Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. 

to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific 

This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were 

tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted 

yellow are required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fi

automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865-04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If 

of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, ora

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results works

6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a m

3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you 

collected more.

7. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the uni

measure.
Information

nformation about chemical analyses of fuels 

, chlorine, fluorine, and metals, such as 

nd selenium. This spreadsheet is intended 

p to 4) fuel analyses at that specific boiler. 

esting for all 4 HAP surrogates were being 

Fields that are highlighted in 

down boxes, included. Gray fields are 

_Testing.xls).

ler on the Boiler Information worksheet.

fuel column of the Boiler Information 

 the Other Fuel Description column.

ethods worksheet. For example: "ASTM 

 Picklist worksheet (orange tab). If the units

le, please fill them in the blank, orange 

e in the Fuels Sample Results worksheet.

s worksheet. You must provide a minimum of 

re not limited to that number if you have 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Test Date

1212100003 Progress Energy Florida, Inc. 001 6/15/2010

1212100003 Progress Energy Florida, Inc. 001 6/16/2010

1212100003 Progress Energy Florida, Inc. 001 6/17/2010

1212100003 Progress Energy Florida, Inc. 001 6/18/2010

1212100003 Progress Energy Florida, Inc. 001 6/19/2010

1212100003 Progress Energy Florida, Inc. 001 6/20/2010

1212100003 Progress Energy Florida, Inc. 001 6/21/2010

1212100003 Progress Energy Florida, Inc. 001 6/22/2010
Fuel Type 1 Fuel Type 2 Fuel Type 3

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)

No.6 Fuel Oil (residual or bunker C)
Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

1210003 Progress Energy Florida, Inc.3 As Received Higher Heating Value

1210003 Progress Energy Florida, Inc.3 As Received % Moisture

1210003 Progress Energy Florida, Inc.3 As Received % Ash

1210003 Progress Energy Florida, Inc.3 As Received % Sulfur

1210003 Progress Energy Florida, Inc.3 Dry basis Antimony

1210003 Progress Energy Florida, Inc.3 Dry basis Arsenic

1210003 Progress Energy Florida, Inc.3 Dry basis Beryllium

1210003 Progress Energy Florida, Inc.3 Dry basis Cadmium

1210003 Progress Energy Florida, Inc.3 Dry basis Chlorine

1210003 Progress Energy Florida, Inc.3 Dry basis Chromium

1210003 Progress Energy Florida, Inc.3 Dry basis Cobalt

1210003 Progress Energy Florida, Inc.3 Dry basis Fluorine

1210003 Progress Energy Florida, Inc.3 Dry basis Lead

1210003 Progress Energy Florida, Inc.3 Dry basis Manganese

1210003 Progress Energy Florida, Inc.3 Dry basis Mercury

1210003 Progress Energy Florida, Inc.3 Dry basis Nickel

1210003 Progress Energy Florida, Inc.3 Dry basis Selenium

1210003 Progress Energy Florida, Inc.3 As Received Carbon

1210003 Progress Energy Florida, Inc.3 As Received Hydrogen

1210003 Progress Energy Florida, Inc.3 As Received Nitrogen
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D3173

ASTM D3174

ASTM D4239

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D4208

ASTM D6357

ASTM D6357

ASTM D3761

ASTM D6357

ASTM D6357

ASTM D6722

ASTM D6357

ASTM D4606

ASTM D5373

ASTM D5373

ASTM D5373
EIA Facility Code Facility Name Boiler ID HAPs Test Group

1212100003 Progress Energy Florida, Inc. 001 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test End 

Date

(MM/DD/YY

YY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture

(as received)

% Ash

(as 

received)

3 6/15/2010 6/15/2010 17560 Btu/gallon 0.15 0.11

3 6/21/2010 6/21/2010 17785 Btu/gallon 0.01 0.02

3 6/22/2010 6/22/2010 17840 Btu/gallon 0.17 0.05

 Fuel Testing Results
% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Antimony

(Dry Basis)

Antimony

Units

1.02 17586 Btu/gallon <0.01 0.11 1.02 56 ppm 0.26 mg/g

1.01 17787 Btu/gallon <0.01 0.02 1.01 74 ppm <0.25 mg/g

1.01 17870 Btu/gallon <0.01 0.05 1.01 139 ppm <0.25 mg/g
Mercury

(Dry Basis)

Mercury

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

<0.01 mg/g <0.25 mg/g <0.25 mg/g <0.25 mg/g <0.25 mg/g

<0.01 mg/g 0.61 mg/g <0.25 mg/g <0.25 mg/g 0.62 mg/g

0.02 mg/g 0.74 mg/g <0.25 mg/g <0.25 mg/g 0.96 mg/g
Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

9.61 mg/g <0.25 mg/g 0.94 mg/g 0.39 mg/g 19

13.82 mg/g <0.25 mg/g 2.33 mg/g 0.5 mg/g 12

18.29 mg/g <0.01 mg/g 11.73 mg/g 0.36 mg/g 16
Note the Proximate/Ultimate data below should be recorded on a dry bas

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen

ppm <0.25 mg/g 0.15 0.11% 88.55% 7.21% 0.17%

ppm <0.25 mg/g 0.01 0.02% 89.48% 8.51% 0.19%

ppm <0.25 mg/g 0.17 0.05% 89.02% 8.60% 0.11%

Proximate Analyses, % by wt Ultimate Analyses, % by wt
 be recorded on a dry basis (including ash).

Total Sulfur Oxygen

1.02% 2.94%

1.01% 0.79%

1.01% 1.21%

mate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

1212100003 Progress Energy Florida, Inc. 001 Acid gas HAPs

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test End 

Date

(MM/DD/YY

YY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as received)

3 6/19/2010 6/19/2010 17660 Btu/gallon 0.01

 Fuel Testing Results
% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

0.07 1.00 17662 Btu/gallon <0.01 0.07 1.00 56 ppm 0.01
Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

mg/g <0.25 mg/g 0.28 mg/g <0.25 mg/g <0.25 mg/g <0.25
Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

mg/g 15.07 mg/g <0.01 mg/g 1.26 mg/g 0.46 mg/g 14
Note the Proximate/Ultimate data below should be recorded on a dry bas

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen

ppm <0.25 mg/g 0.01 0.07 89.42% 7.69% 0.38%

Proximate Analyses, % by wt Ultimate Analyses, % by wt
d be recorded on a dry basis (including ash).

Total Sulfur Oxygen

1.00% 1.44%

mate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

1212100003 Progress Energy Florida, Inc. 001 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test End 

Date

(MM/DD/YY

YY)

Higher Heating Value 

(HHV)

(as received) HHV Units

% Moisture

(as received)

3 6/19/2010 6/19/2010 17779 Btu/gallon 0.21

3 6/20/2010 6/20/2010 17785 Btu/gallon 0.01

 Fuel Testing Results
% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

0.02 1.01 17816 Btu/gallon <0.01 0.02 1.01 101 ppm 0.01

0.02 1.01 17787 Btu/gallon <0.01 0.02 1.01 74 ppm <0.01
Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

mg/g <0.25 mg/g 1.86 mg/g <0.25 mg/g <0.25 mg/g <0.25

mg/g <0.25 mg/g 0.61 mg/g <0.25 mg/g <0.25 mg/g 0.62
Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

mg/g 16.7 mg/g <0.25 mg/g 2.68 mg/g 0.64 mg/g 12

mg/g 13.82 mg/g <0.25 mg/g 2.33 mg/g 0.5 mg/g 12
Note the Proximate/Ultimate data below should be recorded on a dry bas

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen

ppm <0.25 mg/g 0.21 0.02 89.44 8.5 0.16

ppm <0.25 mg/g 0.01 0.12 89.48 8.51 0.19

Proximate Analyses, % by wt Ultimate Analyses, % by wt
 be recorded on a dry basis (including ash).

Total Sulfur Oxygen

1.01 0.87

1.01 0.79

ate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID

1212100003 Progress Energy Florida, Inc. 001

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test End 

Date

(MM/DD/YY

YY)

Higher Heating Value 

(HHV)

(as received)

3 6/16/2010 6/16/2010 17624

3 6/17/2010 6/17/2010 17537

3 6/18/2010 6/18/2010 17660

 Fuel Testing Results
HAPs Test Group

Mercury and non-mercury metalic HAPs

HHV Units

% Moisture

(as received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

Btu/gallon 0.1 0.11 1 17642 Btu/gallon <0.01

Btu/gallon 0.13 0.08 1.02 17560 Btu/gallon <0.01

Btu/gallon 0.11 0.03 1 17679 Btu/gallon <0.01
% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

0.11 1 62 ppm <0.01 mg/g <0.25 mg/g 0.26 mg/g

0.08 1.02 29 ppm <0.01 mg/g <0.25 mg/g 0.78 mg/g

0.03 1 39 ppm 0.01 mg/g <0.25 mg/g 0.52 mg/g
Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

<0.25 mg/g <0.25 mg/g 1.61 mg/g 17.12 mg/g <0.01

<0.25 mg/g <0.25 mg/g 2.15 mg/g 21.4 mg/g <0.25

<0.25 mg/g <0.25 mg/g <0.25 mg/g 15.49 mg/g <0.25
Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

mg/g 0.8 mg/g 0.42 mg/g 16 ppm <0.25 mg/g

mg/g 0.74 mg/g 0.46 mg/g 19 ppm <0.25 mg/g

mg/g 0.74 mg/g 0.43 mg/g 23 ppm <0.25 mg/g
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

0.10 0.11 88.87 7.91 0.15 1 1.96

0.13 0.08 89.36 7.85 0.15 1.02 1.54

0.11 0.03 89.41 7.4 0.24 1 1.92

Proximate Analyses, % by wt Ultimate Analyses, % by wt
ncluding ash).
Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

 unit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm