:-i:'i. tll':i'' i 't-'i:tt i'ti'"

ali,-t (r:), thi; C,;r*pany renrain.s prohibilietl 'jionr firrther ma.ilulhcture of'tho PMN substi::tce bcyouri

_I_---,i4",t.-

thr; applicaUle productio;: limit.

@ The Compariy tilay submit to BPA, within 2 weeks of lirst i:ecomin g awar* of such

cireumstarces" a written statemert explaining why circumstances clearlybeyond the control of the

, ,., ++,...

Company or laboratory will cause or hav$ carrsed development of scientifically iflvalid data' EPA

rvill notiff the Company of its respcnse, in writing, within 4 weeks of receiving the Company's

reporf. EPA's written response may effierl

(i) allow the Company to continue to manufacture the PMN sribstance beyond the

applicable production limit, or

he Company to continue to conduct, or to reconduct, the study in

compliance with paragraphs (b), (c), and (e), if there is sufficient time to conduct or reconduct the

study and submit the report and data to EPA before exceeding the production limit specified in

fficient tims for the Company to comply with paragraphs ft), (c), paragraph (d). If there is insufticient time tor the uompany to compry wILr'

and (e) before exceeding the production limit specified in paragraph (d), the Company may exceed

the production limit, but must otherwise comply with pffagraphs (b), (c), and (e), and shall submit

the report and data to EpA within a reasonable period of time, all as specified by EPA in the notice

described in subparagraph (ixz). EpA will respond to the comp ilny, in writing, within 6 weeks of

::,receivingrthe Company's repo rt and drta,as to ryhether the Compalry.niay*continuerto tnanufacture

beyond the applicable prcduction limit'

EPA SANITIZED Page 17 of 77
.i:

,

_!

.i

!.

niarr.ifactlr':c, ploccssin;1, rlistlrbrition, nsc iinri/,;r rlislrola[ rif t]re Pl\4]i su.bstanr;;;'to mitigatc

.:

oxilosLlres tr: ,rrlto tr-ret:L.;r charar:tcrizitl:e i.islcs l,rresentcil l:y rhc PI/lt{ subsfanct,:. Withip 2 v,rr-:cks-

' frp* repeipt,of such a no{ice, Lhe Cgmpan,ymust cease all manufacfure, pioe**ilg, diStribution, 

,

.,,'+anddisposa1ofthePM{.substange,un1esseither;':i.l

(1) i,vithin?- vtoeks from receipt of the EPA notice, the Compan-y complies wittr

suchrequirer,nentsastltc,.roticespcci1iqS;of:,,

..t , 

l,

., :,

: (2) 'within 4 weeks frorn'receipt of the EPA uotice, the Cpmpany submits to EPA a

(k) Othf Requirements. Regardless ofthe satisfaction ofany other gonditions in this Testing

, ..segdoiq:the@. pm.luixirsficodi[.uqi-taobey all the ter4s pf thisGoosent&derrurtiimt&ufise**ts'sjiL *...-

notified in writing by EPA. The Coinpany. may,.based.upon submitted test data or other relevant

EPA SANITIZED Page 18 of 77
r ing, pracgssing, an'l use of tha PMN $ulstirtce fal Lcl+L@4_st Dunn8manufactur 

, , , : . i, ... ,

.t'

at r,nv site controllcd by the Cornpany (incJudr'rrg iny associate<1 paokaging arrd stqragq and during '

..,' . 

i r.,

, 

. 

,. ]

any cleanirig ir maintbnalcb of equipment associatod with the PMT',I substance)' the CQmpany

. . ",,.. ,l... --:--. ----:-. 

. 

, ." .l .. ,., , '. '' ; .. :

. 

' t ; , : . ' , 

, , ,. . , 

.: ': , , ': I 

"": 

I ,l'l

,.i:,.r ,' i"i '' !

- (1) Geperal Derm.al Pi;te4ionj Eaoh pcrson who is,reasonabl.y likely to be dermally

: :.1','I ' " .: ,:l

:expose{ in $e work areatd ttre plr4N substancc ttrrough direct handling ofthe subsfaiuc or I': :""'".'.. . .., .'.',.

tlrough contacf with.eqUipme,nt on which the sqbstartce may exist, or because the subslancg '1 

'

. , .::. , . . ._ .. ' ided with' and is becomps airtqme iq a frirm listed in ssbp,ara-q4pli (aX2)(i) of this sectro4 is prov,

1eirilr".l to wear, personal protec..tivs eguipment that proviiles a birrier to p.reve,nt.d. fl*4 ."-{potrnp

tq the substanpe in the qppcifiq work area where it is selected for use, Each such item of pcrsonal 

:

protective gquipment must b1 sl.lected and uSed in 

lcoi.dancewith 

OccupatiQnat Safety anjl

:'

rraoean;nttratios f,osiflA?) denrlalprpteclrotrrcquir,emeds at29 CFRi910.132'll9l0.1Ei :

. .,t ,. 

,.',..,"i.

anrl 1910.138.

, (2) specific Derind Prctedv,g ..q.u.lilPen1, The dermal protecti-ve equiprr.eart required by

subparagr-aph (a)(1) of this section must iaclirde, brrt is not limited to, the fellowing items:

1i; Gloves, The following gltves have already b-een tested resulting in no breakthrough

. an6 no permeation by the PMN cheinical: North Silver Shield Gloves; Ansell Barrier Gloves,

r.- -. Norfh Butyl Gloves,-Aqseltr@t lti+rA:6]res'.*uselli1{popreqe Gloves, Apsell So1,.V.6ac'a4idr'{:4jr5."Bei"ai1*:t:r.'*

Alsell Canners.

EPA SANITIZED Page 19 of 77
Frcyant (iss-riai expo$Er; duling oarmal anC cxpected du,:itlicu nnd r:or'riif;ons of exl.:rsure within

u1e worK alea Dy any oBC or a ,:rrnbination of the fbllowing: '

(i) E€rmCdiol1-1:c_$ine. T'estiag the material use.d to rnake the chemical proteciive

'clothingandtheconSEuotionoftIeilot!ingtoestab1ishthatt1reprotective9lothingwil1be ,,.,, ,'.:

impervious for'the.eXpectcd cluration 4qd couditions of exposule. tho tes'ting must subject thc

' ;''.' : .. .,..,. .I ' ::''r:r "' I 

"'i'

combinations of ch&iqal substances to which the clgthing may beexposecl in the work area'

:,

peimeatioli te$ting shallbe condu-cted according tp the American Soqi*), for'.Xesti+g imd M-aterials

,,,,,,,

. (;ASTiWl F'Zg9 "Standard Test lvtethoa for ferrneation of Liquids and Gases tlrougft Proiective ' \:.":--'- !.':'. --:-.--. :

. 

.. .'.'..' . 

.,t 

. 

" I

Clothing Materials undpr C-oqditions of Continuqus Cortact,?? Results $al[ bb reported as tlte .;-1-..,.1----.,..:.-'.;.,...-,]:

,,

imolutirr" poreAioniate as a firnctlon oftime,qnd shall bq docuri:ente{ rn 3ecgrdaage with

.,...::;.'.;..,..'.:::1'\,..l'',.,.].:':':]

AsTIvr F739 rising the fbrniat specified in ASTM Fl 194-99('010) "standard Guidefor

'_l

Do-tupe,fin the Rlxu]ts of Chemiiml Pirineation Testirrg of M4terials Used in Protective

Clgrhing Mdterialsi' gloves may npt be used for a tirng Period'lone€f ttrao they are 4ctuallytested

anrl must be ieplpced at tle end of eapb Wo* shift during which they are exposed to the PMN

substahce.

(ii) Manufacturtr's Sobcifioatipns, Evaluating the specific4tions from the

manufaoturer or supplier of the cheniical protectivrc cloth. rlg, or of the material used in

construction of the clorl ng, to establish that the chemical protective clorhing will be impervious to

stancs alone an{ in likeJ,y,eombinationrwit}rofher,.chr*nioal:substances in the wor"k

EPA SANITIZED Page 20 of 77
-t .,:l

s$otion is 1:rtivii:lecl with iii.il is r:oquircd io ,.,-,oal', at a ininimuln). a lrln'ii.cnai ir,stif:Eie ,i,tt"

()+cupatiolal Safctf anci [{calih ('Nl0SlJ").-certifictl respii'atoi' r,vitir an A^pplied Pr'.:tectit:n }.a.r:.tut:

:

(6rAr,Lr,') of i.il{}g, fiorrr the respirators listerl in subirai:agra'.i:h (uX6lof. this si:c'tioh, a;rcl th-e

,:

respirator is uscd in accr;rdanr)o rn ith OSHi\ and NIOSII respira.iory protection requiiemerrts at?*9

I

,:

CFR 191 0.134 and 42 CFR Part 84. A11 respirators must he issued, used, and'maintaineil

,

accorcling to an appropriate respiratory protection program under the OSHA requirements in29 ':

,

cFR.1910.134.

(S) El$UgALEIate€. The fr:llowing physical states of,air.hor:re chernical sLrbstances are

listed for subparagraphs (a)(1) and (4) of this section:

,,

(i) Particulate (including solids o: liqlid droplets),

(ii) Gas/vapor (aII substances in the gas fonn), or

(iii) Com-bination Gas/Vapor and Particulate (gas and liq-uid/solid physical states

{.i

are both present; a good example is paint spray mist, which contains both liquid droplets and

vapor).

Authorized Reslirators. The following NlosH-certified respirators meet the

minimum requirements for subparagraph (a)(a) of this seetion:

(6)

EPA SANITIZED Page 21 of 77
." 1.j

(i) Any iilii5f{.r;r:ri.i.i,ioil ipoin,errerf, a;l.t ptlnrfyiiirl Iir1l fac'-:piece respirr;*o.r

equipp,rcl with appropria-ie gas/vapor (acid gal;, ot'g;:.'nic -^rapor, or subslani;r:

specific) *a iirirl gcs "

(II) Any I-ffOSiT osrtifie,J p'*werert a,i.i-pwrifi'l**= respil'aior eqillppcrl ''n':fit- ;t

hoodorhe1metanrlapprcpriategas/vapcr(ac]ctgaS,0Ig:}11icvapor;.oI'.

substanco specifir) cu*riOg es with evidence demorustrating prlotection level of

1,000or.greater.l ' 

, _'

(III) Any Nlc}sFl-certified continuous flow supplied-air respirator equipperl

with a fuil facepiece.

(IV) Any Nlg5H-cor,rified L:ontinuous florv smpplted-.flir respitator equipped

*ittt a hio,l or helmeLw'ith evidence demonstrating protection level of 1,000

or greater.

(VI) Any Nl0sH-certified pressnre-1-*:lf or other positive pressure mode

supplied*ain respirator equipped with a fu}l facepiece,

If Ni Cqrlridge S-ervice Li:fb Tesfing has bgefl.Qqndrycied;

(I) Any NlosH-certified continuous flow supplied.aii respirator equipped

with a full facepiece.

(II) Anv Nlg$H-certified continuous flow supplied-air respirator equipped

*iin a hood or helmet with evidence demonstrating protection level of 1,000

or greater.

(III) Any Nl0sH-certified pressure-demand or other positive pressure mode

s upplied-air respirator equipp ed wit!-q'[u!] ece.

osHA has assigned ApFs of 1000 for certain types of hoods and helmets with powered air purifiTing respirators (PAPRS) or

supplied air respirators (sARs) where the manui'acturer can demonstrate adequate air flows to maintain positive pressure inside

the hood or helmet i, rd*rf working conclitions. Flowever, the employer rnust have evidence provided by the respirator manufacturer

that the testing of these respirators demorstrates perfi:nnance at_alcvel 

-oflrotection 

of 1,000 ^olg:ut*tj| receive an APF of 1,000' 'This

Facroi (s\yp,) study #A[i;#,Ji#d,i:tW*'n*-t-;roiifriii^ ti,at rterr.onsrares a Ievel tr pi'otu"iioii'^ofr1;0s0roi'gre-itei;aii'PAPR' 

' ''. ;i

and SARs with helmets/hoods are to be treaterl as loose-fifting faeepiecc respirators, and reccive an APF of 25'

EPA SANITIZED Page 22 of 77
..- i.n. ..

,:.,i'

i

-,' ./ :.'... --:---:., ::-":'Y.*'i-Y -jj.:..:-.::::,.. 1;::--:.'-.

/1/) ';i ':''- 

;l.r;.rluli.-illoPI-'.4T"7 .i:.:t.tC,g;qCr:C',. 1.0 pei'Ctrtl'l;y Wr;iprjrl l:,'',ri)j;,'.ile l-i' j :;r):it';l:;-;t i:y t'r*r, iilt--)7'il/'

'i:

,:

Pro.qrar,isecti.;noftlrisL.rrile:).'Ihis..lx,lrrtpi:irlnisntlta.railaI,*Ieift1reComprxryhasreasonito:

belie 'e h,tt,rirrring itrtenrlefl acfiviticr;, 'll!,c i-t1,41{ Su-ir.ii;1.1Ce in the titixbu.re .may be reconcentratqd

' 

: _ 

' '''"'t '''"' 

'- 

::_' ' _' 

' 

" 

i 

I ' l

abovethe10oi0.1percent1eve1,w}riehev*r'rppii*s.Ift}risordetcontains'NewChexqieal,

Exposure Limits provisions or Release to Water provisions that, respectively, specify a NCEL

I

, a /1

concentr ailan[*'TwA,') or in-skearn concentrotmo ("N") less tha_n the de minimis concentfption ,\, ]

ry:ecilie6 hes-,,then tlris'cJe urinirnis -+xernption does noi apillSi to f itosn :provisions.

I

I

(a)

',. ,,.''. :]:: '

, (l) EPA rem{rmencls and elr, courpg, es theusg o|pollution pr.evelrtion, sguce redggtion,

engi4eering.conhols aod wo.rk practices, rather tlian respirators, uis. a me9p5 of coltrollia!

inhalation exposures w}renev. er practicable-

(2) Whenwer a pemor is reasonably.likely to be exposed to the PMN substance by

inhalation, as an alteriative to compliailce with the respirator requireurenfs in the Protection in ttrq

. \{orkplace section of this Ordo, the Company may oomply with the requirernents of ihis New

thc Co,ptpany may deviate from the respiratgl 

,

requirements itr the Protection in the V/orkplace seetion of this Order, the Company utust:

NtrW CIItrMI CA.L EXP-O S UBE -L-IIAIT

-+.i+-ffi-T-:Tr:-T:--rEPA SANITIZED Page 23 of 77
,:

l'b) Exuosure Limit. ,'

(1) Ge+erai, The followirrg new chemical exposurp limit (T\.ICEL') fo{ the PMN

substance is an interim level determined by EPA based on the limited informatiou available to the

._-,.,

Agency at the time of development of this Order. The NCEL for the PMN substance is as follows:

(i) Tinlp-Weigfuted Aveiase ("TWA']) Limit, The Company shal1 ensure that no

person is exposed to an airborne concenh'ation of the PMN substauce in excess of 0.03 m#m' (thg

' i ,' '.NdEI-) as an, B =hour time-weighted avardgl,wi$grrt using a i**pioifo, ih: aqxordan:e a r,vith

subsection (e) of this Ner,v chemical Exposure Limit section.

EPA SANITIZED Page 24 of 77
. i5,

\/

-I

lU.4 ,r)/t.5f, o,i,.or* tt --= tlti: n;ti':iile.i-'5f ;i:;ll;s i;r ihe a.cl.r.::-i '.vort<-rhift.

(c)Bdqqlasseq+ei4&Jgeliace+d"&eJ@ga]$-e$9a, : . ;

irl'app:"+tlitr l*iilioitia uryqtopilient antl valiclatio:r of tlre q4lirpling and *ilttitul

rnethpd for rtrc PMN Substance, alI tte rcquirerapn+s 9f t{i1 lbsection. 

(c) apPly. )i9r subletucn!

elpqsure mopitoriirg 

"ouaortd 

p. qslant io subsecti= (d) of this Nwl Chemical Exposure Lrmit

section, onty the follffi requirernents apply. (c(l)(i)- (4xii), (4iGv)Oil; faXv)GO, (a)i and (9D

-----,- .a:.:,, : 

.,.,-, ,, ..i.: ,:. ".,. 

, 

.

{4y deviltiori frop-tle re+rirlertlof.this subsltion (:j -"tt te *1ofe0 ln witine !v E?A'

,1,,.,,.-

(Z) Su.tmlssion.of V.erifiqidMethpd an4 qertif,.cation Stalg&qgll 'fhe Comfauy shall

submit to EpA a copy of a validatedsampling and analytical method for ttr9 PMIri' substarice which

i:

satisfies the criteria speoifled r+ this zubsection (c). ilhe method description shall exp:essly state

. 

:.-1: .. . ... ...

how the rnetho.d compares w.ith each quantitative requrgment specified in this zubsectio-n (3), The

suimissign must inclurle a'written stateuie,n! sigped by authorized bf6cials of both the eompany

,-

corducted'pursuant tq subso16Oa (c)(3). To assist EFd iri identiSing'the docum-en, q it shall state '

ir a consprcuous, underlined subject-line at the top of the first page: ItEELS@iSC.and

Anatrtipal {,Iethpd foi pMN.' after which the co .rrect PMN number for thic ohemical substance

shall be stated.

r !:;it{,r.rr:i21ir:+:{it:i46iii[l!BLti@r*Ibm$p4pany shall havq anindrpep4eetle ' --.....{b9,ffi1r,;3gl;tia*"r"*--

(l,Laboratory',) verifi the validity of the analytical method for the PMN Substance, in accordance

(3) Verifi

EPA SANITIZED Page 25 of 77
.. ! / -

r zith i:i:r rr'1,:, ,',q'rirr,rl.,.":I t'ir i.',:i :tib'J:,"ii.i: ). in)(3 ) . ,.1 i'; i1tr, t)i :i1;:"-"7'r '--c "1':: ':iiit-7 to r'ire lt"-:

'i,,ti,. ihe i.,al.,,:,'.':()i7 co1',:,r.,iie,s \i'Ji il ail i:iii; :tc'rin:iremen+:; ;peci|e4 irtlJ:.|s r'':i'l':''Jrlori (r:')i3)'

(ii) ifi.1leperd-q1-ti.-cfue,ts!-i.abalats5,t The inrlependent . Dfercn ? lairoratory must

be zi sepmate anil rlis'rirrct person (z:s deliueil at 40 CFR 720.3(x)) liom 1fur:, {lontparry aud liom any

oth.er perst-rn tvho t:trLi.yhave develr:ped the rnr:lhod for the Coinl:any,

government or pdvatc laboratgry accredi{ation prograrn foi chemical tgsting andlor aOaly.sis,

' '.1, t j l I

(iv) Good Laborato.fv Practice Strin4arq$. The Laboratory verificziti'oq ofttre \ . 

-::-

,,.

analytical method ior the Pilm{sulqtaiice must comnfr.ivrth TscA Good I,aboraiory Praptice

Stardaxds (,.GLp:,) at 40 CFR P?rrt 792. (Cedah proviiions of.the TSCA GLP apPlicablc to

toxicity testing in laboratory animals, such as 40 CFn 792,43 ('Test sysleq carc facilities"),

,-.,

792.45 ('Test systeq supply faoilities') a$ 792.90 ('l$nimal and other test s.yste'to gate'i), are

clemly inapplicable to the NCEI- ruiuirenrents) However, conrpliance with TSCA GLP iS not

requir.grt under'tbisNew Cheqical n.n"r*; f:fr"rt seciilol whero the anatyti"ut method O 

:,*

by a laboraiory accredited !y either; (a) Oie American IAdustrial Hygiene Association ('Atr-LAr')

prograu approveil in advance in writing by EPA'

(v) Analysiq of Dlplicate Sapoles. The Company shall collect six duplicate

,

samples (a totat of 12) at thc iwA conccntation. The samples shall be taken either fro-m a

controlled eirvironment (e.g., a sealed chamber or "glove bo/) which closely rese,lnbles the actual

workplace condiiions or, for solids anfl liquids with very low vapor presstrg by injecting'the PMN

substance onto asamptr&solpdiofl4iddi1g3&Ig.dpptrieate samples shall be collecte-il.o&ridedtical&$r:illi1Y*trl.jlis

collection media, at the same timo, and under the sa-e condifions. One set of six samples shall

EPA SANITIZED Page 26 of 77
i-,ai:;.rrilciy uo.il;; i.i.t t 't:,.,'o,].t:,4 dt,: r:11;i.lr:.i:. i,:, I i ,"?;::'lh+ Cc;rrl:'rr:.iI

(vi) ,iasrpig-,.jq-li:ge-gtrd.n If the iosults oi't.he analysis of duplic*e samples

pursuant to paragraph (oX3Xv) r1c not satir;fy the requileuror,.is in paragraph (c)(3)(vii), the

. Compa:ry must perfoml a sauple iitorage r:tudy as follows: 

..

(D Tdeiisu-t€.$ggrpte.s. The Company shall qollccl six triplieate saurples (a

total of 18) at the 'I'WA concenlration. Tire samples shall be taken ei*ier: fron a controlled

- 

etrvir6fi-nelnt (e.g., a sealed char-rber oq "glove box") which clopelylgsunbles the acttral workplaee

conditions or, for soliils and liquidr with vsry low vapol pressure, by injecling the PMI{ subsltince

onto a satriple collection devicc. The triplicate samples shall be collbcted on identical cqllection

media, at the same time, and under the s;uae conditiqns, One set of six samples sliall immediately

be analyzed by the Company.

(II) Analfisis Atq Sampk Storege. r\ samplo storage waluation.shall be

perforrreil with tho two remaining sets'of six samples, Ore set ofslx saniples shall be aa alyvedby

the Laboratory using the methotl dweloped by or for the Compaoy, and the other shall be.arialyze<l

by the Company on the same day as the Labqratbry anal5zes its six samples. Specializ:ed storage

conditions for tho samples including extraction conditions, time tom sarnpling to o<traction, time

. 

from collection or exnaction (if applicable) to *ulyri, *d ,tooge conditions must be specifietl in

the metlod description.

(vii) Comoarison of Rixults. Ihe differe,nce between the results of the two sets of

six samples analyzed by thelaboratory and the Company as required in either pmagraph (o)(3)(v)

:," ig.;::"-1r:trli(rr).@.)(uiXll) shall be evaluated usinggrt.w6:sryple..t.tpptrv.ifh,ua8q1ialivaliaaces, and the two- . .arru,+ riiii,i]r

sides ofthe critical regions shall not exceda5% significance level. (See r\ttachment C -

EPA SANITIZED Page 27 of 77
wilhi:l i0% of {lre {:tLc vahie, therr iLr; sanr:'.;Ll stolaS,..c iirne hoiurcerr or;ilecli+li aad a-neiysis mmt be

' reduced unti.i tiro 4ve,rLrge ol'oach sctof six lirmpl s is lritlir 1.0% pftlle truc value"

. 

I g) an o*n l The sampling.and ar,,rl5rtical riretlrod urusl ciearly dernonstratc the

:' I .:r :-: ., .r '. "

, 

(D Qe11srd- The sarupling anrl- anal;,lical merhgd, and qlf cxpgsule nionitgnng data

: .' : .' : ,'. 1. ., .,. 

-i. : ,::rri"r-: .:..i.-'i ,, .';r , : :.:... -

felied on by tlie Ccimpany, shall te ac.curatq tq wilb n +25% rt a95% confidence leYel for . 

'

...:'. . r. :.:' '" r'-,''" t -r'::r:':':i'-''''','.1 :.. :. ',

concenhationsofthePMNs9bstan,cerarigir,rsftom1eIraIfth;NCEL9twicethiNc,rr'

lr,:'l ..,:i-;''(, Iii) NCEL Ouantitation Limits,"Ihe analvtical rhcthofl shq,uld be capa$le of '-: - ---:-l -- 'll - 

.,.,, , ,

reliably qridntif-ying tle PIvIITI .ob-.stanee ucross the ful.I raage of'reasonably likcl.1, cxposrrrps. At q

. . -ir,i*o^, the anafu4ical method musqbe capatlq ofieiiffi rying fiom a tower quantitation

'.-,.',^:,,.

. ri'*i ( iQr') of;o1e b.al{theNcP.l ,3 il yoyantiu.{1ir timit ('UQriir at teasl twi11 tte 

,

NCEL. If the Company obtains an expOsure monilothlesrmple thatjs marc than 1-0ilo above the

, 

.. , , 

... ,,,: .},' ,

actia UQr oftte analytical mottiod" the pompmluxst ood wi$n*@ tel(4x0, 

'

:,

, 

' , ($i) f,o,lwrQrl+tilAt'oq Lig.rit $ietrA+o-Noise naiio, The. analytical metl0d shall ,

' , becapableofquantiff,in-gthePlMlVtoaconcentoationofqnghalftheNCELrviihasignalthatisat

least fivp tiues the baseline nois! fevel Easeline npise must be arnplifieil to a measurable lov.el

*teo possible, wen if the required amplification is beyond that used in roufine imalysis of 

. 

.

samples. (If baseline noise camot:e obtainett, another reference must be selectetL This may be a

peak cgnsidered to be noise causedby the reagent matrix.) The sampling preparation method must

,''

..-.iri,{.i,ii.{iscspdeige*,and;meeae6doa"timit for ttie analytical proqpdurexru.ssi+ifud444sa}q+J:isru,',. ".

injection for cliromatographic tecbniques.

EPA SANITIZED Page 28 of 77
i l'' j i.i:=., r.1 I : 

ililili.l -'=Ltl 

" 

i:' tJ'-G I r'..

lt .; .,',{-'^i..:',' i''t ' '': iri-:-::l:i'-f :"i '':::" '! \'':' I

i

r;a1ibi'aitioil slalldarrils witJi n lini';a.t'oor1etatiol of 0.95 ",'i-lrcr:t' i-ive (ii) caiiL:raJion st:mr-larrls i:riust

I

consiuL of onc standard at each o Ithe foilowing c{riicontratici';i: crlo haiJ: the }ICEL (0'5 x ITT(JFI);

betwc*ri o:re half and one iimes i:iie irlCEI-, (>1i.5 x ]'Iijiil,( 1 x ):'lCfiIJ; Qne times the I{CI-{' (1 x

':, 1-,r:,

IrfCEl); between one ancl rrro tirn*s thq NCEL (>1 ;r NCEI ii 1?- x NCEL), arrd twice the H{-EL Q

'I r'.

x NCLiL).

,

develoBgrent/valiclatiol anil suhserluent **po.rrre monitq:fini],,.thc Compary shall conduetboth an

jnitiai instrument calibration and'a c'on'iinuihg calibr r. i'he- Company shall perfonu at least one

,l

ij '. : ", ' '' ': ' " ' ; '' - ' additionalcalibration, confinurng caribiation sample at the NCEI, concenti#ion, and alleast olle 

. 

.

,$arnple per eyer, t p samples analyzgd, T'he continurng calibration 1amnle 

shall falI within 1-. 2570

.. 

I I

of the initial calibration value. If not, thet the initiai calibralion must be repeated, and any samples

:,'

associated with that outlying calibration check must be rg-analyzed, ' 

. , 

,

(I) Initial Calirilation. For method deveJopment and validation, the

Company must calculate the percent of the PMN substance recoYered by the analytical method

from a sarnple containing a known quantity of the PIvIN substance. The s4mple shaIl be taken

either from a controlled environment (*.g., a sealed cfiamber or "glove box") which closely

resembles the actualworkplace conditions or, for solids and liquids with very Iow vapor pressure,

,,matrix spike,,). The calculaJed percent rscovery for each m.atrix spike sha1l be greater than or

EPA SANITIZED Page 29 of 77
: i ilt:';,-'hl'i i;,-ii; lr..ll n+ * it :.rlt;t i; r ;

(vi) Sa1gitfll-g ne:feSi1Cagl-1:r-i-11, I :;o capacity of l1rr; r;arnpling device niust be

\ / .------i- 

--& ' .' ,:

'jtestedarrdr.esu1tsreportedtoshow.rrndera1*'M.andwe1ldefinedsetofconditions.that.the. .l.],,,.-,...n':,.'.,.::t,,],:''

: 

- i,.i- 

, ...':. .r,r I 

,, . _. . ,

l

clwice is capabfe of coll*bting the ".* ln**i"*t in iglid,,liquid or vapor phase with minimal loss.

jlhe sampllng devir:e's ca-pacity (air vr-rlumo aird collectet{ analy[e mass) must be specified.'Fq,

l 

, 

, 

. , 

. 

. 

I 

. 

, ,' . t. .. ' . . 

.

inethor1sthatuseu,15g1b.ent:tubesastiiecoilectioil,i,ileciuJn;evic[enceoftlrecapa.;ityrtrrjstb,e

provided in the form of breakttnough testing. This testing rnust be rlone at a concenttation twice

.r.i a ;', a

the NCEL and uncler conclition-s similar to those pxpected in the workplace. Bt'eaktlrrough is,

,,.

definecl to have occurred w}er the concentratioU of the PMN substance in the.effluent stream is

"qo*l 

io 5Voof the concentration of thE ionrrent sffeam, orwhen Z}t!/oofthe PMN substance is '

detected in the backup section of the sampler.

(vii) Sampli tion

efficieney must be evaluated for the air sampling dwice. A mimmum of six air samples spiked

with the PMN substance at least the NCEL concentration must be prepared. A recovery of at least

75o/o must be obtained for each of the six samples.

(5) precision. The estimate of the coefficient of variation of each set of six sarnples from

::;?-.l,Es.ii=,srithec.ontrolledatmosphere*t paragfaphs,(c)(3)(v)or(vi))lpust"he.Jg6qxtriei,'-*iif,':eii#-i':

than 0.105, including allowance of 0.05 for error due to sampling.

EPA SANITIZED Page 30 of 77
ili l"'l' ,. ;: r, ; l : m i;. .ix,. :':ii'.:': '; t";o. t' : ;' i5 .lr:;; 1L;: ir 'l:,oi ,:tt'':tztf t ' .:tr':"t:'t i:..t':' l' )'5'/'t

o1i:irc estr'mated precisiot ir; ,1r'eah;r thao 0.105, #.:en the Compaily must re.preparc t"ile ,1!zrtii.x

spike, re-sa$plq arrd re-arLaLyze. a1.1, sarnples alsociaterl witii;ruchmaftix spikc or Lipii:ale

siuaples.

,,

recovely is requirgd, Cone?t for reco,very first by <tividing the observsd auoU+t by ihe proportion

. 

- 

.' i . . : " l

recoyered before detemining if mezisurerients fall belqw the NCEL. For eramplg if the observed

: :l ' I'.:J 

' ':'''' 

" 

:'

level is 30 rng/ml iud the percent recovery is 75%, use the value 30 mg/m3/(0.75) = 40 mglpj

;l l'-' 't'" '

when d.eterqIaidg wheper'the feyels are bglow the,expgsure limit .

(7) ReDreseiltativ*es... A11 iamrrle conditions used to develop the inethodqlqgy shall \ , -._--.......-...

mimic thb aetual workplace envir.glpen!'e. Xpected to b9 monitored. Conditions such as thq

.,,,

te6pe-r4ture, fugidi51 lig[r1ing, afld presenoe of othcr chetnicalq, etc. must mi4jc.the co. nditiori-s in

: i '-, i. 

. .. : r.'

the workl ace to be monitoreil.

' (8) Ctanses Affectins Validitv. If the workplape envirorment changes from the initial

conditions desc,ribid in ftrc verified qampling and analytical method in a way reasonabiy likeiy to

invalidite the accuracy of ttre method then ihe Company m.ust comply with the respirator

requirc@erits in the Protection in ihe Workplacq section of this Order, rmless the Compiriry revalidates the method to cotrfirm that the requir.ements for accurAcy and precision in paragraphs

(c)(4) and (S).are met. Examples ofpossible changei iriclude but are not lipited to: introducfion

of a new chemical.substance to the workplace which may interfere with the analysis of tte new

:,srn,:r+.,iqgffifoea};*:lm.ducioqoflight to the.workplace*rhich,may.inteiffiffiiadighrensitive PI-vII{

EPA SANITIZED Page 31 of 77
(,1) Mppjlorine&lqdialExp[su] q=

(l ) Generai. \/_.

. (i) &li*LlCyqL The ,'action level" is defined as an airbome concentration of the

-weightcd average, ec1ua1 to one half the NflEL'MA PMN substance, calculatecl as an B-hour time

i,

specified in subparagraph pxl). For nofl-8-holr wolk shifts, the action level is equal to one half

the NCELn. (The NCpLn is described in subparagrap-h (b)(lxii).) The Company may exceed the

action level withoutpenalty. The puqpose of the action level is solely to determine the requisite

monitoring ftequency.

(ii) Representative Exposure Groups. Whenever exposure monitoring is required

by this New Chemical Exposure Limit section, the Company shall take representative samples of

what the potential exposure of each person who is reasonably likely to be exposed to airbome

. T AY ,

concentrations of the pMN substaflce would be if respirators were not wom. The Company shall

*p.air-of at least one person,that,rc,lrresents;,'gnrl-does*noli;.i.'-i':fi.Ii1*ilr# ;i. . -

unrlerest imate,the potential exposure of every person perfonning the sarno or substantially similar

EPA SANITIZED Page 32 of 77
..?.4 .

i:;:r 

11 ':.iliocrii'e ff:o:lp") .jrh,,.o ;11:ha.iaiio e:'ip:rr.i+tc ite P ll] ir.r!,litani.i1 i1; flt23c1iabl-7 iihel;r io

ocor-i, Iho expor;rue of i:i.ch pcmon reerJ.nof b,jilsclf rlirr:ctly sauplcct i. :hat exposure is ,;:

,"pr.l,unf"r1 lly sarupling ilre L;".pur;ufe oiar;o[hoi per:sort iu I'.D saf ie gxpoijurj gtorp.

':|(iii) Gqod ti{prator11fraqtlq D-. $lmfuIds-, Determir:ations ofpotential i4lalation ' ' l

, _____-_.__:.

': ' r.,.'l. r:.,r, ' 'l .y'. .,... 

": 

-. .,,.

. flcpi sure shall be made dici:rding lo 'ISCA Good Labor.atory Practice Standardp a! 40 CFR Part ' .

. : I ...':1

.a

792,lil1the3irrhplingantlanaIytii,,l,lrnet1rod,]cve,loqcrl1:irisrraotto.subsection(c)oft}ri9}.{ew

',:'' i ', ---. ' :

.'CheEiea1ExposureL.jmi{s9ction,(celqaihpIqvi.sionsoftheTSCA,Gtr?anr|ic,.at}9to,,toxi9itv

itapplir;ablr: +o the. ItrCEI. requircui,xls.) I{cwever; conrpli;i:rcb wit]f I'SCt\- GLP is riot requirbd

where'e.rposLire monitoring s4mplcs or* un{lyredrby a laboratory accreditert by either: (A) the ,+r

,. : . '. : ,,

AII-IA II{LAP; or (B),another comparable program approved in advanie in writing by EPA.

.\.4ffi-. r :

iI-'"'/l

c6ncentrations shall be determined o:r lhe Qasis of samples representing the fuIl shift exposure for

,t ' l' i i

' a. each exposure group, ,

(2) Initial Moniteri{s. Befqre the Company may dwilte from tte respirator requifements

,]

of the ?mtection in the Workplace section, the Compauy shail conduot initial qrposure monitoring

to acc*ately detenliine tho airbo-" 

"oo"*tuution 

of the PMN substarce for each expo$ure group

in which persons are reasonably likely to be exposed to the PMN substaoce. '

rii..r,r* :.. . :.:r,tllr*ri*I.}srx.E${5+dnq+i&H-"sttifui}}ry4iD'.;rrl," ..- . , . +cuxr}:z!3tt*ii3ir:$,}$:&g-{..i1*EiirBxl":i:

EPA SANITIZED Page 33 of 77
EPA SANITIZED Page 34 of 77
r.r

. ,1,r; -.

': ',tt'i'iiii,,'' lri';',i){-;ijlii ;. ' '"''J- ' --.t- -

7i)' f cri tr r' I i aticir o t- t'1i',:;1iJq -.iil i l, \ _ / 

-i:j:-:-::-,...--

{i) If r:e,prcseirtalivr: siunples ta]tr;il rJ;: i ing the inilial t::lpi;sitre ntoititorfurg ievi;al a-n

'1

' :n below the action lwel, tl-rp Ccnrpany may discontinue n"lonitoring for that allbo]llccodcentratonbelowlne.acuonleYct,ulE\-U]llP.'rrytltaJulor^Jllllrr4vl|(,1

oxposuie group, except whei additidnal exposr.irc rT oritoiing is requiiqrl by paragraph (dxo qf i * 

, ^.t 

- , 

. , 

. .... .. 

, , 

r

:^r___-l.-l-:1._.'.. 

. 

.. ,,.,,,.,,:..i,,,-., ,. .. ,. .. 

. 

,.. : , ,

',,,,,- , 

, ,, 

, 

,r,i.'

. ,' . : _ . . '.

' " I '" ;'1:1 ''r ' : 

"'"' t 

"' 

- ' I 

oirborir" *rcentution,:is iod icaleaay xteii'n Ajsqculive miasureriiairs "

tlke.n aI leait 7 day$

' ; i:,:, ,i .'-lt,.. 

. 

.., 

' 

. .

apar.fi aIe below the actiori iet'el, the Co.,fiIpany fnaydiscglli1ge the monitoring tbt that exposure

,'1i

I ' group, 

'r""pi 

*t* ,aaitio"ul moqittiniog rs reqrtiqaa t1n*agraqh (d)(5) of t{is Nex Chernicat

Exposure 1-imlt section, 1gfiere the Pml substance is rlanufachir-edi procqssed, or used irr latahes l.'r I ., , . 'ir',:,,,.. .': . . 

.., 

,, -.. :.' .

.. :

of duratioil less th a4 7 .days,. the 2 consecutive me4st[einen-ts may b e takei at le,ast ?A hour! apatt, ",-*:*--.,=-..:.: :-"'r.- 

. .; _ 

,.;;.:,..,,,.r.., ,. 

, , .. 

,. 

', 

,,..

provided ibat the measur-@reots. accurateliiieflegt th, I higqF$ peak gxpqsur-es.and vanabili:ty ia

. ' : :.;- : l

exDostrre.

,

',.-.

(5) Addifonal Monitoliqs.

(i) For a pre-v-iously monilord oxposUre group, the Company shall, v.ithin 7 days

of anybf the wents listerl below in this paragraph (d)(5)(i), conduct the initial e,(posure

monitoring followe6 by any periodio or additiolal orpoSure monitoriag reqrrired by srbsection (d)

of this New Cherdcal Expos-ure Limit section:

ss.@)sghange-in the prgduction yolumee proeessirrisntfol eErippra{"plr-sonaet

or work practices that may reasonably caise new or additional expostues to thc PMN substamce;

EPA SANITIZED Page 35 of 77
'].'t -

+.

f i) l:.'ill ', ...,"tt", 'j".""t''"'; " ' c,r'r:r Lr ''i'rfuil,itl; t;coui if i' l: s 'i-''l ::ci:'::!-\i \.' ':'li!

..,..:,l,'1.j:,:,'.rcrlr.Iriii,lrr::+l]}:i]0lji!,r..::,,t1]l,l:.1',ii.l,;ililst;l,.ll;ac...i

1rI) wlelorcr elso fhe Cornpany has any i'easoq to sun^pe{'t a cha$ge tiat

may reasonably result in ncw r,:. tCtiiticnLrl exposures to tlic FlVllrl substalcc'

(ii) In no eve,rt i1 t11c aclditioae{ e.<posure monitorial requ1el.CIrt in paras4ph

(d)$)(i) intended to delay implcm:ntation pf any necessiry cleanup or othe,r remediai action.

Duringanyg1eanuporr9medialop9tationsth{,ma1occuq'boibrecommenqingadditionalex1.1ostr1e

monitoring, the Company shall ensure that potentiallV exfosed 

lersons 

u-se at least tle r3sfi"i tW

p.rateorron spelfied in sqqsgctionJ:)ft" f.:"T::f*- *j:t: *::""I*n? or more pTorective

,'. ,,."'.,.,'.1, ]"' ..':

respir4lory equipmeirt rleemed appropriate by the best profqssional judgm.ent of a qualifiecl oxpert

.,, 

,,:i'

(6)'Notifi9? o .

<r1 Wim 15 workiqg {ays after reeerpt of the lesults of any expQsure monitoring

requiied by this Order, tlie Qompany qh411 notifi eacl person wh6se exposure is represented by

:

that pqonitorirg. Th9 nofice shall fdentiS the NCEL; ttre exposure. m.oni{oring results, trind any

t " , '. 

.

co-nespqrdrng respiratory protection reguired by supqectipn'(e)' Afected persons shal be sotfqd

in writing either individually or by posting the information in an appropriate md acceqsible

location,

, (il) Whenever flie NCEL is eiceeded, the written notification required by the

preceding paragraph shall desctibe the action being taken by the Company to reduce inhalation

exposure to or below the NCEL, oi shall r.efer to a document aviilable to ttre person which states

the actions to be taken to reduco exposure.

. - . ,(i),Exerrmtion"basedjbr.Objsoti'iesata,*,Ufhere the Companyhasdqgumm{9ft-tigd, igrulqi.sE$,' ,r,+}i+

reliable objective data dernonstating that, wet under worst-case conditions, employee exposure to

EPA SANITIZED Page 36 of 77
(d)(lXii)), tneo that exposir-re group is cxempt frcni iiis lrIcr.r-Chr:r:riczrl l}'.posurc Iirait section

(except 1:aragraph (d)(5) 'liriititional i.1 rnitorurg" a"rvl su bsectiol (f) '"i i(;iil, Rei:ordlieeping") aird

the respirator requiroments in the Protoction in tfie $or$la':o sectiou of ihis orr]er'. Any such

',

objectu'', e data r4ust acounrlely charactedze actrlal eli?plcyee exposures to 'rfte PMI'T substanqe and

must be obtained under conditionq closely tosembling lte types of rhatuizrlsrproccssqs, go trol - "

methods. work Dracuces. and enviroaqt€o.tal conditions in the Company's current workplace

e data that may be useil to d€rnoqstrate operations with the PMN substance. Exarnples ofobjectiv

that employee exposure will npt exceeal the action level, gven under worst.case contlitiony, inolude

information on tlie physicat and chernicai prrcperties pt'the IMN substance; industry-wide shrfies,

and/or laboratory test results,

(1) Gerleml. Whenever tlte Compa[y has ooi tlducteal eripo$re monito.ring at a workp.lace

and the measured iri accordence with subsection (d)'of this New Chemical Exposure Limit section

airbome concenfration of the PMIri substance fbr any person who is reasonably tikely to be

exposed to the PMN substance by intalation exceeds the NCEL, the Company shall provide those

penlgns the respirators specified in this subsection (e) (rather ttran ttre respiratods) identified in the '

pmtection in the Workplac.e sectionof this Order), and shall ensure that the resPirators are used

(including training, fit testing, and maintearrmce) in accordance with OSIIA and MOSH respiratory

:3prre.";1,;lprotection requirqents at 2S-($i.&-{.9-riQd$eidi.4?gE&fg$;&*+tJl[hen the Companyhas notgg@;-$*"3,$*;14

. measured the airborne conbentration.of the PMN substance at a workplace in accordance with this

EPA SANITIZED Page 37 of 77
i: , ,-r ,-,,r,-...,.,-. -.. ..I.r,: i ..r,.,,r- r'-;t..-. :_.. :.r i,:,,r:-:i ..'

secticn, i.he Cq:lrrpatryshall qelect, 1;.'lvid.r:, rind ensuLr: ihat ilffl'sol]s -.r'ho illi) 1't)asiiri#ly lftely i;':-bc

,.'.]..'...,..'.'.l,I:,

' ':,, ]

/

correspgnds in llle following table tc tire rne.r,Srrred airi;r:ina concenlratiola (*,r itl:r1oie 1'roleqtive

respiiator r,vhich conespon<ls,to a concentration highet'than measured). i - 

, 

' 

,, f-,-f 

. .-- 

:.-". 

, ..* ,

''"'":-i: .].in.l.,.',,..],i

rl

t1 

,

:r:.'

, cffiv{}}rNerrrolhr x,A}rrirCu{,#ilt ANB.fr,S-ff.SF*Q-IiSS,SF-$liiAHle-B,I*aP-&lU

Comcen'trat[CIu, -

'of Fl\fiN Substance

* NCEI,

.''

: l0 x NCEL

i : ' i.'. 

.

(I) AnyNlQSH-certified pbwered air-punfiiUg re.spuator with a hood pr

i[f**i und with applopriite gas/v-apor laqiO gus, organic vapor? or'substatrce

specific) cartridges in corypin{iotr mth HEPA filters.

(II) AnV M0sH-certifi ed'continuous flow supplied-air respirator

equipped with a loose fitting faeepiece, hood, or helmelm Contducted:

(I) Any niiOSff-certified continuous flow supptied-air respirator equipped

*itt aloose fitting facepiece, hood, or helmethyEEL;

EPA SANITIZED Page 38 of 77
:]-

')'"'' : '' -'-i'

iriosu lir.ling far:epi+:r; ivi'lh ap[ii'u1.,,:i*tq p;as/vr:ritr (acl.ll3o, Sanic viwar,

cir srihstance spr;cifii) cartriclges it: .combiiuttio-Lr'with I{EPA filters, '

.,,

(III) Aly}IIOSI'I-.certifiecl contin,lous flow su;p"ptleat-alr respirator equipped

:

'.

({vJ rtniNllt::,:tr cerriij::f *:loi"L,qris florv srapplicc:aii- iespiratr:r , ,

ruelurtitdf*erytq,,WWt Ei :,

(I) tury'NIO SH;c ertin eo co olis ftgrl s urp p lied'air respirator equipped

'.'r,vith.a1oosefittingfuccpiece,ho.ot1,or.he1mct..,.,

I (II) nry UI0SI{=ceititie'd nefal]ve pr*ss ulrcr (demancl) supplierf,*air

i*tpitatol equipped with a full facepicce. ' 

'

tf\qls 9 .P * 50 x NCEfl, qc&fuTe-ttitt*-W.b4

t:. .:..

,, 1 .i r' .i

| ,-

(DAoy'}JIoSH-cer-tineoni,ryurffingfu11facepiec-,-*n,Iljl;;:;r#lj

#itt appropriate gas/vaBor (acid'ges, organic vapol o1 sub

*urtriOges in combination withNl00 (if oil u*tqto]: *:u3t), R109, or P100

filt or an,appropriate canisterircorporating N|00 (ifojl aerosols abseuO;

(U)A"V NIO SH-certifi ed powcryed ai1-p urift'q g'respirator with a ti gh!-

fittirg fulI facepi*** *qrippea wittr appiopriate gaq/vap0r (acid gas, organic

vapor, or substa4ce specific) cartridges in combination with HEPA filters.

(III)Axy NIO SH- certifi ed negative pressure (d emand) s upplied-air

respirator equrpped with a full facepiece.

(IV)A-ny NIO SH-certifi ed cortinuous flow supplied-air respitator equipp ed

with a tighrfifirqg tuIl fbcePiece.

supplied-air respirator" equl:pped with a tight-fittrng fulI facepiece.

EPA SANITIZED Page 39 of 77
(II)A.n;, t'UOStI..certilic+t c;ontinuoliri flov,r sr'i6iijplied'min respi::ator equipped

r,r,ith a iilqhi..flti.ing Juli r'irr;;pior;e. ,

.1

(irI)/nyhT1osI-I"c.i.l,i.iitict.i1;re:;sure.r]c;na.ltdor.oLherpr:sit.ivcpreSSL1remci-lc

..''.,"..i,,t,pliert-aifrespirato'e,1i'ippedrruithdtight-flttingfu1i.facepi*'*. f !a _ :r. 

. r .

l

.;.r .. , ,. : . : i l, , .,. . 

,

:i:,(IV)A11yNIoSH.certi{iednegativi..p.rQssure(denrand)s9lf-contairref..

''':'''"-'i

. : :.e.. r-...:,",".f r..:1,... -j--_. ,,, 

";.,:. 

,

=roo0,qNipt' -lrpqbSq44c,?&twr"iirg;iEtW', Asv-'"lryeWl '

'- : *,.' 

, 

...1,,

(I)A:ry NloSH-cert!fierl powered air purifying ftll facepiece respirator ' equipped with'au appropriatq gas/vanor (acid g4s, organig vapor, or

subJdirce gpecifig) car,hidee'inl comlinatiorr with HEPA filters'

iit g-l"la ". tplnet trpi is Auipp"d ;'itt a ufo1op"ut1gas{yapo1 (qcid

gx, organic vqpqr, or duistmce s?egific) 9ar,qi4ce in gomlq{i9i^wio

greater,

i:

(III)Any NIOSH-c€rtifi ed continuous fl ow supplied-air lespirator equrpppd

. 

([1/)Any NloSH-certified continuous flow supplied-air respirator

erqulpped with a hood or helmet With evidence demonstrating protection

level of 1,000 or greater.

(V1a"V NfOSff-certified pressure-{emaual or other positive pressure mode

iuiUiLd-air 1espirator equipped witli a firll facepiece.

IfNo Cartri&e Serviae Life iesling has been QpnaueAd;

EPA SANITIZED Page 40 of 77
> 10(}0 x NCtrL

(ruax. 1SrS00 x

(it)Auy l..lTOSiJ-r;i;,:iifir# co;:iii rr.i,rr.ti; .ilc.v,r sitia;li-it:;.l"rrir .r'i:s1'-:ii'ato:r r.i1u-i'.pi;eel

r,vitli a hti,,ii r:r hcl iaat tuitii r:riiie;:crt ie tncrnirr.tiin,t4' .;;t'oter:tir:tt le:;cl of l,A{i0

,', ', 1y1'75; , . ,, :.'

a

(III)fury l.{I0SlI-crrrtifir-:r1 Jilesrjuro-clornanil or othcr positivrl tr)l"nssttirc mocle

surppliJm*gir 1i:)s1lil'ator eqi-ripped .,vith a ttll fireepiccr::. fprorr ldes eye/far;e

'F OSI{A h;rs assiE,rccl ,\PFs of 1000 j:'of certairr tyires of hoof"3yl.hr:imets,lvith fow-qr1d

ail pLrriiyilrg; respira.Lr:r i; (PAP.I{s) or strpplied.air relP_irators (SAlts) rvliete lhe lanufq?hlrer

canrlqrnonrt.ate ar1*quate air llor.vs to rraintajrr positive prosstre insidc the hoo{ Srlelnt*t

in normal workin[ conditions. i{o-wever, t}1e employe.r must have evidence Plov-ided b1_!e

respirator: :rrraulfactur:cr that thc tesfing of thesE respirators demonstratcs peqfuryance at a 

.

1eveIofpiotectionof1,0006rgieatertoreceive*lAIq:jt..090.Thisleve1of,

pe.forrrince,'can best tre clemonstrated by'periormiog u Workplace Protection Factor (\YPF)

'ir Simulared Wor(place Protectioh Faeto{(SWfEl study -o11luivalent teqting' Without

tesiimg rtnta that *emnonstratcs alevei olflote.gtiou o"f.l:000" or great'er', all P,AFEs arld

,$Alds-with trrefunets/hoods ar"e fo be treatCId aS ioos+fitt-ftrg facetrrie*e respirators, and

I ..

Any 1li$SH-ccrtified pressure-demancl or oflrer positive pressure mode

(*. gl, oper:/closed circuit) self-comtaimed hraatfui4g allparafus (SCBA)

,'

(:) Redfrctipqi irl:+elpiratlT prqtectipl. After appropriate respiratoryprotection has'

been selected based on the results of actual exposure monitoring conducted at a workplace in

'tF

accordance with subsection (d) of this New Chemical Exposure Limit section, the Company shall

tion in the'WorkPlace not, at that worlqplace, use the respiratory protection requifed by the Protec

section of this Order (unless it is the same as required bythis New Chemisal ExposureLimit

section). Before the Company rnay make any reduction in any respiratory protection selected

pursuant to this New Chemical trxposure Limit section, the Comp?ny must veriff, by 2

appropriate in accordance with palagraph (e)(2). \Yhere the PMN substance is manufactured,

EPA SANITIZED Page 41 of 77
,)rl

' r I -.

(1) Sirggj aLE1} +pJ.i-g1r,,, ..

(i) MgaUfqUfejliq_Qg1t5C_qllue4ili[rgglgniis, When a rrirluc ler+s t]iair the LQI, cf

aph (cX4xiil) t:i ineasu.i'et1, i,'rc Comirany sha1l the aria.lytic*l rnnl-hori (as describe.J iri pa.ragri

estimate potcntial expos Llrc rrsin;; gcriorally cstal-:lishecl ancl a,'cepterlstati.stical t r l ethor-ls. If the

l

Company obtains an exposur* or.onitoring sarnple that is mote than 10% above the aptual IJQL of

the analytical method, the Compan5r must ellsure that its workers weaf at least a NlOSH-cer[if,ed

supplied-air respirator operated in pressure den'rand or othcr positive pressure mode anrl eqi-rii:ped

with a tighf.fitting fgll fbcepiec.e. Arry re<lnctions in this respiratory prr:tection musf cornply with

pTagraph (e)(3). The Company may submil im lrnprovecl analytical method provicled that it

complies fuily with subsection (c) of this New Chemical Exposure Lirnit seotion, including th-e

j. .. /-\/-\ verification required by subsection (c)(3).

(ii) Clbdntrp and Remedial*Actiqqs, During any special oleanup or other remedial

,actions that may occur befor€ oommencing additional exposure mbnitoring (as discussed in

paragraph (d1sxii)), the Company shall exsure that potentially exBosed persons use at least the

respiratory protection specified above in this subsection (e) for the measured airborne

concentration, or more protective respiratory equipment deemed appropriate by the best

professional judgment of a qualified expert.

.,,.r,..,..].r.1 .:r'l;a-i:+ri''--tli,ill'i-i';'':'*'::i.-*r,;a':'.':;1'.3'-E:.1":.rt't'..'.,,-. ... .1, .l .i t, t'I I i;t 11.--. :,-i. ,' i. .-q -;; :'.1-':.'I:i',+j !'ii : 'r r-'

EPA SANITIZED Page 42 of 77
I

:-'r, ii,,,-... ..,!..-......".----

i-. ,' .i I - .t, ,';, i..,i:r.-ii,ri .:, ,.,, ii: ; i ! .,li:

C.r-clei', ihe Cornprxry shail fiii,iirf-ain i.hc ii>llowing rccurit1s itntil 30 yoerl:i ai'i.er ihe tlate they ;iro

.i'i:'

creiit(;cl, anrJ sha-ll mi.,kc therr., r"rttlltir:le fi:r inspection iinrl cupyir'.g by i.iliA in accoi''.lance ',vith

verific;d.ion results obtainecl by both laboratorles; ,:

,..:.' r . .' . : . 

' ': : .1, 'i '.'

' : ' " t 

i J I '''l

- .r '..'i .

,l : , l:r' .,'^, 1 ,,. . ,.,, 

,- ,,.

requircr{nenls:of subsection (cX3), incl*rtin,g, iopies of the pignecl'certilicalion ititetnent and the

t:

t ..

(iii) Records documenting either compliance withthe Good Lhboratory. Pr:actice :.., ::_, : . . :...: .

.'.r'...

Standardsat40CFItPart,7g2,oi,*,*ofalabofat0,ryaccr:edi1edbytheAIIfAoranother

:

1

coqlparaore program approved in advance in writing by EPA Where the Cornpany plEcts to not

'i: t ('

cornpty with TSCA GLP, such ricoids'*hull include the wriuen accreditation frorn the AIHA or

l

;

(lv) Records documentihg all'exposurO monitoring dates, duration, and iesults of i

I

each'sample taken; 

,'

; 

(") Recordq docurnentinl the name, addrgss, work shift, job classification, urd

work arzaof the person monitored and of all other persons whose expo.sures the monitoring is

intended to represent;

, : , , , (oi), r{ny,conditions,thatmiglrf-;have affected the monitoriag resuJlsir .:,*ii.i, .,..tirirtui,.'r,(i

(vii) Notification of exposure mpnitoring results required by paragraph (c1)(6);

EPA SANITIZED Page 43 of 77
.. -) ,i

RISI( NOTIFICATION

-

,:]

. 

. (ix) Reoords clocunrci.'tiag any s,pills, ieaku, rup{':rres q:i othel breakdollq tha't may

,, ,: :

causenqworaridiri3nalexp9$uIP;......;,,.',',.,. t'

' t*f . 

rtc type ofreslirurvr,rytbi!'J a"'ioes rvtim"by,pelolitmed personlif ?oy':

.:r: i -,.' '.,t;.1 :'.;t.,,.:'....,.' ,'. ' .' .'. ' .::,'''.'

,i !. 

. 

' (xi)r Recorrls'tlocume$tlrg ?ny abtiols taken to mitigate gxposures to t1i9 P...l,v$ ' 

.. 

.

, 

:,' : l ] ., ,' :,:,

suUstanoe; ' ': ;' ' ' :"''"' ; . r ' ' 

. .' .' ...', .:'., i

: .1',:..' (xii) Records clocunienting lpliaiice on tle objective data dxemption in paragraph

: (dX7), in;luding: (A) ths sourae ofthe. data, (B) prgtocolg zind rcsu'lts of any relevanl testiog or

.-,"'i.';.. ." ' ,....i . ".,;1.. '' .'. , ... " '1.. : '

4ualjsis,(C)adesbriptionb[ , . i: ,i .: ' : ..., .-. .:. ' -. .. :.

expqsures wifl not exceed t]re actibn level; @J other data relwant to (h6 operatigns, halerials and '

' ' '., . 

't.: ,., : . i. . 

, .l i .. :. '. I 

. 

- I : , t r. ' :. ..,1 

., 

:1 . ..

q-plgy"qixposurps,rollplrbvE."i*rX"o. 

,, 

,., , . 

. 

,.,.r, i, ., l,

:

r ,t ) - ----- - ^izL!- ,^l-l ^- +L^ /anmrqo?i-r l-er.

(a) If as a result of ihe test data requiiei under the terms of this orde1, the Company becomes

aware that the pMN' substance may present a risk of injury to health (or is so notified by EPA), the

against such risk, into a Material bafetyData Sheet ('MSDS'), as described in 40 CFR ssction

721.7!Z{c), within 90 days fr-o* the time the Cornpany becom.es awaro of the new infbnnation' If

EPA SANITIZED Page 44 of 77
(b) The Compatly !+ust ensrre that persong wf,o wi1l r+):eive tlie PI@{ ntrlistaur:e l}9m the

. date the compar.y lecomes u**e nf th" o"* intoqlalio" ux"tibert in palaglaph (a) of this

section, are provided an MSDS containing flre infornation .requiled,updu paragiaph (a) within 90 : -::-'--, ---,I-- --.',,.,.,- 

.. . ,i.: ..,-, ,, : . 

.. ...: . 

-: 

.

davs froin the time the,Co;p*, O"*-i u*#lof tt 

" 

nq* infoo'utiop' ' ' :

,*FJY*Y.9:i:l:*:.:::.:.{-i.i:--_-:::'-1.i:,:.].,...r.,.i,:

i,

RA}d :: , r HffilI-C:WIs-UH[0Str:QHrY;ffiH"-*:=::

(u) UatrcsJlaraa ,!ie;t"-4*''v,tnu['a"v"top.aq4i-!leqen;a . 

: '

. 1,. .:r.. 1;--., i.,..:..,: ir I 

.-

. writtenhlT{d *ryTitrq Pfrgraur for the.rMlri subgtancl. ineaoh 

-w-o,ll 

la:P:: The Entten

. 

, :progparn willjat a mininumrde.scrile ho,w the leguiremer.rF of this section for l1bels, MSD!+ and . 

;

i :'. :; .' .',". . ..,'., ':' r_: '':1i: ' 'l : 11 '',' '' l'l i

t l-. .:'' .,.. , 

r: 

..r ',

communicatiou progran available, upon reques! to all empioyeesl cqnhctor employ'e$s, and their

desrgnatedr****.*";G;ayrervonanJ,*r**a"ffi;:'

- 

prograq, including an exiqting pr-ogram esfablishtd under tle OSIIA Hazard Cornmunication .

Sl4ndad (29 CFR 1910.1200), to oomply'with this paragraph povided thpt thd existing hazanl

com4uSica6on prograo satisfies the reqpireurqts of tfis section, The witten program sha[

' include the following: ' '

(l) A list of chemical substanc€s known to be prestrrt in the wqrk area which are subject to

:.;r;,.liilir':ia..1rs-GA&riotiqa.5{ie.}@onsent order.sigrred byJ&psornpany;qq.to.eflS@&ispr$oEfi@X4 SNUR al . .- . - t.-+

40 C1F-part72l, subpart E The list mult be maintained in each work area where the PMN

EPA SANITIZED Page 45 of 77
(A) A statement of the health hazards(s) and precautionary measure(s), if

any, identified either in paragraph (f) of this section or by the Company, for the PMN substance.

(B) The identity by which the PMN substance may be commonly

EPA SANITIZED Page 46 of 77
i i'. l

CD) A staternent ol'exposut1 anl firccaltionary measurc(s)' if any'

itlentifietl either in paragraph (f) of this sectiQn; or by &e Cornpany, for the PMN substaflce'

G, Th,: Company m.ay use sips, placmds, pror.:tlss shects, batch tickels, opcrati'ng

procedures, or other slch writt<n ,utoialr lo 

1i"u 

of affilrng labols to r.flclMdua] statiorratyprocess

co.ntriiners, as lotrg as the alternative metnOa 

ldenUn"s 

th6 conlarners to ,which it is applicable and

conveys irifoiiriation specified by subparugap.h (b)1rxi) of;this section" Any writtar mateiials

must be readily accessible to the employees in thqii wolk 4reas thrwghorlt cach work shift'

(iii)- The Company-need no! labcl Uortable.containers inlo which the PMN

iliate zubstancC is hansfened from labeled coiitaintrs, antl whiqh ale intended only for the imme

use 

'of the employee who perforfiis the transfer',

(,v)TheCompanyshallnorremoveordefaceariexistirigla.beloncontainersqft}e

pMN substnce. obtaine6 toq per .sons outside the'Company unles's the cofiainer is imme6iately

relabeled with rhe information specified in subnaragtaph (b)(lXi) oithi. .*tioo.

rll e,nsure that each container of the substance leaving its workplace (2) The CoinPanY shi

for distributioa in commerce is labeled in acconilance with this subparagraph (bx2),

'(i)Thelabelshall,ataminimum,containthefoilowinginforrnation:

(A)Theinformationprescribedinsubparagraph(b)(l)(i)ofthissection,

(B) The name and address of the manufactuer or a responsible party who

can provide.additional inforruition onihe,substanre.for,hazarcl evaluation and any,approPriategixrn,*r1 {ii':!:.'-'r!;;

ernergency procedures.

EPA SANITIZED Page 47 of 77
,1--

{:i) 'lhe labct; cr aitcuurtivc Fcmrs of warriing, si all be legiblc and plomincnily dispiayed.

,.,. 

. 

... ,..:.., .-.ll i; ,.' ,t. 

,..,.

: 

. informt,iion may be rr:peqt,;d jn o thei' .ringuages.. ., '

,; 

,,, ,,.

. 

. ,t , ,t :., , ..

." (5) Ifthc label or ultornative iorm oe.waming is tqbe applied to a miilu're oontaininl; the

,i .'., :..''j., ,, 

.,, ,'., :' .-::i .. 

1

: I ' , PiVDtr substanco in conibinaiion w-itfi any gther substance that iS cither subject to another TSCA ' . 

.

, ....1.. 1. . .' ..,:-...', i

:; sectio.n 5(e) Orderapplicable tq th9 Compaliy, oisutje"t to u TSCA sbotion 5(a)(2) SNUR at 40 - -.l

' 1--- ' ll :; '' :j-:i

..:af.RPart72l,ryb,partIIordefinodas,a.h,4zaidotrs.clii:riiica1',unde[ttisoSHA'IJaz;id.',.'. 'il' 

..., 

,, ,,,.ta 

1 ,', .,., ,, : .. 

.,- 

., 

. . 

. 

:'. 

.

' j 

cornr,il*icrrtiori standaxd (29 cFtl lr00Jr001.the cqmopanymbypiesqibeoutrr'e lairel,.M$l)-s,

,',..'.,'..,.:..,.,

* ult"-ative forrir of warning, the mi)asures tg contrpl.Wor.ker'exposure or -e.nvirqnmental reieAse .

: . . ,. .. :..:. '

'-: 1 tr: ..,'i..,,''-' .,.;'., ..'.:.1l"'1 ,' r"'-'1 ."'

. . 

.. ryhich.the Company determi-nes pro'iride tlie geatest degree oiprotection. I{owever, sliould thgq . 

.

,':

. conhblmeasures differ $om the applic.abtre 4geasrlres ryquird un{er tlis Order, $e Company m}!t '

- seek a d*erriiiation of equivalenry fot gucfl alternafive co:rtolmeasures pGtdt to 40 CFR ' . ]

';-. i..'r: 

.,.,. : ,', 

',i,.,.-,n.,'... 

,

'. T2l..30beforepiescribingtheilunderdrissubpriragraph0)(r, . .

,', -- ,- ,-.

. hazards of the PMN substange or ways to protect against the hazards, this new information must be

I .:

added to the tabel witlin'l montlis frbm ttr9 tipe thi: Company becomes awarsof the ne-w 

I j :

information. If the PMN s. pbstance is trot being man-ufactured, processed, 01 rised in lhe '

,.

Company's workplacq the Company mirst add'the new inf<irmation to the label before the PMN

';r+:..,,r1",-isubsfaixse,isreintroduced into thc Wor&ilaBecae4.111f';.1i'5'14:'ri''i1i;;1;1'r:*t$@;*+s,-- ' - -'', r"i*ir*$rrIt

EPA SANITIZED Page 48 of 77
i:-\ :"r "

of this section,

: . (v) Sigus and symptosli of expouur', an{ any medical conditions whigh are

,.',.r :, i l

. .' Sectea to be aggaval.d ty,",.lp",..pre P ai,f.pq +rti{fa"e krrovm to the Comlranv : ' '

':

fY-iil pren+irqa.y lh*at*o to,<nnnolwprter srtposure aatUor env'ronmrxrtat ,

tl

release required by this Cirder, or at+atye co"tol'measures which EPA !1as detemritred under 40

.-,,.',

CFR 721.30 provide substairtialllthe sarne deer. oe olprotiection as the idixrtiEed contol mqisures.

(uiii.) Any generally applicabie prectrutions for safe hrindling and use of the PMN

substance which are lnowi to the Company, ;lslu6ingbppropriate hygieiric prirctices, protective

tsirirj;ru.;.-,ime?sdres:ifuiingpcpdifiagfl,.maialeoance of contaminate4pq+lpwgatrdvrtroriedlIp-$$qilsspcnsg--.

,**,i

to spills and leaks

EPA SANITIZED Page 49 of 77
such;:,; aiipropiil;tr: e,ngin+crihg rn'-rtrois, ; :tk p:Li:c'icli, ci 1;crscrral i:'':':iectivr; c*iuip;igr^t'

(x) Lrrergcncy firl:t aid proicdure*s knov'n to'dro Conpany'

(xi) lho tlate of preparatioir qf the MSDS or rrf its- 

]ast 

rcvision' 

,

(xii) lhp nane, address, and lelephone mrmber of the ComP4nl ol ano*o 

,

: 

. iesporisibli parlyvho can provide additional iuformation on the rhenical substarroc and,any

,:

, appropriate emorgefl oy' pro cedirres.

: 6):ffnoret". i* iofor-utiori is founri or'}nown for any grven ca-tegory oi the MSDS, the

': . .'_. - ,. 

: :' ,,' 

' - , . 't, ' i' : -.,.!': ''"., ,: : :,,,,.

, "orrydrt-*ttteMspstoi"iiralettitaoaee:icablehforh"tio"wifoild" 

,, 

,, ,, 

'

' (r,"; Ae "n"nisA 

irgrqdi*tt *" 

".S*tiaf 

ry t4" yne b.ut tlq sPecifio mpoiifo" v*igg'l* . .

. mixtue to mixture) and similar hazardsi,th g cbmpanymay prepare one MSD-S tq apply to all qf

i

, :l ''. .:' I :, .,,1 ,.: .,".... .l

, 

- .'t :. . 

, .' . ,, ,,.t .'. ::., :-.- ..,, r,,,..: i.

hriaards of thp P. MN zubstance or ways tp protect agarnsf jhe hazardi, this nevv rnfonn+fon mrrslle

.:'..

aililed to the MSDS wiihin 3 months ftom thb timg the Company become,s awaiE of the new '

l-:'':-- ''-:-.i 

-:--- 

--': '' ':"'

.,..'

. iinforination. Ifthe PIrdN Substance is not be+Ug -iiuf*toi,ud, prccessedr or used ih the

company's wortcplace, ttre comphy mirst adtl the new infonlation to ttre MSDS before th9 PMN

I

substance is reintroduced into the wor[plabe:

(6) The Comparry must ensure ttrat pers0ns receiv'rng the PMN substance from the

Cgmpany are provided an appropriate MSDS with their initial shipment and with the fimt shipme,nt.

after an,,MgQsrisrerjgo&ifri provide theMSD.S.uaifhrthclsHPpad+$EiBd'x!tuEc-ryiaiaa.sr

confairr srs 61 5eral it to the person prior to or at tlo time of shipment.

EPA SANITIZED Page 50 of 77
^ 'ire lv.!$,";;'i ii-r itc ''r';ii;plaie, anrl mu;t er:er'r: (i') 'i'he Co:npa:iy l i")t me'i'flJ; r' t Ji':: ! rri'

i:i ir t,c:.k r'ieai,.

itrat it is readily acses5ible d':'tirrg sach vrqli( iidji 'i ) t1' nlt i !$tts 'i'licl i'iey ;ue in t-

(3)TheMSDISm*y,t,.,kr.rtinanyftrrrn,inclurli;rgal;operatirrgpioceclrires,andmaybe

.tlesigredtocovergroupsof.substarrcgsinawor.kareawh,*oitmaybemgrealFroPri4te!oaddress

.:

tlppotoo'lazard;ofaplocesqrathertlranindividual,substalces' I]oyever,1.n.allca1r.thg

" muqt bcirrovicted for the PMN sub$ta iice anrl must bc 'rcadily accessible

requred.uuormalron :

.,''

durins each work shift. to er-nployeeq when ttrey are in their work areas'

: r."r ' '. j;, ,. , '.'. ':r'r;

(9) Xhe MSDS must be printed in Elelilbhowever, thq inforthation pay be i:epeated in

,,,

: ' ..-.. t---

tal pgBlqvsq 3nt1 

---rrabEq 

The Coupany must eniure thal employees are provided

1.'

with,infprm4tigrr and trarrririg oa the PMN substaq.cgl' This informafioq artl qaining must be

provirled at the tiue of gach eimplbyeels inltia assignqent to 4 wgrk 1:" 

*1|"*.t ": l.^ 

.

ifirst tiniq.

(1) Tlie informatiqn provitled to ernployees under this pragraph shall inclqde:

: (i) Therequng@gtrEofthis slqqqon

(iii)ThelocritionandavailabilitvofthewdJtenhazardcommrmicatiotrprogam,'

required untlerparagrap! (a) of this sectio:r, iricluding the list of substanrces required by

subparagraph (a)(1) of this section and MSDSs required by.paragaph (c) of this section' '

(2) The taining provided to ernployees shall inolude:

,.{i$e,=,rrrr.iii*.\,*-(i)Methodsagd&}EBc$Pti{in8ffiatniay;be+sed'+pdetectthepresenceg{releassio&Efilio;1'E*"t$-3i

the pMN substance in or from an employeg's work area (such as exposure monitoring conducted

EPA SANITIZED Page 51 of 77
(ij) T'.he i:ofilntiai hn:i,; air. iroalth Jia::ar+is ,',f tirr; l]h4r-i'i sr-ll;sLance EIj si,ccilierJ in

pa{irriraph (D oi'this sc;ction.

(iii) Tlle measrrres emplcyees ca.n take lr; prr:'iecl tltt-':r'i:r;e;]ves anit the envirot]-'ilrent

i,

Ji'orrr i.ire PMN substancc, incl,ldlng s:1'rccific procc,Jures iltc tlo;trJiilny hi;r; iiriplorncirit:d to protect

employee,s and fhe eir.rirorrmeilf -l'ro;n e,tp,rsurc to ilre P]'.4fi sribstrmr;t:, .inclurlin;5 a.tr'i1.,r;priiite worlc

;

practices, emergency procedures, personal protective eclu.iprtcnt, engineering controls, and oth.er

measures to control worker exposure and/or en+rironmeiital release required under this Order, or

alteinative con,trol measures which EPA has delennined unrl,:r /10 CltR 12L30 provide the same

iiepgee of i:rrott:ction as the speci,fted contral rneasllres.

)i(i") The requirernentS of the hazard communication program developeel by the

.,

Company under this section, inclnding an explanation ofthe labeling system and the MSDS '

required by this section and guidance on obtaining and using appropri atehazard information.

(e) De Minimis Cciirceritrations. fne require*.mts o1 qls Hazard Coitmunicatioq section do not

appiy tq qua[tities of the PMN substance ftat are (1) preserit in the work area only as a mixture

' rmil (2) at a concentation not to exceed 1.0 percearl byweight or volume (0.1 perce,lrt by weight or

volume if the PMN subsiance is identified as a poteirtial carcinogen in paragraph (f) of the Hazard

Communication Progrim section of tlis Order), This exemption is not available if the Company

has reason to believe that, during intended actiiities, ttre PMN substance in the mixture may be

;smerris:r,ftcslidsitralp&abp. re.ihe 1.0 or O.1 percentJeudl:erlirheilea'4pJies*@his&dercontains (1)

New Che,lnical Exposure Limits provisions that speciff a NCEL concentration less than the dc

EPA SANITIZED Page 52 of 77
,,, I .(0 llunranHeAth, linqroarqcrllalX aUgO ls. Tle 

. . 

,

. followiug hunian iicalih ani envjronmcntal hazar:.l and,ptellutionary stalcrhcdts shall appear ';r.r .

': :' ' 

"'"::t: ' ' : 

' 'rl . .. .

Ieachlabeiasspecifiedpparagraph(t)an<ltheMSI)Sa,.p*cifi.di,,p*agraph(c)Oftlrissr:ction: '

j,:,(1).Humanhealthhazardstatements.Thirsubstaflce,inayfduse:

J..,,:','j.;.'',,',,..''.ll

'. 

,. : -.. ....-.;. .. li 

.

: li) skin irritation. r.. 'i. "" '.':.' ;

. \? "-r*- l+.+Yl*-t. 1 ,. .,.,,., 

l

'.,.:' I ,.:.,., ,:

, . 

', 

lii)9entrAnervqus.system."tr"..,]",tl ,,,,., : . .t i, . 

', 

, . :

(i) avoid skin costact. 

,

,

' (iii) avoid breathjng the substance. :

I b.lo* u, 8-hour rim e-.werghted averarge 9f 0'03 mglrri3'

,...,ar*,r.,-,4S,),mr*.amqi6lurrdd+.rem,utio:rary statema.ents. No.ticejo,'.rrer.s$:;st'nrei"FtlE?4Ei-tt!iil,.!E#dl+!E:f,J+e-'--

(i) disposal restrictions aPPlY.

EPA SANITIZED Page 53 of 77
:i '. r ,.. . 

'. :. '.:.. I ..:'.,,,, .., , .. :.

' (S) Exi;iins l{azdril Cor,U&mica.1iolt rrig{.U[",:The Corr,Farty.ngccl not take adfl{!'oUal actions if

;:,..., 

.-".- .--=l i --'t;,.'..,. ".,'; ,i:r.,....:. ."... ,'' .-'

t 

, oirtiog p.grarns and procedures sitisff-ttrfi feq,$rementi of thiS sec.Soli ' i' . ,,^ r, i

' ' ',.1 :... 

, 

.

,:'. ' . ' ' '.1' :'':',.:'. . li ' ,. "' . ..'.'

,:PMNsubstancebyauyot1ierpq#oni]::,..:

, ' ,,,,,, ,:i:'.

. (Z) Sirnsetlollowing i.Ng,R- S"bp*rc.4ph.(r)(1)'+rq efiiire 75 clqys, afterpromulgation 

. 

.'

_ 

j '-.::,,;"i'.,.,:.... .. 

1 ,, ,-' .' ll ,,

.ofafinalsigiffcantnewuserule(:SNUR':)ggverningnhePMNsubstluceundersection5(a)(2)

: of f SCa udess the Compt y i. ootil"d on or beiore thal day of an action ir. a F erlerl Court , 

'

" . :. - ' , ' : . I 1 

.

. ,: :'.: :,^ .l

,sgekingjudi{alreviewoftheSNUR.Ifft9Compau,4is,sonotified,subpragra,ph(a)(1)shaltqot

.,j,.,'',.,.....,,,,1

SNUR have been resolved aad the validity of the SNUR affirmed' '-l : ;

:ill Notec ,tSlUn. When EPA promulgates a final SNiIR for the PIVIN substance and

\, _--:r'

gubparagaph (a)Q) oxpires in accordanc6rvrtl subparag€.ph (aX2), fte Company shall notify eac

person whom it causes, encouragds er sugge$ts to marufacfure the PMN5ubstance of the existence

i

EPA SANITIZED Page 54 of 77
:-

(1) Noti4, in writing ary Pers;-r : 'I .:,: l

. 1.. :.

' a ,' .r':

issuance of this consent orderunder secrlon 5(e) orrsce,lhe P,MI-I *"bstance is sublectto the

export notification requirements of rsc$ section 12(b) and 40 c-FR Part 707 subpaTt D' such

notice shall contain, in the fo1u-fo which it appears in this consbnt ordet, the following 

,.

information:,(1) the ph,g*{ nurnber, and (2) either (A) the specific chemical identity of the PMN

'l

substance, or (B) if the specific c-hemical identity is confidential, the generic chemical identity'

of further distribute'th* PMIN substance to any other person, other than for disposal,

1

'.*: ' tpletelYPolYrrrgrizerl' until afr.er the PMI'{ substance has been corn

..11::: ir::i.;,:,i, r , (3) , campry with trre.. same recpiiremenls a rrd :tesfrictions; if,zury,r'recluirerl of the c0mpar'-y

in fhe Protection in tJre Worlqplace'

lnternet Address (URL) . http.//www.epa.gov

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EPA SANITIZED Page 55 of 77
;

UNITED STATES eTVIRONMENTAL PROTECTION AGENCY

, OFFICE OF CHEMICAL SAFETY

(,:) ll-girti.rrf-.,.fy-lrarrE:<:1'li r'.rrd.$loli1::c." }'ic it'viriml:Llri ir ilj l;aialJraph (b)' ihr: iJotr4ial$PFrf|LurroN PREVENrroN

iiisiii!;utt> tlu: PMII subst'i;;luc out'j lr'lc tlro ( 'ompix'ty li'"' tOr;]pt)raty tl anq;';if ar'il stola-[l{'' in s!'LIcq

.. ' : .1 .., ', ' li "'

,rrltiiliito.rs provitlcrt L\c f'ritrt"itrli tl'icc l'dir'l"lil'io:1'; I'il)'rt'14"t:

(t) Subscqualnt,!o auy srrr:ir cxcr:t.tt tr...:"111;t;1..r 7 ,:rnl} 5P0It 9t stoJ:.l8:: ()f :,;:)aJCi.i i.;nti.,iljc,.s, ilrc

-:. ' ,, . 

. .1 :'

PN)IN subsiatr;emaybe dislrib'uied only qq t[e ComF.,+Y or aPcrsorr who hzis gi-ven theCltnf aaV

..

the writterl agreernent reqriirctl UV patugf'pfr G)' , 

' I '. i

containersandrcmovingorwasbipg.outthePMNsubstancenrayoccuronl,ywhileflrePi.Vlll

substance is in the possesSiOn and conhol oftho Company or a person who has giveri tlre Company

(3),ftesealedcontainersmustbelabeledinaccordancewithpmagraph(bX2)ofthe

Hazard Communication Program section of this Order'

(d) Recipient Non-Copoliance. If, at any tirrie afte,r corrmencing disdributiol iri coumerce'of th€

pm..{substancqtheCompanyobtaiuskrtowledge,thatarecipieotofthesu,bstancehasfailedto

*r"ely with any of the coaditions specified in paraepph (b) of this Distribution section or,Jer

' 

new use of fire pM.N substanoe (as ilefined in 40 CFR Part 721, Subpart E) without submitting a

..,....-.r,,:iri.:sipifioantino;w,'usearotice,tq,nP"A, .the Company sha1l'cr:asesupplyinljittetuitbistaficsifo{hatr:;"'" ' - ' ' '

recipient, unless the Company is able to <looument each of the following:

lnternet Address (URL)' http://wwwepa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 56 of 77
ijiSl.rji:rrii(.ji1 t,;t{li.iCn, Cr !r-ir.ll r,,;:,:i(;i.ii iil ii r;i;r,liil'r:ii;:1: -'ri:'''r ':''r)

snbri-iil.{.iitil a l;i;31ifir:a,itf- flfi'',;Y Li:;{i r--tiii.icu i+ [i,l].'i-"

,'.. .,',..'.:

or is awal.f, of the tenn:; of the signiticax; fir;r,v usil ruli; [i;L tltr: riMN substance and wi]l not engage

in a sigrrificant now use without sr.rb,rriiliilg asigrifir;ant nr,w use noticoto l"lPA;

(3) If, a-ftu l,:cccivirrg a :;Ldi:r:wrertl of ar r'jilr a-ace 1-r a ln a rcciprent nn*Jcr -:OrT'::lrh (dX21

ol.flris llistrjbutiorr scctiou, thr: Conrpany oLrtains l<no'"rleclg,: ihat tlie recipicnt has failed tc comply

with a*y of the conc{itions specifierl in palagraph (ir) of this ilistribuiion section, or kras engaged in

j

a significant new use of the pMN substance wi'rhout sr-rbrrrittirrg a signif icunt new nse noticel'ttl

i

EpA, the Cornpany shall cease supplying the PMN substancc to that recipien[ shall notifii EPA of

the failure to comply, aird shall resume supplying the PhrIN substance to that recipient only upon

written notifipation from the Agency'

(e) Sunset Following SNUR. (1) Subparagraph (b)(2) of tlis Distribution section shdl expire 75

inal SNUR for the PIMI$ substance under section 5(a)(2) of TSC'\

days after promulgation of a f

unless the company is notified on or beforq thaf day of an action in a Federal court seeiking

juilicial roview ofthe SNUR. Ifthe Company is so notified, subparagraph (b)(2) ofthis

Dislribution sectiro^rqs4utoeEaFiseffiItilsnAl4otifies t'he companyin.waiting;thal'aHj&6tlffii1sr'na::I*:Etsiixi3r*ii1

court actions ihvolving the sNUR have been resolved and the validity of the sNUR affitmed'

lnternet Address (URL)' http:i/www,epa,gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 1000/o Postconsumer, Process Chlorine Free Recycled Paper

' .i .,' ',ii.i':"l,ll l,li iii) ,., i : 

;

. 'J_l I ; I lt: l' i ; [.] l;tti-lS'i,ltcr)i] (rr'l.l'rr-")LlI

OFFICE OF CHEMICAL SAFETY

AN9 POLLUTTON'PREVENTION

EPA SANITIZED Page 57 of 77
OFFICE OF.GHEMICAL SAFETY 

.

must be i* rvi:iting mrl mi,st sp*oiJiic,;ily include ;iii jiri:triio :i;tj;ltiriteil ilr.llLe $j'lMURPSrlQrThumevEHrpr

:..

,,i"fi:,.ii6sSignifigairtnr:wpses,tanrl-;rhir:hr'v,iulil itrv;ik"rridniiiclrit::,.Xrileiloti.fl:at:l] ':rit+ .,',.,,,,':,.,

' " ' 

,. 

: .. ,' ,. : 

. . '. ." ..:. ... _' 

' ' I

n*-ffioo.t+ $\tin ana'ex?irationbll:;'ibpaiat-rap^,!trxz)' such noticr:.rnav 

lubstitulq 

h'rthe ' ,

. .,,I... ' . '.- : ' -'

*r;tt* igrrooent rpquired fut ihe introductory'clause of paragaph (b)i so that' ifthe Company 

.

'.,...., ,. --. , 

, 1] , ,,

. gorides S,"rch notice tu the pcrsolis io:who;, it disTibr.iict fJrc ilMI'{ substanct:, tltxr ttre (-ompirny 

.

is notrcquifecir to.obtqiu froh such perqols ltrc rvrilten.agrqerrrurt.spccltiul 4 pdaglapfi , .

':,'',,'',..:.'-..',.':'.j.,,l'.' ': " 

:: ' ': ''i ' :. " ':"

,''.,,,

:.. . .t. 1

' Th" Compa,p., shalldisiiose of th" e,Nr-N'tut;tqqct, dud, any waste sti:ani cortai+ins the,Plvfl{

' ':: l- ." : . : .

substance only as fplloWs, This provision dOes not supersed3 o' p"'-pt *y 4ppticable fedaal'

. ,-,.. 

' 

, , 

t l, ,- . .- 

-.

state,mtl.locailaws.andre,gulationsiftlro,selawsarerriorestringentthantherequiibme'lrtsbelorry. ,:j

(1) [he PMN substance must be disposed of only by:

,.'-

. 

"i 

' 

G) incinuation (destruction anil t"*oua em"iet' cy oi 9i9'99y4, or ' ' : '

(iq uniergound rqiection con@! (cl+ss 1 woll, derp we[ injebtion for hazardous

, -' i

irfacture nrust be rlisposcd of only by:

{'2) Waste streams fiom mail

ivir.l: cf fi ciencY.ofl gg -q9%); o'; (i) inci neratiow (rtesfnr eiitj nlarrd:remi

. 

lnternet Address (URL)' http://www.epa,gov

Recycled/Recyclable ' Printed with Vegetable Oil Based lnks on 1000/o Postcon=,irn*r, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 58 of 77
g.-'H\'? uNrrED 

'TATES 

eruvrnoruMENTAL pRorEcroN AGENcy

,{

OFFICE OF CHEMICAL'SAFETY

'. 

r.., l-i' '\ yi i,iti L -,;,

i r. - --..,,.1. 1,r',irc.r r,.,u.ti r..tit;;;;,:7 fi' " (ri.) WaStC SftC;;:rUl; ir'{}f-{I l-ilit ii-tt;rii r;i' Li}ir.r-l'''r\'t' i/.' ' '' "',

,

/'i ''- ""' "' t {clestructic'r 4ni1r't,iticlvai i"[[ie;ir:iicy of 99'9970); cr

\-

fii) unde;rgrountl injectiorr' con

,]

'.;

'| 

:

BE-J#ffiE-Tg-V"["2-[fi18 . 

, ..1:.. .._: .: 

. r,, ' , 1' -, ":: . 

-

f'hisprovisiondoesnotsupers , : ,,: :-,i ,: , i

'r ' 

r any prrairt*t* or pulposeful release of the PMN

fegulations, The Company is prohibited fron

; r --. ,tuting, piocessing and use cpntaining the Ph4N

substance? or any waste stream from manufa(

,]

.:'

G) fesrldg The Company shall maintain the following records until 5 years after the date they

*:.r,i,1.tte+are.tleateduridshall,make tlreo a.vailable fonrir.xspggtionarrd.nopyingfuiBBAiiin.uoooddrce la.ith

section 1l of TSCA:

lnternet Address (URL)' http:i/www.epa.gov

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EPA SANITIZED Page 59 of 77
lnternet Address (URL)' http://www.epa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumet Process Chlorine Free Recycled Paper

EPA SANITIZED Page 60 of 77
g''-X\a uNrrED srArE$ ENuRb'r.iMENrAL pRorEcroN AGENcy

L%:-1:.,:::.::,j:L:.: 

,,11;i,:r, , ,,.,1o"11|3'o"l ,P9 3o1u''o- ' ''"; ''1;"" f"rt"; "r ' : ''

,:r,orbrr rrf tlii Orilci;

(6)Iier:olrltCocr.rmeritingiir'r:'cietcrininatir;lsrrirrriiirr;rii:yLhljltoteetionirlt#,uifu{uf@aneverrtoN

sccti'n ct'{liis CrCer llir-t r:ltmiicli iri.otgctjvc r:1c''tin2-is i':'i;erv lc s t'; thc ?}'4N rubst?llDo;

:' . r I ": l:ial of

(7) r ,.;645 re,ruircrl hy1,;,: r15aJ;ir (i). cf';:c trl':',v il:lll:3-],::1"11111: 

t-i|l{.|s)l

,.,,

'" 1,itj :or*ra!.to*o*ong *qta..blisrLruTliurrl impr'erncntxion of tliehazard golfl]cation'

prngram requirdd tv *re rt-ard foto*onieotion r'ogram section of thiq or'l'er;

(9) Copies of labels reqyircd;rndar lne lazarcl Cgrnnrrlrication Progr-am sectioa ofthis 

.

O:der; ,. : '. 

, 

l.::-i'.,... i, 

, 

t,

' :- - 

. ': :' ' ' r:' 

ld by the Ilazard Corrmuqication ' '

Program section oflliis Orcler; '. .

i. ..: Lr. .1, :.. t 

.,

01) 'Records documartinc "oml.1il 3wlS.anr annlicable maaufactur[g p-rocessrt$'

usq arul distribudop rpstrictiol.nslin tfr" l,ra".rfa"t"r:rrg and Disuibutiqnsegtons qf this OdE[' . '

iricluding dist-ibutee.s' writtei dgreemen, t to conolY.]$th 

the 

Distibut'ott section oft$ ordari

(12)Recordstlo***tiog*i'pliancewithzuryapplicabledisposalrequire'mentsqrder

the Disposal section ofthis ortler, inclutling method ofdisposal, location of disposal sites, 'dates of,

' fitl ,obut'oce dittosed' 'Where the estimated disposal volirnie is not

disposal, and volume ofP

. lnown to the company and is not reasonably ascertaihable by the company, the company must

maintainotherrecordswhichdernonstrateestablishmentan{implemgrrtationofaprograpthat

; ii..,..-. ensllres complieuree;rui:tli;any'applJeabl*;Cllposa'Li"equi.':{:illr)tlts;

'lnternet Address (URL) 'http://www.epa gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 61 of 77
'' ,,-i -

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

OFFICE OF CHEMICAL SAFETY

i-.. iii 1 i :, : i i ti ry',11,, ;1 S i rcrlrl ri&t.lP nqllUflflJyP R EVE Nr I o N

ftr) appliggbdity, Theprovisiorrs cf this itocordkeeping section are nFplicable onl;rto a'ctivities

rct h,Ianu{"aciLtrt}}.", it'ai:p1ica-*1':, iuLt[ ni-'f i'nl i:cfivities; cf Llrr: ci'tfie Cornpitny anr"[ ils {]i-rntr ?t"- "

Company' s ctlstomel 5; -

rtrl

(*) ph4B. Cqqtrol_l,lur&e,., IJnder the pap'erwolk-Iterluction Act i-lntl its rr:gulations at 5 CljltPart

i

73[,0,particularly 5 C.FR 1320.5(b), the company is notrequired to Iespond to this "collcclion of

rm the Office of infonnation unless this Order displays a cuffentlyva,lid control numbet frc-^^ *:^- -'-1--- -

Management and Budget (,,oMB,,), *d EpA so infon:rs the company. The "collection of

' pSCA $5(e) Consent Order has been approved under currently valid jnformation" required in this

ONIB Control Number 2070-0012'

lnternet Address (URL) . http:/iwww.epa.gov

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EPA SANITIZED Page 62 of 77
g'*Xho- uNrrED srArEs euvnoiit'deumL pRorEcnoN AGENcy

e"Voc i,, 

., ,.., 

**'Tli,"l,:1,',9, irfl ,1,,,,.r,,i :

!r. i(Y -../"_ - 

. . ) : . : _ 

.: . ' . 

. 

_ _ . . 

. 

" . 

. ,. - 

. . .. .' - .

'Zt padlu -i " ''

f..; . r ;. .''.- ;;.i.'.::r ;;;. j.i::...1i., i..1., 

-: -.'.... - - .

may u;;carrionally co:t'jtict r:'n ';ii:e r;i:ll1i;':iicc ilispr:ctio'':': li Conip:rny :'1i:''"t'*'t n"t'#:::';:'J:;:r 

*r.- ,;i$ild

assocrrriet{'w.ili ';ire i,'lv: rI s*1"taa.e: Jlj lat'ilj tate $i"lt' ttoi''""i''oi1g -I'i?'\ Lrx s;rnrrol' rllYlhl#,Itffi rtrlueHrrou

' " ' : 

rt inl.i:rlaliol ;i:;'tiiieqt 8-' 1l:r-' s;:ircdull:;g tu'tt1 urfl'l1iqt'ut1'fi 

. Cornp,-rriy .: iir advaneo i:l; rcqtlui

;;r;, iu"t".r"*,r.t,ii!'**o".."t',' L'ttt't;'.'*o'Jliri:i:irrrti'rtrrl"'ln':A'n'rr,';+"e"t '

,,,, 

.. I .,iil .r,r,'...', : 

, 

'.. 

',.,.. '. ' .-.

inciiltle,br! aronotliulile{i1o1+l}.E 'o4qYrol8i, ;: ; , . 

, ,:l 

,. 

.,,,:: '.,1,

...i,iExpccterl.1aresantti*",*#it'cPL[,h[substanc"witib,,inrriiductiqnwithi4ttlq:,,

..:',. ',':',t 

-- 

,..:... r'':" ''-I ..",...: r":.. -:. : ... .''

Su1DIjCq[uenf12rnonth:i;'|..

gonducting an inspection,for that'i1u1prc s e'

'rhe l]lllN u,rbrtunce aur:|. *ry r*r,,sonaLrly bc exposed io the Ph'{iN, Sullstzuir:e;

(3)Cunerrtjobtit[csorcatcgoneqrorworkerswho.

, 

, ' , (4) Existing exposrrg monitoring daia foi workus who are invollgd in activities 

,,

'' 'l''t :: 

"' 

t

r 

associated with the pMN substancg u"a**J r* ubry be expo$ed to the P$,N sublance;

: '' ' rliance with this Order oi

(6)Anyotherinformationreasona!lvre1atedtodetenrriningcomtr

I Ol gs44uybB9spq,.g' The Company shalf resnon{ to such r-equgsts wthiir a redsoflable

periodoftime,butinnoeventlaterthan3Qdaysafterrecei'vingEPArsrequesl}-Y!enreqrrested

".,1in,'writingby-EP.,A;th.,op*puoy:u.r",poos*,hull.beirrwriting.'To$hhiorlentth+inibenprt.iopjs','.

lnown to or reasonably ascertaiuable by the company at the time of the reques! the compaoy's

InterRet Address (URL) ' http://www epa.gov

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EPA SANITIZED Page 63 of 77
UNITED STATES ENVIRONITTIEruTru PRoTECTIoN AGENCY

.''.,'

, oFrce or cseirllreeL serery

I ,. 

....alrDRoLlrl]:JTi.EREVENTloN

c u.p*f."*riltu to )ii'Apn1iuart 

11 f'I:riopt' (b) rlr'Jl ti': protle'q1;n 'rcurrcl+oulnh.$tt1]: : '

v" s.u.-#cjis$*]l4l,lrl'nlt,I,{Y.^{'.El:ir}I{:rlirlilris,ttliB*s'J C*(}-}LS*EHT:SE-uH}B ' ' 

,

1 Ll 

' 

.rJ vv y q'. "'a-. :. \--l ::.y-.."*:--. : .

rrjrder thir or4*r*o, be trans{''crri;rJ whcn tlic company transru:s iis lnte-rcsts in the }-M}T

,:.',, .,.,.,I 

, 

: ,, 

. , . , :

s*bstancq inctu{ing t}re right to rnanufacti;n: the'PMN substztrtce, to attr:ther person tlutside the

fu) Relation of encemeni'f"Nosl

.": .t1l lfdt'aTfertqtuthlcomnrmrtothut":t*ul,l"Itili-:u*""'

before EPA recewbs a notice ofcorrimenCement of,manufadre (T-{OC")for the PMJ! subgtqnce

.i.

,,

fromt1ieCompanypursuanato40CIR720'102,theSuccess1rrnIhterostmustzubmitanewPMN

to EFA and com, ply fully with Section 5(a)(1) of TSCA imrl40 CFRpartT20 before co4r4encing

manufacfure of the Ph4N substance' i

(2) Aeg-liOC. $the transfer from the Companl' to thq Successor ur Intaltis 

:T*':

after EP.,,-{,receiyes,a;@@hqrsauressor'fJrdn{erest shall compiy withtle'tamspf'&isofder'':adih'11''i"!:'i'.c''t:i't}

shall not be requitcd to submit a new PMN to EPA'

lnternet Address (URL) . http.//www.epa.gov

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EPA SANITIZED Page 64 of 77
:.\SEo sr4D$-

g'' Il'o'rn r#j

. :;li

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

WASHINGTON, D.C. 20460

r..1 I .r-: i,l' .: '1i,.: ljl-1,.i;.,'ii:':.i,it,':":,'.,"'''i '-'' I''": :''

(1) !'l:r;ccessorjnl:ntctest"ric;utsapet:iolrotttsilt':ril':(l'rl:'ii;'':"7n'hli'e;ac1,:j;^e-lr':

OFFICE OF CHEMICAI SAFFTY

'' , i o lt r': ;o r,r l.rrttl'cturc'ti:c iil'vii''[ ' r:''br; ari""' incil 'iin g aAi'roPi]0Q$$b{pnevelrtox (lrrinoai:y's fttl.l irrlctcst rn tnc 1*.,- " ',

rights tu,.rl 1er,1;1 1i.;$irities, thiough a rlrursj'l ior''-ir"nt I 4'1e'J Liy.tlt* il'.,r1p4::v, a'; t'rat's:tr'ror' ancl

.-. 

,.,. 

'.,:. .... 't ,', ''.' r,1,," ''' ' 

'

t.trc fi*c,-,rrsor ir:t Intt-rcrtl as trzu..i".[eica, 

t 

i'1',,: tr-rit xc,1.li'ii,; pc:si;rtr; v",io licqitire l';s$ tli rq ''he flil

'r .-r ... '' 

, I,ir4],l ,iu.bstarr.il suili n,; n. iir;ens'r.e ,,'1i1ii l,:+" a'.1'rci:1u .+ 

1il lild,, : .

ri.*i. *o m" putenl f manufacruring rights msoqiatqri witJr thd PMN t'lou-:", A lu*1ltot * 

.

#;i-,5i.t" iircorrporatea,ucensed'oldoinq bylinessin rihe!lnit"a;St"t"s ittuc",91'{alce with :

,:,!:::Y,**::-.,_.j.,..l.i;',..1,';l:,1l.....,.1.-.,...-,..

' 

. 

| 

, (?,\,rt *rfu, no.u*e.tit means the lggaf in.tr,rm"n4.) uscd to corwey thc irltcrests in the

. : : .... : r : ', .

prurN.rtrt^j", iqsluding therightto mt'tif;"tuq*jpM1 tutttooge' toln tlie Companyto th9

--: 

,. .: . .: . l ': 

'

Suciessor in Literest.

.. . ,' ' ' . .

(ON '::',. ..,, '., ,:,: ,, .'.,., :'.,' , , 

. . 

,

Company shall prolide to tho S. uccassor irr Interest' by registoed mail' a copy of the Conse'nt

, ...': . l] 

. 

, 

,

or{er and the .Notice ofTransfer" doculent w,lich is incorpollted by r€f:rTc,e as Aqgq*t' 

,

!o this Order.

(2)NoticetoEPA'Witirill0busiless'claysoftheeffectivedateofthehansfer'the

Company 3ha[ by registoetl mail, submit the finlv executed Notibe "t",*:ii.:]::t^'O' 

.. ..-,.....u;i.+

ir..u.s."Environmental plotectiooag€Bqjrr*ldilii,r$foEf-rieu1s$lanagerBatBranch (7405);1200r*$'rr*{*:*i*+!i:"}df':'d

P ennsylvania Ave,nug N'W', Wash nglon'D 'C' 2'0460'

lnternet Address (URL). http://www.epa gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 1007o Postcon*,lmer, Process Chlorine Free Recycled Paper

(1) Notice tq SucqqsPor iq

EPA SANITIZED Page 65 of 77
' e tn'';rle av ai irr'Li 'c forj inr;p''x;::ior''

rnarrrrl'aoturcri. Copir.s of ihc i';;rnsl';i i)r:*:i"lrrx't mus1 4 ""::'-''"'." -

. OFFIPE,OF CHEMICAL SAFETY

pLnsuanitoS<:r:tion11cf1,9f'lA,rr:'rlrtstt'oiirr:nft-co1i";,'r'll"c';ftrr::i"it''t'nilmustfimrdlliurloNPREVENrloN

or r;viiions v'i'j,:l.r cxprtjsr;l.y l.ri.) rlsfi:i i::tLiiil / iiir' iiic f i/:l'l irlri'ilan':'r r';iiler ihe lcrns of 1'hi:i { .r'r'iat

ft:) Liabilitv, \."1 :_;_._+ ''' 

,r, The co,u,p*v shaiuic lia],rre fbr complianee with the reqLliremerts of this ordcr r'rtrtil

ilrr,-t-:ffq'ctiverla1eot{Jrct-ransti:rr1+sr;ri[tic1.ai;cv;..i,.,

: : .r:' 'n

order effective as of th.e rJ.ate oJ: traflsfr:r. I

Ja

:)iion shail be conitrued. La'1,r:olribit the Agency fiorn taking '

enfrircement action against the cornpany aftcr theleffe e date of the transfe: for actigns taken' or

omissions made, during the time in which the comp*y **.rfactured, n'ott*led, used'alstrihutea

in eommerce, or disposed of the pMN substance pursuant to the terms of this consent order

lnternet Address (URL) . http://www.epa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on '100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 66 of 77
g'--Hh,- uNrrED 

'TATES 

eruu,*o,uMENTAL pRorEcTroN AGENC'

tffii ASHNGToN,DC zo4oo

,*t rr,,rrr,,r, to mt;riii7 or.i';r'i:l:L: slllrrit'prl'vc i;'ro'visi't'trs c f 'li il; O:::'lcr ' i'hc, cx1:r;srltr;s ?nd risks 

'

ttrl ih'o iltlcu:natiorr EPA dcle-'mined io

iilentitic.il by liFA riuring i';s : ,": r'iow of l'i':;: i)l'4lT :*tbrrtail';e " , 

,

, 1';v-pr'1;;r;1'r;5 ilii ::iirrl r,.,, ii'1,i ", 

;.ji':rl i-tt tltr: i'r':a';:tblc ttl ltris O;'cirr'

g'o**"" in detennining whet-her to anien(l or rcvoke $is Order' EPA will consider all rilcvant

erminatiog' iqcluding' u'here

information available at tho tirne the Ageucymakes tlrat det

t of th.; tr)st {latn or otilu m:c:.'iril:ron that supports the li+dings in this ' approPriatc, artY rcassessmen

otcl.er,arrexaminationofnewtest'dataor+therinf,or.rratiolqramalysis,andimyotherr.clev.rnt

informatiPn.

.ificatiotorrwocaiionifepAdeterrninesthatthe;ctivitiesproposed

BPA will issue a modi

ttr€reitrwilltrotplesentanuffea,sonableriskofinjurytohealthortheenvironrrierrtaridwillnot

resultinsipificantorsubstmtialhuuanexpoSureorsutstantiale,nviroirme,lrtalreleaseinthe

f the health or eirvironmental offects of

absence of data sufEcient to pbrmit a reasoned evaluation o

the PMN substaoce.

In addition, the Company may petition EPA at any time to make other modifications to the

Ianguage ofthis Oriler' .EPA will issue such a modification if EPA tletermines fhat the

,'modi.ficatio:o.is'rrsefrrlTappropriatg.and'consistentwifh,thostrrrotulo:tu,li1:intmtiof,lthiiiaorde-Eas.:u:,i*..alr*,,,,.-

Internet Address (URL) . http:/iwww.epa.gov

Recycled/Recyclable - Printed with Vegetable Oil Based lnks on 100% Postconsumer,.Process Chlorine Free Recycled Paper

issued.

EPA SANITIZED Page 67 of 77
ouat'*aho g ft 'o- r#j

. 

tr'

UN|TEDSTATEsENVlRoNMENTALPRoTEcTloNAGENcY

WASHINGTON. D.C. 20460

. i -.'-':'- 

-. 

-. ..t -...,t .. ,, 

, .' ,,.,.i.'

,,. , ,'i '

.. ,: ' :

i 

-: 

, 

t' 

.

trjis ; " uier; a*d llcrCIby: agrccs that ali inJ'hrniatiln,hetr:in tiiat is clair-rred- ari r:on,f { rrntial i:y rilr:

'' !,.' . : 

.

con parry (pcr seorion 14 of llscA, 40 c1iRpart Tr0 suh,u*t E, and 40 c"rR Part 2) is comoctly

ici,entifiedwithinbraclce[s'on,1.t}iatanyirifb'rrnation.i1ra1ig'-rrotbr3pketedisnotc1ainreda1,

. lnternet Address (URL) . http.//www epa,gov

Recycled/Recyclable . Printed wjth Vegetable Oil Based lnks on 1Od"/o Postconsumer, Process Chlorine Free Recycled Paper

rt

Date

OFFICE OF CHEM

Office ofPollution PrevEntion and Toxics

Title: I- n .

EPA SANITIZED Page 68 of 77
o..sto 

tratto

g Il -ro-

"Mj

UNTTED STATE$ ENVIF9NMENTAL' PROTECilON AGENGY

WASHINGTON, D C 20460

, t,- 1 ', r '1,- ii'' ' 

"';' 

;'i

t 

"Corrryilny'rncans flt+ perr;';il ()f IJf;lr'

contaruers.

lnternet Address (URL)' http://www.epa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 1000/o Postconsumer, Process Chlorine Free Recycled Paper

. 

,lCouirner*ial uso" rn*uirt 1r1r.rii.e 

of a cloniii;al su'l:stt]Ilce cI: afyfil]

''' r ' . ,iorr or- irlerriill,;;iirlrl ,rr- cir ar; ccrltl iLarrl.s) ccde nr'iitbt'x,

r,uo",,o;:;:'ffix;H;;?l#l'nfi1';ilffiH#;,;fi;ii;"iirvi.ro*r*aiiobsr4nceo'iier

.:. ' .' . .: :

r ,,consnrn*.; rrr*uos a.ptivaie indivictu*y,*ff-a chcrrric.al suhsto;,;lr*ri_r#lrffiJJr,**,

contzri ing the clierniqal substanqe in or arou11d,a p.e{,rf1nent or tglwor4ry, }r-E}ur':+}?^- r- 

. 

' , 

, 

,'

sold o-r mdde availab_le t? orrr*uoi* t"r t1r-.1.,'u*e'i4 or ar a p-ermanent or'temporary ,,,

householdor;fu;;;;i"o'**,aa*nooI.oriniecieation...]...,

'l *c-ontain#,***, *ypug, nr*a;,uottre; !"l jtcYlinder,fu*iiTtli-lH:lijlfi*t

tank,, or the like that coltlns 'uii;uragus 'cherni:d 

F1r purposes of this'section, pipes or plpmg

systems, and eng*'s? nret tant; fiiil; #-t rirtcr rio a -r"hicle, are not considergd to be

.y.i,t!|tC!)r'tc.irlsot;ieajii,,ztli,':r,uileji..e:!,iLe.iow.|';

.Nc t2 :'thc al;dc!t".d ij nit' i:t't-

' J'Clrur !cltl caliro" 1;l{laxs rir ; r;ilrEilf i;r, r"'rli' *''.*'', ,', . ..-. ... ,-.;....,. *,,1.,.{lp PoLLI'

*itf, tirt io^,""1"*at' ''r'ol"' t A"'' Loptil i';' lli.: 

"'hr;'r'ricat 

'"' l: '; i |zir''i:: ;i"'i-';iuc"i rute:; cr '

r..rmor:ciahuo,oia,ar.,iovrhirdi;;i,i'',1;;j;;i.lt,"iiti'r"1t"r";',',tsu}.,t;;lrceibrthcpu:pogeclr . .

crrri ri r ir.;i,; rip, i, it;izarrtl $ o ii i l,lirl.iu * '

r/L:J r-..'- - -:.--t)

i,..: -i ii,, i' :.'i -'r, ir,[t.: ir. ii;:fl [.];i;ii'r r.:'Uiu : it;i: i+ r r! . -r: .,. lr, ;. , '.:r,';:'ii;;iiti, iii '.,t', '::''.-",/i{.li..l ii iiilfil.l-li';t'/tj I-tt

,.r1.r-,i7.{}]]|r|ii11iinlilo:l-tilt,i..li,.,lt'i,1

EPA SANITIZED Page 69 of 77
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

WASHINGTON, D C. 20460

Submittea ty ihe COmpany ielevzint to this'Order, , 

. , 

I

t.

.]-11.\-/i j-l,r..rlr:i'-L:rl'l'":,;i' 

: .

, 

'' ' 

,iNorr-encloscd processr; rtearrs *-ny eqolrmerlt fYstcm fuch a1 an t;pi*'rLi 'frir; rr:a'ctor' storage

:ii:::;.T.,til".l,*.'n-;':il#;tl,t,stance, is '* onrib*t,t'r;r[, proi**r*11, o' o',hqjr ivisc

tank,.oJmixing.v9ssei)jr1whichac}rer1i9a1.s*-;'-.-..'\'.,:.

rrseclwfuer.esignificantr1iiei:tctl*;,a.aoftheu.,tk't.'emica1s3-hstance,and.r*.rey',ortt.Piaoei}1rfiIay

, ,]

''';l-: ' 

, 'Nonrindustrial use",mgans use other than,{ a flacility where chemrcal sutstances 9r

mixtuieJ#**unufactored,ruPorted,or'procesSed....'.'].|,,,

I ... | : r

: .,pMN subrr*ial, moans the chemical sub-sthnce descti-bed in the Premanufaqtufe notlce

,i ;L

..piersonal protective equipmenf' means *y *h*1i:il f:ot,-ctive :lilhiie or device placed

on the o"jw,-;i@;"r##rrh; an4. eryolui"io, an identified chernical substance or :

substances jn the work area.. n."*pres-inc[do, b1t 1re ,uyltimited 

to, chemical protectivg

clothing; &prors, hoods, .,fr*iari' gt*', ACe spla3h thields' or equivalent eye protection' and

various types ;I;rpr;; it*i;,rlr"*** arq not included rn this definition.

no*ofo' f'l^rxr nr hemical .,process str.eam,, means all reasonably anticipaterl transfer, flow, or d'isposal of a c

substanc e,regardless of physical state o, *orl*rrtratiorr, thror-rgh all intended ope'rations of

orooes.$inf;,. inclnrling the cieanj-ng o'f equipment' ';'lli::i'

.r-- .iiiii.1-,1 ;:,.-. 

-'-: r'r 

.r: ,..-....-,, 

,1.:,.' ''-l .''':'r:':;::il..;i-"..:...i-..

"Sr;ientifr"ottlit rutiO'] moans nny slgn'.S":tl departnrl from th3lil

thr: Good. I,aboratory practicr: standarrl s at al} crR Yart"' 7t2 wifhr:ut prior r:r 'subscqEent Agency

lnternet Address (URL)' http:/iwww.epa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 70 of 77
. ',ijgitniificd1L'y rxi;;; ',iiLri ilr.id' rr i.,-,;:ilu ,.i,lt,', 'l,r 

' 

i' ii, ;'1;'i111'1''rg,ir dr;r,'oiop jil in aljprreat

r:rririorm ity wi,t *rE iro")1 :;i,orulury ).r:ir:1.1r:r: lj,ra:riliiLrds arLi .i,i:'.A-teviervcd protor:ols, are

i.'cotti.li.tsi1'e, i"t'r'r''atiy itie,ii,l;l'.,t]'ti, ",' "ll'*t"il;'": 

ii'ir'"rl:i':jr'i';.ii; jfjillfj':::*ffliilti?tJ'rl^,- *r*"

I lisraled contir:iler" mens + cioseti c';riteineo 'ii':rr l1:qi'l'r1rrllr lnj ohcmically sqitable ibr

, icirg tgnn contdihmrrtrrf ti .l'n nii ,irrot,ut".i *,0 ti ,,r, ',,o.i,i"l' iltoq,lill beno human e' npqsufe to'

il"r;:;;;;r;;;iu,I rclea-r* otl r.iie lMl'i n:hr:iaix:e ri:nr r:; i'iiis'irxt r'rnd slorritlo'

*Usc rittoaln" rrr'airg -jll'"".'"""!ily *':"i':ijrillt;ti ir"ri';;i'::; ' 'iii'v,' or-eliY:*:t,i::]"':*'.i

s'.lbsiru1cer legfudt"r, ofpnyJ,a*'i"t* ot 

"o-"""'nuLk:rr' 

f ir!.ctir'jt dli 

ioleEded 

oierations of'

, 

: :' '.Wut"oo4tf,"Uoit",f Stot"rit*A"il.easiop,t*mr*,i"A9Cfn ln)L : '

:'II l 

'

. 

,,Work area,, moans a r1r{)rj-i -;.- rlefinerl splcg in.a wQt'k lace w11cre the PMN substance i3

m,,""tf,4iirocesgett,oruse.d*a.wrr"ffil.i,'.y,'-e.'B'IJi:PIesc[t-j.

'auhic ldcation'containing onc or more

"Workplace" means an establislnncnt at one gcggl .l

workareas., 'r j ' ,. .

;!i

lnternet Address {URL) . http //www epa gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 1000/o Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 71 of 77
.6SED sxqlog'' Il 

-o''or#j u N I r E D s rAr E.s E Nvr Roit4,t H$H:. rxr";E c r I o N AG E N c y

. 

,. .- ., r . 

, .:,, :. . 

j, 

..,

/

li t I : . ! t-

,:'/..! ., 'a:1,1.'-. i ', .:. .- : .l t, -'i . l n,. j..',-1. r .'r rY)-ij t'-"-r,, 

.':'''t L) l:Jr\.., -:-.:. i.'-,- a

OFFICE OF CHEMICAL SAFETY

AND POLLUTION PREVENTION

,. jt r1 i ra n./ {'1'., a:.nS ,i;;i'r;i')

.

:i,a*ufacture, processirrg, uso, ai*t itution itr *,r*1*rge airci i-tisposal of the I,MIJ sltbstrince, shali

rre the responsibility of the succnssor i-n lrrteresl, s.uc1gjro,. in Jntcrest also certilies 1-ha1. it is

incorporatetl, liceirsect, or doi-ngu"riir-u* in the IJnited sta.tes in accordance urith' 40 cI'R

'72t).22(a)(.1).

3. cout-rclenJial Business Infonrra.tio_g, The successor in Intuest hcreby:

reasserts,

.

--- 

relinquishes, or

:

modifies '

all Confidential Businqss Inform{ion ('*!{-) claims 1u$-by the Company' pursuant to Section

14 ofTscA and 40 cFR partL,for the PMN subryancrq). 'whe.re,'treassert*" 

9., 

"t?L"qYishes" is

indicated, that designatioo *huribe deemed to f$rv, to.fl| such claims. ffi*I* "modifies" is

indicated, such molificatio, ,nun be explained in detail in an attachment to this Notice of

Transfer. Information which has been previously.disclosed to the publi* (*.{', ? 

*h:}yal identity

thatwas not claiured as cBI"-tth* orifiinat submitter) wouldnot subsequentlybe eligibk: firr

confidential freatment under this Notice of Trlsfcl

,:.-.,

, ', ,. :.,',, ,,.

Recycred/Recyciabre .printed *,,n ,"ni?jill"Jf3::"-".'LYXil',[T+j'ffi."J,Xrt;:r, process chrorine Free Recycred paper

EPA SANITIZED Page 72 of 77
n.-Hon rmj

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

FIilC e ofAutho,naed Officja1

fitt* of Authorized Official

Addlesq

City, State, ZJP Code

OFFICE OF CHEMICAL SAFETY

AND POLLUTION PREVENTION

lnternet Address (URL) . http://www,epa,gov

Recycled/Recyclable . Printedwith Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 73 of 77
o**f,to 

t&to

g af -as

rmj UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

WASHINGTON, D.C. 20460

OFFICE OF CHEMICAL SAFETY

AND POLLUTION PREVENTION

internet Address (URL) . http://www.epa gov

Recycled/Recyclable . Printed with Vegetable Oil Bhsed lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 74 of 77
n..Hon r#j

,, I ii*

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

WASHINGTON, D.C 20460

' . 'i'.,' '

.'i'iiil; :\ilLitlhlttuiltIi::lir-';ii'r';i;

;.irr r:,.i y i:t t:: al .il-:-q r-; i t l; r-r'l i: I i i l i i:r I i ; y tt'". I

{, Lr clt ri,:a1 ) :, z, p o l,l r rr;' .['j r':r ;1' r' i;# io iL'

s,],A]..,I.$,T',.{'jI.,l.-,l.Ji{.]I.lj.'Iii.ii]]j

6 ', Compt.rtr')rfleitflsqtlalies. ' , 

, ' 

, 

,;l ,' ,::

.

,.,.?-,_- .ti-:?-,i 

1 X;)r-/(iii . t),,r.=1, .t* I jt ,/-r\'-;l

,1

. 0 ' F-ortn ilic leriio

: ;.- - l/^

'I- --' (]{r - }(:)i(\ffr + \',vr)"

Compute degieeC of freeclom

where,

wl: sr

I

1, "h1l1r L:

f* (W1 + Wr)zitwr2l(lrt - t; + W i tft"- 1)l

rr2

,t :.i.

l

Xr = Average of the results from the company iaboratory

J'

h=Average of there*ttu rom the independent,]aboratory 

_

r1l - Number of sampl** uouiyzed bytho company laboratory

-l

t1z:N.rmber of samplei aflalyzed by the rndepeutlent labora;tory'

Recycred/Recycraure . printed *i,n v"giiiil:i,iE:3T it*i'.r1HiJffi"""'"Xf,ll,., ,,o.*"s chrorine Free Recycred paper

- ,1

i ril i i-rlbltruE od EnEurcAL sAFEry

r., j' I hfiflFl eEULUT0N PREVENTON

EPA SANITIZED Page 75 of 77
i,/

s2,.87

101.85

87 .44

99.68 i 1:-

1U1.I5

oo j ?1 J .2..(

OFFICE OF CHEMICAL SAFETY

AND POLLUTION PREVENTION

i:liffilvillIJilJ

Ilnainple t

80.ii6

1ilO.01t.

86'04

5? 61

8'1:85

. c.}- i: r-i-1 ''l '{ I t

'-!

iXr - 83.30 -flt 

== 6

..' I -- n7B12 bt f/i '= 46'25 =/,

,

Example 2

,la ! ia.',ir";i-tf )

9'7.11 r , 

r :

91)'83

91 "83

1 t\i:. /l il ' -L \j ') "-t''t itJil.J4

l:

:f

S.,2 = 

q.Z6 Wz= 1'54 f)l tr 'i4

f.-5?t L. o14r

a*eo;*,;il;*,;il;F";.fo*g'**'or'fieeaom,tl:l.e97.5pelcentil,e'no,1n1wil1be..

approximately z-so"*t ich is ffi.il, t#,tq iuso:tute value of t, 2'46t1 . II@ce, the means of

tro data sets,are not signinc#tlr different ai tt "ilo level'

However, iflthis problem had been-tre1t1d as an ?Idh.'ry.t*o 

s31'9le t test' llt ryT*,

would b* *igoifiiffiftiff;;#;rh",i%.revel pgr_u:r.e the absolute of r is greater'than 2'228'

rh-;i.i p;;;."tile point for the t distribution with 10 degrees of freedom'

DaIa Set 1 - - Data Sqt 2

108.0s

96.51,

100.04

104 "33

t 10.32

107.00

lnternet Address (URL) . http://www epa gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

if :. i ,r

EPA SANITIZED Page 76 of 77
-.+sto 

srah.

g" Il "'n

--"*,ffi'"= 

ji:)i

,, 

.i

UNITED STATES ENVIRQNIUIENTAL PROTECTION AGENCY

\iVASHINGTON, D,C. 20460

, i I .- 7-i.. .,.11

r.;t . \l)",t7

OFFICE OF CHEMICAL SAFETY

AND POLLUTION PREVENTION

uii"iri r;r:t$ iti;:;'ii;qriificiirrtly';iii'fi;tr:,rt a.t i[ro ')',\,lr;.;.[ ' ' ]t ',,.

lnternet Address (URL) . http://www.epa.gov

Recycled/Recyclable . Printed with Vegetable Oil Based lnks on 100% Postconsumer, Process Chlorine Free Recycled Paper

EPA SANITIZED Page 77 of 77